SCHEDULED MAINTENANCE
The interaction of oxotrichlorobis(triphenylphosphine)rhenium(V) or oxotetrachlororhenium (VI) with methyl-lithium gives an air-sensitive but thermally very stable red-purple crystalline solid whose spectroscopic and other properties show it to be ReOMe4.
K. Mertis, J. F. Gibson and G. Wilkinson, J. Chem. Soc., Chem. Commun., 1974, 93a DOI: 10.1039/C3974000093A
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