Journal of the Chemical Society, Chemical Communications

Journal of the Chemical Society, Chemical Communications was published between 1972 - 1995.

Paper

J. Chem. Soc., Chem. Commun., 1995, 2507 - 2508, DOI: 10.1039/C39950002507

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Easy access to C,C-bifunctionalized 1H-phosphirene–tungsten complexes: evidence for ambiphilic reaction behaviour of a phosphanediyl–tungsten complex

Annette Ostrowski, Jörg Jeske, Peter G. Jones and Rainer Streubel

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The 2H-azaphosphirene–tungsten complex 1 reacts with ethoxyacetylene 2a or dimethyl acetylenedicarboxylate 2b to yield C,C-bifunctionalized 1H-phosphirene–tungsten complexes 4a,b; compounds 4a,b are characterized by NMR spectroscopy (¹³C, ³¹P) and complex 4a by single-crystal X-ray diffraction.

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