SCHEDULED MAINTENANCE
Using the reduction of an alkyne to cis-alkene as a hydrogen trap, differentially deuterium labelled formic acid is shown to deliver a pair of hydrogen atoms either from the formyl or the carboxy position, which suggests that palladium diformate is a key intermediate in heterogeneous transfer hydrogenation.
J. Yu and J. B. Spencer, Chem. Commun., 1998, 1935 DOI: 10.1039/A803809K
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