Issue 16, 1998
From the journal:

Chemical Communications

Intramolecular macrocyclization of bis(5-methylthio-1,2-dithiole-3-thione)s with triethyl phosphite. A stereoselective route to macrocyclic (Z)-thioxodesaurines

Sandra Rudershausen,   Hans-Jürgen Holdt,   Helmut Reinke,   Hans-Joachim Drexler,   Joachim Teller  and  Manfred Michalik  

Abstract

Intramolecular macrocyclizations of [oligo(oxyethylene)ethylenedithio]bridged bis(5-methylthio-1,2-dithiole-3- thione)s 5a and b with P(OEt)3 in p-xylene furnished the macrocyclic thioxodesaurin (Z)-6, thioxodesaurin (E)-7 and 1,3-dithiafulvene (E)-8, respectively.

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Article information

DOI
https://doi.org/10.1039/A802658K
Article type
Paper

Chem. Commun., 1998, 1653-1654

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Intramolecular macrocyclization of bis(5-methylthio-1,2-dithiole-3-thione)s with triethyl phosphite. A stereoselective route to macrocyclic (Z)-thioxodesaurines

S. Rudershausen, H. Holdt, H. Reinke, H. Drexler, J. Teller and M. Michalik, Chem. Commun., 1998, 1653 DOI: 10.1039/A802658K

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