#TITLE: GMO Food #DESCRIPTION: Proficiency test, 22 rounds and 38 labs #VARIABLES: Labcode; Numeric code (randomised) for lab identity. R1, R2, etc.; results in successive rounds. #UNITS: Mass fraction of GMO relative to native type Times 10^2 (percent by mass) #REFERENCE_VALUES: None #APPLICATION_SECTOR: Food authenticity #ANALYTE: Roundup Ready (TM) soya #MATRIX_TYPE: Foodstuffs #RATIONALE: Proficiency test #DATA_TYPE: Univariate #DATA_STRUCTURE: Crossed; columns are rounds, rows are laboratories #CONDITIONS: Reproducibility #ORIGIN: Experimental #DATE_OF_ORIGIN: Not disclosed #AUTHOR: GEMMA (FAPAS Secretariat) #AUTHOR_ADDRESS: Central Science Laboratory, Sand Hutton, York YO41 1LZ #LITERATURE_REFERENCES: J AOAC Int, 2006, LabCode R1 R2 R3 R4 R5 R6 R7 R8 R9 R10 R11 R12 R13 R14 R15 R16 R17 R18 R19 R20 R21 R22 1 18 * * 2.2 * 2.02 0.6 0.5 1 3.06 0.77 * 5.54 1.06 6.63 12.23 21.23 1.61 0.11 3.45 0.82 16.2 2 2.1 0.14 * 1.66 0 1.67 0.93 1.6 * 0.24 0.67 0.4 1.3 6.4 6.1 9.1 22 1.4 1.4 2.2 0.24 3.7 3 * 0.15 * * * 2.5 1 3 2 4.9 1.34 0.94 4.75 * 5.2 5 4.7 1.8 1.64 2.4 0.5 * 4 * * * * * 0.58 0.2 0.7 1.9 0.73 0.21 0.34 13.9 * 13.8 12.5 11.8 1.5 1.6 3.9 1.9 5.8 5 * 3.2 * 1.75 3.8 3.05 * * * 4.08 0.78 0.52 6.3 6.28 7 2.1 * * * 1.79 0.98 11.7 6 10.69 1.89 * 3.11 6.4 0.97 0.61 1.08 3.51 2 0.61 0.44 6.3 2.48 2.8 3.6 7.8 0.47 0.56 0.66 0.83 5.7 7 7.37 1 0.01 2.1 4 0.7 * * 1.9 0.75 * * 8.5 4.7 * * * 0.15 0.43 * * * 8 6.4 2.1 * 2.3 6.2 0.81 0.1 0.7 2.4 0.5 0.65 0.65 9.6 12 5.8 10.6 4.9 2.2 0.86 2.2 0.75 4.2 9 5.6 1.96909 * 3.19 * 3.48 * * 5.13 2.91 * * 5.56 8.43 * * 5.7 2.23 3.32 * 1.2 * 10 17.7 2.2 * 2.8 11 2.9 0.8 0.6 * * * * 10.9 * * 4.5 * 0.92 * * * 10.3 11 * * * * 0 * 0.5 1.4 0 * 0.16 0.25 * * 4.4 14.4 3.1 * * * 0.4 * 12 * 4.4 * 2.8 * * * * * * 0.7 0.7 8.18 * 4.6 6.8 6.5 * * * * 2 13 10.4 1.98 * 1.49 2.6 0.71 0.69 1.02 5.98 1.7 0.41 0.3 5.1 0.7 3.2 2.7 7.6 0.13 0.22 0.6 1.5 2.7 14 * * * 2.3 * 2.34 0.4 1.4 2.9 2.2 0.2 0.3 4.7 3.6 2.3 2.6 * 0.26 2 3.36 1.6 * 15 * 1.38 * 3.4 * 1.55 * * * * 1.72 1.96 7.5 7.3 11.34 5.57 3.3 1.01 1.21 2.3 0.56 6 16 17 * * * * 0.6 0.3 0.4 * 0.5 * * * 2.5 6 1 * 0.6 0.5 * * * 17 18 * * * 4 1.1 0.8 2.2 4.4 * 0.83 1.97 4.5 54.4 27.12 23.3 17.3 4.7 4.3 1.44 2.56 12.14 18 8 1.7 0.01 1.8 1.5 0.9 0.42 0.98 * 2.3 0.22 0.3 * 8.4 11.5 7.3 * 1 1.9 2.4 * 6.1 19 12.7 7.47 * 3.27 3.4 * 2.69 2.09 1.8 3.9 0.33 0.89 8.3 2.65 15.5 11 24.1 1.19 1.06 * * * 20 9.6 4 0.02 3.4 * * 0.4 0.9 3.6 * 0.23 0.45 * * 7.1 6.6 8 * * * * * 21 6.2 * 0.05 1.9 4 0.5 0.1 0.6 0.2 20 0.5 0.3 5.5 5.7 5.5 5 8.5 1.6 0.7 * * 6 22 10 0.1 * 1.9 * 3.1 0.4 3.8 4.8 * * * 4.17 * 13.9 10.2 11.7 * * * 0.93 8.4 23 7 1.5 * 4 37534 3 * * * 4 * * * * 5.5 6 9 0.6 0.6 * * * 24 3.1 5 0.5 3.8 1.4 3.5 * * 12.62 * * * * * 22.05 23.39 * * * * 1.4 * 25 15 1.2 * 5 * 1.7 * * * * 3.4 3.4 14 25 * * * 8.7 7.6 4.9 1.1 * 26 * 6.98 0.06 7.7 * * 0.2 0.8 2.2 * 0.1 0.3 7.9 * 0.3 5.1 1.9 * * * * 4.4 27 2.52 1.91 * 2.53 * 10.2 * * * * 1.66 1.3 7.4 25.9 10.5 15 7.58 1.03 1.76 1.9 2.7 52.2 28 14 1.4 * 2.6 3.6 0.8 0.4 0.3 3.48 1.7 1.3 0.9 * 17 * * * * * 5.4 1.1 5.3 29 * * * * * * 0.56 2.16 * 4.7 1.75 0.76 4.8 8 5 6 15.5 1.7 1.1 2.6 1.5 14.8 30 * * * 0.71 0.8 * 0.58 1.1 1.4 3.5 2.1 1.2 * 2.9 1.8 1.2 1.8 0.6 2.3 * * * 31 * * * 4.35 3.2 5.56 0.54 1.35 0.22 1.69 1.55 1.75 5.2 9.62 3.35 4.5 3.07 0.37 0.25 5.31 * * 32 * * * 2.83 * 2.37 * * * 4.44 0.52 1.41 5.3 20.82 1.34 * * 0.78 0.62 * * * 33 * * * * * 1.7 1.1 2.9 * 12.3 0.5 1.1 * 0.8 13.3 13.9 * 2 6.2 * * * 34 * * * * * 0.3 0 0 * * * * * 0.3 0.9 1.4 0.7 * * 4.5 2 26.9 35 * * * * * * 0.55 2.6 * 4.3 1.23 0.67 * 11.5 26 14.7 * 2 1.6 * * * 36 * * * * * * 0.3 0.45 6.4 2.6 0.71 0.41 * 4.6 3.3 4.3 7.4 0.94 0.69 * 1.2 * 37 * * * * * * 0.8 1.4 * 2.1 * * 9.43 5.4 4.5 3 * 0.27 0.86 2.38 * * 38 * * * * * * * * 5.3 1.1 0.32 0.48 10.2 2.78 2.7 6.6 4.87 0.85 0.42 1.52 1.39 3.5