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A peer-reviewed journal highlighting the advancement of analytical technologies for wider application by the international scientific community.
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Highlights in Chemical Technology Issue 1
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Contents list for Analytical Methods, issue 1, 2010
Front cover
Anal. Methods, 2010, 2, 1
DOI: 10.1039/b926529p
Inside front cover
Anal. Methods, 2010, 2, 2
DOI: 10.1039/b926530a
Contents
Anal. Methods, 2010, 2, 3
DOI: 10.1039/b926531g
Editorials
Analytical Methods scope
Anal. Methods, 2010, 2, 11
DOI: 10.1039/b926004h
Analytical Methods– an exciting start!
Anal. Methods, 2010, 2, 12
DOI: 10.1039/b925915p
Welcome to Volume 2, Issue 1, of our new journal, Analytical Methods.
Editorial Board profiles
Anal. Methods, 2010, 2, 14
DOI: 10.1039/b926106k
Analytical Methods introduces the profiles of Editorial Board members for 2010.
Papers
Glycoprotein microarray for the fluorescence detection of antibodies produced as a result of erythropoietin (EPO) abuse
Sinéad M. Hardy, C. Jane Roberts, Pamela R. Brown and David A. Russell,
Anal. Methods, 2010, 2, 17
DOI: 10.1039/b9ay00228f
A glycoprotein microarray has been developed for the detection of antibodies produced in response to illicit doping with recombinant human EPO preparations.
Sol-Gel-Au nano-particle modified carbon paste electrode for potentiometric determination of sub ppb level of Al(III)
Mohammad Hossein Mashhadizadeh and Hadi Khani,
Anal. Methods, 2010, 2, 24
DOI: 10.1039/b9ay00103d
This work describes a new carbon paste electrode modified by Sol-Gel-Au nano-particle (SGAN) in the presence of 2,2
-dihydroxy-1-naphthylidine-1-naphthyl methyl amine (DNMA) as ionophore for determination of Al(III) by potentiometric method.
Laser induced breakdown spectroscopy for rapid identification of different types of paper for forensic application
Arnab Sarkar, Suresh K. Aggarwal and D. Alamelu,
Anal. Methods, 2010, 2, 32
DOI: 10.1039/b9ay00145j
LIBS was applied for rapid identification of paper of different origin, using a statistical analysis approach consisting of linear and rank correlation methodology.
Enantioanalysis of S-Ibuprofen using [5–6] fullerene-C70 and diethyl (1,2-methanofullerene C70)-71-71-dicarboxylate
Raluca-Ioana Stefan-van Staden,
Anal. Methods, 2010, 2, 37
DOI: 10.1039/b9ay00086k
[5–6] Fullerene-C70 and diethyl (1,2-methanofullerene C70)-71-71-dicarboxylate are used as chiral selectors for the construction of enantioselective, potentiometric membrane electrodes used in the enantioanalysis of S-Ibuprofen.
Optimization of Tribenuron-methyl determination by differential pulse polarography using experimental design
Soha Ahmadi, Alireza Ghassempour, Ali Reza Fakhari, Mehdi Jalali-Heravi and Hassan Y. Aboul-Enein,
Anal. Methods, 2010, 2, 41
DOI: 10.1039/b9ay00068b
Differential pulse polarography was applied for the determination of the herbicide Tribenuron-methyl. Various parameters affecting the reduction peak current were simultaneously optimized using experimental design.
Method for cadmium and lead longitudinal profiles determination in hair by solid sampling graphite furnace atomic absorption spectrometry
Cassiana Seimi Nomura and Pedro Vitoriano Oliveira,
Anal. Methods, 2010, 2, 49
DOI: 10.1039/b9ay00050j
This paper describes methods for the direct determination of Cd and Pb in hair segments by solid sampling graphite furnace atomic absorption spectrometry. To distinguish endogenous and exogenous content, strands of hair were washed by using two different procedures.
Application of dispersive liquid–liquid microextraction combined with sweeping micellar electrokinetic chromatography for trace analysis of six carbamate pesticides in apples
Shuaihua Zhang, Chao Li, Shuangju Song, Tao Feng, Chun Wang and Zhi Wang,
Anal. Methods, 2010, 2, 54
DOI: 10.1039/b9ay00115h
A rapid and sensitive method for the multiresidue analysis of six commonly used carbamate pesticides in apples was developed by using dispersive liquid–liquid microextraction coupled with sweeping micellar electrokinetic chromatography.
Diethyl sulfide modified silica and calix[4]pyrrole chelating resin: Synthesis and mercury(II) cation retention properties
Angela Danil de Namor and Ismail Abbas,
Anal. Methods, 2010, 2, 63
DOI: 10.1039/b9ay00135b
This paper describes a novel easy to prepare, and inexpensive calixpyrrole oligomer (R1) for the selective extraction of the Hg2+ cation from polluted water.
Development & validation of an in vitro dissolution method with HPLC analysis for misoprostol in formulated dosage form
Jigar Mehta, Kanhaiyalal Patidar, Vipul Patel, Nayan Kshatri and Niranjan Vyas,
Anal. Methods, 2010, 2, 72
DOI: 10.1039/b9ay00188c
A dissolution test for misoprostol tablets containing 200 
g misoprostol (1% in hydroxypropyl methylcellulose) using a reverse-phase liquid chromatography is developed and validated.
Determination of piroxicam in pharmaceutical preparations by continuous-flow chemiluminescence
J. A. Murillo Pulgarín, A. Alañón Molina and N. Boras,
Anal. Methods, 2010, 2, 76
DOI: 10.1039/b9ay00191c
The method described is based on the recording of the whole chemiluminescence intensity-versus-time profile, based on stopped-flow chemistry; this results in high precision, simplicity and rapidity, it facilitates application to routine analysis.
Determination of free acid in rare earth solution by a fixed pH method
Zhaowu Zhu, Zhenyu Bian and Zhiqi Long,
Anal. Methods, 2010, 2, 82
DOI: 10.1039/b9ay00187e
With Ca–EDTA as the masking agent, a fixed pH method was developed for determination of free acid in the solutions containing a large amount of rare earths by direct titration with standard alkali solution.
Quantitative determination of additives in a commercial electroplating nickel bath by spectrophotometry and multivariate analysis
Maider Vidal, José Manuel Amigo, Rasmus Bro, Miren Ostra and Carlos Ubide.,
Anal. Methods, 2010, 2, 86
DOI: 10.1039/b9ay00158a
In an electroplating nickel bath, a number of organic additives, including Supreme Plus Brightener and A-5(2X), are used to improve the plating process as well as to preserve its durability.
Technical Note
An illustration of the physical robustness of silica monolithic rod columns
Paul Geoffrey Stevenson and Ross Andrew Shalliker,
Anal. Methods, 2010, 2, 93
DOI: 10.1039/b9ay00122k
The robustness of silica based monoliths was tested by removing sections with a saw. The performance of the column remained. This procedure can be used to potentially repair defective monoliths.
Back matter
Anal. Methods, 2010, 2, 96
DOI: 10.1039/b926532p
Back cover
Anal. Methods, 2010, 2, 99
DOI: 10.1039/b926533n
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