SCHEDULED MAINTENANCE
A concentrated solution of K[MnO4] undergoes a ready reaction with acetylacetone, in the absence of any buffer, giving a very high yield of the title compound, [Mn(acac)3]. The pH of the solution, recorded immediately after the formation of crystalline [Mn(acac)3], was found to be ca. 5. Electron impact induced mass spectrometry showed the compound to be monometric.
M. N. Bhattacharjee, M. K. Chaudhuri and D. T. Khathing, J. Chem. Soc., Dalton Trans., 1982, 669 DOI: 10.1039/DT9820000669
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