# Electronic Supplementary Material (ESI) for Physical Chemistry Chemical Physics.
# This journal is © the Owner Societies 2017

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_s
_database_code_depnum_ccdc_archive 'CCDC 1527646'
_audit_update_record             
;
2017-01-16 deposited with the CCDC.
2017-05-02 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C23 H28 B10'
_chemical_formula_weight         412.55

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   P-1

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   10.2378(4)
_cell_length_b                   10.7582(5)
_cell_length_c                   11.6502(6)
_cell_angle_alpha                90.007(2)
_cell_angle_beta                 102.099(2)
_cell_angle_gamma                110.257(2)
_cell_volume                     1173.35(9)
_cell_formula_units_Z            2
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    4314
_cell_measurement_theta_min      0.01
_cell_measurement_theta_max      25.680

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.168
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             432
_exptl_absorpt_coefficient_mu    0.059
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      120
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker D8 VENTURE'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            19120
_diffrn_reflns_av_R_equivalents  0.0512
_diffrn_reflns_av_sigmaI/netI    0.0498
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_theta_min         3.46
_diffrn_reflns_theta_max         25.68
_reflns_number_total             4314
_reflns_number_gt                3257
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0199P)²+3.1168P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         4314
_refine_ls_number_parameters     298
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0931
_refine_ls_R_factor_gt           0.0668
_refine_ls_wR_factor_ref         0.1491
_refine_ls_wR_factor_gt          0.1359
_refine_ls_goodness_of_fit_ref   0.939
_refine_ls_restrained_S_all      0.939
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C3 C 0.1978(3) 0.4578(2) 0.3338(2) 0.0156(5) Uani 1 1 d . . .
C11 C -0.0361(3) 0.1626(2) 0.5273(2) 0.0175(5) Uani 1 1 d . . .
C4 C 0.0487(3) 0.3972(2) 0.3055(2) 0.0162(5) Uani 1 1 d . . .
C1 C 0.2722(3) 0.5652(2) 0.2632(2) 0.0155(5) Uani 1 1 d . . .
C6 C 0.0627(3) 0.2667(2) 0.4735(2) 0.0165(5) Uani 1 1 d . . .
C18 C 0.2772(3) 0.3769(3) 0.1005(2) 0.0187(6) Uani 1 1 d . . .
C2 C 0.3172(3) 0.5214(2) 0.1370(2) 0.0161(5) Uani 1 1 d . . .
C5 C -0.0174(3) 0.3018(2) 0.3746(2) 0.0160(5) Uani 1 1 d . . .
C8 C 0.2764(3) 0.4219(3) 0.4326(2) 0.0212(6) Uani 1 1 d . . .
C7 C 0.2095(3) 0.3268(3) 0.5029(2) 0.0218(6) Uani 1 1 d . . .
C9 C -0.1756(3) 0.2208(3) 0.3573(2) 0.0200(6) Uani 1 1 d . . .
C15 C -0.2888(3) 0.0360(3) 0.4912(2) 0.0244(6) Uani 1 1 d . . .
C10 C -0.1742(3) 0.1342(3) 0.4608(2) 0.0188(6) Uani 1 1 d . . .
C13 C -0.1238(3) -0.0046(3) 0.6559(2) 0.0248(6) Uani 1 1 d . . .
C14 C -0.2614(3) -0.0331(3) 0.5892(2) 0.0257(6) Uani 1 1 d . . .
C12 C -0.0086(3) 0.0942(3) 0.6260(2) 0.0226(6) Uani 1 1 d . . .
C23 C 0.1600(3) 0.3159(3) 0.0088(3) 0.0291(7) Uani 1 1 d . . .
C19 C 0.3594(3) 0.3038(3) 0.1528(2) 0.0275(7) Uani 1 1 d . . .
C16 C -0.2318(3) 0.1357(3) 0.2390(2) 0.0285(7) Uani 1 1 d . . .
C17 C -0.2625(3) 0.3104(3) 0.3648(3) 0.0312(7) Uani 1 1 d . . .
C21 C 0.2083(4) 0.1126(3) 0.0222(3) 0.0370(8) Uani 1 1 d . . .
C22 C 0.1257(3) 0.1840(3) -0.0310(3) 0.0371(8) Uani 1 1 d . . .
C20 C 0.3238(4) 0.1719(3) 0.1133(3) 0.0340(7) Uani 1 1 d . . .
B3 B 0.1797(3) 0.5819(3) 0.1262(2) 0.0170(6) Uani 1 1 d . . .
B7 B 0.4730(3) 0.6392(3) 0.1185(3) 0.0184(6) Uani 1 1 d . . .
B8 B 0.3042(3) 0.6326(3) 0.0341(3) 0.0180(6) Uani 1 1 d . . .
B9 B 0.2512(3) 0.7507(3) 0.1005(3) 0.0204(6) Uani 1 1 d . . .
B4 B 0.2299(3) 0.7055(3) 0.2442(3) 0.0188(6) Uani 1 1 d . . .
B5 B 0.3993(3) 0.7125(3) 0.3289(3) 0.0198(6) Uani 1 1 d . . .
B6 B 0.4486(3) 0.5920(3) 0.2614(3) 0.0177(6) Uani 1 1 d . . .
B12 B 0.4343(3) 0.7882(3) 0.0965(3) 0.0204(6) Uani 1 1 d . . .
B11 B 0.5251(3) 0.7619(3) 0.2381(3) 0.0198(6) Uani 1 1 d . . .
B10 B 0.3900(3) 0.8332(3) 0.2267(2) 0.0218(7) Uani 1 1 d . . .
H12A H 0.1003 0.1052 0.6679 0.033 Uiso 1 1 d R . .
H13 H -0.1168 -0.0736 0.7171 0.033 Uiso 1 1 d R . .
H14 H -0.3496 -0.1148 0.6062 0.033 Uiso 1 1 d R . .
H15 H -0.3952 0.0046 0.4407 0.033 Uiso 1 1 d R . .
H18 H 0.2655 0.2914 0.5780 0.033 Uiso 1 1 d R . .
H2 H 0.3890 0.4726 0.4585 0.033 Uiso 1 1 d R . .
H1 H -0.0035 0.4268 0.2282 0.033 Uiso 1 1 d R . .
H5 H 0.4240 0.7292 0.4265 0.033 Uiso 1 1 d R . .
H10 H 0.4162 0.9409 0.2554 0.033 Uiso 1 1 d R . .
H4 H 0.1480 0.7145 0.2807 0.033 Uiso 1 1 d R . .
H11 H 0.6303 0.8164 0.2809 0.033 Uiso 1 1 d R . .
H12 H 0.4918 0.8684 0.0527 0.033 Uiso 1 1 d R . .
H9 H 0.1912 0.8063 0.0536 0.033 Uiso 1 1 d R . .
H3 H 0.0666 0.4988 0.0914 0.033 Uiso 1 1 d R . .
H7 H 0.5471 0.5979 0.0841 0.033 Uiso 1 1 d R . .
H8 H 0.2633 0.5826 -0.0619 0.033 Uiso 1 1 d R . .
H6 H 0.4887 0.5199 0.3045 0.033 Uiso 1 1 d R . .
H23 H 0.0933 0.3692 -0.0362 0.033 Uiso 1 1 d R . .
H22 H 0.0291 0.1396 -0.1015 0.033 Uiso 1 1 d R . .
H21 H 0.1752 0.0170 -0.0123 0.033 Uiso 1 1 d R . .
H20 H 0.3841 0.1186 0.1579 0.033 Uiso 1 1 d R . .
H19 H 0.4560 0.3556 0.2179 0.033 Uiso 1 1 d R . .
H30 H -0.1750 0.0780 0.2273 0.033 Uiso 1 1 d R . .
H31 H -0.2231 0.2009 0.1744 0.033 Uiso 1 1 d R . .
H32 H -0.3364 0.0914 0.2308 0.033 Uiso 1 1 d R . .
H33 H -0.3783 0.2451 0.3605 0.033 Uiso 1 1 d R . .
H34 H -0.2198 0.3739 0.4442 0.033 Uiso 1 1 d R . .
H35 H -0.2661 0.3676 0.2899 0.033 Uiso 1 1 d R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C3 C8 1.397(3) . ?
C3 C4 1.401(3) . ?
C3 C1 1.498(3) . ?
C11 C10 1.391(4) . ?
C11 C12 1.397(4) . ?
C11 C6 1.467(3) . ?
C4 C5 1.381(3) . ?
C4 H1 1.0550 . ?
C1 B4 1.711(4) . ?
C1 B5 1.717(4) . ?
C1 B3 1.720(4) . ?
C1 B6 1.733(4) . ?
C1 C2 1.741(3) . ?
C6 C7 1.380(4) . ?
C6 C5 1.400(3) . ?
C18 C23 1.389(4) . ?
C18 C19 1.394(4) . ?
C18 C2 1.500(4) . ?
C2 B8 1.711(4) . ?
C2 B7 1.715(4) . ?
C2 B6 1.722(4) . ?
C2 B3 1.726(4) . ?
C5 C9 1.520(3) . ?
C8 C7 1.391(4) . ?
C8 H2 1.0659 . ?
C7 H18 1.0867 . ?
C9 C10 1.524(3) . ?
C9 C17 1.535(4) . ?
C9 C16 1.540(4) . ?
C15 C10 1.391(4) . ?
C15 C14 1.395(4) . ?
C15 H15 1.0596 . ?
C13 C14 1.387(4) . ?
C13 C12 1.395(4) . ?
C13 H13 1.0394 . ?
C14 H14 1.0734 . ?
C12 H12A 1.0840 . ?
C23 C22 1.392(4) . ?
C23 H23 1.0914 . ?
C19 C20 1.389(4) . ?
C19 H19 1.0809 . ?
C16 H30 1.0131 . ?
C16 H31 1.0250 . ?
C16 H32 0.9932 . ?
C17 H33 1.1402 . ?
C17 H34 1.0656 . ?
C17 H35 1.0698 . ?
C21 C20 1.373(5) . ?
C21 C22 1.386(5) . ?
C21 H21 1.0174 . ?
C22 H22 1.1012 . ?
C20 H20 1.0436 . ?
B3 B9 1.759(4) . ?
B3 B4 1.776(4) . ?
B3 B8 1.779(4) . ?
B3 H3 1.1790 . ?
B7 B8 1.778(4) . ?
B7 B11 1.780(4) . ?
B7 B6 1.783(4) . ?
B7 B12 1.786(4) . ?
B7 H7 1.1373 . ?
B8 B12 1.776(4) . ?
B8 B9 1.777(4) . ?
B8 H8 1.1675 . ?
B9 B4 1.780(4) . ?
B9 B12 1.786(4) . ?
B9 B10 1.795(4) . ?
B9 H9 1.0716 . ?
B4 B5 1.783(4) . ?
B4 B10 1.788(4) . ?
B4 H4 1.0486 . ?
B5 B10 1.775(4) . ?
B5 B11 1.777(4) . ?
B5 B6 1.782(4) . ?
B5 H5 1.1119 . ?
B6 B11 1.768(4) . ?
B6 H6 1.0748 . ?
B12 B10 1.783(4) . ?
B12 B11 1.791(4) . ?
B12 H12 1.0611 . ?
B11 B10 1.783(4) . ?
B11 H11 1.0437 . ?
B10 H10 1.1288 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C8 C3 C4 119.2(2) . . ?
C8 C3 C1 120.0(2) . . ?
C4 C3 C1 120.7(2) . . ?
C10 C11 C12 121.3(2) . . ?
C10 C11 C6 108.7(2) . . ?
C12 C11 C6 130.1(2) . . ?
C5 C4 C3 119.4(2) . . ?
C5 C4 H1 125.3 . . ?
C3 C4 H1 115.1 . . ?
C3 C1 B4 121.3(2) . . ?
C3 C1 B5 121.8(2) . . ?
B4 C1 B5 62.69(17) . . ?
C3 C1 B3 118.3(2) . . ?
B4 C1 B3 62.34(16) . . ?
B5 C1 B3 112.8(2) . . ?
C3 C1 B6 118.6(2) . . ?
B4 C1 B6 113.06(19) . . ?
B5 C1 B6 62.21(17) . . ?
B3 C1 B6 110.48(19) . . ?
C3 C1 C2 119.1(2) . . ?
B4 C1 C2 109.80(18) . . ?
B5 C1 C2 109.28(18) . . ?
B3 C1 C2 59.83(15) . . ?
B6 C1 C2 59.42(15) . . ?
C7 C6 C5 120.2(2) . . ?
C7 C6 C11 131.6(2) . . ?
C5 C6 C11 108.1(2) . . ?
C23 C18 C19 119.0(3) . . ?
C23 C18 C2 119.6(2) . . ?
C19 C18 C2 121.4(2) . . ?
C18 C2 B8 120.8(2) . . ?
C18 C2 B7 122.2(2) . . ?
B8 C2 B7 62.51(16) . . ?
C18 C2 B6 119.5(2) . . ?
B8 C2 B6 113.0(2) . . ?
B7 C2 B6 62.51(16) . . ?
C18 C2 B3 117.2(2) . . ?
B8 C2 B3 62.34(16) . . ?
B7 C2 B3 113.0(2) . . ?
B6 C2 B3 110.7(2) . . ?
C18 C2 C1 118.95(19) . . ?
B8 C2 C1 109.60(19) . . ?
B7 C2 C1 110.07(19) . . ?
B6 C2 C1 60.04(15) . . ?
B3 C2 C1 59.49(15) . . ?
C4 C5 C6 120.8(2) . . ?
C4 C5 C9 128.0(2) . . ?
C6 C5 C9 111.2(2) . . ?
C7 C8 C3 121.2(2) . . ?
C7 C8 H2 119.0 . . ?
C3 C8 H2 119.7 . . ?
C6 C7 C8 119.1(2) . . ?
C6 C7 H18 116.4 . . ?
C8 C7 H18 124.4 . . ?
C5 C9 C10 100.9(2) . . ?
C5 C9 C17 111.3(2) . . ?
C10 C9 C17 111.9(2) . . ?
C5 C9 C16 110.7(2) . . ?
C10 C9 C16 111.2(2) . . ?
C17 C9 C16 110.5(2) . . ?
C10 C15 C14 118.3(3) . . ?
C10 C15 H15 124.1 . . ?
C14 C15 H15 117.3 . . ?
C15 C10 C11 120.5(2) . . ?
C15 C10 C9 128.4(2) . . ?
C11 C10 C9 111.1(2) . . ?
C14 C13 C12 120.6(2) . . ?
C14 C13 H13 112.8 . . ?
C12 C13 H13 125.8 . . ?
C13 C14 C15 121.3(2) . . ?
C13 C14 H14 121.4 . . ?
C15 C14 H14 117.1 . . ?
C13 C12 C11 118.1(3) . . ?
C13 C12 H12A 120.7 . . ?
C11 C12 H12A 120.3 . . ?
C18 C23 C22 120.6(3) . . ?
C18 C23 H23 121.9 . . ?
C22 C23 H23 117.5 . . ?
C20 C19 C18 120.2(3) . . ?
C20 C19 H19 121.8 . . ?
C18 C19 H19 117.8 . . ?
C9 C16 H30 114.0 . . ?
C9 C16 H31 106.5 . . ?
H30 C16 H31 107.3 . . ?
C9 C16 H32 106.3 . . ?
H30 C16 H32 117.6 . . ?
H31 C16 H32 104.3 . . ?
C9 C17 H33 108.8 . . ?
C9 C17 H34 110.7 . . ?
H33 C17 H34 110.4 . . ?
C9 C17 H35 111.0 . . ?
H33 C17 H35 105.1 . . ?
H34 C17 H35 110.6 . . ?
C20 C21 C22 120.1(3) . . ?
C20 C21 H21 125.6 . . ?
C22 C21 H21 114.3 . . ?
C21 C22 C23 119.7(3) . . ?
C21 C22 H22 122.8 . . ?
C23 C22 H22 117.4 . . ?
C21 C20 C19 120.5(3) . . ?
C21 C20 H20 121.5 . . ?
C19 C20 H20 118.0 . . ?
C1 B3 C2 60.68(15) . . ?
C1 B3 B9 106.2(2) . . ?
C2 B3 B9 106.0(2) . . ?
C1 B3 B4 58.56(15) . . ?
C2 B3 B4 107.5(2) . . ?
B9 B3 B4 60.47(17) . . ?
C1 B3 B8 107.4(2) . . ?
C2 B3 B8 58.40(15) . . ?
B9 B3 B8 60.30(16) . . ?
B4 B3 B8 109.0(2) . . ?
C1 B3 H3 116.1 . . ?
C2 B3 H3 112.4 . . ?
B9 B3 H3 132.6 . . ?
B4 B3 H3 127.4 . . ?
B8 B3 H3 120.6 . . ?
C2 B7 B8 58.63(15) . . ?
C2 B7 B11 105.6(2) . . ?
B8 B7 B11 107.8(2) . . ?
C2 B7 B6 58.93(15) . . ?
B8 B7 B6 107.0(2) . . ?
B11 B7 B6 59.49(16) . . ?
C2 B7 B12 105.4(2) . . ?
B8 B7 B12 59.79(16) . . ?
B11 B7 B12 60.28(17) . . ?
B6 B7 B12 107.3(2) . . ?
C2 B7 H7 114.7 . . ?
B8 B7 H7 123.7 . . ?
B11 B7 H7 125.7 . . ?
B6 B7 H7 113.9 . . ?
B12 B7 H7 133.0 . . ?
C2 B8 B12 106.0(2) . . ?
C2 B8 B9 105.94(19) . . ?
B12 B8 B9 60.34(17) . . ?
C2 B8 B7 58.86(15) . . ?
B12 B8 B7 60.35(17) . . ?
B9 B8 B7 108.5(2) . . ?
C2 B8 B3 59.26(15) . . ?
B12 B8 B3 107.4(2) . . ?
B9 B8 B3 59.31(16) . . ?
B7 B8 B3 107.6(2) . . ?
C2 B8 H8 112.5 . . ?
B12 B8 H8 132.6 . . ?
B9 B8 H8 128.6 . . ?
B7 B8 H8 120.0 . . ?
B3 B8 H8 115.5 . . ?
B3 B9 B8 60.40(16) . . ?
B3 B9 B4 60.22(16) . . ?
B8 B9 B4 108.9(2) . . ?
B3 B9 B12 107.9(2) . . ?
B8 B9 B12 59.80(17) . . ?
B4 B9 B12 108.3(2) . . ?
B3 B9 B10 107.6(2) . . ?
B8 B9 B10 107.7(2) . . ?
B4 B9 B10 60.01(16) . . ?
B12 B9 B10 59.74(16) . . ?
B3 B9 H9 125.0 . . ?
B8 B9 H9 125.0 . . ?
B4 B9 H9 119.5 . . ?
B12 B9 H9 120.8 . . ?
B10 B9 H9 117.8 . . ?
C1 B4 B3 59.10(15) . . ?
C1 B4 B9 105.8(2) . . ?
B3 B4 B9 59.31(16) . . ?
C1 B4 B5 58.82(16) . . ?
B3 B4 B5 107.1(2) . . ?
B9 B4 B5 107.8(2) . . ?
C1 B4 B10 105.5(2) . . ?
B3 B4 B10 107.2(2) . . ?
B9 B4 B10 60.40(16) . . ?
B5 B4 B10 59.61(16) . . ?
C1 B4 H4 119.0 . . ?
B3 B4 H4 117.1 . . ?
B9 B4 H4 123.4 . . ?
B5 B4 H4 124.0 . . ?
B10 B4 H4 128.4 . . ?
C1 B5 B10 105.8(2) . . ?
C1 B5 B11 106.0(2) . . ?
B10 B5 B11 60.24(16) . . ?
C1 B5 B6 59.34(16) . . ?
B10 B5 B6 107.6(2) . . ?
B11 B5 B6 59.56(17) . . ?
C1 B5 B4 58.49(16) . . ?
B10 B5 B4 60.33(16) . . ?
B11 B5 B4 108.3(2) . . ?
B6 B5 B4 107.4(2) . . ?
C1 B5 H5 118.6 . . ?
B10 B5 H5 126.2 . . ?
B11 B5 H5 125.9 . . ?
B6 B5 H5 120.2 . . ?
B4 B5 H5 120.1 . . ?
C2 B6 C1 60.54(15) . . ?
C2 B6 B11 105.8(2) . . ?
C1 B6 B11 105.8(2) . . ?
C2 B6 B5 107.2(2) . . ?
C1 B6 B5 58.45(16) . . ?
B11 B6 B5 60.08(17) . . ?
C2 B6 B7 58.56(15) . . ?
C1 B6 B7 107.34(19) . . ?
B11 B6 B7 60.17(17) . . ?
B5 B6 B7 108.7(2) . . ?
C2 B6 H6 111.5 . . ?
C1 B6 H6 114.2 . . ?
B11 B6 H6 134.9 . . ?
B5 B6 H6 127.0 . . ?
B7 B6 H6 122.0 . . ?
B8 B12 B10 108.3(2) . . ?
B8 B12 B9 59.86(17) . . ?
B10 B12 B9 60.38(16) . . ?
B8 B12 B7 59.86(16) . . ?
B10 B12 B7 108.0(2) . . ?
B9 B12 B7 107.7(2) . . ?
B8 B12 B11 107.4(2) . . ?
B10 B12 B11 59.83(16) . . ?
B9 B12 B11 107.6(2) . . ?
B7 B12 B11 59.69(17) . . ?
B8 B12 H12 128.4 . . ?
B10 B12 H12 115.8 . . ?
B9 B12 H12 123.3 . . ?
B7 B12 H12 124.1 . . ?
B11 B12 H12 117.0 . . ?
B6 B11 B5 60.35(17) . . ?
B6 B11 B7 60.33(16) . . ?
B5 B11 B7 109.0(2) . . ?
B6 B11 B10 107.8(2) . . ?
B5 B11 B10 59.81(16) . . ?
B7 B11 B10 108.3(2) . . ?
B6 B11 B12 107.8(2) . . ?
B5 B11 B12 108.0(2) . . ?
B7 B11 B12 60.03(17) . . ?
B10 B11 B12 59.88(16) . . ?
B6 B11 H11 119.9 . . ?
B5 B11 H11 116.1 . . ?
B7 B11 H11 125.3 . . ?
B10 B11 H11 120.2 . . ?
B12 B11 H11 126.2 . . ?
B5 B10 B11 59.95(16) . . ?
B5 B10 B12 108.4(2) . . ?
B11 B10 B12 60.28(16) . . ?
B5 B10 B4 60.05(16) . . ?
B11 B10 B4 107.9(2) . . ?
B12 B10 B4 108.0(2) . . ?
B5 B10 B9 107.54(19) . . ?
B11 B10 B9 107.6(2) . . ?
B12 B10 B9 59.88(16) . . ?
B4 B10 B9 59.59(16) . . ?
B5 B10 H10 122.4 . . ?
B11 B10 H10 121.9 . . ?
B12 B10 H10 120.7 . . ?
B4 B10 H10 122.2 . . ?
B9 B10 H10 121.8 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C8 C3 C4 C5 -1.0(4) . . . . ?
C1 C3 C4 C5 -177.7(2) . . . . ?
C8 C3 C1 B4 -120.7(3) . . . . ?
C4 C3 C1 B4 56.0(3) . . . . ?
C8 C3 C1 B5 -45.4(3) . . . . ?
C4 C3 C1 B5 131.2(3) . . . . ?
C8 C3 C1 B3 166.1(2) . . . . ?
C4 C3 C1 B3 -17.2(3) . . . . ?
C8 C3 C1 B6 27.9(3) . . . . ?
C4 C3 C1 B6 -155.4(2) . . . . ?
C8 C3 C1 C2 96.8(3) . . . . ?
C4 C3 C1 C2 -86.5(3) . . . . ?
C10 C11 C6 C7 -178.1(3) . . . . ?
C12 C11 C6 C7 0.4(5) . . . . ?
C10 C11 C6 C5 0.6(3) . . . . ?
C12 C11 C6 C5 179.1(3) . . . . ?
C23 C18 C2 B8 -38.6(3) . . . . ?
C19 C18 C2 B8 138.2(3) . . . . ?
C23 C18 C2 B7 -113.5(3) . . . . ?
C19 C18 C2 B7 63.3(3) . . . . ?
C23 C18 C2 B6 172.2(2) . . . . ?
C19 C18 C2 B6 -11.0(4) . . . . ?
C23 C18 C2 B3 33.9(3) . . . . ?
C19 C18 C2 B3 -149.3(2) . . . . ?
C23 C18 C2 C1 102.3(3) . . . . ?
C19 C18 C2 C1 -80.9(3) . . . . ?
C3 C1 C2 C18 1.4(3) . . . . ?
B4 C1 C2 C18 -145.0(2) . . . . ?
B5 C1 C2 C18 148.0(2) . . . . ?
B3 C1 C2 C18 -106.2(2) . . . . ?
B6 C1 C2 C18 109.3(2) . . . . ?
C3 C1 C2 B8 146.2(2) . . . . ?
B4 C1 C2 B8 -0.2(3) . . . . ?
B5 C1 C2 B8 -67.2(2) . . . . ?
B3 C1 C2 B8 38.57(19) . . . . ?
B6 C1 C2 B8 -105.9(2) . . . . ?
C3 C1 C2 B7 -146.8(2) . . . . ?
B4 C1 C2 B7 66.8(2) . . . . ?
B5 C1 C2 B7 -0.2(3) . . . . ?
B3 C1 C2 B7 105.5(2) . . . . ?
B6 C1 C2 B7 -38.93(19) . . . . ?
C3 C1 C2 B6 -107.9(2) . . . . ?
B4 C1 C2 B6 105.7(2) . . . . ?
B5 C1 C2 B6 38.71(19) . . . . ?
B3 C1 C2 B6 144.5(2) . . . . ?
C3 C1 C2 B3 107.7(2) . . . . ?
B4 C1 C2 B3 -38.74(19) . . . . ?
B5 C1 C2 B3 -105.7(2) . . . . ?
B6 C1 C2 B3 -144.5(2) . . . . ?
C3 C4 C5 C6 1.0(4) . . . . ?
C3 C4 C5 C9 -177.6(2) . . . . ?
C7 C6 C5 C4 -0.3(4) . . . . ?
C11 C6 C5 C4 -179.2(2) . . . . ?
C7 C6 C5 C9 178.5(2) . . . . ?
C11 C6 C5 C9 -0.4(3) . . . . ?
C4 C3 C8 C7 0.3(4) . . . . ?
C1 C3 C8 C7 177.0(2) . . . . ?
C5 C6 C7 C8 -0.4(4) . . . . ?
C11 C6 C7 C8 178.2(3) . . . . ?
C3 C8 C7 C6 0.4(4) . . . . ?
C4 C5 C9 C10 178.7(3) . . . . ?
C6 C5 C9 C10 0.0(3) . . . . ?
C4 C5 C9 C17 -62.4(3) . . . . ?
C6 C5 C9 C17 118.9(2) . . . . ?
C4 C5 C9 C16 60.9(3) . . . . ?
C6 C5 C9 C16 -117.8(2) . . . . ?
C14 C15 C10 C11 -0.3(4) . . . . ?
C14 C15 C10 C9 178.6(3) . . . . ?
C12 C11 C10 C15 -0.2(4) . . . . ?
C6 C11 C10 C15 178.4(2) . . . . ?
C12 C11 C10 C9 -179.3(2) . . . . ?
C6 C11 C10 C9 -0.6(3) . . . . ?
C5 C9 C10 C15 -178.5(3) . . . . ?
C17 C9 C10 C15 63.0(4) . . . . ?
C16 C9 C10 C15 -61.1(4) . . . . ?
C5 C9 C10 C11 0.4(3) . . . . ?
C17 C9 C10 C11 -118.1(3) . . . . ?
C16 C9 C10 C11 117.9(2) . . . . ?
C12 C13 C14 C15 -0.3(4) . . . . ?
C10 C15 C14 C13 0.5(4) . . . . ?
C14 C13 C12 C11 -0.2(4) . . . . ?
C10 C11 C12 C13 0.5(4) . . . . ?
C6 C11 C12 C13 -177.9(3) . . . . ?
C19 C18 C23 C22 -0.5(4) . . . . ?
C2 C18 C23 C22 176.3(3) . . . . ?
C23 C18 C19 C20 0.0(4) . . . . ?
C2 C18 C19 C20 -176.8(2) . . . . ?
C20 C21 C22 C23 -0.3(5) . . . . ?
C18 C23 C22 C21 0.7(5) . . . . ?
C22 C21 C20 C19 -0.3(5) . . . . ?
C18 C19 C20 C21 0.5(4) . . . . ?
C3 C1 B3 C2 -109.1(2) . . . . ?
B4 C1 B3 C2 138.3(2) . . . . ?
B5 C1 B3 C2 99.8(2) . . . . ?
B6 C1 B3 C2 32.29(19) . . . . ?
C3 C1 B3 B9 151.3(2) . . . . ?
B4 C1 B3 B9 38.75(19) . . . . ?
B5 C1 B3 B9 0.2(3) . . . . ?
B6 C1 B3 B9 -67.3(2) . . . . ?
C2 C1 B3 B9 -99.6(2) . . . . ?
C3 C1 B3 B4 112.6(2) . . . . ?
B5 C1 B3 B4 -38.6(2) . . . . ?
B6 C1 B3 B4 -106.0(2) . . . . ?
C2 C1 B3 B4 -138.3(2) . . . . ?
C3 C1 B3 B8 -145.4(2) . . . . ?
B4 C1 B3 B8 102.0(2) . . . . ?
B5 C1 B3 B8 63.5(3) . . . . ?
B6 C1 B3 B8 -4.0(3) . . . . ?
C2 C1 B3 B8 -36.30(18) . . . . ?
C18 C2 B3 C1 109.2(2) . . . . ?
B8 C2 B3 C1 -138.5(2) . . . . ?
B7 C2 B3 C1 -100.5(2) . . . . ?
B6 C2 B3 C1 -32.58(18) . . . . ?
C18 C2 B3 B9 -150.9(2) . . . . ?
B8 C2 B3 B9 -38.54(19) . . . . ?
B7 C2 B3 B9 -0.6(3) . . . . ?
B6 C2 B3 B9 67.3(2) . . . . ?
C1 C2 B3 B9 99.9(2) . . . . ?
C18 C2 B3 B4 145.7(2) . . . . ?
B8 C2 B3 B4 -102.0(2) . . . . ?
B7 C2 B3 B4 -64.0(2) . . . . ?
B6 C2 B3 B4 3.9(3) . . . . ?
C1 C2 B3 B4 36.48(17) . . . . ?
C18 C2 B3 B8 -112.3(2) . . . . ?
B7 C2 B3 B8 37.9(2) . . . . ?
B6 C2 B3 B8 105.9(2) . . . . ?
C1 C2 B3 B8 138.5(2) . . . . ?
C18 C2 B7 B8 110.7(3) . . . . ?
B6 C2 B7 B8 -140.1(2) . . . . ?
B3 C2 B7 B8 -37.9(2) . . . . ?
C1 C2 B7 B8 -102.3(2) . . . . ?
C18 C2 B7 B11 -147.6(2) . . . . ?
B8 C2 B7 B11 101.7(2) . . . . ?
B6 C2 B7 B11 -38.46(19) . . . . ?
B3 C2 B7 B11 63.8(2) . . . . ?
C1 C2 B7 B11 -0.6(3) . . . . ?
C18 C2 B7 B6 -109.2(3) . . . . ?
B8 C2 B7 B6 140.1(2) . . . . ?
B3 C2 B7 B6 102.3(2) . . . . ?
C1 C2 B7 B6 37.86(18) . . . . ?
C18 C2 B7 B12 149.6(2) . . . . ?
B8 C2 B7 B12 38.88(19) . . . . ?
B6 C2 B7 B12 -101.2(2) . . . . ?
B3 C2 B7 B12 1.0(3) . . . . ?
C1 C2 B7 B12 -63.4(2) . . . . ?
C18 C2 B8 B12 -152.2(2) . . . . ?
B7 C2 B8 B12 -39.28(19) . . . . ?
B6 C2 B8 B12 -1.1(3) . . . . ?
B3 C2 B8 B12 101.1(2) . . . . ?
C1 C2 B8 B12 63.8(2) . . . . ?
C18 C2 B8 B9 144.8(2) . . . . ?
B7 C2 B8 B9 -102.3(2) . . . . ?
B6 C2 B8 B9 -64.1(3) . . . . ?
B3 C2 B8 B9 38.06(19) . . . . ?
C1 C2 B8 B9 0.7(3) . . . . ?
C18 C2 B8 B7 -112.9(3) . . . . ?
B6 C2 B8 B7 38.2(2) . . . . ?
B3 C2 B8 B7 140.4(2) . . . . ?
C1 C2 B8 B7 103.0(2) . . . . ?
C18 C2 B8 B3 106.7(2) . . . . ?
B7 C2 B8 B3 -140.4(2) . . . . ?
B6 C2 B8 B3 -102.2(2) . . . . ?
C1 C2 B8 B3 -37.33(18) . . . . ?
B11 B7 B8 C2 -97.7(2) . . . . ?
B6 B7 B8 C2 -35.05(19) . . . . ?
B12 B7 B8 C2 -135.5(2) . . . . ?
C2 B7 B8 B12 135.5(2) . . . . ?
B11 B7 B8 B12 37.83(19) . . . . ?
B6 B7 B8 B12 100.5(2) . . . . ?
C2 B7 B8 B9 97.8(2) . . . . ?
B11 B7 B8 B9 0.1(3) . . . . ?
B6 B7 B8 B9 62.8(2) . . . . ?
B12 B7 B8 B9 -37.72(19) . . . . ?
C2 B7 B8 B3 35.12(19) . . . . ?
B11 B7 B8 B3 -62.6(2) . . . . ?
B6 B7 B8 B3 0.1(3) . . . . ?
B12 B7 B8 B3 -100.4(2) . . . . ?
C1 B3 B8 C2 37.30(18) . . . . ?
B9 B3 B8 C2 136.4(2) . . . . ?
B4 B3 B8 C2 99.3(2) . . . . ?
C1 B3 B8 B12 -61.3(2) . . . . ?
C2 B3 B8 B12 -98.6(2) . . . . ?
B9 B3 B8 B12 37.87(19) . . . . ?
B4 B3 B8 B12 0.7(3) . . . . ?
C1 B3 B8 B9 -99.1(2) . . . . ?
C2 B3 B8 B9 -136.4(2) . . . . ?
B4 B3 B8 B9 -37.2(2) . . . . ?
C1 B3 B8 B7 2.4(3) . . . . ?
C2 B3 B8 B7 -34.95(19) . . . . ?
B9 B3 B8 B7 101.5(2) . . . . ?
B4 B3 B8 B7 64.3(3) . . . . ?
C1 B3 B9 B8 101.1(2) . . . . ?
C2 B3 B9 B8 37.66(18) . . . . ?
B4 B3 B9 B8 139.0(2) . . . . ?
C1 B3 B9 B4 -37.86(19) . . . . ?
C2 B3 B9 B4 -101.3(2) . . . . ?
B8 B3 B9 B4 -139.0(2) . . . . ?
C1 B3 B9 B12 63.4(2) . . . . ?
C2 B3 B9 B12 -0.1(3) . . . . ?
B4 B3 B9 B12 101.2(2) . . . . ?
B8 B3 B9 B12 -37.7(2) . . . . ?
C1 B3 B9 B10 0.3(3) . . . . ?
C2 B3 B9 B10 -63.1(2) . . . . ?
B4 B3 B9 B10 38.18(19) . . . . ?
B8 B3 B9 B10 -100.8(2) . . . . ?
C2 B8 B9 B3 -38.04(18) . . . . ?
B12 B8 B9 B3 -137.6(2) . . . . ?
B7 B8 B9 B3 -99.9(2) . . . . ?
C2 B8 B9 B4 -1.0(3) . . . . ?
B12 B8 B9 B4 -100.6(2) . . . . ?
B7 B8 B9 B4 -62.9(3) . . . . ?
B3 B8 B9 B4 37.0(2) . . . . ?
C2 B8 B9 B12 99.6(2) . . . . ?
B7 B8 B9 B12 37.72(19) . . . . ?
B3 B8 B9 B12 137.6(2) . . . . ?
C2 B8 B9 B10 62.6(2) . . . . ?
B12 B8 B9 B10 -37.03(19) . . . . ?
B7 B8 B9 B10 0.7(3) . . . . ?
B3 B8 B9 B10 100.6(2) . . . . ?
C3 C1 B4 B3 -107.9(2) . . . . ?
B5 C1 B4 B3 139.7(2) . . . . ?
B6 C1 B4 B3 101.9(2) . . . . ?
C2 C1 B4 B3 37.65(18) . . . . ?
C3 C1 B4 B9 -146.0(2) . . . . ?
B5 C1 B4 B9 101.6(2) . . . . ?
B3 C1 B4 B9 -38.11(19) . . . . ?
B6 C1 B4 B9 63.8(2) . . . . ?
C2 C1 B4 B9 -0.5(3) . . . . ?
C3 C1 B4 B5 112.4(3) . . . . ?
B3 C1 B4 B5 -139.7(2) . . . . ?
B6 C1 B4 B5 -37.8(2) . . . . ?
C2 C1 B4 B5 -102.1(2) . . . . ?
C3 C1 B4 B10 151.0(2) . . . . ?
B5 C1 B4 B10 38.63(18) . . . . ?
B3 C1 B4 B10 -101.1(2) . . . . ?
B6 C1 B4 B10 0.8(3) . . . . ?
C2 C1 B4 B10 -63.4(2) . . . . ?
C2 B3 B4 C1 -37.42(18) . . . . ?
B9 B3 B4 C1 -136.3(2) . . . . ?
B8 B3 B4 C1 -99.2(2) . . . . ?
C1 B3 B4 B9 136.3(2) . . . . ?
C2 B3 B4 B9 98.9(2) . . . . ?
B8 B3 B4 B9 37.1(2) . . . . ?
C1 B3 B4 B5 35.37(18) . . . . ?
C2 B3 B4 B5 -2.1(3) . . . . ?
B9 B3 B4 B5 -101.0(2) . . . . ?
B8 B3 B4 B5 -63.9(2) . . . . ?
C1 B3 B4 B10 98.1(2) . . . . ?
C2 B3 B4 B10 60.6(2) . . . . ?
B9 B3 B4 B10 -38.26(19) . . . . ?
B8 B3 B4 B10 -1.2(3) . . . . ?
B3 B9 B4 C1 38.01(19) . . . . ?
B8 B9 B4 C1 0.9(3) . . . . ?
B12 B9 B4 C1 -62.6(3) . . . . ?
B10 B9 B4 C1 -99.1(2) . . . . ?
B8 B9 B4 B3 -37.1(2) . . . . ?
B12 B9 B4 B3 -100.6(2) . . . . ?
B10 B9 B4 B3 -137.1(2) . . . . ?
B3 B9 B4 B5 99.7(2) . . . . ?
B8 B9 B4 B5 62.6(3) . . . . ?
B12 B9 B4 B5 -0.9(3) . . . . ?
B10 B9 B4 B5 -37.45(19) . . . . ?
B3 B9 B4 B10 137.1(2) . . . . ?
B8 B9 B4 B10 100.0(2) . . . . ?
B12 B9 B4 B10 36.6(2) . . . . ?
C3 C1 B5 B10 -150.6(2) . . . . ?
B4 C1 B5 B10 -39.04(19) . . . . ?
B3 C1 B5 B10 -0.6(3) . . . . ?
B6 C1 B5 B10 101.3(2) . . . . ?
C2 C1 B5 B10 63.9(2) . . . . ?
C3 C1 B5 B11 146.5(2) . . . . ?
B4 C1 B5 B11 -102.0(2) . . . . ?
B3 C1 B5 B11 -63.5(3) . . . . ?
B6 C1 B5 B11 38.43(19) . . . . ?
C2 C1 B5 B11 0.9(3) . . . . ?
C3 C1 B5 B6 108.0(3) . . . . ?
B4 C1 B5 B6 -140.4(2) . . . . ?
B3 C1 B5 B6 -102.0(2) . . . . ?
C2 C1 B5 B6 -37.48(18) . . . . ?
C3 C1 B5 B4 -111.6(3) . . . . ?
B3 C1 B5 B4 38.4(2) . . . . ?
B6 C1 B5 B4 140.4(2) . . . . ?
C2 C1 B5 B4 102.9(2) . . . . ?
B3 B4 B5 C1 -35.49(18) . . . . ?
B9 B4 B5 C1 -98.0(2) . . . . ?
B10 B4 B5 C1 -135.8(2) . . . . ?
C1 B4 B5 B10 135.8(2) . . . . ?
B3 B4 B5 B10 100.3(2) . . . . ?
B9 B4 B5 B10 37.80(19) . . . . ?
C1 B4 B5 B11 98.0(2) . . . . ?
B3 B4 B5 B11 62.5(3) . . . . ?
B9 B4 B5 B11 0.0(3) . . . . ?
B10 B4 B5 B11 -37.80(19) . . . . ?
C1 B4 B5 B6 35.08(18) . . . . ?
B3 B4 B5 B6 -0.4(3) . . . . ?
B9 B4 B5 B6 -62.9(2) . . . . ?
B10 B4 B5 B6 -100.7(2) . . . . ?
C18 C2 B6 C1 -108.4(2) . . . . ?
B8 C2 B6 C1 100.1(2) . . . . ?
B7 C2 B6 C1 138.3(2) . . . . ?
B3 C2 B6 C1 32.38(18) . . . . ?
C18 C2 B6 B11 152.1(2) . . . . ?
B8 C2 B6 B11 0.7(3) . . . . ?
B7 C2 B6 B11 38.83(19) . . . . ?
B3 C2 B6 B11 -67.1(2) . . . . ?
C1 C2 B6 B11 -99.5(2) . . . . ?
C18 C2 B6 B5 -144.9(2) . . . . ?
B8 C2 B6 B5 63.6(2) . . . . ?
B7 C2 B6 B5 101.8(2) . . . . ?
B3 C2 B6 B5 -4.1(3) . . . . ?
C1 C2 B6 B5 -36.52(18) . . . . ?
C18 C2 B6 B7 113.3(2) . . . . ?
B8 C2 B6 B7 -38.2(2) . . . . ?
B3 C2 B6 B7 -105.9(2) . . . . ?
C1 C2 B6 B7 -138.3(2) . . . . ?
C3 C1 B6 C2 108.8(2) . . . . ?
B4 C1 B6 C2 -100.1(2) . . . . ?
B5 C1 B6 C2 -138.1(2) . . . . ?
B3 C1 B6 C2 -32.45(19) . . . . ?
C3 C1 B6 B11 -151.7(2) . . . . ?
B4 C1 B6 B11 -0.6(3) . . . . ?
B5 C1 B6 B11 -38.61(19) . . . . ?
B3 C1 B6 B11 67.1(2) . . . . ?
C2 C1 B6 B11 99.5(2) . . . . ?
C3 C1 B6 B5 -113.1(2) . . . . ?
B4 C1 B6 B5 38.0(2) . . . . ?
B3 C1 B6 B5 105.7(2) . . . . ?
C2 C1 B6 B5 138.1(2) . . . . ?
C3 C1 B6 B7 145.3(2) . . . . ?
B4 C1 B6 B7 -63.6(3) . . . . ?
B5 C1 B6 B7 -101.7(2) . . . . ?
B3 C1 B6 B7 4.0(3) . . . . ?
C2 C1 B6 B7 36.49(18) . . . . ?
C1 B5 B6 C2 37.45(18) . . . . ?
B10 B5 B6 C2 -60.8(2) . . . . ?
B11 B5 B6 C2 -98.7(2) . . . . ?
B4 B5 B6 C2 2.7(3) . . . . ?
B10 B5 B6 C1 -98.3(2) . . . . ?
B11 B5 B6 C1 -136.1(2) . . . . ?
B4 B5 B6 C1 -34.72(18) . . . . ?
C1 B5 B6 B11 136.1(2) . . . . ?
B10 B5 B6 B11 37.85(19) . . . . ?
B4 B5 B6 B11 101.4(2) . . . . ?
C1 B5 B6 B7 99.3(2) . . . . ?
B10 B5 B6 B7 1.0(3) . . . . ?
B11 B5 B6 B7 -36.8(2) . . . . ?
B4 B5 B6 B7 64.6(2) . . . . ?
B8 B7 B6 C2 34.92(19) . . . . ?
B11 B7 B6 C2 135.9(2) . . . . ?
B12 B7 B6 C2 97.8(2) . . . . ?
C2 B7 B6 C1 -37.37(18) . . . . ?
B8 B7 B6 C1 -2.4(3) . . . . ?
B11 B7 B6 C1 98.6(2) . . . . ?
B12 B7 B6 C1 60.4(2) . . . . ?
C2 B7 B6 B11 -135.9(2) . . . . ?
B8 B7 B6 B11 -101.0(2) . . . . ?
B12 B7 B6 B11 -38.13(19) . . . . ?
C2 B7 B6 B5 -99.1(2) . . . . ?
B8 B7 B6 B5 -64.2(2) . . . . ?
B11 B7 B6 B5 36.8(2) . . . . ?
B12 B7 B6 B5 -1.3(3) . . . . ?
C2 B8 B12 B10 -62.1(2) . . . . ?
B9 B8 B12 B10 37.44(19) . . . . ?
B7 B8 B12 B10 -100.7(2) . . . . ?
B3 B8 B12 B10 0.0(3) . . . . ?
C2 B8 B12 B9 -99.5(2) . . . . ?
B7 B8 B12 B9 -138.1(2) . . . . ?
B3 B8 B12 B9 -37.41(19) . . . . ?
C2 B8 B12 B7 38.57(18) . . . . ?
B9 B8 B12 B7 138.1(2) . . . . ?
B3 B8 B12 B7 100.7(2) . . . . ?
C2 B8 B12 B11 1.1(3) . . . . ?
B9 B8 B12 B11 100.6(2) . . . . ?
B7 B8 B12 B11 -37.5(2) . . . . ?
B3 B8 B12 B11 63.2(3) . . . . ?
B3 B9 B12 B8 38.00(19) . . . . ?
B4 B9 B12 B8 101.7(2) . . . . ?
B10 B9 B12 B8 138.4(2) . . . . ?
B3 B9 B12 B10 -100.4(2) . . . . ?
B8 B9 B12 B10 -138.4(2) . . . . ?
B4 B9 B12 B10 -36.69(19) . . . . ?
B3 B9 B12 B7 0.7(3) . . . . ?
B8 B9 B12 B7 -37.32(19) . . . . ?
B4 B9 B12 B7 64.4(3) . . . . ?
B10 B9 B12 B7 101.1(2) . . . . ?
B3 B9 B12 B11 -62.3(3) . . . . ?
B8 B9 B12 B11 -100.3(2) . . . . ?
B4 B9 B12 B11 1.4(3) . . . . ?
B10 B9 B12 B11 38.09(19) . . . . ?
C2 B7 B12 B8 -38.33(18) . . . . ?
B11 B7 B12 B8 -137.7(2) . . . . ?
B6 B7 B12 B8 -100.0(2) . . . . ?
C2 B7 B12 B10 62.8(2) . . . . ?
B8 B7 B12 B10 101.1(2) . . . . ?
B11 B7 B12 B10 -36.64(19) . . . . ?
B6 B7 B12 B10 1.1(3) . . . . ?
C2 B7 B12 B9 -1.0(3) . . . . ?
B8 B7 B12 B9 37.32(19) . . . . ?
B11 B7 B12 B9 -100.4(2) . . . . ?
B6 B7 B12 B9 -62.7(3) . . . . ?
C2 B7 B12 B11 99.4(2) . . . . ?
B8 B7 B12 B11 137.7(2) . . . . ?
B6 B7 B12 B11 37.77(19) . . . . ?
C2 B6 B11 B5 101.0(2) . . . . ?
C1 B6 B11 B5 37.84(19) . . . . ?
B7 B6 B11 B5 139.1(2) . . . . ?
C2 B6 B11 B7 -38.07(19) . . . . ?
C1 B6 B11 B7 -101.3(2) . . . . ?
B5 B6 B11 B7 -139.1(2) . . . . ?
C2 B6 B11 B10 63.3(2) . . . . ?
C1 B6 B11 B10 0.1(3) . . . . ?
B5 B6 B11 B10 -37.72(19) . . . . ?
B7 B6 B11 B10 101.4(2) . . . . ?
C2 B6 B11 B12 0.1(3) . . . . ?
C1 B6 B11 B12 -63.1(2) . . . . ?
B5 B6 B11 B12 -101.0(2) . . . . ?
B7 B6 B11 B12 38.1(2) . . . . ?
C1 B5 B11 B6 -38.33(18) . . . . ?
B10 B5 B11 B6 -137.6(2) . . . . ?
B4 B5 B11 B6 -99.8(2) . . . . ?
C1 B5 B11 B7 -1.3(3) . . . . ?
B10 B5 B11 B7 -100.6(2) . . . . ?
B6 B5 B11 B7 37.0(2) . . . . ?
B4 B5 B11 B7 -62.8(3) . . . . ?
C1 B5 B11 B10 99.3(2) . . . . ?
B6 B5 B11 B10 137.6(2) . . . . ?
B4 B5 B11 B10 37.84(19) . . . . ?
C1 B5 B11 B12 62.3(3) . . . . ?
B10 B5 B11 B12 -36.97(19) . . . . ?
B6 B5 B11 B12 100.7(2) . . . . ?
B4 B5 B11 B12 0.9(3) . . . . ?
C2 B7 B11 B6 38.19(19) . . . . ?
B8 B7 B11 B6 99.6(2) . . . . ?
B12 B7 B11 B6 137.3(2) . . . . ?
C2 B7 B11 B5 1.2(3) . . . . ?
B8 B7 B11 B5 62.6(3) . . . . ?
B6 B7 B11 B5 -37.0(2) . . . . ?
B12 B7 B11 B5 100.2(2) . . . . ?
C2 B7 B11 B10 -62.3(2) . . . . ?
B8 B7 B11 B10 -0.9(3) . . . . ?
B6 B7 B11 B10 -100.5(2) . . . . ?
B12 B7 B11 B10 36.74(19) . . . . ?
C2 B7 B11 B12 -99.1(2) . . . . ?
B8 B7 B11 B12 -37.62(19) . . . . ?
B6 B7 B11 B12 -137.3(2) . . . . ?
B8 B12 B11 B6 -0.7(3) . . . . ?
B10 B12 B11 B6 100.7(2) . . . . ?
B9 B12 B11 B6 62.4(3) . . . . ?
B7 B12 B11 B6 -38.3(2) . . . . ?
B8 B12 B11 B5 -64.5(3) . . . . ?
B10 B12 B11 B5 36.94(19) . . . . ?
B9 B12 B11 B5 -1.4(3) . . . . ?
B7 B12 B11 B5 -102.0(2) . . . . ?
B8 B12 B11 B7 37.5(2) . . . . ?
B10 B12 B11 B7 139.0(2) . . . . ?
B9 B12 B11 B7 100.6(2) . . . . ?
B8 B12 B11 B10 -101.4(2) . . . . ?
B9 B12 B11 B10 -38.34(19) . . . . ?
B7 B12 B11 B10 -139.0(2) . . . . ?
C1 B5 B10 B11 -99.7(2) . . . . ?
B6 B5 B10 B11 -37.54(19) . . . . ?
B4 B5 B10 B11 -137.9(2) . . . . ?
C1 B5 B10 B12 -62.5(2) . . . . ?
B11 B5 B10 B12 37.25(19) . . . . ?
B6 B5 B10 B12 -0.3(3) . . . . ?
B4 B5 B10 B12 -100.7(2) . . . . ?
C1 B5 B10 B4 38.17(18) . . . . ?
B11 B5 B10 B4 137.9(2) . . . . ?
B6 B5 B10 B4 100.4(2) . . . . ?
C1 B5 B10 B9 0.8(3) . . . . ?
B11 B5 B10 B9 100.5(2) . . . . ?
B6 B5 B10 B9 63.0(2) . . . . ?
B4 B5 B10 B9 -37.37(19) . . . . ?
B6 B11 B10 B5 37.97(19) . . . . ?
B7 B11 B10 B5 101.8(2) . . . . ?
B12 B11 B10 B5 138.6(2) . . . . ?
B6 B11 B10 B12 -100.6(2) . . . . ?
B5 B11 B10 B12 -138.6(2) . . . . ?
B7 B11 B10 B12 -36.80(19) . . . . ?
B6 B11 B10 B4 0.4(3) . . . . ?
B5 B11 B10 B4 -37.60(19) . . . . ?
B7 B11 B10 B4 64.2(2) . . . . ?
B12 B11 B10 B4 101.0(2) . . . . ?
B6 B11 B10 B9 -62.5(2) . . . . ?
B5 B11 B10 B9 -100.5(2) . . . . ?
B7 B11 B10 B9 1.3(3) . . . . ?
B12 B11 B10 B9 38.11(19) . . . . ?
B8 B12 B10 B5 62.8(3) . . . . ?
B9 B12 B10 B5 100.0(2) . . . . ?
B7 B12 B10 B5 -0.5(3) . . . . ?
B11 B12 B10 B5 -37.11(19) . . . . ?
B8 B12 B10 B11 99.9(2) . . . . ?
B9 B12 B10 B11 137.1(2) . . . . ?
B7 B12 B10 B11 36.58(19) . . . . ?
B8 B12 B10 B4 -0.8(3) . . . . ?
B9 B12 B10 B4 36.46(19) . . . . ?
B7 B12 B10 B4 -64.1(2) . . . . ?
B11 B12 B10 B4 -100.7(2) . . . . ?
B8 B12 B10 B9 -37.22(19) . . . . ?
B7 B12 B10 B9 -100.6(2) . . . . ?
B11 B12 B10 B9 -137.1(2) . . . . ?
C1 B4 B10 B5 -38.26(18) . . . . ?
B3 B4 B10 B5 -100.1(2) . . . . ?
B9 B4 B10 B5 -137.9(2) . . . . ?
C1 B4 B10 B11 -0.7(2) . . . . ?
B3 B4 B10 B11 -62.5(2) . . . . ?
B9 B4 B10 B11 -100.3(2) . . . . ?
B5 B4 B10 B11 37.55(19) . . . . ?
C1 B4 B10 B12 63.0(2) . . . . ?
B3 B4 B10 B12 1.2(3) . . . . ?
B9 B4 B10 B12 -36.58(19) . . . . ?
B5 B4 B10 B12 101.3(2) . . . . ?
C1 B4 B10 B9 99.6(2) . . . . ?
B3 B4 B10 B9 37.76(19) . . . . ?
B5 B4 B10 B9 137.9(2) . . . . ?
B3 B9 B10 B5 -0.7(3) . . . . ?
B8 B9 B10 B5 -64.4(2) . . . . ?
B4 B9 B10 B5 37.58(19) . . . . ?
B12 B9 B10 B5 -101.5(2) . . . . ?
B3 B9 B10 B11 62.5(2) . . . . ?
B8 B9 B10 B11 -1.2(3) . . . . ?
B4 B9 B10 B11 100.8(2) . . . . ?
B12 B9 B10 B11 -38.29(19) . . . . ?
B3 B9 B10 B12 100.8(2) . . . . ?
B8 B9 B10 B12 37.06(19) . . . . ?
B4 B9 B10 B12 139.1(2) . . . . ?
B3 B9 B10 B4 -38.28(19) . . . . ?
B8 B9 B10 B4 -102.0(2) . . . . ?
B12 B9 B10 B4 -139.1(2) . . . . ?

_diffrn_measured_fraction_theta_max 0.970
_diffrn_reflns_theta_full        25.68
_diffrn_measured_fraction_theta_full 0.970
_refine_diff_density_max         0.327
_refine_diff_density_min         -0.296
_refine_diff_density_rms         0.058
_exptl_crystal_recrystallization_method 'Re-crystallisation from solvent'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 1536124'
_audit_update_record             
;
2017-03-06 deposited with the CCDC.
2017-05-02 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            pFl-Cb-H
_chemical_melting_point          ?
_chemical_formula_moiety         C27H28B10
_chemical_formula_sum            'C27 H28 B10'
_chemical_formula_weight         460.59

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_H-M   I41/a

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y+3/4, x+1/4, z+1/4'
'-x+1/2, -y, z+1/2'
'y+3/4, -x+3/4, z+3/4'
'x+1/2, y+1/2, z+1/2'
'-y+5/4, x+3/4, z+3/4'
'-x+1, -y+1/2, z+1'
'y+5/4, -x+5/4, z+5/4'
'-x, -y, -z'
'y-3/4, -x-1/4, -z-1/4'
'x-1/2, y, -z-1/2'
'-y-3/4, x-3/4, -z-3/4'
'-x+1/2, -y+1/2, -z+1/2'
'y-1/4, -x+1/4, -z+1/4'
'x, y+1/2, -z'
'-y-1/4, x-1/4, -z-1/4'

_cell_length_a                   29.1255(9)
_cell_length_b                   29.1255(9)
_cell_length_c                   14.6448(5)
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_volume                     12423.1(7)
_cell_formula_units_Z            16
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    5702
_cell_measurement_theta_min      0.01
_cell_measurement_theta_max      25.5

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    0.985
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3839
_exptl_absorpt_coefficient_mu    0.051
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker D8 VENTURE'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            5702
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0173
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_k_max       35
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_theta_min         2.95
_diffrn_reflns_theta_max         25.50
_reflns_number_total             5702
_reflns_number_gt                4954
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.4000P)²+0.3000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         5702
_refine_ls_number_parameters     334
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0952
_refine_ls_R_factor_gt           0.0890
_refine_ls_wR_factor_ref         0.3329
_refine_ls_wR_factor_gt          0.3055
_refine_ls_goodness_of_fit_ref   0.826
_refine_ls_restrained_S_all      0.826
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C -0.20465(7) -0.33284(6) 0.27499(12) 0.0253(5) Uani 1 1 d . . .
C2 C -0.17073(7) -0.37538(7) 0.31074(12) 0.0266(5) Uani 1 1 d . . .
H2A H -0.1540 -0.3908 0.2670 0.032 Uiso 1 1 d R . .
C3 C -0.20223(6) -0.31758(7) 0.17592(12) 0.0247(5) Uani 1 1 d . . .
C4 C -0.22618(6) -0.34136(6) 0.10769(12) 0.0241(5) Uani 1 1 d . . .
H4A H -0.2445 -0.3665 0.1223 0.029 Uiso 1 1 calc R . .
C5 C -0.22195(6) -0.32663(6) 0.01770(13) 0.0244(5) Uani 1 1 d . . .
C6 C -0.19497(6) -0.28878(6) -0.00426(13) 0.0254(5) Uani 1 1 d . . .
C7 C -0.17169(7) -0.26470(7) 0.06433(13) 0.0287(5) Uani 1 1 d . . .
H7A H -0.1537 -0.2394 0.0500 0.034 Uiso 1 1 calc R . .
C8 C -0.17603(7) -0.27933(6) 0.15386(13) 0.0265(5) Uani 1 1 d . . .
H8A H -0.1611 -0.2632 0.2000 0.032 Uiso 1 1 calc R . .
C9 C -0.19573(7) -0.28177(7) -0.10340(13) 0.0265(5) Uani 1 1 d . . .
C10 C -0.22199(6) -0.31673(6) -0.14246(13) 0.0249(5) Uani 1 1 d . . .
C11 C -0.22751(7) -0.31902(7) -0.23660(13) 0.0272(5) Uani 1 1 d . . .
H11A H -0.2445 -0.3425 -0.2632 0.033 Uiso 1 1 calc R . .
C12 C -0.20685(7) -0.28518(7) -0.29034(13) 0.0305(5) Uani 1 1 d . . .
H12A H -0.2101 -0.2863 -0.3535 0.037 Uiso 1 1 calc R . .
C13 C -0.18162(7) -0.25005(7) -0.25091(14) 0.0315(5) Uani 1 1 d . . .
H13A H -0.1685 -0.2276 -0.2878 0.038 Uiso 1 1 calc R . .
C14 C -0.17571(7) -0.24793(7) -0.15661(15) 0.0307(5) Uani 1 1 d . . .
H14A H -0.1588 -0.2244 -0.1301 0.037 Uiso 1 1 calc R . .
C15 C -0.24274(6) -0.34836(6) -0.06872(12) 0.0234(5) Uani 1 1 d . . .
C16 C -0.29489(7) -0.34432(6) -0.07471(13) 0.0251(5) Uani 1 1 d . . .
C17 C -0.31918(7) -0.31297(7) -0.02153(14) 0.0279(5) Uani 1 1 d . . .
H17A H -0.3039 -0.2964 0.0234 0.034 Uiso 1 1 calc R . .
C18 C -0.36596(7) -0.30610(7) -0.03462(14) 0.0308(5) Uani 1 1 d . . .
H18A H -0.3816 -0.2850 0.0016 0.037 Uiso 1 1 calc R . .
C19 C -0.38962(7) -0.33062(7) -0.10181(14) 0.0314(5) Uani 1 1 d . . .
H19A H -0.4209 -0.3259 -0.1107 0.038 Uiso 1 1 calc R . .
C20 C -0.36603(7) -0.36196(7) -0.15486(13) 0.0282(5) Uani 1 1 d . . .
H20A H -0.3815 -0.3784 -0.1997 0.034 Uiso 1 1 calc R . .
C21 C -0.31908(7) -0.36911(7) -0.14159(12) 0.0266(5) Uani 1 1 d . . .
H21A H -0.3037 -0.3905 -0.1774 0.032 Uiso 1 1 calc R . .
C22 C -0.22523(7) -0.39792(6) -0.07506(12) 0.0245(5) Uani 1 1 d . . .
C23 C -0.18383(7) -0.40871(7) -0.11811(13) 0.0272(5) Uani 1 1 d . . .
H23A H -0.1673 -0.3859 -0.1480 0.033 Uiso 1 1 calc R . .
C24 C -0.16709(7) -0.45347(7) -0.11649(13) 0.0293(5) Uani 1 1 d . . .
H24A H -0.1394 -0.4601 -0.1451 0.035 Uiso 1 1 calc R . .
C25 C -0.19087(7) -0.48799(7) -0.07320(13) 0.0295(5) Uani 1 1 d . . .
H25A H -0.1794 -0.5178 -0.0729 0.035 Uiso 1 1 calc R . .
C26 C -0.23230(7) -0.47788(7) -0.02973(14) 0.0296(5) Uani 1 1 d . . .
H26A H -0.2487 -0.5009 -0.0001 0.036 Uiso 1 1 calc R . .
C27 C -0.24881(6) -0.43306(7) -0.03122(13) 0.0270(5) Uani 1 1 d . . .
H27A H -0.2764 -0.4264 -0.0021 0.032 Uiso 1 1 calc R . .
B3 B -0.15691(8) -0.32054(8) 0.34265(15) 0.0277(5) Uani 1 1 d . . .
H3A H -0.1288 -0.3037 0.3136 0.033 Uiso 1 1 d R . .
B4 B -0.21124(8) -0.29360(8) 0.36087(15) 0.0289(5) Uani 1 1 d . . .
H4B H -0.2124 -0.2570 0.3408 0.035 Uiso 1 1 d R . .
B5 B -0.25541(7) -0.33418(8) 0.33466(15) 0.0266(5) Uani 1 1 d . . .
H5A H -0.2832 -0.3227 0.2989 0.032 Uiso 1 1 d R . .
B6 B -0.22817(8) -0.38612(7) 0.30022(14) 0.0269(5) Uani 1 1 d . . .
H6A H -0.2409 -0.4054 0.2497 0.032 Uiso 1 1 d R . .
B7 B -0.19566(8) -0.40767(8) 0.39330(15) 0.0294(5) Uani 1 1 d . . .
H4 H -0.1923 -0.4444 0.3957 0.035 Uiso 1 1 d R . .
B8 B -0.15183(8) -0.36748(8) 0.41911(15) 0.0285(5) Uani 1 1 d . . .
H3 H -0.1196 -0.3837 0.4333 0.034 Uiso 1 1 d R . .
B9 B -0.17861(8) -0.31544(8) 0.45435(15) 0.0293(5) Uani 1 1 d . . .
H9A H -0.1633 -0.2926 0.5024 0.035 Uiso 1 1 d R . .
B10 B -0.23941(8) -0.32400(8) 0.45052(14) 0.0278(5) Uani 1 1 d . . .
H10A H -0.2600 -0.3100 0.4961 0.033 Uiso 1 1 d R . .
B11 B -0.25011(8) -0.38122(8) 0.41143(15) 0.0291(5) Uani 1 1 d . . .
H1 H -0.2777 -0.4026 0.4332 0.035 Uiso 1 1 d R . .
B12 B -0.20275(8) -0.36934(8) 0.48596(15) 0.0284(5) Uani 1 1 d . . .
H2 H -0.2006 -0.3824 0.5528 0.034 Uiso 1 1 d R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C3 1.519(2) . ?
C1 C2 1.669(3) . ?
C1 B4 1.710(3) . ?
C1 B5 1.718(3) . ?
C1 B6 1.736(3) . ?
C1 B3 1.744(3) . ?
C2 B7 1.695(3) . ?
C2 B8 1.695(3) . ?
C2 B6 1.709(3) . ?
C2 B3 1.712(3) . ?
C2 H2A 0.9222 . ?
C3 C8 1.389(3) . ?
C3 C4 1.402(3) . ?
C4 C5 1.391(3) . ?
C4 H4A 0.9300 . ?
C5 C6 1.391(3) . ?
C5 C15 1.539(2) . ?
C6 C7 1.400(3) . ?
C6 C9 1.466(3) . ?
C7 C8 1.384(3) . ?
C7 H7A 0.9300 . ?
C8 H8A 0.9300 . ?
C9 C14 1.385(3) . ?
C9 C10 1.396(3) . ?
C10 C11 1.390(3) . ?
C10 C15 1.543(2) . ?
C11 C12 1.398(3) . ?
C11 H11A 0.9300 . ?
C12 C13 1.386(3) . ?
C12 H12A 0.9300 . ?
C13 C14 1.393(3) . ?
C13 H13A 0.9300 . ?
C14 H14A 0.9300 . ?
C15 C16 1.526(3) . ?
C15 C22 1.534(2) . ?
C16 C17 1.393(3) . ?
C16 C21 1.406(3) . ?
C17 C18 1.391(3) . ?
C17 H17A 0.9300 . ?
C18 C19 1.397(3) . ?
C18 H18A 0.9300 . ?
C19 C20 1.382(3) . ?
C19 H19A 0.9300 . ?
C20 C21 1.397(3) . ?
C20 H20A 0.9300 . ?
C21 H21A 0.9300 . ?
C22 C27 1.390(3) . ?
C22 C23 1.397(3) . ?
C23 C24 1.392(3) . ?
C23 H23A 0.9300 . ?
C24 C25 1.376(3) . ?
C24 H24A 0.9300 . ?
C25 C26 1.396(3) . ?
C25 H25A 0.9300 . ?
C26 C27 1.391(3) . ?
C26 H26A 0.9300 . ?
C27 H27A 0.9300 . ?
B3 B9 1.760(3) . ?
B3 B8 1.773(3) . ?
B3 B4 1.786(3) . ?
B3 H3A 1.0452 . ?
B4 B9 1.784(3) . ?
B4 B10 1.783(3) . ?
B4 B5 1.789(3) . ?
B4 H4B 1.1055 . ?
B5 B11 1.779(3) . ?
B5 B6 1.781(3) . ?
B5 B10 1.784(3) . ?
B5 H5A 1.0201 . ?
B6 B11 1.755(3) . ?
B6 B7 1.774(3) . ?
B6 H6A 0.9991 . ?
B7 B8 1.773(3) . ?
B7 B12 1.769(3) . ?
B7 B11 1.783(3) . ?
B7 H4 1.0740 . ?
B8 B12 1.778(3) . ?
B8 B9 1.781(3) . ?
B8 H3 1.0720 . ?
B9 B12 1.781(3) . ?
B9 B10 1.789(3) . ?
B9 H9A 1.0661 . ?
B10 B12 1.776(3) . ?
B10 B11 1.789(3) . ?
B10 H10A 0.9862 . ?
B11 B12 1.793(3) . ?
B11 H1 1.0666 . ?
B12 H2 1.0522 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C3 C1 C2 119.30(15) . . ?
C3 C1 B4 120.81(16) . . ?
C2 C1 B4 109.38(14) . . ?
C3 C1 B5 122.17(15) . . ?
C2 C1 B5 109.45(14) . . ?
B4 C1 B5 62.90(12) . . ?
C3 C1 B6 118.89(15) . . ?
C2 C1 B6 60.22(12) . . ?
B4 C1 B6 113.36(15) . . ?
B5 C1 B6 62.08(12) . . ?
C3 C1 B3 116.46(16) . . ?
C2 C1 B3 60.16(12) . . ?
B4 C1 B3 62.26(13) . . ?
B5 C1 B3 113.68(14) . . ?
B6 C1 B3 112.16(14) . . ?
C1 C2 B7 112.46(15) . . ?
C1 C2 B8 112.65(15) . . ?
B7 C2 B8 63.05(13) . . ?
C1 C2 B6 61.84(12) . . ?
B7 C2 B6 62.83(12) . . ?
B8 C2 B6 115.28(15) . . ?
C1 C2 B3 62.11(12) . . ?
B7 C2 B3 115.06(15) . . ?
B8 C2 B3 62.72(12) . . ?
B6 C2 B3 115.17(15) . . ?
C1 C2 H2A 117.2 . . ?
B7 C2 H2A 116.8 . . ?
B8 C2 H2A 123.0 . . ?
B6 C2 H2A 111.4 . . ?
B3 C2 H2A 121.4 . . ?
C8 C3 C4 120.28(16) . . ?
C8 C3 C1 118.84(17) . . ?
C4 C3 C1 120.88(17) . . ?
C5 C4 C3 118.59(17) . . ?
C5 C4 H4A 120.7 . . ?
C3 C4 H4A 120.7 . . ?
C6 C5 C4 120.89(17) . . ?
C6 C5 C15 110.97(16) . . ?
C4 C5 C15 128.10(17) . . ?
C5 C6 C7 120.29(17) . . ?
C5 C6 C9 109.32(17) . . ?
C7 C6 C9 130.38(18) . . ?
C8 C7 C6 118.77(18) . . ?
C8 C7 H7A 120.6 . . ?
C6 C7 H7A 120.6 . . ?
C7 C8 C3 121.14(17) . . ?
C7 C8 H8A 119.4 . . ?
C3 C8 H8A 119.4 . . ?
C14 C9 C10 121.27(18) . . ?
C14 C9 C6 130.53(18) . . ?
C10 C9 C6 108.20(17) . . ?
C11 C10 C9 120.33(17) . . ?
C11 C10 C15 128.35(17) . . ?
C9 C10 C15 111.31(16) . . ?
C10 C11 C12 118.36(18) . . ?
C10 C11 H11A 120.8 . . ?
C12 C11 H11A 120.8 . . ?
C13 C12 C11 120.95(18) . . ?
C13 C12 H12A 119.5 . . ?
C11 C12 H12A 119.5 . . ?
C12 C13 C14 120.75(19) . . ?
C12 C13 H13A 119.6 . . ?
C14 C13 H13A 119.6 . . ?
C9 C14 C13 118.31(19) . . ?
C9 C14 H14A 120.8 . . ?
C13 C14 H14A 120.8 . . ?
C16 C15 C22 113.57(15) . . ?
C16 C15 C5 114.03(15) . . ?
C22 C15 C5 107.82(15) . . ?
C16 C15 C10 107.69(14) . . ?
C22 C15 C10 112.91(15) . . ?
C5 C15 C10 100.13(15) . . ?
C17 C16 C21 118.13(18) . . ?
C17 C16 C15 121.59(17) . . ?
C21 C16 C15 119.95(17) . . ?
C18 C17 C16 120.99(19) . . ?
C18 C17 H17A 119.5 . . ?
C16 C17 H17A 119.5 . . ?
C17 C18 C19 120.44(19) . . ?
C17 C18 H18A 119.8 . . ?
C19 C18 H18A 119.8 . . ?
C20 C19 C18 119.24(18) . . ?
C20 C19 H19A 120.4 . . ?
C18 C19 H19A 120.4 . . ?
C19 C20 C21 120.47(18) . . ?
C19 C20 H20A 119.8 . . ?
C21 C20 H20A 119.8 . . ?
C20 C21 C16 120.72(18) . . ?
C20 C21 H21A 119.6 . . ?
C16 C21 H21A 119.6 . . ?
C27 C22 C23 118.00(18) . . ?
C27 C22 C15 120.06(17) . . ?
C23 C22 C15 121.75(17) . . ?
C24 C23 C22 120.36(18) . . ?
C24 C23 H23A 119.8 . . ?
C22 C23 H23A 119.8 . . ?
C25 C24 C23 121.08(18) . . ?
C25 C24 H24A 119.5 . . ?
C23 C24 H24A 119.5 . . ?
C24 C25 C26 119.41(18) . . ?
C24 C25 H25A 120.3 . . ?
C26 C25 H25A 120.3 . . ?
C27 C26 C25 119.32(18) . . ?
C27 C26 H26A 120.3 . . ?
C25 C26 H26A 120.3 . . ?
C26 C27 C22 121.83(18) . . ?
C26 C27 H27A 119.1 . . ?
C22 C27 H27A 119.1 . . ?
C2 B3 C1 57.73(11) . . ?
C2 B3 B9 104.36(15) . . ?
C1 B3 B9 105.02(15) . . ?
C2 B3 B8 58.18(12) . . ?
C1 B3 B8 105.48(15) . . ?
B9 B3 B8 60.54(12) . . ?
C2 B3 B4 104.03(15) . . ?
C1 B3 B4 57.93(12) . . ?
B9 B3 B4 60.39(12) . . ?
B8 B3 B4 108.56(16) . . ?
C2 B3 H3A 120.7 . . ?
C1 B3 H3A 119.3 . . ?
B9 B3 H3A 128.3 . . ?
B8 B3 H3A 123.6 . . ?
B4 B3 H3A 123.3 . . ?
C1 B4 B9 105.44(15) . . ?
C1 B4 B3 59.81(12) . . ?
B9 B4 B3 59.07(13) . . ?
C1 B4 B10 105.14(15) . . ?
B9 B4 B10 60.21(13) . . ?
B3 B4 B10 107.42(16) . . ?
C1 B4 B5 58.76(12) . . ?
B9 B4 B5 108.20(16) . . ?
B3 B4 B5 108.34(15) . . ?
B10 B4 B5 59.93(12) . . ?
C1 B4 H4B 116.9 . . ?
B9 B4 H4B 124.4 . . ?
B3 B4 H4B 114.3 . . ?
B10 B4 H4B 131.3 . . ?
B5 B4 H4B 123.9 . . ?
C1 B5 B11 105.33(15) . . ?
C1 B5 B6 59.46(12) . . ?
B11 B5 B6 59.08(12) . . ?
C1 B5 B10 104.79(14) . . ?
B11 B5 B10 60.29(12) . . ?
B6 B5 B10 107.10(15) . . ?
C1 B5 B4 58.34(11) . . ?
B11 B5 B4 108.11(15) . . ?
B6 B5 B4 107.56(15) . . ?
B10 B5 B4 59.89(12) . . ?
C1 B5 H5A 114.4 . . ?
B11 B5 H5A 130.3 . . ?
B6 B5 H5A 119.1 . . ?
B10 B5 H5A 129.8 . . ?
B4 B5 H5A 117.6 . . ?
C2 B6 C1 57.95(11) . . ?
C2 B6 B11 104.94(15) . . ?
C1 B6 B11 105.57(15) . . ?
C2 B6 B7 58.20(12) . . ?
C1 B6 B7 105.61(15) . . ?
B11 B6 B7 60.68(12) . . ?
C2 B6 B5 104.78(15) . . ?
C1 B6 B5 58.46(12) . . ?
B11 B6 B5 60.40(12) . . ?
B7 B6 B5 108.70(15) . . ?
C2 B6 H6A 122.1 . . ?
C1 B6 H6A 119.3 . . ?
B11 B6 H6A 126.7 . . ?
B7 B6 H6A 124.6 . . ?
B5 B6 H6A 121.4 . . ?
C2 B7 B8 58.49(12) . . ?
C2 B7 B12 104.30(15) . . ?
B8 B7 B12 60.25(13) . . ?
C2 B7 B6 58.97(12) . . ?
B8 B7 B6 108.33(15) . . ?
B12 B7 B6 107.68(16) . . ?
C2 B7 B11 104.33(15) . . ?
B8 B7 B11 108.87(16) . . ?
B12 B7 B11 60.62(13) . . ?
B6 B7 B11 59.13(12) . . ?
C2 B7 H4 122.5 . . ?
B8 B7 H4 125.8 . . ?
B12 B7 H4 127.8 . . ?
B6 B7 H4 115.2 . . ?
B11 B7 H4 120.4 . . ?
C2 B8 B7 58.47(12) . . ?
C2 B8 B3 59.10(12) . . ?
B7 B8 B3 108.32(15) . . ?
C2 B8 B12 103.92(15) . . ?
B7 B8 B12 59.78(13) . . ?
B3 B8 B12 107.55(15) . . ?
C2 B8 B9 104.16(15) . . ?
B7 B8 B9 107.96(16) . . ?
B3 B8 B9 59.36(12) . . ?
B12 B8 B9 60.07(13) . . ?
C2 B8 H3 113.9 . . ?
B7 B8 H3 112.3 . . ?
B3 B8 H3 122.4 . . ?
B12 B8 H3 127.6 . . ?
B9 B8 H3 134.7 . . ?
B3 B9 B12 107.99(15) . . ?
B3 B9 B8 60.10(13) . . ?
B12 B9 B8 59.88(13) . . ?
B3 B9 B4 60.54(12) . . ?
B12 B9 B4 107.66(16) . . ?
B8 B9 B4 108.33(15) . . ?
B3 B9 B10 108.33(15) . . ?
B12 B9 B10 59.65(12) . . ?
B8 B9 B10 107.80(15) . . ?
B4 B9 B10 59.89(13) . . ?
B3 B9 H9A 121.1 . . ?
B12 B9 H9A 122.9 . . ?
B8 B9 H9A 122.5 . . ?
B4 B9 H9A 120.5 . . ?
B10 B9 H9A 121.5 . . ?
B12 B10 B4 107.92(15) . . ?
B12 B10 B5 108.14(15) . . ?
B4 B10 B5 60.18(12) . . ?
B12 B10 B9 59.95(13) . . ?
B4 B10 B9 59.90(12) . . ?
B5 B10 B9 108.14(15) . . ?
B12 B10 B11 60.37(12) . . ?
B4 B10 B11 107.88(15) . . ?
B5 B10 B11 59.71(12) . . ?
B9 B10 B11 108.19(15) . . ?
B12 B10 H10A 118.5 . . ?
B4 B10 H10A 124.9 . . ?
B5 B10 H10A 123.6 . . ?
B9 B10 H10A 121.6 . . ?
B11 B10 H10A 119.8 . . ?
B6 B11 B5 60.52(12) . . ?
B6 B11 B7 60.19(12) . . ?
B5 B11 B7 108.41(15) . . ?
B6 B11 B10 108.01(16) . . ?
B5 B11 B10 60.00(13) . . ?
B7 B11 B10 107.17(15) . . ?
B6 B11 B12 107.49(16) . . ?
B5 B11 B12 107.63(15) . . ?
B7 B11 B12 59.31(12) . . ?
B10 B11 B12 59.44(12) . . ?
B6 B11 H1 120.3 . . ?
B5 B11 H1 125.0 . . ?
B7 B11 H1 117.6 . . ?
B10 B11 H1 125.5 . . ?
B12 B11 H1 120.8 . . ?
B7 B12 B10 108.37(15) . . ?
B7 B12 B8 59.97(13) . . ?
B10 B12 B8 108.55(15) . . ?
B7 B12 B9 108.10(15) . . ?
B10 B12 B9 60.40(13) . . ?
B8 B12 B9 60.05(12) . . ?
B7 B12 B11 60.07(12) . . ?
B10 B12 B11 60.19(13) . . ?
B8 B12 B11 108.21(15) . . ?
B9 B12 B11 108.40(15) . . ?
B7 B12 H2 118.5 . . ?
B10 B12 H2 125.3 . . ?
B8 B12 H2 118.3 . . ?
B9 B12 H2 122.5 . . ?
B11 B12 H2 122.8 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C3 C1 C2 B7 -147.07(17) . . . . ?
B4 C1 C2 B7 67.85(19) . . . . ?
B5 C1 C2 B7 0.7(2) . . . . ?
B6 C1 C2 B7 -38.58(15) . . . . ?
B3 C1 C2 B7 107.44(17) . . . . ?
C3 C1 C2 B8 143.97(17) . . . . ?
B4 C1 C2 B8 -1.1(2) . . . . ?
B5 C1 C2 B8 -68.29(19) . . . . ?
B6 C1 C2 B8 -107.54(17) . . . . ?
B3 C1 C2 B8 38.48(15) . . . . ?
C3 C1 C2 B6 -108.49(18) . . . . ?
B4 C1 C2 B6 106.43(16) . . . . ?
B5 C1 C2 B6 39.26(14) . . . . ?
B3 C1 C2 B6 146.02(15) . . . . ?
C3 C1 C2 B3 105.49(19) . . . . ?
B4 C1 C2 B3 -39.59(15) . . . . ?
B5 C1 C2 B3 -106.77(16) . . . . ?
B6 C1 C2 B3 -146.02(15) . . . . ?
C2 C1 C3 C8 -98.1(2) . . . . ?
B4 C1 C3 C8 43.0(3) . . . . ?
B5 C1 C3 C8 118.4(2) . . . . ?
B6 C1 C3 C8 -168.13(17) . . . . ?
B3 C1 C3 C8 -29.1(2) . . . . ?
C2 C1 C3 C4 82.3(2) . . . . ?
B4 C1 C3 C4 -136.62(19) . . . . ?
B5 C1 C3 C4 -61.2(2) . . . . ?
B6 C1 C3 C4 12.3(3) . . . . ?
B3 C1 C3 C4 151.35(17) . . . . ?
C8 C3 C4 C5 1.9(3) . . . . ?
C1 C3 C4 C5 -178.51(17) . . . . ?
C3 C4 C5 C6 -0.7(3) . . . . ?
C3 C4 C5 C15 176.74(17) . . . . ?
C4 C5 C6 C7 -0.3(3) . . . . ?
C15 C5 C6 C7 -178.14(17) . . . . ?
C4 C5 C6 C9 178.51(16) . . . . ?
C15 C5 C6 C9 0.6(2) . . . . ?
C5 C6 C7 C8 0.1(3) . . . . ?
C9 C6 C7 C8 -178.39(19) . . . . ?
C6 C7 C8 C3 1.1(3) . . . . ?
C4 C3 C8 C7 -2.1(3) . . . . ?
C1 C3 C8 C7 178.28(18) . . . . ?
C5 C6 C9 C14 177.4(2) . . . . ?
C7 C6 C9 C14 -4.0(4) . . . . ?
C5 C6 C9 C10 -2.3(2) . . . . ?
C7 C6 C9 C10 176.3(2) . . . . ?
C14 C9 C10 C11 1.8(3) . . . . ?
C6 C9 C10 C11 -178.45(17) . . . . ?
C14 C9 C10 C15 -176.69(18) . . . . ?
C6 C9 C10 C15 3.0(2) . . . . ?
C9 C10 C11 C12 -1.0(3) . . . . ?
C15 C10 C11 C12 177.22(18) . . . . ?
C10 C11 C12 C13 -0.3(3) . . . . ?
C11 C12 C13 C14 0.8(3) . . . . ?
C10 C9 C14 C13 -1.3(3) . . . . ?
C6 C9 C14 C13 179.11(19) . . . . ?
C12 C13 C14 C9 -0.1(3) . . . . ?
C6 C5 C15 C16 -113.65(18) . . . . ?
C4 C5 C15 C16 68.7(2) . . . . ?
C6 C5 C15 C22 119.25(17) . . . . ?
C4 C5 C15 C22 -58.4(2) . . . . ?
C6 C5 C15 C10 1.0(2) . . . . ?
C4 C5 C15 C10 -176.63(18) . . . . ?
C11 C10 C15 C16 -61.4(2) . . . . ?
C9 C10 C15 C16 116.94(17) . . . . ?
C11 C10 C15 C22 64.7(2) . . . . ?
C9 C10 C15 C22 -116.87(17) . . . . ?
C11 C10 C15 C5 179.13(18) . . . . ?
C9 C10 C15 C5 -2.5(2) . . . . ?
C22 C15 C16 C17 141.39(17) . . . . ?
C5 C15 C16 C17 17.3(2) . . . . ?
C10 C15 C16 C17 -92.8(2) . . . . ?
C22 C15 C16 C21 -45.3(2) . . . . ?
C5 C15 C16 C21 -169.37(16) . . . . ?
C10 C15 C16 C21 80.5(2) . . . . ?
C21 C16 C17 C18 -0.5(3) . . . . ?
C15 C16 C17 C18 172.94(18) . . . . ?
C16 C17 C18 C19 -0.1(3) . . . . ?
C17 C18 C19 C20 0.3(3) . . . . ?
C18 C19 C20 C21 0.0(3) . . . . ?
C19 C20 C21 C16 -0.6(3) . . . . ?
C17 C16 C21 C20 0.8(3) . . . . ?
C15 C16 C21 C20 -172.74(17) . . . . ?
C16 C15 C22 C27 -39.9(2) . . . . ?
C5 C15 C22 C27 87.5(2) . . . . ?
C10 C15 C22 C27 -162.85(17) . . . . ?
C16 C15 C22 C23 145.26(17) . . . . ?
C5 C15 C22 C23 -87.4(2) . . . . ?
C10 C15 C22 C23 22.3(2) . . . . ?
C27 C22 C23 C24 -0.1(3) . . . . ?
C15 C22 C23 C24 174.92(17) . . . . ?
C22 C23 C24 C25 0.4(3) . . . . ?
C23 C24 C25 C26 -0.4(3) . . . . ?
C24 C25 C26 C27 0.1(3) . . . . ?
C25 C26 C27 C22 0.2(3) . . . . ?
C23 C22 C27 C26 -0.2(3) . . . . ?
C15 C22 C27 C26 -175.26(17) . . . . ?
B7 C2 B3 C1 -103.28(17) . . . . ?
B8 C2 B3 C1 -139.75(16) . . . . ?
B6 C2 B3 C1 -32.98(14) . . . . ?
C1 C2 B3 B9 98.90(16) . . . . ?
B7 C2 B3 B9 -4.4(2) . . . . ?
B8 C2 B3 B9 -40.85(15) . . . . ?
B6 C2 B3 B9 65.91(19) . . . . ?
C1 C2 B3 B8 139.75(16) . . . . ?
B7 C2 B3 B8 36.47(16) . . . . ?
B6 C2 B3 B8 106.77(17) . . . . ?
C1 C2 B3 B4 36.39(13) . . . . ?
B7 C2 B3 B4 -66.89(19) . . . . ?
B8 C2 B3 B4 -103.36(16) . . . . ?
B6 C2 B3 B4 3.4(2) . . . . ?
C3 C1 B3 C2 -110.16(17) . . . . ?
B4 C1 B3 C2 137.22(15) . . . . ?
B5 C1 B3 C2 99.65(16) . . . . ?
B6 C1 B3 C2 31.58(14) . . . . ?
C3 C1 B3 B9 152.11(16) . . . . ?
C2 C1 B3 B9 -97.72(16) . . . . ?
B4 C1 B3 B9 39.49(14) . . . . ?
B5 C1 B3 B9 1.9(2) . . . . ?
B6 C1 B3 B9 -66.14(18) . . . . ?
C3 C1 B3 B8 -144.89(16) . . . . ?
C2 C1 B3 B8 -34.73(14) . . . . ?
B4 C1 B3 B8 102.48(16) . . . . ?
B5 C1 B3 B8 64.92(19) . . . . ?
B6 C1 B3 B8 -3.2(2) . . . . ?
C3 C1 B3 B4 112.62(18) . . . . ?
C2 C1 B3 B4 -137.22(15) . . . . ?
B5 C1 B3 B4 -37.57(15) . . . . ?
B6 C1 B3 B4 -105.64(17) . . . . ?
C3 C1 B4 B9 -144.77(17) . . . . ?
C2 C1 B4 B9 -0.3(2) . . . . ?
B5 C1 B4 B9 102.20(17) . . . . ?
B6 C1 B4 B9 64.75(19) . . . . ?
B3 C1 B4 B9 -38.96(15) . . . . ?
C3 C1 B4 B3 -105.81(19) . . . . ?
C2 C1 B4 B3 38.65(14) . . . . ?
B5 C1 B4 B3 141.16(16) . . . . ?
B6 C1 B4 B3 103.71(16) . . . . ?
C3 C1 B4 B10 152.57(17) . . . . ?
C2 C1 B4 B10 -62.97(18) . . . . ?
B5 C1 B4 B10 39.54(14) . . . . ?
B6 C1 B4 B10 2.1(2) . . . . ?
B3 C1 B4 B10 -101.62(16) . . . . ?
C3 C1 B4 B5 113.03(19) . . . . ?
C2 C1 B4 B5 -102.51(16) . . . . ?
B6 C1 B4 B5 -37.45(15) . . . . ?
B3 C1 B4 B5 -141.16(16) . . . . ?
C2 B3 B4 C1 -36.30(13) . . . . ?
B9 B3 B4 C1 -135.05(16) . . . . ?
B8 B3 B4 C1 -97.00(16) . . . . ?
C2 B3 B4 B9 98.75(16) . . . . ?
C1 B3 B4 B9 135.05(16) . . . . ?
B8 B3 B4 B9 38.05(14) . . . . ?
C2 B3 B4 B10 61.41(18) . . . . ?
C1 B3 B4 B10 97.71(16) . . . . ?
B9 B3 B4 B10 -37.34(14) . . . . ?
B8 B3 B4 B10 0.7(2) . . . . ?
C2 B3 B4 B5 -1.90(19) . . . . ?
C1 B3 B4 B5 34.40(14) . . . . ?
B9 B3 B4 B5 -100.65(17) . . . . ?
B8 B3 B4 B5 -62.61(19) . . . . ?
C3 C1 B5 B11 146.93(17) . . . . ?
C2 C1 B5 B11 0.29(19) . . . . ?
B4 C1 B5 B11 -102.10(16) . . . . ?
B6 C1 B5 B11 38.72(13) . . . . ?
B3 C1 B5 B11 -64.79(19) . . . . ?
C3 C1 B5 B6 108.21(19) . . . . ?
C2 C1 B5 B6 -38.43(14) . . . . ?
B4 C1 B5 B6 -140.82(15) . . . . ?
B3 C1 B5 B6 -103.51(16) . . . . ?
C3 C1 B5 B10 -150.40(17) . . . . ?
C2 C1 B5 B10 62.96(18) . . . . ?
B4 C1 B5 B10 -39.44(14) . . . . ?
B6 C1 B5 B10 101.39(15) . . . . ?
B3 C1 B5 B10 -2.1(2) . . . . ?
C3 C1 B5 B4 -110.96(19) . . . . ?
C2 C1 B5 B4 102.39(16) . . . . ?
B6 C1 B5 B4 140.82(15) . . . . ?
B3 C1 B5 B4 37.31(15) . . . . ?
B9 B4 B5 C1 -97.38(16) . . . . ?
B3 B4 B5 C1 -34.83(14) . . . . ?
B10 B4 B5 C1 -134.77(15) . . . . ?
C1 B4 B5 B11 97.19(16) . . . . ?
B9 B4 B5 B11 -0.2(2) . . . . ?
B3 B4 B5 B11 62.36(19) . . . . ?
B10 B4 B5 B11 -37.58(15) . . . . ?
C1 B4 B5 B6 34.80(14) . . . . ?
B9 B4 B5 B6 -62.58(19) . . . . ?
B3 B4 B5 B6 0.0(2) . . . . ?
B10 B4 B5 B6 -99.97(16) . . . . ?
C1 B4 B5 B10 134.77(15) . . . . ?
B9 B4 B5 B10 37.39(15) . . . . ?
B3 B4 B5 B10 99.94(16) . . . . ?
B7 C2 B6 C1 139.62(15) . . . . ?
B8 C2 B6 C1 103.31(17) . . . . ?
B3 C2 B6 C1 33.08(14) . . . . ?
C1 C2 B6 B11 -99.25(16) . . . . ?
B7 C2 B6 B11 40.37(14) . . . . ?
B8 C2 B6 B11 4.1(2) . . . . ?
B3 C2 B6 B11 -66.17(19) . . . . ?
C1 C2 B6 B7 -139.62(15) . . . . ?
B8 C2 B6 B7 -36.31(16) . . . . ?
B3 C2 B6 B7 -106.55(17) . . . . ?
C1 C2 B6 B5 -36.53(13) . . . . ?
B7 C2 B6 B5 103.10(16) . . . . ?
B8 C2 B6 B5 66.78(19) . . . . ?
B3 C2 B6 B5 -3.5(2) . . . . ?
C3 C1 B6 C2 109.16(18) . . . . ?
B4 C1 B6 C2 -99.75(16) . . . . ?
B5 C1 B6 C2 -137.52(15) . . . . ?
B3 C1 B6 C2 -31.56(14) . . . . ?
C3 C1 B6 B11 -152.72(16) . . . . ?
C2 C1 B6 B11 98.12(16) . . . . ?
B4 C1 B6 B11 -1.6(2) . . . . ?
B5 C1 B6 B11 -39.40(14) . . . . ?
B3 C1 B6 B11 66.56(19) . . . . ?
C3 C1 B6 B7 144.02(17) . . . . ?
C2 C1 B6 B7 34.87(13) . . . . ?
B4 C1 B6 B7 -64.88(19) . . . . ?
B5 C1 B6 B7 -102.66(16) . . . . ?
B3 C1 B6 B7 3.31(19) . . . . ?
C3 C1 B6 B5 -113.32(18) . . . . ?
C2 C1 B6 B5 137.52(15) . . . . ?
B4 C1 B6 B5 37.78(15) . . . . ?
B3 C1 B6 B5 105.96(16) . . . . ?
C1 B5 B6 C2 36.30(13) . . . . ?
B11 B5 B6 C2 -99.02(15) . . . . ?
B10 B5 B6 C2 -61.09(18) . . . . ?
B4 B5 B6 C2 1.96(19) . . . . ?
B11 B5 B6 C1 -135.32(15) . . . . ?
B10 B5 B6 C1 -97.39(15) . . . . ?
B4 B5 B6 C1 -34.33(14) . . . . ?
C1 B5 B6 B11 135.32(15) . . . . ?
B10 B5 B6 B11 37.93(15) . . . . ?
B4 B5 B6 B11 100.98(16) . . . . ?
C1 B5 B6 B7 97.21(16) . . . . ?
B11 B5 B6 B7 -38.10(14) . . . . ?
B10 B5 B6 B7 -0.2(2) . . . . ?
B4 B5 B6 B7 62.88(19) . . . . ?
C1 C2 B7 B8 -104.91(17) . . . . ?
B6 C2 B7 B8 -143.07(16) . . . . ?
B3 C2 B7 B8 -36.35(15) . . . . ?
C1 C2 B7 B12 -64.09(19) . . . . ?
B8 C2 B7 B12 40.81(14) . . . . ?
B6 C2 B7 B12 -102.26(16) . . . . ?
B3 C2 B7 B12 4.5(2) . . . . ?
C1 C2 B7 B6 38.17(14) . . . . ?
B8 C2 B7 B6 143.07(16) . . . . ?
B3 C2 B7 B6 106.73(17) . . . . ?
C1 C2 B7 B11 -1.3(2) . . . . ?
B8 C2 B7 B11 103.59(16) . . . . ?
B6 C2 B7 B11 -39.49(14) . . . . ?
B3 C2 B7 B11 67.24(19) . . . . ?
C1 B6 B7 C2 -34.76(13) . . . . ?
B11 B6 B7 C2 -134.12(16) . . . . ?
B5 B6 B7 C2 -96.14(16) . . . . ?
C2 B6 B7 B8 32.65(14) . . . . ?
C1 B6 B7 B8 -2.1(2) . . . . ?
B11 B6 B7 B8 -101.47(17) . . . . ?
B5 B6 B7 B8 -63.49(19) . . . . ?
C2 B6 B7 B12 96.36(16) . . . . ?
C1 B6 B7 B12 61.60(18) . . . . ?
B11 B6 B7 B12 -37.77(15) . . . . ?
B5 B6 B7 B12 0.2(2) . . . . ?
C2 B6 B7 B11 134.12(16) . . . . ?
C1 B6 B7 B11 99.37(16) . . . . ?
B5 B6 B7 B11 37.98(14) . . . . ?
C1 C2 B8 B7 104.61(17) . . . . ?
B6 C2 B8 B7 36.23(16) . . . . ?
B3 C2 B8 B7 142.84(16) . . . . ?
C1 C2 B8 B3 -38.23(15) . . . . ?
B7 C2 B8 B3 -142.84(16) . . . . ?
B6 C2 B8 B3 -106.60(17) . . . . ?
C1 C2 B8 B12 64.11(19) . . . . ?
B7 C2 B8 B12 -40.50(14) . . . . ?
B6 C2 B8 B12 -4.3(2) . . . . ?
B3 C2 B8 B12 102.34(16) . . . . ?
C1 C2 B8 B9 2.0(2) . . . . ?
B7 C2 B8 B9 -102.61(17) . . . . ?
B6 C2 B8 B9 -66.4(2) . . . . ?
B3 C2 B8 B9 40.22(15) . . . . ?
B12 B7 B8 C2 -133.16(16) . . . . ?
B6 B7 B8 C2 -32.84(14) . . . . ?
B11 B7 B8 C2 -95.58(16) . . . . ?
C2 B7 B8 B3 33.09(14) . . . . ?
B12 B7 B8 B3 -100.07(17) . . . . ?
B6 B7 B8 B3 0.3(2) . . . . ?
B11 B7 B8 B3 -62.49(19) . . . . ?
C2 B7 B8 B12 133.16(16) . . . . ?
B6 B7 B8 B12 100.32(17) . . . . ?
B11 B7 B8 B12 37.58(14) . . . . ?
C2 B7 B8 B9 95.90(16) . . . . ?
B12 B7 B8 B9 -37.26(14) . . . . ?
B6 B7 B8 B9 63.05(19) . . . . ?
B11 B7 B8 B9 0.3(2) . . . . ?
C1 B3 B8 C2 34.54(13) . . . . ?
B9 B3 B8 C2 133.30(16) . . . . ?
B4 B3 B8 C2 95.32(16) . . . . ?
C2 B3 B8 B7 -32.84(14) . . . . ?
C1 B3 B8 B7 1.7(2) . . . . ?
B9 B3 B8 B7 100.46(17) . . . . ?
B4 B3 B8 B7 62.47(19) . . . . ?
C2 B3 B8 B12 -96.01(16) . . . . ?
C1 B3 B8 B12 -61.47(18) . . . . ?
B9 B3 B8 B12 37.29(15) . . . . ?
B4 B3 B8 B12 -0.7(2) . . . . ?
C2 B3 B8 B9 -133.30(16) . . . . ?
C1 B3 B8 B9 -98.76(16) . . . . ?
B4 B3 B8 B9 -37.98(15) . . . . ?
C2 B3 B9 B12 2.4(2) . . . . ?
C1 B3 B9 B12 62.24(19) . . . . ?
B8 B3 B9 B12 -37.31(15) . . . . ?
B4 B3 B9 B12 100.54(17) . . . . ?
C2 B3 B9 B8 39.67(14) . . . . ?
C1 B3 B9 B8 99.55(16) . . . . ?
B4 B3 B9 B8 137.85(16) . . . . ?
C2 B3 B9 B4 -98.18(16) . . . . ?
C1 B3 B9 B4 -38.31(14) . . . . ?
B8 B3 B9 B4 -137.85(16) . . . . ?
C2 B3 B9 B10 -60.76(18) . . . . ?
C1 B3 B9 B10 -0.88(19) . . . . ?
B8 B3 B9 B10 -100.43(17) . . . . ?
B4 B3 B9 B10 37.42(14) . . . . ?
C2 B8 B9 B3 -40.09(14) . . . . ?
B7 B8 B9 B3 -101.07(16) . . . . ?
B12 B8 B9 B3 -138.20(16) . . . . ?
C2 B8 B9 B12 98.11(16) . . . . ?
B7 B8 B9 B12 37.13(14) . . . . ?
B3 B8 B9 B12 138.20(16) . . . . ?
C2 B8 B9 B4 -2.1(2) . . . . ?
B7 B8 B9 B4 -63.08(19) . . . . ?
B3 B8 B9 B4 37.99(15) . . . . ?
B12 B8 B9 B4 -100.21(17) . . . . ?
C2 B8 B9 B10 61.23(19) . . . . ?
B7 B8 B9 B10 0.26(19) . . . . ?
B3 B8 B9 B10 101.32(16) . . . . ?
B12 B8 B9 B10 -36.88(14) . . . . ?
C1 B4 B9 B3 39.31(14) . . . . ?
B10 B4 B9 B3 138.18(15) . . . . ?
B5 B4 B9 B3 100.91(17) . . . . ?
C1 B4 B9 B12 -61.78(19) . . . . ?
B3 B4 B9 B12 -101.09(17) . . . . ?
B10 B4 B9 B12 37.08(14) . . . . ?
B5 B4 B9 B12 -0.2(2) . . . . ?
C1 B4 B9 B8 1.5(2) . . . . ?
B3 B4 B9 B8 -37.79(15) . . . . ?
B10 B4 B9 B8 100.38(17) . . . . ?
B5 B4 B9 B8 63.1(2) . . . . ?
C1 B4 B9 B10 -98.87(16) . . . . ?
B3 B4 B9 B10 -138.18(15) . . . . ?
B5 B4 B9 B10 -37.27(14) . . . . ?
C1 B4 B10 B12 62.10(19) . . . . ?
B9 B4 B10 B12 -37.28(15) . . . . ?
B3 B4 B10 B12 -0.4(2) . . . . ?
B5 B4 B10 B12 101.06(16) . . . . ?
C1 B4 B10 B5 -38.96(14) . . . . ?
B9 B4 B10 B5 -138.34(16) . . . . ?
B3 B4 B10 B5 -101.51(16) . . . . ?
C1 B4 B10 B9 99.38(16) . . . . ?
B3 B4 B10 B9 36.84(14) . . . . ?
B5 B4 B10 B9 138.34(16) . . . . ?
C1 B4 B10 B11 -1.7(2) . . . . ?
B9 B4 B10 B11 -101.07(17) . . . . ?
B3 B4 B10 B11 -64.24(19) . . . . ?
B5 B4 B10 B11 37.27(15) . . . . ?
C1 B5 B10 B12 -61.99(18) . . . . ?
B11 B5 B10 B12 37.45(15) . . . . ?
B6 B5 B10 B12 0.1(2) . . . . ?
B4 B5 B10 B12 -100.68(17) . . . . ?
C1 B5 B10 B4 38.69(13) . . . . ?
B11 B5 B10 B4 138.13(16) . . . . ?
B6 B5 B10 B4 100.75(16) . . . . ?
C1 B5 B10 B9 1.45(19) . . . . ?
B11 B5 B10 B9 100.89(17) . . . . ?
B6 B5 B10 B9 63.50(19) . . . . ?
B4 B5 B10 B9 -37.24(15) . . . . ?
C1 B5 B10 B11 -99.45(16) . . . . ?
B6 B5 B10 B11 -37.39(15) . . . . ?
B4 B5 B10 B11 -138.13(16) . . . . ?
B3 B9 B10 B12 100.55(16) . . . . ?
B8 B9 B10 B12 36.98(14) . . . . ?
B4 B9 B10 B12 138.26(15) . . . . ?
B3 B9 B10 B4 -37.71(14) . . . . ?
B12 B9 B10 B4 -138.26(15) . . . . ?
B8 B9 B10 B4 -101.28(16) . . . . ?
B3 B9 B10 B5 -0.3(2) . . . . ?
B12 B9 B10 B5 -100.89(16) . . . . ?
B8 B9 B10 B5 -63.92(19) . . . . ?
B4 B9 B10 B5 37.36(15) . . . . ?
B3 B9 B10 B11 62.84(19) . . . . ?
B12 B9 B10 B11 -37.70(14) . . . . ?
B8 B9 B10 B11 -0.7(2) . . . . ?
B4 B9 B10 B11 100.55(16) . . . . ?
C2 B6 B11 B5 98.75(15) . . . . ?
C1 B6 B11 B5 38.47(13) . . . . ?
B7 B6 B11 B5 137.90(16) . . . . ?
C2 B6 B11 B7 -39.16(14) . . . . ?
C1 B6 B11 B7 -99.43(16) . . . . ?
B5 B6 B11 B7 -137.90(16) . . . . ?
C2 B6 B11 B10 60.72(19) . . . . ?
C1 B6 B11 B10 0.4(2) . . . . ?
B7 B6 B11 B10 99.87(17) . . . . ?
B5 B6 B11 B10 -38.03(15) . . . . ?
C2 B6 B11 B12 -2.0(2) . . . . ?
C1 B6 B11 B12 -62.29(19) . . . . ?
B7 B6 B11 B12 37.14(15) . . . . ?
B5 B6 B11 B12 -100.76(16) . . . . ?
C1 B5 B11 B6 -38.90(14) . . . . ?
B10 B5 B11 B6 -137.43(16) . . . . ?
B4 B5 B11 B6 -100.03(16) . . . . ?
C1 B5 B11 B7 -1.09(19) . . . . ?
B6 B5 B11 B7 37.81(14) . . . . ?
B10 B5 B11 B7 -99.62(17) . . . . ?
B4 B5 B11 B7 -62.21(19) . . . . ?
C1 B5 B11 B10 98.53(15) . . . . ?
B6 B5 B11 B10 137.43(16) . . . . ?
B4 B5 B11 B10 37.40(15) . . . . ?
C1 B5 B11 B12 61.61(18) . . . . ?
B6 B5 B11 B12 100.52(17) . . . . ?
B10 B5 B11 B12 -36.92(14) . . . . ?
B4 B5 B11 B12 0.5(2) . . . . ?
C2 B7 B11 B6 39.41(14) . . . . ?
B8 B7 B11 B6 100.54(16) . . . . ?
B12 B7 B11 B6 137.96(16) . . . . ?
C2 B7 B11 B5 1.45(19) . . . . ?
B8 B7 B11 B5 62.58(19) . . . . ?
B12 B7 B11 B5 100.00(16) . . . . ?
B6 B7 B11 B5 -37.96(14) . . . . ?
C2 B7 B11 B10 -61.89(18) . . . . ?
B8 B7 B11 B10 -0.76(19) . . . . ?
B12 B7 B11 B10 36.66(14) . . . . ?
B6 B7 B11 B10 -101.30(17) . . . . ?
C2 B7 B11 B12 -98.55(16) . . . . ?
B8 B7 B11 B12 -37.42(14) . . . . ?
B6 B7 B11 B12 -137.96(16) . . . . ?
B12 B10 B11 B6 -100.08(17) . . . . ?
B4 B10 B11 B6 0.8(2) . . . . ?
B5 B10 B11 B6 38.26(14) . . . . ?
B9 B10 B11 B6 -62.56(19) . . . . ?
B12 B10 B11 B5 -138.33(16) . . . . ?
B4 B10 B11 B5 -37.47(15) . . . . ?
B9 B10 B11 B5 -100.82(16) . . . . ?
B12 B10 B11 B7 -36.60(14) . . . . ?
B4 B10 B11 B7 64.26(18) . . . . ?
B5 B10 B11 B7 101.73(16) . . . . ?
B9 B10 B11 B7 0.91(19) . . . . ?
B4 B10 B11 B12 100.86(16) . . . . ?
B5 B10 B11 B12 138.33(16) . . . . ?
B9 B10 B11 B12 37.52(14) . . . . ?
C2 B7 B12 B10 61.33(18) . . . . ?
B8 B7 B12 B10 101.25(16) . . . . ?
B6 B7 B12 B10 -0.2(2) . . . . ?
B11 B7 B12 B10 -37.28(15) . . . . ?
C2 B7 B12 B8 -39.92(14) . . . . ?
B6 B7 B12 B8 -101.42(16) . . . . ?
B11 B7 B12 B8 -138.53(16) . . . . ?
C2 B7 B12 B9 -2.6(2) . . . . ?
B8 B7 B12 B9 37.29(15) . . . . ?
B6 B7 B12 B9 -64.13(19) . . . . ?
B11 B7 B12 B9 -101.24(17) . . . . ?
C2 B7 B12 B11 98.61(16) . . . . ?
B8 B7 B12 B11 138.53(16) . . . . ?
B6 B7 B12 B11 37.11(15) . . . . ?
B4 B10 B12 B7 -63.57(19) . . . . ?
B5 B10 B12 B7 0.1(2) . . . . ?
B9 B10 B12 B7 -100.83(16) . . . . ?
B11 B10 B12 B7 37.23(15) . . . . ?
B4 B10 B12 B8 0.0(2) . . . . ?
B5 B10 B12 B8 63.66(19) . . . . ?
B9 B10 B12 B8 -37.24(14) . . . . ?
B11 B10 B12 B8 100.82(16) . . . . ?
B4 B10 B12 B9 37.26(14) . . . . ?
B5 B10 B12 B9 100.89(16) . . . . ?
B11 B10 B12 B9 138.05(15) . . . . ?
B4 B10 B12 B11 -100.80(16) . . . . ?
B5 B10 B12 B11 -37.16(14) . . . . ?
B9 B10 B12 B11 -138.05(15) . . . . ?
C2 B8 B12 B7 39.83(14) . . . . ?
B3 B8 B12 B7 101.37(16) . . . . ?
B9 B8 B12 B7 138.35(16) . . . . ?
C2 B8 B12 B10 -61.13(18) . . . . ?
B7 B8 B12 B10 -100.96(16) . . . . ?
B3 B8 B12 B10 0.4(2) . . . . ?
B9 B8 B12 B10 37.39(14) . . . . ?
C2 B8 B12 B9 -98.52(15) . . . . ?
B7 B8 B12 B9 -138.35(16) . . . . ?
B3 B8 B12 B9 -36.98(14) . . . . ?
C2 B8 B12 B11 2.7(2) . . . . ?
B7 B8 B12 B11 -37.17(14) . . . . ?
B3 B8 B12 B11 64.20(19) . . . . ?
B9 B8 B12 B11 101.18(17) . . . . ?
B3 B9 B12 B7 0.2(2) . . . . ?
B8 B9 B12 B7 -37.25(15) . . . . ?
B4 B9 B12 B7 64.1(2) . . . . ?
B10 B9 B12 B7 101.29(17) . . . . ?
B3 B9 B12 B10 -101.13(16) . . . . ?
B8 B9 B12 B10 -138.54(15) . . . . ?
B4 B9 B12 B10 -37.19(14) . . . . ?
B3 B9 B12 B8 37.41(15) . . . . ?
B4 B9 B12 B8 101.35(17) . . . . ?
B10 B9 B12 B8 138.54(15) . . . . ?
B3 B9 B12 B11 -63.5(2) . . . . ?
B8 B9 B12 B11 -100.86(16) . . . . ?
B4 B9 B12 B11 0.5(2) . . . . ?
B10 B9 B12 B11 37.68(14) . . . . ?
B6 B11 B12 B7 -37.54(15) . . . . ?
B5 B11 B12 B7 -101.35(16) . . . . ?
B10 B11 B12 B7 -138.51(16) . . . . ?
B6 B11 B12 B10 100.98(17) . . . . ?
B5 B11 B12 B10 37.17(14) . . . . ?
B7 B11 B12 B10 138.51(16) . . . . ?
B6 B11 B12 B8 -0.4(2) . . . . ?
B5 B11 B12 B8 -64.22(19) . . . . ?
B7 B11 B12 B8 37.13(15) . . . . ?
B10 B11 B12 B8 -101.39(17) . . . . ?
B6 B11 B12 B9 63.2(2) . . . . ?
B5 B11 B12 B9 -0.6(2) . . . . ?
B7 B11 B12 B9 100.74(17) . . . . ?
B10 B11 B12 B9 -37.77(14) . . . . ?

_diffrn_measured_fraction_theta_max 0.984
_diffrn_reflns_theta_full        25.50
_diffrn_measured_fraction_theta_full 0.984
_refine_diff_density_max         0.704
_refine_diff_density_min         -0.406
_refine_diff_density_rms         0.100
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 1527647'
_audit_update_record             
;
2017-01-16 deposited with the CCDC.
2017-05-02 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C32 H36 B10'
_chemical_formula_weight         528.71

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   P-1

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   10.7377(4)
_cell_length_b                   15.4048(6)
_cell_length_c                   18.3711(7)
_cell_angle_alpha                90.481(2)
_cell_angle_beta                 97.830(2)
_cell_angle_gamma                91.483(2)
_cell_volume                     3009.2(2)
_cell_formula_units_Z            4
_cell_measurement_temperature    120
_cell_measurement_reflns_used    13334
_cell_measurement_theta_min      0.01
_cell_measurement_theta_max      54.39

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.167
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1112
_exptl_absorpt_coefficient_mu    0.061
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      120
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker D8 Venture'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            59826
_diffrn_reflns_av_R_equivalents  0.0490
_diffrn_reflns_av_sigmaI/netI    0.0469
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         2.86
_diffrn_reflns_theta_max         27.19
_reflns_number_total             13334
_reflns_number_gt                10107
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0466P)²+1.6541P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         13334
_refine_ls_number_parameters     777
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0739
_refine_ls_R_factor_gt           0.0489
_refine_ls_wR_factor_ref         0.1145
_refine_ls_wR_factor_gt          0.1033
_refine_ls_goodness_of_fit_ref   0.994
_refine_ls_restrained_S_all      0.994
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C16 C 0.92670(15) 0.50561(10) 0.41819(8) 0.0180(3) Uani 1 1 d . . .
H1A H 0.9898 0.5307 0.3947 0.022 Uiso 1 1 calc R . .
C17 C 0.84771(15) 0.55831(10) 0.45171(8) 0.0189(3) Uani 1 1 d . . .
H2A H 0.8580 0.6184 0.4499 0.023 Uiso 1 1 calc R . .
C3 C 0.75361(14) 0.52242(10) 0.48781(8) 0.0181(3) Uani 1 1 d . . .
H3A H 0.7013 0.5577 0.5107 0.022 Uiso 1 1 calc R . .
C4 C 0.73941(14) 0.43241(10) 0.48896(8) 0.0155(3) Uani 1 1 d . . .
C5 C 0.81775(14) 0.37923(9) 0.45428(8) 0.0145(3) Uani 1 1 d . . .
C6 C 0.91241(14) 0.41571(10) 0.41939(8) 0.0172(3) Uani 1 1 d . . .
H6A H 0.9657 0.3806 0.3971 0.021 Uiso 1 1 calc R . .
C7 C 0.65017(14) 0.37640(9) 0.52210(8) 0.0149(3) Uani 1 1 d . . .
C8 C 0.67313(14) 0.28971(9) 0.50576(8) 0.0145(3) Uani 1 1 d . . .
C9 C 0.78277(14) 0.28385(9) 0.46130(8) 0.0158(3) Uani 1 1 d . . .
C10 C 0.74084(15) 0.24272(10) 0.38495(9) 0.0216(3) Uani 1 1 d . . .
H10A H 0.7191 0.1825 0.3903 0.032 Uiso 1 1 calc R . .
H10B H 0.8083 0.2478 0.3558 0.032 Uiso 1 1 calc R . .
H10C H 0.6690 0.2722 0.3612 0.032 Uiso 1 1 calc R . .
C11 C 0.89204(15) 0.23388(10) 0.50273(10) 0.0236(4) Uani 1 1 d . . .
H11A H 0.8671 0.1739 0.5063 0.035 Uiso 1 1 calc R . .
H11B H 0.9138 0.2583 0.5512 0.035 Uiso 1 1 calc R . .
H11C H 0.9635 0.2382 0.4766 0.035 Uiso 1 1 calc R . .
C12 C 0.59985(14) 0.22290(9) 0.52877(8) 0.0152(3) Uani 1 1 d . . .
H12A H 0.6149 0.1655 0.5174 0.018 Uiso 1 1 calc R . .
C33 C 0.55485(15) 0.39635(10) 0.56280(8) 0.0183(3) Uani 1 1 d . . .
H13A H 0.5402 0.4538 0.5743 0.022 Uiso 1 1 calc R . .
C34 C 0.50297(14) 0.24246(9) 0.56930(8) 0.0148(3) Uani 1 1 d . . .
C15 C 0.48176(15) 0.32934(10) 0.58605(8) 0.0181(3) Uani 1 1 d . . .
H15A H 0.4175 0.3422 0.6133 0.022 Uiso 1 1 calc R . .
C2 C 0.41650(14) 0.17255(9) 0.59218(8) 0.0142(3) Uani 1 1 d . . .
C1 C 0.46700(14) 0.10924(9) 0.66742(8) 0.0142(3) Uani 1 1 d . . .
C18 C 0.59984(14) 0.12132(10) 0.70441(8) 0.0153(3) Uani 1 1 d . . .
C19 C 0.63959(14) 0.19634(10) 0.74507(8) 0.0159(3) Uani 1 1 d . . .
H19A H 0.5851 0.2419 0.7472 0.019 Uiso 1 1 calc R . .
C20 C 0.76043(14) 0.20239(10) 0.78216(8) 0.0163(3) Uani 1 1 d . . .
C21 C 0.84296(14) 0.13402(10) 0.78002(8) 0.0173(3) Uani 1 1 d . . .
C22 C 0.80531(15) 0.06018(10) 0.73823(9) 0.0212(3) Uani 1 1 d . . .
H22A H 0.8605 0.0151 0.7356 0.025 Uiso 1 1 calc R . .
C23 C 0.68474(15) 0.05442(10) 0.70049(8) 0.0195(3) Uani 1 1 d . . .
H23A H 0.6596 0.0053 0.6720 0.023 Uiso 1 1 calc R . .
C24 C 0.95990(14) 0.15640(10) 0.82840(8) 0.0186(3) Uani 1 1 d . . .
C25 C 0.94830(14) 0.23907(10) 0.85851(8) 0.0188(3) Uani 1 1 d . . .
C26 C 1.04583(15) 0.27548(11) 0.90740(9) 0.0234(4) Uani 1 1 d . . .
H26A H 1.0387 0.3304 0.9275 0.028 Uiso 1 1 calc R . .
C27 C 1.15441(15) 0.22878(12) 0.92592(9) 0.0262(4) Uani 1 1 d . . .
H27A H 1.2205 0.2530 0.9583 0.031 Uiso 1 1 calc R . .
C28 C 1.16517(16) 0.14648(12) 0.89663(9) 0.0277(4) Uani 1 1 d . . .
H28A H 1.2380 0.1158 0.9101 0.033 Uiso 1 1 calc R . .
C29 C 1.06835(15) 0.10933(11) 0.84729(9) 0.0245(4) Uani 1 1 d . . .
H29A H 1.0758 0.0543 0.8274 0.029 Uiso 1 1 calc R . .
C30 C 0.82119(15) 0.27696(10) 0.83020(9) 0.0199(3) Uani 1 1 d . . .
C31 C 0.74511(15) 0.29711(11) 0.89303(9) 0.0254(4) Uani 1 1 d . . .
H31A H 0.7854 0.3443 0.9225 0.038 Uiso 1 1 calc R . .
H31B H 0.7407 0.2467 0.9230 0.038 Uiso 1 1 calc R . .
H31C H 0.6617 0.3129 0.8729 0.038 Uiso 1 1 calc R . .
C32 C 0.83573(17) 0.35859(11) 0.78447(11) 0.0310(4) Uani 1 1 d . . .
H32A H 0.8742 0.4047 0.8159 0.047 Uiso 1 1 calc R . .
H32B H 0.7544 0.3758 0.7617 0.047 Uiso 1 1 calc R . .
H32C H 0.8876 0.3463 0.7472 0.047 Uiso 1 1 calc R . .
C13 C 1.15790(13) 0.34521(9) 0.22909(8) 0.0128(3) Uani 1 1 d . . .
C49 C 1.05318(13) 0.39011(9) 0.18203(8) 0.0133(3) Uani 1 1 d . . .
C35 C 0.96479(13) 0.43567(9) 0.21571(8) 0.0138(3) Uani 1 1 d . . .
H35A H 0.9704 0.4375 0.2667 0.017 Uiso 1 1 calc R . .
C36 C 0.86917(14) 0.47786(9) 0.17308(8) 0.0142(3) Uani 1 1 d . . .
C37 C 0.85935(14) 0.47386(9) 0.09606(8) 0.0140(3) Uani 1 1 d . . .
C38 C 0.94600(14) 0.42815(10) 0.06247(8) 0.0161(3) Uani 1 1 d . . .
H38A H 0.9395 0.4254 0.0115 0.019 Uiso 1 1 calc R . .
C39 C 1.04235(14) 0.38666(9) 0.10547(8) 0.0154(3) Uani 1 1 d . . .
H39A H 1.1006 0.3561 0.0830 0.019 Uiso 1 1 calc R . .
C40 C 0.75047(14) 0.52366(9) 0.06489(8) 0.0148(3) Uani 1 1 d . . .
C41 C 0.69554(14) 0.55864(10) 0.12301(8) 0.0167(3) Uani 1 1 d . . .
C42 C 0.59195(15) 0.61051(11) 0.10869(9) 0.0222(3) Uani 1 1 d . . .
H42A H 0.5554 0.6343 0.1471 0.027 Uiso 1 1 calc R . .
C43 C 0.54313(15) 0.62657(11) 0.03602(9) 0.0231(4) Uani 1 1 d . . .
H43A H 0.4739 0.6617 0.0260 0.028 Uiso 1 1 calc R . .
C44 C 0.59662(15) 0.59070(10) -0.02154(9) 0.0210(3) Uani 1 1 d . . .
H44A H 0.5623 0.6014 -0.0698 0.025 Uiso 1 1 calc R . .
C45 C 0.70090(14) 0.53904(10) -0.00775(8) 0.0185(3) Uani 1 1 d . . .
H45A H 0.7370 0.5151 -0.0463 0.022 Uiso 1 1 calc R . .
C46 C 0.76522(14) 0.53280(10) 0.19717(8) 0.0159(3) Uani 1 1 d . . .
C47 C 0.67913(15) 0.47970(11) 0.24166(9) 0.0226(4) Uani 1 1 d . . .
H47A H 0.7255 0.4644 0.2880 0.034 Uiso 1 1 calc R . .
H47B H 0.6495 0.4278 0.2147 0.034 Uiso 1 1 calc R . .
H47C H 0.6087 0.5138 0.2500 0.034 Uiso 1 1 calc R . .
C48 C 0.81907(15) 0.61328(10) 0.24183(8) 0.0202(3) Uani 1 1 d . . .
H48A H 0.8625 0.5955 0.2882 0.030 Uiso 1 1 calc R . .
H48B H 0.7517 0.6504 0.2500 0.030 Uiso 1 1 calc R . .
H48C H 0.8767 0.6443 0.2152 0.030 Uiso 1 1 calc R . .
C14 C 1.15701(13) 0.23244(9) 0.22689(8) 0.0129(3) Uani 1 1 d . . .
C50 C 1.05799(14) 0.18830(9) 0.17229(8) 0.0136(3) Uani 1 1 d . . .
C51 C 1.09351(14) 0.14473(10) 0.11156(8) 0.0164(3) Uani 1 1 d . . .
H51A H 1.1785 0.1391 0.1080 0.020 Uiso 1 1 calc R . .
C52 C 1.00482(14) 0.10981(10) 0.05673(8) 0.0165(3) Uani 1 1 d . . .
H52A H 1.0297 0.0801 0.0171 0.020 Uiso 1 1 calc R . .
C53 C 0.87796(14) 0.11981(9) 0.06182(8) 0.0140(3) Uani 1 1 d . . .
C54 C 0.84163(14) 0.16242(9) 0.12277(8) 0.0133(3) Uani 1 1 d . . .
C55 C 0.93008(14) 0.19569(9) 0.17819(8) 0.0135(3) Uani 1 1 d . . .
H55A H 0.9050 0.2227 0.2190 0.016 Uiso 1 1 calc R . .
C56 C 0.76446(14) 0.09693(9) 0.01051(8) 0.0147(3) Uani 1 1 d . . .
C57 C 0.66020(14) 0.12817(9) 0.03993(8) 0.0152(3) Uani 1 1 d . . .
C58 C 0.54137(14) 0.12005(11) 0.00005(8) 0.0200(3) Uani 1 1 d . . .
H58A H 0.4718 0.1408 0.0191 0.024 Uiso 1 1 calc R . .
C59 C 0.52784(15) 0.08033(11) -0.06890(9) 0.0236(4) Uani 1 1 d . . .
H59A H 0.4484 0.0747 -0.0961 0.028 Uiso 1 1 calc R . .
C60 C 0.63094(15) 0.04886(10) -0.09779(8) 0.0215(3) Uani 1 1 d . . .
H60A H 0.6198 0.0223 -0.1440 0.026 Uiso 1 1 calc R . .
C61 C 0.75027(15) 0.05669(10) -0.05836(8) 0.0175(3) Uani 1 1 d . . .
H61A H 0.8195 0.0355 -0.0775 0.021 Uiso 1 1 calc R . .
C62 C 0.69985(13) 0.17081(9) 0.11491(8) 0.0139(3) Uani 1 1 d . . .
C63 C 0.66555(15) 0.26686(10) 0.11461(9) 0.0198(3) Uani 1 1 d . . .
H63A H 0.5758 0.2713 0.1096 0.030 Uiso 1 1 calc R . .
H63B H 0.6968 0.2952 0.0742 0.030 Uiso 1 1 calc R . .
H63C H 0.7026 0.2941 0.1599 0.030 Uiso 1 1 calc R . .
C64 C 0.64286(15) 0.12303(11) 0.17576(8) 0.0206(3) Uani 1 1 d . . .
H64A H 0.5534 0.1298 0.1690 0.031 Uiso 1 1 calc R . .
H64B H 0.6783 0.1469 0.2227 0.031 Uiso 1 1 calc R . .
H64C H 0.6612 0.0625 0.1738 0.031 Uiso 1 1 calc R . .
B18 B 1.11383(16) 0.28646(10) 0.30170(9) 0.0132(3) Uani 1 1 d . . .
H4 H 0.4512 -0.0468 0.6762 0.017(4) Uiso 1 1 d R . .
B19 B 1.20977(16) 0.19417(11) 0.31264(9) 0.0147(3) Uani 1 1 d . . .
H5 H 0.3602 0.0816 0.7731 0.017(4) Uiso 1 1 d R . .
B23 B 1.24672(16) 0.28767(11) 0.36972(9) 0.0154(3) Uani 1 1 d . . .
H10 H 0.1761 -0.0297 0.6729 0.027(5) Uiso 1 1 d R . .
B17 B 1.21175(16) 0.38167(11) 0.31595(9) 0.0146(3) Uani 1 1 d . . .
H11 H 0.1360 0.1583 0.6945 0.023(4) Uiso 1 1 d R . .
B22 B 1.36995(16) 0.34815(11) 0.33505(9) 0.0169(4) Uani 1 1 d . . .
H6 H 0.3886 0.2447 0.7051 0.015(4) Uiso 1 1 d R . .
B20 B 1.30759(15) 0.19757(11) 0.24213(9) 0.0145(3) Uani 1 1 d . . .
H3 H 0.5294 0.0468 0.5569 0.020(4) Uiso 1 1 d R . .
B15 B 1.27107(15) 0.29186(11) 0.18875(9) 0.0141(3) Uani 1 1 d . . .
H8 H 0.3184 0.1259 0.4724 0.017(4) Uiso 1 1 d R . .
B16 B 1.31020(16) 0.38499(11) 0.24553(10) 0.0162(3) Uani 1 1 d . . .
H9 H 0.2794 -0.0519 0.5356 0.023(4) Uiso 1 1 d R . .
B24 B 1.36896(16) 0.23239(11) 0.33280(9) 0.0163(3) Uani 1 1 d . . .
H12 H 0.0822 0.0824 0.5448 0.024(5) Uiso 1 1 d R . .
B21 B 1.40624(16) 0.29240(11) 0.25544(9) 0.0169(4) Uani 1 1 d . . .
H7 H 0.2229 0.2519 0.5684 0.023(4) Uiso 1 1 d R . .
B4 B 0.39806(17) 0.00772(11) 0.65541(9) 0.0167(4) Uani 1 1 d . . .
H18 H 1.0159 0.2875 0.3109 0.016(4) Uiso 1 1 d R . .
B5 B 0.34278(17) 0.08583(11) 0.71445(9) 0.0173(4) Uani 1 1 d . . .
H19 H 1.1668 0.1342 0.3273 0.018(4) Uiso 1 1 d R . .
B3 B 0.44832(16) 0.06423(11) 0.58001(9) 0.0148(3) Uani 1 1 d . . .
H23 H 1.2339 0.2878 0.4268 0.021(4) Uiso 1 1 d R . .
B8 B 0.31495(17) 0.11254(11) 0.52977(9) 0.0171(4) Uani 1 1 d . . .
H24 H 1.4399 0.1966 0.3671 0.020(4) Uiso 1 1 d R . .
B9 B 0.30061(17) 0.00914(11) 0.56934(10) 0.0178(4) Uani 1 1 d . . .
H22 H 1.4407 0.3866 0.3703 0.019(4) Uiso 1 1 d R . .
B11 B 0.20970(17) 0.13537(11) 0.66485(10) 0.0184(4) Uani 1 1 d . . .
H21 H 1.5003 0.2951 0.2391 0.018(4) Uiso 1 1 d R . .
B10 B 0.23377(17) 0.02213(12) 0.65272(10) 0.0198(4) Uani 1 1 d . . .
H16 H 1.3301 0.4468 0.2196 0.020(4) Uiso 1 1 d R . .
B12 B 0.18199(17) 0.08715(12) 0.57489(10) 0.0194(4) Uani 1 1 d . . .
H15 H 1.2747 0.2903 0.1318 0.013(4) Uiso 1 1 d R . .
B7 B 0.25955(17) 0.19028(11) 0.58891(10) 0.0175(4) Uani 1 1 d . . .
H17 H 1.1743 0.4402 0.3337 0.015(4) Uiso 1 1 d R . .
B6 B 0.35868(16) 0.18888(11) 0.67465(9) 0.0161(3) Uani 1 1 d . . .
H20 H 1.3252 0.1391 0.2139 0.015(4) Uiso 1 1 d R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C16 C17 1.388(2) . ?
C16 C6 1.390(2) . ?
C16 H1A 0.9300 . ?
C17 C3 1.388(2) . ?
C17 H2A 0.9300 . ?
C3 C4 1.392(2) . ?
C3 H3A 0.9300 . ?
C4 C5 1.399(2) . ?
C4 C7 1.469(2) . ?
C5 C6 1.383(2) . ?
C5 C9 1.518(2) . ?
C6 H6A 0.9300 . ?
C7 C33 1.386(2) . ?
C7 C8 1.402(2) . ?
C8 C12 1.383(2) . ?
C8 C9 1.526(2) . ?
C9 C11 1.537(2) . ?
C9 C10 1.539(2) . ?
C10 H10A 0.9600 . ?
C10 H10B 0.9600 . ?
C10 H10C 0.9600 . ?
C11 H11A 0.9600 . ?
C11 H11B 0.9600 . ?
C11 H11C 0.9600 . ?
C12 C34 1.397(2) . ?
C12 H12A 0.9300 . ?
C33 C15 1.386(2) . ?
C33 H13A 0.9300 . ?
C34 C15 1.402(2) . ?
C34 C2 1.504(2) . ?
C15 H15A 0.9300 . ?
C2 B7 1.707(2) . ?
C2 B8 1.717(2) . ?
C2 B3 1.731(2) . ?
C2 C1 1.732(2) . ?
C2 B6 1.733(2) . ?
C1 C18 1.500(2) . ?
C1 B4 1.712(2) . ?
C1 B5 1.718(2) . ?
C1 B3 1.728(2) . ?
C1 B6 1.729(2) . ?
C18 C19 1.396(2) . ?
C18 C23 1.401(2) . ?
C19 C20 1.381(2) . ?
C19 H19A 0.9300 . ?
C20 C21 1.398(2) . ?
C20 C30 1.520(2) . ?
C21 C22 1.387(2) . ?
C21 C24 1.468(2) . ?
C22 C23 1.383(2) . ?
C22 H22A 0.9300 . ?
C23 H23A 0.9300 . ?
C24 C29 1.393(2) . ?
C24 C25 1.399(2) . ?
C25 C26 1.387(2) . ?
C25 C30 1.525(2) . ?
C26 C27 1.390(2) . ?
C26 H26A 0.9300 . ?
C27 C28 1.387(3) . ?
C27 H27A 0.9300 . ?
C28 C29 1.391(2) . ?
C28 H28A 0.9300 . ?
C29 H29A 0.9300 . ?
C30 C32 1.535(2) . ?
C30 C31 1.536(2) . ?
C31 H31A 0.9600 . ?
C31 H31B 0.9600 . ?
C31 H31C 0.9600 . ?
C32 H32A 0.9600 . ?
C32 H32B 0.9600 . ?
C32 H32C 0.9600 . ?
C13 C49 1.509(2) . ?
C13 B17 1.707(2) . ?
C13 B16 1.718(2) . ?
C13 B15 1.729(2) . ?
C13 B18 1.730(2) . ?
C13 C14 1.737(2) . ?
C49 C39 1.396(2) . ?
C49 C35 1.401(2) . ?
C35 C36 1.383(2) . ?
C35 H35A 0.9300 . ?
C36 C37 1.405(2) . ?
C36 C46 1.528(2) . ?
C37 C38 1.387(2) . ?
C37 C40 1.468(2) . ?
C38 C39 1.387(2) . ?
C38 H38A 0.9300 . ?
C39 H39A 0.9300 . ?
C40 C45 1.392(2) . ?
C40 C41 1.399(2) . ?
C41 C42 1.384(2) . ?
C41 C46 1.524(2) . ?
C42 C43 1.393(2) . ?
C42 H42A 0.9300 . ?
C43 C44 1.388(2) . ?
C43 H43A 0.9300 . ?
C44 C45 1.387(2) . ?
C44 H44A 0.9300 . ?
C45 H45A 0.9300 . ?
C46 C48 1.537(2) . ?
C46 C47 1.539(2) . ?
C47 H47A 0.9600 . ?
C47 H47B 0.9600 . ?
C47 H47C 0.9600 . ?
C48 H48A 0.9600 . ?
C48 H48B 0.9600 . ?
C48 H48C 0.9600 . ?
C14 C50 1.503(2) . ?
C14 B20 1.704(2) . ?
C14 B19 1.715(2) . ?
C14 B18 1.723(2) . ?
C14 B15 1.737(2) . ?
C50 C51 1.399(2) . ?
C50 C55 1.400(2) . ?
C51 C52 1.383(2) . ?
C51 H51A 0.9300 . ?
C52 C53 1.390(2) . ?
C52 H52A 0.9300 . ?
C53 C54 1.399(2) . ?
C53 C56 1.469(2) . ?
C54 C55 1.380(2) . ?
C54 C62 1.518(2) . ?
C55 H55A 0.9300 . ?
C56 C61 1.392(2) . ?
C56 C57 1.402(2) . ?
C57 C58 1.384(2) . ?
C57 C62 1.523(2) . ?
C58 C59 1.390(2) . ?
C58 H58A 0.9300 . ?
C59 C60 1.388(2) . ?
C59 H59A 0.9300 . ?
C60 C61 1.385(2) . ?
C60 H60A 0.9300 . ?
C61 H61A 0.9300 . ?
C62 C64 1.531(2) . ?
C62 C63 1.534(2) . ?
C63 H63A 0.9600 . ?
C63 H63B 0.9600 . ?
C63 H63C 0.9600 . ?
C64 H64A 0.9600 . ?
C64 H64B 0.9600 . ?
C64 H64C 0.9600 . ?
B18 B23 1.764(2) . ?
B18 B19 1.774(2) . ?
B18 B17 1.779(2) . ?
B18 H18 1.0885 . ?
B19 B20 1.776(2) . ?
B19 B23 1.779(2) . ?
B19 B24 1.783(2) . ?
B19 H19 1.0745 . ?
B23 B17 1.779(2) . ?
B23 B24 1.789(2) . ?
B23 B22 1.789(2) . ?
B23 H23 1.0756 . ?
B17 B22 1.778(2) . ?
B17 B16 1.779(2) . ?
B17 H17 1.0635 . ?
B22 B24 1.783(2) . ?
B22 B21 1.783(2) . ?
B22 B16 1.785(2) . ?
B22 H22 1.0881 . ?
B20 B21 1.777(2) . ?
B20 B24 1.779(2) . ?
B20 B15 1.782(2) . ?
B20 H20 1.0698 . ?
B15 B21 1.767(2) . ?
B15 B16 1.774(2) . ?
B15 H15 1.0526 . ?
B16 B21 1.778(2) . ?
B16 H16 1.0967 . ?
B24 B21 1.787(2) . ?
B24 H24 1.0851 . ?
B21 H21 1.0915 . ?
B4 B9 1.774(2) . ?
B4 B10 1.778(3) . ?
B4 B3 1.780(2) . ?
B4 B5 1.780(2) . ?
B4 H4 1.0714 . ?
B5 B6 1.767(2) . ?
B5 B11 1.780(3) . ?
B5 B10 1.783(3) . ?
B5 H5 1.0707 . ?
B3 B9 1.765(2) . ?
B3 B8 1.778(2) . ?
B3 H3 1.0584 . ?
B8 B9 1.768(2) . ?
B8 B7 1.778(2) . ?
B8 B12 1.783(3) . ?
B8 H8 1.0808 . ?
B9 B12 1.786(3) . ?
B9 B10 1.790(2) . ?
B9 H9 1.1228 . ?
B11 B6 1.767(2) . ?
B11 B7 1.774(2) . ?
B11 B10 1.787(3) . ?
B11 B12 1.790(3) . ?
B11 H11 1.0843 . ?
B10 B12 1.787(3) . ?
B10 H10 1.0962 . ?
B12 B7 1.775(3) . ?
B12 H12 1.1371 . ?
B7 B6 1.777(2) . ?
B7 H7 1.0877 . ?
B6 H6 1.0405 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C17 C16 C6 120.70(14) . . ?
C17 C16 H1A 119.6 . . ?
C6 C16 H1A 119.6 . . ?
C3 C17 C16 120.76(14) . . ?
C3 C17 H2A 119.6 . . ?
C16 C17 H2A 119.6 . . ?
C17 C3 C4 118.47(14) . . ?
C17 C3 H3A 120.8 . . ?
C4 C3 H3A 120.8 . . ?
C3 C4 C5 120.84(14) . . ?
C3 C4 C7 130.96(14) . . ?
C5 C4 C7 108.20(13) . . ?
C6 C5 C4 120.17(13) . . ?
C6 C5 C9 128.42(13) . . ?
C4 C5 C9 111.41(13) . . ?
C5 C6 C16 119.04(14) . . ?
C5 C6 H6A 120.5 . . ?
C16 C6 H6A 120.5 . . ?
C33 C7 C8 120.36(14) . . ?
C33 C7 C4 131.22(14) . . ?
C8 C7 C4 108.42(13) . . ?
C12 C8 C7 120.66(14) . . ?
C12 C8 C9 128.41(13) . . ?
C7 C8 C9 110.92(13) . . ?
C5 C9 C8 101.03(11) . . ?
C5 C9 C11 111.48(12) . . ?
C8 C9 C11 111.50(13) . . ?
C5 C9 C10 110.42(12) . . ?
C8 C9 C10 111.50(12) . . ?
C11 C9 C10 110.59(13) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C8 C12 C34 119.34(13) . . ?
C8 C12 H12A 120.3 . . ?
C34 C12 H12A 120.3 . . ?
C15 C33 C7 118.93(14) . . ?
C15 C33 H13A 120.5 . . ?
C7 C33 H13A 120.5 . . ?
C12 C34 C15 119.51(14) . . ?
C12 C34 C2 121.33(13) . . ?
C15 C34 C2 119.08(13) . . ?
C33 C15 C34 121.19(14) . . ?
C33 C15 H15A 119.4 . . ?
C34 C15 H15A 119.4 . . ?
C34 C2 B7 120.23(12) . . ?
C34 C2 B8 122.41(12) . . ?
B7 C2 B8 62.55(10) . . ?
C34 C2 B3 120.26(12) . . ?
B7 C2 B3 112.74(12) . . ?
B8 C2 B3 62.11(9) . . ?
C34 C2 C1 119.41(12) . . ?
B7 C2 C1 109.58(11) . . ?
B8 C2 C1 109.60(11) . . ?
B3 C2 C1 59.87(9) . . ?
C34 C2 B6 116.71(12) . . ?
B7 C2 B6 62.22(10) . . ?
B8 C2 B6 112.91(12) . . ?
B3 C2 B6 110.85(11) . . ?
C1 C2 B6 59.85(9) . . ?
C18 C1 B4 120.78(12) . . ?
C18 C1 B5 123.08(12) . . ?
B4 C1 B5 62.51(10) . . ?
C18 C1 B3 116.15(12) . . ?
B4 C1 B3 62.30(9) . . ?
B5 C1 B3 113.09(12) . . ?
C18 C1 B6 120.23(12) . . ?
B4 C1 B6 112.40(12) . . ?
B5 C1 B6 61.70(9) . . ?
B3 C1 B6 111.17(11) . . ?
C18 C1 C2 118.73(12) . . ?
B4 C1 C2 109.58(11) . . ?
B5 C1 C2 109.49(11) . . ?
B3 C1 C2 60.02(9) . . ?
B6 C1 C2 60.08(9) . . ?
C19 C18 C23 119.16(14) . . ?
C19 C18 C1 121.49(13) . . ?
C23 C18 C1 119.30(13) . . ?
C20 C19 C18 119.57(14) . . ?
C20 C19 H19A 120.2 . . ?
C18 C19 H19A 120.2 . . ?
C19 C20 C21 120.81(14) . . ?
C19 C20 C30 127.93(14) . . ?
C21 C20 C30 111.24(13) . . ?
C22 C21 C20 119.97(14) . . ?
C22 C21 C24 131.57(14) . . ?
C20 C21 C24 108.43(13) . . ?
C23 C22 C21 119.23(14) . . ?
C23 C22 H22A 120.4 . . ?
C21 C22 H22A 120.4 . . ?
C22 C23 C18 121.20(14) . . ?
C22 C23 H23A 119.4 . . ?
C18 C23 H23A 119.4 . . ?
C29 C24 C25 120.84(15) . . ?
C29 C24 C21 130.88(15) . . ?
C25 C24 C21 108.26(13) . . ?
C26 C25 C24 120.07(15) . . ?
C26 C25 C30 128.81(15) . . ?
C24 C25 C30 111.13(13) . . ?
C25 C26 C27 119.13(16) . . ?
C25 C26 H26A 120.4 . . ?
C27 C26 H26A 120.4 . . ?
C28 C27 C26 120.71(16) . . ?
C28 C27 H27A 119.6 . . ?
C26 C27 H27A 119.6 . . ?
C27 C28 C29 120.77(16) . . ?
C27 C28 H28A 119.6 . . ?
C29 C28 H28A 119.6 . . ?
C28 C29 C24 118.48(16) . . ?
C28 C29 H29A 120.8 . . ?
C24 C29 H29A 120.8 . . ?
C20 C30 C25 100.87(12) . . ?
C20 C30 C32 110.94(13) . . ?
C25 C30 C32 111.67(13) . . ?
C20 C30 C31 111.17(13) . . ?
C25 C30 C31 111.84(13) . . ?
C32 C30 C31 110.08(14) . . ?
C30 C31 H31A 109.5 . . ?
C30 C31 H31B 109.5 . . ?
H31A C31 H31B 109.5 . . ?
C30 C31 H31C 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
C30 C32 H32A 109.5 . . ?
C30 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C30 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?
C49 C13 B17 121.05(12) . . ?
C49 C13 B16 123.91(12) . . ?
B17 C13 B16 62.60(9) . . ?
C49 C13 B15 120.20(12) . . ?
B17 C13 B15 112.70(11) . . ?
B16 C13 B15 61.95(9) . . ?
C49 C13 B18 115.68(12) . . ?
B17 C13 B18 62.34(9) . . ?
B16 C13 B18 113.02(11) . . ?
B15 C13 B18 110.89(11) . . ?
C49 C13 C14 117.89(11) . . ?
B17 C13 C14 109.52(11) . . ?
B16 C13 C14 109.67(11) . . ?
B15 C13 C14 60.14(9) . . ?
B18 C13 C14 59.62(8) . . ?
C39 C49 C35 119.39(13) . . ?
C39 C49 C13 121.15(13) . . ?
C35 C49 C13 119.46(13) . . ?
C36 C35 C49 119.93(13) . . ?
C36 C35 H35A 120.0 . . ?
C49 C35 H35A 120.0 . . ?
C35 C36 C37 120.09(13) . . ?
C35 C36 C46 129.21(13) . . ?
C37 C36 C46 110.69(12) . . ?
C38 C37 C36 120.16(13) . . ?
C38 C37 C40 131.13(14) . . ?
C36 C37 C40 108.70(13) . . ?
C39 C38 C37 119.51(14) . . ?
C39 C38 H38A 120.2 . . ?
C37 C38 H38A 120.2 . . ?
C38 C39 C49 120.91(14) . . ?
C38 C39 H39A 119.5 . . ?
C49 C39 H39A 119.5 . . ?
C45 C40 C41 120.82(14) . . ?
C45 C40 C37 131.02(14) . . ?
C41 C40 C37 108.15(13) . . ?
C42 C41 C40 120.02(14) . . ?
C42 C41 C46 128.50(14) . . ?
C40 C41 C46 111.48(13) . . ?
C41 C42 C43 119.13(15) . . ?
C41 C42 H42A 120.4 . . ?
C43 C42 H42A 120.4 . . ?
C44 C43 C42 120.73(15) . . ?
C44 C43 H43A 119.6 . . ?
C42 C43 H43A 119.6 . . ?
C45 C44 C43 120.55(14) . . ?
C45 C44 H44A 119.7 . . ?
C43 C44 H44A 119.7 . . ?
C44 C45 C40 118.73(14) . . ?
C44 C45 H45A 120.6 . . ?
C40 C45 H45A 120.6 . . ?
C41 C46 C36 100.97(12) . . ?
C41 C46 C48 110.93(12) . . ?
C36 C46 C48 111.73(12) . . ?
C41 C46 C47 111.36(12) . . ?
C36 C46 C47 111.84(12) . . ?
C48 C46 C47 109.78(12) . . ?
C46 C47 H47A 109.5 . . ?
C46 C47 H47B 109.5 . . ?
H47A C47 H47B 109.5 . . ?
C46 C47 H47C 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
C46 C48 H48A 109.5 . . ?
C46 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C46 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C14 B20 122.12(12) . . ?
C50 C14 B19 125.00(12) . . ?
B20 C14 B19 62.58(9) . . ?
C50 C14 B18 119.76(12) . . ?
B20 C14 B18 112.71(11) . . ?
B19 C14 B18 62.12(9) . . ?
C50 C14 B15 115.05(12) . . ?
B20 C14 B15 62.35(9) . . ?
B19 C14 B15 113.11(11) . . ?
B18 C14 B15 110.82(11) . . ?
C50 C14 C13 116.42(11) . . ?
B20 C14 C13 109.57(11) . . ?
B19 C14 C13 109.79(10) . . ?
B18 C14 C13 59.98(8) . . ?
B15 C14 C13 59.69(8) . . ?
C51 C50 C55 119.31(13) . . ?
C51 C50 C14 119.54(13) . . ?
C55 C50 C14 120.97(13) . . ?
C52 C51 C50 121.36(14) . . ?
C52 C51 H51A 119.3 . . ?
C50 C51 H51A 119.3 . . ?
C51 C52 C53 118.98(13) . . ?
C51 C52 H52A 120.5 . . ?
C53 C52 H52A 120.5 . . ?
C52 C53 C54 120.01(13) . . ?
C52 C53 C56 131.46(13) . . ?
C54 C53 C56 108.44(13) . . ?
C55 C54 C53 120.99(13) . . ?
C55 C54 C62 127.67(13) . . ?
C53 C54 C62 111.21(12) . . ?
C54 C55 C50 119.30(13) . . ?
C54 C55 H55A 120.3 . . ?
C50 C55 H55A 120.3 . . ?
C61 C56 C57 120.88(14) . . ?
C61 C56 C53 130.86(14) . . ?
C57 C56 C53 108.15(13) . . ?
C58 C57 C56 120.00(14) . . ?
C58 C57 C62 128.91(14) . . ?
C56 C57 C62 111.07(13) . . ?
C57 C58 C59 118.89(15) . . ?
C57 C58 H58A 120.6 . . ?
C59 C58 H58A 120.6 . . ?
C60 C59 C58 121.10(15) . . ?
C60 C59 H59A 119.4 . . ?
C58 C59 H59A 119.4 . . ?
C61 C60 C59 120.48(14) . . ?
C61 C60 H60A 119.8 . . ?
C59 C60 H60A 119.8 . . ?
C60 C61 C56 118.65(14) . . ?
C60 C61 H61A 120.7 . . ?
C56 C61 H61A 120.7 . . ?
C54 C62 C57 101.08(11) . . ?
C54 C62 C64 111.88(12) . . ?
C57 C62 C64 111.82(12) . . ?
C54 C62 C63 110.24(12) . . ?
C57 C62 C63 111.32(12) . . ?
C64 C62 C63 110.22(12) . . ?
C62 C63 H63A 109.5 . . ?
C62 C63 H63B 109.5 . . ?
H63A C63 H63B 109.5 . . ?
C62 C63 H63C 109.5 . . ?
H63A C63 H63C 109.5 . . ?
H63B C63 H63C 109.5 . . ?
C62 C64 H64A 109.5 . . ?
C62 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C62 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C14 B18 C13 60.40(8) . . ?
C14 B18 B23 106.12(11) . . ?
C13 B18 B23 105.96(11) . . ?
C14 B18 B19 58.69(9) . . ?
C13 B18 B19 107.40(11) . . ?
B23 B18 B19 60.37(9) . . ?
C14 B18 B17 106.85(11) . . ?
C13 B18 B17 58.19(9) . . ?
B23 B18 B17 60.28(9) . . ?
B19 B18 B17 108.76(12) . . ?
C14 B18 H18 120.9 . . ?
C13 B18 H18 118.1 . . ?
B23 B18 H18 126.5 . . ?
B19 B18 H18 124.9 . . ?
B17 B18 H18 120.6 . . ?
C14 B19 B18 59.18(9) . . ?
C14 B19 B20 58.43(9) . . ?
B18 B19 B20 107.01(11) . . ?
C14 B19 B23 105.84(11) . . ?
B18 B19 B23 59.53(9) . . ?
B20 B19 B23 107.90(12) . . ?
C14 B19 B24 105.58(11) . . ?
B18 B19 B24 107.49(12) . . ?
B20 B19 B24 59.99(9) . . ?
B23 B19 B24 60.30(9) . . ?
C14 B19 H19 115.9 . . ?
B18 B19 H19 117.5 . . ?
B20 B19 H19 121.1 . . ?
B23 B19 H19 127.0 . . ?
B24 B19 H19 129.7 . . ?
B18 B23 B19 60.10(9) . . ?
B18 B23 B17 60.28(9) . . ?
B19 B23 B17 108.54(11) . . ?
B18 B23 B24 107.67(11) . . ?
B19 B23 B24 59.96(9) . . ?
B17 B23 B24 107.76(12) . . ?
B18 B23 B22 107.78(12) . . ?
B19 B23 B22 108.03(12) . . ?
B17 B23 B22 59.78(10) . . ?
B24 B23 B22 59.79(10) . . ?
B18 B23 H23 119.5 . . ?
B19 B23 H23 121.6 . . ?
B17 B23 H23 119.9 . . ?
B24 B23 H23 124.5 . . ?
B22 B23 H23 123.2 . . ?
C13 B17 B22 106.14(11) . . ?
C13 B17 B18 59.47(9) . . ?
B22 B17 B18 107.60(11) . . ?
C13 B17 B23 106.29(11) . . ?
B22 B17 B23 60.39(10) . . ?
B18 B17 B23 59.44(9) . . ?
C13 B17 B16 59.01(9) . . ?
B22 B17 B16 60.23(10) . . ?
B18 B17 B16 107.84(11) . . ?
B23 B17 B16 108.57(12) . . ?
C13 B17 H17 117.4 . . ?
B22 B17 H17 127.0 . . ?
B18 B17 H17 119.7 . . ?
B23 B17 H17 126.4 . . ?
B16 B17 H17 119.6 . . ?
B17 B22 B24 108.04(12) . . ?
B17 B22 B21 107.46(12) . . ?
B24 B22 B21 60.13(10) . . ?
B17 B22 B16 59.91(9) . . ?
B24 B22 B16 108.26(12) . . ?
B21 B22 B16 59.76(10) . . ?
B17 B22 B23 59.83(9) . . ?
B24 B22 B23 60.09(10) . . ?
B21 B22 B23 107.73(12) . . ?
B16 B22 B23 107.88(12) . . ?
B17 B22 H22 121.5 . . ?
B24 B22 H22 122.4 . . ?
B21 B22 H22 121.7 . . ?
B16 B22 H22 120.6 . . ?
B23 B22 H22 122.7 . . ?
C14 B20 B19 58.99(9) . . ?
C14 B20 B21 106.36(11) . . ?
B19 B20 B21 108.45(12) . . ?
C14 B20 B24 106.17(11) . . ?
B19 B20 B24 60.19(9) . . ?
B21 B20 B24 60.32(10) . . ?
C14 B20 B15 59.71(9) . . ?
B19 B20 B15 108.11(11) . . ?
B21 B20 B15 59.54(10) . . ?
B24 B20 B15 107.84(12) . . ?
C14 B20 H20 115.7 . . ?
B19 B20 H20 119.8 . . ?
B21 B20 H20 127.2 . . ?
B24 B20 H20 128.7 . . ?
B15 B20 H20 118.0 . . ?
C13 B15 C14 60.17(8) . . ?
C13 B15 B21 105.80(11) . . ?
C14 B15 B21 105.44(11) . . ?
C13 B15 B16 58.73(9) . . ?
C14 B15 B16 107.14(11) . . ?
B21 B15 B16 60.27(10) . . ?
C13 B15 B20 106.45(11) . . ?
C14 B15 B20 57.94(9) . . ?
B21 B15 B20 60.11(10) . . ?
B16 B15 B20 108.56(12) . . ?
C13 B15 H15 123.9 . . ?
C14 B15 H15 121.1 . . ?
B21 B15 H15 123.4 . . ?
B16 B15 H15 124.0 . . ?
B20 B15 H15 120.0 . . ?
C13 B16 B15 59.32(9) . . ?
C13 B16 B21 105.79(11) . . ?
B15 B16 B21 59.67(9) . . ?
C13 B16 B17 58.39(9) . . ?
B15 B16 B17 107.19(12) . . ?
B21 B16 B17 107.66(12) . . ?
C13 B16 B22 105.36(12) . . ?
B15 B16 B22 107.52(12) . . ?
B21 B16 B22 60.08(10) . . ?
B17 B16 B22 59.86(10) . . ?
C13 B16 H16 116.6 . . ?
B15 B16 H16 118.7 . . ?
B21 B16 H16 127.5 . . ?
B17 B16 H16 120.2 . . ?
B22 B16 H16 128.5 . . ?
B20 B24 B19 59.82(9) . . ?
B20 B24 B22 107.81(12) . . ?
B19 B24 B22 108.12(12) . . ?
B20 B24 B21 59.80(10) . . ?
B19 B24 B21 107.73(12) . . ?
B22 B24 B21 59.94(10) . . ?
B20 B24 B23 107.32(12) . . ?
B19 B24 B23 59.74(9) . . ?
B22 B24 B23 60.11(10) . . ?
B21 B24 B23 107.59(12) . . ?
B20 B24 H24 122.3 . . ?
B19 B24 H24 122.4 . . ?
B22 B24 H24 121.0 . . ?
B21 B24 H24 121.4 . . ?
B23 B24 H24 122.3 . . ?
B15 B21 B20 60.35(9) . . ?
B15 B21 B16 60.06(9) . . ?
B20 B21 B16 108.58(12) . . ?
B15 B21 B22 107.90(12) . . ?
B20 B21 B22 107.88(12) . . ?
B16 B21 B22 60.16(10) . . ?
B15 B21 B24 108.14(12) . . ?
B20 B21 B24 59.88(10) . . ?
B16 B21 B24 108.41(12) . . ?
B22 B21 B24 59.93(10) . . ?
B15 B21 H21 120.8 . . ?
B20 B21 H21 122.1 . . ?
B16 B21 H21 120.2 . . ?
B22 B21 H21 122.1 . . ?
B24 B21 H21 122.9 . . ?
C1 B4 B9 105.97(12) . . ?
C1 B4 B10 106.10(12) . . ?
B9 B4 B10 60.52(10) . . ?
C1 B4 B3 59.28(9) . . ?
B9 B4 B3 59.58(10) . . ?
B10 B4 B3 108.05(12) . . ?
C1 B4 B5 58.88(9) . . ?
B9 B4 B5 108.32(12) . . ?
B10 B4 B5 60.16(10) . . ?
B3 B4 B5 107.73(12) . . ?
C1 B4 H4 118.5 . . ?
B9 B4 H4 124.4 . . ?
B10 B4 H4 127.5 . . ?
B3 B4 H4 117.7 . . ?
B5 B4 H4 122.2 . . ?
C1 B5 B6 59.46(9) . . ?
C1 B5 B4 58.60(9) . . ?
B6 B5 B4 107.45(12) . . ?
C1 B5 B11 106.16(12) . . ?
B6 B5 B11 59.75(10) . . ?
B4 B5 B11 107.91(12) . . ?
C1 B5 B10 105.65(12) . . ?
B6 B5 B10 107.68(12) . . ?
B4 B5 B10 59.86(10) . . ?
B11 B5 B10 60.19(10) . . ?
C1 B5 H5 118.6 . . ?
B6 B5 H5 118.0 . . ?
B4 B5 H5 122.4 . . ?
B11 B5 H5 124.5 . . ?
B10 B5 H5 127.6 . . ?
C1 B3 C2 60.12(8) . . ?
C1 B3 B9 105.66(12) . . ?
C2 B3 B9 105.44(12) . . ?
C1 B3 B8 106.98(11) . . ?
C2 B3 B8 58.56(9) . . ?
B9 B3 B8 59.86(10) . . ?
C1 B3 B4 58.42(9) . . ?
C2 B3 B4 106.59(11) . . ?
B9 B3 B4 60.04(10) . . ?
B8 B3 B4 108.19(12) . . ?
C1 B3 H3 118.8 . . ?
C2 B3 H3 120.2 . . ?
B9 B3 H3 127.3 . . ?
B8 B3 H3 124.1 . . ?
B4 B3 H3 122.2 . . ?
C2 B8 B9 105.92(12) . . ?
C2 B8 B7 58.46(9) . . ?
B9 B8 B7 107.72(12) . . ?
C2 B8 B3 59.33(9) . . ?
B9 B8 B3 59.71(10) . . ?
B7 B8 B3 107.22(12) . . ?
C2 B8 B12 105.65(12) . . ?
B9 B8 B12 60.39(10) . . ?
B7 B8 B12 59.81(10) . . ?
B3 B8 B12 107.92(12) . . ?
C2 B8 H8 116.5 . . ?
B9 B8 H8 126.6 . . ?
B7 B8 H8 121.4 . . ?
B3 B8 H8 117.5 . . ?
B12 B8 H8 129.0 . . ?
B3 B9 B8 60.44(10) . . ?
B3 B9 B4 60.38(10) . . ?
B8 B9 B4 108.92(12) . . ?
B3 B9 B12 108.35(12) . . ?
B8 B9 B12 60.20(10) . . ?
B4 B9 B12 108.16(12) . . ?
B3 B9 B10 108.14(12) . . ?
B8 B9 B10 108.40(12) . . ?
B4 B9 B10 59.85(10) . . ?
B12 B9 B10 59.96(10) . . ?
B3 B9 H9 123.4 . . ?
B8 B9 H9 122.8 . . ?
B4 B9 H9 120.9 . . ?
B12 B9 H9 120.7 . . ?
B10 B9 H9 119.6 . . ?
B6 B11 B7 60.26(10) . . ?
B6 B11 B5 59.77(10) . . ?
B7 B11 B5 108.13(12) . . ?
B6 B11 B10 107.54(12) . . ?
B7 B11 B10 107.66(12) . . ?
B5 B11 B10 59.99(10) . . ?
B6 B11 B12 107.83(12) . . ?
B7 B11 B12 59.72(10) . . ?
B5 B11 B12 108.08(12) . . ?
B10 B11 B12 59.94(10) . . ?
B6 B11 H11 120.7 . . ?
B7 B11 H11 123.5 . . ?
B5 B11 H11 119.1 . . ?
B10 B11 H11 121.6 . . ?
B12 B11 H11 124.1 . . ?
B4 B10 B5 59.97(10) . . ?
B4 B10 B11 107.70(12) . . ?
B5 B10 B11 59.82(10) . . ?
B4 B10 B12 107.94(12) . . ?
B5 B10 B12 108.09(12) . . ?
B11 B10 B12 60.13(10) . . ?
B4 B10 B9 59.63(10) . . ?
B5 B10 B9 107.46(12) . . ?
B11 B10 B9 107.52(12) . . ?
B12 B10 B9 59.91(10) . . ?
B4 B10 H10 119.1 . . ?
B5 B10 H10 121.0 . . ?
B11 B10 H10 124.2 . . ?
B12 B10 H10 123.7 . . ?
B9 B10 H10 121.2 . . ?
B7 B12 B8 59.96(10) . . ?
B7 B12 B9 107.07(12) . . ?
B8 B12 B9 59.41(10) . . ?
B7 B12 B10 107.62(12) . . ?
B8 B12 B10 107.90(12) . . ?
B9 B12 B10 60.13(10) . . ?
B7 B12 B11 59.69(10) . . ?
B8 B12 B11 107.75(12) . . ?
B9 B12 B11 107.53(12) . . ?
B10 B12 B11 59.93(10) . . ?
B7 B12 H12 119.6 . . ?
B8 B12 H12 122.8 . . ?
B9 B12 H12 125.4 . . ?
B10 B12 H12 122.6 . . ?
B11 B12 H12 119.4 . . ?
C2 B7 B11 106.62(12) . . ?
C2 B7 B12 106.39(12) . . ?
B11 B7 B12 60.59(10) . . ?
C2 B7 B6 59.59(9) . . ?
B11 B7 B6 59.66(10) . . ?
B12 B7 B6 108.05(12) . . ?
C2 B7 B8 58.99(9) . . ?
B11 B7 B8 108.69(12) . . ?
B12 B7 B8 60.23(10) . . ?
B6 B7 B8 107.94(12) . . ?
C2 B7 H7 119.0 . . ?
B11 B7 H7 124.0 . . ?
B12 B7 H7 126.1 . . ?
B6 B7 H7 118.9 . . ?
B8 B7 H7 121.5 . . ?
C1 B6 C2 60.07(9) . . ?
C1 B6 B11 106.25(12) . . ?
C2 B6 B11 105.85(12) . . ?
C1 B6 B5 58.84(9) . . ?
C2 B6 B5 107.21(11) . . ?
B11 B6 B5 60.49(10) . . ?
C1 B6 B7 106.56(11) . . ?
C2 B6 B7 58.19(9) . . ?
B11 B6 B7 60.08(10) . . ?
B5 B6 B7 108.56(12) . . ?
C1 B6 H6 118.1 . . ?
C2 B6 H6 117.9 . . ?
B11 B6 H6 128.5 . . ?
B5 B6 H6 123.3 . . ?
B7 B6 H6 123.4 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C6 C16 C17 C3 0.7(2) . . . . ?
C16 C17 C3 C4 -0.7(2) . . . . ?
C17 C3 C4 C5 -0.3(2) . . . . ?
C17 C3 C4 C7 180.00(15) . . . . ?
C3 C4 C5 C6 1.2(2) . . . . ?
C7 C4 C5 C6 -178.98(13) . . . . ?
C3 C4 C5 C9 -178.68(13) . . . . ?
C7 C4 C5 C9 1.11(17) . . . . ?
C4 C5 C6 C16 -1.2(2) . . . . ?
C9 C5 C6 C16 178.67(14) . . . . ?
C17 C16 C6 C5 0.3(2) . . . . ?
C3 C4 C7 C33 -1.0(3) . . . . ?
C5 C4 C7 C33 179.26(16) . . . . ?
C3 C4 C7 C8 178.38(15) . . . . ?
C5 C4 C7 C8 -1.38(17) . . . . ?
C33 C7 C8 C12 1.2(2) . . . . ?
C4 C7 C8 C12 -178.26(13) . . . . ?
C33 C7 C8 C9 -179.44(13) . . . . ?
C4 C7 C8 C9 1.12(16) . . . . ?
C6 C5 C9 C8 179.67(14) . . . . ?
C4 C5 C9 C8 -0.43(15) . . . . ?
C6 C5 C9 C11 61.1(2) . . . . ?
C4 C5 C9 C11 -118.98(14) . . . . ?
C6 C5 C9 C10 -62.2(2) . . . . ?
C4 C5 C9 C10 117.67(14) . . . . ?
C12 C8 C9 C5 178.88(14) . . . . ?
C7 C8 C9 C5 -0.45(15) . . . . ?
C12 C8 C9 C11 -62.6(2) . . . . ?
C7 C8 C9 C11 118.09(14) . . . . ?
C12 C8 C9 C10 61.6(2) . . . . ?
C7 C8 C9 C10 -117.76(14) . . . . ?
C7 C8 C12 C34 -0.7(2) . . . . ?
C9 C8 C12 C34 -179.92(14) . . . . ?
C8 C7 C33 C15 -0.9(2) . . . . ?
C4 C7 C33 C15 178.36(15) . . . . ?
C8 C12 C34 C15 -0.1(2) . . . . ?
C8 C12 C34 C2 176.78(13) . . . . ?
C7 C33 C15 C34 0.2(2) . . . . ?
C12 C34 C15 C33 0.3(2) . . . . ?
C2 C34 C15 C33 -176.62(14) . . . . ?
C12 C34 C2 B7 -139.98(14) . . . . ?
C15 C34 C2 B7 36.9(2) . . . . ?
C12 C34 C2 B8 -65.17(19) . . . . ?
C15 C34 C2 B8 111.71(16) . . . . ?
C12 C34 C2 B3 9.1(2) . . . . ?
C15 C34 C2 B3 -174.02(13) . . . . ?
C12 C34 C2 C1 79.33(17) . . . . ?
C15 C34 C2 C1 -103.79(16) . . . . ?
C12 C34 C2 B6 148.12(14) . . . . ?
C15 C34 C2 B6 -35.00(19) . . . . ?
C34 C2 C1 C18 -4.67(19) . . . . ?
B7 C2 C1 C18 -149.16(13) . . . . ?
B8 C2 C1 C18 143.97(13) . . . . ?
B3 C2 C1 C18 105.30(14) . . . . ?
B6 C2 C1 C18 -110.30(14) . . . . ?
C34 C2 C1 B4 -149.19(13) . . . . ?
B7 C2 C1 B4 66.33(14) . . . . ?
B8 C2 C1 B4 -0.54(15) . . . . ?
B3 C2 C1 B4 -39.21(11) . . . . ?
B6 C2 C1 B4 105.19(13) . . . . ?
C34 C2 C1 B5 144.00(13) . . . . ?
B7 C2 C1 B5 -0.48(15) . . . . ?
B8 C2 C1 B5 -67.35(14) . . . . ?
B3 C2 C1 B5 -106.02(12) . . . . ?
B6 C2 C1 B5 38.38(11) . . . . ?
C34 C2 C1 B3 -109.98(14) . . . . ?
B7 C2 C1 B3 105.54(13) . . . . ?
B8 C2 C1 B3 38.67(11) . . . . ?
B6 C2 C1 B3 144.40(12) . . . . ?
C34 C2 C1 B6 105.63(14) . . . . ?
B7 C2 C1 B6 -38.85(11) . . . . ?
B8 C2 C1 B6 -105.73(13) . . . . ?
B3 C2 C1 B6 -144.40(12) . . . . ?
B4 C1 C18 C19 -149.54(14) . . . . ?
B5 C1 C18 C19 -74.20(19) . . . . ?
B3 C1 C18 C19 138.54(14) . . . . ?
B6 C1 C18 C19 -0.2(2) . . . . ?
C2 C1 C18 C19 70.00(18) . . . . ?
B4 C1 C18 C23 27.9(2) . . . . ?
B5 C1 C18 C23 103.27(16) . . . . ?
B3 C1 C18 C23 -43.98(18) . . . . ?
B6 C1 C18 C23 177.29(13) . . . . ?
C2 C1 C18 C23 -112.52(15) . . . . ?
C23 C18 C19 C20 -1.7(2) . . . . ?
C1 C18 C19 C20 175.81(13) . . . . ?
C18 C19 C20 C21 -0.6(2) . . . . ?
C18 C19 C20 C30 -178.85(14) . . . . ?
C19 C20 C21 C22 2.3(2) . . . . ?
C30 C20 C21 C22 -179.22(14) . . . . ?
C19 C20 C21 C24 -175.92(13) . . . . ?
C30 C20 C21 C24 2.60(17) . . . . ?
C20 C21 C22 C23 -1.6(2) . . . . ?
C24 C21 C22 C23 176.10(15) . . . . ?
C21 C22 C23 C18 -0.7(2) . . . . ?
C19 C18 C23 C22 2.3(2) . . . . ?
C1 C18 C23 C22 -175.20(14) . . . . ?
C22 C21 C24 C29 -0.6(3) . . . . ?
C20 C21 C24 C29 177.30(16) . . . . ?
C22 C21 C24 C25 -179.00(16) . . . . ?
C20 C21 C24 C25 -1.11(17) . . . . ?
C29 C24 C25 C26 0.5(2) . . . . ?
C21 C24 C25 C26 179.09(14) . . . . ?
C29 C24 C25 C30 -179.40(14) . . . . ?
C21 C24 C25 C30 -0.80(17) . . . . ?
C24 C25 C26 C27 -0.1(2) . . . . ?
C30 C25 C26 C27 179.79(15) . . . . ?
C25 C26 C27 C28 -0.6(2) . . . . ?
C26 C27 C28 C29 0.9(3) . . . . ?
C27 C28 C29 C24 -0.5(2) . . . . ?
C25 C24 C29 C28 -0.2(2) . . . . ?
C21 C24 C29 C28 -178.44(16) . . . . ?
C19 C20 C30 C25 175.51(15) . . . . ?
C21 C20 C30 C25 -2.89(16) . . . . ?
C19 C20 C30 C32 -66.1(2) . . . . ?
C21 C20 C30 C32 115.53(15) . . . . ?
C19 C20 C30 C31 56.8(2) . . . . ?
C21 C20 C30 C31 -121.61(15) . . . . ?
C26 C25 C30 C20 -177.70(15) . . . . ?
C24 C25 C30 C20 2.18(16) . . . . ?
C26 C25 C30 C32 64.4(2) . . . . ?
C24 C25 C30 C32 -115.71(15) . . . . ?
C26 C25 C30 C31 -59.5(2) . . . . ?
C24 C25 C30 C31 120.42(15) . . . . ?
B17 C13 C49 C39 153.27(13) . . . . ?
B16 C13 C49 C39 77.31(18) . . . . ?
B15 C13 C49 C39 2.6(2) . . . . ?
B18 C13 C49 C39 -134.90(14) . . . . ?
C14 C13 C49 C39 -67.26(17) . . . . ?
B17 C13 C49 C35 -27.1(2) . . . . ?
B16 C13 C49 C35 -103.07(16) . . . . ?
B15 C13 C49 C35 -177.74(12) . . . . ?
B18 C13 C49 C35 44.73(18) . . . . ?
C14 C13 C49 C35 112.37(14) . . . . ?
C39 C49 C35 C36 -1.1(2) . . . . ?
C13 C49 C35 C36 179.31(13) . . . . ?
C49 C35 C36 C37 1.1(2) . . . . ?
C49 C35 C36 C46 -178.33(14) . . . . ?
C35 C36 C37 C38 -0.5(2) . . . . ?
C46 C36 C37 C38 179.03(13) . . . . ?
C35 C36 C37 C40 179.88(13) . . . . ?
C46 C36 C37 C40 -0.61(16) . . . . ?
C36 C37 C38 C39 -0.1(2) . . . . ?
C40 C37 C38 C39 179.43(15) . . . . ?
C37 C38 C39 C49 0.1(2) . . . . ?
C35 C49 C39 C38 0.5(2) . . . . ?
C13 C49 C39 C38 -179.91(13) . . . . ?
C38 C37 C40 C45 0.8(3) . . . . ?
C36 C37 C40 C45 -179.59(15) . . . . ?
C38 C37 C40 C41 -178.83(15) . . . . ?
C36 C37 C40 C41 0.76(16) . . . . ?
C45 C40 C41 C42 -1.1(2) . . . . ?
C37 C40 C41 C42 178.56(14) . . . . ?
C45 C40 C41 C46 179.70(13) . . . . ?
C37 C40 C41 C46 -0.61(17) . . . . ?
C40 C41 C42 C43 0.5(2) . . . . ?
C46 C41 C42 C43 179.51(15) . . . . ?
C41 C42 C43 C44 0.5(2) . . . . ?
C42 C43 C44 C45 -0.9(2) . . . . ?
C43 C44 C45 C40 0.2(2) . . . . ?
C41 C40 C45 C44 0.8(2) . . . . ?
C37 C40 C45 C44 -178.85(15) . . . . ?
C42 C41 C46 C36 -178.84(15) . . . . ?
C40 C41 C46 C36 0.24(16) . . . . ?
C42 C41 C46 C48 -60.3(2) . . . . ?
C40 C41 C46 C48 118.79(14) . . . . ?
C42 C41 C46 C47 62.3(2) . . . . ?
C40 C41 C46 C47 -118.62(14) . . . . ?
C35 C36 C46 C41 179.69(15) . . . . ?
C37 C36 C46 C41 0.24(15) . . . . ?
C35 C36 C46 C48 61.7(2) . . . . ?
C37 C36 C46 C48 -117.73(14) . . . . ?
C35 C36 C46 C47 -61.8(2) . . . . ?
C37 C36 C46 C47 118.75(14) . . . . ?
C49 C13 C14 C50 5.72(18) . . . . ?
B17 C13 C14 C50 149.52(12) . . . . ?
B16 C13 C14 C50 -143.55(12) . . . . ?
B15 C13 C14 C50 -104.91(13) . . . . ?
B18 C13 C14 C50 110.68(13) . . . . ?
C49 C13 C14 B20 149.52(12) . . . . ?
B17 C13 C14 B20 -66.69(14) . . . . ?
B16 C13 C14 B20 0.24(15) . . . . ?
B15 C13 C14 B20 38.89(11) . . . . ?
B18 C13 C14 B20 -105.53(12) . . . . ?
C49 C13 C14 B19 -143.53(12) . . . . ?
B17 C13 C14 B19 0.26(15) . . . . ?
B16 C13 C14 B19 67.19(14) . . . . ?
B15 C13 C14 B19 105.84(12) . . . . ?
B18 C13 C14 B19 -38.58(11) . . . . ?
C49 C13 C14 B18 -104.95(13) . . . . ?
B17 C13 C14 B18 38.84(11) . . . . ?
B16 C13 C14 B18 105.77(12) . . . . ?
B15 C13 C14 B18 144.42(12) . . . . ?
C49 C13 C14 B15 110.63(14) . . . . ?
B17 C13 C14 B15 -105.57(12) . . . . ?
B16 C13 C14 B15 -38.64(11) . . . . ?
B18 C13 C14 B15 -144.42(12) . . . . ?
B20 C14 C50 C51 -28.0(2) . . . . ?
B19 C14 C50 C51 -105.06(16) . . . . ?
B18 C14 C50 C51 179.84(13) . . . . ?
B15 C14 C50 C51 43.85(18) . . . . ?
C13 C14 C50 C51 110.90(15) . . . . ?
B20 C14 C50 C55 156.90(13) . . . . ?
B19 C14 C50 C55 79.86(18) . . . . ?
B18 C14 C50 C55 4.8(2) . . . . ?
B15 C14 C50 C55 -131.24(14) . . . . ?
C13 C14 C50 C55 -64.18(17) . . . . ?
C55 C50 C51 C52 0.9(2) . . . . ?
C14 C50 C51 C52 -174.28(14) . . . . ?
C50 C51 C52 C53 1.1(2) . . . . ?
C51 C52 C53 C54 -1.8(2) . . . . ?
C51 C52 C53 C56 174.29(15) . . . . ?
C52 C53 C54 C55 0.5(2) . . . . ?
C56 C53 C54 C55 -176.41(13) . . . . ?
C52 C53 C54 C62 176.58(13) . . . . ?
C56 C53 C54 C62 -0.37(16) . . . . ?
C53 C54 C55 C50 1.5(2) . . . . ?
C62 C54 C55 C50 -173.84(14) . . . . ?
C51 C50 C55 C54 -2.2(2) . . . . ?
C14 C50 C55 C54 172.91(13) . . . . ?
C52 C53 C56 C61 1.4(3) . . . . ?
C54 C53 C56 C61 177.84(15) . . . . ?
C52 C53 C56 C57 -174.81(15) . . . . ?
C54 C53 C56 C57 1.67(16) . . . . ?
C61 C56 C57 C58 -0.7(2) . . . . ?
C53 C56 C57 C58 175.91(14) . . . . ?
C61 C56 C57 C62 -178.95(13) . . . . ?
C53 C56 C57 C62 -2.32(16) . . . . ?
C56 C57 C58 C59 0.3(2) . . . . ?
C62 C57 C58 C59 178.17(15) . . . . ?
C57 C58 C59 C60 0.2(2) . . . . ?
C58 C59 C60 C61 -0.2(3) . . . . ?
C59 C60 C61 C56 -0.2(2) . . . . ?
C57 C56 C61 C60 0.7(2) . . . . ?
C53 C56 C61 C60 -175.09(15) . . . . ?
C55 C54 C62 C57 174.77(14) . . . . ?
C53 C54 C62 C57 -0.93(15) . . . . ?
C55 C54 C62 C64 -66.10(19) . . . . ?
C53 C54 C62 C64 118.19(14) . . . . ?
C55 C54 C62 C63 56.93(19) . . . . ?
C53 C54 C62 C63 -118.78(13) . . . . ?
C58 C57 C62 C54 -176.05(15) . . . . ?
C56 C57 C62 C54 1.99(15) . . . . ?
C58 C57 C62 C64 64.8(2) . . . . ?
C56 C57 C62 C64 -117.17(14) . . . . ?
C58 C57 C62 C63 -59.0(2) . . . . ?
C56 C57 C62 C63 119.04(14) . . . . ?
C50 C14 B18 C13 -105.17(13) . . . . ?
B20 C14 B18 C13 100.23(12) . . . . ?
B19 C14 B18 C13 138.41(12) . . . . ?
B15 C14 B18 C13 32.51(11) . . . . ?
C50 C14 B18 B23 155.34(12) . . . . ?
B20 C14 B18 B23 0.74(15) . . . . ?
B19 C14 B18 B23 38.91(11) . . . . ?
B15 C14 B18 B23 -66.99(14) . . . . ?
C13 C14 B18 B23 -99.50(12) . . . . ?
C50 C14 B18 B19 116.42(14) . . . . ?
B20 C14 B18 B19 -38.18(11) . . . . ?
B15 C14 B18 B19 -105.90(12) . . . . ?
C13 C14 B18 B19 -138.41(12) . . . . ?
C50 C14 B18 B17 -141.51(13) . . . . ?
B20 C14 B18 B17 63.89(14) . . . . ?
B19 C14 B18 B17 102.07(12) . . . . ?
B15 C14 B18 B17 -3.84(15) . . . . ?
C13 C14 B18 B17 -36.34(10) . . . . ?
C49 C13 B18 C14 108.65(13) . . . . ?
B17 C13 B18 C14 -138.13(12) . . . . ?
B16 C13 B18 C14 -100.07(12) . . . . ?
B15 C13 B18 C14 -32.69(11) . . . . ?
C49 C13 B18 B23 -151.58(12) . . . . ?
B17 C13 B18 B23 -38.37(11) . . . . ?
B16 C13 B18 B23 -0.30(15) . . . . ?
B15 C13 B18 B23 67.07(13) . . . . ?
C14 C13 B18 B23 99.77(12) . . . . ?
C49 C13 B18 B19 145.12(12) . . . . ?
B17 C13 B18 B19 -101.67(12) . . . . ?
B16 C13 B18 B19 -63.60(14) . . . . ?
B15 C13 B18 B19 3.77(15) . . . . ?
C14 C13 B18 B19 36.47(10) . . . . ?
C49 C13 B18 B17 -113.22(13) . . . . ?
B16 C13 B18 B17 38.06(11) . . . . ?
B15 C13 B18 B17 105.44(12) . . . . ?
C14 C13 B18 B17 138.13(12) . . . . ?
C50 C14 B19 B18 -108.37(15) . . . . ?
B20 C14 B19 B18 140.03(12) . . . . ?
B15 C14 B19 B18 102.21(12) . . . . ?
C13 C14 B19 B18 37.65(10) . . . . ?
C50 C14 B19 B20 111.60(15) . . . . ?
B18 C14 B19 B20 -140.03(12) . . . . ?
B15 C14 B19 B20 -37.83(11) . . . . ?
C13 C14 B19 B20 -102.38(12) . . . . ?
C50 C14 B19 B23 -146.84(13) . . . . ?
B20 C14 B19 B23 101.57(12) . . . . ?
B18 C14 B19 B23 -38.46(11) . . . . ?
B15 C14 B19 B23 63.74(14) . . . . ?
C13 C14 B19 B23 -0.81(15) . . . . ?
C50 C14 B19 B24 150.27(13) . . . . ?
B20 C14 B19 B24 38.68(11) . . . . ?
B18 C14 B19 B24 -101.36(12) . . . . ?
B15 C14 B19 B24 0.85(15) . . . . ?
C13 C14 B19 B24 -63.71(13) . . . . ?
C13 B18 B19 C14 -37.22(10) . . . . ?
B23 B18 B19 C14 -136.03(12) . . . . ?
B17 B18 B19 C14 -98.73(12) . . . . ?
C14 B18 B19 B20 34.91(10) . . . . ?
C13 B18 B19 B20 -2.31(15) . . . . ?
B23 B18 B19 B20 -101.12(13) . . . . ?
B17 B18 B19 B20 -63.82(14) . . . . ?
C14 B18 B19 B23 136.03(12) . . . . ?
C13 B18 B19 B23 98.81(12) . . . . ?
B17 B18 B19 B23 37.30(11) . . . . ?
C14 B18 B19 B24 98.04(12) . . . . ?
C13 B18 B19 B24 60.82(14) . . . . ?
B23 B18 B19 B24 -37.99(11) . . . . ?
B17 B18 B19 B24 -0.69(15) . . . . ?
C14 B18 B23 B19 -38.13(10) . . . . ?
C13 B18 B23 B19 -101.25(12) . . . . ?
B17 B18 B23 B19 -138.65(12) . . . . ?
C14 B18 B23 B17 100.52(12) . . . . ?
C13 B18 B23 B17 37.40(10) . . . . ?
B19 B18 B23 B17 138.65(12) . . . . ?
C14 B18 B23 B24 -0.24(15) . . . . ?
C13 B18 B23 B24 -63.36(14) . . . . ?
B19 B18 B23 B24 37.89(11) . . . . ?
B17 B18 B23 B24 -100.76(13) . . . . ?
C14 B18 B23 B22 62.86(14) . . . . ?
C13 B18 B23 B22 -0.26(15) . . . . ?
B19 B18 B23 B22 100.99(12) . . . . ?
B17 B18 B23 B22 -37.66(11) . . . . ?
C14 B19 B23 B18 38.30(11) . . . . ?
B20 B19 B23 B18 99.60(12) . . . . ?
B24 B19 B23 B18 137.47(12) . . . . ?
C14 B19 B23 B17 1.06(15) . . . . ?
B18 B19 B23 B17 -37.24(11) . . . . ?
B20 B19 B23 B17 62.36(15) . . . . ?
B24 B19 B23 B17 100.23(13) . . . . ?
C14 B19 B23 B24 -99.18(12) . . . . ?
B18 B19 B23 B24 -137.47(12) . . . . ?
B20 B19 B23 B24 -37.88(11) . . . . ?
C14 B19 B23 B22 -62.26(14) . . . . ?
B18 B19 B23 B22 -100.56(13) . . . . ?
B20 B19 B23 B22 -0.96(15) . . . . ?
B24 B19 B23 B22 36.92(11) . . . . ?
C49 C13 B17 B22 -153.97(13) . . . . ?
B16 C13 B17 B22 -39.04(11) . . . . ?
B15 C13 B17 B22 -1.32(15) . . . . ?
B18 C13 B17 B22 101.23(12) . . . . ?
C14 C13 B17 B22 63.58(14) . . . . ?
C49 C13 B17 B18 104.80(14) . . . . ?
B16 C13 B17 B18 -140.27(12) . . . . ?
B15 C13 B17 B18 -102.55(12) . . . . ?
C14 C13 B17 B18 -37.65(10) . . . . ?
C49 C13 B17 B23 142.86(13) . . . . ?
B16 C13 B17 B23 -102.21(12) . . . . ?
B15 C13 B17 B23 -64.49(14) . . . . ?
B18 C13 B17 B23 38.06(11) . . . . ?
C14 C13 B17 B23 0.41(15) . . . . ?
C49 C13 B17 B16 -114.92(14) . . . . ?
B15 C13 B17 B16 37.73(11) . . . . ?
B18 C13 B17 B16 140.27(12) . . . . ?
C14 C13 B17 B16 102.62(12) . . . . ?
C14 B18 B17 C13 37.33(10) . . . . ?
B23 B18 B17 C13 136.59(12) . . . . ?
B19 B18 B17 C13 99.26(12) . . . . ?
C14 B18 B17 B22 -61.38(14) . . . . ?
C13 B18 B17 B22 -98.71(12) . . . . ?
B23 B18 B17 B22 37.88(11) . . . . ?
B19 B18 B17 B22 0.55(15) . . . . ?
C14 B18 B17 B23 -99.27(12) . . . . ?
C13 B18 B17 B23 -136.59(12) . . . . ?
B19 B18 B17 B23 -37.33(11) . . . . ?
C14 B18 B17 B16 2.18(15) . . . . ?
C13 B18 B17 B16 -35.14(11) . . . . ?
B23 B18 B17 B16 101.45(13) . . . . ?
B19 B18 B17 B16 64.12(14) . . . . ?
B18 B23 B17 C13 -38.07(11) . . . . ?
B19 B23 B17 C13 -0.91(15) . . . . ?
B24 B23 B17 C13 62.54(14) . . . . ?
B22 B23 B17 C13 99.61(12) . . . . ?
B18 B23 B17 B22 -137.68(12) . . . . ?
B19 B23 B17 B22 -100.52(13) . . . . ?
B24 B23 B17 B22 -37.07(11) . . . . ?
B19 B23 B17 B18 37.16(11) . . . . ?
B24 B23 B17 B18 100.61(12) . . . . ?
B22 B23 B17 B18 137.68(12) . . . . ?
B18 B23 B17 B16 -100.19(12) . . . . ?
B19 B23 B17 B16 -63.03(15) . . . . ?
B24 B23 B17 B16 0.42(15) . . . . ?
B22 B23 B17 B16 37.49(11) . . . . ?
C13 B17 B22 B24 -62.61(14) . . . . ?
B18 B17 B22 B24 -0.19(15) . . . . ?
B23 B17 B22 B24 37.27(11) . . . . ?
B16 B17 B22 B24 -101.08(13) . . . . ?
C13 B17 B22 B21 0.87(15) . . . . ?
B18 B17 B22 B21 63.29(14) . . . . ?
B23 B17 B22 B21 100.74(13) . . . . ?
B16 B17 B22 B21 -37.60(11) . . . . ?
C13 B17 B22 B16 38.47(11) . . . . ?
B18 B17 B22 B16 100.89(12) . . . . ?
B23 B17 B22 B16 138.35(12) . . . . ?
C13 B17 B22 B23 -99.88(12) . . . . ?
B18 B17 B22 B23 -37.46(11) . . . . ?
B16 B17 B22 B23 -138.35(12) . . . . ?
B18 B23 B22 B17 37.88(11) . . . . ?
B19 B23 B22 B17 101.38(12) . . . . ?
B24 B23 B22 B17 138.38(12) . . . . ?
B18 B23 B22 B24 -100.50(12) . . . . ?
B19 B23 B22 B24 -36.99(11) . . . . ?
B17 B23 B22 B24 -138.38(12) . . . . ?
B18 B23 B22 B21 -62.40(14) . . . . ?
B19 B23 B22 B21 1.10(16) . . . . ?
B17 B23 B22 B21 -100.28(13) . . . . ?
B24 B23 B22 B21 38.10(11) . . . . ?
B18 B23 B22 B16 0.70(15) . . . . ?
B19 B23 B22 B16 64.21(15) . . . . ?
B17 B23 B22 B16 -37.18(11) . . . . ?
B24 B23 B22 B16 101.20(13) . . . . ?
C50 C14 B20 B19 -115.93(15) . . . . ?
B18 C14 B20 B19 37.99(11) . . . . ?
B15 C14 B20 B19 140.45(12) . . . . ?
C13 C14 B20 B19 102.73(11) . . . . ?
C50 C14 B20 B21 142.04(13) . . . . ?
B19 C14 B20 B21 -102.03(12) . . . . ?
B18 C14 B20 B21 -64.04(14) . . . . ?
B15 C14 B20 B21 38.42(11) . . . . ?
C13 C14 B20 B21 0.70(14) . . . . ?
C50 C14 B20 B24 -154.84(13) . . . . ?
B19 C14 B20 B24 -38.91(11) . . . . ?
B18 C14 B20 B24 -0.92(15) . . . . ?
B15 C14 B20 B24 101.54(12) . . . . ?
C13 C14 B20 B24 63.82(13) . . . . ?
C50 C14 B20 B15 103.62(14) . . . . ?
B19 C14 B20 B15 -140.45(12) . . . . ?
B18 C14 B20 B15 -102.46(12) . . . . ?
C13 C14 B20 B15 -37.72(10) . . . . ?
B18 B19 B20 C14 -35.23(10) . . . . ?
B23 B19 B20 C14 -97.95(12) . . . . ?
B24 B19 B20 C14 -135.96(12) . . . . ?
C14 B19 B20 B21 98.39(12) . . . . ?
B18 B19 B20 B21 63.16(14) . . . . ?
B23 B19 B20 B21 0.45(15) . . . . ?
B24 B19 B20 B21 -37.57(11) . . . . ?
C14 B19 B20 B24 135.96(12) . . . . ?
B18 B19 B20 B24 100.73(12) . . . . ?
B23 B19 B20 B24 38.01(11) . . . . ?
C14 B19 B20 B15 35.34(11) . . . . ?
B18 B19 B20 B15 0.11(15) . . . . ?
B23 B19 B20 B15 -62.60(14) . . . . ?
B24 B19 B20 B15 -100.62(13) . . . . ?
C49 C13 B15 C14 -106.86(14) . . . . ?
B17 C13 B15 C14 100.23(12) . . . . ?
B16 C13 B15 C14 138.22(12) . . . . ?
B18 C13 B15 C14 32.50(11) . . . . ?
C49 C13 B15 B21 154.13(12) . . . . ?
B17 C13 B15 B21 1.22(15) . . . . ?
B16 C13 B15 B21 39.21(11) . . . . ?
B18 C13 B15 B21 -66.51(14) . . . . ?
C14 C13 B15 B21 -99.01(12) . . . . ?
C49 C13 B15 B16 114.92(14) . . . . ?
B17 C13 B15 B16 -37.99(12) . . . . ?
B18 C13 B15 B16 -105.72(12) . . . . ?
C14 C13 B15 B16 -138.22(12) . . . . ?
C49 C13 B15 B20 -143.02(13) . . . . ?
B17 C13 B15 B20 64.07(14) . . . . ?
B16 C13 B15 B20 102.05(12) . . . . ?
B18 C13 B15 B20 -3.67(15) . . . . ?
C14 C13 B15 B20 -36.16(10) . . . . ?
C50 C14 B15 C13 107.20(13) . . . . ?
B20 C14 B15 C13 -138.10(11) . . . . ?
B19 C14 B15 C13 -100.19(12) . . . . ?
B18 C14 B15 C13 -32.62(11) . . . . ?
C50 C14 B15 B21 -153.17(12) . . . . ?
B20 C14 B15 B21 -38.48(11) . . . . ?
B19 C14 B15 B21 -0.56(15) . . . . ?
B18 C14 B15 B21 67.01(14) . . . . ?
C13 C14 B15 B21 99.63(12) . . . . ?
C50 C14 B15 B16 143.78(12) . . . . ?
B20 C14 B15 B16 -101.52(12) . . . . ?
B19 C14 B15 B16 -63.61(14) . . . . ?
B18 C14 B15 B16 3.96(15) . . . . ?
C13 C14 B15 B16 36.58(10) . . . . ?
C50 C14 B15 B20 -114.69(13) . . . . ?
B19 C14 B15 B20 37.92(11) . . . . ?
B18 C14 B15 B20 105.49(12) . . . . ?
C13 C14 B15 B20 138.10(11) . . . . ?
C14 B20 B15 C13 37.16(10) . . . . ?
B19 B20 B15 C13 2.12(15) . . . . ?
B21 B20 B15 C13 -99.07(12) . . . . ?
B24 B20 B15 C13 -61.52(14) . . . . ?
B19 B20 B15 C14 -35.04(10) . . . . ?
B21 B20 B15 C14 -136.23(12) . . . . ?
B24 B20 B15 C14 -98.68(12) . . . . ?
C14 B20 B15 B21 136.23(12) . . . . ?
B19 B20 B15 B21 101.19(13) . . . . ?
B24 B20 B15 B21 37.56(11) . . . . ?
C14 B20 B15 B16 99.01(12) . . . . ?
B19 B20 B15 B16 63.96(14) . . . . ?
B21 B20 B15 B16 -37.22(11) . . . . ?
B24 B20 B15 B16 0.33(15) . . . . ?
C49 C13 B16 B15 -109.18(15) . . . . ?
B17 C13 B16 B15 140.24(12) . . . . ?
B18 C13 B16 B15 102.28(12) . . . . ?
C14 C13 B16 B15 37.85(10) . . . . ?
C49 C13 B16 B21 -148.11(13) . . . . ?
B17 C13 B16 B21 101.31(12) . . . . ?
B15 C13 B16 B21 -38.93(11) . . . . ?
B18 C13 B16 B21 63.35(14) . . . . ?
C14 C13 B16 B21 -1.07(15) . . . . ?
C49 C13 B16 B17 110.58(15) . . . . ?
B15 C13 B16 B17 -140.24(12) . . . . ?
B18 C13 B16 B17 -37.96(11) . . . . ?
C14 C13 B16 B17 -102.38(12) . . . . ?
C49 C13 B16 B22 149.28(13) . . . . ?
B17 C13 B16 B22 38.69(11) . . . . ?
B15 C13 B16 B22 -101.54(12) . . . . ?
B18 C13 B16 B22 0.73(15) . . . . ?
C14 C13 B16 B22 -63.69(13) . . . . ?
C14 B15 B16 C13 -37.22(10) . . . . ?
B21 B15 B16 C13 -135.53(12) . . . . ?
B20 B15 B16 C13 -98.38(12) . . . . ?
C13 B15 B16 B21 135.53(12) . . . . ?
C14 B15 B16 B21 98.31(12) . . . . ?
B20 B15 B16 B21 37.16(11) . . . . ?
C13 B15 B16 B17 34.76(11) . . . . ?
C14 B15 B16 B17 -2.46(15) . . . . ?
B21 B15 B16 B17 -100.77(13) . . . . ?
B20 B15 B16 B17 -63.61(14) . . . . ?
C13 B15 B16 B22 97.79(12) . . . . ?
C14 B15 B16 B22 60.57(14) . . . . ?
B21 B15 B16 B22 -37.74(11) . . . . ?
B20 B15 B16 B22 -0.58(15) . . . . ?
B22 B17 B16 C13 135.81(12) . . . . ?
B18 B17 B16 C13 35.33(11) . . . . ?
B23 B17 B16 C13 98.25(12) . . . . ?
C13 B17 B16 B15 -35.16(11) . . . . ?
B22 B17 B16 B15 100.65(13) . . . . ?
B18 B17 B16 B15 0.18(15) . . . . ?
B23 B17 B16 B15 63.09(14) . . . . ?
C13 B17 B16 B21 -98.02(12) . . . . ?
B22 B17 B16 B21 37.79(11) . . . . ?
B18 B17 B16 B21 -62.68(14) . . . . ?
B23 B17 B16 B21 0.23(15) . . . . ?
C13 B17 B16 B22 -135.81(12) . . . . ?
B18 B17 B16 B22 -100.47(12) . . . . ?
B23 B17 B16 B22 -37.56(11) . . . . ?
B17 B22 B16 C13 -38.00(10) . . . . ?
B24 B22 B16 C13 62.70(14) . . . . ?
B21 B22 B16 C13 99.65(12) . . . . ?
B23 B22 B16 C13 -0.86(15) . . . . ?
B17 B22 B16 B15 -100.08(12) . . . . ?
B24 B22 B16 B15 0.62(16) . . . . ?
B21 B22 B16 B15 37.56(11) . . . . ?
B23 B22 B16 B15 -62.95(14) . . . . ?
B17 B22 B16 B21 -137.65(12) . . . . ?
B24 B22 B16 B21 -36.94(11) . . . . ?
B23 B22 B16 B21 -100.51(13) . . . . ?
B24 B22 B16 B17 100.70(13) . . . . ?
B21 B22 B16 B17 137.65(12) . . . . ?
B23 B22 B16 B17 37.14(11) . . . . ?
C14 B20 B24 B19 38.34(11) . . . . ?
B21 B20 B24 B19 138.27(12) . . . . ?
B15 B20 B24 B19 101.06(12) . . . . ?
C14 B20 B24 B22 -62.67(14) . . . . ?
B19 B20 B24 B22 -101.01(13) . . . . ?
B21 B20 B24 B22 37.26(11) . . . . ?
B15 B20 B24 B22 0.05(15) . . . . ?
C14 B20 B24 B21 -99.93(12) . . . . ?
B19 B20 B24 B21 -138.27(12) . . . . ?
B15 B20 B24 B21 -37.21(11) . . . . ?
C14 B20 B24 B23 0.72(15) . . . . ?
B19 B20 B24 B23 -37.63(11) . . . . ?
B21 B20 B24 B23 100.64(13) . . . . ?
B15 B20 B24 B23 63.44(14) . . . . ?
C14 B19 B24 B20 -37.94(10) . . . . ?
B18 B19 B24 B20 -99.92(12) . . . . ?
B23 B19 B24 B20 -137.57(12) . . . . ?
C14 B19 B24 B22 62.55(14) . . . . ?
B18 B19 B24 B22 0.57(15) . . . . ?
B20 B19 B24 B22 100.49(13) . . . . ?
B23 B19 B24 B22 -37.08(11) . . . . ?
C14 B19 B24 B21 -0.79(15) . . . . ?
B18 B19 B24 B21 -62.77(14) . . . . ?
B20 B19 B24 B21 37.15(11) . . . . ?
B23 B19 B24 B21 -100.41(13) . . . . ?
C14 B19 B24 B23 99.63(12) . . . . ?
B18 B19 B24 B23 37.65(11) . . . . ?
B20 B19 B24 B23 137.57(12) . . . . ?
B17 B22 B24 B20 62.99(15) . . . . ?
B21 B22 B24 B20 -37.20(11) . . . . ?
B16 B22 B24 B20 -0.41(16) . . . . ?
B23 B22 B24 B20 100.14(13) . . . . ?
B17 B22 B24 B19 -0.24(16) . . . . ?
B21 B22 B24 B19 -100.42(13) . . . . ?
B16 B22 B24 B19 -63.64(15) . . . . ?
B23 B22 B24 B19 36.92(11) . . . . ?
B17 B22 B24 B21 100.19(13) . . . . ?
B16 B22 B24 B21 36.78(11) . . . . ?
B23 B22 B24 B21 137.34(12) . . . . ?
B17 B22 B24 B23 -37.15(11) . . . . ?
B21 B22 B24 B23 -137.34(12) . . . . ?
B16 B22 B24 B23 -100.55(13) . . . . ?
B18 B23 B24 B20 -0.29(16) . . . . ?
B19 B23 B24 B20 37.66(11) . . . . ?
B17 B23 B24 B20 -63.91(14) . . . . ?
B22 B23 B24 B20 -100.97(13) . . . . ?
B18 B23 B24 B19 -37.95(11) . . . . ?
B17 B23 B24 B19 -101.57(12) . . . . ?
B22 B23 B24 B19 -138.63(12) . . . . ?
B18 B23 B24 B22 100.68(13) . . . . ?
B19 B23 B24 B22 138.63(12) . . . . ?
B17 B23 B24 B22 37.06(11) . . . . ?
B18 B23 B24 B21 62.71(14) . . . . ?
B19 B23 B24 B21 100.66(13) . . . . ?
B17 B23 B24 B21 -0.91(15) . . . . ?
B22 B23 B24 B21 -37.97(11) . . . . ?
C13 B15 B21 B20 100.19(12) . . . . ?
C14 B15 B21 B20 37.46(10) . . . . ?
B16 B15 B21 B20 138.67(12) . . . . ?
C13 B15 B21 B16 -38.48(11) . . . . ?
C14 B15 B21 B16 -101.21(12) . . . . ?
B20 B15 B21 B16 -138.67(12) . . . . ?
C13 B15 B21 B22 -0.61(15) . . . . ?
C14 B15 B21 B22 -63.34(14) . . . . ?
B16 B15 B21 B22 37.87(11) . . . . ?
B20 B15 B21 B22 -100.80(13) . . . . ?
C13 B15 B21 B24 62.76(14) . . . . ?
C14 B15 B21 B24 0.03(15) . . . . ?
B16 B15 B21 B24 101.24(13) . . . . ?
B20 B15 B21 B24 -37.43(11) . . . . ?
C14 B20 B21 B15 -38.50(11) . . . . ?
B19 B20 B21 B15 -100.59(12) . . . . ?
B24 B20 B21 B15 -138.10(12) . . . . ?
C14 B20 B21 B16 -1.36(15) . . . . ?
B19 B20 B21 B16 -63.45(15) . . . . ?
B24 B20 B21 B16 -100.96(13) . . . . ?
B15 B20 B21 B16 37.14(11) . . . . ?
C14 B20 B21 B22 62.33(14) . . . . ?
B19 B20 B21 B22 0.24(16) . . . . ?
B24 B20 B21 B22 -37.27(11) . . . . ?
B15 B20 B21 B22 100.83(13) . . . . ?
C14 B20 B21 B24 99.60(12) . . . . ?
B19 B20 B21 B24 37.51(11) . . . . ?
B15 B20 B21 B24 138.10(12) . . . . ?
C13 B16 B21 B15 38.76(11) . . . . ?
B17 B16 B21 B15 99.97(12) . . . . ?
B22 B16 B21 B15 137.66(12) . . . . ?
C13 B16 B21 B20 1.50(15) . . . . ?
B15 B16 B21 B20 -37.26(11) . . . . ?
B17 B16 B21 B20 62.71(15) . . . . ?
B22 B16 B21 B20 100.40(13) . . . . ?
C13 B16 B21 B22 -98.90(12) . . . . ?
B15 B16 B21 B22 -137.66(12) . . . . ?
B17 B16 B21 B22 -37.69(11) . . . . ?
C13 B16 B21 B24 -62.01(14) . . . . ?
B15 B16 B21 B24 -100.77(13) . . . . ?
B17 B16 B21 B24 -0.80(15) . . . . ?
B22 B16 B21 B24 36.89(11) . . . . ?
B17 B22 B21 B15 -0.16(16) . . . . ?
B24 B22 B21 B15 101.01(13) . . . . ?
B16 B22 B21 B15 -37.83(11) . . . . ?
B23 B22 B21 B15 62.93(15) . . . . ?
B17 B22 B21 B20 -63.92(15) . . . . ?
B24 B22 B21 B20 37.25(11) . . . . ?
B16 B22 B21 B20 -101.59(13) . . . . ?
B23 B22 B21 B20 -0.83(16) . . . . ?
B17 B22 B21 B16 37.67(11) . . . . ?
B24 B22 B21 B16 138.84(12) . . . . ?
B23 B22 B21 B16 100.76(13) . . . . ?
B17 B22 B21 B24 -101.17(13) . . . . ?
B16 B22 B21 B24 -138.84(12) . . . . ?
B23 B22 B21 B24 -38.08(11) . . . . ?
B20 B24 B21 B15 37.64(11) . . . . ?
B19 B24 B21 B15 0.48(15) . . . . ?
B22 B24 B21 B15 -100.60(13) . . . . ?
B23 B24 B21 B15 -62.55(14) . . . . ?
B19 B24 B21 B20 -37.16(11) . . . . ?
B22 B24 B21 B20 -138.24(12) . . . . ?
B23 B24 B21 B20 -100.19(12) . . . . ?
B20 B24 B21 B16 101.25(13) . . . . ?
B19 B24 B21 B16 64.08(14) . . . . ?
B22 B24 B21 B16 -36.99(11) . . . . ?
B23 B24 B21 B16 1.06(16) . . . . ?
B20 B24 B21 B22 138.24(12) . . . . ?
B19 B24 B21 B22 101.08(12) . . . . ?
B23 B24 B21 B22 38.05(11) . . . . ?
C18 C1 B4 B9 -143.96(13) . . . . ?
B5 C1 B4 B9 102.07(13) . . . . ?
B3 C1 B4 B9 -38.50(11) . . . . ?
B6 C1 B4 B9 64.49(14) . . . . ?
C2 C1 B4 B9 -0.30(15) . . . . ?
C18 C1 B4 B10 152.79(13) . . . . ?
B5 C1 B4 B10 38.82(11) . . . . ?
B3 C1 B4 B10 -101.75(13) . . . . ?
B6 C1 B4 B10 1.24(16) . . . . ?
C2 C1 B4 B10 -63.54(14) . . . . ?
C18 C1 B4 B3 -105.46(14) . . . . ?
B5 C1 B4 B3 140.57(12) . . . . ?
B6 C1 B4 B3 102.99(13) . . . . ?
C2 C1 B4 B3 38.20(11) . . . . ?
C18 C1 B4 B5 113.97(14) . . . . ?
B3 C1 B4 B5 -140.57(12) . . . . ?
B6 C1 B4 B5 -37.58(12) . . . . ?
C2 C1 B4 B5 -102.37(12) . . . . ?
C18 C1 B5 B6 109.37(15) . . . . ?
B4 C1 B5 B6 -140.18(12) . . . . ?
B3 C1 B5 B6 -102.49(13) . . . . ?
C2 C1 B5 B6 -37.67(11) . . . . ?
C18 C1 B5 B4 -110.46(15) . . . . ?
B3 C1 B5 B4 37.68(12) . . . . ?
B6 C1 B5 B4 140.18(12) . . . . ?
C2 C1 B5 B4 102.50(12) . . . . ?
C18 C1 B5 B11 148.11(13) . . . . ?
B4 C1 B5 B11 -101.43(13) . . . . ?
B3 C1 B5 B11 -63.75(14) . . . . ?
B6 C1 B5 B11 38.75(11) . . . . ?
C2 C1 B5 B11 1.07(15) . . . . ?
C18 C1 B5 B10 -149.04(13) . . . . ?
B4 C1 B5 B10 -38.58(11) . . . . ?
B3 C1 B5 B10 -0.90(15) . . . . ?
B6 C1 B5 B10 101.59(13) . . . . ?
C2 C1 B5 B10 63.92(14) . . . . ?
B9 B4 B5 C1 -97.97(12) . . . . ?
B10 B4 B5 C1 -136.02(12) . . . . ?
B3 B4 B5 C1 -34.98(11) . . . . ?
C1 B4 B5 B6 35.33(11) . . . . ?
B9 B4 B5 B6 -62.64(15) . . . . ?
B10 B4 B5 B6 -100.70(13) . . . . ?
B3 B4 B5 B6 0.35(16) . . . . ?
C1 B4 B5 B11 98.36(12) . . . . ?
B9 B4 B5 B11 0.39(16) . . . . ?
B10 B4 B5 B11 -37.66(12) . . . . ?
B3 B4 B5 B11 63.38(15) . . . . ?
C1 B4 B5 B10 136.02(12) . . . . ?
B9 B4 B5 B10 38.05(11) . . . . ?
B3 B4 B5 B10 101.05(13) . . . . ?
C18 C1 B3 C2 -109.57(13) . . . . ?
B4 C1 B3 C2 137.72(12) . . . . ?
B5 C1 B3 C2 99.95(12) . . . . ?
B6 C1 B3 C2 32.76(11) . . . . ?
C18 C1 B3 B9 151.35(12) . . . . ?
B4 C1 B3 B9 38.64(11) . . . . ?
B5 C1 B3 B9 0.87(15) . . . . ?
B6 C1 B3 B9 -66.32(14) . . . . ?
C2 C1 B3 B9 -99.08(12) . . . . ?
C18 C1 B3 B8 -146.01(13) . . . . ?
B4 C1 B3 B8 101.27(13) . . . . ?
B5 C1 B3 B8 63.51(14) . . . . ?
B6 C1 B3 B8 -3.69(15) . . . . ?
C2 C1 B3 B8 -36.45(10) . . . . ?
C18 C1 B3 B4 112.71(14) . . . . ?
B5 C1 B3 B4 -37.77(12) . . . . ?
B6 C1 B3 B4 -104.96(13) . . . . ?
C2 C1 B3 B4 -137.72(12) . . . . ?
C34 C2 B3 C1 108.59(14) . . . . ?
B7 C2 B3 C1 -100.19(12) . . . . ?
B8 C2 B3 C1 -138.25(12) . . . . ?
B6 C2 B3 C1 -32.60(11) . . . . ?
C34 C2 B3 B9 -151.96(13) . . . . ?
B7 C2 B3 B9 -0.74(15) . . . . ?
B8 C2 B3 B9 -38.79(11) . . . . ?
C1 C2 B3 B9 99.45(12) . . . . ?
B6 C2 B3 B9 66.85(14) . . . . ?
C34 C2 B3 B8 -113.17(14) . . . . ?
B7 C2 B3 B8 38.06(12) . . . . ?
C1 C2 B3 B8 138.25(12) . . . . ?
B6 C2 B3 B8 105.65(13) . . . . ?
C34 C2 B3 B4 145.32(13) . . . . ?
B7 C2 B3 B4 -63.46(15) . . . . ?
B8 C2 B3 B4 -101.52(13) . . . . ?
C1 C2 B3 B4 36.73(11) . . . . ?
B6 C2 B3 B4 4.13(16) . . . . ?
B9 B4 B3 C1 136.05(12) . . . . ?
B10 B4 B3 C1 98.37(13) . . . . ?
B5 B4 B3 C1 34.81(11) . . . . ?
C1 B4 B3 C2 -37.49(11) . . . . ?
B9 B4 B3 C2 98.56(12) . . . . ?
B10 B4 B3 C2 60.88(15) . . . . ?
B5 B4 B3 C2 -2.68(16) . . . . ?
C1 B4 B3 B9 -136.05(12) . . . . ?
B10 B4 B3 B9 -37.68(11) . . . . ?
B5 B4 B3 B9 -101.24(13) . . . . ?
C1 B4 B3 B8 -99.13(12) . . . . ?
B9 B4 B3 B8 36.92(11) . . . . ?
B10 B4 B3 B8 -0.76(15) . . . . ?
B5 B4 B3 B8 -64.33(15) . . . . ?
C34 C2 B8 B9 148.67(13) . . . . ?
B7 C2 B8 B9 -101.33(13) . . . . ?
B3 C2 B8 B9 38.83(11) . . . . ?
C1 C2 B8 B9 1.14(15) . . . . ?
B6 C2 B8 B9 -63.50(15) . . . . ?
C34 C2 B8 B7 -110.01(15) . . . . ?
B3 C2 B8 B7 140.16(12) . . . . ?
C1 C2 B8 B7 102.47(12) . . . . ?
B6 C2 B8 B7 37.83(12) . . . . ?
C34 C2 B8 B3 109.83(15) . . . . ?
B7 C2 B8 B3 -140.16(12) . . . . ?
C1 C2 B8 B3 -37.69(11) . . . . ?
B6 C2 B8 B3 -102.33(12) . . . . ?
C34 C2 B8 B12 -148.32(13) . . . . ?
B7 C2 B8 B12 -38.31(11) . . . . ?
B3 C2 B8 B12 101.85(13) . . . . ?
C1 C2 B8 B12 64.16(14) . . . . ?
B6 C2 B8 B12 -0.48(16) . . . . ?
C1 B3 B8 C2 37.13(10) . . . . ?
B9 B3 B8 C2 135.71(12) . . . . ?
B4 B3 B8 C2 98.71(12) . . . . ?
C1 B3 B8 B9 -98.57(12) . . . . ?
C2 B3 B8 B9 -135.71(12) . . . . ?
B4 B3 B8 B9 -37.00(11) . . . . ?
C1 B3 B8 B7 2.27(15) . . . . ?
C2 B3 B8 B7 -34.87(11) . . . . ?
B9 B3 B8 B7 100.84(13) . . . . ?
B4 B3 B8 B7 63.84(15) . . . . ?
C1 B3 B8 B12 -60.79(14) . . . . ?
C2 B3 B8 B12 -97.92(13) . . . . ?
B9 B3 B8 B12 37.78(11) . . . . ?
B4 B3 B8 B12 0.79(15) . . . . ?
C1 B3 B9 B8 100.83(12) . . . . ?
C2 B3 B9 B8 38.18(11) . . . . ?
B4 B3 B9 B8 138.71(12) . . . . ?
C1 B3 B9 B4 -37.88(11) . . . . ?
C2 B3 B9 B4 -100.53(12) . . . . ?
B8 B3 B9 B4 -138.71(12) . . . . ?
C1 B3 B9 B12 63.02(14) . . . . ?
C2 B3 B9 B12 0.37(15) . . . . ?
B8 B3 B9 B12 -37.81(11) . . . . ?
B4 B3 B9 B12 100.90(13) . . . . ?
C1 B3 B9 B10 -0.47(15) . . . . ?
C2 B3 B9 B10 -63.12(14) . . . . ?
B8 B3 B9 B10 -101.31(13) . . . . ?
B4 B3 B9 B10 37.41(11) . . . . ?
C2 B8 B9 B3 -38.65(11) . . . . ?
B7 B8 B9 B3 -99.98(13) . . . . ?
B12 B8 B9 B3 -137.89(12) . . . . ?
C2 B8 B9 B4 -1.32(16) . . . . ?
B7 B8 B9 B4 -62.65(15) . . . . ?
B3 B8 B9 B4 37.33(11) . . . . ?
B12 B8 B9 B4 -100.57(13) . . . . ?
C2 B8 B9 B12 99.24(13) . . . . ?
B7 B8 B9 B12 37.92(12) . . . . ?
B3 B8 B9 B12 137.89(12) . . . . ?
C2 B8 B9 B10 62.22(15) . . . . ?
B7 B8 B9 B10 0.89(16) . . . . ?
B3 B8 B9 B10 100.87(13) . . . . ?
B12 B8 B9 B10 -37.02(12) . . . . ?
C1 B4 B9 B3 38.36(11) . . . . ?
B10 B4 B9 B3 138.12(12) . . . . ?
B5 B4 B9 B3 100.23(13) . . . . ?
C1 B4 B9 B8 1.01(16) . . . . ?
B10 B4 B9 B8 100.77(13) . . . . ?
B3 B4 B9 B8 -37.35(11) . . . . ?
B5 B4 B9 B8 62.88(15) . . . . ?
C1 B4 B9 B12 -62.86(14) . . . . ?
B10 B4 B9 B12 36.90(11) . . . . ?
B3 B4 B9 B12 -101.22(13) . . . . ?
B5 B4 B9 B12 -0.99(16) . . . . ?
C1 B4 B9 B10 -99.76(13) . . . . ?
B3 B4 B9 B10 -138.12(12) . . . . ?
B5 B4 B9 B10 -37.89(11) . . . . ?
C1 B5 B11 B6 -38.61(11) . . . . ?
B4 B5 B11 B6 -100.16(13) . . . . ?
B10 B5 B11 B6 -137.68(12) . . . . ?
C1 B5 B11 B7 -1.27(16) . . . . ?
B6 B5 B11 B7 37.34(11) . . . . ?
B4 B5 B11 B7 -62.82(15) . . . . ?
B10 B5 B11 B7 -100.34(13) . . . . ?
C1 B5 B11 B10 99.07(12) . . . . ?
B6 B5 B11 B10 137.68(12) . . . . ?
B4 B5 B11 B10 37.52(11) . . . . ?
C1 B5 B11 B12 61.91(14) . . . . ?
B6 B5 B11 B12 100.53(13) . . . . ?
B4 B5 B11 B12 0.36(16) . . . . ?
B10 B5 B11 B12 -37.16(11) . . . . ?
C1 B4 B10 B5 -38.22(11) . . . . ?
B9 B4 B10 B5 -137.77(12) . . . . ?
B3 B4 B10 B5 -100.50(13) . . . . ?
C1 B4 B10 B11 -0.78(16) . . . . ?
B9 B4 B10 B11 -100.32(13) . . . . ?
B3 B4 B10 B11 -63.06(15) . . . . ?
B5 B4 B10 B11 37.45(11) . . . . ?
C1 B4 B10 B12 62.73(15) . . . . ?
B9 B4 B10 B12 -36.82(12) . . . . ?
B3 B4 B10 B12 0.45(16) . . . . ?
B5 B4 B10 B12 100.95(13) . . . . ?
C1 B4 B10 B9 99.54(12) . . . . ?
B3 B4 B10 B9 37.26(11) . . . . ?
B5 B4 B10 B9 137.77(12) . . . . ?
C1 B5 B10 B4 37.99(11) . . . . ?
B6 B5 B10 B4 100.31(13) . . . . ?
B11 B5 B10 B4 137.93(12) . . . . ?
C1 B5 B10 B11 -99.94(12) . . . . ?
B6 B5 B10 B11 -37.62(11) . . . . ?
B4 B5 B10 B11 -137.93(12) . . . . ?
C1 B5 B10 B12 -62.69(15) . . . . ?
B6 B5 B10 B12 -0.37(16) . . . . ?
B4 B5 B10 B12 -100.68(13) . . . . ?
B11 B5 B10 B12 37.25(12) . . . . ?
C1 B5 B10 B9 0.55(15) . . . . ?
B6 B5 B10 B9 62.87(15) . . . . ?
B4 B5 B10 B9 -37.44(11) . . . . ?
B11 B5 B10 B9 100.49(13) . . . . ?
B6 B11 B10 B4 0.08(16) . . . . ?
B7 B11 B10 B4 63.63(15) . . . . ?
B5 B11 B10 B4 -37.51(11) . . . . ?
B12 B11 B10 B4 100.93(13) . . . . ?
B6 B11 B10 B5 37.59(11) . . . . ?
B7 B11 B10 B5 101.15(13) . . . . ?
B12 B11 B10 B5 138.44(13) . . . . ?
B6 B11 B10 B12 -100.85(13) . . . . ?
B7 B11 B10 B12 -37.29(12) . . . . ?
B5 B11 B10 B12 -138.44(13) . . . . ?
B6 B11 B10 B9 -62.80(15) . . . . ?
B7 B11 B10 B9 0.75(16) . . . . ?
B5 B11 B10 B9 -100.40(13) . . . . ?
B12 B11 B10 B9 38.04(12) . . . . ?
B3 B9 B10 B4 -37.64(11) . . . . ?
B8 B9 B10 B4 -101.65(13) . . . . ?
B12 B9 B10 B4 -138.78(13) . . . . ?
B3 B9 B10 B5 -0.05(16) . . . . ?
B8 B9 B10 B5 -64.06(15) . . . . ?
B4 B9 B10 B5 37.59(11) . . . . ?
B12 B9 B10 B5 -101.19(13) . . . . ?
B3 B9 B10 B11 62.99(15) . . . . ?
B8 B9 B10 B11 -1.02(16) . . . . ?
B4 B9 B10 B11 100.63(13) . . . . ?
B12 B9 B10 B11 -38.15(12) . . . . ?
B3 B9 B10 B12 101.14(13) . . . . ?
B8 B9 B10 B12 37.13(12) . . . . ?
B4 B9 B10 B12 138.78(13) . . . . ?
C2 B8 B12 B7 37.68(11) . . . . ?
B9 B8 B12 B7 137.38(13) . . . . ?
B3 B8 B12 B7 99.90(13) . . . . ?
C2 B8 B12 B9 -99.69(13) . . . . ?
B7 B8 B12 B9 -137.38(13) . . . . ?
B3 B8 B12 B9 -37.48(11) . . . . ?
C2 B8 B12 B10 -62.72(15) . . . . ?
B9 B8 B12 B10 36.97(12) . . . . ?
B7 B8 B12 B10 -100.40(13) . . . . ?
B3 B8 B12 B10 -0.51(16) . . . . ?
C2 B8 B12 B11 0.57(15) . . . . ?
B9 B8 B12 B11 100.26(13) . . . . ?
B7 B8 B12 B11 -37.12(11) . . . . ?
B3 B8 B12 B11 62.78(15) . . . . ?
B3 B9 B12 B7 0.09(16) . . . . ?
B8 B9 B12 B7 -37.82(11) . . . . ?
B4 B9 B12 B7 64.03(15) . . . . ?
B10 B9 B12 B7 100.88(13) . . . . ?
B3 B9 B12 B8 37.91(11) . . . . ?
B4 B9 B12 B8 101.85(13) . . . . ?
B10 B9 B12 B8 138.70(13) . . . . ?
B3 B9 B12 B10 -100.79(13) . . . . ?
B8 B9 B12 B10 -138.70(13) . . . . ?
B4 B9 B12 B10 -36.85(12) . . . . ?
B3 B9 B12 B11 -62.73(15) . . . . ?
B8 B9 B12 B11 -100.65(13) . . . . ?
B4 B9 B12 B11 1.21(16) . . . . ?
B10 B9 B12 B11 38.06(12) . . . . ?
B4 B10 B12 B7 -63.25(15) . . . . ?
B5 B10 B12 B7 0.16(16) . . . . ?
B11 B10 B12 B7 37.27(12) . . . . ?
B9 B10 B12 B7 -99.95(13) . . . . ?
B4 B10 B12 B8 0.04(16) . . . . ?
B5 B10 B12 B8 63.45(15) . . . . ?
B11 B10 B12 B8 100.56(13) . . . . ?
B9 B10 B12 B8 -36.66(11) . . . . ?
B4 B10 B12 B9 36.70(11) . . . . ?
B5 B10 B12 B9 100.11(13) . . . . ?
B11 B10 B12 B9 137.22(13) . . . . ?
B4 B10 B12 B11 -100.52(13) . . . . ?
B5 B10 B12 B11 -37.11(12) . . . . ?
B9 B10 B12 B11 -137.22(13) . . . . ?
B6 B11 B12 B7 -37.70(11) . . . . ?
B5 B11 B12 B7 -100.87(13) . . . . ?
B10 B11 B12 B7 -138.05(13) . . . . ?
B6 B11 B12 B8 -0.46(16) . . . . ?
B7 B11 B12 B8 37.24(11) . . . . ?
B5 B11 B12 B8 -63.63(15) . . . . ?
B10 B11 B12 B8 -100.81(13) . . . . ?
B6 B11 B12 B9 62.20(15) . . . . ?
B7 B11 B12 B9 99.90(13) . . . . ?
B5 B11 B12 B9 -0.97(16) . . . . ?
B10 B11 B12 B9 -38.15(12) . . . . ?
B6 B11 B12 B10 100.35(13) . . . . ?
B7 B11 B12 B10 138.05(13) . . . . ?
B5 B11 B12 B10 37.18(12) . . . . ?
C34 C2 B7 B11 -144.48(13) . . . . ?
B8 C2 B7 B11 102.17(13) . . . . ?
B3 C2 B7 B11 64.29(15) . . . . ?
C1 C2 B7 B11 -0.33(15) . . . . ?
B6 C2 B7 B11 -38.15(11) . . . . ?
C34 C2 B7 B12 152.03(13) . . . . ?
B8 C2 B7 B12 38.68(11) . . . . ?
B3 C2 B7 B12 0.80(16) . . . . ?
C1 C2 B7 B12 -63.82(14) . . . . ?
B6 C2 B7 B12 -101.64(13) . . . . ?
C34 C2 B7 B6 -106.33(14) . . . . ?
B8 C2 B7 B6 140.32(12) . . . . ?
B3 C2 B7 B6 102.44(12) . . . . ?
C1 C2 B7 B6 37.82(11) . . . . ?
C34 C2 B7 B8 113.36(14) . . . . ?
B3 C2 B7 B8 -37.88(11) . . . . ?
C1 C2 B7 B8 -102.50(12) . . . . ?
B6 C2 B7 B8 -140.32(12) . . . . ?
B6 B11 B7 C2 38.12(11) . . . . ?
B5 B11 B7 C2 0.99(16) . . . . ?
B10 B11 B7 C2 -62.39(15) . . . . ?
B12 B11 B7 C2 -99.78(13) . . . . ?
B6 B11 B7 B12 137.90(12) . . . . ?
B5 B11 B7 B12 100.77(13) . . . . ?
B10 B11 B7 B12 37.39(12) . . . . ?
B5 B11 B7 B6 -37.13(11) . . . . ?
B10 B11 B7 B6 -100.51(13) . . . . ?
B12 B11 B7 B6 -137.90(12) . . . . ?
B6 B11 B7 B8 100.30(13) . . . . ?
B5 B11 B7 B8 63.17(15) . . . . ?
B10 B11 B7 B8 -0.21(16) . . . . ?
B12 B11 B7 B8 -37.60(12) . . . . ?
B8 B12 B7 C2 -38.10(11) . . . . ?
B9 B12 B7 C2 -0.52(16) . . . . ?
B10 B12 B7 C2 62.79(15) . . . . ?
B11 B12 B7 C2 100.16(13) . . . . ?
B8 B12 B7 B11 -138.26(13) . . . . ?
B9 B12 B7 B11 -100.68(13) . . . . ?
B10 B12 B7 B11 -37.37(12) . . . . ?
B8 B12 B7 B6 -100.77(13) . . . . ?
B9 B12 B7 B6 -63.20(15) . . . . ?
B10 B12 B7 B6 0.11(16) . . . . ?
B11 B12 B7 B6 37.49(11) . . . . ?
B9 B12 B7 B8 37.58(11) . . . . ?
B10 B12 B7 B8 100.89(13) . . . . ?
B11 B12 B7 B8 138.26(13) . . . . ?
B9 B8 B7 C2 98.14(13) . . . . ?
B3 B8 B7 C2 35.23(11) . . . . ?
B12 B8 B7 C2 136.32(12) . . . . ?
C2 B8 B7 B11 -98.57(13) . . . . ?
B9 B8 B7 B11 -0.42(16) . . . . ?
B3 B8 B7 B11 -63.33(15) . . . . ?
B12 B8 B7 B11 37.75(12) . . . . ?
C2 B8 B7 B12 -136.32(12) . . . . ?
B9 B8 B7 B12 -38.18(12) . . . . ?
B3 B8 B7 B12 -101.09(13) . . . . ?
C2 B8 B7 B6 -35.37(11) . . . . ?
B9 B8 B7 B6 62.77(15) . . . . ?
B3 B8 B7 B6 -0.14(16) . . . . ?
B12 B8 B7 B6 100.95(13) . . . . ?
C18 C1 B6 C2 107.85(14) . . . . ?
B4 C1 B6 C2 -100.43(12) . . . . ?
B5 C1 B6 C2 -138.34(12) . . . . ?
B3 C1 B6 C2 -32.73(11) . . . . ?
C18 C1 B6 B11 -152.92(13) . . . . ?
B4 C1 B6 B11 -1.20(16) . . . . ?
B5 C1 B6 B11 -39.11(11) . . . . ?
B3 C1 B6 B11 66.49(14) . . . . ?
C2 C1 B6 B11 99.23(12) . . . . ?
C18 C1 B6 B5 -113.81(14) . . . . ?
B4 C1 B6 B5 37.92(12) . . . . ?
B3 C1 B6 B5 105.61(13) . . . . ?
C2 C1 B6 B5 138.34(12) . . . . ?
C18 C1 B6 B7 144.17(13) . . . . ?
B4 C1 B6 B7 -64.11(15) . . . . ?
B5 C1 B6 B7 -102.02(13) . . . . ?
B3 C1 B6 B7 3.59(15) . . . . ?
C2 C1 B6 B7 36.32(11) . . . . ?
C34 C2 B6 C1 -110.09(14) . . . . ?
B7 C2 B6 C1 138.08(12) . . . . ?
B8 C2 B6 C1 100.12(12) . . . . ?
B3 C2 B6 C1 32.60(11) . . . . ?
C34 C2 B6 B11 149.99(13) . . . . ?
B7 C2 B6 B11 38.16(11) . . . . ?
B8 C2 B6 B11 0.20(15) . . . . ?
B3 C2 B6 B11 -67.32(14) . . . . ?
C1 C2 B6 B11 -99.92(12) . . . . ?
C34 C2 B6 B5 -146.63(13) . . . . ?
B7 C2 B6 B5 101.54(13) . . . . ?
B8 C2 B6 B5 63.57(15) . . . . ?
B3 C2 B6 B5 -3.94(16) . . . . ?
C1 C2 B6 B5 -36.54(11) . . . . ?
C34 C2 B6 B7 111.83(14) . . . . ?
B8 C2 B6 B7 -37.96(12) . . . . ?
B3 C2 B6 B7 -105.48(13) . . . . ?
C1 C2 B6 B7 -138.08(12) . . . . ?
B7 B11 B6 C1 -100.06(12) . . . . ?
B5 B11 B6 C1 38.34(11) . . . . ?
B10 B11 B6 C1 0.64(15) . . . . ?
B12 B11 B6 C1 -62.60(14) . . . . ?
B7 B11 B6 C2 -37.29(11) . . . . ?
B5 B11 B6 C2 101.11(12) . . . . ?
B10 B11 B6 C2 63.41(14) . . . . ?
B12 B11 B6 C2 0.17(15) . . . . ?
B7 B11 B6 B5 -138.40(12) . . . . ?
B10 B11 B6 B5 -37.69(11) . . . . ?
B12 B11 B6 B5 -100.94(13) . . . . ?
B5 B11 B6 B7 138.40(12) . . . . ?
B10 B11 B6 B7 100.71(13) . . . . ?
B12 B11 B6 B7 37.46(11) . . . . ?
B4 B5 B6 C1 -34.96(11) . . . . ?
B11 B5 B6 C1 -135.90(12) . . . . ?
B10 B5 B6 C1 -98.08(12) . . . . ?
C1 B5 B6 C2 37.09(11) . . . . ?
B4 B5 B6 C2 2.12(16) . . . . ?
B11 B5 B6 C2 -98.81(13) . . . . ?
B10 B5 B6 C2 -61.00(15) . . . . ?
C1 B5 B6 B11 135.90(12) . . . . ?
B4 B5 B6 B11 100.94(13) . . . . ?
B10 B5 B6 B11 37.82(11) . . . . ?
C1 B5 B6 B7 98.53(12) . . . . ?
B4 B5 B6 B7 63.56(15) . . . . ?
B11 B5 B6 B7 -37.37(11) . . . . ?
B10 B5 B6 B7 0.44(16) . . . . ?
C2 B7 B6 C1 -37.16(11) . . . . ?
B11 B7 B6 C1 99.54(13) . . . . ?
B12 B7 B6 C1 61.64(15) . . . . ?
B8 B7 B6 C1 -2.04(16) . . . . ?
B11 B7 B6 C2 136.70(12) . . . . ?
B12 B7 B6 C2 98.80(13) . . . . ?
B8 B7 B6 C2 35.12(11) . . . . ?
C2 B7 B6 B11 -136.70(12) . . . . ?
B12 B7 B6 B11 -37.90(12) . . . . ?
B8 B7 B6 B11 -101.58(13) . . . . ?
C2 B7 B6 B5 -99.15(12) . . . . ?
B11 B7 B6 B5 37.55(11) . . . . ?
B12 B7 B6 B5 -0.35(16) . . . . ?
B8 B7 B6 B5 -64.03(15) . . . . ?

_diffrn_measured_fraction_theta_max 0.995
_diffrn_reflns_theta_full        27.19
_diffrn_measured_fraction_theta_full 0.995
_refine_diff_density_max         0.287
_refine_diff_density_min         -0.294
_refine_diff_density_rms         0.049
