# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2017

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_ma142
_database_code_depnum_ccdc_archive 'CCDC 1575686'
_audit_update_record             
;
2017-12-06 deposited with the CCDC.
2017-12-21 downloaded from the CCDC.
;

#===============================================================================

# 5. CHEMICAL DATA

_chemical_name_systematic        
;
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         
'C36 H36 Cl2 Dy N4 O9 Zn2, 3(C36 H38 Cl2 Dy N4 O9 Zn2), 2(Cl4 Zn), H2 O'
# Ex: 'C12 H16 N2 O6, H2 O' and '(Cd 2+)3, (C6 N6 Cr 3-)2, 2(H2 O)' 
_chemical_formula_structural     ?
_chemical_formula_sum            'C144 H152 Cl16 Dy4 N16 O37 Zn10'
_chemical_formula_iupac          ?
_chemical_formula_weight         4569.71
_chemical_compound_source        'see text'

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 ' International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

#===============================================================================

# 6. CRYSTAL DATA

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_symmetry_Int_Tables_number      2

loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,-y,-z

_cell_length_a                   15.581(3)
_cell_length_b                   20.331(4)
_cell_length_c                   29.683(5)
_cell_angle_alpha                82.897(9)
_cell_angle_beta                 80.573(9)
_cell_angle_gamma                74.654(10)
_cell_volume                     8913(3)
_cell_formula_units_Z            2
_cell_measurement_temperature    296
_cell_measurement_reflns_used    9783
_cell_measurement_theta_min      2.41
_cell_measurement_theta_max      22.97
_cell_special_details            
;
 
;

_exptl_crystal_description       block
_exptl_crystal_colour            'light yellow'

_exptl_crystal_size_max          0.150
_exptl_crystal_size_mid          0.130
_exptl_crystal_size_min          0.100
_exptl_crystal_size_rad          ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.703
_exptl_crystal_density_method    'Not Measured'
_exptl_crystal_F_000             4520
_exptl_absorpt_coefficient_mu    3.283
_exptl_crystal_density_meas_temp ?

_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2012/1 - Bruker AXS area detector scaling and absorption correction'
_exptl_absorpt_correction_T_min  0.650
_exptl_absorpt_correction_T_max  0.745

#===============================================================================

# 7. EXPERIMENTAL DATA

_exptl_special_details           
;
;
_diffrn_ambient_temperature      296
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         ?
_diffrn_radiation_monochromator  ?
_diffrn_detector_area_resol_mean 18.4

# number of measured reflections (redundant set)
_diffrn_reflns_number            114686
_diffrn_reflns_av_R_equivalents  0.0785
_diffrn_reflns_av_unetI/netI     0.0888
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_limit_l_max       35
_diffrn_reflns_theta_min         2.01
_diffrn_reflns_theta_max         25.03
_diffrn_reflns_theta_full        25.03
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_reflns_reduction_process 
;
;

# number of unique reflections
_reflns_number_total             31138
# number of observed reflections (> n sig(I))
_reflns_number_gt                19357
_reflns_threshold_expression     'I > 2σ(I)'
_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick 2014)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'

#===============================================================================

# 8. REFINEMENT DATA

_refine_special_details          SQUEEZE
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'W=1/[Σ²(FO²)+(0.1277P)²] WHERE P=(FO²+2FC²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_abs_structure_details ?
_refine_ls_abs_structure_Flack   .
_refine_ls_number_reflns         31138
_refine_ls_number_parameters     2060
_refine_ls_number_restraints     128
_refine_ls_number_constraints    ?
_refine_ls_R_factor_all          0.1107
_refine_ls_R_factor_gt           0.0658
_refine_ls_wR_factor_ref         0.2138
_refine_ls_wR_factor_gt          0.1837
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_restrained_S_all      1.030
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         2.224
_refine_diff_density_min         -1.614
_refine_diff_density_rms         0.185

#===============================================================================

# 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_thermal_displace_type
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy Uani 0.15684(3) 0.26331(3) 1.03185(2) 1.000 0.0393(2) d . . .
Dy2 Dy Uani 0.56305(4) 0.39452(3) 0.82206(2) 1.000 0.0407(2) d . . .
Dy3 Dy Uani 0.94050(3) 0.14999(2) 0.65480(2) 1.000 0.0357(2) d . . .
Dy4 Dy Uani 0.62715(3) 0.78394(2) 0.55936(2) 1.000 0.0345(2) d . . .
Zn1 Zn Uani 0.03416(8) 0.29417(7) 0.93806(4) 1.000 0.0439(4) d . . .
Zn2 Zn Uani 0.27325(10) 0.22646(7) 1.12527(4) 1.000 0.0522(5) d . . .
Zn3 Zn Uani 0.46057(9) 0.57161(6) 0.81214(4) 1.000 0.0464(4) d . . .
Zn4 Zn Uani 0.67494(10) 0.22363(7) 0.83004(4) 1.000 0.0509(5) d . . .
Zn5 Zn Uani 1.02188(9) -0.02085(7) 0.69992(4) 1.000 0.0453(4) d . . .
Zn6 Zn Uani 0.84666(9) 0.31854(6) 0.61687(4) 1.000 0.0451(4) d . . .
Zn7 Zn Uani 0.73061(9) 0.78146(6) 0.65295(4) 1.000 0.0434(4) d . . .
Zn8 Zn Uani 0.51689(8) 0.77871(6) 0.46498(4) 1.000 0.0404(4) d . . .
Zn9 Zn Uani 0.32834(19) -0.04936(13) 0.84389(9) 1.000 0.1245(11) d . . .
Zn10 Zn Uani 0.1914(3) 0.5879(2) 0.63453(14) 0.650 0.1653(19) d DUP A 1
Zn11 Zn Uani 0.1193(5) 0.5724(4) 0.6642(3) 0.350 0.161(3) d DUP B 2
Cl1 Cl Uani 0.1556(3) 0.2317(2) 1.18043(12) 1.000 0.0929(18) d . . .
Cl2 Cl Uani 0.0010(2) 0.39479(18) 0.89632(13) 1.000 0.0779(12) d . . .
Cl3 Cl Uani 0.4240(2) 0.62709(18) 0.87610(12) 1.000 0.0703(11) d . . .
Cl4 Cl Uani 0.8124(2) 0.24036(18) 0.80111(10) 1.000 0.0648(11) d . . .
Cl5 Cl Uani 1.0472(2) -0.10394(16) 0.65293(11) 1.000 0.0605(11) d . . .
Cl6 Cl Uani 0.7072(2) 0.32819(15) 0.65747(10) 1.000 0.0561(10) d D . .
Cl7 Cl Uani 0.6074(2) 0.80886(17) 0.70523(10) 1.000 0.0646(11) d . . .
Cl8 Cl Uani 0.4985(2) 0.86192(16) 0.40862(10) 1.000 0.0618(11) d . . .
Cl9 Cl Uani 0.3443(5) -0.1450(3) 0.8095(3) 1.000 0.176(4) d . . .
Cl10 Cl Uani 0.1830(6) 0.0134(4) 0.8422(4) 1.000 0.220(5) d . . .
Cl11 Cl Uani 0.4260(4) 0.0054(3) 0.80119(19) 1.000 0.133(3) d . . .
Cl12 Cl Uani 0.3552(6) -0.0818(4) 0.9156(2) 1.000 0.182(4) d . . .
O1 O Uani 0.1790(5) 0.3821(4) 1.0037(3) 1.000 0.056(3) d . . .
O1W O Uani 0.0564(6) 0.2222(5) 1.0913(3) 1.000 0.072(3) d . . .
O2 O Uani 0.2378(5) 0.3051(4) 1.0737(2) 1.000 0.047(2) d . . .
O3 O Uani 0.2485(6) 0.1777(4) 1.0765(3) 1.000 0.054(3) d . . .
O4 O Uani 0.1759(5) 0.1384(4) 1.0173(3) 1.000 0.052(3) d . . .
O5 O Uani 0.3139(5) 0.2316(4) 0.9838(3) 1.000 0.050(3) d . . .
O6 O Uani 0.1631(5) 0.2569(4) 0.9534(2) 1.000 0.043(2) d . . .
O7 O Uani 0.0224(5) 0.3035(4) 1.0062(2) 1.000 0.047(3) d . . .
O8 O Uani 0.0340(5) 0.3684(4) 1.0738(3) 1.000 0.060(3) d . . .
N1 N Uani 0.3628(9) 0.2737(6) 1.1369(4) 1.000 0.085(2) d . . .
N2 N Uani 0.3815(9) 0.1447(6) 1.1350(4) 1.000 0.085(2) d . . .
N3 N Uani 0.0622(7) 0.2187(5) 0.8946(3) 1.000 0.056(4) d . . .
N4 N Uani -0.0843(7) 0.2608(5) 0.9557(3) 1.000 0.050(3) d . . .
Cl13 Cl Uani 0.2947(5) 0.6260(5) 0.5795(3) 0.650 0.211(4) d DUP A 1
Cl14 Cl Uani 0.0691(5) 0.5872(6) 0.5998(3) 0.650 0.183(2) d DUP A 1
Cl15 Cl Uani 0.1430(6) 0.6661(4) 0.6893(3) 0.650 0.1850(19) d DUP A 1
Cl16 Cl Uani 0.2646(7) 0.4849(4) 0.6695(3) 0.650 0.161(3) d DUP A 1
C1 C Uani 0.1362(13) 0.4269(8) 0.9681(6) 1.000 0.120(9) d . . .
C2 C Uani 0.2320(7) 0.4086(6) 1.0264(4) 1.000 0.049(4) d . . .
O2W O Uani 0.6904(5) 0.3878(4) 0.7618(2) 1.000 0.056(3) d . . .
C3 C Uani 0.2528(8) 0.4709(6) 1.0162(4) 1.000 0.052(4) d . . .
C4 C Uani 0.3103(9) 0.4888(6) 1.0397(4) 1.000 0.057(5) d . . .
C5 C Uani 0.3499(9) 0.4444(6) 1.0741(4) 1.000 0.062(5) d . . .
C6 C Uani 0.3271(8) 0.3808(6) 1.0860(4) 1.000 0.052(4) d . . .
C7 C Uani 0.2652(7) 0.3631(5) 1.0636(3) 1.000 0.039(3) d . . .
C8 C Uani 0.3761(11) 0.3316(7) 1.1212(5) 1.000 0.085(2) d . . .
C9 C Uani 0.4257(11) 0.2307(6) 1.1665(5) 1.000 0.085(2) d D . .
O9 O Uani 0.7116(5) 0.4187(4) 0.8493(3) 1.000 0.051(3) d . . .
C10 C Uani 0.4242(11) 0.1605(6) 1.1687(5) 1.000 0.085(2) d D . .
O10 O Uani 0.5835(5) 0.5015(3) 0.8117(2) 1.000 0.044(2) d . . .
O11 O Uani 0.4310(5) 0.4793(4) 0.8183(2) 1.000 0.044(3) d . . .
C11 C Uani 0.4100(11) 0.0921(7) 1.1119(5) 1.000 0.085(2) d . . .
O12 O Uani 0.4150(6) 0.3611(4) 0.8446(3) 1.000 0.061(3) d . . .
C12 C Uani 0.3704(8) 0.0745(5) 1.0789(4) 1.000 0.054(4) d . . .
C13 C Uani 0.2924(8) 0.1152(6) 1.0632(4) 1.000 0.049(4) d . . .
O13 O Uani 0.5204(5) 0.4082(4) 0.9093(2) 1.000 0.054(3) d . . .
O14 O Uani 0.6160(5) 0.3016(4) 0.8723(2) 1.000 0.047(3) d . . .
C14 C Uani 0.2536(8) 0.0935(5) 1.0301(3) 1.000 0.042(4) d . . .
O15 O Uani 0.5874(5) 0.2883(4) 0.7928(3) 1.000 0.053(3) d . . .
C15 C Uani 0.2981(9) 0.0332(6) 1.0099(5) 1.000 0.066(5) d . . .
C16 C Uani 0.3790(9) -0.0057(7) 1.0227(5) 1.000 0.079(6) d . . .
O16 O Uani 0.5081(5) 0.3934(4) 0.7454(2) 1.000 0.050(3) d . . .
C17 C Uani 0.4129(9) 0.0160(7) 1.0586(5) 1.000 0.070(5) d . . .
C18 C Uani 0.1115(10) 0.1125(7) 0.9981(5) 1.000 0.077(6) d . . .
C19 C Uani 0.4005(8) 0.2227(7) 0.9990(4) 1.000 0.066(5) d . . .
C20 C Uani 0.3162(7) 0.2002(6) 0.9455(4) 1.000 0.046(4) d . . .
C21 C Uani 0.2317(7) 0.2137(5) 0.9296(4) 1.000 0.042(3) d . . .
C22 C Uani 0.2229(8) 0.1808(6) 0.8930(4) 1.000 0.054(4) d . . .
C23 C Uani 0.3012(9) 0.1369(7) 0.8707(5) 1.000 0.072(5) d . . .
C24 C Uani 0.3814(10) 0.1240(7) 0.8847(5) 1.000 0.070(5) d . . .
C25 C Uani 0.3895(8) 0.1547(6) 0.9238(5) 1.000 0.061(4) d . . .
C26 C Uani 0.1362(9) 0.1836(7) 0.8796(4) 1.000 0.065(5) d . . .
C27 C Uani -0.0233(9) 0.2113(7) 0.8820(5) 1.000 0.070(5) d . . .
C28 C Uani -0.0929(9) 0.2123(6) 0.9262(5) 1.000 0.067(5) d . . .
C29 C Uani -0.1436(9) 0.2824(7) 0.9855(4) 1.000 0.058(5) d . . .
C30 C Uani -0.1391(7) 0.3265(6) 1.0200(4) 1.000 0.049(4) d . . .
C31 C Uani -0.2178(8) 0.3592(6) 1.0473(4) 1.000 0.060(4) d . . .
C32 C Uani -0.2129(8) 0.3976(7) 1.0829(4) 1.000 0.064(5) d . . .
C33 C Uani -0.1340(8) 0.4043(6) 1.0932(4) 1.000 0.058(5) d . . .
C34 C Uani -0.0544(8) 0.3714(6) 1.0667(4) 1.000 0.049(4) d . . .
C35 C Uani -0.0571(7) 0.3344(5) 1.0300(4) 1.000 0.045(3) d . . .
C36 C Uani 0.0407(10) 0.4034(7) 1.1118(5) 1.000 0.078(6) d . . .
N5 N Uani 0.5216(7) 0.6287(5) 0.7623(3) 1.000 0.060(4) d . . .
N6 N Uani 0.3551(8) 0.6110(5) 0.7753(4) 1.000 0.066(4) d . . .
N7 N Uani 0.6973(7) 0.1569(5) 0.8850(3) 1.000 0.060(4) d . . .
N8 N Uani 0.6376(7) 0.1425(5) 0.8102(4) 1.000 0.061(4) d . . .
Cl17 Cl Uani 0.1616(11) 0.6742(6) 0.6551(7) 0.350 0.178(3) d DUP B 2
Cl18 Cl Uani 0.2467(8) 0.4832(6) 0.6599(5) 0.350 0.164(4) d DUP B 2
Cl19 Cl Uani 0.0309(8) 0.5581(10) 0.7332(3) 0.350 0.166(4) d DUP B 2
Cl20 Cl Uani 0.0401(9) 0.5698(8) 0.6055(4) 0.350 0.150(2) d DUP B 2
O3W O Uani 0.8083(5) 0.1882(4) 0.7083(3) 1.000 0.051(3) d . . .
O17 O Uani 1.0975(5) 0.1677(4) 0.6225(2) 1.000 0.048(3) d . . .
O18 O Uani 1.0649(5) 0.0639(3) 0.6714(2) 1.000 0.041(2) d . . .
O19 O Uani 0.9058(4) 0.0521(3) 0.6900(2) 1.000 0.041(2) d . . .
O20 O Uani 0.7906(5) 0.1151(4) 0.6372(2) 1.000 0.045(2) d . . .
O21 O Uani 0.9814(5) 0.0998(4) 0.5780(2) 1.000 0.048(3) d . . .
O22 O Uani 0.8922(5) 0.2226(3) 0.5916(2) 1.000 0.040(2) d . . .
O23 O Uani 0.9327(5) 0.2643(4) 0.6604(2) 1.000 0.048(3) d . . .
O24 O Uani 0.9949(5) 0.1805(4) 0.7245(2) 1.000 0.058(3) d . . .
C37 C Uani 0.7794(8) 0.3753(7) 0.8747(4) 1.000 0.066(5) d . . .
C38 C Uani 0.7308(8) 0.4788(6) 0.8291(4) 1.000 0.052(4) d . . .
C39 C Uani 0.6591(7) 0.5223(6) 0.8077(3) 1.000 0.043(4) d . . .
C40 C Uani 0.6717(8) 0.5858(5) 0.7850(4) 1.000 0.046(4) d . . .
C41 C Uani 0.7534(9) 0.6037(7) 0.7852(4) 1.000 0.064(5) d . . .
C42 C Uani 0.8182(9) 0.5596(8) 0.8069(5) 1.000 0.074(6) d . . .
C43 C Uani 0.8112(9) 0.4968(7) 0.8277(5) 1.000 0.066(5) d . . .
C44 C Uani 0.6024(9) 0.6323(6) 0.7594(4) 1.000 0.059(5) d . . .
C45 C Uani 0.4601(11) 0.6720(9) 0.7319(6) 1.000 0.102(7) d . . .
C46 C Uani 0.3651(11) 0.6779(8) 0.7526(6) 1.000 0.097(7) d . . .
C47 C Uani 0.2913(9) 0.5846(7) 0.7739(5) 1.000 0.072(5) d . . .
C48 C Uani 0.2842(8) 0.5195(7) 0.7959(4) 1.000 0.061(5) d . . .
C49 C Uani 0.3535(8) 0.4699(6) 0.8166(4) 1.000 0.045(4) d . . .
C50 C Uani 0.3393(8) 0.4082(7) 0.8310(4) 1.000 0.059(5) d . . .
C51 C Uani 0.2577(11) 0.3901(9) 0.8316(5) 1.000 0.090(7) d . . .
C52 C Uani 0.1843(10) 0.4414(10) 0.8152(5) 1.000 0.088(7) d . . .
C53 C Uani 0.1996(10) 0.5015(9) 0.7973(5) 1.000 0.084(6) d . . .
C54 C Uani 0.4124(10) 0.2919(7) 0.8653(5) 1.000 0.087(6) d . . .
C55 C Uani 0.4468(10) 0.4587(7) 0.9282(5) 1.000 0.088(6) d . . .
C56 C Uani 0.5567(8) 0.3537(5) 0.9392(3) 1.000 0.042(4) d . . .
C57 C Uani 0.6047(7) 0.2960(6) 0.9181(3) 1.000 0.042(3) d . . .
C58 C Uani 0.6388(8) 0.2359(6) 0.9455(3) 1.000 0.050(4) d . . .
C59 C Uani 0.6240(9) 0.2385(7) 0.9931(4) 1.000 0.062(5) d . . .
C60 C Uani 0.5801(8) 0.2957(7) 1.0135(4) 1.000 0.061(5) d . . .
C61 C Uani 0.5434(9) 0.3560(7) 0.9869(4) 1.000 0.062(5) d . . .
C62 C Uani 0.6818(8) 0.1677(6) 0.9277(4) 1.000 0.053(4) d . . .
C63 C Uani 0.7280(10) 0.0890(7) 0.8696(5) 1.000 0.077(6) d . . .
C64 C Uani 0.6667(12) 0.0799(6) 0.8397(5) 1.000 0.082(6) d . . .
C65 C Uani 0.5863(11) 0.1472(6) 0.7801(6) 1.000 0.080(6) d . . .
C66 C Uani 0.5414(9) 0.2080(6) 0.7540(4) 1.000 0.056(4) d . . .
C67 C Uani 0.5447(8) 0.2735(6) 0.7618(4) 1.000 0.050(4) d . . .
C68 C Uani 0.4999(8) 0.3304(7) 0.7354(4) 1.000 0.057(5) d . . .
C69 C Uani 0.4495(10) 0.3222(7) 0.7028(4) 1.000 0.071(5) d . . .
C70 C Uani 0.4493(12) 0.2544(8) 0.6968(5) 1.000 0.089(7) d . . .
C71 C Uani 0.4932(12) 0.2017(7) 0.7242(6) 1.000 0.087(7) d . . .
C72 C Uani 0.4827(9) 0.4517(7) 0.7132(4) 1.000 0.069(5) d . . .
N9 N Uani 1.1223(7) -0.0455(5) 0.7390(3) 1.000 0.062(4) d . . .
N10 N Uani 0.9524(8) -0.0524(5) 0.7592(3) 1.000 0.063(4) d . . .
N11 N Uani 0.8348(7) 0.3586(5) 0.5501(3) 1.000 0.055(4) d . . .
N12 N Uani 0.8991(8) 0.4024(5) 0.6152(4) 1.000 0.064(4) d . . .
O4W O Uani 0.5187(5) 0.7744(4) 0.6251(3) 1.000 0.056(3) d . . .
O25 O Uani 0.6635(5) 0.8904(3) 0.5141(2) 1.000 0.044(3) d . . .
O26 O Uani 0.7083(5) 0.8393(3) 0.5922(2) 1.000 0.039(2) d . . .
O27 O Uani 0.7087(5) 0.7150(3) 0.6124(2) 1.000 0.041(2) d . . .
O28 O Uani 0.6149(5) 0.6583(4) 0.5738(3) 1.000 0.054(3) d . . .
O29 O Uani 0.5013(5) 0.9058(4) 0.5800(2) 1.000 0.045(2) d . . .
O30 O Uani 0.4967(4) 0.8166(3) 0.5282(2) 1.000 0.037(2) d . . .
O31 O Uani 0.6407(4) 0.7451(3) 0.4878(2) 1.000 0.041(2) d . . .
O32 O Uani 0.7859(5) 0.7324(4) 0.5205(2) 1.000 0.046(3) d . . .
C73 C Uani 1.1173(9) 0.2233(7) 0.5895(4) 1.000 0.069(5) d . . .
C74 C Uani 1.1689(8) 0.1287(6) 0.6457(4) 1.000 0.048(4) d . . .
C75 C Uani 1.1469(7) 0.0731(6) 0.6726(4) 1.000 0.045(4) d . . .
C76 C Uani 1.2089(7) 0.0336(6) 0.6994(4) 1.000 0.050(4) d . . .
C77 C Uani 1.2926(8) 0.0515(8) 0.6974(5) 1.000 0.069(5) d . . .
C78 C Uani 1.3115(9) 0.1030(7) 0.6715(5) 1.000 0.068(5) d . . .
C79 C Uani 1.2492(9) 0.1434(7) 0.6445(4) 1.000 0.063(5) d . . .
C80 C Uani 1.1908(8) -0.0226(6) 0.7346(4) 1.000 0.059(5) d . . .
C81 C Uani 1.1061(10) -0.1032(8) 0.7753(5) 1.000 0.083(6) d . . .
C82 C Uani 1.0140(11) -0.0874(10) 0.7965(6) 1.000 0.112(8) d . . .
C83 C Uani 0.8692(9) -0.0514(6) 0.7647(5) 1.000 0.064(5) d . . .
C84 C Uani 0.8080(8) -0.0157(6) 0.7334(4) 1.000 0.049(4) d . . .
C85 C Uani 0.8272(7) 0.0350(5) 0.6989(3) 1.000 0.040(3) d . . .
C86 C Uani 0.7632(7) 0.0675(5) 0.6718(4) 1.000 0.046(4) d . . .
C87 C Uani 0.6798(8) 0.0513(7) 0.6783(5) 1.000 0.065(5) d . . .
C88 C Uani 0.6638(9) 0.0006(7) 0.7113(5) 1.000 0.067(5) d . . .
C89 C Uani 0.7269(8) -0.0304(6) 0.7387(5) 1.000 0.062(5) d . . .
C90 C Uani 0.7221(9) 0.1578(7) 0.6117(5) 1.000 0.066(5) d . . .
C91 C Uani 1.0480(11) 0.0353(7) 0.5701(5) 1.000 0.088(6) d . . .
C92 C Uani 0.9584(7) 0.1428(6) 0.5390(3) 1.000 0.044(4) d . . .
C93 C Uani 0.9112(6) 0.2095(5) 0.5482(3) 1.000 0.036(3) d . . .
C94 C Uani 0.8922(7) 0.2550(6) 0.5113(3) 1.000 0.041(4) d . . .
C95 C Uani 0.9137(9) 0.2367(7) 0.4676(4) 1.000 0.057(4) d . . .
C96 C Uani 0.9594(9) 0.1707(9) 0.4594(4) 1.000 0.075(6) d . . .
C97 C Uani 0.9823(8) 0.1212(6) 0.4951(4) 1.000 0.053(4) d . . .
C98 C Uani 0.8569(8) 0.3296(7) 0.5133(4) 1.000 0.060(5) d . . .
C99 C Uani 0.8107(11) 0.4363(6) 0.5512(5) 1.000 0.074(6) d . . .
C100 C Uani 0.8814(10) 0.4519(6) 0.5759(5) 1.000 0.070(5) d . . .
C101 C Uani 0.9531(11) 0.4068(8) 0.6438(6) 1.000 0.090(7) d . . .
C102 C Uani 0.9783(18) 0.3599(11) 0.6804(7) 1.000 0.146(6) d . . .
C103 C Uani 1.0246(17) 0.3782(10) 0.7151(7) 1.000 0.146(6) d . . .
C104 C Uani 1.0617(17) 0.3332(10) 0.7487(7) 1.000 0.146(6) d . . .
C105 C Uani 1.0486(17) 0.2677(10) 0.7541(7) 1.000 0.146(6) d . . .
C106 C Uani 1.0059(10) 0.2458(8) 0.7233(5) 1.000 0.072(6) d . . .
C107 C Uani 0.9698(9) 0.2898(6) 0.6877(4) 1.000 0.058(5) d . . .
C108 C Uani 1.0151(10) 0.1349(7) 0.7636(4) 1.000 0.081(6) d . . .
N13 N Uani 0.5461(7) 0.6860(5) 0.4361(3) 1.000 0.057(4) d . . .
N14 N Uani 0.3934(7) 0.7539(5) 0.4859(3) 1.000 0.047(3) d . . .
N15 N Uani 0.8201(7) 0.8369(5) 0.6583(3) 1.000 0.056(4) d . . .
N16 N Uani 0.8273(7) 0.7010(5) 0.6775(3) 1.000 0.054(3) d . . .
C109 C Uani 0.8666(8) 0.7282(7) 0.5387(5) 1.000 0.069(5) d . . .
C110 C Uani 0.7869(7) 0.6828(6) 0.4935(4) 1.000 0.044(4) d . . .
C111 C Uani 0.8627(8) 0.6267(6) 0.4818(4) 1.000 0.060(4) d . . .
C112 C Uani 0.8541(10) 0.5816(7) 0.4542(6) 1.000 0.083(6) d . . .
C113 C Uani 0.7768(10) 0.5896(7) 0.4365(5) 1.000 0.078(6) d . . .
C114 C Uani 0.7013(8) 0.6442(6) 0.4460(4) 1.000 0.053(4) d . . .
C115 C Uani 0.7070(7) 0.6915(5) 0.4745(4) 1.000 0.047(4) d . . .
C116 C Uani 0.6171(8) 0.6433(6) 0.4300(4) 1.000 0.055(4) d . . .
C117 C Uani 0.4628(9) 0.6790(7) 0.4222(5) 1.000 0.072(6) d . . .
C118 C Uani 0.3836(8) 0.6948(7) 0.4652(4) 1.000 0.062(5) d . . .
C119 C Uani 0.3304(8) 0.7841(6) 0.5149(4) 1.000 0.050(4) d . . .
C120 C Uani 0.3386(7) 0.8366(6) 0.5424(4) 1.000 0.044(4) d . . .
C121 C Uani 0.4176(6) 0.8500(5) 0.5475(3) 1.000 0.036(3) d . . .
C122 C Uani 0.4173(7) 0.8974(6) 0.5767(3) 1.000 0.042(4) d . . .
C123 C Uani 0.3378(8) 0.9332(6) 0.6010(4) 1.000 0.056(4) d . . .
C124 C Uani 0.2579(8) 0.9171(7) 0.5960(4) 1.000 0.059(4) d . . .
C125 C Uani 0.2571(8) 0.8701(7) 0.5675(4) 1.000 0.061(5) d . . .
C126 C Uani 0.5063(8) 0.9492(6) 0.6122(4) 1.000 0.061(5) d . . .
C127 C Uani 0.6242(10) 0.9223(7) 0.4751(4) 1.000 0.074(6) d . . .
C128 C Uani 0.7140(7) 0.9256(5) 0.5322(3) 1.000 0.036(3) d . . .
C129 C Uani 0.7397(6) 0.8928(5) 0.5752(3) 1.000 0.033(3) d . . .
C130 C Uani 0.7952(7) 0.9209(5) 0.5958(3) 1.000 0.040(3) d . . .
C131 C Uani 0.8195(7) 0.9803(5) 0.5748(4) 1.000 0.043(3) d . . .
C132 C Uani 0.7889(8) 1.0113(6) 0.5345(4) 1.000 0.051(4) d . . .
C133 C Uani 0.7351(7) 0.9844(5) 0.5132(4) 1.000 0.044(4) d . . .
C134 C Uani 0.8349(8) 0.8880(6) 0.6360(3) 1.000 0.046(4) d . . .
C135 C Uani 0.8693(10) 0.8008(7) 0.6980(4) 1.000 0.069(5) d . . .
C136 C Uani 0.8983(9) 0.7274(7) 0.6920(4) 1.000 0.063(5) d . . .
C137 C Uani 0.8302(8) 0.6370(7) 0.6782(4) 1.000 0.055(4) d . . .
C138 C Uani 0.7638(8) 0.6121(5) 0.6610(3) 1.000 0.046(4) d . . .
C139 C Uani 0.7089(7) 0.6493(5) 0.6284(4) 1.000 0.043(3) d . . .
C140 C Uani 0.6551(7) 0.6175(5) 0.6098(3) 1.000 0.041(3) d . . .
C141 C Uani 0.6463(8) 0.5531(5) 0.6249(4) 1.000 0.052(4) d . . .
C142 C Uani 0.6972(10) 0.5182(6) 0.6600(5) 1.000 0.067(5) d . . .
C143 C Uani 0.7574(10) 0.5451(6) 0.6747(5) 1.000 0.067(5) d . . .
C144 C Uani 0.5618(12) 0.6263(8) 0.5546(5) 1.000 0.102(8) d . . .
O5W O Uani 0.3722(9) 0.7216(9) 0.6334(5) 1.000 0.169(9) d . . .
H1A H Uiso 0.18110 0.43970 0.94510 1.000 0.1800 c GR . .
H1B H Uiso 0.09730 0.46720 0.98090 1.000 0.1800 c GR . .
H1C H Uiso 0.10170 0.40380 0.95470 1.000 0.1800 c GR . .
H3 H Uiso 0.22750 0.50120 0.99300 1.000 0.0630 c R . .
H4 H Uiso 0.32310 0.53130 1.03260 1.000 0.0690 c R . .
H5 H Uiso 0.39090 0.45610 1.08920 1.000 0.0740 c R . .
H8 H Uiso 0.42050 0.34510 1.13250 1.000 0.1020 c R . .
H9A H Uiso 0.48600 0.23530 1.15490 1.000 0.1020 c R . .
H9B H Uiso 0.41010 0.24620 1.19710 1.000 0.1020 c R . .
H10I H Uiso 0.48560 0.13270 1.16590 1.000 0.1020 c R . .
H10J H Uiso 0.39420 0.14800 1.19850 1.000 0.1020 c R . .
H11 H Uiso 0.46390 0.06230 1.11840 1.000 0.1020 c R . .
H15 H Uiso 0.27320 0.01890 0.98760 1.000 0.0790 c R . .
H16 H Uiso 0.41040 -0.04490 1.00830 1.000 0.0950 c R . .
H17 H Uiso 0.46590 -0.01070 1.06850 1.000 0.0840 c R . .
H18A H Uiso 0.09990 0.07300 1.01690 1.000 0.1140 c GR . .
H18B H Uiso 0.13600 0.10010 0.96760 1.000 0.1140 c GR . .
H18C H Uiso 0.05640 0.14740 0.99730 1.000 0.1140 c GR . .
H19A H Uiso 0.39420 0.25210 1.02290 1.000 0.0990 c GR . .
H19B H Uiso 0.44230 0.23430 0.97370 1.000 0.0990 c GR . .
H19C H Uiso 0.42220 0.17590 1.01040 1.000 0.0990 c GR . .
H23 H Uiso 0.29610 0.11630 0.84530 1.000 0.0860 c R . .
H24 H Uiso 0.43130 0.09540 0.86920 1.000 0.0830 c R . .
H25 H Uiso 0.44450 0.14420 0.93480 1.000 0.0740 c R . .
H26 H Uiso 0.13670 0.15540 0.85710 1.000 0.0780 c R . .
H27A H Uiso -0.01280 0.16860 0.86810 1.000 0.0840 c R . .
H27B H Uiso -0.04620 0.24860 0.85990 1.000 0.0840 c R . .
H28A H Uiso -0.15330 0.22470 0.91800 1.000 0.0800 c R . .
H28B H Uiso -0.08300 0.16700 0.94230 1.000 0.0800 c R . .
H29 H Uiso -0.19730 0.26990 0.98680 1.000 0.0690 c R . .
H31 H Uiso -0.27340 0.35550 1.04190 1.000 0.0710 c R . .
H32 H Uiso -0.26610 0.41930 1.10010 1.000 0.0760 c R . .
H33 H Uiso -0.13270 0.42980 1.11690 1.000 0.0700 c R . .
H36A H Uiso 0.01950 0.38040 1.14000 1.000 0.1180 c GR . .
H36B H Uiso 0.00480 0.44970 1.10910 1.000 0.1180 c GR . .
H36C H Uiso 0.10230 0.40360 1.11180 1.000 0.1180 c GR . .
H2WA H Uiso 0.68500 0.36890 0.73270 1.000 0.0840 d GRD . .
H2WB H Uiso 0.74840 0.35690 0.77020 1.000 0.0840 d GR . .
H37A H Uiso 0.76360 0.33290 0.88530 1.000 0.0980 c GR . .
H37B H Uiso 0.78380 0.39770 0.90060 1.000 0.0980 c GR . .
H37C H Uiso 0.83620 0.36620 0.85530 1.000 0.0980 c GR . .
H41 H Uiso 0.76240 0.64500 0.77060 1.000 0.0770 c R . .
H42 H Uiso 0.87080 0.57260 0.80780 1.000 0.0890 c R . .
H43 H Uiso 0.85910 0.46700 0.84060 1.000 0.0790 c R . .
H44 H Uiso 0.61950 0.66700 0.73950 1.000 0.0700 c R . .
H45A H Uiso 0.47070 0.65240 0.70270 1.000 0.1220 c R . .
H45B H Uiso 0.47140 0.71720 0.72630 1.000 0.1220 c R . .
H46A H Uiso 0.34760 0.71190 0.77480 1.000 0.1150 c R . .
H46B H Uiso 0.32620 0.69260 0.72890 1.000 0.1150 c R . .
H47 H Uiso 0.24550 0.60930 0.75740 1.000 0.0860 c R . .
H51 H Uiso 0.25170 0.34640 0.84230 1.000 0.1080 c R . .
H52 H Uiso 0.12790 0.43310 0.81700 1.000 0.1050 c R . .
H53 H Uiso 0.15320 0.53380 0.78500 1.000 0.1000 c R . .
H54A H Uiso 0.38880 0.26950 0.84540 1.000 0.1300 c GR . .
H54B H Uiso 0.37470 0.29510 0.89440 1.000 0.1300 c GR . .
H54C H Uiso 0.47210 0.26610 0.86970 1.000 0.1300 c GR . .
H55A H Uiso 0.43420 0.49760 0.90620 1.000 0.1320 c GR . .
H55B H Uiso 0.46130 0.47270 0.95520 1.000 0.1320 c GR . .
H55C H Uiso 0.39500 0.44040 0.93620 1.000 0.1320 c GR . .
H59 H Uiso 0.64550 0.19880 1.01140 1.000 0.0740 c R . .
H60 H Uiso 0.57400 0.29550 1.04530 1.000 0.0730 c R . .
H61 H Uiso 0.51170 0.39580 1.00060 1.000 0.0740 c R . .
H62 H Uiso 0.69860 0.13050 0.94880 1.000 0.0640 c R . .
H63A H Uiso 0.72980 0.05520 0.89570 1.000 0.0920 c R . .
H63B H Uiso 0.78820 0.08280 0.85290 1.000 0.0920 c R . .
H64A H Uiso 0.61470 0.06820 0.85830 1.000 0.0980 c R . .
H64B H Uiso 0.69680 0.04240 0.82090 1.000 0.0980 c R . .
H65 H Uiso 0.57630 0.10620 0.77400 1.000 0.0960 c R . .
H69 H Uiso 0.41750 0.35950 0.68580 1.000 0.0850 c R . .
H70 H Uiso 0.41950 0.24590 0.67430 1.000 0.1070 c R . .
H71 H Uiso 0.48800 0.15800 0.72110 1.000 0.1050 c R . .
H72A H Uiso 0.41840 0.46620 0.71560 1.000 0.1040 c GR . .
H72B H Uiso 0.50720 0.43930 0.68270 1.000 0.1040 c GR . .
H72C H Uiso 0.50560 0.48830 0.71980 1.000 0.1040 c GR . .
H3WA H Uiso 0.77270 0.23230 0.69960 1.000 0.0760 d GR . .
H3WB H Uiso 0.82040 0.19170 0.73810 1.000 0.0760 d GR . .
H10A H Uiso 0.93650 0.45000 0.55490 1.000 0.0840 c R . .
H10B H Uiso 0.85990 0.49770 0.58600 1.000 0.0840 c R . .
H10C H Uiso 1.00730 0.09100 0.75930 1.000 0.1210 c GR . .
H10D H Uiso 0.97560 0.15250 0.79010 1.000 0.1210 c GR . .
H10E H Uiso 1.07620 0.13040 0.76790 1.000 0.1210 c GR . .
H73A H Uiso 1.06680 0.24330 0.57330 1.000 0.1040 c GR . .
H73B H Uiso 1.16910 0.20550 0.56800 1.000 0.1040 c GR . .
H73C H Uiso 1.12910 0.25760 0.60540 1.000 0.1040 c GR . .
H77 H Uiso 1.33480 0.02500 0.71540 1.000 0.0830 c R . .
H78 H Uiso 1.36650 0.11300 0.67090 1.000 0.0820 c R . .
H79 H Uiso 1.26260 0.18040 0.62560 1.000 0.0760 c R . .
H80 H Uiso 1.23300 -0.04160 0.75440 1.000 0.0700 c R . .
H81A H Uiso 1.11980 -0.14590 0.76100 1.000 0.1000 c R . .
H81B H Uiso 1.14540 -0.10890 0.79840 1.000 0.1000 c R . .
H82A H Uiso 1.00610 -0.05690 0.82040 1.000 0.1340 c R . .
H82B H Uiso 0.99790 -0.12900 0.81040 1.000 0.1340 c R . .
H83 H Uiso 0.84670 -0.07530 0.79080 1.000 0.0770 c R . .
H87 H Uiso 0.63560 0.07470 0.66040 1.000 0.0790 c R . .
H88 H Uiso 0.61000 -0.01230 0.71480 1.000 0.0800 c R . .
H89 H Uiso 0.71410 -0.06280 0.76190 1.000 0.0750 c R . .
H90A H Uiso 0.66770 0.17270 0.63220 1.000 0.0990 c GR . .
H90B H Uiso 0.71120 0.13220 0.58900 1.000 0.0990 c GR . .
H90C H Uiso 0.74180 0.19700 0.59680 1.000 0.0990 c GR . .
H91A H Uiso 1.10090 0.04430 0.55160 1.000 0.1310 c GR . .
H91B H Uiso 1.02360 0.00720 0.55450 1.000 0.1310 c GR . .
H91C H Uiso 1.06320 0.01190 0.59890 1.000 0.1310 c GR . .
H95 H Uiso 0.89770 0.26890 0.44340 1.000 0.0690 c R . .
H96 H Uiso 0.97530 0.15880 0.42940 1.000 0.0900 c R . .
H97 H Uiso 1.01210 0.07620 0.48980 1.000 0.0630 c R . .
H98 H Uiso 0.85070 0.35680 0.48580 1.000 0.0720 c R . .
H99A H Uiso 0.75100 0.45230 0.56770 1.000 0.0890 c R . .
H99B H Uiso 0.81240 0.45860 0.52040 1.000 0.0890 c R . .
H101 H Uiso 0.97670 0.44500 0.63910 1.000 0.1080 c R . .
H103 H Uiso 1.02850 0.42320 0.71390 1.000 0.1740 c R . .
H104 H Uiso 1.09530 0.34610 0.76760 1.000 0.1740 c R . .
H105 H Uiso 1.06870 0.23790 0.77880 1.000 0.1740 c R . .
H4WA H Uiso 0.53090 0.79170 0.64720 1.000 0.0840 d GR . .
H4WB H Uiso 0.52460 0.73230 0.63420 1.000 0.0840 d GR . .
H10F H Uiso 0.86090 0.76930 0.55290 1.000 0.1030 c GR . .
H10G H Uiso 0.91610 0.72290 0.51440 1.000 0.1030 c GR . .
H10H H Uiso 0.87710 0.68950 0.56100 1.000 0.1030 c GR . .
H11A H Uiso 0.47080 0.63300 0.41370 1.000 0.0870 c R . .
H11B H Uiso 0.44730 0.71100 0.39600 1.000 0.0870 c R . .
H11C H Uiso 0.32530 0.70480 0.45490 1.000 0.0750 c R . .
H11D H Uiso 0.38870 0.65530 0.48760 1.000 0.0750 c R . .
H12A H Uiso 0.49190 0.92900 0.64250 1.000 0.0910 c GR . .
H12B H Uiso 0.46430 0.99270 0.60750 1.000 0.0910 c GR . .
H12C H Uiso 0.56600 0.95550 0.60840 1.000 0.0910 c GR . .
H12D H Uiso 0.66530 0.90910 0.44810 1.000 0.1100 c GR . .
H12E H Uiso 0.61050 0.97110 0.47590 1.000 0.1100 c GR . .
H12F H Uiso 0.56990 0.90850 0.47480 1.000 0.1100 c GR . .
H13A H Uiso 0.92100 0.81850 0.69880 1.000 0.0830 c R . .
H13B H Uiso 0.82970 0.80860 0.72670 1.000 0.0830 c R . .
H13C H Uiso 0.91500 0.70260 0.72060 1.000 0.0760 c R . .
H13D H Uiso 0.95120 0.71880 0.66910 1.000 0.0760 c R . .
H14A H Uiso 0.51590 0.61540 0.57780 1.000 0.1520 c GR . .
H14B H Uiso 0.59870 0.58510 0.54220 1.000 0.1520 c GR . .
H14C H Uiso 0.53440 0.65670 0.53060 1.000 0.1520 c GR . .
H111 H Uiso 0.91650 0.62170 0.49310 1.000 0.0720 c R . .
H112 H Uiso 0.90220 0.54440 0.44710 1.000 0.1000 c R . .
H113 H Uiso 0.77350 0.55770 0.41730 1.000 0.0940 c R . .
H116 H Uiso 0.61830 0.60660 0.41380 1.000 0.0660 c R . .
H119 H Uiso 0.27580 0.77210 0.51880 1.000 0.0590 c R . .
H123 H Uiso 0.33780 0.96650 0.61990 1.000 0.0670 c R . .
H124 H Uiso 0.20420 0.93920 0.61260 1.000 0.0710 c R . .
H125 H Uiso 0.20350 0.86000 0.56460 1.000 0.0730 c R . .
H131 H Uiso 0.85660 0.99900 0.58830 1.000 0.0510 c R . .
H132 H Uiso 0.80490 1.05100 0.52140 1.000 0.0610 c R . .
H133 H Uiso 0.71380 1.00630 0.48640 1.000 0.0530 c R . .
H134 H Uiso 0.87530 0.90770 0.64580 1.000 0.0550 c R . .
H137 H Uiso 0.87720 0.60510 0.69040 1.000 0.0650 c R . .
H141 H Uiso 0.60880 0.53310 0.61280 1.000 0.0630 c R . .
H142 H Uiso 0.68910 0.47600 0.67310 1.000 0.0810 c R . .
H143 H Uiso 0.79570 0.51820 0.69450 1.000 0.0800 c R . .
H5WA H Uiso 0.36560 0.76070 0.64280 1.000 0.2530 d R . .
H5WB H Uiso 0.35900 0.73020 0.60630 1.000 0.2530 d R . .


#===============================================================================

# 10. MOLECULAR GEOMETRY

_geom_special_details            
;
 Bond distances, angles etc. have been calculated using the
 rounded fractional coordinates. All su's are estimated
 from the variances of the (full) variance-covariance matrix.
 The cell esds are taken into account in the estimation of
 distances, angles and torsion angles
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O1 2.549(8) . . yes
Dy1 O1W 2.384(9) . . yes
Dy1 O2 2.280(8) . . yes
Dy1 O3 2.358(9) . . yes
Dy1 O4 2.560(8) . . yes
Dy1 O5 2.586(8) . . yes
Dy1 O6 2.333(6) . . yes
Dy1 O7 2.258(8) . . yes
Dy1 O8 2.737(8) . . yes
Dy2 O13 2.596(6) . . yes
Dy2 O14 2.314(7) . . yes
Dy2 O2W 2.431(7) . . yes
Dy2 O9 2.751(8) . . yes
Dy2 O10 2.257(6) . . yes
Dy2 O11 2.317(8) . . yes
Dy2 O12 2.538(10) . . yes
Dy2 O16 2.564(6) . . yes
Dy2 O15 2.342(8) . . yes
Dy3 O19 2.284(6) . . yes
Dy3 O18 2.317(7) . . yes
Dy3 O21 2.530(6) . . yes
Dy3 O22 2.336(6) . . yes
Dy3 O3W 2.399(8) . . yes
Dy3 O17 2.578(8) . . yes
Dy3 O24 2.560(7) . . yes
Dy3 O20 2.757(8) . . yes
Dy3 O23 2.320(8) . . yes
Dy4 O31 2.315(6) . . yes
Dy4 O32 2.557(8) . . yes
Dy4 O27 2.286(7) . . yes
Dy4 O26 2.290(7) . . yes
Dy4 O29 2.787(8) . . yes
Dy4 O30 2.275(6) . . yes
Dy4 O4W 2.388(9) . . yes
Dy4 O25 2.548(6) . . yes
Dy4 O28 2.590(8) . . yes
Zn1 O7 2.029(6) . . yes
Zn1 N3 2.040(10) . . yes
Zn1 Cl2 2.238(4) . . yes
Zn1 O6 2.056(8) . . yes
Zn1 N4 2.098(11) . . yes
Zn2 O3 1.992(9) . . yes
Zn2 N2 2.061(13) . . yes
Zn2 O2 2.100(7) . . yes
Zn2 Cl1 2.238(4) . . yes
Zn2 N1 1.984(14) . . yes
Zn3 O10 2.062(7) . . yes
Zn3 O11 2.028(8) . . yes
Zn3 N5 2.034(10) . . yes
Zn3 Cl3 2.244(4) . . yes
Zn3 N6 2.053(12) . . yes
Zn4 O14 2.067(7) . . yes
Zn4 O15 1.999(8) . . yes
Zn4 N8 2.066(11) . . yes
Zn4 N7 2.003(9) . . yes
Zn4 Cl4 2.270(4) . . yes
Zn5 O18 2.049(7) . . yes
Zn5 N9 2.020(11) . . yes
Zn5 N10 2.036(10) . . yes
Zn5 Cl5 2.237(3) . . yes
Zn5 O19 2.050(6) . . yes
Zn6 Cl6 2.278(3) . . yes
Zn6 O23 2.029(7) . . yes
Zn6 N11 2.066(9) . . yes
Zn6 O22 2.080(6) . . yes
Zn6 N12 2.069(11) . . yes
Zn7 Cl7 2.253(3) . . yes
Zn7 O26 2.054(6) . . yes
Zn7 N15 2.047(11) . . yes
Zn7 N16 2.058(10) . . yes
Zn7 O27 2.043(6) . . yes
Zn8 Cl8 2.223(3) . . yes
Zn8 N14 2.095(11) . . yes
Zn8 N13 2.077(10) . . yes
Zn8 O31 2.065(7) . . yes
Zn8 O30 2.062(6) . . yes
Zn9 Cl12 2.223(7) . . yes
Zn9 Cl10 2.292(10) . . yes
Zn9 Cl9 2.244(7) . . yes
Zn9 Cl11 2.253(7) . . yes
Zn10 Cl14 2.314(10) . . yes
Zn10 Cl15 2.311(9) . . yes
Zn10 Cl13 2.312(10) . . yes
Zn10 Cl16 2.313(9) . . yes
Zn11 Cl20 2.307(16) . . yes
Zn11 Cl18 2.305(15) . . yes
Zn11 Cl19 2.306(13) . . yes
Zn11 Cl17 2.306(16) . . yes
O1 C1 1.44(2) . . yes
O1 C2 1.391(14) . . yes
O2 C7 1.342(13) . . yes
O3 C13 1.347(14) . . yes
O4 C18 1.466(18) . . yes
O4 C14 1.387(14) . . yes
O5 C20 1.362(14) . . yes
O5 C19 1.452(15) . . yes
O6 C21 1.350(13) . . yes
O7 C35 1.356(13) . . yes
O8 C36 1.437(17) . . yes
O8 C34 1.412(15) . . yes
N1 C8 1.268(19) . . yes
N1 C9 1.46(2) . . yes
N2 C11 1.281(18) . . yes
N2 C10 1.40(2) . . yes
N3 C27 1.490(18) . . yes
N3 C26 1.230(18) . . yes
N4 C29 1.201(16) . . yes
N4 C28 1.442(16) . . yes
C2 C3 1.375(17) . . no
C2 C7 1.423(15) . . no
C3 C4 1.365(19) . . no
C4 C5 1.386(17) . . no
C5 C6 1.419(17) . . no
C6 C8 1.508(19) . . no
C6 C7 1.398(17) . . no
O9 C38 1.377(14) . . yes
O9 C37 1.437(15) . . yes
C9 C10 1.427(17) . . no
O10 C39 1.336(14) . . yes
O11 C49 1.281(15) . . yes
C11 C12 1.37(2) . . no
O12 C54 1.472(16) . . yes
O12 C50 1.391(16) . . yes
C12 C13 1.392(17) . . no
C12 C17 1.359(17) . . no
O13 C56 1.387(12) . . yes
C13 C14 1.403(16) . . no
O13 C55 1.412(17) . . yes
O14 C57 1.336(11) . . yes
C14 C15 1.393(16) . . no
C15 C16 1.38(2) . . no
O15 C67 1.325(15) . . yes
C16 C17 1.43(2) . . no
O16 C72 1.439(15) . . yes
O16 C68 1.392(16) . . yes
C20 C25 1.386(17) . . no
C20 C21 1.418(16) . . no
C21 C22 1.387(16) . . no
C22 C26 1.455(19) . . no
C22 C23 1.424(19) . . no
C23 C24 1.33(2) . . no
C24 C25 1.42(2) . . no
C27 C28 1.56(2) . . no
C29 C30 1.463(17) . . no
C30 C35 1.411(16) . . no
C30 C31 1.407(17) . . no
C31 C32 1.412(17) . . no
C32 C33 1.358(18) . . no
C33 C34 1.406(17) . . no
C34 C35 1.410(16) . . no
C1 H1B 0.9600 . . no
C1 H1C 0.9600 . . no
C1 H1A 0.9600 . . no
O2W H2WA 1.0100 . . no
O2W H2WB 1.0000 . . no
C3 H3 0.9300 . . no
C4 H4 0.9300 . . no
N5 C44 1.269(18) . . yes
C5 H5 0.9300 . . no
N5 C45 1.47(2) . . yes
N6 C46 1.476(19) . . yes
N6 C47 1.257(19) . . yes
N7 C62 1.286(15) . . yes
N7 C63 1.442(17) . . yes
N8 C64 1.463(17) . . yes
N8 C65 1.27(2) . . yes
C8 H8 0.9300 . . no
C9 H9A 0.9700 . . no
C9 H9B 0.9700 . . no
C10 H10J 0.9700 . . no
C10 H10I 0.9700 . . no
C11 H11 0.9300 . . no
C15 H15 0.9300 . . no
C16 H16 0.9300 . . no
C17 H17 0.9300 . . no
C18 H18C 0.9600 . . no
C18 H18B 0.9600 . . no
C18 H18A 0.9600 . . no
C19 H19C 0.9600 . . no
C19 H19A 0.9600 . . no
C19 H19B 0.9600 . . no
C23 H23 0.9300 . . no
C24 H24 0.9300 . . no
C25 H25 0.9300 . . no
C26 H26 0.9300 . . no
C27 H27B 0.9700 . . no
C27 H27A 0.9700 . . no
C28 H28B 0.9700 . . no
C28 H28A 0.9700 . . no
C29 H29 0.9300 . . no
C31 H31 0.9300 . . no
C32 H32 0.9300 . . no
C33 H33 0.9300 . . no
C36 H36B 0.9600 . . no
C36 H36C 0.9600 . . no
C36 H36A 0.9600 . . no
O17 C73 1.464(15) . . yes
O17 C74 1.411(15) . . yes
O18 C75 1.346(14) . . yes
O19 C85 1.337(13) . . yes
O20 C90 1.441(16) . . yes
O20 C86 1.415(13) . . yes
O21 C92 1.397(12) . . yes
O21 C91 1.459(17) . . yes
O22 C93 1.318(11) . . yes
O23 C107 1.294(15) . . yes
O24 C106 1.378(18) . . yes
O24 C108 1.416(14) . . yes
C38 C43 1.39(2) . . no
C38 C39 1.416(17) . . no
C39 C40 1.427(15) . . no
C40 C44 1.479(17) . . no
C40 C41 1.415(19) . . no
C41 C42 1.35(2) . . no
C42 C43 1.37(2) . . no
C45 C46 1.49(3) . . no
C47 C48 1.425(19) . . no
C48 C49 1.431(18) . . no
C48 C53 1.45(2) . . no
C49 C50 1.337(18) . . no
C50 C51 1.41(2) . . no
C51 C52 1.44(3) . . no
C52 C53 1.34(3) . . no
C56 C57 1.375(15) . . no
C56 C61 1.402(15) . . no
C57 C58 1.410(15) . . no
C58 C62 1.491(16) . . no
C58 C59 1.399(15) . . no
C59 C60 1.343(19) . . no
C60 C61 1.411(19) . . no
C63 C64 1.47(2) . . no
C65 C66 1.449(19) . . no
C66 C67 1.395(17) . . no
C66 C71 1.29(2) . . no
C67 C68 1.403(18) . . no
C68 C69 1.393(19) . . no
C69 C70 1.41(2) . . no
C70 C71 1.36(2) . . no
O3W H3WA 0.9500 . . no
O3W H3WB 0.9500 . . no
N9 C81 1.535(18) . . yes
N9 C80 1.255(17) . . yes
N10 C83 1.275(19) . . yes
N10 C82 1.56(2) . . yes
N11 C99 1.527(15) . . yes
N11 C98 1.260(15) . . yes
N12 C101 1.32(2) . . yes
N12 C100 1.455(18) . . yes
C37 H37C 0.9600 . . no
C37 H37A 0.9600 . . no
C37 H37B 0.9600 . . no
C41 H41 0.9300 . . no
C42 H42 0.9300 . . no
C43 H43 0.9300 . . no
C44 H44 0.9300 . . no
C45 H45B 0.9700 . . no
C45 H45A 0.9700 . . no
C46 H46A 0.9700 . . no
C46 H46B 0.9700 . . no
C47 H47 0.9300 . . no
C51 H51 0.9300 . . no
C52 H52 0.9300 . . no
C53 H53 0.9300 . . no
C54 H54A 0.9600 . . no
C54 H54C 0.9600 . . no
C54 H54B 0.9600 . . no
C55 H55B 0.9600 . . no
C55 H55A 0.9600 . . no
C55 H55C 0.9600 . . no
C59 H59 0.9300 . . no
C60 H60 0.9300 . . no
C61 H61 0.9300 . . no
C62 H62 0.9300 . . no
C63 H63A 0.9700 . . no
C63 H63B 0.9700 . . no
C64 H64A 0.9700 . . no
C64 H64B 0.9700 . . no
C65 H65 0.9300 . . no
C69 H69 0.9300 . . no
C70 H70 0.9300 . . no
C71 H71 0.9300 . . no
C72 H72A 0.9600 . . no
C72 H72C 0.9600 . . no
C72 H72B 0.9600 . . no
O25 C128 1.397(13) . . yes
O25 C127 1.404(14) . . yes
O26 C129 1.320(12) . . yes
O27 C139 1.361(12) . . yes
O28 C140 1.396(13) . . yes
O28 C144 1.40(2) . . yes
O29 C126 1.403(14) . . yes
O29 C122 1.384(14) . . yes
O30 C121 1.315(11) . . yes
O31 C115 1.337(12) . . yes
O32 C109 1.426(16) . . yes
O32 C110 1.359(14) . . yes
C74 C79 1.36(2) . . no
C74 C75 1.388(17) . . no
C75 C76 1.376(16) . . no
C76 C80 1.502(17) . . no
C76 C77 1.434(18) . . no
C77 C78 1.29(2) . . no
C78 C79 1.39(2) . . no
C81 C82 1.44(2) . . no
C83 C84 1.434(19) . . no
C84 C89 1.354(18) . . no
C84 C85 1.415(15) . . no
C85 C86 1.364(15) . . no
C86 C87 1.401(17) . . no
C87 C88 1.38(2) . . no
C88 C89 1.35(2) . . no
C92 C97 1.388(15) . . no
C92 C93 1.397(15) . . no
C93 C94 1.362(14) . . no
C94 C98 1.475(18) . . no
C94 C95 1.358(15) . . no
C95 C96 1.37(2) . . no
C96 C97 1.390(19) . . no
C99 C100 1.54(2) . . no
C101 C102 1.39(3) . . no
C102 C107 1.45(3) . . no
C102 C103 1.48(3) . . no
C103 C104 1.36(3) . . no
C104 C105 1.39(3) . . no
C105 C106 1.39(3) . . no
C106 C107 1.389(19) . . no
O4W H4WB 0.8500 . . no
O4W H4WA 0.8500 . . no
N13 C116 1.215(16) . . yes
N13 C117 1.471(18) . . yes
N14 C118 1.468(17) . . yes
N14 C119 1.271(16) . . yes
N15 C134 1.216(15) . . yes
N15 C135 1.516(16) . . yes
N16 C137 1.288(17) . . yes
N16 C136 1.492(18) . . yes
C73 H73C 0.9600 . . no
C73 H73A 0.9600 . . no
C73 H73B 0.9600 . . no
C77 H77 0.9300 . . no
C78 H78 0.9300 . . no
C79 H79 0.9300 . . no
C80 H80 0.9300 . . no
C81 H81A 0.9700 . . no
C81 H81B 0.9700 . . no
C82 H82A 0.9700 . . no
C82 H82B 0.9700 . . no
C83 H83 0.9300 . . no
C87 H87 0.9300 . . no
C88 H88 0.9300 . . no
C89 H89 0.9300 . . no
C90 H90A 0.9600 . . no
C90 H90B 0.9600 . . no
C90 H90C 0.9600 . . no
C91 H91B 0.9600 . . no
C91 H91C 0.9600 . . no
C91 H91A 0.9600 . . no
C95 H95 0.9300 . . no
C96 H96 0.9300 . . no
C97 H97 0.9300 . . no
C98 H98 0.9300 . . no
C99 H99B 0.9700 . . no
C99 H99A 0.9700 . . no
C100 H10B 0.9700 . . no
C100 H10A 0.9700 . . no
C101 H101 0.9300 . . no
C103 H103 0.9300 . . no
C104 H104 0.9300 . . no
C105 H105 0.9300 . . no
C108 H10E 0.9600 . . no
C108 H10C 0.9600 . . no
C108 H10D 0.9600 . . no
C110 C111 1.438(17) . . no
C110 C115 1.410(16) . . no
C111 C112 1.35(2) . . no
C112 C113 1.36(2) . . no
C113 C114 1.405(19) . . no
C114 C116 1.472(18) . . no
C114 C115 1.385(16) . . no
C117 C118 1.622(19) . . no
C119 C120 1.464(17) . . no
C120 C121 1.364(15) . . no
C120 C125 1.410(17) . . no
C121 C122 1.372(14) . . no
C122 C123 1.394(16) . . no
C123 C124 1.403(18) . . no
C124 C125 1.356(18) . . no
C128 C129 1.432(13) . . no
C128 C133 1.355(14) . . no
C129 C130 1.403(14) . . no
C130 C131 1.403(14) . . no
C130 C134 1.442(14) . . no
C131 C132 1.377(16) . . no
C132 C133 1.380(17) . . no
C135 C136 1.465(19) . . no
C137 C138 1.450(18) . . no
C138 C143 1.397(16) . . no
C138 C139 1.410(15) . . no
C139 C140 1.397(15) . . no
C140 C141 1.365(14) . . no
C141 C142 1.417(19) . . no
C142 C143 1.35(2) . . no
C109 H10H 0.9600 . . no
C109 H10G 0.9600 . . no
C109 H10F 0.9600 . . no
C111 H111 0.9300 . . no
C112 H112 0.9300 . . no
C113 H113 0.9300 . . no
C116 H116 0.9300 . . no
C117 H11B 0.9700 . . no
C117 H11A 0.9700 . . no
C118 H11C 0.9700 . . no
C118 H11D 0.9700 . . no
C119 H119 0.9300 . . no
C123 H123 0.9300 . . no
C124 H124 0.9300 . . no
C125 H125 0.9300 . . no
C126 H12C 0.9600 . . no
C126 H12B 0.9600 . . no
C126 H12A 0.9600 . . no
C127 H12E 0.9600 . . no
C127 H12F 0.9600 . . no
C127 H12D 0.9600 . . no
C131 H131 0.9300 . . no
C132 H132 0.9300 . . no
C133 H133 0.9300 . . no
C134 H134 0.9300 . . no
C135 H13B 0.9700 . . no
C135 H13A 0.9700 . . no
C136 H13C 0.9700 . . no
C136 H13D 0.9700 . . no
C137 H137 0.9300 . . no
C141 H141 0.9300 . . no
C142 H142 0.9300 . . no
C143 H143 0.9300 . . no
C144 H14B 0.9600 . . no
C144 H14C 0.9600 . . no
C144 H14A 0.9600 . . no
O5W H5WA 0.8500 . . no
O5W H5WB 0.8500 . . no

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Dy1 O1W 133.5(3) . . . yes
O1 Dy1 O2 64.4(3) . . . yes
O1 Dy1 O3 126.9(3) . . . yes
O1 Dy1 O4 149.9(3) . . . yes
O1 Dy1 O5 79.4(3) . . . yes
O1 Dy1 O6 81.4(3) . . . yes
O1 Dy1 O7 84.5(3) . . . yes
O1 Dy1 O8 65.3(3) . . . yes
O1W Dy1 O2 100.8(3) . . . yes
O1W Dy1 O3 74.3(3) . . . yes
O1W Dy1 O4 75.1(3) . . . yes
O1W Dy1 O5 144.2(3) . . . yes
O1W Dy1 O6 126.2(3) . . . yes
O1W Dy1 O7 76.9(3) . . . yes
O1W Dy1 O8 68.3(3) . . . yes
O2 Dy1 O3 66.5(3) . . . yes
O2 Dy1 O4 127.7(3) . . . yes
O2 Dy1 O5 79.7(3) . . . yes
O2 Dy1 O6 133.0(3) . . . yes
O2 Dy1 O7 134.9(3) . . . yes
O2 Dy1 O8 75.6(3) . . . yes
O3 Dy1 O4 62.2(3) . . . yes
O3 Dy1 O5 73.3(3) . . . yes
O3 Dy1 O6 121.3(3) . . . yes
O3 Dy1 O7 147.4(3) . . . yes
O3 Dy1 O8 119.3(3) . . . yes
O4 Dy1 O5 76.7(3) . . . yes
O4 Dy1 O6 71.4(3) . . . yes
O4 Dy1 O7 95.9(3) . . . yes
O4 Dy1 O8 140.3(3) . . . yes
O5 Dy1 O6 62.4(3) . . . yes
O5 Dy1 O7 127.8(2) . . . yes
O5 Dy1 O8 143.1(2) . . . yes
O6 Dy1 O7 66.3(3) . . . yes
O6 Dy1 O8 119.3(3) . . . yes
O7 Dy1 O8 61.5(3) . . . yes
O2W Dy2 O11 121.6(2) . . . yes
O2W Dy2 O12 142.9(3) . . . yes
O2W Dy2 O13 140.7(2) . . . yes
O2W Dy2 O14 101.9(3) . . . yes
O2W Dy2 O15 74.2(3) . . . yes
O2W Dy2 O16 71.8(2) . . . yes
O9 Dy2 O10 60.5(3) . . . yes
O9 Dy2 O11 121.9(3) . . . yes
O9 Dy2 O12 148.1(3) . . . yes
O9 Dy2 O13 74.9(3) . . . yes
O9 Dy2 O14 74.4(3) . . . yes
O9 Dy2 O15 114.9(3) . . . yes
O9 Dy2 O16 136.0(3) . . . yes
O10 Dy2 O11 66.4(3) . . . yes
O10 Dy2 O12 127.0(3) . . . yes
O10 Dy2 O13 89.1(2) . . . yes
O10 Dy2 O14 131.8(3) . . . yes
O10 Dy2 O15 148.1(3) . . . yes
O10 Dy2 O16 98.0(2) . . . yes
O11 Dy2 O12 61.7(3) . . . yes
O11 Dy2 O13 82.5(2) . . . yes
O11 Dy2 O14 136.5(2) . . . yes
O11 Dy2 O15 122.6(3) . . . yes
O11 Dy2 O16 71.4(2) . . . yes
O12 Dy2 O13 74.3(3) . . . yes
O12 Dy2 O14 83.9(3) . . . yes
O12 Dy2 O15 75.1(3) . . . yes
O12 Dy2 O16 75.9(3) . . . yes
O13 Dy2 O14 62.1(2) . . . yes
O13 Dy2 O15 121.3(3) . . . yes
O13 Dy2 O16 147.1(3) . . . yes
O14 Dy2 O15 65.9(3) . . . yes
O14 Dy2 O16 127.6(3) . . . yes
O15 Dy2 O16 62.4(3) . . . yes
O2W Dy2 O10 75.8(3) . . . yes
O2W Dy2 O9 66.0(2) . . . yes
O3W Dy3 O19 75.0(2) . . . yes
O3W Dy3 O18 124.9(3) . . . yes
O3W Dy3 O22 97.1(3) . . . yes
O3W Dy3 O20 65.8(2) . . . yes
O3W Dy3 O21 138.2(3) . . . yes
O17 Dy3 O18 61.9(2) . . . yes
O17 Dy3 O19 127.6(2) . . . yes
O17 Dy3 O20 146.58(19) . . . yes
O17 Dy3 O21 74.1(2) . . . yes
O17 Dy3 O22 85.4(2) . . . yes
O3W Dy3 O23 75.3(3) . . . yes
O3W Dy3 O24 73.9(3) . . . yes
O18 Dy3 O19 66.4(2) . . . yes
O18 Dy3 O20 119.1(2) . . . yes
O18 Dy3 O21 81.8(2) . . . yes
O18 Dy3 O22 138.0(2) . . . yes
O18 Dy3 O23 121.7(3) . . . yes
O18 Dy3 O24 72.2(2) . . . yes
O19 Dy3 O20 60.0(2) . . . yes
O19 Dy3 O21 91.4(2) . . . yes
O19 Dy3 O22 132.7(2) . . . yes
O19 Dy3 O23 146.7(2) . . . yes
O19 Dy3 O24 95.2(2) . . . yes
O20 Dy3 O21 73.2(2) . . . yes
O20 Dy3 O22 74.0(2) . . . yes
O17 Dy3 O23 73.6(3) . . . yes
O17 Dy3 O24 76.8(2) . . . yes
O20 Dy3 O23 118.8(3) . . . yes
O20 Dy3 O24 136.6(2) . . . yes
O21 Dy3 O22 63.4(2) . . . yes
O21 Dy3 O23 120.9(2) . . . yes
O21 Dy3 O24 147.6(3) . . . yes
O22 Dy3 O23 66.0(2) . . . yes
O22 Dy3 O24 128.0(2) . . . yes
O23 Dy3 O24 62.2(2) . . . yes
O3W Dy3 O17 144.5(3) . . . yes
O4W Dy4 O30 78.4(3) . . . yes
O4W Dy4 O31 129.2(3) . . . yes
O4W Dy4 O29 65.0(2) . . . yes
O25 Dy4 O26 63.3(2) . . . yes
O25 Dy4 O27 125.6(3) . . . yes
O25 Dy4 O28 157.3(2) . . . yes
O25 Dy4 O29 65.7(2) . . . yes
O25 Dy4 O30 85.4(2) . . . yes
O25 Dy4 O31 84.3(2) . . . yes
O4W Dy4 O32 145.0(2) . . . yes
O26 Dy4 O27 66.9(2) . . . yes
O26 Dy4 O28 129.9(2) . . . yes
O26 Dy4 O29 77.8(2) . . . yes
O26 Dy4 O30 134.8(2) . . . yes
O26 Dy4 O31 134.1(2) . . . yes
O26 Dy4 O32 79.4(2) . . . yes
O27 Dy4 O28 62.9(3) . . . yes
O27 Dy4 O29 122.7(2) . . . yes
O27 Dy4 O30 148.2(2) . . . yes
O27 Dy4 O31 118.0(2) . . . yes
O27 Dy4 O32 70.8(2) . . . yes
O28 Dy4 O29 130.7(2) . . . yes
O28 Dy4 O30 91.5(2) . . . yes
O28 Dy4 O31 73.8(2) . . . yes
O25 Dy4 O32 79.8(2) . . . yes
O31 Dy4 O32 62.7(2) . . . yes
O28 Dy4 O32 84.7(3) . . . yes
O29 Dy4 O30 59.2(2) . . . yes
O29 Dy4 O31 119.0(2) . . . yes
O29 Dy4 O32 144.5(2) . . . yes
O30 Dy4 O31 66.9(2) . . . yes
O30 Dy4 O32 128.5(2) . . . yes
O4W Dy4 O28 71.1(3) . . . yes
O4W Dy4 O25 129.7(2) . . . yes
O4W Dy4 O26 96.7(3) . . . yes
O4W Dy4 O27 75.7(3) . . . yes
N3 Zn1 N4 81.0(4) . . . yes
O7 Zn1 N4 84.3(3) . . . yes
Cl2 Zn1 N4 107.6(3) . . . yes
Cl2 Zn1 N3 107.7(3) . . . yes
Cl2 Zn1 O7 113.4(2) . . . yes
O6 Zn1 N3 87.4(4) . . . yes
O6 Zn1 N4 134.1(3) . . . yes
Cl2 Zn1 O6 118.2(2) . . . yes
O7 Zn1 N3 138.8(3) . . . yes
O6 Zn1 O7 75.9(3) . . . yes
Cl1 Zn2 N1 114.6(4) . . . yes
Cl1 Zn2 N2 114.5(4) . . . yes
O2 Zn2 O3 76.8(3) . . . yes
Cl1 Zn2 O3 105.5(3) . . . yes
O3 Zn2 N2 87.9(4) . . . yes
Cl1 Zn2 O2 108.6(2) . . . yes
O3 Zn2 N1 139.9(4) . . . yes
O2 Zn2 N2 136.8(4) . . . yes
N1 Zn2 N2 78.8(5) . . . yes
O2 Zn2 N1 87.4(4) . . . yes
Cl3 Zn3 N5 108.3(3) . . . yes
N5 Zn3 N6 81.7(5) . . . yes
Cl3 Zn3 O11 115.2(2) . . . yes
O11 Zn3 N6 88.9(4) . . . yes
Cl3 Zn3 O10 111.3(2) . . . yes
O11 Zn3 N5 136.5(3) . . . yes
O10 Zn3 N5 87.2(4) . . . yes
O10 Zn3 N6 143.4(4) . . . yes
O10 Zn3 O11 75.6(3) . . . yes
Cl3 Zn3 N6 105.4(3) . . . yes
Cl4 Zn4 N7 104.2(3) . . . yes
O15 Zn4 N7 148.9(4) . . . yes
Cl4 Zn4 O15 106.4(3) . . . yes
Cl4 Zn4 N8 118.9(3) . . . yes
N7 Zn4 N8 80.1(4) . . . yes
O15 Zn4 N8 89.5(4) . . . yes
Cl4 Zn4 O14 105.3(2) . . . yes
O14 Zn4 N8 135.9(4) . . . yes
O14 Zn4 O15 77.0(3) . . . yes
O14 Zn4 N7 90.2(3) . . . yes
Cl5 Zn5 N9 107.3(3) . . . yes
Cl5 Zn5 N10 106.3(3) . . . yes
O18 Zn5 O19 75.8(3) . . . yes
O18 Zn5 N10 138.9(3) . . . yes
Cl5 Zn5 O18 114.67(19) . . . yes
Cl5 Zn5 O19 111.0(2) . . . yes
N9 Zn5 N10 81.7(4) . . . yes
O19 Zn5 N9 141.7(3) . . . yes
O18 Zn5 N9 89.5(4) . . . yes
O19 Zn5 N10 86.6(4) . . . yes
O22 Zn6 N11 87.2(3) . . . yes
Cl6 Zn6 N12 115.2(3) . . . yes
O22 Zn6 O23 76.2(3) . . . yes
O22 Zn6 N12 135.4(4) . . . yes
Cl6 Zn6 O22 109.4(2) . . . yes
Cl6 Zn6 N11 109.4(3) . . . yes
N11 Zn6 N12 80.0(4) . . . yes
O23 Zn6 N11 145.1(4) . . . yes
O23 Zn6 N12 90.6(4) . . . yes
Cl6 Zn6 O23 105.0(2) . . . yes
O26 Zn7 N16 138.3(3) . . . yes
Cl7 Zn7 O27 107.5(2) . . . yes
Cl7 Zn7 O26 109.5(2) . . . yes
Cl7 Zn7 N15 110.8(3) . . . yes
Cl7 Zn7 N16 111.9(3) . . . yes
O26 Zn7 O27 76.0(2) . . . yes
O26 Zn7 N15 86.8(3) . . . yes
N15 Zn7 N16 83.3(4) . . . yes
O27 Zn7 N16 87.1(3) . . . yes
O27 Zn7 N15 141.4(3) . . . yes
O31 Zn8 N14 133.3(3) . . . yes
N13 Zn8 N14 81.2(4) . . . yes
O30 Zn8 O31 75.7(2) . . . yes
O30 Zn8 N13 140.2(3) . . . yes
Cl8 Zn8 N14 107.9(3) . . . yes
O31 Zn8 N13 86.9(3) . . . yes
Cl8 Zn8 O31 118.7(2) . . . yes
O30 Zn8 N14 85.3(3) . . . yes
Cl8 Zn8 N13 107.8(3) . . . yes
Cl8 Zn8 O30 111.96(19) . . . yes
Cl9 Zn9 Cl10 107.2(3) . . . yes
Cl10 Zn9 Cl12 110.9(4) . . . yes
Cl11 Zn9 Cl12 114.8(3) . . . yes
Cl9 Zn9 Cl12 107.0(3) . . . yes
Cl10 Zn9 Cl11 111.2(3) . . . yes
Cl9 Zn9 Cl11 105.4(3) . . . yes
Cl13 Zn10 Cl15 108.0(4) . . . yes
Cl13 Zn10 Cl14 108.0(3) . . . yes
Cl14 Zn10 Cl16 116.8(4) . . . yes
Cl14 Zn10 Cl15 107.9(4) . . . yes
Cl13 Zn10 Cl16 108.0(4) . . . yes
Cl15 Zn10 Cl16 107.9(3) . . . yes
Cl19 Zn11 Cl20 108.8(6) . . . yes
Cl17 Zn11 Cl19 112.7(8) . . . yes
Cl17 Zn11 Cl20 108.8(7) . . . yes
Cl18 Zn11 Cl20 108.8(6) . . . yes
Cl17 Zn11 Cl18 108.8(6) . . . yes
Cl18 Zn11 Cl19 108.9(7) . . . yes
C1 O1 C2 116.1(10) . . . yes
Dy1 O1 C2 118.1(7) . . . yes
Dy1 O1 C1 125.6(9) . . . yes
Zn2 O2 C7 128.5(6) . . . yes
Dy1 O2 Zn2 104.2(3) . . . yes
Dy1 O2 C7 126.8(6) . . . yes
Dy1 O3 Zn2 105.0(3) . . . yes
Dy1 O3 C13 124.6(7) . . . yes
Zn2 O3 C13 128.1(8) . . . yes
Dy1 O4 C18 125.3(7) . . . yes
Dy1 O4 C14 114.8(6) . . . yes
C14 O4 C18 119.9(9) . . . yes
Dy1 O5 C20 114.1(7) . . . yes
Dy1 O5 C19 127.6(7) . . . yes
C19 O5 C20 115.1(9) . . . yes
Dy1 O6 C21 121.6(7) . . . yes
Zn1 O6 C21 127.1(6) . . . yes
Dy1 O6 Zn1 107.0(3) . . . yes
Dy1 O7 Zn1 110.9(3) . . . yes
Zn1 O7 C35 121.2(7) . . . yes
Dy1 O7 C35 127.8(6) . . . yes
C34 O8 C36 115.2(10) . . . yes
Dy1 O8 C36 129.4(8) . . . yes
Dy1 O8 C34 111.8(6) . . . yes
Zn2 N1 C8 130.9(12) . . . yes
Zn2 N1 C9 111.9(9) . . . yes
C8 N1 C9 117.1(14) . . . yes
C10 N2 C11 125.7(14) . . . yes
Zn2 N2 C10 107.0(9) . . . yes
Zn2 N2 C11 127.0(11) . . . yes
Zn1 N3 C27 109.3(8) . . . yes
C26 N3 C27 122.7(11) . . . yes
Zn1 N3 C26 128.0(10) . . . yes
C28 N4 C29 121.3(12) . . . yes
Zn1 N4 C29 124.6(10) . . . yes
Zn1 N4 C28 113.9(8) . . . yes
C3 C2 C7 120.9(11) . . . no
O1 C2 C7 112.2(10) . . . yes
O1 C2 C3 126.9(11) . . . yes
C2 C3 C4 120.8(11) . . . no
C3 C4 C5 120.9(12) . . . no
C4 C5 C6 119.1(12) . . . no
C7 C6 C8 121.5(11) . . . no
C5 C6 C7 120.6(11) . . . no
C5 C6 C8 117.8(12) . . . no
O2 C7 C2 118.0(9) . . . yes
C2 C7 C6 117.5(10) . . . no
O2 C7 C6 124.5(9) . . . yes
N1 C8 C6 126.5(15) . . . yes
Dy2 O9 C38 113.2(7) . . . yes
C37 O9 C38 114.8(9) . . . yes
Dy2 O9 C37 131.1(7) . . . yes
N1 C9 C10 111.5(13) . . . yes
Dy2 O10 C39 129.8(7) . . . yes
Zn3 O10 C39 120.7(6) . . . yes
Dy2 O10 Zn3 109.5(3) . . . yes
N2 C10 C9 114.7(12) . . . yes
Dy2 O11 Zn3 108.4(4) . . . yes
Dy2 O11 C49 126.0(7) . . . yes
N2 C11 C12 127.7(15) . . . yes
Zn3 O11 C49 125.4(7) . . . yes
Dy2 O12 C50 116.3(7) . . . yes
C11 C12 C13 123.6(11) . . . no
Dy2 O12 C54 121.0(8) . . . yes
C50 O12 C54 122.2(11) . . . yes
C13 C12 C17 118.6(12) . . . no
C11 C12 C17 117.7(12) . . . no
Dy2 O13 C55 123.8(7) . . . yes
O3 C13 C12 125.2(11) . . . yes
O3 C13 C14 113.8(11) . . . yes
C12 C13 C14 120.9(10) . . . no
C55 O13 C56 116.6(8) . . . yes
Dy2 O13 C56 117.6(6) . . . yes
C13 C14 C15 119.3(11) . . . no
O4 C14 C13 115.6(9) . . . yes
Dy2 O14 Zn4 103.7(2) . . . yes
Dy2 O14 C57 129.4(7) . . . yes
Zn4 O14 C57 126.6(7) . . . yes
O4 C14 C15 124.9(10) . . . yes
Zn4 O15 C67 127.8(7) . . . yes
Dy2 O15 C67 126.9(7) . . . yes
C14 C15 C16 120.7(13) . . . no
Dy2 O15 Zn4 104.9(4) . . . yes
Dy2 O16 C72 126.1(7) . . . yes
C15 C16 C17 118.1(13) . . . no
C68 O16 C72 118.1(9) . . . yes
Dy2 O16 C68 115.8(6) . . . yes
C12 C17 C16 122.2(13) . . . no
C21 C20 C25 119.4(11) . . . no
O5 C20 C25 126.6(11) . . . yes
O5 C20 C21 113.8(10) . . . yes
O6 C21 C22 124.2(10) . . . yes
O6 C21 C20 115.8(10) . . . yes
C20 C21 C22 119.9(10) . . . no
C23 C22 C26 118.6(11) . . . no
C21 C22 C23 118.3(12) . . . no
C21 C22 C26 122.7(11) . . . no
C22 C23 C24 122.8(13) . . . no
C23 C24 C25 118.9(13) . . . no
C20 C25 C24 120.5(12) . . . no
N3 C26 C22 127.7(12) . . . yes
N3 C27 C28 108.6(11) . . . yes
N4 C28 C27 110.2(11) . . . yes
N4 C29 C30 126.0(13) . . . yes
C31 C30 C35 116.8(11) . . . no
C29 C30 C35 122.7(11) . . . no
C29 C30 C31 120.3(11) . . . no
C30 C31 C32 120.4(12) . . . no
C31 C32 C33 123.0(12) . . . no
C32 C33 C34 117.6(11) . . . no
C33 C34 C35 120.8(11) . . . no
O8 C34 C33 126.3(11) . . . yes
O8 C34 C35 112.9(10) . . . yes
O7 C35 C34 117.6(10) . . . yes
O7 C35 C30 121.1(10) . . . yes
C30 C35 C34 121.3(11) . . . no
H1B C1 H1C 110.00 . . . no
H1A C1 H1C 110.00 . . . no
O1 C1 H1C 109.00 . . . no
H1A C1 H1B 109.00 . . . no
O1 C1 H1A 109.00 . . . no
O1 C1 H1B 109.00 . . . no
Dy2 O2W H2WB 115.00 . . . no
H2WA O2W H2WB 102.00 . . . no
Dy2 O2W H2WA 116.00 . . . no
C4 C3 H3 120.00 . . . no
C2 C3 H3 120.00 . . . no
C3 C4 H4 120.00 . . . no
C5 C4 H4 119.00 . . . no
C4 C5 H5 121.00 . . . no
C6 C5 H5 120.00 . . . no
Zn3 N5 C44 124.7(8) . . . yes
Zn3 N5 C45 113.2(9) . . . yes
C44 N5 C45 121.8(11) . . . yes
Zn3 N6 C47 126.4(9) . . . yes
Zn3 N6 C46 107.6(10) . . . yes
C46 N6 C47 126.0(13) . . . yes
Zn4 N7 C63 108.1(8) . . . yes
Zn4 N7 C62 129.3(8) . . . yes
C62 N7 C63 122.4(10) . . . yes
N1 C8 H8 117.00 . . . no
C64 N8 C65 123.1(12) . . . yes
Zn4 N8 C64 111.4(9) . . . yes
Zn4 N8 C65 125.0(9) . . . yes
C6 C8 H8 117.00 . . . no
C10 C9 H9A 109.00 . . . no
N1 C9 H9B 109.00 . . . no
N1 C9 H9A 109.00 . . . no
H9A C9 H9B 108.00 . . . no
C10 C9 H9B 109.00 . . . no
C9 C10 H10J 109.00 . . . no
H10I C10 H10J 108.00 . . . no
C9 C10 H10I 109.00 . . . no
N2 C10 H10J 109.00 . . . no
N2 C10 H10I 108.00 . . . no
N2 C11 H11 116.00 . . . no
C12 C11 H11 116.00 . . . no
C16 C15 H15 120.00 . . . no
C14 C15 H15 120.00 . . . no
C17 C16 H16 121.00 . . . no
C15 C16 H16 121.00 . . . no
C12 C17 H17 119.00 . . . no
C16 C17 H17 119.00 . . . no
H18A C18 H18B 109.00 . . . no
O4 C18 H18C 109.00 . . . no
O4 C18 H18B 109.00 . . . no
H18A C18 H18C 109.00 . . . no
O4 C18 H18A 110.00 . . . no
H18B C18 H18C 110.00 . . . no
H19A C19 H19B 109.00 . . . no
O5 C19 H19B 109.00 . . . no
O5 C19 H19C 109.00 . . . no
O5 C19 H19A 109.00 . . . no
H19A C19 H19C 110.00 . . . no
H19B C19 H19C 110.00 . . . no
C22 C23 H23 119.00 . . . no
C24 C23 H23 119.00 . . . no
C23 C24 H24 121.00 . . . no
C25 C24 H24 120.00 . . . no
C24 C25 H25 120.00 . . . no
C20 C25 H25 120.00 . . . no
C22 C26 H26 116.00 . . . no
N3 C26 H26 116.00 . . . no
C28 C27 H27A 110.00 . . . no
C28 C27 H27B 110.00 . . . no
N3 C27 H27B 110.00 . . . no
H27A C27 H27B 108.00 . . . no
N3 C27 H27A 110.00 . . . no
C27 C28 H28B 110.00 . . . no
N4 C28 H28A 110.00 . . . no
H28A C28 H28B 108.00 . . . no
N4 C28 H28B 110.00 . . . no
C27 C28 H28A 110.00 . . . no
C30 C29 H29 117.00 . . . no
N4 C29 H29 117.00 . . . no
C32 C31 H31 120.00 . . . no
C30 C31 H31 120.00 . . . no
C33 C32 H32 118.00 . . . no
C31 C32 H32 119.00 . . . no
C32 C33 H33 121.00 . . . no
C34 C33 H33 121.00 . . . no
O8 C36 H36A 110.00 . . . no
H36B C36 H36C 109.00 . . . no
H36A C36 H36B 109.00 . . . no
H36A C36 H36C 109.00 . . . no
O8 C36 H36C 110.00 . . . no
O8 C36 H36B 110.00 . . . no
Dy3 O17 C74 116.0(6) . . . yes
Dy3 O17 C73 126.5(7) . . . yes
C73 O17 C74 116.2(9) . . . yes
Dy3 O18 C75 125.0(6) . . . yes
Zn5 O18 C75 124.9(6) . . . yes
Dy3 O18 Zn5 108.3(3) . . . yes
Zn5 O19 C85 119.5(6) . . . yes
Dy3 O19 Zn5 109.5(3) . . . yes
Dy3 O19 C85 130.5(6) . . . yes
C86 O20 C90 116.6(9) . . . yes
Dy3 O20 C90 125.9(7) . . . yes
Dy3 O20 C86 111.7(6) . . . yes
C91 O21 C92 116.3(8) . . . yes
Dy3 O21 C91 123.2(7) . . . yes
Dy3 O21 C92 118.3(6) . . . yes
Dy3 O22 Zn6 103.7(2) . . . yes
Zn6 O22 C93 126.8(6) . . . yes
Dy3 O22 C93 127.3(6) . . . yes
Dy3 O23 Zn6 105.9(3) . . . yes
Dy3 O23 C107 128.1(7) . . . yes
Zn6 O23 C107 125.9(7) . . . yes
Dy3 O24 C106 117.2(7) . . . yes
Dy3 O24 C108 124.6(7) . . . yes
C106 O24 C108 118.3(10) . . . yes
C39 C38 C43 121.3(11) . . . no
O9 C38 C39 112.7(11) . . . yes
O9 C38 C43 126.0(11) . . . yes
C38 C39 C40 117.8(11) . . . no
O10 C39 C40 125.0(10) . . . yes
O10 C39 C38 117.1(10) . . . yes
C39 C40 C44 121.3(11) . . . no
C41 C40 C44 119.0(10) . . . no
C39 C40 C41 119.7(11) . . . no
C40 C41 C42 118.8(12) . . . no
C41 C42 C43 124.0(14) . . . no
C38 C43 C42 118.3(13) . . . no
N5 C44 C40 125.5(11) . . . yes
N5 C45 C46 110.7(14) . . . yes
N6 C46 C45 109.6(13) . . . yes
N6 C47 C48 124.5(13) . . . yes
C47 C48 C53 117.4(13) . . . no
C47 C48 C49 125.7(12) . . . no
C49 C48 C53 116.9(12) . . . no
O11 C49 C50 118.3(11) . . . yes
C48 C49 C50 117.9(12) . . . no
O11 C49 C48 123.5(11) . . . yes
O12 C50 C49 113.2(11) . . . yes
O12 C50 C51 121.8(13) . . . yes
C49 C50 C51 125.0(13) . . . no
C50 C51 C52 117.8(15) . . . no
C51 C52 C53 117.8(16) . . . no
C48 C53 C52 124.1(15) . . . no
O13 C56 C61 123.3(10) . . . yes
C57 C56 C61 122.6(10) . . . no
O13 C56 C57 114.1(8) . . . yes
C56 C57 C58 118.9(8) . . . no
O14 C57 C56 116.5(9) . . . yes
O14 C57 C58 124.6(10) . . . yes
C57 C58 C62 124.5(9) . . . no
C57 C58 C59 118.1(11) . . . no
C59 C58 C62 117.1(10) . . . no
C58 C59 C60 122.9(12) . . . no
C59 C60 C61 120.1(11) . . . no
C56 C61 C60 117.5(11) . . . no
N7 C62 C58 124.3(10) . . . yes
N7 C63 C64 109.2(12) . . . yes
N8 C64 C63 110.7(12) . . . yes
N8 C65 C66 128.5(12) . . . yes
C67 C66 C71 118.8(12) . . . no
C65 C66 C71 119.0(12) . . . no
C65 C66 C67 122.2(12) . . . no
O15 C67 C66 125.8(11) . . . yes
O15 C67 C68 114.7(11) . . . yes
C66 C67 C68 119.5(12) . . . no
C67 C68 C69 120.6(12) . . . no
O16 C68 C69 124.2(12) . . . yes
O16 C68 C67 115.2(10) . . . yes
C68 C69 C70 116.7(13) . . . no
C69 C70 C71 119.4(15) . . . no
C66 C71 C70 124.8(14) . . . no
Dy3 O3W H3WB 114.00 . . . no
Dy3 O3W H3WA 114.00 . . . no
H3WA O3W H3WB 105.00 . . . no
Zn5 N9 C80 128.6(8) . . . yes
C80 N9 C81 122.8(11) . . . yes
Zn5 N9 C81 108.5(8) . . . yes
Zn5 N10 C82 113.0(9) . . . yes
Zn5 N10 C83 124.8(9) . . . yes
C82 N10 C83 121.8(11) . . . yes
C98 N11 C99 122.7(10) . . . yes
Zn6 N11 C98 130.2(9) . . . yes
Zn6 N11 C99 106.0(7) . . . yes
Zn6 N12 C100 114.2(9) . . . yes
Zn6 N12 C101 123.0(10) . . . yes
C100 N12 C101 122.3(12) . . . yes
O9 C37 H37B 110.00 . . . no
O9 C37 H37A 110.00 . . . no
H37A C37 H37C 109.00 . . . no
O9 C37 H37C 110.00 . . . no
H37A C37 H37B 109.00 . . . no
H37B C37 H37C 110.00 . . . no
C42 C41 H41 121.00 . . . no
C40 C41 H41 121.00 . . . no
C41 C42 H42 118.00 . . . no
C43 C42 H42 118.00 . . . no
C42 C43 H43 121.00 . . . no
C38 C43 H43 121.00 . . . no
C40 C44 H44 117.00 . . . no
N5 C44 H44 117.00 . . . no
C46 C45 H45B 110.00 . . . no
H45A C45 H45B 108.00 . . . no
N5 C45 H45B 110.00 . . . no
C46 C45 H45A 109.00 . . . no
N5 C45 H45A 109.00 . . . no
C45 C46 H46A 110.00 . . . no
C45 C46 H46B 110.00 . . . no
N6 C46 H46B 110.00 . . . no
H46A C46 H46B 108.00 . . . no
N6 C46 H46A 110.00 . . . no
N6 C47 H47 118.00 . . . no
C48 C47 H47 118.00 . . . no
C52 C51 H51 121.00 . . . no
C50 C51 H51 121.00 . . . no
C51 C52 H52 121.00 . . . no
C53 C52 H52 121.00 . . . no
C48 C53 H53 118.00 . . . no
C52 C53 H53 118.00 . . . no
O12 C54 H54B 109.00 . . . no
O12 C54 H54A 109.00 . . . no
O12 C54 H54C 109.00 . . . no
H54B C54 H54C 109.00 . . . no
H54A C54 H54B 110.00 . . . no
H54A C54 H54C 110.00 . . . no
O13 C55 H55B 109.00 . . . no
O13 C55 H55A 110.00 . . . no
H55B C55 H55C 109.00 . . . no
H55A C55 H55B 109.00 . . . no
H55A C55 H55C 110.00 . . . no
O13 C55 H55C 110.00 . . . no
C58 C59 H59 118.00 . . . no
C60 C59 H59 119.00 . . . no
C61 C60 H60 120.00 . . . no
C59 C60 H60 120.00 . . . no
C56 C61 H61 121.00 . . . no
C60 C61 H61 121.00 . . . no
N7 C62 H62 118.00 . . . no
C58 C62 H62 118.00 . . . no
C64 C63 H63B 110.00 . . . no
N7 C63 H63A 110.00 . . . no
N7 C63 H63B 110.00 . . . no
H63A C63 H63B 108.00 . . . no
C64 C63 H63A 110.00 . . . no
N8 C64 H64B 110.00 . . . no
C63 C64 H64B 109.00 . . . no
H64A C64 H64B 108.00 . . . no
C63 C64 H64A 109.00 . . . no
N8 C64 H64A 110.00 . . . no
N8 C65 H65 116.00 . . . no
C66 C65 H65 116.00 . . . no
C68 C69 H69 122.00 . . . no
C70 C69 H69 122.00 . . . no
C69 C70 H70 120.00 . . . no
C71 C70 H70 120.00 . . . no
C70 C71 H71 118.00 . . . no
C66 C71 H71 118.00 . . . no
O16 C72 H72A 109.00 . . . no
H72A C72 H72B 109.00 . . . no
H72A C72 H72C 110.00 . . . no
H72B C72 H72C 110.00 . . . no
O16 C72 H72B 109.00 . . . no
O16 C72 H72C 109.00 . . . no
C127 O25 C128 116.8(8) . . . yes
Dy4 O25 C128 119.1(5) . . . yes
Dy4 O25 C127 123.4(7) . . . yes
Zn7 O26 C129 127.2(6) . . . yes
Dy4 O26 C129 128.8(5) . . . yes
Dy4 O26 Zn7 103.8(3) . . . yes
Dy4 O27 Zn7 104.3(3) . . . yes
Dy4 O27 C139 128.4(7) . . . yes
Zn7 O27 C139 121.3(6) . . . yes
Dy4 O28 C144 128.8(8) . . . yes
Dy4 O28 C140 118.2(6) . . . yes
C140 O28 C144 112.4(9) . . . yes
Dy4 O29 C122 107.7(6) . . . yes
Dy4 O29 C126 125.5(7) . . . yes
C122 O29 C126 117.4(9) . . . yes
Zn8 O30 C121 123.1(6) . . . yes
Dy4 O30 C121 127.2(5) . . . yes
Dy4 O30 Zn8 109.5(3) . . . yes
Dy4 O31 Zn8 107.9(3) . . . yes
Zn8 O31 C115 126.9(6) . . . yes
Dy4 O31 C115 121.0(6) . . . yes
Dy4 O32 C110 111.5(7) . . . yes
C109 O32 C110 117.2(9) . . . yes
Dy4 O32 C109 125.1(7) . . . yes
O17 C74 C75 112.1(10) . . . yes
O17 C74 C79 125.8(11) . . . yes
C75 C74 C79 122.0(12) . . . no
C74 C75 C76 117.7(11) . . . no
O18 C75 C76 125.5(10) . . . yes
O18 C75 C74 116.8(10) . . . yes
C77 C76 C80 117.2(11) . . . no
C75 C76 C80 124.0(11) . . . no
C75 C76 C77 118.4(11) . . . no
C76 C77 C78 122.4(13) . . . no
C77 C78 C79 119.7(14) . . . no
C74 C79 C78 119.9(12) . . . no
N9 C80 C76 124.2(11) . . . yes
N9 C81 C82 110.1(13) . . . yes
N10 C82 C81 108.9(13) . . . yes
N10 C83 C84 124.3(12) . . . yes
C83 C84 C85 123.4(12) . . . no
C83 C84 C89 117.3(12) . . . no
C85 C84 C89 119.3(11) . . . no
O19 C85 C84 124.1(10) . . . yes
C84 C85 C86 118.8(11) . . . no
O19 C85 C86 117.1(9) . . . yes
C85 C86 C87 120.5(11) . . . no
O20 C86 C87 125.3(11) . . . yes
O20 C86 C85 114.2(10) . . . yes
C86 C87 C88 119.5(12) . . . no
C87 C88 C89 119.6(13) . . . no
C84 C89 C88 122.3(13) . . . no
O21 C92 C93 114.0(8) . . . yes
O21 C92 C97 122.7(10) . . . yes
C93 C92 C97 123.4(10) . . . no
O22 C93 C94 126.6(9) . . . yes
C92 C93 C94 116.6(9) . . . no
O22 C93 C92 116.8(8) . . . yes
C93 C94 C98 124.7(9) . . . no
C93 C94 C95 122.5(11) . . . no
C95 C94 C98 112.4(10) . . . no
C94 C95 C96 119.8(11) . . . no
C95 C96 C97 121.4(11) . . . no
C92 C97 C96 116.3(11) . . . no
N11 C98 C94 123.7(11) . . . yes
N11 C99 C100 106.0(11) . . . yes
N12 C100 C99 110.1(11) . . . yes
N12 C101 C102 126.3(17) . . . yes
C101 C102 C103 119.9(19) . . . no
C101 C102 C107 127(2) . . . no
C103 C102 C107 113.4(17) . . . no
C102 C103 C104 124.1(19) . . . no
C103 C104 C105 119(2) . . . no
C104 C105 C106 121.1(19) . . . no
O24 C106 C107 113.7(12) . . . yes
O24 C106 C105 124.9(14) . . . yes
C105 C106 C107 121.5(15) . . . no
C102 C107 C106 120.9(15) . . . no
O23 C107 C102 122.2(13) . . . yes
O23 C107 C106 116.8(11) . . . yes
Dy4 O4W H4WB 109.00 . . . no
Dy4 O4W H4WA 109.00 . . . no
H4WA O4W H4WB 104.00 . . . no
C116 N13 C117 122.9(11) . . . yes
Zn8 N13 C116 129.5(9) . . . yes
Zn8 N13 C117 107.6(8) . . . yes
Zn8 N14 C119 125.7(9) . . . yes
Zn8 N14 C118 114.5(8) . . . yes
C118 N14 C119 119.8(11) . . . yes
C134 N15 C135 123.9(11) . . . yes
Zn7 N15 C135 105.4(8) . . . yes
Zn7 N15 C134 130.7(9) . . . yes
C136 N16 C137 124.0(11) . . . yes
Zn7 N16 C136 109.7(8) . . . yes
Zn7 N16 C137 126.1(9) . . . yes
H73B C73 H73C 109.00 . . . no
O17 C73 H73A 110.00 . . . no
O17 C73 H73C 110.00 . . . no
H73A C73 H73B 109.00 . . . no
H73A C73 H73C 109.00 . . . no
O17 C73 H73B 110.00 . . . no
C76 C77 H77 119.00 . . . no
C78 C77 H77 119.00 . . . no
C77 C78 H78 120.00 . . . no
C79 C78 H78 120.00 . . . no
C78 C79 H79 120.00 . . . no
C74 C79 H79 120.00 . . . no
C76 C80 H80 118.00 . . . no
N9 C80 H80 118.00 . . . no
C82 C81 H81A 110.00 . . . no
C82 C81 H81B 110.00 . . . no
N9 C81 H81A 110.00 . . . no
N9 C81 H81B 110.00 . . . no
H81A C81 H81B 108.00 . . . no
H82A C82 H82B 108.00 . . . no
C81 C82 H82A 110.00 . . . no
N10 C82 H82B 110.00 . . . no
C81 C82 H82B 110.00 . . . no
N10 C82 H82A 110.00 . . . no
N10 C83 H83 118.00 . . . no
C84 C83 H83 118.00 . . . no
C88 C87 H87 120.00 . . . no
C86 C87 H87 120.00 . . . no
C89 C88 H88 120.00 . . . no
C87 C88 H88 120.00 . . . no
C88 C89 H89 119.00 . . . no
C84 C89 H89 119.00 . . . no
H90A C90 H90C 109.00 . . . no
H90A C90 H90B 110.00 . . . no
O20 C90 H90B 109.00 . . . no
H90B C90 H90C 109.00 . . . no
O20 C90 H90A 110.00 . . . no
O20 C90 H90C 109.00 . . . no
H91B C91 H91C 109.00 . . . no
O21 C91 H91C 110.00 . . . no
H91A C91 H91B 109.00 . . . no
O21 C91 H91B 109.00 . . . no
H91A C91 H91C 110.00 . . . no
O21 C91 H91A 109.00 . . . no
C96 C95 H95 120.00 . . . no
C94 C95 H95 120.00 . . . no
C95 C96 H96 119.00 . . . no
C97 C96 H96 119.00 . . . no
C92 C97 H97 122.00 . . . no
C96 C97 H97 122.00 . . . no
C94 C98 H98 118.00 . . . no
N11 C98 H98 118.00 . . . no
N11 C99 H99B 111.00 . . . no
C100 C99 H99B 110.00 . . . no
H99A C99 H99B 109.00 . . . no
C100 C99 H99A 110.00 . . . no
N11 C99 H99A 111.00 . . . no
C99 C100 H10B 110.00 . . . no
N12 C100 H10A 110.00 . . . no
H10A C100 H10B 108.00 . . . no
C99 C100 H10A 110.00 . . . no
N12 C100 H10B 110.00 . . . no
N12 C101 H101 117.00 . . . no
C102 C101 H101 117.00 . . . no
C104 C103 H103 118.00 . . . no
C102 C103 H103 118.00 . . . no
C103 C104 H104 121.00 . . . no
C105 C104 H104 121.00 . . . no
C104 C105 H105 119.00 . . . no
C106 C105 H105 120.00 . . . no
H10D C108 H10E 109.00 . . . no
H10C C108 H10E 110.00 . . . no
H10C C108 H10D 109.00 . . . no
O24 C108 H10C 110.00 . . . no
O24 C108 H10D 109.00 . . . no
O24 C108 H10E 109.00 . . . no
O32 C110 C111 125.2(10) . . . yes
O32 C110 C115 114.7(10) . . . yes
C111 C110 C115 119.9(10) . . . no
C110 C111 C112 118.7(12) . . . no
C111 C112 C113 121.2(14) . . . no
C112 C113 C114 122.6(13) . . . no
C113 C114 C115 118.2(12) . . . no
C113 C114 C116 118.1(11) . . . no
C115 C114 C116 123.2(11) . . . no
C110 C115 C114 119.4(10) . . . no
O31 C115 C110 115.0(9) . . . yes
O31 C115 C114 125.5(10) . . . yes
N13 C116 C114 125.9(11) . . . yes
N13 C117 C118 108.0(10) . . . yes
N14 C118 C117 107.7(10) . . . yes
N14 C119 C120 123.9(12) . . . yes
C119 C120 C125 114.3(11) . . . no
C119 C120 C121 124.9(11) . . . no
C121 C120 C125 120.6(11) . . . no
O30 C121 C120 123.7(9) . . . yes
O30 C121 C122 116.6(9) . . . yes
C120 C121 C122 119.6(10) . . . no
O29 C122 C121 114.7(9) . . . yes
O29 C122 C123 123.7(10) . . . yes
C121 C122 C123 121.6(11) . . . no
C122 C123 C124 117.6(11) . . . no
C123 C124 C125 121.5(12) . . . no
C120 C125 C124 119.1(12) . . . no
C129 C128 C133 122.8(10) . . . no
O25 C128 C129 111.4(8) . . . yes
O25 C128 C133 125.8(9) . . . yes
C128 C129 C130 117.1(9) . . . no
O26 C129 C130 125.8(8) . . . yes
O26 C129 C128 117.1(9) . . . yes
C129 C130 C134 122.5(9) . . . no
C129 C130 C131 119.4(9) . . . no
C131 C130 C134 117.9(10) . . . no
C130 C131 C132 120.6(10) . . . no
C131 C132 C133 121.3(11) . . . no
C128 C133 C132 118.7(10) . . . no
N15 C134 C130 125.9(12) . . . yes
N15 C135 C136 108.5(10) . . . yes
N16 C136 C135 112.7(12) . . . yes
N16 C137 C138 123.3(12) . . . yes
C139 C138 C143 116.9(11) . . . no
C137 C138 C143 118.7(11) . . . no
C137 C138 C139 124.3(10) . . . no
O27 C139 C138 122.6(10) . . . yes
C138 C139 C140 119.7(9) . . . no
O27 C139 C140 117.7(9) . . . yes
C139 C140 C141 122.8(10) . . . no
O28 C140 C141 125.1(10) . . . yes
O28 C140 C139 112.1(9) . . . yes
C140 C141 C142 116.6(11) . . . no
C141 C142 C143 121.3(12) . . . no
C138 C143 C142 122.1(13) . . . no
O32 C109 H10H 109.00 . . . no
O32 C109 H10G 109.00 . . . no
H10G C109 H10H 109.00 . . . no
H10F C109 H10G 109.00 . . . no
H10F C109 H10H 110.00 . . . no
O32 C109 H10F 109.00 . . . no
C110 C111 H111 121.00 . . . no
C112 C111 H111 121.00 . . . no
C113 C112 H112 119.00 . . . no
C111 C112 H112 119.00 . . . no
C112 C113 H113 119.00 . . . no
C114 C113 H113 119.00 . . . no
N13 C116 H116 117.00 . . . no
C114 C116 H116 117.00 . . . no
N13 C117 H11B 110.00 . . . no
C118 C117 H11A 110.00 . . . no
C118 C117 H11B 110.00 . . . no
H11A C117 H11B 108.00 . . . no
N13 C117 H11A 110.00 . . . no
N14 C118 H11C 110.00 . . . no
N14 C118 H11D 110.00 . . . no
C117 C118 H11D 110.00 . . . no
H11C C118 H11D 108.00 . . . no
C117 C118 H11C 110.00 . . . no
N14 C119 H119 118.00 . . . no
C120 C119 H119 118.00 . . . no
C122 C123 H123 121.00 . . . no
C124 C123 H123 121.00 . . . no
C125 C124 H124 119.00 . . . no
C123 C124 H124 119.00 . . . no
C124 C125 H125 120.00 . . . no
C120 C125 H125 120.00 . . . no
O29 C126 H12C 109.00 . . . no
O29 C126 H12B 109.00 . . . no
H12B C126 H12C 110.00 . . . no
H12A C126 H12B 110.00 . . . no
H12A C126 H12C 110.00 . . . no
O29 C126 H12A 109.00 . . . no
H12D C127 H12E 110.00 . . . no
H12D C127 H12F 110.00 . . . no
H12E C127 H12F 110.00 . . . no
O25 C127 H12F 109.00 . . . no
O25 C127 H12D 109.00 . . . no
O25 C127 H12E 109.00 . . . no
C130 C131 H131 120.00 . . . no
C132 C131 H131 120.00 . . . no
C131 C132 H132 119.00 . . . no
C133 C132 H132 119.00 . . . no
C132 C133 H133 120.00 . . . no
C128 C133 H133 121.00 . . . no
N15 C134 H134 117.00 . . . no
C130 C134 H134 117.00 . . . no
N15 C135 H13A 110.00 . . . no
C136 C135 H13B 110.00 . . . no
H13A C135 H13B 108.00 . . . no
N15 C135 H13B 110.00 . . . no
C136 C135 H13A 110.00 . . . no
C135 C136 H13C 109.00 . . . no
N16 C136 H13C 109.00 . . . no
N16 C136 H13D 109.00 . . . no
H13C C136 H13D 108.00 . . . no
C135 C136 H13D 109.00 . . . no
N16 C137 H137 118.00 . . . no
C138 C137 H137 118.00 . . . no
C142 C141 H141 122.00 . . . no
C140 C141 H141 122.00 . . . no
C141 C142 H142 119.00 . . . no
C143 C142 H142 119.00 . . . no
C138 C143 H143 119.00 . . . no
C142 C143 H143 119.00 . . . no
O28 C144 H14C 109.00 . . . no
H14A C144 H14C 109.00 . . . no
H14B C144 H14C 110.00 . . . no
H14A C144 H14B 110.00 . . . no
O28 C144 H14A 110.00 . . . no
O28 C144 H14B 109.00 . . . no
H5WA O5W H5WB 105.00 . . . no

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1W Dy1 O1 C1 -91.5(11) . . . . no
O1W Dy1 O1 C2 83.8(8) . . . . no
O2 Dy1 O1 C1 -171.8(11) . . . . no
O2 Dy1 O1 C2 3.5(7) . . . . no
O3 Dy1 O1 C1 164.2(10) . . . . no
O3 Dy1 O1 C2 -20.5(9) . . . . no
O4 Dy1 O1 C1 66.6(12) . . . . no
O4 Dy1 O1 C2 -118.1(8) . . . . no
O5 Dy1 O1 C1 104.6(11) . . . . no
O5 Dy1 O1 C2 -80.1(8) . . . . no
O6 Dy1 O1 C1 41.3(11) . . . . no
O6 Dy1 O1 C2 -143.4(8) . . . . no
O7 Dy1 O1 C1 -25.5(11) . . . . no
O7 Dy1 O1 C2 149.8(8) . . . . no
O8 Dy1 O1 C1 -86.7(11) . . . . no
O8 Dy1 O1 C2 88.6(8) . . . . no
O1 Dy1 O2 Zn2 -179.0(4) . . . . no
O1 Dy1 O2 C7 -6.4(7) . . . . no
O1W Dy1 O2 Zn2 47.8(4) . . . . no
O1W Dy1 O2 C7 -139.7(8) . . . . no
O3 Dy1 O2 Zn2 -19.7(3) . . . . no
O3 Dy1 O2 C7 152.9(9) . . . . no
O4 Dy1 O2 Zn2 -31.7(4) . . . . no
O4 Dy1 O2 C7 140.9(8) . . . . no
O5 Dy1 O2 Zn2 -95.8(3) . . . . no
O5 Dy1 O2 C7 76.8(8) . . . . no
O6 Dy1 O2 Zn2 -131.3(3) . . . . no
O6 Dy1 O2 C7 41.2(9) . . . . no
O7 Dy1 O2 Zn2 129.9(3) . . . . no
O7 Dy1 O2 C7 -57.5(9) . . . . no
O8 Dy1 O2 Zn2 111.8(3) . . . . no
O8 Dy1 O2 C7 -75.6(8) . . . . no
O1 Dy1 O3 Zn2 44.4(5) . . . . no
O1 Dy1 O3 C13 -119.5(9) . . . . no
O1W Dy1 O3 Zn2 -88.7(4) . . . . no
O1W Dy1 O3 C13 107.4(10) . . . . no
O2 Dy1 O3 Zn2 20.9(3) . . . . no
O2 Dy1 O3 C13 -143.1(10) . . . . no
O4 Dy1 O3 Zn2 -169.8(5) . . . . no
O4 Dy1 O3 C13 26.2(9) . . . . no
O5 Dy1 O3 Zn2 106.7(4) . . . . no
O5 Dy1 O3 C13 -57.3(9) . . . . no
O6 Dy1 O3 Zn2 148.2(3) . . . . no
O6 Dy1 O3 C13 -15.8(10) . . . . no
O7 Dy1 O3 Zn2 -117.4(5) . . . . no
O7 Dy1 O3 C13 78.6(11) . . . . no
O8 Dy1 O3 Zn2 -35.3(5) . . . . no
O8 Dy1 O3 C13 160.7(9) . . . . no
O1 Dy1 O4 C14 92.4(8) . . . . no
O1 Dy1 O4 C18 -89.1(10) . . . . no
O1W Dy1 O4 C14 -103.8(7) . . . . no
O1W Dy1 O4 C18 74.7(9) . . . . no
O2 Dy1 O4 C14 -11.5(8) . . . . no
O2 Dy1 O4 C18 167.0(8) . . . . no
O3 Dy1 O4 C14 -24.0(6) . . . . no
O3 Dy1 O4 C18 154.6(10) . . . . no
O5 Dy1 O4 C14 53.9(7) . . . . no
O5 Dy1 O4 C18 -127.5(9) . . . . no
O6 Dy1 O4 C14 118.9(7) . . . . no
O6 Dy1 O4 C18 -62.5(9) . . . . no
O7 Dy1 O4 C14 -178.6(7) . . . . no
O7 Dy1 O4 C18 0.0(9) . . . . no
O8 Dy1 O4 C14 -127.3(6) . . . . no
O8 Dy1 O4 C18 51.3(11) . . . . no
O1 Dy1 O5 C19 88.5(9) . . . . no
O1 Dy1 O5 C20 -113.0(7) . . . . no
O1W Dy1 O5 C19 -71.3(10) . . . . no
O1W Dy1 O5 C20 87.2(9) . . . . no
O2 Dy1 O5 C19 22.9(9) . . . . no
O2 Dy1 O5 C20 -178.6(8) . . . . no
O3 Dy1 O5 C19 -45.5(9) . . . . no
O3 Dy1 O5 C20 113.0(8) . . . . no
O4 Dy1 O5 C19 -110.1(9) . . . . no
O4 Dy1 O5 C20 48.5(7) . . . . no
O6 Dy1 O5 C19 174.2(9) . . . . no
O6 Dy1 O5 C20 -27.3(7) . . . . no
O7 Dy1 O5 C19 162.9(8) . . . . no
O7 Dy1 O5 C20 -38.6(8) . . . . no
O8 Dy1 O5 C19 71.2(10) . . . . no
O8 Dy1 O5 C20 -130.2(7) . . . . no
O1 Dy1 O6 Zn1 -88.8(3) . . . . no
O1 Dy1 O6 C21 113.1(8) . . . . no
O1W Dy1 O6 Zn1 50.0(5) . . . . no
O1W Dy1 O6 C21 -108.2(8) . . . . no
O2 Dy1 O6 Zn1 -131.1(4) . . . . no
O2 Dy1 O6 C21 70.7(8) . . . . no
O3 Dy1 O6 Zn1 143.0(3) . . . . no
O3 Dy1 O6 C21 -15.2(9) . . . . no
O4 Dy1 O6 Zn1 104.4(4) . . . . no
O4 Dy1 O6 C21 -53.8(7) . . . . no
O5 Dy1 O6 Zn1 -171.3(4) . . . . no
O5 Dy1 O6 C21 30.5(7) . . . . no
O7 Dy1 O6 Zn1 -1.0(3) . . . . no
O7 Dy1 O6 C21 -159.2(8) . . . . no
O8 Dy1 O6 Zn1 -33.5(4) . . . . no
O8 Dy1 O6 C21 168.3(7) . . . . no
O1 Dy1 O7 Zn1 84.1(4) . . . . no
O1 Dy1 O7 C35 -91.8(8) . . . . no
O1W Dy1 O7 Zn1 -138.8(4) . . . . no
O1W Dy1 O7 C35 45.3(8) . . . . no
O2 Dy1 O7 Zn1 128.9(3) . . . . no
O2 Dy1 O7 C35 -46.9(9) . . . . no
O3 Dy1 O7 Zn1 -110.4(5) . . . . no
O3 Dy1 O7 C35 73.7(10) . . . . no
O4 Dy1 O7 Zn1 -65.6(4) . . . . no
O4 Dy1 O7 C35 118.5(8) . . . . no
O5 Dy1 O7 Zn1 12.1(5) . . . . no
O5 Dy1 O7 C35 -163.8(7) . . . . no
O6 Dy1 O7 Zn1 1.1(3) . . . . no
O6 Dy1 O7 C35 -174.8(9) . . . . no
O8 Dy1 O7 Zn1 149.0(5) . . . . no
O8 Dy1 O7 C35 -26.9(8) . . . . no
O1 Dy1 O8 C34 119.1(7) . . . . no
O1 Dy1 O8 C36 -83.6(10) . . . . no
O1W Dy1 O8 C34 -64.7(7) . . . . no
O1W Dy1 O8 C36 92.6(10) . . . . no
O2 Dy1 O8 C34 -172.8(7) . . . . no
O2 Dy1 O8 C36 -15.6(9) . . . . no
O3 Dy1 O8 C34 -120.9(7) . . . . no
O3 Dy1 O8 C36 36.4(10) . . . . no
O4 Dy1 O8 C34 -40.2(9) . . . . no
O4 Dy1 O8 C36 117.0(10) . . . . no
O5 Dy1 O8 C34 137.8(7) . . . . no
O5 Dy1 O8 C36 -65.0(11) . . . . no
O6 Dy1 O8 C34 55.7(8) . . . . no
O6 Dy1 O8 C36 -147.1(9) . . . . no
O7 Dy1 O8 C34 21.7(7) . . . . no
O7 Dy1 O8 C36 179.0(10) . . . . no
O15 Dy2 O13 C56 33.9(8) . . . . no
O16 Dy2 O13 C55 -42.6(11) . . . . no
O16 Dy2 O13 C56 120.7(8) . . . . no
O2W Dy2 O14 Zn4 -45.4(4) . . . . no
O2W Dy2 O14 C57 140.6(9) . . . . no
O9 Dy2 O14 Zn4 -106.0(4) . . . . no
O9 Dy2 O14 C57 79.9(9) . . . . no
O10 Dy2 O14 Zn4 -126.8(3) . . . . no
O10 Dy2 O14 C57 59.1(10) . . . . no
O11 Dy2 O14 Zn4 133.8(3) . . . . no
O11 Dy2 O14 C57 -40.2(10) . . . . no
O12 Dy2 O14 Zn4 97.5(3) . . . . no
O12 Dy2 O14 C57 -76.5(9) . . . . no
O13 Dy2 O14 Zn4 173.0(4) . . . . no
O13 Dy2 O14 C57 -1.0(8) . . . . no
O15 Dy2 O14 Zn4 21.1(3) . . . . no
O15 Dy2 O14 C57 -153.0(10) . . . . no
O16 Dy2 O14 Zn4 30.7(5) . . . . no
O16 Dy2 O14 C57 -143.4(8) . . . . no
O2W Dy2 O15 Zn4 89.3(4) . . . . no
O2W Dy2 O15 C67 -97.3(9) . . . . no
O9 Dy2 O15 Zn4 35.9(4) . . . . no
O9 Dy2 O15 C67 -150.7(9) . . . . no
O10 Dy2 O15 Zn4 109.5(5) . . . . no
O10 Dy2 O15 C67 -77.1(11) . . . . no
O11 Dy2 O15 Zn4 -153.0(3) . . . . no
O11 Dy2 O15 C67 20.4(10) . . . . no
O12 Dy2 O15 Zn4 -111.8(4) . . . . no
O12 Dy2 O15 C67 61.6(9) . . . . no
O13 Dy2 O15 Zn4 -51.1(4) . . . . no
O13 Dy2 O15 C67 122.4(9) . . . . no
O14 Dy2 O15 Zn4 -22.0(3) . . . . no
O14 Dy2 O15 C67 151.5(10) . . . . no
O16 Dy2 O15 Zn4 166.6(5) . . . . no
O16 Dy2 O15 C67 -20.0(9) . . . . no
O2W Dy2 O16 C68 98.9(8) . . . . no
O2W Dy2 O16 C72 -83.3(9) . . . . no
O9 Dy2 O16 C68 115.8(7) . . . . no
O9 Dy2 O16 C72 -66.4(9) . . . . no
O10 Dy2 O16 C68 171.0(7) . . . . no
O10 Dy2 O16 C72 -11.2(9) . . . . no
O11 Dy2 O16 C68 -127.2(8) . . . . no
O11 Dy2 O16 C72 50.6(9) . . . . no
O12 Dy2 O16 C68 -62.8(7) . . . . no
O12 Dy2 O16 C72 115.1(9) . . . . no
O13 Dy2 O16 C68 -88.2(9) . . . . no
O13 Dy2 O16 C72 89.7(9) . . . . no
O14 Dy2 O16 C68 7.8(9) . . . . no
O14 Dy2 O16 C72 -174.4(8) . . . . no
O15 Dy2 O16 C68 17.6(7) . . . . no
O15 Dy2 O16 C72 -164.5(9) . . . . no
O2W Dy2 O9 C37 -100.8(9) . . . . no
O2W Dy2 O9 C38 68.0(7) . . . . no
O10 Dy2 O9 C37 172.5(10) . . . . no
O10 Dy2 O9 C38 -18.7(7) . . . . no
O11 Dy2 O9 C37 145.7(8) . . . . no
O11 Dy2 O9 C38 -45.5(8) . . . . no
O12 Dy2 O9 C37 59.0(11) . . . . no
O12 Dy2 O9 C38 -132.2(7) . . . . no
O13 Dy2 O9 C37 74.9(9) . . . . no
O13 Dy2 O9 C38 -116.4(7) . . . . no
O14 Dy2 O9 C37 10.2(9) . . . . no
O14 Dy2 O9 C38 179.0(8) . . . . no
O15 Dy2 O9 C37 -43.1(10) . . . . no
O15 Dy2 O9 C38 125.7(7) . . . . no
O16 Dy2 O9 C37 -118.4(9) . . . . no
O16 Dy2 O9 C38 50.5(8) . . . . no
O2W Dy2 O10 Zn3 137.2(3) . . . . no
O2W Dy2 O10 C39 -45.8(7) . . . . no
O9 Dy2 O10 Zn3 -152.6(4) . . . . no
O9 Dy2 O10 C39 24.4(7) . . . . no
O11 Dy2 O10 Zn3 2.7(2) . . . . no
O11 Dy2 O10 C39 179.7(7) . . . . no
O12 Dy2 O10 Zn3 -9.9(4) . . . . no
O12 Dy2 O10 C39 167.1(6) . . . . no
O13 Dy2 O10 Zn3 -79.4(3) . . . . no
O13 Dy2 O10 C39 97.6(7) . . . . no
O14 Dy2 O10 Zn3 -129.5(3) . . . . no
O14 Dy2 O10 C39 47.6(8) . . . . no
O15 Dy2 O10 Zn3 117.1(5) . . . . no
O15 Dy2 O10 C39 -65.9(9) . . . . no
O16 Dy2 O10 Zn3 68.3(3) . . . . no
O16 Dy2 O10 C39 -114.7(7) . . . . no
O2W Dy2 O11 Zn3 -57.1(4) . . . . no
O2W Dy2 O11 C49 117.7(8) . . . . no
O9 Dy2 O11 Zn3 22.6(4) . . . . no
O9 Dy2 O11 C49 -162.6(8) . . . . no
O10 Dy2 O11 Zn3 -2.8(2) . . . . no
O10 Dy2 O11 C49 172.0(8) . . . . no
O12 Dy2 O11 Zn3 165.8(4) . . . . no
O12 Dy2 O11 C49 -19.4(8) . . . . no
O13 Dy2 O11 Zn3 89.6(3) . . . . no
O13 Dy2 O11 C49 -95.7(8) . . . . no
O14 Dy2 O11 Zn3 123.8(4) . . . . no
O14 Dy2 O11 C49 -61.4(9) . . . . no
O15 Dy2 O11 Zn3 -147.9(3) . . . . no
O15 Dy2 O11 C49 26.9(9) . . . . no
O16 Dy2 O11 Zn3 -110.6(3) . . . . no
O16 Dy2 O11 C49 64.1(8) . . . . no
O2W Dy2 O12 C50 -90.0(8) . . . . no
O2W Dy2 O12 C54 82.0(9) . . . . no
O9 Dy2 O12 C50 121.7(8) . . . . no
O9 Dy2 O12 C54 -66.3(10) . . . . no
O10 Dy2 O12 C50 29.2(9) . . . . no
O10 Dy2 O12 C54 -158.8(8) . . . . no
O11 Dy2 O12 C50 16.0(7) . . . . no
O11 Dy2 O12 C54 -172.0(9) . . . . no
O13 Dy2 O12 C50 105.8(8) . . . . no
O13 Dy2 O12 C54 -82.2(9) . . . . no
O14 Dy2 O12 C50 168.4(8) . . . . no
O14 Dy2 O12 C54 -19.6(8) . . . . no
O15 Dy2 O12 C50 -125.0(8) . . . . no
O15 Dy2 O12 C54 47.0(8) . . . . no
O16 Dy2 O12 C50 -60.2(8) . . . . no
O16 Dy2 O12 C54 111.8(9) . . . . no
O2W Dy2 O13 C55 126.8(9) . . . . no
O2W Dy2 O13 C56 -70.0(9) . . . . no
O9 Dy2 O13 C55 120.4(9) . . . . no
O9 Dy2 O13 C56 -76.3(8) . . . . no
O10 Dy2 O13 C55 60.8(9) . . . . no
O10 Dy2 O13 C56 -136.0(8) . . . . no
O11 Dy2 O13 C55 -5.6(9) . . . . no
O11 Dy2 O13 C56 157.7(8) . . . . no
O12 Dy2 O13 C55 -68.2(9) . . . . no
O12 Dy2 O13 C56 95.0(8) . . . . no
O14 Dy2 O13 C55 -159.5(10) . . . . no
O14 Dy2 O13 C56 3.7(7) . . . . no
O15 Dy2 O13 C55 -129.4(9) . . . . no
O22 Dy3 O18 C75 69.0(8) . . . . no
O23 Dy3 O18 Zn5 146.0(2) . . . . no
O23 Dy3 O18 C75 -19.3(8) . . . . no
O24 Dy3 O18 Zn5 106.8(3) . . . . no
O24 Dy3 O18 C75 -58.4(7) . . . . no
O3W Dy3 O19 Zn5 -142.3(3) . . . . no
O3W Dy3 O19 C85 46.5(7) . . . . no
O17 Dy3 O19 Zn5 6.8(4) . . . . no
O17 Dy3 O19 C85 -164.3(6) . . . . no
O18 Dy3 O19 Zn5 -2.6(2) . . . . no
O18 Dy3 O19 C85 -173.8(7) . . . . no
O20 Dy3 O19 Zn5 147.3(3) . . . . no
O20 Dy3 O19 C85 -23.8(7) . . . . no
O21 Dy3 O19 Zn5 77.8(3) . . . . no
O21 Dy3 O19 C85 -93.4(7) . . . . no
O22 Dy3 O19 Zn5 131.8(3) . . . . no
O22 Dy3 O19 C85 -39.3(8) . . . . no
O23 Dy3 O19 Zn5 -114.9(4) . . . . no
O23 Dy3 O19 C85 74.0(8) . . . . no
O24 Dy3 O19 Zn5 -70.5(3) . . . . no
O24 Dy3 O19 C85 118.3(7) . . . . no
O3W Dy3 O20 C86 -66.8(6) . . . . no
O3W Dy3 O20 C90 85.0(9) . . . . no
O17 Dy3 O20 C86 133.3(6) . . . . no
O17 Dy3 O20 C90 -74.9(10) . . . . no
O18 Dy3 O20 C86 51.0(6) . . . . no
O18 Dy3 O20 C90 -157.2(8) . . . . no
O19 Dy3 O20 C86 19.3(6) . . . . no
O19 Dy3 O20 C90 171.1(9) . . . . no
O21 Dy3 O20 C86 121.2(6) . . . . no
O21 Dy3 O20 C90 -87.1(8) . . . . no
O22 Dy3 O20 C86 -172.5(6) . . . . no
O22 Dy3 O20 C90 -20.7(8) . . . . no
O23 Dy3 O20 C86 -122.3(6) . . . . no
O23 Dy3 O20 C90 29.5(9) . . . . no
O24 Dy3 O20 C86 -43.5(7) . . . . no
O24 Dy3 O20 C90 108.3(8) . . . . no
O3W Dy3 O21 C91 -124.4(9) . . . . no
O3W Dy3 O21 C92 73.2(8) . . . . no
O17 Dy3 O21 C91 73.4(9) . . . . no
O17 Dy3 O21 C92 -89.1(7) . . . . no
O18 Dy3 O21 C91 10.4(9) . . . . no
O18 Dy3 O21 C92 -152.1(8) . . . . no
O19 Dy3 O21 C91 -55.5(9) . . . . no
O19 Dy3 O21 C92 142.1(7) . . . . no
O20 Dy3 O21 C91 -113.6(9) . . . . no
O20 Dy3 O21 C92 84.0(7) . . . . no
O22 Dy3 O21 C91 166.2(10) . . . . no
O22 Dy3 O21 C92 3.8(7) . . . . no
O23 Dy3 O21 C91 132.5(9) . . . . no
O24 Dy3 O21 C91 46.6(11) . . . . no
O24 Dy3 O21 C92 -115.8(8) . . . . no
O3W Dy3 O22 Zn6 49.5(3) . . . . no
O3W Dy3 O22 C93 -146.6(8) . . . . no
O17 Dy3 O22 Zn6 -94.9(3) . . . . no
O17 Dy3 O22 C93 69.0(8) . . . . no
O18 Dy3 O22 Zn6 -132.2(3) . . . . no
O18 Dy3 O22 C93 31.7(10) . . . . no
O19 Dy3 O22 Zn6 125.7(3) . . . . no
O19 Dy3 O22 C93 -70.4(9) . . . . no
O20 Dy3 O22 Zn6 111.7(3) . . . . no
O20 Dy3 O22 C93 -84.4(8) . . . . no
O21 Dy3 O22 Zn6 -169.5(4) . . . . no
O21 Dy3 O22 C93 -5.6(7) . . . . no
O23 Dy3 O22 Zn6 -20.9(3) . . . . no
O23 Dy3 O22 C93 143.0(9) . . . . no
O24 Dy3 O22 Zn6 -25.6(5) . . . . no
O24 Dy3 O22 C93 138.3(7) . . . . no
O3W Dy3 O23 Zn6 -83.3(3) . . . . no
O3W Dy3 O23 C107 92.3(9) . . . . no
O17 Dy3 O23 Zn6 114.0(3) . . . . no
O17 Dy3 O23 C107 -70.5(9) . . . . no
O18 Dy3 O23 Zn6 154.6(3) . . . . no
O18 Dy3 O23 C107 -29.9(10) . . . . no
O19 Dy3 O23 Zn6 -110.7(4) . . . . no
O19 Dy3 O23 C107 64.9(11) . . . . no
O20 Dy3 O23 Zn6 -32.3(4) . . . . no
O20 Dy3 O23 C107 143.3(9) . . . . no
O21 Dy3 O23 Zn6 54.5(4) . . . . no
O21 Dy3 O23 C107 -129.9(9) . . . . no
O22 Dy3 O23 Zn6 21.7(3) . . . . no
O22 Dy3 O23 C107 -162.8(10) . . . . no
O24 Dy3 O23 Zn6 -162.6(4) . . . . no
O24 Dy3 O23 C107 13.0(9) . . . . no
O3W Dy3 O24 C106 -93.5(9) . . . . no
O3W Dy3 O24 C108 87.2(9) . . . . no
O17 Dy3 O24 C106 66.3(9) . . . . no
O17 Dy3 O24 C108 -113.0(9) . . . . no
O18 Dy3 O24 C106 130.7(9) . . . . no
O18 Dy3 O24 C108 -48.6(9) . . . . no
O19 Dy3 O24 C106 -166.2(9) . . . . no
O19 Dy3 O24 C108 14.5(9) . . . . no
O20 Dy3 O24 C106 -115.5(9) . . . . no
O20 Dy3 O24 C108 65.2(10) . . . . no
O21 Dy3 O24 C106 92.7(10) . . . . no
O21 Dy3 O24 C108 -86.6(10) . . . . no
O22 Dy3 O24 C106 -7.0(10) . . . . no
O22 Dy3 O24 C108 173.7(9) . . . . no
O23 Dy3 O24 C106 -11.9(9) . . . . no
O23 Dy3 O24 C108 168.8(10) . . . . no
O23 Dy3 O17 C74 118.9(7) . . . . no
O24 Dy3 O17 C73 -111.7(8) . . . . no
O3W Dy3 O17 C73 -76.8(9) . . . . no
O3W Dy3 O17 C74 89.3(8) . . . . no
O18 Dy3 O17 C73 171.6(8) . . . . no
O18 Dy3 O17 C74 -22.3(7) . . . . no
O19 Dy3 O17 C73 161.9(7) . . . . no
O19 Dy3 O17 C74 -32.0(8) . . . . no
O20 Dy3 O17 C73 70.5(9) . . . . no
O20 Dy3 O17 C74 -123.4(7) . . . . no
O21 Dy3 O17 C73 82.6(8) . . . . no
O21 Dy3 O17 C74 -111.3(7) . . . . no
O22 Dy3 O17 C73 19.0(8) . . . . no
O22 Dy3 O17 C74 -174.9(7) . . . . no
O23 Dy3 O17 C73 -47.3(8) . . . . no
O19 Dy3 O18 Zn5 2.6(2) . . . . no
O23 Dy3 O21 C92 -29.9(8) . . . . no
O24 Dy3 O17 C74 54.4(7) . . . . no
O3W Dy3 O18 Zn5 52.2(4) . . . . no
O3W Dy3 O18 C75 -113.1(8) . . . . no
O17 Dy3 O18 Zn5 -169.0(3) . . . . no
O17 Dy3 O18 C75 25.8(7) . . . . no
O20 Dy3 O18 C75 167.6(7) . . . . no
O19 Dy3 O18 C75 -162.6(8) . . . . no
O20 Dy3 O18 Zn5 -27.2(3) . . . . no
O22 Dy3 O18 Zn5 -125.7(3) . . . . no
O21 Dy3 O18 Zn5 -92.6(3) . . . . no
O21 Dy3 O18 C75 102.2(8) . . . . no
O31 Dy4 O29 C126 -154.2(7) . . . . no
O29 Dy4 O31 Zn8 -29.5(4) . . . . no
O29 Dy4 O31 C115 172.1(7) . . . . no
O32 Dy4 O29 C122 143.5(5) . . . . no
O30 Dy4 O31 C115 -158.7(7) . . . . no
O32 Dy4 O31 Zn8 -169.1(4) . . . . no
O32 Dy4 O31 C115 32.5(7) . . . . no
O4W Dy4 O32 C109 -62.4(10) . . . . no
O4W Dy4 O32 C110 88.9(8) . . . . no
O25 Dy4 O32 C109 88.6(9) . . . . no
O25 Dy4 O32 C110 -120.1(7) . . . . no
O26 Dy4 O32 C109 24.1(8) . . . . no
O26 Dy4 O32 C110 175.4(7) . . . . no
O27 Dy4 O32 C109 -44.9(8) . . . . no
O27 Dy4 O32 C110 106.3(7) . . . . no
O28 Dy4 O32 C109 -108.1(9) . . . . no
O28 Dy4 O32 C110 43.2(7) . . . . no
O29 Dy4 O32 C109 74.9(9) . . . . no
O30 Dy4 O31 Zn8 -0.3(2) . . . . no
O30 Dy4 O32 C109 164.2(8) . . . . no
O30 Dy4 O32 C110 -44.5(7) . . . . no
O31 Dy4 O32 C109 177.4(9) . . . . no
O31 Dy4 O32 C110 -31.3(6) . . . . no
O32 Dy4 O28 C144 -111.5(11) . . . . no
O4W Dy4 O29 C122 -61.9(5) . . . . no
O4W Dy4 O25 C127 -93.2(8) . . . . no
O4W Dy4 O25 C128 76.6(7) . . . . no
O26 Dy4 O25 C127 -168.8(9) . . . . no
O26 Dy4 O25 C128 1.0(6) . . . . no
O27 Dy4 O25 C127 165.3(8) . . . . no
O27 Dy4 O25 C128 -24.9(7) . . . . no
O28 Dy4 O25 C127 60.2(11) . . . . no
O28 Dy4 O25 C128 -130.0(7) . . . . no
O29 Dy4 O25 C127 -80.7(8) . . . . no
O29 Dy4 O25 C128 89.1(6) . . . . no
O30 Dy4 O25 C127 -22.5(8) . . . . no
O30 Dy4 O25 C128 147.3(7) . . . . no
O31 Dy4 O25 C127 44.7(8) . . . . no
O31 Dy4 O25 C128 -145.5(7) . . . . no
O32 Dy4 O25 C127 108.0(8) . . . . no
O32 Dy4 O25 C128 -82.2(7) . . . . no
O4W Dy4 O26 Zn7 49.2(3) . . . . no
O4W Dy4 O26 C129 -135.3(8) . . . . no
O25 Dy4 O26 Zn7 -179.4(4) . . . . no
O25 Dy4 O26 C129 -3.9(7) . . . . no
O27 Dy4 O26 Zn7 -22.0(3) . . . . no
O27 Dy4 O26 C129 153.5(8) . . . . no
O28 Dy4 O26 Zn7 -21.7(5) . . . . no
O28 Dy4 O26 C129 153.8(7) . . . . no
O29 Dy4 O32 C110 -133.8(7) . . . . no
O30 Dy4 O26 C129 -55.1(9) . . . . no
O31 Dy4 O26 Zn7 -129.4(3) . . . . no
O31 Dy4 O26 C129 46.1(9) . . . . no
O32 Dy4 O26 Zn7 -95.6(3) . . . . no
O32 Dy4 O26 C129 79.9(8) . . . . no
O4W Dy4 O27 Zn7 -81.7(3) . . . . no
O4W Dy4 O27 C139 70.7(8) . . . . no
O25 Dy4 O27 Zn7 47.2(4) . . . . no
O25 Dy4 O27 C139 -160.3(7) . . . . no
O26 Dy4 O27 Zn7 22.2(3) . . . . no
O26 Dy4 O27 C139 174.6(8) . . . . no
O28 Dy4 O27 Zn7 -157.6(4) . . . . no
O28 Dy4 O27 C139 -5.1(8) . . . . no
O29 Dy4 O27 Zn7 -34.7(4) . . . . no
O29 Dy4 O27 C139 117.8(8) . . . . no
O30 Dy4 O27 Zn7 -117.8(4) . . . . no
O30 Dy4 O27 C139 34.6(10) . . . . no
O31 Dy4 O27 Zn7 151.3(3) . . . . no
O31 Dy4 O27 C139 -56.3(8) . . . . no
O32 Dy4 O27 Zn7 108.5(3) . . . . no
O32 Dy4 O27 C139 -99.0(8) . . . . no
O4W Dy4 O28 C140 -75.5(7) . . . . no
O4W Dy4 O28 C144 94.2(11) . . . . no
O25 Dy4 O28 C140 125.8(8) . . . . no
O25 Dy4 O28 C144 -64.4(13) . . . . no
O26 Dy4 O28 C140 7.4(8) . . . . no
O26 Dy4 O28 C144 177.1(10) . . . . no
O27 Dy4 O28 C140 7.7(6) . . . . no
O27 Dy4 O28 C144 177.4(11) . . . . no
O29 Dy4 O28 C140 -103.5(7) . . . . no
O29 Dy4 O28 C144 66.3(11) . . . . no
O30 Dy4 O28 C140 -152.7(7) . . . . no
O30 Dy4 O28 C144 17.1(11) . . . . no
O31 Dy4 O28 C140 141.9(7) . . . . no
O31 Dy4 O28 C144 -48.4(10) . . . . no
O32 Dy4 O28 C140 78.8(7) . . . . no
O32 Dy4 O30 C121 -171.7(7) . . . . no
O4W Dy4 O31 Zn8 50.7(4) . . . . no
O4W Dy4 O29 C126 83.2(8) . . . . no
O25 Dy4 O29 C122 128.7(5) . . . . no
O25 Dy4 O29 C126 -86.2(8) . . . . no
O26 Dy4 O29 C122 -165.4(5) . . . . no
O26 Dy4 O29 C126 -20.2(8) . . . . no
O27 Dy4 O29 C122 -113.3(5) . . . . no
O27 Dy4 O29 C126 31.8(8) . . . . no
O28 Dy4 O29 C122 -32.6(6) . . . . no
O28 Dy4 O29 C126 112.5(8) . . . . no
O30 Dy4 O29 C122 29.1(5) . . . . no
O30 Dy4 O29 C126 174.2(8) . . . . no
O31 Dy4 O29 C122 60.7(6) . . . . no
O31 Dy4 O30 C121 175.6(8) . . . . no
O32 Dy4 O29 C126 -71.4(8) . . . . no
O4W Dy4 O30 Zn8 -141.8(3) . . . . no
O4W Dy4 O30 C121 33.5(7) . . . . no
O25 Dy4 O30 Zn8 86.1(3) . . . . no
O25 Dy4 O30 C121 -98.7(7) . . . . no
O26 Dy4 O30 Zn8 130.4(3) . . . . no
O26 Dy4 O30 C121 -54.4(8) . . . . no
O27 Dy4 O30 Zn8 -106.1(4) . . . . no
O27 Dy4 O30 C121 69.2(8) . . . . no
O28 Dy4 O30 Zn8 -71.4(3) . . . . no
O28 Dy4 O30 C121 103.9(7) . . . . no
O29 Dy4 O30 Zn8 150.5(4) . . . . no
O29 Dy4 O30 C121 -34.2(7) . . . . no
O31 Dy4 O30 Zn8 0.3(2) . . . . no
O29 Dy4 O26 Zn7 111.8(3) . . . . no
O32 Dy4 O30 Zn8 13.1(4) . . . . no
O30 Dy4 O26 Zn7 129.5(3) . . . . no
O27 Dy4 O31 C115 -13.7(8) . . . . no
O4W Dy4 O31 C115 -107.8(7) . . . . no
O25 Dy4 O31 Zn8 -87.7(3) . . . . no
O25 Dy4 O31 C115 113.9(7) . . . . no
O26 Dy4 O31 Zn8 -131.2(3) . . . . no
O26 Dy4 O31 C115 70.4(7) . . . . no
O27 Dy4 O31 Zn8 144.7(3) . . . . no
O29 Dy4 O26 C129 -72.7(8) . . . . no
O28 Dy4 O31 Zn8 98.5(3) . . . . no
O28 Dy4 O31 C115 -59.9(7) . . . . no
N4 Zn1 N3 C27 29.5(8) . . . . no
Cl2 Zn1 O6 C21 -93.1(8) . . . . no
O7 Zn1 O6 C21 157.7(9) . . . . no
Cl2 Zn1 O6 Dy1 110.3(3) . . . . no
N4 Zn1 N3 C26 -151.2(11) . . . . no
N3 Zn1 O6 C21 15.7(8) . . . . no
N4 Zn1 O6 Dy1 -66.1(5) . . . . no
N4 Zn1 O6 C21 90.5(9) . . . . no
Cl2 Zn1 O7 Dy1 -116.1(3) . . . . no
Cl2 Zn1 O7 C35 60.1(8) . . . . no
O6 Zn1 O7 Dy1 -1.2(3) . . . . no
O6 Zn1 O7 C35 175.0(8) . . . . no
N3 Zn1 O7 Dy1 67.7(7) . . . . no
N3 Zn1 O7 C35 -116.1(8) . . . . no
N4 Zn1 O7 Dy1 137.1(4) . . . . no
N4 Zn1 O7 C35 -46.7(8) . . . . no
Cl2 Zn1 N3 C26 103.0(10) . . . . no
O7 Zn1 O6 Dy1 1.1(3) . . . . no
Cl2 Zn1 N3 C27 -76.3(8) . . . . no
N3 Zn1 O6 Dy1 -141.0(4) . . . . no
O7 Zn1 N3 C26 -80.7(12) . . . . no
O7 Zn1 N3 C27 100.0(9) . . . . no
O7 Zn1 N4 C28 -149.7(8) . . . . no
O7 Zn1 N4 C29 35.1(11) . . . . no
N3 Zn1 N4 C28 -8.2(8) . . . . no
Cl2 Zn1 N4 C28 97.6(8) . . . . no
Cl2 Zn1 N4 C29 -77.7(11) . . . . no
O6 Zn1 N4 C28 -85.7(9) . . . . no
O6 Zn1 N4 C29 99.0(11) . . . . no
N3 Zn1 N4 C29 176.5(11) . . . . no
O6 Zn1 N3 C26 -15.8(11) . . . . no
O6 Zn1 N3 C27 164.9(8) . . . . no
N2 Zn2 N1 C8 146.8(15) . . . . no
O3 Zn2 O2 Dy1 22.1(3) . . . . no
N2 Zn2 N1 C9 -29.0(9) . . . . no
O3 Zn2 N1 C9 -102.0(10) . . . . no
O3 Zn2 O2 C7 -150.3(9) . . . . no
N1 Zn2 O2 Dy1 164.9(4) . . . . no
N1 Zn2 O2 C7 -7.5(8) . . . . no
N2 Zn2 O2 Dy1 94.4(6) . . . . no
N2 Zn2 O2 C7 -78.0(10) . . . . no
Cl1 Zn2 O3 Dy1 84.6(3) . . . . no
Cl1 Zn2 O3 C13 -112.2(10) . . . . no
O2 Zn2 O3 Dy1 -21.4(3) . . . . no
O2 Zn2 O3 C13 141.8(10) . . . . no
N1 Zn2 O3 Dy1 -90.8(7) . . . . no
N1 Zn2 O3 C13 72.4(12) . . . . no
N2 Zn2 O3 Dy1 -160.6(5) . . . . no
Cl1 Zn2 O2 Dy1 -80.1(3) . . . . no
Cl1 Zn2 O2 C7 107.6(8) . . . . no
Cl1 Zn2 N2 C11 109.8(13) . . . . no
O2 Zn2 N1 C9 -167.8(9) . . . . no
O3 Zn2 N1 C8 73.8(16) . . . . no
O2 Zn2 N1 C8 8.0(14) . . . . no
O3 Zn2 N2 C11 3.8(14) . . . . no
N1 Zn2 N2 C10 35.9(10) . . . . no
Cl1 Zn2 N2 C10 -76.2(10) . . . . no
O3 Zn2 N2 C10 177.8(10) . . . . no
O2 Zn2 N2 C10 109.6(9) . . . . no
O2 Zn2 N2 C11 -64.4(16) . . . . no
N1 Zn2 N2 C11 -138.2(14) . . . . no
Cl1 Zn2 N1 C9 82.9(9) . . . . no
N2 Zn2 O3 C13 2.6(10) . . . . no
Cl1 Zn2 N1 C8 -101.3(14) . . . . no
Cl3 Zn3 O10 C39 -68.5(6) . . . . no
N6 Zn3 O11 Dy2 149.3(4) . . . . no
N6 Zn3 O11 C49 -25.5(8) . . . . no
N5 Zn3 O11 C49 -102.2(9) . . . . no
Cl3 Zn3 O10 Dy2 108.9(2) . . . . no
O10 Zn3 N5 C44 -33.9(10) . . . . no
O10 Zn3 N5 C45 152.2(9) . . . . no
O11 Zn3 N5 C44 -99.4(10) . . . . no
O11 Zn3 N5 C45 86.7(10) . . . . no
N6 Zn3 N5 C44 -179.0(10) . . . . no
N6 Zn3 N5 C45 7.1(9) . . . . no
Cl3 Zn3 N6 C46 78.5(9) . . . . no
Cl3 Zn3 N6 C47 -98.6(12) . . . . no
O10 Zn3 N6 C46 -102.0(10) . . . . no
O10 Zn3 N6 C47 81.0(14) . . . . no
O11 Zn3 N6 C46 -165.7(9) . . . . no
O11 Zn3 N6 C47 17.3(12) . . . . no
N5 Zn3 O11 Dy2 72.7(6) . . . . no
Cl3 Zn3 N5 C44 77.5(10) . . . . no
Cl3 Zn3 N5 C45 -96.4(9) . . . . no
N6 Zn3 O10 Dy2 -70.7(7) . . . . no
N6 Zn3 O10 C39 112.0(8) . . . . no
Cl3 Zn3 O11 Dy2 -104.2(2) . . . . no
O11 Zn3 O10 Dy2 -3.0(2) . . . . no
O11 Zn3 O10 C39 179.7(6) . . . . no
N5 Zn3 O10 Dy2 -142.6(4) . . . . no
N5 Zn3 O10 C39 40.1(6) . . . . no
N5 Zn3 N6 C47 154.6(12) . . . . no
O10 Zn3 O11 Dy2 2.9(2) . . . . no
O10 Zn3 O11 C49 -172.0(8) . . . . no
Cl3 Zn3 O11 C49 81.0(8) . . . . no
N5 Zn3 N6 C46 -28.3(9) . . . . no
O15 Zn4 O14 C57 151.0(9) . . . . no
N7 Zn4 O14 Dy2 -174.7(4) . . . . no
O15 Zn4 O14 Dy2 -23.2(3) . . . . no
Cl4 Zn4 N7 C62 102.3(12) . . . . no
O14 Zn4 N7 C62 -3.5(12) . . . . no
O14 Zn4 N7 C63 171.0(9) . . . . no
O15 Zn4 N7 C62 -68.0(15) . . . . no
O15 Zn4 N7 C63 106.5(10) . . . . no
N8 Zn4 N7 C62 -140.3(13) . . . . no
N8 Zn4 N7 C63 34.3(9) . . . . no
Cl4 Zn4 N8 C64 87.7(10) . . . . no
Cl4 Zn4 N8 C65 -100.6(13) . . . . no
O14 Zn4 N8 C64 -93.1(10) . . . . no
O14 Zn4 N8 C65 78.6(14) . . . . no
O15 Zn4 N8 C64 -163.7(10) . . . . no
O15 Zn4 N8 C65 8.0(13) . . . . no
Cl4 Zn4 N7 C63 -83.2(9) . . . . no
N8 Zn4 O15 C67 -12.6(10) . . . . no
Cl4 Zn4 O14 Dy2 80.5(3) . . . . no
Cl4 Zn4 O14 C57 -105.2(9) . . . . no
Cl4 Zn4 O15 C67 107.4(9) . . . . no
O14 Zn4 O15 Dy2 23.1(3) . . . . no
O14 Zn4 O15 C67 -150.3(10) . . . . no
N7 Zn4 O14 C57 -0.4(9) . . . . no
N8 Zn4 O14 Dy2 -98.7(5) . . . . no
N8 Zn4 O14 C57 75.6(10) . . . . no
Cl4 Zn4 O15 Dy2 -79.3(3) . . . . no
N7 Zn4 N8 C65 158.5(14) . . . . no
N7 Zn4 O15 C67 -82.4(12) . . . . no
N8 Zn4 O15 Dy2 160.7(4) . . . . no
N7 Zn4 O15 Dy2 90.9(7) . . . . no
N7 Zn4 N8 C64 -13.2(10) . . . . no
Cl5 Zn5 N9 C81 -75.1(8) . . . . no
O18 Zn5 N9 C80 -14.8(11) . . . . no
Cl5 Zn5 N9 C80 100.9(10) . . . . no
N10 Zn5 O19 C85 -42.4(7) . . . . no
N9 Zn5 O19 C85 -114.5(7) . . . . no
Cl5 Zn5 O18 Dy3 104.2(2) . . . . no
Cl5 Zn5 O18 C75 -90.6(7) . . . . no
O19 Zn5 O18 Dy3 -2.7(2) . . . . no
O19 Zn5 O18 C75 162.5(8) . . . . no
N9 Zn5 O18 Dy3 -147.0(3) . . . . no
N9 Zn5 O18 C75 18.3(8) . . . . no
N10 Zn5 O18 Dy3 -70.2(6) . . . . no
N10 Zn5 O18 C75 95.0(9) . . . . no
Cl5 Zn5 O19 Dy3 -108.6(2) . . . . no
Cl5 Zn5 O19 C85 63.7(6) . . . . no
O18 Zn5 O19 Dy3 2.8(2) . . . . no
N9 Zn5 N10 C82 -9.4(9) . . . . no
N9 Zn5 N10 C83 178.0(11) . . . . no
O18 Zn5 O19 C85 175.1(6) . . . . no
N9 Zn5 O19 Dy3 73.2(6) . . . . no
N10 Zn5 O19 Dy3 145.3(4) . . . . no
Cl5 Zn5 N10 C83 -76.3(10) . . . . no
O18 Zn5 N9 C81 169.1(8) . . . . no
O19 Zn5 N9 C80 -80.8(12) . . . . no
O19 Zn5 N9 C81 103.2(9) . . . . no
N10 Zn5 N9 C80 -154.5(11) . . . . no
N10 Zn5 N9 C81 29.4(8) . . . . no
Cl5 Zn5 N10 C82 96.3(9) . . . . no
O19 Zn5 N10 C82 -152.8(9) . . . . no
O18 Zn5 N10 C82 -89.0(10) . . . . no
O18 Zn5 N10 C83 98.4(11) . . . . no
O19 Zn5 N10 C83 34.6(10) . . . . no
O23 Zn6 N11 C99 -112.7(9) . . . . no
Cl6 Zn6 O22 Dy3 -78.8(3) . . . . no
Cl6 Zn6 O22 C93 117.2(8) . . . . no
O22 Zn6 N11 C99 -173.4(9) . . . . no
O23 Zn6 O22 Dy3 22.5(3) . . . . no
O23 Zn6 O22 C93 -141.5(9) . . . . no
N11 Zn6 O22 Dy3 171.6(4) . . . . no
N11 Zn6 O22 C93 7.6(9) . . . . no
N12 Zn6 O22 Dy3 98.9(5) . . . . no
N12 Zn6 O22 C93 -65.1(10) . . . . no
Cl6 Zn6 O23 Dy3 83.8(3) . . . . no
Cl6 Zn6 O23 C107 -91.9(9) . . . . no
O22 Zn6 O23 Dy3 -22.9(3) . . . . no
O22 Zn6 O23 C107 161.4(9) . . . . no
N11 Zn6 O23 Dy3 -86.7(7) . . . . no
N11 Zn6 O23 C107 97.6(10) . . . . no
N11 Zn6 N12 C101 -158.0(13) . . . . no
N12 Zn6 O23 Dy3 -159.9(4) . . . . no
N12 Zn6 O23 C107 24.5(9) . . . . no
O23 Zn6 N11 C98 55.5(15) . . . . no
O22 Zn6 N11 C98 -5.2(12) . . . . no
O22 Zn6 N12 C101 -82.5(13) . . . . no
O23 Zn6 N12 C100 160.1(9) . . . . no
N12 Zn6 N11 C98 131.9(13) . . . . no
N12 Zn6 N11 C99 -36.3(9) . . . . no
Cl6 Zn6 N12 C100 -92.9(9) . . . . no
Cl6 Zn6 N12 C101 95.1(12) . . . . no
O22 Zn6 N12 C100 89.5(10) . . . . no
Cl6 Zn6 N11 C99 77.1(9) . . . . no
O23 Zn6 N12 C101 -11.8(12) . . . . no
N11 Zn6 N12 C100 13.9(9) . . . . no
Cl6 Zn6 N11 C98 -114.8(12) . . . . no
Cl7 Zn7 O26 C129 104.0(7) . . . . no
N15 Zn7 O27 C139 115.5(8) . . . . no
N16 Zn7 O27 Dy4 -165.1(4) . . . . no
Cl7 Zn7 O26 Dy4 -80.4(2) . . . . no
N16 Zn7 O27 C139 40.0(8) . . . . no
Cl7 Zn7 N15 C134 -99.8(11) . . . . no
Cl7 Zn7 N15 C135 80.3(7) . . . . no
O26 Zn7 N15 C134 9.9(11) . . . . no
O26 Zn7 N15 C135 -170.1(7) . . . . no
O27 Zn7 N15 C134 72.6(13) . . . . no
O27 Zn7 N15 C135 -107.4(8) . . . . no
N16 Zn7 N15 C134 149.3(11) . . . . no
N16 Zn7 N15 C135 -30.7(7) . . . . no
Cl7 Zn7 N16 C136 -101.1(7) . . . . no
Cl7 Zn7 N16 C137 82.5(10) . . . . no
Cl7 Zn7 O27 C139 -72.0(8) . . . . no
O26 Zn7 O27 Dy4 -23.5(3) . . . . no
O26 Zn7 O27 C139 -178.4(8) . . . . no
N15 Zn7 O27 Dy4 -89.7(6) . . . . no
O27 Zn7 N16 C136 151.3(7) . . . . no
O27 Zn7 N16 C137 -25.1(10) . . . . no
N15 Zn7 N16 C136 8.7(7) . . . . no
N15 Zn7 N16 C137 -167.7(10) . . . . no
Cl7 Zn7 O27 Dy4 82.9(3) . . . . no
O27 Zn7 O26 Dy4 23.4(3) . . . . no
O27 Zn7 O26 C129 -152.2(8) . . . . no
N15 Zn7 O26 Dy4 168.6(4) . . . . no
N15 Zn7 O26 C129 -7.0(8) . . . . no
N16 Zn7 O26 Dy4 92.5(6) . . . . no
N16 Zn7 O26 C129 -83.1(9) . . . . no
O26 Zn7 N16 C136 86.1(8) . . . . no
O26 Zn7 N16 C137 -90.3(11) . . . . no
Cl8 Zn8 O30 Dy4 -115.9(2) . . . . no
N13 Zn8 O31 Dy4 -143.6(3) . . . . no
O30 Zn8 O31 Dy4 0.3(2) . . . . no
O30 Zn8 O31 C115 157.1(8) . . . . no
N14 Zn8 O31 C115 87.9(8) . . . . no
Cl8 Zn8 N13 C116 106.1(10) . . . . no
Cl8 Zn8 N13 C117 -72.9(8) . . . . no
O30 Zn8 N13 C116 -76.2(12) . . . . no
O30 Zn8 N13 C117 104.8(8) . . . . no
O31 Zn8 N13 C116 -13.1(10) . . . . no
O31 Zn8 N13 C117 167.9(8) . . . . no
N14 Zn8 N13 C116 -147.9(11) . . . . no
N14 Zn8 N13 C117 33.2(8) . . . . no
Cl8 Zn8 N14 C118 96.7(8) . . . . no
Cl8 Zn8 N14 C119 -85.2(10) . . . . no
O30 Zn8 N14 C118 -151.7(8) . . . . no
O30 Zn8 N14 C119 26.4(10) . . . . no
N13 Zn8 O31 C115 13.2(8) . . . . no
N14 Zn8 O31 Dy4 -68.8(5) . . . . no
N13 Zn8 N14 C118 -9.2(8) . . . . no
N13 Zn8 N14 C119 168.8(10) . . . . no
N14 Zn8 O30 Dy4 136.7(4) . . . . no
N14 Zn8 O30 C121 -38.8(7) . . . . no
Cl8 Zn8 O30 C121 68.6(7) . . . . no
O31 Zn8 O30 Dy4 -0.3(2) . . . . no
O31 Zn8 O30 C121 -175.8(7) . . . . no
N13 Zn8 O30 Dy4 66.4(6) . . . . no
N13 Zn8 O30 C121 -109.1(8) . . . . no
Cl8 Zn8 O31 C115 -95.5(8) . . . . no
Cl8 Zn8 O31 Dy4 107.8(2) . . . . no
O31 Zn8 N14 C119 91.7(10) . . . . no
O31 Zn8 N14 C118 -86.4(8) . . . . no
Dy1 O1 C2 C3 179.2(10) . . . . no
C1 O1 C2 C3 -5.1(18) . . . . no
C1 O1 C2 C7 174.9(11) . . . . no
Dy1 O1 C2 C7 -0.9(12) . . . . no
Zn2 O2 C7 C6 2.1(15) . . . . no
Dy1 O2 C7 C6 -168.7(8) . . . . no
Dy1 O2 C7 C2 8.7(13) . . . . no
Zn2 O2 C7 C2 179.4(7) . . . . no
Dy1 O3 C13 C12 154.0(10) . . . . no
Zn2 O3 C13 C12 -6.1(18) . . . . no
Zn2 O3 C13 C14 175.4(8) . . . . no
Dy1 O3 C13 C14 -24.5(14) . . . . no
Dy1 O4 C14 C13 22.6(11) . . . . no
C18 O4 C14 C15 29.7(16) . . . . no
C18 O4 C14 C13 -156.1(11) . . . . no
Dy1 O4 C14 C15 -151.6(10) . . . . no
Dy1 O5 C20 C25 -152.6(10) . . . . no
C19 O5 C20 C25 8.7(17) . . . . no
C19 O5 C20 C21 -175.8(10) . . . . no
Dy1 O5 C20 C21 22.9(12) . . . . no
Dy1 O6 C21 C20 -31.4(12) . . . . no
Dy1 O6 C21 C22 145.7(9) . . . . no
Zn1 O6 C21 C22 -7.9(15) . . . . no
Zn1 O6 C21 C20 175.0(7) . . . . no
Dy1 O7 C35 C34 28.8(13) . . . . no
Dy1 O7 C35 C30 -147.7(9) . . . . no
Zn1 O7 C35 C34 -146.7(8) . . . . no
Zn1 O7 C35 C30 36.8(13) . . . . no
C36 O8 C34 C33 -0.6(16) . . . . no
Dy1 O8 C34 C35 -17.3(11) . . . . no
Dy1 O8 C34 C33 160.1(10) . . . . no
C36 O8 C34 C35 -178.0(10) . . . . no
Zn2 N1 C8 C6 -3(2) . . . . no
C8 N1 C9 C10 -159.5(14) . . . . no
Zn2 N1 C9 C10 17.0(15) . . . . no
C9 N1 C8 C6 172.5(13) . . . . no
C11 N2 C10 C9 136.9(16) . . . . no
Zn2 N2 C10 C9 -37.2(16) . . . . no
Zn2 N2 C11 C12 -7(2) . . . . no
C10 N2 C11 C12 179.7(14) . . . . no
C26 N3 C27 C28 135.9(12) . . . . no
C27 N3 C26 C22 -172.8(12) . . . . no
Zn1 N3 C27 C28 -44.7(11) . . . . no
Zn1 N3 C26 C22 8(2) . . . . no
Zn1 N4 C28 C27 -14.0(13) . . . . no
C29 N4 C28 C27 161.5(12) . . . . no
Zn1 N4 C29 C30 -11.1(19) . . . . no
C28 N4 C29 C30 173.9(12) . . . . no
O1 C2 C7 O2 -4.2(14) . . . . no
O1 C2 C7 C6 173.3(10) . . . . no
C3 C2 C7 O2 175.7(10) . . . . no
C3 C2 C7 C6 -6.8(16) . . . . no
C7 C2 C3 C4 4.1(18) . . . . no
O1 C2 C3 C4 -176.0(11) . . . . no
C2 C3 C4 C5 0.7(19) . . . . no
C3 C4 C5 C6 -2.6(19) . . . . no
C4 C5 C6 C7 -0.4(18) . . . . no
C4 C5 C6 C8 175.8(12) . . . . no
C5 C6 C7 C2 4.8(16) . . . . no
C5 C6 C7 O2 -177.8(10) . . . . no
C5 C6 C8 N1 177.8(14) . . . . no
C7 C6 C8 N1 -6(2) . . . . no
C8 C6 C7 O2 6.2(18) . . . . no
C8 C6 C7 C2 -171.2(11) . . . . no
C37 O9 C38 C43 6.5(17) . . . . no
N1 C9 C10 N2 14.5(19) . . . . no
C37 O9 C38 C39 -175.1(9) . . . . no
Dy2 O9 C38 C43 -164.2(11) . . . . no
Dy2 O9 C38 C39 14.1(11) . . . . no
Dy2 O10 C39 C38 -27.0(12) . . . . no
Dy2 O10 C39 C40 155.3(8) . . . . no
Zn3 O10 C39 C38 149.7(8) . . . . no
Zn3 O10 C39 C40 -27.9(12) . . . . no
N2 C11 C12 C13 4(2) . . . . no
N2 C11 C12 C17 179.9(15) . . . . no
Dy2 O11 C49 C48 -153.0(9) . . . . no
Zn3 O11 C49 C50 -165.6(8) . . . . no
Dy2 O11 C49 C50 20.5(14) . . . . no
Zn3 O11 C49 C48 20.9(15) . . . . no
C11 C12 C17 C16 -177.7(13) . . . . no
Dy2 O12 C50 C51 164.9(10) . . . . no
C11 C12 C13 C14 -178.3(12) . . . . no
C17 C12 C13 O3 -172.6(12) . . . . no
C17 C12 C13 C14 5.8(18) . . . . no
C54 O12 C50 C51 -7.0(18) . . . . no
C13 C12 C17 C16 -2(2) . . . . no
C11 C12 C13 O3 3(2) . . . . no
Dy2 O12 C50 C49 -13.4(13) . . . . no
C54 O12 C50 C49 174.7(11) . . . . no
O3 C13 C14 O4 -1.6(15) . . . . no
C12 C13 C14 C15 -5.6(17) . . . . no
Dy2 O13 C56 C57 -6.0(13) . . . . no
C12 C13 C14 O4 179.8(10) . . . . no
Dy2 O13 C56 C61 176.1(10) . . . . no
O3 C13 C14 C15 173.0(11) . . . . no
C55 O13 C56 C57 158.4(11) . . . . no
C55 O13 C56 C61 -19.5(17) . . . . no
O4 C14 C15 C16 175.1(12) . . . . no
Zn4 O14 C57 C58 5.9(16) . . . . no
Dy2 O14 C57 C56 -1.8(15) . . . . no
C13 C14 C15 C16 1.0(19) . . . . no
Zn4 O14 C57 C56 -174.6(8) . . . . no
Dy2 O14 C57 C58 178.6(9) . . . . no
Zn4 O15 C67 C68 -169.1(8) . . . . no
Zn4 O15 C67 C66 10.9(18) . . . . no
C14 C15 C16 C17 3(2) . . . . no
Dy2 O15 C67 C66 -161.0(10) . . . . no
Dy2 O15 C67 C68 19.0(15) . . . . no
C72 O16 C68 C69 -16.2(17) . . . . no
Dy2 O16 C68 C67 -16.4(13) . . . . no
C72 O16 C68 C67 165.6(11) . . . . no
C15 C16 C17 C12 -3(2) . . . . no
Dy2 O16 C68 C69 161.8(10) . . . . no
C21 C20 C25 C24 2.8(19) . . . . no
O5 C20 C25 C24 178.0(12) . . . . no
O5 C20 C21 C22 -175.0(10) . . . . no
O5 C20 C21 O6 2.2(14) . . . . no
C25 C20 C21 C22 0.8(17) . . . . no
C25 C20 C21 O6 178.0(10) . . . . no
O6 C21 C22 C23 179.5(11) . . . . no
O6 C21 C22 C26 -7.1(18) . . . . no
C20 C21 C22 C23 -3.5(17) . . . . no
C20 C21 C22 C26 169.9(11) . . . . no
C23 C22 C26 N3 -179.2(13) . . . . no
C21 C22 C26 N3 7(2) . . . . no
C21 C22 C23 C24 3(2) . . . . no
C26 C22 C23 C24 -170.8(13) . . . . no
C22 C23 C24 C25 1(2) . . . . no
C23 C24 C25 C20 -3(2) . . . . no
N3 C27 C28 N4 38.0(14) . . . . no
N4 C29 C30 C31 167.5(13) . . . . no
N4 C29 C30 C35 -17(2) . . . . no
C31 C30 C35 C34 2.2(17) . . . . no
C31 C30 C35 O7 178.5(10) . . . . no
C35 C30 C31 C32 -0.2(17) . . . . no
C29 C30 C31 C32 175.2(11) . . . . no
C29 C30 C35 O7 3.2(17) . . . . no
C29 C30 C35 C34 -173.2(11) . . . . no
C30 C31 C32 C33 -1.0(19) . . . . no
C31 C32 C33 C34 0.3(19) . . . . no
C32 C33 C34 O8 -175.6(11) . . . . no
C32 C33 C34 C35 1.7(17) . . . . no
C33 C34 C35 O7 -179.4(10) . . . . no
C33 C34 C35 C30 -3.0(17) . . . . no
O8 C34 C35 O7 -1.9(14) . . . . no
O8 C34 C35 C30 174.6(10) . . . . no
Zn3 N5 C45 C46 15.8(16) . . . . no
C44 N5 C45 C46 -158.3(13) . . . . no
C45 N5 C44 C40 -173.0(12) . . . . no
Zn3 N5 C44 C40 13.6(17) . . . . no
C47 N6 C46 C45 -138.1(15) . . . . no
Zn3 N6 C47 C48 -4(2) . . . . no
C46 N6 C47 C48 179.4(13) . . . . no
Zn3 N6 C46 C45 44.8(15) . . . . no
Zn4 N7 C63 C64 -49.9(13) . . . . no
C63 N7 C62 C58 -171.6(13) . . . . no
Zn4 N7 C62 C58 2(2) . . . . no
C62 N7 C63 C64 125.1(14) . . . . no
Zn4 N8 C65 C66 -2(2) . . . . no
C65 N8 C64 C63 177.8(14) . . . . no
Zn4 N8 C64 C63 -10.3(15) . . . . no
C64 N8 C65 C66 169.3(15) . . . . no
C73 O17 C74 C75 -173.8(10) . . . . no
Dy3 O17 C74 C79 -158.6(10) . . . . no
Dy3 O17 C74 C75 18.7(12) . . . . no
C73 O17 C74 C79 8.9(16) . . . . no
Dy3 O18 C75 C76 150.9(9) . . . . no
Dy3 O18 C75 C74 -26.6(13) . . . . no
Zn5 O18 C75 C74 170.6(8) . . . . no
Zn5 O18 C75 C76 -11.9(15) . . . . no
Dy3 O19 C85 C86 24.2(12) . . . . no
Dy3 O19 C85 C84 -157.8(8) . . . . no
Zn5 O19 C85 C84 31.8(12) . . . . no
Zn5 O19 C85 C86 -146.2(7) . . . . no
Dy3 O20 C86 C85 -17.0(10) . . . . no
C90 O20 C86 C87 10.6(16) . . . . no
Dy3 O20 C86 C87 165.2(10) . . . . no
C90 O20 C86 C85 -171.6(10) . . . . no
C91 O21 C92 C93 -166.0(11) . . . . no
Dy3 O21 C92 C97 176.3(9) . . . . no
Dy3 O21 C92 C93 -2.4(12) . . . . no
C91 O21 C92 C97 12.6(16) . . . . no
Dy3 O22 C93 C94 -171.0(8) . . . . no
Dy3 O22 C93 C92 6.5(13) . . . . no
Zn6 O22 C93 C94 -10.7(15) . . . . no
Zn6 O22 C93 C92 166.9(7) . . . . no
Dy3 O23 C107 C102 164.5(14) . . . . no
Dy3 O23 C107 C106 -12.1(17) . . . . no
Zn6 O23 C107 C102 -21(2) . . . . no
Zn6 O23 C107 C106 162.6(9) . . . . no
Dy3 O24 C106 C105 -168.7(15) . . . . no
C108 O24 C106 C105 11(2) . . . . no
Dy3 O24 C106 C107 11.3(15) . . . . no
C108 O24 C106 C107 -169.3(12) . . . . no
O9 C38 C39 C40 -179.1(9) . . . . no
O9 C38 C39 O10 3.0(14) . . . . no
O9 C38 C43 C42 -178.6(12) . . . . no
C43 C38 C39 O10 -178.5(11) . . . . no
C43 C38 C39 C40 -0.7(17) . . . . no
C39 C38 C43 C42 3.2(19) . . . . no
C38 C39 C40 C41 -1.1(16) . . . . no
O10 C39 C40 C41 176.6(10) . . . . no
O10 C39 C40 C44 -6.1(16) . . . . no
C38 C39 C40 C44 176.2(10) . . . . no
C44 C40 C41 C42 -177.0(12) . . . . no
C39 C40 C41 C42 0.3(18) . . . . no
C39 C40 C44 N5 14.9(18) . . . . no
C41 C40 C44 N5 -167.8(12) . . . . no
C40 C41 C42 C43 2(2) . . . . no
C41 C42 C43 C38 -4(2) . . . . no
N5 C45 C46 N6 -39.9(18) . . . . no
N6 C47 C48 C49 -10(2) . . . . no
N6 C47 C48 C53 170.0(14) . . . . no
C49 C48 C53 C52 -2(2) . . . . no
C47 C48 C53 C52 177.4(15) . . . . no
C47 C48 C49 C50 -172.3(13) . . . . no
C53 C48 C49 O11 -179.2(11) . . . . no
C47 C48 C49 O11 1(2) . . . . no
C53 C48 C49 C50 7.3(17) . . . . no
C48 C49 C50 O12 171.5(10) . . . . no
O11 C49 C50 O12 -2.3(16) . . . . no
O11 C49 C50 C51 179.5(12) . . . . no
C48 C49 C50 C51 -6.7(19) . . . . no
O12 C50 C51 C52 -177.5(12) . . . . no
C49 C50 C51 C52 1(2) . . . . no
C50 C51 C52 C53 5(2) . . . . no
C51 C52 C53 C48 -4(2) . . . . no
C61 C56 C57 O14 -176.9(12) . . . . no
C61 C56 C57 C58 2.7(19) . . . . no
O13 C56 C61 C60 176.6(12) . . . . no
C57 C56 C61 C60 -1(2) . . . . no
O13 C56 C57 O14 5.1(16) . . . . no
O13 C56 C57 C58 -175.3(10) . . . . no
O14 C57 C58 C62 -8(2) . . . . no
O14 C57 C58 C59 177.9(12) . . . . no
C56 C57 C58 C59 -1.7(18) . . . . no
C56 C57 C58 C62 172.0(12) . . . . no
C57 C58 C59 C60 -1(2) . . . . no
C59 C58 C62 N7 177.9(13) . . . . no
C62 C58 C59 C60 -175.1(13) . . . . no
C57 C58 C62 N7 4(2) . . . . no
C58 C59 C60 C61 3(2) . . . . no
C59 C60 C61 C56 -2(2) . . . . no
N7 C63 C64 N8 39.0(16) . . . . no
N8 C65 C66 C71 178.7(17) . . . . no
N8 C65 C66 C67 -5(3) . . . . no
C67 C66 C71 C70 5(3) . . . . no
C71 C66 C67 O15 176.4(14) . . . . no
C65 C66 C71 C70 -178.5(17) . . . . no
C71 C66 C67 C68 -4(2) . . . . no
C65 C66 C67 C68 180.0(13) . . . . no
C65 C66 C67 O15 0(2) . . . . no
O15 C67 C68 O16 0.8(16) . . . . no
C66 C67 C68 O16 -179.3(11) . . . . no
C66 C67 C68 C69 2.5(19) . . . . no
O15 C67 C68 C69 -177.5(12) . . . . no
C67 C68 C69 C70 -3(2) . . . . no
O16 C68 C69 C70 179.4(12) . . . . no
C68 C69 C70 C71 4(2) . . . . no
C69 C70 C71 C66 -5(3) . . . . no
Zn5 N9 C80 C76 4.3(18) . . . . no
C81 N9 C80 C76 179.8(11) . . . . no
Zn5 N9 C81 C82 -46.7(14) . . . . no
C80 N9 C81 C82 137.0(14) . . . . no
Zn5 N10 C82 C81 -14.1(16) . . . . no
C83 N10 C82 C81 158.8(13) . . . . no
Zn5 N10 C83 C84 -13.0(17) . . . . no
C82 N10 C83 C84 175.0(13) . . . . no
Zn6 N11 C98 C94 5(2) . . . . no
C99 N11 C98 C94 171.4(12) . . . . no
Zn6 N11 C99 C100 52.1(12) . . . . no
C98 N11 C99 C100 -117.2(14) . . . . no
Zn6 N12 C100 C99 12.2(14) . . . . no
C101 N12 C100 C99 -175.8(13) . . . . no
Zn6 N12 C101 C102 -4(3) . . . . no
C100 N12 C101 C102 -175.7(18) . . . . no
C127 O25 C128 C129 171.8(9) . . . . no
Dy4 O25 C128 C129 1.3(10) . . . . no
Dy4 O25 C128 C133 -176.9(8) . . . . no
C127 O25 C128 C133 -6.4(15) . . . . no
Zn7 O26 C129 C128 -179.3(6) . . . . no
Dy4 O26 C129 C128 6.2(12) . . . . no
Dy4 O26 C129 C130 -174.6(7) . . . . no
Zn7 O26 C129 C130 -0.1(14) . . . . no
Dy4 O27 C139 C140 2.1(14) . . . . no
Dy4 O27 C139 C138 179.2(7) . . . . no
Zn7 O27 C139 C138 -32.5(14) . . . . no
Zn7 O27 C139 C140 150.4(8) . . . . no
C144 O28 C140 C139 179.2(11) . . . . no
Dy4 O28 C140 C139 -9.4(11) . . . . no
Dy4 O28 C140 C141 172.4(9) . . . . no
C144 O28 C140 C141 1.1(16) . . . . no
Dy4 O29 C122 C123 153.2(9) . . . . no
Dy4 O29 C122 C121 -26.3(9) . . . . no
C126 O29 C122 C121 -174.7(9) . . . . no
C126 O29 C122 C123 4.8(14) . . . . no
Dy4 O30 C121 C122 34.1(11) . . . . no
Dy4 O30 C121 C120 -141.3(8) . . . . no
Zn8 O30 C121 C120 33.4(12) . . . . no
Zn8 O30 C121 C122 -151.3(7) . . . . no
Dy4 O31 C115 C110 -30.0(12) . . . . no
Zn8 O31 C115 C114 -6.9(15) . . . . no
Dy4 O31 C115 C114 147.2(9) . . . . no
Zn8 O31 C115 C110 176.0(7) . . . . no
C109 O32 C110 C111 -0.1(16) . . . . no
Dy4 O32 C110 C111 -153.9(10) . . . . no
Dy4 O32 C110 C115 29.5(11) . . . . no
C109 O32 C110 C115 -176.8(10) . . . . no
O17 C74 C75 O18 2.0(14) . . . . no
O17 C74 C75 C76 -175.7(10) . . . . no
C79 C74 C75 O18 179.4(11) . . . . no
C79 C74 C75 C76 1.7(18) . . . . no
O17 C74 C79 C78 175.7(11) . . . . no
C75 C74 C79 C78 -1.4(19) . . . . no
O18 C75 C76 C77 -178.5(11) . . . . no
O18 C75 C76 C80 -5.5(19) . . . . no
C74 C75 C76 C77 -1.0(17) . . . . no
C74 C75 C76 C80 172.0(11) . . . . no
C75 C76 C77 C78 0(2) . . . . no
C80 C76 C77 C78 -173.5(13) . . . . no
C75 C76 C80 N9 10.0(19) . . . . no
C77 C76 C80 N9 -176.9(12) . . . . no
C76 C77 C78 C79 0(2) . . . . no
C77 C78 C79 C74 0(2) . . . . no
N9 C81 C82 N10 38.4(17) . . . . no
N10 C83 C84 C85 -15.4(19) . . . . no
N10 C83 C84 C89 166.9(12) . . . . no
C83 C84 C85 O19 4.2(17) . . . . no
C83 C84 C85 C86 -177.9(11) . . . . no
C89 C84 C85 O19 -178.1(10) . . . . no
C89 C84 C85 C86 -0.2(16) . . . . no
C83 C84 C89 C88 179.5(13) . . . . no
C85 C84 C89 C88 1.7(19) . . . . no
O19 C85 C86 O20 0.6(13) . . . . no
O19 C85 C86 C87 178.6(10) . . . . no
C84 C85 C86 O20 -177.5(9) . . . . no
C84 C85 C86 C87 0.5(16) . . . . no
O20 C86 C87 C88 175.5(11) . . . . no
C85 C86 C87 C88 -2.2(19) . . . . no
C86 C87 C88 C89 4(2) . . . . no
C87 C88 C89 C84 -3(2) . . . . no
C97 C92 C93 C94 -2.9(17) . . . . no
O21 C92 C97 C96 -176.3(11) . . . . no
C93 C92 C97 C96 2.2(18) . . . . no
O21 C92 C93 C94 175.7(9) . . . . no
C97 C92 C93 O22 179.3(11) . . . . no
O21 C92 C93 O22 -2.1(14) . . . . no
O22 C93 C94 C98 8.3(18) . . . . no
O22 C93 C94 C95 -179.4(11) . . . . no
C92 C93 C94 C95 3.1(17) . . . . no
C92 C93 C94 C98 -169.3(11) . . . . no
C93 C94 C95 C96 -3(2) . . . . no
C95 C94 C98 N11 -178.0(13) . . . . no
C98 C94 C95 C96 170.6(13) . . . . no
C93 C94 C98 N11 -5(2) . . . . no
C94 C95 C96 C97 2(2) . . . . no
C95 C96 C97 C92 -2(2) . . . . no
N11 C99 C100 N12 -41.8(14) . . . . no
N12 C101 C102 C103 -167.7(19) . . . . no
N12 C101 C102 C107 17(3) . . . . no
C101 C102 C107 O23 -3(3) . . . . no
C101 C102 C107 C106 173(2) . . . . no
C103 C102 C107 C106 -2(3) . . . . no
C107 C102 C103 C104 5(3) . . . . no
C103 C102 C107 O23 -178.8(16) . . . . no
C101 C102 C103 C104 -171(2) . . . . no
C102 C103 C104 C105 -7(4) . . . . no
C103 C104 C105 C106 6(3) . . . . no
C104 C105 C106 C107 -4(3) . . . . no
C104 C105 C106 O24 175.9(18) . . . . no
O24 C106 C107 O23 -1.1(18) . . . . no
O24 C106 C107 C102 -177.8(15) . . . . no
C105 C106 C107 O23 178.9(16) . . . . no
C105 C106 C107 C102 2(3) . . . . no
Zn8 N13 C116 C114 6.1(18) . . . . no
C117 N13 C116 C114 -175.1(11) . . . . no
Zn8 N13 C117 C118 -49.4(11) . . . . no
C116 N13 C117 C118 131.5(12) . . . . no
Zn8 N14 C118 C117 -14.5(12) . . . . no
C119 N14 C118 C117 167.4(11) . . . . no
Zn8 N14 C119 C120 -7.4(17) . . . . no
C118 N14 C119 C120 170.6(11) . . . . no
Zn7 N15 C134 C130 -5.3(18) . . . . no
C135 N15 C134 C130 174.7(11) . . . . no
Zn7 N15 C135 C136 48.0(12) . . . . no
C134 N15 C135 C136 -131.9(13) . . . . no
Zn7 N16 C136 C135 16.9(11) . . . . no
C137 N16 C136 C135 -166.7(11) . . . . no
Zn7 N16 C137 C138 0.4(16) . . . . no
C136 N16 C137 C138 -175.5(10) . . . . no
O32 C110 C111 C112 -179.4(12) . . . . no
C115 C110 C111 C112 -2.9(18) . . . . no
O32 C110 C115 O31 -3.4(14) . . . . no
O32 C110 C115 C114 179.3(10) . . . . no
C111 C110 C115 O31 179.8(10) . . . . no
C111 C110 C115 C114 2.4(17) . . . . no
C110 C111 C112 C113 2(2) . . . . no
C111 C112 C113 C114 -1(2) . . . . no
C112 C113 C114 C115 0(2) . . . . no
C112 C113 C114 C116 -172.2(14) . . . . no
C113 C114 C115 O31 -178.2(11) . . . . no
C113 C114 C115 C110 -1.1(17) . . . . no
C116 C114 C115 O31 -6.2(18) . . . . no
C116 C114 C115 C110 170.9(11) . . . . no
C113 C114 C116 N13 178.8(13) . . . . no
C115 C114 C116 N13 7(2) . . . . no
N13 C117 C118 N14 41.8(13) . . . . no
N14 C119 C120 C121 -13.9(19) . . . . no
N14 C119 C120 C125 171.4(11) . . . . no
C119 C120 C121 O30 -0.3(17) . . . . no
C119 C120 C121 C122 -175.6(10) . . . . no
C125 C120 C121 O30 174.1(10) . . . . no
C125 C120 C121 C122 -1.2(16) . . . . no
C119 C120 C125 C124 176.5(11) . . . . no
C121 C120 C125 C124 1.6(18) . . . . no
O30 C121 C122 O29 3.0(13) . . . . no
O30 C121 C122 C123 -176.5(9) . . . . no
C120 C121 C122 O29 178.6(9) . . . . no
C120 C121 C122 C123 -0.9(16) . . . . no
O29 C122 C123 C124 -177.0(10) . . . . no
C121 C122 C123 C124 2.5(16) . . . . no
C122 C123 C124 C125 -2.1(18) . . . . no
C123 C124 C125 C120 0.1(19) . . . . no
O25 C128 C129 O26 -4.3(12) . . . . no
O25 C128 C129 C130 176.4(8) . . . . no
C133 C128 C129 O26 174.0(10) . . . . no
C133 C128 C129 C130 -5.3(15) . . . . no
O25 C128 C133 C132 -177.3(10) . . . . no
C129 C128 C133 C132 4.7(17) . . . . no
O26 C129 C130 C131 -176.6(9) . . . . no
O26 C129 C130 C134 8.7(16) . . . . no
C128 C129 C130 C131 2.6(14) . . . . no
C128 C129 C130 C134 -172.1(10) . . . . no
C129 C130 C131 C132 0.5(16) . . . . no
C134 C130 C131 C132 175.4(10) . . . . no
C129 C130 C134 N15 -6.1(18) . . . . no
C131 C130 C134 N15 179.1(11) . . . . no
C130 C131 C132 C133 -1.2(18) . . . . no
C131 C132 C133 C128 -1.3(17) . . . . no
N15 C135 C136 N16 -43.4(14) . . . . no
N16 C137 C138 C139 23.0(18) . . . . no
N16 C137 C138 C143 -161.9(12) . . . . no
C137 C138 C139 O27 -5.0(17) . . . . no
C137 C138 C139 C140 172.0(10) . . . . no
C143 C138 C139 O27 179.8(11) . . . . no
C143 C138 C139 C140 -3.2(16) . . . . no
C137 C138 C143 C142 -179.9(13) . . . . no
C139 C138 C143 C142 -4.4(19) . . . . no
O27 C139 C140 O28 5.4(14) . . . . no
O27 C139 C140 C141 -176.4(10) . . . . no
C138 C139 C140 O28 -171.8(9) . . . . no
C138 C139 C140 C141 6.4(17) . . . . no
O28 C140 C141 C142 176.0(11) . . . . no
C139 C140 C141 C142 -1.9(17) . . . . no
C140 C141 C142 C143 -5.8(19) . . . . no
C141 C142 C143 C138 9(2) . . . . no

loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
_geom_hbond_publ_flag
#
#D   H   A   D - H  H...A   D...A    D - H...A  symm(A)
#
O2W H2WA Cl6 1.0100 2.4200 3.409(7) 166.00 . yes
O2W H2WB Cl4 1.0000 2.4400 3.287(8) 141.00 . yes
O3W H3WA Cl6 0.9500 2.2700 3.194(9) 163.00 . yes
O3W H3WB Cl4 0.9500 2.1900 3.088(9) 157.00 . yes
O4W H4WA Cl7 0.8500 2.3600 3.172(9) 161.00 . yes
O4W H4WB O5W 0.8500 2.4500 2.733(17) 101.00 . yes
O4W H4WB O28 0.8500 2.4900 2.899(12) 111.00 . yes
O5W H5WA O4W 0.8500 2.4400 2.733(17) 101.00 . yes
O5W H5WB Cl13 0.8500 2.8200 3.231(18) 112.00 . yes
C1 H1C Cl2 0.9600 2.5700 3.46(2) 153.00 . yes
C8 H8 Cl3 0.9300 2.6000 3.449(18) 153.00 2_667 yes
C108 H10D Cl4 0.9600 2.6900 3.416(15) 133.00 . yes
C109 H10F O26 0.9600 2.6000 3.219(15) 123.00 . yes
C127 H12F Cl8 0.9600 2.7800 3.518(15) 134.00 . yes
C135 H13B Cl1 0.9700 2.8100 3.563(12) 136.00 2_667 yes
C32 H32 Cl3 0.9300 2.8200 3.459(13) 127.00 2_567 yes
C47 H47 Cl15 0.9300 2.7300 3.638(17) 164.00 . yes
C53 H53 Cl19 0.9300 2.5500 3.37(2) 147.00 . yes
C54 H54C O14 0.9600 2.5500 3.272(18) 132.00 . yes
C55 H55A Cl3 0.9600 2.6500 3.531(14) 153.00 . yes
C90 H90C O22 0.9600 2.5100 3.202(16) 129.00 . yes
C91 H91C Cl5 0.9600 2.7300 3.514(15) 140.00 . yes
C91 H91C O18 0.9600 2.5200 3.197(16) 128.00 . yes
C112 H112 Cl20 0.9300 2.8200 3.61(2) 143.00 2_666 yes
C113 H113 Cl18 0.9300 2.6200 3.49(2) 155.00 2_666 yes
C134 H134 Cl5 0.9300 2.6700 3.475(13) 146.00 1_565 yes
C137 H137 Cl19 0.9300 2.7800 3.659(19) 157.00 1_655 yes

# Loop Mechanism for Extra Tables(s)

#loop_
#_publ_manuscript_incl_extra_item
#'_geom_extra_tableA_col_1'
#'_geom_extra_tableA_col_2'
#'_geom_extra_tableA_col_3'
#'_geom_extra_table_head_A'
#'_geom_table_footnote_A'
#'_geom_extra_tableB_col_1'
#'_geom_extra_tableB_col_2'
#'_geom_extra_tableB_col_3'
#'_geom_extra_table_head_B'
#'_geom_table_footnote_B'


#
#loop_
#_geom_extra_tableA_col_1
#_geom_extra_tableA_col_2
#_geom_extra_tableA_col_3
# ? ? ?


#
#loop_
#_geom_extra_tableB_col_1
#_geom_extra_tableB_col_2
#_geom_extra_tableB_col_3
# ? ? ?


#
#_geom_table_footnote_A
#;
# ?
#;


#
#_geom_table_footnote_B
#;
# ?
#;


#
#_geom_table_footnote_A
#;
# ?
#;


#
#_geom_table_footnote_B
#;
# ?
#;


#===END



_exptl_crystal_preparation       'Magnetic properties,Luminescent'
