# Electronic Supplementary Material (ESI) for Chemical Science.
# This journal is © The Royal Society of Chemistry 2019

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_Lu2@Td-C76
_database_code_depnum_ccdc_archive 'CCDC 1582214'
_audit_update_record             
;
2017-10-26 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2@Td-C76 Ni(OEP)'
_chemical_name_common            'Lu2@Td-C76 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C76, C36 H44 N4 Ni, 2(C6 H6)'
_chemical_formula_sum            'C124 H56 Lu2 N4 Ni S0'
_chemical_formula_weight         2010.37

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0027 0.0014 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.2922 5.1425 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0053 0.0028 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3436 0.9622 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1098 0.1057 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   23.1698(6)
_cell_length_b                   13.7779(4)
_cell_length_c                   18.0308(4)
_cell_angle_alpha                90
_cell_angle_beta                 93.7760(10)
_cell_angle_gamma                90
_cell_volume                     5743.5(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9728
_cell_measurement_theta_min      2.907
_cell_measurement_theta_max      24.059

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.325
_exptl_crystal_F_000             3992
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.150
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.080
_exptl_absorpt_coefficient_mu    3.104
_shelx_estimated_absorpt_T_min   0.723
_shelx_estimated_absorpt_T_max   0.780
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.5694
_exptl_absorpt_correction_T_max  0.7450
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline BL17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            41184
_diffrn_reflns_av_unetI/netI     0.0267
_diffrn_reflns_av_R_equivalents  0.0435
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_h_max       28
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_theta_min         1.864
_diffrn_reflns_theta_max         24.072
_diffrn_reflns_theta_full        23.048
_diffrn_measured_fraction_theta_max 0.918
_diffrn_measured_fraction_theta_full 0.919
_diffrn_reflns_Laue_measured_fraction_max 0.918
_diffrn_reflns_Laue_measured_fraction_full 0.919
_diffrn_reflns_point_group_measured_fraction_max 0.918
_diffrn_reflns_point_group_measured_fraction_full 0.919
_reflns_number_total             5635
_reflns_number_gt                5454
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1185P)²+102.0963P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         5635
_refine_ls_number_parameters     782
_refine_ls_number_restraints     879
_refine_ls_R_factor_all          0.0937
_refine_ls_R_factor_gt           0.0921
_refine_ls_wR_factor_ref         0.2408
_refine_ls_wR_factor_gt          0.2396
_refine_ls_goodness_of_fit_ref   1.063
_refine_ls_restrained_S_all      1.073
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.30675(6) 0.37287(9) 0.29234(15) 0.0526(5) Uani 0.2441 1 d . . P A 1
Lu2 Lu 0.34087(5) 0.40690(9) 0.29450(8) 0.0280(3) Uani 0.213 1 d . . P A 1
Lu3 Lu 0.35927(18) 0.5551(5) 0.3830(2) 0.0627(14) Uani 0.1156 1 d . . P A 1
Lu4 Lu 0.23416(15) 0.5276(6) 0.2240(3) 0.043(3) Uani 0.104 1 d . . P A 1
Lu5 Lu 0.3177(3) 0.6210(4) 0.3408(3) 0.0506(12) Uani 0.0988 1 d . . P A 1
Lu6 Lu 0.3609(3) 0.5000 0.3900(4) 0.0382(15) Uani 0.0922 2 d S TU P A 1
Lu7 Lu 0.2417(9) 0.5000 0.2149(14) 0.117(11) Uani 0.0725 2 d S T P A 1
Lu8 Lu 0.2878(2) 0.5394(4) 0.2203(3) 0.0366(12) Uani 0.0552 1 d . . P A 1
Lu9 Lu 0.2321(8) 0.5515(12) 0.2409(13) 0.106(9) Uani 0.0449 1 d . . P A 1
Lu10 Lu 0.3391(5) 0.5841(8) 0.3598(8) 0.0281(16) Uiso 0.0369 1 d . U P A 1
Lu11 Lu 0.3195(11) 0.5000 0.4129(15) 0.012(5) Uiso 0.0103 2 d S . P A 1
C1 C 0.35727(11) 0.24599(18) 0.31383(13) 0.084(4) Uani 0.5 1 d G U P A -1
C2 C 0.37720(11) 0.2759(2) 0.38002(12) 0.077(4) Uani 0.5 1 d G U P A -1
C3 C 0.41551(9) 0.3433(2) 0.37250(8) 0.082(4) Uani 0.5 1 d G U P A -1
C4 C 0.42345(8) 0.35191(19) 0.30000(8) 0.088(4) Uani 0.5 1 d G U P A -1
C5 C 0.38709(8) 0.29320(16) 0.26663(11) 0.089(4) Uani 0.5 1 d G U P A -1
C6 C 0.36547(7) 0.30929(14) 0.20366(11) 0.076(4) Uani 0.5 1 d G U P A -1
C7 C 0.37602(5) 0.39049(13) 0.16901(7) 0.067(3) Uani 0.5 1 d G U P A -1
C8 C 0.41429(4) 0.44666(14) 0.19905(5) 0.084(4) Uani 0.5 1 d G U P A -1
C9 C 0.43552(6) 0.42824(17) 0.26341(5) 0.086(4) Uani 0.5 1 d G U P A -1
C10 C 0.45050(6) 0.4968(2) 0.30548(4) 0.091(3) Uani 0.5 1 d G U P A -1
C11 C 0.44752(8) 0.4898(2) 0.37810(4) 0.087(4) Uani 0.5 1 d G U P A -1
C12 C 0.42589(9) 0.4098(3) 0.40556(6) 0.091(4) Uani 0.5 1 d G U P A -1
C13 C 0.39540(11) 0.4198(3) 0.46424(6) 0.092(4) Uani 0.5 1 d G U P A -1
C14 C 0.35066(12) 0.3615(3) 0.47420(9) 0.080(4) Uani 0.5 1 d G U P A -1
C15 C 0.33407(12) 0.2948(3) 0.43144(12) 0.077(4) Uani 0.5 1 d G U P A -1
C16 C 0.28731(12) 0.2753(2) 0.41208(14) 0.080(4) Uani 0.5 1 d G U P A -1
C17 C 0.26954(11) 0.2419(2) 0.34407(16) 0.079(4) Uani 0.5 1 d G U P A -1
C18 C 0.30437(11) 0.22749(18) 0.29686(15) 0.075(4) Uani 0.5 1 d G U P A -1
C19 C 0.28095(9) 0.24737(16) 0.23445(15) 0.071(3) Uani 0.5 1 d G U P A -1
C20 C 0.31178(8) 0.28578(14) 0.18969(13) 0.072(4) Uani 0.5 1 d G U P A -1
C21 C 0.28792(5) 0.34903(16) 0.14301(11) 0.057(3) Uani 0.5 1 d G U P A -1
C22 C 0.32802(4) 0.41199(14) 0.12956(8) 0.050(3) Uani 0.5 1 d G U P A -1
C23 C 0.31413(3) 0.49305(15) 0.11216(8) 0.052(2) Uani 0.5 1 d G U P A -1
C24 C 0.35888(4) 0.56475(13) 0.14131(7) 0.060(3) Uani 0.5 1 d G U P A -1
C25 C 0.39990(4) 0.52707(13) 0.17807(5) 0.062(3) Uani 0.5 1 d G U P A -1
C26 C 0.41679(6) 0.60477(15) 0.22330(7) 0.068(3) Uani 0.5 1 d G U P A -1
C27 C 0.43927(6) 0.58579(18) 0.28476(6) 0.072(3) Uani 0.5 1 d G U P A -1
C28 C 0.43256(8) 0.6378(2) 0.34461(9) 0.073(4) Uani 0.5 1 d G U P A -1
C29 C 0.43450(9) 0.5773(3) 0.40065(6) 0.087(4) Uani 0.5 1 d G U P A -1
C30 C 0.39813(10) 0.5935(3) 0.45314(7) 0.089(4) Uani 0.5 1 d G U P A -1
C31 C 0.38522(11) 0.5102(3) 0.48775(6) 0.089(4) Uani 0.5 1 d G U P A -1
C32 C 0.33360(12) 0.5048(3) 0.51545(8) 0.076(3) Uani 0.5 1 d G U P A -1
C33 C 0.31358(12) 0.4156(3) 0.50732(9) 0.075(4) Uani 0.5 1 d G U P A -1
C34 C 0.26182(12) 0.3900(3) 0.48541(12) 0.073(4) Uani 0.5 1 d G U P A -1
C35 C 0.24347(12) 0.3213(3) 0.44106(14) 0.073(4) Uani 0.5 1 d G U P A -1
C36 C 0.19503(11) 0.3495(3) 0.40645(15) 0.079(4) Uani 0.5 1 d G U P A -1
C37 C 0.18319(9) 0.3236(2) 0.33743(16) 0.069(4) Uani 0.5 1 d G U P A -1
C38 C 0.22394(10) 0.2668(2) 0.30840(16) 0.070(3) Uani 0.5 1 d G U P A -1
C39 C 0.23096(9) 0.27405(19) 0.24202(15) 0.063(4) Uani 0.5 1 d G U P A -1
C40 C 0.20148(6) 0.3393(2) 0.19616(15) 0.058(3) Uani 0.5 1 d G U P A -1
C41 C 0.22935(5) 0.38579(19) 0.13832(12) 0.058(3) Uani 0.5 1 d G U P A -1
C42 C 0.21919(3) 0.4707(2) 0.11712(12) 0.062(3) Uani 0.5 1 d G U P A -1
C43 C 0.26040(3) 0.53363(18) 0.10560(10) 0.056(3) Uani 0.5 1 d G U P A -1
C44 C 0.25205(5) 0.62612(18) 0.13469(12) 0.056(3) Uani 0.5 1 d G U P A -1
C45 C 0.29298(7) 0.67962(15) 0.16708(12) 0.060(4) Uani 0.5 1 d G U P A -1
C46 C 0.34637(6) 0.64482(13) 0.16201(10) 0.060(3) Uani 0.5 1 d G U P A -1
C47 C 0.38928(7) 0.66770(14) 0.21783(10) 0.060(3) Uani 0.5 1 d G U P A -1
C48 C 0.37339(9) 0.73189(16) 0.26758(13) 0.068(4) Uani 0.5 1 d G U P A -1
C49 C 0.39328(10) 0.7100(2) 0.33829(12) 0.052(3) Uani 0.5 1 d G U P A -1
C50 C 0.35035(11) 0.7284(2) 0.38313(13) 0.066(3) Uani 0.5 1 d G U P A -1
C51 C 0.35937(11) 0.6657(3) 0.44961(11) 0.080(4) Uani 0.5 1 d G U P A -1
C52 C 0.30613(12) 0.6562(3) 0.46944(12) 0.078(4) Uani 0.5 1 d G U P A -1
C53 C 0.29488(12) 0.5749(3) 0.50619(10) 0.077(4) Uani 0.5 1 d G U P A -1
C54 C 0.23975(11) 0.5534(3) 0.49041(12) 0.069(4) Uani 0.5 1 d G U P A -1
C55 C 0.22125(11) 0.4641(3) 0.47893(12) 0.076(4) Uani 0.5 1 d G U P A -1
C56 C 0.17693(10) 0.4463(3) 0.43249(14) 0.069(4) Uani 0.5 1 d G U P A -1
C57 C 0.15530(9) 0.5121(3) 0.38231(15) 0.067(3) Uani 0.5 1 d G U P A -1
C58 C 0.13700(7) 0.4782(3) 0.31791(16) 0.059(3) Uani 0.5 1 d G U P A -1
C59 C 0.15219(7) 0.3888(2) 0.29696(16) 0.066(3) Uani 0.5 1 d G U P A -1
C60 C 0.16008(6) 0.3932(2) 0.22479(15) 0.061(3) Uani 0.5 1 d G U P A -1
C61 C 0.14930(4) 0.4828(2) 0.20026(15) 0.060(3) Uani 0.5 1 d G U P A -1
C62 C 0.17605(4) 0.5265(2) 0.14967(14) 0.065(4) Uani 0.5 1 d G U P A -1
C63 C 0.19472(5) 0.6138(2) 0.15477(14) 0.061(3) Uani 0.5 1 d G U P A -1
C64 C 0.18251(7) 0.6651(2) 0.21799(16) 0.056(3) Uani 0.5 1 d G U P A -1
C65 C 0.22296(9) 0.72287(19) 0.23887(16) 0.050(3) Uani 0.5 1 d G U P A -1
C66 C 0.27333(9) 0.72546(16) 0.21089(15) 0.061(3) Uani 0.5 1 d G U P A -1
C67 C 0.31747(10) 0.75524(16) 0.26811(15) 0.066(3) Uani 0.5 1 d G U P A -1
C68 C 0.30397(11) 0.7601(2) 0.33978(15) 0.069(4) Uani 0.5 1 d G U P A -1
C69 C 0.24285(11) 0.7237(2) 0.37378(16) 0.078(4) Uani 0.5 1 d G U P A -1
C70 C 0.25660(11) 0.6864(3) 0.43350(14) 0.071(4) Uani 0.5 1 d G U P A -1
C71 C 0.21539(11) 0.6217(3) 0.44671(14) 0.065(3) Uani 0.5 1 d G U P A -1
C72 C 0.17226(10) 0.6028(3) 0.39303(15) 0.057(3) Uani 0.5 1 d G U P A -1
C73 C 0.16947(9) 0.6533(2) 0.33263(16) 0.054(2) Uani 0.5 1 d G U P A -1
C74 C 0.21232(10) 0.7172(2) 0.32851(16) 0.058(3) Uani 0.5 1 d G U P A -1
C75 C 0.15505(7) 0.6312(2) 0.26778(16) 0.053(2) Uani 0.5 1 d G U P A -1
C76 C 0.13610(6) 0.5353(3) 0.25808(16) 0.053(3) Uani 0.5 1 d G U P A -1
Ni1A Ni 0.48106(3) 0.50000(15) 0.08475(4) 0.0093(3) Uani 1 2 d G T P A 2
N1A N 0.47984(5) 0.36832(15) 0.08616(7) 0.0114(8) Uani 1 1 d G . . A 2
N2A N 0.53559(3) 0.50000(18) 0.16135(5) 0.0127(11) Uani 1 2 d G T P A 2
N4A N 0.42440(4) 0.49999(16) 0.01101(4) 0.0112(11) Uani 1 2 d G T P A 2
C1A C 0.50988(6) 0.31130(16) 0.12957(10) 0.0168(10) Uani 1 1 d G U . A 2
C2A C 0.44785(6) 0.31122(15) 0.04535(9) 0.0152(10) Uani 1 1 d G U . A 2
C3A C 0.41022(6) 0.33912(17) -0.00502(8) 0.0138(7) Uani 1 1 d G U . A 2
H3A H 0.3900 0.2916 -0.0326 0.017 Uiso 1 1 calc R U . A 2
C4A C 0.39855(18) 0.4267(3) -0.0201(3) 0.0138(6) Uani 1 1 d . U . A 2
C5A C 0.35642(18) 0.4546(4) -0.0693(3) 0.0143(6) Uani 1 1 d . U . A 2
C6A C 0.31798(18) 0.3911(3) -0.1079(3) 0.0155(7) Uani 1 1 d . U . A 2
H6A1 H 0.3389 0.3347 -0.1237 0.019 Uiso 1 1 calc R U . A 2
H6A2 H 0.3009 0.4232 -0.1519 0.019 Uiso 1 1 calc R U . A 2
C7A C 0.4578(2) 0.2184(3) 0.0640(3) 0.0189(10) Uani 1 1 d . U . A 2
C8A C 0.4276(2) 0.1405(3) 0.0298(4) 0.0271(13) Uani 1 1 d . U . A 2
H8A1 H 0.4490 0.0810 0.0401 0.033 Uiso 1 1 calc R U . A 2
H8A2 H 0.4248 0.1503 -0.0236 0.033 Uiso 1 1 calc R U . A 2
C9A C 0.3707(2) 0.1306(4) 0.0554(4) 0.0353(15) Uani 1 1 d . U . A 2
H9A1 H 0.3734 0.1139 0.1072 0.053 Uiso 1 1 calc R U . A 2
H9A2 H 0.3503 0.0805 0.0276 0.053 Uiso 1 1 calc R U . A 2
H9A3 H 0.3503 0.1909 0.0485 0.053 Uiso 1 1 calc R U . A 2
C10A C 0.4961(2) 0.2185(3) 0.1156(3) 0.0201(10) Uani 1 1 d . U . A 2
C11A C 0.5195(2) 0.1403(4) 0.1576(4) 0.0296(13) Uani 1 1 d . U . A 2
H11A H 0.5123 0.0806 0.1300 0.035 Uiso 1 1 calc R U . A 2
H11B H 0.5611 0.1487 0.1649 0.035 Uiso 1 1 calc R U . A 2
C12A C 0.4963(3) 0.1321(5) 0.2268(4) 0.0402(17) Uani 1 1 d . U . A 2
H12A H 0.5031 0.1912 0.2543 0.060 Uiso 1 1 calc R U . A 2
H12B H 0.5144 0.0790 0.2538 0.060 Uiso 1 1 calc R U . A 2
H12C H 0.4554 0.1206 0.2200 0.060 Uiso 1 1 calc R U . A 2
C13A C 0.54710(19) 0.3391(4) 0.1800(3) 0.0164(10) Uani 1 1 d . U . A 2
H13A H 0.5676 0.2915 0.2072 0.020 Uiso 1 1 calc R U . A 2
C14A C 0.55835(19) 0.4267(4) 0.1959(3) 0.0154(9) Uani 1 1 d . U . A 2
C15A C 0.59456(19) 0.4545(4) 0.2530(3) 0.0174(10) Uani 1 1 d . U . A 2
C16A C 0.6224(2) 0.3907(4) 0.3035(3) 0.0236(11) Uani 1 1 d . U . A 2
H16A H 0.6539 0.4246 0.3307 0.028 Uiso 1 1 calc R U . A 2
H16B H 0.6390 0.3378 0.2765 0.028 Uiso 1 1 calc R U . A 2
C17A C 0.5850(3) 0.3522(5) 0.3545(4) 0.0298(13) Uani 1 1 d . U . A 2
H17A H 0.5685 0.4043 0.3815 0.045 Uiso 1 1 calc R U . A 2
H17B H 0.6063 0.3100 0.3886 0.045 Uiso 1 1 calc R U . A 2
H17C H 0.5547 0.3162 0.3281 0.045 Uiso 1 1 calc R U . A 2
C18A C 0.2735(2) 0.3611(5) -0.0623(4) 0.0289(13) Uani 1 1 d . U . A 2
H18A H 0.2462 0.3182 -0.0854 0.035 Uiso 1 1 d R U . A 2
H18B H 0.2536 0.4164 -0.0449 0.035 Uiso 1 1 d R U . A 2
H18C H 0.2921 0.3276 -0.0189 0.035 Uiso 1 1 d R U . A 2
C1B C 0.3574(4) 0.0000 0.2369(6) 0.0350(19) Uani 1 2 d S TU P B 3
H1B H 0.3845 0.0000 0.2011 0.042 Uiso 1 2 calc R U P B 3
C2B C 0.3746(4) 0.0000 0.3070(7) 0.048(2) Uani 1 2 d S TU P B 3
H2B H 0.4139 0.0000 0.3213 0.058 Uiso 1 2 calc R U P B 3
C3B C 0.3378(5) 0.0000 0.3556(7) 0.056(3) Uani 1 2 d S TU P B 3
H3B H 0.3499 0.0000 0.4058 0.067 Uiso 1 2 calc R U P B 3
C4B C 0.2829(5) 0.0000 0.3353(6) 0.046(2) Uani 1 2 d S TU P B 3
H4B H 0.2559 0.0000 0.3712 0.055 Uiso 1 2 calc R U P B 3
C5B C 0.2665(4) 0.0000 0.2690(6) 0.0351(19) Uani 1 2 d S TU P B 3
H5B H 0.2271 0.0000 0.2549 0.042 Uiso 1 2 calc R U P B 3
C6B C 0.3051(4) 0.0000 0.2175(5) 0.0307(17) Uani 1 2 d S TU P B 3
H6B H 0.2929 0.0000 0.1673 0.037 Uiso 1 2 calc R U P B 3
C7B C 0.5321(3) 0.1376(8) 0.4382(6) 0.065(2) Uani 1 1 d D U . C 4
H7B H 0.5538 0.1448 0.3970 0.078 Uiso 1 1 calc R U . C 4
C8B C 0.4712(4) 0.1318(9) 0.4338(7) 0.081(3) Uani 1 1 d D U . C 4
H8B H 0.4517 0.1282 0.3872 0.098 Uiso 1 1 calc R U . C 4
C9B C 0.5565(4) 0.1314(10) 0.5123(6) 0.084(3) Uani 1 1 d D U . C 4
H9B H 0.5965 0.1266 0.5195 0.101 Uiso 1 1 calc R U . C 4


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu5 0.898(4) 6_565 ?
Lu1 Lu2 0.9177(18) . ?
Lu1 Lu10 1.507(17) 6_565 ?
Lu1 Lu8 1.807(7) 6_565 ?
Lu1 C18 2.006(3) . ?
Lu1 C19 2.087(3) . ?
Lu1 C1 2.125(3) . ?
Lu1 Lu9 2.174(17) 6_565 ?
Lu1 Lu3 2.208(6) 6_565 ?
Lu1 C20 2.215(3) . ?
Lu1 C17 2.231(3) . ?
Lu1 C5 2.236(2) . ?
Lu2 Lu5 1.092(5) 6_565 ?
Lu2 Lu10 1.187(14) 6_565 ?
Lu2 Lu3 1.707(6) 6_565 ?
Lu2 Lu8 1.906(6) 6_565 ?
Lu2 C5 1.981(2) . ?
Lu2 C4 2.054(2) . ?
Lu2 Lu6 2.173(6) . ?
Lu2 C6 2.222(2) . ?
Lu2 C1 2.272(3) . ?
Lu2 C9 2.3176(18) . ?
Lu2 C3 2.327(2) . ?
Lu3 Lu10 0.727(14) . ?
Lu3 Lu6 0.770(7) . ?
Lu3 Lu11 1.33(2) . ?
Lu3 Lu5 1.496(7) . ?
Lu3 Lu3 1.518(13) 6_565 ?
Lu3 C30 1.594(4) . ?
Lu3 Lu2 1.707(6) 6_565 ?
Lu3 C29 1.778(4) . ?
Lu3 C51 1.940(5) . ?
Lu3 Lu10 2.011(17) 6_565 ?
Lu3 C31 2.040(6) . ?
Lu3 C28 2.195(5) . ?
Lu4 Lu4 0.762(16) 6_565 ?
Lu4 Lu9 1.134(17) 6_565 ?
Lu4 Lu8 1.259(7) . ?
Lu4 Lu8 1.553(8) 6_565 ?
Lu4 C62 1.836(5) . ?
Lu4 C63 1.911(6) . ?
Lu4 C61 2.078(5) . ?
Lu4 C42 2.088(7) . ?
Lu4 C44 2.166(5) . ?
Lu4 C64 2.240(7) . ?
Lu4 C43 2.259(5) . ?
Lu4 C76 2.395(3) . ?
Lu5 Lu10 0.774(13) . ?
Lu5 Lu1 0.898(4) 6_565 ?
Lu5 Lu2 1.093(5) 6_565 ?
Lu5 C50 1.807(4) . ?
Lu5 C68 1.942(6) . ?
Lu5 Lu6 2.111(8) . ?
Lu5 Lu11 2.114(18) . ?
Lu5 C49 2.141(4) . ?
Lu5 C51 2.216(5) . ?
Lu5 C67 2.266(6) . ?
Lu5 C69 2.344(7) . ?
Lu6 Lu3 0.770(7) 6_565 ?
Lu6 Lu11 1.07(3) . ?
Lu6 Lu10 1.364(16) 6_565 ?
Lu6 Lu10 1.364(16) . ?
Lu6 C31 1.819(7) . ?
Lu6 C13 1.873(6) . ?
Lu6 C30 1.889(6) . ?
Lu6 C12 1.958(6) . ?
Lu6 C29 2.009(6) . ?
Lu6 C11 2.037(6) . ?
Lu6 Lu5 2.111(8) 6_565 ?
Lu7 Lu4 0.454(15) 6_565 ?
Lu7 Lu9 0.89(2) . ?
Lu7 Lu9 0.89(2) 6_565 ?
Lu7 Lu8 1.197(18) 6_565 ?
Lu7 Lu8 1.197(18) . ?
Lu7 C42 1.85(2) . ?
Lu7 C62 1.895(16) . ?
Lu7 C43 2.10(3) . ?
Lu7 C41 2.100(15) . ?
Lu7 C61 2.152(19) . ?
Lu7 C63 2.159(12) . ?
Lu7 C44 2.283(17) . ?
Lu8 Lu8 1.085(11) 6_565 ?
Lu8 Lu9 1.38(2) . ?
Lu8 Lu4 1.553(8) 6_565 ?
Lu8 Lu1 1.807(7) 6_565 ?
Lu8 Lu9 1.853(17) 6_565 ?
Lu8 Lu2 1.906(6) 6_565 ?
Lu8 C44 2.081(6) . ?
Lu8 C43 2.125(6) . ?
Lu8 C45 2.164(6) . ?
Lu8 C23 2.177(6) . ?
Lu9 Lu4 1.134(17) 6_565 ?
Lu9 Lu9 1.42(3) 6_565 ?
Lu9 Lu8 1.852(17) 6_565 ?
Lu9 C63 1.93(2) . ?
Lu9 C64 1.970(16) . ?
Lu9 C62 2.057(18) . ?
Lu9 Lu1 2.174(17) 6_565 ?
Lu9 C75 2.178(18) . ?
Lu9 C61 2.220(18) . ?
Lu9 C44 2.25(3) . ?
Lu10 Lu2 1.187(14) 6_565 ?
Lu10 Lu1 1.507(17) 6_565 ?
Lu10 Lu11 1.59(2) . ?
Lu10 C51 2.002(11) . ?
Lu10 Lu3 2.012(17) 6_565 ?
Lu10 C50 2.046(10) . ?
Lu10 C30 2.103(16) . ?
Lu10 C49 2.192(9) . ?
Lu10 C29 2.286(15) . ?
Lu11 Lu3 1.33(2) 6_565 ?
Lu11 Lu10 1.59(2) 6_565 ?
Lu11 C32 1.86(3) . ?
Lu11 C31 1.97(3) . ?
Lu11 C33 2.07(2) . ?
Lu11 C53 2.08(2) . ?
Lu11 Lu5 2.114(18) 6_565 ?
Lu11 C13 2.23(2) . ?
C1 C18 1.2695 . ?
C1 C5 1.3047 . ?
C1 C2 1.3172 . ?
C2 C3 1.2981 . ?
C2 C15 1.4311 . ?
C3 C12 1.1108 . ?
C3 C4 1.3374 . ?
C4 C9 1.2821 . ?
C4 C5 1.2881 . ?
C5 C6 1.2305 . ?
C6 C20 1.2941 . ?
C6 C7 1.3122 . ?
C7 C8 1.2709 . ?
C7 C22 1.3140 . ?
C7 C25 1.9652 . ?
C8 C25 1.2103 . ?
C8 C9 1.2561 . ?
C9 C10 1.2463 . ?
C10 C27 1.3030 . ?
C10 C11 1.3194 . ?
C11 C29 1.3136 . ?
C11 C12 1.3198 . ?
C12 C13 1.3176 . ?
C13 C14 1.3334 . ?
C13 C31 1.3410 . ?
C14 C15 1.2435 . ?
C14 C33 1.3109 . ?
C15 C16 1.1481 . ?
C16 C35 1.3328 . ?
C16 C17 1.3485 . ?
C17 C18 1.2269 . ?
C17 C38 1.2484 . ?
C17 C19 2.0127 . ?
C18 C19 1.2471 . ?
C18 C38 1.9647 . ?
C18 C39 2.0150 . ?
C19 C39 1.2312 . ?
C19 C20 1.2319 . ?
C19 C38 1.9560 . ?
C20 C21 1.3085 . ?
C21 C22 1.3055 . ?
C21 C41 1.4456 . ?
C22 C23 1.1984 . ?
C23 C43 1.3627 . ?
C23 C24 1.5018 . ?
C24 C46 1.2060 . ?
C24 C25 1.2366 . ?
C24 C26 2.0070 . ?
C25 C26 1.3864 . ?
C26 C47 1.0767 . ?
C26 C27 1.2214 . ?
C26 C46 1.9874 . ?
C27 C28 1.3132 . ?
C27 C47 1.9716 . ?
C28 C29 1.3087 . ?
C28 C49 1.3484 . ?
C29 C30 1.3272 . ?
C30 C51 1.3380 . ?
C30 C31 1.3502 . ?
C31 C32 1.3282 . ?
C32 C33 1.3183 . ?
C32 C53 1.3214 . ?
C33 C34 1.2868 . ?
C34 C35 1.2933 . ?
C34 C55 1.3871 . ?
C35 C36 1.3070 . ?
C36 C37 1.3062 . ?
C36 C56 1.4834 . ?
C37 C59 1.3365 . ?
C37 C38 1.3576 . ?
C38 C39 1.2226 . ?
C39 C40 1.3722 . ?
C40 C60 1.3434 . ?
C40 C41 1.4158 . ?
C41 C42 1.2487 . ?
C42 C43 1.3159 . ?
C42 C62 1.4183 . ?
C43 C44 1.3964 . ?
C44 C45 1.3079 . ?
C44 C63 1.4099 . ?
C44 C66 1.9786 . ?
C45 C66 1.1303 . ?
C45 C46 1.3354 . ?
C46 C47 1.4032 . ?
C47 C48 1.3290 . ?
C48 C67 1.3357 . ?
C48 C49 1.3605 . ?
C49 C50 1.3462 . ?
C50 C68 1.3587 . ?
C50 C51 1.4815 . ?
C51 C52 1.3132 . ?
C52 C53 1.3363 . ?
C52 C70 1.3460 . ?
C53 C54 1.3238 . ?
C54 C55 1.3144 . ?
C54 C71 1.3297 . ?
C55 C56 1.3049 . ?
C56 C57 1.3534 . ?
C57 C58 1.2966 . ?
C57 C72 1.3212 . ?
C58 C76 1.3346 . ?
C58 C59 1.3421 . ?
C59 C60 1.3273 . ?
C60 C61 1.3291 . ?
C61 C62 1.2857 . ?
C61 C76 1.3217 . ?
C62 C63 1.2797 . ?
C63 C64 1.3864 . ?
C64 C75 1.2267 . ?
C64 C65 1.2674 . ?
C65 C66 1.3021 . ?
C65 C74 1.6528 . ?
C66 C67 1.4626 . ?
C67 C68 1.3511 . ?
C68 C69 1.6576 . ?
C69 C74 1.0481 . ?
C69 C70 1.2164 . ?
C70 C71 1.3386 . ?
C71 C72 1.3695 . ?
C72 C73 1.2897 . ?
C73 C75 1.2328 . ?
C73 C74 1.3328 . ?
C75 C76 1.3991 . ?
Ni1A N4A 1.8059 . ?
Ni1A N2A 1.8095 . ?
Ni1A N1A 1.815(4) 6_565 ?
Ni1A N1A 1.8147 . ?
N1A C2A 1.2797 . ?
N1A C1A 1.2817 . ?
N2A C14A 1.282(5) 6_565 ?
N2A C14A 1.282(5) . ?
N4A C4A 1.284(5) 6_565 ?
N4A C4A 1.284(5) . ?
C1A C13A 1.271(5) . ?
C1A C10A 1.337(5) . ?
C1A C2A 2.0209 . ?
C2A C3A 1.2761 . ?
C2A C7A 1.339(5) . ?
C3A C4A 1.262(5) . ?
C3A H3A 0.9300 . ?
C4A C5A 1.332(7) . ?
C4A C4A 2.020(9) 6_565 ?
C5A C5A 1.252(10) 6_565 ?
C5A C6A 1.399(6) . ?
C6A C18A 1.421(7) . ?
C6A H6A1 0.9700 . ?
C6A H6A2 0.9700 . ?
C7A C10A 1.243(8) . ?
C7A C8A 1.401(7) . ?
C8A C9A 1.431(8) . ?
C8A H8A1 0.9700 . ?
C8A H8A2 0.9700 . ?
C9A H9A1 0.9600 . ?
C9A H9A2 0.9600 . ?
C9A H9A3 0.9600 . ?
C10A C11A 1.405(7) . ?
C11A C12A 1.396(10) . ?
C11A H11A 0.9700 . ?
C11A H11B 0.9700 . ?
C12A H12A 0.9600 . ?
C12A H12B 0.9600 . ?
C12A H12C 0.9600 . ?
C13A C14A 1.264(7) . ?
C13A H13A 0.9300 . ?
C14A C15A 1.339(7) . ?
C14A C14A 2.019(10) 6_565 ?
C15A C15A 1.254(10) 6_565 ?
C15A C16A 1.394(7) . ?
C16A C17A 1.408(8) . ?
C16A H16A 0.9700 . ?
C16A H16B 0.9700 . ?
C17A H17A 0.9600 . ?
C17A H17B 0.9600 . ?
C17A H17C 0.9600 . ?
C18A H18A 0.9424 . ?
C18A H18B 0.9547 . ?
C18A H18C 0.9830 . ?
C1B C6B 1.238(13) . ?
C1B C2B 1.300(16) . ?
C1B H1B 0.9300 . ?
C2B C3B 1.262(17) . ?
C2B H2B 0.9300 . ?
C3B C4B 1.300(16) . ?
C3B H3B 0.9300 . ?
C4B C5B 1.230(15) . ?
C4B H4B 0.9300 . ?
C5B C6B 1.333(14) . ?
C5B H5B 0.9300 . ?
C6B H6B 0.9300 . ?
C7B C8B 1.410(8) . ?
C7B C9B 1.418(9) . ?
C7B H7B 0.9300 . ?
C8B C9B 1.198(15) 2_656 ?
C8B H8B 0.9300 . ?
C9B C8B 1.198(15) 2_656 ?
C9B H9B 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu5 Lu1 Lu2 74.0(4) 6_565 . ?
Lu5 Lu1 Lu10 23.7(5) 6_565 6_565 ?
Lu2 Lu1 Lu10 52.0(4) . 6_565 ?
Lu5 Lu1 Lu8 132.6(4) 6_565 6_565 ?
Lu2 Lu1 Lu8 81.8(2) . 6_565 ?
Lu10 Lu1 Lu8 113.6(4) 6_565 6_565 ?
Lu5 Lu1 C18 93.5(4) 6_565 . ?
Lu2 Lu1 C18 122.31(15) . . ?
Lu10 Lu1 C18 112.0(4) 6_565 . ?
Lu8 Lu1 C18 133.7(2) 6_565 . ?
Lu5 Lu1 C19 128.1(4) 6_565 . ?
Lu2 Lu1 C19 131.47(18) . . ?
Lu10 Lu1 C19 147.2(4) 6_565 . ?
Lu8 Lu1 C19 98.4(2) 6_565 . ?
C18 Lu1 C19 35.4 . . ?
Lu5 Lu1 C1 77.4(3) 6_565 . ?
Lu2 Lu1 C1 87.13(14) . . ?
Lu10 Lu1 C1 86.5(4) 6_565 . ?
Lu8 Lu1 C1 141.8(2) 6_565 . ?
C18 Lu1 C1 35.6 . . ?
C19 Lu1 C1 62.99(8) . . ?
Lu5 Lu1 Lu9 122.4(7) 6_565 6_565 ?
Lu2 Lu1 Lu9 115.6(4) . 6_565 ?
Lu10 Lu1 Lu9 119.6(7) 6_565 6_565 ?
Lu8 Lu1 Lu9 39.1(6) 6_565 6_565 ?
C18 Lu1 Lu9 118.2(4) . 6_565 ?
C19 Lu1 Lu9 89.4(5) . 6_565 ?
C1 Lu1 Lu9 152.3(5) . 6_565 ?
Lu5 Lu1 Lu3 29.7(4) 6_565 6_565 ?
Lu2 Lu1 Lu3 46.20(18) . 6_565 ?
Lu10 Lu1 Lu3 6.0(3) 6_565 6_565 ?
Lu8 Lu1 Lu3 109.1(2) 6_565 6_565 ?
C18 Lu1 Lu3 115.7(2) . 6_565 ?
C19 Lu1 Lu3 150.28(19) . 6_565 ?
C1 Lu1 Lu3 87.98(18) . 6_565 ?
Lu9 Lu1 Lu3 119.0(6) 6_565 6_565 ?
Lu5 Lu1 C20 146.8(3) 6_565 . ?
Lu2 Lu1 C20 102.69(19) . . ?
Lu10 Lu1 C20 146.8(3) 6_565 . ?
Lu8 Lu1 C20 77.6(2) 6_565 . ?
C18 Lu1 C20 59.74(8) . . ?
C19 Lu1 C20 33.1 . . ?
C1 Lu1 C20 69.40(8) . . ?
Lu9 Lu1 C20 89.3(7) 6_565 . ?
Lu3 Lu1 C20 143.64(13) 6_565 . ?
Lu5 Lu1 C17 76.1(5) 6_565 . ?
Lu2 Lu1 C17 138.7(2) . . ?
Lu10 Lu1 C17 99.6(4) 6_565 . ?
Lu8 Lu1 C17 139.4(2) 6_565 . ?
C18 Lu1 C17 33.1 . . ?
C19 Lu1 C17 55.45(7) . . ?
C1 Lu1 C17 58.77(7) . . ?
Lu9 Lu1 C17 104.3(4) 6_565 . ?
Lu3 Lu1 C17 105.3(2) 6_565 . ?
C20 Lu1 C17 87.37(10) . . ?
Lu5 Lu1 C5 93.6(3) 6_565 . ?
Lu2 Lu1 C5 62.16(12) . . ?
Lu10 Lu1 C5 89.1(3) 6_565 . ?
Lu8 Lu1 C5 110.2(2) 6_565 . ?
C18 Lu1 C5 62.85(7) . . ?
C19 Lu1 C5 72.81(8) . . ?
C1 Lu1 C5 34.7 . . ?
Lu9 Lu1 C5 142.8(7) 6_565 . ?
Lu3 Lu1 C5 87.05(14) 6_565 . ?
C20 Lu1 C5 58.03(6) . . ?
C17 Lu1 C5 92.26(10) . . ?
Lu1 Lu2 Lu5 52.2(3) . 6_565 ?
Lu1 Lu2 Lu10 90.5(7) . 6_565 ?
Lu5 Lu2 Lu10 39.4(5) 6_565 6_565 ?
Lu1 Lu2 Lu3 111.0(2) . 6_565 ?
Lu5 Lu2 Lu3 59.9(3) 6_565 6_565 ?
Lu10 Lu2 Lu3 20.6(6) 6_565 6_565 ?
Lu1 Lu2 Lu8 69.8(2) . 6_565 ?
Lu5 Lu2 Lu8 110.3(3) 6_565 6_565 ?
Lu10 Lu2 Lu8 126.3(5) 6_565 6_565 ?
Lu3 Lu2 Lu8 130.3(2) 6_565 6_565 ?
Lu1 Lu2 C5 93.66(14) . . ?
Lu5 Lu2 C5 102.5(2) 6_565 . ?
Lu10 Lu2 C5 112.9(4) 6_565 . ?
Lu3 Lu2 C5 111.95(17) 6_565 . ?
Lu8 Lu2 C5 117.63(19) 6_565 . ?
Lu1 Lu2 C4 127.63(15) . . ?
Lu5 Lu2 C4 109.7(2) 6_565 . ?
Lu10 Lu2 C4 94.8(5) 6_565 . ?
Lu3 Lu2 C4 83.89(14) 6_565 . ?
Lu8 Lu2 C4 137.13(18) 6_565 . ?
C5 Lu2 C4 37.2 . . ?
Lu1 Lu2 Lu6 118.3(2) . . ?
Lu5 Lu2 Lu6 72.1(4) 6_565 . ?
Lu10 Lu2 Lu6 34.1(6) 6_565 . ?
Lu3 Lu2 Lu6 18.3(2) 6_565 . ?
Lu8 Lu2 Lu6 114.9(2) 6_565 . ?
C5 Lu2 Lu6 125.24(18) . . ?
C4 Lu2 Lu6 91.71(18) . . ?
Lu1 Lu2 C6 85.50(17) . . ?
Lu5 Lu2 C6 120.9(3) 6_565 . ?
Lu10 Lu2 C6 145.3(4) 6_565 . ?
Lu3 Lu2 C6 144.52(15) 6_565 . ?
Lu8 Lu2 C6 84.42(18) 6_565 . ?
C5 Lu2 C6 33.4 . . ?
C4 Lu2 C6 61.91(6) . . ?
Lu6 Lu2 C6 152.82(18) . . ?
Lu1 Lu2 C1 69.08(13) . . ?
Lu5 Lu2 C1 67.9(2) 6_565 . ?
Lu10 Lu2 C1 88.1(5) 6_565 . ?
Lu3 Lu2 C1 97.3(2) 6_565 . ?
Lu8 Lu2 C1 125.47(19) 6_565 . ?
C5 Lu2 C1 34.9 . . ?
C4 Lu2 C1 59.13(6) . . ?
Lu6 Lu2 C1 115.43(15) . . ?
C6 Lu2 C1 58.28(7) . . ?
Lu1 Lu2 C9 151.72(17) . . ?
Lu5 Lu2 C9 138.6(3) 6_565 . ?
Lu10 Lu2 C9 108.8(7) 6_565 . ?
Lu3 Lu2 C9 90.30(17) 6_565 . ?
Lu8 Lu2 C9 110.98(18) 6_565 . ?
C5 Lu2 C9 60.2 . . ?
C4 Lu2 C9 33.4 . . ?
Lu6 Lu2 C9 87.75(17) . . ?
C6 Lu2 C9 66.8 . . ?
C1 Lu2 C9 90.55(8) . . ?
Lu1 Lu2 C3 115.92(18) . . ?
Lu5 Lu2 C3 77.8(3) 6_565 . ?
Lu10 Lu2 C3 60.9(5) 6_565 . ?
Lu3 Lu2 C3 54.58(16) 6_565 . ?
Lu8 Lu2 C3 171.79(18) 6_565 . ?
C5 Lu2 C3 57.53(6) . . ?
C4 Lu2 C3 34.8 . . ?
Lu6 Lu2 C3 68.39(17) . . ?
C6 Lu2 C3 90.07(8) . . ?
C1 Lu2 C3 55.25(5) . . ?
C9 Lu2 C3 61.09(5) . . ?
Lu10 Lu3 Lu6 131.2(12) . . ?
Lu10 Lu3 Lu11 96.3(12) . . ?
Lu6 Lu3 Lu11 53.2(9) . . ?
Lu10 Lu3 Lu5 5.1(8) . . ?
Lu6 Lu3 Lu5 134.9(7) . . ?
Lu11 Lu3 Lu5 96.5(10) . . ?
Lu10 Lu3 Lu3 123.3(9) . 6_565 ?
Lu6 Lu3 Lu3 9.7(7) . 6_565 ?
Lu11 Lu3 Lu3 55.3(7) . 6_565 ?
Lu5 Lu3 Lu3 127.4(2) . 6_565 ?
Lu10 Lu3 C30 125.7(10) . . ?
Lu6 Lu3 C30 100.2(8) . . ?
Lu11 Lu3 C30 103.7(12) . . ?
Lu5 Lu3 C30 120.9(4) . . ?
Lu3 Lu3 C30 109.4(3) 6_565 . ?
Lu10 Lu3 Lu2 35.0(7) . 6_565 ?
Lu6 Lu3 Lu2 117.6(7) . 6_565 ?
Lu11 Lu3 Lu2 114.6(12) . 6_565 ?
Lu5 Lu3 Lu2 39.2(2) . 6_565 ?
Lu3 Lu3 Lu2 107.9(2) 6_565 6_565 ?
C30 Lu3 Lu2 137.1(4) . 6_565 ?
Lu10 Lu3 C29 126.5(9) . . ?
Lu6 Lu3 C29 95.9(7) . . ?
Lu11 Lu3 C29 136.1(12) . . ?
Lu5 Lu3 C29 125.3(4) . . ?
Lu3 Lu3 C29 99.9(3) 6_565 . ?
C30 Lu3 C29 45.96(10) . . ?
Lu2 Lu3 C29 107.2(3) 6_565 . ?
Lu10 Lu3 C51 84.3(10) . . ?
Lu6 Lu3 C51 132.4(7) . . ?
Lu11 Lu3 C51 99.7(9) . . ?
Lu5 Lu3 C51 79.2(3) . . ?
Lu3 Lu3 C51 141.8(2) 6_565 . ?
C30 Lu3 C51 43.13(12) . . ?
Lu2 Lu3 C51 109.1(4) 6_565 . ?
C29 Lu3 C51 78.06(16) . . ?
Lu10 Lu3 Lu10 105.7(11) . 6_565 ?
Lu6 Lu3 Lu10 26.2(7) . 6_565 ?
Lu11 Lu3 Lu10 52.0(8) . 6_565 ?
Lu5 Lu3 Lu10 109.9(4) . 6_565 ?
Lu3 Lu3 Lu10 17.6(3) 6_565 6_565 ?
C30 Lu3 Lu10 126.4(4) . 6_565 ?
Lu2 Lu3 Lu10 93.3(4) 6_565 6_565 ?
C29 Lu3 Lu10 114.4(3) . 6_565 ?
C51 Lu3 Lu10 150.3(4) . 6_565 ?
Lu10 Lu3 C31 147.1(9) . . ?
Lu6 Lu3 C31 62.6(7) . . ?
Lu11 Lu3 C31 67.8(12) . . ?
Lu5 Lu3 C31 142.8(4) . . ?
Lu3 Lu3 C31 72.3(2) 6_565 . ?
C30 Lu3 C31 41.39(13) . . ?
Lu2 Lu3 C31 177.3(3) 6_565 . ?
C29 Lu3 C31 70.17(18) . . ?
C51 Lu3 C31 71.15(13) . . ?
Lu10 Lu3 C31 87.4(3) 6_565 . ?
Lu10 Lu3 C28 90.9(9) . . ?
Lu6 Lu3 C28 122.2(7) . . ?
Lu11 Lu3 C28 172.7(12) . . ?
Lu5 Lu3 C28 90.6(3) . . ?
Lu3 Lu3 C28 121.29(19) 6_565 . ?
C30 Lu3 C28 70.69(16) . . ?
Lu2 Lu3 C28 72.3(2) 6_565 . ?
C29 Lu3 C28 36.60(9) . . ?
C51 Lu3 C28 79.52(19) . . ?
Lu10 Lu3 C28 127.1(3) 6_565 . ?
C31 Lu3 C28 105.23(17) . . ?
Lu4 Lu4 Lu9 16.0(12) 6_565 6_565 ?
Lu4 Lu4 Lu8 97.4(5) 6_565 . ?
Lu9 Lu4 Lu8 101.3(11) 6_565 . ?
Lu4 Lu4 Lu8 53.5(3) 6_565 6_565 ?
Lu9 Lu4 Lu8 59.2(11) 6_565 6_565 ?
Lu8 Lu4 Lu8 43.8(5) . 6_565 ?
Lu4 Lu4 C62 89.5(3) 6_565 . ?
Lu9 Lu4 C62 98.4(10) 6_565 . ?
Lu8 Lu4 C62 129.9(4) . . ?
Lu8 Lu4 C62 121.0(5) 6_565 . ?
Lu4 Lu4 C63 128.4(2) 6_565 . ?
Lu9 Lu4 C63 138.3(11) 6_565 . ?
Lu8 Lu4 C63 108.5(4) . . ?
Lu8 Lu4 C63 133.7(3) 6_565 . ?
C62 Lu4 C63 39.88(10) . . ?
Lu4 Lu4 C61 72.7(2) 6_565 . ?
Lu9 Lu4 C61 73.4(10) 6_565 . ?
Lu8 Lu4 C61 162.0(6) . . ?
Lu8 Lu4 C61 124.3(5) 6_565 . ?
C62 Lu4 C61 37.71(9) . . ?
C63 Lu4 C61 69.22(15) . . ?
Lu4 Lu4 C42 67.9(2) 6_565 . ?
Lu9 Lu4 C42 83.1(11) 6_565 . ?
Lu8 Lu4 C42 96.0(4) . . ?
Lu8 Lu4 C42 79.8(4) 6_565 . ?
C62 Lu4 C42 41.77(13) . . ?
C63 Lu4 C42 65.65(16) . . ?
C61 Lu4 C42 66.50(19) . . ?
Lu4 Lu4 C44 128.8(2) 6_565 . ?
Lu9 Lu4 C44 144.7(13) 6_565 . ?
Lu8 Lu4 C44 69.1(3) . . ?
Lu8 Lu4 C44 98.5(3) 6_565 . ?
C62 Lu4 C44 68.30(16) . . ?
C63 Lu4 C44 39.85(11) . . ?
C61 Lu4 C44 105.0(2) . . ?
C42 Lu4 C44 65.03(13) . . ?
Lu4 Lu4 C64 147.77(15) 6_565 . ?
Lu9 Lu4 C64 142.6(12) 6_565 . ?
Lu8 Lu4 C64 114.5(5) . . ?
Lu8 Lu4 C64 158.0(4) 6_565 . ?
C62 Lu4 C64 66.94(19) . . ?
C63 Lu4 C64 38.00(14) . . ?
C61 Lu4 C64 75.31(16) . . ?
C42 Lu4 C64 102.6(2) . . ?
C44 Lu4 C64 64.0(2) . . ?
Lu4 Lu4 C43 92.1(2) 6_565 . ?
Lu9 Lu4 C43 108.0(12) 6_565 . ?
Lu8 Lu4 C43 67.5(3) . . ?
Lu8 Lu4 C43 73.5(3) 6_565 . ?
C62 Lu4 C43 62.68(15) . . ?
C63 Lu4 C43 60.49(13) . . ?
C61 Lu4 C43 97.3(2) . . ?
C42 Lu4 C43 34.97(8) . . ?
C44 Lu4 C43 36.72(7) . . ?
C64 Lu4 C43 95.7(2) . . ?
Lu4 Lu4 C76 92.5(2) 6_565 . ?
Lu9 Lu4 C76 85.2(12) 6_565 . ?
Lu8 Lu4 C76 164.6(6) . . ?
Lu8 Lu4 C76 144.4(4) 6_565 . ?
C62 Lu4 C76 61.65(11) . . ?
C63 Lu4 C76 73.69(15) . . ?
C61 Lu4 C76 33.42(5) . . ?
C42 Lu4 C76 98.68(19) . . ?
C44 Lu4 C76 113.2(2) . . ?
C64 Lu4 C76 57.44(13) . . ?
C43 Lu4 C76 124.1(2) . . ?
Lu10 Lu5 Lu1 128.5(11) . 6_565 ?
Lu10 Lu5 Lu2 76.9(10) . 6_565 ?
Lu1 Lu5 Lu2 53.8(3) 6_565 6_565 ?
Lu10 Lu5 Lu3 4.8(8) . . ?
Lu1 Lu5 Lu3 133.1(6) 6_565 . ?
Lu2 Lu5 Lu3 80.9(5) 6_565 . ?
Lu10 Lu5 C50 96.5(8) . . ?
Lu1 Lu5 C50 114.7(4) 6_565 . ?
Lu2 Lu5 C50 113.4(3) 6_565 . ?
Lu3 Lu5 C50 92.5(3) . . ?
Lu10 Lu5 C68 138.8(8) . . ?
Lu1 Lu5 C68 82.1(4) 6_565 . ?
Lu2 Lu5 C68 115.4(3) 6_565 . ?
Lu3 Lu5 C68 134.7(3) . . ?
C50 Lu5 C68 42.31(11) . . ?
Lu10 Lu5 Lu6 12.2(7) . . ?
Lu1 Lu5 Lu6 125.4(5) 6_565 . ?
Lu2 Lu5 Lu6 78.4(4) 6_565 . ?
Lu3 Lu5 Lu6 15.0(2) . . ?
C50 Lu5 Lu6 107.2(4) . . ?
C68 Lu5 Lu6 148.9(3) . . ?
Lu10 Lu5 Lu11 39.0(10) . . ?
Lu1 Lu5 Lu11 131.7(7) 6_565 . ?
Lu2 Lu5 Lu11 101.6(8) 6_565 . ?
Lu3 Lu5 Lu11 38.9(7) . . ?
C50 Lu5 Lu11 113.3(7) . . ?
C68 Lu5 Lu11 141.4(7) . . ?
Lu6 Lu5 Lu11 29.3(7) . . ?
Lu10 Lu5 C49 83.4(8) . . ?
Lu1 Lu5 C49 96.0(3) 6_565 . ?
Lu2 Lu5 C49 75.0(2) 6_565 . ?
Lu3 Lu5 C49 81.8(3) . . ?
C50 Lu5 C49 38.72(8) . . ?
C68 Lu5 C49 64.42(13) . . ?
Lu6 Lu5 C49 95.5(3) . . ?
Lu11 Lu5 C49 118.8(8) . . ?
Lu10 Lu5 C51 64.1(8) . . ?
Lu1 Lu5 C51 156.2(3) 6_565 . ?
Lu2 Lu5 C51 124.5(5) 6_565 . ?
Lu3 Lu5 C51 59.3(3) . . ?
C50 Lu5 C51 41.68(10) . . ?
C68 Lu5 C51 78.25(15) . . ?
Lu6 Lu5 C51 71.3(3) . . ?
Lu11 Lu5 C51 71.6(7) . . ?
C49 Lu5 C51 63.27(13) . . ?
Lu10 Lu5 C67 140.3(8) . . ?
Lu1 Lu5 C67 51.0(3) 6_565 . ?
Lu2 Lu5 C67 80.1(3) 6_565 . ?
Lu3 Lu5 C67 140.1(3) . . ?
C50 Lu5 C67 63.99(16) . . ?
C68 Lu5 C67 36.43(11) . . ?
Lu6 Lu5 C67 150.5(3) . . ?
Lu11 Lu5 C67 177.2(7) . . ?
C49 Lu5 C67 59.41(12) . . ?
C51 Lu5 C67 105.67(17) . . ?
Lu10 Lu5 C69 138.4(8) . . ?
Lu1 Lu5 C69 91.4(5) 6_565 . ?
Lu2 Lu5 C69 144.7(5) 6_565 . ?
Lu3 Lu5 C69 134.4(3) . . ?
C50 Lu5 C69 72.3(2) . . ?
C68 Lu5 C69 44.28(14) . . ?
Lu6 Lu5 C69 135.1(3) . . ?
Lu11 Lu5 C69 107.8(7) . . ?
C49 Lu5 C69 106.2(2) . . ?
C51 Lu5 C69 83.96(17) . . ?
C67 Lu5 C69 71.4(2) . . ?
Lu3 Lu6 Lu3 160.6(13) . 6_565 ?
Lu3 Lu6 Lu11 91.6(7) . . ?
Lu3 Lu6 Lu11 91.6(7) 6_565 . ?
Lu3 Lu6 Lu10 139.3(10) . 6_565 ?
Lu3 Lu6 Lu10 23.6(6) 6_565 6_565 ?
Lu11 Lu6 Lu10 80.5(9) . 6_565 ?
Lu3 Lu6 Lu10 23.6(6) . . ?
Lu3 Lu6 Lu10 139.3(10) 6_565 . ?
Lu11 Lu6 Lu10 80.5(9) . . ?
Lu10 Lu6 Lu10 116.3(10) 6_565 . ?
Lu3 Lu6 C31 95.3(7) . . ?
Lu3 Lu6 C31 104.1(7) 6_565 . ?
Lu11 Lu6 C31 81.7(15) . . ?
Lu10 Lu6 C31 122.4(6) 6_565 . ?
Lu10 Lu6 C31 113.9(5) . . ?
Lu3 Lu6 C13 135.5(8) . . ?
Lu3 Lu6 C13 63.3(6) 6_565 . ?
Lu11 Lu6 C13 94.4(13) . . ?
Lu10 Lu6 C13 85.1(5) 6_565 . ?
Lu10 Lu6 C13 156.4(6) . . ?
C31 Lu6 C13 42.56(16) . . ?
Lu3 Lu6 C30 56.1(5) . . ?
Lu3 Lu6 C30 141.9(8) 6_565 . ?
Lu11 Lu6 C30 98.8(11) . . ?
Lu10 Lu6 C30 164.4(6) 6_565 . ?
Lu10 Lu6 C30 78.7(5) . . ?
C31 Lu6 C30 42.65(15) . . ?
C13 Lu6 C30 79.4(3) . . ?
Lu3 Lu6 C12 132.7(8) . . ?
Lu3 Lu6 C12 55.0(5) 6_565 . ?
Lu11 Lu6 C12 130.3(9) . . ?
Lu10 Lu6 C12 77.3(5) 6_565 . ?
Lu10 Lu6 C12 149.1(5) . . ?
C31 Lu6 C12 74.0(3) . . ?
C13 Lu6 C12 40.16(12) . . ?
C30 Lu6 C12 91.7(3) . . ?
Lu3 Lu6 C29 61.7(6) . . ?
Lu3 Lu6 C29 124.8(7) 6_565 . ?
Lu11 Lu6 C29 137.8(10) . . ?
Lu10 Lu6 C29 141.1(5) 6_565 . ?
Lu10 Lu6 C29 83.0(5) . . ?
C31 Lu6 C29 70.1(2) . . ?
C13 Lu6 C29 85.7(3) . . ?
C30 Lu6 C29 39.66(12) . . ?
C12 Lu6 C29 71.5(2) . . ?
Lu3 Lu6 C11 95.1(7) . . ?
Lu3 Lu6 C11 87.3(6) 6_565 . ?
Lu11 Lu6 C11 163.0(16) . . ?
Lu10 Lu6 C11 104.0(5) 6_565 . ?
Lu10 Lu6 C11 111.0(5) . . ?
C31 Lu6 C11 82.1(3) . . ?
C13 Lu6 C11 70.0(2) . . ?
C30 Lu6 C11 72.4(2) . . ?
C12 Lu6 C11 38.51(12) . . ?
C29 Lu6 C11 37.88(12) . . ?
Lu3 Lu6 Lu5 133.8(8) . 6_565 ?
Lu3 Lu6 Lu5 30.1(5) 6_565 6_565 ?
Lu11 Lu6 Lu5 75.5(9) . 6_565 ?
Lu10 Lu6 Lu5 6.9(4) 6_565 6_565 ?
Lu10 Lu6 Lu5 110.5(6) . 6_565 ?
C31 Lu6 Lu5 125.2(3) . 6_565 ?
C13 Lu6 Lu5 90.16(16) . 6_565 ?
C30 Lu6 Lu5 167.8(4) . 6_565 ?
C12 Lu6 Lu5 84.14(15) . 6_565 ?
C29 Lu6 Lu5 146.6(3) . 6_565 ?
C11 Lu6 Lu5 110.1(2) . 6_565 ?
Lu4 Lu7 Lu9 111(5) 6_565 . ?
Lu4 Lu7 Lu9 12(2) 6_565 6_565 ?
Lu9 Lu7 Lu9 106(5) . 6_565 ?
Lu4 Lu7 Lu8 87(2) 6_565 6_565 ?
Lu9 Lu7 Lu8 125(2) . 6_565 ?
Lu9 Lu7 Lu8 81.2(16) 6_565 6_565 ?
Lu4 Lu7 Lu8 135(3) 6_565 . ?
Lu9 Lu7 Lu8 81.2(16) . . ?
Lu9 Lu7 Lu8 125(2) 6_565 . ?
Lu8 Lu7 Lu8 53.9(10) 6_565 . ?
Lu4 Lu7 C42 94(3) 6_565 . ?
Lu9 Lu7 C42 127.9(19) . . ?
Lu9 Lu7 C42 105.4(18) 6_565 . ?
Lu8 Lu7 C42 100.0(15) 6_565 . ?
Lu8 Lu7 C42 111.8(19) . . ?
Lu4 Lu7 C62 94(2) 6_565 . ?
Lu9 Lu7 C62 87.5(16) . . ?
Lu9 Lu7 C62 105.3(18) 6_565 . ?
Lu8 Lu7 C62 144.5(18) 6_565 . ?
Lu8 Lu7 C62 129.7(13) . . ?
C42 Lu7 C62 44.5(4) . . ?
Lu4 Lu7 C43 129(3) 6_565 . ?
Lu9 Lu7 C43 113(2) . . ?
Lu9 Lu7 C43 138(2) 6_565 . ?
Lu8 Lu7 C43 86.5(15) 6_565 . ?
Lu8 Lu7 C43 74.8(13) . . ?
C42 Lu7 C43 38.3(5) . . ?
C62 Lu7 C43 65.3(7) . . ?
Lu4 Lu7 C41 65(3) 6_565 . ?
Lu9 Lu7 C41 157(2) . . ?
Lu9 Lu7 C41 73.8(18) 6_565 . ?
Lu8 Lu7 C41 78.2(9) 6_565 . ?
Lu8 Lu7 C41 118.4(17) . . ?
C42 Lu7 C41 36.2(3) . . ?
C62 Lu7 C41 70.6(6) . . ?
C43 Lu7 C41 64.9(7) . . ?
Lu4 Lu7 C61 63(2) 6_565 . ?
Lu9 Lu7 C61 82.6(19) . . ?
Lu9 Lu7 C61 72.3(18) 6_565 . ?
Lu8 Lu7 C61 146.7(4) 6_565 . ?
Lu8 Lu7 C61 159.3(5) . . ?
C42 Lu7 C61 69.1(5) . . ?
C62 Lu7 C61 36.3(3) . . ?
C43 Lu7 C61 100.1(7) . . ?
C41 Lu7 C61 75.3(4) . . ?
Lu4 Lu7 C63 127(3) 6_565 . ?
Lu9 Lu7 C63 63.2(16) . . ?
Lu9 Lu7 C63 135(2) 6_565 . ?
Lu8 Lu7 C63 142.0(18) 6_565 . ?
Lu8 Lu7 C63 97.5(7) . . ?
C42 Lu7 C63 65.1(5) . . ?
C62 Lu7 C63 36.1(2) . . ?
C43 Lu7 C63 59.8(5) . . ?
C41 Lu7 C63 99.9(8) . . ?
C61 Lu7 C63 63.5(4) . . ?
Lu4 Lu7 C44 158(3) 6_565 . ?
Lu9 Lu7 C44 76.5(19) . . ?
Lu9 Lu7 C44 169.9(19) 6_565 . ?
Lu8 Lu7 C44 105.4(15) 6_565 . ?
Lu8 Lu7 C44 64.9(8) . . ?
C42 Lu7 C44 66.3(7) . . ?
C62 Lu7 C44 64.8(5) . . ?
C43 Lu7 C44 36.9(4) . . ?
C41 Lu7 C44 99.8(10) . . ?
C61 Lu7 C44 98.7(6) . . ?
C63 Lu7 C44 36.9(2) . . ?
Lu8 Lu8 Lu7 63.1(5) 6_565 . ?
Lu8 Lu8 Lu4 82.6(5) 6_565 . ?
Lu7 Lu8 Lu4 21.1(7) . . ?
Lu8 Lu8 Lu9 97.0(8) 6_565 . ?
Lu7 Lu8 Lu9 39.5(10) . . ?
Lu4 Lu8 Lu9 19.1(8) . . ?
Lu8 Lu8 Lu4 53.5(3) 6_565 6_565 ?
Lu7 Lu8 Lu4 11.8(7) . 6_565 ?
Lu4 Lu8 Lu4 29.1(6) . 6_565 ?
Lu9 Lu8 Lu4 45.0(7) . 6_565 ?
Lu8 Lu8 Lu1 132.00(18) 6_565 6_565 ?
Lu7 Lu8 Lu1 122.4(12) . 6_565 ?
Lu4 Lu8 Lu1 104.0(5) . 6_565 ?
Lu9 Lu8 Lu1 85.0(7) . 6_565 ?
Lu4 Lu8 Lu1 121.6(4) 6_565 6_565 ?
Lu8 Lu8 Lu9 47.5(7) 6_565 6_565 ?
Lu7 Lu8 Lu9 23.1(9) . 6_565 ?
Lu4 Lu8 Lu9 36.9(7) . 6_565 ?
Lu9 Lu8 Lu9 49.4(14) . 6_565 ?
Lu4 Lu8 Lu9 11.5(6) 6_565 6_565 ?
Lu1 Lu8 Lu9 116.6(8) 6_565 6_565 ?
Lu8 Lu8 Lu2 112.86(17) 6_565 6_565 ?
Lu7 Lu8 Lu2 139.9(13) . 6_565 ?
Lu4 Lu8 Lu2 127.3(5) . 6_565 ?
Lu9 Lu8 Lu2 109.7(8) . 6_565 ?
Lu4 Lu8 Lu2 133.0(4) 6_565 6_565 ?
Lu1 Lu8 Lu2 28.46(11) 6_565 6_565 ?
Lu9 Lu8 Lu2 123.2(7) 6_565 6_565 ?
Lu8 Lu8 C44 125.06(18) 6_565 . ?
Lu7 Lu8 C44 83.7(8) . . ?
Lu4 Lu8 C44 76.5(3) . . ?
Lu9 Lu8 C44 78.2(9) . . ?
Lu4 Lu8 C44 95.3(4) 6_565 . ?
Lu1 Lu8 C44 102.4(3) 6_565 . ?
Lu9 Lu8 C44 106.8(6) 6_565 . ?
Lu2 Lu8 C44 120.3(3) 6_565 . ?
Lu8 Lu8 C43 87.87(16) 6_565 . ?
Lu7 Lu8 C43 72.3(12) . . ?
Lu4 Lu8 C43 79.2(4) . . ?
Lu9 Lu8 C43 92.4(9) . . ?
Lu4 Lu8 C43 80.2(3) 6_565 . ?
Lu1 Lu8 C43 140.1(3) 6_565 . ?
Lu9 Lu8 C43 90.1(7) 6_565 . ?
Lu2 Lu8 C43 146.6(3) 6_565 . ?
C44 Lu8 C43 38.77(11) . . ?
Lu8 Lu8 C45 153.23(17) 6_565 . ?
Lu7 Lu8 C45 116.3(7) . . ?
Lu4 Lu8 C45 102.8(4) . . ?
Lu9 Lu8 C45 95.3(9) . . ?
Lu4 Lu8 C45 128.1(4) 6_565 . ?
Lu1 Lu8 C45 72.7(2) 6_565 . ?
Lu9 Lu8 C45 138.7(6) 6_565 . ?
Lu2 Lu8 C45 85.0(2) 6_565 . ?
C44 Lu8 C45 35.82(10) . . ?
C43 Lu8 C45 67.87(18) . . ?
Lu8 Lu8 C23 72.96(15) 6_565 . ?
Lu7 Lu8 C23 95.5(13) . . ?
Lu4 Lu8 C23 110.2(5) . . ?
Lu9 Lu8 C23 126.9(9) . . ?
Lu4 Lu8 C23 97.8(3) 6_565 . ?
Lu1 Lu8 C23 140.4(3) 6_565 . ?
Lu9 Lu8 C23 102.8(8) 6_565 . ?
Lu2 Lu8 C23 122.5(3) 6_565 . ?
C44 Lu8 C23 67.98(19) . . ?
C43 Lu8 C23 36.91(11) . . ?
C45 Lu8 C23 80.6(2) . . ?
Lu7 Lu9 Lu4 21.9(17) . 6_565 ?
Lu7 Lu9 Lu8 59.2(17) . . ?
Lu4 Lu9 Lu8 75.8(11) 6_565 . ?
Lu7 Lu9 Lu9 37(2) . 6_565 ?
Lu4 Lu9 Lu9 16.0(12) 6_565 6_565 ?
Lu8 Lu9 Lu9 83.0(8) . 6_565 ?
Lu7 Lu9 Lu8 32.0(13) . 6_565 ?
Lu4 Lu9 Lu8 41.8(7) 6_565 6_565 ?
Lu8 Lu9 Lu8 35.5(5) . 6_565 ?
Lu9 Lu9 Lu8 47.5(7) 6_565 6_565 ?
Lu7 Lu9 C63 93(2) . . ?
Lu4 Lu9 C63 103.6(13) 6_565 . ?
Lu8 Lu9 C63 102.5(14) . . ?
Lu9 Lu9 C63 116.4(5) 6_565 . ?
Lu8 Lu9 C63 114.9(12) 6_565 . ?
Lu7 Lu9 C64 133(2) . . ?
Lu4 Lu9 C64 137.9(14) 6_565 . ?
Lu8 Lu9 C64 125.7(15) . . ?
Lu9 Lu9 C64 142.7(5) 6_565 . ?
Lu8 Lu9 C64 154.1(15) 6_565 . ?
C63 Lu9 C64 41.6(4) . . ?
Lu7 Lu9 C62 67.0(15) . . ?
Lu4 Lu9 C62 70.1(10) 6_565 . ?
Lu8 Lu9 C62 108.5(13) . . ?
Lu9 Lu9 C62 80.4(5) 6_565 . ?
Lu8 Lu9 C62 97.9(8) 6_565 . ?
C63 Lu9 C62 37.3(3) . . ?
C64 Lu9 C62 68.7(6) . . ?
Lu7 Lu9 Lu1 112.9(19) . 6_565 ?
Lu4 Lu9 Lu1 122.0(13) 6_565 6_565 ?
Lu8 Lu9 Lu1 55.9(7) . 6_565 ?
Lu9 Lu9 Lu1 118.7(4) 6_565 6_565 ?
Lu8 Lu9 Lu1 82.2(7) 6_565 6_565 ?
C63 Lu9 Lu1 115.6(11) . 6_565 ?
C64 Lu9 Lu1 98.3(7) . 6_565 ?
C62 Lu9 Lu1 149.8(13) . 6_565 ?
Lu7 Lu9 C75 139(2) . . ?
Lu4 Lu9 C75 126.5(15) 6_565 . ?
Lu8 Lu9 C75 156.6(13) . . ?
Lu9 Lu9 C75 120.3(6) 6_565 . ?
Lu8 Lu9 C75 167.8(12) 6_565 . ?
C63 Lu9 C75 67.9(5) . . ?
C64 Lu9 C75 33.9(3) . . ?
C62 Lu9 C75 77.2(6) . . ?
Lu1 Lu9 C75 107.7(7) 6_565 . ?
Lu7 Lu9 C61 74.1(17) . . ?
Lu4 Lu9 C61 63.4(9) 6_565 . ?
Lu8 Lu9 C61 131.7(11) . . ?
Lu9 Lu9 C61 64.8(4) 6_565 . ?
Lu8 Lu9 C61 104.1(7) 6_565 . ?
C63 Lu9 C61 65.9(5) . . ?
C64 Lu9 C61 77.9(6) . . ?
C62 Lu9 C61 34.7(3) . . ?
Lu1 Lu9 C61 172.4(11) 6_565 . ?
C75 Lu9 C61 65.5(5) . . ?
Lu7 Lu9 C44 81(2) . . ?
Lu4 Lu9 C44 101.3(14) 6_565 . ?
Lu8 Lu9 C44 65.0(10) . . ?
Lu9 Lu9 C44 117.2(4) 6_565 . ?
Lu8 Lu9 C44 87.3(9) 6_565 . ?
C63 Lu9 C44 38.5(5) . . ?
C64 Lu9 C44 66.9(7) . . ?
C62 Lu9 C44 63.2(6) . . ?
Lu1 Lu9 C44 86.6(8) 6_565 . ?
C75 Lu9 C44 100.1(7) . . ?
C61 Lu9 C44 97.8(7) . . ?
Lu3 Lu10 Lu5 170.1(16) . . ?
Lu3 Lu10 Lu2 124.4(10) . 6_565 ?
Lu5 Lu10 Lu2 63.7(12) . 6_565 ?
Lu3 Lu10 Lu6 25.1(7) . . ?
Lu5 Lu10 Lu6 161.0(11) . . ?
Lu2 Lu10 Lu6 116.7(7) 6_565 . ?
Lu3 Lu10 Lu1 161.5(10) . 6_565 ?
Lu5 Lu10 Lu1 27.8(7) . 6_565 ?
Lu2 Lu10 Lu1 37.5(5) 6_565 6_565 ?
Lu6 Lu10 Lu1 144.0(7) . 6_565 ?
Lu3 Lu10 Lu11 56.6(12) . . ?
Lu5 Lu10 Lu11 123.1(13) . . ?
Lu2 Lu10 Lu11 134.8(11) 6_565 . ?
Lu6 Lu10 Lu11 41.6(10) . . ?
Lu1 Lu10 Lu11 128.9(12) 6_565 . ?
Lu3 Lu10 C51 74.6(11) . . ?
Lu5 Lu10 C51 95.6(8) . . ?
Lu2 Lu10 C51 136.2(7) 6_565 . ?
Lu6 Lu10 C51 95.3(9) . . ?
Lu1 Lu10 C51 120.6(7) 6_565 . ?
Lu11 Lu10 C51 89.0(10) . . ?
Lu3 Lu10 Lu3 39.1(7) . 6_565 ?
Lu5 Lu10 Lu3 148.5(10) . 6_565 ?
Lu2 Lu10 Lu3 106.5(6) 6_565 6_565 ?
Lu6 Lu10 Lu3 14.5(3) . 6_565 ?
Lu1 Lu10 Lu3 129.8(5) 6_565 6_565 ?
Lu11 Lu10 Lu3 41.5(9) . 6_565 ?
C51 Lu10 Lu3 109.1(7) . 6_565 ?
Lu3 Lu10 C50 110.3(12) . . ?
Lu5 Lu10 C50 61.4(7) . . ?
Lu2 Lu10 C50 95.2(7) 6_565 . ?
Lu6 Lu10 C50 134.8(10) . . ?
Lu1 Lu10 C50 80.4(6) 6_565 . ?
Lu11 Lu10 C50 128.5(9) . . ?
C51 Lu10 C50 42.92(19) . . ?
Lu3 Lu10 C50 149.2(8) 6_565 . ?
Lu3 Lu10 C30 38.0(9) . . ?
Lu5 Lu10 C30 132.6(9) . . ?
Lu2 Lu10 C30 136.4(7) 6_565 . ?
Lu6 Lu10 C30 61.8(7) . . ?
Lu1 Lu10 C30 152.2(6) 6_565 . ?
Lu11 Lu10 C30 76.0(12) . . ?
C51 Lu10 C30 37.9(3) . . ?
Lu3 Lu10 C30 76.2(5) 6_565 . ?
C50 Lu10 C30 73.0(4) . . ?
Lu3 Lu10 C49 100.5(10) . . ?
Lu5 Lu10 C49 76.0(8) . . ?
Lu2 Lu10 C49 71.6(5) 6_565 . ?
Lu6 Lu10 C49 122.8(8) . . ?
Lu1 Lu10 C49 78.8(5) 6_565 . ?
Lu11 Lu10 C49 150.9(13) . . ?
C51 Lu10 C49 65.9(3) . . ?
Lu3 Lu10 C49 131.6(6) 6_565 . ?
C50 Lu10 C49 36.84(17) . . ?
C30 Lu10 C49 75.0(4) . . ?
Lu3 Lu10 C29 38.7(8) . . ?
Lu5 Lu10 C29 138.3(9) . . ?
Lu2 Lu10 C29 103.1(6) 6_565 . ?
Lu6 Lu10 C29 60.7(6) . . ?
Lu1 Lu10 C29 134.0(5) 6_565 . ?
Lu11 Lu10 C29 94.8(13) . . ?
C51 Lu10 C29 65.9(4) . . ?
Lu3 Lu10 C29 71.7(4) 6_565 . ?
C50 Lu10 C29 82.3(4) . . ?
C30 Lu10 C29 34.9(2) . . ?
C49 Lu10 C29 62.4(3) . . ?
Lu6 Lu11 Lu3 35.2(7) . . ?
Lu6 Lu11 Lu3 35.2(7) . 6_565 ?
Lu3 Lu11 Lu3 69.3(14) . 6_565 ?
Lu6 Lu11 Lu10 57.9(11) . 6_565 ?
Lu3 Lu11 Lu10 86.5(15) . 6_565 ?
Lu3 Lu11 Lu10 27.1(5) 6_565 6_565 ?
Lu6 Lu11 Lu10 57.9(11) . . ?
Lu3 Lu11 Lu10 27.1(5) . . ?
Lu3 Lu11 Lu10 86.5(15) 6_565 . ?
Lu10 Lu11 Lu10 93.7(15) 6_565 . ?
Lu6 Lu11 C32 106.3(19) . . ?
Lu3 Lu11 C32 107.5(14) . . ?
Lu3 Lu11 C32 110.0(15) 6_565 . ?
Lu10 Lu11 C32 126.0(12) 6_565 . ?
Lu10 Lu11 C32 122.4(11) . . ?
Lu6 Lu11 C31 65.9(14) . . ?
Lu3 Lu11 C31 73.4(12) . . ?
Lu3 Lu11 C31 78.1(12) 6_565 . ?
Lu10 Lu11 C31 103.1(13) 6_565 . ?
Lu10 Lu11 C31 97.1(12) . . ?
C32 Lu11 C31 40.5(6) . . ?
Lu6 Lu11 C33 115.2(16) . . ?
Lu3 Lu11 C33 137.4(18) . . ?
Lu3 Lu11 C33 95.6(9) 6_565 . ?
Lu10 Lu11 C33 97.1(5) 6_565 . ?
Lu10 Lu11 C33 160.3(16) . . ?
C32 Lu11 C33 38.7(5) . . ?
C31 Lu11 C33 64.4(8) . . ?
Lu6 Lu11 C53 127.7(16) . . ?
Lu3 Lu11 C53 106.1(8) . . ?
Lu3 Lu11 C53 147.2(18) 6_565 . ?
Lu10 Lu11 C53 162.2(12) 6_565 . ?
Lu10 Lu11 C53 103.3(5) . . ?
C32 Lu11 C53 38.6(5) . . ?
C31 Lu11 C53 69.7(8) . . ?
C33 Lu11 C53 65.1(8) . . ?
Lu6 Lu11 Lu5 75.2(11) . . ?
Lu3 Lu11 Lu5 44.7(6) . . ?
Lu3 Lu11 Lu5 100.8(15) 6_565 . ?
Lu10 Lu11 Lu5 101.5(14) 6_565 . ?
Lu10 Lu11 Lu5 17.9(5) . . ?
C32 Lu11 Lu5 125.4(6) . . ?
C31 Lu11 Lu5 110.4(8) . . ?
C33 Lu11 Lu5 161.4(11) . . ?
C53 Lu11 Lu5 96.3(3) . . ?
Lu6 Lu11 Lu5 75.2(11) . 6_565 ?
Lu3 Lu11 Lu5 100.8(15) . 6_565 ?
Lu3 Lu11 Lu5 44.7(6) 6_565 6_565 ?
Lu10 Lu11 Lu5 17.9(5) 6_565 6_565 ?
Lu10 Lu11 Lu5 101.5(14) . 6_565 ?
C32 Lu11 Lu5 129.5(7) . 6_565 ?
C31 Lu11 Lu5 117.4(9) . 6_565 ?
C33 Lu11 Lu5 93.6(2) . 6_565 ?
C53 Lu11 Lu5 153.1(11) . 6_565 ?
Lu5 Lu11 Lu5 104.2(12) . 6_565 ?
Lu6 Lu11 C13 57.0(11) . . ?
Lu3 Lu11 C13 84.4(13) . . ?
Lu3 Lu11 C13 48.6(8) 6_565 . ?
Lu10 Lu11 C13 68.9(9) 6_565 . ?
Lu10 Lu11 C13 111.3(14) . . ?
C32 Lu11 C13 61.4(7) . . ?
C31 Lu11 C13 36.6(4) . . ?
C33 Lu11 C13 58.2(6) . . ?
C53 Lu11 C13 99.3(11) . . ?
Lu5 Lu11 C13 129.1(12) . . ?
Lu5 Lu11 C13 81.2(5) 6_565 . ?
C18 C1 C5 119.2 . . ?
C18 C1 C2 123.8 . . ?
C5 C1 C2 105.4 . . ?
C18 C1 Lu1 67.03(7) . . ?
C5 C1 Lu1 77.28(6) . . ?
C2 C1 Lu1 93.65(9) . . ?
C18 C1 Lu2 90.57(6) . . ?
C5 C1 Lu2 60.3 . . ?
C2 C1 Lu2 83.03(6) . . ?
Lu1 C1 Lu2 23.79(5) . . ?
C3 C2 C1 109.3 . . ?
C3 C2 C15 116.7 . . ?
C1 C2 C15 115.2 . . ?
C3 C2 Lu2 67.75(5) . . ?
C1 C2 Lu2 65.22(6) . . ?
C15 C2 Lu2 92.7 . . ?
C3 C2 Lu1 88.55(5) . . ?
C1 C2 Lu1 55.59(7) . . ?
C15 C2 Lu1 82.05(5) . . ?
Lu2 C2 Lu1 20.83(4) . . ?
C12 C3 C2 131.3 . . ?
C12 C3 C4 114.4 . . ?
C2 C3 C4 107.7 . . ?
C12 C3 Lu2 98.05(7) . . ?
C2 C3 Lu2 81.16(6) . . ?
C4 C3 Lu2 61.4 . . ?
C12 C3 Lu6 47.33(16) . . ?
C2 C3 Lu6 104.25(13) . . ?
C4 C3 Lu6 98.57(15) . . ?
Lu2 C3 Lu6 52.93(17) . . ?
C12 C3 Lu1 107.90(6) . . ?
C2 C3 Lu1 64.37(5) . . ?
C4 C3 Lu1 70.47(5) . . ?
Lu2 C3 Lu1 16.83(5) . . ?
Lu6 C3 Lu1 60.62(16) . . ?
C9 C4 C5 115.6 . . ?
C9 C4 C3 128.6 . . ?
C5 C4 C3 105.9 . . ?
C9 C4 Lu2 84.64(6) . . ?
C5 C4 Lu2 68.32(8) . . ?
C3 C4 Lu2 83.80(5) . . ?
C9 C4 Lu1 97.86(6) . . ?
C5 C4 Lu1 54.84(6) . . ?
C3 C4 Lu1 81.85(7) . . ?
Lu2 C4 Lu1 15.53(5) . . ?
C6 C5 C4 122.1 . . ?
C6 C5 C1 119.4 . . ?
C4 C5 C1 111.5 . . ?
C6 C5 Lu2 84.12(6) . . ?
C4 C5 Lu2 74.51(7) . . ?
C1 C5 Lu2 84.86(5) . . ?
C6 C5 Lu1 78.99(9) . . ?
C4 C5 Lu1 97.05(8) . . ?
C1 C5 Lu1 68.02(7) . . ?
Lu2 C5 Lu1 24.18(5) . . ?
C5 C6 C20 117.5 . . ?
C5 C6 C7 121.0 . . ?
C20 C6 C7 109.1 . . ?
C5 C6 Lu2 62.46(6) . . ?
C20 C6 Lu2 90.29(6) . . ?
C7 C6 Lu2 84.25(6) . . ?
C5 C6 Lu1 69.89(8) . . ?
C20 C6 Lu1 68.38(7) . . ?
C7 C6 Lu1 98.12(7) . . ?
Lu2 C6 Lu1 23.05(5) . . ?
C8 C7 C6 117.6 . . ?
C8 C7 C22 129.4 . . ?
C6 C7 C22 105.8 . . ?
C8 C7 C25 36.6 . . ?
C6 C7 C25 146.8 . . ?
C22 C7 C25 93.0 . . ?
C8 C7 Lu2 79.42(6) . . ?
C6 C7 Lu2 63.77(6) . . ?
C22 C7 Lu2 99.04(5) . . ?
C25 C7 Lu2 86.80(6) . . ?
C8 C7 Lu1 97.64(6) . . ?
C6 C7 Lu1 54.63(5) . . ?
C22 C7 Lu1 86.63(6) . . ?
C25 C7 Lu1 100.81(6) . . ?
Lu2 C7 Lu1 18.25(5) . . ?
C25 C8 C9 123.8 . . ?
C25 C8 C7 104.7 . . ?
C9 C8 C7 119.4 . . ?
C25 C8 Lu2 102.98(6) . . ?
C9 C8 Lu2 64.68(5) . . ?
C7 C8 Lu2 71.34(6) . . ?
C10 C9 C8 119.1 . . ?
C10 C9 C4 111.7 . . ?
C8 C9 C4 123.8 . . ?
C10 C9 Lu2 100.31(7) . . ?
C8 C9 Lu2 85.98(5) . . ?
C4 C9 Lu2 61.94(6) . . ?
C9 C10 C27 119.8 . . ?
C9 C10 C11 121.2 . . ?
C27 C10 C11 109.3 . . ?
C9 C10 Lu6 99.51(12) . . ?
C27 C10 Lu6 90.00(8) . . ?
C11 C10 Lu6 48.51(16) . . ?
C9 C10 Lu3 109.91(9) . . ?
C27 C10 Lu3 73.93(16) . . ?
C11 C10 Lu3 54.59(12) . . ?
Lu6 C10 Lu3 16.36(14) . . ?
C9 C10 Lu2 53.9 . . ?
C27 C10 Lu2 103.4 . . ?
C11 C10 Lu2 86.1 . . ?
Lu6 C10 Lu2 46.64(13) . . ?
Lu3 C10 Lu2 56.04(9) . . ?
C29 C11 C10 105.5 . . ?
C29 C11 C12 123.3 . . ?
C10 C11 C12 118.6 . . ?
C29 C11 Lu6 69.87(11) . . ?
C10 C11 Lu6 102.5(2) . . ?
C12 C11 Lu6 67.48(11) . . ?
C29 C11 Lu3 52.45(14) . . ?
C10 C11 Lu3 96.73(12) . . ?
C12 C11 Lu3 87.15(17) . . ?
Lu6 C11 Lu3 20.02(15) . . ?
C29 C11 Lu10 52.72(19) . . ?
C10 C11 Lu10 87.4(3) . . ?
C12 C11 Lu10 94.1(2) . . ?
Lu6 C11 Lu10 26.7(3) . . ?
Lu3 C11 Lu10 9.7(2) . . ?
C3 C12 C13 114.1 . . ?
C3 C12 C11 124.1 . . ?
C13 C12 C11 116.8 . . ?
C3 C12 Lu6 108.02(17) . . ?
C13 C12 Lu6 66.45(19) . . ?
C11 C12 Lu6 74.00(14) . . ?
C3 C12 Lu3 117.10(9) . . ?
C13 C12 Lu3 72.21(10) . . ?
C11 C12 Lu3 61.64(11) . . ?
Lu6 C12 Lu3 12.86(17) . . ?
C3 C12 Lu2 58.06(6) . . ?
C13 C12 Lu2 101.1 . . ?
C11 C12 Lu2 90.6 . . ?
Lu6 C12 Lu2 52.43(19) . . ?
Lu3 C12 Lu2 59.38(9) . . ?
C3 C12 Lu11 103.5(4) . . ?
C13 C12 Lu11 52.3(6) . . ?
C11 C12 Lu11 90.3(3) . . ?
Lu6 C12 Lu11 17.1(5) . . ?
Lu3 C12 Lu11 28.7(3) . . ?
Lu2 C12 Lu11 55.8(5) . . ?
C12 C13 C14 120.5 . . ?
C12 C13 C31 117.8 . . ?
C14 C13 C31 111.3 . . ?
C12 C13 Lu6 73.39(18) . . ?
C14 C13 Lu6 98.79(18) . . ?
C31 C13 Lu6 66.58(15) . . ?
C12 C13 Lu11 99.7(7) . . ?
C14 C13 Lu11 75.8(5) . . ?
C31 C13 Lu11 61.3(4) . . ?
Lu6 C13 Lu11 28.6(7) . . ?
C12 C13 Lu3 77.43(11) . . ?
C14 C13 Lu3 107.29(9) . . ?
C31 C13 Lu3 55.24(10) . . ?
Lu6 C13 Lu3 12.57(18) . . ?
Lu11 C13 Lu3 32.4(6) . . ?
C15 C14 C33 121.2 . . ?
C15 C14 C13 125.0 . . ?
C33 C14 C13 104.9 . . ?
C15 C14 Lu11 103.9(6) . . ?
C33 C14 Lu11 63.4(7) . . ?
C13 C14 Lu11 69.9(6) . . ?
C15 C14 Lu6 103.23(14) . . ?
C33 C14 Lu6 86.12(13) . . ?
C13 C14 Lu6 48.82(16) . . ?
Lu11 C14 Lu6 25.7(7) . . ?
C16 C15 C14 127.5 . . ?
C16 C15 C2 116.4 . . ?
C14 C15 C2 109.6 . . ?
C16 C15 Lu1 70.1 . . ?
C14 C15 Lu1 108.57(6) . . ?
C2 C15 Lu1 67.1 . . ?
C16 C15 Lu11 95.4(5) . . ?
C14 C15 Lu11 51.1(5) . . ?
C2 C15 Lu11 100.7(5) . . ?
Lu1 C15 Lu11 59.5(6) . . ?
C16 C15 Lu2 88.2 . . ?
C14 C15 Lu2 95.85(5) . . ?
C2 C15 Lu2 58.0 . . ?
Lu1 C15 Lu2 18.28(4) . . ?
Lu11 C15 Lu2 52.6(6) . . ?
C15 C16 C35 119.8 . . ?
C15 C16 C17 125.6 . . ?
C35 C16 C17 108.9 . . ?
C15 C16 Lu1 85.40(6) . . ?
C35 C16 Lu1 104.90(5) . . ?
C17 C16 Lu1 58.81(7) . . ?
C18 C17 C38 105.1 . . ?
C18 C17 C16 120.7 . . ?
C38 C17 C16 124.9 . . ?
C18 C17 C19 35.9 . . ?
C38 C17 C19 69.2 . . ?
C16 C17 C19 145.9 . . ?
C18 C17 Lu1 63.30(7) . . ?
C38 C17 Lu1 84.22(7) . . ?
C16 C17 Lu1 90.05(9) . . ?
C19 C17 Lu1 58.65(8) . . ?
C18 C17 Lu2 60.8 . . ?
C38 C17 Lu2 95.9 . . ?
C16 C17 Lu2 82.6 . . ?
C19 C17 Lu2 64.3 . . ?
Lu1 C17 Lu2 11.72(6) . . ?
C17 C18 C19 108.9 . . ?
C17 C18 C1 118.0 . . ?
C19 C18 C1 122.0 . . ?
C17 C18 C38 37.8 . . ?
C19 C18 C38 71.1 . . ?
C1 C18 C38 145.7 . . ?
C17 C18 Lu1 83.57(7) . . ?
C19 C18 Lu1 75.85(10) . . ?
C1 C18 Lu1 77.32(7) . . ?
C38 C18 Lu1 75.98(6) . . ?
C17 C18 C39 73.5 . . ?
C19 C18 C39 35.3 . . ?
C1 C18 C39 145.6 . . ?
C38 C18 C39 35.8 . . ?
Lu1 C18 C39 71.75(8) . . ?
C17 C18 Lu2 95.0 . . ?
C19 C18 Lu2 84.24(5) . . ?
C1 C18 Lu2 60.4 . . ?
C38 C18 Lu2 92.9 . . ?
Lu1 C18 Lu2 17.26(5) . . ?
C39 C18 Lu2 87.4 . . ?
C39 C19 C20 122.3 . . ?
C39 C19 C18 108.8 . . ?
C20 C19 C18 116.7 . . ?
C39 C19 C38 37.0 . . ?
C20 C19 C38 146.6 . . ?
C18 C19 C38 71.8 . . ?
C39 C19 C17 73.6 . . ?
C20 C19 C17 141.1 . . ?
C18 C19 C17 35.2 . . ?
C38 C19 C17 36.6 . . ?
C39 C19 Lu1 86.43(6) . . ?
C20 C19 Lu1 79.17(7) . . ?
C18 C19 Lu1 68.74(9) . . ?
C38 C19 Lu1 74.31(6) . . ?
C17 C19 Lu1 65.91(8) . . ?
C39 C19 Lu2 99.8 . . ?
C20 C19 Lu2 67.6 . . ?
C18 C19 Lu2 69.3 . . ?
C38 C19 Lu2 88.2 . . ?
C17 C19 Lu2 75.0 . . ?
Lu1 C19 Lu2 14.32(5) . . ?
C19 C20 C6 124.9 . . ?
C19 C20 C21 118.0 . . ?
C6 C20 C21 108.6 . . ?
C19 C20 Lu1 67.72(6) . . ?
C6 C20 Lu1 78.73(6) . . ?
C21 C20 Lu1 97.67(8) . . ?
C19 C20 Lu2 86.2 . . ?
C6 C20 Lu2 59.6 . . ?
C21 C20 Lu2 96.86(5) . . ?
Lu1 C20 Lu2 20.33(5) . . ?
C22 C21 C20 106.6 . . ?
C22 C21 C41 115.7 . . ?
C20 C21 C41 128.8 . . ?
C22 C21 Lu7 83.5(4) . . ?
C20 C21 Lu7 111.6(4) . . ?
C41 C21 Lu7 50.2(3) . . ?
C22 C21 Lu1 91.9 . . ?
C20 C21 Lu1 53.85(6) . . ?
C41 C21 Lu1 96.0 . . ?
Lu7 C21 Lu1 58.4(4) . . ?
C22 C21 Lu8 61.52(11) . . ?
C20 C21 Lu8 107.43(12) . . ?
C41 C21 Lu8 71.84(11) . . ?
Lu7 C21 Lu8 23.8(4) . . ?
Lu1 C21 Lu8 55.50(12) . . ?
C23 C22 C21 119.1 . . ?
C23 C22 C7 123.7 . . ?
C21 C22 C7 109.7 . . ?
C23 C22 Lu8 55.75(13) . . ?
C21 C22 Lu8 92.43(13) . . ?
C7 C22 Lu8 97.84(13) . . ?
C23 C22 Lu7 64.0(3) . . ?
C21 C22 Lu7 69.6(2) . . ?
C7 C22 Lu7 113.6(4) . . ?
Lu8 C22 Lu7 24.6(3) . . ?
C23 C22 Lu2 106.95(5) . . ?
C21 C22 Lu2 79.9 . . ?
C7 C22 Lu2 55.0 . . ?
Lu8 C22 Lu2 53.50(13) . . ?
Lu7 C22 Lu2 60.1(4) . . ?
C22 C23 C43 129.3 . . ?
C22 C23 C24 110.7 . . ?
C43 C23 C24 111.5 . . ?
C22 C23 Lu8 97.18(15) . . ?
C43 C23 Lu8 69.47(15) . . ?
C24 C23 Lu8 73.83(16) . . ?
C22 C23 Lu7 91.31(15) . . ?
C43 C23 Lu7 54.1(3) . . ?
C24 C23 Lu7 101.0(3) . . ?
Lu8 C23 Lu7 27.5(3) . . ?
C22 C23 Lu4 98.38(15) . . ?
C43 C23 Lu4 50.48(10) . . ?
C24 C23 Lu4 96.20(14) . . ?
Lu8 C23 Lu4 24.35(19) . . ?
Lu7 C23 Lu4 7.45(16) . . ?
C46 C24 C25 114.2 . . ?
C46 C24 C23 122.4 . . ?
C25 C24 C23 113.6 . . ?
C46 C24 C26 71.5 . . ?
C25 C24 C26 42.9 . . ?
C23 C24 C26 148.3 . . ?
C46 C24 Lu8 75.42(15) . . ?
C25 C24 Lu8 99.35(15) . . ?
C23 C24 Lu8 66.81(16) . . ?
C26 C24 Lu8 93.30(16) . . ?
C8 C25 C24 137.6 . . ?
C8 C25 C26 117.5 . . ?
C24 C25 C26 99.7 . . ?
C8 C25 C7 38.7 . . ?
C24 C25 C7 98.9 . . ?
C26 C25 C7 148.8 . . ?
C8 C25 Lu8 102.40(12) . . ?
C24 C25 Lu8 54.41(13) . . ?
C26 C25 Lu8 91.40(13) . . ?
C7 C25 Lu8 79.44(13) . . ?
C47 C26 C27 118.0 . . ?
C47 C26 C25 115.2 . . ?
C27 C26 C25 117.1 . . ?
C47 C26 C46 42.8 . . ?
C27 C26 C46 148.1 . . ?
C25 C26 C46 72.4 . . ?
C47 C26 C24 77.9 . . ?
C27 C26 C24 146.5 . . ?
C25 C26 C24 37.4 . . ?
C46 C26 C24 35.1 . . ?
C26 C27 C10 121.8 . . ?
C26 C27 C28 124.2 . . ?
C10 C27 C28 108.1 . . ?
C26 C27 C47 28.8 . . ?
C10 C27 C47 144.3 . . ?
C28 C27 C47 95.4 . . ?
C26 C27 Lu3 111.18(12) . . ?
C10 C27 Lu3 78.22(17) . . ?
C28 C27 Lu3 54.46(11) . . ?
C47 C27 Lu3 95.22(15) . . ?
C26 C27 Lu10 97.1(4) . . ?
C10 C27 Lu10 90.6(3) . . ?
C28 C27 Lu10 56.9(2) . . ?
C47 C27 Lu10 80.0(4) . . ?
Lu3 C27 Lu10 15.3(3) . . ?
C26 C27 Lu6 115.13(14) . . ?
C10 C27 Lu6 63.87(9) . . ?
C28 C27 Lu6 65.16(10) . . ?
C47 C27 Lu6 105.12(13) . . ?
Lu3 C27 Lu6 14.65(16) . . ?
Lu10 C27 Lu6 27.3(3) . . ?
C29 C28 C27 106.6 . . ?
C29 C28 C49 121.6 . . ?
C27 C28 C49 116.7 . . ?
C29 C28 Lu3 54.08(17) . . ?
C27 C28 Lu3 96.41(12) . . ?
C49 C28 Lu3 83.0(2) . . ?
C29 C28 Lu10 72.0(4) . . ?
C27 C28 Lu10 94.8(2) . . ?
C49 C28 Lu10 67.4(3) . . ?
Lu3 C28 Lu10 18.2(3) . . ?
C29 C28 Lu5 87.03(13) . . ?
C27 C28 Lu5 95.94(10) . . ?
C49 C28 Lu5 52.77(13) . . ?
Lu3 C28 Lu5 34.09(16) . . ?
Lu10 C28 Lu5 16.0(3) . . ?
C29 C28 Lu6 45.92(16) . . ?
C27 C28 Lu6 88.49(13) . . ?
C49 C28 Lu6 96.90(12) . . ?
Lu3 C28 Lu6 14.0(2) . . ?
Lu10 C28 Lu6 30.5(4) . . ?
Lu5 C28 Lu6 46.44(18) . . ?
C28 C29 C11 110.1 . . ?
C28 C29 C30 116.9 . . ?
C11 C29 C30 123.0 . . ?
C28 C29 Lu3 89.3(2) . . ?
C11 C29 Lu3 91.7(2) . . ?
C30 C29 Lu3 59.70(13) . . ?
C28 C29 Lu6 106.18(19) . . ?
C11 C29 Lu6 72.25(13) . . ?
C30 C29 Lu6 65.32(17) . . ?
Lu3 C29 Lu6 22.4(3) . . ?
C28 C29 Lu10 75.0(3) . . ?
C11 C29 Lu10 100.1(2) . . ?
C30 C29 Lu10 65.0(3) . . ?
Lu3 C29 Lu10 14.8(3) . . ?
Lu6 C29 Lu10 36.3(3) . . ?
C28 C29 Lu11 108.0(5) . . ?
C11 C29 Lu11 85.3(3) . . ?
C30 C29 Lu11 51.4(5) . . ?
Lu3 C29 Lu11 18.7(5) . . ?
Lu6 C29 Lu11 14.4(4) . . ?
Lu10 C29 Lu11 33.2(5) . . ?
C28 C29 Lu5 66.29(10) . . ?
C11 C29 Lu5 107.60(9) . . ?
C30 C29 Lu5 67.09(9) . . ?
Lu3 C29 Lu5 24.8(2) . . ?
Lu6 C29 Lu5 46.49(16) . . ?
Lu10 C29 Lu5 10.2(3) . . ?
Lu11 C29 Lu5 42.7(4) . . ?
C29 C30 C51 123.2 . . ?
C29 C30 C31 110.9 . . ?
C51 C30 C31 119.0 . . ?
C29 C30 Lu3 74.34(16) . . ?
C51 C30 Lu3 82.3(3) . . ?
C31 C30 Lu3 87.3(3) . . ?
C29 C30 Lu6 75.02(18) . . ?
C51 C30 Lu6 101.50(18) . . ?
C31 C30 Lu6 65.90(17) . . ?
Lu3 C30 Lu6 23.6(3) . . ?
C29 C30 Lu10 80.1(2) . . ?
C51 C30 Lu10 66.9(3) . . ?
C31 C30 Lu10 99.5(3) . . ?
Lu3 C30 Lu10 16.3(3) . . ?
Lu6 C30 Lu10 39.5(4) . . ?
C29 C30 Lu11 101.9(7) . . ?
C51 C30 Lu11 83.5(4) . . ?
C31 C30 Lu11 58.4(5) . . ?
Lu3 C30 Lu11 34.2(7) . . ?
Lu6 C30 Lu11 27.2(7) . . ?
Lu10 C30 Lu11 41.9(6) . . ?
C29 C30 Lu5 85.86(11) . . ?
C51 C30 Lu5 55.20(12) . . ?
C31 C30 Lu5 107.72(9) . . ?
Lu3 C30 Lu5 28.5(2) . . ?
Lu6 C30 Lu5 51.39(19) . . ?
Lu10 C30 Lu5 12.2(3) . . ?
Lu11 C30 Lu5 49.3(5) . . ?
C32 C31 C13 104.4 . . ?
C32 C31 C30 117.0 . . ?
C13 C31 C30 126.5 . . ?
C32 C31 Lu6 97.5(2) . . ?
C13 C31 Lu6 70.86(11) . . ?
C30 C31 Lu6 71.45(12) . . ?
C32 C31 Lu11 65.1(8) . . ?
C13 C31 Lu11 82.1(3) . . ?
C30 C31 Lu11 85.9(4) . . ?
Lu6 C31 Lu11 32.4(8) . . ?
C32 C31 Lu3 98.47(12) . . ?
C13 C31 Lu3 92.08(19) . . ?
C30 C31 Lu3 51.30(16) . . ?
Lu6 C31 Lu3 22.08(16) . . ?
Lu11 C31 Lu3 38.8(7) . . ?
C32 C31 Lu10 91.54(19) . . ?
C13 C31 Lu10 98.58(19) . . ?
C30 C31 Lu10 50.7(2) . . ?
Lu6 C31 Lu10 27.7(2) . . ?
Lu11 C31 Lu10 36.0(6) . . ?
Lu3 C31 Lu10 8.5(2) . . ?
C33 C32 C53 115.9 . . ?
C33 C32 C31 109.2 . . ?
C53 C32 C31 122.2 . . ?
C33 C32 Lu11 79.6(3) . . ?
C53 C32 Lu11 80.0(5) . . ?
C31 C32 Lu11 74.4(8) . . ?
C33 C32 Lu6 88.98(9) . . ?
C53 C32 Lu6 96.92(13) . . ?
C31 C32 Lu6 49.04(17) . . ?
Lu11 C32 Lu6 25.4(8) . . ?
C33 C32 Lu3 104.31(13) . . ?
C53 C32 Lu3 83.30(16) . . ?
C31 C32 Lu3 51.09(11) . . ?
Lu11 C32 Lu3 29.4(7) . . ?
Lu6 C32 Lu3 17.16(14) . . ?
C34 C33 C14 109.3 . . ?
C34 C33 C32 127.1 . . ?
C14 C33 C32 110.2 . . ?
C34 C33 Lu11 90.7(7) . . ?
C14 C33 Lu11 82.2(6) . . ?
C32 C33 Lu11 61.7(5) . . ?
C34 C33 Lu6 107.15(15) . . ?
C14 C33 Lu6 64.99(9) . . ?
C32 C33 Lu6 61.89(10) . . ?
Lu11 C33 Lu6 20.9(7) . . ?
C33 C34 C35 130.7 . . ?
C33 C34 C55 115.9 . . ?
C35 C34 C55 107.1 . . ?
C33 C34 Lu11 57.7(6) . . ?
C35 C34 Lu11 106.9(5) . . ?
C55 C34 Lu11 83.7(5) . . ?
C34 C35 C36 108.3 . . ?
C34 C35 C16 111.3 . . ?
C36 C35 C16 127.4 . . ?
C37 C36 C35 119.6 . . ?
C37 C36 C56 120.1 . . ?
C35 C36 C56 111.6 . . ?
C36 C37 C59 114.1 . . ?
C36 C37 C38 114.6 . . ?
C59 C37 C38 122.6 . . ?
C39 C38 C17 111.4 . . ?
C39 C38 C37 118.1 . . ?
C17 C38 C37 123.1 . . ?
C39 C38 C19 37.3 . . ?
C17 C38 C19 74.2 . . ?
C37 C38 C19 149.3 . . ?
C39 C38 C18 74.4 . . ?
C17 C38 C18 37.1 . . ?
C37 C38 C18 152.7 . . ?
C19 C38 C18 37.1 . . ?
C39 C38 Lu1 71.29(8) . . ?
C17 C38 Lu1 65.24(7) . . ?
C37 C38 Lu1 105.81(6) . . ?
C19 C38 Lu1 55.29(7) . . ?
C18 C38 Lu1 52.77(6) . . ?
C38 C39 C19 105.7 . . ?
C38 C39 C40 123.4 . . ?
C19 C39 C40 124.3 . . ?
C38 C39 C18 69.9 . . ?
C19 C39 C18 35.9 . . ?
C40 C39 C18 151.0 . . ?
C38 C39 Lu1 79.28(7) . . ?
C19 C39 Lu1 62.13(6) . . ?
C40 C39 Lu1 100.51(7) . . ?
C18 C39 Lu1 53.94(7) . . ?
C60 C40 C39 118.1 . . ?
C60 C40 C41 113.8 . . ?
C39 C40 C41 120.5 . . ?
C60 C40 Lu7 73.6(6) . . ?
C39 C40 Lu7 110.1(4) . . ?
C41 C40 Lu7 59.9(7) . . ?
C60 C40 Lu4 66.51(9) . . ?
C39 C40 Lu4 112.92(10) . . ?
C41 C40 Lu4 64.65(9) . . ?
Lu7 C40 Lu4 7.1(6) . . ?
C60 C40 Lu1 105.81(5) . . ?
C39 C40 Lu1 52.12(5) . . ?
C41 C40 Lu1 87.83(5) . . ?
Lu7 C40 Lu1 58.4(4) . . ?
Lu4 C40 Lu1 62.20(10) . . ?
C42 C41 C40 124.3 . . ?
C42 C41 C21 120.2 . . ?
C40 C41 C21 105.7 . . ?
C42 C41 Lu7 60.9(4) . . ?
C40 C41 Lu7 84.5(7) . . ?
C21 C41 Lu7 97.9(5) . . ?
C42 C41 Lu4 56.89(13) . . ?
C40 C41 Lu4 84.41(10) . . ?
C21 C41 Lu4 103.61(9) . . ?
Lu7 C41 Lu4 5.9(5) . . ?
C42 C41 Lu8 62.59(12) . . ?
C40 C41 Lu8 100.20(12) . . ?
C21 C41 Lu8 79.56(11) . . ?
Lu7 C41 Lu8 21.5(7) . . ?
Lu4 C41 Lu8 25.96(14) . . ?
C42 C41 Lu9 57.3(4) . . ?
C40 C41 Lu9 83.1(5) . . ?
C21 C41 Lu9 104.7(3) . . ?
Lu7 C41 Lu9 6.8(6) . . ?
Lu4 C41 Lu9 1.5(5) . . ?
Lu8 C41 Lu9 27.4(4) . . ?
C41 C42 C43 122.8 . . ?
C41 C42 C62 120.3 . . ?
C43 C42 C62 104.3 . . ?
C41 C42 Lu7 82.94(15) . . ?
C43 C42 Lu7 81.1(6) . . ?
C62 C42 Lu7 69.5(6) . . ?
C41 C42 Lu4 93.0(2) . . ?
C43 C42 Lu4 79.64(14) . . ?
C62 C42 Lu4 59.56(14) . . ?
Lu7 C42 Lu4 11.3(3) . . ?
C41 C42 Lu9 97.8(5) . . ?
C43 C42 Lu9 78.6(5) . . ?
C62 C42 Lu9 55.6(4) . . ?
Lu7 C42 Lu9 16.3(5) . . ?
Lu4 C42 Lu9 5.0(5) . . ?
C41 C42 Lu8 91.62(13) . . ?
C43 C42 Lu8 56.41(13) . . ?
C62 C42 Lu8 85.39(12) . . ?
Lu7 C42 Lu8 25.9(7) . . ?
Lu4 C42 Lu8 29.44(16) . . ?
Lu9 C42 Lu8 31.7(5) . . ?
C42 C43 C23 112.6 . . ?
C42 C43 C44 115.0 . . ?
C23 C43 C44 119.3 . . ?
C42 C43 Lu7 60.6(4) . . ?
C23 C43 Lu7 94.1(5) . . ?
C44 C43 Lu7 78.83(19) . . ?
C42 C43 Lu8 92.54(16) . . ?
C23 C43 Lu8 73.62(15) . . ?
C44 C43 Lu8 68.92(16) . . ?
Lu7 C43 Lu8 32.9(4) . . ?
C42 C43 Lu4 65.39(18) . . ?
C23 C43 Lu4 101.78(13) . . ?
C44 C43 Lu4 68.0(2) . . ?
Lu7 C43 Lu4 11.2(3) . . ?
Lu8 C43 Lu4 33.21(19) . . ?
C42 C43 Lu9 71.4(4) . . ?
C23 C43 Lu9 104.2(4) . . ?
C44 C43 Lu9 60.5(4) . . ?
Lu7 C43 Lu9 18.4(4) . . ?
Lu8 C43 Lu9 32.2(4) . . ?
Lu4 C43 Lu9 7.6(5) . . ?
C45 C44 C43 124.6 . . ?
C45 C44 C63 128.4 . . ?
C43 C44 C63 98.2 . . ?
C45 C44 C66 32.9 . . ?
C43 C44 C66 149.1 . . ?
C63 C44 C66 95.8 . . ?
C45 C44 Lu8 75.58(17) . . ?
C43 C44 Lu8 72.31(17) . . ?
C63 C44 Lu8 94.37(16) . . ?
C66 C44 Lu8 79.25(18) . . ?
C45 C44 Lu4 100.94(17) . . ?
C43 C44 Lu4 75.3(2) . . ?
C63 C44 Lu4 60.27(11) . . ?
C66 C44 Lu4 88.2(2) . . ?
Lu8 C44 Lu4 34.42(19) . . ?
C45 C44 Lu9 93.5(4) . . ?
C43 C44 Lu9 86.8(4) . . ?
C63 C44 Lu9 58.4(4) . . ?
C66 C44 Lu9 77.3(4) . . ?
Lu8 C44 Lu9 36.8(5) . . ?
Lu4 C44 Lu9 11.6(4) . . ?
C45 C44 Lu7 104.5(4) . . ?
C43 C44 Lu7 64.3(5) . . ?
C63 C44 Lu7 66.8(5) . . ?
C66 C44 Lu7 96.8(4) . . ?
Lu8 C44 Lu7 31.4(4) . . ?
Lu4 C44 Lu7 11.3(6) . . ?
Lu9 C44 Lu7 22.5(6) . . ?
C66 C45 C44 108.3 . . ?
C66 C45 C46 131.8 . . ?
C44 C45 C46 114.5 . . ?
C66 C45 Lu8 98.76(16) . . ?
C44 C45 Lu8 68.60(17) . . ?
C46 C45 Lu8 77.79(15) . . ?
C66 C45 Lu9 76.7(4) . . ?
C44 C45 Lu9 57.2(4) . . ?
C46 C45 Lu9 108.6(3) . . ?
Lu8 C45 Lu9 30.9(4) . . ?
C66 C45 Lu4 86.11(15) . . ?
C44 C45 Lu4 51.05(11) . . ?
C46 C45 Lu4 103.74(12) . . ?
Lu8 C45 Lu4 26.68(18) . . ?
Lu9 C45 Lu4 9.5(4) . . ?
C66 C45 Lu7 94.4(5) . . ?
C44 C45 Lu7 49.7(4) . . ?
C46 C45 Lu7 96.5(4) . . ?
Lu8 C45 Lu7 21.7(3) . . ?
Lu9 C45 Lu7 17.7(5) . . ?
Lu4 C45 Lu7 8.6(5) . . ?
C24 C46 C45 126.3 . . ?
C24 C46 C47 104.7 . . ?
C45 C46 C47 119.1 . . ?
C24 C46 C26 73.3 . . ?
C45 C46 C26 142.4 . . ?
C47 C46 C26 31.4 . . ?
C24 C46 Lu8 73.95(15) . . ?
C45 C46 Lu8 67.47(14) . . ?
C47 C46 Lu8 103.10(16) . . ?
C26 C46 Lu8 93.34(15) . . ?
C26 C47 C48 131.5 . . ?
C26 C47 C46 105.8 . . ?
C48 C47 C46 114.8 . . ?
C26 C47 C27 33.2 . . ?
C48 C47 C27 98.4 . . ?
C46 C47 C27 132.1 . . ?
C26 C47 Lu5 96.63(14) . . ?
C48 C47 Lu5 55.85(10) . . ?
C46 C47 Lu5 94.81(11) . . ?
C27 C47 Lu5 75.52(15) . . ?
C26 C47 Lu8 89.05(11) . . ?
C48 C47 Lu8 97.60(12) . . ?
C46 C47 Lu8 49.25(12) . . ?
C27 C47 Lu8 94.84(11) . . ?
Lu5 C47 Lu8 50.48(14) . . ?
C47 C48 C67 118.5 . . ?
C47 C48 C49 113.2 . . ?
C67 C48 C49 108.4 . . ?
C47 C48 Lu5 97.39(12) . . ?
C67 C48 Lu5 66.38(18) . . ?
C49 C48 Lu5 60.90(14) . . ?
C47 C48 Lu10 91.09(17) . . ?
C67 C48 Lu10 81.7(3) . . ?
C49 C48 Lu10 50.9(3) . . ?
Lu5 C48 Lu10 15.4(2) . . ?
C50 C49 C28 127.5 . . ?
C50 C49 C48 107.6 . . ?
C28 C49 C48 115.3 . . ?
C50 C49 Lu5 57.12(14) . . ?
C28 C49 Lu5 97.1(2) . . ?
C48 C49 Lu5 85.38(17) . . ?
C50 C49 Lu10 65.7(2) . . ?
C28 C49 Lu10 78.0(4) . . ?
C48 C49 Lu10 100.3(4) . . ?
Lu5 C49 Lu10 20.5(3) . . ?
C50 C49 Lu3 72.38(13) . . ?
C28 C49 Lu3 63.62(14) . . ?
C48 C49 Lu3 114.07(10) . . ?
Lu5 C49 Lu3 37.51(17) . . ?
Lu10 C49 Lu3 17.1(4) . . ?
C49 C50 C68 107.6 . . ?
C49 C50 C51 107.8 . . ?
C68 C50 C51 135.8 . . ?
C49 C50 Lu5 84.17(17) . . ?
C68 C50 Lu5 74.1(2) . . ?
C51 C50 Lu5 84.1(2) . . ?
C49 C50 Lu10 77.5(2) . . ?
C68 C50 Lu10 96.2(5) . . ?
C51 C50 Lu10 67.0(5) . . ?
Lu5 C50 Lu10 22.1(4) . . ?
C49 C50 Lu3 75.25(10) . . ?
C68 C50 Lu3 112.63(10) . . ?
C51 C50 Lu3 53.97(11) . . ?
Lu5 C50 Lu3 38.6(2) . . ?
Lu10 C50 Lu3 16.5(4) . . ?
C52 C51 C30 123.6 . . ?
C52 C51 C50 101.1 . . ?
C30 C51 C50 122.0 . . ?
C52 C51 Lu3 97.36(12) . . ?
C30 C51 Lu3 54.53(18) . . ?
C50 C51 Lu3 87.9(2) . . ?
C52 C51 Lu10 89.4(3) . . ?
C30 C51 Lu10 75.1(5) . . ?
C50 C51 Lu10 70.1(4) . . ?
Lu3 C51 Lu10 21.2(4) . . ?
C52 C51 Lu5 81.43(14) . . ?
C30 C51 Lu5 95.07(19) . . ?
C50 C51 Lu5 54.23(14) . . ?
Lu3 C51 Lu5 41.53(18) . . ?
Lu10 C51 Lu5 20.3(4) . . ?
C52 C51 Lu6 93.80(14) . . ?
C30 C51 Lu6 47.20(16) . . ?
C50 C51 Lu6 100.87(15) . . ?
Lu3 C51 Lu6 13.0(2) . . ?
Lu10 C51 Lu6 32.6(5) . . ?
Lu5 C51 Lu6 52.4(2) . . ?
C52 C51 Lu11 69.5(6) . . ?
C30 C51 Lu11 64.9(5) . . ?
C50 C51 Lu11 106.5(6) . . ?
Lu3 C51 Lu11 31.3(6) . . ?
Lu10 C51 Lu11 38.8(7) . . ?
Lu5 C51 Lu11 52.3(6) . . ?
Lu6 C51 Lu11 24.4(6) . . ?
C51 C52 C53 115.8 . . ?
C51 C52 C70 128.7 . . ?
C53 C52 C70 108.0 . . ?
C51 C52 Lu10 57.1(3) . . ?
C53 C52 Lu10 98.4(3) . . ?
C70 C52 Lu10 92.2(4) . . ?
C51 C52 Lu5 65.83(13) . . ?
C53 C52 Lu5 110.33(12) . . ?
C70 C52 Lu5 75.11(18) . . ?
Lu10 C52 Lu5 18.6(3) . . ?
C51 C52 Lu11 79.9(6) . . ?
C53 C52 Lu11 59.7(6) . . ?
C70 C52 Lu11 101.6(6) . . ?
Lu10 C52 Lu11 38.7(6) . . ?
Lu5 C52 Lu11 52.1(6) . . ?
C51 C52 Lu3 50.93(10) . . ?
C53 C52 Lu3 87.79(16) . . ?
C70 C52 Lu3 108.31(12) . . ?
Lu10 C52 Lu3 17.1(3) . . ?
Lu5 C52 Lu3 35.66(16) . . ?
Lu11 C52 Lu3 31.7(6) . . ?
C51 C52 Lu6 59.55(11) . . ?
C53 C52 Lu6 74.35(10) . . ?
C70 C52 Lu6 112.07(15) . . ?
Lu10 C52 Lu6 27.5(4) . . ?
Lu5 C52 Lu6 45.4(2) . . ?
Lu11 C52 Lu6 20.4(6) . . ?
Lu3 C52 Lu6 13.44(18) . . ?
C32 C53 C54 120.1 . . ?
C32 C53 C52 121.5 . . ?
C54 C53 C52 107.3 . . ?
C32 C53 Lu11 61.3(6) . . ?
C54 C53 Lu11 91.6(7) . . ?
C52 C53 Lu11 86.7(4) . . ?
C32 C53 Lu3 68.42(16) . . ?
C54 C53 Lu3 111.63(8) . . ?
C52 C53 Lu3 63.38(16) . . ?
Lu11 C53 Lu3 27.6(5) . . ?
C32 C53 Lu6 55.84(12) . . ?
C54 C53 Lu6 108.43(14) . . ?
C52 C53 Lu6 78.97(8) . . ?
Lu11 C53 Lu6 17.2(7) . . ?
Lu3 C53 Lu6 15.59(15) . . ?
C32 C53 Lu10 82.5(3) . . ?
C54 C53 Lu10 102.0(3) . . ?
C52 C53 Lu10 54.5(2) . . ?
Lu11 C53 Lu10 32.3(4) . . ?
Lu3 C53 Lu10 14.5(2) . . ?
Lu6 C53 Lu10 27.4(3) . . ?
C55 C54 C53 122.9 . . ?
C55 C54 C71 116.6 . . ?
C53 C54 C71 109.6 . . ?
C55 C54 Lu11 83.2(3) . . ?
C53 C54 Lu11 56.5(6) . . ?
C71 C54 Lu11 100.2(5) . . ?
C56 C55 C54 120.8 . . ?
C56 C55 C34 114.6 . . ?
C54 C55 C34 117.6 . . ?
C56 C55 Lu11 113.9(6) . . ?
C54 C55 Lu11 67.7(2) . . ?
C34 C55 Lu11 65.4(3) . . ?
C55 C56 C57 123.0 . . ?
C55 C56 C36 98.4 . . ?
C57 C56 C36 119.4 . . ?
C58 C57 C72 123.2 . . ?
C58 C57 C56 116.3 . . ?
C72 C57 C56 116.3 . . ?
C57 C58 C76 119.9 . . ?
C57 C58 C59 120.4 . . ?
C76 C58 C59 107.7 . . ?
C57 C58 Lu9 95.2(4) . . ?
C76 C58 Lu9 51.1(4) . . ?
C59 C58 Lu9 87.9(3) . . ?
C57 C58 Lu4 102.23(13) . . ?
C76 C58 Lu4 51.59(11) . . ?
C59 C58 Lu4 80.10(17) . . ?
Lu9 C58 Lu4 8.6(3) . . ?
C60 C59 C37 117.5 . . ?
C60 C59 C58 106.8 . . ?
C37 C59 C58 127.2 . . ?
C59 C60 C61 109.5 . . ?
C59 C60 C40 120.0 . . ?
C61 C60 C40 120.6 . . ?
C59 C60 Lu7 105.1(6) . . ?
C61 C60 Lu7 62.6(3) . . ?
C40 C60 Lu7 74.1(4) . . ?
C59 C60 Lu4 100.19(12) . . ?
C61 C60 Lu4 55.26(13) . . ?
C40 C60 Lu4 84.30(15) . . ?
Lu7 C60 Lu4 10.2(4) . . ?
C59 C60 Lu9 93.1(5) . . ?
C61 C60 Lu9 53.0(4) . . ?
C40 C60 Lu9 92.0(4) . . ?
Lu7 C60 Lu9 18.3(6) . . ?
Lu4 C60 Lu9 8.6(4) . . ?
C62 C61 C76 116.8 . . ?
C62 C61 C60 125.6 . . ?
C76 C61 C60 107.1 . . ?
C62 C61 Lu4 60.85(13) . . ?
C76 C61 Lu4 86.56(19) . . ?
C60 C61 Lu4 93.0(2) . . ?
C62 C61 Lu7 60.9(6) . . ?
C76 C61 Lu7 97.1(6) . . ?
C60 C61 Lu7 84.1(2) . . ?
Lu4 C61 Lu7 12.1(3) . . ?
C62 C61 Lu9 65.7(6) . . ?
C76 C61 Lu9 75.3(5) . . ?
C60 C61 Lu9 98.4(5) . . ?
Lu4 C61 Lu9 11.5(5) . . ?
Lu7 C61 Lu9 23.3(5) . . ?
C63 C62 C61 124.5 . . ?
C63 C62 C42 107.1 . . ?
C61 C62 C42 115.2 . . ?
C63 C62 Lu4 73.2(3) . . ?
C61 C62 Lu4 81.44(13) . . ?
C42 C62 Lu4 78.7(2) . . ?
C63 C62 Lu7 83.27(17) . . ?
C61 C62 Lu7 82.8(8) . . ?
C42 C62 Lu7 66.0(7) . . ?
Lu4 C62 Lu7 13.9(5) . . ?
C63 C62 Lu9 66.0(6) . . ?
C61 C62 Lu9 79.6(7) . . ?
C42 C62 Lu9 89.8(5) . . ?
Lu4 C62 Lu9 11.7(5) . . ?
Lu7 C62 Lu9 25.5(6) . . ?
C63 C62 Lu8 67.16(12) . . ?
C61 C62 Lu8 100.40(12) . . ?
C42 C62 Lu8 64.46(12) . . ?
Lu4 C62 Lu8 20.06(16) . . ?
Lu7 C62 Lu8 19.1(6) . . ?
Lu9 C62 Lu8 27.6(6) . . ?
C62 C63 C64 116.9 . . ?
C62 C63 C44 114.5 . . ?
C64 C63 C44 113.4 . . ?
C62 C63 Lu4 66.9(2) . . ?
C64 C63 Lu4 84.0(2) . . ?
C44 C63 Lu4 79.87(10) . . ?
C62 C63 Lu9 76.8(5) . . ?
C64 C63 Lu9 70.8(5) . . ?
C44 C63 Lu9 83.1(7) . . ?
Lu4 C63 Lu9 13.5(5) . . ?
C62 C63 Lu7 60.7(3) . . ?
C64 C63 Lu7 94.7(6) . . ?
C44 C63 Lu7 76.4(6) . . ?
Lu4 C63 Lu7 10.7(6) . . ?
Lu9 C63 Lu7 24.2(7) . . ?
C62 C63 Lu8 85.88(14) . . ?
C64 C63 Lu8 92.04(14) . . ?
C44 C63 Lu8 52.91(13) . . ?
Lu4 C63 Lu8 27.33(17) . . ?
Lu9 C63 Lu8 31.1(7) . . ?
Lu7 C63 Lu8 27.1(5) . . ?
C75 C64 C65 115.5 . . ?
C75 C64 C63 123.4 . . ?
C65 C64 C63 112.2 . . ?
C75 C64 Lu9 82.4(7) . . ?
C65 C64 Lu9 91.5(5) . . ?
C63 C64 Lu9 67.6(6) . . ?
C75 C64 Lu4 86.78(10) . . ?
C65 C64 Lu4 97.72(15) . . ?
C63 C64 Lu4 58.04(14) . . ?
Lu9 C64 Lu4 9.9(6) . . ?
C75 C64 Lu7 89.0(6) . . ?
C65 C64 Lu7 99.9(3) . . ?
C63 C64 Lu7 54.0(5) . . ?
Lu9 C64 Lu7 14.0(7) . . ?
Lu4 C64 Lu7 4.1(5) . . ?
C64 C65 C66 124.5 . . ?
C64 C65 C74 96.1 . . ?
C66 C65 C74 125.1 . . ?
C64 C65 Lu9 56.2(4) . . ?
C66 C65 Lu9 87.2(5) . . ?
C74 C65 Lu9 87.5(6) . . ?
C64 C65 Lu4 54.75(9) . . ?
C66 C65 Lu4 83.97(7) . . ?
C74 C65 Lu4 94.08(10) . . ?
Lu9 C65 Lu4 6.6(6) . . ?
C64 C65 Lu8 78.58(12) . . ?
C66 C65 Lu8 60.46(11) . . ?
C74 C65 Lu8 100.30(12) . . ?
Lu9 C65 Lu8 27.0(5) . . ?
Lu4 C65 Lu8 25.07(13) . . ?
C45 C66 C65 131.9 . . ?
C45 C66 C67 110.8 . . ?
C65 C66 C67 109.7 . . ?
C45 C66 C44 38.9 . . ?
C65 C66 C44 93.5 . . ?
C67 C66 C44 144.5 . . ?
C45 C66 Lu8 55.68(13) . . ?
C65 C66 Lu8 93.61(12) . . ?
C67 C66 Lu8 98.63(14) . . ?
C44 C66 Lu8 52.12(14) . . ?
C45 C66 Lu9 78.7(5) . . ?
C65 C66 Lu9 63.4(4) . . ?
C67 C66 Lu9 110.8(4) . . ?
C44 C66 Lu9 55.9(5) . . ?
Lu8 C66 Lu9 30.4(4) . . ?
C45 C66 Lu5 98.67(11) . . ?
C65 C66 Lu5 87.25(11) . . ?
C67 C66 Lu5 51.03(8) . . ?
C44 C66 Lu5 106.17(9) . . ?
Lu8 C66 Lu5 54.16(16) . . ?
Lu9 C66 Lu5 59.7(4) . . ?
C45 C66 Lu4 70.90(11) . . ?
C65 C66 Lu4 69.39(10) . . ?
C67 C66 Lu4 114.60(10) . . ?
C44 C66 Lu4 48.57(11) . . ?
Lu8 C66 Lu4 25.86(15) . . ?
Lu9 C66 Lu4 8.0(5) . . ?
Lu5 C66 Lu4 63.86(12) . . ?
C48 C67 C68 107.7 . . ?
C48 C67 C66 124.1 . . ?
C68 C67 C66 119.6 . . ?
C48 C67 Lu5 80.94(16) . . ?
C68 C67 Lu5 58.60(13) . . ?
C66 C67 Lu5 98.85(13) . . ?
C48 C67 Lu10 71.2(2) . . ?
C68 C67 Lu10 62.48(17) . . ?
C66 C67 Lu10 105.1(2) . . ?
Lu5 C67 Lu10 9.8(2) . . ?
C67 C68 C50 108.1 . . ?
C67 C68 C69 126.6 . . ?
C50 C68 C69 110.6 . . ?
C67 C68 Lu5 84.97(14) . . ?
C50 C68 Lu5 63.56(18) . . ?
C69 C68 Lu5 80.84(15) . . ?
C67 C68 Lu10 89.8(3) . . ?
C50 C68 Lu10 52.1(3) . . ?
C69 C68 Lu10 86.14(19) . . ?
Lu5 C68 Lu10 11.4(3) . . ?
C74 C69 C70 141.0 . . ?
C74 C69 C68 106.7 . . ?
C70 C69 C68 106.0 . . ?
C74 C69 Lu5 102.92(13) . . ?
C70 C69 Lu5 79.34(14) . . ?
C68 C69 Lu5 54.87(10) . . ?
C74 C69 Lu10 110.5(3) . . ?
C70 C69 Lu10 69.4(3) . . ?
C68 C69 Lu10 59.99(19) . . ?
Lu5 C69 Lu10 10.0(2) . . ?
C69 C70 C71 106.9 . . ?
C69 C70 C52 136.2 . . ?
C71 C70 C52 107.7 . . ?
C69 C70 Lu5 71.23(17) . . ?
C71 C70 Lu5 109.27(9) . . ?
C52 C70 Lu5 72.57(16) . . ?
C69 C70 Lu10 86.5(4) . . ?
C71 C70 Lu10 105.56(19) . . ?
C52 C70 Lu10 58.9(3) . . ?
Lu5 C70 Lu10 15.3(3) . . ?
C69 C70 Lu11 110.8(5) . . ?
C71 C70 Lu11 79.0(4) . . ?
C52 C70 Lu11 52.2(5) . . ?
Lu5 C70 Lu11 44.4(5) . . ?
Lu10 C70 Lu11 31.7(5) . . ?
C54 C71 C70 107.3 . . ?
C54 C71 C72 123.1 . . ?
C70 C71 C72 119.8 . . ?
C73 C72 C57 112.9 . . ?
C73 C72 C71 119.2 . . ?
C57 C72 C71 118.6 . . ?
C75 C73 C72 131.6 . . ?
C75 C73 C74 105.4 . . ?
C72 C73 C74 114.0 . . ?
C75 C73 Lu9 53.6(4) . . ?
C72 C73 Lu9 103.9(5) . . ?
C74 C73 Lu9 82.8(4) . . ?
C69 C74 C73 118.7 . . ?
C69 C74 C65 128.4 . . ?
C73 C74 C65 104.2 . . ?
C69 C74 Lu5 55.47(10) . . ?
C73 C74 Lu5 109.58(9) . . ?
C65 C74 Lu5 85.05(11) . . ?
C69 C74 Lu9 112.2(3) . . ?
C73 C74 Lu9 69.3(5) . . ?
C65 C74 Lu9 56.8(5) . . ?
Lu5 C74 Lu9 59.0(3) . . ?
C64 C75 C73 118.6 . . ?
C64 C75 C76 116.2 . . ?
C73 C75 C76 114.5 . . ?
C64 C75 Lu9 63.7(6) . . ?
C73 C75 Lu9 99.2(5) . . ?
C76 C75 Lu9 75.6(5) . . ?
C64 C75 Lu4 63.79(13) . . ?
C73 C75 Lu4 106.43(13) . . ?
C76 C75 Lu4 69.59(16) . . ?
Lu9 C75 Lu4 8.0(5) . . ?
C64 C75 Lu7 66.1(4) . . ?
C73 C75 Lu7 108.3(4) . . ?
C76 C75 Lu7 65.8(3) . . ?
Lu9 C75 Lu7 11.5(5) . . ?
Lu4 C75 Lu7 3.9(3) . . ?
C61 C76 C58 108.8 . . ?
C61 C76 C75 121.9 . . ?
C58 C76 C75 117.9 . . ?
C61 C76 Lu9 70.6(4) . . ?
C58 C76 Lu9 101.8(6) . . ?
C75 C76 Lu9 67.9(4) . . ?
C61 C76 Lu4 60.02(18) . . ?
C58 C76 Lu4 102.52(13) . . ?
C75 C76 Lu4 77.2(2) . . ?
Lu9 C76 Lu4 10.7(4) . . ?
C61 C76 Lu7 53.4(4) . . ?
C58 C76 Lu7 99.4(4) . . ?
C75 C76 Lu7 85.55(11) . . ?
Lu9 C76 Lu7 18.7(4) . . ?
Lu4 C76 Lu7 8.4(2) . . ?
N4A Ni1A N2A 177.7 . . ?
N4A Ni1A N1A 89.9 . 6_565 ?
N2A Ni1A N1A 90.0 . 6_565 ?
N4A Ni1A N1A 89.9 . . ?
N2A Ni1A N1A 90.0 . . ?
N1A Ni1A N1A 177.5 6_565 . ?
C2A N1A C1A 104.2 . . ?
C2A N1A Ni1A 128.0 . . ?
C1A N1A Ni1A 127.8 . . ?
C14A N2A C14A 103.9(5) 6_565 . ?
C14A N2A Ni1A 128.0(3) 6_565 . ?
C14A N2A Ni1A 128.0(2) . . ?
C4A N4A C4A 103.7(4) 6_565 . ?
C4A N4A Ni1A 128.1(2) 6_565 . ?
C4A N4A Ni1A 128.1(2) . . ?
C13A C1A N1A 124.6(2) . . ?
C13A C1A C10A 124.4(3) . . ?
N1A C1A C10A 110.9(2) . . ?
C13A C1A C2A 162.5(2) . . ?
N1A C1A C2A 37.9 . . ?
C10A C1A C2A 73.1(2) . . ?
C3A C2A N1A 124.5 . . ?
C3A C2A C7A 124.4(2) . . ?
N1A C2A C7A 111.1(2) . . ?
C3A C2A C1A 162.4 . . ?
N1A C2A C1A 37.9 . . ?
C7A C2A C1A 73.1(2) . . ?
C4A C3A C2A 124.6(2) . . ?
C4A C3A H3A 117.7 . . ?
C2A C3A H3A 117.7 . . ?
C3A C4A N4A 124.8(4) . . ?
C3A C4A C5A 123.8(4) . . ?
N4A C4A C5A 111.4(4) . . ?
C3A C4A C4A 162.9(2) . 6_565 ?
N4A C4A C4A 38.1(2) . 6_565 ?
C5A C4A C4A 73.2(3) . 6_565 ?
C5A C5A C4A 106.8(3) 6_565 . ?
C5A C5A C6A 128.7(3) 6_565 . ?
C4A C5A C6A 124.4(5) . . ?
C5A C6A C18A 110.9(5) . . ?
C5A C6A H6A1 109.5 . . ?
C18A C6A H6A1 109.5 . . ?
C5A C6A H6A2 109.5 . . ?
C18A C6A H6A2 109.5 . . ?
H6A1 C6A H6A2 108.0 . . ?
C10A C7A C2A 106.8(4) . . ?
C10A C7A C8A 129.9(5) . . ?
C2A C7A C8A 123.3(5) . . ?
C7A C8A C9A 112.0(5) . . ?
C7A C8A H8A1 109.2 . . ?
C9A C8A H8A1 109.2 . . ?
C7A C8A H8A2 109.2 . . ?
C9A C8A H8A2 109.2 . . ?
H8A1 C8A H8A2 107.9 . . ?
C8A C9A H9A1 109.5 . . ?
C8A C9A H9A2 109.5 . . ?
H9A1 C9A H9A2 109.5 . . ?
C8A C9A H9A3 109.5 . . ?
H9A1 C9A H9A3 109.5 . . ?
H9A2 C9A H9A3 109.5 . . ?
C7A C10A C1A 107.0(4) . . ?
C7A C10A C11A 129.3(5) . . ?
C1A C10A C11A 123.5(5) . . ?
C12A C11A C10A 112.7(5) . . ?
C12A C11A H11A 109.1 . . ?
C10A C11A H11A 109.1 . . ?
C12A C11A H11B 109.1 . . ?
C10A C11A H11B 109.1 . . ?
H11A C11A H11B 107.8 . . ?
C11A C12A H12A 109.5 . . ?
C11A C12A H12B 109.5 . . ?
H12A C12A H12B 109.5 . . ?
C11A C12A H12C 109.5 . . ?
H12A C12A H12C 109.5 . . ?
H12B C12A H12C 109.5 . . ?
C14A C13A C1A 124.8(4) . . ?
C14A C13A H13A 117.6 . . ?
C1A C13A H13A 117.6 . . ?
C13A C14A N2A 124.7(5) . . ?
C13A C14A C15A 123.8(5) . . ?
N2A C14A C15A 111.4(4) . . ?
C13A C14A C14A 162.7(3) . 6_565 ?
N2A C14A C14A 38.0(2) . 6_565 ?
C15A C14A C14A 73.4(3) . 6_565 ?
C15A C15A C14A 106.6(3) 6_565 . ?
C15A C15A C16A 129.1(3) 6_565 . ?
C14A C15A C16A 124.2(5) . . ?
C15A C16A C17A 112.7(5) . . ?
C15A C16A H16A 109.1 . . ?
C17A C16A H16A 109.1 . . ?
C15A C16A H16B 109.1 . . ?
C17A C16A H16B 109.1 . . ?
H16A C16A H16B 107.8 . . ?
C16A C17A H17A 109.5 . . ?
C16A C17A H17B 109.5 . . ?
H17A C17A H17B 109.5 . . ?
C16A C17A H17C 109.5 . . ?
H17A C17A H17C 109.5 . . ?
H17B C17A H17C 109.5 . . ?
C6A C18A H18A 114.7 . . ?
C6A C18A H18B 110.0 . . ?
H18A C18A H18B 108.7 . . ?
C6A C18A H18C 107.4 . . ?
H18A C18A H18C 107.7 . . ?
H18B C18A H18C 108.0 . . ?
C6B C1B C2B 120.6(10) . . ?
C6B C1B H1B 119.7 . . ?
C2B C1B H1B 119.7 . . ?
C3B C2B C1B 119.7(11) . . ?
C3B C2B H2B 120.2 . . ?
C1B C2B H2B 120.2 . . ?
C2B C3B C4B 119.9(12) . . ?
C2B C3B H3B 120.0 . . ?
C4B C3B H3B 120.0 . . ?
C5B C4B C3B 120.5(12) . . ?
C5B C4B H4B 119.7 . . ?
C3B C4B H4B 119.7 . . ?
C4B C5B C6B 119.9(9) . . ?
C4B C5B H5B 120.0 . . ?
C6B C5B H5B 120.0 . . ?
C1B C6B C5B 119.4(9) . . ?
C1B C6B H6B 120.3 . . ?
C5B C6B H6B 120.3 . . ?
C8B C7B C9B 112.6(8) . . ?
C8B C7B H7B 123.7 . . ?
C9B C7B H7B 123.7 . . ?
C9B C8B C7B 122.7(11) 2_656 . ?
C9B C8B H8B 118.6 2_656 . ?
C7B C8B H8B 118.6 . . ?
C8B C9B C7B 124.2(10) 2_656 . ?
C8B C9B H9B 117.9 2_656 . ?
C7B C9B H9B 117.9 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Lu10 Lu1 Lu2 Lu5 10.0(5) 6_565 . . 6_565 ?
Lu8 Lu1 Lu2 Lu5 138.9(3) 6_565 . . 6_565 ?
C18 Lu1 Lu2 Lu5 -83.8(4) . . . 6_565 ?
C19 Lu1 Lu2 Lu5 -127.1(4) . . . 6_565 ?
C1 Lu1 Lu2 Lu5 -77.8(3) . . . 6_565 ?
Lu9 Lu1 Lu2 Lu5 118.7(8) 6_565 . . 6_565 ?
Lu3 Lu1 Lu2 Lu5 12.2(3) 6_565 . . 6_565 ?
C20 Lu1 Lu2 Lu5 -145.9(3) . . . 6_565 ?
C17 Lu1 Lu2 Lu5 -45.2(4) . . . 6_565 ?
C5 Lu1 Lu2 Lu5 -103.0(2) . . . 6_565 ?
Lu5 Lu1 Lu2 Lu10 -10.0(5) 6_565 . . 6_565 ?
Lu8 Lu1 Lu2 Lu10 128.9(5) 6_565 . . 6_565 ?
C18 Lu1 Lu2 Lu10 -93.8(5) . . . 6_565 ?
C19 Lu1 Lu2 Lu10 -137.1(5) . . . 6_565 ?
C1 Lu1 Lu2 Lu10 -87.8(4) . . . 6_565 ?
Lu9 Lu1 Lu2 Lu10 108.7(9) 6_565 . . 6_565 ?
Lu3 Lu1 Lu2 Lu10 2.2(5) 6_565 . . 6_565 ?
C20 Lu1 Lu2 Lu10 -155.9(4) . . . 6_565 ?
C17 Lu1 Lu2 Lu10 -55.2(5) . . . 6_565 ?
C5 Lu1 Lu2 Lu10 -113.0(4) . . . 6_565 ?
Lu5 Lu1 Lu2 Lu3 -12.2(3) 6_565 . . 6_565 ?
Lu10 Lu1 Lu2 Lu3 -2.2(5) 6_565 . . 6_565 ?
Lu8 Lu1 Lu2 Lu3 126.7(3) 6_565 . . 6_565 ?
C18 Lu1 Lu2 Lu3 -96.0(3) . . . 6_565 ?
C19 Lu1 Lu2 Lu3 -139.3(3) . . . 6_565 ?
C1 Lu1 Lu2 Lu3 -89.9(2) . . . 6_565 ?
Lu9 Lu1 Lu2 Lu3 106.5(8) 6_565 . . 6_565 ?
C20 Lu1 Lu2 Lu3 -158.1(2) . . . 6_565 ?
C17 Lu1 Lu2 Lu3 -57.4(3) . . . 6_565 ?
C5 Lu1 Lu2 Lu3 -115.2(2) . . . 6_565 ?
Lu5 Lu1 Lu2 Lu8 -138.9(3) 6_565 . . 6_565 ?
Lu10 Lu1 Lu2 Lu8 -128.9(5) 6_565 . . 6_565 ?
C18 Lu1 Lu2 Lu8 137.3(3) . . . 6_565 ?
C19 Lu1 Lu2 Lu8 94.0(3) . . . 6_565 ?
C1 Lu1 Lu2 Lu8 143.4(2) . . . 6_565 ?
Lu9 Lu1 Lu2 Lu8 -20.1(8) 6_565 . . 6_565 ?
Lu3 Lu1 Lu2 Lu8 -126.7(3) 6_565 . . 6_565 ?
C20 Lu1 Lu2 Lu8 75.3(2) . . . 6_565 ?
C17 Lu1 Lu2 Lu8 175.9(3) . . . 6_565 ?
C5 Lu1 Lu2 Lu8 118.1(2) . . . 6_565 ?
Lu5 Lu1 Lu2 C5 103.0(2) 6_565 . . . ?
Lu10 Lu1 Lu2 C5 113.0(4) 6_565 . . . ?
Lu8 Lu1 Lu2 C5 -118.1(2) 6_565 . . . ?
C18 Lu1 Lu2 C5 19.2(2) . . . . ?
C19 Lu1 Lu2 C5 -24.1(3) . . . . ?
C1 Lu1 Lu2 C5 25.25(9) . . . . ?
Lu9 Lu1 Lu2 C5 -138.3(8) 6_565 . . . ?
Lu3 Lu1 Lu2 C5 115.2(2) 6_565 . . . ?
C20 Lu1 Lu2 C5 -42.89(12) . . . . ?
C17 Lu1 Lu2 C5 57.8(3) . . . . ?
Lu5 Lu1 Lu2 C4 86.5(3) 6_565 . . . ?
Lu10 Lu1 Lu2 C4 96.5(5) 6_565 . . . ?
Lu8 Lu1 Lu2 C4 -134.6(2) 6_565 . . . ?
C18 Lu1 Lu2 C4 2.7(4) . . . . ?
C19 Lu1 Lu2 C4 -40.6(4) . . . . ?
C1 Lu1 Lu2 C4 8.8(2) . . . . ?
Lu9 Lu1 Lu2 C4 -154.7(7) 6_565 . . . ?
Lu3 Lu1 Lu2 C4 98.7(3) 6_565 . . . ?
C20 Lu1 Lu2 C4 -59.4(3) . . . . ?
C17 Lu1 Lu2 C4 41.3(4) . . . . ?
C5 Lu1 Lu2 C4 -16.48(14) . . . . ?
Lu5 Lu1 Lu2 Lu6 -30.7(3) 6_565 . . . ?
Lu10 Lu1 Lu2 Lu6 -20.7(4) 6_565 . . . ?
Lu8 Lu1 Lu2 Lu6 108.2(3) 6_565 . . . ?
C18 Lu1 Lu2 Lu6 -114.5(2) . . . . ?
C19 Lu1 Lu2 Lu6 -157.8(2) . . . . ?
C1 Lu1 Lu2 Lu6 -108.45(18) . . . . ?
Lu9 Lu1 Lu2 Lu6 88.0(8) 6_565 . . . ?
Lu3 Lu1 Lu2 Lu6 -18.5(2) 6_565 . . . ?
C20 Lu1 Lu2 Lu6 -176.58(16) . . . . ?
C17 Lu1 Lu2 Lu6 -75.9(3) . . . . ?
C5 Lu1 Lu2 Lu6 -133.7(2) . . . . ?
Lu5 Lu1 Lu2 C6 135.4(2) 6_565 . . . ?
Lu10 Lu1 Lu2 C6 145.4(4) 6_565 . . . ?
Lu8 Lu1 Lu2 C6 -85.70(19) 6_565 . . . ?
C18 Lu1 Lu2 C6 51.6(2) . . . . ?
C19 Lu1 Lu2 C6 8.3(2) . . . . ?
C1 Lu1 Lu2 C6 57.69(8) . . . . ?
Lu9 Lu1 Lu2 C6 -105.8(8) 6_565 . . . ?
Lu3 Lu1 Lu2 C6 147.6(2) 6_565 . . . ?
C20 Lu1 Lu2 C6 -10.45(8) . . . . ?
C17 Lu1 Lu2 C6 90.2(3) . . . . ?
C5 Lu1 Lu2 C6 32.44(4) . . . . ?
Lu5 Lu1 Lu2 C1 77.8(3) 6_565 . . . ?
Lu10 Lu1 Lu2 C1 87.8(4) 6_565 . . . ?
Lu8 Lu1 Lu2 C1 -143.4(2) 6_565 . . . ?
C18 Lu1 Lu2 C1 -6.09(15) . . . . ?
C19 Lu1 Lu2 C1 -49.4(2) . . . . ?
Lu9 Lu1 Lu2 C1 -163.5(8) 6_565 . . . ?
Lu3 Lu1 Lu2 C1 89.9(2) 6_565 . . . ?
C20 Lu1 Lu2 C1 -68.14(8) . . . . ?
C17 Lu1 Lu2 C1 32.5(2) . . . . ?
C5 Lu1 Lu2 C1 -25.25(9) . . . . ?
Lu5 Lu1 Lu2 C9 124.2(4) 6_565 . . . ?
Lu10 Lu1 Lu2 C9 134.2(6) 6_565 . . . ?
Lu8 Lu1 Lu2 C9 -96.9(4) 6_565 . . . ?
C18 Lu1 Lu2 C9 40.4(6) . . . . ?
C19 Lu1 Lu2 C9 -2.9(6) . . . . ?
C1 Lu1 Lu2 C9 46.4(4) . . . . ?
Lu9 Lu1 Lu2 C9 -117.1(8) 6_565 . . . ?
Lu3 Lu1 Lu2 C9 136.4(4) 6_565 . . . ?
C20 Lu1 Lu2 C9 -21.7(4) . . . . ?
C17 Lu1 Lu2 C9 79.0(6) . . . . ?
C5 Lu1 Lu2 C9 21.2(3) . . . . ?
Lu5 Lu1 Lu2 C3 47.6(2) 6_565 . . . ?
Lu10 Lu1 Lu2 C3 57.6(4) 6_565 . . . ?
Lu8 Lu1 Lu2 C3 -173.6(2) 6_565 . . . ?
C18 Lu1 Lu2 C3 -36.3(3) . . . . ?
C19 Lu1 Lu2 C3 -79.6(3) . . . . ?
C1 Lu1 Lu2 C3 -30.20(15) . . . . ?
Lu9 Lu1 Lu2 C3 166.3(7) 6_565 . . . ?
Lu3 Lu1 Lu2 C3 59.7(2) 6_565 . . . ?
C20 Lu1 Lu2 C3 -98.33(18) . . . . ?
C17 Lu1 Lu2 C3 2.3(3) . . . . ?
C5 Lu1 Lu2 C3 -55.45(9) . . . . ?
Lu6 Lu3 Lu5 Lu10 -46(8) . . . . ?
Lu11 Lu3 Lu5 Lu10 -89(8) . . . . ?
Lu3 Lu3 Lu5 Lu10 -38(8) 6_565 . . . ?
C30 Lu3 Lu5 Lu10 161(8) . . . . ?
Lu2 Lu3 Lu5 Lu10 33(8) 6_565 . . . ?
C29 Lu3 Lu5 Lu10 106(8) . . . . ?
C51 Lu3 Lu5 Lu10 173(8) . . . . ?
Lu10 Lu3 Lu5 Lu10 -37(8) 6_565 . . . ?
C31 Lu3 Lu5 Lu10 -150(9) . . . . ?
C28 Lu3 Lu5 Lu10 93(8) . . . . ?
Lu10 Lu3 Lu5 Lu1 -18(8) . . . 6_565 ?
Lu6 Lu3 Lu5 Lu1 -64.6(12) . . . 6_565 ?
Lu11 Lu3 Lu5 Lu1 -107.0(11) . . . 6_565 ?
Lu3 Lu3 Lu5 Lu1 -56.3(6) 6_565 . . 6_565 ?
C30 Lu3 Lu5 Lu1 142.8(4) . . . 6_565 ?
Lu2 Lu3 Lu5 Lu1 14.6(4) 6_565 . . 6_565 ?
C29 Lu3 Lu5 Lu1 87.5(5) . . . 6_565 ?
C51 Lu3 Lu5 Lu1 154.3(5) . . . 6_565 ?
Lu10 Lu3 Lu5 Lu1 -55.1(6) 6_565 . . 6_565 ?
C31 Lu3 Lu5 Lu1 -168.4(4) . . . 6_565 ?
C28 Lu3 Lu5 Lu1 75.1(5) . . . 6_565 ?
Lu10 Lu3 Lu5 Lu2 -33(8) . . . 6_565 ?
Lu6 Lu3 Lu5 Lu2 -79.2(11) . . . 6_565 ?
Lu11 Lu3 Lu5 Lu2 -121.6(10) . . . 6_565 ?
Lu3 Lu3 Lu5 Lu2 -70.9(3) 6_565 . . 6_565 ?
C30 Lu3 Lu5 Lu2 128.2(3) . . . 6_565 ?
C29 Lu3 Lu5 Lu2 72.9(4) . . . 6_565 ?
C51 Lu3 Lu5 Lu2 139.7(2) . . . 6_565 ?
Lu10 Lu3 Lu5 Lu2 -69.7(4) 6_565 . . 6_565 ?
C31 Lu3 Lu5 Lu2 177.1(5) . . . 6_565 ?
C28 Lu3 Lu5 Lu2 60.49(19) . . . 6_565 ?
Lu10 Lu3 Lu5 C50 -146(8) . . . . ?
Lu6 Lu3 Lu5 C50 167.5(10) . . . . ?
Lu11 Lu3 Lu5 C50 125.1(10) . . . . ?
Lu3 Lu3 Lu5 C50 175.75(13) 6_565 . . . ?
C30 Lu3 Lu5 C50 14.9(4) . . . . ?
Lu2 Lu3 Lu5 C50 -113.3(3) 6_565 . . . ?
C29 Lu3 Lu5 C50 -40.5(4) . . . . ?
C51 Lu3 Lu5 C50 26.38(17) . . . . ?
Lu10 Lu3 Lu5 C50 177.0(4) 6_565 . . . ?
C31 Lu3 Lu5 C50 63.7(5) . . . . ?
C28 Lu3 Lu5 C50 -52.8(2) . . . . ?
Lu10 Lu3 Lu5 C68 -150(8) . . . . ?
Lu6 Lu3 Lu5 C68 163.9(9) . . . . ?
Lu11 Lu3 Lu5 C68 121.5(10) . . . . ?
Lu3 Lu3 Lu5 C68 172.2(2) 6_565 . . . ?
C30 Lu3 Lu5 C68 11.3(6) . . . . ?
Lu2 Lu3 Lu5 C68 -116.9(5) 6_565 . . . ?
C29 Lu3 Lu5 C68 -44.0(6) . . . . ?
C51 Lu3 Lu5 C68 22.8(4) . . . . ?
Lu10 Lu3 Lu5 C68 173.4(4) 6_565 . . . ?
C31 Lu3 Lu5 C68 60.1(7) . . . . ?
C28 Lu3 Lu5 C68 -56.4(4) . . . . ?
Lu10 Lu3 Lu5 Lu6 46(8) . . . . ?
Lu11 Lu3 Lu5 Lu6 -42.4(13) . . . . ?
Lu3 Lu3 Lu5 Lu6 8.3(9) 6_565 . . . ?
C30 Lu3 Lu5 Lu6 -152.6(13) . . . . ?
Lu2 Lu3 Lu5 Lu6 79.2(11) 6_565 . . . ?
C29 Lu3 Lu5 Lu6 152.1(13) . . . . ?
C51 Lu3 Lu5 Lu6 -141.1(11) . . . . ?
Lu10 Lu3 Lu5 Lu6 9.5(10) 6_565 . . . ?
C31 Lu3 Lu5 Lu6 -103.8(12) . . . . ?
C28 Lu3 Lu5 Lu6 139.7(11) . . . . ?
Lu10 Lu3 Lu5 Lu11 89(8) . . . . ?
Lu6 Lu3 Lu5 Lu11 42.4(13) . . . . ?
Lu3 Lu3 Lu5 Lu11 50.6(10) 6_565 . . . ?
C30 Lu3 Lu5 Lu11 -110.2(11) . . . . ?
Lu2 Lu3 Lu5 Lu11 121.6(10) 6_565 . . . ?
C29 Lu3 Lu5 Lu11 -165.6(11) . . . . ?
C51 Lu3 Lu5 Lu11 -98.7(10) . . . . ?
Lu10 Lu3 Lu5 Lu11 51.9(10) 6_565 . . . ?
C31 Lu3 Lu5 Lu11 -61.4(11) . . . . ?
C28 Lu3 Lu5 Lu11 -177.9(10) . . . . ?
Lu10 Lu3 Lu5 C49 -109(8) . . . . ?
Lu6 Lu3 Lu5 C49 -155.2(11) . . . . ?
Lu11 Lu3 Lu5 C49 162.4(10) . . . . ?
Lu3 Lu3 Lu5 C49 -146.94(16) 6_565 . . . ?
C30 Lu3 Lu5 C49 52.2(3) . . . . ?
Lu2 Lu3 Lu5 C49 -76.02(19) 6_565 . . . ?
C29 Lu3 Lu5 C49 -3.1(3) . . . . ?
C51 Lu3 Lu5 C49 63.69(15) . . . . ?
Lu10 Lu3 Lu5 C49 -145.7(4) 6_565 . . . ?
C31 Lu3 Lu5 C49 101.0(5) . . . . ?
C28 Lu3 Lu5 C49 -15.52(14) . . . . ?
Lu10 Lu3 Lu5 C51 -173(8) . . . . ?
Lu6 Lu3 Lu5 C51 141.1(11) . . . . ?
Lu11 Lu3 Lu5 C51 98.7(10) . . . . ?
Lu3 Lu3 Lu5 C51 149.4(3) 6_565 . . . ?
C30 Lu3 Lu5 C51 -11.5(2) . . . . ?
Lu2 Lu3 Lu5 C51 -139.7(2) 6_565 . . . ?
C29 Lu3 Lu5 C51 -66.8(3) . . . . ?
Lu10 Lu3 Lu5 C51 150.6(4) 6_565 . . . ?
C31 Lu3 Lu5 C51 37.4(4) . . . . ?
C28 Lu3 Lu5 C51 -79.21(17) . . . . ?
Lu10 Lu3 Lu5 C67 -95(8) . . . . ?
Lu6 Lu3 Lu5 C67 -141.6(10) . . . . ?
Lu11 Lu3 Lu5 C67 176.0(10) . . . . ?
Lu3 Lu3 Lu5 C67 -133.3(3) 6_565 . . . ?
C30 Lu3 Lu5 C67 65.8(6) . . . . ?
Lu2 Lu3 Lu5 C67 -62.4(4) 6_565 . . . ?
C29 Lu3 Lu5 C67 10.4(7) . . . . ?
C51 Lu3 Lu5 C67 77.3(4) . . . . ?
Lu10 Lu3 Lu5 C67 -132.1(5) 6_565 . . . ?
C31 Lu3 Lu5 C67 114.6(6) . . . . ?
C28 Lu3 Lu5 C67 -1.9(5) . . . . ?
Lu10 Lu3 Lu5 C69 146(8) . . . . ?
Lu6 Lu3 Lu5 C69 100.0(11) . . . . ?
Lu11 Lu3 Lu5 C69 57.6(10) . . . . ?
Lu3 Lu3 Lu5 C69 108.3(3) 6_565 . . . ?
C30 Lu3 Lu5 C69 -52.6(5) . . . . ?
Lu2 Lu3 Lu5 C69 179.2(4) 6_565 . . . ?
C29 Lu3 Lu5 C69 -107.9(4) . . . . ?
C51 Lu3 Lu5 C69 -41.1(3) . . . . ?
Lu10 Lu3 Lu5 C69 109.5(4) 6_565 . . . ?
C31 Lu3 Lu5 C69 -3.7(7) . . . . ?
C28 Lu3 Lu5 C69 -120.3(3) . . . . ?
Lu10 Lu3 Lu6 Lu3 38(5) . . . 6_565 ?
Lu11 Lu3 Lu6 Lu3 99(4) . . . 6_565 ?
Lu5 Lu3 Lu6 Lu3 43(4) . . . 6_565 ?
C30 Lu3 Lu6 Lu3 -161(4) . . . 6_565 ?
Lu2 Lu3 Lu6 Lu3 -2(4) 6_565 . . 6_565 ?
C29 Lu3 Lu6 Lu3 -115(4) . . . 6_565 ?
C51 Lu3 Lu6 Lu3 166(3) . . . 6_565 ?
Lu10 Lu3 Lu6 Lu3 22(3) 6_565 . . 6_565 ?
C31 Lu3 Lu6 Lu3 -179(100) . . . 6_565 ?
C28 Lu3 Lu6 Lu3 -87(4) . . . 6_565 ?
Lu10 Lu3 Lu6 Lu11 -62(2) . . . . ?
Lu5 Lu3 Lu6 Lu11 -56.8(18) . . . . ?
Lu3 Lu3 Lu6 Lu11 -99(4) 6_565 . . . ?
C30 Lu3 Lu6 Lu11 99.6(16) . . . . ?
Lu2 Lu3 Lu6 Lu11 -101.2(16) 6_565 . . . ?
C29 Lu3 Lu6 Lu11 145.8(15) . . . . ?
C51 Lu3 Lu6 Lu11 66.6(18) . . . . ?
Lu10 Lu3 Lu6 Lu11 -77.3(19) 6_565 . . . ?
C31 Lu3 Lu6 Lu11 81.8(15) . . . . ?
C28 Lu3 Lu6 Lu11 173.1(15) . . . . ?
Lu10 Lu3 Lu6 Lu10 16(2) . . . 6_565 ?
Lu11 Lu3 Lu6 Lu10 77.3(19) . . . 6_565 ?
Lu5 Lu3 Lu6 Lu10 21(2) . . . 6_565 ?
Lu3 Lu3 Lu6 Lu10 -22(3) 6_565 . . 6_565 ?
C30 Lu3 Lu6 Lu10 176.9(11) . . . 6_565 ?
Lu2 Lu3 Lu6 Lu10 -23.9(16) 6_565 . . 6_565 ?
C29 Lu3 Lu6 Lu10 -136.9(12) . . . 6_565 ?
C51 Lu3 Lu6 Lu10 143.9(10) . . . 6_565 ?
C31 Lu3 Lu6 Lu10 159.1(15) . . . 6_565 ?
C28 Lu3 Lu6 Lu10 -109.6(12) . . . 6_565 ?
Lu11 Lu3 Lu6 Lu10 62(2) . . . . ?
Lu5 Lu3 Lu6 Lu10 4.9(10) . . . . ?
Lu3 Lu3 Lu6 Lu10 -38(5) 6_565 . . . ?
C30 Lu3 Lu6 Lu10 161.3(15) . . . . ?
Lu2 Lu3 Lu6 Lu10 -39.5(11) 6_565 . . . ?
C29 Lu3 Lu6 Lu10 -152.5(15) . . . . ?
C51 Lu3 Lu6 Lu10 128.3(18) . . . . ?
Lu10 Lu3 Lu6 Lu10 -16(2) 6_565 . . . ?
C31 Lu3 Lu6 Lu10 143.5(12) . . . . ?
C28 Lu3 Lu6 Lu10 -125.2(16) . . . . ?
Lu10 Lu3 Lu6 C31 -143.5(13) . . . . ?
Lu11 Lu3 Lu6 C31 -81.8(15) . . . . ?
Lu5 Lu3 Lu6 C31 -138.6(8) . . . . ?
Lu3 Lu3 Lu6 C31 179(100) 6_565 . . . ?
C30 Lu3 Lu6 C31 17.8(5) . . . . ?
Lu2 Lu3 Lu6 C31 177.0(3) 6_565 . . . ?
C29 Lu3 Lu6 C31 64.0(4) . . . . ?
C51 Lu3 Lu6 C31 -15.2(9) . . . . ?
Lu10 Lu3 Lu6 C31 -159.1(15) 6_565 . . . ?
C28 Lu3 Lu6 C31 91.3(6) . . . . ?
Lu10 Lu3 Lu6 C13 -159.6(11) . . . . ?
Lu11 Lu3 Lu6 C13 -97.9(18) . . . . ?
Lu5 Lu3 Lu6 C13 -154.7(5) . . . . ?
Lu3 Lu3 Lu6 C13 163(5) 6_565 . . . ?
C30 Lu3 Lu6 C13 1.7(11) . . . . ?
Lu2 Lu3 Lu6 C13 160.9(5) 6_565 . . . ?
C29 Lu3 Lu6 C13 47.9(10) . . . . ?
C51 Lu3 Lu6 C13 -31.3(15) . . . . ?
Lu10 Lu3 Lu6 C13 -175(2) 6_565 . . . ?
C31 Lu3 Lu6 C13 -16.1(7) . . . . ?
C28 Lu3 Lu6 C13 75.2(11) . . . . ?
Lu10 Lu3 Lu6 C30 -161.3(15) . . . . ?
Lu11 Lu3 Lu6 C30 -99.6(16) . . . . ?
Lu5 Lu3 Lu6 C30 -156.3(11) . . . . ?
Lu3 Lu3 Lu6 C30 161(4) 6_565 . . . ?
Lu2 Lu3 Lu6 C30 159.2(7) 6_565 . . . ?
C29 Lu3 Lu6 C30 46.26(18) . . . . ?
C51 Lu3 Lu6 C30 -33.0(5) . . . . ?
Lu10 Lu3 Lu6 C30 -176.9(11) 6_565 . . . ?
C31 Lu3 Lu6 C30 -17.8(5) . . . . ?
C28 Lu3 Lu6 C30 73.5(5) . . . . ?
Lu10 Lu3 Lu6 C12 143.4(12) . . . . ?
Lu11 Lu3 Lu6 C12 -154.8(19) . . . . ?
Lu5 Lu3 Lu6 C12 148.4(6) . . . . ?
Lu3 Lu3 Lu6 C12 106(4) 6_565 . . . ?
C30 Lu3 Lu6 C12 -55.3(10) . . . . ?
Lu2 Lu3 Lu6 C12 103.9(9) 6_565 . . . ?
C29 Lu3 Lu6 C12 -9.0(10) . . . . ?
C51 Lu3 Lu6 C12 -88.2(11) . . . . ?
Lu10 Lu3 Lu6 C12 127.8(19) 6_565 . . . ?
C31 Lu3 Lu6 C12 -73.1(8) . . . . ?
C28 Lu3 Lu6 C12 18.3(13) . . . . ?
Lu10 Lu3 Lu6 C29 152.5(15) . . . . ?
Lu11 Lu3 Lu6 C29 -145.8(15) . . . . ?
Lu5 Lu3 Lu6 C29 157.4(10) . . . . ?
Lu3 Lu3 Lu6 C29 115(4) 6_565 . . . ?
C30 Lu3 Lu6 C29 -46.26(18) . . . . ?
Lu2 Lu3 Lu6 C29 112.9(6) 6_565 . . . ?
C51 Lu3 Lu6 C29 -79.2(7) . . . . ?
Lu10 Lu3 Lu6 C29 136.9(12) 6_565 . . . ?
C31 Lu3 Lu6 C29 -64.0(4) . . . . ?
C28 Lu3 Lu6 C29 27.3(4) . . . . ?
Lu10 Lu3 Lu6 C11 134.0(13) . . . . ?
Lu11 Lu3 Lu6 C11 -164.3(16) . . . . ?
Lu5 Lu3 Lu6 C11 138.9(8) . . . . ?
Lu3 Lu3 Lu6 C11 96(4) 6_565 . . . ?
C30 Lu3 Lu6 C11 -64.8(4) . . . . ?
Lu2 Lu3 Lu6 C11 94.4(5) 6_565 . . . ?
C29 Lu3 Lu6 C11 -18.5(4) . . . . ?
C51 Lu3 Lu6 C11 -97.7(7) . . . . ?
Lu10 Lu3 Lu6 C11 118.4(14) 6_565 . . . ?
C31 Lu3 Lu6 C11 -82.6(4) . . . . ?
C28 Lu3 Lu6 C11 8.8(7) . . . . ?
Lu10 Lu3 Lu6 Lu5 10(2) . . . 6_565 ?
Lu11 Lu3 Lu6 Lu5 71.3(17) . . . 6_565 ?
Lu5 Lu3 Lu6 Lu5 14.5(16) . . . 6_565 ?
Lu3 Lu3 Lu6 Lu5 -28(3) 6_565 . . 6_565 ?
C30 Lu3 Lu6 Lu5 170.8(6) . . . 6_565 ?
Lu2 Lu3 Lu6 Lu5 -29.9(13) 6_565 . . 6_565 ?
C29 Lu3 Lu6 Lu5 -142.9(7) . . . 6_565 ?
C51 Lu3 Lu6 Lu5 137.9(6) . . . 6_565 ?
Lu10 Lu3 Lu6 Lu5 -6.0(7) 6_565 . . 6_565 ?
C31 Lu3 Lu6 Lu5 153.1(11) . . . 6_565 ?
C28 Lu3 Lu6 Lu5 -115.6(8) . . . 6_565 ?
Lu4 Lu7 Lu8 Lu8 34(5) 6_565 . . 6_565 ?
Lu9 Lu7 Lu8 Lu8 146(2) . . . 6_565 ?
Lu9 Lu7 Lu8 Lu8 42(3) 6_565 . . 6_565 ?
C42 Lu7 Lu8 Lu8 -86.5(9) . . . 6_565 ?
C62 Lu7 Lu8 Lu8 -135(2) . . . 6_565 ?
C43 Lu7 Lu8 Lu8 -96.8(8) . . . 6_565 ?
C41 Lu7 Lu8 Lu8 -47.1(4) . . . 6_565 ?
C61 Lu7 Lu8 Lu8 -175(6) . . . 6_565 ?
C63 Lu7 Lu8 Lu8 -152.6(15) . . . 6_565 ?
C44 Lu7 Lu8 Lu8 -134.8(7) . . . 6_565 ?
Lu4 Lu7 Lu8 Lu4 -122(9) 6_565 . . . ?
Lu9 Lu7 Lu8 Lu4 -11(2) . . . . ?
Lu9 Lu7 Lu8 Lu4 -114(6) 6_565 . . . ?
Lu8 Lu7 Lu8 Lu4 -157(4) 6_565 . . . ?
C42 Lu7 Lu8 Lu4 117(3) . . . . ?
C62 Lu7 Lu8 Lu4 68.6(17) . . . . ?
C43 Lu7 Lu8 Lu4 107(3) . . . . ?
C41 Lu7 Lu8 Lu4 156(4) . . . . ?
C61 Lu7 Lu8 Lu4 28(3) . . . . ?
C63 Lu7 Lu8 Lu4 51(2) . . . . ?
C44 Lu7 Lu8 Lu4 69(3) . . . . ?
Lu4 Lu7 Lu8 Lu9 -112(7) 6_565 . . . ?
Lu9 Lu7 Lu8 Lu9 -104(5) 6_565 . . . ?
Lu8 Lu7 Lu8 Lu9 -146(2) 6_565 . . . ?
C42 Lu7 Lu8 Lu9 127(2) . . . . ?
C62 Lu7 Lu8 Lu9 79.3(17) . . . . ?
C43 Lu7 Lu8 Lu9 117.1(19) . . . . ?
C41 Lu7 Lu8 Lu9 167(3) . . . . ?
C61 Lu7 Lu8 Lu9 39(4) . . . . ?
C63 Lu7 Lu8 Lu9 61.3(16) . . . . ?
C44 Lu7 Lu8 Lu9 79.2(19) . . . . ?
Lu9 Lu7 Lu8 Lu4 112(7) . . . 6_565 ?
Lu9 Lu7 Lu8 Lu4 8(4) 6_565 . . 6_565 ?
Lu8 Lu7 Lu8 Lu4 -34(5) 6_565 . . 6_565 ?
C42 Lu7 Lu8 Lu4 -121(6) . . . 6_565 ?
C62 Lu7 Lu8 Lu4 -169(8) . . . 6_565 ?
C43 Lu7 Lu8 Lu4 -131(6) . . . 6_565 ?
C41 Lu7 Lu8 Lu4 -81(5) . . . 6_565 ?
C61 Lu7 Lu8 Lu4 151(11) . . . 6_565 ?
C63 Lu7 Lu8 Lu4 173(7) . . . 6_565 ?
C44 Lu7 Lu8 Lu4 -169(6) . . . 6_565 ?
Lu4 Lu7 Lu8 Lu1 -90(6) 6_565 . . 6_565 ?
Lu9 Lu7 Lu8 Lu1 22(2) . . . 6_565 ?
Lu9 Lu7 Lu8 Lu1 -82(3) 6_565 . . 6_565 ?
Lu8 Lu7 Lu8 Lu1 -124.5(5) 6_565 . . 6_565 ?
C42 Lu7 Lu8 Lu1 149.0(6) . . . 6_565 ?
C62 Lu7 Lu8 Lu1 101(2) . . . 6_565 ?
C43 Lu7 Lu8 Lu1 138.7(6) . . . 6_565 ?
C41 Lu7 Lu8 Lu1 -171.6(6) . . . 6_565 ?
C61 Lu7 Lu8 Lu1 61(6) . . . 6_565 ?
C63 Lu7 Lu8 Lu1 82.9(12) . . . 6_565 ?
C44 Lu7 Lu8 Lu1 100.7(6) . . . 6_565 ?
Lu4 Lu7 Lu8 Lu9 -8(4) 6_565 . . 6_565 ?
Lu9 Lu7 Lu8 Lu9 104(5) . . . 6_565 ?
Lu8 Lu7 Lu8 Lu9 -42(3) 6_565 . . 6_565 ?
C42 Lu7 Lu8 Lu9 -129(4) . . . 6_565 ?
C62 Lu7 Lu8 Lu9 -177(5) . . . 6_565 ?
C43 Lu7 Lu8 Lu9 -139(3) . . . 6_565 ?
C41 Lu7 Lu8 Lu9 -89(3) . . . 6_565 ?
C61 Lu7 Lu8 Lu9 143(8) . . . 6_565 ?
C63 Lu7 Lu8 Lu9 165(4) . . . 6_565 ?
C44 Lu7 Lu8 Lu9 -177(3) . . . 6_565 ?
Lu4 Lu7 Lu8 Lu2 -60(6) 6_565 . . 6_565 ?
Lu9 Lu7 Lu8 Lu2 52(2) . . . 6_565 ?
Lu9 Lu7 Lu8 Lu2 -52(4) 6_565 . . 6_565 ?
Lu8 Lu7 Lu8 Lu2 -94.2(10) 6_565 . . 6_565 ?
C42 Lu7 Lu8 Lu2 179.3(5) . . . 6_565 ?
C62 Lu7 Lu8 Lu2 131.1(16) . . . 6_565 ?
C43 Lu7 Lu8 Lu2 169.0(7) . . . 6_565 ?
C41 Lu7 Lu8 Lu2 -141.3(11) . . . 6_565 ?
C61 Lu7 Lu8 Lu2 91(5) . . . 6_565 ?
C63 Lu7 Lu8 Lu2 113.2(9) . . . 6_565 ?
C44 Lu7 Lu8 Lu2 131.0(8) . . . 6_565 ?
Lu4 Lu7 Lu8 C44 169(6) 6_565 . . . ?
Lu9 Lu7 Lu8 C44 -79.2(19) . . . . ?
Lu9 Lu7 Lu8 C44 177(3) 6_565 . . . ?
Lu8 Lu7 Lu8 C44 134.8(7) 6_565 . . . ?
C42 Lu7 Lu8 C44 48.3(4) . . . . ?
C62 Lu7 Lu8 C44 0.1(16) . . . . ?
C43 Lu7 Lu8 C44 37.99(13) . . . . ?
C41 Lu7 Lu8 C44 87.7(10) . . . . ?
C61 Lu7 Lu8 C44 -40(5) . . . . ?
C63 Lu7 Lu8 C44 -17.8(7) . . . . ?
Lu4 Lu7 Lu8 C43 131(6) 6_565 . . . ?
Lu9 Lu7 Lu8 C43 -117.1(19) . . . . ?
Lu9 Lu7 Lu8 C43 139(3) 6_565 . . . ?
Lu8 Lu7 Lu8 C43 96.8(8) 6_565 . . . ?
C42 Lu7 Lu8 C43 10.3(3) . . . . ?
C62 Lu7 Lu8 C43 -37.9(16) . . . . ?
C41 Lu7 Lu8 C43 49.7(10) . . . . ?
C61 Lu7 Lu8 C43 -78(5) . . . . ?
C63 Lu7 Lu8 C43 -55.8(7) . . . . ?
C44 Lu7 Lu8 C43 -37.99(13) . . . . ?
Lu4 Lu7 Lu8 C45 -176(5) 6_565 . . . ?
Lu9 Lu7 Lu8 C45 -64(2) . . . . ?
Lu9 Lu7 Lu8 C45 -168(3) 6_565 . . . ?
Lu8 Lu7 Lu8 C45 150.0(2) 6_565 . . . ?
C42 Lu7 Lu8 C45 63.4(10) . . . . ?
C62 Lu7 Lu8 C45 15(2) . . . . ?
C43 Lu7 Lu8 C45 53.2(8) . . . . ?
C41 Lu7 Lu8 C45 102.9(6) . . . . ?
C61 Lu7 Lu8 C45 -25(6) . . . . ?
C63 Lu7 Lu8 C45 -2.7(15) . . . . ?
C44 Lu7 Lu8 C45 15.2(7) . . . . ?
Lu4 Lu7 Lu8 C23 102(6) 6_565 . . . ?
Lu9 Lu7 Lu8 C23 -146(2) . . . . ?
Lu9 Lu7 Lu8 C23 110(3) 6_565 . . . ?
Lu8 Lu7 Lu8 C23 67.7(7) 6_565 . . . ?
C42 Lu7 Lu8 C23 -18.8(5) . . . . ?
C62 Lu7 Lu8 C23 -67.0(17) . . . . ?
C43 Lu7 Lu8 C23 -29.1(2) . . . . ?
C41 Lu7 Lu8 C23 20.6(10) . . . . ?
C61 Lu7 Lu8 C23 -107(5) . . . . ?
C63 Lu7 Lu8 C23 -84.9(8) . . . . ?
C44 Lu7 Lu8 C23 -67.1(2) . . . . ?
Lu4 Lu4 Lu8 Lu8 0.003(0) 6_565 . . 6_565 ?
Lu9 Lu4 Lu8 Lu8 15.7(12) 6_565 . . 6_565 ?
C62 Lu4 Lu8 Lu8 -95.6(7) . . . 6_565 ?
C63 Lu4 Lu8 Lu8 -134.7(4) . . . 6_565 ?
C61 Lu4 Lu8 Lu8 -55.1(16) . . . 6_565 ?
C42 Lu4 Lu8 Lu8 -68.5(3) . . . 6_565 ?
C44 Lu4 Lu8 Lu8 -128.82(15) . . . 6_565 ?
C64 Lu4 Lu8 Lu8 -175.2(3) . . . 6_565 ?
C43 Lu4 Lu8 Lu8 -89.22(15) . . . 6_565 ?
C76 Lu4 Lu8 Lu8 129.5(18) . . . 6_565 ?
Lu4 Lu4 Lu8 Lu7 21(3) 6_565 . . . ?
Lu9 Lu4 Lu8 Lu7 37(3) 6_565 . . . ?
Lu8 Lu4 Lu8 Lu7 21(3) 6_565 . . . ?
C62 Lu4 Lu8 Lu7 -75(3) . . . . ?
C63 Lu4 Lu8 Lu7 -114(3) . . . . ?
C61 Lu4 Lu8 Lu7 -34(3) . . . . ?
C42 Lu4 Lu8 Lu7 -48(3) . . . . ?
C44 Lu4 Lu8 Lu7 -108(3) . . . . ?
C64 Lu4 Lu8 Lu7 -154(3) . . . . ?
C43 Lu4 Lu8 Lu7 -68(3) . . . . ?
C76 Lu4 Lu8 Lu7 150(4) . . . . ?
Lu4 Lu4 Lu8 Lu9 -138(3) 6_565 . . . ?
Lu9 Lu4 Lu8 Lu9 -122(4) 6_565 . . . ?
Lu8 Lu4 Lu8 Lu9 -138(3) 6_565 . . . ?
C62 Lu4 Lu8 Lu9 126(3) . . . . ?
C63 Lu4 Lu8 Lu9 87(3) . . . . ?
C61 Lu4 Lu8 Lu9 167(4) . . . . ?
C42 Lu4 Lu8 Lu9 153(3) . . . . ?
C44 Lu4 Lu8 Lu9 93(3) . . . . ?
C64 Lu4 Lu8 Lu9 47(3) . . . . ?
C43 Lu4 Lu8 Lu9 133(3) . . . . ?
C76 Lu4 Lu8 Lu9 -9(3) . . . . ?
Lu9 Lu4 Lu8 Lu4 15.7(12) 6_565 . . 6_565 ?
Lu8 Lu4 Lu8 Lu4 -0.003(0) 6_565 . . 6_565 ?
C62 Lu4 Lu8 Lu4 -95.6(7) . . . 6_565 ?
C63 Lu4 Lu8 Lu4 -134.8(4) . . . 6_565 ?
C61 Lu4 Lu8 Lu4 -55.1(16) . . . 6_565 ?
C42 Lu4 Lu8 Lu4 -68.5(3) . . . 6_565 ?
C44 Lu4 Lu8 Lu4 -128.82(15) . . . 6_565 ?
C64 Lu4 Lu8 Lu4 -175.2(3) . . . 6_565 ?
C43 Lu4 Lu8 Lu4 -89.22(15) . . . 6_565 ?
C76 Lu4 Lu8 Lu4 129.5(18) . . . 6_565 ?
Lu4 Lu4 Lu8 Lu1 -131.5(2) 6_565 . . 6_565 ?
Lu9 Lu4 Lu8 Lu1 -115.8(12) 6_565 . . 6_565 ?
Lu8 Lu4 Lu8 Lu1 -131.5(2) 6_565 . . 6_565 ?
C62 Lu4 Lu8 Lu1 132.9(7) . . . 6_565 ?
C63 Lu4 Lu8 Lu1 93.7(4) . . . 6_565 ?
C61 Lu4 Lu8 Lu1 173.3(15) . . . 6_565 ?
C42 Lu4 Lu8 Lu1 160.0(3) . . . 6_565 ?
C44 Lu4 Lu8 Lu1 99.6(3) . . . 6_565 ?
C64 Lu4 Lu8 Lu1 53.2(4) . . . 6_565 ?
C43 Lu4 Lu8 Lu1 139.2(3) . . . 6_565 ?
C76 Lu4 Lu8 Lu1 -2.0(19) . . . 6_565 ?
Lu4 Lu4 Lu8 Lu9 -15.7(12) 6_565 . . 6_565 ?
Lu8 Lu4 Lu8 Lu9 -15.7(12) 6_565 . . 6_565 ?
C62 Lu4 Lu8 Lu9 -111.3(13) . . . 6_565 ?
C63 Lu4 Lu8 Lu9 -150.5(13) . . . 6_565 ?
C61 Lu4 Lu8 Lu9 -70.8(17) . . . 6_565 ?
C42 Lu4 Lu8 Lu9 -84.2(12) . . . 6_565 ?
C44 Lu4 Lu8 Lu9 -144.5(12) . . . 6_565 ?
C64 Lu4 Lu8 Lu9 169.1(13) . . . 6_565 ?
C43 Lu4 Lu8 Lu9 -104.9(12) . . . 6_565 ?
C76 Lu4 Lu8 Lu9 114(2) . . . 6_565 ?
Lu4 Lu4 Lu8 Lu2 -113.2(5) 6_565 . . 6_565 ?
Lu9 Lu4 Lu8 Lu2 -97.5(13) 6_565 . . 6_565 ?
Lu8 Lu4 Lu8 Lu2 -113.2(5) 6_565 . . 6_565 ?
C62 Lu4 Lu8 Lu2 151.2(5) . . . 6_565 ?
C63 Lu4 Lu8 Lu2 112.0(4) . . . 6_565 ?
C61 Lu4 Lu8 Lu2 -168.3(13) . . . 6_565 ?
C42 Lu4 Lu8 Lu2 178.3(4) . . . 6_565 ?
C44 Lu4 Lu8 Lu2 118.0(5) . . . 6_565 ?
C64 Lu4 Lu8 Lu2 71.6(5) . . . 6_565 ?
C43 Lu4 Lu8 Lu2 157.6(5) . . . 6_565 ?
C76 Lu4 Lu8 Lu2 16(2) . . . 6_565 ?
Lu4 Lu4 Lu8 C44 128.82(15) 6_565 . . . ?
Lu9 Lu4 Lu8 C44 144.5(12) 6_565 . . . ?
Lu8 Lu4 Lu8 C44 128.82(15) 6_565 . . . ?
C62 Lu4 Lu8 C44 33.3(7) . . . . ?
C63 Lu4 Lu8 C44 -5.9(3) . . . . ?
C61 Lu4 Lu8 C44 73.7(16) . . . . ?
C42 Lu4 Lu8 C44 60.4(2) . . . . ?
C64 Lu4 Lu8 C44 -46.4(3) . . . . ?
C43 Lu4 Lu8 C44 39.60(9) . . . . ?
C76 Lu4 Lu8 C44 -101.7(18) . . . . ?
Lu4 Lu4 Lu8 C43 89.22(15) 6_565 . . . ?
Lu9 Lu4 Lu8 C43 104.9(12) 6_565 . . . ?
Lu8 Lu4 Lu8 C43 89.22(15) 6_565 . . . ?
C62 Lu4 Lu8 C43 -6.3(7) . . . . ?
C63 Lu4 Lu8 C43 -45.5(4) . . . . ?
C61 Lu4 Lu8 C43 34.1(16) . . . . ?
C42 Lu4 Lu8 C43 20.8(2) . . . . ?
C44 Lu4 Lu8 C43 -39.60(9) . . . . ?
C64 Lu4 Lu8 C43 -86.0(3) . . . . ?
C76 Lu4 Lu8 C43 -141.3(18) . . . . ?
Lu4 Lu4 Lu8 C45 153.4(2) 6_565 . . . ?
Lu9 Lu4 Lu8 C45 169.1(12) 6_565 . . . ?
Lu8 Lu4 Lu8 C45 153.4(2) 6_565 . . . ?
C62 Lu4 Lu8 C45 57.8(8) . . . . ?
C63 Lu4 Lu8 C45 18.6(5) . . . . ?
C61 Lu4 Lu8 C45 98.2(17) . . . . ?
C42 Lu4 Lu8 C45 84.9(4) . . . . ?
C44 Lu4 Lu8 C45 24.5(2) . . . . ?
C64 Lu4 Lu8 C45 -21.9(5) . . . . ?
C43 Lu4 Lu8 C45 64.1(3) . . . . ?
C76 Lu4 Lu8 C45 -77.1(18) . . . . ?
Lu4 Lu4 Lu8 C23 68.8(3) 6_565 . . . ?
Lu9 Lu4 Lu8 C23 84.5(13) 6_565 . . . ?
Lu8 Lu4 Lu8 C23 68.8(3) 6_565 . . . ?
C62 Lu4 Lu8 C23 -26.8(9) . . . . ?
C63 Lu4 Lu8 C23 -66.0(6) . . . . ?
C61 Lu4 Lu8 C23 13.6(18) . . . . ?
C42 Lu4 Lu8 C23 0.3(4) . . . . ?
C44 Lu4 Lu8 C23 -60.1(3) . . . . ?
C64 Lu4 Lu8 C23 -106.5(4) . . . . ?
C43 Lu4 Lu8 C23 -20.5(2) . . . . ?
C76 Lu4 Lu8 C23 -161.7(16) . . . . ?
Lu9 Lu7 Lu9 Lu4 -12(2) 6_565 . . 6_565 ?
Lu8 Lu7 Lu9 Lu4 -102(4) 6_565 . . 6_565 ?
Lu8 Lu7 Lu9 Lu4 -136(3) . . . 6_565 ?
C42 Lu7 Lu9 Lu4 114(4) . . . 6_565 ?
C62 Lu7 Lu9 Lu4 94(3) . . . 6_565 ?
C43 Lu7 Lu9 Lu4 155(4) . . . 6_565 ?
C41 Lu7 Lu9 Lu4 75(7) . . . 6_565 ?
C61 Lu7 Lu9 Lu4 57(3) . . . 6_565 ?
C63 Lu7 Lu9 Lu4 121(3) . . . 6_565 ?
C44 Lu7 Lu9 Lu4 158(3) . . . 6_565 ?
Lu4 Lu7 Lu9 Lu8 136(3) 6_565 . . . ?
Lu9 Lu7 Lu9 Lu8 124(2) 6_565 . . . ?
Lu8 Lu7 Lu9 Lu8 33(2) 6_565 . . . ?
C42 Lu7 Lu9 Lu8 -111(3) . . . . ?
C62 Lu7 Lu9 Lu8 -130.9(13) . . . . ?
C43 Lu7 Lu9 Lu8 -69.2(14) . . . . ?
C41 Lu7 Lu9 Lu8 -149(7) . . . . ?
C61 Lu7 Lu9 Lu8 -167.0(12) . . . . ?
C63 Lu7 Lu9 Lu8 -103.0(11) . . . . ?
C44 Lu7 Lu9 Lu8 -66.2(8) . . . . ?
Lu4 Lu7 Lu9 Lu9 12(2) 6_565 . . 6_565 ?
Lu8 Lu7 Lu9 Lu9 -91(3) 6_565 . . 6_565 ?
Lu8 Lu7 Lu9 Lu9 -124(2) . . . 6_565 ?
C42 Lu7 Lu9 Lu9 125(4) . . . 6_565 ?
C62 Lu7 Lu9 Lu9 105(2) . . . 6_565 ?
C43 Lu7 Lu9 Lu9 167(3) . . . 6_565 ?
C41 Lu7 Lu9 Lu9 87(7) . . . 6_565 ?
C61 Lu7 Lu9 Lu9 69(2) . . . 6_565 ?
C63 Lu7 Lu9 Lu9 133.1(19) . . . 6_565 ?
C44 Lu7 Lu9 Lu9 170(2) . . . 6_565 ?
Lu4 Lu7 Lu9 Lu8 102(4) 6_565 . . 6_565 ?
Lu9 Lu7 Lu9 Lu8 91(3) 6_565 . . 6_565 ?
Lu8 Lu7 Lu9 Lu8 -33(2) . . . 6_565 ?
C42 Lu7 Lu9 Lu8 -144(5) . . . 6_565 ?
C62 Lu7 Lu9 Lu8 -164(3) . . . 6_565 ?
C43 Lu7 Lu9 Lu8 -103(3) . . . 6_565 ?
C41 Lu7 Lu9 Lu8 177(9) . . . 6_565 ?
C61 Lu7 Lu9 Lu8 160(3) . . . 6_565 ?
C63 Lu7 Lu9 Lu8 -136(2) . . . 6_565 ?
C44 Lu7 Lu9 Lu8 -100(3) . . . 6_565 ?
Lu4 Lu7 Lu9 C63 -121(3) 6_565 . . . ?
Lu9 Lu7 Lu9 C63 -133.1(19) 6_565 . . . ?
Lu8 Lu7 Lu9 C63 136(2) 6_565 . . . ?
Lu8 Lu7 Lu9 C63 103.0(11) . . . . ?
C42 Lu7 Lu9 C63 -8(3) . . . . ?
C62 Lu7 Lu9 C63 -27.9(10) . . . . ?
C43 Lu7 Lu9 C63 33.8(16) . . . . ?
C41 Lu7 Lu9 C63 -46(7) . . . . ?
C61 Lu7 Lu9 C63 -64.0(8) . . . . ?
C44 Lu7 Lu9 C63 36.8(6) . . . . ?
Lu4 Lu7 Lu9 C64 -113(4) 6_565 . . . ?
Lu9 Lu7 Lu9 C64 -124(3) 6_565 . . . ?
Lu8 Lu7 Lu9 C64 145.3(19) 6_565 . . . ?
Lu8 Lu7 Lu9 C64 112(3) . . . . ?
C42 Lu7 Lu9 C64 1(5) . . . . ?
C62 Lu7 Lu9 C64 -19(3) . . . . ?
C43 Lu7 Lu9 C64 43(4) . . . . ?
C41 Lu7 Lu9 C64 -38(9) . . . . ?
C61 Lu7 Lu9 C64 -55(3) . . . . ?
C63 Lu7 Lu9 C64 9(2) . . . . ?
C44 Lu7 Lu9 C64 46(3) . . . . ?
Lu4 Lu7 Lu9 C62 -94(3) 6_565 . . . ?
Lu9 Lu7 Lu9 C62 -105(2) 6_565 . . . ?
Lu8 Lu7 Lu9 C62 164(3) 6_565 . . . ?
Lu8 Lu7 Lu9 C62 130.9(13) . . . . ?
C42 Lu7 Lu9 C62 20.0(19) . . . . ?
C43 Lu7 Lu9 C62 61.7(10) . . . . ?
C41 Lu7 Lu9 C62 -19(6) . . . . ?
C61 Lu7 Lu9 C62 -36.2(4) . . . . ?
C63 Lu7 Lu9 C62 27.9(10) . . . . ?
C44 Lu7 Lu9 C62 64.7(6) . . . . ?
Lu4 Lu7 Lu9 Lu1 119(3) 6_565 . . 6_565 ?
Lu9 Lu7 Lu9 Lu1 108(2) 6_565 . . 6_565 ?
Lu8 Lu7 Lu9 Lu1 17(4) 6_565 . . 6_565 ?
Lu8 Lu7 Lu9 Lu1 -16.2(19) . . . 6_565 ?
C42 Lu7 Lu9 Lu1 -127.1(18) . . . 6_565 ?
C62 Lu7 Lu9 Lu1 -147.1(15) . . . 6_565 ?
C43 Lu7 Lu9 Lu1 -85.4(18) . . . 6_565 ?
C41 Lu7 Lu9 Lu1 -166(5) . . . 6_565 ?
C61 Lu7 Lu9 Lu1 176.7(16) . . . 6_565 ?
C63 Lu7 Lu9 Lu1 -119(2) . . . 6_565 ?
C44 Lu7 Lu9 Lu1 -82.4(16) . . . 6_565 ?
Lu4 Lu7 Lu9 C75 -63(5) 6_565 . . . ?
Lu9 Lu7 Lu9 C75 -75(4) 6_565 . . . ?
Lu8 Lu7 Lu9 C75 -165.4(19) 6_565 . . . ?
Lu8 Lu7 Lu9 C75 161(3) . . . . ?
C42 Lu7 Lu9 C75 50(5) . . . . ?
C62 Lu7 Lu9 C75 30(4) . . . . ?
C43 Lu7 Lu9 C75 92(4) . . . . ?
C41 Lu7 Lu9 C75 12(10) . . . . ?
C61 Lu7 Lu9 C75 -6(3) . . . . ?
C63 Lu7 Lu9 C75 58(3) . . . . ?
C44 Lu7 Lu9 C75 95(3) . . . . ?
Lu4 Lu7 Lu9 C61 -57(3) 6_565 . . . ?
Lu9 Lu7 Lu9 C61 -69(2) 6_565 . . . ?
Lu8 Lu7 Lu9 C61 -160(3) 6_565 . . . ?
Lu8 Lu7 Lu9 C61 167.0(12) . . . . ?
C42 Lu7 Lu9 C61 56(2) . . . . ?
C62 Lu7 Lu9 C61 36.2(4) . . . . ?
C43 Lu7 Lu9 C61 97.8(12) . . . . ?
C41 Lu7 Lu9 C61 18(6) . . . . ?
C63 Lu7 Lu9 C61 64.0(8) . . . . ?
C44 Lu7 Lu9 C61 100.9(5) . . . . ?
Lu4 Lu7 Lu9 C44 -158(3) 6_565 . . . ?
Lu9 Lu7 Lu9 C44 -170(2) 6_565 . . . ?
Lu8 Lu7 Lu9 C44 100(3) 6_565 . . . ?
Lu8 Lu7 Lu9 C44 66.2(8) . . . . ?
C42 Lu7 Lu9 C44 -45(2) . . . . ?
C62 Lu7 Lu9 C44 -64.7(6) . . . . ?
C43 Lu7 Lu9 C44 -3.0(12) . . . . ?
C41 Lu7 Lu9 C44 -83(7) . . . . ?
C61 Lu7 Lu9 C44 -100.9(5) . . . . ?
C63 Lu7 Lu9 C44 -36.8(6) . . . . ?
Lu8 Lu8 Lu9 Lu7 -30(2) 6_565 . . . ?
Lu4 Lu8 Lu9 Lu7 12(2) . . . . ?
Lu4 Lu8 Lu9 Lu7 -15.6(17) 6_565 . . . ?
Lu1 Lu8 Lu9 Lu7 -162(2) 6_565 . . . ?
Lu9 Lu8 Lu9 Lu7 -30(2) 6_565 . . . ?
Lu2 Lu8 Lu9 Lu7 -147.5(18) 6_565 . . . ?
C44 Lu8 Lu9 Lu7 94(2) . . . . ?
C43 Lu8 Lu9 Lu7 58(2) . . . . ?
C45 Lu8 Lu9 Lu7 126(2) . . . . ?
C23 Lu8 Lu9 Lu7 44(2) . . . . ?
Lu8 Lu8 Lu9 Lu4 -14.5(11) 6_565 . . 6_565 ?
Lu7 Lu8 Lu9 Lu4 15.6(17) . . . 6_565 ?
Lu4 Lu8 Lu9 Lu4 27(2) . . . 6_565 ?
Lu1 Lu8 Lu9 Lu4 -146.3(10) 6_565 . . 6_565 ?
Lu9 Lu8 Lu9 Lu4 -14.5(11) 6_565 . . 6_565 ?
Lu2 Lu8 Lu9 Lu4 -131.8(8) 6_565 . . 6_565 ?
C44 Lu8 Lu9 Lu4 110.0(10) . . . 6_565 ?
C43 Lu8 Lu9 Lu4 73.6(10) . . . 6_565 ?
C45 Lu8 Lu9 Lu4 141.6(9) . . . 6_565 ?
C23 Lu8 Lu9 Lu4 59.4(15) . . . 6_565 ?
Lu8 Lu8 Lu9 Lu9 0.002(1) 6_565 . . 6_565 ?
Lu7 Lu8 Lu9 Lu9 30(2) . . . 6_565 ?
Lu4 Lu8 Lu9 Lu9 42(3) . . . 6_565 ?
Lu4 Lu8 Lu9 Lu9 14.5(11) 6_565 . . 6_565 ?
Lu1 Lu8 Lu9 Lu9 -131.8(2) 6_565 . . 6_565 ?
Lu2 Lu8 Lu9 Lu9 -117.3(5) 6_565 . . 6_565 ?
C44 Lu8 Lu9 Lu9 124.5(2) . . . 6_565 ?
C43 Lu8 Lu9 Lu9 88.1(2) . . . 6_565 ?
C45 Lu8 Lu9 Lu9 156.1(3) . . . 6_565 ?
C23 Lu8 Lu9 Lu9 73.9(7) . . . 6_565 ?
Lu7 Lu8 Lu9 Lu8 30(2) . . . 6_565 ?
Lu4 Lu8 Lu9 Lu8 42(3) . . . 6_565 ?
Lu4 Lu8 Lu9 Lu8 14.5(11) 6_565 . . 6_565 ?
Lu1 Lu8 Lu9 Lu8 -131.8(2) 6_565 . . 6_565 ?
Lu9 Lu8 Lu9 Lu8 -0.002(2) 6_565 . . 6_565 ?
Lu2 Lu8 Lu9 Lu8 -117.3(5) 6_565 . . 6_565 ?
C44 Lu8 Lu9 Lu8 124.5(2) . . . 6_565 ?
C43 Lu8 Lu9 Lu8 88.1(2) . . . 6_565 ?
C45 Lu8 Lu9 Lu8 156.1(3) . . . 6_565 ?
C23 Lu8 Lu9 Lu8 73.9(7) . . . 6_565 ?
Lu8 Lu8 Lu9 C63 -115.6(6) 6_565 . . . ?
Lu7 Lu8 Lu9 C63 -85.5(19) . . . . ?
Lu4 Lu8 Lu9 C63 -74(3) . . . . ?
Lu4 Lu8 Lu9 C63 -101.1(12) 6_565 . . . ?
Lu1 Lu8 Lu9 C63 112.6(7) 6_565 . . . ?
Lu9 Lu8 Lu9 C63 -115.6(6) 6_565 . . . ?
Lu2 Lu8 Lu9 C63 127.0(6) 6_565 . . . ?
C44 Lu8 Lu9 C63 8.8(5) . . . . ?
C43 Lu8 Lu9 C63 -27.5(7) . . . . ?
C45 Lu8 Lu9 C63 40.5(7) . . . . ?
C23 Lu8 Lu9 C63 -41.7(12) . . . . ?
Lu8 Lu8 Lu9 C64 -154.0(11) 6_565 . . . ?
Lu7 Lu8 Lu9 C64 -124(3) . . . . ?
Lu4 Lu8 Lu9 C64 -112(4) . . . . ?
Lu4 Lu8 Lu9 C64 -140(2) 6_565 . . . ?
Lu1 Lu8 Lu9 C64 74.2(12) 6_565 . . . ?
Lu9 Lu8 Lu9 C64 -154.0(11) 6_565 . . . ?
Lu2 Lu8 Lu9 C64 88.7(13) 6_565 . . . ?
C44 Lu8 Lu9 C64 -29.5(11) . . . . ?
C43 Lu8 Lu9 C64 -65.9(12) . . . . ?
C45 Lu8 Lu9 C64 2.1(13) . . . . ?
C23 Lu8 Lu9 C64 -80.1(13) . . . . ?
Lu8 Lu8 Lu9 C62 -77.4(9) 6_565 . . . ?
Lu7 Lu8 Lu9 C62 -47.3(16) . . . . ?
Lu4 Lu8 Lu9 C62 -36(2) . . . . ?
Lu4 Lu8 Lu9 C62 -62.9(9) 6_565 . . . ?
Lu1 Lu8 Lu9 C62 150.9(9) 6_565 . . . ?
Lu9 Lu8 Lu9 C62 -77.4(9) 6_565 . . . ?
Lu2 Lu8 Lu9 C62 165.3(6) 6_565 . . . ?
C44 Lu8 Lu9 C62 47.1(8) . . . . ?
C43 Lu8 Lu9 C62 10.8(9) . . . . ?
C45 Lu8 Lu9 C62 78.8(9) . . . . ?
C23 Lu8 Lu9 C62 -3.5(15) . . . . ?
Lu8 Lu8 Lu9 Lu1 131.8(2) 6_565 . . 6_565 ?
Lu7 Lu8 Lu9 Lu1 162(2) . . . 6_565 ?
Lu4 Lu8 Lu9 Lu1 174(3) . . . 6_565 ?
Lu4 Lu8 Lu9 Lu1 146.3(10) 6_565 . . 6_565 ?
Lu9 Lu8 Lu9 Lu1 131.8(2) 6_565 . . 6_565 ?
Lu2 Lu8 Lu9 Lu1 14.4(4) 6_565 . . 6_565 ?
C44 Lu8 Lu9 Lu1 -103.8(3) . . . 6_565 ?
C43 Lu8 Lu9 Lu1 -140.1(3) . . . 6_565 ?
C45 Lu8 Lu9 Lu1 -72.1(3) . . . 6_565 ?
C23 Lu8 Lu9 Lu1 -154.4(7) . . . 6_565 ?
Lu8 Lu8 Lu9 C75 -178(3) 6_565 . . . ?
Lu7 Lu8 Lu9 C75 -148(5) . . . . ?
Lu4 Lu8 Lu9 C75 -136(6) . . . . ?
Lu4 Lu8 Lu9 C75 -164(4) 6_565 . . . ?
Lu1 Lu8 Lu9 C75 50(3) 6_565 . . . ?
Lu9 Lu8 Lu9 C75 -178(3) 6_565 . . . ?
Lu2 Lu8 Lu9 C75 64(4) 6_565 . . . ?
C44 Lu8 Lu9 C75 -54(3) . . . . ?
C43 Lu8 Lu9 C75 -90(3) . . . . ?
C45 Lu8 Lu9 C75 -22(3) . . . . ?
C23 Lu8 Lu9 C75 -104(3) . . . . ?
Lu8 Lu8 Lu9 C61 -46.9(17) 6_565 . . . ?
Lu7 Lu8 Lu9 C61 -16.8(15) . . . . ?
Lu4 Lu8 Lu9 C61 -5.1(16) . . . . ?
Lu4 Lu8 Lu9 C61 -32.4(10) 6_565 . . . ?
Lu1 Lu8 Lu9 C61 -178.7(17) 6_565 . . . ?
Lu9 Lu8 Lu9 C61 -46.9(17) 6_565 . . . ?
Lu2 Lu8 Lu9 C61 -164.2(13) 6_565 . . . ?
C44 Lu8 Lu9 C61 77.6(16) . . . . ?
C43 Lu8 Lu9 C61 41.2(16) . . . . ?
C45 Lu8 Lu9 C61 109.2(16) . . . . ?
C23 Lu8 Lu9 C61 27(2) . . . . ?
Lu8 Lu8 Lu9 C44 -124.5(2) 6_565 . . . ?
Lu7 Lu8 Lu9 C44 -94(2) . . . . ?
Lu4 Lu8 Lu9 C44 -83(3) . . . . ?
Lu4 Lu8 Lu9 C44 -110.0(10) 6_565 . . . ?
Lu1 Lu8 Lu9 C44 103.8(3) 6_565 . . . ?
Lu9 Lu8 Lu9 C44 -124.5(2) 6_565 . . . ?
Lu2 Lu8 Lu9 C44 118.2(4) 6_565 . . . ?
C43 Lu8 Lu9 C44 -36.31(19) . . . . ?
C45 Lu8 Lu9 C44 31.7(2) . . . . ?
C23 Lu8 Lu9 C44 -50.6(7) . . . . ?
Lu6 Lu3 Lu10 Lu2 -79.7(17) . . . 6_565 ?
Lu11 Lu3 Lu10 Lu2 -124.9(14) . . . 6_565 ?
Lu5 Lu3 Lu10 Lu2 143(9) . . . 6_565 ?
Lu3 Lu3 Lu10 Lu2 -72.6(13) 6_565 . . 6_565 ?
C30 Lu3 Lu10 Lu2 123.2(10) . . . 6_565 ?
C29 Lu3 Lu10 Lu2 65.4(16) . . . 6_565 ?
C51 Lu3 Lu10 Lu2 135.9(11) . . . 6_565 ?
Lu10 Lu3 Lu10 Lu2 -72.6(13) 6_565 . . 6_565 ?
C31 Lu3 Lu10 Lu2 177.0(6) . . . 6_565 ?
C28 Lu3 Lu10 Lu2 56.6(11) . . . 6_565 ?
Lu11 Lu3 Lu10 Lu6 -45.2(14) . . . . ?
Lu5 Lu3 Lu10 Lu6 -137(8) . . . . ?
Lu3 Lu3 Lu10 Lu6 7.1(9) 6_565 . . . ?
C30 Lu3 Lu10 Lu6 -157.1(18) . . . . ?
Lu2 Lu3 Lu10 Lu6 79.7(17) 6_565 . . . ?
C29 Lu3 Lu10 Lu6 145.1(18) . . . . ?
C51 Lu3 Lu10 Lu6 -144.4(13) . . . . ?
Lu10 Lu3 Lu10 Lu6 7.1(9) 6_565 . . . ?
C31 Lu3 Lu10 Lu6 -103(2) . . . . ?
C28 Lu3 Lu10 Lu6 136.3(13) . . . . ?
Lu6 Lu3 Lu10 Lu1 -68(4) . . . 6_565 ?
Lu11 Lu3 Lu10 Lu1 -114(4) . . . 6_565 ?
Lu5 Lu3 Lu10 Lu1 154(12) . . . 6_565 ?
Lu3 Lu3 Lu10 Lu1 -61(4) 6_565 . . 6_565 ?
C30 Lu3 Lu10 Lu1 134(3) . . . 6_565 ?
Lu2 Lu3 Lu10 Lu1 11(2) 6_565 . . 6_565 ?
C29 Lu3 Lu10 Lu1 77(4) . . . 6_565 ?
C51 Lu3 Lu10 Lu1 147(4) . . . 6_565 ?
Lu10 Lu3 Lu10 Lu1 -61(4) 6_565 . . 6_565 ?
C31 Lu3 Lu10 Lu1 -172(2) . . . 6_565 ?
C28 Lu3 Lu10 Lu1 68(4) . . . 6_565 ?
Lu6 Lu3 Lu10 Lu11 45.2(14) . . . . ?
Lu5 Lu3 Lu10 Lu11 -92(8) . . . . ?
Lu3 Lu3 Lu10 Lu11 52.3(10) 6_565 . . . ?
C30 Lu3 Lu10 Lu11 -111.9(13) . . . . ?
Lu2 Lu3 Lu10 Lu11 124.9(14) 6_565 . . . ?
C29 Lu3 Lu10 Lu11 -169.7(14) . . . . ?
C51 Lu3 Lu10 Lu11 -99.2(10) . . . . ?
Lu10 Lu3 Lu10 Lu11 52.3(10) 6_565 . . . ?
C31 Lu3 Lu10 Lu11 -58.1(17) . . . . ?
C28 Lu3 Lu10 Lu11 -178.6(10) . . . . ?
Lu6 Lu3 Lu10 C51 144.4(13) . . . . ?
Lu11 Lu3 Lu10 C51 99.2(10) . . . . ?
Lu5 Lu3 Lu10 C51 7(8) . . . . ?
Lu3 Lu3 Lu10 C51 151.5(5) 6_565 . . . ?
C30 Lu3 Lu10 C51 -12.7(7) . . . . ?
Lu2 Lu3 Lu10 C51 -135.9(11) 6_565 . . . ?
C29 Lu3 Lu10 C51 -70.5(8) . . . . ?
Lu10 Lu3 Lu10 C51 151.5(5) 6_565 . . . ?
C31 Lu3 Lu10 C51 41.1(15) . . . . ?
C28 Lu3 Lu10 C51 -79.37(19) . . . . ?
Lu6 Lu3 Lu10 Lu3 -7.1(9) . . . 6_565 ?
Lu11 Lu3 Lu10 Lu3 -52.3(10) . . . 6_565 ?
Lu5 Lu3 Lu10 Lu3 -144(8) . . . 6_565 ?
C30 Lu3 Lu10 Lu3 -164.2(12) . . . 6_565 ?
Lu2 Lu3 Lu10 Lu3 72.6(13) 6_565 . . 6_565 ?
C29 Lu3 Lu10 Lu3 138.0(12) . . . 6_565 ?
C51 Lu3 Lu10 Lu3 -151.5(5) . . . 6_565 ?
Lu10 Lu3 Lu10 Lu3 -0.001(4) 6_565 . . 6_565 ?
C31 Lu3 Lu10 Lu3 -110.4(17) . . . 6_565 ?
C28 Lu3 Lu10 Lu3 129.2(6) . . . 6_565 ?
Lu6 Lu3 Lu10 C50 168.6(10) . . . . ?
Lu11 Lu3 Lu10 C50 123.4(10) . . . . ?
Lu5 Lu3 Lu10 C50 32(8) . . . . ?
Lu3 Lu3 Lu10 C50 175.70(13) 6_565 . . . ?
C30 Lu3 Lu10 C50 11.5(12) . . . . ?
Lu2 Lu3 Lu10 C50 -111.7(13) 6_565 . . . ?
C29 Lu3 Lu10 C50 -46.3(11) . . . . ?
C51 Lu3 Lu10 C50 24.2(5) . . . . ?
Lu10 Lu3 Lu10 C50 175.70(13) 6_565 . . . ?
C31 Lu3 Lu10 C50 65.3(17) . . . . ?
C28 Lu3 Lu10 C50 -55.1(6) . . . . ?
Lu6 Lu3 Lu10 C30 157.1(18) . . . . ?
Lu11 Lu3 Lu10 C30 111.9(13) . . . . ?
Lu5 Lu3 Lu10 C30 20(9) . . . . ?
Lu3 Lu3 Lu10 C30 164.2(12) 6_565 . . . ?
Lu2 Lu3 Lu10 C30 -123.2(10) 6_565 . . . ?
C29 Lu3 Lu10 C30 -57.8(7) . . . . ?
C51 Lu3 Lu10 C30 12.7(7) . . . . ?
Lu10 Lu3 Lu10 C30 164.2(12) 6_565 . . . ?
C31 Lu3 Lu10 C30 53.8(12) . . . . ?
C28 Lu3 Lu10 C30 -66.6(7) . . . . ?
Lu6 Lu3 Lu10 C49 -154.5(11) . . . . ?
Lu11 Lu3 Lu10 C49 160.4(9) . . . . ?
Lu5 Lu3 Lu10 C49 68(8) . . . . ?
Lu3 Lu3 Lu10 C49 -147.4(3) 6_565 . . . ?
C30 Lu3 Lu10 C49 48.5(9) . . . . ?
Lu2 Lu3 Lu10 C49 -74.8(10) 6_565 . . . ?
C29 Lu3 Lu10 C49 -9.3(11) . . . . ?
C51 Lu3 Lu10 C49 61.2(4) . . . . ?
Lu10 Lu3 Lu10 C49 -147.4(3) 6_565 . . . ?
C31 Lu3 Lu10 C49 102.3(14) . . . . ?
C28 Lu3 Lu10 C49 -18.2(4) . . . . ?
Lu6 Lu3 Lu10 C29 -145.1(18) . . . . ?
Lu11 Lu3 Lu10 C29 169.7(14) . . . . ?
Lu5 Lu3 Lu10 C29 78(9) . . . . ?
Lu3 Lu3 Lu10 C29 -138.0(12) 6_565 . . . ?
C30 Lu3 Lu10 C29 57.8(7) . . . . ?
Lu2 Lu3 Lu10 C29 -65.4(16) 6_565 . . . ?
C51 Lu3 Lu10 C29 70.5(8) . . . . ?
Lu10 Lu3 Lu10 C29 -138.0(12) 6_565 . . . ?
C31 Lu3 Lu10 C29 111.6(19) . . . . ?
C28 Lu3 Lu10 C29 -8.8(6) . . . . ?
Lu1 Lu5 Lu10 Lu2 16.4(8) 6_565 . . 6_565 ?
Lu3 Lu5 Lu10 Lu2 -147(8) . . . 6_565 ?
C50 Lu5 Lu10 Lu2 -112.6(3) . . . 6_565 ?
C68 Lu5 Lu10 Lu2 -113.7(10) . . . 6_565 ?
Lu6 Lu5 Lu10 Lu2 96(4) . . . 6_565 ?
Lu11 Lu5 Lu10 Lu2 128.0(14) . . . 6_565 ?
C49 Lu5 Lu10 Lu2 -76.1(2) . . . 6_565 ?
C51 Lu5 Lu10 Lu2 -139.5(4) . . . 6_565 ?
C67 Lu5 Lu10 Lu2 -56.1(12) . . . 6_565 ?
C69 Lu5 Lu10 Lu2 176.8(8) . . . 6_565 ?
Lu1 Lu5 Lu10 Lu6 -80(4) 6_565 . . . ?
Lu2 Lu5 Lu10 Lu6 -96(4) 6_565 . . . ?
Lu3 Lu5 Lu10 Lu6 117(10) . . . . ?
C50 Lu5 Lu10 Lu6 151(4) . . . . ?
C68 Lu5 Lu10 Lu6 150(3) . . . . ?
Lu11 Lu5 Lu10 Lu6 32(3) . . . . ?
C49 Lu5 Lu10 Lu6 -172(4) . . . . ?
C51 Lu5 Lu10 Lu6 125(4) . . . . ?
C67 Lu5 Lu10 Lu6 -152(3) . . . . ?
C69 Lu5 Lu10 Lu6 81(4) . . . . ?
Lu2 Lu5 Lu10 Lu1 -16.4(8) 6_565 . . 6_565 ?
Lu3 Lu5 Lu10 Lu1 -163(8) . . . 6_565 ?
C50 Lu5 Lu10 Lu1 -129.0(9) . . . 6_565 ?
C68 Lu5 Lu10 Lu1 -130.1(16) . . . 6_565 ?
Lu6 Lu5 Lu10 Lu1 80(4) . . . 6_565 ?
Lu11 Lu5 Lu10 Lu1 111.7(14) . . . 6_565 ?
C49 Lu5 Lu10 Lu1 -92.5(8) . . . 6_565 ?
C51 Lu5 Lu10 Lu1 -155.9(6) . . . 6_565 ?
C67 Lu5 Lu10 Lu1 -72.5(12) . . . 6_565 ?
C69 Lu5 Lu10 Lu1 160.4(16) . . . 6_565 ?
Lu1 Lu5 Lu10 Lu11 -111.7(14) 6_565 . . . ?
Lu2 Lu5 Lu10 Lu11 -128.0(14) 6_565 . . . ?
Lu3 Lu5 Lu10 Lu11 85(8) . . . . ?
C50 Lu5 Lu10 Lu11 119.4(13) . . . . ?
C68 Lu5 Lu10 Lu11 118.2(14) . . . . ?
Lu6 Lu5 Lu10 Lu11 -32(3) . . . . ?
C49 Lu5 Lu10 Lu11 155.9(14) . . . . ?
C51 Lu5 Lu10 Lu11 92.5(14) . . . . ?
C67 Lu5 Lu10 Lu11 175.8(10) . . . . ?
C69 Lu5 Lu10 Lu11 48.8(19) . . . . ?
Lu1 Lu5 Lu10 C51 155.9(6) 6_565 . . . ?
Lu2 Lu5 Lu10 C51 139.5(4) 6_565 . . . ?
Lu3 Lu5 Lu10 C51 -7(8) . . . . ?
C50 Lu5 Lu10 C51 26.9(4) . . . . ?
C68 Lu5 Lu10 C51 25.8(13) . . . . ?
Lu6 Lu5 Lu10 C51 -125(4) . . . . ?
Lu11 Lu5 Lu10 C51 -92.5(14) . . . . ?
C49 Lu5 Lu10 C51 63.4(3) . . . . ?
C67 Lu5 Lu10 C51 83.4(12) . . . . ?
C69 Lu5 Lu10 C51 -43.7(11) . . . . ?
Lu1 Lu5 Lu10 Lu3 -62(2) 6_565 . . 6_565 ?
Lu2 Lu5 Lu10 Lu3 -78.4(18) 6_565 . . 6_565 ?
Lu3 Lu5 Lu10 Lu3 135(10) . . . 6_565 ?
C50 Lu5 Lu10 Lu3 169.0(17) . . . 6_565 ?
C68 Lu5 Lu10 Lu3 167.9(9) . . . 6_565 ?
Lu6 Lu5 Lu10 Lu3 18(2) . . . 6_565 ?
Lu11 Lu5 Lu10 Lu3 49.7(17) . . . 6_565 ?
C49 Lu5 Lu10 Lu3 -154.5(18) . . . 6_565 ?
C51 Lu5 Lu10 Lu3 142(2) . . . 6_565 ?
C67 Lu5 Lu10 Lu3 -134.5(12) . . . 6_565 ?
C69 Lu5 Lu10 Lu3 98(2) . . . 6_565 ?
Lu1 Lu5 Lu10 C50 129.0(9) 6_565 . . . ?
Lu2 Lu5 Lu10 C50 112.6(3) 6_565 . . . ?
Lu3 Lu5 Lu10 C50 -34(9) . . . . ?
C68 Lu5 Lu10 C50 -1.1(8) . . . . ?
Lu6 Lu5 Lu10 C50 -151(4) . . . . ?
Lu11 Lu5 Lu10 C50 -119.4(13) . . . . ?
C49 Lu5 Lu10 C50 36.5(2) . . . . ?
C51 Lu5 Lu10 C50 -26.9(4) . . . . ?
C67 Lu5 Lu10 C50 56.4(10) . . . . ?
C69 Lu5 Lu10 C50 -70.6(9) . . . . ?
Lu1 Lu5 Lu10 C30 146.3(7) 6_565 . . . ?
Lu2 Lu5 Lu10 C30 130.0(11) 6_565 . . . ?
Lu3 Lu5 Lu10 C30 -17(8) . . . . ?
C50 Lu5 Lu10 C30 17.4(11) . . . . ?
C68 Lu5 Lu10 C30 16.2(19) . . . . ?
Lu6 Lu5 Lu10 C30 -134(4) . . . . ?
Lu11 Lu5 Lu10 C30 -102.0(18) . . . . ?
C49 Lu5 Lu10 C30 53.9(10) . . . . ?
C51 Lu5 Lu10 C30 -9.6(7) . . . . ?
C67 Lu5 Lu10 C30 73.8(17) . . . . ?
C69 Lu5 Lu10 C30 -53.2(16) . . . . ?
Lu1 Lu5 Lu10 C49 92.5(8) 6_565 . . . ?
Lu2 Lu5 Lu10 C49 76.1(2) 6_565 . . . ?
Lu3 Lu5 Lu10 C49 -70(8) . . . . ?
C50 Lu5 Lu10 C49 -36.5(2) . . . . ?
C68 Lu5 Lu10 C49 -37.6(10) . . . . ?
Lu6 Lu5 Lu10 C49 172(4) . . . . ?
Lu11 Lu5 Lu10 C49 -155.9(14) . . . . ?
C51 Lu5 Lu10 C49 -63.4(3) . . . . ?
C67 Lu5 Lu10 C49 19.9(11) . . . . ?
C69 Lu5 Lu10 C49 -107.1(9) . . . . ?
Lu1 Lu5 Lu10 C29 96.4(14) 6_565 . . . ?
Lu2 Lu5 Lu10 C29 80.0(12) 6_565 . . . ?
Lu3 Lu5 Lu10 C29 -67(8) . . . . ?
C50 Lu5 Lu10 C29 -32.6(14) . . . . ?
C68 Lu5 Lu10 C29 -34(2) . . . . ?
Lu6 Lu5 Lu10 C29 176(5) . . . . ?
Lu11 Lu5 Lu10 C29 -152(2) . . . . ?
C49 Lu5 Lu10 C29 3.9(12) . . . . ?
C51 Lu5 Lu10 C29 -59.5(12) . . . . ?
C67 Lu5 Lu10 C29 24(2) . . . . ?
C69 Lu5 Lu10 C29 -103.2(13) . . . . ?
Lu3 Lu6 Lu10 Lu3 -162(2) 6_565 . . . ?
Lu11 Lu6 Lu10 Lu3 116.8(19) . . . . ?
Lu10 Lu6 Lu10 Lu3 -168.7(15) 6_565 . . . ?
C31 Lu6 Lu10 Lu3 40.4(14) . . . . ?
C13 Lu6 Lu10 Lu3 37.7(18) . . . . ?
C30 Lu6 Lu10 Lu3 15.8(13) . . . . ?
C12 Lu6 Lu10 Lu3 -58.4(19) . . . . ?
C29 Lu6 Lu10 Lu3 -24.2(13) . . . . ?
C11 Lu6 Lu10 Lu3 -50.2(14) . . . . ?
Lu5 Lu6 Lu10 Lu3 -172.6(15) 6_565 . . . ?
Lu3 Lu6 Lu10 Lu5 -159(5) . . . . ?
Lu3 Lu6 Lu10 Lu5 39(4) 6_565 . . . ?
Lu11 Lu6 Lu10 Lu5 -42(4) . . . . ?
Lu10 Lu6 Lu10 Lu5 32(4) 6_565 . . . ?
C31 Lu6 Lu10 Lu5 -118(4) . . . . ?
C13 Lu6 Lu10 Lu5 -121(4) . . . . ?
C30 Lu6 Lu10 Lu5 -143(4) . . . . ?
C12 Lu6 Lu10 Lu5 143(3) . . . . ?
C29 Lu6 Lu10 Lu5 177(4) . . . . ?
C11 Lu6 Lu10 Lu5 151(4) . . . . ?
Lu5 Lu6 Lu10 Lu5 28(4) 6_565 . . . ?
Lu3 Lu6 Lu10 Lu2 114.7(16) . . . 6_565 ?
Lu3 Lu6 Lu10 Lu2 -47.1(17) 6_565 . . 6_565 ?
Lu11 Lu6 Lu10 Lu2 -128.4(16) . . . 6_565 ?
Lu10 Lu6 Lu10 Lu2 -54.0(13) 6_565 . . 6_565 ?
C31 Lu6 Lu10 Lu2 155.1(7) . . . 6_565 ?
C13 Lu6 Lu10 Lu2 152.5(11) . . . 6_565 ?
C30 Lu6 Lu10 Lu2 130.5(8) . . . 6_565 ?
C12 Lu6 Lu10 Lu2 56.3(16) . . . 6_565 ?
C29 Lu6 Lu10 Lu2 90.5(8) . . . 6_565 ?
C11 Lu6 Lu10 Lu2 64.6(9) . . . 6_565 ?
Lu5 Lu6 Lu10 Lu2 -57.9(9) 6_565 . . 6_565 ?
Lu3 Lu6 Lu10 Lu1 150(2) . . . 6_565 ?
Lu3 Lu6 Lu10 Lu1 -12(2) 6_565 . . 6_565 ?
Lu11 Lu6 Lu10 Lu1 -93.3(19) . . . 6_565 ?
Lu10 Lu6 Lu10 Lu1 -18.9(18) 6_565 . . 6_565 ?
C31 Lu6 Lu10 Lu1 -169.7(9) . . . 6_565 ?
C13 Lu6 Lu10 Lu1 -172.4(7) . . . 6_565 ?
C30 Lu6 Lu10 Lu1 165.6(11) . . . 6_565 ?
C12 Lu6 Lu10 Lu1 91.4(15) . . . 6_565 ?
C29 Lu6 Lu10 Lu1 125.7(11) . . . 6_565 ?
C11 Lu6 Lu10 Lu1 99.7(11) . . . 6_565 ?
Lu5 Lu6 Lu10 Lu1 -22.8(13) 6_565 . . 6_565 ?
Lu3 Lu6 Lu10 Lu11 -116.8(19) . . . . ?
Lu3 Lu6 Lu10 Lu11 81.4(18) 6_565 . . . ?
Lu10 Lu6 Lu10 Lu11 74.4(14) 6_565 . . . ?
C31 Lu6 Lu10 Lu11 -76.4(14) . . . . ?
C13 Lu6 Lu10 Lu11 -79(2) . . . . ?
C30 Lu6 Lu10 Lu11 -101.1(13) . . . . ?
C12 Lu6 Lu10 Lu11 -175.2(18) . . . . ?
C29 Lu6 Lu10 Lu11 -141.0(14) . . . . ?
C11 Lu6 Lu10 Lu11 -167.0(14) . . . . ?
Lu5 Lu6 Lu10 Lu11 70.5(13) 6_565 . . . ?
Lu3 Lu6 Lu10 C51 -34.3(13) . . . . ?
Lu3 Lu6 Lu10 C51 163.9(13) 6_565 . . . ?
Lu11 Lu6 Lu10 C51 82.5(13) . . . . ?
Lu10 Lu6 Lu10 C51 157.0(6) 6_565 . . . ?
C31 Lu6 Lu10 C51 6.1(6) . . . . ?
C13 Lu6 Lu10 C51 3.4(15) . . . . ?
C30 Lu6 Lu10 C51 -18.5(3) . . . . ?
C12 Lu6 Lu10 C51 -92.7(11) . . . . ?
C29 Lu6 Lu10 C51 -58.5(3) . . . . ?
C11 Lu6 Lu10 C51 -84.5(5) . . . . ?
Lu5 Lu6 Lu10 C51 153.0(3) 6_565 . . . ?
Lu3 Lu6 Lu10 Lu3 162(2) . . . 6_565 ?
Lu11 Lu6 Lu10 Lu3 -81.4(18) . . . 6_565 ?
Lu10 Lu6 Lu10 Lu3 -6.9(9) 6_565 . . 6_565 ?
C31 Lu6 Lu10 Lu3 -157.8(17) . . . 6_565 ?
C13 Lu6 Lu10 Lu3 -160(3) . . . 6_565 ?
C30 Lu6 Lu10 Lu3 177.6(14) . . . 6_565 ?
C12 Lu6 Lu10 Lu3 103.4(19) . . . 6_565 ?
C29 Lu6 Lu10 Lu3 137.6(14) . . . 6_565 ?
C11 Lu6 Lu10 Lu3 111.6(15) . . . 6_565 ?
Lu5 Lu6 Lu10 Lu3 -10.8(11) 6_565 . . 6_565 ?
Lu3 Lu6 Lu10 C50 -15.1(14) . . . . ?
Lu3 Lu6 Lu10 C50 -176.9(11) 6_565 . . . ?
Lu11 Lu6 Lu10 C50 101.7(14) . . . . ?
Lu10 Lu6 Lu10 C50 176.2(2) 6_565 . . . ?
C31 Lu6 Lu10 C50 25.3(10) . . . . ?
C13 Lu6 Lu10 C50 23(2) . . . . ?
C30 Lu6 Lu10 C50 0.7(7) . . . . ?
C12 Lu6 Lu10 C50 -73.5(15) . . . . ?
C29 Lu6 Lu10 C50 -39.3(8) . . . . ?
C11 Lu6 Lu10 C50 -65.3(9) . . . . ?
Lu5 Lu6 Lu10 C50 172.2(6) 6_565 . . . ?
Lu3 Lu6 Lu10 C30 -15.8(13) . . . . ?
Lu3 Lu6 Lu10 C30 -177.6(14) 6_565 . . . ?
Lu11 Lu6 Lu10 C30 101.1(14) . . . . ?
Lu10 Lu6 Lu10 C30 175.5(8) 6_565 . . . ?
C31 Lu6 Lu10 C30 24.6(3) . . . . ?
C13 Lu6 Lu10 C30 22.0(13) . . . . ?
C12 Lu6 Lu10 C30 -74.2(11) . . . . ?
C29 Lu6 Lu10 C30 -39.97(13) . . . . ?
C11 Lu6 Lu10 C30 -65.9(3) . . . . ?
Lu5 Lu6 Lu10 C30 171.6(4) 6_565 . . . ?
Lu3 Lu6 Lu10 C49 30.3(13) . . . . ?
Lu3 Lu6 Lu10 C49 -131.5(13) 6_565 . . . ?
Lu11 Lu6 Lu10 C49 147.1(15) . . . . ?
Lu10 Lu6 Lu10 C49 -138.4(6) 6_565 . . . ?
C31 Lu6 Lu10 C49 70.7(8) . . . . ?
C13 Lu6 Lu10 C49 68.0(16) . . . . ?
C30 Lu6 Lu10 C49 46.1(6) . . . . ?
C12 Lu6 Lu10 C49 -28.1(16) . . . . ?
C29 Lu6 Lu10 C49 6.1(6) . . . . ?
C11 Lu6 Lu10 C49 -19.9(9) . . . . ?
Lu5 Lu6 Lu10 C49 -142.3(6) 6_565 . . . ?
Lu3 Lu6 Lu10 C29 24.2(13) . . . . ?
Lu3 Lu6 Lu10 C29 -137.6(14) 6_565 . . . ?
Lu11 Lu6 Lu10 C29 141.0(14) . . . . ?
Lu10 Lu6 Lu10 C29 -144.5(8) 6_565 . . . ?
C31 Lu6 Lu10 C29 64.6(3) . . . . ?
C13 Lu6 Lu10 C29 61.9(13) . . . . ?
C30 Lu6 Lu10 C29 39.97(13) . . . . ?
C12 Lu6 Lu10 C29 -34.2(10) . . . . ?
C11 Lu6 Lu10 C29 -26.0(3) . . . . ?
Lu5 Lu6 Lu10 C29 -148.4(4) 6_565 . . . ?
Lu3 Lu6 Lu11 Lu3 -160.8(13) 6_565 . . . ?
Lu10 Lu6 Lu11 Lu3 -139.9(10) 6_565 . . . ?
Lu10 Lu6 Lu11 Lu3 -21.0(7) . . . . ?
C31 Lu6 Lu11 Lu3 95.1(7) . . . . ?
C13 Lu6 Lu11 Lu3 135.8(8) . . . . ?
C30 Lu6 Lu11 Lu3 55.9(5) . . . . ?
C12 Lu6 Lu11 Lu3 155.8(16) . . . . ?
C29 Lu6 Lu11 Lu3 47.5(13) . . . . ?
C11 Lu6 Lu11 Lu3 113.2(17) . . . . ?
Lu5 Lu6 Lu11 Lu3 -135.1(8) 6_565 . . . ?
Lu3 Lu6 Lu11 Lu3 160.8(13) . . . 6_565 ?
Lu10 Lu6 Lu11 Lu3 21.0(7) 6_565 . . 6_565 ?
Lu10 Lu6 Lu11 Lu3 139.9(10) . . . 6_565 ?
C31 Lu6 Lu11 Lu3 -104.0(7) . . . 6_565 ?
C13 Lu6 Lu11 Lu3 -63.3(5) . . . 6_565 ?
C30 Lu6 Lu11 Lu3 -143.2(9) . . . 6_565 ?
C12 Lu6 Lu11 Lu3 -43.3(11) . . . 6_565 ?
C29 Lu6 Lu11 Lu3 -151.7(18) . . . 6_565 ?
C11 Lu6 Lu11 Lu3 -85.9(12) . . . 6_565 ?
Lu5 Lu6 Lu11 Lu3 25.7(7) 6_565 . . 6_565 ?
Lu3 Lu6 Lu11 Lu10 139.9(10) . . . 6_565 ?
Lu3 Lu6 Lu11 Lu10 -21.0(7) 6_565 . . 6_565 ?
Lu10 Lu6 Lu11 Lu10 118.9(11) . . . 6_565 ?
C31 Lu6 Lu11 Lu10 -125.0(6) . . . 6_565 ?
C13 Lu6 Lu11 Lu10 -84.3(6) . . . 6_565 ?
C30 Lu6 Lu11 Lu10 -164.2(6) . . . 6_565 ?
C12 Lu6 Lu11 Lu10 -64.3(14) . . . 6_565 ?
C29 Lu6 Lu11 Lu10 -172.7(14) . . . 6_565 ?
C11 Lu6 Lu11 Lu10 -106.9(15) . . . 6_565 ?
Lu5 Lu6 Lu11 Lu10 4.7(5) 6_565 . . 6_565 ?
Lu3 Lu6 Lu11 Lu10 21.0(7) . . . . ?
Lu3 Lu6 Lu11 Lu10 -139.9(10) 6_565 . . . ?
Lu10 Lu6 Lu11 Lu10 -118.9(11) 6_565 . . . ?
C31 Lu6 Lu11 Lu10 116.1(6) . . . . ?
C13 Lu6 Lu11 Lu10 156.8(6) . . . . ?
C30 Lu6 Lu11 Lu10 76.9(6) . . . . ?
C12 Lu6 Lu11 Lu10 176.8(12) . . . . ?
C29 Lu6 Lu11 Lu10 68.4(17) . . . . ?
C11 Lu6 Lu11 Lu10 134.2(13) . . . . ?
Lu5 Lu6 Lu11 Lu10 -114.1(8) 6_565 . . . ?
Lu3 Lu6 Lu11 C32 -97.5(7) . . . . ?
Lu3 Lu6 Lu11 C32 101.7(7) 6_565 . . . ?
Lu10 Lu6 Lu11 C32 122.7(6) 6_565 . . . ?
Lu10 Lu6 Lu11 C32 -118.4(6) . . . . ?
C31 Lu6 Lu11 C32 -2.35(4) . . . . ?
C13 Lu6 Lu11 C32 38.38(15) . . . . ?
C30 Lu6 Lu11 C32 -41.5(3) . . . . ?
C12 Lu6 Lu11 C32 58.4(11) . . . . ?
C29 Lu6 Lu11 C32 -50.0(15) . . . . ?
C11 Lu6 Lu11 C32 15.8(12) . . . . ?
Lu5 Lu6 Lu11 C32 127.4(4) 6_565 . . . ?
Lu3 Lu6 Lu11 C31 -95.1(7) . . . . ?
Lu3 Lu6 Lu11 C31 104.0(7) 6_565 . . . ?
Lu10 Lu6 Lu11 C31 125.0(6) 6_565 . . . ?
Lu10 Lu6 Lu11 C31 -116.1(6) . . . . ?
C13 Lu6 Lu11 C31 40.73(18) . . . . ?
C30 Lu6 Lu11 C31 -39.2(3) . . . . ?
C12 Lu6 Lu11 C31 60.7(12) . . . . ?
C29 Lu6 Lu11 C31 -47.7(14) . . . . ?
C11 Lu6 Lu11 C31 18.1(13) . . . . ?
Lu5 Lu6 Lu11 C31 129.8(4) 6_565 . . . ?
Lu3 Lu6 Lu11 C33 -137.9(11) . . . . ?
Lu3 Lu6 Lu11 C33 61.3(13) 6_565 . . . ?
Lu10 Lu6 Lu11 C33 82.2(10) 6_565 . . . ?
Lu10 Lu6 Lu11 C33 -158.9(13) . . . . ?
C31 Lu6 Lu11 C33 -42.8(10) . . . . ?
C13 Lu6 Lu11 C33 -2.1(11) . . . . ?
C30 Lu6 Lu11 C33 -82.0(8) . . . . ?
C12 Lu6 Lu11 C33 18(2) . . . . ?
C29 Lu6 Lu11 C33 -90.5(6) . . . . ?
C11 Lu6 Lu11 C33 -25(2) . . . . ?
Lu5 Lu6 Lu11 C33 87.0(7) 6_565 . . . ?
Lu3 Lu6 Lu11 C53 -60.8(16) . . . . ?
Lu3 Lu6 Lu11 C53 138.3(14) 6_565 . . . ?
Lu10 Lu6 Lu11 C53 159.3(16) 6_565 . . . ?
Lu10 Lu6 Lu11 C53 -81.8(13) . . . . ?
C31 Lu6 Lu11 C53 34.3(13) . . . . ?
C13 Lu6 Lu11 C53 75.0(13) . . . . ?
C30 Lu6 Lu11 C53 -4.9(15) . . . . ?
C12 Lu6 Lu11 C53 95.0(4) . . . . ?
C29 Lu6 Lu11 C53 -13(3) . . . . ?
C11 Lu6 Lu11 C53 52.4(4) . . . . ?
Lu5 Lu6 Lu11 C53 164.0(16) 6_565 . . . ?
Lu3 Lu6 Lu11 Lu5 25.7(7) . . . . ?
Lu3 Lu6 Lu11 Lu5 -135.1(8) 6_565 . . . ?
Lu10 Lu6 Lu11 Lu5 -114.1(8) 6_565 . . . ?
Lu10 Lu6 Lu11 Lu5 4.7(5) . . . . ?
C31 Lu6 Lu11 Lu5 120.8(3) . . . . ?
C13 Lu6 Lu11 Lu5 161.6(4) . . . . ?
C30 Lu6 Lu11 Lu5 81.6(5) . . . . ?
C12 Lu6 Lu11 Lu5 -178.5(10) . . . . ?
C29 Lu6 Lu11 Lu5 73.2(17) . . . . ?
C11 Lu6 Lu11 Lu5 138.9(11) . . . . ?
Lu5 Lu6 Lu11 Lu5 -109.4(7) 6_565 . . . ?
Lu3 Lu6 Lu11 Lu5 135.1(8) . . . 6_565 ?
Lu3 Lu6 Lu11 Lu5 -25.7(7) 6_565 . . 6_565 ?
Lu10 Lu6 Lu11 Lu5 -4.7(5) 6_565 . . 6_565 ?
Lu10 Lu6 Lu11 Lu5 114.1(8) . . . 6_565 ?
C31 Lu6 Lu11 Lu5 -129.8(4) . . . 6_565 ?
C13 Lu6 Lu11 Lu5 -89.0(4) . . . 6_565 ?
C30 Lu6 Lu11 Lu5 -168.9(4) . . . 6_565 ?
C12 Lu6 Lu11 Lu5 -69.1(14) . . . 6_565 ?
C29 Lu6 Lu11 Lu5 -177.4(12) . . . 6_565 ?
C11 Lu6 Lu11 Lu5 -111.7(16) . . . 6_565 ?
Lu3 Lu6 Lu11 C13 -135.8(8) . . . . ?
Lu3 Lu6 Lu11 C13 63.3(5) 6_565 . . . ?
Lu10 Lu6 Lu11 C13 84.3(6) 6_565 . . . ?
Lu10 Lu6 Lu11 C13 -156.8(6) . . . . ?
C31 Lu6 Lu11 C13 -40.73(18) . . . . ?
C30 Lu6 Lu11 C13 -79.9(4) . . . . ?
C12 Lu6 Lu11 C13 20.0(11) . . . . ?
C29 Lu6 Lu11 C13 -88.4(16) . . . . ?
C11 Lu6 Lu11 C13 -22.6(12) . . . . ?
Lu5 Lu6 Lu11 C13 89.0(4) 6_565 . . . ?
Lu10 Lu3 Lu11 Lu6 138.2(15) . . . . ?
Lu5 Lu3 Lu11 Lu6 143.4(12) . . . . ?
Lu3 Lu3 Lu11 Lu6 11.7(8) 6_565 . . . ?
C30 Lu3 Lu11 Lu6 -92.6(12) . . . . ?
Lu2 Lu3 Lu11 Lu6 107.1(12) 6_565 . . . ?
C29 Lu3 Lu11 Lu6 -53.7(18) . . . . ?
C51 Lu3 Lu11 Lu6 -136.5(11) . . . . ?
Lu10 Lu3 Lu11 Lu6 33.2(10) 6_565 . . . ?
C31 Lu3 Lu11 Lu6 -71.6(11) . . . . ?
Lu10 Lu3 Lu11 Lu3 126.5(11) . . . 6_565 ?
Lu6 Lu3 Lu11 Lu3 -11.7(8) . . . 6_565 ?
Lu5 Lu3 Lu11 Lu3 131.7(8) . . . 6_565 ?
C30 Lu3 Lu11 Lu3 -104.3(8) . . . 6_565 ?
Lu2 Lu3 Lu11 Lu3 95.4(9) 6_565 . . 6_565 ?
C29 Lu3 Lu11 Lu3 -65.4(16) . . . 6_565 ?
C51 Lu3 Lu11 Lu3 -148.2(7) . . . 6_565 ?
Lu10 Lu3 Lu11 Lu3 21.5(5) 6_565 . . 6_565 ?
C31 Lu3 Lu11 Lu3 -83.3(8) . . . 6_565 ?
Lu10 Lu3 Lu11 Lu10 105.1(15) . . . 6_565 ?
Lu6 Lu3 Lu11 Lu10 -33.2(10) . . . 6_565 ?
Lu5 Lu3 Lu11 Lu10 110.2(10) . . . 6_565 ?
Lu3 Lu3 Lu11 Lu10 -21.5(5) 6_565 . . 6_565 ?
C30 Lu3 Lu11 Lu10 -125.8(9) . . . 6_565 ?
Lu2 Lu3 Lu11 Lu10 73.9(12) 6_565 . . 6_565 ?
C29 Lu3 Lu11 Lu10 -86.8(16) . . . 6_565 ?
C51 Lu3 Lu11 Lu10 -169.7(8) . . . 6_565 ?
C31 Lu3 Lu11 Lu10 -104.8(10) . . . 6_565 ?
Lu6 Lu3 Lu11 Lu10 -138.2(15) . . . . ?
Lu5 Lu3 Lu11 Lu10 5.1(8) . . . . ?
Lu3 Lu3 Lu11 Lu10 -126.5(11) 6_565 . . . ?
C30 Lu3 Lu11 Lu10 129.2(11) . . . . ?
Lu2 Lu3 Lu11 Lu10 -31.2(7) 6_565 . . . ?
C29 Lu3 Lu11 Lu10 168.1(16) . . . . ?
C51 Lu3 Lu11 Lu10 85.2(10) . . . . ?
Lu10 Lu3 Lu11 Lu10 -105.1(15) 6_565 . . . ?
C31 Lu3 Lu11 Lu10 150.1(9) . . . . ?
Lu10 Lu3 Lu11 C32 -128.2(11) . . . . ?
Lu6 Lu3 Lu11 C32 93.6(15) . . . . ?
Lu5 Lu3 Lu11 C32 -123.0(8) . . . . ?
Lu3 Lu3 Lu11 C32 105.3(13) 6_565 . . . ?
C30 Lu3 Lu11 C32 1.0(10) . . . . ?
Lu2 Lu3 Lu11 C32 -159.3(6) 6_565 . . . ?
C29 Lu3 Lu11 C32 39.9(14) . . . . ?
C51 Lu3 Lu11 C32 -42.9(9) . . . . ?
Lu10 Lu3 Lu11 C32 126.8(15) 6_565 . . . ?
C31 Lu3 Lu11 C32 22.0(6) . . . . ?
Lu10 Lu3 Lu11 C31 -150.1(9) . . . . ?
Lu6 Lu3 Lu11 C31 71.6(11) . . . . ?
Lu5 Lu3 Lu11 C31 -145.0(4) . . . . ?
Lu3 Lu3 Lu11 C31 83.3(8) 6_565 . . . ?
C30 Lu3 Lu11 C31 -21.0(5) . . . . ?
Lu2 Lu3 Lu11 C31 178.7(4) 6_565 . . . ?
C29 Lu3 Lu11 C31 17.9(12) . . . . ?
C51 Lu3 Lu11 C31 -64.9(4) . . . . ?
Lu10 Lu3 Lu11 C31 104.8(10) 6_565 . . . ?
Lu10 Lu3 Lu11 C33 -158.3(15) . . . . ?
Lu6 Lu3 Lu11 C33 63.5(15) . . . . ?
Lu5 Lu3 Lu11 C33 -153.1(14) . . . . ?
Lu3 Lu3 Lu11 C33 75.2(14) 6_565 . . . ?
C30 Lu3 Lu11 C33 -29.1(17) . . . . ?
Lu2 Lu3 Lu11 C33 170.6(12) 6_565 . . . ?
C29 Lu3 Lu11 C33 10(2) . . . . ?
C51 Lu3 Lu11 C33 -73.0(15) . . . . ?
Lu10 Lu3 Lu11 C33 96.7(16) 6_565 . . . ?
C31 Lu3 Lu11 C33 -8.1(13) . . . . ?
Lu10 Lu3 Lu11 C53 -87.8(14) . . . . ?
Lu6 Lu3 Lu11 C53 134(2) . . . . ?
Lu5 Lu3 Lu11 C53 -82.6(11) . . . . ?
Lu3 Lu3 Lu11 C53 145.7(18) 6_565 . . . ?
C30 Lu3 Lu11 C53 41.4(12) . . . . ?
Lu2 Lu3 Lu11 C53 -118.9(10) 6_565 . . . ?
C29 Lu3 Lu11 C53 80.3(12) . . . . ?
C51 Lu3 Lu11 C53 -2.5(12) . . . . ?
Lu10 Lu3 Lu11 C53 167.2(19) 6_565 . . . ?
C31 Lu3 Lu11 C53 62.4(10) . . . . ?
Lu10 Lu3 Lu11 Lu5 -5.1(8) . . . . ?
Lu6 Lu3 Lu11 Lu5 -143.4(12) . . . . ?
Lu3 Lu3 Lu11 Lu5 -131.7(8) 6_565 . . . ?
C30 Lu3 Lu11 Lu5 124.0(6) . . . . ?
Lu2 Lu3 Lu11 Lu5 -36.3(4) 6_565 . . . ?
C29 Lu3 Lu11 Lu5 162.9(12) . . . . ?
C51 Lu3 Lu11 Lu5 80.1(4) . . . . ?
Lu10 Lu3 Lu11 Lu5 -110.2(10) 6_565 . . . ?
C31 Lu3 Lu11 Lu5 145.0(4) . . . . ?
Lu10 Lu3 Lu11 Lu5 94.2(12) . . . 6_565 ?
Lu6 Lu3 Lu11 Lu5 -44.0(9) . . . 6_565 ?
Lu5 Lu3 Lu11 Lu5 99.4(9) . . . 6_565 ?
Lu3 Lu3 Lu11 Lu5 -32.3(3) 6_565 . . 6_565 ?
C30 Lu3 Lu11 Lu5 -136.6(8) . . . 6_565 ?
Lu2 Lu3 Lu11 Lu5 63.1(11) 6_565 . . 6_565 ?
C29 Lu3 Lu11 Lu5 -97.7(15) . . . 6_565 ?
C51 Lu3 Lu11 Lu5 179.5(7) . . . 6_565 ?
Lu10 Lu3 Lu11 Lu5 -10.8(5) 6_565 . . 6_565 ?
C31 Lu3 Lu11 Lu5 -115.6(9) . . . 6_565 ?
Lu10 Lu3 Lu11 C13 174.2(9) . . . . ?
Lu6 Lu3 Lu11 C13 36.0(9) . . . . ?
Lu5 Lu3 Lu11 C13 179.3(4) . . . . ?
Lu3 Lu3 Lu11 C13 47.6(5) 6_565 . . . ?
C30 Lu3 Lu11 C13 -56.7(6) . . . . ?
Lu2 Lu3 Lu11 C13 143.0(5) 6_565 . . . ?
C29 Lu3 Lu11 C13 -17.7(14) . . . . ?
C51 Lu3 Lu11 C13 -100.6(5) . . . . ?
Lu10 Lu3 Lu11 C13 69.1(8) 6_565 . . . ?
C31 Lu3 Lu11 C13 -35.7(4) . . . . ?
Lu3 Lu10 Lu11 Lu6 -27.0(10) . . . . ?
Lu5 Lu10 Lu11 Lu6 164.9(15) . . . . ?
Lu2 Lu10 Lu11 Lu6 80(2) 6_565 . . . ?
Lu1 Lu10 Lu11 Lu6 131.1(12) 6_565 . . . ?
C51 Lu10 Lu11 Lu6 -99.1(12) . . . . ?
Lu3 Lu10 Lu11 Lu6 21.9(7) 6_565 . . . ?
C50 Lu10 Lu11 Lu6 -117.3(14) . . . . ?
C30 Lu10 Lu11 Lu6 -63.0(11) . . . . ?
C49 Lu10 Lu11 Lu6 -70(2) . . . . ?
C29 Lu10 Lu11 Lu6 -33.4(11) . . . . ?
Lu5 Lu10 Lu11 Lu3 -168(2) . . . . ?
Lu2 Lu10 Lu11 Lu3 107.5(18) 6_565 . . . ?
Lu6 Lu10 Lu11 Lu3 27.0(10) . . . . ?
Lu1 Lu10 Lu11 Lu3 158.0(13) 6_565 . . . ?
C51 Lu10 Lu11 Lu3 -72.1(11) . . . . ?
Lu3 Lu10 Lu11 Lu3 48.9(12) 6_565 . . . ?
C50 Lu10 Lu11 Lu3 -90.4(17) . . . . ?
C30 Lu10 Lu11 Lu3 -36.0(9) . . . . ?
C49 Lu10 Lu11 Lu3 -43(2) . . . . ?
C29 Lu10 Lu11 Lu3 -6.4(9) . . . . ?
Lu3 Lu10 Lu11 Lu3 -48.9(12) . . . 6_565 ?
Lu5 Lu10 Lu11 Lu3 143.0(13) . . . 6_565 ?
Lu2 Lu10 Lu11 Lu3 59(2) 6_565 . . 6_565 ?
Lu6 Lu10 Lu11 Lu3 -21.9(7) . . . 6_565 ?
Lu1 Lu10 Lu11 Lu3 109.2(13) 6_565 . . 6_565 ?
C51 Lu10 Lu11 Lu3 -121.0(11) . . . 6_565 ?
C50 Lu10 Lu11 Lu3 -139.2(10) . . . 6_565 ?
C30 Lu10 Lu11 Lu3 -84.9(11) . . . 6_565 ?
C49 Lu10 Lu11 Lu3 -91.6(19) . . . 6_565 ?
C29 Lu10 Lu11 Lu3 -55.3(11) . . . 6_565 ?
Lu3 Lu10 Lu11 Lu10 -75.0(16) . . . 6_565 ?
Lu5 Lu10 Lu11 Lu10 116.9(13) . . . 6_565 ?
Lu2 Lu10 Lu11 Lu10 33(3) 6_565 . . 6_565 ?
Lu6 Lu10 Lu11 Lu10 -48.0(11) . . . 6_565 ?
Lu1 Lu10 Lu11 Lu10 83.1(16) 6_565 . . 6_565 ?
C51 Lu10 Lu11 Lu10 -147.1(11) . . . 6_565 ?
Lu3 Lu10 Lu11 Lu10 -26.1(6) 6_565 . . 6_565 ?
C50 Lu10 Lu11 Lu10 -165.3(5) . . . 6_565 ?
C30 Lu10 Lu11 Lu10 -111.0(12) . . . 6_565 ?
C49 Lu10 Lu11 Lu10 -117.7(15) . . . 6_565 ?
C29 Lu10 Lu11 Lu10 -81.4(13) . . . 6_565 ?
Lu3 Lu10 Lu11 C32 62.7(16) . . . . ?
Lu5 Lu10 Lu11 C32 -105(2) . . . . ?
Lu2 Lu10 Lu11 C32 170.1(13) 6_565 . . . ?
Lu6 Lu10 Lu11 C32 90(2) . . . . ?
Lu1 Lu10 Lu11 C32 -139.3(12) 6_565 . . . ?
C51 Lu10 Lu11 C32 -9.4(15) . . . . ?
Lu3 Lu10 Lu11 C32 112(2) 6_565 . . . ?
C50 Lu10 Lu11 C32 -28(2) . . . . ?
C30 Lu10 Lu11 C32 26.6(13) . . . . ?
C49 Lu10 Lu11 C32 20(3) . . . . ?
C29 Lu10 Lu11 C32 56.2(15) . . . . ?
Lu3 Lu10 Lu11 C31 28.7(9) . . . . ?
Lu5 Lu10 Lu11 C31 -139.4(13) . . . . ?
Lu2 Lu10 Lu11 C31 136.2(16) 6_565 . . . ?
Lu6 Lu10 Lu11 C31 55.7(10) . . . . ?
Lu1 Lu10 Lu11 C31 -173.2(6) 6_565 . . . ?
C51 Lu10 Lu11 C31 -43.4(8) . . . . ?
Lu3 Lu10 Lu11 C31 77.6(12) 6_565 . . . ?
C50 Lu10 Lu11 C31 -61.6(16) . . . . ?
C30 Lu10 Lu11 C31 -7.3(5) . . . . ?
C49 Lu10 Lu11 C31 -14(2) . . . . ?
C29 Lu10 Lu11 C31 22.3(8) . . . . ?
Lu3 Lu10 Lu11 C33 48(4) . . . . ?
Lu5 Lu10 Lu11 C33 -120(4) . . . . ?
Lu2 Lu10 Lu11 C33 155(3) 6_565 . . . ?
Lu6 Lu10 Lu11 C33 75(4) . . . . ?
Lu1 Lu10 Lu11 C33 -154(4) 6_565 . . . ?
C51 Lu10 Lu11 C33 -24(4) . . . . ?
Lu3 Lu10 Lu11 C33 97(5) 6_565 . . . ?
C50 Lu10 Lu11 C33 -42(5) . . . . ?
C30 Lu10 Lu11 C33 12(4) . . . . ?
C49 Lu10 Lu11 C33 5(6) . . . . ?
C29 Lu10 Lu11 C33 42(4) . . . . ?
Lu3 Lu10 Lu11 C53 99.4(15) . . . . ?
Lu5 Lu10 Lu11 C53 -68.7(18) . . . . ?
Lu2 Lu10 Lu11 C53 -153.1(14) 6_565 . . . ?
Lu6 Lu10 Lu11 C53 126.4(19) . . . . ?
Lu1 Lu10 Lu11 C53 -102.5(12) 6_565 . . . ?
C51 Lu10 Lu11 C53 27.3(11) . . . . ?
Lu3 Lu10 Lu11 C53 148(2) 6_565 . . . ?
C50 Lu10 Lu11 C53 9(2) . . . . ?
C30 Lu10 Lu11 C53 63.4(9) . . . . ?
C49 Lu10 Lu11 C53 57(2) . . . . ?
C29 Lu10 Lu11 C53 93.0(10) . . . . ?
Lu3 Lu10 Lu11 Lu5 168(2) . . . . ?
Lu2 Lu10 Lu11 Lu5 -84(2) 6_565 . . . ?
Lu6 Lu10 Lu11 Lu5 -164.9(15) . . . . ?
Lu1 Lu10 Lu11 Lu5 -33.8(11) 6_565 . . . ?
C51 Lu10 Lu11 Lu5 96.0(12) . . . . ?
Lu3 Lu10 Lu11 Lu5 -143.0(13) 6_565 . . . ?
C50 Lu10 Lu11 Lu5 77.8(13) . . . . ?
C30 Lu10 Lu11 Lu5 132.1(13) . . . . ?
C49 Lu10 Lu11 Lu5 125(2) . . . . ?
C29 Lu10 Lu11 Lu5 161.7(15) . . . . ?
Lu3 Lu10 Lu11 Lu5 -91.2(14) . . . 6_565 ?
Lu5 Lu10 Lu11 Lu5 100.7(14) . . . 6_565 ?
Lu2 Lu10 Lu11 Lu5 16(2) 6_565 . . 6_565 ?
Lu6 Lu10 Lu11 Lu5 -64.2(10) . . . 6_565 ?
Lu1 Lu10 Lu11 Lu5 66.9(14) 6_565 . . 6_565 ?
C51 Lu10 Lu11 Lu5 -163.3(10) . . . 6_565 ?
Lu3 Lu10 Lu11 Lu5 -42.3(6) 6_565 . . 6_565 ?
C50 Lu10 Lu11 Lu5 178.5(8) . . . 6_565 ?
C30 Lu10 Lu11 Lu5 -127.2(11) . . . 6_565 ?
C49 Lu10 Lu11 Lu5 -133.9(14) . . . 6_565 ?
C29 Lu10 Lu11 Lu5 -97.6(10) . . . 6_565 ?
Lu3 Lu10 Lu11 C13 -6.2(10) . . . . ?
Lu5 Lu10 Lu11 C13 -174.3(12) . . . . ?
Lu2 Lu10 Lu11 C13 101(2) 6_565 . . . ?
Lu6 Lu10 Lu11 C13 20.8(6) . . . . ?
Lu1 Lu10 Lu11 C13 151.8(8) 6_565 . . . ?
C51 Lu10 Lu11 C13 -78.3(10) . . . . ?
Lu3 Lu10 Lu11 C13 42.6(7) 6_565 . . . ?
C50 Lu10 Lu11 C13 -96.6(13) . . . . ?
C30 Lu10 Lu11 C13 -42.3(8) . . . . ?
C49 Lu10 Lu11 C13 -49(2) . . . . ?
C29 Lu10 Lu11 C13 -12.6(10) . . . . ?
C18 C1 C2 C3 -138.9 . . . . ?
C5 C1 C2 C3 3.6 . . . . ?
Lu1 C1 C2 C3 -74.19(6) . . . . ?
Lu2 C1 C2 C3 -52.9 . . . . ?
C18 C1 C2 C15 -5.2 . . . . ?
C5 C1 C2 C15 137.3 . . . . ?
Lu1 C1 C2 C15 59.49(6) . . . . ?
Lu2 C1 C2 C15 80.8 . . . . ?
C18 C1 C2 Lu2 -86.0 . . . . ?
C5 C1 C2 Lu2 56.5 . . . . ?
Lu1 C1 C2 Lu2 -21.32(6) . . . . ?
C18 C1 C2 Lu1 -64.67(6) . . . . ?
C5 C1 C2 Lu1 77.81(6) . . . . ?
Lu2 C1 C2 Lu1 21.32(6) . . . . ?
C1 C2 C3 C12 144.4 . . . . ?
C15 C2 C3 C12 11.5 . . . . ?
Lu2 C2 C3 C12 92.98(5) . . . . ?
Lu1 C2 C3 C12 91.86(6) . . . . ?
C1 C2 C3 C4 -4.6 . . . . ?
C15 C2 C3 C4 -137.5 . . . . ?
Lu2 C2 C3 C4 -56.02(5) . . . . ?
Lu1 C2 C3 C4 -57.14(6) . . . . ?
C1 C2 C3 Lu2 51.45(5) . . . . ?
C15 C2 C3 Lu2 -81.48(5) . . . . ?
Lu1 C2 C3 Lu2 -1.12(6) . . . . ?
C1 C2 C3 Lu6 99.46(17) . . . . ?
C15 C2 C3 Lu6 -33.46(17) . . . . ?
Lu2 C2 C3 Lu6 48.02(17) . . . . ?
Lu1 C2 C3 Lu6 46.90(18) . . . . ?
C1 C2 C3 Lu1 52.57(6) . . . . ?
C15 C2 C3 Lu1 -80.36(6) . . . . ?
Lu2 C2 C3 Lu1 1.12(6) . . . . ?
C12 C3 C4 C9 -7.8 . . . . ?
C2 C3 C4 C9 147.1 . . . . ?
Lu2 C3 C4 C9 78.05(8) . . . . ?
Lu6 C3 C4 C9 39.02(14) . . . . ?
Lu1 C3 C4 C9 93.58(6) . . . . ?
C12 C3 C4 C5 -151.2 . . . . ?
C2 C3 C4 C5 3.7 . . . . ?
Lu2 C3 C4 C5 -65.34(8) . . . . ?
Lu6 C3 C4 C5 -104.37(14) . . . . ?
Lu1 C3 C4 C5 -49.81(6) . . . . ?
C12 C3 C4 Lu2 -85.85(8) . . . . ?
C2 C3 C4 Lu2 69.00(8) . . . . ?
Lu6 C3 C4 Lu2 -39.03(14) . . . . ?
Lu1 C3 C4 Lu2 15.53(5) . . . . ?
C12 C3 C4 Lu1 -101.38(6) . . . . ?
C2 C3 C4 Lu1 53.47(6) . . . . ?
Lu2 C3 C4 Lu1 -15.53(5) . . . . ?
Lu6 C3 C4 Lu1 -54.56(14) . . . . ?
C9 C4 C5 C6 0.2 . . . . ?
C3 C4 C5 C6 149.1 . . . . ?
Lu2 C4 C5 C6 72.57(6) . . . . ?
Lu1 C4 C5 C6 81.40(8) . . . . ?
C9 C4 C5 C1 -150.3 . . . . ?
C3 C4 C5 C1 -1.4 . . . . ?
Lu2 C4 C5 C1 -77.93(6) . . . . ?
Lu1 C4 C5 C1 -69.10(8) . . . . ?
C9 C4 C5 Lu2 -72.39(6) . . . . ?
C3 C4 C5 Lu2 76.48(6) . . . . ?
Lu1 C4 C5 Lu2 8.83(8) . . . . ?
C9 C4 C5 Lu1 -81.22(8) . . . . ?
C3 C4 C5 Lu1 67.66(8) . . . . ?
Lu2 C4 C5 Lu1 -8.83(8) . . . . ?
C18 C1 C5 C6 -8.1 . . . . ?
C2 C1 C5 C6 -152.7 . . . . ?
Lu1 C1 C5 C6 -62.37(9) . . . . ?
Lu2 C1 C5 C6 -80.29(7) . . . . ?
C18 C1 C5 C4 143.3 . . . . ?
C2 C1 C5 C4 -1.3 . . . . ?
Lu1 C1 C5 C4 89.04(9) . . . . ?
Lu2 C1 C5 C4 71.11(7) . . . . ?
C18 C1 C5 Lu2 72.20(7) . . . . ?
C2 C1 C5 Lu2 -72.39(7) . . . . ?
Lu1 C1 C5 Lu2 17.93(8) . . . . ?
C18 C1 C5 Lu1 54.27(9) . . . . ?
C2 C1 C5 Lu1 -90.32(9) . . . . ?
Lu2 C1 C5 Lu1 -17.93(8) . . . . ?
C4 C5 C6 C20 -142.2 . . . . ?
C1 C5 C6 C20 6.1 . . . . ?
Lu2 C5 C6 C20 -74.61(6) . . . . ?
Lu1 C5 C6 C20 -50.71(7) . . . . ?
C4 C5 C6 C7 -4.0 . . . . ?
C1 C5 C6 C7 144.2 . . . . ?
Lu2 C5 C6 C7 63.53(6) . . . . ?
Lu1 C5 C6 C7 87.43(7) . . . . ?
C4 C5 C6 Lu2 -67.56(6) . . . . ?
C1 C5 C6 Lu2 80.72(6) . . . . ?
Lu1 C5 C6 Lu2 23.90(5) . . . . ?
C4 C5 C6 Lu1 -91.46(7) . . . . ?
C1 C5 C6 Lu1 56.82(7) . . . . ?
Lu2 C5 C6 Lu1 -23.90(5) . . . . ?
C5 C6 C7 C8 7.9 . . . . ?
C20 C6 C7 C8 149.1 . . . . ?
Lu2 C6 C7 C8 60.78(6) . . . . ?
Lu1 C6 C7 C8 79.23(8) . . . . ?
C5 C6 C7 C22 -145.4 . . . . ?
C20 C6 C7 C22 -4.1 . . . . ?
Lu2 C6 C7 C22 -92.44(6) . . . . ?
Lu1 C6 C7 C22 -73.99(8) . . . . ?
C5 C6 C7 C25 -23.1 . . . . ?
C20 C6 C7 C25 118.1 . . . . ?
Lu2 C6 C7 C25 29.80(6) . . . . ?
Lu1 C6 C7 C25 48.25(8) . . . . ?
C5 C6 C7 Lu2 -52.92(6) . . . . ?
C20 C6 C7 Lu2 88.30(6) . . . . ?
Lu1 C6 C7 Lu2 18.45(6) . . . . ?
C5 C6 C7 Lu1 -71.37(7) . . . . ?
C20 C6 C7 Lu1 69.85(7) . . . . ?
Lu2 C6 C7 Lu1 -18.45(6) . . . . ?
C6 C7 C8 C25 -151.8 . . . . ?
C22 C7 C8 C25 -5.9 . . . . ?
Lu2 C7 C8 C25 -99.00(6) . . . . ?
Lu1 C7 C8 C25 -97.86(6) . . . . ?
C6 C7 C8 C9 -7.9 . . . . ?
C22 C7 C8 C9 138.0 . . . . ?
C25 C7 C8 C9 143.9 . . . . ?
Lu2 C7 C8 C9 44.93(6) . . . . ?
Lu1 C7 C8 C9 46.07(6) . . . . ?
C6 C7 C8 Lu2 -52.79(6) . . . . ?
C22 C7 C8 Lu2 93.06(6) . . . . ?
C25 C7 C8 Lu2 99.00(6) . . . . ?
Lu1 C7 C8 Lu2 1.14(4) . . . . ?
C25 C8 C9 C10 -10.6 . . . . ?
C7 C8 C9 C10 -147.3 . . . . ?
Lu2 C8 C9 C10 -99.57(7) . . . . ?
C25 C8 C9 C4 141.1 . . . . ?
C7 C8 C9 C4 4.4 . . . . ?
Lu2 C8 C9 C4 52.12(7) . . . . ?
C25 C8 C9 Lu2 88.97(7) . . . . ?
C7 C8 C9 Lu2 -47.75(7) . . . . ?
C5 C4 C9 C10 153.2 . . . . ?
C3 C4 C9 C10 12.7 . . . . ?
Lu2 C4 C9 C10 90.35(7) . . . . ?
Lu1 C4 C9 C10 98.52(7) . . . . ?
C5 C4 C9 C8 -0.3 . . . . ?
C3 C4 C9 C8 -140.8 . . . . ?
Lu2 C4 C9 C8 -63.15(7) . . . . ?
Lu1 C4 C9 C8 -54.97(7) . . . . ?
C5 C4 C9 Lu2 62.82(7) . . . . ?
C3 C4 C9 Lu2 -77.65(7) . . . . ?
Lu1 C4 C9 Lu2 8.17(7) . . . . ?
C8 C9 C10 C27 6.1 . . . . ?
C4 C9 C10 C27 -148.8 . . . . ?
Lu2 C9 C10 C27 -85.00(6) . . . . ?
C8 C9 C10 C11 148.5 . . . . ?
C4 C9 C10 C11 -6.4 . . . . ?
Lu2 C9 C10 C11 57.34(6) . . . . ?
C8 C9 C10 Lu6 101.62(13) . . . . ?
C4 C9 C10 Lu6 -53.27(13) . . . . ?
Lu2 C9 C10 Lu6 10.49(13) . . . . ?
C8 C9 C10 Lu3 88.54(16) . . . . ?
C4 C9 C10 Lu3 -66.35(16) . . . . ?
Lu2 C9 C10 Lu3 -2.59(16) . . . . ?
C8 C9 C10 Lu2 91.13(6) . . . . ?
C4 C9 C10 Lu2 -63.76(6) . . . . ?
C9 C10 C11 C29 -146.2 . . . . ?
C27 C10 C11 C29 -0.4 . . . . ?
Lu6 C10 C11 C29 -72.29(9) . . . . ?
Lu3 C10 C11 C29 -52.83(16) . . . . ?
Lu2 C10 C11 C29 -103.16(5) . . . . ?
C9 C10 C11 C12 -2.9 . . . . ?
C27 C10 C11 C12 142.9 . . . . ?
Lu6 C10 C11 C12 70.97(9) . . . . ?
Lu3 C10 C11 C12 90.43(16) . . . . ?
Lu2 C10 C11 C12 40.10(5) . . . . ?
C9 C10 C11 Lu6 -73.87(9) . . . . ?
C27 C10 C11 Lu6 71.93(9) . . . . ?
Lu3 C10 C11 Lu6 19.46(14) . . . . ?
Lu2 C10 C11 Lu6 -30.87(6) . . . . ?
C9 C10 C11 Lu3 -93.33(16) . . . . ?
C27 C10 C11 Lu3 52.47(16) . . . . ?
Lu6 C10 C11 Lu3 -19.46(15) . . . . ?
Lu2 C10 C11 Lu3 -50.33(15) . . . . ?
C9 C10 C11 Lu10 -96.10(19) . . . . ?
C27 C10 C11 Lu10 49.70(19) . . . . ?
Lu6 C10 C11 Lu10 -22.23(18) . . . . ?
Lu3 C10 C11 Lu10 -2.8(2) . . . . ?
Lu2 C10 C11 Lu10 -53.10(18) . . . . ?
C2 C3 C12 C13 3.0 . . . . ?
C4 C3 C12 C13 150.4 . . . . ?
Lu2 C3 C12 C13 88.3 . . . . ?
Lu6 C3 C12 C13 71.66(18) . . . . ?
Lu1 C3 C12 C13 74.23(5) . . . . ?
C2 C3 C12 C11 -151.2 . . . . ?
C4 C3 C12 C11 -3.8 . . . . ?
Lu2 C3 C12 C11 -66.0 . . . . ?
Lu6 C3 C12 C11 -82.56(18) . . . . ?
Lu1 C3 C12 C11 -79.98(5) . . . . ?
C2 C3 C12 Lu6 -68.67(18) . . . . ?
C4 C3 C12 Lu6 78.73(18) . . . . ?
Lu2 C3 C12 Lu6 16.60(18) . . . . ?
Lu1 C3 C12 Lu6 2.58(19) . . . . ?
C2 C3 C12 Lu3 -78.56(12) . . . . ?
C4 C3 C12 Lu3 68.85(12) . . . . ?
Lu2 C3 C12 Lu3 6.72(12) . . . . ?
Lu6 C3 C12 Lu3 -9.9(2) . . . . ?
Lu1 C3 C12 Lu3 -7.30(13) . . . . ?
C2 C3 C12 Lu2 -85.3 . . . . ?
C4 C3 C12 Lu2 62.1 . . . . ?
Lu6 C3 C12 Lu2 -16.60(18) . . . . ?
Lu1 C3 C12 Lu2 -14.02(6) . . . . ?
C2 C3 C12 Lu11 -51.5(5) . . . . ?
C4 C3 C12 Lu11 95.9(5) . . . . ?
Lu2 C3 C12 Lu11 33.8(5) . . . . ?
Lu6 C3 C12 Lu11 17.2(6) . . . . ?
Lu1 C3 C12 Lu11 19.7(5) . . . . ?
C29 C11 C12 C3 145.3 . . . . ?
C10 C11 C12 C3 8.9 . . . . ?
Lu6 C11 C12 C3 101.2(2) . . . . ?
Lu3 C11 C12 C3 105.03(10) . . . . ?
Lu10 C11 C12 C3 98.1(2) . . . . ?
C29 C11 C12 C13 -8.3 . . . . ?
C10 C11 C12 C13 -144.7 . . . . ?
Lu6 C11 C12 C13 -52.4(2) . . . . ?
Lu3 C11 C12 C13 -48.55(10) . . . . ?
Lu10 C11 C12 C13 -55.4(2) . . . . ?
C29 C11 C12 Lu6 44.1(2) . . . . ?
C10 C11 C12 Lu6 -92.3(2) . . . . ?
Lu3 C11 C12 Lu6 3.8(2) . . . . ?
Lu10 C11 C12 Lu6 -3.1(3) . . . . ?
C29 C11 C12 Lu3 40.28(10) . . . . ?
C10 C11 C12 Lu3 -96.12(10) . . . . ?
Lu6 C11 C12 Lu3 -3.8(2) . . . . ?
Lu10 C11 C12 Lu3 -6.9(2) . . . . ?
C29 C11 C12 Lu2 94.5 . . . . ?
C10 C11 C12 Lu2 -41.9 . . . . ?
Lu6 C11 C12 Lu2 50.4(2) . . . . ?
Lu3 C11 C12 Lu2 54.22(10) . . . . ?
Lu10 C11 C12 Lu2 47.3(2) . . . . ?
C29 C11 C12 Lu11 38.7(5) . . . . ?
C10 C11 C12 Lu11 -97.7(5) . . . . ?
Lu6 C11 C12 Lu11 -5.4(6) . . . . ?
Lu3 C11 C12 Lu11 -1.6(6) . . . . ?
Lu10 C11 C12 Lu11 -8.4(6) . . . . ?
C3 C12 C13 C14 -9.5 . . . . ?
C11 C12 C13 C14 146.7 . . . . ?
Lu6 C12 C13 C14 90.52(17) . . . . ?
Lu3 C12 C13 C14 102.83(10) . . . . ?
Lu2 C12 C13 C14 50.28(6) . . . . ?
Lu11 C12 C13 C14 79.2(4) . . . . ?
C3 C12 C13 C31 -151.3 . . . . ?
C11 C12 C13 C31 4.9 . . . . ?
Lu6 C12 C13 C31 -51.27(17) . . . . ?
Lu3 C12 C13 C31 -38.97(10) . . . . ?
Lu2 C12 C13 C31 -91.52(6) . . . . ?
Lu11 C12 C13 C31 -62.6(4) . . . . ?
C3 C12 C13 Lu6 -100.06(17) . . . . ?
C11 C12 C13 Lu6 56.15(17) . . . . ?
Lu3 C12 C13 Lu6 12.30(19) . . . . ?
Lu2 C12 C13 Lu6 -40.25(16) . . . . ?
Lu11 C12 C13 Lu6 -11.3(4) . . . . ?
C3 C12 C13 Lu11 -88.7(4) . . . . ?
C11 C12 C13 Lu11 67.5(4) . . . . ?
Lu6 C12 C13 Lu11 11.3(4) . . . . ?
Lu3 C12 C13 Lu11 23.6(4) . . . . ?
Lu2 C12 C13 Lu11 -28.9(3) . . . . ?
C3 C12 C13 Lu3 -112.36(10) . . . . ?
C11 C12 C13 Lu3 43.85(10) . . . . ?
Lu6 C12 C13 Lu3 -12.30(19) . . . . ?
Lu2 C12 C13 Lu3 -52.55(9) . . . . ?
Lu11 C12 C13 Lu3 -23.6(4) . . . . ?
Lu3 Lu6 C13 C12 -107.1(11) . . . . ?
Lu3 Lu6 C13 C12 66.5(6) 6_565 . . . ?
Lu11 Lu6 C13 C12 156.2(9) . . . . ?
Lu10 Lu6 C13 C12 76.1(4) 6_565 . . . ?
Lu10 Lu6 C13 C12 -127.6(14) . . . . ?
C31 Lu6 C13 C12 -131.20(12) . . . . ?
C30 Lu6 C13 C12 -105.67(18) . . . . ?
C29 Lu6 C13 C12 -66.15(14) . . . . ?
C11 Lu6 C13 C12 -30.73(6) . . . . ?
Lu5 Lu6 C13 C12 80.7(2) 6_565 . . . ?
Lu3 Lu6 C13 C14 133.5(11) . . . . ?
Lu3 Lu6 C13 C14 -52.8(7) 6_565 . . . ?
Lu11 Lu6 C13 C14 36.8(9) . . . . ?
Lu10 Lu6 C13 C14 -43.3(5) 6_565 . . . ?
Lu10 Lu6 C13 C14 113.1(14) . . . . ?
C31 Lu6 C13 C14 109.44(7) . . . . ?
C30 Lu6 C13 C14 134.97(14) . . . . ?
C12 Lu6 C13 C14 -119.4 . . . . ?
C29 Lu6 C13 C14 174.49(12) . . . . ?
C11 Lu6 C13 C14 -150.09(7) . . . . ?
Lu5 Lu6 C13 C14 -38.7(2) 6_565 . . . ?
Lu3 Lu6 C13 C31 24.1(10) . . . . ?
Lu3 Lu6 C13 C31 -162.2(7) 6_565 . . . ?
Lu11 Lu6 C13 C31 -72.6(9) . . . . ?
Lu10 Lu6 C13 C31 -152.7(5) 6_565 . . . ?
Lu10 Lu6 C13 C31 3.6(13) . . . . ?
C30 Lu6 C13 C31 25.53(8) . . . . ?
C12 Lu6 C13 C31 131.20(12) . . . . ?
C29 Lu6 C13 C31 65.05(12) . . . . ?
C11 Lu6 C13 C31 100.47(13) . . . . ?
Lu5 Lu6 C13 C31 -148.1(3) 6_565 . . . ?
Lu3 Lu6 C13 Lu11 96.8(14) . . . . ?
Lu3 Lu6 C13 Lu11 -89.6(11) 6_565 . . . ?
Lu10 Lu6 C13 Lu11 -80.1(10) 6_565 . . . ?
Lu10 Lu6 C13 Lu11 76.3(17) . . . . ?
C31 Lu6 C13 Lu11 72.6(9) . . . . ?
C30 Lu6 C13 Lu11 98.2(9) . . . . ?
C12 Lu6 C13 Lu11 -156.2(9) . . . . ?
C29 Lu6 C13 Lu11 137.7(10) . . . . ?
C11 Lu6 C13 Lu11 173.1(9) . . . . ?
Lu5 Lu6 C13 Lu11 -75.5(9) 6_565 . . . ?
Lu3 Lu6 C13 Lu3 173.6(17) 6_565 . . . ?
Lu11 Lu6 C13 Lu3 -96.8(14) . . . . ?
Lu10 Lu6 C13 Lu3 -176.9(14) 6_565 . . . ?
Lu10 Lu6 C13 Lu3 -20.5(10) . . . . ?
C31 Lu6 C13 Lu3 -24.1(10) . . . . ?
C30 Lu6 C13 Lu3 1.4(9) . . . . ?
C12 Lu6 C13 Lu3 107.1(11) . . . . ?
C29 Lu6 C13 Lu3 40.9(10) . . . . ?
C11 Lu6 C13 Lu3 76.4(11) . . . . ?
Lu5 Lu6 C13 Lu3 -172.2(12) 6_565 . . . ?
C12 C13 C14 C15 0.2 . . . . ?
C31 C13 C14 C15 144.3 . . . . ?
Lu6 C13 C14 C15 76.08(17) . . . . ?
Lu11 C13 C14 C15 93.3(7) . . . . ?
Lu3 C13 C14 C15 85.59(11) . . . . ?
C12 C13 C14 C33 -146.8 . . . . ?
C31 C13 C14 C33 -2.8 . . . . ?
Lu6 C13 C14 C33 -70.99(17) . . . . ?
Lu11 C13 C14 C33 -53.8(7) . . . . ?
Lu3 C13 C14 C33 -61.48(11) . . . . ?
C12 C13 C14 Lu11 -93.0(7) . . . . ?
C31 C13 C14 Lu11 51.0(7) . . . . ?
Lu6 C13 C14 Lu11 -17.2(7) . . . . ?
Lu3 C13 C14 Lu11 -7.7(7) . . . . ?
C12 C13 C14 Lu6 -75.84(17) . . . . ?
C31 C13 C14 Lu6 68.20(17) . . . . ?
Lu11 C13 C14 Lu6 17.2(7) . . . . ?
Lu3 C13 C14 Lu6 9.5(2) . . . . ?
C33 C14 C15 C16 4.8 . . . . ?
C13 C14 C15 C16 -137.3 . . . . ?
Lu11 C14 C15 C16 -62.3(7) . . . . ?
Lu6 C14 C15 C16 -88.71(15) . . . . ?
C33 C14 C15 C2 155.2 . . . . ?
C13 C14 C15 C2 13.0 . . . . ?
Lu11 C14 C15 C2 88.1(7) . . . . ?
Lu6 C14 C15 C2 61.67(15) . . . . ?
C33 C14 C15 Lu1 83.6 . . . . ?
C13 C14 C15 Lu1 -58.5 . . . . ?
Lu11 C14 C15 Lu1 16.5(7) . . . . ?
Lu6 C14 C15 Lu1 -9.90(15) . . . . ?
C33 C14 C15 Lu11 67.1(7) . . . . ?
C13 C14 C15 Lu11 -75.0(7) . . . . ?
Lu6 C14 C15 Lu11 -26.4(7) . . . . ?
C33 C14 C15 Lu2 97.1 . . . . ?
C13 C14 C15 Lu2 -45.0 . . . . ?
Lu11 C14 C15 Lu2 30.0(7) . . . . ?
Lu6 C14 C15 Lu2 3.58(15) . . . . ?
C3 C2 C15 C16 135.9 . . . . ?
C1 C2 C15 C16 5.7 . . . . ?
Lu2 C2 C15 C16 69.46(6) . . . . ?
Lu1 C2 C15 C16 51.53(6) . . . . ?
C3 C2 C15 C14 -18.2 . . . . ?
C1 C2 C15 C14 -148.4 . . . . ?
Lu2 C2 C15 C14 -84.56(6) . . . . ?
Lu1 C2 C15 C14 -102.50(6) . . . . ?
C3 C2 C15 Lu1 84.34(6) . . . . ?
C1 C2 C15 Lu1 -45.87(6) . . . . ?
Lu2 C2 C15 Lu1 17.93(5) . . . . ?
C3 C2 C15 Lu11 34.2(5) . . . . ?
C1 C2 C15 Lu11 -96.0(5) . . . . ?
Lu2 C2 C15 Lu11 -32.2(5) . . . . ?
Lu1 C2 C15 Lu11 -50.1(5) . . . . ?
C3 C2 C15 Lu2 66.40(6) . . . . ?
C1 C2 C15 Lu2 -63.80(6) . . . . ?
Lu1 C2 C15 Lu2 -17.93(5) . . . . ?
C14 C15 C16 C35 -6.0 . . . . ?
C2 C15 C16 C35 -154.6 . . . . ?
Lu1 C15 C16 C35 -104.55(6) . . . . ?
Lu11 C15 C16 C35 -49.8(6) . . . . ?
Lu2 C15 C16 C35 -102.0 . . . . ?
C14 C15 C16 C17 144.5 . . . . ?
C2 C15 C16 C17 -4.2 . . . . ?
Lu1 C15 C16 C17 45.86(6) . . . . ?
Lu11 C15 C16 C17 100.6(6) . . . . ?
Lu2 C15 C16 C17 48.4 . . . . ?
C14 C15 C16 Lu1 98.60(6) . . . . ?
C2 C15 C16 Lu1 -50.07(6) . . . . ?
Lu11 C15 C16 Lu1 54.8(6) . . . . ?
Lu2 C15 C16 Lu1 2.57(4) . . . . ?
C15 C16 C17 C18 1.8 . . . . ?
C35 C16 C17 C18 154.9 . . . . ?
Lu1 C16 C17 C18 58.53(6) . . . . ?
C15 C16 C17 C38 -139.7 . . . . ?
C35 C16 C17 C38 13.4 . . . . ?
Lu1 C16 C17 C38 -82.98(6) . . . . ?
C15 C16 C17 C19 -34.7 . . . . ?
C35 C16 C17 C19 118.3 . . . . ?
Lu1 C16 C17 C19 21.99(6) . . . . ?
C15 C16 C17 Lu1 -56.74(6) . . . . ?
C35 C16 C17 Lu1 96.34(6) . . . . ?
C15 C16 C17 Lu2 -47.7 . . . . ?
C35 C16 C17 Lu2 105.4 . . . . ?
Lu1 C16 C17 Lu2 9.03(4) . . . . ?
C38 C17 C18 C19 2.8 . . . . ?
C16 C17 C18 C19 -145.3 . . . . ?
Lu1 C17 C18 C19 -72.63(9) . . . . ?
Lu2 C17 C18 C19 -85.60(5) . . . . ?
C38 C17 C18 C1 147.3 . . . . ?
C16 C17 C18 C1 -0.7 . . . . ?
C19 C17 C18 C1 144.6 . . . . ?
Lu1 C17 C18 C1 71.94(9) . . . . ?
Lu2 C17 C18 C1 58.97(5) . . . . ?
C16 C17 C18 C38 -148.1 . . . . ?
C19 C17 C18 C38 -2.8 . . . . ?
Lu1 C17 C18 C38 -75.39(9) . . . . ?
Lu2 C17 C18 C38 -88.37(5) . . . . ?
C38 C17 C18 Lu1 75.39(9) . . . . ?
C16 C17 C18 Lu1 -72.69(9) . . . . ?
C19 C17 C18 Lu1 72.63(9) . . . . ?
Lu2 C17 C18 Lu1 -12.98(8) . . . . ?
C38 C17 C18 C39 2.6 . . . . ?
C16 C17 C18 C39 -145.5 . . . . ?
C19 C17 C18 C39 -0.2 . . . . ?
Lu1 C17 C18 C39 -72.82(9) . . . . ?
Lu2 C17 C18 C39 -85.79(5) . . . . ?
C38 C17 C18 Lu2 88.37(5) . . . . ?
C16 C17 C18 Lu2 -59.71(5) . . . . ?
C19 C17 C18 Lu2 85.60(5) . . . . ?
Lu1 C17 C18 Lu2 12.98(8) . . . . ?
C5 C1 C18 C17 -134.9 . . . . ?
C2 C1 C18 C17 2.9 . . . . ?
Lu1 C1 C18 C17 -75.55(9) . . . . ?
Lu2 C1 C18 C17 -79.1 . . . . ?
C5 C1 C18 C19 4.9 . . . . ?
C2 C1 C18 C19 142.6 . . . . ?
Lu1 C1 C18 C19 64.17(9) . . . . ?
Lu2 C1 C18 C19 60.6 . . . . ?
C5 C1 C18 C38 -98.8 . . . . ?
C2 C1 C18 C38 38.9 . . . . ?
Lu1 C1 C18 C38 -39.52(9) . . . . ?
Lu2 C1 C18 C38 -43.1 . . . . ?
C5 C1 C18 Lu1 -59.32(9) . . . . ?
C2 C1 C18 Lu1 78.43(9) . . . . ?
Lu2 C1 C18 Lu1 -3.56(9) . . . . ?
C5 C1 C18 C39 -32.9 . . . . ?
C2 C1 C18 C39 104.8 . . . . ?
Lu1 C1 C18 C39 26.39(9) . . . . ?
Lu2 C1 C18 C39 22.8 . . . . ?
C5 C1 C18 Lu2 -55.8 . . . . ?
C2 C1 C18 Lu2 82.0 . . . . ?
Lu1 C1 C18 Lu2 3.56(9) . . . . ?
C17 C18 C19 C39 -0.3 . . . . ?
C1 C18 C19 C39 -143.2 . . . . ?
C38 C18 C19 C39 1.5 . . . . ?
Lu1 C18 C19 C39 -78.29(6) . . . . ?
Lu2 C18 C19 C39 -93.6 . . . . ?
C17 C18 C19 C20 143.1 . . . . ?
C1 C18 C19 C20 0.2 . . . . ?
C38 C18 C19 C20 144.9 . . . . ?
Lu1 C18 C19 C20 65.11(6) . . . . ?
C39 C18 C19 C20 143.4 . . . . ?
Lu2 C18 C19 C20 49.8 . . . . ?
C17 C18 C19 C38 -1.8 . . . . ?
C1 C18 C19 C38 -144.7 . . . . ?
Lu1 C18 C19 C38 -79.77(6) . . . . ?
C39 C18 C19 C38 -1.5 . . . . ?
Lu2 C18 C19 C38 -95.1 . . . . ?
C1 C18 C19 C17 -142.9 . . . . ?
C38 C18 C19 C17 1.8 . . . . ?
Lu1 C18 C19 C17 -77.98(6) . . . . ?
C39 C18 C19 C17 0.3 . . . . ?
Lu2 C18 C19 C17 -93.3 . . . . ?
C17 C18 C19 Lu1 77.98(6) . . . . ?
C1 C18 C19 Lu1 -64.91(6) . . . . ?
C38 C18 C19 Lu1 79.77(6) . . . . ?
C39 C18 C19 Lu1 78.29(6) . . . . ?
Lu2 C18 C19 Lu1 -15.33(5) . . . . ?
C17 C18 C19 Lu2 93.3 . . . . ?
C1 C18 C19 Lu2 -49.6 . . . . ?
C38 C18 C19 Lu2 95.1 . . . . ?
Lu1 C18 C19 Lu2 15.33(5) . . . . ?
C39 C18 C19 Lu2 93.6 . . . . ?
C39 C19 C20 C6 135.8 . . . . ?
C18 C19 C20 C6 -2.3 . . . . ?
C38 C19 C20 C6 95.0 . . . . ?
C17 C19 C20 C6 31.2 . . . . ?
Lu1 C19 C20 C6 57.12(8) . . . . ?
Lu2 C19 C20 C6 48.28(5) . . . . ?
C39 C19 C20 C21 -8.2 . . . . ?
C18 C19 C20 C21 -146.3 . . . . ?
C38 C19 C20 C21 -49.0 . . . . ?
C17 C19 C20 C21 -112.8 . . . . ?
Lu1 C19 C20 C21 -86.89(8) . . . . ?
Lu2 C19 C20 C21 -95.73(5) . . . . ?
C39 C19 C20 Lu1 78.70(8) . . . . ?
C18 C19 C20 Lu1 -59.39(8) . . . . ?
C38 C19 C20 Lu1 37.91(8) . . . . ?
C17 C19 C20 Lu1 -25.88(8) . . . . ?
Lu2 C19 C20 Lu1 -8.84(6) . . . . ?
C39 C19 C20 Lu2 87.54(5) . . . . ?
C18 C19 C20 Lu2 -50.55(5) . . . . ?
C38 C19 C20 Lu2 46.75(5) . . . . ?
C17 C19 C20 Lu2 -17.0 . . . . ?
Lu1 C19 C20 Lu2 8.84(6) . . . . ?
C5 C6 C20 C19 -1.0 . . . . ?
C7 C6 C20 C19 -143.7 . . . . ?
Lu2 C6 C20 C19 -59.74(6) . . . . ?
Lu1 C6 C20 C19 -52.41(8) . . . . ?
C5 C6 C20 C21 145.8 . . . . ?
C7 C6 C20 C21 3.1 . . . . ?
Lu2 C6 C20 C21 87.06(6) . . . . ?
Lu1 C6 C20 C21 94.39(8) . . . . ?
C5 C6 C20 Lu1 51.42(8) . . . . ?
C7 C6 C20 Lu1 -91.34(8) . . . . ?
Lu2 C6 C20 Lu1 -7.33(6) . . . . ?
C5 C6 C20 Lu2 58.75(6) . . . . ?
C7 C6 C20 Lu2 -84.01(6) . . . . ?
Lu1 C6 C20 Lu2 7.33(6) . . . . ?
C19 C20 C21 C22 148.7 . . . . ?
C6 C20 C21 C22 -0.7 . . . . ?
Lu1 C20 C21 C22 79.95(6) . . . . ?
Lu2 C20 C21 C22 59.5 . . . . ?
C19 C20 C21 C41 3.7 . . . . ?
C6 C20 C21 C41 -145.7 . . . . ?
Lu1 C20 C21 C41 -65.11(6) . . . . ?
Lu2 C20 C21 C41 -85.6 . . . . ?
C19 C20 C21 Lu7 59.2(4) . . . . ?
C6 C20 C21 Lu7 -90.2(4) . . . . ?
Lu1 C20 C21 Lu7 -9.6(4) . . . . ?
Lu2 C20 C21 Lu7 -30.0(4) . . . . ?
C19 C20 C21 Lu1 68.79(6) . . . . ?
C6 C20 C21 Lu1 -80.63(6) . . . . ?
Lu2 C20 C21 Lu1 -20.48(5) . . . . ?
C19 C20 C21 Lu8 84.08(11) . . . . ?
C6 C20 C21 Lu8 -65.35(11) . . . . ?
Lu1 C20 C21 Lu8 15.28(12) . . . . ?
Lu2 C20 C21 Lu8 -5.19(12) . . . . ?
C20 C21 C22 C23 -152.8 . . . . ?
C41 C21 C22 C23 -2.5 . . . . ?
Lu7 C21 C22 C23 -42.2(4) . . . . ?
Lu1 C21 C22 C23 -100.08(5) . . . . ?
Lu8 C21 C22 C23 -51.62(13) . . . . ?
C20 C21 C22 C7 -1.9 . . . . ?
C41 C21 C22 C7 148.4 . . . . ?
Lu7 C21 C22 C7 108.7(4) . . . . ?
Lu1 C21 C22 C7 50.76(5) . . . . ?
Lu8 C21 C22 C7 99.22(13) . . . . ?
C20 C21 C22 Lu8 -101.17(13) . . . . ?
C41 C21 C22 Lu8 49.14(13) . . . . ?
Lu7 C21 C22 Lu8 9.5(4) . . . . ?
Lu1 C21 C22 Lu8 -48.46(13) . . . . ?
C20 C21 C22 Lu7 -110.6(4) . . . . ?
C41 C21 C22 Lu7 39.7(4) . . . . ?
Lu1 C21 C22 Lu7 -57.9(4) . . . . ?
Lu8 C21 C22 Lu7 -9.5(4) . . . . ?
C20 C21 C22 Lu2 -48.9 . . . . ?
C41 C21 C22 Lu2 101.4 . . . . ?
Lu7 C21 C22 Lu2 61.7(4) . . . . ?
Lu1 C21 C22 Lu2 3.77(4) . . . . ?
Lu8 C21 C22 Lu2 52.23(13) . . . . ?
C8 C7 C22 C23 4.1 . . . . ?
C6 C7 C22 C23 152.9 . . . . ?
C25 C7 C22 C23 0.6 . . . . ?
Lu2 C7 C22 C23 87.79(6) . . . . ?
Lu1 C7 C22 C23 101.21(6) . . . . ?
C8 C7 C22 C21 -145.1 . . . . ?
C6 C7 C22 C21 3.7 . . . . ?
C25 C7 C22 C21 -148.7 . . . . ?
Lu2 C7 C22 C21 -61.42(6) . . . . ?
Lu1 C7 C22 C21 -48.00(6) . . . . ?
C8 C7 C22 Lu8 -49.69(13) . . . . ?
C6 C7 C22 Lu8 99.17(13) . . . . ?
C25 C7 C22 Lu8 -53.22(13) . . . . ?
Lu2 C7 C22 Lu8 34.01(13) . . . . ?
Lu1 C7 C22 Lu8 47.44(13) . . . . ?
C8 C7 C22 Lu7 -69.5(2) . . . . ?
C6 C7 C22 Lu7 79.4(2) . . . . ?
C25 C7 C22 Lu7 -73.0(2) . . . . ?
Lu2 C7 C22 Lu7 14.2(2) . . . . ?
Lu1 C7 C22 Lu7 27.7(2) . . . . ?
C8 C7 C22 Lu2 -83.70(6) . . . . ?
C6 C7 C22 Lu2 65.16(6) . . . . ?
C25 C7 C22 Lu2 -87.24(6) . . . . ?
Lu1 C7 C22 Lu2 13.42(4) . . . . ?
C21 C22 C23 C43 2.1 . . . . ?
C7 C22 C23 C43 -144.5 . . . . ?
Lu8 C22 C23 C43 -69.29(16) . . . . ?
Lu7 C22 C23 C43 -42.4(3) . . . . ?
Lu2 C22 C23 C43 -85.6 . . . . ?
C21 C22 C23 C24 146.7 . . . . ?
C7 C22 C23 C24 0.2 . . . . ?
Lu8 C22 C23 C24 75.37(16) . . . . ?
Lu7 C22 C23 C24 102.3(3) . . . . ?
Lu2 C22 C23 C24 59.1 . . . . ?
C21 C22 C23 Lu8 71.35(16) . . . . ?
C7 C22 C23 Lu8 -75.18(16) . . . . ?
Lu7 C22 C23 Lu8 26.9(4) . . . . ?
Lu2 C22 C23 Lu8 -16.28(16) . . . . ?
C21 C22 C23 Lu7 44.4(3) . . . . ?
C7 C22 C23 Lu7 -102.1(3) . . . . ?
Lu8 C22 C23 Lu7 -26.9(4) . . . . ?
Lu2 C22 C23 Lu7 -43.2(3) . . . . ?
C21 C22 C23 Lu4 46.80(12) . . . . ?
C7 C22 C23 Lu4 -99.74(12) . . . . ?
Lu8 C22 C23 Lu4 -24.56(19) . . . . ?
Lu7 C22 C23 Lu4 2.4(4) . . . . ?
Lu2 C22 C23 Lu4 -40.84(12) . . . . ?
C22 C23 C24 C46 -145.1 . . . . ?
C43 C23 C24 C46 6.1 . . . . ?
Lu8 C23 C24 C46 -53.42(16) . . . . ?
Lu7 C23 C24 C46 -49.4(3) . . . . ?
Lu4 C23 C24 C46 -43.69(12) . . . . ?
C22 C23 C24 C25 -1.3 . . . . ?
C43 C23 C24 C25 149.9 . . . . ?
Lu8 C23 C24 C25 90.34(16) . . . . ?
Lu7 C23 C24 C25 94.3(3) . . . . ?
Lu4 C23 C24 C25 100.07(12) . . . . ?
C22 C23 C24 C26 -36.8 . . . . ?
C43 C23 C24 C26 114.4 . . . . ?
Lu8 C23 C24 C26 54.87(16) . . . . ?
Lu7 C23 C24 C26 58.9(3) . . . . ?
Lu4 C23 C24 C26 64.61(12) . . . . ?
C22 C23 C24 Lu8 -91.68(16) . . . . ?
C43 C23 C24 Lu8 59.56(16) . . . . ?
Lu7 C23 C24 Lu8 4.0(3) . . . . ?
Lu4 C23 C24 Lu8 9.73(19) . . . . ?
C9 C8 C25 C24 -136.9 . . . . ?
C7 C8 C25 C24 4.9 . . . . ?
Lu2 C8 C25 C24 -68.88(6) . . . . ?
C9 C8 C25 C26 11.3 . . . . ?
C7 C8 C25 C26 153.1 . . . . ?
Lu2 C8 C25 C26 79.35(6) . . . . ?
C9 C8 C25 C7 -141.8 . . . . ?
Lu2 C8 C25 C7 -73.80(6) . . . . ?
C9 C8 C25 Lu8 -86.90(14) . . . . ?
C7 C8 C25 Lu8 54.94(14) . . . . ?
Lu2 C8 C25 Lu8 -18.86(14) . . . . ?
C46 C24 C25 C8 145.1 . . . . ?
C23 C24 C25 C8 -1.7 . . . . ?
C26 C24 C25 C8 151.7 . . . . ?
Lu8 C24 C25 C8 66.97(16) . . . . ?
C46 C24 C25 C26 -6.6 . . . . ?
C23 C24 C25 C26 -153.4 . . . . ?
Lu8 C24 C25 C26 -84.75(16) . . . . ?
C46 C24 C25 C7 148.2 . . . . ?
C23 C24 C25 C7 1.4 . . . . ?
C26 C24 C25 C7 154.8 . . . . ?
Lu8 C24 C25 C7 70.09(16) . . . . ?
C46 C24 C25 Lu8 78.13(16) . . . . ?
C23 C24 C25 Lu8 -68.68(16) . . . . ?
C26 C24 C25 Lu8 84.75(16) . . . . ?
C8 C25 C26 C47 -153.5 . . . . ?
C24 C25 C26 C47 5.4 . . . . ?
C7 C25 C26 C47 -120.5 . . . . ?
Lu8 C25 C26 C47 -48.73(12) . . . . ?
C8 C25 C26 C27 -8.0 . . . . ?
C24 C25 C26 C27 150.8 . . . . ?
C7 C25 C26 C27 25.0 . . . . ?
Lu8 C25 C26 C27 96.74(12) . . . . ?
C8 C25 C26 C46 -155.0 . . . . ?
C24 C25 C26 C46 3.8 . . . . ?
C7 C25 C26 C46 -122.0 . . . . ?
Lu8 C25 C26 C46 -50.26(12) . . . . ?
C8 C25 C26 C24 -158.9 . . . . ?
C7 C25 C26 C24 -125.8 . . . . ?
Lu8 C25 C26 C24 -54.10(12) . . . . ?
C47 C26 C27 C10 148.9 . . . . ?
C25 C26 C27 C10 4.4 . . . . ?
C46 C26 C27 C10 104.8 . . . . ?
C24 C26 C27 C10 36.8 . . . . ?
C47 C26 C27 C28 -0.8 . . . . ?
C25 C26 C27 C28 -145.2 . . . . ?
C46 C26 C27 C28 -44.9 . . . . ?
C24 C26 C27 C28 -112.8 . . . . ?
C25 C26 C27 C47 -144.5 . . . . ?
C46 C26 C27 C47 -44.1 . . . . ?
C24 C26 C27 C47 -112.0 . . . . ?
C47 C26 C27 Lu3 59.88(16) . . . . ?
C25 C26 C27 Lu3 -84.60(16) . . . . ?
C46 C26 C27 Lu3 15.78(16) . . . . ?
C24 C26 C27 Lu3 -52.16(16) . . . . ?
C47 C26 C27 Lu10 53.7(2) . . . . ?
C25 C26 C27 Lu10 -90.7(2) . . . . ?
C46 C26 C27 Lu10 9.6(2) . . . . ?
C24 C26 C27 Lu10 -58.3(2) . . . . ?
C47 C26 C27 Lu6 75.24(8) . . . . ?
C25 C26 C27 Lu6 -69.24(8) . . . . ?
C46 C26 C27 Lu6 31.14(8) . . . . ?
C24 C26 C27 Lu6 -36.80(8) . . . . ?
C9 C10 C27 C26 -3.7 . . . . ?
C11 C10 C27 C26 -150.0 . . . . ?
Lu6 C10 C27 C26 -104.63(15) . . . . ?
Lu3 C10 C27 C26 -107.76(8) . . . . ?
Lu2 C10 C27 C26 -59.5 . . . . ?
C9 C10 C27 C28 150.2 . . . . ?
C11 C10 C27 C28 3.9 . . . . ?
Lu6 C10 C27 C28 49.28(15) . . . . ?
Lu3 C10 C27 C28 46.15(8) . . . . ?
Lu2 C10 C27 C28 94.4 . . . . ?
C9 C10 C27 C47 21.6 . . . . ?
C11 C10 C27 C47 -124.7 . . . . ?
Lu6 C10 C27 C47 -79.34(15) . . . . ?
Lu3 C10 C27 C47 -82.47(8) . . . . ?
Lu2 C10 C27 C47 -34.2 . . . . ?
C9 C10 C27 Lu3 104.10(8) . . . . ?
C11 C10 C27 Lu3 -42.27(8) . . . . ?
Lu6 C10 C27 Lu3 3.13(18) . . . . ?
Lu2 C10 C27 Lu3 48.24(8) . . . . ?
C9 C10 C27 Lu10 95.1(3) . . . . ?
C11 C10 C27 Lu10 -51.3(3) . . . . ?
Lu6 C10 C27 Lu10 -5.9(3) . . . . ?
Lu3 C10 C27 Lu10 -9.0(3) . . . . ?
Lu2 C10 C27 Lu10 39.2(3) . . . . ?
C9 C10 C27 Lu6 100.96(15) . . . . ?
C11 C10 C27 Lu6 -45.40(15) . . . . ?
Lu3 C10 C27 Lu6 -3.13(18) . . . . ?
Lu2 C10 C27 Lu6 45.11(15) . . . . ?
C26 C27 C28 C29 147.3 . . . . ?
C10 C27 C28 C29 -5.8 . . . . ?
C47 C27 C28 C29 146.9 . . . . ?
Lu3 C27 C28 C29 54.37(19) . . . . ?
Lu10 C27 C28 C29 72.6(4) . . . . ?
Lu6 C27 C28 C29 42.76(14) . . . . ?
C26 C27 C28 C49 7.6 . . . . ?
C10 C27 C28 C49 -145.5 . . . . ?
C47 C27 C28 C49 7.2 . . . . ?
Lu3 C27 C28 C49 -85.35(19) . . . . ?
Lu10 C27 C28 C49 -67.1(4) . . . . ?
Lu6 C27 C28 C49 -96.97(14) . . . . ?
C26 C27 C28 Lu3 92.94(19) . . . . ?
C10 C27 C28 Lu3 -60.19(19) . . . . ?
C47 C27 C28 Lu3 92.57(19) . . . . ?
Lu10 C27 C28 Lu3 18.3(3) . . . . ?
Lu6 C27 C28 Lu3 -11.6(2) . . . . ?
C26 C27 C28 Lu10 74.7(4) . . . . ?
C10 C27 C28 Lu10 -78.5(4) . . . . ?
C47 C27 C28 Lu10 74.3(4) . . . . ?
Lu3 C27 C28 Lu10 -18.3(3) . . . . ?
Lu6 C27 C28 Lu10 -29.9(4) . . . . ?
C26 C27 C28 Lu5 58.64(14) . . . . ?
C10 C27 C28 Lu5 -94.48(14) . . . . ?
C47 C27 C28 Lu5 58.28(14) . . . . ?
Lu3 C27 C28 Lu5 -34.29(16) . . . . ?
Lu10 C27 C28 Lu5 -16.0(3) . . . . ?
Lu6 C27 C28 Lu5 -45.91(19) . . . . ?
C26 C27 C28 Lu6 104.55(14) . . . . ?
C10 C27 C28 Lu6 -48.57(14) . . . . ?
C47 C27 C28 Lu6 104.19(14) . . . . ?
Lu3 C27 C28 Lu6 11.6(2) . . . . ?
Lu10 C27 C28 Lu6 29.9(4) . . . . ?
C27 C28 C29 C11 5.7 . . . . ?
C49 C28 C29 C11 143.0 . . . . ?
Lu3 C28 C29 C11 91.55(18) . . . . ?
Lu10 C28 C29 C11 95.5(2) . . . . ?
Lu5 C28 C29 C11 101.03(10) . . . . ?
Lu6 C28 C29 C11 76.58(15) . . . . ?
C27 C28 C29 C30 -141.0 . . . . ?
C49 C28 C29 C30 -3.7 . . . . ?
Lu3 C28 C29 C30 -55.13(18) . . . . ?
Lu10 C28 C29 C30 -51.2(2) . . . . ?
Lu5 C28 C29 C30 -45.65(10) . . . . ?
Lu6 C28 C29 C30 -70.10(15) . . . . ?
C27 C28 C29 Lu3 -85.83(18) . . . . ?
C49 C28 C29 Lu3 51.46(18) . . . . ?
Lu10 C28 C29 Lu3 3.9(3) . . . . ?
Lu5 C28 C29 Lu3 9.48(18) . . . . ?
Lu6 C28 C29 Lu3 -15.0(2) . . . . ?
C27 C28 C29 Lu6 -70.86(15) . . . . ?
C49 C28 C29 Lu6 66.43(15) . . . . ?
Lu3 C28 C29 Lu6 15.0(2) . . . . ?
Lu10 C28 C29 Lu6 18.9(3) . . . . ?
Lu5 C28 C29 Lu6 24.45(17) . . . . ?
C27 C28 C29 Lu10 -89.7(2) . . . . ?
C49 C28 C29 Lu10 47.6(2) . . . . ?
Lu3 C28 C29 Lu10 -3.9(3) . . . . ?
Lu5 C28 C29 Lu10 5.6(2) . . . . ?
Lu6 C28 C29 Lu10 -18.9(3) . . . . ?
C27 C28 C29 Lu11 -85.8(4) . . . . ?
C49 C28 C29 Lu11 51.5(4) . . . . ?
Lu3 C28 C29 Lu11 0.1(4) . . . . ?
Lu10 C28 C29 Lu11 4.0(4) . . . . ?
Lu5 C28 C29 Lu11 9.5(4) . . . . ?
Lu6 C28 C29 Lu11 -14.9(4) . . . . ?
C27 C28 C29 Lu5 -95.31(10) . . . . ?
C49 C28 C29 Lu5 41.98(10) . . . . ?
Lu3 C28 C29 Lu5 -9.48(18) . . . . ?
Lu10 C28 C29 Lu5 -5.6(2) . . . . ?
Lu6 C28 C29 Lu5 -24.45(17) . . . . ?
C10 C11 C29 C28 -3.3 . . . . ?
C12 C11 C29 C28 -144.4 . . . . ?
Lu6 C11 C29 C28 -101.2(2) . . . . ?
Lu3 C11 C29 C28 -89.89(18) . . . . ?
Lu10 C11 C29 C28 -77.6(3) . . . . ?
C10 C11 C29 C30 140.9 . . . . ?
C12 C11 C29 C30 -0.2 . . . . ?
Lu6 C11 C29 C30 43.0(2) . . . . ?
Lu3 C11 C29 C30 54.34(18) . . . . ?
Lu10 C11 C29 C30 66.6(3) . . . . ?
C10 C11 C29 Lu3 86.54(18) . . . . ?
C12 C11 C29 Lu3 -54.54(18) . . . . ?
Lu6 C11 C29 Lu3 -11.3(3) . . . . ?
Lu10 C11 C29 Lu3 12.3(3) . . . . ?
C10 C11 C29 Lu6 97.9(2) . . . . ?
C12 C11 C29 Lu6 -43.2(2) . . . . ?
Lu3 C11 C29 Lu6 11.3(3) . . . . ?
Lu10 C11 C29 Lu6 23.6(4) . . . . ?
C10 C11 C29 Lu10 74.3(3) . . . . ?
C12 C11 C29 Lu10 -66.8(3) . . . . ?
Lu6 C11 C29 Lu10 -23.6(4) . . . . ?
Lu3 C11 C29 Lu10 -12.3(3) . . . . ?
C10 C11 C29 Lu11 104.1(5) . . . . ?
C12 C11 C29 Lu11 -37.0(5) . . . . ?
Lu6 C11 C29 Lu11 6.2(6) . . . . ?
Lu3 C11 C29 Lu11 17.6(6) . . . . ?
Lu10 C11 C29 Lu11 29.8(6) . . . . ?
C10 C11 C29 Lu5 67.19(10) . . . . ?
C12 C11 C29 Lu5 -73.90(10) . . . . ?
Lu6 C11 C29 Lu5 -30.7(2) . . . . ?
Lu3 C11 C29 Lu5 -19.36(18) . . . . ?
Lu10 C11 C29 Lu5 -7.1(3) . . . . ?
Lu10 Lu3 C29 C28 -14.9(11) . . . . ?
Lu6 Lu3 C29 C28 139.4(7) . . . . ?
Lu11 Lu3 C29 C28 179.9(13) . . . . ?
Lu5 Lu3 C29 C28 -21.1(4) . . . . ?
Lu3 Lu3 C29 C28 130.48(4) 6_565 . . . ?
C30 Lu3 C29 C28 -122.03(15) . . . . ?
Lu2 Lu3 C29 C28 18.1(3) 6_565 . . . ?
C51 Lu3 C29 C28 -88.44(16) . . . . ?
Lu10 Lu3 C29 C28 120.1(4) 6_565 . . . ?
C31 Lu3 C29 C28 -162.50(12) . . . . ?
Lu10 Lu3 C29 C11 -125.0(11) . . . . ?
Lu6 Lu3 C29 C11 29.4(7) . . . . ?
Lu11 Lu3 C29 C11 69.8(13) . . . . ?
Lu5 Lu3 C29 C11 -131.1(4) . . . . ?
Lu3 Lu3 C29 C11 20.43(5) 6_565 . . . ?
C30 Lu3 C29 C11 127.92(14) . . . . ?
Lu2 Lu3 C29 C11 -91.9(3) 6_565 . . . ?
C51 Lu3 C29 C11 161.51(15) . . . . ?
Lu10 Lu3 C29 C11 10.0(4) 6_565 . . . ?
C31 Lu3 C29 C11 87.46(12) . . . . ?
C28 Lu3 C29 C11 -110.0 . . . . ?
Lu10 Lu3 C29 C30 107.1(12) . . . . ?
Lu6 Lu3 C29 C30 -98.5(7) . . . . ?
Lu11 Lu3 C29 C30 -58.1(12) . . . . ?
Lu5 Lu3 C29 C30 100.9(4) . . . . ?
Lu3 Lu3 C29 C30 -107.49(17) 6_565 . . . ?
Lu2 Lu3 C29 C30 140.2(4) 6_565 . . . ?
C51 Lu3 C29 C30 33.58(5) . . . . ?
Lu10 Lu3 C29 C30 -117.9(4) 6_565 . . . ?
C31 Lu3 C29 C30 -40.47(6) . . . . ?
C28 Lu3 C29 C30 122.03(15) . . . . ?
Lu10 Lu3 C29 Lu6 -154.4(14) . . . . ?
Lu11 Lu3 C29 Lu6 40.4(13) . . . . ?
Lu5 Lu3 C29 Lu6 -160.5(9) . . . . ?
Lu3 Lu3 C29 Lu6 -8.9(6) 6_565 . . . ?
C30 Lu3 C29 Lu6 98.5(7) . . . . ?
Lu2 Lu3 C29 Lu6 -121.3(8) 6_565 . . . ?
C51 Lu3 C29 Lu6 132.1(7) . . . . ?
Lu10 Lu3 C29 Lu6 -19.4(7) 6_565 . . . ?
C31 Lu3 C29 Lu6 58.1(7) . . . . ?
C28 Lu3 C29 Lu6 -139.4(7) . . . . ?
Lu6 Lu3 C29 Lu10 154.4(14) . . . . ?
Lu11 Lu3 C29 Lu10 -165.2(19) . . . . ?
Lu5 Lu3 C29 Lu10 -6.1(10) . . . . ?
Lu3 Lu3 C29 Lu10 145.4(11) 6_565 . . . ?
C30 Lu3 C29 Lu10 -107.1(12) . . . . ?
Lu2 Lu3 C29 Lu10 33.1(10) 6_565 . . . ?
C51 Lu3 C29 Lu10 -73.5(12) . . . . ?
Lu10 Lu3 C29 Lu10 135.0(14) 6_565 . . . ?
C31 Lu3 C29 Lu10 -147.6(12) . . . . ?
C28 Lu3 C29 Lu10 14.9(11) . . . . ?
Lu10 Lu3 C29 Lu11 165.2(19) . . . . ?
Lu6 Lu3 C29 Lu11 -40.4(13) . . . . ?
Lu5 Lu3 C29 Lu11 159.1(14) . . . . ?
Lu3 Lu3 C29 Lu11 -49.4(13) 6_565 . . . ?
C30 Lu3 C29 Lu11 58.1(12) . . . . ?
Lu2 Lu3 C29 Lu11 -161.7(14) 6_565 . . . ?
C51 Lu3 C29 Lu11 91.7(12) . . . . ?
Lu10 Lu3 C29 Lu11 -59.8(12) 6_565 . . . ?
C31 Lu3 C29 Lu11 17.7(12) . . . . ?
C28 Lu3 C29 Lu11 -179.9(13) . . . . ?
Lu10 Lu3 C29 Lu5 6.1(10) . . . . ?
Lu6 Lu3 C29 Lu5 160.5(9) . . . . ?
Lu11 Lu3 C29 Lu5 -159.1(14) . . . . ?
Lu3 Lu3 C29 Lu5 151.6(4) 6_565 . . . ?
C30 Lu3 C29 Lu5 -100.9(4) . . . . ?
Lu2 Lu3 C29 Lu5 39.2(3) 6_565 . . . ?
C51 Lu3 C29 Lu5 -67.4(4) . . . . ?
Lu10 Lu3 C29 Lu5 141.1(6) 6_565 . . . ?
C31 Lu3 C29 Lu5 -141.4(4) . . . . ?
C28 Lu3 C29 Lu5 21.1(4) . . . . ?
C28 C29 C30 C51 2.3 . . . . ?
C11 C29 C30 C51 -139.7 . . . . ?
Lu3 C29 C30 C51 -69.6(3) . . . . ?
Lu6 C29 C30 C51 -94.11(17) . . . . ?
Lu10 C29 C30 C51 -54.0(3) . . . . ?
Lu11 C29 C30 C51 -90.0(4) . . . . ?
Lu5 C29 C30 C51 -43.04(10) . . . . ?
C28 C29 C30 C31 152.7 . . . . ?
C11 C29 C30 C31 10.7 . . . . ?
Lu3 C29 C30 C31 80.8(3) . . . . ?
Lu6 C29 C30 C31 56.33(17) . . . . ?
Lu10 C29 C30 C31 96.5(3) . . . . ?
Lu11 C29 C30 C31 60.5(4) . . . . ?
Lu5 C29 C30 C31 107.40(10) . . . . ?
C28 C29 C30 Lu3 71.8(3) . . . . ?
C11 C29 C30 Lu3 -70.2(3) . . . . ?
Lu6 C29 C30 Lu3 -24.5(3) . . . . ?
Lu10 C29 C30 Lu3 15.6(3) . . . . ?
Lu11 C29 C30 Lu3 -20.4(5) . . . . ?
Lu5 C29 C30 Lu3 26.6(3) . . . . ?
C28 C29 C30 Lu6 96.37(17) . . . . ?
C11 C29 C30 Lu6 -45.63(18) . . . . ?
Lu3 C29 C30 Lu6 24.5(3) . . . . ?
Lu10 C29 C30 Lu6 40.2(4) . . . . ?
Lu11 C29 C30 Lu6 4.2(5) . . . . ?
Lu5 C29 C30 Lu6 51.07(19) . . . . ?
C28 C29 C30 Lu10 56.2(3) . . . . ?
C11 C29 C30 Lu10 -85.8(3) . . . . ?
Lu3 C29 C30 Lu10 -15.6(3) . . . . ?
Lu6 C29 C30 Lu10 -40.2(4) . . . . ?
Lu11 C29 C30 Lu10 -36.0(5) . . . . ?
Lu5 C29 C30 Lu10 10.9(3) . . . . ?
C28 C29 C30 Lu11 92.2(4) . . . . ?
C11 C29 C30 Lu11 -49.8(4) . . . . ?
Lu3 C29 C30 Lu11 20.4(5) . . . . ?
Lu6 C29 C30 Lu11 -4.2(5) . . . . ?
Lu10 C29 C30 Lu11 36.0(5) . . . . ?
Lu5 C29 C30 Lu11 46.9(4) . . . . ?
C28 C29 C30 Lu5 45.30(10) . . . . ?
C11 C29 C30 Lu5 -96.71(10) . . . . ?
Lu3 C29 C30 Lu5 -26.6(3) . . . . ?
Lu6 C29 C30 Lu5 -51.07(19) . . . . ?
Lu10 C29 C30 Lu5 -10.9(3) . . . . ?
Lu11 C29 C30 Lu5 -46.9(4) . . . . ?
Lu10 Lu3 C30 C29 -109.0(10) . . . . ?
Lu6 Lu3 C30 C29 88.3(7) . . . . ?
Lu11 Lu3 C30 C29 142.7(8) . . . . ?
Lu5 Lu3 C30 C29 -111.0(4) . . . . ?
Lu3 Lu3 C30 C29 85.00(10) 6_565 . . . ?
Lu2 Lu3 C30 C29 -64.1(5) 6_565 . . . ?
C51 Lu3 C30 C29 -127.67(10) . . . . ?
Lu10 Lu3 C30 C29 90.0(4) 6_565 . . . ?
C31 Lu3 C30 C29 112.56(9) . . . . ?
C28 Lu3 C30 C29 -32.4 . . . . ?
Lu10 Lu3 C30 C51 18.7(10) . . . . ?
Lu6 Lu3 C30 C51 -144.0(7) . . . . ?
Lu11 Lu3 C30 C51 -89.7(8) . . . . ?
Lu5 Lu3 C30 C51 16.7(3) . . . . ?
Lu3 Lu3 C30 C51 -147.34(8) 6_565 . . . ?
Lu2 Lu3 C30 C51 63.6(5) 6_565 . . . ?
C29 Lu3 C30 C51 127.67(10) . . . . ?
Lu10 Lu3 C30 C51 -142.3(4) 6_565 . . . ?
C31 Lu3 C30 C51 -119.8 . . . . ?
C28 Lu3 C30 C51 95.28(13) . . . . ?
Lu10 Lu3 C30 C31 138.5(10) . . . . ?
Lu6 Lu3 C30 C31 -24.2(7) . . . . ?
Lu11 Lu3 C30 C31 30.1(8) . . . . ?
Lu5 Lu3 C30 C31 136.4(4) . . . . ?
Lu3 Lu3 C30 C31 -27.56(6) 6_565 . . . ?
Lu2 Lu3 C30 C31 -176.7(5) 6_565 . . . ?
C29 Lu3 C30 C31 -112.56(9) . . . . ?
C51 Lu3 C30 C31 119.8 . . . . ?
Lu10 Lu3 C30 C31 -22.5(4) 6_565 . . . ?
C28 Lu3 C30 C31 -144.95(12) . . . . ?
Lu10 Lu3 C30 Lu6 162.7(14) . . . . ?
Lu11 Lu3 C30 Lu6 54.3(10) . . . . ?
Lu5 Lu3 C30 Lu6 160.7(9) . . . . ?
Lu3 Lu3 C30 Lu6 -3.3(6) 6_565 . . . ?
Lu2 Lu3 C30 Lu6 -152.4(11) 6_565 . . . ?
C29 Lu3 C30 Lu6 -88.3(7) . . . . ?
C51 Lu3 C30 Lu6 144.0(7) . . . . ?
Lu10 Lu3 C30 Lu6 1.7(6) 6_565 . . . ?
C31 Lu3 C30 Lu6 24.2(7) . . . . ?
C28 Lu3 C30 Lu6 -120.7(7) . . . . ?
Lu6 Lu3 C30 Lu10 -162.7(14) . . . . ?
Lu11 Lu3 C30 Lu10 -108.4(13) . . . . ?
Lu5 Lu3 C30 Lu10 -2.0(9) . . . . ?
Lu3 Lu3 C30 Lu10 -166.0(10) 6_565 . . . ?
Lu2 Lu3 C30 Lu10 44.9(10) 6_565 . . . ?
C29 Lu3 C30 Lu10 109.0(10) . . . . ?
C51 Lu3 C30 Lu10 -18.7(10) . . . . ?
Lu10 Lu3 C30 Lu10 -161.0(14) 6_565 . . . ?
C31 Lu3 C30 Lu10 -138.5(10) . . . . ?
C28 Lu3 C30 Lu10 76.6(10) . . . . ?
Lu10 Lu3 C30 Lu11 108.4(13) . . . . ?
Lu6 Lu3 C30 Lu11 -54.3(10) . . . . ?
Lu5 Lu3 C30 Lu11 106.3(9) . . . . ?
Lu3 Lu3 C30 Lu11 -57.7(8) 6_565 . . . ?
Lu2 Lu3 C30 Lu11 153.2(11) 6_565 . . . ?
C29 Lu3 C30 Lu11 -142.7(8) . . . . ?
C51 Lu3 C30 Lu11 89.7(8) . . . . ?
Lu10 Lu3 C30 Lu11 -52.6(8) 6_565 . . . ?
C31 Lu3 C30 Lu11 -30.1(8) . . . . ?
C28 Lu3 C30 Lu11 -175.1(8) . . . . ?
Lu10 Lu3 C30 Lu5 2.0(9) . . . . ?
Lu6 Lu3 C30 Lu5 -160.7(9) . . . . ?
Lu11 Lu3 C30 Lu5 -106.3(9) . . . . ?
Lu3 Lu3 C30 Lu5 -164.0(4) 6_565 . . . ?
Lu2 Lu3 C30 Lu5 46.9(5) 6_565 . . . ?
C29 Lu3 C30 Lu5 111.0(4) . . . . ?
C51 Lu3 C30 Lu5 -16.7(3) . . . . ?
Lu10 Lu3 C30 Lu5 -158.9(7) 6_565 . . . ?
C31 Lu3 C30 Lu5 -136.4(4) . . . . ?
C28 Lu3 C30 Lu5 78.6(4) . . . . ?
Lu3 Lu6 C30 C29 -85.1(7) . . . . ?
Lu3 Lu6 C30 C29 84.8(13) 6_565 . . . ?
Lu11 Lu6 C30 C29 -171.1(11) . . . . ?
Lu10 Lu6 C30 C29 103(2) 6_565 . . . ?
Lu10 Lu6 C30 C29 -92.6(4) . . . . ?
C31 Lu6 C30 C29 121.59(11) . . . . ?
C13 Lu6 C30 C29 96.11(17) . . . . ?
C12 Lu6 C30 C29 57.70(16) . . . . ?
C11 Lu6 C30 C29 23.92(7) . . . . ?
Lu5 Lu6 C30 C29 127.7(16) 6_565 . . . ?
Lu3 Lu6 C30 C51 36.5(7) . . . . ?
Lu3 Lu6 C30 C51 -153.6(12) 6_565 . . . ?
Lu11 Lu6 C30 C51 -49.5(11) . . . . ?
Lu10 Lu6 C30 C51 -136(2) 6_565 . . . ?
Lu10 Lu6 C30 C51 28.9(5) . . . . ?
C31 Lu6 C30 C51 -116.84(7) . . . . ?
C13 Lu6 C30 C51 -142.32(13) . . . . ?
C12 Lu6 C30 C51 179.27(14) . . . . ?
C29 Lu6 C30 C51 121.6 . . . . ?
C11 Lu6 C30 C51 145.49(9) . . . . ?
Lu5 Lu6 C30 C51 -110.7(16) 6_565 . . . ?
Lu3 Lu6 C30 C31 153.3(7) . . . . ?
Lu3 Lu6 C30 C31 -36.8(12) 6_565 . . . ?
Lu11 Lu6 C30 C31 67.3(11) . . . . ?
Lu10 Lu6 C30 C31 -19(2) 6_565 . . . ?
Lu10 Lu6 C30 C31 145.8(5) . . . . ?
C13 Lu6 C30 C31 -25.48(9) . . . . ?
C12 Lu6 C30 C31 -63.89(15) . . . . ?
C29 Lu6 C30 C31 -121.59(11) . . . . ?
C11 Lu6 C30 C31 -97.67(14) . . . . ?
Lu5 Lu6 C30 C31 6.1(15) 6_565 . . . ?
Lu3 Lu6 C30 Lu3 169.9(19) 6_565 . . . ?
Lu11 Lu6 C30 Lu3 -86.0(13) . . . . ?
Lu10 Lu6 C30 Lu3 -172(3) 6_565 . . . ?
Lu10 Lu6 C30 Lu3 -7.5(6) . . . . ?
C31 Lu6 C30 Lu3 -153.3(7) . . . . ?
C13 Lu6 C30 Lu3 -178.8(8) . . . . ?
C12 Lu6 C30 Lu3 142.8(8) . . . . ?
C29 Lu6 C30 Lu3 85.1(7) . . . . ?
C11 Lu6 C30 Lu3 109.0(7) . . . . ?
Lu5 Lu6 C30 Lu3 -147(2) 6_565 . . . ?
Lu3 Lu6 C30 Lu10 7.5(6) . . . . ?
Lu3 Lu6 C30 Lu10 177.4(15) 6_565 . . . ?
Lu11 Lu6 C30 Lu10 -78.4(11) . . . . ?
Lu10 Lu6 C30 Lu10 -165(3) 6_565 . . . ?
C31 Lu6 C30 Lu10 -145.8(5) . . . . ?
C13 Lu6 C30 Lu10 -171.3(5) . . . . ?
C12 Lu6 C30 Lu10 150.3(6) . . . . ?
C29 Lu6 C30 Lu10 92.6(4) . . . . ?
C11 Lu6 C30 Lu10 116.6(5) . . . . ?
Lu5 Lu6 C30 Lu10 -139.6(18) 6_565 . . . ?
Lu3 Lu6 C30 Lu11 86.0(13) . . . . ?
Lu3 Lu6 C30 Lu11 -104.1(17) 6_565 . . . ?
Lu10 Lu6 C30 Lu11 -86(2) 6_565 . . . ?
Lu10 Lu6 C30 Lu11 78.4(11) . . . . ?
C31 Lu6 C30 Lu11 -67.3(11) . . . . ?
C13 Lu6 C30 Lu11 -92.8(11) . . . . ?
C12 Lu6 C30 Lu11 -131.2(11) . . . . ?
C29 Lu6 C30 Lu11 171.1(11) . . . . ?
C11 Lu6 C30 Lu11 -165.0(11) . . . . ?
Lu5 Lu6 C30 Lu11 -61.2(19) 6_565 . . . ?
Lu3 Lu6 C30 Lu5 11.7(6) . . . . ?
Lu3 Lu6 C30 Lu5 -178.4(14) 6_565 . . . ?
Lu11 Lu6 C30 Lu5 -74.3(11) . . . . ?
Lu10 Lu6 C30 Lu5 -161(2) 6_565 . . . ?
Lu10 Lu6 C30 Lu5 4.1(4) . . . . ?
C31 Lu6 C30 Lu5 -141.6(3) . . . . ?
C13 Lu6 C30 Lu5 -167.1(3) . . . . ?
C12 Lu6 C30 Lu5 154.5(3) . . . . ?
C29 Lu6 C30 Lu5 96.8(2) . . . . ?
C11 Lu6 C30 Lu5 120.7(3) . . . . ?
Lu5 Lu6 C30 Lu5 -135.5(18) 6_565 . . . ?
C12 C13 C31 C32 147.6 . . . . ?
C14 C13 C31 C32 2.5 . . . . ?
Lu6 C13 C31 C32 93.1(2) . . . . ?
Lu11 C13 C31 C32 61.7(7) . . . . ?
Lu3 C13 C31 C32 99.29(12) . . . . ?
C12 C13 C31 C30 7.1 . . . . ?
C14 C13 C31 C30 -138.1 . . . . ?
Lu6 C13 C31 C30 -47.5(2) . . . . ?
Lu11 C13 C31 C30 -78.9(7) . . . . ?
Lu3 C13 C31 C30 -41.29(12) . . . . ?
C12 C13 C31 Lu6 54.6(2) . . . . ?
C14 C13 C31 Lu6 -90.6(2) . . . . ?
Lu11 C13 C31 Lu6 -31.4(8) . . . . ?
Lu3 C13 C31 Lu6 6.2(3) . . . . ?
C12 C13 C31 Lu11 85.9(7) . . . . ?
C14 C13 C31 Lu11 -59.2(7) . . . . ?
Lu6 C13 C31 Lu11 31.4(8) . . . . ?
Lu3 C13 C31 Lu11 37.6(8) . . . . ?
C12 C13 C31 Lu3 48.35(12) . . . . ?
C14 C13 C31 Lu3 -96.79(12) . . . . ?
Lu6 C13 C31 Lu3 -6.2(3) . . . . ?
Lu11 C13 C31 Lu3 -37.6(8) . . . . ?
C12 C13 C31 Lu10 53.8(2) . . . . ?
C14 C13 C31 Lu10 -91.3(2) . . . . ?
Lu6 C13 C31 Lu10 -0.7(3) . . . . ?
Lu11 C13 C31 Lu10 -32.1(8) . . . . ?
Lu3 C13 C31 Lu10 5.5(2) . . . . ?
C29 C30 C31 C32 -150.8 . . . . ?
C51 C30 C31 C32 1.0 . . . . ?
Lu3 C30 C31 C32 -78.7(2) . . . . ?
Lu6 C30 C31 C32 -89.1(2) . . . . ?
Lu10 C30 C31 C32 -67.8(2) . . . . ?
Lu11 C30 C31 C32 -59.4(7) . . . . ?
Lu5 C30 C31 C32 -58.46(13) . . . . ?
C29 C30 C31 C13 -14.4 . . . . ?
C51 C30 C31 C13 137.4 . . . . ?
Lu3 C30 C31 C13 57.7(2) . . . . ?
Lu6 C30 C31 C13 47.3(2) . . . . ?
Lu10 C30 C31 C13 68.6(2) . . . . ?
Lu11 C30 C31 C13 77.0(7) . . . . ?
Lu5 C30 C31 C13 77.89(13) . . . . ?
C29 C30 C31 Lu6 -61.7(2) . . . . ?
C51 C30 C31 Lu6 90.1(2) . . . . ?
Lu3 C30 C31 Lu6 10.4(3) . . . . ?
Lu10 C30 C31 Lu6 21.3(3) . . . . ?
Lu11 C30 C31 Lu6 29.7(7) . . . . ?
Lu5 C30 C31 Lu6 30.6(2) . . . . ?
C29 C30 C31 Lu11 -91.4(7) . . . . ?
C51 C30 C31 Lu11 60.4(7) . . . . ?
Lu3 C30 C31 Lu11 -19.3(7) . . . . ?
Lu6 C30 C31 Lu11 -29.7(7) . . . . ?
Lu10 C30 C31 Lu11 -8.4(7) . . . . ?
Lu5 C30 C31 Lu11 0.9(7) . . . . ?
C29 C30 C31 Lu3 -72.1(2) . . . . ?
C51 C30 C31 Lu3 79.7(2) . . . . ?
Lu6 C30 C31 Lu3 -10.4(3) . . . . ?
Lu10 C30 C31 Lu3 10.9(3) . . . . ?
Lu11 C30 C31 Lu3 19.3(7) . . . . ?
Lu5 C30 C31 Lu3 20.2(2) . . . . ?
C29 C30 C31 Lu10 -83.0(2) . . . . ?
C51 C30 C31 Lu10 68.8(2) . . . . ?
Lu3 C30 C31 Lu10 -10.9(3) . . . . ?
Lu6 C30 C31 Lu10 -21.3(3) . . . . ?
Lu11 C30 C31 Lu10 8.4(7) . . . . ?
Lu5 C30 C31 Lu10 9.3(3) . . . . ?
Lu3 Lu6 C31 C32 94.0(7) . . . . ?
Lu3 Lu6 C31 C32 -86.4(7) 6_565 . . . ?
Lu11 Lu6 C31 C32 3.18(12) . . . . ?
Lu10 Lu6 C31 C32 -70.0(6) 6_565 . . . ?
Lu10 Lu6 C31 C32 78.9(5) . . . . ?
C13 Lu6 C31 C32 -102.69(7) . . . . ?
C30 Lu6 C31 C32 116.01(6) . . . . ?
C12 Lu6 C31 C32 -133.00(10) . . . . ?
C29 Lu6 C31 C32 151.33(7) . . . . ?
C11 Lu6 C31 C32 -171.55(6) . . . . ?
Lu5 Lu6 C31 C32 -62.4(3) 6_565 . . . ?
Lu3 Lu6 C31 C13 -163.3(7) . . . . ?
Lu3 Lu6 C31 C13 16.3(6) 6_565 . . . ?
Lu11 Lu6 C31 C13 105.87(14) . . . . ?
Lu10 Lu6 C31 C13 32.7(6) 6_565 . . . ?
Lu10 Lu6 C31 C13 -178.4(6) . . . . ?
C30 Lu6 C31 C13 -141.30(13) . . . . ?
C12 Lu6 C31 C13 -30.3 . . . . ?
C29 Lu6 C31 C13 -105.98(14) . . . . ?
C11 Lu6 C31 C13 -68.86(9) . . . . ?
Lu5 Lu6 C31 C13 40.3(3) 6_565 . . . ?
Lu3 Lu6 C31 C30 -22.0(6) . . . . ?
Lu3 Lu6 C31 C30 157.6(8) 6_565 . . . ?
Lu11 Lu6 C31 C30 -112.84(14) . . . . ?
Lu10 Lu6 C31 C30 174.0(6) 6_565 . . . ?
Lu10 Lu6 C31 C30 -37.1(5) . . . . ?
C13 Lu6 C31 C30 141.30(13) . . . . ?
C12 Lu6 C31 C30 110.98(16) . . . . ?
C29 Lu6 C31 C30 35.3 . . . . ?
C11 Lu6 C31 C30 72.44(10) . . . . ?
Lu5 Lu6 C31 C30 -178.4(4) 6_565 . . . ?
Lu3 Lu6 C31 Lu11 90.8(7) . . . . ?
Lu3 Lu6 C31 Lu11 -89.6(7) 6_565 . . . ?
Lu10 Lu6 C31 Lu11 -73.1(6) 6_565 . . . ?
Lu10 Lu6 C31 Lu11 75.7(5) . . . . ?
C13 Lu6 C31 Lu11 -105.87(14) . . . . ?
C30 Lu6 C31 Lu11 112.84(14) . . . . ?
C12 Lu6 C31 Lu11 -136.18(16) . . . . ?
C29 Lu6 C31 Lu11 148.15(15) . . . . ?
C11 Lu6 C31 Lu11 -174.72(14) . . . . ?
Lu5 Lu6 C31 Lu11 -65.6(4) 6_565 . . . ?
Lu3 Lu6 C31 Lu3 179.6(14) 6_565 . . . ?
Lu11 Lu6 C31 Lu3 -90.8(7) . . . . ?
Lu10 Lu6 C31 Lu3 -164.0(11) 6_565 . . . ?
Lu10 Lu6 C31 Lu3 -15.1(5) . . . . ?
C13 Lu6 C31 Lu3 163.3(7) . . . . ?
C30 Lu6 C31 Lu3 22.0(6) . . . . ?
C12 Lu6 C31 Lu3 133.0(7) . . . . ?
C29 Lu6 C31 Lu3 57.3(6) . . . . ?
C11 Lu6 C31 Lu3 94.4(7) . . . . ?
Lu5 Lu6 C31 Lu3 -156.4(10) 6_565 . . . ?
Lu3 Lu6 C31 Lu10 15.1(5) . . . . ?
Lu3 Lu6 C31 Lu10 -165.3(11) 6_565 . . . ?
Lu11 Lu6 C31 Lu10 -75.7(5) . . . . ?
Lu10 Lu6 C31 Lu10 -148.9(11) 6_565 . . . ?
C13 Lu6 C31 Lu10 178.4(6) . . . . ?
C30 Lu6 C31 Lu10 37.1(5) . . . . ?
C12 Lu6 C31 Lu10 148.1(6) . . . . ?
C29 Lu6 C31 Lu10 72.4(5) . . . . ?
C11 Lu6 C31 Lu10 109.6(5) . . . . ?
Lu5 Lu6 C31 Lu10 -141.3(8) 6_565 . . . ?
C13 C31 C32 C33 -1.2 . . . . ?
C30 C31 C32 C33 143.8 . . . . ?
Lu6 C31 C32 C33 70.87(10) . . . . ?
Lu11 C31 C32 C33 72.75(12) . . . . ?
Lu3 C31 C32 C33 93.15(18) . . . . ?
Lu10 C31 C32 C33 98.05(19) . . . . ?
C13 C31 C32 C53 -141.1 . . . . ?
C30 C31 C32 C53 3.9 . . . . ?
Lu6 C31 C32 C53 -69.06(10) . . . . ?
Lu11 C31 C32 C53 -67.18(12) . . . . ?
Lu3 C31 C32 C53 -46.78(18) . . . . ?
Lu10 C31 C32 C53 -41.89(19) . . . . ?
C13 C31 C32 Lu11 -73.96(12) . . . . ?
C30 C31 C32 Lu11 71.09(12) . . . . ?
Lu6 C31 C32 Lu11 -1.88(7) . . . . ?
Lu3 C31 C32 Lu11 20.40(18) . . . . ?
Lu10 C31 C32 Lu11 25.3(2) . . . . ?
C13 C31 C32 Lu6 -72.09(10) . . . . ?
C30 C31 C32 Lu6 72.97(10) . . . . ?
Lu11 C31 C32 Lu6 1.88(7) . . . . ?
Lu3 C31 C32 Lu6 22.28(17) . . . . ?
Lu10 C31 C32 Lu6 27.2(2) . . . . ?
C13 C31 C32 Lu3 -94.36(18) . . . . ?
C30 C31 C32 Lu3 50.69(19) . . . . ?
Lu6 C31 C32 Lu3 -22.28(17) . . . . ?
Lu11 C31 C32 Lu3 -20.40(18) . . . . ?
Lu10 C31 C32 Lu3 4.9(3) . . . . ?
Lu6 Lu11 C32 C33 -110.22(18) . . . . ?
Lu3 Lu11 C32 C33 -147.1(11) . . . . ?
Lu3 Lu11 C32 C33 -73.3(8) 6_565 . . . ?
Lu10 Lu11 C32 C33 -48.4(15) 6_565 . . . ?
Lu10 Lu11 C32 C33 -172.1(17) . . . . ?
C31 Lu11 C32 C33 -113.52(16) . . . . ?
C53 Lu11 C32 C33 118.9(3) . . . . ?
Lu5 Lu11 C32 C33 166.6(16) . . . . ?
Lu5 Lu11 C32 C33 -26.2(15) 6_565 . . . ?
C13 Lu11 C32 C33 -73.83(7) . . . . ?
Lu6 Lu11 C32 C53 130.90(13) . . . . ?
Lu3 Lu11 C32 C53 94.0(8) . . . . ?
Lu3 Lu11 C32 C53 167.8(11) 6_565 . . . ?
Lu10 Lu11 C32 C53 -167.3(17) 6_565 . . . ?
Lu10 Lu11 C32 C53 69.0(15) . . . . ?
C31 Lu11 C32 C53 127.60(10) . . . . ?
C33 Lu11 C32 C53 -118.9(2) . . . . ?
Lu5 Lu11 C32 C53 47.7(14) . . . . ?
Lu5 Lu11 C32 C53 -145.0(17) 6_565 . . . ?
C13 Lu11 C32 C53 167.3(3) . . . . ?
Lu6 Lu11 C32 C31 3.30(7) . . . . ?
Lu3 Lu11 C32 C31 -33.6(9) . . . . ?
Lu3 Lu11 C32 C31 40.2(10) 6_565 . . . ?
Lu10 Lu11 C32 C31 65.1(17) 6_565 . . . ?
Lu10 Lu11 C32 C31 -58.6(15) . . . . ?
C33 Lu11 C32 C31 113.52(16) . . . . ?
C53 Lu11 C32 C31 -127.60(10) . . . . ?
Lu5 Lu11 C32 C31 -79.9(14) . . . . ?
Lu5 Lu11 C32 C31 87.4(16) 6_565 . . . ?
C13 Lu11 C32 C31 39.7(2) . . . . ?
Lu3 Lu11 C32 Lu6 -36.9(9) . . . . ?
Lu3 Lu11 C32 Lu6 36.9(10) 6_565 . . . ?
Lu10 Lu11 C32 Lu6 61.8(17) 6_565 . . . ?
Lu10 Lu11 C32 Lu6 -61.9(15) . . . . ?
C31 Lu11 C32 Lu6 -3.30(7) . . . . ?
C33 Lu11 C32 Lu6 110.22(18) . . . . ?
C53 Lu11 C32 Lu6 -130.90(13) . . . . ?
Lu5 Lu11 C32 Lu6 -83.2(14) . . . . ?
Lu5 Lu11 C32 Lu6 84.0(16) 6_565 . . . ?
C13 Lu11 C32 Lu6 36.4(2) . . . . ?
Lu6 Lu11 C32 Lu3 36.9(9) . . . . ?
Lu3 Lu11 C32 Lu3 73.8(19) 6_565 . . . ?
Lu10 Lu11 C32 Lu3 99(3) 6_565 . . . ?
Lu10 Lu11 C32 Lu3 -25.1(7) . . . . ?
C31 Lu11 C32 Lu3 33.6(9) . . . . ?
C33 Lu11 C32 Lu3 147.1(11) . . . . ?
C53 Lu11 C32 Lu3 -94.0(8) . . . . ?
Lu5 Lu11 C32 Lu3 -46.4(6) . . . . ?
Lu5 Lu11 C32 Lu3 121(3) 6_565 . . . ?
C13 Lu11 C32 Lu3 73.2(11) . . . . ?
C15 C14 C33 C34 -2.7 . . . . ?
C13 C14 C33 C34 146.0 . . . . ?
Lu11 C14 C33 C34 88.0(6) . . . . ?
Lu6 C14 C33 C34 100.47(16) . . . . ?
C15 C14 C33 C32 -146.7 . . . . ?
C13 C14 C33 C32 2.0 . . . . ?
Lu11 C14 C33 C32 -56.0(6) . . . . ?
Lu6 C14 C33 C32 -43.53(16) . . . . ?
C15 C14 C33 Lu11 -90.7(6) . . . . ?
C13 C14 C33 Lu11 58.0(6) . . . . ?
Lu6 C14 C33 Lu11 12.5(7) . . . . ?
C15 C14 C33 Lu6 -103.13(16) . . . . ?
C13 C14 C33 Lu6 45.50(16) . . . . ?
Lu11 C14 C33 Lu6 -12.5(7) . . . . ?
C53 C32 C33 C34 6.3 . . . . ?
C31 C32 C33 C34 -136.4 . . . . ?
Lu11 C32 C33 C34 -67.1(8) . . . . ?
Lu6 C32 C33 C34 -90.87(16) . . . . ?
Lu3 C32 C33 C34 -83.09(14) . . . . ?
C53 C32 C33 C14 142.2 . . . . ?
C31 C32 C33 C14 -0.5 . . . . ?
Lu11 C32 C33 C14 68.8(8) . . . . ?
Lu6 C32 C33 C14 45.05(16) . . . . ?
Lu3 C32 C33 C14 52.83(14) . . . . ?
C53 C32 C33 Lu11 73.4(8) . . . . ?
C31 C32 C33 Lu11 -69.3(8) . . . . ?
Lu6 C32 C33 Lu11 -23.8(8) . . . . ?
Lu3 C32 C33 Lu11 -16.0(8) . . . . ?
C53 C32 C33 Lu6 97.20(16) . . . . ?
C31 C32 C33 Lu6 -45.53(16) . . . . ?
Lu11 C32 C33 Lu6 23.8(8) . . . . ?
Lu3 C32 C33 Lu6 7.8(2) . . . . ?
C14 C33 C34 C35 2.9 . . . . ?
C32 C33 C34 C35 139.1 . . . . ?
Lu11 C33 C34 C35 84.9(5) . . . . ?
Lu6 C33 C34 C35 71.74(9) . . . . ?
C14 C33 C34 C55 -145.1 . . . . ?
C32 C33 C34 C55 -8.9 . . . . ?
Lu11 C33 C34 C55 -63.2(5) . . . . ?
Lu6 C33 C34 C55 -76.28(9) . . . . ?
C14 C33 C34 Lu11 -82.0(5) . . . . ?
C32 C33 C34 Lu11 54.2(5) . . . . ?
Lu6 C33 C34 Lu11 -13.1(5) . . . . ?
C33 C34 C35 C36 -148.5 . . . . ?
C55 C34 C35 C36 1.6 . . . . ?
Lu11 C34 C35 C36 -86.9(5) . . . . ?
C33 C34 C35 C16 -3.9 . . . . ?
C55 C34 C35 C16 146.2 . . . . ?
Lu11 C34 C35 C16 57.7(5) . . . . ?
C15 C16 C35 C34 5.0 . . . . ?
C17 C16 C35 C34 -149.9 . . . . ?
Lu1 C16 C35 C34 -88.31(7) . . . . ?
C15 C16 C35 C36 141.1 . . . . ?
C17 C16 C35 C36 -13.7 . . . . ?
Lu1 C16 C35 C36 47.88(7) . . . . ?
C34 C35 C36 C37 144.7 . . . . ?
C16 C35 C36 C37 7.5 . . . . ?
C34 C35 C36 C56 -2.9 . . . . ?
C16 C35 C36 C56 -140.1 . . . . ?
C35 C36 C37 C59 -148.0 . . . . ?
C56 C36 C37 C59 -3.1 . . . . ?
C35 C36 C37 C38 0.8 . . . . ?
C56 C36 C37 C38 145.7 . . . . ?
C18 C17 C38 C39 -4.4 . . . . ?
C16 C17 C38 C39 142.0 . . . . ?
C19 C17 C38 C39 -2.6 . . . . ?
Lu1 C17 C38 C39 55.97(8) . . . . ?
Lu2 C17 C38 C39 57.0 . . . . ?
C18 C17 C38 C37 -153.6 . . . . ?
C16 C17 C38 C37 -7.3 . . . . ?
C19 C17 C38 C37 -151.9 . . . . ?
Lu1 C17 C38 C37 -93.28(8) . . . . ?
Lu2 C17 C38 C37 -92.3 . . . . ?
C18 C17 C38 C19 -1.7 . . . . ?
C16 C17 C38 C19 144.6 . . . . ?
Lu1 C17 C38 C19 58.60(8) . . . . ?
Lu2 C17 C38 C19 59.6 . . . . ?
C16 C17 C38 C18 146.3 . . . . ?
C19 C17 C38 C18 1.7 . . . . ?
Lu1 C17 C38 C18 60.34(8) . . . . ?
Lu2 C17 C38 C18 61.3 . . . . ?
C18 C17 C38 Lu1 -60.34(8) . . . . ?
C16 C17 C38 Lu1 86.01(8) . . . . ?
C19 C17 C38 Lu1 -58.60(8) . . . . ?
Lu2 C17 C38 Lu1 1.00(6) . . . . ?
C36 C37 C38 C39 -148.1 . . . . ?
C59 C37 C38 C39 -2.3 . . . . ?
C36 C37 C38 C17 -0.8 . . . . ?
C59 C37 C38 C17 145.0 . . . . ?
C36 C37 C38 C19 -118.2 . . . . ?
C59 C37 C38 C19 27.6 . . . . ?
C36 C37 C38 C18 -36.5 . . . . ?
C59 C37 C38 C18 109.3 . . . . ?
C36 C37 C38 Lu1 -71.25(8) . . . . ?
C59 C37 C38 Lu1 74.57(8) . . . . ?
C17 C38 C39 C19 4.2 . . . . ?
C37 C38 C39 C19 155.1 . . . . ?
C18 C38 C39 C19 1.5 . . . . ?
Lu1 C38 C39 C19 56.80(6) . . . . ?
C17 C38 C39 C40 -148.2 . . . . ?
C37 C38 C39 C40 2.7 . . . . ?
C19 C38 C39 C40 -152.4 . . . . ?
C18 C38 C39 C40 -150.9 . . . . ?
Lu1 C38 C39 C40 -95.60(6) . . . . ?
C17 C38 C39 C18 2.7 . . . . ?
C37 C38 C39 C18 153.7 . . . . ?
C19 C38 C39 C18 -1.5 . . . . ?
Lu1 C38 C39 C18 55.35(6) . . . . ?
C17 C38 C39 Lu1 -52.61(6) . . . . ?
C37 C38 C39 Lu1 98.34(6) . . . . ?
C19 C38 C39 Lu1 -56.80(6) . . . . ?
C18 C38 C39 Lu1 -55.35(6) . . . . ?
C20 C19 C39 C38 -143.2 . . . . ?
C18 C19 C39 C38 -2.3 . . . . ?
C17 C19 C39 C38 -2.5 . . . . ?
Lu1 C19 C39 C38 -68.44(8) . . . . ?
Lu2 C19 C39 C38 -73.6 . . . . ?
C20 C19 C39 C40 8.8 . . . . ?
C18 C19 C39 C40 149.8 . . . . ?
C38 C19 C39 C40 152.1 . . . . ?
C17 C19 C39 C40 149.6 . . . . ?
Lu1 C19 C39 C40 83.64(8) . . . . ?
Lu2 C19 C39 C40 78.5 . . . . ?
C20 C19 C39 C18 -140.9 . . . . ?
C38 C19 C39 C18 2.3 . . . . ?
C17 C19 C39 C18 -0.2 . . . . ?
Lu1 C19 C39 C18 -66.11(8) . . . . ?
Lu2 C19 C39 C18 -71.3 . . . . ?
C20 C19 C39 Lu1 -74.80(8) . . . . ?
C18 C19 C39 Lu1 66.11(8) . . . . ?
C38 C19 C39 Lu1 68.44(8) . . . . ?
C17 C19 C39 Lu1 65.92(8) . . . . ?
Lu2 C19 C39 Lu1 -5.17(8) . . . . ?
C38 C39 C40 C60 -4.6 . . . . ?
C19 C39 C40 C60 -152.0 . . . . ?
C18 C39 C40 C60 -114.5 . . . . ?
Lu1 C39 C40 C60 -88.64(6) . . . . ?
C38 C39 C40 C41 143.1 . . . . ?
C19 C39 C40 C41 -4.2 . . . . ?
C18 C39 C40 C41 33.3 . . . . ?
Lu1 C39 C40 C41 59.10(6) . . . . ?
C38 C39 C40 Lu7 77.0(7) . . . . ?
C19 C39 C40 Lu7 -70.3(7) . . . . ?
C18 C39 C40 Lu7 -32.8(7) . . . . ?
Lu1 C39 C40 Lu7 -7.0(7) . . . . ?
C38 C39 C40 Lu4 69.99(9) . . . . ?
C19 C39 C40 Lu4 -77.34(9) . . . . ?
C18 C39 C40 Lu4 -39.84(9) . . . . ?
Lu1 C39 C40 Lu4 -14.01(11) . . . . ?
C38 C39 C40 Lu1 84.01(6) . . . . ?
C19 C39 C40 Lu1 -63.33(6) . . . . ?
C18 C39 C40 Lu1 -25.82(6) . . . . ?
C60 C40 C41 C42 3.3 . . . . ?
C39 C40 C41 C42 -145.8 . . . . ?
Lu7 C40 C41 C42 -48.9(4) . . . . ?
Lu4 C40 C41 C42 -42.99(11) . . . . ?
Lu1 C40 C41 C42 -103.09(5) . . . . ?
C60 C40 C41 C21 148.8 . . . . ?
C39 C40 C41 C21 -0.2 . . . . ?
Lu7 C40 C41 C21 96.7(4) . . . . ?
Lu4 C40 C41 C21 102.60(11) . . . . ?
Lu1 C40 C41 C21 42.49(5) . . . . ?
C60 C40 C41 Lu7 52.1(4) . . . . ?
C39 C40 C41 Lu7 -96.9(4) . . . . ?
Lu4 C40 C41 Lu7 5.9(4) . . . . ?
Lu1 C40 C41 Lu7 -54.2(4) . . . . ?
C60 C40 C41 Lu4 46.24(11) . . . . ?
C39 C40 C41 Lu4 -102.77(11) . . . . ?
Lu7 C40 C41 Lu4 -5.9(4) . . . . ?
Lu1 C40 C41 Lu4 -60.10(11) . . . . ?
C60 C40 C41 Lu8 66.92(11) . . . . ?
C39 C40 C41 Lu8 -82.09(11) . . . . ?
Lu7 C40 C41 Lu8 14.8(4) . . . . ?
Lu4 C40 C41 Lu8 20.69(15) . . . . ?
Lu1 C40 C41 Lu8 -39.42(11) . . . . ?
C60 C40 C41 Lu9 45.4(3) . . . . ?
C39 C40 C41 Lu9 -103.6(3) . . . . ?
Lu7 C40 C41 Lu9 -6.7(6) . . . . ?
Lu4 C40 C41 Lu9 -0.8(4) . . . . ?
Lu1 C40 C41 Lu9 -60.9(3) . . . . ?
C22 C21 C41 C42 5.1 . . . . ?
C20 C21 C41 C42 147.6 . . . . ?
Lu7 C21 C41 C42 60.8(6) . . . . ?
Lu1 C21 C41 C42 100.19(6) . . . . ?
Lu8 C21 C41 C42 49.52(12) . . . . ?
C22 C21 C41 C40 -142.2 . . . . ?
C20 C21 C41 C40 0.3 . . . . ?
Lu7 C21 C41 C40 -86.5(6) . . . . ?
Lu1 C21 C41 C40 -47.11(6) . . . . ?
Lu8 C21 C41 C40 -97.78(12) . . . . ?
C22 C21 C41 Lu7 -55.7(6) . . . . ?
C20 C21 C41 Lu7 86.8(6) . . . . ?
Lu1 C21 C41 Lu7 39.4(6) . . . . ?
Lu8 C21 C41 Lu7 -11.3(6) . . . . ?
C22 C21 C41 Lu4 -54.26(12) . . . . ?
C20 C21 C41 Lu4 88.24(12) . . . . ?
Lu7 C21 C41 Lu4 1.5(6) . . . . ?
Lu1 C21 C41 Lu4 40.81(12) . . . . ?
Lu8 C21 C41 Lu4 -9.86(16) . . . . ?
C22 C21 C41 Lu8 -44.40(12) . . . . ?
C20 C21 C41 Lu8 98.10(12) . . . . ?
Lu7 C21 C41 Lu8 11.3(6) . . . . ?
Lu1 C21 C41 Lu8 50.67(13) . . . . ?
C22 C21 C41 Lu9 -55.3(5) . . . . ?
C20 C21 C41 Lu9 87.2(5) . . . . ?
Lu7 C21 C41 Lu9 0.4(8) . . . . ?
Lu1 C21 C41 Lu9 39.7(5) . . . . ?
Lu8 C21 C41 Lu9 -10.9(5) . . . . ?
C40 C41 C42 C43 133.7 . . . . ?
C21 C41 C42 C43 -7.2 . . . . ?
Lu7 C41 C42 C43 74.6(7) . . . . ?
Lu4 C41 C42 C43 79.63(9) . . . . ?
Lu8 C41 C42 C43 50.20(13) . . . . ?
Lu9 C41 C42 C43 81.4(5) . . . . ?
C40 C41 C42 C62 -2.1 . . . . ?
C21 C41 C42 C62 -143.0 . . . . ?
Lu7 C41 C42 C62 -61.2(7) . . . . ?
Lu4 C41 C42 C62 -56.18(9) . . . . ?
Lu8 C41 C42 C62 -85.61(13) . . . . ?
Lu9 C41 C42 C62 -54.4(5) . . . . ?
C40 C41 C42 Lu7 59.1(7) . . . . ?
C21 C41 C42 Lu7 -81.8(7) . . . . ?
Lu4 C41 C42 Lu7 5.0(8) . . . . ?
Lu8 C41 C42 Lu7 -24.4(7) . . . . ?
Lu9 C41 C42 Lu7 6.8(9) . . . . ?
C40 C41 C42 Lu4 54.10(9) . . . . ?
C21 C41 C42 Lu4 -86.85(9) . . . . ?
Lu7 C41 C42 Lu4 -5.0(8) . . . . ?
Lu8 C41 C42 Lu4 -29.43(16) . . . . ?
Lu9 C41 C42 Lu4 1.7(5) . . . . ?
C40 C41 C42 Lu9 52.4(5) . . . . ?
C21 C41 C42 Lu9 -88.6(5) . . . . ?
Lu7 C41 C42 Lu9 -6.8(9) . . . . ?
Lu4 C41 C42 Lu9 -1.7(5) . . . . ?
Lu8 C41 C42 Lu9 -31.2(5) . . . . ?
C40 C41 C42 Lu8 83.53(13) . . . . ?
C21 C41 C42 Lu8 -57.42(13) . . . . ?
Lu7 C41 C42 Lu8 24.4(7) . . . . ?
Lu4 C41 C42 Lu8 29.43(16) . . . . ?
Lu9 C41 C42 Lu8 31.2(5) . . . . ?
Lu4 Lu7 C42 C41 -34(3) 6_565 . . . ?
Lu9 Lu7 C42 C41 -155(3) . . . . ?
Lu9 Lu7 C42 C41 -30(2) 6_565 . . . ?
Lu8 Lu7 C42 C41 53.8(8) 6_565 . . . ?
Lu8 Lu7 C42 C41 108.7(7) . . . . ?
C62 Lu7 C42 C41 -126.1(3) . . . . ?
C43 Lu7 C42 C41 124.87(16) . . . . ?
C61 Lu7 C42 C41 -93.48(14) . . . . ?
C63 Lu7 C42 C41 -163.1(4) . . . . ?
C44 Lu7 C42 C41 156.3(4) . . . . ?
Lu4 Lu7 C42 C43 -159(3) 6_565 . . . ?
Lu9 Lu7 C42 C43 80(3) . . . . ?
Lu9 Lu7 C42 C43 -155(2) 6_565 . . . ?
Lu8 Lu7 C42 C43 -71.1(9) 6_565 . . . ?
Lu8 Lu7 C42 C43 -16.1(5) . . . . ?
C62 Lu7 C42 C43 109.01(12) . . . . ?
C41 Lu7 C42 C43 -124.87(16) . . . . ?
C61 Lu7 C42 C43 141.65(11) . . . . ?
C63 Lu7 C42 C43 72.1(3) . . . . ?
C44 Lu7 C42 C43 31.5(2) . . . . ?
Lu4 Lu7 C42 C62 92(3) 6_565 . . . ?
Lu9 Lu7 C42 C62 -29(3) . . . . ?
Lu9 Lu7 C42 C62 96(2) 6_565 . . . ?
Lu8 Lu7 C42 C62 179.9(10) 6_565 . . . ?
Lu8 Lu7 C42 C62 -125.2(5) . . . . ?
C43 Lu7 C42 C62 -109.01(12) . . . . ?
C41 Lu7 C42 C62 126.1(3) . . . . ?
C61 Lu7 C42 C62 32.64(14) . . . . ?
C63 Lu7 C42 C62 -36.94(18) . . . . ?
C44 Lu7 C42 C62 -77.54(15) . . . . ?
Lu4 Lu7 C42 Lu4 119(6) 6_565 . . . ?
Lu9 Lu7 C42 Lu4 -2(2) . . . . ?
Lu9 Lu7 C42 Lu4 124(5) 6_565 . . . ?
Lu8 Lu7 C42 Lu4 -153(4) 6_565 . . . ?
Lu8 Lu7 C42 Lu4 -98(3) . . . . ?
C62 Lu7 C42 Lu4 27(3) . . . . ?
C43 Lu7 C42 Lu4 -82(4) . . . . ?
C41 Lu7 C42 Lu4 153(4) . . . . ?
C61 Lu7 C42 Lu4 60(4) . . . . ?
C63 Lu7 C42 Lu4 -10(3) . . . . ?
C44 Lu7 C42 Lu4 -50(3) . . . . ?
Lu4 Lu7 C42 Lu9 121(5) 6_565 . . . ?
Lu9 Lu7 C42 Lu9 126(5) 6_565 . . . ?
Lu8 Lu7 C42 Lu9 -151(4) 6_565 . . . ?
Lu8 Lu7 C42 Lu9 -96(3) . . . . ?
C62 Lu7 C42 Lu9 29(3) . . . . ?
C43 Lu7 C42 Lu9 -80(3) . . . . ?
C41 Lu7 C42 Lu9 155(3) . . . . ?
C61 Lu7 C42 Lu9 62(3) . . . . ?
C63 Lu7 C42 Lu9 -8(3) . . . . ?
C44 Lu7 C42 Lu9 -48(3) . . . . ?
Lu4 Lu7 C42 Lu8 -143(3) 6_565 . . . ?
Lu9 Lu7 C42 Lu8 96(3) . . . . ?
Lu9 Lu7 C42 Lu8 -139(3) 6_565 . . . ?
Lu8 Lu7 C42 Lu8 -55.0(13) 6_565 . . . ?
C62 Lu7 C42 Lu8 125.2(5) . . . . ?
C43 Lu7 C42 Lu8 16.1(5) . . . . ?
C41 Lu7 C42 Lu8 -108.7(7) . . . . ?
C61 Lu7 C42 Lu8 157.8(6) . . . . ?
C63 Lu7 C42 Lu8 88.2(4) . . . . ?
C44 Lu7 C42 Lu8 47.6(4) . . . . ?
C41 C42 C43 C23 6.1 . . . . ?
C62 C42 C43 C23 147.7 . . . . ?
Lu7 C42 C43 C23 81.7(4) . . . . ?
Lu4 C42 C43 C23 93.01(18) . . . . ?
Lu9 C42 C43 C23 98.0(4) . . . . ?
Lu8 C42 C43 C23 73.30(15) . . . . ?
C41 C42 C43 C44 -135.1 . . . . ?
C62 C42 C43 C44 6.5 . . . . ?
Lu7 C42 C43 C44 -59.5(4) . . . . ?
Lu4 C42 C43 C44 -48.17(18) . . . . ?
Lu9 C42 C43 C44 -43.2(4) . . . . ?
Lu8 C42 C43 C44 -67.88(15) . . . . ?
C41 C42 C43 Lu7 -75.6(4) . . . . ?
C62 C42 C43 Lu7 66.0(4) . . . . ?
Lu4 C42 C43 Lu7 11.3(4) . . . . ?
Lu9 C42 C43 Lu7 16.4(6) . . . . ?
Lu8 C42 C43 Lu7 -8.4(4) . . . . ?
C41 C42 C43 Lu8 -67.21(15) . . . . ?
C62 C42 C43 Lu8 74.40(15) . . . . ?
Lu7 C42 C43 Lu8 8.4(4) . . . . ?
Lu4 C42 C43 Lu8 19.7(2) . . . . ?
Lu9 C42 C43 Lu8 24.7(4) . . . . ?
C41 C42 C43 Lu4 -86.92(18) . . . . ?
C62 C42 C43 Lu4 54.68(18) . . . . ?
Lu7 C42 C43 Lu4 -11.3(4) . . . . ?
Lu9 C42 C43 Lu4 5.0(5) . . . . ?
Lu8 C42 C43 Lu4 -19.7(2) . . . . ?
C41 C42 C43 Lu9 -91.9(4) . . . . ?
C62 C42 C43 Lu9 49.7(4) . . . . ?
Lu7 C42 C43 Lu9 -16.4(6) . . . . ?
Lu4 C42 C43 Lu9 -5.0(5) . . . . ?
Lu8 C42 C43 Lu9 -24.7(4) . . . . ?
C22 C23 C43 C42 -3.5 . . . . ?
C24 C23 C43 C42 -148.0 . . . . ?
Lu8 C23 C43 C42 -85.85(17) . . . . ?
Lu7 C23 C43 C42 -59.8(2) . . . . ?
Lu4 C23 C43 C42 -68.0(2) . . . . ?
C22 C23 C43 C44 135.8 . . . . ?
C24 C23 C43 C44 -8.7 . . . . ?
Lu8 C23 C43 C44 53.46(17) . . . . ?
Lu7 C23 C43 C44 79.5(2) . . . . ?
Lu4 C23 C43 C44 71.3(2) . . . . ?
C22 C23 C43 Lu7 56.3(2) . . . . ?
C24 C23 C43 Lu7 -88.2(2) . . . . ?
Lu8 C23 C43 Lu7 -26.0(3) . . . . ?
Lu4 C23 C43 Lu7 -8.2(3) . . . . ?
C22 C23 C43 Lu8 82.30(17) . . . . ?
C24 C23 C43 Lu8 -62.15(17) . . . . ?
Lu7 C23 C43 Lu8 26.0(3) . . . . ?
Lu4 C23 C43 Lu8 17.8(3) . . . . ?
C22 C23 C43 Lu4 64.5(2) . . . . ?
C24 C23 C43 Lu4 -80.0(2) . . . . ?
Lu8 C23 C43 Lu4 -17.8(3) . . . . ?
Lu7 C23 C43 Lu4 8.2(3) . . . . ?
C22 C23 C43 Lu9 71.9(4) . . . . ?
C24 C23 C43 Lu9 -72.5(4) . . . . ?
Lu8 C23 C43 Lu9 -10.4(5) . . . . ?
Lu7 C23 C43 Lu9 15.7(5) . . . . ?
Lu4 C23 C43 Lu9 7.4(5) . . . . ?
C42 C43 C44 C45 140.2 . . . . ?
C23 C43 C44 C45 1.8 . . . . ?
Lu7 C43 C44 C45 90.3(5) . . . . ?
Lu8 C43 C44 C45 57.49(16) . . . . ?
Lu4 C43 C44 C45 93.26(11) . . . . ?
Lu9 C43 C44 C45 92.0(4) . . . . ?
C42 C43 C44 C63 -9.3 . . . . ?
C23 C43 C44 C63 -147.7 . . . . ?
Lu7 C43 C44 C63 -59.2(5) . . . . ?
Lu8 C43 C44 C63 -91.99(17) . . . . ?
Lu4 C43 C44 C63 -56.22(11) . . . . ?
Lu9 C43 C44 C63 -57.4(4) . . . . ?
C42 C43 C44 C66 106.7 . . . . ?
C23 C43 C44 C66 -31.7 . . . . ?
Lu7 C43 C44 C66 56.8(5) . . . . ?
Lu8 C43 C44 C66 24.04(16) . . . . ?
Lu4 C43 C44 C66 59.82(11) . . . . ?
Lu9 C43 C44 C66 58.6(4) . . . . ?
C42 C43 C44 Lu8 82.70(17) . . . . ?
C23 C43 C44 Lu8 -55.70(17) . . . . ?
Lu7 C43 C44 Lu8 32.8(5) . . . . ?
Lu4 C43 C44 Lu8 35.8(2) . . . . ?
Lu9 C43 C44 Lu8 34.5(5) . . . . ?
C42 C43 C44 Lu4 46.93(11) . . . . ?
C23 C43 C44 Lu4 -91.47(11) . . . . ?
Lu7 C43 C44 Lu4 -3.0(5) . . . . ?
Lu8 C43 C44 Lu4 -35.8(2) . . . . ?
Lu9 C43 C44 Lu4 -1.2(5) . . . . ?
C42 C43 C44 Lu9 48.2(4) . . . . ?
C23 C43 C44 Lu9 -90.2(4) . . . . ?
Lu7 C43 C44 Lu9 -1.8(7) . . . . ?
Lu8 C43 C44 Lu9 -34.5(5) . . . . ?
Lu4 C43 C44 Lu9 1.2(5) . . . . ?
C42 C43 C44 Lu7 49.9(5) . . . . ?
C23 C43 C44 Lu7 -88.5(5) . . . . ?
Lu8 C43 C44 Lu7 -32.8(5) . . . . ?
Lu4 C43 C44 Lu7 3.0(5) . . . . ?
Lu9 C43 C44 Lu7 1.8(7) . . . . ?
C43 C44 C45 C66 -148.5 . . . . ?
C63 C44 C45 C66 -8.4 . . . . ?
Lu8 C44 C45 C66 -92.46(16) . . . . ?
Lu4 C44 C45 C66 -68.99(18) . . . . ?
Lu9 C44 C45 C66 -60.0(4) . . . . ?
Lu7 C44 C45 C66 -80.0(6) . . . . ?
C43 C44 C45 C46 8.6 . . . . ?
C63 C44 C45 C46 148.7 . . . . ?
C66 C44 C45 C46 157.1 . . . . ?
Lu8 C44 C45 C46 64.64(16) . . . . ?
Lu4 C44 C45 C46 88.12(18) . . . . ?
Lu9 C44 C45 C46 97.1(4) . . . . ?
Lu7 C44 C45 C46 77.1(6) . . . . ?
C43 C44 C45 Lu8 -56.06(16) . . . . ?
C63 C44 C45 Lu8 84.07(16) . . . . ?
C66 C44 C45 Lu8 92.46(16) . . . . ?
Lu4 C44 C45 Lu8 23.5(2) . . . . ?
Lu9 C44 C45 Lu8 32.4(4) . . . . ?
Lu7 C44 C45 Lu8 12.5(6) . . . . ?
C43 C44 C45 Lu9 -88.5(4) . . . . ?
C63 C44 C45 Lu9 51.6(4) . . . . ?
C66 C44 C45 Lu9 60.0(4) . . . . ?
Lu8 C44 C45 Lu9 -32.4(4) . . . . ?
Lu4 C44 C45 Lu9 -9.0(4) . . . . ?
Lu7 C44 C45 Lu9 -20.0(7) . . . . ?
C43 C44 C45 Lu4 -79.53(18) . . . . ?
C63 C44 C45 Lu4 60.59(18) . . . . ?
C66 C44 C45 Lu4 68.99(18) . . . . ?
Lu8 C44 C45 Lu4 -23.5(2) . . . . ?
Lu9 C44 C45 Lu4 9.0(4) . . . . ?
Lu7 C44 C45 Lu4 -11.0(6) . . . . ?
C43 C44 C45 Lu7 -68.5(6) . . . . ?
C63 C44 C45 Lu7 71.6(6) . . . . ?
C66 C44 C45 Lu7 80.0(6) . . . . ?
Lu8 C44 C45 Lu7 -12.5(6) . . . . ?
Lu4 C44 C45 Lu7 11.0(6) . . . . ?
Lu9 C44 C45 Lu7 20.0(7) . . . . ?
C25 C24 C46 C45 -138.9 . . . . ?
C23 C24 C46 C45 4.6 . . . . ?
C26 C24 C46 C45 -143.7 . . . . ?
Lu8 C24 C46 C45 -45.06(16) . . . . ?
C25 C24 C46 C47 5.8 . . . . ?
C23 C24 C46 C47 149.4 . . . . ?
C26 C24 C46 C47 1.1 . . . . ?
Lu8 C24 C46 C47 99.68(16) . . . . ?
C25 C24 C46 C26 4.7 . . . . ?
C23 C24 C46 C26 148.3 . . . . ?
Lu8 C24 C46 C26 98.60(16) . . . . ?
C25 C24 C46 Lu8 -93.85(16) . . . . ?
C23 C24 C46 Lu8 49.71(16) . . . . ?
C26 C24 C46 Lu8 -98.60(16) . . . . ?
C66 C45 C46 C24 138.3 . . . . ?
C44 C45 C46 C24 -12.0 . . . . ?
Lu8 C45 C46 C24 47.44(18) . . . . ?
Lu9 C45 C46 C24 49.7(4) . . . . ?
Lu4 C45 C46 C24 41.17(14) . . . . ?
Lu7 C45 C46 C24 36.4(4) . . . . ?
C66 C45 C46 C47 -2.0 . . . . ?
C44 C45 C46 C47 -152.3 . . . . ?
Lu8 C45 C46 C47 -92.86(18) . . . . ?
Lu9 C45 C46 C47 -90.6(4) . . . . ?
Lu4 C45 C46 C47 -99.13(14) . . . . ?
Lu7 C45 C46 C47 -103.9(4) . . . . ?
C66 C45 C46 C26 26.7 . . . . ?
C44 C45 C46 C26 -123.6 . . . . ?
Lu8 C45 C46 C26 -64.23(18) . . . . ?
Lu9 C45 C46 C26 -62.0(4) . . . . ?
Lu4 C45 C46 C26 -70.50(14) . . . . ?
Lu7 C45 C46 C26 -75.2(4) . . . . ?
C66 C45 C46 Lu8 90.90(18) . . . . ?
C44 C45 C46 Lu8 -59.41(18) . . . . ?
Lu9 C45 C46 Lu8 2.3(4) . . . . ?
Lu4 C45 C46 Lu8 -6.3(2) . . . . ?
Lu7 C45 C46 Lu8 -11.0(5) . . . . ?
C27 C26 C47 C48 -1.0 . . . . ?
C25 C26 C47 C48 144.1 . . . . ?
C46 C26 C47 C48 146.2 . . . . ?
C24 C26 C47 C48 147.4 . . . . ?
C27 C26 C47 C46 -147.3 . . . . ?
C25 C26 C47 C46 -2.1 . . . . ?
C24 C26 C47 C46 1.2 . . . . ?
C25 C26 C47 C27 145.1 . . . . ?
C46 C26 C47 C27 147.3 . . . . ?
C24 C26 C47 C27 148.5 . . . . ?
C27 C26 C47 Lu5 -50.35(9) . . . . ?
C25 C26 C47 Lu5 94.78(9) . . . . ?
C46 C26 C47 Lu5 96.92(9) . . . . ?
C24 C26 C47 Lu5 98.11(9) . . . . ?
C27 C26 C47 Lu8 -100.36(12) . . . . ?
C25 C26 C47 Lu8 44.77(12) . . . . ?
C46 C26 C47 Lu8 46.91(12) . . . . ?
C24 C26 C47 Lu8 48.10(12) . . . . ?
C24 C46 C47 C26 -2.0 . . . . ?
C45 C46 C47 C26 145.8 . . . . ?
Lu8 C46 C47 C26 74.56(15) . . . . ?
C24 C46 C47 C48 -154.7 . . . . ?
C45 C46 C47 C48 -6.9 . . . . ?
C26 C46 C47 C48 -152.7 . . . . ?
Lu8 C46 C47 C48 -78.16(15) . . . . ?
C24 C46 C47 C27 -25.5 . . . . ?
C45 C46 C47 C27 122.4 . . . . ?
C26 C46 C47 C27 -23.5 . . . . ?
Lu8 C46 C47 C27 51.08(15) . . . . ?
C24 C46 C47 Lu5 -100.28(13) . . . . ?
C45 C46 C47 Lu5 47.56(13) . . . . ?
C26 C46 C47 Lu5 -98.29(13) . . . . ?
Lu8 C46 C47 Lu5 -23.72(19) . . . . ?
C24 C46 C47 Lu8 -76.56(15) . . . . ?
C45 C46 C47 Lu8 71.29(15) . . . . ?
C26 C46 C47 Lu8 -74.56(15) . . . . ?
C26 C47 C48 C67 -132.6 . . . . ?
C46 C47 C48 C67 11.3 . . . . ?
C27 C47 C48 C67 -133.2 . . . . ?
Lu5 C47 C48 C67 -67.08(17) . . . . ?
Lu8 C47 C48 C67 -37.12(12) . . . . ?
C26 C47 C48 C49 -4.1 . . . . ?
C46 C47 C48 C49 139.8 . . . . ?
C27 C47 C48 C49 -4.7 . . . . ?
Lu5 C47 C48 C49 61.45(17) . . . . ?
Lu8 C47 C48 C49 91.41(12) . . . . ?
C26 C47 C48 Lu5 -65.54(17) . . . . ?
C46 C47 C48 Lu5 78.38(17) . . . . ?
C27 C47 C48 Lu5 -66.11(17) . . . . ?
Lu8 C47 C48 Lu5 29.96(19) . . . . ?
C26 C47 C48 Lu10 -51.4(3) . . . . ?
C46 C47 C48 Lu10 92.5(3) . . . . ?
C27 C47 C48 Lu10 -52.0(3) . . . . ?
Lu5 C47 C48 Lu10 14.1(3) . . . . ?
Lu8 C47 C48 Lu10 44.1(3) . . . . ?
C29 C28 C49 C50 -3.5 . . . . ?
C27 C28 C49 C50 129.9 . . . . ?
Lu3 C28 C49 C50 36.21(10) . . . . ?
Lu10 C28 C49 C50 46.0(4) . . . . ?
Lu5 C28 C49 C50 53.57(14) . . . . ?
Lu6 C28 C49 C50 38.09(15) . . . . ?
C29 C28 C49 C48 -145.3 . . . . ?
C27 C28 C49 C48 -11.9 . . . . ?
Lu3 C28 C49 C48 -105.60(10) . . . . ?
Lu10 C28 C49 C48 -95.8(4) . . . . ?
Lu5 C28 C49 C48 -88.24(14) . . . . ?
Lu6 C28 C49 C48 -103.72(15) . . . . ?
C29 C28 C49 Lu5 -57.02(14) . . . . ?
C27 C28 C49 Lu5 76.31(14) . . . . ?
Lu3 C28 C49 Lu5 -17.36(15) . . . . ?
Lu10 C28 C49 Lu5 -7.5(3) . . . . ?
Lu6 C28 C49 Lu5 -15.5(2) . . . . ?
C29 C28 C49 Lu10 -49.5(4) . . . . ?
C27 C28 C49 Lu10 83.9(4) . . . . ?
Lu3 C28 C49 Lu10 -9.8(4) . . . . ?
Lu5 C28 C49 Lu10 7.5(3) . . . . ?
Lu6 C28 C49 Lu10 -7.9(4) . . . . ?
C29 C28 C49 Lu3 -39.66(10) . . . . ?
C27 C28 C49 Lu3 93.67(10) . . . . ?
Lu10 C28 C49 Lu3 9.8(4) . . . . ?
Lu5 C28 C49 Lu3 17.36(15) . . . . ?
Lu6 C28 C49 Lu3 1.9(2) . . . . ?
C47 C48 C49 C50 -138.8 . . . . ?
C67 C48 C49 C50 -5.3 . . . . ?
Lu5 C48 C49 C50 -53.32(17) . . . . ?
Lu10 C48 C49 C50 -67.5(3) . . . . ?
C47 C48 C49 C28 10.2 . . . . ?
C67 C48 C49 C28 143.8 . . . . ?
Lu5 C48 C49 C28 95.71(17) . . . . ?
Lu10 C48 C49 C28 81.5(3) . . . . ?
C47 C48 C49 Lu5 -85.51(17) . . . . ?
C67 C48 C49 Lu5 48.06(17) . . . . ?
Lu10 C48 C49 Lu5 -14.2(3) . . . . ?
C47 C48 C49 Lu10 -71.3(3) . . . . ?
C67 C48 C49 Lu10 62.3(3) . . . . ?
Lu5 C48 C49 Lu10 14.2(3) . . . . ?
C47 C48 C49 Lu3 -60.70(15) . . . . ?
C67 C48 C49 Lu3 72.87(15) . . . . ?
Lu5 C48 C49 Lu3 24.81(18) . . . . ?
Lu10 C48 C49 Lu3 10.6(3) . . . . ?
C28 C49 C50 C68 -143.2 . . . . ?
C48 C49 C50 C68 0.9 . . . . ?
Lu5 C49 C50 C68 -71.3(2) . . . . ?
Lu10 C49 C50 C68 -92.6(5) . . . . ?
Lu3 C49 C50 C68 -109.50(11) . . . . ?
C28 C49 C50 C51 9.9 . . . . ?
C48 C49 C50 C51 154.0 . . . . ?
Lu5 C49 C50 C51 81.9(2) . . . . ?
Lu10 C49 C50 C51 60.5(5) . . . . ?
Lu3 C49 C50 C51 43.66(11) . . . . ?
C28 C49 C50 Lu5 -71.9(2) . . . . ?
C48 C49 C50 Lu5 72.2(2) . . . . ?
Lu10 C49 C50 Lu5 -21.3(4) . . . . ?
Lu3 C49 C50 Lu5 -38.2(2) . . . . ?
C28 C49 C50 Lu10 -50.6(5) . . . . ?
C48 C49 C50 Lu10 93.5(5) . . . . ?
Lu5 C49 C50 Lu10 21.3(4) . . . . ?
Lu3 C49 C50 Lu10 -16.9(4) . . . . ?
C28 C49 C50 Lu3 -33.73(11) . . . . ?
C48 C49 C50 Lu3 110.36(11) . . . . ?
Lu5 C49 C50 Lu3 38.2(2) . . . . ?
Lu10 C49 C50 Lu3 16.9(4) . . . . ?
Lu10 Lu5 C50 C49 70.9(8) . . . . ?
Lu1 Lu5 C50 C49 -67.0(6) 6_565 . . . ?
Lu2 Lu5 C50 C49 -7.6(5) 6_565 . . . ?
Lu3 Lu5 C50 C49 73.6(3) . . . . ?
C68 Lu5 C50 C49 -110.19(5) . . . . ?
Lu6 Lu5 C50 C49 77.0(3) . . . . ?
Lu11 Lu5 C50 C49 107.6(8) . . . . ?
C51 Lu5 C50 C49 108.6 . . . . ?
C67 Lu5 C50 C49 -72.74(7) . . . . ?
C69 Lu5 C50 C49 -150.24(11) . . . . ?
Lu10 Lu5 C50 C68 -178.9(8) . . . . ?
Lu1 Lu5 C50 C68 43.2(5) 6_565 . . . ?
Lu2 Lu5 C50 C68 102.6(5) 6_565 . . . ?
Lu3 Lu5 C50 C68 -176.2(3) . . . . ?
Lu6 Lu5 C50 C68 -172.9(3) . . . . ?
Lu11 Lu5 C50 C68 -142.2(8) . . . . ?
C49 Lu5 C50 C68 110.19(5) . . . . ?
C51 Lu5 C50 C68 -141.16(6) . . . . ?
C67 Lu5 C50 C68 37.45(6) . . . . ?
C69 Lu5 C50 C68 -40.05(8) . . . . ?
Lu10 Lu5 C50 C51 -37.7(8) . . . . ?
Lu1 Lu5 C50 C51 -175.7(6) 6_565 . . . ?
Lu2 Lu5 C50 C51 -116.2(5) 6_565 . . . ?
Lu3 Lu5 C50 C51 -35.1(2) . . . . ?
C68 Lu5 C50 C51 141.16(6) . . . . ?
Lu6 Lu5 C50 C51 -31.7(2) . . . . ?
Lu11 Lu5 C50 C51 -1.1(8) . . . . ?
C49 Lu5 C50 C51 -108.6 . . . . ?
C67 Lu5 C50 C51 178.61(10) . . . . ?
C69 Lu5 C50 C51 101.11(9) . . . . ?
Lu1 Lu5 C50 Lu10 -137.9(12) 6_565 . . . ?
Lu2 Lu5 C50 Lu10 -78.5(11) 6_565 . . . ?
Lu3 Lu5 C50 Lu10 2.7(7) . . . . ?
C68 Lu5 C50 Lu10 178.9(8) . . . . ?
Lu6 Lu5 C50 Lu10 6.0(7) . . . . ?
Lu11 Lu5 C50 Lu10 36.7(10) . . . . ?
C49 Lu5 C50 Lu10 -70.9(8) . . . . ?
C51 Lu5 C50 Lu10 37.7(8) . . . . ?
C67 Lu5 C50 Lu10 -143.6(8) . . . . ?
C69 Lu5 C50 Lu10 138.9(8) . . . . ?
Lu10 Lu5 C50 Lu3 -2.7(7) . . . . ?
Lu1 Lu5 C50 Lu3 -140.6(7) 6_565 . . . ?
Lu2 Lu5 C50 Lu3 -81.2(6) 6_565 . . . ?
C68 Lu5 C50 Lu3 176.2(3) . . . . ?
Lu6 Lu5 C50 Lu3 3.4(3) . . . . ?
Lu11 Lu5 C50 Lu3 34.0(8) . . . . ?
C49 Lu5 C50 Lu3 -73.6(3) . . . . ?
C51 Lu5 C50 Lu3 35.1(2) . . . . ?
C67 Lu5 C50 Lu3 -146.3(3) . . . . ?
C69 Lu5 C50 Lu3 136.2(3) . . . . ?
C29 C30 C51 C52 139.1 . . . . ?
C31 C30 C51 C52 -9.1 . . . . ?
Lu3 C30 C51 C52 73.48(19) . . . . ?
Lu6 C30 C51 C52 59.56(18) . . . . ?
Lu10 C30 C51 C52 79.1(3) . . . . ?
Lu11 C30 C51 C52 39.1(7) . . . . ?
Lu5 C30 C51 C52 83.07(11) . . . . ?
C29 C30 C51 C50 5.5 . . . . ?
C31 C30 C51 C50 -142.6 . . . . ?
Lu3 C30 C51 C50 -60.05(19) . . . . ?
Lu6 C30 C51 C50 -73.97(18) . . . . ?
Lu10 C30 C51 C50 -54.4(3) . . . . ?
Lu11 C30 C51 C50 -94.5(7) . . . . ?
Lu5 C30 C51 C50 -50.45(11) . . . . ?
C29 C30 C51 Lu3 65.58(19) . . . . ?
C31 C30 C51 Lu3 -82.60(19) . . . . ?
Lu6 C30 C51 Lu3 -13.9(3) . . . . ?
Lu10 C30 C51 Lu3 5.6(3) . . . . ?
Lu11 C30 C51 Lu3 -34.4(7) . . . . ?
Lu5 C30 C51 Lu3 9.6(2) . . . . ?
C29 C30 C51 Lu10 60.0(3) . . . . ?
C31 C30 C51 Lu10 -88.2(3) . . . . ?
Lu3 C30 C51 Lu10 -5.6(3) . . . . ?
Lu6 C30 C51 Lu10 -19.5(4) . . . . ?
Lu11 C30 C51 Lu10 -40.0(7) . . . . ?
Lu5 C30 C51 Lu10 4.0(3) . . . . ?
C29 C30 C51 Lu5 55.99(11) . . . . ?
C31 C30 C51 Lu5 -92.20(11) . . . . ?
Lu3 C30 C51 Lu5 -9.6(2) . . . . ?
Lu6 C30 C51 Lu5 -23.5(2) . . . . ?
Lu10 C30 C51 Lu5 -4.0(3) . . . . ?
Lu11 C30 C51 Lu5 -44.0(7) . . . . ?
C29 C30 C51 Lu6 79.51(18) . . . . ?
C31 C30 C51 Lu6 -68.68(18) . . . . ?
Lu3 C30 C51 Lu6 13.9(3) . . . . ?
Lu10 C30 C51 Lu6 19.5(4) . . . . ?
Lu11 C30 C51 Lu6 -20.5(7) . . . . ?
Lu5 C30 C51 Lu6 23.5(2) . . . . ?
C29 C30 C51 Lu11 100.0(7) . . . . ?
C31 C30 C51 Lu11 -48.2(7) . . . . ?
Lu3 C30 C51 Lu11 34.4(7) . . . . ?
Lu6 C30 C51 Lu11 20.5(7) . . . . ?
Lu10 C30 C51 Lu11 40.0(7) . . . . ?
Lu5 C30 C51 Lu11 44.0(7) . . . . ?
C49 C50 C51 C52 -152.7 . . . . ?
C68 C50 C51 C52 -10.9 . . . . ?
Lu5 C50 C51 C52 -70.8(2) . . . . ?
Lu10 C50 C51 C52 -85.3(3) . . . . ?
Lu3 C50 C51 C52 -97.08(13) . . . . ?
C49 C50 C51 C30 -10.7 . . . . ?
C68 C50 C51 C30 131.2 . . . . ?
Lu5 C50 C51 C30 71.2(2) . . . . ?
Lu10 C50 C51 C30 56.7(3) . . . . ?
Lu3 C50 C51 C30 44.92(13) . . . . ?
C49 C50 C51 Lu3 -55.64(13) . . . . ?
C68 C50 C51 Lu3 86.23(13) . . . . ?
Lu5 C50 C51 Lu3 26.3(2) . . . . ?
Lu10 C50 C51 Lu3 11.8(3) . . . . ?
C49 C50 C51 Lu10 -67.4(3) . . . . ?
C68 C50 C51 Lu10 74.4(3) . . . . ?
Lu5 C50 C51 Lu10 14.5(3) . . . . ?
Lu3 C50 C51 Lu10 -11.8(3) . . . . ?
C49 C50 C51 Lu5 -81.9(2) . . . . ?
C68 C50 C51 Lu5 59.9(2) . . . . ?
Lu10 C50 C51 Lu5 -14.5(3) . . . . ?
Lu3 C50 C51 Lu5 -26.3(2) . . . . ?
C49 C50 C51 Lu6 -56.61(15) . . . . ?
C68 C50 C51 Lu6 85.26(15) . . . . ?
Lu5 C50 C51 Lu6 25.3(2) . . . . ?
Lu10 C50 C51 Lu6 10.8(4) . . . . ?
Lu3 C50 C51 Lu6 -1.0(2) . . . . ?
C49 C50 C51 Lu11 -81.1(6) . . . . ?
C68 C50 C51 Lu11 60.8(6) . . . . ?
Lu5 C50 C51 Lu11 0.9(6) . . . . ?
Lu10 C50 C51 Lu11 -13.6(7) . . . . ?
Lu3 C50 C51 Lu11 -25.4(6) . . . . ?
C30 C51 C52 C53 11.5 . . . . ?
C50 C51 C52 C53 152.7 . . . . ?
Lu3 C51 C52 C53 63.4(2) . . . . ?
Lu10 C51 C52 C53 83.1(5) . . . . ?
Lu5 C51 C52 C53 101.89(17) . . . . ?
Lu6 C51 C52 C53 50.81(16) . . . . ?
Lu11 C51 C52 C53 49.0(6) . . . . ?
C30 C51 C52 C70 -134.4 . . . . ?
C50 C51 C52 C70 6.8 . . . . ?
Lu3 C51 C52 C70 -82.4(2) . . . . ?
Lu10 C51 C52 C70 -62.8(5) . . . . ?
Lu5 C51 C52 C70 -43.96(17) . . . . ?
Lu6 C51 C52 C70 -95.03(16) . . . . ?
Lu11 C51 C52 C70 -96.8(6) . . . . ?
C30 C51 C52 Lu10 -71.6(5) . . . . ?
C50 C51 C52 Lu10 69.6(5) . . . . ?
Lu3 C51 C52 Lu10 -19.7(4) . . . . ?
Lu5 C51 C52 Lu10 18.8(4) . . . . ?
Lu6 C51 C52 Lu10 -32.3(5) . . . . ?
Lu11 C51 C52 Lu10 -34.1(8) . . . . ?
C30 C51 C52 Lu5 -90.42(17) . . . . ?
C50 C51 C52 Lu5 50.79(17) . . . . ?
Lu3 C51 C52 Lu5 -38.48(18) . . . . ?
Lu10 C51 C52 Lu5 -18.8(4) . . . . ?
Lu6 C51 C52 Lu5 -51.1(2) . . . . ?
Lu11 C51 C52 Lu5 -52.9(6) . . . . ?
C30 C51 C52 Lu11 -37.5(6) . . . . ?
C50 C51 C52 Lu11 103.7(6) . . . . ?
Lu3 C51 C52 Lu11 14.4(7) . . . . ?
Lu10 C51 C52 Lu11 34.1(8) . . . . ?
Lu5 C51 C52 Lu11 52.9(6) . . . . ?
Lu6 C51 C52 Lu11 1.8(6) . . . . ?
C30 C51 C52 Lu3 -51.9(2) . . . . ?
C50 C51 C52 Lu3 89.3(2) . . . . ?
Lu10 C51 C52 Lu3 19.7(4) . . . . ?
Lu5 C51 C52 Lu3 38.48(18) . . . . ?
Lu6 C51 C52 Lu3 -12.6(3) . . . . ?
Lu11 C51 C52 Lu3 -14.4(7) . . . . ?
C30 C51 C52 Lu6 -39.34(16) . . . . ?
C50 C51 C52 Lu6 101.87(16) . . . . ?
Lu3 C51 C52 Lu6 12.6(3) . . . . ?
Lu10 C51 C52 Lu6 32.3(5) . . . . ?
Lu5 C51 C52 Lu6 51.1(2) . . . . ?
Lu11 C51 C52 Lu6 -1.8(6) . . . . ?
C33 C32 C53 C54 0.6 . . . . ?
C31 C32 C53 C54 138.1 . . . . ?
Lu11 C32 C53 C54 73.7(6) . . . . ?
Lu6 C32 C53 C54 92.80(13) . . . . ?
Lu3 C32 C53 C54 103.25(9) . . . . ?
C33 C32 C53 C52 -138.8 . . . . ?
C31 C32 C53 C52 -1.3 . . . . ?
Lu11 C32 C53 C52 -65.7(6) . . . . ?
Lu6 C32 C53 C52 -46.57(13) . . . . ?
Lu3 C32 C53 C52 -36.12(9) . . . . ?
C33 C32 C53 Lu11 -73.2(6) . . . . ?
C31 C32 C53 Lu11 64.4(6) . . . . ?
Lu6 C32 C53 Lu11 19.1(6) . . . . ?
Lu3 C32 C53 Lu11 29.5(6) . . . . ?
C33 C32 C53 Lu3 -102.69(10) . . . . ?
C31 C32 C53 Lu3 34.82(9) . . . . ?
Lu11 C32 C53 Lu3 -29.5(6) . . . . ?
Lu6 C32 C53 Lu3 -10.45(16) . . . . ?
C33 C32 C53 Lu6 -92.24(13) . . . . ?
C31 C32 C53 Lu6 45.27(13) . . . . ?
Lu11 C32 C53 Lu6 -19.1(6) . . . . ?
Lu3 C32 C53 Lu6 10.45(16) . . . . ?
C33 C32 C53 Lu10 -99.0(2) . . . . ?
C31 C32 C53 Lu10 38.5(2) . . . . ?
Lu11 C32 C53 Lu10 -25.8(6) . . . . ?
Lu6 C32 C53 Lu10 -6.7(2) . . . . ?
Lu3 C32 C53 Lu10 3.7(2) . . . . ?
C51 C52 C53 C32 -6.2 . . . . ?
C70 C52 C53 C32 146.4 . . . . ?
Lu10 C52 C53 C32 51.3(4) . . . . ?
Lu5 C52 C53 C32 66.00(17) . . . . ?
Lu11 C52 C53 C32 53.2(7) . . . . ?
Lu3 C52 C53 C32 37.82(10) . . . . ?
Lu6 C52 C53 C32 37.75(15) . . . . ?
C51 C52 C53 C54 -150.0 . . . . ?
C70 C52 C53 C54 2.6 . . . . ?
Lu10 C52 C53 C54 -92.5(4) . . . . ?
Lu5 C52 C53 C54 -77.80(17) . . . . ?
Lu11 C52 C53 C54 -90.6(7) . . . . ?
Lu3 C52 C53 C54 -105.99(10) . . . . ?
Lu6 C52 C53 C54 -106.06(15) . . . . ?
C51 C52 C53 Lu11 -59.4(7) . . . . ?
C70 C52 C53 Lu11 93.2(7) . . . . ?
Lu10 C52 C53 Lu11 -1.9(8) . . . . ?
Lu5 C52 C53 Lu11 12.8(7) . . . . ?
Lu3 C52 C53 Lu11 -15.4(7) . . . . ?
Lu6 C52 C53 Lu11 -15.5(7) . . . . ?
C51 C52 C53 Lu3 -44.01(10) . . . . ?
C70 C52 C53 Lu3 108.54(10) . . . . ?
Lu10 C52 C53 Lu3 13.4(3) . . . . ?
Lu5 C52 C53 Lu3 28.19(15) . . . . ?
Lu11 C52 C53 Lu3 15.4(7) . . . . ?
Lu6 C52 C53 Lu3 -0.07(19) . . . . ?
C51 C52 C53 Lu6 -43.94(15) . . . . ?
C70 C52 C53 Lu6 108.61(15) . . . . ?
Lu10 C52 C53 Lu6 13.5(4) . . . . ?
Lu5 C52 C53 Lu6 28.3(2) . . . . ?
Lu11 C52 C53 Lu6 15.5(7) . . . . ?
Lu3 C52 C53 Lu6 0.07(19) . . . . ?
C51 C52 C53 Lu10 -57.4(4) . . . . ?
C70 C52 C53 Lu10 95.1(4) . . . . ?
Lu5 C52 C53 Lu10 14.7(3) . . . . ?
Lu11 C52 C53 Lu10 1.9(8) . . . . ?
Lu3 C52 C53 Lu10 -13.4(3) . . . . ?
Lu6 C52 C53 Lu10 -13.5(4) . . . . ?
C32 C53 C54 C55 -4.1 . . . . ?
C52 C53 C54 C55 140.3 . . . . ?
Lu11 C53 C54 C55 53.3(4) . . . . ?
Lu3 C53 C54 C55 72.74(17) . . . . ?
Lu6 C53 C54 C55 56.49(10) . . . . ?
Lu10 C53 C54 C55 84.1(3) . . . . ?
C32 C53 C54 C71 -146.9 . . . . ?
C52 C53 C54 C71 -2.5 . . . . ?
Lu11 C53 C54 C71 -89.5(4) . . . . ?
Lu3 C53 C54 C71 -70.05(17) . . . . ?
Lu6 C53 C54 C71 -86.30(10) . . . . ?
Lu10 C53 C54 C71 -58.7(3) . . . . ?
C32 C53 C54 Lu11 -57.4(4) . . . . ?
C52 C53 C54 Lu11 87.0(4) . . . . ?
Lu3 C53 C54 Lu11 19.4(5) . . . . ?
Lu6 C53 C54 Lu11 3.2(4) . . . . ?
Lu10 C53 C54 Lu11 30.8(5) . . . . ?
C53 C54 C55 C56 -147.7 . . . . ?
C71 C54 C55 C56 -7.3 . . . . ?
Lu11 C54 C55 C56 -105.4(6) . . . . ?
C53 C54 C55 C34 1.4 . . . . ?
C71 C54 C55 C34 141.8 . . . . ?
Lu11 C54 C55 C34 43.7(6) . . . . ?
C53 C54 C55 Lu11 -42.3(6) . . . . ?
C71 C54 C55 Lu11 98.1(6) . . . . ?
C33 C34 C55 C56 155.6 . . . . ?
C35 C34 C55 C56 0.4 . . . . ?
Lu11 C34 C55 C56 106.3(6) . . . . ?
C33 C34 C55 C54 4.7 . . . . ?
C35 C34 C55 C54 -150.5 . . . . ?
Lu11 C34 C55 C54 -44.7(6) . . . . ?
C33 C34 C55 Lu11 49.3(6) . . . . ?
C35 C34 C55 Lu11 -105.8(6) . . . . ?
C54 C55 C56 C57 14.7 . . . . ?
C34 C55 C56 C57 -135.2 . . . . ?
Lu11 C55 C56 C57 -62.63(16) . . . . ?
C54 C55 C56 C36 148.0 . . . . ?
C34 C55 C56 C36 -1.9 . . . . ?
Lu11 C55 C56 C36 70.68(16) . . . . ?
C37 C36 C56 C55 -144.5 . . . . ?
C35 C36 C56 C55 2.9 . . . . ?
C37 C36 C56 C57 -9.0 . . . . ?
C35 C36 C56 C57 138.5 . . . . ?
C55 C56 C57 C58 142.7 . . . . ?
C36 C56 C57 C58 18.4 . . . . ?
C55 C56 C57 C72 -15.0 . . . . ?
C36 C56 C57 C72 -139.3 . . . . ?
C72 C57 C58 C76 1.7 . . . . ?
C56 C57 C58 C76 -154.3 . . . . ?
C72 C57 C58 C59 139.9 . . . . ?
C56 C57 C58 C59 -16.2 . . . . ?
C72 C57 C58 Lu9 49.3(3) . . . . ?
C56 C57 C58 Lu9 -106.7(3) . . . . ?
C72 C57 C58 Lu4 54.26(15) . . . . ?
C56 C57 C58 Lu4 -101.76(15) . . . . ?
C36 C37 C59 C60 149.7 . . . . ?
C38 C37 C59 C60 3.7 . . . . ?
C36 C37 C59 C58 6.0 . . . . ?
C38 C37 C59 C58 -139.9 . . . . ?
C57 C58 C59 C60 -142.7 . . . . ?
C76 C58 C59 C60 -0.2 . . . . ?
Lu9 C58 C59 C60 -48.0(4) . . . . ?
Lu4 C58 C59 C60 -44.29(10) . . . . ?
C57 C58 C59 C37 4.0 . . . . ?
C76 C58 C59 C37 146.6 . . . . ?
Lu9 C58 C59 C37 98.8(4) . . . . ?
Lu4 C58 C59 C37 102.43(10) . . . . ?
C37 C59 C60 C61 -151.4 . . . . ?
C58 C59 C60 C61 -0.9 . . . . ?
C37 C59 C60 C40 -5.6 . . . . ?
C58 C59 C60 C40 144.9 . . . . ?
C37 C59 C60 Lu7 -85.6(3) . . . . ?
C58 C59 C60 Lu7 64.8(3) . . . . ?
C37 C59 C60 Lu4 -94.82(15) . . . . ?
C58 C59 C60 Lu4 55.65(15) . . . . ?
C37 C59 C60 Lu9 -99.7(3) . . . . ?
C58 C59 C60 Lu9 50.7(3) . . . . ?
C39 C40 C60 C59 5.9 . . . . ?
C41 C40 C60 C59 -143.9 . . . . ?
Lu7 C40 C60 C59 -98.5(5) . . . . ?
Lu4 C40 C60 C59 -98.49(11) . . . . ?
Lu1 C40 C60 C59 -49.15(6) . . . . ?
C39 C40 C60 C61 148.0 . . . . ?
C41 C40 C60 C61 -1.8 . . . . ?
Lu7 C40 C60 C61 43.6(5) . . . . ?
Lu4 C40 C60 C61 43.57(11) . . . . ?
Lu1 C40 C60 C61 92.91(6) . . . . ?
C39 C40 C60 Lu7 104.4(5) . . . . ?
C41 C40 C60 Lu7 -45.4(5) . . . . ?
Lu4 C40 C60 Lu7 0.0(6) . . . . ?
Lu1 C40 C60 Lu7 49.3(5) . . . . ?
C39 C40 C60 Lu4 104.44(11) . . . . ?
C41 C40 C60 Lu4 -45.37(11) . . . . ?
Lu7 C40 C60 Lu4 0.0(6) . . . . ?
Lu1 C40 C60 Lu4 49.34(11) . . . . ?
C39 C40 C60 Lu9 100.7(5) . . . . ?
C41 C40 C60 Lu9 -49.1(5) . . . . ?
Lu7 C40 C60 Lu9 -3.7(7) . . . . ?
Lu4 C40 C60 Lu9 -3.7(5) . . . . ?
Lu1 C40 C60 Lu9 45.6(5) . . . . ?
C59 C60 C61 C62 144.8 . . . . ?
C40 C60 C61 C62 -0.8 . . . . ?
Lu7 C60 C61 C62 47.5(7) . . . . ?
Lu4 C60 C61 C62 55.82(16) . . . . ?
Lu9 C60 C61 C62 66.0(6) . . . . ?
C59 C60 C61 C76 1.7 . . . . ?
C40 C60 C61 C76 -143.9 . . . . ?
Lu7 C60 C61 C76 -95.6(7) . . . . ?
Lu4 C60 C61 C76 -87.33(16) . . . . ?
Lu9 C60 C61 C76 -77.1(6) . . . . ?
C59 C60 C61 Lu4 89.01(16) . . . . ?
C40 C60 C61 Lu4 -56.57(16) . . . . ?
Lu7 C60 C61 Lu4 -8.3(7) . . . . ?
Lu9 C60 C61 Lu4 10.2(6) . . . . ?
C59 C60 C61 Lu7 97.3(7) . . . . ?
C40 C60 C61 Lu7 -48.3(7) . . . . ?
Lu4 C60 C61 Lu7 8.3(7) . . . . ?
Lu9 C60 C61 Lu7 18.5(9) . . . . ?
C59 C60 C61 Lu9 78.8(6) . . . . ?
C40 C60 C61 Lu9 -66.8(6) . . . . ?
Lu7 C60 C61 Lu9 -18.5(9) . . . . ?
Lu4 C60 C61 Lu9 -10.2(6) . . . . ?
C76 C61 C62 C63 6.2 . . . . ?
C60 C61 C62 C63 -133.8 . . . . ?
Lu4 C61 C62 C63 -62.8(3) . . . . ?
Lu7 C61 C62 C63 -76.7(4) . . . . ?
Lu9 C61 C62 C63 -51.1(4) . . . . ?
C76 C61 C62 C42 142.1 . . . . ?
C60 C61 C62 C42 2.0 . . . . ?
Lu4 C61 C62 C42 73.1(3) . . . . ?
Lu7 C61 C62 C42 59.2(4) . . . . ?
Lu9 C61 C62 C42 84.8(4) . . . . ?
C76 C61 C62 Lu4 69.0(3) . . . . ?
C60 C61 C62 Lu4 -71.1(3) . . . . ?
Lu7 C61 C62 Lu4 -13.9(4) . . . . ?
Lu9 C61 C62 Lu4 11.7(5) . . . . ?
C76 C61 C62 Lu7 82.9(4) . . . . ?
C60 C61 C62 Lu7 -57.1(4) . . . . ?
Lu4 C61 C62 Lu7 13.9(4) . . . . ?
Lu9 C61 C62 Lu7 25.6(5) . . . . ?
C76 C61 C62 Lu9 57.3(4) . . . . ?
C60 C61 C62 Lu9 -82.8(4) . . . . ?
Lu4 C61 C62 Lu9 -11.7(5) . . . . ?
Lu7 C61 C62 Lu9 -25.6(5) . . . . ?
C76 C61 C62 Lu8 75.57(12) . . . . ?
C60 C61 C62 Lu8 -64.50(12) . . . . ?
Lu4 C61 C62 Lu8 6.6(3) . . . . ?
Lu7 C61 C62 Lu8 -7.4(4) . . . . ?
Lu9 C61 C62 Lu8 18.3(4) . . . . ?
C41 C42 C62 C63 142.5 . . . . ?
C43 C42 C62 C63 -0.3 . . . . ?
Lu7 C42 C62 C63 74.3(5) . . . . ?
Lu4 C42 C62 C63 68.3(2) . . . . ?
Lu9 C42 C62 C63 64.7(6) . . . . ?
Lu8 C42 C62 C63 53.30(13) . . . . ?
C41 C42 C62 C61 -0.6 . . . . ?
C43 C42 C62 C61 -143.4 . . . . ?
Lu7 C42 C62 C61 -68.8(5) . . . . ?
Lu4 C42 C62 C61 -74.8(2) . . . . ?
Lu9 C42 C62 C61 -78.4(6) . . . . ?
Lu8 C42 C62 C61 -89.79(13) . . . . ?
C41 C42 C62 Lu4 74.2(2) . . . . ?
C43 C42 C62 Lu4 -68.6(2) . . . . ?
Lu7 C42 C62 Lu4 6.0(6) . . . . ?
Lu9 C42 C62 Lu4 -3.6(7) . . . . ?
Lu8 C42 C62 Lu4 -15.0(2) . . . . ?
C41 C42 C62 Lu7 68.2(5) . . . . ?
C43 C42 C62 Lu7 -74.6(5) . . . . ?
Lu4 C42 C62 Lu7 -6.0(6) . . . . ?
Lu9 C42 C62 Lu7 -9.6(8) . . . . ?
Lu8 C42 C62 Lu7 -21.0(5) . . . . ?
C41 C42 C62 Lu9 77.8(6) . . . . ?
C43 C42 C62 Lu9 -65.0(6) . . . . ?
Lu7 C42 C62 Lu9 9.6(8) . . . . ?
Lu4 C42 C62 Lu9 3.6(7) . . . . ?
Lu8 C42 C62 Lu9 -11.4(7) . . . . ?
C41 C42 C62 Lu8 89.18(13) . . . . ?
C43 C42 C62 Lu8 -53.60(13) . . . . ?
Lu7 C42 C62 Lu8 21.0(5) . . . . ?
Lu4 C42 C62 Lu8 15.0(2) . . . . ?
Lu9 C42 C62 Lu8 11.4(7) . . . . ?
Lu4 Lu4 C62 C63 -168.34(5) 6_565 . . . ?
Lu9 Lu4 C62 C63 178.3(13) 6_565 . . . ?
Lu8 Lu4 C62 C63 -69.1(8) . . . . ?
Lu8 Lu4 C62 C63 -122.6(4) 6_565 . . . ?
C61 Lu4 C62 C63 130.02(8) . . . . ?
C42 Lu4 C62 C63 -112.0 . . . . ?
C44 Lu4 C62 C63 -35.67(9) . . . . ?
C64 Lu4 C62 C63 34.29(6) . . . . ?
C43 Lu4 C62 C63 -75.73(8) . . . . ?
C76 Lu4 C62 C63 98.51(12) . . . . ?
Lu4 Lu4 C62 C61 61.65(5) 6_565 . . . ?
Lu9 Lu4 C62 C61 48.3(13) 6_565 . . . ?
Lu8 Lu4 C62 C61 160.9(8) . . . . ?
Lu8 Lu4 C62 C61 107.3(4) 6_565 . . . ?
C63 Lu4 C62 C61 -130.02(8) . . . . ?
C42 Lu4 C62 C61 117.99(8) . . . . ?
C44 Lu4 C62 C61 -165.69(16) . . . . ?
C64 Lu4 C62 C61 -95.73(6) . . . . ?
C43 Lu4 C62 C61 154.26(14) . . . . ?
C76 Lu4 C62 C61 -31.5 . . . . ?
Lu4 Lu4 C62 C42 -56.34(4) 6_565 . . . ?
Lu9 Lu4 C62 C42 -69.7(13) 6_565 . . . ?
Lu8 Lu4 C62 C42 42.9(8) . . . . ?
Lu8 Lu4 C62 C42 -10.6(4) 6_565 . . . ?
C63 Lu4 C62 C42 112.0 . . . . ?
C61 Lu4 C62 C42 -117.99(8) . . . . ?
C44 Lu4 C62 C42 76.32(9) . . . . ?
C64 Lu4 C62 C42 146.28(9) . . . . ?
C43 Lu4 C62 C42 36.27(7) . . . . ?
C76 Lu4 C62 C42 -149.50(13) . . . . ?
Lu4 Lu4 C62 Lu7 -33(3) 6_565 . . . ?
Lu9 Lu4 C62 Lu7 -46(3) 6_565 . . . ?
Lu8 Lu4 C62 Lu7 66(3) . . . . ?
Lu8 Lu4 C62 Lu7 13(3) 6_565 . . . ?
C63 Lu4 C62 Lu7 135(3) . . . . ?
C61 Lu4 C62 Lu7 -95(3) . . . . ?
C42 Lu4 C62 Lu7 23(3) . . . . ?
C44 Lu4 C62 Lu7 100(3) . . . . ?
C64 Lu4 C62 Lu7 170(3) . . . . ?
C43 Lu4 C62 Lu7 60(3) . . . . ?
C76 Lu4 C62 Lu7 -126(3) . . . . ?
Lu4 Lu4 C62 Lu9 142(4) 6_565 . . . ?
Lu9 Lu4 C62 Lu9 128(5) 6_565 . . . ?
Lu8 Lu4 C62 Lu9 -119(4) . . . . ?
Lu8 Lu4 C62 Lu9 -173(4) 6_565 . . . ?
C63 Lu4 C62 Lu9 -50(4) . . . . ?
C61 Lu4 C62 Lu9 80(4) . . . . ?
C42 Lu4 C62 Lu9 -162(4) . . . . ?
C44 Lu4 C62 Lu9 -86(4) . . . . ?
C64 Lu4 C62 Lu9 -16(4) . . . . ?
C43 Lu4 C62 Lu9 -126(4) . . . . ?
C76 Lu4 C62 Lu9 49(4) . . . . ?
Lu4 Lu4 C62 Lu8 -99.2(8) 6_565 . . . ?
Lu9 Lu4 C62 Lu8 -112.5(14) 6_565 . . . ?
Lu8 Lu4 C62 Lu8 -53.5(7) 6_565 . . . ?
C63 Lu4 C62 Lu8 69.1(8) . . . . ?
C61 Lu4 C62 Lu8 -160.9(8) . . . . ?
C42 Lu4 C62 Lu8 -42.9(8) . . . . ?
C44 Lu4 C62 Lu8 33.5(7) . . . . ?
C64 Lu4 C62 Lu8 103.4(8) . . . . ?
C43 Lu4 C62 Lu8 -6.6(7) . . . . ?
C76 Lu4 C62 Lu8 167.6(9) . . . . ?
Lu4 Lu7 C62 C63 156(3) 6_565 . . . ?
Lu9 Lu7 C62 C63 45(2) . . . . ?
Lu9 Lu7 C62 C63 151(3) 6_565 . . . ?
Lu8 Lu7 C62 C63 -112(2) 6_565 . . . ?
Lu8 Lu7 C62 C63 -31.3(18) . . . . ?
C42 Lu7 C62 C63 -112.2(3) . . . . ?
C43 Lu7 C62 C63 -71.98(6) . . . . ?
C41 Lu7 C62 C63 -142.5(5) . . . . ?
C61 Lu7 C62 C63 126.10(15) . . . . ?
C44 Lu7 C62 C63 -31.2(2) . . . . ?
Lu4 Lu7 C62 C61 30(3) 6_565 . . . ?
Lu9 Lu7 C62 C61 -81(2) . . . . ?
Lu9 Lu7 C62 C61 25(2) 6_565 . . . ?
Lu8 Lu7 C62 C61 121.5(18) 6_565 . . . ?
Lu8 Lu7 C62 C61 -157(2) . . . . ?
C42 Lu7 C62 C61 121.73(16) . . . . ?
C43 Lu7 C62 C61 161.92(15) . . . . ?
C41 Lu7 C62 C61 91.4(4) . . . . ?
C63 Lu7 C62 C61 -126.10(15) . . . . ?
C44 Lu7 C62 C61 -157.3(3) . . . . ?
Lu4 Lu7 C62 C42 -91(3) 6_565 . . . ?
Lu9 Lu7 C62 C42 157(2) . . . . ?
Lu9 Lu7 C62 C42 -97(2) 6_565 . . . ?
Lu8 Lu7 C62 C42 -0.2(17) 6_565 . . . ?
Lu8 Lu7 C62 C42 81(2) . . . . ?
C43 Lu7 C62 C42 40.2(3) . . . . ?
C41 Lu7 C62 C42 -30.4(3) . . . . ?
C61 Lu7 C62 C42 -121.73(15) . . . . ?
C63 Lu7 C62 C42 112.2(3) . . . . ?
C44 Lu7 C62 C42 81.0(5) . . . . ?
Lu4 Lu7 C62 Lu4 114(6) 6_565 . . . ?
Lu9 Lu7 C62 Lu4 3(2) . . . . ?
Lu9 Lu7 C62 Lu4 109(5) 6_565 . . . ?
Lu8 Lu7 C62 Lu4 -155(5) 6_565 . . . ?
Lu8 Lu7 C62 Lu4 -73.8(14) . . . . ?
C42 Lu7 C62 Lu4 -155(3) . . . . ?
C43 Lu7 C62 Lu4 -115(3) . . . . ?
C41 Lu7 C62 Lu4 175(4) . . . . ?
C61 Lu7 C62 Lu4 84(3) . . . . ?
C63 Lu7 C62 Lu4 -43(3) . . . . ?
C44 Lu7 C62 Lu4 -74(3) . . . . ?
Lu4 Lu7 C62 Lu9 111(5) 6_565 . . . ?
Lu9 Lu7 C62 Lu9 106(5) 6_565 . . . ?
Lu8 Lu7 C62 Lu9 -157(4) 6_565 . . . ?
Lu8 Lu7 C62 Lu9 -76.4(17) . . . . ?
C42 Lu7 C62 Lu9 -157(2) . . . . ?
C43 Lu7 C62 Lu9 -117(2) . . . . ?
C41 Lu7 C62 Lu9 172(3) . . . . ?
C61 Lu7 C62 Lu9 81(2) . . . . ?
C63 Lu7 C62 Lu9 -45(2) . . . . ?
C44 Lu7 C62 Lu9 -76(2) . . . . ?
Lu4 Lu7 C62 Lu8 -172(5) 6_565 . . . ?
Lu9 Lu7 C62 Lu8 76.4(17) . . . . ?
Lu9 Lu7 C62 Lu8 -177(4) 6_565 . . . ?
Lu8 Lu7 C62 Lu8 -81(4) 6_565 . . . ?
C42 Lu7 C62 Lu8 -81(2) . . . . ?
C43 Lu7 C62 Lu8 -40.7(19) . . . . ?
C41 Lu7 C62 Lu8 -111(2) . . . . ?
C61 Lu7 C62 Lu8 157(2) . . . . ?
C63 Lu7 C62 Lu8 31.3(18) . . . . ?
C44 Lu7 C62 Lu8 0.1(17) . . . . ?
C61 C62 C63 C64 -3.1 . . . . ?
C42 C62 C63 C64 -141.9 . . . . ?
Lu4 C62 C63 C64 -69.85(15) . . . . ?
Lu7 C62 C63 C64 -79.6(8) . . . . ?
Lu9 C62 C63 C64 -60.1(7) . . . . ?
Lu8 C62 C63 C64 -90.20(13) . . . . ?
C61 C62 C63 C44 132.9 . . . . ?
C42 C62 C63 C44 -5.9 . . . . ?
Lu4 C62 C63 C44 66.15(15) . . . . ?
Lu7 C62 C63 C44 56.4(8) . . . . ?
Lu9 C62 C63 C44 75.9(7) . . . . ?
Lu8 C62 C63 C44 45.80(13) . . . . ?
C61 C62 C63 Lu4 66.70(15) . . . . ?
C42 C62 C63 Lu4 -72.07(15) . . . . ?
Lu7 C62 C63 Lu4 -9.7(9) . . . . ?
Lu9 C62 C63 Lu4 9.8(7) . . . . ?
Lu8 C62 C63 Lu4 -20.3(2) . . . . ?
C61 C62 C63 Lu9 56.9(7) . . . . ?
C42 C62 C63 Lu9 -81.8(7) . . . . ?
Lu4 C62 C63 Lu9 -9.8(7) . . . . ?
Lu7 C62 C63 Lu9 -19.5(10) . . . . ?
Lu8 C62 C63 Lu9 -30.1(7) . . . . ?
C61 C62 C63 Lu7 76.4(8) . . . . ?
C42 C62 C63 Lu7 -62.3(8) . . . . ?
Lu4 C62 C63 Lu7 9.7(9) . . . . ?
Lu9 C62 C63 Lu7 19.5(10) . . . . ?
Lu8 C62 C63 Lu7 -10.6(9) . . . . ?
C61 C62 C63 Lu8 87.05(13) . . . . ?
C42 C62 C63 Lu8 -51.72(13) . . . . ?
Lu4 C62 C63 Lu8 20.3(2) . . . . ?
Lu7 C62 C63 Lu8 10.6(9) . . . . ?
Lu9 C62 C63 Lu8 30.1(7) . . . . ?
C45 C44 C63 C62 -138.7 . . . . ?
C43 C44 C63 C62 9.0 . . . . ?
C66 C44 C63 C62 -143.3 . . . . ?
Lu8 C44 C63 C62 -63.69(18) . . . . ?
Lu4 C44 C63 C62 -58.7(2) . . . . ?
Lu9 C44 C63 C62 -72.0(5) . . . . ?
Lu7 C44 C63 C62 -48.4(5) . . . . ?
C45 C44 C63 C64 -1.2 . . . . ?
C43 C44 C63 C64 146.6 . . . . ?
C66 C44 C63 C64 -5.7 . . . . ?
Lu8 C44 C63 C64 73.87(18) . . . . ?
Lu4 C44 C63 C64 78.8(2) . . . . ?
Lu9 C44 C63 C64 65.5(5) . . . . ?
Lu7 C44 C63 C64 89.2(5) . . . . ?
C45 C44 C63 Lu4 -80.0(2) . . . . ?
C43 C44 C63 Lu4 67.8(2) . . . . ?
C66 C44 C63 Lu4 -84.6(2) . . . . ?
Lu8 C44 C63 Lu4 -5.0(3) . . . . ?
Lu9 C44 C63 Lu4 -13.3(5) . . . . ?
Lu7 C44 C63 Lu4 10.4(5) . . . . ?
C45 C44 C63 Lu9 -66.7(5) . . . . ?
C43 C44 C63 Lu9 81.1(5) . . . . ?
C66 C44 C63 Lu9 -71.3(5) . . . . ?
Lu8 C44 C63 Lu9 8.3(5) . . . . ?
Lu4 C44 C63 Lu9 13.3(5) . . . . ?
Lu7 C44 C63 Lu9 23.7(6) . . . . ?
C45 C44 C63 Lu7 -90.4(5) . . . . ?
C43 C44 C63 Lu7 57.4(5) . . . . ?
C66 C44 C63 Lu7 -94.9(5) . . . . ?
Lu8 C44 C63 Lu7 -15.3(5) . . . . ?
Lu4 C44 C63 Lu7 -10.4(5) . . . . ?
Lu9 C44 C63 Lu7 -23.7(6) . . . . ?
C45 C44 C63 Lu8 -75.04(18) . . . . ?
C43 C44 C63 Lu8 72.73(18) . . . . ?
C66 C44 C63 Lu8 -79.61(18) . . . . ?
Lu4 C44 C63 Lu8 5.0(3) . . . . ?
Lu9 C44 C63 Lu8 -8.3(5) . . . . ?
Lu7 C44 C63 Lu8 15.3(5) . . . . ?
C62 C63 C64 C75 -0.3 . . . . ?
C44 C63 C64 C75 -136.8 . . . . ?
Lu4 C63 C64 C75 -60.56(15) . . . . ?
Lu9 C63 C64 C75 -63.6(7) . . . . ?
Lu7 C63 C64 C75 -59.6(5) . . . . ?
Lu8 C63 C64 C75 -86.71(13) . . . . ?
C62 C63 C64 C65 145.5 . . . . ?
C44 C63 C64 C65 9.0 . . . . ?
Lu4 C63 C64 C65 85.22(15) . . . . ?
Lu9 C63 C64 C65 82.2(7) . . . . ?
Lu7 C63 C64 C65 86.1(5) . . . . ?
Lu8 C63 C64 C65 59.07(13) . . . . ?
C62 C63 C64 Lu9 63.3(7) . . . . ?
C44 C63 C64 Lu9 -73.2(7) . . . . ?
Lu4 C63 C64 Lu9 3.1(8) . . . . ?
Lu7 C63 C64 Lu9 4.0(9) . . . . ?
Lu8 C63 C64 Lu9 -23.1(7) . . . . ?
C62 C63 C64 Lu4 60.26(15) . . . . ?
C44 C63 C64 Lu4 -76.22(15) . . . . ?
Lu9 C63 C64 Lu4 -3.1(7) . . . . ?
Lu7 C63 C64 Lu4 0.9(6) . . . . ?
Lu8 C63 C64 Lu4 -26.15(19) . . . . ?
C62 C63 C64 Lu7 59.3(5) . . . . ?
C44 C63 C64 Lu7 -77.1(5) . . . . ?
Lu4 C63 C64 Lu7 -0.9(6) . . . . ?
Lu9 C63 C64 Lu7 -4.0(9) . . . . ?
Lu8 C63 C64 Lu7 -27.1(5) . . . . ?
C75 C64 C65 C66 140.2 . . . . ?
C63 C64 C65 C66 -8.5 . . . . ?
Lu9 C64 C65 C66 57.9(7) . . . . ?
Lu4 C64 C65 C66 50.09(11) . . . . ?
Lu7 C64 C65 C66 46.6(6) . . . . ?
C75 C64 C65 C74 -0.6 . . . . ?
C63 C64 C65 C74 -149.3 . . . . ?
Lu9 C64 C65 C74 -82.9(7) . . . . ?
Lu4 C64 C65 C74 -90.72(11) . . . . ?
Lu7 C64 C65 C74 -94.2(6) . . . . ?
C75 C64 C65 Lu9 82.3(7) . . . . ?
C63 C64 C65 Lu9 -66.4(7) . . . . ?
Lu4 C64 C65 Lu9 -7.8(7) . . . . ?
Lu7 C64 C65 Lu9 -11.3(9) . . . . ?
C75 C64 C65 Lu4 90.11(11) . . . . ?
C63 C64 C65 Lu4 -58.56(11) . . . . ?
Lu9 C64 C65 Lu4 7.8(7) . . . . ?
Lu7 C64 C65 Lu4 -3.5(6) . . . . ?
C75 C64 C65 Lu8 98.71(12) . . . . ?
C63 C64 C65 Lu8 -49.96(12) . . . . ?
Lu9 C64 C65 Lu8 16.4(7) . . . . ?
Lu4 C64 C65 Lu8 8.61(15) . . . . ?
Lu7 C64 C65 Lu8 5.1(6) . . . . ?
C44 C45 C66 C65 10.9 . . . . ?
C46 C45 C66 C65 -140.7 . . . . ?
Lu8 C45 C66 C65 -59.32(16) . . . . ?
Lu9 C45 C66 C65 -37.5(4) . . . . ?
Lu4 C45 C66 C65 -35.75(10) . . . . ?
Lu7 C45 C66 C65 -37.9(3) . . . . ?
C44 C45 C66 C67 156.5 . . . . ?
C46 C45 C66 C67 4.9 . . . . ?
Lu8 C45 C66 C67 86.30(16) . . . . ?
Lu9 C45 C66 C67 108.1(4) . . . . ?
Lu4 C45 C66 C67 109.86(10) . . . . ?
Lu7 C45 C66 C67 107.7(3) . . . . ?
C46 C45 C66 C44 -151.7 . . . . ?
Lu8 C45 C66 C44 -70.25(16) . . . . ?
Lu9 C45 C66 C44 -48.4(4) . . . . ?
Lu4 C45 C66 C44 -46.69(10) . . . . ?
Lu7 C45 C66 C44 -48.8(3) . . . . ?
C44 C45 C66 Lu8 70.25(16) . . . . ?
C46 C45 C66 Lu8 -81.42(16) . . . . ?
Lu9 C45 C66 Lu8 21.8(4) . . . . ?
Lu4 C45 C66 Lu8 23.56(18) . . . . ?
Lu7 C45 C66 Lu8 21.4(3) . . . . ?
C44 C45 C66 Lu9 48.4(4) . . . . ?
C46 C45 C66 Lu9 -103.2(4) . . . . ?
Lu8 C45 C66 Lu9 -21.8(4) . . . . ?
Lu4 C45 C66 Lu9 1.7(4) . . . . ?
Lu7 C45 C66 Lu9 -0.4(5) . . . . ?
C44 C45 C66 Lu5 105.05(9) . . . . ?
C46 C45 C66 Lu5 -46.62(9) . . . . ?
Lu8 C45 C66 Lu5 34.80(18) . . . . ?
Lu9 C45 C66 Lu5 56.6(4) . . . . ?
Lu4 C45 C66 Lu5 58.36(12) . . . . ?
Lu7 C45 C66 Lu5 56.2(3) . . . . ?
C44 C45 C66 Lu4 46.69(10) . . . . ?
C46 C45 C66 Lu4 -104.98(10) . . . . ?
Lu8 C45 C66 Lu4 -23.56(18) . . . . ?
Lu9 C45 C66 Lu4 -1.7(4) . . . . ?
Lu7 C45 C66 Lu4 -2.2(4) . . . . ?
C64 C65 C66 C45 -2.9 . . . . ?
C74 C65 C66 C45 126.9 . . . . ?
Lu9 C65 C66 C45 41.9(5) . . . . ?
Lu4 C65 C66 C45 36.15(11) . . . . ?
Lu8 C65 C66 C45 45.38(14) . . . . ?
C64 C65 C66 C67 -148.8 . . . . ?
C74 C65 C66 C67 -19.0 . . . . ?
Lu9 C65 C66 C67 -104.0(5) . . . . ?
Lu4 C65 C66 C67 -109.73(11) . . . . ?
Lu8 C65 C66 C67 -100.50(14) . . . . ?
C64 C65 C66 C44 4.0 . . . . ?
C74 C65 C66 C44 133.7 . . . . ?
Lu9 C65 C66 C44 48.8(5) . . . . ?
Lu4 C65 C66 C44 43.00(11) . . . . ?
Lu8 C65 C66 C44 52.23(14) . . . . ?
C64 C65 C66 Lu8 -48.27(14) . . . . ?
C74 C65 C66 Lu8 81.52(14) . . . . ?
Lu9 C65 C66 Lu8 -3.5(5) . . . . ?
Lu4 C65 C66 Lu8 -9.23(16) . . . . ?
C64 C65 C66 Lu9 -44.8(5) . . . . ?
C74 C65 C66 Lu9 85.0(5) . . . . ?
Lu4 C65 C66 Lu9 -5.8(5) . . . . ?
Lu8 C65 C66 Lu9 3.5(5) . . . . ?
C64 C65 C66 Lu5 -102.09(9) . . . . ?
C74 C65 C66 Lu5 27.70(9) . . . . ?
Lu9 C65 C66 Lu5 -57.3(5) . . . . ?
Lu4 C65 C66 Lu5 -63.05(14) . . . . ?
Lu8 C65 C66 Lu5 -53.82(16) . . . . ?
C64 C65 C66 Lu4 -39.04(11) . . . . ?
C74 C65 C66 Lu4 90.75(11) . . . . ?
Lu9 C65 C66 Lu4 5.8(5) . . . . ?
Lu8 C65 C66 Lu4 9.23(16) . . . . ?
C47 C48 C67 C68 138.3 . . . . ?
C49 C48 C67 C68 7.6 . . . . ?
Lu5 C48 C67 C68 52.78(11) . . . . ?
Lu10 C48 C67 C68 51.6(2) . . . . ?
C47 C48 C67 C66 -9.1 . . . . ?
C49 C48 C67 C66 -139.8 . . . . ?
Lu5 C48 C67 C66 -94.60(11) . . . . ?
Lu10 C48 C67 C66 -95.8(2) . . . . ?
C47 C48 C67 Lu5 85.54(11) . . . . ?
C49 C48 C67 Lu5 -45.18(11) . . . . ?
Lu10 C48 C67 Lu5 -1.2(2) . . . . ?
C47 C48 C67 Lu10 86.7(2) . . . . ?
C49 C48 C67 Lu10 -44.0(2) . . . . ?
Lu5 C48 C67 Lu10 1.2(2) . . . . ?
C45 C66 C67 C48 0.7 . . . . ?
C65 C66 C67 C48 154.2 . . . . ?
C44 C66 C67 C48 26.2 . . . . ?
Lu8 C66 C67 C48 57.19(13) . . . . ?
Lu9 C66 C67 C48 86.1(5) . . . . ?
Lu5 C66 C67 C48 85.01(15) . . . . ?
Lu4 C66 C67 C48 78.51(11) . . . . ?
C45 C66 C67 C68 -143.1 . . . . ?
C65 C66 C67 C68 10.4 . . . . ?
C44 C66 C67 C68 -117.6 . . . . ?
Lu8 C66 C67 C68 -86.63(13) . . . . ?
Lu9 C66 C67 C68 -57.7(5) . . . . ?
Lu5 C66 C67 C68 -58.81(15) . . . . ?
Lu4 C66 C67 C68 -65.30(11) . . . . ?
C45 C66 C67 Lu5 -84.30(15) . . . . ?
C65 C66 C67 Lu5 69.19(15) . . . . ?
C44 C66 C67 Lu5 -58.79(15) . . . . ?
Lu8 C66 C67 Lu5 -27.8(2) . . . . ?
Lu9 C66 C67 Lu5 1.1(5) . . . . ?
Lu4 C66 C67 Lu5 -6.50(19) . . . . ?
C45 C66 C67 Lu10 -76.53(17) . . . . ?
C65 C66 C67 Lu10 76.96(17) . . . . ?
C44 C66 C67 Lu10 -51.02(17) . . . . ?
Lu8 C66 C67 Lu10 -20.0(2) . . . . ?
Lu9 C66 C67 Lu10 8.9(5) . . . . ?
Lu5 C66 C67 Lu10 7.8(2) . . . . ?
Lu4 C66 C67 Lu10 1.3(2) . . . . ?
C48 C67 C68 C50 -7.0 . . . . ?
C66 C67 C68 C50 142.1 . . . . ?
Lu5 C67 C68 C50 60.07(18) . . . . ?
Lu10 C67 C68 C50 49.7(3) . . . . ?
C48 C67 C68 C69 -141.8 . . . . ?
C66 C67 C68 C69 7.3 . . . . ?
Lu5 C67 C68 C69 -74.68(18) . . . . ?
Lu10 C67 C68 C69 -85.0(3) . . . . ?
C48 C67 C68 Lu5 -67.12(18) . . . . ?
C66 C67 C68 Lu5 82.01(18) . . . . ?
Lu10 C67 C68 Lu5 -10.4(3) . . . . ?
C48 C67 C68 Lu10 -56.8(3) . . . . ?
C66 C67 C68 Lu10 92.4(3) . . . . ?
Lu5 C67 C68 Lu10 10.4(3) . . . . ?
C49 C50 C68 C67 3.8 . . . . ?
C51 C50 C68 C67 -138.1 . . . . ?
Lu5 C50 C68 C67 -74.62(16) . . . . ?
Lu10 C50 C68 C67 -75.0(3) . . . . ?
Lu3 C50 C68 C67 -77.17(11) . . . . ?
C49 C50 C68 C69 146.2 . . . . ?
C51 C50 C68 C69 4.3 . . . . ?
Lu5 C50 C68 C69 67.84(16) . . . . ?
Lu10 C50 C68 C69 67.4(3) . . . . ?
Lu3 C50 C68 C69 65.28(11) . . . . ?
C49 C50 C68 Lu5 78.40(16) . . . . ?
C51 C50 C68 Lu5 -63.51(16) . . . . ?
Lu10 C50 C68 Lu5 -0.4(3) . . . . ?
Lu3 C50 C68 Lu5 -2.56(19) . . . . ?
C49 C50 C68 Lu10 78.8(3) . . . . ?
C51 C50 C68 Lu10 -63.1(3) . . . . ?
Lu5 C50 C68 Lu10 0.4(3) . . . . ?
Lu3 C50 C68 Lu10 -2.1(3) . . . . ?
C67 C68 C69 C74 -17.6 . . . . ?
C50 C68 C69 C74 -151.4 . . . . ?
Lu5 C68 C69 C74 -94.27(17) . . . . ?
Lu10 C68 C69 C74 -104.5(3) . . . . ?
C67 C68 C69 C70 140.8 . . . . ?
C50 C68 C69 C70 7.0 . . . . ?
Lu5 C68 C69 C70 64.12(17) . . . . ?
Lu10 C68 C69 C70 53.9(3) . . . . ?
C67 C68 C69 Lu5 76.69(17) . . . . ?
C50 C68 C69 Lu5 -57.13(17) . . . . ?
Lu10 C68 C69 Lu5 -10.2(3) . . . . ?
C67 C68 C69 Lu10 86.9(3) . . . . ?
C50 C68 C69 Lu10 -46.9(3) . . . . ?
Lu5 C68 C69 Lu10 10.2(3) . . . . ?
C74 C69 C70 C71 -7.7 . . . . ?
C68 C69 C70 C71 -153.6 . . . . ?
Lu5 C69 C70 C71 -105.14(10) . . . . ?
Lu10 C69 C70 C71 -105.2(2) . . . . ?
C74 C69 C70 C52 133.2 . . . . ?
C68 C69 C70 C52 -12.7 . . . . ?
Lu5 C69 C70 C52 35.75(10) . . . . ?
Lu10 C69 C70 C52 35.7(2) . . . . ?
C74 C69 C70 Lu5 97.41(10) . . . . ?
C68 C69 C70 Lu5 -48.48(10) . . . . ?
Lu10 C69 C70 Lu5 -0.1(2) . . . . ?
C74 C69 C70 Lu10 97.5(2) . . . . ?
C68 C69 C70 Lu10 -48.4(2) . . . . ?
Lu5 C69 C70 Lu10 0.1(2) . . . . ?
C74 C69 C70 Lu11 76.7(5) . . . . ?
C68 C69 C70 Lu11 -69.2(5) . . . . ?
Lu5 C69 C70 Lu11 -20.8(5) . . . . ?
Lu10 C69 C70 Lu11 -20.8(5) . . . . ?
C51 C52 C70 C69 5.5 . . . . ?
C53 C52 C70 C69 -142.4 . . . . ?
Lu10 C52 C70 C69 -42.9(2) . . . . ?
Lu5 C52 C70 C69 -35.44(11) . . . . ?
Lu11 C52 C70 C69 -80.7(6) . . . . ?
Lu3 C52 C70 C69 -48.65(15) . . . . ?
Lu6 C52 C70 C69 -62.41(11) . . . . ?
C51 C52 C70 C71 146.2 . . . . ?
C53 C52 C70 C71 -1.7 . . . . ?
Lu10 C52 C70 C71 97.8(2) . . . . ?
Lu5 C52 C70 C71 105.23(11) . . . . ?
Lu11 C52 C70 C71 59.9(6) . . . . ?
Lu3 C52 C70 C71 92.01(15) . . . . ?
Lu6 C52 C70 C71 78.26(11) . . . . ?
C51 C52 C70 Lu5 40.94(11) . . . . ?
C53 C52 C70 Lu5 -106.95(11) . . . . ?
Lu10 C52 C70 Lu5 -7.4(2) . . . . ?
Lu11 C52 C70 Lu5 -45.3(6) . . . . ?
Lu3 C52 C70 Lu5 -13.22(15) . . . . ?
Lu6 C52 C70 Lu5 -26.97(13) . . . . ?
C51 C52 C70 Lu10 48.4(2) . . . . ?
C53 C52 C70 Lu10 -99.5(2) . . . . ?
Lu5 C52 C70 Lu10 7.4(2) . . . . ?
Lu11 C52 C70 Lu10 -37.9(6) . . . . ?
Lu3 C52 C70 Lu10 -5.8(3) . . . . ?
Lu6 C52 C70 Lu10 -19.6(3) . . . . ?
C51 C52 C70 Lu11 86.2(6) . . . . ?
C53 C52 C70 Lu11 -61.7(6) . . . . ?
Lu10 C52 C70 Lu11 37.9(6) . . . . ?
Lu5 C52 C70 Lu11 45.3(6) . . . . ?
Lu3 C52 C70 Lu11 32.1(6) . . . . ?
Lu6 C52 C70 Lu11 18.3(6) . . . . ?
C55 C54 C71 C70 -144.0 . . . . ?
C53 C54 C71 C70 1.4 . . . . ?
Lu11 C54 C71 C70 -56.5(5) . . . . ?
C55 C54 C71 C72 1.4 . . . . ?
C53 C54 C71 C72 146.8 . . . . ?
Lu11 C54 C71 C72 88.9(5) . . . . ?
C69 C70 C71 C54 152.9 . . . . ?
C52 C70 C71 C54 0.2 . . . . ?
Lu5 C70 C71 C54 77.42(18) . . . . ?
Lu10 C70 C71 C54 61.9(4) . . . . ?
Lu11 C70 C71 C54 44.4(5) . . . . ?
C69 C70 C71 C72 6.2 . . . . ?
C52 C70 C71 C72 -146.5 . . . . ?
Lu5 C70 C71 C72 -69.32(18) . . . . ?
Lu10 C70 C71 C72 -84.8(4) . . . . ?
Lu11 C70 C71 C72 -102.4(5) . . . . ?
C58 C57 C72 C73 -1.0 . . . . ?
C56 C57 C72 C73 155.0 . . . . ?
C58 C57 C72 C71 -147.5 . . . . ?
C56 C57 C72 C71 8.5 . . . . ?
C54 C71 C72 C73 -146.7 . . . . ?
C70 C71 C72 C73 -5.4 . . . . ?
C54 C71 C72 C57 -2.4 . . . . ?
C70 C71 C72 C57 139.0 . . . . ?
C57 C72 C73 C75 -1.6 . . . . ?
C71 C72 C73 C75 144.7 . . . . ?
C57 C72 C73 C74 -143.3 . . . . ?
C71 C72 C73 C74 3.0 . . . . ?
C57 C72 C73 Lu9 -55.0(4) . . . . ?
C71 C72 C73 Lu9 91.3(4) . . . . ?
C70 C69 C74 C73 6.1 . . . . ?
C68 C69 C74 C73 151.8 . . . . ?
Lu5 C69 C74 C73 95.00(12) . . . . ?
Lu10 C69 C74 C73 88.2(2) . . . . ?
C70 C69 C74 C65 -136.2 . . . . ?
C68 C69 C74 C65 9.6 . . . . ?
Lu5 C69 C74 C65 -47.24(12) . . . . ?
Lu10 C69 C74 C65 -54.0(2) . . . . ?
C70 C69 C74 Lu5 -88.95(12) . . . . ?
C68 C69 C74 Lu5 56.80(12) . . . . ?
Lu10 C69 C74 Lu5 -6.8(2) . . . . ?
C70 C69 C74 Lu9 -71.7(5) . . . . ?
C68 C69 C74 Lu9 74.0(5) . . . . ?
Lu5 C69 C74 Lu9 17.2(6) . . . . ?
Lu10 C69 C74 Lu9 10.5(6) . . . . ?
C75 C73 C74 C69 -153.8 . . . . ?
C72 C73 C74 C69 -2.6 . . . . ?
Lu9 C73 C74 C69 -104.7(4) . . . . ?
C75 C73 C74 C65 -3.5 . . . . ?
C72 C73 C74 C65 147.7 . . . . ?
Lu9 C73 C74 C65 45.6(4) . . . . ?
C75 C73 C74 Lu5 -93.22(11) . . . . ?
C72 C73 C74 Lu5 58.00(11) . . . . ?
Lu9 C73 C74 Lu5 -44.1(4) . . . . ?
C75 C73 C74 Lu9 -49.1(4) . . . . ?
C72 C73 C74 Lu9 102.1(4) . . . . ?
C64 C65 C74 C69 148.9 . . . . ?
C66 C65 C74 C69 8.4 . . . . ?
Lu9 C65 C74 C69 93.3(4) . . . . ?
Lu4 C65 C74 C69 93.92(8) . . . . ?
Lu8 C65 C74 C69 69.42(12) . . . . ?
C64 C65 C74 C73 2.5 . . . . ?
C66 C65 C74 C73 -137.9 . . . . ?
Lu9 C65 C74 C73 -53.1(4) . . . . ?
Lu4 C65 C74 C73 -52.43(8) . . . . ?
Lu8 C65 C74 C73 -76.92(12) . . . . ?
C64 C65 C74 Lu5 111.49(8) . . . . ?
C66 C65 C74 Lu5 -28.95(8) . . . . ?
Lu9 C65 C74 Lu5 55.9(4) . . . . ?
Lu4 C65 C74 Lu5 56.54(11) . . . . ?
Lu8 C65 C74 Lu5 32.04(14) . . . . ?
C64 C65 C74 Lu9 55.6(4) . . . . ?
C66 C65 C74 Lu9 -84.9(4) . . . . ?
Lu4 C65 C74 Lu9 0.6(5) . . . . ?
Lu8 C65 C74 Lu9 -23.9(5) . . . . ?
C65 C64 C75 C73 -1.8 . . . . ?
C63 C64 C75 C73 142.9 . . . . ?
Lu9 C64 C75 C73 86.2(5) . . . . ?
Lu4 C64 C75 C73 95.19(16) . . . . ?
Lu7 C64 C75 C73 98.6(3) . . . . ?
C65 C64 C75 C76 -144.5 . . . . ?
C63 C64 C75 C76 0.3 . . . . ?
Lu9 C64 C75 C76 -56.4(5) . . . . ?
Lu4 C64 C75 C76 -47.48(16) . . . . ?
Lu7 C64 C75 C76 -44.1(3) . . . . ?
C65 C64 C75 Lu9 -88.1(5) . . . . ?
C63 C64 C75 Lu9 56.7(5) . . . . ?
Lu4 C64 C75 Lu9 9.0(5) . . . . ?
Lu7 C64 C75 Lu9 12.4(6) . . . . ?
C65 C64 C75 Lu4 -97.02(16) . . . . ?
C63 C64 C75 Lu4 47.74(16) . . . . ?
Lu9 C64 C75 Lu4 -9.0(5) . . . . ?
Lu7 C64 C75 Lu4 3.4(4) . . . . ?
C65 C64 C75 Lu7 -100.4(3) . . . . ?
C63 C64 C75 Lu7 44.3(3) . . . . ?
Lu9 C64 C75 Lu7 -12.4(6) . . . . ?
Lu4 C64 C75 Lu7 -3.4(4) . . . . ?
C72 C73 C75 C64 -140.4 . . . . ?
C74 C73 C75 C64 3.6 . . . . ?
Lu9 C73 C75 C64 -65.0(6) . . . . ?
C72 C73 C75 C76 2.9 . . . . ?
C74 C73 C75 C76 146.9 . . . . ?
Lu9 C73 C75 C76 78.3(6) . . . . ?
C72 C73 C75 Lu9 -75.4(6) . . . . ?
C74 C73 C75 Lu9 68.6(6) . . . . ?
C72 C73 C75 Lu4 -71.69(16) . . . . ?
C74 C73 C75 Lu4 72.31(15) . . . . ?
Lu9 C73 C75 Lu4 3.7(7) . . . . ?
C72 C73 C75 Lu7 -68.2(3) . . . . ?
C74 C73 C75 Lu7 75.8(3) . . . . ?
Lu9 C73 C75 Lu7 7.2(7) . . . . ?
C62 C61 C76 C58 -148.7 . . . . ?
C60 C61 C76 C58 -1.8 . . . . ?
Lu4 C61 C76 C58 -93.90(18) . . . . ?
Lu7 C61 C76 C58 -87.8(4) . . . . ?
Lu9 C61 C76 C58 -96.2(6) . . . . ?
C62 C61 C76 C75 -6.1 . . . . ?
C60 C61 C76 C75 140.8 . . . . ?
Lu4 C61 C76 C75 48.67(18) . . . . ?
Lu7 C61 C76 C75 54.8(4) . . . . ?
Lu9 C61 C76 C75 46.4(6) . . . . ?
C62 C61 C76 Lu9 -52.4(6) . . . . ?
C60 C61 C76 Lu9 94.4(6) . . . . ?
Lu4 C61 C76 Lu9 2.3(6) . . . . ?
Lu7 C61 C76 Lu9 8.4(7) . . . . ?
C62 C61 C76 Lu4 -54.77(18) . . . . ?
C60 C61 C76 Lu4 92.13(18) . . . . ?
Lu7 C61 C76 Lu4 6.1(5) . . . . ?
Lu9 C61 C76 Lu4 -2.3(6) . . . . ?
C62 C61 C76 Lu7 -60.9(4) . . . . ?
C60 C61 C76 Lu7 86.0(4) . . . . ?
Lu4 C61 C76 Lu7 -6.1(5) . . . . ?
Lu9 C61 C76 Lu7 -8.4(7) . . . . ?
C57 C58 C76 C61 144.0 . . . . ?
C59 C58 C76 C61 1.2 . . . . ?
Lu9 C58 C76 C61 73.2(4) . . . . ?
Lu4 C58 C76 C61 62.3(2) . . . . ?
C57 C58 C76 C75 -0.3 . . . . ?
C59 C58 C76 C75 -143.1 . . . . ?
Lu9 C58 C76 C75 -71.0(4) . . . . ?
Lu4 C58 C76 C75 -82.0(2) . . . . ?
C57 C58 C76 Lu9 70.8(4) . . . . ?
C59 C58 C76 Lu9 -72.0(4) . . . . ?
Lu4 C58 C76 Lu9 -11.0(4) . . . . ?
C57 C58 C76 Lu4 81.7(2) . . . . ?
C59 C58 C76 Lu4 -61.1(2) . . . . ?
Lu9 C58 C76 Lu4 11.0(4) . . . . ?
C57 C58 C76 Lu7 89.6(3) . . . . ?
C59 C58 C76 Lu7 -53.2(3) . . . . ?
Lu9 C58 C76 Lu7 18.9(4) . . . . ?
Lu4 C58 C76 Lu7 7.9(3) . . . . ?
C64 C75 C76 C61 3.0 . . . . ?
C73 C75 C76 C61 -141.2 . . . . ?
Lu9 C75 C76 C61 -47.4(6) . . . . ?
Lu4 C75 C76 C61 -41.84(12) . . . . ?
Lu7 C75 C76 C61 -41.1(5) . . . . ?
C64 C75 C76 C58 142.4 . . . . ?
C73 C75 C76 C58 -1.8 . . . . ?
Lu9 C75 C76 C58 92.0(6) . . . . ?
Lu4 C75 C76 C58 97.55(12) . . . . ?
Lu7 C75 C76 C58 98.3(5) . . . . ?
C64 C75 C76 Lu9 50.5(6) . . . . ?
C73 C75 C76 Lu9 -93.7(6) . . . . ?
Lu4 C75 C76 Lu9 5.6(6) . . . . ?
Lu7 C75 C76 Lu9 6.3(8) . . . . ?
C64 C75 C76 Lu4 44.88(12) . . . . ?
C73 C75 C76 Lu4 -99.33(12) . . . . ?
Lu9 C75 C76 Lu4 -5.6(6) . . . . ?
Lu7 C75 C76 Lu4 0.7(5) . . . . ?
C64 C75 C76 Lu7 44.2(5) . . . . ?
C73 C75 C76 Lu7 -100.0(5) . . . . ?
Lu9 C75 C76 Lu7 -6.3(8) . . . . ?
Lu4 C75 C76 Lu7 -0.7(5) . . . . ?
N4A Ni1A N1A C2A 0.3 . . . . ?
N2A Ni1A N1A C2A 178.0 . . . . ?
N4A Ni1A N1A C1A -177.8 . . . . ?
N2A Ni1A N1A C1A -0.1 . . . . ?
N1A Ni1A N2A C14A 0.6(3) 6_565 . . 6_565 ?
N1A Ni1A N2A C14A -176.9(3) . . . 6_565 ?
N1A Ni1A N2A C14A 176.9(3) 6_565 . . . ?
N1A Ni1A N2A C14A -0.6(3) . . . . ?
N1A Ni1A N4A C4A -0.7(3) 6_565 . . 6_565 ?
N1A Ni1A N4A C4A 176.9(3) . . . 6_565 ?
N1A Ni1A N4A C4A -176.9(3) 6_565 . . . ?
N1A Ni1A N4A C4A 0.7(3) . . . . ?
C2A N1A C1A C13A -179.2(3) . . . . ?
Ni1A N1A C1A C13A -0.7(3) . . . . ?
C2A N1A C1A C10A -0.3(3) . . . . ?
Ni1A N1A C1A C10A 178.1(3) . . . . ?
Ni1A N1A C1A C2A 178.5 . . . . ?
C1A N1A C2A C3A 178.6 . . . . ?
Ni1A N1A C2A C3A 0.2 . . . . ?
C1A N1A C2A C7A 0.5(3) . . . . ?
Ni1A N1A C2A C7A -178.0(3) . . . . ?
Ni1A N1A C2A C1A -178.5 . . . . ?
N1A C2A C3A C4A -1.8(3) . . . . ?
C7A C2A C3A C4A 176.1(4) . . . . ?
C1A C2A C3A C4A 1.0(3) . . . . ?
C2A C3A C4A N4A 2.9(6) . . . . ?
C2A C3A C4A C5A -175.2(4) . . . . ?
C2A C3A C4A C4A 1.3(9) . . . 6_565 ?
C4A N4A C4A C3A -179.23(15) 6_565 . . . ?
Ni1A N4A C4A C3A -2.3(6) . . . . ?
C4A N4A C4A C5A -0.9(6) 6_565 . . . ?
Ni1A N4A C4A C5A 176.0(3) . . . . ?
Ni1A N4A C4A C4A 176.9(4) . . . 6_565 ?
C3A C4A C5A C5A 178.9(4) . . . 6_565 ?
N4A C4A C5A C5A 0.6(4) . . . 6_565 ?
C4A C4A C5A C5A -0.003(2) 6_565 . . 6_565 ?
C3A C4A C5A C6A 3.3(8) . . . . ?
N4A C4A C5A C6A -175.0(4) . . . . ?
C4A C4A C5A C6A -175.6(5) 6_565 . . . ?
C5A C5A C6A C18A -95.3(5) 6_565 . . . ?
C4A C5A C6A C18A 79.3(6) . . . . ?
C3A C2A C7A C10A -178.6(3) . . . . ?
N1A C2A C7A C10A -0.5(5) . . . . ?
C1A C2A C7A C10A -0.2(4) . . . . ?
C3A C2A C7A C8A 0.0(7) . . . . ?
N1A C2A C7A C8A 178.1(5) . . . . ?
C1A C2A C7A C8A 178.4(6) . . . . ?
C10A C7A C8A C9A 101.8(7) . . . . ?
C2A C7A C8A C9A -76.5(7) . . . . ?
C2A C7A C10A C1A 0.2(6) . . . . ?
C8A C7A C10A C1A -178.2(6) . . . . ?
C2A C7A C10A C11A 176.0(6) . . . . ?
C8A C7A C10A C11A -2.5(11) . . . . ?
C13A C1A C10A C7A 178.9(4) . . . . ?
N1A C1A C10A C7A 0.0(5) . . . . ?
C2A C1A C10A C7A -0.2(4) . . . . ?
C13A C1A C10A C11A 2.9(7) . . . . ?
N1A C1A C10A C11A -176.0(5) . . . . ?
C2A C1A C10A C11A -176.2(6) . . . . ?
C7A C10A C11A C12A -100.3(8) . . . . ?
C1A C10A C11A C12A 74.8(7) . . . . ?
N1A C1A C13A C14A 2.4(7) . . . . ?
C10A C1A C13A C14A -176.3(5) . . . . ?
C2A C1A C13A C14A 0.6(12) . . . . ?
C1A C13A C14A N2A -3.2(8) . . . . ?
C1A C13A C14A C15A 174.7(4) . . . . ?
C1A C13A C14A C14A -1.6(15) . . . 6_565 ?
C14A N2A C14A C13A 179.2(3) 6_565 . . . ?
Ni1A N2A C14A C13A 2.3(7) . . . . ?
C14A N2A C14A C15A 1.1(6) 6_565 . . . ?
Ni1A N2A C14A C15A -175.9(3) . . . . ?
Ni1A N2A C14A C14A -177.0(5) . . . 6_565 ?
C13A C14A C15A C15A -178.9(4) . . . 6_565 ?
N2A C14A C15A C15A -0.7(4) . . . 6_565 ?
C14A C14A C15A C15A -0.001(2) 6_565 . . 6_565 ?
C13A C14A C15A C16A -2.8(8) . . . . ?
N2A C14A C15A C16A 175.4(5) . . . . ?
C14A C14A C15A C16A 176.1(6) 6_565 . . . ?
C15A C15A C16A C17A 100.7(5) 6_565 . . . ?
C14A C15A C16A C17A -74.4(7) . . . . ?
C6B C1B C2B C3B 0.000(1) . . . . ?
C1B C2B C3B C4B 0.000(1) . . . . ?
C2B C3B C4B C5B 0.000(2) . . . . ?
C3B C4B C5B C6B 0.000(1) . . . . ?
C2B C1B C6B C5B 0.000(1) . . . . ?
C4B C5B C6B C1B 0.000(1) . . . . ?
C9B C7B C8B C9B 6.9(16) . . . 2_656 ?
C8B C7B C9B C8B -7.7(17) . . . 2_656 ?

_refine_diff_density_max         1.498
_refine_diff_density_min         -1.034
_refine_diff_density_rms         0.144


_vrf_PLAT029_Lu2@Td-C76          
;
PROBLEM: PLAT029 Type_3  _diffrn_measured_fraction_theta_full value Low 
RESPONSE: Because of limited beamtime available, data was collected from only 
one crystal. The completeness of this data especialy in the highest resolution 
shell was restrained by some shaded areas (cryo-system or the beamstop)
;

_vrf_PLAT307_Lu2@Td-C76          
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2@Td-C76          
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2@D3h-C78
_database_code_depnum_ccdc_archive 'CCDC 1582215'
_audit_update_record             
;
2017-10-26 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2@D3h-C78 Ni(OEP)'
_chemical_name_common            'Lu2@D3h-C78 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C78, C36 H44 N4 Ni, 2(C6 H6)'
_chemical_formula_sum            'C126 H56 Lu2 N4 Ni'
_chemical_formula_weight         2034.39

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0027 0.0014 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0053 0.0028 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3436 0.9622 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.2922 5.1425 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   25.274(5)
_cell_length_b                   14.939(5)
_cell_length_c                   19.653(5)
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 93.796(5)
_cell_angle_gamma                90.000(5)
_cell_volume                     7404(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9171
_cell_measurement_theta_min      2.492
_cell_measurement_theta_max      23.138

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.825
_exptl_crystal_F_000             4040
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.180
_exptl_crystal_size_mid          0.120
_exptl_crystal_size_min          0.100
_exptl_absorpt_coefficient_mu    2.409
_shelx_estimated_absorpt_T_min   0.742
_shelx_estimated_absorpt_T_max   0.786
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.3879
_exptl_absorpt_correction_T_max  0.7449
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline BL17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            49423
_diffrn_reflns_av_unetI/netI     0.0257
_diffrn_reflns_av_R_equivalents  0.0389
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_h_max       30
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         0.953
_diffrn_reflns_theta_max         23.144
_diffrn_reflns_theta_full        23.048
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measured_fraction_theta_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_point_group_measured_fraction_full 0.992
_reflns_number_total             7021
_reflns_number_gt                6327
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1747P)²+89.9882P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7021
_refine_ls_number_parameters     801
_refine_ls_number_restraints     774
_refine_ls_R_factor_all          0.0997
_refine_ls_R_factor_gt           0.0928
_refine_ls_wR_factor_ref         0.2807
_refine_ls_wR_factor_gt          0.2724
_refine_ls_goodness_of_fit_ref   1.055
_refine_ls_restrained_S_all      1.096
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.26079(6) 0.0000 0.38803(7) 0.0334(3) Uani 0.3825 2 d S TU P A 2
Lu2 Lu 0.33864(6) 0.07865(9) 0.27630(8) 0.0376(4) Uani 0.2593 1 d . U P A 2
Lu3 Lu 0.37872(17) 0.0370(4) 0.3586(3) 0.1112(18) Uani 0.1277 1 d . U P A 2
Lu4 Lu 0.3362(5) 0.1066(9) 0.3022(7) 0.134(3) Uani 0.0995 1 d . U P A 2
Lu5 Lu 0.2564(5) -0.0422(10) 0.3741(8) 0.144(4) Uani 0.0917 1 d . U P A 2
Lu6 Lu 0.3072(6) 0.1245(8) 0.2917(9) 0.109(3) Uani 0.0691 1 d . U P A 2
Lu7 Lu 0.2335(3) -0.0276(8) 0.3533(5) 0.085(3) Uani 0.0679 1 d . U P A 2
Lu8 Lu 0.3564(10) 0.0000 0.3982(13) 0.164(6) Uani 0.0664 2 d S TU P A 2
Lu9 Lu 0.3109(6) 0.1015(9) 0.2511(5) 0.096(3) Uani 0.0603 1 d . U P A 2
C1 C 0.40799(4) -0.0177(3) 0.18474(5) 0.078(5) Uani 0.5 1 d G U P B -1
C2 C 0.36591(4) -0.0489(3) 0.14937(7) 0.073(4) Uani 0.5 1 d G U P B -1
C3 C 0.34996(7) -0.1422(3) 0.16381(12) 0.072(4) Uani 0.5 1 d G U P B -1
C4 C 0.39115(9) -0.1690(2) 0.21579(13) 0.072(4) Uani 0.5 1 d G U P B -1
C5 C 0.42669(6) -0.0896(2) 0.23322(8) 0.076(5) Uani 0.5 1 d G U P B -1
C6 C 0.44567(8) -0.0776(2) 0.29990(7) 0.083(5) Uani 0.5 1 d G U P B -1
C7 C 0.46342(7) 0.0115(2) 0.32002(4) 0.093(5) Uani 0.5 1 d G U P B -1
C8 C 0.45059(7) 0.0883(2) 0.27299(7) 0.090(5) Uani 0.5 1 d G U P B -1
C9 C 0.41313(5) 0.0615(2) 0.20774(7) 0.090(5) Uani 0.5 1 d G U P B -1
C10 C 0.37702(7) 0.1291(2) 0.18199(11) 0.091(5) Uani 0.5 1 d G U P B -1
C11 C 0.33381(5) 0.0923(3) 0.13064(10) 0.080(5) Uani 0.5 1 d G U P B -1
C12 C 0.32411(3) 0.0129(3) 0.12113(8) 0.076(4) Uani 0.5 1 d G U P B -1
C13 C 0.27250(3) -0.0260(3) 0.10908(10) 0.072(4) Uani 0.5 1 d G U P B -1
C14 C 0.26009(6) -0.1161(3) 0.13085(13) 0.074(5) Uani 0.5 1 d G U P B -1
C15 C 0.29711(8) -0.1629(3) 0.16229(15) 0.074(5) Uani 0.5 1 d G U P B -1
C16 C 0.28101(11) -0.2256(2) 0.20447(19) 0.067(4) Uani 0.5 1 d G U P B -1
C17 C 0.32128(13) -0.2541(2) 0.2610(2) 0.079(5) Uani 0.5 1 d G U P B -1
C18 C 0.37225(12) -0.22504(19) 0.27184(17) 0.079(5) Uani 0.5 1 d G U P B -1
C19 C 0.39578(12) -0.2074(2) 0.34141(16) 0.074(4) Uani 0.5 1 d G U P B -1
C20 C 0.43119(10) -0.1356(2) 0.36029(11) 0.087(5) Uani 0.5 1 d G U P B -1
C21 C 0.42748(11) -0.0929(2) 0.42938(8) 0.091(5) Uani 0.5 1 d G U P B -1
C22 C 0.43961(11) -0.0112(3) 0.44414(5) 0.095(5) Uani 0.5 1 d G U P B -1
C23 C 0.45958(9) 0.0411(2) 0.39017(5) 0.095(5) Uani 0.5 1 d G U P B -1
C24 C 0.44673(10) 0.1363(2) 0.38816(10) 0.095(5) Uani 0.5 1 d G U P B -1
C25 C 0.43631(9) 0.1636(2) 0.31723(12) 0.078(4) Uani 0.5 1 d G U P B -1
C26 C 0.39679(11) 0.2290(2) 0.28813(17) 0.087(5) Uani 0.5 1 d G U P B -1
C27 C 0.36998(10) 0.2112(2) 0.22102(16) 0.079(5) Uani 0.5 1 d G U P B -1
C28 C 0.31772(10) 0.2215(2) 0.19190(18) 0.102(5) Uani 0.5 1 d G U P B -1
C29 C 0.28881(7) 0.1609(3) 0.13838(15) 0.079(5) Uani 0.5 1 d G U P B -1
C30 C 0.24061(6) 0.1266(3) 0.12981(15) 0.077(5) Uani 0.5 1 d G U P B -1
C31 C 0.22834(3) 0.0321(3) 0.11222(12) 0.078(5) Uani 0.5 1 d G U P B -1
C32 C 0.18724(4) -0.0230(3) 0.13769(14) 0.078(3) Uani 0.5 1 d G U P B -1
C33 C 0.21021(6) -0.1080(3) 0.14480(15) 0.078(3) Uani 0.5 1 d G U P B -1
C34 C 0.19240(8) -0.1571(3) 0.19321(18) 0.075(3) Uani 0.5 1 d G U P B -1
C35 C 0.22569(11) -0.2183(3) 0.2224(2) 0.072(3) Uani 0.5 1 d G U P B -1
C36 C 0.21023(12) -0.2220(3) 0.2939(2) 0.077(3) Uani 0.5 1 d G U P B -1
C37 C 0.24954(14) -0.2329(2) 0.3533(2) 0.102(6) Uani 0.5 1 d G U P B -1
C38 C 0.30514(14) -0.2579(2) 0.3343(2) 0.090(5) Uani 0.5 1 d G U P B -1
C39 C 0.34827(14) -0.2235(2) 0.38250(17) 0.097(5) Uani 0.5 1 d G U P B -1
C40 C 0.34431(14) -0.1743(3) 0.44656(15) 0.105(6) Uani 0.5 1 d G U P B -1
C41 C 0.38170(13) -0.1120(3) 0.46550(10) 0.107(6) Uani 0.5 1 d G U P B -1
C42 C 0.36538(13) -0.0282(3) 0.50559(7) 0.092(6) Uani 0.5 1 d G U P B -1
C43 C 0.40569(12) 0.0298(3) 0.48838(6) 0.096(6) Uani 0.5 1 d G U P B -1
C44 C 0.38970(13) 0.1270(3) 0.48251(11) 0.095(5) Uani 0.5 1 d G U P B -1
C45 C 0.40588(12) 0.1721(2) 0.42980(13) 0.100(5) Uani 0.5 1 d G U P B -1
C46 C 0.37064(13) 0.2336(2) 0.40259(18) 0.080(5) Uani 0.5 1 d G U P B -1
C47 C 0.36535(13) 0.26496(19) 0.3318(2) 0.096(5) Uani 0.5 1 d G U P B -1
C48 C 0.30995(13) 0.27420(19) 0.2972(2) 0.089(5) Uani 0.5 1 d G U P B -1
C49 C 0.28515(11) 0.2489(2) 0.2320(2) 0.101(6) Uani 0.5 1 d G U P B -1
C50 C 0.23146(11) 0.2240(2) 0.2408(2) 0.086(5) Uani 0.5 1 d G U P B -1
C51 C 0.21125(8) 0.1665(3) 0.17667(18) 0.098(5) Uani 0.5 1 d G U P B -1
C52 C 0.15882(6) 0.1009(3) 0.20592(17) 0.090(5) Uani 0.5 1 d G U P B -1
C53 C 0.15387(4) 0.0223(3) 0.18520(16) 0.096(5) Uani 0.5 1 d G U P B -1
C54 C 0.13739(6) -0.0319(3) 0.24703(17) 0.087(5) Uani 0.5 1 d G U P B -1
C55 C 0.15940(8) -0.1300(3) 0.24730(18) 0.086(5) Uani 0.5 1 d G U P B -1
C56 C 0.16827(11) -0.1656(3) 0.31050(19) 0.078(5) Uani 0.5 1 d G U P B -1
C57 C 0.15903(10) -0.1014(3) 0.36624(17) 0.097(5) Uani 0.5 1 d G U P B -1
C58 C 0.20385(12) -0.1200(3) 0.43664(16) 0.103(5) Uani 0.5 1 d G U P B -1
C59 C 0.24395(14) -0.1903(3) 0.42058(18) 0.107(6) Uani 0.5 1 d G U P B -1
C60 C 0.28935(14) -0.1594(3) 0.46757(15) 0.093(5) Uani 0.5 1 d G U P B -1
C61 C 0.28242(13) -0.0799(3) 0.50157(12) 0.084(5) Uani 0.5 1 d G U P B -1
C62 C 0.31080(13) 0.0883(3) 0.50474(11) 0.096(5) Uani 0.5 1 d G U P B -1
C63 C 0.31665(13) 0.0134(3) 0.51565(9) 0.095(5) Uani 0.5 1 d G U P B -1
C64 C 0.33716(13) 0.1416(3) 0.48997(13) 0.087(5) Uani 0.5 1 d G U P B -1
C65 C 0.31878(14) 0.2303(2) 0.42905(19) 0.097(5) Uani 0.5 1 d G U P B -1
C66 C 0.27602(13) 0.2199(3) 0.41379(19) 0.087(5) Uani 0.5 1 d G U P B -1
C67 C 0.27113(13) 0.2597(2) 0.3460(2) 0.100(6) Uani 0.5 1 d G U P B -1
C68 C 0.22414(12) 0.2243(2) 0.3135(2) 0.094(5) Uani 0.5 1 d G U P B -1
C69 C 0.18208(10) 0.1634(3) 0.32870(19) 0.080(5) Uani 0.5 1 d G U P B -1
C70 C 0.15349(8) 0.1184(3) 0.27796(18) 0.076(5) Uani 0.5 1 d G U P B -1
C71 C 0.13739(7) 0.0205(3) 0.30208(17) 0.090(5) Uani 0.5 1 d G U P B -1
C72 C 0.14752(9) 0.0130(3) 0.36305(17) 0.095(5) Uani 0.5 1 d G U P B -1
C73 C 0.16985(11) 0.0554(3) 0.41774(16) 0.092(5) Uani 0.5 1 d G U P B -1
C74 C 0.20521(12) 0.0369(3) 0.47204(14) 0.090(5) Uani 0.5 1 d G U P B -1
C75 C 0.23578(13) -0.0458(3) 0.49085(13) 0.099(6) Uani 0.5 1 d G U P B -1
C76 C 0.24621(13) 0.0970(3) 0.48831(14) 0.089(5) Uani 0.5 1 d G U P B -1
C77 C 0.23789(12) 0.1688(3) 0.43461(17) 0.092(5) Uani 0.5 1 d G U P B -1
C78 C 0.18860(11) 0.1403(3) 0.39248(18) 0.084(5) Uani 0.5 1 d G U P B -1
Ni1A Ni 0.48054(3) 0.0000(4) 0.08314(4) 0.0166(3) Uani 1 2 d G T P B 2
C1A C 0.58966(9) 0.1487(3) 0.34641(12) 0.0404(14) Uani 1 1 d G . . B 2
H1AA H 0.6105 0.1862 0.3775 0.061 Uiso 1 1 calc R U . B 2
H1AB H 0.5740 0.1014 0.3713 0.061 Uiso 1 1 calc R U . B 2
H1AC H 0.5622 0.1837 0.3232 0.061 Uiso 1 1 calc R U . B 2
N3A N 0.47942(15) 0.1313(3) 0.0841(2) 0.0217(9) Uani 1 1 d . . . B 2
N2A N 0.4236(2) 0.0000 0.0112(3) 0.0190(12) Uani 1 2 d S T P B 2
C3A C 0.5960(2) 0.0451(4) 0.2459(3) 0.0259(11) Uani 1 1 d . . . B 2
C4A C 0.55883(19) 0.0726(3) 0.1912(3) 0.0218(10) Uani 1 1 d . . . B 2
C5A C 0.54748(19) 0.1608(3) 0.1754(3) 0.0232(11) Uani 1 1 d . . . B 2
H5A H 0.5668 0.2048 0.1994 0.028 Uiso 1 1 calc R U . B 2
C6A C 0.50956(19) 0.1877(3) 0.1267(3) 0.0229(10) Uani 1 1 d . . . B 2
C7A C 0.4960(2) 0.2802(3) 0.1134(3) 0.0289(12) Uani 1 1 d . . . B 2
C8A C 0.5199(3) 0.3580(4) 0.1531(4) 0.0417(16) Uani 1 1 d . . . B 2
H8AA H 0.5126 0.4126 0.1274 0.050 Uiso 1 1 calc R U . B 2
H8AB H 0.5580 0.3504 0.1581 0.050 Uiso 1 1 calc R U . B 2
C9A C 0.4988(3) 0.3682(5) 0.2235(4) 0.056(2) Uani 1 1 d . . . B 2
H9AA H 0.5172 0.4161 0.2475 0.084 Uiso 1 1 calc R U . B 2
H9AB H 0.5044 0.3135 0.2486 0.084 Uiso 1 1 calc R U . B 2
H9AC H 0.4616 0.3814 0.2188 0.084 Uiso 1 1 calc R U . B 2
C10A C 0.3721(3) 0.3690(5) 0.0566(4) 0.0485(17) Uani 1 1 d . . . B 2
H10A H 0.3546 0.4190 0.0344 0.073 Uiso 1 1 calc R U . B 2
H10B H 0.3753 0.3790 0.1049 0.073 Uiso 1 1 calc R U . B 2
H10C H 0.3518 0.3156 0.0470 0.073 Uiso 1 1 calc R U . B 2
C11A C 0.4274(2) 0.3581(4) 0.0301(4) 0.0382(15) Uani 1 1 d . . . B 2
H11A H 0.4240 0.3496 -0.0189 0.046 Uiso 1 1 calc R U . B 2
H11B H 0.4476 0.4126 0.0393 0.046 Uiso 1 1 calc R U . B 2
C12A C 0.4573(2) 0.2800(3) 0.0627(3) 0.0284(12) Uani 1 1 d . . . B 2
C13A C 0.44724(19) 0.1874(3) 0.0450(3) 0.0225(10) Uani 1 1 d . . . B 2
C15A C 0.40933(19) 0.1603(3) -0.0041(3) 0.0224(10) Uani 1 1 d . . . B 2
H15A H 0.3903 0.2043 -0.0286 0.027 Uiso 1 1 calc R U . B 2
C16A C 0.39773(18) 0.0726(3) -0.0191(3) 0.0199(10) Uani 1 1 d . . . B 2
C17A C 0.35568(19) 0.0454(3) -0.0677(3) 0.0217(10) Uani 1 1 d . . . B 2
C18A C 0.3176(2) 0.1082(4) -0.1052(3) 0.0262(11) Uani 1 1 d . . . B 2
H18A H 0.3020 0.0786 -0.1457 0.031 Uiso 1 1 calc R U . B 2
H18B H 0.3367 0.1603 -0.1197 0.031 Uiso 1 1 calc R U . B 2
C19A C 0.2735(2) 0.1382(5) -0.0612(3) 0.0410(15) Uani 1 1 d . . . B 2
H19A H 0.2483 0.1738 -0.0881 0.062 Uiso 1 1 calc R U . B 2
H19B H 0.2884 0.1732 -0.0237 0.062 Uiso 1 1 calc R U . B 2
H19C H 0.2560 0.0866 -0.0441 0.062 Uiso 1 1 calc R U . B 2
C2A C 0.6251(2) 0.1086(4) 0.2943(3) 0.0336(13) Uani 1 1 d . . . B 2
H2AA H 0.6399 0.1567 0.2685 0.040 Uiso 1 1 calc R U . B 2
H2AB H 0.6542 0.0771 0.3183 0.040 Uiso 1 1 calc R U . B 2
N1A N 0.5353(2) 0.0000 0.1577(3) 0.0208(12) Uani 1 2 d S T P B 2
C1B C 0.3759(4) 0.5000 0.3049(6) 0.062(3) Uani 1 2 d S T P C 3
H1B H 0.4118 0.5000 0.3184 0.074 Uiso 1 2 calc R U P C 3
C2B C 0.3593(4) 0.5000 0.2376(5) 0.045(2) Uani 1 2 d S T P C 3
H2B H 0.3844 0.5000 0.2051 0.054 Uiso 1 2 calc R U P C 3
C3B C 0.3072(4) 0.5000 0.2167(5) 0.040(2) Uani 1 2 d S T P C 3
H3B H 0.2967 0.5000 0.1704 0.048 Uiso 1 2 calc R U P C 3
C4B C 0.2695(4) 0.5000 0.2650(5) 0.046(2) Uani 1 2 d S T P C 3
H4B H 0.2337 0.5000 0.2511 0.055 Uiso 1 2 calc R U P C 3
C5B C 0.2851(5) 0.5000 0.3338(5) 0.059(3) Uani 1 2 d S T P C 3
H5B H 0.2600 0.5000 0.3662 0.071 Uiso 1 2 calc R U P C 3
C6B C 0.3379(6) 0.5000 0.3533(6) 0.078(4) Uani 1 2 d S T P C 3
H6B H 0.3488 0.5000 0.3994 0.093 Uiso 1 2 calc R U P C 3
C1C C 0.5294(5) 0.3605(9) 0.4402(7) 0.090(3) Uani 1 1 d . . . D 4
H1C H 0.5473 0.3512 0.4009 0.108 Uiso 1 1 calc R U . D 4
C2C C 0.4743(8) 0.3682(16) 0.4405(10) 0.153(8) Uani 1 1 d . . . D 4
H2C H 0.4551 0.3739 0.3986 0.184 Uiso 1 1 calc R U . D 4
C3C C 0.4465(6) 0.368(2) 0.4983(13) 0.183(11) Uani 1 1 d . . . D 4
H3C H 0.4097 0.3729 0.4940 0.219 Uiso 1 1 calc R U . D 4


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu5 0.693(17) . ?
Lu1 Lu5 0.693(17) 6 ?
Lu1 Lu7 1.025(11) . ?
Lu1 Lu7 1.025(11) 6 ?
Lu1 Lu8 2.41(2) . ?
Lu1 Lu6 2.952(14) 6 ?
Lu1 Lu6 2.952(14) . ?
Lu1 Lu4 3.073(13) 6 ?
Lu1 Lu4 3.073(13) . ?
Lu1 Lu3 3.123(5) 6 ?
Lu1 Lu3 3.123(5) . ?
Lu1 Lu2 3.2628(17) . ?
Lu2 Lu4 0.665(14) . ?
Lu2 Lu9 0.898(12) . ?
Lu2 Lu6 1.107(17) . ?
Lu2 Lu3 1.952(5) . ?
Lu2 Lu2 2.350(3) 6 ?
Lu2 Lu3 2.532(6) 6 ?
Lu2 Lu8 2.68(2) . ?
Lu2 Lu4 2.816(14) 6 ?
Lu2 Lu9 2.817(14) 6 ?
Lu2 Lu5 2.972(14) 6 ?
Lu2 Lu6 3.157(14) 6 ?
Lu2 Lu7 3.236(9) 6 ?
Lu3 Lu3 1.107(12) 6 ?
Lu3 Lu8 1.14(2) . ?
Lu3 Lu4 1.818(14) . ?
Lu3 Lu6 2.528(14) . ?
Lu3 Lu2 2.532(6) 6 ?
Lu3 Lu4 2.614(15) 6 ?
Lu3 Lu9 2.800(12) . ?
Lu3 Lu5 3.126(14) 6 ?
Lu3 Lu6 3.242(14) 6 ?
Lu3 Lu5 3.342(14) . ?
Lu4 Lu6 0.796(14) . ?
Lu4 Lu9 1.156(16) . ?
Lu4 Lu8 2.50(2) . ?
Lu4 Lu3 2.614(15) 6 ?
Lu4 Lu5 2.71(2) 6 ?
Lu4 Lu2 2.816(14) 6 ?
Lu4 Lu7 3.081(16) 6 ?
Lu4 Lu4 3.19(3) 6 ?
Lu4 Lu9 3.317(17) 6 ?
Lu5 Lu7 0.722(14) . ?
Lu5 Lu7 1.249(15) 6 ?
Lu5 Lu5 1.26(3) 6 ?
Lu5 Lu6 2.46(2) 6 ?
Lu5 Lu8 2.62(3) . ?
Lu5 Lu4 2.71(2) 6 ?
Lu5 Lu2 2.972(14) 6 ?
Lu5 Lu9 2.993(19) 6 ?
Lu5 Lu3 3.127(14) 6 ?
Lu5 Lu6 3.278(18) . ?
Lu6 Lu9 0.878(18) . ?
Lu6 Lu5 2.46(2) 6 ?
Lu6 Lu7 2.708(17) 6 ?
Lu6 Lu8 3.01(2) . ?
Lu6 Lu2 3.157(14) 6 ?
Lu6 Lu7 3.224(16) . ?
Lu6 Lu3 3.242(14) 6 ?
Lu7 Lu7 0.82(2) 6 ?
Lu7 Lu5 1.249(15) 6 ?
Lu7 Lu6 2.708(17) 6 ?
Lu7 Lu4 3.081(16) 6 ?
Lu7 Lu9 3.099(15) 6 ?
Lu7 Lu8 3.20(3) . ?
Lu7 Lu2 3.236(9) 6 ?
Lu7 Lu9 3.479(14) . ?
Lu8 Lu3 1.14(2) 6 ?
Lu8 Lu4 2.50(2) 6 ?
Lu8 Lu5 2.62(3) 6 ?
Lu8 Lu2 2.68(2) 6 ?
Lu8 Lu6 3.01(2) 6 ?
Lu9 Lu2 2.817(14) 6 ?
Lu9 Lu5 2.993(19) 6 ?
Lu9 Lu9 3.03(3) 6 ?
Lu9 Lu7 3.100(15) 6 ?
Lu9 Lu4 3.317(17) 6 ?
Lu9 Lu3 3.346(13) 6 ?
C1 C9 1.2697 . ?
C1 C2 1.3164 . ?
C1 C5 1.4920 . ?
C2 C12 1.4825 . ?
C2 C3 1.4839 . ?
C3 C15 1.3696 . ?
C3 C4 1.4650 . ?
C4 C18 1.4876 . ?
C4 C5 1.5129 . ?
C5 C6 1.3772 . ?
C6 C7 1.4512 . ?
C6 C20 1.5332 . ?
C7 C23 1.4574 . ?
C7 C8 1.4957 . ?
C8 C25 1.4809 . ?
C8 C9 1.5940 . ?
C9 C10 1.4316 . ?
C10 C27 1.4637 . ?
C10 C11 1.5387 . ?
C11 C12 1.2240 . ?
C11 C29 1.5450 . ?
C12 C13 1.4330 . ?
C13 C31 1.4177 . ?
C13 C14 1.4525 . ?
C14 C15 1.2923 . ?
C14 C33 1.3134 . ?
C15 C16 1.3327 . ?
C16 C35 1.4683 . ?
C16 C17 1.5174 . ?
C17 C18 1.3627 . ?
C17 C38 1.5235 . ?
C18 C19 1.4781 . ?
C19 C20 1.4298 . ?
C19 C39 1.5100 . ?
C20 C21 1.5087 . ?
C21 C22 1.2874 . ?
C21 C41 1.4259 . ?
C22 C43 1.4015 . ?
C22 C23 1.4356 . ?
C23 C24 1.4587 . ?
C24 C25 1.4595 . ?
C24 C45 1.4607 . ?
C25 C26 1.4840 . ?
C26 C47 1.3220 . ?
C26 C27 1.4664 . ?
C27 C28 1.4126 . ?
C28 C49 1.2457 . ?
C28 C29 1.5356 . ?
C29 C30 1.3217 . ?
C30 C51 1.3583 . ?
C30 C31 1.4824 . ?
C31 C32 1.4408 . ?
C32 C33 1.3995 . ?
C32 C53 1.4650 . ?
C33 C34 1.3044 . ?
C34 C35 1.3454 . ?
C34 C55 1.4514 . ?
C35 C36 1.4839 . ?
C36 C56 1.4098 . ?
C36 C37 1.4920 . ?
C37 C59 1.4818 . ?
C37 C38 1.5244 . ?
C38 C39 1.4879 . ?
C39 C40 1.4664 . ?
C40 C41 1.3607 . ?
C40 C60 1.4919 . ?
C41 C42 1.5501 . ?
C42 C43 1.3958 . ?
C42 C63 1.4051 . ?
C43 C44 1.5098 . ?
C44 C45 1.3229 . ?
C44 C64 1.3631 . ?
C45 C46 1.3636 . ?
C46 C65 1.4426 . ?
C46 C47 1.4657 . ?
C47 C48 1.5216 . ?
C48 C67 1.4327 . ?
C48 C49 1.4400 . ?
C49 C50 1.4282 . ?
C50 C68 1.4542 . ?
C50 C51 1.5811 . ?
C51 C52 1.7745 . ?
C52 C53 1.2458 . ?
C52 C70 1.4549 . ?
C53 C54 1.5404 . ?
C54 C71 1.3351 . ?
C54 C55 1.5685 . ?
C55 C56 1.3558 . ?
C56 C57 1.4858 . ?
C57 C72 1.7340 . ?
C57 C58 1.7514 . ?
C58 C59 1.5070 . ?
C58 C75 1.7031 . ?
C59 C60 1.4974 . ?
C60 C61 1.3788 . ?
C61 C75 1.2885 . ?
C61 C63 1.6543 . ?
C62 C64 1.0902 . ?
C62 C63 1.1463 . ?
C62 C76 1.6483 . ?
C64 C65 1.8250 . ?
C65 C66 1.1132 . ?
C65 C67 2.0120 . ?
C66 C77 1.3153 . ?
C66 C67 1.4572 . ?
C67 C68 1.4133 . ?
C68 C69 1.4456 . ?
C69 C78 1.2997 . ?
C69 C70 1.3681 . ?
C70 C71 1.5987 . ?
C71 C72 1.2139 . ?
C72 C73 1.3395 . ?
C73 C74 1.3737 . ?
C73 C78 1.4534 . ?
C74 C76 1.3920 . ?
C74 C75 1.4915 . ?
C76 C77 1.5098 . ?
C77 C78 1.5108 . ?
Ni1A N2A 1.949(6) . ?
Ni1A N1A 1.949(6) . ?
Ni1A N3A 1.961(7) 6 ?
Ni1A N3A 1.961(7) . ?
C1A C2A 1.526(7) . ?
N3A C13A 1.369(6) . ?
N3A C6A 1.380(6) . ?
N2A C16A 1.382(6) . ?
N2A C16A 1.382(6) 6 ?
C3A C3A 1.348(11) 6 ?
C3A C4A 1.440(7) . ?
C3A C2A 1.501(7) . ?
C4A C5A 1.379(7) . ?
C4A N1A 1.382(6) . ?
C5A C6A 1.370(7) . ?
C6A C7A 1.444(7) . ?
C7A C12A 1.349(8) . ?
C7A C8A 1.504(7) . ?
C8A C9A 1.523(12) . ?
C10A C11A 1.531(9) . ?
C11A C12A 1.509(7) . ?
C12A C13A 1.444(7) . ?
C13A C15A 1.374(7) . ?
C15A C16A 1.371(7) . ?
C16A C17A 1.439(7) . ?
C17A C17A 1.358(10) 6 ?
C17A C18A 1.502(7) . ?
C18A C19A 1.522(8) . ?
N1A C4A 1.382(6) 6 ?
C1B C2B 1.361(15) . ?
C1B C6B 1.394(18) . ?
C2B C3B 1.352(14) . ?
C3B C4B 1.388(14) . ?
C4B C5B 1.382(14) . ?
C5B C6B 1.364(18) . ?
C1C C3C 1.32(2) 2_656 ?
C1C C2C 1.40(2) . ?
C2C C3C 1.38(3) . ?
C3C C1C 1.32(2) 2_656 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu5 Lu1 Lu5 131(2) . 6 ?
Lu5 Lu1 Lu7 44.7(12) . . ?
Lu5 Lu1 Lu7 91.2(14) 6 . ?
Lu5 Lu1 Lu7 91.1(14) . 6 ?
Lu5 Lu1 Lu7 44.7(12) 6 6 ?
Lu7 Lu1 Lu7 47.4(12) . 6 ?
Lu5 Lu1 Lu8 99.5(12) . . ?
Lu5 Lu1 Lu8 99.5(12) 6 . ?
Lu7 Lu1 Lu8 133.1(7) . . ?
Lu7 Lu1 Lu8 133.1(7) 6 . ?
Lu5 Lu1 Lu6 39.9(11) . 6 ?
Lu5 Lu1 Lu6 112.3(12) 6 6 ?
Lu7 Lu1 Lu6 66.3(6) . 6 ?
Lu7 Lu1 Lu6 96.0(6) 6 6 ?
Lu8 Lu1 Lu6 67.4(5) . 6 ?
Lu5 Lu1 Lu6 112.3(12) . . ?
Lu5 Lu1 Lu6 39.9(11) 6 . ?
Lu7 Lu1 Lu6 96.0(6) . . ?
Lu7 Lu1 Lu6 66.3(6) 6 . ?
Lu8 Lu1 Lu6 67.4(5) . . ?
Lu6 Lu1 Lu6 78.1(6) 6 . ?
Lu5 Lu1 Lu4 53.1(11) . 6 ?
Lu5 Lu1 Lu4 110.0(11) 6 6 ?
Lu7 Lu1 Lu4 80.9(6) . 6 ?
Lu7 Lu1 Lu4 105.0(6) 6 6 ?
Lu8 Lu1 Lu4 52.5(5) . 6 ?
Lu6 Lu1 Lu4 15.0(3) 6 6 ?
Lu6 Lu1 Lu4 71.8(4) . 6 ?
Lu5 Lu1 Lu4 110.0(11) . . ?
Lu5 Lu1 Lu4 53.1(11) 6 . ?
Lu7 Lu1 Lu4 105.0(6) . . ?
Lu7 Lu1 Lu4 80.9(6) 6 . ?
Lu8 Lu1 Lu4 52.5(5) . . ?
Lu6 Lu1 Lu4 71.8(4) 6 . ?
Lu6 Lu1 Lu4 15.0(3) . . ?
Lu4 Lu1 Lu4 62.5(6) 6 . ?
Lu5 Lu1 Lu3 83.9(11) . 6 ?
Lu5 Lu1 Lu3 102.5(11) 6 6 ?
Lu7 Lu1 Lu3 114.5(5) . 6 ?
Lu7 Lu1 Lu3 123.9(5) 6 6 ?
Lu8 Lu1 Lu3 18.6(5) . 6 ?
Lu6 Lu1 Lu3 49.1(3) 6 6 ?
Lu6 Lu1 Lu3 64.4(3) . 6 ?
Lu4 Lu1 Lu3 34.1(3) 6 6 ?
Lu4 Lu1 Lu3 49.9(3) . 6 ?
Lu5 Lu1 Lu3 102.5(11) . . ?
Lu5 Lu1 Lu3 83.9(11) 6 . ?
Lu7 Lu1 Lu3 123.9(5) . . ?
Lu7 Lu1 Lu3 114.5(5) 6 . ?
Lu8 Lu1 Lu3 18.6(5) . . ?
Lu6 Lu1 Lu3 64.4(3) 6 . ?
Lu6 Lu1 Lu3 49.1(3) . . ?
Lu4 Lu1 Lu3 49.9(3) 6 . ?
Lu4 Lu1 Lu3 34.1(3) . . ?
Lu3 Lu1 Lu3 20.4(2) 6 . ?
Lu5 Lu1 Lu2 98.5(11) . . ?
Lu5 Lu1 Lu2 59.6(11) 6 . ?
Lu7 Lu1 Lu2 96.1(5) . . ?
Lu7 Lu1 Lu2 79.5(5) 6 . ?
Lu8 Lu1 Lu2 53.9(6) . . ?
Lu6 Lu1 Lu2 60.8(3) 6 . ?
Lu6 Lu1 Lu2 19.7(3) . . ?
Lu4 Lu1 Lu2 52.7(3) 6 . ?
Lu4 Lu1 Lu2 11.5(3) . . ?
Lu3 Lu1 Lu2 46.65(11) 6 . ?
Lu3 Lu1 Lu2 35.51(10) . . ?
Lu4 Lu2 Lu9 94.3(14) . . ?
Lu4 Lu2 Lu6 45.4(12) . . ?
Lu9 Lu2 Lu6 50.7(9) . . ?
Lu4 Lu2 Lu3 68.6(12) . . ?
Lu9 Lu2 Lu3 157.0(9) . . ?
Lu6 Lu2 Lu3 108.3(8) . . ?
Lu4 Lu2 Lu2 129.0(11) . 6 ?
Lu9 Lu2 Lu2 112.4(8) . 6 ?
Lu6 Lu2 Lu2 128.2(6) . 6 ?
Lu3 Lu2 Lu2 71.43(18) . 6 ?
Lu4 Lu2 Lu3 89.6(12) . 6 ?
Lu9 Lu2 Lu3 151.2(7) . 6 ?
Lu6 Lu2 Lu3 120.8(8) . 6 ?
Lu3 Lu2 Lu3 24.5(3) . 6 ?
Lu2 Lu2 Lu3 46.95(13) 6 6 ?
Lu4 Lu2 Lu8 67.0(12) . . ?
Lu9 Lu2 Lu8 137.5(10) . . ?
Lu6 Lu2 Lu8 96.2(9) . . ?
Lu3 Lu2 Lu8 22.0(5) . . ?
Lu2 Lu2 Lu8 64.0(2) 6 . ?
Lu3 Lu2 Lu8 25.0(4) 6 . ?
Lu4 Lu2 Lu4 118.4(14) . 6 ?
Lu9 Lu2 Lu4 116.6(8) . 6 ?
Lu6 Lu2 Lu4 122.3(7) . 6 ?
Lu3 Lu2 Lu4 63.5(3) . 6 ?
Lu2 Lu2 Lu4 10.6(3) 6 6 ?
Lu3 Lu2 Lu4 39.3(3) 6 6 ?
Lu8 Lu2 Lu4 54.0(4) . 6 ?
Lu4 Lu2 Lu9 134.5(11) . 6 ?
Lu9 Lu2 Lu9 95.2(10) . 6 ?
Lu6 Lu2 Lu9 117.7(6) . 6 ?
Lu3 Lu2 Lu9 87.2(3) . 6 ?
Lu2 Lu2 Lu9 17.1(2) 6 6 ?
Lu3 Lu2 Lu9 62.9(3) 6 6 ?
Lu8 Lu2 Lu9 76.3(3) . 6 ?
Lu4 Lu2 Lu9 23.7(3) 6 6 ?
Lu4 Lu2 Lu5 61.1(11) . 6 ?
Lu9 Lu2 Lu5 82.7(9) . 6 ?
Lu6 Lu2 Lu5 52.5(8) . 6 ?
Lu3 Lu2 Lu5 75.7(3) . 6 ?
Lu2 Lu2 Lu5 79.5(3) 6 6 ?
Lu3 Lu2 Lu5 74.3(3) 6 6 ?
Lu8 Lu2 Lu5 54.9(6) . 6 ?
Lu4 Lu2 Lu5 71.3(4) 6 6 ?
Lu9 Lu2 Lu5 76.2(4) 6 6 ?
Lu4 Lu2 Lu6 119.7(11) . 6 ?
Lu9 Lu2 Lu6 103.1(8) . 6 ?
Lu6 Lu2 Lu6 112.3(9) . 6 ?
Lu3 Lu2 Lu6 74.6(3) . 6 ?
Lu2 Lu2 Lu6 16.0(3) 6 6 ?
Lu3 Lu2 Lu6 51.3(3) 6 6 ?
Lu8 Lu2 Lu6 61.4(4) . 6 ?
Lu4 Lu2 Lu6 13.8(3) 6 6 ?
Lu9 Lu2 Lu6 15.6(3) 6 6 ?
Lu5 Lu2 Lu6 64.6(4) 6 6 ?
Lu4 Lu2 Lu7 70.7(11) . 6 ?
Lu9 Lu2 Lu7 73.3(8) . 6 ?
Lu6 Lu2 Lu7 52.5(7) . 6 ?
Lu3 Lu2 Lu7 86.3(2) . 6 ?
Lu2 Lu2 Lu7 76.4(2) 6 6 ?
Lu3 Lu2 Lu7 81.2(2) 6 6 ?
Lu8 Lu2 Lu7 64.7(6) . 6 ?
Lu4 Lu2 Lu7 69.8(4) 6 6 ?
Lu9 Lu2 Lu7 69.8(3) 6 6 ?
Lu5 Lu2 Lu7 12.4(3) 6 6 ?
Lu6 Lu2 Lu7 60.6(3) 6 6 ?
Lu3 Lu3 Lu8 60.8(7) 6 . ?
Lu3 Lu3 Lu4 124.9(4) 6 . ?
Lu8 Lu3 Lu4 113.4(12) . . ?
Lu3 Lu3 Lu2 108.57(18) 6 . ?
Lu8 Lu3 Lu2 118.0(13) . . ?
Lu4 Lu3 Lu2 19.9(5) . . ?
Lu3 Lu3 Lu6 121.1(3) 6 . ?
Lu8 Lu3 Lu6 103.8(12) . . ?
Lu4 Lu3 Lu6 9.6(6) . . ?
Lu2 Lu3 Lu6 24.6(4) . . ?
Lu3 Lu3 Lu2 46.95(13) 6 6 ?
Lu8 Lu3 Lu2 84.8(11) . 6 ?
Lu4 Lu3 Lu2 78.8(5) . 6 ?
Lu2 Lu3 Lu2 61.62(15) . 6 ?
Lu6 Lu3 Lu2 77.2(3) . 6 ?
Lu3 Lu3 Lu4 34.8(3) 6 6 ?
Lu8 Lu3 Lu4 71.4(10) . 6 ?
Lu4 Lu3 Lu4 90.1(7) . 6 ?
Lu2 Lu3 Lu4 74.6(3) . 6 ?
Lu6 Lu3 Lu4 86.8(4) . 6 ?
Lu2 Lu3 Lu4 14.7(3) 6 6 ?
Lu3 Lu3 Lu9 110.1(3) 6 . ?
Lu8 Lu3 Lu9 112.2(13) . . ?
Lu4 Lu3 Lu9 15.5(6) . . ?
Lu2 Lu3 Lu9 7.2(3) . . ?
Lu6 Lu3 Lu9 18.1(5) . . ?
Lu2 Lu3 Lu9 63.5(3) 6 . ?
Lu4 Lu3 Lu9 75.5(4) 6 . ?
Lu3 Lu3 Lu1 79.79(11) 6 . ?
Lu8 Lu3 Lu1 42.5(12) . . ?
Lu4 Lu3 Lu1 71.4(4) . . ?
Lu2 Lu3 Lu1 76.15(14) . . ?
Lu6 Lu3 Lu1 61.9(3) . . ?
Lu2 Lu3 Lu1 69.58(11) 6 . ?
Lu4 Lu3 Lu1 64.1(3) 6 . ?
Lu9 Lu3 Lu1 69.9(3) . . ?
Lu3 Lu3 Lu5 91.4(3) 6 6 ?
Lu8 Lu3 Lu5 53.6(12) . 6 ?
Lu4 Lu3 Lu5 59.8(5) . 6 ?
Lu2 Lu3 Lu5 67.1(3) . 6 ?
Lu6 Lu3 Lu5 50.2(5) . 6 ?
Lu2 Lu3 Lu5 73.9(3) 6 6 ?
Lu4 Lu3 Lu5 71.4(4) 6 6 ?
Lu9 Lu3 Lu5 60.4(4) . 6 ?
Lu1 Lu3 Lu5 12.7(3) . 6 ?
Lu3 Lu3 Lu6 41.9(2) 6 6 ?
Lu8 Lu3 Lu6 68.1(11) . 6 ?
Lu4 Lu3 Lu6 83.5(4) . 6 ?
Lu2 Lu3 Lu6 69.9(3) . 6 ?
Lu6 Lu3 Lu6 79.2(5) . 6 ?
Lu2 Lu3 Lu6 17.1(3) 6 6 ?
Lu4 Lu3 Lu6 9.6(4) 6 6 ?
Lu9 Lu3 Lu6 69.7(4) . 6 ?
Lu1 Lu3 Lu6 55.2(3) . 6 ?
Lu5 Lu3 Lu6 61.9(4) 6 6 ?
Lu3 Lu3 Lu5 69.3(3) 6 . ?
Lu8 Lu3 Lu5 42.3(13) . . ?
Lu4 Lu3 Lu5 75.3(5) . . ?
Lu2 Lu3 Lu5 75.9(3) . . ?
Lu6 Lu3 Lu5 66.2(4) . . ?
Lu2 Lu3 Lu5 58.9(3) 6 . ?
Lu4 Lu3 Lu5 52.5(4) 6 . ?
Lu9 Lu3 Lu5 70.6(4) . . ?
Lu1 Lu3 Lu5 11.7(3) . . ?
Lu5 Lu3 Lu5 22.2(5) 6 . ?
Lu6 Lu3 Lu5 43.9(4) 6 . ?
Lu2 Lu4 Lu6 98(2) . . ?
Lu2 Lu4 Lu9 50.8(12) . . ?
Lu6 Lu4 Lu9 49.4(17) . . ?
Lu2 Lu4 Lu3 91.5(14) . . ?
Lu6 Lu4 Lu3 148.0(19) . . ?
Lu9 Lu4 Lu3 139.6(15) . . ?
Lu2 Lu4 Lu8 98.8(14) . . ?
Lu6 Lu4 Lu8 123.4(19) . . ?
Lu9 Lu4 Lu8 133.4(12) . . ?
Lu3 Lu4 Lu8 24.7(6) . . ?
Lu2 Lu4 Lu3 75.6(12) . 6 ?
Lu6 Lu4 Lu3 137.1(16) . 6 ?
Lu9 Lu4 Lu3 120.1(13) . 6 ?
Lu3 Lu4 Lu3 20.3(3) . 6 ?
Lu8 Lu4 Lu3 25.5(5) . 6 ?
Lu2 Lu4 Lu5 106.6(12) . 6 ?
Lu6 Lu4 Lu5 63.2(16) . 6 ?
Lu9 Lu4 Lu5 92.4(10) . 6 ?
Lu3 Lu4 Lu5 84.8(6) . 6 ?
Lu8 Lu4 Lu5 60.1(7) . 6 ?
Lu3 Lu4 Lu5 77.7(5) 6 6 ?
Lu2 Lu4 Lu2 40.4(10) . 6 ?
Lu6 Lu4 Lu2 108.3(16) . 6 ?
Lu9 Lu4 Lu2 78.2(11) . 6 ?
Lu3 Lu4 Lu2 61.9(5) . 6 ?
Lu8 Lu4 Lu2 60.2(5) . 6 ?
Lu3 Lu4 Lu2 41.9(3) 6 6 ?
Lu5 Lu4 Lu2 76.8(4) 6 6 ?
Lu2 Lu4 Lu1 100.7(12) . . ?
Lu6 Lu4 Lu1 73.8(15) . . ?
Lu9 Lu4 Lu1 96.6(9) . . ?
Lu3 Lu4 Lu1 74.5(4) . . ?
Lu8 Lu4 Lu1 50.0(6) . . ?
Lu3 Lu4 Lu1 66.0(3) 6 . ?
Lu5 Lu4 Lu1 11.8(3) 6 . ?
Lu2 Lu4 Lu1 67.1(3) 6 . ?
Lu2 Lu4 Lu7 97.5(12) . 6 ?
Lu6 Lu4 Lu7 55.3(14) . 6 ?
Lu9 Lu4 Lu7 80.1(9) . 6 ?
Lu3 Lu4 Lu7 93.4(5) . 6 ?
Lu8 Lu4 Lu7 69.1(7) . 6 ?
Lu3 Lu4 Lu7 83.0(4) 6 6 ?
Lu5 Lu4 Lu7 12.3(4) 6 6 ?
Lu2 Lu4 Lu7 73.2(4) 6 6 ?
Lu1 Lu4 Lu7 19.2(2) . 6 ?
Lu2 Lu4 Lu4 51.0(11) . 6 ?
Lu6 Lu4 Lu4 109.6(15) . 6 ?
Lu9 Lu4 Lu4 86.2(10) . 6 ?
Lu3 Lu4 Lu4 55.1(4) . 6 ?
Lu8 Lu4 Lu4 50.3(5) . 6 ?
Lu3 Lu4 Lu4 34.8(3) 6 6 ?
Lu5 Lu4 Lu4 69.2(4) 6 6 ?
Lu2 Lu4 Lu4 10.6(3) 6 6 ?
Lu1 Lu4 Lu4 58.8(3) . 6 ?
Lu7 Lu4 Lu4 67.5(3) 6 6 ?
Lu2 Lu4 Lu9 37.3(10) . 6 ?
Lu6 Lu4 Lu9 94.6(16) . 6 ?
Lu9 Lu4 Lu9 65.9(11) . 6 ?
Lu3 Lu4 Lu9 75.1(5) . 6 ?
Lu8 Lu4 Lu9 69.9(5) . 6 ?
Lu3 Lu4 Lu9 54.8(3) 6 6 ?
Lu5 Lu4 Lu9 71.9(5) 6 6 ?
Lu2 Lu4 Lu9 14.0(2) 6 6 ?
Lu1 Lu4 Lu9 64.3(3) . 6 ?
Lu7 Lu4 Lu9 65.8(4) 6 6 ?
Lu4 Lu4 Lu9 20.3(3) 6 6 ?
Lu1 Lu5 Lu7 93(2) . . ?
Lu1 Lu5 Lu7 55.1(11) . 6 ?
Lu7 Lu5 Lu7 38.9(16) . 6 ?
Lu1 Lu5 Lu5 24.6(12) . 6 ?
Lu7 Lu5 Lu5 72(2) . 6 ?
Lu7 Lu5 Lu5 33.4(7) 6 6 ?
Lu1 Lu5 Lu6 129.7(13) . 6 ?
Lu7 Lu5 Lu6 102(2) . 6 ?
Lu7 Lu5 Lu6 116.9(11) 6 6 ?
Lu5 Lu5 Lu6 120.0(5) 6 6 ?
Lu1 Lu5 Lu8 65.4(11) . . ?
Lu7 Lu5 Lu8 139.5(19) . . ?
Lu7 Lu5 Lu8 106.3(8) 6 . ?
Lu5 Lu5 Lu8 76.1(4) 6 . ?
Lu6 Lu5 Lu8 72.6(7) 6 . ?
Lu1 Lu5 Lu4 115.1(13) . 6 ?
Lu7 Lu5 Lu4 114.3(19) . 6 ?
Lu7 Lu5 Lu4 118.1(11) 6 6 ?
Lu5 Lu5 Lu4 110.8(4) 6 6 ?
Lu6 Lu5 Lu4 16.8(3) 6 6 ?
Lu8 Lu5 Lu4 55.8(6) . 6 ?
Lu1 Lu5 Lu2 108.8(12) . 6 ?
Lu7 Lu5 Lu2 105.1(17) . 6 ?
Lu7 Lu5 Lu2 105.7(10) 6 6 ?
Lu5 Lu5 Lu2 100.5(3) 6 6 ?
Lu6 Lu5 Lu2 20.9(4) 6 6 ?
Lu8 Lu5 Lu2 56.9(6) . 6 ?
Lu4 Lu5 Lu2 12.4(3) 6 6 ?
Lu1 Lu5 Lu9 121.2(12) . 6 ?
Lu7 Lu5 Lu9 91.7(18) . 6 ?
Lu7 Lu5 Lu9 102.2(10) 6 6 ?
Lu5 Lu5 Lu9 107.2(4) 6 6 ?
Lu6 Lu5 Lu9 14.8(4) 6 6 ?
Lu8 Lu5 Lu9 74.2(7) . 6 ?
Lu4 Lu5 Lu9 22.7(4) 6 6 ?
Lu2 Lu5 Lu9 17.3(3) 6 6 ?
Lu1 Lu5 Lu3 83.3(12) . 6 ?
Lu7 Lu5 Lu3 134.5(16) . 6 ?
Lu7 Lu5 Lu3 112.9(8) 6 6 ?
Lu5 Lu5 Lu3 88.6(3) 6 6 ?
Lu6 Lu5 Lu3 52.2(4) 6 6 ?
Lu8 Lu5 Lu3 20.4(5) . 6 ?
Lu4 Lu5 Lu3 35.4(3) 6 6 ?
Lu2 Lu5 Lu3 37.22(19) 6 6 ?
Lu9 Lu5 Lu3 54.4(4) 6 6 ?
Lu1 Lu5 Lu6 56.4(10) . . ?
Lu7 Lu5 Lu6 79.4(16) . . ?
Lu7 Lu5 Lu6 52.6(7) 6 . ?
Lu5 Lu5 Lu6 40.5(4) 6 . ?
Lu6 Lu5 Lu6 79.4(7) 6 . ?
Lu8 Lu5 Lu6 60.1(5) . . ?
Lu4 Lu5 Lu6 71.6(5) 6 . ?
Lu2 Lu5 Lu6 60.4(4) 6 . ?
Lu9 Lu5 Lu6 67.1(5) 6 . ?
Lu3 Lu5 Lu6 60.8(4) 6 . ?
Lu1 Lu5 Lu3 65.8(11) . . ?
Lu7 Lu5 Lu3 123.7(17) . . ?
Lu7 Lu5 Lu3 95.0(7) 6 . ?
Lu5 Lu5 Lu3 69.2(3) 6 . ?
Lu6 Lu5 Lu3 65.9(5) 6 . ?
Lu8 Lu5 Lu3 17.0(5) . . ?
Lu4 Lu5 Lu3 49.8(4) 6 . ?
Lu2 Lu5 Lu3 46.8(2) 6 . ?
Lu9 Lu5 Lu3 63.5(4) 6 . ?
Lu3 Lu5 Lu3 19.3(2) 6 . ?
Lu6 Lu5 Lu3 44.9(3) . . ?
Lu4 Lu6 Lu9 87(2) . . ?
Lu4 Lu6 Lu2 36.5(14) . . ?
Lu9 Lu6 Lu2 52.2(14) . . ?
Lu4 Lu6 Lu5 100.0(17) . 6 ?
Lu9 Lu6 Lu5 119.6(13) . 6 ?
Lu2 Lu6 Lu5 106.6(8) . 6 ?
Lu4 Lu6 Lu3 22.4(14) . . ?
Lu9 Lu6 Lu3 98.8(16) . . ?
Lu2 Lu6 Lu3 47.1(6) . . ?
Lu5 Lu6 Lu3 77.6(5) 6 . ?
Lu4 Lu6 Lu7 110.8(16) . 6 ?
Lu9 Lu6 Lu7 108.4(13) . 6 ?
Lu2 Lu6 Lu7 108.6(8) . 6 ?
Lu5 Lu6 Lu7 15.1(4) 6 6 ?
Lu3 Lu6 Lu7 88.9(5) . 6 ?
Lu4 Lu6 Lu1 91.2(15) . . ?
Lu9 Lu6 Lu1 114.0(12) . . ?
Lu2 Lu6 Lu1 96.2(7) . . ?
Lu5 Lu6 Lu1 10.4(3) 6 . ?
Lu3 Lu6 Lu1 69.0(3) . . ?
Lu7 Lu6 Lu1 20.3(2) 6 . ?
Lu4 Lu6 Lu8 43.9(15) . . ?
Lu9 Lu6 Lu8 108.9(16) . . ?
Lu2 Lu6 Lu8 62.3(8) . . ?
Lu5 Lu6 Lu8 56.1(6) 6 . ?
Lu3 Lu6 Lu8 21.5(5) . . ?
Lu7 Lu6 Lu8 67.9(6) 6 . ?
Lu1 Lu6 Lu8 47.7(5) . . ?
Lu4 Lu6 Lu2 57.9(15) . 6 ?
Lu9 Lu6 Lu2 59.6(12) . 6 ?
Lu2 Lu6 Lu2 35.8(5) . 6 ?
Lu5 Lu6 Lu2 74.2(4) 6 6 ?
Lu3 Lu6 Lu2 51.4(3) . 6 ?
Lu7 Lu6 Lu2 73.4(4) 6 6 ?
Lu1 Lu6 Lu2 64.5(2) . 6 ?
Lu8 Lu6 Lu2 51.5(4) . 6 ?
Lu4 Lu6 Lu7 102.2(15) . . ?
Lu9 Lu6 Lu7 99.5(12) . . ?
Lu2 Lu6 Lu7 96.3(7) . . ?
Lu5 Lu6 Lu7 20.2(4) 6 . ?
Lu3 Lu6 Lu7 81.5(4) . . ?
Lu7 Lu6 Lu7 12.5(4) 6 . ?
Lu1 Lu6 Lu7 18.4(2) . . ?
Lu8 Lu6 Lu7 61.7(5) . . ?
Lu2 Lu6 Lu7 60.9(3) 6 . ?
Lu4 Lu6 Lu3 33.3(13) . 6 ?
Lu9 Lu6 Lu3 89.2(15) . 6 ?
Lu2 Lu6 Lu3 42.1(6) . 6 ?
Lu5 Lu6 Lu3 70.2(5) 6 6 ?
Lu3 Lu6 Lu3 17.0(2) . 6 ?
Lu7 Lu6 Lu3 78.6(4) 6 6 ?
Lu1 Lu6 Lu3 60.3(3) . 6 ?
Lu8 Lu6 Lu3 20.5(4) . 6 ?
Lu2 Lu6 Lu3 35.49(18) 6 6 ?
Lu7 Lu6 Lu3 69.1(3) . 6 ?
Lu4 Lu6 Lu5 90.0(15) . . ?
Lu9 Lu6 Lu5 102.7(12) . . ?
Lu2 Lu6 Lu5 88.6(7) . . ?
Lu5 Lu6 Lu5 19.5(5) 6 . ?
Lu3 Lu6 Lu5 68.9(4) . . ?
Lu7 Lu6 Lu5 21.5(3) 6 . ?
Lu1 Lu6 Lu5 11.3(3) . . ?
Lu8 Lu6 Lu5 49.0(5) . . ?
Lu2 Lu6 Lu5 55.0(3) 6 . ?
Lu7 Lu6 Lu5 12.7(2) . . ?
Lu3 Lu6 Lu5 57.3(3) 6 . ?
Lu5 Lu7 Lu7 108(2) . 6 ?
Lu5 Lu7 Lu1 42.5(17) . . ?
Lu7 Lu7 Lu1 66.3(6) 6 . ?
Lu5 Lu7 Lu5 74(2) . 6 ?
Lu7 Lu7 Lu5 33.4(7) 6 6 ?
Lu1 Lu7 Lu5 33.7(10) . 6 ?
Lu5 Lu7 Lu6 62.6(18) . 6 ?
Lu7 Lu7 Lu6 122.3(4) 6 6 ?
Lu1 Lu7 Lu6 93.4(6) . 6 ?
Lu5 Lu7 Lu6 105.9(9) 6 6 ?
Lu5 Lu7 Lu4 53.4(16) . 6 ?
Lu7 Lu7 Lu4 112.6(4) 6 6 ?
Lu1 Lu7 Lu4 79.9(5) . 6 ?
Lu5 Lu7 Lu4 92.5(8) 6 6 ?
Lu6 Lu7 Lu4 14.0(3) 6 6 ?
Lu5 Lu7 Lu9 74.9(17) . 6 ?
Lu7 Lu7 Lu9 110.9(4) 6 6 ?
Lu1 Lu7 Lu9 98.5(5) . 6 ?
Lu5 Lu7 Lu9 102.1(9) 6 6 ?
Lu6 Lu7 Lu9 15.6(3) 6 6 ?
Lu4 Lu7 Lu9 21.6(3) 6 6 ?
Lu5 Lu7 Lu8 32.1(15) . . ?
Lu7 Lu7 Lu8 82.6(2) 6 . ?
Lu1 Lu7 Lu8 33.4(5) . . ?
Lu5 Lu7 Lu8 51.7(7) 6 . ?
Lu6 Lu7 Lu8 60.5(5) 6 . ?
Lu4 Lu7 Lu8 46.8(4) 6 . ?
Lu9 Lu7 Lu8 65.2(5) 6 . ?
Lu5 Lu7 Lu6 87.9(16) . . ?
Lu7 Lu7 Lu6 45.2(4) 6 . ?
Lu1 Lu7 Lu6 65.6(6) . . ?
Lu5 Lu7 Lu6 42.9(9) 6 . ?
Lu6 Lu7 Lu6 77.1(7) 6 . ?
Lu4 Lu7 Lu6 68.1(4) 6 . ?
Lu9 Lu7 Lu6 66.6(5) 6 . ?
Lu8 Lu7 Lu6 55.8(4) . . ?
Lu5 Lu7 Lu2 62.5(16) . 6 ?
Lu7 Lu7 Lu2 103.6(2) 6 6 ?
Lu1 Lu7 Lu2 82.4(4) . 6 ?
Lu5 Lu7 Lu2 88.3(8) 6 6 ?
Lu6 Lu7 Lu2 18.9(3) 6 6 ?
Lu4 Lu7 Lu2 11.8(3) 6 6 ?
Lu9 Lu7 Lu2 16.1(2) 6 6 ?
Lu8 Lu7 Lu2 49.2(4) . 6 ?
Lu6 Lu7 Lu2 58.5(3) . 6 ?
Lu5 Lu7 Lu9 91.8(15) . . ?
Lu7 Lu7 Lu9 56.3(3) 6 . ?
Lu1 Lu7 Lu9 77.4(5) . . ?
Lu5 Lu7 Lu9 57.2(9) 6 . ?
Lu6 Lu7 Lu9 66.9(5) 6 . ?
Lu4 Lu7 Lu9 60.4(4) 6 . ?
Lu9 Lu7 Lu9 54.5(6) 6 . ?
Lu8 Lu7 Lu9 61.0(5) . . ?
Lu6 Lu7 Lu9 14.4(3) . . ?
Lu2 Lu7 Lu9 49.4(3) 6 . ?
Lu5 Lu7 Lu4 75.5(15) . . ?
Lu7 Lu7 Lu4 54.8(3) 6 . ?
Lu1 Lu7 Lu4 58.5(5) . . ?
Lu5 Lu7 Lu4 43.4(8) 6 . ?
Lu6 Lu7 Lu4 68.3(4) 6 . ?
Lu4 Lu7 Lu4 57.7(5) 6 . ?
Lu9 Lu7 Lu4 60.2(4) 6 . ?
Lu8 Lu7 Lu4 43.6(4) . . ?
Lu6 Lu7 Lu4 12.9(3) . . ?
Lu2 Lu7 Lu4 49.4(3) 6 . ?
Lu9 Lu7 Lu4 19.1(3) . . ?
Lu3 Lu8 Lu3 58.3(14) . 6 ?
Lu3 Lu8 Lu1 118.9(15) . . ?
Lu3 Lu8 Lu1 118.9(15) 6 . ?
Lu3 Lu8 Lu4 83.0(13) . 6 ?
Lu3 Lu8 Lu4 42.0(9) 6 6 ?
Lu1 Lu8 Lu4 77.5(7) . 6 ?
Lu3 Lu8 Lu4 42.0(9) . . ?
Lu3 Lu8 Lu4 83.0(13) 6 . ?
Lu1 Lu8 Lu4 77.5(7) . . ?
Lu4 Lu8 Lu4 79.3(10) 6 . ?
Lu3 Lu8 Lu5 106.0(13) . 6 ?
Lu3 Lu8 Lu5 120.7(17) 6 6 ?
Lu1 Lu8 Lu5 15.2(4) . 6 ?
Lu4 Lu8 Lu5 82.5(8) 6 6 ?
Lu4 Lu8 Lu5 64.1(7) . 6 ?
Lu3 Lu8 Lu5 120.7(17) . . ?
Lu3 Lu8 Lu5 106.0(14) 6 . ?
Lu1 Lu8 Lu5 15.2(4) . . ?
Lu4 Lu8 Lu5 64.1(7) 6 . ?
Lu4 Lu8 Lu5 82.5(8) . . ?
Lu5 Lu8 Lu5 27.9(7) 6 . ?
Lu3 Lu8 Lu2 40.0(9) . . ?
Lu3 Lu8 Lu2 70.2(12) 6 . ?
Lu1 Lu8 Lu2 79.5(7) . . ?
Lu4 Lu8 Lu2 65.8(7) 6 . ?
Lu4 Lu8 Lu2 14.2(4) . . ?
Lu5 Lu8 Lu2 68.3(7) 6 . ?
Lu5 Lu8 Lu2 80.9(8) . . ?
Lu3 Lu8 Lu2 70.2(12) . 6 ?
Lu3 Lu8 Lu2 40.0(9) 6 6 ?
Lu1 Lu8 Lu2 79.5(7) . 6 ?
Lu4 Lu8 Lu2 14.2(4) 6 6 ?
Lu4 Lu8 Lu2 65.8(7) . 6 ?
Lu5 Lu8 Lu2 80.9(8) 6 6 ?
Lu5 Lu8 Lu2 68.3(7) . 6 ?
Lu2 Lu8 Lu2 52.0(5) . 6 ?
Lu3 Lu8 Lu6 91.5(14) . 6 ?
Lu3 Lu8 Lu6 54.7(10) 6 6 ?
Lu1 Lu8 Lu6 64.9(6) . 6 ?
Lu4 Lu8 Lu6 12.8(4) 6 6 ?
Lu4 Lu8 Lu6 79.3(8) . 6 ?
Lu5 Lu8 Lu6 70.9(7) 6 6 ?
Lu5 Lu8 Lu6 51.3(6) . 6 ?
Lu2 Lu8 Lu6 67.1(6) . 6 ?
Lu2 Lu8 Lu6 21.5(4) 6 6 ?
Lu3 Lu8 Lu6 54.7(10) . . ?
Lu3 Lu8 Lu6 91.4(14) 6 . ?
Lu1 Lu8 Lu6 64.9(6) . . ?
Lu4 Lu8 Lu6 79.3(8) 6 . ?
Lu4 Lu8 Lu6 12.8(4) . . ?
Lu5 Lu8 Lu6 51.3(6) 6 . ?
Lu5 Lu8 Lu6 70.9(7) . . ?
Lu2 Lu8 Lu6 21.5(4) . . ?
Lu2 Lu8 Lu6 67.2(6) 6 . ?
Lu6 Lu8 Lu6 76.4(8) 6 . ?
Lu3 Lu8 Lu7 113.0(15) . . ?
Lu3 Lu8 Lu7 105.4(14) 6 . ?
Lu1 Lu8 Lu7 13.5(3) . . ?
Lu4 Lu8 Lu7 64.1(6) 6 . ?
Lu4 Lu8 Lu7 74.2(7) . . ?
Lu5 Lu8 Lu7 22.0(4) 6 . ?
Lu5 Lu8 Lu7 8.4(4) . . ?
Lu2 Lu8 Lu7 73.0(6) . . ?
Lu2 Lu8 Lu7 66.1(5) 6 . ?
Lu6 Lu8 Lu7 51.6(5) 6 . ?
Lu6 Lu8 Lu7 62.5(6) . . ?
Lu6 Lu9 Lu2 77.1(12) . . ?
Lu6 Lu9 Lu4 43.4(11) . . ?
Lu2 Lu9 Lu4 35.0(8) . . ?
Lu6 Lu9 Lu3 63.2(13) . . ?
Lu2 Lu9 Lu3 15.8(6) . . ?
Lu4 Lu9 Lu3 24.9(10) . . ?
Lu6 Lu9 Lu2 104.8(13) . 6 ?
Lu2 Lu9 Lu2 50.5(7) . 6 ?
Lu4 Lu9 Lu2 78.1(10) . 6 ?
Lu3 Lu9 Lu2 53.6(3) . 6 ?
Lu6 Lu9 Lu5 45.6(11) . 6 ?
Lu2 Lu9 Lu5 80.0(7) . 6 ?
Lu4 Lu9 Lu5 64.9(9) . 6 ?
Lu3 Lu9 Lu5 65.2(4) . 6 ?
Lu2 Lu9 Lu5 72.4(4) 6 6 ?
Lu6 Lu9 Lu9 113.0(12) . 6 ?
Lu2 Lu9 Lu9 67.6(8) . 6 ?
Lu4 Lu9 Lu9 93.8(10) . 6 ?
Lu3 Lu9 Lu9 69.9(3) . 6 ?
Lu2 Lu9 Lu9 17.1(2) 6 6 ?
Lu5 Lu9 Lu9 72.8(4) 6 6 ?
Lu6 Lu9 Lu7 56.0(12) . 6 ?
Lu2 Lu9 Lu7 90.6(7) . 6 ?
Lu4 Lu9 Lu7 78.3(9) . 6 ?
Lu3 Lu9 Lu7 76.7(3) . 6 ?
Lu2 Lu9 Lu7 72.9(3) 6 6 ?
Lu5 Lu9 Lu7 13.5(3) 6 6 ?
Lu9 Lu9 Lu7 69.1(4) 6 6 ?
Lu6 Lu9 Lu4 97.1(12) . 6 ?
Lu2 Lu9 Lu4 49.4(7) . 6 ?
Lu4 Lu9 Lu4 73.4(11) . 6 ?
Lu3 Lu9 Lu4 49.7(3) . 6 ?
Lu2 Lu9 Lu4 8.2(2) 6 6 ?
Lu5 Lu9 Lu4 64.4(4) 6 6 ?
Lu9 Lu9 Lu4 20.3(3) 6 6 ?
Lu7 Lu9 Lu4 65.6(4) 6 6 ?
Lu6 Lu9 Lu3 75.6(13) . 6 ?
Lu2 Lu9 Lu3 21.4(5) . 6 ?
Lu4 Lu9 Lu3 42.5(10) . 6 ?
Lu3 Lu9 Lu3 18.1(2) . 6 ?
Lu2 Lu9 Lu3 35.63(16) 6 6 ?
Lu5 Lu9 Lu3 63.3(4) 6 6 ?
Lu9 Lu9 Lu3 51.8(2) 6 6 ?
Lu7 Lu9 Lu3 71.9(3) 6 6 ?
Lu4 Lu9 Lu3 31.7(3) 6 6 ?
Lu6 Lu9 Lu8 56.9(13) . . ?
Lu2 Lu9 Lu8 32.2(7) . . ?
Lu4 Lu9 Lu8 32.3(8) . . ?
Lu3 Lu9 Lu8 18.0(4) . . ?
Lu2 Lu9 Lu8 50.0(3) 6 . ?
Lu5 Lu9 Lu8 47.8(5) 6 . ?
Lu9 Lu9 Lu8 63.5(3) 6 . ?
Lu7 Lu9 Lu8 58.8(5) 6 . ?
Lu4 Lu9 Lu8 43.6(3) 6 . ?
Lu3 Lu9 Lu8 19.4(3) 6 . ?
Lu6 Lu9 Lu1 52.4(11) . . ?
Lu2 Lu9 Lu1 73.3(6) . . ?
Lu4 Lu9 Lu1 63.7(8) . . ?
Lu3 Lu9 Lu1 59.5(2) . . ?
Lu2 Lu9 Lu1 62.42(19) 6 . ?
Lu5 Lu9 Lu1 10.0(3) 6 . ?
Lu9 Lu9 Lu1 63.6(3) 6 . ?
Lu7 Lu9 Lu1 17.32(19) 6 . ?
Lu4 Lu9 Lu1 54.4(3) 6 . ?
Lu3 Lu9 Lu1 55.10(17) 6 . ?
Lu8 Lu9 Lu1 41.5(4) . . ?
C9 C1 C2 125.3 . . ?
C9 C1 C5 115.0 . . ?
C2 C1 C5 107.0 . . ?
C1 C2 C12 120.5 . . ?
C1 C2 C3 116.8 . . ?
C12 C2 C3 117.4 . . ?
C15 C3 C4 126.9 . . ?
C15 C3 C2 119.0 . . ?
C4 C3 C2 101.6 . . ?
C3 C4 C18 114.9 . . ?
C3 C4 C5 109.1 . . ?
C18 C4 C5 119.2 . . ?
C6 C5 C1 126.1 . . ?
C6 C5 C4 118.8 . . ?
C1 C5 C4 105.2 . . ?
C5 C6 C7 117.4 . . ?
C5 C6 C20 125.2 . . ?
C7 C6 C20 113.1 . . ?
C6 C7 C23 119.9 . . ?
C6 C7 C8 119.0 . . ?
C23 C7 C8 109.0 . . ?
C25 C8 C7 105.7 . . ?
C25 C8 C9 120.6 . . ?
C7 C8 C9 113.4 . . ?
C1 C9 C10 118.9 . . ?
C1 C9 C8 124.2 . . ?
C10 C9 C8 116.0 . . ?
C9 C10 C27 120.2 . . ?
C9 C10 C11 112.8 . . ?
C27 C10 C11 122.5 . . ?
C12 C11 C10 124.9 . . ?
C12 C11 C29 121.1 . . ?
C10 C11 C29 101.2 . . ?
C11 C12 C13 126.1 . . ?
C11 C12 C2 114.6 . . ?
C13 C12 C2 115.3 . . ?
C31 C13 C12 117.1 . . ?
C31 C13 C14 111.6 . . ?
C12 C13 C14 122.6 . . ?
C15 C14 C33 128.6 . . ?
C15 C14 C13 118.6 . . ?
C33 C14 C13 101.9 . . ?
C14 C15 C16 115.9 . . ?
C14 C15 C3 124.2 . . ?
C16 C15 C3 118.9 . . ?
C15 C16 C35 115.6 . . ?
C15 C16 C17 115.8 . . ?
C35 C16 C17 116.6 . . ?
C18 C17 C16 127.3 . . ?
C18 C17 C38 100.0 . . ?
C16 C17 C38 119.6 . . ?
C17 C18 C19 121.3 . . ?
C17 C18 C4 114.2 . . ?
C19 C18 C4 117.1 . . ?
C20 C19 C18 125.5 . . ?
C20 C19 C39 119.1 . . ?
C18 C19 C39 100.4 . . ?
C19 C20 C21 118.4 . . ?
C19 C20 C6 113.6 . . ?
C21 C20 C6 119.3 . . ?
C22 C21 C41 105.5 . . ?
C22 C21 C20 125.2 . . ?
C41 C21 C20 117.7 . . ?
C21 C22 C43 114.1 . . ?
C21 C22 C23 116.1 . . ?
C43 C22 C23 118.7 . . ?
C22 C23 C7 125.6 . . ?
C22 C23 C24 117.5 . . ?
C7 C23 C24 107.4 . . ?
C23 C24 C25 108.9 . . ?
C23 C24 C45 120.4 . . ?
C25 C24 C45 110.1 . . ?
C24 C25 C8 108.2 . . ?
C24 C25 C26 128.8 . . ?
C8 C25 C26 117.2 . . ?
C47 C26 C27 113.3 . . ?
C47 C26 C25 115.8 . . ?
C27 C26 C25 119.1 . . ?
C28 C27 C10 91.2 . . ?
C28 C27 C26 135.1 . . ?
C10 C27 C26 123.9 . . ?
C49 C28 C27 114.7 . . ?
C49 C28 C29 108.8 . . ?
C27 C28 C29 127.1 . . ?
C30 C29 C28 135.1 . . ?
C30 C29 C11 114.2 . . ?
C28 C29 C11 97.9 . . ?
C29 C30 C51 106.5 . . ?
C29 C30 C31 125.1 . . ?
C51 C30 C31 117.5 . . ?
C13 C31 C32 104.7 . . ?
C13 C31 C30 116.1 . . ?
C32 C31 C30 127.4 . . ?
C33 C32 C31 104.4 . . ?
C33 C32 C53 127.5 . . ?
C31 C32 C53 114.6 . . ?
C34 C33 C14 118.9 . . ?
C34 C33 C32 114.9 . . ?
C14 C33 C32 117.4 . . ?
C33 C34 C35 117.2 . . ?
C33 C34 C55 128.3 . . ?
C35 C34 C55 104.5 . . ?
C34 C35 C16 121.8 . . ?
C34 C35 C36 103.4 . . ?
C16 C35 C36 122.6 . . ?
C56 C36 C35 116.5 . . ?
C56 C36 C37 110.8 . . ?
C35 C36 C37 122.8 . . ?
C59 C37 C36 123.6 . . ?
C59 C37 C38 117.9 . . ?
C36 C37 C38 114.3 . . ?
C39 C38 C17 111.0 . . ?
C39 C38 C37 114.0 . . ?
C17 C38 C37 122.1 . . ?
C40 C39 C38 129.1 . . ?
C40 C39 C19 118.8 . . ?
C38 C39 C19 106.8 . . ?
C41 C40 C39 119.4 . . ?
C41 C40 C60 117.7 . . ?
C39 C40 C60 115.5 . . ?
C40 C41 C21 124.9 . . ?
C40 C41 C42 119.2 . . ?
C21 C41 C42 110.1 . . ?
C43 C42 C63 114.9 . . ?
C43 C42 C41 98.9 . . ?
C63 C42 C41 133.9 . . ?
C42 C43 C22 111.4 . . ?
C42 C43 C44 114.8 . . ?
C22 C43 C44 123.0 . . ?
C45 C44 C64 110.9 . . ?
C45 C44 C43 117.0 . . ?
C64 C44 C43 113.8 . . ?
C44 C45 C46 115.0 . . ?
C44 C45 C24 121.3 . . ?
C46 C45 C24 119.6 . . ?
C45 C46 C65 114.9 . . ?
C45 C46 C47 127.1 . . ?
C65 C46 C47 109.0 . . ?
C26 C47 C46 117.7 . . ?
C26 C47 C48 108.8 . . ?
C46 C47 C48 118.4 . . ?
C67 C48 C49 106.2 . . ?
C67 C48 C47 109.8 . . ?
C49 C48 C47 135.0 . . ?
C28 C49 C50 131.6 . . ?
C28 C49 C48 112.5 . . ?
C50 C49 C48 108.8 . . ?
C49 C50 C68 107.6 . . ?
C49 C50 C51 107.7 . . ?
C68 C50 C51 136.9 . . ?
C30 C51 C50 128.1 . . ?
C30 C51 C52 115.5 . . ?
C50 C51 C52 104.5 . . ?
C53 C52 C70 118.3 . . ?
C53 C52 C51 118.4 . . ?
C70 C52 C51 109.6 . . ?
C52 C53 C32 126.5 . . ?
C52 C53 C54 105.3 . . ?
C32 C53 C54 117.2 . . ?
C71 C54 C53 110.2 . . ?
C71 C54 C55 124.4 . . ?
C53 C54 C55 112.3 . . ?
C56 C55 C34 119.6 . . ?
C56 C55 C54 114.0 . . ?
C34 C55 C54 118.6 . . ?
C55 C56 C36 95.9 . . ?
C55 C56 C57 113.5 . . ?
C36 C56 C57 135.6 . . ?
C56 C57 C72 130.1 . . ?
C56 C57 C58 110.8 . . ?
C72 C57 C58 106.5 . . ?
C59 C58 C75 106.7 . . ?
C59 C58 C57 110.7 . . ?
C75 C58 C57 130.2 . . ?
C37 C59 C60 124.6 . . ?
C37 C59 C58 126.2 . . ?
C60 C59 C58 98.9 . . ?
C61 C60 C40 114.4 . . ?
C61 C60 C59 116.6 . . ?
C40 C60 C59 118.2 . . ?
C75 C61 C60 113.9 . . ?
C75 C61 C63 99.0 . . ?
C60 C61 C63 136.4 . . ?
C64 C62 C63 133.6 . . ?
C64 C62 C76 120.3 . . ?
C63 C62 C76 103.2 . . ?
C62 C63 C42 120.6 . . ?
C62 C63 C61 137.0 . . ?
C42 C63 C61 93.3 . . ?
C62 C64 C44 121.9 . . ?
C62 C64 C65 124.9 . . ?
C44 C64 C65 104.6 . . ?
C66 C65 C46 142.8 . . ?
C66 C65 C64 106.0 . . ?
C46 C65 C64 93.6 . . ?
C66 C65 C67 45.1 . . ?
C46 C65 C67 102.1 . . ?
C64 C65 C67 143.5 . . ?
C65 C66 C77 135.7 . . ?
C65 C66 C67 102.2 . . ?
C77 C66 C67 120.1 . . ?
C68 C67 C48 110.3 . . ?
C68 C67 C66 106.1 . . ?
C48 C67 C66 130.8 . . ?
C68 C67 C65 136.4 . . ?
C48 C67 C65 100.1 . . ?
C66 C67 C65 32.7 . . ?
C67 C68 C69 138.6 . . ?
C67 C68 C50 106.7 . . ?
C69 C68 C50 110.1 . . ?
C78 C69 C70 126.9 . . ?
C78 C69 C68 108.5 . . ?
C70 C69 C68 121.3 . . ?
C69 C70 C52 136.0 . . ?
C69 C70 C71 111.4 . . ?
C52 C70 C71 99.5 . . ?
C72 C71 C54 137.3 . . ?
C72 C71 C70 109.6 . . ?
C54 C71 C70 106.4 . . ?
C71 C72 C73 143.0 . . ?
C71 C72 C57 98.7 . . ?
C73 C72 C57 112.1 . . ?
C72 C73 C74 138.3 . . ?
C72 C73 C78 105.6 . . ?
C74 C73 C78 103.3 . . ?
C73 C74 C76 119.0 . . ?
C73 C74 C75 131.2 . . ?
C76 C74 C75 96.4 . . ?
C61 C75 C74 145.2 . . ?
C61 C75 C58 103.6 . . ?
C74 C75 C58 99.7 . . ?
C74 C76 C77 103.3 . . ?
C74 C76 C62 134.9 . . ?
C77 C76 C62 106.5 . . ?
C66 C77 C76 124.0 . . ?
C66 C77 C78 126.0 . . ?
C76 C77 C78 104.7 . . ?
C69 C78 C73 122.5 . . ?
C69 C78 C77 120.1 . . ?
C73 C78 C77 109.5 . . ?
N2A Ni1A N1A 177.7(3) . . ?
N2A Ni1A N3A 89.8(2) . 6 ?
N1A Ni1A N3A 90.1(2) . 6 ?
N2A Ni1A N3A 89.8(2) . . ?
N1A Ni1A N3A 90.1(2) . . ?
N3A Ni1A N3A 177.9(3) 6 . ?
C13A N3A C6A 104.4(4) . . ?
C13A N3A Ni1A 128.0(3) . . ?
C6A N3A Ni1A 127.5(3) . . ?
C16A N2A C16A 103.4(6) . 6 ?
C16A N2A Ni1A 128.2(3) . . ?
C16A N2A Ni1A 128.2(3) 6 . ?
C3A C3A C4A 106.6(3) 6 . ?
C3A C3A C2A 129.2(3) 6 . ?
C4A C3A C2A 124.1(5) . . ?
C5A C4A N1A 124.5(5) . . ?
C5A C4A C3A 123.8(5) . . ?
N1A C4A C3A 111.7(5) . . ?
C6A C5A C4A 124.3(5) . . ?
C5A C6A N3A 125.2(5) . . ?
C5A C6A C7A 123.7(5) . . ?
N3A C6A C7A 111.1(4) . . ?
C12A C7A C6A 106.4(4) . . ?
C12A C7A C8A 129.2(5) . . ?
C6A C7A C8A 124.3(5) . . ?
C7A C8A C9A 113.3(6) . . ?
C12A C11A C10A 112.3(6) . . ?
C7A C12A C13A 106.7(4) . . ?
C7A C12A C11A 129.0(5) . . ?
C13A C12A C11A 124.3(5) . . ?
N3A C13A C15A 125.0(5) . . ?
N3A C13A C12A 111.3(4) . . ?
C15A C13A C12A 123.7(5) . . ?
C16A C15A C13A 124.2(5) . . ?
C15A C16A N2A 124.6(4) . . ?
C15A C16A C17A 123.4(4) . . ?
N2A C16A C17A 111.9(4) . . ?
C17A C17A C16A 106.4(3) 6 . ?
C17A C17A C18A 128.6(3) 6 . ?
C16A C17A C18A 124.8(5) . . ?
C17A C18A C19A 112.0(5) . . ?
C3A C2A C1A 112.9(4) . . ?
C4A N1A C4A 103.4(6) . 6 ?
C4A N1A Ni1A 128.3(3) . . ?
C4A N1A Ni1A 128.3(3) 6 . ?
C2B C1B C6B 118.8(10) . . ?
C3B C2B C1B 121.7(10) . . ?
C2B C3B C4B 119.3(9) . . ?
C5B C4B C3B 120.3(9) . . ?
C6B C5B C4B 119.0(11) . . ?
C5B C6B C1B 120.8(10) . . ?
C3C C1C C2C 112.9(14) 2_656 . ?
C3C C2C C1C 124.5(17) . . ?
C1C C3C C2C 121.7(14) 2_656 . ?

_refine_diff_density_max         2.177
_refine_diff_density_min         -1.687
_refine_diff_density_rms         0.194


_vrf_PLAT307_Lu2@D3h-C78         
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2@D3h-C78         
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT939_Lu2@D3h-C78         
;
PROBLEM: PLAT939 Type_3 Large Value of Not (SHELXL) Weight Optimized S 
RESPONSE: Because of limited beamtime available, data was collected from only 
one crystal.The large value of not weight optimized S may caused by the severe 
disoder of the internal metal atoms
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2@C2v-C84
_database_code_depnum_ccdc_archive 'CCDC 1582217'
_audit_update_record             
;
2017-10-26 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2@C2v-C84 Ni(OEP)'
_chemical_name_common            'Lu2@C2v-C84 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C84, C36 H44 N4 Ni, C6 H6 '
_chemical_formula_sum            'C126 H50 Lu2 N4 Ni'
_chemical_formula_weight         2028.35

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0027 0.0014 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0053 0.0028 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3436 0.9622 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.2922 5.1425 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   25.410(5)
_cell_length_b                   15.110(5)
_cell_length_c                   19.917(5)
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 94.510(5)
_cell_angle_gamma                90.000(5)
_cell_volume                     7623(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9835
_cell_measurement_theta_min      2.325
_cell_measurement_theta_max      23.133

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.767
_exptl_crystal_F_000             4016
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.120
_exptl_crystal_size_mid          0.080
_exptl_crystal_size_min          0.070
_exptl_absorpt_coefficient_mu    2.339
_shelx_estimated_absorpt_T_min   0.799
_shelx_estimated_absorpt_T_max   0.849
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.5218
_exptl_absorpt_correction_T_max  0.7449
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline BL17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            51276
_diffrn_reflns_av_unetI/netI     0.0303
_diffrn_reflns_av_R_equivalents  0.0504
_diffrn_reflns_limit_h_min       -29
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         1.687
_diffrn_reflns_theta_max         23.133
_diffrn_reflns_theta_full        23.048
_diffrn_measured_fraction_theta_max 0.974
_diffrn_measured_fraction_theta_full 0.974
_diffrn_reflns_Laue_measured_fraction_max 0.974
_diffrn_reflns_Laue_measured_fraction_full 0.974
_diffrn_reflns_point_group_measured_fraction_max 0.974
_diffrn_reflns_point_group_measured_fraction_full 0.974
_reflns_number_total             7072
_reflns_number_gt                6280
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1486P)²+43.3856P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7072
_refine_ls_number_parameters     866
_refine_ls_number_restraints     864
_refine_ls_R_factor_all          0.0890
_refine_ls_R_factor_gt           0.0818
_refine_ls_wR_factor_ref         0.2438
_refine_ls_wR_factor_gt          0.2353
_refine_ls_goodness_of_fit_ref   1.068
_refine_ls_restrained_S_all      1.131
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.26604(14) 0.0431(2) 0.1465(2) 0.0640(9) Uani 0.1517 1 d . . P A 1
Lu2 Lu 0.18947(7) 0.04085(13) 0.27450(8) 0.0597(5) Uani 0.1508 1 d . . P A 1
Lu3 Lu 0.15949(12) 0.0884(2) 0.22996(15) 0.0515(6) Uani 0.1353 1 d . . P A 1
Lu4 Lu 0.14742(12) 0.1165(2) 0.1962(3) 0.0708(10) Uani 0.1117 1 d . . P A 1
Lu5 Lu 0.17179(18) 0.1103(2) 0.1448(2) 0.0453(9) Uani 0.0787 1 d . . P A 1
Lu6 Lu 0.1996(3) 0.1114(4) 0.1333(3) 0.0787(15) Uani 0.0775 1 d . U P A 1
Lu7 Lu 0.1906(2) 0.0000 0.0852(2) 0.0539(13) Uani 0.0664 2 d S TU P A 1
Lu8 Lu 0.1311(2) 0.0557(5) 0.1928(3) 0.0770(15) Uani 0.0631 1 d . U P A 1
Lu9 Lu 0.2526(3) 0.0446(7) 0.1259(3) 0.046(2) Uani 0.0564 1 d . U P A 1
Lu10 Lu 0.2376(9) 0.0000 0.1051(10) 0.081(3) Uani 0.0363 2 d S TU P A 1
Lu11 Lu 0.2004(9) 0.1337(9) 0.1869(9) 0.123(4) Uani 0.0325 1 d . U P A 1
Lu12 Lu 0.1712(10) 0.1162(13) 0.2438(12) 0.110(6) Uani 0.0312 1 d . U P A 1
Lu13 Lu 0.2102(8) -0.0588(13) 0.1038(7) 0.090(3) Uani 0.0292 1 d . U P A 1
Lu14 Lu 0.2530(10) 0.0848(17) 0.1678(10) 0.098(4) Uani 0.0228 1 d . U P A 1
Lu15 Lu 0.2751(14) 0.0000 0.2078(16) 0.090(6) Uani 0.0156 2 d S TU P A 1
C1 C 0.10201(13) 0.0151(3) 0.33016(16) 0.121(5) Uani 0.5 1 d G U P A -1
C2 C 0.13883(15) -0.0477(3) 0.36138(13) 0.098(5) Uani 0.5 1 d G U P A -1
C3 C 0.14350(16) -0.1480(2) 0.33619(16) 0.102(5) Uani 0.5 1 d G U P A -1
C4 C 0.10837(15) -0.1770(2) 0.28724(19) 0.123(6) Uani 0.5 1 d G U P A -1
C5 C 0.07549(12) -0.1072(3) 0.2693(2) 0.139(6) Uani 0.5 1 d G U P A -1
C6 C 0.05041(10) -0.1049(3) 0.2093(2) 0.135(6) Uani 0.5 1 d G U P A -1
C7 C 0.03672(7) -0.0229(3) 0.1877(2) 0.118(6) Uani 0.5 1 d G U P A -1
C8 C 0.05276(8) 0.0358(3) 0.2364(2) 0.144(6) Uani 0.5 1 d G U P A -1
C9 C 0.07006(11) -0.0236(3) 0.2861(2) 0.161(6) Uani 0.5 1 d G U P A -1
C10 C 0.11926(13) 0.0968(3) 0.33832(15) 0.111(5) Uani 0.5 1 d G U P A -1
C11 C 0.16620(15) 0.0889(3) 0.37469(11) 0.064(3) Uani 0.5 1 d G U P A -1
C12 C 0.17841(16) 0.0040(3) 0.38806(10) 0.087(3) Uani 0.5 1 d G U P A -1
C13 C 0.23030(17) -0.0299(3) 0.39458(10) 0.089(4) Uani 0.5 1 d G U P A -1
C14 C 0.24097(17) -0.1144(3) 0.37847(12) 0.086(4) Uani 0.5 1 d G U P A -1
C15 C 0.19454(17) -0.1594(2) 0.35151(14) 0.111(5) Uani 0.5 1 d G U P A -1
C16 C 0.21096(17) -0.2255(2) 0.30598(17) 0.112(6) Uani 0.5 1 d G U P A -1
C17 C 0.17280(17) -0.26681(19) 0.23616(19) 0.097(5) Uani 0.5 1 d G U P A -1
C18 C 0.11383(15) -0.2304(2) 0.2357(2) 0.107(5) Uani 0.5 1 d G U P A -1
C19 C 0.09574(14) -0.2197(2) 0.1745(2) 0.116(5) Uani 0.5 1 d G U P A -1
C20 C 0.05740(11) -0.1671(3) 0.1686(2) 0.117(6) Uani 0.5 1 d G U P A -1
C21 C 0.05785(12) -0.1353(3) 0.0990(2) 0.113(5) Uani 0.5 1 d G U P A -1
C22 C 0.04645(11) -0.0421(3) 0.0787(2) 0.115(5) Uani 0.5 1 d G U P A -1
C23 C 0.03523(9) 0.0224(3) 0.1275(2) 0.105(5) Uani 0.5 1 d G U P A -1
C24 C 0.04755(11) 0.0934(3) 0.1174(2) 0.096(5) Uani 0.5 1 d G U P A -1
C25 C 0.06667(11) 0.1589(3) 0.1743(2) 0.103(5) Uani 0.5 1 d G U P A -1
C26 C 0.06423(10) 0.1222(3) 0.2356(2) 0.114(5) Uani 0.5 1 d G U P A -1
C27 C 0.10150(12) 0.1480(2) 0.28621(18) 0.122(6) Uani 0.5 1 d G U P A -1
C28 C 0.13075(14) 0.2100(2) 0.28689(17) 0.083(4) Uani 0.5 1 d G U P A -1
C29 C 0.18158(15) 0.2190(2) 0.31309(15) 0.073(3) Uani 0.5 1 d G U P A -1
C30 C 0.20680(15) 0.1620(2) 0.36342(12) 0.077(4) Uani 0.5 1 d G U P A -1
C31 C 0.25331(15) 0.1321(3) 0.36824(13) 0.066(3) Uani 0.5 1 d G U P A -1
C32 C 0.26997(15) 0.0388(3) 0.39014(12) 0.088(4) Uani 0.5 1 d G U P A -1
C33 C 0.32070(13) 0.0239(3) 0.35642(17) 0.105(5) Uani 0.5 1 d G U P A -1
C34 C 0.32610(13) -0.0769(3) 0.33871(18) 0.107(5) Uani 0.5 1 d G U P A -1
C35 C 0.28676(16) -0.1408(3) 0.34742(16) 0.101(5) Uani 0.5 1 d G U P A -1
C36 C 0.26575(16) -0.2086(2) 0.30109(17) 0.138(6) Uani 0.5 1 d G U P A -1
C37 C 0.29410(15) -0.2185(2) 0.2532(2) 0.138(6) Uani 0.5 1 d G U P A -1
C38 C 0.25861(15) -0.2521(2) 0.19411(19) 0.082(4) Uani 0.5 1 d G U P A -1
C39 C 0.20327(16) -0.27091(19) 0.17505(19) 0.069(4) Uani 0.5 1 d G U P A -1
C40 C 0.17812(15) -0.2453(2) 0.10630(18) 0.073(4) Uani 0.5 1 d G U P A -1
C41 C 0.12313(15) -0.2242(2) 0.10413(19) 0.085(4) Uani 0.5 1 d G U P A -1
C42 C 0.09519(14) -0.1735(3) 0.06600(19) 0.099(5) Uani 0.5 1 d G U P A -1
C43 C 0.11196(16) -0.1292(3) 0.01856(16) 0.105(5) Uani 0.5 1 d G U P A -1
C44 C 0.10705(17) -0.0351(3) 0.00125(14) 0.113(6) Uani 0.5 1 d G U P A -1
C45 C 0.07224(15) 0.0119(3) 0.02896(17) 0.116(5) Uani 0.5 1 d G U P A -1
C46 C 0.07238(15) 0.0887(3) 0.05128(18) 0.103(5) Uani 0.5 1 d G U P A -1
C47 C 0.11680(18) 0.1479(3) 0.03973(15) 0.109(5) Uani 0.5 1 d G U P A -1
C48 C 0.13028(18) 0.2290(2) 0.09037(17) 0.114(6) Uani 0.5 1 d G U P A -1
C49 C 0.10605(15) 0.2310(2) 0.15451(19) 0.116(5) Uani 0.5 1 d G U P A -1
C50 C 0.13351(15) 0.2536(2) 0.21320(19) 0.098(5) Uani 0.5 1 d G U P A -1
C51 C 0.18914(16) 0.27408(19) 0.20654(18) 0.093(5) Uani 0.5 1 d G U P A -1
C52 C 0.21562(15) 0.2505(2) 0.27580(16) 0.063(3) Uani 0.5 1 d G U P A -1
C53 C 0.26397(14) 0.2340(2) 0.27054(17) 0.046(2) Uani 0.5 1 d G U P A -1
C54 C 0.29310(13) 0.1713(3) 0.31910(17) 0.090(4) Uani 0.5 1 d G U P A -1
C55 C 0.33339(11) 0.1019(3) 0.31083(19) 0.112(5) Uani 0.5 1 d G U P A -1
C56 C 0.34779(9) 0.1070(3) 0.2498(2) 0.110(5) Uani 0.5 1 d G U P A -1
C57 C 0.36489(8) 0.0151(3) 0.2434(2) 0.097(4) Uani 0.5 1 d G U P A -1
C58 C 0.35349(10) -0.0742(3) 0.2765(2) 0.087(4) Uani 0.5 1 d G U P A -1
C59 C 0.33721(12) -0.1569(3) 0.2391(2) 0.092(5) Uani 0.5 1 d G U P A -1
C60 C 0.33264(11) -0.1531(3) 0.1623(2) 0.112(5) Uani 0.5 1 d G U P A -1
C61 C 0.29035(14) -0.2168(3) 0.1375(2) 0.111(5) Uani 0.5 1 d G U P A -1
C62 C 0.26693(15) -0.1800(3) 0.07267(17) 0.122(5) Uani 0.5 1 d G U P A -1
C63 C 0.20729(16) -0.2075(2) 0.05946(16) 0.108(5) Uani 0.5 1 d G U P A -1
C64 C 0.18054(17) -0.1531(3) 0.01627(13) 0.094(4) Uani 0.5 1 d G U P A -1
C65 C 0.18895(18) -0.0670(3) -0.01598(10) 0.122(5) Uani 0.5 1 d G U P A -1
C66 C 0.15258(19) 0.0169(3) -0.01645(10) 0.117(5) Uani 0.5 1 d G U P A -1
C67 C 0.15820(19) 0.1178(3) 0.00354(11) 0.098(5) Uani 0.5 1 d G U P A -1
C68 C 0.21796(19) 0.1137(3) 0.00804(11) 0.123(5) Uani 0.5 1 d G U P A -1
C69 C 0.23117(19) 0.1847(3) 0.05104(14) 0.147(6) Uani 0.5 1 d G U P A -1
C70 C 0.19207(19) 0.2385(2) 0.08118(16) 0.118(6) Uani 0.5 1 d G U P A -1
C71 C 0.21621(17) 0.2654(2) 0.14736(17) 0.108(6) Uani 0.5 1 d G U P A -1
C72 C 0.26971(16) 0.2351(2) 0.15267(18) 0.108(5) Uani 0.5 1 d G U P A -1
C73 C 0.29680(13) 0.2150(2) 0.21186(19) 0.104(5) Uani 0.5 1 d G U P A -1
C74 C 0.33592(11) 0.1546(3) 0.1989(2) 0.102(5) Uani 0.5 1 d G U P A -1
C75 C 0.34711(11) 0.0965(3) 0.1466(2) 0.132(6) Uani 0.5 1 d G U P A -1
C76 C 0.36284(9) 0.0067(3) 0.1664(2) 0.108(4) Uani 0.5 1 d G U P A -1
C77 C 0.34868(10) -0.0719(3) 0.1267(2) 0.121(5) Uani 0.5 1 d G U P A -1
C78 C 0.31740(14) -0.0597(3) 0.06648(19) 0.154(6) Uani 0.5 1 d G U P A -1
C79 C 0.27099(16) -0.1080(3) 0.03036(15) 0.140(6) Uani 0.5 1 d G U P A -1
C80 C 0.23733(18) -0.0371(3) -0.00412(11) 0.141(6) Uani 0.5 1 d G U P A -1
C81 C 0.26188(18) 0.0509(3) 0.00969(13) 0.148(6) Uani 0.5 1 d G U P A -1
C82 C 0.31401(16) 0.0324(3) 0.04569(18) 0.154(6) Uani 0.5 1 d G U P A -1
C83 C 0.31549(15) 0.1135(3) 0.08538(19) 0.157(6) Uani 0.5 1 d G U P A -1
C84 C 0.28094(17) 0.1896(3) 0.09234(18) 0.128(6) Uani 0.5 1 d G U P A -1
Ni1A Ni 0.01908(2) 0.0000 0.41868(3) 0.0184(2) Uani 1 2 d S T P B 2
C1A C -0.08989(19) 0.1465(3) 0.1572(2) 0.0392(10) Uani 1 1 d . . . B 2
H1AA H -0.0749 0.0996 0.1323 0.059 Uiso 1 1 calc R U . B 2
H1AB H -0.0621 0.1801 0.1805 0.059 Uiso 1 1 calc R U . B 2
H1AC H -0.1105 0.1844 0.1268 0.059 Uiso 1 1 calc R U . B 2
N2A N 0.02031(12) 0.1299(2) 0.41714(15) 0.0213(7) Uani 1 1 d . . . B 2
C2A C -0.12520(17) 0.1070(3) 0.2084(2) 0.0342(10) Uani 1 1 d . . . B 2
H2AA H -0.1400 0.1546 0.2336 0.041 Uiso 1 1 calc R U . B 2
H2AB H -0.1543 0.0756 0.1845 0.041 Uiso 1 1 calc R U . B 2
N3A N 0.07632(17) 0.0000 0.4904(2) 0.0204(9) Uani 1 2 d S T P B 2
C4A C -0.05916(15) 0.0722(3) 0.31161(18) 0.0228(8) Uani 1 1 d . . . B 2
C5A C -0.04809(15) 0.1587(3) 0.32676(19) 0.0260(8) Uani 1 1 d . . . B 2
H5A H -0.0674 0.2019 0.3024 0.031 Uiso 1 1 calc R U . B 2
C6A C -0.01037(15) 0.1861(3) 0.37550(19) 0.0248(8) Uani 1 1 d . . . B 2
C7A C 0.00331(16) 0.2774(3) 0.3885(2) 0.0300(9) Uani 1 1 d . . . B 2
C8A C -0.02097(19) 0.3539(3) 0.3499(3) 0.0410(11) Uani 1 1 d . . . B 2
H8AA H -0.0147 0.4076 0.3760 0.049 Uiso 1 1 calc R U . B 2
H8AB H -0.0588 0.3450 0.3434 0.049 Uiso 1 1 calc R U . B 2
C9A C 0.0012(2) 0.3655(4) 0.2809(3) 0.0553(15) Uani 1 1 d . . . B 2
H9AA H -0.0068 0.3139 0.2539 0.083 Uiso 1 1 calc R U . B 2
H9AB H 0.0387 0.3733 0.2870 0.083 Uiso 1 1 calc R U . B 2
H9AC H -0.0146 0.4166 0.2588 0.083 Uiso 1 1 calc R U . B 2
C10A C 0.04264(16) 0.2770(3) 0.4394(2) 0.0290(9) Uani 1 1 d . . . B 2
C11A C 0.07271(17) 0.3539(3) 0.4714(3) 0.0378(10) Uani 1 1 d . . . B 2
H11A H 0.0774 0.3444 0.5197 0.045 Uiso 1 1 calc R U . B 2
H11B H 0.0521 0.4074 0.4635 0.045 Uiso 1 1 calc R U . B 2
C12A C 0.1264(2) 0.3670(3) 0.4447(3) 0.0485(13) Uani 1 1 d . . . B 2
H12A H 0.1220 0.3808 0.3975 0.073 Uiso 1 1 calc R U . B 2
H12B H 0.1467 0.3137 0.4511 0.073 Uiso 1 1 calc R U . B 2
H12C H 0.1444 0.4147 0.4685 0.073 Uiso 1 1 calc R U . B 2
C13A C 0.05268(15) 0.1859(3) 0.45652(19) 0.0242(8) Uani 1 1 d . . . B 2
C14A C 0.09060(15) 0.1585(3) 0.50503(19) 0.0243(8) Uani 1 1 d . . . B 2
H14A H 0.1097 0.2017 0.5296 0.029 Uiso 1 1 calc R U . B 2
C15A C 0.10222(15) 0.0719(3) 0.51960(18) 0.0226(8) Uani 1 1 d . . . B 2
C16A C 0.14460(15) 0.0447(3) 0.56768(18) 0.0238(8) Uani 1 1 d . . . B 2
C17A C 0.18263(16) 0.1070(3) 0.6048(2) 0.0296(9) Uani 1 1 d . . . B 2
H17A H 0.1982 0.0780 0.6450 0.036 Uiso 1 1 calc R U . B 2
H17B H 0.1636 0.1586 0.6188 0.036 Uiso 1 1 calc R U . B 2
C18A C 0.22638(18) 0.1364(4) 0.5617(2) 0.0424(11) Uani 1 1 d . . . B 2
H18A H 0.2455 0.0855 0.5482 0.064 Uiso 1 1 calc R U . B 2
H18B H 0.2500 0.1755 0.5873 0.064 Uiso 1 1 calc R U . B 2
H18C H 0.2112 0.1667 0.5225 0.064 Uiso 1 1 calc R U . B 2
C3A C -0.09602(15) 0.0445(3) 0.25680(19) 0.0270(8) Uani 1 1 d . . . B 2
N1A N -0.03593(18) 0.0000 0.3446(2) 0.0232(9) Uani 1 2 d S T P B 2
C1B C 0.1259(4) 0.5000 0.1959(6) 0.082(3) Uani 1 2 d S T P C 3
H1B H 0.0901 0.5000 0.1820 0.099 Uiso 1 2 calc R U P C 3
C2B C 0.1412(3) 0.5000 0.2629(4) 0.0517(18) Uani 1 2 d S T P C 3
H2B H 0.1161 0.5000 0.2944 0.062 Uiso 1 2 calc R U P C 3
C3B C 0.1934(3) 0.5000 0.2835(3) 0.0440(16) Uani 1 2 d S T P C 3
H3B H 0.2041 0.5000 0.3292 0.053 Uiso 1 2 calc R U P C 3
C4B C 0.2309(3) 0.5000 0.2362(3) 0.0437(16) Uani 1 2 d S T P C 3
H4B H 0.2665 0.5000 0.2508 0.052 Uiso 1 2 calc R U P C 3
C5B C 0.2163(4) 0.5000 0.1690(3) 0.0496(18) Uani 1 2 d S T P C 3
H5B H 0.2418 0.5000 0.1378 0.060 Uiso 1 2 calc R U P C 3
C6B C 0.1628(4) 0.5000 0.1474(5) 0.076(3) Uani 1 2 d S T P C 3
H6B H 0.1518 0.5000 0.1017 0.091 Uiso 1 2 calc R U P C 3


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu9 0.513(6) . ?
Lu1 Lu14 0.84(3) . ?
Lu1 Lu10 1.24(2) . ?
Lu1 Lu1 1.301(7) 6 ?
Lu1 Lu15 1.39(3) . ?
Lu1 Lu9 1.420(8) 6 ?
Lu1 Lu13 1.614(17) 6 ?
Lu1 Lu6 1.978(9) . ?
Lu1 Lu14 2.01(3) 6 ?
Lu1 C83 2.106(4) . ?
Lu1 C75 2.212(4) . ?
Lu1 Lu13 2.218(18) . ?
Lu2 Lu2 1.234(4) 6 ?
Lu2 Lu3 1.333(4) . ?
Lu2 Lu12 1.36(2) . ?
Lu2 Lu8 2.126(7) . ?
Lu2 Lu4 2.148(5) . ?
Lu2 C11 2.246(2) . ?
Lu2 Lu3 2.253(4) 6 ?
Lu2 Lu11 2.273(17) . ?
Lu2 C12 2.367(3) . ?
Lu2 C10 2.423(3) . ?
Lu2 Lu12 2.48(2) 6 ?
Lu2 C30 2.561(3) . ?
Lu3 Lu12 0.573(19) . ?
Lu3 Lu4 0.832(4) . ?
Lu3 Lu8 1.109(8) . ?
Lu3 Lu11 1.56(2) . ?
Lu3 Lu5 1.779(5) . ?
Lu3 C27 2.120(3) . ?
Lu3 Lu2 2.253(4) 6 ?
Lu3 Lu6 2.276(7) . ?
Lu3 C28 2.307(4) . ?
Lu3 Lu8 2.393(7) 6 ?
Lu3 C10 2.463(3) . ?
Lu4 Lu8 1.008(8) . ?
Lu4 Lu12 1.08(3) . ?
Lu4 Lu5 1.241(6) . ?
Lu4 Lu11 1.40(2) . ?
Lu4 Lu6 1.898(9) . ?
Lu4 C50 2.133(5) . ?
Lu4 C49 2.157(4) . ?
Lu4 C25 2.161(4) . ?
Lu4 C27 2.265(5) . ?
Lu4 C26 2.313(4) . ?
Lu5 Lu6 0.761(6) . ?
Lu5 Lu11 1.121(19) . ?
Lu5 Lu13 1.53(2) 6 ?
Lu5 Lu8 1.678(8) . ?
Lu5 Lu12 1.97(2) . ?
Lu5 Lu14 2.11(3) . ?
Lu5 Lu7 2.123(5) . ?
Lu5 C48 2.307(4) . ?
Lu5 Lu9 2.338(11) . ?
Lu5 C70 2.393(5) . ?
Lu6 Lu13 1.035(19) 6 ?
Lu6 Lu11 1.119(18) . ?
Lu6 Lu14 1.52(3) . ?
Lu6 Lu9 1.697(13) . ?
Lu6 Lu7 1.941(8) . ?
Lu6 Lu10 2.040(12) . ?
Lu6 C69 2.181(6) . ?
Lu6 C70 2.184(6) . ?
Lu7 Lu13 1.071(19) . ?
Lu7 Lu13 1.071(19) 6 ?
Lu7 Lu10 1.23(3) . ?
Lu7 Lu9 1.843(9) . ?
Lu7 Lu9 1.843(9) 6 ?
Lu7 Lu6 1.941(8) 6 ?
Lu7 Lu5 2.123(5) 6 ?
Lu7 C66 2.188(5) . ?
Lu7 C65 2.252(5) . ?
Lu7 C80 2.285(5) . ?
Lu8 Lu12 1.66(2) . ?
Lu8 Lu8 1.682(14) 6 ?
Lu8 Lu11 2.13(2) . ?
Lu8 C26 2.203(5) . ?
Lu8 C8 2.254(6) . ?
Lu8 C25 2.270(5) . ?
Lu8 Lu3 2.393(7) 6 ?
Lu9 Lu10 0.864(17) . ?
Lu9 Lu14 1.03(2) . ?
Lu9 Lu13 1.15(2) 6 ?
Lu9 Lu9 1.35(2) 6 ?
Lu9 Lu1 1.420(8) 6 ?
Lu9 Lu15 1.82(3) . ?
Lu9 Lu13 1.93(2) . ?
Lu9 C83 2.120(10) . ?
Lu9 Lu14 2.13(3) 6 ?
Lu10 Lu9 0.864(17) 6 ?
Lu10 Lu13 1.13(2) 6 ?
Lu10 Lu13 1.13(2) . ?
Lu10 Lu1 1.24(2) 6 ?
Lu10 Lu14 1.81(3) 6 ?
Lu10 Lu14 1.81(3) . ?
Lu10 Lu6 2.040(12) 6 ?
Lu10 C81 2.184(13) . ?
Lu11 Lu12 1.43(3) . ?
Lu11 Lu14 1.60(3) . ?
Lu11 Lu13 2.04(3) 6 ?
Lu11 C51 2.180(14) . ?
Lu11 C71 2.189(15) . ?
Lu12 C28 1.99(2) . ?
Lu12 C27 2.08(3) . ?
Lu12 C29 2.08(2) . ?
Lu12 C50 2.35(2) . ?
Lu12 C52 2.385(19) . ?
Lu13 Lu6 1.035(19) 6 ?
Lu13 Lu9 1.15(2) 6 ?
Lu13 Lu5 1.53(2) 6 ?
Lu13 Lu1 1.614(17) 6 ?
Lu13 Lu14 1.66(3) 6 ?
Lu13 Lu13 1.78(4) 6 ?
Lu13 Lu11 2.04(3) 6 ?
Lu13 C64 2.329(14) . ?
Lu14 Lu15 1.59(3) . ?
Lu14 Lu13 1.66(3) 6 ?
Lu14 Lu1 2.01(3) 6 ?
Lu14 Lu9 2.13(3) 6 ?
Lu14 C84 2.333(19) . ?
Lu14 C72 2.34(2) . ?
Lu15 Lu1 1.39(3) 6 ?
Lu15 Lu14 1.59(3) 6 ?
Lu15 Lu9 1.82(3) 6 ?
Lu15 C57 2.35(4) . ?
Lu15 C76 2.44(4) . ?
Lu15 C56 2.55(3) . ?
Lu15 C58 2.58(3) . ?
Lu15 Lu13 2.70(4) 6 ?
C1 C9 1.2880 . ?
C1 C10 1.3160 . ?
C1 C2 1.4391 . ?
C2 C12 1.3492 . ?
C2 C3 1.6046 . ?
C3 C15 1.3199 . ?
C3 C4 1.3424 . ?
C4 C18 1.3206 . ?
C4 C5 1.3752 . ?
C5 C6 1.3102 . ?
C5 C9 1.3169 . ?
C6 C20 1.2618 . ?
C6 C7 1.3491 . ?
C6 C9 1.9950 . ?
C7 C8 1.3535 . ?
C7 C23 1.3776 . ?
C8 C26 1.3372 . ?
C8 C9 1.3834 . ?
C10 C27 1.3436 . ?
C10 C11 1.3513 . ?
C10 C28 2.0257 . ?
C11 C12 1.3414 . ?
C11 C30 1.5393 . ?
C12 C13 1.4111 . ?
C13 C14 1.3493 . ?
C13 C32 1.4547 . ?
C14 C35 1.4171 . ?
C14 C15 1.4293 . ?
C15 C16 1.4329 . ?
C16 C36 1.4263 . ?
C16 C17 1.7469 . ?
C17 C39 1.4943 . ?
C17 C18 1.5958 . ?
C18 C19 1.2783 . ?
C19 C20 1.2556 . ?
C19 C41 1.6152 . ?
C20 C21 1.4687 . ?
C21 C42 1.3275 . ?
C21 C22 1.4868 . ?
C22 C23 1.4216 . ?
C22 C45 1.4770 . ?
C23 C24 1.1395 . ?
C24 C46 1.5055 . ?
C24 C25 1.5534 . ?
C25 C26 1.3460 . ?
C25 C49 1.5509 . ?
C26 C27 1.3845 . ?
C27 C28 1.1946 . ?
C28 C29 1.3612 . ?
C28 C50 1.6154 . ?
C29 C52 1.2761 . ?
C29 C30 1.4342 . ?
C30 C31 1.2618 . ?
C31 C32 1.5248 . ?
C31 C54 1.5770 . ?
C32 C33 1.5163 . ?
C33 C55 1.5377 . ?
C33 C34 1.5711 . ?
C34 C35 1.4105 . ?
C34 C58 1.4680 . ?
C35 C36 1.4518 . ?
C36 C37 1.2488 . ?
C37 C59 1.4814 . ?
C37 C38 1.5131 . ?
C38 C39 1.4553 . ?
C38 C61 1.5325 . ?
C39 C40 1.5151 . ?
C40 C63 1.3622 . ?
C40 C41 1.4305 . ?
C41 C42 1.2585 . ?
C42 C43 1.2591 . ?
C43 C44 1.4667 . ?
C43 C64 1.7837 . ?
C44 C45 1.2912 . ?
C44 C66 1.4644 . ?
C45 C46 1.2431 . ?
C46 C47 1.4719 . ?
C47 C67 1.3971 . ?
C47 C48 1.6070 . ?
C48 C49 1.4614 . ?
C48 C70 1.6014 . ?
C49 C50 1.3572 . ?
C50 C51 1.4632 . ?
C51 C71 1.4167 . ?
C51 C52 1.5285 . ?
C52 C53 1.2663 . ?
C53 C54 1.5061 . ?
C53 C73 1.5157 . ?
C54 C55 1.4834 . ?
C55 C56 1.2993 . ?
C56 C74 1.2600 . ?
C56 C57 1.4636 . ?
C57 C76 1.5346 . ?
C57 C58 1.5387 . ?
C58 C59 1.4966 . ?
C59 C60 1.5266 . ?
C60 C77 1.4894 . ?
C60 C61 1.4972 . ?
C61 C62 1.4866 . ?
C62 C79 1.3858 . ?
C62 C63 1.5731 . ?
C63 C64 1.3365 . ?
C64 C65 1.4734 . ?
C65 C80 1.3133 . ?
C65 C66 1.5690 . ?
C66 C67 1.5788 . ?
C67 C68 1.5154 . ?
C68 C69 1.3974 . ?
C68 C81 1.4629 . ?
C69 C70 1.4497 . ?
C69 C84 1.4553 . ?
C70 C71 1.4668 . ?
C71 C72 1.4302 . ?
C72 C73 1.3522 . ?
C72 C84 1.4325 . ?
C73 C74 1.3884 . ?
C74 C75 1.4078 . ?
C75 C83 1.4304 . ?
C75 C76 1.4598 . ?
C76 C77 1.4564 . ?
C77 C78 1.3984 . ?
C78 C82 1.4511 . ?
C78 C79 1.5192 . ?
C79 C80 1.5019 . ?
C80 C81 1.4862 . ?
C81 C82 1.4828 . ?
C82 C83 1.4581 . ?
C83 C84 1.4600 . ?
Ni1A N1A 1.951(4) . ?
Ni1A N3A 1.957(4) . ?
Ni1A N2A 1.963(3) 6 ?
Ni1A N2A 1.963(3) . ?
C1A C2A 1.531(6) . ?
N2A C13A 1.381(5) . ?
N2A C6A 1.384(5) . ?
C2A C3A 1.502(5) . ?
N3A C15A 1.375(4) . ?
N3A C15A 1.375(4) 6 ?
C4A C5A 1.365(6) . ?
C4A N1A 1.382(5) . ?
C4A C3A 1.443(5) . ?
C5A C6A 1.373(5) . ?
C6A C7A 1.441(6) . ?
C7A C10A 1.366(6) . ?
C7A C8A 1.495(6) . ?
C8A C9A 1.535(8) . ?
C10A C13A 1.436(5) . ?
C10A C11A 1.504(6) . ?
C11A C12A 1.515(7) . ?
C13A C14A 1.374(5) . ?
C14A C15A 1.367(6) . ?
C15A C16A 1.443(5) . ?
C16A C16A 1.351(8) 6 ?
C16A C17A 1.501(5) . ?
C17A C18A 1.523(6) . ?
C3A C3A 1.345(8) 6 ?
N1A C4A 1.381(5) 6 ?
C1B C2B 1.361(13) . ?
C1B C6B 1.397(16) . ?
C2B C3B 1.356(11) . ?
C3B C4B 1.391(10) . ?
C4B C5B 1.360(10) . ?
C5B C6B 1.394(13) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu9 Lu1 Lu14 96(2) . . ?
Lu9 Lu1 Lu10 34.4(15) . . ?
Lu14 Lu1 Lu10 119.8(19) . . ?
Lu9 Lu1 Lu1 92.6(15) . 6 ?
Lu14 Lu1 Lu1 138.4(12) . 6 ?
Lu10 Lu1 Lu1 58.3(7) . 6 ?
Lu9 Lu1 Lu15 141(2) . . ?
Lu14 Lu1 Lu15 87.2(19) . . ?
Lu10 Lu1 Lu15 112.8(11) . . ?
Lu1 Lu1 Lu15 62.0(7) 6 . ?
Lu9 Lu1 Lu9 71.5(16) . 6 ?
Lu14 Lu1 Lu9 138.4(15) . 6 ?
Lu10 Lu1 Lu9 37.1(7) . 6 ?
Lu1 Lu1 Lu9 21.2(2) 6 6 ?
Lu15 Lu1 Lu9 80.6(7) . 6 ?
Lu9 Lu1 Lu13 21.5(14) . 6 ?
Lu14 Lu1 Lu13 77.9(19) . 6 ?
Lu10 Lu1 Lu13 44.2(9) . 6 ?
Lu1 Lu1 Lu13 98.5(7) 6 6 ?
Lu15 Lu1 Lu13 127.7(16) . 6 ?
Lu9 Lu1 Lu13 78.7(8) 6 6 ?
Lu9 Lu1 Lu6 50.4(13) . . ?
Lu14 Lu1 Lu6 46.5(18) . . ?
Lu10 Lu1 Lu6 74.8(8) . . ?
Lu1 Lu1 Lu6 121.5(2) 6 . ?
Lu15 Lu1 Lu6 116.3(14) . . ?
Lu9 Lu1 Lu6 105.4(5) 6 . ?
Lu13 Lu1 Lu6 31.5(7) 6 . ?
Lu9 Lu1 Lu14 95.9(16) . 6 ?
Lu14 Lu1 Lu14 122.3(17) . 6 ?
Lu10 Lu1 Lu14 62.5(10) . 6 ?
Lu1 Lu1 Lu14 16.1(5) 6 6 ?
Lu15 Lu1 Lu14 51.8(10) . 6 ?
Lu9 Lu1 Lu14 29.0(7) 6 6 ?
Lu13 Lu1 Lu14 95.8(11) 6 6 ?
Lu6 Lu1 Lu14 112.1(8) . 6 ?
Lu9 Lu1 C83 84.6(14) . . ?
Lu14 Lu1 C83 100.9(12) . . ?
Lu10 Lu1 C83 103.0(6) . . ?
Lu1 Lu1 C83 120.38(16) 6 . ?
Lu15 Lu1 C83 132.9(15) . . ?
Lu9 Lu1 C83 116.5(5) 6 . ?
Lu13 Lu1 C83 99.2(5) 6 . ?
Lu6 Lu1 C83 101.6(3) . . ?
Lu14 Lu1 C83 136.4(5) 6 . ?
Lu9 Lu1 C75 123.1(14) . . ?
Lu14 Lu1 C75 97.5(15) . . ?
Lu10 Lu1 C75 133.4(7) . . ?
Lu1 Lu1 C75 111.41(16) 6 . ?
Lu15 Lu1 C75 94.6(15) . . ?
Lu9 Lu1 C75 122.9(5) 6 . ?
Lu13 Lu1 C75 136.6(6) 6 . ?
Lu6 Lu1 C75 126.4(3) . . ?
Lu14 Lu1 C75 121.3(8) 6 . ?
C83 Lu1 C75 38.59(7) . . ?
Lu9 Lu1 Lu13 50.2(15) . . ?
Lu14 Lu1 Lu13 116.6(16) . . ?
Lu10 Lu1 Lu13 19.4(7) . . ?
Lu1 Lu1 Lu13 46.0(5) 6 . ?
Lu15 Lu1 Lu13 94.0(11) . . ?
Lu9 Lu1 Lu13 27.1(6) 6 . ?
Lu13 Lu1 Lu13 52.5(12) 6 . ?
Lu6 Lu1 Lu13 78.3(5) . . ?
Lu14 Lu1 Lu13 45.8(9) 6 . ?
C83 Lu1 Lu13 121.5(5) . . ?
C75 Lu1 Lu13 145.2(5) . . ?
Lu2 Lu2 Lu3 122.63(14) 6 . ?
Lu2 Lu2 Lu12 147.1(10) 6 . ?
Lu3 Lu2 Lu12 24.6(9) . . ?
Lu2 Lu2 Lu8 96.0(2) 6 . ?
Lu3 Lu2 Lu8 26.6(2) . . ?
Lu12 Lu2 Lu8 51.2(9) . . ?
Lu2 Lu2 Lu4 122.12(12) 6 . ?
Lu3 Lu2 Lu4 5.70(16) . . ?
Lu12 Lu2 Lu4 25.0(9) . . ?
Lu8 Lu2 Lu4 27.3(2) . . ?
Lu2 Lu2 C11 108.86(12) 6 . ?
Lu3 Lu2 C11 103.90(17) . . ?
Lu12 Lu2 C11 91.4(10) . . ?
Lu8 Lu2 C11 115.45(18) . . ?
Lu4 Lu2 C11 108.79(18) . . ?
Lu2 Lu2 Lu3 29.90(10) 6 6 ?
Lu3 Lu2 Lu3 92.7(2) . 6 ?
Lu12 Lu2 Lu3 117.2(10) . 6 ?
Lu8 Lu2 Lu3 66.2(2) . 6 ?
Lu4 Lu2 Lu3 92.40(15) . 6 ?
C11 Lu2 Lu3 121.71(14) . 6 ?
Lu2 Lu2 Lu11 128.1(4) 6 . ?
Lu3 Lu2 Lu11 41.8(6) . . ?
Lu12 Lu2 Lu11 36.3(11) . . ?
Lu8 Lu2 Lu11 57.8(6) . . ?
Lu4 Lu2 Lu11 36.7(6) . . ?
C11 Lu2 Lu11 122.6(4) . . ?
Lu3 Lu2 Lu11 106.9(4) 6 . ?
Lu2 Lu2 C12 76.40(11) 6 . ?
Lu3 Lu2 C12 131.14(17) . . ?
Lu12 Lu2 C12 124.5(10) . . ?
Lu8 Lu2 C12 128.9(2) . . ?
Lu4 Lu2 C12 136.78(17) . . ?
C11 Lu2 C12 33.7 . . ?
Lu3 Lu2 C12 96.35(14) 6 . ?
Lu11 Lu2 C12 155.4(4) . . ?
Lu2 Lu2 C10 110.43(11) 6 . ?
Lu3 Lu2 C10 75.82(16) . . ?
Lu12 Lu2 C10 72.8(10) . . ?
Lu8 Lu2 C10 82.35(17) . . ?
Lu4 Lu2 C10 81.40(16) . . ?
C11 Lu2 C10 33.4 . . ?
Lu3 Lu2 C10 105.61(14) 6 . ?
Lu11 Lu2 C10 109.1(5) . . ?
C12 Lu2 C10 55.47(5) . . ?
Lu2 Lu2 Lu12 17.3(6) 6 6 ?
Lu3 Lu2 Lu12 105.4(6) . 6 ?
Lu12 Lu2 Lu12 129.8(15) . 6 ?
Lu8 Lu2 Lu12 78.9(6) . 6 ?
Lu4 Lu2 Lu12 104.9(6) . 6 ?
C11 Lu2 Lu12 118.1(6) . 6 ?
Lu3 Lu2 Lu12 12.7(6) 6 6 ?
Lu11 Lu2 Lu12 115.6(7) . 6 ?
C12 Lu2 Lu12 88.7(6) . 6 ?
C10 Lu2 Lu12 109.4(6) . 6 ?
Lu2 Lu2 C30 135.61(10) 6 . ?
Lu3 Lu2 C30 97.65(17) . . ?
Lu12 Lu2 C30 75.3(10) . . ?
Lu8 Lu2 C30 121.7(2) . . ?
Lu4 Lu2 C30 99.82(17) . . ?
C11 Lu2 C30 36.6 . . ?
Lu3 Lu2 C30 157.87(13) 6 . ?
Lu11 Lu2 C30 93.7(4) . . ?
C12 Lu2 C30 62.23(6) . . ?
C10 Lu2 C30 58.76(6) . . ?
Lu12 Lu2 C30 150.6(6) 6 . ?
Lu12 Lu3 Lu4 99(3) . . ?
Lu12 Lu3 Lu8 159(3) . . ?
Lu4 Lu3 Lu8 60.6(4) . . ?
Lu12 Lu3 Lu2 80(3) . . ?
Lu4 Lu3 Lu2 165.1(4) . . ?
Lu8 Lu3 Lu2 120.7(4) . . ?
Lu12 Lu3 Lu11 66(2) . . ?
Lu4 Lu3 Lu11 63.3(8) . . ?
Lu8 Lu3 Lu11 104.8(8) . . ?
Lu2 Lu3 Lu11 103.4(8) . . ?
Lu12 Lu3 Lu5 101(2) . . ?
Lu4 Lu3 Lu5 38.5(3) . . ?
Lu8 Lu3 Lu5 66.4(4) . . ?
Lu2 Lu3 Lu5 126.9(2) . . ?
Lu11 Lu3 Lu5 38.6(7) . . ?
Lu12 Lu3 C27 78(3) . . ?
Lu4 Lu3 C27 89.0(4) . . ?
Lu8 Lu3 C27 95.8(3) . . ?
Lu2 Lu3 C27 105.18(19) . . ?
Lu11 Lu3 C27 128.8(6) . . ?
Lu5 Lu3 C27 127.3(3) . . ?
Lu12 Lu3 Lu2 107(3) . 6 ?
Lu4 Lu3 Lu2 148.3(4) . 6 ?
Lu8 Lu3 Lu2 93.3(4) . 6 ?
Lu2 Lu3 Lu2 27.48(12) . 6 ?
Lu11 Lu3 Lu2 112.2(7) . 6 ?
Lu5 Lu3 Lu2 117.20(17) . 6 ?
C27 Lu3 Lu2 112.80(17) . 6 ?
Lu12 Lu3 Lu6 93(2) . . ?
Lu4 Lu3 Lu6 53.2(4) . . ?
Lu8 Lu3 Lu6 79.3(4) . . ?
Lu2 Lu3 Lu6 112.0(2) . . ?
Lu11 Lu3 Lu6 26.3(6) . . ?
Lu5 Lu3 Lu6 16.5(2) . . ?
C27 Lu3 Lu6 139.4(3) . . ?
Lu2 Lu3 Lu6 107.8(2) 6 . ?
Lu12 Lu3 C28 50(3) . . ?
Lu4 Lu3 C28 83.2(4) . . ?
Lu8 Lu3 C28 118.0(3) . . ?
Lu2 Lu3 C28 106.77(19) . . ?
Lu11 Lu3 C28 99.9(6) . . ?
Lu5 Lu3 C28 114.0(2) . . ?
C27 Lu3 C28 30.9 . . ?
Lu2 Lu3 C28 127.37(17) 6 . ?
Lu6 Lu3 C28 118.4(2) . . ?
Lu12 Lu3 Lu8 161(3) . 6 ?
Lu4 Lu3 Lu8 97.5(4) . 6 ?
Lu8 Lu3 Lu8 39.0(4) . 6 ?
Lu2 Lu3 Lu8 81.8(3) . 6 ?
Lu11 Lu3 Lu8 115.3(6) . 6 ?
Lu5 Lu3 Lu8 86.9(2) . 6 ?
C27 Lu3 Lu8 110.2(2) . 6 ?
Lu2 Lu3 Lu8 54.4(2) 6 6 ?
Lu6 Lu3 Lu8 91.2(2) . 6 ?
C28 Lu3 Lu8 141.0(2) . 6 ?
Lu12 Lu3 C10 77(2) . . ?
Lu4 Lu3 C10 122.0(4) . . ?
Lu8 Lu3 C10 108.4(4) . . ?
Lu2 Lu3 C10 72.52(16) . . ?
Lu11 Lu3 C10 143.3(6) . . ?
Lu5 Lu3 C10 160.3(2) . . ?
C27 Lu3 C10 33.0 . . ?
Lu2 Lu3 C10 81.40(14) 6 . ?
Lu6 Lu3 C10 168.0(2) . . ?
C28 Lu3 C10 50.13(6) . . ?
Lu8 Lu3 C10 100.5(2) 6 . ?
Lu3 Lu4 Lu8 73.4(5) . . ?
Lu3 Lu4 Lu12 31.4(10) . . ?
Lu8 Lu4 Lu12 104.7(12) . . ?
Lu3 Lu4 Lu5 116.9(4) . . ?
Lu8 Lu4 Lu5 96.0(6) . . ?
Lu12 Lu4 Lu5 116.1(14) . . ?
Lu3 Lu4 Lu11 84.5(8) . . ?
Lu8 Lu4 Lu11 123.8(7) . . ?
Lu12 Lu4 Lu11 68.9(14) . . ?
Lu5 Lu4 Lu11 49.9(8) . . ?
Lu3 Lu4 Lu6 106.3(4) . . ?
Lu8 Lu4 Lu6 102.9(5) . . ?
Lu12 Lu4 Lu6 101.9(13) . . ?
Lu5 Lu4 Lu6 14.4(3) . . ?
Lu11 Lu4 Lu6 35.8(7) . . ?
Lu3 Lu4 C50 114.9(5) . . ?
Lu8 Lu4 C50 145.5(4) . . ?
Lu12 Lu4 C50 87.3(12) . . ?
Lu5 Lu4 C50 107.6(3) . . ?
Lu11 Lu4 C50 90.8(6) . . ?
Lu6 Lu4 C50 106.1(3) . . ?
Lu3 Lu4 Lu2 9.2(2) . . ?
Lu8 Lu4 Lu2 75.1(5) . . ?
Lu12 Lu4 Lu2 31.9(11) . . ?
Lu5 Lu4 Lu2 107.9(2) . . ?
Lu11 Lu4 Lu2 76.5(7) . . ?
Lu6 Lu4 Lu2 97.1(2) . . ?
C50 Lu4 Lu2 118.7(3) . . ?
Lu3 Lu4 C49 149.0(5) . . ?
Lu8 Lu4 C49 121.3(5) . . ?
Lu12 Lu4 C49 124.2(12) . . ?
Lu5 Lu4 C49 90.1(3) . . ?
Lu11 Lu4 C49 104.2(7) . . ?
Lu6 Lu4 C49 97.1(3) . . ?
C50 Lu4 C49 36.88(7) . . ?
Lu2 Lu4 C49 154.9(3) . . ?
Lu3 Lu4 C25 126.7(4) . . ?
Lu8 Lu4 C25 83.0(4) . . ?
Lu12 Lu4 C25 129.3(14) . . ?
Lu5 Lu4 C25 112.5(4) . . ?
Lu11 Lu4 C25 145.8(7) . . ?
Lu6 Lu4 C25 125.5(3) . . ?
C50 Lu4 C25 65.01(11) . . ?
Lu2 Lu4 C25 135.6(3) . . ?
C49 Lu4 C25 42.10(8) . . ?
Lu3 Lu4 C27 69.4(4) . . ?
Lu8 Lu4 C27 90.6(4) . . ?
Lu12 Lu4 C27 66.2(14) . . ?
Lu5 Lu4 C27 171.9(3) . . ?
Lu11 Lu4 C27 128.9(8) . . ?
Lu6 Lu4 C27 164.2(3) . . ?
C50 Lu4 C27 64.41(14) . . ?
Lu2 Lu4 C27 78.2(2) . . ?
C49 Lu4 C27 82.53(14) . . ?
C25 Lu4 C27 63.73(11) . . ?
Lu3 Lu4 C26 92.0(4) . . ?
Lu8 Lu4 C26 71.1(3) . . ?
Lu12 Lu4 C26 99.6(13) . . ?
Lu5 Lu4 C26 144.2(4) . . ?
Lu11 Lu4 C26 162.4(7) . . ?
Lu6 Lu4 C26 158.5(3) . . ?
C50 Lu4 C26 75.09(13) . . ?
Lu2 Lu4 C26 100.9(2) . . ?
C49 Lu4 C26 70.71(11) . . ?
C25 Lu4 C26 34.80(6) . . ?
C27 Lu4 C26 35.19(7) . . ?
Lu6 Lu5 Lu11 70.0(13) . . ?
Lu6 Lu5 Lu4 141.7(8) . . ?
Lu11 Lu5 Lu4 72.3(11) . . ?
Lu6 Lu5 Lu13 37.2(9) . 6 ?
Lu11 Lu5 Lu13 99.0(13) . 6 ?
Lu4 Lu5 Lu13 149.0(6) . 6 ?
Lu6 Lu5 Lu8 144.2(6) . . ?
Lu11 Lu5 Lu8 97.0(11) . . ?
Lu4 Lu5 Lu8 36.7(3) . . ?
Lu13 Lu5 Lu8 120.0(7) 6 . ?
Lu6 Lu5 Lu3 122.0(7) . . ?
Lu11 Lu5 Lu3 59.9(11) . . ?
Lu4 Lu5 Lu3 24.66(17) . . ?
Lu13 Lu5 Lu3 125.5(6) 6 . ?
Lu8 Lu5 Lu3 37.3(3) . . ?
Lu6 Lu5 Lu12 112.4(10) . . ?
Lu11 Lu5 Lu12 45.2(13) . . ?
Lu4 Lu5 Lu12 29.5(8) . . ?
Lu13 Lu5 Lu12 127.6(10) 6 . ?
Lu8 Lu5 Lu12 53.2(6) . . ?
Lu3 Lu5 Lu12 16.5(5) . . ?
Lu6 Lu5 Lu14 32.3(7) . . ?
Lu11 Lu5 Lu14 48.1(12) . . ?
Lu4 Lu5 Lu14 112.1(6) . . ?
Lu13 Lu5 Lu14 51.1(9) 6 . ?
Lu8 Lu5 Lu14 114.9(6) . . ?
Lu3 Lu5 Lu14 90.1(6) . . ?
Lu12 Lu5 Lu14 82.8(10) . . ?
Lu6 Lu5 Lu7 65.9(7) . . ?
Lu11 Lu5 Lu7 120.3(10) . . ?
Lu4 Lu5 Lu7 132.0(3) . . ?
Lu13 Lu5 Lu7 28.7(7) 6 . ?
Lu8 Lu5 Lu7 96.2(3) . . ?
Lu3 Lu5 Lu7 116.8(2) . . ?
Lu12 Lu5 Lu7 127.8(7) . . ?
Lu14 Lu5 Lu7 73.7(7) . . ?
Lu6 Lu5 C48 104.1(6) . . ?
Lu11 Lu5 C48 110.6(8) . . ?
Lu4 Lu5 C48 95.2(3) . . ?
Lu13 Lu5 C48 115.5(6) 6 . ?
Lu8 Lu5 C48 111.8(3) . . ?
Lu3 Lu5 C48 119.0(2) . . ?
Lu12 Lu5 C48 113.3(7) . . ?
Lu14 Lu5 C48 130.3(6) . . ?
Lu7 Lu5 C48 117.5(2) . . ?
Lu6 Lu5 Lu9 27.3(6) . . ?
Lu11 Lu5 Lu9 74.3(11) . . ?
Lu4 Lu5 Lu9 131.8(3) . . ?
Lu13 Lu5 Lu9 25.2(6) 6 . ?
Lu8 Lu5 Lu9 118.1(3) . . ?
Lu3 Lu5 Lu9 107.3(3) . . ?
Lu12 Lu5 Lu9 104.8(8) . . ?
Lu14 Lu5 Lu9 26.2(7) . . ?
Lu7 Lu5 Lu9 48.5(3) . . ?
C48 Lu5 Lu9 129.0(3) . . ?
Lu6 Lu5 C70 65.1(6) . . ?
Lu11 Lu5 C70 89.3(9) . . ?
Lu4 Lu5 C70 121.3(3) . . ?
Lu13 Lu5 C70 87.5(6) 6 . ?
Lu8 Lu5 C70 150.2(3) . . ?
Lu3 Lu5 C70 135.8(2) . . ?
Lu12 Lu5 C70 120.8(6) . . ?
Lu14 Lu5 C70 90.9(6) . . ?
Lu7 Lu5 C70 105.8(2) . . ?
C48 Lu5 C70 39.79(7) . . ?
Lu9 Lu5 C70 91.7(3) . . ?
Lu5 Lu6 Lu13 116.3(14) . 6 ?
Lu5 Lu6 Lu11 70.3(13) . . ?
Lu13 Lu6 Lu11 141.9(13) 6 . ?
Lu5 Lu6 Lu14 132.2(10) . . ?
Lu13 Lu6 Lu14 78.1(14) 6 . ?
Lu11 Lu6 Lu14 72.6(14) . . ?
Lu5 Lu6 Lu9 140.9(8) . . ?
Lu13 Lu6 Lu9 41.7(10) 6 . ?
Lu11 Lu6 Lu9 107.9(12) . . ?
Lu14 Lu6 Lu9 36.9(10) . . ?
Lu5 Lu6 Lu4 23.9(5) . . ?
Lu13 Lu6 Lu4 129.1(10) 6 . ?
Lu11 Lu6 Lu4 46.9(12) . . ?
Lu14 Lu6 Lu4 110.8(8) . . ?
Lu9 Lu6 Lu4 132.9(4) . . ?
Lu5 Lu6 Lu7 93.1(7) . . ?
Lu13 Lu6 Lu7 23.2(10) 6 . ?
Lu11 Lu6 Lu7 136.4(8) . . ?
Lu14 Lu6 Lu7 93.5(10) . . ?
Lu9 Lu6 Lu7 60.4(4) . . ?
Lu4 Lu6 Lu7 107.4(3) . . ?
Lu5 Lu6 Lu1 138.8(6) . . ?
Lu13 Lu6 Lu1 54.5(10) 6 . ?
Lu11 Lu6 Lu1 94.6(12) . . ?
Lu14 Lu6 Lu1 23.6(9) . . ?
Lu9 Lu6 Lu1 13.5(2) . . ?
Lu4 Lu6 Lu1 124.5(3) . . ?
Lu7 Lu6 Lu1 71.4(4) . . ?
Lu5 Lu6 Lu10 122.5(8) . . ?
Lu13 Lu6 Lu10 20.4(11) 6 . ?
Lu11 Lu6 Lu10 122.6(12) . . ?
Lu14 Lu6 Lu10 58.9(11) . . ?
Lu9 Lu6 Lu10 24.6(7) . . ?
Lu4 Lu6 Lu10 125.8(4) . . ?
Lu7 Lu6 Lu10 35.9(7) . . ?
Lu1 Lu6 Lu10 35.8(7) . . ?
Lu5 Lu6 C69 130.0(7) . . ?
Lu13 Lu6 C69 80.6(8) 6 . ?
Lu11 Lu6 C69 125.7(10) . . ?
Lu14 Lu6 C69 96.1(8) . . ?
Lu9 Lu6 C69 84.1(5) . . ?
Lu4 Lu6 C69 142.4(4) . . ?
Lu7 Lu6 C69 96.1(3) . . ?
Lu1 Lu6 C69 90.3(4) . . ?
Lu10 Lu6 C69 90.2(5) . . ?
Lu5 Lu6 C70 96.5(7) . . ?
Lu13 Lu6 C70 115.0(8) 6 . ?
Lu11 Lu6 C70 100.5(9) . . ?
Lu14 Lu6 C70 119.2(8) . . ?
Lu9 Lu6 C70 121.5(5) . . ?
Lu4 Lu6 C70 103.8(4) . . ?
Lu7 Lu6 C70 121.7(3) . . ?
Lu1 Lu6 C70 124.4(4) . . ?
Lu10 Lu6 C70 128.4(5) . . ?
C69 Lu6 C70 38.79(9) . . ?
Lu5 Lu6 Lu3 41.5(5) . . ?
Lu13 Lu6 Lu3 121.1(8) 6 . ?
Lu11 Lu6 Lu3 38.1(10) . . ?
Lu14 Lu6 Lu3 91.1(8) . . ?
Lu9 Lu6 Lu3 113.2(4) . . ?
Lu4 Lu6 Lu3 20.54(13) . . ?
Lu7 Lu6 Lu3 104.0(3) . . ?
Lu1 Lu6 Lu3 104.0(2) . . ?
Lu10 Lu6 Lu3 111.1(4) . . ?
C69 Lu6 Lu3 158.2(4) . . ?
C70 Lu6 Lu3 120.5(4) . . ?
Lu13 Lu7 Lu13 112(2) . 6 ?
Lu13 Lu7 Lu10 58.3(11) . . ?
Lu13 Lu7 Lu10 58.3(11) 6 . ?
Lu13 Lu7 Lu9 78.1(11) . . ?
Lu13 Lu7 Lu9 35.5(11) 6 . ?
Lu10 Lu7 Lu9 23.3(4) . . ?
Lu13 Lu7 Lu9 35.5(11) . 6 ?
Lu13 Lu7 Lu9 78.1(11) 6 6 ?
Lu10 Lu7 Lu9 23.3(4) . 6 ?
Lu9 Lu7 Lu9 42.9(7) . 6 ?
Lu13 Lu7 Lu6 22.4(10) . 6 ?
Lu13 Lu7 Lu6 121.0(9) 6 6 ?
Lu10 Lu7 Lu6 76.5(4) . 6 ?
Lu9 Lu7 Lu6 92.0(4) . 6 ?
Lu9 Lu7 Lu6 53.2(4) 6 6 ?
Lu13 Lu7 Lu6 121.0(9) . . ?
Lu13 Lu7 Lu6 22.4(10) 6 . ?
Lu10 Lu7 Lu6 76.5(4) . . ?
Lu9 Lu7 Lu6 53.2(4) . . ?
Lu9 Lu7 Lu6 92.0(4) 6 . ?
Lu6 Lu7 Lu6 120.2(4) 6 . ?
Lu13 Lu7 Lu5 43.4(11) . 6 ?
Lu13 Lu7 Lu5 125.2(7) 6 6 ?
Lu10 Lu7 Lu5 94.3(5) . 6 ?
Lu9 Lu7 Lu5 105.2(4) . 6 ?
Lu9 Lu7 Lu5 71.8(4) 6 6 ?
Lu6 Lu7 Lu5 21.0(2) 6 6 ?
Lu6 Lu7 Lu5 115.3(3) . 6 ?
Lu13 Lu7 Lu5 125.2(7) . . ?
Lu13 Lu7 Lu5 43.4(11) 6 . ?
Lu10 Lu7 Lu5 94.3(5) . . ?
Lu9 Lu7 Lu5 71.8(4) . . ?
Lu9 Lu7 Lu5 105.2(4) 6 . ?
Lu6 Lu7 Lu5 115.3(3) 6 . ?
Lu6 Lu7 Lu5 21.0(2) . . ?
Lu5 Lu7 Lu5 103.5(3) 6 . ?
Lu13 Lu7 C66 125.2(7) . . ?
Lu13 Lu7 C66 112.5(7) 6 . ?
Lu10 Lu7 C66 130.3(8) . . ?
Lu9 Lu7 C66 131.7(4) . . ?
Lu9 Lu7 C66 138.6(4) 6 . ?
Lu6 Lu7 C66 125.8(2) 6 . ?
Lu6 Lu7 C66 112.4(2) . . ?
Lu5 Lu7 C66 120.5(3) 6 . ?
Lu5 Lu7 C66 108.9(2) . . ?
Lu13 Lu7 C65 84.9(7) . . ?
Lu13 Lu7 C65 131.2(8) 6 . ?
Lu10 Lu7 C65 103.8(7) . . ?
Lu9 Lu7 C65 120.9(4) . . ?
Lu9 Lu7 C65 100.6(3) 6 . ?
Lu6 Lu7 C65 92.57(19) 6 . ?
Lu6 Lu7 C65 145.5(2) . . ?
Lu5 Lu7 C65 99.13(17) 6 . ?
Lu5 Lu7 C65 149.8(3) . . ?
C66 Lu7 C65 41.36(9) . . ?
Lu13 Lu7 C80 79.0(8) . . ?
Lu13 Lu7 C80 102.6(10) 6 . ?
Lu10 Lu7 C80 72.5(7) . . ?
Lu9 Lu7 C80 87.3(4) . . ?
Lu9 Lu7 C80 76.9(3) 6 . ?
Lu6 Lu7 C80 97.0(3) 6 . ?
Lu6 Lu7 C80 123.2(3) . . ?
Lu5 Lu7 C80 113.35(19) 6 . ?
Lu5 Lu7 C80 141.4(2) . . ?
C66 Lu7 C80 61.80(13) . . ?
C65 Lu7 C80 33.65(7) . . ?
Lu4 Lu8 Lu3 46.0(4) . . ?
Lu4 Lu8 Lu12 39.2(9) . . ?
Lu3 Lu8 Lu12 7.0(10) . . ?
Lu4 Lu8 Lu5 47.3(4) . . ?
Lu3 Lu8 Lu5 76.3(4) . . ?
Lu12 Lu8 Lu5 72.6(9) . . ?
Lu4 Lu8 Lu8 155.7(3) . 6 ?
Lu3 Lu8 Lu8 116.5(4) . 6 ?
Lu12 Lu8 Lu8 123.5(9) . 6 ?
Lu5 Lu8 Lu8 119.5(2) . 6 ?
Lu4 Lu8 Lu2 77.6(5) . . ?
Lu3 Lu8 Lu2 32.6(3) . . ?
Lu12 Lu8 Lu2 39.6(8) . . ?
Lu5 Lu8 Lu2 93.7(3) . . ?
Lu8 Lu8 Lu2 84.0(2) 6 . ?
Lu4 Lu8 Lu11 33.1(5) . . ?
Lu3 Lu8 Lu11 45.0(6) . . ?
Lu12 Lu8 Lu11 42.0(9) . . ?
Lu5 Lu8 Lu11 31.5(5) . . ?
Lu8 Lu8 Lu11 123.6(5) 6 . ?
Lu2 Lu8 Lu11 64.6(5) . . ?
Lu4 Lu8 C26 83.3(4) . . ?
Lu3 Lu8 C26 91.1(4) . . ?
Lu12 Lu8 C26 88.1(10) . . ?
Lu5 Lu8 C26 121.6(4) . . ?
Lu8 Lu8 C26 117.1(2) 6 . ?
Lu2 Lu8 C26 105.4(3) . . ?
Lu11 Lu8 C26 115.8(6) . . ?
Lu4 Lu8 C8 117.8(4) . . ?
Lu3 Lu8 C8 110.5(4) . . ?
Lu12 Lu8 C8 110.9(9) . . ?
Lu5 Lu8 C8 152.5(4) . . ?
Lu8 Lu8 C8 82.4(2) 6 . ?
Lu2 Lu8 C8 106.0(3) . . ?
Lu11 Lu8 C8 148.6(6) . . ?
C26 Lu8 C8 34.89(8) . . ?
Lu4 Lu8 C25 70.9(4) . . ?
Lu3 Lu8 C25 103.0(4) . . ?
Lu12 Lu8 C25 97.0(10) . . ?
Lu5 Lu8 C25 92.2(3) . . ?
Lu8 Lu8 C25 133.4(2) 6 . ?
Lu2 Lu8 C25 130.3(3) . . ?
Lu11 Lu8 C25 101.5(6) . . ?
C26 Lu8 C25 34.98(8) . . ?
C8 Lu8 C25 60.39(13) . . ?
Lu4 Lu8 Lu6 52.3(4) . . ?
Lu3 Lu8 Lu6 73.0(4) . . ?
Lu12 Lu8 Lu6 70.5(9) . . ?
Lu5 Lu8 Lu6 11.0(2) . . ?
Lu8 Lu8 Lu6 111.1(2) 6 . ?
Lu2 Lu8 Lu6 85.6(3) . . ?
Lu11 Lu8 Lu6 28.5(5) . . ?
C26 Lu8 Lu6 131.3(4) . . ?
C8 Lu8 Lu6 163.4(4) . . ?
C25 Lu8 Lu6 103.1(3) . . ?
Lu4 Lu8 Lu3 134.1(6) . 6 ?
Lu3 Lu8 Lu3 92.0(5) . 6 ?
Lu12 Lu8 Lu3 99.0(9) . 6 ?
Lu5 Lu8 Lu3 116.1(2) . 6 ?
Lu8 Lu8 Lu3 24.5(2) 6 6 ?
Lu2 Lu8 Lu3 59.48(19) . 6 ?
Lu11 Lu8 Lu3 106.9(5) . 6 ?
C26 Lu8 Lu3 121.2(3) . 6 ?
C8 Lu8 Lu3 90.8(3) . 6 ?
C25 Lu8 Lu3 150.6(4) . 6 ?
Lu6 Lu8 Lu3 105.4(2) . 6 ?
Lu1 Lu9 Lu10 126(2) . . ?
Lu1 Lu9 Lu14 54.3(19) . . ?
Lu10 Lu9 Lu14 145.4(17) . . ?
Lu1 Lu9 Lu13 149.1(19) . 6 ?
Lu10 Lu9 Lu13 66.3(15) . 6 ?
Lu14 Lu9 Lu13 99(2) . 6 ?
Lu1 Lu9 Lu9 87.4(15) . 6 ?
Lu10 Lu9 Lu9 38.7(14) . 6 ?
Lu14 Lu9 Lu9 126.0(14) . 6 ?
Lu13 Lu9 Lu9 100.8(11) 6 6 ?
Lu1 Lu9 Lu1 66.2(14) . 6 ?
Lu10 Lu9 Lu1 59.8(15) . 6 ?
Lu14 Lu9 Lu1 109.2(15) . 6 ?
Lu13 Lu9 Lu1 118.8(12) 6 6 ?
Lu9 Lu9 Lu1 21.2(2) 6 6 ?
Lu1 Lu9 Lu6 116.2(15) . . ?
Lu10 Lu9 Lu6 100.5(15) . . ?
Lu14 Lu9 Lu6 62.5(17) . . ?
Lu13 Lu9 Lu6 36.7(11) 6 . ?
Lu9 Lu9 Lu6 126.5(4) 6 . ?
Lu1 Lu9 Lu6 134.7(7) 6 . ?
Lu1 Lu9 Lu15 28.6(15) . . ?
Lu10 Lu9 Lu15 103.7(15) . . ?
Lu14 Lu9 Lu15 60.6(16) . . ?
Lu13 Lu9 Lu15 129.2(14) 6 . ?
Lu9 Lu9 Lu15 68.2(5) 6 . ?
Lu1 Lu9 Lu15 48.9(5) 6 . ?
Lu6 Lu9 Lu15 109.8(10) . . ?
Lu1 Lu9 Lu7 145.9(17) . . ?
Lu10 Lu9 Lu7 34.3(14) . . ?
Lu14 Lu9 Lu7 121.7(16) . . ?
Lu13 Lu9 Lu7 32.6(11) 6 . ?
Lu9 Lu9 Lu7 68.5(3) 6 . ?
Lu1 Lu9 Lu7 87.9(5) 6 . ?
Lu6 Lu9 Lu7 66.4(4) . . ?
Lu15 Lu9 Lu7 117.3(10) . . ?
Lu1 Lu9 Lu13 118.0(17) . . ?
Lu10 Lu9 Lu13 16.5(10) . . ?
Lu14 Lu9 Lu13 129.1(13) . . ?
Lu13 Lu9 Lu13 64.8(15) 6 . ?
Lu9 Lu9 Lu13 35.9(6) 6 . ?
Lu1 Lu9 Lu13 55.1(6) 6 . ?
Lu6 Lu9 Lu13 94.0(7) . . ?
Lu15 Lu9 Lu13 92.0(9) . . ?
Lu7 Lu9 Lu13 32.9(6) . . ?
Lu1 Lu9 C83 81.5(13) . . ?
Lu10 Lu9 C83 121.2(10) . . ?
Lu14 Lu9 C83 93.4(12) . . ?
Lu13 Lu9 C83 118.3(9) 6 . ?
Lu9 Lu9 C83 119.4(3) 6 . ?
Lu1 Lu9 C83 113.4(6) 6 . ?
Lu6 Lu9 C83 111.6(6) . . ?
Lu15 Lu9 C83 109.3(11) . . ?
Lu7 Lu9 C83 131.0(4) . . ?
Lu13 Lu9 C83 137.3(6) . . ?
Lu1 Lu9 Lu14 70.2(16) . 6 ?
Lu10 Lu9 Lu14 57.2(16) . 6 ?
Lu14 Lu9 Lu14 102.9(18) . 6 ?
Lu13 Lu9 Lu14 107.3(13) 6 6 ?
Lu9 Lu9 Lu14 23.1(6) 6 6 ?
Lu1 Lu9 Lu14 15.3(6) 6 6 ?
Lu6 Lu9 Lu14 119.5(8) . 6 ?
Lu15 Lu9 Lu14 46.7(8) . 6 ?
Lu7 Lu9 Lu14 79.3(9) . 6 ?
Lu13 Lu9 Lu14 47.9(10) . 6 ?
C83 Lu9 Lu14 128.4(8) . 6 ?
Lu9 Lu10 Lu9 103(3) . 6 ?
Lu9 Lu10 Lu13 69.2(11) . 6 ?
Lu9 Lu10 Lu13 150.9(17) 6 6 ?
Lu9 Lu10 Lu13 150.9(17) . . ?
Lu9 Lu10 Lu13 69.2(11) 6 . ?
Lu13 Lu10 Lu13 104(3) 6 . ?
Lu9 Lu10 Lu7 122.4(14) . . ?
Lu9 Lu10 Lu7 122.4(14) 6 . ?
Lu13 Lu10 Lu7 53.8(15) 6 . ?
Lu13 Lu10 Lu7 53.8(15) . . ?
Lu9 Lu10 Lu1 19.6(9) . . ?
Lu9 Lu10 Lu1 83(2) 6 . ?
Lu13 Lu10 Lu1 85.9(11) 6 . ?
Lu13 Lu10 Lu1 139.2(17) . . ?
Lu7 Lu10 Lu1 135.8(9) . . ?
Lu9 Lu10 Lu1 83(2) . 6 ?
Lu9 Lu10 Lu1 19.6(9) 6 6 ?
Lu13 Lu10 Lu1 139.2(17) 6 6 ?
Lu13 Lu10 Lu1 85.9(11) . 6 ?
Lu7 Lu10 Lu1 135.8(9) . 6 ?
Lu1 Lu10 Lu1 63.4(13) . 6 ?
Lu9 Lu10 Lu14 99(2) . 6 ?
Lu9 Lu10 Lu14 18.9(10) 6 6 ?
Lu13 Lu10 Lu14 132.3(13) 6 6 ?
Lu13 Lu10 Lu14 63.8(14) . 6 ?
Lu7 Lu10 Lu14 112.0(12) . 6 ?
Lu1 Lu10 Lu14 80.2(16) . 6 ?
Lu1 Lu10 Lu14 23.8(10) 6 6 ?
Lu9 Lu10 Lu14 18.9(10) . . ?
Lu9 Lu10 Lu14 99(2) 6 . ?
Lu13 Lu10 Lu14 63.8(14) 6 . ?
Lu13 Lu10 Lu14 132.3(13) . . ?
Lu7 Lu10 Lu14 112.0(12) . . ?
Lu1 Lu10 Lu14 23.8(10) . . ?
Lu1 Lu10 Lu14 80.2(16) 6 . ?
Lu14 Lu10 Lu14 90.1(19) 6 . ?
Lu9 Lu10 Lu6 135.4(15) . 6 ?
Lu9 Lu10 Lu6 54.9(9) 6 6 ?
Lu13 Lu10 Lu6 110.6(16) 6 6 ?
Lu13 Lu10 Lu6 18.6(10) . 6 ?
Lu7 Lu10 Lu6 67.7(6) . 6 ?
Lu1 Lu10 Lu6 121.0(11) . 6 ?
Lu1 Lu10 Lu6 69.3(4) 6 6 ?
Lu14 Lu10 Lu6 46.2(10) 6 6 ?
Lu14 Lu10 Lu6 118.4(9) . 6 ?
Lu9 Lu10 Lu6 54.9(9) . . ?
Lu9 Lu10 Lu6 135.4(15) 6 . ?
Lu13 Lu10 Lu6 18.6(10) 6 . ?
Lu13 Lu10 Lu6 110.6(16) . . ?
Lu7 Lu10 Lu6 67.7(6) . . ?
Lu1 Lu10 Lu6 69.3(4) . . ?
Lu1 Lu10 Lu6 121.0(11) 6 . ?
Lu14 Lu10 Lu6 118.4(9) 6 . ?
Lu14 Lu10 Lu6 46.2(10) . . ?
Lu6 Lu10 Lu6 111.2(8) 6 . ?
Lu9 Lu10 C81 89.9(9) . . ?
Lu9 Lu10 C81 123.2(13) 6 . ?
Lu13 Lu10 C81 85.3(10) 6 . ?
Lu13 Lu10 C81 118.3(16) . . ?
Lu7 Lu10 C81 93.0(12) . . ?
Lu1 Lu10 C81 101.8(7) . . ?
Lu1 Lu10 C81 125.1(12) 6 . ?
Lu14 Lu10 C81 142.1(11) 6 . ?
Lu14 Lu10 C81 106.9(7) . . ?
Lu6 Lu10 C81 134.6(9) 6 . ?
Lu6 Lu10 C81 96.9(5) . . ?
Lu6 Lu11 Lu5 39.7(7) . . ?
Lu6 Lu11 Lu4 97.3(15) . . ?
Lu5 Lu11 Lu4 57.8(11) . . ?
Lu6 Lu11 Lu12 137.1(19) . . ?
Lu5 Lu11 Lu12 100.9(19) . . ?
Lu4 Lu11 Lu12 45.1(13) . . ?
Lu6 Lu11 Lu3 115.6(14) . . ?
Lu5 Lu11 Lu3 81.5(13) . . ?
Lu4 Lu11 Lu3 32.2(5) . . ?
Lu12 Lu11 Lu3 21.6(8) . . ?
Lu6 Lu11 Lu14 65.5(13) . . ?
Lu5 Lu11 Lu14 100.5(14) . . ?
Lu4 Lu11 Lu14 141.0(12) . . ?
Lu12 Lu11 Lu14 126.8(17) . . ?
Lu3 Lu11 Lu14 122.3(12) . . ?
Lu6 Lu11 Lu13 18.3(7) . 6 ?
Lu5 Lu11 Lu13 48.0(9) . 6 ?
Lu4 Lu11 Lu13 100.7(11) . 6 ?
Lu12 Lu11 Lu13 130.3(13) . 6 ?
Lu3 Lu11 Lu13 109.5(9) . 6 ?
Lu14 Lu11 Lu13 52.6(11) . 6 ?
Lu6 Lu11 Lu8 86.2(11) . . ?
Lu5 Lu11 Lu8 51.5(9) . . ?
Lu4 Lu11 Lu8 23.2(3) . . ?
Lu12 Lu11 Lu8 51.0(11) . . ?
Lu3 Lu11 Lu8 30.2(4) . . ?
Lu14 Lu11 Lu8 117.8(10) . . ?
Lu13 Lu11 Lu8 83.8(8) 6 . ?
Lu6 Lu11 C51 118.2(11) . . ?
Lu5 Lu11 C51 110.8(12) . . ?
Lu4 Lu11 C51 90.9(9) . . ?
Lu12 Lu11 C51 87.4(12) . . ?
Lu3 Lu11 C51 103.1(10) . . ?
Lu14 Lu11 C51 128.0(13) . . ?
Lu13 Lu11 C51 135.4(10) 6 . ?
Lu8 Lu11 C51 114.1(10) . . ?
Lu6 Lu11 C71 85.4(10) . . ?
Lu5 Lu11 C71 98.3(10) . . ?
Lu4 Lu11 C71 115.1(11) . . ?
Lu12 Lu11 C71 125.2(13) . . ?
Lu3 Lu11 C71 138.4(11) . . ?
Lu14 Lu11 C71 98.9(12) . . ?
Lu13 Lu11 C71 100.1(9) 6 . ?
Lu8 Lu11 C71 134.4(10) . . ?
C51 Lu11 C71 37.8(2) . . ?
Lu6 Lu11 Lu2 123.6(10) . . ?
Lu5 Lu11 Lu2 105.6(11) . . ?
Lu4 Lu11 Lu2 66.8(7) . . ?
Lu12 Lu11 Lu2 34.2(11) . . ?
Lu3 Lu11 Lu2 34.8(4) . . ?
Lu14 Lu11 Lu2 93.0(10) . . ?
Lu13 Lu11 Lu2 108.1(7) 6 . ?
Lu8 Lu11 Lu2 57.6(5) . . ?
C51 Lu11 Lu2 115.9(8) . . ?
C71 Lu11 Lu2 150.9(8) . . ?
Lu6 Lu11 Lu9 44.5(9) . . ?
Lu5 Lu11 Lu9 77.8(10) . . ?
Lu4 Lu11 Lu9 124.2(9) . . ?
Lu12 Lu11 Lu9 131.9(13) . . ?
Lu3 Lu11 Lu9 118.1(8) . . ?
Lu14 Lu11 Lu9 22.7(9) . . ?
Lu13 Lu11 Lu9 30.0(6) 6 . ?
Lu8 Lu11 Lu9 102.6(6) . . ?
C51 Lu11 Lu9 138.8(10) . . ?
C71 Lu11 Lu9 102.2(9) . . ?
Lu2 Lu11 Lu9 98.9(6) . . ?
Lu3 Lu12 Lu4 49(2) . . ?
Lu3 Lu12 Lu2 76(2) . . ?
Lu4 Lu12 Lu2 123.0(17) . . ?
Lu3 Lu12 Lu11 92(3) . . ?
Lu4 Lu12 Lu11 66.0(15) . . ?
Lu2 Lu12 Lu11 109.5(19) . . ?
Lu3 Lu12 Lu8 14(2) . . ?
Lu4 Lu12 Lu8 36.0(7) . . ?
Lu2 Lu12 Lu8 89.2(10) . . ?
Lu11 Lu12 Lu8 87.0(15) . . ?
Lu3 Lu12 Lu5 62(2) . . ?
Lu4 Lu12 Lu5 34.3(8) . . ?
Lu2 Lu12 Lu5 112.6(14) . . ?
Lu11 Lu12 Lu5 33.9(10) . . ?
Lu8 Lu12 Lu5 54.2(8) . . ?
Lu3 Lu12 C28 118(3) . . ?
Lu4 Lu12 C28 95.9(17) . . ?
Lu2 Lu12 C28 125.1(15) . . ?
Lu11 Lu12 C28 122.0(14) . . ?
Lu8 Lu12 C28 110.1(15) . . ?
Lu5 Lu12 C28 120.5(13) . . ?
Lu3 Lu12 C27 86(3) . . ?
Lu4 Lu12 C27 85.4(16) . . ?
Lu2 Lu12 C27 106.5(12) . . ?
Lu11 Lu12 C27 142.4(19) . . ?
Lu8 Lu12 C27 82.8(11) . . ?
Lu5 Lu12 C27 119.3(14) . . ?
C28 Lu12 C27 34.1(4) . . ?
Lu3 Lu12 C29 154(3) . . ?
Lu4 Lu12 C29 127.6(18) . . ?
Lu2 Lu12 C29 107.9(14) . . ?
Lu11 Lu12 C29 110.0(12) . . ?
Lu8 Lu12 C29 149.1(17) . . ?
Lu5 Lu12 C29 133.2(11) . . ?
C28 Lu12 C29 39.0(4) . . ?
C27 Lu12 C29 68.0(7) . . ?
Lu3 Lu12 C50 110(3) . . ?
Lu4 Lu12 C50 65.2(12) . . ?
Lu2 Lu12 C50 167.8(16) . . ?
Lu11 Lu12 C50 81.7(12) . . ?
Lu8 Lu12 C50 96.3(13) . . ?
Lu5 Lu12 C50 79.3(9) . . ?
C28 Lu12 C50 42.8(5) . . ?
C27 Lu12 C50 63.7(7) . . ?
C29 Lu12 C50 62.6(6) . . ?
Lu3 Lu12 Lu6 73(2) . . ?
Lu4 Lu12 Lu6 51.5(10) . . ?
Lu2 Lu12 Lu6 105.9(13) . . ?
Lu11 Lu12 Lu6 18.7(8) . . ?
Lu8 Lu12 Lu6 68.3(9) . . ?
Lu5 Lu12 Lu6 17.3(3) . . ?
C28 Lu12 Lu6 129.0(12) . . ?
C27 Lu12 Lu6 135.7(13) . . ?
C29 Lu12 Lu6 127.3(9) . . ?
C50 Lu12 Lu6 86.2(8) . . ?
Lu3 Lu12 C52 166(3) . . ?
Lu4 Lu12 C52 116.7(14) . . ?
Lu2 Lu12 C52 117.2(15) . . ?
Lu11 Lu12 C52 77.9(10) . . ?
Lu8 Lu12 C52 152.7(15) . . ?
Lu5 Lu12 C52 105.3(9) . . ?
C28 Lu12 C52 61.8(5) . . ?
C27 Lu12 C52 95.4(9) . . ?
C29 Lu12 C52 32.3(3) . . ?
C50 Lu12 C52 59.4(5) . . ?
Lu6 Lu12 C52 95.9(7) . . ?
Lu6 Lu13 Lu7 134.4(19) 6 . ?
Lu6 Lu13 Lu10 141(2) 6 . ?
Lu7 Lu13 Lu10 68(2) . . ?
Lu6 Lu13 Lu9 101.6(16) 6 6 ?
Lu7 Lu13 Lu9 111.9(19) . 6 ?
Lu10 Lu13 Lu9 44.5(13) . 6 ?
Lu6 Lu13 Lu5 26.4(7) 6 6 ?
Lu7 Lu13 Lu5 108.0(14) . 6 ?
Lu10 Lu13 Lu5 143.6(12) . 6 ?
Lu9 Lu13 Lu5 120.4(13) 6 6 ?
Lu6 Lu13 Lu1 94.0(13) 6 6 ?
Lu7 Lu13 Lu1 115.2(16) . 6 ?
Lu10 Lu13 Lu1 49.9(13) . 6 ?
Lu9 Lu13 Lu1 9.4(5) 6 6 ?
Lu5 Lu13 Lu1 111.3(10) 6 6 ?
Lu6 Lu13 Lu14 64.2(14) 6 6 ?
Lu7 Lu13 Lu14 136.2(16) . 6 ?
Lu10 Lu13 Lu14 78.5(17) . 6 ?
Lu9 Lu13 Lu14 38.0(12) 6 6 ?
Lu5 Lu13 Lu14 82.9(13) 6 6 ?
Lu1 Lu13 Lu14 29.8(10) 6 6 ?
Lu6 Lu13 Lu13 140.1(8) 6 6 ?
Lu7 Lu13 Lu13 33.9(10) . 6 ?
Lu10 Lu13 Lu13 38.0(14) . 6 ?
Lu9 Lu13 Lu13 79.2(11) 6 6 ?
Lu5 Lu13 Lu13 120.5(6) 6 6 ?
Lu1 Lu13 Lu13 81.5(7) 6 6 ?
Lu14 Lu13 Lu13 103.7(12) 6 6 ?
Lu6 Lu13 Lu9 131.0(11) 6 . ?
Lu7 Lu13 Lu9 69.1(11) . . ?
Lu10 Lu13 Lu9 12.6(8) . . ?
Lu9 Lu13 Lu9 43.3(10) 6 . ?
Lu5 Lu13 Lu9 131.0(7) 6 . ?
Lu1 Lu13 Lu9 46.2(6) 6 . ?
Lu14 Lu13 Lu9 72.2(13) 6 . ?
Lu13 Lu13 Lu9 35.9(6) 6 . ?
Lu6 Lu13 Lu11 19.8(7) 6 6 ?
Lu7 Lu13 Lu11 131.3(13) . 6 ?
Lu10 Lu13 Lu11 122.2(16) . 6 ?
Lu9 Lu13 Lu11 87.9(12) 6 6 ?
Lu5 Lu13 Lu11 32.9(8) 6 6 ?
Lu1 Lu13 Lu11 79.2(9) 6 6 ?
Lu14 Lu13 Lu11 50.1(12) 6 6 ?
Lu13 Lu13 Lu11 123.7(6) 6 6 ?
Lu9 Lu13 Lu11 111.5(8) . 6 ?
Lu6 Lu13 Lu1 120.1(11) 6 . ?
Lu7 Lu13 Lu1 79.8(11) . . ?
Lu10 Lu13 Lu1 21.4(11) . . ?
Lu9 Lu13 Lu1 34.2(8) 6 . ?
Lu5 Lu13 Lu1 124.2(7) 6 . ?
Lu1 Lu13 Lu1 35.5(5) 6 . ?
Lu14 Lu13 Lu1 60.5(12) 6 . ?
Lu13 Lu13 Lu1 46.0(5) 6 . ?
Lu9 Lu13 Lu1 11.8(3) . . ?
Lu11 Lu13 Lu1 100.9(8) 6 . ?
Lu6 Lu13 C64 82.7(10) 6 . ?
Lu7 Lu13 C64 97.7(9) . . ?
Lu10 Lu13 C64 131.4(14) . . ?
Lu9 Lu13 C64 129.6(11) 6 . ?
Lu5 Lu13 C64 84.7(9) 6 . ?
Lu1 Lu13 C64 134.7(9) 6 . ?
Lu14 Lu13 C64 125.8(13) 6 . ?
Lu13 Lu13 C64 127.7(5) 6 . ?
Lu9 Lu13 C64 143.9(9) . . ?
Lu11 Lu13 C64 102.5(10) 6 . ?
Lu1 Lu13 C64 150.5(9) . . ?
Lu1 Lu14 Lu9 29.7(9) . . ?
Lu1 Lu14 Lu6 110(2) . . ?
Lu9 Lu14 Lu6 80.7(16) . . ?
Lu1 Lu14 Lu15 61(2) . . ?
Lu9 Lu14 Lu15 85(2) . . ?
Lu6 Lu14 Lu15 134.9(18) . . ?
Lu1 Lu14 Lu11 147(2) . . ?
Lu9 Lu14 Lu11 121(2) . . ?
Lu6 Lu14 Lu11 41.9(10) . . ?
Lu15 Lu14 Lu11 121.6(18) . . ?
Lu1 Lu14 Lu13 72.3(17) . 6 ?
Lu9 Lu14 Lu13 43.4(12) . 6 ?
Lu6 Lu14 Lu13 37.7(9) . 6 ?
Lu15 Lu14 Lu13 112.4(18) . 6 ?
Lu11 Lu14 Lu13 77.4(16) . 6 ?
Lu1 Lu14 Lu10 36.4(13) . . ?
Lu9 Lu14 Lu10 15.7(8) . . ?
Lu6 Lu14 Lu10 74.9(12) . . ?
Lu15 Lu14 Lu10 79.9(17) . . ?
Lu11 Lu14 Lu10 110.6(17) . . ?
Lu13 Lu14 Lu10 37.7(10) 6 . ?
Lu1 Lu14 Lu1 25.4(9) . 6 ?
Lu9 Lu14 Lu1 41.9(11) . 6 ?
Lu6 Lu14 Lu1 108.3(12) . 6 ?
Lu15 Lu14 Lu1 43.4(13) . 6 ?
Lu11 Lu14 Lu1 130.5(13) . 6 ?
Lu13 Lu14 Lu1 73.7(12) 6 6 ?
Lu10 Lu14 Lu1 37.3(8) . 6 ?
Lu1 Lu14 Lu5 116(2) . . ?
Lu9 Lu14 Lu5 89.1(16) . . ?
Lu6 Lu14 Lu5 15.5(4) . . ?
Lu15 Lu14 Lu5 123.9(16) . . ?
Lu11 Lu14 Lu5 31.5(8) . . ?
Lu13 Lu14 Lu5 46.0(10) 6 . ?
Lu10 Lu14 Lu5 80.0(12) . . ?
Lu1 Lu14 Lu5 107.7(10) 6 . ?
Lu1 Lu14 Lu9 26.3(10) . 6 ?
Lu9 Lu14 Lu9 30.9(10) . 6 ?
Lu6 Lu14 Lu9 95.1(11) . 6 ?
Lu15 Lu14 Lu9 56.3(13) . 6 ?
Lu11 Lu14 Lu9 122.7(13) . 6 ?
Lu13 Lu14 Lu9 59.9(11) 6 6 ?
Lu10 Lu14 Lu9 23.7(7) . 6 ?
Lu1 Lu14 Lu9 13.9(2) 6 6 ?
Lu5 Lu14 Lu9 96.2(9) . 6 ?
Lu1 Lu14 C84 91.8(13) . . ?
Lu9 Lu14 C84 82.1(12) . . ?
Lu6 Lu14 C84 80.5(10) . . ?
Lu15 Lu14 C84 139(2) . . ?
Lu11 Lu14 C84 98.1(14) . . ?
Lu13 Lu14 C84 83.1(10) 6 . ?
Lu10 Lu14 C84 95.5(9) . . ?
Lu1 Lu14 C84 116.9(10) 6 . ?
Lu5 Lu14 C84 94.5(10) . . ?
Lu9 Lu14 C84 111.3(10) 6 . ?
Lu1 Lu14 C72 125.4(15) . . ?
Lu9 Lu14 C72 117.3(14) . . ?
Lu6 Lu14 C72 81.3(12) . . ?
Lu15 Lu14 C72 142.1(17) . . ?
Lu11 Lu14 C72 75.2(12) . . ?
Lu13 Lu14 C72 104.2(14) 6 . ?
Lu10 Lu14 C72 129.1(11) . . ?
Lu1 Lu14 C72 150.7(11) 6 . ?
Lu5 Lu14 C72 88.8(11) . . ?
Lu9 Lu14 C72 147.1(10) 6 . ?
C84 Lu14 C72 35.7(3) . . ?
Lu1 Lu15 Lu1 55.9(13) 6 . ?
Lu1 Lu15 Lu14 32.0(9) 6 6 ?
Lu1 Lu15 Lu14 84.8(19) . 6 ?
Lu1 Lu15 Lu14 84.8(19) 6 . ?
Lu1 Lu15 Lu14 32.0(9) . . ?
Lu14 Lu15 Lu14 108(3) 6 . ?
Lu1 Lu15 Lu9 50.5(11) 6 . ?
Lu1 Lu15 Lu9 10.2(5) . . ?
Lu14 Lu15 Lu9 77.0(17) 6 . ?
Lu14 Lu15 Lu9 34.5(11) . . ?
Lu1 Lu15 Lu9 10.2(5) 6 6 ?
Lu1 Lu15 Lu9 50.5(11) . 6 ?
Lu14 Lu15 Lu9 34.5(11) 6 6 ?
Lu14 Lu15 Lu9 77.0(17) . 6 ?
Lu9 Lu15 Lu9 43.6(10) . 6 ?
Lu1 Lu15 Lu10 31.4(8) 6 . ?
Lu1 Lu15 Lu10 31.4(8) . . ?
Lu14 Lu15 Lu10 54.5(13) 6 . ?
Lu14 Lu15 Lu10 54.5(13) . . ?
Lu9 Lu15 Lu10 22.6(5) . . ?
Lu9 Lu15 Lu10 22.6(5) 6 . ?
Lu1 Lu15 C57 113.7(19) 6 . ?
Lu1 Lu15 C57 108.1(17) . . ?
Lu14 Lu15 C57 121.8(16) 6 . ?
Lu14 Lu15 C57 111.8(15) . . ?
Lu9 Lu15 C57 117.7(15) . . ?
Lu9 Lu15 C57 122.5(16) 6 . ?
Lu10 Lu15 C57 128.6(16) . . ?
Lu1 Lu15 C76 79.3(15) 6 . ?
Lu1 Lu15 C76 77.0(14) . . ?
Lu14 Lu15 C76 99.3(16) 6 . ?
Lu14 Lu15 C76 95.4(15) . . ?
Lu9 Lu15 C76 85.0(12) . . ?
Lu9 Lu15 C76 86.8(12) 6 . ?
Lu10 Lu15 C76 91.5(12) . . ?
C57 Lu15 C76 37.3(6) . . ?
Lu1 Lu15 C56 130.8(19) 6 . ?
Lu1 Lu15 C56 93.3(10) . . ?
Lu14 Lu15 C56 154(2) 6 . ?
Lu14 Lu15 C56 82.6(10) . . ?
Lu9 Lu15 C56 103.2(8) . . ?
Lu9 Lu15 C56 134.4(16) 6 . ?
Lu10 Lu15 C56 123.9(11) . . ?
C57 Lu15 C56 34.5(5) . . ?
C76 Lu15 C56 54.9(7) . . ?
Lu1 Lu15 C58 109.3(13) 6 . ?
Lu1 Lu15 C58 138(2) . . ?
Lu14 Lu15 C58 98.3(11) 6 . ?
Lu14 Lu15 C58 147.6(18) . . ?
Lu9 Lu15 C58 144.4(17) . . ?
Lu9 Lu15 C58 119.4(10) 6 . ?
Lu10 Lu15 C58 139.2(12) . . ?
C57 Lu15 C58 36.0(5) . . ?
C76 Lu15 C58 60.6(8) . . ?
C56 Lu15 C58 65.9(9) . . ?
Lu1 Lu15 Lu13 55.2(12) 6 6 ?
Lu1 Lu15 Lu13 28.3(10) . 6 ?
Lu14 Lu15 Lu13 73.1(16) 6 6 ?
Lu14 Lu15 Lu13 34.6(12) . 6 ?
Lu9 Lu15 Lu13 19.3(7) . 6 ?
Lu9 Lu15 Lu13 45.7(9) 6 6 ?
Lu10 Lu15 Lu13 24.0(6) . 6 ?
C57 Lu15 Lu13 136.2(12) . 6 ?
C76 Lu15 Lu13 104.3(11) . 6 ?
C56 Lu15 Lu13 115.3(7) . 6 ?
C58 Lu15 Lu13 161.9(14) . 6 ?
C9 C1 C10 134.1 . . ?
C9 C1 C2 110.4 . . ?
C10 C1 C2 111.5 . . ?
C9 C1 Lu2 107.02(6) . . ?
C10 C1 Lu2 67.87(8) . . ?
C2 C1 Lu2 74.53(8) . . ?
C9 C1 Lu3 91.75(8) . . ?
C10 C1 Lu3 61.86(8) . . ?
C2 C1 Lu3 102.20(9) . . ?
Lu2 C1 Lu3 28.36(9) . . ?
C9 C1 Lu8 69.74(16) . . ?
C10 C1 Lu8 79.31(16) . . ?
C2 C1 Lu8 109.59(10) . . ?
Lu2 C1 Lu8 44.48(13) . . ?
Lu3 C1 Lu8 22.01(16) . . ?
C9 C1 Lu12 102.1(5) . . ?
C10 C1 Lu12 52.0(4) . . ?
C2 C1 Lu12 101.2(5) . . ?
Lu2 C1 Lu12 27.1(5) . . ?
Lu3 C1 Lu12 10.8(4) . . ?
Lu8 C1 Lu12 32.4(4) . . ?
C12 C2 C1 103.2 . . ?
C12 C2 C3 126.8 . . ?
C1 C2 C3 123.3 . . ?
C12 C2 Lu2 64.69(6) . . ?
C1 C2 Lu2 73.31(7) . . ?
C3 C2 Lu2 103.00(7) . . ?
C15 C3 C4 135.3 . . ?
C15 C3 C2 98.4 . . ?
C4 C3 C2 118.3 . . ?
C18 C4 C3 131.2 . . ?
C18 C4 C5 111.4 . . ?
C3 C4 C5 107.1 . . ?
C6 C5 C9 98.8 . . ?
C6 C5 C4 120.0 . . ?
C9 C5 C4 138.0 . . ?
C20 C6 C5 118.9 . . ?
C20 C6 C7 121.7 . . ?
C5 C6 C7 114.2 . . ?
C20 C6 C9 155.7 . . ?
C5 C6 C9 40.7 . . ?
C7 C6 C9 73.8 . . ?
C6 C7 C8 108.5 . . ?
C6 C7 C23 136.3 . . ?
C8 C7 C23 106.5 . . ?
C6 C7 Lu8 100.83(14) . . ?
C8 C7 Lu8 57.50(14) . . ?
C23 C7 Lu8 77.03(15) . . ?
C26 C8 C7 133.2 . . ?
C26 C8 C9 125.8 . . ?
C7 C8 C9 98.5 . . ?
C26 C8 Lu8 70.46(19) . . ?
C7 C8 Lu8 92.1(2) . . ?
C9 C8 Lu8 96.98(17) . . ?
C26 C8 Lu3 61.07(9) . . ?
C7 C8 Lu3 112.71(7) . . ?
C9 C8 Lu3 87.88(9) . . ?
Lu8 C8 Lu3 21.46(19) . . ?
C26 C8 Lu4 52.65(9) . . ?
C7 C8 Lu4 106.89(12) . . ?
C9 C8 Lu4 104.44(10) . . ?
Lu8 C8 Lu4 18.13(18) . . ?
Lu3 C8 Lu4 16.77(9) . . ?
C1 C9 C5 122.4 . . ?
C1 C9 C8 109.9 . . ?
C5 C9 C8 118.3 . . ?
C1 C9 C6 155.3 . . ?
C5 C9 C6 40.5 . . ?
C8 C9 C6 78.7 . . ?
C1 C9 Lu8 84.54(17) . . ?
C5 C9 Lu8 99.67(14) . . ?
C8 C9 Lu8 53.47(12) . . ?
C6 C9 Lu8 82.63(17) . . ?
C1 C10 C27 110.9 . . ?
C1 C10 C11 104.7 . . ?
C27 C10 C11 133.9 . . ?
C1 C10 C28 142.1 . . ?
C27 C10 C28 34.6 . . ?
C11 C10 C28 100.9 . . ?
C1 C10 Lu12 102.5(5) . . ?
C27 C10 Lu12 59.8(7) . . ?
C11 C10 Lu12 85.1(7) . . ?
C28 C10 Lu12 52.5(5) . . ?
C1 C10 Lu2 81.93(8) . . ?
C27 C10 Lu2 90.69(8) . . ?
C11 C10 Lu2 66.10(7) . . ?
C28 C10 Lu2 83.56(9) . . ?
Lu12 C10 Lu2 32.6(6) . . ?
C1 C10 Lu3 90.04(10) . . ?
C27 C10 Lu3 59.34(10) . . ?
C11 C10 Lu3 93.18(10) . . ?
C28 C10 Lu3 60.93(10) . . ?
Lu12 C10 Lu3 13.4(5) . . ?
Lu2 C10 Lu3 31.66(10) . . ?
C1 C10 Lu4 94.50(9) . . ?
C27 C10 Lu4 45.74(7) . . ?
C11 C10 Lu4 104.44(8) . . ?
C28 C10 Lu4 51.87(9) . . ?
Lu12 C10 Lu4 19.6(6) . . ?
Lu2 C10 Lu4 45.30(9) . . ?
Lu3 C10 Lu4 13.66(9) . . ?
C12 C11 C10 111.8 . . ?
C12 C11 C30 124.6 . . ?
C10 C11 C30 115.6 . . ?
C12 C11 Lu2 78.13(9) . . ?
C10 C11 Lu2 80.52(8) . . ?
C30 C11 Lu2 82.88(9) . . ?
C12 C11 Lu12 108.4(5) . . ?
C10 C11 Lu12 64.4(6) . . ?
C30 C11 Lu12 70.2(4) . . ?
Lu2 C11 Lu12 30.7(5) . . ?
C12 C11 Lu3 101.02(9) . . ?
C10 C11 Lu3 58.83(8) . . ?
C30 C11 Lu3 80.98(8) . . ?
Lu2 C11 Lu3 26.76(9) . . ?
Lu12 C11 Lu3 11.0(4) . . ?
C11 C12 C2 108.8 . . ?
C11 C12 C13 124.4 . . ?
C2 C12 C13 119.2 . . ?
C11 C12 Lu2 68.20(8) . . ?
C2 C12 Lu2 84.30(8) . . ?
C13 C12 Lu2 89.61(8) . . ?
C14 C13 C12 121.7 . . ?
C14 C13 C32 120.5 . . ?
C12 C13 C32 112.5 . . ?
C14 C13 Lu2 103.32(7) . . ?
C12 C13 Lu2 59.49(6) . . ?
C32 C13 Lu2 83.42(7) . . ?
C13 C14 C35 123.8 . . ?
C13 C14 C15 111.4 . . ?
C35 C14 C15 112.6 . . ?
C3 C15 C14 142.4 . . ?
C3 C15 C16 105.9 . . ?
C14 C15 C16 107.2 . . ?
C36 C16 C15 104.6 . . ?
C36 C16 C17 119.6 . . ?
C15 C16 C17 125.6 . . ?
C39 C17 C18 123.8 . . ?
C39 C17 C16 111.9 . . ?
C18 C17 C16 110.1 . . ?
C19 C18 C4 127.7 . . ?
C19 C18 C17 108.4 . . ?
C4 C18 C17 111.2 . . ?
C20 C19 C18 112.8 . . ?
C20 C19 C41 109.2 . . ?
C18 C19 C41 132.5 . . ?
C19 C20 C6 123.9 . . ?
C19 C20 C21 103.4 . . ?
C6 C20 C21 112.0 . . ?
C42 C21 C20 112.6 . . ?
C42 C21 C22 114.1 . . ?
C20 C21 C22 123.4 . . ?
C23 C22 C45 101.7 . . ?
C23 C22 C21 120.7 . . ?
C45 C22 C21 128.2 . . ?
C24 C23 C7 129.2 . . ?
C24 C23 C22 116.9 . . ?
C7 C23 C22 105.0 . . ?
C24 C23 Lu8 70.27(16) . . ?
C7 C23 Lu8 73.35(16) . . ?
C22 C23 Lu8 103.49(13) . . ?
C23 C24 C46 104.5 . . ?
C23 C24 C25 123.0 . . ?
C46 C24 C25 122.7 . . ?
C23 C24 Lu8 85.03(19) . . ?
C46 C24 Lu8 96.70(14) . . ?
C25 C24 Lu8 61.15(16) . . ?
C23 C24 Lu4 104.95(10) . . ?
C46 C24 Lu4 94.01(11) . . ?
C25 C24 Lu4 46.98(9) . . ?
Lu8 C24 Lu4 20.09(17) . . ?
C26 C25 C49 126.6 . . ?
C26 C25 C24 111.4 . . ?
C49 C25 C24 115.7 . . ?
C26 C25 Lu4 78.77(15) . . ?
C49 C25 Lu4 68.79(13) . . ?
C24 C25 Lu4 101.31(15) . . ?
C26 C25 Lu8 69.77(17) . . ?
C49 C25 Lu8 93.0(2) . . ?
C24 C25 Lu8 82.0(2) . . ?
Lu4 C25 Lu8 26.1(2) . . ?
C26 C25 Lu3 64.72(8) . . ?
C49 C25 Lu3 79.84(9) . . ?
C24 C25 Lu3 104.94(8) . . ?
Lu4 C25 Lu3 14.09(13) . . ?
Lu8 C25 Lu3 23.2(2) . . ?
C26 C25 Lu5 100.93(9) . . ?
C49 C25 Lu5 59.93(10) . . ?
C24 C25 Lu5 86.04(10) . . ?
Lu4 C25 Lu5 23.49(17) . . ?
Lu8 C25 Lu5 35.69(19) . . ?
Lu3 C25 Lu5 36.84(10) . . ?
C26 C25 Lu12 65.9(4) . . ?
C49 C25 Lu12 72.5(4) . . ?
C24 C25 Lu12 114.8(4) . . ?
Lu4 C25 Lu12 16.4(5) . . ?
Lu8 C25 Lu12 33.6(4) . . ?
Lu3 C25 Lu12 10.6(4) . . ?
Lu5 C25 Lu12 39.5(5) . . ?
C8 C26 C25 116.0 . . ?
C8 C26 C27 113.8 . . ?
C25 C26 C27 117.8 . . ?
C8 C26 Lu8 74.6(2) . . ?
C25 C26 Lu8 75.25(19) . . ?
C27 C26 Lu8 84.6(2) . . ?
C8 C26 Lu4 100.00(12) . . ?
C25 C26 Lu4 66.42(14) . . ?
C27 C26 Lu4 70.51(15) . . ?
Lu8 C26 Lu4 25.6(2) . . ?
C8 C26 Lu3 90.82(10) . . ?
C25 C26 Lu3 85.96(10) . . ?
C27 C26 Lu3 58.50(8) . . ?
Lu8 C26 Lu3 26.5(2) . . ?
Lu4 C26 Lu3 19.55(11) . . ?
C8 C26 Lu12 100.7(4) . . ?
C25 C26 Lu12 87.2(5) . . ?
C27 C26 Lu12 48.7(5) . . ?
Lu8 C26 Lu12 37.6(5) . . ?
Lu4 C26 Lu12 23.2(5) . . ?
Lu3 C26 Lu12 11.6(4) . . ?
C28 C27 C10 105.7 . . ?
C28 C27 C26 128.2 . . ?
C10 C27 C26 124.7 . . ?
C28 C27 Lu12 68.7(5) . . ?
C10 C27 Lu12 86.3(7) . . ?
C26 C27 Lu12 101.2(7) . . ?
C28 C27 Lu3 83.18(11) . . ?
C10 C27 Lu3 87.63(12) . . ?
C26 C27 Lu3 87.67(11) . . ?
Lu12 C27 Lu3 15.6(5) . . ?
C28 C27 Lu4 79.35(12) . . ?
C10 C27 Lu4 109.12(12) . . ?
C26 C27 Lu4 74.31(12) . . ?
Lu12 C27 Lu4 28.5(7) . . ?
Lu3 C27 Lu4 21.55(10) . . ?
C28 C27 Lu8 102.90(19) . . ?
C10 C27 Lu8 98.74(16) . . ?
C26 C27 Lu8 61.77(16) . . ?
Lu12 C27 Lu8 41.3(6) . . ?
Lu3 C27 Lu8 26.30(18) . . ?
Lu4 C27 Lu8 23.88(17) . . ?
C28 C27 Lu2 87.35(7) . . ?
C10 C27 Lu2 60.47(6) . . ?
C26 C27 Lu2 106.42(6) . . ?
Lu12 C27 Lu2 27.8(6) . . ?
Lu3 C27 Lu2 27.52(11) . . ?
Lu4 C27 Lu2 49.04(12) . . ?
Lu8 C27 Lu2 47.13(15) . . ?
C27 C28 C29 130.8 . . ?
C27 C28 C50 112.4 . . ?
C29 C28 C50 101.5 . . ?
C27 C28 Lu12 77.2(6) . . ?
C29 C28 Lu12 74.3(7) . . ?
C50 C28 Lu12 80.7(7) . . ?
C27 C28 C10 39.7 . . ?
C29 C28 C10 93.5 . . ?
C50 C28 C10 145.3 . . ?
Lu12 C28 C10 73.5(6) . . ?
C27 C28 Lu3 65.88(10) . . ?
C29 C28 Lu3 86.60(10) . . ?
C50 C28 Lu3 80.81(11) . . ?
Lu12 C28 Lu3 12.7(7) . . ?
C10 C28 Lu3 68.94(10) . . ?
C27 C28 Lu4 70.78(12) . . ?
C29 C28 Lu4 97.55(10) . . ?
C50 C28 Lu4 61.66(13) . . ?
Lu12 C28 Lu4 27.2(8) . . ?
C10 C28 Lu4 85.60(13) . . ?
Lu3 C28 Lu4 20.52(10) . . ?
C27 C28 Lu2 69.03(6) . . ?
C29 C28 Lu2 69.59(6) . . ?
C50 C28 Lu2 102.5 . . ?
Lu12 C28 Lu2 21.9(7) . . ?
C10 C28 Lu2 53.93(6) . . ?
Lu3 C28 Lu2 25.38(10) . . ?
Lu4 C28 Lu2 45.66(12) . . ?
C52 C29 C28 118.7 . . ?
C52 C29 C30 110.2 . . ?
C28 C29 C30 124.5 . . ?
C52 C29 Lu12 87.1(6) . . ?
C28 C29 Lu12 66.7(8) . . ?
C30 C29 Lu12 92.4(7) . . ?
C52 C29 Lu3 92.02(8) . . ?
C28 C29 Lu3 62.00(9) . . ?
C30 C29 Lu3 92.95(10) . . ?
Lu12 C29 Lu3 5.5(7) . . ?
C52 C29 Lu2 97.62(6) . . ?
C28 C29 Lu2 83.41(6) . . ?
C30 C29 Lu2 65.06(6) . . ?
Lu12 C29 Lu2 27.3(7) . . ?
Lu3 C29 Lu2 28.17(10) . . ?
C52 C29 Lu4 84.58(10) . . ?
C28 C29 Lu4 54.43(7) . . ?
C30 C29 Lu4 109.41(9) . . ?
Lu12 C29 Lu4 17.4(8) . . ?
Lu3 C29 Lu4 16.57(8) . . ?
Lu2 C29 Lu4 44.40(10) . . ?
C52 C29 Lu11 59.7(4) . . ?
C28 C29 Lu11 80.7(4) . . ?
C30 C29 Lu11 104.1(3) . . ?
Lu12 C29 Lu11 27.6(7) . . ?
Lu3 C29 Lu11 32.3(4) . . ?
Lu2 C29 Lu11 46.9(3) . . ?
Lu4 C29 Lu11 28.0(4) . . ?
C31 C30 C29 129.2 . . ?
C31 C30 C11 111.5 . . ?
C29 C30 C11 105.4 . . ?
C31 C30 Lu2 84.59(7) . . ?
C29 C30 Lu2 84.42(8) . . ?
C11 C30 Lu2 60.50(7) . . ?
C31 C30 Lu12 103.4(6) . . ?
C29 C30 Lu12 53.8(5) . . ?
C11 C30 Lu12 75.6(4) . . ?
Lu2 C30 Lu12 30.6(5) . . ?
C30 C31 C32 126.2 . . ?
C30 C31 C54 117.4 . . ?
C32 C31 C54 110.3 . . ?
C30 C31 Lu2 68.19(7) . . ?
C32 C31 Lu2 82.35(8) . . ?
C54 C31 Lu2 98.04(6) . . ?
C13 C32 C33 122.5 . . ?
C13 C32 C31 119.9 . . ?
C33 C32 C31 103.7 . . ?
C13 C32 Lu2 67.34(7) . . ?
C33 C32 Lu2 102.5 . . ?
C31 C32 Lu2 66.93(7) . . ?
C32 C33 C55 111.9 . . ?
C32 C33 C34 109.6 . . ?
C55 C33 C34 125.7 . . ?
C35 C34 C58 120.7 . . ?
C35 C34 C33 124.1 . . ?
C58 C34 C33 102.6 . . ?
C34 C35 C14 118.4 . . ?
C34 C35 C36 129.3 . . ?
C14 C35 C36 101.7 . . ?
C37 C36 C16 130.9 . . ?
C37 C36 C35 111.4 . . ?
C16 C36 C35 113.3 . . ?
C36 C37 C59 123.2 . . ?
C36 C37 C38 106.9 . . ?
C59 C37 C38 117.9 . . ?
C39 C38 C37 140.6 . . ?
C39 C38 C61 115.5 . . ?
C37 C38 C61 98.0 . . ?
C38 C39 C17 109.3 . . ?
C38 C39 C40 121.1 . . ?
C17 C39 C40 121.1 . . ?
C63 C40 C41 118.0 . . ?
C63 C40 C39 120.8 . . ?
C41 C40 C39 115.2 . . ?
C63 C40 Lu13 54.5(3) . . ?
C41 C40 Lu13 93.3(4) . . ?
C39 C40 Lu13 99.4(3) . . ?
C42 C41 C40 131.1 . . ?
C42 C41 C19 103.7 . . ?
C40 C41 C19 118.0 . . ?
C41 C42 C43 124.6 . . ?
C41 C42 C21 110.9 . . ?
C43 C42 C21 116.0 . . ?
C42 C43 C44 131.6 . . ?
C42 C43 C64 107.5 . . ?
C44 C43 C64 104.8 . . ?
C45 C44 C66 112.9 . . ?
C45 C44 C43 118.7 . . ?
C66 C44 C43 121.5 . . ?
C45 C44 Lu7 99.33(11) . . ?
C66 C44 Lu7 55.65(11) . . ?
C43 C44 Lu7 89.81(8) . . ?
C46 C45 C44 133.1 . . ?
C46 C45 C22 105.4 . . ?
C44 C45 C22 109.8 . . ?
C45 C46 C47 119.5 . . ?
C45 C46 C24 111.5 . . ?
C47 C46 C24 119.2 . . ?
C67 C47 C46 120.1 . . ?
C67 C47 C48 116.1 . . ?
C46 C47 C48 119.6 . . ?
C67 C47 Lu5 87.94(12) . . ?
C46 C47 Lu5 96.71(13) . . ?
C48 C47 Lu5 64.41(11) . . ?
C67 C47 Lu6 73.59(18) . . ?
C46 C47 Lu6 109.11(13) . . ?
C48 C47 Lu6 67.32(17) . . ?
Lu5 C47 Lu6 15.67(11) . . ?
C49 C48 C70 125.6 . . ?
C49 C48 C47 118.7 . . ?
C70 C48 C47 99.2 . . ?
C49 C48 Lu5 79.25(13) . . ?
C70 C48 Lu5 72.99(14) . . ?
C47 C48 Lu5 76.67(12) . . ?
C49 C48 Lu6 92.77(16) . . ?
C70 C48 Lu6 56.87(15) . . ?
C47 C48 Lu6 77.90(17) . . ?
Lu5 C48 Lu6 16.51(11) . . ?
C49 C48 Lu4 52.22(10) . . ?
C70 C48 Lu4 92.65(8) . . ?
C47 C48 Lu4 91.32(12) . . ?
Lu5 C48 Lu4 27.05(14) . . ?
Lu6 C48 Lu4 41.76(17) . . ?
C49 C48 Lu11 73.1(4) . . ?
C70 C48 Lu11 64.1(4) . . ?
C47 C48 Lu11 97.3(3) . . ?
Lu5 C48 Lu11 21.2(3) . . ?
Lu6 C48 Lu11 22.7(4) . . ?
Lu4 C48 Lu11 28.6(4) . . ?
C50 C49 C48 122.3 . . ?
C50 C49 C25 104.9 . . ?
C48 C49 C25 122.2 . . ?
C50 C49 Lu4 70.62(15) . . ?
C48 C49 Lu4 95.40(15) . . ?
C25 C49 Lu4 69.11(12) . . ?
C50 C49 Lu5 87.04(11) . . ?
C48 C49 Lu5 65.54(11) . . ?
C25 C49 Lu5 87.46(13) . . ?
Lu4 C49 Lu5 29.88(17) . . ?
C50 C49 Lu8 85.05(16) . . ?
C48 C49 Lu8 96.62(12) . . ?
C25 C49 Lu8 53.65(14) . . ?
Lu4 C49 Lu8 17.81(17) . . ?
Lu5 C49 Lu8 36.23(15) . . ?
C50 C49 Lu11 64.4(3) . . ?
C48 C49 Lu11 77.4(4) . . ?
C25 C49 Lu11 97.4(4) . . ?
Lu4 C49 Lu11 28.5(4) . . ?
Lu5 C49 Lu11 23.1(3) . . ?
Lu8 C49 Lu11 44.2(4) . . ?
C50 C49 Lu3 63.44(8) . . ?
C48 C49 Lu3 103.01(6) . . ?
C25 C49 Lu3 68.42(8) . . ?
Lu4 C49 Lu3 8.50(15) . . ?
Lu5 C49 Lu3 37.56(11) . . ?
Lu8 C49 Lu3 22.30(16) . . ?
Lu11 C49 Lu3 31.4(4) . . ?
C50 C49 Lu12 52.7(4) . . ?
C48 C49 Lu12 105.3(5) . . ?
C25 C49 Lu12 76.9(4) . . ?
Lu4 C49 Lu12 18.0(4) . . ?
Lu5 C49 Lu12 42.0(5) . . ?
Lu8 C49 Lu12 33.6(4) . . ?
Lu11 C49 Lu12 28.7(6) . . ?
Lu3 C49 Lu12 11.3(4) . . ?
C49 C50 C51 114.2 . . ?
C49 C50 C28 128.6 . . ?
C51 C50 C28 106.3 . . ?
C49 C50 Lu4 72.50(15) . . ?
C51 C50 Lu4 91.03(11) . . ?
C28 C50 Lu4 76.54(16) . . ?
C49 C50 Lu12 99.9(6) . . ?
C51 C50 Lu12 80.4(6) . . ?
C28 C50 Lu12 56.6(6) . . ?
Lu4 C50 Lu12 27.5(6) . . ?
C49 C50 Lu11 87.1(4) . . ?
C51 C50 Lu11 58.1(4) . . ?
C28 C50 Lu11 88.5(4) . . ?
Lu4 C50 Lu11 33.0(4) . . ?
Lu12 C50 Lu11 33.4(7) . . ?
C49 C50 Lu3 88.68(9) . . ?
C51 C50 Lu3 88.71(8) . . ?
C28 C50 Lu3 61.30(8) . . ?
Lu4 C50 Lu3 16.90(14) . . ?
Lu12 C50 Lu3 12.0(6) . . ?
Lu11 C50 Lu3 35.1(4) . . ?
C49 C50 Lu5 63.71(10) . . ?
C51 C50 Lu5 75.05(12) . . ?
C28 C50 Lu5 99.76(10) . . ?
Lu4 C50 Lu5 25.23(16) . . ?
Lu12 C50 Lu5 44.4(6) . . ?
Lu11 C50 Lu5 23.8(4) . . ?
Lu3 C50 Lu5 38.52(10) . . ?
C71 C51 C50 126.3 . . ?
C71 C51 C52 121.4 . . ?
C50 C51 C52 103.2 . . ?
C71 C51 Lu11 71.4(5) . . ?
C50 C51 Lu11 87.2(6) . . ?
C52 C51 Lu11 83.2(5) . . ?
C71 C51 Lu12 105.3(5) . . ?
C50 C51 Lu12 65.2(6) . . ?
C52 C51 Lu12 66.2(6) . . ?
Lu11 C51 Lu12 34.0(7) . . ?
C71 C51 Lu4 94.04(12) . . ?
C50 C51 Lu4 54.86(8) . . ?
C52 C51 Lu4 90.35(12) . . ?
Lu11 C51 Lu4 32.4(6) . . ?
Lu12 C51 Lu4 24.2(6) . . ?
C71 C51 Lu5 67.69(11) . . ?
C50 C51 Lu5 74.41(11) . . ?
C52 C51 Lu5 103.59(9) . . ?
Lu11 C51 Lu5 22.1(5) . . ?
Lu12 C51 Lu5 43.2(5) . . ?
Lu4 C51 Lu5 26.36(14) . . ?
C71 C51 Lu6 55.19(12) . . ?
C50 C51 Lu6 89.65(16) . . ?
C52 C51 Lu6 101.94(12) . . ?
Lu11 C51 Lu6 20.0(5) . . ?
Lu12 C51 Lu6 51.3(5) . . ?
Lu4 C51 Lu6 40.05(17) . . ?
Lu5 C51 Lu6 15.32(12) . . ?
C71 C51 Lu3 100.95(6) . . ?
C50 C51 Lu3 61.58(7) . . ?
C52 C51 Lu3 74.69(8) . . ?
Lu11 C51 Lu3 30.9(6) . . ?
Lu12 C51 Lu3 8.5(6) . . ?
Lu4 C51 Lu3 15.71(10) . . ?
Lu5 C51 Lu3 36.00(10) . . ?
Lu6 C51 Lu3 45.91(12) . . ?
C53 C52 C29 132.9 . . ?
C53 C52 C51 109.4 . . ?
C29 C52 C51 110.0 . . ?
C53 C52 Lu12 104.5(7) . . ?
C29 C52 Lu12 60.6(6) . . ?
C51 C52 Lu12 78.0(6) . . ?
C53 C52 Lu11 84.2(5) . . ?
C29 C52 Lu11 94.2(5) . . ?
C51 C52 Lu11 59.6(4) . . ?
Lu12 C52 Lu11 33.8(7) . . ?
C53 C52 Lu3 105.02(7) . . ?
C29 C52 Lu3 62.31(6) . . ?
C51 C52 Lu3 75.25(9) . . ?
Lu12 C52 Lu3 2.7(6) . . ?
Lu11 C52 Lu3 31.9(5) . . ?
C52 C53 C54 120.2 . . ?
C52 C53 C73 134.2 . . ?
C54 C53 C73 96.0 . . ?
C52 C53 Lu11 67.9(5) . . ?
C54 C53 Lu11 106.5(3) . . ?
C73 C53 Lu11 75.9(5) . . ?
C52 C53 Lu12 51.1(5) . . ?
C54 C53 Lu12 94.7(5) . . ?
C73 C53 Lu12 103.0(5) . . ?
Lu11 C53 Lu12 28.7(6) . . ?
C55 C54 C53 133.0 . . ?
C55 C54 C31 106.6 . . ?
C53 C54 C31 109.2 . . ?
C56 C55 C54 108.0 . . ?
C56 C55 C33 133.3 . . ?
C54 C55 C33 107.3 . . ?
C56 C55 Lu15 62.1(6) . . ?
C54 C55 Lu15 97.8(6) . . ?
C33 C55 Lu15 83.7(5) . . ?
C74 C56 C55 136.0 . . ?
C74 C56 C57 121.7 . . ?
C55 C56 C57 97.6 . . ?
C74 C56 Lu15 88.7(6) . . ?
C55 C56 Lu15 91.1(7) . . ?
C57 C56 Lu15 65.3(5) . . ?
C74 C56 Lu14 57.5(4) . . ?
C55 C56 Lu14 104.1(4) . . ?
C57 C56 Lu14 94.8(6) . . ?
Lu15 C56 Lu14 33.9(7) . . ?
C74 C56 Lu1 61.20(9) . . ?
C55 C56 Lu1 113.34(8) . . ?
C57 C56 Lu1 80.07(10) . . ?
Lu15 C56 Lu1 27.8(7) . . ?
Lu14 C56 Lu1 16.5(6) . . ?
C56 C57 C76 100.2 . . ?
C56 C57 C58 136.6 . . ?
C76 C57 C58 111.3 . . ?
C56 C57 Lu15 80.21(18) . . ?
C76 C57 Lu15 74.6(8) . . ?
C58 C57 Lu15 80.4(4) . . ?
C34 C58 C59 105.4 . . ?
C34 C58 C57 120.3 . . ?
C59 C58 C57 124.9 . . ?
C34 C58 Lu15 93.6(7) . . ?
C59 C58 Lu15 85.8(4) . . ?
C57 C58 Lu15 63.6(5) . . ?
C37 C59 C58 127.6 . . ?
C37 C59 C60 102.4 . . ?
C58 C59 C60 117.6 . . ?
C37 C59 Lu15 99.0(6) . . ?
C58 C59 Lu15 63.1(6) . . ?
C60 C59 Lu15 75.8(6) . . ?
C77 C60 C61 126.1 . . ?
C77 C60 C59 120.4 . . ?
C61 C60 C59 107.6 . . ?
C77 C60 Lu15 70.0(5) . . ?
C61 C60 Lu15 104.3(6) . . ?
C59 C60 Lu15 73.7(6) . . ?
C62 C61 C60 105.9 . . ?
C62 C61 C38 124.8 . . ?
C60 C61 C38 112.8 . . ?
C79 C62 C61 141.1 . . ?
C79 C62 C63 102.8 . . ?
C61 C62 C63 111.2 . . ?
C79 C62 Lu13 68.8(5) . . ?
C61 C62 Lu13 105.3(4) . . ?
C63 C62 Lu13 70.1(5) . . ?
C79 C62 Lu10 55.4(3) . . ?
C61 C62 Lu10 104.4(4) . . ?
C63 C62 Lu10 91.3(5) . . ?
Lu13 C62 Lu10 22.3(6) . . ?
C64 C63 C40 115.0 . . ?
C64 C63 C62 112.3 . . ?
C40 C63 C62 124.4 . . ?
C64 C63 Lu13 70.2(4) . . ?
C40 C63 Lu13 98.2(4) . . ?
C62 C63 Lu13 72.1(5) . . ?
C63 C64 C65 137.7 . . ?
C63 C64 C43 123.8 . . ?
C65 C64 C43 90.5 . . ?
C63 C64 Lu13 77.1(5) . . ?
C65 C64 Lu13 74.8(5) . . ?
C43 C64 Lu13 96.7(5) . . ?
C63 C64 Lu7 100.23(12) . . ?
C65 C64 Lu7 56.81(10) . . ?
C43 C64 Lu7 82.35(15) . . ?
Lu13 C64 Lu7 23.2(5) . . ?
C80 C65 C64 113.0 . . ?
C80 C65 C66 105.4 . . ?
C64 C65 C66 127.6 . . ?
C80 C65 Lu7 74.55(17) . . ?
C64 C65 Lu7 90.00(10) . . ?
C66 C65 Lu7 67.12(14) . . ?
C80 C65 Lu13 70.8(5) . . ?
C64 C65 Lu13 69.0(5) . . ?
C66 C65 Lu13 92.9(4) . . ?
Lu7 C65 Lu13 26.3(4) . . ?
C80 C65 Lu10 51.7(3) . . ?
C64 C65 Lu10 90.74(15) . . ?
C66 C65 Lu10 86.2(3) . . ?
Lu7 C65 Lu10 25.1(4) . . ?
Lu13 C65 Lu10 23.4(5) . . ?
C44 C66 C65 92.3 . . ?
C44 C66 C67 121.0 . . ?
C65 C66 C67 137.5 . . ?
C44 C66 Lu7 90.80(15) . . ?
C65 C66 Lu7 71.52(12) . . ?
C67 C66 Lu7 81.66(9) . . ?
C44 C66 Lu13 87.0(4) . . ?
C65 C66 Lu13 54.9(3) . . ?
C67 C66 Lu13 98.1(4) . . ?
Lu7 C66 Lu13 17.3(3) . . ?
C47 C67 C68 140.7 . . ?
C47 C67 C66 112.8 . . ?
C68 C67 C66 92.6 . . ?
C47 C67 Lu7 96.80(14) . . ?
C68 C67 Lu7 69.89(15) . . ?
C66 C67 Lu7 59.76(10) . . ?
C47 C67 Lu6 76.8(2) . . ?
C68 C67 Lu6 68.29(18) . . ?
C66 C67 Lu6 103.08(15) . . ?
Lu7 C67 Lu6 43.44(16) . . ?
C47 C67 Lu5 62.27(10) . . ?
C68 C67 Lu5 83.99(11) . . ?
C66 C67 Lu5 102.44(10) . . ?
Lu7 C67 Lu5 46.65(11) . . ?
Lu6 C67 Lu5 15.72(14) . . ?
C69 C68 C81 109.8 . . ?
C69 C68 C67 101.3 . . ?
C81 C68 C67 141.9 . . ?
C69 C68 Lu7 102.80(11) . . ?
C81 C68 Lu7 77.55(14) . . ?
C67 C68 Lu7 74.46(16) . . ?
C69 C68 Lu6 57.96(15) . . ?
C81 C68 Lu6 99.52(18) . . ?
C67 C68 Lu6 78.53(18) . . ?
Lu7 C68 Lu6 45.46(16) . . ?
C69 C68 Lu10 91.7(3) . . ?
C81 C68 Lu10 56.9(3) . . ?
C67 C68 Lu10 101.7(5) . . ?
Lu7 C68 Lu10 28.0(5) . . ?
Lu6 C68 Lu10 46.4(3) . . ?
C69 C68 Lu9 73.3(2) . . ?
C81 C68 Lu9 61.7(2) . . ?
C67 C68 Lu9 109.2(2) . . ?
Lu7 C68 Lu9 42.1(2) . . ?
Lu6 C68 Lu9 37.8(3) . . ?
Lu10 C68 Lu9 18.9(4) . . ?
C68 C69 C70 123.0 . . ?
C68 C69 C84 122.8 . . ?
C70 C69 C84 109.3 . . ?
C68 C69 Lu6 89.1(2) . . ?
C70 C69 Lu6 70.7(2) . . ?
C84 C69 Lu6 87.5(2) . . ?
C68 C69 Lu9 75.96(17) . . ?
C70 C69 Lu9 109.6(2) . . ?
C84 C69 Lu9 65.64(18) . . ?
Lu6 C69 Lu9 40.1(3) . . ?
C68 C69 Lu5 89.09(10) . . ?
C70 C69 Lu5 60.95(9) . . ?
C84 C69 Lu5 97.85(10) . . ?
Lu6 C69 Lu5 12.3(2) . . ?
Lu9 C69 Lu5 51.7(2) . . ?
C68 C69 Lu14 96.7(5) . . ?
C70 C69 Lu14 93.2(6) . . ?
C84 C69 Lu14 56.6(4) . . ?
Lu6 C69 Lu14 32.9(5) . . ?
Lu9 C69 Lu14 21.7(5) . . ?
Lu5 C69 Lu14 45.0(5) . . ?
C68 C69 Lu1 83.29(11) . . ?
C70 C69 Lu1 108.69(8) . . ?
C84 C69 Lu1 57.97(10) . . ?
Lu6 C69 Lu1 42.1(2) . . ?
Lu9 C69 Lu1 8.09(19) . . ?
Lu5 C69 Lu1 54.24(10) . . ?
Lu14 C69 Lu1 16.6(5) . . ?
C68 C69 Lu11 106.9(3) . . ?
C70 C69 Lu11 62.0(4) . . ?
C84 C69 Lu11 77.2(4) . . ?
Lu6 C69 Lu11 17.8(3) . . ?
Lu9 C69 Lu11 48.1(4) . . ?
Lu5 C69 Lu11 22.1(4) . . ?
Lu14 C69 Lu11 32.0(7) . . ?
Lu1 C69 Lu11 46.7(4) . . ?
C69 C70 C71 106.0 . . ?
C69 C70 C48 135.0 . . ?
C71 C70 C48 105.5 . . ?
C69 C70 Lu6 70.5(2) . . ?
C71 C70 Lu6 78.56(19) . . ?
C48 C70 Lu6 85.3(2) . . ?
C69 C70 Lu5 87.07(12) . . ?
C71 C70 Lu5 80.80(12) . . ?
C48 C70 Lu5 67.22(12) . . ?
Lu6 C70 Lu5 18.43(19) . . ?
C69 C70 Lu11 88.8(4) . . ?
C71 C70 Lu11 56.3(4) . . ?
C48 C70 Lu11 82.6(5) . . ?
Lu6 C70 Lu11 24.7(4) . . ?
Lu5 C70 Lu11 25.2(4) . . ?
C51 C71 C72 119.3 . . ?
C51 C71 C70 125.3 . . ?
C72 C71 C70 107.8 . . ?
C51 C71 Lu11 70.7(5) . . ?
C72 C71 Lu11 83.3(6) . . ?
C70 C71 Lu11 89.8(5) . . ?
C51 C71 Lu6 95.52(19) . . ?
C72 C71 Lu6 81.6(2) . . ?
C70 C71 Lu6 64.23(14) . . ?
Lu11 C71 Lu6 28.0(5) . . ?
C51 C71 Lu5 82.03(11) . . ?
C72 C71 Lu5 97.03(11) . . ?
C70 C71 Lu5 65.34(10) . . ?
Lu11 C71 Lu5 25.3(5) . . ?
Lu6 C71 Lu5 16.85(17) . . ?
C51 C71 Lu14 98.2(4) . . ?
C72 C71 Lu14 52.8(4) . . ?
C70 C71 Lu14 88.5(4) . . ?
Lu11 C71 Lu14 33.0(7) . . ?
Lu6 C71 Lu14 31.6(5) . . ?
Lu5 C71 Lu14 44.8(5) . . ?
C73 C72 C71 123.5 . . ?
C73 C72 C84 120.1 . . ?
C71 C72 C84 110.0 . . ?
C73 C72 Lu14 75.7(6) . . ?
C71 C72 Lu14 98.0(7) . . ?
C84 C72 Lu14 72.0(5) . . ?
C73 C72 Lu11 86.9(4) . . ?
C71 C72 Lu11 61.6(4) . . ?
C84 C72 Lu11 97.3(4) . . ?
Lu14 C72 Lu11 38.7(8) . . ?
C73 C72 Lu6 105.33(12) . . ?
C71 C72 Lu6 65.24(19) . . ?
C84 C72 Lu6 73.03(19) . . ?
Lu14 C72 Lu6 35.6(7) . . ?
Lu11 C72 Lu6 25.4(4) . . ?
C73 C72 Lu1 79.89(11) . . ?
C71 C72 Lu1 106.77(8) . . ?
C84 C72 Lu1 59.54(9) . . ?
Lu14 C72 Lu1 13.7(6) . . ?
Lu11 C72 Lu1 51.0(4) . . ?
Lu6 C72 Lu1 41.68(19) . . ?
C73 C72 Lu9 89.75(13) . . ?
C71 C72 Lu9 99.91(18) . . ?
C84 C72 Lu9 54.34(16) . . ?
Lu14 C72 Lu9 18.1(5) . . ?
Lu11 C72 Lu9 49.2(4) . . ?
Lu6 C72 Lu9 34.9(3) . . ?
Lu1 C72 Lu9 10.01(13) . . ?
C72 C73 C74 108.0 . . ?
C72 C73 C53 110.9 . . ?
C74 C73 C53 135.5 . . ?
C72 C73 Lu14 71.1(6) . . ?
C74 C73 Lu14 73.2(7) . . ?
C53 C73 Lu14 99.8(5) . . ?
C72 C73 Lu11 63.8(4) . . ?
C74 C73 Lu11 108.3(4) . . ?
C53 C73 Lu11 71.8(4) . . ?
Lu14 C73 Lu11 35.4(8) . . ?
C72 C73 Lu1 73.60(10) . . ?
C74 C73 Lu1 60.87(8) . . ?
C53 C73 Lu1 111.10(7) . . ?
Lu14 C73 Lu1 12.9(7) . . ?
Lu11 C73 Lu1 48.2(4) . . ?
C56 C74 C73 110.8 . . ?
C56 C74 C75 100.9 . . ?
C73 C74 C75 137.4 . . ?
C56 C74 Lu14 96.1(6) . . ?
C73 C74 Lu14 73.1(7) . . ?
C75 C74 Lu14 76.0(6) . . ?
C56 C74 Lu1 93.74(11) . . ?
C73 C74 Lu1 91.40(10) . . ?
C75 C74 Lu1 58.09(9) . . ?
Lu14 C74 Lu1 18.8(7) . . ?
C56 C74 Lu15 64.7(7) . . ?
C73 C74 Lu15 97.4(6) . . ?
C75 C74 Lu15 70.9(6) . . ?
Lu14 C74 Lu15 34.3(9) . . ?
Lu1 C74 Lu15 29.3(7) . . ?
C56 C74 Lu9 100.94(18) . . ?
C73 C74 Lu9 88.0(2) . . ?
C75 C74 Lu9 57.88(19) . . ?
Lu14 C74 Lu9 18.3(6) . . ?
Lu1 C74 Lu9 7.3(2) . . ?
Lu15 C74 Lu9 36.4(7) . . ?
C74 C75 C83 112.7 . . ?
C74 C75 C76 116.5 . . ?
C83 C75 C76 121.4 . . ?
C74 C75 Lu1 89.22(13) . . ?
C83 C75 Lu1 66.68(13) . . ?
C76 C75 Lu1 84.06(13) . . ?
C74 C75 Lu14 70.3(6) . . ?
C83 C75 Lu14 70.8(5) . . ?
C76 C75 Lu14 97.8(6) . . ?
Lu1 C75 Lu14 19.8(6) . . ?
C74 C75 Lu9 94.0(2) . . ?
C83 C75 Lu9 56.92(18) . . ?
C76 C75 Lu9 89.6(3) . . ?
Lu1 C75 Lu9 9.8(2) . . ?
Lu14 C75 Lu9 23.8(6) . . ?
C74 C75 Lu15 79.6(5) . . ?
C83 C75 Lu15 97.3(7) . . ?
C76 C75 Lu15 63.8(5) . . ?
Lu1 C75 Lu15 30.8(8) . . ?
Lu14 C75 Lu15 35.4(8) . . ?
Lu9 C75 Lu15 40.4(7) . . ?
C77 C76 C75 124.1 . . ?
C77 C76 C57 126.7 . . ?
C75 C76 C57 100.4 . . ?
C77 C76 Lu15 87.5(5) . . ?
C75 C76 Lu15 83.8(3) . . ?
C57 C76 Lu15 68.1(8) . . ?
C77 C76 Lu1 84.01(12) . . ?
C75 C76 Lu1 60.78(11) . . ?
C57 C76 Lu1 95.48(11) . . ?
Lu15 C76 Lu1 32.4(7) . . ?
C77 C76 Lu9 79.54(19) . . ?
C75 C76 Lu9 60.3(2) . . ?
C57 C76 Lu9 102.54(14) . . ?
Lu15 C76 Lu9 38.4(7) . . ?
Lu1 C76 Lu9 7.07(19) . . ?
C78 C77 C76 117.3 . . ?
C78 C77 C60 111.0 . . ?
C76 C77 C60 118.6 . . ?
C78 C77 Lu1 69.75(11) . . ?
C76 C77 Lu1 64.55(11) . . ?
C60 C77 Lu1 102.07(9) . . ?
C78 C77 Lu15 94.8(7) . . ?
C76 C77 Lu15 61.0(5) . . ?
C60 C77 Lu15 79.9(3) . . ?
Lu1 C77 Lu15 28.9(6) . . ?
C77 C78 C82 112.9 . . ?
C77 C78 C79 135.3 . . ?
C82 C78 C79 107.4 . . ?
C77 C78 Lu10 102.2(6) . . ?
C82 C78 Lu10 72.49(16) . . ?
C79 C78 Lu10 71.8(5) . . ?
C77 C78 Lu9 91.54(14) . . ?
C82 C78 Lu9 61.9(2) . . ?
C79 C78 Lu9 90.61(17) . . ?
Lu10 C78 Lu9 19.1(4) . . ?
C77 C78 Lu1 80.47(12) . . ?
C82 C78 Lu1 65.69(10) . . ?
C79 C78 Lu1 99.56(11) . . ?
Lu10 C78 Lu1 27.9(5) . . ?
Lu9 C78 Lu1 11.18(13) . . ?
C77 C78 Lu13 105.4(3) . . ?
C82 C78 Lu13 91.9(4) . . ?
C79 C78 Lu13 53.8(3) . . ?
Lu10 C78 Lu13 22.4(4) . . ?
Lu9 C78 Lu13 40.7(4) . . ?
Lu1 C78 Lu13 47.1(3) . . ?
C62 C79 C80 140.4 . . ?
C62 C79 C78 100.5 . . ?
C80 C79 C78 105.5 . . ?
C62 C79 Lu13 77.5(5) . . ?
C80 C79 Lu13 71.2(5) . . ?
C78 C79 Lu13 94.5(4) . . ?
C62 C79 Lu10 96.3(3) . . ?
C80 C79 Lu10 65.4(5) . . ?
C78 C79 Lu10 71.3(6) . . ?
Lu13 C79 Lu10 27.5(5) . . ?
C62 C79 Lu7 97.19(9) . . ?
C80 C79 Lu7 51.49(10) . . ?
C78 C79 Lu7 95.47(11) . . ?
Lu13 C79 Lu7 20.2(5) . . ?
Lu10 C79 Lu7 24.7(6) . . ?
C65 C80 C81 135.6 . . ?
C65 C80 C79 109.2 . . ?
C81 C80 C79 109.7 . . ?
C65 C80 Lu10 101.0(6) . . ?
C81 C80 Lu10 68.2(2) . . ?
C79 C80 Lu10 77.1(4) . . ?
C65 C80 Lu7 71.80(15) . . ?
C81 C80 Lu7 82.67(11) . . ?
C79 C80 Lu7 97.55(13) . . ?
Lu10 C80 Lu7 31.5(6) . . ?
C65 C80 Lu13 77.1(5) . . ?
C81 C80 Lu13 96.1(5) . . ?
C79 C80 Lu13 71.2(5) . . ?
Lu10 C80 Lu13 28.5(5) . . ?
Lu7 C80 Lu13 26.8(5) . . ?
C65 C80 Lu9 111.63(19) . . ?
C81 C80 Lu9 54.7(2) . . ?
C79 C80 Lu9 82.1(2) . . ?
Lu10 C80 Lu9 13.6(3) . . ?
Lu7 C80 Lu9 39.9(2) . . ?
Lu13 C80 Lu9 42.0(5) . . ?
C68 C81 C82 141.7 . . ?
C68 C81 C80 105.5 . . ?
C82 C81 C80 105.4 . . ?
C68 C81 Lu10 88.9(5) . . ?
C82 C81 Lu10 79.3(7) . . ?
C80 C81 Lu10 72.7(4) . . ?
C68 C81 Lu9 85.0(3) . . ?
C82 C81 Lu9 70.8(2) . . ?
C80 C81 Lu9 94.2(2) . . ?
Lu10 C81 Lu9 21.6(5) . . ?
C68 C81 Lu7 68.55(11) . . ?
C82 C81 Lu7 107.79(13) . . ?
C80 C81 Lu7 62.20(9) . . ?
Lu10 C81 Lu7 28.6(7) . . ?
Lu9 C81 Lu7 43.8(2) . . ?
C68 C81 Lu1 91.16(9) . . ?
C82 C81 Lu1 62.91(9) . . ?
C80 C81 Lu1 97.40(11) . . ?
Lu10 C81 Lu1 26.4(5) . . ?
Lu9 C81 Lu1 8.0(2) . . ?
Lu7 C81 Lu1 51.16(14) . . ?
C68 C81 Lu13 90.1(4) . . ?
C82 C81 Lu13 90.7(4) . . ?
C80 C81 Lu13 53.2(3) . . ?
Lu10 C81 Lu13 20.1(5) . . ?
Lu9 C81 Lu13 41.6(4) . . ?
Lu7 C81 Lu13 21.5(4) . . ?
Lu1 C81 Lu13 46.4(3) . . ?
C78 C82 C83 130.8 . . ?
C78 C82 C81 110.5 . . ?
C83 C82 C81 95.0 . . ?
C78 C82 Lu9 84.7(3) . . ?
C83 C82 Lu9 63.3(2) . . ?
C81 C82 Lu9 72.24(18) . . ?
C78 C82 Lu10 72.3(2) . . ?
C83 C82 Lu10 83.8(3) . . ?
C81 C82 Lu10 63.3(6) . . ?
Lu9 C82 Lu10 21.0(4) . . ?
C78 C82 Lu1 81.41(12) . . ?
C83 C82 Lu1 59.36(12) . . ?
C81 C82 Lu1 84.26(12) . . ?
Lu9 C82 Lu1 12.10(16) . . ?
Lu10 C82 Lu1 29.6(5) . . ?
C75 C83 C82 107.4 . . ?
C75 C83 C84 111.2 . . ?
C82 C83 C84 136.4 . . ?
C75 C83 Lu1 74.73(14) . . ?
C82 C83 Lu1 84.08(14) . . ?
C84 C83 Lu1 87.30(13) . . ?
C75 C83 Lu9 88.65(18) . . ?
C82 C83 Lu9 78.8(3) . . ?
C84 C83 Lu9 82.7(3) . . ?
Lu1 C83 Lu9 13.95(17) . . ?
C75 C83 Lu14 75.1(6) . . ?
C82 C83 Lu14 103.1(6) . . ?
C84 C83 Lu14 69.2(7) . . ?
Lu1 C83 Lu14 20.1(6) . . ?
Lu9 C83 Lu14 25.3(6) . . ?
C75 C83 Lu10 97.6(5) . . ?
C82 C83 Lu10 63.4(2) . . ?
C84 C83 Lu10 91.9(3) . . ?
Lu1 C83 Lu10 26.8(4) . . ?
Lu9 C83 Lu10 16.1(3) . . ?
Lu14 C83 Lu10 41.3(6) . . ?
C72 C84 C69 106.1 . . ?
C72 C84 C83 128.2 . . ?
C69 C84 C83 114.1 . . ?
C72 C84 Lu14 72.2(6) . . ?
C69 C84 Lu14 92.0(6) . . ?
C83 C84 Lu14 75.0(7) . . ?
C72 C84 Lu9 96.87(19) . . ?
C69 C84 Lu9 81.10(18) . . ?
C83 C84 Lu9 60.4(2) . . ?
Lu14 C84 Lu9 25.0(6) . . ?
C72 C84 Lu1 90.94(11) . . ?
C69 C84 Lu1 92.53(12) . . ?
C83 C84 Lu1 57.10(9) . . ?
Lu14 C84 Lu1 19.6(7) . . ?
Lu9 C84 Lu1 11.79(14) . . ?
C72 C84 Lu6 74.73(18) . . ?
C69 C84 Lu6 58.05(14) . . ?
C83 C84 Lu6 99.91(19) . . ?
Lu14 C84 Lu6 35.9(7) . . ?
Lu9 C84 Lu6 39.7(3) . . ?
Lu1 C84 Lu6 45.87(17) . . ?
N1A Ni1A N3A 177.76(18) . . ?
N1A Ni1A N2A 89.97(8) . 6 ?
N3A Ni1A N2A 89.98(8) . 6 ?
N1A Ni1A N2A 89.97(8) . . ?
N3A Ni1A N2A 89.98(8) . . ?
N2A Ni1A N2A 177.34(19) 6 . ?
C13A N2A C6A 104.3(3) . . ?
C13A N2A Ni1A 127.8(2) . . ?
C6A N2A Ni1A 127.9(2) . . ?
C3A C2A C1A 112.7(4) . . ?
C15A N3A C15A 104.3(4) . 6 ?
C15A N3A Ni1A 127.8(2) . . ?
C15A N3A Ni1A 127.8(2) 6 . ?
C5A C4A N1A 125.3(3) . . ?
C5A C4A C3A 123.7(3) . . ?
N1A C4A C3A 111.0(3) . . ?
C4A C5A C6A 124.4(4) . . ?
C5A C6A N2A 124.6(4) . . ?
C5A C6A C7A 124.1(4) . . ?
N2A C6A C7A 111.3(3) . . ?
C10A C7A C6A 106.4(3) . . ?
C10A C7A C8A 129.3(4) . . ?
C6A C7A C8A 124.3(4) . . ?
C7A C8A C9A 112.6(4) . . ?
C7A C10A C13A 106.6(3) . . ?
C7A C10A C11A 129.0(4) . . ?
C13A C10A C11A 124.4(4) . . ?
C10A C11A C12A 113.2(4) . . ?
C14A C13A N2A 124.6(3) . . ?
C14A C13A C10A 123.9(4) . . ?
N2A C13A C10A 111.5(3) . . ?
C15A C14A C13A 124.5(4) . . ?
C14A C15A N3A 125.3(3) . . ?
C14A C15A C16A 123.4(3) . . ?
N3A C15A C16A 111.3(3) . . ?
C16A C16A C15A 106.5(2) 6 . ?
C16A C16A C17A 128.8(2) 6 . ?
C15A C16A C17A 124.5(4) . . ?
C16A C17A C18A 112.0(3) . . ?
C3A C3A C4A 106.8(2) 6 . ?
C3A C3A C2A 128.9(2) 6 . ?
C4A C3A C2A 124.1(4) . . ?
C4A N1A C4A 104.3(4) 6 . ?
C4A N1A Ni1A 127.8(2) 6 . ?
C4A N1A Ni1A 127.8(2) . . ?
C2B C1B C6B 121.5(9) . . ?
C3B C2B C1B 119.6(8) . . ?
C2B C3B C4B 120.0(7) . . ?
C5B C4B C3B 121.3(7) . . ?
C4B C5B C6B 119.1(8) . . ?
C5B C6B C1B 118.6(8) . . ?

_refine_diff_density_max         1.015
_refine_diff_density_min         -1.434
_refine_diff_density_rms         0.118



_vrf_PLAT307_Lu2@C2v-C84         
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2@C2v-C84         
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2C2@C2v-C86
_database_code_depnum_ccdc_archive 'CCDC 1836828'
_audit_update_record             
;
2018-04-13 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2C2@C2v-C86 Ni(OEP)'
_chemical_name_common            'Lu2C2@C2v-C86 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C88, C36 H44 N4 Ni, C6 H6'
_chemical_formula_sum            'C130 H50 Lu2 N4 Ni'
_chemical_formula_weight         2076.39

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.4720 5.8584 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.604(5)
_cell_length_b                   15.012(5)
_cell_length_c                   19.852(5)
_cell_angle_alpha                85.556(5)
_cell_angle_beta                 88.966(5)
_cell_angle_gamma                62.445(5)
_cell_volume                     3846(2)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9717
_cell_measurement_theta_min      2.503
_cell_measurement_theta_max      23.153

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.793
_exptl_crystal_F_000             2056
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.180
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.100
_exptl_absorpt_coefficient_mu    2.859
_shelx_estimated_absorpt_T_min   0.604
_shelx_estimated_absorpt_T_max   0.751
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.6095
_exptl_absorpt_correction_T_max  0.7449
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71069
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean 8.3
_diffrn_reflns_number            50267
_diffrn_reflns_av_unetI/netI     0.0398
_diffrn_reflns_av_R_equivalents  0.0477
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         1.864
_diffrn_reflns_theta_max         25.369
_diffrn_reflns_theta_full        25.240
_diffrn_measured_fraction_theta_max 0.932
_diffrn_measured_fraction_theta_full 0.934
_diffrn_reflns_Laue_measured_fraction_max 0.932
_diffrn_reflns_Laue_measured_fraction_full 0.934
_diffrn_reflns_point_group_measured_fraction_max 0.932
_diffrn_reflns_point_group_measured_fraction_full 0.934
_reflns_number_total             13162
_reflns_number_gt                11621
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1310P)²+51.6410P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         13162
_refine_ls_number_parameters     1342
_refine_ls_number_restraints     1217
_refine_ls_R_factor_all          0.1157
_refine_ls_R_factor_gt           0.1047
_refine_ls_wR_factor_ref         0.2816
_refine_ls_wR_factor_gt          0.2705
_refine_ls_goodness_of_fit_ref   1.058
_refine_ls_restrained_S_all      1.085
_refine_ls_shift/su_max          0.088
_refine_ls_shift/su_mean         0.002

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.75611(10) 0.21649(9) 0.20436(6) 0.0222(3) Uani 0.2498 1 d . . P A 1
Lu2 Lu 0.8232(5) 0.2035(4) 0.2442(3) 0.0446(13) Uani 0.0776 1 d . . P A 1
Lu3 Lu 0.83217(11) 0.12425(10) 0.23343(7) 0.0261(3) Uani 0.2625 1 d . . P A 1
Lu4 Lu 0.84848(9) 0.05771(8) 0.28631(7) 0.0245(3) Uani 0.2604 1 d . . P A 1
Lu5 Lu 0.761(3) 0.0472(19) 0.284(2) 0.141(9) Uani 0.0357 1 d . U P A 1
Lu6 Lu 0.786(2) 0.114(2) 0.2236(18) 0.168(9) Uani 0.0517 1 d . U P A 1
Lu7 Lu 0.800(3) 0.0372(18) 0.3458(18) 0.219(11) Uani 0.0623 1 d . U P A 1
Lu8 Lu 0.56711(13) 0.34417(11) 0.31357(9) 0.0270(4) Uani 0.2545 1 d . U P A 1
Lu9 Lu 0.57237(12) 0.30136(10) 0.36300(9) 0.0318(4) Uani 0.2561 1 d . U P A 1
Lu10 Lu 0.5520(4) 0.2429(4) 0.3600(3) 0.0508(14) Uani 0.0804 1 d . U P A 1
Lu11 Lu 0.63568(10) 0.22388(9) 0.41121(6) 0.0236(3) Uani 0.2413 1 d . U P A 1
Lu12 Lu 0.6130(14) 0.3279(12) 0.3740(9) 0.115(4) Uani 0.0616 1 d . U P A 1
Lu13 Lu 0.5740(13) 0.3233(12) 0.2998(10) 0.193(6) Uani 0.1062 1 d . U P A 1
C1E C 0.7288(9) 0.2304(8) 0.3142(5) 0.050(2) Uani 1 1 d . U . A 1
C2E C 0.7196(11) 0.1616(9) 0.3278(6) 0.070(4) Uani 1 1 d . U . A 1
C1 C 0.8232(14) -0.0852(12) 0.2116(11) 0.096(4) Uani 1 1 d . U . B 2
C2 C 0.9305(9) -0.1059(7) 0.2379(7) 0.063(3) Uani 1 1 d . U . B 2
C3 C 0.9603(8) -0.0406(7) 0.2001(6) 0.053(3) Uani 1 1 d . U . B 2
C4 C 0.8839(10) 0.0187(8) 0.1480(7) 0.061(3) Uani 1 1 d . U . B 2
C5 C 0.7931(12) 0.0018(10) 0.1580(9) 0.087(4) Uani 1 1 d . U . B 2
C6 C 0.6936(15) 0.0726(13) 0.1496(9) 0.096(4) Uani 1 1 d . U . B 2
C7 C 0.6766(16) 0.1609(12) 0.1203(7) 0.091(4) Uani 1 1 d . U . B 2
C8 C 0.7643(12) 0.1843(10) 0.1026(7) 0.072(3) Uani 1 1 d . U . B 2
C9 C 0.8692(11) 0.1160(9) 0.1217(7) 0.066(3) Uani 1 1 d . U . B 2
C10 C 0.9299(10) 0.1573(9) 0.1496(6) 0.060(3) Uani 1 1 d . U . B 2
C11 C 0.9951(9) 0.1030(9) 0.2067(6) 0.057(3) Uani 1 1 d . U . B 2
C12 C 1.0088(8) 0.0060(8) 0.2334(6) 0.050(2) Uani 1 1 d . U . B 2
C13 C 1.0221(9) -0.0087(8) 0.3051(6) 0.055(3) Uani 1 1 d . U . B 2
C14 C 0.9913(9) -0.0761(9) 0.3409(7) 0.071(4) Uani 1 1 d D U . B 2
C15 C 0.9534(10) -0.1280(8) 0.3082(9) 0.075(4) Uani 1 1 d . U . B 2
C16 C 0.8808(11) -0.1538(9) 0.3464(9) 0.081(4) Uani 1 1 d . U . B 2
C17 C 0.7911(16) -0.1426(9) 0.3108(10) 0.099(5) Uani 1 1 d . U . B 2
C18 C 0.7526(19) -0.0938(15) 0.2534(13) 0.123(5) Uani 1 1 d . U . B 2
C19 C 0.6477(13) -0.0227(12) 0.2455(10) 0.097(5) Uani 1 1 d . U . B 2
C20 C 0.6101(12) 0.0743(13) 0.1965(7) 0.081(4) Uani 1 1 d D U . B 2
C21 C 0.5219(13) 0.1605(12) 0.2163(8) 0.083(4) Uani 1 1 d D U . B 2
C22 C 0.5089(13) 0.2551(14) 0.1767(9) 0.090(4) Uani 1 1 d . U . B 2
C23 C 0.5806(10) 0.2575(10) 0.1301(6) 0.063(3) Uani 1 1 d . U . B 2
C24 C 0.6114(11) 0.3345(9) 0.1197(6) 0.070(3) Uani 1 1 d . U . B 2
C25 C 0.7223(11) 0.2910(9) 0.1040(6) 0.066(3) Uani 1 1 d . U . B 2
C26 C 0.7805(10) 0.3328(9) 0.1304(7) 0.066(3) Uani 1 1 d . U . B 2
C27 C 0.8852(9) 0.2645(9) 0.1542(6) 0.059(3) Uani 1 1 d . U . B 2
C28 C 0.9210(10) 0.2861(10) 0.2148(8) 0.079(4) Uani 1 1 d D U . B 2
C29 C 0.9936(10) 0.1744(11) 0.2505(8) 0.078(3) Uani 1 1 d D U . B 2
C30 C 0.9971(12) 0.1641(14) 0.3151(11) 0.092(4) Uani 1 1 d . U . B 2
C31 C 1.0093(10) 0.0729(11) 0.3425(7) 0.075(4) Uani 1 1 d D U . B 2
C32 C 0.9563(12) 0.0678(13) 0.4148(7) 0.098(5) Uani 1 1 d D U . B 2
C33 C 0.9477(11) -0.0362(13) 0.4133(7) 0.105(5) Uani 1 1 d D U . B 2
C34 C 0.9047(15) 0.1456(18) 0.4479(9) 0.121(6) Uani 1 1 d . U . B 2
C35 C 0.9083(14) 0.2402(14) 0.4145(10) 0.099(5) Uani 1 1 d . U . B 2
C36 C 0.9455(11) 0.2565(15) 0.3509(11) 0.098(4) Uani 1 1 d . U . B 2
C37 C 0.8771(15) 0.3569(16) 0.3255(11) 0.104(5) Uani 1 1 d . U . B 2
C38 C 0.8682(16) 0.3636(14) 0.2508(12) 0.108(5) Uani 1 1 d . U . B 2
C39 C 0.7783(12) 0.4305(10) 0.2277(9) 0.087(3) Uani 1 1 d . U . B 2
C40 C 0.7279(11) 0.4218(8) 0.1682(7) 0.071(3) Uani 1 1 d . U . B 2
C41 C 0.6221(10) 0.4650(8) 0.1772(7) 0.066(3) Uani 1 1 d . U . B 2
C42 C 0.5622(10) 0.4193(9) 0.1535(7) 0.069(3) Uani 1 1 d . U . B 2
C43 C 0.4773(9) 0.4235(9) 0.1913(7) 0.067(3) Uani 1 1 d . U . B 2
C44 C 0.4563(10) 0.3412(11) 0.1997(7) 0.078(3) Uani 1 1 d D U . B 2
C45 C 0.4038(10) 0.3426(11) 0.2725(7) 0.074(3) Uani 1 1 d D U . B 2
C46 C 0.4166(16) 0.2598(18) 0.3060(13) 0.122(5) Uani 1 1 d . U . B 2
C47 C 0.4720(14) 0.1608(16) 0.2761(12) 0.112(5) Uani 1 1 d . U . B 2
C48 C 0.5042(14) 0.0813(15) 0.3106(10) 0.129(5) Uani 1 1 d D U . B 2
C49 C 0.5870(15) -0.0110(12) 0.3059(8) 0.101(4) Uani 1 1 d D U . B 2
C50 C 0.6078(17) -0.0511(14) 0.3735(10) 0.130(6) Uani 1 1 d D U . B 2
C51 C 0.7002(15) -0.1079(11) 0.3671(12) 0.104(4) Uani 1 1 d . U . B 2
C52 C 0.7548(14) -0.1036(9) 0.4328(8) 0.104(5) Uani 1 1 d D U . B 2
C53 C 0.8573(12) -0.1216(9) 0.4163(7) 0.083(4) Uani 1 1 d D U . B 2
C54 C 0.6832(11) 0.4955(8) 0.2767(9) 0.078(4) Uani 1 1 d . U . B 2
C55 C 0.5964(10) 0.5111(7) 0.2392(8) 0.073(3) Uani 1 1 d . U . B 2
C56 C 0.5079(10) 0.5185(7) 0.2779(8) 0.070(3) Uani 1 1 d . U . B 2
C57 C 0.4484(10) 0.4788(9) 0.2527(8) 0.075(4) Uani 1 1 d . U . B 2
C58 C 0.4008(9) 0.4332(9) 0.2973(7) 0.067(3) Uani 1 1 d . U . B 2
C59 C 0.4113(9) 0.4317(9) 0.3696(7) 0.067(3) Uani 1 1 d . U . B 2
C60 C 0.4751(10) 0.4694(8) 0.3945(7) 0.068(3) Uani 1 1 d . U . B 2
C61 C 0.5226(9) 0.5126(7) 0.3474(8) 0.069(3) Uani 1 1 d . U . B 2
C62 C 0.4047(12) 0.3472(11) 0.4030(8) 0.079(4) Uani 1 1 d . U . B 2
C63 C 0.4033(19) 0.2637(19) 0.3682(12) 0.143(7) Uani 1 1 d D U . B 2
C64 C 0.4714(19) 0.0894(18) 0.3767(11) 0.170(8) Uani 1 1 d D U . B 2
C65 C 0.455(2) 0.1726(17) 0.4242(11) 0.141(6) Uani 1 1 d D U . B 2
C66 C 0.554(2) 0.0237(19) 0.4178(10) 0.146(7) Uani 1 1 d D U . B 2
C67 C 0.617(2) 0.0199(15) 0.4753(11) 0.135(7) Uani 1 1 d . U . B 2
C68 C 0.7114(17) -0.0367(12) 0.4815(8) 0.119(6) Uani 1 1 d D U . B 2
C69 C 0.4640(12) 0.3003(11) 0.4653(8) 0.084(4) Uani 1 1 d D U . B 2
C70 C 0.4878(17) 0.1903(13) 0.4765(9) 0.113(6) Uani 1 1 d D U . B 2
C71 C 0.7049(16) 0.4740(13) 0.3458(14) 0.121(5) Uani 1 1 d . U . B 2
C72 C 0.6232(14) 0.4887(11) 0.3774(10) 0.109(5) Uani 1 1 d D U . B 2
C73 C 0.5411(11) 0.4152(12) 0.4511(7) 0.084(4) Uani 1 1 d . U . B 2
C74 C 0.5366(13) 0.3305(13) 0.4882(7) 0.094(5) Uani 1 1 d . U . B 2
C75 C 0.8039(12) 0.3955(12) 0.3791(12) 0.104(5) Uani 1 1 d . U . B 2
C76 C 0.8254(14) 0.3216(17) 0.4313(8) 0.114(4) Uani 1 1 d D U . B 2
C77 C 0.7255(13) 0.3316(15) 0.4725(8) 0.125(4) Uani 1 1 d D U . B 2
C78 C 0.6413(14) 0.4157(14) 0.4452(8) 0.118(4) Uani 1 1 d D U . B 2
C79 C 0.7356(16) 0.2257(15) 0.4996(9) 0.136(3) Uani 1 1 d D U . B 2
C80 C 0.6389(17) 0.2553(17) 0.5113(9) 0.138(4) Uani 1 1 d . U . B 2
C81 C 0.8197(16) 0.1313(13) 0.4893(8) 0.133(4) Uani 1 1 d D U . B 2
C82 C 0.7302(15) 0.0396(15) 0.5028(8) 0.143(4) Uani 1 1 d D U . B 2
C83 C 0.578(2) 0.1237(18) 0.5031(9) 0.142(4) Uani 1 1 d . U . B 2
C84 C 0.6516(19) 0.1423(18) 0.5186(9) 0.141(4) Uani 1 1 d . U . B 2
C85 C 0.8863(14) -0.0564(12) 0.4473(8) 0.130(5) Uani 1 1 d D U . B 2
C86 C 0.8285(14) 0.0202(13) 0.4871(7) 0.134(4) Uani 1 1 d D U . B 2
Ni1A Ni 0.52253(6) 0.01905(6) 0.08297(5) 0.0175(2) Uani 1 1 d . . . C 3
C1A C 0.6752(5) 0.0269(5) -0.0169(4) 0.0213(14) Uani 1 1 d . U . C 3
N2A N 0.3969(4) 0.1490(4) 0.0820(3) 0.0181(12) Uani 1 1 d . . . C 3
C2A C 0.6925(5) 0.0935(5) -0.0659(4) 0.0221(15) Uani 1 1 d . U . C 3
N3A N 0.4663(4) -0.0349(4) 0.1563(3) 0.0199(12) Uani 1 1 d . . . C 3
C4A C 0.8709(6) 0.0768(7) -0.0560(5) 0.038(2) Uani 1 1 d . U . C 3
H4AA H 0.9338 0.0599 -0.0799 0.058 Uiso 1 1 calc R U . C 3
H4AB H 0.8848 0.0313 -0.0164 0.058 Uiso 1 1 calc R U . C 3
H4AC H 0.8431 0.1446 -0.0431 0.058 Uiso 1 1 calc R U . C 3
N4A N 0.6500(4) -0.1090(4) 0.0872(3) 0.0182(12) Uani 1 1 d . . . C 3
C5A C 0.6047(6) 0.1825(5) -0.0681(4) 0.0223(15) Uani 1 1 d . U . C 3
C6A C 0.5839(6) 0.2795(5) -0.1085(4) 0.0269(16) Uani 1 1 d . U . C 3
H6AA H 0.5116 0.3149 -0.1224 0.032 Uiso 1 1 calc R U . C 3
H6AB H 0.6250 0.2642 -0.1489 0.032 Uiso 1 1 calc R U . C 3
C7A C 0.6096(8) 0.3470(6) -0.0677(5) 0.042(2) Uani 1 1 d . U . C 3
H7AA H 0.6049 0.4034 -0.0966 0.062 Uiso 1 1 calc R U . C 3
H7AB H 0.6785 0.3094 -0.0493 0.062 Uiso 1 1 calc R U . C 3
H7AC H 0.5617 0.3709 -0.0316 0.062 Uiso 1 1 calc R U . C 3
C8A C 0.5361(6) 0.1701(5) -0.0206(4) 0.0216(15) Uani 1 1 d . U . C 3
C9A C 0.4397(6) 0.2451(5) -0.0070(4) 0.0222(15) Uani 1 1 d . U . C 3
H9A H 0.4165 0.3068 -0.0321 0.027 Uiso 1 1 calc R U . C 3
C10A C 0.3756(5) 0.2355(5) 0.0407(4) 0.0218(15) Uani 1 1 d . U . C 3
C11A C 0.2757(6) 0.3165(5) 0.0551(4) 0.0252(15) Uani 1 1 d . U . C 3
C12A C 0.2300(6) 0.4208(5) 0.0205(5) 0.0310(18) Uani 1 1 d . U . C 3
H12A H 0.1557 0.4530 0.0256 0.037 Uiso 1 1 calc R U . C 3
H12B H 0.2439 0.4162 -0.0274 0.037 Uiso 1 1 calc R U . C 3
C13A C 0.2730(7) 0.4863(6) 0.0486(5) 0.040(2) Uani 1 1 d . U . C 3
H13A H 0.2404 0.5523 0.0254 0.060 Uiso 1 1 calc R U . C 3
H13B H 0.3462 0.4563 0.0420 0.060 Uiso 1 1 calc R U . C 3
H13C H 0.2592 0.4914 0.0960 0.060 Uiso 1 1 calc R U . C 3
C14A C 0.2359(6) 0.2796(5) 0.1057(4) 0.0287(16) Uani 1 1 d . U . C 3
C15A C 0.1359(6) 0.3315(6) 0.1415(5) 0.037(2) Uani 1 1 d . U . C 3
H15A H 0.1050 0.2865 0.1474 0.045 Uiso 1 1 calc R U . C 3
H15B H 0.0890 0.3906 0.1136 0.045 Uiso 1 1 calc R U . C 3
C16A C 0.1482(8) 0.3635(7) 0.2104(6) 0.048(2) Uani 1 1 d . U . C 3
H16A H 0.0817 0.3975 0.2304 0.073 Uiso 1 1 calc R U . C 3
H16B H 0.1786 0.4081 0.2050 0.073 Uiso 1 1 calc R U . C 3
H16C H 0.1920 0.3050 0.2391 0.073 Uiso 1 1 calc R U . C 3
C17A C 0.2996(6) 0.1120(5) 0.1710(4) 0.0253(15) Uani 1 1 d . U . C 3
H17A H 0.2384 0.1371 0.1949 0.030 Uiso 1 1 calc R U . C 3
C18A C 0.3725(6) 0.0146(5) 0.1870(4) 0.0220(14) Uani 1 1 d . U . C 3
C19A C 0.3603(6) -0.0495(5) 0.2414(4) 0.0251(15) Uani 1 1 d . U . C 3
C20A C 0.2711(7) -0.0155(6) 0.2869(5) 0.039(2) Uani 1 1 d . U . C 3
H20A H 0.2710 -0.0743 0.3108 0.047 Uiso 1 1 calc R U . C 3
H20B H 0.2081 0.0186 0.2597 0.047 Uiso 1 1 calc R U . C 3
C21A C 0.2701(9) 0.0541(7) 0.3381(5) 0.052(3) Uani 1 1 d . U . C 3
H21A H 0.2119 0.0702 0.3669 0.078 Uiso 1 1 calc R U . C 3
H21B H 0.2650 0.1149 0.3150 0.078 Uiso 1 1 calc R U . C 3
H21C H 0.3327 0.0216 0.3649 0.078 Uiso 1 1 calc R U . C 3
C22A C 0.4475(6) -0.1389(5) 0.2420(4) 0.0238(15) Uani 1 1 d . U . C 3
C23A C 0.4760(6) -0.2312(5) 0.2896(4) 0.0299(17) Uani 1 1 d . U . C 3
H23A H 0.5063 -0.2903 0.2640 0.036 Uiso 1 1 calc R U . C 3
H23B H 0.4138 -0.2278 0.3100 0.036 Uiso 1 1 calc R U . C 3
C24A C 0.5521(7) -0.2427(6) 0.3455(4) 0.037(2) Uani 1 1 d . U . C 3
H24A H 0.5631 -0.2995 0.3762 0.056 Uiso 1 1 calc R U . C 3
H24B H 0.5244 -0.1828 0.3694 0.056 Uiso 1 1 calc R U . C 3
H24C H 0.6165 -0.2532 0.3259 0.056 Uiso 1 1 calc R U . C 3
C25A C 0.5119(5) -0.1289(5) 0.1895(4) 0.0201(14) Uani 1 1 d . U . C 3
C26A C 0.6743(5) -0.1950(5) 0.1296(4) 0.0222(15) Uani 1 1 d . U . C 3
C27A C 0.7771(6) -0.2729(5) 0.1186(4) 0.0253(16) Uani 1 1 d . U . C 3
C28A C 0.8267(6) -0.3742(5) 0.1572(5) 0.0317(18) Uani 1 1 d . U . C 3
H28A H 0.8826 -0.4208 0.1309 0.038 Uiso 1 1 calc R U . C 3
H28B H 0.7762 -0.3990 0.1631 0.038 Uiso 1 1 calc R U . C 3
C29A C 0.8697(7) -0.3725(6) 0.2267(5) 0.042(2) Uani 1 1 d . U . C 3
H29A H 0.9026 -0.4396 0.2482 0.063 Uiso 1 1 calc R U . C 3
H29B H 0.8142 -0.3297 0.2540 0.063 Uiso 1 1 calc R U . C 3
H29C H 0.9191 -0.3473 0.2213 0.063 Uiso 1 1 calc R U . C 3
C30A C 0.7376(5) -0.1338(5) 0.0494(4) 0.0234(15) Uani 1 1 d . U . C 3
C31A C 0.7495(6) -0.0701(5) 0.0002(4) 0.0244(15) Uani 1 1 d . U . C 3
H31A H 0.8115 -0.0941 -0.0227 0.029 Uiso 1 1 calc R U . C 3
C32A C 0.8169(6) -0.2356(5) 0.0681(4) 0.0287(17) Uani 1 1 d . U . C 3
C33A C 0.6079(6) -0.2044(5) 0.1768(4) 0.0214(14) Uani 1 1 d . U . C 3
H33A H 0.6299 -0.2662 0.2017 0.026 Uiso 1 1 calc R U . C 3
C35A C 0.3120(6) 0.1759(5) 0.1208(4) 0.0237(15) Uani 1 1 d . U . C 3
C36A C 0.9948(7) -0.2455(7) 0.0650(6) 0.048(2) Uani 1 1 d . U . C 3
H36A H 1.0622 -0.2826 0.0467 0.072 Uiso 1 1 calc R U . C 3
H36B H 0.9991 -0.2555 0.1134 0.072 Uiso 1 1 calc R U . C 3
H36C H 0.9688 -0.1751 0.0515 0.072 Uiso 1 1 calc R U . C 3
C34A C 0.9215(6) -0.2829(6) 0.0382(5) 0.0326(18) Uani 1 1 d . U . C 3
H34A H 0.9144 -0.2689 -0.0105 0.039 Uiso 1 1 calc R U . C 3
H34B H 0.9521 -0.3554 0.0478 0.039 Uiso 1 1 calc R U . C 3
C3A C 0.7921(6) 0.0681(6) -0.1022(4) 0.0295(17) Uani 1 1 d . U . C 3
H3AA H 0.7785 0.1136 -0.1424 0.035 Uiso 1 1 calc R U . C 3
H3AB H 0.8208 -0.0001 -0.1160 0.035 Uiso 1 1 calc R U . C 3
N1A N 0.5800(5) 0.0739(4) 0.0111(3) 0.0225(13) Uani 1 1 d . . . C 3
C1B C 0.8085(7) 0.3076(7) -0.2139(6) 0.047(2) Uani 1 1 d . U . D 4
H1B H 0.8044 0.2906 -0.1683 0.057 Uiso 1 1 calc R U . D 4
C6B C 0.7732(7) 0.2708(8) -0.2647(6) 0.054(3) Uani 1 1 d . U . D 4
H6B H 0.7444 0.2287 -0.2509 0.065 Uiso 1 1 calc R U . D 4
C5B C 0.7772(7) 0.2912(7) -0.3331(6) 0.049(2) Uani 1 1 d . U . D 4
H5B H 0.7530 0.2643 -0.3649 0.059 Uiso 1 1 calc R U . D 4
C4B C 0.8213(9) 0.3567(8) -0.3516(7) 0.064(3) Uani 1 1 d . U . D 4
H4B H 0.8264 0.3733 -0.3972 0.076 Uiso 1 1 calc R U . D 4
C3B C 0.8569(9) 0.3963(8) -0.3031(7) 0.064(3) Uani 1 1 d . U . D 4
H3B H 0.8849 0.4392 -0.3160 0.076 Uiso 1 1 calc R U . D 4
C2B C 0.8498(8) 0.3708(8) -0.2357(7) 0.061(3) Uani 1 1 d . U . D 4
H2B H 0.8738 0.3973 -0.2035 0.073 Uiso 1 1 calc R U . D 4


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu2 1.204(7) . ?
Lu1 Lu3 1.4003(18) . ?
Lu1 Lu6 1.41(3) . ?
Lu1 C1E 2.218(11) . ?
Lu1 Lu4 2.5790(17) . ?
Lu1 C2E 2.648(14) . ?
Lu1 Lu5 2.86(4) . ?
Lu1 Lu13 3.096(18) . ?
Lu1 Lu8 3.395(2) . ?
Lu1 Lu7 3.58(3) . ?
Lu2 Lu3 1.171(6) . ?
Lu2 Lu6 1.74(3) . ?
Lu2 C1E 1.871(13) . ?
Lu2 Lu4 2.146(5) . ?
Lu2 C2E 2.463(16) . ?
Lu2 Lu5 2.93(3) . ?
Lu2 Lu7 3.22(4) . ?
Lu2 Lu13 3.437(18) . ?
Lu2 Lu8 3.648(6) . ?
Lu2 Lu12 3.836(17) . ?
Lu3 Lu6 0.79(3) . ?
Lu3 Lu4 1.3352(19) . ?
Lu3 Lu5 2.08(4) . ?
Lu3 C1E 2.339(12) . ?
Lu3 C2E 2.392(16) . ?
Lu3 Lu7 2.64(4) . ?
Lu3 Lu13 3.859(16) . ?
Lu4 Lu5 1.36(3) . ?
Lu4 Lu7 1.45(4) . ?
Lu4 Lu6 1.50(3) . ?
Lu4 C2E 2.020(16) . ?
Lu4 C1E 2.465(11) . ?
Lu5 Lu7 1.33(4) . ?
Lu5 Lu6 1.65(5) . ?
Lu5 C2E 1.83(3) . ?
Lu5 C1E 2.68(2) . ?
Lu5 Lu10 3.53(3) . ?
Lu5 Lu11 3.63(3) . ?
Lu5 Lu13 3.80(3) . ?
Lu6 C2E 2.29(4) . ?
Lu6 C1E 2.46(3) . ?
Lu6 Lu7 2.57(5) . ?
Lu6 Lu13 3.65(3) . ?
Lu7 C2E 1.70(2) . ?
Lu7 C1E 2.61(3) . ?
Lu7 Lu11 3.09(3) . ?
Lu7 Lu10 3.53(3) . ?
Lu7 Lu9 3.86(2) . ?
Lu8 Lu9 1.114(3) . ?
Lu8 Lu12 1.335(18) . ?
Lu8 Lu10 1.816(6) . ?
Lu8 C1E 2.182(11) . ?
Lu8 Lu11 2.424(2) . ?
Lu8 C2E 2.609(13) . ?
Lu9 Lu12 0.89(2) . ?
Lu9 Lu10 1.055(6) . ?
Lu9 Lu13 1.274(19) . ?
Lu9 Lu11 1.410(2) . ?
Lu9 C1E 2.263(12) . ?
Lu9 C2E 2.348(15) . ?
Lu10 Lu11 1.512(6) . ?
Lu10 Lu13 1.76(2) . ?
Lu10 Lu12 1.90(2) . ?
Lu10 C2E 2.278(17) . ?
Lu10 C1E 2.650(12) . ?
Lu11 Lu12 1.564(19) . ?
Lu11 C2E 2.056(16) . ?
Lu11 C1E 2.360(11) . ?
Lu11 Lu13 2.499(18) . ?
Lu12 Lu13 1.61(2) . ?
Lu12 C1E 2.078(19) . ?
Lu12 C2E 2.49(2) . ?
Lu13 C1E 2.046(19) . ?
Lu13 C2E 2.405(18) . ?
C1E C2E 1.114(14) . ?
C1 C18 1.36(3) . ?
C1 C5 1.52(2) . ?
C1 C2 1.54(2) . ?
C2 C3 1.408(17) . ?
C2 C15 1.42(2) . ?
C3 C12 1.405(16) . ?
C3 C4 1.444(16) . ?
C4 C9 1.431(16) . ?
C4 C5 1.47(2) . ?
C5 C6 1.35(2) . ?
C6 C7 1.32(2) . ?
C6 C20 1.51(2) . ?
C7 C23 1.50(2) . ?
C7 C8 1.51(2) . ?
C8 C25 1.428(17) . ?
C8 C9 1.43(2) . ?
C9 C10 1.434(19) . ?
C10 C11 1.427(17) . ?
C10 C27 1.440(16) . ?
C11 C29 1.422(19) . ?
C11 C12 1.434(15) . ?
C12 C13 1.427(16) . ?
C13 C31 1.417(17) . ?
C13 C14 1.425(17) . ?
C14 C15 1.35(2) . ?
C14 C33 1.606(17) . ?
C15 C16 1.468(19) . ?
C16 C17 1.43(2) . ?
C16 C53 1.49(2) . ?
C17 C18 1.29(3) . ?
C17 C51 1.64(3) . ?
C18 C19 1.41(3) . ?
C19 C49 1.45(2) . ?
C19 C20 1.56(2) . ?
C20 C21 1.417(19) . ?
C21 C47 1.38(3) . ?
C21 C22 1.50(2) . ?
C22 C44 1.28(2) . ?
C22 C23 1.40(2) . ?
C23 C24 1.423(18) . ?
C24 C42 1.362(19) . ?
C24 C25 1.48(2) . ?
C25 C26 1.397(19) . ?
C26 C27 1.454(17) . ?
C26 C40 1.46(2) . ?
C27 C28 1.44(2) . ?
C28 C38 1.32(2) . ?
C28 C29 1.624(16) . ?
C29 C30 1.28(2) . ?
C30 C31 1.36(2) . ?
C30 C36 1.47(2) . ?
C31 C32 1.633(16) . ?
C32 C34 1.28(3) . ?
C32 C33 1.63(2) . ?
C33 C85 1.24(2) . ?
C34 C35 1.54(3) . ?
C34 C81 1.56(3) . ?
C35 C76 1.32(2) . ?
C35 C36 1.41(3) . ?
C36 C37 1.42(3) . ?
C37 C75 1.45(3) . ?
C37 C38 1.48(3) . ?
C38 C39 1.29(2) . ?
C39 C40 1.45(2) . ?
C39 C54 1.63(2) . ?
C40 C41 1.386(19) . ?
C41 C55 1.42(2) . ?
C41 C42 1.441(18) . ?
C42 C43 1.416(19) . ?
C43 C44 1.402(19) . ?
C43 C57 1.47(2) . ?
C44 C45 1.621(16) . ?
C45 C46 1.30(2) . ?
C45 C58 1.464(19) . ?
C46 C63 1.25(3) . ?
C46 C47 1.49(3) . ?
C47 C48 1.22(3) . ?
C48 C49 1.362(17) . ?
C48 C64 1.382(17) . ?
C49 C50 1.407(16) . ?
C49 C51 1.98(3) . ?
C50 C51 1.23(3) . ?
C50 C66 1.401(17) . ?
C51 C52 1.56(3) . ?
C52 C68 1.372(17) . ?
C52 C53 1.430(17) . ?
C53 C85 1.414(18) . ?
C54 C55 1.395(19) . ?
C54 C71 1.39(3) . ?
C55 C56 1.46(2) . ?
C56 C57 1.379(18) . ?
C56 C61 1.39(2) . ?
C57 C58 1.44(2) . ?
C58 C59 1.444(18) . ?
C59 C60 1.407(19) . ?
C59 C62 1.43(2) . ?
C60 C73 1.424(18) . ?
C60 C61 1.44(2) . ?
C61 C72 1.47(2) . ?
C62 C69 1.45(2) . ?
C62 C63 1.49(3) . ?
C63 C65 1.59(2) . ?
C64 C66 1.378(18) . ?
C64 C65 1.551(19) . ?
C65 C70 1.25(3) . ?
C65 C66 2.03(3) . ?
C66 C67 1.47(3) . ?
C67 C68 1.24(3) . ?
C67 C83 1.53(3) . ?
C67 C82 1.90(4) . ?
C68 C82 1.391(19) . ?
C69 C74 1.43(2) . ?
C69 C70 1.52(2) . ?
C70 C83 1.32(3) . ?
C71 C72 1.27(3) . ?
C71 C75 1.50(3) . ?
C72 C78 1.613(18) . ?
C73 C74 1.45(2) . ?
C73 C78 1.47(3) . ?
C74 C80 1.45(2) . ?
C75 C76 1.38(3) . ?
C76 C77 1.610(17) . ?
C77 C78 1.37(2) . ?
C77 C79 1.578(17) . ?
C79 C80 1.29(3) . ?
C79 C81 1.41(2) . ?
C80 C84 1.61(4) . ?
C81 C86 1.617(17) . ?
C82 C86 1.361(18) . ?
C82 C84 1.49(3) . ?
C82 C83 1.98(3) . ?
C83 C84 1.27(4) . ?
C85 C86 1.370(17) . ?
Ni1A N1A 1.957(6) . ?
Ni1A N4A 1.959(6) . ?
Ni1A N3A 1.960(6) . ?
Ni1A N2A 1.964(6) . ?
C1A N1A 1.366(10) . ?
C1A C31A 1.374(10) . ?
C1A C2A 1.443(9) . ?
N2A C35A 1.357(10) . ?
N2A C10A 1.387(8) . ?
C2A C5A 1.356(10) . ?
C2A C3A 1.507(11) . ?
N3A C25A 1.367(8) . ?
N3A C18A 1.378(10) . ?
C4A C3A 1.541(11) . ?
N4A C30A 1.381(10) . ?
N4A C26A 1.386(8) . ?
C5A C8A 1.429(10) . ?
C5A C6A 1.507(9) . ?
C6A C7A 1.521(11) . ?
C8A C9A 1.374(11) . ?
C8A N1A 1.382(8) . ?
C9A C10A 1.367(11) . ?
C10A C11A 1.444(10) . ?
C11A C14A 1.358(11) . ?
C11A C12A 1.501(9) . ?
C12A C13A 1.529(11) . ?
C14A C35A 1.445(10) . ?
C14A C15A 1.497(12) . ?
C15A C16A 1.523(14) . ?
C17A C18A 1.369(10) . ?
C17A C35A 1.398(10) . ?
C18A C19A 1.454(9) . ?
C19A C22A 1.356(11) . ?
C19A C20A 1.479(12) . ?
C20A C21A 1.508(14) . ?
C22A C25A 1.438(10) . ?
C22A C23A 1.504(9) . ?
C23A C24A 1.527(12) . ?
C25A C33A 1.369(10) . ?
C26A C33A 1.383(11) . ?
C26A C27A 1.439(10) . ?
C27A C32A 1.360(11) . ?
C27A C28A 1.498(9) . ?
C28A C29A 1.532(13) . ?
C30A C31A 1.379(10) . ?
C30A C32A 1.451(9) . ?
C32A C34A 1.489(11) . ?
C36A C34A 1.538(12) . ?
C1B C2B 1.381(16) . ?
C1B C6B 1.398(15) . ?
C6B C5B 1.377(16) . ?
C5B C4B 1.427(16) . ?
C4B C3B 1.395(18) . ?
C3B C2B 1.379(18) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu2 Lu1 Lu3 52.8(2) . . ?
Lu2 Lu1 Lu6 83.0(12) . . ?
Lu3 Lu1 Lu6 32.5(12) . . ?
Lu2 Lu1 C1E 57.5(4) . . ?
Lu3 Lu1 C1E 76.9(3) . . ?
Lu6 Lu1 C1E 82.2(14) . . ?
Lu2 Lu1 Lu4 55.7(2) . . ?
Lu3 Lu1 Lu4 18.99(7) . . ?
Lu6 Lu1 Lu4 28.8(11) . . ?
C1E Lu1 Lu4 61.3(3) . . ?
Lu2 Lu1 C2E 67.9(4) . . ?
Lu3 Lu1 C2E 64.0(3) . . ?
Lu6 Lu1 C2E 59.8(14) . . ?
C1E Lu1 C2E 24.5(3) . . ?
Lu4 Lu1 C2E 45.4(3) . . ?
Lu2 Lu1 Lu5 81.5(6) . . ?
Lu3 Lu1 Lu5 43.4(7) . . ?
Lu6 Lu1 Lu5 22.6(16) . . ?
C1E Lu1 Lu5 62.3(7) . . ?
Lu4 Lu1 Lu5 28.3(6) . . ?
C2E Lu1 Lu5 38.5(7) . . ?
Lu2 Lu1 Lu13 96.0(4) . . ?
Lu3 Lu1 Lu13 112.7(3) . . ?
Lu6 Lu1 Lu13 101.5(15) . . ?
C1E Lu1 Lu13 41.3(4) . . ?
Lu4 Lu1 Lu13 94.1(3) . . ?
C2E Lu1 Lu13 48.7(4) . . ?
Lu5 Lu1 Lu13 79.3(8) . . ?
Lu2 Lu1 Lu8 92.3(3) . . ?
Lu3 Lu1 Lu8 112.87(9) . . ?
Lu6 Lu1 Lu8 104.2(14) . . ?
C1E Lu1 Lu8 39.1(3) . . ?
Lu4 Lu1 Lu8 94.67(6) . . ?
C2E Lu1 Lu8 49.3(3) . . ?
Lu5 Lu1 Lu8 81.8(7) . . ?
Lu13 Lu1 Lu8 4.9(4) . . ?
Lu2 Lu1 Lu7 63.2(7) . . ?
Lu3 Lu1 Lu7 38.8(5) . . ?
Lu6 Lu1 Lu7 35.8(14) . . ?
C1E Lu1 Lu7 46.6(5) . . ?
Lu4 Lu1 Lu7 19.8(5) . . ?
C2E Lu1 Lu7 26.6(5) . . ?
Lu5 Lu1 Lu7 20.1(7) . . ?
Lu13 Lu1 Lu7 74.7(6) . . ?
Lu8 Lu1 Lu7 75.7(5) . . ?
Lu3 Lu2 Lu1 72.2(4) . . ?
Lu3 Lu2 Lu6 22.0(10) . . ?
Lu1 Lu2 Lu6 53.6(11) . . ?
Lu3 Lu2 C1E 97.9(5) . . ?
Lu1 Lu2 C1E 89.6(5) . . ?
Lu6 Lu2 C1E 85.9(12) . . ?
Lu3 Lu2 Lu4 33.45(16) . . ?
Lu1 Lu2 Lu4 96.6(3) . . ?
Lu6 Lu2 Lu4 44.0(11) . . ?
C1E Lu2 Lu4 75.4(4) . . ?
Lu3 Lu2 C2E 72.7(4) . . ?
Lu1 Lu2 C2E 85.1(4) . . ?
Lu6 Lu2 C2E 63.3(13) . . ?
C1E Lu2 C2E 25.4(4) . . ?
Lu4 Lu2 C2E 51.4(3) . . ?
Lu3 Lu2 Lu5 34.4(7) . . ?
Lu1 Lu2 Lu5 74.5(7) . . ?
Lu6 Lu2 Lu5 29.1(14) . . ?
C1E Lu2 Lu5 63.5(8) . . ?
Lu4 Lu2 Lu5 25.5(6) . . ?
C2E Lu2 Lu5 38.3(8) . . ?
Lu3 Lu2 Lu7 50.7(6) . . ?
Lu1 Lu2 Lu7 97.3(7) . . ?
Lu6 Lu2 Lu7 52.7(14) . . ?
C1E Lu2 Lu7 54.2(6) . . ?
Lu4 Lu2 Lu7 21.3(5) . . ?
C2E Lu2 Lu7 31.2(6) . . ?
Lu5 Lu2 Lu7 24.4(8) . . ?
Lu3 Lu2 Lu13 102.3(5) . . ?
Lu1 Lu2 Lu13 63.6(4) . . ?
Lu6 Lu2 Lu13 82.7(11) . . ?
C1E Lu2 Lu13 30.1(4) . . ?
Lu4 Lu2 Lu13 93.7(4) . . ?
C2E Lu2 Lu13 44.4(4) . . ?
Lu5 Lu2 Lu13 72.8(7) . . ?
Lu7 Lu2 Lu13 75.3(6) . . ?
Lu3 Lu2 Lu8 107.1(3) . . ?
Lu1 Lu2 Lu8 68.4(2) . . ?
Lu6 Lu2 Lu8 87.9(11) . . ?
C1E Lu2 Lu8 28.1(3) . . ?
Lu4 Lu2 Lu8 96.21(18) . . ?
C2E Lu2 Lu8 45.6(3) . . ?
Lu5 Lu2 Lu8 76.5(7) . . ?
Lu7 Lu2 Lu8 76.8(5) . . ?
Lu13 Lu2 Lu8 5.6(4) . . ?
Lu3 Lu2 Lu12 111.2(4) . . ?
Lu1 Lu2 Lu12 88.3(4) . . ?
Lu6 Lu2 Lu12 96.8(12) . . ?
C1E Lu2 Lu12 14.5(4) . . ?
Lu4 Lu2 Lu12 89.9(3) . . ?
C2E Lu2 Lu12 39.5(4) . . ?
Lu5 Lu2 Lu12 77.0(8) . . ?
Lu7 Lu2 Lu12 68.7(6) . . ?
Lu13 Lu2 Lu12 24.8(4) . . ?
Lu8 Lu2 Lu12 20.4(3) . . ?
Lu6 Lu3 Lu2 124(2) . . ?
Lu6 Lu3 Lu4 86(3) . . ?
Lu2 Lu3 Lu4 117.6(3) . . ?
Lu6 Lu3 Lu1 74(2) . . ?
Lu2 Lu3 Lu1 55.0(3) . . ?
Lu4 Lu3 Lu1 141.05(13) . . ?
Lu6 Lu3 Lu5 47(3) . . ?
Lu2 Lu3 Lu5 127.0(8) . . ?
Lu4 Lu3 Lu5 40.0(9) . . ?
Lu1 Lu3 Lu5 109.0(9) . . ?
Lu6 Lu3 C1E 90(2) . . ?
Lu2 Lu3 C1E 52.4(4) . . ?
Lu4 Lu3 C1E 79.1(3) . . ?
Lu1 Lu3 C1E 67.4(3) . . ?
Lu5 Lu3 C1E 74.6(8) . . ?
Lu6 Lu3 C2E 73(2) . . ?
Lu2 Lu3 C2E 79.4(4) . . ?
Lu4 Lu3 C2E 57.6(3) . . ?
Lu1 Lu3 C2E 84.2(3) . . ?
Lu5 Lu3 C2E 47.6(8) . . ?
C1E Lu3 C2E 27.2(3) . . ?
Lu6 Lu3 Lu7 76(3) . . ?
Lu2 Lu3 Lu7 109.3(7) . . ?
Lu4 Lu3 Lu7 19.3(6) . . ?
Lu1 Lu3 Lu7 121.8(6) . . ?
Lu5 Lu3 Lu7 29.9(10) . . ?
C1E Lu3 Lu7 63.0(6) . . ?
C2E Lu3 Lu7 39.0(6) . . ?
Lu6 Lu3 Lu13 69(2) . . ?
Lu2 Lu3 Lu13 60.5(5) . . ?
Lu4 Lu3 Lu13 93.9(3) . . ?
Lu1 Lu3 Lu13 47.7(3) . . ?
Lu5 Lu3 Lu13 72.8(9) . . ?
C1E Lu3 Lu13 26.3(4) . . ?
C2E Lu3 Lu13 36.5(4) . . ?
Lu7 Lu3 Lu13 74.9(6) . . ?
Lu3 Lu4 Lu5 100.8(17) . . ?
Lu3 Lu4 Lu7 143.0(9) . . ?
Lu5 Lu4 Lu7 57(2) . . ?
Lu3 Lu4 Lu6 31.4(12) . . ?
Lu5 Lu4 Lu6 70(2) . . ?
Lu7 Lu4 Lu6 121.2(18) . . ?
Lu3 Lu4 C2E 88.5(3) . . ?
Lu5 Lu4 C2E 61.8(11) . . ?
Lu7 Lu4 C2E 55.7(9) . . ?
Lu6 Lu4 C2E 79.6(12) . . ?
Lu3 Lu4 Lu2 28.91(17) . . ?
Lu5 Lu4 Lu2 111.7(14) . . ?
Lu7 Lu4 Lu2 126.3(10) . . ?
Lu6 Lu4 Lu2 53.5(10) . . ?
C2E Lu4 Lu2 72.4(4) . . ?
Lu3 Lu4 C1E 68.7(3) . . ?
Lu5 Lu4 C1E 83.8(10) . . ?
Lu7 Lu4 C1E 79.2(10) . . ?
Lu6 Lu4 C1E 72.1(10) . . ?
C2E Lu4 C1E 26.5(4) . . ?
Lu2 Lu4 C1E 47.2(3) . . ?
Lu3 Lu4 Lu1 19.96(7) . . ?
Lu5 Lu4 Lu1 87.3(16) . . ?
Lu7 Lu4 Lu1 123.0(9) . . ?
Lu6 Lu4 Lu1 26.8(9) . . ?
C2E Lu4 Lu1 69.1(3) . . ?
Lu2 Lu4 Lu1 27.63(18) . . ?
C1E Lu4 Lu1 52.1(2) . . ?
Lu7 Lu5 Lu4 65(2) . . ?
Lu7 Lu5 Lu6 119(3) . . ?
Lu4 Lu5 Lu6 59.2(18) . . ?
Lu7 Lu5 C2E 62.7(15) . . ?
Lu4 Lu5 C2E 77.2(10) . . ?
Lu6 Lu5 C2E 82.4(14) . . ?
Lu7 Lu5 Lu3 99(2) . . ?
Lu4 Lu5 Lu3 39.2(11) . . ?
Lu6 Lu5 Lu3 20.5(10) . . ?
C2E Lu5 Lu3 75.4(10) . . ?
Lu7 Lu5 C1E 72.6(15) . . ?
Lu4 Lu5 C1E 66.0(8) . . ?
Lu6 Lu5 C1E 64.2(11) . . ?
C2E Lu5 C1E 18.5(7) . . ?
Lu3 Lu5 C1E 57.2(6) . . ?
Lu7 Lu5 Lu1 112(2) . . ?
Lu4 Lu5 Lu1 64.4(14) . . ?
Lu6 Lu5 Lu1 19.2(10) . . ?
C2E Lu5 Lu1 64.5(10) . . ?
Lu3 Lu5 Lu1 27.6(5) . . ?
C1E Lu5 Lu1 47.1(5) . . ?
Lu7 Lu5 Lu2 90(2) . . ?
Lu4 Lu5 Lu2 42.8(10) . . ?
Lu6 Lu5 Lu2 30.9(9) . . ?
C2E Lu5 Lu2 56.8(9) . . ?
Lu3 Lu5 Lu2 18.6(2) . . ?
C1E Lu5 Lu2 38.6(5) . . ?
Lu1 Lu5 Lu2 24.0(3) . . ?
Lu7 Lu5 Lu10 79.2(19) . . ?
Lu4 Lu5 Lu10 111.8(11) . . ?
Lu6 Lu5 Lu10 99.6(14) . . ?
C2E Lu5 Lu10 34.6(9) . . ?
Lu3 Lu5 Lu10 101.9(8) . . ?
C1E Lu5 Lu10 48.1(5) . . ?
Lu1 Lu5 Lu10 80.6(6) . . ?
Lu2 Lu5 Lu10 84.4(6) . . ?
Lu7 Lu5 Lu11 56.0(16) . . ?
Lu4 Lu5 Lu11 93.0(11) . . ?
Lu6 Lu5 Lu11 103.7(12) . . ?
C2E Lu5 Lu11 22.1(9) . . ?
Lu3 Lu5 Lu11 97.4(6) . . ?
C1E Lu5 Lu11 40.5(5) . . ?
Lu1 Lu5 Lu11 85.2(5) . . ?
Lu2 Lu5 Lu11 78.8(5) . . ?
Lu10 Lu5 Lu11 24.3(2) . . ?
Lu7 Lu5 Lu13 91.9(16) . . ?
Lu4 Lu5 Lu13 96.0(11) . . ?
Lu6 Lu5 Lu13 72.1(13) . . ?
C2E Lu5 Lu13 30.1(8) . . ?
Lu3 Lu5 Lu13 75.8(8) . . ?
C1E Lu5 Lu13 31.1(5) . . ?
Lu1 Lu5 Lu13 53.1(5) . . ?
Lu2 Lu5 Lu13 59.7(6) . . ?
Lu10 Lu5 Lu13 27.5(4) . . ?
Lu11 Lu5 Lu13 39.2(4) . . ?
Lu3 Lu6 Lu1 73(2) . . ?
Lu3 Lu6 Lu4 62(2) . . ?
Lu1 Lu6 Lu4 124.4(17) . . ?
Lu3 Lu6 Lu5 112(3) . . ?
Lu1 Lu6 Lu5 138(2) . . ?
Lu4 Lu6 Lu5 50.8(16) . . ?
Lu3 Lu6 Lu2 33.9(13) . . ?
Lu1 Lu6 Lu2 43.4(8) . . ?
Lu4 Lu6 Lu2 82.5(12) . . ?
Lu5 Lu6 Lu2 120(2) . . ?
Lu3 Lu6 C2E 88(2) . . ?
Lu1 Lu6 C2E 88.1(13) . . ?
Lu4 Lu6 C2E 60.2(12) . . ?
Lu5 Lu6 C2E 52.2(14) . . ?
Lu2 Lu6 C2E 74.0(10) . . ?
Lu3 Lu6 C1E 71.8(18) . . ?
Lu1 Lu6 C1E 63.2(9) . . ?
Lu4 Lu6 C1E 72.3(11) . . ?
Lu5 Lu6 C1E 78.8(16) . . ?
Lu2 Lu6 C1E 49.3(7) . . ?
C2E Lu6 C1E 26.8(5) . . ?
Lu3 Lu6 Lu7 86(3) . . ?
Lu1 Lu6 Lu7 125.5(17) . . ?
Lu4 Lu6 Lu7 28.8(11) . . ?
Lu5 Lu6 Lu7 26.9(13) . . ?
Lu2 Lu6 Lu7 94.7(15) . . ?
C2E Lu6 Lu7 40.3(9) . . ?
C1E Lu6 Lu7 62.5(10) . . ?
Lu3 Lu6 Lu13 99.7(19) . . ?
Lu1 Lu6 Lu13 56.3(11) . . ?
Lu4 Lu6 Lu13 99.5(14) . . ?
Lu5 Lu6 Lu13 82.5(16) . . ?
Lu2 Lu6 Lu13 69.1(9) . . ?
C2E Lu6 Lu13 40.1(6) . . ?
C1E Lu6 Lu13 32.3(5) . . ?
Lu7 Lu6 Lu13 79.7(10) . . ?
Lu5 Lu7 Lu4 58(2) . . ?
Lu5 Lu7 C2E 73.0(16) . . ?
Lu4 Lu7 C2E 79.4(16) . . ?
Lu5 Lu7 Lu6 33.9(19) . . ?
Lu4 Lu7 Lu6 30.0(10) . . ?
C2E Lu7 Lu6 60.8(12) . . ?
Lu5 Lu7 C1E 78.3(16) . . ?
Lu4 Lu7 C1E 67.8(11) . . ?
C2E Lu7 C1E 17.2(8) . . ?
Lu6 Lu7 C1E 56.6(9) . . ?
Lu5 Lu7 Lu3 51(2) . . ?
Lu4 Lu7 Lu3 17.7(5) . . ?
C2E Lu7 Lu3 62.5(12) . . ?
Lu6 Lu7 Lu3 17.3(7) . . ?
C1E Lu7 Lu3 52.8(7) . . ?
Lu5 Lu7 Lu11 103.1(18) . . ?
Lu4 Lu7 Lu11 115.8(13) . . ?
C2E Lu7 Lu11 38.6(9) . . ?
Lu6 Lu7 Lu11 99.3(9) . . ?
C1E Lu7 Lu11 48.0(5) . . ?
Lu3 Lu7 Lu11 100.2(8) . . ?
Lu5 Lu7 Lu2 65(2) . . ?
Lu4 Lu7 Lu2 32.5(7) . . ?
C2E Lu7 Lu2 48.8(11) . . ?
Lu6 Lu7 Lu2 32.5(7) . . ?
C1E Lu7 Lu2 35.5(5) . . ?
Lu3 Lu7 Lu2 20.1(3) . . ?
Lu11 Lu7 Lu2 83.4(6) . . ?
Lu5 Lu7 Lu10 79.0(18) . . ?
Lu4 Lu7 Lu10 108.7(11) . . ?
C2E Lu7 Lu10 31.9(10) . . ?
Lu6 Lu7 Lu10 83.7(9) . . ?
C1E Lu7 Lu10 48.3(5) . . ?
Lu3 Lu7 Lu10 91.0(6) . . ?
Lu11 Lu7 Lu10 25.3(2) . . ?
Lu2 Lu7 Lu10 80.3(5) . . ?
Lu5 Lu7 Lu1 47.5(18) . . ?
Lu4 Lu7 Lu1 37.1(7) . . ?
C2E Lu7 Lu1 44.3(10) . . ?
Lu6 Lu7 Lu1 18.7(6) . . ?
C1E Lu7 Lu1 38.1(5) . . ?
Lu3 Lu7 Lu1 19.4(2) . . ?
Lu11 Lu7 Lu1 82.8(5) . . ?
Lu2 Lu7 Lu1 19.5(2) . . ?
Lu10 Lu7 Lu1 71.7(4) . . ?
Lu5 Lu7 Lu9 84.6(16) . . ?
Lu4 Lu7 Lu9 100.2(11) . . ?
C2E Lu7 Lu9 20.8(9) . . ?
Lu6 Lu7 Lu9 80.1(8) . . ?
C1E Lu7 Lu9 34.7(4) . . ?
Lu3 Lu7 Lu9 83.3(6) . . ?
Lu11 Lu7 Lu9 19.73(15) . . ?
Lu2 Lu7 Lu9 69.1(5) . . ?
Lu10 Lu7 Lu9 15.65(14) . . ?
Lu1 Lu7 Lu9 64.7(4) . . ?
Lu9 Lu8 Lu12 41.5(9) . . ?
Lu9 Lu8 Lu10 32.2(2) . . ?
Lu12 Lu8 Lu10 72.5(10) . . ?
Lu9 Lu8 C1E 79.6(3) . . ?
Lu12 Lu8 C1E 67.6(7) . . ?
Lu10 Lu8 C1E 82.5(3) . . ?
Lu9 Lu8 Lu11 18.27(9) . . ?
Lu12 Lu8 Lu11 36.4(9) . . ?
Lu10 Lu8 Lu11 38.54(19) . . ?
C1E Lu8 Lu11 61.4(3) . . ?
Lu9 Lu8 C2E 64.2(3) . . ?
Lu12 Lu8 C2E 70.0(7) . . ?
Lu10 Lu8 C2E 58.8(4) . . ?
C1E Lu8 C2E 24.9(4) . . ?
Lu11 Lu8 C2E 48.0(3) . . ?
Lu9 Lu8 Lu1 114.43(12) . . ?
Lu12 Lu8 Lu1 106.6(7) . . ?
Lu10 Lu8 Lu1 101.8(2) . . ?
C1E Lu8 Lu1 39.9(3) . . ?
Lu11 Lu8 Lu1 97.67(6) . . ?
C2E Lu8 Lu1 50.3(3) . . ?
Lu9 Lu8 Lu2 103.11(14) . . ?
Lu12 Lu8 Lu2 87.8(7) . . ?
Lu10 Lu8 Lu2 100.6(2) . . ?
C1E Lu8 Lu2 23.8(3) . . ?
Lu11 Lu8 Lu2 85.02(10) . . ?
C2E Lu8 Lu2 42.4(3) . . ?
Lu1 Lu8 Lu2 19.26(10) . . ?
Lu12 Lu9 Lu10 155.1(10) . . ?
Lu12 Lu9 Lu8 82.6(11) . . ?
Lu10 Lu9 Lu8 113.6(4) . . ?
Lu12 Lu9 Lu13 94.1(15) . . ?
Lu10 Lu9 Lu13 97.9(11) . . ?
Lu8 Lu9 Lu13 18.1(9) . . ?
Lu12 Lu9 Lu11 82.2(11) . . ?
Lu10 Lu9 Lu11 74.1(3) . . ?
Lu8 Lu9 Lu11 147.38(17) . . ?
Lu13 Lu9 Lu11 137.1(6) . . ?
Lu12 Lu9 C1E 66.7(10) . . ?
Lu10 Lu9 C1E 99.5(4) . . ?
Lu8 Lu9 C1E 71.5(3) . . ?
Lu13 Lu9 C1E 63.6(8) . . ?
Lu11 Lu9 C1E 76.0(3) . . ?
Lu12 Lu9 C2E 88.6(10) . . ?
Lu10 Lu9 C2E 73.1(4) . . ?
Lu8 Lu9 C2E 90.6(3) . . ?
Lu13 Lu9 C2E 76.9(7) . . ?
Lu11 Lu9 C2E 60.4(3) . . ?
C1E Lu9 C2E 27.9(4) . . ?
Lu12 Lu9 Lu7 93.8(11) . . ?
Lu10 Lu9 Lu7 64.5(7) . . ?
Lu8 Lu9 Lu7 105.0(6) . . ?
Lu13 Lu9 Lu7 90.4(8) . . ?
Lu11 Lu9 Lu7 47.7(5) . . ?
C1E Lu9 Lu7 41.1(7) . . ?
C2E Lu9 Lu7 14.8(6) . . ?
Lu9 Lu10 Lu11 63.7(3) . . ?
Lu9 Lu10 Lu13 45.7(7) . . ?
Lu11 Lu10 Lu13 99.2(7) . . ?
Lu9 Lu10 Lu8 34.2(2) . . ?
Lu11 Lu10 Lu8 93.0(3) . . ?
Lu13 Lu10 Lu8 12.9(6) . . ?
Lu9 Lu10 Lu12 11.4(5) . . ?
Lu11 Lu10 Lu12 53.0(5) . . ?
Lu13 Lu10 Lu12 51.8(8) . . ?
Lu8 Lu10 Lu12 42.0(5) . . ?
Lu9 Lu10 C2E 80.5(4) . . ?
Lu11 Lu10 C2E 61.8(3) . . ?
Lu13 Lu10 C2E 71.7(6) . . ?
Lu8 Lu10 C2E 78.3(3) . . ?
Lu12 Lu10 C2E 72.5(5) . . ?
Lu9 Lu10 C1E 57.4(3) . . ?
Lu11 Lu10 C1E 62.2(3) . . ?
Lu13 Lu10 C1E 50.5(6) . . ?
Lu8 Lu10 C1E 54.7(3) . . ?
Lu12 Lu10 C1E 51.2(5) . . ?
C2E Lu10 C1E 24.7(3) . . ?
Lu9 Lu10 Lu5 106.3(6) . . ?
Lu11 Lu10 Lu5 81.5(5) . . ?
Lu13 Lu10 Lu5 84.8(9) . . ?
Lu8 Lu10 Lu5 95.2(7) . . ?
Lu12 Lu10 Lu5 99.2(7) . . ?
C2E Lu10 Lu5 27.1(5) . . ?
C1E Lu10 Lu5 48.9(5) . . ?
Lu9 Lu10 Lu7 99.8(7) . . ?
Lu11 Lu10 Lu7 60.6(6) . . ?
Lu13 Lu10 Lu7 94.5(8) . . ?
Lu8 Lu10 Lu7 101.5(7) . . ?
Lu12 Lu10 Lu7 90.1(8) . . ?
C2E Lu10 Lu7 23.2(7) . . ?
C1E Lu10 Lu7 47.4(7) . . ?
Lu5 Lu10 Lu7 21.7(7) . . ?
Lu9 Lu11 Lu10 42.2(2) . . ?
Lu9 Lu11 Lu12 34.4(7) . . ?
Lu10 Lu11 Lu12 76.4(8) . . ?
Lu9 Lu11 C2E 83.1(3) . . ?
Lu10 Lu11 C2E 77.7(4) . . ?
Lu12 Lu11 C2E 85.9(7) . . ?
Lu9 Lu11 C1E 68.5(3) . . ?
Lu10 Lu11 C1E 83.3(3) . . ?
Lu12 Lu11 C1E 60.0(6) . . ?
C2E Lu11 C1E 28.2(4) . . ?
Lu9 Lu11 Lu8 14.34(8) . . ?
Lu10 Lu11 Lu8 48.4(2) . . ?
Lu12 Lu11 Lu8 30.4(7) . . ?
C2E Lu11 Lu8 70.7(3) . . ?
C1E Lu11 Lu8 54.3(3) . . ?
Lu9 Lu11 Lu13 20.3(4) . . ?
Lu10 Lu11 Lu13 44.2(6) . . ?
Lu12 Lu11 Lu13 38.6(8) . . ?
C2E Lu11 Lu13 62.8(5) . . ?
C1E Lu11 Lu13 49.7(5) . . ?
Lu8 Lu11 Lu13 9.3(4) . . ?
Lu9 Lu11 Lu7 112.6(6) . . ?
Lu10 Lu11 Lu7 94.1(7) . . ?
Lu12 Lu11 Lu7 115.4(9) . . ?
C2E Lu11 Lu7 31.0(7) . . ?
C1E Lu11 Lu7 55.5(7) . . ?
Lu8 Lu11 Lu7 101.3(6) . . ?
Lu13 Lu11 Lu7 92.9(7) . . ?
Lu9 Lu11 Lu5 92.9(6) . . ?
Lu10 Lu11 Lu5 74.2(5) . . ?
Lu12 Lu11 Lu5 103.4(9) . . ?
C2E Lu11 Lu5 19.5(7) . . ?
C1E Lu11 Lu5 47.6(7) . . ?
Lu8 Lu11 Lu5 83.1(6) . . ?
Lu13 Lu11 Lu5 74.1(7) . . ?
Lu7 Lu11 Lu5 21.0(7) . . ?
Lu9 Lu12 Lu8 55.8(10) . . ?
Lu9 Lu12 Lu11 63.3(11) . . ?
Lu8 Lu12 Lu11 113.2(14) . . ?
Lu9 Lu12 Lu13 52.3(12) . . ?
Lu8 Lu12 Lu13 11.9(6) . . ?
Lu11 Lu12 Lu13 104.0(14) . . ?
Lu9 Lu12 Lu10 13.5(6) . . ?
Lu8 Lu12 Lu10 65.5(9) . . ?
Lu11 Lu12 Lu10 50.6(7) . . ?
Lu13 Lu12 Lu10 59.6(11) . . ?
Lu9 Lu12 C1E 90.1(11) . . ?
Lu8 Lu12 C1E 76.0(8) . . ?
Lu11 Lu12 C1E 79.4(7) . . ?
Lu13 Lu12 C1E 66.0(8) . . ?
Lu10 Lu12 C1E 83.4(7) . . ?
Lu9 Lu12 C2E 70.4(10) . . ?
Lu8 Lu12 C2E 79.8(8) . . ?
Lu11 Lu12 C2E 55.4(6) . . ?
Lu13 Lu12 C2E 67.9(8) . . ?
Lu10 Lu12 C2E 60.7(6) . . ?
C1E Lu12 C2E 26.3(5) . . ?
Lu9 Lu12 Lu2 97.4(11) . . ?
Lu8 Lu12 Lu2 71.8(7) . . ?
Lu11 Lu12 Lu2 92.3(6) . . ?
Lu13 Lu12 Lu2 63.6(8) . . ?
Lu10 Lu12 Lu2 92.8(6) . . ?
C1E Lu12 Lu2 13.0(4) . . ?
C2E Lu12 Lu2 39.0(4) . . ?
Lu9 Lu13 Lu12 33.7(9) . . ?
Lu9 Lu13 Lu10 36.4(6) . . ?
Lu12 Lu13 Lu10 68.6(11) . . ?
Lu9 Lu13 C1E 82.4(8) . . ?
Lu12 Lu13 C1E 68.1(9) . . ?
Lu10 Lu13 C1E 87.9(7) . . ?
Lu9 Lu13 C2E 72.0(7) . . ?
Lu12 Lu13 C2E 73.8(8) . . ?
Lu10 Lu13 C2E 64.1(6) . . ?
C1E Lu13 C2E 27.5(4) . . ?
Lu9 Lu13 Lu11 22.6(4) . . ?
Lu12 Lu13 Lu11 37.4(8) . . ?
Lu10 Lu13 Lu11 36.7(4) . . ?
C1E Lu13 Lu11 61.6(5) . . ?
C2E Lu13 Lu11 49.5(5) . . ?
Lu9 Lu13 Lu1 126.5(8) . . ?
Lu12 Lu13 Lu1 112.0(10) . . ?
Lu10 Lu13 Lu1 115.3(7) . . ?
C1E Lu13 Lu1 45.7(5) . . ?
C2E Lu13 Lu1 55.9(5) . . ?
Lu11 Lu13 Lu1 104.1(5) . . ?
Lu9 Lu13 Lu2 109.7(8) . . ?
Lu12 Lu13 Lu2 91.6(10) . . ?
Lu10 Lu13 Lu2 109.9(6) . . ?
C1E Lu13 Lu2 27.3(4) . . ?
C2E Lu13 Lu2 45.8(5) . . ?
Lu11 Lu13 Lu2 88.6(4) . . ?
Lu1 Lu13 Lu2 20.39(16) . . ?
Lu9 Lu13 Lu6 109.7(9) . . ?
Lu12 Lu13 Lu6 106.9(9) . . ?
Lu10 Lu13 Lu6 93.1(8) . . ?
C1E Lu13 Lu6 40.0(6) . . ?
C2E Lu13 Lu6 37.9(7) . . ?
Lu11 Lu13 Lu6 87.4(7) . . ?
Lu1 Lu13 Lu6 22.3(6) . . ?
Lu2 Lu13 Lu6 28.2(5) . . ?
Lu9 Lu13 Lu5 87.6(10) . . ?
Lu12 Lu13 Lu5 95.7(9) . . ?
Lu10 Lu13 Lu5 67.7(8) . . ?
C1E Lu13 Lu5 42.7(6) . . ?
C2E Lu13 Lu5 22.4(6) . . ?
Lu11 Lu13 Lu5 66.7(7) . . ?
Lu1 Lu13 Lu5 47.6(7) . . ?
Lu2 Lu13 Lu5 47.5(6) . . ?
Lu6 Lu13 Lu5 25.4(8) . . ?
Lu9 Lu13 Lu3 107.4(7) . . ?
Lu12 Lu13 Lu3 98.6(8) . . ?
Lu10 Lu13 Lu3 97.6(6) . . ?
C1E Lu13 Lu3 30.5(4) . . ?
C2E Lu13 Lu3 36.3(4) . . ?
Lu11 Lu13 Lu3 84.9(4) . . ?
Lu1 Lu13 Lu3 19.55(10) . . ?
Lu2 Lu13 Lu3 17.25(12) . . ?
Lu6 Lu13 Lu3 11.6(4) . . ?
Lu5 Lu13 Lu3 31.4(6) . . ?
C2E C1E Lu2 108.6(12) . . ?
C2E C1E Lu13 94.5(12) . . ?
Lu2 C1E Lu13 122.6(8) . . ?
C2E C1E Lu12 98.0(13) . . ?
Lu2 C1E Lu12 152.5(8) . . ?
Lu13 C1E Lu12 45.9(7) . . ?
C2E C1E Lu8 99.5(10) . . ?
Lu2 C1E Lu8 128.2(5) . . ?
Lu13 C1E Lu8 10.4(6) . . ?
Lu12 C1E Lu8 36.4(5) . . ?
C2E C1E Lu1 99.9(10) . . ?
Lu2 C1E Lu1 32.9(3) . . ?
Lu13 C1E Lu1 93.0(7) . . ?
Lu12 C1E Lu1 136.2(7) . . ?
Lu8 C1E Lu1 101.0(4) . . ?
C2E C1E Lu9 80.3(11) . . ?
Lu2 C1E Lu9 156.6(6) . . ?
Lu13 C1E Lu9 33.9(6) . . ?
Lu12 C1E Lu9 23.2(6) . . ?
Lu8 C1E Lu9 28.95(16) . . ?
Lu1 C1E Lu9 125.7(5) . . ?
C2E C1E Lu3 79.1(11) . . ?
Lu2 C1E Lu3 29.7(2) . . ?
Lu13 C1E Lu3 123.2(7) . . ?
Lu12 C1E Lu3 168.7(8) . . ?
Lu8 C1E Lu3 132.9(5) . . ?
Lu1 C1E Lu3 35.66(19) . . ?
Lu9 C1E Lu3 146.8(5) . . ?
C2E C1E Lu11 60.6(10) . . ?
Lu2 C1E Lu11 166.3(6) . . ?
Lu13 C1E Lu11 68.7(7) . . ?
Lu12 C1E Lu11 40.6(6) . . ?
Lu8 C1E Lu11 64.4(3) . . ?
Lu1 C1E Lu11 150.5(5) . . ?
Lu9 C1E Lu11 35.44(18) . . ?
Lu3 C1E Lu11 139.3(5) . . ?
C2E C1E Lu6 68.0(13) . . ?
Lu2 C1E Lu6 44.8(9) . . ?
Lu13 C1E Lu6 107.7(10) . . ?
Lu12 C1E Lu6 150.8(10) . . ?
Lu8 C1E Lu6 118.0(8) . . ?
Lu1 C1E Lu6 34.6(9) . . ?
Lu9 C1E Lu6 128.2(9) . . ?
Lu3 C1E Lu6 18.6(7) . . ?
Lu11 C1E Lu6 127.6(10) . . ?
C2E C1E Lu4 53.9(10) . . ?
Lu2 C1E Lu4 57.4(3) . . ?
Lu13 C1E Lu4 134.9(8) . . ?
Lu12 C1E Lu4 150.1(7) . . ?
Lu8 C1E Lu4 144.6(5) . . ?
Lu1 C1E Lu4 66.6(3) . . ?
Lu9 C1E Lu4 134.0(5) . . ?
Lu3 C1E Lu4 32.13(16) . . ?
Lu11 C1E Lu4 109.5(4) . . ?
Lu6 C1E Lu4 35.6(8) . . ?
C2E C1E Lu7 26.8(12) . . ?
Lu2 C1E Lu7 90.3(9) . . ?
Lu13 C1E Lu7 121.2(12) . . ?
Lu12 C1E Lu7 117.2(11) . . ?
Lu8 C1E Lu7 126.2(10) . . ?
Lu1 C1E Lu7 95.3(9) . . ?
Lu9 C1E Lu7 104.2(9) . . ?
Lu3 C1E Lu7 64.2(8) . . ?
Lu11 C1E Lu7 76.5(9) . . ?
Lu6 C1E Lu7 60.8(12) . . ?
Lu4 C1E Lu7 33.0(8) . . ?
C1E C2E Lu7 136.0(19) . . ?
C1E C2E Lu5 130(2) . . ?
Lu7 C2E Lu5 44.3(14) . . ?
C1E C2E Lu4 99.7(12) . . ?
Lu7 C2E Lu4 44.9(14) . . ?
Lu5 C2E Lu4 41.0(11) . . ?
C1E C2E Lu11 91.3(10) . . ?
Lu7 C2E Lu11 110.4(14) . . ?
Lu5 C2E Lu11 138.4(15) . . ?
Lu4 C2E Lu11 150.5(6) . . ?
C1E C2E Lu10 96.7(11) . . ?
Lu7 C2E Lu10 124.9(16) . . ?
Lu5 C2E Lu10 118.3(12) . . ?
Lu4 C2E Lu10 159.3(6) . . ?
Lu11 C2E Lu10 40.4(4) . . ?
C1E C2E Lu6 85.2(13) . . ?
Lu7 C2E Lu6 78.9(15) . . ?
Lu5 C2E Lu6 45.4(15) . . ?
Lu4 C2E Lu6 40.3(8) . . ?
Lu11 C2E Lu6 169.2(10) . . ?
Lu10 C2E Lu6 129.8(9) . . ?
C1E C2E Lu9 71.8(10) . . ?
Lu7 C2E Lu9 144.4(15) . . ?
Lu5 C2E Lu9 142.8(11) . . ?
Lu4 C2E Lu9 170.6(7) . . ?
Lu11 C2E Lu9 36.6(3) . . ?
Lu10 C2E Lu9 26.3(2) . . ?
Lu6 C2E Lu9 132.9(9) . . ?
C1E C2E Lu3 73.7(10) . . ?
Lu7 C2E Lu3 78.5(14) . . ?
Lu5 C2E Lu3 57.1(14) . . ?
Lu4 C2E Lu3 33.9(3) . . ?
Lu11 C2E Lu3 164.1(5) . . ?
Lu10 C2E Lu3 144.7(5) . . ?
Lu6 C2E Lu3 19.2(7) . . ?
Lu9 C2E Lu3 137.0(5) . . ?
C1E C2E Lu13 58.0(10) . . ?
Lu7 C2E Lu13 165.7(16) . . ?
Lu5 C2E Lu13 127.5(13) . . ?
Lu4 C2E Lu13 140.7(8) . . ?
Lu11 C2E Lu13 67.6(6) . . ?
Lu10 C2E Lu13 44.1(6) . . ?
Lu6 C2E Lu13 102.0(10) . . ?
Lu9 C2E Lu13 31.1(5) . . ?
Lu3 C2E Lu13 107.1(7) . . ?
C1E C2E Lu2 46.0(9) . . ?
Lu7 C2E Lu2 100.0(15) . . ?
Lu5 C2E Lu2 84.9(15) . . ?
Lu4 C2E Lu2 56.2(4) . . ?
Lu11 C2E Lu2 136.5(5) . . ?
Lu10 C2E Lu2 133.9(5) . . ?
Lu6 C2E Lu2 42.7(8) . . ?
Lu9 C2E Lu2 114.6(4) . . ?
Lu3 C2E Lu2 27.9(2) . . ?
Lu13 C2E Lu2 89.8(7) . . ?
C1E C2E Lu12 55.7(10) . . ?
Lu7 C2E Lu12 146.3(14) . . ?
Lu5 C2E Lu12 163.3(12) . . ?
Lu4 C2E Lu12 153.4(8) . . ?
Lu11 C2E Lu12 38.8(5) . . ?
Lu10 C2E Lu12 46.8(6) . . ?
Lu6 C2E Lu12 133.5(10) . . ?
Lu9 C2E Lu12 21.0(5) . . ?
Lu3 C2E Lu12 128.4(7) . . ?
Lu13 C2E Lu12 38.3(6) . . ?
Lu2 C2E Lu12 101.5(6) . . ?
C18 C1 C5 121.8(18) . . ?
C18 C1 C2 121.6(19) . . ?
C5 C1 C2 104.8(12) . . ?
C3 C2 C15 120.4(12) . . ?
C3 C2 C1 108.0(12) . . ?
C15 C2 C1 119.1(13) . . ?
C12 C3 C2 119.2(11) . . ?
C12 C3 C4 118.1(10) . . ?
C2 C3 C4 110.6(11) . . ?
C9 C4 C3 122.2(12) . . ?
C9 C4 C5 118.8(11) . . ?
C3 C4 C5 108.9(12) . . ?
C6 C5 C4 125.9(15) . . ?
C6 C5 C1 120.4(18) . . ?
C4 C5 C1 106.7(11) . . ?
C7 C6 C5 117(2) . . ?
C7 C6 C20 115.3(18) . . ?
C5 C6 C20 122.1(17) . . ?
C6 C7 C23 123.7(19) . . ?
C6 C7 C8 121.3(17) . . ?
C23 C7 C8 109.2(12) . . ?
C25 C8 C9 122.6(13) . . ?
C25 C8 C7 105.6(13) . . ?
C9 C8 C7 122.1(11) . . ?
C4 C9 C8 113.6(12) . . ?
C4 C9 C10 118.9(12) . . ?
C8 C9 C10 117.5(11) . . ?
C11 C10 C9 117.7(10) . . ?
C11 C10 C27 111.4(12) . . ?
C9 C10 C27 119.4(11) . . ?
C29 C11 C10 107.9(11) . . ?
C29 C11 C12 120.8(12) . . ?
C10 C11 C12 122.9(11) . . ?
C3 C12 C13 119.9(10) . . ?
C3 C12 C11 119.1(11) . . ?
C13 C12 C11 112.9(10) . . ?
C31 C13 C14 113.2(12) . . ?
C31 C13 C12 119.6(10) . . ?
C14 C13 C12 118.5(11) . . ?
C15 C14 C13 121.4(13) . . ?
C15 C14 C33 120.3(13) . . ?
C13 C14 C33 109.8(12) . . ?
C14 C15 C2 119.9(11) . . ?
C14 C15 C16 115.5(15) . . ?
C2 C15 C16 114.2(14) . . ?
C17 C16 C15 117.3(15) . . ?
C17 C16 C53 112.3(15) . . ?
C15 C16 C53 117.5(14) . . ?
C18 C17 C16 128.7(18) . . ?
C18 C17 C51 109.3(19) . . ?
C16 C17 C51 104.6(15) . . ?
C17 C18 C1 114(2) . . ?
C17 C18 C19 122(3) . . ?
C1 C18 C19 120(2) . . ?
C18 C19 C49 115.0(19) . . ?
C18 C19 C20 122.4(19) . . ?
C49 C19 C20 114.5(15) . . ?
C21 C20 C6 126.9(15) . . ?
C21 C20 C19 116.3(14) . . ?
C6 C20 C19 112.7(15) . . ?
C47 C21 C20 122.7(16) . . ?
C47 C21 C22 123.1(18) . . ?
C20 C21 C22 112.0(16) . . ?
C44 C22 C23 110.9(16) . . ?
C44 C22 C21 121.0(18) . . ?
C23 C22 C21 123.2(16) . . ?
C22 C23 C24 126.3(14) . . ?
C22 C23 C7 118.3(13) . . ?
C24 C23 C7 105.1(13) . . ?
C42 C24 C23 118.9(14) . . ?
C42 C24 C25 122.3(13) . . ?
C23 C24 C25 110.7(12) . . ?
C26 C25 C8 120.5(13) . . ?
C26 C25 C24 118.6(12) . . ?
C8 C25 C24 109.3(12) . . ?
C25 C26 C27 117.8(11) . . ?
C25 C26 C40 118.7(12) . . ?
C27 C26 C40 114.4(13) . . ?
C10 C27 C28 110.4(11) . . ?
C10 C27 C26 122.0(12) . . ?
C28 C27 C26 117.7(12) . . ?
C38 C28 C27 126.1(16) . . ?
C38 C28 C29 121.5(16) . . ?
C27 C28 C29 102.6(11) . . ?
C30 C29 C11 126.0(14) . . ?
C30 C29 C28 117.4(14) . . ?
C11 C29 C28 107.6(12) . . ?
C29 C30 C31 114.9(16) . . ?
C29 C30 C36 117.2(18) . . ?
C31 C30 C36 122.4(18) . . ?
C30 C31 C13 125.1(14) . . ?
C30 C31 C32 118.8(14) . . ?
C13 C31 C32 110.2(12) . . ?
C34 C32 C33 130.4(19) . . ?
C34 C32 C31 123.0(18) . . ?
C33 C32 C31 102.3(11) . . ?
C85 C33 C14 125.7(18) . . ?
C85 C33 C32 124.7(17) . . ?
C14 C33 C32 104.4(11) . . ?
C32 C34 C35 112(2) . . ?
C32 C34 C81 109(2) . . ?
C35 C34 C81 132.2(18) . . ?
C76 C35 C36 111.7(18) . . ?
C76 C35 C34 109(2) . . ?
C36 C35 C34 130.6(18) . . ?
C35 C36 C37 107.1(16) . . ?
C35 C36 C30 112.7(18) . . ?
C37 C36 C30 129.7(19) . . ?
C36 C37 C75 103.5(17) . . ?
C36 C37 C38 110.7(19) . . ?
C75 C37 C38 134.3(19) . . ?
C39 C38 C28 118(2) . . ?
C39 C38 C37 113(2) . . ?
C28 C38 C37 123(2) . . ?
C38 C39 C40 124.5(18) . . ?
C38 C39 C54 122.9(18) . . ?
C40 C39 C54 104.3(12) . . ?
C41 C40 C26 120.8(13) . . ?
C41 C40 C39 110.0(14) . . ?
C26 C40 C39 119.1(12) . . ?
C40 C41 C55 110.1(13) . . ?
C40 C41 C42 121.0(13) . . ?
C55 C41 C42 119.1(13) . . ?
C24 C42 C43 113.7(12) . . ?
C24 C42 C41 118.4(13) . . ?
C43 C42 C41 119.7(13) . . ?
C44 C43 C42 121.9(13) . . ?
C44 C43 C57 109.3(12) . . ?
C42 C43 C57 119.4(12) . . ?
C22 C44 C43 126.4(16) . . ?
C22 C44 C45 116.7(14) . . ?
C43 C44 C45 109.0(12) . . ?
C46 C45 C58 129.3(17) . . ?
C46 C45 C44 121.3(17) . . ?
C58 C45 C44 100.5(11) . . ?
C63 C46 C45 116(2) . . ?
C63 C46 C47 121(2) . . ?
C45 C46 C47 121(2) . . ?
C48 C47 C21 116.9(19) . . ?
C48 C47 C46 122(2) . . ?
C21 C47 C46 116.2(18) . . ?
C47 C48 C49 133.3(18) . . ?
C47 C48 C64 115(2) . . ?
C49 C48 C64 108.9(13) . . ?
C48 C49 C50 103.0(12) . . ?
C48 C49 C19 116.0(14) . . ?
C50 C49 C19 135.4(17) . . ?
C48 C49 C51 135.9(13) . . ?
C50 C49 C51 38.1(11) . . ?
C19 C49 C51 97.3(14) . . ?
C51 C50 C66 133(2) . . ?
C51 C50 C49 96.9(19) . . ?
C66 C50 C49 110.9(12) . . ?
C50 C51 C52 106(2) . . ?
C50 C51 C17 142(2) . . ?
C52 C51 C17 104.3(13) . . ?
C50 C51 C49 45.0(11) . . ?
C52 C51 C49 136.5(12) . . ?
C17 C51 C49 96.7(13) . . ?
C68 C52 C53 113.4(16) . . ?
C68 C52 C51 126.5(17) . . ?
C53 C52 C51 108.1(13) . . ?
C85 C53 C52 112.3(15) . . ?
C85 C53 C16 126.7(14) . . ?
C52 C53 C16 109.9(12) . . ?
C55 C54 C71 130.6(17) . . ?
C55 C54 C39 102.7(14) . . ?
C71 C54 C39 115.5(14) . . ?
C54 C55 C41 112.8(13) . . ?
C54 C55 C56 116.2(14) . . ?
C41 C55 C56 121.9(12) . . ?
C57 C56 C61 119.1(14) . . ?
C57 C56 C55 118.0(14) . . ?
C61 C56 C55 113.7(13) . . ?
C56 C57 C58 120.8(14) . . ?
C56 C57 C43 121.5(14) . . ?
C58 C57 C43 107.6(12) . . ?
C57 C58 C59 120.3(13) . . ?
C57 C58 C45 113.3(13) . . ?
C59 C58 C45 115.7(12) . . ?
C60 C59 C62 121.9(13) . . ?
C60 C59 C58 118.1(13) . . ?
C62 C59 C58 110.8(13) . . ?
C59 C60 C73 118.0(14) . . ?
C59 C60 C61 119.1(12) . . ?
C73 C60 C61 112.0(13) . . ?
C56 C61 C60 122.4(12) . . ?
C56 C61 C72 121.6(15) . . ?
C60 C61 C72 106.3(14) . . ?
C59 C62 C69 118.9(15) . . ?
C59 C62 C63 124.7(16) . . ?
C69 C62 C63 105.5(15) . . ?
C46 C63 C62 120(2) . . ?
C46 C63 C65 126(2) . . ?
C62 C63 C65 101.2(18) . . ?
C66 C64 C48 108.0(13) . . ?
C66 C64 C65 88(2) . . ?
C48 C64 C65 128(2) . . ?
C70 C65 C64 144(2) . . ?
C70 C65 C63 117(2) . . ?
C64 C65 C63 95.4(19) . . ?
C70 C65 C66 101.8(17) . . ?
C64 C65 C66 42.6(11) . . ?
C63 C65 C66 132.0(17) . . ?
C64 C66 C50 100.3(13) . . ?
C64 C66 C67 142(2) . . ?
C50 C66 C67 113(2) . . ?
C64 C66 C65 49.6(12) . . ?
C50 C66 C65 144.8(14) . . ?
C67 C66 C65 92.8(17) . . ?
C68 C67 C66 124(2) . . ?
C68 C67 C83 116(3) . . ?
C66 C67 C83 111.6(18) . . ?
C68 C67 C82 47.0(13) . . ?
C66 C67 C82 145.0(17) . . ?
C83 C67 C82 69.5(17) . . ?
C67 C68 C52 116(2) . . ?
C67 C68 C82 92.4(18) . . ?
C52 C68 C82 132.7(17) . . ?
C74 C69 C62 120.3(14) . . ?
C74 C69 C70 119.3(16) . . ?
C62 C69 C70 111.3(16) . . ?
C65 C70 C83 119(2) . . ?
C65 C70 C69 104.7(16) . . ?
C83 C70 C69 119(2) . . ?
C72 C71 C54 110.0(19) . . ?
C72 C71 C75 115(2) . . ?
C54 C71 C75 127(2) . . ?
C71 C72 C61 127(2) . . ?
C71 C72 C78 114.9(19) . . ?
C61 C72 C78 108.4(15) . . ?
C60 C73 C74 122.6(16) . . ?
C60 C73 C78 111.4(16) . . ?
C74 C73 C78 118.7(14) . . ?
C69 C74 C73 117.6(14) . . ?
C69 C74 C80 120.1(19) . . ?
C73 C74 C80 110.7(19) . . ?
C76 C75 C37 110.4(15) . . ?
C76 C75 C71 133(2) . . ?
C37 C75 C71 106(2) . . ?
C35 C76 C75 107.2(18) . . ?
C35 C76 C77 130(2) . . ?
C75 C76 C77 114.2(16) . . ?
C78 C77 C79 129.7(17) . . ?
C78 C77 C76 107.8(17) . . ?
C79 C77 C76 112.3(16) . . ?
C77 C78 C73 117(2) . . ?
C77 C78 C72 133.2(17) . . ?
C73 C78 C72 101.5(13) . . ?
C80 C79 C81 134(3) . . ?
C80 C79 C77 97.2(17) . . ?
C81 C79 C77 126(2) . . ?
C79 C80 C74 142(2) . . ?
C79 C80 C84 93.7(18) . . ?
C74 C80 C84 113(2) . . ?
C79 C81 C34 110(2) . . ?
C79 C81 C86 132(2) . . ?
C34 C81 C86 113.4(16) . . ?
C86 C82 C68 109.2(16) . . ?
C86 C82 C84 121(2) . . ?
C68 C82 C84 127(2) . . ?
C86 C82 C67 143.2(16) . . ?
C68 C82 C67 40.7(11) . . ?
C84 C82 C67 86.4(17) . . ?
C86 C82 C83 154.6(17) . . ?
C68 C82 C83 86.8(16) . . ?
C84 C82 C83 40.0(15) . . ?
C67 C82 C83 46.5(11) . . ?
C84 C83 C70 126(3) . . ?
C84 C83 C67 113(2) . . ?
C70 C83 C67 113(2) . . ?
C84 C83 C82 48.7(14) . . ?
C70 C83 C82 154.5(17) . . ?
C67 C83 C82 64.0(14) . . ?
C83 C84 C82 91(2) . . ?
C83 C84 C80 121.8(19) . . ?
C82 C84 C80 138(2) . . ?
C33 C85 C86 110.6(19) . . ?
C33 C85 C53 113.3(16) . . ?
C86 C85 C53 128.6(18) . . ?
C82 C86 C85 120.1(17) . . ?
C82 C86 C81 100.5(16) . . ?
C85 C86 C81 130.7(17) . . ?
N1A Ni1A N4A 90.1(2) . . ?
N1A Ni1A N3A 178.8(2) . . ?
N4A Ni1A N3A 89.9(2) . . ?
N1A Ni1A N2A 90.2(2) . . ?
N4A Ni1A N2A 177.6(2) . . ?
N3A Ni1A N2A 89.7(2) . . ?
N1A C1A C31A 125.8(6) . . ?
N1A C1A C2A 111.8(6) . . ?
C31A C1A C2A 122.4(7) . . ?
C35A N2A C10A 104.1(6) . . ?
C35A N2A Ni1A 128.9(4) . . ?
C10A N2A Ni1A 127.0(5) . . ?
C5A C2A C1A 105.9(6) . . ?
C5A C2A C3A 128.6(6) . . ?
C1A C2A C3A 125.3(6) . . ?
C25A N3A C18A 104.6(6) . . ?
C25A N3A Ni1A 127.9(5) . . ?
C18A N3A Ni1A 127.4(4) . . ?
C30A N4A C26A 103.8(6) . . ?
C30A N4A Ni1A 127.9(4) . . ?
C26A N4A Ni1A 128.2(5) . . ?
C2A C5A C8A 106.9(6) . . ?
C2A C5A C6A 127.7(7) . . ?
C8A C5A C6A 125.3(7) . . ?
C5A C6A C7A 111.6(6) . . ?
C9A C8A N1A 124.4(7) . . ?
C9A C8A C5A 124.2(6) . . ?
N1A C8A C5A 111.4(6) . . ?
C10A C9A C8A 124.6(6) . . ?
C9A C10A N2A 125.5(6) . . ?
C9A C10A C11A 123.4(6) . . ?
N2A C10A C11A 111.0(6) . . ?
C14A C11A C10A 106.6(6) . . ?
C14A C11A C12A 128.6(7) . . ?
C10A C11A C12A 124.7(7) . . ?
C11A C12A C13A 112.8(6) . . ?
C11A C14A C35A 105.7(7) . . ?
C11A C14A C15A 129.5(7) . . ?
C35A C14A C15A 124.7(7) . . ?
C14A C15A C16A 113.2(8) . . ?
C18A C17A C35A 123.6(7) . . ?
C17A C18A N3A 125.9(6) . . ?
C17A C18A C19A 122.9(7) . . ?
N3A C18A C19A 111.2(6) . . ?
C22A C19A C18A 105.7(7) . . ?
C22A C19A C20A 130.2(7) . . ?
C18A C19A C20A 124.0(6) . . ?
C19A C20A C21A 114.5(8) . . ?
C19A C22A C25A 107.1(6) . . ?
C19A C22A C23A 127.8(7) . . ?
C25A C22A C23A 125.1(7) . . ?
C22A C23A C24A 113.1(6) . . ?
N3A C25A C33A 125.6(6) . . ?
N3A C25A C22A 111.5(6) . . ?
C33A C25A C22A 123.0(6) . . ?
C33A C26A N4A 124.0(6) . . ?
C33A C26A C27A 124.3(6) . . ?
N4A C26A C27A 111.7(6) . . ?
C32A C27A C26A 106.7(6) . . ?
C32A C27A C28A 128.6(7) . . ?
C26A C27A C28A 124.6(7) . . ?
C27A C28A C29A 113.2(7) . . ?
C31A C30A N4A 124.6(6) . . ?
C31A C30A C32A 123.7(7) . . ?
N4A C30A C32A 111.7(6) . . ?
C1A C31A C30A 123.9(7) . . ?
C27A C32A C30A 106.1(7) . . ?
C27A C32A C34A 129.4(7) . . ?
C30A C32A C34A 124.4(7) . . ?
C25A C33A C26A 124.4(6) . . ?
N2A C35A C17A 124.4(6) . . ?
N2A C35A C14A 112.5(6) . . ?
C17A C35A C14A 123.1(7) . . ?
C32A C34A C36A 113.5(8) . . ?
C2A C3A C4A 110.8(7) . . ?
C1A N1A C8A 104.1(6) . . ?
C1A N1A Ni1A 127.7(4) . . ?
C8A N1A Ni1A 128.2(5) . . ?
C2B C1B C6B 115.9(12) . . ?
C5B C6B C1B 125.9(11) . . ?
C6B C5B C4B 114.9(11) . . ?
C3B C4B C5B 121.6(13) . . ?
C2B C3B C4B 119.0(12) . . ?
C3B C2B C1B 122.7(12) . . ?

_refine_diff_density_max         1.924
_refine_diff_density_min         -1.978
_refine_diff_density_rms         0.180



_vrf_PLAT029_Lu2C2@C2v-C86       
;
PROBLEM: PLAT029 Type_3  _diffrn_measured_fraction_theta_full value Low 
RESPONSE: Because of limited beamtime available, data was collected from only 
one crystal. The completeness of this data especialy in the highest resolution 
shell was restrained by some shaded areas (cryo-system or the beamstop)
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2C2@Cs-C88
_database_code_depnum_ccdc_archive 'CCDC 1836829'
_audit_update_record             
;
2018-04-13 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2C2@Cs-C88 Ni(OEP)'
_chemical_name_common            'Lu2C2@Cs-C88 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C90, C36 H44 N4 Ni, 1.6(C6 H6), 0.4(C S2)'
_chemical_formula_sum            'C136 H53.60 Lu2 N4 Ni S0.80'
_chemical_formula_weight         2177.69

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0027 0.0014 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0053 0.0028 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1098 0.1057 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3436 0.9622 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.2922 5.1425 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.749(5)
_cell_length_b                   15.029(5)
_cell_length_c                   19.899(5)
_cell_angle_alpha                84.624(5)
_cell_angle_beta                 88.620(5)
_cell_angle_gamma                62.644(5)
_cell_volume                     3899(2)
_cell_formula_units_Z            2
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9723
_cell_measurement_theta_min      2.503
_cell_measurement_theta_max      23.127

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.855
_exptl_crystal_F_000             2161
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.150
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.080
_exptl_absorpt_coefficient_mu    2.309
_shelx_estimated_absorpt_T_min   0.758
_shelx_estimated_absorpt_T_max   0.831
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.4105
_exptl_absorpt_correction_T_max  0.7449
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline BL17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            44643
_diffrn_reflns_av_unetI/netI     0.0691
_diffrn_reflns_av_R_equivalents  0.0703
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         0.944
_diffrn_reflns_theta_max         23.154
_diffrn_reflns_theta_full        23.048
_diffrn_measured_fraction_theta_max 0.913
_diffrn_measured_fraction_theta_full 0.914
_diffrn_reflns_Laue_measured_fraction_max 0.913
_diffrn_reflns_Laue_measured_fraction_full 0.914
_diffrn_reflns_point_group_measured_fraction_max 0.913
_diffrn_reflns_point_group_measured_fraction_full 0.914
_reflns_number_total             13054
_reflns_number_gt                11440
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1659P)²+37.0596P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         13054
_refine_ls_number_parameters     1466
_refine_ls_number_restraints     1714
_refine_ls_R_factor_all          0.0991
_refine_ls_R_factor_gt           0.0916
_refine_ls_wR_factor_ref         0.2637
_refine_ls_wR_factor_gt          0.2540
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_restrained_S_all      0.998
_refine_ls_shift/su_max          0.021
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.6161(3) 0.1346(3) 0.87770(19) 0.0418(8) Uani 0.1148 1 d . U P A 1
Lu2 Lu 0.5916(12) 0.3606(13) 0.8161(10) 0.055(3) Uani 0.0311 1 d . U P A 1
Lu3 Lu 0.5718(4) 0.3010(3) 0.86765(16) 0.0380(6) Uani 0.4908 1 d . U P A 1
Lu4 Lu 0.5718(8) 0.3121(7) 0.8507(4) 0.0405(14) Uani 0.2151 1 d . U P A 1
Lu5 Lu 0.509(2) 0.349(2) 0.8541(15) 0.049(3) Uani 0.0212 1 d . U P A 1
Lu6 Lu 0.5777(12) 0.2161(13) 0.8893(9) 0.044(2) Uani 0.0275 1 d . U P A 1
Lu7 Lu 0.8380(3) 0.0540(3) 0.75803(13) 0.0225(5) Uani 0.5782 1 d . U P A 1
Lu8 Lu 0.7797(9) 0.0204(8) 0.8136(6) 0.0360(19) Uani 0.0342 1 d . U P A 1
Lu9 Lu 0.8617(19) 0.076(2) 0.7971(17) 0.030(3) Uani 0.0169 1 d . U P A 1
Lu10 Lu 0.775(2) 0.0515(19) 0.7677(13) 0.032(3) Uani 0.0176 1 d . U P A 1
Lu11 Lu 0.8226(3) 0.2153(3) 0.73250(19) 0.0363(8) Uani 0.106 1 d . U P A 1
Lu12 Lu 0.894(2) 0.023(2) 0.7590(13) 0.032(3) Uani 0.0202 1 d . U P A 1
Lu13 Lu 0.860(3) 0.042(3) 0.821(2) 0.032(3) Uani 0.0102 1 d . U P A 1
Lu14 Lu 0.777(2) 0.095(2) 0.7505(12) 0.030(2) Uiso 0.0176 1 d . U P A 1
Lu15 Lu 0.8195(17) 0.0415(16) 0.7343(14) 0.032(3) Uani 0.0249 1 d . U P A 1
Lu16 Lu 0.8350(14) 0.0507(13) 0.7719(6) 0.027(2) Uani 0.14 1 d . U P A 1
Lu17 Lu 0.801(4) 0.068(4) 0.702(3) 0.028(4) Uani 0.0076 1 d . U P A 1
Lu18 Lu 0.5490(14) 0.2776(16) 0.8270(12) 0.054(3) Uani 0.0276 1 d . U P A 1
Lu19 Lu 0.8347(16) 0.1329(16) 0.7325(11) 0.029(2) Uiso 0.0168 1 d . U P A 1
Lu20 Lu 0.6283(19) 0.2716(18) 0.8724(13) 0.045(3) Uani 0.0255 1 d . U P A 1
Lu21 Lu 0.594(2) 0.313(2) 0.902(2) 0.046(3) Uani 0.018 1 d . U P A 1
Lu22 Lu 0.638(2) 0.327(2) 0.8625(17) 0.051(3) Uani 0.017 1 d . U P A 1
Lu23 Lu 0.666(3) 0.226(3) 0.918(2) 0.045(4) Uani 0.0114 1 d . U P A 1
Lu24 Lu 0.916(3) -0.016(3) 0.787(2) 0.029(3) Uani 0.0097 1 d . U P A 1
C1C C 0.7094(14) 0.1523(13) 0.8335(9) 0.0411(18) Uani 0.5736 1 d . U P A 1
C2C C 0.7209(8) 0.2187(7) 0.8021(5) 0.0411(18) Uani 1 1 d . U . A 1
C3C C 0.6777(19) 0.2064(17) 0.7606(12) 0.0411(18) Uani 0.4264 1 d . U P A 1
Ni1A Ni 0.52299(7) 0.01793(6) 0.58210(4) 0.0178(3) Uani 1 1 d . . . B 2
N1A N 0.4667(5) -0.0368(4) 0.6559(3) 0.0190(7) Uani 1 1 d . . . B 2
N2A N 0.3981(5) 0.1484(4) 0.5805(3) 0.0190(7) Uani 1 1 d . . . B 2
N3A N 0.5809(5) 0.0742(5) 0.5100(3) 0.0215(13) Uani 1 1 d . . . B 2
N4A N 0.6503(5) -0.1107(4) 0.5862(3) 0.0190(7) Uani 1 1 d . . . B 2
C1A C 0.5140(6) -0.1322(6) 0.6892(4) 0.0240(6) Uani 1 1 d . U . B 2
C2A C 0.4499(6) -0.1422(6) 0.7429(4) 0.0240(6) Uani 1 1 d . U . B 2
C3A C 0.4795(6) -0.2338(6) 0.7918(4) 0.0240(6) Uani 1 1 d . U . B 2
H3AA H 0.5102 -0.2932 0.7672 0.029 Uiso 1 1 calc R U . B 2
H3AB H 0.4184 -0.2315 0.8127 0.029 Uiso 1 1 calc R U . B 2
C4A C 0.5534(6) -0.2435(6) 0.8465(4) 0.0240(6) Uani 1 1 d . U . B 2
H4AA H 0.5693 -0.3033 0.8761 0.036 Uiso 1 1 calc R U . B 2
H4AB H 0.5230 -0.1858 0.8719 0.036 Uiso 1 1 calc R U . B 2
H4AC H 0.6149 -0.2475 0.8264 0.036 Uiso 1 1 calc R U . B 2
C5A C 0.3638(6) -0.0532(6) 0.7408(4) 0.0240(6) Uani 1 1 d . U . B 2
C6A C 0.2752(6) -0.0204(6) 0.7876(4) 0.0240(6) Uani 1 1 d . U . B 2
H6AA H 0.2754 -0.0793 0.8122 0.029 Uiso 1 1 calc R U . B 2
H6AB H 0.2121 0.0146 0.7613 0.029 Uiso 1 1 calc R U . B 2
C7A C 0.2787(7) 0.0487(7) 0.8379(4) 0.0319(18) Uani 1 1 d . U . B 2
H7AA H 0.2218 0.0663 0.8674 0.048 Uiso 1 1 calc R U . B 2
H7AB H 0.2754 0.1086 0.8139 0.048 Uiso 1 1 calc R U . B 2
H7AC H 0.3412 0.0145 0.8641 0.048 Uiso 1 1 calc R U . B 2
C8A C 0.3760(6) 0.0110(6) 0.6863(4) 0.0215(15) Uani 1 1 d . U . B 2
C9A C 0.3027(6) 0.1093(6) 0.6695(4) 0.0221(15) Uani 1 1 d . U . B 2
H9A H 0.2417 0.1334 0.6927 0.027 Uiso 1 1 calc R U . B 2
C10A C 0.3151(6) 0.1729(6) 0.6208(4) 0.0236(15) Uani 1 1 d . U . B 2
C11A C 0.2404(6) 0.2776(6) 0.6054(4) 0.0266(16) Uani 1 1 d . U . B 2
C12A C 0.1422(6) 0.3291(6) 0.6424(5) 0.0319(18) Uani 1 1 d . U . B 2
H12A H 0.1114 0.2841 0.6491 0.038 Uiso 1 1 calc R U . B 2
H12B H 0.0954 0.3885 0.6146 0.038 Uiso 1 1 calc R U . B 2
C13A C 0.2794(6) 0.3144(6) 0.5541(4) 0.0232(15) Uani 1 1 d . U . B 2
C14A C 0.2325(6) 0.4206(6) 0.5203(4) 0.0287(17) Uani 1 1 d . U . B 2
H14A H 0.1592 0.4518 0.5267 0.034 Uiso 1 1 calc R U . B 2
H14B H 0.2442 0.4181 0.4722 0.034 Uiso 1 1 calc R U . B 2
C15A C 0.2751(8) 0.4853(6) 0.5474(5) 0.038(2) Uani 1 1 d . U . B 2
H15A H 0.2453 0.5504 0.5224 0.057 Uiso 1 1 calc R U . B 2
H15B H 0.3479 0.4538 0.5426 0.057 Uiso 1 1 calc R U . B 2
H15C H 0.2590 0.4926 0.5942 0.057 Uiso 1 1 calc R U . B 2
C16A C 0.3765(6) 0.2358(5) 0.5400(4) 0.0206(14) Uani 1 1 d . U . B 2
C17A C 0.4407(6) 0.2453(5) 0.4918(4) 0.0209(15) Uani 1 1 d . U . B 2
H17A H 0.4179 0.3066 0.4657 0.025 Uiso 1 1 calc R U . B 2
C18A C 0.5354(6) 0.1709(6) 0.4796(4) 0.0240(6) Uani 1 1 d . U . B 2
C19A C 0.6048(6) 0.1845(6) 0.4311(4) 0.0233(15) Uani 1 1 d . U . B 2
C20A C 0.5835(6) 0.2824(6) 0.3922(4) 0.0275(17) Uani 1 1 d . U . B 2
H20A H 0.5120 0.3175 0.3783 0.033 Uiso 1 1 calc R U . B 2
H20B H 0.6239 0.2693 0.3517 0.033 Uiso 1 1 calc R U . B 2
C21A C 0.6081(8) 0.3496(6) 0.4334(5) 0.040(2) Uani 1 1 d . U . B 2
H21A H 0.5974 0.4096 0.4058 0.060 Uiso 1 1 calc R U . B 2
H21B H 0.6780 0.3141 0.4488 0.060 Uiso 1 1 calc R U . B 2
H21C H 0.5643 0.3672 0.4716 0.060 Uiso 1 1 calc R U . B 2
C22A C 0.6913(6) 0.0965(6) 0.4336(4) 0.0235(15) Uani 1 1 d . U . B 2
C23A C 0.7892(6) 0.0727(6) 0.3980(4) 0.0258(16) Uani 1 1 d . U . B 2
H23A H 0.7750 0.1165 0.3564 0.031 Uiso 1 1 calc R U . B 2
H23B H 0.8193 0.0038 0.3863 0.031 Uiso 1 1 calc R U . B 2
C24A C 0.8653(7) 0.0860(8) 0.4417(5) 0.037(2) Uani 1 1 d . U . B 2
H24A H 0.9243 0.0765 0.4158 0.055 Uiso 1 1 calc R U . B 2
H24B H 0.8855 0.0373 0.4804 0.055 Uiso 1 1 calc R U . B 2
H24C H 0.8337 0.1526 0.4563 0.055 Uiso 1 1 calc R U . B 2
C25A C 0.7480(6) -0.0701(6) 0.4987(4) 0.0220(15) Uani 1 1 d . U . B 2
H25A H 0.8085 -0.0942 0.4751 0.026 Uiso 1 1 calc R U . B 2
C26A C 0.7349(6) -0.1337(5) 0.5484(4) 0.0217(15) Uani 1 1 d . U . B 2
C27A C 0.8143(6) -0.2355(6) 0.5667(4) 0.0266(16) Uani 1 1 d . U . B 2
C28A C 0.9154(6) -0.2836(6) 0.5355(4) 0.0293(17) Uani 1 1 d . U . B 2
H28A H 0.9068 -0.2674 0.4869 0.035 Uiso 1 1 calc R U . B 2
H28B H 0.9434 -0.3560 0.5444 0.035 Uiso 1 1 calc R U . B 2
C29A C 0.9917(7) -0.2515(7) 0.5607(5) 0.041(2) Uani 1 1 d . U . B 2
H29A H 1.0548 -0.2840 0.5375 0.061 Uiso 1 1 calc R U . B 2
H29B H 1.0038 -0.2705 0.6084 0.061 Uiso 1 1 calc R U . B 2
H29C H 0.9647 -0.1799 0.5523 0.061 Uiso 1 1 calc R U . B 2
C30A C 0.7741(6) -0.2727(5) 0.6175(4) 0.0237(15) Uani 1 1 d . U . B 2
C31A C 0.8253(6) -0.3749(6) 0.6579(5) 0.0301(17) Uani 1 1 d . U . B 2
H31A H 0.7756 -0.3999 0.6658 0.036 Uiso 1 1 calc R U . B 2
H31B H 0.8794 -0.4214 0.6313 0.036 Uiso 1 1 calc R U . B 2
C32A C 0.8696(8) -0.3735(7) 0.7244(5) 0.041(2) Uani 1 1 d . U . B 2
H32A H 0.9004 -0.4401 0.7472 0.061 Uiso 1 1 calc R U . B 2
H32B H 0.8165 -0.3287 0.7515 0.061 Uiso 1 1 calc R U . B 2
H32C H 0.9205 -0.3507 0.7171 0.061 Uiso 1 1 calc R U . B 2
C33A C 0.6742(6) -0.1966(6) 0.6290(4) 0.0228(15) Uani 1 1 d . U . B 2
C34A C 0.6084(6) -0.2059(5) 0.6769(4) 0.0209(15) Uani 1 1 d . U . B 2
H34A H 0.6307 -0.2675 0.7025 0.025 Uiso 1 1 calc R U . B 2
C35A C 0.6745(6) 0.0277(5) 0.4830(3) 0.0194(14) Uani 1 1 d . U . B 2
C36A C 0.1554(8) 0.3602(8) 0.7110(5) 0.047(2) Uani 1 1 d . U . B 2
H36A H 0.0901 0.3929 0.7316 0.071 Uiso 1 1 calc R U . B 2
H36B H 0.1847 0.4056 0.7049 0.071 Uiso 1 1 calc R U . B 2
H36C H 0.1998 0.3015 0.7395 0.071 Uiso 1 1 calc R U . B 2
C1 C 0.4770(10) 0.1223(11) 0.9163(7) 0.063(3) Uani 1 1 d . U . C 3
C2 C 0.4997(10) 0.1662(10) 0.9692(6) 0.060(3) Uani 1 1 d . U . C 3
C3 C 0.5944(10) 0.0985(12) 0.9999(6) 0.067(3) Uani 1 1 d . U . C 3
C4 C 0.6285(12) 0.0057(11) 0.9757(7) 0.072(3) Uani 1 1 d . U . C 3
C5 C 0.5549(13) 0.0185(12) 0.9243(8) 0.079(4) Uani 1 1 d . U . C 3
C6 C 0.5894(14) -0.0316(13) 0.8708(9) 0.084(4) Uani 1 1 d . U . C 3
C7 C 0.5548(11) 0.0183(13) 0.8026(7) 0.071(3) Uani 1 1 d . U . C 3
C8 C 0.4843(11) 0.1212(14) 0.7923(6) 0.070(3) Uani 1 1 d . U . C 3
C9 C 0.4402(10) 0.1729(13) 0.8550(7) 0.072(3) Uani 1 1 d . U . C 3
C10 C 0.4015(9) 0.2830(13) 0.8509(7) 0.069(3) Uani 1 1 d . U . C 3
C11 C 0.4061(9) 0.3315(11) 0.9060(7) 0.063(3) Uani 1 1 d . U . C 3
C12 C 0.4679(9) 0.2700(10) 0.9659(6) 0.056(3) Uani 1 1 d . U . C 3
C13 C 0.5301(11) 0.3076(11) 0.9927(6) 0.062(3) Uani 1 1 d . U . C 3
C14 C 0.6328(11) 0.2358(12) 1.0162(6) 0.064(3) Uani 1 1 d . U . C 3
C15 C 0.6691(10) 0.1315(12) 1.0174(5) 0.062(3) Uani 1 1 d . U . C 3
C16 C 0.7781(11) 0.0692(12) 1.0025(6) 0.071(4) Uani 1 1 d . U . C 3
C17 C 0.8034(12) -0.0243(12) 0.9814(7) 0.083(4) Uani 1 1 d . U . C 3
C18 C 0.7293(14) -0.0559(12) 0.9708(9) 0.090(5) Uani 1 1 d . U . C 3
C19 C 0.7671(15) -0.1173(11) 0.9161(11) 0.096(5) Uani 1 1 d . U . C 3
C20 C 0.6950(14) -0.1034(11) 0.8661(10) 0.087(4) Uani 1 1 d . U . C 3
C21 C 0.7249(14) -0.1079(12) 0.7994(10) 0.086(4) Uani 1 1 d . U . C 3
C22 C 0.6406(14) -0.0339(14) 0.7603(8) 0.083(4) Uani 1 1 d . U . C 3
C23 C 0.6491(13) 0.0221(15) 0.7017(7) 0.082(4) Uani 1 1 d . U . C 3
C24 C 0.5767(11) 0.1242(15) 0.6859(6) 0.077(4) Uani 1 1 d . U . C 3
C25 C 0.4946(11) 0.1775(16) 0.7302(7) 0.079(4) Uani 1 1 d . U . C 3
C26 C 0.4426(10) 0.2856(18) 0.7293(8) 0.096(5) Uani 1 1 d . U . C 3
C27 C 0.3980(9) 0.3365(16) 0.7892(8) 0.090(5) Uani 1 1 d . U . C 3
C28 C 0.4004(11) 0.4300(14) 0.8078(10) 0.105(6) Uani 1 1 d . U . C 3
C29 C 0.4069(12) 0.4271(12) 0.8799(9) 0.083(4) Uani 1 1 d . U . C 3
C30 C 0.4690(17) 0.4584(13) 0.9107(12) 0.105(5) Uani 1 1 d . U . C 3
C31 C 0.5315(14) 0.3974(13) 0.9669(9) 0.086(4) Uani 1 1 d . U . C 3
C32 C 0.6353(15) 0.3822(14) 0.9728(9) 0.090(4) Uani 1 1 d . U . C 3
C33 C 0.6962(12) 0.2791(14) 1.0036(6) 0.076(4) Uani 1 1 d . U . C 3
C34 C 0.7998(11) 0.2254(13) 0.9876(6) 0.069(3) Uani 1 1 d . U . C 3
C35 C 0.8412(9) 0.1193(12) 0.9822(5) 0.064(3) Uani 1 1 d . U . C 3
C36 C 0.9276(9) 0.0694(13) 0.9381(6) 0.075(4) Uani 1 1 d . U . C 3
C37 C 0.9480(10) -0.0279(12) 0.9160(7) 0.077(4) Uani 1 1 d . U . C 3
C38 C 0.8869(12) -0.0726(11) 0.9382(9) 0.091(5) Uani 1 1 d . U . C 3
C39 C 0.8622(13) -0.1303(10) 0.8949(10) 0.089(5) Uani 1 1 d . U . C 3
C40 C 0.8956(14) -0.1434(10) 0.8278(11) 0.088(4) Uani 1 1 d . U . C 3
C41 C 0.8255(15) -0.1312(11) 0.7790(11) 0.090(4) Uani 1 1 d . U . C 3
C42 C 0.8352(15) -0.0914(12) 0.7122(10) 0.087(4) Uani 1 1 d . U . C 3
C43 C 0.7476(13) -0.0117(15) 0.6746(8) 0.084(4) Uani 1 1 d . U . C 3
C44 C 0.7776(12) 0.0464(15) 0.6352(6) 0.076(4) Uani 1 1 d . U . C 3
C45 C 0.7075(12) 0.1508(15) 0.6136(5) 0.076(4) Uani 1 1 d . U . C 3
C46 C 0.6067(12) 0.1913(17) 0.6377(6) 0.084(4) Uani 1 1 d . U . C 3
C47 C 0.5526(13) 0.2934(19) 0.6367(7) 0.104(6) Uani 1 1 d . U . C 3
C48 C 0.4709(11) 0.3436(19) 0.6823(8) 0.102(5) Uani 1 1 d . U . C 3
C49 C 0.4712(13) 0.4329(17) 0.6979(10) 0.116(7) Uani 1 1 d . U . C 3
C50 C 0.4437(14) 0.4720(15) 0.7624(12) 0.117(7) Uani 1 1 d . U . C 3
C51 C 0.5008(18) 0.5134(11) 0.7913(14) 0.113(6) Uani 1 1 d . U . C 3
C52 C 0.5220(16) 0.5019(11) 0.8632(13) 0.105(5) Uani 1 1 d . U . C 3
C53 C 0.6192(18) 0.4930(12) 0.8702(14) 0.110(5) Uani 1 1 d . U . C 3
C54 C 0.6785(16) 0.4340(15) 0.9269(11) 0.101(5) Uani 1 1 d . U . C 3
C55 C 0.7798(15) 0.3840(15) 0.9202(11) 0.097(4) Uani 1 1 d . U . C 3
C56 C 0.8441(13) 0.2802(15) 0.9505(7) 0.081(4) Uani 1 1 d . U . C 3
C57 C 0.5910(19) 0.5090(11) 0.7566(14) 0.119(6) Uani 1 1 d . U . C 3
C58 C 0.9292(11) 0.2287(14) 0.9096(6) 0.071(3) Uani 1 1 d . U . C 3
C59 C 0.9688(9) 0.1256(12) 0.8988(6) 0.064(3) Uani 1 1 d . U . C 3
C60 C 1.0182(8) 0.0926(12) 0.8345(6) 0.063(3) Uani 1 1 d . U . C 3
C61 C 1.0287(8) 0.0038(10) 0.8126(6) 0.056(3) Uani 1 1 d . U . C 3
C62 C 0.9969(9) -0.0577(10) 0.8516(8) 0.074(4) Uani 1 1 d . U . C 3
C63 C 0.9709(11) -0.1135(9) 0.8064(11) 0.083(4) Uani 1 1 d . U . C 3
C64 C 0.9930(11) -0.0887(10) 0.7425(9) 0.073(3) Uani 1 1 d . U . C 3
C65 C 0.9226(13) -0.0725(13) 0.6875(9) 0.081(4) Uani 1 1 d . U . C 3
C66 C 0.8841(11) 0.0142(13) 0.6422(7) 0.070(3) Uani 1 1 d . U . C 3
C67 C 0.9226(10) 0.0906(13) 0.6395(6) 0.065(3) Uani 1 1 d . U . C 3
C68 C 0.8594(10) 0.1839(13) 0.6129(6) 0.069(3) Uani 1 1 d . U . C 3
C69 C 0.7541(12) 0.2124(15) 0.5962(5) 0.074(4) Uani 1 1 d . U . C 3
C70 C 0.6999(14) 0.3191(16) 0.6039(6) 0.091(5) Uani 1 1 d . U . C 3
C71 C 0.6003(13) 0.3648(16) 0.6221(8) 0.107(6) Uani 1 1 d . U . C 3
C72 C 0.561(2) 0.4407(19) 0.6642(12) 0.141(8) Uani 1 1 d . U . C 3
C73 C 0.6201(17) 0.4723(12) 0.6961(12) 0.106(6) Uani 1 1 d . U . C 3
C74 C 0.6614(18) 0.4969(10) 0.8077(14) 0.107(5) Uani 1 1 d . U . C 3
C75 C 0.7712(17) 0.4445(11) 0.7969(12) 0.100(5) Uani 1 1 d . U . C 3
C76 C 0.8294(14) 0.3938(12) 0.8570(10) 0.087(4) Uani 1 1 d . U . C 3
C77 C 0.9227(13) 0.3036(13) 0.8524(8) 0.077(4) Uani 1 1 d . U . C 3
C78 C 0.9603(11) 0.2751(12) 0.7917(7) 0.069(3) Uani 1 1 d . U . C 3
C79 C 1.0170(9) 0.1647(11) 0.7844(7) 0.062(3) Uani 1 1 d . U . C 3
C80 C 1.0011(9) 0.1576(10) 0.7151(7) 0.057(3) Uani 1 1 d . U . C 3
C81 C 0.9966(8) 0.0754(10) 0.6934(6) 0.051(2) Uani 1 1 d . U . C 3
C82 C 1.0238(8) -0.0107(9) 0.7414(7) 0.056(3) Uani 1 1 d . U . C 3
C83 C 0.9086(12) 0.3264(11) 0.7324(8) 0.074(3) Uani 1 1 d . U . C 3
C84 C 0.9331(11) 0.2583(11) 0.6824(7) 0.067(3) Uani 1 1 d . U . C 3
C85 C 0.8662(12) 0.2679(12) 0.6337(6) 0.073(4) Uani 1 1 d . U . C 3
C86 C 0.7677(14) 0.3495(13) 0.6293(8) 0.086(4) Uani 1 1 d . U . C 3
C87 C 0.7345(16) 0.4215(11) 0.6777(10) 0.098(5) Uani 1 1 d . U . C 3
C88 C 0.8054(15) 0.4094(11) 0.7327(10) 0.090(4) Uani 1 1 d . U . C 3
C1B C 1.1554(10) -0.3739(9) 0.7378(7) 0.059(3) Uani 1 1 d . U . D 4
H1B H 1.1304 -0.4009 0.7073 0.071 Uiso 1 1 calc R U . D 4
C4B C 1.2287(8) -0.2928(8) 0.8318(5) 0.050(3) Uani 1 1 d . U . D 4
H4B H 1.2544 -0.2666 0.8624 0.060 Uiso 1 1 calc R U . D 4
C5B C 1.2343(9) -0.2775(8) 0.7630(5) 0.048(2) Uani 1 1 d . U . D 4
H5B H 1.2641 -0.2367 0.7479 0.057 Uiso 1 1 calc R U . D 4
C6B C 1.2009(8) -0.3155(7) 0.7129(6) 0.048(2) Uani 1 1 d . U . D 4
H6B H 1.2086 -0.3027 0.6670 0.057 Uiso 1 1 calc R U . D 4
C2B C 1.1454(10) -0.3938(10) 0.8052(8) 0.068(3) Uani 1 1 d . U . D 4
H2B H 1.1156 -0.4350 0.8192 0.081 Uiso 1 1 calc R U . D 4
C3B C 1.1781(10) -0.3546(11) 0.8519(6) 0.065(3) Uani 1 1 d . U . D 4
H3B H 1.1682 -0.3672 0.8974 0.078 Uiso 1 1 calc R U . D 4
C1D C 0.0857(15) 0.3573(16) 0.9600(8) 0.097(7) Uani 0.6 1 d G U P E 5
H1D H 0.0623 0.3432 0.9214 0.116 Uiso 0.6 1 calc R U P E 5
C3D C 0.1702(15) 0.3753(18) 0.9568(9) 0.099(7) Uani 0.6 1 d G U P E 5
H3D H 0.2033 0.3732 0.9162 0.118 Uiso 0.6 1 calc R U P E 5
C4D C 0.2053(14) 0.3964(19) 1.0145(11) 0.092(8) Uani 0.6 1 d G U P E 5
H4D H 0.2619 0.4084 1.0124 0.110 Uiso 0.6 1 calc R U P E 5
C5D C 0.1559(16) 0.3996(15) 1.0752(9) 0.071(5) Uani 0.6 1 d G U P E 5
H5D H 0.1794 0.4137 1.1138 0.085 Uiso 0.6 1 calc R U P E 5
C6D C 0.0714(14) 0.3816(13) 1.0784(8) 0.087(6) Uani 0.6 1 d G U P E 5
H6D H 0.0384 0.3837 1.1190 0.104 Uiso 0.6 1 calc R U P E 5
C7D C 0.0363(11) 0.3605(14) 1.0207(10) 0.086(6) Uani 0.6 1 d G U P E 5
H7D H -0.0202 0.3485 1.0228 0.103 Uiso 0.6 1 calc R U P E 5
C1E C 0.190(3) 0.332(3) 0.9839(11) 0.089(8) Uani 0.4 1 d D U P F 6
S1E S 0.1469(13) 0.3101(14) 0.9233(8) 0.128(5) Uani 0.4 1 d D . P F 6
S2E S 0.2106(17) 0.3798(18) 1.0410(10) 0.136(7) Uani 0.4 1 d D . P F 6


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu6 1.132(17) . ?
Lu1 C1C 1.725(18) . ?
Lu1 Lu23 2.06(4) . ?
Lu1 Lu18 2.07(2) . ?
Lu1 Lu20 2.14(2) . ?
Lu1 Lu3 2.265(6) . ?
Lu1 Lu4 2.445(9) . ?
Lu1 Lu8 2.618(13) . ?
Lu1 Lu21 2.64(3) . ?
Lu1 C2C 2.752(10) . ?
Lu1 C3C 2.78(2) . ?
Lu1 Lu5 2.85(3) . ?
Lu2 Lu4 1.09(2) . ?
Lu2 Lu22 1.10(3) . ?
Lu2 Lu3 1.41(2) . ?
Lu2 Lu5 1.49(3) . ?
Lu2 Lu20 1.56(3) . ?
Lu2 Lu18 1.63(3) . ?
Lu2 Lu21 1.79(4) . ?
Lu2 C2C 2.147(19) . ?
Lu2 C3C 2.43(3) . ?
Lu2 Lu6 2.59(3) . ?
Lu2 Lu23 2.59(5) . ?
Lu2 C1C 2.79(2) . ?
Lu3 Lu20 0.75(3) . ?
Lu3 Lu21 0.83(4) . ?
Lu3 Lu5 0.90(3) . ?
Lu3 Lu18 1.03(3) . ?
Lu3 Lu22 1.21(3) . ?
Lu3 Lu6 1.272(17) . ?
Lu3 Lu23 1.62(4) . ?
Lu3 C1C 2.37(2) . ?
Lu3 C2C 2.394(12) . ?
Lu3 C3C 2.71(3) . ?
Lu4 Lu5 0.83(3) . ?
Lu4 Lu20 0.87(3) . ?
Lu4 Lu18 0.90(3) . ?
Lu4 Lu21 1.08(4) . ?
Lu4 Lu22 1.13(3) . ?
Lu4 Lu6 1.536(18) . ?
Lu4 Lu23 1.87(5) . ?
Lu4 C2C 2.248(15) . ?
Lu4 C1C 2.38(2) . ?
Lu4 C3C 2.51(3) . ?
Lu5 Lu18 1.13(3) . ?
Lu5 Lu21 1.45(5) . ?
Lu5 Lu20 1.62(4) . ?
Lu5 Lu22 1.78(4) . ?
Lu5 Lu6 1.84(3) . ?
Lu5 Lu23 2.47(5) . ?
Lu6 Lu20 1.37(3) . ?
Lu6 Lu18 1.42(3) . ?
Lu6 Lu23 1.51(4) . ?
Lu6 Lu21 1.62(4) . ?
Lu6 C1C 2.08(3) . ?
Lu6 Lu22 2.24(4) . ?
Lu6 C2C 2.713(18) . ?
Lu7 Lu15 0.63(3) . ?
Lu7 Lu12 0.74(3) . ?
Lu7 Lu14 0.83(3) . ?
Lu7 Lu10 0.96(3) . ?
Lu7 Lu9 1.00(4) . ?
Lu7 Lu17 1.22(6) . ?
Lu7 Lu19 1.22(2) . ?
Lu7 Lu24 1.25(4) . ?
Lu7 Lu13 1.28(5) . ?
Lu7 Lu8 1.571(13) . ?
Lu7 Lu11 2.336(5) . ?
Lu7 C1C 2.40(2) . ?
Lu8 Lu10 0.98(3) . ?
Lu8 Lu16 1.34(2) . ?
Lu8 Lu13 1.39(4) . ?
Lu8 Lu14 1.59(3) . ?
Lu8 Lu15 1.72(3) . ?
Lu8 Lu9 1.77(3) . ?
Lu8 C1C 1.84(2) . ?
Lu8 Lu24 1.91(4) . ?
Lu8 Lu12 2.00(3) . ?
Lu8 Lu17 2.33(6) . ?
Lu8 Lu19 2.61(2) . ?
Lu9 Lu13 0.66(4) . ?
Lu9 Lu16 0.85(3) . ?
Lu9 Lu12 1.09(4) . ?
Lu9 Lu24 1.26(5) . ?
Lu9 Lu19 1.43(4) . ?
Lu9 Lu14 1.48(4) . ?
Lu9 Lu10 1.61(4) . ?
Lu9 Lu15 1.63(5) . ?
Lu9 C1C 2.14(3) . ?
Lu9 Lu17 2.16(7) . ?
Lu10 Lu14 0.71(3) . ?
Lu10 Lu16 0.88(3) . ?
Lu10 Lu15 0.89(3) . ?
Lu10 Lu17 1.39(6) . ?
Lu10 Lu12 1.61(4) . ?
Lu10 Lu13 1.61(5) . ?
Lu10 Lu24 1.88(5) . ?
Lu10 Lu19 1.88(4) . ?
Lu10 C1C 1.98(3) . ?
Lu11 Lu19 1.17(2) . ?
Lu11 C2C 2.004(11) . ?
Lu11 Lu14 2.21(3) . ?
Lu11 C3C 2.26(2) . ?
Lu11 Lu16 2.450(17) . ?
Lu11 Lu17 2.51(5) . ?
Lu11 Lu12 2.59(3) . ?
Lu11 Lu15 2.63(2) . ?
Lu11 Lu13 2.83(5) . ?
Lu12 Lu24 0.72(4) . ?
Lu12 Lu16 0.82(3) . ?
Lu12 Lu15 1.12(4) . ?
Lu12 Lu13 1.33(5) . ?
Lu12 Lu19 1.52(3) . ?
Lu12 Lu14 1.57(4) . ?
Lu12 Lu17 1.65(6) . ?
Lu13 Lu16 1.03(5) . ?
Lu13 Lu24 1.15(6) . ?
Lu13 Lu14 1.76(5) . ?
Lu13 Lu15 1.84(6) . ?
Lu13 Lu19 2.05(5) . ?
Lu13 C1C 2.10(4) . ?
Lu13 Lu17 2.48(8) . ?
Lu14 Lu15 0.84(3) . ?
Lu14 Lu16 0.89(3) . ?
Lu14 Lu17 1.08(6) . ?
Lu14 Lu19 1.26(4) . ?
Lu14 C3C 1.67(4) . ?
Lu14 C1C 1.97(3) . ?
Lu15 Lu17 0.72(5) . ?
Lu15 Lu16 0.83(3) . ?
Lu15 Lu19 1.49(3) . ?
Lu15 Lu24 1.63(5) . ?
Lu15 C3C 2.49(3) . ?
Lu16 Lu24 1.18(5) . ?
Lu16 Lu19 1.40(3) . ?
Lu16 Lu17 1.46(6) . ?
Lu16 C1C 2.21(2) . ?
Lu16 C3C 2.42(3) . ?
Lu17 Lu19 1.47(6) . ?
Lu17 Lu24 2.26(7) . ?
Lu17 C3C 2.43(6) . ?
Lu18 Lu20 1.46(3) . ?
Lu18 Lu21 1.86(5) . ?
Lu18 Lu22 1.95(4) . ?
Lu18 C3C 2.18(3) . ?
Lu18 C1C 2.24(3) . ?
Lu18 C2C 2.33(2) . ?
Lu19 C3C 2.14(3) . ?
Lu19 C2C 2.15(3) . ?
Lu20 Lu21 0.87(4) . ?
Lu20 Lu22 0.91(3) . ?
Lu20 Lu23 1.07(5) . ?
Lu20 C1C 1.87(3) . ?
Lu20 C2C 1.89(3) . ?
Lu21 Lu22 1.07(5) . ?
Lu21 Lu23 1.26(5) . ?
Lu21 C1C 2.70(4) . ?
Lu21 C2C 2.71(4) . ?
Lu22 Lu23 1.68(5) . ?
Lu22 C2C 2.02(3) . ?
Lu22 C1C 2.46(4) . ?
Lu22 C3C 2.72(4) . ?
Lu23 C1C 2.03(5) . ?
Lu23 C2C 2.42(4) . ?
C1C C2C 1.203(19) . ?
C1C C3C 1.56(3) . ?
C2C C3C 1.13(2) . ?
Ni1A N1A 1.966(6) . ?
Ni1A N3A 1.969(6) . ?
Ni1A N2A 1.977(6) . ?
Ni1A N4A 1.978(6) . ?
N1A C8A 1.353(10) . ?
N1A C1A 1.380(9) . ?
N2A C10A 1.368(10) . ?
N2A C16A 1.380(9) . ?
N3A C35A 1.353(10) . ?
N3A C18A 1.375(9) . ?
N4A C26A 1.360(10) . ?
N4A C33A 1.381(9) . ?
C1A C34A 1.358(11) . ?
C1A C2A 1.453(10) . ?
C2A C5A 1.354(11) . ?
C2A C3A 1.500(9) . ?
C3A C4A 1.508(10) . ?
C5A C8A 1.446(9) . ?
C5A C6A 1.502(11) . ?
C6A C7A 1.525(11) . ?
C8A C9A 1.386(11) . ?
C9A C10A 1.366(10) . ?
C10A C11A 1.456(11) . ?
C11A C13A 1.355(11) . ?
C11A C12A 1.505(12) . ?
C12A C36A 1.527(14) . ?
C13A C16A 1.419(11) . ?
C13A C14A 1.511(10) . ?
C14A C15A 1.520(11) . ?
C16A C17A 1.376(10) . ?
C17A C18A 1.364(11) . ?
C18A C19A 1.458(10) . ?
C19A C22A 1.349(11) . ?
C19A C20A 1.496(10) . ?
C20A C21A 1.527(11) . ?
C22A C35A 1.460(9) . ?
C22A C23A 1.496(10) . ?
C23A C24A 1.531(11) . ?
C25A C35A 1.378(11) . ?
C25A C26A 1.383(10) . ?
C26A C27A 1.453(11) . ?
C27A C30A 1.362(11) . ?
C27A C28A 1.478(12) . ?
C28A C29A 1.523(12) . ?
C30A C33A 1.420(11) . ?
C30A C31A 1.519(9) . ?
C31A C32A 1.496(13) . ?
C33A C34A 1.387(11) . ?
C1 C9 1.36(2) . ?
C1 C2 1.416(19) . ?
C1 C5 1.45(2) . ?
C2 C12 1.402(19) . ?
C2 C3 1.407(19) . ?
C3 C4 1.38(2) . ?
C3 C15 1.462(19) . ?
C4 C18 1.35(2) . ?
C4 C5 1.44(2) . ?
C5 C6 1.32(2) . ?
C6 C20 1.44(2) . ?
C6 C7 1.47(2) . ?
C7 C8 1.41(2) . ?
C7 C22 1.44(2) . ?
C8 C25 1.48(2) . ?
C8 C9 1.503(19) . ?
C9 C10 1.48(2) . ?
C10 C11 1.39(2) . ?
C10 C27 1.39(2) . ?
C11 C12 1.475(18) . ?
C11 C29 1.49(2) . ?
C12 C13 1.416(18) . ?
C13 C31 1.41(2) . ?
C13 C14 1.45(2) . ?
C14 C33 1.370(19) . ?
C14 C15 1.40(2) . ?
C15 C16 1.48(2) . ?
C16 C17 1.38(2) . ?
C16 C35 1.472(18) . ?
C17 C18 1.41(2) . ?
C17 C38 1.42(2) . ?
C18 C19 1.43(3) . ?
C19 C39 1.39(2) . ?
C19 C20 1.40(3) . ?
C20 C21 1.39(2) . ?
C21 C22 1.41(3) . ?
C21 C41 1.42(2) . ?
C22 C23 1.41(2) . ?
C23 C43 1.41(2) . ?
C23 C24 1.42(2) . ?
C24 C25 1.44(2) . ?
C24 C46 1.53(2) . ?
C25 C26 1.44(3) . ?
C26 C48 1.40(3) . ?
C26 C27 1.45(3) . ?
C27 C28 1.50(3) . ?
C28 C50 1.36(3) . ?
C28 C29 1.44(3) . ?
C29 C30 1.38(3) . ?
C30 C31 1.42(3) . ?
C30 C52 1.50(3) . ?
C31 C32 1.45(2) . ?
C32 C54 1.46(3) . ?
C32 C33 1.47(3) . ?
C33 C34 1.41(2) . ?
C34 C56 1.42(2) . ?
C34 C35 1.44(2) . ?
C35 C36 1.47(2) . ?
C36 C59 1.42(2) . ?
C36 C37 1.46(2) . ?
C37 C38 1.39(2) . ?
C37 C62 1.46(2) . ?
C38 C39 1.44(3) . ?
C39 C40 1.41(3) . ?
C40 C41 1.38(3) . ?
C40 C63 1.42(2) . ?
C41 C42 1.44(3) . ?
C42 C43 1.46(3) . ?
C42 C65 1.50(2) . ?
C43 C44 1.34(2) . ?
C44 C66 1.42(2) . ?
C44 C45 1.46(2) . ?
C45 C69 1.40(2) . ?
C45 C46 1.41(2) . ?
C46 C47 1.36(3) . ?
C47 C48 1.44(3) . ?
C47 C71 1.53(3) . ?
C48 C49 1.41(3) . ?
C49 C50 1.43(3) . ?
C49 C72 1.52(3) . ?
C50 C51 1.41(3) . ?
C51 C52 1.45(3) . ?
C51 C57 1.46(3) . ?
C52 C53 1.39(3) . ?
C53 C74 1.38(3) . ?
C53 C54 1.40(3) . ?
C54 C55 1.34(3) . ?
C55 C76 1.47(3) . ?
C55 C56 1.48(3) . ?
C56 C58 1.42(2) . ?
C57 C73 1.35(3) . ?
C57 C74 1.41(3) . ?
C58 C59 1.42(2) . ?
C58 C77 1.50(2) . ?
C59 C60 1.468(18) . ?
C60 C61 1.38(2) . ?
C60 C79 1.40(2) . ?
C61 C62 1.387(18) . ?
C61 C82 1.462(19) . ?
C62 C63 1.45(3) . ?
C63 C64 1.37(2) . ?
C64 C82 1.437(17) . ?
C64 C65 1.45(2) . ?
C65 C66 1.40(2) . ?
C66 C67 1.49(2) . ?
C67 C68 1.34(2) . ?
C67 C81 1.475(16) . ?
C68 C85 1.41(2) . ?
C68 C69 1.446(19) . ?
C69 C70 1.45(3) . ?
C70 C71 1.36(2) . ?
C70 C86 1.40(2) . ?
C71 C72 1.37(3) . ?
C72 C73 1.36(3) . ?
C73 C87 1.55(3) . ?
C74 C75 1.46(3) . ?
C75 C88 1.42(3) . ?
C75 C76 1.42(3) . ?
C76 C77 1.43(2) . ?
C77 C78 1.34(2) . ?
C78 C83 1.38(2) . ?
C78 C79 1.50(2) . ?
C79 C80 1.426(18) . ?
C80 C81 1.376(17) . ?
C80 C84 1.47(2) . ?
C81 C82 1.434(17) . ?
C83 C84 1.42(2) . ?
C83 C88 1.46(2) . ?
C84 C85 1.35(2) . ?
C85 C86 1.40(2) . ?
C86 C87 1.42(3) . ?
C87 C88 1.47(3) . ?
C1B C2B 1.366(19) . ?
C1B C6B 1.383(16) . ?
C4B C5B 1.374(15) . ?
C4B C3B 1.460(18) . ?
C5B C6B 1.397(16) . ?
C2B C3B 1.35(2) . ?
C1D C3D 1.3900 . ?
C1D C7D 1.3900 . ?
C3D C4D 1.3900 . ?
C4D C5D 1.3900 . ?
C5D C6D 1.3900 . ?
C6D C7D 1.3900 . ?
C1E S2E 1.507(10) . ?
C1E S1E 1.507(10) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu6 Lu1 C1C 90.8(10) . . ?
Lu6 Lu1 Lu23 45.8(14) . . ?
C1C Lu1 Lu23 64.1(12) . . ?
Lu6 Lu1 Lu18 40.7(11) . . ?
C1C Lu1 Lu18 71.7(8) . . ?
Lu23 Lu1 Lu18 69.2(14) . . ?
Lu6 Lu1 Lu20 34.6(10) . . ?
C1C Lu1 Lu20 56.6(9) . . ?
Lu23 Lu1 Lu20 29.5(13) . . ?
Lu18 Lu1 Lu20 40.5(9) . . ?
Lu6 Lu1 Lu3 20.9(8) . . ?
C1C Lu1 Lu3 71.5(6) . . ?
Lu23 Lu1 Lu3 43.6(12) . . ?
Lu18 Lu1 Lu3 27.1(7) . . ?
Lu20 Lu1 Lu3 19.2(7) . . ?
Lu6 Lu1 Lu4 27.8(8) . . ?
C1C Lu1 Lu4 66.9(6) . . ?
Lu23 Lu1 Lu4 48.1(13) . . ?
Lu18 Lu1 Lu4 21.1(8) . . ?
Lu20 Lu1 Lu4 20.5(8) . . ?
Lu3 Lu1 Lu4 7.6(3) . . ?
Lu6 Lu1 Lu8 135.4(8) . . ?
C1C Lu1 Lu8 44.6(7) . . ?
Lu23 Lu1 Lu8 100.0(11) . . ?
Lu18 Lu1 Lu8 108.8(6) . . ?
Lu20 Lu1 Lu8 100.9(7) . . ?
Lu3 Lu1 Lu8 115.8(3) . . ?
Lu4 Lu1 Lu8 110.5(3) . . ?
Lu6 Lu1 Lu21 20.3(10) . . ?
C1C Lu1 Lu21 73.3(9) . . ?
Lu23 Lu1 Lu21 27.8(14) . . ?
Lu18 Lu1 Lu21 44.7(12) . . ?
Lu20 Lu1 Lu21 17.2(8) . . ?
Lu3 Lu1 Lu21 17.6(8) . . ?
Lu4 Lu1 Lu21 24.2(9) . . ?
Lu8 Lu1 Lu21 117.0(7) . . ?
Lu6 Lu1 C2C 76.1(8) . . ?
C1C Lu1 C2C 16.5(6) . . ?
Lu23 Lu1 C2C 58.2(11) . . ?
Lu18 Lu1 C2C 55.5(6) . . ?
Lu20 Lu1 C2C 43.2(7) . . ?
Lu3 Lu1 C2C 56.0(3) . . ?
Lu4 Lu1 C2C 50.8(3) . . ?
Lu8 Lu1 C2C 59.9(3) . . ?
Lu21 Lu1 C2C 60.4(7) . . ?
Lu6 Lu1 C3C 84.7(10) . . ?
C1C Lu1 C3C 30.4(7) . . ?
Lu23 Lu1 C3C 80.1(12) . . ?
Lu18 Lu1 C3C 50.9(7) . . ?
Lu20 Lu1 C3C 58.6(8) . . ?
Lu3 Lu1 C3C 64.1(5) . . ?
Lu4 Lu1 C3C 56.9(5) . . ?
Lu8 Lu1 C3C 57.9(6) . . ?
Lu21 Lu1 C3C 74.9(9) . . ?
C2C Lu1 C3C 23.6(5) . . ?
Lu6 Lu1 Lu5 21.3(11) . . ?
C1C Lu1 Lu5 82.0(8) . . ?
Lu23 Lu1 Lu5 57.8(13) . . ?
Lu18 Lu1 Lu5 19.6(8) . . ?
Lu20 Lu1 Lu5 34.4(9) . . ?
Lu3 Lu1 Lu5 15.3(5) . . ?
Lu4 Lu1 Lu5 15.8(5) . . ?
Lu8 Lu1 Lu5 124.2(6) . . ?
Lu21 Lu1 Lu5 30.3(9) . . ?
C2C Lu1 Lu5 65.7(6) . . ?
C3C Lu1 Lu5 67.6(8) . . ?
Lu4 Lu2 Lu22 62(2) . . ?
Lu4 Lu2 Lu3 7.4(7) . . ?
Lu22 Lu2 Lu3 55.9(19) . . ?
Lu4 Lu2 Lu5 33.4(14) . . ?
Lu22 Lu2 Lu5 86(2) . . ?
Lu3 Lu2 Lu5 35.9(12) . . ?
Lu4 Lu2 Lu20 32.7(11) . . ?
Lu22 Lu2 Lu20 35.1(18) . . ?
Lu3 Lu2 Lu20 28.6(10) . . ?
Lu5 Lu2 Lu20 64.5(17) . . ?
Lu4 Lu2 Lu18 31.5(12) . . ?
Lu22 Lu2 Lu18 89(2) . . ?
Lu3 Lu2 Lu18 38.8(10) . . ?
Lu5 Lu2 Lu18 42.4(14) . . ?
Lu20 Lu2 Lu18 54.5(13) . . ?
Lu4 Lu2 Lu21 34.6(12) . . ?
Lu22 Lu2 Lu21 34.2(19) . . ?
Lu3 Lu2 Lu21 27.2(12) . . ?
Lu5 Lu2 Lu21 51.7(16) . . ?
Lu20 Lu2 Lu21 29.1(12) . . ?
Lu18 Lu2 Lu21 65.9(17) . . ?
Lu4 Lu2 C2C 80.9(10) . . ?
Lu22 Lu2 C2C 68.2(17) . . ?
Lu3 Lu2 C2C 81.7(8) . . ?
Lu5 Lu2 C2C 112.3(15) . . ?
Lu20 Lu2 C2C 58.8(10) . . ?
Lu18 Lu2 C2C 74.7(9) . . ?
Lu21 Lu2 C2C 86.8(12) . . ?
Lu4 Lu2 C3C 81.4(12) . . ?
Lu22 Lu2 C3C 93.2(18) . . ?
Lu3 Lu2 C3C 85.5(10) . . ?
Lu5 Lu2 C3C 103.8(15) . . ?
Lu20 Lu2 C3C 73.0(12) . . ?
Lu18 Lu2 C3C 61.4(10) . . ?
Lu21 Lu2 C3C 101.7(14) . . ?
C2C Lu2 C3C 27.8(6) . . ?
Lu4 Lu2 Lu6 11.7(8) . . ?
Lu22 Lu2 Lu6 59.8(19) . . ?
Lu3 Lu2 Lu6 14.8(5) . . ?
Lu5 Lu2 Lu6 44.4(13) . . ?
Lu20 Lu2 Lu6 26.0(10) . . ?
Lu18 Lu2 Lu6 29.8(10) . . ?
Lu21 Lu2 Lu6 38.4(13) . . ?
C2C Lu2 Lu6 69.3(7) . . ?
C3C Lu2 Lu6 70.8(8) . . ?
Lu4 Lu2 Lu23 39.0(12) . . ?
Lu22 Lu2 Lu23 27(2) . . ?
Lu3 Lu2 Lu23 33.8(9) . . ?
Lu5 Lu2 Lu23 68.9(15) . . ?
Lu20 Lu2 Lu23 8.6(12) . . ?
Lu18 Lu2 Lu23 63.0(13) . . ?
Lu21 Lu2 Lu23 26.2(13) . . ?
C2C Lu2 Lu23 60.7(10) . . ?
C3C Lu2 Lu23 78.2(11) . . ?
Lu6 Lu2 Lu23 33.9(10) . . ?
Lu4 Lu2 C1C 57.0(9) . . ?
Lu22 Lu2 C1C 61.6(18) . . ?
Lu3 Lu2 C1C 58.3(7) . . ?
Lu5 Lu2 C1C 88.4(14) . . ?
Lu20 Lu2 C1C 39.5(10) . . ?
Lu18 Lu2 C1C 53.7(9) . . ?
Lu21 Lu2 C1C 68.5(12) . . ?
C2C Lu2 C1C 24.0(5) . . ?
C3C Lu2 C1C 34.0(7) . . ?
Lu6 Lu2 C1C 45.3(6) . . ?
Lu23 Lu2 C1C 44.2(10) . . ?
Lu20 Lu3 Lu21 66(2) . . ?
Lu20 Lu3 Lu5 163(3) . . ?
Lu21 Lu3 Lu5 114(3) . . ?
Lu20 Lu3 Lu18 109(2) . . ?
Lu21 Lu3 Lu18 173(2) . . ?
Lu5 Lu3 Lu18 72(2) . . ?
Lu20 Lu3 Lu22 49(2) . . ?
Lu21 Lu3 Lu22 60(3) . . ?
Lu5 Lu3 Lu22 115(2) . . ?
Lu18 Lu3 Lu22 121(2) . . ?
Lu20 Lu3 Lu6 80.9(18) . . ?
Lu21 Lu3 Lu6 99(2) . . ?
Lu5 Lu3 Lu6 115.4(18) . . ?
Lu18 Lu3 Lu6 75.4(15) . . ?
Lu22 Lu3 Lu6 129.6(17) . . ?
Lu20 Lu3 Lu2 86.4(19) . . ?
Lu21 Lu3 Lu2 102(2) . . ?
Lu5 Lu3 Lu2 76.6(18) . . ?
Lu18 Lu3 Lu2 82.1(15) . . ?
Lu22 Lu3 Lu2 48.7(16) . . ?
Lu6 Lu3 Lu2 148.8(11) . . ?
Lu20 Lu3 Lu23 33(2) . . ?
Lu21 Lu3 Lu23 50(3) . . ?
Lu5 Lu3 Lu23 159(2) . . ?
Lu18 Lu3 Lu23 123.3(19) . . ?
Lu22 Lu3 Lu23 71(2) . . ?
Lu6 Lu3 Lu23 61.6(15) . . ?
Lu2 Lu3 Lu23 117.1(15) . . ?
Lu20 Lu3 Lu1 71.0(16) . . ?
Lu21 Lu3 Lu1 107(2) . . ?
Lu5 Lu3 Lu1 122.9(16) . . ?
Lu18 Lu3 Lu1 66.1(12) . . ?
Lu22 Lu3 Lu1 119.2(14) . . ?
Lu6 Lu3 Lu1 18.5(7) . . ?
Lu2 Lu3 Lu1 130.5(7) . . ?
Lu23 Lu3 Lu1 61.5(14) . . ?
Lu20 Lu3 C1C 40.5(18) . . ?
Lu21 Lu3 C1C 104(2) . . ?
Lu5 Lu3 C1C 141.3(19) . . ?
Lu18 Lu3 C1C 70.2(11) . . ?
Lu22 Lu3 C1C 79.7(15) . . ?
Lu6 Lu3 C1C 60.9(8) . . ?
Lu2 Lu3 C1C 91.2(8) . . ?
Lu23 Lu3 C1C 57.5(15) . . ?
Lu1 Lu3 C1C 43.6(4) . . ?
Lu20 Lu3 C2C 40.5(19) . . ?
Lu21 Lu3 C2C 104(2) . . ?
Lu5 Lu3 C2C 129.2(19) . . ?
Lu18 Lu3 C2C 73.8(11) . . ?
Lu22 Lu3 C2C 57.2(15) . . ?
Lu6 Lu3 C2C 90.1(8) . . ?
Lu2 Lu3 C2C 62.6(7) . . ?
Lu23 Lu3 C2C 71.2(14) . . ?
Lu1 Lu3 C2C 72.4(3) . . ?
C1C Lu3 C2C 29.2(5) . . ?
Lu20 Lu3 C3C 64(2) . . ?
Lu21 Lu3 C3C 128(2) . . ?
Lu5 Lu3 C3C 110.1(19) . . ?
Lu18 Lu3 C3C 49.2(12) . . ?
Lu22 Lu3 C3C 77.5(16) . . ?
Lu6 Lu3 C3C 85.6(9) . . ?
Lu2 Lu3 C3C 63.3(8) . . ?
Lu23 Lu3 C3C 90.3(15) . . ?
Lu1 Lu3 C3C 67.3(5) . . ?
C1C Lu3 C3C 35.0(6) . . ?
C2C Lu3 C3C 24.6(5) . . ?
Lu5 Lu4 Lu20 145(3) . . ?
Lu5 Lu4 Lu18 81(2) . . ?
Lu20 Lu4 Lu18 111(2) . . ?
Lu5 Lu4 Lu21 98(3) . . ?
Lu20 Lu4 Lu21 51(2) . . ?
Lu18 Lu4 Lu21 139(2) . . ?
Lu5 Lu4 Lu2 101(2) . . ?
Lu20 Lu4 Lu2 104.8(18) . . ?
Lu18 Lu4 Lu2 110(2) . . ?
Lu21 Lu4 Lu2 110.7(18) . . ?
Lu5 Lu4 Lu22 130(2) . . ?
Lu20 Lu4 Lu22 52.2(19) . . ?
Lu18 Lu4 Lu22 147(2) . . ?
Lu21 Lu4 Lu22 58(2) . . ?
Lu2 Lu4 Lu22 59.1(19) . . ?
Lu5 Lu4 Lu6 98(2) . . ?
Lu20 Lu4 Lu6 62.4(16) . . ?
Lu18 Lu4 Lu6 65.4(17) . . ?
Lu21 Lu4 Lu6 74.3(17) . . ?
Lu2 Lu4 Lu6 160.0(13) . . ?
Lu22 Lu4 Lu6 113.6(18) . . ?
Lu5 Lu4 Lu23 128(2) . . ?
Lu20 Lu4 Lu23 17.4(19) . . ?
Lu18 Lu4 Lu23 110.6(19) . . ?
Lu21 Lu4 Lu23 40(2) . . ?
Lu2 Lu4 Lu23 119.5(16) . . ?
Lu22 Lu4 Lu23 62(2) . . ?
Lu6 Lu4 Lu23 51.5(13) . . ?
Lu5 Lu4 C2C 159(2) . . ?
Lu20 Lu4 C2C 55.0(16) . . ?
Lu18 Lu4 C2C 83.5(13) . . ?
Lu21 Lu4 C2C 103.5(17) . . ?
Lu2 Lu4 C2C 70.5(10) . . ?
Lu22 Lu4 C2C 63.4(16) . . ?
Lu6 Lu4 C2C 89.5(8) . . ?
Lu23 Lu4 C2C 71.3(12) . . ?
Lu5 Lu4 C1C 149.3(19) . . ?
Lu20 Lu4 C1C 45.2(17) . . ?
Lu18 Lu4 C1C 70.6(13) . . ?
Lu21 Lu4 C1C 95.5(18) . . ?
Lu2 Lu4 C1C 100.4(11) . . ?
Lu22 Lu4 C1C 80.7(16) . . ?
Lu6 Lu4 C1C 59.6(8) . . ?
Lu23 Lu4 C1C 55.5(13) . . ?
C2C Lu4 C1C 30.0(5) . . ?
Lu5 Lu4 Lu1 111.1(18) . . ?
Lu20 Lu4 Lu1 59.6(15) . . ?
Lu18 Lu4 Lu1 55.7(14) . . ?
Lu21 Lu4 Lu1 87.9(17) . . ?
Lu2 Lu4 Lu1 140.8(11) . . ?
Lu22 Lu4 Lu1 111.2(17) . . ?
Lu6 Lu4 Lu1 20.1(7) . . ?
Lu23 Lu4 Lu1 55.1(12) . . ?
C2C Lu4 Lu1 71.7(4) . . ?
C1C Lu4 Lu1 41.9(4) . . ?
Lu5 Lu4 C3C 133(2) . . ?
Lu20 Lu4 C3C 77.6(18) . . ?
Lu18 Lu4 C3C 58.9(14) . . ?
Lu21 Lu4 C3C 128.6(18) . . ?
Lu2 Lu4 C3C 73.3(11) . . ?
Lu22 Lu4 C3C 88.2(17) . . ?
Lu6 Lu4 C3C 88.4(9) . . ?
Lu23 Lu4 C3C 91.4(14) . . ?
C2C Lu4 C3C 26.8(6) . . ?
C1C Lu4 C3C 37.2(6) . . ?
Lu1 Lu4 C3C 68.3(5) . . ?
Lu4 Lu5 Lu3 23.8(10) . . ?
Lu4 Lu5 Lu18 52(2) . . ?
Lu3 Lu5 Lu18 60(2) . . ?
Lu4 Lu5 Lu21 48(2) . . ?
Lu3 Lu5 Lu21 31.7(18) . . ?
Lu18 Lu5 Lu21 91(3) . . ?
Lu4 Lu5 Lu2 46.0(16) . . ?
Lu3 Lu5 Lu2 67.5(18) . . ?
Lu18 Lu5 Lu2 76(2) . . ?
Lu21 Lu5 Lu2 74.9(19) . . ?
Lu4 Lu5 Lu20 17.7(16) . . ?
Lu3 Lu5 Lu20 7.8(12) . . ?
Lu18 Lu5 Lu20 61(2) . . ?
Lu21 Lu5 Lu20 32.2(16) . . ?
Lu2 Lu5 Lu20 59.8(14) . . ?
Lu4 Lu5 Lu22 29.4(16) . . ?
Lu3 Lu5 Lu22 37.9(15) . . ?
Lu18 Lu5 Lu22 81(2) . . ?
Lu21 Lu5 Lu22 37.1(18) . . ?
Lu2 Lu5 Lu22 37.8(14) . . ?
Lu20 Lu5 Lu22 30.6(12) . . ?
Lu4 Lu5 Lu6 55.7(17) . . ?
Lu3 Lu5 Lu6 38.6(13) . . ?
Lu18 Lu5 Lu6 50.5(17) . . ?
Lu21 Lu5 Lu6 57.6(17) . . ?
Lu2 Lu5 Lu6 101.3(18) . . ?
Lu20 Lu5 Lu6 46.0(11) . . ?
Lu22 Lu5 Lu6 76.5(16) . . ?
Lu4 Lu5 Lu23 36.3(19) . . ?
Lu3 Lu5 Lu23 13.3(16) . . ?
Lu18 Lu5 Lu23 70(2) . . ?
Lu21 Lu5 Lu23 22.3(17) . . ?
Lu2 Lu5 Lu23 77.1(16) . . ?
Lu20 Lu5 Lu23 18.8(12) . . ?
Lu22 Lu5 Lu23 42.7(15) . . ?
Lu6 Lu5 Lu23 37.4(12) . . ?
Lu4 Lu5 Lu1 53.1(16) . . ?
Lu3 Lu5 Lu1 41.8(13) . . ?
Lu18 Lu5 Lu1 37.8(16) . . ?
Lu21 Lu5 Lu1 66.6(16) . . ?
Lu2 Lu5 Lu1 96.3(15) . . ?
Lu20 Lu5 Lu1 48.1(10) . . ?
Lu22 Lu5 Lu1 78.4(14) . . ?
Lu6 Lu5 Lu1 12.9(7) . . ?
Lu23 Lu5 Lu1 44.8(11) . . ?
Lu1 Lu6 Lu3 140.7(14) . . ?
Lu1 Lu6 Lu20 117.3(16) . . ?
Lu3 Lu6 Lu20 32.6(12) . . ?
Lu1 Lu6 Lu18 108.0(16) . . ?
Lu3 Lu6 Lu18 44.6(12) . . ?
Lu20 Lu6 Lu18 63.1(16) . . ?
Lu1 Lu6 Lu23 101.6(19) . . ?
Lu3 Lu6 Lu23 70.5(18) . . ?
Lu20 Lu6 Lu23 43.4(18) . . ?
Lu18 Lu6 Lu23 106(2) . . ?
Lu1 Lu6 Lu4 132.1(14) . . ?
Lu3 Lu6 Lu4 10.1(5) . . ?
Lu20 Lu6 Lu4 34.2(13) . . ?
Lu18 Lu6 Lu4 35.3(12) . . ?
Lu23 Lu6 Lu4 75.8(18) . . ?
Lu1 Lu6 Lu21 145.7(16) . . ?
Lu3 Lu6 Lu21 30.6(14) . . ?
Lu20 Lu6 Lu21 32.3(13) . . ?
Lu18 Lu6 Lu21 75.2(19) . . ?
Lu23 Lu6 Lu21 47(2) . . ?
Lu4 Lu6 Lu21 40.0(15) . . ?
Lu1 Lu6 Lu5 145.8(17) . . ?
Lu3 Lu6 Lu5 26.0(9) . . ?
Lu20 Lu6 Lu5 58.5(16) . . ?
Lu18 Lu6 Lu5 38.0(13) . . ?
Lu23 Lu6 Lu5 94.6(19) . . ?
Lu4 Lu6 Lu5 26.6(9) . . ?
Lu21 Lu6 Lu5 49.0(15) . . ?
Lu1 Lu6 C1C 56.1(8) . . ?
Lu3 Lu6 C1C 86.7(9) . . ?
Lu20 Lu6 C1C 61.7(12) . . ?
Lu18 Lu6 C1C 77.3(11) . . ?
Lu23 Lu6 C1C 66.7(17) . . ?
Lu4 Lu6 C1C 80.7(9) . . ?
Lu21 Lu6 C1C 93.1(13) . . ?
Lu5 Lu6 C1C 105.4(12) . . ?
Lu1 Lu6 Lu22 125.3(13) . . ?
Lu3 Lu6 Lu22 24.5(9) . . ?
Lu20 Lu6 Lu22 8.5(13) . . ?
Lu18 Lu6 Lu22 59.5(15) . . ?
Lu23 Lu6 Lu22 48.4(18) . . ?
Lu4 Lu6 Lu22 27.5(9) . . ?
Lu21 Lu6 Lu22 26.6(15) . . ?
Lu5 Lu6 Lu22 50.5(12) . . ?
C1C Lu6 Lu22 69.3(10) . . ?
Lu1 Lu6 Lu2 124.5(11) . . ?
Lu3 Lu6 Lu2 16.5(6) . . ?
Lu20 Lu6 Lu2 29.9(13) . . ?
Lu18 Lu6 Lu2 34.7(12) . . ?
Lu23 Lu6 Lu2 73.0(18) . . ?
Lu4 Lu6 Lu2 8.3(6) . . ?
Lu21 Lu6 Lu2 43.1(15) . . ?
Lu5 Lu6 Lu2 34.3(9) . . ?
C1C Lu6 Lu2 72.5(7) . . ?
Lu22 Lu6 Lu2 25.0(9) . . ?
Lu1 Lu6 C2C 80.0(8) . . ?
Lu3 Lu6 C2C 61.9(6) . . ?
Lu20 Lu6 C2C 40.3(11) . . ?
Lu18 Lu6 C2C 59.1(10) . . ?
Lu23 Lu6 C2C 62.5(16) . . ?
Lu4 Lu6 C2C 56.0(6) . . ?
Lu21 Lu6 C2C 72.7(13) . . ?
Lu5 Lu6 C2C 81.3(10) . . ?
C1C Lu6 C2C 24.8(5) . . ?
Lu22 Lu6 C2C 46.8(8) . . ?
Lu2 Lu6 C2C 47.7(5) . . ?
Lu15 Lu7 Lu12 108(3) . . ?
Lu15 Lu7 Lu14 69(2) . . ?
Lu12 Lu7 Lu14 169(3) . . ?
Lu15 Lu7 Lu10 64(2) . . ?
Lu12 Lu7 Lu10 143(3) . . ?
Lu14 Lu7 Lu10 46.1(17) . . ?
Lu15 Lu7 Lu9 175(2) . . ?
Lu12 Lu7 Lu9 76(2) . . ?
Lu14 Lu7 Lu9 108(2) . . ?
Lu10 Lu7 Lu9 111(2) . . ?
Lu15 Lu7 Lu17 28(3) . . ?
Lu12 Lu7 Lu17 112(3) . . ?
Lu14 Lu7 Lu17 60(3) . . ?
Lu10 Lu7 Lu17 79(3) . . ?
Lu9 Lu7 Lu17 153(3) . . ?
Lu15 Lu7 Lu19 101(2) . . ?
Lu12 Lu7 Lu19 98(2) . . ?
Lu14 Lu7 Lu19 73(2) . . ?
Lu10 Lu7 Lu19 118.8(19) . . ?
Lu9 Lu7 Lu19 79.6(18) . . ?
Lu17 Lu7 Lu19 74(2) . . ?
Lu15 Lu7 Lu24 115(3) . . ?
Lu12 Lu7 Lu24 31(2) . . ?
Lu14 Lu7 Lu24 160(3) . . ?
Lu10 Lu7 Lu24 116(2) . . ?
Lu9 Lu7 Lu24 67(2) . . ?
Lu17 Lu7 Lu24 133(3) . . ?
Lu19 Lu7 Lu24 123.1(19) . . ?
Lu15 Lu7 Lu13 147(3) . . ?
Lu12 Lu7 Lu13 77(3) . . ?
Lu14 Lu7 Lu13 111(2) . . ?
Lu10 Lu7 Lu13 91(2) . . ?
Lu9 Lu7 Lu13 30.8(18) . . ?
Lu17 Lu7 Lu13 170(3) . . ?
Lu19 Lu7 Lu13 110(2) . . ?
Lu24 Lu7 Lu13 54(3) . . ?
Lu15 Lu7 Lu8 93(2) . . ?
Lu12 Lu7 Lu8 115(2) . . ?
Lu14 Lu7 Lu8 75.7(18) . . ?
Lu10 Lu7 Lu8 36.1(15) . . ?
Lu9 Lu7 Lu8 83.6(16) . . ?
Lu17 Lu7 Lu8 113(2) . . ?
Lu19 Lu7 Lu8 137.5(12) . . ?
Lu24 Lu7 Lu8 84.1(18) . . ?
Lu13 Lu7 Lu8 57(2) . . ?
Lu15 Lu7 Lu11 111(2) . . ?
Lu12 Lu7 Lu11 101.7(19) . . ?
Lu14 Lu7 Lu11 71.0(19) . . ?
Lu10 Lu7 Lu11 115.1(16) . . ?
Lu9 Lu7 Lu11 69.4(15) . . ?
Lu17 Lu7 Lu11 84(2) . . ?
Lu19 Lu7 Lu11 12.2(11) . . ?
Lu24 Lu7 Lu11 121.6(17) . . ?
Lu13 Lu7 Lu11 98.9(19) . . ?
Lu8 Lu7 Lu11 127.2(5) . . ?
Lu15 Lu7 C1C 112(2) . . ?
Lu12 Lu7 C1C 137(2) . . ?
Lu14 Lu7 C1C 50.0(17) . . ?
Lu10 Lu7 C1C 53.3(15) . . ?
Lu9 Lu7 C1C 63.5(14) . . ?
Lu17 Lu7 C1C 110(2) . . ?
Lu19 Lu7 C1C 87.4(11) . . ?
Lu24 Lu7 C1C 114.1(19) . . ?
Lu13 Lu7 C1C 61.2(18) . . ?
Lu8 Lu7 C1C 50.3(6) . . ?
Lu11 Lu7 C1C 76.9(4) . . ?
Lu10 Lu8 Lu16 41.1(18) . . ?
Lu10 Lu8 Lu13 84(3) . . ?
Lu16 Lu8 Lu13 44(2) . . ?
Lu10 Lu8 Lu7 35.4(19) . . ?
Lu16 Lu8 Lu7 6.5(9) . . ?
Lu13 Lu8 Lu7 51(2) . . ?
Lu10 Lu8 Lu14 16.9(17) . . ?
Lu16 Lu8 Lu14 34.3(13) . . ?
Lu13 Lu8 Lu14 72(2) . . ?
Lu7 Lu8 Lu14 30.6(11) . . ?
Lu10 Lu8 Lu15 21.8(19) . . ?
Lu16 Lu8 Lu15 28.0(12) . . ?
Lu13 Lu8 Lu15 72(2) . . ?
Lu7 Lu8 Lu15 21.6(8) . . ?
Lu14 Lu8 Lu15 29.2(11) . . ?
Lu10 Lu8 Lu9 65(2) . . ?
Lu16 Lu8 Lu9 27.9(10) . . ?
Lu13 Lu8 Lu9 20.0(18) . . ?
Lu7 Lu8 Lu9 34.2(12) . . ?
Lu14 Lu8 Lu9 52.2(14) . . ?
Lu15 Lu8 Lu9 55.8(15) . . ?
Lu10 Lu8 C1C 82.9(17) . . ?
Lu16 Lu8 C1C 86.6(11) . . ?
Lu13 Lu8 C1C 79.8(18) . . ?
Lu7 Lu8 C1C 88.7(8) . . ?
Lu14 Lu8 C1C 69.5(12) . . ?
Lu15 Lu8 C1C 98.2(10) . . ?
Lu9 Lu8 C1C 72.8(11) . . ?
Lu10 Lu8 Lu24 74(2) . . ?
Lu16 Lu8 Lu24 37.6(15) . . ?
Lu13 Lu8 Lu24 37(2) . . ?
Lu7 Lu8 Lu24 40.8(14) . . ?
Lu14 Lu8 Lu24 71.4(18) . . ?
Lu15 Lu8 Lu24 53.0(16) . . ?
Lu9 Lu8 Lu24 40.0(15) . . ?
C1C Lu8 Lu24 112.8(14) . . ?
Lu10 Lu8 Lu12 53(2) . . ?
Lu16 Lu8 Lu12 17.4(10) . . ?
Lu13 Lu8 Lu12 41(2) . . ?
Lu7 Lu8 Lu12 19.7(9) . . ?
Lu14 Lu8 Lu12 50.3(14) . . ?
Lu15 Lu8 Lu12 33.9(12) . . ?
Lu9 Lu8 Lu12 32.9(12) . . ?
C1C Lu8 Lu12 101.7(10) . . ?
Lu24 Lu8 Lu12 21.2(12) . . ?
Lu10 Lu8 Lu17 12(2) . . ?
Lu16 Lu8 Lu17 35.0(14) . . ?
Lu13 Lu8 Lu17 79(2) . . ?
Lu7 Lu8 Lu17 28.6(13) . . ?
Lu14 Lu8 Lu17 23.3(15) . . ?
Lu15 Lu8 Lu17 10.7(13) . . ?
Lu9 Lu8 Lu17 61.6(17) . . ?
C1C Lu8 Lu17 92.4(14) . . ?
Lu24 Lu8 Lu17 63.6(19) . . ?
Lu12 Lu8 Lu17 43.9(15) . . ?
Lu10 Lu8 Lu19 34.3(18) . . ?
Lu16 Lu8 Lu19 18.1(9) . . ?
Lu13 Lu8 Lu19 51(2) . . ?
Lu7 Lu8 Lu19 18.5(5) . . ?
Lu14 Lu8 Lu19 20.9(11) . . ?
Lu15 Lu8 Lu19 32.7(9) . . ?
Lu9 Lu8 Lu19 31.3(12) . . ?
C1C Lu8 Lu19 70.4(8) . . ?
Lu24 Lu8 Lu19 55.1(14) . . ?
Lu12 Lu8 Lu19 35.5(9) . . ?
Lu17 Lu8 Lu19 33.9(14) . . ?
Lu13 Lu9 Lu16 85(5) . . ?
Lu13 Lu9 Lu7 99(5) . . ?
Lu16 Lu9 Lu7 15.1(14) . . ?
Lu13 Lu9 Lu12 95(5) . . ?
Lu16 Lu9 Lu12 48(3) . . ?
Lu7 Lu9 Lu12 41(2) . . ?
Lu13 Lu9 Lu24 65(5) . . ?
Lu16 Lu9 Lu24 64(3) . . ?
Lu7 Lu9 Lu24 66(3) . . ?
Lu12 Lu9 Lu24 34.9(19) . . ?
Lu13 Lu9 Lu19 154(6) . . ?
Lu16 Lu9 Lu19 70(3) . . ?
Lu7 Lu9 Lu19 57.2(18) . . ?
Lu12 Lu9 Lu19 73(3) . . ?
Lu24 Lu9 Lu19 108(3) . . ?
Lu13 Lu9 Lu14 104(5) . . ?
Lu16 Lu9 Lu14 33(2) . . ?
Lu7 Lu9 Lu14 32.4(14) . . ?
Lu12 Lu9 Lu14 73(3) . . ?
Lu24 Lu9 Lu14 97(3) . . ?
Lu19 Lu9 Lu14 51.2(18) . . ?
Lu13 Lu9 Lu10 78(5) . . ?
Lu16 Lu9 Lu10 22.0(17) . . ?
Lu7 Lu9 Lu10 33.7(14) . . ?
Lu12 Lu9 Lu10 70(3) . . ?
Lu24 Lu9 Lu10 81(3) . . ?
Lu19 Lu9 Lu10 76(2) . . ?
Lu14 Lu9 Lu10 26.1(11) . . ?
Lu13 Lu9 Lu15 98(5) . . ?
Lu16 Lu9 Lu15 13.9(19) . . ?
Lu7 Lu9 Lu15 1.8(9) . . ?
Lu12 Lu9 Lu15 43(2) . . ?
Lu24 Lu9 Lu15 67(3) . . ?
Lu19 Lu9 Lu15 57.6(17) . . ?
Lu14 Lu9 Lu15 31.0(14) . . ?
Lu10 Lu9 Lu15 31.9(13) . . ?
Lu13 Lu9 Lu8 46(4) . . ?
Lu16 Lu9 Lu8 47.2(18) . . ?
Lu7 Lu9 Lu8 62.2(15) . . ?
Lu12 Lu9 Lu8 85(2) . . ?
Lu24 Lu9 Lu8 76(2) . . ?
Lu19 Lu9 Lu8 109(2) . . ?
Lu14 Lu9 Lu8 57.7(15) . . ?
Lu10 Lu9 Lu8 33.2(11) . . ?
Lu15 Lu9 Lu8 60.8(14) . . ?
Lu13 Lu9 C1C 78(4) . . ?
Lu16 Lu9 C1C 83(2) . . ?
Lu7 Lu9 C1C 91.9(17) . . ?
Lu12 Lu9 C1C 132(3) . . ?
Lu24 Lu9 C1C 131(2) . . ?
Lu19 Lu9 C1C 93.0(16) . . ?
Lu14 Lu9 C1C 62.6(14) . . ?
Lu10 Lu9 C1C 61.6(13) . . ?
Lu15 Lu9 C1C 90.1(15) . . ?
Lu8 Lu9 C1C 55.3(9) . . ?
Lu13 Lu9 Lu17 112(5) . . ?
Lu16 Lu9 Lu17 28(2) . . ?
Lu7 Lu9 Lu17 14.9(16) . . ?
Lu12 Lu9 Lu17 48(3) . . ?
Lu24 Lu9 Lu17 78(3) . . ?
Lu19 Lu9 Lu17 42.6(18) . . ?
Lu14 Lu9 Lu17 27.2(17) . . ?
Lu10 Lu9 Lu17 40.2(17) . . ?
Lu15 Lu9 Lu17 15.0(14) . . ?
Lu8 Lu9 Lu17 72.3(18) . . ?
C1C Lu9 Lu17 89.8(17) . . ?
Lu14 Lu10 Lu16 67(4) . . ?
Lu14 Lu10 Lu15 62(3) . . ?
Lu16 Lu10 Lu15 56(3) . . ?
Lu14 Lu10 Lu7 58(3) . . ?
Lu16 Lu10 Lu7 17.0(11) . . ?
Lu15 Lu10 Lu7 40(2) . . ?
Lu14 Lu10 Lu8 140(4) . . ?
Lu16 Lu10 Lu8 92(3) . . ?
Lu15 Lu10 Lu8 134(4) . . ?
Lu7 Lu10 Lu8 109(3) . . ?
Lu14 Lu10 Lu17 50(3) . . ?
Lu16 Lu10 Lu17 76(3) . . ?
Lu15 Lu10 Lu17 27(2) . . ?
Lu7 Lu10 Lu17 59(3) . . ?
Lu8 Lu10 Lu17 160(4) . . ?
Lu14 Lu10 Lu12 74(4) . . ?
Lu16 Lu10 Lu12 18.4(16) . . ?
Lu15 Lu10 Lu12 42(2) . . ?
Lu7 Lu10 Lu12 16.1(12) . . ?
Lu8 Lu10 Lu12 98(2) . . ?
Lu17 Lu10 Lu12 66(3) . . ?
Lu14 Lu10 Lu9 66(3) . . ?
Lu16 Lu10 Lu9 21.2(16) . . ?
Lu15 Lu10 Lu9 75(3) . . ?
Lu7 Lu10 Lu9 35.3(15) . . ?
Lu8 Lu10 Lu9 82(2) . . ?
Lu17 Lu10 Lu9 91(3) . . ?
Lu12 Lu10 Lu9 39.4(15) . . ?
Lu14 Lu10 Lu13 90(4) . . ?
Lu16 Lu10 Lu13 35(2) . . ?
Lu15 Lu10 Lu13 90(3) . . ?
Lu7 Lu10 Lu13 52(2) . . ?
Lu8 Lu10 Lu13 59(2) . . ?
Lu17 Lu10 Lu13 111(3) . . ?
Lu12 Lu10 Lu13 49(2) . . ?
Lu9 Lu10 Lu13 23.7(14) . . ?
Lu14 Lu10 Lu24 94(4) . . ?
Lu16 Lu10 Lu24 28.0(19) . . ?
Lu15 Lu10 Lu24 60(3) . . ?
Lu7 Lu10 Lu24 36.9(17) . . ?
Lu8 Lu10 Lu24 77(2) . . ?
Lu17 Lu10 Lu24 86(3) . . ?
Lu12 Lu10 Lu24 22.3(12) . . ?
Lu9 Lu10 Lu24 41.6(17) . . ?
Lu13 Lu10 Lu24 37(2) . . ?
Lu14 Lu10 Lu19 23(3) . . ?
Lu16 Lu10 Lu19 44.4(18) . . ?
Lu15 Lu10 Lu19 51(2) . . ?
Lu7 Lu10 Lu19 34.7(13) . . ?
Lu8 Lu10 Lu19 129(2) . . ?
Lu17 Lu10 Lu19 50(2) . . ?
Lu12 Lu10 Lu19 50.8(14) . . ?
Lu9 Lu10 Lu19 47.6(15) . . ?
Lu13 Lu10 Lu19 71(2) . . ?
Lu24 Lu10 Lu19 70.7(17) . . ?
Lu14 Lu10 C1C 79(3) . . ?
Lu16 Lu10 C1C 94(2) . . ?
Lu15 Lu10 C1C 137(3) . . ?
Lu7 Lu10 C1C 103.9(19) . . ?
Lu8 Lu10 C1C 67.8(16) . . ?
Lu17 Lu10 C1C 128(3) . . ?
Lu12 Lu10 C1C 111.9(17) . . ?
Lu9 Lu10 C1C 72.5(15) . . ?
Lu13 Lu10 C1C 70.9(17) . . ?
Lu24 Lu10 C1C 108.2(18) . . ?
Lu19 Lu10 C1C 86.2(13) . . ?
Lu19 Lu11 C2C 80.8(12) . . ?
Lu19 Lu11 Lu9 36.5(14) . . ?
C2C Lu11 Lu9 63.3(7) . . ?
Lu19 Lu11 Lu14 25.6(14) . . ?
C2C Lu11 Lu14 57.4(8) . . ?
Lu9 Lu11 Lu14 39.3(11) . . ?
Lu19 Lu11 C3C 69.3(12) . . ?
C2C Lu11 C3C 30.1(7) . . ?
Lu9 Lu11 C3C 71.0(9) . . ?
Lu14 Lu11 C3C 43.9(10) . . ?
Lu19 Lu11 Lu7 12.8(11) . . ?
C2C Lu11 Lu7 70.1(3) . . ?
Lu9 Lu11 Lu7 25.2(10) . . ?
Lu14 Lu11 Lu7 20.9(7) . . ?
C3C Lu11 Lu7 63.7(6) . . ?
Lu19 Lu11 Lu16 19.0(11) . . ?
C2C Lu11 Lu16 65.2(5) . . ?
Lu9 Lu11 Lu16 20.2(8) . . ?
Lu14 Lu11 Lu16 21.3(9) . . ?
C3C Lu11 Lu16 61.7(7) . . ?
Lu7 Lu11 Lu16 6.2(4) . . ?
Lu19 Lu11 Lu17 19.8(17) . . ?
C2C Lu11 Lu17 81.4(12) . . ?
Lu9 Lu11 Lu17 54.0(17) . . ?
Lu14 Lu11 Lu17 25.4(13) . . ?
C3C Lu11 Lu17 61.0(12) . . ?
Lu7 Lu11 Lu17 28.8(14) . . ?
Lu16 Lu11 Lu17 34.1(14) . . ?
Lu19 Lu11 Lu12 17.9(12) . . ?
C2C Lu11 Lu12 82.7(7) . . ?
Lu9 Lu11 Lu12 24.6(10) . . ?
Lu14 Lu11 Lu12 37.1(10) . . ?
C3C Lu11 Lu12 79.8(9) . . ?
Lu7 Lu11 Lu12 16.3(6) . . ?
Lu16 Lu11 Lu12 18.5(7) . . ?
Lu17 Lu11 Lu12 37.7(14) . . ?
Lu19 Lu11 Lu15 8.7(12) . . ?
C2C Lu11 Lu15 74.1(6) . . ?
Lu9 Lu11 Lu15 38.2(11) . . ?
Lu14 Lu11 Lu15 17.4(8) . . ?
C3C Lu11 Lu15 60.8(8) . . ?
Lu7 Lu11 Lu15 13.0(6) . . ?
Lu16 Lu11 Lu15 18.3(7) . . ?
Lu17 Lu11 Lu15 15.8(11) . . ?
Lu12 Lu11 Lu15 24.7(8) . . ?
Lu19 Lu11 Lu13 38.4(13) . . ?
C2C Lu11 Lu13 59.3(9) . . ?
Lu9 Lu11 Lu13 4.0(10) . . ?
Lu14 Lu11 Lu13 38.4(11) . . ?
C3C Lu11 Lu13 67.8(10) . . ?
Lu7 Lu11 Lu13 26.5(8) . . ?
Lu16 Lu11 Lu13 20.9(9) . . ?
Lu17 Lu11 Lu13 55.0(17) . . ?
Lu12 Lu11 Lu13 27.9(10) . . ?
Lu15 Lu11 Lu13 39.2(11) . . ?
Lu19 Lu11 Lu10 25.0(12) . . ?
C2C Lu11 Lu10 56.2(6) . . ?
Lu9 Lu11 Lu10 33.8(10) . . ?
Lu14 Lu11 Lu10 5.6(8) . . ?
C3C Lu11 Lu10 46.2(8) . . ?
Lu7 Lu11 Lu10 17.6(6) . . ?
Lu16 Lu11 Lu10 16.7(6) . . ?
Lu17 Lu11 Lu10 28.9(13) . . ?
Lu12 Lu11 Lu10 33.8(9) . . ?
Lu15 Lu11 Lu10 18.0(7) . . ?
Lu13 Lu11 Lu10 32.8(10) . . ?
Lu24 Lu12 Lu7 117(5) . . ?
Lu24 Lu12 Lu16 99(4) . . ?
Lu7 Lu12 Lu16 20.0(14) . . ?
Lu24 Lu12 Lu9 86(4) . . ?
Lu7 Lu12 Lu9 63(3) . . ?
Lu16 Lu12 Lu9 51(2) . . ?
Lu24 Lu12 Lu15 123(4) . . ?
Lu7 Lu12 Lu15 32.6(18) . . ?
Lu16 Lu12 Lu15 48(2) . . ?
Lu9 Lu12 Lu15 95(3) . . ?
Lu24 Lu12 Lu13 60(4) . . ?
Lu7 Lu12 Lu13 70(3) . . ?
Lu16 Lu12 Lu13 51(2) . . ?
Lu9 Lu12 Lu13 29.8(19) . . ?
Lu15 Lu12 Lu13 98(3) . . ?
Lu24 Lu12 Lu19 150(4) . . ?
Lu7 Lu12 Lu19 52.8(19) . . ?
Lu16 Lu12 Lu19 66(2) . . ?
Lu9 Lu12 Lu19 64(2) . . ?
Lu15 Lu12 Lu19 67(2) . . ?
Lu13 Lu12 Lu19 92(3) . . ?
Lu24 Lu12 Lu14 123(4) . . ?
Lu7 Lu12 Lu14 5.6(15) . . ?
Lu16 Lu12 Lu14 25.2(17) . . ?
Lu9 Lu12 Lu14 65(2) . . ?
Lu15 Lu12 Lu14 31.3(16) . . ?
Lu13 Lu12 Lu14 74(2) . . ?
Lu19 Lu12 Lu14 48.2(16) . . ?
Lu24 Lu12 Lu10 100(4) . . ?
Lu7 Lu12 Lu10 21.1(15) . . ?
Lu16 Lu12 Lu10 19.7(19) . . ?
Lu9 Lu12 Lu10 70(2) . . ?
Lu15 Lu12 Lu10 32.2(17) . . ?
Lu13 Lu12 Lu10 66(2) . . ?
Lu19 Lu12 Lu10 73.9(18) . . ?
Lu14 Lu12 Lu10 25.8(10) . . ?
Lu24 Lu12 Lu17 142(4) . . ?
Lu7 Lu12 Lu17 43(2) . . ?
Lu16 Lu12 Lu17 62(3) . . ?
Lu9 Lu12 Lu17 102(3) . . ?
Lu15 Lu12 Lu17 20.4(18) . . ?
Lu13 Lu12 Lu17 113(3) . . ?
Lu19 Lu12 Lu17 55(2) . . ?
Lu14 Lu12 Lu17 39(2) . . ?
Lu10 Lu12 Lu17 51(2) . . ?
Lu24 Lu12 Lu8 72(4) . . ?
Lu7 Lu12 Lu8 45.5(16) . . ?
Lu16 Lu12 Lu8 29.1(15) . . ?
Lu9 Lu12 Lu8 62(2) . . ?
Lu15 Lu12 Lu8 59.4(19) . . ?
Lu13 Lu12 Lu8 44(2) . . ?
Lu19 Lu12 Lu8 94.7(17) . . ?
Lu14 Lu12 Lu8 51.1(13) . . ?
Lu10 Lu12 Lu8 28.9(10) . . ?
Lu17 Lu12 Lu8 79(2) . . ?
Lu24 Lu12 Lu11 140(4) . . ?
Lu7 Lu12 Lu11 62.0(18) . . ?
Lu16 Lu12 Lu11 71.1(19) . . ?
Lu9 Lu12 Lu11 56.9(19) . . ?
Lu15 Lu12 Lu11 79.7(19) . . ?
Lu13 Lu12 Lu11 86(2) . . ?
Lu19 Lu12 Lu11 13.7(9) . . ?
Lu14 Lu12 Lu11 58.2(13) . . ?
Lu10 Lu12 Lu11 82.9(15) . . ?
Lu17 Lu12 Lu11 68.6(19) . . ?
Lu8 Lu12 Lu11 99.2(11) . . ?
Lu9 Lu13 Lu16 56(4) . . ?
Lu9 Lu13 Lu24 84(5) . . ?
Lu16 Lu13 Lu24 65(3) . . ?
Lu9 Lu13 Lu7 51(4) . . ?
Lu16 Lu13 Lu7 6.8(13) . . ?
Lu24 Lu13 Lu7 62(3) . . ?
Lu9 Lu13 Lu12 55(4) . . ?
Lu16 Lu13 Lu12 38(2) . . ?
Lu24 Lu13 Lu12 33(2) . . ?
Lu7 Lu13 Lu12 33.0(17) . . ?
Lu9 Lu13 Lu8 114(5) . . ?
Lu16 Lu13 Lu8 65(2) . . ?
Lu24 Lu13 Lu8 97(3) . . ?
Lu7 Lu13 Lu8 72(2) . . ?
Lu12 Lu13 Lu8 95(3) . . ?
Lu9 Lu13 Lu10 78(5) . . ?
Lu16 Lu13 Lu10 29.7(17) . . ?
Lu24 Lu13 Lu10 84(3) . . ?
Lu7 Lu13 Lu10 36.5(16) . . ?
Lu12 Lu13 Lu10 66(3) . . ?
Lu8 Lu13 Lu10 37.0(15) . . ?
Lu9 Lu13 Lu14 55(4) . . ?
Lu16 Lu13 Lu14 22.2(17) . . ?
Lu24 Lu13 Lu14 87(4) . . ?
Lu7 Lu13 Lu14 26.2(13) . . ?
Lu12 Lu13 Lu14 59(2) . . ?
Lu8 Lu13 Lu14 59.1(18) . . ?
Lu10 Lu13 Lu14 23.9(11) . . ?
Lu9 Lu13 Lu15 61(5) . . ?
Lu16 Lu13 Lu15 6.6(18) . . ?
Lu24 Lu13 Lu15 61(3) . . ?
Lu7 Lu13 Lu15 10.7(10) . . ?
Lu12 Lu13 Lu15 36.9(19) . . ?
Lu8 Lu13 Lu15 62.5(17) . . ?
Lu10 Lu13 Lu15 29.0(13) . . ?
Lu14 Lu13 Lu15 27.0(12) . . ?
Lu9 Lu13 Lu19 18(4) . . ?
Lu16 Lu13 Lu19 38(2) . . ?
Lu24 Lu13 Lu19 81(3) . . ?
Lu7 Lu13 Lu19 34.2(14) . . ?
Lu12 Lu13 Lu19 48(2) . . ?
Lu8 Lu13 Lu19 97(2) . . ?
Lu10 Lu13 Lu19 60.6(19) . . ?
Lu14 Lu13 Lu19 37.7(14) . . ?
Lu15 Lu13 Lu19 44.5(14) . . ?
Lu9 Lu13 C1C 85(4) . . ?
Lu16 Lu13 C1C 82(2) . . ?
Lu24 Lu13 C1C 146(4) . . ?
Lu7 Lu13 C1C 87(2) . . ?
Lu12 Lu13 C1C 119(3) . . ?
Lu8 Lu13 C1C 59.7(15) . . ?
Lu10 Lu13 C1C 62.7(16) . . ?
Lu14 Lu13 C1C 60.4(15) . . ?
Lu15 Lu13 C1C 86.0(18) . . ?
Lu19 Lu13 C1C 79.0(17) . . ?
Lu9 Lu13 Lu17 53(5) . . ?
Lu16 Lu13 Lu17 2(2) . . ?
Lu24 Lu13 Lu17 65(3) . . ?
Lu7 Lu13 Lu17 5.1(13) . . ?
Lu12 Lu13 Lu17 38(2) . . ?
Lu8 Lu13 Lu17 67(2) . . ?
Lu10 Lu13 Lu17 31.5(17) . . ?
Lu14 Lu13 Lu17 22.0(15) . . ?
Lu15 Lu13 Lu17 8.6(13) . . ?
Lu19 Lu13 Lu17 36.2(15) . . ?
C1C Lu13 Lu17 82.4(19) . . ?
Lu10 Lu14 Lu7 76(4) . . ?
Lu10 Lu14 Lu15 69(3) . . ?
Lu7 Lu14 Lu15 44(2) . . ?
Lu10 Lu14 Lu16 65(3) . . ?
Lu7 Lu14 Lu16 18.4(12) . . ?
Lu15 Lu14 Lu16 57(3) . . ?
Lu10 Lu14 Lu17 100(4) . . ?
Lu7 Lu14 Lu17 78(4) . . ?
Lu15 Lu14 Lu17 42(3) . . ?
Lu16 Lu14 Lu17 95(4) . . ?
Lu10 Lu14 Lu19 144(4) . . ?
Lu7 Lu14 Lu19 68(2) . . ?
Lu15 Lu14 Lu19 87(3) . . ?
Lu16 Lu14 Lu19 79(2) . . ?
Lu17 Lu14 Lu19 77(3) . . ?
Lu10 Lu14 Lu9 87(3) . . ?
Lu7 Lu14 Lu9 40.0(16) . . ?
Lu15 Lu14 Lu9 84(3) . . ?
Lu16 Lu14 Lu9 31.2(16) . . ?
Lu17 Lu14 Lu9 114(4) . . ?
Lu19 Lu14 Lu9 62.4(18) . . ?
Lu10 Lu14 Lu12 81(4) . . ?
Lu7 Lu14 Lu12 5.0(13) . . ?
Lu15 Lu14 Lu12 43(3) . . ?
Lu16 Lu14 Lu12 23.1(16) . . ?
Lu17 Lu14 Lu12 75(3) . . ?
Lu19 Lu14 Lu12 64.0(18) . . ?
Lu9 Lu14 Lu12 41.7(16) . . ?
Lu10 Lu14 Lu8 24(2) . . ?
Lu7 Lu14 Lu8 73.7(18) . . ?
Lu15 Lu14 Lu8 84(3) . . ?
Lu16 Lu14 Lu8 57.7(17) . . ?
Lu17 Lu14 Lu8 121(3) . . ?
Lu19 Lu14 Lu8 132(2) . . ?
Lu9 Lu14 Lu8 70.2(16) . . ?
Lu12 Lu14 Lu8 78.6(16) . . ?
Lu10 Lu14 C3C 117(4) . . ?
Lu7 Lu14 C3C 149(3) . . ?
Lu15 Lu14 C3C 164(3) . . ?
Lu16 Lu14 C3C 139(3) . . ?
Lu17 Lu14 C3C 123(4) . . ?
Lu19 Lu14 C3C 93(2) . . ?
Lu9 Lu14 C3C 110(2) . . ?
Lu12 Lu14 C3C 149(2) . . ?
Lu8 Lu14 C3C 106.9(18) . . ?
Lu10 Lu14 Lu13 67(3) . . ?
Lu7 Lu14 Lu13 42.7(18) . . ?
Lu15 Lu14 Lu13 82(3) . . ?
Lu16 Lu14 Lu13 25.7(18) . . ?
Lu17 Lu14 Lu13 120(4) . . ?
Lu19 Lu14 Lu13 84(2) . . ?
Lu9 Lu14 Lu13 21.4(14) . . ?
Lu12 Lu14 Lu13 46.5(18) . . ?
Lu8 Lu14 Lu13 48.8(17) . . ?
C3C Lu14 Lu13 114(2) . . ?
Lu10 Lu14 C1C 81(3) . . ?
Lu7 Lu14 C1C 111(2) . . ?
Lu15 Lu14 C1C 145(3) . . ?
Lu16 Lu14 C1C 94(2) . . ?
Lu17 Lu14 C1C 171(4) . . ?
Lu19 Lu14 C1C 107.8(19) . . ?
Lu9 Lu14 C1C 75.5(15) . . ?
Lu12 Lu14 C1C 114.6(17) . . ?
Lu8 Lu14 C1C 61.5(11) . . ?
C3C Lu14 C1C 50.1(12) . . ?
Lu13 Lu14 C1C 68.5(17) . . ?
Lu7 Lu15 Lu17 128(6) . . ?
Lu7 Lu15 Lu16 16.3(16) . . ?
Lu17 Lu15 Lu16 141(6) . . ?
Lu7 Lu15 Lu14 67(3) . . ?
Lu17 Lu15 Lu14 87(5) . . ?
Lu16 Lu15 Lu14 65(3) . . ?
Lu7 Lu15 Lu10 76(3) . . ?
Lu17 Lu15 Lu10 119(5) . . ?
Lu16 Lu15 Lu10 61(3) . . ?
Lu14 Lu15 Lu10 48(2) . . ?
Lu7 Lu15 Lu12 39(2) . . ?
Lu17 Lu15 Lu12 127(5) . . ?
Lu16 Lu15 Lu12 47(2) . . ?
Lu14 Lu15 Lu12 105(4) . . ?
Lu10 Lu15 Lu12 106(4) . . ?
Lu7 Lu15 Lu19 53.9(18) . . ?
Lu17 Lu15 Lu19 74(5) . . ?
Lu16 Lu15 Lu19 68(2) . . ?
Lu14 Lu15 Lu19 58(2) . . ?
Lu10 Lu15 Lu19 102(3) . . ?
Lu12 Lu15 Lu19 70(2) . . ?
Lu7 Lu15 Lu24 44(2) . . ?
Lu17 Lu15 Lu24 147(5) . . ?
Lu16 Lu15 Lu24 44(2) . . ?
Lu14 Lu15 Lu24 108(3) . . ?
Lu10 Lu15 Lu24 92(3) . . ?
Lu12 Lu15 Lu24 21.9(16) . . ?
Lu19 Lu15 Lu24 89(2) . . ?
Lu7 Lu15 Lu9 2.8(15) . . ?
Lu17 Lu15 Lu9 129(5) . . ?
Lu16 Lu15 Lu9 14(2) . . ?
Lu14 Lu15 Lu9 65(3) . . ?
Lu10 Lu15 Lu9 73(3) . . ?
Lu12 Lu15 Lu9 41.6(19) . . ?
Lu19 Lu15 Lu9 54.5(15) . . ?
Lu24 Lu15 Lu9 45.6(19) . . ?
Lu7 Lu15 Lu8 66(2) . . ?
Lu17 Lu15 Lu8 143(4) . . ?
Lu16 Lu15 Lu8 49(2) . . ?
Lu14 Lu15 Lu8 66(2) . . ?
Lu10 Lu15 Lu8 24(2) . . ?
Lu12 Lu15 Lu8 87(2) . . ?
Lu19 Lu15 Lu8 108.6(18) . . ?
Lu24 Lu15 Lu8 69.3(18) . . ?
Lu9 Lu15 Lu8 63.4(14) . . ?
Lu7 Lu15 Lu13 22(2) . . ?
Lu17 Lu15 Lu13 149(5) . . ?
Lu16 Lu15 Lu13 8(2) . . ?
Lu14 Lu15 Lu13 71(3) . . ?
Lu10 Lu15 Lu13 61(3) . . ?
Lu12 Lu15 Lu13 45(2) . . ?
Lu19 Lu15 Lu13 75(2) . . ?
Lu24 Lu15 Lu13 38(2) . . ?
Lu9 Lu15 Lu13 20.8(13) . . ?
Lu8 Lu15 Lu13 45.7(16) . . ?
Lu7 Lu15 C3C 76.5(19) . . ?
Lu17 Lu15 C3C 77(4) . . ?
Lu16 Lu15 C3C 75(2) . . ?
Lu14 Lu15 C3C 11(2) . . ?
Lu10 Lu15 C3C 54(2) . . ?
Lu12 Lu15 C3C 114(2) . . ?
Lu19 Lu15 C3C 58.9(12) . . ?
Lu24 Lu15 C3C 119(2) . . ?
Lu9 Lu15 C3C 74.3(13) . . ?
Lu8 Lu15 C3C 74.2(10) . . ?
Lu13 Lu15 C3C 81.6(16) . . ?
Lu12 Lu16 Lu15 85(3) . . ?
Lu12 Lu16 Lu9 81(3) . . ?
Lu15 Lu16 Lu9 152(4) . . ?
Lu12 Lu16 Lu10 142(3) . . ?
Lu15 Lu16 Lu10 63(3) . . ?
Lu9 Lu16 Lu10 137(3) . . ?
Lu12 Lu16 Lu14 132(3) . . ?
Lu15 Lu16 Lu14 58(2) . . ?
Lu9 Lu16 Lu14 116(3) . . ?
Lu10 Lu16 Lu14 47(2) . . ?
Lu12 Lu16 Lu13 91(3) . . ?
Lu15 Lu16 Lu13 165(4) . . ?
Lu9 Lu16 Lu13 40(2) . . ?
Lu10 Lu16 Lu13 115(3) . . ?
Lu14 Lu16 Lu13 132(3) . . ?
Lu12 Lu16 Lu24 37(2) . . ?
Lu15 Lu16 Lu24 107(3) . . ?
Lu9 Lu16 Lu24 75(3) . . ?
Lu10 Lu16 Lu24 131(3) . . ?
Lu14 Lu16 Lu24 166(3) . . ?
Lu13 Lu16 Lu24 62(3) . . ?
Lu12 Lu16 Lu8 133(2) . . ?
Lu15 Lu16 Lu8 103(3) . . ?
Lu9 Lu16 Lu8 105(2) . . ?
Lu10 Lu16 Lu8 46.6(18) . . ?
Lu14 Lu16 Lu8 88(2) . . ?
Lu13 Lu16 Lu8 70(3) . . ?
Lu24 Lu16 Lu8 98(2) . . ?
Lu12 Lu16 Lu19 82(2) . . ?
Lu15 Lu16 Lu19 79(2) . . ?
Lu9 Lu16 Lu19 75(3) . . ?
Lu10 Lu16 Lu19 109(2) . . ?
Lu14 Lu16 Lu19 62(2) . . ?
Lu13 Lu16 Lu19 114(3) . . ?
Lu24 Lu16 Lu19 115(2) . . ?
Lu8 Lu16 Lu19 144.5(17) . . ?
Lu12 Lu16 Lu17 88(3) . . ?
Lu15 Lu16 Lu17 18(2) . . ?
Lu9 Lu16 Lu17 136(3) . . ?
Lu10 Lu16 Lu17 68(3) . . ?
Lu14 Lu16 Lu17 48(3) . . ?
Lu13 Lu16 Lu17 176(4) . . ?
Lu24 Lu16 Lu17 118(3) . . ?
Lu8 Lu16 Lu17 113(2) . . ?
Lu19 Lu16 Lu17 62(2) . . ?
Lu12 Lu16 C1C 155(2) . . ?
Lu15 Lu16 C1C 117(2) . . ?
Lu9 Lu16 C1C 74(2) . . ?
Lu10 Lu16 C1C 63.0(19) . . ?
Lu14 Lu16 C1C 62.3(19) . . ?
Lu13 Lu16 C1C 70(2) . . ?
Lu24 Lu16 C1C 132(2) . . ?
Lu8 Lu16 C1C 56.2(8) . . ?
Lu19 Lu16 C1C 91.0(13) . . ?
Lu17 Lu16 C1C 110(2) . . ?
Lu12 Lu16 C3C 144(2) . . ?
Lu15 Lu16 C3C 85(2) . . ?
Lu9 Lu16 C3C 91(2) . . ?
Lu10 Lu16 C3C 58(2) . . ?
Lu14 Lu16 C3C 27.0(18) . . ?
Lu13 Lu16 C3C 106(2) . . ?
Lu24 Lu16 C3C 166(2) . . ?
Lu8 Lu16 C3C 83.0(11) . . ?
Lu19 Lu16 C3C 61.7(12) . . ?
Lu17 Lu16 C3C 73(2) . . ?
C1C Lu16 C3C 39.1(7) . . ?
Lu15 Lu17 Lu14 51(4) . . ?
Lu15 Lu17 Lu7 24(3) . . ?
Lu14 Lu17 Lu7 42(3) . . ?
Lu15 Lu17 Lu10 34(3) . . ?
Lu14 Lu17 Lu10 30(2) . . ?
Lu7 Lu17 Lu10 42(2) . . ?
Lu15 Lu17 Lu16 21(3) . . ?
Lu14 Lu17 Lu16 38(3) . . ?
Lu7 Lu17 Lu16 6.5(9) . . ?
Lu10 Lu17 Lu16 36(2) . . ?
Lu15 Lu17 Lu19 77(5) . . ?
Lu14 Lu17 Lu19 57(3) . . ?
Lu7 Lu17 Lu19 53(2) . . ?
Lu10 Lu17 Lu19 82(3) . . ?
Lu16 Lu17 Lu19 57(2) . . ?
Lu15 Lu17 Lu12 33(4) . . ?
Lu14 Lu17 Lu12 66(4) . . ?
Lu7 Lu17 Lu12 24.5(15) . . ?
Lu10 Lu17 Lu12 63(3) . . ?
Lu16 Lu17 Lu12 29.9(16) . . ?
Lu19 Lu17 Lu12 58(2) . . ?
Lu15 Lu17 Lu9 36(4) . . ?
Lu14 Lu17 Lu9 39(3) . . ?
Lu7 Lu17 Lu9 12.2(13) . . ?
Lu10 Lu17 Lu9 48(2) . . ?
Lu16 Lu17 Lu9 15.9(13) . . ?
Lu19 Lu17 Lu9 41(2) . . ?
Lu12 Lu17 Lu9 29.6(15) . . ?
Lu15 Lu17 Lu24 23(3) . . ?
Lu14 Lu17 Lu24 65(4) . . ?
Lu7 Lu17 Lu24 23.9(17) . . ?
Lu10 Lu17 Lu24 56(3) . . ?
Lu16 Lu17 Lu24 27.3(17) . . ?
Lu19 Lu17 Lu24 68(3) . . ?
Lu12 Lu17 Lu24 11.4(13) . . ?
Lu9 Lu17 Lu24 33.1(16) . . ?
Lu15 Lu17 Lu8 26(3) . . ?
Lu14 Lu17 Lu8 36(2) . . ?
Lu7 Lu17 Lu8 38.2(16) . . ?
Lu10 Lu17 Lu8 8.0(15) . . ?
Lu16 Lu17 Lu8 31.9(14) . . ?
Lu19 Lu17 Lu8 83(3) . . ?
Lu12 Lu17 Lu8 57(2) . . ?
Lu9 Lu17 Lu8 46.1(14) . . ?
Lu24 Lu17 Lu8 49.0(16) . . ?
Lu15 Lu17 C3C 87(5) . . ?
Lu14 Lu17 C3C 35(2) . . ?
Lu7 Lu17 C3C 75(3) . . ?
Lu10 Lu17 C3C 59(2) . . ?
Lu16 Lu17 C3C 72(2) . . ?
Lu19 Lu17 C3C 61(2) . . ?
Lu12 Lu17 C3C 98(3) . . ?
Lu9 Lu17 C3C 68.3(18) . . ?
Lu24 Lu17 C3C 99(2) . . ?
Lu8 Lu17 C3C 66.6(15) . . ?
Lu15 Lu17 Lu13 23(4) . . ?
Lu14 Lu17 Lu13 38(3) . . ?
Lu7 Lu17 Lu13 5.4(14) . . ?
Lu10 Lu17 Lu13 37(2) . . ?
Lu16 Lu17 Lu13 1.7(15) . . ?
Lu19 Lu17 Lu13 56(2) . . ?
Lu12 Lu17 Lu13 29.5(17) . . ?
Lu9 Lu17 Lu13 14.3(11) . . ?
Lu24 Lu17 Lu13 27.5(15) . . ?
Lu8 Lu17 Lu13 33.3(14) . . ?
C3C Lu17 Lu13 71.6(19) . . ?
Lu4 Lu18 Lu3 20.2(7) . . ?
Lu4 Lu18 Lu5 46.5(18) . . ?
Lu3 Lu18 Lu5 48.5(18) . . ?
Lu4 Lu18 Lu6 79.2(18) . . ?
Lu3 Lu18 Lu6 60.0(14) . . ?
Lu5 Lu18 Lu6 92(2) . . ?
Lu4 Lu18 Lu20 33.7(15) . . ?
Lu3 Lu18 Lu20 28.8(12) . . ?
Lu5 Lu18 Lu20 76(2) . . ?
Lu6 Lu18 Lu20 56.7(14) . . ?
Lu4 Lu18 Lu2 38.9(14) . . ?
Lu3 Lu18 Lu2 59.0(14) . . ?
Lu5 Lu18 Lu2 62.0(18) . . ?
Lu6 Lu18 Lu2 115.5(19) . . ?
Lu20 Lu18 Lu2 60.1(15) . . ?
Lu4 Lu18 Lu21 22.4(13) . . ?
Lu3 Lu18 Lu21 3.0(11) . . ?
Lu5 Lu18 Lu21 51(2) . . ?
Lu6 Lu18 Lu21 57.3(14) . . ?
Lu20 Lu18 Lu21 26.9(12) . . ?
Lu2 Lu18 Lu21 61.0(15) . . ?
Lu4 Lu18 Lu22 18.4(13) . . ?
Lu3 Lu18 Lu22 31.9(12) . . ?
Lu5 Lu18 Lu22 64(2) . . ?
Lu6 Lu18 Lu22 81.7(16) . . ?
Lu20 Lu18 Lu22 26.3(13) . . ?
Lu2 Lu18 Lu22 34.1(12) . . ?
Lu21 Lu18 Lu22 32.6(14) . . ?
Lu4 Lu18 Lu1 103.2(17) . . ?
Lu3 Lu18 Lu1 86.8(13) . . ?
Lu5 Lu18 Lu1 123(2) . . ?
Lu6 Lu18 Lu1 31.3(8) . . ?
Lu20 Lu18 Lu1 72.2(12) . . ?
Lu2 Lu18 Lu1 129.6(14) . . ?
Lu21 Lu18 Lu1 83.9(13) . . ?
Lu22 Lu18 Lu1 98.1(13) . . ?
Lu4 Lu18 C3C 100.3(17) . . ?
Lu3 Lu18 C3C 109.8(15) . . ?
Lu5 Lu18 C3C 140(2) . . ?
Lu6 Lu18 C3C 105.4(13) . . ?
Lu20 Lu18 C3C 82.9(13) . . ?
Lu2 Lu18 C3C 77.7(11) . . ?
Lu21 Lu18 C3C 108.8(14) . . ?
Lu22 Lu18 C3C 82.0(13) . . ?
Lu1 Lu18 C3C 81.6(9) . . ?
Lu4 Lu18 C1C 87.0(15) . . ?
Lu3 Lu18 C1C 84.1(13) . . ?
Lu5 Lu18 C1C 132(2) . . ?
Lu6 Lu18 C1C 64.5(10) . . ?
Lu20 Lu18 C1C 55.9(12) . . ?
Lu2 Lu18 C1C 90.5(11) . . ?
Lu21 Lu18 C1C 81.7(13) . . ?
Lu22 Lu18 C1C 71.4(11) . . ?
Lu1 Lu18 C1C 46.9(6) . . ?
C3C Lu18 C1C 41.3(8) . . ?
Lu4 Lu18 C2C 73.7(14) . . ?
Lu3 Lu18 C2C 81.0(12) . . ?
Lu5 Lu18 C2C 119(2) . . ?
Lu6 Lu18 C2C 89.3(11) . . ?
Lu20 Lu18 C2C 54.2(11) . . ?
Lu2 Lu18 C2C 62.8(9) . . ?
Lu21 Lu18 C2C 79.9(12) . . ?
Lu22 Lu18 C2C 55.3(10) . . ?
Lu1 Lu18 C2C 77.2(6) . . ?
C3C Lu18 C2C 28.9(7) . . ?
C1C Lu18 C2C 30.4(5) . . ?
Lu11 Lu19 Lu7 155(2) . . ?
Lu11 Lu19 Lu14 131(2) . . ?
Lu7 Lu19 Lu14 39.2(15) . . ?
Lu11 Lu19 Lu16 145(2) . . ?
Lu7 Lu19 Lu16 9.8(8) . . ?
Lu14 Lu19 Lu16 38.9(16) . . ?
Lu11 Lu19 Lu9 115(2) . . ?
Lu7 Lu19 Lu9 43.3(15) . . ?
Lu14 Lu19 Lu9 66.4(19) . . ?
Lu16 Lu19 Lu9 35.1(13) . . ?
Lu11 Lu19 Lu17 145(3) . . ?
Lu7 Lu19 Lu17 53(2) . . ?
Lu14 Lu19 Lu17 46(2) . . ?
Lu16 Lu19 Lu17 61(2) . . ?
Lu9 Lu19 Lu17 96(3) . . ?
Lu11 Lu19 Lu15 164(2) . . ?
Lu7 Lu19 Lu15 24.7(12) . . ?
Lu14 Lu19 Lu15 34.6(15) . . ?
Lu16 Lu19 Lu15 33.2(14) . . ?
Lu9 Lu19 Lu15 68(2) . . ?
Lu17 Lu19 Lu15 28.1(19) . . ?
Lu11 Lu19 Lu12 148.5(19) . . ?
Lu7 Lu19 Lu12 28.8(11) . . ?
Lu14 Lu19 Lu12 68(2) . . ?
Lu16 Lu19 Lu12 32.4(14) . . ?
Lu9 Lu19 Lu12 43.1(16) . . ?
Lu17 Lu19 Lu12 67(3) . . ?
Lu15 Lu19 Lu12 43.6(15) . . ?
Lu11 Lu19 Lu10 139.8(19) . . ?
Lu7 Lu19 Lu10 26.5(10) . . ?
Lu14 Lu19 Lu10 12.8(15) . . ?
Lu16 Lu19 Lu10 26.2(10) . . ?
Lu9 Lu19 Lu10 56.3(16) . . ?
Lu17 Lu19 Lu10 47(2) . . ?
Lu15 Lu19 Lu10 27.7(12) . . ?
Lu12 Lu19 Lu10 55.3(15) . . ?
Lu11 Lu19 Lu13 120.9(18) . . ?
Lu7 Lu19 Lu13 35.9(13) . . ?
Lu14 Lu19 Lu13 58.6(19) . . ?
Lu16 Lu19 Lu13 27.3(15) . . ?
Lu9 Lu19 Lu13 8.1(18) . . ?
Lu17 Lu19 Lu13 88(3) . . ?
Lu15 Lu19 Lu13 60.4(18) . . ?
Lu12 Lu19 Lu13 40.3(16) . . ?
Lu10 Lu19 Lu13 48.2(15) . . ?
Lu11 Lu19 C3C 80.0(13) . . ?
Lu7 Lu19 C3C 87.7(13) . . ?
Lu14 Lu19 C3C 51.1(16) . . ?
Lu16 Lu19 C3C 83.3(14) . . ?
Lu9 Lu19 C3C 90.3(16) . . ?
Lu17 Lu19 C3C 82(2) . . ?
Lu15 Lu19 C3C 84.7(14) . . ?
Lu12 Lu19 C3C 115.6(17) . . ?
Lu10 Lu19 C3C 62.2(12) . . ?
Lu13 Lu19 C3C 86.6(15) . . ?
Lu11 Lu19 C2C 66.8(11) . . ?
Lu7 Lu19 C2C 91.7(12) . . ?
Lu14 Lu19 C2C 67.3(16) . . ?
Lu16 Lu19 C2C 83.5(12) . . ?
Lu9 Lu19 C2C 72.9(14) . . ?
Lu17 Lu19 C2C 109(2) . . ?
Lu15 Lu19 C2C 100.9(15) . . ?
Lu12 Lu19 C2C 112.0(16) . . ?
Lu10 Lu19 C2C 73.4(11) . . ?
Lu13 Lu19 C2C 72.9(13) . . ?
C3C Lu19 C2C 30.6(7) . . ?
Lu3 Lu20 Lu21 62(3) . . ?
Lu3 Lu20 Lu4 24.4(11) . . ?
Lu21 Lu20 Lu4 77(3) . . ?
Lu3 Lu20 Lu22 93(3) . . ?
Lu21 Lu20 Lu22 74(3) . . ?
Lu4 Lu20 Lu22 79(3) . . ?
Lu3 Lu20 Lu23 124(3) . . ?
Lu21 Lu20 Lu23 80(4) . . ?
Lu4 Lu20 Lu23 149(3) . . ?
Lu22 Lu20 Lu23 115(4) . . ?
Lu3 Lu20 Lu6 66.5(17) . . ?
Lu21 Lu20 Lu6 90(3) . . ?
Lu4 Lu20 Lu6 83.5(18) . . ?
Lu22 Lu20 Lu6 159(3) . . ?
Lu23 Lu20 Lu6 75(2) . . ?
Lu3 Lu20 Lu18 41.8(16) . . ?
Lu21 Lu20 Lu18 103(3) . . ?
Lu4 Lu20 Lu18 35.3(15) . . ?
Lu22 Lu20 Lu18 109(3) . . ?
Lu23 Lu20 Lu18 135(3) . . ?
Lu6 Lu20 Lu18 60.2(15) . . ?
Lu3 Lu20 Lu2 64.9(19) . . ?
Lu21 Lu20 Lu2 90(3) . . ?
Lu4 Lu20 Lu2 42.5(14) . . ?
Lu22 Lu20 Lu2 44(2) . . ?
Lu23 Lu20 Lu2 159(3) . . ?
Lu6 Lu20 Lu2 124(2) . . ?
Lu18 Lu20 Lu2 65.4(16) . . ?
Lu3 Lu20 Lu5 9.4(14) . . ?
Lu21 Lu20 Lu5 63(3) . . ?
Lu4 Lu20 Lu5 16.9(14) . . ?
Lu22 Lu20 Lu5 84(3) . . ?
Lu23 Lu20 Lu5 132(3) . . ?
Lu6 Lu20 Lu5 75.5(16) . . ?
Lu18 Lu20 Lu5 42.8(14) . . ?
Lu2 Lu20 Lu5 55.7(14) . . ?
Lu3 Lu20 C1C 124(2) . . ?
Lu21 Lu20 C1C 161(3) . . ?
Lu4 Lu20 C1C 116(2) . . ?
Lu22 Lu20 C1C 121(3) . . ?
Lu23 Lu20 C1C 82(3) . . ?
Lu6 Lu20 C1C 78.1(13) . . ?
Lu18 Lu20 C1C 83.8(14) . . ?
Lu2 Lu20 C1C 108.6(15) . . ?
Lu5 Lu20 C1C 126.6(17) . . ?
Lu3 Lu20 C2C 125(3) . . ?
Lu21 Lu20 C2C 158(3) . . ?
Lu4 Lu20 C2C 103(2) . . ?
Lu22 Lu20 C2C 84(2) . . ?
Lu23 Lu20 C2C 106(3) . . ?
Lu6 Lu20 C2C 111.7(15) . . ?
Lu18 Lu20 C2C 87.0(14) . . ?
Lu2 Lu20 C2C 76.4(12) . . ?
Lu5 Lu20 C2C 119.6(17) . . ?
C1C Lu20 C2C 37.3(8) . . ?
Lu3 Lu20 Lu1 89.8(17) . . ?
Lu21 Lu20 Lu1 116(2) . . ?
Lu4 Lu20 Lu1 99.9(17) . . ?
Lu22 Lu20 Lu1 170(3) . . ?
Lu23 Lu20 Lu1 71(2) . . ?
Lu6 Lu20 Lu1 28.0(8) . . ?
Lu18 Lu20 Lu1 67.3(12) . . ?
Lu2 Lu20 Lu1 129.9(16) . . ?
Lu5 Lu20 Lu1 97.5(13) . . ?
C1C Lu20 Lu1 50.4(8) . . ?
C2C Lu20 Lu1 85.9(10) . . ?
Lu3 Lu21 Lu20 52(3) . . ?
Lu3 Lu21 Lu22 77(3) . . ?
Lu20 Lu21 Lu22 55(3) . . ?
Lu3 Lu21 Lu4 15.9(12) . . ?
Lu20 Lu21 Lu4 51(3) . . ?
Lu22 Lu21 Lu4 63(3) . . ?
Lu3 Lu21 Lu23 99(4) . . ?
Lu20 Lu21 Lu23 57(3) . . ?
Lu22 Lu21 Lu23 92(3) . . ?
Lu4 Lu21 Lu23 106(4) . . ?
Lu3 Lu21 Lu5 34.3(19) . . ?
Lu20 Lu21 Lu5 85(4) . . ?
Lu22 Lu21 Lu5 88(3) . . ?
Lu4 Lu21 Lu5 34.7(16) . . ?
Lu23 Lu21 Lu5 132(4) . . ?
Lu3 Lu21 Lu6 50.8(19) . . ?
Lu20 Lu21 Lu6 58(2) . . ?
Lu22 Lu21 Lu6 111(3) . . ?
Lu4 Lu21 Lu6 65.7(19) . . ?
Lu23 Lu21 Lu6 62(2) . . ?
Lu5 Lu21 Lu6 73(2) . . ?
Lu3 Lu21 Lu2 51(2) . . ?
Lu20 Lu21 Lu2 61(3) . . ?
Lu22 Lu21 Lu2 35(2) . . ?
Lu4 Lu21 Lu2 34.7(13) . . ?
Lu23 Lu21 Lu2 115(3) . . ?
Lu5 Lu21 Lu2 53.4(17) . . ?
Lu6 Lu21 Lu2 99(2) . . ?
Lu3 Lu21 Lu18 3.7(14) . . ?
Lu20 Lu21 Lu18 50(3) . . ?
Lu22 Lu21 Lu18 78(3) . . ?
Lu4 Lu21 Lu18 18.5(12) . . ?
Lu23 Lu21 Lu18 95(3) . . ?
Lu5 Lu21 Lu18 37.5(16) . . ?
Lu6 Lu21 Lu18 47.5(14) . . ?
Lu2 Lu21 Lu18 53.0(15) . . ?
Lu3 Lu21 Lu1 55.1(19) . . ?
Lu20 Lu21 Lu1 47(2) . . ?
Lu22 Lu21 Lu1 102(3) . . ?
Lu4 Lu21 Lu1 67.9(16) . . ?
Lu23 Lu21 Lu1 50(2) . . ?
Lu5 Lu21 Lu1 83.1(19) . . ?
Lu6 Lu21 Lu1 14.0(7) . . ?
Lu2 Lu21 Lu1 96.9(17) . . ?
Lu18 Lu21 Lu1 51.5(10) . . ?
Lu3 Lu21 C1C 58.2(19) . . ?
Lu20 Lu21 C1C 13(2) . . ?
Lu22 Lu21 C1C 66(2) . . ?
Lu4 Lu21 C1C 61.0(17) . . ?
Lu23 Lu21 C1C 45(2) . . ?
Lu5 Lu21 C1C 92(2) . . ?
Lu6 Lu21 C1C 50.1(11) . . ?
Lu2 Lu21 C1C 73.5(14) . . ?
Lu18 Lu21 C1C 55.2(11) . . ?
Lu1 Lu21 C1C 37.7(6) . . ?
Lu3 Lu21 C2C 59.0(19) . . ?
Lu20 Lu21 C2C 15.0(18) . . ?
Lu22 Lu21 C2C 40(2) . . ?
Lu4 Lu21 C2C 53.6(15) . . ?
Lu23 Lu21 C2C 63(2) . . ?
Lu5 Lu21 C2C 88(2) . . ?
Lu6 Lu21 C2C 72.6(14) . . ?
Lu2 Lu21 C2C 52.2(10) . . ?
Lu18 Lu21 C2C 57.6(12) . . ?
Lu1 Lu21 C2C 61.9(8) . . ?
C1C Lu21 C2C 25.6(5) . . ?
Lu20 Lu22 Lu21 51(3) . . ?
Lu20 Lu22 Lu2 101(3) . . ?
Lu21 Lu22 Lu2 111(3) . . ?
Lu20 Lu22 Lu4 49(2) . . ?
Lu21 Lu22 Lu4 59(3) . . ?
Lu2 Lu22 Lu4 58.4(19) . . ?
Lu20 Lu22 Lu3 38(2) . . ?
Lu21 Lu22 Lu3 42(2) . . ?
Lu2 Lu22 Lu3 75(2) . . ?
Lu4 Lu22 Lu3 17.4(6) . . ?
Lu20 Lu22 Lu23 35(3) . . ?
Lu21 Lu22 Lu23 49(2) . . ?
Lu2 Lu22 Lu23 137(3) . . ?
Lu4 Lu22 Lu23 81(2) . . ?
Lu3 Lu22 Lu23 66(2) . . ?
Lu20 Lu22 Lu5 65(3) . . ?
Lu21 Lu22 Lu5 55(3) . . ?
Lu2 Lu22 Lu5 56.3(18) . . ?
Lu4 Lu22 Lu5 21.1(12) . . ?
Lu3 Lu22 Lu5 27.1(11) . . ?
Lu23 Lu22 Lu5 91(2) . . ?
Lu20 Lu22 Lu18 45(2) . . ?
Lu21 Lu22 Lu18 69(3) . . ?
Lu2 Lu22 Lu18 56.6(18) . . ?
Lu4 Lu22 Lu18 14.6(11) . . ?
Lu3 Lu22 Lu18 26.9(11) . . ?
Lu23 Lu22 Lu18 80(2) . . ?
Lu5 Lu22 Lu18 35.0(12) . . ?
Lu20 Lu22 C2C 69(2) . . ?
Lu21 Lu22 C2C 120(3) . . ?
Lu2 Lu22 C2C 81.5(19) . . ?
Lu4 Lu22 C2C 86.4(19) . . ?
Lu3 Lu22 C2C 92.5(19) . . ?
Lu23 Lu22 C2C 81.3(18) . . ?
Lu5 Lu22 C2C 106.2(19) . . ?
Lu18 Lu22 C2C 71.8(13) . . ?
Lu20 Lu22 Lu6 13(2) . . ?
Lu21 Lu22 Lu6 42(2) . . ?
Lu2 Lu22 Lu6 95(2) . . ?
Lu4 Lu22 Lu6 38.9(13) . . ?
Lu3 Lu22 Lu6 25.9(10) . . ?
Lu23 Lu22 Lu6 42.3(17) . . ?
Lu5 Lu22 Lu6 53.0(13) . . ?
Lu18 Lu22 Lu6 38.9(10) . . ?
C2C Lu22 Lu6 78.9(12) . . ?
Lu20 Lu22 C1C 41(2) . . ?
Lu21 Lu22 C1C 91(3) . . ?
Lu2 Lu22 C1C 95(2) . . ?
Lu4 Lu22 C1C 72.3(17) . . ?
Lu3 Lu22 C1C 71.5(15) . . ?
Lu23 Lu22 C1C 54.8(17) . . ?
Lu5 Lu22 C1C 93.3(16) . . ?
Lu18 Lu22 C1C 59.8(11) . . ?
C2C Lu22 C1C 29.0(7) . . ?
Lu6 Lu22 C1C 52.1(9) . . ?
Lu20 Lu22 C3C 65(2) . . ?
Lu21 Lu22 C3C 113(3) . . ?
Lu2 Lu22 C3C 63.1(17) . . ?
Lu4 Lu22 C3C 67.2(16) . . ?
Lu3 Lu22 C3C 76.8(16) . . ?
Lu23 Lu22 C3C 88.7(19) . . ?
Lu5 Lu22 C3C 85.6(16) . . ?
Lu18 Lu22 C3C 52.7(11) . . ?
C2C Lu22 C3C 21.8(7) . . ?
Lu6 Lu22 C3C 70.9(11) . . ?
C1C Lu22 C3C 34.7(7) . . ?
Lu20 Lu23 Lu21 43(3) . . ?
Lu20 Lu23 Lu6 61(2) . . ?
Lu21 Lu23 Lu6 71(3) . . ?
Lu20 Lu23 Lu3 22.4(16) . . ?
Lu21 Lu23 Lu3 31(2) . . ?
Lu6 Lu23 Lu3 47.9(15) . . ?
Lu20 Lu23 Lu22 29.5(18) . . ?
Lu21 Lu23 Lu22 40(2) . . ?
Lu6 Lu23 Lu22 89(3) . . ?
Lu3 Lu23 Lu22 43.0(15) . . ?
Lu20 Lu23 Lu4 14.0(15) . . ?
Lu21 Lu23 Lu4 34(2) . . ?
Lu6 Lu23 Lu4 52.8(16) . . ?
Lu3 Lu23 Lu4 8.5(5) . . ?
Lu22 Lu23 Lu4 36.7(15) . . ?
Lu20 Lu23 C1C 66(2) . . ?
Lu21 Lu23 C1C 108(3) . . ?
Lu6 Lu23 C1C 70.2(19) . . ?
Lu3 Lu23 C1C 80(2) . . ?
Lu22 Lu23 C1C 83(2) . . ?
Lu4 Lu23 C1C 75.0(17) . . ?
Lu20 Lu23 Lu1 79(3) . . ?
Lu21 Lu23 Lu1 102(3) . . ?
Lu6 Lu23 Lu1 32.6(10) . . ?
Lu3 Lu23 Lu1 75.0(17) . . ?
Lu22 Lu23 Lu1 109(3) . . ?
Lu4 Lu23 Lu1 76.7(16) . . ?
C1C Lu23 Lu1 49.9(11) . . ?
Lu20 Lu23 Lu18 26.0(18) . . ?
Lu21 Lu23 Lu18 52(3) . . ?
Lu6 Lu23 Lu18 35.6(14) . . ?
Lu3 Lu23 Lu18 21.6(9) . . ?
Lu22 Lu23 Lu18 55.1(18) . . ?
Lu4 Lu23 Lu18 21.1(9) . . ?
C1C Lu23 Lu18 61.2(14) . . ?
Lu1 Lu23 Lu18 55.7(12) . . ?
Lu20 Lu23 C2C 49(2) . . ?
Lu21 Lu23 C2C 89(3) . . ?
Lu6 Lu23 C2C 84(2) . . ?
Lu3 Lu23 C2C 69.5(16) . . ?
Lu22 Lu23 C2C 55.4(16) . . ?
Lu4 Lu23 C2C 61.7(13) . . ?
C1C Lu23 C2C 29.8(8) . . ?
Lu1 Lu23 C2C 75.3(14) . . ?
Lu18 Lu23 C2C 58.4(12) . . ?
Lu20 Lu23 Lu5 29.2(18) . . ?
Lu21 Lu23 Lu5 26(2) . . ?
Lu6 Lu23 Lu5 47.9(15) . . ?
Lu3 Lu23 Lu5 7.3(8) . . ?
Lu22 Lu23 Lu5 46.0(16) . . ?
Lu4 Lu23 Lu5 15.3(8) . . ?
C1C Lu23 Lu5 87.2(18) . . ?
Lu1 Lu23 Lu5 77.3(15) . . ?
Lu18 Lu23 Lu5 27.1(9) . . ?
C2C Lu23 Lu5 76.8(15) . . ?
Lu20 Lu23 Lu2 12.5(17) . . ?
Lu21 Lu23 Lu2 39(2) . . ?
Lu6 Lu23 Lu2 73.0(19) . . ?
Lu3 Lu23 Lu2 29.1(9) . . ?
Lu22 Lu23 Lu2 17.0(13) . . ?
Lu4 Lu23 Lu2 21.5(8) . . ?
C1C Lu23 Lu2 73.2(15) . . ?
Lu1 Lu23 Lu2 91.9(17) . . ?
Lu18 Lu23 Lu2 38.2(10) . . ?
C2C Lu23 Lu2 50.7(10) . . ?
Lu5 Lu23 Lu2 34.1(9) . . ?
Lu12 Lu24 Lu13 87(5) . . ?
Lu12 Lu24 Lu16 44(3) . . ?
Lu13 Lu24 Lu16 53(3) . . ?
Lu12 Lu24 Lu7 32(3) . . ?
Lu13 Lu24 Lu7 64(3) . . ?
Lu16 Lu24 Lu7 12.9(8) . . ?
Lu12 Lu24 Lu9 59(4) . . ?
Lu13 Lu24 Lu9 31(2) . . ?
Lu16 Lu24 Lu9 41(2) . . ?
Lu7 Lu24 Lu9 47(2) . . ?
Lu12 Lu24 Lu15 35(3) . . ?
Lu13 Lu24 Lu15 81(3) . . ?
Lu16 Lu24 Lu15 29.1(16) . . ?
Lu7 Lu24 Lu15 20.6(11) . . ?
Lu9 Lu24 Lu15 67(3) . . ?
Lu12 Lu24 Lu10 58(4) . . ?
Lu13 Lu24 Lu10 59(3) . . ?
Lu16 Lu24 Lu10 20.6(15) . . ?
Lu7 Lu24 Lu10 27.3(12) . . ?
Lu9 Lu24 Lu10 58(2) . . ?
Lu15 Lu24 Lu10 28.4(13) . . ?
Lu12 Lu24 Lu8 87(4) . . ?
Lu13 Lu24 Lu8 46(2) . . ?
Lu16 Lu24 Lu8 44.1(15) . . ?
Lu7 Lu24 Lu8 55.1(14) . . ?
Lu9 Lu24 Lu8 64(2) . . ?
Lu15 Lu24 Lu8 57.7(15) . . ?
Lu10 Lu24 Lu8 29.8(10) . . ?
Lu12 Lu24 Lu14 40(3) . . ?
Lu13 Lu24 Lu14 59(3) . . ?
Lu16 Lu24 Lu14 6.2(13) . . ?
Lu7 Lu24 Lu14 8.1(10) . . ?
Lu9 Lu24 Lu14 46(2) . . ?
Lu15 Lu24 Lu14 23.0(12) . . ?
Lu10 Lu24 Lu14 20.2(9) . . ?
Lu8 Lu24 Lu14 47.0(12) . . ?
Lu12 Lu24 Lu19 20(3) . . ?
Lu13 Lu24 Lu19 68(3) . . ?
Lu16 Lu24 Lu19 35.5(16) . . ?
Lu7 Lu24 Lu19 28.1(12) . . ?
Lu9 Lu24 Lu19 39(2) . . ?
Lu15 Lu24 Lu19 43.0(14) . . ?
Lu10 Lu24 Lu19 54.7(16) . . ?
Lu8 Lu24 Lu19 79.1(17) . . ?
Lu14 Lu24 Lu19 34.5(12) . . ?
Lu12 Lu24 Lu17 27(3) . . ?
Lu13 Lu24 Lu17 87(3) . . ?
Lu16 Lu24 Lu17 35(2) . . ?
Lu7 Lu24 Lu17 23.2(17) . . ?
Lu9 Lu24 Lu17 69(3) . . ?
Lu15 Lu24 Lu17 10.0(14) . . ?
Lu10 Lu24 Lu17 37.9(16) . . ?
Lu8 Lu24 Lu17 67.5(18) . . ?
Lu14 Lu24 Lu17 28.4(15) . . ?
Lu19 Lu24 Lu17 38.5(16) . . ?
Lu12 Lu24 Lu11 32(3) . . ?
Lu13 Lu24 Lu11 62(3) . . ?
Lu16 Lu24 Lu11 42.9(17) . . ?
Lu7 Lu24 Lu11 38.8(13) . . ?
Lu9 Lu24 Lu11 31.1(19) . . ?
Lu15 Lu24 Lu11 55.8(15) . . ?
Lu10 Lu24 Lu11 63.4(15) . . ?
Lu8 Lu24 Lu11 83.5(15) . . ?
Lu14 Lu24 Lu11 43.7(11) . . ?
Lu19 Lu24 Lu11 13.3(7) . . ?
Lu17 Lu24 Lu11 51.7(15) . . ?
C2C C1C C3C 46.1(11) . . ?
C2C C1C Lu1 139.5(15) . . ?
C3C C1C Lu1 115.6(14) . . ?
C2C C1C Lu8 122.0(15) . . ?
C3C C1C Lu8 100.0(14) . . ?
Lu1 C1C Lu8 94.3(9) . . ?
C2C C1C Lu20 72.3(12) . . ?
C3C C1C Lu20 91.8(15) . . ?
Lu1 C1C Lu20 73.0(10) . . ?
Lu8 C1C Lu20 165.6(13) . . ?
C2C C1C Lu14 75.5(13) . . ?
C3C C1C Lu14 55.1(14) . . ?
Lu1 C1C Lu14 128.6(12) . . ?
Lu8 C1C Lu14 49.1(10) . . ?
Lu20 C1C Lu14 144.9(14) . . ?
C2C C1C Lu10 96.2(15) . . ?
C3C C1C Lu10 71.4(14) . . ?
Lu1 C1C Lu10 111.9(12) . . ?
Lu8 C1C Lu10 29.3(8) . . ?
Lu20 C1C Lu10 163.0(14) . . ?
Lu14 C1C Lu10 20.8(8) . . ?
C2C C1C Lu23 93.4(16) . . ?
C3C C1C Lu23 123.1(19) . . ?
Lu1 C1C Lu23 66.0(12) . . ?
Lu8 C1C Lu23 136.8(16) . . ?
Lu20 C1C Lu23 31.6(13) . . ?
Lu14 C1C Lu23 165.4(16) . . ?
Lu10 C1C Lu23 165.3(17) . . ?
C2C C1C Lu6 108.7(14) . . ?
C3C C1C Lu6 105.1(14) . . ?
Lu1 C1C Lu6 33.0(6) . . ?
Lu8 C1C Lu6 127.3(10) . . ?
Lu20 C1C Lu6 40.2(9) . . ?
Lu14 C1C Lu6 149.5(13) . . ?
Lu10 C1C Lu6 141.2(13) . . ?
Lu23 C1C Lu6 43.1(12) . . ?
C2C C1C Lu13 94.2(18) . . ?
C3C C1C Lu13 102.4(19) . . ?
Lu1 C1C Lu13 126.4(16) . . ?
Lu8 C1C Lu13 40.6(13) . . ?
Lu20 C1C Lu13 144.3(16) . . ?
Lu14 C1C Lu13 51.1(15) . . ?
Lu10 C1C Lu13 46.4(14) . . ?
Lu23 C1C Lu13 121.9(19) . . ?
Lu6 C1C Lu13 152.0(17) . . ?
C2C C1C Lu9 76.9(13) . . ?
C3C C1C Lu9 86.9(16) . . ?
Lu1 C1C Lu9 143.5(12) . . ?
Lu8 C1C Lu9 51.9(10) . . ?
Lu20 C1C Lu9 137.9(14) . . ?
Lu14 C1C Lu9 42.0(13) . . ?
Lu10 C1C Lu9 45.9(13) . . ?
Lu23 C1C Lu9 126.8(17) . . ?
Lu6 C1C Lu9 167.4(14) . . ?
Lu13 C1C Lu9 17.9(11) . . ?
C2C C1C Lu16 85.2(12) . . ?
C3C C1C Lu16 77.5(13) . . ?
Lu1 C1C Lu16 130.8(10) . . ?
Lu8 C1C Lu16 37.2(7) . . ?
Lu20 C1C Lu16 156.2(12) . . ?
Lu14 C1C Lu16 23.8(9) . . ?
Lu10 C1C Lu16 23.4(9) . . ?
Lu23 C1C Lu16 148.3(15) . . ?
Lu6 C1C Lu16 163.3(11) . . ?
Lu13 C1C Lu16 27.4(13) . . ?
Lu9 C1C Lu16 22.5(9) . . ?
C3C C2C C1C 84.0(14) . . ?
C3C C2C Lu20 107.1(17) . . ?
C1C C2C Lu20 70.4(13) . . ?
C3C C2C Lu11 87.3(14) . . ?
C1C C2C Lu11 131.5(12) . . ?
Lu20 C2C Lu11 156.0(8) . . ?
C3C C2C Lu22 116.8(18) . . ?
C1C C2C Lu22 96.5(15) . . ?
Lu20 C2C Lu22 26.8(10) . . ?
Lu11 C2C Lu22 129.4(10) . . ?
C3C C2C Lu14 55.4(15) . . ?
C1C C2C Lu14 69.5(13) . . ?
Lu20 C2C Lu14 137.6(11) . . ?
Lu11 C2C Lu14 66.4(8) . . ?
Lu22 C2C Lu14 163.9(13) . . ?
C3C C2C Lu2 90.2(15) . . ?
C1C C2C Lu2 109.3(13) . . ?
Lu20 C2C Lu2 44.8(10) . . ?
Lu11 C2C Lu2 118.4(7) . . ?
Lu22 C2C Lu2 30.3(10) . . ?
Lu14 C2C Lu2 145.5(10) . . ?
C3C C2C Lu19 74.3(16) . . ?
C1C C2C Lu19 99.9(13) . . ?
Lu20 C2C Lu19 169.7(11) . . ?
Lu11 C2C Lu19 32.4(6) . . ?
Lu22 C2C Lu19 161.2(12) . . ?
Lu14 C2C Lu19 34.9(10) . . ?
Lu2 C2C Lu19 145.3(9) . . ?
C3C C2C Lu9 96.0(17) . . ?
C1C C2C Lu9 71.1(13) . . ?
Lu20 C2C Lu9 132.0(12) . . ?
Lu11 C2C Lu9 62.5(8) . . ?
Lu22 C2C Lu9 143.9(14) . . ?
Lu14 C2C Lu9 40.7(12) . . ?
Lu2 C2C Lu9 173.8(12) . . ?
Lu19 C2C Lu9 38.3(10) . . ?
C3C C2C Lu4 89.5(15) . . ?
C1C C2C Lu4 80.9(11) . . ?
Lu20 C2C Lu4 22.1(9) . . ?
Lu11 C2C Lu4 146.8(5) . . ?
Lu22 C2C Lu4 30.2(10) . . ?
Lu14 C2C Lu4 135.1(9) . . ?
Lu2 C2C Lu4 28.5(6) . . ?
Lu19 C2C Lu4 163.5(8) . . ?
Lu9 C2C Lu4 150.6(9) . . ?
C3C C2C Lu18 68.6(16) . . ?
C1C C2C Lu18 71.0(12) . . ?
Lu20 C2C Lu18 38.8(9) . . ?
Lu11 C2C Lu18 146.3(7) . . ?
Lu22 C2C Lu18 52.9(11) . . ?
Lu14 C2C Lu18 112.9(11) . . ?
Lu2 C2C Lu18 42.5(8) . . ?
Lu19 C2C Lu18 142.4(9) . . ?
Lu9 C2C Lu18 140.2(10) . . ?
Lu4 C2C Lu18 22.7(7) . . ?
C3C C2C Lu3 93.7(15) . . ?
C1C C2C Lu3 74.4(11) . . ?
Lu20 C2C Lu3 14.9(8) . . ?
Lu11 C2C Lu3 154.0(5) . . ?
Lu22 C2C Lu3 30.3(9) . . ?
Lu14 C2C Lu3 133.9(9) . . ?
Lu2 C2C Lu3 35.7(6) . . ?
Lu19 C2C Lu3 167.3(7) . . ?
Lu9 C2C Lu3 142.8(8) . . ?
Lu4 C2C Lu3 8.2(2) . . ?
Lu18 C2C Lu3 25.2(6) . . ?
C2C C3C C1C 49.9(11) . . ?
C2C C3C Lu14 90.7(18) . . ?
C1C C3C Lu14 74.8(15) . . ?
C2C C3C Lu10 92.5(16) . . ?
C1C C3C Lu10 63.6(13) . . ?
Lu14 C3C Lu10 17.6(11) . . ?
C2C C3C Lu19 75.1(15) . . ?
C1C C3C Lu19 89.4(14) . . ?
Lu14 C3C Lu19 36.0(12) . . ?
Lu10 C3C Lu19 52.8(12) . . ?
C2C C3C Lu18 82.6(17) . . ?
C1C C3C Lu18 71.4(14) . . ?
Lu14 C3C Lu18 140.7(16) . . ?
Lu10 C3C Lu18 123.6(14) . . ?
Lu19 C3C Lu18 156.9(14) . . ?
C2C C3C Lu11 62.5(12) . . ?
C1C C3C Lu11 99.1(13) . . ?
Lu14 C3C Lu11 66.5(12) . . ?
Lu10 C3C Lu11 82.7(12) . . ?
Lu19 C3C Lu11 30.7(7) . . ?
Lu18 C3C Lu11 138.0(13) . . ?
C2C C3C Lu16 77.0(14) . . ?
C1C C3C Lu16 63.4(11) . . ?
Lu14 C3C Lu16 14.1(9) . . ?
Lu10 C3C Lu16 21.0(9) . . ?
Lu19 C3C Lu16 35.0(8) . . ?
Lu18 C3C Lu16 133.4(12) . . ?
Lu11 C3C Lu16 63.1(8) . . ?
C2C C3C Lu7 80.8(14) . . ?
C1C C3C Lu7 70.1(11) . . ?
Lu14 C3C Lu7 10.2(9) . . ?
Lu10 C3C Lu7 23.0(9) . . ?
Lu19 C3C Lu7 30.3(7) . . ?
Lu18 C3C Lu7 140.0(12) . . ?
Lu11 C3C Lu7 59.7(6) . . ?
Lu16 C3C Lu7 6.7(3) . . ?
C2C C3C Lu17 107(2) . . ?
C1C C3C Lu17 96(2) . . ?
Lu14 C3C Lu17 21.9(17) . . ?
Lu10 C3C Lu17 34.8(15) . . ?
Lu19 C3C Lu17 36.7(14) . . ?
Lu18 C3C Lu17 154.5(16) . . ?
Lu11 C3C Lu17 64.7(13) . . ?
Lu16 C3C Lu17 35.0(15) . . ?
Lu7 C3C Lu17 29.0(15) . . ?
C2C C3C Lu2 62.0(13) . . ?
C1C C3C Lu2 85.5(14) . . ?
Lu14 C3C Lu2 152.7(15) . . ?
Lu10 C3C Lu2 148.8(14) . . ?
Lu19 C3C Lu2 127.4(12) . . ?
Lu18 C3C Lu2 40.9(9) . . ?
Lu11 C3C Lu2 99.0(9) . . ?
Lu16 C3C Lu2 138.8(11) . . ?
Lu7 C3C Lu2 142.8(11) . . ?
Lu17 C3C Lu2 163.7(16) . . ?
C2C C3C Lu20 46.9(13) . . ?
C1C C3C Lu20 49.0(12) . . ?
Lu14 C3C Lu20 122.6(15) . . ?
Lu10 C3C Lu20 112.6(13) . . ?
Lu19 C3C Lu20 121.2(13) . . ?
Lu18 C3C Lu20 35.9(9) . . ?
Lu11 C3C Lu20 107.2(10) . . ?
Lu16 C3C Lu20 109.5(11) . . ?
Lu7 C3C Lu20 115.7(11) . . ?
Lu17 C3C Lu20 144.4(19) . . ?
Lu2 C3C Lu20 37.0(8) . . ?
N1A Ni1A N3A 178.4(2) . . ?
N1A Ni1A N2A 89.6(2) . . ?
N3A Ni1A N2A 90.3(2) . . ?
N1A Ni1A N4A 90.4(2) . . ?
N3A Ni1A N4A 89.6(3) . . ?
N2A Ni1A N4A 177.8(2) . . ?
C8A N1A C1A 105.5(6) . . ?
C8A N1A Ni1A 127.8(5) . . ?
C1A N1A Ni1A 126.7(5) . . ?
C10A N2A C16A 104.6(6) . . ?
C10A N2A Ni1A 127.5(5) . . ?
C16A N2A Ni1A 127.8(5) . . ?
C35A N3A C18A 106.3(6) . . ?
C35A N3A Ni1A 127.3(5) . . ?
C18A N3A Ni1A 126.3(5) . . ?
C26A N4A C33A 104.4(6) . . ?
C26A N4A Ni1A 127.7(5) . . ?
C33A N4A Ni1A 127.8(5) . . ?
C34A C1A N1A 126.2(6) . . ?
C34A C1A C2A 123.6(7) . . ?
N1A C1A C2A 110.1(7) . . ?
C5A C2A C1A 106.6(6) . . ?
C5A C2A C3A 128.7(7) . . ?
C1A C2A C3A 124.7(7) . . ?
C2A C3A C4A 113.5(6) . . ?
C2A C5A C8A 106.3(7) . . ?
C2A C5A C6A 128.8(6) . . ?
C8A C5A C6A 124.7(7) . . ?
C5A C6A C7A 112.4(6) . . ?
N1A C8A C9A 125.8(6) . . ?
N1A C8A C5A 111.5(6) . . ?
C9A C8A C5A 122.7(7) . . ?
C10A C9A C8A 123.5(7) . . ?
C9A C10A N2A 125.6(7) . . ?
C9A C10A C11A 123.6(7) . . ?
N2A C10A C11A 110.8(6) . . ?
C13A C11A C10A 105.9(7) . . ?
C13A C11A C12A 130.0(7) . . ?
C10A C11A C12A 124.1(7) . . ?
C11A C12A C36A 113.8(7) . . ?
C11A C13A C16A 107.2(7) . . ?
C11A C13A C14A 127.1(8) . . ?
C16A C13A C14A 125.6(7) . . ?
C13A C14A C15A 113.2(7) . . ?
C17A C16A N2A 124.3(7) . . ?
C17A C16A C13A 124.3(6) . . ?
N2A C16A C13A 111.4(6) . . ?
C18A C17A C16A 124.4(6) . . ?
C17A C18A N3A 126.8(7) . . ?
C17A C18A C19A 123.6(7) . . ?
N3A C18A C19A 109.6(7) . . ?
C22A C19A C18A 107.1(6) . . ?
C22A C19A C20A 128.4(7) . . ?
C18A C19A C20A 124.3(7) . . ?
C19A C20A C21A 112.1(6) . . ?
C19A C22A C35A 106.1(7) . . ?
C19A C22A C23A 128.6(6) . . ?
C35A C22A C23A 125.1(7) . . ?
C22A C23A C24A 111.7(7) . . ?
C35A C25A C26A 122.4(7) . . ?
N4A C26A C25A 125.9(7) . . ?
N4A C26A C27A 112.0(6) . . ?
C25A C26A C27A 122.1(7) . . ?
C30A C27A C26A 104.8(7) . . ?
C30A C27A C28A 129.7(7) . . ?
C26A C27A C28A 125.6(7) . . ?
C27A C28A C29A 114.0(7) . . ?
C27A C30A C33A 107.7(7) . . ?
C27A C30A C31A 127.8(8) . . ?
C33A C30A C31A 124.4(7) . . ?
C32A C31A C30A 113.9(7) . . ?
N4A C33A C34A 123.8(7) . . ?
N4A C33A C30A 111.1(6) . . ?
C34A C33A C30A 125.1(7) . . ?
C1A C34A C33A 125.1(6) . . ?
N3A C35A C25A 127.1(6) . . ?
N3A C35A C22A 110.8(6) . . ?
C25A C35A C22A 122.1(7) . . ?
C9 C1 C2 122.6(13) . . ?
C9 C1 C5 122.6(13) . . ?
C2 C1 C5 103.7(13) . . ?
C12 C2 C3 119.6(12) . . ?
C12 C2 C1 121.5(12) . . ?
C3 C2 C1 110.1(14) . . ?
C4 C3 C2 109.7(14) . . ?
C4 C3 C15 118.9(13) . . ?
C2 C3 C15 121.5(13) . . ?
C18 C4 C3 120.9(15) . . ?
C18 C4 C5 122.4(16) . . ?
C3 C4 C5 105.9(14) . . ?
C6 C5 C4 117.6(16) . . ?
C6 C5 C1 119.8(16) . . ?
C4 C5 C1 109.8(13) . . ?
C5 C6 C20 121.5(18) . . ?
C5 C6 C7 120.8(17) . . ?
C20 C6 C7 106.7(14) . . ?
C8 C7 C22 125.3(14) . . ?
C8 C7 C6 121.2(13) . . ?
C22 C7 C6 104.6(15) . . ?
C7 C8 C25 116.8(14) . . ?
C7 C8 C9 116.0(13) . . ?
C25 C8 C9 121.2(16) . . ?
C1 C9 C10 116.0(13) . . ?
C1 C9 C8 119.2(15) . . ?
C10 C9 C8 117.6(14) . . ?
C11 C10 C27 113.1(16) . . ?
C11 C10 C9 122.0(13) . . ?
C27 C10 C9 120.1(16) . . ?
C10 C11 C12 118.6(13) . . ?
C10 C11 C29 108.0(13) . . ?
C12 C11 C29 121.4(13) . . ?
C2 C12 C13 120.9(12) . . ?
C2 C12 C11 116.7(12) . . ?
C13 C12 C11 114.1(12) . . ?
C31 C13 C12 123.8(14) . . ?
C31 C13 C14 108.4(13) . . ?
C12 C13 C14 118.1(13) . . ?
C33 C14 C15 121.4(14) . . ?
C33 C14 C13 108.8(14) . . ?
C15 C14 C13 122.4(11) . . ?
C14 C15 C3 115.9(12) . . ?
C14 C15 C16 118.0(12) . . ?
C3 C15 C16 119.3(14) . . ?
C17 C16 C35 119.5(14) . . ?
C17 C16 C15 116.0(13) . . ?
C35 C16 C15 119.0(13) . . ?
C16 C17 C18 122.0(15) . . ?
C16 C17 C38 122.0(15) . . ?
C18 C17 C38 109.1(18) . . ?
C4 C18 C17 122.0(17) . . ?
C4 C18 C19 120.8(19) . . ?
C17 C18 C19 104.3(15) . . ?
C39 C19 C20 117.4(19) . . ?
C39 C19 C18 113.6(19) . . ?
C20 C19 C18 116.1(17) . . ?
C21 C20 C19 118.1(16) . . ?
C21 C20 C6 110.6(18) . . ?
C19 C20 C6 121.3(17) . . ?
C20 C21 C22 106.9(16) . . ?
C20 C21 C41 123.9(19) . . ?
C22 C21 C41 119.7(17) . . ?
C23 C22 C21 124.1(15) . . ?
C23 C22 C7 116.4(18) . . ?
C21 C22 C7 110.9(15) . . ?
C22 C23 C43 116.4(19) . . ?
C22 C23 C24 121.2(15) . . ?
C43 C23 C24 118.2(16) . . ?
C23 C24 C25 122.0(14) . . ?
C23 C24 C46 118.9(14) . . ?
C25 C24 C46 114.8(17) . . ?
C24 C25 C26 123.4(15) . . ?
C24 C25 C8 118.0(17) . . ?
C26 C25 C8 115.9(15) . . ?
C48 C26 C25 119.3(17) . . ?
C48 C26 C27 113(2) . . ?
C25 C26 C27 122.5(16) . . ?
C10 C27 C26 121.5(19) . . ?
C10 C27 C28 104.3(16) . . ?
C26 C27 C28 125.3(17) . . ?
C50 C28 C29 126(2) . . ?
C50 C28 C27 116(2) . . ?
C29 C28 C27 109.6(15) . . ?
C30 C29 C28 121.6(19) . . ?
C30 C29 C11 119.9(16) . . ?
C28 C29 C11 104.9(16) . . ?
C29 C30 C31 118.7(18) . . ?
C29 C30 C52 115(2) . . ?
C31 C30 C52 113(2) . . ?
C13 C31 C30 121.9(17) . . ?
C13 C31 C32 107.7(16) . . ?
C30 C31 C32 119.7(18) . . ?
C31 C32 C54 123(2) . . ?
C31 C32 C33 106.7(14) . . ?
C54 C32 C33 122.7(17) . . ?
C14 C33 C34 124.0(16) . . ?
C14 C33 C32 108.5(15) . . ?
C34 C33 C32 119.6(14) . . ?
C33 C34 C56 117.0(16) . . ?
C33 C34 C35 118.2(13) . . ?
C56 C34 C35 119.2(13) . . ?
C34 C35 C36 119.8(12) . . ?
C34 C35 C16 118.7(13) . . ?
C36 C35 C16 118.5(15) . . ?
C59 C36 C37 117.0(13) . . ?
C59 C36 C35 120.6(15) . . ?
C37 C36 C35 119.0(14) . . ?
C38 C37 C62 114.9(17) . . ?
C38 C37 C36 119.8(15) . . ?
C62 C37 C36 119.9(13) . . ?
C37 C38 C17 121.1(18) . . ?
C37 C38 C39 121.0(16) . . ?
C17 C38 C39 108.9(16) . . ?
C19 C39 C40 124(2) . . ?
C19 C39 C38 103.9(18) . . ?
C40 C39 C38 122.9(14) . . ?
C41 C40 C39 117.7(17) . . ?
C41 C40 C63 115.4(18) . . ?
C39 C40 C63 118.0(19) . . ?
C40 C41 C21 117.9(18) . . ?
C40 C41 C42 118.1(16) . . ?
C21 C41 C42 116(2) . . ?
C41 C42 C43 121.6(16) . . ?
C41 C42 C65 126.2(18) . . ?
C43 C42 C65 103.2(15) . . ?
C44 C43 C23 124.3(19) . . ?
C44 C43 C42 109.6(14) . . ?
C23 C43 C42 119.5(17) . . ?
C43 C44 C66 112.1(17) . . ?
C43 C44 C45 121.6(15) . . ?
C66 C44 C45 120.8(14) . . ?
C69 C45 C46 121.1(18) . . ?
C69 C45 C44 114.9(14) . . ?
C46 C45 C44 118.2(15) . . ?
C47 C46 C45 117.7(17) . . ?
C47 C46 C24 119.7(15) . . ?
C45 C46 C24 118.8(18) . . ?
C46 C47 C48 123.5(18) . . ?
C46 C47 C71 123.5(16) . . ?
C48 C47 C71 105(2) . . ?
C26 C48 C49 122(2) . . ?
C26 C48 C47 119(2) . . ?
C49 C48 C47 109.4(19) . . ?
C48 C49 C50 123.5(19) . . ?
C48 C49 C72 109(2) . . ?
C50 C49 C72 116(3) . . ?
C28 C50 C51 115(2) . . ?
C28 C50 C49 119(3) . . ?
C51 C50 C49 120(2) . . ?
C50 C51 C52 123(2) . . ?
C50 C51 C57 119(2) . . ?
C52 C51 C57 107(2) . . ?
C53 C52 C51 106(2) . . ?
C53 C52 C30 128(2) . . ?
C51 C52 C30 119(2) . . ?
C74 C53 C52 111(3) . . ?
C74 C53 C54 122(2) . . ?
C52 C53 C54 118(2) . . ?
C55 C54 C53 118(2) . . ?
C55 C54 C32 115(2) . . ?
C53 C54 C32 117.7(19) . . ?
C54 C55 C76 122(2) . . ?
C54 C55 C56 123.9(18) . . ?
C76 C55 C56 105.5(16) . . ?
C34 C56 C58 119.2(16) . . ?
C34 C56 C55 120.8(15) . . ?
C58 C56 C55 110.8(16) . . ?
C73 C57 C74 123(2) . . ?
C73 C57 C51 124(3) . . ?
C74 C57 C51 106(2) . . ?
C59 C58 C56 123.9(13) . . ?
C59 C58 C77 119.9(12) . . ?
C56 C58 C77 105.9(15) . . ?
C58 C59 C36 116.8(13) . . ?
C58 C59 C60 118.4(13) . . ?
C36 C59 C60 120.9(14) . . ?
C61 C60 C79 116.1(12) . . ?
C61 C60 C59 120.1(13) . . ?
C79 C60 C59 119.0(14) . . ?
C60 C61 C62 121.2(14) . . ?
C60 C61 C82 123.2(11) . . ?
C62 C61 C82 109.1(13) . . ?
C61 C62 C63 107.9(14) . . ?
C61 C62 C37 120.4(15) . . ?
C63 C62 C37 124.0(14) . . ?
C64 C63 C40 129.1(19) . . ?
C64 C63 C62 107.2(13) . . ?
C40 C63 C62 117.4(17) . . ?
C63 C64 C82 111.3(15) . . ?
C63 C64 C65 118.9(14) . . ?
C82 C64 C65 112.7(14) . . ?
C66 C65 C64 122.4(13) . . ?
C66 C65 C42 108.7(16) . . ?
C64 C65 C42 111.1(15) . . ?
C65 C66 C44 106.3(14) . . ?
C65 C66 C67 123.3(13) . . ?
C44 C66 C67 119.6(15) . . ?
C68 C67 C81 120.0(14) . . ?
C68 C67 C66 117.1(12) . . ?
C81 C67 C66 115.4(13) . . ?
C67 C68 C85 120.6(13) . . ?
C67 C68 C69 121.1(14) . . ?
C85 C68 C69 109.3(15) . . ?
C45 C69 C68 123.4(16) . . ?
C45 C69 C70 120.1(14) . . ?
C68 C69 C70 104.7(15) . . ?
C71 C70 C86 119(2) . . ?
C71 C70 C69 122.1(19) . . ?
C86 C70 C69 108.9(15) . . ?
C70 C71 C72 124(2) . . ?
C70 C71 C47 114.6(19) . . ?
C72 C71 C47 110.4(19) . . ?
C73 C72 C71 123(2) . . ?
C73 C72 C49 122(3) . . ?
C71 C72 C49 105(3) . . ?
C57 C73 C72 119(2) . . ?
C57 C73 C87 121(2) . . ?
C72 C73 C87 115(2) . . ?
C53 C74 C57 109(2) . . ?
C53 C74 C75 122(2) . . ?
C57 C74 C75 121(2) . . ?
C88 C75 C76 121.6(18) . . ?
C88 C75 C74 118(2) . . ?
C76 C75 C74 113(2) . . ?
C75 C76 C77 118.8(16) . . ?
C75 C76 C55 121.2(17) . . ?
C77 C76 C55 108.8(17) . . ?
C78 C77 C76 119.9(17) . . ?
C78 C77 C58 121.6(15) . . ?
C76 C77 C58 108.7(13) . . ?
C77 C78 C83 122.2(16) . . ?
C77 C78 C79 117.6(14) . . ?
C83 C78 C79 110.3(12) . . ?
C60 C79 C80 120.9(12) . . ?
C60 C79 C78 122.3(12) . . ?
C80 C79 C78 103.8(12) . . ?
C81 C80 C79 122.2(12) . . ?
C81 C80 C84 118.7(11) . . ?
C79 C80 C84 109.6(13) . . ?
C80 C81 C82 117.4(11) . . ?
C80 C81 C67 119.3(12) . . ?
C82 C81 C67 116.7(11) . . ?
C81 C82 C64 128.8(13) . . ?
C81 C82 C61 117.2(11) . . ?
C64 C82 C61 104.1(12) . . ?
C78 C83 C84 109.3(14) . . ?
C78 C83 C88 121.3(14) . . ?
C84 C83 C88 118.7(15) . . ?
C85 C84 C83 123.1(15) . . ?
C85 C84 C80 119.5(13) . . ?
C83 C84 C80 106.7(13) . . ?
C84 C85 C86 120.7(16) . . ?
C84 C85 C68 121.8(14) . . ?
C86 C85 C68 107.7(14) . . ?
C70 C86 C85 109.2(17) . . ?
C70 C86 C87 120.1(17) . . ?
C85 C86 C87 120.9(17) . . ?
C86 C87 C88 118.9(17) . . ?
C86 C87 C73 119(2) . . ?
C88 C87 C73 114.8(18) . . ?
C75 C88 C83 115.1(18) . . ?
C75 C88 C87 122.4(18) . . ?
C83 C88 C87 117.7(16) . . ?
C2B C1B C6B 123.1(12) . . ?
C5B C4B C3B 113.0(11) . . ?
C4B C5B C6B 128.1(11) . . ?
C1B C6B C5B 113.7(11) . . ?
C3B C2B C1B 121.1(12) . . ?
C2B C3B C4B 121.0(11) . . ?
C3D C1D C7D 120.0 . . ?
C1D C3D C4D 120.0 . . ?
C3D C4D C5D 120.0 . . ?
C6D C5D C4D 120.0 . . ?
C7D C6D C5D 120.0 . . ?
C6D C7D C1D 120.0 . . ?
S2E C1E S1E 166(3) . . ?

_refine_diff_density_max         1.917
_refine_diff_density_min         -2.525
_refine_diff_density_rms         0.210


_vrf_PLAT029_Lu2C2@Cs-C88        
;
PROBLEM: PLAT029 Type_3  _diffrn_measured_fraction_theta_full value Low 
RESPONSE: Because of limited beamtime available, data was collected from only 
one crystal. The completeness of this data especialy in the highest resolution 
shell was restrained by some shaded areas (cryo-system or the beamstop)
;

_vrf_PLAT307_Lu2C2@Cs-C88        
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2C2@Cs-C88        
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2@Cs8-C86
_database_code_depnum_ccdc_archive 'CCDC 1582218'
_audit_update_record             
;
2017-10-26 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2@Cs(8)-C86 Ni(OEP)'
_chemical_name_common            'Lu2@Cs(8)-C86 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         '2(Lu2 C86), 3(C36 H44 N4 Ni), 2(C6 H6) '
_chemical_formula_sum            'C292 H144 Lu4 N12 Ni3'
_chemical_formula_weight         4696.19

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.4720 5.8584 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   24.454(5)
_cell_length_b                   18.039(5)
_cell_length_c                   22.303(5)
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 101.767(5)
_cell_angle_gamma                90.000(5)
_cell_volume                     9632(4)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9800
_cell_measurement_theta_min      2.930
_cell_measurement_theta_max      25.381

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.619
_exptl_crystal_F_000             4696
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.120
_exptl_crystal_size_min          0.080
_exptl_absorpt_coefficient_mu    2.388
_shelx_estimated_absorpt_T_min   0.716
_shelx_estimated_absorpt_T_max   0.826
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.4917
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71069
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean 8.3
_diffrn_reflns_number            50408
_diffrn_reflns_av_unetI/netI     0.0417
_diffrn_reflns_av_R_equivalents  0.0523
_diffrn_reflns_limit_h_min       -29
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_theta_min         2.929
_diffrn_reflns_theta_max         25.415
_diffrn_reflns_theta_full        25.240
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measured_fraction_theta_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.989
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.989
_diffrn_reflns_point_group_measured_fraction_full 0.992
_reflns_number_total             9087
_reflns_number_gt                6268
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0145P)²+368.2036P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         9087
_refine_ls_number_parameters     847
_refine_ls_number_restraints     1050
_refine_ls_R_factor_all          0.1807
_refine_ls_R_factor_gt           0.1332
_refine_ls_wR_factor_ref         0.2976
_refine_ls_wR_factor_gt          0.2687
_refine_ls_goodness_of_fit_ref   1.014
_refine_ls_restrained_S_all      0.996
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.64256(8) 0.07773(11) 0.22166(10) 0.0668(6) Uani 0.3021 1 d . U P A 1
Lu2 Lu 0.72422(9) 0.04215(14) 0.32572(10) 0.0880(7) Uani 0.315 1 d . U P A 1
Lu3 Lu 0.62777(17) 0.0000 0.2304(2) 0.122(2) Uani 0.241 2 d S TU P A 1
Lu4 Lu 0.7564(2) 0.0981(4) 0.2765(3) 0.0851(17) Uani 0.1211 1 d . U P A 1
Lu5 Lu 0.7316(9) 0.0865(10) 0.3039(9) 0.111(5) Uani 0.0538 1 d . U P A 1
Lu6 Lu 0.7855(7) 0.0000 0.2278(14) 0.24(2) Uani 0.0641 2 d S T P A 1
Lu7 Lu 0.6237(9) 0.0000 0.2653(11) 0.093(5) Uani 0.0432 2 d S TU P A 1
Lu8 Lu 0.6717(12) 0.0932(18) 0.2012(15) 0.131(8) Uani 0.0338 1 d . U P A 1
C1 C 0.7824(3) -0.1655(4) 0.1252(3) 0.124(6) Uani 0.5 1 d G U P A -1
C2 C 0.8339(3) -0.1443(4) 0.1685(4) 0.126(6) Uani 0.5 1 d G U P A -1
C3 C 0.8296(2) -0.1713(4) 0.2299(4) 0.130(6) Uani 0.5 1 d G U P A -1
C4 C 0.7798(3) -0.2192(3) 0.2221(3) 0.125(6) Uani 0.5 1 d G U P A -1
C5 C 0.7490(3) -0.2113(3) 0.1586(3) 0.126(6) Uani 0.5 1 d G U P A -1
C6 C 0.6877(3) -0.2030(3) 0.1409(3) 0.117(8) Uani 0.5 1 d G U P A -1
C7 C 0.6732(3) -0.1420(3) 0.1019(2) 0.121(9) Uani 0.5 1 d G U P A -1
C8 C 0.6937(3) -0.1059(4) 0.0751(2) 0.112(8) Uani 0.5 1 d G U P A -1
C9 C 0.7618(3) -0.1234(4) 0.0869(3) 0.114(8) Uani 0.5 1 d G U P A -1
C10 C 0.7895(3) -0.0527(5) 0.0766(3) 0.115(8) Uani 0.5 1 d G U P A -1
C11 C 0.8378(3) -0.0332(5) 0.1151(3) 0.132(8) Uani 0.5 1 d G U P A -1
C12 C 0.8627(2) -0.0789(5) 0.1678(4) 0.124(8) Uani 0.5 1 d G U P A -1
C13 C 0.87611(18) -0.0298(4) 0.2220(4) 0.129(8) Uani 0.5 1 d G U P A -1
C14 C 0.86431(16) -0.0600(4) 0.2799(3) 0.114(8) Uani 0.5 1 d G U P A -1
C15 C 0.8442(2) -0.1297(3) 0.2865(3) 0.126(8) Uani 0.5 1 d G U P A -1
C16 C 0.8221(2) -0.1454(3) 0.3355(3) 0.128(9) Uani 0.5 1 d G U P A -1
C17 C 0.7754(3) -0.1971(3) 0.3314(3) 0.130(9) Uani 0.5 1 d G U P A -1
C18 C 0.7472(3) -0.2393(3) 0.2680(3) 0.139(9) Uani 0.5 1 d G U P A -1
C19 C 0.6849(3) -0.2393(3) 0.2502(3) 0.133(9) Uani 0.5 1 d G U P A -1
C20 C 0.6545(3) -0.2160(3) 0.1888(3) 0.127(9) Uani 0.5 1 d G U P A -1
C21 C 0.6022(2) -0.1795(3) 0.2071(3) 0.121(9) Uani 0.5 1 d G U P A -1
C22 C 0.5841(2) -0.1126(3) 0.1559(3) 0.108(8) Uani 0.5 1 d G U P A -1
C23 C 0.6196(3) -0.0934(3) 0.1083(2) 0.116(8) Uani 0.5 1 d G U P A -1
C24 C 0.6172(3) -0.0161(4) 0.0900(2) 0.102(7) Uani 0.5 1 d G U P A -1
C25 C 0.6558(3) 0.0193(4) 0.06600(17) 0.104(7) Uani 0.5 1 d G U P A -1
C26 C 0.6975(3) -0.0320(4) 0.05548(17) 0.118(8) Uani 0.5 1 d G U P A -1
C27 C 0.7501(4) -0.0008(5) 0.0515(2) 0.136(7) Uani 0.5 1 d G U P A -1
C28 C 0.7572(4) 0.0771(5) 0.0640(2) 0.120(8) Uani 0.5 1 d G U P A -1
C29 C 0.8145(3) 0.0937(5) 0.1138(3) 0.131(8) Uani 0.5 1 d G U P A -1
C30 C 0.8466(3) 0.0452(5) 0.1344(4) 0.132(8) Uani 0.5 1 d G U P A -1
C31 C 0.8647(2) 0.0465(4) 0.2008(4) 0.144(8) Uani 0.5 1 d G U P A -1
C32 C 0.85651(18) 0.1045(4) 0.2437(4) 0.118(8) Uani 0.5 1 d G U P A -1
C33 C 0.84437(16) 0.0805(3) 0.3048(3) 0.125(8) Uani 0.5 1 d G U P A -1
C34 C 0.85324(16) -0.0084(4) 0.3207(3) 0.108(6) Uani 0.5 1 d G U P A -1
C35 C 0.8356(2) -0.0230(4) 0.3682(3) 0.0388(4) Uani 0.5 1 d G U P A -1
C36 C 0.8152(3) -0.0916(3) 0.3757(3) 0.100(7) Uani 0.5 1 d G U P A -1
C37 C 0.7808(3) -0.0868(4) 0.4087(2) 0.120(8) Uani 0.5 1 d G U P A -1
C38 C 0.7224(3) -0.1392(4) 0.3994(2) 0.118(8) Uani 0.5 1 d G U P A -1
C39 C 0.7295(3) -0.1918(3) 0.3614(3) 0.126(9) Uani 0.5 1 d G U P A -1
C40 C 0.6812(3) -0.2184(3) 0.3109(3) 0.131(9) Uani 0.5 1 d G U P A -1
C41 C 0.6346(3) -0.1844(3) 0.3171(3) 0.125(9) Uani 0.5 1 d G U P A -1
C42 C 0.5923(2) -0.1654(3) 0.2597(4) 0.106(8) Uani 0.5 1 d G U P A -1
C43 C 0.55244(19) -0.0952(4) 0.2481(4) 0.111(8) Uani 0.5 1 d G U P A -1
C44 C 0.55239(17) -0.0782(3) 0.1810(4) 0.102(8) Uani 0.5 1 d G U P A -1
C45 C 0.54982(16) 0.0151(4) 0.1624(3) 0.106(7) Uani 0.5 1 d G U P A -1
C46 C 0.5763(2) 0.0287(3) 0.1178(3) 0.099(8) Uani 0.5 1 d G U P A -1
C47 C 0.5833(2) 0.1101(3) 0.1156(3) 0.096(7) Uani 0.5 1 d G U P A -1
C48 C 0.6274(3) 0.1385(3) 0.1058(2) 0.101(8) Uani 0.5 1 d G U P A -1
C49 C 0.6580(3) 0.1004(4) 0.07437(19) 0.104(8) Uani 0.5 1 d G U P A -1
C50 C 0.7192(3) 0.1211(4) 0.0720(2) 0.110(8) Uani 0.5 1 d G U P A -1
C51 C 0.7345(3) 0.1766(4) 0.1139(3) 0.107(7) Uani 0.5 1 d G U P A -1
C52 C 0.7936(3) 0.1662(4) 0.1388(3) 0.117(8) Uani 0.5 1 d G U P A -1
C53 C 0.8242(2) 0.1596(4) 0.2044(3) 0.129(8) Uani 0.5 1 d G U P A -1
C54 C 0.7963(2) 0.2014(3) 0.2425(3) 0.111(8) Uani 0.5 1 d G U P A -1
C55 C 0.7954(2) 0.1945(3) 0.2987(3) 0.110(8) Uani 0.5 1 d G U P A -1
C56 C 0.8156(2) 0.1293(3) 0.3321(3) 0.119(8) Uani 0.5 1 d G U P A -1
C57 C 0.7930(3) 0.1154(3) 0.3843(2) 0.103(8) Uani 0.5 1 d G U P A -1
C58 C 0.8064(3) 0.0341(4) 0.3970(2) 0.087(6) Uani 0.5 1 d G U P A -1
C59 C 0.7724(3) -0.0153(4) 0.42630(17) 0.106(7) Uani 0.5 1 d G U P A -1
C60 C 0.7234(3) 0.0218(4) 0.43254(17) 0.117(8) Uani 0.5 1 d G U P A -1
C61 C 0.6735(3) -0.0296(4) 0.4235(2) 0.123(8) Uani 0.5 1 d G U P A -1
C62 C 0.6783(3) -0.1137(4) 0.4004(3) 0.140(9) Uani 0.5 1 d G U P A -1
C63 C 0.6198(3) -0.1301(4) 0.3524(3) 0.132(9) Uani 0.5 1 d G U P A -1
C64 C 0.5829(3) -0.0540(4) 0.3425(3) 0.135(9) Uani 0.5 1 d G U P A -1
C65 C 0.5523(2) -0.0591(4) 0.2792(4) 0.133(9) Uani 0.5 1 d G U P A -1
C66 C 0.54283(18) 0.0215(4) 0.2760(4) 0.130(8) Uani 0.5 1 d G U P A -1
C67 C 0.53579(14) 0.0417(4) 0.2112(4) 0.109(8) Uani 0.5 1 d G U P A -1
C68 C 0.56090(18) 0.1310(3) 0.2194(4) 0.109(8) Uani 0.5 1 d G U P A -1
C69 C 0.5758(2) 0.1525(3) 0.1686(3) 0.109(8) Uani 0.5 1 d G U P A -1
C70 C 0.6191(2) 0.2070(3) 0.1885(3) 0.100(7) Uani 0.5 1 d G U P A -1
C71 C 0.6445(3) 0.1960(3) 0.1429(3) 0.097(7) Uani 0.5 1 d G U P A -1
C72 C 0.7088(3) 0.2176(3) 0.1570(3) 0.092(7) Uani 0.5 1 d G U P A -1
C73 C 0.7346(3) 0.2371(3) 0.2118(3) 0.083(6) Uani 0.5 1 d G U P A -1
C74 C 0.7066(3) 0.2380(3) 0.2625(3) 0.099(7) Uani 0.5 1 d G U P A -1
C75 C 0.7423(3) 0.2128(3) 0.3177(3) 0.103(8) Uani 0.5 1 d G U P A -1
C76 C 0.7082(3) 0.1833(3) 0.3580(3) 0.126(8) Uani 0.5 1 d G U P A -1
C77 C 0.7491(3) 0.1368(4) 0.3994(2) 0.113(8) Uani 0.5 1 d G U P A -1
C78 C 0.7048(3) 0.0832(4) 0.4185(2) 0.106(8) Uani 0.5 1 d G U P A -1
C79 C 0.6480(3) 0.1060(4) 0.3940(3) 0.119(7) Uani 0.5 1 d G U P A -1
C80 C 0.6059(3) 0.0755(4) 0.3687(3) 0.117(8) Uani 0.5 1 d G U P A -1
C81 C 0.6158(3) 0.0081(5) 0.3892(3) 0.136(7) Uani 0.5 1 d G U P A -1
C82 C 0.5653(2) 0.0786(4) 0.3132(4) 0.120(8) Uani 0.5 1 d G U P A -1
C83 C 0.5764(2) 0.1477(4) 0.2824(4) 0.106(7) Uani 0.5 1 d G U P A -1
C84 C 0.6228(2) 0.1939(3) 0.2949(3) 0.105(7) Uani 0.5 1 d G U P A -1
C85 C 0.6494(2) 0.2265(3) 0.2411(3) 0.103(7) Uani 0.5 1 d G U P A -1
C86 C 0.6557(3) 0.1697(4) 0.3567(3) 0.103(7) Uani 0.5 1 d G U P A -1
C87 C 0.8541(6) 0.5127(13) 0.4176(7) 0.0388(4) Uani 0.25 1 d G U P B -2
H87 H 0.8357 0.5115 0.4502 0.047 Uiso 0.25 1 calc R U P B -2
C88 C 0.9121(6) 0.5102(14) 0.4285(6) 0.0388(4) Uani 0.25 1 d G U P B -2
H88 H 0.9326 0.5074 0.4685 0.047 Uiso 0.25 1 calc R U P B -2
C89 C 0.9396(4) 0.5120(13) 0.3797(8) 0.0388(4) Uani 0.25 1 d G U P B -2
H89 H 0.9784 0.5103 0.3871 0.047 Uiso 0.25 1 calc R U P B -2
C90 C 0.9090(6) 0.5162(12) 0.3200(7) 0.0388(4) Uani 0.25 1 d G U P B -2
H90 H 0.9274 0.5174 0.2874 0.047 Uiso 0.25 1 calc R U P B -2
C91 C 0.8510(6) 0.5187(11) 0.3091(6) 0.0388(4) Uani 0.25 1 d G U P B -2
H91 H 0.8305 0.5215 0.2691 0.047 Uiso 0.25 1 calc R U P B -2
C92 C 0.8235(4) 0.5169(12) 0.3578(8) 0.0388(4) Uani 0.25 1 d G U P B -2
H92 H 0.7847 0.5186 0.3505 0.047 Uiso 0.25 1 calc R U P B -2
Ni1 Ni 0.95446(6) 0.0000 0.42903(8) 0.0388(4) Uani 1 2 d S T P C 2
C93 C 0.8992(3) 0.0614(5) 0.5271(4) 0.0388(4) Uani 1 1 d . U . C 2
C94 C 0.9309(3) 0.1549(5) 0.4669(4) 0.0388(4) Uani 1 1 d . U . C 2
C95 C 0.9724(3) 0.1545(5) 0.3871(4) 0.0388(4) Uani 1 1 d . U . C 2
C96 C 1.0069(3) 0.0611(5) 0.3279(4) 0.0388(4) Uani 1 1 d . U . C 2
N3 N 0.9920(4) 0.0000 0.3584(5) 0.0388(4) Uani 1 2 d S T P C 2
N1 N 0.9168(4) 0.0000 0.4978(5) 0.0388(4) Uani 1 2 d S T P C 2
C97 C 0.7871(3) 0.1190(5) 0.5795(4) 0.0388(4) Uani 1 1 d . U . C 2
H97A H 0.7901 0.1431 0.5419 0.058 Uiso 1 1 calc R U . C 2
H97B H 0.7729 0.1534 0.6054 0.058 Uiso 1 1 calc R U . C 2
H97C H 0.7622 0.0775 0.5707 0.058 Uiso 1 1 calc R U . C 2
N2 N 0.9536(3) 0.1080(5) 0.4272(3) 0.049(2) Uani 1 1 d . . . C 2
C98 C 0.8447(4) 0.0919(7) 0.6121(5) 0.059(3) Uani 1 1 d . U . C 2
H98A H 0.8693 0.1342 0.6221 0.071 Uiso 1 1 calc R U . C 2
H98B H 0.8414 0.0680 0.6502 0.071 Uiso 1 1 calc R U . C 2
C99 C 0.9070(3) 0.1327(6) 0.5125(5) 0.051(2) Uani 1 1 d . U . C 2
H99 H 0.8947 0.1692 0.5360 0.061 Uiso 1 1 calc R U . C 2
C100 C 0.9376(4) 0.2304(6) 0.4488(5) 0.058(3) Uani 1 1 d . U . C 2
C101 C 0.9156(4) 0.2958(6) 0.4803(6) 0.068(3) Uani 1 1 d . U . C 2
H10A H 0.9354 0.3402 0.4727 0.081 Uiso 1 1 calc R U . C 2
H10B H 0.9237 0.2871 0.5242 0.081 Uiso 1 1 calc R U . C 2
C102 C 0.8523(5) 0.3092(7) 0.4590(6) 0.080(4) Uani 1 1 d . U . C 2
H10C H 0.8440 0.3202 0.4160 0.120 Uiso 1 1 calc R U . C 2
H10D H 0.8412 0.3502 0.4813 0.120 Uiso 1 1 calc R U . C 2
H10E H 0.8322 0.2655 0.4665 0.120 Uiso 1 1 calc R U . C 2
C103 C 0.9632(4) 0.2309(6) 0.4008(6) 0.063(3) Uani 1 1 d . U . C 2
C104 C 0.9774(5) 0.2946(7) 0.3620(6) 0.079(4) Uani 1 1 d . U . C 2
H10F H 1.0140 0.2856 0.3529 0.095 Uiso 1 1 calc R U . C 2
H10G H 0.9796 0.3400 0.3857 0.095 Uiso 1 1 calc R U . C 2
C105 C 0.9355(5) 0.3055(7) 0.3020(6) 0.083(4) Uani 1 1 d . U . C 2
H10H H 0.9451 0.3492 0.2818 0.125 Uiso 1 1 calc R U . C 2
H10I H 0.8987 0.3112 0.3103 0.125 Uiso 1 1 calc R U . C 2
H10J H 0.9363 0.2632 0.2761 0.125 Uiso 1 1 calc R U . C 2
C106 C 0.9995(4) 0.1332(7) 0.3400(5) 0.061(3) Uani 1 1 d . U . C 2
H106 H 1.0125 0.1695 0.3167 0.073 Uiso 1 1 calc R U . C 2
C107 C 1.0559(5) 0.0930(8) 0.2387(5) 0.079(4) Uani 1 1 d . U . C 2
H10K H 1.0825 0.0680 0.2187 0.094 Uiso 1 1 calc R U . C 2
H10L H 1.0758 0.1318 0.2643 0.094 Uiso 1 1 calc R U . C 2
C108 C 1.0343(4) 0.0381(7) 0.2790(5) 0.063(3) Uani 1 1 d . U . C 2
C109 C 1.0095(6) 0.1295(11) 0.1884(6) 0.114(6) Uani 1 1 d . U . C 2
H10M H 1.0267 0.1590 0.1615 0.171 Uiso 1 1 calc R U . C 2
H10N H 0.9861 0.1604 0.2076 0.171 Uiso 1 1 calc R U . C 2
H10O H 0.9872 0.0914 0.1651 0.171 Uiso 1 1 calc R U . C 2
C110 C 0.8706(4) 0.0377(5) 0.5738(5) 0.050(2) Uani 1 1 d . U . C 2
Ni2 Ni 0.5000 0.0000 0.0000 0.0684(9) Uani 1 4 d S T P D 3
C126 C 0.5000 0.1889(12) 0.0000 0.088(6) Uani 1 2 d S TU P D 3
H126 H 0.5000 0.2404 0.0000 0.105 Uiso 1 2 calc R U P D 3
C127 C 0.4651(6) 0.1530(7) 0.0311(6) 0.078(4) Uani 1 1 d . U . D 3
C128 C 0.3744(9) 0.2986(9) 0.0083(8) 0.136(7) Uani 1 1 d . U . D 3
H12A H 0.3897 0.2967 -0.0281 0.203 Uiso 1 1 calc R U . D 3
H12B H 0.3633 0.3485 0.0149 0.203 Uiso 1 1 calc R U . D 3
H12C H 0.3424 0.2665 0.0035 0.203 Uiso 1 1 calc R U . D 3
C129 C 0.4181(8) 0.2732(8) 0.0628(7) 0.103(5) Uani 1 1 d . U . D 3
H12D H 0.4531 0.2983 0.0619 0.124 Uiso 1 1 calc R U . D 3
H12E H 0.4065 0.2878 0.1001 0.124 Uiso 1 1 calc R U . D 3
C130 C 0.4280(7) 0.1906(8) 0.0642(6) 0.092(4) Uani 1 1 d . U . D 3
C131 C 0.3013(7) 0.1338(10) 0.0979(8) 0.117(6) Uani 1 1 d . U . D 3
H13A H 0.2935 0.1680 0.0642 0.176 Uiso 1 1 calc R U . D 3
H13B H 0.2756 0.1419 0.1244 0.176 Uiso 1 1 calc R U . D 3
H13C H 0.2976 0.0840 0.0826 0.176 Uiso 1 1 calc R U . D 3
C132 C 0.3613(7) 0.1462(9) 0.1338(8) 0.109(5) Uani 1 1 d . U . D 3
H13D H 0.3645 0.1953 0.1518 0.131 Uiso 1 1 calc R U . D 3
H13E H 0.3700 0.1102 0.1667 0.131 Uiso 1 1 calc R U . D 3
C133 C 0.4020(7) 0.1381(8) 0.0919(7) 0.093(4) Uani 1 1 d . U . D 3
C134 C 0.4227(6) 0.0676(8) 0.0745(6) 0.082(4) Uani 1 1 d . U . D 3
C135 C 0.4072(8) 0.0000 0.0919(9) 0.080(5) Uani 1 2 d S TU P D 3
H135 H 0.3830 0.0000 0.1192 0.096 Uiso 1 2 calc R U P D 3
N6 N 0.4612(4) 0.0773(6) 0.0364(4) 0.072(3) Uani 1 1 d . . . D 3
C1E C 0.7127(7) 0.4812(9) 0.2321(7) 0.0388(4) Uani 0.25 1 d G U P E -5
H1E H 0.7277 0.4686 0.2725 0.047 Uiso 0.25 1 calc R U P E -5
C3E C 0.7149(7) 0.5542(8) 0.2128(8) 0.0388(4) Uani 0.25 1 d G U P E -5
H3E H 0.7314 0.5904 0.2403 0.047 Uiso 0.25 1 calc R U P E -5
C2E C 0.6926(8) 0.5731(8) 0.1523(9) 0.0388(4) Uani 0.25 1 d G U P E -5
H2E H 0.6941 0.6219 0.1394 0.047 Uiso 0.25 1 calc R U P E -5
C4E C 0.6680(7) 0.5190(9) 0.1112(7) 0.0388(4) Uani 0.25 1 d G U P E -5
H4E H 0.6531 0.5316 0.0707 0.047 Uiso 0.25 1 calc R U P E -5
C5E C 0.6658(7) 0.4459(8) 0.1305(8) 0.0388(4) Uani 0.25 1 d G U P E -5
H5E H 0.6494 0.4097 0.1029 0.047 Uiso 0.25 1 calc R U P E -5
C6E C 0.6882(8) 0.4271(8) 0.1909(9) 0.0388(4) Uani 0.25 1 d G U P E -5
H6E H 0.6867 0.3782 0.2038 0.047 Uiso 0.25 1 calc R U P E -5


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu8 0.96(3) . ?
Lu1 Lu3 1.471(3) . ?
Lu1 Lu7 1.819(15) . ?
Lu1 C68 2.207(4) . ?
Lu1 C69 2.258(4) . ?
Lu1 C70 2.478(5) . ?
Lu1 Lu5 2.550(17) . ?
Lu1 C47 2.575(5) . ?
Lu1 C83 2.634(5) . ?
Lu1 C45 2.635(5) . ?
Lu1 C67 2.654(5) . ?
Lu1 C46 2.692(5) . ?
Lu2 Lu5 0.972(19) . ?
Lu2 Lu2 1.521(5) 6 ?
Lu2 Lu4 1.788(7) . ?
Lu2 C58 2.299(4) . ?
Lu2 C57 2.320(5) . ?
Lu2 C78 2.335(5) . ?
Lu2 C77 2.362(5) . ?
Lu2 Lu5 2.385(19) 6 ?
Lu2 C60 2.414(5) . ?
Lu2 C59 2.533(5) . ?
Lu2 Lu7 2.66(2) . ?
Lu2 C76 2.696(5) . ?
Lu3 Lu7 0.81(2) . ?
Lu3 Lu1 1.471(3) 6 ?
Lu3 Lu8 2.17(4) 6 ?
Lu3 Lu8 2.17(4) . ?
Lu3 C45 2.197(5) . ?
Lu3 C67 2.327(5) . ?
Lu3 C44 2.403(5) . ?
Lu3 C66 2.522(7) . ?
Lu3 C65 2.560(7) . ?
Lu3 C43 2.608(6) . ?
Lu3 C46 2.621(7) . ?
Lu4 Lu5 0.97(2) . ?
Lu4 C56 1.793(6) . ?
Lu4 C55 1.996(7) . ?
Lu4 C33 2.138(7) . ?
Lu4 Lu6 2.267(18) . ?
Lu4 C54 2.301(8) . ?
Lu4 C75 2.318(8) . ?
Lu4 Lu8 2.39(3) . ?
Lu4 C57 2.407(7) . ?
Lu4 C32 2.697(8) . ?
Lu4 C53 2.766(9) . ?
Lu5 C57 2.153(16) . ?
Lu5 C56 2.164(18) . ?
Lu5 C76 2.26(2) . ?
Lu5 C77 2.273(18) . ?
Lu5 C75 2.307(18) . ?
Lu5 Lu2 2.385(19) 6 ?
Lu5 Lu8 2.46(3) . ?
Lu5 C55 2.514(18) . ?
Lu5 C58 2.65(2) . ?
Lu6 Lu4 2.267(19) 6 ?
Lu6 C31 2.30(2) . ?
Lu6 C14 2.306(17) . ?
Lu6 C13 2.308(18) . ?
Lu6 C34 2.38(3) . ?
Lu6 C33 2.47(2) . ?
Lu6 C32 2.538(12) . ?
Lu6 Lu5 2.82(3) 6 ?
Lu6 C12 2.90(2) . ?
Lu6 C15 2.912(14) . ?
Lu7 Lu1 1.819(15) 6 ?
Lu7 C66 2.08(2) . ?
Lu7 C65 2.123(19) . ?
Lu7 C67 2.36(2) . ?
Lu7 C64 2.37(2) . ?
Lu7 C82 2.412(19) . ?
Lu7 C43 2.421(15) . ?
Lu7 C45 2.63(2) . ?
Lu7 Lu8 2.63(4) 6 ?
Lu7 Lu8 2.63(4) . ?
Lu8 C71 2.28(3) . ?
Lu8 C48 2.33(3) . ?
Lu8 C70 2.41(3) . ?
Lu8 C69 2.54(3) . ?
Lu8 C47 2.59(3) . ?
Lu8 C85 2.66(3) . ?
Lu8 C72 2.68(4) . ?
C1 C9 1.1758 . ?
C1 C5 1.4684 . ?
C1 C2 1.4726 . ?
C2 C12 1.3757 . ?
C2 C3 1.4766 . ?
C3 C15 1.4486 . ?
C3 C4 1.4740 . ?
C4 C18 1.4655 . ?
C4 C5 1.4707 . ?
C5 C6 1.4776 . ?
C6 C7 1.4009 . ?
C6 C20 1.4870 . ?
C7 C8 1.0768 . ?
C7 C23 1.6065 . ?
C8 C26 1.4106 . ?
C8 C9 1.6624 . ?
C9 C10 1.4837 . ?
C10 C11 1.3587 . ?
C10 C27 1.3783 . ?
C11 C12 1.4610 . ?
C11 C30 1.4810 . ?
C12 C13 1.4805 . ?
C13 C31 1.4641 . ?
C13 C14 1.4830 . ?
C14 C34 1.3666 . ?
C14 C15 1.3697 . ?
C15 C16 1.3437 . ?
C16 C36 1.3545 . ?
C16 C17 1.4639 . ?
C17 C39 1.4239 . ?
C17 C18 1.6293 . ?
C18 C19 1.4945 . ?
C19 C40 1.4271 . ?
C19 C20 1.4790 . ?
C20 C21 1.5648 . ?
C21 C42 1.2702 . ?
C21 C22 1.6578 . ?
C22 C44 1.2144 . ?
C22 C23 1.5412 . ?
C23 C24 1.4506 . ?
C24 C25 1.3384 . ?
C24 C46 1.5134 . ?
C25 C26 1.4319 . ?
C25 C49 1.4745 . ?
C26 C27 1.4228 . ?
C27 C28 1.4355 . ?
C28 C50 1.2623 . ?
C28 C29 1.6300 . ?
C29 C30 1.2011 . ?
C29 C52 1.5486 . ?
C30 C31 1.4571 . ?
C31 C32 1.4586 . ?
C32 C53 1.4486 . ?
C32 C33 1.5170 . ?
C33 C56 1.3459 . ?
C33 C34 1.6476 . ?
C34 C35 1.2524 . ?
C35 C36 1.3569 . ?
C35 C58 1.4732 . ?
C36 C37 1.2282 . ?
C37 C59 1.3760 . ?
C37 C38 1.6887 . ?
C38 C62 1.1764 . ?
C38 C39 1.3066 . ?
C39 C40 1.5324 . ?
C40 C41 1.3255 . ?
C41 C63 1.3524 . ?
C41 C42 1.5124 . ?
C42 C43 1.5865 . ?
C43 C65 0.9526 . ?
C43 C44 1.5286 . ?
C44 C45 1.7328 . ?
C45 C67 1.2978 . ?
C45 C46 1.3163 . ?
C46 C47 1.4796 . ?
C47 C48 1.2531 . ?
C47 C69 1.4499 . ?
C48 C49 1.3184 . ?
C48 C71 1.3396 . ?
C49 C50 1.5531 . ?
C50 C51 1.3691 . ?
C51 C52 1.4507 . ?
C51 C72 1.4535 . ?
C52 C53 1.5055 . ?
C53 C54 1.4122 . ?
C54 C55 1.2633 . ?
C54 C73 1.6553 . ?
C55 C56 1.4250 . ?
C55 C75 1.4848 . ?
C56 C57 1.4090 . ?
C57 C77 1.2499 . ?
C57 C58 1.5166 . ?
C58 C59 1.4618 . ?
C59 C60 1.4030 . ?
C60 C78 1.2133 . ?
C60 C61 1.5122 . ?
C61 C81 1.6136 . ?
C61 C62 1.6147 . ?
C62 C63 1.6296 . ?
C63 C64 1.6337 . ?
C64 C65 1.4588 . ?
C64 C81 1.6260 . ?
C65 C66 1.4726 . ?
C66 C82 1.3656 . ?
C66 C67 1.4662 . ?
C67 C68 1.7198 . ?
C68 C69 1.3179 . ?
C68 C83 1.4112 . ?
C69 C70 1.4473 . ?
C69 C71 2.0400 . ?
C70 C85 1.3008 . ?
C70 C71 1.3104 . ?
C71 C72 1.5869 . ?
C72 C73 1.3033 . ?
C73 C74 1.4370 . ?
C74 C85 1.3984 . ?
C74 C75 1.4306 . ?
C75 C76 1.4466 . ?
C76 C86 1.2998 . ?
C76 C77 1.4768 . ?
C77 C78 1.5746 . ?
C78 C79 1.4454 . ?
C79 C80 1.2016 . ?
C79 C86 1.4535 . ?
C79 C81 1.9272 . ?
C80 C81 1.3038 . ?
C80 C82 1.4219 . ?
C82 C83 1.4746 . ?
C83 C84 1.3879 . ?
C84 C86 1.5124 . ?
C84 C85 1.5902 . ?
C87 C88 1.3900 . ?
C87 C92 1.3900 . ?
C88 C89 1.3900 . ?
C89 C90 1.3900 . ?
C90 C91 1.3900 . ?
C91 C92 1.3900 . ?
Ni1 N1 1.945(11) . ?
Ni1 N2 1.948(8) 6 ?
Ni1 N2 1.949(8) . ?
Ni1 N3 1.978(11) . ?
C93 C99 1.349(13) . ?
C93 N1 1.398(10) . ?
C93 C110 1.431(13) . ?
C94 C99 1.333(13) . ?
C94 N2 1.417(12) . ?
C94 C100 1.439(14) . ?
C95 N2 1.372(12) . ?
C95 C106 1.405(14) . ?
C95 C103 1.439(14) . ?
C96 C106 1.347(14) . ?
C96 N3 1.382(11) . ?
C96 C108 1.453(13) . ?
N3 C96 1.382(11) 6 ?
N1 C93 1.398(10) 6 ?
C97 C98 1.527(12) . ?
C98 C110 1.520(14) . ?
C100 C103 1.345(15) . ?
C100 C101 1.527(16) . ?
C101 C102 1.543(14) . ?
C103 C104 1.521(15) . ?
C104 C105 1.523(15) . ?
C107 C108 1.504(16) . ?
C107 C109 1.569(18) . ?
C108 C108 1.38(2) 6 ?
C110 C110 1.36(2) 6 ?
Ni2 N6 1.953(11) . ?
Ni2 N6 1.953(11) 6 ?
Ni2 N6 1.953(11) 2_655 ?
Ni2 N6 1.953(11) 5_655 ?
C126 C127 1.367(16) . ?
C126 C127 1.367(16) 2_655 ?
C127 N6 1.376(16) . ?
C127 C130 1.45(2) . ?
C128 C129 1.52(2) . ?
C129 C130 1.51(2) . ?
C130 C133 1.36(2) . ?
C131 C132 1.54(2) . ?
C132 C133 1.51(2) . ?
C133 C134 1.451(19) . ?
C134 C135 1.356(17) . ?
C134 N6 1.403(17) . ?
C135 C134 1.356(17) 6 ?
C1E C3E 1.3900 . ?
C1E C6E 1.3900 . ?
C3E C2E 1.3900 . ?
C2E C4E 1.3900 . ?
C4E C5E 1.3900 . ?
C5E C6E 1.3900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu8 Lu1 Lu3 124(2) . . ?
Lu8 Lu1 Lu7 140.4(17) . . ?
Lu3 Lu1 Lu7 25.6(5) . . ?
Lu8 Lu1 C68 128.0(16) . . ?
Lu3 Lu1 C68 99.9(3) . . ?
Lu7 Lu1 C68 91.2(6) . . ?
Lu8 Lu1 C69 96.0(15) . . ?
Lu3 Lu1 C69 117.9(2) . . ?
Lu7 Lu1 C69 120.4(7) . . ?
C68 Lu1 C69 34.31(6) . . ?
Lu8 Lu1 C70 74.5(17) . . ?
Lu3 Lu1 C70 152.7(2) . . ?
Lu7 Lu1 C70 144.8(6) . . ?
C68 Lu1 C70 55.29(10) . . ?
C69 Lu1 C70 35.20(7) . . ?
Lu8 Lu1 Lu5 73.6(18) . . ?
Lu3 Lu1 Lu5 99.3(5) . . ?
Lu7 Lu1 Lu5 86.3(8) . . ?
C68 Lu1 Lu5 128.7(5) . . ?
C69 Lu1 Lu5 139.5(5) . . ?
C70 Lu1 Lu5 105.5(4) . . ?
Lu8 Lu1 C47 80.3(17) . . ?
Lu3 Lu1 C47 103.3(3) . . ?
Lu7 Lu1 C47 120.6(7) . . ?
C68 Lu1 C47 62.85(10) . . ?
C69 Lu1 C47 34.12(6) . . ?
C70 Lu1 C47 57.33(10) . . ?
Lu5 Lu1 C47 152.2(5) . . ?
Lu8 Lu1 C83 134(2) . . ?
Lu3 Lu1 C83 101.3(3) . . ?
Lu7 Lu1 C83 81.1(6) . . ?
C68 Lu1 C83 32.39(7) . . ?
C69 Lu1 C83 61.91(11) . . ?
C70 Lu1 C83 64.75(11) . . ?
Lu5 Lu1 C83 97.1(5) . . ?
C47 Lu1 C83 94.25(13) . . ?
Lu8 Lu1 C45 122(2) . . ?
Lu3 Lu1 C45 56.5(2) . . ?
Lu7 Lu1 C45 69.6(7) . . ?
C68 Lu1 C45 59.53(10) . . ?
C69 Lu1 C45 62.40(10) . . ?
C70 Lu1 C45 97.51(13) . . ?
Lu5 Lu1 C45 155.3(5) . . ?
C47 Lu1 C45 51.04(8) . . ?
C83 Lu1 C45 84.69(13) . . ?
Lu8 Lu1 C67 147.1(18) . . ?
Lu3 Lu1 C67 61.0(2) . . ?
Lu7 Lu1 C67 60.4(7) . . ?
C68 Lu1 C67 40.13(8) . . ?
C69 Lu1 C67 60.47(9) . . ?
C70 Lu1 C67 92.33(12) . . ?
Lu5 Lu1 C67 139.3(5) . . ?
C47 Lu1 C67 67.40(10) . . ?
C83 Lu1 C67 57.75(10) . . ?
C45 Lu1 C67 28.4 . . ?
Lu8 Lu1 C46 94(2) . . ?
Lu3 Lu1 C46 71.3(2) . . ?
Lu7 Lu1 C46 91.9(7) . . ?
C68 Lu1 C46 74.94(11) . . ?
C69 Lu1 C46 60.06(10) . . ?
C70 Lu1 C46 89.44(14) . . ?
Lu5 Lu1 C46 156.3(5) . . ?
C47 Lu1 C46 32.54(6) . . ?
C83 Lu1 C46 105.97(13) . . ?
C45 Lu1 C46 28.6 . . ?
C67 Lu1 C46 55.61(9) . . ?
Lu5 Lu2 Lu2 145.4(13) . 6 ?
Lu5 Lu2 Lu4 22.8(14) . . ?
Lu2 Lu2 Lu4 124.4(2) 6 . ?
Lu5 Lu2 C58 99.9(11) . . ?
Lu2 Lu2 C58 86.39(18) 6 . ?
Lu4 Lu2 C58 91.6(3) . . ?
Lu5 Lu2 C57 68.0(9) . . ?
Lu2 Lu2 C57 124.72(17) 6 . ?
Lu4 Lu2 C57 70.4(3) . . ?
C58 Lu2 C57 38.33(7) . . ?
Lu5 Lu2 C78 105.9(12) . . ?
Lu2 Lu2 C78 108.5(2) 6 . ?
Lu4 Lu2 C78 124.0(3) . . ?
C58 Lu2 C78 73.37(12) . . ?
C57 Lu2 C78 64.90(11) . . ?
Lu5 Lu2 C77 72.8(10) . . ?
Lu2 Lu2 C77 136.32(18) 6 . ?
Lu4 Lu2 C77 86.3(3) . . ?
C58 Lu2 C77 59.97(10) . . ?
C57 Lu2 C77 30.95(6) . . ?
C78 Lu2 C77 39.17(7) . . ?
Lu5 Lu2 Lu5 132.1(18) . 6 ?
Lu2 Lu2 Lu5 13.4(5) 6 6 ?
Lu4 Lu2 Lu5 111.3(6) . 6 ?
C58 Lu2 Lu5 89.3(5) . 6 ?
C57 Lu2 Lu5 126.3(5) . 6 ?
C78 Lu2 Lu5 121.7(5) . 6 ?
C77 Lu2 Lu5 145.7(4) . 6 ?
Lu5 Lu2 C60 131.2(11) . . ?
Lu2 Lu2 C60 81.26(19) 6 . ?
Lu4 Lu2 C60 141.7(3) . . ?
C58 Lu2 C60 59.32(10) . . ?
C57 Lu2 C60 71.47(11) . . ?
C78 Lu2 C60 29.54(6) . . ?
C77 Lu2 C60 58.44(10) . . ?
Lu5 Lu2 C60 94.0(5) 6 . ?
Lu5 Lu2 C59 132.8(10) . . ?
Lu2 Lu2 C59 65.84(16) 6 . ?
Lu4 Lu2 C59 126.3(3) . . ?
C58 Lu2 C59 34.79(6) . . ?
C57 Lu2 C59 65.30(10) . . ?
C78 Lu2 C59 59.12(10) . . ?
C77 Lu2 C59 70.90(11) . . ?
Lu5 Lu2 C59 75.0(4) 6 . ?
C60 Lu2 C59 32.84(6) . . ?
Lu5 Lu2 Lu7 103.2(11) . . ?
Lu2 Lu2 Lu7 73.40(14) 6 . ?
Lu4 Lu2 Lu7 109.1(5) . . ?
C58 Lu2 Lu7 156.8(4) . . ?
C57 Lu2 Lu7 159.4(3) . . ?
C78 Lu2 Lu7 101.9(5) . . ?
C77 Lu2 Lu7 129.7(4) . . ?
Lu5 Lu2 Lu7 73.7(5) 6 . ?
C60 Lu2 Lu7 105.3(6) . . ?
C59 Lu2 Lu7 123.1(4) . . ?
Lu5 Lu2 C76 53.7(13) . . ?
Lu2 Lu2 C76 160.79(16) 6 . ?
Lu4 Lu2 C76 74.7(3) . . ?
C58 Lu2 C76 91.68(16) . . ?
C57 Lu2 C76 55.98(12) . . ?
C78 Lu2 C76 52.94(10) . . ?
C77 Lu2 C76 33.12(7) . . ?
Lu5 Lu2 C76 173.8(6) 6 . ?
C60 Lu2 C76 81.34(13) . . ?
C59 Lu2 C76 102.53(14) . . ?
Lu7 Lu2 C76 103.6(3) . . ?
Lu7 Lu3 Lu1 102.1(4) . 6 ?
Lu7 Lu3 Lu1 102.1(4) . . ?
Lu1 Lu3 Lu1 144.9(4) 6 . ?
Lu7 Lu3 Lu8 117.2(12) . 6 ?
Lu1 Lu3 Lu8 21.5(9) 6 6 ?
Lu1 Lu3 Lu8 123.4(9) . 6 ?
Lu7 Lu3 Lu8 117.2(12) . . ?
Lu1 Lu3 Lu8 123.4(9) 6 . ?
Lu1 Lu3 Lu8 21.5(9) . . ?
Lu8 Lu3 Lu8 101.9(17) 6 . ?
Lu7 Lu3 C45 114.0(17) . . ?
Lu1 Lu3 C45 103.3(3) 6 . ?
Lu1 Lu3 C45 89.6(2) . . ?
Lu8 Lu3 C45 107.6(8) 6 . ?
Lu8 Lu3 C45 96.3(7) . . ?
Lu7 Lu3 C67 82.7(16) . . ?
Lu1 Lu3 C67 122.6(3) 6 . ?
Lu1 Lu3 C67 85.5(2) . . ?
Lu8 Lu3 C67 135.7(7) 6 . ?
Lu8 Lu3 C67 102.3(7) . . ?
C45 Lu3 C67 33.18(7) . . ?
Lu7 Lu3 C44 102.1(13) . . ?
Lu1 Lu3 C44 64.27(19) 6 . ?
Lu1 Lu3 C44 133.3(3) . . ?
Lu8 Lu3 C44 77.7(7) 6 . ?
Lu8 Lu3 C44 134.4(9) . . ?
C45 Lu3 C44 43.97(10) . . ?
C67 Lu3 C44 58.90(12) . . ?
Lu7 Lu3 C66 48.3(16) . . ?
Lu1 Lu3 C66 116.4(3) 6 . ?
Lu1 Lu3 C66 98.7(3) . . ?
Lu8 Lu3 C66 137.7(8) 6 . ?
Lu8 Lu3 C66 120.1(8) . . ?
C45 Lu3 C66 65.75(14) . . ?
C67 Lu3 C66 34.90(9) . . ?
C44 Lu3 C66 69.98(15) . . ?
Lu7 Lu3 C65 49.1(14) . . ?
Lu1 Lu3 C65 82.9(2) 6 . ?
Lu1 Lu3 C65 132.2(3) . . ?
Lu8 Lu3 C65 104.4(9) 6 . ?
Lu8 Lu3 C65 153.7(9) . . ?
C45 Lu3 C65 75.30(16) . . ?
C67 Lu3 C65 57.27(14) . . ?
C44 Lu3 C65 53.01(12) . . ?
C66 Lu3 C65 33.67(9) . . ?
Lu7 Lu3 C43 67.8(12) . . ?
Lu1 Lu3 C43 65.9(2) 6 . ?
Lu1 Lu3 C43 148.0(3) . . ?
Lu8 Lu3 C43 86.7(8) 6 . ?
Lu8 Lu3 C43 165.1(7) . . ?
C45 Lu3 C43 69.29(14) . . ?
C67 Lu3 C43 63.56(14) . . ?
C44 Lu3 C43 35.22(8) . . ?
C66 Lu3 C43 51.30(12) . . ?
C65 Lu3 C43 21.2 . . ?
Lu7 Lu3 C46 142.8(16) . . ?
Lu1 Lu3 C46 98.3(3) 6 . ?
Lu1 Lu3 C46 76.6(2) . . ?
Lu8 Lu3 C46 92.1(9) 6 . ?
Lu8 Lu3 C46 74.3(8) . . ?
C45 Lu3 C46 30.10(9) . . ?
C67 Lu3 C46 60.18(13) . . ?
C44 Lu3 C46 60.22(14) . . ?
C66 Lu3 C46 94.70(17) . . ?
C65 Lu3 C46 104.09(18) . . ?
C43 Lu3 C46 93.42(17) . . ?
Lu5 Lu4 Lu2 22.9(13) . . ?
Lu5 Lu4 C56 98.8(11) . . ?
Lu2 Lu4 C56 98.5(4) . . ?
Lu5 Lu4 C55 111.2(11) . . ?
Lu2 Lu4 C55 126.0(4) . . ?
C56 Lu4 C55 43.79(15) . . ?
Lu5 Lu4 C33 120.2(13) . . ?
Lu2 Lu4 C33 106.1(3) . . ?
C56 Lu4 C33 38.80(13) . . ?
C55 Lu4 C33 69.8(2) . . ?
Lu5 Lu4 Lu6 115.6(14) . . ?
Lu2 Lu4 Lu6 94.2(6) . . ?
C56 Lu4 Lu6 106.7(6) . . ?
C55 Lu4 Lu6 128.1(5) . . ?
C33 Lu4 Lu6 68.3(5) . . ?
Lu5 Lu4 C54 138.2(13) . . ?
Lu2 Lu4 C54 158.2(4) . . ?
C56 Lu4 C54 68.8(2) . . ?
C55 Lu4 C54 33.24(13) . . ?
C33 Lu4 C54 75.5(2) . . ?
Lu6 Lu4 C54 106.2(6) . . ?
Lu5 Lu4 C75 77.3(12) . . ?
Lu2 Lu4 C75 98.1(4) . . ?
C56 Lu4 C75 67.1(2) . . ?
C55 Lu4 C75 39.39(14) . . ?
C33 Lu4 C75 103.8(3) . . ?
Lu6 Lu4 C75 166.9(6) . . ?
C54 Lu4 C75 61.0(2) . . ?
Lu5 Lu4 Lu8 82.6(14) . . ?
Lu2 Lu4 Lu8 89.0(9) . . ?
C56 Lu4 Lu8 163.8(9) . . ?
C55 Lu4 Lu8 120.6(9) . . ?
C33 Lu4 Lu8 151.4(9) . . ?
Lu6 Lu4 Lu8 86.9(10) . . ?
C54 Lu4 Lu8 99.4(9) . . ?
C75 Lu4 Lu8 97.7(8) . . ?
Lu5 Lu4 C57 63.3(10) . . ?
Lu2 Lu4 C57 65.2(3) . . ?
C56 Lu4 C57 35.54(14) . . ?
C55 Lu4 C57 65.07(18) . . ?
C33 Lu4 C57 65.02(17) . . ?
Lu6 Lu4 C57 119.4(7) . . ?
C54 Lu4 C57 97.4(2) . . ?
C75 Lu4 C57 62.88(19) . . ?
Lu8 Lu4 C57 143.1(9) . . ?
Lu5 Lu4 C32 154.3(14) . . ?
Lu2 Lu4 C32 136.8(3) . . ?
C56 Lu4 C32 61.6(2) . . ?
C55 Lu4 C32 67.4(2) . . ?
C33 Lu4 C32 34.16(12) . . ?
Lu6 Lu4 C32 60.8(5) . . ?
C54 Lu4 C32 53.63(17) . . ?
C75 Lu4 C32 106.6(3) . . ?
Lu8 Lu4 C32 121.1(9) . . ?
C57 Lu4 C32 95.3(2) . . ?
Lu5 Lu4 C53 168.9(13) . . ?
Lu2 Lu4 C53 167.0(4) . . ?
C56 Lu4 C53 77.4(3) . . ?
C55 Lu4 C53 58.8(2) . . ?
C33 Lu4 C53 63.0(2) . . ?
Lu6 Lu4 C53 75.5(6) . . ?
C54 Lu4 C53 30.64(11) . . ?
C75 Lu4 C53 91.6(3) . . ?
Lu8 Lu4 C53 98.2(9) . . ?
C57 Lu4 C53 112.6(2) . . ?
C32 Lu4 C53 30.72(9) . . ?
Lu4 Lu5 Lu2 134(3) . . ?
Lu4 Lu5 C57 93.0(12) . . ?
Lu2 Lu5 C57 87.3(12) . . ?
Lu4 Lu5 C56 55.0(9) . . ?
Lu2 Lu5 C56 114.2(15) . . ?
C57 Lu5 C56 38.1(3) . . ?
Lu4 Lu5 C76 115.4(14) . . ?
Lu2 Lu5 C76 106.0(16) . . ?
C57 Lu5 C76 65.1(5) . . ?
C56 Lu5 C76 84.2(5) . . ?
Lu4 Lu5 C77 118.8(12) . . ?
Lu2 Lu5 C77 83.1(12) . . ?
C57 Lu5 C77 32.7(2) . . ?
C56 Lu5 C77 66.4(4) . . ?
C76 Lu5 C77 38.0(3) . . ?
Lu4 Lu5 C75 78.5(11) . . ?
Lu2 Lu5 C75 140.7(16) . . ?
C57 Lu5 C75 67.0(4) . . ?
C56 Lu5 C75 62.2(4) . . ?
C76 Lu5 C75 36.9(3) . . ?
C77 Lu5 C75 59.1(4) . . ?
Lu4 Lu5 Lu2 115.0(17) . 6 ?
Lu2 Lu5 Lu2 21.2(8) . 6 ?
C57 Lu5 Lu2 97.8(8) . 6 ?
C56 Lu5 Lu2 113.2(9) . 6 ?
C76 Lu5 Lu2 127.2(10) . 6 ?
C77 Lu5 Lu2 101.9(8) . 6 ?
C75 Lu5 Lu2 160.9(10) . 6 ?
Lu4 Lu5 Lu8 74.4(14) . . ?
Lu2 Lu5 Lu8 111.8(13) . . ?
C57 Lu5 Lu8 161.0(12) . . ?
C56 Lu5 Lu8 127.1(13) . . ?
C76 Lu5 Lu8 106.9(11) . . ?
C77 Lu5 Lu8 144.7(13) . . ?
C75 Lu5 Lu8 96.0(11) . . ?
Lu2 Lu5 Lu8 100.5(10) 6 . ?
Lu4 Lu5 C55 47.7(8) . . ?
Lu2 Lu5 C55 147.3(14) . . ?
C57 Lu5 C55 61.1(4) . . ?
C56 Lu5 C55 34.4(3) . . ?
C76 Lu5 C55 69.8(4) . . ?
C77 Lu5 C55 74.6(4) . . ?
C75 Lu5 C55 35.5(3) . . ?
Lu2 Lu5 C55 146.8(10) 6 . ?
Lu8 Lu5 C55 100.1(11) . . ?
Lu4 Lu5 Lu1 96.4(13) . . ?
Lu2 Lu5 Lu1 95.2(10) . . ?
C57 Lu5 Lu1 164.1(11) . . ?
C56 Lu5 Lu1 148.4(10) . . ?
C76 Lu5 Lu1 99.2(8) . . ?
C77 Lu5 Lu1 132.0(10) . . ?
C75 Lu5 Lu1 102.4(8) . . ?
Lu2 Lu5 Lu1 89.8(5) 6 . ?
Lu8 Lu5 Lu1 22.1(8) . . ?
C55 Lu5 Lu1 117.5(8) . . ?
Lu4 Lu5 C58 98.7(15) . . ?
Lu2 Lu5 C58 58.9(10) . . ?
C57 Lu5 C58 35.0(3) . . ?
C56 Lu5 C58 55.7(4) . . ?
C76 Lu5 C58 93.9(6) . . ?
C77 Lu5 C58 55.9(4) . . ?
C75 Lu5 C58 101.9(5) . . ?
Lu2 Lu5 C58 64.0(5) 6 . ?
Lu8 Lu5 C58 159.1(12) . . ?
C55 Lu5 C58 88.7(5) . . ?
Lu1 Lu5 C58 153.5(8) . . ?
Lu4 Lu6 Lu4 102.7(11) . 6 ?
Lu4 Lu6 C31 101.8(4) . . ?
Lu4 Lu6 C31 140.7(7) 6 . ?
Lu4 Lu6 C14 115.9(11) . . ?
Lu4 Lu6 C14 72.8(6) 6 . ?
C31 Lu6 C14 69.0(5) . . ?
Lu4 Lu6 C13 127.4(7) . . ?
Lu4 Lu6 C13 104.1(5) 6 . ?
C31 Lu6 C13 37.1(3) . . ?
C14 Lu6 C13 37.5(3) . . ?
Lu4 Lu6 C34 82.1(9) . . ?
Lu4 Lu6 C34 76.3(8) 6 . ?
C31 Lu6 C34 77.2(5) . . ?
C14 Lu6 C34 33.9(3) . . ?
C13 Lu6 C34 61.9(5) . . ?
Lu4 Lu6 C33 53.4(5) . . ?
Lu4 Lu6 C33 108.7(12) 6 . ?
C31 Lu6 C33 64.3(4) . . ?
C14 Lu6 C33 67.5(6) . . ?
C13 Lu6 C33 75.4(5) . . ?
C34 Lu6 C33 39.6(4) . . ?
Lu4 Lu6 C32 68.0(3) . . ?
Lu4 Lu6 C32 141.8(12) 6 . ?
C31 Lu6 C32 34.7(2) . . ?
C14 Lu6 C32 78.5(5) . . ?
C13 Lu6 C32 62.9(4) . . ?
C34 Lu6 C32 65.9(5) . . ?
C33 Lu6 C32 35.2(2) . . ?
Lu4 Lu6 Lu5 84.9(10) . 6 ?
Lu4 Lu6 Lu5 18.0(4) 6 6 ?
C31 Lu6 Lu5 151.7(10) . 6 ?
C14 Lu6 Lu5 83.2(8) . 6 ?
C13 Lu6 Lu5 118.4(7) . 6 ?
C34 Lu6 Lu5 76.6(9) . 6 ?
C33 Lu6 Lu5 100.6(11) . 6 ?
C32 Lu6 Lu5 135.8(12) . 6 ?
Lu4 Lu6 Lu5 18.0(4) . . ?
Lu4 Lu6 Lu5 84.9(10) 6 . ?
C31 Lu6 Lu5 118.5(6) . . ?
C14 Lu6 Lu5 113.6(12) . . ?
C13 Lu6 Lu5 137.2(10) . . ?
C34 Lu6 Lu5 80.7(9) . . ?
C33 Lu6 Lu5 62.3(6) . . ?
C32 Lu6 Lu5 84.0(6) . . ?
Lu5 Lu6 Lu5 67.1(10) 6 . ?
Lu4 Lu6 C12 154.5(6) . . ?
Lu4 Lu6 C12 97.8(3) 6 . ?
C31 Lu6 C12 52.9(5) . . ?
C14 Lu6 C12 56.4(4) . . ?
C13 Lu6 C12 30.4(3) . . ?
C34 Lu6 C12 88.2(5) . . ?
C33 Lu6 C12 105.5(6) . . ?
C32 Lu6 C12 86.5(6) . . ?
Lu5 Lu6 C12 115.7(4) 6 . ?
Lu5 Lu6 C12 167.6(9) . . ?
Lu4 Lu6 C15 125.8(12) . . ?
Lu4 Lu6 C15 48.0(3) 6 . ?
C31 Lu6 C15 92.7(5) . . ?
C14 Lu6 C15 27.42(15) . . ?
C13 Lu6 C15 56.5(3) . . ?
C34 Lu6 C15 50.6(3) . . ?
C33 Lu6 C15 89.8(7) . . ?
C32 Lu6 C15 105.9(6) . . ?
Lu5 Lu6 C15 62.2(5) 6 . ?
Lu5 Lu6 C15 114.9(11) . . ?
C12 Lu6 C15 60.4(3) . . ?
Lu3 Lu7 Lu1 52.2(7) . 6 ?
Lu3 Lu7 Lu1 52.2(7) . . ?
Lu1 Lu7 Lu1 100.9(12) 6 . ?
Lu3 Lu7 C66 115(2) . . ?
Lu1 Lu7 C66 123.8(9) 6 . ?
Lu1 Lu7 C66 105.6(7) . . ?
Lu3 Lu7 C65 114.2(17) . . ?
Lu1 Lu7 C65 89.8(5) 6 . ?
Lu1 Lu7 C65 140.5(11) . . ?
C66 Lu7 C65 41.0(4) . . ?
Lu3 Lu7 C67 77.6(16) . . ?
Lu1 Lu7 C67 106.0(10) 6 . ?
Lu1 Lu7 C67 77.6(6) . . ?
C66 Lu7 C67 37.9(3) . . ?
C65 Lu7 C67 62.9(6) . . ?
Lu3 Lu7 C64 149.0(13) . . ?
Lu1 Lu7 C64 105.2(4) 6 . ?
Lu1 Lu7 C64 153.6(8) . . ?
C66 Lu7 C64 56.0(6) . . ?
C65 Lu7 C64 37.4(4) . . ?
C67 Lu7 C64 91.6(8) . . ?
Lu3 Lu7 C82 129.0(14) . . ?
Lu1 Lu7 C82 158.1(10) 6 . ?
Lu1 Lu7 C82 91.2(3) . . ?
C66 Lu7 C82 34.4(3) . . ?
C65 Lu7 C82 69.6(6) . . ?
C67 Lu7 C82 58.6(4) . . ?
C64 Lu7 C82 62.9(6) . . ?
Lu3 Lu7 C43 94.2(13) . . ?
Lu1 Lu7 C43 67.7(4) 6 . ?
Lu1 Lu7 C43 135.7(12) . . ?
C66 Lu7 C43 58.6(5) . . ?
C65 Lu7 C43 23.01(16) . . ?
C67 Lu7 C43 66.1(5) . . ?
C64 Lu7 C43 55.0(4) . . ?
C82 Lu7 C43 90.9(7) . . ?
Lu3 Lu7 C45 49.8(14) . . ?
Lu1 Lu7 C45 79.5(8) 6 . ?
Lu1 Lu7 C45 70.0(7) . . ?
C66 Lu7 C45 65.2(6) . . ?
C65 Lu7 C45 75.0(6) . . ?
C67 Lu7 C45 29.5(3) . . ?
C64 Lu7 C45 111.1(8) . . ?
C82 Lu7 C45 87.8(6) . . ?
C43 Lu7 C45 65.9(5) . . ?
Lu3 Lu7 Lu8 47.0(11) . 6 ?
Lu1 Lu7 Lu8 13.5(6) 6 6 ?
Lu1 Lu7 Lu8 90.7(12) . 6 ?
C66 Lu7 Lu8 136.2(10) . 6 ?
C65 Lu7 Lu8 103.3(7) . 6 ?
C67 Lu7 Lu8 112.7(11) . 6 ?
C64 Lu7 Lu8 115.6(8) . 6 ?
C82 Lu7 Lu8 170.4(11) . 6 ?
C43 Lu7 Lu8 81.2(7) . 6 ?
C45 Lu7 Lu8 84.0(10) . 6 ?
Lu3 Lu7 Lu8 47.0(11) . . ?
Lu1 Lu7 Lu8 90.7(12) 6 . ?
Lu1 Lu7 Lu8 13.5(6) . . ?
C66 Lu7 Lu8 118.9(8) . . ?
C65 Lu7 Lu8 150.7(12) . . ?
C67 Lu7 Lu8 88.8(8) . . ?
C64 Lu7 Lu8 163.3(11) . . ?
C82 Lu7 Lu8 103.6(7) . . ?
C43 Lu7 Lu8 138.9(13) . . ?
C45 Lu7 Lu8 76.3(9) . . ?
Lu8 Lu7 Lu8 79.4(16) 6 . ?
Lu1 Lu8 Lu3 34.1(14) . . ?
Lu1 Lu8 C71 110.4(19) . . ?
Lu3 Lu8 C71 134.2(14) . . ?
Lu1 Lu8 C48 106.5(19) . . ?
Lu3 Lu8 C48 112.3(14) . . ?
C71 Lu8 C48 33.7(4) . . ?
Lu1 Lu8 Lu4 107(2) . . ?
Lu3 Lu8 Lu4 103.3(11) . . ?
C71 Lu8 Lu4 118.7(15) . . ?
C48 Lu8 Lu4 143.5(17) . . ?
Lu1 Lu8 C70 82.8(18) . . ?
Lu3 Lu8 C70 114.3(14) . . ?
C71 Lu8 C70 32.3(4) . . ?
C48 Lu8 C70 57.1(6) . . ?
Lu4 Lu8 C70 114.6(15) . . ?
Lu1 Lu8 Lu5 84(2) . . ?
Lu3 Lu8 Lu5 85.4(11) . . ?
C71 Lu8 Lu5 128.3(16) . . ?
C48 Lu8 Lu5 161.1(17) . . ?
Lu4 Lu8 Lu5 23.0(5) . . ?
C70 Lu8 Lu5 110.7(15) . . ?
Lu1 Lu8 C69 62.0(13) . . ?
Lu3 Lu8 C69 85.9(11) . . ?
C71 Lu8 C69 49.6(5) . . ?
C48 Lu8 C69 50.4(5) . . ?
Lu4 Lu8 C69 143.3(16) . . ?
C70 Lu8 C69 33.8(3) . . ?
Lu5 Lu8 C69 128.8(16) . . ?
Lu1 Lu8 C47 78.3(17) . . ?
Lu3 Lu8 C47 85.5(11) . . ?
C71 Lu8 C47 52.0(5) . . ?
C48 Lu8 C47 28.9(3) . . ?
Lu4 Lu8 C47 170.6(16) . . ?
C70 Lu8 C47 57.9(5) . . ?
Lu5 Lu8 C47 160.2(17) . . ?
C69 Lu8 C47 32.8(3) . . ?
Lu1 Lu8 Lu7 26.1(13) . . ?
Lu3 Lu8 Lu7 15.8(5) . . ?
C71 Lu8 Lu7 135.9(14) . . ?
C48 Lu8 Lu7 123.0(14) . . ?
Lu4 Lu8 Lu7 93.5(11) . . ?
C70 Lu8 Lu7 108.8(13) . . ?
Lu5 Lu8 Lu7 73.1(11) . . ?
C69 Lu8 Lu7 86.4(11) . . ?
C47 Lu8 Lu7 94.5(12) . . ?
Lu1 Lu8 C85 83(2) . . ?
Lu3 Lu8 C85 117.0(14) . . ?
C71 Lu8 C85 53.2(7) . . ?
C48 Lu8 C85 84.2(9) . . ?
Lu4 Lu8 C85 86.5(11) . . ?
C70 Lu8 C85 29.2(4) . . ?
Lu5 Lu8 C85 81.8(11) . . ?
C69 Lu8 C85 58.4(6) . . ?
C47 Lu8 C85 86.7(8) . . ?
Lu7 Lu8 C85 104.6(13) . . ?
Lu1 Lu8 C72 139(2) . . ?
Lu3 Lu8 C72 170.3(12) . . ?
C71 Lu8 C72 36.2(5) . . ?
C48 Lu8 C72 60.0(7) . . ?
Lu4 Lu8 C72 85.2(11) . . ?
C70 Lu8 C72 57.1(7) . . ?
Lu5 Lu8 C72 101.6(13) . . ?
C69 Lu8 C72 84.5(8) . . ?
C47 Lu8 C72 85.7(8) . . ?
Lu7 Lu8 C72 162.9(15) . . ?
C85 Lu8 C72 58.3(7) . . ?
C9 C1 C5 122.1 . . ?
C9 C1 C2 119.5 . . ?
C5 C1 C2 107.6 . . ?
C12 C2 C1 125.8 . . ?
C12 C2 C3 115.3 . . ?
C1 C2 C3 108.1 . . ?
C15 C3 C4 117.2 . . ?
C15 C3 C2 125.9 . . ?
C4 C3 C2 107.3 . . ?
C18 C4 C5 116.8 . . ?
C18 C4 C3 128.1 . . ?
C5 C4 C3 107.8 . . ?
C1 C5 C4 108.3 . . ?
C1 C5 C6 116.6 . . ?
C4 C5 C6 124.1 . . ?
C7 C6 C5 111.1 . . ?
C7 C6 C20 117.6 . . ?
C5 C6 C20 117.7 . . ?
C8 C7 C6 137.0 . . ?
C8 C7 C23 101.5 . . ?
C6 C7 C23 118.8 . . ?
C7 C8 C26 144.3 . . ?
C7 C8 C9 111.3 . . ?
C26 C8 C9 95.9 . . ?
C1 C9 C10 121.7 . . ?
C1 C9 C8 120.3 . . ?
C10 C9 C8 106.6 . . ?
C11 C10 C27 121.8 . . ?
C11 C10 C9 119.4 . . ?
C27 C10 C9 110.1 . . ?
C10 C11 C12 121.9 . . ?
C10 C11 C30 119.1 . . ?
C12 C11 C30 107.1 . . ?
C2 C12 C11 111.3 . . ?
C2 C12 C13 122.1 . . ?
C11 C12 C13 107.8 . . ?
C2 C12 Lu6 91.8(2) . . ?
C11 C12 Lu6 83.7(5) . . ?
C13 C12 Lu6 52.1(4) . . ?
C31 C13 C12 107.6 . . ?
C31 C13 C14 124.6 . . ?
C12 C13 C14 116.2 . . ?
C31 C13 Lu6 71.1(3) . . ?
C12 C13 Lu6 97.5(6) . . ?
C14 C13 Lu6 71.2(7) . . ?
C34 C14 C15 115.4 . . ?
C34 C14 C13 115.5 . . ?
C15 C14 C13 124.7 . . ?
C34 C14 Lu6 76.0(6) . . ?
C15 C14 Lu6 101.7(3) . . ?
C13 C14 Lu6 71.3(7) . . ?
C16 C15 C14 119.6 . . ?
C16 C15 C3 122.1 . . ?
C14 C15 C3 114.3 . . ?
C16 C15 Lu6 107.0(5) . . ?
C14 C15 Lu6 50.8(3) . . ?
C3 C15 Lu6 90.7(5) . . ?
C15 C16 C36 120.9 . . ?
C15 C16 C17 121.3 . . ?
C36 C16 C17 107.3 . . ?
C39 C17 C16 127.4 . . ?
C39 C17 C18 101.8 . . ?
C16 C17 C18 122.7 . . ?
C4 C18 C19 119.1 . . ?
C4 C18 C17 107.2 . . ?
C19 C18 C17 117.3 . . ?
C40 C19 C20 133.4 . . ?
C40 C19 C18 90.3 . . ?
C20 C19 C18 122.5 . . ?
C19 C20 C6 117.7 . . ?
C19 C20 C21 99.3 . . ?
C6 C20 C21 135.7 . . ?
C42 C21 C20 130.0 . . ?
C42 C21 C22 114.6 . . ?
C20 C21 C22 104.2 . . ?
C44 C22 C23 134.8 . . ?
C44 C22 C21 99.2 . . ?
C23 C22 C21 121.9 . . ?
C44 C22 Lu3 62.81(13) . . ?
C23 C22 Lu3 92.74(15) . . ?
C21 C22 Lu3 96.15(13) . . ?
C24 C23 C22 114.4 . . ?
C24 C23 C7 119.1 . . ?
C22 C23 C7 121.5 . . ?
C25 C24 C23 125.4 . . ?
C25 C24 C46 119.2 . . ?
C23 C24 C46 113.1 . . ?
C24 C25 C26 110.0 . . ?
C24 C25 C49 115.7 . . ?
C26 C25 C49 130.8 . . ?
C8 C26 C27 120.7 . . ?
C8 C26 C25 117.7 . . ?
C27 C26 C25 115.9 . . ?
C10 C27 C26 105.7 . . ?
C10 C27 C28 122.6 . . ?
C26 C27 C28 116.8 . . ?
C50 C28 C27 125.3 . . ?
C50 C28 C29 110.1 . . ?
C27 C28 C29 111.4 . . ?
C30 C29 C52 135.7 . . ?
C30 C29 C28 122.0 . . ?
C52 C29 C28 95.7 . . ?
C29 C30 C31 114.5 . . ?
C29 C30 C11 122.7 . . ?
C31 C30 C11 107.8 . . ?
C29 C30 Lu6 95.0(3) . . ?
C31 C30 Lu6 51.1(4) . . ?
C11 C30 Lu6 82.8(2) . . ?
C30 C31 C32 128.6 . . ?
C30 C31 C13 108.1 . . ?
C32 C31 C13 120.4 . . ?
C30 C31 Lu6 99.4(7) . . ?
C32 C31 Lu6 81.7(5) . . ?
C13 C31 Lu6 71.8(3) . . ?
C53 C32 C31 103.1 . . ?
C53 C32 C33 123.9 . . ?
C31 C32 C33 117.6 . . ?
C53 C32 Lu6 98.7(4) . . ?
C31 C32 Lu6 63.7(6) . . ?
C33 C32 Lu6 70.1(7) . . ?
C53 C32 Lu4 77.29(17) . . ?
C31 C32 Lu4 113.63(15) . . ?
C33 C32 Lu4 52.31(16) . . ?
Lu6 C32 Lu4 51.2(5) . . ?
C56 C33 C32 115.8 . . ?
C56 C33 C34 126.7 . . ?
C32 C33 C34 115.4 . . ?
C56 C33 Lu4 56.6(2) . . ?
C32 C33 Lu4 93.5(2) . . ?
C34 C33 Lu4 106.8(2) . . ?
C56 C33 Lu6 114.4(4) . . ?
C32 C33 Lu6 74.7(6) . . ?
C34 C33 Lu6 67.0(4) . . ?
Lu4 C33 Lu6 58.3(4) . . ?
C56 C33 Lu5 50.4(3) . . ?
C32 C33 Lu5 111.2(4) . . ?
C34 C33 Lu5 97.3(4) . . ?
Lu4 C33 Lu5 17.7(4) . . ?
Lu6 C33 Lu5 65.1(6) . . ?
C35 C34 C14 124.7 . . ?
C35 C34 C33 109.5 . . ?
C14 C34 C33 123.7 . . ?
C35 C34 Lu6 116.9(6) . . ?
C14 C34 Lu6 70.2(4) . . ?
C33 C34 Lu6 73.33(14) . . ?
C34 C35 C36 119.7 . . ?
C34 C35 C58 120.2 . . ?
C36 C35 C58 111.2 . . ?
C34 C35 Lu2 95.70(10) . . ?
C36 C35 Lu2 93.75(12) . . ?
C58 C35 Lu2 50.35(9) . . ?
C37 C36 C16 129.8 . . ?
C37 C36 C35 108.8 . . ?
C16 C36 C35 118.2 . . ?
C36 C37 C59 113.4 . . ?
C36 C37 C38 123.5 . . ?
C59 C37 C38 112.8 . . ?
C62 C38 C39 122.6 . . ?
C62 C38 C37 122.3 . . ?
C39 C38 C37 105.4 . . ?
C38 C39 C17 125.1 . . ?
C38 C39 C40 121.4 . . ?
C17 C39 C40 101.3 . . ?
C41 C40 C19 116.2 . . ?
C41 C40 C39 109.2 . . ?
C19 C40 C39 126.4 . . ?
C40 C41 C63 137.2 . . ?
C40 C41 C42 118.1 . . ?
C63 C41 C42 96.4 . . ?
C21 C42 C41 120.7 . . ?
C21 C42 C43 103.6 . . ?
C41 C42 C43 127.6 . . ?
C65 C43 C44 125.3 . . ?
C65 C43 C42 121.4 . . ?
C44 C43 C42 101.3 . . ?
C65 C43 Lu7 60.6(5) . . ?
C44 C43 Lu7 82.5(6) . . ?
C42 C43 Lu7 98.1(4) . . ?
C65 C43 Lu3 76.57(16) . . ?
C44 C43 Lu3 65.07(16) . . ?
C42 C43 Lu3 96.91(11) . . ?
Lu7 C43 Lu3 17.9(5) . . ?
C22 C44 C43 118.4 . . ?
C22 C44 C45 112.4 . . ?
C43 C44 C45 115.0 . . ?
C22 C44 Lu3 90.48(16) . . ?
C43 C44 Lu3 79.71(18) . . ?
C45 C44 Lu3 61.68(13) . . ?
C22 C44 Lu7 101.9(4) . . ?
C43 C44 Lu7 63.2(5) . . ?
C45 C44 Lu7 69.1(3) . . ?
Lu3 C44 Lu7 17.0(4) . . ?
C67 C45 C46 145.1 . . ?
C67 C45 C44 99.3 . . ?
C46 C45 C44 111.2 . . ?
C67 C45 Lu3 78.93(19) . . ?
C46 C45 Lu3 93.07(19) . . ?
C44 C45 Lu3 74.35(14) . . ?
C67 C45 Lu7 63.8(5) . . ?
C46 C45 Lu7 108.8(5) . . ?
C44 C45 Lu7 72.88(14) . . ?
Lu3 C45 Lu7 16.2(5) . . ?
C67 C45 Lu1 76.63(12) . . ?
C46 C45 Lu1 78.10(13) . . ?
C44 C45 Lu1 108.13(11) . . ?
Lu3 C45 Lu1 33.93(8) . . ?
Lu7 C45 Lu1 40.4(3) . . ?
C45 C46 C47 106.7 . . ?
C45 C46 C24 132.6 . . ?
C47 C46 C24 115.2 . . ?
C45 C46 Lu3 56.83(14) . . ?
C47 C46 Lu3 100.98(11) . . ?
C24 C46 Lu3 93.29(14) . . ?
C45 C46 Lu1 73.31(12) . . ?
C47 C46 Lu1 69.40(11) . . ?
C24 C46 Lu1 101.26(10) . . ?
Lu3 C46 Lu1 32.11(8) . . ?
C45 C46 Lu8 92.6(7) . . ?
C47 C46 Lu8 62.7(6) . . ?
C24 C46 Lu8 88.0(7) . . ?
Lu3 C46 Lu8 45.7(7) . . ?
Lu1 C46 Lu8 19.3(7) . . ?
C48 C47 C69 100.6 . . ?
C48 C47 C46 121.4 . . ?
C69 C47 C46 117.6 . . ?
C48 C47 Lu1 84.86(12) . . ?
C69 C47 Lu1 60.87(11) . . ?
C46 C47 Lu1 78.06(12) . . ?
C48 C47 Lu8 63.8(8) . . ?
C69 C47 Lu8 71.8(8) . . ?
C46 C47 Lu8 86.9(8) . . ?
Lu1 C47 Lu8 21.5(8) . . ?
C47 C48 C49 118.8 . . ?
C47 C48 C71 112.4 . . ?
C49 C48 C71 126.4 . . ?
C47 C48 Lu8 87.3(9) . . ?
C49 C48 Lu8 95.4(8) . . ?
C71 C48 Lu8 71.3(9) . . ?
C47 C48 Lu1 68.27(10) . . ?
C49 C48 Lu1 107.96(10) . . ?
C71 C48 Lu1 76.38(11) . . ?
Lu8 C48 Lu1 19.5(8) . . ?
C48 C49 C25 125.1 . . ?
C48 C49 C50 123.2 . . ?
C25 C49 C50 104.2 . . ?
C48 C49 Lu8 56.4(6) . . ?
C25 C49 Lu8 94.4(7) . . ?
C50 C49 Lu8 97.4(7) . . ?
C28 C50 C51 116.7 . . ?
C28 C50 C49 126.6 . . ?
C51 C50 C49 106.5 . . ?
C50 C51 C52 106.2 . . ?
C50 C51 C72 136.8 . . ?
C52 C51 C72 110.1 . . ?
C51 C52 C53 129.8 . . ?
C51 C52 C29 110.3 . . ?
C53 C52 C29 98.4 . . ?
C54 C53 C32 105.8 . . ?
C54 C53 C52 109.8 . . ?
C32 C53 C52 138.1 . . ?
C54 C53 Lu4 56.14(17) . . ?
C32 C53 Lu4 71.99(15) . . ?
C52 C53 Lu4 111.09(13) . . ?
C55 C54 C53 130.7 . . ?
C55 C54 C73 104.6 . . ?
C53 C54 C73 118.0 . . ?
C55 C54 Lu4 59.99(18) . . ?
C53 C54 Lu4 93.2(2) . . ?
C73 C54 Lu4 92.32(17) . . ?
C54 C55 C56 121.7 . . ?
C54 C55 C75 116.9 . . ?
C56 C55 C75 105.3 . . ?
C54 C55 Lu4 86.8(2) . . ?
C56 C55 Lu4 60.5(2) . . ?
C75 C55 Lu4 82.1(2) . . ?
C54 C55 Lu5 105.0(4) . . ?
C56 C55 Lu5 59.2(5) . . ?
C75 C55 Lu5 64.6(5) . . ?
Lu4 C55 Lu5 21.0(5) . . ?
C33 C56 C57 125.9 . . ?
C33 C56 C55 117.4 . . ?
C57 C56 C55 115.2 . . ?
C33 C56 Lu4 84.6(3) . . ?
C57 C56 Lu4 96.8(3) . . ?
C55 C56 Lu4 75.7(3) . . ?
C33 C56 Lu5 100.9(6) . . ?
C57 C56 Lu5 70.5(6) . . ?
C55 C56 Lu5 86.3(6) . . ?
Lu4 C56 Lu5 26.3(5) . . ?
C33 C56 Lu2 95.68(11) . . ?
C57 C56 Lu2 58.82(9) . . ?
C55 C56 Lu2 104.93(11) . . ?
Lu4 C56 Lu2 40.7(3) . . ?
Lu5 C56 Lu2 19.1(5) . . ?
C77 C57 C56 132.1 . . ?
C77 C57 C58 114.4 . . ?
C56 C57 C58 102.8 . . ?
C77 C57 Lu5 78.9(6) . . ?
C56 C57 Lu5 71.4(6) . . ?
C58 C57 Lu5 90.6(5) . . ?
C77 C57 Lu2 76.36(13) . . ?
C56 C57 Lu2 89.88(13) . . ?
C58 C57 Lu2 70.09(13) . . ?
Lu5 C57 Lu2 24.7(5) . . ?
C77 C57 Lu4 98.31(18) . . ?
C56 C57 Lu4 47.69(19) . . ?
C58 C57 Lu4 94.86(19) . . ?
Lu5 C57 Lu4 23.7(5) . . ?
Lu2 C57 Lu4 44.40(17) . . ?
C59 C58 C35 97.9 . . ?
C59 C58 C57 123.6 . . ?
C35 C58 C57 134.4 . . ?
C59 C58 Lu2 81.38(15) . . ?
C35 C58 Lu2 100.09(12) . . ?
C57 C58 Lu2 71.58(15) . . ?
C59 C58 Lu5 101.7(5) . . ?
C35 C58 Lu5 103.1(5) . . ?
C57 C58 Lu5 54.5(4) . . ?
Lu2 C58 Lu5 21.2(4) . . ?
C59 C58 Lu4 118.53(14) . . ?
C35 C58 Lu4 91.40(16) . . ?
C57 C58 Lu4 54.34(15) . . ?
Lu2 C58 Lu4 37.26(14) . . ?
Lu5 C58 Lu4 18.9(5) . . ?
C37 C59 C60 131.0 . . ?
C37 C59 C58 108.2 . . ?
C60 C59 C58 109.1 . . ?
C37 C59 Lu2 101.59(12) . . ?
C60 C59 Lu2 68.94(12) . . ?
C58 C59 Lu2 63.82(13) . . ?
C78 C60 C59 133.8 . . ?
C78 C60 C61 106.0 . . ?
C59 C60 C61 112.0 . . ?
C78 C60 Lu2 71.62(13) . . ?
C59 C60 Lu2 78.23(12) . . ?
C61 C60 Lu2 97.46(13) . . ?
C60 C61 C81 114.2 . . ?
C60 C61 C62 120.7 . . ?
C81 C61 C62 111.0 . . ?
C38 C62 C61 120.0 . . ?
C38 C62 C63 127.0 . . ?
C61 C62 C63 105.6 . . ?
C41 C63 C62 102.2 . . ?
C41 C63 C64 137.5 . . ?
C62 C63 C64 108.9 . . ?
C65 C64 C81 138.8 . . ?
C65 C64 C63 103.7 . . ?
C81 C64 C63 107.7 . . ?
C65 C64 Lu7 62.1(5) . . ?
C81 C64 Lu7 87.4(4) . . ?
C63 C64 Lu7 98.0(3) . . ?
C43 C65 C64 132.2 . . ?
C43 C65 C66 131.6 . . ?
C64 C65 C66 91.7 . . ?
C43 C65 Lu7 96.4(5) . . ?
C64 C65 Lu7 80.5(7) . . ?
C66 C65 Lu7 67.8(3) . . ?
C43 C65 Lu3 82.21(14) . . ?
C64 C65 Lu3 96.53(14) . . ?
C66 C65 Lu3 71.76(12) . . ?
Lu7 C65 Lu3 16.7(6) . . ?
C82 C66 C67 111.3 . . ?
C82 C66 C65 132.5 . . ?
C67 C66 C65 106.3 . . ?
C82 C66 Lu7 86.4(4) . . ?
C67 C66 Lu7 81.7(7) . . ?
C65 C66 Lu7 71.16(19) . . ?
C82 C66 Lu3 95.68(13) . . ?
C67 C66 Lu3 65.26(15) . . ?
C65 C66 Lu3 74.56(12) . . ?
Lu7 C66 Lu3 16.8(6) . . ?
C45 C67 C66 137.4 . . ?
C45 C67 C68 106.6 . . ?
C66 C67 C68 99.2 . . ?
C45 C67 Lu3 67.89(18) . . ?
C66 C67 Lu3 79.84(19) . . ?
C68 C67 Lu3 88.42(13) . . ?
C45 C67 Lu7 86.7(6) . . ?
C66 C67 Lu7 60.4(6) . . ?
C68 C67 Lu7 88.6(2) . . ?
Lu3 C67 Lu7 19.7(5) . . ?
C45 C67 Lu1 74.97(12) . . ?
C66 C67 Lu1 93.34(12) . . ?
C68 C67 Lu1 55.80(11) . . ?
Lu3 C67 Lu1 33.53(8) . . ?
Lu7 C67 Lu1 42.0(4) . . ?
C69 C68 C83 136.7 . . ?
C69 C68 C67 109.9 . . ?
C83 C68 C67 108.9 . . ?
C69 C68 Lu1 74.96(15) . . ?
C83 C68 Lu1 90.69(13) . . ?
C67 C68 Lu1 84.07(14) . . ?
C69 C68 Lu3 93.65(15) . . ?
C83 C68 Lu3 93.38(14) . . ?
C67 C68 Lu3 54.56(11) . . ?
Lu1 C68 Lu3 30.49(11) . . ?
C69 C68 Lu7 109.0(5) . . ?
C83 C68 Lu7 78.9(5) . . ?
C67 C68 Lu7 54.9(4) . . ?
Lu1 C68 Lu7 39.0(4) . . ?
Lu3 C68 Lu7 16.1(4) . . ?
C69 C68 Lu8 61.3(6) . . ?
C83 C68 Lu8 96.9(7) . . ?
C67 C68 Lu8 95.1(7) . . ?
Lu1 C68 Lu8 15.1(6) . . ?
Lu3 C68 Lu8 44.2(7) . . ?
Lu7 C68 Lu8 54.1(8) . . ?
C68 C69 C70 104.5 . . ?
C68 C69 C47 130.4 . . ?
C70 C69 C47 113.7 . . ?
C68 C69 C71 138.0 . . ?
C70 C69 C71 39.8 . . ?
C47 C69 C71 74.1 . . ?
C68 C69 Lu1 70.73(14) . . ?
C70 C69 Lu1 80.74(13) . . ?
C47 C69 Lu1 85.01(14) . . ?
C71 C69 Lu1 80.10(14) . . ?
C68 C69 Lu8 91.7(8) . . ?
C70 C69 Lu8 67.9(8) . . ?
C47 C69 Lu8 75.4(8) . . ?
C71 C69 Lu8 58.5(8) . . ?
Lu1 C69 Lu8 22.1(8) . . ?
C85 C70 C71 117.9 . . ?
C85 C70 C69 134.9 . . ?
C71 C70 C69 95.3 . . ?
C85 C70 Lu8 86.2(8) . . ?
C71 C70 Lu8 68.7(9) . . ?
C69 C70 Lu8 78.3(8) . . ?
C85 C70 Lu1 86.06(11) . . ?
C71 C70 Lu1 88.39(13) . . ?
C69 C70 Lu1 64.06(10) . . ?
Lu8 C70 Lu1 22.7(8) . . ?
C70 C71 C48 117.3 . . ?
C70 C71 C72 114.6 . . ?
C48 C71 C72 118.9 . . ?
C70 C71 C69 44.9 . . ?
C48 C71 C69 72.8 . . ?
C72 C71 C69 151.4 . . ?
C70 C71 Lu8 79.0(9) . . ?
C48 C71 Lu8 75.0(9) . . ?
C72 C71 Lu8 85.7(8) . . ?
C69 C71 Lu8 71.8(8) . . ?
C70 C71 Lu1 63.40(11) . . ?
C48 C71 Lu1 75.60(11) . . ?
C72 C71 Lu1 101.97(8) . . ?
C69 C71 Lu1 53.41(9) . . ?
Lu8 C71 Lu1 19.0(8) . . ?
C73 C72 C51 124.5 . . ?
C73 C72 C71 121.5 . . ?
C51 C72 C71 106.8 . . ?
C73 C72 Lu8 91.0(7) . . ?
C51 C72 Lu8 92.4(8) . . ?
C71 C72 Lu8 58.2(6) . . ?
C72 C73 C74 121.6 . . ?
C72 C73 C54 120.5 . . ?
C74 C73 C54 102.6 . . ?
C72 C73 Lu4 103.76(13) . . ?
C74 C73 Lu4 71.65(17) . . ?
C54 C73 Lu4 52.75(14) . . ?
C85 C74 C75 129.8 . . ?
C85 C74 C73 109.5 . . ?
C75 C74 C73 111.6 . . ?
C85 C74 Lu4 106.74(13) . . ?
C75 C74 Lu4 55.99(14) . . ?
C73 C74 Lu4 79.11(18) . . ?
C85 C74 Lu5 95.8(4) . . ?
C75 C74 Lu5 51.4(3) . . ?
C73 C74 Lu5 97.9(5) . . ?
Lu4 C74 Lu5 19.4(4) . . ?
C74 C75 C76 108.8 . . ?
C74 C75 C55 104.0 . . ?
C76 C75 C55 138.2 . . ?
C74 C75 Lu5 99.6(5) . . ?
C76 C75 Lu5 69.8(6) . . ?
C55 C75 Lu5 79.9(6) . . ?
C74 C75 Lu4 93.23(17) . . ?
C76 C75 Lu4 94.0(2) . . ?
C55 C75 Lu4 58.52(19) . . ?
Lu5 C75 Lu4 24.2(5) . . ?
C86 C76 C75 138.4 . . ?
C86 C76 C77 116.5 . . ?
C75 C76 C77 101.2 . . ?
C86 C76 Lu5 101.5(5) . . ?
C75 C76 Lu5 73.3(5) . . ?
C77 C76 Lu5 71.4(5) . . ?
C86 C76 Lu2 90.75(12) . . ?
C75 C76 Lu2 92.76(12) . . ?
C77 C76 Lu2 60.89(9) . . ?
Lu5 C76 Lu2 20.3(5) . . ?
C86 C76 Lu4 115.12(13) . . ?
C75 C76 Lu4 55.21(17) . . ?
C77 C76 Lu4 76.91(15) . . ?
Lu5 C76 Lu4 18.1(5) . . ?
Lu2 C76 Lu4 37.78(15) . . ?
C57 C77 C76 121.1 . . ?
C57 C77 C78 124.0 . . ?
C76 C77 C78 95.9 . . ?
C57 C77 Lu5 68.4(6) . . ?
C76 C77 Lu5 70.6(6) . . ?
C78 C77 Lu5 90.0(5) . . ?
C57 C77 Lu2 72.68(13) . . ?
C76 C77 Lu2 85.99(12) . . ?
C78 C77 Lu2 69.51(14) . . ?
Lu5 C77 Lu2 24.1(5) . . ?
C57 C77 Lu4 56.15(13) . . ?
C76 C77 Lu4 72.98(15) . . ?
C78 C77 Lu4 106.83(15) . . ?
Lu5 C77 Lu4 17.2(5) . . ?
Lu2 C77 Lu4 38.47(15) . . ?
C60 C78 C79 129.6 . . ?
C60 C78 C77 112.9 . . ?
C79 C78 C77 112.6 . . ?
C60 C78 Lu2 78.84(14) . . ?
C79 C78 Lu2 96.21(12) . . ?
C77 C78 Lu2 71.32(15) . . ?
C60 C78 Lu5 96.4(4) . . ?
C79 C78 Lu5 92.0(4) . . ?
C77 C78 Lu5 55.3(3) . . ?
Lu2 C78 Lu5 19.8(3) . . ?
C80 C79 C78 135.5 . . ?
C80 C79 C86 107.0 . . ?
C78 C79 C86 102.4 . . ?
C80 C79 C81 41.7 . . ?
C78 C79 C81 96.4 . . ?
C86 C79 C81 142.4 . . ?
C80 C79 Lu2 98.84(10) . . ?
C78 C79 Lu2 53.82(8) . . ?
C86 C79 Lu2 80.82(12) . . ?
C81 C79 Lu2 84.59(12) . . ?
C79 C80 C81 100.5 . . ?
C79 C80 C82 140.4 . . ?
C81 C80 C82 112.9 . . ?
C79 C80 Lu7 110.4(4) . . ?
C81 C80 Lu7 77.6(3) . . ?
C82 C80 Lu7 59.9(4) . . ?
C80 C81 C61 129.8 . . ?
C80 C81 C64 112.7 . . ?
C61 C81 C64 106.5 . . ?
C80 C81 C79 37.8 . . ?
C61 C81 C79 92.9 . . ?
C64 C81 C79 144.1 . . ?
C80 C81 Lu7 75.47(14) . . ?
C61 C81 Lu7 102.4(4) . . ?
C64 C81 Lu7 57.3(3) . . ?
C79 C81 Lu7 89.6(2) . . ?
C66 C82 C80 128.4 . . ?
C66 C82 C83 116.4 . . ?
C80 C82 C83 106.0 . . ?
C66 C82 Lu7 59.2(4) . . ?
C80 C82 Lu7 89.4(6) . . ?
C83 C82 Lu7 96.2(4) . . ?
C66 C82 Lu3 57.24(10) . . ?
C80 C82 Lu3 99.49(11) . . ?
C83 C82 Lu3 86.98(11) . . ?
Lu7 C82 Lu3 12.1(5) . . ?
C84 C83 C68 111.8 . . ?
C84 C83 C82 129.4 . . ?
C68 C83 C82 104.2 . . ?
C84 C83 Lu1 80.17(11) . . ?
C68 C83 Lu1 56.91(9) . . ?
C82 C83 Lu1 91.44(12) . . ?
C84 C83 Lu7 104.0(4) . . ?
C68 C83 Lu7 73.2(5) . . ?
C82 C83 Lu7 54.1(4) . . ?
Lu1 C83 Lu7 37.4(4) . . ?
C83 C84 C86 105.8 . . ?
C83 C84 C85 120.9 . . ?
C86 C84 C85 124.8 . . ?
C83 C84 Lu1 70.13(10) . . ?
C86 C84 Lu1 101.28(9) . . ?
C85 C84 Lu1 71.71(12) . . ?
C70 C85 C74 133.8 . . ?
C70 C85 C84 109.6 . . ?
C74 C85 C84 109.4 . . ?
C70 C85 Lu8 64.6(6) . . ?
C74 C85 Lu8 89.3(7) . . ?
C84 C85 Lu8 93.5(8) . . ?
C70 C85 Lu1 65.43(9) . . ?
C74 C85 Lu1 103.00(8) . . ?
C84 C85 Lu1 74.55(12) . . ?
Lu8 C85 Lu1 20.6(8) . . ?
C76 C86 C79 112.3 . . ?
C76 C86 C84 107.8 . . ?
C79 C86 C84 129.9 . . ?
C76 C86 Lu5 51.7(3) . . ?
C79 C86 Lu5 89.5(4) . . ?
C84 C86 Lu5 92.7(4) . . ?
C88 C87 C92 120.0 . . ?
C89 C88 C87 120.0 . . ?
C88 C89 C90 120.0 . . ?
C89 C90 C91 120.0 . . ?
C92 C91 C90 120.0 . . ?
C91 C92 C87 120.0 . . ?
N1 Ni1 N2 90.7(3) . 6 ?
N1 Ni1 N2 90.7(3) . . ?
N2 Ni1 N2 177.6(4) 6 . ?
N1 Ni1 N3 179.3(4) . . ?
N2 Ni1 N3 89.3(3) 6 . ?
N2 Ni1 N3 89.3(3) . . ?
C99 C93 N1 124.7(9) . . ?
C99 C93 C110 125.1(9) . . ?
N1 C93 C110 110.2(8) . . ?
C99 C94 N2 125.8(9) . . ?
C99 C94 C100 126.3(9) . . ?
N2 C94 C100 107.9(8) . . ?
N2 C95 C106 126.4(9) . . ?
N2 C95 C103 111.0(9) . . ?
C106 C95 C103 122.5(10) . . ?
C106 C96 N3 127.8(9) . . ?
C106 C96 C108 121.8(10) . . ?
N3 C96 C108 110.4(8) . . ?
C96 N3 C96 105.9(10) 6 . ?
C96 N3 Ni1 127.0(5) 6 . ?
C96 N3 Ni1 127.0(5) . . ?
C93 N1 C93 104.9(10) . 6 ?
C93 N1 Ni1 127.5(5) . . ?
C93 N1 Ni1 127.5(5) 6 . ?
C95 N2 C94 105.6(8) . . ?
C95 N2 Ni1 128.4(7) . . ?
C94 N2 Ni1 126.0(6) . . ?
C110 C98 C97 112.9(8) . . ?
C94 C99 C93 125.2(10) . . ?
C103 C100 C94 109.1(10) . . ?
C103 C100 C101 128.8(10) . . ?
C94 C100 C101 122.0(10) . . ?
C100 C101 C102 113.9(9) . . ?
C100 C103 C95 106.3(10) . . ?
C100 C103 C104 131.0(12) . . ?
C95 C103 C104 122.6(11) . . ?
C103 C104 C105 114.0(9) . . ?
C96 C106 C95 121.0(10) . . ?
C108 C107 C109 114.4(10) . . ?
C108 C108 C96 106.6(6) 6 . ?
C108 C108 C107 131.1(7) 6 . ?
C96 C108 C107 122.2(11) . . ?
C110 C110 C93 107.4(5) 6 . ?
C110 C110 C98 130.0(6) 6 . ?
C93 C110 C98 122.5(9) . . ?
N6 Ni2 N6 91.1(7) . 6 ?
N6 Ni2 N6 88.9(7) . 2_655 ?
N6 Ni2 N6 180.0(9) 6 2_655 ?
N6 Ni2 N6 180.0 . 5_655 ?
N6 Ni2 N6 88.9(7) 6 5_655 ?
N6 Ni2 N6 91.1(7) 2_655 5_655 ?
C127 C126 C127 124(2) . 2_655 ?
C126 C127 N6 125.1(16) . . ?
C126 C127 C130 123.9(14) . . ?
N6 C127 C130 111.1(13) . . ?
C130 C129 C128 113.4(12) . . ?
C133 C130 C127 107.8(14) . . ?
C133 C130 C129 127.6(16) . . ?
C127 C130 C129 124.5(15) . . ?
C133 C132 C131 110.1(14) . . ?
C130 C133 C134 105.6(15) . . ?
C130 C133 C132 130.2(15) . . ?
C134 C133 C132 124.1(15) . . ?
C135 C134 N6 123.2(15) . . ?
C135 C134 C133 125.4(16) . . ?
N6 C134 C133 111.5(13) . . ?
C134 C135 C134 128(2) . 6 ?
C127 N6 C134 104.1(12) . . ?
C127 N6 Ni2 128.7(11) . . ?
C134 N6 Ni2 127.3(9) . . ?
C3E C1E C6E 120.0 . . ?
C2E C3E C1E 120.0 . . ?
C3E C2E C4E 120.0 . . ?
C5E C4E C2E 120.0 . . ?
C4E C5E C6E 120.0 . . ?
C5E C6E C1E 120.0 . . ?

_refine_diff_density_max         1.974
_refine_diff_density_min         -1.607
_refine_diff_density_rms         0.165


_vrf_PLAT307_Lu2@Cs8-C86         
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2@Cs8-C86         
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT973_Lu2@Cs8-C86         
;
PROBLEM: PLAT973 Type_2  Check Calcd Positive Residual Density on Ni1 3.06 eA-3   
RESPONSE: There are no big Q peaks around the Ni1.The Positive 
Residual Density on Ni1 may caused by the severe disoder of the 
internal metal atoms
;

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2@C2v-C80
_database_code_depnum_ccdc_archive 'CCDC 1582216'
_audit_update_record             
;
2017-10-26 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2@C2v-C80 Ni(OEP)'
_chemical_name_common            'Lu2@C2v-C80 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C80, C36 H44 N4 Ni, 2(C6 H6)'
_chemical_formula_sum            'C128 H56 Lu2 N4 Ni'
_chemical_formula_weight         2058.41

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0027 0.0014 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.2922 5.1425 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0053 0.0028 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3436 0.9622 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   25.186(5)
_cell_length_b                   15.099(5)
_cell_length_c                   19.694(5)
_cell_angle_alpha                90
_cell_angle_beta                 94.158(5)
_cell_angle_gamma                90
_cell_volume                     7470(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9941
_cell_measurement_theta_min      2.654
_cell_measurement_theta_max      23.163

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.830
_exptl_crystal_F_000             4088
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.100
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.060
_exptl_absorpt_coefficient_mu    2.389
_shelx_estimated_absorpt_T_min   0.787
_shelx_estimated_absorpt_T_max   0.866
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.4605
_exptl_absorpt_correction_T_max  0.7449
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline BL17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            50453
_diffrn_reflns_av_unetI/netI     0.0272
_diffrn_reflns_av_R_equivalents  0.0439
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_h_max       30
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         0.952
_diffrn_reflns_theta_max         23.177
_diffrn_reflns_theta_full        23.048
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measured_fraction_theta_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_point_group_measured_fraction_full 0.996
_reflns_number_total             7127
_reflns_number_gt                6155
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1813P)²+100.2916P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7127
_refine_ls_number_parameters     884
_refine_ls_number_restraints     1152
_refine_ls_R_factor_all          0.1238
_refine_ls_R_factor_gt           0.1125
_refine_ls_wR_factor_ref         0.3111
_refine_ls_wR_factor_gt          0.2978
_refine_ls_goodness_of_fit_ref   1.036
_refine_ls_restrained_S_all      1.117
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.34108(7) 0.38089(14) 0.29085(12) 0.0434(5) Uani 0.1576 1 d . U P A 1
Lu2 Lu 0.38206(10) 0.5000 0.34053(15) 0.0556(9) Uani 0.1493 2 d S TU P A 1
Lu3 Lu 0.29954(19) 0.3924(3) 0.3366(3) 0.0816(11) Uani 0.114 1 d . U P A 1
Lu4 Lu 0.24004(15) 0.5328(3) 0.3570(2) 0.0306(7) Uani 0.1131 1 d . U P A 1
Lu5 Lu 0.23831(16) 0.4399(3) 0.3264(3) 0.0478(10) Uani 0.0926 1 d . U P A 1
Lu6 Lu 0.37234(13) 0.4151(3) 0.3339(2) 0.0465(9) Uani 0.0794 1 d . U P A 1
Lu7 Lu 0.2989(6) 0.5000 0.4146(7) 0.116(3) Uiso 0.0769 2 d S U P A 1
Lu8 Lu 0.2170(6) 0.5000 0.3533(8) 0.081(3) Uani 0.0672 2 d S TU P A 1
Lu9 Lu 0.3155(5) 0.3888(6) 0.2582(4) 0.078(2) Uani 0.0583 1 d . U P A 1
Lu10 Lu 0.3020(3) 0.4547(7) 0.2194(4) 0.085(2) Uani 0.0583 1 d . U P A 1
Lu11 Lu 0.2611(5) 0.5000 0.2051(6) 0.075(3) Uani 0.0536 2 d S TU P A 1
Lu12 Lu 0.2464(10) 0.5000 0.3647(15) 0.078(4) Uani 0.0533 2 d S TU P A 1
Lu13 Lu 0.2646(6) 0.4314(9) 0.3690(6) 0.095(2) Uani 0.0528 1 d . U P A 1
Lu14 Lu 0.3260(5) 0.4219(8) 0.3562(5) 0.0586(19) Uani 0.0375 1 d . U P A 1
Lu15 Lu 0.3425(8) 0.3668(16) 0.3553(12) 0.046(3) Uani 0.0138 1 d . U P A 1
Lu16 Lu 0.3328(7) 0.4374(16) 0.2610(11) 0.063(3) Uani 0.0223 1 d . U P A 1
C1 C 0.3662(2) 0.4284(4) 0.1510(2) 0.133(7) Uani 0.5 1 d G U P A -1
C21 C 0.2014(2) 0.4594(5) 0.1290(2) 0.144(7) Uani 0.5 1 d G U P A -1
C22 C 0.1656(2) 0.5106(5) 0.1503(3) 0.165(7) Uani 0.5 1 d G U P A -1
C2 C 0.40516(19) 0.4856(4) 0.1887(2) 0.106(5) Uani 0.5 1 d G U P A -1
C3 C 0.3850(2) 0.5750(4) 0.1751(2) 0.120(6) Uani 0.5 1 d G U P A -1
C4 C 0.3352(3) 0.5749(4) 0.13189(16) 0.104(6) Uani 0.5 1 d G U P A -1
C5 C 0.3257(3) 0.4844(4) 0.11575(15) 0.133(6) Uani 0.5 1 d G U P A -1
C6 C 0.2808(3) 0.4496(4) 0.10330(16) 0.136(7) Uani 0.5 1 d G U P A -1
C7 C 0.2666(3) 0.3651(4) 0.1242(2) 0.126(6) Uani 0.5 1 d G U P A -1
C8 C 0.3087(2) 0.3080(4) 0.1562(3) 0.128(6) Uani 0.5 1 d G U P A -1
C9 C 0.3640(2) 0.3374(4) 0.1762(3) 0.124(6) Uani 0.5 1 d G U P A -1
C10 C 0.3945(2) 0.3060(4) 0.2385(3) 0.131(7) Uani 0.5 1 d G U P A -1
C11 C 0.42969(16) 0.3663(4) 0.2828(3) 0.135(7) Uani 0.5 1 d G U P A -1
C12 C 0.43803(15) 0.4524(4) 0.2467(3) 0.109(6) Uani 0.5 1 d G U P A -1
C13 C 0.45937(12) 0.5234(4) 0.2985(3) 0.105(6) Uani 0.5 1 d G U P A -1
C14 C 0.44578(15) 0.6131(4) 0.2781(3) 0.092(5) Uani 0.5 1 d G U P A -1
C15 C 0.4085(2) 0.6388(4) 0.2211(2) 0.109(6) Uani 0.5 1 d G U P A -1
C16 C 0.3649(2) 0.7144(4) 0.2089(2) 0.123(6) Uani 0.5 1 d G U P A -1
C17 C 0.3208(3) 0.6990(4) 0.1814(2) 0.128(7) Uani 0.5 1 d G U P A -1
C18 C 0.2991(3) 0.6351(4) 0.13844(18) 0.129(7) Uani 0.5 1 d G U P A -1
C19 C 0.2493(3) 0.6006(4) 0.12318(19) 0.138(7) Uani 0.5 1 d G U P A -1
C20 C 0.2415(3) 0.5115(4) 0.10881(17) 0.141(7) Uani 0.5 1 d G U P A -1
C23 C 0.2186(2) 0.3786(4) 0.1548(2) 0.139(6) Uani 0.5 1 d G U P A -1
C24 C 0.2061(2) 0.3076(4) 0.2055(3) 0.119(6) Uani 0.5 1 d G U P A -1
C25 C 0.2464(2) 0.2506(3) 0.2401(3) 0.105(6) Uani 0.5 1 d G U P A -1
C26 C 0.3029(2) 0.2506(3) 0.2154(3) 0.131(7) Uani 0.5 1 d G U P A -1
C27 C 0.3507(2) 0.2500(3) 0.2640(3) 0.150(7) Uani 0.5 1 d G U P A -1
C28 C 0.3482(2) 0.2367(3) 0.3374(3) 0.160(7) Uani 0.5 1 d G U P A -1
C29 C 0.3872(2) 0.2879(3) 0.3837(3) 0.146(7) Uani 0.5 1 d G U P A -1
C30 C 0.3740(3) 0.3317(4) 0.4561(3) 0.139(7) Uani 0.5 1 d G U P A -1
C31 C 0.4148(2) 0.3999(4) 0.4640(3) 0.128(7) Uani 0.5 1 d G U P A -1
C32 C 0.43132(18) 0.3433(4) 0.3580(3) 0.136(7) Uani 0.5 1 d G U P A -1
C33 C 0.45260(17) 0.4105(4) 0.3976(3) 0.121(7) Uani 0.5 1 d G U P A -1
C34 C 0.46379(12) 0.5094(4) 0.3696(3) 0.110(5) Uani 0.5 1 d G U P A -1
C35 C 0.44815(14) 0.5721(4) 0.4064(3) 0.096(5) Uani 0.5 1 d G U P A -1
C36 C 0.44331(15) 0.6436(4) 0.3441(3) 0.088(5) Uani 0.5 1 d G U P A -1
C37 C 0.40453(18) 0.7117(3) 0.3441(3) 0.083(5) Uani 0.5 1 d G U P A -1
C38 C 0.3845(2) 0.7369(3) 0.2879(3) 0.079(5) Uani 0.5 1 d G U P A -1
C39 C 0.3227(2) 0.7708(3) 0.2825(3) 0.090(5) Uani 0.5 1 d G U P A -1
C40 C 0.2837(2) 0.7386(3) 0.2167(3) 0.124(6) Uani 0.5 1 d G U P A -1
C41 C 0.2346(2) 0.7060(4) 0.2012(3) 0.129(7) Uani 0.5 1 d G U P A -1
C42 C 0.2128(2) 0.6505(4) 0.1531(3) 0.127(7) Uani 0.5 1 d G U P A -1
C43 C 0.1738(2) 0.5934(5) 0.1718(3) 0.120(7) Uani 0.5 1 d G U P A -1
C44 C 0.15118(15) 0.5939(5) 0.2314(3) 0.136(7) Uani 0.5 1 d G U P A -1
C45 C 0.13721(13) 0.5108(5) 0.2464(3) 0.133(5) Uani 0.5 1 d G U P A -1
C46 C 0.15685(16) 0.4522(5) 0.2017(3) 0.133(5) Uani 0.5 1 d G U P A -1
C47 C 0.17029(17) 0.3631(4) 0.2269(3) 0.129(5) Uani 0.5 1 d G U P A -1
C48 C 0.16634(17) 0.3512(4) 0.2971(3) 0.098(5) Uani 0.5 1 d G U P A -1
C49 C 0.2049(2) 0.2864(4) 0.3426(3) 0.106(6) Uani 0.5 1 d G U P A -1
C50 C 0.2465(2) 0.2378(3) 0.3144(3) 0.110(6) Uani 0.5 1 d G U P A -1
C51 C 0.2937(3) 0.2386(3) 0.3645(3) 0.143(7) Uani 0.5 1 d G U P A -1
C52 C 0.2812(3) 0.2837(4) 0.4296(3) 0.135(7) Uani 0.5 1 d G U P A -1
C53 C 0.3192(3) 0.3314(4) 0.4766(2) 0.134(7) Uani 0.5 1 d G U P A -1
C54 C 0.3021(3) 0.4144(4) 0.50156(17) 0.133(7) Uani 0.5 1 d G U P A -1
C55 C 0.3435(3) 0.4837(4) 0.51363(15) 0.106(6) Uani 0.5 1 d G U P A -1
C56 C 0.3962(2) 0.4818(4) 0.4918(2) 0.119(6) Uani 0.5 1 d G U P A -1
C57 C 0.41920(18) 0.5582(4) 0.4596(2) 0.099(6) Uani 0.5 1 d G U P A -1
C58 C 0.3840(2) 0.6360(4) 0.4632(2) 0.099(6) Uani 0.5 1 d G U P A -1
C59 C 0.3715(2) 0.7180(3) 0.4094(2) 0.071(4) Uani 0.5 1 d G U P A -1
C60 C 0.3213(2) 0.7462(3) 0.3959(3) 0.070(4) Uani 0.5 1 d G U P A -1
C61 C 0.2954(2) 0.7671(3) 0.3271(3) 0.078(5) Uani 0.5 1 d G U P A -1
C62 C 0.2388(2) 0.7415(3) 0.3206(3) 0.113(6) Uani 0.5 1 d G U P A -1
C63 C 0.2124(2) 0.7170(4) 0.2578(3) 0.126(6) Uani 0.5 1 d G U P A -1
C64 C 0.16835(17) 0.6648(4) 0.2659(3) 0.120(6) Uani 0.5 1 d G U P A -1
C65 C 0.16731(15) 0.6486(4) 0.3356(3) 0.123(6) Uani 0.5 1 d G U P A -1
C66 C 0.14805(13) 0.5622(5) 0.3558(3) 0.138(7) Uani 0.5 1 d G U P A -1
C67 C 0.13762(11) 0.4991(5) 0.3151(3) 0.127(5) Uani 0.5 1 d G U P A -1
C68 C 0.14845(15) 0.4141(5) 0.3395(3) 0.111(6) Uani 0.5 1 d G U P A -1
C69 C 0.16822(18) 0.4374(5) 0.4056(3) 0.132(6) Uani 0.5 1 d G U P A -1
C70 C 0.2064(2) 0.3867(5) 0.4492(3) 0.138(7) Uani 0.5 1 d G U P A -1
C71 C 0.2258(2) 0.3105(4) 0.4143(3) 0.119(6) Uani 0.5 1 d G U P A -1
C72 C 0.2465(3) 0.4327(5) 0.4912(2) 0.123(6) Uani 0.5 1 d G U P A -1
C73 C 0.2511(2) 0.5290(5) 0.49652(19) 0.132(7) Uani 0.5 1 d G U P A -1
C74 C 0.3107(2) 0.5618(4) 0.51083(15) 0.132(7) Uani 0.5 1 d G U P A -1
C75 C 0.3341(2) 0.6412(4) 0.48872(18) 0.109(6) Uani 0.5 1 d G U P A -1
C76 C 0.2889(2) 0.7023(4) 0.4434(2) 0.108(6) Uani 0.5 1 d G U P A -1
C77 C 0.2360(2) 0.6635(4) 0.4332(3) 0.131(7) Uani 0.5 1 d G U P A -1
C78 C 0.20926(18) 0.6972(4) 0.3695(3) 0.133(7) Uani 0.5 1 d G U P A -1
C79 C 0.2123(2) 0.5802(5) 0.4574(3) 0.142(7) Uani 0.5 1 d G U P A -1
C80 C 0.16990(17) 0.5321(5) 0.4230(3) 0.141(7) Uani 0.5 1 d G U P A -1
C81 C 0.5915(3) 0.3525(5) 0.3465(3) 0.0450(16) Uani 1 1 d . U . B 2
H81A H 0.5628 0.3208 0.3228 0.067 Uiso 1 1 calc R U . B 2
H81B H 0.5774 0.3990 0.3731 0.067 Uiso 1 1 calc R U . B 2
H81C H 0.6121 0.3127 0.3758 0.067 Uiso 1 1 calc R U . B 2
N3 N 0.4233(2) 0.5000 0.0119(3) 0.0219(12) Uani 1 2 d S T P B 2
N2 N 0.47957(15) 0.3699(3) 0.0848(2) 0.0223(9) Uani 1 1 d . . . B 2
N1 N 0.5366(2) 0.5000 0.1583(3) 0.0215(12) Uani 1 2 d S T P B 2
Ni1 Ni 0.48083(3) 0.5000 0.08382(4) 0.0191(3) Uani 1 2 d S T P B 2
C82 C 0.6272(2) 0.3928(4) 0.2947(3) 0.0356(13) Uani 1 1 d . U . B 2
H82A H 0.6563 0.4244 0.3188 0.043 Uiso 1 1 calc R U . B 2
H82B H 0.6423 0.3454 0.2690 0.043 Uiso 1 1 calc R U . B 2
C83 C 0.5975(2) 0.4553(4) 0.2461(3) 0.0282(11) Uani 1 1 d . U . B 2
C84 C 0.55984(18) 0.4281(3) 0.1916(3) 0.0230(10) Uani 1 1 d . U . B 2
C85 C 0.5490(2) 0.3414(4) 0.1757(3) 0.0262(11) Uani 1 1 d . U . B 2
H85 H 0.5689 0.2980 0.1994 0.031 Uiso 1 1 calc R U . B 2
C86 C 0.51047(19) 0.3141(3) 0.1268(3) 0.0257(11) Uani 1 1 d . U . B 2
C87 C 0.4970(2) 0.2227(4) 0.1133(3) 0.0298(12) Uani 1 1 d . U . B 2
C88 C 0.5217(3) 0.1453(4) 0.1522(4) 0.0419(15) Uani 1 1 d . U . B 2
H88A H 0.5599 0.1538 0.1578 0.050 Uiso 1 1 calc R U . B 2
H88B H 0.5149 0.0917 0.1259 0.050 Uiso 1 1 calc R U . B 2
C89 C 0.5003(3) 0.1334(5) 0.2222(4) 0.057(2) Uani 1 1 d . U . B 2
H89A H 0.4624 0.1259 0.2172 0.086 Uiso 1 1 calc R U . B 2
H89B H 0.5089 0.1847 0.2496 0.086 Uiso 1 1 calc R U . B 2
H89C H 0.5163 0.0819 0.2439 0.086 Uiso 1 1 calc R U . B 2
C90 C 0.4578(2) 0.2228(4) 0.0626(3) 0.0285(11) Uani 1 1 d . U . B 2
C91 C 0.4281(2) 0.1459(4) 0.0296(4) 0.0383(14) Uani 1 1 d . U . B 2
H91A H 0.4490 0.0925 0.0378 0.046 Uiso 1 1 calc R U . B 2
H91B H 0.4243 0.1555 -0.0192 0.046 Uiso 1 1 calc R U . B 2
C92 C 0.3732(3) 0.1318(5) 0.0552(4) 0.0483(17) Uani 1 1 d . U . B 2
H92A H 0.3522 0.1843 0.0470 0.072 Uiso 1 1 calc R U . B 2
H92B H 0.3767 0.1196 0.1032 0.072 Uiso 1 1 calc R U . B 2
H92C H 0.3561 0.0827 0.0316 0.072 Uiso 1 1 calc R U . B 2
C93 C 0.44766(19) 0.3141(4) 0.0453(3) 0.0249(11) Uani 1 1 d . U . B 2
C94 C 0.40917(19) 0.3417(4) -0.0039(3) 0.0244(11) Uani 1 1 d . U . B 2
H94 H 0.3899 0.2984 -0.0285 0.029 Uiso 1 1 calc R U . B 2
C95 C 0.39764(18) 0.4275(4) -0.0186(3) 0.0231(10) Uani 1 1 d . U . B 2
C96 C 0.35526(19) 0.4553(4) -0.0677(3) 0.0262(11) Uani 1 1 d . U . B 2
C97 C 0.3174(2) 0.3937(4) -0.1058(3) 0.0313(12) Uani 1 1 d . U . B 2
H97A H 0.3367 0.3421 -0.1199 0.038 Uiso 1 1 calc R U . B 2
H97B H 0.3022 0.4231 -0.1465 0.038 Uiso 1 1 calc R U . B 2
C98 C 0.2724(2) 0.3637(5) -0.0628(4) 0.0475(17) Uani 1 1 d . U . B 2
H98A H 0.2542 0.4147 -0.0468 0.071 Uiso 1 1 calc R U . B 2
H98B H 0.2870 0.3300 -0.0245 0.071 Uiso 1 1 calc R U . B 2
H98C H 0.2477 0.3277 -0.0900 0.071 Uiso 1 1 calc R U . B 2
C105 C 0.3614(5) 0.0000 0.2380(6) 0.059(3) Uani 1 2 d S TU P C 4
H105 H 0.3869 0.0000 0.2062 0.071 Uiso 1 2 calc R U P C 4
C106 C 0.3093(4) 0.0000 0.2154(5) 0.044(2) Uani 1 2 d S TU P C 4
H106 H 0.2987 0.0000 0.1692 0.053 Uiso 1 2 calc R U P C 4
C107 C 0.2717(4) 0.0000 0.2656(5) 0.050(2) Uani 1 2 d S TU P C 4
H107 H 0.2358 0.0000 0.2508 0.060 Uiso 1 2 calc R U P C 4
C108 C 0.2842(5) 0.0000 0.3336(5) 0.052(2) Uani 1 2 d S TU P C 4
H108 H 0.2584 0.0000 0.3650 0.063 Uiso 1 2 calc R U P C 4
C109 C 0.3394(6) 0.0000 0.3537(7) 0.081(4) Uani 1 2 d S TU P C 4
H109 H 0.3504 0.0000 0.3998 0.097 Uiso 1 2 calc R U P C 4
C110 C 0.3778(6) 0.0000 0.3051(7) 0.082(4) Uani 1 2 d S TU P C 4
H110 H 0.4139 0.0000 0.3188 0.098 Uiso 1 2 calc R U P C 4
C99 C 0.5133(11) 0.1824(18) 0.5456(10) 0.182(10) Uani 0.5 1 d G U P D -3
H99 H 0.5262 0.2085 0.5863 0.218 Uiso 0.5 1 calc R U P D -3
C100 C 0.5433(8) 0.1855(16) 0.4891(12) 0.162(9) Uani 0.5 1 d G U P D -3
H100 H 0.5763 0.2135 0.4920 0.194 Uiso 0.5 1 calc R U P D -3
C101 C 0.5241(8) 0.1465(16) 0.4282(11) 0.100(7) Uani 0.5 1 d G U P D -3
H101 H 0.5441 0.1485 0.3904 0.120 Uiso 0.5 1 calc R U P D -3
C102 C 0.4748(9) 0.1045(15) 0.4239(11) 0.141(8) Uani 0.5 1 d G U P D -3
H102 H 0.4619 0.0785 0.3832 0.169 Uiso 0.5 1 calc R U P D -3
C103 C 0.4448(8) 0.1015(16) 0.4804(13) 0.155(9) Uani 0.5 1 d G U P D -3
H103 H 0.4119 0.0734 0.4775 0.186 Uiso 0.5 1 calc R U P D -3
C104 C 0.4641(11) 0.1404(19) 0.5412(11) 0.151(10) Uani 0.5 1 d G U P D -3
H104 H 0.4440 0.1384 0.5790 0.181 Uiso 0.5 1 calc R U P D -3


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu9 0.885(9) . ?
Lu1 Lu16 1.05(2) . ?
Lu1 Lu6 1.228(5) . ?
Lu1 Lu15 1.29(2) . ?
Lu1 Lu3 1.440(5) . ?
Lu1 Lu14 1.502(12) . ?
Lu1 Lu10 1.998(9) . ?
Lu1 C27 2.065(5) . ?
Lu1 C10 2.087(4) . ?
Lu1 C11 2.260(4) . ?
Lu1 Lu2 2.261(3) . ?
Lu1 C28 2.364(5) . ?
Lu2 Lu6 1.311(4) . ?
Lu2 Lu6 1.311(4) 6_565 ?
Lu2 Lu14 1.883(12) 6_565 ?
Lu2 Lu14 1.883(12) . ?
Lu2 C34 2.101(4) . ?
Lu2 Lu16 2.15(2) . ?
Lu2 Lu16 2.15(2) 6_565 ?
Lu2 C13 2.198(4) . ?
Lu2 Lu1 2.261(3) 6_565 ?
Lu2 Lu15 2.27(2) 6_565 ?
Lu2 Lu15 2.27(2) . ?
Lu3 Lu14 0.868(11) . ?
Lu3 Lu15 1.18(2) . ?
Lu3 Lu13 1.267(14) . ?
Lu3 Lu9 1.626(10) . ?
Lu3 Lu5 1.699(6) . ?
Lu3 Lu6 1.870(6) . ?
Lu3 Lu16 1.89(2) . ?
Lu3 Lu4 1.942(6) 6_565 ?
Lu3 Lu12 2.200(17) . ?
Lu3 Lu7 2.236(11) . ?
Lu3 C51 2.393(6) . ?
Lu4 Lu12 0.539(11) . ?
Lu4 Lu5 0.730(5) 6_565 ?
Lu4 Lu8 0.762(10) . ?
Lu4 Lu13 0.843(14) 6_565 ?
Lu4 Lu4 0.989(9) 6_565 ?
Lu4 Lu5 1.526(8) . ?
Lu4 Lu13 1.661(15) . ?
Lu4 Lu7 1.867(14) . ?
Lu4 Lu3 1.942(6) 6_565 ?
Lu4 C79 2.260(5) . ?
Lu4 C80 2.268(5) . ?
Lu4 Lu14 2.272(12) 6_565 ?
Lu5 Lu4 0.730(5) 6_565 ?
Lu5 Lu13 1.039(15) . ?
Lu5 Lu12 1.189(19) . ?
Lu5 Lu8 1.198(10) . ?
Lu5 Lu5 1.816(10) 6_565 ?
Lu5 Lu13 2.200(14) 6_565 ?
Lu5 Lu14 2.260(12) . ?
Lu5 C48 2.293(6) . ?
Lu5 C68 2.329(5) . ?
Lu5 Lu7 2.405(14) . ?
Lu6 Lu15 1.15(2) . ?
Lu6 Lu14 1.281(12) . ?
Lu6 Lu16 1.72(2) . ?
Lu6 C32 1.871(5) . ?
Lu6 C11 1.964(5) . ?
Lu6 Lu9 2.030(11) . ?
Lu6 C29 2.176(6) . ?
Lu6 C33 2.302(5) . ?
Lu6 C12 2.534(6) . ?
Lu7 Lu13 1.585(17) . ?
Lu7 Lu13 1.585(17) 6_565 ?
Lu7 Lu12 1.59(3) . ?
Lu7 Lu14 1.814(16) . ?
Lu7 Lu14 1.814(16) 6_565 ?
Lu7 Lu4 1.867(14) 6_565 ?
Lu7 C74 2.115(13) . ?
Lu7 C73 2.129(14) . ?
Lu7 C54 2.143(12) . ?
Lu7 C55 2.193(14) . ?
Lu7 Lu3 2.236(11) 6_565 ?
Lu8 Lu12 0.76(3) . ?
Lu8 Lu4 0.762(10) 6_565 ?
Lu8 Lu5 1.198(10) 6_565 ?
Lu8 Lu13 1.598(18) . ?
Lu8 Lu13 1.598(18) 6_565 ?
Lu8 C69 1.910(12) . ?
Lu8 C80 1.939(13) . ?
Lu8 C66 1.978(14) . ?
Lu8 C67 2.084(16) . ?
Lu8 C68 2.161(13) . ?
Lu9 Lu16 0.85(2) . ?
Lu9 Lu10 1.286(13) . ?
Lu9 Lu14 1.994(14) . ?
Lu9 Lu15 2.01(2) . ?
Lu9 C9 2.232(9) . ?
Lu9 C26 2.264(10) . ?
Lu9 C27 2.275(10) . ?
Lu9 C8 2.344(8) . ?
Lu9 Lu11 2.363(12) . ?
Lu10 Lu16 1.12(2) . ?
Lu10 Lu11 1.251(13) . ?
Lu10 Lu10 1.37(2) 6_565 ?
Lu10 Lu16 1.96(3) 6_565 ?
Lu10 C1 2.213(8) . ?
Lu10 C5 2.213(8) . ?
Lu10 C6 2.311(8) . ?
Lu10 C7 2.427(9) . ?
Lu10 Lu9 2.500(14) 6_565 ?
Lu11 Lu10 1.251(13) 6_565 ?
Lu11 C20 1.932(11) . ?
Lu11 C21 2.134(10) . ?
Lu11 C19 2.220(9) . ?
Lu11 C6 2.233(13) . ?
Lu11 Lu16 2.25(2) 6_565 ?
Lu11 Lu16 2.25(2) . ?
Lu11 C23 2.309(7) . ?
Lu11 Lu9 2.363(12) 6_565 ?
Lu11 C5 2.492(15) . ?
Lu12 Lu4 0.539(11) 6_565 ?
Lu12 Lu13 1.133(18) . ?
Lu12 Lu13 1.133(18) 6_565 ?
Lu12 Lu5 1.189(19) 6_565 ?
Lu12 Lu3 2.200(17) 6_565 ?
Lu12 Lu14 2.34(2) . ?
Lu12 Lu14 2.34(2) 6_565 ?
Lu13 Lu4 0.843(14) 6_565 ?
Lu13 Lu14 1.589(17) . ?
Lu13 Lu13 2.07(3) 6_565 ?
Lu13 Lu5 2.200(14) 6_565 ?
Lu13 Lu15 2.22(3) . ?
Lu13 C71 2.283(11) . ?
Lu14 Lu15 0.93(2) . ?
Lu14 Lu16 1.91(2) . ?
Lu14 Lu4 2.272(12) 6_565 ?
Lu15 C29 1.71(2) . ?
Lu15 C28 2.00(3) . ?
Lu15 Lu16 2.14(3) . ?
Lu15 C30 2.15(2) . ?
Lu15 C32 2.26(2) . ?
Lu16 Lu16 1.89(5) 6_565 ?
Lu16 Lu10 1.96(3) 6_565 ?
Lu16 C1 2.38(2) . ?
C1 C5 1.4610 . ?
C1 C9 1.4623 . ?
C1 C2 1.4675 . ?
C21 C22 1.2802 . ?
C21 C20 1.3631 . ?
C21 C23 1.3795 . ?
C21 C46 1.8839 . ?
C22 C43 1.3319 . ?
C22 C46 1.3717 . ?
C2 C12 1.4503 . ?
C2 C3 1.4601 . ?
C3 C15 1.4208 . ?
C3 C4 1.4640 . ?
C4 C18 1.2985 . ?
C4 C5 1.4204 . ?
C5 C6 1.2546 . ?
C6 C20 1.3703 . ?
C6 C7 1.3942 . ?
C7 C23 1.4040 . ?
C7 C8 1.4727 . ?
C8 C26 1.4674 . ?
C8 C9 1.4862 . ?
C9 C10 1.4785 . ?
C10 C11 1.5033 . ?
C10 C27 1.5048 . ?
C11 C12 1.5050 . ?
C11 C32 1.5186 . ?
C12 C13 1.5494 . ?
C13 C34 1.4113 . ?
C13 C14 1.4475 . ?
C14 C36 1.3832 . ?
C14 C15 1.4632 . ?
C15 C16 1.5901 . ?
C16 C17 1.2240 . ?
C16 C38 1.6323 . ?
C17 C40 1.3447 . ?
C17 C18 1.3707 . ?
C18 C19 1.3707 . ?
C19 C42 1.3549 . ?
C19 C20 1.3866 . ?
C23 C24 1.5134 . ?
C23 C47 1.9508 . ?
C24 C47 1.3217 . ?
C24 C25 1.4622 . ?
C25 C50 1.4772 . ?
C25 C26 1.5369 . ?
C26 C27 1.4834 . ?
C27 C28 1.4654 . ?
C28 C29 1.5033 . ?
C28 C51 1.5095 . ?
C29 C32 1.5074 . ?
C29 C30 1.6291 . ?
C30 C31 1.4533 . ?
C30 C53 1.4674 . ?
C31 C56 1.4440 . ?
C31 C33 1.6807 . ?
C32 C33 1.3659 . ?
C33 C34 1.6236 . ?
C34 C35 1.2735 . ?
C35 C57 1.3345 . ?
C35 C36 1.6335 . ?
C36 C37 1.4173 . ?
C37 C38 1.2429 . ?
C37 C59 1.5853 . ?
C38 C39 1.6338 . ?
C39 C61 1.1544 . ?
C39 C40 1.6443 . ?
C40 C41 1.3450 . ?
C41 C63 1.2938 . ?
C41 C42 1.3501 . ?
C42 C43 1.3777 . ?
C43 C44 1.3417 . ?
C44 C64 1.3231 . ?
C44 C45 1.3422 . ?
C45 C67 1.3643 . ?
C45 C46 1.3654 . ?
C46 C47 1.4652 . ?
C47 C48 1.4047 . ?
C48 C68 1.3625 . ?
C48 C49 1.6046 . ?
C49 C50 1.4251 . ?
C49 C71 1.5139 . ?
C50 C51 1.4881 . ?
C51 C52 1.5049 . ?
C52 C71 1.4621 . ?
C52 C53 1.4719 . ?
C53 C54 1.4242 . ?
C54 C72 1.4267 . ?
C54 C55 1.4841 . ?
C55 C56 1.4265 . ?
C55 C74 1.4380 . ?
C56 C57 1.4562 . ?
C57 C58 1.4777 . ?
C58 C75 1.3880 . ?
C58 C59 1.6440 . ?
C59 C60 1.3417 . ?
C60 C76 1.4467 . ?
C60 C61 1.4958 . ?
C61 C62 1.4750 . ?
C62 C63 1.4087 . ?
C62 C78 1.4253 . ?
C63 C64 1.3806 . ?
C64 C65 1.3954 . ?
C65 C78 1.4142 . ?
C65 C66 1.4584 . ?
C66 C67 1.2596 . ?
C66 C80 1.4684 . ?
C67 C68 1.3916 . ?
C68 C69 1.4046 . ?
C69 C70 1.4581 . ?
C69 C80 1.4697 . ?
C70 C72 1.4379 . ?
C70 C71 1.4446 . ?
C72 C73 1.4623 . ?
C73 C79 1.4266 . ?
C73 C74 1.5868 . ?
C74 C75 1.4187 . ?
C75 C76 1.6733 . ?
C76 C77 1.4544 . ?
C77 C78 1.4713 . ?
C77 C79 1.4863 . ?
C79 C80 1.4211 . ?
C81 C82 1.533(9) . ?
N3 C95 1.386(6) 6_565 ?
N3 C95 1.386(6) . ?
N3 Ni1 1.951(6) . ?
N2 C93 1.368(7) . ?
N2 C86 1.380(7) . ?
N2 Ni1 1.965(4) . ?
N1 C84 1.378(6) . ?
N1 C84 1.378(6) 6_565 ?
N1 Ni1 1.956(6) . ?
Ni1 N2 1.965(4) 6_565 ?
C82 C83 1.502(7) . ?
C83 C83 1.351(12) 6_565 ?
C83 C84 1.440(7) . ?
C84 C85 1.369(8) . ?
C85 C86 1.380(7) . ?
C86 C87 1.441(7) . ?
C87 C90 1.353(8) . ?
C87 C88 1.507(8) . ?
C88 C89 1.526(11) . ?
C90 C93 1.439(8) . ?
C90 C91 1.503(8) . ?
C91 C92 1.521(9) . ?
C93 C94 1.383(7) . ?
C94 C95 1.354(8) . ?
C95 C96 1.450(7) . ?
C96 C96 1.350(11) 6_565 ?
C96 C97 1.495(7) . ?
C97 C98 1.532(8) . ?
C105 C110 1.355(18) . ?
C105 C106 1.355(15) . ?
C106 C107 1.418(15) . ?
C107 C108 1.352(14) . ?
C108 C109 1.415(19) . ?
C109 C110 1.41(2) . ?
C99 C100 1.3900 . ?
C99 C104 1.3900 . ?
C100 C101 1.3900 . ?
C101 C102 1.3900 . ?
C102 C103 1.3900 . ?
C103 C104 1.3900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu9 Lu1 Lu16 51.5(11) . . ?
Lu9 Lu1 Lu6 147.4(7) . . ?
Lu16 Lu1 Lu6 97.9(12) . . ?
Lu9 Lu1 Lu15 135.0(12) . . ?
Lu16 Lu1 Lu15 132.8(16) . . ?
Lu6 Lu1 Lu15 54.3(10) . . ?
Lu9 Lu1 Lu3 85.2(7) . . ?
Lu16 Lu1 Lu3 97.4(10) . . ?
Lu6 Lu1 Lu3 88.6(3) . . ?
Lu15 Lu1 Lu3 51.0(10) . . ?
Lu9 Lu1 Lu14 110.6(7) . . ?
Lu16 Lu1 Lu14 95.4(12) . . ?
Lu6 Lu1 Lu14 54.9(5) . . ?
Lu15 Lu1 Lu14 38.0(11) . . ?
Lu3 Lu1 Lu14 34.2(4) . . ?
Lu9 Lu1 Lu10 28.0(7) . . ?
Lu16 Lu1 Lu10 23.5(12) . . ?
Lu6 Lu1 Lu10 120.7(4) . . ?
Lu15 Lu1 Lu10 139.9(11) . . ?
Lu3 Lu1 Lu10 91.8(3) . . ?
Lu14 Lu1 Lu10 103.4(5) . . ?
Lu9 Lu1 C27 92.0(6) . . ?
Lu16 Lu1 C27 131.1(13) . . ?
Lu6 Lu1 C27 119.8(3) . . ?
Lu15 Lu1 C27 95.7(11) . . ?
Lu3 Lu1 C27 112.4(3) . . ?
Lu14 Lu1 C27 131.0(5) . . ?
Lu10 Lu1 C27 114.5(3) . . ?
Lu9 Lu1 C10 100.1(6) . . ?
Lu16 Lu1 C10 105.8(11) . . ?
Lu6 Lu1 C10 99.5(3) . . ?
Lu15 Lu1 C10 115.2(11) . . ?
Lu3 Lu1 C10 154.0(3) . . ?
Lu14 Lu1 C10 149.2(5) . . ?
Lu10 Lu1 C10 104.9(3) . . ?
C27 Lu1 C10 42.50(9) . . ?
Lu9 Lu1 C11 129.2(7) . . ?
Lu16 Lu1 C11 101.4(10) . . ?
Lu6 Lu1 C11 60.2(2) . . ?
Lu15 Lu1 C11 95.5(10) . . ?
Lu3 Lu1 C11 145.3(3) . . ?
Lu14 Lu1 C11 114.4(5) . . ?
Lu10 Lu1 C11 116.3(3) . . ?
C27 Lu1 C11 75.71(14) . . ?
C10 Lu1 C11 40.22(8) . . ?
Lu9 Lu1 Lu2 119.6(6) . . ?
Lu16 Lu1 Lu2 70.3(12) . . ?
Lu6 Lu1 Lu2 28.0(2) . . ?
Lu15 Lu1 Lu2 74.0(11) . . ?
Lu3 Lu1 Lu2 87.9(2) . . ?
Lu14 Lu1 Lu2 55.8(5) . . ?
Lu10 Lu1 Lu2 92.7(3) . . ?
C27 Lu1 Lu2 144.5(2) . . ?
C10 Lu1 Lu2 110.75(19) . . ?
C11 Lu1 Lu2 71.70(16) . . ?
Lu9 Lu1 C28 115.9(7) . . ?
Lu16 Lu1 C28 166.7(13) . . ?
Lu6 Lu1 C28 95.3(3) . . ?
Lu15 Lu1 C28 57.9(11) . . ?
Lu3 Lu1 C28 84.7(2) . . ?
Lu14 Lu1 C28 93.6(5) . . ?
Lu10 Lu1 C28 143.8(3) . . ?
C27 Lu1 C28 37.89(9) . . ?
C10 Lu1 C28 70.06(14) . . ?
C11 Lu1 C28 83.65(16) . . ?
Lu2 Lu1 C28 123.0(2) . . ?
Lu6 Lu2 Lu6 156.3(4) . 6_565 ?
Lu6 Lu2 Lu14 119.5(4) . 6_565 ?
Lu6 Lu2 Lu14 42.8(4) 6_565 6_565 ?
Lu6 Lu2 Lu14 42.8(4) . . ?
Lu6 Lu2 Lu14 119.5(4) 6_565 . ?
Lu14 Lu2 Lu14 77.6(7) 6_565 . ?
Lu6 Lu2 C34 105.4(3) . . ?
Lu6 Lu2 C34 97.7(3) 6_565 . ?
Lu14 Lu2 C34 130.1(4) 6_565 . ?
Lu14 Lu2 C34 136.8(4) . . ?
Lu6 Lu2 Lu16 53.3(7) . . ?
Lu6 Lu2 Lu16 105.3(7) 6_565 . ?
Lu14 Lu2 Lu16 89.7(6) 6_565 . ?
Lu14 Lu2 Lu16 56.2(6) . . ?
C34 Lu2 Lu16 137.0(5) . . ?
Lu6 Lu2 Lu16 105.3(7) . 6_565 ?
Lu6 Lu2 Lu16 53.3(7) 6_565 6_565 ?
Lu14 Lu2 Lu16 56.2(6) 6_565 6_565 ?
Lu14 Lu2 Lu16 89.7(6) . 6_565 ?
C34 Lu2 Lu16 132.3(6) . 6_565 ?
Lu16 Lu2 Lu16 52.3(13) . 6_565 ?
Lu6 Lu2 C13 106.5(3) . . ?
Lu6 Lu2 C13 88.3(3) 6_565 . ?
Lu14 Lu2 C13 131.0(4) 6_565 . ?
Lu14 Lu2 C13 149.1(4) . . ?
C34 Lu2 C13 38.24(7) . . ?
Lu16 Lu2 C13 106.1(5) . . ?
Lu16 Lu2 C13 97.8(5) 6_565 . ?
Lu6 Lu2 Lu1 131.3(2) . 6_565 ?
Lu6 Lu2 Lu1 26.13(19) 6_565 6_565 ?
Lu14 Lu2 Lu1 41.3(4) 6_565 6_565 ?
Lu14 Lu2 Lu1 104.2(3) . 6_565 ?
C34 Lu2 Lu1 118.2(2) . 6_565 ?
Lu16 Lu2 Lu1 79.2(6) . 6_565 ?
Lu16 Lu2 Lu1 27.4(6) 6_565 6_565 ?
C13 Lu2 Lu1 95.64(19) . 6_565 ?
Lu6 Lu2 Lu1 26.13(19) . . ?
Lu6 Lu2 Lu1 131.3(2) 6_565 . ?
Lu14 Lu2 Lu1 104.2(3) 6_565 . ?
Lu14 Lu2 Lu1 41.3(4) . . ?
C34 Lu2 Lu1 125.38(19) . . ?
Lu16 Lu2 Lu1 27.4(6) . . ?
Lu16 Lu2 Lu1 79.2(6) 6_565 . ?
C13 Lu2 Lu1 110.73(18) . . ?
Lu1 Lu2 Lu1 105.41(17) 6_565 . ?
Lu6 Lu2 Lu15 143.0(6) . 6_565 ?
Lu6 Lu2 Lu15 21.0(7) 6_565 6_565 ?
Lu14 Lu2 Lu15 23.6(6) 6_565 6_565 ?
Lu14 Lu2 Lu15 101.1(8) . 6_565 ?
C34 Lu2 Lu15 109.6(5) . 6_565 ?
Lu16 Lu2 Lu15 104.4(8) . 6_565 ?
Lu16 Lu2 Lu15 57.9(8) 6_565 6_565 ?
C13 Lu2 Lu15 108.3(6) . 6_565 ?
Lu1 Lu2 Lu15 33.0(6) 6_565 6_565 ?
Lu1 Lu2 Lu15 124.7(5) . 6_565 ?
Lu6 Lu2 Lu15 20.9(7) . . ?
Lu6 Lu2 Lu15 143.0(6) 6_565 . ?
Lu14 Lu2 Lu15 101.1(8) 6_565 . ?
Lu14 Lu2 Lu15 23.6(6) . . ?
C34 Lu2 Lu15 117.0(6) . . ?
Lu16 Lu2 Lu15 57.9(8) . . ?
Lu16 Lu2 Lu15 104.3(8) 6_565 . ?
C13 Lu2 Lu15 126.8(6) . . ?
Lu1 Lu2 Lu15 124.7(5) 6_565 . ?
Lu1 Lu2 Lu15 33.0(6) . . ?
Lu15 Lu2 Lu15 124.5(12) 6_565 . ?
Lu14 Lu3 Lu15 51.2(13) . . ?
Lu14 Lu3 Lu13 94.4(11) . . ?
Lu15 Lu3 Lu13 130.4(15) . . ?
Lu14 Lu3 Lu1 76.8(8) . . ?
Lu15 Lu3 Lu1 57.7(12) . . ?
Lu13 Lu3 Lu1 158.8(6) . . ?
Lu14 Lu3 Lu9 101.9(9) . . ?
Lu15 Lu3 Lu9 90.1(13) . . ?
Lu13 Lu3 Lu9 136.2(8) . . ?
Lu1 Lu3 Lu9 32.8(4) . . ?
Lu14 Lu3 Lu5 119.8(9) . . ?
Lu15 Lu3 Lu5 167.7(14) . . ?
Lu13 Lu3 Lu5 37.5(7) . . ?
Lu1 Lu3 Lu5 132.1(4) . . ?
Lu9 Lu3 Lu5 100.8(5) . . ?
Lu14 Lu3 Lu6 36.5(8) . . ?
Lu15 Lu3 Lu6 36.1(12) . . ?
Lu13 Lu3 Lu6 130.3(7) . . ?
Lu1 Lu3 Lu6 41.1(2) . . ?
Lu9 Lu3 Lu6 70.6(5) . . ?
Lu5 Lu3 Lu6 143.4(3) . . ?
Lu14 Lu3 Lu16 78.3(10) . . ?
Lu15 Lu3 Lu16 85.2(14) . . ?
Lu13 Lu3 Lu16 126.4(9) . . ?
Lu1 Lu3 Lu16 33.4(7) . . ?
Lu9 Lu3 Lu16 26.8(6) . . ?
Lu5 Lu3 Lu16 101.8(7) . . ?
Lu6 Lu3 Lu16 54.5(6) . . ?
Lu14 Lu3 Lu4 100.9(9) . 6_565 ?
Lu15 Lu3 Lu4 145.9(13) . 6_565 ?
Lu13 Lu3 Lu4 18.6(6) . 6_565 ?
Lu1 Lu3 Lu4 143.7(3) . 6_565 ?
Lu9 Lu3 Lu4 117.7(4) . 6_565 ?
Lu5 Lu3 Lu4 21.84(18) . 6_565 ?
Lu6 Lu3 Lu4 132.3(3) . 6_565 ?
Lu16 Lu3 Lu4 110.3(7) . 6_565 ?
Lu14 Lu3 Lu12 88.3(11) . . ?
Lu15 Lu3 Lu12 136.2(15) . . ?
Lu13 Lu3 Lu12 22.2(8) . . ?
Lu1 Lu3 Lu12 136.8(6) . . ?
Lu9 Lu3 Lu12 117.4(8) . . ?
Lu5 Lu3 Lu12 32.4(7) . . ?
Lu6 Lu3 Lu12 119.2(6) . . ?
Lu16 Lu3 Lu12 104.2(9) . . ?
Lu4 Lu3 Lu12 13.1(5) 6_565 . ?
Lu14 Lu3 Lu7 50.6(9) . . ?
Lu15 Lu3 Lu7 94.3(13) . . ?
Lu13 Lu3 Lu7 43.8(7) . . ?
Lu1 Lu3 Lu7 124.0(4) . . ?
Lu9 Lu3 Lu7 133.8(5) . . ?
Lu5 Lu3 Lu7 73.9(4) . . ?
Lu6 Lu3 Lu7 86.7(4) . . ?
Lu16 Lu3 Lu7 107.8(8) . . ?
Lu4 Lu3 Lu7 52.5(4) 6_565 . ?
Lu12 Lu3 Lu7 41.9(8) . . ?
Lu14 Lu3 C51 117.0(9) . . ?
Lu15 Lu3 C51 71.4(12) . . ?
Lu13 Lu3 C51 106.2(6) . . ?
Lu1 Lu3 C51 94.9(3) . . ?
Lu9 Lu3 C51 102.0(4) . . ?
Lu5 Lu3 C51 111.5(3) . . ?
Lu6 Lu3 C51 105.1(3) . . ?
Lu16 Lu3 C51 124.6(8) . . ?
Lu4 Lu3 C51 117.1(3) 6_565 . ?
Lu12 Lu3 C51 127.6(6) . . ?
Lu7 Lu3 C51 123.0(4) . . ?
Lu12 Lu4 Lu5 139(3) . 6_565 ?
Lu12 Lu4 Lu8 69(3) . . ?
Lu5 Lu4 Lu8 106.8(13) 6_565 . ?
Lu12 Lu4 Lu13 108(3) . 6_565 ?
Lu5 Lu4 Lu13 82.3(11) 6_565 6_565 ?
Lu8 Lu4 Lu13 169.2(15) . 6_565 ?
Lu12 Lu4 Lu4 23(3) . 6_565 ?
Lu5 Lu4 Lu4 124.5(5) 6_565 6_565 ?
Lu8 Lu4 Lu4 49.5(8) . 6_565 ?
Lu13 Lu4 Lu4 129.9(10) 6_565 6_565 ?
Lu12 Lu4 Lu5 43(3) . . ?
Lu5 Lu4 Lu5 101.3(6) 6_565 . ?
Lu8 Lu4 Lu5 50.6(9) . . ?
Lu13 Lu4 Lu5 134.4(9) 6_565 . ?
Lu4 Lu4 Lu5 23.21(19) 6_565 . ?
Lu12 Lu4 Lu13 9(3) . . ?
Lu5 Lu4 Lu13 129.7(7) 6_565 . ?
Lu8 Lu4 Lu13 71.9(10) . . ?
Lu13 Lu4 Lu13 107.0(14) 6_565 . ?
Lu4 Lu4 Lu13 22.9(5) 6_565 . ?
Lu5 Lu4 Lu13 37.7(5) . . ?
Lu12 Lu4 Lu7 51(3) . . ?
Lu5 Lu4 Lu7 130.5(7) 6_565 . ?
Lu8 Lu4 Lu7 116.9(12) . . ?
Lu13 Lu4 Lu7 57.7(10) 6_565 . ?
Lu4 Lu4 Lu7 74.63(18) 6_565 . ?
Lu5 Lu4 Lu7 89.7(3) . . ?
Lu13 Lu4 Lu7 53.0(5) . . ?
Lu12 Lu4 Lu3 112(3) . 6_565 ?
Lu5 Lu4 Lu3 60.0(5) 6_565 6_565 ?
Lu8 Lu4 Lu3 162.1(12) . 6_565 ?
Lu13 Lu4 Lu3 28.6(9) 6_565 6_565 ?
Lu4 Lu4 Lu3 125.58(17) 6_565 6_565 ?
Lu5 Lu4 Lu3 117.0(3) . 6_565 ?
Lu13 Lu4 Lu3 106.2(5) . 6_565 ?
Lu7 Lu4 Lu3 71.9(4) . 6_565 ?
Lu12 Lu4 C79 99(3) . . ?
Lu5 Lu4 C79 122.7(6) 6_565 . ?
Lu8 Lu4 C79 90.4(10) . . ?
Lu13 Lu4 C79 79.7(8) 6_565 . ?
Lu4 Lu4 C79 108.5(2) 6_565 . ?
Lu5 Lu4 C79 129.4(3) . . ?
Lu13 Lu4 C79 107.7(5) . . ?
Lu7 Lu4 C79 80.5(5) . . ?
Lu3 Lu4 C79 106.8(3) 6_565 . ?
Lu12 Lu4 C80 94(3) . . ?
Lu5 Lu4 C80 118.3(5) 6_565 . ?
Lu8 Lu4 C80 55.4(9) . . ?
Lu13 Lu4 C80 115.5(8) 6_565 . ?
Lu4 Lu4 C80 89.7(2) 6_565 . ?
Lu5 Lu4 C80 102.8(3) . . ?
Lu13 Lu4 C80 102.3(5) . . ?
Lu7 Lu4 C80 105.6(5) . . ?
Lu3 Lu4 C80 140.0(3) 6_565 . ?
C79 Lu4 C80 36.58(8) . . ?
Lu12 Lu4 Lu14 91(3) . 6_565 ?
Lu5 Lu4 Lu14 79.8(6) 6_565 6_565 ?
Lu8 Lu4 Lu14 156.2(9) . 6_565 ?
Lu13 Lu4 Lu14 29.2(8) 6_565 6_565 ?
Lu4 Lu4 Lu14 107.6(3) 6_565 6_565 ?
Lu5 Lu4 Lu14 105.9(4) . 6_565 ?
Lu13 Lu4 Lu14 86.1(6) . 6_565 ?
Lu7 Lu4 Lu14 50.8(5) . 6_565 ?
Lu3 Lu4 Lu14 22.0(3) 6_565 6_565 ?
C79 Lu4 Lu14 105.4(3) . 6_565 ?
C80 Lu4 Lu14 141.9(4) . 6_565 ?
Lu4 Lu5 Lu13 53.6(9) 6_565 . ?
Lu4 Lu5 Lu12 17.4(13) 6_565 . ?
Lu13 Lu5 Lu12 60.7(14) . . ?
Lu4 Lu5 Lu8 37.5(9) 6_565 . ?
Lu13 Lu5 Lu8 90.9(13) . . ?
Lu12 Lu5 Lu8 37.1(15) . . ?
Lu4 Lu5 Lu4 32.3(4) 6_565 . ?
Lu13 Lu5 Lu4 78.2(9) . . ?
Lu12 Lu5 Lu4 17.9(12) . . ?
Lu8 Lu5 Lu4 29.5(6) . . ?
Lu4 Lu5 Lu3 98.1(6) 6_565 . ?
Lu13 Lu5 Lu3 48.0(8) . . ?
Lu12 Lu5 Lu3 97.7(13) . . ?
Lu8 Lu5 Lu3 134.4(9) . . ?
Lu4 Lu5 Lu3 109.9(3) . . ?
Lu4 Lu5 Lu5 55.5(5) 6_565 6_565 ?
Lu13 Lu5 Lu5 97.1(8) . 6_565 ?
Lu12 Lu5 Lu5 40.2(11) . 6_565 ?
Lu8 Lu5 Lu5 40.7(5) . 6_565 ?
Lu4 Lu5 Lu5 23.20(19) . 6_565 ?
Lu3 Lu5 Lu5 114.9(2) . 6_565 ?
Lu4 Lu5 Lu13 35.6(5) 6_565 6_565 ?
Lu13 Lu5 Lu13 69.1(11) . 6_565 ?
Lu12 Lu5 Lu13 18.2(11) . 6_565 ?
Lu8 Lu5 Lu13 45.1(8) . 6_565 ?
Lu4 Lu5 Lu13 15.9(4) . 6_565 ?
Lu3 Lu5 Lu13 94.7(4) . 6_565 ?
Lu5 Lu5 Lu13 27.9(4) 6_565 6_565 ?
Lu4 Lu5 Lu14 81.6(6) 6_565 . ?
Lu13 Lu5 Lu14 38.8(7) . . ?
Lu12 Lu5 Lu14 78.9(13) . . ?
Lu8 Lu5 Lu14 115.9(9) . . ?
Lu4 Lu5 Lu14 90.5(4) . . ?
Lu3 Lu5 Lu14 19.5(3) . . ?
Lu5 Lu5 Lu14 96.9(3) 6_565 . ?
Lu13 Lu5 Lu14 75.2(5) 6_565 . ?
Lu4 Lu5 C48 122.5(6) 6_565 . ?
Lu13 Lu5 C48 125.3(7) . . ?
Lu12 Lu5 C48 134.6(13) . . ?
Lu8 Lu5 C48 100.5(7) . . ?
Lu4 Lu5 C48 129.4(4) . . ?
Lu3 Lu5 C48 118.5(4) . . ?
Lu5 Lu5 C48 125.7(2) 6_565 . ?
Lu13 Lu5 C48 145.4(5) 6_565 . ?
Lu14 Lu5 C48 137.3(4) . . ?
Lu4 Lu5 C68 90.2(5) 6_565 . ?
Lu13 Lu5 C68 117.3(7) . . ?
Lu12 Lu5 C68 100.4(13) . . ?
Lu8 Lu5 C68 66.9(7) . . ?
Lu4 Lu5 C68 96.3(3) . . ?
Lu3 Lu5 C68 142.8(3) . . ?
Lu5 Lu5 C68 99.6(2) 6_565 . ?
Lu13 Lu5 C68 112.0(5) 6_565 . ?
Lu14 Lu5 C68 152.8(4) . . ?
C48 Lu5 C68 34.27(7) . . ?
Lu4 Lu5 Lu7 36.2(5) 6_565 . ?
Lu13 Lu5 Lu7 29.4(8) . . ?
Lu12 Lu5 Lu7 35.1(12) . . ?
Lu8 Lu5 Lu7 71.1(9) . . ?
Lu4 Lu5 Lu7 50.9(2) . . ?
Lu3 Lu5 Lu7 63.3(3) . . ?
Lu5 Lu5 Lu7 67.82(17) 6_565 . ?
Lu13 Lu5 Lu7 39.9(4) 6_565 . ?
Lu14 Lu5 Lu7 45.6(4) . . ?
C48 Lu5 Lu7 148.3(4) . . ?
C68 Lu5 Lu7 123.6(4) . . ?
Lu15 Lu6 Lu1 65.4(12) . . ?
Lu15 Lu6 Lu14 44.6(12) . . ?
Lu1 Lu6 Lu14 73.5(6) . . ?
Lu15 Lu6 Lu2 135.0(14) . . ?
Lu1 Lu6 Lu2 125.8(3) . . ?
Lu14 Lu6 Lu2 93.2(6) . . ?
Lu15 Lu6 Lu16 94.4(13) . . ?
Lu1 Lu6 Lu16 37.1(8) . . ?
Lu14 Lu6 Lu16 77.5(8) . . ?
Lu2 Lu6 Lu16 89.1(8) . . ?
Lu15 Lu6 Lu3 37.3(11) . . ?
Lu1 Lu6 Lu3 50.4(2) . . ?
Lu14 Lu6 Lu3 23.8(5) . . ?
Lu2 Lu6 Lu3 110.7(3) . . ?
Lu16 Lu6 Lu3 63.3(6) . . ?
Lu15 Lu6 C32 93.9(11) . . ?
Lu1 Lu6 C32 112.9(4) . . ?
Lu14 Lu6 C32 133.3(6) . . ?
Lu2 Lu6 C32 113.7(3) . . ?
Lu16 Lu6 C32 136.5(8) . . ?
Lu3 Lu6 C32 130.5(3) . . ?
Lu15 Lu6 C11 118.4(13) . . ?
Lu1 Lu6 C11 86.9(3) . . ?
Lu14 Lu6 C11 158.2(7) . . ?
Lu2 Lu6 C11 106.2(3) . . ?
Lu16 Lu6 C11 92.8(7) . . ?
Lu3 Lu6 C11 134.9(3) . . ?
C32 Lu6 C11 46.58(12) . . ?
Lu15 Lu6 Lu9 72.6(12) . . ?
Lu1 Lu6 Lu9 13.6(3) . . ?
Lu14 Lu6 Lu9 69.9(6) . . ?
Lu2 Lu6 Lu9 112.4(4) . . ?
Lu16 Lu6 Lu9 24.5(7) . . ?
Lu3 Lu6 Lu9 49.1(4) . . ?
C32 Lu6 Lu9 125.3(4) . . ?
C11 Lu6 Lu9 93.2(4) . . ?
Lu15 Lu6 C29 51.0(11) . . ?
Lu1 Lu6 C29 91.2(3) . . ?
Lu14 Lu6 C29 92.7(6) . . ?
Lu2 Lu6 C29 142.6(3) . . ?
Lu16 Lu6 C29 128.2(8) . . ?
Lu3 Lu6 C29 87.9(3) . . ?
C32 Lu6 C29 42.91(12) . . ?
C11 Lu6 C29 77.9(2) . . ?
Lu9 Lu6 C29 104.3(4) . . ?
Lu15 Lu6 C33 110.6(11) . . ?
Lu1 Lu6 C33 149.0(3) . . ?
Lu14 Lu6 C33 127.0(6) . . ?
Lu2 Lu6 C33 79.9(3) . . ?
Lu16 Lu6 C33 153.3(7) . . ?
Lu3 Lu6 C33 143.4(3) . . ?
C32 Lu6 C33 36.39(9) . . ?
C11 Lu6 C33 67.60(15) . . ?
Lu9 Lu6 C33 159.9(4) . . ?
C29 Lu6 C33 67.18(15) . . ?
Lu15 Lu6 C12 150.1(14) . . ?
Lu1 Lu6 C12 92.4(3) . . ?
Lu14 Lu6 C12 150.6(5) . . ?
Lu2 Lu6 C12 73.9(2) . . ?
Lu16 Lu6 C12 76.0(6) . . ?
Lu3 Lu6 C12 138.6(3) . . ?
C32 Lu6 C12 75.83(17) . . ?
C11 Lu6 C12 36.38(10) . . ?
Lu9 Lu6 C12 90.3(4) . . ?
C29 Lu6 C12 113.7(2) . . ?
C33 Lu6 C12 77.62(15) . . ?
Lu13 Lu7 Lu13 81.6(12) . 6_565 ?
Lu13 Lu7 Lu12 41.9(7) . . ?
Lu13 Lu7 Lu12 41.9(7) 6_565 . ?
Lu13 Lu7 Lu14 55.3(7) . . ?
Lu13 Lu7 Lu14 106.3(9) 6_565 . ?
Lu12 Lu7 Lu14 86.7(10) . . ?
Lu13 Lu7 Lu14 106.3(9) . 6_565 ?
Lu13 Lu7 Lu14 55.3(7) 6_565 6_565 ?
Lu12 Lu7 Lu14 86.7(10) . 6_565 ?
Lu14 Lu7 Lu14 81.2(9) . 6_565 ?
Lu13 Lu7 Lu4 56.8(7) . . ?
Lu13 Lu7 Lu4 26.7(6) 6_565 . ?
Lu12 Lu7 Lu4 15.39(19) . . ?
Lu14 Lu7 Lu4 96.1(7) . . ?
Lu14 Lu7 Lu4 76.2(6) 6_565 . ?
Lu13 Lu7 Lu4 26.7(6) . 6_565 ?
Lu13 Lu7 Lu4 56.8(7) 6_565 6_565 ?
Lu12 Lu7 Lu4 15.39(19) . 6_565 ?
Lu14 Lu7 Lu4 76.2(6) . 6_565 ?
Lu14 Lu7 Lu4 96.1(7) 6_565 6_565 ?
Lu4 Lu7 Lu4 30.7(4) . 6_565 ?
Lu13 Lu7 C74 146.2(9) . . ?
Lu13 Lu7 C74 104.8(6) 6_565 . ?
Lu12 Lu7 C74 127.6(10) . . ?
Lu14 Lu7 C74 145.1(8) . . ?
Lu14 Lu7 C74 104.2(5) 6_565 . ?
Lu4 Lu7 C74 118.7(6) . . ?
Lu4 Lu7 C74 135.6(8) 6_565 . ?
Lu13 Lu7 C73 104.4(8) . . ?
Lu13 Lu7 C73 88.9(7) 6_565 . ?
Lu12 Lu7 C73 88.7(11) . . ?
Lu14 Lu7 C73 150.9(6) . . ?
Lu14 Lu7 C73 127.3(5) 6_565 . ?
Lu4 Lu7 C73 86.4(6) . . ?
Lu4 Lu7 C73 92.7(6) 6_565 . ?
C74 Lu7 C73 43.9(3) . . ?
Lu13 Lu7 C54 92.6(5) . . ?
Lu13 Lu7 C54 146.5(10) 6_565 . ?
Lu12 Lu7 C54 118.4(9) . . ?
Lu14 Lu7 C54 96.9(4) . . ?
Lu14 Lu7 C54 154.8(9) 6_565 . ?
Lu4 Lu7 C54 128.8(7) . . ?
Lu4 Lu7 C54 107.9(5) 6_565 . ?
C74 Lu7 C54 63.6(4) . . ?
C73 Lu7 C54 60.5(4) . . ?
Lu13 Lu7 C55 130.8(6) . . ?
Lu13 Lu7 C55 143.1(7) 6_565 . ?
Lu12 Lu7 C55 154.0(12) . . ?
Lu14 Lu7 C55 107.4(6) . . ?
Lu14 Lu7 C55 116.4(7) 6_565 . ?
Lu4 Lu7 C55 154.5(8) . . ?
Lu4 Lu7 C55 147.5(6) 6_565 . ?
C74 Lu7 C55 39.0(2) . . ?
C73 Lu7 C55 68.3(4) . . ?
C54 Lu7 C55 40.0(2) . . ?
Lu13 Lu7 Lu3 96.7(8) . 6_565 ?
Lu13 Lu7 Lu3 33.6(5) 6_565 6_565 ?
Lu12 Lu7 Lu3 67.8(7) . 6_565 ?
Lu14 Lu7 Lu3 90.9(7) . 6_565 ?
Lu14 Lu7 Lu3 21.7(4) 6_565 6_565 ?
Lu4 Lu7 Lu3 55.6(3) . 6_565 ?
Lu4 Lu7 Lu3 79.7(5) 6_565 6_565 ?
C74 Lu7 Lu3 106.7(2) . 6_565 ?
C73 Lu7 Lu3 113.8(4) . 6_565 ?
C54 Lu7 Lu3 170.2(5) . 6_565 ?
C55 Lu7 Lu3 131.6(5) . 6_565 ?
Lu12 Lu8 Lu4 41.5(10) . . ?
Lu12 Lu8 Lu4 41.5(10) . 6_565 ?
Lu4 Lu8 Lu4 81.0(17) . 6_565 ?
Lu12 Lu8 Lu5 70.8(16) . . ?
Lu4 Lu8 Lu5 99.9(14) . . ?
Lu4 Lu8 Lu5 35.7(6) 6_565 . ?
Lu12 Lu8 Lu5 70.8(16) . 6_565 ?
Lu4 Lu8 Lu5 35.7(6) . 6_565 ?
Lu4 Lu8 Lu5 99.9(14) 6_565 6_565 ?
Lu5 Lu8 Lu5 98.6(11) . 6_565 ?
Lu12 Lu8 Lu13 40.5(6) . . ?
Lu4 Lu8 Lu13 81.2(13) . . ?
Lu4 Lu8 Lu13 5.7(8) 6_565 . ?
Lu5 Lu8 Lu13 40.5(7) . . ?
Lu5 Lu8 Lu13 102.8(11) 6_565 . ?
Lu12 Lu8 Lu13 40.5(6) . 6_565 ?
Lu4 Lu8 Lu13 5.7(8) . 6_565 ?
Lu4 Lu8 Lu13 81.2(13) 6_565 6_565 ?
Lu5 Lu8 Lu13 102.8(11) . 6_565 ?
Lu5 Lu8 Lu13 40.5(7) 6_565 6_565 ?
Lu13 Lu8 Lu13 80.8(12) . 6_565 ?
Lu12 Lu8 C69 120(2) . . ?
Lu4 Lu8 C69 141.7(15) . . ?
Lu4 Lu8 C69 98.2(8) 6_565 . ?
Lu5 Lu8 C69 101.0(4) . . ?
Lu5 Lu8 C69 160.1(8) 6_565 . ?
Lu13 Lu8 C69 94.5(6) . . ?
Lu13 Lu8 C69 136.0(10) 6_565 . ?
Lu12 Lu8 C80 115(3) . . ?
Lu4 Lu8 C80 105.7(10) . . ?
Lu4 Lu8 C80 126.5(14) 6_565 . ?
Lu5 Lu8 C80 145.0(7) . . ?
Lu5 Lu8 C80 116.1(5) 6_565 . ?
Lu13 Lu8 C80 121.0(9) . . ?
Lu13 Lu8 C80 101.0(7) 6_565 . ?
C69 Lu8 C80 44.9(3) . . ?
Lu12 Lu8 C66 146.5(15) . . ?
Lu4 Lu8 C66 110.7(7) . . ?
Lu4 Lu8 C66 165.9(11) 6_565 . ?
Lu5 Lu8 C66 142.5(11) . . ?
Lu5 Lu8 C66 94.2(6) 6_565 . ?
Lu13 Lu8 C66 162.0(9) . . ?
Lu13 Lu8 C66 109.6(5) 6_565 . ?
C69 Lu8 C66 67.7(5) . . ?
C80 Lu8 C66 44.0(3) . . ?
Lu12 Lu8 C67 176(3) . . ?
Lu4 Lu8 C67 137.9(11) . . ?
Lu4 Lu8 C67 137.2(10) 6_565 . ?
Lu5 Lu8 C67 106.5(9) . . ?
Lu5 Lu8 C67 107.1(9) 6_565 . ?
Lu13 Lu8 C67 138.8(6) . . ?
Lu13 Lu8 C67 139.5(6) 6_565 . ?
C69 Lu8 C67 63.5(4) . . ?
C80 Lu8 C67 68.7(5) . . ?
C66 Lu8 C67 36.0(3) . . ?
Lu12 Lu8 C68 142.3(6) . . ?
Lu4 Lu8 C68 176.2(13) . . ?
Lu4 Lu8 C68 102.6(7) 6_565 . ?
Lu5 Lu8 C68 82.5(5) . . ?
Lu5 Lu8 C68 141.2(12) 6_565 . ?
Lu13 Lu8 C68 102.5(5) . . ?
Lu13 Lu8 C68 174.4(9) 6_565 . ?
C69 Lu8 C68 39.8(2) . . ?
C80 Lu8 C68 73.4(5) . . ?
C66 Lu8 C68 66.0(5) . . ?
C67 Lu8 C68 38.2(3) . . ?
Lu16 Lu9 Lu1 74.2(17) . . ?
Lu16 Lu9 Lu10 58.9(17) . . ?
Lu1 Lu9 Lu10 133.1(12) . . ?
Lu16 Lu9 Lu3 94.0(15) . . ?
Lu1 Lu9 Lu3 62.0(5) . . ?
Lu10 Lu9 Lu3 117.8(7) . . ?
Lu16 Lu9 Lu14 72.0(16) . . ?
Lu1 Lu9 Lu14 44.8(5) . . ?
Lu10 Lu9 Lu14 113.1(7) . . ?
Lu3 Lu9 Lu14 25.2(3) . . ?
Lu16 Lu9 Lu15 86.9(18) . . ?
Lu1 Lu9 Lu15 26.9(8) . . ?
Lu10 Lu9 Lu15 138.6(10) . . ?
Lu3 Lu9 Lu15 36.0(7) . . ?
Lu14 Lu9 Lu15 26.9(7) . . ?
Lu16 Lu9 Lu6 57.0(16) . . ?
Lu1 Lu9 Lu6 19.0(4) . . ?
Lu10 Lu9 Lu6 115.3(8) . . ?
Lu3 Lu9 Lu6 60.3(3) . . ?
Lu14 Lu9 Lu6 37.1(4) . . ?
Lu15 Lu9 Lu6 33.0(7) . . ?
Lu16 Lu9 C9 92.4(17) . . ?
Lu1 Lu9 C9 94.1(7) . . ?
Lu10 Lu9 C9 88.5(6) . . ?
Lu3 Lu9 C9 152.3(6) . . ?
Lu14 Lu9 C9 138.3(7) . . ?
Lu15 Lu9 C9 117.8(8) . . ?
Lu6 Lu9 C9 101.9(5) . . ?
Lu16 Lu9 C26 150.9(17) . . ?
Lu1 Lu9 C26 102.8(7) . . ?
Lu10 Lu9 C26 117.9(6) . . ?
Lu3 Lu9 C26 110.3(6) . . ?
Lu14 Lu9 C26 126.6(6) . . ?
Lu15 Lu9 C26 103.4(8) . . ?
Lu6 Lu9 C26 121.7(5) . . ?
C9 Lu9 C26 58.7(2) . . ?
Lu16 Lu9 C27 126.5(18) . . ?
Lu1 Lu9 C27 65.1(6) . . ?
Lu10 Lu9 C27 145.9(6) . . ?
Lu3 Lu9 C27 96.1(5) . . ?
Lu14 Lu9 C27 99.1(5) . . ?
Lu15 Lu9 C27 72.3(8) . . ?
Lu6 Lu9 C27 83.8(4) . . ?
C9 Lu9 C27 59.0(2) . . ?
C26 Lu9 C27 38.15(16) . . ?
Lu16 Lu9 C8 120.5(17) . . ?
Lu1 Lu9 C8 123.8(7) . . ?
Lu10 Lu9 C8 83.9(6) . . ?
Lu3 Lu9 C8 145.5(7) . . ?
Lu14 Lu9 C8 163.0(6) . . ?
Lu15 Lu9 C8 136.7(9) . . ?
Lu6 Lu9 C8 137.3(5) . . ?
C9 Lu9 C8 37.80(13) . . ?
C26 Lu9 C8 37.08(14) . . ?
C27 Lu9 C8 64.4(2) . . ?
Lu16 Lu9 Lu11 72.1(17) . . ?
Lu1 Lu9 Lu11 141.8(8) . . ?
Lu10 Lu9 Lu11 21.0(5) . . ?
Lu3 Lu9 Lu11 102.8(5) . . ?
Lu14 Lu9 Lu11 106.4(5) . . ?
Lu15 Lu9 Lu11 133.1(9) . . ?
Lu6 Lu9 Lu11 122.8(5) . . ?
C9 Lu9 Lu11 104.9(5) . . ?
C26 Lu9 Lu11 115.4(5) . . ?
C27 Lu9 Lu11 152.7(5) . . ?
C8 Lu9 Lu11 89.2(4) . . ?
Lu16 Lu10 Lu11 144.0(14) . . ?
Lu16 Lu10 Lu9 40.8(11) . . ?
Lu11 Lu10 Lu9 137.3(10) . . ?
Lu16 Lu10 Lu10 103.5(13) . 6_565 ?
Lu11 Lu10 Lu10 56.9(5) . 6_565 ?
Lu9 Lu10 Lu10 140.7(5) . 6_565 ?
Lu16 Lu10 Lu16 69.9(18) . 6_565 ?
Lu11 Lu10 Lu16 86.2(9) . 6_565 ?
Lu9 Lu10 Lu16 108.4(9) . 6_565 ?
Lu10 Lu10 Lu16 33.7(7) 6_565 6_565 ?
Lu16 Lu10 Lu1 22.0(12) . . ?
Lu11 Lu10 Lu1 145.0(8) . . ?
Lu9 Lu10 Lu1 18.9(5) . . ?
Lu10 Lu10 Lu1 123.9(3) 6_565 . ?
Lu16 Lu10 Lu1 90.6(7) 6_565 . ?
Lu16 Lu10 C1 84.6(10) . . ?
Lu11 Lu10 C1 125.9(8) . . ?
Lu9 Lu10 C1 92.8(7) . . ?
Lu10 Lu10 C1 100.3(3) 6_565 . ?
Lu16 Lu10 C1 96.9(6) 6_565 . ?
Lu1 Lu10 C1 89.1(4) . . ?
Lu16 Lu10 C5 120.3(11) . . ?
Lu11 Lu10 C5 87.4(7) . . ?
Lu9 Lu10 C5 128.9(7) . . ?
Lu10 Lu10 C5 78.3(3) 6_565 . ?
Lu16 Lu10 C5 95.3(7) 6_565 . ?
Lu1 Lu10 C5 127.7(4) . . ?
C1 Lu10 C5 38.55(14) . . ?
Lu16 Lu10 C6 144.7(12) . . ?
Lu11 Lu10 C6 70.6(6) . . ?
Lu9 Lu10 C6 126.5(7) . . ?
Lu10 Lu10 C6 91.9(3) 6_565 . ?
Lu16 Lu10 C6 119.8(8) 6_565 . ?
Lu1 Lu10 C6 138.2(5) . . ?
C1 Lu10 C6 61.2(2) . . ?
C5 Lu10 C6 32.11(11) . . ?
Lu16 Lu10 C7 129.2(14) . . ?
Lu11 Lu10 C7 83.2(6) . . ?
Lu9 Lu10 C7 95.4(7) . . ?
Lu10 Lu10 C7 123.9(3) 6_565 . ?
Lu16 Lu10 C7 154.0(8) 6_565 . ?
Lu1 Lu10 C7 111.6(5) . . ?
C1 Lu10 C7 71.0(3) . . ?
C5 Lu10 C7 60.6(2) . . ?
C6 Lu10 C7 34.12(12) . . ?
Lu16 Lu10 Lu3 45.3(10) . . ?
Lu11 Lu10 Lu3 109.8(7) . . ?
Lu9 Lu10 Lu3 35.2(4) . . ?
Lu10 Lu10 Lu3 112.1(3) 6_565 . ?
Lu16 Lu10 Lu3 87.8(7) 6_565 . ?
Lu1 Lu10 Lu3 35.19(17) . . ?
C1 Lu10 Lu3 124.3(4) . . ?
C5 Lu10 Lu3 162.8(5) . . ?
C6 Lu10 Lu3 151.9(5) . . ?
C7 Lu10 Lu3 118.1(4) . . ?
Lu16 Lu10 Lu9 85.7(14) . 6_565 ?
Lu11 Lu10 Lu9 69.1(6) . 6_565 ?
Lu9 Lu10 Lu9 121.7(7) . 6_565 ?
Lu10 Lu10 Lu9 19.0(3) 6_565 6_565 ?
Lu16 Lu10 Lu9 17.1(6) 6_565 6_565 ?
Lu1 Lu10 Lu9 105.2(4) . 6_565 ?
C1 Lu10 Lu9 105.4(4) . 6_565 ?
C5 Lu10 Lu9 92.9(4) . 6_565 ?
C6 Lu10 Lu9 110.5(4) . 6_565 ?
C7 Lu10 Lu9 142.8(5) . 6_565 ?
Lu3 Lu10 Lu9 94.9(3) . 6_565 ?
Lu10 Lu11 Lu10 66.3(11) 6_565 . ?
Lu10 Lu11 C20 108.6(8) 6_565 . ?
Lu10 Lu11 C20 114.7(9) . . ?
Lu10 Lu11 C21 147.3(9) 6_565 . ?
Lu10 Lu11 C21 121.8(6) . . ?
C20 Lu11 C21 38.78(19) . . ?
Lu10 Lu11 C19 81.6(6) 6_565 . ?
Lu10 Lu11 C19 127.1(10) . . ?
C20 Lu11 C19 38.23(18) . . ?
C21 Lu11 C19 68.7(3) . . ?
Lu10 Lu11 C6 99.0(9) 6_565 . ?
Lu10 Lu11 C6 77.5(7) . . ?
C20 Lu11 C6 37.5(2) . . ?
C21 Lu11 C6 57.5(3) . . ?
C19 Lu11 C6 66.9(3) . . ?
Lu10 Lu11 Lu16 17.0(7) 6_565 6_565 ?
Lu10 Lu11 Lu16 60.2(8) . 6_565 ?
C20 Lu11 Lu16 125.5(8) . 6_565 ?
C21 Lu11 Lu16 164.2(8) . 6_565 ?
C19 Lu11 Lu16 97.4(7) . 6_565 ?
C6 Lu11 Lu16 111.1(8) . 6_565 ?
Lu10 Lu11 Lu16 60.2(8) 6_565 . ?
Lu10 Lu11 Lu16 17.0(7) . . ?
C20 Lu11 Lu16 131.0(9) . . ?
C21 Lu11 Lu16 136.2(7) . . ?
C19 Lu11 Lu16 134.7(8) . . ?
C6 Lu11 Lu16 94.2(7) . . ?
Lu16 Lu11 Lu16 49.6(12) 6_565 . ?
Lu10 Lu11 C23 151.5(9) 6_565 . ?
Lu10 Lu11 C23 90.6(5) . . ?
C20 Lu11 C23 64.7(3) . . ?
C21 Lu11 C23 35.91(13) . . ?
C19 Lu11 C23 101.4(4) . . ?
C6 Lu11 C23 58.0(2) . . ?
Lu16 Lu11 C23 150.8(7) 6_565 . ?
Lu16 Lu11 C23 101.9(6) . . ?
Lu10 Lu11 Lu9 21.6(5) 6_565 6_565 ?
Lu10 Lu11 Lu9 81.2(7) . 6_565 ?
C20 Lu11 Lu9 118.0(5) . 6_565 ?
C21 Lu11 Lu9 150.6(4) . 6_565 ?
C19 Lu11 Lu9 83.0(3) . 6_565 ?
C6 Lu11 Lu9 118.7(6) . 6_565 ?
Lu16 Lu11 Lu9 21.1(5) 6_565 6_565 ?
Lu16 Lu11 Lu9 70.4(8) . 6_565 ?
C23 Lu11 Lu9 171.8(6) . 6_565 ?
Lu10 Lu11 Lu9 81.2(7) 6_565 . ?
Lu10 Lu11 Lu9 21.6(5) . . ?
C20 Lu11 Lu9 126.6(5) . . ?
C21 Lu11 Lu9 117.6(3) . . ?
C19 Lu11 Lu9 148.3(8) . . ?
C6 Lu11 Lu9 89.8(4) . . ?
Lu16 Lu11 Lu9 70.4(8) 6_565 . ?
Lu16 Lu11 Lu9 21.1(5) . . ?
C23 Lu11 Lu9 82.0(3) . . ?
Lu9 Lu11 Lu9 90.6(6) 6_565 . ?
Lu10 Lu11 C5 69.0(7) 6_565 . ?
Lu10 Lu11 C5 62.5(7) . . ?
C20 Lu11 C5 56.6(4) . . ?
C21 Lu11 C5 86.6(4) . . ?
C19 Lu11 C5 67.2(4) . . ?
C6 Lu11 C5 30.17(19) . . ?
Lu16 Lu11 C5 81.0(6) 6_565 . ?
Lu16 Lu11 C5 76.4(6) . . ?
C23 Lu11 C5 85.9(4) . . ?
Lu9 Lu11 C5 89.6(5) 6_565 . ?
Lu9 Lu11 C5 81.8(5) . . ?
Lu4 Lu12 Lu4 133(6) . 6_565 ?
Lu4 Lu12 Lu8 70(3) . . ?
Lu4 Lu12 Lu8 70(3) 6_565 . ?
Lu4 Lu12 Lu13 166(4) . . ?
Lu4 Lu12 Lu13 45.0(18) 6_565 . ?
Lu8 Lu12 Lu13 113.8(15) . . ?
Lu4 Lu12 Lu13 45.0(18) . 6_565 ?
Lu4 Lu12 Lu13 166(4) 6_565 6_565 ?
Lu8 Lu12 Lu13 113.8(15) . 6_565 ?
Lu13 Lu12 Lu13 132(3) . 6_565 ?
Lu4 Lu12 Lu5 24(2) . 6_565 ?
Lu4 Lu12 Lu5 119(4) 6_565 6_565 ?
Lu8 Lu12 Lu5 72(2) . 6_565 ?
Lu13 Lu12 Lu5 143(3) . 6_565 ?
Lu13 Lu12 Lu5 53.1(9) 6_565 6_565 ?
Lu4 Lu12 Lu5 119(4) . . ?
Lu4 Lu12 Lu5 24(2) 6_565 . ?
Lu8 Lu12 Lu5 72(2) . . ?
Lu13 Lu12 Lu5 53.1(9) . . ?
Lu13 Lu12 Lu5 143(3) 6_565 . ?
Lu5 Lu12 Lu5 100(2) 6_565 . ?
Lu4 Lu12 Lu7 113(3) . . ?
Lu4 Lu12 Lu7 113(3) 6_565 . ?
Lu8 Lu12 Lu7 159(3) . . ?
Lu13 Lu12 Lu7 68.9(16) . . ?
Lu13 Lu12 Lu7 68.9(16) 6_565 . ?
Lu5 Lu12 Lu7 119.3(14) 6_565 . ?
Lu5 Lu12 Lu7 119.3(14) . . ?
Lu4 Lu12 Lu3 141(4) . . ?
Lu4 Lu12 Lu3 55(2) 6_565 . ?
Lu8 Lu12 Lu3 121.6(17) . . ?
Lu13 Lu12 Lu3 25.0(9) . . ?
Lu13 Lu12 Lu3 116.3(17) 6_565 . ?
Lu5 Lu12 Lu3 119.0(17) 6_565 . ?
Lu5 Lu12 Lu3 49.9(7) . . ?
Lu7 Lu12 Lu3 70.2(8) . . ?
Lu4 Lu12 Lu3 55(2) . 6_565 ?
Lu4 Lu12 Lu3 141(4) 6_565 6_565 ?
Lu8 Lu12 Lu3 121.6(17) . 6_565 ?
Lu13 Lu12 Lu3 116.3(17) . 6_565 ?
Lu13 Lu12 Lu3 25.0(9) 6_565 6_565 ?
Lu5 Lu12 Lu3 49.9(7) 6_565 6_565 ?
Lu5 Lu12 Lu3 119.0(17) . 6_565 ?
Lu7 Lu12 Lu3 70.2(8) . 6_565 ?
Lu3 Lu12 Lu3 95.2(10) . 6_565 ?
Lu4 Lu12 Lu14 133(3) . . ?
Lu4 Lu12 Lu14 76(3) 6_565 . ?
Lu8 Lu12 Lu14 143.3(18) . . ?
Lu13 Lu12 Lu14 37.0(11) . . ?
Lu13 Lu12 Lu14 97.0(17) 6_565 . ?
Lu5 Lu12 Lu14 116.7(16) 6_565 . ?
Lu5 Lu12 Lu14 71.3(10) . . ?
Lu7 Lu12 Lu14 50.7(8) . . ?
Lu3 Lu12 Lu14 21.7(3) . . ?
Lu3 Lu12 Lu14 79.4(9) 6_565 . ?
Lu4 Lu12 Lu14 76(3) . 6_565 ?
Lu4 Lu12 Lu14 133(3) 6_565 6_565 ?
Lu8 Lu12 Lu14 143.3(18) . 6_565 ?
Lu13 Lu12 Lu14 97.0(17) . 6_565 ?
Lu13 Lu12 Lu14 37.0(11) 6_565 6_565 ?
Lu5 Lu12 Lu14 71.3(10) 6_565 6_565 ?
Lu5 Lu12 Lu14 116.6(16) . 6_565 ?
Lu7 Lu12 Lu14 50.7(8) . 6_565 ?
Lu3 Lu12 Lu14 79.4(9) . 6_565 ?
Lu3 Lu12 Lu14 21.7(3) 6_565 6_565 ?
Lu14 Lu12 Lu14 60.5(9) . 6_565 ?
Lu4 Lu13 Lu5 44.1(8) 6_565 . ?
Lu4 Lu13 Lu12 26.9(14) 6_565 . ?
Lu5 Lu13 Lu12 66.2(17) . . ?
Lu4 Lu13 Lu3 132.9(13) 6_565 . ?
Lu5 Lu13 Lu3 94.4(11) . . ?
Lu12 Lu13 Lu3 132.8(15) . . ?
Lu4 Lu13 Lu7 95.6(12) 6_565 . ?
Lu5 Lu13 Lu7 131.8(12) . . ?
Lu12 Lu13 Lu7 69.2(17) . . ?
Lu3 Lu13 Lu7 102.7(10) . . ?
Lu4 Lu13 Lu14 135.8(11) 6_565 . ?
Lu5 Lu13 Lu14 117.1(10) . . ?
Lu12 Lu13 Lu14 117.6(15) . . ?
Lu3 Lu13 Lu14 33.0(5) . . ?
Lu7 Lu13 Lu14 69.7(8) . . ?
Lu4 Lu13 Lu8 5.1(7) 6_565 . ?
Lu5 Lu13 Lu8 48.5(9) . . ?
Lu12 Lu13 Lu8 25.8(14) . . ?
Lu3 Lu13 Lu8 138.0(11) . . ?
Lu7 Lu13 Lu8 93.2(10) . . ?
Lu14 Lu13 Lu8 138.9(9) . . ?
Lu4 Lu13 Lu4 27.2(6) 6_565 . ?
Lu5 Lu13 Lu4 64.0(8) . . ?
Lu12 Lu13 Lu4 4.4(14) . . ?
Lu3 Lu13 Lu4 128.5(8) . . ?
Lu7 Lu13 Lu4 70.2(7) . . ?
Lu14 Lu13 Lu4 114.7(8) . . ?
Lu8 Lu13 Lu4 26.9(4) . . ?
Lu4 Lu13 Lu13 50.1(10) 6_565 6_565 ?
Lu5 Lu13 Lu13 82.9(8) . 6_565 ?
Lu12 Lu13 Lu13 24.0(14) . 6_565 ?
Lu3 Lu13 Lu13 117.7(5) . 6_565 ?
Lu7 Lu13 Lu13 49.2(6) . 6_565 ?
Lu14 Lu13 Lu13 95.2(7) . 6_565 ?
Lu8 Lu13 Lu13 49.6(6) . 6_565 ?
Lu4 Lu13 Lu13 22.9(5) . 6_565 ?
Lu4 Lu13 Lu5 29.7(6) 6_565 6_565 ?
Lu5 Lu13 Lu5 55.0(7) . 6_565 ?
Lu12 Lu13 Lu5 19.1(14) . 6_565 ?
Lu3 Lu13 Lu5 114.8(7) . 6_565 ?
Lu7 Lu13 Lu5 77.0(6) . 6_565 ?
Lu14 Lu13 Lu5 106.8(7) . 6_565 ?
Lu8 Lu13 Lu5 32.1(5) . 6_565 ?
Lu4 Lu13 Lu5 14.8(2) . 6_565 ?
Lu13 Lu13 Lu5 27.9(4) 6_565 6_565 ?
Lu4 Lu13 Lu15 152.2(12) 6_565 . ?
Lu5 Lu13 Lu15 118.3(12) . . ?
Lu12 Lu13 Lu15 138.4(15) . . ?
Lu3 Lu13 Lu15 23.9(8) . . ?
Lu7 Lu13 Lu15 84.6(10) . . ?
Lu14 Lu13 Lu15 20.9(8) . . ?
Lu8 Lu13 Lu15 156.5(10) . . ?
Lu4 Lu13 Lu15 135.2(9) . . ?
Lu13 Lu13 Lu15 116.0(7) 6_565 . ?
Lu5 Lu13 Lu15 125.8(8) 6_565 . ?
Lu4 Lu13 C71 107.2(10) 6_565 . ?
Lu5 Lu13 C71 98.5(8) . . ?
Lu12 Lu13 C71 125.3(14) . . ?
Lu3 Lu13 C71 99.0(8) . . ?
Lu7 Lu13 C71 122.2(8) . . ?
Lu14 Lu13 C71 116.0(9) . . ?
Lu8 Lu13 C71 104.9(7) . . ?
Lu4 Lu13 C71 128.8(7) . . ?
Lu13 Lu13 C71 143.1(4) 6_565 . ?
Lu5 Lu13 C71 136.8(7) 6_565 . ?
Lu15 Lu13 C71 95.9(8) . . ?
Lu3 Lu14 Lu15 82.2(18) . . ?
Lu3 Lu14 Lu6 119.7(12) . . ?
Lu15 Lu14 Lu6 60.1(16) . . ?
Lu3 Lu14 Lu1 69.0(8) . . ?
Lu15 Lu14 Lu1 58.3(17) . . ?
Lu6 Lu14 Lu1 51.6(5) . . ?
Lu3 Lu14 Lu13 52.7(9) . . ?
Lu15 Lu14 Lu13 121.7(18) . . ?
Lu6 Lu14 Lu13 169.0(10) . . ?
Lu1 Lu14 Lu13 118.8(9) . . ?
Lu3 Lu14 Lu7 107.7(11) . . ?
Lu15 Lu14 Lu7 141.5(18) . . ?
Lu6 Lu14 Lu7 131.5(10) . . ?
Lu1 Lu14 Lu7 160.2(8) . . ?
Lu13 Lu14 Lu7 55.0(7) . . ?
Lu3 Lu14 Lu2 143.9(10) . . ?
Lu15 Lu14 Lu2 102.4(16) . . ?
Lu6 Lu14 Lu2 44.0(4) . . ?
Lu1 Lu14 Lu2 83.0(5) . . ?
Lu13 Lu14 Lu2 135.9(9) . . ?
Lu7 Lu14 Lu2 91.0(7) . . ?
Lu3 Lu14 Lu16 75.3(10) . . ?
Lu15 Lu14 Lu16 91.1(19) . . ?
Lu6 Lu14 Lu16 61.6(7) . . ?
Lu1 Lu14 Lu16 33.1(7) . . ?
Lu13 Lu14 Lu16 107.5(9) . . ?
Lu7 Lu14 Lu16 127.3(10) . . ?
Lu2 Lu14 Lu16 68.9(7) . . ?
Lu3 Lu14 Lu9 52.9(8) . . ?
Lu15 Lu14 Lu9 77.6(17) . . ?
Lu6 Lu14 Lu9 73.0(6) . . ?
Lu1 Lu14 Lu9 24.5(3) . . ?
Lu13 Lu14 Lu9 96.5(8) . . ?
Lu7 Lu14 Lu9 138.3(8) . . ?
Lu2 Lu14 Lu9 92.6(6) . . ?
Lu16 Lu14 Lu9 25.1(6) . . ?
Lu3 Lu14 Lu5 40.7(6) . . ?
Lu15 Lu14 Lu5 122.2(17) . . ?
Lu6 Lu14 Lu5 144.9(7) . . ?
Lu1 Lu14 Lu5 97.5(6) . . ?
Lu13 Lu14 Lu5 24.2(5) . . ?
Lu7 Lu14 Lu5 71.4(6) . . ?
Lu2 Lu14 Lu5 127.7(6) . . ?
Lu16 Lu14 Lu5 83.4(7) . . ?
Lu9 Lu14 Lu5 73.7(5) . . ?
Lu3 Lu14 Lu4 57.1(7) . 6_565 ?
Lu15 Lu14 Lu4 134.2(17) . 6_565 ?
Lu6 Lu14 Lu4 156.8(7) . 6_565 ?
Lu1 Lu14 Lu4 115.5(6) . 6_565 ?
Lu13 Lu14 Lu4 15.0(5) . 6_565 ?
Lu7 Lu14 Lu4 52.9(5) . 6_565 ?
Lu2 Lu14 Lu4 122.6(6) . 6_565 ?
Lu16 Lu14 Lu4 97.0(7) . 6_565 ?
Lu9 Lu14 Lu4 91.3(5) . 6_565 ?
Lu5 Lu14 Lu4 18.53(16) . 6_565 ?
Lu3 Lu14 Lu12 69.9(9) . . ?
Lu15 Lu14 Lu12 146.9(17) . . ?
Lu6 Lu14 Lu12 150.5(9) . . ?
Lu1 Lu14 Lu12 122.7(9) . . ?
Lu13 Lu14 Lu12 25.4(6) . . ?
Lu7 Lu14 Lu12 42.6(8) . . ?
Lu2 Lu14 Lu12 110.6(6) . . ?
Lu16 Lu14 Lu12 98.4(10) . . ?
Lu9 Lu14 Lu12 98.1(9) . . ?
Lu5 Lu14 Lu12 29.9(6) . . ?
Lu4 Lu14 Lu12 13.3(4) 6_565 . ?
Lu14 Lu15 Lu6 75.3(19) . . ?
Lu14 Lu15 Lu3 46.6(12) . . ?
Lu6 Lu15 Lu3 106.6(18) . . ?
Lu14 Lu15 Lu1 83.7(18) . . ?
Lu6 Lu15 Lu1 60.3(12) . . ?
Lu3 Lu15 Lu1 71.3(12) . . ?
Lu14 Lu15 C29 155(2) . . ?
Lu6 Lu15 C29 97.4(14) . . ?
Lu3 Lu15 C29 153.9(19) . . ?
Lu1 Lu15 C29 114.2(17) . . ?
Lu14 Lu15 C28 157(2) . . ?
Lu6 Lu15 C28 120.0(18) . . ?
Lu3 Lu15 C28 110.0(15) . . ?
Lu1 Lu15 C28 89.2(14) . . ?
C29 Lu15 C28 47.0(6) . . ?
Lu14 Lu15 Lu9 75.5(15) . . ?
Lu6 Lu15 Lu9 74.4(13) . . ?
Lu3 Lu15 Lu9 53.9(10) . . ?
Lu1 Lu15 Lu9 18.1(5) . . ?
C29 Lu15 Lu9 126.6(15) . . ?
C28 Lu15 Lu9 91.0(11) . . ?
Lu14 Lu15 Lu16 63.2(16) . . ?
Lu6 Lu15 Lu16 53.3(11) . . ?
Lu3 Lu15 Lu16 61.5(11) . . ?
Lu1 Lu15 Lu16 21.1(8) . . ?
C29 Lu15 Lu16 131.5(15) . . ?
C28 Lu15 Lu16 109.9(13) . . ?
Lu9 Lu15 Lu16 23.4(6) . . ?
Lu14 Lu15 C30 110(2) . . ?
Lu6 Lu15 C30 106.7(13) . . ?
Lu3 Lu15 C30 129.5(18) . . ?
Lu1 Lu15 C30 159.2(16) . . ?
C29 Lu15 C30 48.3(6) . . ?
C28 Lu15 C30 84.0(9) . . ?
Lu9 Lu15 C30 174.7(14) . . ?
Lu16 Lu15 C30 159.3(13) . . ?
Lu14 Lu15 Lu13 37.5(13) . . ?
Lu6 Lu15 Lu13 111.8(16) . . ?
Lu3 Lu15 Lu13 25.7(9) . . ?
Lu1 Lu15 Lu13 94.9(12) . . ?
C29 Lu15 Lu13 146.5(14) . . ?
C28 Lu15 Lu13 121.8(11) . . ?
Lu9 Lu15 Lu13 78.6(8) . . ?
Lu16 Lu15 Lu13 80.8(9) . . ?
C30 Lu15 Lu13 105.5(11) . . ?
Lu14 Lu15 C32 126(2) . . ?
Lu6 Lu15 C32 55.6(9) . . ?
Lu3 Lu15 C32 160.0(18) . . ?
Lu1 Lu15 C32 90.3(12) . . ?
C29 Lu15 C32 41.8(5) . . ?
C28 Lu15 C32 76.5(8) . . ?
Lu9 Lu15 C32 108.2(11) . . ?
Lu16 Lu15 C32 98.6(11) . . ?
C30 Lu15 C32 69.0(6) . . ?
Lu13 Lu15 C32 161.0(13) . . ?
Lu14 Lu15 Lu2 54.0(14) . . ?
Lu6 Lu15 Lu2 24.1(8) . . ?
Lu3 Lu15 Lu2 94.0(14) . . ?
Lu1 Lu15 Lu2 73.0(11) . . ?
C29 Lu15 Lu2 112.0(10) . . ?
C28 Lu15 Lu2 143.9(12) . . ?
Lu9 Lu15 Lu2 81.6(9) . . ?
Lu16 Lu15 Lu2 58.1(9) . . ?
C30 Lu15 Lu2 101.6(9) . . ?
Lu13 Lu15 Lu2 91.5(9) . . ?
C32 Lu15 Lu2 72.5(7) . . ?
Lu9 Lu16 Lu1 54.3(15) . . ?
Lu9 Lu16 Lu10 80.3(19) . . ?
Lu1 Lu16 Lu10 135(2) . . ?
Lu9 Lu16 Lu6 98(2) . . ?
Lu1 Lu16 Lu6 45.0(9) . . ?
Lu10 Lu16 Lu6 170.6(16) . . ?
Lu9 Lu16 Lu3 59.2(13) . . ?
Lu1 Lu16 Lu3 49.2(8) . . ?
Lu10 Lu16 Lu3 109.8(13) . . ?
Lu6 Lu16 Lu3 62.2(7) . . ?
Lu9 Lu16 Lu16 149.4(16) . 6_565 ?
Lu1 Lu16 Lu16 144.4(13) . 6_565 ?
Lu10 Lu16 Lu16 76.5(13) . 6_565 ?
Lu6 Lu16 Lu16 101.3(8) . 6_565 ?
Lu3 Lu16 Lu16 111.1(7) . 6_565 ?
Lu9 Lu16 Lu14 82.9(16) . . ?
Lu1 Lu16 Lu14 51.5(10) . . ?
Lu10 Lu16 Lu14 130.0(14) . . ?
Lu6 Lu16 Lu14 40.9(6) . . ?
Lu3 Lu16 Lu14 26.4(4) . . ?
Lu16 Lu16 Lu14 97.0(8) 6_565 . ?
Lu9 Lu16 Lu10 120(2) . 6_565 ?
Lu1 Lu16 Lu10 165.5(15) . 6_565 ?
Lu10 Lu16 Lu10 42.8(11) . 6_565 ?
Lu6 Lu16 Lu10 134.4(14) . 6_565 ?
Lu3 Lu16 Lu10 116.4(10) . 6_565 ?
Lu16 Lu16 Lu10 33.7(7) 6_565 6_565 ?
Lu14 Lu16 Lu10 116.9(12) . 6_565 ?
Lu9 Lu16 Lu15 69.7(17) . . ?
Lu1 Lu16 Lu15 26.2(10) . . ?
Lu10 Lu16 Lu15 141.5(16) . . ?
Lu6 Lu16 Lu15 32.3(7) . . ?
Lu3 Lu16 Lu15 33.4(7) . . ?
Lu16 Lu16 Lu15 119.8(9) 6_565 . ?
Lu14 Lu16 Lu15 25.8(8) . . ?
Lu10 Lu16 Lu15 142.6(13) 6_565 . ?
Lu9 Lu16 Lu2 134(2) . . ?
Lu1 Lu16 Lu2 82.4(13) . . ?
Lu10 Lu16 Lu2 140.0(18) . . ?
Lu6 Lu16 Lu2 37.6(5) . . ?
Lu3 Lu16 Lu2 81.3(8) . . ?
Lu16 Lu16 Lu2 63.9(6) 6_565 . ?
Lu14 Lu16 Lu2 54.9(7) . . ?
Lu10 Lu16 Lu2 97.4(10) 6_565 . ?
Lu15 Lu16 Lu2 64.0(9) . . ?
Lu9 Lu16 Lu11 86.8(17) . . ?
Lu1 Lu16 Lu11 137.4(15) . . ?
Lu10 Lu16 Lu11 19.1(8) . . ?
Lu6 Lu16 Lu11 152.2(12) . . ?
Lu3 Lu16 Lu11 98.7(8) . . ?
Lu16 Lu16 Lu11 65.2(6) 6_565 . ?
Lu14 Lu16 Lu11 113.9(10) . . ?
Lu10 Lu16 Lu11 33.7(4) 6_565 . ?
Lu15 Lu16 Lu11 132.1(11) . . ?
Lu2 Lu16 Lu11 124.9(11) . . ?
Lu9 Lu16 C1 96.0(18) . . ?
Lu1 Lu16 C1 113.2(15) . . ?
Lu10 Lu16 C1 67.6(10) . . ?
Lu6 Lu16 C1 121.7(9) . . ?
Lu3 Lu16 C1 154.5(13) . . ?
Lu16 Lu16 C1 93.3(6) 6_565 . ?
Lu14 Lu16 C1 161.4(12) . . ?
Lu10 Lu16 C1 79.8(8) 6_565 . ?
Lu15 Lu16 C1 137.3(12) . . ?
Lu2 Lu16 C1 117.7(8) . . ?
Lu11 Lu16 C1 84.4(8) . . ?
C5 C1 C9 131.5 . . ?
C5 C1 C2 108.6 . . ?
C9 C1 C2 114.9 . . ?
C5 C1 Lu10 70.7(3) . . ?
C9 C1 Lu10 85.1(3) . . ?
C2 C1 Lu10 94.5(2) . . ?
C5 C1 Lu16 96.8(5) . . ?
C9 C1 Lu16 73.8(6) . . ?
C2 C1 Lu16 77.0(5) . . ?
Lu10 C1 Lu16 27.8(5) . . ?
C5 C1 Lu9 98.7(2) . . ?
C9 C1 Lu9 58.6(2) . . ?
C2 C1 Lu9 94.3(2) . . ?
Lu10 C1 Lu9 29.4(3) . . ?
Lu16 C1 Lu9 18.9(5) . . ?
C5 C1 Lu1 113.21(9) . . ?
C9 C1 Lu1 56.00(9) . . ?
C2 C1 Lu1 81.53(9) . . ?
Lu10 C1 Lu1 42.5(2) . . ?
Lu16 C1 Lu1 19.0(6) . . ?
Lu9 C1 Lu1 16.9(2) . . ?
C22 C21 C20 107.6 . . ?
C22 C21 C23 128.6 . . ?
C20 C21 C23 113.4 . . ?
C22 C21 C46 46.7 . . ?
C20 C21 C46 138.6 . . ?
C23 C21 C46 81.9 . . ?
C22 C21 Lu11 94.3(3) . . ?
C20 C21 Lu11 62.6(3) . . ?
C23 C21 Lu11 78.97(16) . . ?
C46 C21 Lu11 85.0(4) . . ?
C22 C21 Lu10 113.99(19) . . ?
C20 C21 Lu10 64.72(19) . . ?
C23 C21 Lu10 61.9(2) . . ?
C46 C21 Lu10 94.17(16) . . ?
Lu11 C21 Lu10 20.8(3) . . ?
C21 C22 C43 125.1 . . ?
C21 C22 C46 90.5 . . ?
C43 C22 C46 113.5 . . ?
C21 C22 Lu11 55.9(2) . . ?
C43 C22 Lu11 78.83(13) . . ?
C46 C22 Lu11 81.1(2) . . ?
C12 C2 C3 129.3 . . ?
C12 C2 C1 121.2 . . ?
C3 C2 C1 103.9 . . ?
C12 C2 Lu16 81.3(5) . . ?
C3 C2 Lu16 96.6(5) . . ?
C1 C2 Lu16 68.1(5) . . ?
C12 C2 Lu10 105.23(19) . . ?
C3 C2 Lu10 82.9(2) . . ?
C1 C2 Lu10 53.34(19) . . ?
Lu16 C2 Lu10 24.0(5) . . ?
C15 C3 C2 112.8 . . ?
C15 C3 C4 132.1 . . ?
C2 C3 C4 112.2 . . ?
C15 C3 Lu10 120.06(17) . . ?
C2 C3 Lu10 67.7(2) . . ?
C4 C3 Lu10 64.88(17) . . ?
C18 C4 C5 125.9 . . ?
C18 C4 C3 121.3 . . ?
C5 C4 C3 104.7 . . ?
C18 C4 Lu10 99.0(2) . . ?
C5 C4 Lu10 55.6(2) . . ?
C3 C4 Lu10 85.45(18) . . ?
C18 C4 Lu11 73.88(18) . . ?
C5 C4 Lu11 66.56(17) . . ?
C3 C4 Lu11 106.7(2) . . ?
Lu10 C4 Lu11 27.0(2) . . ?
C6 C5 C4 125.6 . . ?
C6 C5 C1 116.0 . . ?
C4 C5 C1 110.5 . . ?
C6 C5 Lu10 78.2(2) . . ?
C4 C5 Lu10 92.4(3) . . ?
C1 C5 Lu10 70.7(3) . . ?
C6 C5 Lu11 63.4(2) . . ?
C4 C5 Lu11 81.91(13) . . ?
C1 C5 Lu11 100.8(2) . . ?
Lu10 C5 Lu11 30.1(3) . . ?
C6 C5 Lu16 94.5(4) . . ?
C4 C5 Lu16 91.0(5) . . ?
C1 C5 Lu16 53.6(4) . . ?
Lu10 C5 Lu16 19.1(4) . . ?
Lu11 C5 Lu16 48.1(4) . . ?
C5 C6 C20 110.1 . . ?
C5 C6 C7 124.8 . . ?
C20 C6 C7 113.5 . . ?
C5 C6 Lu11 86.4(3) . . ?
C20 C6 Lu11 59.2(2) . . ?
C7 C6 Lu11 88.16(19) . . ?
C5 C6 Lu10 69.7(2) . . ?
C20 C6 Lu10 90.9(3) . . ?
C7 C6 Lu10 77.5(3) . . ?
Lu11 C6 Lu10 31.9(3) . . ?
C6 C7 C23 104.0 . . ?
C6 C7 C8 118.1 . . ?
C23 C7 C8 121.1 . . ?
C6 C7 Lu10 68.4(2) . . ?
C23 C7 Lu10 82.4(2) . . ?
C8 C7 Lu10 77.5(3) . . ?
C6 C7 Lu11 59.3(3) . . ?
C23 C7 Lu11 62.4(3) . . ?
C8 C7 Lu11 105.4(2) . . ?
Lu10 C7 Lu11 28.6(3) . . ?
C6 C7 Lu9 93.3(2) . . ?
C23 C7 Lu9 85.0(2) . . ?
C8 C7 Lu9 55.1(2) . . ?
Lu10 C7 Lu9 26.7(3) . . ?
Lu11 C7 Lu9 51.2(3) . . ?
C26 C8 C7 125.1 . . ?
C26 C8 C9 96.5 . . ?
C7 C8 C9 124.7 . . ?
C26 C8 Lu9 68.5(3) . . ?
C7 C8 Lu9 93.9(3) . . ?
C9 C8 Lu9 67.0(3) . . ?
C26 C8 Lu10 96.5(2) . . ?
C7 C8 Lu10 68.2(2) . . ?
C9 C8 Lu10 72.9(2) . . ?
Lu9 C8 Lu10 30.1(3) . . ?
C26 C8 Lu16 82.0(4) . . ?
C7 C8 Lu16 90.9(4) . . ?
C9 C8 Lu16 57.5(4) . . ?
Lu9 C8 Lu16 14.8(4) . . ?
Lu10 C8 Lu16 22.8(5) . . ?
C26 C8 Lu1 62.72(10) . . ?
C7 C8 Lu1 108.14(9) . . ?
C9 C8 Lu1 56.99(8) . . ?
Lu9 C8 Lu1 14.5(2) . . ?
Lu10 C8 Lu1 42.0(2) . . ?
Lu16 C8 Lu1 20.8(5) . . ?
C1 C9 C10 123.6 . . ?
C1 C9 C8 104.4 . . ?
C10 C9 C8 123.0 . . ?
C1 C9 Lu9 87.4(3) . . ?
C10 C9 Lu9 77.9(3) . . ?
C8 C9 Lu9 75.2(3) . . ?
C1 C9 Lu16 70.8(5) . . ?
C10 C9 Lu16 78.7(5) . . ?
C8 C9 Lu16 91.4(5) . . ?
Lu9 C9 Lu16 20.6(5) . . ?
C1 C9 Lu1 94.47(12) . . ?
C10 C9 Lu1 57.75(11) . . ?
C8 C9 Lu1 92.57(10) . . ?
Lu9 C9 Lu1 21.0(2) . . ?
Lu16 C9 Lu1 24.8(5) . . ?
C1 C9 Lu10 60.0(2) . . ?
C10 C9 Lu10 103.94(19) . . ?
C8 C9 Lu10 73.2(2) . . ?
Lu9 C9 Lu10 30.3(3) . . ?
Lu16 C9 Lu10 25.8(5) . . ?
Lu1 C9 Lu10 46.99(19) . . ?
C9 C10 C11 122.4 . . ?
C9 C10 C27 96.2 . . ?
C11 C10 C27 124.2 . . ?
C9 C10 Lu1 85.44(14) . . ?
C11 C10 Lu1 76.08(12) . . ?
C27 C10 Lu1 67.97(13) . . ?
C9 C10 Lu9 65.2(2) . . ?
C11 C10 Lu9 93.0(2) . . ?
C27 C10 Lu9 66.6(3) . . ?
Lu1 C10 Lu9 21.23(18) . . ?
C9 C10 Lu16 67.1(5) . . ?
C11 C10 Lu16 76.8(5) . . ?
C27 C10 Lu16 84.8(5) . . ?
Lu1 C10 Lu16 23.0(5) . . ?
Lu9 C10 Lu16 19.3(4) . . ?
C9 C10 Lu6 105.73(12) . . ?
C11 C10 Lu6 48.96(11) . . ?
C27 C10 Lu6 85.01(13) . . ?
Lu1 C10 Lu6 27.89(12) . . ?
Lu9 C10 Lu6 47.8(2) . . ?
Lu16 C10 Lu6 38.9(5) . . ?
C9 C10 Lu15 108.7(4) . . ?
C11 C10 Lu15 68.1(4) . . ?
C27 C10 Lu15 61.7(5) . . ?
Lu1 C10 Lu15 23.8(4) . . ?
Lu9 C10 Lu15 43.6(5) . . ?
Lu16 C10 Lu15 45.8(7) . . ?
Lu6 C10 Lu15 23.5(5) . . ?
C10 C11 C12 110.2 . . ?
C10 C11 C32 113.6 . . ?
C12 C11 C32 131.5 . . ?
C10 C11 Lu6 95.76(17) . . ?
C12 C11 Lu6 92.92(18) . . ?
C32 C11 Lu6 63.51(16) . . ?
C10 C11 Lu1 63.70(11) . . ?
C12 C11 Lu1 96.95(13) . . ?
C32 C11 Lu1 84.86(13) . . ?
Lu6 C11 Lu1 32.87(15) . . ?
C10 C11 Lu2 116.41(9) . . ?
C12 C11 Lu2 68.06(11) . . ?
C32 C11 Lu2 74.67(11) . . ?
Lu6 C11 Lu2 28.38(15) . . ?
Lu1 C11 Lu2 54.17(11) . . ?
C10 C11 Lu16 70.0(5) . . ?
C12 C11 Lu16 74.6(5) . . ?
C32 C11 Lu16 102.0(4) . . ?
Lu6 C11 Lu16 40.0(5) . . ?
Lu1 C11 Lu16 22.6(5) . . ?
Lu2 C11 Lu16 47.6(5) . . ?
C10 C11 Lu15 80.9(5) . . ?
C12 C11 Lu15 113.2(5) . . ?
C32 C11 Lu15 56.7(5) . . ?
Lu6 C11 Lu15 21.9(5) . . ?
Lu1 C11 Lu15 28.2(5) . . ?
Lu2 C11 Lu15 50.2(5) . . ?
Lu16 C11 Lu15 46.9(6) . . ?
C10 C11 Lu9 55.89(17) . . ?
C12 C11 Lu9 89.5(2) . . ?
C32 C11 Lu9 98.38(19) . . ?
Lu6 C11 Lu9 44.3(2) . . ?
Lu1 C11 Lu9 13.67(17) . . ?
Lu2 C11 Lu9 60.52(18) . . ?
Lu16 C11 Lu9 17.0(5) . . ?
Lu15 C11 Lu9 41.9(5) . . ?
C2 C12 C11 125.4 . . ?
C2 C12 C13 115.6 . . ?
C11 C12 C13 109.9 . . ?
C2 C12 Lu2 99.36(10) . . ?
C11 C12 Lu2 78.14(11) . . ?
C13 C12 Lu2 60.20(10) . . ?
C2 C12 Lu6 104.33(12) . . ?
C11 C12 Lu6 50.70(14) . . ?
C13 C12 Lu6 85.37(14) . . ?
Lu2 C12 Lu6 30.12(11) . . ?
C2 C12 Lu16 66.5(5) . . ?
C11 C12 Lu16 72.9(5) . . ?
C13 C12 Lu16 106.6(5) . . ?
Lu2 C12 Lu16 48.6(5) . . ?
Lu6 C12 Lu16 38.3(5) . . ?
C2 C12 Lu1 85.35(10) . . ?
C11 C12 Lu1 51.59(10) . . ?
C13 C12 Lu1 108.87(9) . . ?
Lu2 C12 Lu1 49.23(9) . . ?
Lu6 C12 Lu1 25.38(12) . . ?
Lu16 C12 Lu1 21.5(5) . . ?
C34 C13 C14 114.6 . . ?
C34 C13 C12 123.3 . . ?
C14 C13 C12 113.6 . . ?
C34 C13 Lu2 67.13(12) . . ?
C14 C13 Lu2 93.25(12) . . ?
C12 C13 Lu2 82.10(12) . . ?
C34 C13 Lu6 71.31(12) . . ?
C14 C13 Lu6 115.65(11) . . ?
C12 C13 Lu6 61.97(12) . . ?
Lu2 C13 Lu6 26.05(11) . . ?
C36 C14 C13 94.4 . . ?
C36 C14 C15 124.3 . . ?
C13 C14 C15 125.9 . . ?
C36 C14 Lu2 73.43(10) . . ?
C13 C14 Lu2 54.39(9) . . ?
C15 C14 Lu2 98.50(9) . . ?
C3 C15 C14 121.6 . . ?
C3 C15 C16 98.1 . . ?
C14 C15 C16 134.7 . . ?
C17 C16 C15 121.7 . . ?
C17 C16 C38 131.5 . . ?
C15 C16 C38 81.3 . . ?
C16 C17 C40 109.3 . . ?
C16 C17 C18 135.8 . . ?
C40 C17 C18 111.7 . . ?
C4 C18 C19 110.5 . . ?
C4 C18 C17 107.6 . . ?
C19 C18 C17 136.1 . . ?
C4 C18 Lu11 77.9(3) . . ?
C19 C18 Lu11 57.2(2) . . ?
C17 C18 Lu11 112.3(2) . . ?
C42 C19 C18 109.4 . . ?
C42 C19 C20 122.6 . . ?
C18 C19 C20 121.7 . . ?
C42 C19 Lu11 97.1(3) . . ?
C18 C19 Lu11 91.6(3) . . ?
C20 C19 Lu11 59.6(2) . . ?
C21 C20 C6 100.6 . . ?
C21 C20 C19 126.6 . . ?
C6 C20 C19 125.9 . . ?
C21 C20 Lu11 78.7(4) . . ?
C6 C20 Lu11 83.2(3) . . ?
C19 C20 Lu11 82.21(16) . . ?
C21 C20 Lu10 88.2(2) . . ?
C6 C20 Lu10 58.7(2) . . ?
C19 C20 Lu10 94.6(2) . . ?
Lu11 C20 Lu10 24.9(4) . . ?
C21 C23 C7 103.2 . . ?
C21 C23 C24 142.5 . . ?
C7 C23 C24 114.1 . . ?
C21 C23 C47 100.2 . . ?
C7 C23 C47 153.8 . . ?
C24 C23 C47 42.6 . . ?
C21 C23 Lu11 65.1(2) . . ?
C7 C23 Lu11 85.0(4) . . ?
C24 C23 Lu11 113.1(3) . . ?
C47 C23 Lu11 94.4(4) . . ?
C21 C23 Lu10 90.6(2) . . ?
C7 C23 Lu10 65.77(19) . . ?
C24 C23 Lu10 100.8(2) . . ?
C47 C23 Lu10 102.62(18) . . ?
Lu11 C23 Lu10 28.3(3) . . ?
C47 C24 C25 133.8 . . ?
C47 C24 C23 86.7 . . ?
C25 C24 C23 123.5 . . ?
C24 C25 C50 119.3 . . ?
C24 C25 C26 118.8 . . ?
C50 C25 C26 112.3 . . ?
C24 C25 Lu9 91.5(2) . . ?
C50 C25 Lu9 90.93(19) . . ?
C26 C25 Lu9 56.2(2) . . ?
C8 C26 C27 113.1 . . ?
C8 C26 C25 113.5 . . ?
C27 C26 C25 121.5 . . ?
C8 C26 Lu9 74.4(3) . . ?
C27 C26 Lu9 71.3(3) . . ?
C25 C26 Lu9 89.4(3) . . ?
C8 C26 Lu1 87.27(11) . . ?
C27 C26 Lu1 52.26(11) . . ?
C25 C26 Lu1 97.49(9) . . ?
Lu9 C26 Lu1 19.3(2) . . ?
C28 C27 C26 123.2 . . ?
C28 C27 C10 119.4 . . ?
C26 C27 C10 111.2 . . ?
C28 C27 Lu1 82.17(14) . . ?
C26 C27 Lu1 93.13(13) . . ?
C10 C27 Lu1 69.54(12) . . ?
C28 C27 Lu9 97.5(2) . . ?
C26 C27 Lu9 70.5(3) . . ?
C10 C27 Lu9 76.0(3) . . ?
Lu1 C27 Lu9 22.9(2) . . ?
C28 C27 Lu15 52.0(5) . . ?
C26 C27 Lu15 110.5(5) . . ?
C10 C27 Lu15 86.9(5) . . ?
Lu1 C27 Lu15 30.3(5) . . ?
Lu9 C27 Lu15 49.0(5) . . ?
C28 C27 Lu16 97.9(4) . . ?
C26 C27 Lu16 82.0(4) . . ?
C10 C27 Lu16 63.7(4) . . ?
Lu1 C27 Lu16 16.0(4) . . ?
Lu9 C27 Lu16 13.8(4) . . ?
Lu15 C27 Lu16 46.2(7) . . ?
C28 C27 Lu6 70.52(12) . . ?
C26 C27 Lu6 114.83(10) . . ?
C10 C27 Lu6 63.62(11) . . ?
Lu1 C27 Lu6 21.71(12) . . ?
Lu9 C27 Lu6 44.5(3) . . ?
Lu15 C27 Lu6 23.4(5) . . ?
Lu16 C27 Lu6 34.9(4) . . ?
C28 C27 Lu3 64.34(12) . . ?
C26 C27 Lu3 86.89(13) . . ?
C10 C27 Lu3 96.29(11) . . ?
Lu1 C27 Lu3 27.02(12) . . ?
Lu9 C27 Lu3 33.4(2) . . ?
Lu15 C27 Lu3 23.6(5) . . ?
Lu16 C27 Lu3 38.0(4) . . ?
Lu6 C27 Lu3 37.51(13) . . ?
C27 C28 C29 117.1 . . ?
C27 C28 C51 116.8 . . ?
C29 C28 C51 110.4 . . ?
C27 C28 Lu15 92.8(7) . . ?
C29 C28 Lu15 56.1(6) . . ?
C51 C28 Lu15 80.8(7) . . ?
C27 C28 Lu1 59.94(11) . . ?
C29 C28 Lu1 77.91(11) . . ?
C51 C28 Lu1 94.24(10) . . ?
Lu15 C28 Lu1 33.0(7) . . ?
C27 C28 Lu3 85.77(14) . . ?
C29 C28 Lu3 80.22(14) . . ?
C51 C28 Lu3 63.44(13) . . ?
Lu15 C28 Lu3 24.8(6) . . ?
Lu1 C28 Lu3 32.75(13) . . ?
C27 C28 Lu6 79.47(13) . . ?
C29 C28 Lu6 51.66(11) . . ?
C51 C28 Lu6 101.41(11) . . ?
Lu15 C28 Lu6 21.1(7) . . ?
Lu1 C28 Lu6 26.28(11) . . ?
Lu3 C28 Lu6 40.35(14) . . ?
C27 C28 Lu9 51.98(17) . . ?
C29 C28 Lu9 93.9(2) . . ?
C51 C28 Lu9 86.8(2) . . ?
Lu15 C28 Lu9 44.6(7) . . ?
Lu1 C28 Lu9 16.1(2) . . ?
Lu3 C28 Lu9 34.0(2) . . ?
Lu6 C28 Lu9 42.3(2) . . ?
C27 C28 Lu14 91.0(2) . . ?
C29 C28 Lu14 63.2(2) . . ?
C51 C28 Lu14 75.3(2) . . ?
Lu15 C28 Lu14 7.4(6) . . ?
Lu1 C28 Lu14 31.4(2) . . ?
Lu3 C28 Lu14 17.4(2) . . ?
Lu6 C28 Lu14 26.1(3) . . ?
Lu9 C28 Lu14 40.6(3) . . ?
C28 C29 C32 123.1 . . ?
C28 C29 C30 125.0 . . ?
C32 C29 C30 105.7 . . ?
C28 C29 Lu15 76.9(8) . . ?
C32 C29 Lu15 89.2(8) . . ?
C30 C29 Lu15 80.2(9) . . ?
C28 C29 Lu6 95.53(15) . . ?
C32 C29 Lu6 57.69(13) . . ?
C30 C29 Lu6 89.76(16) . . ?
Lu15 C29 Lu6 31.5(8) . . ?
C28 C29 Lu1 66.43(11) . . ?
C32 C29 Lu1 76.05(10) . . ?
C30 C29 Lu1 107.20(10) . . ?
Lu15 C29 Lu1 27.7(9) . . ?
Lu6 C29 Lu1 29.14(14) . . ?
C28 C29 Lu14 85.5(3) . . ?
C32 C29 Lu14 86.4(3) . . ?
C30 C29 Lu14 73.0(3) . . ?
Lu15 C29 Lu14 8.9(9) . . ?
Lu6 C29 Lu14 29.8(3) . . ?
Lu1 C29 Lu14 34.2(3) . . ?
C28 C29 Lu3 68.04(13) . . ?
C32 C29 Lu3 99.04(12) . . ?
C30 C29 Lu3 81.66(13) . . ?
Lu15 C29 Lu3 10.6(8) . . ?
Lu6 C29 Lu3 41.56(15) . . ?
Lu1 C29 Lu3 30.68(12) . . ?
Lu14 C29 Lu3 17.8(3) . . ?
C31 C30 C53 130.1 . . ?
C31 C30 C29 101.2 . . ?
C53 C30 C29 119.7 . . ?
C31 C30 Lu15 97.8(6) . . ?
C53 C30 Lu15 87.9(6) . . ?
C29 C30 Lu15 51.5(7) . . ?
C31 C30 Lu14 89.8(3) . . ?
C53 C30 Lu14 79.4(3) . . ?
C29 C30 Lu14 70.5(3) . . ?
Lu15 C30 Lu14 19.6(7) . . ?
C31 C30 Lu6 74.49(12) . . ?
C53 C30 Lu6 106.94(10) . . ?
C29 C30 Lu6 53.33(13) . . ?
Lu15 C30 Lu6 23.9(6) . . ?
Lu14 C30 Lu6 27.7(3) . . ?
C56 C31 C30 113.7 . . ?
C56 C31 C33 115.5 . . ?
C30 C31 C33 114.8 . . ?
C56 C31 Lu6 99.77(13) . . ?
C30 C31 Lu6 74.44(13) . . ?
C33 C31 Lu6 57.58(11) . . ?
C56 C31 Lu15 103.7(5) . . ?
C30 C31 Lu15 50.7(5) . . ?
C33 C31 Lu15 78.0(5) . . ?
Lu6 C31 Lu15 24.2(5) . . ?
C56 C31 Lu2 78.08(9) . . ?
C30 C31 Lu2 97.02(8) . . ?
C33 C31 Lu2 56.36(8) . . ?
Lu6 C31 Lu2 26.49(10) . . ?
Lu15 C31 Lu2 47.0(5) . . ?
C56 C31 Lu14 85.9(3) . . ?
C30 C31 Lu14 61.1(3) . . ?
C33 C31 Lu14 82.8(2) . . ?
Lu6 C31 Lu14 25.4(2) . . ?
Lu15 C31 Lu14 18.1(5) . . ?
Lu2 C31 Lu14 37.1(2) . . ?
C33 C32 C29 119.2 . . ?
C33 C32 C11 111.8 . . ?
C29 C32 C11 119.1 . . ?
C33 C32 Lu6 89.24(19) . . ?
C29 C32 Lu6 79.40(18) . . ?
C11 C32 Lu6 69.91(18) . . ?
C33 C32 Lu15 104.1(7) . . ?
C29 C32 Lu15 49.0(6) . . ?
C11 C32 Lu15 89.2(6) . . ?
Lu6 C32 Lu15 30.4(6) . . ?
C33 C32 Lu1 114.84(10) . . ?
C29 C32 Lu1 69.82(11) . . ?
C11 C32 Lu1 59.68(10) . . ?
Lu6 C32 Lu1 25.72(17) . . ?
Lu15 C32 Lu1 29.5(6) . . ?
C33 C32 Lu2 64.98(9) . . ?
C29 C32 Lu2 100.85(9) . . ?
C11 C32 Lu2 72.22(10) . . ?
Lu6 C32 Lu2 26.59(16) . . ?
Lu15 C32 Lu2 53.9(6) . . ?
Lu1 C32 Lu2 50.59(10) . . ?
C33 C32 Lu14 91.4(3) . . ?
C29 C32 Lu14 62.4(3) . . ?
C11 C32 Lu14 86.3(2) . . ?
Lu6 C32 Lu14 18.7(3) . . ?
Lu15 C32 Lu14 15.1(7) . . ?
Lu1 C32 Lu14 31.0(2) . . ?
Lu2 C32 Lu14 39.2(3) . . ?
C32 C33 C34 123.9 . . ?
C32 C33 C31 98.8 . . ?
C34 C33 C31 118.4 . . ?
C32 C33 Lu6 54.37(16) . . ?
C34 C33 Lu6 87.37(15) . . ?
C31 C33 Lu6 84.37(15) . . ?
C32 C33 Lu2 84.55(11) . . ?
C34 C33 Lu2 58.16(10) . . ?
C31 C33 Lu2 88.66(11) . . ?
Lu6 C33 Lu2 31.91(12) . . ?
C32 C33 Lu15 48.9(5) . . ?
C34 C33 Lu15 107.2(5) . . ?
C31 C33 Lu15 67.6(5) . . ?
Lu6 C33 Lu15 21.7(5) . . ?
Lu2 C33 Lu15 49.3(5) . . ?
C35 C34 C13 116.6 . . ?
C35 C34 C33 114.9 . . ?
C13 C34 C33 118.2 . . ?
C35 C34 Lu2 82.41(13) . . ?
C13 C34 Lu2 74.63(14) . . ?
C33 C34 Lu2 80.80(13) . . ?
C35 C34 Lu6 104.04(12) . . ?
C13 C34 Lu6 79.67(12) . . ?
C33 C34 Lu6 56.57(12) . . ?
Lu2 C34 Lu6 27.30(10) . . ?
C34 C35 C57 122.6 . . ?
C34 C35 C36 94.2 . . ?
C57 C35 C36 132.7 . . ?
C34 C35 Lu2 64.44(11) . . ?
C57 C35 Lu2 87.34(12) . . ?
C36 C35 Lu2 82.96(12) . . ?
C14 C36 C37 108.6 . . ?
C14 C36 C35 118.7 . . ?
C37 C36 C35 119.5 . . ?
C14 C36 Lu2 76.66(11) . . ?
C37 C36 Lu2 101.11(9) . . ?
C35 C36 Lu2 59.48(10) . . ?
C38 C37 C36 117.2 . . ?
C38 C37 C59 120.1 . . ?
C36 C37 C59 116.5 . . ?
C37 C38 C16 149.3 . . ?
C37 C38 C39 118.5 . . ?
C16 C38 C39 77.5 . . ?
C61 C39 C38 123.6 . . ?
C61 C39 C40 103.3 . . ?
C38 C39 C40 118.1 . . ?
C17 C40 C41 112.5 . . ?
C17 C40 C39 98.1 . . ?
C41 C40 C39 140.8 . . ?
C63 C41 C40 101.8 . . ?
C63 C41 C42 120.4 . . ?
C40 C41 C42 134.8 . . ?
C41 C42 C19 113.4 . . ?
C41 C42 C43 117.5 . . ?
C19 C42 C43 106.7 . . ?
C41 C42 Lu11 96.12(19) . . ?
C19 C42 Lu11 53.5(3) . . ?
C43 C42 Lu11 71.8(3) . . ?
C22 C43 C44 102.6 . . ?
C22 C43 C42 126.9 . . ?
C44 C43 C42 125.9 . . ?
C22 C43 Lu11 71.68(15) . . ?
C44 C43 Lu11 100.6(3) . . ?
C42 C43 Lu11 78.7(2) . . ?
C64 C44 C43 108.1 . . ?
C64 C44 C45 136.4 . . ?
C43 C44 C45 108.8 . . ?
C44 C45 C67 110.8 . . ?
C44 C45 C46 110.6 . . ?
C67 C45 C46 125.4 . . ?
C44 C45 Lu8 91.95(15) . . ?
C67 C45 Lu8 45.2(3) . . ?
C46 C45 Lu8 100.0(2) . . ?
C45 C46 C22 98.3 . . ?
C45 C46 C47 117.5 . . ?
C22 C46 C47 142.6 . . ?
C45 C46 C21 135.7 . . ?
C22 C46 C21 42.8 . . ?
C47 C46 C21 100.1 . . ?
C45 C46 Lu11 101.9(2) . . ?
C22 C46 Lu11 69.0(2) . . ?
C47 C46 Lu11 92.08(14) . . ?
C21 C46 Lu11 51.4(3) . . ?
C24 C47 C48 109.4 . . ?
C24 C47 C46 128.3 . . ?
C48 C47 C46 114.9 . . ?
C24 C47 C23 50.8 . . ?
C48 C47 C23 145.5 . . ?
C46 C47 C23 77.5 . . ?
C24 C47 Lu5 95.18(15) . . ?
C48 C47 Lu5 55.98(11) . . ?
C46 C47 Lu5 88.39(14) . . ?
C23 C47 Lu5 94.49(12) . . ?
C68 C48 C47 124.3 . . ?
C68 C48 C49 107.2 . . ?
C47 C48 C49 123.0 . . ?
C68 C48 Lu5 74.31(19) . . ?
C47 C48 Lu5 93.50(16) . . ?
C49 C48 Lu5 77.30(17) . . ?
C68 C48 Lu8 49.8(3) . . ?
C47 C48 Lu8 103.0(3) . . ?
C49 C48 Lu8 91.6(3) . . ?
Lu5 C48 Lu8 25.1(3) . . ?
C50 C49 C71 105.7 . . ?
C50 C49 C48 121.9 . . ?
C71 C49 C48 122.0 . . ?
C50 C49 Lu5 99.48(16) . . ?
C71 C49 Lu5 78.41(16) . . ?
C48 C49 Lu5 63.81(14) . . ?
C50 C49 Lu13 94.5(3) . . ?
C71 C49 Lu13 58.2(3) . . ?
C48 C49 Lu13 85.4(3) . . ?
Lu5 C49 Lu13 22.8(3) . . ?
C50 C49 Lu3 68.69(13) . . ?
C71 C49 Lu3 70.86(13) . . ?
C48 C49 Lu3 96.19(12) . . ?
Lu5 C49 Lu3 35.96(14) . . ?
Lu13 C49 Lu3 26.0(3) . . ?
C49 C50 C25 111.8 . . ?
C49 C50 C51 108.2 . . ?
C25 C50 C51 126.8 . . ?
C49 C50 Lu3 81.98(13) . . ?
C25 C50 Lu3 90.67(14) . . ?
C51 C50 Lu3 61.63(13) . . ?
C50 C51 C52 111.2 . . ?
C50 C51 C28 118.0 . . ?
C52 C51 C28 124.1 . . ?
C50 C51 Lu15 111.1(5) . . ?
C52 C51 Lu15 80.4(7) . . ?
C28 C51 Lu15 59.0(6) . . ?
C50 C51 Lu3 85.20(16) . . ?
C52 C51 Lu3 77.11(16) . . ?
C28 C51 Lu3 82.21(14) . . ?
Lu15 C51 Lu3 29.1(5) . . ?
C50 C51 Lu14 100.7(2) . . ?
C52 C51 Lu14 72.1(2) . . ?
C28 C51 Lu14 74.4(2) . . ?
Lu15 C51 Lu14 16.1(6) . . ?
Lu3 C51 Lu14 15.5(2) . . ?
C50 C51 Lu1 90.77(10) . . ?
C52 C51 Lu1 102.16(9) . . ?
C28 C51 Lu1 54.45(9) . . ?
Lu15 C51 Lu1 25.5(6) . . ?
Lu3 C51 Lu1 29.69(13) . . ?
Lu14 C51 Lu1 30.1(2) . . ?
C71 C52 C53 124.1 . . ?
C71 C52 C51 101.8 . . ?
C53 C52 C51 126.2 . . ?
C71 C52 Lu3 83.85(14) . . ?
C53 C52 Lu3 89.60(15) . . ?
C51 C52 Lu3 67.40(15) . . ?
C71 C52 Lu15 110.9(5) . . ?
C53 C52 Lu15 74.0(5) . . ?
C51 C52 Lu15 63.8(6) . . ?
Lu3 C52 Lu15 27.0(5) . . ?
C71 C52 Lu13 62.6(3) . . ?
C53 C52 Lu13 86.7(3) . . ?
C51 C52 Lu13 91.9(3) . . ?
Lu3 C52 Lu13 28.9(3) . . ?
Lu15 C52 Lu13 51.9(6) . . ?
C71 C52 Lu14 95.8(2) . . ?
C53 C52 Lu14 72.2(2) . . ?
C51 C52 Lu14 77.4(3) . . ?
Lu3 C52 Lu14 17.6(2) . . ?
Lu15 C52 Lu14 19.1(5) . . ?
Lu13 C52 Lu14 34.0(4) . . ?
C54 C53 C30 114.0 . . ?
C54 C53 C52 116.7 . . ?
C30 C53 C52 114.2 . . ?
C54 C53 Lu15 103.5(6) . . ?
C30 C53 Lu15 57.1(5) . . ?
C52 C53 Lu15 72.4(5) . . ?
C54 C53 Lu14 84.2(3) . . ?
C30 C53 Lu14 69.0(2) . . ?
C52 C53 Lu14 77.2(3) . . ?
Lu15 C53 Lu14 19.7(5) . . ?
C54 C53 Lu7 46.6(3) . . ?
C30 C53 Lu7 91.2(3) . . ?
C52 C53 Lu7 94.5(3) . . ?
Lu15 C53 Lu7 57.3(6) . . ?
Lu14 C53 Lu7 37.7(4) . . ?
C54 C53 Lu13 69.6(3) . . ?
C30 C53 Lu13 101.8(2) . . ?
C52 C53 Lu13 62.5(3) . . ?
Lu15 C53 Lu13 47.9(6) . . ?
Lu14 C53 Lu13 32.8(3) . . ?
Lu7 C53 Lu13 32.1(4) . . ?
C54 C53 Lu3 90.74(12) . . ?
C30 C53 Lu3 80.61(12) . . ?
C52 C53 Lu3 60.07(12) . . ?
Lu15 C53 Lu3 23.8(5) . . ?
Lu14 C53 Lu3 17.3(2) . . ?
Lu7 C53 Lu3 45.6(3) . . ?
Lu13 C53 Lu3 25.3(3) . . ?
C53 C54 C72 116.0 . . ?
C53 C54 C55 116.7 . . ?
C72 C54 C55 123.9 . . ?
C53 C54 Lu7 104.5(3) . . ?
C72 C54 Lu7 77.9(4) . . ?
C55 C54 Lu7 71.8(3) . . ?
C53 C54 Lu13 81.1(3) . . ?
C72 C54 Lu13 65.0(3) . . ?
C55 C54 Lu13 106.1(3) . . ?
Lu7 C54 Lu13 35.5(4) . . ?
C53 C54 Lu14 67.3(2) . . ?
C72 C54 Lu14 96.9(2) . . ?
C55 C54 Lu14 86.5(3) . . ?
Lu7 C54 Lu14 37.3(4) . . ?
Lu13 C54 Lu14 32.1(3) . . ?
C56 C55 C74 123.4 . . ?
C56 C55 C54 126.6 . . ?
C74 C55 C54 100.2 . . ?
C56 C55 Lu7 99.3(4) . . ?
C74 C55 Lu7 67.6(2) . . ?
C54 C55 Lu7 68.2(2) . . ?
C55 C56 C31 117.7 . . ?
C55 C56 C57 121.6 . . ?
C31 C56 C57 111.3 . . ?
C55 C56 Lu7 50.5(3) . . ?
C31 C56 Lu7 99.90(18) . . ?
C57 C56 Lu7 92.6(2) . . ?
C55 C56 Lu2 104.58(8) . . ?
C31 C56 Lu2 73.70(9) . . ?
C57 C56 Lu2 60.95(9) . . ?
Lu7 C56 Lu2 54.1(3) . . ?
C35 C57 C56 136.4 . . ?
C35 C57 C58 106.0 . . ?
C56 C57 C58 110.5 . . ?
C35 C57 Lu2 61.98(10) . . ?
C56 C57 Lu2 89.88(11) . . ?
C58 C57 Lu2 97.70(10) . . ?
C75 C58 C57 128.6 . . ?
C75 C58 C59 93.2 . . ?
C57 C58 C59 130.9 . . ?
C60 C59 C37 113.6 . . ?
C60 C59 C58 120.0 . . ?
C37 C59 C58 113.0 . . ?
C59 C60 C76 107.2 . . ?
C59 C60 C61 126.2 . . ?
C76 C60 C61 116.9 . . ?
C39 C61 C62 124.9 . . ?
C39 C61 C60 117.0 . . ?
C62 C61 C60 112.3 . . ?
C63 C62 C78 103.6 . . ?
C63 C62 C61 122.4 . . ?
C78 C62 C61 127.8 . . ?
C41 C63 C64 115.2 . . ?
C41 C63 C62 125.8 . . ?
C64 C63 C62 112.3 . . ?
C44 C64 C63 129.7 . . ?
C44 C64 C65 109.6 . . ?
C63 C64 C65 106.6 . . ?
C64 C65 C78 107.9 . . ?
C64 C65 C66 117.1 . . ?
C78 C65 C66 126.0 . . ?
C64 C65 Lu4 102.61(13) . . ?
C78 C65 Lu4 76.96(14) . . ?
C66 C65 Lu4 65.73(15) . . ?
C64 C65 Lu8 104.0(3) . . ?
C78 C65 Lu8 92.8(3) . . ?
C66 C65 Lu8 49.6(3) . . ?
Lu4 C65 Lu8 17.1(3) . . ?
C67 C66 C65 124.1 . . ?
C67 C66 C80 112.8 . . ?
C65 C66 C80 114.4 . . ?
C67 C66 Lu8 76.6(4) . . ?
C65 C66 Lu8 96.2(3) . . ?
C80 C66 Lu8 66.6(4) . . ?
C67 C66 Lu4 91.35(15) . . ?
C65 C66 Lu4 79.94(17) . . ?
C80 C66 Lu4 68.21(15) . . ?
Lu8 C66 Lu4 17.6(2) . . ?
C67 C66 Lu12 85.7(5) . . ?
C65 C66 Lu12 90.4(3) . . ?
C80 C66 Lu12 62.7(6) . . ?
Lu8 C66 Lu12 9.1(6) . . ?
Lu4 C66 Lu12 10.5(3) . . ?
C66 C67 C45 121.3 . . ?
C66 C67 C68 116.8 . . ?
C45 C67 C68 116.7 . . ?
C66 C67 Lu8 67.4(3) . . ?
C45 C67 Lu8 107.2(4) . . ?
C68 C67 Lu8 73.88(19) . . ?
C66 C67 Lu5 92.70(16) . . ?
C45 C67 Lu5 93.69(14) . . ?
C68 C67 Lu5 60.22(13) . . ?
Lu8 C67 Lu5 25.3(3) . . ?
C66 C67 Lu4 60.83(12) . . ?
C45 C67 Lu4 102.56(12) . . ?
C68 C67 Lu4 84.78(15) . . ?
Lu8 C67 Lu4 10.90(16) . . ?
Lu5 C67 Lu4 32.94(17) . . ?
C66 C67 Lu12 68.1(3) . . ?
C45 C67 Lu12 106.2(6) . . ?
C68 C67 Lu12 74.07(19) . . ?
Lu8 C67 Lu12 1.1(7) . . ?
Lu5 C67 Lu12 24.6(3) . . ?
Lu4 C67 Lu12 10.76(13) . . ?
C48 C68 C67 119.7 . . ?
C48 C68 C69 129.2 . . ?
C67 C68 C69 97.8 . . ?
C48 C68 Lu8 101.5(3) . . ?
C67 C68 Lu8 67.9(3) . . ?
C69 C68 Lu8 60.4(4) . . ?
C48 C68 Lu5 71.4(2) . . ?
C67 C68 Lu5 88.55(17) . . ?
C69 C68 Lu5 77.24(18) . . ?
Lu8 C68 Lu5 30.6(3) . . ?
C48 C68 Lu12 96.0(4) . . ?
C67 C68 Lu12 77.4(3) . . ?
C69 C68 Lu12 58.1(6) . . ?
Lu8 C68 Lu12 9.5(4) . . ?
Lu5 C68 Lu12 24.7(4) . . ?
C48 C68 Lu4 101.90(11) . . ?
C67 C68 Lu4 66.91(12) . . ?
C69 C68 Lu4 60.86(11) . . ?
Lu8 C68 Lu4 1.0(3) . . ?
Lu5 C68 Lu4 31.27(18) . . ?
Lu12 C68 Lu4 10.5(3) . . ?
C48 C68 Lu13 79.3(3) . . ?
C67 C68 Lu13 98.8(3) . . ?
C69 C68 Lu13 61.1(3) . . ?
Lu8 C68 Lu13 31.9(3) . . ?
Lu5 C68 Lu13 18.2(2) . . ?
Lu12 C68 Lu13 22.5(4) . . ?
Lu4 C68 Lu13 32.8(3) . . ?
C68 C69 C70 126.0 . . ?
C68 C69 C80 117.5 . . ?
C70 C69 C80 111.6 . . ?
C68 C69 Lu8 79.8(5) . . ?
C70 C69 Lu8 98.9(5) . . ?
C80 C69 Lu8 68.6(3) . . ?
C68 C69 Lu12 91.9(7) . . ?
C70 C69 Lu12 83.2(6) . . ?
C80 C69 Lu12 71.4(3) . . ?
Lu8 C69 Lu12 16.1(9) . . ?
C68 C69 Lu5 68.61(15) . . ?
C70 C69 Lu5 84.74(15) . . ?
C80 C69 Lu5 97.12(17) . . ?
Lu8 C69 Lu5 28.8(2) . . ?
Lu12 C69 Lu5 28.5(5) . . ?
C68 C69 Lu4 90.40(13) . . ?
C70 C69 Lu4 93.60(13) . . ?
C80 C69 Lu4 61.92(13) . . ?
Lu8 C69 Lu4 10.7(4) . . ?
Lu12 C69 Lu4 11.9(3) . . ?
Lu5 C69 Lu4 35.51(16) . . ?
C68 C69 Lu13 90.5(3) . . ?
C70 C69 Lu13 63.5(3) . . ?
C80 C69 Lu13 95.0(3) . . ?
Lu8 C69 Lu13 38.0(4) . . ?
Lu12 C69 Lu13 26.0(4) . . ?
Lu5 C69 Lu13 23.6(3) . . ?
Lu4 C69 Lu13 37.7(3) . . ?
C72 C70 C71 114.2 . . ?
C72 C70 C69 119.4 . . ?
C71 C70 C69 111.7 . . ?
C72 C70 Lu13 78.4(4) . . ?
C71 C70 Lu13 69.9(4) . . ?
C69 C70 Lu13 82.5(4) . . ?
C72 C70 Lu8 89.7(3) . . ?
C71 C70 Lu8 97.1(2) . . ?
C69 C70 Lu8 47.1(3) . . ?
Lu13 C70 Lu8 37.6(5) . . ?
C72 C70 Lu12 76.4(6) . . ?
C71 C70 Lu12 93.3(4) . . ?
C69 C70 Lu12 63.5(6) . . ?
Lu13 C70 Lu12 25.4(5) . . ?
Lu8 C70 Lu12 16.7(7) . . ?
C72 C70 Lu5 97.34(13) . . ?
C71 C70 Lu5 71.32(16) . . ?
C69 C70 Lu5 63.07(13) . . ?
Lu13 C70 Lu5 22.0(4) . . ?
Lu8 C70 Lu5 25.9(2) . . ?
Lu12 C70 Lu5 25.5(5) . . ?
C70 C71 C52 118.3 . . ?
C70 C71 C49 121.9 . . ?
C52 C71 C49 112.8 . . ?
C70 C71 Lu13 73.7(4) . . ?
C52 C71 Lu13 82.7(4) . . ?
C49 C71 Lu13 87.6(4) . . ?
C70 C71 Lu5 77.52(17) . . ?
C52 C71 Lu5 100.51(12) . . ?
C49 C71 Lu5 67.48(16) . . ?
Lu13 C71 Lu5 22.9(4) . . ?
C70 C71 Lu3 99.83(13) . . ?
C52 C71 Lu3 64.63(13) . . ?
C49 C71 Lu3 78.19(14) . . ?
Lu13 C71 Lu3 26.8(4) . . ?
Lu5 C71 Lu3 36.40(14) . . ?
C54 C72 C70 129.1 . . ?
C54 C72 C73 96.4 . . ?
C70 C72 C73 124.7 . . ?
C54 C72 Lu7 65.0(3) . . ?
C70 C72 Lu7 104.3(3) . . ?
C73 C72 Lu7 64.1(2) . . ?
C54 C72 Lu13 83.6(4) . . ?
C70 C72 Lu13 67.0(3) . . ?
C73 C72 Lu13 93.3(3) . . ?
Lu7 C72 Lu13 38.4(4) . . ?
C54 C72 Lu12 98.0(5) . . ?
C70 C72 Lu12 72.3(5) . . ?
C73 C72 Lu12 71.6(3) . . ?
Lu7 C72 Lu12 36.0(6) . . ?
Lu13 C72 Lu12 24.9(4) . . ?
C54 C72 Lu8 112.2(3) . . ?
C70 C72 Lu8 61.1(2) . . ?
C73 C72 Lu8 74.67(15) . . ?
Lu7 C72 Lu8 50.5(4) . . ?
Lu13 C72 Lu8 32.9(4) . . ?
Lu12 C72 Lu8 14.6(6) . . ?
C79 C73 C72 116.9 . . ?
C79 C73 C74 121.9 . . ?
C72 C73 C74 113.0 . . ?
C79 C73 Lu7 96.0(3) . . ?
C72 C73 Lu7 77.71(16) . . ?
C74 C73 Lu7 67.6(4) . . ?
C79 C73 Lu12 65.0(4) . . ?
C72 C73 Lu12 76.47(15) . . ?
C74 C73 Lu12 101.6(5) . . ?
Lu7 C73 Lu12 37.2(7) . . ?
C79 C73 Lu4 55.38(11) . . ?
C72 C73 Lu4 86.98(15) . . ?
C74 C73 Lu4 101.37(11) . . ?
Lu7 C73 Lu4 42.8(4) . . ?
Lu12 C73 Lu4 11.25(19) . . ?
C79 C73 Lu8 54.4(2) . . ?
C72 C73 Lu8 76.46(12) . . ?
C74 C73 Lu8 115.2(3) . . ?
Lu7 C73 Lu8 51.7(5) . . ?
Lu12 C73 Lu8 14.5(6) . . ?
Lu4 C73 Lu8 15.04(19) . . ?
C79 C73 Lu13 85.9(3) . . ?
C72 C73 Lu13 57.1(2) . . ?
C74 C73 Lu13 98.1(3) . . ?
Lu7 C73 Lu13 31.3(4) . . ?
Lu12 C73 Lu13 22.5(4) . . ?
Lu4 C73 Lu13 33.7(3) . . ?
Lu8 C73 Lu13 31.6(3) . . ?
C75 C74 C55 117.0 . . ?
C75 C74 C73 128.2 . . ?
C55 C74 C73 106.5 . . ?
C75 C74 Lu7 97.6(3) . . ?
C55 C74 Lu7 73.5(3) . . ?
C73 C74 Lu7 68.5(4) . . ?
C58 C75 C74 118.1 . . ?
C58 C75 C76 115.9 . . ?
C74 C75 C76 110.3 . . ?
C58 C75 Lu7 91.7(3) . . ?
C74 C75 Lu7 51.0(3) . . ?
C76 C75 Lu7 87.8(3) . . ?
C60 C76 C77 130.5 . . ?
C60 C76 C75 101.7 . . ?
C77 C76 C75 115.6 . . ?
C76 C77 C78 109.6 . . ?
C76 C77 C79 133.0 . . ?
C78 C77 C79 113.3 . . ?
C76 C77 Lu4 109.05(12) . . ?
C78 C77 Lu4 78.26(14) . . ?
C79 C77 Lu4 63.65(15) . . ?
C76 C77 Lu12 107.5(5) . . ?
C78 C77 Lu12 87.0(6) . . ?
C79 C77 Lu12 57.9(5) . . ?
Lu4 C77 Lu12 8.9(6) . . ?
C76 C77 Lu8 121.5(3) . . ?
C78 C77 Lu8 77.8(3) . . ?
C79 C77 Lu8 53.7(3) . . ?
Lu4 C77 Lu8 12.9(3) . . ?
Lu12 C77 Lu8 14.9(6) . . ?
C76 C77 Lu7 82.0(2) . . ?
C78 C77 Lu7 113.5(3) . . ?
C79 C77 Lu7 64.3(2) . . ?
Lu4 C77 Lu7 38.8(3) . . ?
Lu12 C77 Lu7 31.6(6) . . ?
Lu8 C77 Lu7 46.0(4) . . ?
C65 C78 C62 109.3 . . ?
C65 C78 C77 120.3 . . ?
C62 C78 C77 120.6 . . ?
C65 C78 Lu4 71.30(12) . . ?
C62 C78 Lu4 102.01(13) . . ?
C77 C78 Lu4 68.37(13) . . ?
C80 C79 C73 116.2 . . ?
C80 C79 C77 125.9 . . ?
C73 C79 C77 110.8 . . ?
C80 C79 Lu4 71.99(15) . . ?
C73 C79 Lu4 93.33(15) . . ?
C77 C79 Lu4 80.25(18) . . ?
C80 C79 Lu8 54.2(4) . . ?
C73 C79 Lu8 96.6(3) . . ?
C77 C79 Lu8 96.2(2) . . ?
Lu4 C79 Lu8 18.6(3) . . ?
C80 C79 Lu12 71.2(6) . . ?
C73 C79 Lu12 82.5(6) . . ?
C77 C79 Lu12 90.5(3) . . ?
Lu4 C79 Lu12 12.8(4) . . ?
Lu8 C79 Lu12 18.2(8) . . ?
C80 C79 Lu7 102.7(2) . . ?
C73 C79 Lu7 52.1(3) . . ?
C77 C79 Lu7 85.74(17) . . ?
Lu4 C79 Lu7 43.3(3) . . ?
Lu8 C79 Lu7 53.9(5) . . ?
Lu12 C79 Lu7 35.9(7) . . ?
C79 C80 C66 119.4 . . ?
C79 C80 C69 128.0 . . ?
C66 C80 C69 95.1 . . ?
C79 C80 Lu8 89.3(4) . . ?
C66 C80 Lu8 69.4(5) . . ?
C69 C80 Lu8 66.5(2) . . ?
C79 C80 Lu4 71.43(15) . . ?
C66 C80 Lu4 74.84(15) . . ?
C69 C80 Lu4 83.20(17) . . ?
Lu8 C80 Lu4 18.9(3) . . ?
C79 C80 Lu12 74.1(6) . . ?
C66 C80 Lu12 83.7(7) . . ?
C69 C80 Lu12 72.5(2) . . ?
Lu8 C80 Lu12 16.9(9) . . ?
Lu4 C80 Lu12 13.1(3) . . ?
C95 N3 C95 104.4(6) 6_565 . ?
C95 N3 Ni1 127.8(3) 6_565 . ?
C95 N3 Ni1 127.8(3) . . ?
C93 N2 C86 104.3(4) . . ?
C93 N2 Ni1 128.3(3) . . ?
C86 N2 Ni1 127.4(3) . . ?
C84 N1 C84 104.1(6) . 6_565 ?
C84 N1 Ni1 127.9(3) . . ?
C84 N1 Ni1 127.9(3) 6_565 . ?
N3 Ni1 N1 177.9(2) . . ?
N3 Ni1 N2 89.74(12) . 6_565 ?
N1 Ni1 N2 90.22(12) . 6_565 ?
N3 Ni1 N2 89.74(12) . . ?
N1 Ni1 N2 90.22(12) . . ?
N2 Ni1 N2 177.8(2) 6_565 . ?
C83 C82 C81 112.6(5) . . ?
C83 C83 C84 106.6(3) 6_565 . ?
C83 C83 C82 128.9(3) 6_565 . ?
C84 C83 C82 124.4(5) . . ?
C85 C84 N1 125.0(5) . . ?
C85 C84 C83 123.6(5) . . ?
N1 C84 C83 111.4(5) . . ?
C84 C85 C86 124.3(5) . . ?
N2 C86 C85 125.0(5) . . ?
N2 C86 C87 111.1(4) . . ?
C85 C86 C87 123.9(5) . . ?
C90 C87 C86 106.5(5) . . ?
C90 C87 C88 128.9(5) . . ?
C86 C87 C88 124.5(5) . . ?
C87 C88 C89 113.1(6) . . ?
C87 C90 C93 106.4(5) . . ?
C87 C90 C91 129.2(5) . . ?
C93 C90 C91 124.3(5) . . ?
C90 C91 C92 113.5(5) . . ?
N2 C93 C94 124.4(5) . . ?
N2 C93 C90 111.6(4) . . ?
C94 C93 C90 123.9(5) . . ?
C95 C94 C93 124.5(5) . . ?
C94 C95 N3 125.2(4) . . ?
C94 C95 C96 123.8(5) . . ?
N3 C95 C96 111.0(5) . . ?
C96 C96 C95 106.8(3) 6_565 . ?
C96 C96 C97 128.5(3) 6_565 . ?
C95 C96 C97 124.5(5) . . ?
C96 C97 C98 112.1(5) . . ?
C110 C105 C106 122.7(12) . . ?
C105 C106 C107 116.8(9) . . ?
C108 C107 C106 124.7(10) . . ?
C107 C108 C109 115.6(11) . . ?
C110 C109 C108 121.1(12) . . ?
C105 C110 C109 119.1(13) . . ?
C100 C99 C104 120.0 . . ?
C101 C100 C99 120.0 . . ?
C102 C101 C100 120.0 . . ?
C101 C102 C103 120.0 . . ?
C104 C103 C102 120.0 . . ?
C103 C104 C99 120.0 . . ?

_refine_diff_density_max         1.698
_refine_diff_density_min         -2.056
_refine_diff_density_rms         0.162


_vrf_PLAT307_Lu2@C2v-C80         
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2@C2v-C80         
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu3N@D2-C88
_database_code_depnum_ccdc_archive 'CCDC 1836830'
_audit_update_record             
;
2018-07-19 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu3N@D2-C88 Ni(OEP)'
_chemical_name_common            'Lu3N@D2-C88 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         '2(Lu3 N C88), 3(C36 H44 N4 Ni), 2(C6 H6)'
_chemical_formula_sum            'C296 H144 Lu6 N14 Ni3'
_chemical_formula_weight         5122.19

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0027 0.0014 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0053 0.0028 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3436 0.9622 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.2922 5.1425 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   24.634(5)
_cell_length_b                   17.744(5)
_cell_length_c                   23.328(5)
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 103.220(5)
_cell_angle_gamma                90.000(5)
_cell_volume                     9927(4)
_cell_formula_units_Z            2
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9767
_cell_measurement_theta_min      2.265
_cell_measurement_theta_max      23.362

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.714
_exptl_crystal_F_000             5056
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.080
_exptl_crystal_size_mid          0.060
_exptl_crystal_size_min          0.040
_exptl_absorpt_coefficient_mu    2.679
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.5094
_exptl_absorpt_correction_T_max  0.7449
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline BL17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            41924
_diffrn_reflns_av_unetI/netI     0.0247
_diffrn_reflns_av_R_equivalents  0.0283
_diffrn_reflns_limit_h_min       -29
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_theta_min         2.602
_diffrn_reflns_theta_max         23.226
_diffrn_reflns_theta_full        23.048
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             9471
_reflns_number_gt                7593
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0455P)²+462.2852P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         9471
_refine_ls_number_parameters     908
_refine_ls_number_restraints     859
_refine_ls_R_factor_all          0.1766
_refine_ls_R_factor_gt           0.1516
_refine_ls_wR_factor_ref         0.3417
_refine_ls_wR_factor_gt          0.3278
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_restrained_S_all      1.135
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.7488(3) 0.5472(4) 0.3329(3) 0.1041(17) Uani 0.1611 1 d . U P A 1
N1 N 0.7875(4) 0.5000 0.2666(5) 0.0344(9) Uani 1 2 d S T P A 1
Lu2 Lu 0.74962(15) 0.3777(2) 0.2456(2) 0.0973(12) Uani 0.2322 1 d . U P A 1
Lu3 Lu 0.7110(3) 0.5000 0.2927(3) 0.122(2) Uani 0.2124 2 d S TU P A 1
Lu4 Lu 0.7696(3) 0.5000 0.3518(3) 0.150(2) Uani 0.2933 2 d S TU P A 1
Lu5 Lu 0.7776(3) 0.4013(3) 0.2025(3) 0.182(2) Uani 0.2621 1 d . U P A 1
Lu6 Lu 0.8093(5) 0.3821(5) 0.3062(5) 0.144(3) Uani 0.1421 1 d . U P A 1
Lu7 Lu 0.7225(4) 0.4291(7) 0.2835(5) 0.141(3) Uani 0.1218 1 d . U P A 1
Lu8 Lu 0.7900(5) 0.5695(8) 0.3452(5) 0.121(3) Uani 0.1009 1 d . U P A 1
Lu9 Lu 0.8407(6) 0.3960(8) 0.2777(7) 0.170(5) Uani 0.1155 1 d . U P A 1
Lu10 Lu 0.8134(8) 0.4556(10) 0.1856(8) 0.226(5) Uani 0.1113 1 d . U P A 1
C1 C 0.6631(2) 0.3624(4) 0.1714(3) 0.102(8) Uani 0.5 1 d G U P A -1
C2 C 0.63833(19) 0.3912(4) 0.2192(3) 0.098(7) Uani 0.5 1 d G U P A -1
C3 C 0.6559(2) 0.3409(4) 0.2699(3) 0.100(7) Uani 0.5 1 d G U P A -1
C4 C 0.6948(3) 0.2842(4) 0.2541(3) 0.117(8) Uani 0.5 1 d G U P A -1
C5 C 0.7028(3) 0.3013(3) 0.1943(3) 0.114(8) Uani 0.5 1 d G U P A -1
C6 C 0.7548(3) 0.2869(3) 0.1695(3) 0.116(8) Uani 0.5 1 d G U P A -1
C7 C 0.7685(3) 0.3349(4) 0.1214(2) 0.110(7) Uani 0.5 1 d G U P A -1
C8 C 0.7208(3) 0.3951(4) 0.10919(19) 0.097(7) Uani 0.5 1 d G U P A -1
C9 C 0.6772(2) 0.4220(4) 0.1332(2) 0.096(7) Uani 0.5 1 d G U P A -1
C10 C 0.66222(19) 0.5038(4) 0.1398(2) 0.072(5) Uani 0.5 1 d G U P A -1
C11 C 0.63933(14) 0.5213(4) 0.1823(3) 0.079(6) Uani 0.5 1 d G U P A -1
C12 C 0.62584(14) 0.4660(4) 0.2323(3) 0.086(6) Uani 0.5 1 d G U P A -1
C13 C 0.62329(16) 0.4885(5) 0.2869(3) 0.089(6) Uani 0.5 1 d G U P A -1
C14 C 0.6443(2) 0.4402(5) 0.3355(3) 0.097(7) Uani 0.5 1 d G U P A -1
C15 C 0.6604(2) 0.3757(5) 0.3318(3) 0.089(6) Uani 0.5 1 d G U P A -1
C16 C 0.7095(3) 0.3394(5) 0.3750(3) 0.088(6) Uani 0.5 1 d G U P A -1
C17 C 0.7458(3) 0.2795(4) 0.3589(3) 0.115(7) Uani 0.5 1 d G U P A -1
C18 C 0.7525(3) 0.2655(3) 0.2964(3) 0.111(7) Uani 0.5 1 d G U P A -1
C19 C 0.7999(4) 0.2428(3) 0.2695(4) 0.110(7) Uani 0.5 1 d G U P A -1
C20 C 0.8100(4) 0.2648(3) 0.2093(3) 0.116(8) Uani 0.5 1 d G U P A -1
C21 C 0.8564(3) 0.2979(4) 0.1848(3) 0.106(7) Uani 0.5 1 d G U P A -1
C22 C 0.8312(3) 0.3415(4) 0.1314(3) 0.102(7) Uani 0.5 1 d G U P A -1
C23 C 0.8633(3) 0.4039(4) 0.1221(3) 0.103(7) Uani 0.5 1 d G U P A -1
C24 C 0.8223(3) 0.4448(4) 0.09074(19) 0.101(7) Uani 0.5 1 d G U P A -1
C25 C 0.7580(3) 0.4417(4) 0.08352(15) 0.091(7) Uani 0.5 1 d G U P A -1
C26 C 0.7371(3) 0.5249(4) 0.08264(14) 0.075(6) Uani 0.5 1 d G U P A -1
C27 C 0.6929(2) 0.5414(4) 0.10764(18) 0.072(6) Uani 0.5 1 d G U P A -1
C28 C 0.6955(2) 0.6254(4) 0.1279(2) 0.065(5) Uani 0.5 1 d G U P A -1
C29 C 0.6707(2) 0.6441(4) 0.1770(3) 0.081(7) Uani 0.5 1 d G U P A -1
C30 C 0.64341(17) 0.5973(4) 0.2086(3) 0.096(7) Uani 0.5 1 d G U P A -1
C31 C 0.6410(2) 0.6152(4) 0.2670(3) 0.099(7) Uani 0.5 1 d G U P A -1
C32 C 0.6320(2) 0.5634(5) 0.3077(3) 0.103(7) Uani 0.5 1 d G U P A -1
C33 C 0.6605(3) 0.5607(5) 0.3670(3) 0.108(7) Uani 0.5 1 d G U P A -1
C34 C 0.6699(3) 0.4844(5) 0.3848(3) 0.105(7) Uani 0.5 1 d G U P A -1
C35 C 0.7075(3) 0.4614(5) 0.4158(2) 0.104(7) Uani 0.5 1 d G U P A -1
C36 C 0.7455(3) 0.3842(5) 0.4225(2) 0.096(6) Uani 0.5 1 d G U P A -1
C37 C 0.8046(3) 0.3622(5) 0.4261(2) 0.095(4) Uani 0.5 1 d G U P A -1
C38 C 0.8041(3) 0.3037(4) 0.3793(3) 0.095(4) Uani 0.5 1 d G U P A -1
C39 C 0.8572(3) 0.2962(4) 0.3604(3) 0.095(4) Uani 0.5 1 d G U P A -1
C40 C 0.8672(3) 0.2724(4) 0.3026(3) 0.095(4) Uani 0.5 1 d G U P A -1
C41 C 0.9136(3) 0.3173(4) 0.2901(3) 0.085(6) Uani 0.5 1 d G U P A -1
C42 C 0.9071(3) 0.3237(4) 0.2201(3) 0.099(7) Uani 0.5 1 d G U P A -1
C43 C 0.9323(2) 0.3936(5) 0.2148(3) 0.101(7) Uani 0.5 1 d G U P A -1
C44 C 0.9115(3) 0.4320(5) 0.1595(3) 0.094(6) Uani 0.5 1 d G U P A -1
C45 C 0.9221(2) 0.5120(5) 0.1691(3) 0.104(6) Uani 0.5 1 d G U P A -1
C46 C 0.8840(3) 0.5519(4) 0.1321(3) 0.094(6) Uani 0.5 1 d G U P A -1
C47 C 0.8417(3) 0.5280(4) 0.0960(2) 0.086(6) Uani 0.5 1 d G U P A -1
C48 C 0.7879(3) 0.5779(4) 0.08500(19) 0.074(6) Uani 0.5 1 d G U P A -1
C49 C 0.7935(3) 0.6502(4) 0.1108(3) 0.080(6) Uani 0.5 1 d G U P A -1
C50 C 0.7418(3) 0.6762(4) 0.1284(3) 0.063(5) Uani 0.5 1 d G U P A -1
C51 C 0.7428(3) 0.7264(3) 0.1785(3) 0.090(7) Uani 0.5 1 d G U P A -1
C52 C 0.6971(3) 0.7098(3) 0.2057(3) 0.094(7) Uani 0.5 1 d G U P A -1
C53 C 0.7027(3) 0.7184(4) 0.2656(3) 0.126(8) Uani 0.5 1 d G U P A -1
C54 C 0.6711(3) 0.6767(4) 0.2939(3) 0.120(8) Uani 0.5 1 d G U P A -1
C55 C 0.6967(3) 0.6740(4) 0.3519(3) 0.122(7) Uani 0.5 1 d G U P A -1
C56 C 0.7009(3) 0.6134(5) 0.3880(3) 0.115(7) Uani 0.5 1 d G U P A -1
C57 C 0.7428(3) 0.5665(5) 0.4331(2) 0.105(7) Uani 0.5 1 d G U P A -1
C58 C 0.7653(3) 0.4936(6) 0.44884(17) 0.121(6) Uani 0.5 1 d G U P A -1
C59 C 0.8227(3) 0.4951(6) 0.44776(14) 0.130(7) Uani 0.5 1 d G U P A -1
C60 C 0.8412(3) 0.4178(5) 0.43763(17) 0.122(7) Uani 0.5 1 d G U P A -1
C61 C 0.8839(2) 0.4294(5) 0.40563(19) 0.141(8) Uani 0.5 1 d G U P A -1
C62 C 0.8948(2) 0.3612(5) 0.3792(3) 0.109(7) Uani 0.5 1 d G U P A -1
C63 C 0.9294(2) 0.3741(5) 0.3360(3) 0.097(7) Uani 0.5 1 d G U P A -1
C64 C 0.95172(15) 0.4458(5) 0.3212(3) 0.120(7) Uani 0.5 1 d G U P A -1
C65 C 0.95338(16) 0.4499(5) 0.2596(3) 0.109(7) Uani 0.5 1 d G U P A -1
C66 C 0.95124(17) 0.5225(5) 0.2296(3) 0.110(7) Uani 0.5 1 d G U P A -1
C67 C 0.95098(16) 0.5882(5) 0.2686(3) 0.117(7) Uani 0.5 1 d G U P A -1
C68 C 0.9213(2) 0.6415(4) 0.2256(3) 0.112(7) Uani 0.5 1 d G U P A -1
C69 C 0.8933(3) 0.6290(4) 0.1640(3) 0.098(6) Uani 0.5 1 d G U P A -1
C70 C 0.8456(3) 0.6795(4) 0.1491(3) 0.098(7) Uani 0.5 1 d G U P A -1
C71 C 0.8447(3) 0.7254(3) 0.2011(3) 0.107(7) Uani 0.5 1 d G U P A -1
C72 C 0.7935(3) 0.7488(3) 0.2191(4) 0.114(7) Uani 0.5 1 d G U P A -1
C73 C 0.7912(3) 0.7473(3) 0.2815(4) 0.127(8) Uani 0.5 1 d G U P A -1
C74 C 0.7447(3) 0.7460(4) 0.3084(4) 0.129(8) Uani 0.5 1 d G U P A -1
C75 C 0.7486(3) 0.6967(4) 0.3550(3) 0.132(7) Uani 0.5 1 d G U P A -1
C76 C 0.7953(4) 0.6886(5) 0.4024(3) 0.131(6) Uani 0.5 1 d G U P A -1
C77 C 0.7863(3) 0.6129(5) 0.4224(2) 0.131(6) Uani 0.5 1 d G U P A -1
C78 C 0.8357(3) 0.5688(5) 0.43140(17) 0.140(6) Uani 0.5 1 d DG U P A -1
C79 C 0.8845(3) 0.5643(5) 0.4188(2) 0.142(6) Uani 0.5 1 d G U P A -1
C80 C 0.9100(2) 0.5030(5) 0.3988(2) 0.134(6) Uani 0.5 1 d G U P A -1
C81 C 0.93613(15) 0.5117(5) 0.3524(3) 0.136(7) Uani 0.5 1 d G U P A -1
C82 C 0.93674(17) 0.5818(5) 0.3259(3) 0.142(8) Uani 0.5 1 d G U P A -1
C83 C 0.9112(2) 0.6432(5) 0.3459(3) 0.148(9) Uani 0.5 1 d G U P A -1
C84 C 0.8919(3) 0.7060(4) 0.3088(3) 0.136(8) Uani 0.5 1 d G U P A -1
C85 C 0.8917(3) 0.7019(4) 0.2477(4) 0.127(8) Uani 0.5 1 d G U P A -1
C86 C 0.8425(3) 0.7299(4) 0.3262(3) 0.128(8) Uani 0.5 1 d G U P A -1
C87 C 0.8455(3) 0.6947(5) 0.3815(3) 0.131(8) Uani 0.5 1 d G U P A -1
C88 C 0.8851(3) 0.6344(5) 0.3924(3) 0.131(8) Uani 0.5 1 d DG U P A -1
Ni1A Ni 0.54414(5) 0.5000 0.07083(6) 0.0187(3) Uani 1 2 d S T P B 2
C1A C 0.7126(4) 0.3797(6) -0.0688(5) 0.043(2) Uani 1 1 d . . . B 2
H1AA H 0.7266 0.3447 -0.0933 0.064 Uiso 1 1 calc R U . B 2
H1AB H 0.7091 0.3549 -0.0332 0.064 Uiso 1 1 calc R U . B 2
H1AC H 0.7381 0.4213 -0.0592 0.064 Uiso 1 1 calc R U . B 2
N2A N 0.5455(3) 0.3898(4) 0.0718(3) 0.0344(9) Uani 1 1 d . . . B 2
C2A C 0.6554(3) 0.4090(5) -0.1017(4) 0.0285(18) Uani 1 1 d . . . B 2
H2AA H 0.6594 0.4349 -0.1371 0.034 Uiso 1 1 calc R U . B 2
H2AB H 0.6306 0.3665 -0.1136 0.034 Uiso 1 1 calc R U . B 2
Ni2A Ni 1.0000 0.5000 0.5000 0.0313(5) Uani 1 4 d S T P C 2
N3A N 0.5065(4) 0.5000 0.1367(5) 0.0344(9) Uani 1 2 d S T P B 2
C3A C 0.6296(3) 0.4618(4) -0.0650(3) 0.0223(16) Uani 1 1 d . . . B 2
C4A C 0.6007(3) 0.4390(4) -0.0210(3) 0.0199(15) Uani 1 1 d . . . B 2
N4A N 1.0352(3) 0.4217(4) 0.4619(3) 0.0344(9) Uani 1 1 d . . . C 2
C5A C 0.5922(3) 0.3649(5) -0.0074(4) 0.0240(16) Uani 1 1 d . . . B 2
H5A H 0.6044 0.3277 -0.0296 0.029 Uiso 1 1 calc R U . B 2
C6A C 0.5674(3) 0.3423(4) 0.0362(4) 0.0222(16) Uani 1 1 d . . . B 2
C7A C 0.5609(3) 0.2638(4) 0.0513(4) 0.0281(18) Uani 1 1 d . . . B 2
C8A C 0.5807(4) 0.1984(5) 0.0206(5) 0.035(2) Uani 1 1 d . . . B 2
H8AA H 0.5733 0.2086 -0.0213 0.042 Uiso 1 1 calc R U . B 2
H8AB H 0.5601 0.1536 0.0263 0.042 Uiso 1 1 calc R U . B 2
C9A C 0.6435(4) 0.1838(6) 0.0439(5) 0.054(3) Uani 1 1 d . . . B 2
H9AA H 0.6549 0.1428 0.0225 0.081 Uiso 1 1 calc R U . B 2
H9AB H 0.6507 0.1712 0.0850 0.081 Uiso 1 1 calc R U . B 2
H9AC H 0.6640 0.2283 0.0388 0.081 Uiso 1 1 calc R U . B 2
C10A C 0.5353(3) 0.2644(5) 0.0963(4) 0.0308(19) Uani 1 1 d . . . B 2
C11A C 0.5191(4) 0.1985(5) 0.1297(5) 0.039(2) Uani 1 1 d . . . B 2
H11A H 0.5164 0.1536 0.1054 0.047 Uiso 1 1 calc R U . B 2
H11B H 0.4826 0.2079 0.1373 0.047 Uiso 1 1 calc R U . B 2
C12A C 0.5607(5) 0.1841(7) 0.1883(5) 0.061(3) Uani 1 1 d . . . B 2
H12A H 0.5970 0.1747 0.1811 0.092 Uiso 1 1 calc R U . B 2
H12B H 0.5490 0.1410 0.2072 0.092 Uiso 1 1 calc R U . B 2
H12C H 0.5623 0.2274 0.2132 0.092 Uiso 1 1 calc R U . B 2
C13A C 0.5253(3) 0.3422(4) 0.1088(3) 0.0221(16) Uani 1 1 d . . . B 2
C14A C 0.4990(3) 0.3650(5) 0.1516(4) 0.0274(18) Uani 1 1 d . . . B 2
H14A H 0.4864 0.3278 0.1734 0.033 Uiso 1 1 calc R U . B 2
C15A C 0.4899(3) 0.4386(5) 0.1645(3) 0.0238(16) Uani 1 1 d . . . B 2
C16A C 0.4632(3) 0.4624(5) 0.2106(4) 0.0304(18) Uani 1 1 d . . . B 2
C17A C 0.4425(4) 0.4089(6) 0.2511(4) 0.038(2) Uani 1 1 d . . . B 2
H17A H 0.4225 0.3680 0.2278 0.045 Uiso 1 1 calc R U . B 2
H17B H 0.4162 0.4354 0.2691 0.045 Uiso 1 1 calc R U . B 2
C18A C 0.4883(5) 0.3756(7) 0.2994(4) 0.054(3) Uani 1 1 d . . . B 2
H18A H 0.5148 0.3498 0.2820 0.082 Uiso 1 1 calc R U . B 2
H18B H 0.4722 0.3407 0.3223 0.082 Uiso 1 1 calc R U . B 2
H18C H 0.5067 0.4153 0.3244 0.082 Uiso 1 1 calc R U . B 2
C19A C 1.0000 0.3080(7) 0.5000 0.039(3) Uani 1 2 d S T P C 2
H19A H 1.0000 0.2555 0.5000 0.047 Uiso 1 2 calc R U P C 2
C20A C 1.0314(4) 0.3442(5) 0.4669(4) 0.037(2) Uani 1 1 d . . . C 2
C21A C 1.0647(4) 0.3060(5) 0.4327(4) 0.041(2) Uani 1 1 d . . . C 2
C22A C 1.0728(5) 0.2223(6) 0.4306(5) 0.053(3) Uani 1 1 d . . . C 2
H22A H 1.0817 0.2091 0.3934 0.063 Uiso 1 1 calc R U . C 2
H22B H 1.0382 0.1972 0.4323 0.063 Uiso 1 1 calc R U . C 2
C23A C 1.1189(6) 0.1940(7) 0.4807(6) 0.073(4) Uani 1 1 d . . . C 2
H23A H 1.1245 0.1411 0.4757 0.109 Uiso 1 1 calc R U . C 2
H23B H 1.1085 0.2023 0.5174 0.109 Uiso 1 1 calc R U . C 2
H23C H 1.1527 0.2207 0.4806 0.109 Uiso 1 1 calc R U . C 2
C24A C 1.0886(5) 0.3599(6) 0.4058(5) 0.048(3) Uani 1 1 d . . . C 2
C25A C 1.1297(6) 0.3520(7) 0.3672(5) 0.064(3) Uani 1 1 d . . . C 2
H25A H 1.1277 0.3010 0.3519 0.077 Uiso 1 1 calc R U . C 2
H25B H 1.1191 0.3861 0.3341 0.077 Uiso 1 1 calc R U . C 2
C26A C 1.1879(6) 0.3682(8) 0.3983(7) 0.076(4) Uani 1 1 d . . . C 2
H26A H 1.2118 0.3637 0.3713 0.114 Uiso 1 1 calc R U . C 2
H26B H 1.1994 0.3329 0.4300 0.114 Uiso 1 1 calc R U . C 2
H26C H 1.1902 0.4185 0.4139 0.114 Uiso 1 1 calc R U . C 2
C27A C 1.0701(4) 0.4312(5) 0.4239(4) 0.042(2) Uani 1 1 d . . . C 2
C28A C 1.0860(7) 0.5000 0.4056(6) 0.044(3) Uani 1 2 d S T P C 2
H28A H 1.1089 0.5000 0.3790 0.053 Uiso 1 2 calc R U P C 2
N1A N 0.5833(4) 0.5000 0.0057(5) 0.0344(9) Uani 1 2 d S T P B 2
C1D C 0.732(3) 0.0000 0.182(3) 0.31(5) Uani 1 2 d S T P D 3
H1D H 0.7409 0.0000 0.1451 0.376 Uiso 1 2 calc R U P D 3
C4D C 0.6745(17) 0.0000 0.2555(19) 0.163(18) Uani 1 2 d S T P D 3
H4D H 0.6492 0.0000 0.2796 0.195 Uiso 1 2 calc R U P D 3
C2D C 0.7261(14) 0.0606(12) 0.2046(14) 0.193(16) Uani 1 1 d . . . D 3
H2D H 0.7456 0.1031 0.1975 0.232 Uiso 1 1 calc R U . D 3
C3D C 0.6922(9) 0.0633(10) 0.2387(8) 0.110(7) Uani 1 1 d . . . D 3
H3D H 0.6806 0.1092 0.2511 0.132 Uiso 1 1 calc R U . D 3


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu4 1.028(7) . ?
Lu1 Lu8 1.066(12) . ?
Lu1 Lu7 1.259(12) 6_565 ?
Lu1 Lu3 1.431(9) . ?
Lu1 Lu1 1.676(15) 6_565 ?
Lu1 Lu6 2.147(14) 6_565 ?
Lu1 N1 2.162(11) . ?
Lu1 C56 2.262(6) . ?
Lu1 Lu8 2.296(14) 6_565 ?
Lu1 C77 2.385(9) . ?
Lu1 C57 2.401(7) . ?
Lu1 Lu7 2.409(13) . ?
N1 Lu3 2.109(12) . ?
N1 Lu4 2.132(13) . ?
N1 Lu7 2.142(13) 6_565 ?
N1 Lu7 2.142(13) . ?
N1 Lu1 2.162(11) 6_565 ?
N1 Lu8 2.198(14) 6_565 ?
N1 Lu8 2.198(14) . ?
N1 Lu9 2.244(14) 6_565 ?
N1 Lu9 2.244(13) . ?
N1 Lu10 2.27(2) 6_565 ?
N1 Lu10 2.27(2) . ?
Lu2 Lu5 1.408(8) . ?
Lu2 Lu7 1.525(13) . ?
Lu2 Lu6 1.792(9) . ?
Lu2 C5 1.992(6) . ?
Lu2 C4 2.176(6) . ?
Lu2 Lu9 2.222(15) . ?
Lu2 C18 2.308(6) . ?
Lu2 C6 2.423(7) . ?
Lu2 C1 2.435(6) . ?
Lu2 Lu1 2.437(8) 6_565 ?
Lu2 Lu8 2.490(14) 6_565 ?
Lu3 Lu7 1.319(13) 6_565 ?
Lu3 Lu7 1.319(13) . ?
Lu3 Lu1 1.431(9) 6_565 ?
Lu3 Lu4 1.754(11) . ?
Lu3 C13 2.142(7) . ?
Lu3 C12 2.323(8) . ?
Lu3 C32 2.341(7) . ?
Lu3 C14 2.360(7) . ?
Lu3 Lu8 2.391(14) . ?
Lu3 Lu8 2.392(14) 6_565 ?
Lu4 Lu1 1.028(7) 6_565 ?
Lu4 Lu8 1.354(14) 6_565 ?
Lu4 Lu8 1.354(14) . ?
Lu4 Lu7 2.151(12) . ?
Lu4 Lu7 2.151(12) 6_565 ?
Lu4 C58 2.293(7) . ?
Lu4 C59 2.321(9) . ?
Lu4 C57 2.449(7) . ?
Lu4 C35 2.466(8) . ?
Lu5 Lu10 1.42(2) . ?
Lu5 Lu9 2.064(14) . ?
Lu5 C7 2.197(7) . ?
Lu5 C6 2.198(7) . ?
Lu5 C8 2.305(7) . ?
Lu5 Lu6 2.390(12) . ?
Lu5 C5 2.533(9) . ?
Lu5 C20 2.545(8) . ?
Lu5 C22 2.574(8) . ?
Lu5 Lu7 2.613(14) . ?
Lu6 Lu9 1.157(16) . ?
Lu6 Lu8 1.410(15) 6_565 ?
Lu6 Lu1 2.146(14) 6_565 ?
Lu6 C39 2.154(9) . ?
Lu6 C38 2.228(11) . ?
Lu6 Lu7 2.243(15) . ?
Lu6 C62 2.416(10) . ?
Lu6 C40 2.427(12) . ?
Lu6 C18 2.479(11) . ?
Lu7 Lu1 1.259(12) 6_565 ?
Lu7 Lu8 1.935(16) 6_565 ?
Lu7 C3 2.236(10) . ?
Lu7 C15 2.301(11) . ?
Lu7 C2 2.361(10) . ?
Lu7 C12 2.495(11) . ?
Lu8 Lu6 1.410(15) 6_565 ?
Lu8 Lu7 1.935(16) 6_565 ?
Lu8 C77 1.979(11) . ?
Lu8 C78 2.068(13) . ?
Lu8 Lu1 2.296(14) 6_565 ?
Lu8 Lu9 2.306(19) 6_565 ?
Lu8 Lu8 2.47(3) 6_565 ?
Lu8 C76 2.486(13) . ?
Lu9 C41 2.241(13) . ?
Lu9 Lu8 2.306(19) 6_565 ?
Lu9 C40 2.324(14) . ?
Lu9 C63 2.327(13) . ?
Lu9 Lu10 2.35(2) . ?
Lu9 C62 2.514(15) . ?
Lu9 C39 2.584(16) . ?
Lu9 C42 2.670(16) . ?
Lu10 Lu10 1.58(3) 6_565 ?
Lu10 C24 2.28(2) . ?
Lu10 C23 2.32(2) . ?
Lu10 C25 2.471(18) . ?
Lu10 C22 2.479(17) . ?
Lu10 C44 2.66(2) . ?
Lu10 C47 2.68(2) . ?
Lu10 C7 2.702(17) . ?
C1 C9 1.4736 . ?
C1 C5 1.4770 . ?
C1 C2 1.4804 . ?
C2 C12 1.4116 . ?
C2 C3 1.4661 . ?
C3 C4 1.4915 . ?
C3 C15 1.5514 . ?
C4 C5 1.4843 . ?
C4 C18 1.5688 . ?
C5 C6 1.5419 . ?
C6 C7 1.5076 . ?
C6 C20 1.5123 . ?
C7 C22 1.5131 . ?
C7 C8 1.5668 . ?
C8 C9 1.4033 . ?
C8 C25 1.4606 . ?
C9 C10 1.5141 . ?
C10 C11 1.2853 . ?
C10 C27 1.3566 . ?
C11 C30 1.4751 . ?
C11 C12 1.6145 . ?
C12 C13 1.3496 . ?
C13 C32 1.4143 . ?
C13 C14 1.4221 . ?
C14 C15 1.2207 . ?
C14 C34 1.4149 . ?
C15 C16 1.5299 . ?
C16 C36 1.4823 . ?
C16 C17 1.4902 . ?
C17 C38 1.4687 . ?
C17 C18 1.5258 . ?
C18 C19 1.5008 . ?
C19 C20 1.5313 . ?
C19 C40 1.7426 . ?
C20 C21 1.5091 . ?
C21 C42 1.4077 . ?
C21 C22 1.4761 . ?
C22 C23 1.4074 . ?
C23 C24 1.3206 . ?
C23 C44 1.3935 . ?
C24 C47 1.5485 . ?
C24 C25 1.5541 . ?
C25 C26 1.5622 . ?
C26 C27 1.3782 . ?
C26 C48 1.5577 . ?
C27 C28 1.5603 . ?
C28 C50 1.4521 . ?
C28 C29 1.4556 . ?
C29 C30 1.3816 . ?
C29 C52 1.4251 . ?
C30 C31 1.4129 . ?
C31 C32 1.3750 . ?
C31 C54 1.3869 . ?
C32 C33 1.4021 . ?
C33 C56 1.3711 . ?
C33 C34 1.4208 . ?
C34 C35 1.1133 . ?
C35 C58 1.5635 . ?
C35 C36 1.6478 . ?
C36 C37 1.4902 . ?
C37 C60 1.3218 . ?
C37 C38 1.5048 . ?
C38 C39 1.4791 . ?
C39 C62 1.4822 . ?
C39 C40 1.4875 . ?
C40 C41 1.4765 . ?
C41 C63 1.4569 . ?
C41 C42 1.6078 . ?
C42 C43 1.4041 . ?
C43 C44 1.4461 . ?
C43 C65 1.4539 . ?
C44 C45 1.4521 . ?
C45 C46 1.3247 . ?
C45 C66 1.4415 . ?
C46 C47 1.2567 . ?
C46 C69 1.5477 . ?
C47 C48 1.5646 . ?
C48 C49 1.4097 . ?
C49 C70 1.4805 . ?
C49 C50 1.4961 . ?
C50 C51 1.4658 . ?
C51 C72 1.4402 . ?
C51 C52 1.4427 . ?
C52 C53 1.3811 . ?
C53 C54 1.3521 . ?
C53 C74 1.3547 . ?
C54 C55 1.3562 . ?
C55 C75 1.3265 . ?
C55 C56 1.3550 . ?
C56 C57 1.5400 . ?
C57 C77 1.4198 . ?
C57 C58 1.4200 . ?
C58 C59 1.4200 . ?
C59 C78 1.4200 . ?
C59 C60 1.4812 . ?
C60 C61 1.4368 . ?
C61 C62 1.4118 . ?
C61 C80 1.4808 . ?
C62 C63 1.4785 . ?
C63 C64 1.4584 . ?
C64 C65 1.4489 . ?
C64 C81 1.4745 . ?
C65 C66 1.4612 . ?
C66 C67 1.4793 . ?
C67 C68 1.4503 . ?
C67 C82 1.4616 . ?
C68 C85 1.4556 . ?
C68 C69 1.4619 . ?
C69 C70 1.4546 . ?
C70 C71 1.4655 . ?
C71 C85 1.4547 . ?
C71 C72 1.4772 . ?
C72 C73 1.4704 . ?
C73 C74 1.4267 . ?
C73 C86 1.4763 . ?
C74 C75 1.3812 . ?
C75 C76 1.4077 . ?
C76 C87 1.4350 . ?
C76 C77 1.4539 . ?
C77 C78 1.4201 . ?
C78 C79 1.3031 . ?
C79 C88 1.3900 . ?
C79 C80 1.3900 . ?
C80 C81 1.3900 . ?
C81 C82 1.3900 . ?
C82 C83 1.3900 . ?
C83 C88 1.3900 . ?
C83 C84 1.4250 . ?
C84 C85 1.4279 . ?
C84 C86 1.4308 . ?
C86 C87 1.4179 . ?
C87 C88 1.4306 . ?
Ni1A N2A 1.956(8) . ?
Ni1A N2A 1.956(8) 6_565 ?
Ni1A N3A 1.969(11) . ?
Ni1A N1A 1.977(12) . ?
C1A C2A 1.535(12) . ?
N2A C6A 1.378(11) . ?
N2A C13A 1.378(11) . ?
C2A C3A 1.505(11) . ?
Ni2A N4A 1.956(8) 6_565 ?
Ni2A N4A 1.956(8) 2_756 ?
Ni2A N4A 1.956(8) 5_766 ?
Ni2A N4A 1.956(8) . ?
N3A C15A 1.377(10) 6_565 ?
N3A C15A 1.377(10) . ?
C3A C3A 1.356(16) 6_565 ?
C3A C4A 1.435(10) . ?
C4A N1A 1.367(10) . ?
C4A C5A 1.379(11) . ?
N4A C27A 1.378(13) . ?
N4A C20A 1.385(12) . ?
C5A C6A 1.362(11) . ?
C6A C7A 1.455(11) . ?
C7A C10A 1.344(12) . ?
C7A C8A 1.502(12) . ?
C8A C9A 1.539(13) . ?
C10A C13A 1.443(11) . ?
C10A C11A 1.509(12) . ?
C11A C12A 1.531(15) . ?
C13A C14A 1.369(11) . ?
C14A C15A 1.372(12) . ?
C15A C16A 1.445(11) . ?
C16A C16A 1.334(18) 6_565 ?
C16A C17A 1.509(12) . ?
C17A C18A 1.521(14) . ?
C19A C20A 1.372(12) . ?
C19A C20A 1.372(11) 2_756 ?
C20A C21A 1.438(14) . ?
C21A C24A 1.352(15) . ?
C21A C22A 1.501(14) . ?
C22A C23A 1.516(17) . ?
C24A C27A 1.442(14) . ?
C24A C25A 1.505(16) . ?
C25A C26A 1.478(19) . ?
C27A C28A 1.379(12) . ?
C28A C27A 1.379(12) 6_565 ?
N1A C4A 1.367(10) 6_565 ?
C1D C2D 1.22(3) 6 ?
C1D C2D 1.22(3) . ?
C4D C3D 1.30(2) 6 ?
C4D C3D 1.30(2) . ?
C2D C3D 1.28(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu4 Lu1 Lu8 80.6(10) . . ?
Lu4 Lu1 Lu7 140.1(10) . 6_565 ?
Lu8 Lu1 Lu7 112.4(12) . 6_565 ?
Lu4 Lu1 Lu3 89.4(8) . . ?
Lu8 Lu1 Lu3 146.1(8) . . ?
Lu7 Lu1 Lu3 58.3(7) 6_565 . ?
Lu4 Lu1 Lu1 35.4(7) . 6_565 ?
Lu8 Lu1 Lu1 111.8(9) . 6_565 ?
Lu7 Lu1 Lu1 109.5(7) 6_565 6_565 ?
Lu3 Lu1 Lu1 54.2(3) . 6_565 ?
Lu4 Lu1 Lu6 106.8(7) . 6_565 ?
Lu8 Lu1 Lu6 34.8(8) . 6_565 ?
Lu7 Lu1 Lu6 77.6(7) 6_565 6_565 ?
Lu3 Lu1 Lu6 122.9(5) . 6_565 ?
Lu1 Lu1 Lu6 125.7(3) 6_565 6_565 ?
Lu4 Lu1 N1 74.5(5) . . ?
Lu8 Lu1 N1 77.7(7) . . ?
Lu7 Lu1 N1 72.1(6) 6_565 . ?
Lu3 Lu1 N1 68.4(4) . . ?
Lu1 Lu1 N1 67.2(2) 6_565 . ?
Lu6 Lu1 N1 64.5(3) 6_565 . ?
Lu4 Lu1 C56 116.9(7) . . ?
Lu8 Lu1 C56 104.1(8) . . ?
Lu7 Lu1 C56 97.0(6) 6_565 . ?
Lu3 Lu1 C56 109.3(5) . . ?
Lu1 Lu1 C56 121.3(3) 6_565 . ?
Lu6 Lu1 C56 110.4(5) 6_565 . ?
N1 Lu1 C56 168.5(5) . . ?
Lu4 Lu1 Lu8 17.8(5) . 6_565 ?
Lu8 Lu1 Lu8 86.2(11) . 6_565 ?
Lu7 Lu1 Lu8 122.4(7) 6_565 6_565 ?
Lu3 Lu1 Lu8 75.9(4) . 6_565 ?
Lu1 Lu1 Lu8 25.5(3) 6_565 6_565 ?
Lu6 Lu1 Lu8 104.3(4) 6_565 6_565 ?
N1 Lu1 Lu8 59.0(3) . 6_565 ?
C56 Lu1 Lu8 132.1(5) . 6_565 ?
Lu4 Lu1 C77 88.1(7) . . ?
Lu8 Lu1 C77 55.1(7) . . ?
Lu7 Lu1 C77 130.8(8) 6_565 . ?
Lu3 Lu1 C77 157.4(5) . . ?
Lu1 Lu1 C77 119.3(3) 6_565 . ?
Lu6 Lu1 C77 79.2(4) 6_565 . ?
N1 Lu1 C77 132.0(5) . . ?
C56 Lu1 C77 52.93(16) . . ?
Lu8 Lu1 C77 105.1(5) 6_565 . ?
Lu4 Lu1 C57 80.4(6) . . ?
Lu8 Lu1 C57 87.3(8) . . ?
Lu7 Lu1 C57 135.4(6) 6_565 . ?
Lu3 Lu1 C57 123.0(5) . . ?
Lu1 Lu1 C57 98.2(3) 6_565 . ?
Lu6 Lu1 C57 113.6(5) 6_565 . ?
N1 Lu1 C57 152.5(5) . . ?
C56 Lu1 C57 38.43(10) . . ?
Lu8 Lu1 C57 97.5(5) 6_565 . ?
C77 Lu1 C57 34.52(11) . . ?
Lu4 Lu1 Lu7 63.2(7) . . ?
Lu8 Lu1 Lu7 125.9(9) . . ?
Lu7 Lu1 Lu7 80.0(9) 6_565 . ?
Lu3 Lu1 Lu7 27.6(4) . . ?
Lu1 Lu1 Lu7 29.5(3) 6_565 . ?
Lu6 Lu1 Lu7 119.9(4) 6_565 . ?
N1 Lu1 Lu7 55.6(3) . . ?
C56 Lu1 Lu7 127.3(5) . . ?
Lu8 Lu1 Lu7 48.5(4) 6_565 . ?
C77 Lu1 Lu7 148.5(5) . . ?
C57 Lu1 Lu7 121.4(5) . . ?
Lu3 N1 Lu4 48.8(4) . . ?
Lu3 N1 Lu7 36.1(4) . 6_565 ?
Lu4 N1 Lu7 60.4(5) . 6_565 ?
Lu3 N1 Lu7 36.1(4) . . ?
Lu4 N1 Lu7 60.4(5) . . ?
Lu7 N1 Lu7 72.0(8) 6_565 . ?
Lu3 N1 Lu1 39.1(3) . 6_565 ?
Lu4 N1 Lu1 27.7(2) . 6_565 ?
Lu7 N1 Lu1 68.1(5) 6_565 6_565 ?
Lu7 N1 Lu1 34.0(4) . 6_565 ?
Lu3 N1 Lu1 39.1(3) . . ?
Lu4 N1 Lu1 27.7(2) . . ?
Lu7 N1 Lu1 34.0(4) 6_565 . ?
Lu7 N1 Lu1 68.1(5) . . ?
Lu1 N1 Lu1 45.6(5) 6_565 . ?
Lu3 N1 Lu8 67.4(5) . 6_565 ?
Lu4 N1 Lu8 36.4(4) . 6_565 ?
Lu7 N1 Lu8 93.3(6) 6_565 6_565 ?
Lu7 N1 Lu8 52.9(5) . 6_565 ?
Lu1 N1 Lu8 28.3(3) 6_565 6_565 ?
Lu1 N1 Lu8 63.5(5) . 6_565 ?
Lu3 N1 Lu8 67.4(5) . . ?
Lu4 N1 Lu8 36.4(4) . . ?
Lu7 N1 Lu8 52.9(5) 6_565 . ?
Lu7 N1 Lu8 93.3(6) . . ?
Lu1 N1 Lu8 63.5(5) 6_565 . ?
Lu1 N1 Lu8 28.3(3) . . ?
Lu8 N1 Lu8 68.3(8) 6_565 . ?
Lu3 N1 Lu9 120.3(5) . 6_565 ?
Lu4 N1 Lu9 97.7(6) . 6_565 ?
Lu7 N1 Lu9 86.5(6) 6_565 6_565 ?
Lu7 N1 Lu9 154.7(8) . 6_565 ?
Lu1 N1 Lu9 125.3(7) 6_565 6_565 ?
Lu1 N1 Lu9 86.6(6) . 6_565 ?
Lu8 N1 Lu9 117.5(7) 6_565 6_565 ?
Lu8 N1 Lu9 62.5(6) . 6_565 ?
Lu3 N1 Lu9 120.3(5) . . ?
Lu4 N1 Lu9 97.7(6) . . ?
Lu7 N1 Lu9 154.7(8) 6_565 . ?
Lu7 N1 Lu9 86.4(6) . . ?
Lu1 N1 Lu9 86.6(6) 6_565 . ?
Lu1 N1 Lu9 125.3(7) . . ?
Lu8 N1 Lu9 62.5(6) 6_565 . ?
Lu8 N1 Lu9 117.5(7) . . ?
Lu9 N1 Lu9 110.6(9) 6_565 . ?
Lu3 N1 Lu10 132.9(7) . 6_565 ?
Lu4 N1 Lu10 159.0(5) . 6_565 ?
Lu7 N1 Lu10 108.3(6) 6_565 6_565 ?
Lu7 N1 Lu10 136.1(7) . 6_565 ?
Lu1 N1 Lu10 169.7(7) 6_565 6_565 ?
Lu1 N1 Lu10 135.6(5) . 6_565 ?
Lu8 N1 Lu10 158.3(7) 6_565 6_565 ?
Lu8 N1 Lu10 122.7(6) . 6_565 ?
Lu9 N1 Lu10 62.7(7) 6_565 6_565 ?
Lu9 N1 Lu10 96.4(8) . 6_565 ?
Lu3 N1 Lu10 132.9(7) . . ?
Lu4 N1 Lu10 159.0(5) . . ?
Lu7 N1 Lu10 136.1(7) 6_565 . ?
Lu7 N1 Lu10 108.3(6) . . ?
Lu1 N1 Lu10 135.6(5) 6_565 . ?
Lu1 N1 Lu10 169.7(7) . . ?
Lu8 N1 Lu10 122.7(6) 6_565 . ?
Lu8 N1 Lu10 158.3(7) . . ?
Lu9 N1 Lu10 96.4(8) 6_565 . ?
Lu9 N1 Lu10 62.7(7) . . ?
Lu10 N1 Lu10 40.6(10) 6_565 . ?
Lu5 Lu2 Lu7 125.9(5) . . ?
Lu5 Lu2 Lu6 95.9(5) . . ?
Lu7 Lu2 Lu6 84.7(6) . . ?
Lu5 Lu2 C5 94.8(4) . . ?
Lu7 Lu2 C5 119.0(5) . . ?
Lu6 Lu2 C5 139.6(4) . . ?
Lu5 Lu2 C4 135.0(4) . . ?
Lu7 Lu2 C4 92.3(5) . . ?
Lu6 Lu2 C4 112.1(4) . . ?
C5 Lu2 C4 41.44(11) . . ?
Lu5 Lu2 Lu9 64.8(5) . . ?
Lu7 Lu2 Lu9 105.1(5) . . ?
Lu6 Lu2 Lu9 31.2(5) . . ?
C5 Lu2 Lu9 134.7(5) . . ?
C4 Lu2 Lu9 133.0(5) . . ?
Lu5 Lu2 C18 131.4(4) . . ?
Lu7 Lu2 C18 100.7(5) . . ?
Lu6 Lu2 C18 73.2(4) . . ?
C5 Lu2 C18 70.57(19) . . ?
C4 Lu2 C18 40.82(11) . . ?
Lu9 Lu2 C18 92.5(5) . . ?
Lu5 Lu2 N1 69.0(4) . . ?
Lu7 Lu2 N1 62.4(4) . . ?
Lu6 Lu2 N1 65.4(4) . . ?
C5 Lu2 N1 153.4(4) . . ?
C4 Lu2 N1 154.5(4) . . ?
Lu9 Lu2 N1 58.4(4) . . ?
C18 Lu2 N1 136.0(4) . . ?
Lu5 Lu2 C6 63.7(3) . . ?
Lu7 Lu2 C6 157.7(4) . . ?
Lu6 Lu2 C6 115.8(5) . . ?
C5 Lu2 C6 39.38(13) . . ?
C4 Lu2 C6 72.41(19) . . ?
Lu9 Lu2 C6 97.2(5) . . ?
C18 Lu2 C6 78.6(2) . . ?
N1 Lu2 C6 132.6(4) . . ?
Lu5 Lu2 C1 90.9(3) . . ?
Lu7 Lu2 C1 92.9(4) . . ?
Lu6 Lu2 C1 172.9(5) . . ?
C5 Lu2 C1 37.31(10) . . ?
C4 Lu2 C1 61.29(14) . . ?
Lu9 Lu2 C1 155.2(5) . . ?
C18 Lu2 C1 100.9(2) . . ?
N1 Lu2 C1 119.2(3) . . ?
C6 Lu2 C1 65.70(16) . . ?
Lu5 Lu2 Lu1 122.2(3) . 6_565 ?
Lu7 Lu2 Lu1 26.0(4) . 6_565 ?
Lu6 Lu2 Lu1 58.7(5) . 6_565 ?
C5 Lu2 Lu1 139.5(4) . 6_565 ?
C4 Lu2 Lu1 102.5(3) . 6_565 ?
Lu9 Lu2 Lu1 80.8(5) . 6_565 ?
C18 Lu2 Lu1 92.8(3) . 6_565 ?
N1 Lu2 Lu1 53.5(3) . 6_565 ?
C6 Lu2 Lu1 171.1(3) . 6_565 ?
C1 Lu2 Lu1 118.8(3) . 6_565 ?
Lu5 Lu2 Lu8 113.5(4) . 6_565 ?
Lu7 Lu2 Lu8 51.0(5) . 6_565 ?
Lu6 Lu2 Lu8 33.7(5) . 6_565 ?
C5 Lu2 Lu8 150.4(4) . 6_565 ?
C4 Lu2 Lu8 109.0(4) . 6_565 ?
Lu9 Lu2 Lu8 58.3(5) . 6_565 ?
C18 Lu2 Lu8 83.5(4) . 6_565 ?
N1 Lu2 Lu8 53.7(4) . 6_565 ?
C6 Lu2 Lu8 149.0(4) . 6_565 ?
C1 Lu2 Lu8 143.5(4) . 6_565 ?
Lu1 Lu2 Lu8 25.0(3) 6_565 6_565 ?
Lu7 Lu3 Lu7 145.2(11) 6_565 . ?
Lu7 Lu3 Lu1 122.3(8) 6_565 6_565 ?
Lu7 Lu3 Lu1 54.3(5) . 6_565 ?
Lu7 Lu3 Lu1 54.3(5) 6_565 . ?
Lu7 Lu3 Lu1 122.3(8) . . ?
Lu1 Lu3 Lu1 71.7(7) 6_565 . ?
Lu7 Lu3 Lu4 87.7(6) 6_565 . ?
Lu7 Lu3 Lu4 87.7(6) . . ?
Lu1 Lu3 Lu4 35.9(3) 6_565 . ?
Lu1 Lu3 Lu4 35.9(3) . . ?
Lu7 Lu3 N1 73.3(5) 6_565 . ?
Lu7 Lu3 N1 73.3(5) . . ?
Lu1 Lu3 N1 72.4(4) 6_565 . ?
Lu1 Lu3 N1 72.4(4) . . ?
Lu4 Lu3 N1 66.2(4) . . ?
Lu7 Lu3 C13 109.4(6) 6_565 . ?
Lu7 Lu3 C13 98.6(5) . . ?
Lu1 Lu3 C13 118.8(4) 6_565 . ?
Lu1 Lu3 C13 126.4(5) . . ?
Lu4 Lu3 C13 133.4(5) . . ?
N1 Lu3 C13 159.4(5) . . ?
Lu7 Lu3 C12 110.2(6) 6_565 . ?
Lu7 Lu3 C12 81.4(6) . . ?
Lu1 Lu3 C12 127.4(4) 6_565 . ?
Lu1 Lu3 C12 155.7(4) . . ?
Lu4 Lu3 C12 160.7(3) . . ?
N1 Lu3 C12 124.5(5) . . ?
C13 Lu3 C12 34.89(12) . . ?
Lu7 Lu3 C32 77.5(5) 6_565 . ?
Lu7 Lu3 C32 134.5(6) . . ?
Lu1 Lu3 C32 128.5(5) 6_565 . ?
Lu1 Lu3 C32 93.4(4) . . ?
Lu4 Lu3 C32 116.5(4) . . ?
N1 Lu3 C32 150.5(2) . . ?
C13 Lu3 C32 36.44(11) . . ?
C12 Lu3 C32 63.25(19) . . ?
Lu7 Lu3 C14 134.0(6) 6_565 . ?
Lu7 Lu3 C14 80.6(6) . . ?
Lu1 Lu3 C14 82.6(4) 6_565 . ?
Lu1 Lu3 C14 113.5(5) . . ?
Lu4 Lu3 C14 101.3(4) . . ?
N1 Lu3 C14 151.2(3) . . ?
C13 Lu3 C14 36.42(11) . . ?
C12 Lu3 C14 61.41(17) . . ?
C32 Lu3 C14 58.04(16) . . ?
Lu7 Lu3 Lu8 53.9(6) 6_565 . ?
Lu7 Lu3 Lu8 113.3(7) . . ?
Lu1 Lu3 Lu8 68.6(5) 6_565 . ?
Lu1 Lu3 Lu8 14.4(3) . . ?
Lu4 Lu3 Lu8 33.9(3) . . ?
N1 Lu3 Lu8 58.1(4) . . ?
C13 Lu3 Lu8 140.6(4) . . ?
C12 Lu3 Lu8 163.9(4) . . ?
C32 Lu3 Lu8 106.4(4) . . ?
C14 Lu3 Lu8 125.4(5) . . ?
Lu7 Lu3 Lu8 113.3(7) 6_565 6_565 ?
Lu7 Lu3 Lu8 53.9(6) . 6_565 ?
Lu1 Lu3 Lu8 14.4(3) 6_565 6_565 ?
Lu1 Lu3 Lu8 68.6(5) . 6_565 ?
Lu4 Lu3 Lu8 33.9(3) . 6_565 ?
N1 Lu3 Lu8 58.1(4) . 6_565 ?
C13 Lu3 Lu8 132.4(4) . 6_565 ?
C12 Lu3 Lu8 133.9(4) . 6_565 ?
C32 Lu3 Lu8 141.2(5) . 6_565 ?
C14 Lu3 Lu8 96.7(4) . 6_565 ?
Lu8 Lu3 Lu8 62.1(7) . 6_565 ?
Lu1 Lu4 Lu1 109.2(14) 6_565 . ?
Lu1 Lu4 Lu8 50.9(6) 6_565 6_565 ?
Lu1 Lu4 Lu8 148.8(10) . 6_565 ?
Lu1 Lu4 Lu8 148.8(10) 6_565 . ?
Lu1 Lu4 Lu8 50.9(6) . . ?
Lu8 Lu4 Lu8 131.2(12) 6_565 . ?
Lu1 Lu4 Lu3 54.7(7) 6_565 . ?
Lu1 Lu4 Lu3 54.7(7) . . ?
Lu8 Lu4 Lu3 99.8(7) 6_565 . ?
Lu8 Lu4 Lu3 99.8(7) . . ?
Lu1 Lu4 N1 77.8(5) 6_565 . ?
Lu1 Lu4 N1 77.8(5) . . ?
Lu8 Lu4 N1 74.4(5) 6_565 . ?
Lu8 Lu4 N1 74.4(5) . . ?
Lu3 Lu4 N1 64.9(4) . . ?
Lu1 Lu4 Lu7 22.0(6) 6_565 . ?
Lu1 Lu4 Lu7 91.5(8) . . ?
Lu8 Lu4 Lu7 62.2(7) 6_565 . ?
Lu8 Lu4 Lu7 126.8(7) . . ?
Lu3 Lu4 Lu7 37.8(3) . . ?
N1 Lu4 Lu7 60.0(4) . . ?
Lu1 Lu4 Lu7 91.5(8) 6_565 6_565 ?
Lu1 Lu4 Lu7 22.0(6) . 6_565 ?
Lu8 Lu4 Lu7 126.8(7) 6_565 6_565 ?
Lu8 Lu4 Lu7 62.2(7) . 6_565 ?
Lu3 Lu4 Lu7 37.8(3) . 6_565 ?
N1 Lu4 Lu7 60.0(4) . 6_565 ?
Lu7 Lu4 Lu7 71.6(7) . 6_565 ?
Lu1 Lu4 C58 104.6(6) 6_565 . ?
Lu1 Lu4 C58 109.4(6) . . ?
Lu8 Lu4 C58 99.8(6) 6_565 . ?
Lu8 Lu4 C58 105.1(6) . . ?
Lu3 Lu4 C58 124.0(5) . . ?
N1 Lu4 C58 170.6(5) . . ?
Lu7 Lu4 C58 124.3(5) . . ?
Lu7 Lu4 C58 128.4(5) 6_565 . ?
Lu1 Lu4 C59 120.0(6) 6_565 . ?
Lu1 Lu4 C59 124.1(7) . . ?
Lu8 Lu4 C59 86.3(7) 6_565 . ?
Lu8 Lu4 C59 90.2(7) . . ?
Lu3 Lu4 C59 159.9(5) . . ?
N1 Lu4 C59 135.1(5) . . ?
Lu7 Lu4 C59 141.5(4) . . ?
Lu7 Lu4 C59 145.7(4) 6_565 . ?
C58 Lu4 C59 35.85(12) . . ?
Lu1 Lu4 C57 122.0(7) 6_565 . ?
Lu1 Lu4 C57 75.2(5) . . ?
Lu8 Lu4 C57 134.5(6) 6_565 . ?
Lu8 Lu4 C57 79.8(5) . . ?
Lu3 Lu4 C57 106.8(4) . . ?
N1 Lu4 C57 150.7(2) . . ?
Lu7 Lu4 C57 131.4(5) . . ?
Lu7 Lu4 C57 95.6(4) 6_565 . ?
C58 Lu4 C57 34.66(10) . . ?
C59 Lu4 C57 57.53(17) . . ?
Lu1 Lu4 C35 73.5(6) 6_565 . ?
Lu1 Lu4 C35 99.7(7) . . ?
Lu8 Lu4 C35 96.6(6) 6_565 . ?
Lu8 Lu4 C35 128.3(6) . . ?
Lu3 Lu4 C35 87.8(4) . . ?
N1 Lu4 C35 148.6(5) . . ?
Lu7 Lu4 C35 89.0(4) . . ?
Lu7 Lu4 C35 107.9(5) 6_565 . ?
C58 Lu4 C35 38.15(12) . . ?
C59 Lu4 C35 72.3(2) . . ?
C57 Lu4 C35 49.51(14) . . ?
Lu2 Lu5 Lu10 146.8(8) . . ?
Lu2 Lu5 Lu9 77.0(6) . . ?
Lu10 Lu5 Lu9 82.6(9) . . ?
Lu2 Lu5 C7 119.1(5) . . ?
Lu10 Lu5 C7 94.2(9) . . ?
Lu9 Lu5 C7 128.0(5) . . ?
Lu2 Lu5 C6 81.2(4) . . ?
Lu10 Lu5 C6 130.8(9) . . ?
Lu9 Lu5 C6 109.8(5) . . ?
C7 Lu5 C6 40.12(11) . . ?
Lu2 Lu5 N1 75.8(4) . . ?
Lu10 Lu5 N1 71.4(8) . . ?
Lu9 Lu5 N1 62.0(5) . . ?
C7 Lu5 N1 162.2(5) . . ?
C6 Lu5 N1 156.8(6) . . ?
Lu2 Lu5 C8 111.7(4) . . ?
Lu10 Lu5 C8 93.0(9) . . ?
Lu9 Lu5 C8 167.8(6) . . ?
C7 Lu5 C8 40.64(12) . . ?
C6 Lu5 C8 64.80(16) . . ?
N1 Lu5 C8 127.4(4) . . ?
Lu2 Lu5 Lu6 48.2(4) . . ?
Lu10 Lu5 Lu6 107.3(8) . . ?
Lu9 Lu5 Lu6 28.9(5) . . ?
C7 Lu5 Lu6 137.8(4) . . ?
C6 Lu5 Lu6 102.8(4) . . ?
N1 Lu5 Lu6 58.9(3) . . ?
C8 Lu5 Lu6 159.4(5) . . ?
Lu2 Lu5 C5 51.6(3) . . ?
Lu10 Lu5 C5 160.2(9) . . ?
Lu9 Lu5 C5 115.2(6) . . ?
C7 Lu5 C5 68.30(19) . . ?
C6 Lu5 C5 37.20(14) . . ?
N1 Lu5 C5 123.6(5) . . ?
C8 Lu5 C5 67.77(18) . . ?
Lu6 Lu5 C5 92.3(4) . . ?
Lu2 Lu5 C20 82.5(4) . . ?
Lu10 Lu5 C20 117.2(9) . . ?
Lu9 Lu5 C20 74.9(5) . . ?
C7 Lu5 C20 60.77(17) . . ?
C6 Lu5 C20 36.27(12) . . ?
N1 Lu5 C20 134.8(4) . . ?
C8 Lu5 C20 97.3(2) . . ?
Lu6 Lu5 C20 77.0(4) . . ?
C5 Lu5 C20 63.2(2) . . ?
Lu2 Lu5 C22 138.2(4) . . ?
Lu10 Lu5 C22 70.0(8) . . ?
Lu9 Lu5 C22 97.5(5) . . ?
C7 Lu5 C22 35.89(13) . . ?
C6 Lu5 C22 61.38(18) . . ?
N1 Lu5 C22 138.3(5) . . ?
C8 Lu5 C22 70.3(2) . . ?
Lu6 Lu5 C22 119.7(4) . . ?
C5 Lu5 C22 97.7(2) . . ?
C20 Lu5 C22 56.47(16) . . ?
Lu2 Lu5 Lu7 28.2(3) . . ?
Lu10 Lu5 Lu7 122.1(8) . . ?
Lu9 Lu5 Lu7 79.0(6) . . ?
C7 Lu5 Lu7 139.2(4) . . ?
C6 Lu5 Lu7 107.1(5) . . ?
N1 Lu5 Lu7 51.4(4) . . ?
C8 Lu5 Lu7 112.8(4) . . ?
Lu6 Lu5 Lu7 53.0(4) . . ?
C5 Lu5 Lu7 72.4(4) . . ?
C20 Lu5 Lu7 110.0(5) . . ?
C22 Lu5 Lu7 166.3(5) . . ?
Lu9 Lu6 Lu8 127.6(13) . 6_565 ?
Lu9 Lu6 Lu2 95.3(11) . . ?
Lu8 Lu6 Lu2 101.4(8) 6_565 . ?
Lu9 Lu6 Lu1 130.0(10) . 6_565 ?
Lu8 Lu6 Lu1 25.6(6) 6_565 6_565 ?
Lu2 Lu6 Lu1 75.8(5) . 6_565 ?
Lu9 Lu6 C39 98.0(10) . . ?
Lu8 Lu6 C39 105.8(8) 6_565 . ?
Lu2 Lu6 C39 132.2(6) . . ?
Lu1 Lu6 C39 124.5(6) 6_565 . ?
Lu9 Lu6 C38 137.5(11) . . ?
Lu8 Lu6 C38 78.4(8) 6_565 . ?
Lu2 Lu6 C38 113.3(6) . . ?
Lu1 Lu6 C38 88.7(6) 6_565 . ?
C39 Lu6 C38 39.41(17) . . ?
Lu9 Lu6 Lu7 120.8(10) . . ?
Lu8 Lu6 Lu7 58.8(7) 6_565 . ?
Lu2 Lu6 Lu7 42.6(4) . . ?
Lu1 Lu6 Lu7 33.2(4) 6_565 . ?
C39 Lu6 Lu7 140.0(7) . . ?
C38 Lu6 Lu7 101.2(6) . . ?
Lu9 Lu6 N1 72.6(9) . . ?
Lu8 Lu6 N1 67.9(6) 6_565 . ?
Lu2 Lu6 N1 69.5(4) . . ?
Lu1 Lu6 N1 58.1(4) 6_565 . ?
C39 Lu6 N1 157.9(6) . . ?
C38 Lu6 N1 145.7(7) . . ?
Lu7 Lu6 N1 56.3(4) . . ?
Lu9 Lu6 Lu5 59.7(9) . . ?
Lu8 Lu6 Lu5 119.1(7) 6_565 . ?
Lu2 Lu6 Lu5 35.9(3) . . ?
Lu1 Lu6 Lu5 97.1(4) 6_565 . ?
C39 Lu6 Lu5 134.7(6) . . ?
C38 Lu6 Lu5 143.2(5) . . ?
Lu7 Lu6 Lu5 68.6(4) . . ?
N1 Lu6 Lu5 58.1(3) . . ?
Lu9 Lu6 C62 81.2(10) . . ?
Lu8 Lu6 C62 90.4(7) 6_565 . ?
Lu2 Lu6 C62 167.1(7) . . ?
Lu1 Lu6 C62 115.9(6) 6_565 . ?
C39 Lu6 C62 37.30(15) . . ?
C38 Lu6 C62 63.8(2) . . ?
Lu7 Lu6 C62 148.7(7) . . ?
N1 Lu6 C62 120.6(5) . . ?
Lu5 Lu6 C62 140.0(7) . . ?
Lu9 Lu6 C40 71.0(10) . . ?
Lu8 Lu6 C40 143.0(8) 6_565 . ?
Lu2 Lu6 C40 108.7(6) . . ?
Lu1 Lu6 C40 158.7(6) 6_565 . ?
C39 Lu6 C40 37.30(18) . . ?
C38 Lu6 C40 70.3(3) . . ?
Lu7 Lu6 C40 145.7(6) . . ?
N1 Lu6 C40 143.3(7) . . ?
Lu5 Lu6 C40 97.9(5) . . ?
C62 Lu6 C40 58.4(2) . . ?
Lu9 Lu6 C18 124.3(13) . . ?
Lu8 Lu6 C18 107.5(9) 6_565 . ?
Lu2 Lu6 C18 63.0(3) . . ?
Lu1 Lu6 C18 95.7(5) 6_565 . ?
C39 Lu6 C18 71.6(3) . . ?
C38 Lu6 C18 54.5(2) . . ?
Lu7 Lu6 C18 78.5(5) . . ?
N1 Lu6 C18 130.3(5) . . ?
Lu5 Lu6 C18 88.8(4) . . ?
C62 Lu6 C18 108.6(4) . . ?
C40 Lu6 C18 69.6(3) . . ?
Lu1 Lu7 Lu3 67.4(8) 6_565 . ?
Lu1 Lu7 Lu2 121.9(9) 6_565 . ?
Lu3 Lu7 Lu2 143.6(10) . . ?
Lu1 Lu7 Lu8 30.6(6) 6_565 6_565 ?
Lu3 Lu7 Lu8 92.7(8) . 6_565 ?
Lu2 Lu7 Lu8 91.3(7) . 6_565 ?
Lu1 Lu7 N1 73.9(5) 6_565 . ?
Lu3 Lu7 N1 70.6(5) . . ?
Lu2 Lu7 N1 78.5(5) . . ?
Lu8 Lu7 N1 65.0(5) 6_565 . ?
Lu1 Lu7 Lu4 17.8(4) 6_565 . ?
Lu3 Lu7 Lu4 54.5(5) . . ?
Lu2 Lu7 Lu4 123.0(6) . . ?
Lu8 Lu7 Lu4 38.3(5) 6_565 . ?
N1 Lu7 Lu4 59.5(4) . . ?
Lu1 Lu7 C3 124.8(8) 6_565 . ?
Lu3 Lu7 C3 120.9(7) . . ?
Lu2 Lu7 C3 84.5(5) . . ?
Lu8 Lu7 C3 126.3(7) 6_565 . ?
N1 Lu7 C3 160.0(7) . . ?
Lu4 Lu7 C3 140.2(6) . . ?
Lu1 Lu7 Lu6 69.2(6) 6_565 . ?
Lu3 Lu7 Lu6 123.0(7) . . ?
Lu2 Lu7 Lu6 52.7(5) . . ?
Lu8 Lu7 Lu6 38.6(5) 6_565 . ?
N1 Lu7 Lu6 63.2(4) . . ?
Lu4 Lu7 Lu6 73.7(4) . . ?
C3 Lu7 Lu6 113.7(6) . . ?
Lu1 Lu7 C15 87.1(7) 6_565 . ?
Lu3 Lu7 C15 96.9(7) . . ?
Lu2 Lu7 C15 117.8(6) . . ?
Lu8 Lu7 C15 101.3(6) 6_565 . ?
N1 Lu7 C15 160.0(7) . . ?
Lu4 Lu7 C15 100.6(6) . . ?
C3 Lu7 C15 39.95(18) . . ?
Lu6 Lu7 C15 115.9(6) . . ?
Lu1 Lu7 C2 150.4(9) 6_565 . ?
Lu3 Lu7 C2 100.7(7) . . ?
Lu2 Lu7 C2 84.3(5) . . ?
Lu8 Lu7 C2 163.0(7) 6_565 . ?
N1 Lu7 C2 129.4(6) . . ?
Lu4 Lu7 C2 152.1(7) . . ?
C3 Lu7 C2 37.07(15) . . ?
Lu6 Lu7 C2 134.1(7) . . ?
C15 Lu7 C2 66.9(3) . . ?
Lu1 Lu7 Lu1 41.0(6) 6_565 . ?
Lu3 Lu7 Lu1 30.2(5) . . ?
Lu2 Lu7 Lu1 133.8(5) . . ?
Lu8 Lu7 Lu1 62.7(5) 6_565 . ?
N1 Lu7 Lu1 56.4(4) . . ?
Lu4 Lu7 Lu1 25.2(2) . . ?
C3 Lu7 Lu1 141.7(6) . . ?
Lu6 Lu7 Lu1 94.2(4) . . ?
C15 Lu7 Lu1 105.0(6) . . ?
C2 Lu7 Lu1 130.7(6) . . ?
Lu1 Lu7 C12 125.9(9) 6_565 . ?
Lu3 Lu7 C12 67.1(6) . . ?
Lu2 Lu7 C12 112.1(6) . . ?
Lu8 Lu7 C12 156.4(8) 6_565 . ?
N1 Lu7 C12 115.4(6) . . ?
Lu4 Lu7 C12 119.7(6) . . ?
C3 Lu7 C12 61.8(2) . . ?
Lu6 Lu7 C12 164.7(7) . . ?
C15 Lu7 C12 71.0(3) . . ?
C2 Lu7 C12 33.66(14) . . ?
Lu1 Lu7 C12 97.1(5) . . ?
Lu1 Lu8 Lu4 48.5(7) . . ?
Lu1 Lu8 Lu6 119.6(13) . 6_565 ?
Lu4 Lu8 Lu6 144.8(10) . 6_565 ?
Lu1 Lu8 Lu7 37.0(7) . 6_565 ?
Lu4 Lu8 Lu7 79.6(8) . 6_565 ?
Lu6 Lu8 Lu7 82.6(8) 6_565 6_565 ?
Lu1 Lu8 C77 98.6(8) . . ?
Lu4 Lu8 C77 98.9(7) . . ?
Lu6 Lu8 C77 116.3(9) 6_565 . ?
Lu7 Lu8 C77 117.5(7) 6_565 . ?
Lu1 Lu8 C78 122.1(10) . . ?
Lu4 Lu8 C78 91.0(8) . . ?
Lu6 Lu8 C78 116.2(9) 6_565 . ?
Lu7 Lu8 C78 155.2(8) 6_565 . ?
C77 Lu8 C78 41.0(2) . . ?
Lu1 Lu8 N1 74.0(7) . . ?
Lu4 Lu8 N1 69.1(6) . . ?
Lu6 Lu8 N1 75.7(6) 6_565 . ?
Lu7 Lu8 N1 62.1(5) 6_565 . ?
C77 Lu8 N1 168.0(8) . . ?
C78 Lu8 N1 135.5(7) . . ?
Lu1 Lu8 Lu1 42.7(8) . 6_565 ?
Lu4 Lu8 Lu1 13.4(4) . 6_565 ?
Lu6 Lu8 Lu1 132.3(8) 6_565 6_565 ?
Lu7 Lu8 Lu1 68.8(5) 6_565 6_565 ?
C77 Lu8 Lu1 110.7(6) . 6_565 ?
C78 Lu8 Lu1 104.1(7) . 6_565 ?
N1 Lu8 Lu1 57.5(4) . 6_565 ?
Lu1 Lu8 Lu9 123.1(10) . 6_565 ?
Lu4 Lu8 Lu9 126.4(8) . 6_565 ?
Lu6 Lu8 Lu9 23.4(6) 6_565 6_565 ?
Lu7 Lu8 Lu9 89.8(7) 6_565 6_565 ?
C77 Lu8 Lu9 131.5(8) . 6_565 ?
C78 Lu8 Lu9 114.0(7) . 6_565 ?
N1 Lu8 Lu9 59.7(5) . 6_565 ?
Lu1 Lu8 Lu9 116.6(6) 6_565 6_565 ?
Lu1 Lu8 Lu3 19.5(5) . . ?
Lu4 Lu8 Lu3 46.3(6) . . ?
Lu6 Lu8 Lu3 109.8(8) 6_565 . ?
Lu7 Lu8 Lu3 33.4(4) 6_565 . ?
C77 Lu8 Lu3 117.7(6) . . ?
C78 Lu8 Lu3 133.8(7) . . ?
N1 Lu8 Lu3 54.5(4) . . ?
Lu1 Lu8 Lu3 35.5(3) 6_565 . ?
Lu9 Lu8 Lu3 107.0(6) 6_565 . ?
Lu1 Lu8 Lu8 68.2(9) . 6_565 ?
Lu4 Lu8 Lu8 24.4(6) . 6_565 ?
Lu6 Lu8 Lu8 127.5(6) 6_565 6_565 ?
Lu7 Lu8 Lu8 90.7(5) 6_565 6_565 ?
C77 Lu8 Lu8 112.9(5) . 6_565 ?
C78 Lu8 Lu8 89.7(5) . 6_565 ?
N1 Lu8 Lu8 55.9(4) . 6_565 ?
Lu1 Lu8 Lu8 25.5(3) 6_565 6_565 ?
Lu9 Lu8 Lu8 105.4(5) 6_565 6_565 ?
Lu3 Lu8 Lu8 58.9(3) . 6_565 ?
Lu1 Lu8 C76 112.9(9) . . ?
Lu4 Lu8 C76 133.4(7) . . ?
Lu6 Lu8 C76 81.1(8) 6_565 . ?
Lu7 Lu8 C76 108.6(7) 6_565 . ?
C77 Lu8 C76 35.8(2) . . ?
C78 Lu8 C76 62.2(3) . . ?
N1 Lu8 C76 155.8(7) . . ?
Lu1 Lu8 C76 143.2(6) 6_565 . ?
Lu9 Lu8 C76 99.9(7) 6_565 . ?
Lu3 Lu8 C76 130.5(6) . . ?
Lu8 Lu8 C76 148.2(4) 6_565 . ?
Lu6 Lu9 Lu5 91.4(10) . . ?
Lu6 Lu9 Lu2 53.4(8) . . ?
Lu5 Lu9 Lu2 38.1(3) . . ?
Lu6 Lu9 C41 114.5(12) . . ?
Lu5 Lu9 C41 124.4(8) . . ?
Lu2 Lu9 C41 132.1(8) . . ?
Lu6 Lu9 N1 77.9(9) . . ?
Lu5 Lu9 N1 63.7(4) . . ?
Lu2 Lu9 N1 64.1(4) . . ?
C41 Lu9 N1 163.2(9) . . ?
Lu6 Lu9 Lu8 29.0(8) . 6_565 ?
Lu5 Lu9 Lu8 98.5(7) . 6_565 ?
Lu2 Lu9 Lu8 66.7(6) . 6_565 ?
C41 Lu9 Lu8 128.3(8) . 6_565 ?
N1 Lu9 Lu8 57.7(5) . 6_565 ?
Lu6 Lu9 C40 80.9(11) . . ?
Lu5 Lu9 C40 111.7(7) . . ?
Lu2 Lu9 C40 98.6(7) . . ?
C41 Lu9 C40 37.7(2) . . ?
N1 Lu9 C40 158.1(9) . . ?
Lu8 Lu9 C40 104.1(8) 6_565 . ?
Lu6 Lu9 C63 106.9(11) . . ?
Lu5 Lu9 C63 158.3(9) . . ?
Lu2 Lu9 C63 155.9(9) . . ?
C41 Lu9 C63 37.1(2) . . ?
N1 Lu9 C63 130.6(8) . . ?
Lu8 Lu9 C63 103.2(7) 6_565 . ?
C40 Lu9 C63 61.6(3) . . ?
Lu6 Lu9 Lu10 122.1(11) . . ?
Lu5 Lu9 Lu10 36.9(5) . . ?
Lu2 Lu9 Lu10 72.7(6) . . ?
C41 Lu9 Lu10 116.9(9) . . ?
N1 Lu9 Lu10 59.2(6) . . ?
Lu8 Lu9 Lu10 114.7(7) 6_565 . ?
C40 Lu9 Lu10 131.2(8) . . ?
C63 Lu9 Lu10 130.1(10) . . ?
Lu6 Lu9 C62 71.7(10) . . ?
Lu5 Lu9 C62 161.1(9) . . ?
Lu2 Lu9 C62 123.9(8) . . ?
C41 Lu9 C62 59.2(3) . . ?
N1 Lu9 C62 118.7(7) . . ?
Lu8 Lu9 C62 71.0(6) 6_565 . ?
C40 Lu9 C62 58.3(3) . . ?
C63 Lu9 C62 35.3(2) . . ?
Lu10 Lu9 C62 161.9(9) . . ?
Lu6 Lu9 C39 55.6(9) . . ?
Lu5 Lu9 C39 128.7(8) . . ?
Lu2 Lu9 C39 97.1(7) . . ?
C41 Lu9 C39 59.4(3) . . ?
N1 Lu9 C39 129.6(8) . . ?
Lu8 Lu9 C39 71.8(6) 6_565 . ?
C40 Lu9 C39 34.8(2) . . ?
C63 Lu9 C39 58.8(3) . . ?
Lu10 Lu9 C39 162.7(8) . . ?
C62 Lu9 C39 33.8(2) . . ?
Lu6 Lu9 C42 138.9(13) . . ?
Lu5 Lu9 C42 91.4(6) . . ?
Lu2 Lu9 C42 116.6(7) . . ?
C41 Lu9 C42 36.9(2) . . ?
N1 Lu9 C42 138.3(8) . . ?
Lu8 Lu9 C42 163.9(8) 6_565 . ?
C40 Lu9 C42 60.2(3) . . ?
C63 Lu9 C42 67.2(4) . . ?
Lu10 Lu9 C42 80.6(7) . . ?
C62 Lu9 C42 95.8(4) . . ?
C39 Lu9 C42 92.1(4) . . ?
Lu5 Lu10 Lu10 132.6(8) . 6_565 ?
Lu5 Lu10 N1 72.2(9) . . ?
Lu10 Lu10 N1 69.7(5) 6_565 . ?
Lu5 Lu10 C24 114.5(10) . . ?
Lu10 Lu10 C24 94.8(5) 6_565 . ?
N1 Lu10 C24 160.9(9) . . ?
Lu5 Lu10 C23 111.3(10) . . ?
Lu10 Lu10 C23 113.3(5) 6_565 . ?
N1 Lu10 C23 163.8(10) . . ?
C24 Lu10 C23 33.4(3) . . ?
Lu5 Lu10 Lu9 60.5(9) . . ?
Lu10 Lu10 Lu9 116.7(5) 6_565 . ?
N1 Lu10 Lu9 58.1(6) . . ?
C24 Lu10 Lu9 141.1(9) . . ?
C23 Lu10 Lu9 108.8(8) . . ?
Lu5 Lu10 C25 87.6(9) . . ?
Lu10 Lu10 C25 95.8(4) 6_565 . ?
N1 Lu10 C25 129.7(9) . . ?
C24 Lu10 C25 37.9(3) . . ?
C23 Lu10 C25 66.5(5) . . ?
Lu9 Lu10 C25 144.6(9) . . ?
Lu5 Lu10 C22 77.4(8) . . ?
Lu10 Lu10 C22 144.8(5) 6_565 . ?
N1 Lu10 C22 145.5(10) . . ?
C24 Lu10 C22 50.9(4) . . ?
C23 Lu10 C22 33.9(3) . . ?
Lu9 Lu10 C22 92.9(7) . . ?
C25 Lu10 C22 63.3(4) . . ?
Lu5 Lu10 C44 127.7(10) . . ?
Lu10 Lu10 C44 99.1(4) 6_565 . ?
N1 Lu10 C44 133.6(8) . . ?
C24 Lu10 C44 58.0(5) . . ?
C23 Lu10 C44 31.6(3) . . ?
Lu9 Lu10 C44 93.1(8) . . ?
C25 Lu10 C44 95.4(7) . . ?
C22 Lu10 C44 58.5(4) . . ?
Lu5 Lu10 C47 146.1(11) . . ?
Lu10 Lu10 C47 61.3(4) 6_565 . ?
N1 Lu10 C47 131.0(7) . . ?
C24 Lu10 C47 35.3(3) . . ?
C23 Lu10 C47 54.6(5) . . ?
Lu9 Lu10 C47 149.1(10) . . ?
C25 Lu10 C47 58.7(5) . . ?
C22 Lu10 C47 83.4(6) . . ?
C44 Lu10 C47 59.0(5) . . ?
Lu5 Lu10 C7 54.2(6) . . ?
Lu10 Lu10 C7 142.5(4) 6_565 . ?
N1 Lu10 C7 125.4(9) . . ?
C24 Lu10 C7 60.8(4) . . ?
C23 Lu10 C7 62.7(4) . . ?
Lu9 Lu10 C7 98.4(8) . . ?
C25 Lu10 C7 47.2(3) . . ?
C22 Lu10 C7 33.6(2) . . ?
C44 Lu10 C7 91.5(6) . . ?
C47 Lu10 C7 95.4(6) . . ?
Lu5 Lu10 Lu2 16.5(5) . . ?
Lu10 Lu10 Lu2 120.7(4) 6_565 . ?
N1 Lu10 Lu2 55.9(5) . . ?
C24 Lu10 Lu2 130.8(7) . . ?
C23 Lu10 Lu2 125.7(7) . . ?
Lu9 Lu10 Lu2 51.5(6) . . ?
C25 Lu10 Lu2 100.9(7) . . ?
C22 Lu10 Lu2 92.2(6) . . ?
C44 Lu10 Lu2 134.7(7) . . ?
C47 Lu10 Lu2 158.9(8) . . ?
C7 Lu10 Lu2 70.7(5) . . ?
C9 C1 C5 121.2 . . ?
C9 C1 C2 113.7 . . ?
C5 C1 C2 109.5 . . ?
C9 C1 Lu2 93.49(15) . . ?
C5 C1 Lu2 54.83(16) . . ?
C2 C1 Lu2 82.50(18) . . ?
C9 C1 Lu5 67.75(19) . . ?
C5 C1 Lu5 63.10(17) . . ?
C2 C1 Lu5 106.31(15) . . ?
Lu2 C1 Lu5 29.81(17) . . ?
C9 C1 Lu7 96.3(2) . . ?
C5 C1 Lu7 79.6(3) . . ?
C2 C1 Lu7 52.9(2) . . ?
Lu2 C1 Lu7 31.2(2) . . ?
Lu5 C1 Lu7 53.8(3) . . ?
C12 C2 C3 116.0 . . ?
C12 C2 C1 129.4 . . ?
C3 C2 C1 107.5 . . ?
C12 C2 Lu7 78.4(3) . . ?
C3 C2 Lu7 66.8(3) . . ?
C1 C2 Lu7 97.1(3) . . ?
C12 C2 Lu2 107.25(14) . . ?
C3 C2 Lu2 70.23(14) . . ?
C1 C2 Lu2 64.28(15) . . ?
Lu7 C2 Lu2 34.5(3) . . ?
C12 C2 Lu3 51.97(14) . . ?
C3 C2 Lu3 84.28(16) . . ?
C1 C2 Lu3 111.69(14) . . ?
Lu7 C2 Lu3 26.5(3) . . ?
Lu2 C2 Lu3 57.66(15) . . ?
C2 C3 C4 107.4 . . ?
C2 C3 C15 116.9 . . ?
C4 C3 C15 125.9 . . ?
C2 C3 Lu7 76.1(3) . . ?
C4 C3 Lu7 90.9(4) . . ?
C15 C3 Lu7 72.3(4) . . ?
C2 C3 Lu2 77.49(14) . . ?
C4 C3 Lu2 57.30(15) . . ?
C15 C3 Lu2 103.09(15) . . ?
Lu7 C3 Lu2 36.0(3) . . ?
C5 C4 C3 109.0 . . ?
C5 C4 C18 109.7 . . ?
C3 C4 C18 121.9 . . ?
C5 C4 Lu2 62.63(18) . . ?
C3 C4 Lu2 87.47(19) . . ?
C18 C4 Lu2 74.13(16) . . ?
C5 C4 Lu7 87.9(3) . . ?
C3 C4 Lu7 55.7(2) . . ?
C18 C4 Lu7 84.4(2) . . ?
Lu2 C4 Lu7 34.3(3) . . ?
C1 C5 C4 105.7 . . ?
C1 C5 C6 121.6 . . ?
C4 C5 C6 128.3 . . ?
C1 C5 Lu2 87.86(19) . . ?
C4 C5 Lu2 75.94(19) . . ?
C6 C5 Lu2 85.6(2) . . ?
C1 C5 Lu5 85.57(18) . . ?
C4 C5 Lu5 108.87(19) . . ?
C6 C5 Lu5 59.51(18) . . ?
Lu2 C5 Lu5 33.64(19) . . ?
C7 C6 C20 106.3 . . ?
C7 C6 C5 122.2 . . ?
C20 C6 C5 121.3 . . ?
C7 C6 Lu5 69.9(3) . . ?
C20 C6 Lu5 84.46(19) . . ?
C5 C6 Lu5 83.3(2) . . ?
C7 C6 Lu2 103.26(15) . . ?
C20 C6 Lu2 85.02(15) . . ?
C5 C6 Lu2 55.05(14) . . ?
Lu5 C6 Lu2 35.1(2) . . ?
C6 C7 C22 108.9 . . ?
C6 C7 C8 103.5 . . ?
C22 C7 C8 132.3 . . ?
C6 C7 Lu5 70.0(3) . . ?
C22 C7 Lu5 85.8(2) . . ?
C8 C7 Lu5 73.4(2) . . ?
C6 C7 Lu10 99.6(5) . . ?
C22 C7 Lu10 65.1(4) . . ?
C8 C7 Lu10 75.8(4) . . ?
Lu5 C7 Lu10 31.7(5) . . ?
C9 C8 C25 125.5 . . ?
C9 C8 C7 140.4 . . ?
C25 C8 C7 86.8 . . ?
C9 C8 Lu5 87.8(2) . . ?
C25 C8 Lu5 93.3(3) . . ?
C7 C8 Lu5 65.97(19) . . ?
C9 C8 Lu10 101.7(4) . . ?
C25 C8 Lu10 62.8(5) . . ?
C7 C8 Lu10 71.0(4) . . ?
Lu5 C8 Lu10 30.8(5) . . ?
C8 C9 C1 107.7 . . ?
C8 C9 C10 126.4 . . ?
C1 C9 C10 122.0 . . ?
C8 C9 Lu5 60.31(18) . . ?
C1 C9 Lu5 81.3(2) . . ?
C10 C9 Lu5 106.62(15) . . ?
C8 C9 Lu2 84.35(15) . . ?
C1 C9 Lu2 56.28(12) . . ?
C10 C9 Lu2 106.26(13) . . ?
Lu5 C9 Lu2 28.74(19) . . ?
C11 C10 C27 135.0 . . ?
C11 C10 C9 118.0 . . ?
C27 C10 C9 103.6 . . ?
C10 C11 C30 122.7 . . ?
C10 C11 C12 127.5 . . ?
C30 C11 C12 105.2 . . ?
C10 C11 Lu3 112.46(14) . . ?
C30 C11 Lu3 76.84(14) . . ?
C12 C11 Lu3 56.19(14) . . ?
C13 C12 C2 122.7 . . ?
C13 C12 C11 124.3 . . ?
C2 C12 C11 109.0 . . ?
C13 C12 Lu3 65.20(19) . . ?
C2 C12 Lu3 99.44(16) . . ?
C11 C12 Lu3 88.54(19) . . ?
C13 C12 Lu7 82.6(3) . . ?
C2 C12 Lu7 68.0(3) . . ?
C11 C12 Lu7 100.0(3) . . ?
Lu3 C12 Lu7 31.5(3) . . ?
C12 C13 C32 124.4 . . ?
C12 C13 C14 119.3 . . ?
C32 C13 C14 107.0 . . ?
C12 C13 Lu3 79.9(2) . . ?
C32 C13 Lu3 79.44(18) . . ?
C14 C13 Lu3 80.2(2) . . ?
C12 C13 Lu7 67.4(3) . . ?
C32 C13 Lu7 108.2(3) . . ?
C14 C13 Lu7 67.6(3) . . ?
Lu3 C13 Lu7 29.1(2) . . ?
C15 C14 C34 119.0 . . ?
C15 C14 C13 124.9 . . ?
C34 C14 C13 109.2 . . ?
C15 C14 Lu3 96.99(16) . . ?
C34 C14 Lu3 82.6(2) . . ?
C13 C14 Lu3 63.4(2) . . ?
C15 C14 Lu7 66.0(3) . . ?
C34 C14 Lu7 100.8(3) . . ?
C13 C14 Lu7 80.8(3) . . ?
Lu3 C14 Lu7 31.2(3) . . ?
C14 C15 C16 124.7 . . ?
C14 C15 C3 119.0 . . ?
C16 C15 C3 108.8 . . ?
C14 C15 Lu7 85.0(4) . . ?
C16 C15 Lu7 88.9(3) . . ?
C3 C15 Lu7 67.8(3) . . ?
C14 C15 Lu3 57.23(14) . . ?
C16 C15 Lu3 101.73(17) . . ?
C3 C15 Lu3 87.31(18) . . ?
Lu7 C15 Lu3 28.0(3) . . ?
C36 C16 C17 106.2 . . ?
C36 C16 C15 121.0 . . ?
C17 C16 C15 124.3 . . ?
C36 C16 Lu7 96.6(2) . . ?
C17 C16 Lu7 92.0(3) . . ?
C15 C16 Lu7 57.1(2) . . ?
C38 C17 C16 108.0 . . ?
C38 C17 C18 92.6 . . ?
C16 C17 C18 124.0 . . ?
C38 C17 Lu6 50.38(19) . . ?
C16 C17 Lu6 94.2(3) . . ?
C18 C17 Lu6 60.1(3) . . ?
C19 C18 C17 135.1 . . ?
C19 C18 C4 118.2 . . ?
C17 C18 C4 106.6 . . ?
C19 C18 Lu2 87.30(18) . . ?
C17 C18 Lu2 110.64(18) . . ?
C4 C18 Lu2 65.05(14) . . ?
C19 C18 Lu6 77.7(3) . . ?
C17 C18 Lu6 87.6(3) . . ?
C4 C18 Lu6 107.0(2) . . ?
Lu2 C18 Lu6 43.8(2) . . ?
C18 C19 C20 128.3 . . ?
C18 C19 C40 119.1 . . ?
C20 C19 C40 89.5 . . ?
C18 C19 Lu6 68.1(3) . . ?
C20 C19 Lu6 92.2(3) . . ?
C40 C19 Lu6 64.2(2) . . ?
C18 C19 Lu2 58.88(15) . . ?
C20 C19 Lu2 75.40(15) . . ?
C40 C19 Lu2 99.77(12) . . ?
Lu6 C19 Lu2 39.5(2) . . ?
C18 C19 Lu9 90.7(3) . . ?
C20 C19 Lu9 72.2(4) . . ?
C40 C19 Lu9 53.5(3) . . ?
Lu6 C19 Lu9 23.6(3) . . ?
Lu2 C19 Lu9 46.7(3) . . ?
C21 C20 C6 108.5 . . ?
C21 C20 C19 138.0 . . ?
C6 C20 C19 108.5 . . ?
C21 C20 Lu5 81.9(2) . . ?
C6 C20 Lu5 59.28(15) . . ?
C19 C20 Lu5 100.7(2) . . ?
C21 C20 Lu2 110.08(13) . . ?
C6 C20 Lu2 61.66(12) . . ?
C19 C20 Lu2 71.89(14) . . ?
Lu5 C20 Lu2 30.6(2) . . ?
C21 C20 Lu9 76.3(4) . . ?
C6 C20 Lu9 102.7(3) . . ?
C19 C20 Lu9 76.8(4) . . ?
Lu5 C20 Lu9 44.8(3) . . ?
Lu2 C20 Lu9 47.0(3) . . ?
C42 C21 C22 118.0 . . ?
C42 C21 C20 123.6 . . ?
C22 C21 C20 108.4 . . ?
C42 C21 Lu5 104.90(14) . . ?
C22 C21 Lu5 66.79(18) . . ?
C20 C21 Lu5 65.5(2) . . ?
C42 C21 Lu9 67.4(3) . . ?
C22 C21 Lu9 102.5(3) . . ?
C20 C21 Lu9 73.0(4) . . ?
Lu5 C21 Lu9 42.9(3) . . ?
C23 C22 C21 113.6 . . ?
C23 C22 C7 128.8 . . ?
C21 C22 C7 107.8 . . ?
C23 C22 Lu10 66.8(5) . . ?
C21 C22 Lu10 95.0(5) . . ?
C7 C22 Lu10 81.3(5) . . ?
C23 C22 Lu5 99.4(2) . . ?
C21 C22 Lu5 81.40(18) . . ?
C7 C22 Lu5 58.34(15) . . ?
Lu10 C22 Lu5 32.6(5) . . ?
C24 C23 C44 125.8 . . ?
C24 C23 C22 97.5 . . ?
C44 C23 C22 127.8 . . ?
C24 C23 Lu10 71.7(5) . . ?
C44 C23 Lu10 87.6(4) . . ?
C22 C23 Lu10 79.3(5) . . ?
C23 C24 C47 107.2 . . ?
C23 C24 C25 132.3 . . ?
C47 C24 C25 109.3 . . ?
C23 C24 Lu10 74.9(5) . . ?
C47 C24 Lu10 86.5(5) . . ?
C25 C24 Lu10 77.7(5) . . ?
C8 C25 C24 134.1 . . ?
C8 C25 C26 107.6 . . ?
C24 C25 C26 107.0 . . ?
C8 C25 Lu10 85.5(5) . . ?
C24 C25 Lu10 64.4(5) . . ?
C26 C25 Lu10 91.5(4) . . ?
C8 C25 Lu5 55.32(18) . . ?
C24 C25 Lu5 87.78(18) . . ?
C26 C25 Lu5 103.66(15) . . ?
Lu10 C25 Lu5 30.5(5) . . ?
C27 C26 C48 124.2 . . ?
C27 C26 C25 119.1 . . ?
C48 C26 C25 108.1 . . ?
C27 C26 Lu10 99.3(4) . . ?
C48 C26 Lu10 82.3(4) . . ?
C25 C26 Lu10 56.6(3) . . ?
C10 C27 C26 136.4 . . ?
C10 C27 C28 106.9 . . ?
C26 C27 C28 110.5 . . ?
C50 C28 C29 108.8 . . ?
C50 C28 C27 124.9 . . ?
C29 C28 C27 117.5 . . ?
C30 C29 C52 117.8 . . ?
C30 C29 C28 128.7 . . ?
C52 C29 C28 109.1 . . ?
C29 C30 C31 120.8 . . ?
C29 C30 C11 108.9 . . ?
C31 C30 C11 126.3 . . ?
C29 C30 Lu3 116.94(14) . . ?
C31 C30 Lu3 67.58(16) . . ?
C11 C30 Lu3 72.87(16) . . ?
C32 C31 C54 111.5 . . ?
C32 C31 C30 124.4 . . ?
C54 C31 C30 118.5 . . ?
C32 C31 Lu3 61.78(16) . . ?
C54 C31 Lu3 104.56(17) . . ?
C30 C31 Lu3 82.93(19) . . ?
C31 C32 C33 125.5 . . ?
C31 C32 C13 115.2 . . ?
C33 C32 C13 108.0 . . ?
C31 C32 Lu3 87.05(18) . . ?
C33 C32 Lu3 83.4(2) . . ?
C13 C32 Lu3 64.11(17) . . ?
C31 C32 Lu1 83.97(19) . . ?
C33 C32 Lu1 62.13(15) . . ?
C13 C32 Lu1 92.5(2) . . ?
Lu3 C32 Lu1 30.49(19) . . ?
C56 C33 C32 119.3 . . ?
C56 C33 C34 119.3 . . ?
C32 C33 C34 109.4 . . ?
C56 C33 Lu1 64.3(2) . . ?
C32 C33 Lu1 88.0(2) . . ?
C34 C33 Lu1 84.7(2) . . ?
C56 C33 Lu3 95.97(16) . . ?
C32 C33 Lu3 64.05(19) . . ?
C34 C33 Lu3 74.23(16) . . ?
Lu1 C33 Lu3 32.7(2) . . ?
C35 C34 C14 118.4 . . ?
C35 C34 C33 126.4 . . ?
C14 C34 C33 106.1 . . ?
C35 C34 Lu3 98.78(17) . . ?
C14 C34 Lu3 64.65(17) . . ?
C33 C34 Lu3 73.90(14) . . ?
C35 C34 Lu1 82.4(2) . . ?
C14 C34 Lu1 95.49(18) . . ?
C33 C34 Lu1 64.38(19) . . ?
Lu3 C34 Lu1 30.91(19) . . ?
C35 C34 Lu4 63.57(17) . . ?
C14 C34 Lu4 95.14(17) . . ?
C33 C34 Lu4 85.24(15) . . ?
Lu3 C34 Lu4 38.2(2) . . ?
Lu1 C34 Lu4 21.54(15) . . ?
C34 C35 C58 135.6 . . ?
C34 C35 C36 137.4 . . ?
C58 C35 C36 79.8 . . ?
C34 C35 Lu4 92.6(2) . . ?
C58 C35 Lu4 64.9(2) . . ?
C36 C35 Lu4 82.55(18) . . ?
C34 C35 Lu1 74.65(19) . . ?
C58 C35 Lu1 73.2(2) . . ?
C36 C35 Lu1 103.14(17) . . ?
Lu4 C35 Lu1 21.00(16) . . ?
C34 C35 Lu3 59.48(14) . . ?
C58 C35 Lu3 99.67(14) . . ?
C36 C35 Lu3 98.18(13) . . ?
Lu4 C35 Lu3 36.1(2) . . ?
Lu1 C35 Lu3 28.44(18) . . ?
C16 C36 C37 108.1 . . ?
C16 C36 C35 98.3 . . ?
C37 C36 C35 138.6 . . ?
C16 C36 Lu4 97.17(18) . . ?
C37 C36 Lu4 83.64(19) . . ?
C35 C36 Lu4 61.49(17) . . ?
C60 C37 C36 115.3 . . ?
C60 C37 C38 123.7 . . ?
C36 C37 C38 107.1 . . ?
C60 C37 Lu6 85.9(2) . . ?
C36 C37 Lu6 99.8(2) . . ?
C38 C37 Lu6 50.8(2) . . ?
C17 C38 C39 138.0 . . ?
C17 C38 C37 106.4 . . ?
C39 C38 C37 114.6 . . ?
C17 C38 Lu6 99.1(3) . . ?
C39 C38 Lu6 67.6(3) . . ?
C37 C38 Lu6 97.6(3) . . ?
C38 C39 C62 112.2 . . ?
C38 C39 C40 129.6 . . ?
C62 C39 C40 105.4 . . ?
C38 C39 Lu6 73.0(4) . . ?
C62 C39 Lu6 81.0(3) . . ?
C40 C39 Lu6 81.4(4) . . ?
C38 C39 Lu9 99.3(3) . . ?
C62 C39 Lu9 70.5(4) . . ?
C40 C39 Lu9 63.0(4) . . ?
Lu6 C39 Lu9 26.3(4) . . ?
C41 C40 C39 108.8 . . ?
C41 C40 C19 141.0 . . ?
C39 C40 C19 98.5 . . ?
C41 C40 Lu9 68.1(4) . . ?
C39 C40 Lu9 82.2(4) . . ?
C19 C40 Lu9 89.4(4) . . ?
C41 C40 Lu6 93.5(3) . . ?
C39 C40 Lu6 61.3(3) . . ?
C19 C40 Lu6 75.5(3) . . ?
Lu9 C40 Lu6 28.1(4) . . ?
C63 C41 C40 108.5 . . ?
C63 C41 C42 130.2 . . ?
C40 C41 C42 109.7 . . ?
C63 C41 Lu9 74.7(4) . . ?
C40 C41 Lu9 74.2(5) . . ?
C42 C41 Lu9 86.2(4) . . ?
C63 C41 Lu6 74.2(2) . . ?
C40 C41 Lu6 56.1(2) . . ?
C42 C41 Lu6 102.5(2) . . ?
Lu9 C41 Lu6 21.2(4) . . ?
C43 C42 C21 125.9 . . ?
C43 C42 C41 102.0 . . ?
C21 C42 C41 116.1 . . ?
C43 C42 Lu9 87.3(4) . . ?
C21 C42 Lu9 83.4(3) . . ?
C41 C42 Lu9 56.9(3) . . ?
C42 C43 C44 115.0 . . ?
C42 C43 C65 129.5 . . ?
C44 C43 C65 108.2 . . ?
C42 C43 Lu9 64.4(3) . . ?
C44 C43 Lu9 106.3(3) . . ?
C65 C43 Lu9 79.7(3) . . ?
C23 C44 C43 117.9 . . ?
C23 C44 C45 122.9 . . ?
C43 C44 C45 108.0 . . ?
C23 C44 Lu10 60.7(4) . . ?
C43 C44 Lu10 91.4(4) . . ?
C45 C44 Lu10 87.2(4) . . ?
C46 C45 C66 133.5 . . ?
C46 C45 C44 110.3 . . ?
C66 C45 C44 108.1 . . ?
C46 C45 Lu10 74.9(4) . . ?
C66 C45 Lu10 100.3(4) . . ?
C44 C45 Lu10 63.5(3) . . ?
C47 C46 C45 127.7 . . ?
C47 C46 C69 129.0 . . ?
C45 C46 C69 98.9 . . ?
C47 C46 Lu10 66.6(4) . . ?
C45 C46 Lu10 79.1(4) . . ?
C69 C46 Lu10 110.5(3) . . ?
C46 C47 C24 124.7 . . ?
C46 C47 C48 117.4 . . ?
C24 C47 C48 107.0 . . ?
C46 C47 Lu10 87.8(4) . . ?
C24 C47 Lu10 58.2(4) . . ?
C48 C47 Lu10 92.2(4) . . ?
C49 C48 C26 124.3 . . ?
C49 C48 C47 116.7 . . ?
C26 C48 C47 107.9 . . ?
C48 C49 C70 124.3 . . ?
C48 C49 C50 113.0 . . ?
C70 C49 C50 113.6 . . ?
C28 C50 C51 104.6 . . ?
C28 C50 C49 121.5 . . ?
C51 C50 C49 123.1 . . ?
C72 C51 C52 114.4 . . ?
C72 C51 C50 123.0 . . ?
C52 C51 C50 110.8 . . ?
C53 C52 C29 119.6 . . ?
C53 C52 C51 121.0 . . ?
C29 C52 C51 106.2 . . ?
C54 C53 C74 105.4 . . ?
C54 C53 C52 119.9 . . ?
C74 C53 C52 132.0 . . ?
C53 C54 C55 108.5 . . ?
C53 C54 C31 121.2 . . ?
C55 C54 C31 120.2 . . ?
C75 C55 C56 105.8 . . ?
C75 C55 C54 105.5 . . ?
C56 C55 C54 126.9 . . ?
C75 C55 Lu1 76.8(2) . . ?
C56 C55 Lu1 57.67(17) . . ?
C54 C55 Lu1 89.83(19) . . ?
C75 C55 Lu8 56.5(3) . . ?
C56 C55 Lu8 65.8(3) . . ?
C54 C55 Lu8 99.1(2) . . ?
Lu1 C55 Lu8 20.8(3) . . ?
C55 C56 C33 111.9 . . ?
C55 C56 C57 142.9 . . ?
C33 C56 C57 101.2 . . ?
C55 C56 Lu1 91.9(2) . . ?
C33 C56 Lu1 82.7(3) . . ?
C57 C56 Lu1 75.7(2) . . ?
C55 C56 Lu8 87.2(3) . . ?
C33 C56 Lu8 104.6(3) . . ?
C57 C56 Lu8 68.0(3) . . ?
Lu1 C56 Lu8 22.3(3) . . ?
C55 C56 Lu4 109.77(14) . . ?
C33 C56 Lu4 81.08(18) . . ?
C57 C56 Lu4 58.31(16) . . ?
Lu1 C56 Lu4 18.6(2) . . ?
Lu8 C56 Lu4 27.8(3) . . ?
C77 C57 C58 108.0 . . ?
C77 C57 C56 88.9 . . ?
C58 C57 C56 146.0 . . ?
C77 C57 Lu1 72.1(2) . . ?
C58 C57 Lu1 90.9(2) . . ?
C56 C57 Lu1 65.9(2) . . ?
C77 C57 Lu4 78.15(19) . . ?
C58 C57 Lu4 66.65(18) . . ?
C56 C57 Lu4 89.3(2) . . ?
Lu1 C57 Lu4 24.45(18) . . ?
C77 C57 Lu8 49.6(3) . . ?
C58 C57 Lu8 90.3(3) . . ?
C56 C57 Lu8 78.4(3) . . ?
Lu1 C57 Lu8 24.4(3) . . ?
Lu4 C57 Lu8 31.1(3) . . ?
C57 C58 C59 108.0 . . ?
C57 C58 C35 87.1 . . ?
C59 C58 C35 142.7 . . ?
C57 C58 Lu4 78.69(19) . . ?
C59 C58 Lu4 73.2(2) . . ?
C35 C58 Lu4 76.9(2) . . ?
C57 C58 Lu1 58.76(17) . . ?
C59 C58 Lu1 84.37(17) . . ?
C35 C58 Lu1 74.6(2) . . ?
Lu4 C58 Lu1 20.20(14) . . ?
C57 C58 Lu8 61.0(3) . . ?
C59 C58 Lu8 65.4(3) . . ?
C35 C58 Lu8 95.6(3) . . ?
Lu4 C58 Lu8 26.3(3) . . ?
Lu1 C58 Lu8 21.1(2) . . ?
C58 C59 C78 108.0 . . ?
C58 C59 C60 109.3 . . ?
C78 C59 C60 135.5 . . ?
C58 C59 Lu4 71.0(2) . . ?
C78 C59 Lu4 79.54(18) . . ?
C60 C59 Lu4 90.39(18) . . ?
C58 C59 Lu8 85.9(3) . . ?
C78 C59 Lu8 49.4(3) . . ?
C60 C59 Lu8 110.7(3) . . ?
Lu4 C59 Lu8 30.2(3) . . ?
C37 C60 C61 123.1 . . ?
C37 C60 C59 120.2 . . ?
C61 C60 C59 103.9 . . ?
C37 C60 Lu4 87.41(17) . . ?
C61 C60 Lu4 88.29(17) . . ?
C59 C60 Lu4 57.17(15) . . ?
C62 C61 C60 109.9 . . ?
C62 C61 C80 125.3 . . ?
C60 C61 C80 124.7 . . ?
C62 C61 Lu6 61.7(3) . . ?
C60 C61 Lu6 88.1(3) . . ?
C80 C61 Lu6 113.7(2) . . ?
C62 C61 Lu9 56.9(3) . . ?
C60 C61 Lu9 110.8(3) . . ?
C80 C61 Lu9 97.5(3) . . ?
Lu6 C61 Lu9 22.8(3) . . ?
C61 C62 C63 111.3 . . ?
C61 C62 C39 128.8 . . ?
C63 C62 C39 109.8 . . ?
C61 C62 Lu6 87.3(3) . . ?
C63 C62 Lu6 92.4(3) . . ?
C39 C62 Lu6 61.7(3) . . ?
C61 C62 Lu9 95.1(3) . . ?
C63 C62 Lu9 65.4(4) . . ?
C39 C62 Lu9 75.7(4) . . ?
Lu6 C62 Lu9 27.1(4) . . ?
C41 C63 C64 118.7 . . ?
C41 C63 C62 107.2 . . ?
C64 C63 C62 127.1 . . ?
C41 C63 Lu9 68.2(4) . . ?
C64 C63 Lu9 94.0(4) . . ?
C62 C63 Lu9 79.3(5) . . ?
C41 C63 Lu6 76.7(3) . . ?
C64 C63 Lu6 108.7(2) . . ?
C62 C63 Lu6 56.8(2) . . ?
Lu9 C63 Lu6 22.6(4) . . ?
C65 C64 C63 112.1 . . ?
C65 C64 C81 121.2 . . ?
C63 C64 C81 114.9 . . ?
C65 C64 Lu9 84.5(4) . . ?
C63 C64 Lu9 55.1(3) . . ?
C81 C64 Lu9 94.9(3) . . ?
C64 C65 C43 126.3 . . ?
C64 C65 C66 120.9 . . ?
C43 C65 C66 107.1 . . ?
C45 C66 C65 108.1 . . ?
C45 C66 C67 129.3 . . ?
C65 C66 C67 113.8 . . ?
C68 C67 C82 119.7 . . ?
C68 C67 C66 99.2 . . ?
C82 C67 C66 122.6 . . ?
C67 C68 C85 116.7 . . ?
C67 C68 C69 129.2 . . ?
C85 C68 C69 107.3 . . ?
C70 C69 C68 108.3 . . ?
C70 C69 C46 114.0 . . ?
C68 C69 C46 126.2 . . ?
C69 C70 C71 108.0 . . ?
C69 C70 C49 118.0 . . ?
C71 C70 C49 121.3 . . ?
C85 C71 C70 107.4 . . ?
C85 C71 C72 116.9 . . ?
C70 C71 C72 124.5 . . ?
C51 C72 C73 115.0 . . ?
C51 C72 C71 113.9 . . ?
C73 C72 C71 120.3 . . ?
C74 C73 C72 130.8 . . ?
C74 C73 C86 109.2 . . ?
C72 C73 C86 118.9 . . ?
C53 C74 C75 104.8 . . ?
C53 C74 C73 103.7 . . ?
C75 C74 C73 116.0 . . ?
C55 C75 C74 104.9 . . ?
C55 C75 C76 128.0 . . ?
C74 C75 C76 125.4 . . ?
C55 C75 Lu8 97.4(3) . . ?
C74 C75 Lu8 117.0(3) . . ?
C76 C75 Lu8 72.8(3) . . ?
C55 C75 Lu1 74.61(18) . . ?
C74 C75 Lu1 118.30(17) . . ?
C76 C75 Lu1 90.7(2) . . ?
Lu8 C75 Lu1 23.2(3) . . ?
C75 C76 C87 109.8 . . ?
C75 C76 C77 101.0 . . ?
C87 C76 C77 112.6 . . ?
C75 C76 Lu8 74.5(3) . . ?
C87 C76 Lu8 79.9(3) . . ?
C77 C76 Lu8 52.7(3) . . ?
C57 C77 C78 108.0 . . ?
C57 C77 C76 140.2 . . ?
C78 C77 C76 111.7 . . ?
C57 C77 Lu8 97.4(4) . . ?
C78 C77 Lu8 72.9(4) . . ?
C76 C77 Lu8 91.5(5) . . ?
C57 C77 Lu1 73.3(2) . . ?
C78 C77 Lu1 90.5(2) . . ?
C76 C77 Lu1 103.2(2) . . ?
Lu8 C77 Lu1 26.2(3) . . ?
C57 C77 Lu4 69.06(18) . . ?
C78 C77 Lu4 70.8(2) . . ?
C76 C77 Lu4 121.96(16) . . ?
Lu8 C77 Lu4 31.4(4) . . ?
Lu1 C77 Lu4 23.60(19) . . ?
C79 C78 C59 106.3 . . ?
C79 C78 C77 143.4 . . ?
C59 C78 C77 108.0 . . ?
C79 C78 Lu8 96.1(4) . . ?
C59 C78 Lu8 99.2(4) . . ?
C77 C78 Lu8 66.1(4) . . ?
C79 C78 Lu4 106.36(19) . . ?
C59 C78 Lu4 66.36(17) . . ?
C77 C78 Lu4 76.60(19) . . ?
Lu8 C78 Lu4 32.9(4) . . ?
C79 C78 Lu1 112.37(13) . . ?
C59 C78 Lu1 85.2(2) . . ?
C77 C78 Lu1 58.89(15) . . ?
Lu8 C78 Lu1 18.9(4) . . ?
Lu4 C78 Lu1 21.55(14) . . ?
C78 C79 C88 98.6 . . ?
C78 C79 C80 129.4 . . ?
C88 C79 C80 120.0 . . ?
C78 C79 Lu8 53.5(3) . . ?
C88 C79 Lu8 76.7(3) . . ?
C80 C79 Lu8 102.4(3) . . ?
C81 C80 C79 120.0 . . ?
C81 C80 C61 118.2 . . ?
C79 C80 C61 114.4 . . ?
C80 C81 C82 120.0 . . ?
C80 C81 C64 121.0 . . ?
C82 C81 C64 117.5 . . ?
C81 C82 C83 120.0 . . ?
C81 C82 C67 120.2 . . ?
C83 C82 C67 118.0 . . ?
C88 C83 C82 120.0 . . ?
C88 C83 C84 114.3 . . ?
C82 C83 C84 121.5 . . ?
C83 C84 C85 119.4 . . ?
C83 C84 C86 104.3 . . ?
C85 C84 C86 119.3 . . ?
C84 C85 C71 123.5 . . ?
C84 C85 C68 120.3 . . ?
C71 C85 C68 108.9 . . ?
C87 C86 C84 104.9 . . ?
C87 C86 C73 126.4 . . ?
C84 C86 C73 120.5 . . ?
C86 C87 C88 112.5 . . ?
C86 C87 C76 118.2 . . ?
C88 C87 C76 119.2 . . ?
C86 C87 Lu8 99.4(3) . . ?
C88 C87 Lu8 73.2(3) . . ?
C76 C87 Lu8 67.8(3) . . ?
C83 C88 C79 120.0 . . ?
C83 C88 C87 101.3 . . ?
C79 C88 C87 132.3 . . ?
C83 C88 Lu8 104.5(3) . . ?
C79 C88 Lu8 72.2(3) . . ?
C87 C88 Lu8 75.3(3) . . ?
N2A Ni1A N2A 177.9(4) . 6_565 ?
N2A Ni1A N3A 90.0(2) . . ?
N2A Ni1A N3A 90.0(2) 6_565 . ?
N2A Ni1A N1A 90.0(2) . . ?
N2A Ni1A N1A 90.0(2) 6_565 . ?
N3A Ni1A N1A 178.9(4) . . ?
C6A N2A C13A 104.4(7) . . ?
C6A N2A Ni1A 127.7(6) . . ?
C13A N2A Ni1A 127.8(6) . . ?
C3A C2A C1A 112.6(7) . . ?
N4A Ni2A N4A 180.0(3) 6_565 2_756 ?
N4A Ni2A N4A 89.5(5) 6_565 5_766 ?
N4A Ni2A N4A 90.5(5) 2_756 5_766 ?
N4A Ni2A N4A 90.5(5) 6_565 . ?
N4A Ni2A N4A 89.5(5) 2_756 . ?
N4A Ni2A N4A 180.0 5_766 . ?
C15A N3A C15A 104.6(10) 6_565 . ?
C15A N3A Ni1A 127.7(5) 6_565 . ?
C15A N3A Ni1A 127.7(5) . . ?
C3A C3A C4A 106.4(4) 6_565 . ?
C3A C3A C2A 128.5(5) 6_565 . ?
C4A C3A C2A 125.0(7) . . ?
N1A C4A C5A 124.8(7) . . ?
N1A C4A C3A 111.2(7) . . ?
C5A C4A C3A 124.0(7) . . ?
C27A N4A C20A 103.9(8) . . ?
C27A N4A Ni2A 127.7(6) . . ?
C20A N4A Ni2A 128.4(7) . . ?
C6A C5A C4A 124.7(7) . . ?
C5A C6A N2A 125.2(7) . . ?
C5A C6A C7A 123.7(7) . . ?
N2A C6A C7A 111.1(7) . . ?
C10A C7A C6A 106.2(7) . . ?
C10A C7A C8A 129.8(8) . . ?
C6A C7A C8A 124.0(8) . . ?
C7A C8A C9A 111.8(8) . . ?
C7A C10A C13A 107.3(7) . . ?
C7A C10A C11A 128.7(8) . . ?
C13A C10A C11A 124.1(8) . . ?
C10A C11A C12A 112.8(8) . . ?
C14A C13A N2A 124.9(7) . . ?
C14A C13A C10A 124.1(7) . . ?
N2A C13A C10A 111.0(7) . . ?
C13A C14A C15A 124.8(7) . . ?
C14A C15A N3A 124.7(8) . . ?
C14A C15A C16A 124.6(8) . . ?
N3A C15A C16A 110.7(8) . . ?
C16A C16A C15A 107.0(5) 6_565 . ?
C16A C16A C17A 129.0(5) 6_565 . ?
C15A C16A C17A 123.9(8) . . ?
C16A C17A C18A 114.1(8) . . ?
C20A C19A C20A 124.1(12) . 2_756 ?
C19A C20A N4A 124.8(9) . . ?
C19A C20A C21A 123.9(9) . . ?
N4A C20A C21A 111.3(9) . . ?
C24A C21A C20A 106.8(9) . . ?
C24A C21A C22A 127.6(10) . . ?
C20A C21A C22A 125.6(10) . . ?
C21A C22A C23A 112.6(9) . . ?
C21A C24A C27A 106.5(9) . . ?
C21A C24A C25A 129.5(10) . . ?
C27A C24A C25A 123.9(10) . . ?
C26A C25A C24A 113.4(10) . . ?
N4A C27A C28A 124.8(10) . . ?
N4A C27A C24A 111.6(9) . . ?
C28A C27A C24A 123.7(10) . . ?
C27A C28A C27A 124.5(14) . 6_565 ?
C4A N1A C4A 104.8(10) . 6_565 ?
C4A N1A Ni1A 127.6(5) . . ?
C4A N1A Ni1A 127.6(5) 6_565 . ?
C2D C1D C2D 123(5) 6 . ?
C3D C4D C3D 120(3) 6 . ?
C1D C2D C3D 117(3) . . ?
C2D C3D C4D 118(2) . . ?

_refine_diff_density_max         1.879
_refine_diff_density_min         -6.281
_refine_diff_density_rms         0.207



_vrf_PLAT308_Lu3N@D2-C88         
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2@C1-C88
_database_code_depnum_ccdc_archive 'CCDC 1836827'
_audit_update_record             
;
2018-04-13 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2@C1-C88 Ni(OEP)'
_chemical_name_common            'Lu2@C1-C88 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C88, C36 H44 N4 Ni, 2(C6 H6)'
_chemical_formula_sum            'C136 H56 Lu2 N4 Ni S0'
_chemical_formula_weight         2154.50

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0027 0.0014 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0053 0.0028 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1098 0.1057 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3436 0.9622 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.2922 5.1425 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   24.121(5)
_cell_length_b                   18.190(5)
_cell_length_c                   18.497(5)
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 90.466(5)
_cell_angle_gamma                90.000(5)
_cell_volume                     8115(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9904
_cell_measurement_theta_min      2.975
_cell_measurement_theta_max      25.412

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.763
_exptl_crystal_F_000             4280
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.120
_exptl_crystal_size_mid          0.080
_exptl_crystal_size_min          0.050
_exptl_absorpt_coefficient_mu    2.203
_shelx_estimated_absorpt_T_min   0.809
_shelx_estimated_absorpt_T_max   0.896
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.5739
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline BL17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            53464
_diffrn_reflns_av_unetI/netI     0.0204
_diffrn_reflns_av_R_equivalents  0.0319
_diffrn_reflns_limit_h_min       -28
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_theta_min         2.730
_diffrn_reflns_theta_max         23.235
_diffrn_reflns_theta_full        23.048
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             7719
_reflns_number_gt                6378
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0598P)²+64.2135P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7719
_refine_ls_number_parameters     914
_refine_ls_number_restraints     1029
_refine_ls_R_factor_all          0.0740
_refine_ls_R_factor_gt           0.0586
_refine_ls_wR_factor_ref         0.1530
_refine_ls_wR_factor_gt          0.1370
_refine_ls_goodness_of_fit_ref   1.042
_refine_ls_restrained_S_all      1.067
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.17022(2) 0.0000 0.35160(3) 0.04151(18) Uani 0.5265 2 d S TU P A 1
Lu2 Lu 0.30185(3) 0.08953(4) 0.35106(5) 0.03643(19) Uani 0.2691 1 d . U P A 1
Lu3 Lu 0.2552(2) -0.0240(3) 0.1927(2) 0.0643(14) Uani 0.0662 1 d . U P A 1
Lu4 Lu 0.18258(18) 0.0638(3) 0.3553(3) 0.0799(14) Uani 0.065 1 d . U P A 1
Lu5 Lu 0.2743(3) 0.0887(4) 0.3775(4) 0.103(2) Uani 0.0596 1 d . U P A 1
Lu6 Lu 0.1986(3) 0.0932(3) 0.2909(4) 0.105(2) Uani 0.0633 1 d . U P A 1
Lu7 Lu 0.3094(6) 0.0000 0.3796(7) 0.119(4) Uani 0.045 2 d S TU P A 1
Lu8 Lu 0.3390(3) 0.0000 0.2941(7) 0.175(5) Uani 0.0658 2 d S TU P A 1
Lu9 Lu 0.2356(11) 0.0000 0.4248(8) 0.101(4) Uani 0.0351 2 d S TU P A 1
Lu10 Lu 0.2940(10) 0.0000 0.2008(9) 0.081(4) Uani 0.0247 2 d S TU P A 1
Lu11 Lu 0.2293(10) -0.1001(12) 0.2524(11) 0.095(4) Uani 0.0204 1 d . U P A 1
Lu12 Lu 0.2734(6) -0.0557(8) 0.2086(6) 0.092(3) Uani 0.0342 1 d . U P A 1
Lu13 Lu 0.2060(6) -0.0358(7) 0.4060(6) 0.086(3) Uani 0.0286 1 d . U P A 1
Lu14 Lu 0.2954(11) 0.0963(12) 0.2595(16) 0.099(6) Uani 0.0151 1 d . U P A 1
Lu15 Lu 0.2535(10) 0.0445(14) 0.4145(10) 0.084(4) Uani 0.0175 1 d . U P A 1
Lu16 Lu 0.2235(13) -0.0399(17) 0.2259(12) 0.078(4) Uani 0.0125 1 d . U P A 1
C1 C 0.09446(7) -0.0675(2) 0.26618(16) 0.093(5) Uani 0.5 1 d DG U P A -1
C2 C 0.07638(6) -0.0434(2) 0.34256(17) 0.089(4) Uani 0.5 1 d DG U P A -1
C3 C 0.07766(7) 0.0309(2) 0.36112(17) 0.094(5) Uani 0.5 1 d G U P A -1
C4 C 0.08791(7) 0.0553(2) 0.28562(17) 0.078(4) Uani 0.5 1 d DG U P A -1
C5 C 0.10010(7) 0.0095(2) 0.23414(15) 0.087(3) Uani 0.5 1 d G U P A -1
C6 C 0.15493(11) -0.1386(2) 0.18515(16) 0.102(5) Uani 0.5 1 d G U P A -1
C7 C 0.15462(10) -0.0602(2) 0.15920(12) 0.100(5) Uani 0.5 1 d DG U P A -1
C8 C 0.16029(11) 0.0761(2) 0.14806(13) 0.061(3) Uani 0.5 1 d G U P A -1
C9 C 0.11771(9) -0.1262(2) 0.25423(17) 0.097(6) Uani 0.5 1 d DG U P A -1
C10 C 0.12638(11) -0.1789(2) 0.31921(19) 0.059(3) Uani 0.5 1 d DG U P A -1
C11 C 0.12461(10) -0.1578(2) 0.38977(18) 0.083(4) Uani 0.5 1 d G U P A -1
C12 C 0.09606(8) -0.0863(2) 0.40199(17) 0.085(4) Uani 0.5 1 d G U P A -1
C13 C 0.12532(10) -0.0626(2) 0.46566(14) 0.098(5) Uani 0.5 1 d G U P A -1
C14 C 0.12076(10) 0.0256(2) 0.47273(14) 0.090(5) Uani 0.5 1 d G U P A -1
C15 C 0.09762(9) 0.0617(2) 0.42108(16) 0.107(6) Uani 0.5 1 d G U P A -1
C16 C 0.11684(11) 0.1254(2) 0.40659(18) 0.122(6) Uani 0.5 1 d G U P A -1
C17 C 0.11186(11) 0.1450(2) 0.33730(19) 0.119(6) Uani 0.5 1 d G U P A -1
C18 C 0.11273(10) 0.1292(2) 0.26349(18) 0.089(5) Uani 0.5 1 d DG U P A -1
C19 C 0.14622(11) 0.1365(2) 0.20485(17) 0.058(3) Uani 0.5 1 d G U P A -1
C20 C 0.13488(9) -0.0034(2) 0.17501(13) 0.065(2) Uani 0.5 1 d G U P A -1
C21 C 0.20501(12) 0.0564(2) 0.10927(11) 0.082(4) Uani 0.5 1 d DG U P A -1
C22 C 0.22413(12) -0.0091(3) 0.08717(9) 0.074(3) Uani 0.5 1 d DG U P A -1
C23 C 0.20087(12) -0.0824(2) 0.11036(11) 0.092(5) Uani 0.5 1 d DG U P A -1
C24 C 0.24824(14) -0.1373(2) 0.10930(13) 0.100(5) Uani 0.5 1 d DG U P A -1
C25 C 0.24223(14) -0.1822(2) 0.15029(16) 0.084(5) Uani 0.5 1 d G U P A -1
C26 C 0.19075(13) -0.1916(2) 0.18848(18) 0.072(4) Uani 0.5 1 d G U P A -1
C27 C 0.20518(14) -0.23774(17) 0.2490(2) 0.078(4) Uani 0.5 1 d G U P A -1
C28 C 0.17318(14) -0.22998(17) 0.3181(2) 0.065(3) Uani 0.5 1 d G U P A -1
C29 C 0.20206(14) -0.23316(17) 0.3739(2) 0.082(4) Uani 0.5 1 d G U P A -1
C30 C 0.17015(12) -0.18193(19) 0.42917(18) 0.076(4) Uani 0.5 1 d G U P A -1
C31 C 0.20568(12) -0.1379(2) 0.48019(14) 0.095(5) Uani 0.5 1 d G U P A -1
C32 C 0.17771(11) -0.0722(2) 0.50276(12) 0.095(5) Uani 0.5 1 d G U P A -1
C33 C 0.20635(12) -0.0165(2) 0.52375(9) 0.097(5) Uani 0.5 1 d G U P A -1
C34 C 0.16850(12) 0.0418(2) 0.51084(12) 0.097(5) Uani 0.5 1 d G U P A -1
C35 C 0.18539(13) 0.1200(2) 0.49146(14) 0.126(7) Uani 0.5 1 d DG U P A -1
C36 C 0.16254(13) 0.1553(2) 0.44917(17) 0.116(6) Uani 0.5 1 d G U P A -1
C37 C 0.19528(15) 0.20845(18) 0.4065(2) 0.112(6) Uani 0.5 1 d G U P A -1
C38 C 0.15243(14) 0.20045(19) 0.3329(2) 0.122(6) Uani 0.5 1 d G U P A -1
C39 C 0.19392(15) 0.22745(17) 0.2764(2) 0.111(6) Uani 0.5 1 d G U P A -1
C40 C 0.17957(13) 0.19393(19) 0.21899(19) 0.104(5) Uani 0.5 1 d G U P A -1
C41 C 0.23550(14) 0.1903(2) 0.16763(18) 0.105(6) Uani 0.5 1 d DG U P A -1
C42 C 0.24360(13) 0.1218(2) 0.11981(13) 0.099(5) Uani 0.5 1 d DG U P A -1
C43 C 0.30205(13) 0.1082(2) 0.10228(13) 0.082(4) Uani 0.5 1 d DG U P A -1
C44 C 0.32234(12) 0.0277(3) 0.09104(10) 0.080(4) Uani 0.5 1 d DG U P A -1
C45 C 0.28037(13) -0.0285(3) 0.07770(9) 0.087(4) Uani 0.5 1 d G U P A -1
C46 C 0.29293(13) -0.0863(2) 0.09894(11) 0.101(5) Uani 0.5 1 d DG U P A -1
C47 C 0.33702(12) -0.1198(2) 0.14250(14) 0.096(5) Uani 0.5 1 d G U P A -1
C48 C 0.33192(13) -0.1746(2) 0.18302(17) 0.099(5) Uani 0.5 1 d G U P A -1
C49 C 0.28505(14) -0.21286(19) 0.18865(19) 0.081(4) Uani 0.5 1 d G U P A -1
C50 C 0.26079(15) -0.24863(16) 0.2524(2) 0.069(3) Uani 0.5 1 d G U P A -1
C51 C 0.29045(14) -0.24590(15) 0.3131(2) 0.078(4) Uani 0.5 1 d G U P A -1
C52 C 0.25600(14) -0.23776(15) 0.3811(2) 0.073(4) Uani 0.5 1 d G U P A -1
C53 C 0.28879(13) -0.19132(17) 0.42833(17) 0.071(4) Uani 0.5 1 d G U P A -1
C54 C 0.26080(12) -0.13668(19) 0.47824(13) 0.083(4) Uani 0.5 1 d G U P A -1
C55 C 0.29456(11) -0.0745(2) 0.49039(11) 0.081(4) Uani 0.5 1 d G U P A -1
C56 C 0.26442(12) -0.0103(2) 0.51988(8) 0.099(4) Uani 0.5 1 d G U P A -1
C57 C 0.28577(12) 0.0560(2) 0.51752(10) 0.107(6) Uani 0.5 1 d G U P A -1
C58 C 0.24380(14) 0.1117(2) 0.51127(13) 0.120(6) Uani 0.5 1 d DG U P A -1
C59 C 0.28033(15) 0.17309(19) 0.46504(16) 0.093(5) Uani 0.5 1 d G U P A -1
C60 C 0.25241(15) 0.21384(16) 0.41192(19) 0.108(6) Uani 0.5 1 d G U P A -1
C61 C 0.28727(15) 0.23738(15) 0.3426(2) 0.094(5) Uani 0.5 1 d G U P A -1
C62 C 0.25404(16) 0.24291(15) 0.2845(2) 0.110(6) Uani 0.5 1 d G U P A -1
C63 C 0.28283(15) 0.22090(18) 0.2124(2) 0.091(5) Uani 0.5 1 d G U P A -1
C64 C 0.33585(13) 0.1880(2) 0.20323(18) 0.067(4) Uani 0.5 1 d G U P A -1
C65 C 0.34993(12) 0.1321(2) 0.15146(16) 0.078(4) Uani 0.5 1 d G U P A -1
C66 C 0.38537(10) 0.0786(2) 0.16686(15) 0.078(4) Uani 0.5 1 d G U P A -1
C67 C 0.37042(10) 0.0131(2) 0.12921(13) 0.083(4) Uani 0.5 1 d G U P A -1
C68 C 0.38078(10) -0.0596(2) 0.16064(14) 0.085(5) Uani 0.5 1 d G U P A -1
C69 C 0.40992(8) -0.0740(2) 0.23706(16) 0.086(5) Uani 0.5 1 d G U P A -1
C70 C 0.39438(9) -0.1355(2) 0.27904(18) 0.098(5) Uani 0.5 1 d DG U P A -1
C71 C 0.35510(12) -0.19124(19) 0.25476(19) 0.108(6) Uani 0.5 1 d DG U P A -1
C72 C 0.34290(13) -0.21032(17) 0.3171(2) 0.086(4) Uani 0.5 1 d G U P A -1
C73 C 0.33821(11) -0.17980(17) 0.39082(18) 0.067(3) Uani 0.5 1 d G U P A -1
C74 C 0.37023(9) -0.11237(19) 0.40341(15) 0.065(3) Uani 0.5 1 d G U P A -1
C75 C 0.34757(9) -0.0627(2) 0.45530(12) 0.073(4) Uani 0.5 1 d G U P A -1
C76 C 0.36880(9) 0.0169(2) 0.44855(12) 0.079(4) Uani 0.5 1 d G U P A -1
C77 C 0.33550(12) 0.0729(2) 0.48569(12) 0.097(5) Uani 0.5 1 d G U P A -1
C78 C 0.33532(13) 0.14707(19) 0.45528(16) 0.083(4) Uani 0.5 1 d G U P A -1
C79 C 0.36818(13) 0.16796(19) 0.39546(18) 0.076(4) Uani 0.5 1 d G U P A -1
C80 C 0.33768(14) 0.21146(17) 0.3401(2) 0.072(4) Uani 0.5 1 d G U P A -1
C81 C 0.36893(12) 0.17922(19) 0.26928(19) 0.048(3) Uani 0.5 1 d G U P A -1
C82 C 0.40302(9) 0.1191(2) 0.28163(17) 0.056(3) Uani 0.5 1 d G U P A -1
C83 C 0.41191(8) 0.0593(2) 0.22263(16) 0.072(4) Uani 0.5 1 d G U P A -1
C84 C 0.42334(6) -0.0086(2) 0.26214(16) 0.075(3) Uani 0.5 1 d G U P A -1
C85 C 0.42060(6) -0.0156(2) 0.33767(16) 0.072(3) Uani 0.5 1 d G U P A -1
C86 C 0.40158(7) -0.0886(2) 0.34593(16) 0.079(4) Uani 0.5 1 d G U P A -1
C87 C 0.40243(8) 0.0366(2) 0.39078(15) 0.070(3) Uani 0.5 1 d G U P A -1
C88 C 0.40361(10) 0.1136(2) 0.36376(17) 0.067(3) Uani 0.5 1 d G U P A -1
Ni1A Ni 0.03232(2) 0.0000 0.08542(3) 0.02034(17) Uani 1 2 d S T P B 2
C1A C -0.10188(17) -0.0894(2) 0.3150(2) 0.0359(9) Uani 1 1 d . . . B 2
H1AA H -0.1182 -0.1293 0.2872 0.043 Uiso 1 1 calc R U . B 2
H1AB H -0.1317 -0.0637 0.3391 0.043 Uiso 1 1 calc R U . B 2
N2A N 0.08369(17) 0.0000 0.0035(2) 0.0227(9) Uani 1 2 d S T P B 2
C2A C -0.07403(15) -0.0373(2) 0.2640(2) 0.0289(8) Uani 1 1 d . . . B 2
N3A N 0.03385(11) -0.10789(17) 0.08657(16) 0.0222(6) Uani 1 1 d . . . B 2
C3A C -0.02784(14) -0.1323(2) 0.1882(2) 0.0253(8) Uani 1 1 d . . . B 2
H3A H -0.0446 -0.1686 0.2159 0.030 Uiso 1 1 calc R U . B 2
C4A C 0.00672(14) -0.1543(2) 0.13346(19) 0.0237(7) Uani 1 1 d . . . B 2
N4A N -0.01764(17) 0.0000 0.1687(2) 0.0229(9) Uani 1 2 d S T P B 2
C5A C 0.01919(15) -0.2304(2) 0.1180(2) 0.0268(8) Uani 1 1 d . . . B 2
C6A C -0.00130(17) -0.2948(2) 0.1607(2) 0.0325(9) Uani 1 1 d . . . B 2
H6AA H 0.0000 -0.3385 0.1306 0.039 Uiso 1 1 calc R U . B 2
H6AB H -0.0397 -0.2864 0.1737 0.039 Uiso 1 1 calc R U . B 2
C7A C 0.0326(2) -0.3083(3) 0.2293(3) 0.0517(12) Uani 1 1 d . . . B 2
H7AA H 0.0702 -0.3194 0.2167 0.078 Uiso 1 1 calc R U . B 2
H7AB H 0.0171 -0.3489 0.2554 0.078 Uiso 1 1 calc R U . B 2
H7AC H 0.0319 -0.2651 0.2591 0.078 Uiso 1 1 calc R U . B 2
C8A C 0.05348(15) -0.2304(2) 0.0600(2) 0.0261(8) Uani 1 1 d . . . B 2
C9A C 0.07940(17) -0.2947(2) 0.0230(2) 0.0327(9) Uani 1 1 d . . . B 2
H9AA H 0.0810 -0.2850 -0.0285 0.039 Uiso 1 1 calc R U . B 2
H9AB H 0.0562 -0.3377 0.0299 0.039 Uiso 1 1 calc R U . B 2
C10A C 0.1376(2) -0.3111(3) 0.0511(3) 0.0554(14) Uani 1 1 d . . . B 2
H10A H 0.1512 -0.3551 0.0286 0.083 Uiso 1 1 calc R U . B 2
H10B H 0.1365 -0.3180 0.1025 0.083 Uiso 1 1 calc R U . B 2
H10C H 0.1616 -0.2708 0.0399 0.083 Uiso 1 1 calc R U . B 2
C11A C 0.06232(14) -0.1541(2) 0.04173(19) 0.0223(7) Uani 1 1 d . . . B 2
C12A C 0.09574(14) -0.1317(2) -0.01412(19) 0.0246(7) Uani 1 1 d . . . B 2
H12A H 0.1122 -0.1679 -0.0423 0.030 Uiso 1 1 calc R U . B 2
C13A C 0.10645(14) -0.0598(2) -0.03101(18) 0.0218(7) Uani 1 1 d . . . B 2
C14A C 0.14376(14) -0.0374(2) -0.08740(19) 0.0254(7) Uani 1 1 d . . . B 2
C15A C -0.03914(14) -0.0599(2) 0.20467(19) 0.0236(7) Uani 1 1 d . . . B 2
C16A C 0.17690(16) -0.0887(2) -0.1336(2) 0.0298(8) Uani 1 1 d . . . B 2
H16A H 0.1859 -0.0642 -0.1786 0.036 Uiso 1 1 calc R U . B 2
H16B H 0.1544 -0.1314 -0.1453 0.036 Uiso 1 1 calc R U . B 2
C17A C 0.23068(19) -0.1143(3) -0.0969(3) 0.0484(12) Uani 1 1 d . . . B 2
H17A H 0.2506 -0.1459 -0.1291 0.073 Uiso 1 1 calc R U . B 2
H17B H 0.2220 -0.1406 -0.0535 0.073 Uiso 1 1 calc R U . B 2
H17C H 0.2531 -0.0723 -0.0852 0.073 Uiso 1 1 calc R U . B 2
C18A C -0.0630(2) -0.1218(3) 0.3719(2) 0.0474(11) Uani 1 1 d . . . B 2
H18A H -0.0336 -0.1480 0.3485 0.071 Uiso 1 1 calc R U . B 2
H18B H -0.0833 -0.1549 0.4022 0.071 Uiso 1 1 calc R U . B 2
H18C H -0.0476 -0.0829 0.4008 0.071 Uiso 1 1 calc R U . B 2
C1B C 0.2673(5) 0.0000 0.7052(5) 0.081(3) Uani 1 2 d DS T P C 3
H1B H 0.2291 0.0000 0.7122 0.098 Uiso 1 2 calc R U P C 3
C2B C 0.2941(4) 0.0642(4) 0.7002(4) 0.094(2) Uani 1 1 d D . . C 3
H2B H 0.2748 0.1081 0.7058 0.113 Uiso 1 1 calc R U . C 3
C3B C 0.3498(4) 0.0651(5) 0.6870(5) 0.117(3) Uani 1 1 d D . . C 3
H3B H 0.3680 0.1099 0.6825 0.140 Uiso 1 1 calc R U . C 3
C4B C 0.3797(6) 0.0000 0.6801(8) 0.135(6) Uani 1 2 d DS T P C 3
H4B H 0.4176 0.0000 0.6715 0.162 Uiso 1 2 calc R U P C 3
C3C C 0.4805(3) 0.1147(6) 0.5315(6) 0.126(4) Uani 1 1 d . . . D 4
H3C H 0.4690 0.0707 0.5521 0.151 Uiso 1 1 calc R U . D 4
C4C C 0.4815(3) 0.2365(6) 0.5288(6) 0.117(4) Uani 1 1 d . . . D 4
H4C H 0.4703 0.2819 0.5467 0.141 Uiso 1 1 calc R U . D 4
C2C C 0.4623(3) 0.1806(6) 0.5581(4) 0.081(2) Uani 1 1 d . . . D 4
H2C H 0.4370 0.1834 0.5957 0.097 Uiso 1 1 calc R U . D 4


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu4 1.199(6) 6 ?
Lu1 Lu4 1.199(6) . ?
Lu1 Lu13 1.473(16) 6 ?
Lu1 Lu13 1.473(16) . ?
Lu1 Lu9 2.07(2) . ?
Lu1 Lu6 2.147(7) . ?
Lu1 Lu6 2.147(7) 6 ?
Lu1 C3 2.3104(17) . ?
Lu1 C2 2.402(2) . ?
Lu1 Lu15 2.45(2) 6 ?
Lu1 Lu15 2.45(2) . ?
Lu1 C15 2.452(2) . ?
Lu2 Lu5 0.829(7) . ?
Lu2 Lu14 1.70(3) . ?
Lu2 Lu7 1.721(4) . ?
Lu2 Lu15 1.85(2) . ?
Lu2 Lu8 2.140(7) . ?
Lu2 C79 2.291(2) . ?
Lu2 C78 2.332(2) . ?
Lu2 C80 2.390(3) . ?
Lu2 C88 2.503(2) . ?
Lu2 Lu11 2.525(17) 6 ?
Lu2 C77 2.630(2) . ?
Lu2 C59 2.654(3) . ?
Lu3 Lu12 0.779(13) . ?
Lu3 Lu3 0.874(11) 6 ?
Lu3 Lu16 1.03(3) . ?
Lu3 Lu10 1.04(2) . ?
Lu3 Lu16 1.52(3) 6 ?
Lu3 Lu12 1.542(17) 6 ?
Lu3 Lu11 1.88(3) . ?
Lu3 Lu14 2.04(3) 6 ?
Lu3 C22 2.103(5) . ?
Lu3 C45 2.218(5) . ?
Lu3 C23 2.266(5) . ?
Lu3 C46 2.268(6) . ?
Lu4 Lu13 1.204(15) 6 ?
Lu4 Lu6 1.363(9) . ?
Lu4 Lu15 2.05(3) . ?
Lu4 Lu13 2.115(15) . ?
Lu4 Lu9 2.146(18) . ?
Lu4 C16 2.168(4) . ?
Lu4 C17 2.279(5) . ?
Lu4 Lu5 2.292(9) . ?
Lu4 Lu11 2.32(2) 6 ?
Lu4 Lu4 2.319(12) 6 ?
Lu4 C15 2.393(4) . ?
Lu5 Lu15 1.17(2) . ?
Lu5 Lu7 1.823(11) . ?
Lu5 Lu13 1.982(15) 6 ?
Lu5 Lu9 2.063(14) . ?
Lu5 C59 2.235(6) . ?
Lu5 Lu14 2.25(3) . ?
Lu5 C78 2.308(6) . ?
Lu5 Lu6 2.420(10) . ?
Lu5 C60 2.422(8) . ?
Lu5 C77 2.494(8) . ?
Lu6 Lu11 1.04(2) 6 ?
Lu6 Lu16 1.66(3) 6 ?
Lu6 C19 2.173(6) . ?
Lu6 C18 2.227(6) . ?
Lu6 C40 2.309(6) . ?
Lu6 Lu13 2.376(15) 6 ?
Lu6 C38 2.380(7) . ?
Lu6 Lu14 2.41(2) . ?
Lu6 C17 2.456(7) . ?
Lu7 Lu15 1.70(3) . ?
Lu7 Lu15 1.70(3) 6 ?
Lu7 Lu2 1.721(4) 6 ?
Lu7 Lu8 1.740(19) . ?
Lu7 Lu5 1.823(11) 6 ?
Lu7 C76 1.935(10) . ?
Lu7 Lu9 1.97(3) . ?
Lu7 C75 2.021(8) . ?
Lu7 C87 2.348(12) . ?
Lu7 C77 2.446(10) . ?
Lu8 Lu10 2.03(2) . ?
Lu8 C84 2.130(8) . ?
Lu8 Lu2 2.140(7) 6 ?
Lu8 C85 2.140(9) . ?
Lu8 Lu14 2.14(3) . ?
Lu8 Lu14 2.14(3) 6 ?
Lu8 C86 2.403(7) . ?
Lu8 C69 2.425(8) . ?
Lu8 C87 2.437(11) . ?
Lu8 Lu12 2.447(16) 6 ?
Lu9 Lu15 0.94(2) . ?
Lu9 Lu15 0.94(2) 6 ?
Lu9 Lu13 1.024(18) . ?
Lu9 Lu13 1.024(18) 6 ?
Lu9 C56 1.896(16) . ?
Lu9 C33 1.989(16) . ?
Lu9 Lu5 2.063(14) 6 ?
Lu9 Lu4 2.146(18) 6 ?
Lu10 Lu3 1.04(2) 6 ?
Lu10 Lu12 1.138(19) 6 ?
Lu10 Lu12 1.138(19) . ?
Lu10 Lu16 1.91(4) . ?
Lu10 Lu16 1.91(4) 6 ?
Lu10 Lu14 2.06(3) 6 ?
Lu10 Lu14 2.06(3) . ?
Lu10 C44 2.205(15) . ?
Lu10 C67 2.29(2) . ?
Lu10 C45 2.355(17) . ?
Lu11 Lu6 1.04(2) 6 ?
Lu11 Lu16 1.21(3) . ?
Lu11 Lu12 1.57(3) . ?
Lu11 Lu14 1.60(4) 6 ?
Lu11 C26 2.240(17) . ?
Lu11 C6 2.285(18) . ?
Lu11 Lu4 2.32(2) 6 ?
Lu11 C25 2.430(18) . ?
Lu11 Lu2 2.525(17) 6 ?
Lu11 Lu5 2.556(18) 6 ?
Lu11 C27 2.57(2) . ?
Lu12 Lu16 1.28(3) . ?
Lu12 Lu14 1.31(3) 6 ?
Lu12 Lu3 1.542(17) 6 ?
Lu12 Lu12 2.02(3) 6 ?
Lu12 Lu16 2.14(3) 6 ?
Lu12 C46 2.160(10) . ?
Lu12 C47 2.290(11) . ?
Lu12 C24 2.436(11) . ?
Lu13 Lu15 1.17(2) 6 ?
Lu13 Lu4 1.205(15) 6 ?
Lu13 Lu13 1.30(3) 6 ?
Lu13 Lu15 1.86(2) . ?
Lu13 Lu5 1.982(15) 6 ?
Lu13 C32 2.032(9) . ?
Lu13 C33 2.206(12) . ?
Lu13 C13 2.298(11) . ?
Lu13 C31 2.309(12) . ?
Lu14 Lu12 1.31(3) 6 ?
Lu14 Lu11 1.60(4) 6 ?
Lu14 Lu3 2.04(3) 6 ?
Lu14 Lu16 2.10(4) 6 ?
Lu14 C64 2.198(17) . ?
Lu14 C81 2.33(2) . ?
Lu14 C63 2.45(2) . ?
Lu15 Lu13 1.17(2) 6 ?
Lu15 Lu15 1.62(5) 6 ?
Lu15 C57 2.063(19) . ?
Lu15 C58 2.180(17) . ?
Lu15 C56 2.20(2) . ?
Lu15 C77 2.42(2) . ?
Lu16 Lu16 1.45(6) 6 ?
Lu16 Lu3 1.52(3) 6 ?
Lu16 Lu6 1.66(3) 6 ?
Lu16 C7 2.10(2) . ?
Lu16 Lu14 2.10(4) 6 ?
Lu16 Lu12 2.14(3) 6 ?
Lu16 C23 2.335(18) . ?
Lu16 C20 2.42(3) . ?
C1 C9 1.2267 . ?
C1 C5 1.5282 . ?
C1 C2 1.5456 . ?
C2 C3 1.3939 . ?
C2 C12 1.4267 . ?
C3 C15 1.3293 . ?
C3 C4 1.4879 . ?
C4 C5 1.3001 . ?
C4 C18 1.5289 . ?
C4 C17 1.9751 . ?
C5 C20 1.4038 . ?
C6 C26 1.2956 . ?
C6 C7 1.5044 . ?
C6 C9 1.5838 . ?
C7 C20 1.1761 . ?
C7 C23 1.4967 . ?
C8 C21 1.3490 . ?
C8 C19 1.5592 . ?
C8 C20 1.6498 . ?
C9 C10 1.5506 . ?
C10 C11 1.3615 . ?
C10 C28 1.4621 . ?
C11 C30 1.3848 . ?
C11 C12 1.4894 . ?
C12 C13 1.4341 . ?
C13 C32 1.4435 . ?
C13 C14 1.6136 . ?
C14 C15 1.2834 . ?
C14 C34 1.3776 . ?
C15 C16 1.2782 . ?
C16 C17 1.3346 . ?
C16 C36 1.4550 . ?
C17 C18 1.3954 . ?
C17 C38 1.4083 . ?
C18 C19 1.3643 . ?
C19 C40 1.3425 . ?
C21 C22 1.3433 . ?
C21 C42 1.5219 . ?
C22 C45 1.4138 . ?
C22 C23 1.5100 . ?
C23 C24 1.5176 . ?
C24 C25 1.1245 . ?
C24 C46 1.4365 . ?
C25 C49 1.3670 . ?
C25 C26 1.4438 . ?
C26 C27 1.4394 . ?
C27 C50 1.3570 . ?
C27 C28 1.5050 . ?
C28 C29 1.2426 . ?
C29 C52 1.3096 . ?
C29 C30 1.5867 . ?
C30 C31 1.5013 . ?
C31 C54 1.3306 . ?
C31 C32 1.4362 . ?
C32 C33 1.2849 . ?
C33 C56 1.4076 . ?
C33 C34 1.4179 . ?
C34 C35 1.5226 . ?
C35 C36 1.1497 . ?
C35 C58 1.4606 . ?
C36 C37 1.4798 . ?
C37 C60 1.3843 . ?
C37 C38 1.7092 . ?
C38 C39 1.5343 . ?
C39 C40 1.2694 . ?
C39 C62 1.4837 . ?
C40 C41 1.6577 . ?
C41 C63 1.5107 . ?
C41 C42 1.5422 . ?
C42 C43 1.4703 . ?
C43 C65 1.5280 . ?
C43 C44 1.5570 . ?
C44 C67 1.3789 . ?
C44 C45 1.4592 . ?
C45 C46 1.1615 . ?
C46 C47 1.4620 . ?
C47 C48 1.2536 . ?
C47 C68 1.5555 . ?
C48 C49 1.3324 . ?
C48 C71 1.4675 . ?
C49 C50 1.4724 . ?
C50 C51 1.3271 . ?
C51 C72 1.4224 . ?
C51 C52 1.5203 . ?
C52 C53 1.4462 . ?
C53 C73 1.4000 . ?
C53 C54 1.5185 . ?
C54 C55 1.4101 . ?
C55 C75 1.4547 . ?
C55 C56 1.4832 . ?
C56 C57 1.3118 . ?
C57 C77 1.3751 . ?
C57 C58 1.4355 . ?
C58 C59 1.6639 . ?
C59 C60 1.3992 . ?
C59 C78 1.4213 . ?
C60 C61 1.5975 . ?
C61 C80 1.3053 . ?
C61 C62 1.3384 . ?
C62 C63 1.5617 . ?
C63 C64 1.4237 . ?
C64 C65 1.4383 . ?
C64 C81 1.4625 . ?
C65 C66 1.3257 . ?
C66 C83 1.2592 . ?
C66 C67 1.4246 . ?
C67 C68 1.4649 . ?
C68 C69 1.5951 . ?
C69 C84 1.3160 . ?
C69 C70 1.4150 . ?
C70 C71 1.4558 . ?
C70 C86 1.5121 . ?
C70 C72 1.9753 . ?
C71 C72 1.2411 . ?
C72 C73 1.4783 . ?
C73 C74 1.4670 . ?
C74 C86 1.3792 . ?
C74 C75 1.4306 . ?
C75 C76 1.5401 . ?
C76 C87 1.3940 . ?
C76 C77 1.4706 . ?
C77 C78 1.4624 . ?
C78 C79 1.4183 . ?
C79 C88 1.4353 . ?
C79 C80 1.4839 . ?
C80 C81 1.6266 . ?
C81 C82 1.3854 . ?
C82 C88 1.5226 . ?
C82 C83 1.5570 . ?
C83 C84 1.4606 . ?
C84 C85 1.4050 . ?
C85 C86 1.4140 . ?
C85 C87 1.4371 . ?
C87 C88 1.4868 . ?
Ni1A N3A 1.963(3) . ?
Ni1A N3A 1.963(3) 6 ?
Ni1A N4A 1.963(4) . ?
Ni1A N2A 1.965(4) . ?
C1A C2A 1.500(5) . ?
C1A C18A 1.522(6) . ?
N2A C13A 1.377(4) . ?
N2A C13A 1.377(4) 6 ?
C2A C2A 1.355(8) 6 ?
C2A C15A 1.448(5) . ?
N3A C11A 1.369(5) . ?
N3A C4A 1.380(5) . ?
C3A C4A 1.377(5) . ?
C3A C15A 1.379(5) . ?
C4A C5A 1.445(5) . ?
N4A C15A 1.381(4) 6 ?
N4A C15A 1.381(4) . ?
C5A C8A 1.360(5) . ?
C5A C6A 1.499(5) . ?
C6A C7A 1.525(6) . ?
C8A C11A 1.445(5) . ?
C8A C9A 1.496(5) . ?
C9A C10A 1.522(6) . ?
C11A C12A 1.377(5) . ?
C12A C13A 1.371(5) . ?
C13A C14A 1.442(5) . ?
C14A C14A 1.360(8) 6 ?
C14A C16A 1.501(5) . ?
C16A C17A 1.531(6) . ?
C1B C2B 1.338(8) . ?
C1B C2B 1.338(8) 6 ?
C2B C3B 1.368(11) . ?
C3B C4B 1.393(11) . ?
C4B C3B 1.393(11) 6 ?
C3C C2C 1.371(12) . ?
C3C C3C 1.50(2) 2_656 ?
C4C C2C 1.243(12) . ?
C4C C4C 1.39(2) 2_656 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu4 Lu1 Lu4 150.5(4) 6 . ?
Lu4 Lu1 Lu13 104.2(6) 6 6 ?
Lu4 Lu1 Lu13 52.4(6) . 6 ?
Lu4 Lu1 Lu13 52.4(6) 6 . ?
Lu4 Lu1 Lu13 104.2(6) . . ?
Lu13 Lu1 Lu13 52.5(11) 6 . ?
Lu4 Lu1 Lu9 77.0(3) 6 . ?
Lu4 Lu1 Lu9 77.0(3) . . ?
Lu13 Lu1 Lu9 27.6(5) 6 . ?
Lu13 Lu1 Lu9 27.6(5) . . ?
Lu4 Lu1 Lu6 135.4(3) 6 . ?
Lu4 Lu1 Lu6 35.5(3) . . ?
Lu13 Lu1 Lu6 79.6(5) 6 . ?
Lu13 Lu1 Lu6 121.2(5) . . ?
Lu9 Lu1 Lu6 95.6(4) . . ?
Lu4 Lu1 Lu6 35.5(3) 6 6 ?
Lu4 Lu1 Lu6 135.4(3) . 6 ?
Lu13 Lu1 Lu6 121.2(5) 6 6 ?
Lu13 Lu1 Lu6 79.6(5) . 6 ?
Lu9 Lu1 Lu6 95.6(4) . 6 ?
Lu6 Lu1 Lu6 104.2(4) . 6 ?
Lu4 Lu1 C3 118.1(2) 6 . ?
Lu4 Lu1 C3 90.0(2) . . ?
Lu13 Lu1 C3 113.7(4) 6 . ?
Lu13 Lu1 C3 128.1(4) . . ?
Lu9 Lu1 C3 133.0(5) . . ?
Lu6 Lu1 C3 99.22(18) . . ?
Lu6 Lu1 C3 122.96(18) 6 . ?
Lu4 Lu1 C2 85.4(2) 6 . ?
Lu4 Lu1 C2 123.7(2) . . ?
Lu13 Lu1 C2 137.8(4) 6 . ?
Lu13 Lu1 C2 116.7(5) . . ?
Lu9 Lu1 C2 139.3(5) . . ?
Lu6 Lu1 C2 121.80(18) . . ?
Lu6 Lu1 C2 90.50(17) 6 . ?
C3 Lu1 C2 34.3 . . ?
Lu4 Lu1 Lu15 56.7(7) 6 6 ?
Lu4 Lu1 Lu15 95.2(7) . 6 ?
Lu13 Lu1 Lu15 49.3(7) 6 6 ?
Lu13 Lu1 Lu15 19.2(6) . 6 ?
Lu9 Lu1 Lu15 22.0(6) . 6 ?
Lu6 Lu1 Lu15 104.2(6) . 6 ?
Lu6 Lu1 Lu15 74.0(6) 6 6 ?
C3 Lu1 Lu15 146.4(5) . 6 ?
C2 Lu1 Lu15 133.9(6) . 6 ?
Lu4 Lu1 Lu15 95.2(7) 6 . ?
Lu4 Lu1 Lu15 56.7(7) . . ?
Lu13 Lu1 Lu15 19.2(6) 6 . ?
Lu13 Lu1 Lu15 49.3(7) . . ?
Lu9 Lu1 Lu15 22.0(6) . . ?
Lu6 Lu1 Lu15 74.0(6) . . ?
Lu6 Lu1 Lu15 104.2(6) 6 . ?
C3 Lu1 Lu15 132.2(5) . . ?
C2 Lu1 Lu15 155.5(5) . . ?
Lu15 Lu1 Lu15 38.6(13) 6 . ?
Lu4 Lu1 C15 126.2(2) 6 . ?
Lu4 Lu1 C15 72.9(2) . . ?
Lu13 Lu1 C15 81.8(4) 6 . ?
Lu13 Lu1 C15 105.2(4) . . ?
Lu9 Lu1 C15 101.6(5) . . ?
Lu6 Lu1 C15 98.3(2) . . ?
Lu6 Lu1 C15 150.10(18) 6 . ?
C3 Lu1 C15 32.2 . . ?
C2 Lu1 C15 60.7 . . ?
Lu15 Lu1 C15 119.2(5) 6 . ?
Lu15 Lu1 C15 100.7(5) . . ?
Lu5 Lu2 Lu14 121.4(10) . . ?
Lu5 Lu2 Lu7 83.4(8) . . ?
Lu14 Lu2 Lu7 112.5(8) . . ?
Lu5 Lu2 Lu15 26.6(10) . . ?
Lu14 Lu2 Lu15 127.6(10) . . ?
Lu7 Lu2 Lu15 56.8(10) . . ?
Lu5 Lu2 Lu8 128.2(5) . . ?
Lu14 Lu2 Lu8 66.5(9) . . ?
Lu7 Lu2 Lu8 52.2(6) . . ?
Lu15 Lu2 Lu8 104.1(8) . . ?
Lu5 Lu2 C79 111.1(4) . . ?
Lu14 Lu2 C79 111.6(7) . . ?
Lu7 Lu2 C79 114.0(3) . . ?
Lu15 Lu2 C79 119.3(6) . . ?
Lu8 Lu2 C79 110.9(2) . . ?
Lu5 Lu2 C78 78.1(4) . . ?
Lu14 Lu2 C78 144.8(7) . . ?
Lu7 Lu2 C78 97.8(4) . . ?
Lu15 Lu2 C78 83.7(6) . . ?
Lu8 Lu2 C78 127.2(3) . . ?
C79 Lu2 C78 35.7 . . ?
Lu5 Lu2 C80 111.0(5) . . ?
Lu14 Lu2 C80 83.0(7) . . ?
Lu7 Lu2 C80 150.1(4) . . ?
Lu15 Lu2 C80 133.9(7) . . ?
Lu8 Lu2 C80 120.8(2) . . ?
C79 Lu2 C80 36.9 . . ?
C78 Lu2 C80 61.98(6) . . ?
Lu5 Lu2 C88 137.6(5) . . ?
Lu14 Lu2 C88 99.3(8) . . ?
Lu7 Lu2 C88 92.0(4) . . ?
Lu15 Lu2 C88 129.8(8) . . ?
Lu8 Lu2 C88 76.4(2) . . ?
C79 Lu2 C88 34.5 . . ?
C78 Lu2 C88 60.7 . . ?
C80 Lu2 C88 59.36(5) . . ?
Lu5 Lu2 Lu11 82.8(8) . 6 ?
Lu14 Lu2 Lu11 38.7(10) . 6 ?
Lu7 Lu2 Lu11 111.4(6) . 6 ?
Lu15 Lu2 Lu11 93.2(9) . 6 ?
Lu8 Lu2 Lu11 89.6(6) . 6 ?
C79 Lu2 Lu11 133.6(5) . 6 ?
C78 Lu2 Lu11 142.8(6) . 6 ?
C80 Lu2 Lu11 96.7(5) . 6 ?
C88 Lu2 Lu11 136.7(5) . 6 ?
Lu5 Lu2 C77 71.4(5) . . ?
Lu14 Lu2 C77 167.0(9) . . ?
Lu7 Lu2 C77 64.5(4) . . ?
Lu15 Lu2 C77 62.6(7) . . ?
Lu8 Lu2 C77 104.5(3) . . ?
C79 Lu2 C77 61.53(5) . . ?
C78 Lu2 C77 33.6 . . ?
C80 Lu2 C77 94.47(8) . . ?
C88 Lu2 C77 68.68(5) . . ?
Lu11 Lu2 C77 154.1(6) 6 . ?
Lu5 Lu2 C59 51.5(4) . . ?
Lu14 Lu2 C59 137.0(8) . . ?
Lu7 Lu2 C59 108.6(5) . . ?
Lu15 Lu2 C59 67.7(6) . . ?
Lu8 Lu2 C59 155.8(3) . . ?
C79 Lu2 C59 59.94(6) . . ?
C78 Lu2 C59 32.3 . . ?
C80 Lu2 C59 66.97(7) . . ?
C88 Lu2 C59 91.33(7) . . ?
Lu11 Lu2 C59 113.1(6) 6 . ?
C77 Lu2 C59 51.3 . . ?
Lu12 Lu3 Lu3 137.6(12) . 6 ?
Lu12 Lu3 Lu16 89(2) . . ?
Lu3 Lu3 Lu16 106.3(17) 6 . ?
Lu12 Lu3 Lu10 75.8(14) . . ?
Lu3 Lu3 Lu10 65.2(7) 6 . ?
Lu16 Lu3 Lu10 134.7(15) . . ?
Lu12 Lu3 Lu16 133.8(12) . 6 ?
Lu3 Lu3 Lu16 40.3(10) 6 6 ?
Lu16 Lu3 Lu16 66(3) . 6 ?
Lu10 Lu3 Lu16 94.3(13) . 6 ?
Lu12 Lu3 Lu12 117.7(17) . 6 ?
Lu3 Lu3 Lu12 19.9(5) 6 6 ?
Lu16 Lu3 Lu12 111.1(17) . 6 ?
Lu10 Lu3 Lu12 47.6(9) . 6 ?
Lu16 Lu3 Lu12 49.3(12) 6 6 ?
Lu12 Lu3 Lu11 54.7(14) . . ?
Lu3 Lu3 Lu11 137.4(6) 6 . ?
Lu16 Lu3 Lu11 35.8(18) . . ?
Lu10 Lu3 Lu11 121.8(11) . . ?
Lu16 Lu3 Lu11 98.9(11) 6 . ?
Lu12 Lu3 Lu11 132.4(8) 6 . ?
Lu12 Lu3 Lu14 15.0(10) . 6 ?
Lu3 Lu3 Lu14 130.0(8) 6 6 ?
Lu16 Lu3 Lu14 79.0(18) . 6 ?
Lu10 Lu3 Lu14 76.2(11) . 6 ?
Lu16 Lu3 Lu14 118.9(9) 6 6 ?
Lu12 Lu3 Lu14 110.9(9) 6 6 ?
Lu11 Lu3 Lu14 47.9(10) . 6 ?
Lu12 Lu3 C22 129.9(10) . . ?
Lu3 Lu3 C22 82.60(19) 6 . ?
Lu16 Lu3 C22 109.3(13) . . ?
Lu10 Lu3 C22 113.1(10) . . ?
Lu16 Lu3 C22 95.7(8) 6 . ?
Lu12 Lu3 C22 98.9(4) 6 . ?
Lu11 Lu3 C22 121.5(5) . . ?
Lu14 Lu3 C22 143.9(7) 6 . ?
Lu12 Lu3 C45 100.3(11) . . ?
Lu3 Lu3 C45 92.12(18) 6 . ?
Lu16 Lu3 C45 140.8(11) . . ?
Lu10 Lu3 C45 84.3(9) . . ?
Lu16 Lu3 C45 123.9(8) 6 . ?
Lu12 Lu3 C45 98.0(5) 6 . ?
Lu11 Lu3 C45 129.1(6) . . ?
Lu14 Lu3 C45 115.1(7) 6 . ?
C22 Lu3 C45 38.08(9) . . ?
Lu12 Lu3 C23 103.2(11) . . ?
Lu3 Lu3 C23 117.96(17) 6 . ?
Lu16 Lu3 C23 80.9(11) . . ?
Lu10 Lu3 C23 143.8(9) . . ?
Lu16 Lu3 C23 109.8(10) 6 . ?
Lu12 Lu3 C23 137.0(4) 6 . ?
Lu11 Lu3 C23 81.8(5) . . ?
Lu14 Lu3 C23 112.0(8) 6 . ?
C22 Lu3 C23 40.22(8) . . ?
C45 Lu3 C23 59.96(12) . . ?
Lu12 Lu3 C46 72.1(10) . . ?
Lu3 Lu3 C46 119.98(17) 6 . ?
Lu16 Lu3 C46 128.6(15) . . ?
Lu10 Lu3 C46 87.4(8) . . ?
Lu16 Lu3 C46 153.6(7) 6 . ?
Lu12 Lu3 C46 120.1(7) 6 . ?
Lu11 Lu3 C46 102.6(7) . . ?
Lu14 Lu3 C46 87.1(6) 6 . ?
C22 Lu3 C46 59.79(14) . . ?
C45 Lu3 C46 29.99(8) . . ?
C23 Lu3 C46 59.03(13) . . ?
Lu1 Lu4 Lu13 75.6(7) . 6 ?
Lu1 Lu4 Lu6 113.7(6) . . ?
Lu13 Lu4 Lu6 135.3(7) 6 . ?
Lu1 Lu4 Lu15 94.1(8) . . ?
Lu13 Lu4 Lu15 29.4(8) 6 . ?
Lu6 Lu4 Lu15 107.0(7) . . ?
Lu1 Lu4 Lu13 42.5(5) . . ?
Lu13 Lu4 Lu13 34.0(8) 6 . ?
Lu6 Lu4 Lu13 130.3(4) . . ?
Lu15 Lu4 Lu13 53.1(7) . . ?
Lu1 Lu4 Lu9 70.0(4) . . ?
Lu13 Lu4 Lu9 14.4(6) 6 . ?
Lu6 Lu4 Lu9 124.3(6) . . ?
Lu15 Lu4 Lu9 25.7(6) . . ?
Lu13 Lu4 Lu9 27.8(4) . . ?
Lu1 Lu4 C16 110.0(3) . . ?
Lu13 Lu4 C16 102.6(5) 6 . ?
Lu6 Lu4 C16 113.1(4) . . ?
Lu15 Lu4 C16 117.6(6) . . ?
Lu13 Lu4 C16 116.3(4) . . ?
Lu9 Lu4 C16 116.8(5) . . ?
Lu1 Lu4 C17 115.7(3) . . ?
Lu13 Lu4 C17 137.2(6) 6 . ?
Lu6 Lu4 C17 80.5(3) . . ?
Lu15 Lu4 C17 143.8(7) . . ?
Lu13 Lu4 C17 144.8(4) . . ?
Lu9 Lu4 C17 151.5(5) . . ?
C16 Lu4 C17 34.81(7) . . ?
Lu1 Lu4 Lu5 116.2(3) . . ?
Lu13 Lu4 Lu5 59.8(7) 6 . ?
Lu6 Lu4 Lu5 78.4(4) . . ?
Lu15 Lu4 Lu5 30.6(7) . . ?
Lu13 Lu4 Lu5 80.5(5) . . ?
Lu9 Lu4 Lu5 55.3(6) . . ?
C16 Lu4 Lu5 121.8(3) . . ?
C17 Lu4 Lu5 128.2(4) . . ?
Lu1 Lu4 Lu11 110.6(7) . 6 ?
Lu13 Lu4 Lu11 122.1(8) 6 6 ?
Lu6 Lu4 Lu11 13.5(5) . 6 ?
Lu15 Lu4 Lu11 94.5(8) . 6 ?
Lu13 Lu4 Lu11 118.6(6) . 6 ?
Lu9 Lu4 Lu11 110.8(7) . 6 ?
C16 Lu4 Lu11 125.1(6) . 6 ?
C17 Lu4 Lu11 93.7(5) . 6 ?
Lu5 Lu4 Lu11 67.4(5) . 6 ?
Lu1 Lu4 Lu4 14.7(2) . 6 ?
Lu13 Lu4 Lu4 65.0(7) 6 6 ?
Lu6 Lu4 Lu4 113.1(4) . 6 ?
Lu15 Lu4 Lu4 80.2(7) . 6 ?
Lu13 Lu4 Lu4 31.1(4) . 6 ?
Lu9 Lu4 Lu4 57.3(4) . 6 ?
C16 Lu4 Lu4 121.17(19) . 6 ?
C17 Lu4 Lu4 130.41(19) . 6 ?
Lu5 Lu4 Lu4 101.4(2) . 6 ?
Lu11 Lu4 Lu4 106.6(6) 6 6 ?
Lu1 Lu4 C15 78.5(2) . . ?
Lu13 Lu4 C15 89.8(6) 6 . ?
Lu6 Lu4 C15 134.5(4) . . ?
Lu15 Lu4 C15 116.0(6) . . ?
Lu13 Lu4 C15 89.3(4) . . ?
Lu9 Lu4 C15 101.2(6) . . ?
C16 Lu4 C15 32.07(6) . . ?
C17 Lu4 C15 56.03(9) . . ?
Lu5 Lu4 C15 137.8(3) . . ?
Lu11 Lu4 C15 147.9(5) 6 . ?
Lu4 Lu4 C15 89.09(17) 6 . ?
Lu2 Lu5 Lu15 134.9(16) . . ?
Lu2 Lu5 Lu7 69.7(7) . . ?
Lu15 Lu5 Lu7 65.2(14) . . ?
Lu2 Lu5 Lu13 146.9(6) . 6 ?
Lu15 Lu5 Lu13 31.9(13) . 6 ?
Lu7 Lu5 Lu13 87.2(7) . 6 ?
Lu2 Lu5 Lu9 129.2(9) . . ?
Lu15 Lu5 Lu9 10.8(10) . . ?
Lu7 Lu5 Lu9 60.7(8) . . ?
Lu13 Lu5 Lu9 29.2(6) 6 . ?
Lu2 Lu5 C59 111.6(5) . . ?
Lu15 Lu5 C59 94.2(10) . . ?
Lu7 Lu5 C59 124.4(5) . . ?
Lu13 Lu5 C59 101.0(4) 6 . ?
Lu9 Lu5 C59 104.9(5) . . ?
Lu2 Lu5 Lu14 40.3(8) . . ?
Lu15 Lu5 Lu14 135.3(11) . . ?
Lu7 Lu5 Lu14 88.0(8) . . ?
Lu13 Lu5 Lu14 118.9(8) 6 . ?
Lu9 Lu5 Lu14 124.5(7) . . ?
C59 Lu5 Lu14 130.3(7) . . ?
Lu2 Lu5 Lu4 132.4(6) . . ?
Lu15 Lu5 Lu4 63.4(12) . . ?
Lu7 Lu5 Lu4 106.0(5) . . ?
Lu13 Lu5 Lu4 31.7(5) 6 . ?
Lu9 Lu5 Lu4 58.8(7) . . ?
C59 Lu5 Lu4 108.9(4) . . ?
Lu14 Lu5 Lu4 93.6(8) . . ?
Lu2 Lu5 C78 81.3(4) . . ?
Lu15 Lu5 C78 103.0(10) . . ?
Lu7 Lu5 C78 95.7(5) . . ?
Lu13 Lu5 C78 125.8(5) 6 . ?
Lu9 Lu5 C78 112.6(6) . . ?
C59 Lu5 C78 36.42(9) . . ?
Lu14 Lu5 C78 115.3(7) . . ?
Lu4 Lu5 C78 144.4(4) . . ?
Lu2 Lu5 Lu6 102.3(6) . . ?
Lu15 Lu5 Lu6 94.9(12) . . ?
Lu7 Lu5 Lu6 113.0(4) . . ?
Lu13 Lu5 Lu6 64.4(5) 6 . ?
Lu9 Lu5 Lu6 88.0(6) . . ?
C59 Lu5 Lu6 120.1(4) . . ?
Lu14 Lu5 Lu6 62.1(8) . . ?
Lu4 Lu5 Lu6 33.5(2) . . ?
C78 Lu5 Lu6 150.6(4) . . ?
Lu2 Lu5 C60 108.4(6) . . ?
Lu15 Lu5 C60 113.3(12) . . ?
Lu7 Lu5 C60 158.2(5) . . ?
Lu13 Lu5 C60 101.7(5) 6 . ?
Lu9 Lu5 C60 121.6(5) . . ?
C59 Lu5 C60 34.67(11) . . ?
Lu14 Lu5 C60 104.4(7) . . ?
Lu4 Lu5 C60 91.2(3) . . ?
C78 Lu5 C60 62.84(15) . . ?
Lu6 Lu5 C60 88.7(4) . . ?
Lu2 Lu5 C77 90.2(6) . . ?
Lu15 Lu5 C77 72.8(12) . . ?
Lu7 Lu5 C77 67.0(4) . . ?
Lu13 Lu5 C77 102.6(5) 6 . ?
Lu9 Lu5 C77 80.6(6) . . ?
C59 Lu5 C77 57.56(15) . . ?
Lu14 Lu5 C77 130.4(8) . . ?
Lu4 Lu5 C77 133.3(4) . . ?
C78 Lu5 C77 35.19(11) . . ?
Lu6 Lu5 C77 166.7(4) . . ?
C60 Lu5 C77 91.54(19) . . ?
Lu11 Lu6 Lu4 148.7(11) 6 . ?
Lu11 Lu6 Lu16 46.4(15) 6 6 ?
Lu4 Lu6 Lu16 120.6(9) . 6 ?
Lu11 Lu6 Lu1 133.3(13) 6 . ?
Lu4 Lu6 Lu1 30.7(3) . . ?
Lu16 Lu6 Lu1 92.1(9) 6 . ?
Lu11 Lu6 C19 82.4(10) 6 . ?
Lu4 Lu6 C19 127.9(4) . . ?
Lu16 Lu6 C19 83.9(8) 6 . ?
Lu1 Lu6 C19 118.9(3) . . ?
Lu11 Lu6 C18 118.3(11) 6 . ?
Lu4 Lu6 C18 92.6(4) . . ?
Lu16 Lu6 C18 110.4(9) 6 . ?
Lu1 Lu6 C18 93.0(3) . . ?
C19 Lu6 C18 36.10(9) . . ?
Lu11 Lu6 C40 69.4(11) 6 . ?
Lu4 Lu6 C40 139.3(5) . . ?
Lu16 Lu6 C40 96.8(8) 6 . ?
Lu1 Lu6 C40 149.9(3) . . ?
C19 Lu6 C40 34.69(9) . . ?
C18 Lu6 C40 56.97(13) . . ?
Lu11 Lu6 Lu13 128.2(11) 6 6 ?
Lu4 Lu6 Lu13 20.9(4) . 6 ?
Lu16 Lu6 Lu13 111.5(8) 6 6 ?
Lu1 Lu6 Lu13 37.6(4) . 6 ?
C19 Lu6 Lu13 148.8(5) . 6 ?
C18 Lu6 Lu13 113.4(5) . 6 ?
C40 Lu6 Lu13 151.4(5) . 6 ?
Lu11 Lu6 C38 117.5(13) 6 . ?
Lu4 Lu6 C38 84.3(4) . . ?
Lu16 Lu6 C38 152.6(8) 6 . ?
Lu1 Lu6 C38 108.9(3) . . ?
C19 Lu6 C38 70.77(15) . . ?
C18 Lu6 C38 52.87(13) . . ?
C40 Lu6 C38 56.34(13) . . ?
Lu13 Lu6 C38 95.7(4) 6 . ?
Lu11 Lu6 Lu14 30.1(12) 6 . ?
Lu4 Lu6 Lu14 120.1(8) . . ?
Lu16 Lu6 Lu14 58.8(12) 6 . ?
Lu1 Lu6 Lu14 117.3(6) . . ?
C19 Lu6 Lu14 111.9(8) . . ?
C18 Lu6 Lu14 147.0(7) . . ?
C40 Lu6 Lu14 91.7(6) . . ?
Lu13 Lu6 Lu14 99.2(8) 6 . ?
C38 Lu6 Lu14 121.0(6) . . ?
Lu11 Lu6 Lu5 85.4(11) 6 . ?
Lu4 Lu6 Lu5 68.1(4) . . ?
Lu16 Lu6 Lu5 100.6(9) 6 . ?
Lu1 Lu6 Lu5 82.5(3) . . ?
C19 Lu6 Lu5 158.1(4) . . ?
C18 Lu6 Lu5 148.9(4) . . ?
C40 Lu6 Lu5 123.6(4) . . ?
Lu13 Lu6 Lu5 48.8(4) 6 . ?
C38 Lu6 Lu5 99.4(4) . . ?
Lu14 Lu6 Lu5 55.5(8) . . ?
Lu11 Lu6 C17 143.8(11) 6 . ?
Lu4 Lu6 C17 66.3(3) . . ?
Lu16 Lu6 C17 142.3(10) 6 . ?
Lu1 Lu6 C17 81.1(3) . . ?
C19 Lu6 C17 67.95(15) . . ?
C18 Lu6 C17 34.23(9) . . ?
C40 Lu6 C17 74.37(15) . . ?
Lu13 Lu6 C17 85.1(4) 6 . ?
C38 Lu6 C17 33.81(9) . . ?
Lu14 Lu6 C17 154.7(7) . . ?
Lu5 Lu6 C17 115.0(4) . . ?
Lu15 Lu7 Lu15 56.8(18) . 6 ?
Lu15 Lu7 Lu2 118.9(10) . 6 ?
Lu15 Lu7 Lu2 65.4(9) 6 6 ?
Lu15 Lu7 Lu2 65.4(9) . . ?
Lu15 Lu7 Lu2 119.0(10) 6 . ?
Lu2 Lu7 Lu2 142.2(7) 6 . ?
Lu15 Lu7 Lu8 132.5(10) . . ?
Lu15 Lu7 Lu8 132.5(10) 6 . ?
Lu2 Lu7 Lu8 76.4(5) 6 . ?
Lu2 Lu7 Lu8 76.4(5) . . ?
Lu15 Lu7 Lu5 93.5(11) . 6 ?
Lu15 Lu7 Lu5 38.6(9) 6 6 ?
Lu2 Lu7 Lu5 26.8(2) 6 6 ?
Lu2 Lu7 Lu5 141.5(6) . 6 ?
Lu8 Lu7 Lu5 100.1(5) . 6 ?
Lu15 Lu7 Lu5 38.6(9) . . ?
Lu15 Lu7 Lu5 93.5(11) 6 . ?
Lu2 Lu7 Lu5 141.5(6) 6 . ?
Lu2 Lu7 Lu5 26.9(2) . . ?
Lu8 Lu7 Lu5 100.1(5) . . ?
Lu5 Lu7 Lu5 124.6(8) 6 . ?
Lu15 Lu7 C76 105.0(9) . . ?
Lu15 Lu7 C76 114.2(10) 6 . ?
Lu2 Lu7 C76 115.4(4) 6 . ?
Lu2 Lu7 C76 97.4(3) . . ?
Lu8 Lu7 C76 107.0(8) . . ?
Lu5 Lu7 C76 119.7(5) 6 . ?
Lu5 Lu7 C76 102.4(4) . . ?
Lu15 Lu7 Lu9 28.4(9) . . ?
Lu15 Lu7 Lu9 28.4(9) 6 . ?
Lu2 Lu7 Lu9 92.1(5) 6 . ?
Lu2 Lu7 Lu9 92.1(5) . . ?
Lu8 Lu7 Lu9 139.7(8) . . ?
Lu5 Lu7 Lu9 65.7(5) 6 . ?
Lu5 Lu7 Lu9 65.7(5) . . ?
C76 Lu7 Lu9 112.8(9) . . ?
Lu15 Lu7 C75 111.3(11) . . ?
Lu15 Lu7 C75 80.0(8) 6 . ?
Lu2 Lu7 C75 74.07(18) 6 . ?
Lu2 Lu7 C75 142.4(5) . . ?
Lu8 Lu7 C75 116.2(7) . . ?
Lu5 Lu7 C75 74.0(3) 6 . ?
Lu5 Lu7 C75 136.3(7) . . ?
C76 Lu7 C75 45.8(2) . . ?
Lu9 Lu7 C75 96.6(7) . . ?
Lu15 Lu7 C87 126.1(8) . . ?
Lu15 Lu7 C87 149.3(9) 6 . ?
Lu2 Lu7 C87 113.2(6) 6 . ?
Lu2 Lu7 C87 81.8(4) . . ?
Lu8 Lu7 C87 71.4(6) . . ?
Lu5 Lu7 C87 134.2(5) 6 . ?
Lu5 Lu7 C87 101.2(3) . . ?
C76 Lu7 C87 36.4(2) . . ?
Lu9 Lu7 C87 145.9(7) . . ?
C75 Lu7 C87 70.7(3) . . ?
Lu15 Lu7 C77 68.7(8) . . ?
Lu15 Lu7 C77 98.8(10) 6 . ?
Lu2 Lu7 C77 141.7(5) 6 . ?
Lu2 Lu7 C77 76.1(2) . . ?
Lu8 Lu7 C77 128.6(6) . . ?
Lu5 Lu7 C77 127.8(7) 6 . ?
Lu5 Lu7 C77 69.7(3) . . ?
C76 Lu7 C77 36.96(17) . . ?
Lu9 Lu7 C77 83.5(7) . . ?
C75 Lu7 C77 68.7(3) . . ?
C87 Lu7 C77 62.4(2) . . ?
Lu7 Lu8 Lu10 123.5(8) . . ?
Lu7 Lu8 C84 130.7(7) . . ?
Lu10 Lu8 C84 105.6(8) . . ?
Lu7 Lu8 Lu2 51.4(3) . . ?
Lu10 Lu8 Lu2 101.3(5) . . ?
C84 Lu8 Lu2 126.7(3) . . ?
Lu7 Lu8 Lu2 51.4(3) . 6 ?
Lu10 Lu8 Lu2 101.3(5) . 6 ?
C84 Lu8 Lu2 119.1(2) . 6 ?
Lu2 Lu8 Lu2 99.1(5) . 6 ?
Lu7 Lu8 C85 92.3(6) . . ?
Lu10 Lu8 C85 143.4(8) . . ?
C84 Lu8 C85 38.43(14) . . ?
Lu2 Lu8 C85 107.6(4) . . ?
Lu2 Lu8 C85 95.8(4) 6 . ?
Lu7 Lu8 Lu14 93.9(8) . . ?
Lu10 Lu8 Lu14 59.2(9) . . ?
C84 Lu8 Lu14 116.4(6) . . ?
Lu2 Lu8 Lu14 47.0(8) . . ?
Lu2 Lu8 Lu14 124.4(6) 6 . ?
C85 Lu8 Lu14 132.0(7) . . ?
Lu7 Lu8 Lu14 93.9(8) . 6 ?
Lu10 Lu8 Lu14 59.2(9) . 6 ?
C84 Lu8 Lu14 109.0(6) . 6 ?
Lu2 Lu8 Lu14 124.4(6) . 6 ?
Lu2 Lu8 Lu14 47.0(8) 6 6 ?
C85 Lu8 Lu14 116.9(7) . 6 ?
Lu14 Lu8 Lu14 110.0(15) . 6 ?
Lu7 Lu8 C86 84.2(5) . . ?
Lu10 Lu8 C86 132.0(4) . . ?
C84 Lu8 C86 57.50(17) . . ?
Lu2 Lu8 C86 125.3(6) . . ?
Lu2 Lu8 C86 63.7(2) 6 . ?
C85 Lu8 C86 35.68(12) . . ?
Lu14 Lu8 C86 167.1(9) . . ?
Lu14 Lu8 C86 82.9(8) 6 . ?
Lu7 Lu8 C69 133.7(5) . . ?
Lu10 Lu8 C69 90.2(7) . . ?
C84 Lu8 C69 32.78(12) . . ?
Lu2 Lu8 C69 159.4(3) . . ?
Lu2 Lu8 C69 95.26(12) 6 . ?
C85 Lu8 C69 55.96(17) . . ?
Lu14 Lu8 C69 132.1(9) . . ?
Lu14 Lu8 C69 76.2(6) 6 . ?
C86 Lu8 C69 50.06(12) . . ?
Lu7 Lu8 C87 66.0(5) . . ?
Lu10 Lu8 C87 162.1(4) . . ?
C84 Lu8 C87 68.2(2) . . ?
Lu2 Lu8 C87 72.2(3) . . ?
Lu2 Lu8 C87 96.3(5) 6 . ?
C85 Lu8 C87 35.86(16) . . ?
Lu14 Lu8 C87 107.5(8) . . ?
Lu14 Lu8 C87 138.4(9) 6 . ?
C86 Lu8 C87 60.1(2) . . ?
C69 Lu8 C87 91.7(3) . . ?
Lu7 Lu8 Lu12 108.6(6) . 6 ?
Lu10 Lu8 Lu12 27.5(5) . 6 ?
C84 Lu8 Lu12 117.7(6) . 6 ?
Lu2 Lu8 Lu12 74.5(4) . 6 ?
Lu2 Lu8 Lu12 111.2(4) 6 6 ?
C85 Lu8 Lu12 152.4(5) . 6 ?
Lu14 Lu8 Lu12 32.2(8) . 6 ?
Lu14 Lu8 Lu12 80.3(10) 6 6 ?
C86 Lu8 Lu12 159.4(6) . 6 ?
C69 Lu8 Lu12 113.8(6) . 6 ?
C87 Lu8 Lu12 139.5(4) . 6 ?
Lu15 Lu9 Lu15 119(4) . 6 ?
Lu15 Lu9 Lu13 143(3) . . ?
Lu15 Lu9 Lu13 72.7(18) 6 . ?
Lu15 Lu9 Lu13 72.7(18) . 6 ?
Lu15 Lu9 Lu13 143(3) 6 6 ?
Lu13 Lu9 Lu13 79(2) . 6 ?
Lu15 Lu9 C56 96(2) . . ?
Lu15 Lu9 C56 86.3(19) 6 . ?
Lu13 Lu9 C56 120.1(11) . . ?
Lu13 Lu9 C56 128.8(12) 6 . ?
Lu15 Lu9 Lu7 60(2) . . ?
Lu15 Lu9 Lu7 60(2) 6 . ?
Lu13 Lu9 Lu7 118.9(13) . . ?
Lu13 Lu9 Lu7 118.9(13) 6 . ?
C56 Lu9 Lu7 93.8(11) . . ?
Lu15 Lu9 C33 118.9(15) . . ?
Lu15 Lu9 C33 102.9(14) 6 . ?
Lu13 Lu9 C33 88.1(13) . . ?
Lu13 Lu9 C33 99.1(15) 6 . ?
C56 Lu9 C33 42.4(3) . . ?
Lu7 Lu9 C33 135.8(12) . . ?
Lu15 Lu9 Lu5 112(2) . 6 ?
Lu15 Lu9 Lu5 13.5(12) 6 6 ?
Lu13 Lu9 Lu5 71.0(10) . 6 ?
Lu13 Lu9 Lu5 132.1(13) 6 6 ?
C56 Lu9 Lu5 98.7(8) . 6 ?
Lu7 Lu9 Lu5 53.6(5) . 6 ?
C33 Lu9 Lu5 115.9(4) . 6 ?
Lu15 Lu9 Lu5 13.5(12) . . ?
Lu15 Lu9 Lu5 112(2) 6 . ?
Lu13 Lu9 Lu5 132.1(13) . . ?
Lu13 Lu9 Lu5 71.0(10) 6 . ?
C56 Lu9 Lu5 107.8(9) . . ?
Lu7 Lu9 Lu5 53.6(5) . . ?
C33 Lu9 Lu5 132.3(5) . . ?
Lu5 Lu9 Lu5 103.0(10) 6 . ?
Lu15 Lu9 Lu1 103(2) . . ?
Lu15 Lu9 Lu1 103(2) 6 . ?
Lu13 Lu9 Lu1 41.8(11) . . ?
Lu13 Lu9 Lu1 41.8(11) 6 . ?
C56 Lu9 Lu1 151.5(12) . . ?
Lu7 Lu9 Lu1 114.1(7) . . ?
C33 Lu9 Lu1 109.2(11) . . ?
Lu5 Lu9 Lu1 93.9(6) 6 . ?
Lu5 Lu9 Lu1 93.9(6) . . ?
Lu15 Lu9 Lu4 72(2) . . ?
Lu15 Lu9 Lu4 128(2) 6 . ?
Lu13 Lu9 Lu4 74.4(14) . . ?
Lu13 Lu9 Lu4 17.0(7) 6 . ?
C56 Lu9 Lu4 145.3(7) . . ?
Lu7 Lu9 Lu4 106.3(6) . . ?
C33 Lu9 Lu4 114.8(11) . . ?
Lu5 Lu9 Lu4 116.0(7) 6 . ?
Lu5 Lu9 Lu4 66.0(4) . . ?
Lu1 Lu9 Lu4 33.0(4) . . ?
Lu15 Lu9 Lu4 128(2) . 6 ?
Lu15 Lu9 Lu4 72(2) 6 6 ?
Lu13 Lu9 Lu4 17.0(7) . 6 ?
Lu13 Lu9 Lu4 74.4(14) 6 6 ?
C56 Lu9 Lu4 135.7(5) . 6 ?
Lu7 Lu9 Lu4 106.3(6) . 6 ?
C33 Lu9 Lu4 104.9(9) . 6 ?
Lu5 Lu9 Lu4 66.0(4) 6 6 ?
Lu5 Lu9 Lu4 116.0(7) . 6 ?
Lu1 Lu9 Lu4 33.0(4) . 6 ?
Lu4 Lu9 Lu4 65.4(7) . 6 ?
Lu3 Lu10 Lu3 49.6(14) . 6 ?
Lu3 Lu10 Lu12 90(2) . 6 ?
Lu3 Lu10 Lu12 41.6(9) 6 6 ?
Lu3 Lu10 Lu12 41.6(9) . . ?
Lu3 Lu10 Lu12 90(2) 6 . ?
Lu12 Lu10 Lu12 126(3) 6 . ?
Lu3 Lu10 Lu16 22.5(8) . . ?
Lu3 Lu10 Lu16 52.7(13) 6 . ?
Lu12 Lu10 Lu16 85.1(18) 6 . ?
Lu12 Lu10 Lu16 40.5(14) . . ?
Lu3 Lu10 Lu16 52.7(13) . 6 ?
Lu3 Lu10 Lu16 22.5(8) 6 6 ?
Lu12 Lu10 Lu16 40.5(14) 6 6 ?
Lu12 Lu10 Lu16 85.1(18) . 6 ?
Lu16 Lu10 Lu16 44.6(19) . 6 ?
Lu3 Lu10 Lu8 126.5(11) . . ?
Lu3 Lu10 Lu8 126.5(11) 6 . ?
Lu12 Lu10 Lu8 97.1(13) 6 . ?
Lu12 Lu10 Lu8 97.1(13) . . ?
Lu16 Lu10 Lu8 105.2(9) . . ?
Lu16 Lu10 Lu8 105.2(9) 6 . ?
Lu3 Lu10 Lu14 74.3(10) . 6 ?
Lu3 Lu10 Lu14 116.3(15) 6 6 ?
Lu12 Lu10 Lu14 133.9(15) 6 6 ?
Lu12 Lu10 Lu14 35.1(13) . 6 ?
Lu16 Lu10 Lu14 63.9(12) . 6 ?
Lu16 Lu10 Lu14 101.8(12) 6 6 ?
Lu8 Lu10 Lu14 63.0(10) . 6 ?
Lu3 Lu10 Lu14 116.3(15) . . ?
Lu3 Lu10 Lu14 74.3(10) 6 . ?
Lu12 Lu10 Lu14 35.1(13) 6 . ?
Lu12 Lu10 Lu14 133.9(15) . . ?
Lu16 Lu10 Lu14 101.8(12) . . ?
Lu16 Lu10 Lu14 63.9(12) 6 . ?
Lu8 Lu10 Lu14 63.0(10) . . ?
Lu14 Lu10 Lu14 116.4(16) 6 . ?
Lu3 Lu10 C44 104.4(13) . . ?
Lu3 Lu10 C44 93.2(10) 6 . ?
Lu12 Lu10 C44 93.0(9) 6 . ?
Lu12 Lu10 C44 117.4(12) . . ?
Lu16 Lu10 C44 126.5(12) . . ?
Lu16 Lu10 C44 114.9(10) 6 . ?
Lu8 Lu10 C44 128.0(12) . . ?
Lu14 Lu10 C44 132.5(8) 6 . ?
Lu14 Lu10 C44 106.7(7) . . ?
Lu3 Lu10 C67 133.3(11) . . ?
Lu3 Lu10 C67 126.8(10) 6 . ?
Lu12 Lu10 C67 109.7(11) 6 . ?
Lu12 Lu10 C67 121.4(11) . . ?
Lu16 Lu10 C67 154.5(9) . . ?
Lu16 Lu10 C67 145.5(9) 6 . ?
Lu8 Lu10 C67 93.7(10) . . ?
Lu14 Lu10 C67 112.5(10) 6 . ?
Lu14 Lu10 C67 101.9(9) . . ?
C44 Lu10 C67 35.7(3) . . ?
Lu3 Lu10 C45 69.6(10) . . ?
Lu3 Lu10 C45 80.5(12) 6 . ?
Lu12 Lu10 C45 105.2(14) 6 . ?
Lu12 Lu10 C45 82.5(11) . . ?
Lu16 Lu10 C45 92.0(10) . . ?
Lu16 Lu10 C45 101.6(12) 6 . ?
Lu8 Lu10 C45 153.0(11) . . ?
Lu14 Lu10 C45 108.9(8) 6 . ?
Lu14 Lu10 C45 134.3(10) . . ?
C44 Lu10 C45 37.1(3) . . ?
C67 Lu10 C45 64.6(4) . . ?
Lu6 Lu11 Lu16 95(2) 6 . ?
Lu6 Lu11 Lu12 141.4(19) 6 . ?
Lu16 Lu11 Lu12 53.0(18) . . ?
Lu6 Lu11 Lu14 130.8(17) 6 6 ?
Lu16 Lu11 Lu14 96(2) . 6 ?
Lu12 Lu11 Lu14 48.7(13) . 6 ?
Lu6 Lu11 Lu3 123.7(18) 6 . ?
Lu16 Lu11 Lu3 29.8(16) . . ?
Lu12 Lu11 Lu3 24.0(6) . . ?
Lu14 Lu11 Lu3 71.4(14) 6 . ?
Lu6 Lu11 C26 99.0(14) 6 . ?
Lu16 Lu11 C26 114.5(15) . . ?
Lu12 Lu11 C26 113.0(11) . . ?
Lu14 Lu11 C26 119.0(14) 6 . ?
Lu3 Lu11 C26 112.0(9) . . ?
Lu6 Lu11 C6 81.3(13) 6 . ?
Lu16 Lu11 C6 88.3(16) . . ?
Lu12 Lu11 C6 114.2(11) . . ?
Lu14 Lu11 C6 146.6(15) 6 . ?
Lu3 Lu11 C6 99.7(9) . . ?
C26 Lu11 C6 33.3(2) . . ?
Lu6 Lu11 Lu4 17.8(6) 6 6 ?
Lu16 Lu11 Lu4 91.1(17) . 6 ?
Lu12 Lu11 Lu4 127.9(11) . 6 ?
Lu14 Lu11 Lu4 114.3(12) 6 6 ?
Lu3 Lu11 Lu4 116.0(10) . 6 ?
C26 Lu11 Lu4 116.3(11) . 6 ?
C6 Lu11 Lu4 98.6(9) . 6 ?
Lu6 Lu11 C25 134.7(15) 6 . ?
Lu16 Lu11 C25 104.9(15) . . ?
Lu12 Lu11 C25 79.8(9) . . ?
Lu14 Lu11 C25 87.5(13) 6 . ?
Lu3 Lu11 C25 87.2(8) . . ?
C26 Lu11 C25 35.7(2) . . ?
C6 Lu11 C25 59.6(4) . . ?
Lu4 Lu11 C25 151.7(11) 6 . ?
Lu6 Lu11 Lu2 89.4(11) 6 6 ?
Lu16 Lu11 Lu2 107.5(15) . 6 ?
Lu12 Lu11 Lu2 82.3(9) . 6 ?
Lu14 Lu11 Lu2 41.7(11) 6 6 ?
Lu3 Lu11 Lu2 97.9(8) . 6 ?
C26 Lu11 Lu2 136.1(11) . 6 ?
C6 Lu11 Lu2 162.4(12) . 6 ?
Lu4 Lu11 Lu2 74.0(5) 6 6 ?
C25 Lu11 Lu2 121.1(9) . 6 ?
Lu6 Lu11 Lu5 70.7(10) 6 6 ?
Lu16 Lu11 Lu5 109.9(13) . 6 ?
Lu12 Lu11 Lu5 98.2(9) . 6 ?
Lu14 Lu11 Lu5 60.5(12) 6 6 ?
Lu3 Lu11 Lu5 109.4(8) . 6 ?
C26 Lu11 Lu5 135.2(11) . 6 ?
C6 Lu11 Lu5 147.5(12) . 6 ?
Lu4 Lu11 Lu5 55.9(4) 6 6 ?
C25 Lu11 Lu5 134.2(10) . 6 ?
Lu2 Lu11 Lu5 18.8(2) 6 6 ?
Lu6 Lu11 C27 88.4(15) 6 . ?
Lu16 Lu11 C27 148.0(15) . . ?
Lu12 Lu11 C27 130.1(12) . . ?
Lu14 Lu11 C27 105.6(13) 6 . ?
Lu3 Lu11 C27 141.1(9) . . ?
C26 Lu11 C27 33.9(3) . . ?
C6 Lu11 C27 60.7(5) . . ?
Lu4 Lu11 C27 100.7(9) 6 . ?
C25 Lu11 C27 54.0(4) . . ?
Lu2 Lu11 C27 104.3(8) 6 . ?
Lu5 Lu11 C27 101.3(8) 6 . ?
Lu3 Lu12 Lu10 62.6(18) . . ?
Lu3 Lu12 Lu16 53.4(17) . . ?
Lu10 Lu12 Lu16 104(2) . . ?
Lu3 Lu12 Lu14 156.1(16) . 6 ?
Lu10 Lu12 Lu14 115(2) . 6 ?
Lu16 Lu12 Lu14 109(2) . 6 ?
Lu3 Lu12 Lu3 22.5(8) . 6 ?
Lu10 Lu12 Lu3 42.5(14) . 6 ?
Lu16 Lu12 Lu3 64.6(17) . 6 ?
Lu14 Lu12 Lu3 141.5(13) 6 6 ?
Lu3 Lu12 Lu11 101.3(16) . . ?
Lu10 Lu12 Lu11 145.6(14) . . ?
Lu16 Lu12 Lu11 49.0(16) . . ?
Lu14 Lu12 Lu11 67.0(16) 6 . ?
Lu3 Lu12 Lu11 113.1(12) 6 . ?
Lu3 Lu12 Lu12 42.4(12) . 6 ?
Lu10 Lu12 Lu12 27.2(13) . 6 ?
Lu16 Lu12 Lu12 77.0(17) . 6 ?
Lu14 Lu12 Lu12 124.5(13) 6 6 ?
Lu3 Lu12 Lu12 19.9(5) 6 6 ?
Lu11 Lu12 Lu12 121.1(9) . 6 ?
Lu3 Lu12 Lu16 30.9(9) . 6 ?
Lu10 Lu12 Lu16 62.8(15) . 6 ?
Lu16 Lu12 Lu16 41.4(19) . 6 ?
Lu14 Lu12 Lu16 125.3(12) 6 6 ?
Lu3 Lu12 Lu16 26.6(7) 6 6 ?
Lu11 Lu12 Lu16 87.6(12) . 6 ?
Lu12 Lu12 Lu16 35.6(9) 6 6 ?
Lu3 Lu12 C46 87.8(11) . . ?
Lu10 Lu12 C46 90.6(11) . . ?
Lu16 Lu12 C46 120.4(12) . . ?
Lu14 Lu12 C46 116.1(11) 6 . ?
Lu3 Lu12 C46 97.3(8) 6 . ?
Lu11 Lu12 C46 120.5(9) . . ?
Lu12 Lu12 C46 105.0(5) 6 . ?
Lu16 Lu12 C46 118.6(9) 6 . ?
Lu3 Lu12 C47 123.4(13) . . ?
Lu10 Lu12 C47 95.1(12) . . ?
Lu16 Lu12 C47 152.1(13) . . ?
Lu14 Lu12 C47 79.9(10) 6 . ?
Lu3 Lu12 C47 124.6(9) 6 . ?
Lu11 Lu12 C47 118.3(11) . . ?
Lu12 Lu12 C47 120.6(4) 6 . ?
Lu16 Lu12 C47 150.9(11) 6 . ?
C46 Lu12 C47 38.21(18) . . ?
Lu3 Lu12 C24 91.7(11) . . ?
Lu10 Lu12 C24 123.6(13) . . ?
Lu16 Lu12 C24 95.6(11) . . ?
Lu14 Lu12 C24 107.2(13) 6 . ?
Lu3 Lu12 C24 111.2(6) 6 . ?
Lu11 Lu12 C24 84.8(8) . . ?
Lu12 Lu12 C24 127.6(4) 6 . ?
Lu16 Lu12 C24 118.2(9) 6 . ?
C46 Lu12 C24 35.80(16) . . ?
C47 Lu12 C24 56.6(2) . . ?
Lu3 Lu12 Lu8 107.3(13) . . ?
Lu10 Lu12 Lu8 55.5(13) . . ?
Lu16 Lu12 Lu8 110.4(10) . . ?
Lu14 Lu12 Lu8 60.8(13) 6 . ?
Lu3 Lu12 Lu8 85.2(6) 6 . ?
Lu11 Lu12 Lu8 108.5(8) . . ?
Lu12 Lu12 Lu8 65.6(4) 6 . ?
Lu16 Lu12 Lu8 85.9(8) 6 . ?
C46 Lu12 Lu8 124.6(7) . . ?
C47 Lu12 Lu8 97.1(6) . . ?
C24 Lu12 Lu8 153.5(6) . . ?
Lu9 Lu13 Lu15 50.3(13) . 6 ?
Lu9 Lu13 Lu4 148.7(13) . 6 ?
Lu15 Lu13 Lu4 120.2(17) 6 6 ?
Lu9 Lu13 Lu13 50.5(12) . 6 ?
Lu15 Lu13 Lu13 97.8(16) 6 6 ?
Lu4 Lu13 Lu13 115.0(7) 6 6 ?
Lu9 Lu13 Lu1 110.7(13) . . ?
Lu15 Lu13 Lu1 136.3(11) 6 . ?
Lu4 Lu13 Lu1 52.0(7) 6 . ?
Lu13 Lu13 Lu1 63.7(5) 6 . ?
Lu9 Lu13 Lu15 17.5(12) . . ?
Lu15 Lu13 Lu15 60(2) 6 . ?
Lu4 Lu13 Lu15 133.0(10) 6 . ?
Lu13 Lu13 Lu15 38.3(9) 6 . ?
Lu1 Lu13 Lu15 93.9(9) . . ?
Lu9 Lu13 Lu5 79.8(13) . 6 ?
Lu15 Lu13 Lu5 32.0(14) 6 6 ?
Lu4 Lu13 Lu5 88.5(7) 6 6 ?
Lu13 Lu13 Lu5 119.0(4) 6 6 ?
Lu1 Lu13 Lu5 121.1(6) . 6 ?
Lu15 Lu13 Lu5 83.8(9) . 6 ?
Lu9 Lu13 C32 98.4(12) . . ?
Lu15 Lu13 C32 100.0(12) 6 . ?
Lu4 Lu13 C32 112.9(8) 6 . ?
Lu13 Lu13 C32 109.0(4) 6 . ?
Lu1 Lu13 C32 123.1(8) . . ?
Lu15 Lu13 C32 113.1(9) . . ?
Lu5 Lu13 C32 111.2(7) 6 . ?
Lu9 Lu13 Lu4 77.8(12) . . ?
Lu15 Lu13 Lu4 115.8(15) 6 . ?
Lu4 Lu13 Lu4 83.9(9) 6 . ?
Lu13 Lu13 Lu4 31.1(4) 6 . ?
Lu1 Lu13 Lu4 33.3(3) . . ?
Lu15 Lu13 Lu4 61.8(9) . . ?
Lu5 Lu13 Lu4 121.2(5) 6 . ?
C32 Lu13 Lu4 125.4(6) . . ?
Lu9 Lu13 C33 64.3(12) . . ?
Lu15 Lu13 C33 83.9(13) 6 . ?
Lu4 Lu13 C33 146.5(8) 6 . ?
Lu13 Lu13 C33 80.8(3) 6 . ?
Lu1 Lu13 C33 126.9(7) . . ?
Lu15 Lu13 C33 78.1(8) . . ?
Lu5 Lu13 C33 110.1(8) 6 . ?
C32 Lu13 C33 34.99(18) . . ?
Lu4 Lu13 C33 107.5(6) . . ?
Lu9 Lu13 C13 124.2(14) . . ?
Lu15 Lu13 C13 137.9(12) 6 . ?
Lu4 Lu13 C13 83.7(7) 6 . ?
Lu13 Lu13 C13 102.3(4) 6 . ?
Lu1 Lu13 C13 85.8(7) . . ?
Lu15 Lu13 C13 130.4(8) . . ?
Lu5 Lu13 C13 137.2(7) 6 . ?
C32 Lu13 C13 38.32(17) . . ?
Lu4 Lu13 C13 99.8(6) . . ?
C33 Lu13 C13 63.6(2) . . ?
Lu9 Lu13 C31 108.4(12) . . ?
Lu15 Lu13 C31 79.5(13) 6 . ?
Lu4 Lu13 C31 96.9(8) 6 . ?
Lu13 Lu13 C31 143.5(3) 6 . ?
Lu1 Lu13 C31 139.2(8) . . ?
Lu15 Lu13 C31 125.9(11) . . ?
Lu5 Lu13 C31 77.0(5) 6 . ?
C32 Lu13 C31 38.0(2) . . ?
Lu4 Lu13 C31 161.8(6) . . ?
C33 Lu13 C31 62.7(3) . . ?
C13 Lu13 C31 62.4(2) . . ?
Lu12 Lu14 Lu11 64.3(17) 6 6 ?
Lu12 Lu14 Lu2 135.1(13) 6 . ?
Lu11 Lu14 Lu2 99.6(14) 6 . ?
Lu12 Lu14 Lu3 8.9(6) 6 6 ?
Lu11 Lu14 Lu3 60.7(13) 6 6 ?
Lu2 Lu14 Lu3 126.4(9) . 6 ?
Lu12 Lu14 Lu10 30.1(11) 6 . ?
Lu11 Lu14 Lu10 89.0(17) 6 . ?
Lu2 Lu14 Lu10 117.6(12) . . ?
Lu3 Lu14 Lu10 29.4(8) 6 . ?
Lu12 Lu14 Lu16 35.1(12) 6 6 ?
Lu11 Lu14 Lu16 34.8(12) 6 6 ?
Lu2 Lu14 Lu16 109.0(11) . 6 ?
Lu3 Lu14 Lu16 28.6(9) 6 6 ?
Lu10 Lu14 Lu16 54.6(13) . 6 ?
Lu12 Lu14 Lu8 87.0(13) 6 . ?
Lu11 Lu14 Lu8 123.1(12) 6 . ?
Lu2 Lu14 Lu8 66.6(10) . . ?
Lu3 Lu14 Lu8 83.3(9) 6 . ?
Lu10 Lu14 Lu8 57.8(9) . . ?
Lu16 Lu14 Lu8 95.2(11) 6 . ?
Lu12 Lu14 C64 105.6(16) 6 . ?
Lu11 Lu14 C64 112.0(16) 6 . ?
Lu2 Lu14 C64 119.2(14) . . ?
Lu3 Lu14 C64 114.3(13) 6 . ?
Lu10 Lu14 C64 113.6(12) . . ?
Lu16 Lu14 C64 126.8(16) 6 . ?
Lu8 Lu14 C64 123.0(12) . . ?
Lu12 Lu14 Lu5 124.7(11) 6 . ?
Lu11 Lu14 Lu5 81.3(12) 6 . ?
Lu2 Lu14 Lu5 18.3(3) . . ?
Lu3 Lu14 Lu5 115.9(8) 6 . ?
Lu10 Lu14 Lu5 117.1(9) . . ?
Lu16 Lu14 Lu5 93.6(10) 6 . ?
Lu8 Lu14 Lu5 76.9(10) . . ?
C64 Lu14 Lu5 127.6(13) . . ?
Lu12 Lu14 C81 136.6(15) 6 . ?
Lu11 Lu14 C81 137.2(16) 6 . ?
Lu2 Lu14 C81 84.6(12) . . ?
Lu3 Lu14 C81 145.0(12) 6 . ?
Lu10 Lu14 C81 126.8(13) . . ?
Lu16 Lu14 C81 164.1(15) 6 . ?
Lu8 Lu14 C81 97.8(12) . . ?
C64 Lu14 C81 37.5(3) . . ?
Lu5 Lu14 C81 98.2(12) . . ?
Lu12 Lu14 Lu6 76.8(13) 6 . ?
Lu11 Lu14 Lu6 19.0(7) 6 . ?
Lu2 Lu14 Lu6 80.7(8) . . ?
Lu3 Lu14 Lu6 71.0(8) 6 . ?
Lu10 Lu14 Lu6 95.5(12) . . ?
Lu16 Lu14 Lu6 42.5(10) 6 . ?
Lu8 Lu14 Lu6 112.5(8) . . ?
C64 Lu14 Lu6 124.5(12) . . ?
Lu5 Lu14 Lu6 62.4(6) . . ?
C81 Lu14 Lu6 137.1(12) . . ?
Lu12 Lu14 C63 102.7(17) 6 . ?
Lu11 Lu14 C63 79.1(13) 6 . ?
Lu2 Lu14 C63 115.5(12) . . ?
Lu3 Lu14 C63 108.9(14) 6 . ?
Lu10 Lu14 C63 126.8(15) . . ?
Lu16 Lu14 C63 104.3(15) 6 . ?
Lu8 Lu14 C63 157.7(11) . . ?
C64 Lu14 C63 35.2(3) . . ?
Lu5 Lu14 C63 112.0(11) . . ?
C81 Lu14 C63 61.4(4) . . ?
Lu6 Lu14 C63 89.4(9) . . ?
Lu9 Lu15 Lu13 57.0(16) . 6 ?
Lu9 Lu15 Lu5 156(2) . . ?
Lu13 Lu15 Lu5 116(2) 6 . ?
Lu9 Lu15 Lu15 30(2) . 6 ?
Lu13 Lu15 Lu15 82.2(16) 6 6 ?
Lu5 Lu15 Lu15 133.4(11) . 6 ?
Lu9 Lu15 Lu7 92(3) . . ?
Lu13 Lu15 Lu7 131.5(16) 6 . ?
Lu5 Lu15 Lu7 76.2(12) . . ?
Lu15 Lu15 Lu7 61.6(9) 6 . ?
Lu9 Lu15 Lu2 143(2) . . ?
Lu13 Lu15 Lu2 126.7(19) 6 . ?
Lu5 Lu15 Lu2 18.5(6) . . ?
Lu15 Lu15 Lu2 116.2(8) 6 . ?
Lu7 Lu15 Lu2 57.7(7) . . ?
Lu9 Lu15 Lu13 19.2(15) . . ?
Lu13 Lu15 Lu13 43.9(13) 6 . ?
Lu5 Lu15 Lu13 139.0(14) . . ?
Lu15 Lu15 Lu13 38.3(9) 6 . ?
Lu7 Lu15 Lu13 94.7(12) . . ?
Lu2 Lu15 Lu13 133.1(10) . . ?
Lu9 Lu15 Lu4 83(2) . . ?
Lu13 Lu15 Lu4 30.4(10) 6 . ?
Lu5 Lu15 Lu4 86.0(15) . . ?
Lu15 Lu15 Lu4 99.8(7) 6 . ?
Lu7 Lu15 Lu4 122.4(10) . . ?
Lu2 Lu15 Lu4 96.5(11) . . ?
Lu13 Lu15 Lu4 65.1(8) . . ?
Lu9 Lu15 C57 94(2) . . ?
Lu13 Lu15 C57 120.1(14) 6 . ?
Lu5 Lu15 C57 108.1(14) . . ?
Lu15 Lu15 C57 95.8(8) 6 . ?
Lu7 Lu15 C57 96.0(12) . . ?
Lu2 Lu15 C57 107.9(11) . . ?
Lu13 Lu15 C57 112.6(13) . . ?
Lu4 Lu15 C57 141.4(11) . . ?
Lu9 Lu15 C58 105.3(16) . . ?
Lu13 Lu15 C58 94.3(13) 6 . ?
Lu5 Lu15 C58 98.3(13) . . ?
Lu15 Lu15 C58 124.0(7) 6 . ?
Lu7 Lu15 C58 131.9(13) . . ?
Lu2 Lu15 C58 110.2(11) . . ?
Lu13 Lu15 C58 116.0(11) . . ?
Lu4 Lu15 C58 104.3(11) . . ?
C57 Lu15 C58 39.4(3) . . ?
Lu9 Lu15 C56 58.8(19) . . ?
Lu13 Lu15 C56 99.7(16) 6 . ?
Lu5 Lu15 C56 141.2(16) . . ?
Lu15 Lu15 C56 63.1(6) 6 . ?
Lu7 Lu15 C56 91.8(13) . . ?
Lu2 Lu15 C56 133.6(13) . . ?
Lu13 Lu15 C56 77.8(11) . . ?
Lu4 Lu15 C56 129.9(11) . . ?
C57 Lu15 C56 35.6(4) . . ?
C58 Lu15 C56 62.6(5) . . ?
Lu9 Lu15 C77 117(3) . . ?
Lu13 Lu15 C77 154.1(14) 6 . ?
Lu5 Lu15 C77 79.7(12) . . ?
Lu15 Lu15 C77 102.3(7) 6 . ?
Lu7 Lu15 C77 70.3(9) . . ?
Lu2 Lu15 C77 74.7(8) . . ?
Lu13 Lu15 C77 135.4(15) . . ?
Lu4 Lu15 C77 157.9(13) . . ?
C57 Lu15 C77 34.6(3) . . ?
C58 Lu15 C77 61.8(5) . . ?
C56 Lu15 C77 61.6(6) . . ?
Lu3 Lu16 Lu11 114(3) . . ?
Lu3 Lu16 Lu12 37.5(13) . . ?
Lu11 Lu16 Lu12 78(2) . . ?
Lu3 Lu16 Lu16 73.7(17) . 6 ?
Lu11 Lu16 Lu16 155.1(12) . 6 ?
Lu12 Lu16 Lu16 103.0(17) . 6 ?
Lu3 Lu16 Lu3 33.4(12) . 6 ?
Lu11 Lu16 Lu3 143(3) . 6 ?
Lu12 Lu16 Lu3 66.1(18) . 6 ?
Lu16 Lu16 Lu3 40.3(10) 6 6 ?
Lu3 Lu16 Lu6 151(3) . 6 ?
Lu11 Lu16 Lu6 38.6(15) . 6 ?
Lu12 Lu16 Lu6 113(2) . 6 ?
Lu16 Lu16 Lu6 125.7(9) 6 6 ?
Lu3 Lu16 Lu6 157.4(13) 6 6 ?
Lu3 Lu16 Lu10 22.8(10) . . ?
Lu11 Lu16 Lu10 110(2) . . ?
Lu12 Lu16 Lu10 35.3(13) . . ?
Lu16 Lu16 Lu10 67.7(9) 6 . ?
Lu3 Lu16 Lu10 33.0(8) 6 . ?
Lu6 Lu16 Lu10 136.6(16) 6 . ?
Lu3 Lu16 C7 106.7(14) . . ?
Lu11 Lu16 C7 100(2) . . ?
Lu12 Lu16 C7 123.7(13) . . ?
Lu16 Lu16 C7 100.2(9) 6 . ?
Lu3 Lu16 C7 107.2(14) 6 . ?
Lu6 Lu16 C7 91.9(15) 6 . ?
Lu10 Lu16 C7 128.8(15) . . ?
Lu3 Lu16 Lu14 72.4(17) . 6 ?
Lu11 Lu16 Lu14 49.1(17) . 6 ?
Lu12 Lu16 Lu14 36.0(12) . 6 ?
Lu16 Lu16 Lu14 119.2(11) 6 6 ?
Lu3 Lu16 Lu14 94.4(16) 6 6 ?
Lu6 Lu16 Lu14 78.7(14) 6 6 ?
Lu10 Lu16 Lu14 61.6(12) . 6 ?
C7 Lu16 Lu14 137.3(15) . 6 ?
Lu3 Lu16 Lu12 42.3(15) . 6 ?
Lu11 Lu16 Lu12 137(2) . 6 ?
Lu12 Lu16 Lu12 67.3(19) . 6 ?
Lu16 Lu16 Lu12 35.7(9) 6 6 ?
Lu3 Lu16 Lu12 15.2(5) 6 6 ?
Lu6 Lu16 Lu12 142.2(11) 6 6 ?
Lu10 Lu16 Lu12 32.0(8) . 6 ?
C7 Lu16 Lu12 120.0(15) . 6 ?
Lu14 Lu16 Lu12 88.7(14) 6 6 ?
Lu3 Lu16 C23 73.4(10) . . ?
Lu11 Lu16 C23 95.5(15) . . ?
Lu12 Lu16 C23 84.8(12) . . ?
Lu16 Lu16 C23 109.4(8) 6 . ?
Lu3 Lu16 C23 89.9(11) 6 . ?
Lu6 Lu16 C23 112.7(15) 6 . ?
Lu10 Lu16 C23 96.0(12) . . ?
C7 Lu16 C23 39.0(3) . . ?
Lu14 Lu16 C23 107.1(13) 6 . ?
Lu12 Lu16 C23 105.1(13) 6 . ?
Lu3 Lu16 C20 110.5(19) . . ?
Lu11 Lu16 C20 120(2) . . ?
Lu12 Lu16 C20 142.4(17) . . ?
Lu16 Lu16 C20 74.1(7) 6 . ?
Lu3 Lu16 C20 94.5(14) 6 . ?
Lu6 Lu16 C20 96.7(14) 6 . ?
Lu10 Lu16 C20 125.9(16) . . ?
C7 Lu16 C20 29.0(4) . . ?
Lu14 Lu16 C20 166.1(15) 6 . ?
Lu12 Lu16 C20 102.4(13) 6 . ?
C23 Lu16 C20 62.3(5) . . ?
C9 C1 C5 133.3 . . ?
C9 C1 C2 123.0 . . ?
C5 C1 C2 96.9 . . ?
C9 C1 Lu1 101.12(6) . . ?
C5 C1 Lu1 75.40(6) . . ?
C2 C1 Lu1 62.0 . . ?
C3 C2 C12 109.5 . . ?
C3 C2 C1 119.6 . . ?
C12 C2 C1 117.0 . . ?
C3 C2 Lu1 69.24(7) . . ?
C12 C2 Lu1 79.55(6) . . ?
C1 C2 Lu1 83.36(5) . . ?
C15 C3 C2 128.4 . . ?
C15 C3 C4 126.6 . . ?
C2 C3 C4 93.5 . . ?
C15 C3 Lu1 79.77(6) . . ?
C2 C3 Lu1 76.41(8) . . ?
C4 C3 Lu1 80.39(6) . . ?
C15 C3 Lu4 65.95(14) . . ?
C2 C3 Lu4 103.41(14) . . ?
C4 C3 Lu4 73.95(13) . . ?
Lu1 C3 Lu4 27.43(12) . . ?
C5 C4 C3 122.5 . . ?
C5 C4 C18 106.0 . . ?
C3 C4 C18 125.6 . . ?
C5 C4 C17 144.7 . . ?
C3 C4 C17 80.9 . . ?
C18 C4 C17 44.7 . . ?
C5 C4 Lu1 85.27(6) . . ?
C3 C4 Lu1 64.2 . . ?
C18 C4 Lu1 99.85(7) . . ?
C17 C4 Lu1 82.51(7) . . ?
C5 C4 Lu4 101.33(12) . . ?
C3 C4 Lu4 72.94(12) . . ?
C18 C4 Lu4 74.81(14) . . ?
C17 C4 Lu4 57.49(14) . . ?
Lu1 C4 Lu4 26.87(13) . . ?
C5 C4 Lu6 87.79(18) . . ?
C3 C4 Lu6 102.07(17) . . ?
C18 C4 Lu6 53.76(12) . . ?
C17 C4 Lu6 59.81(17) . . ?
Lu1 C4 Lu6 47.67(12) . . ?
Lu4 C4 Lu6 29.23(19) . . ?
C4 C5 C20 144.9 . . ?
C4 C5 C1 106.4 . . ?
C20 C5 C1 101.8 . . ?
C4 C5 Lu1 66.59(5) . . ?
C20 C5 Lu1 103.7 . . ?
C1 C5 Lu1 72.04(7) . . ?
C26 C6 C7 136.2 . . ?
C26 C6 C9 116.7 . . ?
C7 C6 C9 96.9 . . ?
C26 C6 Lu11 71.4(6) . . ?
C7 C6 Lu11 83.4(6) . . ?
C9 C6 Lu11 88.0(6) . . ?
C26 C6 Lu16 94.5(7) . . ?
C7 C6 Lu16 55.2(7) . . ?
C9 C6 Lu16 91.8(6) . . ?
Lu11 C6 Lu16 28.2(7) . . ?
C20 C7 C23 133.8 . . ?
C20 C7 C6 139.0 . . ?
C23 C7 C6 86.3 . . ?
C20 C7 Lu16 91.1(8) . . ?
C23 C7 Lu16 79.1(7) . . ?
C6 C7 Lu16 88.7(9) . . ?
C20 C7 Lu3 95.61(15) . . ?
C23 C7 Lu3 60.69(13) . . ?
C6 C7 Lu3 99.36(14) . . ?
Lu16 C7 Lu3 22.3(8) . . ?
C20 C7 Lu11 111.2(4) . . ?
C23 C7 Lu11 78.9(5) . . ?
C6 C7 Lu11 61.3(5) . . ?
Lu16 C7 Lu11 27.4(9) . . ?
Lu3 C7 Lu11 42.6(6) . . ?
C21 C8 C19 136.5 . . ?
C21 C8 C20 103.2 . . ?
C19 C8 C20 109.3 . . ?
C21 C8 Lu6 105.74(14) . . ?
C19 C8 Lu6 50.23(12) . . ?
C20 C8 Lu6 86.14(15) . . ?
C21 C8 Lu16 70.1(6) . . ?
C19 C8 Lu16 106.7(4) . . ?
C20 C8 Lu16 54.6(6) . . ?
Lu6 C8 Lu16 57.2(4) . . ?
C1 C9 C10 117.2 . . ?
C1 C9 C6 122.2 . . ?
C10 C9 C6 117.6 . . ?
C1 C9 Lu11 107.6(4) . . ?
C10 C9 Lu11 89.4(5) . . ?
C6 C9 Lu11 56.6(4) . . ?
C11 C10 C28 102.9 . . ?
C11 C10 C9 124.3 . . ?
C28 C10 C9 118.8 . . ?
C10 C11 C30 112.6 . . ?
C10 C11 C12 114.2 . . ?
C30 C11 C12 124.2 . . ?
C10 C11 Lu13 106.3(2) . . ?
C30 C11 Lu13 70.3(3) . . ?
C12 C11 Lu13 68.9(3) . . ?
C2 C12 C13 128.8 . . ?
C2 C12 C11 120.8 . . ?
C13 C12 C11 99.3 . . ?
C2 C12 Lu1 67.2 . . ?
C13 C12 Lu1 77.0 . . ?
C11 C12 Lu1 98.90(6) . . ?
C2 C12 Lu13 98.6(3) . . ?
C13 C12 Lu13 54.7(2) . . ?
C11 C12 Lu13 81.5(3) . . ?
Lu1 C12 Lu13 31.4(3) . . ?
C12 C13 C32 141.0 . . ?
C12 C13 C14 109.4 . . ?
C32 C13 C14 98.1 . . ?
C12 C13 Lu13 94.7(4) . . ?
C32 C13 Lu13 60.8(4) . . ?
C14 C13 Lu13 83.5(3) . . ?
C12 C13 Lu1 71.05(5) . . ?
C32 C13 Lu1 93.9 . . ?
C14 C13 Lu1 70.37(7) . . ?
Lu13 C13 Lu1 33.8(4) . . ?
C15 C14 C34 128.9 . . ?
C15 C14 C13 118.6 . . ?
C34 C14 C13 101.4 . . ?
C15 C14 Lu1 69.42(6) . . ?
C34 C14 Lu1 95.3 . . ?
C13 C14 Lu1 73.69(7) . . ?
C15 C14 Lu13 101.7(3) . . ?
C34 C14 Lu13 71.4(3) . . ?
C13 C14 Lu13 59.4(3) . . ?
Lu1 C14 Lu13 32.6(3) . . ?
C15 C14 Lu4 61.00(10) . . ?
C34 C14 Lu4 83.86(14) . . ?
C13 C14 Lu4 98.64(13) . . ?
Lu1 C14 Lu4 25.85(13) . . ?
Lu13 C14 Lu4 46.2(3) . . ?
C15 C14 Lu9 105.1(3) . . ?
C34 C14 Lu9 53.5(3) . . ?
C13 C14 Lu9 75.77(10) . . ?
Lu1 C14 Lu9 43.2(3) . . ?
Lu13 C14 Lu9 20.2(3) . . ?
Lu4 C14 Lu9 44.1(3) . . ?
C16 C15 C14 117.7 . . ?
C16 C15 C3 109.7 . . ?
C14 C15 C3 123.9 . . ?
C16 C15 Lu4 64.23(16) . . ?
C14 C15 Lu4 91.02(14) . . ?
C3 C15 Lu4 83.57(17) . . ?
C16 C15 Lu1 92.49(7) . . ?
C14 C15 Lu1 81.24(6) . . ?
C3 C15 Lu1 68.0 . . ?
Lu4 C15 Lu1 28.63(15) . . ?
C15 C16 C17 114.4 . . ?
C15 C16 C36 120.0 . . ?
C17 C16 C36 118.8 . . ?
C15 C16 Lu4 83.69(17) . . ?
C17 C16 Lu4 77.16(16) . . ?
C36 C16 Lu4 82.93(18) . . ?
C15 C16 Lu1 60.5 . . ?
C17 C16 Lu1 84.7 . . ?
C36 C16 Lu1 98.7 . . ?
Lu4 C16 Lu1 23.60(16) . . ?
C15 C16 Lu6 102.42(14) . . ?
C17 C16 Lu6 54.41(11) . . ?
C36 C16 Lu6 87.67(15) . . ?
Lu4 C16 Lu6 24.88(17) . . ?
Lu1 C16 Lu6 43.39(12) . . ?
C16 C17 C18 152.0 . . ?
C16 C17 C38 100.9 . . ?
C18 C17 C38 94.3 . . ?
C16 C17 C4 105.6 . . ?
C18 C17 C4 50.4 . . ?
C38 C17 C4 139.9 . . ?
C16 C17 Lu4 68.02(14) . . ?
C18 C17 Lu4 89.53(16) . . ?
C38 C17 Lu4 87.32(17) . . ?
C4 C17 Lu4 75.55(18) . . ?
C16 C17 Lu6 99.36(17) . . ?
C18 C17 Lu6 63.87(19) . . ?
C38 C17 Lu6 70.15(18) . . ?
C4 C17 Lu6 76.14(19) . . ?
Lu4 C17 Lu6 33.19(19) . . ?
C19 C18 C17 140.5 . . ?
C19 C18 C4 122.3 . . ?
C17 C18 C4 84.8 . . ?
C19 C18 Lu6 69.8(2) . . ?
C17 C18 Lu6 81.9(2) . . ?
C4 C18 Lu6 92.62(18) . . ?
C19 C18 Lu4 100.07(10) . . ?
C17 C18 Lu4 58.87(12) . . ?
C4 C18 Lu4 71.55(14) . . ?
Lu6 C18 Lu4 30.8(2) . . ?
C40 C19 C18 106.2 . . ?
C40 C19 C8 123.1 . . ?
C18 C19 C8 126.9 . . ?
C40 C19 Lu6 78.2(2) . . ?
C18 C19 Lu6 74.1(2) . . ?
C8 C19 Lu6 96.3(2) . . ?
C7 C20 C5 125.9 . . ?
C7 C20 C8 122.9 . . ?
C5 C20 C8 108.3 . . ?
C7 C20 Lu16 59.9(6) . . ?
C5 C20 Lu16 105.9(6) . . ?
C8 C20 Lu16 91.6(8) . . ?
C7 C20 Lu3 60.96(12) . . ?
C5 C20 Lu3 122.01(10) . . ?
C8 C20 Lu3 77.11(12) . . ?
Lu16 C20 Lu3 19.1(7) . . ?
C22 C21 C8 132.5 . . ?
C22 C21 C42 121.4 . . ?
C8 C21 C42 102.4 . . ?
C22 C21 Lu3 59.37(14) . . ?
C8 C21 Lu3 102.60(15) . . ?
C42 C21 Lu3 95.03(14) . . ?
C22 C21 Lu16 68.2(5) . . ?
C8 C21 Lu16 83.1(6) . . ?
C42 C21 Lu16 107.2(6) . . ?
Lu3 C21 Lu16 21.0(6) . . ?
C22 C21 Lu10 67.08(19) . . ?
C8 C21 Lu10 112.0(3) . . ?
C42 C21 Lu10 75.7(2) . . ?
Lu3 C21 Lu10 20.1(3) . . ?
Lu16 C21 Lu10 38.9(7) . . ?
C21 C22 C45 126.2 . . ?
C21 C22 C23 124.6 . . ?
C45 C22 C23 100.0 . . ?
C21 C22 Lu3 87.29(18) . . ?
C45 C22 Lu3 75.37(18) . . ?
C23 C22 Lu3 75.71(16) . . ?
C21 C22 Lu16 83.5(6) . . ?
C45 C22 Lu16 94.6(6) . . ?
C23 C22 Lu16 62.0(7) . . ?
Lu3 C22 Lu16 21.6(6) . . ?
C21 C22 Lu12 100.2(3) . . ?
C45 C22 Lu12 66.7(3) . . ?
C23 C22 Lu12 69.2(3) . . ?
Lu3 C22 Lu12 12.9(3) . . ?
Lu16 C22 Lu12 27.9(7) . . ?
C21 C22 Lu10 85.5(2) . . ?
C45 C22 Lu10 61.1(4) . . ?
C23 C22 Lu10 93.7(2) . . ?
Lu3 C22 Lu10 20.9(4) . . ?
Lu16 C22 Lu10 42.1(7) . . ?
Lu12 C22 Lu10 24.5(4) . . ?
C7 C23 C22 102.3 . . ?
C7 C23 C24 138.6 . . ?
C22 C23 C24 107.2 . . ?
C7 C23 Lu3 84.15(17) . . ?
C22 C23 Lu3 64.06(14) . . ?
C24 C23 Lu3 83.43(17) . . ?
C7 C23 Lu16 61.8(8) . . ?
C22 C23 Lu16 83.2(9) . . ?
C24 C23 Lu16 93.4(7) . . ?
Lu3 C23 Lu16 25.7(8) . . ?
C7 C23 Lu12 91.6(3) . . ?
C22 C23 Lu12 77.3(4) . . ?
C24 C23 Lu12 67.9(3) . . ?
Lu3 C23 Lu12 17.2(3) . . ?
Lu16 C23 Lu12 29.8(8) . . ?
C7 C23 Lu11 68.5(5) . . ?
C22 C23 Lu11 106.6(5) . . ?
C24 C23 Lu11 75.6(5) . . ?
Lu3 C23 Lu11 43.0(5) . . ?
Lu16 C23 Lu11 26.1(8) . . ?
Lu12 C23 Lu11 34.3(6) . . ?
C25 C24 C46 131.3 . . ?
C25 C24 C23 111.6 . . ?
C46 C24 C23 98.2 . . ?
C25 C24 Lu12 88.1(4) . . ?
C46 C24 Lu12 61.6(4) . . ?
C23 C24 Lu12 76.8(3) . . ?
C25 C24 Lu3 100.68(12) . . ?
C46 C24 Lu3 61.18(14) . . ?
C23 C24 Lu3 60.79(13) . . ?
Lu12 C24 Lu3 17.6(3) . . ?
C25 C24 Lu11 60.7(5) . . ?
C46 C24 Lu11 95.7(5) . . ?
C23 C24 Lu11 72.4(5) . . ?
Lu12 C24 Lu11 34.2(6) . . ?
Lu3 C24 Lu11 40.9(5) . . ?
C25 C24 Lu16 85.0(7) . . ?
C46 C24 Lu16 82.0(7) . . ?
C23 C24 Lu16 54.6(5) . . ?
Lu12 C24 Lu16 26.4(7) . . ?
Lu3 C24 Lu16 20.9(7) . . ?
Lu11 C24 Lu16 24.7(7) . . ?
C24 C25 C49 123.0 . . ?
C24 C25 C26 122.1 . . ?
C49 C25 C26 110.3 . . ?
C24 C25 Lu11 95.5(6) . . ?
C49 C25 Lu11 87.0(5) . . ?
C26 C25 Lu11 64.9(6) . . ?
C24 C25 Lu12 66.8(3) . . ?
C49 C25 Lu12 86.1(3) . . ?
C26 C25 Lu12 98.4(3) . . ?
Lu11 C25 Lu12 35.6(6) . . ?
C24 C25 Lu16 72.9(6) . . ?
C49 C25 Lu16 103.1(5) . . ?
C26 C25 Lu16 74.9(7) . . ?
Lu11 C25 Lu16 23.1(7) . . ?
Lu12 C25 Lu16 25.4(7) . . ?
C6 C26 C27 128.9 . . ?
C6 C26 C25 117.7 . . ?
C27 C26 C25 104.2 . . ?
C6 C26 Lu11 75.3(6) . . ?
C27 C26 Lu11 85.7(6) . . ?
C25 C26 Lu11 79.4(6) . . ?
C6 C26 Lu16 59.5(6) . . ?
C27 C26 Lu16 107.4(5) . . ?
C25 C26 Lu16 77.0(6) . . ?
Lu11 C26 Lu16 21.9(6) . . ?
C50 C27 C26 110.7 . . ?
C50 C27 C28 119.2 . . ?
C26 C27 C28 118.9 . . ?
C50 C27 Lu11 85.3(5) . . ?
C26 C27 Lu11 60.3(4) . . ?
C28 C27 Lu11 90.3(5) . . ?
C29 C28 C10 116.4 . . ?
C29 C28 C27 114.4 . . ?
C10 C28 C27 118.2 . . ?
C29 C28 Lu11 97.0(3) . . ?
C10 C28 Lu11 81.7(4) . . ?
C27 C28 Lu11 59.4(4) . . ?
C28 C29 C52 129.6 . . ?
C28 C29 C30 103.7 . . ?
C52 C29 C30 117.3 . . ?
C11 C30 C31 127.4 . . ?
C11 C30 C29 103.5 . . ?
C31 C30 C29 116.2 . . ?
C11 C30 Lu13 82.2(3) . . ?
C31 C30 Lu13 54.6(3) . . ?
C29 C30 Lu13 107.7(2) . . ?
C54 C31 C32 117.8 . . ?
C54 C31 C30 123.9 . . ?
C32 C31 C30 111.1 . . ?
C54 C31 Lu13 87.8(4) . . ?
C32 C31 Lu13 60.5(3) . . ?
C30 C31 Lu13 93.5(4) . . ?
C54 C31 Lu9 73.5(5) . . ?
C32 C31 Lu9 59.0(4) . . ?
C30 C31 Lu9 113.2(4) . . ?
Lu13 C31 Lu9 20.2(5) . . ?
C33 C32 C31 119.4 . . ?
C33 C32 C13 121.0 . . ?
C31 C32 C13 111.9 . . ?
C33 C32 Lu13 79.9(4) . . ?
C31 C32 Lu13 81.5(4) . . ?
C13 C32 Lu13 80.9(5) . . ?
C33 C32 Lu9 55.8(3) . . ?
C31 C32 Lu9 90.2(3) . . ?
C13 C32 Lu9 99.2(5) . . ?
Lu13 C32 Lu9 24.9(5) . . ?
C32 C33 C56 125.5 . . ?
C32 C33 C34 101.3 . . ?
C56 C33 C34 124.8 . . ?
C32 C33 Lu9 92.0(4) . . ?
C56 C33 Lu9 65.2(7) . . ?
C34 C33 Lu9 88.0(5) . . ?
C32 C33 Lu13 65.1(3) . . ?
C56 C33 Lu13 87.6(4) . . ?
C34 C33 Lu13 87.5(4) . . ?
Lu9 C33 Lu13 27.6(5) . . ?
C32 C33 Lu15 110.0(4) . . ?
C56 C33 Lu15 58.7(6) . . ?
C34 C33 Lu15 80.4(6) . . ?
Lu9 C33 Lu15 18.6(5) . . ?
Lu13 C33 Lu15 45.0(5) . . ?
C14 C34 C33 117.4 . . ?
C14 C34 C35 107.7 . . ?
C33 C34 C35 124.4 . . ?
C14 C34 Lu9 99.1(5) . . ?
C33 C34 Lu9 55.9(3) . . ?
C35 C34 Lu9 87.53(18) . . ?
C14 C34 Lu13 78.1(4) . . ?
C33 C34 Lu13 59.1(3) . . ?
C35 C34 Lu13 103.8(3) . . ?
Lu9 C34 Lu13 23.4(4) . . ?
C14 C34 Lu15 107.4(4) . . ?
C33 C34 Lu15 68.7(6) . . ?
C35 C34 Lu15 68.0(6) . . ?
Lu9 C34 Lu15 19.8(5) . . ?
Lu13 C34 Lu15 41.0(5) . . ?
C14 C34 Lu4 68.25(11) . . ?
C33 C34 Lu4 100.82(9) . . ?
C35 C34 Lu4 66.92(14) . . ?
Lu9 C34 Lu4 46.2(4) . . ?
Lu13 C34 Lu4 44.7(3) . . ?
Lu15 C34 Lu4 42.4(5) . . ?
C36 C35 C58 133.2 . . ?
C36 C35 C34 123.7 . . ?
C58 C35 C34 95.9 . . ?
C36 C35 Lu15 103.1(6) . . ?
C58 C35 Lu15 57.7(5) . . ?
C34 C35 Lu15 78.8(6) . . ?
C36 C35 Lu4 64.65(11) . . ?
C58 C35 Lu4 102.12(9) . . ?
C34 C35 Lu4 82.08(14) . . ?
Lu15 C35 Lu4 45.5(5) . . ?
C36 C35 Lu9 110.1(3) . . ?
C58 C35 Lu9 67.0(5) . . ?
C34 C35 Lu9 59.4(3) . . ?
Lu15 C35 Lu9 19.7(5) . . ?
Lu4 C35 Lu9 45.8(4) . . ?
C35 C36 C16 121.1 . . ?
C35 C36 C37 118.2 . . ?
C16 C36 C37 111.1 . . ?
C35 C36 Lu4 90.34(13) . . ?
C16 C36 Lu4 61.09(12) . . ?
C37 C36 Lu4 87.53(14) . . ?
C60 C37 C36 122.9 . . ?
C60 C37 C38 131.2 . . ?
C36 C37 C38 92.7 . . ?
C60 C37 Lu4 101.31(9) . . ?
C36 C37 Lu4 60.77(11) . . ?
C38 C37 Lu4 65.69(12) . . ?
C60 C37 Lu5 54.58(13) . . ?
C36 C37 Lu5 87.89(16) . . ?
C38 C37 Lu5 100.37(13) . . ?
Lu4 C37 Lu5 46.83(15) . . ?
C17 C38 C39 136.6 . . ?
C17 C38 C37 115.5 . . ?
C39 C38 C37 97.0 . . ?
C17 C38 Lu6 76.03(18) . . ?
C39 C38 Lu6 74.37(19) . . ?
C37 C38 Lu6 92.75(18) . . ?
C17 C38 Lu4 60.24(12) . . ?
C39 C38 Lu4 103.25(10) . . ?
C37 C38 Lu4 77.87(15) . . ?
Lu6 C38 Lu4 31.1(2) . . ?
C40 C39 C62 115.9 . . ?
C40 C39 C38 104.0 . . ?
C62 C39 C38 129.3 . . ?
C40 C39 Lu6 68.1(2) . . ?
C62 C39 Lu6 97.65(15) . . ?
C38 C39 Lu6 68.72(19) . . ?
C39 C40 C19 134.1 . . ?
C39 C40 C41 106.3 . . ?
C19 C40 C41 110.3 . . ?
C39 C40 Lu6 81.3(2) . . ?
C19 C40 Lu6 67.1(2) . . ?
C41 C40 Lu6 98.06(18) . . ?
C63 C41 C42 120.9 . . ?
C63 C41 C40 106.6 . . ?
C42 C41 C40 117.9 . . ?
C63 C41 Lu14 60.6(5) . . ?
C42 C41 Lu14 77.7(6) . . ?
C40 C41 Lu14 95.4(4) . . ?
C43 C42 C21 115.2 . . ?
C43 C42 C41 112.9 . . ?
C21 C42 C41 128.7 . . ?
C43 C42 Lu14 76.2(5) . . ?
C21 C42 Lu14 104.4(4) . . ?
C41 C42 Lu14 71.0(5) . . ?
C43 C42 Lu10 65.8(4) . . ?
C21 C42 Lu10 74.1(4) . . ?
C41 C42 Lu10 111.8(3) . . ?
Lu14 C42 Lu10 41.4(5) . . ?
C43 C42 Lu3 82.13(13) . . ?
C21 C42 Lu3 54.48(10) . . ?
C41 C42 Lu3 118.10(11) . . ?
Lu14 C42 Lu3 54.4(4) . . ?
Lu10 C42 Lu3 20.3(4) . . ?
C42 C43 C65 122.8 . . ?
C42 C43 C44 119.4 . . ?
C65 C43 C44 96.4 . . ?
C42 C43 Lu10 84.2(5) . . ?
C65 C43 Lu10 82.2(5) . . ?
C44 C43 Lu10 55.1(3) . . ?
C42 C43 Lu14 74.5(6) . . ?
C65 C43 Lu14 58.4(5) . . ?
C44 C43 Lu14 94.8(5) . . ?
Lu10 C43 Lu14 42.9(5) . . ?
C67 C44 C45 122.0 . . ?
C67 C44 C43 112.2 . . ?
C45 C44 C43 117.6 . . ?
C67 C44 Lu10 75.5(7) . . ?
C45 C44 Lu10 77.0(5) . . ?
C43 C44 Lu10 89.5(2) . . ?
C67 C44 Lu3 94.80(11) . . ?
C45 C44 Lu3 56.39(11) . . ?
C43 C44 Lu3 92.55(14) . . ?
Lu10 C44 Lu3 22.3(6) . . ?
C67 C44 Lu12 82.0(3) . . ?
C45 C44 Lu12 58.4(2) . . ?
C43 C44 Lu12 105.1(2) . . ?
Lu10 C44 Lu12 20.3(4) . . ?
Lu3 C44 Lu12 15.2(2) . . ?
C46 C45 C22 115.6 . . ?
C46 C45 C44 113.5 . . ?
C22 C45 C44 118.0 . . ?
C46 C45 Lu3 77.39(17) . . ?
C22 C45 Lu3 66.54(15) . . ?
C44 C45 Lu3 90.38(15) . . ?
C46 C45 Lu10 80.7(2) . . ?
C22 C45 Lu10 87.3(6) . . ?
C44 C45 Lu10 65.8(4) . . ?
Lu3 C45 Lu10 26.1(5) . . ?
C46 C45 Lu12 60.6(3) . . ?
C22 C45 Lu12 81.7(3) . . ?
C44 C45 Lu12 91.6(4) . . ?
Lu3 C45 Lu12 18.0(3) . . ?
Lu10 C45 Lu12 27.1(4) . . ?
C45 C46 C24 115.8 . . ?
C45 C46 C47 138.6 . . ?
C24 C46 C47 101.6 . . ?
C45 C46 Lu12 91.5(4) . . ?
C24 C46 Lu12 82.6(4) . . ?
C47 C46 Lu12 75.7(4) . . ?
C45 C46 Lu3 72.63(14) . . ?
C24 C46 Lu3 85.11(15) . . ?
C47 C46 Lu3 94.65(13) . . ?
Lu12 C46 Lu3 20.1(4) . . ?
C45 C46 Lu10 71.4(3) . . ?
C24 C46 Lu10 108.3(5) . . ?
C47 C46 Lu10 80.8(5) . . ?
Lu12 C46 Lu10 27.7(5) . . ?
Lu3 C46 Lu10 25.1(5) . . ?
C48 C47 C46 125.9 . . ?
C48 C47 C68 120.0 . . ?
C46 C47 C68 108.4 . . ?
C48 C47 Lu12 90.9(4) . . ?
C46 C47 Lu12 66.1(3) . . ?
C68 C47 Lu12 89.0(4) . . ?
C48 C47 Lu10 111.7(3) . . ?
C46 C47 Lu10 66.1(5) . . ?
C68 C47 Lu10 66.4(5) . . ?
Lu12 C47 Lu10 25.4(6) . . ?
C48 C47 Lu3 102.93(12) . . ?
C46 C47 Lu3 53.94(9) . . ?
C68 C47 Lu3 88.23(12) . . ?
Lu12 C47 Lu3 13.4(4) . . ?
Lu10 C47 Lu3 21.9(5) . . ?
C47 C48 C49 123.3 . . ?
C47 C48 C71 131.8 . . ?
C49 C48 C71 98.0 . . ?
C47 C48 Lu12 60.6(3) . . ?
C49 C48 Lu12 87.6(3) . . ?
C71 C48 Lu12 102.0(3) . . ?
C48 C49 C25 112.6 . . ?
C48 C49 C50 129.5 . . ?
C25 C49 C50 107.0 . . ?
C48 C49 Lu11 93.6(5) . . ?
C25 C49 Lu11 62.9(4) . . ?
C50 C49 Lu11 77.6(5) . . ?
C48 C49 Lu12 65.0(3) . . ?
C25 C49 Lu12 65.8(3) . . ?
C50 C49 Lu12 107.1(3) . . ?
Lu11 C49 Lu12 32.2(6) . . ?
C51 C50 C27 124.1 . . ?
C51 C50 C49 116.5 . . ?
C27 C50 C49 107.3 . . ?
C51 C50 Lu11 96.2(3) . . ?
C27 C50 Lu11 65.9(5) . . ?
C49 C50 Lu11 71.6(5) . . ?
C50 C51 C72 122.3 . . ?
C50 C51 C52 114.1 . . ?
C72 C51 C52 113.9 . . ?
C29 C52 C53 124.2 . . ?
C29 C52 C51 118.2 . . ?
C53 C52 C51 104.9 . . ?
C73 C53 C52 104.6 . . ?
C73 C53 C54 126.0 . . ?
C52 C53 C54 120.4 . . ?
C31 C54 C55 125.8 . . ?
C31 C54 C53 117.1 . . ?
C55 C54 C53 111.3 . . ?
C31 C54 Lu13 61.7(3) . . ?
C55 C54 Lu13 78.9(3) . . ?
C53 C54 Lu13 111.9(2) . . ?
C31 C54 Lu9 78.8(5) . . ?
C55 C54 Lu9 57.1(5) . . ?
C53 C54 Lu9 118.2(3) . . ?
Lu13 C54 Lu9 21.9(4) . . ?
C54 C55 C75 123.8 . . ?
C54 C55 C56 114.0 . . ?
C75 C55 C56 118.8 . . ?
C54 C55 Lu9 92.0(4) . . ?
C75 C55 Lu9 102.7(5) . . ?
C56 C55 Lu9 55.1(3) . . ?
C54 C55 Lu7 113.12(18) . . ?
C75 C55 Lu7 54.4(3) . . ?
C56 C55 Lu7 87.0(3) . . ?
Lu9 C55 Lu7 48.5(6) . . ?
C54 C55 Lu13 70.6(3) . . ?
C75 C55 Lu13 113.15(18) . . ?
C56 C55 Lu13 67.9(3) . . ?
Lu9 C55 Lu13 21.4(4) . . ?
Lu7 C55 Lu13 60.3(3) . . ?
C54 C55 Lu15 110.1(5) . . ?
C75 C55 Lu15 88.2(5) . . ?
C56 C55 Lu15 52.7(4) . . ?
Lu9 C55 Lu15 18.7(6) . . ?
Lu7 C55 Lu15 37.5(5) . . ?
Lu13 C55 Lu15 39.7(5) . . ?
C57 C56 C33 117.8 . . ?
C57 C56 C55 121.2 . . ?
C33 C56 C55 116.5 . . ?
C57 C56 Lu9 91.1(3) . . ?
C33 C56 Lu9 72.4(7) . . ?
C55 C56 Lu9 85.1(4) . . ?
C57 C56 Lu15 66.3(6) . . ?
C33 C56 Lu15 88.3(6) . . ?
C55 C56 Lu15 95.0(6) . . ?
Lu9 C56 Lu15 25.1(6) . . ?
C57 C56 Lu13 110.6(3) . . ?
C33 C56 Lu13 59.2(2) . . ?
C55 C56 Lu13 79.8(3) . . ?
Lu9 C56 Lu13 20.2(5) . . ?
Lu15 C56 Lu13 45.2(6) . . ?
C57 C56 Lu7 75.82(9) . . ?
C33 C56 Lu7 116.2(2) . . ?
C55 C56 Lu7 61.41(10) . . ?
Lu9 C56 Lu7 44.2(8) . . ?
Lu15 C56 Lu7 37.1(6) . . ?
Lu13 C56 Lu7 58.0(3) . . ?
C56 C57 C77 124.3 . . ?
C56 C57 C58 111.9 . . ?
C77 C57 C58 115.2 . . ?
C56 C57 Lu15 78.0(7) . . ?
C77 C57 Lu15 87.2(6) . . ?
C58 C57 Lu15 74.7(7) . . ?
C56 C57 Lu9 54.5(2) . . ?
C77 C57 Lu9 103.4(5) . . ?
C58 C57 Lu9 83.5(4) . . ?
Lu15 C57 Lu9 23.7(7) . . ?
C56 C57 Lu5 101.50(15) . . ?
C77 C57 Lu5 67.60(17) . . ?
C58 C57 Lu5 72.37(19) . . ?
Lu15 C57 Lu5 24.6(7) . . ?
Lu9 C57 Lu5 48.2(3) . . ?
C56 C57 Lu7 77.26(17) . . ?
C77 C57 Lu7 60.5(2) . . ?
C58 C57 Lu7 109.31(17) . . ?
Lu15 C57 Lu7 37.1(7) . . ?
Lu9 C57 Lu7 44.0(6) . . ?
Lu5 C57 Lu7 38.8(2) . . ?
C57 C58 C35 140.5 . . ?
C57 C58 C59 98.0 . . ?
C35 C58 C59 108.4 . . ?
C57 C58 Lu15 65.9(7) . . ?
C35 C58 Lu15 87.8(7) . . ?
C59 C58 Lu15 83.9(7) . . ?
C57 C58 Lu9 63.1(5) . . ?
C35 C58 Lu9 81.8(5) . . ?
C59 C58 Lu9 104.3(4) . . ?
Lu15 C58 Lu9 20.5(6) . . ?
C57 C58 Lu5 76.2(2) . . ?
C35 C58 Lu5 93.28(19) . . ?
C59 C58 Lu5 57.85(16) . . ?
Lu15 C58 Lu5 26.2(7) . . ?
Lu9 C58 Lu5 46.6(4) . . ?
C60 C59 C78 122.1 . . ?
C60 C59 C58 117.6 . . ?
C78 C59 C58 109.9 . . ?
C60 C59 Lu5 80.0(2) . . ?
C78 C59 Lu5 74.6(2) . . ?
C58 C59 Lu5 83.1(2) . . ?
C60 C59 Lu15 96.2(6) . . ?
C78 C59 Lu15 83.4(6) . . ?
C58 C59 Lu15 56.6(5) . . ?
Lu5 C59 Lu15 26.7(5) . . ?
C60 C59 Lu2 80.88(6) . . ?
C78 C59 Lu2 61.3 . . ?
C58 C59 Lu2 97.55(6) . . ?
Lu5 C59 Lu2 16.88(18) . . ?
Lu15 C59 Lu2 41.3(5) . . ?
C37 C60 C59 119.1 . . ?
C37 C60 C61 119.4 . . ?
C59 C60 C61 116.9 . . ?
C37 C60 Lu5 97.67(18) . . ?
C59 C60 Lu5 65.30(19) . . ?
C61 C60 Lu5 85.64(19) . . ?
C37 C60 Lu2 109.9 . . ?
C59 C60 Lu2 69.5 . . ?
C61 C60 Lu2 70.42(5) . . ?
Lu5 C60 Lu2 16.33(17) . . ?
C80 C61 C62 123.5 . . ?
C80 C61 C60 115.3 . . ?
C62 C61 C60 110.4 . . ?
C80 C61 Lu2 61.6 . . ?
C62 C61 Lu2 101.4 . . ?
C60 C61 Lu2 75.94(5) . . ?
C80 C61 Lu5 76.40(18) . . ?
C62 C61 Lu5 100.98(15) . . ?
C60 C61 Lu5 59.67(15) . . ?
Lu2 C61 Lu5 17.20(15) . . ?
C61 C62 C39 130.3 . . ?
C61 C62 C63 113.5 . . ?
C39 C62 C63 107.8 . . ?
C61 C62 Lu14 81.6(7) . . ?
C39 C62 Lu14 98.5(5) . . ?
C63 C62 Lu14 57.9(5) . . ?
C64 C63 C41 117.1 . . ?
C64 C63 C62 128.0 . . ?
C41 C63 C62 102.9 . . ?
C64 C63 Lu14 62.8(6) . . ?
C41 C63 Lu14 86.9(7) . . ?
C62 C63 Lu14 89.3(6) . . ?
C63 C64 C65 126.4 . . ?
C63 C64 C81 115.5 . . ?
C65 C64 C81 110.4 . . ?
C63 C64 Lu14 82.0(7) . . ?
C65 C64 Lu14 83.6(7) . . ?
C81 C64 Lu14 76.3(9) . . ?
C66 C65 C64 122.1 . . ?
C66 C65 C43 113.6 . . ?
C64 C65 C43 114.6 . . ?
C66 C65 Lu14 88.8(6) . . ?
C64 C65 Lu14 61.4(5) . . ?
C43 C65 Lu14 90.1(7) . . ?
C66 C65 Lu10 68.0(4) . . ?
C64 C65 Lu10 105.2(3) . . ?
C43 C65 Lu10 66.4(4) . . ?
Lu14 C65 Lu10 44.1(6) . . ?
C83 C66 C65 134.7 . . ?
C83 C66 C67 107.1 . . ?
C65 C66 C67 110.5 . . ?
C83 C66 Lu10 94.2(4) . . ?
C65 C66 Lu10 85.0(3) . . ?
C67 C66 Lu10 57.9(3) . . ?
C83 C66 Lu14 85.5(7) . . ?
C65 C66 Lu14 62.9(5) . . ?
C67 C66 Lu14 101.6(5) . . ?
Lu10 C66 Lu14 44.0(5) . . ?
C83 C66 Lu8 53.94(17) . . ?
C65 C66 Lu8 106.06(12) . . ?
C67 C66 Lu8 83.68(16) . . ?
Lu10 C66 Lu8 41.5(4) . . ?
Lu14 C66 Lu8 43.3(5) . . ?
C44 C67 C66 107.3 . . ?
C44 C67 C68 121.2 . . ?
C66 C67 C68 121.3 . . ?
C44 C67 Lu10 68.8(5) . . ?
C66 C67 Lu10 90.3(3) . . ?
C68 C67 Lu10 79.2(3) . . ?
C67 C68 C47 115.9 . . ?
C67 C68 C69 124.9 . . ?
C47 C68 C69 111.7 . . ?
C67 C68 Lu10 65.3(2) . . ?
C47 C68 Lu10 78.4(3) . . ?
C69 C68 Lu10 100.0(4) . . ?
C67 C68 Lu12 86.9(4) . . ?
C47 C68 Lu12 56.5(3) . . ?
C69 C68 Lu12 97.4(3) . . ?
Lu10 C68 Lu12 24.5(4) . . ?
C67 C68 Lu8 86.61(13) . . ?
C47 C68 Lu8 102.00(12) . . ?
C69 C68 Lu8 57.17(17) . . ?
Lu10 C68 Lu8 43.7(5) . . ?
Lu12 C68 Lu8 51.4(3) . . ?
C84 C69 C70 126.0 . . ?
C84 C69 C68 105.7 . . ?
C70 C69 C68 119.9 . . ?
C84 C69 Lu8 61.17(14) . . ?
C70 C69 Lu8 90.53(19) . . ?
C68 C69 Lu8 89.3(3) . . ?
C69 C70 C71 123.8 . . ?
C69 C70 C86 88.4 . . ?
C71 C70 C86 135.7 . . ?
C69 C70 C72 155.6 . . ?
C71 C70 C72 38.8 . . ?
C86 C70 C72 99.6 . . ?
C69 C70 Lu8 59.3(2) . . ?
C71 C70 Lu8 109.35(16) . . ?
C86 C70 Lu8 58.4(2) . . ?
C72 C70 Lu8 105.50(17) . . ?
C72 C71 C70 93.8 . . ?
C72 C71 C48 143.7 . . ?
C70 C71 C48 112.2 . . ?
C71 C72 C51 107.3 . . ?
C71 C72 C73 140.6 . . ?
C51 C72 C73 98.3 . . ?
C71 C72 C70 47.3 . . ?
C51 C72 C70 148.9 . . ?
C73 C72 C70 97.1 . . ?
C53 C73 C74 119.7 . . ?
C53 C73 C72 118.2 . . ?
C74 C73 C72 114.6 . . ?
C86 C74 C75 122.3 . . ?
C86 C74 C73 115.5 . . ?
C75 C74 C73 115.6 . . ?
C86 C74 Lu7 86.2(4) . . ?
C75 C74 Lu7 52.2(3) . . ?
C73 C74 Lu7 109.9(2) . . ?
C86 C74 Lu8 52.90(18) . . ?
C75 C74 Lu8 85.7(2) . . ?
C73 C74 Lu8 109.71(15) . . ?
Lu7 C74 Lu8 35.8(4) . . ?
C74 C75 C55 123.2 . . ?
C74 C75 C76 114.2 . . ?
C55 C75 C76 118.0 . . ?
C74 C75 Lu7 93.8(4) . . ?
C55 C75 Lu7 89.8(4) . . ?
C76 C75 Lu7 64.2(2) . . ?
C74 C75 Lu9 117.7(2) . . ?
C55 C75 Lu9 48.9(3) . . ?
C76 C75 Lu9 85.8(2) . . ?
Lu7 C75 Lu9 41.1(5) . . ?
C87 C76 C77 120.2 . . ?
C87 C76 C75 120.0 . . ?
C77 C76 C75 115.4 . . ?
C87 C76 Lu7 88.2(5) . . ?
C77 C76 Lu7 90.8(4) . . ?
C75 C76 Lu7 70.09(17) . . ?
C87 C76 Lu2 73.48(5) . . ?
C77 C76 Lu2 69.72(6) . . ?
C75 C76 Lu2 108.10(5) . . ?
Lu7 C76 Lu2 38.38(10) . . ?
C87 C76 Lu15 110.7(4) . . ?
C77 C76 Lu15 56.8(4) . . ?
C75 C76 Lu15 82.0(5) . . ?
Lu7 C76 Lu15 34.7(5) . . ?
Lu2 C76 Lu15 38.2(5) . . ?
C87 C76 Lu5 89.81(15) . . ?
C77 C76 Lu5 58.30(12) . . ?
C75 C76 Lu5 101.38(14) . . ?
Lu7 C76 Lu5 37.42(19) . . ?
Lu2 C76 Lu5 16.39(14) . . ?
Lu15 C76 Lu5 23.2(5) . . ?
C87 C76 Lu8 54.86(15) . . ?
C77 C76 Lu8 113.18(12) . . ?
C75 C76 Lu8 84.39(9) . . ?
Lu7 C76 Lu8 34.3(5) . . ?
Lu2 C76 Lu8 43.87(10) . . ?
Lu15 C76 Lu8 65.3(4) . . ?
Lu5 C76 Lu8 55.29(17) . . ?
C57 C77 C78 111.7 . . ?
C57 C77 C76 121.8 . . ?
C78 C77 C76 117.3 . . ?
C57 C77 Lu15 58.3(5) . . ?
C78 C77 Lu15 89.3(7) . . ?
C76 C77 Lu15 92.6(5) . . ?
C57 C77 Lu7 90.2(4) . . ?
C78 C77 Lu7 101.06(18) . . ?
C76 C77 Lu7 52.3(3) . . ?
Lu15 C77 Lu7 41.0(6) . . ?
C57 C77 Lu5 81.75(18) . . ?
C78 C77 Lu5 65.47(18) . . ?
C76 C77 Lu5 91.58(18) . . ?
Lu15 C77 Lu5 27.5(6) . . ?
Lu7 C77 Lu5 43.3(2) . . ?
C57 C77 Lu2 99.6 . . ?
C78 C77 Lu2 61.94(6) . . ?
C76 C77 Lu2 78.65(6) . . ?
Lu15 C77 Lu2 42.7(5) . . ?
Lu7 C77 Lu2 39.43(15) . . ?
Lu5 C77 Lu2 18.37(17) . . ?
C57 C77 Lu9 49.7(3) . . ?
C78 C77 Lu9 105.47(19) . . ?
C76 C77 Lu9 87.6(3) . . ?
Lu15 C77 Lu9 16.4(7) . . ?
Lu7 C77 Lu9 41.4(5) . . ?
Lu5 C77 Lu9 43.3(3) . . ?
Lu2 C77 Lu9 56.5(3) . . ?
C79 C78 C59 122.5 . . ?
C79 C78 C77 123.2 . . ?
C59 C78 C77 105.0 . . ?
C79 C78 Lu5 89.69(19) . . ?
C59 C78 Lu5 69.0(2) . . ?
C77 C78 Lu5 79.3(2) . . ?
C79 C78 Lu2 70.56(6) . . ?
C59 C78 Lu2 86.40(6) . . ?
C77 C78 Lu2 84.46(7) . . ?
Lu5 C78 Lu2 20.57(17) . . ?
C79 C78 Lu15 111.3(4) . . ?
C59 C78 Lu15 66.5(5) . . ?
C77 C78 Lu15 59.4(6) . . ?
Lu5 C78 Lu15 23.9(5) . . ?
Lu2 C78 Lu15 40.8(4) . . ?
C78 C79 C88 118.2 . . ?
C78 C79 C80 113.8 . . ?
C88 C79 C80 112.3 . . ?
C78 C79 Lu2 73.72(6) . . ?
C88 C79 Lu2 80.85(7) . . ?
C80 C79 Lu2 75.17(7) . . ?
C78 C79 Lu5 58.65(15) . . ?
C88 C79 Lu5 94.79(18) . . ?
C80 C79 Lu5 77.8(2) . . ?
Lu2 C79 Lu5 16.62(13) . . ?
C61 C80 C79 128.7 . . ?
C61 C80 C81 126.6 . . ?
C79 C80 C81 97.6 . . ?
C61 C80 Lu2 89.70(6) . . ?
C79 C80 Lu2 67.94(5) . . ?
C81 C80 Lu2 84.48(6) . . ?
C61 C80 Lu14 87.3(6) . . ?
C79 C80 Lu14 98.4(6) . . ?
C81 C80 Lu14 57.5(4) . . ?
Lu2 C80 Lu14 37.8(5) . . ?
C61 C80 Lu5 76.61(19) . . ?
C79 C80 Lu5 70.90(18) . . ?
C81 C80 Lu5 99.75(14) . . ?
Lu2 C80 Lu5 16.06(15) . . ?
Lu14 C80 Lu5 47.8(5) . . ?
C82 C81 C64 122.8 . . ?
C82 C81 C80 115.5 . . ?
C64 C81 C80 112.4 . . ?
C82 C81 Lu14 87.3(7) . . ?
C64 C81 Lu14 66.2(7) . . ?
C80 C81 Lu14 86.5(7) . . ?
C82 C81 Lu2 78.06(6) . . ?
C64 C81 Lu2 101.8 . . ?
C80 C81 Lu2 59.57(6) . . ?
Lu14 C81 Lu2 38.0(7) . . ?
C81 C82 C88 102.6 . . ?
C81 C82 C83 121.4 . . ?
C88 C82 C83 130.8 . . ?
C81 C82 Lu14 61.3(5) . . ?
C88 C82 Lu14 98.3(6) . . ?
C83 C82 Lu14 85.6(6) . . ?
C81 C82 Lu8 108.13(15) . . ?
C88 C82 Lu8 82.0(3) . . ?
C83 C82 Lu8 65.0(2) . . ?
Lu14 C82 Lu8 47.3(5) . . ?
C81 C82 Lu2 73.20(6) . . ?
C88 C82 Lu2 62.2 . . ?
C83 C82 Lu2 108.09(5) . . ?
Lu14 C82 Lu2 36.1(6) . . ?
Lu8 C82 Lu2 45.77(19) . . ?
C66 C83 C84 137.5 . . ?
C66 C83 C82 107.9 . . ?
C84 C83 C82 105.5 . . ?
C66 C83 Lu8 101.6(2) . . ?
C84 C83 Lu8 59.51(15) . . ?
C82 C83 Lu8 80.0(2) . . ?
C66 C83 Lu14 69.5(6) . . ?
C84 C83 Lu14 104.6(4) . . ?
C82 C83 Lu14 63.0(6) . . ?
Lu8 C83 Lu14 45.1(4) . . ?
C69 C84 C85 104.8 . . ?
C69 C84 C83 122.9 . . ?
C85 C84 C83 124.3 . . ?
C69 C84 Lu8 86.05(16) . . ?
C85 C84 Lu8 71.2(3) . . ?
C83 C84 Lu8 84.3(2) . . ?
C84 C85 C86 102.1 . . ?
C84 C85 C87 129.6 . . ?
C86 C85 C87 116.5 . . ?
C84 C85 Lu8 70.4(3) . . ?
C86 C85 Lu8 82.34(11) . . ?
C87 C85 Lu8 83.4(3) . . ?
C84 C85 Lu7 108.5(2) . . ?
C86 C85 Lu7 75.75(7) . . ?
C87 C85 Lu7 56.51(16) . . ?
Lu8 C85 Lu7 38.2(4) . . ?
C74 C86 C85 123.9 . . ?
C74 C86 C70 113.2 . . ?
C85 C86 C70 118.5 . . ?
C74 C86 Lu8 99.8(3) . . ?
C85 C86 Lu8 61.98(14) . . ?
C70 C86 Lu8 89.1(3) . . ?
C74 C86 Lu7 64.6(2) . . ?
C85 C86 Lu7 75.17(18) . . ?
C70 C86 Lu7 114.71(19) . . ?
Lu8 C86 Lu7 37.9(4) . . ?
C76 C87 C85 122.4 . . ?
C76 C87 C88 120.9 . . ?
C85 C87 C88 112.7 . . ?
C76 C87 Lu7 55.4(3) . . ?
C85 C87 Lu7 92.8(3) . . ?
C88 C87 Lu7 104.98(13) . . ?
C76 C87 Lu8 97.2(2) . . ?
C85 C87 Lu8 60.73(18) . . ?
C88 C87 Lu8 91.41(13) . . ?
Lu7 C87 Lu8 42.6(4) . . ?
C76 C87 Lu2 76.92(6) . . ?
C85 C87 Lu2 109.09(5) . . ?
C88 C87 Lu2 66.02(6) . . ?
Lu7 C87 Lu2 39.02(10) . . ?
Lu8 C87 Lu2 48.83(15) . . ?
C79 C88 C87 119.9 . . ?
C79 C88 C82 111.2 . . ?
C87 C88 C82 113.4 . . ?
C79 C88 Lu2 64.66(6) . . ?
C87 C88 Lu2 81.10(7) . . ?
C82 C88 Lu2 85.22(5) . . ?
C79 C88 Lu8 110.76(15) . . ?
C87 C88 Lu8 57.59(19) . . ?
C82 C88 Lu8 66.5(2) . . ?
Lu2 C88 Lu8 46.12(16) . . ?
N3A Ni1A N3A 177.52(17) . 6 ?
N3A Ni1A N4A 90.18(9) . . ?
N3A Ni1A N4A 90.17(9) 6 . ?
N3A Ni1A N2A 89.80(9) . . ?
N3A Ni1A N2A 89.80(9) 6 . ?
N4A Ni1A N2A 178.78(17) . . ?
C2A C1A C18A 113.8(3) . . ?
C13A N2A C13A 104.2(4) . 6 ?
C13A N2A Ni1A 127.9(2) . . ?
C13A N2A Ni1A 127.9(2) 6 . ?
C2A C2A C15A 106.5(2) 6 . ?
C2A C2A C1A 129.2(2) 6 . ?
C15A C2A C1A 124.2(4) . . ?
C11A N3A C4A 104.4(3) . . ?
C11A N3A Ni1A 128.1(2) . . ?
C4A N3A Ni1A 127.6(2) . . ?
C4A C3A C15A 124.2(3) . . ?
C3A C4A N3A 125.3(3) . . ?
C3A C4A C5A 123.5(3) . . ?
N3A C4A C5A 111.2(3) . . ?
C15A N4A C15A 104.3(4) 6 . ?
C15A N4A Ni1A 127.9(2) 6 . ?
C15A N4A Ni1A 127.9(2) . . ?
C8A C5A C4A 106.5(3) . . ?
C8A C5A C6A 128.4(4) . . ?
C4A C5A C6A 125.1(3) . . ?
C5A C6A C7A 112.8(3) . . ?
C5A C8A C11A 106.1(3) . . ?
C5A C8A C9A 128.3(3) . . ?
C11A C8A C9A 125.6(3) . . ?
C8A C9A C10A 112.6(4) . . ?
N3A C11A C12A 125.0(3) . . ?
N3A C11A C8A 111.8(3) . . ?
C12A C11A C8A 123.2(3) . . ?
C13A C12A C11A 124.4(3) . . ?
C12A C13A N2A 124.9(3) . . ?
C12A C13A C14A 123.7(3) . . ?
N2A C13A C14A 111.5(3) . . ?
C14A C14A C13A 106.4(2) 6 . ?
C14A C14A C16A 128.5(2) 6 . ?
C13A C14A C16A 125.1(3) . . ?
C3A C15A N4A 124.9(3) . . ?
C3A C15A C2A 123.8(3) . . ?
N4A C15A C2A 111.3(3) . . ?
C14A C16A C17A 112.9(3) . . ?
C2B C1B C2B 121.5(11) . 6 ?
C1B C2B C3B 119.9(8) . . ?
C2B C3B C4B 121.1(9) . . ?
C3B C4B C3B 116.4(12) . 6 ?
C2C C3C C3C 118.9(5) . 2_656 ?
C2C C4C C4C 125.2(6) . 2_656 ?
C4C C2C C3C 115.9(8) . . ?

_refine_diff_density_max         1.079
_refine_diff_density_min         -1.056
_refine_diff_density_rms         0.095



_vrf_PLAT307_Lu2@C1-C88          
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2@C1-C88          
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Lu2@Cs15-C86
_database_code_depnum_ccdc_archive 'CCDC 1582219'
_audit_update_record             
;
2017-10-26 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'Lu2@Cs(15)-C86 Ni(OEP)'
_chemical_name_common            'Lu2@Cs(15)-C86 Ni(OEP)'
_chemical_melting_point          ?
_chemical_formula_moiety         'Lu2 C86, C36 H44 N4 Ni, 2(C6 H6) '
_chemical_formula_sum            'C134 H56 Lu2 N4 Ni'
_chemical_formula_weight         2130.47

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.4720 5.8584 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           12
_space_group_name_H-M_alt        'C 2/m'
_space_group_name_Hall           '-C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'

_cell_length_a                   24.149(5)
_cell_length_b                   18.020(5)
_cell_length_c                   18.486(5)
_cell_angle_alpha                90
_cell_angle_beta                 90.220(5)
_cell_angle_gamma                90
_cell_volume                     8044(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9777
_cell_measurement_theta_min      2.978
_cell_measurement_theta_max      25.485

_exptl_crystal_description       Block
_exptl_crystal_colour            Black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.759
_exptl_crystal_F_000             4232
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.180
_exptl_crystal_size_mid          0.120
_exptl_crystal_size_min          0.100
_exptl_absorpt_coefficient_mu    2.736
_shelx_estimated_absorpt_T_min   0.681
_shelx_estimated_absorpt_T_max   0.761
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.6470
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71069
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean 8.3
_diffrn_reflns_number            38173
_diffrn_reflns_av_unetI/netI     0.0208
_diffrn_reflns_av_R_equivalents  0.0258
_diffrn_reflns_limit_h_min       -29
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_theta_min         2.979
_diffrn_reflns_theta_max         25.479
_diffrn_reflns_theta_full        25.240
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             7675
_reflns_number_gt                6457
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1417P)²+43.7460P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         7675
_refine_ls_number_parameters     866
_refine_ls_number_restraints     883
_refine_ls_R_factor_all          0.0907
_refine_ls_R_factor_gt           0.0787
_refine_ls_wR_factor_ref         0.2352
_refine_ls_wR_factor_gt          0.2200
_refine_ls_goodness_of_fit_ref   1.022
_refine_ls_restrained_S_all      1.090
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Lu1 Lu 0.16622(6) 0.5000 0.17050(9) 0.0714(6) Uani 0.2083 2 d S TU P A 1
Lu2 Lu 0.26754(11) 0.54897(16) 0.28439(12) 0.0692(8) Uani 0.1479 1 d . U P A 1
Lu3 Lu 0.33186(13) 0.5000 0.1713(3) 0.1204(18) Uani 0.1445 2 d S TU P A 1
Lu4 Lu 0.31880(7) 0.44539(11) 0.19414(9) 0.0449(4) Uani 0.1344 1 d . U P A 1
Lu5 Lu 0.2376(5) 0.4597(5) 0.0973(3) 0.173(4) Uani 0.1129 1 d . U P A 1
Lu6 Lu 0.2802(5) 0.4191(5) 0.2486(6) 0.232(5) Uani 0.1051 1 d . U P A 1
Lu7 Lu 0.20860(18) 0.4209(3) 0.1366(3) 0.0633(9) Uani 0.0865 1 d . U P A 1
Lu8 Lu 0.1916(3) 0.4245(4) 0.1817(5) 0.109(2) Uani 0.071 1 d . U P A 1
Lu9 Lu 0.2465(2) 0.5269(4) 0.0827(3) 0.0520(11) Uani 0.0689 1 d . U P A 1
Lu10 Lu 0.2420(4) 0.4796(5) 0.2955(3) 0.100(4) Uani 0.0529 1 d . U P A 1
Lu11 Lu 0.1902(4) 0.5373(8) 0.1291(7) 0.117(4) Uani 0.044 1 d . U P A 1
C1 C 0.30831(17) 0.27257(19) 0.2295(2) 0.109(5) Uani 0.5 1 d G U P A -1
C2 C 0.31516(17) 0.3100(2) 0.2999(2) 0.115(5) Uani 0.5 1 d G U P A -1
C3 C 0.27230(18) 0.3202(2) 0.3382(2) 0.113(6) Uani 0.5 1 d G U P A -1
C4 C 0.22428(18) 0.2904(2) 0.3055(2) 0.130(6) Uani 0.5 1 d G U P A -1
C5 C 0.25261(18) 0.25871(17) 0.2421(2) 0.131(6) Uani 0.5 1 d G U P A -1
C6 C 0.22638(18) 0.25739(18) 0.1964(3) 0.123(6) Uani 0.5 1 d G U P A -1
C7 C 0.24210(18) 0.2702(2) 0.1203(2) 0.115(6) Uani 0.5 1 d G U P A -1
C8 C 0.31435(17) 0.2931(2) 0.0995(2) 0.131(6) Uani 0.5 1 d G U P A -1
C9 C 0.34496(16) 0.2913(2) 0.1682(3) 0.129(7) Uani 0.5 1 d G U P A -1
C10 C 0.38686(12) 0.3509(2) 0.1667(2) 0.117(6) Uani 0.5 1 d G U P A -1
C11 C 0.39237(11) 0.3892(2) 0.2403(2) 0.116(6) Uani 0.5 1 d G U P A -1
C12 C 0.35435(14) 0.3702(2) 0.3004(2) 0.110(6) Uani 0.5 1 d G U P A -1
C13 C 0.34396(14) 0.4352(2) 0.34947(16) 0.110(5) Uani 0.5 1 d G U P A -1
C14 C 0.29871(17) 0.4443(3) 0.39589(12) 0.134(7) Uani 0.5 1 d G U P A -1
C15 C 0.26040(18) 0.3761(2) 0.38551(15) 0.122(6) Uani 0.5 1 d G U P A -1
C16 C 0.21216(18) 0.4109(3) 0.40113(14) 0.101(5) Uani 0.5 1 d G U P A -1
C17 C 0.16730(16) 0.3840(2) 0.35935(18) 0.113(5) Uani 0.5 1 d G U P A -1
C18 C 0.17515(17) 0.3234(2) 0.3151(2) 0.123(6) Uani 0.5 1 d G U P A -1
C19 C 0.14276(15) 0.3183(2) 0.2418(2) 0.117(6) Uani 0.5 1 d G U P A -1
C20 C 0.16901(16) 0.2833(2) 0.1789(2) 0.095(5) Uani 0.5 1 d G U P A -1
C21 C 0.16062(15) 0.3164(2) 0.1100(2) 0.091(4) Uani 0.5 1 d G U P A -1
C22 C 0.21397(17) 0.3103(2) 0.0607(2) 0.097(5) Uani 0.5 1 d G U P A -1
C23 C 0.23069(17) 0.3624(3) 0.02058(16) 0.112(5) Uani 0.5 1 d G U P A -1
C24 C 0.29608(17) 0.3933(3) 0.00696(15) 0.152(7) Uani 0.5 1 d G U P A -1
C25 C 0.33887(16) 0.3495(3) 0.0510(2) 0.137(6) Uani 0.5 1 d G U P A -1
C26 C 0.38763(13) 0.3780(3) 0.0919(2) 0.163(8) Uani 0.5 1 d G U P A -1
C27 C 0.40488(12) 0.4552(3) 0.0770(2) 0.139(7) Uani 0.5 1 d G U P A -1
C28 C 0.42020(9) 0.4798(3) 0.1396(2) 0.106(6) Uani 0.5 1 d G U P A -1
C29 C 0.41364(8) 0.4595(3) 0.2102(2) 0.109(5) Uani 0.5 1 d G U P A -1
C30 C 0.40238(9) 0.5203(3) 0.2633(2) 0.121(6) Uani 0.5 1 d G U P A -1
C31 C 0.35185(14) 0.5763(2) 0.33529(18) 0.122(6) Uani 0.5 1 d G U P A -1
C32 C 0.37001(12) 0.5014(2) 0.32428(18) 0.090(4) Uani 0.5 1 d G U P A -1
C33 C 0.30661(17) 0.5885(2) 0.37872(15) 0.114(5) Uani 0.5 1 d G U P A -1
C34 C 0.27905(18) 0.5180(3) 0.40946(11) 0.092(5) Uani 0.5 1 d G U P A -1
C35 C 0.22596(18) 0.5396(3) 0.41475(11) 0.115(6) Uani 0.5 1 d G U P A -1
C36 C 0.18376(18) 0.4724(3) 0.40607(13) 0.102(5) Uani 0.5 1 d G U P A -1
C37 C 0.13610(15) 0.4837(3) 0.37047(18) 0.105(5) Uani 0.5 1 d G U P A -1
C38 C 0.12403(14) 0.4124(3) 0.3310(2) 0.125(6) Uani 0.5 1 d G U P A -1
C39 C 0.09416(11) 0.4427(3) 0.2835(2) 0.111(6) Uani 0.5 1 d G U P A -1
C40 C 0.10304(11) 0.3773(3) 0.2311(2) 0.101(5) Uani 0.5 1 d G U P A -1
C41 C 0.09605(10) 0.4084(3) 0.1577(2) 0.097(5) Uani 0.5 1 d G U P A -1
C42 C 0.12870(13) 0.3801(3) 0.0992(2) 0.092(5) Uani 0.5 1 d G U P A -1
C43 C 0.14572(14) 0.4379(3) 0.04496(18) 0.109(5) Uani 0.5 1 d G U P A -1
C44 C 0.22427(18) 0.4903(3) -0.02232(10) 0.124(5) Uani 0.5 1 d G U P A -1
C45 C 0.19457(17) 0.4264(3) 0.00568(14) 0.120(6) Uani 0.5 1 d G U P A -1
C46 C 0.28178(19) 0.5210(3) -0.02919(11) 0.128(6) Uani 0.5 1 d G U P A -1
C47 C 0.32104(18) 0.4662(3) -0.01609(13) 0.134(7) Uani 0.5 1 d G U P A -1
C48 C 0.37270(15) 0.4932(3) 0.02019(18) 0.152(6) Uani 0.5 1 d G U P A -1
C49 C 0.36235(16) 0.5596(3) 0.02450(18) 0.134(7) Uani 0.5 1 d G U P A -1
C50 C 0.39020(13) 0.5860(3) 0.0766(2) 0.116(6) Uani 0.5 1 d G U P A -1
C51 C 0.41245(10) 0.5670(3) 0.1308(2) 0.112(6) Uani 0.5 1 d G U P A -1
C52 C 0.41162(9) 0.5777(3) 0.2051(2) 0.127(6) Uani 0.5 1 d G U P A -1
C53 C 0.38445(12) 0.6370(2) 0.2266(2) 0.136(6) Uani 0.5 1 d G U P A -1
C54 C 0.35864(14) 0.6453(2) 0.2880(2) 0.095(5) Uani 0.5 1 d G U P A -1
C55 C 0.32600(16) 0.6953(2) 0.2680(2) 0.125(6) Uani 0.5 1 d G U P A -1
C56 C 0.26252(18) 0.71018(19) 0.3005(2) 0.132(6) Uani 0.5 1 d G U P A -1
C57 C 0.25931(18) 0.6596(2) 0.35855(19) 0.134(7) Uani 0.5 1 d G U P A -1
C58 C 0.20894(18) 0.6276(2) 0.37790(17) 0.120(6) Uani 0.5 1 d G U P A -1
C59 C 0.15666(16) 0.6406(2) 0.3433(2) 0.098(5) Uani 0.5 1 d G U P A -1
C60 C 0.11989(14) 0.5616(3) 0.3408(2) 0.103(5) Uani 0.5 1 d G U P A -1
C61 C 0.09134(10) 0.5741(3) 0.2636(2) 0.099(5) Uani 0.5 1 d G U P A -1
C62 C 0.07944(8) 0.4883(3) 0.2402(2) 0.102(4) Uani 0.5 1 d G U P A -1
C63 C 0.08060(8) 0.4751(3) 0.1701(2) 0.100(5) Uani 0.5 1 d G U P A -1
C64 C 0.09404(10) 0.5326(3) 0.1156(2) 0.112(5) Uani 0.5 1 d G U P A -1
C65 C 0.12553(13) 0.5105(3) 0.05366(19) 0.106(4) Uani 0.5 1 d G U P A -1
C66 C 0.15281(16) 0.5737(3) 0.02310(18) 0.152(7) Uani 0.5 1 d G U P A -1
C67 C 0.20405(18) 0.5637(3) -0.01206(13) 0.155(7) Uani 0.5 1 d G U P A -1
C68 C 0.24272(19) 0.6218(3) -0.00385(16) 0.141(6) Uani 0.5 1 d G U P A -1
C69 C 0.29417(19) 0.6291(3) 0.00096(17) 0.141(6) Uani 0.5 1 d G U P A -1
C70 C 0.31503(18) 0.5789(3) -0.00988(15) 0.126(6) Uani 0.5 1 d G U P A -1
C71 C 0.31318(18) 0.6737(3) 0.0535(2) 0.135(6) Uani 0.5 1 d G U P A -1
C72 C 0.36266(15) 0.6502(3) 0.0908(2) 0.141(7) Uani 0.5 1 d G U P A -1
C73 C 0.36584(15) 0.6777(2) 0.1570(2) 0.119(6) Uani 0.5 1 d G U P A -1
C74 C 0.31817(17) 0.72050(19) 0.1940(3) 0.122(6) Uani 0.5 1 d G U P A -1
C75 C 0.27022(18) 0.73915(18) 0.1640(3) 0.106(5) Uani 0.5 1 d G U P A -1
C76 C 0.20517(18) 0.73662(19) 0.1864(3) 0.131(6) Uani 0.5 1 d G U P A -1
C77 C 0.21108(18) 0.72577(19) 0.2632(2) 0.105(5) Uani 0.5 1 d G U P A -1
C78 C 0.16115(17) 0.6931(2) 0.2871(2) 0.110(6) Uani 0.5 1 d G U P A -1
C79 C 0.12739(14) 0.6761(2) 0.2259(3) 0.116(6) Uani 0.5 1 d G U P A -1
C80 C 0.10361(12) 0.6268(3) 0.2073(3) 0.118(6) Uani 0.5 1 d G U P A -1
C81 C 0.10436(12) 0.6096(3) 0.1371(2) 0.117(6) Uani 0.5 1 d G U P A -1
C82 C 0.14752(16) 0.6365(3) 0.0677(2) 0.154(7) Uani 0.5 1 d G U P A -1
C83 C 0.18691(17) 0.6867(2) 0.0878(2) 0.168(8) Uani 0.5 1 d G U P A -1
C84 C 0.23676(18) 0.6779(3) 0.0487(2) 0.149(6) Uani 0.5 1 d G U P A -1
C85 C 0.27110(19) 0.7138(2) 0.0898(2) 0.113(6) Uani 0.5 1 d G U P A -1
C86 C 0.15552(16) 0.7018(2) 0.1619(3) 0.144(7) Uani 0.5 1 d G U P A -1
Ni1A Ni 0.46792(2) 0.5000 0.41606(3) 0.0203(2) Uani 1 2 d S T P B 2
N1A N 0.51798(17) 0.5000 0.3324(2) 0.0243(9) Uani 1 2 d S T P B 2
N2A N 0.46649(11) 0.39139(17) 0.41482(15) 0.0226(6) Uani 1 1 d . . . B 2
N3A N 0.41630(17) 0.5000 0.4977(2) 0.0237(9) Uani 1 2 d S T P B 2
C1A C 0.5632(2) 0.3782(3) 0.1286(3) 0.0523(12) Uani 1 1 d . . . B 2
H1AA H 0.5494 0.4177 0.0988 0.078 Uiso 1 1 calc R U . B 2
H1AB H 0.5328 0.3537 0.1519 0.078 Uiso 1 1 calc R U . B 2
H1AC H 0.5828 0.3432 0.0991 0.078 Uiso 1 1 calc R U . B 2
C2A C 0.60243(18) 0.4099(3) 0.1860(2) 0.0396(10) Uani 1 1 d . . . B 2
H2AA H 0.6184 0.3693 0.2135 0.048 Uiso 1 1 calc R U . B 2
H2AB H 0.6325 0.4357 0.1620 0.048 Uiso 1 1 calc R U . B 2
C3A C 0.57427(15) 0.4624(2) 0.2370(2) 0.0304(8) Uani 1 1 d . . . B 2
C4A C 0.53916(14) 0.4397(2) 0.29650(19) 0.0260(7) Uani 1 1 d . . . B 2
C5A C 0.52815(15) 0.3668(2) 0.3127(2) 0.0281(8) Uani 1 1 d . . . B 2
H5A H 0.5451 0.3302 0.2850 0.034 Uiso 1 1 calc R U . B 2
C6A C 0.49350(14) 0.3446(2) 0.36756(19) 0.0246(7) Uani 1 1 d . . . B 2
C7A C 0.48070(15) 0.2679(2) 0.3827(2) 0.0284(8) Uani 1 1 d . . . B 2
C8A C 0.50120(17) 0.2033(2) 0.3396(2) 0.0358(9) Uani 1 1 d . . . B 2
H8AA H 0.4996 0.1589 0.3693 0.043 Uiso 1 1 calc R U . B 2
H8AB H 0.5396 0.2117 0.3270 0.043 Uiso 1 1 calc R U . B 2
C9A C 0.4679(2) 0.1905(3) 0.2709(3) 0.0539(13) Uani 1 1 d . . . B 2
H9AA H 0.4725 0.2321 0.2390 0.081 Uiso 1 1 calc R U . B 2
H9AB H 0.4294 0.1851 0.2828 0.081 Uiso 1 1 calc R U . B 2
H9AC H 0.4807 0.1462 0.2474 0.081 Uiso 1 1 calc R U . B 2
C10A C 0.44621(15) 0.2680(2) 0.4408(2) 0.0275(8) Uani 1 1 d . . . B 2
C11A C 0.42010(16) 0.2031(2) 0.4779(2) 0.0342(9) Uani 1 1 d . . . B 2
H11A H 0.4192 0.2123 0.5296 0.041 Uiso 1 1 calc R U . B 2
H11B H 0.4426 0.1593 0.4698 0.041 Uiso 1 1 calc R U . B 2
C12A C 0.3611(2) 0.1883(3) 0.4507(3) 0.0564(13) Uani 1 1 d . . . B 2
H12A H 0.3618 0.1791 0.3996 0.085 Uiso 1 1 calc R U . B 2
H12B H 0.3383 0.2308 0.4604 0.085 Uiso 1 1 calc R U . B 2
H12C H 0.3462 0.1458 0.4752 0.085 Uiso 1 1 calc R U . B 2
C13A C 0.43785(14) 0.3449(2) 0.45959(19) 0.0246(7) Uani 1 1 d . . . B 2
C14A C 0.40410(14) 0.3669(2) 0.51553(19) 0.0260(7) Uani 1 1 d . . . B 2
H14A H 0.3876 0.3303 0.5436 0.031 Uiso 1 1 calc R U . B 2
C15A C 0.39336(14) 0.4399(2) 0.53227(19) 0.0240(7) Uani 1 1 d . . . B 2
C16A C 0.35593(14) 0.4623(2) 0.58871(19) 0.0263(7) Uani 1 1 d . . . B 2
C17A C 0.32251(16) 0.4106(2) 0.6345(2) 0.0319(8) Uani 1 1 d . . . B 2
H17A H 0.3134 0.4353 0.6795 0.038 Uiso 1 1 calc R U . B 2
H17B H 0.3449 0.3675 0.6462 0.038 Uiso 1 1 calc R U . B 2
C18A C 0.26936(19) 0.3849(3) 0.5982(3) 0.0502(12) Uani 1 1 d . . . B 2
H18A H 0.2465 0.4271 0.5875 0.075 Uiso 1 1 calc R U . B 2
H18B H 0.2499 0.3520 0.6301 0.075 Uiso 1 1 calc R U . B 2
H18C H 0.2781 0.3593 0.5542 0.075 Uiso 1 1 calc R U . B 2
C1B C 0.3805(8) 0.0000 0.1774(9) 0.190(12) Uani 1 2 d DS T P C 3
H1BA H 0.4177 0.0000 0.1644 0.229 Uiso 1 2 calc R U P C 3
C2B C 0.3472(6) 0.0692(6) 0.1891(8) 0.161(6) Uani 1 1 d D . . C 3
H2B H 0.3642 0.1153 0.1850 0.193 Uiso 1 1 calc R U . C 3
C3B C 0.2944(5) 0.0653(5) 0.2050(5) 0.103(3) Uani 1 1 d . . . C 3
H3B H 0.2735 0.1077 0.2140 0.124 Uiso 1 1 calc R U . C 3
C4B C 0.2728(7) 0.0000 0.2074(6) 0.113(5) Uani 1 2 d S T P C 3
H4B H 0.2345 0.0000 0.2118 0.136 Uiso 1 2 calc R U P C 3
C1C C 0.4816(4) 0.2391(7) 0.0285(7) 0.136(4) Uani 1 1 d . . . D 4
H1C H 0.4711 0.2853 0.0462 0.163 Uiso 1 1 calc R U . D 4
C2C C 0.4610(3) 0.1848(6) 0.0584(4) 0.090(2) Uani 1 1 d . . . D 4
H2C H 0.4351 0.1888 0.0953 0.108 Uiso 1 1 calc R U . D 4
C3C C 0.4800(4) 0.1162(7) 0.0321(7) 0.149(5) Uani 1 1 d . . . D 4
H3C H 0.4685 0.0720 0.0530 0.179 Uiso 1 1 calc R U . D 4


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Lu1 Lu11 1.174(10) . ?
Lu1 Lu11 1.174(10) 6_565 ?
Lu1 Lu8 1.506(9) . ?
Lu1 Lu8 1.506(9) 6_565 ?
Lu1 Lu7 1.864(5) . ?
Lu1 Lu7 1.864(5) 6_565 ?
Lu1 C64 2.098(2) . ?
Lu1 C63 2.116(2) . ?
Lu1 Lu5 2.312(10) 6_565 ?
Lu1 Lu5 2.313(10) . ?
Lu1 C41 2.377(3) . ?
Lu1 C65 2.377(3) . ?
Lu2 Lu10 0.830(6) 6_565 ?
Lu2 Lu6 0.929(13) 6_565 ?
Lu2 Lu10 1.409(10) . ?
Lu2 Lu2 1.765(6) 6_565 ?
Lu2 Lu4 2.084(3) 6_565 ?
Lu2 C33 2.104(3) . ?
Lu2 C31 2.293(3) . ?
Lu2 C34 2.394(3) . ?
Lu2 C57 2.428(4) . ?
Lu2 Lu6 2.452(12) . ?
Lu2 C35 2.620(4) . ?
Lu2 C58 2.649(3) . ?
Lu3 Lu4 1.116(3) 6_565 ?
Lu3 Lu4 1.116(3) . ?
Lu3 C29 2.222(4) . ?
Lu3 C28 2.244(4) . ?
Lu3 Lu6 2.395(13) . ?
Lu3 Lu6 2.395(13) 6_565 ?
Lu3 C51 2.412(4) . ?
Lu3 C30 2.430(5) . ?
Lu3 C52 2.459(4) . ?
Lu3 C27 2.613(5) . ?
Lu3 Lu9 2.673(7) 6_565 ?
Lu3 Lu9 2.673(7) . ?
Lu4 Lu6 1.455(14) . ?
Lu4 Lu4 1.968(4) 6_565 ?
Lu4 Lu2 2.084(3) 6_565 ?
Lu4 C11 2.213(3) . ?
Lu4 C29 2.322(3) . ?
Lu4 C10 2.422(3) . ?
Lu4 C12 2.534(3) . ?
Lu4 Lu5 2.662(9) . ?
Lu4 Lu10 2.712(7) . ?
Lu4 C28 2.723(3) . ?
Lu4 C30 2.741(3) . ?
Lu5 Lu9 0.422(13) 6_565 ?
Lu5 Lu7 1.230(10) . ?
Lu5 Lu9 1.259(8) . ?
Lu5 Lu11 1.290(13) 6_565 ?
Lu5 Lu5 1.452(19) 6_565 ?
Lu5 Lu11 1.901(16) . ?
Lu5 Lu8 2.021(11) . ?
Lu5 C45 2.073(7) . ?
Lu5 C23 2.262(8) . ?
Lu5 C44 2.301(7) . ?
Lu5 Lu7 2.377(10) 6_565 ?
Lu6 Lu2 0.929(13) 6_565 ?
Lu6 Lu10 1.672(14) . ?
Lu6 C12 2.212(9) . ?
Lu6 Lu10 2.222(15) 6_565 ?
Lu6 C2 2.340(8) . ?
Lu6 C13 2.432(9) . ?
Lu6 C3 2.440(10) . ?
Lu6 Lu8 2.468(11) . ?
Lu6 C15 2.691(13) . ?
Lu7 Lu11 0.885(11) 6_565 ?
Lu7 Lu8 0.933(9) . ?
Lu7 Lu9 1.651(8) 6_565 ?
Lu7 Lu11 2.149(17) . ?
Lu7 C42 2.176(4) . ?
Lu7 C21 2.264(5) . ?
Lu7 C43 2.292(5) . ?
Lu7 Lu9 2.343(8) . ?
Lu7 Lu5 2.377(10) 6_565 ?
Lu7 C22 2.441(5) . ?
Lu8 Lu11 1.192(17) 6_565 ?
Lu8 Lu11 2.254(12) . ?
Lu8 C42 2.292(6) . ?
Lu8 C41 2.366(6) . ?
Lu8 Lu9 2.428(10) 6_565 ?
Lu8 C21 2.471(8) . ?
Lu8 C40 2.479(7) . ?
Lu8 C19 2.509(6) . ?
Lu9 Lu5 0.422(13) 6_565 ?
Lu9 Lu9 0.970(13) 6_565 ?
Lu9 Lu11 1.621(16) . ?
Lu9 Lu7 1.651(8) 6_565 ?
Lu9 Lu11 1.983(19) 6_565 ?
Lu9 C44 2.117(6) . ?
Lu9 C67 2.131(6) . ?
Lu9 C46 2.242(6) . ?
Lu9 C68 2.342(7) . ?
Lu9 Lu8 2.428(10) 6_565 ?
Lu10 Lu10 0.735(18) 6_565 ?
Lu10 Lu2 0.830(6) 6_565 ?
Lu10 Lu6 2.222(15) 6_565 ?
Lu10 C34 2.388(8) . ?
Lu10 C14 2.388(7) . ?
Lu10 C16 2.424(7) . ?
Lu10 C35 2.486(7) . ?
Lu10 C36 2.489(7) . ?
Lu10 C15 2.537(7) . ?
Lu11 Lu7 0.885(11) 6_565 ?
Lu11 Lu8 1.192(17) 6_565 ?
Lu11 Lu5 1.290(13) 6_565 ?
Lu11 Lu11 1.34(3) 6_565 ?
Lu11 Lu9 1.983(19) 6_565 ?
Lu11 C65 2.145(9) . ?
Lu11 C66 2.251(8) . ?
C1 C5 1.3886 . ?
C1 C2 1.4738 . ?
C1 C9 1.4803 . ?
C2 C3 1.2695 . ?
C2 C12 1.4396 . ?
C3 C15 1.3657 . ?
C3 C4 1.4115 . ?
C4 C18 1.3395 . ?
C4 C5 1.4744 . ?
C5 C6 1.0554 . ?
C6 C7 1.4757 . ?
C6 C20 1.4963 . ?
C7 C22 1.4813 . ?
C7 C8 1.8354 . ?
C8 C9 1.4675 . ?
C8 C25 1.4796 . ?
C9 C10 1.4750 . ?
C10 C26 1.4675 . ?
C10 C11 1.5315 . ?
C11 C29 1.4753 . ?
C11 C12 1.4849 . ?
C12 C13 1.5032 . ?
C13 C14 1.4016 . ?
C13 C32 1.4273 . ?
C14 C34 1.4334 . ?
C14 C15 1.5490 . ?
C15 C16 1.3544 . ?
C16 C36 1.3072 . ?
C16 C17 1.4133 . ?
C17 C38 1.2734 . ?
C17 C18 1.3780 . ?
C17 C36 1.8540 . ?
C17 C37 1.9582 . ?
C18 C19 1.5646 . ?
C19 C40 1.4439 . ?
C19 C20 1.4696 . ?
C20 C21 1.4206 . ?
C21 C42 1.3960 . ?
C21 C22 1.5845 . ?
C22 C23 1.2622 . ?
C23 C45 1.4727 . ?
C23 C24 1.6943 . ?
C24 C47 1.5075 . ?
C24 C25 1.5318 . ?
C25 C26 1.4881 . ?
C26 C27 1.4767 . ?
C27 C28 1.2928 . ?
C27 C48 1.4729 . ?
C28 C29 1.3665 . ?
C28 C51 1.5908 . ?
C29 C30 1.4969 . ?
C30 C32 1.4155 . ?
C30 C52 1.5101 . ?
C31 C33 1.3761 . ?
C31 C32 1.4341 . ?
C31 C54 1.5305 . ?
C33 C34 1.5433 . ?
C33 C57 1.7553 . ?
C34 C35 1.3432 . ?
C35 C36 1.5899 . ?
C35 C58 1.7749 . ?
C36 C37 1.3392 . ?
C37 C38 1.5050 . ?
C37 C60 1.5572 . ?
C37 C39 2.0357 . ?
C38 C39 1.2602 . ?
C38 C40 2.0158 . ?
C39 C62 1.1994 . ?
C39 C40 1.5414 . ?
C40 C41 1.4768 . ?
C41 C63 1.2799 . ?
C41 C42 1.4344 . ?
C42 C43 1.5048 . ?
C43 C45 1.4030 . ?
C43 C65 1.4050 . ?
C44 C67 1.4217 . ?
C44 C45 1.4525 . ?
C44 C46 1.5007 . ?
C46 C70 1.3630 . ?
C46 C47 1.3897 . ?
C47 C48 1.4959 . ?
C47 C70 2.0391 . ?
C48 C49 1.2247 . ?
C48 C50 2.0151 . ?
C49 C50 1.2663 . ?
C49 C70 1.3506 . ?
C50 C51 1.1854 . ?
C50 C72 1.3604 . ?
C51 C52 1.3854 . ?
C52 C53 1.3168 . ?
C53 C54 1.3049 . ?
C53 C73 1.5471 . ?
C53 C55 1.9213 . ?
C54 C55 1.2515 . ?
C55 C74 1.4530 . ?
C55 C56 1.6704 . ?
C56 C57 1.4100 . ?
C56 C77 1.4469 . ?
C57 C58 1.3936 . ?
C58 C59 1.4323 . ?
C59 C78 1.4088 . ?
C59 C60 1.6791 . ?
C60 C61 1.5981 . ?
C61 C80 1.4399 . ?
C61 C62 1.6301 . ?
C62 C63 1.3183 . ?
C63 C64 1.4821 . ?
C64 C65 1.4333 . ?
C64 C81 1.4639 . ?
C65 C66 1.4322 . ?
C66 C82 1.4062 . ?
C66 C67 1.4116 . ?
C67 C68 1.4108 . ?
C68 C69 1.2523 . ?
C68 C84 1.4104 . ?
C68 C70 1.9133 . ?
C69 C70 1.0556 . ?
C69 C71 1.3405 . ?
C69 C84 1.8664 . ?
C71 C85 1.4182 . ?
C71 C72 1.4402 . ?
C71 C84 1.8490 . ?
C72 C73 1.3218 . ?
C73 C74 1.5475 . ?
C74 C75 1.3253 . ?
C75 C85 1.4457 . ?
C75 C76 1.6265 . ?
C76 C86 1.4255 . ?
C76 C77 1.4394 . ?
C77 C78 1.4145 . ?
C78 C79 1.4249 . ?
C79 C80 1.1114 . ?
C79 C86 1.4427 . ?
C80 C81 1.3353 . ?
C80 C86 2.0272 . ?
C81 C82 1.7261 . ?
C82 C83 1.3634 . ?
C83 C84 1.4160 . ?
C83 C86 1.5915 . ?
C84 C85 1.2961 . ?
Ni1A N2A 1.958(3) . ?
Ni1A N2A 1.958(3) 6_565 ?
Ni1A N3A 1.962(4) . ?
Ni1A N1A 1.966(4) . ?
N1A C4A 1.374(4) . ?
N1A C4A 1.374(4) 6_565 ?
N2A C13A 1.367(5) . ?
N2A C6A 1.380(5) . ?
N3A C15A 1.375(4) . ?
N3A C15A 1.375(4) 6_565 ?
C1A C2A 1.530(7) . ?
C1A H1AA 0.9600 . ?
C1A H1AB 0.9600 . ?
C1A H1AC 0.9600 . ?
C2A C3A 1.501(5) . ?
C2A H2AA 0.9700 . ?
C2A H2AB 0.9700 . ?
C3A C3A 1.354(8) 6_565 ?
C3A C4A 1.451(5) . ?
C4A C5A 1.374(5) . ?
C5A C6A 1.376(5) . ?
C5A H5A 0.9300 . ?
C6A C7A 1.445(5) . ?
C7A C10A 1.361(6) . ?
C7A C8A 1.496(5) . ?
C8A C9A 1.519(6) . ?
C8A H8AA 0.9700 . ?
C8A H8AB 0.9700 . ?
C9A H9AA 0.9600 . ?
C9A H9AB 0.9600 . ?
C9A H9AC 0.9600 . ?
C10A C13A 1.444(5) . ?
C10A C11A 1.497(5) . ?
C11A C12A 1.533(6) . ?
C11A H11A 0.9700 . ?
C11A H11B 0.9700 . ?
C12A H12A 0.9600 . ?
C12A H12B 0.9600 . ?
C12A H12C 0.9600 . ?
C13A C14A 1.377(5) . ?
C14A C15A 1.375(5) . ?
C14A H14A 0.9300 . ?
C15A C16A 1.441(5) . ?
C16A C16A 1.358(8) 6_565 ?
C16A C17A 1.497(5) . ?
C17A C18A 1.518(6) . ?
C17A H17A 0.9700 . ?
C17A H17B 0.9700 . ?
C18A H18A 0.9600 . ?
C18A H18B 0.9600 . ?
C18A H18C 0.9600 . ?
C1B C2B 1.500(14) 6 ?
C1B C2B 1.500(14) . ?
C1B H1BA 0.9300 . ?
C2B C3B 1.312(16) . ?
C2B H2B 0.9300 . ?
C3B C4B 1.288(11) . ?
C3B H3B 0.9300 . ?
C4B C3B 1.288(11) 6 ?
C4B H4B 0.9300 . ?
C1C C2C 1.230(14) . ?
C1C C1C 1.38(2) 2_655 ?
C1C H1C 0.9300 . ?
C2C C3C 1.406(15) . ?
C2C H2C 0.9300 . ?
C3C C3C 1.53(3) 2_655 ?
C3C H3C 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu11 Lu1 Lu11 69.9(18) . 6_565 ?
Lu11 Lu1 Lu8 113.9(8) . . ?
Lu11 Lu1 Lu8 51.0(8) 6_565 . ?
Lu11 Lu1 Lu8 51.0(8) . 6_565 ?
Lu11 Lu1 Lu8 113.9(8) 6_565 6_565 ?
Lu8 Lu1 Lu8 129.2(3) . 6_565 ?
Lu11 Lu1 Lu7 86.9(9) . . ?
Lu11 Lu1 Lu7 21.6(8) 6_565 . ?
Lu8 Lu1 Lu7 29.8(3) . . ?
Lu8 Lu1 Lu7 120.9(3) 6_565 . ?
Lu11 Lu1 Lu7 21.6(8) . 6_565 ?
Lu11 Lu1 Lu7 86.9(9) 6_565 6_565 ?
Lu8 Lu1 Lu7 120.9(3) . 6_565 ?
Lu8 Lu1 Lu7 29.8(3) 6_565 6_565 ?
Lu7 Lu1 Lu7 99.7(3) . 6_565 ?
Lu11 Lu1 C64 86.3(4) . . ?
Lu11 Lu1 C64 104.8(4) 6_565 . ?
Lu8 Lu1 C64 131.0(2) . . ?
Lu8 Lu1 C64 98.7(2) 6_565 . ?
Lu7 Lu1 C64 120.53(19) . . ?
Lu7 Lu1 C64 94.58(17) 6_565 . ?
Lu11 Lu1 C63 127.2(4) . . ?
Lu11 Lu1 C63 111.2(5) 6_565 . ?
Lu8 Lu1 C63 101.9(2) . . ?
Lu8 Lu1 C63 126.1(3) 6_565 . ?
Lu7 Lu1 C63 112.00(18) . . ?
Lu7 Lu1 C63 134.33(18) 6_565 . ?
C64 Lu1 C63 41.2 . . ?
Lu11 Lu1 Lu5 21.2(7) . 6_565 ?
Lu11 Lu1 Lu5 55.0(8) 6_565 6_565 ?
Lu8 Lu1 Lu5 93.4(4) . 6_565 ?
Lu8 Lu1 Lu5 59.5(4) 6_565 6_565 ?
Lu7 Lu1 Lu5 68.4(3) . 6_565 ?
Lu7 Lu1 Lu5 32.0(3) 6_565 6_565 ?
C64 Lu1 Lu5 104.4(2) . 6_565 ?
C63 Lu1 Lu5 142.7(2) . 6_565 ?
Lu11 Lu1 Lu5 55.0(8) . . ?
Lu11 Lu1 Lu5 21.2(7) 6_565 . ?
Lu8 Lu1 Lu5 59.5(4) . . ?
Lu8 Lu1 Lu5 93.4(4) 6_565 . ?
Lu7 Lu1 Lu5 32.0(3) . . ?
Lu7 Lu1 Lu5 68.4(3) 6_565 . ?
C64 Lu1 Lu5 115.2(2) . . ?
C63 Lu1 Lu5 131.5(2) . . ?
Lu5 Lu1 Lu5 36.6(5) 6_565 . ?
Lu11 Lu1 C41 133.4(6) . . ?
Lu11 Lu1 C41 83.7(7) 6_565 . ?
Lu8 Lu1 C41 71.1(2) . . ?
Lu8 Lu1 C41 158.5(2) 6_565 . ?
Lu7 Lu1 C41 80.08(16) . . ?
Lu7 Lu1 C41 152.9(2) 6_565 . ?
C64 Lu1 C41 63.62(7) . . ?
C63 Lu1 C41 32.4 . . ?
Lu5 Lu1 C41 133.9(2) 6_565 . ?
Lu5 Lu1 C41 104.9(3) . . ?
Lu11 Lu1 C65 64.2(5) . . ?
Lu11 Lu1 C65 69.9(5) 6_565 . ?
Lu8 Lu1 C65 111.3(3) . . ?
Lu8 Lu1 C65 102.7(3) 6_565 . ?
Lu7 Lu1 C65 88.9(2) . . ?
Lu7 Lu1 C65 81.94(19) 6_565 . ?
C64 Lu1 C65 36.7 . . ?
C63 Lu1 C65 67.25(7) . . ?
Lu5 Lu1 C65 75.5(2) 6_565 . ?
Lu5 Lu1 C65 78.5(2) . . ?
C41 Lu1 C65 70.91(8) . . ?
Lu10 Lu2 Lu6 143.8(9) 6_565 6_565 ?
Lu10 Lu2 Lu10 24.1(7) 6_565 . ?
Lu6 Lu2 Lu10 143.0(6) 6_565 . ?
Lu10 Lu2 Lu2 51.6(7) 6_565 6_565 ?
Lu6 Lu2 Lu2 128.3(7) 6_565 6_565 ?
Lu10 Lu2 Lu2 27.5(3) . 6_565 ?
Lu10 Lu2 Lu4 132.3(5) 6_565 6_565 ?
Lu6 Lu2 Lu4 37.1(8) 6_565 6_565 ?
Lu10 Lu2 Lu4 114.9(3) . 6_565 ?
Lu2 Lu2 Lu4 92.79(10) 6_565 6_565 ?
Lu10 Lu2 C33 109.6(5) 6_565 . ?
Lu6 Lu2 C33 103.5(6) 6_565 . ?
Lu10 Lu2 C33 112.0(4) . . ?
Lu2 Lu2 C33 109.79(15) 6_565 . ?
Lu4 Lu2 C33 112.42(19) 6_565 . ?
Lu10 Lu2 C31 133.7(7) 6_565 . ?
Lu6 Lu2 C31 82.3(6) 6_565 . ?
Lu10 Lu2 C31 121.2(4) . . ?
Lu2 Lu2 C31 102.38(13) 6_565 . ?
Lu4 Lu2 C31 77.81(15) 6_565 . ?
C33 Lu2 C31 36.16(5) . . ?
Lu10 Lu2 C34 72.5(6) 6_565 . ?
Lu6 Lu2 C34 142.7(6) 6_565 . ?
Lu10 Lu2 C34 72.6(3) . . ?
Lu2 Lu2 C34 76.52(13) 6_565 . ?
Lu4 Lu2 C34 135.86(15) 6_565 . ?
C33 Lu2 C34 39.48(5) . . ?
C31 Lu2 C34 63.51(7) . . ?
Lu10 Lu2 C57 107.9(6) 6_565 . ?
Lu6 Lu2 C57 85.5(7) 6_565 . ?
Lu10 Lu2 C57 127.5(3) . . ?
Lu2 Lu2 C57 145.19(13) 6_565 . ?
Lu4 Lu2 C57 117.5(2) 6_565 . ?
C33 Lu2 C57 44.88(7) . . ?
C31 Lu2 C57 70.53(10) . . ?
C34 Lu2 C57 69.84(8) . . ?
Lu10 Lu2 Lu6 64.4(7) 6_565 . ?
Lu6 Lu2 Lu6 111.0(10) 6_565 . ?
Lu10 Lu2 Lu6 41.2(4) . . ?
Lu2 Lu2 Lu6 17.3(3) 6_565 . ?
Lu4 Lu2 Lu6 75.9(4) 6_565 . ?
C33 Lu2 Lu6 119.4(2) . . ?
C31 Lu2 Lu6 101.8(3) . . ?
C34 Lu2 Lu6 91.4(2) . . ?
C57 Lu2 Lu6 161.2(3) . . ?
Lu10 Lu2 C35 56.2(5) 6_565 . ?
Lu6 Lu2 C35 145.4(7) 6_565 . ?
Lu10 Lu2 C35 68.8(3) . . ?
Lu2 Lu2 C35 86.29(12) 6_565 . ?
Lu4 Lu2 C35 166.08(15) 6_565 . ?
C33 Lu2 C35 55.36(7) . . ?
C31 Lu2 C35 88.81(9) . . ?
C34 Lu2 C35 30.7 . . ?
C57 Lu2 C35 60.08(7) . . ?
Lu6 Lu2 C35 103.6(3) . . ?
Lu10 Lu2 C58 76.8(6) 6_565 . ?
Lu6 Lu2 C58 108.1(8) 6_565 . ?
Lu10 Lu2 C58 98.3(3) . . ?
Lu2 Lu2 C58 122.35(13) 6_565 . ?
Lu4 Lu2 C58 144.77(19) 6_565 . ?
C33 Lu2 C58 61.12(8) . . ?
C31 Lu2 C58 95.35(10) . . ?
C34 Lu2 C58 63.56(7) . . ?
C57 Lu2 C58 31.5 . . ?
Lu6 Lu2 C58 139.0(4) . . ?
C35 Lu2 C58 39.4 . . ?
Lu4 Lu3 Lu4 123.6(5) 6_565 . ?
Lu4 Lu3 C29 114.8(3) 6_565 . ?
Lu4 Lu3 C29 80.8(2) . . ?
Lu4 Lu3 C28 120.8(2) 6_565 . ?
Lu4 Lu3 C28 103.1(2) . . ?
C29 Lu3 C28 35.62(6) . . ?
Lu4 Lu3 Lu6 99.4(4) 6_565 . ?
Lu4 Lu3 Lu6 24.5(3) . . ?
C29 Lu3 Lu6 94.1(3) . . ?
C28 Lu3 Lu6 123.7(3) . . ?
Lu4 Lu3 Lu6 24.5(3) 6_565 6_565 ?
Lu4 Lu3 Lu6 99.4(4) . 6_565 ?
C29 Lu3 Lu6 118.1(3) . 6_565 ?
C28 Lu3 Lu6 138.8(3) . 6_565 ?
Lu6 Lu3 Lu6 75.0(6) . 6_565 ?
Lu4 Lu3 C51 84.56(18) 6_565 . ?
Lu4 Lu3 C51 142.0(2) . . ?
C29 Lu3 C51 63.13(10) . . ?
C28 Lu3 C51 39.75(7) . . ?
Lu6 Lu3 C51 155.9(3) . . ?
Lu6 Lu3 C51 107.7(3) 6_565 . ?
Lu4 Lu3 C30 78.5(2) 6_565 . ?
Lu4 Lu3 C30 93.8(3) . . ?
C29 Lu3 C30 37.20(7) . . ?
C28 Lu3 C30 62.82(10) . . ?
Lu6 Lu3 C30 92.3(3) . . ?
Lu6 Lu3 C30 81.8(3) 6_565 . ?
C51 Lu3 C30 65.02(9) . . ?
Lu4 Lu3 C52 67.97(18) 6_565 . ?
Lu4 Lu3 C52 128.9(3) . . ?
C29 Lu3 C52 53.90(8) . . ?
C28 Lu3 C52 54.14(8) . . ?
Lu6 Lu3 C52 127.2(3) . . ?
Lu6 Lu3 C52 85.0(3) 6_565 . ?
C51 Lu3 C52 33.0 . . ?
C30 Lu3 C52 35.98(6) . . ?
Lu4 Lu3 C27 135.8(3) 6_565 . ?
Lu4 Lu3 C27 99.9(2) . . ?
C29 Lu3 C27 60.89(10) . . ?
C28 Lu3 C27 29.64(6) . . ?
Lu6 Lu3 C27 124.4(3) . . ?
Lu6 Lu3 C27 160.2(3) 6_565 . ?
C51 Lu3 C27 53.16(9) . . ?
C30 Lu3 C27 92.35(12) . . ?
C52 Lu3 C27 79.36(12) . . ?
Lu4 Lu3 Lu9 100.0(2) 6_565 6_565 ?
Lu4 Lu3 Lu9 81.6(2) . 6_565 ?
C29 Lu3 Lu9 145.2(2) . 6_565 ?
C28 Lu3 Lu9 122.8(3) . 6_565 ?
Lu6 Lu3 Lu9 81.5(3) . 6_565 ?
Lu6 Lu3 Lu9 94.2(3) 6_565 6_565 ?
C51 Lu3 Lu9 121.4(3) . 6_565 ?
C30 Lu3 Lu9 173.4(3) . 6_565 ?
C52 Lu3 Lu9 149.3(2) . 6_565 ?
C27 Lu3 Lu9 93.2(2) . 6_565 ?
Lu4 Lu3 Lu9 81.6(2) 6_565 . ?
Lu4 Lu3 Lu9 100.0(2) . . ?
C29 Lu3 Lu9 160.1(3) . . ?
C28 Lu3 Lu9 126.9(3) . . ?
Lu6 Lu3 Lu9 94.2(3) . . ?
Lu6 Lu3 Lu9 81.5(3) 6_565 . ?
C51 Lu3 Lu9 109.9(2) . . ?
C30 Lu3 Lu9 159.83(19) . . ?
C52 Lu3 Lu9 130.81(19) . . ?
C27 Lu3 Lu9 99.6(2) . . ?
Lu9 Lu3 Lu9 20.9(3) 6_565 . ?
Lu3 Lu4 Lu6 137.0(5) . . ?
Lu3 Lu4 Lu4 28.2(2) . 6_565 ?
Lu6 Lu4 Lu4 109.0(4) . 6_565 ?
Lu3 Lu4 Lu2 115.4(3) . 6_565 ?
Lu6 Lu4 Lu2 22.7(4) . 6_565 ?
Lu4 Lu4 Lu2 87.21(10) 6_565 6_565 ?
Lu3 Lu4 C11 108.7(2) . . ?
Lu6 Lu4 C11 95.8(4) . . ?
Lu4 Lu4 C11 117.21(13) 6_565 . ?
Lu2 Lu4 C11 101.08(15) 6_565 . ?
Lu3 Lu4 C29 70.9(2) . . ?
Lu6 Lu4 C29 125.6(3) . . ?
Lu4 Lu4 C29 83.72(12) 6_565 . ?
Lu2 Lu4 C29 118.73(14) 6_565 . ?
C11 Lu4 C29 37.9 . . ?
Lu3 Lu4 C10 110.4(2) . . ?
Lu6 Lu4 C10 110.7(4) . . ?
Lu4 Lu4 C10 134.69(12) 6_565 . ?
Lu2 Lu4 C10 127.41(16) 6_565 . ?
C11 Lu4 C10 38.3 . . ?
C29 Lu4 C10 55.54(6) . . ?
Lu3 Lu4 C12 132.0(3) . . ?
Lu6 Lu4 C12 60.4(3) . . ?
Lu4 Lu4 C12 122.34(11) 6_565 . ?
Lu2 Lu4 C12 66.78(13) 6_565 . ?
C11 Lu4 C12 35.6 . . ?
C29 Lu4 C12 68.17(7) . . ?
C10 Lu4 C12 63.77(8) . . ?
Lu3 Lu4 Lu5 82.5(3) . . ?
Lu6 Lu4 Lu5 91.4(4) . . ?
Lu4 Lu4 Lu5 84.4(2) 6_565 . ?
Lu2 Lu4 Lu5 95.5(2) 6_565 . ?
C11 Lu4 Lu5 153.1(2) . . ?
C29 Lu4 Lu5 143.0(3) . . ?
C10 Lu4 Lu5 115.2(2) . . ?
C12 Lu4 Lu5 145.0(3) . . ?
Lu3 Lu4 Lu10 104.8(3) . . ?
Lu6 Lu4 Lu10 32.2(5) . . ?
Lu4 Lu4 Lu10 76.9(2) 6_565 . ?
Lu2 Lu4 Lu10 13.08(15) 6_565 . ?
C11 Lu4 Lu10 112.80(19) . . ?
C29 Lu4 Lu10 124.3(2) . . ?
C10 Lu4 Lu10 140.4(2) . . ?
C12 Lu4 Lu10 79.42(17) . . ?
Lu5 Lu4 Lu10 86.5(3) . . ?
Lu3 Lu4 C28 53.4(2) . . ?
Lu6 Lu4 C28 155.6(3) . . ?
Lu4 Lu4 C28 76.83(11) 6_565 . ?
Lu2 Lu4 C28 145.40(13) 6_565 . ?
C11 Lu4 C28 61.65(6) . . ?
C29 Lu4 C28 30.1 . . ?
C10 Lu4 C28 58.06(6) . . ?
C12 Lu4 C28 96.12(8) . . ?
Lu5 Lu4 C28 112.9(2) . . ?
Lu10 Lu4 C28 145.3(2) . . ?
Lu3 Lu4 C30 62.2(2) . . ?
Lu6 Lu4 C30 108.1(4) . . ?
Lu4 Lu4 C30 60.49(9) 6_565 . ?
Lu2 Lu4 C30 92.35(12) 6_565 . ?
C11 Lu4 C30 57.08(6) . . ?
C29 Lu4 C30 33.1 . . ?
C10 Lu4 C30 86.85(8) . . ?
C12 Lu4 C30 69.82(7) . . ?
Lu5 Lu4 C30 143.6(2) . . ?
Lu10 Lu4 C30 94.0(2) . . ?
C28 Lu4 C30 53.07(6) . . ?
Lu9 Lu5 Lu7 175(2) 6_565 . ?
Lu9 Lu5 Lu9 39.2(16) 6_565 . ?
Lu7 Lu5 Lu9 140.5(9) . . ?
Lu9 Lu5 Lu11 136(3) 6_565 6_565 ?
Lu7 Lu5 Lu11 41.0(7) . 6_565 ?
Lu9 Lu5 Lu11 102.1(12) . 6_565 ?
Lu9 Lu5 Lu5 55.2(18) 6_565 6_565 ?
Lu7 Lu5 Lu5 124.7(5) . 6_565 ?
Lu9 Lu5 Lu5 16.0(5) . 6_565 ?
Lu11 Lu5 Lu5 87.6(9) 6_565 6_565 ?
Lu9 Lu5 Lu11 95(2) 6_565 . ?
Lu7 Lu5 Lu11 83.7(6) . . ?
Lu9 Lu5 Lu11 57.5(6) . . ?
Lu11 Lu5 Lu11 45.0(10) 6_565 . ?
Lu5 Lu5 Lu11 42.7(4) 6_565 . ?
Lu9 Lu5 Lu8 163(2) 6_565 . ?
Lu7 Lu5 Lu8 18.0(3) . . ?
Lu9 Lu5 Lu8 124.2(7) . . ?
Lu11 Lu5 Lu8 33.9(7) 6_565 . ?
Lu5 Lu5 Lu8 108.3(4) 6_565 . ?
Lu11 Lu5 Lu8 70.1(4) . . ?
Lu9 Lu5 C45 83.9(15) 6_565 . ?
Lu7 Lu5 C45 91.9(6) . . ?
Lu9 Lu5 C45 100.8(6) . . ?
Lu11 Lu5 C45 86.6(7) 6_565 . ?
Lu5 Lu5 C45 106.8(3) 6_565 . ?
Lu11 Lu5 C45 99.4(6) . . ?
Lu8 Lu5 C45 105.3(5) . . ?
Lu9 Lu5 C23 94.4(16) 6_565 . ?
Lu7 Lu5 C23 83.6(5) . . ?
Lu9 Lu5 C23 128.5(6) . . ?
Lu11 Lu5 C23 104.7(7) 6_565 . ?
Lu5 Lu5 C23 140.9(2) 6_565 . ?
Lu11 Lu5 C23 136.1(6) . . ?
Lu8 Lu5 C23 101.6(5) . . ?
C45 Lu5 C23 39.41(13) . . ?
Lu9 Lu5 C44 46.7(15) 6_565 . ?
Lu7 Lu5 C44 128.8(6) . . ?
Lu9 Lu5 C44 65.5(5) . . ?
Lu11 Lu5 C44 107.8(9) 6_565 . ?
Lu5 Lu5 C44 76.1(3) 6_565 . ?
Lu11 Lu5 C44 92.2(6) . . ?
Lu8 Lu5 C44 137.9(6) . . ?
C45 Lu5 C44 38.34(11) . . ?
C23 Lu5 C44 64.73(15) . . ?
Lu9 Lu5 Lu1 125(2) 6_565 . ?
Lu7 Lu5 Lu1 53.5(4) . . ?
Lu9 Lu5 Lu1 87.3(6) . . ?
Lu11 Lu5 Lu1 19.2(5) 6_565 . ?
Lu5 Lu5 Lu1 71.7(2) 6_565 . ?
Lu11 Lu5 Lu1 30.4(3) . . ?
Lu8 Lu5 Lu1 40.0(3) . . ?
C45 Lu5 Lu1 101.3(5) . . ?
C23 Lu5 Lu1 123.8(5) . . ?
C44 Lu5 Lu1 112.6(4) . . ?
Lu9 Lu5 Lu7 80.3(18) 6_565 6_565 ?
Lu7 Lu5 Lu7 99.5(6) . 6_565 ?
Lu9 Lu5 Lu7 41.1(4) . 6_565 ?
Lu11 Lu5 Lu7 63.9(9) 6_565 6_565 ?
Lu5 Lu5 Lu7 25.2(2) 6_565 6_565 ?
Lu11 Lu5 Lu7 20.2(2) . 6_565 ?
Lu8 Lu5 Lu7 83.4(4) . 6_565 ?
C45 Lu5 Lu7 111.3(5) . 6_565 ?
C23 Lu5 Lu7 150.7(5) . 6_565 ?
C44 Lu5 Lu7 92.1(4) . 6_565 ?
Lu1 Lu5 Lu7 46.8(2) . 6_565 ?
Lu2 Lu6 Lu4 120.2(10) 6_565 . ?
Lu2 Lu6 Lu10 17.0(4) 6_565 . ?
Lu4 Lu6 Lu10 120.1(7) . . ?
Lu2 Lu6 C12 101.9(7) 6_565 . ?
Lu4 Lu6 C12 84.8(6) . . ?
Lu10 Lu6 C12 118.8(6) . . ?
Lu2 Lu6 Lu10 22.5(4) 6_565 6_565 ?
Lu4 Lu6 Lu10 105.7(6) . 6_565 ?
Lu10 Lu6 Lu10 14.5(4) . 6_565 ?
C12 Lu6 Lu10 119.6(5) . 6_565 ?
Lu2 Lu6 C2 110.5(8) 6_565 . ?
Lu4 Lu6 C2 108.8(7) . . ?
Lu10 Lu6 C2 122.5(7) . . ?
C12 Lu6 C2 36.74(13) . . ?
Lu10 Lu6 C2 133.0(6) 6_565 . ?
Lu2 Lu6 Lu3 102.7(8) 6_565 . ?
Lu4 Lu6 Lu3 18.5(2) . . ?
Lu10 Lu6 Lu3 101.6(6) . . ?
C12 Lu6 Lu3 94.5(5) . . ?
Lu10 Lu6 Lu3 87.2(4) 6_565 . ?
C2 Lu6 Lu3 124.4(6) . . ?
Lu2 Lu6 C13 65.7(6) 6_565 . ?
Lu4 Lu6 C13 94.9(5) . . ?
Lu10 Lu6 C13 82.7(6) . . ?
C12 Lu6 C13 37.40(14) . . ?
Lu10 Lu6 C13 82.2(5) 6_565 . ?
C2 Lu6 C13 64.06(19) . . ?
Lu3 Lu6 C13 93.1(4) . . ?
Lu2 Lu6 C3 86.7(8) 6_565 . ?
Lu4 Lu6 C3 139.4(7) . . ?
Lu10 Lu6 C3 94.6(7) . . ?
C12 Lu6 C3 58.67(19) . . ?
Lu10 Lu6 C3 107.5(6) 6_565 . ?
C2 Lu6 C3 30.71(11) . . ?
Lu3 Lu6 C3 153.0(5) . . ?
C13 Lu6 C3 67.5(2) . . ?
Lu2 Lu6 Lu2 34.4(5) 6_565 . ?
Lu4 Lu6 Lu2 87.5(5) . . ?
Lu10 Lu6 Lu2 33.7(4) . . ?
C12 Lu6 Lu2 111.4(4) . . ?
Lu10 Lu6 Lu2 19.7(2) 6_565 . ?
C2 Lu6 Lu2 137.6(5) . . ?
Lu3 Lu6 Lu2 69.2(3) . . ?
C13 Lu6 Lu2 76.0(3) . . ?
C3 Lu6 Lu2 120.2(5) . . ?
Lu2 Lu6 Lu8 92.7(8) 6_565 . ?
Lu4 Lu6 Lu8 101.4(5) . . ?
Lu10 Lu6 Lu8 75.9(5) . . ?
C12 Lu6 Lu8 158.7(5) . . ?
Lu10 Lu6 Lu8 78.7(4) 6_565 . ?
C2 Lu6 Lu8 123.2(5) . . ?
Lu3 Lu6 Lu8 97.5(3) . . ?
C13 Lu6 Lu8 157.6(7) . . ?
C3 Lu6 Lu8 107.4(5) . . ?
Lu2 Lu6 Lu8 89.4(4) . . ?
Lu2 Lu6 C15 56.5(6) 6_565 . ?
Lu4 Lu6 C15 149.4(5) . . ?
Lu10 Lu6 C15 66.4(5) . . ?
C12 Lu6 C15 67.9(2) . . ?
Lu10 Lu6 C15 78.1(5) 6_565 . ?
C2 Lu6 C15 56.1(2) . . ?
Lu3 Lu6 C15 146.1(5) . . ?
C13 Lu6 C15 55.0(2) . . ?
C3 Lu6 C15 30.37(15) . . ?
Lu2 Lu6 C15 89.9(4) . . ?
Lu8 Lu6 C15 109.0(6) . . ?
Lu11 Lu7 Lu8 81.9(11) 6_565 . ?
Lu11 Lu7 Lu5 73.1(11) 6_565 . ?
Lu8 Lu7 Lu5 137.9(7) . . ?
Lu11 Lu7 Lu9 72.5(12) 6_565 6_565 ?
Lu8 Lu7 Lu9 138.4(6) . 6_565 ?
Lu5 Lu7 Lu9 1.2(5) . 6_565 ?
Lu11 Lu7 Lu1 29.2(9) 6_565 . ?
Lu8 Lu7 Lu1 53.3(6) . . ?
Lu5 Lu7 Lu1 94.5(6) . . ?
Lu9 Lu7 Lu1 94.2(3) 6_565 . ?
Lu11 Lu7 Lu11 19.2(7) 6_565 . ?
Lu8 Lu7 Lu11 84.2(7) . . ?
Lu5 Lu7 Lu11 61.6(5) . . ?
Lu9 Lu7 Lu11 61.3(5) 6_565 . ?
Lu1 Lu7 Lu11 33.1(4) . . ?
Lu11 Lu7 C42 78.1(7) 6_565 . ?
Lu8 Lu7 C42 85.1(4) . . ?
Lu5 Lu7 C42 120.7(5) . . ?
Lu9 Lu7 C42 119.6(3) 6_565 . ?
Lu1 Lu7 C42 83.0(2) . . ?
Lu11 Lu7 C42 97.3(3) . . ?
Lu11 Lu7 C21 114.6(7) 6_565 . ?
Lu8 Lu7 C21 91.5(5) . . ?
Lu5 Lu7 C21 129.5(4) . . ?
Lu9 Lu7 C21 128.8(3) 6_565 . ?
Lu1 Lu7 C21 115.3(2) . . ?
Lu11 Lu7 C21 133.8(3) . . ?
C42 Lu7 C21 36.58(7) . . ?
Lu11 Lu7 C43 55.8(6) 6_565 . ?
Lu8 Lu7 C43 111.0(6) . . ?
Lu5 Lu7 C43 82.2(5) . . ?
Lu9 Lu7 C43 81.0(3) 6_565 . ?
Lu1 Lu7 C43 77.5(2) . . ?
Lu11 Lu7 C43 71.6(3) . . ?
C42 Lu7 C43 39.26(8) . . ?
C21 Lu7 C43 67.24(10) . . ?
Lu11 Lu7 Lu9 55.6(11) 6_565 . ?
Lu8 Lu7 Lu9 119.9(6) . . ?
Lu5 Lu7 Lu9 20.0(5) . . ?
Lu9 Lu7 Lu9 19.9(3) 6_565 . ?
Lu1 Lu7 Lu9 74.7(2) . . ?
Lu11 Lu7 Lu9 42.0(4) . . ?
C42 Lu7 Lu9 119.2(3) . . ?
C21 Lu7 Lu9 141.8(3) . . ?
C43 Lu7 Lu9 80.5(3) . . ?
Lu11 Lu7 Lu5 47.9(10) 6_565 6_565 ?
Lu8 Lu7 Lu5 110.0(6) . 6_565 ?
Lu5 Lu7 Lu5 30.1(5) . 6_565 ?
Lu9 Lu7 Lu5 30.1(3) 6_565 6_565 ?
Lu1 Lu7 Lu5 64.8(3) . 6_565 ?
Lu11 Lu7 Lu5 32.6(4) . 6_565 ?
C42 Lu7 Lu5 118.1(4) . 6_565 ?
C21 Lu7 Lu5 146.8(3) . 6_565 ?
C43 Lu7 Lu5 81.3(3) . 6_565 ?
Lu9 Lu7 Lu5 10.2(3) . 6_565 ?
Lu11 Lu7 C22 129.1(7) 6_565 . ?
Lu8 Lu7 C22 126.5(7) . . ?
Lu5 Lu7 C22 95.3(4) . . ?
Lu9 Lu7 C22 95.0(3) 6_565 . ?
Lu1 Lu7 C22 147.9(2) . . ?
Lu11 Lu7 C22 140.4(5) . . ?
C42 Lu7 C22 65.81(10) . . ?
C21 Lu7 C22 39.13(7) . . ?
C43 Lu7 C22 73.76(11) . . ?
Lu9 Lu7 C22 113.5(3) . . ?
Lu5 Lu7 C22 123.1(3) 6_565 . ?
Lu7 Lu8 Lu11 47.3(5) . 6_565 ?
Lu7 Lu8 Lu1 96.9(7) . . ?
Lu11 Lu8 Lu1 49.9(6) 6_565 . ?
Lu7 Lu8 Lu5 24.1(4) . . ?
Lu11 Lu8 Lu5 37.1(6) 6_565 . ?
Lu1 Lu8 Lu5 80.5(4) . . ?
Lu7 Lu8 Lu11 71.5(7) . . ?
Lu11 Lu8 Lu11 29.2(8) 6_565 . ?
Lu1 Lu8 Lu11 28.4(4) . . ?
Lu5 Lu8 Lu11 52.5(4) . . ?
Lu7 Lu8 C42 71.0(4) . . ?
Lu11 Lu8 C42 69.0(6) 6_565 . ?
Lu1 Lu8 C42 87.5(3) . . ?
Lu5 Lu8 C42 87.8(4) . . ?
Lu11 Lu8 C42 91.1(3) . . ?
Lu7 Lu8 C41 104.9(5) . . ?
Lu11 Lu8 C41 83.9(6) 6_565 . ?
Lu1 Lu8 C41 71.9(3) . . ?
Lu5 Lu8 C41 115.7(4) . . ?
Lu11 Lu8 C41 91.0(4) . . ?
C42 Lu8 C41 35.83(8) . . ?
Lu7 Lu8 Lu9 26.8(4) . 6_565 ?
Lu11 Lu8 Lu9 35.9(6) 6_565 6_565 ?
Lu1 Lu8 Lu9 78.1(3) . 6_565 ?
Lu5 Lu8 Lu9 2.9(4) . 6_565 ?
Lu11 Lu8 Lu9 49.9(5) . 6_565 ?
C42 Lu8 Lu9 89.2(3) . 6_565 ?
C41 Lu8 Lu9 116.0(3) . 6_565 ?
Lu7 Lu8 Lu6 93.5(7) . . ?
Lu11 Lu8 Lu6 116.9(6) 6_565 . ?
Lu1 Lu8 Lu6 117.1(4) . . ?
Lu5 Lu8 Lu6 85.5(5) . . ?
Lu11 Lu8 Lu6 105.3(3) . . ?
C42 Lu8 Lu6 152.9(6) . . ?
C41 Lu8 Lu6 158.7(5) . . ?
Lu9 Lu8 Lu6 85.3(4) 6_565 . ?
Lu7 Lu8 C21 66.4(6) . . ?
Lu11 Lu8 C21 90.5(7) 6_565 . ?
Lu1 Lu8 C21 121.1(3) . . ?
Lu5 Lu8 C21 90.0(4) . . ?
Lu11 Lu8 C21 118.4(4) . . ?
C42 Lu8 C21 33.82(10) . . ?
C41 Lu8 C21 60.63(13) . . ?
Lu9 Lu8 C21 92.5(4) 6_565 . ?
Lu6 Lu8 C21 119.8(5) . . ?
Lu7 Lu8 C40 133.5(5) . . ?
Lu11 Lu8 C40 118.5(7) 6_565 . ?
Lu1 Lu8 C40 90.6(4) . . ?
Lu5 Lu8 C40 150.4(4) . . ?
Lu11 Lu8 C40 117.2(5) . . ?
C42 Lu8 C40 63.57(13) . . ?
C41 Lu8 C40 35.40(9) . . ?
Lu9 Lu8 C40 151.1(3) 6_565 . ?
Lu6 Lu8 C40 123.3(5) . . ?
C21 Lu8 C40 70.57(14) . . ?
Lu7 Lu8 C19 123.5(8) . . ?
Lu11 Lu8 C19 142.2(6) 6_565 . ?
Lu1 Lu8 C19 123.9(5) . . ?
Lu5 Lu8 C19 147.4(5) . . ?
Lu11 Lu8 C19 150.8(5) . . ?
C42 Lu8 C19 73.56(15) . . ?
C41 Lu8 C19 61.94(13) . . ?
Lu9 Lu8 C19 150.2(5) 6_565 . ?
Lu6 Lu8 C19 99.0(4) . . ?
C21 Lu8 C19 59.66(15) . . ?
C40 Lu8 C19 33.65(8) . . ?
Lu5 Lu9 Lu9 124.8(18) 6_565 6_565 ?
Lu5 Lu9 Lu5 109(2) 6_565 . ?
Lu9 Lu9 Lu5 16.0(5) 6_565 . ?
Lu5 Lu9 Lu11 33(2) 6_565 . ?
Lu9 Lu9 Lu11 96.7(5) 6_565 . ?
Lu5 Lu9 Lu11 81.6(7) . . ?
Lu5 Lu9 Lu7 3.5(16) 6_565 6_565 ?
Lu9 Lu9 Lu7 124.7(2) 6_565 6_565 ?
Lu5 Lu9 Lu7 108.8(7) . 6_565 ?
Lu11 Lu9 Lu7 31.4(5) . 6_565 ?
Lu5 Lu9 Lu11 72.8(19) 6_565 6_565 ?
Lu9 Lu9 Lu11 54.3(4) 6_565 6_565 ?
Lu5 Lu9 Lu11 39.5(6) . 6_565 ?
Lu11 Lu9 Lu11 42.4(7) . 6_565 ?
Lu7 Lu9 Lu11 71.9(4) 6_565 6_565 ?
Lu5 Lu9 C44 129.8(18) 6_565 . ?
Lu9 Lu9 C44 71.9(2) 6_565 . ?
Lu5 Lu9 C44 81.7(4) . . ?
Lu11 Lu9 C44 108.1(4) . . ?
Lu7 Lu9 C44 126.3(4) 6_565 . ?
Lu11 Lu9 C44 92.5(3) 6_565 . ?
Lu5 Lu9 C67 96.1(17) 6_565 . ?
Lu9 Lu9 C67 108.1(2) 6_565 . ?
Lu5 Lu9 C67 113.2(6) . . ?
Lu11 Lu9 C67 89.8(4) . . ?
Lu7 Lu9 C67 93.1(4) 6_565 . ?
Lu11 Lu9 C67 102.0(3) 6_565 . ?
C44 Lu9 C67 39.10(10) . . ?
Lu5 Lu9 C46 144.7(18) 6_565 . ?
Lu9 Lu9 C46 87.3(2) 6_565 . ?
Lu5 Lu9 C46 102.6(5) . . ?
Lu11 Lu9 C46 144.7(4) . . ?
Lu7 Lu9 C46 142.9(4) 6_565 . ?
Lu11 Lu9 C46 129.4(4) 6_565 . ?
C44 Lu9 C46 40.15(11) . . ?
C67 Lu9 C46 55.96(15) . . ?
Lu5 Lu9 C68 90.2(17) 6_565 . ?
Lu9 Lu9 C68 136.86(19) 6_565 . ?
Lu5 Lu9 C68 147.4(6) . . ?
Lu11 Lu9 C68 104.3(5) . . ?
Lu7 Lu9 C68 88.7(3) 6_565 . ?
Lu11 Lu9 C68 134.1(4) 6_565 . ?
C44 Lu9 C68 65.94(17) . . ?
C67 Lu9 C68 36.38(11) . . ?
C46 Lu9 C68 54.47(14) . . ?
Lu5 Lu9 Lu7 89.5(18) 6_565 . ?
Lu9 Lu9 Lu7 35.39(18) 6_565 . ?
Lu5 Lu9 Lu7 19.5(5) . . ?
Lu11 Lu9 Lu7 62.6(5) . . ?
Lu7 Lu9 Lu7 89.4(3) 6_565 . ?
Lu11 Lu9 Lu7 21.6(3) 6_565 . ?
C44 Lu9 Lu7 92.2(3) . . ?
C67 Lu9 Lu7 114.6(3) . . ?
C46 Lu9 Lu7 120.3(3) . . ?
C68 Lu9 Lu7 150.6(3) . . ?
Lu5 Lu9 Lu8 13.8(17) 6_565 6_565 ?
Lu9 Lu9 Lu8 111.1(3) 6_565 6_565 ?
Lu5 Lu9 Lu8 95.2(6) . 6_565 ?
Lu11 Lu9 Lu8 25.5(5) . 6_565 ?
Lu7 Lu9 Lu8 14.8(3) 6_565 6_565 ?
Lu11 Lu9 Lu8 60.5(3) 6_565 6_565 ?
C44 Lu9 Lu8 131.8(3) . 6_565 ?
C67 Lu9 Lu8 104.2(3) . 6_565 ?
C46 Lu9 Lu8 157.4(4) . 6_565 ?
C68 Lu9 Lu8 103.4(4) . 6_565 ?
Lu7 Lu9 Lu8 76.0(3) . 6_565 ?
Lu10 Lu10 Lu2 128.4(7) 6_565 6_565 ?
Lu10 Lu10 Lu2 27.5(3) 6_565 . ?
Lu2 Lu10 Lu2 100.9(8) 6_565 . ?
Lu10 Lu10 Lu6 130.7(5) 6_565 . ?
Lu2 Lu10 Lu6 19.2(5) 6_565 . ?
Lu2 Lu10 Lu6 105.1(6) . . ?
Lu10 Lu10 Lu6 34.8(4) 6_565 6_565 ?
Lu2 Lu10 Lu6 96.0(8) 6_565 6_565 ?
Lu2 Lu10 Lu6 14.6(3) . 6_565 ?
Lu6 Lu10 Lu6 95.9(8) . 6_565 ?
Lu10 Lu10 C34 73.1(2) 6_565 . ?
Lu2 Lu10 C34 97.0(7) 6_565 . ?
Lu2 Lu10 C34 73.1(4) . . ?
Lu6 Lu10 C34 116.2(5) . . ?
Lu6 Lu10 C34 87.2(4) 6_565 . ?
Lu10 Lu10 C14 105.5(3) 6_565 . ?
Lu2 Lu10 C14 66.6(5) 6_565 . ?
Lu2 Lu10 C14 95.7(5) . . ?
Lu6 Lu10 C14 85.1(4) . . ?
Lu6 Lu10 C14 106.6(5) 6_565 . ?
C34 Lu10 C14 34.93(11) . . ?
Lu10 Lu10 C16 120.7(2) 6_565 . ?
Lu2 Lu10 C16 96.1(6) 6_565 . ?
Lu2 Lu10 C16 134.6(5) . . ?
Lu6 Lu10 C16 104.5(6) . . ?
Lu6 Lu10 C16 149.2(5) 6_565 . ?
C34 Lu10 C16 63.20(15) . . ?
C14 Lu10 C16 53.80(13) . . ?
Lu10 Lu10 C35 64.2(2) 6_565 . ?
Lu2 Lu10 C35 127.4(7) 6_565 . ?
Lu2 Lu10 C35 79.3(4) . . ?
Lu6 Lu10 C35 146.2(5) . . ?
Lu6 Lu10 C35 93.2(4) 6_565 . ?
C34 Lu10 C35 31.91(10) . . ?
C14 Lu10 C35 61.18(17) . . ?
C16 Lu10 C35 57.33(14) . . ?
Lu10 Lu10 C36 93.0(2) 6_565 . ?
Lu2 Lu10 C36 126.4(6) 6_565 . ?
Lu2 Lu10 C36 114.5(4) . . ?
Lu6 Lu10 C36 134.9(6) . . ?
Lu6 Lu10 C36 126.9(5) 6_565 . ?
C34 Lu10 C36 60.11(15) . . ?
C14 Lu10 C36 70.87(16) . . ?
C16 Lu10 C36 30.82(8) . . ?
C35 Lu10 C36 37.27(10) . . ?
Lu10 Lu10 C15 137.3(2) 6_565 . ?
Lu2 Lu10 C15 65.0(5) 6_565 . ?
Lu2 Lu10 C15 132.2(5) . . ?
Lu6 Lu10 C15 76.4(5) . . ?
Lu6 Lu10 C15 142.0(5) 6_565 . ?
C34 Lu10 C15 64.56(16) . . ?
C14 Lu10 C15 36.50(10) . . ?
C16 Lu10 C15 31.58(9) . . ?
C35 Lu10 C15 76.43(17) . . ?
C36 Lu10 C15 61.39(15) . . ?
Lu10 Lu10 Lu8 112.3(2) 6_565 . ?
Lu2 Lu10 Lu8 84.8(7) 6_565 . ?
Lu2 Lu10 Lu8 114.9(4) . . ?
Lu6 Lu10 Lu8 65.9(5) . . ?
Lu6 Lu10 Lu8 100.9(3) 6_565 . ?
C34 Lu10 Lu8 171.4(4) . . ?
C14 Lu10 Lu8 141.8(4) . . ?
C16 Lu10 Lu8 108.3(4) . . ?
C35 Lu10 Lu8 143.3(4) . . ?
C36 Lu10 Lu8 112.1(4) . . ?
C15 Lu10 Lu8 109.1(4) . . ?
Lu7 Lu11 Lu1 129.3(17) 6_565 . ?
Lu7 Lu11 Lu8 50.8(10) 6_565 6_565 ?
Lu1 Lu11 Lu8 79.1(11) . 6_565 ?
Lu7 Lu11 Lu5 65.9(8) 6_565 6_565 ?
Lu1 Lu11 Lu5 139.6(11) . 6_565 ?
Lu8 Lu11 Lu5 109.0(10) 6_565 6_565 ?
Lu7 Lu11 Lu11 148.3(7) 6_565 6_565 ?
Lu1 Lu11 Lu11 55.1(9) . 6_565 ?
Lu8 Lu11 Lu11 125.2(7) 6_565 6_565 ?
Lu5 Lu11 Lu11 92.4(9) 6_565 6_565 ?
Lu7 Lu11 Lu9 76.2(9) 6_565 . ?
Lu1 Lu11 Lu9 134.1(11) . . ?
Lu8 Lu11 Lu9 118.6(8) 6_565 . ?
Lu5 Lu11 Lu9 10.4(7) 6_565 . ?
Lu11 Lu11 Lu9 83.3(5) 6_565 . ?
Lu7 Lu11 Lu5 111.8(10) 6_565 . ?
Lu1 Lu11 Lu5 94.6(9) . . ?
Lu8 Lu11 Lu5 131.4(6) 6_565 . ?
Lu5 Lu11 Lu5 49.7(9) 6_565 . ?
Lu11 Lu11 Lu5 42.7(4) 6_565 . ?
Lu9 Lu11 Lu5 40.9(5) . . ?
Lu7 Lu11 Lu9 102.7(11) 6_565 6_565 ?
Lu1 Lu11 Lu9 106.8(10) . 6_565 ?
Lu8 Lu11 Lu9 132.3(6) 6_565 6_565 ?
Lu5 Lu11 Lu9 38.4(7) 6_565 6_565 ?
Lu11 Lu11 Lu9 54.3(4) 6_565 6_565 ?
Lu9 Lu11 Lu9 29.1(5) . 6_565 ?
Lu5 Lu11 Lu9 12.2(4) . 6_565 ?
Lu7 Lu11 C65 131.2(7) 6_565 . ?
Lu1 Lu11 C65 86.3(5) . . ?
Lu8 Lu11 C65 132.7(10) 6_565 . ?
Lu5 Lu11 C65 111.1(10) 6_565 . ?
Lu11 Lu11 C65 77.0(4) 6_565 . ?
Lu9 Lu11 C65 103.9(8) . . ?
Lu5 Lu11 C65 94.1(8) . . ?
Lu9 Lu11 C65 94.9(7) 6_565 . ?
Lu7 Lu11 Lu7 135.8(8) 6_565 . ?
Lu1 Lu11 Lu7 60.0(6) . . ?
Lu8 Lu11 Lu7 120.3(7) 6_565 . ?
Lu5 Lu11 Lu7 83.5(10) 6_565 . ?
Lu11 Lu11 Lu7 12.50(19) 6_565 . ?
Lu9 Lu11 Lu7 75.4(7) . . ?
Lu5 Lu11 Lu7 34.7(4) . . ?
Lu9 Lu11 Lu7 46.9(4) 6_565 . ?
C65 Lu11 Lu7 88.4(6) . . ?
Lu7 Lu11 C66 95.1(7) 6_565 . ?
Lu1 Lu11 C66 122.5(5) . . ?
Lu8 Lu11 C66 123.5(10) 6_565 . ?
Lu5 Lu11 C66 86.9(7) 6_565 . ?
Lu11 Lu11 C66 106.9(4) 6_565 . ?
Lu9 Lu11 C66 84.7(6) . . ?
Lu5 Lu11 C66 100.7(8) . . ?
Lu9 Lu11 C66 93.8(6) 6_565 . ?
C65 Lu11 C66 37.93(14) . . ?
Lu7 Lu11 C66 115.0(7) . . ?
Lu7 Lu11 Lu8 133.8(6) 6_565 . ?
Lu1 Lu11 Lu8 37.6(5) . . ?
Lu8 Lu11 Lu8 99.7(9) 6_565 . ?
Lu5 Lu11 Lu8 102.8(9) 6_565 . ?
Lu11 Lu11 Lu8 25.6(4) 6_565 . ?
Lu9 Lu11 Lu8 96.5(7) . . ?
Lu5 Lu11 Lu8 57.5(5) . . ?
Lu9 Lu11 Lu8 69.6(5) 6_565 . ?
C65 Lu11 Lu8 95.0(5) . . ?
Lu7 Lu11 Lu8 24.3(2) . . ?
C66 Lu11 Lu8 130.0(6) . . ?
C5 C1 C2 92.3 . . ?
C5 C1 C9 138.8 . . ?
C2 C1 C9 120.4 . . ?
C5 C1 Lu6 84.9(3) . . ?
C2 C1 Lu6 58.3(2) . . ?
C9 C1 Lu6 91.6(3) . . ?
C3 C2 C12 115.1 . . ?
C3 C2 C1 118.0 . . ?
C12 C2 C1 115.0 . . ?
C3 C2 Lu6 79.0(4) . . ?
C12 C2 Lu6 66.8(3) . . ?
C1 C2 Lu6 89.3(3) . . ?
C2 C3 C15 129.7 . . ?
C2 C3 C4 112.1 . . ?
C15 C3 C4 112.3 . . ?
C2 C3 Lu6 70.3(3) . . ?
C15 C3 Lu6 85.0(3) . . ?
C4 C3 Lu6 93.1(2) . . ?
C18 C4 C3 120.1 . . ?
C18 C4 C5 133.7 . . ?
C3 C4 C5 96.0 . . ?
C18 C4 Lu6 96.2(3) . . ?
C3 C4 Lu6 57.68(17) . . ?
C5 C4 Lu6 78.6(3) . . ?
C6 C5 C1 116.7 . . ?
C6 C5 C4 111.5 . . ?
C1 C5 C4 121.1 . . ?
C6 C5 Lu6 100.84(16) . . ?
C1 C5 Lu6 67.3(3) . . ?
C4 C5 Lu6 72.2(3) . . ?
C5 C6 C7 127.2 . . ?
C5 C6 C20 135.9 . . ?
C7 C6 C20 89.2 . . ?
C6 C7 C22 131.8 . . ?
C6 C7 C8 118.9 . . ?
C22 C7 C8 99.6 . . ?
C6 C7 Lu7 88.49(12) . . ?
C22 C7 Lu7 58.91(10) . . ?
C8 C7 Lu7 94.46(10) . . ?
C9 C8 C25 109.8 . . ?
C9 C8 C7 106.8 . . ?
C25 C8 C7 131.7 . . ?
C8 C9 C10 108.1 . . ?
C8 C9 C1 111.6 . . ?
C10 C9 C1 126.3 . . ?
C8 C9 Lu4 90.71(6) . . ?
C10 C9 Lu4 56.92(6) . . ?
C1 C9 Lu4 87.72(7) . . ?
C26 C10 C9 105.8 . . ?
C26 C10 C11 133.2 . . ?
C9 C10 C11 111.7 . . ?
C26 C10 Lu4 88.49(8) . . ?
C9 C10 Lu4 92.39(9) . . ?
C11 C10 Lu4 63.45(7) . . ?
C29 C11 C12 134.2 . . ?
C29 C11 C10 94.7 . . ?
C12 C11 C10 120.6 . . ?
C29 C11 Lu4 75.09(10) . . ?
C12 C11 Lu4 84.06(9) . . ?
C10 C11 Lu4 78.29(8) . . ?
C29 C11 Lu6 101.3(2) . . ?
C12 C11 Lu6 52.8(2) . . ?
C10 C11 Lu6 93.2(3) . . ?
Lu4 C11 Lu6 31.5(2) . . ?
C29 C11 Lu3 52.74(8) . . ?
C12 C11 Lu3 100.60(10) . . ?
C10 C11 Lu3 82.72(11) . . ?
Lu4 C11 Lu3 22.35(8) . . ?
Lu6 C11 Lu3 51.2(2) . . ?
C2 C12 C11 125.3 . . ?
C2 C12 C13 118.7 . . ?
C11 C12 C13 112.1 . . ?
C2 C12 Lu6 76.5(3) . . ?
C11 C12 Lu6 94.9(4) . . ?
C13 C12 Lu6 79.3(3) . . ?
C2 C12 Lu4 100.21(8) . . ?
C11 C12 Lu4 60.29(6) . . ?
C13 C12 Lu4 89.65(8) . . ?
Lu6 C12 Lu4 34.9(4) . . ?
C14 C13 C32 116.6 . . ?
C14 C13 C12 126.4 . . ?
C32 C13 C12 112.3 . . ?
C14 C13 Lu6 89.5(4) . . ?
C32 C13 Lu6 97.4(3) . . ?
C12 C13 Lu6 63.3(3) . . ?
C14 C13 Lu10 59.53(13) . . ?
C32 C13 Lu10 91.9(2) . . ?
C12 C13 Lu10 99.11(19) . . ?
Lu6 C13 Lu10 36.8(3) . . ?
C14 C13 Lu4 115.6 . . ?
C32 C13 Lu4 73.65(8) . . ?
C12 C13 Lu4 59.59(7) . . ?
Lu6 C13 Lu4 29.6(3) . . ?
Lu10 C13 Lu4 56.64(13) . . ?
C13 C14 C34 118.4 . . ?
C13 C14 C15 107.3 . . ?
C34 C14 C15 123.9 . . ?
C13 C14 Lu10 90.08(18) . . ?
C34 C14 Lu10 72.5(2) . . ?
C15 C14 Lu10 77.0(3) . . ?
C13 C14 Lu6 60.5(3) . . ?
C34 C14 Lu6 105.6(2) . . ?
C15 C14 Lu6 69.9(2) . . ?
Lu10 C14 Lu6 36.6(3) . . ?
C13 C14 Lu2 80.87(7) . . ?
C34 C14 Lu2 55.57(6) . . ?
C15 C14 Lu2 105.97(8) . . ?
Lu10 C14 Lu2 29.0(2) . . ?
Lu6 C14 Lu2 51.05(19) . . ?
C16 C15 C3 131.3 . . ?
C16 C15 C14 97.0 . . ?
C3 C15 C14 122.5 . . ?
C16 C15 Lu10 69.62(18) . . ?
C3 C15 Lu10 99.13(19) . . ?
C14 C15 Lu10 66.5(2) . . ?
C16 C15 Lu6 102.9(3) . . ?
C3 C15 Lu6 64.6(2) . . ?
C14 C15 Lu6 77.3(2) . . ?
Lu10 C15 Lu6 37.2(3) . . ?
C36 C16 C15 149.2 . . ?
C36 C16 C17 85.8 . . ?
C15 C16 C17 112.6 . . ?
C36 C16 Lu10 77.3(2) . . ?
C15 C16 Lu10 78.79(19) . . ?
C17 C16 Lu10 88.0(2) . . ?
C38 C17 C18 100.9 . . ?
C38 C17 C16 135.5 . . ?
C18 C17 C16 119.2 . . ?
C38 C17 C36 91.2 . . ?
C18 C17 C36 158.1 . . ?
C16 C17 C36 44.7 . . ?
C38 C17 C37 50.2 . . ?
C18 C17 C37 147.4 . . ?
C16 C17 C37 85.6 . . ?
C36 C17 C37 41.0 . . ?
C38 C17 Lu10 96.36(16) . . ?
C18 C17 Lu10 98.57(18) . . ?
C16 C17 Lu10 61.28(16) . . ?
C36 C17 Lu10 61.59(18) . . ?
C37 C17 Lu10 74.06(17) . . ?
C4 C18 C17 123.7 . . ?
C4 C18 C19 107.4 . . ?
C17 C18 C19 119.4 . . ?
C40 C19 C20 119.7 . . ?
C40 C19 C18 113.9 . . ?
C20 C19 C18 119.7 . . ?
C40 C19 Lu8 72.0(2) . . ?
C20 C19 Lu8 76.8(3) . . ?
C18 C19 Lu8 96.00(16) . . ?
C21 C20 C19 118.0 . . ?
C21 C20 C6 117.0 . . ?
C19 C20 C6 111.4 . . ?
C21 C20 Lu8 68.70(18) . . ?
C19 C20 Lu8 69.8(2) . . ?
C6 C20 Lu8 96.14(17) . . ?
C21 C20 Lu7 54.53(10) . . ?
C19 C20 Lu7 89.37(11) . . ?
C6 C20 Lu7 91.14(11) . . ?
Lu8 C20 Lu7 19.7(2) . . ?
C42 C21 C20 123.3 . . ?
C42 C21 C22 115.1 . . ?
C20 C21 C22 111.9 . . ?
C42 C21 Lu7 68.25(15) . . ?
C20 C21 Lu7 94.74(16) . . ?
C22 C21 Lu7 76.47(14) . . ?
C42 C21 Lu8 66.07(19) . . ?
C20 C21 Lu8 78.92(18) . . ?
C22 C21 Lu8 96.8(2) . . ?
Lu7 C21 Lu8 22.17(17) . . ?
C23 C22 C7 130.8 . . ?
C23 C22 C21 123.3 . . ?
C7 C22 C21 88.7 . . ?
C23 C22 Lu7 75.51(16) . . ?
C7 C22 Lu7 89.78(15) . . ?
C21 C22 Lu7 64.40(13) . . ?
C23 C22 Lu5 50.99(15) . . ?
C7 C22 Lu5 101.24(16) . . ?
C21 C22 Lu5 87.7(2) . . ?
Lu7 C22 Lu5 25.6(2) . . ?
C22 C23 C45 120.1 . . ?
C22 C23 C24 129.2 . . ?
C45 C23 C24 105.4 . . ?
C22 C23 Lu5 103.3(2) . . ?
C45 C23 Lu5 63.4(3) . . ?
C24 C23 Lu5 76.8(3) . . ?
C22 C23 Lu7 74.59(15) . . ?
C45 C23 Lu7 72.27(15) . . ?
C24 C23 Lu7 101.22(11) . . ?
Lu5 C23 Lu7 29.9(3) . . ?
C47 C24 C25 109.2 . . ?
C47 C24 C23 134.6 . . ?
C25 C24 C23 112.3 . . ?
C47 C24 Lu5 89.9(2) . . ?
C25 C24 Lu5 105.8(2) . . ?
C23 C24 Lu5 61.9(2) . . ?
C8 C25 C26 104.3 . . ?
C8 C25 C24 113.9 . . ?
C26 C25 C24 128.5 . . ?
C10 C26 C27 119.7 . . ?
C10 C26 C25 110.5 . . ?
C27 C26 C25 117.0 . . ?
C10 C26 Lu4 59.90(7) . . ?
C27 C26 Lu4 83.50(8) . . ?
C25 C26 Lu4 91.25(6) . . ?
C10 C26 Lu3 76.90(10) . . ?
C27 C26 Lu3 61.63(8) . . ?
C25 C26 Lu3 98.46(8) . . ?
Lu4 C26 Lu3 22.06(7) . . ?
C28 C27 C48 128.8 . . ?
C28 C27 C26 103.7 . . ?
C48 C27 C26 115.0 . . ?
C28 C27 Lu3 59.16(10) . . ?
C48 C27 Lu3 88.64(10) . . ?
C26 C27 Lu3 88.55(8) . . ?
C27 C28 C29 136.9 . . ?
C27 C28 C51 102.4 . . ?
C29 C28 C51 110.4 . . ?
C27 C28 Lu3 91.20(13) . . ?
C29 C28 Lu3 71.32(14) . . ?
C51 C28 Lu3 75.82(10) . . ?
C27 C28 Lu4 89.92(7) . . ?
C29 C28 Lu4 58.48(6) . . ?
C51 C28 Lu4 99.04(8) . . ?
Lu3 C28 Lu4 23.53(6) . . ?
C28 C29 C11 129.2 . . ?
C28 C29 C30 116.9 . . ?
C11 C29 C30 108.5 . . ?
C28 C29 Lu3 73.06(14) . . ?
C11 C29 Lu3 95.36(10) . . ?
C30 C29 Lu3 78.94(13) . . ?
C28 C29 Lu4 91.41(8) . . ?
C11 C29 Lu4 67.04(9) . . ?
C30 C29 Lu4 89.00(8) . . ?
Lu3 C29 Lu4 28.33(7) . . ?
C32 C30 C29 116.6 . . ?
C32 C30 C52 144.7 . . ?
C29 C30 C52 90.3 . . ?
C32 C30 Lu3 97.64(12) . . ?
C29 C30 Lu3 63.86(10) . . ?
C52 C30 Lu3 73.07(10) . . ?
C32 C30 Lu4 81.06(7) . . ?
C29 C30 Lu4 57.91(6) . . ?
C52 C30 Lu4 96.58(8) . . ?
Lu3 C30 Lu4 23.98(7) . . ?
C33 C31 C32 118.5 . . ?
C33 C31 C54 106.9 . . ?
C32 C31 C54 130.6 . . ?
C33 C31 Lu2 64.41(8) . . ?
C32 C31 Lu2 90.65(10) . . ?
C54 C31 Lu2 92.10(12) . . ?
C30 C32 C13 135.0 . . ?
C30 C32 C31 93.2 . . ?
C13 C32 C31 127.2 . . ?
C30 C32 Lu2 102.29(9) . . ?
C13 C32 Lu2 87.16(10) . . ?
C31 C32 Lu2 57.51(9) . . ?
C30 C32 Lu4 69.92(7) . . ?
C13 C32 Lu4 77.99(8) . . ?
C31 C32 Lu4 108.50(7) . . ?
Lu2 C32 Lu4 59.80(6) . . ?
C30 C32 Lu3 54.17(8) . . ?
C13 C32 Lu3 99.69(7) . . ?
C31 C32 Lu3 92.81(7) . . ?
Lu2 C32 Lu3 57.71(8) . . ?
Lu4 C32 Lu3 21.93(5) . . ?
C30 C32 Lu6 98.6(3) . . ?
C13 C32 Lu6 54.21(19) . . ?
C31 C32 Lu6 108.3(2) . . ?
Lu2 C32 Lu6 50.8(2) . . ?
Lu4 C32 Lu6 28.7(3) . . ?
Lu3 C32 Lu6 47.5(2) . . ?
C31 C33 C34 115.3 . . ?
C31 C33 C57 120.7 . . ?
C34 C33 C57 113.4 . . ?
C31 C33 Lu2 79.44(10) . . ?
C34 C33 Lu2 80.44(13) . . ?
C57 C33 Lu2 77.39(11) . . ?
C31 C33 Lu10 90.49(15) . . ?
C34 C33 Lu10 54.15(13) . . ?
C57 C33 Lu10 91.86(16) . . ?
Lu2 C33 Lu10 26.41(17) . . ?
C35 C34 C14 126.7 . . ?
C35 C34 C33 101.7 . . ?
C14 C34 C33 123.7 . . ?
C35 C34 Lu10 78.1(2) . . ?
C14 C34 Lu10 72.6(2) . . ?
C33 C34 Lu10 94.3(2) . . ?
C35 C34 Lu2 84.02(9) . . ?
C14 C34 Lu2 94.83(9) . . ?
C33 C34 Lu2 60.07(11) . . ?
Lu10 C34 Lu2 34.3(2) . . ?
C34 C35 C36 112.6 . . ?
C34 C35 C58 116.8 . . ?
C36 C35 C58 119.6 . . ?
C34 C35 Lu10 70.0(2) . . ?
C36 C35 Lu10 71.5(2) . . ?
C58 C35 Lu10 94.87(18) . . ?
C34 C35 Lu2 65.32(7) . . ?
C36 C35 Lu2 101.79(9) . . ?
C58 C35 Lu2 71.22(9) . . ?
Lu10 C35 Lu2 31.9(2) . . ?
C16 C36 C37 123.0 . . ?
C16 C36 C35 108.4 . . ?
C37 C36 C35 118.9 . . ?
C16 C36 C17 49.5 . . ?
C37 C36 C17 73.7 . . ?
C35 C36 C17 146.8 . . ?
C16 C36 Lu10 71.85(19) . . ?
C37 C36 Lu10 94.36(19) . . ?
C35 C36 Lu10 71.3(2) . . ?
C17 C36 Lu10 77.5(2) . . ?
C36 C37 C38 105.8 . . ?
C36 C37 C60 121.6 . . ?
C38 C37 C60 123.5 . . ?
C36 C37 C17 65.3 . . ?
C38 C37 C17 40.6 . . ?
C60 C37 C17 152.4 . . ?
C36 C37 C39 139.2 . . ?
C38 C37 C39 38.1 . . ?
C60 C37 C39 85.7 . . ?
C17 C37 C39 77.0 . . ?
C36 C37 Lu10 58.38(14) . . ?
C38 C37 Lu10 85.2(2) . . ?
C60 C37 Lu10 94.30(16) . . ?
C17 C37 Lu10 65.70(19) . . ?
C39 C37 Lu10 92.89(17) . . ?
C39 C38 C17 158.0 . . ?
C39 C38 C37 94.4 . . ?
C17 C38 C37 89.2 . . ?
C39 C38 C40 49.9 . . ?
C17 C38 C40 117.0 . . ?
C37 C38 C40 139.4 . . ?
C62 C39 C38 158.4 . . ?
C62 C39 C40 98.5 . . ?
C38 C39 C40 91.5 . . ?
C62 C39 C37 115.0 . . ?
C38 C39 C37 47.5 . . ?
C40 C39 C37 134.7 . . ?
C62 C39 Lu1 57.01(6) . . ?
C38 C39 Lu1 108.19(5) . . ?
C40 C39 Lu1 74.68(8) . . ?
C37 C39 Lu1 98.11(6) . . ?
C19 C40 C41 118.6 . . ?
C19 C40 C39 124.8 . . ?
C41 C40 C39 105.7 . . ?
C19 C40 C38 86.6 . . ?
C41 C40 C38 138.6 . . ?
C39 C40 C38 38.7 . . ?
C19 C40 Lu8 74.3(2) . . ?
C41 C40 Lu8 68.10(17) . . ?
C39 C40 Lu8 95.2(2) . . ?
C38 C40 Lu8 90.89(19) . . ?
C19 C40 Lu1 105.21(6) . . ?
C41 C40 Lu1 54.32(6) . . ?
C39 C40 Lu1 74.64(7) . . ?
C38 C40 Lu1 89.09(6) . . ?
Lu8 C40 Lu1 31.1(2) . . ?
C63 C41 C42 129.1 . . ?
C63 C41 C40 103.0 . . ?
C42 C41 C40 119.8 . . ?
C63 C41 Lu8 97.8(2) . . ?
C42 C41 Lu8 69.3(3) . . ?
C40 C41 Lu8 76.50(19) . . ?
C63 C41 Lu1 62.48(8) . . ?
C42 C41 Lu1 85.88(8) . . ?
C40 C41 Lu1 95.37(8) . . ?
Lu8 C41 Lu1 37.0(2) . . ?
C63 C41 Lu7 103.70(12) . . ?
C42 C41 Lu7 51.50(9) . . ?
C40 C41 Lu7 92.96(13) . . ?
Lu8 C41 Lu7 19.1(2) . . ?
Lu1 C41 Lu7 41.78(9) . . ?
C21 C42 C41 119.3 . . ?
C21 C42 C43 120.8 . . ?
C41 C42 C43 114.1 . . ?
C21 C42 Lu7 75.16(17) . . ?
C41 C42 Lu7 97.44(14) . . ?
C43 C42 Lu7 74.56(18) . . ?
C21 C42 Lu8 80.1(2) . . ?
C41 C42 Lu8 74.9(3) . . ?
C43 C42 Lu8 91.13(18) . . ?
Lu7 C42 Lu8 23.9(2) . . ?
C21 C42 Lu1 113.97(6) . . ?
C41 C42 Lu1 61.94(6) . . ?
C43 C42 Lu1 71.18(7) . . ?
Lu7 C42 Lu1 43.54(13) . . ?
Lu8 C42 Lu1 34.1(2) . . ?
C45 C43 C65 119.3 . . ?
C45 C43 C42 118.4 . . ?
C65 C43 C42 118.2 . . ?
C45 C43 Lu7 78.87(14) . . ?
C65 C43 Lu7 105.61(13) . . ?
C42 C43 Lu7 66.19(15) . . ?
C45 C43 Lu5 57.71(19) . . ?
C65 C43 Lu5 96.9(2) . . ?
C42 C43 Lu5 95.6(2) . . ?
Lu7 C43 Lu5 29.8(2) . . ?
C45 C43 Lu11 93.7(3) . . ?
C65 C43 Lu11 55.5(2) . . ?
C42 C43 Lu11 101.0(2) . . ?
Lu7 C43 Lu11 51.6(3) . . ?
Lu5 C43 Lu11 44.1(3) . . ?
C45 C43 Lu1 111.39(6) . . ?
C65 C43 Lu1 64.27(7) . . ?
C42 C43 Lu1 75.91(8) . . ?
Lu7 C43 Lu1 43.96(11) . . ?
Lu5 C43 Lu1 54.13(19) . . ?
Lu11 C43 Lu1 26.0(2) . . ?
C45 C43 Lu8 97.2(2) . . ?
C65 C43 Lu8 96.6(2) . . ?
C42 C43 Lu8 55.93(12) . . ?
Lu7 C43 Lu8 18.3(2) . . ?
Lu5 C43 Lu8 45.1(2) . . ?
Lu11 C43 Lu8 49.5(2) . . ?
Lu1 C43 Lu8 32.3(2) . . ?
C67 C44 C45 121.2 . . ?
C67 C44 C46 89.3 . . ?
C45 C44 C46 141.3 . . ?
C67 C44 Lu9 71.0(2) . . ?
C45 C44 Lu9 92.52(18) . . ?
C46 C44 Lu9 74.41(15) . . ?
C67 C44 Lu5 98.1(2) . . ?
C45 C44 Lu5 62.3(3) . . ?
C46 C44 Lu5 92.5(3) . . ?
Lu9 C44 Lu5 32.78(18) . . ?
C43 C45 C44 119.0 . . ?
C43 C45 C23 121.2 . . ?
C44 C45 C23 113.3 . . ?
C43 C45 Lu5 87.4(3) . . ?
C44 C45 Lu5 79.4(3) . . ?
C23 C45 Lu5 77.2(3) . . ?
C43 C45 Lu7 66.88(12) . . ?
C44 C45 Lu7 108.57(12) . . ?
C23 C45 Lu7 72.72(14) . . ?
Lu5 C45 Lu7 30.2(3) . . ?
C43 C45 Lu9 91.08(14) . . ?
C44 C45 Lu9 53.84(14) . . ?
C23 C45 Lu9 99.11(16) . . ?
Lu5 C45 Lu9 28.2(3) . . ?
Lu7 C45 Lu9 54.98(16) . . ?
C70 C46 C47 95.6 . . ?
C70 C46 C44 143.5 . . ?
C47 C46 C44 110.8 . . ?
C70 C46 Lu9 87.01(16) . . ?
C47 C46 Lu9 97.73(19) . . ?
C44 C46 Lu9 65.44(14) . . ?
C70 C46 Lu5 107.98(17) . . ?
C47 C46 Lu5 80.6(2) . . ?
C44 C46 Lu5 55.2(2) . . ?
Lu9 C46 Lu5 26.02(15) . . ?
C46 C47 C48 114.4 . . ?
C46 C47 C24 113.3 . . ?
C48 C47 C24 119.4 . . ?
C46 C47 C70 41.7 . . ?
C48 C47 C70 73.1 . . ?
C24 C47 C70 145.4 . . ?
C46 C47 Lu9 52.72(14) . . ?
C48 C47 Lu9 96.77(12) . . ?
C24 C47 Lu9 84.10(15) . . ?
C70 C47 Lu9 61.75(15) . . ?
C46 C47 Lu5 71.4(2) . . ?
C48 C47 Lu5 105.54(16) . . ?
C24 C47 Lu5 58.9(2) . . ?
C70 C47 Lu5 87.1(2) . . ?
Lu9 C47 Lu5 25.37(15) . . ?
C49 C48 C27 121.1 . . ?
C49 C48 C47 100.2 . . ?
C27 C48 C47 127.2 . . ?
C49 C48 C50 36.7 . . ?
C27 C48 C50 84.7 . . ?
C47 C48 C50 132.5 . . ?
C49 C48 Lu3 80.21(7) . . ?
C27 C48 Lu3 61.63(7) . . ?
C47 C48 Lu3 98.97(7) . . ?
C50 C48 Lu3 63.14(7) . . ?
C48 C49 C50 108.0 . . ?
C48 C49 C70 113.2 . . ?
C50 C49 C70 135.0 . . ?
C51 C50 C49 140.6 . . ?
C51 C50 C72 107.7 . . ?
C49 C50 C72 102.0 . . ?
C51 C50 C48 107.0 . . ?
C49 C50 C48 35.3 . . ?
C72 C50 C48 134.7 . . ?
C51 C50 Lu3 61.84(9) . . ?
C49 C50 Lu3 90.05(10) . . ?
C72 C50 Lu3 96.06(8) . . ?
C48 C50 Lu3 75.73(10) . . ?
C50 C51 C52 142.1 . . ?
C50 C51 C28 115.1 . . ?
C52 C51 C28 92.2 . . ?
C50 C51 Lu3 92.48(12) . . ?
C52 C51 Lu3 75.34(13) . . ?
C28 C51 Lu3 64.43(9) . . ?
C53 C52 C51 114.9 . . ?
C53 C52 C30 105.3 . . ?
C51 C52 C30 127.9 . . ?
C53 C52 Lu3 98.51(9) . . ?
C51 C52 Lu3 71.63(13) . . ?
C30 C52 Lu3 70.95(12) . . ?
C54 C53 C52 126.6 . . ?
C54 C53 C73 122.0 . . ?
C52 C53 C73 106.1 . . ?
C54 C53 C55 40.2 . . ?
C52 C53 C55 158.8 . . ?
C73 C53 C55 82.0 . . ?
C54 C53 Lu3 100.99(10) . . ?
C52 C53 Lu3 55.35(7) . . ?
C73 C53 Lu3 89.18(10) . . ?
C55 C53 Lu3 106.21(8) . . ?
C55 C54 C53 97.4 . . ?
C55 C54 C31 133.2 . . ?
C53 C54 C31 117.1 . . ?
C55 C54 Lu2 86.87(8) . . ?
C53 C54 Lu2 106.60(6) . . ?
C31 C54 Lu2 54.83(8) . . ?
C54 C55 C74 125.6 . . ?
C54 C55 C56 126.0 . . ?
C74 C55 C56 99.9 . . ?
C54 C55 C53 42.3 . . ?
C74 C55 C53 83.6 . . ?
C56 C55 C53 155.2 . . ?
C57 C56 C77 116.1 . . ?
C57 C56 C55 102.9 . . ?
C77 C56 C55 130.3 . . ?
C57 C56 Lu2 55.77(7) . . ?
C77 C56 Lu2 100.37(6) . . ?
C55 C56 Lu2 76.42(8) . . ?
C58 C57 C56 120.9 . . ?
C58 C57 C33 102.2 . . ?
C56 C57 C33 126.6 . . ?
C58 C57 Lu2 83.06(10) . . ?
C56 C57 Lu2 95.54(10) . . ?
C33 C57 Lu2 57.73(8) . . ?
C57 C58 C59 125.9 . . ?
C57 C58 C35 105.5 . . ?
C59 C58 C35 121.3 . . ?
C57 C58 Lu2 65.46(10) . . ?
C59 C58 Lu2 105.58(7) . . ?
C35 C58 Lu2 69.42(10) . . ?
C78 C59 C58 111.6 . . ?
C78 C59 C60 126.2 . . ?
C58 C59 C60 109.8 . . ?
C37 C60 C61 123.3 . . ?
C37 C60 C59 128.5 . . ?
C61 C60 C59 97.6 . . ?
C80 C61 C60 130.4 . . ?
C80 C61 C62 118.1 . . ?
C60 C61 C62 100.3 . . ?
C80 C61 Lu1 74.84(8) . . ?
C60 C61 Lu1 101.64(6) . . ?
C62 C61 Lu1 60.32(7) . . ?
C39 C62 C63 121.6 . . ?
C39 C62 C61 114.9 . . ?
C63 C62 C61 115.3 . . ?
C39 C62 Lu1 98.99(8) . . ?
C63 C62 Lu1 58.78(7) . . ?
C61 C62 Lu1 84.76(9) . . ?
C41 C63 C62 110.7 . . ?
C41 C63 C64 118.0 . . ?
C62 C63 C64 123.2 . . ?
C41 C63 Lu1 85.07(10) . . ?
C62 C63 Lu1 89.02(9) . . ?
C64 C63 Lu1 68.75(9) . . ?
C41 C63 Lu8 55.65(16) . . ?
C62 C63 Lu8 90.42(19) . . ?
C64 C63 Lu8 93.83(15) . . ?
Lu1 C63 Lu8 31.28(13) . . ?
C41 C63 Lu11 92.7(3) . . ?
C62 C63 Lu11 101.8(3) . . ?
C64 C63 Lu11 50.66(15) . . ?
Lu1 C63 Lu11 18.32(15) . . ?
Lu8 C63 Lu11 45.5(2) . . ?
C65 C64 C81 112.9 . . ?
C65 C64 C63 117.9 . . ?
C81 C64 C63 121.0 . . ?
C65 C64 Lu1 82.31(9) . . ?
C81 C64 Lu1 89.63(10) . . ?
C63 C64 Lu1 70.06(9) . . ?
C65 C64 Lu11 64.2(4) . . ?
C81 C64 Lu11 76.6(4) . . ?
C63 C64 Lu11 100.0(2) . . ?
Lu1 C64 Lu11 30.1(2) . . ?
C43 C65 C66 122.3 . . ?
C43 C65 C64 122.4 . . ?
C66 C65 C64 109.9 . . ?
C43 C65 Lu11 91.8(4) . . ?
C66 C65 Lu11 75.1(3) . . ?
C64 C65 Lu11 78.8(4) . . ?
C43 C65 Lu1 83.55(9) . . ?
C66 C65 Lu1 103.45(8) . . ?
C64 C65 Lu1 60.99(7) . . ?
Lu11 C65 Lu1 29.5(3) . . ?
C43 C65 Lu5 55.08(18) . . ?
C66 C65 Lu5 86.1(2) . . ?
C64 C65 Lu5 110.78(13) . . ?
Lu11 C65 Lu5 39.7(4) . . ?
Lu1 C65 Lu5 49.80(14) . . ?
C43 C65 Lu9 76.87(15) . . ?
C66 C65 Lu9 62.65(14) . . ?
C64 C65 Lu9 110.57(12) . . ?
Lu11 C65 Lu9 31.8(4) . . ?
Lu1 C65 Lu9 56.18(12) . . ?
Lu5 C65 Lu9 24.44(16) . . ?
C82 C66 C67 117.0 . . ?
C82 C66 C65 111.5 . . ?
C67 C66 C65 119.0 . . ?
C82 C66 Lu11 76.2(5) . . ?
C67 C66 Lu11 90.8(4) . . ?
C65 C66 Lu11 67.0(3) . . ?
C82 C66 Lu9 95.28(16) . . ?
C67 C66 Lu9 53.28(13) . . ?
C65 C66 Lu9 88.67(14) . . ?
Lu11 C66 Lu9 37.5(4) . . ?
C68 C67 C66 115.9 . . ?
C68 C67 C44 118.5 . . ?
C66 C67 C44 118.8 . . ?
C68 C67 Lu9 79.99(18) . . ?
C66 C67 Lu9 94.65(17) . . ?
C44 C67 Lu9 69.9(2) . . ?
C68 C67 Lu11 96.4(2) . . ?
C66 C67 Lu11 57.3(2) . . ?
C44 C67 Lu11 90.5(4) . . ?
Lu9 C67 Lu11 37.3(3) . . ?
C68 C67 Lu5 102.9(2) . . ?
C66 C67 Lu5 90.3(2) . . ?
C44 C67 Lu5 52.51(16) . . ?
Lu9 C67 Lu5 23.77(19) . . ?
Lu11 C67 Lu5 39.9(3) . . ?
C69 C68 C84 88.8 . . ?
C69 C68 C67 137.9 . . ?
C84 C68 C67 122.5 . . ?
C69 C68 C70 30.8 . . ?
C84 C68 C70 115.2 . . ?
C67 C68 C70 107.3 . . ?
C69 C68 Lu9 89.58(14) . . ?
C84 C68 Lu9 93.31(17) . . ?
C67 C68 Lu9 63.63(14) . . ?
C70 C68 Lu9 73.25(16) . . ?
C70 C69 C68 111.7 . . ?
C70 C69 C71 119.3 . . ?
C68 C69 C71 116.9 . . ?
C70 C69 C84 148.2 . . ?
C68 C69 C84 49.1 . . ?
C71 C69 C84 68.2 . . ?
C70 C69 Lu9 73.77(16) . . ?
C68 C69 Lu9 62.20(13) . . ?
C71 C69 Lu9 98.70(13) . . ?
C84 C69 Lu9 74.52(16) . . ?
C69 C70 C49 122.3 . . ?
C69 C70 C46 115.1 . . ?
C49 C70 C46 115.0 . . ?
C69 C70 C68 37.5 . . ?
C49 C70 C68 147.9 . . ?
C46 C70 C68 77.7 . . ?
C69 C70 C47 154.0 . . ?
C49 C70 C47 73.2 . . ?
C46 C70 C47 42.7 . . ?
C68 C70 C47 118.1 . . ?
C69 C70 Lu9 82.92(18) . . ?
C49 C70 Lu9 98.01(14) . . ?
C46 C70 Lu9 60.90(15) . . ?
C68 C70 Lu9 61.10(16) . . ?
C47 C70 Lu9 73.73(18) . . ?
C69 C71 C85 113.9 . . ?
C69 C71 C72 116.9 . . ?
C85 C71 C72 121.2 . . ?
C69 C71 C84 69.5 . . ?
C85 C71 C84 44.3 . . ?
C72 C71 C84 149.5 . . ?
C73 C72 C50 118.0 . . ?
C73 C72 C71 112.2 . . ?
C50 C72 C71 124.2 . . ?
C72 C73 C53 127.4 . . ?
C72 C73 C74 123.7 . . ?
C53 C73 C74 94.7 . . ?
C75 C74 C55 125.7 . . ?
C75 C74 C73 126.3 . . ?
C55 C74 C73 99.6 . . ?
C74 C75 C85 107.5 . . ?
C74 C75 C76 136.9 . . ?
C85 C75 C76 104.5 . . ?
C86 C76 C77 109.4 . . ?
C86 C76 C75 138.1 . . ?
C77 C76 C75 99.3 . . ?
C78 C77 C76 106.5 . . ?
C78 C77 C56 120.1 . . ?
C76 C77 C56 125.4 . . ?
C59 C78 C77 125.3 . . ?
C59 C78 C79 113.3 . . ?
C77 C78 C79 109.1 . . ?
C80 C79 C78 135.3 . . ?
C80 C79 C86 104.3 . . ?
C78 C79 C86 108.2 . . ?
C79 C80 C81 118.5 . . ?
C79 C80 C61 114.3 . . ?
C81 C80 C61 123.6 . . ?
C79 C80 C86 43.6 . . ?
C81 C80 C86 75.0 . . ?
C61 C80 C86 150.2 . . ?
C79 C80 Lu1 116.40(6) . . ?
C81 C80 Lu1 64.42(6) . . ?
C61 C80 Lu1 75.68(7) . . ?
C86 C80 Lu1 96.13(7) . . ?
C80 C81 C64 118.8 . . ?
C80 C81 C82 131.9 . . ?
C64 C81 C82 99.6 . . ?
C80 C81 Lu11 101.3(3) . . ?
C64 C81 Lu11 67.9(3) . . ?
C82 C81 Lu11 65.9(2) . . ?
C80 C81 Lu1 87.40(7) . . ?
C64 C81 Lu1 55.34(7) . . ?
C82 C81 Lu1 92.45(7) . . ?
Lu11 C81 Lu1 27.0(2) . . ?
C83 C82 C66 129.0 . . ?
C83 C82 C81 113.9 . . ?
C66 C82 C81 105.4 . . ?
C83 C82 Lu11 93.9(3) . . ?
C66 C82 Lu11 68.3(4) . . ?
C81 C82 Lu11 72.1(3) . . ?
C82 C83 C84 112.4 . . ?
C82 C83 C86 90.8 . . ?
C84 C83 C86 150.2 . . ?
C82 C83 Lu11 57.02(15) . . ?
C84 C83 Lu11 90.5(3) . . ?
C86 C83 Lu11 86.7(3) . . ?
C85 C84 C68 134.1 . . ?
C85 C84 C83 100.8 . . ?
C68 C84 C83 121.4 . . ?
C85 C84 C71 49.9 . . ?
C68 C84 C71 84.2 . . ?
C83 C84 C71 146.1 . . ?
C85 C84 C69 92.2 . . ?
C68 C84 C69 42.1 . . ?
C83 C84 C69 158.2 . . ?
C71 C84 C69 42.3 . . ?
C85 C84 Lu9 107.43(11) . . ?
C68 C84 Lu9 56.53(13) . . ?
C83 C84 Lu9 93.66(12) . . ?
C71 C84 Lu9 82.28(12) . . ?
C69 C84 Lu9 65.56(13) . . ?
C84 C85 C71 85.8 . . ?
C84 C85 C75 134.7 . . ?
C71 C85 C75 128.5 . . ?
C76 C86 C79 106.2 . . ?
C76 C86 C83 86.9 . . ?
C79 C86 C83 151.4 . . ?
C76 C86 C80 133.1 . . ?
C79 C86 C80 32.1 . . ?
C83 C86 C80 122.7 . . ?
N2A Ni1A N2A 177.58(16) . 6_565 ?
N2A Ni1A N3A 89.87(8) . . ?
N2A Ni1A N3A 89.87(8) 6_565 . ?
N2A Ni1A N1A 90.10(8) . . ?
N2A Ni1A N1A 90.10(8) 6_565 . ?
N3A Ni1A N1A 178.49(16) . . ?
C4A N1A C4A 104.6(4) . 6_565 ?
C4A N1A Ni1A 127.7(2) . . ?
C4A N1A Ni1A 127.7(2) 6_565 . ?
C13A N2A C6A 104.5(3) . . ?
C13A N2A Ni1A 127.9(2) . . ?
C6A N2A Ni1A 127.6(2) . . ?
C15A N3A C15A 104.0(4) . 6_565 ?
C15A N3A Ni1A 128.0(2) . . ?
C15A N3A Ni1A 128.0(2) 6_565 . ?
C2A C1A H1AA 109.5 . . ?
C2A C1A H1AB 109.5 . . ?
H1AA C1A H1AB 109.5 . . ?
C2A C1A H1AC 109.5 . . ?
H1AA C1A H1AC 109.5 . . ?
H1AB C1A H1AC 109.5 . . ?
C3A C2A C1A 113.0(4) . . ?
C3A C2A H2AA 109.0 . . ?
C1A C2A H2AA 109.0 . . ?
C3A C2A H2AB 109.0 . . ?
C1A C2A H2AB 109.0 . . ?
H2AA C2A H2AB 107.8 . . ?
C3A C3A C4A 106.4(2) 6_565 . ?
C3A C3A C2A 129.1(2) 6_565 . ?
C4A C3A C2A 124.5(4) . . ?
N1A C4A C5A 125.4(3) . . ?
N1A C4A C3A 111.3(3) . . ?
C5A C4A C3A 123.4(3) . . ?
C4A C5A C6A 123.8(3) . . ?
C4A C5A H5A 118.1 . . ?
C6A C5A H5A 118.1 . . ?
C5A C6A N2A 125.4(3) . . ?
C5A C6A C7A 123.5(3) . . ?
N2A C6A C7A 111.1(3) . . ?
C10A C7A C6A 106.5(3) . . ?
C10A C7A C8A 128.8(4) . . ?
C6A C7A C8A 124.7(3) . . ?
C7A C8A C9A 112.8(3) . . ?
C7A C8A H8AA 109.0 . . ?
C9A C8A H8AA 109.0 . . ?
C7A C8A H8AB 109.0 . . ?
C9A C8A H8AB 109.0 . . ?
H8AA C8A H8AB 107.8 . . ?
C8A C9A H9AA 109.5 . . ?
C8A C9A H9AB 109.5 . . ?
H9AA C9A H9AB 109.5 . . ?
C8A C9A H9AC 109.5 . . ?
H9AA C9A H9AC 109.5 . . ?
H9AB C9A H9AC 109.5 . . ?
C7A C10A C13A 106.2(3) . . ?
C7A C10A C11A 128.3(3) . . ?
C13A C10A C11A 125.5(3) . . ?
C10A C11A C12A 112.2(4) . . ?
C10A C11A H11A 109.2 . . ?
C12A C11A H11A 109.2 . . ?
C10A C11A H11B 109.2 . . ?
C12A C11A H11B 109.2 . . ?
H11A C11A H11B 107.9 . . ?
C11A C12A H12A 109.5 . . ?
C11A C12A H12B 109.5 . . ?
H12A C12A H12B 109.5 . . ?
C11A C12A H12C 109.5 . . ?
H12A C12A H12C 109.5 . . ?
H12B C12A H12C 109.5 . . ?
N2A C13A C14A 125.5(3) . . ?
N2A C13A C10A 111.7(3) . . ?
C14A C13A C10A 122.7(3) . . ?
C15A C14A C13A 123.8(3) . . ?
C15A C14A H14A 118.1 . . ?
C13A C14A H14A 118.1 . . ?
C14A C15A N3A 124.9(3) . . ?
C14A C15A C16A 123.4(3) . . ?
N3A C15A C16A 111.7(3) . . ?
C16A C16A C15A 106.3(2) 6_565 . ?
C16A C16A C17A 128.5(2) 6_565 . ?
C15A C16A C17A 125.1(3) . . ?
C16A C17A C18A 113.4(3) . . ?
C16A C17A H17A 108.9 . . ?
C18A C17A H17A 108.9 . . ?
C16A C17A H17B 108.9 . . ?
C18A C17A H17B 108.9 . . ?
H17A C17A H17B 107.7 . . ?
C17A C18A H18A 109.5 . . ?
C17A C18A H18B 109.5 . . ?
H18A C18A H18B 109.5 . . ?
C17A C18A H18C 109.5 . . ?
H18A C18A H18C 109.5 . . ?
H18B C18A H18C 109.5 . . ?
C2B C1B C2B 112.5(15) 6 . ?
C2B C1B H1BA 123.8 6 . ?
C2B C1B H1BA 123.8 . . ?
C3B C2B C1B 120.7(12) . . ?
C3B C2B H2B 119.6 . . ?
C1B C2B H2B 119.6 . . ?
C4B C3B C2B 116.7(12) . . ?
C4B C3B H3B 121.7 . . ?
C2B C3B H3B 121.7 . . ?
C3B C4B C3B 132.2(17) 6 . ?
C3B C4B H4B 113.9 6 . ?
C3B C4B H4B 113.9 . . ?
C2C C1C C1C 127.3(7) . 2_655 ?
C2C C1C H1C 116.4 . . ?
C1C C1C H1C 116.4 2_655 . ?
C1C C2C C3C 114.2(9) . . ?
C1C C2C H2C 122.9 . . ?
C3C C2C H2C 122.9 . . ?
C2C C3C C3C 118.4(6) . 2_655 ?
C2C C3C H3C 120.8 . . ?
C3C C3C H3C 120.8 2_655 . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Lu4 Lu3 Lu4 Lu6 8.3(8) 6_565 . . . ?
C29 Lu3 Lu4 Lu6 122.1(6) . . . . ?
C28 Lu3 Lu4 Lu6 150.1(5) . . . . ?
Lu6 Lu3 Lu4 Lu6 4.8(5) 6_565 . . . ?
C51 Lu3 Lu4 Lu6 140.1(6) . . . . ?
C30 Lu3 Lu4 Lu6 87.1(6) . . . . ?
C52 Lu3 Lu4 Lu6 95.9(6) . . . . ?
C27 Lu3 Lu4 Lu6 -179.8(5) . . . . ?
Lu9 Lu3 Lu4 Lu6 -88.1(6) 6_565 . . . ?
Lu9 Lu3 Lu4 Lu6 -78.1(6) . . . . ?
C29 Lu3 Lu4 Lu4 113.7(5) . . . 6_565 ?
C28 Lu3 Lu4 Lu4 141.8(6) . . . 6_565 ?
Lu6 Lu3 Lu4 Lu4 -8.3(8) . . . 6_565 ?
Lu6 Lu3 Lu4 Lu4 -3.5(3) 6_565 . . 6_565 ?
C51 Lu3 Lu4 Lu4 131.8(9) . . . 6_565 ?
C30 Lu3 Lu4 Lu4 78.8(4) . . . 6_565 ?
C52 Lu3 Lu4 Lu4 87.6(6) . . . 6_565 ?
C27 Lu3 Lu4 Lu4 171.8(5) . . . 6_565 ?
Lu9 Lu3 Lu4 Lu4 -96.4(4) 6_565 . . 6_565 ?
Lu9 Lu3 Lu4 Lu4 -86.4(4) . . . 6_565 ?
Lu4 Lu3 Lu4 Lu2 -0.3(5) 6_565 . . 6_565 ?
C29 Lu3 Lu4 Lu2 113.48(17) . . . 6_565 ?
C28 Lu3 Lu4 Lu2 141.48(18) . . . 6_565 ?
Lu6 Lu3 Lu4 Lu2 -8.6(5) . . . 6_565 ?
Lu6 Lu3 Lu4 Lu2 -3.8(3) 6_565 . . 6_565 ?
C51 Lu3 Lu4 Lu2 131.5(5) . . . 6_565 ?
C30 Lu3 Lu4 Lu2 78.51(19) . . . 6_565 ?
C52 Lu3 Lu4 Lu2 87.3(3) . . . 6_565 ?
C27 Lu3 Lu4 Lu2 171.57(14) . . . 6_565 ?
Lu9 Lu3 Lu4 Lu2 -96.7(2) 6_565 . . 6_565 ?
Lu9 Lu3 Lu4 Lu2 -86.7(3) . . . 6_565 ?
Lu4 Lu3 Lu4 C11 -112.9(4) 6_565 . . . ?
C29 Lu3 Lu4 C11 0.81(18) . . . . ?
C28 Lu3 Lu4 C11 28.8(3) . . . . ?
Lu6 Lu3 Lu4 C11 -121.3(6) . . . . ?
Lu6 Lu3 Lu4 C11 -116.4(3) 6_565 . . . ?
C51 Lu3 Lu4 C11 18.9(6) . . . . ?
C30 Lu3 Lu4 C11 -34.2(2) . . . . ?
C52 Lu3 Lu4 C11 -25.3(4) . . . . ?
C27 Lu3 Lu4 C11 58.9(2) . . . . ?
Lu9 Lu3 Lu4 C11 150.66(18) 6_565 . . . ?
Lu9 Lu3 Lu4 C11 160.62(19) . . . . ?
Lu4 Lu3 Lu4 C29 -113.7(5) 6_565 . . . ?
C28 Lu3 Lu4 C29 28.01(11) . . . . ?
Lu6 Lu3 Lu4 C29 -122.1(6) . . . . ?
Lu6 Lu3 Lu4 C29 -117.2(3) 6_565 . . . ?
C51 Lu3 Lu4 C29 18.0(4) . . . . ?
C30 Lu3 Lu4 C29 -34.97(6) . . . . ?
C52 Lu3 Lu4 C29 -26.2(2) . . . . ?
C27 Lu3 Lu4 C29 58.10(10) . . . . ?
Lu9 Lu3 Lu4 C29 149.9(2) 6_565 . . . ?
Lu9 Lu3 Lu4 C29 159.8(3) . . . . ?
Lu4 Lu3 Lu4 C10 -153.6(3) 6_565 . . . ?
C29 Lu3 Lu4 C10 -39.85(18) . . . . ?
C28 Lu3 Lu4 C10 -11.8(3) . . . . ?
Lu6 Lu3 Lu4 C10 -161.9(6) . . . . ?
Lu6 Lu3 Lu4 C10 -157.1(2) 6_565 . . . ?
C51 Lu3 Lu4 C10 -21.8(6) . . . . ?
C30 Lu3 Lu4 C10 -74.8(2) . . . . ?
C52 Lu3 Lu4 C10 -66.0(4) . . . . ?
C27 Lu3 Lu4 C10 18.2(2) . . . . ?
Lu9 Lu3 Lu4 C10 110.00(19) 6_565 . . . ?
Lu9 Lu3 Lu4 C10 120.0(2) . . . . ?
Lu4 Lu3 Lu4 C12 -81.1(4) 6_565 . . . ?
C29 Lu3 Lu4 C12 32.7(3) . . . . ?
C28 Lu3 Lu4 C12 60.7(4) . . . . ?
Lu6 Lu3 Lu4 C12 -89.4(7) . . . . ?
Lu6 Lu3 Lu4 C12 -84.6(3) 6_565 . . . ?
C51 Lu3 Lu4 C12 50.7(7) . . . . ?
C30 Lu3 Lu4 C12 -2.3(3) . . . . ?
C52 Lu3 Lu4 C12 6.5(5) . . . . ?
C27 Lu3 Lu4 C12 90.8(3) . . . . ?
Lu9 Lu3 Lu4 C12 -177.5(2) 6_565 . . . ?
Lu9 Lu3 Lu4 C12 -167.5(2) . . . . ?
Lu4 Lu3 Lu4 Lu5 92.2(4) 6_565 . . . ?
C29 Lu3 Lu4 Lu5 -154.0(2) . . . . ?
C28 Lu3 Lu4 Lu5 -126.0(3) . . . . ?
Lu6 Lu3 Lu4 Lu5 83.9(6) . . . . ?
Lu6 Lu3 Lu4 Lu5 88.8(3) 6_565 . . . ?
C51 Lu3 Lu4 Lu5 -136.0(6) . . . . ?
C30 Lu3 Lu4 Lu5 171.0(3) . . . . ?
C52 Lu3 Lu4 Lu5 179.8(4) . . . . ?
C27 Lu3 Lu4 Lu5 -95.9(3) . . . . ?
Lu9 Lu3 Lu4 Lu5 -4.2(3) 6_565 . . . ?
Lu9 Lu3 Lu4 Lu5 5.8(3) . . . . ?
Lu4 Lu3 Lu4 Lu10 7.9(5) 6_565 . . . ?
C29 Lu3 Lu4 Lu10 121.7(2) . . . . ?
C28 Lu3 Lu4 Lu10 149.7(3) . . . . ?
Lu6 Lu3 Lu4 Lu10 -0.4(6) . . . . ?
Lu6 Lu3 Lu4 Lu10 4.4(3) 6_565 . . . ?
C51 Lu3 Lu4 Lu10 139.7(5) . . . . ?
C30 Lu3 Lu4 Lu10 86.7(2) . . . . ?
C52 Lu3 Lu4 Lu10 95.5(4) . . . . ?
C27 Lu3 Lu4 Lu10 179.7(2) . . . . ?
Lu9 Lu3 Lu4 Lu10 -88.5(2) 6_565 . . . ?
Lu9 Lu3 Lu4 Lu10 -78.5(3) . . . . ?
Lu4 Lu3 Lu4 C28 -141.8(6) 6_565 . . . ?
C29 Lu3 Lu4 C28 -28.01(11) . . . . ?
Lu6 Lu3 Lu4 C28 -150.1(5) . . . . ?
Lu6 Lu3 Lu4 C28 -145.2(4) 6_565 . . . ?
C51 Lu3 Lu4 C28 -10.0(3) . . . . ?
C30 Lu3 Lu4 C28 -62.97(14) . . . . ?
C52 Lu3 Lu4 C28 -54.2(2) . . . . ?
C27 Lu3 Lu4 C28 30.09(9) . . . . ?
Lu9 Lu3 Lu4 C28 121.8(3) 6_565 . . . ?
Lu9 Lu3 Lu4 C28 131.8(3) . . . . ?
Lu4 Lu3 Lu4 C30 -78.8(4) 6_565 . . . ?
C29 Lu3 Lu4 C30 34.97(6) . . . . ?
C28 Lu3 Lu4 C30 62.97(14) . . . . ?
Lu6 Lu3 Lu4 C30 -87.1(6) . . . . ?
Lu6 Lu3 Lu4 C30 -82.3(3) 6_565 . . . ?
C51 Lu3 Lu4 C30 53.0(4) . . . . ?
C52 Lu3 Lu4 C30 8.8(2) . . . . ?
C27 Lu3 Lu4 C30 93.06(15) . . . . ?
Lu9 Lu3 Lu4 C30 -175.2(2) 6_565 . . . ?
Lu9 Lu3 Lu4 C30 -165.2(3) . . . . ?
Lu3 Lu4 Lu6 Lu2 -20.5(12) . . . 6_565 ?
Lu4 Lu4 Lu6 Lu2 -16.4(9) 6_565 . . 6_565 ?
C11 Lu4 Lu6 Lu2 105.0(8) . . . 6_565 ?
C29 Lu4 Lu6 Lu2 79.6(9) . . . 6_565 ?
C10 Lu4 Lu6 Lu2 141.4(7) . . . 6_565 ?
C12 Lu4 Lu6 Lu2 100.7(9) . . . 6_565 ?
Lu5 Lu4 Lu6 Lu2 -100.9(8) . . . 6_565 ?
Lu10 Lu4 Lu6 Lu2 -19.7(5) . . . 6_565 ?
C28 Lu4 Lu6 Lu2 83.8(13) . . . 6_565 ?
C30 Lu4 Lu6 Lu2 47.8(9) . . . 6_565 ?
Lu3 Lu4 Lu6 Lu10 -0.8(10) . . . . ?
Lu4 Lu4 Lu6 Lu10 3.4(7) 6_565 . . . ?
Lu2 Lu4 Lu6 Lu10 19.7(5) 6_565 . . . ?
C11 Lu4 Lu6 Lu10 124.8(6) . . . . ?
C29 Lu4 Lu6 Lu10 99.4(6) . . . . ?
C10 Lu4 Lu6 Lu10 161.1(5) . . . . ?
C12 Lu4 Lu6 Lu10 120.4(8) . . . . ?
Lu5 Lu4 Lu6 Lu10 -81.2(7) . . . . ?
C28 Lu4 Lu6 Lu10 103.6(10) . . . . ?
C30 Lu4 Lu6 Lu10 67.6(7) . . . . ?
Lu3 Lu4 Lu6 C12 -121.2(5) . . . . ?
Lu4 Lu4 Lu6 C12 -117.1(2) 6_565 . . . ?
Lu2 Lu4 Lu6 C12 -100.7(9) 6_565 . . . ?
C11 Lu4 Lu6 C12 4.3(3) . . . . ?
C29 Lu4 Lu6 C12 -21.1(6) . . . . ?
C10 Lu4 Lu6 C12 40.7(4) . . . . ?
Lu5 Lu4 Lu6 C12 158.4(3) . . . . ?
Lu10 Lu4 Lu6 C12 -120.4(8) . . . . ?
C28 Lu4 Lu6 C12 -16.9(13) . . . . ?
C30 Lu4 Lu6 C12 -52.9(4) . . . . ?
Lu3 Lu4 Lu6 Lu10 -1.9(8) . . . 6_565 ?
Lu4 Lu4 Lu6 Lu10 2.3(5) 6_565 . . 6_565 ?
Lu2 Lu4 Lu6 Lu10 18.6(6) 6_565 . . 6_565 ?
C11 Lu4 Lu6 Lu10 123.7(4) . . . 6_565 ?
C29 Lu4 Lu6 Lu10 98.3(4) . . . 6_565 ?
C10 Lu4 Lu6 Lu10 160.0(3) . . . 6_565 ?
C12 Lu4 Lu6 Lu10 119.3(6) . . . 6_565 ?
Lu5 Lu4 Lu6 Lu10 -82.3(4) . . . 6_565 ?
Lu10 Lu4 Lu6 Lu10 -1.1(2) . . . 6_565 ?
C28 Lu4 Lu6 Lu10 102.5(10) . . . 6_565 ?
C30 Lu4 Lu6 Lu10 66.5(4) . . . 6_565 ?
Lu3 Lu4 Lu6 C2 -149.4(4) . . . . ?
Lu4 Lu4 Lu6 C2 -145.2(3) 6_565 . . . ?
Lu2 Lu4 Lu6 C2 -128.9(11) 6_565 . . . ?
C11 Lu4 Lu6 C2 -23.9(5) . . . . ?
C29 Lu4 Lu6 C2 -49.2(7) . . . . ?
C10 Lu4 Lu6 C2 12.5(6) . . . . ?
C12 Lu4 Lu6 C2 -28.2(2) . . . . ?
Lu5 Lu4 Lu6 C2 130.2(5) . . . . ?
Lu10 Lu4 Lu6 C2 -148.6(10) . . . . ?
C28 Lu4 Lu6 C2 -45.1(14) . . . . ?
C30 Lu4 Lu6 C2 -81.1(5) . . . . ?
Lu4 Lu4 Lu6 Lu3 4.1(4) 6_565 . . . ?
Lu2 Lu4 Lu6 Lu3 20.5(12) 6_565 . . . ?
C11 Lu4 Lu6 Lu3 125.5(6) . . . . ?
C29 Lu4 Lu6 Lu3 100.2(7) . . . . ?
C10 Lu4 Lu6 Lu3 161.9(7) . . . . ?
C12 Lu4 Lu6 Lu3 121.2(5) . . . . ?
Lu5 Lu4 Lu6 Lu3 -80.4(5) . . . . ?
Lu10 Lu4 Lu6 Lu3 0.8(10) . . . . ?
C28 Lu4 Lu6 Lu3 104.3(13) . . . . ?
C30 Lu4 Lu6 Lu3 68.3(5) . . . . ?
Lu3 Lu4 Lu6 C13 -85.2(6) . . . . ?
Lu4 Lu4 Lu6 C13 -81.0(3) 6_565 . . . ?
Lu2 Lu4 Lu6 C13 -64.7(8) 6_565 . . . ?
C11 Lu4 Lu6 C13 40.4(3) . . . . ?
C29 Lu4 Lu6 C13 15.0(6) . . . . ?
C10 Lu4 Lu6 C13 76.7(4) . . . . ?
C12 Lu4 Lu6 C13 36.05(13) . . . . ?
Lu5 Lu4 Lu6 C13 -165.6(3) . . . . ?
Lu10 Lu4 Lu6 C13 -84.4(8) . . . . ?
C28 Lu4 Lu6 C13 19.2(13) . . . . ?
C30 Lu4 Lu6 C13 -16.8(4) . . . . ?
Lu3 Lu4 Lu6 C3 -145.8(7) . . . . ?
Lu4 Lu4 Lu6 C3 -141.7(8) 6_565 . . . ?
Lu2 Lu4 Lu6 C3 -125.3(15) 6_565 . . . ?
C11 Lu4 Lu6 C3 -20.3(9) . . . . ?
C29 Lu4 Lu6 C3 -45.7(12) . . . . ?
C10 Lu4 Lu6 C3 16.1(10) . . . . ?
C12 Lu4 Lu6 C3 -24.6(6) . . . . ?
Lu5 Lu4 Lu6 C3 133.8(9) . . . . ?
Lu10 Lu4 Lu6 C3 -145.0(14) . . . . ?
C28 Lu4 Lu6 C3 -41.5(18) . . . . ?
C30 Lu4 Lu6 C3 -77.5(9) . . . . ?
Lu3 Lu4 Lu6 Lu2 -9.4(7) . . . . ?
Lu4 Lu4 Lu6 Lu2 -5.3(3) 6_565 . . . ?
Lu2 Lu4 Lu6 Lu2 11.1(6) 6_565 . . . ?
C11 Lu4 Lu6 Lu2 116.1(2) . . . . ?
C29 Lu4 Lu6 Lu2 90.7(4) . . . . ?
C10 Lu4 Lu6 Lu2 152.44(17) . . . . ?
C12 Lu4 Lu6 Lu2 111.8(4) . . . . ?
Lu5 Lu4 Lu6 Lu2 -89.9(3) . . . . ?
Lu10 Lu4 Lu6 Lu2 -8.7(5) . . . . ?
C28 Lu4 Lu6 Lu2 94.9(10) . . . . ?
C30 Lu4 Lu6 Lu2 58.9(3) . . . . ?
Lu3 Lu4 Lu6 Lu8 79.4(7) . . . . ?
Lu4 Lu4 Lu6 Lu8 83.6(5) 6_565 . . . ?
Lu2 Lu4 Lu6 Lu8 99.9(9) 6_565 . . . ?
C11 Lu4 Lu6 Lu8 -155.0(4) . . . . ?
C29 Lu4 Lu6 Lu8 179.6(3) . . . . ?
C10 Lu4 Lu6 Lu8 -118.7(4) . . . . ?
C12 Lu4 Lu6 Lu8 -159.4(6) . . . . ?
Lu5 Lu4 Lu6 Lu8 -1.0(5) . . . . ?
Lu10 Lu4 Lu6 Lu8 80.2(6) . . . . ?
C28 Lu4 Lu6 Lu8 -176.3(8) . . . . ?
C30 Lu4 Lu6 Lu8 147.7(3) . . . . ?
Lu3 Lu4 Lu6 C15 -95.0(12) . . . . ?
Lu4 Lu4 Lu6 C15 -90.8(12) 6_565 . . . ?
Lu2 Lu4 Lu6 C15 -74.4(14) 6_565 . . . ?
C11 Lu4 Lu6 C15 30.6(13) . . . . ?
C29 Lu4 Lu6 C15 5.2(15) . . . . ?
C10 Lu4 Lu6 C15 66.9(13) . . . . ?
C12 Lu4 Lu6 C15 26.3(10) . . . . ?
Lu5 Lu4 Lu6 C15 -175.4(12) . . . . ?
Lu10 Lu4 Lu6 C15 -94.2(16) . . . . ?
C28 Lu4 Lu6 C15 9(2) . . . . ?
C30 Lu4 Lu6 C15 -26.6(13) . . . . ?
Lu9 Lu5 Lu7 Lu11 27.0(13) . . . 6_565 ?
Lu5 Lu5 Lu7 Lu11 29.4(6) 6_565 . . 6_565 ?
Lu11 Lu5 Lu7 Lu11 16.7(4) . . . 6_565 ?
Lu8 Lu5 Lu7 Lu11 56.3(12) . . . 6_565 ?
C45 Lu5 Lu7 Lu11 -82.6(7) . . . 6_565 ?
C23 Lu5 Lu7 Lu11 -121.2(7) . . . 6_565 ?
C44 Lu5 Lu7 Lu11 -71.0(10) . . . 6_565 ?
Lu1 Lu5 Lu7 Lu11 20.1(5) . . . 6_565 ?
Lu7 Lu5 Lu7 Lu11 29.4(6) 6_565 . . 6_565 ?
Lu9 Lu5 Lu7 Lu8 -29(2) . . . . ?
Lu11 Lu5 Lu7 Lu8 -56.3(12) 6_565 . . . ?
Lu5 Lu5 Lu7 Lu8 -26.8(15) 6_565 . . . ?
Lu11 Lu5 Lu7 Lu8 -39.5(14) . . . . ?
C45 Lu5 Lu7 Lu8 -138.8(12) . . . . ?
C23 Lu5 Lu7 Lu8 -177.4(12) . . . . ?
C44 Lu5 Lu7 Lu8 -127.3(11) . . . . ?
Lu1 Lu5 Lu7 Lu8 -36.2(11) . . . . ?
Lu7 Lu5 Lu7 Lu8 -26.8(15) 6_565 . . . ?
Lu9 Lu5 Lu7 Lu9 84(29) . . . 6_565 ?
Lu11 Lu5 Lu7 Lu9 57(29) 6_565 . . 6_565 ?
Lu5 Lu5 Lu7 Lu9 86(29) 6_565 . . 6_565 ?
Lu11 Lu5 Lu7 Lu9 74(29) . . . 6_565 ?
Lu8 Lu5 Lu7 Lu9 113(28) . . . 6_565 ?
C45 Lu5 Lu7 Lu9 -26(28) . . . 6_565 ?
C23 Lu5 Lu7 Lu9 -64(29) . . . 6_565 ?
C44 Lu5 Lu7 Lu9 -14(28) . . . 6_565 ?
Lu1 Lu5 Lu7 Lu9 77(29) . . . 6_565 ?
Lu7 Lu5 Lu7 Lu9 86(29) 6_565 . . 6_565 ?
Lu9 Lu5 Lu7 Lu1 6.9(14) . . . . ?
Lu11 Lu5 Lu7 Lu1 -20.1(5) 6_565 . . . ?
Lu5 Lu5 Lu7 Lu1 9.3(4) 6_565 . . . ?
Lu11 Lu5 Lu7 Lu1 -3.4(4) . . . . ?
Lu8 Lu5 Lu7 Lu1 36.2(11) . . . . ?
C45 Lu5 Lu7 Lu1 -102.7(3) . . . . ?
C23 Lu5 Lu7 Lu1 -141.3(3) . . . . ?
C44 Lu5 Lu7 Lu1 -91.1(7) . . . . ?
Lu7 Lu5 Lu7 Lu1 9.3(4) 6_565 . . . ?
Lu9 Lu5 Lu7 Lu11 10.3(11) . . . . ?
Lu11 Lu5 Lu7 Lu11 -16.7(4) 6_565 . . . ?
Lu5 Lu5 Lu7 Lu11 12.7(3) 6_565 . . . ?
Lu8 Lu5 Lu7 Lu11 39.5(14) . . . . ?
C45 Lu5 Lu7 Lu11 -99.3(6) . . . . ?
C23 Lu5 Lu7 Lu11 -137.9(5) . . . . ?
C44 Lu5 Lu7 Lu11 -87.8(10) . . . . ?
Lu1 Lu5 Lu7 Lu11 3.4(4) . . . . ?
Lu7 Lu5 Lu7 Lu11 12.7(3) 6_565 . . . ?
Lu9 Lu5 Lu7 C42 91.4(12) . . . . ?
Lu11 Lu5 Lu7 C42 64.4(7) 6_565 . . . ?
Lu5 Lu5 Lu7 C42 93.8(4) 6_565 . . . ?
Lu11 Lu5 Lu7 C42 81.1(4) . . . . ?
Lu8 Lu5 Lu7 C42 120.7(15) . . . . ?
C45 Lu5 Lu7 C42 -18.2(6) . . . . ?
C23 Lu5 Lu7 C42 -56.8(5) . . . . ?
C44 Lu5 Lu7 C42 -6.6(11) . . . . ?
Lu1 Lu5 Lu7 C42 84.5(5) . . . . ?
Lu7 Lu5 Lu7 C42 93.8(4) 6_565 . . . ?
Lu9 Lu5 Lu7 C21 135.3(10) . . . . ?
Lu11 Lu5 Lu7 C21 108.3(8) 6_565 . . . ?
Lu5 Lu5 Lu7 C21 137.7(4) 6_565 . . . ?
Lu11 Lu5 Lu7 C21 125.0(5) . . . . ?
Lu8 Lu5 Lu7 C21 164.6(17) . . . . ?
C45 Lu5 Lu7 C21 25.7(8) . . . . ?
C23 Lu5 Lu7 C21 -12.9(7) . . . . ?
C44 Lu5 Lu7 C21 37.3(12) . . . . ?
Lu1 Lu5 Lu7 C21 128.4(7) . . . . ?
Lu7 Lu5 Lu7 C21 137.7(4) 6_565 . . . ?
Lu9 Lu5 Lu7 C43 83.6(13) . . . . ?
Lu11 Lu5 Lu7 C43 56.6(6) 6_565 . . . ?
Lu5 Lu5 Lu7 C43 86.0(3) 6_565 . . . ?
Lu11 Lu5 Lu7 C43 73.3(4) . . . . ?
Lu8 Lu5 Lu7 C43 112.8(13) . . . . ?
C45 Lu5 Lu7 C43 -26.0(3) . . . . ?
C23 Lu5 Lu7 C43 -64.60(19) . . . . ?
C44 Lu5 Lu7 C43 -14.5(7) . . . . ?
Lu1 Lu5 Lu7 C43 76.7(2) . . . . ?
Lu7 Lu5 Lu7 C43 86.0(3) 6_565 . . . ?
Lu11 Lu5 Lu7 Lu9 -27.0(13) 6_565 . . . ?
Lu5 Lu5 Lu7 Lu9 2.4(10) 6_565 . . . ?
Lu11 Lu5 Lu7 Lu9 -10.3(11) . . . . ?
Lu8 Lu5 Lu7 Lu9 29(2) . . . . ?
C45 Lu5 Lu7 Lu9 -109.6(15) . . . . ?
C23 Lu5 Lu7 Lu9 -148.1(15) . . . . ?
C44 Lu5 Lu7 Lu9 -98.0(18) . . . . ?
Lu1 Lu5 Lu7 Lu9 -6.9(14) . . . . ?
Lu7 Lu5 Lu7 Lu9 2.4(10) 6_565 . . . ?
Lu9 Lu5 Lu7 Lu5 -2.4(10) . . . 6_565 ?
Lu11 Lu5 Lu7 Lu5 -29.4(6) 6_565 . . 6_565 ?
Lu11 Lu5 Lu7 Lu5 -12.7(3) . . . 6_565 ?
Lu8 Lu5 Lu7 Lu5 26.8(15) . . . 6_565 ?
C45 Lu5 Lu7 Lu5 -112.0(6) . . . 6_565 ?
C23 Lu5 Lu7 Lu5 -150.6(5) . . . 6_565 ?
C44 Lu5 Lu7 Lu5 -100.5(9) . . . 6_565 ?
Lu1 Lu5 Lu7 Lu5 -9.3(4) . . . 6_565 ?
Lu7 Lu5 Lu7 Lu5 0.002(2) 6_565 . . 6_565 ?
Lu9 Lu5 Lu7 C22 156.3(13) . . . . ?
Lu11 Lu5 Lu7 C22 129.4(6) 6_565 . . . ?
Lu5 Lu5 Lu7 C22 158.8(3) 6_565 . . . ?
Lu11 Lu5 Lu7 C22 146.1(4) . . . . ?
Lu8 Lu5 Lu7 C22 -174.4(14) . . . . ?
C45 Lu5 Lu7 C22 46.8(4) . . . . ?
C23 Lu5 Lu7 C22 8.2(3) . . . . ?
C44 Lu5 Lu7 C22 58.3(8) . . . . ?
Lu1 Lu5 Lu7 C22 149.4(3) . . . . ?
Lu7 Lu5 Lu7 C22 158.8(2) 6_565 . . . ?
Lu11 Lu1 Lu7 Lu11 -36.9(17) . . . 6_565 ?
Lu8 Lu1 Lu7 Lu11 167.2(16) . . . 6_565 ?
Lu8 Lu1 Lu7 Lu11 -76.9(16) 6_565 . . 6_565 ?
Lu7 Lu1 Lu7 Lu11 -54.3(15) 6_565 . . 6_565 ?
C64 Lu1 Lu7 Lu11 46.9(16) . . . 6_565 ?
C63 Lu1 Lu7 Lu11 92.2(15) . . . 6_565 ?
Lu5 Lu1 Lu7 Lu11 -47.5(15) 6_565 . . 6_565 ?
Lu5 Lu1 Lu7 Lu11 -42.4(15) . . . 6_565 ?
C41 Lu1 Lu7 Lu11 98.1(15) . . . 6_565 ?
C65 Lu1 Lu7 Lu11 27.3(15) . . . 6_565 ?
Lu11 Lu1 Lu7 Lu8 155.9(7) . . . . ?
Lu11 Lu1 Lu7 Lu8 -167.2(16) 6_565 . . . ?
Lu8 Lu1 Lu7 Lu8 115.9(7) 6_565 . . . ?
Lu7 Lu1 Lu7 Lu8 138.5(4) 6_565 . . . ?
C64 Lu1 Lu7 Lu8 -120.3(4) . . . . ?
C63 Lu1 Lu7 Lu8 -75.0(5) . . . . ?
Lu5 Lu1 Lu7 Lu8 145.3(5) 6_565 . . . ?
Lu5 Lu1 Lu7 Lu8 150.4(6) . . . . ?
C41 Lu1 Lu7 Lu8 -69.1(4) . . . . ?
C65 Lu1 Lu7 Lu8 -139.9(4) . . . . ?
Lu11 Lu1 Lu7 Lu5 5.4(7) . . . . ?
Lu11 Lu1 Lu7 Lu5 42.4(15) 6_565 . . . ?
Lu8 Lu1 Lu7 Lu5 -150.4(6) . . . . ?
Lu8 Lu1 Lu7 Lu5 -34.5(7) 6_565 . . . ?
Lu7 Lu1 Lu7 Lu5 -12.0(5) 6_565 . . . ?
C64 Lu1 Lu7 Lu5 89.3(4) . . . . ?
C63 Lu1 Lu7 Lu5 134.6(4) . . . . ?
Lu5 Lu1 Lu7 Lu5 -5.2(2) 6_565 . . . ?
C41 Lu1 Lu7 Lu5 140.5(4) . . . . ?
C65 Lu1 Lu7 Lu5 69.7(4) . . . . ?
Lu11 Lu1 Lu7 Lu9 4.3(5) . . . 6_565 ?
Lu11 Lu1 Lu7 Lu9 41.2(15) 6_565 . . 6_565 ?
Lu8 Lu1 Lu7 Lu9 -151.6(5) . . . 6_565 ?
Lu8 Lu1 Lu7 Lu9 -35.7(5) 6_565 . . 6_565 ?
Lu7 Lu1 Lu7 Lu9 -13.1(4) 6_565 . . 6_565 ?
C64 Lu1 Lu7 Lu9 88.1(3) . . . 6_565 ?
C63 Lu1 Lu7 Lu9 133.4(3) . . . 6_565 ?
Lu5 Lu1 Lu7 Lu9 -6.3(4) 6_565 . . 6_565 ?
Lu5 Lu1 Lu7 Lu9 -1.2(5) . . . 6_565 ?
C41 Lu1 Lu7 Lu9 139.3(3) . . . 6_565 ?
C65 Lu1 Lu7 Lu9 68.5(3) . . . 6_565 ?
Lu11 Lu1 Lu7 Lu11 36.9(17) 6_565 . . . ?
Lu8 Lu1 Lu7 Lu11 -155.9(7) . . . . ?
Lu8 Lu1 Lu7 Lu11 -39.9(5) 6_565 . . . ?
Lu7 Lu1 Lu7 Lu11 -17.4(5) 6_565 . . . ?
C64 Lu1 Lu7 Lu11 83.9(5) . . . . ?
C63 Lu1 Lu7 Lu11 129.1(5) . . . . ?
Lu5 Lu1 Lu7 Lu11 -10.6(5) 6_565 . . . ?
Lu5 Lu1 Lu7 Lu11 -5.4(7) . . . . ?
C41 Lu1 Lu7 Lu11 135.0(5) . . . . ?
C65 Lu1 Lu7 Lu11 64.2(5) . . . . ?
Lu11 Lu1 Lu7 C42 -115.0(5) . . . . ?
Lu11 Lu1 Lu7 C42 -78.1(15) 6_565 . . . ?
Lu8 Lu1 Lu7 C42 89.1(5) . . . . ?
Lu8 Lu1 Lu7 C42 -155.0(4) 6_565 . . . ?
Lu7 Lu1 Lu7 C42 -132.42(16) 6_565 . . . ?
C64 Lu1 Lu7 C42 -31.2(2) . . . . ?
C63 Lu1 Lu7 C42 14.1(2) . . . . ?
Lu5 Lu1 Lu7 C42 -125.6(3) 6_565 . . . ?
Lu5 Lu1 Lu7 C42 -120.5(5) . . . . ?
C41 Lu1 Lu7 C42 20.02(11) . . . . ?
C65 Lu1 Lu7 C42 -50.78(14) . . . . ?
Lu11 Lu1 Lu7 C21 -132.6(5) . . . . ?
Lu11 Lu1 Lu7 C21 -95.7(15) 6_565 . . . ?
Lu8 Lu1 Lu7 C21 71.5(5) . . . . ?
Lu8 Lu1 Lu7 C21 -172.5(4) 6_565 . . . ?
Lu7 Lu1 Lu7 C21 -149.99(17) 6_565 . . . ?
C64 Lu1 Lu7 C21 -48.7(4) . . . . ?
C63 Lu1 Lu7 C21 -3.5(3) . . . . ?
Lu5 Lu1 Lu7 C21 -143.2(4) 6_565 . . . ?
Lu5 Lu1 Lu7 C21 -138.0(6) . . . . ?
C41 Lu1 Lu7 C21 2.5(2) . . . . ?
C65 Lu1 Lu7 C21 -68.4(2) . . . . ?
Lu11 Lu1 Lu7 C43 -75.5(5) . . . . ?
Lu11 Lu1 Lu7 C43 -38.6(15) 6_565 . . . ?
Lu8 Lu1 Lu7 C43 128.6(5) . . . . ?
Lu8 Lu1 Lu7 C43 -115.5(4) 6_565 . . . ?
Lu7 Lu1 Lu7 C43 -92.93(19) 6_565 . . . ?
C64 Lu1 Lu7 C43 8.3(2) . . . . ?
C63 Lu1 Lu7 C43 53.58(19) . . . . ?
Lu5 Lu1 Lu7 C43 -86.2(3) 6_565 . . . ?
Lu5 Lu1 Lu7 C43 -81.0(5) . . . . ?
C41 Lu1 Lu7 C43 59.51(10) . . . . ?
C65 Lu1 Lu7 C43 -11.30(10) . . . . ?
Lu11 Lu1 Lu7 Lu9 7.9(4) . . . . ?
Lu11 Lu1 Lu7 Lu9 44.8(15) 6_565 . . . ?
Lu8 Lu1 Lu7 Lu9 -148.0(5) . . . . ?
Lu8 Lu1 Lu7 Lu9 -32.1(5) 6_565 . . . ?
Lu7 Lu1 Lu7 Lu9 -9.5(3) 6_565 . . . ?
C64 Lu1 Lu7 Lu9 91.7(2) . . . . ?
C63 Lu1 Lu7 Lu9 137.0(2) . . . . ?
Lu5 Lu1 Lu7 Lu9 -2.7(3) 6_565 . . . ?
Lu5 Lu1 Lu7 Lu9 2.4(5) . . . . ?
C41 Lu1 Lu7 Lu9 142.92(19) . . . . ?
C65 Lu1 Lu7 Lu9 72.12(18) . . . . ?
Lu11 Lu1 Lu7 Lu5 10.6(5) . . . 6_565 ?
Lu11 Lu1 Lu7 Lu5 47.5(15) 6_565 . . 6_565 ?
Lu8 Lu1 Lu7 Lu5 -145.3(5) . . . 6_565 ?
Lu8 Lu1 Lu7 Lu5 -29.3(5) 6_565 . . 6_565 ?
Lu7 Lu1 Lu7 Lu5 -6.8(3) 6_565 . . 6_565 ?
C64 Lu1 Lu7 Lu5 94.5(3) . . . 6_565 ?
C63 Lu1 Lu7 Lu5 139.7(3) . . . 6_565 ?
Lu5 Lu1 Lu7 Lu5 5.2(2) . . . 6_565 ?
C41 Lu1 Lu7 Lu5 145.7(2) . . . 6_565 ?
C65 Lu1 Lu7 Lu5 74.9(2) . . . 6_565 ?
Lu11 Lu1 Lu7 C22 -102.0(7) . . . . ?
Lu11 Lu1 Lu7 C22 -65.1(16) 6_565 . . . ?
Lu8 Lu1 Lu7 C22 102.1(8) . . . . ?
Lu8 Lu1 Lu7 C22 -142.0(5) 6_565 . . . ?
Lu7 Lu1 Lu7 C22 -119.4(5) 6_565 . . . ?
C64 Lu1 Lu7 C22 -18.2(7) . . . . ?
C63 Lu1 Lu7 C22 27.1(7) . . . . ?
Lu5 Lu1 Lu7 C22 -112.7(7) 6_565 . . . ?
Lu5 Lu1 Lu7 C22 -107.5(8) . . . . ?
C41 Lu1 Lu7 C22 33.0(6) . . . . ?
C65 Lu1 Lu7 C22 -37.8(6) . . . . ?
Lu5 Lu7 Lu8 Lu11 53.5(12) . . . 6_565 ?
Lu9 Lu7 Lu8 Lu11 51.8(10) 6_565 . . 6_565 ?
Lu1 Lu7 Lu8 Lu11 6.3(7) . . . 6_565 ?
Lu11 Lu7 Lu8 Lu11 19.2(6) . . . 6_565 ?
C42 Lu7 Lu8 Lu11 -78.6(7) . . . 6_565 ?
C21 Lu7 Lu8 Lu11 -114.7(7) . . . 6_565 ?
C43 Lu7 Lu8 Lu11 -48.6(8) . . . 6_565 ?
Lu9 Lu7 Lu8 Lu11 42.4(7) . . . 6_565 ?
Lu5 Lu7 Lu8 Lu11 39.5(7) 6_565 . . 6_565 ?
C22 Lu7 Lu8 Lu11 -133.5(9) . . . 6_565 ?
Lu11 Lu7 Lu8 Lu1 -6.3(7) 6_565 . . . ?
Lu5 Lu7 Lu8 Lu1 47.2(13) . . . . ?
Lu9 Lu7 Lu8 Lu1 45.6(10) 6_565 . . . ?
Lu11 Lu7 Lu8 Lu1 12.9(3) . . . . ?
C42 Lu7 Lu8 Lu1 -84.9(3) . . . . ?
C21 Lu7 Lu8 Lu1 -120.9(3) . . . . ?
C43 Lu7 Lu8 Lu1 -54.8(5) . . . . ?
Lu9 Lu7 Lu8 Lu1 36.1(6) . . . . ?
Lu5 Lu7 Lu8 Lu1 33.2(5) 6_565 . . . ?
C22 Lu7 Lu8 Lu1 -139.8(5) . . . . ?
Lu11 Lu7 Lu8 Lu5 -53.5(12) 6_565 . . . ?
Lu9 Lu7 Lu8 Lu5 -1.6(9) 6_565 . . . ?
Lu1 Lu7 Lu8 Lu5 -47.2(13) . . . . ?
Lu11 Lu7 Lu8 Lu5 -34.3(12) . . . . ?
C42 Lu7 Lu8 Lu5 -132.1(13) . . . . ?
C21 Lu7 Lu8 Lu5 -168.2(13) . . . . ?
C43 Lu7 Lu8 Lu5 -102.0(14) . . . . ?
Lu9 Lu7 Lu8 Lu5 -11.1(10) . . . . ?
Lu5 Lu7 Lu8 Lu5 -14.0(9) 6_565 . . . ?
C22 Lu7 Lu8 Lu5 173.0(17) . . . . ?
Lu11 Lu7 Lu8 Lu11 -19.2(6) 6_565 . . . ?
Lu5 Lu7 Lu8 Lu11 34.3(12) . . . . ?
Lu9 Lu7 Lu8 Lu11 32.6(9) 6_565 . . . ?
Lu1 Lu7 Lu8 Lu11 -12.9(3) . . . . ?
C42 Lu7 Lu8 Lu11 -97.8(2) . . . . ?
C21 Lu7 Lu8 Lu11 -133.9(3) . . . . ?
C43 Lu7 Lu8 Lu11 -67.8(4) . . . . ?
Lu9 Lu7 Lu8 Lu11 23.2(5) . . . . ?
Lu5 Lu7 Lu8 Lu11 20.3(4) 6_565 . . . ?
C22 Lu7 Lu8 Lu11 -152.7(6) . . . . ?
Lu11 Lu7 Lu8 C42 78.6(7) 6_565 . . . ?
Lu5 Lu7 Lu8 C42 132.1(13) . . . . ?
Lu9 Lu7 Lu8 C42 130.5(10) 6_565 . . . ?
Lu1 Lu7 Lu8 C42 84.9(3) . . . . ?
Lu11 Lu7 Lu8 C42 97.8(2) . . . . ?
C21 Lu7 Lu8 C42 -36.06(9) . . . . ?
C43 Lu7 Lu8 C42 30.1(3) . . . . ?
Lu9 Lu7 Lu8 C42 121.0(5) . . . . ?
Lu5 Lu7 Lu8 C42 118.1(5) 6_565 . . . ?
C22 Lu7 Lu8 C42 -54.9(5) . . . . ?
Lu11 Lu7 Lu8 C41 66.8(8) 6_565 . . . ?
Lu5 Lu7 Lu8 C41 120.2(10) . . . . ?
Lu9 Lu7 Lu8 C41 118.6(7) 6_565 . . . ?
Lu1 Lu7 Lu8 C41 73.0(4) . . . . ?
Lu11 Lu7 Lu8 C41 86.0(5) . . . . ?
C42 Lu7 Lu8 C41 -11.9(4) . . . . ?
C21 Lu7 Lu8 C41 -47.9(5) . . . . ?
C43 Lu7 Lu8 C41 18.2(7) . . . . ?
Lu9 Lu7 Lu8 C41 109.1(4) . . . . ?
Lu5 Lu7 Lu8 C41 106.3(4) 6_565 . . . ?
C22 Lu7 Lu8 C41 -66.7(9) . . . . ?
Lu11 Lu7 Lu8 Lu9 -51.8(10) 6_565 . . 6_565 ?
Lu5 Lu7 Lu8 Lu9 1.6(9) . . . 6_565 ?
Lu1 Lu7 Lu8 Lu9 -45.6(10) . . . 6_565 ?
Lu11 Lu7 Lu8 Lu9 -32.6(9) . . . 6_565 ?
C42 Lu7 Lu8 Lu9 -130.5(10) . . . 6_565 ?
C21 Lu7 Lu8 Lu9 -166.5(10) . . . 6_565 ?
C43 Lu7 Lu8 Lu9 -100.4(11) . . . 6_565 ?
Lu9 Lu7 Lu8 Lu9 -9.5(5) . . . 6_565 ?
Lu5 Lu7 Lu8 Lu9 -12.3(7) 6_565 . . 6_565 ?
C22 Lu7 Lu8 Lu9 174.7(14) . . . 6_565 ?
Lu11 Lu7 Lu8 Lu6 -124.1(7) 6_565 . . . ?
Lu5 Lu7 Lu8 Lu6 -70.7(13) . . . . ?
Lu9 Lu7 Lu8 Lu6 -72.3(11) 6_565 . . . ?
Lu1 Lu7 Lu8 Lu6 -117.9(4) . . . . ?
Lu11 Lu7 Lu8 Lu6 -104.9(3) . . . . ?
C42 Lu7 Lu8 Lu6 157.2(3) . . . . ?
C21 Lu7 Lu8 Lu6 121.2(3) . . . . ?
C43 Lu7 Lu8 Lu6 -172.7(3) . . . . ?
Lu9 Lu7 Lu8 Lu6 -81.8(6) . . . . ?
Lu5 Lu7 Lu8 Lu6 -84.6(5) 6_565 . . . ?
C22 Lu7 Lu8 Lu6 102.4(5) . . . . ?
Lu11 Lu7 Lu8 C21 114.7(7) 6_565 . . . ?
Lu5 Lu7 Lu8 C21 168.2(13) . . . . ?
Lu9 Lu7 Lu8 C21 166.5(10) 6_565 . . . ?
Lu1 Lu7 Lu8 C21 120.9(3) . . . . ?
Lu11 Lu7 Lu8 C21 133.9(3) . . . . ?
C42 Lu7 Lu8 C21 36.06(9) . . . . ?
C43 Lu7 Lu8 C21 66.1(3) . . . . ?
Lu9 Lu7 Lu8 C21 157.0(6) . . . . ?
Lu5 Lu7 Lu8 C21 154.2(5) 6_565 . . . ?
C22 Lu7 Lu8 C21 -18.8(4) . . . . ?
Lu11 Lu7 Lu8 C40 91.1(11) 6_565 . . . ?
Lu5 Lu7 Lu8 C40 144.6(9) . . . . ?
Lu9 Lu7 Lu8 C40 143.0(5) 6_565 . . . ?
Lu1 Lu7 Lu8 C40 97.4(10) . . . . ?
Lu11 Lu7 Lu8 C40 110.3(10) . . . . ?
C42 Lu7 Lu8 C40 12.5(10) . . . . ?
C21 Lu7 Lu8 C40 -23.5(10) . . . . ?
C43 Lu7 Lu8 C40 42.6(12) . . . . ?
Lu9 Lu7 Lu8 C40 133.5(7) . . . . ?
Lu5 Lu7 Lu8 C40 130.6(8) 6_565 . . . ?
C22 Lu7 Lu8 C40 -42.4(14) . . . . ?
Lu11 Lu7 Lu8 C19 132.7(8) 6_565 . . . ?
Lu5 Lu7 Lu8 C19 -173.8(9) . . . . ?
Lu9 Lu7 Lu8 C19 -175.5(5) 6_565 . . . ?
Lu1 Lu7 Lu8 C19 139.0(7) . . . . ?
Lu11 Lu7 Lu8 C19 151.9(6) . . . . ?
C42 Lu7 Lu8 C19 54.1(6) . . . . ?
C21 Lu7 Lu8 C19 18.0(7) . . . . ?
C43 Lu7 Lu8 C19 84.1(8) . . . . ?
Lu9 Lu7 Lu8 C19 175.1(3) . . . . ?
Lu5 Lu7 Lu8 C19 172.2(4) 6_565 . . . ?
C22 Lu7 Lu8 C19 -0.8(11) . . . . ?
Lu11 Lu1 Lu8 Lu7 -26.5(9) . . . . ?
Lu11 Lu1 Lu8 Lu7 6.0(7) 6_565 . . . ?
Lu8 Lu1 Lu8 Lu7 -84.7(9) 6_565 . . . ?
Lu7 Lu1 Lu8 Lu7 -49.6(6) 6_565 . . . ?
C64 Lu1 Lu8 Lu7 80.5(5) . . . . ?
C63 Lu1 Lu8 Lu7 113.8(4) . . . . ?
Lu5 Lu1 Lu8 Lu7 -32.1(5) 6_565 . . . ?
Lu5 Lu1 Lu8 Lu7 -17.7(4) . . . . ?
C41 Lu1 Lu8 Lu7 103.4(5) . . . . ?
C65 Lu1 Lu8 Lu7 43.8(5) . . . . ?
Lu11 Lu1 Lu8 Lu11 -32.5(11) . . . 6_565 ?
Lu8 Lu1 Lu8 Lu11 -90.8(10) 6_565 . . 6_565 ?
Lu7 Lu1 Lu8 Lu11 -6.0(7) . . . 6_565 ?
Lu7 Lu1 Lu8 Lu11 -55.6(7) 6_565 . . 6_565 ?
C64 Lu1 Lu8 Lu11 74.5(7) . . . 6_565 ?
C63 Lu1 Lu8 Lu11 107.7(6) . . . 6_565 ?
Lu5 Lu1 Lu8 Lu11 -38.1(6) 6_565 . . 6_565 ?
Lu5 Lu1 Lu8 Lu11 -23.7(6) . . . 6_565 ?
C41 Lu1 Lu8 Lu11 97.4(7) . . . 6_565 ?
C65 Lu1 Lu8 Lu11 37.7(7) . . . 6_565 ?
Lu11 Lu1 Lu8 Lu5 -8.8(8) . . . . ?
Lu11 Lu1 Lu8 Lu5 23.7(6) 6_565 . . . ?
Lu8 Lu1 Lu8 Lu5 -67.1(9) 6_565 . . . ?
Lu7 Lu1 Lu8 Lu5 17.7(4) . . . . ?
Lu7 Lu1 Lu8 Lu5 -31.9(5) 6_565 . . . ?
C64 Lu1 Lu8 Lu5 98.2(4) . . . . ?
C63 Lu1 Lu8 Lu5 131.4(3) . . . . ?
Lu5 Lu1 Lu8 Lu5 -14.4(2) 6_565 . . . ?
C41 Lu1 Lu8 Lu5 121.1(3) . . . . ?
C65 Lu1 Lu8 Lu5 61.4(3) . . . . ?
Lu11 Lu1 Lu8 Lu11 32.5(11) 6_565 . . . ?
Lu8 Lu1 Lu8 Lu11 -58.2(8) 6_565 . . . ?
Lu7 Lu1 Lu8 Lu11 26.5(9) . . . . ?
Lu7 Lu1 Lu8 Lu11 -23.1(6) 6_565 . . . ?
C64 Lu1 Lu8 Lu11 107.0(8) . . . . ?
C63 Lu1 Lu8 Lu11 140.3(7) . . . . ?
Lu5 Lu1 Lu8 Lu11 -5.5(7) 6_565 . . . ?
Lu5 Lu1 Lu8 Lu11 8.8(8) . . . . ?
C41 Lu1 Lu8 Lu11 129.9(6) . . . . ?
C65 Lu1 Lu8 Lu11 70.3(7) . . . . ?
Lu11 Lu1 Lu8 C42 -97.0(7) . . . . ?
Lu11 Lu1 Lu8 C42 -64.5(7) 6_565 . . . ?
Lu8 Lu1 Lu8 C42 -155.3(6) 6_565 . . . ?
Lu7 Lu1 Lu8 C42 -70.5(5) . . . . ?
Lu7 Lu1 Lu8 C42 -120.1(2) 6_565 . . . ?
C64 Lu1 Lu8 C42 10.0(5) . . . . ?
C63 Lu1 Lu8 C42 43.2(3) . . . . ?
Lu5 Lu1 Lu8 C42 -102.6(3) 6_565 . . . ?
Lu5 Lu1 Lu8 C42 -88.2(4) . . . . ?
C41 Lu1 Lu8 C42 32.93(10) . . . . ?
C65 Lu1 Lu8 C42 -26.7(3) . . . . ?
Lu11 Lu1 Lu8 C41 -129.9(6) . . . . ?
Lu11 Lu1 Lu8 C41 -97.4(7) 6_565 . . . ?
Lu8 Lu1 Lu8 C41 171.8(7) 6_565 . . . ?
Lu7 Lu1 Lu8 C41 -103.4(5) . . . . ?
Lu7 Lu1 Lu8 C41 -153.0(3) 6_565 . . . ?
C64 Lu1 Lu8 C41 -22.9(4) . . . . ?
C63 Lu1 Lu8 C41 10.3(2) . . . . ?
Lu5 Lu1 Lu8 C41 -135.5(3) 6_565 . . . ?
Lu5 Lu1 Lu8 C41 -121.1(3) . . . . ?
C65 Lu1 Lu8 C41 -59.7(2) . . . . ?
Lu11 Lu1 Lu8 Lu9 -7.3(7) . . . 6_565 ?
Lu11 Lu1 Lu8 Lu9 25.3(6) 6_565 . . 6_565 ?
Lu8 Lu1 Lu8 Lu9 -65.5(8) 6_565 . . 6_565 ?
Lu7 Lu1 Lu8 Lu9 19.2(4) . . . 6_565 ?
Lu7 Lu1 Lu8 Lu9 -30.3(4) 6_565 . . 6_565 ?
C64 Lu1 Lu8 Lu9 99.7(4) . . . 6_565 ?
C63 Lu1 Lu8 Lu9 133.0(2) . . . 6_565 ?
Lu5 Lu1 Lu8 Lu9 -12.8(3) 6_565 . . 6_565 ?
Lu5 Lu1 Lu8 Lu9 1.6(3) . . . 6_565 ?
C41 Lu1 Lu8 Lu9 122.7(3) . . . 6_565 ?
C65 Lu1 Lu8 Lu9 63.0(2) . . . 6_565 ?
Lu11 Lu1 Lu8 Lu6 71.0(10) . . . . ?
Lu11 Lu1 Lu8 Lu6 103.5(8) 6_565 . . . ?
Lu8 Lu1 Lu8 Lu6 12.8(12) 6_565 . . . ?
Lu7 Lu1 Lu8 Lu6 97.5(7) . . . . ?
Lu7 Lu1 Lu8 Lu6 48.0(8) 6_565 . . . ?
C64 Lu1 Lu8 Lu6 178.0(4) . . . . ?
C63 Lu1 Lu8 Lu6 -148.7(5) . . . . ?
Lu5 Lu1 Lu8 Lu6 65.5(6) 6_565 . . . ?
Lu5 Lu1 Lu8 Lu6 79.9(6) . . . . ?
C41 Lu1 Lu8 Lu6 -159.0(7) . . . . ?
C65 Lu1 Lu8 Lu6 141.3(5) . . . . ?
Lu11 Lu1 Lu8 C21 -93.0(7) . . . . ?
Lu11 Lu1 Lu8 C21 -60.5(7) 6_565 . . . ?
Lu8 Lu1 Lu8 C21 -151.3(4) 6_565 . . . ?
Lu7 Lu1 Lu8 C21 -66.5(6) . . . . ?
Lu7 Lu1 Lu8 C21 -116.1(3) 6_565 . . . ?
C64 Lu1 Lu8 C21 14.0(8) . . . . ?
C63 Lu1 Lu8 C21 47.2(5) . . . . ?
Lu5 Lu1 Lu8 C21 -98.6(5) 6_565 . . . ?
Lu5 Lu1 Lu8 C21 -84.2(6) . . . . ?
C41 Lu1 Lu8 C21 36.9(3) . . . . ?
C65 Lu1 Lu8 C21 -22.7(5) . . . . ?
Lu11 Lu1 Lu8 C40 -160.5(6) . . . . ?
Lu11 Lu1 Lu8 C40 -128.0(7) 6_565 . . . ?
Lu8 Lu1 Lu8 C40 141.2(6) 6_565 . . . ?
Lu7 Lu1 Lu8 C40 -134.0(5) . . . . ?
Lu7 Lu1 Lu8 C40 176.4(2) 6_565 . . . ?
C64 Lu1 Lu8 C40 -53.5(5) . . . . ?
C63 Lu1 Lu8 C40 -20.3(3) . . . . ?
Lu5 Lu1 Lu8 C40 -166.1(3) 6_565 . . . ?
Lu5 Lu1 Lu8 C40 -151.7(4) . . . . ?
C41 Lu1 Lu8 C40 -30.59(9) . . . . ?
C65 Lu1 Lu8 C40 -90.3(3) . . . . ?
Lu11 Lu1 Lu8 C19 -165.2(6) . . . . ?
Lu11 Lu1 Lu8 C19 -132.7(8) 6_565 . . . ?
Lu8 Lu1 Lu8 C19 136.5(4) 6_565 . . . ?
Lu7 Lu1 Lu8 C19 -138.7(7) . . . . ?
Lu7 Lu1 Lu8 C19 171.7(3) 6_565 . . . ?
C64 Lu1 Lu8 C19 -58.2(7) . . . . ?
C63 Lu1 Lu8 C19 -25.0(5) . . . . ?
Lu5 Lu1 Lu8 C19 -170.8(4) 6_565 . . . ?
Lu5 Lu1 Lu8 C19 -156.4(6) . . . . ?
C41 Lu1 Lu8 C19 -35.3(3) . . . . ?
C65 Lu1 Lu8 C19 -95.0(5) . . . . ?
Lu9 Lu5 Lu9 Lu5 180.004(11) 6_565 . . 6_565 ?
Lu7 Lu5 Lu9 Lu5 7(3) . . . 6_565 ?
Lu11 Lu5 Lu9 Lu5 25(2) 6_565 . . 6_565 ?
Lu11 Lu5 Lu9 Lu5 19(2) . . . 6_565 ?
Lu8 Lu5 Lu9 Lu5 -3(3) . . . 6_565 ?
C45 Lu5 Lu9 Lu5 113.9(17) . . . 6_565 ?
C23 Lu5 Lu9 Lu5 145.3(13) . . . 6_565 ?
C44 Lu5 Lu9 Lu5 129(2) . . . 6_565 ?
Lu1 Lu5 Lu9 Lu5 13(2) . . . 6_565 ?
Lu7 Lu5 Lu9 Lu5 3.7(17) 6_565 . . 6_565 ?
Lu7 Lu5 Lu9 Lu9 -173(3) . . . 6_565 ?
Lu11 Lu5 Lu9 Lu9 -155(2) 6_565 . . 6_565 ?
Lu5 Lu5 Lu9 Lu9 180(100) 6_565 . . 6_565 ?
Lu11 Lu5 Lu9 Lu9 -161(2) . . . 6_565 ?
Lu8 Lu5 Lu9 Lu9 177(3) . . . 6_565 ?
C45 Lu5 Lu9 Lu9 -66.1(17) . . . 6_565 ?
C23 Lu5 Lu9 Lu9 -34.8(13) . . . 6_565 ?
C44 Lu5 Lu9 Lu9 -51(2) . . . 6_565 ?
Lu1 Lu5 Lu9 Lu9 -167(2) . . . 6_565 ?
Lu7 Lu5 Lu9 Lu9 -176.3(17) 6_565 . . 6_565 ?
Lu9 Lu5 Lu9 Lu11 161(2) 6_565 . . . ?
Lu7 Lu5 Lu9 Lu11 -12.1(13) . . . . ?
Lu11 Lu5 Lu9 Lu11 5.6(5) 6_565 . . . ?
Lu5 Lu5 Lu9 Lu11 -19(2) 6_565 . . . ?
Lu8 Lu5 Lu9 Lu11 -22.7(7) . . . . ?
C45 Lu5 Lu9 Lu11 94.4(6) . . . . ?
C23 Lu5 Lu9 Lu11 125.8(10) . . . . ?
C44 Lu5 Lu9 Lu11 109.8(4) . . . . ?
Lu1 Lu5 Lu9 Lu11 -6.6(4) . . . . ?
Lu7 Lu5 Lu9 Lu11 -15.8(5) 6_565 . . . ?
Lu9 Lu5 Lu9 Lu7 176.3(17) 6_565 . . 6_565 ?
Lu7 Lu5 Lu9 Lu7 3.7(16) . . . 6_565 ?
Lu11 Lu5 Lu9 Lu7 21.4(9) 6_565 . . 6_565 ?
Lu5 Lu5 Lu9 Lu7 -3.7(17) 6_565 . . 6_565 ?
Lu11 Lu5 Lu9 Lu7 15.8(5) . . . 6_565 ?
Lu8 Lu5 Lu9 Lu7 -6.9(11) . . . 6_565 ?
C45 Lu5 Lu9 Lu7 110.2(4) . . . 6_565 ?
C23 Lu5 Lu9 Lu7 141.6(7) . . . 6_565 ?
C44 Lu5 Lu9 Lu7 125.6(4) . . . 6_565 ?
Lu1 Lu5 Lu9 Lu7 9.2(5) . . . 6_565 ?
Lu9 Lu5 Lu9 Lu11 155(2) 6_565 . . 6_565 ?
Lu7 Lu5 Lu9 Lu11 -17.7(9) . . . 6_565 ?
Lu5 Lu5 Lu9 Lu11 -25(2) 6_565 . . 6_565 ?
Lu11 Lu5 Lu9 Lu11 -5.6(5) . . . 6_565 ?
Lu8 Lu5 Lu9 Lu11 -28.3(5) . . . 6_565 ?
C45 Lu5 Lu9 Lu11 88.8(9) . . . 6_565 ?
C23 Lu5 Lu9 Lu11 120.2(13) . . . 6_565 ?
C44 Lu5 Lu9 Lu11 104.2(6) . . . 6_565 ?
Lu1 Lu5 Lu9 Lu11 -12.2(5) . . . 6_565 ?
Lu7 Lu5 Lu9 Lu11 -21.4(9) 6_565 . . 6_565 ?
Lu9 Lu5 Lu9 C44 51(2) 6_565 . . . ?
Lu7 Lu5 Lu9 C44 -122.0(13) . . . . ?
Lu11 Lu5 Lu9 C44 -104.2(6) 6_565 . . . ?
Lu5 Lu5 Lu9 C44 -129(2) 6_565 . . . ?
Lu11 Lu5 Lu9 C44 -109.8(4) . . . . ?
Lu8 Lu5 Lu9 C44 -132.5(8) . . . . ?
C45 Lu5 Lu9 C44 -15.4(4) . . . . ?
C23 Lu5 Lu9 C44 16.0(9) . . . . ?
Lu1 Lu5 Lu9 C44 -116.4(2) . . . . ?
Lu7 Lu5 Lu9 C44 -125.6(4) 6_565 . . . ?
Lu9 Lu5 Lu9 C67 74(2) 6_565 . . . ?
Lu7 Lu5 Lu9 C67 -98.3(12) . . . . ?
Lu11 Lu5 Lu9 C67 -80.6(6) 6_565 . . . ?
Lu5 Lu5 Lu9 C67 -106(2) 6_565 . . . ?
Lu11 Lu5 Lu9 C67 -86.2(5) . . . . ?
Lu8 Lu5 Lu9 C67 -108.9(6) . . . . ?
C45 Lu5 Lu9 C67 8.2(8) . . . . ?
C23 Lu5 Lu9 C67 39.6(12) . . . . ?
C44 Lu5 Lu9 C67 23.7(4) . . . . ?
Lu1 Lu5 Lu9 C67 -92.8(4) . . . . ?
Lu7 Lu5 Lu9 C67 -102.0(7) 6_565 . . . ?
Lu9 Lu5 Lu9 C46 16(2) 6_565 . . . ?
Lu7 Lu5 Lu9 C46 -156.4(11) . . . . ?
Lu11 Lu5 Lu9 C46 -138.7(5) 6_565 . . . ?
Lu5 Lu5 Lu9 C46 -164(2) 6_565 . . . ?
Lu11 Lu5 Lu9 C46 -144.3(5) . . . . ?
Lu8 Lu5 Lu9 C46 -167.0(5) . . . . ?
C45 Lu5 Lu9 C46 -49.9(6) . . . . ?
C23 Lu5 Lu9 C46 -18.5(11) . . . . ?
C44 Lu5 Lu9 C46 -34.5(3) . . . . ?
Lu1 Lu5 Lu9 C46 -150.9(2) . . . . ?
Lu7 Lu5 Lu9 C46 -160.1(6) 6_565 . . . ?
Lu9 Lu5 Lu9 C68 57(3) 6_565 . . . ?
Lu7 Lu5 Lu9 C68 -115.5(10) . . . . ?
Lu11 Lu5 Lu9 C68 -97.7(11) 6_565 . . . ?
Lu5 Lu5 Lu9 C68 -123(3) 6_565 . . . ?
Lu11 Lu5 Lu9 C68 -103.3(12) . . . . ?
Lu8 Lu5 Lu9 C68 -126.0(8) . . . . ?
C45 Lu5 Lu9 C68 -8.9(16) . . . . ?
C23 Lu5 Lu9 C68 22(2) . . . . ?
C44 Lu5 Lu9 C68 6.5(12) . . . . ?
Lu1 Lu5 Lu9 C68 -109.9(11) . . . . ?
Lu7 Lu5 Lu9 C68 -119.1(15) 6_565 . . . ?
Lu9 Lu5 Lu9 Lu7 173(3) 6_565 . . . ?
Lu11 Lu5 Lu9 Lu7 17.7(9) 6_565 . . . ?
Lu5 Lu5 Lu9 Lu7 -7(3) 6_565 . . . ?
Lu11 Lu5 Lu9 Lu7 12.1(13) . . . . ?
Lu8 Lu5 Lu9 Lu7 -10.5(7) . . . . ?
C45 Lu5 Lu9 Lu7 106.5(16) . . . . ?
C23 Lu5 Lu9 Lu7 138(2) . . . . ?
C44 Lu5 Lu9 Lu7 122.0(13) . . . . ?
Lu1 Lu5 Lu9 Lu7 5.5(11) . . . . ?
Lu7 Lu5 Lu9 Lu7 -3.7(16) 6_565 . . . ?
Lu9 Lu5 Lu9 Lu8 -177.8(19) 6_565 . . 6_565 ?
Lu7 Lu5 Lu9 Lu8 9.6(14) . . . 6_565 ?
Lu11 Lu5 Lu9 Lu8 27.3(7) 6_565 . . 6_565 ?
Lu5 Lu5 Lu9 Lu8 2.2(19) 6_565 . . 6_565 ?
Lu11 Lu5 Lu9 Lu8 21.7(4) . . . 6_565 ?
Lu8 Lu5 Lu9 Lu8 -1.0(8) . . . 6_565 ?
C45 Lu5 Lu9 Lu8 116.1(4) . . . 6_565 ?
C23 Lu5 Lu9 Lu8 147.5(8) . . . 6_565 ?
C44 Lu5 Lu9 Lu8 131.5(3) . . . 6_565 ?
Lu1 Lu5 Lu9 Lu8 15.1(3) . . . 6_565 ?
Lu7 Lu5 Lu9 Lu8 5.9(3) 6_565 . . 6_565 ?
Lu6 Lu2 Lu10 Lu10 -108.6(16) 6_565 . . 6_565 ?
Lu2 Lu2 Lu10 Lu10 179.987(9) 6_565 . . 6_565 ?
Lu4 Lu2 Lu10 Lu10 -141.0(7) 6_565 . . 6_565 ?
C33 Lu2 Lu10 Lu10 89.1(6) . . . 6_565 ?
C31 Lu2 Lu10 Lu10 128.5(7) . . . 6_565 ?
C34 Lu2 Lu10 Lu10 85.9(6) . . . 6_565 ?
C57 Lu2 Lu10 Lu10 39.9(4) . . . 6_565 ?
Lu6 Lu2 Lu10 Lu10 -160.8(4) . . . 6_565 ?
C35 Lu2 Lu10 Lu10 53.6(7) . . . 6_565 ?
C58 Lu2 Lu10 Lu10 27.0(5) . . . 6_565 ?
Lu10 Lu2 Lu10 Lu2 -179.987(8) 6_565 . . 6_565 ?
Lu6 Lu2 Lu10 Lu2 71.4(16) 6_565 . . 6_565 ?
Lu4 Lu2 Lu10 Lu2 39.0(7) 6_565 . . 6_565 ?
C33 Lu2 Lu10 Lu2 -90.9(6) . . . 6_565 ?
C31 Lu2 Lu10 Lu2 -51.5(7) . . . 6_565 ?
C34 Lu2 Lu10 Lu2 -94.1(6) . . . 6_565 ?
C57 Lu2 Lu10 Lu2 -140.1(4) . . . 6_565 ?
Lu6 Lu2 Lu10 Lu2 19.2(4) . . . 6_565 ?
C35 Lu2 Lu10 Lu2 -126.4(7) . . . 6_565 ?
C58 Lu2 Lu10 Lu2 -153.0(5) . . . 6_565 ?
Lu10 Lu2 Lu10 Lu6 160.8(4) 6_565 . . . ?
Lu6 Lu2 Lu10 Lu6 52.2(15) 6_565 . . . ?
Lu2 Lu2 Lu10 Lu6 -19.2(4) 6_565 . . . ?
Lu4 Lu2 Lu10 Lu6 19.8(6) 6_565 . . . ?
C33 Lu2 Lu10 Lu6 -110.1(4) . . . . ?
C31 Lu2 Lu10 Lu6 -70.7(5) . . . . ?
C34 Lu2 Lu10 Lu6 -113.3(5) . . . . ?
C57 Lu2 Lu10 Lu6 -159.3(4) . . . . ?
C35 Lu2 Lu10 Lu6 -145.6(5) . . . . ?
C58 Lu2 Lu10 Lu6 -172.2(4) . . . . ?
Lu10 Lu2 Lu10 Lu6 108.6(16) 6_565 . . 6_565 ?
Lu2 Lu2 Lu10 Lu6 -71.4(16) 6_565 . . 6_565 ?
Lu4 Lu2 Lu10 Lu6 -32.4(14) 6_565 . . 6_565 ?
C33 Lu2 Lu10 Lu6 -162.3(15) . . . 6_565 ?
C31 Lu2 Lu10 Lu6 -123.0(15) . . . 6_565 ?
C34 Lu2 Lu10 Lu6 -165.6(14) . . . 6_565 ?
C57 Lu2 Lu10 Lu6 148.5(15) . . . 6_565 ?
Lu6 Lu2 Lu10 Lu6 -52.2(15) . . . 6_565 ?
C35 Lu2 Lu10 Lu6 162.2(14) . . . 6_565 ?
C58 Lu2 Lu10 Lu6 135.6(14) . . . 6_565 ?
Lu10 Lu2 Lu10 C34 -85.9(6) 6_565 . . . ?
Lu6 Lu2 Lu10 C34 165.6(14) 6_565 . . . ?
Lu2 Lu2 Lu10 C34 94.1(6) 6_565 . . . ?
Lu4 Lu2 Lu10 C34 133.1(2) 6_565 . . . ?
C33 Lu2 Lu10 C34 3.3(2) . . . . ?
C31 Lu2 Lu10 C34 42.6(3) . . . . ?
C57 Lu2 Lu10 C34 -45.9(3) . . . . ?
Lu6 Lu2 Lu10 C34 113.3(5) . . . . ?
C35 Lu2 Lu10 C34 -32.29(6) . . . . ?
C58 Lu2 Lu10 C34 -58.86(15) . . . . ?
Lu10 Lu2 Lu10 C14 -112.8(6) 6_565 . . . ?
Lu6 Lu2 Lu10 C14 138.7(14) 6_565 . . . ?
Lu2 Lu2 Lu10 C14 67.2(6) 6_565 . . . ?
Lu4 Lu2 Lu10 C14 106.2(3) 6_565 . . . ?
C33 Lu2 Lu10 C14 -23.6(3) . . . . ?
C31 Lu2 Lu10 C14 15.7(4) . . . . ?
C34 Lu2 Lu10 C14 -26.90(12) . . . . ?
C57 Lu2 Lu10 C14 -72.8(4) . . . . ?
Lu6 Lu2 Lu10 C14 86.4(5) . . . . ?
C35 Lu2 Lu10 C14 -59.19(16) . . . . ?
C58 Lu2 Lu10 C14 -85.8(2) . . . . ?
Lu10 Lu2 Lu10 C16 -70.0(10) 6_565 . . . ?
Lu6 Lu2 Lu10 C16 -178.6(13) 6_565 . . . ?
Lu2 Lu2 Lu10 C16 110.0(10) 6_565 . . . ?
Lu4 Lu2 Lu10 C16 149.0(5) 6_565 . . . ?
C33 Lu2 Lu10 C16 19.1(7) . . . . ?
C31 Lu2 Lu10 C16 58.4(6) . . . . ?
C34 Lu2 Lu10 C16 15.8(5) . . . . ?
C57 Lu2 Lu10 C16 -30.1(8) . . . . ?
Lu6 Lu2 Lu10 C16 129.2(9) . . . . ?
C35 Lu2 Lu10 C16 -16.5(4) . . . . ?
C58 Lu2 Lu10 C16 -43.0(6) . . . . ?
Lu10 Lu2 Lu10 C35 -53.6(7) 6_565 . . . ?
Lu6 Lu2 Lu10 C35 -162.2(14) 6_565 . . . ?
Lu2 Lu2 Lu10 C35 126.4(7) 6_565 . . . ?
Lu4 Lu2 Lu10 C35 165.43(17) 6_565 . . . ?
C33 Lu2 Lu10 C35 35.5(2) . . . . ?
C31 Lu2 Lu10 C35 74.9(2) . . . . ?
C34 Lu2 Lu10 C35 32.29(6) . . . . ?
C57 Lu2 Lu10 C35 -13.6(4) . . . . ?
Lu6 Lu2 Lu10 C35 145.6(5) . . . . ?
C58 Lu2 Lu10 C35 -26.58(18) . . . . ?
Lu10 Lu2 Lu10 C36 -41.2(9) 6_565 . . . ?
Lu6 Lu2 Lu10 C36 -149.8(14) 6_565 . . . ?
Lu2 Lu2 Lu10 C36 138.8(9) 6_565 . . . ?
Lu4 Lu2 Lu10 C36 177.8(2) 6_565 . . . ?
C33 Lu2 Lu10 C36 47.9(4) . . . . ?
C31 Lu2 Lu10 C36 87.3(4) . . . . ?
C34 Lu2 Lu10 C36 44.7(3) . . . . ?
C57 Lu2 Lu10 C36 -1.3(6) . . . . ?
Lu6 Lu2 Lu10 C36 158.0(7) . . . . ?
C35 Lu2 Lu10 C36 12.4(2) . . . . ?
C58 Lu2 Lu10 C36 -14.2(4) . . . . ?
Lu10 Lu2 Lu10 C15 -113.9(7) 6_565 . . . ?
Lu6 Lu2 Lu10 C15 137.5(14) 6_565 . . . ?
Lu2 Lu2 Lu10 C15 66.1(6) 6_565 . . . ?
Lu4 Lu2 Lu10 C15 105.1(5) 6_565 . . . ?
C33 Lu2 Lu10 C15 -24.8(6) . . . . ?
C31 Lu2 Lu10 C15 14.5(6) . . . . ?
C34 Lu2 Lu10 C15 -28.1(4) . . . . ?
C57 Lu2 Lu10 C15 -74.0(6) . . . . ?
Lu6 Lu2 Lu10 C15 85.3(7) . . . . ?
C35 Lu2 Lu10 C15 -60.4(4) . . . . ?
C58 Lu2 Lu10 C15 -86.9(5) . . . . ?
Lu10 Lu2 Lu10 Lu8 90.7(7) 6_565 . . . ?
Lu6 Lu2 Lu10 Lu8 -17.9(16) 6_565 . . . ?
Lu2 Lu2 Lu10 Lu8 -89.3(7) 6_565 . . . ?
Lu4 Lu2 Lu10 Lu8 -50.3(5) 6_565 . . . ?
C33 Lu2 Lu10 Lu8 179.9(4) . . . . ?
C31 Lu2 Lu10 Lu8 -140.8(4) . . . . ?
C34 Lu2 Lu10 Lu8 176.6(5) . . . . ?
C57 Lu2 Lu10 Lu8 130.7(4) . . . . ?
Lu6 Lu2 Lu10 Lu8 -70.1(5) . . . . ?
C35 Lu2 Lu10 Lu8 144.3(5) . . . . ?
C58 Lu2 Lu10 Lu8 117.7(4) . . . . ?
Lu2 Lu6 Lu10 Lu10 91.1(17) 6_565 . . 6_565 ?
Lu4 Lu6 Lu10 Lu10 -4.2(9) . . . 6_565 ?
C12 Lu6 Lu10 Lu10 97.3(6) . . . 6_565 ?
C2 Lu6 Lu10 Lu10 140.0(5) . . . 6_565 ?
Lu3 Lu6 Lu10 Lu10 -4.5(6) . . . 6_565 ?
C13 Lu6 Lu10 Lu10 87.2(4) . . . 6_565 ?
C3 Lu6 Lu10 Lu10 153.8(3) . . . 6_565 ?
Lu2 Lu6 Lu10 Lu10 11.5(3) . . . 6_565 ?
Lu8 Lu6 Lu10 Lu10 -99.4(4) . . . 6_565 ?
C15 Lu6 Lu10 Lu10 142.2(4) . . . 6_565 ?
Lu4 Lu6 Lu10 Lu2 -95.3(18) . . . 6_565 ?
C12 Lu6 Lu10 Lu2 6.2(14) . . . 6_565 ?
Lu10 Lu6 Lu10 Lu2 -91.1(17) 6_565 . . 6_565 ?
C2 Lu6 Lu10 Lu2 49.0(15) . . . 6_565 ?
Lu3 Lu6 Lu10 Lu2 -95.6(17) . . . 6_565 ?
C13 Lu6 Lu10 Lu2 -3.9(14) . . . 6_565 ?
C3 Lu6 Lu10 Lu2 62.7(15) . . . 6_565 ?
Lu2 Lu6 Lu10 Lu2 -79.5(18) . . . 6_565 ?
Lu8 Lu6 Lu10 Lu2 169.6(18) . . . 6_565 ?
C15 Lu6 Lu10 Lu2 51.1(15) . . . 6_565 ?
Lu2 Lu6 Lu10 Lu2 79.5(18) 6_565 . . . ?
Lu4 Lu6 Lu10 Lu2 -15.8(8) . . . . ?
C12 Lu6 Lu10 Lu2 85.7(7) . . . . ?
Lu10 Lu6 Lu10 Lu2 -11.5(3) 6_565 . . . ?
C2 Lu6 Lu10 Lu2 128.5(6) . . . . ?
Lu3 Lu6 Lu10 Lu2 -16.0(6) . . . . ?
C13 Lu6 Lu10 Lu2 75.7(5) . . . . ?
C3 Lu6 Lu10 Lu2 142.3(4) . . . . ?
Lu8 Lu6 Lu10 Lu2 -110.9(4) . . . . ?
C15 Lu6 Lu10 Lu2 130.6(5) . . . . ?
Lu2 Lu6 Lu10 Lu6 91.1(17) 6_565 . . 6_565 ?
Lu4 Lu6 Lu10 Lu6 -4.2(9) . . . 6_565 ?
C12 Lu6 Lu10 Lu6 97.3(6) . . . 6_565 ?
Lu10 Lu6 Lu10 Lu6 0.005(5) 6_565 . . 6_565 ?
C2 Lu6 Lu10 Lu6 140.1(5) . . . 6_565 ?
Lu3 Lu6 Lu10 Lu6 -4.5(6) . . . 6_565 ?
C13 Lu6 Lu10 Lu6 87.2(4) . . . 6_565 ?
C3 Lu6 Lu10 Lu6 153.8(3) . . . 6_565 ?
Lu2 Lu6 Lu10 Lu6 11.6(3) . . . 6_565 ?
Lu8 Lu6 Lu10 Lu6 -99.4(4) . . . 6_565 ?
C15 Lu6 Lu10 Lu6 142.2(4) . . . 6_565 ?
Lu2 Lu6 Lu10 C34 1.2(16) 6_565 . . . ?
Lu4 Lu6 Lu10 C34 -94.1(6) . . . . ?
C12 Lu6 Lu10 C34 7.4(10) . . . . ?
Lu10 Lu6 Lu10 C34 -89.8(7) 6_565 . . . ?
C2 Lu6 Lu10 C34 50.2(10) . . . . ?
Lu3 Lu6 Lu10 C34 -94.3(5) . . . . ?
C13 Lu6 Lu10 C34 -2.6(6) . . . . ?
C3 Lu6 Lu10 C34 64.0(6) . . . . ?
Lu2 Lu6 Lu10 C34 -78.3(7) . . . . ?
Lu8 Lu6 Lu10 C34 170.8(5) . . . . ?
C15 Lu6 Lu10 C34 52.3(4) . . . . ?
Lu2 Lu6 Lu10 C14 -15.1(15) 6_565 . . . ?
Lu4 Lu6 Lu10 C14 -110.4(6) . . . . ?
C12 Lu6 Lu10 C14 -8.9(7) . . . . ?
Lu10 Lu6 Lu10 C14 -106.2(5) 6_565 . . . ?
C2 Lu6 Lu10 C14 33.9(7) . . . . ?
Lu3 Lu6 Lu10 C14 -110.7(4) . . . . ?
C13 Lu6 Lu10 C14 -19.0(3) . . . . ?
C3 Lu6 Lu10 C14 47.6(3) . . . . ?
Lu2 Lu6 Lu10 C14 -94.6(5) . . . . ?
Lu8 Lu6 Lu10 C14 154.5(4) . . . . ?
C15 Lu6 Lu10 C14 35.99(11) . . . . ?
Lu2 Lu6 Lu10 C16 -65.7(16) 6_565 . . . ?
Lu4 Lu6 Lu10 C16 -161.0(5) . . . . ?
C12 Lu6 Lu10 C16 -59.5(8) . . . . ?
Lu10 Lu6 Lu10 C16 -156.8(7) 6_565 . . . ?
C2 Lu6 Lu10 C16 -16.7(9) . . . . ?
Lu3 Lu6 Lu10 C16 -161.3(3) . . . . ?
C13 Lu6 Lu10 C16 -69.6(4) . . . . ?
C3 Lu6 Lu10 C16 -3.0(5) . . . . ?
Lu2 Lu6 Lu10 C16 -145.2(7) . . . . ?
Lu8 Lu6 Lu10 C16 103.8(4) . . . . ?
C15 Lu6 Lu10 C16 -14.6(3) . . . . ?
Lu2 Lu6 Lu10 C35 -13.8(19) 6_565 . . . ?
Lu4 Lu6 Lu10 C35 -109.1(10) . . . . ?
C12 Lu6 Lu10 C35 -7.6(17) . . . . ?
Lu10 Lu6 Lu10 C35 -104.8(14) 6_565 . . . ?
C2 Lu6 Lu10 C35 35.2(17) . . . . ?
Lu3 Lu6 Lu10 C35 -109.3(11) . . . . ?
C13 Lu6 Lu10 C35 -17.6(13) . . . . ?
C3 Lu6 Lu10 C35 49.0(13) . . . . ?
Lu2 Lu6 Lu10 C35 -93.3(13) . . . . ?
Lu8 Lu6 Lu10 C35 155.8(11) . . . . ?
C15 Lu6 Lu10 C35 37.3(11) . . . . ?
Lu2 Lu6 Lu10 C36 -71.7(17) 6_565 . . . ?
Lu4 Lu6 Lu10 C36 -167.0(5) . . . . ?
C12 Lu6 Lu10 C36 -65.5(12) . . . . ?
Lu10 Lu6 Lu10 C36 -162.8(10) 6_565 . . . ?
C2 Lu6 Lu10 C36 -22.7(12) . . . . ?
Lu3 Lu6 Lu10 C36 -167.3(6) . . . . ?
C13 Lu6 Lu10 C36 -75.6(8) . . . . ?
C3 Lu6 Lu10 C36 -9.0(9) . . . . ?
Lu2 Lu6 Lu10 C36 -151.2(11) . . . . ?
Lu8 Lu6 Lu10 C36 97.9(7) . . . . ?
C15 Lu6 Lu10 C36 -20.6(6) . . . . ?
Lu2 Lu6 Lu10 C15 -51.1(15) 6_565 . . . ?
Lu4 Lu6 Lu10 C15 -146.4(6) . . . . ?
C12 Lu6 Lu10 C15 -44.9(6) . . . . ?
Lu10 Lu6 Lu10 C15 -142.2(4) 6_565 . . . ?
C2 Lu6 Lu10 C15 -2.1(6) . . . . ?
Lu3 Lu6 Lu10 C15 -146.6(4) . . . . ?
C13 Lu6 Lu10 C15 -54.9(2) . . . . ?
C3 Lu6 Lu10 C15 11.6(3) . . . . ?
Lu2 Lu6 Lu10 C15 -130.6(5) . . . . ?
Lu8 Lu6 Lu10 C15 118.5(4) . . . . ?
Lu2 Lu6 Lu10 Lu8 -169.6(18) 6_565 . . . ?
Lu4 Lu6 Lu10 Lu8 95.1(6) . . . . ?
C12 Lu6 Lu10 Lu8 -163.4(8) . . . . ?
Lu10 Lu6 Lu10 Lu8 99.4(4) 6_565 . . . ?
C2 Lu6 Lu10 Lu8 -120.6(8) . . . . ?
Lu3 Lu6 Lu10 Lu8 94.9(3) . . . . ?
C13 Lu6 Lu10 Lu8 -173.4(4) . . . . ?
C3 Lu6 Lu10 Lu8 -106.8(4) . . . . ?
Lu2 Lu6 Lu10 Lu8 110.9(4) . . . . ?
C15 Lu6 Lu10 Lu8 -118.5(4) . . . . ?
Lu11 Lu1 Lu11 Lu7 -140.3(14) 6_565 . . 6_565 ?
Lu8 Lu1 Lu11 Lu7 -113.9(16) . . . 6_565 ?
Lu8 Lu1 Lu11 Lu7 8.1(11) 6_565 . . 6_565 ?
Lu7 Lu1 Lu11 Lu7 -126.7(14) . . . 6_565 ?
C64 Lu1 Lu11 Lu7 112.4(15) . . . 6_565 ?
C63 Lu1 Lu11 Lu7 117.8(9) . . . 6_565 ?
Lu5 Lu1 Lu11 Lu7 -98.4(15) 6_565 . . 6_565 ?
Lu5 Lu1 Lu11 Lu7 -123.2(13) . . . 6_565 ?
C41 Lu1 Lu11 Lu7 160.1(8) . . . 6_565 ?
C65 Lu1 Lu11 Lu7 143.0(18) . . . 6_565 ?
Lu11 Lu1 Lu11 Lu8 -148.4(5) 6_565 . . 6_565 ?
Lu8 Lu1 Lu11 Lu8 -122.0(8) . . . 6_565 ?
Lu7 Lu1 Lu11 Lu8 -134.8(5) . . . 6_565 ?
Lu7 Lu1 Lu11 Lu8 -8.1(11) 6_565 . . 6_565 ?
C64 Lu1 Lu11 Lu8 104.3(5) . . . 6_565 ?
C63 Lu1 Lu11 Lu8 109.7(5) . . . 6_565 ?
Lu5 Lu1 Lu11 Lu8 -106.5(19) 6_565 . . 6_565 ?
Lu5 Lu1 Lu11 Lu8 -131.3(5) . . . 6_565 ?
C41 Lu1 Lu11 Lu8 151.9(4) . . . 6_565 ?
C65 Lu1 Lu11 Lu8 134.8(8) . . . 6_565 ?
Lu11 Lu1 Lu11 Lu5 -42(2) 6_565 . . 6_565 ?
Lu8 Lu1 Lu11 Lu5 -15(2) . . . 6_565 ?
Lu8 Lu1 Lu11 Lu5 106.5(19) 6_565 . . 6_565 ?
Lu7 Lu1 Lu11 Lu5 -28(2) . . . 6_565 ?
Lu7 Lu1 Lu11 Lu5 98.4(15) 6_565 . . 6_565 ?
C64 Lu1 Lu11 Lu5 -149(2) . . . 6_565 ?
C63 Lu1 Lu11 Lu5 -143.8(15) . . . 6_565 ?
Lu5 Lu1 Lu11 Lu5 -24.8(17) . . . 6_565 ?
C41 Lu1 Lu11 Lu5 -101.5(16) . . . 6_565 ?
C65 Lu1 Lu11 Lu5 -119(2) . . . 6_565 ?
Lu8 Lu1 Lu11 Lu11 26.4(3) . . . 6_565 ?
Lu8 Lu1 Lu11 Lu11 148.4(5) 6_565 . . 6_565 ?
Lu7 Lu1 Lu11 Lu11 13.6(3) . . . 6_565 ?
Lu7 Lu1 Lu11 Lu11 140.3(14) 6_565 . . 6_565 ?
C64 Lu1 Lu11 Lu11 -107.3(3) . . . 6_565 ?
C63 Lu1 Lu11 Lu11 -101.9(8) . . . 6_565 ?
Lu5 Lu1 Lu11 Lu11 42(2) 6_565 . . 6_565 ?
Lu5 Lu1 Lu11 Lu11 17.1(6) . . . 6_565 ?
C41 Lu1 Lu11 Lu11 -59.6(8) . . . 6_565 ?
C65 Lu1 Lu11 Lu11 -76.7(4) . . . 6_565 ?
Lu11 Lu1 Lu11 Lu9 -29.0(13) 6_565 . . . ?
Lu8 Lu1 Lu11 Lu9 -2.6(15) . . . . ?
Lu8 Lu1 Lu11 Lu9 119.4(10) 6_565 . . . ?
Lu7 Lu1 Lu11 Lu9 -15.4(12) . . . . ?
Lu7 Lu1 Lu11 Lu9 111.3(12) 6_565 . . . ?
C64 Lu1 Lu11 Lu9 -136.3(12) . . . . ?
C63 Lu1 Lu11 Lu9 -130.9(7) . . . . ?
Lu5 Lu1 Lu11 Lu9 12.9(11) 6_565 . . . ?
Lu5 Lu1 Lu11 Lu9 -11.9(9) . . . . ?
C41 Lu1 Lu11 Lu9 -88.7(8) . . . . ?
C65 Lu1 Lu11 Lu9 -105.8(15) . . . . ?
Lu11 Lu1 Lu11 Lu5 -17.1(6) 6_565 . . . ?
Lu8 Lu1 Lu11 Lu5 9.3(8) . . . . ?
Lu8 Lu1 Lu11 Lu5 131.3(5) 6_565 . . . ?
Lu7 Lu1 Lu11 Lu5 -3.5(4) . . . . ?
Lu7 Lu1 Lu11 Lu5 123.2(13) 6_565 . . . ?
C64 Lu1 Lu11 Lu5 -124.4(5) . . . . ?
C63 Lu1 Lu11 Lu5 -119.0(5) . . . . ?
Lu5 Lu1 Lu11 Lu5 24.8(17) 6_565 . . . ?
C41 Lu1 Lu11 Lu5 -76.8(6) . . . . ?
C65 Lu1 Lu11 Lu5 -93.8(8) . . . . ?
Lu11 Lu1 Lu11 Lu9 -17.3(6) 6_565 . . 6_565 ?
Lu8 Lu1 Lu11 Lu9 9.1(8) . . . 6_565 ?
Lu8 Lu1 Lu11 Lu9 131.1(5) 6_565 . . 6_565 ?
Lu7 Lu1 Lu11 Lu9 -3.7(5) . . . 6_565 ?
Lu7 Lu1 Lu11 Lu9 123.0(13) 6_565 . . 6_565 ?
C64 Lu1 Lu11 Lu9 -124.6(5) . . . 6_565 ?
C63 Lu1 Lu11 Lu9 -119.2(5) . . . 6_565 ?
Lu5 Lu1 Lu11 Lu9 24.6(17) 6_565 . . 6_565 ?
Lu5 Lu1 Lu11 Lu9 -0.2(4) . . . 6_565 ?
C41 Lu1 Lu11 Lu9 -76.9(6) . . . 6_565 ?
C65 Lu1 Lu11 Lu9 -94.0(8) . . . 6_565 ?
Lu11 Lu1 Lu11 C65 76.7(4) 6_565 . . . ?
Lu8 Lu1 Lu11 C65 103.1(4) . . . . ?
Lu8 Lu1 Lu11 C65 -134.8(8) 6_565 . . . ?
Lu7 Lu1 Lu11 C65 90.3(4) . . . . ?
Lu7 Lu1 Lu11 C65 -143.0(18) 6_565 . . . ?
C64 Lu1 Lu11 C65 -30.6(4) . . . . ?
C63 Lu1 Lu11 C65 -25.1(11) . . . . ?
Lu5 Lu1 Lu11 C65 119(2) 6_565 . . . ?
Lu5 Lu1 Lu11 C65 93.8(8) . . . . ?
C41 Lu1 Lu11 C65 17.1(11) . . . . ?
Lu11 Lu1 Lu11 Lu7 -13.6(3) 6_565 . . . ?
Lu8 Lu1 Lu11 Lu7 12.8(4) . . . . ?
Lu8 Lu1 Lu11 Lu7 134.8(5) 6_565 . . . ?
Lu7 Lu1 Lu11 Lu7 126.7(14) 6_565 . . . ?
C64 Lu1 Lu11 Lu7 -120.9(2) . . . . ?
C63 Lu1 Lu11 Lu7 -115.5(7) . . . . ?
Lu5 Lu1 Lu11 Lu7 28(2) 6_565 . . . ?
Lu5 Lu1 Lu11 Lu7 3.5(4) . . . . ?
C41 Lu1 Lu11 Lu7 -73.2(7) . . . . ?
C65 Lu1 Lu11 Lu7 -90.3(4) . . . . ?
Lu11 Lu1 Lu11 C66 88.6(11) 6_565 . . . ?
Lu8 Lu1 Lu11 C66 115.0(9) . . . . ?
Lu8 Lu1 Lu11 C66 -122.9(15) 6_565 . . . ?
Lu7 Lu1 Lu11 C66 102.2(11) . . . . ?
Lu7 Lu1 Lu11 C66 -131(2) 6_565 . . . ?
C64 Lu1 Lu11 C66 -18.7(11) . . . . ?
C63 Lu1 Lu11 C66 -13.2(18) . . . . ?
Lu5 Lu1 Lu11 C66 131(3) 6_565 . . . ?
Lu5 Lu1 Lu11 C66 105.7(14) . . . . ?
C41 Lu1 Lu11 C66 29.0(18) . . . . ?
C65 Lu1 Lu11 C66 11.9(7) . . . . ?
Lu11 Lu1 Lu11 Lu8 -26.4(3) 6_565 . . . ?
Lu8 Lu1 Lu11 Lu8 122.0(8) 6_565 . . . ?
Lu7 Lu1 Lu11 Lu8 -12.8(4) . . . . ?
Lu7 Lu1 Lu11 Lu8 113.9(16) 6_565 . . . ?
C64 Lu1 Lu11 Lu8 -133.7(4) . . . . ?
C63 Lu1 Lu11 Lu8 -128.3(10) . . . . ?
Lu5 Lu1 Lu11 Lu8 15(2) 6_565 . . . ?
Lu5 Lu1 Lu11 Lu8 -9.3(8) . . . . ?
C41 Lu1 Lu11 Lu8 -86.1(10) . . . . ?
C65 Lu1 Lu11 Lu8 -103.1(4) . . . . ?
Lu5 Lu9 Lu11 Lu7 5(3) 6_565 . . 6_565 ?
Lu9 Lu9 Lu11 Lu7 155.6(5) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu7 150.3(8) . . . 6_565 ?
Lu11 Lu9 Lu11 Lu7 155.6(5) 6_565 . . 6_565 ?
C44 Lu9 Lu11 Lu7 -131.3(6) . . . 6_565 ?
C67 Lu9 Lu11 Lu7 -96.2(6) . . . 6_565 ?
C46 Lu9 Lu11 Lu7 -109.7(10) . . . 6_565 ?
C68 Lu9 Lu11 Lu7 -62.4(6) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu7 145.8(7) . . . 6_565 ?
Lu8 Lu9 Lu11 Lu7 28.9(8) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu1 -127(3) 6_565 . . . ?
Lu9 Lu9 Lu11 Lu1 23.6(13) 6_565 . . . ?
Lu5 Lu9 Lu11 Lu1 18.3(12) . . . . ?
Lu7 Lu9 Lu11 Lu1 -132.0(15) 6_565 . . . ?
Lu11 Lu9 Lu11 Lu1 23.6(13) 6_565 . . . ?
C44 Lu9 Lu11 Lu1 96.7(12) . . . . ?
C67 Lu9 Lu11 Lu1 131.8(13) . . . . ?
C46 Lu9 Lu11 Lu1 118.3(10) . . . . ?
C68 Lu9 Lu11 Lu1 165.6(11) . . . . ?
Lu7 Lu9 Lu11 Lu1 13.8(11) . . . . ?
Lu8 Lu9 Lu11 Lu1 -103.1(12) 6_565 . . . ?
Lu5 Lu9 Lu11 Lu8 -24(3) 6_565 . . 6_565 ?
Lu9 Lu9 Lu11 Lu8 126.7(9) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu8 121.4(10) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu8 -28.9(8) 6_565 . . 6_565 ?
Lu11 Lu9 Lu11 Lu8 126.7(9) 6_565 . . 6_565 ?
C44 Lu9 Lu11 Lu8 -160.2(8) . . . 6_565 ?
C67 Lu9 Lu11 Lu8 -125.1(9) . . . 6_565 ?
C46 Lu9 Lu11 Lu8 -138.6(8) . . . 6_565 ?
C68 Lu9 Lu11 Lu8 -91.3(9) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu8 116.9(9) . . . 6_565 ?
Lu9 Lu9 Lu11 Lu5 150(3) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu5 145(3) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu5 -5(3) 6_565 . . 6_565 ?
Lu11 Lu9 Lu11 Lu5 150(3) 6_565 . . 6_565 ?
C44 Lu9 Lu11 Lu5 -137(3) . . . 6_565 ?
C67 Lu9 Lu11 Lu5 -101(3) . . . 6_565 ?
C46 Lu9 Lu11 Lu5 -115(3) . . . 6_565 ?
C68 Lu9 Lu11 Lu5 -68(3) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu5 140(3) . . . 6_565 ?
Lu8 Lu9 Lu11 Lu5 24(3) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu11 -150(3) 6_565 . . 6_565 ?
Lu9 Lu9 Lu11 Lu11 -0.001(1) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu11 -5.3(5) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu11 -155.6(5) 6_565 . . 6_565 ?
C44 Lu9 Lu11 Lu11 73.0(3) . . . 6_565 ?
C67 Lu9 Lu11 Lu11 108.2(2) . . . 6_565 ?
C46 Lu9 Lu11 Lu11 94.7(9) . . . 6_565 ?
C68 Lu9 Lu11 Lu11 142.0(3) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu11 -9.8(3) . . . 6_565 ?
Lu8 Lu9 Lu11 Lu11 -126.7(9) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu5 -145(3) 6_565 . . . ?
Lu9 Lu9 Lu11 Lu5 5.3(5) 6_565 . . . ?
Lu7 Lu9 Lu11 Lu5 -150.3(8) 6_565 . . . ?
Lu11 Lu9 Lu11 Lu5 5.3(5) 6_565 . . . ?
C44 Lu9 Lu11 Lu5 78.3(5) . . . . ?
C67 Lu9 Lu11 Lu5 113.5(5) . . . . ?
C46 Lu9 Lu11 Lu5 100.0(9) . . . . ?
C68 Lu9 Lu11 Lu5 147.3(6) . . . . ?
Lu7 Lu9 Lu11 Lu5 -4.5(4) . . . . ?
Lu8 Lu9 Lu11 Lu5 -121.4(10) 6_565 . . . ?
Lu5 Lu9 Lu11 Lu9 -150(3) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 Lu9 -5.3(5) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu9 -155.6(5) 6_565 . . 6_565 ?
Lu11 Lu9 Lu11 Lu9 0.001(2) 6_565 . . 6_565 ?
C44 Lu9 Lu11 Lu9 73.0(3) . . . 6_565 ?
C67 Lu9 Lu11 Lu9 108.2(2) . . . 6_565 ?
C46 Lu9 Lu11 Lu9 94.7(9) . . . 6_565 ?
C68 Lu9 Lu11 Lu9 142.0(3) . . . 6_565 ?
Lu7 Lu9 Lu11 Lu9 -9.8(3) . . . 6_565 ?
Lu8 Lu9 Lu11 Lu9 -126.7(9) 6_565 . . 6_565 ?
Lu5 Lu9 Lu11 C65 135(3) 6_565 . . . ?
Lu9 Lu9 Lu11 C65 -74.8(5) 6_565 . . . ?
Lu5 Lu9 Lu11 C65 -80.1(7) . . . . ?
Lu7 Lu9 Lu11 C65 129.6(8) 6_565 . . . ?
Lu11 Lu9 Lu11 C65 -74.8(5) 6_565 . . . ?
C44 Lu9 Lu11 C65 -1.7(6) . . . . ?
C67 Lu9 Lu11 C65 33.4(5) . . . . ?
C46 Lu9 Lu11 C65 19.9(13) . . . . ?
C68 Lu9 Lu11 C65 67.2(6) . . . . ?
Lu7 Lu9 Lu11 C65 -84.6(6) . . . . ?
Lu8 Lu9 Lu11 C65 158.5(13) 6_565 . . . ?
Lu5 Lu9 Lu11 Lu7 -140(3) 6_565 . . . ?
Lu9 Lu9 Lu11 Lu7 9.8(3) 6_565 . . . ?
Lu5 Lu9 Lu11 Lu7 4.5(4) . . . . ?
Lu7 Lu9 Lu11 Lu7 -145.8(7) 6_565 . . . ?
Lu11 Lu9 Lu11 Lu7 9.8(3) 6_565 . . . ?
C44 Lu9 Lu11 Lu7 82.9(4) . . . . ?
C67 Lu9 Lu11 Lu7 118.0(3) . . . . ?
C46 Lu9 Lu11 Lu7 104.5(9) . . . . ?
C68 Lu9 Lu11 Lu7 151.8(3) . . . . ?
Lu8 Lu9 Lu11 Lu7 -116.9(9) 6_565 . . . ?
Lu5 Lu9 Lu11 C66 102(3) 6_565 . . . ?
Lu9 Lu9 Lu11 C66 -107.8(3) 6_565 . . . ?
Lu5 Lu9 Lu11 C66 -113.0(7) . . . . ?
Lu7 Lu9 Lu11 C66 96.6(6) 6_565 . . . ?
Lu11 Lu9 Lu11 C66 -107.8(3) 6_565 . . . ?
C44 Lu9 Lu11 C66 -34.7(5) . . . . ?
C67 Lu9 Lu11 C66 0.5(3) . . . . ?
C46 Lu9 Lu11 C66 -13.0(11) . . . . ?
C68 Lu9 Lu11 C66 34.2(5) . . . . ?
Lu7 Lu9 Lu11 C66 -117.6(5) . . . . ?
Lu8 Lu9 Lu11 C66 125.5(12) 6_565 . . . ?
Lu5 Lu9 Lu11 Lu8 -128(3) 6_565 . . . ?
Lu9 Lu9 Lu11 Lu8 22.0(4) 6_565 . . . ?
Lu5 Lu9 Lu11 Lu8 16.7(5) . . . . ?
Lu7 Lu9 Lu11 Lu8 -133.6(7) 6_565 . . . ?
Lu11 Lu9 Lu11 Lu8 22.0(4) 6_565 . . . ?
C44 Lu9 Lu11 Lu8 95.0(4) . . . . ?
C67 Lu9 Lu11 Lu8 130.2(4) . . . . ?
C46 Lu9 Lu11 Lu8 116.7(8) . . . . ?
C68 Lu9 Lu11 Lu8 164.0(3) . . . . ?
Lu7 Lu9 Lu11 Lu8 12.2(2) . . . . ?
Lu8 Lu9 Lu11 Lu8 -104.7(9) 6_565 . . . ?
C5 C1 C2 C3 -5.5 . . . . ?
C9 C1 C2 C3 148.2 . . . . ?
Lu6 C1 C2 C3 77.1(4) . . . . ?
C5 C1 C2 C12 -146.4 . . . . ?
C9 C1 C2 C12 7.2 . . . . ?
Lu6 C1 C2 C12 -63.8(4) . . . . ?
C5 C1 C2 Lu6 -82.6(4) . . . . ?
C9 C1 C2 Lu6 71.1(4) . . . . ?
C12 C2 C3 C15 -7.7 . . . . ?
C1 C2 C3 C15 -148.6 . . . . ?
Lu6 C2 C3 C15 -65.4(3) . . . . ?
C12 C2 C3 C4 142.9 . . . . ?
C1 C2 C3 C4 1.9 . . . . ?
Lu6 C2 C3 C4 85.2(3) . . . . ?
C12 C2 C3 Lu6 57.7(3) . . . . ?
C1 C2 C3 Lu6 -83.2(3) . . . . ?
C2 C3 C4 C18 -147.3 . . . . ?
C15 C3 C4 C18 8.6 . . . . ?
Lu6 C3 C4 C18 -77.3(3) . . . . ?
C2 C3 C4 C5 2.5 . . . . ?
C15 C3 C4 C5 158.3 . . . . ?
Lu6 C3 C4 C5 72.5(3) . . . . ?
C2 C3 C4 Lu6 -69.9(3) . . . . ?
C15 C3 C4 Lu6 85.9(3) . . . . ?
C2 C1 C5 C6 149.0 . . . . ?
C9 C1 C5 C6 4.5 . . . . ?
Lu6 C1 C5 C6 91.1(2) . . . . ?
C2 C1 C5 C4 7.5 . . . . ?
C9 C1 C5 C4 -137.0 . . . . ?
Lu6 C1 C5 C4 -50.4(2) . . . . ?
C2 C1 C5 Lu6 57.9(2) . . . . ?
C9 C1 C5 Lu6 -86.6(2) . . . . ?
C18 C4 C5 C6 -7.3 . . . . ?
C3 C4 C5 C6 -150.2 . . . . ?
Lu6 C4 C5 C6 -94.94(17) . . . . ?
C18 C4 C5 C1 135.9 . . . . ?
C3 C4 C5 C1 -7.0 . . . . ?
Lu6 C4 C5 C1 48.27(17) . . . . ?
C18 C4 C5 Lu6 87.66(17) . . . . ?
C3 C4 C5 Lu6 -55.28(17) . . . . ?
C1 C5 C6 C7 -1.4 . . . . ?
C4 C5 C6 C7 143.6 . . . . ?
Lu6 C5 C6 C7 68.6(3) . . . . ?
C1 C5 C6 C20 -140.9 . . . . ?
C4 C5 C6 C20 4.1 . . . . ?
Lu6 C5 C6 C20 -70.9(3) . . . . ?
C5 C6 C7 C22 -140.0 . . . . ?
C20 C6 C7 C22 13.2 . . . . ?
C5 C6 C7 C8 -1.4 . . . . ?
C20 C6 C7 C8 151.7 . . . . ?
C5 C6 C7 Lu7 -95.70(8) . . . . ?
C20 C6 C7 Lu7 57.45(8) . . . . ?
C6 C7 C8 C9 2.2 . . . . ?
C22 C7 C8 C9 152.2 . . . . ?
Lu7 C7 C8 C9 92.97(11) . . . . ?
C6 C7 C8 C25 -135.7 . . . . ?
C22 C7 C8 C25 14.3 . . . . ?
Lu7 C7 C8 C25 -44.92(11) . . . . ?
C25 C8 C9 C10 4.4 . . . . ?
C7 C8 C9 C10 -143.4 . . . . ?
C25 C8 C9 C1 147.5 . . . . ?
C7 C8 C9 C1 -0.4 . . . . ?
C25 C8 C9 Lu4 59.66(6) . . . . ?
C7 C8 C9 Lu4 -88.19(6) . . . . ?
C5 C1 C9 C8 -3.1 . . . . ?
C2 C1 C9 C8 -140.9 . . . . ?
Lu6 C1 C9 C8 -87.23(19) . . . . ?
C5 C1 C9 C10 131.7 . . . . ?
C2 C1 C9 C10 -6.0 . . . . ?
Lu6 C1 C9 C10 47.63(19) . . . . ?
C5 C1 C9 Lu4 86.71(5) . . . . ?
C2 C1 C9 Lu4 -51.00(5) . . . . ?
Lu6 C1 C9 Lu4 2.64(19) . . . . ?
C8 C9 C10 C26 -10.5 . . . . ?
C1 C9 C10 C26 -146.6 . . . . ?
Lu4 C9 C10 C26 -89.11(7) . . . . ?
C8 C9 C10 C11 140.9 . . . . ?
C1 C9 C10 C11 4.8 . . . . ?
Lu4 C9 C10 C11 62.31(7) . . . . ?
C8 C9 C10 Lu4 78.61(7) . . . . ?
C1 C9 C10 Lu4 -57.47(7) . . . . ?
C26 C10 C11 C29 -14.4 . . . . ?
C9 C10 C11 C29 -155.2 . . . . ?
Lu4 C10 C11 C29 -73.70(10) . . . . ?
C26 C10 C11 C12 135.2 . . . . ?
C9 C10 C11 C12 -5.6 . . . . ?
Lu4 C10 C11 C12 75.82(10) . . . . ?
C26 C10 C11 Lu4 59.33(10) . . . . ?
C9 C10 C11 Lu4 -81.47(10) . . . . ?
C26 C10 C11 Lu6 87.3(2) . . . . ?
C9 C10 C11 Lu6 -53.5(2) . . . . ?
Lu4 C10 C11 Lu6 28.0(2) . . . . ?
C26 C10 C11 Lu3 37.11(8) . . . . ?
C9 C10 C11 Lu3 -103.69(8) . . . . ?
Lu4 C10 C11 Lu3 -22.23(9) . . . . ?
C3 C2 C12 C11 -151.0 . . . . ?
C1 C2 C12 C11 -8.8 . . . . ?
Lu6 C2 C12 C11 -86.4(4) . . . . ?
C3 C2 C12 C13 5.0 . . . . ?
C1 C2 C12 C13 147.1 . . . . ?
Lu6 C2 C12 C13 69.5(4) . . . . ?
C3 C2 C12 Lu6 -64.5(4) . . . . ?
C1 C2 C12 Lu6 77.6(4) . . . . ?
C3 C2 C12 Lu4 -90.28(7) . . . . ?
C1 C2 C12 Lu4 51.86(7) . . . . ?
Lu6 C2 C12 Lu4 -25.7(4) . . . . ?
C29 C11 C12 C2 143.6 . . . . ?
C10 C11 C12 C2 8.5 . . . . ?
Lu4 C11 C12 C2 81.14(10) . . . . ?
Lu6 C11 C12 C2 76.9(3) . . . . ?
Lu3 C11 C12 C2 96.24(9) . . . . ?
C29 C11 C12 C13 -13.7 . . . . ?
C10 C11 C12 C13 -148.8 . . . . ?
Lu4 C11 C12 C13 -76.15(10) . . . . ?
Lu6 C11 C12 C13 -80.4(3) . . . . ?
Lu3 C11 C12 C13 -61.05(9) . . . . ?
C29 C11 C12 Lu6 66.7(3) . . . . ?
C10 C11 C12 Lu6 -68.4(3) . . . . ?
Lu4 C11 C12 Lu6 4.2(3) . . . . ?
Lu3 C11 C12 Lu6 19.4(3) . . . . ?
C29 C11 C12 Lu4 62.46(10) . . . . ?
C10 C11 C12 Lu4 -72.65(10) . . . . ?
Lu6 C11 C12 Lu4 -4.2(3) . . . . ?
Lu3 C11 C12 Lu4 15.10(9) . . . . ?
C2 C12 C13 C14 -0.5 . . . . ?
C11 C12 C13 C14 158.5 . . . . ?
Lu6 C12 C13 C14 67.5(4) . . . . ?
Lu4 C12 C13 C14 100.96(7) . . . . ?
C2 C12 C13 C32 -155.0 . . . . ?
C11 C12 C13 C32 3.9 . . . . ?
Lu6 C12 C13 C32 -87.1(4) . . . . ?
Lu4 C12 C13 C32 -53.58(7) . . . . ?
C2 C12 C13 Lu6 -68.0(4) . . . . ?
C11 C12 C13 Lu6 91.0(4) . . . . ?
Lu4 C12 C13 Lu6 33.5(3) . . . . ?
C2 C12 C13 Lu10 -59.19(17) . . . . ?
C11 C12 C13 Lu10 99.76(17) . . . . ?
Lu6 C12 C13 Lu10 8.8(4) . . . . ?
Lu4 C12 C13 Lu10 42.27(17) . . . . ?
C2 C12 C13 Lu4 -101.47(7) . . . . ?
C11 C12 C13 Lu4 57.49(7) . . . . ?
Lu6 C12 C13 Lu4 -33.5(3) . . . . ?
C32 C13 C14 C34 5.4 . . . . ?
C12 C13 C14 C34 -148.2 . . . . ?
Lu6 C13 C14 C34 -92.6(2) . . . . ?
Lu10 C13 C14 C34 -70.1(2) . . . . ?
Lu4 C13 C14 C34 -78.37(9) . . . . ?
C32 C13 C14 C15 151.8 . . . . ?
C12 C13 C14 C15 -1.8 . . . . ?
Lu6 C13 C14 C15 53.9(2) . . . . ?
Lu10 C13 C14 C15 76.4(2) . . . . ?
Lu4 C13 C14 C15 68.08(9) . . . . ?
C32 C13 C14 Lu10 75.4(3) . . . . ?
C12 C13 C14 Lu10 -78.2(2) . . . . ?
Lu6 C13 C14 Lu10 -22.5(3) . . . . ?
Lu4 C13 C14 Lu10 -8.3(2) . . . . ?
C32 C13 C14 Lu6 98.0(2) . . . . ?
C12 C13 C14 Lu6 -55.6(2) . . . . ?
Lu10 C13 C14 Lu6 22.5(3) . . . . ?
Lu4 C13 C14 Lu6 14.2(2) . . . . ?
C32 C13 C14 Lu2 47.82(8) . . . . ?
C12 C13 C14 Lu2 -105.78(8) . . . . ?
Lu6 C13 C14 Lu2 -50.1(2) . . . . ?
Lu10 C13 C14 Lu2 -27.6(2) . . . . ?
Lu4 C13 C14 Lu2 -35.91(8) . . . . ?
C2 C3 C15 C16 144.1 . . . . ?
C4 C3 C15 C16 -6.4 . . . . ?
Lu6 C3 C15 C16 84.9(3) . . . . ?
C2 C3 C15 C14 5.4 . . . . ?
C4 C3 C15 C14 -145.1 . . . . ?
Lu6 C3 C15 C14 -53.8(3) . . . . ?
C2 C3 C15 Lu10 73.3(2) . . . . ?
C4 C3 C15 Lu10 -77.2(2) . . . . ?
Lu6 C3 C15 Lu10 14.1(3) . . . . ?
C2 C3 C15 Lu6 59.2(3) . . . . ?
C4 C3 C15 Lu6 -91.3(3) . . . . ?
C13 C14 C15 C16 -150.1 . . . . ?
C34 C14 C15 C16 -6.0 . . . . ?
Lu10 C14 C15 C16 -64.18(18) . . . . ?
Lu6 C14 C15 C16 -101.7(3) . . . . ?
Lu2 C14 C15 C16 -64.92(7) . . . . ?
C13 C14 C15 C3 -0.1 . . . . ?
C34 C14 C15 C3 144.1 . . . . ?
Lu10 C14 C15 C3 85.89(18) . . . . ?
Lu6 C14 C15 C3 48.3(3) . . . . ?
Lu2 C14 C15 C3 85.16(7) . . . . ?
C13 C14 C15 Lu10 -85.95(18) . . . . ?
C34 C14 C15 Lu10 58.18(18) . . . . ?
Lu6 C14 C15 Lu10 -37.5(3) . . . . ?
Lu2 C14 C15 Lu10 -0.73(17) . . . . ?
C13 C14 C15 Lu6 -48.4(3) . . . . ?
C34 C14 C15 Lu6 95.7(3) . . . . ?
Lu10 C14 C15 Lu6 37.5(3) . . . . ?
Lu2 C14 C15 Lu6 36.8(3) . . . . ?
C3 C15 C16 C36 -124.0 . . . . ?
C14 C15 C16 C36 21.9 . . . . ?
Lu10 C15 C16 C36 -39.8(2) . . . . ?
Lu6 C15 C16 C36 -56.6(2) . . . . ?
C3 C15 C16 C17 -1.2 . . . . ?
C14 C15 C16 C17 144.8 . . . . ?
Lu10 C15 C16 C17 83.0(2) . . . . ?
Lu6 C15 C16 C17 66.2(2) . . . . ?
C3 C15 C16 Lu10 -84.2(2) . . . . ?
C14 C15 C16 Lu10 61.7(2) . . . . ?
Lu6 C15 C16 Lu10 -16.8(3) . . . . ?
C36 C16 C17 C38 9.6 . . . . ?
C15 C16 C17 C38 -144.8 . . . . ?
Lu10 C16 C17 C38 -67.8(2) . . . . ?
C36 C16 C17 C18 161.0 . . . . ?
C15 C16 C17 C18 6.6 . . . . ?
Lu10 C16 C17 C18 83.6(2) . . . . ?
C15 C16 C17 C36 -154.4 . . . . ?
Lu10 C16 C17 C36 -77.4(2) . . . . ?
C36 C16 C17 C37 3.2 . . . . ?
C15 C16 C17 C37 -151.2 . . . . ?
Lu10 C16 C17 C37 -74.2(2) . . . . ?
C36 C16 C17 Lu10 77.4(2) . . . . ?
C15 C16 C17 Lu10 -77.0(2) . . . . ?
C3 C4 C18 C17 -3.9 . . . . ?
C5 C4 C18 C17 -140.1 . . . . ?
Lu6 C4 C18 C17 -59.9(2) . . . . ?
C3 C4 C18 C19 141.9 . . . . ?
C5 C4 C18 C19 5.8 . . . . ?
Lu6 C4 C18 C19 85.9(2) . . . . ?
C38 C17 C18 C4 155.7 . . . . ?
C16 C17 C18 C4 -4.4 . . . . ?
C36 C17 C18 C4 33.4 . . . . ?
C37 C17 C18 C4 131.2 . . . . ?
Lu10 C17 C18 C4 57.44(16) . . . . ?
C38 C17 C18 C19 13.6 . . . . ?
C16 C17 C18 C19 -146.4 . . . . ?
C36 C17 C18 C19 -108.6 . . . . ?
C37 C17 C18 C19 -10.8 . . . . ?
Lu10 C17 C18 C19 -84.58(16) . . . . ?
C4 C18 C19 C40 -152.7 . . . . ?
C17 C18 C19 C40 -5.2 . . . . ?
C4 C18 C19 C20 -1.5 . . . . ?
C17 C18 C19 C20 146.1 . . . . ?
C4 C18 C19 Lu8 -79.7(3) . . . . ?
C17 C18 C19 Lu8 67.8(3) . . . . ?
C40 C19 C20 C21 9.4 . . . . ?
C18 C19 C20 C21 -140.1 . . . . ?
Lu8 C19 C20 C21 -50.69(16) . . . . ?
C40 C19 C20 C6 148.9 . . . . ?
C18 C19 C20 C6 -0.7 . . . . ?
Lu8 C19 C20 C6 88.76(16) . . . . ?
C40 C19 C20 Lu8 60.12(16) . . . . ?
C18 C19 C20 Lu8 -89.44(16) . . . . ?
C40 C19 C20 Lu7 57.91(10) . . . . ?
C18 C19 C20 Lu7 -91.66(10) . . . . ?
Lu8 C19 C20 Lu7 -2.2(2) . . . . ?
C5 C6 C20 C21 138.8 . . . . ?
C7 C6 C20 C21 -10.0 . . . . ?
C5 C6 C20 C19 -1.0 . . . . ?
C7 C6 C20 C19 -149.9 . . . . ?
C5 C6 C20 Lu8 69.7(2) . . . . ?
C7 C6 C20 Lu8 -79.2(2) . . . . ?
C5 C6 C20 Lu7 88.72(10) . . . . ?
C7 C6 C20 Lu7 -60.11(10) . . . . ?
C19 C20 C21 C42 -0.2 . . . . ?
C6 C20 C21 C42 -137.4 . . . . ?
Lu8 C20 C21 C42 -51.4(2) . . . . ?
Lu7 C20 C21 C42 -67.02(14) . . . . ?
C19 C20 C21 C22 144.1 . . . . ?
C6 C20 C21 C22 6.9 . . . . ?
Lu8 C20 C21 C22 92.9(2) . . . . ?
Lu7 C20 C21 C22 77.31(14) . . . . ?
C19 C20 C21 Lu7 66.81(14) . . . . ?
C6 C20 C21 Lu7 -70.41(14) . . . . ?
Lu8 C20 C21 Lu7 15.6(2) . . . . ?
C19 C20 C21 Lu8 51.2(2) . . . . ?
C6 C20 C21 Lu8 -86.0(2) . . . . ?
Lu7 C20 C21 Lu8 -15.6(2) . . . . ?
C6 C7 C22 C23 125.1 . . . . ?
C8 C7 C22 C23 -18.9 . . . . ?
Lu7 C7 C22 C23 70.50(13) . . . . ?
C6 C7 C22 C21 -9.8 . . . . ?
C8 C7 C22 C21 -153.8 . . . . ?
Lu7 C7 C22 C21 -64.40(13) . . . . ?
C6 C7 C22 Lu7 54.57(13) . . . . ?
C8 C7 C22 Lu7 -89.41(13) . . . . ?
C6 C7 C22 Lu5 77.6(2) . . . . ?
C8 C7 C22 Lu5 -66.4(2) . . . . ?
Lu7 C7 C22 Lu5 23.0(2) . . . . ?
C42 C21 C22 C23 8.0 . . . . ?
C20 C21 C22 C23 -139.4 . . . . ?
Lu7 C21 C22 C23 -49.72(16) . . . . ?
Lu8 C21 C22 C23 -58.69(18) . . . . ?
C42 C21 C22 C7 148.1 . . . . ?
C20 C21 C22 C7 0.7 . . . . ?
Lu7 C21 C22 C7 90.36(16) . . . . ?
Lu8 C21 C22 C7 81.39(18) . . . . ?
C42 C21 C22 Lu7 57.73(16) . . . . ?
C20 C21 C22 Lu7 -89.71(16) . . . . ?
Lu8 C21 C22 Lu7 -9.0(2) . . . . ?
C42 C21 C22 Lu5 46.79(16) . . . . ?
C20 C21 C22 Lu5 -100.65(16) . . . . ?
Lu7 C21 C22 Lu5 -10.9(2) . . . . ?
Lu8 C21 C22 Lu5 -19.9(2) . . . . ?
C7 C22 C23 C45 -135.1 . . . . ?
C21 C22 C23 C45 -13.1 . . . . ?
Lu7 C22 C23 C45 -58.34(12) . . . . ?
Lu5 C22 C23 C45 -66.7(3) . . . . ?
C7 C22 C23 C24 15.2 . . . . ?
C21 C22 C23 C24 137.3 . . . . ?
Lu7 C22 C23 C24 92.04(12) . . . . ?
Lu5 C22 C23 C24 83.7(3) . . . . ?
C7 C22 C23 Lu5 -68.4(3) . . . . ?
C21 C22 C23 Lu5 53.7(3) . . . . ?
Lu7 C22 C23 Lu5 8.4(3) . . . . ?
C7 C22 C23 Lu7 -76.81(12) . . . . ?
C21 C22 C23 Lu7 45.28(12) . . . . ?
Lu5 C22 C23 Lu7 -8.4(3) . . . . ?
C22 C23 C24 C47 -154.6 . . . . ?
C45 C23 C24 C47 -0.9 . . . . ?
Lu5 C23 C24 C47 -58.1(2) . . . . ?
Lu7 C23 C24 C47 -75.43(16) . . . . ?
C22 C23 C24 C25 0.1 . . . . ?
C45 C23 C24 C25 153.8 . . . . ?
Lu5 C23 C24 C25 96.6(2) . . . . ?
Lu7 C23 C24 C25 79.27(16) . . . . ?
C22 C23 C24 Lu5 -96.5(2) . . . . ?
C45 C23 C24 Lu5 57.1(2) . . . . ?
Lu7 C23 C24 Lu5 -17.4(3) . . . . ?
C9 C8 C25 C26 3.4 . . . . ?
C7 C8 C25 C26 140.4 . . . . ?
C9 C8 C25 C24 -141.3 . . . . ?
C7 C8 C25 C24 -4.3 . . . . ?
C47 C24 C25 C8 157.5 . . . . ?
C23 C24 C25 C8 -3.7 . . . . ?
Lu5 C24 C25 C8 61.9(3) . . . . ?
C47 C24 C25 C26 23.2 . . . . ?
C23 C24 C25 C26 -138.0 . . . . ?
Lu5 C24 C25 C26 -72.4(3) . . . . ?
C9 C10 C26 C27 153.3 . . . . ?
C11 C10 C26 C27 10.9 . . . . ?
Lu4 C10 C26 C27 61.27(8) . . . . ?
C9 C10 C26 C25 13.0 . . . . ?
C11 C10 C26 C25 -129.4 . . . . ?
Lu4 C10 C26 C25 -79.06(8) . . . . ?
C9 C10 C26 Lu4 92.06(8) . . . . ?
C11 C10 C26 Lu4 -50.33(8) . . . . ?
C9 C10 C26 Lu3 107.27(7) . . . . ?
C11 C10 C26 Lu3 -35.12(7) . . . . ?
Lu4 C10 C26 Lu3 15.21(8) . . . . ?
C8 C25 C26 C10 -10.2 . . . . ?
C24 C25 C26 C10 127.3 . . . . ?
C8 C25 C26 C27 -151.7 . . . . ?
C24 C25 C26 C27 -14.2 . . . . ?
C8 C25 C26 Lu4 -68.39(8) . . . . ?
C24 C25 C26 Lu4 69.12(8) . . . . ?
C8 C25 C26 Lu3 -89.33(10) . . . . ?
C24 C25 C26 Lu3 48.18(10) . . . . ?
C10 C26 C27 C28 4.9 . . . . ?
C25 C26 C27 C28 142.7 . . . . ?
Lu4 C26 C27 C28 54.66(6) . . . . ?
Lu3 C26 C27 C28 57.73(10) . . . . ?
C10 C26 C27 C48 -140.7 . . . . ?
C25 C26 C27 C48 -2.8 . . . . ?
Lu4 C26 C27 C48 -90.90(6) . . . . ?
Lu3 C26 C27 C48 -87.83(10) . . . . ?
C10 C26 C27 Lu3 -52.85(10) . . . . ?
C25 C26 C27 Lu3 85.01(10) . . . . ?
Lu4 C26 C27 Lu3 -3.08(10) . . . . ?
C48 C27 C28 C29 122.5 . . . . ?
C26 C27 C28 C29 -16.4 . . . . ?
Lu3 C27 C28 C29 63.48(10) . . . . ?
C48 C27 C28 C51 -16.7 . . . . ?
C26 C27 C28 C51 -155.6 . . . . ?
Lu3 C27 C28 C51 -75.74(10) . . . . ?
C48 C27 C28 Lu3 59.00(10) . . . . ?
C26 C27 C28 Lu3 -79.90(10) . . . . ?
C48 C27 C28 Lu4 82.50(8) . . . . ?
C26 C27 C28 Lu4 -56.40(8) . . . . ?
Lu3 C27 C28 Lu4 23.50(6) . . . . ?
C27 C28 C29 C11 12.2 . . . . ?
C51 C28 C29 C11 149.3 . . . . ?
Lu3 C28 C29 C11 82.98(10) . . . . ?
Lu4 C28 C29 C11 61.09(9) . . . . ?
C27 C28 C29 C30 -138.5 . . . . ?
C51 C28 C29 C30 -1.4 . . . . ?
Lu3 C28 C29 C30 -67.70(10) . . . . ?
Lu4 C28 C29 C30 -89.59(9) . . . . ?
C27 C28 C29 Lu3 -70.80(10) . . . . ?
C51 C28 C29 Lu3 66.33(10) . . . . ?
Lu4 C28 C29 Lu3 -21.89(7) . . . . ?
C27 C28 C29 Lu4 -48.92(9) . . . . ?
C51 C28 C29 Lu4 88.22(9) . . . . ?
Lu3 C28 C29 Lu4 21.89(7) . . . . ?
C12 C11 C29 C28 -137.8 . . . . ?
C10 C11 C29 C28 4.7 . . . . ?
Lu4 C11 C29 C28 -71.89(8) . . . . ?
Lu6 C11 C29 C28 -89.5(3) . . . . ?
Lu3 C11 C29 C28 -72.48(14) . . . . ?
C12 C11 C29 C30 14.8 . . . . ?
C10 C11 C29 C30 157.2 . . . . ?
Lu4 C11 C29 C30 80.70(8) . . . . ?
Lu6 C11 C29 C30 63.1(3) . . . . ?
Lu3 C11 C29 C30 80.10(14) . . . . ?
C12 C11 C29 Lu3 -65.28(14) . . . . ?
C10 C11 C29 Lu3 77.14(14) . . . . ?
Lu4 C11 C29 Lu3 0.59(13) . . . . ?
Lu6 C11 C29 Lu3 -17.0(3) . . . . ?
C12 C11 C29 Lu4 -65.88(8) . . . . ?
C10 C11 C29 Lu4 76.54(8) . . . . ?
Lu6 C11 C29 Lu4 -17.6(3) . . . . ?
Lu3 C11 C29 Lu4 -0.59(13) . . . . ?
C28 C29 C30 C32 149.8 . . . . ?
C11 C29 C30 C32 -6.6 . . . . ?
Lu3 C29 C30 C32 85.42(12) . . . . ?
Lu4 C29 C30 C32 58.75(9) . . . . ?
C28 C29 C30 C52 -6.5 . . . . ?
C11 C29 C30 C52 -162.9 . . . . ?
Lu3 C29 C30 C52 -70.91(12) . . . . ?
Lu4 C29 C30 C52 -97.57(9) . . . . ?
C28 C29 C30 Lu3 64.40(12) . . . . ?
C11 C29 C30 Lu3 -92.01(12) . . . . ?
Lu4 C29 C30 Lu3 -26.67(10) . . . . ?
C28 C29 C30 Lu4 91.07(9) . . . . ?
C11 C29 C30 Lu4 -65.34(9) . . . . ?
Lu3 C29 C30 Lu4 26.67(10) . . . . ?
C29 C30 C32 C13 0.1 . . . . ?
C52 C30 C32 C13 136.0 . . . . ?
Lu3 C30 C32 C13 64.66(9) . . . . ?
Lu4 C30 C32 C13 47.28(7) . . . . ?
C29 C30 C32 C31 -155.7 . . . . ?
C52 C30 C32 C31 -19.8 . . . . ?
Lu3 C30 C32 C31 -91.15(9) . . . . ?
Lu4 C30 C32 C31 -108.54(7) . . . . ?
C29 C30 C32 Lu2 -98.26(9) . . . . ?
C52 C30 C32 Lu2 37.65(9) . . . . ?
Lu3 C30 C32 Lu2 -33.73(8) . . . . ?
Lu4 C30 C32 Lu2 -51.11(8) . . . . ?
C29 C30 C32 Lu4 -47.15(7) . . . . ?
C52 C30 C32 Lu4 88.76(7) . . . . ?
Lu3 C30 C32 Lu4 17.39(5) . . . . ?
C29 C30 C32 Lu3 -64.54(9) . . . . ?
C52 C30 C32 Lu3 71.38(9) . . . . ?
Lu4 C30 C32 Lu3 -17.39(5) . . . . ?
C29 C30 C32 Lu6 -46.67(19) . . . . ?
C52 C30 C32 Lu6 89.24(19) . . . . ?
Lu3 C30 C32 Lu6 17.86(19) . . . . ?
Lu4 C30 C32 Lu6 0.48(19) . . . . ?
C14 C13 C32 C30 -155.8 . . . . ?
C12 C13 C32 C30 1.5 . . . . ?
Lu6 C13 C32 C30 -62.7(3) . . . . ?
Lu10 C13 C32 C30 -99.19(15) . . . . ?
Lu4 C13 C32 C30 -44.87(5) . . . . ?
C14 C13 C32 C31 -6.7 . . . . ?
C12 C13 C32 C31 150.5 . . . . ?
Lu6 C13 C32 C31 86.4(3) . . . . ?
Lu10 C13 C32 C31 49.90(15) . . . . ?
Lu4 C13 C32 C31 104.23(5) . . . . ?
C14 C13 C32 Lu2 -51.20(6) . . . . ?
C12 C13 C32 Lu2 106.03(6) . . . . ?
Lu6 C13 C32 Lu2 41.9(3) . . . . ?
Lu10 C13 C32 Lu2 5.39(16) . . . . ?
Lu4 C13 C32 Lu2 59.71(6) . . . . ?
C14 C13 C32 Lu4 -110.91(5) . . . . ?
C12 C13 C32 Lu4 46.32(5) . . . . ?
Lu6 C13 C32 Lu4 -17.8(3) . . . . ?
Lu10 C13 C32 Lu4 -54.33(15) . . . . ?
C14 C13 C32 Lu3 -107.75(8) . . . . ?
C12 C13 C32 Lu3 49.48(8) . . . . ?
Lu6 C13 C32 Lu3 -14.7(3) . . . . ?
Lu10 C13 C32 Lu3 -51.17(16) . . . . ?
Lu4 C13 C32 Lu3 3.16(7) . . . . ?
C14 C13 C32 Lu6 -93.1(3) . . . . ?
C12 C13 C32 Lu6 64.1(3) . . . . ?
Lu10 C13 C32 Lu6 -36.5(4) . . . . ?
Lu4 C13 C32 Lu6 17.8(3) . . . . ?
C33 C31 C32 C30 163.5 . . . . ?
C54 C31 C32 C30 9.2 . . . . ?
Lu2 C31 C32 C30 102.54(10) . . . . ?
C33 C31 C32 C13 4.8 . . . . ?
C54 C31 C32 C13 -149.4 . . . . ?
Lu2 C31 C32 C13 -56.12(10) . . . . ?
C33 C31 C32 Lu2 60.96(10) . . . . ?
C54 C31 C32 Lu2 -93.33(10) . . . . ?
C33 C31 C32 Lu4 93.60(7) . . . . ?
C54 C31 C32 Lu4 -60.68(7) . . . . ?
Lu2 C31 C32 Lu4 32.65(10) . . . . ?
C33 C31 C32 Lu3 109.24(8) . . . . ?
C54 C31 C32 Lu3 -45.04(8) . . . . ?
Lu2 C31 C32 Lu3 48.29(11) . . . . ?
C33 C31 C32 Lu6 63.3(3) . . . . ?
C54 C31 C32 Lu6 -91.0(3) . . . . ?
Lu2 C31 C32 Lu6 2.4(3) . . . . ?
C32 C31 C33 C34 -1.7 . . . . ?
C54 C31 C33 C34 158.1 . . . . ?
Lu2 C31 C33 C34 74.04(13) . . . . ?
C32 C31 C33 C57 -144.1 . . . . ?
C54 C31 C33 C57 15.8 . . . . ?
Lu2 C31 C33 C57 -68.35(13) . . . . ?
C32 C31 C33 Lu2 -75.76(13) . . . . ?
C54 C31 C33 Lu2 84.10(13) . . . . ?
C32 C31 C33 Lu10 -51.65(14) . . . . ?
C54 C31 C33 Lu10 108.21(14) . . . . ?
Lu2 C31 C33 Lu10 24.11(18) . . . . ?
C13 C14 C34 C35 140.0 . . . . ?
C15 C14 C34 C35 -0.5 . . . . ?
Lu10 C14 C34 C35 59.8(2) . . . . ?
Lu6 C14 C34 C35 75.6(3) . . . . ?
Lu2 C14 C34 C35 86.13(10) . . . . ?
C13 C14 C34 C33 -3.0 . . . . ?
C15 C14 C34 C33 -143.6 . . . . ?
Lu10 C14 C34 C33 -83.3(2) . . . . ?
Lu6 C14 C34 C33 -67.5(3) . . . . ?
Lu2 C14 C34 C33 -56.95(10) . . . . ?
C13 C14 C34 Lu10 80.3(2) . . . . ?
C15 C14 C34 Lu10 -60.2(2) . . . . ?
Lu6 C14 C34 Lu10 15.8(4) . . . . ?
Lu2 C14 C34 Lu10 26.4(2) . . . . ?
C13 C14 C34 Lu2 53.92(10) . . . . ?
C15 C14 C34 Lu2 -86.60(10) . . . . ?
Lu10 C14 C34 Lu2 -26.4(2) . . . . ?
Lu6 C14 C34 Lu2 -10.6(3) . . . . ?
C31 C33 C34 C35 -149.4 . . . . ?
C57 C33 C34 C35 -4.3 . . . . ?
Lu2 C33 C34 C35 -76.02(10) . . . . ?
Lu10 C33 C34 C35 -78.71(19) . . . . ?
C31 C33 C34 C14 1.1 . . . . ?
C57 C33 C34 C14 146.2 . . . . ?
Lu2 C33 C34 C14 74.52(10) . . . . ?
Lu10 C33 C34 C14 71.83(19) . . . . ?
C31 C33 C34 Lu10 -70.74(19) . . . . ?
C57 C33 C34 Lu10 74.37(19) . . . . ?
Lu2 C33 C34 Lu10 2.69(18) . . . . ?
C31 C33 C34 Lu2 -73.42(10) . . . . ?
C57 C33 C34 Lu2 71.68(10) . . . . ?
Lu10 C33 C34 Lu2 -2.69(18) . . . . ?
C14 C34 C35 C36 1.4 . . . . ?
C33 C34 C35 C36 150.7 . . . . ?
Lu10 C34 C35 C36 58.8(2) . . . . ?
Lu2 C34 C35 C36 93.00(11) . . . . ?
C14 C34 C35 C58 -142.6 . . . . ?
C33 C34 C35 C58 6.7 . . . . ?
Lu10 C34 C35 C58 -85.3(2) . . . . ?
Lu2 C34 C35 C58 -51.06(11) . . . . ?
C14 C34 C35 Lu10 -57.4(2) . . . . ?
C33 C34 C35 Lu10 91.9(2) . . . . ?
Lu2 C34 C35 Lu10 34.2(2) . . . . ?
C14 C34 C35 Lu2 -91.58(11) . . . . ?
C33 C34 C35 Lu2 57.74(11) . . . . ?
Lu10 C34 C35 Lu2 -34.2(2) . . . . ?
C15 C16 C36 C37 123.3 . . . . ?
C17 C16 C36 C37 -5.6 . . . . ?
Lu10 C16 C36 C37 83.3(2) . . . . ?
C15 C16 C36 C35 -22.2 . . . . ?
C17 C16 C36 C35 -151.1 . . . . ?
Lu10 C16 C36 C35 -62.3(2) . . . . ?
C15 C16 C36 C17 128.9 . . . . ?
Lu10 C16 C36 C17 88.9(2) . . . . ?
C15 C16 C36 Lu10 40.1(2) . . . . ?
C17 C16 C36 Lu10 -88.9(2) . . . . ?
C34 C35 C36 C16 4.7 . . . . ?
C58 C35 C36 C16 147.6 . . . . ?
Lu10 C35 C36 C16 62.62(18) . . . . ?
Lu2 C35 C36 C16 72.64(8) . . . . ?
C34 C35 C36 C37 -142.5 . . . . ?
C58 C35 C36 C37 0.5 . . . . ?
Lu10 C35 C36 C37 -84.51(18) . . . . ?
Lu2 C35 C36 C37 -74.49(8) . . . . ?
C34 C35 C36 C17 -37.5 . . . . ?
C58 C35 C36 C17 105.4 . . . . ?
Lu10 C35 C36 C17 20.45(18) . . . . ?
Lu2 C35 C36 C17 30.47(8) . . . . ?
C34 C35 C36 Lu10 -57.96(18) . . . . ?
C58 C35 C36 Lu10 84.96(18) . . . . ?
Lu2 C35 C36 Lu10 10.02(18) . . . . ?
C38 C17 C36 C16 -173.3 . . . . ?
C18 C17 C36 C16 -49.4 . . . . ?
C37 C17 C36 C16 -175.1 . . . . ?
Lu10 C17 C36 C16 -76.70(18) . . . . ?
C38 C17 C36 C37 1.8 . . . . ?
C18 C17 C36 C37 125.7 . . . . ?
C16 C17 C36 C37 175.1 . . . . ?
Lu10 C17 C36 C37 98.40(18) . . . . ?
C38 C17 C36 C35 -116.4 . . . . ?
C18 C17 C36 C35 7.5 . . . . ?
C16 C17 C36 C35 56.9 . . . . ?
C37 C17 C36 C35 -118.2 . . . . ?
Lu10 C17 C36 C35 -19.81(18) . . . . ?
C38 C17 C36 Lu10 -96.58(18) . . . . ?
C18 C17 C36 Lu10 27.27(18) . . . . ?
C16 C17 C36 Lu10 76.70(18) . . . . ?
C37 C17 C36 Lu10 -98.40(18) . . . . ?
C16 C36 C37 C38 2.8 . . . . ?
C35 C36 C37 C38 145.0 . . . . ?
C17 C36 C37 C38 -1.6 . . . . ?
Lu10 C36 C37 C38 74.0(2) . . . . ?
C16 C36 C37 C60 -145.2 . . . . ?
C35 C36 C37 C60 -3.0 . . . . ?
C17 C36 C37 C60 -149.6 . . . . ?
Lu10 C36 C37 C60 -74.0(2) . . . . ?
C16 C36 C37 C17 4.4 . . . . ?
C35 C36 C37 C17 146.6 . . . . ?
Lu10 C36 C37 C17 75.6(2) . . . . ?
C16 C36 C37 C39 -19.7 . . . . ?
C35 C36 C37 C39 122.4 . . . . ?
C17 C36 C37 C39 -24.2 . . . . ?
Lu10 C36 C37 C39 51.4(2) . . . . ?
C16 C36 C37 Lu10 -71.2(2) . . . . ?
C35 C36 C37 Lu10 71.0(2) . . . . ?
C17 C36 C37 Lu10 -75.6(2) . . . . ?
C18 C17 C38 C39 -63.3 . . . . ?
C16 C17 C38 C39 91.6 . . . . ?
C36 C17 C38 C39 98.3 . . . . ?
C37 C17 C38 C39 99.8 . . . . ?
Lu10 C17 C38 C39 36.74(17) . . . . ?
C18 C17 C38 C37 -163.1 . . . . ?
C16 C17 C38 C37 -8.3 . . . . ?
C36 C17 C38 C37 -1.6 . . . . ?
Lu10 C17 C38 C37 -63.10(18) . . . . ?
C18 C17 C38 C40 -15.5 . . . . ?
C16 C17 C38 C40 139.4 . . . . ?
C36 C17 C38 C40 146.1 . . . . ?
C37 C17 C38 C40 147.7 . . . . ?
Lu10 C17 C38 C40 84.57(18) . . . . ?
C36 C37 C38 C39 -156.0 . . . . ?
C60 C37 C38 C39 -8.8 . . . . ?
C17 C37 C38 C39 -158.3 . . . . ?
Lu10 C37 C38 C39 -100.83(13) . . . . ?
C36 C37 C38 C17 2.2 . . . . ?
C60 C37 C38 C17 149.5 . . . . ?
C39 C37 C38 C17 158.3 . . . . ?
Lu10 C37 C38 C17 57.46(13) . . . . ?
C36 C37 C38 C40 -130.7 . . . . ?
C60 C37 C38 C40 16.5 . . . . ?
C17 C37 C38 C40 -132.9 . . . . ?
C39 C37 C38 C40 25.3 . . . . ?
Lu10 C37 C38 C40 -75.48(13) . . . . ?
C17 C38 C39 C62 -57.9 . . . . ?
C37 C38 C39 C62 40.9 . . . . ?
C40 C38 C39 C62 -117.7 . . . . ?
C17 C38 C39 C40 59.8 . . . . ?
C37 C38 C39 C40 158.6 . . . . ?
C17 C38 C39 C37 -98.9 . . . . ?
C40 C38 C39 C37 -158.6 . . . . ?
C17 C38 C39 Lu1 -14.58(8) . . . . ?
C37 C38 C39 Lu1 84.28(8) . . . . ?
C40 C38 C39 Lu1 -74.35(8) . . . . ?
C20 C19 C40 C41 -9.0 . . . . ?
C18 C19 C40 C41 142.2 . . . . ?
Lu8 C19 C40 C41 53.5(2) . . . . ?
C20 C19 C40 C39 -148.0 . . . . ?
C18 C19 C40 C39 3.2 . . . . ?
Lu8 C19 C40 C39 -85.4(2) . . . . ?
C20 C19 C40 C38 -154.5 . . . . ?
C18 C19 C40 C38 -3.2 . . . . ?
Lu8 C19 C40 C38 -91.9(2) . . . . ?
C20 C19 C40 Lu8 -62.6(2) . . . . ?
C18 C19 C40 Lu8 88.7(2) . . . . ?
C20 C19 C40 Lu1 -66.32(7) . . . . ?
C18 C19 C40 Lu1 84.89(7) . . . . ?
Lu8 C19 C40 Lu1 -3.8(2) . . . . ?
C62 C39 C40 C19 150.4 . . . . ?
C38 C39 C40 C19 -10.4 . . . . ?
C37 C39 C40 C19 11.8 . . . . ?
Lu1 C39 C40 C19 98.08(5) . . . . ?
C62 C39 C40 C41 7.2 . . . . ?
C38 C39 C40 C41 -153.6 . . . . ?
C37 C39 C40 C41 -131.4 . . . . ?
Lu1 C39 C40 C41 -45.12(5) . . . . ?
C62 C39 C40 C38 160.8 . . . . ?
C37 C39 C40 C38 22.2 . . . . ?
Lu1 C39 C40 C38 108.47(5) . . . . ?
C62 C39 C40 Lu8 75.87(18) . . . . ?
C38 C39 C40 Lu8 -84.89(18) . . . . ?
C37 C39 C40 Lu8 -62.68(18) . . . . ?
Lu1 C39 C40 Lu8 23.58(17) . . . . ?
C62 C39 C40 Lu1 52.30(5) . . . . ?
C38 C39 C40 Lu1 -108.47(5) . . . . ?
C37 C39 C40 Lu1 -86.25(5) . . . . ?
C19 C40 C41 C63 -151.6 . . . . ?
C39 C40 C41 C63 -5.7 . . . . ?
C38 C40 C41 C63 -30.6 . . . . ?
Lu8 C40 C41 C63 -95.1(3) . . . . ?
Lu1 C40 C41 C63 -62.96(8) . . . . ?
C19 C40 C41 C42 -0.3 . . . . ?
C39 C40 C41 C42 145.6 . . . . ?
C38 C40 C41 C42 120.7 . . . . ?
Lu8 C40 C41 C42 56.2(3) . . . . ?
Lu1 C40 C41 C42 88.32(8) . . . . ?
C19 C40 C41 Lu8 -56.6(3) . . . . ?
C39 C40 C41 Lu8 89.4(3) . . . . ?
C38 C40 C41 Lu8 64.5(3) . . . . ?
Lu1 C40 C41 Lu8 32.1(2) . . . . ?
C19 C40 C41 Lu1 -88.66(8) . . . . ?
C39 C40 C41 Lu1 57.26(8) . . . . ?
C38 C40 C41 Lu1 32.40(8) . . . . ?
Lu8 C40 C41 Lu1 -32.1(2) . . . . ?
C19 C40 C41 Lu7 -46.83(10) . . . . ?
C39 C40 C41 Lu7 99.09(10) . . . . ?
C38 C40 C41 Lu7 74.23(10) . . . . ?
Lu8 C40 C41 Lu7 9.7(3) . . . . ?
Lu1 C40 C41 Lu7 41.83(9) . . . . ?
C20 C21 C42 C41 -9.2 . . . . ?
C22 C21 C42 C41 -152.5 . . . . ?
Lu7 C21 C42 C41 -90.27(16) . . . . ?
Lu8 C21 C42 C41 -66.3(2) . . . . ?
C20 C21 C42 C43 142.4 . . . . ?
C22 C21 C42 C43 -0.8 . . . . ?
Lu7 C21 C42 C43 61.41(16) . . . . ?
Lu8 C21 C42 C43 85.4(2) . . . . ?
C20 C21 C42 Lu7 81.04(16) . . . . ?
C22 C21 C42 Lu7 -62.25(16) . . . . ?
Lu8 C21 C42 Lu7 23.97(18) . . . . ?
C20 C21 C42 Lu8 57.1(2) . . . . ?
C22 C21 C42 Lu8 -86.2(2) . . . . ?
Lu7 C21 C42 Lu8 -23.97(18) . . . . ?
C20 C21 C42 Lu1 60.84(7) . . . . ?
C22 C21 C42 Lu1 -82.45(8) . . . . ?
Lu7 C21 C42 Lu1 -20.19(15) . . . . ?
Lu8 C21 C42 Lu1 3.8(2) . . . . ?
C63 C41 C42 C21 152.3 . . . . ?
C40 C41 C42 C21 9.4 . . . . ?
Lu8 C41 C42 C21 69.2(2) . . . . ?
Lu1 C41 C42 C21 103.22(8) . . . . ?
Lu7 C41 C42 C21 77.12(18) . . . . ?
C63 C41 C42 C43 -1.2 . . . . ?
C40 C41 C42 C43 -144.1 . . . . ?
Lu8 C41 C42 C43 -84.3(2) . . . . ?
Lu1 C41 C42 C43 -50.26(8) . . . . ?
Lu7 C41 C42 C43 -76.36(18) . . . . ?
C63 C41 C42 Lu7 75.17(18) . . . . ?
C40 C41 C42 Lu7 -67.74(18) . . . . ?
Lu8 C41 C42 Lu7 -8.0(3) . . . . ?
Lu1 C41 C42 Lu7 26.10(17) . . . . ?
C63 C41 C42 Lu8 83.1(2) . . . . ?
C40 C41 C42 Lu8 -59.8(2) . . . . ?
Lu1 C41 C42 Lu8 34.07(19) . . . . ?
Lu7 C41 C42 Lu8 8.0(3) . . . . ?
C63 C41 C42 Lu1 49.07(8) . . . . ?
C40 C41 C42 Lu1 -93.84(8) . . . . ?
Lu8 C41 C42 Lu1 -34.07(19) . . . . ?
Lu7 C41 C42 Lu1 -26.10(17) . . . . ?
C21 C42 C43 C45 -0.3 . . . . ?
C41 C42 C43 C45 152.8 . . . . ?
Lu7 C42 C43 C45 61.43(14) . . . . ?
Lu8 C42 C43 C45 78.9(3) . . . . ?
Lu1 C42 C43 C45 106.97(6) . . . . ?
C21 C42 C43 C65 -157.3 . . . . ?
C41 C42 C43 C65 -4.2 . . . . ?
Lu7 C42 C43 C65 -95.57(14) . . . . ?
Lu8 C42 C43 C65 -78.1(3) . . . . ?
Lu1 C42 C43 C65 -50.03(6) . . . . ?
C21 C42 C43 Lu7 -61.72(14) . . . . ?
C41 C42 C43 Lu7 91.34(14) . . . . ?
Lu8 C42 C43 Lu7 17.4(3) . . . . ?
Lu1 C42 C43 Lu7 45.54(13) . . . . ?
C21 C42 C43 Lu5 -56.4(2) . . . . ?
C41 C42 C43 Lu5 96.6(2) . . . . ?
Lu7 C42 C43 Lu5 5.3(2) . . . . ?
Lu8 C42 C43 Lu5 22.7(3) . . . . ?
Lu1 C42 C43 Lu5 50.8(2) . . . . ?
C21 C42 C43 Lu11 -100.7(3) . . . . ?
C41 C42 C43 Lu11 52.4(3) . . . . ?
Lu7 C42 C43 Lu11 -39.0(3) . . . . ?
Lu8 C42 C43 Lu11 -21.5(4) . . . . ?
Lu1 C42 C43 Lu11 6.6(3) . . . . ?
C21 C42 C43 Lu1 -107.26(6) . . . . ?
C41 C42 C43 Lu1 45.80(6) . . . . ?
Lu7 C42 C43 Lu1 -45.54(13) . . . . ?
Lu8 C42 C43 Lu1 -28.1(3) . . . . ?
C21 C42 C43 Lu8 -79.2(3) . . . . ?
C41 C42 C43 Lu8 73.9(3) . . . . ?
Lu7 C42 C43 Lu8 -17.4(3) . . . . ?
Lu1 C42 C43 Lu8 28.1(3) . . . . ?
C65 C43 C45 C44 2.6 . . . . ?
C42 C43 C45 C44 -154.1 . . . . ?
Lu7 C43 C45 C44 -99.16(15) . . . . ?
Lu5 C43 C45 C44 -76.3(3) . . . . ?
Lu11 C43 C45 C44 -49.5(2) . . . . ?
Lu1 C43 C45 C44 -69.04(9) . . . . ?
Lu8 C43 C45 C44 -99.12(16) . . . . ?
C65 C43 C45 C23 152.3 . . . . ?
C42 C43 C45 C23 -4.4 . . . . ?
Lu7 C43 C45 C23 50.53(15) . . . . ?
Lu5 C43 C45 C23 73.4(3) . . . . ?
Lu11 C43 C45 C23 100.2(2) . . . . ?
Lu1 C43 C45 C23 80.66(9) . . . . ?
Lu8 C43 C45 C23 50.57(16) . . . . ?
C65 C43 C45 Lu5 78.9(3) . . . . ?
C42 C43 C45 Lu5 -77.8(3) . . . . ?
Lu7 C43 C45 Lu5 -22.8(3) . . . . ?
Lu11 C43 C45 Lu5 26.9(3) . . . . ?
Lu1 C43 C45 Lu5 7.3(3) . . . . ?
Lu8 C43 C45 Lu5 -22.8(3) . . . . ?
C65 C43 C45 Lu7 101.77(15) . . . . ?
C42 C43 C45 Lu7 -54.97(15) . . . . ?
Lu5 C43 C45 Lu7 22.8(3) . . . . ?
Lu11 C43 C45 Lu7 49.7(2) . . . . ?
Lu1 C43 C45 Lu7 30.12(12) . . . . ?
Lu8 C43 C45 Lu7 0.0(2) . . . . ?
C65 C43 C45 Lu9 50.98(16) . . . . ?
C42 C43 C45 Lu9 -105.76(16) . . . . ?
Lu7 C43 C45 Lu9 -50.80(19) . . . . ?
Lu5 C43 C45 Lu9 -27.9(3) . . . . ?
Lu11 C43 C45 Lu9 -1.1(2) . . . . ?
Lu1 C43 C45 Lu9 -20.67(15) . . . . ?
Lu8 C43 C45 Lu9 -50.8(2) . . . . ?
C67 C44 C45 C43 -1.5 . . . . ?
C46 C44 C45 C43 135.7 . . . . ?
Lu9 C44 C45 C43 67.75(19) . . . . ?
Lu5 C44 C45 C43 81.0(3) . . . . ?
C67 C44 C45 C23 -153.4 . . . . ?
C46 C44 C45 C23 -16.3 . . . . ?
Lu9 C44 C45 C23 -84.21(19) . . . . ?
Lu5 C44 C45 C23 -71.0(3) . . . . ?
C67 C44 C45 Lu5 -82.4(3) . . . . ?
C46 C44 C45 Lu5 54.7(3) . . . . ?
Lu9 C44 C45 Lu5 -13.2(4) . . . . ?
C67 C44 C45 Lu7 -74.77(14) . . . . ?
C46 C44 C45 Lu7 62.40(14) . . . . ?
Lu9 C44 C45 Lu7 -5.5(2) . . . . ?
Lu5 C44 C45 Lu7 7.7(3) . . . . ?
C67 C44 C45 Lu9 -69.23(19) . . . . ?
C46 C44 C45 Lu9 67.95(19) . . . . ?
Lu5 C44 C45 Lu9 13.2(4) . . . . ?
C22 C23 C45 C43 11.4 . . . . ?
C24 C23 C45 C43 -145.1 . . . . ?
Lu5 C23 C45 C43 -79.0(3) . . . . ?
Lu7 C23 C45 C43 -48.03(12) . . . . ?
C22 C23 C45 C44 162.7 . . . . ?
C24 C23 C45 C44 6.2 . . . . ?
Lu5 C23 C45 C44 72.3(3) . . . . ?
Lu7 C23 C45 C44 103.25(12) . . . . ?
C22 C23 C45 Lu5 90.4(3) . . . . ?
C24 C23 C45 Lu5 -66.2(3) . . . . ?
Lu7 C23 C45 Lu5 30.9(3) . . . . ?
C22 C23 C45 Lu7 59.48(12) . . . . ?
C24 C23 C45 Lu7 -97.10(12) . . . . ?
Lu5 C23 C45 Lu7 -30.9(3) . . . . ?
C22 C23 C45 Lu9 108.29(13) . . . . ?
C24 C23 C45 Lu9 -48.29(13) . . . . ?
Lu5 C23 C45 Lu9 17.9(3) . . . . ?
Lu7 C23 C45 Lu9 48.81(16) . . . . ?
C67 C44 C46 C70 26.1 . . . . ?
C45 C44 C46 C70 -118.4 . . . . ?
Lu9 C44 C46 C70 -44.3(2) . . . . ?
Lu5 C44 C46 C70 -72.0(2) . . . . ?
C67 C44 C46 C47 159.6 . . . . ?
C45 C44 C46 C47 15.1 . . . . ?
Lu9 C44 C46 C47 89.1(2) . . . . ?
Lu5 C44 C46 C47 61.5(2) . . . . ?
C67 C44 C46 Lu9 70.5(2) . . . . ?
C45 C44 C46 Lu9 -74.0(2) . . . . ?
Lu5 C44 C46 Lu9 -27.7(2) . . . . ?
C67 C44 C46 Lu5 98.1(2) . . . . ?
C45 C44 C46 Lu5 -46.4(2) . . . . ?
Lu9 C44 C46 Lu5 27.7(2) . . . . ?
C70 C46 C47 C48 8.3 . . . . ?
C44 C46 C47 C48 -146.0 . . . . ?
Lu9 C46 C47 C48 -79.44(16) . . . . ?
Lu5 C46 C47 C48 -99.06(17) . . . . ?
C70 C46 C47 C24 149.8 . . . . ?
C44 C46 C47 C24 -4.5 . . . . ?
Lu9 C46 C47 C24 62.07(16) . . . . ?
Lu5 C46 C47 C24 42.44(17) . . . . ?
C44 C46 C47 C70 -154.3 . . . . ?
Lu9 C46 C47 C70 -87.73(16) . . . . ?
Lu5 C46 C47 C70 -107.35(17) . . . . ?
C70 C46 C47 Lu9 87.73(16) . . . . ?
C44 C46 C47 Lu9 -66.60(16) . . . . ?
Lu5 C46 C47 Lu9 -19.6(2) . . . . ?
C70 C46 C47 Lu5 107.35(17) . . . . ?
C44 C46 C47 Lu5 -46.98(17) . . . . ?
Lu9 C46 C47 Lu5 19.6(2) . . . . ?
C25 C24 C47 C46 -155.1 . . . . ?
C23 C24 C47 C46 0.1 . . . . ?
Lu5 C24 C47 C46 -48.3(2) . . . . ?
C25 C24 C47 C48 -15.7 . . . . ?
C23 C24 C47 C48 139.6 . . . . ?
Lu5 C24 C47 C48 91.1(2) . . . . ?
C25 C24 C47 C70 -119.0 . . . . ?
C23 C24 C47 C70 36.3 . . . . ?
Lu5 C24 C47 C70 -12.2(2) . . . . ?
C25 C24 C47 Lu9 -110.13(12) . . . . ?
C23 C24 C47 Lu9 45.11(12) . . . . ?
Lu5 C24 C47 Lu9 -3.3(3) . . . . ?
C25 C24 C47 Lu5 -106.8(2) . . . . ?
C23 C24 C47 Lu5 48.5(2) . . . . ?
C28 C27 C48 C49 9.2 . . . . ?
C26 C27 C48 C49 144.3 . . . . ?
Lu3 C27 C48 C49 56.58(8) . . . . ?
C28 C27 C48 C47 -126.6 . . . . ?
C26 C27 C48 C47 8.6 . . . . ?
Lu3 C27 C48 C47 -79.19(8) . . . . ?
C28 C27 C48 C50 14.8 . . . . ?
C26 C27 C48 C50 150.0 . . . . ?
Lu3 C27 C48 C50 62.23(8) . . . . ?
C28 C27 C48 Lu3 -47.40(8) . . . . ?
C26 C27 C48 Lu3 87.77(8) . . . . ?
C46 C47 C48 C49 -1.7 . . . . ?
C24 C47 C48 C49 -140.7 . . . . ?
C70 C47 C48 C49 4.0 . . . . ?
Lu9 C47 C48 C49 -53.71(15) . . . . ?
Lu5 C47 C48 C49 -78.0(2) . . . . ?
C46 C47 C48 C27 140.9 . . . . ?
C24 C47 C48 C27 1.9 . . . . ?
C70 C47 C48 C27 146.6 . . . . ?
Lu9 C47 C48 C27 88.91(15) . . . . ?
Lu5 C47 C48 C27 64.6(2) . . . . ?
C46 C47 C48 C50 18.2 . . . . ?
C24 C47 C48 C50 -120.7 . . . . ?
C70 C47 C48 C50 24.0 . . . . ?
Lu9 C47 C48 C50 -33.73(15) . . . . ?
Lu5 C47 C48 C50 -58.0(2) . . . . ?
C46 C47 C48 Lu3 79.84(7) . . . . ?
C24 C47 C48 Lu3 -59.16(7) . . . . ?
C70 C47 C48 Lu3 85.59(7) . . . . ?
Lu9 C47 C48 Lu3 27.87(14) . . . . ?
Lu5 C47 C48 Lu3 3.6(2) . . . . ?
C27 C48 C49 C50 9.4 . . . . ?
C47 C48 C49 C50 155.1 . . . . ?
Lu3 C48 C49 C50 57.61(7) . . . . ?
C27 C48 C49 C70 -151.9 . . . . ?
C47 C48 C49 C70 -6.3 . . . . ?
C50 C48 C49 C70 -161.4 . . . . ?
Lu3 C48 C49 C70 -103.76(7) . . . . ?
C48 C49 C50 C51 -22.6 . . . . ?
C70 C49 C50 C51 132.8 . . . . ?
C48 C49 C50 C72 -160.9 . . . . ?
C70 C49 C50 C72 -5.4 . . . . ?
C70 C49 C50 C48 155.5 . . . . ?
C48 C49 C50 Lu3 -64.69(8) . . . . ?
C70 C49 C50 Lu3 90.76(8) . . . . ?
C49 C50 C51 C52 -118.6 . . . . ?
C72 C50 C51 C52 18.3 . . . . ?
C48 C50 C51 C52 -132.0 . . . . ?
Lu3 C50 C51 C52 -69.12(10) . . . . ?
C49 C50 C51 C28 13.4 . . . . ?
C72 C50 C51 C28 150.3 . . . . ?
C48 C50 C51 C28 -0.1 . . . . ?
Lu3 C50 C51 C28 62.83(10) . . . . ?
C49 C50 C51 Lu3 -49.47(10) . . . . ?
C72 C50 C51 Lu3 87.44(10) . . . . ?
C48 C50 C51 Lu3 -62.91(10) . . . . ?
C27 C28 C51 C50 7.9 . . . . ?
C29 C28 C51 C50 -143.7 . . . . ?
Lu3 C28 C51 C50 -80.16(14) . . . . ?
Lu4 C28 C51 C50 -84.02(6) . . . . ?
C27 C28 C51 C52 160.7 . . . . ?
C29 C28 C51 C52 9.1 . . . . ?
Lu3 C28 C51 C52 72.61(14) . . . . ?
Lu4 C28 C51 C52 68.75(6) . . . . ?
C27 C28 C51 Lu3 88.07(14) . . . . ?
C29 C28 C51 Lu3 -63.49(14) . . . . ?
Lu4 C28 C51 Lu3 -3.86(13) . . . . ?
C50 C51 C52 C53 -16.3 . . . . ?
C28 C51 C52 C53 -153.9 . . . . ?
Lu3 C51 C52 C53 -91.02(9) . . . . ?
C50 C51 C52 C30 120.7 . . . . ?
C28 C51 C52 C30 -16.9 . . . . ?
Lu3 C51 C52 C30 45.98(9) . . . . ?
C50 C51 C52 Lu3 74.76(9) . . . . ?
C28 C51 C52 Lu3 -62.85(9) . . . . ?
C32 C30 C52 C53 14.8 . . . . ?
C29 C30 C52 C53 156.4 . . . . ?
Lu3 C30 C52 C53 93.88(11) . . . . ?
Lu4 C30 C52 C53 98.64(6) . . . . ?
C32 C30 C52 C51 -125.3 . . . . ?
C29 C30 C52 C51 16.3 . . . . ?
Lu3 C30 C52 C51 -46.22(11) . . . . ?
Lu4 C30 C52 C51 -41.46(6) . . . . ?
C32 C30 C52 Lu3 -79.05(11) . . . . ?
C29 C30 C52 Lu3 62.47(11) . . . . ?
Lu4 C30 C52 Lu3 4.76(9) . . . . ?
C51 C52 C53 C54 150.6 . . . . ?
C30 C52 C53 C54 4.5 . . . . ?
Lu3 C52 C53 C54 76.97(13) . . . . ?
C51 C52 C53 C73 -3.8 . . . . ?
C30 C52 C53 C73 -149.9 . . . . ?
Lu3 C52 C53 C73 -77.45(13) . . . . ?
C51 C52 C53 C55 106.1 . . . . ?
C30 C52 C53 C55 -40.0 . . . . ?
Lu3 C52 C53 C55 32.48(13) . . . . ?
C51 C52 C53 Lu3 73.63(13) . . . . ?
C30 C52 C53 Lu3 -72.47(13) . . . . ?
C52 C53 C54 C55 -156.9 . . . . ?
C73 C53 C54 C55 -6.2 . . . . ?
Lu3 C53 C54 C55 -102.16(8) . . . . ?
C52 C53 C54 C31 -9.5 . . . . ?
C73 C53 C54 C31 141.2 . . . . ?
C55 C53 C54 C31 147.4 . . . . ?
Lu3 C53 C54 C31 45.26(8) . . . . ?
C52 C53 C54 Lu2 -67.96(8) . . . . ?
C73 C53 C54 Lu2 82.75(8) . . . . ?
C55 C53 C54 Lu2 88.94(8) . . . . ?
Lu3 C53 C54 Lu2 -13.23(9) . . . . ?
C33 C31 C54 C55 -22.8 . . . . ?
C32 C31 C54 C55 133.7 . . . . ?
Lu2 C31 C54 C55 41.07(8) . . . . ?
C33 C31 C54 C53 -155.7 . . . . ?
C32 C31 C54 C53 0.8 . . . . ?
Lu2 C31 C54 C53 -91.82(8) . . . . ?
C33 C31 C54 Lu2 -63.86(8) . . . . ?
C32 C31 C54 Lu2 92.66(8) . . . . ?
C53 C54 C55 C74 9.0 . . . . ?
C31 C54 C55 C74 -129.9 . . . . ?
Lu2 C54 C55 C74 -97.35(6) . . . . ?
C53 C54 C55 C56 150.3 . . . . ?
C31 C54 C55 C56 11.5 . . . . ?
Lu2 C54 C55 C56 44.01(6) . . . . ?
C31 C54 C55 C53 -138.9 . . . . ?
Lu2 C54 C55 C53 -106.34(6) . . . . ?
C54 C55 C56 C57 6.3 . . . . ?
C74 C55 C56 C57 155.3 . . . . ?
C53 C55 C56 C57 59.0 . . . . ?
C54 C55 C56 C77 -135.4 . . . . ?
C74 C55 C56 C77 13.6 . . . . ?
C53 C55 C56 C77 -82.8 . . . . ?
C54 C55 C56 Lu2 -43.19(6) . . . . ?
C74 C55 C56 Lu2 105.77(6) . . . . ?
C53 C55 C56 Lu2 9.43(6) . . . . ?
C77 C56 C57 C58 -0.4 . . . . ?
C55 C56 C57 C58 -148.7 . . . . ?
Lu2 C56 C57 C58 -85.22(9) . . . . ?
C77 C56 C57 C33 138.2 . . . . ?
C55 C56 C57 C33 -10.0 . . . . ?
Lu2 C56 C57 C33 53.43(9) . . . . ?
C77 C56 C57 Lu2 84.82(9) . . . . ?
C55 C56 C57 Lu2 -63.44(9) . . . . ?
C31 C33 C57 C58 143.0 . . . . ?
C34 C33 C57 C58 0.0 . . . . ?
Lu2 C33 C57 C58 73.56(13) . . . . ?
Lu10 C33 C57 C58 51.31(14) . . . . ?
C31 C33 C57 C56 -1.5 . . . . ?
C34 C33 C57 C56 -144.6 . . . . ?
Lu2 C33 C57 C56 -70.96(13) . . . . ?
Lu10 C33 C57 C56 -93.21(14) . . . . ?
C31 C33 C57 Lu2 69.43(13) . . . . ?
C34 C33 C57 Lu2 -73.60(13) . . . . ?
Lu10 C33 C57 Lu2 -22.25(15) . . . . ?
C56 C57 C58 C59 0.4 . . . . ?
C33 C57 C58 C59 -146.7 . . . . ?
Lu2 C57 C58 C59 -91.94(8) . . . . ?
C56 C57 C58 C35 150.5 . . . . ?
C33 C57 C58 C35 3.4 . . . . ?
Lu2 C57 C58 C35 58.17(8) . . . . ?
C56 C57 C58 Lu2 92.32(8) . . . . ?
C33 C57 C58 Lu2 -54.78(8) . . . . ?
C34 C35 C58 C57 -7.3 . . . . ?
C36 C35 C58 C57 -148.8 . . . . ?
Lu10 C35 C58 C57 -77.4(2) . . . . ?
Lu2 C35 C58 C57 -55.64(9) . . . . ?
C34 C35 C58 C59 144.4 . . . . ?
C36 C35 C58 C59 3.0 . . . . ?
Lu10 C35 C58 C59 74.4(2) . . . . ?
Lu2 C35 C58 C59 96.15(9) . . . . ?
C34 C35 C58 Lu2 48.30(8) . . . . ?
C36 C35 C58 Lu2 -93.14(9) . . . . ?
Lu10 C35 C58 Lu2 -21.7(2) . . . . ?
C57 C58 C59 C78 -2.1 . . . . ?
C35 C58 C59 C78 -147.9 . . . . ?
Lu2 C58 C59 C78 -72.82(11) . . . . ?
C57 C58 C59 C60 142.8 . . . . ?
C35 C58 C59 C60 -3.0 . . . . ?
Lu2 C58 C59 C60 72.06(11) . . . . ?
C36 C37 C60 C61 139.3 . . . . ?
C38 C37 C60 C61 -3.0 . . . . ?
C17 C37 C60 C61 42.4 . . . . ?
C39 C37 C60 C61 -8.5 . . . . ?
Lu10 C37 C60 C61 84.10(18) . . . . ?
C36 C37 C60 C59 2.9 . . . . ?
C38 C37 C60 C59 -139.4 . . . . ?
C17 C37 C60 C59 -93.9 . . . . ?
C39 C37 C60 C59 -144.8 . . . . ?
Lu10 C37 C60 C59 -52.27(18) . . . . ?
C78 C59 C60 C37 139.0 . . . . ?
C58 C59 C60 C37 0.5 . . . . ?
C78 C59 C60 C61 -5.4 . . . . ?
C58 C59 C60 C61 -143.9 . . . . ?
C37 C60 C61 C80 -133.9 . . . . ?
C59 C60 C61 C80 13.1 . . . . ?
C37 C60 C61 C62 7.6 . . . . ?
C59 C60 C61 C62 154.6 . . . . ?
C37 C60 C61 Lu1 -53.98(7) . . . . ?
C59 C60 C61 Lu1 93.03(8) . . . . ?
C38 C39 C62 C63 109.8 . . . . ?
C40 C39 C62 C63 -6.7 . . . . ?
C37 C39 C62 C63 142.0 . . . . ?
Lu1 C39 C62 C63 58.75(8) . . . . ?
C38 C39 C62 C61 -37.3 . . . . ?
C40 C39 C62 C61 -153.8 . . . . ?
C37 C39 C62 C61 -5.1 . . . . ?
Lu1 C39 C62 C61 -88.37(8) . . . . ?
C38 C39 C62 Lu1 51.04(8) . . . . ?
C40 C39 C62 Lu1 -65.47(8) . . . . ?
C37 C39 C62 Lu1 83.25(8) . . . . ?
C80 C61 C62 C39 147.3 . . . . ?
C60 C61 C62 C39 -0.1 . . . . ?
Lu1 C61 C62 C39 97.49(7) . . . . ?
C80 C61 C62 C63 -1.9 . . . . ?
C60 C61 C62 C63 -149.4 . . . . ?
Lu1 C61 C62 C63 -51.75(7) . . . . ?
C80 C61 C62 Lu1 49.85(7) . . . . ?
C60 C61 C62 Lu1 -97.64(7) . . . . ?
C42 C41 C63 C62 -145.3 . . . . ?
C40 C41 C63 C62 2.2 . . . . ?
Lu8 C41 C63 C62 -75.6(2) . . . . ?
Lu1 C41 C63 C62 -87.08(9) . . . . ?
Lu7 C41 C63 C62 -94.12(12) . . . . ?
C42 C41 C63 C64 4.6 . . . . ?
C40 C41 C63 C64 152.1 . . . . ?
Lu8 C41 C63 C64 74.2(2) . . . . ?
Lu1 C41 C63 C64 62.74(9) . . . . ?
Lu7 C41 C63 C64 55.70(12) . . . . ?
C42 C41 C63 Lu1 -58.17(9) . . . . ?
C40 C41 C63 Lu1 89.32(9) . . . . ?
Lu8 C41 C63 Lu1 11.5(2) . . . . ?
Lu7 C41 C63 Lu1 -7.03(13) . . . . ?
C42 C41 C63 Lu8 -69.6(2) . . . . ?
C40 C41 C63 Lu8 77.9(2) . . . . ?
Lu1 C41 C63 Lu8 -11.5(2) . . . . ?
Lu7 C41 C63 Lu8 -18.49(18) . . . . ?
C42 C41 C63 Lu11 -41.5(2) . . . . ?
C40 C41 C63 Lu11 106.0(2) . . . . ?
Lu8 C41 C63 Lu11 28.1(3) . . . . ?
Lu1 C41 C63 Lu11 16.6(2) . . . . ?
Lu7 C41 C63 Lu11 9.6(2) . . . . ?
C39 C62 C63 C41 3.5 . . . . ?
C61 C62 C63 C41 150.5 . . . . ?
Lu1 C62 C63 C41 84.36(10) . . . . ?
C39 C62 C63 C64 -144.5 . . . . ?
C61 C62 C63 C64 2.5 . . . . ?
Lu1 C62 C63 C64 -63.60(10) . . . . ?
C39 C62 C63 Lu1 -80.88(10) . . . . ?
C61 C62 C63 Lu1 66.12(10) . . . . ?
C39 C62 C63 Lu8 -49.63(14) . . . . ?
C61 C62 C63 Lu8 97.37(14) . . . . ?
Lu1 C62 C63 Lu8 31.25(13) . . . . ?
C39 C62 C63 Lu11 -94.1(3) . . . . ?
C61 C62 C63 Lu11 52.9(3) . . . . ?
Lu1 C62 C63 Lu11 -13.2(3) . . . . ?
C41 C63 C64 C65 -2.5 . . . . ?
C62 C63 C64 C65 143.3 . . . . ?
Lu1 C63 C64 C65 69.34(11) . . . . ?
Lu8 C63 C64 C65 50.26(18) . . . . ?
Lu11 C63 C64 C65 66.0(5) . . . . ?
C41 C63 C64 C81 -148.8 . . . . ?
C62 C63 C64 C81 -3.0 . . . . ?
Lu1 C63 C64 C81 -76.94(11) . . . . ?
Lu8 C63 C64 C81 -96.02(18) . . . . ?
Lu11 C63 C64 C81 -80.3(5) . . . . ?
C41 C63 C64 Lu1 -71.85(11) . . . . ?
C62 C63 C64 Lu1 73.93(11) . . . . ?
Lu8 C63 C64 Lu1 -19.08(19) . . . . ?
Lu11 C63 C64 Lu1 -3.3(5) . . . . ?
C41 C63 C64 Lu11 -68.5(5) . . . . ?
C62 C63 C64 Lu11 77.3(5) . . . . ?
Lu1 C63 C64 Lu11 3.3(5) . . . . ?
Lu8 C63 C64 Lu11 -15.7(5) . . . . ?
C45 C43 C65 C66 0.7 . . . . ?
C42 C43 C65 C66 157.5 . . . . ?
Lu7 C43 C65 C66 86.48(15) . . . . ?
Lu5 C43 C65 C66 57.36(19) . . . . ?
Lu11 C43 C65 C66 73.5(3) . . . . ?
Lu1 C43 C65 C66 101.85(7) . . . . ?
Lu8 C43 C65 C66 102.77(14) . . . . ?
C45 C43 C65 C64 -150.7 . . . . ?
C42 C43 C65 C64 6.1 . . . . ?
Lu7 C43 C65 C64 -64.87(15) . . . . ?
Lu5 C43 C65 C64 -94.0(2) . . . . ?
Lu11 C43 C65 C64 -77.9(3) . . . . ?
Lu1 C43 C65 C64 -49.50(7) . . . . ?
Lu8 C43 C65 C64 -48.58(14) . . . . ?
C45 C43 C65 Lu11 -72.8(3) . . . . ?
C42 C43 C65 Lu11 84.0(3) . . . . ?
Lu7 C43 C65 Lu11 13.0(4) . . . . ?
Lu5 C43 C65 Lu11 -16.1(3) . . . . ?
Lu1 C43 C65 Lu11 28.4(3) . . . . ?
Lu8 C43 C65 Lu11 29.3(4) . . . . ?
C45 C43 C65 Lu1 -101.18(7) . . . . ?
C42 C43 C65 Lu1 55.61(7) . . . . ?
Lu7 C43 C65 Lu1 -15.37(14) . . . . ?
Lu5 C43 C65 Lu1 -44.5(2) . . . . ?
Lu11 C43 C65 Lu1 -28.4(3) . . . . ?
Lu8 C43 C65 Lu1 0.91(14) . . . . ?
C45 C43 C65 Lu5 -56.68(19) . . . . ?
C42 C43 C65 Lu5 100.1(2) . . . . ?
Lu7 C43 C65 Lu5 29.1(2) . . . . ?
Lu11 C43 C65 Lu5 16.1(3) . . . . ?
Lu1 C43 C65 Lu5 44.5(2) . . . . ?
Lu8 C43 C65 Lu5 45.4(2) . . . . ?
C45 C43 C65 Lu9 -44.46(12) . . . . ?
C42 C43 C65 Lu9 112.32(12) . . . . ?
Lu7 C43 C65 Lu9 41.34(17) . . . . ?
Lu5 C43 C65 Lu9 12.2(2) . . . . ?
Lu11 C43 C65 Lu9 28.3(3) . . . . ?
Lu1 C43 C65 Lu9 56.72(13) . . . . ?
Lu8 C43 C65 Lu9 57.63(18) . . . . ?
C81 C64 C65 C43 146.1 . . . . ?
C63 C64 C65 C43 -2.8 . . . . ?
Lu1 C64 C65 C43 59.76(10) . . . . ?
Lu11 C64 C65 C43 85.0(3) . . . . ?
C81 C64 C65 C66 -8.4 . . . . ?
C63 C64 C65 C66 -157.3 . . . . ?
Lu1 C64 C65 C66 -94.70(10) . . . . ?
Lu11 C64 C65 C66 -69.4(3) . . . . ?
C81 C64 C65 Lu11 61.1(3) . . . . ?
C63 C64 C65 Lu11 -87.8(3) . . . . ?
Lu1 C64 C65 Lu11 -25.3(3) . . . . ?
C81 C64 C65 Lu1 86.31(10) . . . . ?
C63 C64 C65 Lu1 -62.57(10) . . . . ?
Lu11 C64 C65 Lu1 25.3(3) . . . . ?
C81 C64 C65 Lu5 85.1(2) . . . . ?
C63 C64 C65 Lu5 -63.8(2) . . . . ?
Lu1 C64 C65 Lu5 -1.3(2) . . . . ?
Lu11 C64 C65 Lu5 24.0(3) . . . . ?
C81 C64 C65 Lu9 58.90(16) . . . . ?
C63 C64 C65 Lu9 -89.98(16) . . . . ?
Lu1 C64 C65 Lu9 -27.41(15) . . . . ?
Lu11 C64 C65 Lu9 -2.2(3) . . . . ?
C43 C65 C66 C82 -146.1 . . . . ?
C64 C65 C66 C82 8.3 . . . . ?
Lu11 C65 C66 C82 -63.6(5) . . . . ?
Lu1 C65 C66 C82 -55.31(8) . . . . ?
Lu5 C65 C66 C82 -102.35(13) . . . . ?
Lu9 C65 C66 C82 -95.14(15) . . . . ?
C43 C65 C66 C67 -5.2 . . . . ?
C64 C65 C66 C67 149.3 . . . . ?
Lu11 C65 C66 C67 77.4(5) . . . . ?
Lu1 C65 C66 C67 85.64(8) . . . . ?
Lu5 C65 C66 C67 38.60(13) . . . . ?
Lu9 C65 C66 C67 45.81(15) . . . . ?
C43 C65 C66 Lu11 -82.6(5) . . . . ?
C64 C65 C66 Lu11 71.9(5) . . . . ?
Lu1 C65 C66 Lu11 8.2(5) . . . . ?
Lu5 C65 C66 Lu11 -38.8(5) . . . . ?
Lu9 C65 C66 Lu11 -31.6(5) . . . . ?
C43 C65 C66 Lu9 -51.00(15) . . . . ?
C64 C65 C66 Lu9 103.49(15) . . . . ?
Lu11 C65 C66 Lu9 31.6(5) . . . . ?
Lu1 C65 C66 Lu9 39.83(14) . . . . ?
Lu5 C65 C66 Lu9 -7.21(18) . . . . ?
C82 C66 C67 C68 -5.7 . . . . ?
C65 C66 C67 C68 -144.5 . . . . ?
Lu11 C66 C67 C68 -80.6(4) . . . . ?
Lu9 C66 C67 C68 -81.1(2) . . . . ?
C82 C66 C67 C44 145.0 . . . . ?
C65 C66 C67 C44 6.2 . . . . ?
Lu11 C66 C67 C44 70.1(4) . . . . ?
Lu9 C66 C67 C44 69.6(2) . . . . ?
C82 C66 C67 Lu9 75.4(2) . . . . ?
C65 C66 C67 Lu9 -63.4(2) . . . . ?
Lu11 C66 C67 Lu9 0.5(4) . . . . ?
C82 C66 C67 Lu11 74.9(4) . . . . ?
C65 C66 C67 Lu11 -63.9(4) . . . . ?
Lu9 C66 C67 Lu11 -0.5(4) . . . . ?
C82 C66 C67 Lu5 98.81(17) . . . . ?
C65 C66 C67 Lu5 -40.03(17) . . . . ?
Lu11 C66 C67 Lu5 23.9(4) . . . . ?
Lu9 C66 C67 Lu5 23.39(17) . . . . ?
C45 C44 C67 C68 147.0 . . . . ?
C46 C44 C67 C68 -7.9 . . . . ?
Lu9 C44 C67 C68 65.86(16) . . . . ?
Lu5 C44 C67 C68 84.5(3) . . . . ?
C45 C44 C67 C66 -3.0 . . . . ?
C46 C44 C67 C66 -157.8 . . . . ?
Lu9 C44 C67 C66 -84.10(16) . . . . ?
Lu5 C44 C67 C66 -65.5(3) . . . . ?
C45 C44 C67 Lu9 81.10(16) . . . . ?
C46 C44 C67 Lu9 -73.75(16) . . . . ?
Lu5 C44 C67 Lu9 18.6(3) . . . . ?
C45 C44 C67 Lu11 49.35(17) . . . . ?
C46 C44 C67 Lu11 -105.50(17) . . . . ?
Lu9 C44 C67 Lu11 -31.8(2) . . . . ?
Lu5 C44 C67 Lu11 -13.1(3) . . . . ?
C45 C44 C67 Lu5 62.5(3) . . . . ?
C46 C44 C67 Lu5 -92.4(3) . . . . ?
Lu9 C44 C67 Lu5 -18.6(3) . . . . ?
C66 C67 C68 C69 146.2 . . . . ?
C44 C67 C68 C69 -4.6 . . . . ?
Lu9 C67 C68 C69 55.85(19) . . . . ?
Lu11 C67 C68 C69 89.5(3) . . . . ?
Lu5 C67 C68 C69 49.5(2) . . . . ?
C66 C67 C68 C84 14.2 . . . . ?
C44 C67 C68 C84 -136.6 . . . . ?
Lu9 C67 C68 C84 -76.14(19) . . . . ?
Lu11 C67 C68 C84 -42.5(3) . . . . ?
Lu5 C67 C68 C84 -82.5(2) . . . . ?
C66 C67 C68 C70 150.9 . . . . ?
C44 C67 C68 C70 0.1 . . . . ?
Lu9 C67 C68 C70 60.55(19) . . . . ?
Lu11 C67 C68 C70 94.2(3) . . . . ?
Lu5 C67 C68 C70 54.2(2) . . . . ?
C66 C67 C68 Lu9 90.34(19) . . . . ?
C44 C67 C68 Lu9 -60.49(19) . . . . ?
Lu11 C67 C68 Lu9 33.6(4) . . . . ?
Lu5 C67 C68 Lu9 -6.4(3) . . . . ?
C84 C68 C69 C70 150.0 . . . . ?
C67 C68 C69 C70 8.8 . . . . ?
Lu9 C68 C69 C70 56.63(17) . . . . ?
C84 C68 C69 C71 7.6 . . . . ?
C67 C68 C69 C71 -133.5 . . . . ?
C70 C68 C69 C71 -142.3 . . . . ?
Lu9 C68 C69 C71 -85.68(17) . . . . ?
C67 C68 C69 C84 -141.2 . . . . ?
C70 C68 C69 C84 -150.0 . . . . ?
Lu9 C68 C69 C84 -93.32(17) . . . . ?
C84 C68 C69 Lu9 93.32(17) . . . . ?
C67 C68 C69 Lu9 -47.86(17) . . . . ?
C70 C68 C69 Lu9 -56.63(17) . . . . ?
C68 C69 C70 C49 -145.3 . . . . ?
C71 C69 C70 C49 -4.0 . . . . ?
C84 C69 C70 C49 -99.4 . . . . ?
Lu9 C69 C70 C49 -95.03(13) . . . . ?
C68 C69 C70 C46 2.9 . . . . ?
C71 C69 C70 C46 144.2 . . . . ?
C84 C69 C70 C46 48.8 . . . . ?
Lu9 C69 C70 C46 53.17(13) . . . . ?
C71 C69 C70 C68 141.3 . . . . ?
C84 C69 C70 C68 45.9 . . . . ?
Lu9 C69 C70 C68 50.30(13) . . . . ?
C68 C69 C70 C47 -24.3 . . . . ?
C71 C69 C70 C47 117.0 . . . . ?
C84 C69 C70 C47 21.6 . . . . ?
Lu9 C69 C70 C47 26.01(13) . . . . ?
C68 C69 C70 Lu9 -50.30(13) . . . . ?
C71 C69 C70 Lu9 91.01(13) . . . . ?
C84 C69 C70 Lu9 -4.40(12) . . . . ?
C48 C49 C70 C69 161.7 . . . . ?
C50 C49 C70 C69 7.1 . . . . ?
C48 C49 C70 C46 13.4 . . . . ?
C50 C49 C70 C46 -141.1 . . . . ?
C48 C49 C70 C68 121.0 . . . . ?
C50 C49 C70 C68 -33.5 . . . . ?
C48 C49 C70 C47 4.8 . . . . ?
C50 C49 C70 C47 -149.8 . . . . ?
C48 C49 C70 Lu9 74.99(17) . . . . ?
C50 C49 C70 Lu9 -79.56(17) . . . . ?
C47 C46 C70 C69 -162.8 . . . . ?
C44 C46 C70 C69 -25.8 . . . . ?
Lu9 C46 C70 C69 -65.37(19) . . . . ?
Lu5 C46 C70 C69 -81.0(2) . . . . ?
C47 C46 C70 C49 -12.3 . . . . ?
C44 C46 C70 C49 124.7 . . . . ?
Lu9 C46 C70 C49 85.19(19) . . . . ?
Lu5 C46 C70 C49 69.6(2) . . . . ?
C47 C46 C70 C68 -161.1 . . . . ?
C44 C46 C70 C68 -24.0 . . . . ?
Lu9 C46 C70 C68 -63.58(19) . . . . ?
Lu5 C46 C70 C68 -79.2(2) . . . . ?
C44 C46 C70 C47 137.0 . . . . ?
Lu9 C46 C70 C47 97.48(19) . . . . ?
Lu5 C46 C70 C47 81.9(2) . . . . ?
C47 C46 C70 Lu9 -97.48(19) . . . . ?
C44 C46 C70 Lu9 39.54(19) . . . . ?
Lu5 C46 C70 Lu9 -15.6(3) . . . . ?
C70 C69 C71 C85 -147.5 . . . . ?
C68 C69 C71 C85 -8.1 . . . . ?
C84 C69 C71 C85 -1.9 . . . . ?
Lu9 C69 C71 C85 -71.29(16) . . . . ?
C70 C69 C71 C72 1.8 . . . . ?
C68 C69 C71 C72 141.2 . . . . ?
C84 C69 C71 C72 147.4 . . . . ?
Lu9 C69 C71 C72 77.98(16) . . . . ?
C70 C69 C71 C84 -145.6 . . . . ?
C68 C69 C71 C84 -6.2 . . . . ?
Lu9 C69 C71 C84 -69.38(15) . . . . ?
C51 C50 C72 C73 0.4 . . . . ?
C49 C50 C72 C73 154.1 . . . . ?
C48 C50 C72 C73 138.7 . . . . ?
Lu3 C50 C72 C73 62.77(10) . . . . ?
C51 C50 C72 C71 -151.3 . . . . ?
C49 C50 C72 C71 2.4 . . . . ?
C48 C50 C72 C71 -13.0 . . . . ?
Lu3 C50 C72 C71 -88.92(10) . . . . ?
C69 C71 C72 C73 -154.2 . . . . ?
C85 C71 C72 C73 -7.3 . . . . ?
C84 C71 C72 C73 -59.1 . . . . ?
C69 C71 C72 C50 -1.1 . . . . ?
C85 C71 C72 C50 145.8 . . . . ?
C84 C71 C72 C50 94.1 . . . . ?
C50 C72 C73 C53 -17.1 . . . . ?
C71 C72 C73 C53 137.9 . . . . ?
C50 C72 C73 C74 -146.6 . . . . ?
C71 C72 C73 C74 8.3 . . . . ?
C54 C53 C73 C72 -137.8 . . . . ?
C52 C53 C73 C72 18.1 . . . . ?
C55 C53 C73 C72 -141.9 . . . . ?
Lu3 C53 C73 C72 -35.37(8) . . . . ?
C54 C53 C73 C74 2.1 . . . . ?
C52 C53 C73 C74 158.0 . . . . ?
C55 C53 C73 C74 -1.9 . . . . ?
Lu3 C53 C73 C74 104.57(8) . . . . ?
C54 C55 C74 C75 141.2 . . . . ?
C56 C55 C74 C75 -7.9 . . . . ?
C53 C55 C74 C75 147.3 . . . . ?
C54 C55 C74 C73 -8.1 . . . . ?
C56 C55 C74 C73 -157.3 . . . . ?
C53 C55 C74 C73 -2.1 . . . . ?
C72 C73 C74 C75 -4.4 . . . . ?
C53 C73 C74 C75 -146.5 . . . . ?
C72 C73 C74 C55 144.6 . . . . ?
C53 C73 C74 C55 2.6 . . . . ?
C55 C74 C75 C85 -142.8 . . . . ?
C73 C74 C75 C85 -1.4 . . . . ?
C55 C74 C75 C76 -6.7 . . . . ?
C73 C74 C75 C76 134.7 . . . . ?
C74 C75 C76 C86 -117.4 . . . . ?
C85 C75 C76 C86 19.4 . . . . ?
C74 C75 C76 C77 16.0 . . . . ?
C85 C75 C76 C77 152.9 . . . . ?
C86 C76 C77 C78 -7.9 . . . . ?
C75 C76 C77 C78 -156.9 . . . . ?
C86 C76 C77 C56 140.4 . . . . ?
C75 C76 C77 C56 -8.6 . . . . ?
C57 C56 C77 C78 2.3 . . . . ?
C55 C56 C77 C78 140.1 . . . . ?
Lu2 C56 C77 C78 59.15(8) . . . . ?
C57 C56 C77 C76 -142.1 . . . . ?
C55 C56 C77 C76 -4.4 . . . . ?
Lu2 C56 C77 C76 -85.28(7) . . . . ?
C58 C59 C78 C77 4.2 . . . . ?
C60 C59 C78 C77 -133.7 . . . . ?
C58 C59 C78 C79 142.1 . . . . ?
C60 C59 C78 C79 4.2 . . . . ?
C76 C77 C78 C59 145.8 . . . . ?
C56 C77 C78 C59 -4.6 . . . . ?
C76 C77 C78 C79 6.4 . . . . ?
C56 C77 C78 C79 -143.9 . . . . ?
C59 C78 C79 C80 -12.8 . . . . ?
C77 C78 C79 C80 131.9 . . . . ?
C59 C78 C79 C86 -147.3 . . . . ?
C77 C78 C79 C86 -2.7 . . . . ?
C78 C79 C80 C81 -139.9 . . . . ?
C86 C79 C80 C81 -4.2 . . . . ?
C78 C79 C80 C61 19.4 . . . . ?
C86 C79 C80 C61 155.1 . . . . ?
C78 C79 C80 C86 -135.7 . . . . ?
C78 C79 C80 Lu1 -66.06(8) . . . . ?
C86 C79 C80 Lu1 69.61(7) . . . . ?
C60 C61 C80 C79 -20.3 . . . . ?
C62 C61 C80 C79 -156.3 . . . . ?
Lu1 C61 C80 C79 -112.84(6) . . . . ?
C60 C61 C80 C81 137.8 . . . . ?
C62 C61 C80 C81 1.8 . . . . ?
Lu1 C61 C80 C81 45.24(6) . . . . ?
C60 C61 C80 C86 15.5 . . . . ?
C62 C61 C80 C86 -120.5 . . . . ?
Lu1 C61 C80 C86 -77.05(6) . . . . ?
C60 C61 C80 Lu1 92.52(6) . . . . ?
C62 C61 C80 Lu1 -43.47(6) . . . . ?
C79 C80 C81 C64 155.1 . . . . ?
C61 C80 C81 C64 -2.1 . . . . ?
C86 C80 C81 C64 152.1 . . . . ?
Lu1 C80 C81 C64 47.59(7) . . . . ?
C79 C80 C81 C82 16.5 . . . . ?
C61 C80 C81 C82 -140.7 . . . . ?
C86 C80 C81 C82 13.6 . . . . ?
Lu1 C80 C81 C82 -90.96(7) . . . . ?
C79 C80 C81 Lu11 84.2(3) . . . . ?
C61 C80 C81 Lu11 -73.0(3) . . . . ?
C86 C80 C81 Lu11 81.2(3) . . . . ?
Lu1 C80 C81 Lu11 -23.3(3) . . . . ?
C79 C80 C81 Lu1 107.51(7) . . . . ?
C61 C80 C81 Lu1 -49.71(7) . . . . ?
C86 C80 C81 Lu1 104.52(7) . . . . ?
C65 C64 C81 C80 -145.2 . . . . ?
C63 C64 C81 C80 2.6 . . . . ?
Lu1 C64 C81 C80 -63.72(9) . . . . ?
Lu11 C64 C81 C80 -91.1(3) . . . . ?
C65 C64 C81 C82 4.8 . . . . ?
C63 C64 C81 C82 152.6 . . . . ?
Lu1 C64 C81 C82 86.31(9) . . . . ?
Lu11 C64 C81 C82 58.9(3) . . . . ?
C65 C64 C81 Lu11 -54.1(3) . . . . ?
C63 C64 C81 Lu11 93.7(3) . . . . ?
Lu1 C64 C81 Lu11 27.4(3) . . . . ?
C65 C64 C81 Lu1 -81.48(9) . . . . ?
C63 C64 C81 Lu1 66.31(9) . . . . ?
Lu11 C64 C81 Lu1 -27.4(3) . . . . ?
C67 C66 C82 C83 -6.9 . . . . ?
C65 C66 C82 C83 134.9 . . . . ?
Lu11 C66 C82 C83 76.8(3) . . . . ?
Lu9 C66 C82 C83 44.26(13) . . . . ?
C67 C66 C82 C81 -146.8 . . . . ?
C65 C66 C82 C81 -5.0 . . . . ?
Lu11 C66 C82 C81 -63.1(3) . . . . ?
Lu9 C66 C82 C81 -95.64(13) . . . . ?
C67 C66 C82 Lu11 -83.7(3) . . . . ?
C65 C66 C82 Lu11 58.1(3) . . . . ?
Lu9 C66 C82 Lu11 -32.6(3) . . . . ?
C80 C81 C82 C83 -2.7 . . . . ?
C64 C81 C82 C83 -146.7 . . . . ?
Lu11 C81 C82 C83 -86.2(4) . . . . ?
Lu1 C81 C82 C83 -91.41(7) . . . . ?
C80 C81 C82 C66 144.1 . . . . ?
C64 C81 C82 C66 0.1 . . . . ?
Lu11 C81 C82 C66 60.5(4) . . . . ?
Lu1 C81 C82 C66 55.37(7) . . . . ?
C80 C81 C82 Lu11 83.5(4) . . . . ?
C64 C81 C82 Lu11 -60.4(4) . . . . ?
Lu1 C81 C82 Lu11 -5.2(4) . . . . ?
C66 C82 C83 C84 10.1 . . . . ?
C81 C82 C83 C84 147.4 . . . . ?
Lu11 C82 C83 C84 75.2(4) . . . . ?
C66 C82 C83 C86 -150.6 . . . . ?
C81 C82 C83 C86 -13.4 . . . . ?
Lu11 C82 C83 C86 -85.6(4) . . . . ?
C66 C82 C83 Lu11 -65.1(4) . . . . ?
C81 C82 C83 Lu11 72.1(4) . . . . ?
C69 C68 C84 C85 -7.6 . . . . ?
C67 C68 C84 C85 142.6 . . . . ?
C70 C68 C84 C85 8.9 . . . . ?
Lu9 C68 C84 C85 81.95(14) . . . . ?
C69 C68 C84 C83 -161.2 . . . . ?
C67 C68 C84 C83 -11.1 . . . . ?
C70 C68 C84 C83 -144.8 . . . . ?
Lu9 C68 C84 C83 -71.73(14) . . . . ?
C69 C68 C84 C71 -5.0 . . . . ?
C67 C68 C84 C71 145.2 . . . . ?
C70 C68 C84 C71 11.5 . . . . ?
Lu9 C68 C84 C71 84.55(14) . . . . ?
C67 C68 C84 C69 150.1 . . . . ?
C70 C68 C84 C69 16.5 . . . . ?
Lu9 C68 C84 C69 89.51(14) . . . . ?
C69 C68 C84 Lu9 -89.51(14) . . . . ?
C67 C68 C84 Lu9 60.61(14) . . . . ?
C70 C68 C84 Lu9 -73.03(14) . . . . ?
C82 C83 C84 C85 -162.0 . . . . ?
C86 C83 C84 C85 -23.5 . . . . ?
Lu11 C83 C84 C85 -107.8(2) . . . . ?
C82 C83 C84 C68 -0.9 . . . . ?
C86 C83 C84 C68 137.6 . . . . ?
Lu11 C83 C84 C68 53.3(2) . . . . ?
C82 C83 C84 C71 -135.1 . . . . ?
C86 C83 C84 C71 3.5 . . . . ?
Lu11 C83 C84 C71 -80.9(2) . . . . ?
C82 C83 C84 C69 -36.5 . . . . ?
C86 C83 C84 C69 102.1 . . . . ?
Lu11 C83 C84 C69 17.8(2) . . . . ?
C82 C83 C84 Lu9 -53.48(12) . . . . ?
C86 C83 C84 Lu9 85.07(12) . . . . ?
Lu11 C83 C84 Lu9 0.7(2) . . . . ?
C69 C71 C84 C85 -177.5 . . . . ?
C72 C71 C84 C85 73.9 . . . . ?
C69 C71 C84 C68 4.9 . . . . ?
C85 C71 C84 C68 -177.6 . . . . ?
C72 C71 C84 C68 -103.6 . . . . ?
C69 C71 C84 C83 146.9 . . . . ?
C85 C71 C84 C83 -35.6 . . . . ?
C72 C71 C84 C83 38.4 . . . . ?
C85 C71 C84 C69 177.5 . . . . ?
C72 C71 C84 C69 -108.6 . . . . ?
C69 C71 C84 Lu9 61.88(13) . . . . ?
C85 C71 C84 Lu9 -120.63(13) . . . . ?
C72 C71 C84 Lu9 -46.68(12) . . . . ?
C70 C69 C84 C85 112.6 . . . . ?
C68 C69 C84 C85 174.6 . . . . ?
C71 C69 C84 C85 1.9 . . . . ?
Lu9 C69 C84 C85 108.18(13) . . . . ?
C70 C69 C84 C68 -62.0 . . . . ?
C71 C69 C84 C68 -172.7 . . . . ?
Lu9 C69 C84 C68 -66.39(13) . . . . ?
C70 C69 C84 C83 -14.3 . . . . ?
C68 C69 C84 C83 47.7 . . . . ?
C71 C69 C84 C83 -125.0 . . . . ?
Lu9 C69 C84 C83 -18.72(13) . . . . ?
C70 C69 C84 C71 110.7 . . . . ?
C68 C69 C84 C71 172.7 . . . . ?
Lu9 C69 C84 C71 106.27(13) . . . . ?
C70 C69 C84 Lu9 4.39(13) . . . . ?
C68 C69 C84 Lu9 66.39(13) . . . . ?
C71 C69 C84 Lu9 -106.27(13) . . . . ?
C68 C84 C85 C71 3.4 . . . . ?
C83 C84 C85 C71 160.7 . . . . ?
C69 C84 C85 C71 -1.7 . . . . ?
Lu9 C84 C85 C71 63.35(13) . . . . ?
C68 C84 C85 C75 -140.2 . . . . ?
C83 C84 C85 C75 17.1 . . . . ?
C71 C84 C85 C75 -143.6 . . . . ?
C69 C84 C85 C75 -145.3 . . . . ?
Lu9 C84 C85 C75 -80.24(13) . . . . ?
C69 C71 C85 C84 2.6 . . . . ?
C72 C71 C85 C84 -145.2 . . . . ?
C69 C71 C85 C75 149.9 . . . . ?
C72 C71 C85 C75 2.1 . . . . ?
C84 C71 C85 C75 147.3 . . . . ?
C74 C75 C85 C84 133.1 . . . . ?
C76 C75 C85 C84 -17.5 . . . . ?
C74 C75 C85 C71 2.3 . . . . ?
C76 C75 C85 C71 -148.3 . . . . ?
C77 C76 C86 C79 6.2 . . . . ?
C75 C76 C86 C79 136.8 . . . . ?
C77 C76 C86 C83 -147.9 . . . . ?
C75 C76 C86 C83 -17.4 . . . . ?
C77 C76 C86 C80 -14.4 . . . . ?
C75 C76 C86 C80 116.1 . . . . ?
C80 C79 C86 C76 -151.0 . . . . ?
C78 C79 C86 C76 -2.2 . . . . ?
C80 C79 C86 C83 -36.5 . . . . ?
C78 C79 C86 C83 112.4 . . . . ?
C78 C79 C86 C80 148.8 . . . . ?
C82 C83 C86 C76 165.1 . . . . ?
C84 C83 C86 C76 22.8 . . . . ?
Lu11 C83 C86 C76 108.19(15) . . . . ?
C82 C83 C86 C79 46.1 . . . . ?
C84 C83 C86 C79 -96.2 . . . . ?
Lu11 C83 C86 C79 -10.81(15) . . . . ?
C82 C83 C86 C80 24.1 . . . . ?
C84 C83 C86 C80 -118.2 . . . . ?
Lu11 C83 C86 C80 -32.85(15) . . . . ?
C1A C2A C3A C3A -100.3(4) . . . 6_565 ?
C1A C2A C3A C4A 77.6(5) . . . . ?
C4A N1A C4A C5A -178.6(2) 6_565 . . . ?
Ni1A N1A C4A C5A 0.9(6) . . . . ?
C4A N1A C4A C3A 0.0(5) 6_565 . . . ?
Ni1A N1A C4A C3A 179.5(3) . . . . ?
C3A C3A C4A N1A 0.0(3) 6_565 . . . ?
C2A C3A C4A N1A -178.3(4) . . . . ?
C3A C3A C4A C5A 178.6(3) 6_565 . . . ?
C2A C3A C4A C5A 0.3(6) . . . . ?
N1A C4A C5A C6A 0.6(6) . . . . ?
C3A C4A C5A C6A -177.8(3) . . . . ?
C4A C5A C6A N2A -2.0(6) . . . . ?
C4A C5A C6A C7A 177.9(4) . . . . ?
C13A N2A C6A C5A -179.3(3) . . . . ?
Ni1A N2A C6A C5A 1.7(5) . . . . ?
C13A N2A C6A C7A 0.8(4) . . . . ?
Ni1A N2A C6A C7A -178.1(2) . . . . ?
C5A C6A C7A C10A 179.1(3) . . . . ?
N2A C6A C7A C10A -1.0(4) . . . . ?
C5A C6A C7A C8A -2.6(6) . . . . ?
N2A C6A C7A C8A 177.2(3) . . . . ?
C10A C7A C8A C9A 97.4(5) . . . . ?
C6A C7A C8A C9A -80.5(5) . . . . ?
C6A C7A C10A C13A 0.7(4) . . . . ?
C8A C7A C10A C13A -177.4(4) . . . . ?
C6A C7A C10A C11A 179.2(4) . . . . ?
C8A C7A C10A C11A 1.1(7) . . . . ?
C7A C10A C11A C12A -96.2(5) . . . . ?
C13A C10A C11A C12A 82.1(5) . . . . ?
C6A N2A C13A C14A -179.4(3) . . . . ?
Ni1A N2A C13A C14A -0.4(5) . . . . ?
C6A N2A C13A C10A -0.4(4) . . . . ?
Ni1A N2A C13A C10A 178.6(2) . . . . ?
C7A C10A C13A N2A -0.3(4) . . . . ?
C11A C10A C13A N2A -178.8(3) . . . . ?
C7A C10A C13A C14A 178.8(3) . . . . ?
C11A C10A C13A C14A 0.2(6) . . . . ?
N2A C13A C14A C15A 2.2(6) . . . . ?
C10A C13A C14A C15A -176.7(3) . . . . ?
C13A C14A C15A N3A -2.7(6) . . . . ?
C13A C14A C15A C16A 177.0(3) . . . . ?
C15A N3A C15A C14A 179.6(2) 6_565 . . . ?
Ni1A N3A C15A C14A 1.4(6) . . . . ?
C15A N3A C15A C16A -0.1(5) 6_565 . . . ?
Ni1A N3A C15A C16A -178.3(3) . . . . ?
C14A C15A C16A C16A -179.7(3) . . . 6_565 ?
N3A C15A C16A C16A 0.0(3) . . . 6_565 ?
C14A C15A C16A C17A -2.3(6) . . . . ?
N3A C15A C16A C17A 177.4(3) . . . . ?
C16A C16A C17A C18A 94.6(4) 6_565 . . . ?
C15A C16A C17A C18A -82.2(5) . . . . ?
C2B C1B C2B C3B -2(2) 6 . . . ?
C1B C2B C3B C4B -2(2) . . . . ?
C2B C3B C4B C3B 9(2) . . . 6 ?
C1C C1C C2C C3C 3(2) 2_655 . . . ?
C1C C2C C3C C3C -3.7(16) . . . 2_655 ?

_refine_diff_density_max         1.093
_refine_diff_density_min         -0.983
_refine_diff_density_rms         0.104



_vrf_PLAT307_Lu2@Cs15-C86        
;
PROBLEM: PLAT307 Type_2 Test for Isolated Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;

_vrf_PLAT308_Lu2@Cs15-C86        
;
PROBLEM: PLAT308 Type_2 Test for single bonded Metal Atoms  
RESPONSE: There is no covalent bond between Lu and carbon atoms
;
