# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2019

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_207c1-3
_database_code_depnum_ccdc_archive 'CCDC 1943953'
loop_
_audit_author_name
_audit_author_address
'Zhao-rui Wen'
;Xiamen University
China
;
_audit_update_record             
;
2019-07-29 deposited with the CCDC.	2019-10-07 downloaded from the CCDC.
;
_audit_creation_date             2019-07-30
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2014/8
_chemical_name_common            ?
_chemical_name_systematic        '[Au7Ag9]n'
_chemical_formula_moiety         'C116 H84 Ag9 Au7 F21 Fe3 O14 P6, B F4'
_chemical_formula_sum            'C116 H84 Ag9 Au7 B F25 Fe3 O14 P6'
_chemical_formula_weight         4890.60
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.7746(3)
_cell_length_b                   17.3633(4)
_cell_length_c                   30.4935(6)
_cell_angle_alpha                88.524(2)
_cell_angle_beta                 86.188(2)
_cell_angle_gamma                65.006(2)
_cell_volume                     7074.4(3)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    23957
_cell_measurement_temperature    100.01(10)
_cell_measurement_theta_max      28.3100
_cell_measurement_theta_min      3.5340
_shelx_estimated_absorpt_T_max   0.470
_shelx_estimated_absorpt_T_min   0.176
_exptl_absorpt_coefficient_mu    8.889
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.43981
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.39.46e (Rigaku Oxford Diffraction, 2018)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    2.296
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             4532
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0542
_diffrn_reflns_av_unetI/netI     0.0828
_diffrn_reflns_Laue_measured_fraction_full 0.988
_diffrn_reflns_Laue_measured_fraction_max 0.988
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       36
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            45544
_diffrn_reflns_point_group_measured_fraction_full 0.988
_diffrn_reflns_point_group_measured_fraction_max 0.988
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         25.000
_diffrn_reflns_theta_min         3.404
_diffrn_ambient_temperature      100.01(10)
_diffrn_detector_area_resol_mean 10.4741
_diffrn_detector_type            Atlas
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω     -6.00  20.25   0.75   13.34    --   -9.18 -99.00  30.00   35
  2  ω    -55.00  35.00   0.75   13.34    --    9.57 -37.00-120.00  120
  3  ω    -16.00  82.25   0.75   13.34    --    9.57  37.00  60.00  131
  4  ω    -20.00  74.50   0.75   13.34    --    9.57  67.00-176.00  126
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at home/near, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                19089
_reflns_number_total             24649
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)'
_computing_data_collection       'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)'
_computing_data_reduction        'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         5.861
_refine_diff_density_min         -6.108
_refine_diff_density_rms         0.454
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     884
_refine_ls_number_reflns         24649
_refine_ls_number_restraints     10
_refine_ls_R_factor_all          0.1638
_refine_ls_R_factor_gt           0.1468
_refine_ls_restrained_S_all      1.049
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1083P)²+1390.3540P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3585
_refine_ls_wR_factor_ref         0.3668
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Restrained distances
 B49-F32
 1.412 with sigma of 0.02
 B49-F58
 1.412 with sigma of 0.02
 B49-F55
 1.412 with sigma of 0.02
 B49-F200
 1.412 with sigma of 0.02
 F32-F58
 2.301 with sigma of 0.02
 F32-F55
 2.301 with sigma of 0.02
 F32-F200
 2.301 with sigma of 0.02
 F58-F55
 2.301 with sigma of 0.02
 F58-F200
 2.301 with sigma of 0.02
 F200-F55
 2.301 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
Uanis(C7DA) = Uanis(C6DA) = Uanis(C9BA) = Uanis(C40) = Uanis(C74) = Uanis(C52)
Uanis(C8AA) = Uanis(C7AA) = Uanis(C96) = Uanis(C42) = Uanis(C62) = Uanis(C64)
Uanis(C45) = Uanis(C23) = Uanis(C41) = Uanis(C6AA) = Uanis(C4EA)
Uanis(C85) = Uanis(C65) = Uanis(C16) = Uanis(C90) = Uanis(C71)
Uanis(C39) = Uanis(C3CA) = Uanis(C4CA) = Uanis(C5CA) = Uanis(C1BA) = Uanis(C84)
Uanis(C80) = Uanis(C28) = Uanis(C3DA) = Uanis(C2DA) = Uanis(C1DA) = Uanis(C73)
Uanis(C3EA) = Uanis(C6CA) = Uanis(C78) = Uanis(C7CA) = Uanis(C8CA) = Uanis(C37)
Uanis(C33) = Uanis(C60) = Uanis(C92) = Uanis(C38) = Uanis(C36)
Uanis(C76) = Uanis(C3BA) = Uanis(C48) = Uanis(C4BA) = Uanis(C88)
Uanis(C75) = Uanis(C3AA) = Uanis(C87) = Uanis(C2AA) = Uanis(C4AA) = Uanis(C54)
Uanis(C5DA) = Uanis(C49) = Uanis(C51) = Uanis(C99) = Uanis(C69) = Uanis(C95)
Uanis(C1EA) = Uanis(C47) = Uanis(C1AA) = Uanis(C53) = Uanis(C13) = Uanis(C46)
Uanis(C72) = Uanis(C98) = Uanis(C30) = Uanis(C32) = Uanis(C18) = Uanis(C91)
Uanis(C56) = Uanis(C7BA) = Uanis(C19) = Uanis(C0AA) = Uanis(C6BA)
Uanis(C67) = Uanis(C5BA) = Uanis(C61) = Uanis(C63) = Uanis(C86)
Uanis(C8DA) = Uanis(C6EA) = Uanis(C2CA) = Uanis(C50) = Uanis(C0CA) = Uanis(C1CA)
Uanis(C0EA) = Uanis(C9DA) = Uanis(C8BA) = Uanis(C57) = Uanis(C66) = Uanis(C29)
Uanis(O1AA) = Uanis(O12) = Uanis(C2EA) = Uanis(O31) = Uanis(C0BA) = Uanis(F35)
= Uanis(F5) = Uanis(F13)
Uanis(O9) = Uanis(C70) = Uanis(O40) = Uanis(C7EA) = Uanis(F36) = Uanis(F83) =
Uanis(F94)
Uanis(C5EA) = Uanis(C2BA) = Uanis(O21) = Uanis(O38)
Uanis(F16) = Uanis(F15) = Uanis(F0AA) = Uanis(C4DA) = Uanis(C43)
Uanis(C81) = Uanis(C5AA) = Uanis(F20) = Uanis(F1AA) = Uanis(F3)
Uanis(C24) = Uanis(O16) = Uanis(O15) = Uanis(C9AA) = Uanis(F87) = Uanis(F43) =
Uanis(F46)
Uanis(Ag0F) = Uanis(C77) = Uanis(C44) = Uanis(F25) = Uanis(F34) = Uanis(F53)
Uiso(F200) = Uiso(B49) = Uiso(F55) = Uiso(F58) = Uiso(F32)
Uanis(C9CA) = Uanis(C8EA) = Uanis(C0DA) = Uanis(C20) = Uanis(C31) = Uanis(C34)
4. Others
 Fixed Sof: O1AA(0.5) O12(0.5)
5.a Ternary CH refined with riding coordinates:
 C16(H16)
5.b Aromatic/amide H refined with riding coordinates:
 C33(H33), C48(H48), C38(H38), C18(H18), C19(H19), C23(H23), C30(H30),
 C32(H32), C40(H40), C41(H41), C42(H42), C46(H46), C0AA(H0AA), C56(H56),
 C60(H60), C62(H62), C63(H63), C65(H65), C72(H72), C76(H76), C85(H85), C86(H86),
  C90(H90), C92(H92), C98(H98), C99(H99), C29(H29), C4AA(H4AA), C1AA(H1AA),
 C39(H39), C1CA(H1CA), C1BA(H1BA), C8AA(H8AA), C2AA(H2AA), C47(H47), C5BA(H5BA),
  C51(H51), C52(H52), C53(H53), C54(H54), C4BA(H4BA), C61(H61), C6BA(H6BA),
 C3AA(H3AA), C66(H66), C3BA(H3BA), C6AA(H6AA), C0CA(H0CA), C7AA(H7AA), C80(H80),
  C4EA(H4EA), C8BA(H8BA), C2CA(H2CA), C9BA(H9BA), C95(H95), C96(H96),
 C2DA(H2DA), C28(H28), C5CA(H5CA), C37(H37), C4CA(H4CA), C3CA(H3CA), C7DA(H7DA),
  C8CA(H8CA), C1EA(H1EA), C49(H49), C3DA(H3DA), C5DA(H5DA), C9DA(H9DA),
 C6DA(H6DA), C8DA(H8DA), C7CA(H7CA), C75(H75), C6CA(H6CA), C0EA(H0EA),
 C1DA(H1DA), C6EA(H6EA), C3EA(H3EA), C34(H34), C31(H31), C0DA(H0DA), C8EA(H8EA),
  C9CA(H9CA)
5.c Fitted hexagon refined as free rotating group:
 C34(C31,C20,C0DA,C8EA,C9CA)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au01 Au 0.77053(10) 0.49201(9) 0.25363(4) 0.0368(3) Uani 1 1 d . . . . .
Au02 Au 0.70533(10) 0.49594(9) 0.34020(4) 0.0386(3) Uani 1 1 d . . . . .
Au03 Au 0.68725(12) 0.63766(10) 0.20734(5) 0.0442(4) Uani 1 1 d . . . . .
Au04 Au 0.81489(10) 0.34380(9) 0.20728(5) 0.0415(3) Uani 1 1 d . . . . .
Au05 Au 0.84126(11) 0.48617(10) 0.16832(5) 0.0436(4) Uani 1 1 d . . . . .
Au06 Au 0.72395(11) 0.64174(10) 0.29927(5) 0.0437(4) Uani 1 1 d . . . . .
Au07 Au 0.85545(11) 0.34207(10) 0.29959(5) 0.0437(4) Uani 1 1 d . . . . .
Ag08 Ag 0.63495(19) 0.49878(18) 0.19349(9) 0.0391(6) Uani 1 1 d . . . . .
Ag09 Ag 0.57099(19) 0.59309(18) 0.27464(9) 0.0405(6) Uani 1 1 d . . . . .
Ag0A Ag 0.6527(2) 0.40613(18) 0.27531(9) 0.0408(6) Uani 1 1 d . . . . .
Ag0B Ag 0.9003(2) 0.4844(2) 0.31689(9) 0.0497(7) Uani 1 1 d . . . . .
Ag0C Ag 0.9725(2) 0.3834(2) 0.23403(10) 0.0516(8) Uani 1 1 d . . . . .
Ag0D Ag 0.8955(2) 0.5746(2) 0.23598(10) 0.0538(8) Uani 1 1 d . . . . .
Ag0E Ag 0.4572(2) 0.5093(2) 0.24686(10) 0.0461(7) Uani 1 1 d . . . . .
Ag0F Ag 1.0550(2) 0.4624(2) 0.17251(11) 0.0567(8) Uani 1 1 d . . . . .
Fe0H Fe 0.9641(4) 0.0707(3) 0.25482(19) 0.0474(13) Uani 1 1 d . . . . .
Fe0I Fe 0.7351(4) 0.6919(4) 0.06879(19) 0.0471(13) Uani 1 1 d . . . . .
Fe0J Fe 0.6001(4) 0.6979(4) 0.4415(2) 0.0523(14) Uani 1 1 d . . . . .
P0K P 0.9499(7) 0.2174(7) 0.3355(3) 0.048(2) Uani 1 1 d . . . . .
P0L P 0.6821(8) 0.7639(7) 0.3399(4) 0.049(2) Uani 1 1 d . . . . .
P0M P 0.6298(7) 0.4974(7) 0.4081(3) 0.043(2) Uani 1 1 d . . . . .
P0N P 0.8931(7) 0.4887(7) 0.0953(3) 0.046(2) Uani 1 1 d . . . . .
P00O P 0.8365(8) 0.2214(7) 0.1715(3) 0.047(2) Uani 1 1 d . . . . .
P00P P 0.5953(8) 0.7534(7) 0.1670(3) 0.047(2) Uani 1 1 d . . . . .
O8 O 0.600(2) 0.306(2) 0.2818(9) 0.058(8) Uani 1 1 d . . . . .
O14 O 0.545(3) 0.5106(19) 0.1388(9) 0.063(8) Uani 1 1 d . . . . .
O15 O 1.071(3) 0.591(3) 0.1630(13) 0.087(4) Uani 1 1 d . . . . .
O16 O 0.944(3) 0.671(2) 0.2076(13) 0.087(4) Uani 1 1 d . . . . .
O17 O 0.4704(18) 0.3780(15) 0.2375(10) 0.051(7) Uani 1 1 d . . . . .
O20 O 0.3919(18) 0.5570(18) 0.1780(10) 0.055(7) Uani 1 1 d . . . . .
O21 O 1.191(2) 0.3337(19) 0.1790(10) 0.061(4) Uani 1 1 d . . . . .
C24 C 1.021(5) 0.655(4) 0.182(2) 0.087(4) Uani 1 1 d . . . . .
O31 O 1.088(2) 0.376(2) 0.2850(12) 0.077(4) Uani 1 1 d . . . . .
C33 C 1.036(3) 0.044(3) 0.3106(14) 0.052(4) Uani 1 1 d . . . . .
H33 H 1.0161 0.0251 0.3368 0.062 Uiso 1 1 calc R . . . .
C36 C 1.008(3) 0.126(3) 0.3031(14) 0.052(4) Uani 1 1 d . . . . .
O38 O 1.091(2) 0.2693(18) 0.2003(10) 0.061(4) Uani 1 1 d . . . . .
C48 C 0.921(3) 0.043(2) 0.1977(14) 0.048(4) Uani 1 1 d . . . . .
H48 H 0.9611 0.0230 0.1719 0.058 Uiso 1 1 calc R . . . .
C50 C 0.463(4) 0.785(3) 0.1837(18) 0.072(5) Uani 1 1 d . . . . .
Ag1 Ag 0.2335(3) 0.5346(3) 0.20110(14) 0.0702(10) Uani 1 1 d . . . . .
C44 C 0.443(3) 0.543(3) 0.1413(15) 0.0567(8) Uani 1 1 d . . . . .
C38 C 1.067(3) 0.119(3) 0.2599(14) 0.052(4) Uani 1 1 d . . . . .
H38 H 1.0711 0.1643 0.2442 0.062 Uiso 1 1 calc R . . . .
O40 O 0.950(3) 0.527(3) 0.3735(14) 0.093(5) Uani 1 1 d . . . . .
C43 C 0.528(5) 0.316(4) 0.257(2) 0.091(5) Uani 1 1 d . . . . .
O9 O 1.010(3) 0.581(3) 0.3154(14) 0.093(5) Uani 1 1 d . . . . .
C13 C 0.840(3) 0.441(3) 0.0563(14) 0.052(4) Uani 1 1 d . . . . .
C16 C 0.555(3) 0.623(2) 0.4776(14) 0.049(4) Uani 1 1 d . . . . .
H16 H 0.5936 0.5845 0.5003 0.059 Uiso 1 1 calc R . . . .
C18 C 1.092(3) 0.470(3) 0.0818(13) 0.056(4) Uani 1 1 d . . . . .
H18 H 1.0624 0.5294 0.0815 0.067 Uiso 1 1 calc R . . . .
C19 C 0.857(3) 0.659(2) 0.1023(14) 0.050(4) Uani 1 1 d . . . . .
H19 H 0.8582 0.6547 0.1328 0.060 Uiso 1 1 calc R . . . .
C23 C 0.744(3) 0.672(3) 0.4200(15) 0.058(5) Uani 1 1 d . . . . .
H23 H 0.7911 0.6244 0.4049 0.070 Uiso 1 1 calc R . . . .
F25 F 0.4239(17) 0.4962(15) 0.0749(8) 0.0567(8) Uani 1 1 d . . . . .
C30 C 1.235(3) 0.338(3) 0.0764(13) 0.056(4) Uani 1 1 d . . . . .
H30 H 1.3039 0.3066 0.0721 0.067 Uiso 1 1 calc R . . . .
C32 C 1.195(3) 0.427(3) 0.0776(13) 0.056(4) Uani 1 1 d . . . . .
H32 H 1.2364 0.4553 0.0757 0.067 Uiso 1 1 calc R . . . .
F34 F 0.2967(17) 0.5828(15) 0.1060(8) 0.0567(8) Uani 1 1 d . . . . .
F36 F 1.090(2) 0.548(2) 0.4206(12) 0.093(5) Uani 1 1 d . . . . .
O0AA O 0.333(2) 0.612(2) 0.2874(11) 0.072(9) Uani 1 1 d . . . . .
C40 C 0.564(3) 0.921(3) 0.2983(18) 0.065(5) Uani 1 1 d . . . . .
H40 H 0.6242 0.9234 0.2891 0.078 Uiso 1 1 calc R . . . .
C41 C 0.738(3) 0.672(3) 0.4629(15) 0.058(5) Uani 1 1 d . . . . .
H41 H 0.7707 0.6291 0.4825 0.070 Uiso 1 1 calc R . . . .
C42 C 0.928(3) 0.800(2) 0.3026(17) 0.060(5) Uani 1 1 d . . . . .
H42 H 0.9784 0.7779 0.2803 0.072 Uiso 1 1 calc R . . . .
C45 C 0.682(3) 0.739(3) 0.3977(15) 0.058(5) Uani 1 1 d . . . . .
C46 C 0.886(3) 0.415(3) 0.0160(14) 0.052(4) Uani 1 1 d . . . . .
H46 H 0.9436 0.4214 0.0067 0.063 Uiso 1 1 calc R . . . .
C0AA C 0.843(3) 0.735(3) 0.0767(14) 0.050(4) Uani 1 1 d . . . . .
H0AA H 0.8310 0.7881 0.0881 0.060 Uiso 1 1 calc R . . . .
O52 O 0.428(2) 0.677(2) 0.3105(10) 0.062(8) Uani 1 1 d . . . . .
F53 F 0.4051(17) 0.6202(15) 0.0785(8) 0.0567(8) Uani 1 1 d . . . . .
C56 C 0.864(3) 0.624(2) 0.0332(14) 0.050(4) Uani 1 1 d . . . . .
H56 H 0.8696 0.5923 0.0084 0.060 Uiso 1 1 calc R . . . .
C57 C 0.624(3) 0.845(3) 0.1733(18) 0.065(5) Uani 1 1 d . . . . .
C60 C 1.093(3) -0.012(3) 0.2801(14) 0.052(4) Uani 1 1 d . . . . .
H60 H 1.1141 -0.0706 0.2805 0.062 Uiso 1 1 calc R . . . .
C62 C 0.860(3) 0.776(2) 0.3063(17) 0.060(5) Uani 1 1 d . . . . .
H62 H 0.8643 0.7354 0.2860 0.072 Uiso 1 1 calc R . . . .
C63 C 0.604(3) 0.801(3) 0.0723(13) 0.052(4) Uani 1 1 d . . . . .
H63 H 0.5984 0.8560 0.0741 0.062 Uiso 1 1 calc R . . . .
C64 C 0.781(3) 0.801(2) 0.3360(17) 0.060(5) Uani 1 1 d . . . . .
C65 C 0.479(3) 0.710(2) 0.4858(14) 0.049(4) Uani 1 1 d . . . . .
H65 H 0.4573 0.7401 0.5121 0.059 Uiso 1 1 calc R . . . .
C69 C 0.730(4) 0.223(3) 0.1483(17) 0.069(5) Uani 1 1 d . . . . .
C70 C 1.003(4) 0.563(4) 0.357(2) 0.093(5) Uani 1 1 d . . . . .
C71 C 0.559(3) 0.603(2) 0.4349(14) 0.049(4) Uani 1 1 d . . . . .
C72 C 1.075(3) 0.339(3) 0.0861(13) 0.056(4) Uani 1 1 d . . . . .
H72 H 1.0348 0.3091 0.0890 0.067 Uiso 1 1 calc R . . . .
C74 C 0.569(3) 0.850(3) 0.3263(18) 0.065(5) Uani 1 1 d . . . . .
C76 C 0.835(3) 0.055(2) 0.2659(14) 0.048(4) Uani 1 1 d . . . . .
H76 H 0.8082 0.0439 0.2924 0.058 Uiso 1 1 calc R . . . .
C77 C 0.394(3) 0.562(3) 0.1002(14) 0.0567(8) Uani 1 1 d . . . . .
C78 C 0.881(5) 0.184(4) 0.379(2) 0.093(8) Uani 1 1 d . . . . .
F83 F 0.976(2) 0.663(2) 0.4139(11) 0.093(5) Uani 1 1 d . . . . .
C85 C 0.446(3) 0.736(2) 0.4433(14) 0.049(4) Uani 1 1 d . . . . .
H85 H 0.3958 0.7885 0.4369 0.059 Uiso 1 1 calc R . . . .
C86 C 0.622(3) 0.671(3) 0.0407(13) 0.052(4) Uani 1 1 d . . . . .
H86 H 0.6317 0.6319 0.0188 0.062 Uiso 1 1 calc R . . . .
C87 C 0.940(4) 0.181(3) 0.1254(17) 0.067(5) Uani 1 1 d . . . . .
C88 C 0.865(3) 0.132(2) 0.2095(14) 0.048(4) Uani 1 1 d . . . . .
C90 C 0.499(3) 0.674(2) 0.4119(14) 0.049(4) Uani 1 1 d . . . . .
H90 H 0.4940 0.6794 0.3817 0.059 Uiso 1 1 calc R . . . .
C91 C 1.035(3) 0.428(3) 0.0864(13) 0.056(4) Uani 1 1 d . . . . .
C92 C 1.113(3) 0.036(3) 0.2479(14) 0.052(4) Uani 1 1 d . . . . .
H92 H 1.1517 0.0148 0.2220 0.062 Uiso 1 1 calc R . . . .
F94 F 1.111(2) 0.625(2) 0.3716(11) 0.093(5) Uani 1 1 d . . . . .
C98 C 1.177(3) 0.299(3) 0.0812(13) 0.056(4) Uani 1 1 d . . . . .
H98 H 1.2064 0.2397 0.0814 0.067 Uiso 1 1 calc R . . . .
C99 C 0.646(4) 0.298(3) 0.1433(17) 0.069(5) Uani 1 1 d . . . . .
H99 H 0.6483 0.3480 0.1527 0.083 Uiso 1 1 calc R . . . .
F3 F 0.1806(18) 0.7540(17) 0.3218(10) 0.071(4) Uani 1 1 d . . . . .
F5 F 1.1945(17) 0.4280(19) 0.3432(10) 0.077(4) Uani 1 1 d . . . . .
F12 F 1.346(2) 0.1814(18) 0.1652(11) 0.082(9) Uani 1 1 d . . . . .
F13 F 1.2894(18) 0.3298(19) 0.2985(10) 0.077(4) Uani 1 1 d . . . . .
F19 F 1.295(2) 0.1690(18) 0.2318(12) 0.086(9) Uani 1 1 d . . . . .
F20 F 0.2757(18) 0.7996(17) 0.3502(10) 0.071(4) Uani 1 1 d . . . . .
F24 F 1.252(2) 0.120(2) 0.1763(12) 0.109(13) Uani 1 1 d . . . . .
C29 C 0.739(3) 0.901(3) 0.1977(18) 0.065(5) Uani 1 1 d . . . . .
H29 H 0.7978 0.8940 0.2097 0.078 Uiso 1 1 calc R . . . .
C4AA C 1.103(4) 0.121(3) 0.1004(16) 0.067(5) Uani 1 1 d . . . . .
H4AA H 1.1710 0.0935 0.1051 0.081 Uiso 1 1 calc R . . . .
C5AA C 0.265(3) 0.726(3) 0.3385(19) 0.071(4) Uani 1 1 d . . . . .
F35 F 1.2717(18) 0.4462(19) 0.2870(10) 0.077(4) Uani 1 1 d . . . . .
C1AA C 0.713(3) 0.400(3) 0.0408(14) 0.052(4) Uani 1 1 d . . . . .
H1AA H 0.6530 0.3962 0.0494 0.063 Uiso 1 1 calc R . . . .
C39 C 0.677(4) 0.387(3) 0.4788(14) 0.059(4) Uani 1 1 d . . . . .
H39 H 0.6135 0.3877 0.4795 0.070 Uiso 1 1 calc R . . . .
C1CA C 0.330(3) 0.828(3) 0.2366(19) 0.072(5) Uani 1 1 d . . . . .
H1CA H 0.3042 0.8481 0.2648 0.086 Uiso 1 1 calc R . . . .
C1BA C 0.809(3) 0.432(3) 0.4541(15) 0.059(4) Uani 1 1 d . . . . .
H1BA H 0.8294 0.4617 0.4330 0.070 Uiso 1 1 calc R . . . .
F43 F 1.129(2) 0.718(2) 0.1615(11) 0.087(4) Uani 1 1 d . . . . .
C8AA C 0.767(3) 0.870(2) 0.3602(17) 0.060(5) Uani 1 1 d . . . . .
H8AA H 0.7063 0.8991 0.3763 0.072 Uiso 1 1 calc R . . . .
C2AA C 1.046(4) 0.143(3) 0.1350(17) 0.067(5) Uani 1 1 d . . . . .
H2AA H 1.0692 0.1363 0.1632 0.081 Uiso 1 1 calc R . . . .
F46 F 1.009(2) 0.791(2) 0.1919(11) 0.087(4) Uani 1 1 d . . . . .
C47 C 0.757(3) 0.369(3) -0.0003(14) 0.052(4) Uani 1 1 d . . . . .
H47 H 0.7303 0.3434 -0.0189 0.063 Uiso 1 1 calc R . . . .
C5BA C 0.618(3) 0.652(3) 0.0871(13) 0.052(4) Uani 1 1 d . . . . .
H5BA H 0.6206 0.6029 0.1004 0.062 Uiso 1 1 calc R . . . .
C51 C 0.558(4) 0.306(3) 0.1254(17) 0.069(5) Uani 1 1 d . . . . .
H51 H 0.5047 0.3587 0.1232 0.083 Uiso 1 1 calc R . . . .
C52 C 0.465(3) 0.860(3) 0.3407(18) 0.065(5) Uani 1 1 d . . . . .
H52 H 0.4580 0.8168 0.3570 0.078 Uiso 1 1 calc R . . . .
C53 C 0.751(3) 0.437(3) 0.0699(14) 0.052(4) Uani 1 1 d . . . . .
H53 H 0.7184 0.4571 0.0972 0.063 Uiso 1 1 calc R . . . .
C54 C 1.082(4) 0.132(3) 0.0576(17) 0.067(5) Uani 1 1 d . . . . .
H54 H 1.1312 0.1126 0.0349 0.081 Uiso 1 1 calc R . . . .
C4BA C 0.819(3) 0.133(3) 0.2480(14) 0.048(4) Uani 1 1 d . . . . .
H4BA H 0.7785 0.1842 0.2624 0.058 Uiso 1 1 calc R . . . .
C2BA C 1.266(4) 0.186(3) 0.1901(16) 0.061(4) Uani 1 1 d . . . . .
C61 C 0.611(3) 0.749(3) 0.0324(14) 0.052(4) Uani 1 1 d . . . . .
H61 H 0.6079 0.7705 0.0040 0.062 Uiso 1 1 calc R . . . .
C6BA C 0.850(3) 0.716(3) 0.0340(14) 0.050(4) Uani 1 1 d . . . . .
H6BA H 0.8472 0.7511 0.0100 0.060 Uiso 1 1 calc R . . . .
C3AA C 0.914(4) 0.196(3) 0.0835(16) 0.067(5) Uani 1 1 d . . . . .
H3AA H 0.8467 0.2240 0.0782 0.081 Uiso 1 1 calc R . . . .
C66 C 0.713(3) 0.835(3) 0.1916(18) 0.065(5) Uani 1 1 d . . . . .
H66 H 0.7577 0.7814 0.2000 0.078 Uiso 1 1 calc R . . . .
C67 C 0.609(3) 0.737(3) 0.1095(13) 0.052(4) Uani 1 1 d . . . . .
C0BA C 1.228(3) 0.401(4) 0.300(2) 0.077(4) Uani 1 1 d . . . . .
C3BA C 0.905(3) -0.007(3) 0.2320(14) 0.048(4) Uani 1 1 d . . . . .
H3BA H 0.9327 -0.0663 0.2334 0.058 Uiso 1 1 calc R . . . .
C6AA C 0.662(3) 0.763(3) 0.4719(15) 0.058(5) Uani 1 1 d . . . . .
H6AA H 0.6380 0.7850 0.4999 0.070 Uiso 1 1 calc R . . . .
C73 C 0.535(4) 0.457(4) 0.4059(18) 0.074(6) Uani 1 1 d . . . . .
C0CA C 0.425(4) 0.813(3) 0.2254(18) 0.072(5) Uani 1 1 d . . . . .
H0CA H 0.4642 0.8211 0.2456 0.086 Uiso 1 1 calc R . . . .
C7AA C 0.850(3) 0.898(2) 0.3611(17) 0.060(5) Uani 1 1 d . . . . .
H7AA H 0.8468 0.9400 0.3805 0.072 Uiso 1 1 calc R . . . .
C80 C 0.439(4) 0.503(4) 0.4132(17) 0.074(6) Uani 1 1 d . . . . .
H80 H 0.4156 0.5602 0.4211 0.089 Uiso 1 1 calc R . . . .
C81 C 0.355(3) 0.667(3) 0.3105(18) 0.071(4) Uani 1 1 d . . . . .
C4EA C 0.629(3) 0.812(3) 0.4305(15) 0.058(5) Uani 1 1 d . . . . .
H4EA H 0.5887 0.8689 0.4261 0.070 Uiso 1 1 calc R . . . .
C84 C 0.710(3) 0.433(3) 0.4497(14) 0.059(4) Uani 1 1 d . . . . .
F87 F 1.009(2) 0.755(2) 0.1279(11) 0.087(4) Uani 1 1 d . . . . .
C8BA C 0.555(3) 0.930(3) 0.1648(18) 0.065(5) Uani 1 1 d . . . . .
H8BA H 0.4946 0.9407 0.1529 0.078 Uiso 1 1 calc R . . . .
C2CA C 0.401(3) 0.776(3) 0.1531(19) 0.072(5) Uani 1 1 d . . . . .
H2CA H 0.4253 0.7668 0.1238 0.086 Uiso 1 1 calc R . . . .
C9BA C 0.482(3) 0.983(3) 0.2851(18) 0.065(5) Uani 1 1 d . . . . .
H9BA H 0.4830 1.0213 0.2634 0.078 Uiso 1 1 calc R . . . .
C7BA C 0.867(3) 0.597(2) 0.0764(14) 0.050(4) Uani 1 1 d . . . . .
C95 C 0.727(4) 0.144(3) 0.1273(17) 0.069(5) Uani 1 1 d . . . . .
H95 H 0.7821 0.0913 0.1262 0.083 Uiso 1 1 calc R . . . .
C96 C 0.930(3) 0.859(2) 0.3312(16) 0.060(5) Uani 1 1 d . . . . .
H96 H 0.9849 0.8724 0.3305 0.072 Uiso 1 1 calc R . . . .
C9AA C 1.035(5) 0.739(4) 0.166(2) 0.087(4) Uani 1 1 d . . . . .
O1AA O 1.121(5) 0.481(5) 0.243(3) 0.077(4) Uani 0.5 1 d . . P . .
O12 O 1.071(5) 0.518(5) 0.258(3) 0.077(4) Uani 0.5 1 d . . P . .
F15 F 0.598(2) 0.165(2) 0.2354(12) 0.091(5) Uani 1 1 d . . . . .
F16 F 0.497(2) 0.202(2) 0.2955(12) 0.091(5) Uani 1 1 d . . . . .
C2DA C 0.507(4) 0.336(4) 0.3791(17) 0.074(6) Uani 1 1 d . . . . .
H2DA H 0.5372 0.2806 0.3678 0.089 Uiso 1 1 calc R . . . .
F0AA F 0.442(2) 0.236(2) 0.2304(12) 0.091(5) Uani 1 1 d . . . . .
C28 C 0.369(4) 0.466(4) 0.4090(17) 0.074(6) Uani 1 1 d . . . . .
H28 H 0.3020 0.4956 0.4187 0.089 Uiso 1 1 calc R . . . .
C5CA C 0.870(4) 0.394(3) 0.4840(14) 0.059(4) Uani 1 1 d . . . . .
H5CA H 0.9284 0.4013 0.4868 0.070 Uiso 1 1 calc R . . . .
C37 C 0.786(5) 0.128(4) 0.4419(19) 0.093(8) Uani 1 1 d . . . . .
H37 H 0.7512 0.1108 0.4638 0.112 Uiso 1 1 calc R . . . .
C4CA C 0.840(3) 0.340(3) 0.5128(15) 0.059(4) Uani 1 1 d . . . . .
H4CA H 0.8821 0.3082 0.5343 0.070 Uiso 1 1 calc R . . . .
C3CA C 0.754(3) 0.336(3) 0.5087(14) 0.059(4) Uani 1 1 d . . . . .
H3CA H 0.7415 0.2969 0.5264 0.070 Uiso 1 1 calc R . . . .
C7DA C 0.390(3) 0.921(3) 0.3322(18) 0.065(5) Uani 1 1 d . . . . .
H7DA H 0.3288 0.9252 0.3437 0.078 Uiso 1 1 calc R . . . .
C8CA C 0.752(5) 0.144(4) 0.4008(19) 0.093(8) Uani 1 1 d . . . . .
H8CA H 0.6991 0.1319 0.3930 0.112 Uiso 1 1 calc R . . . .
C1EA C 0.842(3) 0.377(3) -0.0114(15) 0.052(4) Uani 1 1 d . . . . .
H1EA H 0.8736 0.3575 -0.0388 0.063 Uiso 1 1 calc R . . . .
C49 C 0.550(4) 0.231(3) 0.1105(17) 0.069(5) Uani 1 1 d . . . . .
H49 H 0.4910 0.2315 0.1012 0.083 Uiso 1 1 calc R . . . .
C4DA C 0.516(5) 0.225(4) 0.257(2) 0.091(5) Uani 1 1 d . . . . .
C3DA C 0.400(4) 0.386(4) 0.3907(17) 0.074(6) Uani 1 1 d . . . . .
H3DA H 0.3539 0.3642 0.3858 0.089 Uiso 1 1 calc R . . . .
C2EA C 1.136(3) 0.423(4) 0.273(2) 0.077(4) Uani 1 1 d . . . . .
C5DA C 0.646(4) 0.154(3) 0.1118(17) 0.069(5) Uani 1 1 d . . . . .
H5DA H 0.6458 0.1059 0.0991 0.083 Uiso 1 1 calc R . . . .
C9DA C 0.574(3) 0.987(3) 0.1728(18) 0.065(5) Uani 1 1 d . . . . .
H9DA H 0.5231 1.0418 0.1711 0.078 Uiso 1 1 calc R . . . .
C6DA C 0.393(3) 0.987(3) 0.3057(18) 0.065(5) Uani 1 1 d . . . . .
H6DA H 0.3339 1.0350 0.3016 0.078 Uiso 1 1 calc R . . . .
C8DA C 0.269(4) 0.816(3) 0.2076(18) 0.072(5) Uani 1 1 d . . . . .
H8DA H 0.2022 0.8292 0.2164 0.086 Uiso 1 1 calc R . . . .
C7CA C 0.803(5) 0.180(4) 0.369(2) 0.093(8) Uani 1 1 d . . . . .
H7CA H 0.7764 0.1999 0.3421 0.112 Uiso 1 1 calc R . . . .
C75 C 0.980(4) 0.174(3) 0.0497(17) 0.067(5) Uani 1 1 d . . . . .
H75 H 0.9598 0.1851 0.0211 0.081 Uiso 1 1 calc R . . . .
C6CA C 0.913(5) 0.182(4) 0.4213(19) 0.093(8) Uani 1 1 d . . . . .
H6CA H 0.9555 0.2051 0.4291 0.112 Uiso 1 1 calc R . . . .
C0EA C 0.670(3) 0.978(3) 0.1849(17) 0.065(5) Uani 1 1 d . . . . .
H0EA H 0.6850 1.0249 0.1840 0.078 Uiso 1 1 calc R . . . .
C1DA C 0.558(4) 0.390(4) 0.3888(17) 0.074(6) Uani 1 1 d . . . . .
H1DA H 0.6254 0.3660 0.3790 0.089 Uiso 1 1 calc R . . . .
F1AA F 0.2581(18) 0.6899(17) 0.3777(10) 0.071(4) Uani 1 1 d . . . . .
C5EA C 1.178(4) 0.263(3) 0.1906(15) 0.061(4) Uani 1 1 d . . . . .
C7EA C 1.054(5) 0.591(4) 0.390(2) 0.093(5) Uani 1 1 d . . . . .
C6EA C 0.307(3) 0.782(3) 0.1640(18) 0.072(5) Uani 1 1 d . . . . .
H6EA H 0.2712 0.7658 0.1451 0.086 Uiso 1 1 calc R . . . .
C3EA C 0.871(5) 0.138(4) 0.452(2) 0.093(8) Uani 1 1 d . . . . .
H3EA H 0.9010 0.1161 0.4780 0.112 Uiso 1 1 calc R . . . .
F32 F 0.581(4) 0.070(4) 0.3727(17) 0.245(17) Uiso 1 1 d D . . . .
B49 B 0.516(3) 0.093(3) 0.4110(15) 0.245(17) Uiso 1 1 d D . . . .
F55 F 0.572(5) 0.087(4) 0.4478(18) 0.245(17) Uiso 1 1 d D . . . .
F200 F 0.444(4) 0.177(3) 0.406(2) 0.245(17) Uiso 1 1 d D . . . .
F58 F 0.469(5) 0.037(4) 0.417(2) 0.245(17) Uiso 1 1 d D . . . .
C34 C 1.102(3) 0.315(3) 0.4053(15) 0.115(10) Uani 1 1 d . . . . .
H34 H 1.0867 0.3640 0.4216 0.138 Uiso 1 1 calc R . . . .
C31 C 1.028(2) 0.304(3) 0.3845(15) 0.115(10) Uani 1 1 d G . . . .
H31 H 0.9623 0.3452 0.3869 0.138 Uiso 1 1 calc R . . . .
C20 C 1.051(3) 0.230(3) 0.3603(15) 0.115(10) Uani 1 1 d G . . . .
C0DA C 1.149(3) 0.168(3) 0.3568(15) 0.115(10) Uani 1 1 d G . . . .
H0DA H 1.1647 0.1192 0.3405 0.138 Uiso 1 1 calc R . . . .
C8EA C 1.224(2) 0.180(3) 0.3775(15) 0.115(10) Uani 1 1 d G . . . .
H8EA H 1.2890 0.1380 0.3752 0.138 Uiso 1 1 calc R . . . .
C9CA C 1.200(3) 0.253(3) 0.4018(15) 0.115(10) Uani 1 1 d G . . . .
H9CA H 1.2500 0.2605 0.4157 0.138 Uiso 1 1 calc R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au01 Au02 2.7416(19) . ?
Au01 Au03 2.706(2) . ?
Au01 Au04 2.773(2) . ?
Au01 Au05 2.7263(19) . ?
Au01 Au06 2.778(2) . ?
Au01 Au07 2.757(2) . ?
Au01 Ag08 2.769(3) . ?
Au01 Ag09 2.760(3) . ?
Au01 Ag0A 2.772(3) . ?
Au01 Ag0B 2.771(3) . ?
Au01 Ag0C 2.808(3) . ?
Au01 Ag0D 2.797(3) . ?
Au02 Au06 2.902(2) . ?
Au02 Au07 2.896(2) . ?
Au02 Ag09 2.882(3) . ?
Au02 Ag0A 2.888(3) . ?
Au02 Ag0B 2.844(3) . ?
Au02 P0M 2.282(9) . ?
Au03 Au05 2.873(2) . ?
Au03 Au06 2.899(2) . ?
Au03 Ag08 2.874(3) . ?
Au03 Ag09 2.887(3) . ?
Au03 Ag0D 2.982(4) . ?
Au03 P00P 2.277(11) . ?
Au04 Au05 2.877(2) . ?
Au04 Au07 2.914(2) . ?
Au04 Ag08 2.921(3) . ?
Au04 Ag0A 2.912(3) . ?
Au04 Ag0C 2.863(3) . ?
Au04 P00O 2.304(11) . ?
Au05 Ag08 3.010(3) . ?
Au05 Ag0C 2.893(3) . ?
Au05 Ag0D 2.946(3) . ?
Au05 Ag0F 3.018(4) . ?
Au05 P0N 2.311(10) . ?
Au06 Ag09 2.874(3) . ?
Au06 Ag0B 2.938(4) . ?
Au06 Ag0D 2.912(3) . ?
Au06 P0L 2.312(10) . ?
Au07 Ag0A 2.863(3) . ?
Au07 Ag0B 2.885(4) . ?
Au07 Ag0C 2.832(3) . ?
Au07 P0K 2.315(11) . ?
Ag08 Ag09 2.879(4) . ?
Ag08 Ag0A 2.899(4) . ?
Ag08 Ag0E 2.936(4) . ?
Ag08 O14 2.15(3) . ?
Ag09 Ag0A 2.947(4) . ?
Ag09 Ag0E 2.825(4) . ?
Ag09 O52 2.22(3) . ?
Ag0A Ag0E 2.860(4) . ?
Ag0A O8 2.18(3) . ?
Ag0B Ag0C 2.981(4) . ?
Ag0B Ag0D 2.877(5) . ?
Ag0B O31 2.74(3) . ?
Ag0B O40 2.18(4) . ?
Ag0C Ag0D 3.021(5) . ?
Ag0C Ag0F 2.804(5) . ?
Ag0C O31 2.34(3) . ?
Ag0C O38 2.24(3) . ?
Ag0D Ag0F 2.967(5) . ?
Ag0D O16 2.22(4) . ?
Ag0D O12 2.49(6) . ?
Ag0E O17 2.23(2) . ?
Ag0E O20 2.35(3) . ?
Ag0E O0AA 2.26(4) . ?
Ag0F O15 2.35(4) . ?
Ag0F O21 2.30(3) . ?
Ag0F O1AA 2.49(7) . ?
Fe0H C33 2.00(4) . ?
Fe0H C36 2.06(4) . ?
Fe0H C48 2.03(4) . ?
Fe0H C38 2.04(4) . ?
Fe0H C60 2.02(4) . ?
Fe0H C76 2.04(4) . ?
Fe0H C88 2.01(4) . ?
Fe0H C92 2.02(4) . ?
Fe0H C4BA 1.97(4) . ?
Fe0H C3BA 2.05(4) . ?
Fe0I C19 1.99(4) . ?
Fe0I C0AA 2.06(4) . ?
Fe0I C56 2.02(4) . ?
Fe0I C63 2.05(4) . ?
Fe0I C86 2.09(4) . ?
Fe0I C5BA 2.15(4) . ?
Fe0I C61 2.06(4) . ?
Fe0I C6BA 2.13(4) . ?
Fe0I C67 2.03(4) . ?
Fe0I C7BA 1.97(4) . ?
Fe0J C16 1.97(4) . ?
Fe0J C23 2.04(4) . ?
Fe0J C41 2.04(4) . ?
Fe0J C45 2.05(4) . ?
Fe0J C65 2.11(4) . ?
Fe0J C71 2.00(4) . ?
Fe0J C85 2.08(4) . ?
Fe0J C90 1.99(4) . ?
Fe0J C6AA 1.99(4) . ?
Fe0J C4EA 2.20(5) . ?
P0K C36 1.74(4) . ?
P0K C78 1.84(5) . ?
P0K C20 1.82(3) . ?
P0L C45 1.80(5) . ?
P0L C64 1.82(4) . ?
P0L C74 1.77(5) . ?
P0M C71 1.86(4) . ?
P0M C73 1.81(5) . ?
P0M C84 1.80(5) . ?
P0N C13 1.85(4) . ?
P0N C91 1.90(5) . ?
P0N C7BA 1.84(4) . ?
P00O C69 1.75(5) . ?
P00O C87 1.92(5) . ?
P00O C88 1.84(4) . ?
P00P C50 1.84(5) . ?
P00P C57 1.83(5) . ?
P00P C67 1.77(4) . ?
O8 C43 1.29(7) . ?
O14 C44 1.37(5) . ?
O15 C24 1.17(7) . ?
O15 Ag1 2.53(4) 1_655 ?
O16 C24 1.26(7) . ?
O17 C43 1.23(7) . ?
O20 Ag1 2.58(3) . ?
O20 C44 1.28(5) . ?
O21 C5EA 1.36(5) . ?
C24 C9AA 1.61(8) . ?
O31 C2EA 1.33(6) . ?
C33 H33 0.9300 . ?
C33 C36 1.34(6) . ?
C33 C60 1.32(6) . ?
C36 C38 1.51(6) . ?
O38 C5EA 1.25(5) . ?
C48 H48 0.9300 . ?
C48 C88 1.44(6) . ?
C48 C3BA 1.42(5) . ?
C50 C0CA 1.37(7) . ?
C50 C2CA 1.39(7) . ?
Ag1 O15 2.53(4) 1_455 ?
Ag1 O1AA 2.49(7) 1_455 ?
C44 C77 1.45(6) . ?
C38 H38 0.9300 . ?
C38 C92 1.36(6) . ?
O40 C70 1.26(7) . ?
C43 C4DA 1.65(8) . ?
O9 C70 1.30(7) . ?
C13 C46 1.35(6) . ?
C13 C53 1.40(6) . ?
C16 H16 0.9800 . ?
C16 C65 1.47(5) . ?
C16 C71 1.35(6) . ?
C18 H18 0.9300 . ?
C18 C32 1.39(6) . ?
C18 C91 1.33(6) . ?
C19 H19 0.9300 . ?
C19 C0AA 1.47(6) . ?
C19 C7BA 1.30(6) . ?
C23 H23 0.9300 . ?
C23 C41 1.30(6) . ?
C23 C45 1.34(7) . ?
F25 C77 1.30(5) . ?
C30 H30 0.9300 . ?
C30 C32 1.40(6) . ?
C30 C98 1.31(6) . ?
C32 H32 0.9300 . ?
F34 C77 1.32(5) . ?
F36 C7EA 1.19(7) . ?
O0AA C81 1.35(6) . ?
C40 H40 0.9300 . ?
C40 C74 1.46(7) . ?
C40 C9BA 1.31(6) . ?
C41 H41 0.9300 . ?
C41 C6AA 1.51(6) . ?
C42 H42 0.9300 . ?
C42 C62 1.24(6) . ?
C42 C96 1.37(6) . ?
C45 C4EA 1.53(6) . ?
C46 H46 0.9300 . ?
C46 C1EA 1.42(6) . ?
C0AA H0AA 0.9300 . ?
C0AA C6BA 1.34(6) . ?
O52 C81 1.17(5) . ?
F53 C77 1.25(5) . ?
C56 H56 0.9300 . ?
C56 C6BA 1.52(6) . ?
C56 C7BA 1.38(6) . ?
C57 C66 1.41(6) . ?
C57 C8BA 1.43(6) . ?
C60 H60 0.9300 . ?
C60 C92 1.37(6) . ?
C62 H62 0.9300 . ?
C62 C64 1.36(6) . ?
C63 H63 0.9300 . ?
C63 C61 1.50(6) . ?
C63 C67 1.54(6) . ?
C64 C8AA 1.35(6) . ?
C65 H65 0.9300 . ?
C65 C85 1.41(6) . ?
C69 C99 1.38(7) . ?
C69 C95 1.56(7) . ?
C70 C7EA 1.51(8) . ?
C71 C90 1.39(5) . ?
C72 H72 0.9300 . ?
C72 C91 1.42(6) . ?
C72 C98 1.37(6) . ?
C74 C52 1.51(6) . ?
C76 H76 0.9300 . ?
C76 C4BA 1.38(5) . ?
C76 C3BA 1.52(6) . ?
C78 C7CA 1.25(8) . ?
C78 C6CA 1.39(9) . ?
F83 C7EA 1.45(7) . ?
C85 H85 0.9300 . ?
C85 C90 1.38(6) . ?
C86 H86 0.9300 . ?
C86 C5BA 1.45(6) . ?
C86 C61 1.31(6) . ?
C87 C2AA 1.47(7) . ?
C87 C3AA 1.34(7) . ?
C88 C4BA 1.31(6) . ?
C90 H90 0.9300 . ?
C92 H92 0.9300 . ?
F94 C7EA 1.31(7) . ?
C98 H98 0.9300 . ?
C99 H99 0.9300 . ?
C99 C51 1.40(6) . ?
F3 C5AA 1.27(5) . ?
F5 C0BA 1.40(6) . ?
F12 C2BA 1.35(5) . ?
F13 C0BA 1.18(6) . ?
F19 C2BA 1.36(6) . ?
F20 C5AA 1.41(5) . ?
F24 C2BA 1.32(6) . ?
C29 H29 0.9300 . ?
C29 C66 1.36(6) . ?
C29 C0EA 1.36(6) . ?
C4AA H4AA 0.9300 . ?
C4AA C2AA 1.26(6) . ?
C4AA C54 1.35(7) . ?
C5AA C81 1.51(6) . ?
C5AA F1AA 1.35(6) . ?
F35 C0BA 1.26(6) . ?
C1AA H1AA 0.9300 . ?
C1AA C47 1.39(6) . ?
C1AA C53 1.38(6) . ?
C39 H39 0.9300 . ?
C39 C84 1.38(6) . ?
C39 C3CA 1.47(6) . ?
C1CA H1CA 0.9300 . ?
C1CA C0CA 1.33(6) . ?
C1CA C8DA 1.39(7) . ?
C1BA H1BA 0.9300 . ?
C1BA C84 1.47(6) . ?
C1BA C5CA 1.29(6) . ?
F43 C9AA 1.29(7) . ?
C8AA H8AA 0.9300 . ?
C8AA C7AA 1.51(6) . ?
C2AA H2AA 0.9300 . ?
F46 C9AA 1.12(7) . ?
C47 H47 0.9300 . ?
C47 C1EA 1.34(6) . ?
C5BA H5BA 0.9300 . ?
C5BA C67 1.59(6) . ?
C51 H51 0.9300 . ?
C51 C49 1.43(7) . ?
C52 H52 0.9300 . ?
C52 C7DA 1.20(6) . ?
C53 H53 0.9300 . ?
C54 H54 0.9300 . ?
C54 C75 1.40(7) . ?
C4BA H4BA 0.9300 . ?
C2BA C5EA 1.41(6) . ?
C61 H61 0.9300 . ?
C6BA H6BA 0.9300 . ?
C3AA H3AA 0.9300 . ?
C3AA C75 1.32(6) . ?
C66 H66 0.9300 . ?
C0BA C2EA 1.53(7) . ?
C3BA H3BA 0.9300 . ?
C6AA H6AA 0.9300 . ?
C6AA C4EA 1.49(7) . ?
C73 C80 1.31(7) . ?
C73 C1DA 1.19(7) . ?
C0CA H0CA 0.9300 . ?
C7AA H7AA 0.9300 . ?
C7AA C96 1.38(6) . ?
C80 H80 0.9300 . ?
C80 C28 1.46(6) . ?
C4EA H4EA 0.9300 . ?
F87 C9AA 1.25(7) . ?
C8BA H8BA 0.9300 . ?
C8BA C9DA 1.17(6) . ?
C2CA H2CA 0.9300 . ?
C2CA C6EA 1.37(6) . ?
C9BA H9BA 0.9300 . ?
C9BA C6DA 1.39(6) . ?
C95 H95 0.9300 . ?
C95 C5DA 1.26(6) . ?
C96 H96 0.9300 . ?
O1AA Ag1 2.49(7) 1_655 ?
O1AA O12 0.86(8) . ?
O1AA C2EA 1.30(9) . ?
O12 C2EA 1.58(9) . ?
F15 C4DA 1.36(7) . ?
F16 C4DA 1.29(7) . ?
C2DA H2DA 0.9300 . ?
C2DA C3DA 1.47(7) . ?
C2DA C1DA 1.48(7) . ?
F0AA C4DA 1.35(7) . ?
C28 H28 0.9300 . ?
C28 C3DA 1.38(8) . ?
C5CA H5CA 0.9300 . ?
C5CA C4CA 1.45(6) . ?
C37 H37 0.9300 . ?
C37 C8CA 1.36(8) . ?
C37 C3EA 1.39(8) . ?
C4CA H4CA 0.9300 . ?
C4CA C3CA 1.31(6) . ?
C3CA H3CA 0.9300 . ?
C7DA H7DA 0.9300 . ?
C7DA C6DA 1.39(7) . ?
C8CA H8CA 0.9300 . ?
C8CA C7CA 1.47(7) . ?
C1EA H1EA 0.9300 . ?
C49 H49 0.9300 . ?
C49 C5DA 1.49(7) . ?
C3DA H3DA 0.9300 . ?
C5DA H5DA 0.9300 . ?
C9DA H9DA 0.9300 . ?
C9DA C0EA 1.43(6) . ?
C6DA H6DA 0.9300 . ?
C8DA H8DA 0.9300 . ?
C8DA C6EA 1.45(7) . ?
C7CA H7CA 0.9300 . ?
C75 H75 0.9300 . ?
C6CA H6CA 0.9300 . ?
C6CA C3EA 1.46(7) . ?
C0EA H0EA 0.9300 . ?
C1DA H1DA 0.9300 . ?
C6EA H6EA 0.9300 . ?
C3EA H3EA 0.9300 . ?
F32 B49 1.406(18) . ?
B49 F55 1.413(18) . ?
B49 F200 1.413(18) . ?
B49 F58 1.409(18) . ?
C34 H34 0.9300 . ?
C34 C31 1.3900 . ?
C34 C9CA 1.3900 . ?
C31 H31 0.9300 . ?
C31 C20 1.3900 . ?
C20 C0DA 1.3900 . ?
C0DA H0DA 0.9300 . ?
C0DA C8EA 1.3900 . ?
C8EA H8EA 0.9300 . ?
C8EA C9CA 1.3900 . ?
C9CA H9CA 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au02 Au01 Au04 116.94(7) . . ?
Au02 Au01 Au06 63.44(5) . . ?
Au02 Au01 Au07 63.57(5) . . ?
Au02 Au01 Ag08 115.24(8) . . ?
Au02 Au01 Ag09 63.18(7) . . ?
Au02 Au01 Ag0A 63.17(7) . . ?
Au02 Au01 Ag0B 62.12(7) . . ?
Au02 Au01 Ag0C 115.34(8) . . ?
Au02 Au01 Ag0D 114.48(8) . . ?
Au03 Au01 Au02 117.19(7) . . ?
Au03 Au01 Au04 115.46(6) . . ?
Au03 Au01 Au05 63.87(5) . . ?
Au03 Au01 Au06 63.81(5) . . ?
Au03 Au01 Au07 179.05(7) . . ?
Au03 Au01 Ag08 63.32(7) . . ?
Au03 Au01 Ag09 63.76(7) . . ?
Au03 Au01 Ag0A 117.31(8) . . ?
Au03 Au01 Ag0B 117.87(9) . . ?
Au03 Au01 Ag0C 118.54(9) . . ?
Au03 Au01 Ag0D 65.61(9) . . ?
Au04 Au01 Au06 179.18(8) . . ?
Au04 Au01 Ag0C 61.73(8) . . ?
Au04 Au01 Ag0D 117.19(9) . . ?
Au05 Au01 Au02 178.24(7) . . ?
Au05 Au01 Au04 63.07(5) . . ?
Au05 Au01 Au06 116.57(7) . . ?
Au05 Au01 Au07 115.39(7) . . ?
Au05 Au01 Ag08 66.43(7) . . ?
Au05 Au01 Ag09 118.49(8) . . ?
Au05 Au01 Ag0A 117.82(8) . . ?
Au05 Au01 Ag0B 116.20(8) . . ?
Au05 Au01 Ag0C 63.01(8) . . ?
Au05 Au01 Ag0D 64.46(8) . . ?
Au06 Au01 Ag0C 118.87(9) . . ?
Au06 Au01 Ag0D 62.97(8) . . ?
Au07 Au01 Au04 63.59(5) . . ?
Au07 Au01 Au06 117.14(6) . . ?
Au07 Au01 Ag08 115.91(8) . . ?
Au07 Au01 Ag09 116.52(8) . . ?
Au07 Au01 Ag0A 62.38(7) . . ?
Au07 Au01 Ag0B 62.92(8) . . ?
Au07 Au01 Ag0C 61.17(8) . . ?
Au07 Au01 Ag0D 114.74(9) . . ?
Ag08 Au01 Au04 63.61(7) . . ?
Ag08 Au01 Au06 115.59(8) . . ?
Ag08 Au01 Ag0A 63.10(8) . . ?
Ag08 Au01 Ag0B 177.34(10) . . ?
Ag08 Au01 Ag0C 117.22(10) . . ?
Ag08 Au01 Ag0D 120.14(10) . . ?
Ag09 Au01 Au04 116.91(8) . . ?
Ag09 Au01 Au06 62.52(7) . . ?
Ag09 Au01 Ag08 62.76(8) . . ?
Ag09 Au01 Ag0A 64.38(9) . . ?
Ag09 Au01 Ag0B 115.34(10) . . ?
Ag09 Au01 Ag0C 177.58(11) . . ?
Ag09 Au01 Ag0D 117.01(11) . . ?
Ag0A Au01 Au04 63.37(7) . . ?
Ag0A Au01 Au06 116.52(8) . . ?
Ag0A Au01 Ag0C 113.33(11) . . ?
Ag0A Au01 Ag0D 176.74(11) . . ?
Ag0B Au01 Au04 116.86(9) . . ?
Ag0B Au01 Au06 63.95(8) . . ?
Ag0B Au01 Ag0A 114.56(10) . . ?
Ag0B Au01 Ag0C 64.60(9) . . ?
Ag0B Au01 Ag0D 62.21(10) . . ?
Ag0D Au01 Ag0C 65.24(11) . . ?
Au01 Au02 Au06 58.89(5) . . ?
Au01 Au02 Au07 58.48(5) . . ?
Au01 Au02 Ag09 58.72(6) . . ?
Au01 Au02 Ag0A 58.93(7) . . ?
Au01 Au02 Ag0B 59.45(7) . . ?
Au07 Au02 Au06 109.08(6) . . ?
Ag09 Au02 Au06 59.58(7) . . ?
Ag09 Au02 Au07 108.58(7) . . ?
Ag09 Au02 Ag0A 61.42(8) . . ?
Ag0A Au02 Au06 109.20(8) . . ?
Ag0A Au02 Au07 59.34(7) . . ?
Ag0B Au02 Au06 61.50(8) . . ?
Ag0B Au02 Au07 60.33(8) . . ?
Ag0B Au02 Ag09 109.40(9) . . ?
Ag0B Au02 Ag0A 108.89(9) . . ?
P0M Au02 Au01 171.0(3) . . ?
P0M Au02 Au06 124.5(3) . . ?
P0M Au02 Au07 122.7(3) . . ?
P0M Au02 Ag09 114.6(3) . . ?
P0M Au02 Ag0A 113.1(3) . . ?
P0M Au02 Ag0B 129.5(3) . . ?
Au01 Au03 Au05 58.41(5) . . ?
Au01 Au03 Au06 59.31(5) . . ?
Au01 Au03 Ag08 59.42(7) . . ?
Au01 Au03 Ag09 59.04(7) . . ?
Au01 Au03 Ag0D 58.67(7) . . ?
Au05 Au03 Au06 108.43(7) . . ?
Au05 Au03 Ag08 63.17(7) . . ?
Au05 Au03 Ag09 109.87(8) . . ?
Au05 Au03 Ag0D 60.39(7) . . ?
Au06 Au03 Ag0D 59.34(7) . . ?
Ag08 Au03 Au06 108.79(8) . . ?
Ag08 Au03 Ag09 59.96(8) . . ?
Ag08 Au03 Ag0D 110.90(10) . . ?
Ag09 Au03 Au06 59.56(7) . . ?
Ag09 Au03 Ag0D 107.67(9) . . ?
P00P Au03 Au01 170.1(3) . . ?
P00P Au03 Au05 122.7(3) . . ?
P00P Au03 Au06 124.9(3) . . ?
P00P Au03 Ag08 111.5(3) . . ?
P00P Au03 Ag09 114.0(3) . . ?
P00P Au03 Ag0D 131.1(3) . . ?
Au01 Au04 Au05 57.67(5) . . ?
Au01 Au04 Au07 57.94(5) . . ?
Au01 Au04 Ag08 58.13(7) . . ?
Au01 Au04 Ag0A 58.30(7) . . ?
Au01 Au04 Ag0C 59.73(8) . . ?
Au05 Au04 Au07 106.34(6) . . ?
Au05 Au04 Ag08 62.56(7) . . ?
Au05 Au04 Ag0A 108.85(8) . . ?
Au07 Au04 Ag08 106.81(7) . . ?
Ag0A Au04 Au07 58.87(7) . . ?
Ag0A Au04 Ag08 59.61(8) . . ?
Ag0C Au04 Au05 60.52(8) . . ?
Ag0C Au04 Au07 58.70(7) . . ?
Ag0C Au04 Ag08 110.79(10) . . ?
Ag0C Au04 Ag0A 107.63(9) . . ?
P00O Au04 Au01 174.3(3) . . ?
P00O Au04 Au05 126.1(3) . . ?
P00O Au04 Au07 121.4(3) . . ?
P00O Au04 Ag08 118.7(3) . . ?
P00O Au04 Ag0A 116.1(3) . . ?
P00O Au04 Ag0C 125.4(3) . . ?
Au01 Au05 Au03 57.71(5) . . ?
Au01 Au05 Au04 59.25(5) . . ?
Au01 Au05 Ag08 57.47(6) . . ?
Au01 Au05 Ag0C 59.87(7) . . ?
Au01 Au05 Ag0D 58.93(7) . . ?
Au01 Au05 Ag0F 105.38(8) . . ?
Au03 Au05 Au04 107.35(6) . . ?
Au03 Au05 Ag08 58.43(7) . . ?
Au03 Au05 Ag0C 110.56(8) . . ?
Au03 Au05 Ag0D 61.63(8) . . ?
Au03 Au05 Ag0F 117.36(9) . . ?
Au04 Au05 Ag08 59.44(7) . . ?
Au04 Au05 Ag0C 59.51(8) . . ?
Au04 Au05 Ag0D 109.45(8) . . ?
Au04 Au05 Ag0F 110.67(9) . . ?
Ag08 Au05 Ag0F 162.54(10) . . ?
Ag0C Au05 Ag08 107.49(9) . . ?
Ag0C Au05 Ag0D 62.31(10) . . ?
Ag0C Au05 Ag0F 56.59(9) . . ?
Ag0D Au05 Ag08 108.15(9) . . ?
Ag0D Au05 Ag0F 59.64(9) . . ?
P0N Au05 Au01 176.6(3) . . ?
P0N Au05 Au03 119.0(3) . . ?
P0N Au05 Au04 122.8(3) . . ?
P0N Au05 Ag08 120.6(3) . . ?
P0N Au05 Ag0C 123.4(3) . . ?
P0N Au05 Ag0D 120.9(3) . . ?
P0N Au05 Ag0F 76.7(3) . . ?
Au01 Au06 Au02 57.67(5) . . ?
Au01 Au06 Au03 56.88(5) . . ?
Au01 Au06 Ag09 58.44(7) . . ?
Au01 Au06 Ag0B 57.91(7) . . ?
Au01 Au06 Ag0D 58.83(7) . . ?
Au02 Au06 Ag0B 58.28(7) . . ?
Au02 Au06 Ag0D 106.48(9) . . ?
Au03 Au06 Au02 106.54(6) . . ?
Au03 Au06 Ag0B 106.97(8) . . ?
Au03 Au06 Ag0D 61.75(8) . . ?
Ag09 Au06 Au02 59.86(7) . . ?
Ag09 Au06 Au03 60.02(7) . . ?
Ag09 Au06 Ag0B 107.05(9) . . ?
Ag09 Au06 Ag0D 109.98(9) . . ?
Ag0D Au06 Ag0B 58.90(9) . . ?
P0L Au06 Au01 177.3(3) . . ?
P0L Au06 Au02 119.7(3) . . ?
P0L Au06 Au03 125.0(3) . . ?
P0L Au06 Ag09 120.3(3) . . ?
P0L Au06 Ag0B 121.6(3) . . ?
P0L Au06 Ag0D 123.5(3) . . ?
Au01 Au07 Au02 57.95(5) . . ?
Au01 Au07 Au04 58.47(5) . . ?
Au01 Au07 Ag0A 59.07(7) . . ?
Au01 Au07 Ag0B 58.78(7) . . ?
Au01 Au07 Ag0C 60.30(8) . . ?
Au02 Au07 Au04 108.00(6) . . ?
Ag0A Au07 Au02 60.19(7) . . ?
Ag0A Au07 Au04 60.54(7) . . ?
Ag0A Au07 Ag0B 108.44(10) . . ?
Ag0B Au07 Au02 58.94(7) . . ?
Ag0B Au07 Au04 109.09(8) . . ?
Ag0C Au07 Au02 109.90(9) . . ?
Ag0C Au07 Au04 59.76(7) . . ?
Ag0C Au07 Ag0A 109.88(9) . . ?
Ag0C Au07 Ag0B 62.85(9) . . ?
P0K Au07 Au01 171.2(3) . . ?
P0K Au07 Au02 126.2(3) . . ?
P0K Au07 Au04 121.9(3) . . ?
P0K Au07 Ag0A 129.5(3) . . ?
P0K Au07 Ag0B 115.3(3) . . ?
P0K Au07 Ag0C 111.6(3) . . ?
Au01 Ag08 Au03 57.26(7) . . ?
Au01 Ag08 Au04 58.26(7) . . ?
Au01 Ag08 Au05 56.10(6) . . ?
Au01 Ag08 Ag09 58.46(8) . . ?
Au01 Ag08 Ag0A 58.50(8) . . ?
Au01 Ag08 Ag0E 105.06(11) . . ?
Au03 Ag08 Au04 106.14(9) . . ?
Au03 Ag08 Au05 58.40(7) . . ?
Au03 Ag08 Ag09 60.24(8) . . ?
Au03 Ag08 Ag0A 108.25(10) . . ?
Au03 Ag08 Ag0E 113.80(11) . . ?
Au04 Ag08 Au05 58.00(6) . . ?
Au04 Ag08 Ag0E 114.04(11) . . ?
Ag09 Ag08 Au04 108.78(10) . . ?
Ag09 Ag08 Au05 106.34(10) . . ?
Ag09 Ag08 Ag0A 61.33(10) . . ?
Ag09 Ag08 Ag0E 58.13(9) . . ?
Ag0A Ag08 Au04 60.06(8) . . ?
Ag0A Ag08 Au05 105.63(10) . . ?
Ag0A Ag08 Ag0E 58.70(9) . . ?
Ag0E Ag08 Au05 161.16(12) . . ?
O14 Ag08 Au01 170.0(8) . . ?
O14 Ag08 Au03 116.3(7) . . ?
O14 Ag08 Au04 121.2(9) . . ?
O14 Ag08 Au05 114.4(8) . . ?
O14 Ag08 Ag09 126.8(9) . . ?
O14 Ag08 Ag0A 130.9(7) . . ?
O14 Ag08 Ag0E 84.4(8) . . ?
Au01 Ag09 Au02 58.10(7) . . ?
Au01 Ag09 Au03 57.20(7) . . ?
Au01 Ag09 Au06 59.05(7) . . ?
Au01 Ag09 Ag08 58.78(8) . . ?
Au01 Ag09 Ag0A 58.01(8) . . ?
Au01 Ag09 Ag0E 108.37(11) . . ?
Au02 Ag09 Au03 107.40(9) . . ?
Au02 Ag09 Ag0A 59.39(8) . . ?
Au03 Ag09 Ag0A 106.62(10) . . ?
Au06 Ag09 Au02 60.56(7) . . ?
Au06 Ag09 Au03 60.42(7) . . ?
Au06 Ag09 Ag08 109.36(10) . . ?
Au06 Ag09 Ag0A 108.37(10) . . ?
Ag08 Ag09 Au02 107.78(11) . . ?
Ag08 Ag09 Au03 59.80(8) . . ?
Ag08 Ag09 Ag0A 59.68(9) . . ?
Ag0E Ag09 Au02 111.40(12) . . ?
Ag0E Ag09 Au03 116.89(11) . . ?
Ag0E Ag09 Au06 167.07(13) . . ?
Ag0E Ag09 Ag08 61.95(10) . . ?
Ag0E Ag09 Ag0A 59.37(10) . . ?
O52 Ag09 Au01 162.8(9) . . ?
O52 Ag09 Au02 106.7(8) . . ?
O52 Ag09 Au03 128.7(8) . . ?
O52 Ag09 Au06 107.8(8) . . ?
O52 Ag09 Ag08 138.2(9) . . ?
O52 Ag09 Ag0A 123.6(7) . . ?
O52 Ag09 Ag0E 83.8(8) . . ?
Au01 Ag0A Au02 57.90(7) . . ?
Au01 Ag0A Au04 58.33(7) . . ?
Au01 Ag0A Au07 58.56(7) . . ?
Au01 Ag0A Ag08 58.40(8) . . ?
Au01 Ag0A Ag09 57.61(8) . . ?
Au01 Ag0A Ag0E 107.04(11) . . ?
Au02 Ag0A Au04 108.25(9) . . ?
Au02 Ag0A Ag08 107.06(11) . . ?
Au02 Ag0A Ag09 59.19(8) . . ?
Au04 Ag0A Ag09 107.17(10) . . ?
Au07 Ag0A Au02 60.47(7) . . ?
Au07 Ag0A Au04 60.58(7) . . ?
Au07 Ag0A Ag08 108.75(10) . . ?
Au07 Ag0A Ag09 107.70(10) . . ?
Ag08 Ag0A Au04 60.34(8) . . ?
Ag08 Ag0A Ag09 59.00(9) . . ?
Ag0E Ag0A Au02 110.20(11) . . ?
Ag0E Ag0A Au04 116.65(11) . . ?
Ag0E Ag0A Au07 165.19(13) . . ?
Ag0E Ag0A Ag08 61.29(10) . . ?
Ag0E Ag0A Ag09 58.20(10) . . ?
O8 Ag0A Au01 161.9(8) . . ?
O8 Ag0A Au02 131.5(8) . . ?
O8 Ag0A Au04 104.4(8) . . ?
O8 Ag0A Au07 109.9(8) . . ?
O8 Ag0A Ag08 120.1(8) . . ?
O8 Ag0A Ag09 139.3(8) . . ?
O8 Ag0A Ag0E 84.9(8) . . ?
Au01 Ag0B Au02 58.43(7) . . ?
Au01 Ag0B Au06 58.14(7) . . ?
Au01 Ag0B Au07 58.30(7) . . ?
Au01 Ag0B Ag0C 58.29(8) . . ?
Au01 Ag0B Ag0D 59.33(9) . . ?
Au02 Ag0B Au06 60.22(7) . . ?
Au02 Ag0B Au07 60.72(7) . . ?
Au02 Ag0B Ag0C 107.19(11) . . ?
Au02 Ag0B Ag0D 109.00(12) . . ?
Au06 Ag0B Ag0C 108.67(11) . . ?
Au07 Ag0B Au06 108.38(10) . . ?
Au07 Ag0B Ag0C 57.70(9) . . ?
Ag0D Ag0B Au06 60.08(10) . . ?
Ag0D Ag0B Au07 108.54(11) . . ?
Ag0D Ag0B Ag0C 62.06(11) . . ?
O31 Ag0B Au01 106.4(8) . . ?
O31 Ag0B Au02 143.4(8) . . ?
O31 Ag0B Au06 144.4(8) . . ?
O31 Ag0B Au07 82.8(8) . . ?
O31 Ag0B Ag0C 48.2(7) . . ?
O31 Ag0B Ag0D 84.3(8) . . ?
O40 Ag0B Au01 156.5(11) . . ?
O40 Ag0B Au02 107.4(10) . . ?
O40 Ag0B Au06 99.0(11) . . ?
O40 Ag0B Au07 134.6(12) . . ?
O40 Ag0B Ag0C 143.2(10) . . ?
O40 Ag0B Ag0D 116.4(12) . . ?
O40 Ag0B O31 95.6(13) . . ?
Au01 Ag0C Au04 58.54(7) . . ?
Au01 Ag0C Au05 57.12(7) . . ?
Au01 Ag0C Au07 58.53(7) . . ?
Au01 Ag0C Ag0B 57.11(8) . . ?
Au01 Ag0C Ag0D 57.21(9) . . ?
Au04 Ag0C Au05 59.97(7) . . ?
Au04 Ag0C Ag0B 107.83(11) . . ?
Au04 Ag0C Ag0D 107.75(12) . . ?
Au05 Ag0C Ag0B 105.22(12) . . ?
Au05 Ag0C Ag0D 59.72(10) . . ?
Au07 Ag0C Au04 61.54(7) . . ?
Au07 Ag0C Au05 108.12(10) . . ?
Au07 Ag0C Ag0B 59.45(9) . . ?
Au07 Ag0C Ag0D 106.06(11) . . ?
Ag0B Ag0C Ag0D 57.27(11) . . ?
Ag0F Ag0C Au01 109.13(14) . . ?
Ag0F Ag0C Au04 117.66(13) . . ?
Ag0F Ag0C Au05 63.97(10) . . ?
Ag0F Ag0C Au07 166.86(15) . . ?
Ag0F Ag0C Ag0B 111.09(15) . . ?
Ag0F Ag0C Ag0D 61.10(11) . . ?
O31 Ag0C Au01 117.5(8) . . ?
O31 Ag0C Au04 151.1(9) . . ?
O31 Ag0C Au05 145.7(9) . . ?
O31 Ag0C Au07 91.4(9) . . ?
O31 Ag0C Ag0B 60.4(8) . . ?
O31 Ag0C Ag0D 88.3(9) . . ?
O31 Ag0C Ag0F 91.0(9) . . ?
O38 Ag0C Au01 151.3(8) . . ?
O38 Ag0C Au04 92.9(8) . . ?
O38 Ag0C Au05 107.8(8) . . ?
O38 Ag0C Au07 113.2(8) . . ?
O38 Ag0C Ag0B 146.6(8) . . ?
O38 Ag0C Ag0D 140.7(8) . . ?
O38 Ag0C Ag0F 79.8(8) . . ?
O38 Ag0C O31 88.8(12) . . ?
Au01 Ag0D Au03 55.72(7) . . ?
Au01 Ag0D Au05 56.61(7) . . ?
Au01 Ag0D Au06 58.20(7) . . ?
Au01 Ag0D Ag0B 58.46(9) . . ?
Au01 Ag0D Ag0C 57.55(9) . . ?
Au01 Ag0D Ag0F 104.96(13) . . ?
Au03 Ag0D Ag0C 104.28(11) . . ?
Au05 Ag0D Au03 57.98(7) . . ?
Au05 Ag0D Ag0C 57.97(9) . . ?
Au05 Ag0D Ag0F 61.39(9) . . ?
Au06 Ag0D Au03 58.91(7) . . ?
Au06 Ag0D Au05 106.13(10) . . ?
Au06 Ag0D Ag0C 108.31(11) . . ?
Au06 Ag0D Ag0F 162.96(14) . . ?
Ag0B Ag0D Au03 106.40(11) . . ?
Ag0B Ag0D Au05 106.55(12) . . ?
Ag0B Ag0D Au06 61.01(9) . . ?
Ag0B Ag0D Ag0C 60.67(11) . . ?
Ag0B Ag0D Ag0F 109.47(15) . . ?
Ag0F Ag0D Au03 115.60(12) . . ?
Ag0F Ag0D Ag0C 55.84(11) . . ?
O16 Ag0D Au01 157.8(11) . . ?
O16 Ag0D Au03 102.2(11) . . ?
O16 Ag0D Au05 112.5(11) . . ?
O16 Ag0D Au06 114.5(10) . . ?
O16 Ag0D Ag0B 139.7(11) . . ?
O16 Ag0D Ag0C 136.8(10) . . ?
O16 Ag0D Ag0F 82.0(10) . . ?
O16 Ag0D O12 79(2) . . ?
O12 Ag0D Au01 123.5(18) . . ?
O12 Ag0D Au03 177.9(18) . . ?
O12 Ag0D Au05 120.0(18) . . ?
O12 Ag0D Au06 122.6(18) . . ?
O12 Ag0D Ag0B 73.9(18) . . ?
O12 Ag0D Ag0C 74.1(18) . . ?
O12 Ag0D Ag0F 62.5(18) . . ?
Ag09 Ag0E Ag08 59.93(9) . . ?
Ag09 Ag0E Ag0A 62.44(10) . . ?
Ag0A Ag0E Ag08 60.01(9) . . ?
O17 Ag0E Ag08 99.9(7) . . ?
O17 Ag0E Ag09 139.9(6) . . ?
O17 Ag0E Ag0A 77.5(6) . . ?
O17 Ag0E O20 94.0(10) . . ?
O17 Ag0E O0AA 125.4(11) . . ?
O20 Ag0E Ag08 78.0(6) . . ?
O20 Ag0E Ag09 112.6(7) . . ?
O20 Ag0E Ag0A 134.2(6) . . ?
O0AA Ag0E Ag08 134.7(8) . . ?
O0AA Ag0E Ag09 82.4(7) . . ?
O0AA Ag0E Ag0A 125.2(8) . . ?
O0AA Ag0E O20 96.6(11) . . ?
Ag0C Ag0F Au05 59.44(9) . . ?
Ag0C Ag0F Ag0D 63.06(12) . . ?
Ag0D Ag0F Au05 58.97(9) . . ?
O15 Ag0F Au05 112.2(10) . . ?
O15 Ag0F Ag0C 139.5(10) . . ?
O15 Ag0F Ag0D 78.7(10) . . ?
O15 Ag0F O1AA 76(2) . . ?
O21 Ag0F Au05 125.3(8) . . ?
O21 Ag0F Ag0C 80.3(8) . . ?
O21 Ag0F Ag0D 133.5(7) . . ?
O21 Ag0F O15 122.3(13) . . ?
O21 Ag0F O1AA 78.1(18) . . ?
O1AA Ag0F Au05 121.4(16) . . ?
O1AA Ag0F Ag0C 77.4(18) . . ?
O1AA Ag0F Ag0D 67.2(16) . . ?
C33 Fe0H C36 38.4(16) . . ?
C33 Fe0H C48 155.3(16) . . ?
C33 Fe0H C38 64.3(17) . . ?
C33 Fe0H C60 38.4(16) . . ?
C33 Fe0H C76 108.2(17) . . ?
C33 Fe0H C88 161.9(17) . . ?
C33 Fe0H C92 64.1(17) . . ?
C33 Fe0H C3BA 120.8(17) . . ?
C48 Fe0H C36 164.3(16) . . ?
C48 Fe0H C38 125.3(16) . . ?
C48 Fe0H C76 69.9(16) . . ?
C48 Fe0H C3BA 40.8(15) . . ?
C38 Fe0H C36 43.1(16) . . ?
C38 Fe0H C76 159.5(17) . . ?
C38 Fe0H C3BA 157.0(17) . . ?
C60 Fe0H C36 68.3(16) . . ?
C60 Fe0H C48 120.1(17) . . ?
C60 Fe0H C38 66.3(17) . . ?
C60 Fe0H C76 120.8(17) . . ?
C60 Fe0H C3BA 103.0(17) . . ?
C76 Fe0H C36 118.7(17) . . ?
C76 Fe0H C3BA 43.5(16) . . ?
C88 Fe0H C36 126.4(16) . . ?
C88 Fe0H C48 41.9(16) . . ?
C88 Fe0H C38 112.5(16) . . ?
C88 Fe0H C60 159.0(18) . . ?
C88 Fe0H C76 68.3(15) . . ?
C88 Fe0H C92 125.8(17) . . ?
C88 Fe0H C3BA 69.8(15) . . ?
C92 Fe0H C36 69.8(16) . . ?
C92 Fe0H C48 107.6(17) . . ?
C92 Fe0H C38 39.3(16) . . ?
C92 Fe0H C60 39.6(16) . . ?
C92 Fe0H C76 157.2(16) . . ?
C92 Fe0H C3BA 119.7(17) . . ?
C4BA Fe0H C33 128.0(17) . . ?
C4BA Fe0H C36 110.1(16) . . ?
C4BA Fe0H C48 67.2(17) . . ?
C4BA Fe0H C38 127.9(16) . . ?
C4BA Fe0H C60 158.9(17) . . ?
C4BA Fe0H C76 40.1(15) . . ?
C4BA Fe0H C88 38.4(16) . . ?
C4BA Fe0H C92 161.3(16) . . ?
C4BA Fe0H C3BA 69.0(16) . . ?
C3BA Fe0H C36 154.3(17) . . ?
C19 Fe0I C0AA 42.6(16) . . ?
C19 Fe0I C56 66.1(17) . . ?
C19 Fe0I C63 130.0(17) . . ?
C19 Fe0I C86 154.6(17) . . ?
C19 Fe0I C5BA 122.8(17) . . ?
C19 Fe0I C61 168.6(17) . . ?
C19 Fe0I C6BA 67.1(17) . . ?
C19 Fe0I C67 111.1(17) . . ?
C0AA Fe0I C86 160.1(17) . . ?
C0AA Fe0I C5BA 158.2(16) . . ?
C0AA Fe0I C61 126.3(17) . . ?
C0AA Fe0I C6BA 37.2(16) . . ?
C56 Fe0I C0AA 67.5(16) . . ?
C56 Fe0I C63 146.0(17) . . ?
C56 Fe0I C86 107.2(16) . . ?
C56 Fe0I C5BA 126.6(16) . . ?
C56 Fe0I C61 114.8(16) . . ?
C56 Fe0I C6BA 42.8(15) . . ?
C56 Fe0I C67 168.7(17) . . ?
C63 Fe0I C0AA 103.4(17) . . ?
C63 Fe0I C86 69.8(16) . . ?
C63 Fe0I C5BA 73.9(16) . . ?
C63 Fe0I C61 42.9(15) . . ?
C63 Fe0I C6BA 110.0(16) . . ?
C86 Fe0I C5BA 39.9(15) . . ?
C86 Fe0I C6BA 125.9(16) . . ?
C61 Fe0I C86 36.8(16) . . ?
C61 Fe0I C5BA 66.6(17) . . ?
C61 Fe0I C6BA 105.4(17) . . ?
C6BA Fe0I C5BA 164.3(16) . . ?
C67 Fe0I C0AA 118.6(17) . . ?
C67 Fe0I C63 44.4(16) . . ?
C67 Fe0I C86 70.3(16) . . ?
C67 Fe0I C5BA 44.6(16) . . ?
C67 Fe0I C61 70.2(16) . . ?
C67 Fe0I C6BA 147.6(17) . . ?
C7BA Fe0I C19 38.2(16) . . ?
C7BA Fe0I C0AA 68.6(16) . . ?
C7BA Fe0I C56 40.5(16) . . ?
C7BA Fe0I C63 168.1(17) . . ?
C7BA Fe0I C86 120.6(17) . . ?
C7BA Fe0I C5BA 110.0(16) . . ?
C7BA Fe0I C61 149.0(16) . . ?
C7BA Fe0I C6BA 69.4(16) . . ?
C7BA Fe0I C67 130.6(17) . . ?
C16 Fe0J C23 126.3(18) . . ?
C16 Fe0J C41 103.8(19) . . ?
C16 Fe0J C45 161.8(17) . . ?
C16 Fe0J C65 41.9(14) . . ?
C16 Fe0J C71 39.7(17) . . ?
C16 Fe0J C85 66.7(16) . . ?
C16 Fe0J C90 68.7(17) . . ?
C16 Fe0J C6AA 117.6(19) . . ?
C16 Fe0J C4EA 153.3(16) . . ?
C23 Fe0J C45 38.3(18) . . ?
C23 Fe0J C65 158.4(18) . . ?
C23 Fe0J C85 162.3(18) . . ?
C23 Fe0J C4EA 66.2(17) . . ?
C41 Fe0J C23 37.3(17) . . ?
C41 Fe0J C45 68.2(19) . . ?
C41 Fe0J C65 121.4(17) . . ?
C41 Fe0J C85 159.3(17) . . ?
C41 Fe0J C4EA 71.9(18) . . ?
C45 Fe0J C65 156.3(16) . . ?
C45 Fe0J C85 126.1(18) . . ?
C45 Fe0J C4EA 41.9(15) . . ?
C65 Fe0J C4EA 117.0(15) . . ?
C71 Fe0J C23 115.1(17) . . ?
C71 Fe0J C41 119.4(18) . . ?
C71 Fe0J C45 128.7(17) . . ?
C71 Fe0J C65 68.2(16) . . ?
C71 Fe0J C85 65.8(15) . . ?
C71 Fe0J C4EA 164.2(18) . . ?
C85 Fe0J C65 39.3(16) . . ?
C85 Fe0J C4EA 107.9(16) . . ?
C90 Fe0J C23 128.7(17) . . ?
C90 Fe0J C41 156.3(16) . . ?
C90 Fe0J C45 111.7(17) . . ?
C90 Fe0J C65 68.8(17) . . ?
C90 Fe0J C71 40.8(16) . . ?
C90 Fe0J C85 39.7(16) . . ?
C90 Fe0J C6AA 159.5(17) . . ?
C90 Fe0J C4EA 125.0(17) . . ?
C6AA Fe0J C23 65.3(17) . . ?
C6AA Fe0J C41 44.1(17) . . ?
C6AA Fe0J C45 68.8(18) . . ?
C6AA Fe0J C65 102.2(17) . . ?
C6AA Fe0J C71 154.5(19) . . ?
C6AA Fe0J C85 122.3(16) . . ?
C6AA Fe0J C4EA 41.3(18) . . ?
C36 P0K Au07 116.5(14) . . ?
C36 P0K C78 103(3) . . ?
C36 P0K C20 105.2(19) . . ?
C78 P0K Au07 115(2) . . ?
C20 P0K Au07 108.6(18) . . ?
C20 P0K C78 108(3) . . ?
C45 P0L Au06 109.4(15) . . ?
C45 P0L C64 100(2) . . ?
C64 P0L Au06 112.3(14) . . ?
C74 P0L Au06 114.7(15) . . ?
C74 P0L C45 112(2) . . ?
C74 P0L C64 108(2) . . ?
C71 P0M Au02 116.9(13) . . ?
C73 P0M Au02 111.1(18) . . ?
C73 P0M C71 103(2) . . ?
C84 P0M Au02 116.3(15) . . ?
C84 P0M C71 104(2) . . ?
C84 P0M C73 104(2) . . ?
C13 P0N Au05 115.5(14) . . ?
C13 P0N C91 105.4(19) . . ?
C91 P0N Au05 111.3(13) . . ?
C7BA P0N Au05 112.0(13) . . ?
C7BA P0N C13 107.5(19) . . ?
C7BA P0N C91 104.2(19) . . ?
C69 P00O Au04 115.8(18) . . ?
C69 P00O C87 105(2) . . ?
C69 P00O C88 101(2) . . ?
C87 P00O Au04 117.1(15) . . ?
C88 P00O Au04 111.8(14) . . ?
C88 P00O C87 105(2) . . ?
C50 P00P Au03 107.8(18) . . ?
C57 P00P Au03 114.5(16) . . ?
C57 P00P C50 109(2) . . ?
C67 P00P Au03 115.1(14) . . ?
C67 P00P C50 107(2) . . ?
C67 P00P C57 103(2) . . ?
C43 O8 Ag0A 115(3) . . ?
C44 O14 Ag08 125(3) . . ?
Ag0F O15 Ag1 92.6(14) . 1_655 ?
C24 O15 Ag0F 125(4) . . ?
C24 O15 Ag1 104(4) . 1_655 ?
C24 O16 Ag0D 124(4) . . ?
C43 O17 Ag0E 123(3) . . ?
Ag0E O20 Ag1 91.1(9) . . ?
C44 O20 Ag0E 125(3) . . ?
C44 O20 Ag1 130(3) . . ?
C5EA O21 Ag0F 120(3) . . ?
O15 C24 O16 129(6) . . ?
O15 C24 C9AA 117(5) . . ?
O16 C24 C9AA 112(5) . . ?
Ag0C O31 Ag0B 71.4(8) . . ?
C2EA O31 Ag0B 107(3) . . ?
C2EA O31 Ag0C 112(3) . . ?
Fe0H C33 H33 126.7 . . ?
C36 C33 Fe0H 73(3) . . ?
C36 C33 H33 120.5 . . ?
C60 C33 Fe0H 72(2) . . ?
C60 C33 H33 120.5 . . ?
C60 C33 C36 119(4) . . ?
P0K C36 Fe0H 135(2) . . ?
C33 C36 Fe0H 69(3) . . ?
C33 C36 P0K 134(4) . . ?
C33 C36 C38 98(4) . . ?
C38 C36 Fe0H 68(2) . . ?
C38 C36 P0K 126(3) . . ?
C5EA O38 Ag0C 123(3) . . ?
Fe0H C48 H48 126.9 . . ?
C88 C48 Fe0H 69(2) . . ?
C88 C48 H48 125.8 . . ?
C3BA C48 Fe0H 70(2) . . ?
C3BA C48 H48 125.8 . . ?
C3BA C48 C88 108(4) . . ?
C0CA C50 P00P 121(4) . . ?
C0CA C50 C2CA 120(5) . . ?
C2CA C50 P00P 118(4) . . ?
O15 Ag1 O20 127.1(11) 1_455 . ?
O1AA Ag1 O15 72.9(18) 1_455 1_455 ?
O1AA Ag1 O20 159.9(17) 1_455 . ?
O14 C44 C77 117(4) . . ?
O20 C44 O14 122(4) . . ?
O20 C44 C77 121(4) . . ?
Fe0H C38 H38 127.3 . . ?
C36 C38 Fe0H 69(2) . . ?
C36 C38 H38 125.7 . . ?
C92 C38 Fe0H 69(2) . . ?
C92 C38 C36 109(4) . . ?
C92 C38 H38 125.7 . . ?
C70 O40 Ag0B 104(4) . . ?
O8 C43 C4DA 108(5) . . ?
O17 C43 O8 132(5) . . ?
O17 C43 C4DA 120(5) . . ?
C46 C13 P0N 121(3) . . ?
C46 C13 C53 122(4) . . ?
C53 C13 P0N 117(3) . . ?
Fe0J C16 H16 124.9 . . ?
C65 C16 Fe0J 74(2) . . ?
C65 C16 H16 124.9 . . ?
C71 C16 Fe0J 71(2) . . ?
C71 C16 H16 124.9 . . ?
C71 C16 C65 110(4) . . ?
C32 C18 H18 119.7 . . ?
C91 C18 H18 119.7 . . ?
C91 C18 C32 121(4) . . ?
Fe0I C19 H19 125.2 . . ?
C0AA C19 Fe0I 71(2) . . ?
C0AA C19 H19 124.9 . . ?
C7BA C19 Fe0I 70(3) . . ?
C7BA C19 H19 124.9 . . ?
C7BA C19 C0AA 110(4) . . ?
Fe0J C23 H23 129.8 . . ?
C41 C23 Fe0J 71(3) . . ?
C41 C23 H23 119.9 . . ?
C41 C23 C45 120(4) . . ?
C45 C23 Fe0J 71(3) . . ?
C45 C23 H23 119.9 . . ?
C32 C30 H30 119.7 . . ?
C98 C30 H30 119.7 . . ?
C98 C30 C32 121(4) . . ?
C18 C32 C30 117(4) . . ?
C18 C32 H32 121.5 . . ?
C30 C32 H32 121.5 . . ?
C81 O0AA Ag0E 119(3) . . ?
C74 C40 H40 117.0 . . ?
C9BA C40 H40 117.0 . . ?
C9BA C40 C74 126(4) . . ?
Fe0J C41 H41 124.2 . . ?
C23 C41 Fe0J 71(3) . . ?
C23 C41 H41 129.6 . . ?
C23 C41 C6AA 101(4) . . ?
C6AA C41 Fe0J 67(2) . . ?
C6AA C41 H41 129.6 . . ?
C62 C42 H42 119.8 . . ?
C62 C42 C96 120(4) . . ?
C96 C42 H42 119.8 . . ?
P0L C45 Fe0J 137(2) . . ?
C23 C45 Fe0J 70(3) . . ?
C23 C45 P0L 131(3) . . ?
C23 C45 C4EA 108(4) . . ?
C4EA C45 Fe0J 74(2) . . ?
C4EA C45 P0L 118(4) . . ?
C13 C46 H46 121.4 . . ?
C13 C46 C1EA 117(4) . . ?
C1EA C46 H46 121.4 . . ?
Fe0I C0AA H0AA 125.2 . . ?
C19 C0AA Fe0I 66(2) . . ?
C19 C0AA H0AA 125.9 . . ?
C6BA C0AA Fe0I 74(3) . . ?
C6BA C0AA C19 108(4) . . ?
C6BA C0AA H0AA 125.9 . . ?
C81 O52 Ag09 123(3) . . ?
Fe0I C56 H56 125.1 . . ?
C6BA C56 Fe0I 72(2) . . ?
C6BA C56 H56 126.3 . . ?
C7BA C56 Fe0I 68(2) . . ?
C7BA C56 H56 126.3 . . ?
C7BA C56 C6BA 107(4) . . ?
C66 C57 P00P 121(3) . . ?
C66 C57 C8BA 116(4) . . ?
C8BA C57 P00P 123(3) . . ?
Fe0H C60 H60 124.3 . . ?
C33 C60 Fe0H 70(2) . . ?
C33 C60 H60 127.5 . . ?
C33 C60 C92 105(4) . . ?
C92 C60 Fe0H 70(2) . . ?
C92 C60 H60 127.5 . . ?
C42 C62 H62 115.7 . . ?
C42 C62 C64 129(5) . . ?
C64 C62 H62 115.7 . . ?
Fe0I C63 H63 126.2 . . ?
C61 C63 Fe0I 69(2) . . ?
C61 C63 H63 129.4 . . ?
C61 C63 C67 101(3) . . ?
C67 C63 Fe0I 67(2) . . ?
C67 C63 H63 129.4 . . ?
C62 C64 P0L 127(4) . . ?
C8AA C64 P0L 118(3) . . ?
C8AA C64 C62 115(4) . . ?
Fe0J C65 H65 129.1 . . ?
C16 C65 Fe0J 64(2) . . ?
C16 C65 H65 129.2 . . ?
C85 C65 Fe0J 69(2) . . ?
C85 C65 C16 102(4) . . ?
C85 C65 H65 129.2 . . ?
C99 C69 P00O 122(4) . . ?
C99 C69 C95 115(4) . . ?
C95 C69 P00O 123(4) . . ?
O40 C70 O9 126(5) . . ?
O40 C70 C7EA 114(6) . . ?
O9 C70 C7EA 120(6) . . ?
P0M C71 Fe0J 129(2) . . ?
C16 C71 Fe0J 69(2) . . ?
C16 C71 P0M 128(3) . . ?
C16 C71 C90 109(4) . . ?
C90 C71 Fe0J 69(2) . . ?
C90 C71 P0M 122(3) . . ?
C91 C72 H72 122.6 . . ?
C98 C72 H72 122.6 . . ?
C98 C72 C91 115(4) . . ?
C40 C74 P0L 125(3) . . ?
C40 C74 C52 110(4) . . ?
C52 C74 P0L 126(4) . . ?
Fe0H C76 H76 127.7 . . ?
C4BA C76 Fe0H 67(2) . . ?
C4BA C76 H76 128.2 . . ?
C4BA C76 C3BA 104(4) . . ?
C3BA C76 Fe0H 68(2) . . ?
C3BA C76 H76 128.2 . . ?
F25 C77 C44 112(4) . . ?
F25 C77 F34 102(3) . . ?
F34 C77 C44 112(4) . . ?
F53 C77 C44 114(4) . . ?
F53 C77 F25 108(4) . . ?
F53 C77 F34 108(4) . . ?
C7CA C78 P0K 117(5) . . ?
C7CA C78 C6CA 126(6) . . ?
C6CA C78 P0K 116(5) . . ?
Fe0J C85 H85 129.6 . . ?
C65 C85 Fe0J 72(2) . . ?
C65 C85 H85 123.8 . . ?
C90 C85 Fe0J 67(2) . . ?
C90 C85 C65 112(4) . . ?
C90 C85 H85 123.8 . . ?
Fe0I C86 H86 125.7 . . ?
C5BA C86 Fe0I 72(2) . . ?
C5BA C86 H86 123.0 . . ?
C61 C86 Fe0I 71(3) . . ?
C61 C86 H86 123.0 . . ?
C61 C86 C5BA 114(4) . . ?
C2AA C87 P00O 121(4) . . ?
C3AA C87 P00O 119(4) . . ?
C3AA C87 C2AA 120(5) . . ?
P00O C88 Fe0H 139(2) . . ?
C48 C88 Fe0H 70(2) . . ?
C48 C88 P00O 125(3) . . ?
C4BA C88 Fe0H 69(2) . . ?
C4BA C88 P00O 126(3) . . ?
C4BA C88 C48 107(4) . . ?
Fe0J C90 H90 121.1 . . ?
C71 C90 Fe0J 70(2) . . ?
C71 C90 H90 127.0 . . ?
C85 C90 Fe0J 74(3) . . ?
C85 C90 C71 106(4) . . ?
C85 C90 H90 127.0 . . ?
C18 C91 P0N 120(4) . . ?
C18 C91 C72 122(4) . . ?
C72 C91 P0N 117(4) . . ?
Fe0H C92 H92 124.2 . . ?
C38 C92 Fe0H 71(2) . . ?
C38 C92 C60 109(4) . . ?
C38 C92 H92 125.5 . . ?
C60 C92 Fe0H 71(2) . . ?
C60 C92 H92 125.5 . . ?
C30 C98 C72 124(5) . . ?
C30 C98 H98 117.8 . . ?
C72 C98 H98 117.8 . . ?
C69 C99 H99 117.3 . . ?
C69 C99 C51 125(5) . . ?
C51 C99 H99 117.3 . . ?
C66 C29 H29 122.8 . . ?
C66 C29 C0EA 114(4) . . ?
C0EA C29 H29 122.8 . . ?
C2AA C4AA H4AA 114.6 . . ?
C2AA C4AA C54 131(6) . . ?
C54 C4AA H4AA 114.6 . . ?
F3 C5AA F20 104(4) . . ?
F3 C5AA C81 117(5) . . ?
F3 C5AA F1AA 109(4) . . ?
F20 C5AA C81 111(4) . . ?
F1AA C5AA F20 103(4) . . ?
F1AA C5AA C81 111(4) . . ?
C47 C1AA H1AA 117.9 . . ?
C53 C1AA H1AA 117.9 . . ?
C53 C1AA C47 124(4) . . ?
C84 C39 H39 124.1 . . ?
C84 C39 C3CA 112(4) . . ?
C3CA C39 H39 124.1 . . ?
C0CA C1CA H1CA 118.8 . . ?
C0CA C1CA C8DA 122(5) . . ?
C8DA C1CA H1CA 118.8 . . ?
C84 C1BA H1BA 116.3 . . ?
C5CA C1BA H1BA 116.3 . . ?
C5CA C1BA C84 127(5) . . ?
C64 C8AA H8AA 120.2 . . ?
C64 C8AA C7AA 120(4) . . ?
C7AA C8AA H8AA 120.2 . . ?
C87 C2AA H2AA 124.1 . . ?
C4AA C2AA C87 112(5) . . ?
C4AA C2AA H2AA 124.1 . . ?
C1AA C47 H47 122.2 . . ?
C1EA C47 C1AA 116(4) . . ?
C1EA C47 H47 122.2 . . ?
Fe0I C5BA H5BA 131.0 . . ?
C86 C5BA Fe0I 68(2) . . ?
C86 C5BA H5BA 128.7 . . ?
C86 C5BA C67 103(4) . . ?
C67 C5BA Fe0I 64(2) . . ?
C67 C5BA H5BA 128.7 . . ?
C99 C51 H51 120.0 . . ?
C99 C51 C49 120(5) . . ?
C49 C51 H51 120.0 . . ?
C74 C52 H52 118.3 . . ?
C7DA C52 C74 123(5) . . ?
C7DA C52 H52 118.3 . . ?
C13 C53 H53 121.7 . . ?
C1AA C53 C13 117(4) . . ?
C1AA C53 H53 121.7 . . ?
C4AA C54 H54 122.2 . . ?
C4AA C54 C75 116(5) . . ?
C75 C54 H54 122.2 . . ?
Fe0H C4BA H4BA 124.3 . . ?
C76 C4BA Fe0H 73(2) . . ?
C76 C4BA H4BA 122.2 . . ?
C88 C4BA Fe0H 72(2) . . ?
C88 C4BA C76 116(4) . . ?
C88 C4BA H4BA 122.2 . . ?
F12 C2BA F19 106(4) . . ?
F12 C2BA C5EA 118(4) . . ?
F19 C2BA C5EA 108(4) . . ?
F24 C2BA F12 103(4) . . ?
F24 C2BA F19 107(4) . . ?
F24 C2BA C5EA 114(4) . . ?
Fe0I C61 H61 128.3 . . ?
C63 C61 Fe0I 68(2) . . ?
C63 C61 H61 122.7 . . ?
C86 C61 Fe0I 73(3) . . ?
C86 C61 C63 115(4) . . ?
C86 C61 H61 122.7 . . ?
Fe0I C6BA H6BA 130.4 . . ?
C0AA C6BA Fe0I 69(2) . . ?
C0AA C6BA C56 105(4) . . ?
C0AA C6BA H6BA 127.6 . . ?
C56 C6BA Fe0I 65(2) . . ?
C56 C6BA H6BA 127.6 . . ?
C87 C3AA H3AA 118.5 . . ?
C75 C3AA C87 123(5) . . ?
C75 C3AA H3AA 118.5 . . ?
C57 C66 H66 118.2 . . ?
C29 C66 C57 124(4) . . ?
C29 C66 H66 118.2 . . ?
P00P C67 Fe0I 130(2) . . ?
C63 C67 Fe0I 69(2) . . ?
C63 C67 P00P 129(3) . . ?
C63 C67 C5BA 107(3) . . ?
C5BA C67 Fe0I 71(2) . . ?
C5BA C67 P00P 123(3) . . ?
F5 C0BA C2EA 109(4) . . ?
F13 C0BA F5 112(5) . . ?
F13 C0BA F35 106(4) . . ?
F13 C0BA C2EA 118(5) . . ?
F35 C0BA F5 103(4) . . ?
F35 C0BA C2EA 108(5) . . ?
Fe0H C3BA H3BA 127.2 . . ?
C48 C3BA Fe0H 69(2) . . ?
C48 C3BA C76 105(3) . . ?
C48 C3BA H3BA 127.4 . . ?
C76 C3BA Fe0H 68(2) . . ?
C76 C3BA H3BA 127.4 . . ?
Fe0J C6AA H6AA 121.2 . . ?
C41 C6AA Fe0J 69(2) . . ?
C41 C6AA H6AA 124.0 . . ?
C4EA C6AA Fe0J 77(3) . . ?
C4EA C6AA C41 112(4) . . ?
C4EA C6AA H6AA 124.0 . . ?
C80 C73 P0M 124(5) . . ?
C1DA C73 P0M 118(5) . . ?
C1DA C73 C80 116(5) . . ?
C50 C0CA H0CA 120.6 . . ?
C1CA C0CA C50 119(5) . . ?
C1CA C0CA H0CA 120.6 . . ?
C8AA C7AA H7AA 122.1 . . ?
C96 C7AA C8AA 116(4) . . ?
C96 C7AA H7AA 122.1 . . ?
C73 C80 H80 119.9 . . ?
C73 C80 C28 120(6) . . ?
C28 C80 H80 119.9 . . ?
O0AA C81 C5AA 112(4) . . ?
O52 C81 O0AA 130(4) . . ?
O52 C81 C5AA 118(5) . . ?
Fe0J C4EA H4EA 134.3 . . ?
C45 C4EA Fe0J 64(2) . . ?
C45 C4EA H4EA 130.8 . . ?
C6AA C4EA Fe0J 62(2) . . ?
C6AA C4EA C45 98(4) . . ?
C6AA C4EA H4EA 130.8 . . ?
C39 C84 P0M 120(4) . . ?
C39 C84 C1BA 119(4) . . ?
C1BA C84 P0M 121(3) . . ?
C57 C8BA H8BA 119.8 . . ?
C9DA C8BA C57 120(5) . . ?
C9DA C8BA H8BA 119.8 . . ?
C50 C2CA H2CA 118.4 . . ?
C6EA C2CA C50 123(5) . . ?
C6EA C2CA H2CA 118.4 . . ?
C40 C9BA H9BA 122.2 . . ?
C40 C9BA C6DA 116(5) . . ?
C6DA C9BA H9BA 122.2 . . ?
P0N C7BA Fe0I 128(2) . . ?
C19 C7BA Fe0I 72(2) . . ?
C19 C7BA P0N 124(3) . . ?
C19 C7BA C56 109(4) . . ?
C56 C7BA Fe0I 72(2) . . ?
C56 C7BA P0N 127(3) . . ?
C69 C95 H95 121.7 . . ?
C5DA C95 C69 117(5) . . ?
C5DA C95 H95 121.7 . . ?
C42 C96 C7AA 119(4) . . ?
C42 C96 H96 120.4 . . ?
C7AA C96 H96 120.4 . . ?
F43 C9AA C24 108(5) . . ?
F46 C9AA C24 115(6) . . ?
F46 C9AA F43 102(6) . . ?
F46 C9AA F87 121(6) . . ?
F87 C9AA C24 108(5) . . ?
F87 C9AA F43 102(5) . . ?
Ag1 O1AA Ag0F 90(3) 1_655 . ?
O12 O1AA Ag0F 107(7) . . ?
O12 O1AA Ag1 117(9) . 1_655 ?
O12 O1AA C2EA 91(9) . . ?
C2EA O1AA Ag0F 118(5) . . ?
C2EA O1AA Ag1 133(4) . 1_655 ?
O1AA O12 Ag0D 123(8) . . ?
O1AA O12 C2EA 56(7) . . ?
C2EA O12 Ag0D 126(4) . . ?
C3DA C2DA H2DA 126.9 . . ?
C3DA C2DA C1DA 106(5) . . ?
C1DA C2DA H2DA 126.9 . . ?
C80 C28 H28 119.7 . . ?
C3DA C28 C80 121(5) . . ?
C3DA C28 H28 119.7 . . ?
C1BA C5CA H5CA 122.9 . . ?
C1BA C5CA C4CA 114(4) . . ?
C4CA C5CA H5CA 122.9 . . ?
C8CA C37 H37 119.5 . . ?
C8CA C37 C3EA 121(5) . . ?
C3EA C37 H37 119.5 . . ?
C5CA C4CA H4CA 119.8 . . ?
C3CA C4CA C5CA 120(5) . . ?
C3CA C4CA H4CA 119.8 . . ?
C39 C3CA H3CA 116.8 . . ?
C4CA C3CA C39 126(5) . . ?
C4CA C3CA H3CA 116.8 . . ?
C52 C7DA H7DA 118.8 . . ?
C52 C7DA C6DA 122(5) . . ?
C6DA C7DA H7DA 118.8 . . ?
C37 C8CA H8CA 121.6 . . ?
C37 C8CA C7CA 117(6) . . ?
C7CA C8CA H8CA 121.6 . . ?
C46 C1EA H1EA 117.9 . . ?
C47 C1EA C46 124(4) . . ?
C47 C1EA H1EA 117.9 . . ?
C51 C49 H49 123.8 . . ?
C51 C49 C5DA 112(4) . . ?
C5DA C49 H49 123.8 . . ?
F15 C4DA C43 110(5) . . ?
F16 C4DA C43 113(5) . . ?
F16 C4DA F15 113(5) . . ?
F16 C4DA F0AA 110(5) . . ?
F0AA C4DA C43 107(5) . . ?
F0AA C4DA F15 102(5) . . ?
C2DA C3DA H3DA 120.3 . . ?
C28 C3DA C2DA 119(5) . . ?
C28 C3DA H3DA 120.3 . . ?
O31 C2EA C0BA 111(5) . . ?
O31 C2EA O12 117(4) . . ?
C0BA C2EA O12 122(5) . . ?
O1AA C2EA O31 132(5) . . ?
O1AA C2EA C0BA 117(5) . . ?
O1AA C2EA O12 33(4) . . ?
C95 C5DA C49 130(5) . . ?
C95 C5DA H5DA 115.0 . . ?
C49 C5DA H5DA 115.0 . . ?
C8BA C9DA H9DA 117.9 . . ?
C8BA C9DA C0EA 124(5) . . ?
C0EA C9DA H9DA 117.9 . . ?
C9BA C6DA C7DA 122(4) . . ?
C9BA C6DA H6DA 119.2 . . ?
C7DA C6DA H6DA 119.2 . . ?
C1CA C8DA H8DA 119.7 . . ?
C1CA C8DA C6EA 121(4) . . ?
C6EA C8DA H8DA 119.7 . . ?
C78 C7CA C8CA 119(6) . . ?
C78 C7CA H7CA 120.3 . . ?
C8CA C7CA H7CA 120.3 . . ?
C54 C75 H75 120.7 . . ?
C3AA C75 C54 119(5) . . ?
C3AA C75 H75 120.7 . . ?
C78 C6CA H6CA 123.9 . . ?
C78 C6CA C3EA 112(6) . . ?
C3EA C6CA H6CA 123.9 . . ?
C29 C0EA C9DA 120(4) . . ?
C29 C0EA H0EA 120.0 . . ?
C9DA C0EA H0EA 120.0 . . ?
C73 C1DA C2DA 136(6) . . ?
C73 C1DA H1DA 111.8 . . ?
C2DA C1DA H1DA 111.8 . . ?
O21 C5EA C2BA 116(4) . . ?
O38 C5EA O21 119(4) . . ?
O38 C5EA C2BA 124(4) . . ?
F36 C7EA C70 121(6) . . ?
F36 C7EA F83 99(5) . . ?
F36 C7EA F94 112(5) . . ?
F83 C7EA C70 107(5) . . ?
F94 C7EA C70 112(6) . . ?
F94 C7EA F83 103(5) . . ?
C2CA C6EA C8DA 114(5) . . ?
C2CA C6EA H6EA 123.2 . . ?
C8DA C6EA H6EA 123.2 . . ?
C37 C3EA C6CA 120(6) . . ?
C37 C3EA H3EA 120.0 . . ?
C6CA C3EA H3EA 120.0 . . ?
F32 B49 F55 109.8(17) . . ?
F32 B49 F200 108.3(17) . . ?
F32 B49 F58 109.9(18) . . ?
F55 B49 F200 110.0(17) . . ?
F58 B49 F55 109.4(17) . . ?
F58 B49 F200 109.5(17) . . ?
C31 C34 H34 120.0 . . ?
C31 C34 C9CA 120.0 . . ?
C9CA C34 H34 120.0 . . ?
C34 C31 H31 120.0 . . ?
C34 C31 C20 120.0 . . ?
C20 C31 H31 120.0 . . ?
C31 C20 P0K 118(2) . . ?
C31 C20 C0DA 120.0 . . ?
C0DA C20 P0K 122(2) . . ?
C20 C0DA H0DA 120.0 . . ?
C20 C0DA C8EA 120.0 . . ?
C8EA C0DA H0DA 120.0 . . ?
C0DA C8EA H8EA 120.0 . . ?
C9CA C8EA C0DA 120.0 . . ?
C9CA C8EA H8EA 120.0 . . ?
C34 C9CA H9CA 120.0 . . ?
C8EA C9CA C34 120.0 . . ?
C8EA C9CA H9CA 120.0 . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
- Detector area scaling
;
# SQUEEZE RESULTS (Version =  30118)
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.013 0.000 0.000 779 603 ' '
2 -0.002 1.000 0.500 487 397 ' '
3 0.000 0.500 0.500 38 11 ' '
_platon_squeeze_void_probe_radius 1.20
_platon_squeeze_details          ?
