# Electronic Supplementary Material (ESI) for Nanoscale.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_11_a
_database_code_depnum_ccdc_archive 'CCDC 1909219'
loop_
_audit_author_name
_audit_author_address
'Guangxiong Duan'
;Huazhong University of Science and Technology
China
;
_audit_update_record             
;
2019-04-10 deposited with the CCDC.	2019-12-13 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2016/6
_shelx_SHELXL_version_number     2016/6
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C173 H189 Ag28 Mo4 O21 P12'
_chemical_formula_weight         6379.99

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 2/c'
_space_group_name_Hall           '-C 2yc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   57.470(5)
_cell_length_b                   33.556(3)
_cell_length_c                   39.361(7)
_cell_angle_alpha                90
_cell_angle_beta                 122.9670(10)
_cell_angle_gamma                90
_cell_volume                     63684(14)
_cell_formula_units_Z            8
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9624
_cell_measurement_theta_min      2.85
_cell_measurement_theta_max      24.62

_exptl_crystal_description       block
_exptl_crystal_colour            black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_density_diffrn    1.331
_exptl_crystal_F_000             24472
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.32
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.16
_exptl_absorpt_coefficient_mu    1.922
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.581
_exptl_absorpt_correction_T_max  0.735
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-III CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            180080
_diffrn_reflns_av_unetI/netI     0.1026
_diffrn_reflns_av_R_equivalents  0.0734
_diffrn_reflns_limit_h_min       -67
_diffrn_reflns_limit_h_max       67
_diffrn_reflns_limit_k_min       -39
_diffrn_reflns_limit_k_max       39
_diffrn_reflns_limit_l_min       -45
_diffrn_reflns_limit_l_max       46
_diffrn_reflns_theta_min         2.829
_diffrn_reflns_theta_max         24.786
_diffrn_reflns_theta_full        24.786
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measured_fraction_theta_full 0.983
_diffrn_reflns_Laue_measured_fraction_max 0.983
_diffrn_reflns_Laue_measured_fraction_full 0.983
_diffrn_reflns_point_group_measured_fraction_max 0.983
_diffrn_reflns_point_group_measured_fraction_full 0.983
_reflns_number_total             53842
_reflns_number_gt                27271
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX3'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1883P)²+2657.4924P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         53842
_refine_ls_number_parameters     2131
_refine_ls_number_restraints     2010
_refine_ls_R_factor_all          0.1798
_refine_ls_R_factor_gt           0.1177
_refine_ls_wR_factor_ref         0.3572
_refine_ls_wR_factor_gt          0.3143
_refine_ls_goodness_of_fit_ref   1.007
_refine_ls_restrained_S_all      0.994
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.33712(3) 0.45211(4) 0.48549(4) 0.0447(3) Uani 1 1 d . . . . .
C13 C 0.1512(4) 0.5217(6) 0.2120(7) 0.106(6) Uani 1 1 d G U . . .
C1 C 0.1571(3) 0.4825(6) 0.2254(6) 0.098(6) Uani 1 1 d G U . . .
H1 H 0.175600 0.472944 0.239314 0.118 Uiso 1 1 calc R U . . .
C4 C 0.1358(5) 0.4572(5) 0.2186(6) 0.109(6) Uani 1 1 d G U . . .
H4 H 0.139742 0.430359 0.227764 0.131 Uiso 1 1 calc R U . . .
C54 C 0.1086(4) 0.4711(6) 0.1983(7) 0.120(6) Uani 1 1 d G U . . .
H54 H 0.094070 0.453811 0.193577 0.144 Uiso 1 1 calc R U . . .
C21 C 0.1028(4) 0.5103(7) 0.1848(7) 0.131(6) Uani 1 1 d G U . . .
H21 H 0.084255 0.519849 0.170941 0.157 Uiso 1 1 calc R U . . .
C53 C 0.1241(5) 0.5356(5) 0.1917(7) 0.123(6) Uani 1 1 d G U . . .
H53 H 0.120112 0.562434 0.182491 0.148 Uiso 1 1 calc R U . . .
Ag2 Ag 0.34579(3) 0.53860(4) 0.48441(4) 0.0456(3) Uani 1 1 d . . . . .
Ag3 Ag 0.29711(3) 0.50877(4) 0.48342(4) 0.0459(4) Uani 1 1 d . . . . .
Ag4 Ag 0.30943(4) 0.60132(4) 0.47358(5) 0.0540(4) Uani 1 1 d . . . . .
Ag5 Ag 0.25497(3) 0.57211(4) 0.44089(5) 0.0511(4) Uani 1 1 d . . . . .
Ag6 Ag 0.26656(4) 0.61886(4) 0.39251(5) 0.0525(4) Uani 1 1 d . . . . .
Ag7 Ag 0.23438(3) 0.54666(4) 0.35063(5) 0.0485(4) Uani 1 1 d . . . . .
Ag8 Ag 0.36851(3) 0.47755(4) 0.39679(5) 0.0508(4) Uani 1 1 d . . . . .
Ag9 Ag 0.27356(3) 0.57802(4) 0.33554(5) 0.0453(4) Uani 1 1 d . . . . .
Ag10 Ag 0.32639(3) 0.58706(4) 0.41565(4) 0.0461(4) Uani 1 1 d . . . . .
Ag11 Ag 0.37689(3) 0.54631(4) 0.44415(5) 0.0517(4) Uani 1 1 d . . . . .
Ag12 Ag 0.32457(3) 0.53786(4) 0.35186(5) 0.0460(4) Uani 1 1 d . . . . .
Ag13 Ag 0.27623(3) 0.51763(4) 0.27648(5) 0.0511(4) Uani 1 1 d . . . . .
Ag14 Ag 0.22716(3) 0.52409(4) 0.27632(5) 0.0528(4) Uani 1 1 d . . . . .
Ag15 Ag 0.38197(3) 0.46915(4) 0.47749(5) 0.0500(4) Uani 1 1 d . . . . .
Ag16 Ag 0.30383(3) 0.38032(4) 0.44438(5) 0.0491(4) Uani 1 1 d . . . . .
Ag17 Ag 0.33550(3) 0.41849(4) 0.41828(5) 0.0462(4) Uani 1 1 d . . . . .
Ag18 Ag 0.24669(3) 0.39934(4) 0.39393(5) 0.0503(4) Uani 1 1 d . . . . .
Ag19 Ag 0.31304(3) 0.45581(4) 0.33747(5) 0.0468(4) Uani 1 1 d . . . . .
Ag20 Ag 0.24990(3) 0.44826(4) 0.27803(5) 0.0508(4) Uani 1 1 d . . . . .
Ag21 Ag 0.23200(3) 0.45985(4) 0.33580(5) 0.0467(4) Uani 1 1 d . . . . .
Ag22 Ag 0.27644(3) 0.40949(4) 0.35386(5) 0.0458(4) Uani 1 1 d . . . . .
Ag23 Ag 0.28687(3) 0.45685(4) 0.41566(4) 0.0383(3) Uani 1 1 d . . . . .
Ag24 Ag 0.27597(3) 0.49801(4) 0.34464(4) 0.0386(3) Uani 1 1 d . . . . .
Ag25 Ag 0.28727(3) 0.54213(4) 0.41448(4) 0.0381(3) Uani 1 1 d . . . . .
Ag26 Ag 0.33068(3) 0.49807(4) 0.41606(4) 0.0379(3) Uani 1 1 d . . . . .
Ag27 Ag 0.27809(3) 0.42897(4) 0.47409(5) 0.0509(4) Uani 1 1 d . . . . .
Ag28 Ag 0.24408(3) 0.49128(4) 0.41473(5) 0.0465(4) Uani 1 1 d . . . . .
Mo1 Mo 0.32220(4) 0.63602(5) 0.33964(6) 0.0522(5) Uani 1 1 d . . . . .
Mo2 Mo 0.17930(4) 0.49854(6) 0.33724(6) 0.0586(5) Uani 1 1 d . . . . .
Mo3 Mo 0.35796(4) 0.50102(5) 0.57041(5) 0.0541(5) Uani 1 1 d . . . . .
Mo4 Mo 0.32035(4) 0.35657(5) 0.34345(6) 0.0556(5) Uani 1 1 d . . . . .
P1 P 0.23142(13) 0.39356(16) 0.22931(17) 0.0572(14) Uani 1 1 d . . . . .
P2 P 0.24759(13) 0.68470(14) 0.36309(17) 0.0549(14) Uani 1 1 d . . . . .
P3 P 0.33679(12) 0.64465(16) 0.53267(17) 0.0528(13) Uani 1 1 d . . . . .
P4 P 0.41113(12) 0.59931(15) 0.46567(19) 0.0547(14) Uani 1 1 d . . . . .
P5 P 0.20657(11) 0.35477(16) 0.36356(18) 0.0542(13) Uani 1 1 d . . . . .
P7 P 0.42388(12) 0.44247(16) 0.53752(17) 0.0523(13) Uani 1 1 d . . . . .
P8 P 0.32885(13) 0.31724(16) 0.4714(2) 0.0604(15) Uani 1 1 d . . . . .
P9 P 0.28211(13) 0.53567(17) 0.22134(18) 0.0579(14) Uani 1 1 d . . . . .
P10 P 0.39301(12) 0.45543(16) 0.36537(17) 0.0535(13) Uani 1 1 d . . . . .
P11 P 0.27425(13) 0.41542(15) 0.53209(17) 0.0546(14) Uani 1 1 d . . . . .
P12 P 0.22293(13) 0.58617(16) 0.46241(19) 0.0581(15) Uani 1 1 d . . . . .
P6 P 0.18152(13) 0.55237(18) 0.2271(2) 0.0664(16) Uani 1 1 d . . . . .
O1 O 0.2897(6) 0.2521(6) 0.2857(9) 0.174(13) Uani 1 1 d . . . . .
O2 O 0.3399(3) 0.6367(3) 0.3937(4) 0.047(3) Uani 1 1 d . . . . .
O3 O 0.2364(7) 0.2497(8) 0.2548(9) 0.169(12) Uani 1 1 d . . . . .
O4 O 0.1882(3) 0.4553(4) 0.3184(4) 0.052(3) Uani 1 1 d . . . . .
O5 O 0.3217(3) 0.5026(4) 0.5504(3) 0.047(3) Uani 1 1 d . . . . .
O6 O 0.1996(3) 0.4952(4) 0.3913(4) 0.051(3) Uani 1 1 d . . . . .
O7 O 0.1890(3) 0.5422(4) 0.3236(4) 0.056(3) Uani 1 1 d . . . . .
O8 O 0.1434(3) 0.4978(4) 0.3185(5) 0.073(5) Uani 1 1 d . . . . .
O9 O 0.3433(3) 0.3615(4) 0.3978(5) 0.059(4) Uani 1 1 d . . . . .
O10 O 0.3248(3) 0.3993(4) 0.3211(4) 0.052(3) Uani 1 1 d . . . . .
O11 O 0.2853(3) 0.3557(4) 0.3303(4) 0.053(3) Uani 1 1 d . . . . .
O12 O 0.3270(3) 0.3123(4) 0.3258(5) 0.068(4) Uani 1 1 d . . . . .
O13 O 0.3308(3) 0.5921(4) 0.3240(4) 0.055(3) Uani 1 1 d . . . . .
O14 O 0.2864(3) 0.6358(3) 0.3201(4) 0.044(3) Uani 1 1 d . . . . .
O15 O 0.3312(4) 0.6786(4) 0.3226(5) 0.072(5) Uani 1 1 d . . . . .
O16 O 0.3662(3) 0.5426(4) 0.5513(4) 0.052(3) Uani 1 1 d . . . . .
O17 O 0.3650(2) 0.4567(4) 0.5523(3) 0.051(3) Uani 1 1 d . . . . .
O18 O 0.3778(4) 0.5027(5) 0.6242(4) 0.073(5) Uani 1 1 d . . . . .
O19 O 0.3431(8) 0.4706(15) 0.6612(10) 0.24(2) Uani 1 1 d . . . . .
O20 O 0.4339(9) 0.4420(12) 0.6670(12) 0.237(18) Uani 1 1 d . . . . .
O21 O 0.1139(10) 0.4078(16) 0.2919(17) 0.35(4) Uani 1 1 d . . . . .
C3 C 0.2754(6) 0.7217(7) 0.3783(8) 0.074(5) Uani 1 1 d . U . . .
C6 C 0.3067(8) 0.2194(11) 0.2998(12) 0.142(14) Uani 1 1 d . U . . .
H6A H 0.298201 0.198538 0.307070 0.213 Uiso 1 1 calc R U . . .
H6B H 0.324674 0.226851 0.323760 0.213 Uiso 1 1 calc R U . . .
H6C H 0.309291 0.209450 0.278706 0.213 Uiso 1 1 calc R U . . .
C7 C 0.3285(5) 0.6971(6) 0.5235(7) 0.056(4) Uani 1 1 d . U . . .
C8 C 0.2163(4) 0.3020(6) 0.3774(6) 0.052(4) Uani 1 1 d . U . . .
C9 C 0.2404(5) 0.2936(6) 0.4127(7) 0.059(4) Uani 1 1 d . U . . .
H9 H 0.251978 0.315264 0.428300 0.070 Uiso 1 1 calc R U . . .
C10 C 0.4674(5) 0.3949(7) 0.5493(8) 0.074(4) Uani 1 1 d . U . . .
H10 H 0.466576 0.382843 0.570465 0.088 Uiso 1 1 calc R U . . .
C11 C 0.4807(5) 0.5368(8) 0.5433(8) 0.081(5) Uani 1 1 d . U . . .
H11 H 0.486497 0.509892 0.545227 0.097 Uiso 1 1 calc R U . . .
C12 C 0.3314(5) 0.4898(7) 0.2540(8) 0.080(5) Uani 1 1 d . U . . .
H12A H 0.318267 0.472575 0.256189 0.095 Uiso 1 1 calc R U . . .
H12B H 0.335019 0.477189 0.234611 0.095 Uiso 1 1 calc R U . . .
C15 C 0.1493(7) 0.4204(9) 0.1113(10) 0.106(6) Uani 1 1 d . U . . .
H15 H 0.133615 0.428442 0.085914 0.127 Uiso 1 1 calc R U . . .
C16 C 0.3564(6) 0.5082(8) 0.6722(8) 0.078(7) Uani 1 1 d . U . . .
H16A H 0.366916 0.511876 0.659534 0.117 Uiso 1 1 calc R U . . .
H16B H 0.368992 0.509609 0.701716 0.117 Uiso 1 1 calc R U . . .
H16C H 0.342361 0.529271 0.663012 0.117 Uiso 1 1 calc R U . . .
C17 C 0.4168(8) 0.4585(12) 0.6759(11) 0.129(12) Uani 1 1 d . U . . .
H17A H 0.400430 0.468767 0.651055 0.193 Uiso 1 1 calc R U . . .
H17B H 0.426341 0.480408 0.695032 0.193 Uiso 1 1 calc R U . . .
H17C H 0.411172 0.438408 0.688051 0.193 Uiso 1 1 calc R U . . .
C19 C 0.3020(6) 0.7086(8) 0.3979(8) 0.080(5) Uani 1 1 d . U . . .
H19 H 0.306897 0.681476 0.405058 0.097 Uiso 1 1 calc R U . . .
C20 C 0.1068(7) 0.4388(10) 0.2790(11) 0.112(11) Uani 1 1 d . U . . .
H20A H 0.087487 0.437710 0.255924 0.168 Uiso 1 1 calc R U . . .
H20B H 0.118547 0.449123 0.270081 0.168 Uiso 1 1 calc R U . . .
H20C H 0.108122 0.456385 0.299898 0.168 Uiso 1 1 calc R U . . .
C22 C 0.3210(6) 0.7370(9) 0.4065(9) 0.095(5) Uani 1 1 d . U . . .
H22 H 0.339461 0.728586 0.416417 0.114 Uiso 1 1 calc R U . . .
C23 C 0.3160(7) 0.7758(9) 0.4021(9) 0.097(5) Uani 1 1 d . U . . .
H23 H 0.330682 0.794376 0.411112 0.117 Uiso 1 1 calc R U . . .
C24 C 0.2894(6) 0.7885(9) 0.3845(8) 0.087(5) Uani 1 1 d . U . . .
H24 H 0.285022 0.815811 0.377807 0.104 Uiso 1 1 calc R U . . .
C25 C 0.3778(5) 0.3565(7) 0.5204(7) 0.067(4) Uani 1 1 d . U . . .
H25A H 0.367515 0.381396 0.507422 0.081 Uiso 1 1 calc R U . . .
H25B H 0.375062 0.350011 0.542492 0.081 Uiso 1 1 calc R U . . .
C26 C 0.2974(6) 0.2824(9) 0.3965(9) 0.089(5) Uani 1 1 d . U . . .
H26 H 0.289256 0.307932 0.386664 0.107 Uiso 1 1 calc R U . . .
C27 C 0.3072(5) 0.2903(7) 0.5514(7) 0.066(4) Uani 1 1 d . U . . .
H27 H 0.293454 0.298324 0.556429 0.079 Uiso 1 1 calc R U . . .
C28 C 0.3288(5) 0.2965(6) 0.5145(7) 0.064(4) Uani 1 1 d . U . . .
C29 C 0.3326(5) 0.3652(7) 0.6432(8) 0.071(4) Uani 1 1 d . U . . .
H29 H 0.333927 0.357030 0.667246 0.085 Uiso 1 1 calc R U . . .
C49 C 0.1774(5) 0.5656(6) 0.1788(6) 0.111(6) Uani 1 1 d G U . . .
C50 C 0.1994(4) 0.5859(7) 0.1814(6) 0.113(6) Uani 1 1 d G U . . .
H50 H 0.215721 0.591097 0.207188 0.136 Uiso 1 1 calc R U . . .
C51 C 0.1976(4) 0.5986(6) 0.1464(7) 0.114(6) Uani 1 1 d G U . . .
H51 H 0.212597 0.612473 0.148249 0.137 Uiso 1 1 calc R U . . .
C52 C 0.1737(5) 0.5910(7) 0.1088(6) 0.123(6) Uani 1 1 d G U . . .
H52 H 0.172418 0.599639 0.084829 0.147 Uiso 1 1 calc R U . . .
C2 C 0.1517(4) 0.5706(7) 0.1061(6) 0.127(7) Uani 1 1 d G U . . .
H2 H 0.135361 0.565428 0.080349 0.152 Uiso 1 1 calc R U . . .
C14 C 0.1535(4) 0.5579(6) 0.1411(8) 0.126(6) Uani 1 1 d G U . . .
H14 H 0.138484 0.544052 0.139289 0.151 Uiso 1 1 calc R U . . .
C30 C 0.2471(5) 0.3816(6) 0.5218(7) 0.059(4) Uani 1 1 d . U . . .
C31 C 0.1622(7) 0.4470(9) 0.1408(9) 0.102(6) Uani 1 1 d . U . . .
H31 H 0.153637 0.472015 0.138089 0.122 Uiso 1 1 calc R U . . .
C32 C 0.1991(6) 0.4034(8) 0.1827(9) 0.088(5) Uani 1 1 d . U . . .
C33 C 0.2543(5) 0.3724(7) 0.2143(7) 0.064(4) Uani 1 1 d . U . . .
C34 C 0.2736(5) 0.5868(6) 0.2054(7) 0.058(4) Uani 1 1 d . U . . .
C35 C 0.4160(5) 0.6145(7) 0.4264(8) 0.069(4) Uani 1 1 d . U . . .
C36 C 0.2699(6) 0.7629(7) 0.3767(8) 0.076(5) Uani 1 1 d . U . . .
H36 H 0.252265 0.771970 0.369963 0.092 Uiso 1 1 calc R U . . .
C37 C 0.2891(6) 0.2507(9) 0.3708(9) 0.091(5) Uani 1 1 d . U . . .
H37 H 0.276348 0.255313 0.342650 0.109 Uiso 1 1 calc R U . . .
C38 C 0.4305(6) 0.3310(9) 0.4064(9) 0.096(5) Uani 1 1 d . U . . .
H38 H 0.437764 0.304930 0.415234 0.115 Uiso 1 1 calc R U . . .
C39 C 0.2248(5) 0.7056(6) 0.3755(7) 0.063(4) Uani 1 1 d . U . . .
C40 C 0.2044(5) 0.7338(7) 0.3514(8) 0.074(4) Uani 1 1 d . U . . .
H40 H 0.204396 0.743695 0.328774 0.088 Uiso 1 1 calc R U . . .
C41 C 0.1852(6) 0.7481(7) 0.3567(9) 0.080(5) Uani 1 1 d . U . . .
H41 H 0.169337 0.762012 0.336075 0.096 Uiso 1 1 calc R U . . .
C42 C 0.1899(5) 0.7417(8) 0.3924(8) 0.082(5) Uani 1 1 d . U . . .
H42 H 0.179471 0.756697 0.400128 0.098 Uiso 1 1 calc R U . . .
C43 C 0.2101(5) 0.7127(7) 0.4218(9) 0.082(5) Uani 1 1 d . U . . .
H43 H 0.211898 0.707033 0.446770 0.098 Uiso 1 1 calc R U . . .
C44 C 0.2259(5) 0.6947(7) 0.4102(8) 0.074(5) Uani 1 1 d . U . . .
H44 H 0.238087 0.673968 0.426625 0.089 Uiso 1 1 calc R U . . .
C45 C 0.2282(5) 0.6824(7) 0.3095(7) 0.077(5) Uani 1 1 d . U . . .
H45A H 0.221743 0.709589 0.298744 0.092 Uiso 1 1 calc R U . . .
H45B H 0.240647 0.673554 0.300922 0.092 Uiso 1 1 calc R U . . .
C46 C 0.2034(5) 0.6552(7) 0.2906(8) 0.074(5) Uani 1 1 d . U . . .
H46A H 0.204138 0.640447 0.312923 0.089 Uiso 1 1 calc R U . . .
H46B H 0.186747 0.672363 0.278211 0.089 Uiso 1 1 calc R U . . .
C47 C 0.1990(6) 0.6263(8) 0.2605(8) 0.084(5) Uani 1 1 d . U . . .
H47A H 0.215954 0.609889 0.272009 0.101 Uiso 1 1 calc R U . . .
H47B H 0.196708 0.640859 0.237044 0.101 Uiso 1 1 calc R U . . .
C48 C 0.1753(6) 0.5992(8) 0.2455(9) 0.088(6) Uani 1 1 d . U . . .
H48A H 0.158292 0.612198 0.223202 0.105 Uiso 1 1 calc R U . . .
H48B H 0.172324 0.593283 0.267564 0.105 Uiso 1 1 calc R U . . .
C55 C 0.1900(5) 0.6057(7) 0.4229(7) 0.066(4) Uani 1 1 d . U . . .
C56 C 0.1719(5) 0.6230(7) 0.4306(8) 0.071(4) Uani 1 1 d . U . . .
H56 H 0.176214 0.625229 0.457468 0.085 Uiso 1 1 calc R U . . .
C57 C 0.1454(5) 0.6384(8) 0.3958(8) 0.081(5) Uani 1 1 d . U . . .
H57A H 0.130311 0.624200 0.395751 0.097 Uiso 1 1 calc R U . . .
H57B H 0.144089 0.666784 0.401426 0.097 Uiso 1 1 calc R U . . .
C58 C 0.1397(6) 0.6364(8) 0.3569(8) 0.084(5) Uani 1 1 d . U . . .
H58A H 0.135689 0.663878 0.345965 0.100 Uiso 1 1 calc R U . . .
H58B H 0.122295 0.620979 0.340512 0.100 Uiso 1 1 calc R U . . .
C59 C 0.1593(6) 0.6200(8) 0.3501(9) 0.086(5) Uani 1 1 d . U . . .
H59 H 0.155849 0.619699 0.323609 0.103 Uiso 1 1 calc R U . . .
C60 C 0.1824(5) 0.6052(7) 0.3805(7) 0.073(5) Uani 1 1 d . U . . .
H60 H 0.195067 0.593419 0.375041 0.088 Uiso 1 1 calc R U . . .
C61 C 0.2345(4) 0.6181(6) 0.5040(6) 0.052(4) Uani 1 1 d . U . . .
C62 C 0.2256(5) 0.6161(6) 0.5300(6) 0.061(4) Uani 1 1 d . U . . .
H62 H 0.211575 0.597461 0.524698 0.073 Uiso 1 1 calc R U . . .
C63 C 0.2372(5) 0.6419(7) 0.5659(7) 0.069(4) Uani 1 1 d . U . . .
H63 H 0.231139 0.640456 0.584030 0.083 Uiso 1 1 calc R U . . .
C64 C 0.2564(5) 0.6671(7) 0.5710(7) 0.073(4) Uani 1 1 d . U . . .
H64 H 0.264010 0.684092 0.593952 0.088 Uiso 1 1 calc R U . . .
C65 C 0.2667(5) 0.6714(7) 0.5463(7) 0.071(4) Uani 1 1 d . U . . .
H65 H 0.280265 0.691041 0.551660 0.086 Uiso 1 1 calc R U . . .
C66 C 0.2565(5) 0.6461(6) 0.5139(7) 0.061(4) Uani 1 1 d . U . . .
H66 H 0.264056 0.646975 0.497573 0.074 Uiso 1 1 calc R U . . .
C67 C 0.2154(5) 0.5391(7) 0.4785(8) 0.078(5) Uani 1 1 d . U . . .
H67A H 0.203182 0.544197 0.488591 0.093 Uiso 1 1 calc R U . . .
H67B H 0.205652 0.520568 0.455234 0.093 Uiso 1 1 calc R U . . .
C68 C 0.2419(5) 0.5209(7) 0.5112(8) 0.077(5) Uani 1 1 d . U . . .
H68A H 0.255450 0.521606 0.503067 0.093 Uiso 1 1 calc R U . . .
H68B H 0.249534 0.537005 0.536163 0.093 Uiso 1 1 calc R U . . .
C068 C 0.2232(8) 0.2476(10) 0.2104(11) 0.122(11) Uani 1 1 d . U . . .
H06A H 0.204664 0.235820 0.197933 0.182 Uiso 1 1 calc R U . . .
H06B H 0.234506 0.231028 0.204320 0.182 Uiso 1 1 calc R U . . .
H06C H 0.221596 0.274468 0.199670 0.182 Uiso 1 1 calc R U . . .
C69 C 0.2383(5) 0.4798(7) 0.5197(8) 0.074(5) Uani 1 1 d . U . . .
H69A H 0.229569 0.464155 0.494318 0.089 Uiso 1 1 calc R U . . .
H69B H 0.225702 0.479357 0.529487 0.089 Uiso 1 1 calc R U . . .
C70 C 0.2657(5) 0.4602(6) 0.5512(7) 0.068(5) Uani 1 1 d . U . . .
H70A H 0.264852 0.452405 0.574803 0.081 Uiso 1 1 calc R U . . .
H70B H 0.280797 0.480000 0.560733 0.081 Uiso 1 1 calc R U . . .
C71 C 0.3050(5) 0.3949(6) 0.5738(7) 0.058(4) Uani 1 1 d . U . . .
C72 C 0.3062(5) 0.3786(6) 0.6066(7) 0.062(4) Uani 1 1 d . U . . .
H72 H 0.289464 0.375699 0.605932 0.074 Uiso 1 1 calc R U . . .
C73 C 0.3553(6) 0.3655(7) 0.6396(8) 0.079(5) Uani 1 1 d . U . . .
H73 H 0.372050 0.353030 0.660046 0.095 Uiso 1 1 calc R U . . .
C74 C 0.3544(6) 0.3832(7) 0.6077(8) 0.077(5) Uani 1 1 d . U . . .
H74 H 0.370904 0.385770 0.607732 0.092 Uiso 1 1 calc R U . . .
C75 C 0.3312(5) 0.3963(7) 0.5775(7) 0.067(4) Uani 1 1 d . U . . .
H75 H 0.331473 0.408029 0.555758 0.081 Uiso 1 1 calc R U . . .
C76 C 0.2384(5) 0.3543(6) 0.4935(7) 0.065(4) Uani 1 1 d . U . . .
H76 H 0.246843 0.354111 0.478384 0.078 Uiso 1 1 calc R U . . .
C77 C 0.2185(6) 0.3259(8) 0.4836(8) 0.082(5) Uani 1 1 d . U . . .
H77 H 0.213222 0.306587 0.463059 0.098 Uiso 1 1 calc R U . . .
C78 C 0.2060(5) 0.3281(8) 0.5074(8) 0.078(5) Uani 1 1 d . U . . .
H78 H 0.192591 0.308672 0.503049 0.094 Uiso 1 1 calc R U . . .
C79 C 0.2127(5) 0.3564(7) 0.5350(7) 0.071(4) Uani 1 1 d . U . . .
H79 H 0.203423 0.358569 0.548780 0.085 Uiso 1 1 calc R U . . .
C80 C 0.2330(5) 0.3816(7) 0.5426(7) 0.062(4) Uani 1 1 d . U . . .
H80 H 0.238470 0.400961 0.563284 0.074 Uiso 1 1 calc R U . . .
C81 C 0.3065(5) 0.3051(6) 0.5160(7) 0.062(4) Uani 1 1 d . U . . .
H81 H 0.291234 0.319832 0.495311 0.075 Uiso 1 1 calc R U . . .
C82 C 0.3263(5) 0.2668(7) 0.5753(8) 0.077(5) Uani 1 1 d . U . . .
H82 H 0.324679 0.255574 0.596066 0.093 Uiso 1 1 calc R U . . .
C83 C 0.3487(6) 0.2556(7) 0.5753(8) 0.079(5) Uani 1 1 d . U . . .
H83 H 0.362115 0.237211 0.594008 0.095 Uiso 1 1 calc R U . . .
C84 C 0.3502(5) 0.2753(7) 0.5426(7) 0.073(4) Uani 1 1 d . U . . .
H84 H 0.366372 0.272599 0.541882 0.088 Uiso 1 1 calc R U . . .
C85 C 0.3166(6) 0.2774(8) 0.4349(9) 0.081(5) Uani 1 1 d . U . . .
C86 C 0.3284(6) 0.2382(8) 0.4488(9) 0.084(5) Uani 1 1 d . U . . .
H86 H 0.341996 0.232531 0.476409 0.101 Uiso 1 1 calc R U . . .
C87 C 0.3181(6) 0.2087(8) 0.4181(9) 0.090(5) Uani 1 1 d . U . . .
H87 H 0.327215 0.183643 0.424841 0.108 Uiso 1 1 calc R U . . .
C88 C 0.2979(7) 0.2138(9) 0.3830(10) 0.098(5) Uani 1 1 d . U . . .
H88 H 0.288973 0.191851 0.365310 0.118 Uiso 1 1 calc R U . . .
C89 C 0.3660(4) 0.3246(6) 0.4906(7) 0.060(4) Uani 1 1 d . U . . .
H89A H 0.376334 0.299619 0.503107 0.072 Uiso 1 1 calc R U . . .
H89B H 0.367987 0.331288 0.467773 0.072 Uiso 1 1 calc R U . . .
C90 C 0.4072(5) 0.3638(7) 0.5380(8) 0.072(5) Uani 1 1 d . U . . .
H90A H 0.410419 0.364832 0.515773 0.087 Uiso 1 1 calc R U . . .
H90B H 0.417696 0.340792 0.555367 0.087 Uiso 1 1 calc R U . . .
C91 C 0.4192(5) 0.4022(7) 0.5635(7) 0.068(5) Uani 1 1 d . U . . .
H91A H 0.437286 0.395796 0.588369 0.082 Uiso 1 1 calc R U . . .
H91B H 0.406572 0.411161 0.571797 0.082 Uiso 1 1 calc R U . . .
C92 C 0.4492(4) 0.4243(6) 0.5273(7) 0.057(4) Uani 1 1 d . U . . .
C93 C 0.4881(6) 0.3812(8) 0.5420(8) 0.083(5) Uani 1 1 d . U . . .
H93 H 0.501496 0.361678 0.558557 0.099 Uiso 1 1 calc R U . . .
C94 C 0.4869(5) 0.3987(7) 0.5088(8) 0.078(5) Uani 1 1 d . U . . .
H94 H 0.500026 0.390335 0.502611 0.094 Uiso 1 1 calc R U . . .
C95 C 0.4688(5) 0.4258(7) 0.4858(8) 0.072(4) Uani 1 1 d . U . . .
H95 H 0.468789 0.437184 0.463702 0.086 Uiso 1 1 calc R U . . .
C96 C 0.4477(5) 0.4385(7) 0.4959(7) 0.063(4) Uani 1 1 d . U . . .
H96 H 0.433471 0.456964 0.478935 0.076 Uiso 1 1 calc R U . . .
C97 C 0.4416(5) 0.4789(6) 0.5767(7) 0.058(4) Uani 1 1 d . U . . .
C98 C 0.4675(5) 0.4727(7) 0.6090(7) 0.065(4) Uani 1 1 d . U . . .
H98 H 0.476724 0.448370 0.611186 0.078 Uiso 1 1 calc R U . . .
C99 C 0.4810(5) 0.5016(7) 0.6392(8) 0.073(4) Uani 1 1 d . U . . .
H99 H 0.499482 0.497063 0.661215 0.087 Uiso 1 1 calc R U . . .
C100 C 0.4677(5) 0.5368(8) 0.6374(8) 0.077(5) Uani 1 1 d . U . . .
H100 H 0.476487 0.555374 0.659111 0.093 Uiso 1 1 calc R U . . .
C101 C 0.4408(5) 0.5448(7) 0.6028(7) 0.076(5) Uani 1 1 d . U . . .
H101 H 0.432088 0.569934 0.599068 0.091 Uiso 1 1 calc R U . . .
C102 C 0.4280(5) 0.5149(7) 0.5752(7) 0.066(4) Uani 1 1 d . U . . .
H102 H 0.409096 0.518278 0.554006 0.079 Uiso 1 1 calc R U . . .
C103 C 0.4453(5) 0.5873(7) 0.5072(7) 0.062(4) Uani 1 1 d . U . . .
C104 C 0.4547(5) 0.5482(7) 0.5131(7) 0.065(4) Uani 1 1 d . U . . .
H104 H 0.442271 0.528355 0.495187 0.079 Uiso 1 1 calc R U . . .
C105 C 0.4980(6) 0.5640(8) 0.5700(8) 0.081(5) Uani 1 1 d . U . . .
H105 H 0.516398 0.556304 0.590096 0.098 Uiso 1 1 calc R U . . .
C106 C 0.4902(5) 0.6019(8) 0.5695(8) 0.080(5) Uani 1 1 d . U . . .
H106 H 0.501927 0.620010 0.590492 0.095 Uiso 1 1 calc R U . . .
C107 C 0.4627(5) 0.6140(7) 0.5347(7) 0.071(4) Uani 1 1 d . U . . .
H107 H 0.457334 0.641215 0.531815 0.085 Uiso 1 1 calc R U . . .
C108 C 0.3978(5) 0.6021(8) 0.3862(8) 0.076(4) Uani 1 1 d . U . . .
H108 H 0.383378 0.583763 0.380101 0.091 Uiso 1 1 calc R U . . .
C109 C 0.4003(6) 0.6155(9) 0.3566(9) 0.091(5) Uani 1 1 d . U . . .
H109 H 0.387035 0.607711 0.329467 0.110 Uiso 1 1 calc R U . . .
C110 C 0.4203(6) 0.6389(9) 0.3639(10) 0.094(5) Uani 1 1 d . U . . .
H110 H 0.420862 0.647740 0.341418 0.113 Uiso 1 1 calc R U . . .
C111 C 0.4395(6) 0.6513(8) 0.3993(8) 0.088(5) Uani 1 1 d . U . . .
H11A H 0.440414 0.680622 0.397718 0.105 Uiso 1 1 calc R U . . .
H11B H 0.457296 0.640602 0.404749 0.105 Uiso 1 1 calc R U . . .
C112 C 0.4382(5) 0.6416(8) 0.4368(8) 0.076(4) Uani 1 1 d . U . . .
H11C H 0.455972 0.629719 0.458315 0.091 Uiso 1 1 calc R U . . .
H11D H 0.435361 0.666595 0.447558 0.091 Uiso 1 1 calc R U . . .
C113 C 0.4012(6) 0.6430(8) 0.4799(9) 0.094(6) Uani 1 1 d . U . . .
H11E H 0.415640 0.663785 0.488880 0.113 Uiso 1 1 calc R U . . .
H11F H 0.383559 0.653444 0.456654 0.113 Uiso 1 1 calc R U . . .
C114 C 0.3975(6) 0.6309(8) 0.5167(9) 0.090(5) Uani 1 1 d . U . . .
H11G H 0.389712 0.603684 0.511756 0.108 Uiso 1 1 calc R U . . .
H11H H 0.416076 0.630293 0.542237 0.108 Uiso 1 1 calc R U . . .
C115 C 0.3807(6) 0.6564(8) 0.5215(9) 0.094(5) Uani 1 1 d . U . . .
H11I H 0.362794 0.659068 0.495156 0.112 Uiso 1 1 calc R U . . .
H11J H 0.389482 0.683077 0.528995 0.112 Uiso 1 1 calc R U . . .
C116 C 0.3748(5) 0.6430(8) 0.5539(8) 0.082(6) Uani 1 1 d . U . . .
H11K H 0.384708 0.660834 0.577769 0.098 Uiso 1 1 calc R U . . .
H11L H 0.381803 0.615580 0.562907 0.098 Uiso 1 1 calc R U . . .
C117 C 0.3330(5) 0.6327(6) 0.5729(7) 0.060(4) Uani 1 1 d . U . . .
C118 C 0.3430(5) 0.6565(6) 0.6067(6) 0.059(4) Uani 1 1 d . U . . .
H118 H 0.352101 0.680726 0.608250 0.071 Uiso 1 1 calc R U . . .
C119 C 0.3403(5) 0.6460(7) 0.6392(7) 0.069(4) Uani 1 1 d . U . . .
H11M H 0.329864 0.667451 0.642402 0.083 Uiso 1 1 calc R U . . .
H11N H 0.359133 0.645414 0.664229 0.083 Uiso 1 1 calc R U . . .
C120 C 0.3265(5) 0.6073(7) 0.6360(7) 0.074(4) Uani 1 1 d . U . . .
H12C H 0.339199 0.591416 0.660424 0.088 Uiso 1 1 calc R U . . .
H12D H 0.309753 0.613013 0.636399 0.088 Uiso 1 1 calc R U . . .
C121 C 0.3188(5) 0.5847(7) 0.6034(7) 0.070(4) Uani 1 1 d . U . . .
H121 H 0.311194 0.559137 0.601843 0.084 Uiso 1 1 calc R U . . .
C122 C 0.3213(5) 0.5958(7) 0.5741(7) 0.065(4) Uani 1 1 d . U . . .
H122 H 0.314838 0.578074 0.551898 0.078 Uiso 1 1 calc R U . . .
C123 C 0.2489(5) 0.2567(7) 0.4270(8) 0.070(4) Uani 1 1 d . U . . .
H123 H 0.265582 0.251301 0.452226 0.084 Uiso 1 1 calc R U . . .
C124 C 0.2301(5) 0.2253(7) 0.4001(8) 0.073(4) Uani 1 1 d . U . . .
H124 H 0.234769 0.198691 0.409754 0.087 Uiso 1 1 calc R U . . .
C125 C 0.2079(5) 0.2301(7) 0.3649(8) 0.070(4) Uani 1 1 d . U . . .
H125 H 0.197616 0.208310 0.347837 0.084 Uiso 1 1 calc R U . . .
C126 C 0.1998(5) 0.2709(6) 0.3530(7) 0.068(4) Uani 1 1 d . U . . .
H126 H 0.182896 0.276549 0.328069 0.081 Uiso 1 1 calc R U . . .
C127 C 0.1844(5) 0.3669(7) 0.3809(7) 0.071(4) Uani 1 1 d . U . . .
C128 C 0.1627(5) 0.3395(8) 0.3742(8) 0.077(5) Uani 1 1 d . U . . .
H128 H 0.159807 0.315214 0.359948 0.092 Uiso 1 1 calc R U . . .
C129 C 0.1447(6) 0.3498(8) 0.3900(8) 0.087(5) Uani 1 1 d . U . . .
H129 H 0.131403 0.331567 0.388134 0.104 Uiso 1 1 calc R U . . .
C130 C 0.1484(6) 0.3878(8) 0.4076(9) 0.089(5) Uani 1 1 d . U . . .
H130 H 0.137131 0.395814 0.417276 0.107 Uiso 1 1 calc R U . . .
C131 C 0.1691(6) 0.4141(8) 0.4110(8) 0.083(5) Uani 1 1 d . U . . .
H131 H 0.170469 0.440086 0.421482 0.100 Uiso 1 1 calc R U . . .
C132 C 0.1846(5) 0.3533(7) 0.3074(7) 0.072(5) Uani 1 1 d . U . . .
H13A H 0.168403 0.335877 0.298839 0.086 Uiso 1 1 calc R U . . .
H13B H 0.177554 0.380471 0.297093 0.086 Uiso 1 1 calc R U . . .
C133 C 0.1997(6) 0.3385(8) 0.2893(8) 0.078(5) Uani 1 1 d . U . . .
H13C H 0.189822 0.314692 0.272886 0.094 Uiso 1 1 calc R U . . .
H13D H 0.218312 0.329795 0.311538 0.094 Uiso 1 1 calc R U . . .
C134 C 0.2033(5) 0.3669(7) 0.2631(7) 0.073(5) Uani 1 1 d . U . . .
H13E H 0.210832 0.392325 0.277872 0.088 Uiso 1 1 calc R U . . .
H13F H 0.184870 0.372592 0.238420 0.088 Uiso 1 1 calc R U . . .
C135 C 0.2222(5) 0.3517(7) 0.2505(7) 0.067(5) Uani 1 1 d . U . . .
H13G H 0.212789 0.330517 0.229868 0.080 Uiso 1 1 calc R U . . .
H13H H 0.239242 0.340327 0.274177 0.080 Uiso 1 1 calc R U . . .
C136 C 0.1873(7) 0.3744(9) 0.1528(10) 0.106(6) Uani 1 1 d . U . . .
H136 H 0.197006 0.350632 0.154837 0.127 Uiso 1 1 calc R U . . .
C137 C 0.1579(7) 0.3824(10) 0.1165(10) 0.115(6) Uani 1 1 d . U . . .
H137 H 0.146394 0.361773 0.098714 0.138 Uiso 1 1 calc R U . . .
C138 C 0.1885(6) 0.4391(9) 0.1764(9) 0.090(5) Uani 1 1 d . U . . .
H138 H 0.198293 0.459662 0.195584 0.108 Uiso 1 1 calc R U . . .
C139 C 0.2587(6) 0.3919(7) 0.1897(8) 0.078(5) Uani 1 1 d . U . . .
H139 H 0.249396 0.416444 0.178713 0.093 Uiso 1 1 calc R U . . .
C140 C 0.2773(6) 0.3775(8) 0.1785(8) 0.085(5) Uani 1 1 d . U . . .
H140 H 0.280695 0.392456 0.161159 0.102 Uiso 1 1 calc R U . . .
C141 C 0.2895(5) 0.3421(7) 0.1934(8) 0.075(4) Uani 1 1 d . U . . .
H141 H 0.301261 0.331858 0.185563 0.090 Uiso 1 1 calc R U . . .
C142 C 0.2859(5) 0.3204(8) 0.2190(8) 0.074(4) Uani 1 1 d . U . . .
H142 H 0.294878 0.295420 0.228812 0.089 Uiso 1 1 calc R U . . .
C143 C 0.2686(5) 0.3360(7) 0.2306(8) 0.075(4) Uani 1 1 d . U . . .
H143 H 0.266427 0.321856 0.249599 0.090 Uiso 1 1 calc R U . . .
C144 C 0.4215(4) 0.4884(6) 0.3739(7) 0.056(4) Uani 1 1 d . U . . .
C145 C 0.4290(5) 0.4910(7) 0.3480(7) 0.061(4) Uani 1 1 d . U . . .
H145 H 0.419832 0.474808 0.324366 0.073 Uiso 1 1 calc R U . . .
C146 C 0.4497(5) 0.5162(7) 0.3536(7) 0.066(4) Uani 1 1 d . U . . .
H146 H 0.454290 0.518350 0.333885 0.080 Uiso 1 1 calc R U . . .
C147 C 0.4637(5) 0.5386(7) 0.3892(7) 0.068(4) Uani 1 1 d . U . . .
H147 H 0.477833 0.556669 0.393730 0.082 Uiso 1 1 calc R U . . .
C148 C 0.4570(5) 0.5346(7) 0.4185(7) 0.068(4) Uani 1 1 d . U . . .
H148 H 0.466845 0.548799 0.443346 0.082 Uiso 1 1 calc R U . . .
C149 C 0.4350(5) 0.5089(7) 0.4095(7) 0.066(4) Uani 1 1 d . U . . .
H149 H 0.429626 0.505749 0.428232 0.080 Uiso 1 1 calc R U . . .
C150 C 0.4087(5) 0.4062(7) 0.3824(8) 0.071(4) Uani 1 1 d . U . . .
C151 C 0.4273(5) 0.3929(8) 0.3730(8) 0.083(5) Uani 1 1 d . U . . .
H151 H 0.433398 0.409788 0.360016 0.100 Uiso 1 1 calc R U . . .
C152 C 0.4372(6) 0.3520(8) 0.3837(9) 0.092(5) Uani 1 1 d . U . . .
H152 H 0.448171 0.340410 0.374941 0.111 Uiso 1 1 calc R U . . .
C153 C 0.4121(6) 0.3480(8) 0.4176(9) 0.092(5) Uani 1 1 d . U . . .
H153 H 0.408012 0.333995 0.434764 0.110 Uiso 1 1 calc R U . . .
C154 C 0.4017(6) 0.3822(7) 0.4036(8) 0.079(5) Uani 1 1 d . U . . .
H154 H 0.388055 0.391797 0.408161 0.095 Uiso 1 1 calc R U . . .
C155 C 0.3688(5) 0.4532(7) 0.3088(7) 0.067(5) Uani 1 1 d . U . . .
H15A H 0.379055 0.444087 0.296522 0.080 Uiso 1 1 calc R U . . .
H15B H 0.353763 0.433888 0.301421 0.080 Uiso 1 1 calc R U . . .
C156 C 0.3570(5) 0.4925(7) 0.2931(7) 0.067(4) Uani 1 1 d . U . . .
H15C H 0.353557 0.506009 0.312319 0.080 Uiso 1 1 calc R U . . .
H15D H 0.370440 0.508800 0.290768 0.080 Uiso 1 1 calc R U . . .
C157 C 0.3177(5) 0.5318(7) 0.2373(8) 0.075(5) Uani 1 1 d . U . . .
H15E H 0.319202 0.538499 0.214098 0.090 Uiso 1 1 calc R U . . .
H15F H 0.328488 0.551864 0.258702 0.090 Uiso 1 1 calc R U . . .
C158 C 0.2688(5) 0.6005(6) 0.1685(7) 0.060(4) Uani 1 1 d . U . . .
H158 H 0.267717 0.582060 0.149398 0.073 Uiso 1 1 calc R U . . .
C159 C 0.2656(5) 0.6412(6) 0.1595(7) 0.063(4) Uani 1 1 d . U . . .
H159 H 0.263586 0.650727 0.135343 0.076 Uiso 1 1 calc R U . . .
C160 C 0.2653(5) 0.6668(7) 0.1859(7) 0.067(4) Uani 1 1 d . U . . .
H160 H 0.263318 0.694440 0.179686 0.080 Uiso 1 1 calc R U . . .
C161 C 0.2677(5) 0.6553(7) 0.2203(7) 0.068(4) Uani 1 1 d . U . . .
H161 H 0.267257 0.674393 0.237692 0.082 Uiso 1 1 calc R U . . .
C162 C 0.2710(5) 0.6132(6) 0.2305(7) 0.062(4) Uani 1 1 d . U . . .
H162 H 0.271303 0.603928 0.253615 0.074 Uiso 1 1 calc R U . . .
C163 C 0.2739(6) 0.4888(7) 0.1555(8) 0.079(5) Uani 1 1 d . U . . .
H163 H 0.293132 0.491398 0.165934 0.095 Uiso 1 1 calc R U . . .
C164 C 0.2562(6) 0.4662(8) 0.1190(8) 0.080(5) Uani 1 1 d . U . . .
H164 H 0.264615 0.451839 0.107688 0.096 Uiso 1 1 calc R U . . .
C165 C 0.2282(6) 0.4643(8) 0.0998(9) 0.090(5) Uani 1 1 d . U . . .
H165 H 0.216263 0.452042 0.074270 0.108 Uiso 1 1 calc R U . . .
C166 C 0.2193(7) 0.4828(8) 0.1226(9) 0.093(5) Uani 1 1 d . U . . .
H166 H 0.200138 0.480292 0.112312 0.112 Uiso 1 1 calc R U . . .
C167 C 0.2622(6) 0.5075(7) 0.1762(7) 0.072(4) Uani 1 1 d . U . . .
C168 C 0.2344(6) 0.5039(8) 0.1575(8) 0.089(5) Uani 1 1 d . U . . .
H168 H 0.225359 0.516415 0.168843 0.106 Uiso 1 1 calc R U . . .
C169 C 0.3013(5) 0.7065(7) 0.4914(7) 0.065(4) Uani 1 1 d . U . . .
H169 H 0.288140 0.686424 0.475490 0.078 Uiso 1 1 calc R U . . .
C170 C 0.2951(6) 0.7460(7) 0.4845(8) 0.077(5) Uani 1 1 d . U . . .
H170 H 0.277043 0.754252 0.463513 0.092 Uiso 1 1 calc R U . . .
C171 C 0.3165(6) 0.7757(7) 0.5097(8) 0.076(5) Uani 1 1 d . U . . .
H171 H 0.311565 0.803076 0.504790 0.091 Uiso 1 1 calc R U . . .
C172 C 0.3403(6) 0.7670(7) 0.5366(8) 0.076(5) Uani 1 1 d . U . . .
H172 H 0.354253 0.786658 0.550978 0.091 Uiso 1 1 calc R U . . .
C173 C 0.3455(5) 0.7271(6) 0.5446(8) 0.070(4) Uani 1 1 d . U . . .
H173 H 0.363102 0.720129 0.567604 0.084 Uiso 1 1 calc R U . . .
C174 C 0.1864(6) 0.4038(8) 0.4003(8) 0.078(5) Uani 1 1 d . U . . .
H174 H 0.200837 0.421804 0.405779 0.093 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O17 2.218(11) . ?
Ag1 Ag23 2.698(2) . ?
Ag1 Ag15 2.820(2) . ?
Ag1 Ag17 2.830(2) . ?
Ag1 Ag2 2.9488(19) . ?
Ag1 Ag3 2.951(2) . ?
Ag1 Ag16 2.952(2) . ?
Ag1 Ag26 2.9805(19) . ?
Ag1 Ag27 3.264(2) . ?
C13 C1 1.3900 . ?
C13 C53 1.3900 . ?
C13 P6 1.821(17) . ?
C1 C4 1.3900 . ?
C1 H1 0.9500 . ?
C4 C54 1.3900 . ?
C4 H4 0.9500 . ?
C54 C21 1.3900 . ?
C54 H54 0.9500 . ?
C21 C53 1.3900 . ?
C21 H21 0.9500 . ?
C53 H53 0.9500 . ?
Ag2 O16 2.227(13) . ?
Ag2 Ag26 2.7017(19) . ?
Ag2 Ag10 2.816(2) . ?
Ag2 Ag4 2.830(2) . ?
Ag2 Ag3 2.951(2) . ?
Ag2 Ag25 2.971(2) . ?
Ag2 Ag11 2.976(2) . ?
Ag2 Ag15 3.232(2) . ?
Ag3 O5 2.223(11) . ?
Ag3 Ag25 2.6956(19) . ?
Ag3 Ag28 2.824(2) . ?
Ag3 Ag27 2.840(2) . ?
Ag3 Ag5 2.962(2) . ?
Ag3 Ag23 2.9642(19) . ?
Ag3 Ag4 3.255(2) . ?
Ag4 P3 2.453(6) . ?
Ag4 Ag25 2.784(2) . ?
Ag4 Ag5 2.833(2) . ?
Ag4 Ag6 2.836(2) . ?
Ag4 Ag10 2.966(2) . ?
Ag5 P12 2.455(5) . ?
Ag5 Ag25 2.7636(19) . ?
Ag5 Ag6 2.813(2) . ?
Ag5 Ag28 2.847(2) . ?
Ag5 Ag7 3.190(2) . ?
Ag6 P2 2.457(5) . ?
Ag6 Ag25 2.7700(19) . ?
Ag6 Ag9 2.837(2) . ?
Ag6 Ag7 2.948(2) . ?
Ag6 Ag10 3.222(2) . ?
Ag7 O7 2.219(13) . ?
Ag7 Ag25 2.695(2) . ?
Ag7 Ag14 2.825(2) . ?
Ag7 Ag9 2.826(2) . ?
Ag7 Ag28 2.933(2) . ?
Ag7 Ag21 2.960(2) . ?
Ag7 Ag24 3.0084(19) . ?
Ag8 P10 2.441(5) . ?
Ag8 Ag26 2.7517(19) . ?
Ag8 Ag19 2.837(2) . ?
Ag8 Ag11 2.838(2) . ?
Ag8 Ag15 2.845(2) . ?
Ag8 Ag12 2.956(2) . ?
Ag8 Ag17 3.161(2) . ?
Ag9 O14 2.271(11) . ?
Ag9 Ag24 2.7025(18) . ?
Ag9 Ag12 2.962(2) . ?
Ag9 Ag10 2.972(2) . ?
Ag9 Ag14 3.009(2) . ?
Ag9 Ag25 3.0103(19) . ?
Ag9 Ag13 3.150(2) . ?
Ag10 O2 2.205(11) . ?
Ag10 Ag25 2.6865(19) . ?
Ag10 Ag11 2.830(2) . ?
Ag10 Ag12 2.959(2) . ?
Ag10 Ag26 2.9957(18) . ?
Ag11 P4 2.437(5) . ?
Ag11 Ag26 2.775(2) . ?
Ag11 Ag15 2.845(2) . ?
Ag11 Ag12 3.230(2) . ?
Ag12 O13 2.251(12) . ?
Ag12 Ag26 2.7066(19) . ?
Ag12 Ag19 2.8162(19) . ?
Ag12 Ag13 2.830(2) . ?
Ag12 Ag24 2.9673(19) . ?
Ag13 P9 2.447(5) . ?
Ag13 Ag24 2.7701(19) . ?
Ag13 Ag20 2.795(2) . ?
Ag13 Ag14 2.825(2) . ?
Ag13 Ag19 3.003(2) . ?
Ag14 P6 2.450(6) . ?
Ag14 Ag24 2.767(2) . ?
Ag14 Ag20 2.844(2) . ?
Ag14 Ag21 3.081(2) . ?
Ag15 P7 2.448(6) . ?
Ag15 Ag26 2.778(2) . ?
Ag15 Ag17 2.946(2) . ?
Ag16 P8 2.452(6) . ?
Ag16 Ag23 2.7611(18) . ?
Ag16 Ag18 2.835(2) . ?
Ag16 Ag17 2.837(2) . ?
Ag16 Ag27 2.847(2) . ?
Ag16 Ag22 3.167(2) . ?
Ag17 O9 2.213(11) . ?
Ag17 Ag26 2.6811(18) . ?
Ag17 Ag22 2.945(2) . ?
Ag17 Ag19 2.980(2) . ?
Ag17 Ag23 3.0273(19) . ?
Ag18 P5 2.446(5) . ?
Ag18 Ag23 2.7638(19) . ?
Ag18 Ag21 2.823(2) . ?
Ag18 Ag27 2.829(2) . ?
Ag18 Ag22 2.909(2) . ?
Ag18 Ag28 3.217(2) . ?
Ag19 O10 2.221(11) . ?
Ag19 Ag24 2.6977(19) . ?
Ag19 Ag22 2.9552(19) . ?
Ag19 Ag26 3.0322(19) . ?
Ag19 Ag20 3.077(2) . ?
Ag20 P1 2.441(6) . ?
Ag20 Ag24 2.762(2) . ?
Ag20 Ag22 2.824(2) . ?
Ag20 Ag21 2.988(2) . ?
Ag21 O4 2.228(13) . ?
Ag21 Ag24 2.6815(19) . ?
Ag21 Ag22 2.812(2) . ?
Ag21 Ag28 2.983(2) . ?
Ag21 Ag23 3.008(2) . ?
Ag22 O11 2.212(11) . ?
Ag22 Ag23 2.6863(19) . ?
Ag22 Ag24 2.9907(18) . ?
Ag22 Mo4 3.289(2) . ?
Ag23 Ag28 2.6997(19) . ?
Ag23 Ag27 2.7716(19) . ?
Ag23 Ag25 2.8625(17) . ?
Ag23 Ag26 2.8651(18) . ?
Ag23 Ag24 2.8652(18) . ?
Ag24 Ag26 2.858(2) . ?
Ag24 Ag25 2.8686(18) . ?
Ag25 Ag26 2.8716(18) . ?
Ag25 Ag28 3.0167(19) . ?
Ag27 P11 2.453(5) . ?
Ag27 Ag28 2.947(2) . ?
Ag28 O6 2.199(13) . ?
Ag28 Mo2 3.296(3) . ?
Mo1 O14 1.762(13) . ?
Mo1 O13 1.768(13) . ?
Mo1 O15 1.770(12) . ?
Mo1 O2 1.790(13) . ?
Mo2 O7 1.753(13) . ?
Mo2 O8 1.772(13) . ?
Mo2 O6 1.789(14) . ?
Mo2 O4 1.822(14) . ?
Mo3 O16 1.769(13) . ?
Mo3 O18 1.778(13) . ?
Mo3 O5 1.785(14) . ?
Mo3 O17 1.790(14) . ?
Mo4 O12 1.766(12) . ?
Mo4 O10 1.772(13) . ?
Mo4 O11 1.784(13) . ?
Mo4 O9 1.811(15) . ?
P1 C32 1.79(3) . ?
P1 C135 1.85(2) . ?
P1 C33 1.85(2) . ?
P2 C45 1.77(2) . ?
P2 C39 1.77(2) . ?
P2 C3 1.85(3) . ?
P3 C117 1.76(2) . ?
P3 C7 1.81(2) . ?
P3 C116 1.87(3) . ?
P4 C113 1.77(3) . ?
P4 C103 1.79(2) . ?
P4 C35 1.79(2) . ?
P5 C127 1.79(2) . ?
P5 C8 1.85(2) . ?
P5 C132 1.86(2) . ?
P7 C97 1.79(2) . ?
P7 C91 1.80(2) . ?
P7 C92 1.810(19) . ?
P8 C85 1.80(3) . ?
P8 C28 1.84(2) . ?
P8 C89 1.86(2) . ?
P9 C167 1.78(2) . ?
P9 C157 1.79(3) . ?
P9 C34 1.80(2) . ?
P10 C150 1.83(2) . ?
P10 C144 1.85(2) . ?
P10 C155 1.88(2) . ?
P11 C71 1.77(2) . ?
P11 C30 1.79(2) . ?
P11 C70 1.86(2) . ?
P12 C61 1.756(19) . ?
P12 C55 1.80(2) . ?
P12 C67 1.84(2) . ?
P6 C49 1.840(17) . ?
P6 C48 1.85(3) . ?
O1 C6 1.37(4) . ?
O3 C068 1.48(4) . ?
O19 C16 1.42(5) . ?
O20 C17 1.33(4) . ?
O21 C20 1.13(5) . ?
C3 C19 1.36(3) . ?
C3 C36 1.41(3) . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C173 1.33(3) . ?
C7 C169 1.41(3) . ?
C8 C9 1.35(3) . ?
C8 C126 1.39(3) . ?
C9 C123 1.34(3) . ?
C9 H9 0.9500 . ?
C10 C92 1.35(3) . ?
C10 C93 1.44(3) . ?
C10 H10 0.9500 . ?
C11 C105 1.34(3) . ?
C11 C104 1.37(3) . ?
C11 H11 0.9500 . ?
C12 C156 1.44(3) . ?
C12 C157 1.57(3) . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C15 C31 1.33(4) . ?
C15 C137 1.34(4) . ?
C15 H15 0.9500 . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C19 C22 1.35(4) . ?
C19 H19 0.9500 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C22 C23 1.32(4) . ?
C22 H22 0.9500 . ?
C23 C24 1.36(4) . ?
C23 H23 0.9500 . ?
C24 C36 1.31(3) . ?
C24 H24 0.9500 . ?
C25 C90 1.45(3) . ?
C25 C89 1.45(3) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C26 C85 1.31(4) . ?
C26 C37 1.36(4) . ?
C26 H26 0.9500 . ?
C27 C82 1.26(3) . ?
C27 C81 1.46(3) . ?
C27 H27 0.9500 . ?
C28 C84 1.33(3) . ?
C28 C81 1.35(3) . ?
C29 C73 1.39(3) . ?
C29 C72 1.48(3) . ?
C29 H29 0.9500 . ?
C49 C50 1.3900 . ?
C49 C14 1.3900 . ?
C50 C51 1.3900 . ?
C50 H50 0.9500 . ?
C51 C52 1.3900 . ?
C51 H51 0.9500 . ?
C52 C2 1.3900 . ?
C52 H52 0.9500 . ?
C2 C14 1.3900 . ?
C2 H2 0.9500 . ?
C14 H14 0.9500 . ?
C30 C76 1.31(3) . ?
C30 C80 1.43(3) . ?
C31 C138 1.42(4) . ?
C31 H31 0.9500 . ?
C32 C138 1.31(4) . ?
C32 C136 1.39(4) . ?
C33 C139 1.30(3) . ?
C33 C143 1.42(3) . ?
C34 C162 1.40(3) . ?
C34 C158 1.40(3) . ?
C35 C108 1.40(3) . ?
C35 C112 1.43(3) . ?
C36 H36 0.9500 . ?
C37 C88 1.32(4) . ?
C37 H37 0.9500 . ?
C38 C152 1.35(4) . ?
C38 C153 1.47(4) . ?
C38 H38 0.9500 . ?
C39 C44 1.38(3) . ?
C39 C40 1.40(3) . ?
C40 C41 1.32(3) . ?
C40 H40 0.9500 . ?
C41 C42 1.30(3) . ?
C41 H41 0.9500 . ?
C42 C43 1.47(4) . ?
C42 H42 0.9500 . ?
C43 C44 1.36(3) . ?
C43 H43 0.9500 . ?
C44 H44 0.9500 . ?
C45 C46 1.50(3) . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C46 C47 1.44(3) . ?
C46 H46A 0.9900 . ?
C46 H46B 0.9900 . ?
C47 C48 1.47(4) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
C48 H48A 0.9900 . ?
C48 H48B 0.9900 . ?
C55 C56 1.36(3) . ?
C55 C60 1.48(3) . ?
C56 C57 1.48(3) . ?
C56 H56 0.9500 . ?
C57 C58 1.38(3) . ?
C57 H57A 0.9900 . ?
C57 H57B 0.9900 . ?
C58 C59 1.41(3) . ?
C58 H58A 0.9900 . ?
C58 H58B 0.9900 . ?
C59 C60 1.31(3) . ?
C59 H59 0.9500 . ?
C60 H60 0.9500 . ?
C61 C62 1.37(3) . ?
C61 C66 1.45(3) . ?
C62 C63 1.47(3) . ?
C62 H62 0.9500 . ?
C63 C64 1.32(3) . ?
C63 H63 0.9500 . ?
C64 C65 1.40(3) . ?
C64 H64 0.9500 . ?
C65 C66 1.37(3) . ?
C65 H65 0.9500 . ?
C66 H66 0.9500 . ?
C67 C68 1.49(3) . ?
C67 H67A 0.9900 . ?
C67 H67B 0.9900 . ?
C68 C69 1.46(3) . ?
C68 H68A 0.9900 . ?
C68 H68B 0.9900 . ?
C068 H06A 0.9800 . ?
C068 H06B 0.9800 . ?
C068 H06C 0.9800 . ?
C69 C70 1.52(3) . ?
C69 H69A 0.9900 . ?
C69 H69B 0.9900 . ?
C70 H70A 0.9900 . ?
C70 H70B 0.9900 . ?
C71 C72 1.37(3) . ?
C71 C75 1.43(3) . ?
C72 H72 0.9500 . ?
C73 C74 1.36(3) . ?
C73 H73 0.9500 . ?
C74 C75 1.29(3) . ?
C74 H74 0.9500 . ?
C75 H75 0.9500 . ?
C76 C77 1.38(3) . ?
C76 H76 0.9500 . ?
C77 C78 1.46(3) . ?
C77 H77 0.9500 . ?
C78 C79 1.33(3) . ?
C78 H78 0.9500 . ?
C79 C80 1.34(3) . ?
C79 H79 0.9500 . ?
C80 H80 0.9500 . ?
C81 H81 0.9500 . ?
C82 C83 1.34(3) . ?
C82 H82 0.9500 . ?
C83 C84 1.49(3) . ?
C83 H83 0.9500 . ?
C84 H84 0.9500 . ?
C85 C86 1.45(4) . ?
C86 C87 1.42(4) . ?
C86 H86 0.9500 . ?
C87 C88 1.24(4) . ?
C87 H87 0.9500 . ?
C88 H88 0.9500 . ?
C89 H89A 0.9900 . ?
C89 H89B 0.9900 . ?
C90 C91 1.54(3) . ?
C90 H90A 0.9900 . ?
C90 H90B 0.9900 . ?
C91 H91A 0.9900 . ?
C91 H91B 0.9900 . ?
C92 C96 1.29(3) . ?
C93 C94 1.40(4) . ?
C93 H93 0.9500 . ?
C94 C95 1.30(3) . ?
C94 H94 0.9500 . ?
C95 C96 1.53(3) . ?
C95 H95 0.9500 . ?
C96 H96 0.9500 . ?
C97 C98 1.35(3) . ?
C97 C102 1.42(3) . ?
C98 C99 1.40(3) . ?
C98 H98 0.9500 . ?
C99 C100 1.39(3) . ?
C99 H99 0.9500 . ?
C100 C101 1.42(3) . ?
C100 H100 0.9500 . ?
C101 C102 1.36(3) . ?
C101 H101 0.9500 . ?
C102 H102 0.9500 . ?
C103 C107 1.34(3) . ?
C103 C104 1.39(3) . ?
C104 H104 0.9500 . ?
C105 C106 1.34(3) . ?
C105 H105 0.9500 . ?
C106 C107 1.48(3) . ?
C106 H106 0.9500 . ?
C107 H107 0.9500 . ?
C108 C109 1.33(3) . ?
C108 H108 0.9500 . ?
C109 C110 1.29(4) . ?
C109 H109 0.9500 . ?
C110 C111 1.29(4) . ?
C110 H110 0.9500 . ?
C111 C112 1.56(3) . ?
C111 H11A 0.9900 . ?
C111 H11B 0.9900 . ?
C112 H11C 0.9900 . ?
C112 H11D 0.9900 . ?
C113 C114 1.62(4) . ?
C113 H11E 0.9900 . ?
C113 H11F 0.9900 . ?
C114 C115 1.38(3) . ?
C114 H11G 0.9900 . ?
C114 H11H 0.9900 . ?
C115 C116 1.55(4) . ?
C115 H11I 0.9900 . ?
C115 H11J 0.9900 . ?
C116 H11K 0.9900 . ?
C116 H11L 0.9900 . ?
C117 C118 1.38(3) . ?
C117 C122 1.42(3) . ?
C118 C119 1.41(3) . ?
C118 H118 0.9500 . ?
C119 C120 1.49(3) . ?
C119 H11M 0.9900 . ?
C119 H11N 0.9900 . ?
C120 C121 1.34(3) . ?
C120 H12C 0.9900 . ?
C120 H12D 0.9900 . ?
C121 C122 1.29(3) . ?
C121 H121 0.9500 . ?
C122 H122 0.9500 . ?
C123 C124 1.47(3) . ?
C123 H123 0.9500 . ?
C124 C125 1.28(3) . ?
C124 H124 0.9500 . ?
C125 C126 1.44(3) . ?
C125 H125 0.9500 . ?
C126 H126 0.9500 . ?
C127 C174 1.43(3) . ?
C127 C128 1.46(3) . ?
C128 C129 1.51(3) . ?
C128 H128 0.9500 . ?
C129 C130 1.41(4) . ?
C129 H129 0.9500 . ?
C130 C131 1.43(4) . ?
C130 H130 0.9500 . ?
C131 C174 1.32(3) . ?
C131 H131 0.9500 . ?
C132 C133 1.48(3) . ?
C132 H13A 0.9900 . ?
C132 H13B 0.9900 . ?
C133 C134 1.50(3) . ?
C133 H13C 0.9900 . ?
C133 H13D 0.9900 . ?
C134 C135 1.51(3) . ?
C134 H13E 0.9900 . ?
C134 H13F 0.9900 . ?
C135 H13G 0.9900 . ?
C135 H13H 0.9900 . ?
C136 C137 1.53(4) . ?
C136 H136 0.9500 . ?
C137 H137 0.9500 . ?
C138 H138 0.9500 . ?
C139 C140 1.44(3) . ?
C139 H139 0.9500 . ?
C140 C141 1.34(3) . ?
C140 H140 0.9500 . ?
C141 C142 1.34(3) . ?
C141 H141 0.9500 . ?
C142 C143 1.40(3) . ?
C142 H142 0.9500 . ?
C143 H143 0.9500 . ?
C144 C145 1.31(3) . ?
C144 C149 1.36(3) . ?
C145 C146 1.37(3) . ?
C145 H145 0.9500 . ?
C146 C147 1.40(3) . ?
C146 H146 0.9500 . ?
C147 C148 1.41(3) . ?
C147 H147 0.9500 . ?
C148 C149 1.40(3) . ?
C148 H148 0.9500 . ?
C149 H149 0.9500 . ?
C150 C154 1.37(3) . ?
C150 C151 1.38(3) . ?
C151 C152 1.46(4) . ?
C151 H151 0.9500 . ?
C152 H152 0.9500 . ?
C153 C154 1.27(3) . ?
C153 H153 0.9500 . ?
C154 H154 0.9500 . ?
C155 C156 1.46(3) . ?
C155 H15A 0.9900 . ?
C155 H15B 0.9900 . ?
C156 H15C 0.9900 . ?
C156 H15D 0.9900 . ?
C157 H15E 0.9900 . ?
C157 H15F 0.9900 . ?
C158 C159 1.40(3) . ?
C158 H158 0.9500 . ?
C159 C160 1.35(3) . ?
C159 H159 0.9500 . ?
C160 C161 1.34(3) . ?
C160 H160 0.9500 . ?
C161 C162 1.45(3) . ?
C161 H161 0.9500 . ?
C162 H162 0.9500 . ?
C163 C164 1.44(3) . ?
C163 C167 1.45(3) . ?
C163 H163 0.9500 . ?
C164 C165 1.35(4) . ?
C164 H164 0.9500 . ?
C165 C166 1.40(4) . ?
C165 H165 0.9500 . ?
C166 C168 1.36(4) . ?
C166 H166 0.9500 . ?
C167 C168 1.35(4) . ?
C168 H168 0.9500 . ?
C169 C170 1.36(3) . ?
C169 H169 0.9500 . ?
C170 C171 1.47(3) . ?
C170 H170 0.9500 . ?
C171 C172 1.23(3) . ?
C171 H171 0.9500 . ?
C172 C173 1.37(3) . ?
C172 H172 0.9500 . ?
C173 H173 0.9500 . ?
C174 H174 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O17 Ag1 Ag23 152.4(4) . . ?
O17 Ag1 Ag15 90.2(3) . . ?
Ag23 Ag1 Ag15 114.26(6) . . ?
O17 Ag1 Ag17 140.4(4) . . ?
Ag23 Ag1 Ag17 66.35(5) . . ?
Ag15 Ag1 Ag17 62.85(5) . . ?
O17 Ag1 Ag2 86.0(3) . . ?
Ag23 Ag1 Ag2 91.31(6) . . ?
Ag15 Ag1 Ag2 68.10(5) . . ?
Ag17 Ag1 Ag2 107.38(6) . . ?
O17 Ag1 Ag3 92.2(4) . . ?
Ag23 Ag1 Ag3 63.12(5) . . ?
Ag15 Ag1 Ag3 127.74(6) . . ?
Ag17 Ag1 Ag3 127.03(7) . . ?
Ag2 Ag1 Ag3 60.04(5) . . ?
O17 Ag1 Ag16 122.8(3) . . ?
Ag23 Ag1 Ag16 58.30(5) . . ?
Ag15 Ag1 Ag16 117.61(6) . . ?
Ag17 Ag1 Ag16 58.71(5) . . ?
Ag2 Ag1 Ag16 149.26(7) . . ?
Ag3 Ag1 Ag16 104.35(6) . . ?
O17 Ag1 Ag26 134.4(3) . . ?
Ag23 Ag1 Ag26 60.36(5) . . ?
Ag15 Ag1 Ag26 57.16(5) . . ?
Ag17 Ag1 Ag26 54.88(4) . . ?
Ag2 Ag1 Ag26 54.21(4) . . ?
Ag3 Ag1 Ag26 86.28(5) . . ?
Ag16 Ag1 Ag26 101.52(6) . . ?
O17 Ag1 Ag27 101.9(3) . . ?
Ag23 Ag1 Ag27 54.40(5) . . ?
Ag15 Ag1 Ag27 167.82(7) . . ?
Ag17 Ag1 Ag27 105.88(6) . . ?
Ag2 Ag1 Ag27 113.78(6) . . ?
Ag3 Ag1 Ag27 54.09(5) . . ?
Ag16 Ag1 Ag27 54.22(5) . . ?
Ag26 Ag1 Ag27 113.32(6) . . ?
C1 C13 C53 120.0 . . ?
C1 C13 P6 114.9(13) . . ?
C53 C13 P6 124.9(13) . . ?
C4 C1 C13 120.0 . . ?
C4 C1 H1 120.0 . . ?
C13 C1 H1 120.0 . . ?
C54 C4 C1 120.0 . . ?
C54 C4 H4 120.0 . . ?
C1 C4 H4 120.0 . . ?
C4 C54 C21 120.0 . . ?
C4 C54 H54 120.0 . . ?
C21 C54 H54 120.0 . . ?
C54 C21 C53 120.0 . . ?
C54 C21 H21 120.0 . . ?
C53 C21 H21 120.0 . . ?
C21 C53 C13 120.0 . . ?
C21 C53 H53 120.0 . . ?
C13 C53 H53 120.0 . . ?
O16 Ag2 Ag26 152.2(3) . . ?
O16 Ag2 Ag10 141.2(3) . . ?
Ag26 Ag2 Ag10 65.73(5) . . ?
O16 Ag2 Ag4 90.2(3) . . ?
Ag26 Ag2 Ag4 114.42(7) . . ?
Ag10 Ag2 Ag4 63.38(5) . . ?
O16 Ag2 Ag1 91.6(3) . . ?
Ag26 Ag2 Ag1 63.49(5) . . ?
Ag10 Ag2 Ag1 126.91(7) . . ?
Ag4 Ag2 Ag1 128.13(7) . . ?
O16 Ag2 Ag3 85.5(3) . . ?
Ag26 Ag2 Ag3 91.57(6) . . ?
Ag10 Ag2 Ag3 107.84(6) . . ?
Ag4 Ag2 Ag3 68.49(5) . . ?
Ag1 Ag2 Ag3 60.01(5) . . ?
O16 Ag2 Ag25 134.0(4) . . ?
Ag26 Ag2 Ag25 60.60(5) . . ?
Ag10 Ag2 Ag25 55.24(5) . . ?
Ag4 Ag2 Ag25 57.31(5) . . ?
Ag1 Ag2 Ag25 86.43(5) . . ?
Ag3 Ag2 Ag25 54.15(5) . . ?
O16 Ag2 Ag11 122.8(4) . . ?
Ag26 Ag2 Ag11 58.28(5) . . ?
Ag10 Ag2 Ag11 58.42(5) . . ?
Ag4 Ag2 Ag11 117.60(6) . . ?
Ag1 Ag2 Ag11 104.38(6) . . ?
Ag3 Ag2 Ag11 149.56(7) . . ?
Ag25 Ag2 Ag11 102.02(6) . . ?
O16 Ag2 Ag15 101.2(3) . . ?
Ag26 Ag2 Ag15 54.97(5) . . ?
Ag10 Ag2 Ag15 105.77(6) . . ?
Ag4 Ag2 Ag15 168.46(7) . . ?
Ag1 Ag2 Ag15 54.05(4) . . ?
Ag3 Ag2 Ag15 113.77(6) . . ?
Ag25 Ag2 Ag15 113.99(6) . . ?
Ag11 Ag2 Ag15 54.37(5) . . ?
O5 Ag3 Ag25 152.1(3) . . ?
O5 Ag3 Ag28 140.7(3) . . ?
Ag25 Ag3 Ag28 66.21(5) . . ?
O5 Ag3 Ag27 90.9(3) . . ?
Ag25 Ag3 Ag27 113.98(6) . . ?
Ag28 Ag3 Ag27 62.70(5) . . ?
O5 Ag3 Ag1 85.7(3) . . ?
Ag25 Ag3 Ag1 91.66(5) . . ?
Ag28 Ag3 Ag1 108.15(6) . . ?
Ag27 Ag3 Ag1 68.60(5) . . ?
O5 Ag3 Ag2 91.8(3) . . ?
Ag25 Ag3 Ag2 63.30(5) . . ?
Ag28 Ag3 Ag2 127.20(6) . . ?
Ag27 Ag3 Ag2 128.09(6) . . ?
Ag1 Ag3 Ag2 59.95(5) . . ?
O5 Ag3 Ag5 122.2(3) . . ?
Ag25 Ag3 Ag5 58.26(5) . . ?
Ag28 Ag3 Ag5 58.90(5) . . ?
Ag27 Ag3 Ag5 117.70(7) . . ?
Ag1 Ag3 Ag5 149.69(6) . . ?
Ag2 Ag3 Ag5 103.99(6) . . ?
O5 Ag3 Ag23 134.4(3) . . ?
Ag25 Ag3 Ag23 60.54(5) . . ?
Ag28 Ag3 Ag23 55.54(5) . . ?
Ag27 Ag3 Ag23 57.00(5) . . ?
Ag1 Ag3 Ag23 54.28(5) . . ?
Ag2 Ag3 Ag23 86.21(5) . . ?
Ag5 Ag3 Ag23 102.26(6) . . ?
O5 Ag3 Ag4 101.1(3) . . ?
Ag25 Ag3 Ag4 54.83(5) . . ?
Ag28 Ag3 Ag4 106.00(6) . . ?
Ag27 Ag3 Ag4 167.88(7) . . ?
Ag1 Ag3 Ag4 113.67(6) . . ?
Ag2 Ag3 Ag4 53.99(5) . . ?
Ag5 Ag3 Ag4 53.98(5) . . ?
Ag23 Ag3 Ag4 113.78(6) . . ?
P3 Ag4 Ag25 168.76(15) . . ?
P3 Ag4 Ag2 104.97(15) . . ?
Ag25 Ag4 Ag2 63.90(5) . . ?
P3 Ag4 Ag5 127.98(14) . . ?
Ag25 Ag4 Ag5 58.93(5) . . ?
Ag2 Ag4 Ag5 110.72(6) . . ?
P3 Ag4 Ag6 131.30(15) . . ?
Ag25 Ag4 Ag6 59.05(5) . . ?
Ag2 Ag4 Ag6 116.24(7) . . ?
Ag5 Ag4 Ag6 59.49(6) . . ?
P3 Ag4 Ag10 121.02(14) . . ?
Ag25 Ag4 Ag10 55.60(5) . . ?
Ag2 Ag4 Ag10 58.08(5) . . ?
Ag5 Ag4 Ag10 109.82(7) . . ?
Ag6 Ag4 Ag10 67.43(6) . . ?
P3 Ag4 Ag3 121.43(15) . . ?
Ag25 Ag4 Ag3 52.31(4) . . ?
Ag2 Ag4 Ag3 57.52(5) . . ?
Ag5 Ag4 Ag3 57.72(5) . . ?
Ag6 Ag4 Ag3 102.70(6) . . ?
Ag10 Ag4 Ag3 96.97(5) . . ?
P12 Ag5 Ag25 169.42(15) . . ?
P12 Ag5 Ag6 128.66(14) . . ?
Ag25 Ag5 Ag6 59.56(5) . . ?
P12 Ag5 Ag4 128.85(16) . . ?
Ag25 Ag5 Ag4 59.65(5) . . ?
Ag6 Ag5 Ag4 60.30(6) . . ?
P12 Ag5 Ag28 104.43(14) . . ?
Ag25 Ag5 Ag28 65.03(5) . . ?
Ag6 Ag5 Ag28 111.90(6) . . ?
Ag4 Ag5 Ag28 117.70(7) . . ?
P12 Ag5 Ag3 118.62(15) . . ?
Ag25 Ag5 Ag3 56.04(5) . . ?
Ag6 Ag5 Ag3 111.15(6) . . ?
Ag4 Ag5 Ag3 68.30(6) . . ?
Ag28 Ag5 Ag3 58.13(5) . . ?
P12 Ag5 Ag7 122.84(17) . . ?
Ag25 Ag5 Ag7 53.25(5) . . ?
Ag6 Ag5 Ag7 58.42(5) . . ?
Ag4 Ag5 Ag7 104.30(6) . . ?
Ag28 Ag5 Ag7 57.79(5) . . ?
Ag3 Ag5 Ag7 97.53(5) . . ?
P2 Ag6 Ag25 171.12(14) . . ?
P2 Ag6 Ag5 127.79(15) . . ?
Ag25 Ag6 Ag5 59.34(5) . . ?
P2 Ag6 Ag4 127.44(15) . . ?
Ag25 Ag6 Ag4 59.55(5) . . ?
Ag5 Ag6 Ag4 60.21(6) . . ?
P2 Ag6 Ag9 106.21(14) . . ?
Ag25 Ag6 Ag9 64.93(5) . . ?
Ag5 Ag6 Ag9 116.97(6) . . ?
Ag4 Ag6 Ag9 112.27(7) . . ?
P2 Ag6 Ag7 119.54(16) . . ?
Ag25 Ag6 Ag7 56.15(5) . . ?
Ag5 Ag6 Ag7 67.20(5) . . ?
Ag4 Ag6 Ag7 110.80(6) . . ?
Ag9 Ag6 Ag7 58.46(5) . . ?
P2 Ag6 Ag10 124.23(16) . . ?
Ag25 Ag6 Ag10 52.62(4) . . ?
Ag5 Ag6 Ag10 103.49(6) . . ?
Ag4 Ag6 Ag10 58.21(5) . . ?
Ag9 Ag6 Ag10 58.33(5) . . ?
Ag7 Ag6 Ag10 97.72(5) . . ?
O7 Ag7 Ag25 151.3(4) . . ?
O7 Ag7 Ag14 90.7(4) . . ?
Ag25 Ag7 Ag14 113.95(7) . . ?
O7 Ag7 Ag9 141.8(4) . . ?
Ag25 Ag7 Ag9 66.02(5) . . ?
Ag14 Ag7 Ag9 64.35(5) . . ?
O7 Ag7 Ag28 89.6(3) . . ?
Ag25 Ag7 Ag28 64.67(5) . . ?
Ag14 Ag7 Ag28 124.95(7) . . ?
Ag9 Ag7 Ag28 128.07(7) . . ?
O7 Ag7 Ag6 122.7(4) . . ?
Ag25 Ag7 Ag6 58.59(5) . . ?
Ag14 Ag7 Ag6 119.56(6) . . ?
Ag9 Ag7 Ag6 58.82(5) . . ?
Ag28 Ag7 Ag6 105.79(6) . . ?
O7 Ag7 Ag21 85.5(3) . . ?
Ag25 Ag7 Ag21 92.06(6) . . ?
Ag14 Ag7 Ag21 64.32(5) . . ?
Ag9 Ag7 Ag21 106.35(6) . . ?
Ag28 Ag7 Ag21 60.84(5) . . ?
Ag6 Ag7 Ag21 150.10(7) . . ?
O7 Ag7 Ag24 134.5(4) . . ?
Ag25 Ag7 Ag24 60.09(5) . . ?
Ag14 Ag7 Ag24 56.53(5) . . ?
Ag9 Ag7 Ag24 55.08(4) . . ?
Ag28 Ag7 Ag24 86.35(5) . . ?
Ag6 Ag7 Ag24 101.91(6) . . ?
Ag21 Ag7 Ag24 53.39(4) . . ?
O7 Ag7 Ag5 100.4(4) . . ?
Ag25 Ag7 Ag5 55.25(5) . . ?
Ag14 Ag7 Ag5 168.92(7) . . ?
Ag9 Ag7 Ag5 106.22(6) . . ?
Ag28 Ag7 Ag5 55.24(5) . . ?
Ag6 Ag7 Ag5 54.38(5) . . ?
Ag21 Ag7 Ag5 115.63(6) . . ?
Ag24 Ag7 Ag5 113.80(6) . . ?
P10 Ag8 Ag26 167.40(16) . . ?
P10 Ag8 Ag19 101.80(15) . . ?
Ag26 Ag8 Ag19 65.70(5) . . ?
P10 Ag8 Ag11 129.92(15) . . ?
Ag26 Ag8 Ag11 59.50(5) . . ?
Ag19 Ag8 Ag11 117.56(7) . . ?
P10 Ag8 Ag15 130.87(16) . . ?
Ag26 Ag8 Ag15 59.50(5) . . ?
Ag19 Ag8 Ag15 113.23(6) . . ?
Ag11 Ag8 Ag15 60.08(5) . . ?
P10 Ag8 Ag12 116.46(15) . . ?
Ag26 Ag8 Ag12 56.47(5) . . ?
Ag19 Ag8 Ag12 58.13(5) . . ?
Ag11 Ag8 Ag12 67.72(5) . . ?
Ag15 Ag8 Ag12 111.12(6) . . ?
P10 Ag8 Ag17 122.73(14) . . ?
Ag26 Ag8 Ag17 53.39(4) . . ?
Ag19 Ag8 Ag17 59.31(5) . . ?
Ag11 Ag8 Ag17 104.23(6) . . ?
Ag15 Ag8 Ag17 58.47(5) . . ?
Ag12 Ag8 Ag17 98.48(6) . . ?
O14 Ag9 Ag24 152.0(3) . . ?
O14 Ag9 Ag7 141.8(3) . . ?
Ag24 Ag9 Ag7 65.89(5) . . ?
O14 Ag9 Ag6 90.4(3) . . ?
Ag24 Ag9 Ag6 113.21(6) . . ?
Ag7 Ag9 Ag6 62.72(5) . . ?
O14 Ag9 Ag12 91.1(3) . . ?
Ag24 Ag9 Ag12 62.99(5) . . ?
Ag7 Ag9 Ag12 126.35(6) . . ?
Ag6 Ag9 Ag12 126.70(7) . . ?
O14 Ag9 Ag10 84.5(3) . . ?
Ag24 Ag9 Ag10 90.67(6) . . ?
Ag7 Ag9 Ag10 106.60(6) . . ?
Ag6 Ag9 Ag10 67.33(6) . . ?
Ag12 Ag9 Ag10 59.82(5) . . ?
O14 Ag9 Ag14 125.8(3) . . ?
Ag24 Ag9 Ag14 57.65(5) . . ?
Ag7 Ag9 Ag14 57.81(5) . . ?
Ag6 Ag9 Ag14 117.10(7) . . ?
Ag12 Ag9 Ag14 104.46(6) . . ?
Ag10 Ag9 Ag14 147.80(6) . . ?
O14 Ag9 Ag25 132.6(3) . . ?
Ag24 Ag9 Ag25 60.00(4) . . ?
Ag7 Ag9 Ag25 54.89(5) . . ?
Ag6 Ag9 Ag25 56.46(5) . . ?
Ag12 Ag9 Ag25 85.52(5) . . ?
Ag10 Ag9 Ag25 53.36(5) . . ?
Ag14 Ag9 Ag25 100.52(6) . . ?
O14 Ag9 Ag13 101.4(3) . . ?
Ag24 Ag9 Ag13 55.87(5) . . ?
Ag7 Ag9 Ag13 106.25(6) . . ?
Ag6 Ag9 Ag13 168.17(6) . . ?
Ag12 Ag9 Ag13 55.07(5) . . ?
Ag10 Ag9 Ag13 114.63(6) . . ?
Ag14 Ag9 Ag13 54.54(5) . . ?
Ag25 Ag9 Ag13 114.45(5) . . ?
O2 Ag10 Ag25 152.6(3) . . ?
O2 Ag10 Ag2 140.7(4) . . ?
Ag25 Ag10 Ag2 65.31(5) . . ?
O2 Ag10 Ag11 90.9(3) . . ?
Ag25 Ag10 Ag11 113.81(6) . . ?
Ag2 Ag10 Ag11 63.61(5) . . ?
O2 Ag10 Ag12 86.9(3) . . ?
Ag25 Ag10 Ag12 91.69(6) . . ?
Ag2 Ag10 Ag12 107.82(6) . . ?
Ag11 Ag10 Ag12 67.78(5) . . ?
O2 Ag10 Ag4 120.9(3) . . ?
Ag25 Ag10 Ag4 58.78(5) . . ?
Ag2 Ag10 Ag4 58.54(5) . . ?
Ag11 Ag10 Ag4 117.92(7) . . ?
Ag12 Ag10 Ag4 150.19(7) . . ?
O2 Ag10 Ag9 92.0(3) . . ?
Ag25 Ag10 Ag9 64.05(5) . . ?
Ag2 Ag10 Ag9 127.04(6) . . ?
Ag11 Ag10 Ag9 127.34(7) . . ?
Ag12 Ag10 Ag9 59.92(5) . . ?
Ag4 Ag10 Ag9 105.00(6) . . ?
O2 Ag10 Ag26 135.2(3) . . ?
Ag25 Ag10 Ag26 60.42(4) . . ?
Ag2 Ag10 Ag26 55.30(5) . . ?
Ag11 Ag10 Ag26 56.80(5) . . ?
Ag12 Ag10 Ag26 54.07(4) . . ?
Ag4 Ag10 Ag26 102.54(5) . . ?
Ag9 Ag10 Ag26 86.42(5) . . ?
O2 Ag10 Ag6 100.9(3) . . ?
Ag25 Ag10 Ag6 55.01(5) . . ?
Ag2 Ag10 Ag6 105.45(6) . . ?
Ag11 Ag10 Ag6 168.10(6) . . ?
Ag12 Ag10 Ag6 113.91(6) . . ?
Ag4 Ag10 Ag6 54.36(5) . . ?
Ag9 Ag10 Ag6 54.34(5) . . ?
Ag26 Ag10 Ag6 113.81(6) . . ?
P4 Ag11 Ag26 168.80(14) . . ?
P4 Ag11 Ag10 104.19(14) . . ?
Ag26 Ag11 Ag10 64.61(5) . . ?
P4 Ag11 Ag8 129.63(14) . . ?
Ag26 Ag11 Ag8 58.70(5) . . ?
Ag10 Ag11 Ag8 111.20(7) . . ?
P4 Ag11 Ag15 130.02(16) . . ?
Ag26 Ag11 Ag15 59.24(5) . . ?
Ag10 Ag11 Ag15 116.64(6) . . ?
Ag8 Ag11 Ag15 60.09(5) . . ?
P4 Ag11 Ag2 118.94(15) . . ?
Ag26 Ag11 Ag2 55.92(5) . . ?
Ag10 Ag11 Ag2 57.97(5) . . ?
Ag8 Ag11 Ag2 110.05(6) . . ?
Ag15 Ag11 Ag2 67.41(5) . . ?
P4 Ag11 Ag12 122.44(16) . . ?
Ag26 Ag11 Ag12 52.93(5) . . ?
Ag10 Ag11 Ag12 58.01(5) . . ?
Ag8 Ag11 Ag12 57.89(5) . . ?
Ag15 Ag11 Ag12 103.76(6) . . ?
Ag2 Ag11 Ag12 97.47(6) . . ?
O13 Ag12 Ag26 151.5(4) . . ?
O13 Ag12 Ag19 140.8(4) . . ?
Ag26 Ag12 Ag19 66.57(5) . . ?
O13 Ag12 Ag13 90.5(4) . . ?
Ag26 Ag12 Ag13 114.52(6) . . ?
Ag19 Ag12 Ag13 64.25(5) . . ?
O13 Ag12 Ag8 122.3(3) . . ?
Ag26 Ag12 Ag8 57.94(5) . . ?
Ag19 Ag12 Ag8 58.80(5) . . ?
Ag13 Ag12 Ag8 119.65(6) . . ?
O13 Ag12 Ag10 91.2(4) . . ?
Ag26 Ag12 Ag10 63.66(5) . . ?
Ag19 Ag12 Ag10 127.73(6) . . ?
Ag13 Ag12 Ag10 125.78(7) . . ?
Ag8 Ag12 Ag10 104.48(6) . . ?
O13 Ag12 Ag9 85.8(3) . . ?
Ag26 Ag12 Ag9 92.14(5) . . ?
Ag19 Ag12 Ag9 107.73(6) . . ?
Ag13 Ag12 Ag9 65.84(5) . . ?
Ag8 Ag12 Ag9 149.74(6) . . ?
Ag10 Ag12 Ag9 60.26(5) . . ?
O13 Ag12 Ag24 135.1(3) . . ?
Ag26 Ag12 Ag24 60.28(5) . . ?
Ag19 Ag12 Ag24 55.53(4) . . ?
Ag13 Ag12 Ag24 57.02(5) . . ?
Ag8 Ag12 Ag24 101.65(5) . . ?
Ag10 Ag12 Ag24 85.96(5) . . ?
Ag9 Ag12 Ag24 54.23(4) . . ?
O13 Ag12 Ag11 100.3(4) . . ?
Ag26 Ag12 Ag11 54.88(5) . . ?
Ag19 Ag12 Ag11 106.57(6) . . ?
Ag13 Ag12 Ag11 169.15(6) . . ?
Ag8 Ag12 Ag11 54.40(5) . . ?
Ag10 Ag12 Ag11 54.21(5) . . ?
Ag9 Ag12 Ag11 114.19(6) . . ?
Ag24 Ag12 Ag11 113.51(6) . . ?
P9 Ag13 Ag24 173.56(17) . . ?
P9 Ag13 Ag20 124.27(16) . . ?
Ag24 Ag13 Ag20 59.52(5) . . ?
P9 Ag13 Ag14 126.77(16) . . ?
Ag24 Ag13 Ag14 59.27(5) . . ?
Ag20 Ag13 Ag14 60.81(5) . . ?
P9 Ag13 Ag12 109.86(16) . . ?
Ag24 Ag13 Ag12 63.98(5) . . ?
Ag20 Ag13 Ag12 114.28(6) . . ?
Ag14 Ag13 Ag12 113.15(7) . . ?
P9 Ag13 Ag19 120.17(15) . . ?
Ag24 Ag13 Ag19 55.55(5) . . ?
Ag20 Ag13 Ag19 63.99(5) . . ?
Ag14 Ag13 Ag19 108.85(6) . . ?
Ag12 Ag13 Ag19 57.65(5) . . ?
P9 Ag13 Ag9 125.51(15) . . ?
Ag24 Ag13 Ag9 53.86(4) . . ?
Ag20 Ag13 Ag9 105.99(6) . . ?
Ag14 Ag13 Ag9 60.19(5) . . ?
Ag12 Ag13 Ag9 59.09(5) . . ?
Ag19 Ag13 Ag9 98.66(6) . . ?
P6 Ag14 Ag24 166.85(17) . . ?
P6 Ag14 Ag13 132.04(17) . . ?
Ag24 Ag14 Ag13 59.38(5) . . ?
P6 Ag14 Ag7 101.84(17) . . ?
Ag24 Ag14 Ag7 65.08(5) . . ?
Ag13 Ag14 Ag7 115.74(7) . . ?
P6 Ag14 Ag20 130.22(16) . . ?
Ag24 Ag14 Ag20 58.96(5) . . ?
Ag13 Ag14 Ag20 59.07(5) . . ?
Ag7 Ag14 Ag20 114.13(7) . . ?
P6 Ag14 Ag9 119.71(16) . . ?
Ag24 Ag14 Ag9 55.60(5) . . ?
Ag13 Ag14 Ag9 65.26(5) . . ?
Ag7 Ag14 Ag9 57.85(5) . . ?
Ag20 Ag14 Ag9 108.52(7) . . ?
P6 Ag14 Ag21 119.12(17) . . ?
Ag24 Ag14 Ag21 54.26(5) . . ?
Ag13 Ag14 Ag21 105.51(6) . . ?
Ag7 Ag14 Ag21 59.96(5) . . ?
Ag20 Ag14 Ag21 60.39(5) . . ?
Ag9 Ag14 Ag21 99.02(6) . . ?
P7 Ag15 Ag26 171.28(14) . . ?
P7 Ag15 Ag1 107.29(14) . . ?
Ag26 Ag15 Ag1 64.33(5) . . ?
P7 Ag15 Ag11 125.32(14) . . ?
Ag26 Ag15 Ag11 59.12(5) . . ?
Ag1 Ag15 Ag11 111.44(6) . . ?
P7 Ag15 Ag8 129.84(14) . . ?
Ag26 Ag15 Ag8 58.58(5) . . ?
Ag1 Ag15 Ag8 115.80(7) . . ?
Ag11 Ag15 Ag8 59.83(5) . . ?
P7 Ag15 Ag17 123.01(14) . . ?
Ag26 Ag15 Ag17 55.77(5) . . ?
Ag1 Ag15 Ag17 58.75(5) . . ?
Ag11 Ag15 Ag17 109.81(7) . . ?
Ag8 Ag15 Ag17 66.13(5) . . ?
P7 Ag15 Ag2 121.51(15) . . ?
Ag26 Ag15 Ag2 52.77(5) . . ?
Ag1 Ag15 Ag2 57.85(5) . . ?
Ag11 Ag15 Ag2 58.23(5) . . ?
Ag8 Ag15 Ag2 103.08(6) . . ?
Ag17 Ag15 Ag2 97.76(6) . . ?
P8 Ag16 Ag23 166.71(15) . . ?
P8 Ag16 Ag18 132.88(16) . . ?
Ag23 Ag16 Ag18 59.18(5) . . ?
P8 Ag16 Ag17 101.89(14) . . ?
Ag23 Ag16 Ag17 65.46(5) . . ?
Ag18 Ag16 Ag17 111.81(6) . . ?
P8 Ag16 Ag27 129.09(15) . . ?
Ag23 Ag16 Ag27 59.22(5) . . ?
Ag18 Ag16 Ag27 59.73(6) . . ?
Ag17 Ag16 Ag27 117.97(6) . . ?
P8 Ag16 Ag1 114.49(16) . . ?
Ag23 Ag16 Ag1 56.25(5) . . ?
Ag18 Ag16 Ag1 111.01(6) . . ?
Ag17 Ag16 Ag1 58.51(5) . . ?
Ag27 Ag16 Ag1 68.50(5) . . ?
P8 Ag16 Ag22 124.70(16) . . ?
Ag23 Ag16 Ag22 53.36(4) . . ?
Ag18 Ag16 Ag22 57.67(5) . . ?
Ag17 Ag16 Ag22 58.45(5) . . ?
Ag27 Ag16 Ag22 103.52(6) . . ?
Ag1 Ag16 Ag22 98.14(5) . . ?
O9 Ag17 Ag26 152.4(4) . . ?
O9 Ag17 Ag1 140.7(4) . . ?
Ag26 Ag17 Ag1 65.41(5) . . ?
O9 Ag17 Ag16 92.2(4) . . ?
Ag26 Ag17 Ag16 112.73(6) . . ?
Ag1 Ag17 Ag16 62.78(5) . . ?
O9 Ag17 Ag22 88.0(4) . . ?
Ag26 Ag17 Ag22 91.37(6) . . ?
Ag1 Ag17 Ag22 106.38(6) . . ?
Ag16 Ag17 Ag22 66.39(5) . . ?
O9 Ag17 Ag15 120.7(4) . . ?
Ag26 Ag17 Ag15 58.95(5) . . ?
Ag1 Ag17 Ag15 58.40(5) . . ?
Ag16 Ag17 Ag15 117.27(7) . . ?
Ag22 Ag17 Ag15 149.78(6) . . ?
O9 Ag17 Ag19 91.8(4) . . ?
Ag26 Ag17 Ag19 64.51(5) . . ?
Ag1 Ag17 Ag19 127.22(6) . . ?
Ag16 Ag17 Ag19 125.85(7) . . ?
Ag22 Ag17 Ag19 59.83(5) . . ?
Ag15 Ag17 Ag19 106.36(6) . . ?
O9 Ag17 Ag23 136.1(4) . . ?
Ag26 Ag17 Ag23 59.89(4) . . ?
Ag1 Ag17 Ag23 54.73(5) . . ?
Ag16 Ag17 Ag23 56.07(4) . . ?
Ag22 Ag17 Ag23 53.44(5) . . ?
Ag15 Ag17 Ag23 101.78(6) . . ?
Ag19 Ag17 Ag23 85.95(5) . . ?
O9 Ag17 Ag8 100.1(4) . . ?
Ag26 Ag17 Ag8 55.47(5) . . ?
Ag1 Ag17 Ag8 106.32(6) . . ?
Ag16 Ag17 Ag8 167.73(6) . . ?
Ag22 Ag17 Ag8 114.35(6) . . ?
Ag15 Ag17 Ag8 55.41(5) . . ?
Ag19 Ag17 Ag8 54.92(5) . . ?
Ag23 Ag17 Ag8 113.69(6) . . ?
P5 Ag18 Ag23 170.03(16) . . ?
P5 Ag18 Ag21 104.89(15) . . ?
Ag23 Ag18 Ag21 65.15(5) . . ?
P5 Ag18 Ag27 128.27(15) . . ?
Ag23 Ag18 Ag27 59.40(5) . . ?
Ag21 Ag18 Ag27 112.28(6) . . ?
P5 Ag18 Ag16 129.00(15) . . ?
Ag23 Ag18 Ag16 59.08(5) . . ?
Ag21 Ag18 Ag16 116.83(6) . . ?
Ag27 Ag18 Ag16 60.34(5) . . ?
P5 Ag18 Ag22 118.86(15) . . ?
Ag23 Ag18 Ag22 56.46(5) . . ?
Ag21 Ag18 Ag22 58.75(5) . . ?
Ag27 Ag18 Ag22 110.93(7) . . ?
Ag16 Ag18 Ag22 66.90(5) . . ?
P5 Ag18 Ag28 123.27(15) . . ?
Ag23 Ag18 Ag28 53.01(4) . . ?
Ag21 Ag18 Ag28 58.77(5) . . ?
Ag27 Ag18 Ag28 57.91(5) . . ?
Ag16 Ag18 Ag28 103.56(6) . . ?
Ag22 Ag18 Ag28 98.54(5) . . ?
O10 Ag19 Ag24 149.3(4) . . ?
O10 Ag19 Ag12 144.8(3) . . ?
Ag24 Ag19 Ag12 65.07(5) . . ?
O10 Ag19 Ag8 94.3(4) . . ?
Ag24 Ag19 Ag8 112.13(6) . . ?
Ag12 Ag19 Ag8 63.07(5) . . ?
O10 Ag19 Ag22 88.8(3) . . ?
Ag24 Ag19 Ag22 63.69(5) . . ?
Ag12 Ag19 Ag22 126.00(6) . . ?
Ag8 Ag19 Ag22 124.77(7) . . ?
O10 Ag19 Ag17 85.8(3) . . ?
Ag24 Ag19 Ag17 90.97(6) . . ?
Ag12 Ag19 Ag17 106.16(6) . . ?
Ag8 Ag19 Ag17 65.77(5) . . ?
Ag22 Ag19 Ag17 59.50(5) . . ?
O10 Ag19 Ag13 123.4(4) . . ?
Ag24 Ag19 Ag13 57.86(5) . . ?
Ag12 Ag19 Ag13 58.11(5) . . ?
Ag8 Ag19 Ag13 117.89(6) . . ?
Ag22 Ag19 Ag13 105.20(6) . . ?
Ag17 Ag19 Ag13 148.33(6) . . ?
O10 Ag19 Ag26 135.2(4) . . ?
Ag24 Ag19 Ag26 59.50(5) . . ?
Ag12 Ag19 Ag26 54.98(4) . . ?
Ag8 Ag19 Ag26 55.80(5) . . ?
Ag22 Ag19 Ag26 84.60(5) . . ?
Ag17 Ag19 Ag26 52.95(4) . . ?
Ag13 Ag19 Ag26 101.04(5) . . ?
O10 Ag19 Ag20 97.4(4) . . ?
Ag24 Ag19 Ag20 56.70(5) . . ?
Ag12 Ag19 Ag20 106.52(6) . . ?
Ag8 Ag19 Ag20 168.32(7) . . ?
Ag22 Ag19 Ag20 55.78(5) . . ?
Ag17 Ag19 Ag20 115.06(6) . . ?
Ag13 Ag19 Ag20 54.72(5) . . ?
Ag26 Ag19 Ag20 114.55(6) . . ?
P1 Ag20 Ag24 168.38(16) . . ?
P1 Ag20 Ag13 128.21(15) . . ?
Ag24 Ag20 Ag13 59.79(5) . . ?
P1 Ag20 Ag22 103.75(15) . . ?
Ag24 Ag20 Ag22 64.73(5) . . ?
Ag13 Ag20 Ag22 114.79(7) . . ?
P1 Ag20 Ag14 131.01(16) . . ?
Ag24 Ag20 Ag14 59.13(5) . . ?
Ag13 Ag20 Ag14 60.12(5) . . ?
Ag22 Ag20 Ag14 114.46(6) . . ?
P1 Ag20 Ag21 120.86(15) . . ?
Ag24 Ag20 Ag21 55.43(5) . . ?
Ag13 Ag20 Ag21 108.84(6) . . ?
Ag22 Ag20 Ag21 57.80(5) . . ?
Ag14 Ag20 Ag21 63.73(5) . . ?
P1 Ag20 Ag19 119.22(16) . . ?
Ag24 Ag20 Ag19 54.71(5) . . ?
Ag13 Ag20 Ag19 61.28(5) . . ?
Ag22 Ag20 Ag19 59.93(5) . . ?
Ag14 Ag20 Ag19 106.32(6) . . ?
Ag21 Ag20 Ag19 99.36(6) . . ?
O4 Ag21 Ag24 154.3(3) . . ?
O4 Ag21 Ag22 139.1(4) . . ?
Ag24 Ag21 Ag22 65.91(5) . . ?
O4 Ag21 Ag18 89.4(3) . . ?
Ag24 Ag21 Ag18 113.15(7) . . ?
Ag22 Ag21 Ag18 62.15(5) . . ?
O4 Ag21 Ag7 92.9(4) . . ?
Ag24 Ag21 Ag7 64.24(5) . . ?
Ag22 Ag21 Ag7 127.12(7) . . ?
Ag18 Ag21 Ag7 125.93(7) . . ?
O4 Ag21 Ag28 85.8(3) . . ?
Ag24 Ag21 Ag28 91.56(6) . . ?
Ag22 Ag21 Ag28 106.53(6) . . ?
Ag18 Ag21 Ag28 67.21(5) . . ?
Ag7 Ag21 Ag28 59.13(5) . . ?
O4 Ag21 Ag20 123.9(3) . . ?
Ag24 Ag21 Ag20 58.02(5) . . ?
Ag22 Ag21 Ag20 58.17(5) . . ?
Ag18 Ag21 Ag20 116.63(6) . . ?
Ag7 Ag21 Ag20 106.27(6) . . ?
Ag28 Ag21 Ag20 149.02(7) . . ?
O4 Ag21 Ag23 133.3(3) . . ?
Ag24 Ag21 Ag23 60.15(5) . . ?
Ag22 Ag21 Ag23 54.85(5) . . ?
Ag18 Ag21 Ag23 56.48(5) . . ?
Ag7 Ag21 Ag23 85.25(5) . . ?
Ag28 Ag21 Ag23 53.56(5) . . ?
Ag20 Ag21 Ag23 101.05(6) . . ?
O4 Ag21 Ag14 101.3(3) . . ?
Ag24 Ag21 Ag14 56.88(5) . . ?
Ag22 Ag21 Ag14 107.85(6) . . ?
Ag18 Ag21 Ag14 169.25(7) . . ?
Ag7 Ag21 Ag14 55.72(5) . . ?
Ag28 Ag21 Ag14 114.68(6) . . ?
Ag20 Ag21 Ag14 55.87(5) . . ?
Ag23 Ag21 Ag14 115.29(6) . . ?
O11 Ag22 Ag23 150.9(4) . . ?
O11 Ag22 Ag21 140.3(4) . . ?
Ag23 Ag22 Ag21 66.29(5) . . ?
O11 Ag22 Ag20 92.7(4) . . ?
Ag23 Ag22 Ag20 114.25(6) . . ?
Ag21 Ag22 Ag20 64.02(5) . . ?
O11 Ag22 Ag18 118.0(3) . . ?
Ag23 Ag22 Ag18 59.04(5) . . ?
Ag21 Ag22 Ag18 59.10(5) . . ?
Ag20 Ag22 Ag18 119.22(7) . . ?
O11 Ag22 Ag17 91.4(4) . . ?
Ag23 Ag22 Ag17 64.84(5) . . ?
Ag21 Ag22 Ag17 128.21(6) . . ?
Ag20 Ag22 Ag17 124.71(7) . . ?
Ag18 Ag22 Ag17 106.69(6) . . ?
O11 Ag22 Ag19 89.0(3) . . ?
Ag23 Ag22 Ag19 92.98(6) . . ?
Ag21 Ag22 Ag19 106.57(6) . . ?
Ag20 Ag22 Ag19 64.29(5) . . ?
Ag18 Ag22 Ag19 151.41(7) . . ?
Ag17 Ag22 Ag19 60.68(5) . . ?
O11 Ag22 Ag24 138.4(3) . . ?
Ag23 Ag22 Ag24 60.34(5) . . ?
Ag21 Ag22 Ag24 54.94(5) . . ?
Ag20 Ag22 Ag24 56.64(5) . . ?
Ag18 Ag22 Ag24 102.29(6) . . ?
Ag17 Ag22 Ag24 86.14(5) . . ?
Ag19 Ag22 Ag24 53.96(4) . . ?
O11 Ag22 Ag16 97.6(4) . . ?
Ag23 Ag22 Ag16 55.57(5) . . ?
Ag21 Ag22 Ag16 107.28(6) . . ?
Ag20 Ag22 Ag16 169.62(6) . . ?
Ag18 Ag22 Ag16 55.43(5) . . ?
Ag17 Ag22 Ag16 55.16(5) . . ?
Ag19 Ag22 Ag16 115.54(6) . . ?
Ag24 Ag22 Ag16 114.19(6) . . ?
O11 Ag22 Mo4 30.6(3) . . ?
Ag23 Ag22 Mo4 128.61(7) . . ?
Ag21 Ag22 Mo4 161.08(7) . . ?
Ag20 Ag22 Mo4 97.30(6) . . ?
Ag18 Ag22 Mo4 136.18(6) . . ?
Ag17 Ag22 Mo4 63.88(5) . . ?
Ag19 Ag22 Mo4 64.61(5) . . ?
Ag24 Ag22 Mo4 118.56(6) . . ?
Ag16 Ag22 Mo4 91.60(6) . . ?
Ag22 Ag23 Ag1 118.38(6) . . ?
Ag22 Ag23 Ag28 119.22(7) . . ?
Ag1 Ag23 Ag28 120.08(6) . . ?
Ag22 Ag23 Ag16 71.07(5) . . ?
Ag1 Ag23 Ag16 65.45(5) . . ?
Ag28 Ag23 Ag16 121.30(6) . . ?
Ag22 Ag23 Ag18 64.50(5) . . ?
Ag1 Ag23 Ag18 121.67(6) . . ?
Ag28 Ag23 Ag18 72.12(5) . . ?
Ag16 Ag23 Ag18 61.74(5) . . ?
Ag22 Ag23 Ag27 120.01(6) . . ?
Ag1 Ag23 Ag27 73.27(6) . . ?
Ag28 Ag23 Ag27 65.15(5) . . ?
Ag16 Ag23 Ag27 61.93(5) . . ?
Ag18 Ag23 Ag27 61.48(5) . . ?
Ag22 Ag23 Ag25 125.21(6) . . ?
Ag1 Ag23 Ag25 93.55(6) . . ?
Ag28 Ag23 Ag25 65.61(5) . . ?
Ag16 Ag23 Ag25 158.81(7) . . ?
Ag18 Ag23 Ag25 134.89(7) . . ?
Ag27 Ag23 Ag25 110.95(6) . . ?
Ag22 Ag23 Ag26 93.03(5) . . ?
Ag1 Ag23 Ag26 64.71(5) . . ?
Ag28 Ag23 Ag26 125.79(6) . . ?
Ag16 Ag23 Ag26 109.48(6) . . ?
Ag18 Ag23 Ag26 157.29(6) . . ?
Ag27 Ag23 Ag26 135.62(7) . . ?
Ag25 Ag23 Ag26 60.18(4) . . ?
Ag22 Ag23 Ag24 65.10(5) . . ?
Ag1 Ag23 Ag24 124.53(6) . . ?
Ag28 Ag23 Ag24 93.82(6) . . ?
Ag16 Ag23 Ag24 133.54(6) . . ?
Ag18 Ag23 Ag24 109.41(6) . . ?
Ag27 Ag23 Ag24 158.51(7) . . ?
Ag25 Ag23 Ag24 60.11(4) . . ?
Ag26 Ag23 Ag24 59.84(5) . . ?
Ag22 Ag23 Ag3 178.72(7) . . ?
Ag1 Ag23 Ag3 62.60(5) . . ?
Ag28 Ag23 Ag3 59.60(5) . . ?
Ag16 Ag23 Ag3 108.99(6) . . ?
Ag18 Ag23 Ag3 114.35(6) . . ?
Ag27 Ag23 Ag3 59.24(5) . . ?
Ag25 Ag23 Ag3 55.08(4) . . ?
Ag26 Ag23 Ag3 88.15(5) . . ?
Ag24 Ag23 Ag3 115.18(6) . . ?
Ag22 Ag23 Ag21 58.87(5) . . ?
Ag1 Ag23 Ag21 177.16(6) . . ?
Ag28 Ag23 Ag21 62.75(5) . . ?
Ag16 Ag23 Ag21 113.25(6) . . ?
Ag18 Ag23 Ag21 58.38(5) . . ?
Ag27 Ag23 Ag21 108.52(6) . . ?
Ag25 Ag23 Ag21 87.85(5) . . ?
Ag26 Ag23 Ag21 114.07(6) . . ?
Ag24 Ag23 Ag21 54.26(5) . . ?
Ag3 Ag23 Ag21 120.16(6) . . ?
Ag22 Ag23 Ag17 61.72(5) . . ?
Ag1 Ag23 Ag17 58.92(5) . . ?
Ag28 Ag23 Ag17 179.00(7) . . ?
Ag16 Ag23 Ag17 58.47(5) . . ?
Ag18 Ag23 Ag17 108.30(6) . . ?
Ag27 Ag23 Ag17 114.19(6) . . ?
Ag25 Ag23 Ag17 114.22(6) . . ?
Ag26 Ag23 Ag17 54.05(4) . . ?
Ag24 Ag23 Ag17 86.89(5) . . ?
Ag3 Ag23 Ag17 119.45(6) . . ?
Ag21 Ag23 Ag17 118.25(6) . . ?
Ag21 Ag24 Ag19 118.56(6) . . ?
Ag21 Ag24 Ag9 118.72(6) . . ?
Ag19 Ag24 Ag9 119.61(6) . . ?
Ag21 Ag24 Ag20 66.55(5) . . ?
Ag19 Ag24 Ag20 68.59(6) . . ?
Ag9 Ag24 Ag20 120.82(7) . . ?
Ag21 Ag24 Ag14 68.86(6) . . ?
Ag19 Ag24 Ag14 120.34(7) . . ?
Ag9 Ag24 Ag14 66.75(5) . . ?
Ag20 Ag24 Ag14 61.92(5) . . ?
Ag21 Ag24 Ag13 119.28(7) . . ?
Ag19 Ag24 Ag13 66.60(5) . . ?
Ag9 Ag24 Ag13 70.27(5) . . ?
Ag20 Ag24 Ag13 60.69(5) . . ?
Ag14 Ag24 Ag13 61.35(6) . . ?
Ag21 Ag24 Ag26 125.64(6) . . ?
Ag19 Ag24 Ag26 66.08(5) . . ?
Ag9 Ag24 Ag26 94.55(6) . . ?
Ag20 Ag24 Ag26 132.24(6) . . ?
Ag14 Ag24 Ag26 161.18(6) . . ?
Ag13 Ag24 Ag26 111.70(6) . . ?
Ag21 Ag24 Ag23 65.59(5) . . ?
Ag19 Ag24 Ag23 94.77(6) . . ?
Ag9 Ag24 Ag23 125.20(6) . . ?
Ag20 Ag24 Ag23 110.64(6) . . ?
Ag14 Ag24 Ag23 131.94(6) . . ?
Ag13 Ag24 Ag23 161.08(7) . . ?
Ag26 Ag24 Ag23 60.08(5) . . ?
Ag21 Ag24 Ag25 94.40(6) . . ?
Ag19 Ag24 Ag25 126.26(7) . . ?
Ag9 Ag24 Ag25 65.33(5) . . ?
Ag20 Ag24 Ag25 160.82(7) . . ?
Ag14 Ag24 Ag25 110.43(6) . . ?
Ag13 Ag24 Ag25 133.45(6) . . ?
Ag26 Ag24 Ag25 60.19(5) . . ?
Ag23 Ag24 Ag25 59.90(4) . . ?
Ag21 Ag24 Ag12 177.55(7) . . ?
Ag19 Ag24 Ag12 59.39(5) . . ?
Ag9 Ag24 Ag12 62.78(5) . . ?
Ag20 Ag24 Ag12 111.07(6) . . ?
Ag14 Ag24 Ag12 110.75(6) . . ?
Ag13 Ag24 Ag12 59.00(5) . . ?
Ag26 Ag24 Ag12 55.33(5) . . ?
Ag23 Ag24 Ag12 115.41(6) . . ?
Ag25 Ag24 Ag12 88.01(5) . . ?
Ag21 Ag24 Ag22 59.15(5) . . ?
Ag19 Ag24 Ag22 62.35(5) . . ?
Ag9 Ag24 Ag22 177.86(7) . . ?
Ag20 Ag24 Ag22 58.63(5) . . ?
Ag14 Ag24 Ag22 111.68(6) . . ?
Ag13 Ag24 Ag22 110.43(6) . . ?
Ag26 Ag24 Ag22 87.07(5) . . ?
Ag23 Ag24 Ag22 54.56(4) . . ?
Ag25 Ag24 Ag22 114.46(6) . . ?
Ag12 Ag24 Ag22 119.35(6) . . ?
Ag21 Ag24 Ag7 62.37(5) . . ?
Ag19 Ag24 Ag7 178.29(6) . . ?
Ag9 Ag24 Ag7 59.04(5) . . ?
Ag20 Ag24 Ag7 111.02(6) . . ?
Ag14 Ag24 Ag7 58.39(5) . . ?
Ag13 Ag24 Ag7 111.72(6) . . ?
Ag26 Ag24 Ag7 114.72(6) . . ?
Ag23 Ag24 Ag7 86.92(5) . . ?
Ag25 Ag24 Ag7 54.53(5) . . ?
Ag12 Ag24 Ag7 119.64(6) . . ?
Ag22 Ag24 Ag7 118.99(6) . . ?
Ag10 Ag25 Ag7 119.54(6) . . ?
Ag10 Ag25 Ag3 120.04(7) . . ?
Ag7 Ag25 Ag3 118.32(6) . . ?
Ag10 Ag25 Ag5 121.09(6) . . ?
Ag7 Ag25 Ag5 71.50(6) . . ?
Ag3 Ag25 Ag5 65.70(5) . . ?
Ag10 Ag25 Ag6 72.37(5) . . ?
Ag7 Ag25 Ag6 65.26(5) . . ?
Ag3 Ag25 Ag6 121.30(6) . . ?
Ag5 Ag25 Ag6 61.10(5) . . ?
Ag10 Ag25 Ag4 65.63(5) . . ?
Ag7 Ag25 Ag4 120.65(6) . . ?
Ag3 Ag25 Ag4 72.85(6) . . ?
Ag5 Ag25 Ag4 61.42(5) . . ?
Ag6 Ag25 Ag4 61.41(5) . . ?
Ag10 Ag25 Ag23 125.08(6) . . ?
Ag7 Ag25 Ag23 93.25(6) . . ?
Ag3 Ag25 Ag23 64.38(5) . . ?
Ag5 Ag25 Ag23 110.17(6) . . ?
Ag6 Ag25 Ag23 158.20(7) . . ?
Ag4 Ag25 Ag23 134.71(7) . . ?
Ag10 Ag25 Ag24 93.26(5) . . ?
Ag7 Ag25 Ag24 65.38(5) . . ?
Ag3 Ag25 Ag24 124.36(6) . . ?
Ag5 Ag25 Ag24 134.45(7) . . ?
Ag6 Ag25 Ag24 110.24(6) . . ?
Ag4 Ag25 Ag24 158.57(7) . . ?
Ag23 Ag25 Ag24 59.99(4) . . ?
Ag10 Ag25 Ag26 65.13(5) . . ?
Ag7 Ag25 Ag26 125.10(6) . . ?
Ag3 Ag25 Ag26 93.46(6) . . ?
Ag5 Ag25 Ag26 158.86(7) . . ?
Ag6 Ag25 Ag26 134.91(6) . . ?
Ag4 Ag25 Ag26 110.62(6) . . ?
Ag23 Ag25 Ag26 59.95(4) . . ?
Ag24 Ag25 Ag26 59.72(5) . . ?
Ag10 Ag25 Ag2 59.45(5) . . ?
Ag7 Ag25 Ag2 178.93(7) . . ?
Ag3 Ag25 Ag2 62.55(5) . . ?
Ag5 Ag25 Ag2 108.63(6) . . ?
Ag6 Ag25 Ag2 113.82(6) . . ?
Ag4 Ag25 Ag2 58.80(5) . . ?
Ag23 Ag25 Ag2 87.70(5) . . ?
Ag24 Ag25 Ag2 114.77(6) . . ?
Ag26 Ag25 Ag2 55.05(5) . . ?
Ag10 Ag25 Ag9 62.59(5) . . ?
Ag7 Ag25 Ag9 59.08(5) . . ?
Ag3 Ag25 Ag9 177.36(7) . . ?
Ag5 Ag25 Ag9 112.99(6) . . ?
Ag6 Ag25 Ag9 58.62(5) . . ?
Ag4 Ag25 Ag9 108.71(6) . . ?
Ag23 Ag25 Ag9 114.64(6) . . ?
Ag24 Ag25 Ag9 54.67(4) . . ?
Ag26 Ag25 Ag9 87.97(5) . . ?
Ag2 Ag25 Ag9 120.05(6) . . ?
Ag10 Ag25 Ag28 178.97(8) . . ?
Ag7 Ag25 Ag28 61.48(5) . . ?
Ag3 Ag25 Ag28 58.94(5) . . ?
Ag5 Ag25 Ag28 58.83(5) . . ?
Ag6 Ag25 Ag28 108.20(6) . . ?
Ag4 Ag25 Ag28 113.82(6) . . ?
Ag23 Ag25 Ag28 54.59(4) . . ?
Ag24 Ag25 Ag28 87.35(5) . . ?
Ag26 Ag25 Ag28 114.55(5) . . ?
Ag2 Ag25 Ag28 119.54(6) . . ?
Ag9 Ag25 Ag28 118.43(6) . . ?
Ag17 Ag26 Ag2 119.82(6) . . ?
Ag17 Ag26 Ag12 118.71(6) . . ?
Ag2 Ag26 Ag12 119.31(6) . . ?
Ag17 Ag26 Ag8 71.13(5) . . ?
Ag2 Ag26 Ag8 121.76(7) . . ?
Ag12 Ag26 Ag8 65.58(5) . . ?
Ag17 Ag26 Ag11 120.56(7) . . ?
Ag2 Ag26 Ag11 65.81(5) . . ?
Ag12 Ag26 Ag11 72.19(6) . . ?
Ag8 Ag26 Ag11 61.79(5) . . ?
Ag17 Ag26 Ag15 65.28(5) . . ?
Ag2 Ag26 Ag15 72.26(6) . . ?
Ag12 Ag26 Ag15 121.47(6) . . ?
Ag8 Ag26 Ag15 61.92(5) . . ?
Ag11 Ag26 Ag15 61.64(5) . . ?
Ag17 Ag26 Ag24 94.03(6) . . ?
Ag2 Ag26 Ag24 124.42(6) . . ?
Ag12 Ag26 Ag24 64.38(5) . . ?
Ag8 Ag26 Ag24 109.88(6) . . ?
Ag11 Ag26 Ag24 133.98(6) . . ?
Ag15 Ag26 Ag24 159.06(6) . . ?
Ag17 Ag26 Ag23 66.06(5) . . ?
Ag2 Ag26 Ag23 93.08(5) . . ?
Ag12 Ag26 Ag23 124.46(7) . . ?
Ag8 Ag26 Ag23 134.55(6) . . ?
Ag11 Ag26 Ag23 158.65(7) . . ?
Ag15 Ag26 Ag23 110.42(6) . . ?
Ag24 Ag26 Ag23 60.08(5) . . ?
Ag17 Ag26 Ag25 125.92(6) . . ?
Ag2 Ag26 Ag25 64.34(5) . . ?
Ag12 Ag26 Ag25 93.21(5) . . ?
Ag8 Ag26 Ag25 158.50(6) . . ?
Ag11 Ag26 Ag25 109.88(6) . . ?
Ag15 Ag26 Ag25 134.14(6) . . ?
Ag24 Ag26 Ag25 60.09(5) . . ?
Ag23 Ag26 Ag25 59.87(4) . . ?
Ag17 Ag26 Ag1 59.71(5) . . ?
Ag2 Ag26 Ag1 62.30(5) . . ?
Ag12 Ag26 Ag1 178.39(6) . . ?
Ag8 Ag26 Ag1 113.62(6) . . ?
Ag11 Ag26 Ag1 108.78(6) . . ?
Ag15 Ag26 Ag1 58.51(5) . . ?
Ag24 Ag26 Ag1 115.01(6) . . ?
Ag23 Ag26 Ag1 54.94(5) . . ?
Ag25 Ag26 Ag1 87.67(5) . . ?
Ag17 Ag26 Ag10 178.64(8) . . ?
Ag2 Ag26 Ag10 58.97(5) . . ?
Ag12 Ag26 Ag10 62.27(5) . . ?
Ag8 Ag26 Ag10 108.84(6) . . ?
Ag11 Ag26 Ag10 58.59(5) . . ?
Ag15 Ag26 Ag10 113.46(6) . . ?
Ag24 Ag26 Ag10 87.26(5) . . ?
Ag23 Ag26 Ag10 114.31(6) . . ?
Ag25 Ag26 Ag10 54.45(4) . . ?
Ag1 Ag26 Ag10 119.31(6) . . ?
Ag17 Ag26 Ag19 62.53(5) . . ?
Ag2 Ag26 Ag19 177.65(6) . . ?
Ag12 Ag26 Ag19 58.45(5) . . ?
Ag8 Ag26 Ag19 58.49(5) . . ?
Ag11 Ag26 Ag19 113.30(6) . . ?
Ag15 Ag26 Ag19 109.38(6) . . ?
Ag24 Ag26 Ag19 54.42(4) . . ?
Ag23 Ag26 Ag19 87.92(5) . . ?
Ag25 Ag26 Ag19 114.49(6) . . ?
Ag1 Ag26 Ag19 119.95(6) . . ?
Ag10 Ag26 Ag19 118.67(6) . . ?
P11 Ag27 Ag23 169.78(15) . . ?
P11 Ag27 Ag18 130.33(16) . . ?
Ag23 Ag27 Ag18 59.13(5) . . ?
P11 Ag27 Ag3 106.12(14) . . ?
Ag23 Ag27 Ag3 63.76(5) . . ?
Ag18 Ag27 Ag3 116.27(6) . . ?
P11 Ag27 Ag16 127.31(14) . . ?
Ag23 Ag27 Ag16 58.86(5) . . ?
Ag18 Ag27 Ag16 59.93(5) . . ?
Ag3 Ag27 Ag16 110.15(6) . . ?
P11 Ag27 Ag28 120.84(14) . . ?
Ag23 Ag27 Ag28 56.24(5) . . ?
Ag18 Ag27 Ag28 67.65(5) . . ?
Ag3 Ag27 Ag28 58.39(5) . . ?
Ag16 Ag27 Ag28 110.49(6) . . ?
P11 Ag27 Ag1 121.96(16) . . ?
Ag23 Ag27 Ag1 52.33(5) . . ?
Ag18 Ag27 Ag1 102.79(6) . . ?
Ag3 Ag27 Ag1 57.31(5) . . ?
Ag16 Ag27 Ag1 57.28(5) . . ?
Ag28 Ag27 Ag1 97.57(5) . . ?
O6 Ag28 Ag23 150.9(3) . . ?
O6 Ag28 Ag3 142.3(3) . . ?
Ag23 Ag28 Ag3 64.86(5) . . ?
O6 Ag28 Ag5 94.1(3) . . ?
Ag23 Ag28 Ag5 112.54(6) . . ?
Ag3 Ag28 Ag5 62.96(5) . . ?
O6 Ag28 Ag7 88.1(4) . . ?
Ag23 Ag28 Ag7 91.61(6) . . ?
Ag3 Ag28 Ag7 107.02(6) . . ?
Ag5 Ag28 Ag7 66.97(5) . . ?
O6 Ag28 Ag27 119.6(3) . . ?
Ag23 Ag28 Ag27 58.60(5) . . ?
Ag3 Ag28 Ag27 58.91(5) . . ?
Ag5 Ag28 Ag27 117.96(7) . . ?
Ag7 Ag28 Ag27 149.93(7) . . ?
O6 Ag28 Ag21 91.5(3) . . ?
Ag23 Ag28 Ag21 63.69(5) . . ?
Ag3 Ag28 Ag21 126.07(6) . . ?
Ag5 Ag28 Ag21 126.45(6) . . ?
Ag7 Ag28 Ag21 60.03(5) . . ?
Ag27 Ag28 Ag21 104.65(6) . . ?
O6 Ag28 Ag25 137.3(3) . . ?
Ag23 Ag28 Ag25 59.79(5) . . ?
Ag3 Ag28 Ag25 54.85(5) . . ?
Ag5 Ag28 Ag25 56.15(5) . . ?
Ag7 Ag28 Ag25 53.85(5) . . ?
Ag27 Ag28 Ag25 102.24(6) . . ?
Ag21 Ag28 Ag25 85.53(5) . . ?
O6 Ag28 Ag18 99.0(3) . . ?
Ag23 Ag28 Ag18 54.86(5) . . ?
Ag3 Ag28 Ag18 105.51(6) . . ?
Ag5 Ag28 Ag18 166.96(7) . . ?
Ag7 Ag28 Ag18 113.71(6) . . ?
Ag27 Ag28 Ag18 54.44(5) . . ?
Ag21 Ag28 Ag18 54.01(4) . . ?
Ag25 Ag28 Ag18 112.90(6) . . ?
O6 Ag28 Mo2 30.4(3) . . ?
Ag23 Ag28 Mo2 127.31(7) . . ?
Ag3 Ag28 Mo2 163.27(7) . . ?
Ag5 Ag28 Mo2 100.35(6) . . ?
Ag7 Ag28 Mo2 64.33(5) . . ?
Ag27 Ag28 Mo2 135.58(7) . . ?
Ag21 Ag28 Mo2 63.69(5) . . ?
Ag25 Ag28 Mo2 118.17(6) . . ?
Ag18 Ag28 Mo2 91.21(6) . . ?
O14 Mo1 O13 108.9(6) . . ?
O14 Mo1 O15 110.5(7) . . ?
O13 Mo1 O15 110.4(6) . . ?
O14 Mo1 O2 107.1(6) . . ?
O13 Mo1 O2 109.8(6) . . ?
O15 Mo1 O2 110.1(6) . . ?
O7 Mo2 O8 112.2(7) . . ?
O7 Mo2 O6 107.8(6) . . ?
O8 Mo2 O6 110.6(7) . . ?
O7 Mo2 O4 109.5(6) . . ?
O8 Mo2 O4 109.8(6) . . ?
O6 Mo2 O4 106.7(6) . . ?
O7 Mo2 Ag28 87.5(4) . . ?
O8 Mo2 Ag28 148.9(6) . . ?
O6 Mo2 Ag28 38.5(4) . . ?
O4 Mo2 Ag28 83.8(4) . . ?
O16 Mo3 O18 109.6(7) . . ?
O16 Mo3 O5 108.0(6) . . ?
O18 Mo3 O5 111.2(7) . . ?
O16 Mo3 O17 108.3(6) . . ?
O18 Mo3 O17 111.4(6) . . ?
O5 Mo3 O17 108.3(5) . . ?
O12 Mo4 O10 111.4(6) . . ?
O12 Mo4 O11 108.9(7) . . ?
O10 Mo4 O11 108.2(6) . . ?
O12 Mo4 O9 111.6(6) . . ?
O10 Mo4 O9 107.7(6) . . ?
O11 Mo4 O9 109.0(6) . . ?
O12 Mo4 Ag22 148.0(5) . . ?
O10 Mo4 Ag22 87.2(4) . . ?
O11 Mo4 Ag22 39.1(4) . . ?
O9 Mo4 Ag22 85.3(4) . . ?
C32 P1 C135 102.2(12) . . ?
C32 P1 C33 105.3(12) . . ?
C135 P1 C33 106.2(10) . . ?
C32 P1 Ag20 115.6(9) . . ?
C135 P1 Ag20 109.0(8) . . ?
C33 P1 Ag20 117.3(8) . . ?
C45 P2 C39 105.3(12) . . ?
C45 P2 C3 106.8(12) . . ?
C39 P2 C3 106.5(10) . . ?
C45 P2 Ag6 110.6(8) . . ?
C39 P2 Ag6 115.5(8) . . ?
C3 P2 Ag6 111.6(9) . . ?
C117 P3 C7 104.6(9) . . ?
C117 P3 C116 106.2(11) . . ?
C7 P3 C116 103.7(11) . . ?
C117 P3 Ag4 112.9(8) . . ?
C7 P3 Ag4 115.1(8) . . ?
C116 P3 Ag4 113.4(8) . . ?
C113 P4 C103 106.2(13) . . ?
C113 P4 C35 105.4(12) . . ?
C103 P4 C35 104.2(10) . . ?
C113 P4 Ag11 112.1(10) . . ?
C103 P4 Ag11 115.5(8) . . ?
C35 P4 Ag11 112.5(9) . . ?
C127 P5 C8 105.6(10) . . ?
C127 P5 C132 107.2(11) . . ?
C8 P5 C132 103.1(10) . . ?
C127 P5 Ag18 110.6(8) . . ?
C8 P5 Ag18 112.9(7) . . ?
C132 P5 Ag18 116.6(8) . . ?
C97 P7 C91 102.4(10) . . ?
C97 P7 C92 105.8(10) . . ?
C91 P7 C92 105.0(11) . . ?
C97 P7 Ag15 112.4(8) . . ?
C91 P7 Ag15 116.7(8) . . ?
C92 P7 Ag15 113.4(8) . . ?
C85 P8 C28 105.0(11) . . ?
C85 P8 C89 106.8(11) . . ?
C28 P8 C89 104.7(11) . . ?
C85 P8 Ag16 114.4(10) . . ?
C28 P8 Ag16 115.6(8) . . ?
C89 P8 Ag16 109.6(7) . . ?
C167 P9 C157 107.7(11) . . ?
C167 P9 C34 104.7(11) . . ?
C157 P9 C34 103.5(11) . . ?
C167 P9 Ag13 115.5(8) . . ?
C157 P9 Ag13 110.7(8) . . ?
C34 P9 Ag13 113.8(7) . . ?
C150 P10 C144 105.2(10) . . ?
C150 P10 C155 107.4(11) . . ?
C144 P10 C155 104.4(10) . . ?
C150 P10 Ag8 113.2(8) . . ?
C144 P10 Ag8 115.1(7) . . ?
C155 P10 Ag8 110.8(7) . . ?
C71 P11 C30 105.7(10) . . ?
C71 P11 C70 106.8(10) . . ?
C30 P11 C70 102.4(10) . . ?
C71 P11 Ag27 112.6(7) . . ?
C30 P11 Ag27 114.5(7) . . ?
C70 P11 Ag27 113.8(8) . . ?
C61 P12 C55 105.8(10) . . ?
C61 P12 C67 104.1(11) . . ?
C55 P12 C67 106.0(12) . . ?
C61 P12 Ag5 117.6(7) . . ?
C55 P12 Ag5 114.0(7) . . ?
C67 P12 Ag5 108.4(9) . . ?
C13 P6 C49 103.6(11) . . ?
C13 P6 C48 104.7(12) . . ?
C49 P6 C48 104.9(12) . . ?
C13 P6 Ag14 117.5(8) . . ?
C49 P6 Ag14 113.0(8) . . ?
C48 P6 Ag14 111.9(9) . . ?
Mo1 O2 Ag10 111.2(6) . . ?
Mo2 O4 Ag21 109.9(6) . . ?
Mo3 O5 Ag3 111.1(5) . . ?
Mo2 O6 Ag28 111.1(6) . . ?
Mo2 O7 Ag7 113.4(6) . . ?
Mo4 O9 Ag17 110.3(7) . . ?
Mo4 O10 Ag19 113.5(5) . . ?
Mo4 O11 Ag22 110.3(6) . . ?
Mo1 O13 Ag12 110.9(6) . . ?
Mo1 O14 Ag9 111.0(5) . . ?
Mo3 O16 Ag2 111.4(6) . . ?
Mo3 O17 Ag1 110.8(6) . . ?
C19 C3 C36 120(3) . . ?
C19 C3 P2 118(2) . . ?
C36 C3 P2 121(2) . . ?
O1 C6 H6A 109.5 . . ?
O1 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
O1 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C173 C7 C169 118(2) . . ?
C173 C7 P3 125.9(19) . . ?
C169 C7 P3 116.1(16) . . ?
C9 C8 C126 119(2) . . ?
C9 C8 P5 118.5(16) . . ?
C126 C8 P5 122.3(18) . . ?
C123 C9 C8 124(2) . . ?
C123 C9 H9 118.0 . . ?
C8 C9 H9 118.0 . . ?
C92 C10 C93 123(2) . . ?
C92 C10 H10 118.6 . . ?
C93 C10 H10 118.6 . . ?
C105 C11 C104 119(3) . . ?
C105 C11 H11 120.5 . . ?
C104 C11 H11 120.5 . . ?
C156 C12 C157 112(2) . . ?
C156 C12 H12A 109.2 . . ?
C157 C12 H12A 109.2 . . ?
C156 C12 H12B 109.2 . . ?
C157 C12 H12B 109.2 . . ?
H12A C12 H12B 107.9 . . ?
C31 C15 C137 121(3) . . ?
C31 C15 H15 119.3 . . ?
C137 C15 H15 119.3 . . ?
O19 C16 H16A 109.5 . . ?
O19 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
O19 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
O20 C17 H17A 109.5 . . ?
O20 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
O20 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C22 C19 C3 115(3) . . ?
C22 C19 H19 122.5 . . ?
C3 C19 H19 122.5 . . ?
O21 C20 H20A 109.5 . . ?
O21 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
O21 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
C23 C22 C19 125(3) . . ?
C23 C22 H22 117.6 . . ?
C19 C22 H22 117.6 . . ?
C22 C23 C24 119(3) . . ?
C22 C23 H23 120.6 . . ?
C24 C23 H23 120.6 . . ?
C36 C24 C23 120(3) . . ?
C36 C24 H24 120.1 . . ?
C23 C24 H24 120.1 . . ?
C90 C25 C89 115(2) . . ?
C90 C25 H25A 108.6 . . ?
C89 C25 H25A 108.6 . . ?
C90 C25 H25B 108.6 . . ?
C89 C25 H25B 108.6 . . ?
H25A C25 H25B 107.5 . . ?
C85 C26 C37 119(3) . . ?
C85 C26 H26 120.3 . . ?
C37 C26 H26 120.3 . . ?
C82 C27 C81 119(2) . . ?
C82 C27 H27 120.6 . . ?
C81 C27 H27 120.6 . . ?
C84 C28 C81 123(2) . . ?
C84 C28 P8 120.5(19) . . ?
C81 C28 P8 116.2(17) . . ?
C73 C29 C72 115(2) . . ?
C73 C29 H29 122.4 . . ?
C72 C29 H29 122.4 . . ?
C50 C49 C14 120.0 . . ?
C50 C49 P6 116.1(14) . . ?
C14 C49 P6 123.8(14) . . ?
C51 C50 C49 120.0 . . ?
C51 C50 H50 120.0 . . ?
C49 C50 H50 120.0 . . ?
C50 C51 C52 120.0 . . ?
C50 C51 H51 120.0 . . ?
C52 C51 H51 120.0 . . ?
C51 C52 C2 120.0 . . ?
C51 C52 H52 120.0 . . ?
C2 C52 H52 120.0 . . ?
C14 C2 C52 120.0 . . ?
C14 C2 H2 120.0 . . ?
C52 C2 H2 120.0 . . ?
C2 C14 C49 120.0 . . ?
C2 C14 H14 120.0 . . ?
C49 C14 H14 120.0 . . ?
C76 C30 C80 114(2) . . ?
C76 C30 P11 121.2(17) . . ?
C80 C30 P11 124.3(17) . . ?
C15 C31 C138 122(3) . . ?
C15 C31 H31 119.1 . . ?
C138 C31 H31 119.1 . . ?
C138 C32 C136 121(3) . . ?
C138 C32 P1 119(2) . . ?
C136 C32 P1 120(2) . . ?
C139 C33 C143 118(2) . . ?
C139 C33 P1 120.2(19) . . ?
C143 C33 P1 121.6(17) . . ?
C162 C34 C158 119(2) . . ?
C162 C34 P9 118.0(16) . . ?
C158 C34 P9 122.6(16) . . ?
C108 C35 C112 121(2) . . ?
C108 C35 P4 121.3(18) . . ?
C112 C35 P4 117.8(19) . . ?
C24 C36 C3 119(3) . . ?
C24 C36 H36 120.3 . . ?
C3 C36 H36 120.3 . . ?
C88 C37 C26 123(3) . . ?
C88 C37 H37 118.3 . . ?
C26 C37 H37 118.3 . . ?
C152 C38 C153 121(3) . . ?
C152 C38 H38 119.7 . . ?
C153 C38 H38 119.7 . . ?
C44 C39 C40 115(2) . . ?
C44 C39 P2 121.8(18) . . ?
C40 C39 P2 123.6(19) . . ?
C41 C40 C39 127(3) . . ?
C41 C40 H40 116.4 . . ?
C39 C40 H40 116.4 . . ?
C42 C41 C40 114(3) . . ?
C42 C41 H41 122.8 . . ?
C40 C41 H41 122.8 . . ?
C41 C42 C43 125(3) . . ?
C41 C42 H42 117.6 . . ?
C43 C42 H42 117.6 . . ?
C44 C43 C42 115(3) . . ?
C44 C43 H43 122.7 . . ?
C42 C43 H43 122.7 . . ?
C43 C44 C39 122(2) . . ?
C43 C44 H44 118.8 . . ?
C39 C44 H44 118.8 . . ?
C46 C45 P2 115.5(18) . . ?
C46 C45 H45A 108.4 . . ?
P2 C45 H45A 108.4 . . ?
C46 C45 H45B 108.4 . . ?
P2 C45 H45B 108.4 . . ?
H45A C45 H45B 107.5 . . ?
C47 C46 C45 121(2) . . ?
C47 C46 H46A 107.1 . . ?
C45 C46 H46A 107.1 . . ?
C47 C46 H46B 107.1 . . ?
C45 C46 H46B 107.1 . . ?
H46A C46 H46B 106.8 . . ?
C46 C47 C48 117(2) . . ?
C46 C47 H47A 108.0 . . ?
C48 C47 H47A 108.0 . . ?
C46 C47 H47B 108.0 . . ?
C48 C47 H47B 108.0 . . ?
H47A C47 H47B 107.2 . . ?
C47 C48 P6 110.4(19) . . ?
C47 C48 H48A 109.6 . . ?
P6 C48 H48A 109.6 . . ?
C47 C48 H48B 109.6 . . ?
P6 C48 H48B 109.6 . . ?
H48A C48 H48B 108.1 . . ?
C56 C55 C60 118(2) . . ?
C56 C55 P12 122.3(19) . . ?
C60 C55 P12 119.8(16) . . ?
C55 C56 C57 118(2) . . ?
C55 C56 H56 121.0 . . ?
C57 C56 H56 121.0 . . ?
C58 C57 C56 121(2) . . ?
C58 C57 H57A 107.1 . . ?
C56 C57 H57A 107.1 . . ?
C58 C57 H57B 107.1 . . ?
C56 C57 H57B 107.1 . . ?
H57A C57 H57B 106.8 . . ?
C57 C58 C59 120(3) . . ?
C57 C58 H58A 107.4 . . ?
C59 C58 H58A 107.4 . . ?
C57 C58 H58B 107.4 . . ?
C59 C58 H58B 107.4 . . ?
H58A C58 H58B 106.9 . . ?
C60 C59 C58 120(3) . . ?
C60 C59 H59 120.2 . . ?
C58 C59 H59 120.2 . . ?
C59 C60 C55 124(2) . . ?
C59 C60 H60 118.1 . . ?
C55 C60 H60 118.1 . . ?
C62 C61 C66 117.1(19) . . ?
C62 C61 P12 124.0(17) . . ?
C66 C61 P12 118.6(14) . . ?
C61 C62 C63 122(2) . . ?
C61 C62 H62 119.0 . . ?
C63 C62 H62 119.0 . . ?
C64 C63 C62 115(2) . . ?
C64 C63 H63 122.3 . . ?
C62 C63 H63 122.3 . . ?
C63 C64 C65 127(2) . . ?
C63 C64 H64 116.6 . . ?
C65 C64 H64 116.6 . . ?
C66 C65 C64 117(2) . . ?
C66 C65 H65 121.5 . . ?
C64 C65 H65 121.5 . . ?
C65 C66 C61 121(2) . . ?
C65 C66 H66 119.3 . . ?
C61 C66 H66 119.3 . . ?
C68 C67 P12 109.0(17) . . ?
C68 C67 H67A 109.9 . . ?
P12 C67 H67A 109.9 . . ?
C68 C67 H67B 109.9 . . ?
P12 C67 H67B 109.9 . . ?
H67A C67 H67B 108.3 . . ?
C69 C68 C67 112(2) . . ?
C69 C68 H68A 109.1 . . ?
C67 C68 H68A 109.1 . . ?
C69 C68 H68B 109.1 . . ?
C67 C68 H68B 109.1 . . ?
H68A C68 H68B 107.9 . . ?
O3 C068 H06A 109.5 . . ?
O3 C068 H06B 109.5 . . ?
H06A C068 H06B 109.5 . . ?
O3 C068 H06C 109.5 . . ?
H06A C068 H06C 109.5 . . ?
H06B C068 H06C 109.5 . . ?
C68 C69 C70 113(2) . . ?
C68 C69 H69A 109.1 . . ?
C70 C69 H69A 109.1 . . ?
C68 C69 H69B 109.1 . . ?
C70 C69 H69B 109.1 . . ?
H69A C69 H69B 107.8 . . ?
C69 C70 P11 113.6(17) . . ?
C69 C70 H70A 108.8 . . ?
P11 C70 H70A 108.8 . . ?
C69 C70 H70B 108.8 . . ?
P11 C70 H70B 108.8 . . ?
H70A C70 H70B 107.7 . . ?
C72 C71 C75 114(2) . . ?
C72 C71 P11 122.7(17) . . ?
C75 C71 P11 123.1(17) . . ?
C71 C72 C29 122(2) . . ?
C71 C72 H72 118.9 . . ?
C29 C72 H72 118.9 . . ?
C74 C73 C29 122(3) . . ?
C74 C73 H73 119.0 . . ?
C29 C73 H73 119.0 . . ?
C75 C74 C73 120(3) . . ?
C75 C74 H74 120.0 . . ?
C73 C74 H74 120.0 . . ?
C74 C75 C71 126(2) . . ?
C74 C75 H75 117.0 . . ?
C71 C75 H75 117.0 . . ?
C30 C76 C77 127(2) . . ?
C30 C76 H76 116.7 . . ?
C77 C76 H76 116.7 . . ?
C76 C77 C78 114(2) . . ?
C76 C77 H77 122.9 . . ?
C78 C77 H77 122.9 . . ?
C79 C78 C77 122(2) . . ?
C79 C78 H78 118.9 . . ?
C77 C78 H78 118.9 . . ?
C78 C79 C80 118(2) . . ?
C78 C79 H79 121.1 . . ?
C80 C79 H79 121.1 . . ?
C79 C80 C30 124(2) . . ?
C79 C80 H80 117.8 . . ?
C30 C80 H80 117.8 . . ?
C28 C81 C27 116(2) . . ?
C28 C81 H81 122.0 . . ?
C27 C81 H81 122.0 . . ?
C27 C82 C83 128(3) . . ?
C27 C82 H82 115.8 . . ?
C83 C82 H82 115.8 . . ?
C82 C83 C84 113(2) . . ?
C82 C83 H83 123.7 . . ?
C84 C83 H83 123.7 . . ?
C28 C84 C83 120(2) . . ?
C28 C84 H84 120.1 . . ?
C83 C84 H84 120.1 . . ?
C26 C85 C86 119(3) . . ?
C26 C85 P8 123(2) . . ?
C86 C85 P8 118(2) . . ?
C87 C86 C85 115(3) . . ?
C87 C86 H86 122.5 . . ?
C85 C86 H86 122.5 . . ?
C88 C87 C86 124(3) . . ?
C88 C87 H87 118.1 . . ?
C86 C87 H87 118.1 . . ?
C87 C88 C37 118(3) . . ?
C87 C88 H88 120.9 . . ?
C37 C88 H88 120.9 . . ?
C25 C89 P8 110.9(15) . . ?
C25 C89 H89A 109.5 . . ?
P8 C89 H89A 109.5 . . ?
C25 C89 H89B 109.5 . . ?
P8 C89 H89B 109.5 . . ?
H89A C89 H89B 108.1 . . ?
C25 C90 C91 116(2) . . ?
C25 C90 H90A 108.2 . . ?
C91 C90 H90A 108.2 . . ?
C25 C90 H90B 108.2 . . ?
C91 C90 H90B 108.2 . . ?
H90A C90 H90B 107.4 . . ?
C90 C91 P7 114.2(17) . . ?
C90 C91 H91A 108.7 . . ?
P7 C91 H91A 108.7 . . ?
C90 C91 H91B 108.7 . . ?
P7 C91 H91B 108.7 . . ?
H91A C91 H91B 107.6 . . ?
C96 C92 C10 121(2) . . ?
C96 C92 P7 116.6(17) . . ?
C10 C92 P7 122.7(18) . . ?
C94 C93 C10 115(2) . . ?
C94 C93 H93 122.3 . . ?
C10 C93 H93 122.3 . . ?
C95 C94 C93 123(2) . . ?
C95 C94 H94 118.3 . . ?
C93 C94 H94 118.3 . . ?
C94 C95 C96 118(2) . . ?
C94 C95 H95 121.2 . . ?
C96 C95 H95 121.2 . . ?
C92 C96 C95 120(2) . . ?
C92 C96 H96 120.0 . . ?
C95 C96 H96 120.0 . . ?
C98 C97 C102 118(2) . . ?
C98 C97 P7 121.7(18) . . ?
C102 C97 P7 120.3(18) . . ?
C97 C98 C99 121(2) . . ?
C97 C98 H98 119.6 . . ?
C99 C98 H98 119.6 . . ?
C100 C99 C98 121(2) . . ?
C100 C99 H99 119.5 . . ?
C98 C99 H99 119.5 . . ?
C99 C100 C101 119(2) . . ?
C99 C100 H100 120.4 . . ?
C101 C100 H100 120.4 . . ?
C102 C101 C100 117(2) . . ?
C102 C101 H101 121.4 . . ?
C100 C101 H101 121.4 . . ?
C101 C102 C97 123(2) . . ?
C101 C102 H102 118.4 . . ?
C97 C102 H102 118.4 . . ?
C107 C103 C104 116(2) . . ?
C107 C103 P4 123.7(19) . . ?
C104 C103 P4 120.0(18) . . ?
C11 C104 C103 124(2) . . ?
C11 C104 H104 118.2 . . ?
C103 C104 H104 118.2 . . ?
C11 C105 C106 122(3) . . ?
C11 C105 H105 118.8 . . ?
C106 C105 H105 118.8 . . ?
C105 C106 C107 117(2) . . ?
C105 C106 H106 121.5 . . ?
C107 C106 H106 121.5 . . ?
C103 C107 C106 121(2) . . ?
C103 C107 H107 119.5 . . ?
C106 C107 H107 119.5 . . ?
C109 C108 C35 121(3) . . ?
C109 C108 H108 119.4 . . ?
C35 C108 H108 119.4 . . ?
C110 C109 C108 121(3) . . ?
C110 C109 H109 119.3 . . ?
C108 C109 H109 119.3 . . ?
C111 C110 C109 125(3) . . ?
C111 C110 H110 117.5 . . ?
C109 C110 H110 117.5 . . ?
C110 C111 C112 120(3) . . ?
C110 C111 H11A 107.3 . . ?
C112 C111 H11A 107.3 . . ?
C110 C111 H11B 107.3 . . ?
C112 C111 H11B 107.3 . . ?
H11A C111 H11B 106.9 . . ?
C35 C112 C111 111(2) . . ?
C35 C112 H11C 109.5 . . ?
C111 C112 H11C 109.5 . . ?
C35 C112 H11D 109.5 . . ?
C111 C112 H11D 109.5 . . ?
H11C C112 H11D 108.1 . . ?
C114 C113 P4 107.2(18) . . ?
C114 C113 H11E 110.3 . . ?
P4 C113 H11E 110.3 . . ?
C114 C113 H11F 110.3 . . ?
P4 C113 H11F 110.3 . . ?
H11E C113 H11F 108.5 . . ?
C115 C114 C113 114(2) . . ?
C115 C114 H11G 108.7 . . ?
C113 C114 H11G 108.7 . . ?
C115 C114 H11H 108.7 . . ?
C113 C114 H11H 108.7 . . ?
H11G C114 H11H 107.6 . . ?
C114 C115 C116 115(2) . . ?
C114 C115 H11I 108.6 . . ?
C116 C115 H11I 108.6 . . ?
C114 C115 H11J 108.6 . . ?
C116 C115 H11J 108.6 . . ?
H11I C115 H11J 107.6 . . ?
C115 C116 P3 110.4(19) . . ?
C115 C116 H11K 109.6 . . ?
P3 C116 H11K 109.6 . . ?
C115 C116 H11L 109.6 . . ?
P3 C116 H11L 109.6 . . ?
H11K C116 H11L 108.1 . . ?
C118 C117 C122 115(2) . . ?
C118 C117 P3 122.9(18) . . ?
C122 C117 P3 121.4(16) . . ?
C117 C118 C119 122(2) . . ?
C117 C118 H118 118.9 . . ?
C119 C118 H118 118.9 . . ?
C118 C119 C120 117(2) . . ?
C118 C119 H11M 108.0 . . ?
C120 C119 H11M 108.0 . . ?
C118 C119 H11N 108.0 . . ?
C120 C119 H11N 108.0 . . ?
H11M C119 H11N 107.3 . . ?
C121 C120 C119 117(2) . . ?
C121 C120 H12C 108.0 . . ?
C119 C120 H12C 108.0 . . ?
C121 C120 H12D 108.0 . . ?
C119 C120 H12D 108.0 . . ?
H12C C120 H12D 107.3 . . ?
C122 C121 C120 124(2) . . ?
C122 C121 H121 118.2 . . ?
C120 C121 H121 118.2 . . ?
C121 C122 C117 124(2) . . ?
C121 C122 H122 117.8 . . ?
C117 C122 H122 117.8 . . ?
C9 C123 C124 114(2) . . ?
C9 C123 H123 123.1 . . ?
C124 C123 H123 123.1 . . ?
C125 C124 C123 127(2) . . ?
C125 C124 H124 116.7 . . ?
C123 C124 H124 116.7 . . ?
C124 C125 C126 115(2) . . ?
C124 C125 H125 122.4 . . ?
C126 C125 H125 122.4 . . ?
C8 C126 C125 121(2) . . ?
C8 C126 H126 119.6 . . ?
C125 C126 H126 119.6 . . ?
C174 C127 C128 117(2) . . ?
C174 C127 P5 122.3(19) . . ?
C128 C127 P5 120.3(18) . . ?
C127 C128 C129 119(2) . . ?
C127 C128 H128 120.3 . . ?
C129 C128 H128 120.3 . . ?
C130 C129 C128 117(2) . . ?
C130 C129 H129 121.4 . . ?
C128 C129 H129 121.4 . . ?
C129 C130 C131 120(3) . . ?
C129 C130 H130 120.0 . . ?
C131 C130 H130 120.0 . . ?
C174 C131 C130 123(3) . . ?
C174 C131 H131 118.5 . . ?
C130 C131 H131 118.5 . . ?
C133 C132 P5 112.7(18) . . ?
C133 C132 H13A 109.0 . . ?
P5 C132 H13A 109.0 . . ?
C133 C132 H13B 109.0 . . ?
P5 C132 H13B 109.0 . . ?
H13A C132 H13B 107.8 . . ?
C132 C133 C134 117(2) . . ?
C132 C133 H13C 108.0 . . ?
C134 C133 H13C 108.0 . . ?
C132 C133 H13D 108.0 . . ?
C134 C133 H13D 108.0 . . ?
H13C C133 H13D 107.2 . . ?
C133 C134 C135 114(2) . . ?
C133 C134 H13E 108.8 . . ?
C135 C134 H13E 108.8 . . ?
C133 C134 H13F 108.8 . . ?
C135 C134 H13F 108.8 . . ?
H13E C134 H13F 107.6 . . ?
C134 C135 P1 109.0(16) . . ?
C134 C135 H13G 109.9 . . ?
P1 C135 H13G 109.9 . . ?
C134 C135 H13H 109.9 . . ?
P1 C135 H13H 109.9 . . ?
H13G C135 H13H 108.3 . . ?
C32 C136 C137 117(3) . . ?
C32 C136 H136 121.6 . . ?
C137 C136 H136 121.6 . . ?
C15 C137 C136 116(3) . . ?
C15 C137 H137 122.0 . . ?
C136 C137 H137 122.0 . . ?
C32 C138 C31 120(3) . . ?
C32 C138 H138 120.1 . . ?
C31 C138 H138 120.1 . . ?
C33 C139 C140 122(2) . . ?
C33 C139 H139 118.8 . . ?
C140 C139 H139 118.8 . . ?
C141 C140 C139 117(2) . . ?
C141 C140 H140 121.3 . . ?
C139 C140 H140 121.3 . . ?
C140 C141 C142 124(2) . . ?
C140 C141 H141 118.2 . . ?
C142 C141 H141 118.2 . . ?
C141 C142 C143 118(2) . . ?
C141 C142 H142 121.1 . . ?
C143 C142 H142 121.1 . . ?
C142 C143 C33 121(2) . . ?
C142 C143 H143 119.6 . . ?
C33 C143 H143 119.6 . . ?
C145 C144 C149 122(2) . . ?
C145 C144 P10 122.2(18) . . ?
C149 C144 P10 116.2(16) . . ?
C144 C145 C146 122(2) . . ?
C144 C145 H145 118.8 . . ?
C146 C145 H145 118.8 . . ?
C145 C146 C147 118(2) . . ?
C145 C146 H146 121.0 . . ?
C147 C146 H146 121.0 . . ?
C146 C147 C148 120(2) . . ?
C146 C147 H147 119.8 . . ?
C148 C147 H147 119.8 . . ?
C149 C148 C147 117(2) . . ?
C149 C148 H148 121.3 . . ?
C147 C148 H148 121.3 . . ?
C144 C149 C148 120(2) . . ?
C144 C149 H149 120.0 . . ?
C148 C149 H149 120.0 . . ?
C154 C150 C151 120(2) . . ?
C154 C150 P10 120.4(19) . . ?
C151 C150 P10 119.5(18) . . ?
C150 C151 C152 118(2) . . ?
C150 C151 H151 121.1 . . ?
C152 C151 H151 121.1 . . ?
C38 C152 C151 118(3) . . ?
C38 C152 H152 120.8 . . ?
C151 C152 H152 120.8 . . ?
C154 C153 C38 118(3) . . ?
C154 C153 H153 121.1 . . ?
C38 C153 H153 121.1 . . ?
C153 C154 C150 125(3) . . ?
C153 C154 H154 117.6 . . ?
C150 C154 H154 117.6 . . ?
C156 C155 P10 109.8(16) . . ?
C156 C155 H15A 109.7 . . ?
P10 C155 H15A 109.7 . . ?
C156 C155 H15B 109.7 . . ?
P10 C155 H15B 109.7 . . ?
H15A C155 H15B 108.2 . . ?
C12 C156 C155 111(2) . . ?
C12 C156 H15C 109.4 . . ?
C155 C156 H15C 109.4 . . ?
C12 C156 H15D 109.4 . . ?
C155 C156 H15D 109.4 . . ?
H15C C156 H15D 108.0 . . ?
C12 C157 P9 115.4(18) . . ?
C12 C157 H15E 108.4 . . ?
P9 C157 H15E 108.4 . . ?
C12 C157 H15F 108.4 . . ?
P9 C157 H15F 108.4 . . ?
H15E C157 H15F 107.5 . . ?
C159 C158 C34 121(2) . . ?
C159 C158 H158 119.7 . . ?
C34 C158 H158 119.7 . . ?
C160 C159 C158 119(2) . . ?
C160 C159 H159 120.6 . . ?
C158 C159 H159 120.6 . . ?
C161 C160 C159 124(2) . . ?
C161 C160 H160 118.2 . . ?
C159 C160 H160 118.2 . . ?
C160 C161 C162 119(2) . . ?
C160 C161 H161 120.4 . . ?
C162 C161 H161 120.4 . . ?
C34 C162 C161 118(2) . . ?
C34 C162 H162 121.1 . . ?
C161 C162 H162 121.1 . . ?
C164 C163 C167 119(3) . . ?
C164 C163 H163 120.3 . . ?
C167 C163 H163 120.3 . . ?
C165 C164 C163 124(3) . . ?
C165 C164 H164 117.9 . . ?
C163 C164 H164 117.9 . . ?
C164 C165 C166 111(3) . . ?
C164 C165 H165 124.5 . . ?
C166 C165 H165 124.5 . . ?
C168 C166 C165 129(3) . . ?
C168 C166 H166 115.7 . . ?
C165 C166 H166 115.7 . . ?
C168 C167 C163 115(2) . . ?
C168 C167 P9 121.3(19) . . ?
C163 C167 P9 123(2) . . ?
C167 C168 C166 121(3) . . ?
C167 C168 H168 119.6 . . ?
C166 C168 H168 119.6 . . ?
C170 C169 C7 116(2) . . ?
C170 C169 H169 121.9 . . ?
C7 C169 H169 121.9 . . ?
C169 C170 C171 120(2) . . ?
C169 C170 H170 120.2 . . ?
C171 C170 H170 120.2 . . ?
C172 C171 C170 124(3) . . ?
C172 C171 H171 118.2 . . ?
C170 C171 H171 118.2 . . ?
C171 C172 C173 116(3) . . ?
C171 C172 H172 122.2 . . ?
C173 C172 H172 122.2 . . ?
C7 C173 C172 127(3) . . ?
C7 C173 H173 116.5 . . ?
C172 C173 H173 116.5 . . ?
C131 C174 C127 123(3) . . ?
C131 C174 H174 118.6 . . ?
C127 C174 H174 118.6 . . ?

_refine_diff_density_max         4.797
_refine_diff_density_min         -2.601
_refine_diff_density_rms         0.297


loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.000 0.324 -0.005 14819 5593 ' '
2 0.250 0.250 0.000 7 -1 ' '
3 0.500 0.989 0.114 14819 5593 ' '
4 0.750 0.750 0.000 7 -1 ' '
5 0.250 0.750 0.500 7 -1 ' '
6 0.750 0.250 0.500 7 -1 ' '
_platon_squeeze_void_probe_radius 1.20
_platon_squeeze_details          ?
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_3
_database_code_depnum_ccdc_archive 'CCDC 1909221'
loop_
_audit_author_name
_audit_author_address
'Guangxiong Duan'
;Huazhong University of Science and Technology
China
;
_audit_update_record             
;
2019-04-10 deposited with the CCDC.	2019-12-13 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2016/6
_shelx_SHELXL_version_number     2016/6
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C337 H339 Ag32 Mo4 N3 O26 P24'
_chemical_formula_weight         9425.97

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           5
_space_group_name_H-M_alt        'C 2'
_space_group_name_Hall           'C 2y'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'

_cell_length_a                   41.161(3)
_cell_length_b                   24.6172(13)
_cell_length_c                   40.061(2)
_cell_angle_alpha                90
_cell_angle_beta                 103.141(2)
_cell_angle_gamma                90
_cell_volume                     39529(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9606
_cell_measurement_theta_min      2.368
_cell_measurement_theta_max      23.1175

_exptl_crystal_description       block
_exptl_crystal_colour            black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_density_diffrn    1.584
_exptl_crystal_F_000             18488
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.32
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.16
_exptl_absorpt_coefficient_mu    1.42
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.623
_exptl_absorpt_correction_T_max  0.748
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline B17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            259222
_diffrn_reflns_av_unetI/netI     0.0611
_diffrn_reflns_av_R_equivalents  0.0659
_diffrn_reflns_limit_h_min       -49
_diffrn_reflns_limit_h_max       49
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_l_min       -48
_diffrn_reflns_limit_l_max       48
_diffrn_reflns_theta_min         0.971
_diffrn_reflns_theta_max         25.382
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_point_group_measured_fraction_full 0.999
_reflns_number_total             72440
_reflns_number_gt                62950
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.950
_reflns_Friedel_fraction_max     0.997
_reflns_Friedel_fraction_full    0.999

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX3'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0993P)²+1355.5005P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
;
 Flack x determined using 27578 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.251(7)
_chemical_absolute_configuration ?
_refine_ls_number_reflns         72440
_refine_ls_number_parameters     3856
_refine_ls_number_restraints     2304
_refine_ls_R_factor_all          0.0819
_refine_ls_R_factor_gt           0.0674
_refine_ls_wR_factor_ref         0.1938
_refine_ls_wR_factor_gt          0.1802
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_restrained_S_all      1.021
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.81318(4) 0.67326(6) 0.73827(4) 0.0279(3) Uani 1 1 d . . . . .
Ag2 Ag 0.80981(4) 0.65342(6) 0.80763(4) 0.0280(3) Uani 1 1 d . . . . .
Ag3 Ag 0.83925(4) 0.57483(6) 0.77087(4) 0.0289(3) Uani 1 1 d . . . . .
Ag4 Ag 0.74844(4) 0.69584(5) 0.75980(3) 0.0206(3) Uani 1 1 d . . . . .
Ag5 Ag 0.75141(3) 0.66013(5) 0.68876(4) 0.0202(3) Uani 1 1 d . . . . .
Ag6 Ag 0.77075(3) 0.59478(5) 0.75405(3) 0.0188(3) Uani 1 1 d . . . . .
Ag7 Ag 0.79338(3) 0.56934(6) 0.69833(3) 0.0211(3) Uani 1 1 d . . . . .
Ag8 Ag 0.79781(4) 0.48229(6) 0.75350(4) 0.0229(3) Uani 1 1 d . . . . .
Ag9 Ag 0.78935(4) 0.53737(6) 0.81214(4) 0.0248(3) Uani 1 1 d . . . . .
Ag10 Ag 0.74377(4) 0.62971(6) 0.81585(3) 0.0228(3) Uani 1 1 d . . . . .
Ag11 Ag 0.74359(3) 0.56968(6) 0.63562(3) 0.0215(3) Uani 1 1 d . . . . .
Ag12 Ag 0.74860(3) 0.47190(5) 0.68628(4) 0.0205(3) Uani 1 1 d . . . . .
Ag13 Ag 0.76557(4) 0.42838(6) 0.80588(4) 0.0264(3) Uani 1 1 d . . . . .
Ag14 Ag 0.73333(3) 0.49730(5) 0.75430(3) 0.0190(3) Uani 1 1 d . . . . .
Ag15 Ag 0.71952(3) 0.56680(5) 0.69487(3) 0.0170(2) Uani 1 1 d . . . . .
Ag16 Ag 0.70207(3) 0.60056(5) 0.75691(3) 0.0170(3) Uani 1 1 d . . . . .
Ag17 Ag 0.68516(3) 0.67211(5) 0.70549(3) 0.0188(3) Uani 1 1 d . . . . .
Ag18 Ag 0.68820(4) 0.70293(5) 0.78168(4) 0.0240(3) Uani 1 1 d . . . . .
Ag19 Ag 0.67165(4) 0.60373(6) 0.81165(4) 0.0260(3) Uani 1 1 d . . . . .
Ag20 Ag 0.63594(3) 0.63397(6) 0.74533(4) 0.0238(3) Uani 1 1 d . . . . .
Ag21 Ag 0.66178(3) 0.51529(5) 0.75914(4) 0.0211(3) Uani 1 1 d . . . . .
Ag22 Ag 0.71773(4) 0.51618(6) 0.81468(4) 0.0244(3) Uani 1 1 d . . . . .
Ag23 Ag 0.69564(4) 0.41405(6) 0.77446(4) 0.0249(3) Uani 1 1 d . . . . .
Ag24 Ag 0.68627(3) 0.46015(5) 0.70198(4) 0.0210(3) Uani 1 1 d . . . . .
Ag25 Ag 0.68440(4) 0.51019(6) 0.63735(4) 0.0230(3) Uani 1 1 d . . . . .
Ag26 Ag 0.74626(4) 0.39092(5) 0.73737(4) 0.0254(3) Uani 1 1 d . . . . .
Ag27 Ag 0.68396(3) 0.62646(5) 0.63957(3) 0.0203(3) Uani 1 1 d . . . . .
Ag28 Ag 0.65350(3) 0.57097(5) 0.69165(3) 0.0203(3) Uani 1 1 d . . . . .
Ag29 Ag 0.79703(6) 0.55050(7) 0.99623(5) 0.0506(5) Uani 1 1 d . . . . .
Ag30 Ag 0.90253(5) 0.36687(9) 0.64035(5) 0.0486(5) Uani 1 1 d . . . . .
Ag31 Ag 0.50466(6) 0.38542(9) 0.65606(9) 0.0792(9) Uani 1 1 d . . . . .
Ag32 Ag 0.71817(5) 0.96072(8) 0.65946(5) 0.0444(4) Uani 1 1 d . . . . .
Mo1 Mo 0.72548(4) 0.78656(6) 0.69781(4) 0.0219(3) Uani 1 1 d . . . . .
Mo2 Mo 0.76948(5) 0.55713(7) 0.88684(4) 0.0295(4) Uani 1 1 d . . . . .
Mo3 Mo 0.82861(4) 0.45214(7) 0.68637(4) 0.0253(4) Uani 1 1 d . . . . .
Mo4 Mo 0.60459(4) 0.46460(7) 0.69389(5) 0.0259(4) Uani 1 1 d . . . . .
P1 P 0.77362(14) 0.5782(2) 0.58902(12) 0.0271(11) Uani 1 1 d . . . . .
P2 P 0.65524(15) 0.4462(2) 0.59269(14) 0.0329(12) Uani 1 1 d . . . . .
P3 P 0.64703(14) 0.68640(19) 0.59799(13) 0.0265(11) Uani 1 1 d . . . . .
P4 P 0.57668(13) 0.6601(3) 0.72751(17) 0.0366(13) Uani 1 1 d . . . . .
P5 P 0.68348(14) 0.7969(2) 0.80241(14) 0.0267(11) Uani 1 1 d . . . . .
P6 P 0.65052(16) 0.5984(2) 0.86415(14) 0.0341(12) Uani 1 1 d . . . . .
P7 P 0.89756(14) 0.5419(3) 0.78722(17) 0.0389(14) Uani 1 1 d . . . . .
P8 P 0.79885(19) 0.3788(2) 0.85527(15) 0.0457(17) Uani 1 1 d . . . . .
P9 P 0.65475(14) 0.3544(2) 0.79308(14) 0.0292(11) Uani 1 1 d . . . . .
P10 P 0.83837(15) 0.7014(2) 0.86002(15) 0.0360(13) Uani 1 1 d . . . . .
P11 P 0.84539(15) 0.7454(2) 0.7185(2) 0.0471(17) Uani 1 1 d . . . . .
P12 P 0.75751(14) 0.3000(2) 0.71615(15) 0.0299(12) Uani 1 1 d . . . . .
P13 P 0.53187(19) 0.2972(3) 0.6490(2) 0.065(2) Uani 1 1 d . . . . .
P14 P 0.49074(17) 0.4455(3) 0.6043(2) 0.0538(19) Uani 1 1 d . . . . .
P15 P 0.49386(18) 0.4191(4) 0.7102(3) 0.080(3) Uani 1 1 d . . . . .
P16 P 0.65867(16) 0.9680(3) 0.66172(16) 0.0456(16) Uani 1 1 d . . . . .
P17 P 0.76153(17) 0.9824(2) 0.71134(17) 0.0409(14) Uani 1 1 d . . . . .
P18 P 0.73563(15) 0.9275(2) 0.60807(16) 0.0349(13) Uani 1 1 d . . . . .
P19 P 0.7533(3) 0.4839(4) 0.9982(2) 0.069(2) Uani 1 1 d . . . . .
P20 P 0.7849(2) 0.6480(3) 1.00092(15) 0.053(2) Uani 1 1 d . . . . .
P21 P 0.8536(2) 0.5185(3) 0.99806(17) 0.058(2) Uani 1 1 d . . . . .
P22 P 0.91979(17) 0.3172(3) 0.69508(17) 0.0469(16) Uani 1 1 d . . . . .
P23 P 0.92755(17) 0.4570(3) 0.63211(18) 0.0492(16) Uani 1 1 d . . . . .
P24 P 0.85712(15) 0.3326(2) 0.59402(15) 0.0329(12) Uani 1 1 d . . . . .
O1 O 0.5662(3) 0.4332(5) 0.6797(4) 0.029(3) Uani 1 1 d . U . . .
O2 O 0.6363(3) 0.4228(6) 0.6840(4) 0.031(3) Uani 1 1 d . U . . .
O3 O 0.6126(3) 0.4741(5) 0.7390(4) 0.028(3) Uani 1 1 d . U . . .
O4 O 0.6049(3) 0.5288(5) 0.6731(3) 0.025(3) Uani 1 1 d . U . . .
O5 O 0.8576(4) 0.4177(6) 0.6693(4) 0.032(3) Uani 1 1 d . U . . .
O6 O 0.7874(3) 0.4258(5) 0.6676(3) 0.026(3) Uani 1 1 d . U . . .
O7 O 0.8375(3) 0.4430(5) 0.7318(3) 0.026(3) Uani 1 1 d . U . . .
O8 O 0.8303(3) 0.5216(6) 0.6762(4) 0.031(3) Uani 1 1 d . U . . .
O9 O 0.7241(3) 0.8539(5) 0.6852(3) 0.024(3) Uani 1 1 d . U . . .
O10 O 0.7479(3) 0.7478(5) 0.6732(3) 0.026(3) Uani 1 1 d . U . . .
O11 O 0.7448(3) 0.7826(5) 0.7419(3) 0.024(3) Uani 1 1 d . U . . .
O12 O 0.6838(3) 0.7602(5) 0.6906(3) 0.022(3) Uani 1 1 d . U . . .
O13 O 0.7504(4) 0.6218(6) 0.8727(4) 0.033(3) Uani 1 1 d . U . . .
O14 O 0.8054(4) 0.5476(6) 0.8693(4) 0.034(3) Uani 1 1 d . U . . .
O15 O 0.7393(4) 0.5049(6) 0.8721(3) 0.029(3) Uani 1 1 d . U . . .
O16 O 0.7815(4) 0.5552(6) 0.9321(4) 0.036(3) Uani 1 1 d . U . . .
O18 O 0.6905(11) 1.1278(19) 0.5776(11) 0.153(10) Uani 1 1 d . U . . .
O19 O 0.7420(11) 1.1024(18) 0.5951(11) 0.144(10) Uani 1 1 d . U . . .
O20 O 0.7059(10) 1.0819(17) 0.6218(11) 0.146(10) Uani 1 1 d . U . . .
O21 O 0.964(2) 0.274(4) 0.6200(16) 0.34(3) Uani 1 1 d D U . . .
O22 O 0.6994(10) 0.3308(14) 0.4873(10) 0.128(12) Uani 1 1 d . U . . .
O23 O 0.408(2) 0.312(4) 0.5579(17) 0.36(3) Uani 1 1 d D U . . .
O24 O 0.439(2) 0.310(4) 0.617(2) 0.35(3) Uani 1 1 d D U . . .
O25 O 0.404(2) 0.387(3) 0.596(2) 0.35(3) Uani 1 1 d D U . . .
O26 O 0.957(2) 0.231(3) 0.565(2) 0.34(3) Uani 1 1 d D U . . .
O27 O 0.983(2) 0.319(3) 0.575(2) 0.34(3) Uani 1 1 d D U . . .
N1 N 0.7162(16) 1.104(2) 0.5961(15) 0.143(9) Uani 1 1 d . U . . .
N3 N 0.962(3) 0.279(3) 0.5848(18) 0.34(3) Uani 1 1 d D U . . .
N4 N 0.412(3) 0.331(3) 0.5922(17) 0.35(3) Uani 1 1 d D U . . .
C1 C 0.7496(6) 0.5675(11) 0.5450(5) 0.043(4) Uani 1 1 d . U . . .
C2 C 0.7233(7) 0.5305(11) 0.5404(6) 0.047(5) Uani 1 1 d . U . . .
H2 H 0.717182 0.515164 0.559884 0.057 Uiso 1 1 calc R U . . .
C3 C 0.7065(8) 0.5164(12) 0.5088(6) 0.054(5) Uani 1 1 d . U . . .
H3 H 0.687915 0.492633 0.505967 0.064 Uiso 1 1 calc R U . . .
C4 C 0.7168(8) 0.5371(13) 0.4796(6) 0.056(5) Uani 1 1 d . U . . .
H4 H 0.705477 0.526554 0.457164 0.067 Uiso 1 1 calc R U . . .
C5 C 0.7428(7) 0.5720(13) 0.4841(6) 0.051(5) Uani 1 1 d . U . . .
H5 H 0.750037 0.587042 0.465247 0.061 Uiso 1 1 calc R U . . .
C6 C 0.7580(7) 0.5845(11) 0.5168(6) 0.048(5) Uani 1 1 d . U . . .
H6 H 0.776803 0.607888 0.519865 0.057 Uiso 1 1 calc R U . . .
C7 C 0.7903(6) 0.6464(9) 0.5897(6) 0.033(4) Uani 1 1 d . U . . .
C8 C 0.8177(6) 0.6592(9) 0.5726(6) 0.041(4) Uani 1 1 d . U . . .
H8 H 0.826852 0.632120 0.560503 0.049 Uiso 1 1 calc R U . . .
C9 C 0.8295(6) 0.7112(9) 0.5747(7) 0.042(4) Uani 1 1 d . U . . .
H9 H 0.847032 0.719895 0.563825 0.051 Uiso 1 1 calc R U . . .
C10 C 0.8174(7) 0.7503(10) 0.5913(7) 0.044(4) Uani 1 1 d . U . . .
H10 H 0.826368 0.785994 0.592242 0.052 Uiso 1 1 calc R U . . .
C11 C 0.7912(6) 0.7383(9) 0.6075(7) 0.043(4) Uani 1 1 d . U . . .
H11 H 0.781890 0.766151 0.618877 0.051 Uiso 1 1 calc R U . . .
C12 C 0.7795(6) 0.6875(9) 0.6068(6) 0.035(4) Uani 1 1 d . U . . .
H12 H 0.762741 0.679930 0.618980 0.042 Uiso 1 1 calc R U . . .
C13 C 0.7788(6) 0.9366(8) 0.6052(6) 0.035(4) Uani 1 1 d . U . . .
C14 C 0.7963(6) 0.8994(9) 0.5902(7) 0.043(4) Uani 1 1 d . U . . .
H14 H 0.785928 0.866218 0.581511 0.052 Uiso 1 1 calc R U . . .
C15 C 0.8290(6) 0.9101(10) 0.5878(7) 0.046(4) Uani 1 1 d . U . . .
H15 H 0.841032 0.883723 0.578129 0.055 Uiso 1 1 calc R U . . .
C16 C 0.8436(6) 0.9578(9) 0.5990(7) 0.042(4) Uani 1 1 d . U . . .
H16 H 0.866060 0.964182 0.597661 0.050 Uiso 1 1 calc R U . . .
C17 C 0.8261(6) 0.9983(9) 0.6126(7) 0.041(4) Uani 1 1 d . U . . .
H17 H 0.835884 1.032531 0.619741 0.049 Uiso 1 1 calc R U . . .
C18 C 0.7939(6) 0.9857(9) 0.6150(6) 0.037(4) Uani 1 1 d . U . . .
H18 H 0.781556 1.012440 0.623930 0.044 Uiso 1 1 calc R U . . .
C19 C 0.6468(6) 0.6796(9) 0.5525(5) 0.035(4) Uani 1 1 d . U . . .
C20 C 0.6754(7) 0.6592(10) 0.5436(6) 0.044(4) Uani 1 1 d . U . . .
H20 H 0.693672 0.647756 0.561224 0.052 Uiso 1 1 calc R U . . .
C21 C 0.6777(8) 0.6553(11) 0.5104(6) 0.051(5) Uani 1 1 d . U . . .
H21 H 0.696942 0.640240 0.504623 0.062 Uiso 1 1 calc R U . . .
C22 C 0.6501(7) 0.6748(11) 0.4839(6) 0.052(5) Uani 1 1 d . U . . .
H22 H 0.650884 0.672405 0.460466 0.063 Uiso 1 1 calc R U . . .
C23 C 0.6227(8) 0.6967(10) 0.4931(7) 0.052(5) Uani 1 1 d . U . . .
H23 H 0.604345 0.708948 0.475814 0.062 Uiso 1 1 calc R U . . .
C24 C 0.6217(7) 0.7010(10) 0.5262(6) 0.047(5) Uani 1 1 d . U . . .
H24 H 0.603439 0.719220 0.532047 0.056 Uiso 1 1 calc R U . . .
C25 C 0.6034(5) 0.6761(9) 0.5997(6) 0.036(4) Uani 1 1 d . U . . .
C26 C 0.5949(5) 0.6256(10) 0.6122(7) 0.042(4) Uani 1 1 d . U . . .
H26 H 0.611419 0.598545 0.619610 0.050 Uiso 1 1 calc R U . . .
C27 C 0.5622(6) 0.6165(11) 0.6133(7) 0.050(5) Uani 1 1 d . U . . .
H27 H 0.556450 0.582246 0.621229 0.059 Uiso 1 1 calc R U . . .
C28 C 0.5380(7) 0.6537(12) 0.6038(8) 0.056(5) Uani 1 1 d . U . . .
H28 H 0.515833 0.646234 0.605647 0.067 Uiso 1 1 calc R U . . .
C29 C 0.5460(6) 0.7022(12) 0.5916(8) 0.056(5) Uani 1 1 d . U . . .
H29 H 0.529090 0.728812 0.584518 0.067 Uiso 1 1 calc R U . . .
C30 C 0.5783(6) 0.7131(10) 0.5894(7) 0.045(5) Uani 1 1 d . U . . .
H30 H 0.583274 0.747175 0.580562 0.054 Uiso 1 1 calc R U . . .
C31 C 0.6542(6) 0.7600(7) 0.6051(6) 0.033(4) Uani 1 1 d . U . . .
H31A H 0.636617 0.780302 0.588889 0.039 Uiso 1 1 calc R U . . .
H31B H 0.652372 0.769222 0.628636 0.039 Uiso 1 1 calc R U . . .
C32 C 0.6877(5) 0.7776(7) 0.6003(5) 0.028(4) Uani 1 1 d . U . . .
H32A H 0.689741 0.767088 0.576996 0.033 Uiso 1 1 calc R U . . .
H32B H 0.705215 0.757985 0.616971 0.033 Uiso 1 1 calc R U . . .
C33 C 0.6937(5) 0.8381(8) 0.6049(5) 0.029(4) Uani 1 1 d . U . . .
H33A H 0.677929 0.857782 0.586490 0.035 Uiso 1 1 calc R U . . .
H33B H 0.689329 0.849531 0.627119 0.035 Uiso 1 1 calc R U . . .
C34 C 0.7290(6) 0.8534(9) 0.6037(6) 0.036(4) Uani 1 1 d . U . . .
H34A H 0.733642 0.841082 0.581751 0.044 Uiso 1 1 calc R U . . .
H34B H 0.744806 0.834634 0.622544 0.044 Uiso 1 1 calc R U . . .
C35 C 0.7197(6) 0.2767(10) 0.6862(7) 0.042(4) Uani 1 1 d . U . . .
C36 C 0.7181(7) 0.2336(11) 0.6618(7) 0.053(5) Uani 1 1 d . U . . .
H36 H 0.738249 0.215950 0.660254 0.064 Uiso 1 1 calc R U . . .
C37 C 0.6897(8) 0.2172(12) 0.6411(8) 0.062(5) Uani 1 1 d . U . . .
H37 H 0.689368 0.186846 0.626401 0.075 Uiso 1 1 calc R U . . .
C38 C 0.6604(7) 0.2458(12) 0.6418(8) 0.059(5) Uani 1 1 d . U . . .
H38 H 0.639774 0.234042 0.627747 0.071 Uiso 1 1 calc R U . . .
C39 C 0.6611(6) 0.2892(10) 0.6617(7) 0.047(5) Uani 1 1 d . U . . .
H39 H 0.641479 0.310160 0.660320 0.057 Uiso 1 1 calc R U . . .
C40 C 0.6913(6) 0.3043(10) 0.6851(7) 0.043(4) Uani 1 1 d . U . . .
H40 H 0.691390 0.334096 0.700197 0.052 Uiso 1 1 calc R U . . .
C41 C 0.7908(5) 0.2932(10) 0.6928(6) 0.037(5) Uani 1 1 d . U . . .
H41A H 0.789806 0.256197 0.682891 0.045 Uiso 1 1 calc R U . . .
H41B H 0.786603 0.319372 0.673520 0.045 Uiso 1 1 calc R U . . .
C365 C 0.7368(14) 0.525(2) 1.0932(14) 0.139(9) Uani 1 1 d D U . . .
H365 H 0.749354 0.542297 1.113091 0.167 Uiso 1 1 calc R U . . .
C364 C 0.7044(14) 0.507(2) 1.0934(14) 0.138(9) Uani 1 1 d D U . . .
H364 H 0.691729 0.517771 1.109279 0.166 Uiso 1 1 calc R U . . .
C363 C 0.6939(15) 0.470(2) 1.0664(13) 0.137(9) Uani 1 1 d D U . . .
H363 H 0.675103 0.448209 1.068001 0.165 Uiso 1 1 calc R U . . .
C362 C 0.7522(15) 0.518(2) 1.0642(12) 0.137(9) Uani 1 1 d D U . . .
H362 H 0.773594 0.533333 1.065166 0.164 Uiso 1 1 calc R U . . .
C361 C 0.7071(14) 0.459(2) 1.0370(14) 0.136(9) Uani 1 1 d D U . . .
H361 H 0.696977 0.432928 1.020105 0.164 Uiso 1 1 calc R U . . .
C360 C 0.7360(14) 0.488(2) 1.0341(14) 0.136(9) Uani 1 1 d D U . . .
C42 C 0.8261(5) 0.3030(10) 0.7150(6) 0.035(4) Uani 1 1 d . U . . .
H42A H 0.827072 0.340068 0.724716 0.042 Uiso 1 1 calc R U . . .
H42B H 0.830142 0.277004 0.734364 0.042 Uiso 1 1 calc R U . . .
C43 C 0.8538(6) 0.2970(10) 0.6959(6) 0.037(4) Uani 1 1 d . U . . .
H43A H 0.856605 0.258233 0.690478 0.044 Uiso 1 1 calc R U . . .
H43B H 0.848158 0.317526 0.674082 0.044 Uiso 1 1 calc R U . . .
C44 C 0.8846(6) 0.3180(10) 0.7177(6) 0.042(5) Uani 1 1 d . U . . .
H44A H 0.890691 0.295660 0.738717 0.051 Uiso 1 1 calc R U . . .
H44B H 0.880838 0.355680 0.724565 0.051 Uiso 1 1 calc R U . . .
C45 C 0.8093(6) 0.5339(8) 0.5921(6) 0.032(4) Uani 1 1 d . U . . .
H45A H 0.820459 0.543012 0.573406 0.038 Uiso 1 1 calc R U . . .
H45B H 0.825353 0.541092 0.614119 0.038 Uiso 1 1 calc R U . . .
C46 C 0.8008(6) 0.4736(8) 0.5901(5) 0.031(4) Uani 1 1 d . U . . .
H46A H 0.792035 0.463770 0.610347 0.037 Uiso 1 1 calc R U . . .
H46B H 0.782673 0.467360 0.569485 0.037 Uiso 1 1 calc R U . . .
C47 C 0.8288(6) 0.4368(9) 0.5885(6) 0.033(4) Uani 1 1 d . U . . .
H47A H 0.848320 0.447002 0.606886 0.040 Uiso 1 1 calc R U . . .
H47B H 0.835021 0.441960 0.566291 0.040 Uiso 1 1 calc R U . . .
C48 C 0.8209(6) 0.3759(9) 0.5926(6) 0.034(4) Uani 1 1 d . U . . .
H48A H 0.802731 0.364659 0.573142 0.041 Uiso 1 1 calc R U . . .
H48B H 0.813024 0.370966 0.613950 0.041 Uiso 1 1 calc R U . . .
C49 C 0.9180(6) 0.5050(12) 0.6629(7) 0.050(5) Uani 1 1 d . U . . .
H49A H 0.930944 0.538733 0.662003 0.060 Uiso 1 1 calc R U . . .
H49B H 0.894057 0.514498 0.656047 0.060 Uiso 1 1 calc R U . . .
C50 C 0.9259(6) 0.4838(11) 0.7007(7) 0.047(5) Uani 1 1 d . U . . .
H50A H 0.915510 0.447680 0.701543 0.057 Uiso 1 1 calc R U . . .
H50B H 0.950311 0.479788 0.709224 0.057 Uiso 1 1 calc R U . . .
C51 C 0.9124(6) 0.5235(11) 0.7236(7) 0.045(5) Uani 1 1 d . U . . .
H51A H 0.926452 0.556554 0.727222 0.054 Uiso 1 1 calc R U . . .
H51B H 0.889420 0.534298 0.712197 0.054 Uiso 1 1 calc R U . . .
C52 C 0.9124(6) 0.4976(11) 0.7581(6) 0.044(5) Uani 1 1 d . U . . .
H52A H 0.935349 0.485846 0.768939 0.052 Uiso 1 1 calc R U . . .
H52B H 0.898130 0.464710 0.754188 0.052 Uiso 1 1 calc R U . . .
C53 C 0.6505(6) 0.9103(10) 0.6879(6) 0.039(5) Uani 1 1 d . U . . .
H53A H 0.626571 0.910304 0.688264 0.047 Uiso 1 1 calc R U . . .
H53B H 0.655219 0.876186 0.676812 0.047 Uiso 1 1 calc R U . . .
C54 C 0.6699(6) 0.9107(9) 0.7227(6) 0.038(4) Uani 1 1 d . U . . .
H54A H 0.663379 0.942717 0.734675 0.045 Uiso 1 1 calc R U . . .
H54B H 0.693762 0.914669 0.722491 0.045 Uiso 1 1 calc R U . . .
C55 C 0.6655(5) 0.8595(8) 0.7428(5) 0.029(4) Uani 1 1 d . U . . .
H55A H 0.642875 0.859840 0.747558 0.035 Uiso 1 1 calc R U . . .
H55B H 0.667013 0.827291 0.728490 0.035 Uiso 1 1 calc R U . . .
C56 C 0.6910(6) 0.8544(9) 0.7763(5) 0.033(4) Uani 1 1 d . U . . .
H56A H 0.690977 0.888333 0.789580 0.039 Uiso 1 1 calc R U . . .
H56B H 0.713368 0.850481 0.771357 0.039 Uiso 1 1 calc R U . . .
C57 C 0.6369(7) 0.5255(10) 0.5440(6) 0.044(5) Uani 1 1 d . U . . .
H57 H 0.641160 0.549816 0.562866 0.053 Uiso 1 1 calc R U . . .
C58 C 0.6248(7) 0.5462(11) 0.5111(6) 0.050(5) Uani 1 1 d . U . . .
H58 H 0.623076 0.584298 0.507238 0.060 Uiso 1 1 calc R U . . .
C59 C 0.6153(8) 0.5102(12) 0.4843(7) 0.055(5) Uani 1 1 d . U . . .
H59 H 0.604734 0.523828 0.462296 0.066 Uiso 1 1 calc R U . . .
C60 C 0.6204(7) 0.4576(11) 0.4881(7) 0.053(5) Uani 1 1 d . U . . .
H60 H 0.615551 0.433915 0.468865 0.064 Uiso 1 1 calc R U . . .
C61 C 0.6327(7) 0.4377(11) 0.5202(6) 0.048(5) Uani 1 1 d . U . . .
H61 H 0.634624 0.399364 0.522946 0.058 Uiso 1 1 calc R U . . .
C62 C 0.6430(7) 0.4707(10) 0.5499(6) 0.042(4) Uani 1 1 d . U . . .
C63 C 0.6824(6) 0.3872(9) 0.5902(6) 0.039(4) Uani 1 1 d . U . . .
C64 C 0.7151(6) 0.3924(10) 0.6048(6) 0.039(4) Uani 1 1 d . U . . .
H64 H 0.723282 0.426114 0.614808 0.047 Uiso 1 1 calc R U . . .
C65 C 0.7377(7) 0.3481(11) 0.6053(7) 0.048(5) Uani 1 1 d . U . . .
H65 H 0.760590 0.351944 0.616254 0.057 Uiso 1 1 calc R U . . .
C66 C 0.7261(7) 0.3005(11) 0.5901(7) 0.053(5) Uani 1 1 d . U . . .
H66 H 0.740946 0.271092 0.589723 0.063 Uiso 1 1 calc R U . . .
C67 C 0.6926(7) 0.2949(11) 0.5751(7) 0.051(5) Uani 1 1 d . U . . .
H67 H 0.684616 0.261569 0.564424 0.061 Uiso 1 1 calc R U . . .
C68 C 0.6701(7) 0.3379(10) 0.5755(7) 0.047(5) Uani 1 1 d . U . . .
H68 H 0.646976 0.333317 0.565897 0.056 Uiso 1 1 calc R U . . .
C69 C 0.7898(8) 0.2599(11) 0.7787(7) 0.055(5) Uani 1 1 d . U . . .
H69 H 0.793535 0.297246 0.784129 0.066 Uiso 1 1 calc R U . . .
C70 C 0.8053(9) 0.2211(12) 0.8022(8) 0.065(6) Uani 1 1 d . U . . .
H70 H 0.820921 0.231219 0.822488 0.078 Uiso 1 1 calc R U . . .
C71 C 0.7971(8) 0.1675(11) 0.7950(8) 0.061(5) Uani 1 1 d . U . . .
H71 H 0.806569 0.140100 0.811004 0.073 Uiso 1 1 calc R U . . .
C72 C 0.7753(7) 0.1532(11) 0.7649(8) 0.056(5) Uani 1 1 d . U . . .
H72 H 0.769284 0.116119 0.761103 0.067 Uiso 1 1 calc R U . . .
C73 C 0.7620(7) 0.1904(9) 0.7400(8) 0.050(5) Uani 1 1 d . U . . .
H73 H 0.748362 0.179703 0.718580 0.059 Uiso 1 1 calc R U . . .
C74 C 0.7696(6) 0.2457(9) 0.7481(6) 0.039(4) Uani 1 1 d . U . . .
C75 C 0.5994(7) 0.7461(11) 0.6959(7) 0.049(5) Uani 1 1 d . U . . .
H75 H 0.620456 0.734739 0.709222 0.059 Uiso 1 1 calc R U . . .
C76 C 0.5721(6) 0.7185(11) 0.6991(7) 0.048(5) Uani 1 1 d . U . . .
C77 C 0.5432(8) 0.7341(12) 0.6780(8) 0.064(6) Uani 1 1 d . U . . .
H77 H 0.523223 0.714356 0.677190 0.076 Uiso 1 1 calc R U . . .
C78 C 0.5432(8) 0.7812(13) 0.6567(9) 0.066(6) Uani 1 1 d . U . . .
H78 H 0.522837 0.793158 0.642145 0.079 Uiso 1 1 calc R U . . .
C79 C 0.5679(8) 0.8051(13) 0.6570(9) 0.066(6) Uani 1 1 d . U . . .
H79 H 0.566140 0.837730 0.644058 0.079 Uiso 1 1 calc R U . . .
C80 C 0.5986(7) 0.7900(12) 0.6741(8) 0.057(5) Uani 1 1 d . U . . .
H80 H 0.618273 0.808205 0.671545 0.069 Uiso 1 1 calc R U . . .
C81 C 0.7411(10) 0.6665(13) 1.0029(8) 0.071(6) Uani 1 1 d . U . . .
C82 C 0.7335(11) 0.6530(15) 1.0323(8) 0.081(7) Uani 1 1 d . U . . .
H82 H 0.750441 0.641760 1.051305 0.097 Uiso 1 1 calc R U . . .
C83 C 0.7003(12) 0.6556(18) 1.0351(9) 0.093(7) Uani 1 1 d . U . . .
H83 H 0.694604 0.645546 1.055985 0.111 Uiso 1 1 calc R U . . .
C84 C 0.6752(12) 0.6732(17) 1.0068(9) 0.090(7) Uani 1 1 d . U . . .
H84 H 0.652940 0.677849 1.009284 0.109 Uiso 1 1 calc R U . . .
C85 C 0.6831(11) 0.6839(16) 0.9749(9) 0.084(7) Uani 1 1 d . U . . .
H85 H 0.666899 0.692748 0.954702 0.101 Uiso 1 1 calc R U . . .
C86 C 0.7197(10) 0.6798(13) 0.9763(8) 0.072(6) Uani 1 1 d . U . . .
H86 H 0.727201 0.687547 0.956063 0.086 Uiso 1 1 calc R U . . .
C87 C 0.8730(10) 0.4725(15) 1.0325(8) 0.080(7) Uani 1 1 d . U . . .
C88 C 0.9038(11) 0.4524(16) 1.0341(9) 0.086(7) Uani 1 1 d . U . . .
H88 H 0.915690 0.464045 1.017656 0.103 Uiso 1 1 calc R U . . .
C89 C 0.9193(11) 0.4132(17) 1.0601(9) 0.092(7) Uani 1 1 d . U . . .
H89 H 0.939725 0.395516 1.059823 0.111 Uiso 1 1 calc R U . . .
C90 C 0.9010(11) 0.4032(16) 1.0868(9) 0.091(7) Uani 1 1 d . U . . .
H90 H 0.910263 0.380193 1.105602 0.109 Uiso 1 1 calc R U . . .
C91 C 0.8708(11) 0.4267(16) 1.0850(9) 0.089(7) Uani 1 1 d . U . . .
H91 H 0.859405 0.419585 1.102706 0.107 Uiso 1 1 calc R U . . .
C92 C 0.8561(11) 0.4600(16) 1.0589(9) 0.086(7) Uani 1 1 d . U . . .
H92 H 0.834703 0.474885 1.058163 0.103 Uiso 1 1 calc R U . . .
C93 C 0.6422(8) 0.6649(11) 0.8803(6) 0.052(5) Uani 1 1 d . U . . .
C94 C 0.6690(8) 0.7009(11) 0.8855(7) 0.055(5) Uani 1 1 d . U . . .
H94 H 0.689418 0.689552 0.880491 0.066 Uiso 1 1 calc R U . . .
C95 C 0.6664(9) 0.7534(11) 0.8980(7) 0.061(5) Uani 1 1 d . U . . .
H95 H 0.684594 0.778132 0.901018 0.073 Uiso 1 1 calc R U . . .
C96 C 0.6359(9) 0.7684(12) 0.9061(7) 0.060(5) Uani 1 1 d . U . . .
H96 H 0.633552 0.803785 0.914712 0.072 Uiso 1 1 calc R U . . .
C97 C 0.6092(9) 0.7318(12) 0.9014(7) 0.063(5) Uani 1 1 d . U . . .
H97 H 0.588674 0.742906 0.906311 0.075 Uiso 1 1 calc R U . . .
C98 C 0.6126(8) 0.6801(12) 0.8899(7) 0.057(5) Uani 1 1 d . U . . .
H98 H 0.594963 0.654646 0.888441 0.069 Uiso 1 1 calc R U . . .
C99 C 0.8060(6) 0.7928(9) 0.8300(7) 0.042(4) Uani 1 1 d . U . . .
H99 H 0.795399 0.767144 0.813338 0.050 Uiso 1 1 calc R U . . .
C100 C 0.8297(6) 0.7731(10) 0.8567(7) 0.044(4) Uani 1 1 d . U . . .
C101 C 0.8454(7) 0.8125(10) 0.8811(7) 0.051(5) Uani 1 1 d . U . . .
H101 H 0.860804 0.800495 0.901128 0.061 Uiso 1 1 calc R U . . .
C102 C 0.8390(8) 0.8675(10) 0.8767(8) 0.055(5) Uani 1 1 d . U . . .
H102 H 0.851187 0.893508 0.892139 0.066 Uiso 1 1 calc R U . . .
C103 C 0.8134(8) 0.8836(11) 0.8479(8) 0.059(5) Uani 1 1 d . U . . .
H103 H 0.808717 0.921280 0.844635 0.071 Uiso 1 1 calc R U . . .
C104 C 0.7953(7) 0.8479(10) 0.8246(8) 0.052(5) Uani 1 1 d . U . . .
H104 H 0.777241 0.858842 0.806544 0.062 Uiso 1 1 calc R U . . .
C105 C 0.7331(7) 0.7675(11) 0.8594(6) 0.046(5) Uani 1 1 d . U . . .
H105 H 0.731792 0.732630 0.849026 0.055 Uiso 1 1 calc R U . . .
C106 C 0.7540(7) 0.7771(12) 0.8914(7) 0.053(5) Uani 1 1 d . U . . .
H106 H 0.766141 0.747666 0.903582 0.063 Uiso 1 1 calc R U . . .
C107 C 0.7578(7) 0.8287(12) 0.9059(7) 0.051(5) Uani 1 1 d . U . . .
H107 H 0.774390 0.835009 0.926224 0.061 Uiso 1 1 calc R U . . .
C108 C 0.7383(7) 0.8690(12) 0.8916(6) 0.050(5) Uani 1 1 d . U . . .
H108 H 0.740140 0.903240 0.902869 0.060 Uiso 1 1 calc R U . . .
C109 C 0.7140(7) 0.8623(10) 0.8588(6) 0.048(5) Uani 1 1 d . U . . .
H109 H 0.699191 0.890586 0.848825 0.057 Uiso 1 1 calc R U . . .
C110 C 0.7140(6) 0.8110(9) 0.8431(6) 0.037(4) Uani 1 1 d . U . . .
C111 C 0.5535(6) 0.6744(12) 0.7605(7) 0.047(5) Uani 1 1 d . U . . .
C112 C 0.5621(7) 0.6431(14) 0.7895(8) 0.061(5) Uani 1 1 d . U . . .
H112 H 0.580375 0.618583 0.792759 0.073 Uiso 1 1 calc R U . . .
C113 C 0.5426(8) 0.6488(16) 0.8144(9) 0.070(6) Uani 1 1 d . U . . .
H113 H 0.548165 0.627965 0.834892 0.084 Uiso 1 1 calc R U . . .
C114 C 0.5179(7) 0.6815(15) 0.8099(8) 0.065(5) Uani 1 1 d . U . . .
H114 H 0.504776 0.682919 0.826542 0.078 Uiso 1 1 calc R U . . .
C115 C 0.5098(6) 0.7141(14) 0.7820(7) 0.059(5) Uani 1 1 d . U . . .
H115 H 0.492064 0.739498 0.779846 0.070 Uiso 1 1 calc R U . . .
C116 C 0.5272(5) 0.7103(12) 0.7570(7) 0.048(5) Uani 1 1 d . U . . .
H116 H 0.521243 0.732413 0.737074 0.057 Uiso 1 1 calc R U . . .
C117 C 0.6142(6) 0.5562(11) 0.8592(7) 0.052(5) Uani 1 1 d . U . . .
C118 C 0.5966(7) 0.5510(12) 0.8858(8) 0.058(5) Uani 1 1 d . U . . .
H118 H 0.602959 0.569073 0.907272 0.070 Uiso 1 1 calc R U . . .
C119 C 0.5683(8) 0.5153(13) 0.8768(9) 0.068(6) Uani 1 1 d . U . . .
H119 H 0.554487 0.510572 0.892604 0.082 Uiso 1 1 calc R U . . .
C120 C 0.5610(9) 0.4892(15) 0.8479(10) 0.080(6) Uani 1 1 d . U . . .
H120 H 0.541267 0.467947 0.843973 0.095 Uiso 1 1 calc R U . . .
C121 C 0.5773(8) 0.4884(14) 0.8233(10) 0.070(6) Uani 1 1 d . U . . .
H121 H 0.571934 0.465714 0.803639 0.084 Uiso 1 1 calc R U . . .
C122 C 0.6041(6) 0.5261(11) 0.8301(8) 0.051(5) Uani 1 1 d . U . . .
H122 H 0.616222 0.530765 0.812684 0.061 Uiso 1 1 calc R U . . .
C123 C 0.6238(9) 1.0259(14) 0.7036(9) 0.073(6) Uani 1 1 d . U . . .
H123 H 0.614380 0.992442 0.708494 0.087 Uiso 1 1 calc R U . . .
C124 C 0.6472(7) 0.3763(9) 0.8340(6) 0.044(4) Uani 1 1 d . U . . .
C125 C 0.6716(8) 0.4086(10) 0.8547(6) 0.049(5) Uani 1 1 d . U . . .
H125 H 0.690876 0.419637 0.847198 0.059 Uiso 1 1 calc R U . . .
C126 C 0.6667(9) 0.4244(11) 0.8870(7) 0.060(5) Uani 1 1 d . U . . .
H126 H 0.683464 0.445885 0.901259 0.072 Uiso 1 1 calc R U . . .
C127 C 0.6392(9) 0.4105(12) 0.8991(8) 0.061(5) Uani 1 1 d . U . . .
H127 H 0.637178 0.420589 0.921416 0.074 Uiso 1 1 calc R U . . .
C128 C 0.6144(9) 0.3808(12) 0.8771(8) 0.061(5) Uani 1 1 d . U . . .
H128 H 0.594264 0.371947 0.883590 0.074 Uiso 1 1 calc R U . . .
C129 C 0.6193(8) 0.3658(12) 0.8481(8) 0.057(5) Uani 1 1 d . U . . .
H129 H 0.601928 0.344921 0.834217 0.069 Uiso 1 1 calc R U . . .
C130 C 0.6668(7) 0.2841(9) 0.8002(7) 0.047(5) Uani 1 1 d . U . . .
C131 C 0.6487(8) 0.2468(10) 0.8150(8) 0.057(5) Uani 1 1 d . U . . .
H131 H 0.629001 0.257938 0.821649 0.068 Uiso 1 1 calc R U . . .
C132 C 0.6600(9) 0.1917(10) 0.8202(8) 0.066(6) Uani 1 1 d . U . . .
H132 H 0.648195 0.166428 0.830867 0.079 Uiso 1 1 calc R U . . .
C133 C 0.6865(9) 0.1766(11) 0.8101(8) 0.068(6) Uani 1 1 d . U . . .
H133 H 0.693020 0.139612 0.813267 0.082 Uiso 1 1 calc R U . . .
C134 C 0.7058(10) 0.2109(11) 0.7951(8) 0.070(6) Uani 1 1 d . U . . .
H134 H 0.725003 0.198049 0.788122 0.084 Uiso 1 1 calc R U . . .
C135 C 0.6953(9) 0.2672(11) 0.7904(8) 0.060(5) Uani 1 1 d . U . . .
H135 H 0.708006 0.292415 0.780698 0.072 Uiso 1 1 calc R U . . .
C136 C 0.7618(11) 0.4145(15) 0.9957(9) 0.093(8) Uani 1 1 d . U . . .
C137 C 0.7549(12) 0.3861(16) 0.9639(10) 0.096(8) Uani 1 1 d . U . . .
H137 H 0.742473 0.405558 0.944773 0.115 Uiso 1 1 calc R U . . .
C138 C 0.7645(12) 0.3316(16) 0.9571(10) 0.097(8) Uani 1 1 d . U . . .
H138 H 0.759325 0.315094 0.935070 0.116 Uiso 1 1 calc R U . . .
C139 C 0.7825(11) 0.3054(16) 0.9874(9) 0.092(8) Uani 1 1 d . U . . .
H139 H 0.791514 0.269996 0.986758 0.110 Uiso 1 1 calc R U . . .
C140 C 0.7863(12) 0.3341(16) 1.0178(9) 0.094(8) Uani 1 1 d . U . . .
H140 H 0.796443 0.314684 1.037971 0.113 Uiso 1 1 calc R U . . .
C141 C 0.7773(11) 0.3877(15) 1.0230(9) 0.091(8) Uani 1 1 d . U . . .
H141 H 0.782058 0.403892 1.045111 0.109 Uiso 1 1 calc R U . . .
C142 C 0.9047(8) 0.5037(14) 0.8276(9) 0.069(6) Uani 1 1 d . U . . .
C143 C 0.8799(7) 0.5077(13) 0.8468(8) 0.066(6) Uani 1 1 d . U . . .
H143 H 0.859887 0.527303 0.838135 0.079 Uiso 1 1 calc R U . . .
C144 C 0.8857(9) 0.4823(15) 0.8787(9) 0.076(6) Uani 1 1 d . U . . .
H144 H 0.869949 0.484789 0.892653 0.091 Uiso 1 1 calc R U . . .
C145 C 0.9148(10) 0.4535(16) 0.8893(10) 0.085(7) Uani 1 1 d . U . . .
H145 H 0.919021 0.437820 0.911497 0.101 Uiso 1 1 calc R U . . .
C146 C 0.9364(10) 0.4464(16) 0.8720(10) 0.087(7) Uani 1 1 d . U . . .
H146 H 0.955468 0.424265 0.880033 0.104 Uiso 1 1 calc R U . . .
C147 C 0.9308(9) 0.4718(15) 0.8415(10) 0.081(7) Uani 1 1 d . U . . .
H147 H 0.947103 0.466616 0.828423 0.097 Uiso 1 1 calc R U . . .
C148 C 0.8764(7) 0.7788(14) 0.7509(8) 0.061(6) Uani 1 1 d . U . . .
C149 C 0.8714(8) 0.7870(17) 0.7804(9) 0.077(6) Uani 1 1 d . U . . .
H149 H 0.853532 0.766740 0.785669 0.093 Uiso 1 1 calc R U . . .
C150 C 0.8868(8) 0.8186(17) 0.8046(10) 0.080(6) Uani 1 1 d . U . . .
H150 H 0.878185 0.828463 0.823776 0.096 Uiso 1 1 calc R U . . .
C151 C 0.9181(8) 0.8374(17) 0.7996(10) 0.078(6) Uani 1 1 d . U . . .
H151 H 0.931598 0.860061 0.816362 0.094 Uiso 1 1 calc R U . . .
C152 C 0.9279(8) 0.8243(15) 0.7734(9) 0.071(6) Uani 1 1 d . U . . .
H152 H 0.949765 0.834435 0.771808 0.086 Uiso 1 1 calc R U . . .
C153 C 0.9083(7) 0.7959(14) 0.7468(8) 0.064(6) Uani 1 1 d . U . . .
H153 H 0.915649 0.788000 0.726495 0.077 Uiso 1 1 calc R U . . .
C154 C 0.8841(7) 0.6898(15) 0.8722(10) 0.079(7) Uani 1 1 d . U . . .
C155 C 0.8918(8) 0.6331(17) 0.8792(11) 0.090(7) Uani 1 1 d . U . . .
H155 H 0.874944 0.606705 0.879231 0.107 Uiso 1 1 calc R U . . .
C156 C 0.9250(9) 0.6199(18) 0.8859(11) 0.096(8) Uani 1 1 d . U . . .
H156 H 0.931615 0.582948 0.888897 0.115 Uiso 1 1 calc R U . . .
C157 C 0.9499(9) 0.6619(18) 0.8885(12) 0.102(8) Uani 1 1 d . U . . .
H157 H 0.972641 0.651624 0.892130 0.123 Uiso 1 1 calc R U . . .
C158 C 0.9422(10) 0.7147(19) 0.8861(12) 0.105(8) Uani 1 1 d . U . . .
H158 H 0.958959 0.741954 0.890526 0.127 Uiso 1 1 calc R U . . .
C159 C 0.9071(9) 0.7286(18) 0.8763(12) 0.095(8) Uani 1 1 d . U . . .
H159 H 0.900522 0.765578 0.872785 0.114 Uiso 1 1 calc R U . . .
C160 C 0.9303(7) 0.5944(13) 0.7938(11) 0.075(7) Uani 1 1 d . U . . .
C161 C 0.9642(8) 0.5817(15) 0.8034(11) 0.088(7) Uani 1 1 d . U . . .
H161 H 0.971342 0.544906 0.804707 0.106 Uiso 1 1 calc R U . . .
C162 C 0.9867(9) 0.6225(17) 0.8108(13) 0.102(8) Uani 1 1 d . U . . .
H162 H 1.009510 0.613958 0.819916 0.122 Uiso 1 1 calc R U . . .
C163 C 0.9782(10) 0.6718(17) 0.8058(13) 0.105(8) Uani 1 1 d . U . . .
H163 H 0.994988 0.698382 0.805820 0.126 Uiso 1 1 calc R U . . .
C164 C 0.9434(10) 0.6890(17) 0.8000(12) 0.103(8) Uani 1 1 d . U . . .
H164 H 0.937296 0.726202 0.800074 0.123 Uiso 1 1 calc R U . . .
C165 C 0.9190(9) 0.6461(15) 0.7941(11) 0.091(7) Uani 1 1 d . U . . .
H165 H 0.895824 0.653783 0.790448 0.109 Uiso 1 1 calc R U . . .
C166 C 0.6427(6) 0.8116(10) 0.8103(6) 0.042(4) Uani 1 1 d . U . . .
C167 C 0.6210(6) 0.7689(11) 0.8113(6) 0.044(4) Uani 1 1 d . U . . .
H167 H 0.627215 0.733108 0.806430 0.053 Uiso 1 1 calc R U . . .
C168 C 0.5900(7) 0.7775(13) 0.8191(7) 0.053(5) Uani 1 1 d . U . . .
H168 H 0.575733 0.747753 0.820572 0.063 Uiso 1 1 calc R U . . .
C169 C 0.5804(7) 0.8302(14) 0.8248(8) 0.060(5) Uani 1 1 d . U . . .
H169 H 0.558721 0.836965 0.828524 0.072 Uiso 1 1 calc R U . . .
C170 C 0.6014(7) 0.8709(13) 0.8251(8) 0.058(5) Uani 1 1 d . U . . .
H170 H 0.595367 0.906048 0.831346 0.069 Uiso 1 1 calc R U . . .
C171 C 0.6320(7) 0.8642(12) 0.8165(7) 0.052(5) Uani 1 1 d . U . . .
H171 H 0.645625 0.894846 0.814853 0.062 Uiso 1 1 calc R U . . .
C172 C 0.8253(7) 0.6772(9) 0.8980(5) 0.047(5) Uani 1 1 d . U . . .
H17A H 0.800649 0.679253 0.893498 0.056 Uiso 1 1 calc R U . . .
H17B H 0.831623 0.638498 0.901557 0.056 Uiso 1 1 calc R U . . .
C173 C 0.8402(8) 0.7089(10) 0.9318(6) 0.051(5) Uani 1 1 d . U . . .
H17C H 0.831493 0.746538 0.929979 0.061 Uiso 1 1 calc R U . . .
H17D H 0.864801 0.710593 0.935537 0.061 Uiso 1 1 calc R U . . .
C174 C 0.8304(8) 0.6794(11) 0.9628(6) 0.055(5) Uani 1 1 d . U . . .
H17E H 0.844221 0.694382 0.984312 0.066 Uiso 1 1 calc R U . . .
H17F H 0.835960 0.640400 0.961869 0.066 Uiso 1 1 calc R U . . .
C175 C 0.7915(8) 0.6848(10) 0.9640(6) 0.054(6) Uani 1 1 d . U . . .
H17G H 0.777175 0.669608 0.942825 0.065 Uiso 1 1 calc R U . . .
H17H H 0.785544 0.723540 0.965705 0.065 Uiso 1 1 calc R U . . .
C176 C 0.7175(9) 0.4936(13) 0.9639(8) 0.067(7) Uani 1 1 d . U . . .
H17I H 0.724332 0.489399 0.941868 0.080 Uiso 1 1 calc R U . . .
H17J H 0.701048 0.464825 0.965082 0.080 Uiso 1 1 calc R U . . .
C177 C 0.7015(9) 0.5465(13) 0.9643(8) 0.067(6) Uani 1 1 d . U . . .
H17K H 0.718613 0.574938 0.964579 0.080 Uiso 1 1 calc R U . . .
H17L H 0.694031 0.549632 0.985983 0.080 Uiso 1 1 calc R U . . .
C178 C 0.6714(7) 0.5592(13) 0.9343(7) 0.057(5) Uani 1 1 d . U . . .
H17M H 0.659560 0.591467 0.940485 0.069 Uiso 1 1 calc R U . . .
H17N H 0.655652 0.528218 0.931457 0.069 Uiso 1 1 calc R U . . .
C179 C 0.6809(6) 0.5703(11) 0.8995(6) 0.045(5) Uani 1 1 d . U . . .
H17O H 0.688609 0.535419 0.891634 0.054 Uiso 1 1 calc R U . . .
H17P H 0.700381 0.595057 0.904128 0.054 Uiso 1 1 calc R U . . .
C180 C 0.8090(8) 0.4182(10) 0.8942(6) 0.054(6) Uani 1 1 d . U . . .
H18A H 0.819066 0.452722 0.888826 0.064 Uiso 1 1 calc R U . . .
H18B H 0.787816 0.427493 0.900519 0.064 Uiso 1 1 calc R U . . .
C181 C 0.8325(8) 0.3938(11) 0.9260(6) 0.058(6) Uani 1 1 d . U . . .
H18C H 0.855372 0.391543 0.922275 0.070 Uiso 1 1 calc R U . . .
H18D H 0.825022 0.356621 0.929999 0.070 Uiso 1 1 calc R U . . .
C182 C 0.8324(9) 0.4303(12) 0.9584(7) 0.066(6) Uani 1 1 d . U . . .
H18E H 0.809385 0.442644 0.957809 0.079 Uiso 1 1 calc R U . . .
H18F H 0.840236 0.408626 0.979524 0.079 Uiso 1 1 calc R U . . .
C183 C 0.8552(9) 0.4799(12) 0.9592(6) 0.062(6) Uani 1 1 d . U . . .
H18G H 0.847216 0.502572 0.938524 0.074 Uiso 1 1 calc R U . . .
H18H H 0.878298 0.468150 0.959787 0.074 Uiso 1 1 calc R U . . .
C184 C 0.7766(13) 0.3215(16) 0.8678(9) 0.086(8) Uani 1 1 d . U . . .
C185 C 0.7884(13) 0.2734(16) 0.8761(9) 0.093(8) Uani 1 1 d . U . . .
H185 H 0.811175 0.265299 0.876971 0.111 Uiso 1 1 calc R U . . .
C186 C 0.7639(13) 0.2282(18) 0.8846(9) 0.096(8) Uani 1 1 d . U . . .
H186 H 0.771151 0.191664 0.888777 0.115 Uiso 1 1 calc R U . . .
C187 C 0.7335(14) 0.2426(19) 0.8857(10) 0.102(8) Uani 1 1 d . U . . .
H187 H 0.718827 0.216701 0.891905 0.123 Uiso 1 1 calc R U . . .
C188 C 0.7219(14) 0.2993(19) 0.8775(10) 0.106(8) Uani 1 1 d . U . . .
H188 H 0.700819 0.312953 0.879426 0.127 Uiso 1 1 calc R U . . .
C189 C 0.7465(14) 0.3302(19) 0.8662(10) 0.101(8) Uani 1 1 d . U . . .
H189 H 0.738557 0.363553 0.855527 0.121 Uiso 1 1 calc R U . . .
C190 C 0.5487(7) 0.6101(13) 0.6998(9) 0.065(7) Uani 1 1 d . U . . .
H19A H 0.527216 0.627569 0.688897 0.078 Uiso 1 1 calc R U . . .
H19B H 0.559231 0.596827 0.681429 0.078 Uiso 1 1 calc R U . . .
C191 C 0.5428(7) 0.5642(14) 0.7214(9) 0.069(6) Uani 1 1 d . U . . .
H19C H 0.533747 0.578223 0.740601 0.082 Uiso 1 1 calc R U . . .
H19D H 0.564248 0.545928 0.731221 0.082 Uiso 1 1 calc R U . . .
C192 C 0.5174(7) 0.5213(13) 0.7002(10) 0.070(6) Uani 1 1 d . U . . .
H19E H 0.494592 0.536539 0.693525 0.084 Uiso 1 1 calc R U . . .
H19F H 0.524540 0.509511 0.679353 0.084 Uiso 1 1 calc R U . . .
C193 C 0.5191(7) 0.4752(15) 0.7252(10) 0.072(7) Uani 1 1 d . U . . .
H19G H 0.512744 0.489275 0.745984 0.087 Uiso 1 1 calc R U . . .
H19H H 0.542519 0.462720 0.732119 0.087 Uiso 1 1 calc R U . . .
C194 C 0.5301(7) 0.4728(11) 0.5980(7) 0.051(5) Uani 1 1 d . U . . .
H19I H 0.525895 0.492671 0.575964 0.061 Uiso 1 1 calc R U . . .
H19J H 0.538942 0.499184 0.616524 0.061 Uiso 1 1 calc R U . . .
C195 C 0.5562(6) 0.4296(10) 0.5979(7) 0.044(5) Uani 1 1 d . U . . .
H19K H 0.559554 0.407604 0.619053 0.053 Uiso 1 1 calc R U . . .
H19L H 0.548786 0.405144 0.577980 0.053 Uiso 1 1 calc R U . . .
C196 C 0.5883(6) 0.4566(10) 0.5957(6) 0.038(4) Uani 1 1 d . U . . .
H19M H 0.594683 0.483325 0.614566 0.045 Uiso 1 1 calc R U . . .
H19N H 0.585312 0.476364 0.573715 0.045 Uiso 1 1 calc R U . . .
C197 C 0.6164(6) 0.4139(9) 0.5984(6) 0.040(5) Uani 1 1 d . U . . .
H19O H 0.609369 0.385747 0.580588 0.048 Uiso 1 1 calc R U . . .
H19P H 0.620537 0.396033 0.621083 0.048 Uiso 1 1 calc R U . . .
C198 C 0.5739(6) 0.3002(10) 0.6735(7) 0.043(5) Uani 1 1 d . U . . .
H19Q H 0.584922 0.265069 0.671266 0.052 Uiso 1 1 calc R U . . .
H19R H 0.585925 0.328777 0.663790 0.052 Uiso 1 1 calc R U . . .
C199 C 0.5766(6) 0.3120(9) 0.7115(6) 0.039(4) Uani 1 1 d . U . . .
H19S H 0.567227 0.280785 0.721648 0.047 Uiso 1 1 calc R U . . .
H19T H 0.562650 0.344099 0.713331 0.047 Uiso 1 1 calc R U . . .
C200 C 0.6119(5) 0.3227(9) 0.7327(6) 0.035(4) Uani 1 1 d . U . . .
H20A H 0.624407 0.288063 0.735997 0.042 Uiso 1 1 calc R U . . .
H20B H 0.623473 0.347599 0.719840 0.042 Uiso 1 1 calc R U . . .
C201 C 0.6125(5) 0.3461(8) 0.7658(6) 0.033(4) Uani 1 1 d . U . . .
H20C H 0.599302 0.322683 0.777869 0.040 Uiso 1 1 calc R U . . .
H20D H 0.601480 0.382086 0.762420 0.040 Uiso 1 1 calc R U . . .
C202 C 0.8215(10) 0.8032(13) 0.6984(11) 0.091(9) Uani 1 1 d . U . . .
H20E H 0.832655 0.818521 0.681131 0.109 Uiso 1 1 calc R U . . .
H20F H 0.799170 0.790321 0.686173 0.109 Uiso 1 1 calc R U . . .
C203 C 0.8175(9) 0.8420(13) 0.7192(11) 0.086(8) Uani 1 1 d . U . . .
H20G H 0.839252 0.852305 0.734149 0.104 Uiso 1 1 calc R U . . .
H20H H 0.802533 0.829891 0.733946 0.104 Uiso 1 1 calc R U . . .
C204 C 0.8003(8) 0.8960(12) 0.6946(11) 0.079(7) Uani 1 1 d . U . . .
H20I H 0.817046 0.918132 0.686356 0.095 Uiso 1 1 calc R U . . .
H20J H 0.781846 0.885572 0.675211 0.095 Uiso 1 1 calc R U . . .
C205 C 0.7878(7) 0.9240(10) 0.7256(10) 0.069(7) Uani 1 1 d . U . . .
H20K H 0.807351 0.935504 0.743526 0.083 Uiso 1 1 calc R U . . .
H20L H 0.775110 0.897087 0.735987 0.083 Uiso 1 1 calc R U . . .
C206 C 0.6262(8) 0.9605(17) 0.6226(8) 0.073(6) Uani 1 1 d . U . . .
C207 C 0.6128(8) 0.9073(18) 0.6126(8) 0.076(6) Uani 1 1 d . U . . .
H207 H 0.620211 0.877241 0.627165 0.092 Uiso 1 1 calc R U . . .
C208 C 0.5881(9) 0.8983(19) 0.5806(9) 0.083(7) Uani 1 1 d . U . . .
H208 H 0.579521 0.863608 0.572862 0.100 Uiso 1 1 calc R U . . .
C209 C 0.5787(10) 0.946(2) 0.5631(10) 0.093(7) Uani 1 1 d . U . . .
H209 H 0.561286 0.941690 0.543089 0.112 Uiso 1 1 calc R U . . .
C210 C 0.5894(10) 0.994(2) 0.5692(10) 0.096(7) Uani 1 1 d . U . . .
H210 H 0.581965 1.022850 0.553513 0.116 Uiso 1 1 calc R U . . .
C211 C 0.6147(9) 1.0037(19) 0.6027(8) 0.086(7) Uani 1 1 d . U . . .
H211 H 0.622205 1.039303 0.609546 0.103 Uiso 1 1 calc R U . . .
C212 C 0.9167(8) 0.4918(15) 0.5911(8) 0.067(6) Uani 1 1 d . U . . .
C213 C 0.9209(9) 0.4673(16) 0.5623(8) 0.078(6) Uani 1 1 d . U . . .
H213 H 0.929068 0.431136 0.563506 0.094 Uiso 1 1 calc R U . . .
C214 C 0.9136(10) 0.4930(17) 0.5314(9) 0.088(7) Uani 1 1 d . U . . .
H214 H 0.916266 0.474508 0.511412 0.106 Uiso 1 1 calc R U . . .
C215 C 0.9024(9) 0.5464(16) 0.5292(9) 0.079(6) Uani 1 1 d . U . . .
H215 H 0.900029 0.565768 0.508312 0.095 Uiso 1 1 calc R U . . .
C216 C 0.8948(8) 0.5707(17) 0.5566(8) 0.075(6) Uani 1 1 d . U . . .
H216 H 0.884482 0.605368 0.554807 0.090 Uiso 1 1 calc R U . . .
C217 C 0.9029(9) 0.5426(16) 0.5876(9) 0.075(6) Uani 1 1 d . U . . .
H217 H 0.898635 0.559757 0.607396 0.090 Uiso 1 1 calc R U . . .
C218 C 0.8665(7) 0.7211(16) 0.6865(8) 0.066(6) Uani 1 1 d . U . . .
C219 C 0.8667(7) 0.6653(16) 0.6800(8) 0.068(6) Uani 1 1 d . U . . .
H219 H 0.858492 0.641584 0.694936 0.082 Uiso 1 1 calc R U . . .
C220 C 0.8775(8) 0.6435(18) 0.6545(9) 0.079(6) Uani 1 1 d . U . . .
H220 H 0.873585 0.606508 0.648110 0.094 Uiso 1 1 calc R U . . .
C221 C 0.8958(9) 0.680(2) 0.6369(10) 0.091(7) Uani 1 1 d . U . . .
H221 H 0.905883 0.665232 0.619801 0.109 Uiso 1 1 calc R U . . .
C222 C 0.8990(9) 0.732(2) 0.6433(10) 0.091(7) Uani 1 1 d . U . . .
H222 H 0.911371 0.753742 0.631262 0.109 Uiso 1 1 calc R U . . .
C223 C 0.8847(8) 0.7535(19) 0.6673(9) 0.080(6) Uani 1 1 d . U . . .
H223 H 0.886702 0.791507 0.671513 0.097 Uiso 1 1 calc R U . . .
C224 C 0.5356(11) 0.2752(16) 0.6085(10) 0.118(11) Uani 1 1 d D U . . .
C225 C 0.5075(12) 0.2534(17) 0.5860(9) 0.130(11) Uani 1 1 d D U . . .
H225 H 0.489086 0.239600 0.593969 0.156 Uiso 1 1 calc R U . . .
C226 C 0.5079(13) 0.253(2) 0.5507(10) 0.135(11) Uani 1 1 d D U . . .
H226 H 0.489286 0.261707 0.532703 0.163 Uiso 1 1 calc R U . . .
C227 C 0.5395(11) 0.2378(17) 0.5456(11) 0.128(11) Uani 1 1 d D U . . .
H227 H 0.540589 0.210197 0.529328 0.154 Uiso 1 1 calc R U . . .
C228 C 0.5704(11) 0.2621(15) 0.5640(8) 0.120(11) Uani 1 1 d D U . . .
H228 H 0.590445 0.265107 0.556207 0.144 Uiso 1 1 calc R U . . .
C229 C 0.5650(12) 0.2808(16) 0.5960(9) 0.115(11) Uani 1 1 d D U . . .
H229 H 0.583103 0.299070 0.610529 0.138 Uiso 1 1 calc R U . . .
C230 C 0.8396(7) 0.3566(12) 0.8454(8) 0.061(6) Uani 1 1 d . U . . .
C231 C 0.8603(8) 0.3238(14) 0.8690(9) 0.078(7) Uani 1 1 d . U . . .
H231 H 0.855589 0.312828 0.890166 0.094 Uiso 1 1 calc R U . . .
C232 C 0.8907(9) 0.3075(16) 0.8577(10) 0.087(7) Uani 1 1 d . U . . .
H232 H 0.906111 0.282598 0.870926 0.104 Uiso 1 1 calc R U . . .
C233 C 0.8967(10) 0.3298(16) 0.8266(11) 0.089(7) Uani 1 1 d . U . . .
H233 H 0.917491 0.322061 0.821048 0.106 Uiso 1 1 calc R U . . .
C234 C 0.8758(8) 0.3597(14) 0.8055(10) 0.076(6) Uani 1 1 d . U . . .
H234 H 0.880218 0.372944 0.784735 0.091 Uiso 1 1 calc R U . . .
C235 C 0.8456(7) 0.3713(13) 0.8157(8) 0.061(6) Uani 1 1 d . U . . .
H235 H 0.828708 0.390844 0.800199 0.074 Uiso 1 1 calc R U . . .
C236 C 0.6462(9) 1.0284(13) 0.6816(8) 0.067(6) Uani 1 1 d . U . . .
C237 C 0.6161(10) 1.0746(16) 0.7177(10) 0.085(7) Uani 1 1 d . U . . .
H237 H 0.600009 1.074090 0.731300 0.102 Uiso 1 1 calc R U . . .
C238 C 0.6292(11) 1.1183(17) 0.7134(11) 0.094(7) Uani 1 1 d . U . . .
H238 H 0.622158 1.149170 0.724107 0.113 Uiso 1 1 calc R U . . .
C239 C 0.6529(11) 1.1270(17) 0.6945(11) 0.094(7) Uani 1 1 d . U . . .
H239 H 0.663188 1.161222 0.693157 0.113 Uiso 1 1 calc R U . . .
C240 C 0.6608(10) 1.0783(14) 0.6768(9) 0.081(6) Uani 1 1 d . U . . .
H240 H 0.675792 1.080589 0.662050 0.097 Uiso 1 1 calc R U . . .
C241 C 0.6647(9) 0.9981(15) 0.5345(8) 0.075(6) Uani 1 1 d . U . . .
H241 H 0.644050 1.016108 0.533336 0.090 Uiso 1 1 calc R U . . .
C242 C 0.6834(8) 0.9805(14) 0.5649(8) 0.068(6) Uani 1 1 d . U . . .
H242 H 0.676185 0.988416 0.585329 0.082 Uiso 1 1 calc R U . . .
C243 C 0.7117(7) 0.9522(11) 0.5671(6) 0.048(5) Uani 1 1 d . U . . .
C244 C 0.7237(8) 0.9425(12) 0.5373(7) 0.056(5) Uani 1 1 d . U . . .
H244 H 0.744141 0.923932 0.538369 0.068 Uiso 1 1 calc R U . . .
C245 C 0.7045(8) 0.9609(14) 0.5066(7) 0.065(6) Uani 1 1 d . U . . .
H245 H 0.711500 0.953023 0.486128 0.078 Uiso 1 1 calc R U . . .
C246 C 0.8417(10) 0.3401(16) 0.4896(8) 0.077(6) Uani 1 1 d . U . . .
H246 H 0.823591 0.339023 0.470026 0.093 Uiso 1 1 calc R U . . .
C247 C 0.8367(10) 0.3364(14) 0.5209(7) 0.070(6) Uani 1 1 d . U . . .
H247 H 0.814500 0.333891 0.523844 0.084 Uiso 1 1 calc R U . . .
C248 C 0.8644(8) 0.3360(11) 0.5512(6) 0.052(5) Uani 1 1 d . U . . .
C249 C 0.8931(9) 0.3378(14) 0.5461(8) 0.068(6) Uani 1 1 d . U . . .
H249 H 0.911602 0.335099 0.565191 0.082 Uiso 1 1 calc R U . . .
C250 C 0.9325(14) 0.6538(19) 1.0036(12) 0.119(9) Uani 1 1 d . U . . .
H250 H 0.951551 0.676479 1.006284 0.142 Uiso 1 1 calc R U . . .
C251 C 0.9192(13) 0.6308(18) 0.9737(12) 0.110(8) Uani 1 1 d . U . . .
H251 H 0.925957 0.642357 0.953680 0.132 Uiso 1 1 calc R U . . .
C252 C 0.8944(12) 0.5883(15) 0.9712(10) 0.098(8) Uani 1 1 d . U . . .
H252 H 0.884236 0.573165 0.949520 0.117 Uiso 1 1 calc R U . . .
C253 C 0.8856(12) 0.5702(17) 1.0002(10) 0.095(8) Uani 1 1 d . U . . .
C254 C 0.8977(13) 0.5959(17) 1.0281(11) 0.106(8) Uani 1 1 d . U . . .
H254 H 0.892878 0.581528 1.048501 0.127 Uiso 1 1 calc R U . . .
C255 C 0.9173(14) 0.6434(19) 1.0316(12) 0.116(9) Uani 1 1 d . U . . .
H255 H 0.920249 0.666570 1.051033 0.139 Uiso 1 1 calc R U . . .
C256 C 0.9254(8) 0.2078(14) 0.7173(10) 0.073(6) Uani 1 1 d . U . . .
H256 H 0.915794 0.220360 0.735367 0.087 Uiso 1 1 calc R U . . .
C257 C 0.9303(7) 0.2446(13) 0.6938(9) 0.064(6) Uani 1 1 d . U . . .
C258 C 0.9440(8) 0.2256(15) 0.6676(10) 0.075(6) Uani 1 1 d . U . . .
H258 H 0.948005 0.250083 0.650623 0.090 Uiso 1 1 calc R U . . .
C259 C 0.8298(12) 0.6564(17) 1.0622(9) 0.099(8) Uani 1 1 d . U . . .
H259 H 0.827329 0.618064 1.062519 0.118 Uiso 1 1 calc R U . . .
C260 C 0.8109(12) 0.6840(15) 1.0360(8) 0.089(7) Uani 1 1 d . U . . .
C261 C 0.8075(13) 0.7419(17) 1.0390(9) 0.098(8) Uani 1 1 d . U . . .
H261 H 0.792798 0.761886 1.021594 0.118 Uiso 1 1 calc R U . . .
C262 C 0.4207(7) 0.5952(12) 0.5974(9) 0.060(5) Uani 1 1 d . U . . .
H262 H 0.405927 0.625126 0.596064 0.072 Uiso 1 1 calc R U . . .
C263 C 0.4171(7) 0.5486(11) 0.6162(9) 0.060(5) Uani 1 1 d . U . . .
H263 H 0.399289 0.546845 0.627722 0.072 Uiso 1 1 calc R U . . .
C265 C 0.3924(8) 0.4271(17) 0.6779(9) 0.076(6) Uani 1 1 d . U . . .
H265 H 0.375524 0.408325 0.661961 0.091 Uiso 1 1 calc R U . . .
C266 C 0.3838(8) 0.4715(17) 0.6966(9) 0.078(6) Uani 1 1 d . U . . .
H266 H 0.361107 0.481484 0.694429 0.094 Uiso 1 1 calc R U . . .
C267 C 0.8541(13) 0.6815(18) 1.0901(10) 0.105(8) Uani 1 1 d . U . . .
H267 H 0.870513 0.661681 1.105919 0.125 Uiso 1 1 calc R U . . .
C268 C 0.8504(13) 0.7397(18) 1.0912(10) 0.104(8) Uani 1 1 d . U . . .
H268 H 0.865049 0.759874 1.108523 0.125 Uiso 1 1 calc R U . . .
C269 C 0.8256(13) 0.7676(18) 1.0671(10) 0.102(8) Uani 1 1 d . U . . .
H269 H 0.821499 0.804865 1.070688 0.123 Uiso 1 1 calc R U . . .
C270 C 0.8748(10) 0.3456(16) 0.4864(9) 0.079(6) Uani 1 1 d . U . . .
H270 H 0.878424 0.350655 0.464010 0.095 Uiso 1 1 calc R U . . .
C271 C 0.8997(11) 0.3443(16) 0.5106(9) 0.079(6) Uani 1 1 d . U . . .
H271 H 0.921674 0.347217 0.507093 0.095 Uiso 1 1 calc R U . . .
C272 C 0.9523(8) 0.1686(16) 0.6657(11) 0.082(7) Uani 1 1 d . U . . .
H272 H 0.962216 0.154067 0.648392 0.098 Uiso 1 1 calc R U . . .
C273 C 0.9449(9) 0.1396(18) 0.6898(11) 0.089(7) Uani 1 1 d . U . . .
H273 H 0.948479 0.101776 0.687481 0.107 Uiso 1 1 calc R U . . .
C274 C 0.9335(9) 0.1521(16) 0.7168(11) 0.085(7) Uani 1 1 d . U . . .
H274 H 0.930974 0.126839 0.733966 0.102 Uiso 1 1 calc R U . . .
C275 C 0.8594(6) 0.2250(9) 0.6149(6) 0.037(4) Uani 1 1 d . U . . .
H275 H 0.881017 0.234063 0.627874 0.044 Uiso 1 1 calc R U . . .
C276 C 0.8403(6) 0.2638(9) 0.5958(6) 0.034(4) Uani 1 1 d . U . . .
C277 C 0.8075(6) 0.2502(10) 0.5793(7) 0.044(4) Uani 1 1 d . U . . .
H277 H 0.792882 0.277338 0.567376 0.053 Uiso 1 1 calc R U . . .
C278 C 0.4090(8) 0.4997(19) 0.7179(10) 0.085(6) Uani 1 1 d . U . . .
H278 H 0.403739 0.531262 0.729310 0.102 Uiso 1 1 calc R U . . .
C279 C 0.4417(8) 0.4831(18) 0.7232(9) 0.080(6) Uani 1 1 d . U . . .
H279 H 0.458314 0.502972 0.738703 0.096 Uiso 1 1 calc R U . . .
C280 C 0.4511(7) 0.4384(16) 0.7066(8) 0.070(6) Uani 1 1 d . U . . .
C281 C 0.4258(7) 0.4106(15) 0.6827(8) 0.067(6) Uani 1 1 d . U . . .
H281 H 0.431509 0.380893 0.669989 0.081 Uiso 1 1 calc R U . . .
C282 C 0.4684(7) 0.5534(11) 0.5828(8) 0.058(5) Uani 1 1 d . U . . .
H282 H 0.486275 0.555423 0.571535 0.070 Uiso 1 1 calc R U . . .
C283 C 0.4639(6) 0.5055(10) 0.6022(7) 0.048(5) Uani 1 1 d . U . . .
C284 C 0.4388(7) 0.5051(11) 0.6186(8) 0.054(5) Uani 1 1 d . U . . .
H284 H 0.435953 0.474349 0.631948 0.064 Uiso 1 1 calc R U . . .
C285 C 0.7771(8) 1.0748(9) 0.6801(7) 0.053(5) Uani 1 1 d . U . . .
H285 H 0.756173 1.069370 0.664540 0.063 Uiso 1 1 calc R U . . .
C286 C 0.7885(8) 1.0382(9) 0.7067(7) 0.049(5) Uani 1 1 d . U . . .
C287 C 0.8198(8) 1.0444(11) 0.7287(9) 0.062(5) Uani 1 1 d . U . . .
H287 H 0.827966 1.018247 0.745940 0.074 Uiso 1 1 calc R U . . .
C288 C 0.4578(12) 0.349(2) 0.5206(12) 0.100(8) Uani 1 1 d . U . . .
H288 H 0.449434 0.312960 0.519893 0.120 Uiso 1 1 calc R U . . .
C289 C 0.4731(11) 0.371(2) 0.5520(13) 0.101(8) Uani 1 1 d . U . . .
H289 H 0.480948 0.345218 0.569539 0.122 Uiso 1 1 calc R U . . .
C290 C 0.4780(12) 0.418(2) 0.5606(13) 0.102(8) Uani 1 1 d . U . . .
C291 C 0.4710(12) 0.451(2) 0.5279(13) 0.107(8) Uani 1 1 d . U . . .
H291 H 0.475186 0.489396 0.529906 0.129 Uiso 1 1 calc R U . . .
C292 C 0.8387(10) 1.0901(12) 0.7248(10) 0.072(6) Uani 1 1 d . U . . .
H292 H 0.859537 1.095972 0.740463 0.087 Uiso 1 1 calc R U . . .
C293 C 0.8282(9) 1.1259(12) 0.6994(9) 0.067(5) Uani 1 1 d . U . . .
H293 H 0.842249 1.155531 0.697043 0.080 Uiso 1 1 calc R U . . .
C294 C 0.7975(9) 1.1212(10) 0.6765(8) 0.062(5) Uani 1 1 d . U . . .
H294 H 0.790246 1.147513 0.659094 0.074 Uiso 1 1 calc R U . . .
C295 C 0.7059(12) 1.0480(17) 0.7734(8) 0.109(9) Uani 1 1 d D U . . .
H295 H 0.688139 1.073559 0.769885 0.131 Uiso 1 1 calc R U . . .
C297 C 0.7194(13) 1.0320(18) 0.7460(10) 0.105(9) Uani 1 1 d D U . . .
H297 H 0.708553 1.044386 0.723752 0.126 Uiso 1 1 calc R U . . .
C298 C 0.7477(12) 0.9992(16) 0.7485(8) 0.099(8) Uani 1 1 d D U . . .
C299 C 0.4464(7) 0.5959(12) 0.5810(9) 0.062(5) Uani 1 1 d . U . . .
H299 H 0.449206 0.626951 0.567845 0.074 Uiso 1 1 calc R U . . .
C300 C 0.9827(10) 0.3849(18) 0.7795(13) 0.102(8) Uani 1 1 d . U . . .
H300 H 0.980202 0.402104 0.799988 0.122 Uiso 1 1 calc R U . . .
C301 C 0.9568(10) 0.3604(16) 0.7574(12) 0.091(8) Uani 1 1 d . U . . .
H301 H 0.936866 0.354425 0.765156 0.110 Uiso 1 1 calc R U . . .
C302 C 0.9573(10) 0.3442(17) 0.7259(12) 0.092(8) Uani 1 1 d . U . . .
C303 C 0.4734(15) 0.198(2) 0.6951(16) 0.137(10) Uani 1 1 d . U . . .
H303 H 0.456054 0.206242 0.706432 0.164 Uiso 1 1 calc R U . . .
C304 C 0.8474(6) 0.1711(9) 0.6157(6) 0.039(4) Uani 1 1 d . U . . .
H304 H 0.861299 0.143802 0.628249 0.047 Uiso 1 1 calc R U . . .
C305 C 0.8155(6) 0.1587(10) 0.5980(6) 0.040(4) Uani 1 1 d . U . . .
H305 H 0.807392 0.122660 0.598642 0.048 Uiso 1 1 calc R U . . .
C306 C 0.7960(7) 0.1961(10) 0.5803(7) 0.046(5) Uani 1 1 d . U . . .
H306 H 0.774167 0.186735 0.568030 0.055 Uiso 1 1 calc R U . . .
C307 C 0.6767(9) 0.9892(15) 0.5047(8) 0.071(6) Uani 1 1 d . U . . .
H307 H 0.664884 1.003378 0.483263 0.085 Uiso 1 1 calc R U . . .
C308 C 0.4595(12) 0.432(2) 0.4970(13) 0.106(8) Uani 1 1 d . U . . .
H308 H 0.454575 0.454661 0.477490 0.128 Uiso 1 1 calc R U . . .
C309 C 0.4547(12) 0.3741(19) 0.4936(13) 0.103(8) Uani 1 1 d . U . . .
H309 H 0.449514 0.356545 0.471925 0.123 Uiso 1 1 calc R U . . .
C313 C 1.0126(11) 0.3830(19) 0.7700(14) 0.109(8) Uani 1 1 d . U . . .
H313 H 1.032296 0.395212 0.785441 0.131 Uiso 1 1 calc R U . . .
C314 C 1.0140(12) 0.365(2) 0.7404(14) 0.115(8) Uani 1 1 d . U . . .
H314 H 1.033524 0.370213 0.731899 0.138 Uiso 1 1 calc R U . . .
C317 C 0.4887(15) 0.234(2) 0.6722(15) 0.132(10) Uani 1 1 d . U . . .
H317 H 0.473964 0.260820 0.660024 0.158 Uiso 1 1 calc R U . . .
C318 C 0.5152(15) 0.235(2) 0.6668(15) 0.124(9) Uani 1 1 d . U . . .
C319 C 0.5317(16) 0.190(2) 0.6711(16) 0.138(10) Uani 1 1 d . U . . .
H319 H 0.553137 0.191585 0.666026 0.166 Uiso 1 1 calc R U . . .
C320 C 0.5228(11) 0.2989(19) 0.7818(18) 0.21(2) Uani 1 1 d G U . . .
H320 H 0.530964 0.262750 0.782545 0.254 Uiso 1 1 calc R U . . .
C323 C 0.5133(11) 0.326(3) 0.7506(13) 0.21(2) Uani 1 1 d G U . . .
H323 H 0.515053 0.308055 0.730009 0.250 Uiso 1 1 calc R U . . .
C334 C 0.5014(10) 0.379(3) 0.7495(13) 0.21(2) Uani 1 1 d G U . . .
C335 C 0.4989(11) 0.4048(18) 0.7796(19) 0.22(2) Uani 1 1 d G U . . .
H335 H 0.490732 0.440977 0.778841 0.262 Uiso 1 1 calc R U . . .
C336 C 0.5083(13) 0.378(3) 0.8108(13) 0.23(2) Uani 1 1 d G U . . .
H336 H 0.506642 0.395673 0.831378 0.270 Uiso 1 1 calc R U . . .
C337 C 0.5203(10) 0.325(3) 0.8119(12) 0.22(2) Uani 1 1 d G U . . .
H337 H 0.526758 0.306559 0.833230 0.267 Uiso 1 1 calc R U . . .
C328 C 0.9861(11) 0.336(2) 0.7203(14) 0.112(8) Uani 1 1 d . U . . .
H328 H 0.989019 0.311625 0.703016 0.135 Uiso 1 1 calc R U . . .
C329 C 0.5226(16) 0.137(2) 0.6827(16) 0.144(10) Uani 1 1 d . U . . .
H329 H 0.533756 0.103609 0.682243 0.172 Uiso 1 1 calc R U . . .
C330 C 0.4917(15) 0.148(2) 0.6953(16) 0.138(10) Uani 1 1 d . U . . .
H330 H 0.482891 0.117179 0.704799 0.166 Uiso 1 1 calc R U . . .
C331 C 0.7403(12) 0.9822(19) 0.8059(11) 0.120(9) Uani 1 1 d D U . . .
H331 H 0.743325 0.958500 0.825059 0.144 Uiso 1 1 calc R U . . .
C332 C 0.7184(12) 1.0266(18) 0.8055(10) 0.116(9) Uani 1 1 d D U . . .
H332 H 0.712797 1.040503 0.825600 0.140 Uiso 1 1 calc R U . . .
C333 C 0.7584(12) 0.9696(18) 0.7801(9) 0.116(9) Uani 1 1 d D U . . .
H333 H 0.776001 0.943743 0.783694 0.139 Uiso 1 1 calc R U . . .
C338 C 0.7174(19) 0.3766(18) 0.5072(13) 0.18(4) Uani 1 1 d . . . . .
H33C H 0.736553 0.386651 0.497709 0.265 Uiso 1 1 calc R U . . .
H33D H 0.725314 0.365708 0.531191 0.265 Uiso 1 1 calc R U . . .
H33E H 0.702380 0.407765 0.505800 0.265 Uiso 1 1 calc R U . . .
C339 C 0.9726(9) 0.4616(17) 0.6400(11) 0.083(6) Uani 1 1 d . U . . .
C341 C 1.0229(9) 0.5034(19) 0.6454(13) 0.100(7) Uani 1 1 d . U . . .
H341 H 1.027273 0.535246 0.633830 0.120 Uiso 1 1 calc R U . A 1
C342 C 1.0425(10) 0.4644(18) 0.6505(13) 0.099(7) Uani 1 1 d . U . . .
H342 H 1.063216 0.458290 0.666312 0.119 Uiso 1 1 calc R U . B 1
C340 C 0.9930(19) 0.497(4) 0.658(3) 0.088(7) Uani 0.46(3) 1 d . U P C 1
H340 H 0.988625 0.516813 0.677208 0.106 Uiso 0.46(3) 1 calc R U P C 1
C343 C 1.0204(19) 0.428(4) 0.621(3) 0.090(8) Uani 0.46(3) 1 d . U P C 1
H343 H 1.030115 0.414015 0.603196 0.108 Uiso 0.46(3) 1 calc R U P C 1
C344 C 0.9850(18) 0.417(4) 0.620(2) 0.085(8) Uani 0.46(3) 1 d . U P C 1
H344 H 0.972387 0.386597 0.609133 0.102 Uiso 0.46(3) 1 calc R U P C 1
C372 C 1.0295(17) 0.440(3) 0.678(2) 0.096(7) Uani 0.54(3) 1 d . U P C 2
H372 H 1.043587 0.433377 0.699518 0.115 Uiso 0.54(3) 1 calc R U P C 2
C371 C 0.9929(16) 0.427(3) 0.671(2) 0.088(7) Uani 0.54(3) 1 d . U P C 2
H371 H 0.983290 0.401167 0.682920 0.106 Uiso 0.54(3) 1 calc R U P C 2
C370 C 0.9891(17) 0.506(3) 0.628(2) 0.090(7) Uani 0.54(3) 1 d . U P C 2
H370 H 0.979262 0.533010 0.611662 0.108 Uiso 0.54(3) 1 calc R U P C 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 P11 2.453(6) . ?
Ag1 Ag6 2.772(2) . ?
Ag1 Ag3 2.844(2) . ?
Ag1 Ag2 2.856(2) . ?
Ag1 Ag5 2.865(2) . ?
Ag1 Ag7 3.029(2) . ?
Ag1 Ag4 3.033(2) . ?
Ag2 P10 2.462(5) . ?
Ag2 Ag6 2.7762(19) . ?
Ag2 Ag3 2.862(2) . ?
Ag2 Ag10 2.871(2) . ?
Ag2 Ag4 2.990(2) . ?
Ag2 Ag9 2.995(2) . ?
Ag3 P7 2.476(6) . ?
Ag3 Ag6 2.7894(19) . ?
Ag3 Ag8 2.836(2) . ?
Ag3 Ag9 3.057(2) . ?
Ag3 Ag7 3.088(2) . ?
Ag4 O11 2.247(13) . ?
Ag4 Ag6 2.6799(19) . ?
Ag4 Ag10 2.8151(19) . ?
Ag4 Ag18 2.817(2) . ?
Ag4 Ag5 3.0074(19) . ?
Ag4 Ag16 3.0094(19) . ?
Ag4 Ag17 3.0466(19) . ?
Ag5 O10 2.242(13) . ?
Ag5 Ag15 2.6846(19) . ?
Ag5 Ag7 2.7974(19) . ?
Ag5 Ag17 2.9670(19) . ?
Ag5 Ag6 3.0195(19) . ?
Ag5 Ag11 3.0465(19) . ?
Ag5 Ag27 3.1289(19) . ?
Ag6 Ag7 2.6809(19) . ?
Ag6 Ag9 2.681(2) . ?
Ag6 Ag14 2.8526(18) . ?
Ag6 Ag16 2.8588(18) . ?
Ag6 Ag15 2.8755(17) . ?
Ag6 Ag8 2.9866(19) . ?
Ag6 Ag10 3.0580(19) . ?
Ag7 O8 2.257(13) . ?
Ag7 Ag11 2.8582(19) . ?
Ag7 Ag12 2.996(2) . ?
Ag7 Ag15 3.0120(18) . ?
Ag7 Ag8 3.054(2) . ?
Ag8 O7 2.237(12) . ?
Ag8 Ag14 2.687(2) . ?
Ag8 Ag9 2.802(2) . ?
Ag8 Ag12 2.9898(19) . ?
Ag8 Ag13 3.032(2) . ?
Ag8 Ag26 3.059(2) . ?
Ag9 O14 2.247(14) . ?
Ag9 Ag13 2.848(2) . ?
Ag9 Ag10 2.972(2) . ?
Ag9 Ag22 3.018(2) . ?
Ag9 Ag14 3.0381(19) . ?
Ag10 O13 2.239(14) . ?
Ag10 Ag16 2.6818(19) . ?
Ag10 Ag18 2.988(2) . ?
Ag10 Ag22 2.990(2) . ?
Ag10 Ag19 3.004(2) . ?
Ag11 P1 2.471(5) . ?
Ag11 Ag15 2.7730(18) . ?
Ag11 Ag25 2.857(2) . ?
Ag11 Ag27 2.8603(19) . ?
Ag11 Ag12 3.1249(19) . ?
Ag12 O6 2.222(13) . ?
Ag12 Ag15 2.6824(18) . ?
Ag12 Ag24 2.792(2) . ?
Ag12 Ag26 2.874(2) . ?
Ag12 Ag14 2.9982(19) . ?
Ag12 Ag25 3.0593(19) . ?
Ag13 P8 2.460(6) . ?
Ag13 Ag14 2.7679(19) . ?
Ag13 Ag26 2.832(2) . ?
Ag13 Ag23 2.889(2) . ?
Ag13 Ag22 2.998(2) . ?
Ag14 Ag24 2.6713(19) . ?
Ag14 Ag22 2.6806(19) . ?
Ag14 Ag26 2.7865(19) . ?
Ag14 Ag23 2.798(2) . ?
Ag14 Ag16 2.8618(18) . ?
Ag14 Ag15 2.8816(18) . ?
Ag14 Ag21 3.0277(19) . ?
Ag15 Ag28 2.6931(18) . ?
Ag15 Ag27 2.7809(18) . ?
Ag15 Ag25 2.7977(18) . ?
Ag15 Ag16 2.8630(18) . ?
Ag15 Ag24 3.0042(19) . ?
Ag15 Ag17 3.0293(18) . ?
Ag16 Ag17 2.6792(18) . ?
Ag16 Ag21 2.6892(19) . ?
Ag16 Ag19 2.7623(19) . ?
Ag16 Ag20 2.7796(19) . ?
Ag16 Ag18 2.8140(18) . ?
Ag16 Ag28 2.9976(18) . ?
Ag16 Ag22 3.0672(19) . ?
Ag17 O12 2.247(12) . ?
Ag17 Ag28 2.8064(19) . ?
Ag17 Ag27 2.8600(19) . ?
Ag17 Ag20 3.0004(19) . ?
Ag17 Ag18 3.1198(19) . ?
Ag18 P5 2.481(5) . ?
Ag18 Ag20 2.865(2) . ?
Ag18 Ag19 2.871(2) . ?
Ag19 P6 2.455(5) . ?
Ag19 Ag20 2.828(2) . ?
Ag19 Ag22 2.855(2) . ?
Ag19 Ag21 2.990(2) . ?
Ag20 P4 2.466(6) . ?
Ag20 Ag28 2.874(2) . ?
Ag20 Ag21 3.1153(19) . ?
Ag21 O3 2.243(13) . ?
Ag21 Ag22 2.815(2) . ?
Ag21 Ag23 2.8533(19) . ?
Ag21 Ag28 2.9809(19) . ?
Ag21 Ag24 3.025(2) . ?
Ag22 O15 2.288(13) . ?
Ag22 Ag23 3.013(2) . ?
Ag23 P9 2.473(6) . ?
Ag23 Ag26 2.877(2) . ?
Ag23 Ag24 3.059(2) . ?
Ag24 O2 2.217(14) . ?
Ag24 Ag25 2.852(2) . ?
Ag24 Ag28 3.0298(19) . ?
Ag24 Ag26 3.069(2) . ?
Ag25 P2 2.480(5) . ?
Ag25 Ag27 2.8640(18) . ?
Ag25 Ag28 3.1380(19) . ?
Ag26 P12 2.476(5) . ?
Ag27 P3 2.472(5) . ?
Ag27 Ag28 2.997(2) . ?
Ag28 O4 2.224(13) . ?
Ag29 P21 2.445(10) . ?
Ag29 P19 2.449(10) . ?
Ag29 P20 2.468(7) . ?
Ag29 O16 2.505(15) . ?
Ag30 P24 2.465(6) . ?
Ag30 P22 2.469(7) . ?
Ag30 P23 2.500(8) . ?
Ag31 P15 2.456(12) . ?
Ag31 P13 2.488(9) . ?
Ag31 P14 2.504(9) . ?
Ag32 P18 2.469(6) . ?
Ag32 P17 2.470(7) . ?
Ag32 P16 2.478(6) . ?
Mo1 O9 1.730(13) . ?
Mo1 O11 1.767(13) . ?
Mo1 O10 1.772(13) . ?
Mo1 O12 1.797(13) . ?
Mo2 O16 1.768(15) . ?
Mo2 O14 1.791(15) . ?
Mo2 O15 1.791(14) . ?
Mo2 O13 1.809(15) . ?
Mo3 O5 1.728(14) . ?
Mo3 O8 1.763(15) . ?
Mo3 O7 1.787(14) . ?
Mo3 O6 1.813(14) . ?
Mo4 O1 1.735(13) . ?
Mo4 O2 1.776(14) . ?
Mo4 O3 1.777(14) . ?
Mo4 O4 1.789(13) . ?
P1 C45 1.81(2) . ?
P1 C7 1.81(2) . ?
P1 C1 1.83(2) . ?
P2 C62 1.78(2) . ?
P2 C197 1.84(3) . ?
P2 C63 1.85(2) . ?
P3 C19 1.83(2) . ?
P3 C25 1.83(2) . ?
P3 C31 1.847(19) . ?
P4 C76 1.82(3) . ?
P4 C111 1.83(2) . ?
P4 C190 1.87(3) . ?
P5 C166 1.81(2) . ?
P5 C56 1.83(2) . ?
P5 C110 1.85(2) . ?
P6 C117 1.80(3) . ?
P6 C179 1.80(2) . ?
P6 C93 1.82(3) . ?
P7 C52 1.80(2) . ?
P7 C142 1.84(4) . ?
P7 C160 1.84(3) . ?
P8 C180 1.80(3) . ?
P8 C184 1.81(4) . ?
P8 C230 1.89(3) . ?
P9 C130 1.81(2) . ?
P9 C124 1.82(3) . ?
P9 C201 1.84(2) . ?
P10 C100 1.80(3) . ?
P10 C172 1.82(3) . ?
P10 C154 1.85(3) . ?
P11 C148 1.80(3) . ?
P11 C218 1.81(3) . ?
P11 C202 1.81(3) . ?
P12 C35 1.83(2) . ?
P12 C41 1.83(2) . ?
P12 C74 1.84(2) . ?
P13 C224 1.75(5) . ?
P13 C198 1.78(2) . ?
P13 C318 1.88(5) . ?
P14 C194 1.83(3) . ?
P14 C283 1.84(2) . ?
P14 C290 1.84(5) . ?
P15 C193 1.75(3) . ?
P15 C280 1.80(3) . ?
P15 C334 1.83(4) . ?
P16 C236 1.81(3) . ?
P16 C206 1.82(3) . ?
P16 C53 1.84(2) . ?
P17 C298 1.76(4) . ?
P17 C286 1.80(2) . ?
P17 C205 1.81(3) . ?
P18 C243 1.82(3) . ?
P18 C13 1.82(2) . ?
P18 C34 1.85(2) . ?
P19 C360 1.75(6) . ?
P19 C136 1.75(4) . ?
P19 C176 1.79(3) . ?
P20 C260 1.79(3) . ?
P20 C175 1.81(3) . ?
P20 C81 1.88(4) . ?
P21 C253 1.82(4) . ?
P21 C87 1.82(3) . ?
P21 C183 1.84(3) . ?
P22 C257 1.84(3) . ?
P22 C302 1.87(4) . ?
P22 C44 1.88(2) . ?
P23 C339 1.81(4) . ?
P23 C212 1.81(3) . ?
P23 C49 1.81(3) . ?
P24 C248 1.81(2) . ?
P24 C48 1.82(2) . ?
P24 C276 1.84(2) . ?
O18 N1 1.29(6) . ?
O19 N1 1.07(6) . ?
O20 N1 1.31(6) . ?
O21 N3 1.41(3) . ?
O22 C338 1.48(7) . ?
O23 N4 1.43(3) . ?
O24 N4 1.43(3) . ?
O25 N4 1.42(3) . ?
O26 N3 1.40(3) . ?
O27 N3 1.42(3) . ?
C1 C6 1.32(3) . ?
C1 C2 1.39(4) . ?
C2 C3 1.34(4) . ?
C3 C4 1.43(4) . ?
C4 C5 1.35(4) . ?
C5 C6 1.35(3) . ?
C7 C12 1.35(3) . ?
C7 C8 1.48(3) . ?
C8 C9 1.36(3) . ?
C9 C10 1.33(3) . ?
C10 C11 1.41(4) . ?
C11 C12 1.34(3) . ?
C13 C18 1.37(3) . ?
C13 C14 1.38(3) . ?
C14 C15 1.40(3) . ?
C15 C16 1.35(3) . ?
C16 C17 1.41(3) . ?
C17 C18 1.39(3) . ?
C19 C20 1.40(3) . ?
C19 C24 1.40(3) . ?
C20 C21 1.36(3) . ?
C21 C22 1.45(4) . ?
C22 C23 1.37(4) . ?
C23 C24 1.34(4) . ?
C25 C30 1.37(3) . ?
C25 C26 1.41(3) . ?
C26 C27 1.38(3) . ?
C27 C28 1.34(4) . ?
C28 C29 1.36(4) . ?
C29 C30 1.38(4) . ?
C31 C32 1.50(3) . ?
C32 C33 1.52(3) . ?
C33 C34 1.51(3) . ?
C35 C40 1.34(3) . ?
C35 C36 1.43(4) . ?
C36 C37 1.33(4) . ?
C37 C38 1.40(4) . ?
C38 C39 1.33(4) . ?
C39 C40 1.43(3) . ?
C41 C42 1.54(3) . ?
C365 C364 1.41(3) . ?
C365 C362 1.45(3) . ?
C364 C363 1.41(3) . ?
C363 C361 1.43(3) . ?
C362 C360 1.43(3) . ?
C361 C360 1.43(3) . ?
C42 C43 1.52(3) . ?
C43 C44 1.46(4) . ?
C45 C46 1.52(3) . ?
C46 C47 1.48(3) . ?
C47 C48 1.55(3) . ?
C49 C50 1.57(4) . ?
C50 C51 1.53(3) . ?
C51 C52 1.52(4) . ?
C53 C54 1.44(3) . ?
C54 C55 1.53(3) . ?
C55 C56 1.51(3) . ?
C57 C62 1.38(3) . ?
C57 C58 1.40(3) . ?
C58 C59 1.38(4) . ?
C59 C60 1.32(4) . ?
C60 C61 1.36(4) . ?
C61 C62 1.43(3) . ?
C63 C64 1.35(3) . ?
C63 C68 1.39(3) . ?
C64 C65 1.43(4) . ?
C65 C66 1.36(4) . ?
C66 C67 1.38(4) . ?
C67 C68 1.41(3) . ?
C69 C74 1.36(4) . ?
C69 C70 1.39(4) . ?
C70 C71 1.38(4) . ?
C71 C72 1.38(4) . ?
C72 C73 1.37(4) . ?
C73 C74 1.42(3) . ?
C75 C76 1.35(4) . ?
C75 C80 1.38(4) . ?
C76 C77 1.35(4) . ?
C77 C78 1.44(5) . ?
C78 C79 1.17(4) . ?
C79 C80 1.35(4) . ?
C81 C86 1.26(5) . ?
C81 C82 1.33(4) . ?
C82 C83 1.40(6) . ?
C83 C84 1.42(6) . ?
C84 C85 1.41(5) . ?
C85 C86 1.50(6) . ?
C87 C88 1.35(6) . ?
C87 C92 1.42(6) . ?
C88 C89 1.46(5) . ?
C89 C90 1.46(6) . ?
C90 C91 1.36(6) . ?
C91 C92 1.36(5) . ?
C93 C94 1.39(4) . ?
C93 C98 1.41(4) . ?
C94 C95 1.40(4) . ?
C95 C96 1.41(4) . ?
C96 C97 1.40(5) . ?
C97 C98 1.37(4) . ?
C99 C100 1.36(4) . ?
C99 C104 1.43(3) . ?
C100 C101 1.42(3) . ?
C101 C102 1.38(4) . ?
C102 C103 1.43(4) . ?
C103 C104 1.37(4) . ?
C105 C106 1.39(4) . ?
C105 C110 1.40(3) . ?
C106 C107 1.39(4) . ?
C107 C108 1.32(4) . ?
C108 C109 1.47(4) . ?
C109 C110 1.41(3) . ?
C111 C112 1.37(4) . ?
C111 C116 1.38(3) . ?
C112 C113 1.42(4) . ?
C113 C114 1.28(4) . ?
C114 C115 1.36(4) . ?
C115 C116 1.36(4) . ?
C117 C122 1.37(4) . ?
C117 C118 1.42(4) . ?
C118 C119 1.44(4) . ?
C119 C120 1.30(5) . ?
C120 C121 1.31(5) . ?
C121 C122 1.42(4) . ?
C123 C237 1.39(5) . ?
C123 C236 1.41(4) . ?
C124 C125 1.40(4) . ?
C124 C129 1.42(4) . ?
C125 C126 1.41(4) . ?
C126 C127 1.37(4) . ?
C127 C128 1.39(5) . ?
C128 C129 1.28(4) . ?
C130 C135 1.38(4) . ?
C130 C131 1.40(4) . ?
C131 C132 1.43(4) . ?
C132 C133 1.30(5) . ?
C133 C134 1.39(5) . ?
C134 C135 1.45(4) . ?
C136 C141 1.31(4) . ?
C136 C137 1.42(6) . ?
C137 C138 1.44(6) . ?
C138 C139 1.42(5) . ?
C139 C140 1.39(5) . ?
C140 C141 1.40(6) . ?
C142 C147 1.35(4) . ?
C142 C143 1.41(5) . ?
C143 C144 1.39(5) . ?
C144 C145 1.37(5) . ?
C145 C146 1.25(5) . ?
C146 C147 1.34(5) . ?
C148 C149 1.26(4) . ?
C148 C153 1.42(3) . ?
C149 C150 1.29(5) . ?
C150 C151 1.42(4) . ?
C151 C152 1.25(5) . ?
C152 C153 1.37(4) . ?
C154 C159 1.33(5) . ?
C154 C155 1.44(5) . ?
C155 C156 1.37(5) . ?
C156 C157 1.44(6) . ?
C157 C158 1.34(6) . ?
C158 C159 1.45(5) . ?
C160 C165 1.36(5) . ?
C160 C161 1.39(4) . ?
C161 C162 1.35(5) . ?
C162 C163 1.27(6) . ?
C163 C164 1.46(6) . ?
C164 C165 1.44(5) . ?
C166 C167 1.39(4) . ?
C166 C171 1.41(3) . ?
C167 C168 1.40(3) . ?
C168 C169 1.39(4) . ?
C169 C170 1.32(4) . ?
C170 C171 1.39(4) . ?
C172 C173 1.56(3) . ?
C173 C174 1.57(4) . ?
C174 C175 1.62(4) . ?
C176 C177 1.46(5) . ?
C177 C178 1.55(4) . ?
C178 C179 1.56(3) . ?
C180 C181 1.54(3) . ?
C181 C182 1.58(4) . ?
C182 C183 1.53(4) . ?
C184 C189 1.24(6) . ?
C184 C185 1.30(6) . ?
C185 C186 1.59(6) . ?
C186 C187 1.31(6) . ?
C187 C188 1.49(7) . ?
C188 C189 1.42(6) . ?
C190 C191 1.48(4) . ?
C191 C192 1.59(4) . ?
C192 C193 1.51(5) . ?
C194 C195 1.51(3) . ?
C195 C196 1.50(3) . ?
C196 C197 1.55(3) . ?
C198 C199 1.53(4) . ?
C199 C200 1.53(3) . ?
C200 C201 1.44(3) . ?
C202 C203 1.30(5) . ?
C203 C204 1.71(5) . ?
C204 C205 1.61(5) . ?
C206 C211 1.35(5) . ?
C206 C207 1.44(5) . ?
C207 C208 1.46(5) . ?
C208 C209 1.37(6) . ?
C209 C210 1.28(6) . ?
C210 C211 1.52(5) . ?
C212 C213 1.35(5) . ?
C212 C217 1.37(5) . ?
C213 C214 1.36(5) . ?
C214 C215 1.39(5) . ?
C215 C216 1.34(5) . ?
C216 C217 1.40(4) . ?
C218 C219 1.40(5) . ?
C218 C223 1.43(5) . ?
C219 C220 1.32(5) . ?
C220 C221 1.45(5) . ?
C221 C222 1.30(6) . ?
C222 C223 1.35(5) . ?
C224 C225 1.40(3) . ?
C224 C229 1.42(3) . ?
C225 C226 1.42(3) . ?
C226 C227 1.41(3) . ?
C227 C228 1.44(3) . ?
C228 C229 1.43(3) . ?
C230 C235 1.32(5) . ?
C230 C231 1.38(4) . ?
C231 C232 1.48(5) . ?
C232 C233 1.44(6) . ?
C233 C234 1.29(5) . ?
C234 C235 1.42(5) . ?
C236 C240 1.40(5) . ?
C237 C238 1.23(6) . ?
C238 C239 1.38(6) . ?
C239 C240 1.47(5) . ?
C241 C242 1.36(4) . ?
C241 C307 1.41(4) . ?
C242 C243 1.35(4) . ?
C243 C244 1.41(4) . ?
C244 C245 1.38(4) . ?
C245 C307 1.33(4) . ?
C246 C247 1.32(4) . ?
C246 C270 1.41(5) . ?
C247 C248 1.46(4) . ?
C248 C249 1.25(4) . ?
C249 C271 1.51(4) . ?
C250 C251 1.33(6) . ?
C250 C255 1.43(7) . ?
C251 C252 1.45(6) . ?
C252 C253 1.37(6) . ?
C253 C254 1.28(5) . ?
C254 C255 1.41(6) . ?
C256 C257 1.36(5) . ?
C256 C274 1.41(5) . ?
C257 C258 1.38(4) . ?
C258 C272 1.45(5) . ?
C259 C260 1.34(5) . ?
C259 C267 1.46(5) . ?
C260 C261 1.44(5) . ?
C261 C269 1.36(5) . ?
C262 C299 1.37(4) . ?
C262 C263 1.40(4) . ?
C263 C284 1.39(4) . ?
C265 C281 1.40(4) . ?
C265 C266 1.42(5) . ?
C266 C278 1.37(5) . ?
C267 C268 1.44(6) . ?
C268 C269 1.41(6) . ?
C270 C271 1.24(5) . ?
C272 C273 1.29(6) . ?
C273 C274 1.31(6) . ?
C275 C276 1.36(3) . ?
C275 C304 1.42(3) . ?
C276 C277 1.40(3) . ?
C277 C306 1.42(4) . ?
C278 C279 1.38(5) . ?
C279 C280 1.39(5) . ?
C280 C281 1.42(4) . ?
C282 C299 1.37(4) . ?
C282 C283 1.45(4) . ?
C283 C284 1.34(4) . ?
C285 C286 1.39(4) . ?
C285 C294 1.44(4) . ?
C286 C287 1.39(4) . ?
C287 C292 1.40(4) . ?
C288 C309 1.23(6) . ?
C288 C289 1.38(6) . ?
C289 C290 1.20(6) . ?
C290 C291 1.53(7) . ?
C291 C308 1.31(6) . ?
C292 C293 1.34(5) . ?
C293 C294 1.39(5) . ?
C295 C332 1.38(3) . ?
C295 C297 1.40(3) . ?
C297 C298 1.40(6) . ?
C298 C333 1.44(3) . ?
C300 C301 1.36(5) . ?
C300 C313 1.37(6) . ?
C301 C302 1.33(6) . ?
C302 C328 1.27(6) . ?
C303 C330 1.45(8) . ?
C303 C317 1.52(7) . ?
C304 C305 1.38(4) . ?
C305 C306 1.32(3) . ?
C308 C309 1.43(6) . ?
C313 C314 1.28(7) . ?
C314 C328 1.43(6) . ?
C317 C318 1.16(7) . ?
C318 C319 1.29(7) . ?
C319 C329 1.46(7) . ?
C320 C323 1.3900 . ?
C320 C337 1.3900 . ?
C323 C334 1.3900 . ?
C334 C335 1.3900 . ?
C335 C336 1.3900 . ?
C336 C337 1.3900 . ?
C329 C330 1.49(8) . ?
C331 C332 1.41(3) . ?
C331 C333 1.44(3) . ?
C339 C340 1.32(10) . ?
C339 C370 1.44(9) . ?
C339 C344 1.52(9) . ?
C339 C371 1.56(9) . ?
C341 C342 1.24(5) . ?
C341 C370 1.41(8) . ?
C341 C340 1.44(9) . ?
C341 C372 2.00(10) . ?
C342 C372 1.45(9) . ?
C342 C343 1.60(10) . ?
C343 C344 1.48(10) . ?
C372 C371 1.50(9) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P11 Ag1 Ag6 173.24(19) . . ?
P11 Ag1 Ag3 126.14(16) . . ?
Ag6 Ag1 Ag3 59.54(5) . . ?
P11 Ag1 Ag2 126.0(2) . . ?
Ag6 Ag1 Ag2 59.09(5) . . ?
Ag3 Ag1 Ag2 60.28(5) . . ?
P11 Ag1 Ag5 108.52(19) . . ?
Ag6 Ag1 Ag5 64.74(5) . . ?
Ag3 Ag1 Ag5 113.86(6) . . ?
Ag2 Ag1 Ag5 114.99(6) . . ?
P11 Ag1 Ag7 122.7(2) . . ?
Ag6 Ag1 Ag7 54.83(5) . . ?
Ag3 Ag1 Ag7 63.34(5) . . ?
Ag2 Ag1 Ag7 107.62(6) . . ?
Ag5 Ag1 Ag7 56.58(4) . . ?
P11 Ag1 Ag4 122.27(17) . . ?
Ag6 Ag1 Ag4 54.76(5) . . ?
Ag3 Ag1 Ag4 106.83(6) . . ?
Ag2 Ag1 Ag4 60.95(5) . . ?
Ag5 Ag1 Ag4 61.23(5) . . ?
Ag7 Ag1 Ag4 99.01(5) . . ?
P10 Ag2 Ag6 171.52(18) . . ?
P10 Ag2 Ag1 128.92(17) . . ?
Ag6 Ag2 Ag1 58.95(5) . . ?
P10 Ag2 Ag3 125.94(16) . . ?
Ag6 Ag2 Ag3 59.28(5) . . ?
Ag1 Ag2 Ag3 59.66(5) . . ?
P10 Ag2 Ag10 106.32(17) . . ?
Ag6 Ag2 Ag10 65.54(5) . . ?
Ag1 Ag2 Ag10 113.77(6) . . ?
Ag3 Ag2 Ag10 116.37(6) . . ?
P10 Ag2 Ag4 123.30(16) . . ?
Ag6 Ag2 Ag4 55.24(5) . . ?
Ag1 Ag2 Ag4 62.46(5) . . ?
Ag3 Ag2 Ag4 107.52(6) . . ?
Ag10 Ag2 Ag4 57.36(5) . . ?
P10 Ag2 Ag9 119.50(16) . . ?
Ag6 Ag2 Ag9 55.20(5) . . ?
Ag1 Ag2 Ag9 107.35(6) . . ?
Ag3 Ag2 Ag9 62.87(5) . . ?
Ag10 Ag2 Ag9 60.84(5) . . ?
Ag4 Ag2 Ag9 99.42(6) . . ?
P7 Ag3 Ag6 170.85(18) . . ?
P7 Ag3 Ag8 107.16(16) . . ?
Ag6 Ag3 Ag8 64.13(5) . . ?
P7 Ag3 Ag1 129.93(18) . . ?
Ag6 Ag3 Ag1 58.94(5) . . ?
Ag8 Ag3 Ag1 115.37(6) . . ?
P7 Ag3 Ag2 125.68(16) . . ?
Ag6 Ag3 Ag2 58.82(5) . . ?
Ag8 Ag3 Ag2 111.58(7) . . ?
Ag1 Ag3 Ag2 60.05(5) . . ?
P7 Ag3 Ag9 119.23(17) . . ?
Ag6 Ag3 Ag9 54.36(5) . . ?
Ag8 Ag3 Ag9 56.63(5) . . ?
Ag1 Ag3 Ag9 106.00(6) . . ?
Ag2 Ag3 Ag9 60.69(5) . . ?
P7 Ag3 Ag7 125.68(16) . . ?
Ag6 Ag3 Ag7 53.99(4) . . ?
Ag8 Ag3 Ag7 61.90(5) . . ?
Ag1 Ag3 Ag7 61.25(5) . . ?
Ag2 Ag3 Ag7 105.90(6) . . ?
Ag9 Ag3 Ag7 98.83(5) . . ?
O11 Ag4 Ag6 148.7(3) . . ?
O11 Ag4 Ag10 142.4(3) . . ?
Ag6 Ag4 Ag10 67.58(5) . . ?
O11 Ag4 Ag18 92.4(3) . . ?
Ag6 Ag4 Ag18 115.30(6) . . ?
Ag10 Ag4 Ag18 64.10(5) . . ?
O11 Ag4 Ag2 121.4(3) . . ?
Ag6 Ag4 Ag2 58.32(5) . . ?
Ag10 Ag4 Ag2 59.19(5) . . ?
Ag18 Ag4 Ag2 119.82(6) . . ?
O11 Ag4 Ag5 89.4(3) . . ?
Ag6 Ag4 Ag5 63.83(5) . . ?
Ag10 Ag4 Ag5 127.63(6) . . ?
Ag18 Ag4 Ag5 122.73(6) . . ?
Ag2 Ag4 Ag5 107.11(6) . . ?
O11 Ag4 Ag16 137.1(3) . . ?
Ag6 Ag4 Ag16 60.00(5) . . ?
Ag10 Ag4 Ag16 54.71(4) . . ?
Ag18 Ag4 Ag16 57.65(5) . . ?
Ag2 Ag4 Ag16 100.86(6) . . ?
Ag5 Ag4 Ag16 84.13(5) . . ?
O11 Ag4 Ag1 94.7(3) . . ?
Ag6 Ag4 Ag1 57.66(5) . . ?
Ag10 Ag4 Ag1 110.16(6) . . ?
Ag18 Ag4 Ag1 172.88(7) . . ?
Ag2 Ag4 Ag1 56.60(5) . . ?
Ag5 Ag4 Ag1 56.63(5) . . ?
Ag16 Ag4 Ag1 115.90(6) . . ?
O11 Ag4 Ag17 88.3(3) . . ?
Ag6 Ag4 Ag17 90.85(5) . . ?
Ag10 Ag4 Ag17 104.86(6) . . ?
Ag18 Ag4 Ag17 64.15(5) . . ?
Ag2 Ag4 Ag17 148.34(6) . . ?
Ag5 Ag4 Ag17 58.69(4) . . ?
Ag16 Ag4 Ag17 52.51(4) . . ?
Ag1 Ag4 Ag17 115.19(6) . . ?
O10 Ag5 Ag15 147.9(4) . . ?
O10 Ag5 Ag7 143.8(3) . . ?
Ag15 Ag5 Ag7 66.62(5) . . ?
O10 Ag5 Ag1 94.3(4) . . ?
Ag15 Ag5 Ag1 114.12(6) . . ?
Ag7 Ag5 Ag1 64.66(5) . . ?
O10 Ag5 Ag17 87.8(3) . . ?
Ag15 Ag5 Ag17 64.60(5) . . ?
Ag7 Ag5 Ag17 128.25(6) . . ?
Ag1 Ag5 Ag17 123.29(6) . . ?
O10 Ag5 Ag4 88.1(3) . . ?
Ag15 Ag5 Ag4 92.18(5) . . ?
Ag7 Ag5 Ag4 105.10(6) . . ?
Ag1 Ag5 Ag4 62.14(5) . . ?
Ag17 Ag5 Ag4 61.32(5) . . ?
O10 Ag5 Ag6 137.8(4) . . ?
Ag15 Ag5 Ag6 60.21(4) . . ?
Ag7 Ag5 Ag6 54.73(4) . . ?
Ag1 Ag5 Ag6 56.13(5) . . ?
Ag17 Ag5 Ag6 86.11(5) . . ?
Ag4 Ag5 Ag6 52.80(4) . . ?
O10 Ag5 Ag11 121.3(4) . . ?
Ag15 Ag5 Ag11 57.46(4) . . ?
Ag7 Ag5 Ag11 58.38(4) . . ?
Ag1 Ag5 Ag11 120.14(6) . . ?
Ag17 Ag5 Ag11 105.91(5) . . ?
Ag4 Ag5 Ag11 148.68(6) . . ?
Ag6 Ag5 Ag11 100.43(5) . . ?
O10 Ag5 Ag27 95.0(4) . . ?
Ag15 Ag5 Ag27 56.53(4) . . ?
Ag7 Ag5 Ag27 107.85(5) . . ?
Ag1 Ag5 Ag27 170.57(6) . . ?
Ag17 Ag5 Ag27 55.89(4) . . ?
Ag4 Ag5 Ag27 116.89(6) . . ?
Ag6 Ag5 Ag27 115.21(5) . . ?
Ag11 Ag5 Ag27 55.17(4) . . ?
Ag4 Ag6 Ag7 118.62(7) . . ?
Ag4 Ag6 Ag9 116.78(6) . . ?
Ag7 Ag6 Ag9 120.99(7) . . ?
Ag4 Ag6 Ag1 67.58(5) . . ?
Ag7 Ag6 Ag1 67.46(6) . . ?
Ag9 Ag6 Ag1 119.66(7) . . ?
Ag4 Ag6 Ag2 66.44(5) . . ?
Ag7 Ag6 Ag2 121.03(7) . . ?
Ag9 Ag6 Ag2 66.55(5) . . ?
Ag1 Ag6 Ag2 61.96(5) . . ?
Ag4 Ag6 Ag3 119.34(6) . . ?
Ag7 Ag6 Ag3 68.69(5) . . ?
Ag9 Ag6 Ag3 67.92(6) . . ?
Ag1 Ag6 Ag3 61.52(5) . . ?
Ag2 Ag6 Ag3 61.90(5) . . ?
Ag4 Ag6 Ag14 125.78(6) . . ?
Ag7 Ag6 Ag14 95.54(6) . . ?
Ag9 Ag6 Ag14 66.52(5) . . ?
Ag1 Ag6 Ag14 162.88(7) . . ?
Ag2 Ag6 Ag14 130.77(7) . . ?
Ag3 Ag6 Ag14 111.59(6) . . ?
Ag4 Ag6 Ag16 65.73(5) . . ?
Ag7 Ag6 Ag16 125.37(6) . . ?
Ag9 Ag6 Ag16 94.67(6) . . ?
Ag1 Ag6 Ag16 130.88(6) . . ?
Ag2 Ag6 Ag16 110.31(6) . . ?
Ag3 Ag6 Ag16 162.47(7) . . ?
Ag14 Ag6 Ag16 60.14(5) . . ?
Ag4 Ag6 Ag15 95.26(6) . . ?
Ag7 Ag6 Ag15 65.54(5) . . ?
Ag9 Ag6 Ag15 126.91(6) . . ?
Ag1 Ag6 Ag15 111.15(6) . . ?
Ag2 Ag6 Ag15 161.66(7) . . ?
Ag3 Ag6 Ag15 131.95(6) . . ?
Ag14 Ag6 Ag15 60.40(4) . . ?
Ag16 Ag6 Ag15 59.90(4) . . ?
Ag4 Ag6 Ag8 175.56(7) . . ?
Ag7 Ag6 Ag8 64.95(5) . . ?
Ag9 Ag6 Ag8 58.96(5) . . ?
Ag1 Ag6 Ag8 112.90(6) . . ?
Ag2 Ag6 Ag8 109.67(6) . . ?
Ag3 Ag6 Ag8 58.70(5) . . ?
Ag14 Ag6 Ag8 54.73(5) . . ?
Ag16 Ag6 Ag8 114.85(6) . . ?
Ag15 Ag6 Ag8 88.66(5) . . ?
Ag4 Ag6 Ag5 63.37(5) . . ?
Ag7 Ag6 Ag5 58.42(5) . . ?
Ag9 Ag6 Ag5 178.72(7) . . ?
Ag1 Ag6 Ag5 59.12(5) . . ?
Ag2 Ag6 Ag5 112.64(6) . . ?
Ag3 Ag6 Ag5 110.86(6) . . ?
Ag14 Ag6 Ag5 114.52(6) . . ?
Ag16 Ag6 Ag5 86.54(5) . . ?
Ag15 Ag6 Ag5 54.11(4) . . ?
Ag8 Ag6 Ag5 120.86(6) . . ?
Ag4 Ag6 Ag10 58.32(5) . . ?
Ag7 Ag6 Ag10 176.92(7) . . ?
Ag9 Ag6 Ag10 61.98(5) . . ?
Ag1 Ag6 Ag10 110.63(6) . . ?
Ag2 Ag6 Ag10 58.73(5) . . ?
Ag3 Ag6 Ag10 112.78(6) . . ?
Ag14 Ag6 Ag10 86.44(5) . . ?
Ag16 Ag6 Ag10 53.78(4) . . ?
Ag15 Ag6 Ag10 113.68(6) . . ?
Ag8 Ag6 Ag10 118.12(6) . . ?
Ag5 Ag6 Ag10 118.60(6) . . ?
O8 Ag7 Ag6 147.3(4) . . ?
O8 Ag7 Ag5 144.3(4) . . ?
Ag6 Ag7 Ag5 66.86(5) . . ?
O8 Ag7 Ag11 93.9(4) . . ?
Ag6 Ag7 Ag11 114.57(6) . . ?
Ag5 Ag7 Ag11 65.18(5) . . ?
O8 Ag7 Ag12 88.0(4) . . ?
Ag6 Ag7 Ag12 90.21(5) . . ?
Ag5 Ag7 Ag12 106.23(5) . . ?
Ag11 Ag7 Ag12 64.47(5) . . ?
O8 Ag7 Ag15 137.3(4) . . ?
Ag6 Ag7 Ag15 60.34(4) . . ?
Ag5 Ag7 Ag15 54.90(4) . . ?
Ag11 Ag7 Ag15 56.30(4) . . ?
Ag12 Ag7 Ag15 53.03(4) . . ?
O8 Ag7 Ag1 121.5(4) . . ?
Ag6 Ag7 Ag1 57.71(5) . . ?
Ag5 Ag7 Ag1 58.76(5) . . ?
Ag11 Ag7 Ag1 120.99(6) . . ?
Ag12 Ag7 Ag1 147.45(6) . . ?
Ag15 Ag7 Ag1 100.92(5) . . ?
O8 Ag7 Ag8 89.1(4) . . ?
Ag6 Ag7 Ag8 62.37(5) . . ?
Ag5 Ag7 Ag8 126.39(6) . . ?
Ag11 Ag7 Ag8 123.44(6) . . ?
Ag12 Ag7 Ag8 59.22(5) . . ?
Ag15 Ag7 Ag8 84.97(5) . . ?
Ag1 Ag7 Ag8 104.23(6) . . ?
O8 Ag7 Ag3 94.0(4) . . ?
Ag6 Ag7 Ag3 57.32(5) . . ?
Ag5 Ag7 Ag3 108.70(6) . . ?
Ag11 Ag7 Ag3 171.86(6) . . ?
Ag12 Ag7 Ag3 114.13(6) . . ?
Ag15 Ag7 Ag3 116.05(6) . . ?
Ag1 Ag7 Ag3 55.42(5) . . ?
Ag8 Ag7 Ag3 55.00(5) . . ?
O7 Ag8 Ag14 151.0(3) . . ?
O7 Ag8 Ag9 140.9(3) . . ?
Ag14 Ag8 Ag9 67.18(5) . . ?
O7 Ag8 Ag3 89.5(4) . . ?
Ag14 Ag8 Ag3 115.29(6) . . ?
Ag9 Ag8 Ag3 65.67(5) . . ?
O7 Ag8 Ag6 135.3(4) . . ?
Ag14 Ag8 Ag6 60.09(5) . . ?
Ag9 Ag8 Ag6 55.07(5) . . ?
Ag3 Ag8 Ag6 57.18(5) . . ?
O7 Ag8 Ag12 91.0(3) . . ?
Ag14 Ag8 Ag12 63.50(5) . . ?
Ag9 Ag8 Ag12 127.50(6) . . ?
Ag3 Ag8 Ag12 122.42(6) . . ?
Ag6 Ag8 Ag12 84.75(5) . . ?
O7 Ag8 Ag13 123.6(4) . . ?
Ag14 Ag8 Ag13 57.52(5) . . ?
Ag9 Ag8 Ag13 58.28(5) . . ?
Ag3 Ag8 Ag13 121.02(6) . . ?
Ag6 Ag8 Ag13 100.26(6) . . ?
Ag12 Ag8 Ag13 105.81(6) . . ?
O7 Ag8 Ag7 87.2(4) . . ?
Ag14 Ag8 Ag7 90.89(5) . . ?
Ag9 Ag8 Ag7 105.59(6) . . ?
Ag3 Ag8 Ag7 63.10(5) . . ?
Ag6 Ag8 Ag7 52.68(4) . . ?
Ag12 Ag8 Ag7 59.43(4) . . ?
Ag13 Ag8 Ag7 147.62(6) . . ?
O7 Ag8 Ag26 97.6(4) . . ?
Ag14 Ag8 Ag26 57.59(5) . . ?
Ag9 Ag8 Ag26 108.70(6) . . ?
Ag3 Ag8 Ag26 172.81(7) . . ?
Ag6 Ag8 Ag26 116.19(6) . . ?
Ag12 Ag8 Ag26 56.73(5) . . ?
Ag13 Ag8 Ag26 55.42(5) . . ?
Ag7 Ag8 Ag26 116.02(6) . . ?
O14 Ag9 Ag6 141.7(4) . . ?
O14 Ag9 Ag8 147.6(4) . . ?
Ag6 Ag9 Ag8 65.97(5) . . ?
O14 Ag9 Ag13 102.2(4) . . ?
Ag6 Ag9 Ag13 113.29(6) . . ?
Ag8 Ag9 Ag13 64.90(5) . . ?
O14 Ag9 Ag10 84.6(4) . . ?
Ag6 Ag9 Ag10 65.25(5) . . ?
Ag8 Ag9 Ag10 127.74(6) . . ?
Ag13 Ag9 Ag10 121.10(7) . . ?
O14 Ag9 Ag2 86.2(4) . . ?
Ag6 Ag9 Ag2 58.25(5) . . ?
Ag8 Ag9 Ag2 108.71(6) . . ?
Ag13 Ag9 Ag2 171.52(7) . . ?
Ag10 Ag9 Ag2 57.52(5) . . ?
O14 Ag9 Ag22 92.7(4) . . ?
Ag6 Ag9 Ag22 91.83(6) . . ?
Ag8 Ag9 Ag22 104.66(6) . . ?
Ag13 Ag9 Ag22 61.39(5) . . ?
Ag10 Ag9 Ag22 59.87(5) . . ?
Ag2 Ag9 Ag22 117.19(6) . . ?
O14 Ag9 Ag14 144.0(4) . . ?
Ag6 Ag9 Ag14 59.45(5) . . ?
Ag8 Ag9 Ag14 54.60(5) . . ?
Ag13 Ag9 Ag14 55.99(4) . . ?
Ag10 Ag9 Ag14 84.73(5) . . ?
Ag2 Ag9 Ag14 116.02(6) . . ?
Ag22 Ag9 Ag14 52.54(4) . . ?
O14 Ag9 Ag3 116.1(4) . . ?
Ag6 Ag9 Ag3 57.72(5) . . ?
Ag8 Ag9 Ag3 57.71(5) . . ?
Ag13 Ag9 Ag3 119.76(6) . . ?
Ag10 Ag9 Ag3 107.80(6) . . ?
Ag2 Ag9 Ag3 56.44(5) . . ?
Ag22 Ag9 Ag3 148.41(6) . . ?
Ag14 Ag9 Ag3 99.91(6) . . ?
O13 Ag10 Ag16 141.0(4) . . ?
O13 Ag10 Ag4 147.8(4) . . ?
Ag16 Ag10 Ag4 66.34(5) . . ?
O13 Ag10 Ag2 103.6(4) . . ?
Ag16 Ag10 Ag2 112.74(6) . . ?
Ag4 Ag10 Ag2 63.44(5) . . ?
O13 Ag10 Ag9 93.0(4) . . ?
Ag16 Ag10 Ag9 92.09(5) . . ?
Ag4 Ag10 Ag9 104.12(6) . . ?
Ag2 Ag10 Ag9 61.64(5) . . ?
O13 Ag10 Ag18 114.9(4) . . ?
Ag16 Ag10 Ag18 59.21(5) . . ?
Ag4 Ag10 Ag18 57.98(5) . . ?
Ag2 Ag10 Ag18 118.08(6) . . ?
Ag9 Ag10 Ag18 149.82(6) . . ?
O13 Ag10 Ag22 84.0(4) . . ?
Ag16 Ag10 Ag22 65.22(5) . . ?
Ag4 Ag10 Ag22 128.12(6) . . ?
Ag2 Ag10 Ag22 122.25(6) . . ?
Ag9 Ag10 Ag22 60.83(5) . . ?
Ag18 Ag10 Ag22 108.81(6) . . ?
O13 Ag10 Ag19 85.9(4) . . ?
Ag16 Ag10 Ag19 57.81(5) . . ?
Ag4 Ag10 Ag19 108.92(6) . . ?
Ag2 Ag10 Ag19 170.46(7) . . ?
Ag9 Ag10 Ag19 117.48(6) . . ?
Ag18 Ag10 Ag19 57.25(5) . . ?
Ag22 Ag10 Ag19 56.90(5) . . ?
O13 Ag10 Ag6 144.7(4) . . ?
Ag16 Ag10 Ag6 59.31(4) . . ?
Ag4 Ag10 Ag6 54.11(4) . . ?
Ag2 Ag10 Ag6 55.73(5) . . ?
Ag9 Ag10 Ag6 52.77(4) . . ?
Ag18 Ag10 Ag6 100.36(5) . . ?
Ag22 Ag10 Ag6 85.38(5) . . ?
Ag19 Ag10 Ag6 115.53(6) . . ?
P1 Ag11 Ag15 170.49(14) . . ?
P1 Ag11 Ag25 129.61(14) . . ?
Ag15 Ag11 Ag25 59.57(5) . . ?
P1 Ag11 Ag7 106.41(14) . . ?
Ag15 Ag11 Ag7 64.65(5) . . ?
Ag25 Ag11 Ag7 114.97(6) . . ?
P1 Ag11 Ag27 125.68(13) . . ?
Ag15 Ag11 Ag27 59.14(5) . . ?
Ag25 Ag11 Ag27 60.12(5) . . ?
Ag7 Ag11 Ag27 113.93(6) . . ?
P1 Ag11 Ag5 118.32(14) . . ?
Ag15 Ag11 Ag5 54.70(4) . . ?
Ag25 Ag11 Ag5 108.23(6) . . ?
Ag7 Ag11 Ag5 56.45(4) . . ?
Ag27 Ag11 Ag5 63.88(5) . . ?
P1 Ag11 Ag12 125.85(13) . . ?
Ag15 Ag11 Ag12 53.70(4) . . ?
Ag25 Ag11 Ag12 61.32(5) . . ?
Ag7 Ag11 Ag12 59.91(5) . . ?
Ag27 Ag11 Ag12 105.74(6) . . ?
Ag5 Ag11 Ag12 97.37(5) . . ?
O6 Ag12 Ag15 149.7(4) . . ?
O6 Ag12 Ag24 142.2(4) . . ?
Ag15 Ag12 Ag24 66.53(5) . . ?
O6 Ag12 Ag26 91.6(3) . . ?
Ag15 Ag12 Ag26 115.12(6) . . ?
Ag24 Ag12 Ag26 65.57(5) . . ?
O6 Ag12 Ag8 87.5(3) . . ?
Ag15 Ag12 Ag8 92.33(5) . . ?
Ag24 Ag12 Ag8 105.96(6) . . ?
Ag26 Ag12 Ag8 62.84(5) . . ?
O6 Ag12 Ag7 90.0(4) . . ?
Ag15 Ag12 Ag7 63.78(5) . . ?
Ag24 Ag12 Ag7 127.57(6) . . ?
Ag26 Ag12 Ag7 124.02(6) . . ?
Ag8 Ag12 Ag7 61.35(5) . . ?
O6 Ag12 Ag14 136.7(3) . . ?
Ag15 Ag12 Ag14 60.66(4) . . ?
Ag24 Ag12 Ag14 54.81(5) . . ?
Ag26 Ag12 Ag14 56.61(5) . . ?
Ag8 Ag12 Ag14 53.32(4) . . ?
Ag7 Ag12 Ag14 86.27(5) . . ?
O6 Ag12 Ag25 121.6(3) . . ?
Ag15 Ag12 Ag25 57.88(4) . . ?
Ag24 Ag12 Ag25 58.14(5) . . ?
Ag26 Ag12 Ag25 120.40(6) . . ?
Ag8 Ag12 Ag25 149.36(6) . . ?
Ag7 Ag12 Ag25 105.47(5) . . ?
Ag14 Ag12 Ag25 100.90(5) . . ?
O6 Ag12 Ag11 96.9(3) . . ?
Ag15 Ag12 Ag11 56.43(4) . . ?
Ag24 Ag12 Ag11 107.33(6) . . ?
Ag26 Ag12 Ag11 171.39(6) . . ?
Ag8 Ag12 Ag11 116.76(6) . . ?
Ag7 Ag12 Ag11 55.62(4) . . ?
Ag14 Ag12 Ag11 115.67(5) . . ?
Ag25 Ag12 Ag11 55.02(4) . . ?
P8 Ag13 Ag14 171.71(18) . . ?
P8 Ag13 Ag26 126.88(16) . . ?
Ag14 Ag13 Ag26 59.67(5) . . ?
P8 Ag13 Ag9 106.22(17) . . ?
Ag14 Ag13 Ag9 65.49(5) . . ?
Ag26 Ag13 Ag9 114.04(6) . . ?
P8 Ag13 Ag23 127.4(2) . . ?
Ag14 Ag13 Ag23 59.24(5) . . ?
Ag26 Ag13 Ag23 60.38(5) . . ?
Ag9 Ag13 Ag23 116.23(6) . . ?
P8 Ag13 Ag22 121.58(17) . . ?
Ag14 Ag13 Ag22 55.23(5) . . ?
Ag26 Ag13 Ag22 107.55(6) . . ?
Ag9 Ag13 Ag22 62.11(5) . . ?
Ag23 Ag13 Ag22 61.54(5) . . ?
P8 Ag13 Ag8 121.5(2) . . ?
Ag14 Ag13 Ag8 54.97(5) . . ?
Ag26 Ag13 Ag8 62.77(5) . . ?
Ag9 Ag13 Ag8 56.82(5) . . ?
Ag23 Ag13 Ag8 107.55(6) . . ?
Ag22 Ag13 Ag8 99.69(6) . . ?
Ag24 Ag14 Ag22 119.18(7) . . ?
Ag24 Ag14 Ag8 119.05(6) . . ?
Ag22 Ag14 Ag8 118.33(7) . . ?
Ag24 Ag14 Ag13 120.99(6) . . ?
Ag22 Ag14 Ag13 66.75(5) . . ?
Ag8 Ag14 Ag13 67.51(5) . . ?
Ag24 Ag14 Ag26 68.40(5) . . ?
Ag22 Ag14 Ag26 118.73(6) . . ?
Ag8 Ag14 Ag26 67.92(5) . . ?
Ag13 Ag14 Ag26 61.32(5) . . ?
Ag24 Ag14 Ag23 67.97(5) . . ?
Ag22 Ag14 Ag23 66.69(5) . . ?
Ag8 Ag14 Ag23 121.11(6) . . ?
Ag13 Ag14 Ag23 62.53(5) . . ?
Ag26 Ag14 Ag23 62.03(5) . . ?
Ag24 Ag14 Ag6 125.53(6) . . ?
Ag22 Ag14 Ag6 95.60(6) . . ?
Ag8 Ag14 Ag6 65.17(5) . . ?
Ag13 Ag14 Ag6 110.53(6) . . ?
Ag26 Ag14 Ag6 131.04(7) . . ?
Ag23 Ag14 Ag6 162.25(7) . . ?
Ag24 Ag14 Ag16 94.64(6) . . ?
Ag22 Ag14 Ag16 67.11(5) . . ?
Ag8 Ag14 Ag16 125.18(6) . . ?
Ag13 Ag14 Ag16 131.33(6) . . ?
Ag26 Ag14 Ag16 162.94(7) . . ?
Ag23 Ag14 Ag16 110.89(6) . . ?
Ag6 Ag14 Ag16 60.04(4) . . ?
Ag24 Ag14 Ag15 65.38(5) . . ?
Ag22 Ag14 Ag15 126.86(6) . . ?
Ag8 Ag14 Ag15 94.68(6) . . ?
Ag13 Ag14 Ag15 162.12(7) . . ?
Ag26 Ag14 Ag15 111.69(6) . . ?
Ag23 Ag14 Ag15 130.93(6) . . ?
Ag6 Ag14 Ag15 60.19(4) . . ?
Ag16 Ag14 Ag15 59.80(4) . . ?
Ag24 Ag14 Ag12 58.67(5) . . ?
Ag22 Ag14 Ag12 177.39(7) . . ?
Ag8 Ag14 Ag12 63.18(5) . . ?
Ag13 Ag14 Ag12 112.75(6) . . ?
Ag26 Ag14 Ag12 59.45(5) . . ?
Ag23 Ag14 Ag12 110.74(6) . . ?
Ag6 Ag14 Ag12 86.98(5) . . ?
Ag16 Ag14 Ag12 114.04(6) . . ?
Ag15 Ag14 Ag12 54.24(4) . . ?
Ag24 Ag14 Ag21 63.76(5) . . ?
Ag22 Ag14 Ag21 58.72(5) . . ?
Ag8 Ag14 Ag21 177.04(7) . . ?
Ag13 Ag14 Ag21 110.49(6) . . ?
Ag26 Ag14 Ag21 113.29(6) . . ?
Ag23 Ag14 Ag21 58.49(5) . . ?
Ag6 Ag14 Ag21 114.27(5) . . ?
Ag16 Ag14 Ag21 54.25(4) . . ?
Ag15 Ag14 Ag21 87.36(5) . . ?
Ag12 Ag14 Ag21 119.78(6) . . ?
Ag24 Ag14 Ag9 177.27(7) . . ?
Ag22 Ag14 Ag9 63.35(5) . . ?
Ag8 Ag14 Ag9 58.22(5) . . ?
Ag13 Ag14 Ag9 58.52(5) . . ?
Ag26 Ag14 Ag9 109.69(6) . . ?
Ag23 Ag14 Ag9 113.09(6) . . ?
Ag6 Ag14 Ag9 54.04(5) . . ?
Ag16 Ag14 Ag9 87.32(5) . . ?
Ag15 Ag14 Ag9 114.23(6) . . ?
Ag12 Ag14 Ag9 118.77(6) . . ?
Ag21 Ag14 Ag9 118.97(6) . . ?
Ag12 Ag15 Ag5 119.47(6) . . ?
Ag12 Ag15 Ag28 120.13(6) . . ?
Ag5 Ag15 Ag28 118.16(6) . . ?
Ag12 Ag15 Ag11 69.87(5) . . ?
Ag5 Ag15 Ag11 67.84(5) . . ?
Ag28 Ag15 Ag11 120.74(6) . . ?
Ag12 Ag15 Ag27 121.82(6) . . ?
Ag5 Ag15 Ag27 69.82(5) . . ?
Ag28 Ag15 Ag27 66.36(5) . . ?
Ag11 Ag15 Ag27 62.00(5) . . ?
Ag12 Ag15 Ag25 67.83(5) . . ?
Ag5 Ag15 Ag25 121.54(6) . . ?
Ag28 Ag15 Ag25 69.68(5) . . ?
Ag11 Ag15 Ag25 61.71(5) . . ?
Ag27 Ag15 Ag25 61.78(5) . . ?
Ag12 Ag15 Ag16 124.85(6) . . ?
Ag5 Ag15 Ag16 93.15(5) . . ?
Ag28 Ag15 Ag16 65.22(5) . . ?
Ag11 Ag15 Ag16 160.85(7) . . ?
Ag27 Ag15 Ag16 110.35(6) . . ?
Ag25 Ag15 Ag16 132.45(6) . . ?
Ag12 Ag15 Ag6 92.83(5) . . ?
Ag5 Ag15 Ag6 65.68(5) . . ?
Ag28 Ag15 Ag6 124.97(6) . . ?
Ag11 Ag15 Ag6 111.21(6) . . ?
Ag27 Ag15 Ag6 133.23(6) . . ?
Ag25 Ag15 Ag6 160.59(6) . . ?
Ag16 Ag15 Ag6 59.76(4) . . ?
Ag12 Ag15 Ag14 65.10(5) . . ?
Ag5 Ag15 Ag14 125.08(6) . . ?
Ag28 Ag15 Ag14 93.99(6) . . ?
Ag11 Ag15 Ag14 132.89(6) . . ?
Ag27 Ag15 Ag14 160.22(6) . . ?
Ag25 Ag15 Ag14 110.65(6) . . ?
Ag16 Ag15 Ag14 59.76(4) . . ?
Ag6 Ag15 Ag14 59.40(4) . . ?
Ag12 Ag15 Ag24 58.48(5) . . ?
Ag5 Ag15 Ag24 177.86(6) . . ?
Ag28 Ag15 Ag24 63.98(5) . . ?
Ag11 Ag15 Ag24 111.27(6) . . ?
Ag27 Ag15 Ag24 111.62(6) . . ?
Ag25 Ag15 Ag24 58.77(5) . . ?
Ag16 Ag15 Ag24 87.81(5) . . ?
Ag6 Ag15 Ag24 113.30(5) . . ?
Ag14 Ag15 Ag24 53.94(4) . . ?
Ag12 Ag15 Ag7 63.19(5) . . ?
Ag5 Ag15 Ag7 58.48(5) . . ?
Ag28 Ag15 Ag7 176.62(7) . . ?
Ag11 Ag15 Ag7 59.04(4) . . ?
Ag27 Ag15 Ag7 111.64(6) . . ?
Ag25 Ag15 Ag7 112.05(6) . . ?
Ag16 Ag15 Ag7 113.82(5) . . ?
Ag6 Ag15 Ag7 54.11(4) . . ?
Ag14 Ag15 Ag7 88.10(5) . . ?
Ag24 Ag15 Ag7 119.38(6) . . ?
Ag12 Ag15 Ag17 178.26(7) . . ?
Ag5 Ag15 Ag17 62.22(5) . . ?
Ag28 Ag15 Ag17 58.38(5) . . ?
Ag11 Ag15 Ag17 111.56(6) . . ?
Ag27 Ag15 Ag17 58.79(4) . . ?
Ag25 Ag15 Ag17 111.82(5) . . ?
Ag16 Ag15 Ag17 54.00(4) . . ?
Ag6 Ag15 Ag17 87.56(5) . . ?
Ag14 Ag15 Ag17 113.75(5) . . ?
Ag24 Ag15 Ag17 119.82(5) . . ?
Ag7 Ag15 Ag17 118.32(6) . . ?
Ag17 Ag16 Ag10 120.23(6) . . ?
Ag17 Ag16 Ag21 118.97(6) . . ?
Ag10 Ag16 Ag21 117.11(6) . . ?
Ag17 Ag16 Ag19 120.42(6) . . ?
Ag10 Ag16 Ag19 66.95(5) . . ?
Ag21 Ag16 Ag19 66.51(5) . . ?
Ag17 Ag16 Ag20 66.66(5) . . ?
Ag10 Ag16 Ag20 118.31(6) . . ?
Ag21 Ag16 Ag20 69.43(5) . . ?
Ag19 Ag16 Ag20 61.36(5) . . ?
Ag17 Ag16 Ag18 69.16(5) . . ?
Ag10 Ag16 Ag18 65.83(5) . . ?
Ag21 Ag16 Ag18 120.75(6) . . ?
Ag19 Ag16 Ag18 61.96(5) . . ?
Ag20 Ag16 Ag18 61.61(5) . . ?
Ag17 Ag16 Ag6 95.07(6) . . ?
Ag10 Ag16 Ag6 66.91(5) . . ?
Ag21 Ag16 Ag6 125.83(6) . . ?
Ag19 Ag16 Ag6 131.61(6) . . ?
Ag20 Ag16 Ag6 161.41(7) . . ?
Ag18 Ag16 Ag6 109.91(6) . . ?
Ag17 Ag16 Ag14 126.60(6) . . ?
Ag10 Ag16 Ag14 93.82(6) . . ?
Ag21 Ag16 Ag14 66.02(5) . . ?
Ag19 Ag16 Ag14 110.05(6) . . ?
Ag20 Ag16 Ag14 133.48(6) . . ?
Ag18 Ag16 Ag14 159.60(7) . . ?
Ag6 Ag16 Ag14 59.82(5) . . ?
Ag17 Ag16 Ag15 66.17(5) . . ?
Ag10 Ag16 Ag15 127.25(6) . . ?
Ag21 Ag16 Ag15 94.62(5) . . ?
Ag19 Ag16 Ag15 161.05(7) . . ?
Ag20 Ag16 Ag15 111.74(6) . . ?
Ag18 Ag16 Ag15 132.62(6) . . ?
Ag6 Ag16 Ag15 60.34(4) . . ?
Ag14 Ag16 Ag15 60.44(4) . . ?
Ag17 Ag16 Ag28 58.94(5) . . ?
Ag10 Ag16 Ag28 177.79(7) . . ?
Ag21 Ag16 Ag28 62.95(5) . . ?
Ag19 Ag16 Ag28 111.49(6) . . ?
Ag20 Ag16 Ag28 59.52(5) . . ?
Ag18 Ag16 Ag28 112.12(6) . . ?
Ag6 Ag16 Ag28 114.99(5) . . ?
Ag14 Ag16 Ag28 88.20(5) . . ?
Ag15 Ag16 Ag28 54.66(4) . . ?
Ag17 Ag16 Ag4 64.46(5) . . ?
Ag10 Ag16 Ag4 58.96(5) . . ?
Ag21 Ag16 Ag4 176.00(6) . . ?
Ag19 Ag16 Ag4 110.21(6) . . ?
Ag20 Ag16 Ag4 111.36(6) . . ?
Ag18 Ag16 Ag4 57.74(5) . . ?
Ag6 Ag16 Ag4 54.27(4) . . ?
Ag14 Ag16 Ag4 114.03(6) . . ?
Ag15 Ag16 Ag4 88.71(5) . . ?
Ag28 Ag16 Ag4 120.95(6) . . ?
Ag17 Ag16 Ag22 177.00(7) . . ?
Ag10 Ag16 Ag22 62.24(5) . . ?
Ag21 Ag16 Ag22 58.11(5) . . ?
Ag19 Ag16 Ag22 58.37(5) . . ?
Ag20 Ag16 Ag22 110.87(6) . . ?
Ag18 Ag16 Ag22 111.42(6) . . ?
Ag6 Ag16 Ag22 87.50(5) . . ?
Ag14 Ag16 Ag22 53.62(4) . . ?
Ag15 Ag16 Ag22 114.03(5) . . ?
Ag28 Ag16 Ag22 118.53(6) . . ?
Ag4 Ag16 Ag22 118.43(6) . . ?
O12 Ag17 Ag16 145.6(4) . . ?
O12 Ag17 Ag28 145.2(4) . . ?
Ag16 Ag17 Ag28 66.20(5) . . ?
O12 Ag17 Ag27 98.0(3) . . ?
Ag16 Ag17 Ag27 113.49(6) . . ?
Ag28 Ag17 Ag27 63.85(5) . . ?
O12 Ag17 Ag5 90.3(3) . . ?
Ag16 Ag17 Ag5 90.97(5) . . ?
Ag28 Ag17 Ag5 106.05(6) . . ?
Ag27 Ag17 Ag5 64.92(5) . . ?
O12 Ag17 Ag20 117.6(3) . . ?
Ag16 Ag17 Ag20 58.27(5) . . ?
Ag28 Ag17 Ag20 59.21(5) . . ?
Ag27 Ag17 Ag20 119.74(6) . . ?
Ag5 Ag17 Ag20 148.80(6) . . ?
O12 Ag17 Ag15 140.7(3) . . ?
Ag16 Ag17 Ag15 59.83(4) . . ?
Ag28 Ag17 Ag15 54.81(4) . . ?
Ag27 Ag17 Ag15 56.26(4) . . ?
Ag5 Ag17 Ag15 53.18(4) . . ?
Ag20 Ag17 Ag15 101.55(5) . . ?
O12 Ag17 Ag4 88.3(3) . . ?
Ag16 Ag17 Ag4 63.03(5) . . ?
Ag28 Ag17 Ag4 126.46(6) . . ?
Ag27 Ag17 Ag4 124.56(6) . . ?
Ag5 Ag17 Ag4 60.00(5) . . ?
Ag20 Ag17 Ag4 104.55(6) . . ?
Ag15 Ag17 Ag4 85.05(5) . . ?
O12 Ag17 Ag18 91.0(3) . . ?
Ag16 Ag17 Ag18 57.46(4) . . ?
Ag28 Ag17 Ag18 108.82(6) . . ?
Ag27 Ag17 Ag18 170.86(6) . . ?
Ag5 Ag17 Ag18 114.25(6) . . ?
Ag20 Ag17 Ag18 55.77(5) . . ?
Ag15 Ag17 Ag18 115.43(5) . . ?
Ag4 Ag17 Ag18 54.35(4) . . ?
P5 Ag18 Ag16 172.26(14) . . ?
P5 Ag18 Ag4 107.67(14) . . ?
Ag16 Ag18 Ag4 64.61(5) . . ?
P5 Ag18 Ag20 128.03(14) . . ?
Ag16 Ag18 Ag20 58.61(5) . . ?
Ag4 Ag18 Ag20 114.67(6) . . ?
P5 Ag18 Ag19 127.54(14) . . ?
Ag16 Ag18 Ag19 58.13(5) . . ?
Ag4 Ag18 Ag19 112.75(6) . . ?
Ag20 Ag18 Ag19 59.08(5) . . ?
P5 Ag18 Ag10 121.29(14) . . ?
Ag16 Ag18 Ag10 54.96(5) . . ?
Ag4 Ag18 Ag10 57.93(5) . . ?
Ag20 Ag18 Ag10 106.46(6) . . ?
Ag19 Ag18 Ag10 61.64(5) . . ?
P5 Ag18 Ag17 124.44(14) . . ?
Ag16 Ag18 Ag17 53.38(4) . . ?
Ag4 Ag18 Ag17 61.50(5) . . ?
Ag20 Ag18 Ag17 60.00(5) . . ?
Ag19 Ag18 Ag17 103.98(5) . . ?
Ag10 Ag18 Ag17 99.07(5) . . ?
P6 Ag19 Ag16 172.39(16) . . ?
P6 Ag19 Ag20 127.53(17) . . ?
Ag16 Ag19 Ag20 59.62(5) . . ?
P6 Ag19 Ag22 106.53(15) . . ?
Ag16 Ag19 Ag22 66.16(5) . . ?
Ag20 Ag19 Ag22 115.92(6) . . ?
P6 Ag19 Ag18 124.58(15) . . ?
Ag16 Ag19 Ag18 59.90(5) . . ?
Ag20 Ag19 Ag18 60.35(5) . . ?
Ag22 Ag19 Ag18 116.19(7) . . ?
P6 Ag19 Ag21 123.08(15) . . ?
Ag16 Ag19 Ag21 55.57(5) . . ?
Ag20 Ag19 Ag21 64.68(5) . . ?
Ag22 Ag19 Ag21 57.53(5) . . ?
Ag18 Ag19 Ag21 109.41(6) . . ?
P6 Ag19 Ag10 120.09(17) . . ?
Ag16 Ag19 Ag10 55.24(5) . . ?
Ag20 Ag19 Ag10 107.01(6) . . ?
Ag22 Ag19 Ag10 61.30(5) . . ?
Ag18 Ag19 Ag10 61.11(5) . . ?
Ag21 Ag19 Ag10 99.72(6) . . ?
P4 Ag20 Ag16 172.80(17) . . ?
P4 Ag20 Ag19 127.53(16) . . ?
Ag16 Ag20 Ag19 59.02(5) . . ?
P4 Ag20 Ag18 124.87(16) . . ?
Ag16 Ag20 Ag18 59.79(5) . . ?
Ag19 Ag20 Ag18 60.57(5) . . ?
P4 Ag20 Ag28 108.94(16) . . ?
Ag16 Ag20 Ag28 64.02(5) . . ?
Ag19 Ag20 Ag28 113.30(6) . . ?
Ag18 Ag20 Ag28 114.37(6) . . ?
P4 Ag20 Ag17 120.50(15) . . ?
Ag16 Ag20 Ag17 55.07(4) . . ?
Ag19 Ag20 Ag17 108.21(6) . . ?
Ag18 Ag20 Ag17 64.22(5) . . ?
Ag28 Ag20 Ag17 57.03(4) . . ?
P4 Ag20 Ag21 124.84(15) . . ?
Ag16 Ag20 Ag21 53.92(4) . . ?
Ag19 Ag20 Ag21 60.18(5) . . ?
Ag18 Ag20 Ag21 106.20(6) . . ?
Ag28 Ag20 Ag21 59.54(5) . . ?
Ag17 Ag20 Ag21 98.24(5) . . ?
O3 Ag21 Ag16 148.6(3) . . ?
O3 Ag21 Ag22 142.8(4) . . ?
Ag16 Ag21 Ag22 67.69(5) . . ?
O3 Ag21 Ag23 92.3(3) . . ?
Ag16 Ag21 Ag23 114.47(6) . . ?
Ag22 Ag21 Ag23 64.22(5) . . ?
O3 Ag21 Ag28 88.5(4) . . ?
Ag16 Ag21 Ag28 63.59(5) . . ?
Ag22 Ag21 Ag28 128.14(6) . . ?
Ag23 Ag21 Ag28 123.11(6) . . ?
O3 Ag21 Ag19 123.3(4) . . ?
Ag16 Ag21 Ag19 57.92(5) . . ?
Ag22 Ag21 Ag19 58.83(5) . . ?
Ag23 Ag21 Ag19 120.20(6) . . ?
Ag28 Ag21 Ag19 105.81(5) . . ?
O3 Ag21 Ag24 87.3(4) . . ?
Ag16 Ag21 Ag24 90.63(5) . . ?
Ag22 Ag21 Ag24 104.38(6) . . ?
Ag23 Ag21 Ag24 62.63(5) . . ?
Ag28 Ag21 Ag24 60.59(5) . . ?
Ag19 Ag21 Ag24 147.55(6) . . ?
O3 Ag21 Ag14 136.2(4) . . ?
Ag16 Ag21 Ag14 59.73(5) . . ?
Ag22 Ag21 Ag14 54.47(5) . . ?
Ag23 Ag21 Ag14 56.73(5) . . ?
Ag28 Ag21 Ag14 85.50(5) . . ?
Ag19 Ag21 Ag14 99.96(6) . . ?
Ag24 Ag21 Ag14 52.38(4) . . ?
O3 Ag21 Ag20 96.7(3) . . ?
Ag16 Ag21 Ag20 56.65(5) . . ?
Ag22 Ag21 Ag20 108.54(6) . . ?
Ag23 Ag21 Ag20 170.99(7) . . ?
Ag28 Ag21 Ag20 56.20(4) . . ?
Ag19 Ag21 Ag20 55.14(5) . . ?
Ag24 Ag21 Ag20 116.45(6) . . ?
Ag14 Ag21 Ag20 115.06(5) . . ?
O15 Ag22 Ag14 140.2(4) . . ?
O15 Ag22 Ag21 148.8(4) . . ?
Ag14 Ag22 Ag21 66.81(5) . . ?
O15 Ag22 Ag19 103.7(4) . . ?
Ag14 Ag22 Ag19 112.68(6) . . ?
Ag21 Ag22 Ag19 63.64(5) . . ?
O15 Ag22 Ag10 92.4(4) . . ?
Ag14 Ag22 Ag10 91.01(6) . . ?
Ag21 Ag22 Ag10 104.21(6) . . ?
Ag19 Ag22 Ag10 61.80(5) . . ?
O15 Ag22 Ag13 85.2(4) . . ?
Ag14 Ag22 Ag13 58.02(5) . . ?
Ag21 Ag22 Ag13 110.03(6) . . ?
Ag19 Ag22 Ag13 170.69(7) . . ?
Ag10 Ag22 Ag13 115.66(6) . . ?
O15 Ag22 Ag23 116.0(4) . . ?
Ag14 Ag22 Ag23 58.52(5) . . ?
Ag21 Ag22 Ag23 58.51(5) . . ?
Ag19 Ag22 Ag23 119.36(6) . . ?
Ag10 Ag22 Ag23 148.42(6) . . ?
Ag13 Ag22 Ag23 57.45(5) . . ?
O15 Ag22 Ag9 84.0(4) . . ?
Ag14 Ag22 Ag9 64.11(5) . . ?
Ag21 Ag22 Ag9 127.19(6) . . ?
Ag19 Ag22 Ag9 120.84(6) . . ?
Ag10 Ag22 Ag9 59.31(5) . . ?
Ag13 Ag22 Ag9 56.50(5) . . ?
Ag23 Ag22 Ag9 107.73(6) . . ?
O15 Ag22 Ag16 143.9(4) . . ?
Ag14 Ag22 Ag16 59.27(4) . . ?
Ag21 Ag22 Ag16 54.20(4) . . ?
Ag19 Ag22 Ag16 55.46(4) . . ?
Ag10 Ag22 Ag16 52.54(4) . . ?
Ag13 Ag22 Ag16 115.50(6) . . ?
Ag23 Ag22 Ag16 100.11(5) . . ?
Ag9 Ag22 Ag16 84.08(5) . . ?
P9 Ag23 Ag14 169.11(14) . . ?
P9 Ag23 Ag21 104.54(14) . . ?
Ag14 Ag23 Ag21 64.78(5) . . ?
P9 Ag23 Ag26 131.34(14) . . ?
Ag14 Ag23 Ag26 58.79(5) . . ?
Ag21 Ag23 Ag26 115.94(6) . . ?
P9 Ag23 Ag13 128.32(14) . . ?
Ag14 Ag23 Ag13 58.22(5) . . ?
Ag21 Ag23 Ag13 112.12(6) . . ?
Ag26 Ag23 Ag13 58.83(5) . . ?
P9 Ag23 Ag22 118.52(15) . . ?
Ag14 Ag23 Ag22 54.79(5) . . ?
Ag21 Ag23 Ag22 57.28(5) . . ?
Ag26 Ag23 Ag22 105.98(6) . . ?
Ag13 Ag23 Ag22 61.02(5) . . ?
P9 Ag23 Ag24 123.99(14) . . ?
Ag14 Ag23 Ag24 54.05(5) . . ?
Ag21 Ag23 Ag24 61.43(5) . . ?
Ag26 Ag23 Ag24 62.17(5) . . ?
Ag13 Ag23 Ag24 105.45(6) . . ?
Ag22 Ag23 Ag24 98.96(5) . . ?
O2 Ag24 Ag14 148.2(4) . . ?
O2 Ag24 Ag12 143.3(4) . . ?
Ag14 Ag24 Ag12 66.52(5) . . ?
O2 Ag24 Ag25 93.0(4) . . ?
Ag14 Ag24 Ag25 115.43(6) . . ?
Ag12 Ag24 Ag25 65.63(5) . . ?
O2 Ag24 Ag15 137.8(4) . . ?
Ag14 Ag24 Ag15 60.69(5) . . ?
Ag12 Ag24 Ag15 54.99(4) . . ?
Ag25 Ag24 Ag15 57.00(4) . . ?
O2 Ag24 Ag21 89.3(4) . . ?
Ag14 Ag24 Ag21 63.86(5) . . ?
Ag12 Ag24 Ag21 127.25(6) . . ?
Ag25 Ag24 Ag21 123.26(6) . . ?
Ag15 Ag24 Ag21 85.24(5) . . ?
O2 Ag24 Ag28 88.7(4) . . ?
Ag14 Ag24 Ag28 91.13(5) . . ?
Ag12 Ag24 Ag28 106.22(6) . . ?
Ag25 Ag24 Ag28 64.40(5) . . ?
Ag15 Ag24 Ag28 53.01(4) . . ?
Ag21 Ag24 Ag28 58.98(4) . . ?
O2 Ag24 Ag23 93.5(4) . . ?
Ag14 Ag24 Ag23 57.98(5) . . ?
Ag12 Ag24 Ag23 109.16(6) . . ?
Ag25 Ag24 Ag23 173.37(7) . . ?
Ag15 Ag24 Ag23 116.90(6) . . ?
Ag21 Ag24 Ag23 55.93(4) . . ?
Ag28 Ag24 Ag23 114.82(6) . . ?
O2 Ag24 Ag26 120.6(4) . . ?
Ag14 Ag24 Ag26 57.58(5) . . ?
Ag12 Ag24 Ag26 58.51(5) . . ?
Ag25 Ag24 Ag26 120.79(6) . . ?
Ag15 Ag24 Ag26 101.13(5) . . ?
Ag21 Ag24 Ag26 105.72(6) . . ?
Ag28 Ag24 Ag26 148.16(6) . . ?
Ag23 Ag24 Ag26 56.01(5) . . ?
P2 Ag25 Ag15 170.25(15) . . ?
P2 Ag25 Ag24 106.81(15) . . ?
Ag15 Ag25 Ag24 64.23(5) . . ?
P2 Ag25 Ag11 125.72(16) . . ?
Ag15 Ag25 Ag11 58.72(5) . . ?
Ag24 Ag25 Ag11 113.34(6) . . ?
P2 Ag25 Ag27 130.71(15) . . ?
Ag15 Ag25 Ag27 58.82(5) . . ?
Ag24 Ag25 Ag27 113.73(6) . . ?
Ag11 Ag25 Ag27 59.99(5) . . ?
P2 Ag25 Ag12 118.19(14) . . ?
Ag15 Ag25 Ag12 54.29(4) . . ?
Ag24 Ag25 Ag12 56.24(5) . . ?
Ag11 Ag25 Ag12 63.66(5) . . ?
Ag27 Ag25 Ag12 107.38(6) . . ?
P2 Ag25 Ag28 126.68(16) . . ?
Ag15 Ag25 Ag28 53.59(4) . . ?
Ag24 Ag25 Ag28 60.54(5) . . ?
Ag11 Ag25 Ag28 104.75(5) . . ?
Ag27 Ag25 Ag28 59.70(5) . . ?
Ag12 Ag25 Ag28 97.46(5) . . ?
P12 Ag26 Ag14 173.96(15) . . ?
P12 Ag26 Ag13 126.44(15) . . ?
Ag14 Ag26 Ag13 59.02(5) . . ?
P12 Ag26 Ag12 110.09(15) . . ?
Ag14 Ag26 Ag12 63.94(5) . . ?
Ag13 Ag26 Ag12 114.62(6) . . ?
P12 Ag26 Ag23 124.76(14) . . ?
Ag14 Ag26 Ag23 59.18(5) . . ?
Ag13 Ag26 Ag23 60.79(5) . . ?
Ag12 Ag26 Ag23 112.08(6) . . ?
P12 Ag26 Ag8 124.24(14) . . ?
Ag14 Ag26 Ag8 54.49(5) . . ?
Ag13 Ag26 Ag8 61.80(5) . . ?
Ag12 Ag26 Ag8 60.43(5) . . ?
Ag23 Ag26 Ag8 107.12(6) . . ?
P12 Ag26 Ag24 122.49(15) . . ?
Ag14 Ag26 Ag24 54.02(4) . . ?
Ag13 Ag26 Ag24 106.61(6) . . ?
Ag12 Ag26 Ag24 55.92(5) . . ?
Ag23 Ag26 Ag24 61.82(5) . . ?
Ag8 Ag26 Ag24 97.81(5) . . ?
P3 Ag27 Ag15 169.65(14) . . ?
P3 Ag27 Ag17 105.46(13) . . ?
Ag15 Ag27 Ag17 64.94(5) . . ?
P3 Ag27 Ag11 131.17(14) . . ?
Ag15 Ag27 Ag11 58.87(5) . . ?
Ag17 Ag27 Ag11 114.09(6) . . ?
P3 Ag27 Ag25 125.66(13) . . ?
Ag15 Ag27 Ag25 59.40(5) . . ?
Ag17 Ag27 Ag25 114.99(6) . . ?
Ag11 Ag27 Ag25 59.88(5) . . ?
P3 Ag27 Ag28 116.80(14) . . ?
Ag15 Ag27 Ag28 55.42(4) . . ?
Ag17 Ag27 Ag28 57.21(4) . . ?
Ag11 Ag27 Ag28 108.41(6) . . ?
Ag25 Ag27 Ag28 64.70(5) . . ?
P3 Ag27 Ag5 126.00(14) . . ?
Ag15 Ag27 Ag5 53.64(4) . . ?
Ag17 Ag27 Ag5 59.19(4) . . ?
Ag11 Ag27 Ag5 60.95(5) . . ?
Ag25 Ag27 Ag5 105.86(6) . . ?
Ag28 Ag27 Ag5 97.70(5) . . ?
O4 Ag28 Ag15 144.9(3) . . ?
O4 Ag28 Ag17 145.2(3) . . ?
Ag15 Ag28 Ag17 66.81(5) . . ?
O4 Ag28 Ag20 98.1(3) . . ?
Ag15 Ag28 Ag20 114.05(6) . . ?
Ag17 Ag28 Ag20 63.76(5) . . ?
O4 Ag28 Ag21 89.8(3) . . ?
Ag15 Ag28 Ag21 91.89(5) . . ?
Ag17 Ag28 Ag21 106.06(6) . . ?
Ag20 Ag28 Ag21 64.27(5) . . ?
O4 Ag28 Ag27 117.8(3) . . ?
Ag15 Ag28 Ag27 58.22(5) . . ?
Ag17 Ag28 Ag27 58.95(5) . . ?
Ag20 Ag28 Ag27 119.42(6) . . ?
Ag21 Ag28 Ag27 149.48(6) . . ?
O4 Ag28 Ag16 140.8(3) . . ?
Ag15 Ag28 Ag16 60.13(4) . . ?
Ag17 Ag28 Ag16 54.86(4) . . ?
Ag20 Ag28 Ag16 56.47(4) . . ?
Ag21 Ag28 Ag16 53.46(4) . . ?
Ag27 Ag28 Ag16 101.24(5) . . ?
O4 Ag28 Ag24 87.9(3) . . ?
Ag15 Ag28 Ag24 63.01(5) . . ?
Ag17 Ag28 Ag24 126.84(6) . . ?
Ag20 Ag28 Ag24 124.31(6) . . ?
Ag21 Ag28 Ag24 60.43(5) . . ?
Ag27 Ag28 Ag24 105.18(5) . . ?
Ag16 Ag28 Ag24 84.94(5) . . ?
O4 Ag28 Ag25 91.2(3) . . ?
Ag15 Ag28 Ag25 56.73(4) . . ?
Ag17 Ag28 Ag25 108.47(6) . . ?
Ag20 Ag28 Ag25 170.61(6) . . ?
Ag21 Ag28 Ag25 115.39(6) . . ?
Ag27 Ag28 Ag25 55.60(4) . . ?
Ag16 Ag28 Ag25 115.18(5) . . ?
Ag24 Ag28 Ag25 55.06(4) . . ?
P21 Ag29 P19 119.1(3) . . ?
P21 Ag29 P20 121.2(3) . . ?
P19 Ag29 P20 119.1(3) . . ?
P21 Ag29 O16 93.7(4) . . ?
P19 Ag29 O16 92.7(4) . . ?
P20 Ag29 O16 91.4(4) . . ?
P24 Ag30 P22 121.0(2) . . ?
P24 Ag30 P23 118.0(2) . . ?
P22 Ag30 P23 120.8(3) . . ?
P15 Ag31 P13 124.9(3) . . ?
P15 Ag31 P14 118.6(3) . . ?
P13 Ag31 P14 116.4(3) . . ?
P18 Ag32 P17 118.8(2) . . ?
P18 Ag32 P16 122.1(2) . . ?
P17 Ag32 P16 119.0(2) . . ?
O9 Mo1 O11 108.8(6) . . ?
O9 Mo1 O10 109.9(6) . . ?
O11 Mo1 O10 110.7(6) . . ?
O9 Mo1 O12 109.4(6) . . ?
O11 Mo1 O12 109.7(6) . . ?
O10 Mo1 O12 108.3(6) . . ?
O16 Mo2 O14 109.6(7) . . ?
O16 Mo2 O15 109.3(6) . . ?
O14 Mo2 O15 110.4(7) . . ?
O16 Mo2 O13 110.2(7) . . ?
O14 Mo2 O13 109.3(7) . . ?
O15 Mo2 O13 108.0(6) . . ?
O5 Mo3 O8 108.4(7) . . ?
O5 Mo3 O7 110.0(6) . . ?
O8 Mo3 O7 110.4(6) . . ?
O5 Mo3 O6 109.1(6) . . ?
O8 Mo3 O6 109.5(6) . . ?
O7 Mo3 O6 109.4(6) . . ?
O1 Mo4 O2 109.4(7) . . ?
O1 Mo4 O3 109.6(7) . . ?
O2 Mo4 O3 109.0(6) . . ?
O1 Mo4 O4 110.2(6) . . ?
O2 Mo4 O4 108.9(7) . . ?
O3 Mo4 O4 109.7(6) . . ?
C45 P1 C7 105.0(10) . . ?
C45 P1 C1 103.4(10) . . ?
C7 P1 C1 105.5(12) . . ?
C45 P1 Ag11 115.7(7) . . ?
C7 P1 Ag11 108.7(7) . . ?
C1 P1 Ag11 117.4(9) . . ?
C62 P2 C197 101.7(12) . . ?
C62 P2 C63 104.9(11) . . ?
C197 P2 C63 102.7(11) . . ?
C62 P2 Ag25 117.6(8) . . ?
C197 P2 Ag25 118.4(8) . . ?
C63 P2 Ag25 109.8(8) . . ?
C19 P3 C25 104.0(11) . . ?
C19 P3 C31 102.0(10) . . ?
C25 P3 C31 104.7(10) . . ?
C19 P3 Ag27 118.7(7) . . ?
C25 P3 Ag27 110.5(8) . . ?
C31 P3 Ag27 115.5(7) . . ?
C76 P4 C111 107.6(13) . . ?
C76 P4 C190 100.8(14) . . ?
C111 P4 C190 101.8(12) . . ?
C76 P4 Ag20 110.0(8) . . ?
C111 P4 Ag20 118.9(8) . . ?
C190 P4 Ag20 115.8(11) . . ?
C166 P5 C56 103.3(11) . . ?
C166 P5 C110 106.2(11) . . ?
C56 P5 C110 100.9(10) . . ?
C166 P5 Ag18 112.9(8) . . ?
C56 P5 Ag18 119.6(7) . . ?
C110 P5 Ag18 112.4(8) . . ?
C117 P6 C179 106.1(12) . . ?
C117 P6 C93 109.8(14) . . ?
C179 P6 C93 102.7(13) . . ?
C117 P6 Ag19 112.6(10) . . ?
C179 P6 Ag19 112.1(8) . . ?
C93 P6 Ag19 112.9(8) . . ?
C52 P7 C142 104.4(13) . . ?
C52 P7 C160 100.0(15) . . ?
C142 P7 C160 105.5(17) . . ?
C52 P7 Ag3 118.5(8) . . ?
C142 P7 Ag3 110.6(11) . . ?
C160 P7 Ag3 116.3(11) . . ?
C180 P8 C184 102.2(15) . . ?
C180 P8 C230 107.1(14) . . ?
C184 P8 C230 111.2(19) . . ?
C180 P8 Ag13 113.9(8) . . ?
C184 P8 Ag13 112.6(15) . . ?
C230 P8 Ag13 109.5(10) . . ?
C130 P9 C124 103.8(11) . . ?
C130 P9 C201 100.2(12) . . ?
C124 P9 C201 103.7(12) . . ?
C130 P9 Ag23 115.8(9) . . ?
C124 P9 Ag23 111.3(8) . . ?
C201 P9 Ag23 120.1(7) . . ?
C100 P10 C172 106.9(12) . . ?
C100 P10 C154 110.0(14) . . ?
C172 P10 C154 101.8(17) . . ?
C100 P10 Ag2 111.0(9) . . ?
C172 P10 Ag2 112.3(7) . . ?
C154 P10 Ag2 114.2(11) . . ?
C148 P11 C218 106.6(14) . . ?
C148 P11 C202 100.6(16) . . ?
C218 P11 C202 104.3(19) . . ?
C148 P11 Ag1 116.4(10) . . ?
C218 P11 Ag1 111.9(12) . . ?
C202 P11 Ag1 115.6(15) . . ?
C35 P12 C41 105.0(11) . . ?
C35 P12 C74 106.5(11) . . ?
C41 P12 C74 100.1(10) . . ?
C35 P12 Ag26 108.1(8) . . ?
C41 P12 Ag26 118.5(8) . . ?
C74 P12 Ag26 117.3(7) . . ?
C224 P13 C198 104.1(17) . . ?
C224 P13 C318 102(2) . . ?
C198 P13 C318 103(2) . . ?
C224 P13 Ag31 120.8(14) . . ?
C198 P13 Ag31 107.9(9) . . ?
C318 P13 Ag31 117(2) . . ?
C194 P14 C283 103.9(12) . . ?
C194 P14 C290 94.3(18) . . ?
C283 P14 C290 102.6(18) . . ?
C194 P14 Ag31 106.8(9) . . ?
C283 P14 Ag31 122.4(10) . . ?
C290 P14 Ag31 122.0(16) . . ?
C193 P15 C280 108.2(17) . . ?
C193 P15 C334 99(2) . . ?
C280 P15 C334 100.7(19) . . ?
C193 P15 Ag31 110.9(11) . . ?
C280 P15 Ag31 112.9(12) . . ?
C334 P15 Ag31 123(2) . . ?
C236 P16 C206 103.5(17) . . ?
C236 P16 C53 106.0(12) . . ?
C206 P16 C53 102.7(15) . . ?
C236 P16 Ag32 117.1(12) . . ?
C206 P16 Ag32 119.9(11) . . ?
C53 P16 Ag32 105.9(8) . . ?
C298 P17 C286 103.6(16) . . ?
C298 P17 C205 101.7(19) . . ?
C286 P17 C205 107.5(13) . . ?
C298 P17 Ag32 116.9(16) . . ?
C286 P17 Ag32 114.9(10) . . ?
C205 P17 Ag32 111.1(10) . . ?
C243 P18 C13 103.7(12) . . ?
C243 P18 C34 102.0(12) . . ?
C13 P18 C34 104.0(10) . . ?
C243 P18 Ag32 116.2(8) . . ?
C13 P18 Ag32 119.0(8) . . ?
C34 P18 Ag32 110.0(8) . . ?
C360 P19 C136 104(2) . . ?
C360 P19 C176 102(2) . . ?
C136 P19 C176 103.2(17) . . ?
C360 P19 Ag29 115.0(18) . . ?
C136 P19 Ag29 119.5(16) . . ?
C176 P19 Ag29 111.6(11) . . ?
C260 P20 C175 102.8(16) . . ?
C260 P20 C81 104.7(18) . . ?
C175 P20 C81 103.6(14) . . ?
C260 P20 Ag29 116.5(14) . . ?
C175 P20 Ag29 110.8(9) . . ?
C81 P20 Ag29 116.8(11) . . ?
C253 P21 C87 102.3(18) . . ?
C253 P21 C183 103.7(17) . . ?
C87 P21 C183 103.1(15) . . ?
C253 P21 Ag29 116.8(15) . . ?
C87 P21 Ag29 118.2(15) . . ?
C183 P21 Ag29 110.9(12) . . ?
C257 P22 C302 101.5(16) . . ?
C257 P22 C44 103.7(14) . . ?
C302 P22 C44 106.9(17) . . ?
C257 P22 Ag30 118.5(11) . . ?
C302 P22 Ag30 116.1(16) . . ?
C44 P22 Ag30 109.0(7) . . ?
C339 P23 C212 99.3(17) . . ?
C339 P23 C49 102.2(16) . . ?
C212 P23 C49 105.1(15) . . ?
C339 P23 Ag30 117.9(13) . . ?
C212 P23 Ag30 120.9(11) . . ?
C49 P23 Ag30 109.2(10) . . ?
C248 P24 C48 104.6(12) . . ?
C248 P24 C276 103.0(12) . . ?
C48 P24 C276 103.2(10) . . ?
C248 P24 Ag30 116.0(11) . . ?
C48 P24 Ag30 107.3(8) . . ?
C276 P24 Ag30 121.0(8) . . ?
Mo4 O2 Ag24 111.3(7) . . ?
Mo4 O3 Ag21 111.7(7) . . ?
Mo4 O4 Ag28 111.0(6) . . ?
Mo3 O6 Ag12 110.7(6) . . ?
Mo3 O7 Ag8 110.1(6) . . ?
Mo3 O8 Ag7 110.3(7) . . ?
Mo1 O10 Ag5 111.9(6) . . ?
Mo1 O11 Ag4 110.7(6) . . ?
Mo1 O12 Ag17 109.9(6) . . ?
Mo2 O13 Ag10 109.8(7) . . ?
Mo2 O14 Ag9 109.7(7) . . ?
Mo2 O15 Ag22 109.0(6) . . ?
Mo2 O16 Ag29 178.1(9) . . ?
O19 N1 O18 133(7) . . ?
O19 N1 O20 121(7) . . ?
O18 N1 O20 105(5) . . ?
O26 N3 O21 117(4) . . ?
O26 N3 O27 117(4) . . ?
O21 N3 O27 117(4) . . ?
O25 N4 O23 116(5) . . ?
O25 N4 O24 116(5) . . ?
O23 N4 O24 117(5) . . ?
C6 C1 C2 116(2) . . ?
C6 C1 P1 126(2) . . ?
C2 C1 P1 117.0(18) . . ?
C3 C2 C1 121(3) . . ?
C2 C3 C4 120(3) . . ?
C5 C4 C3 119(3) . . ?
C4 C5 C6 117(3) . . ?
C1 C6 C5 127(3) . . ?
C12 C7 C8 117(2) . . ?
C12 C7 P1 122.2(17) . . ?
C8 C7 P1 121.1(16) . . ?
C9 C8 C7 118(2) . . ?
C10 C9 C8 123(2) . . ?
C9 C10 C11 119(2) . . ?
C12 C11 C10 120(2) . . ?
C11 C12 C7 123(2) . . ?
C18 C13 C14 117(2) . . ?
C18 C13 P18 118.4(16) . . ?
C14 C13 P18 123.9(17) . . ?
C13 C14 C15 121(2) . . ?
C16 C15 C14 120(2) . . ?
C15 C16 C17 121(2) . . ?
C18 C17 C16 117(2) . . ?
C13 C18 C17 124(2) . . ?
C20 C19 C24 118(2) . . ?
C20 C19 P3 118.3(16) . . ?
C24 C19 P3 123.5(19) . . ?
C21 C20 C19 122(2) . . ?
C20 C21 C22 118(3) . . ?
C23 C22 C21 119(2) . . ?
C24 C23 C22 120(3) . . ?
C23 C24 C19 122(3) . . ?
C30 C25 C26 118(2) . . ?
C30 C25 P3 125.1(19) . . ?
C26 C25 P3 117.2(16) . . ?
C27 C26 C25 118(2) . . ?
C28 C27 C26 123(3) . . ?
C27 C28 C29 119(3) . . ?
C28 C29 C30 121(3) . . ?
C25 C30 C29 121(3) . . ?
C32 C31 P3 112.5(14) . . ?
C31 C32 C33 113.5(16) . . ?
C34 C33 C32 111.9(18) . . ?
C33 C34 P18 111.4(15) . . ?
C40 C35 C36 117(2) . . ?
C40 C35 P12 117.8(19) . . ?
C36 C35 P12 125.4(19) . . ?
C37 C36 C35 123(3) . . ?
C36 C37 C38 118(3) . . ?
C39 C38 C37 121(3) . . ?
C38 C39 C40 120(2) . . ?
C35 C40 C39 121(2) . . ?
C42 C41 P12 114.0(16) . . ?
C364 C365 C362 124(6) . . ?
C365 C364 C363 109(6) . . ?
C364 C363 C361 130(6) . . ?
C360 C362 C365 122(6) . . ?
C360 C361 C363 117(5) . . ?
C361 C360 C362 116(5) . . ?
C361 C360 P19 122(4) . . ?
C362 C360 P19 122(4) . . ?
C43 C42 C41 114.3(19) . . ?
C44 C43 C42 108(2) . . ?
C43 C44 P22 111.6(17) . . ?
C46 C45 P1 114.2(16) . . ?
C47 C46 C45 115.3(19) . . ?
C46 C47 C48 113.9(18) . . ?
C47 C48 P24 112.4(15) . . ?
C50 C49 P23 114.3(19) . . ?
C51 C50 C49 110(2) . . ?
C52 C51 C50 111(2) . . ?
C51 C52 P7 113.8(18) . . ?
C54 C53 P16 114.5(17) . . ?
C53 C54 C55 113.5(19) . . ?
C56 C55 C54 113.2(18) . . ?
C55 C56 P5 113.5(15) . . ?
C62 C57 C58 122(2) . . ?
C59 C58 C57 119(3) . . ?
C60 C59 C58 122(3) . . ?
C59 C60 C61 119(3) . . ?
C60 C61 C62 124(2) . . ?
C57 C62 C61 114(2) . . ?
C57 C62 P2 119.9(17) . . ?
C61 C62 P2 125.2(19) . . ?
C64 C63 C68 120(2) . . ?
C64 C63 P2 117.3(18) . . ?
C68 C63 P2 122.8(19) . . ?
C63 C64 C65 121(2) . . ?
C66 C65 C64 119(3) . . ?
C65 C66 C67 120(2) . . ?
C66 C67 C68 121(3) . . ?
C63 C68 C67 119(3) . . ?
C74 C69 C70 122(3) . . ?
C71 C70 C69 118(3) . . ?
C70 C71 C72 120(3) . . ?
C73 C72 C71 123(3) . . ?
C72 C73 C74 116(3) . . ?
C69 C74 C73 121(2) . . ?
C69 C74 P12 117.0(18) . . ?
C73 C74 P12 122(2) . . ?
C76 C75 C80 124(3) . . ?
C75 C76 C77 116(3) . . ?
C75 C76 P4 119(2) . . ?
C77 C76 P4 125(2) . . ?
C76 C77 C78 119(3) . . ?
C79 C78 C77 121(3) . . ?
C78 C79 C80 125(4) . . ?
C79 C80 C75 115(3) . . ?
C86 C81 C82 124(4) . . ?
C86 C81 P20 121(3) . . ?
C82 C81 P20 114(3) . . ?
C81 C82 C83 120(4) . . ?
C82 C83 C84 120(4) . . ?
C85 C84 C83 120(4) . . ?
C84 C85 C86 113(4) . . ?
C81 C86 C85 124(3) . . ?
C88 C87 C92 120(3) . . ?
C88 C87 P21 120(3) . . ?
C92 C87 P21 120(3) . . ?
C87 C88 C89 122(4) . . ?
C88 C89 C90 115(4) . . ?
C91 C90 C89 120(3) . . ?
C90 C91 C92 123(4) . . ?
C91 C92 C87 120(4) . . ?
C94 C93 C98 120(3) . . ?
C94 C93 P6 115(2) . . ?
C98 C93 P6 126(2) . . ?
C93 C94 C95 121(3) . . ?
C94 C95 C96 118(3) . . ?
C97 C96 C95 121(3) . . ?
C98 C97 C96 120(3) . . ?
C97 C98 C93 120(3) . . ?
C100 C99 C104 127(2) . . ?
C99 C100 C101 115(2) . . ?
C99 C100 P10 120.1(19) . . ?
C101 C100 P10 124(2) . . ?
C102 C101 C100 122(3) . . ?
C101 C102 C103 117(3) . . ?
C104 C103 C102 124(3) . . ?
C103 C104 C99 114(3) . . ?
C106 C105 C110 118(2) . . ?
C107 C106 C105 122(3) . . ?
C108 C107 C106 120(3) . . ?
C107 C108 C109 122(3) . . ?
C110 C109 C108 115(2) . . ?
C105 C110 C109 122(2) . . ?
C105 C110 P5 117.6(18) . . ?
C109 C110 P5 119.4(19) . . ?
C112 C111 C116 119(2) . . ?
C112 C111 P4 115(2) . . ?
C116 C111 P4 125(2) . . ?
C111 C112 C113 117(3) . . ?
C114 C113 C112 121(3) . . ?
C113 C114 C115 122(3) . . ?
C114 C115 C116 120(3) . . ?
C115 C116 C111 120(3) . . ?
C122 C117 C118 119(3) . . ?
C122 C117 P6 119(2) . . ?
C118 C117 P6 121(2) . . ?
C117 C118 C119 113(3) . . ?
C120 C119 C118 122(3) . . ?
C119 C120 C121 129(4) . . ?
C120 C121 C122 111(4) . . ?
C117 C122 C121 126(3) . . ?
C237 C123 C236 117(3) . . ?
C125 C124 C129 114(2) . . ?
C125 C124 P9 117(2) . . ?
C129 C124 P9 129(2) . . ?
C124 C125 C126 118(3) . . ?
C127 C126 C125 124(3) . . ?
C126 C127 C128 117(3) . . ?
C129 C128 C127 119(3) . . ?
C128 C129 C124 128(3) . . ?
C135 C130 C131 119(2) . . ?
C135 C130 P9 117.7(19) . . ?
C131 C130 P9 123(2) . . ?
C130 C131 C132 120(3) . . ?
C133 C132 C131 120(3) . . ?
C132 C133 C134 124(3) . . ?
C133 C134 C135 117(3) . . ?
C130 C135 C134 120(3) . . ?
C141 C136 C137 117(4) . . ?
C141 C136 P19 121(3) . . ?
C137 C136 P19 122(3) . . ?
C136 C137 C138 128(3) . . ?
C139 C138 C137 112(4) . . ?
C140 C139 C138 117(4) . . ?
C139 C140 C141 129(3) . . ?
C136 C141 C140 116(4) . . ?
C147 C142 C143 115(3) . . ?
C147 C142 P7 128(3) . . ?
C143 C142 P7 117(2) . . ?
C144 C143 C142 118(3) . . ?
C145 C144 C143 118(4) . . ?
C146 C145 C144 125(4) . . ?
C145 C146 C147 116(4) . . ?
C146 C147 C142 127(4) . . ?
C149 C148 C153 114(3) . . ?
C149 C148 P11 121(2) . . ?
C153 C148 P11 125(2) . . ?
C148 C149 C150 130(3) . . ?
C149 C150 C151 113(3) . . ?
C152 C151 C150 121(4) . . ?
C151 C152 C153 123(3) . . ?
C152 C153 C148 117(3) . . ?
C159 C154 C155 123(3) . . ?
C159 C154 P10 125(3) . . ?
C155 C154 P10 111(2) . . ?
C156 C155 C154 116(4) . . ?
C155 C156 C157 120(4) . . ?
C158 C157 C156 123(4) . . ?
C157 C158 C159 117(4) . . ?
C154 C159 C158 120(4) . . ?
C165 C160 C161 122(3) . . ?
C165 C160 P7 115(2) . . ?
C161 C160 P7 122(3) . . ?
C162 C161 C160 119(4) . . ?
C163 C162 C161 122(4) . . ?
C162 C163 C164 122(4) . . ?
C165 C164 C163 116(4) . . ?
C160 C165 C164 117(3) . . ?
C167 C166 C171 118(2) . . ?
C167 C166 P5 118.9(18) . . ?
C171 C166 P5 123(2) . . ?
C166 C167 C168 121(2) . . ?
C169 C168 C167 119(3) . . ?
C170 C169 C168 120(3) . . ?
C169 C170 C171 123(3) . . ?
C170 C171 C166 119(3) . . ?
C173 C172 P10 115.3(18) . . ?
C172 C173 C174 110(2) . . ?
C173 C174 C175 115(2) . . ?
C174 C175 P20 108.5(17) . . ?
C177 C176 P19 114(2) . . ?
C176 C177 C178 117(3) . . ?
C177 C178 C179 114(2) . . ?
C178 C179 P6 119.9(18) . . ?
C181 C180 P8 119.1(19) . . ?
C180 C181 C182 110(2) . . ?
C183 C182 C181 111(3) . . ?
C182 C183 P21 107(2) . . ?
C189 C184 C185 119(5) . . ?
C189 C184 P8 114(4) . . ?
C185 C184 P8 127(4) . . ?
C184 C185 C186 118(5) . . ?
C187 C186 C185 118(4) . . ?
C186 C187 C188 121(5) . . ?
C189 C188 C187 111(5) . . ?
C184 C189 C188 132(5) . . ?
C191 C190 P4 108(2) . . ?
C190 C191 C192 112(3) . . ?
C193 C192 C191 103(3) . . ?
C192 C193 P15 116(3) . . ?
C195 C194 P14 113(2) . . ?
C196 C195 C194 109(2) . . ?
C195 C196 C197 110(2) . . ?
C196 C197 P2 110.8(17) . . ?
C199 C198 P13 113.5(18) . . ?
C198 C199 C200 116(2) . . ?
C201 C200 C199 113(2) . . ?
C200 C201 P9 113.9(16) . . ?
C203 C202 P11 115(3) . . ?
C202 C203 C204 107(3) . . ?
C205 C204 C203 93(3) . . ?
C204 C205 P17 112(2) . . ?
C211 C206 C207 119(3) . . ?
C211 C206 P16 121(3) . . ?
C207 C206 P16 119(3) . . ?
C206 C207 C208 122(4) . . ?
C209 C208 C207 112(4) . . ?
C210 C209 C208 131(4) . . ?
C209 C210 C211 117(4) . . ?
C206 C211 C210 119(4) . . ?
C213 C212 C217 117(3) . . ?
C213 C212 P23 121(3) . . ?
C217 C212 P23 122(3) . . ?
C212 C213 C214 122(4) . . ?
C213 C214 C215 120(4) . . ?
C216 C215 C214 120(3) . . ?
C215 C216 C217 117(4) . . ?
C212 C217 C216 124(4) . . ?
C219 C218 C223 115(3) . . ?
C219 C218 P11 119(3) . . ?
C223 C218 P11 126(3) . . ?
C220 C219 C218 124(4) . . ?
C219 C220 C221 115(4) . . ?
C222 C221 C220 123(4) . . ?
C221 C222 C223 120(4) . . ?
C222 C223 C218 122(4) . . ?
C225 C224 C229 117(4) . . ?
C225 C224 P13 119(4) . . ?
C229 C224 P13 124(3) . . ?
C224 C225 C226 117(4) . . ?
C227 C226 C225 111(4) . . ?
C226 C227 C228 123(4) . . ?
C229 C228 C227 107(4) . . ?
C224 C229 C228 127(4) . . ?
C235 C230 C231 124(3) . . ?
C235 C230 P8 118(2) . . ?
C231 C230 P8 118(3) . . ?
C230 C231 C232 113(4) . . ?
C233 C232 C231 119(3) . . ?
C234 C233 C232 124(4) . . ?
C233 C234 C235 115(4) . . ?
C230 C235 C234 124(3) . . ?
C240 C236 C123 119(3) . . ?
C240 C236 P16 119(2) . . ?
C123 C236 P16 122(3) . . ?
C238 C237 C123 123(4) . . ?
C237 C238 C239 127(4) . . ?
C238 C239 C240 113(4) . . ?
C236 C240 C239 120(3) . . ?
C242 C241 C307 118(3) . . ?
C243 C242 C241 122(3) . . ?
C242 C243 C244 120(3) . . ?
C242 C243 P18 121(2) . . ?
C244 C243 P18 119(2) . . ?
C245 C244 C243 117(3) . . ?
C307 C245 C244 123(3) . . ?
C247 C246 C270 117(4) . . ?
C246 C247 C248 122(3) . . ?
C249 C248 C247 117(3) . . ?
C249 C248 P24 122(3) . . ?
C247 C248 P24 121(2) . . ?
C248 C249 C271 122(3) . . ?
C251 C250 C255 118(5) . . ?
C250 C251 C252 121(5) . . ?
C253 C252 C251 120(4) . . ?
C254 C253 C252 117(4) . . ?
C254 C253 P21 121(4) . . ?
C252 C253 P21 121(3) . . ?
C253 C254 C255 126(5) . . ?
C254 C255 C250 114(4) . . ?
C257 C256 C274 124(4) . . ?
C256 C257 C258 117(3) . . ?
C256 C257 P22 124(2) . . ?
C258 C257 P22 119(3) . . ?
C257 C258 C272 121(4) . . ?
C260 C259 C267 124(4) . . ?
C259 C260 C261 119(3) . . ?
C259 C260 P20 120(3) . . ?
C261 C260 P20 120(3) . . ?
C269 C261 C260 119(4) . . ?
C299 C262 C263 117(3) . . ?
C284 C263 C262 121(3) . . ?
C281 C265 C266 120(3) . . ?
C278 C266 C265 118(3) . . ?
C268 C267 C259 113(4) . . ?
C269 C268 C267 122(4) . . ?
C261 C269 C268 121(4) . . ?
C271 C270 C246 125(4) . . ?
C270 C271 C249 116(4) . . ?
C273 C272 C258 113(4) . . ?
C272 C273 C274 133(4) . . ?
C273 C274 C256 112(4) . . ?
C276 C275 C304 121(2) . . ?
C275 C276 C277 118(2) . . ?
C275 C276 P24 119.6(18) . . ?
C277 C276 P24 122.2(17) . . ?
C276 C277 C306 120(2) . . ?
C266 C278 C279 121(4) . . ?
C278 C279 C280 122(3) . . ?
C279 C280 C281 118(3) . . ?
C279 C280 P15 123(3) . . ?
C281 C280 P15 119(3) . . ?
C265 C281 C280 120(3) . . ?
C299 C282 C283 119(3) . . ?
C284 C283 C282 118(2) . . ?
C284 C283 P14 120(2) . . ?
C282 C283 P14 122(2) . . ?
C283 C284 C263 121(3) . . ?
C286 C285 C294 119(3) . . ?
C287 C286 C285 121(2) . . ?
C287 C286 P17 121(2) . . ?
C285 C286 P17 118(2) . . ?
C286 C287 C292 118(3) . . ?
C309 C288 C289 123(5) . . ?
C290 C289 C288 131(6) . . ?
C289 C290 C291 107(5) . . ?
C289 C290 P14 129(5) . . ?
C291 C290 P14 125(4) . . ?
C308 C291 C290 124(5) . . ?
C293 C292 C287 121(4) . . ?
C292 C293 C294 122(3) . . ?
C293 C294 C285 118(3) . . ?
C332 C295 C297 120(4) . . ?
C295 C297 C298 125(4) . . ?
C297 C298 C333 116(4) . . ?
C297 C298 P17 120(3) . . ?
C333 C298 P17 122(3) . . ?
C262 C299 C282 122(3) . . ?
C301 C300 C313 115(5) . . ?
C302 C301 C300 125(5) . . ?
C328 C302 C301 115(4) . . ?
C328 C302 P22 120(4) . . ?
C301 C302 P22 123(3) . . ?
C330 C303 C317 103(6) . . ?
C305 C304 C275 119(2) . . ?
C306 C305 C304 121(2) . . ?
C305 C306 C277 121(2) . . ?
C245 C307 C241 120(3) . . ?
C291 C308 C309 118(5) . . ?
C288 C309 C308 116(5) . . ?
C314 C313 C300 120(5) . . ?
C313 C314 C328 119(5) . . ?
C318 C317 C303 132(6) . . ?
C317 C318 C319 117(6) . . ?
C317 C318 P13 122(5) . . ?
C319 C318 P13 121(5) . . ?
C318 C319 C329 130(7) . . ?
C323 C320 C337 120.0 . . ?
C320 C323 C334 120.0 . . ?
C335 C334 C323 120.0 . . ?
C335 C334 P15 118(5) . . ?
C323 C334 P15 122(5) . . ?
C334 C335 C336 120.0 . . ?
C335 C336 C337 120.0 . . ?
C336 C337 C320 120.0 . . ?
C302 C328 C314 119(5) . . ?
C319 C329 C330 105(6) . . ?
C303 C330 C329 129(5) . . ?
C332 C331 C333 126(4) . . ?
C295 C332 C331 114(4) . . ?
C331 C333 C298 115(4) . . ?
C340 C339 C344 122(5) . . ?
C370 C339 C371 118(5) . . ?
C340 C339 P23 130(4) . . ?
C370 C339 P23 122(4) . . ?
C344 C339 P23 108(4) . . ?
C371 C339 P23 117(3) . . ?
C342 C341 C370 131(5) . . ?
C342 C341 C340 116(6) . . ?
C342 C341 C372 46(3) . . ?
C370 C341 C372 110(5) . . ?
C341 C342 C372 96(5) . . ?
C341 C342 C343 94(5) . . ?
C339 C340 C341 111(7) . . ?
C344 C343 C342 121(7) . . ?
C343 C344 C339 107(7) . . ?
C342 C372 C371 118(7) . . ?
C342 C372 C341 38(3) . . ?
C371 C372 C341 94(5) . . ?
C372 C371 C339 111(6) . . ?
C341 C370 C339 106(6) . . ?

_refine_diff_density_max         3.140
_refine_diff_density_min         -2.117
_refine_diff_density_rms         0.249



# start Validation Reply Form
_vrf_PLAT602_3                   
;

PROBLEM:  VERY LARGE Solvent Accessible VOID(S) in Structure ! Info  
RESPONSE: The compound contains a large number of severely 
disordered methanol molecules of crystallization,
which 
could not be fully modelled.  The large voids are due to 
these disordered solvents.

;

# end Validation Reply Form
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_11_a_CCDC1
_database_code_depnum_ccdc_archive 'CCDC 1909220'
loop_
_audit_author_name
_audit_author_address
'Guangxiong Duan'
;Huazhong University of Science and Technology
China
;
_audit_update_record             
;
2019-04-10 deposited with the CCDC.	2019-12-13 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2016/6
_shelx_SHELXL_version_number     2016/6
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C168 H170 Ag28 O17 P12 W4'
_chemical_formula_weight         6588.43

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0034 0.0017 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0114 0.0062 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1041 0.0961 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8826 1.1200 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.7857 6.9448 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 2/c'
_space_group_name_Hall           '-C 2yc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   57.246(3)
_cell_length_b                   33.4588(16)
_cell_length_c                   38.553(4)
_cell_angle_alpha                90
_cell_angle_beta                 120.8820(10)
_cell_angle_gamma                90
_cell_volume                     63375(8)
_cell_formula_units_Z            8
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9640
_cell_measurement_theta_min      22.55
_cell_measurement_theta_max      2.24

_exptl_crystal_description       block
_exptl_crystal_colour            black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_density_diffrn    1.381
_exptl_crystal_F_000             24848
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.240
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.160
_exptl_absorpt_coefficient_mu    2.54
_shelx_estimated_absorpt_T_min   0.512
_shelx_estimated_absorpt_T_max   0.627
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.571
_exptl_absorpt_correction_T_max  0.666
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.6525
_diffrn_radiation_type           synchrotron
_diffrn_source                   'SSRF, Beamline B17B'
_diffrn_measurement_device_type  'CCD MX300-HE'
_diffrn_measurement_method       'phi scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            366423
_diffrn_reflns_av_unetI/netI     0.0456
_diffrn_reflns_av_R_equivalents  0.0674
_diffrn_reflns_limit_h_min       -67
_diffrn_reflns_limit_h_max       67
_diffrn_reflns_limit_k_min       -39
_diffrn_reflns_limit_k_max       39
_diffrn_reflns_limit_l_min       -45
_diffrn_reflns_limit_l_max       45
_diffrn_reflns_theta_min         1.088
_diffrn_reflns_theta_max         24.711
_diffrn_reflns_theta_full        24.711
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measured_fraction_theta_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_point_group_measured_fraction_full 0.995
_reflns_number_total             53734
_reflns_number_gt                37228
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX3'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1170P)²+9787.0635P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         53734
_refine_ls_number_parameters     2056
_refine_ls_number_restraints     975
_refine_ls_R_factor_all          0.1762
_refine_ls_R_factor_gt           0.1214
_refine_ls_wR_factor_ref         0.3674
_refine_ls_wR_factor_gt          0.3161
_refine_ls_goodness_of_fit_ref   1.074
_refine_ls_restrained_S_all      1.065
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 0.32800(2) 0.36067(3) 0.33963(4) 0.0579(3) Uani 1 1 d . . . . .
W2 W 0.32653(3) 0.64341(3) 0.34623(4) 0.0628(3) Uani 1 1 d . . . . .
W3 W 0.18563(2) 0.49547(4) 0.33925(4) 0.0637(3) Uani 1 1 d . . . . .
W4 W 0.35929(3) 0.49654(3) 0.57339(3) 0.0617(3) Uani 1 1 d . . . . .
Ag1 Ag 0.31919(4) 0.54368(5) 0.33945(6) 0.0520(4) Uani 1 1 d . . . . .
Ag2 Ag 0.34031(4) 0.54623(5) 0.48841(6) 0.0517(4) Uani 1 1 d . . . . .
Ag3 Ag 0.30049(4) 0.48705(5) 0.48633(6) 0.0497(4) Uani 1 1 d . . . . .
Ag4 Ag 0.24961(4) 0.50594(5) 0.41833(6) 0.0515(4) Uani 1 1 d . . . . .
Ag5 Ag 0.23806(4) 0.53819(5) 0.33949(6) 0.0518(4) Uani 1 1 d . . . . .
Ag6 Ag 0.24130(4) 0.44989(5) 0.35340(6) 0.0532(4) Uani 1 1 d . . . . .
Ag7 Ag 0.27494(4) 0.37733(5) 0.39568(6) 0.0528(4) Uani 1 1 d . . . . .
Ag8 Ag 0.28063(4) 0.42125(5) 0.33680(6) 0.0513(4) Uani 1 1 d . . . . .
Ag9 Ag 0.38476(4) 0.52799(6) 0.47770(6) 0.0555(5) Uani 1 1 d . . . . .
Ag10 Ag 0.29238(4) 0.45530(5) 0.41694(5) 0.0432(4) Uani 1 1 d . . . . .
Ag11 Ag 0.28189(4) 0.50060(5) 0.34639(5) 0.0443(4) Uani 1 1 d . . . . .
Ag12 Ag 0.30889(4) 0.61920(5) 0.44809(7) 0.0588(5) Uani 1 1 d . . . . .
Ag13 Ag 0.33108(4) 0.41013(5) 0.41691(6) 0.0507(4) Uani 1 1 d . . . . .
Ag14 Ag 0.25900(4) 0.42371(5) 0.44208(6) 0.0518(4) Uani 1 1 d . . . . .
Ag15 Ag 0.29203(4) 0.54117(4) 0.41870(5) 0.0431(4) Uani 1 1 d . . . . .
Ag16 Ag 0.34954(4) 0.45994(5) 0.48569(6) 0.0516(4) Uani 1 1 d . . . . .
Ag17 Ag 0.33113(4) 0.46043(5) 0.35285(6) 0.0535(4) Uani 1 1 d . . . . .
Ag18 Ag 0.28184(4) 0.58949(5) 0.35643(6) 0.0523(4) Uani 1 1 d . . . . .
Ag19 Ag 0.28492(4) 0.56867(5) 0.48075(6) 0.0530(4) Uani 1 1 d . . . . .
Ag20 Ag 0.37320(4) 0.52162(5) 0.39689(6) 0.0553(5) Uani 1 1 d . . . . .
Ag21 Ag 0.38066(4) 0.45154(5) 0.44296(6) 0.0571(5) Uani 1 1 d . . . . .
Ag22 Ag 0.33966(4) 0.57917(5) 0.42004(6) 0.0502(4) Uani 1 1 d . . . . .
Ag23 Ag 0.33511(4) 0.49924(5) 0.41692(5) 0.0445(4) Uani 1 1 d . . . . .
Ag24 Ag 0.31422(4) 0.39620(5) 0.47728(6) 0.0546(5) Uani 1 1 d . . . . .
Ag25 Ag 0.23509(4) 0.47308(6) 0.27802(6) 0.0604(5) Uani 1 1 d . . . . .
Ag26 Ag 0.25260(4) 0.59809(5) 0.40065(6) 0.0556(5) Uani 1 1 d . . . . .
Ag27 Ag 0.25531(4) 0.55095(5) 0.28001(6) 0.0577(5) Uani 1 1 d . . . . .
Ag28 Ag 0.28496(5) 0.48481(6) 0.27795(6) 0.0605(5) Uani 1 1 d . . . . .
P1 P 0.34023(16) 0.3551(2) 0.5390(2) 0.0601(17) Uani 1 1 d . . . . .
P2 P 0.41495(15) 0.3985(2) 0.4713(3) 0.0643(19) Uani 1 1 d . . . . .
P3 P 0.42386(14) 0.5599(2) 0.5359(2) 0.0604(17) Uani 1 1 d . . . . .
P4 P 0.39810(16) 0.5453(2) 0.3648(3) 0.0682(19) Uani 1 1 d . . . . .
P5 P 0.29176(17) 0.4713(2) 0.2205(2) 0.071(2) Uani 1 1 d . . . . .
P6 P 0.23426(17) 0.6032(2) 0.2288(2) 0.0632(18) Uani 1 1 d . . . . .
P7 P 0.18980(17) 0.4464(2) 0.2286(3) 0.075(2) Uani 1 1 d . . . . .
P8 P 0.21167(16) 0.64004(19) 0.3711(2) 0.0588(17) Uani 1 1 d . . . . .
P9 P 0.27865(16) 0.5763(2) 0.5397(2) 0.0585(17) Uani 1 1 d . . . . .
P10 P 0.25598(15) 0.31322(18) 0.3614(2) 0.0575(16) Uani 1 1 d . . . . .
P11 P 0.22355(16) 0.4096(2) 0.4584(2) 0.0584(17) Uani 1 1 d . . . . .
P12 P 0.33038(17) 0.68551(18) 0.4673(3) 0.0643(19) Uani 1 1 d . . . . .
O1 O 0.3329(4) 0.6005(5) 0.3244(6) 0.064(5) Uani 1 1 d . . . . .
O2 O 0.3412(4) 0.4046(5) 0.3288(6) 0.063(5) Uani 1 1 d . . . . .
O3 O 0.3658(4) 0.5430(5) 0.5566(5) 0.064(5) Uani 1 1 d . . . . .
O4 O 0.3425(8) 0.3061(8) 0.4492(10) 0.121(9) Uani 1 1 d D . . . .
H1 H 0.340(9) 0.306(11) 0.425(5) 0.181 Uiso 1 1 d D U . . .
H2 H 0.345(11) 0.281(3) 0.456(11) 0.181 Uiso 1 1 d D U . . .
O5 O 0.3699(4) 0.4563(5) 0.5535(5) 0.063(5) Uani 1 1 d . . . . .
O6 O 0.3774(5) 0.4939(7) 0.6268(6) 0.082(6) Uani 1 1 d . . . . .
O7 O 0.3234(4) 0.4935(5) 0.5546(5) 0.071(5) Uani 1 1 d . . . . .
O8 O 0.3431(4) 0.3571(4) 0.3922(6) 0.060(4) Uani 1 1 d . . . . .
O9 O 0.3364(4) 0.3187(5) 0.3200(7) 0.076(6) Uani 1 1 d . . . . .
O10 O 0.2917(4) 0.3647(4) 0.3169(5) 0.058(4) Uani 1 1 d . . . . .
O11 O 0.3457(4) 0.6393(5) 0.3995(6) 0.068(5) Uani 1 1 d . . . . .
O12 O 0.3358(5) 0.6875(5) 0.3304(7) 0.083(6) Uani 1 1 d . . . . .
O13 O 0.2913(4) 0.6436(5) 0.3305(6) 0.068(5) Uani 1 1 d . . . . .
O14 O 0.2045(4) 0.4980(5) 0.3928(6) 0.062(5) Uani 1 1 d . . . . .
O15 O 0.1938(3) 0.5385(5) 0.3199(5) 0.060(4) Uani 1 1 d . . . . .
O16 O 0.1959(4) 0.4511(5) 0.3237(6) 0.063(5) Uani 1 1 d . . . . .
O17 O 0.1499(4) 0.4940(7) 0.3212(7) 0.083(6) Uani 1 1 d . . . . .
C1 C 0.2320(6) 0.2922(7) 0.3751(9) 0.061(4) Uani 1 1 d . U . . .
C2 C 0.2111(6) 0.2677(8) 0.3481(10) 0.070(5) Uani 1 1 d . U . . .
H2Z H 0.209579 0.260437 0.323210 0.084 Uiso 1 1 calc R U . . .
C3 C 0.1920(6) 0.2536(8) 0.3577(11) 0.077(5) Uani 1 1 d . U . . .
H3 H 0.177181 0.237712 0.338782 0.092 Uiso 1 1 calc R U . . .
C4 C 0.1947(6) 0.2628(8) 0.3947(10) 0.074(5) Uani 1 1 d . U . . .
H4 H 0.182380 0.252169 0.401885 0.088 Uiso 1 1 calc R U . . .
C5 C 0.2160(6) 0.2883(8) 0.4213(10) 0.073(5) Uani 1 1 d . U . . .
H5 H 0.218046 0.295978 0.446444 0.087 Uiso 1 1 calc R U . . .
C6 C 0.2346(6) 0.3023(8) 0.4094(10) 0.069(5) Uani 1 1 d . U . . .
H6 H 0.249098 0.319426 0.427119 0.082 Uiso 1 1 calc R U . . .
C7 C 0.2796(7) 0.2729(8) 0.3710(11) 0.078(5) Uani 1 1 d . U . . .
C8 C 0.2180(6) 0.6933(7) 0.3810(8) 0.053(4) Uani 1 1 d . U . . .
C9 C 0.2908(7) 0.2684(9) 0.3447(11) 0.082(6) Uani 1 1 d . U . . .
H9 H 0.285068 0.285480 0.321965 0.098 Uiso 1 1 calc R U . . .
C10 C 0.3098(7) 0.2394(9) 0.3532(11) 0.084(6) Uani 1 1 d . U . . .
H10 H 0.316544 0.235561 0.335560 0.100 Uiso 1 1 calc R U . . .
C11 C 0.2871(7) 0.2465(9) 0.4006(11) 0.081(5) Uani 1 1 d . U . . .
H11 H 0.279796 0.248437 0.417787 0.097 Uiso 1 1 calc R U . . .
C12 C 0.3055(7) 0.2159(9) 0.4067(11) 0.085(6) Uani 1 1 d . U . . .
H12 H 0.308012 0.195149 0.425139 0.102 Uiso 1 1 calc R U . . .
C13 C 0.2348(6) 0.3761(8) 0.5018(8) 0.060(4) Uani 1 1 d . U . . .
C14 C 0.2228(6) 0.3763(8) 0.5251(9) 0.067(5) Uani 1 1 d . U . . .
H14 H 0.207742 0.393185 0.518536 0.081 Uiso 1 1 calc R U . . .
C15 C 0.2341(6) 0.3497(8) 0.5603(9) 0.067(5) Uani 1 1 d . U . . .
H15 H 0.226911 0.350347 0.577676 0.081 Uiso 1 1 calc R U . . .
C16 C 0.2548(6) 0.3240(9) 0.5685(9) 0.071(5) Uani 1 1 d . U . . .
H16 H 0.261275 0.305651 0.590389 0.085 Uiso 1 1 calc R U . . .
C17 C 0.2661(6) 0.3251(8) 0.5442(9) 0.070(5) Uani 1 1 d . U . . .
H17 H 0.281195 0.308355 0.550439 0.084 Uiso 1 1 calc R U . . .
C18 C 0.2559(6) 0.3503(8) 0.5110(9) 0.071(5) Uani 1 1 d . U . . .
H18 H 0.263640 0.349729 0.494262 0.085 Uiso 1 1 calc R U . . .
C19 C 0.3322(6) 0.3676(8) 0.5764(9) 0.068(5) Uani 1 1 d . U . . .
C20 C 0.3419(7) 0.3437(9) 0.6114(9) 0.071(5) Uani 1 1 d . U . . .
H20 H 0.352816 0.320716 0.615666 0.085 Uiso 1 1 calc R U . . .
C21 C 0.3342(7) 0.3560(9) 0.6408(10) 0.078(5) Uani 1 1 d . U . . .
H21 H 0.339290 0.339418 0.663595 0.094 Uiso 1 1 calc R U . . .
C22 C 0.3195(7) 0.3916(9) 0.6366(10) 0.082(5) Uani 1 1 d . U . . .
H22 H 0.315272 0.399818 0.656297 0.098 Uiso 1 1 calc R U . . .
C23 C 0.3119(7) 0.4133(10) 0.6023(10) 0.082(5) Uani 1 1 d . U . . .
H23 H 0.301597 0.436912 0.597991 0.098 Uiso 1 1 calc R U . . .
C24 C 0.3181(7) 0.4031(9) 0.5744(10) 0.074(5) Uani 1 1 d . U . . .
H24 H 0.312829 0.420617 0.552172 0.089 Uiso 1 1 calc R U . . .
C25 C 0.3326(7) 0.3022(8) 0.5304(10) 0.075(5) Uani 1 1 d . U . . .
C26 C 0.3784(7) 0.3562(8) 0.5677(10) 0.078(6) Uani 1 1 d . U . . .
H26A H 0.384592 0.383802 0.577207 0.094 Uiso 1 1 calc R U . . .
H26B H 0.385265 0.338887 0.591870 0.094 Uiso 1 1 calc R U . . .
C27 C 0.3912(7) 0.3417(8) 0.5419(10) 0.078(6) Uani 1 1 d . U . . .
H27A H 0.409368 0.330157 0.560234 0.094 Uiso 1 1 calc R U . . .
H27B H 0.379551 0.320390 0.523133 0.094 Uiso 1 1 calc R U . . .
C28 C 0.3937(7) 0.3738(8) 0.5188(10) 0.075(5) Uani 1 1 d . U . . .
H28A H 0.406454 0.394193 0.537534 0.089 Uiso 1 1 calc R U . . .
H28B H 0.375771 0.386621 0.501743 0.089 Uiso 1 1 calc R U . . .
C29 C 0.4046(7) 0.3577(8) 0.4908(10) 0.077(6) Uani 1 1 d . U . . .
H29A H 0.390052 0.342203 0.468078 0.092 Uiso 1 1 calc R U . . .
H29B H 0.420240 0.339570 0.506664 0.092 Uiso 1 1 calc R U . . .
C30 C 0.3075(7) 0.2903(8) 0.5034(10) 0.076(5) Uani 1 1 d . U . . .
H30 H 0.294271 0.309587 0.486800 0.091 Uiso 1 1 calc R U . . .
C31 C 0.3183(8) 0.2229(10) 0.5179(11) 0.088(6) Uani 1 1 d . U . . .
H31 H 0.313219 0.195585 0.512426 0.105 Uiso 1 1 calc R U . . .
C32 C 0.3000(8) 0.2496(9) 0.4990(10) 0.081(6) Uani 1 1 d . U . . .
H32 H 0.281508 0.242067 0.482078 0.097 Uiso 1 1 calc R U . . .
C33 C 0.1930(6) 0.3889(9) 0.4184(10) 0.076(5) Uani 1 1 d . U . . .
C34 C 0.1720(6) 0.3736(9) 0.4229(11) 0.083(6) Uani 1 1 d . U . . .
H34 H 0.173201 0.374064 0.448420 0.099 Uiso 1 1 calc R U . . .
C35 C 0.1892(6) 0.3865(10) 0.3786(10) 0.079(5) Uani 1 1 d . U . . .
H35 H 0.202073 0.398913 0.373411 0.095 Uiso 1 1 calc R U . . .
C36 C 0.1684(7) 0.3677(10) 0.3494(12) 0.090(6) Uani 1 1 d . U . . .
H36 H 0.169092 0.362551 0.325665 0.108 Uiso 1 1 calc R U . . .
C37 C 0.1454(7) 0.3544(10) 0.3493(12) 0.092(6) Uani 1 1 d . U . . .
H37 H 0.129489 0.344567 0.326154 0.110 Uiso 1 1 calc R U . . .
C38 C 0.1895(7) 0.6261(8) 0.3891(11) 0.080(5) Uani 1 1 d . U . . .
C39 C 0.1927(7) 0.6372(9) 0.3173(9) 0.075(6) Uani 1 1 d . U . . .
H39A H 0.186238 0.609426 0.308934 0.091 Uiso 1 1 calc R U . . .
H39B H 0.176551 0.654744 0.306637 0.091 Uiso 1 1 calc R U . . .
C40 C 0.2096(8) 0.6496(10) 0.2992(10) 0.081(6) Uani 1 1 d . U . . .
H40A H 0.206769 0.678581 0.293511 0.097 Uiso 1 1 calc R U . . .
H40B H 0.228987 0.645890 0.320301 0.097 Uiso 1 1 calc R U . . .
C41 C 0.2055(8) 0.6306(10) 0.2638(10) 0.083(6) Uani 1 1 d . U . . .
H41A H 0.186117 0.634106 0.242533 0.100 Uiso 1 1 calc R U . . .
H41B H 0.208554 0.601565 0.269377 0.100 Uiso 1 1 calc R U . . .
C42 C 0.2231(7) 0.6446(10) 0.2467(11) 0.082(6) Uani 1 1 d . U . . .
H42A H 0.239198 0.659085 0.267957 0.098 Uiso 1 1 calc R U . . .
H42B H 0.212490 0.663453 0.224093 0.098 Uiso 1 1 calc R U . . .
C43 C 0.2669(7) 0.5301(8) 0.5496(10) 0.076(6) Uani 1 1 d . U . . .
H43A H 0.281813 0.510125 0.560157 0.091 Uiso 1 1 calc R U . . .
H43B H 0.262170 0.534629 0.570613 0.091 Uiso 1 1 calc R U . . .
C44 C 0.2419(7) 0.5135(9) 0.5112(10) 0.083(6) Uani 1 1 d . U . . .
H44A H 0.225193 0.525323 0.508431 0.100 Uiso 1 1 calc R U . . .
H44B H 0.242908 0.521394 0.487247 0.100 Uiso 1 1 calc R U . . .
C45 C 0.2403(8) 0.4722(9) 0.5122(10) 0.084(6) Uani 1 1 d . U . . .
H45A H 0.241268 0.464133 0.537608 0.100 Uiso 1 1 calc R U . . .
H45B H 0.256187 0.460288 0.512238 0.100 Uiso 1 1 calc R U . . .
C46 C 0.2127(7) 0.4545(9) 0.4742(10) 0.078(6) Uani 1 1 d . U . . .
H46A H 0.204237 0.474323 0.452032 0.094 Uiso 1 1 calc R U . . .
H46B H 0.199370 0.447452 0.482422 0.094 Uiso 1 1 calc R U . . .
C47 C 0.2522(6) 0.6117(8) 0.5308(9) 0.068(5) Uani 1 1 d . U . . .
C48 C 0.3065(7) 0.5902(11) 0.5884(10) 0.085(6) Uani 1 1 d . U . . .
C49 C 0.2402(7) 0.6109(9) 0.5547(10) 0.073(5) Uani 1 1 d . U . . .
H49 H 0.245811 0.591699 0.575645 0.088 Uiso 1 1 calc R U . . .
C50 C 0.2428(7) 0.6377(9) 0.4984(10) 0.074(5) Uani 1 1 d . U . . .
H50 H 0.249858 0.637084 0.480870 0.089 Uiso 1 1 calc R U . . .
C51 C 0.2221(7) 0.6657(10) 0.4923(11) 0.085(6) Uani 1 1 d . U . . .
H51 H 0.216003 0.684383 0.470807 0.103 Uiso 1 1 calc R U . . .
C52 C 0.1926(8) 0.5892(9) 0.4078(12) 0.092(6) Uani 1 1 d . U . . .
H52 H 0.206718 0.571726 0.411296 0.110 Uiso 1 1 calc R U . . .
C53 C 0.1680(7) 0.6512(9) 0.3819(12) 0.089(6) Uani 1 1 d . U . . .
H53 H 0.164767 0.675568 0.367499 0.106 Uiso 1 1 calc R U . . .
C54 C 0.3136(9) 0.7225(9) 0.4273(12) 0.096(7) Uani 1 1 d . U . . .
C55 C 0.3275(9) 0.7086(9) 0.5078(11) 0.090(6) Uani 1 1 d . U . . .
C56 C 0.4154(8) 0.6057(11) 0.5526(12) 0.095(7) Uani 1 1 d . U . . .
H56A H 0.405633 0.599097 0.566930 0.114 Uiso 1 1 calc R U . . .
H56B H 0.432219 0.620295 0.571524 0.114 Uiso 1 1 calc R U . . .
C57 C 0.4416(7) 0.5285(13) 0.5785(11) 0.094(6) Uani 1 1 d . U . . .
C58 C 0.4493(6) 0.5774(10) 0.5244(11) 0.082(6) Uani 1 1 d . U . . .
C59 C 0.3117(7) 0.6301(12) 0.5979(11) 0.091(6) Uani 1 1 d . U . . .
H59 H 0.299838 0.649830 0.579528 0.109 Uiso 1 1 calc R U . . .
C60 C 0.3346(8) 0.6416(12) 0.6347(11) 0.095(6) Uani 1 1 d . U . . .
H60 H 0.336957 0.669424 0.640216 0.115 Uiso 1 1 calc R U . . .
C61 C 0.4246(7) 0.5125(12) 0.3713(13) 0.093(6) Uani 1 1 d . U . . .
C62 C 0.3774(7) 0.5525(10) 0.3114(11) 0.094(8) Uani 1 1 d . U . . .
H62A H 0.363751 0.573583 0.305789 0.112 Uiso 1 1 calc R U . . .
H62B H 0.388879 0.561469 0.300637 0.112 Uiso 1 1 calc R U . . .
C63 C 0.4137(7) 0.5925(10) 0.3838(12) 0.091(6) Uani 1 1 d . U . . .
C64 C 0.2200(7) 0.6382(9) 0.5473(10) 0.079(5) Uani 1 1 d . U . . .
H64 H 0.212183 0.637787 0.563832 0.095 Uiso 1 1 calc R U . . .
C65 C 0.2107(7) 0.6670(9) 0.5157(11) 0.082(5) Uani 1 1 d . U . . .
H65 H 0.197133 0.686083 0.511231 0.098 Uiso 1 1 calc R U . . .
C66 C 0.1768(8) 0.5784(10) 0.4202(13) 0.101(6) Uani 1 1 d . U . . .
H66 H 0.179823 0.553492 0.433724 0.121 Uiso 1 1 calc R U . . .
C67 C 0.1510(8) 0.6383(10) 0.3971(13) 0.099(6) Uani 1 1 d . U . . .
H67 H 0.137018 0.655368 0.394926 0.118 Uiso 1 1 calc R U . . .
C68 C 0.2411(6) 0.7047(8) 0.4165(9) 0.065(5) Uani 1 1 d . U . . .
H68 H 0.252494 0.684711 0.434914 0.078 Uiso 1 1 calc R U . . .
C69 C 0.2478(6) 0.7434(8) 0.4256(9) 0.068(5) Uani 1 1 d . U . . .
H69 H 0.264279 0.750827 0.449449 0.082 Uiso 1 1 calc R U . . .
C70 C 0.2300(6) 0.7727(8) 0.3991(9) 0.069(5) Uani 1 1 d . U . . .
H70 H 0.234483 0.800108 0.405609 0.083 Uiso 1 1 calc R U . . .
C71 C 0.2073(7) 0.7636(8) 0.3657(9) 0.069(5) Uani 1 1 d . U . . .
H71 H 0.195561 0.783978 0.348276 0.083 Uiso 1 1 calc R U . . .
C72 C 0.2008(6) 0.7234(7) 0.3563(9) 0.063(5) Uani 1 1 d . U . . .
H72 H 0.184182 0.716376 0.332570 0.076 Uiso 1 1 calc R U . . .
C73 C 0.2047(7) 0.5871(12) 0.1837(9) 0.087(6) Uani 1 1 d . U . . .
C74 C 0.2561(7) 0.6260(9) 0.2123(9) 0.078(5) Uani 1 1 d . U . . .
C75 C 0.2047(8) 0.5491(13) 0.1683(10) 0.097(6) Uani 1 1 d . U . . .
H75 H 0.220995 0.533906 0.181969 0.116 Uiso 1 1 calc R U . . .
C76 C 0.1798(8) 0.6080(13) 0.1625(10) 0.099(7) Uani 1 1 d . U . . .
H76 H 0.179164 0.634111 0.171536 0.119 Uiso 1 1 calc R U . . .
C77 C 0.2440(8) 0.6500(10) 0.1792(10) 0.085(6) Uani 1 1 d . U . . .
H77 H 0.224820 0.653299 0.163572 0.102 Uiso 1 1 calc R U . . .
C78 C 0.2620(8) 0.6702(10) 0.1690(10) 0.086(6) Uani 1 1 d . U . . .
H78 H 0.255067 0.688692 0.147266 0.103 Uiso 1 1 calc R U . . .
C79 C 0.2847(8) 0.6188(10) 0.2337(10) 0.085(6) Uani 1 1 d . U . . .
H79 H 0.292486 0.600235 0.255411 0.103 Uiso 1 1 calc R U . . .
C80 C 0.2996(8) 0.6372(10) 0.2239(11) 0.087(6) Uani 1 1 d . U . . .
H80 H 0.318764 0.633234 0.239863 0.105 Uiso 1 1 calc R U . . .
C81 C 0.1851(8) 0.4331(11) 0.1801(10) 0.092(7) Uani 1 1 d . U . . .
C82 C 0.1596(9) 0.4371(11) 0.1428(11) 0.104(7) Uani 1 1 d . U . . .
H82 H 0.144171 0.447945 0.142574 0.125 Uiso 1 1 calc R U . . .
C83 C 0.2057(8) 0.4162(11) 0.1780(11) 0.094(7) Uani 1 1 d . U . . .
H83 H 0.222981 0.414199 0.202069 0.113 Uiso 1 1 calc R U . . .
C84 C 0.2030(9) 0.4010(11) 0.1415(11) 0.101(7) Uani 1 1 d . U . . .
H84 H 0.218227 0.389247 0.141806 0.121 Uiso 1 1 calc R U . . .
C85 C 0.2777(7) 0.3947(9) 0.2273(10) 0.078(5) Uani 1 1 d . U . . .
H85 H 0.276057 0.404886 0.248946 0.094 Uiso 1 1 calc R U . . .
C86 C 0.2729(7) 0.3528(9) 0.2162(10) 0.084(6) Uani 1 1 d . U . . .
H86 H 0.268040 0.335397 0.230897 0.101 Uiso 1 1 calc R U . . .
C87 C 0.2750(7) 0.3386(9) 0.1868(10) 0.082(6) Uani 1 1 d . U . . .
H87 H 0.272130 0.310942 0.180638 0.099 Uiso 1 1 calc R U . . .
C88 C 0.2813(7) 0.3631(9) 0.1645(10) 0.080(5) Uani 1 1 d . U . . .
H88 H 0.282295 0.352512 0.142449 0.096 Uiso 1 1 calc R U . . .
C89 C 0.2863(7) 0.4039(9) 0.1739(10) 0.076(5) Uani 1 1 d . U . . .
H89 H 0.290646 0.421404 0.158680 0.092 Uiso 1 1 calc R U . . .
C90 C 0.2845(7) 0.4178(9) 0.2067(10) 0.076(5) Uani 1 1 d . U . . .
C91 C 0.1487(7) 0.3573(10) 0.3881(11) 0.089(6) Uani 1 1 d . U . . .
H91 H 0.134318 0.347727 0.391304 0.107 Uiso 1 1 calc R U . . .
C92 C 0.2903(8) 0.6617(11) 0.1925(11) 0.091(6) Uani 1 1 d . U . . .
H92 H 0.302472 0.673543 0.185727 0.109 Uiso 1 1 calc R U . . .
C93 C 0.1813(7) 0.4010(10) 0.2440(10) 0.088(7) Uani 1 1 d . U . . .
H93A H 0.179563 0.405878 0.267898 0.105 Uiso 1 1 calc R U . . .
H93B H 0.163743 0.390589 0.221900 0.105 Uiso 1 1 calc R U . . .
C94 C 0.1627(5) 0.4803(7) 0.2182(10) 0.115(8) Uani 1 1 d G U . . .
C127 C 0.1673(4) 0.5211(8) 0.2179(10) 0.116(8) Uani 1 1 d G U . . .
H127 H 0.184549 0.530441 0.223680 0.139 Uiso 1 1 calc R U . . .
C128 C 0.1465(5) 0.5482(6) 0.2093(10) 0.121(8) Uani 1 1 d G U . . .
H128 H 0.149674 0.576015 0.209114 0.146 Uiso 1 1 calc R U . . .
C165 C 0.1212(5) 0.5345(7) 0.2009(10) 0.123(8) Uani 1 1 d G U . . .
H165 H 0.107073 0.552967 0.194993 0.148 Uiso 1 1 calc R U . . .
C164 C 0.1166(4) 0.4937(8) 0.2012(10) 0.128(8) Uani 1 1 d G U . . .
H164 H 0.099347 0.484343 0.195437 0.154 Uiso 1 1 calc R U . . .
C166 C 0.1374(5) 0.4666(6) 0.2098(10) 0.124(8) Uani 1 1 d G U . . .
H166 H 0.134222 0.438768 0.210002 0.149 Uiso 1 1 calc R U . . .
C95 C 0.3244(8) 0.4791(12) 0.2272(15) 0.118(9) Uani 1 1 d . U . . .
H95A H 0.336059 0.456600 0.243586 0.141 Uiso 1 1 calc R U . . .
H95B H 0.322528 0.477259 0.200331 0.141 Uiso 1 1 calc R U . . .
C96 C 0.4671(7) 0.6050(11) 0.5444(12) 0.093(6) Uani 1 1 d . U . . .
H96 H 0.466367 0.618864 0.565301 0.111 Uiso 1 1 calc R U . . .
C97 C 0.4498(7) 0.5617(11) 0.4928(12) 0.089(6) Uani 1 1 d . U . . .
H97 H 0.436747 0.541614 0.477686 0.107 Uiso 1 1 calc R U . . .
C98 C 0.4672(7) 0.5719(11) 0.4807(13) 0.100(7) Uani 1 1 d . U . . .
H98 H 0.465939 0.560222 0.457276 0.120 Uiso 1 1 calc R U . . .
C99 C 0.4873(7) 0.6001(12) 0.5036(13) 0.100(7) Uani 1 1 d . U . . .
H99 H 0.500026 0.608279 0.496267 0.120 Uiso 1 1 calc R U . . .
C100 C 0.4344(7) 0.6082(11) 0.3778(13) 0.097(6) Uani 1 1 d . U . . .
H100 H 0.441265 0.593393 0.363903 0.116 Uiso 1 1 calc R U . . .
C101 C 0.4047(8) 0.6163(11) 0.4053(13) 0.099(7) Uani 1 1 d . U . . .
H101 H 0.391533 0.606598 0.411094 0.119 Uiso 1 1 calc R U . . .
C102 C 0.4360(8) 0.4866(12) 0.4043(13) 0.099(7) Uani 1 1 d . U . . .
H102 H 0.428989 0.487416 0.421894 0.119 Uiso 1 1 calc R U . . .
C103 C 0.4572(8) 0.4592(12) 0.4135(14) 0.105(7) Uani 1 1 d . U . . .
H103 H 0.465899 0.444835 0.438268 0.126 Uiso 1 1 calc R U . . .
C104 C 0.4645(8) 0.4545(13) 0.3866(14) 0.107(7) Uani 1 1 d . U . . .
H104 H 0.476679 0.433641 0.389728 0.129 Uiso 1 1 calc R U . . .
C105 C 0.4550(8) 0.4782(13) 0.3556(14) 0.103(7) Uani 1 1 d . U . . .
H105 H 0.462609 0.476481 0.338748 0.124 Uiso 1 1 calc R U . . .
C106 C 0.3197(8) 0.2145(9) 0.3881(11) 0.086(6) Uani 1 1 d . U . . .
H106 H 0.335287 0.198076 0.397319 0.104 Uiso 1 1 calc R U . . .
C107 C 0.3535(8) 0.2719(9) 0.5533(11) 0.088(6) Uani 1 1 d . U . . .
H107 H 0.371943 0.278463 0.572143 0.105 Uiso 1 1 calc R U . . .
C108 C 0.3439(8) 0.2318(10) 0.5448(12) 0.094(6) Uani 1 1 d . U . . .
H108 H 0.356325 0.210732 0.558977 0.113 Uiso 1 1 calc R U . . .
C109 C 0.3666(8) 0.6883(12) 0.4836(12) 0.099(8) Uani 1 1 d . U . . .
H10A H 0.368852 0.680871 0.460634 0.119 Uiso 1 1 calc R U . . .
H10B H 0.372890 0.716194 0.491181 0.119 Uiso 1 1 calc R U . . .
C110 C 0.3830(9) 0.6632(12) 0.5165(12) 0.103(7) Uani 1 1 d . U . . .
H11X H 0.396303 0.680935 0.538272 0.124 Uiso 1 1 calc R U . . .
H11Y H 0.371027 0.652641 0.525856 0.124 Uiso 1 1 calc R U . . .
C111 C 0.3973(8) 0.6320(12) 0.5159(12) 0.102(7) Uani 1 1 d . U . . .
H11A H 0.409187 0.642239 0.506209 0.122 Uiso 1 1 calc R U . . .
H11B H 0.384073 0.613772 0.494596 0.122 Uiso 1 1 calc R U . . .
C112 C 0.4468(7) 0.4149(10) 0.5125(11) 0.083(6) Uani 1 1 d . U . . .
C113 C 0.4553(7) 0.4529(10) 0.5131(12) 0.089(6) Uani 1 1 d . U . . .
H113 H 0.443846 0.470106 0.491282 0.106 Uiso 1 1 calc R U . . .
C114 C 0.4795(7) 0.4678(12) 0.5438(12) 0.096(6) Uani 1 1 d . U . . .
H114 H 0.485459 0.493898 0.542318 0.115 Uiso 1 1 calc R U . . .
C115 C 0.4611(8) 0.3894(12) 0.5434(12) 0.099(7) Uani 1 1 d . U . . .
H115 H 0.455077 0.363325 0.544706 0.118 Uiso 1 1 calc R U . . .
C116 C 0.4653(8) 0.5373(13) 0.6125(11) 0.102(7) Uani 1 1 d . U . . .
H116 H 0.474035 0.562171 0.614841 0.122 Uiso 1 1 calc R U . . .
C117 C 0.4299(8) 0.4898(13) 0.5766(12) 0.101(7) Uani 1 1 d . U . . .
H117 H 0.413619 0.481713 0.552886 0.121 Uiso 1 1 calc R U . . .
C118 C 0.4426(8) 0.4643(14) 0.6099(12) 0.105(7) Uani 1 1 d . U . . .
H118 H 0.434303 0.439510 0.609424 0.127 Uiso 1 1 calc R U . . .
C119 C 0.3071(8) 0.7002(9) 0.5135(11) 0.088(6) Uani 1 1 d . U . . .
H119 H 0.294227 0.680631 0.496623 0.106 Uiso 1 1 calc R U . . .
C120 C 0.3035(9) 0.7190(10) 0.5434(12) 0.098(6) Uani 1 1 d . U . . .
H120 H 0.288401 0.712026 0.546032 0.117 Uiso 1 1 calc R U . . .
C121 C 0.3472(9) 0.7358(9) 0.5356(12) 0.099(7) Uani 1 1 d . U . . .
H121 H 0.362914 0.741886 0.534058 0.119 Uiso 1 1 calc R U . . .
C122 C 0.3241(7) 0.5626(12) 0.6168(10) 0.089(6) Uani 1 1 d . U . . .
H122 H 0.320721 0.534909 0.611156 0.106 Uiso 1 1 calc R U . . .
C123 C 0.4237(7) 0.3752(11) 0.4373(12) 0.091(6) Uani 1 1 d . U . . .
C124 C 0.4099(8) 0.3851(12) 0.3961(13) 0.103(7) Uani 1 1 d . U . . .
H124 H 0.396231 0.405174 0.385878 0.124 Uiso 1 1 calc R U . . .
C125 C 0.4166(8) 0.3651(12) 0.3696(14) 0.106(7) Uani 1 1 d . U . . .
H125 H 0.407584 0.371299 0.341560 0.127 Uiso 1 1 calc R U . . .
C126 C 0.4451(7) 0.3467(11) 0.4518(13) 0.096(6) Uani 1 1 d . U . . .
H126 H 0.455350 0.341600 0.479993 0.115 Uiso 1 1 calc R U . . .
C129 C 0.3196(10) 0.7619(10) 0.4333(13) 0.106(7) Uani 1 1 d . U . . .
H129 H 0.332705 0.771083 0.459516 0.127 Uiso 1 1 calc R U . . .
C130 C 0.2920(10) 0.7079(11) 0.3887(12) 0.107(7) Uani 1 1 d . U . . .
H130 H 0.287523 0.680266 0.384655 0.128 Uiso 1 1 calc R U . . .
C131 C 0.4158(8) 0.6538(11) 0.4174(14) 0.106(7) Uani 1 1 d . U . . .
H131 H 0.408066 0.670695 0.428652 0.127 Uiso 1 1 calc R U . . .
C132 C 0.2361(6) 0.3203(9) 0.3063(9) 0.074(6) Uani 1 1 d . U . . .
H13A H 0.248264 0.329076 0.296513 0.088 Uiso 1 1 calc R U . . .
H13B H 0.227501 0.294802 0.292838 0.088 Uiso 1 1 calc R U . . .
C133 C 0.2147(7) 0.3512(10) 0.2962(9) 0.080(6) Uani 1 1 d . U . . .
H13C H 0.222252 0.372501 0.316979 0.096 Uiso 1 1 calc R U . . .
H13D H 0.199217 0.338800 0.296747 0.096 Uiso 1 1 calc R U . . .
C134 C 0.2046(8) 0.3697(11) 0.2547(10) 0.092(6) Uani 1 1 d . U . . .
H13E H 0.197616 0.348391 0.234018 0.110 Uiso 1 1 calc R U . . .
H13F H 0.219902 0.383110 0.254467 0.110 Uiso 1 1 calc R U . . .
C135 C 0.4517(8) 0.3263(12) 0.4276(13) 0.103(7) Uani 1 1 d . U . . .
H135 H 0.465619 0.306504 0.437632 0.124 Uiso 1 1 calc R U . . .
C136 C 0.4364(8) 0.3368(12) 0.3863(14) 0.104(7) Uani 1 1 d . U . . .
H136 H 0.440245 0.322646 0.368416 0.124 Uiso 1 1 calc R U . . .
C137 C 0.4330(7) 0.5081(12) 0.3450(13) 0.101(7) Uani 1 1 d . U . . .
H137 H 0.425357 0.523189 0.320710 0.121 Uiso 1 1 calc R U . . .
C138 C 0.2703(7) 0.4973(10) 0.1751(10) 0.080(6) Uani 1 1 d . U . . .
C139 C 0.2447(8) 0.4815(11) 0.1419(10) 0.090(6) Uani 1 1 d . U . . .
H139 H 0.239550 0.455213 0.144553 0.108 Uiso 1 1 calc R U . . .
C140 C 0.2275(9) 0.5023(11) 0.1072(12) 0.101(7) Uani 1 1 d . U . . .
H140 H 0.210946 0.491242 0.086225 0.122 Uiso 1 1 calc R U . . .
C141 C 0.2359(8) 0.5396(11) 0.1049(12) 0.097(6) Uani 1 1 d . U . . .
H141 H 0.225002 0.553945 0.080414 0.116 Uiso 1 1 calc R U . . .
C142 C 0.2566(8) 0.5569(12) 0.1321(11) 0.095(6) Uani 1 1 d . U . . .
H142 H 0.260453 0.583584 0.128281 0.114 Uiso 1 1 calc R U . . .
C143 C 0.2732(8) 0.5380(11) 0.1664(11) 0.092(6) Uani 1 1 d . U . . .
H143 H 0.288212 0.552606 0.186765 0.111 Uiso 1 1 calc R U . . .
C144 C 0.1824(8) 0.5319(15) 0.1342(11) 0.109(7) Uani 1 1 d . U . . .
H144 H 0.182935 0.505635 0.125205 0.131 Uiso 1 1 calc R U . . .
C145 C 0.1545(9) 0.5922(14) 0.1270(11) 0.110(7) Uani 1 1 d . U . . .
H145 H 0.137343 0.605308 0.114939 0.132 Uiso 1 1 calc R U . . .
C146 C 0.1590(9) 0.5568(15) 0.1142(12) 0.117(7) Uani 1 1 d . U . . .
H146 H 0.144734 0.547607 0.088676 0.141 Uiso 1 1 calc R U . . .
C147 C 0.1579(9) 0.4247(12) 0.1072(12) 0.110(7) Uani 1 1 d . U . . .
H147 H 0.141923 0.430756 0.082183 0.132 Uiso 1 1 calc R U . . .
C148 C 0.1791(9) 0.4034(12) 0.1070(12) 0.106(7) Uani 1 1 d . U . . .
H148 H 0.176444 0.391192 0.083029 0.127 Uiso 1 1 calc R U . . .
C149 C 0.3622(8) 0.5126(11) 0.2894(12) 0.102(8) Uani 1 1 d . U . . .
H14E H 0.375527 0.493729 0.289358 0.123 Uiso 1 1 calc R U . . .
H14F H 0.354566 0.499989 0.304690 0.123 Uiso 1 1 calc R U . . .
C150 C 0.3403(8) 0.5195(12) 0.2478(14) 0.115(8) Uani 1 1 d . U . . .
H15A H 0.347997 0.530551 0.232008 0.138 Uiso 1 1 calc R U . . .
H15B H 0.327415 0.539378 0.247626 0.138 Uiso 1 1 calc R U . . .
C151 C 0.4880(8) 0.6152(12) 0.5359(13) 0.104(7) Uani 1 1 d . U . . .
H151 H 0.502292 0.632698 0.553405 0.125 Uiso 1 1 calc R U . . .
C152 C 0.4356(8) 0.6680(12) 0.4148(14) 0.111(7) Uani 1 1 d . U . . .
H152 H 0.443859 0.692672 0.427379 0.133 Uiso 1 1 calc R U . . .
C153 C 0.4446(8) 0.6472(11) 0.3937(14) 0.104(7) Uani 1 1 d . U . . .
H153 H 0.457970 0.658834 0.389331 0.125 Uiso 1 1 calc R U . . .
C154 C 0.3433(10) 0.7545(10) 0.5664(13) 0.108(7) Uani 1 1 d . U . . .
H154 H 0.356622 0.772398 0.585290 0.129 Uiso 1 1 calc R U . . .
C155 C 0.3214(9) 0.7467(10) 0.5682(13) 0.102(7) Uani 1 1 d . U . . .
H155 H 0.318277 0.760501 0.586885 0.123 Uiso 1 1 calc R U . . .
C156 C 0.4773(8) 0.5091(14) 0.6447(13) 0.110(7) Uani 1 1 d . U . . .
H156 H 0.493824 0.516153 0.668579 0.132 Uiso 1 1 calc R U . . .
C157 C 0.4668(8) 0.4746(14) 0.6431(13) 0.110(7) Uani 1 1 d . U . . .
H157 H 0.475902 0.456444 0.664952 0.132 Uiso 1 1 calc R U . . .
C158 C 0.3069(10) 0.7895(11) 0.4016(13) 0.111(7) Uani 1 1 d . U . . .
H158 H 0.311567 0.817007 0.406215 0.134 Uiso 1 1 calc R U . . .
C159 C 0.2884(10) 0.7769(11) 0.3654(14) 0.114(8) Uani 1 1 d . U . . .
H159 H 0.281582 0.795027 0.343345 0.137 Uiso 1 1 calc R U . . .
C160 C 0.2779(11) 0.7354(11) 0.3578(14) 0.115(8) Uani 1 1 d . U . . .
H160 H 0.262238 0.727965 0.332905 0.138 Uiso 1 1 calc R U . . .
C161 C 0.3464(8) 0.5747(13) 0.6531(11) 0.100(7) Uani 1 1 d . U . . .
H161 H 0.357880 0.555528 0.672565 0.120 Uiso 1 1 calc R U . . .
C162 C 0.3521(8) 0.6190(13) 0.6612(11) 0.103(7) Uani 1 1 d . U . . .
H162 H 0.367846 0.628976 0.684593 0.123 Uiso 1 1 calc R U . . .
C163 C 0.1549(8) 0.6024(10) 0.4145(13) 0.102(6) Uani 1 1 d . U . . .
H163 H 0.142927 0.593102 0.422874 0.122 Uiso 1 1 calc R U . . .
C167 C 0.4939(8) 0.4451(12) 0.5746(14) 0.105(7) Uani 1 1 d . U . . .
H167 H 0.509598 0.455744 0.597479 0.126 Uiso 1 1 calc R U . . .
C168 C 0.4872(8) 0.4070(12) 0.5751(13) 0.105(7) Uani 1 1 d . U . . .
H168 H 0.499795 0.390337 0.596606 0.127 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
W1 O8 1.752(19) . ?
W1 O9 1.775(15) . ?
W1 O2 1.797(17) . ?
W1 O10 1.797(19) . ?
W2 O11 1.77(2) . ?
W2 O12 1.778(16) . ?
W2 O13 1.78(2) . ?
W2 O1 1.795(15) . ?
W3 O14 1.78(2) . ?
W3 O15 1.789(17) . ?
W3 O17 1.79(2) . ?
W3 O16 1.808(17) . ?
W4 O6 1.77(2) . ?
W4 O3 1.796(17) . ?
W4 O7 1.80(2) . ?
W4 O5 1.800(18) . ?
Ag1 O1 2.244(16) . ?
Ag1 Ag11 2.701(2) . ?
Ag1 Ag20 2.825(3) . ?
Ag1 Ag17 2.852(2) . ?
Ag1 Ag28 2.928(3) . ?
Ag1 Ag22 2.949(3) . ?
Ag1 Ag18 2.964(3) . ?
Ag1 Ag23 3.028(3) . ?
Ag1 Ag27 3.175(3) . ?
Ag2 O3 2.262(17) . ?
Ag2 Ag15 2.695(3) . ?
Ag2 Ag22 2.840(3) . ?
Ag2 Ag9 2.846(3) . ?
Ag2 Ag16 2.947(2) . ?
Ag2 Ag12 2.957(3) . ?
Ag2 Ag3 2.989(3) . ?
Ag2 Ag23 3.052(2) . ?
Ag2 Ag19 3.122(3) . ?
Ag3 O7 2.270(17) . ?
Ag3 Ag10 2.688(2) . ?
Ag3 Ag4 2.814(3) . ?
Ag3 Ag19 2.846(2) . ?
Ag3 Ag16 2.963(3) . ?
Ag3 Ag14 2.981(3) . ?
Ag3 Ag15 3.002(2) . ?
Ag3 Ag24 3.203(2) . ?
Ag4 O14 2.256(18) . ?
Ag4 Ag15 2.692(2) . ?
Ag4 Ag14 2.862(2) . ?
Ag4 Ag5 2.963(3) . ?
Ag4 Ag6 2.964(3) . ?
Ag4 Ag10 3.000(2) . ?
Ag4 Ag19 3.048(3) . ?
Ag4 Ag26 3.181(2) . ?
Ag5 O15 2.242(17) . ?
Ag5 Ag11 2.695(2) . ?
Ag5 Ag18 2.824(3) . ?
Ag5 Ag26 2.873(3) . ?
Ag5 Ag27 2.957(3) . ?
Ag5 Ag6 2.992(2) . ?
Ag5 Ag15 3.032(3) . ?
Ag5 Ag25 3.159(3) . ?
Ag6 O16 2.241(17) . ?
Ag6 Ag10 2.689(3) . ?
Ag6 Ag8 2.807(3) . ?
Ag6 Ag25 2.848(3) . ?
Ag6 Ag11 3.000(2) . ?
Ag6 Ag7 3.006(3) . ?
Ag6 Ag14 3.150(3) . ?
Ag7 P10 2.460(6) . ?
Ag7 Ag10 2.763(2) . ?
Ag7 Ag24 2.844(3) . ?
Ag7 Ag14 2.849(3) . ?
Ag7 Ag8 2.860(3) . ?
Ag7 Ag13 3.083(3) . ?
Ag8 O10 2.251(15) . ?
Ag8 Ag11 2.677(2) . ?
Ag8 Ag17 2.937(3) . ?
Ag8 Ag13 2.977(3) . ?
Ag8 Ag25 2.979(3) . ?
Ag8 Ag10 3.027(2) . ?
Ag8 Ag28 3.211(3) . ?
Ag9 P3 2.456(7) . ?
Ag9 Ag23 2.767(3) . ?
Ag9 Ag21 2.840(3) . ?
Ag9 Ag20 2.841(3) . ?
Ag9 Ag22 2.941(3) . ?
Ag9 Ag16 3.159(3) . ?
Ag10 Ag13 2.683(2) . ?
Ag10 Ag14 2.758(2) . ?
Ag10 Ag24 2.811(2) . ?
Ag10 Ag23 2.855(2) . ?
Ag10 Ag15 2.874(2) . ?
Ag10 Ag11 2.895(2) . ?
Ag10 Ag16 2.976(3) . ?
Ag11 Ag27 2.776(3) . ?
Ag11 Ag25 2.779(3) . ?
Ag11 Ag28 2.784(3) . ?
Ag11 Ag23 2.859(3) . ?
Ag11 Ag15 2.879(2) . ?
Ag11 Ag18 2.999(2) . ?
Ag11 Ag17 3.016(3) . ?
Ag12 P12 2.459(7) . ?
Ag12 Ag15 2.812(2) . ?
Ag12 Ag22 2.832(3) . ?
Ag12 Ag19 2.846(3) . ?
Ag12 Ag26 2.860(3) . ?
Ag12 Ag18 3.203(3) . ?
Ag13 O8 2.281(15) . ?
Ag13 Ag16 2.837(3) . ?
Ag13 Ag21 2.839(3) . ?
Ag13 Ag24 2.979(3) . ?
Ag13 Ag17 2.990(3) . ?
Ag13 Ag23 2.990(2) . ?
Ag14 P11 2.460(7) . ?
Ag14 Ag24 2.877(3) . ?
Ag15 Ag18 2.698(2) . ?
Ag15 Ag26 2.756(2) . ?
Ag15 Ag19 2.781(2) . ?
Ag15 Ag23 2.869(2) . ?
Ag15 Ag22 2.985(2) . ?
Ag16 O5 2.255(18) . ?
Ag16 Ag23 2.682(3) . ?
Ag16 Ag24 2.841(3) . ?
Ag16 Ag21 2.996(3) . ?
Ag17 O2 2.285(16) . ?
Ag17 Ag23 2.695(2) . ?
Ag17 Ag28 2.856(3) . ?
Ag17 Ag20 2.945(3) . ?
Ag17 Ag21 3.176(3) . ?
Ag18 O13 2.267(17) . ?
Ag18 Ag27 2.839(3) . ?
Ag18 Ag26 2.953(3) . ?
Ag18 Ag22 2.959(3) . ?
Ag19 P9 2.488(7) . ?
Ag19 Ag26 2.840(3) . ?
Ag20 P4 2.451(7) . ?
Ag20 Ag23 2.764(2) . ?
Ag20 Ag21 2.838(3) . ?
Ag20 Ag22 3.155(3) . ?
Ag21 P2 2.450(7) . ?
Ag21 Ag23 2.769(3) . ?
Ag22 O11 2.254(16) . ?
Ag22 Ag23 2.684(2) . ?
Ag24 P1 2.477(7) . ?
Ag25 P7 2.464(8) . ?
Ag25 Ag27 2.836(3) . ?
Ag25 Ag28 2.884(3) . ?
Ag26 P8 2.453(7) . ?
Ag27 P6 2.442(7) . ?
Ag27 Ag28 2.815(3) . ?
Ag28 P5 2.481(8) . ?
P1 C19 1.77(3) . ?
P1 C25 1.81(3) . ?
P1 C26 1.88(3) . ?
P2 C112 1.78(4) . ?
P2 C29 1.80(3) . ?
P2 C123 1.80(3) . ?
P3 C57 1.77(4) . ?
P3 C56 1.82(3) . ?
P3 C58 1.82(3) . ?
P4 C63 1.78(3) . ?
P4 C61 1.78(4) . ?
P4 C62 1.79(4) . ?
P5 C95 1.77(4) . ?
P5 C138 1.77(4) . ?
P5 C90 1.85(3) . ?
P6 C73 1.78(4) . ?
P6 C42 1.81(3) . ?
P6 C74 1.84(3) . ?
P7 C93 1.79(3) . ?
P7 C94 1.794(19) . ?
P7 C81 1.80(4) . ?
P8 C39 1.79(3) . ?
P8 C38 1.79(3) . ?
P8 C8 1.82(2) . ?
P9 C48 1.79(4) . ?
P9 C43 1.80(3) . ?
P9 C47 1.81(3) . ?
P10 C7 1.81(3) . ?
P10 C132 1.84(3) . ?
P10 C1 1.84(2) . ?
P11 C33 1.78(3) . ?
P11 C13 1.83(3) . ?
P11 C46 1.85(3) . ?
P12 C54 1.82(4) . ?
P12 C55 1.82(3) . ?
P12 C109 1.83(4) . ?
C1 C6 1.30(4) . ?
C1 C2 1.38(4) . ?
C2 C3 1.40(4) . ?
C3 C4 1.39(4) . ?
C4 C5 1.41(4) . ?
C5 C6 1.43(4) . ?
C7 C11 1.33(4) . ?
C7 C9 1.46(4) . ?
C8 C68 1.38(4) . ?
C8 C72 1.39(3) . ?
C9 C10 1.37(4) . ?
C10 C106 1.43(5) . ?
C11 C12 1.40(4) . ?
C12 C106 1.33(4) . ?
C13 C18 1.37(4) . ?
C13 C14 1.38(4) . ?
C14 C15 1.47(4) . ?
C15 C16 1.36(4) . ?
C16 C17 1.39(4) . ?
C17 C18 1.39(4) . ?
C19 C20 1.41(4) . ?
C19 C24 1.41(4) . ?
C20 C21 1.47(4) . ?
C21 C22 1.42(4) . ?
C22 C23 1.37(4) . ?
C23 C24 1.34(4) . ?
C25 C30 1.33(5) . ?
C25 C107 1.47(5) . ?
C26 C27 1.58(4) . ?
C27 C28 1.45(4) . ?
C28 C29 1.59(4) . ?
C30 C32 1.41(4) . ?
C31 C32 1.28(5) . ?
C31 C108 1.33(5) . ?
C33 C34 1.39(4) . ?
C33 C35 1.44(5) . ?
C34 C91 1.43(5) . ?
C35 C36 1.31(5) . ?
C36 C37 1.39(4) . ?
C37 C91 1.41(5) . ?
C38 C53 1.39(4) . ?
C38 C52 1.39(4) . ?
C39 C40 1.51(4) . ?
C40 C41 1.41(4) . ?
C41 C42 1.54(4) . ?
C43 C44 1.54(5) . ?
C44 C45 1.39(4) . ?
C45 C46 1.62(5) . ?
C47 C50 1.38(4) . ?
C47 C49 1.41(3) . ?
C48 C59 1.38(5) . ?
C48 C122 1.39(5) . ?
C49 C64 1.38(4) . ?
C50 C51 1.43(4) . ?
C51 C65 1.36(4) . ?
C52 C66 1.27(4) . ?
C53 C67 1.44(4) . ?
C54 C129 1.35(5) . ?
C54 C130 1.45(6) . ?
C55 C119 1.32(5) . ?
C55 C121 1.42(5) . ?
C56 C111 1.53(5) . ?
C57 C116 1.35(5) . ?
C57 C117 1.44(5) . ?
C58 C96 1.30(4) . ?
C58 C97 1.34(5) . ?
C59 C60 1.40(5) . ?
C60 C162 1.25(5) . ?
C61 C137 1.34(5) . ?
C61 C102 1.39(6) . ?
C62 C149 1.58(5) . ?
C63 C101 1.42(5) . ?
C63 C100 1.42(4) . ?
C64 C65 1.42(4) . ?
C66 C163 1.40(5) . ?
C67 C163 1.34(5) . ?
C68 C69 1.35(4) . ?
C69 C70 1.41(4) . ?
C70 C71 1.31(4) . ?
C71 C72 1.39(4) . ?
C73 C75 1.40(5) . ?
C73 C76 1.41(5) . ?
C74 C77 1.36(4) . ?
C74 C79 1.42(5) . ?
C75 C144 1.40(5) . ?
C76 C145 1.49(5) . ?
C77 C78 1.44(5) . ?
C78 C92 1.42(5) . ?
C79 C80 1.26(4) . ?
C80 C92 1.32(5) . ?
C81 C83 1.35(5) . ?
C81 C82 1.44(5) . ?
C82 C147 1.39(5) . ?
C83 C84 1.42(5) . ?
C84 C148 1.33(5) . ?
C85 C90 1.30(4) . ?
C85 C86 1.45(4) . ?
C86 C87 1.29(4) . ?
C87 C88 1.36(4) . ?
C88 C89 1.40(4) . ?
C89 C90 1.39(4) . ?
C93 C134 1.57(5) . ?
C94 C127 1.3900 . ?
C94 C166 1.3900 . ?
C127 C128 1.3900 . ?
C128 C165 1.3900 . ?
C165 C164 1.3900 . ?
C164 C166 1.3900 . ?
C95 C150 1.59(5) . ?
C96 C151 1.43(5) . ?
C97 C98 1.34(5) . ?
C98 C99 1.40(5) . ?
C99 C151 1.32(5) . ?
C100 C153 1.43(5) . ?
C101 C131 1.38(5) . ?
C102 C103 1.41(5) . ?
C103 C104 1.31(5) . ?
C104 C105 1.30(6) . ?
C105 C137 1.49(5) . ?
C107 C108 1.42(4) . ?
C109 C110 1.40(5) . ?
C110 C111 1.33(5) . ?
C112 C115 1.34(5) . ?
C112 C113 1.36(5) . ?
C113 C114 1.37(5) . ?
C114 C167 1.29(5) . ?
C115 C168 1.48(5) . ?
C116 C156 1.42(5) . ?
C117 C118 1.39(5) . ?
C118 C157 1.36(5) . ?
C119 C120 1.42(4) . ?
C120 C155 1.35(5) . ?
C121 C154 1.46(5) . ?
C122 C161 1.38(5) . ?
C123 C124 1.41(5) . ?
C123 C126 1.42(5) . ?
C124 C125 1.43(5) . ?
C125 C136 1.36(6) . ?
C126 C135 1.36(5) . ?
C129 C158 1.40(5) . ?
C130 C160 1.39(5) . ?
C131 C152 1.28(5) . ?
C132 C133 1.49(4) . ?
C133 C134 1.52(4) . ?
C135 C136 1.41(6) . ?
C138 C143 1.43(5) . ?
C138 C139 1.46(5) . ?
C139 C140 1.38(5) . ?
C140 C141 1.36(5) . ?
C141 C142 1.25(5) . ?
C142 C143 1.33(5) . ?
C144 C146 1.43(6) . ?
C145 C146 1.36(6) . ?
C147 C148 1.41(6) . ?
C149 C150 1.46(5) . ?
C152 C153 1.36(5) . ?
C154 C155 1.31(5) . ?
C156 C157 1.29(6) . ?
C158 C159 1.31(6) . ?
C159 C160 1.48(6) . ?
C161 C162 1.52(6) . ?
C167 C168 1.33(5) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O8 W1 O9 111.0(9) . . ?
O8 W1 O2 107.9(8) . . ?
O9 W1 O2 108.2(8) . . ?
O8 W1 O10 109.3(8) . . ?
O9 W1 O10 110.4(8) . . ?
O2 W1 O10 110.0(8) . . ?
O11 W2 O12 110.2(10) . . ?
O11 W2 O13 108.4(8) . . ?
O12 W2 O13 111.3(9) . . ?
O11 W2 O1 109.2(9) . . ?
O12 W2 O1 109.6(8) . . ?
O13 W2 O1 108.1(8) . . ?
O14 W3 O15 108.3(8) . . ?
O14 W3 O17 110.2(9) . . ?
O15 W3 O17 110.6(9) . . ?
O14 W3 O16 108.5(8) . . ?
O15 W3 O16 108.9(8) . . ?
O17 W3 O16 110.4(10) . . ?
O6 W4 O3 110.8(9) . . ?
O6 W4 O7 109.4(9) . . ?
O3 W4 O7 108.1(8) . . ?
O6 W4 O5 109.5(9) . . ?
O3 W4 O5 108.4(9) . . ?
O7 W4 O5 110.5(8) . . ?
O1 Ag1 Ag11 151.3(5) . . ?
O1 Ag1 Ag20 92.1(5) . . ?
Ag11 Ag1 Ag20 112.69(8) . . ?
O1 Ag1 Ag17 142.3(5) . . ?
Ag11 Ag1 Ag17 65.73(6) . . ?
Ag20 Ag1 Ag17 62.51(7) . . ?
O1 Ag1 Ag28 122.5(5) . . ?
Ag11 Ag1 Ag28 59.12(7) . . ?
Ag20 Ag1 Ag28 117.86(8) . . ?
Ag17 Ag1 Ag28 59.21(7) . . ?
O1 Ag1 Ag22 85.9(4) . . ?
Ag11 Ag1 Ag22 90.99(7) . . ?
Ag20 Ag1 Ag22 66.19(7) . . ?
Ag17 Ag1 Ag22 105.89(8) . . ?
Ag28 Ag1 Ag22 149.64(8) . . ?
O1 Ag1 Ag18 90.4(4) . . ?
Ag11 Ag1 Ag18 63.74(6) . . ?
Ag20 Ag1 Ag18 125.83(9) . . ?
Ag17 Ag1 Ag18 126.74(8) . . ?
Ag28 Ag1 Ag18 105.55(8) . . ?
Ag22 Ag1 Ag18 60.05(6) . . ?
O1 Ag1 Ag23 134.7(5) . . ?
Ag11 Ag1 Ag23 59.55(6) . . ?
Ag20 Ag1 Ag23 56.23(6) . . ?
Ag17 Ag1 Ag23 54.46(6) . . ?
Ag28 Ag1 Ag23 101.88(7) . . ?
Ag22 Ag1 Ag23 53.34(6) . . ?
Ag18 Ag1 Ag23 85.54(7) . . ?
O1 Ag1 Ag27 100.0(5) . . ?
Ag11 Ag1 Ag27 55.68(6) . . ?
Ag20 Ag1 Ag27 167.83(8) . . ?
Ag17 Ag1 Ag27 106.61(8) . . ?
Ag28 Ag1 Ag27 54.75(6) . . ?
Ag22 Ag1 Ag27 114.66(8) . . ?
Ag18 Ag1 Ag27 54.95(6) . . ?
Ag23 Ag1 Ag27 113.68(7) . . ?
O3 Ag2 Ag15 151.2(5) . . ?
O3 Ag2 Ag22 142.2(5) . . ?
Ag15 Ag2 Ag22 65.21(7) . . ?
O3 Ag2 Ag9 93.8(5) . . ?
Ag15 Ag2 Ag9 112.18(8) . . ?
Ag22 Ag2 Ag9 62.30(7) . . ?
O3 Ag2 Ag16 88.5(4) . . ?
Ag15 Ag2 Ag16 90.79(7) . . ?
Ag22 Ag2 Ag16 105.33(7) . . ?
Ag9 Ag2 Ag16 66.08(6) . . ?
O3 Ag2 Ag12 120.4(4) . . ?
Ag15 Ag2 Ag12 59.47(7) . . ?
Ag22 Ag2 Ag12 58.46(6) . . ?
Ag9 Ag2 Ag12 116.67(8) . . ?
Ag16 Ag2 Ag12 149.57(9) . . ?
O3 Ag2 Ag3 91.6(5) . . ?
Ag15 Ag2 Ag3 63.52(6) . . ?
Ag22 Ag2 Ag3 125.86(8) . . ?
Ag9 Ag2 Ag3 125.48(8) . . ?
Ag16 Ag2 Ag3 59.89(6) . . ?
Ag12 Ag2 Ag3 106.45(8) . . ?
O3 Ag2 Ag23 136.9(5) . . ?
Ag15 Ag2 Ag23 59.50(6) . . ?
Ag22 Ag2 Ag23 54.05(6) . . ?
Ag9 Ag2 Ag23 55.83(6) . . ?
Ag16 Ag2 Ag23 53.08(6) . . ?
Ag12 Ag2 Ag23 101.52(8) . . ?
Ag3 Ag2 Ag23 85.12(6) . . ?
O3 Ag2 Ag19 98.1(5) . . ?
Ag15 Ag2 Ag19 56.56(6) . . ?
Ag22 Ag2 Ag19 106.87(8) . . ?
Ag9 Ag2 Ag19 168.10(9) . . ?
Ag16 Ag2 Ag19 115.12(7) . . ?
Ag12 Ag2 Ag19 55.76(6) . . ?
Ag3 Ag2 Ag19 55.48(6) . . ?
Ag23 Ag2 Ag19 114.53(8) . . ?
O7 Ag3 Ag10 153.3(5) . . ?
O7 Ag3 Ag4 139.9(6) . . ?
Ag10 Ag3 Ag4 66.05(7) . . ?
O7 Ag3 Ag19 88.2(5) . . ?
Ag10 Ag3 Ag19 114.63(8) . . ?
Ag4 Ag3 Ag19 65.15(7) . . ?
O7 Ag3 Ag16 93.0(6) . . ?
Ag10 Ag3 Ag16 63.33(6) . . ?
Ag4 Ag3 Ag16 126.39(8) . . ?
Ag19 Ag3 Ag16 123.68(8) . . ?
O7 Ag3 Ag14 123.2(5) . . ?
Ag10 Ag3 Ag14 57.96(6) . . ?
Ag4 Ag3 Ag14 59.12(6) . . ?
Ag19 Ag3 Ag14 120.82(9) . . ?
Ag16 Ag3 Ag14 104.93(7) . . ?
O7 Ag3 Ag2 85.8(5) . . ?
Ag10 Ag3 Ag2 91.63(7) . . ?
Ag4 Ag3 Ag2 106.66(8) . . ?
Ag19 Ag3 Ag2 64.63(6) . . ?
Ag16 Ag3 Ag2 59.35(6) . . ?
Ag14 Ag3 Ag2 149.21(8) . . ?
O7 Ag3 Ag15 133.6(5) . . ?
Ag10 Ag3 Ag15 60.38(6) . . ?
Ag4 Ag3 Ag15 55.04(6) . . ?
Ag19 Ag3 Ag15 56.71(6) . . ?
Ag16 Ag3 Ag15 84.76(7) . . ?
Ag14 Ag3 Ag15 101.88(7) . . ?
Ag2 Ag3 Ag15 53.47(6) . . ?
O7 Ag3 Ag24 100.8(5) . . ?
Ag10 Ag3 Ag24 56.17(6) . . ?
Ag4 Ag3 Ag24 107.83(8) . . ?
Ag19 Ag3 Ag24 170.78(9) . . ?
Ag16 Ag3 Ag24 54.69(6) . . ?
Ag14 Ag3 Ag24 55.31(6) . . ?
Ag2 Ag3 Ag24 113.90(7) . . ?
Ag15 Ag3 Ag24 114.65(7) . . ?
O14 Ag4 Ag15 151.7(4) . . ?
O14 Ag4 Ag3 141.7(4) . . ?
Ag15 Ag4 Ag3 66.04(7) . . ?
O14 Ag4 Ag14 90.6(4) . . ?
Ag15 Ag4 Ag14 113.47(8) . . ?
Ag3 Ag4 Ag14 63.35(7) . . ?
O14 Ag4 Ag5 89.6(4) . . ?
Ag15 Ag4 Ag5 64.65(6) . . ?
Ag3 Ag4 Ag5 128.09(8) . . ?
Ag14 Ag4 Ag5 125.77(8) . . ?
O14 Ag4 Ag6 84.6(5) . . ?
Ag15 Ag4 Ag6 92.00(7) . . ?
Ag3 Ag4 Ag6 106.58(8) . . ?
Ag14 Ag4 Ag6 65.43(6) . . ?
Ag5 Ag4 Ag6 60.63(6) . . ?
O14 Ag4 Ag10 133.3(5) . . ?
Ag15 Ag4 Ag10 60.36(6) . . ?
Ag3 Ag4 Ag10 54.96(6) . . ?
Ag14 Ag4 Ag10 56.07(6) . . ?
Ag5 Ag4 Ag10 86.67(7) . . ?
Ag6 Ag4 Ag10 53.59(6) . . ?
O14 Ag4 Ag19 124.9(5) . . ?
Ag15 Ag4 Ag19 57.57(6) . . ?
Ag3 Ag4 Ag19 57.94(6) . . ?
Ag14 Ag4 Ag19 118.03(8) . . ?
Ag5 Ag4 Ag19 105.53(7) . . ?
Ag6 Ag4 Ag19 148.93(8) . . ?
Ag10 Ag4 Ag19 100.76(7) . . ?
O14 Ag4 Ag26 101.3(4) . . ?
Ag15 Ag4 Ag26 55.21(6) . . ?
Ag3 Ag4 Ag26 105.88(8) . . ?
Ag14 Ag4 Ag26 168.05(9) . . ?
Ag5 Ag4 Ag26 55.62(6) . . ?
Ag6 Ag4 Ag26 115.80(8) . . ?
Ag10 Ag4 Ag26 114.17(7) . . ?
Ag19 Ag4 Ag26 54.20(6) . . ?
O15 Ag5 Ag11 150.4(5) . . ?
O15 Ag5 Ag18 142.3(4) . . ?
Ag11 Ag5 Ag18 65.80(7) . . ?
O15 Ag5 Ag26 94.3(5) . . ?
Ag11 Ag5 Ag26 112.44(9) . . ?
Ag18 Ag5 Ag26 62.44(7) . . ?
O15 Ag5 Ag27 120.5(4) . . ?
Ag11 Ag5 Ag27 58.61(6) . . ?
Ag18 Ag5 Ag27 58.77(7) . . ?
Ag26 Ag5 Ag27 117.68(8) . . ?
O15 Ag5 Ag4 88.0(4) . . ?
Ag11 Ag5 Ag4 91.29(7) . . ?
Ag18 Ag5 Ag4 106.25(8) . . ?
Ag26 Ag5 Ag4 66.04(6) . . ?
Ag27 Ag5 Ag4 149.41(9) . . ?
O15 Ag5 Ag6 91.1(4) . . ?
Ag11 Ag5 Ag6 63.42(6) . . ?
Ag18 Ag5 Ag6 126.36(8) . . ?
Ag26 Ag5 Ag6 125.21(8) . . ?
Ag27 Ag5 Ag6 105.48(7) . . ?
Ag4 Ag5 Ag6 59.72(6) . . ?
O15 Ag5 Ag15 136.9(5) . . ?
Ag11 Ag5 Ag15 60.02(6) . . ?
Ag18 Ag5 Ag15 54.74(6) . . ?
Ag26 Ag5 Ag15 55.56(6) . . ?
Ag27 Ag5 Ag15 101.72(8) . . ?
Ag4 Ag5 Ag15 53.36(6) . . ?
Ag6 Ag5 Ag15 85.10(7) . . ?
O15 Ag5 Ag25 97.7(5) . . ?
Ag11 Ag5 Ag25 56.02(6) . . ?
Ag18 Ag5 Ag25 107.01(8) . . ?
Ag26 Ag5 Ag25 168.02(9) . . ?
Ag27 Ag5 Ag25 55.14(6) . . ?
Ag4 Ag5 Ag25 114.60(7) . . ?
Ag6 Ag5 Ag25 55.10(6) . . ?
Ag15 Ag5 Ag25 114.39(7) . . ?
O16 Ag6 Ag10 154.0(5) . . ?
O16 Ag6 Ag8 138.2(5) . . ?
Ag10 Ag6 Ag8 66.82(7) . . ?
O16 Ag6 Ag25 88.2(5) . . ?
Ag10 Ag6 Ag25 114.78(8) . . ?
Ag8 Ag6 Ag25 63.58(7) . . ?
O16 Ag6 Ag4 93.5(5) . . ?
Ag10 Ag6 Ag4 63.89(6) . . ?
Ag8 Ag6 Ag4 127.50(9) . . ?
Ag25 Ag6 Ag4 124.82(8) . . ?
O16 Ag6 Ag5 86.7(4) . . ?
Ag10 Ag6 Ag5 92.02(7) . . ?
Ag8 Ag6 Ag5 106.23(8) . . ?
Ag25 Ag6 Ag5 65.43(7) . . ?
Ag4 Ag6 Ag5 59.66(6) . . ?
O16 Ag6 Ag11 133.9(5) . . ?
Ag10 Ag6 Ag11 60.89(6) . . ?
Ag8 Ag6 Ag11 54.78(6) . . ?
Ag25 Ag6 Ag11 56.69(6) . . ?
Ag4 Ag6 Ag11 85.54(7) . . ?
Ag5 Ag6 Ag11 53.47(6) . . ?
O16 Ag6 Ag7 123.0(5) . . ?
Ag10 Ag6 Ag7 57.73(6) . . ?
Ag8 Ag6 Ag7 58.82(6) . . ?
Ag25 Ag6 Ag7 118.88(8) . . ?
Ag4 Ag6 Ag7 105.82(8) . . ?
Ag5 Ag6 Ag7 149.13(9) . . ?
Ag11 Ag6 Ag7 101.27(7) . . ?
O16 Ag6 Ag14 101.7(5) . . ?
Ag10 Ag6 Ag14 55.70(6) . . ?
Ag8 Ag6 Ag14 107.68(8) . . ?
Ag25 Ag6 Ag14 170.09(9) . . ?
Ag4 Ag6 Ag14 55.72(6) . . ?
Ag5 Ag6 Ag14 115.15(8) . . ?
Ag11 Ag6 Ag14 114.99(8) . . ?
Ag7 Ag6 Ag14 55.06(6) . . ?
P10 Ag7 Ag10 167.21(19) . . ?
P10 Ag7 Ag24 131.90(19) . . ?
Ag10 Ag7 Ag24 60.14(6) . . ?
P10 Ag7 Ag14 128.09(18) . . ?
Ag10 Ag7 Ag14 58.85(6) . . ?
Ag24 Ag7 Ag14 60.71(7) . . ?
P10 Ag7 Ag8 102.73(18) . . ?
Ag10 Ag7 Ag8 65.13(6) . . ?
Ag24 Ag7 Ag8 114.61(8) . . ?
Ag14 Ag7 Ag8 114.98(8) . . ?
P10 Ag7 Ag6 115.4(2) . . ?
Ag10 Ag7 Ag6 55.37(6) . . ?
Ag24 Ag7 Ag6 110.08(7) . . ?
Ag14 Ag7 Ag6 65.05(7) . . ?
Ag8 Ag7 Ag6 57.11(6) . . ?
P10 Ag7 Ag13 124.43(19) . . ?
Ag10 Ag7 Ag13 54.30(6) . . ?
Ag24 Ag7 Ag13 60.18(6) . . ?
Ag14 Ag7 Ag13 105.40(7) . . ?
Ag8 Ag7 Ag13 59.99(6) . . ?
Ag6 Ag7 Ag13 98.45(7) . . ?
O10 Ag8 Ag11 152.6(4) . . ?
O10 Ag8 Ag6 139.9(5) . . ?
Ag11 Ag8 Ag6 66.28(6) . . ?
O10 Ag8 Ag7 90.4(4) . . ?
Ag11 Ag8 Ag7 113.95(8) . . ?
Ag6 Ag8 Ag7 64.07(7) . . ?
O10 Ag8 Ag17 91.6(5) . . ?
Ag11 Ag8 Ag17 64.80(6) . . ?
Ag6 Ag8 Ag17 128.15(8) . . ?
Ag7 Ag8 Ag17 124.27(9) . . ?
O10 Ag8 Ag13 87.5(5) . . ?
Ag11 Ag8 Ag13 92.15(7) . . ?
Ag6 Ag8 Ag13 105.70(8) . . ?
Ag7 Ag8 Ag13 63.73(7) . . ?
Ag17 Ag8 Ag13 60.74(6) . . ?
O10 Ag8 Ag25 121.3(5) . . ?
Ag11 Ag8 Ag25 58.58(6) . . ?
Ag6 Ag8 Ag25 58.89(7) . . ?
Ag7 Ag8 Ag25 119.41(9) . . ?
Ag17 Ag8 Ag25 106.44(8) . . ?
Ag13 Ag8 Ag25 150.01(8) . . ?
O10 Ag8 Ag10 135.3(4) . . ?
Ag11 Ag8 Ag10 60.63(6) . . ?
Ag6 Ag8 Ag10 54.73(6) . . ?
Ag7 Ag8 Ag10 55.89(6) . . ?
Ag17 Ag8 Ag10 86.44(7) . . ?
Ag13 Ag8 Ag10 53.06(6) . . ?
Ag25 Ag8 Ag10 101.91(7) . . ?
O10 Ag8 Ag28 100.2(4) . . ?
Ag11 Ag8 Ag28 55.54(6) . . ?
Ag6 Ag8 Ag28 107.28(8) . . ?
Ag7 Ag8 Ag28 169.37(8) . . ?
Ag17 Ag8 Ag28 55.14(6) . . ?
Ag13 Ag8 Ag28 115.48(8) . . ?
Ag25 Ag8 Ag28 55.38(7) . . ?
Ag10 Ag8 Ag28 114.50(7) . . ?
P3 Ag9 Ag23 169.51(19) . . ?
P3 Ag9 Ag21 129.70(19) . . ?
Ag23 Ag9 Ag21 59.16(6) . . ?
P3 Ag9 Ag20 128.6(2) . . ?
Ag23 Ag9 Ag20 59.03(7) . . ?
Ag21 Ag9 Ag20 59.94(7) . . ?
P3 Ag9 Ag2 103.75(18) . . ?
Ag23 Ag9 Ag2 65.86(7) . . ?
Ag21 Ag9 Ag2 113.45(8) . . ?
Ag20 Ag9 Ag2 116.93(9) . . ?
P3 Ag9 Ag22 118.15(19) . . ?
Ag23 Ag9 Ag22 55.99(6) . . ?
Ag21 Ag9 Ag22 109.87(8) . . ?
Ag20 Ag9 Ag22 66.10(7) . . ?
Ag2 Ag9 Ag22 58.75(6) . . ?
P3 Ag9 Ag16 123.6(2) . . ?
Ag23 Ag9 Ag16 53.31(6) . . ?
Ag21 Ag9 Ag16 59.64(6) . . ?
Ag20 Ag9 Ag16 104.58(8) . . ?
Ag2 Ag9 Ag16 58.50(6) . . ?
Ag22 Ag9 Ag16 97.86(7) . . ?
Ag13 Ag10 Ag3 120.15(9) . . ?
Ag13 Ag10 Ag6 118.28(8) . . ?
Ag3 Ag10 Ag6 119.01(8) . . ?
Ag13 Ag10 Ag14 120.36(8) . . ?
Ag3 Ag10 Ag14 66.35(7) . . ?
Ag6 Ag10 Ag14 70.66(7) . . ?
Ag13 Ag10 Ag7 68.94(7) . . ?
Ag3 Ag10 Ag7 121.33(8) . . ?
Ag6 Ag10 Ag7 66.90(7) . . ?
Ag14 Ag10 Ag7 62.12(6) . . ?
Ag13 Ag10 Ag24 65.62(7) . . ?
Ag3 Ag10 Ag24 71.23(7) . . ?
Ag6 Ag10 Ag24 121.36(8) . . ?
Ag14 Ag10 Ag24 62.21(7) . . ?
Ag7 Ag10 Ag24 61.36(6) . . ?
Ag13 Ag10 Ag23 65.29(6) . . ?
Ag3 Ag10 Ag23 94.96(7) . . ?
Ag6 Ag10 Ag23 124.45(8) . . ?
Ag14 Ag10 Ag23 161.05(8) . . ?
Ag7 Ag10 Ag23 131.71(8) . . ?
Ag24 Ag10 Ag23 110.20(8) . . ?
Ag13 Ag10 Ag15 125.38(8) . . ?
Ag3 Ag10 Ag15 65.24(6) . . ?
Ag6 Ag10 Ag15 94.09(7) . . ?
Ag14 Ag10 Ag15 111.12(7) . . ?
Ag7 Ag10 Ag15 160.91(9) . . ?
Ag24 Ag10 Ag15 133.58(8) . . ?
Ag23 Ag10 Ag15 60.10(6) . . ?
Ag13 Ag10 Ag11 93.87(7) . . ?
Ag3 Ag10 Ag11 125.08(7) . . ?
Ag6 Ag10 Ag11 64.86(6) . . ?
Ag14 Ag10 Ag11 133.15(8) . . ?
Ag7 Ag10 Ag11 110.28(7) . . ?
Ag24 Ag10 Ag11 159.33(8) . . ?
Ag23 Ag10 Ag11 59.63(6) . . ?
Ag15 Ag10 Ag11 59.88(5) . . ?
Ag13 Ag10 Ag16 59.92(6) . . ?
Ag3 Ag10 Ag16 62.85(6) . . ?
Ag6 Ag10 Ag16 178.14(9) . . ?
Ag14 Ag10 Ag16 110.52(8) . . ?
Ag7 Ag10 Ag16 112.23(8) . . ?
Ag24 Ag10 Ag16 58.72(6) . . ?
Ag23 Ag10 Ag16 54.73(6) . . ?
Ag15 Ag10 Ag16 86.82(7) . . ?
Ag11 Ag10 Ag16 114.35(7) . . ?
Ag13 Ag10 Ag4 179.14(10) . . ?
Ag3 Ag10 Ag4 58.99(6) . . ?
Ag6 Ag10 Ag4 62.52(6) . . ?
Ag14 Ag10 Ag4 59.43(6) . . ?
Ag7 Ag10 Ag4 111.39(8) . . ?
Ag24 Ag10 Ag4 113.77(8) . . ?
Ag23 Ag10 Ag4 114.61(7) . . ?
Ag15 Ag10 Ag4 54.51(5) . . ?
Ag11 Ag10 Ag4 86.76(6) . . ?
Ag16 Ag10 Ag4 119.28(7) . . ?
Ag13 Ag10 Ag8 62.50(6) . . ?
Ag3 Ag10 Ag8 177.34(9) . . ?
Ag6 Ag10 Ag8 58.45(6) . . ?
Ag14 Ag10 Ag8 112.54(7) . . ?
Ag7 Ag10 Ag8 58.98(6) . . ?
Ag24 Ag10 Ag8 110.57(7) . . ?
Ag23 Ag10 Ag8 86.27(6) . . ?
Ag15 Ag10 Ag8 113.56(7) . . ?
Ag11 Ag10 Ag8 53.68(5) . . ?
Ag16 Ag10 Ag8 119.69(7) . . ?
Ag4 Ag10 Ag8 118.36(8) . . ?
Ag8 Ag11 Ag5 119.44(8) . . ?
Ag8 Ag11 Ag1 118.84(8) . . ?
Ag5 Ag11 Ag1 118.98(8) . . ?
Ag8 Ag11 Ag27 120.76(8) . . ?
Ag5 Ag11 Ag27 65.41(7) . . ?
Ag1 Ag11 Ag27 70.85(7) . . ?
Ag8 Ag11 Ag25 66.16(7) . . ?
Ag5 Ag11 Ag25 70.46(7) . . ?
Ag1 Ag11 Ag25 120.61(9) . . ?
Ag27 Ag11 Ag25 61.40(7) . . ?
Ag8 Ag11 Ag28 72.00(7) . . ?
Ag5 Ag11 Ag28 120.24(9) . . ?
Ag1 Ag11 Ag28 64.51(7) . . ?
Ag27 Ag11 Ag28 60.83(7) . . ?
Ag25 Ag11 Ag28 62.44(7) . . ?
Ag8 Ag11 Ag23 93.19(7) . . ?
Ag5 Ag11 Ag23 125.80(8) . . ?
Ag1 Ag11 Ag23 65.93(7) . . ?
Ag27 Ag11 Ag23 134.34(8) . . ?
Ag25 Ag11 Ag23 159.17(8) . . ?
Ag28 Ag11 Ag23 110.10(8) . . ?
Ag8 Ag11 Ag15 125.39(8) . . ?
Ag5 Ag11 Ag15 65.81(6) . . ?
Ag1 Ag11 Ag15 93.88(7) . . ?
Ag27 Ag11 Ag15 110.45(7) . . ?
Ag25 Ag11 Ag15 133.74(8) . . ?
Ag28 Ag11 Ag15 158.11(8) . . ?
Ag23 Ag11 Ag15 59.99(6) . . ?
Ag8 Ag11 Ag10 65.69(6) . . ?
Ag5 Ag11 Ag10 94.05(7) . . ?
Ag1 Ag11 Ag10 125.41(8) . . ?
Ag27 Ag11 Ag10 159.26(9) . . ?
Ag25 Ag11 Ag10 110.58(8) . . ?
Ag28 Ag11 Ag10 135.05(8) . . ?
Ag23 Ag11 Ag10 59.48(6) . . ?
Ag15 Ag11 Ag10 59.70(5) . . ?
Ag8 Ag11 Ag18 178.59(9) . . ?
Ag5 Ag11 Ag18 59.17(6) . . ?
Ag1 Ag11 Ag18 62.41(6) . . ?
Ag27 Ag11 Ag18 58.73(6) . . ?
Ag25 Ag11 Ag18 112.74(8) . . ?
Ag28 Ag11 Ag18 108.38(7) . . ?
Ag23 Ag11 Ag18 87.95(7) . . ?
Ag15 Ag11 Ag18 54.60(5) . . ?
Ag10 Ag11 Ag18 114.29(7) . . ?
Ag8 Ag11 Ag6 58.94(6) . . ?
Ag5 Ag11 Ag6 63.12(6) . . ?
Ag1 Ag11 Ag6 177.78(8) . . ?
Ag27 Ag11 Ag6 110.06(8) . . ?
Ag25 Ag11 Ag6 58.91(7) . . ?
Ag28 Ag11 Ag6 114.00(8) . . ?
Ag23 Ag11 Ag6 113.70(7) . . ?
Ag15 Ag11 Ag6 87.70(7) . . ?
Ag10 Ag11 Ag6 54.24(6) . . ?
Ag18 Ag11 Ag6 119.81(7) . . ?
Ag8 Ag11 Ag17 61.77(6) . . ?
Ag5 Ag11 Ag17 178.41(8) . . ?
Ag1 Ag11 Ag17 59.54(6) . . ?
Ag27 Ag11 Ag17 113.17(8) . . ?
Ag25 Ag11 Ag17 109.63(8) . . ?
Ag28 Ag11 Ag17 58.84(7) . . ?
Ag23 Ag11 Ag17 54.53(6) . . ?
Ag15 Ag11 Ag17 114.51(8) . . ?
Ag10 Ag11 Ag17 87.41(7) . . ?
Ag18 Ag11 Ag17 119.62(7) . . ?
Ag6 Ag11 Ag17 118.35(7) . . ?
P12 Ag12 Ag15 166.91(19) . . ?
P12 Ag12 Ag22 103.22(19) . . ?
Ag15 Ag12 Ag22 63.85(6) . . ?
P12 Ag12 Ag19 133.05(19) . . ?
Ag15 Ag12 Ag19 58.88(6) . . ?
Ag22 Ag12 Ag19 115.07(8) . . ?
P12 Ag12 Ag26 129.9(2) . . ?
Ag15 Ag12 Ag26 58.13(6) . . ?
Ag22 Ag12 Ag26 110.88(8) . . ?
Ag19 Ag12 Ag26 59.69(7) . . ?
P12 Ag12 Ag2 120.7(2) . . ?
Ag15 Ag12 Ag2 55.63(6) . . ?
Ag22 Ag12 Ag2 58.70(6) . . ?
Ag19 Ag12 Ag2 65.05(7) . . ?
Ag26 Ag12 Ag2 108.30(8) . . ?
P12 Ag12 Ag18 119.8(2) . . ?
Ag15 Ag12 Ag18 52.82(6) . . ?
Ag22 Ag12 Ag18 58.34(6) . . ?
Ag19 Ag12 Ag18 103.53(8) . . ?
Ag26 Ag12 Ag18 57.97(7) . . ?
Ag2 Ag12 Ag18 98.21(7) . . ?
O8 Ag13 Ag10 149.9(5) . . ?
O8 Ag13 Ag16 143.1(5) . . ?
Ag10 Ag13 Ag16 65.17(6) . . ?
O8 Ag13 Ag21 93.8(5) . . ?
Ag10 Ag13 Ag21 113.63(8) . . ?
Ag16 Ag13 Ag21 63.73(7) . . ?
O8 Ag13 Ag8 90.2(5) . . ?
Ag10 Ag13 Ag8 64.43(6) . . ?
Ag16 Ag13 Ag8 126.44(8) . . ?
Ag21 Ag13 Ag8 124.58(8) . . ?
O8 Ag13 Ag24 119.5(4) . . ?
Ag10 Ag13 Ag24 59.26(6) . . ?
Ag16 Ag13 Ag24 58.42(6) . . ?
Ag21 Ag13 Ag24 117.78(9) . . ?
Ag8 Ag13 Ag24 107.42(8) . . ?
O8 Ag13 Ag17 87.9(4) . . ?
Ag10 Ag13 Ag17 91.97(7) . . ?
Ag16 Ag13 Ag17 106.47(7) . . ?
Ag21 Ag13 Ag17 65.97(7) . . ?
Ag8 Ag13 Ag17 58.96(6) . . ?
Ag24 Ag13 Ag17 150.65(8) . . ?
O8 Ag13 Ag23 137.4(4) . . ?
Ag10 Ag13 Ag23 60.13(6) . . ?
Ag16 Ag13 Ag23 54.72(6) . . ?
Ag21 Ag13 Ag23 56.65(6) . . ?
Ag8 Ag13 Ag23 84.79(7) . . ?
Ag24 Ag13 Ag23 102.23(7) . . ?
Ag17 Ag13 Ag23 53.57(6) . . ?
O8 Ag13 Ag7 96.3(5) . . ?
Ag10 Ag13 Ag7 56.76(6) . . ?
Ag16 Ag13 Ag7 107.14(8) . . ?
Ag21 Ag13 Ag7 169.91(8) . . ?
Ag8 Ag13 Ag7 56.29(6) . . ?
Ag24 Ag13 Ag7 55.94(6) . . ?
Ag17 Ag13 Ag7 115.09(8) . . ?
Ag23 Ag13 Ag7 115.14(7) . . ?
P11 Ag14 Ag10 167.12(19) . . ?
P11 Ag14 Ag7 128.95(17) . . ?
Ag10 Ag14 Ag7 59.02(6) . . ?
P11 Ag14 Ag4 102.82(18) . . ?
Ag10 Ag14 Ag4 64.50(6) . . ?
Ag7 Ag14 Ag4 113.01(8) . . ?
P11 Ag14 Ag24 132.0(2) . . ?
Ag10 Ag14 Ag24 59.79(6) . . ?
Ag7 Ag14 Ag24 59.57(7) . . ?
Ag4 Ag14 Ag24 116.04(8) . . ?
P11 Ag14 Ag3 120.64(18) . . ?
Ag10 Ag14 Ag3 55.69(6) . . ?
Ag7 Ag14 Ag3 109.20(8) . . ?
Ag4 Ag14 Ag3 57.53(6) . . ?
Ag24 Ag14 Ag3 66.28(6) . . ?
P11 Ag14 Ag6 118.9(2) . . ?
Ag10 Ag14 Ag6 53.64(6) . . ?
Ag7 Ag14 Ag6 59.89(6) . . ?
Ag4 Ag14 Ag6 58.85(6) . . ?
Ag24 Ag14 Ag6 105.33(7) . . ?
Ag3 Ag14 Ag6 98.13(7) . . ?
Ag4 Ag15 Ag2 119.55(8) . . ?
Ag4 Ag15 Ag18 118.36(9) . . ?
Ag2 Ag15 Ag18 119.49(8) . . ?
Ag4 Ag15 Ag26 71.44(7) . . ?
Ag2 Ag15 Ag26 119.75(8) . . ?
Ag18 Ag15 Ag26 65.55(7) . . ?
Ag4 Ag15 Ag19 67.64(7) . . ?
Ag2 Ag15 Ag19 69.48(7) . . ?
Ag18 Ag15 Ag19 120.45(8) . . ?
Ag26 Ag15 Ag19 61.71(7) . . ?
Ag4 Ag15 Ag12 122.04(8) . . ?
Ag2 Ag15 Ag12 64.90(7) . . ?
Ag18 Ag15 Ag12 71.03(7) . . ?
Ag26 Ag15 Ag12 61.79(7) . . ?
Ag19 Ag15 Ag12 61.17(6) . . ?
Ag4 Ag15 Ag23 124.74(7) . . ?
Ag2 Ag15 Ag23 66.45(6) . . ?
Ag18 Ag15 Ag23 93.87(7) . . ?
Ag26 Ag15 Ag23 159.18(8) . . ?
Ag19 Ag15 Ag23 133.60(9) . . ?
Ag12 Ag15 Ag23 110.01(8) . . ?
Ag4 Ag15 Ag10 65.13(6) . . ?
Ag2 Ag15 Ag10 94.04(7) . . ?
Ag18 Ag15 Ag10 125.37(8) . . ?
Ag26 Ag15 Ag10 134.40(8) . . ?
Ag19 Ag15 Ag10 110.91(7) . . ?
Ag12 Ag15 Ag10 158.81(9) . . ?
Ag23 Ag15 Ag10 59.61(6) . . ?
Ag4 Ag15 Ag11 93.18(7) . . ?
Ag2 Ag15 Ag11 126.08(8) . . ?
Ag18 Ag15 Ag11 64.97(6) . . ?
Ag26 Ag15 Ag11 110.45(8) . . ?
Ag19 Ag15 Ag11 160.58(9) . . ?
Ag12 Ag15 Ag11 133.20(8) . . ?
Ag23 Ag15 Ag11 59.65(6) . . ?
Ag10 Ag15 Ag11 60.42(5) . . ?
Ag4 Ag15 Ag22 179.06(9) . . ?
Ag2 Ag15 Ag22 59.73(6) . . ?
Ag18 Ag15 Ag22 62.51(6) . . ?
Ag26 Ag15 Ag22 109.42(7) . . ?
Ag19 Ag15 Ag22 112.33(7) . . ?
Ag12 Ag15 Ag22 58.40(6) . . ?
Ag23 Ag15 Ag22 54.53(5) . . ?
Ag10 Ag15 Ag22 114.14(7) . . ?
Ag11 Ag15 Ag22 86.89(6) . . ?
Ag4 Ag15 Ag3 58.92(6) . . ?
Ag2 Ag15 Ag3 63.01(6) . . ?
Ag18 Ag15 Ag3 177.27(9) . . ?
Ag26 Ag15 Ag3 112.48(7) . . ?
Ag19 Ag15 Ag3 58.82(6) . . ?
Ag12 Ag15 Ag3 109.94(8) . . ?
Ag23 Ag15 Ag3 88.19(6) . . ?
Ag10 Ag15 Ag3 54.38(5) . . ?
Ag11 Ag15 Ag3 114.77(7) . . ?
Ag22 Ag15 Ag3 120.21(8) . . ?
Ag4 Ag15 Ag5 62.00(6) . . ?
Ag2 Ag15 Ag5 178.09(8) . . ?
Ag18 Ag15 Ag5 58.69(6) . . ?
Ag26 Ag15 Ag5 59.29(6) . . ?
Ag19 Ag15 Ag5 110.72(8) . . ?
Ag12 Ag15 Ag5 113.44(8) . . ?
Ag23 Ag15 Ag5 113.81(7) . . ?
Ag10 Ag15 Ag5 87.66(6) . . ?
Ag11 Ag15 Ag5 54.17(6) . . ?
Ag22 Ag15 Ag5 118.73(7) . . ?
Ag3 Ag15 Ag5 118.79(7) . . ?
O5 Ag16 Ag23 152.5(5) . . ?
O5 Ag16 Ag13 140.8(5) . . ?
Ag23 Ag16 Ag13 65.55(7) . . ?
O5 Ag16 Ag24 90.3(5) . . ?
Ag23 Ag16 Ag24 114.54(8) . . ?
Ag13 Ag16 Ag24 63.28(7) . . ?
O5 Ag16 Ag2 90.4(4) . . ?
Ag23 Ag16 Ag2 65.48(6) . . ?
Ag13 Ag16 Ag2 128.41(9) . . ?
Ag24 Ag16 Ag2 127.55(9) . . ?
O5 Ag16 Ag3 86.2(5) . . ?
Ag23 Ag16 Ag3 92.62(7) . . ?
Ag13 Ag16 Ag3 106.72(8) . . ?
Ag24 Ag16 Ag3 66.96(7) . . ?
Ag2 Ag16 Ag3 60.77(6) . . ?
O5 Ag16 Ag10 135.0(5) . . ?
Ag23 Ag16 Ag10 60.34(6) . . ?
Ag13 Ag16 Ag10 54.91(6) . . ?
Ag24 Ag16 Ag10 57.74(6) . . ?
Ag2 Ag16 Ag10 86.99(7) . . ?
Ag3 Ag16 Ag10 53.82(6) . . ?
O5 Ag16 Ag21 122.3(5) . . ?
Ag23 Ag16 Ag21 58.06(6) . . ?
Ag13 Ag16 Ag21 58.16(6) . . ?
Ag24 Ag16 Ag21 117.13(8) . . ?
Ag2 Ag16 Ag21 106.24(7) . . ?
Ag3 Ag16 Ag21 150.07(9) . . ?
Ag10 Ag16 Ag21 101.41(8) . . ?
O5 Ag16 Ag9 100.2(5) . . ?
Ag23 Ag16 Ag9 55.84(6) . . ?
Ag13 Ag16 Ag9 106.41(8) . . ?
Ag24 Ag16 Ag9 169.25(9) . . ?
Ag2 Ag16 Ag9 55.43(6) . . ?
Ag3 Ag16 Ag9 115.79(7) . . ?
Ag10 Ag16 Ag9 114.58(8) . . ?
Ag21 Ag16 Ag9 54.89(6) . . ?
O2 Ag17 Ag23 147.7(5) . . ?
O2 Ag17 Ag1 144.3(5) . . ?
Ag23 Ag17 Ag1 66.10(6) . . ?
O2 Ag17 Ag28 96.8(5) . . ?
Ag23 Ag17 Ag28 112.84(8) . . ?
Ag1 Ag17 Ag28 61.73(7) . . ?
O2 Ag17 Ag8 88.6(4) . . ?
Ag23 Ag17 Ag8 91.10(7) . . ?
Ag1 Ag17 Ag8 106.22(8) . . ?
Ag28 Ag17 Ag8 67.31(7) . . ?
O2 Ag17 Ag20 120.0(5) . . ?
Ag23 Ag17 Ag20 58.48(6) . . ?
Ag1 Ag17 Ag20 58.30(7) . . ?
Ag28 Ag17 Ag20 116.29(8) . . ?
Ag8 Ag17 Ag20 148.98(8) . . ?
O2 Ag17 Ag13 89.0(5) . . ?
Ag23 Ag17 Ag13 63.23(6) . . ?
Ag1 Ag17 Ag13 126.70(8) . . ?
Ag28 Ag17 Ag13 127.10(9) . . ?
Ag8 Ag17 Ag13 60.30(6) . . ?
Ag20 Ag17 Ag13 105.20(8) . . ?
O2 Ag17 Ag11 138.6(5) . . ?
Ag23 Ag17 Ag11 59.77(6) . . ?
Ag1 Ag17 Ag11 54.73(6) . . ?
Ag28 Ag17 Ag11 56.52(6) . . ?
Ag8 Ag17 Ag11 53.43(6) . . ?
Ag20 Ag17 Ag11 101.00(7) . . ?
Ag13 Ag17 Ag11 85.52(7) . . ?
O2 Ag17 Ag21 95.6(5) . . ?
Ag23 Ag17 Ag21 55.56(6) . . ?
Ag1 Ag17 Ag21 106.62(8) . . ?
Ag28 Ag17 Ag21 167.48(8) . . ?
Ag8 Ag17 Ag21 114.73(8) . . ?
Ag20 Ag17 Ag21 55.09(6) . . ?
Ag13 Ag17 Ag21 54.72(6) . . ?
Ag11 Ag17 Ag21 113.82(7) . . ?
O13 Ag18 Ag15 151.7(5) . . ?
O13 Ag18 Ag5 140.3(6) . . ?
Ag15 Ag18 Ag5 66.57(7) . . ?
O13 Ag18 Ag27 91.5(5) . . ?
Ag15 Ag18 Ag27 114.04(8) . . ?
Ag5 Ag18 Ag27 62.95(7) . . ?
O13 Ag18 Ag26 120.8(4) . . ?
Ag15 Ag18 Ag26 58.16(6) . . ?
Ag5 Ag18 Ag26 59.60(6) . . ?
Ag27 Ag18 Ag26 118.93(9) . . ?
O13 Ag18 Ag22 92.3(6) . . ?
Ag15 Ag18 Ag22 63.49(6) . . ?
Ag5 Ag18 Ag22 127.10(8) . . ?
Ag27 Ag18 Ag22 125.60(8) . . ?
Ag26 Ag18 Ag22 104.91(8) . . ?
O13 Ag18 Ag1 87.3(5) . . ?
Ag15 Ag18 Ag1 92.04(7) . . ?
Ag5 Ag18 Ag1 106.84(7) . . ?
Ag27 Ag18 Ag1 66.30(7) . . ?
Ag26 Ag18 Ag1 149.85(8) . . ?
Ag22 Ag18 Ag1 59.73(6) . . ?
O13 Ag18 Ag11 136.0(4) . . ?
Ag15 Ag18 Ag11 60.43(6) . . ?
Ag5 Ag18 Ag11 55.04(6) . . ?
Ag27 Ag18 Ag11 56.70(6) . . ?
Ag26 Ag18 Ag11 102.10(7) . . ?
Ag22 Ag18 Ag11 85.21(7) . . ?
Ag1 Ag18 Ag11 53.85(6) . . ?
O13 Ag18 Ag12 98.6(5) . . ?
Ag15 Ag18 Ag12 56.15(6) . . ?
Ag5 Ag18 Ag12 108.24(8) . . ?
Ag27 Ag18 Ag12 169.88(8) . . ?
Ag26 Ag18 Ag12 55.18(6) . . ?
Ag22 Ag18 Ag12 54.56(6) . . ?
Ag1 Ag18 Ag12 114.15(8) . . ?
Ag11 Ag18 Ag12 114.72(7) . . ?
P9 Ag19 Ag15 166.54(17) . . ?
P9 Ag19 Ag26 129.7(2) . . ?
Ag15 Ag19 Ag26 58.70(6) . . ?
P9 Ag19 Ag12 132.17(18) . . ?
Ag15 Ag19 Ag12 59.96(6) . . ?
Ag26 Ag19 Ag12 60.39(7) . . ?
P9 Ag19 Ag3 102.45(17) . . ?
Ag15 Ag19 Ag3 64.47(6) . . ?
Ag26 Ag19 Ag3 114.75(8) . . ?
Ag12 Ag19 Ag3 113.56(8) . . ?
P9 Ag19 Ag4 116.33(18) . . ?
Ag15 Ag19 Ag4 54.79(6) . . ?
Ag26 Ag19 Ag4 65.30(7) . . ?
Ag12 Ag19 Ag4 109.55(8) . . ?
Ag3 Ag19 Ag4 56.90(6) . . ?
P9 Ag19 Ag2 123.6(2) . . ?
Ag15 Ag19 Ag2 53.96(6) . . ?
Ag26 Ag19 Ag2 104.44(7) . . ?
Ag12 Ag19 Ag2 59.18(6) . . ?
Ag3 Ag19 Ag2 59.90(6) . . ?
Ag4 Ag19 Ag2 97.97(7) . . ?
P4 Ag20 Ag23 167.3(2) . . ?
P4 Ag20 Ag1 101.9(2) . . ?
Ag23 Ag20 Ag1 65.60(7) . . ?
P4 Ag20 Ag21 130.0(2) . . ?
Ag23 Ag20 Ag21 59.22(6) . . ?
Ag1 Ag20 Ag21 117.33(8) . . ?
P4 Ag20 Ag9 131.4(2) . . ?
Ag23 Ag20 Ag9 59.15(6) . . ?
Ag1 Ag20 Ag9 112.66(8) . . ?
Ag21 Ag20 Ag9 60.02(7) . . ?
P4 Ag20 Ag17 116.7(2) . . ?
Ag23 Ag20 Ag17 56.22(6) . . ?
Ag1 Ag20 Ag17 59.18(6) . . ?
Ag21 Ag20 Ag17 66.58(7) . . ?
Ag9 Ag20 Ag17 110.22(8) . . ?
P4 Ag20 Ag22 122.8(2) . . ?
Ag23 Ag20 Ag22 53.44(5) . . ?
Ag1 Ag20 Ag22 58.80(6) . . ?
Ag21 Ag20 Ag22 104.19(8) . . ?
Ag9 Ag20 Ag22 58.47(6) . . ?
Ag17 Ag20 Ag22 98.69(7) . . ?
P2 Ag21 Ag23 165.83(19) . . ?
P2 Ag21 Ag20 135.0(2) . . ?
Ag23 Ag21 Ag20 59.05(6) . . ?
P2 Ag21 Ag13 103.34(18) . . ?
Ag23 Ag21 Ag13 64.44(6) . . ?
Ag20 Ag21 Ag13 112.32(9) . . ?
P2 Ag21 Ag9 126.1(2) . . ?
Ag23 Ag21 Ag9 59.10(6) . . ?
Ag20 Ag21 Ag9 60.04(7) . . ?
Ag13 Ag21 Ag9 115.60(8) . . ?
P2 Ag21 Ag16 112.9(2) . . ?
Ag23 Ag21 Ag16 55.27(6) . . ?
Ag20 Ag21 Ag16 109.00(8) . . ?
Ag13 Ag21 Ag16 58.11(6) . . ?
Ag9 Ag21 Ag16 65.47(7) . . ?
P2 Ag21 Ag17 128.1(2) . . ?
Ag23 Ag21 Ag17 53.38(6) . . ?
Ag20 Ag21 Ag17 58.33(6) . . ?
Ag13 Ag21 Ag17 59.31(6) . . ?
Ag9 Ag21 Ag17 104.05(8) . . ?
Ag16 Ag21 Ag17 98.27(7) . . ?
O11 Ag22 Ag23 154.6(5) . . ?
O11 Ag22 Ag12 87.1(5) . . ?
Ag23 Ag22 Ag12 115.04(8) . . ?
O11 Ag22 Ag2 137.9(5) . . ?
Ag23 Ag22 Ag2 67.02(6) . . ?
Ag12 Ag22 Ag2 62.84(7) . . ?
O11 Ag22 Ag9 123.5(5) . . ?
Ag23 Ag22 Ag9 58.73(6) . . ?
Ag12 Ag22 Ag9 117.61(9) . . ?
Ag2 Ag22 Ag9 58.95(7) . . ?
O11 Ag22 Ag1 92.2(5) . . ?
Ag23 Ag22 Ag1 64.82(6) . . ?
Ag12 Ag22 Ag1 127.15(9) . . ?
Ag2 Ag22 Ag1 129.08(8) . . ?
Ag9 Ag22 Ag1 106.37(7) . . ?
O11 Ag22 Ag18 85.0(5) . . ?
Ag23 Ag22 Ag18 92.16(7) . . ?
Ag12 Ag22 Ag18 67.11(7) . . ?
Ag2 Ag22 Ag18 106.90(8) . . ?
Ag9 Ag22 Ag18 150.34(8) . . ?
Ag1 Ag22 Ag18 60.22(6) . . ?
O11 Ag22 Ag15 132.7(5) . . ?
Ag23 Ag22 Ag15 60.52(6) . . ?
Ag12 Ag22 Ag15 57.75(6) . . ?
Ag2 Ag22 Ag15 55.06(6) . . ?
Ag9 Ag22 Ag15 101.81(7) . . ?
Ag1 Ag22 Ag15 86.84(7) . . ?
Ag18 Ag22 Ag15 53.99(6) . . ?
O11 Ag22 Ag20 102.7(5) . . ?
Ag23 Ag22 Ag20 55.81(6) . . ?
Ag12 Ag22 Ag20 170.02(8) . . ?
Ag2 Ag22 Ag20 107.80(8) . . ?
Ag9 Ag22 Ag20 55.43(6) . . ?
Ag1 Ag22 Ag20 55.01(6) . . ?
Ag18 Ag22 Ag20 114.91(8) . . ?
Ag15 Ag22 Ag20 114.73(7) . . ?
Ag16 Ag23 Ag22 118.08(8) . . ?
Ag16 Ag23 Ag17 120.54(8) . . ?
Ag22 Ag23 Ag17 118.81(8) . . ?
Ag16 Ag23 Ag20 121.47(9) . . ?
Ag22 Ag23 Ag20 70.75(7) . . ?
Ag17 Ag23 Ag20 65.30(7) . . ?
Ag16 Ag23 Ag9 70.85(7) . . ?
Ag22 Ag23 Ag9 65.28(7) . . ?
Ag17 Ag23 Ag9 120.70(8) . . ?
Ag20 Ag23 Ag9 61.82(7) . . ?
Ag16 Ag23 Ag21 66.67(7) . . ?
Ag22 Ag23 Ag21 120.43(8) . . ?
Ag17 Ag23 Ag21 71.06(7) . . ?
Ag20 Ag23 Ag21 61.73(7) . . ?
Ag9 Ag23 Ag21 61.74(7) . . ?
Ag16 Ag23 Ag10 64.93(6) . . ?
Ag22 Ag23 Ag10 125.22(8) . . ?
Ag17 Ag23 Ag10 94.75(7) . . ?
Ag20 Ag23 Ag10 159.83(8) . . ?
Ag9 Ag23 Ag10 133.36(8) . . ?
Ag21 Ag23 Ag10 110.53(7) . . ?
Ag16 Ag23 Ag11 125.82(8) . . ?
Ag22 Ag23 Ag11 93.34(7) . . ?
Ag17 Ag23 Ag11 65.70(7) . . ?
Ag20 Ag23 Ag11 109.77(8) . . ?
Ag9 Ag23 Ag11 158.40(8) . . ?
Ag21 Ag23 Ag11 134.39(8) . . ?
Ag10 Ag23 Ag11 60.89(6) . . ?
Ag16 Ag23 Ag15 92.78(7) . . ?
Ag22 Ag23 Ag15 64.94(6) . . ?
Ag17 Ag23 Ag15 126.05(8) . . ?
Ag20 Ag23 Ag15 133.27(8) . . ?
Ag9 Ag23 Ag15 109.37(7) . . ?
Ag21 Ag23 Ag15 159.12(9) . . ?
Ag10 Ag23 Ag15 60.29(6) . . ?
Ag11 Ag23 Ag15 60.36(6) . . ?
Ag16 Ag23 Ag13 59.73(6) . . ?
Ag22 Ag23 Ag13 177.79(9) . . ?
Ag17 Ag23 Ag13 63.21(6) . . ?
Ag20 Ag23 Ag13 109.99(7) . . ?
Ag9 Ag23 Ag13 113.10(8) . . ?
Ag21 Ag23 Ag13 58.91(6) . . ?
Ag10 Ag23 Ag13 54.58(5) . . ?
Ag11 Ag23 Ag13 88.36(7) . . ?
Ag15 Ag23 Ag13 114.86(7) . . ?
Ag16 Ag23 Ag1 179.64(9) . . ?
Ag22 Ag23 Ag1 61.83(6) . . ?
Ag17 Ag23 Ag1 59.43(6) . . ?
Ag20 Ag23 Ag1 58.17(7) . . ?
Ag9 Ag23 Ag1 108.84(7) . . ?
Ag21 Ag23 Ag1 113.04(8) . . ?
Ag10 Ag23 Ag1 115.41(8) . . ?
Ag11 Ag23 Ag1 54.53(6) . . ?
Ag15 Ag23 Ag1 87.50(7) . . ?
Ag13 Ag23 Ag1 120.36(7) . . ?
Ag16 Ag23 Ag2 61.45(6) . . ?
Ag22 Ag23 Ag2 58.93(6) . . ?
Ag17 Ag23 Ag2 177.68(8) . . ?
Ag20 Ag23 Ag2 112.80(7) . . ?
Ag9 Ag23 Ag2 58.30(6) . . ?
Ag21 Ag23 Ag2 109.41(8) . . ?
Ag10 Ag23 Ag2 87.21(6) . . ?
Ag11 Ag23 Ag2 114.39(7) . . ?
Ag15 Ag23 Ag2 54.05(6) . . ?
Ag13 Ag23 Ag2 119.04(7) . . ?
Ag1 Ag23 Ag2 118.57(7) . . ?
P1 Ag24 Ag10 168.12(19) . . ?
P1 Ag24 Ag16 105.40(19) . . ?
Ag10 Ag24 Ag16 63.54(6) . . ?
P1 Ag24 Ag7 133.14(19) . . ?
Ag10 Ag24 Ag7 58.49(6) . . ?
Ag16 Ag24 Ag7 113.90(8) . . ?
P1 Ag24 Ag14 127.14(19) . . ?
Ag10 Ag24 Ag14 58.00(6) . . ?
Ag16 Ag24 Ag14 111.04(8) . . ?
Ag7 Ag24 Ag14 59.72(7) . . ?
P1 Ag24 Ag13 124.2(2) . . ?
Ag10 Ag24 Ag13 55.12(6) . . ?
Ag16 Ag24 Ag13 58.30(6) . . ?
Ag7 Ag24 Ag13 63.89(7) . . ?
Ag14 Ag24 Ag13 107.43(8) . . ?
P1 Ag24 Ag3 118.82(19) . . ?
Ag10 Ag24 Ag3 52.60(5) . . ?
Ag16 Ag24 Ag3 58.34(6) . . ?
Ag7 Ag24 Ag3 103.42(8) . . ?
Ag14 Ag24 Ag3 58.41(6) . . ?
Ag13 Ag24 Ag3 97.62(7) . . ?
P7 Ag25 Ag11 166.5(2) . . ?
P7 Ag25 Ag27 127.3(2) . . ?
Ag11 Ag25 Ag27 59.24(7) . . ?
P7 Ag25 Ag6 102.7(2) . . ?
Ag11 Ag25 Ag6 64.40(7) . . ?
Ag27 Ag25 Ag6 112.79(8) . . ?
P7 Ag25 Ag28 134.3(2) . . ?
Ag11 Ag25 Ag28 58.85(7) . . ?
Ag27 Ag25 Ag28 58.95(7) . . ?
Ag6 Ag25 Ag28 115.65(9) . . ?
P7 Ag25 Ag8 122.7(2) . . ?
Ag11 Ag25 Ag8 55.27(6) . . ?
Ag27 Ag25 Ag8 109.17(9) . . ?
Ag6 Ag25 Ag8 57.53(6) . . ?
Ag28 Ag25 Ag8 66.39(7) . . ?
P7 Ag25 Ag5 117.4(2) . . ?
Ag11 Ag25 Ag5 53.52(6) . . ?
Ag27 Ag25 Ag5 58.81(6) . . ?
Ag6 Ag25 Ag5 59.47(6) . . ?
Ag28 Ag25 Ag5 103.57(8) . . ?
Ag8 Ag25 Ag5 98.15(7) . . ?
P8 Ag26 Ag15 167.4(2) . . ?
P8 Ag26 Ag19 129.55(18) . . ?
Ag15 Ag26 Ag19 59.59(6) . . ?
P8 Ag26 Ag12 130.53(19) . . ?
Ag15 Ag26 Ag12 60.08(6) . . ?
Ag19 Ag26 Ag12 59.92(7) . . ?
P8 Ag26 Ag5 102.30(19) . . ?
Ag15 Ag26 Ag5 65.15(6) . . ?
Ag19 Ag26 Ag5 113.79(8) . . ?
Ag12 Ag26 Ag5 116.99(8) . . ?
P8 Ag26 Ag18 118.52(18) . . ?
Ag15 Ag26 Ag18 56.29(6) . . ?
Ag19 Ag26 Ag18 110.37(8) . . ?
Ag12 Ag26 Ag18 66.84(7) . . ?
Ag5 Ag26 Ag18 57.96(6) . . ?
P8 Ag26 Ag4 120.69(19) . . ?
Ag15 Ag26 Ag4 53.36(6) . . ?
Ag19 Ag26 Ag4 60.50(6) . . ?
Ag12 Ag26 Ag4 105.61(8) . . ?
Ag5 Ag26 Ag4 58.33(6) . . ?
Ag18 Ag26 Ag4 97.93(7) . . ?
P6 Ag27 Ag11 171.6(2) . . ?
P6 Ag27 Ag28 126.47(18) . . ?
Ag11 Ag27 Ag28 59.72(7) . . ?
P6 Ag27 Ag25 127.6(2) . . ?
Ag11 Ag27 Ag25 59.36(6) . . ?
Ag28 Ag27 Ag25 61.37(7) . . ?
P6 Ag27 Ag18 107.06(19) . . ?
Ag11 Ag27 Ag18 64.57(6) . . ?
Ag28 Ag27 Ag18 112.17(9) . . ?
Ag25 Ag27 Ag18 116.03(8) . . ?
P6 Ag27 Ag5 120.52(18) . . ?
Ag11 Ag27 Ag5 55.98(6) . . ?
Ag28 Ag27 Ag5 110.78(8) . . ?
Ag25 Ag27 Ag5 66.05(7) . . ?
Ag18 Ag27 Ag5 58.28(6) . . ?
P6 Ag27 Ag1 123.1(2) . . ?
Ag11 Ag27 Ag1 53.47(6) . . ?
Ag28 Ag27 Ag1 58.15(7) . . ?
Ag25 Ag27 Ag1 104.60(8) . . ?
Ag18 Ag27 Ag1 58.75(6) . . ?
Ag5 Ag27 Ag1 98.54(7) . . ?
P5 Ag28 Ag11 175.4(2) . . ?
P5 Ag28 Ag27 122.8(2) . . ?
Ag11 Ag28 Ag27 59.45(6) . . ?
P5 Ag28 Ag17 111.3(2) . . ?
Ag11 Ag28 Ag17 64.64(7) . . ?
Ag27 Ag28 Ag17 117.04(8) . . ?
P5 Ag28 Ag25 125.9(2) . . ?
Ag11 Ag28 Ag25 58.71(7) . . ?
Ag27 Ag28 Ag25 59.68(7) . . ?
Ag17 Ag28 Ag25 111.29(9) . . ?
P5 Ag28 Ag1 120.0(2) . . ?
Ag11 Ag28 Ag1 56.37(6) . . ?
Ag27 Ag28 Ag1 67.10(7) . . ?
Ag17 Ag28 Ag1 59.07(7) . . ?
Ag25 Ag28 Ag1 110.01(8) . . ?
P5 Ag28 Ag8 128.0(2) . . ?
Ag11 Ag28 Ag8 52.46(6) . . ?
Ag27 Ag28 Ag8 103.56(8) . . ?
Ag17 Ag28 Ag8 57.54(6) . . ?
Ag25 Ag28 Ag8 58.23(7) . . ?
Ag1 Ag28 Ag8 97.80(7) . . ?
C19 P1 C25 103.9(13) . . ?
C19 P1 C26 103.0(15) . . ?
C25 P1 C26 103.0(15) . . ?
C19 P1 Ag24 111.8(10) . . ?
C25 P1 Ag24 113.4(11) . . ?
C26 P1 Ag24 120.0(10) . . ?
C112 P2 C29 105.5(17) . . ?
C112 P2 C123 104.0(16) . . ?
C29 P2 C123 104.5(16) . . ?
C112 P2 Ag21 113.1(11) . . ?
C29 P2 Ag21 112.1(11) . . ?
C123 P2 Ag21 116.6(15) . . ?
C57 P3 C56 107.6(18) . . ?
C57 P3 C58 105.5(17) . . ?
C56 P3 C58 102.0(16) . . ?
C57 P3 Ag9 114.2(13) . . ?
C56 P3 Ag9 113.9(13) . . ?
C58 P3 Ag9 112.6(11) . . ?
C63 P4 C61 106.2(16) . . ?
C63 P4 C62 104.6(18) . . ?
C61 P4 C62 105.1(17) . . ?
C63 P4 Ag20 112.2(12) . . ?
C61 P4 Ag20 113.8(14) . . ?
C62 P4 Ag20 114.2(12) . . ?
C95 P5 C138 103(2) . . ?
C95 P5 C90 104.4(17) . . ?
C138 P5 C90 104.6(16) . . ?
C95 P5 Ag28 118.6(15) . . ?
C138 P5 Ag28 116.5(11) . . ?
C90 P5 Ag28 108.5(10) . . ?
C73 P6 C42 105.1(17) . . ?
C73 P6 C74 105.3(15) . . ?
C42 P6 C74 104.4(15) . . ?
C73 P6 Ag27 113.6(13) . . ?
C42 P6 Ag27 111.4(11) . . ?
C74 P6 Ag27 115.9(11) . . ?
C93 P7 C94 105.1(16) . . ?
C93 P7 C81 102.3(17) . . ?
C94 P7 C81 105.9(17) . . ?
C93 P7 Ag25 114.1(12) . . ?
C94 P7 Ag25 113.0(10) . . ?
C81 P7 Ag25 115.3(13) . . ?
C39 P8 C38 107.9(16) . . ?
C39 P8 C8 103.5(13) . . ?
C38 P8 C8 106.2(12) . . ?
C39 P8 Ag26 112.0(10) . . ?
C38 P8 Ag26 111.7(11) . . ?
C8 P8 Ag26 115.0(9) . . ?
C48 P9 C43 103.2(17) . . ?
C48 P9 C47 103.7(15) . . ?
C43 P9 C47 103.7(14) . . ?
C48 P9 Ag19 121.0(11) . . ?
C43 P9 Ag19 110.5(10) . . ?
C47 P9 Ag19 113.0(9) . . ?
C7 P10 C132 106.7(15) . . ?
C7 P10 C1 104.1(12) . . ?
C132 P10 C1 105.7(14) . . ?
C7 P10 Ag7 117.6(11) . . ?
C132 P10 Ag7 110.4(10) . . ?
C1 P10 Ag7 111.5(9) . . ?
C33 P11 C13 106.4(13) . . ?
C33 P11 C46 104.8(16) . . ?
C13 P11 C46 102.5(13) . . ?
C33 P11 Ag14 115.3(11) . . ?
C13 P11 Ag14 113.6(9) . . ?
C46 P11 Ag14 113.1(10) . . ?
C54 P12 C55 101.3(15) . . ?
C54 P12 C109 105.5(18) . . ?
C55 P12 C109 105.6(18) . . ?
C54 P12 Ag12 113.2(14) . . ?
C55 P12 Ag12 112.9(11) . . ?
C109 P12 Ag12 116.8(13) . . ?
W2 O1 Ag1 111.9(7) . . ?
W1 O2 Ag17 110.6(8) . . ?
W4 O3 Ag2 109.3(8) . . ?
W4 O5 Ag16 111.6(8) . . ?
W4 O7 Ag3 109.5(9) . . ?
W1 O8 Ag13 110.8(8) . . ?
W1 O10 Ag8 110.8(8) . . ?
W2 O11 Ag22 111.2(8) . . ?
W2 O13 Ag18 109.3(9) . . ?
W3 O14 Ag4 113.0(7) . . ?
W3 O15 Ag5 110.4(8) . . ?
W3 O16 Ag6 109.5(8) . . ?
C6 C1 C2 121(2) . . ?
C6 C1 P10 119(2) . . ?
C2 C1 P10 120(2) . . ?
C1 C2 C3 119(3) . . ?
C4 C3 C2 120(3) . . ?
C3 C4 C5 119(3) . . ?
C4 C5 C6 118(3) . . ?
C1 C6 C5 122(3) . . ?
C11 C7 C9 118(3) . . ?
C11 C7 P10 123(2) . . ?
C9 C7 P10 119(2) . . ?
C68 C8 C72 118(2) . . ?
C68 C8 P8 117.7(18) . . ?
C72 C8 P8 125(2) . . ?
C10 C9 C7 119(3) . . ?
C9 C10 C106 122(3) . . ?
C7 C11 C12 121(3) . . ?
C106 C12 C11 123(3) . . ?
C18 C13 C14 120(3) . . ?
C18 C13 P11 118(2) . . ?
C14 C13 P11 122(2) . . ?
C13 C14 C15 118(3) . . ?
C16 C15 C14 121(3) . . ?
C15 C16 C17 119(3) . . ?
C18 C17 C16 121(3) . . ?
C13 C18 C17 121(3) . . ?
C20 C19 C24 117(3) . . ?
C20 C19 P1 120(2) . . ?
C24 C19 P1 122(2) . . ?
C19 C20 C21 117(3) . . ?
C22 C21 C20 123(3) . . ?
C23 C22 C21 116(3) . . ?
C24 C23 C22 124(3) . . ?
C23 C24 C19 123(3) . . ?
C30 C25 C107 119(3) . . ?
C30 C25 P1 120(3) . . ?
C107 C25 P1 121(3) . . ?
C27 C26 P1 113(2) . . ?
C28 C27 C26 113(2) . . ?
C27 C28 C29 111(2) . . ?
C28 C29 P2 110.7(19) . . ?
C25 C30 C32 121(3) . . ?
C32 C31 C108 123(3) . . ?
C31 C32 C30 120(4) . . ?
C34 C33 C35 116(3) . . ?
C34 C33 P11 124(3) . . ?
C35 C33 P11 119(2) . . ?
C33 C34 C91 118(3) . . ?
C36 C35 C33 121(3) . . ?
C35 C36 C37 127(4) . . ?
C36 C37 C91 111(3) . . ?
C53 C38 C52 120(3) . . ?
C53 C38 P8 120(2) . . ?
C52 C38 P8 120(2) . . ?
C40 C39 P8 112(2) . . ?
C41 C40 C39 119(3) . . ?
C40 C41 C42 117(3) . . ?
C41 C42 P6 112(2) . . ?
C44 C43 P9 112(2) . . ?
C45 C44 C43 112(3) . . ?
C44 C45 C46 113(3) . . ?
C45 C46 P11 105(2) . . ?
C50 C47 C49 120(3) . . ?
C50 C47 P9 119.0(19) . . ?
C49 C47 P9 120(2) . . ?
C59 C48 C122 118(3) . . ?
C59 C48 P9 119(3) . . ?
C122 C48 P9 123(3) . . ?
C64 C49 C47 119(3) . . ?
C47 C50 C51 118(3) . . ?
C65 C51 C50 123(3) . . ?
C66 C52 C38 121(3) . . ?
C38 C53 C67 117(3) . . ?
C129 C54 C130 121(4) . . ?
C129 C54 P12 123(3) . . ?
C130 C54 P12 116(3) . . ?
C119 C55 C121 116(3) . . ?
C119 C55 P12 122(3) . . ?
C121 C55 P12 122(3) . . ?
C111 C56 P3 109(3) . . ?
C116 C57 C117 117(4) . . ?
C116 C57 P3 126(3) . . ?
C117 C57 P3 117(3) . . ?
C96 C58 C97 116(3) . . ?
C96 C58 P3 125(3) . . ?
C97 C58 P3 119(2) . . ?
C48 C59 C60 120(4) . . ?
C162 C60 C59 127(4) . . ?
C137 C61 C102 116(4) . . ?
C137 C61 P4 125(4) . . ?
C102 C61 P4 119(3) . . ?
C149 C62 P4 111(3) . . ?
C101 C63 C100 118(3) . . ?
C101 C63 P4 119(2) . . ?
C100 C63 P4 123(3) . . ?
C49 C64 C65 122(3) . . ?
C51 C65 C64 117(3) . . ?
C52 C66 C163 122(4) . . ?
C163 C67 C53 120(3) . . ?
C69 C68 C8 122(3) . . ?
C68 C69 C70 118(3) . . ?
C71 C70 C69 122(3) . . ?
C70 C71 C72 118(3) . . ?
C8 C72 C71 121(3) . . ?
C75 C73 C76 115(4) . . ?
C75 C73 P6 119(3) . . ?
C76 C73 P6 126(3) . . ?
C77 C74 C79 122(3) . . ?
C77 C74 P6 118(3) . . ?
C79 C74 P6 121(2) . . ?
C144 C75 C73 125(4) . . ?
C73 C76 C145 125(4) . . ?
C74 C77 C78 116(4) . . ?
C92 C78 C77 118(3) . . ?
C80 C79 C74 120(3) . . ?
C79 C80 C92 124(4) . . ?
C83 C81 C82 117(4) . . ?
C83 C81 P7 120(3) . . ?
C82 C81 P7 123(3) . . ?
C147 C82 C81 119(4) . . ?
C81 C83 C84 124(4) . . ?
C148 C84 C83 120(4) . . ?
C90 C85 C86 118(3) . . ?
C87 C86 C85 122(3) . . ?
C86 C87 C88 120(3) . . ?
C87 C88 C89 120(3) . . ?
C90 C89 C88 117(3) . . ?
C85 C90 C89 123(3) . . ?
C85 C90 P5 119(2) . . ?
C89 C90 P5 118(2) . . ?
C37 C91 C34 125(3) . . ?
C80 C92 C78 120(4) . . ?
C134 C93 P7 108(3) . . ?
C127 C94 C166 120.0 . . ?
C127 C94 P7 118.5(16) . . ?
C166 C94 P7 121.5(16) . . ?
C128 C127 C94 120.0 . . ?
C127 C128 C165 120.0 . . ?
C128 C165 C164 120.0 . . ?
C166 C164 C165 120.0 . . ?
C164 C166 C94 120.0 . . ?
C150 C95 P5 119(3) . . ?
C58 C96 C151 122(4) . . ?
C58 C97 C98 126(3) . . ?
C97 C98 C99 118(4) . . ?
C151 C99 C98 118(4) . . ?
C63 C100 C153 117(4) . . ?
C131 C101 C63 118(3) . . ?
C61 C102 C103 125(4) . . ?
C104 C103 C102 117(5) . . ?
C105 C104 C103 120(5) . . ?
C104 C105 C137 124(4) . . ?
C12 C106 C10 115(3) . . ?
C108 C107 C25 114(3) . . ?
C31 C108 C107 122(4) . . ?
C110 C109 P12 113(3) . . ?
C111 C110 C109 126(4) . . ?
C110 C111 C56 124(4) . . ?
C115 C112 C113 122(4) . . ?
C115 C112 P2 118(3) . . ?
C113 C112 P2 120(3) . . ?
C112 C113 C114 123(4) . . ?
C167 C114 C113 118(4) . . ?
C112 C115 C168 112(4) . . ?
C57 C116 C156 120(4) . . ?
C118 C117 C57 120(4) . . ?
C157 C118 C117 120(4) . . ?
C55 C119 C120 123(4) . . ?
C155 C120 C119 120(4) . . ?
C55 C121 C154 119(4) . . ?
C161 C122 C48 121(4) . . ?
C124 C123 C126 118(3) . . ?
C124 C123 P2 121(3) . . ?
C126 C123 P2 121(3) . . ?
C123 C124 C125 120(4) . . ?
C136 C125 C124 117(4) . . ?
C135 C126 C123 124(4) . . ?
C54 C129 C158 122(4) . . ?
C160 C130 C54 118(4) . . ?
C152 C131 C101 126(4) . . ?
C133 C132 P10 109(2) . . ?
C132 C133 C134 112(3) . . ?
C133 C134 C93 111(3) . . ?
C126 C135 C136 115(4) . . ?
C125 C136 C135 126(4) . . ?
C61 C137 C105 117(4) . . ?
C143 C138 C139 109(3) . . ?
C143 C138 P5 126(3) . . ?
C139 C138 P5 124(3) . . ?
C140 C139 C138 124(3) . . ?
C141 C140 C139 115(4) . . ?
C142 C141 C140 126(4) . . ?
C141 C142 C143 120(4) . . ?
C142 C143 C138 125(4) . . ?
C75 C144 C146 115(4) . . ?
C146 C145 C76 112(4) . . ?
C145 C146 C144 128(4) . . ?
C82 C147 C148 122(4) . . ?
C84 C148 C147 118(4) . . ?
C150 C149 C62 112(4) . . ?
C149 C150 C95 111(4) . . ?
C99 C151 C96 120(3) . . ?
C131 C152 C153 119(4) . . ?
C152 C153 C100 122(3) . . ?
C155 C154 C121 120(4) . . ?
C154 C155 C120 120(4) . . ?
C157 C156 C116 123(4) . . ?
C156 C157 C118 120(5) . . ?
C159 C158 C129 119(4) . . ?
C158 C159 C160 122(4) . . ?
C130 C160 C159 117(5) . . ?
C122 C161 C162 119(4) . . ?
C60 C162 C161 115(4) . . ?
C67 C163 C66 120(3) . . ?
C114 C167 C168 122(4) . . ?
C167 C168 C115 123(4) . . ?

_refine_diff_density_max         3.546
_refine_diff_density_min         -2.354
_refine_diff_density_rms         0.336


_vrf_PLAT602_11_a                
;

PROBLEM:  VERY LARGE Solvent Accessible VOID(S) in Structure ! Info  
RESPONSE: The compound contains a large number of severely 
disordered methanol molecules of crystallization,
which 
could not be fully modelled.  The large voids are due to 
these disordered solvents.

;

# end Validation Reply Form
