
data_Ni15Te12O34Cl10
 
_audit_creation_method            SHELXL-97 
_chemical_name_systematic 
; 
 ? 
; 
_chemical_name_common             ? 
_chemical_melting_point           ? 
_chemical_formula_moiety          'Cl10 Ni15 O34 Te12'
_chemical_formula_sum 
 'Cl10 Ni15 O34 Te12' 
_chemical_formula_weight          3310.35 
 
loop_ 
 _atom_type_symbol 
 _atom_type_description 
 _atom_type_scat_dispersion_real 
 _atom_type_scat_dispersion_imag 
 _atom_type_scat_source 
 'O'  'O'   0.0106   0.0060 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Cl'  'Cl'   0.1484   0.1585 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Ni'  'Ni'   0.3393   1.1124 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Te'  'Te'  -0.5308   1.6751 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 
_symmetry_cell_setting            triclinic
_symmetry_space_group_name_H-M    P-1
_symmetry_space_group_name_Hall   -P1
 
loop_ 
 _symmetry_equiv_pos_as_xyz 
 'x, y, z' 
 '-x, -y, -z' 
 
_cell_length_a                    10.3248(6) 
_cell_length_b                    10.3249(6) 
_cell_length_c                    11.6460(8) 
_cell_angle_alpha                 73.782(6) 
_cell_angle_beta                  73.782(6) 
_cell_angle_gamma                 63.51(2) 
_cell_volume                      1049.53(21) 
_cell_formula_units_Z             1 
_cell_measurement_temperature     293(2) 
_cell_measurement_reflns_used     24105 
_cell_measurement_theta_min       3.6715
_cell_measurement_theta_max       34.5197
 
_exptl_crystal_description        block
_exptl_crystal_colour             brown
_exptl_crystal_size_max           0.1483
_exptl_crystal_size_mid           0.1063
_exptl_crystal_size_min           0.0606
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_diffrn     5.238 
_exptl_crystal_density_method     'not measured' 
_exptl_crystal_F_000              1486 
_exptl_absorpt_coefficient_mu     15.469 
_exptl_absorpt_correction_type    analytical
_exptl_absorpt_correction_T_min   0.166
_exptl_absorpt_correction_T_max   0.405
_exptl_absorpt_process_details    
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.32.15 (release 10-01-2008 CrysAlis171 .NET)
(compiled Jan 10 2008,16:37:18)
Analytical numeric absorption correction using a multifaceted crystal
			model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
;
 
_exptl_special_details 
; 
 ? 
; 
 
_diffrn_ambient_temperature       293(2) 
_diffrn_radiation_wavelength      0.71073 
_diffrn_radiation_type            MoK\a 
_diffrn_radiation_source          'fine-focus sealed tube' 
_diffrn_radiation_monochromator   graphite 
_diffrn_measurement_device_type   'Oxford Xcalibur3 Diffractometer'
_diffrn_measurement_method        'f\scan' 
_diffrn_detector_area_resol_mean  ? 
_diffrn_standards_number          0 
_diffrn_standards_interval_count  0 
_diffrn_standards_interval_time   0
_diffrn_standards_decay_%         0 
_diffrn_reflns_number             24105 
_diffrn_reflns_av_R_equivalents   0.0228 
_diffrn_reflns_av_sigmaI/netI     0.0142 
_diffrn_reflns_limit_h_min        -12 
_diffrn_reflns_limit_h_max        12 
_diffrn_reflns_limit_k_min        -12 
_diffrn_reflns_limit_k_max        12 
_diffrn_reflns_limit_l_min        -14 
_diffrn_reflns_limit_l_max        14 
_diffrn_reflns_theta_min          4.14 
_diffrn_reflns_theta_max          26.37 
_reflns_number_total              4117 
_reflns_number_gt                 3872 
_reflns_threshold_expression      >2sigma(I) 
 
_computing_data_collection        ? 
_computing_cell_refinement        ? 
_computing_data_reduction         ? 
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)' 
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)' 
_computing_molecular_graphics     ? 
_computing_publication_material   ? 
 
_refine_special_details 
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
; 
 
_refine_ls_structure_factor_coef  Fsqd  
_refine_ls_matrix_type            full 
_refine_ls_weighting_scheme       calc  
_refine_ls_weighting_details 
 'calc w=1/[σ²(Fo²)+(0.0407P)²+7.1561P] where P=(Fo²+2Fc²)/3' 
_atom_sites_solution_primary      direct 
_atom_sites_solution_secondary    difmap 
_atom_sites_solution_hydrogens    '.'
_refine_ls_hydrogen_treatment     'constr'
_refine_ls_extinction_method      SHELXL 
_refine_ls_extinction_coef        0.00446(16) 
_refine_ls_extinction_expression 
 'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^' 
_refine_ls_number_reflns          4117 
_refine_ls_number_parameters      323 
_refine_ls_number_restraints      0 
_refine_ls_R_factor_all           0.0273 
_refine_ls_R_factor_gt            0.0246 
_refine_ls_wR_factor_ref          0.0696 
_refine_ls_wR_factor_gt           0.0688 
_refine_ls_goodness_of_fit_ref    1.160 
_refine_ls_restrained_S_all       1.160 
_refine_ls_shift/su_max           0.001 
_refine_ls_shift/su_mean          0.000 
 
loop_ 
 _atom_site_label 
 _atom_site_type_symbol 
 _atom_site_fract_x 
 _atom_site_fract_y 
 _atom_site_fract_z 
 _atom_site_U_iso_or_equiv 
 _atom_site_adp_type 
 _atom_site_occupancy 
 _atom_site_symmetry_multiplicity 
 _atom_site_calc_flag 
 _atom_site_refinement_flags 
 _atom_site_disorder_assembly 
 _atom_site_disorder_group 
Te1 Te 0.92985(4) 0.93140(4) -0.18534(4) 0.00705(11) Uani 1 1 d . . . 
Te2 Te 0.89314(4) 0.81794(4) 0.25306(4) 0.00819(11) Uani 1 1 d . . . 
Te3 Te 0.72145(4) 0.71164(4) -0.10159(4) 0.00692(11) Uani 1 1 d . . . 
Te4 Te 0.76483(4) 0.20708(4) 0.01113(4) 0.00670(11) Uani 1 1 d . . . 
Te5 Te 0.44335(4) -0.04559(4) 0.38061(4) 0.00734(11) Uani 1 1 d . . . 
Te6 Te -0.05734(4) 0.44296(4) 0.38305(4) 0.00744(11) Uani 1 1 d . . . 
Ni1 Ni 0.96673(9) 0.61832(9) 0.07826(7) 0.00748(18) Uani 1 1 d . . . 
Ni2 Ni 0.79809(9) 0.41108(9) 0.16836(8) 0.00817(18) Uani 1 1 d . . . 
Ni3 Ni 0.42521(9) 0.78789(9) 0.17096(7) 0.00797(18) Uani 1 1 d . . . 
Ni4 Ni 0.5000 0.5000 0.0000 0.0066(2) Uani 1 2 d S . . 
Ni5 Ni 0.24998(9) 0.55773(9) 0.25017(8) 0.00899(18) Uani 1 1 d . . . 
Ni6 Ni 0.54480(9) 0.25936(9) 0.24556(8) 0.00967(19) Uani 1 1 d . . . 
Ni7 Ni 0.62121(9) -0.03322(9) 0.07824(7) 0.00734(18) Uani 1 1 d . . . 
Ni8 Ni 0.26769(9) 0.26255(9) 0.46575(8) 0.00946(18) Uani 1 1 d . . . 
Cl1 Cl 0.60835(18) 0.59434(18) 0.27183(15) 0.0142(3) Uani 1 1 d . . . 
Cl2 Cl 0.21565(18) 0.76308(18) 0.33662(15) 0.0143(3) Uani 1 1 d . . . 
Cl3 Cl 0.77090(19) 0.20744(19) 0.33189(15) 0.0168(3) Uani 1 1 d . . . 
Cl4 Cl 0.4135(2) 0.4067(2) 0.39368(18) 0.0211(4) Uani 1 1 d . . . 
Cl5 Cl 0.11152(18) 0.13897(18) 0.45624(17) 0.0169(4) Uani 1 1 d . . . 
O1 O 1.0260(5) 1.0166(5) -0.1342(4) 0.0113(10) Uani 1 1 d . . . 
O2 O 0.7454(5) 1.0274(5) -0.0820(4) 0.0099(9) Uani 1 1 d . . . 
O3 O 1.0098(5) 0.7482(5) -0.0831(4) 0.0113(10) Uani 1 1 d . . . 
O4 O 1.0680(5) 0.6742(5) 0.1762(4) 0.0100(9) Uani 1 1 d . . . 
O5 O 0.8013(5) 0.8049(5) 0.1416(4) 0.0108(9) Uani 1 1 d . . . 
O6 O 0.8429(5) 0.5564(5) 0.0052(4) 0.0095(9) Uani 1 1 d . . . 
O7 O 0.5719(5) 0.8292(5) 0.0092(4) 0.0102(9) Uani 1 1 d . . . 
O8 O 0.6276(5) 0.6061(5) -0.1301(4) 0.0071(9) Uani 1 1 d . . . 
O9 O 0.6623(5) 0.3691(5) 0.1013(4) 0.0088(9) Uani 1 1 d . . . 
O10 O 0.6267(5) 0.3357(5) -0.0995(4) 0.0075(9) Uani 1 1 d . . . 
O11 O 0.6463(5) 0.1199(5) 0.1303(4) 0.0106(9) Uani 1 1 d . . . 
O12 O 0.4681(5) -0.0664(5) 0.2201(4) 0.0107(9) Uani 1 1 d . . . 
O13 O 0.6347(5) -0.0999(5) 0.4030(4) 0.0151(10) Uani 1 1 d . . . 
O14 O 0.4080(5) 0.1553(5) 0.3327(4) 0.0109(9) Uani 1 1 d . . . 
O15 O 0.1343(5) 0.4337(5) 0.3634(5) 0.0135(10) Uani 1 1 d . . . 
O16 O -0.0501(5) 0.4520(5) 0.2195(4) 0.0095(9) Uani 1 1 d . . . 
O17 O -0.1390(5) 0.6480(5) 0.3829(4) 0.0115(10) Uani 1 1 d . . . 
 
 
_geom_special_details 
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
; 
 
loop_ 
 _geom_bond_atom_site_label_1 
 _geom_bond_atom_site_label_2 
 _geom_bond_distance 
 _geom_bond_site_symmetry_2 
 _geom_bond_publ_flag 
Te1 O1 1.875(4) . ? 
Te1 O3 1.891(5) . ? 
Te1 O2 1.939(4) . ? 
Te2 O5 1.872(4) . ? 
Te2 O4 1.927(4) . ? 
Te2 O17 2.057(5) 1_655 ? 
Te2 O1 2.200(5) 2_775 ? 
Te3 O8 1.887(4) . ? 
Te3 O7 1.901(4) . ? 
Te3 O6 1.911(5) . ? 
Te4 O11 1.889(4) . ? 
Te4 O9 1.950(4) . ? 
Te4 O10 1.959(4) . ? 
Te4 O2 2.497(4) 1_545 ? 
Te5 O13 1.872(5) . ? 
Te5 O12 1.875(4) . ? 
Te5 O14 1.881(4) . ? 
Te6 O16 1.862(4) . ? 
Te6 O15 1.889(5) . ? 
Te6 O17 1.897(4) . ? 
Te6 Cl5 2.8412(18) . ? 
Ni1 O3 2.046(5) . ? 
Ni1 O16 2.053(5) 1_655 ? 
Ni1 O4 2.074(4) . ? 
Ni1 O5 2.080(4) . ? 
Ni1 O6 2.100(4) . ? 
Ni1 O6 2.194(4) 2_765 ? 
Ni2 O9 2.027(4) . ? 
Ni2 O16 2.059(5) 1_655 ? 
Ni2 O3 2.128(5) 2_765 ? 
Ni2 O6 2.148(5) . ? 
Ni2 Cl1 2.3492(17) . ? 
Ni2 Cl3 2.4734(19) . ? 
Ni3 O12 2.000(4) 1_565 ? 
Ni3 O10 2.015(4) 2_665 ? 
Ni3 O7 2.135(5) . ? 
Ni3 O2 2.175(5) 2_675 ? 
Ni3 Cl1 2.3469(19) . ? 
Ni3 Cl2 2.5210(18) . ? 
Ni4 O10 2.050(4) 2_665 ? 
Ni4 O10 2.050(4) . ? 
Ni4 O9 2.054(5) 2_665 ? 
Ni4 O9 2.054(5) . ? 
Ni4 O8 2.116(4) . ? 
Ni4 O8 2.116(4) 2_665 ? 
Ni5 O4 2.007(5) 1_455 ? 
Ni5 O15 2.085(5) . ? 
Ni5 O10 2.199(4) 2_665 ? 
Ni5 O8 2.200(4) 2_665 ? 
Ni5 Cl4 2.418(2) . ? 
Ni5 Cl2 2.4408(17) . ? 
Ni6 O11 1.980(4) . ? 
Ni6 O14 2.031(4) . ? 
Ni6 O9 2.145(4) . ? 
Ni6 O8 2.234(5) 2_665 ? 
Ni6 Cl4 2.3339(19) . ? 
Ni6 Cl3 2.577(2) . ? 
Ni7 O11 1.981(4) . ? 
Ni7 O12 2.013(4) . ? 
Ni7 O5 2.024(5) 1_545 ? 
Ni7 O2 2.060(5) 1_545 ? 
Ni7 O7 2.106(4) 1_545 ? 
Ni7 O7 2.375(5) 2_665 ? 
Ni8 O14 2.000(5) . ? 
Ni8 O15 2.002(5) . ? 
Ni8 O13 2.022(5) 2_656 ? 
Ni8 O17 2.058(4) 2_566 ? 
Ni8 Cl4 2.4041(19) . ? 
Ni8 Cl5 2.5007(18) . ? 

 
loop_ 
 _geom_angle_atom_site_label_1 
 _geom_angle_atom_site_label_2 
 _geom_angle_atom_site_label_3 
 _geom_angle 
 _geom_angle_site_symmetry_1 
 _geom_angle_site_symmetry_3 
 _geom_angle_publ_flag 
O1 Te1 O3 93.3(2) . . ? 
O1 Te1 O2 92.07(19) . . ? 
O3 Te1 O2 101.1(2) . . ? 
O5 Te2 O4 84.87(19) . . ? 
O5 Te2 O17 95.2(2) . 1_655 ? 
O4 Te2 O17 88.33(19) . 1_655 ? 
O5 Te2 O1 96.98(19) . 2_775 ? 
O4 Te2 O1 86.28(18) . 2_775 ? 
O17 Te2 O1 166.15(18) 1_655 2_775 ? 
O8 Te3 O7 101.90(19) . . ? 
O8 Te3 O6 97.66(19) . . ? 
O7 Te3 O6 101.7(2) . . ? 
O11 Te4 O9 84.16(18) . . ? 
O11 Te4 O10 100.3(2) . . ? 
O9 Te4 O10 83.42(19) . . ? 
O11 Te4 O2 73.39(17) . 1_545 ? 
O9 Te4 O2 147.19(16) . 1_545 ? 
O10 Te4 O2 77.60(16) . 1_545 ? 
O13 Te5 O12 104.1(2) . . ? 
O13 Te5 O14 93.4(2) . . ? 
O12 Te5 O14 92.0(2) . . ? 
O16 Te6 O15 95.9(2) . . ? 
O16 Te6 O17 98.2(2) . . ? 
O15 Te6 O17 90.8(2) . . ? 
O16 Te6 Cl5 101.29(15) . . ? 
O15 Te6 Cl5 76.53(15) . . ? 
O17 Te6 Cl5 157.67(15) . . ? 
O3 Ni1 O16 167.70(18) . 1_655 ? 
O3 Ni1 O4 96.07(19) . . ? 
O16 Ni1 O4 90.00(18) 1_655 . ? 
O3 Ni1 O5 89.30(19) . . ? 
O16 Ni1 O5 102.56(18) 1_655 . ? 
O4 Ni1 O5 76.21(17) . . ? 
O3 Ni1 O6 91.79(19) . . ? 
O16 Ni1 O6 83.10(18) 1_655 . ? 
O4 Ni1 O6 171.04(18) . . ? 
O5 Ni1 O6 99.66(17) . . ? 
O3 Ni1 O6 83.22(18) . 2_765 ? 
O16 Ni1 O6 85.17(18) 1_655 2_765 ? 
O4 Ni1 O6 100.37(17) . 2_765 ? 
O5 Ni1 O6 171.44(18) . 2_765 ? 
O6 Ni1 O6 84.80(18) . 2_765 ? 
O9 Ni2 O16 174.18(18) . 1_655 ? 
O9 Ni2 O3 92.83(18) . 2_765 ? 
O16 Ni2 O3 82.76(18) 1_655 2_765 ? 
O9 Ni2 O6 93.90(18) . . ? 
O16 Ni2 O6 81.78(17) 1_655 . ? 
O3 Ni2 O6 82.45(17) 2_765 . ? 
O9 Ni2 Cl1 95.10(13) . . ? 
O16 Ni2 Cl1 89.30(13) 1_655 . ? 
O3 Ni2 Cl1 172.06(14) 2_765 . ? 
O6 Ni2 Cl1 96.62(13) . . ? 
O9 Ni2 Cl3 81.63(14) . . ? 
O16 Ni2 Cl3 101.93(14) 1_655 . ? 
O3 Ni2 Cl3 87.85(13) 2_765 . ? 
O6 Ni2 Cl3 169.13(13) . . ? 
Cl1 Ni2 Cl3 93.66(6) . . ? 
O12 Ni3 O10 171.44(19) 1_565 2_665 ? 
O12 Ni3 O7 81.65(17) 1_565 . ? 
O10 Ni3 O7 93.33(17) 2_665 . ? 
O12 Ni3 O2 88.02(18) 1_565 2_675 ? 
O10 Ni3 O2 84.62(17) 2_665 2_675 ? 
O7 Ni3 O2 84.91(18) . 2_675 ? 
O12 Ni3 Cl1 90.02(15) 1_565 . ? 
O10 Ni3 Cl1 97.40(14) 2_665 . ? 
O7 Ni3 Cl1 95.70(14) . . ? 
O2 Ni3 Cl1 177.84(13) 2_675 . ? 
O12 Ni3 Cl2 102.35(13) 1_565 . ? 
O10 Ni3 Cl2 81.40(13) 2_665 . ? 
O7 Ni3 Cl2 169.15(14) . . ? 
O2 Ni3 Cl2 85.16(13) 2_675 . ? 
Cl1 Ni3 Cl2 94.39(6) . . ? 
O10 Ni4 O10 180.0 2_665 . ? 
O10 Ni4 O9 78.64(17) 2_665 2_665 ? 
O10 Ni4 O9 101.36(17) . 2_665 ? 
O10 Ni4 O9 101.36(17) 2_665 . ? 
O10 Ni4 O9 78.64(17) . . ? 
O9 Ni4 O9 180.0(3) 2_665 . ? 
O10 Ni4 O8 98.57(17) 2_665 . ? 
O10 Ni4 O8 81.43(17) . . ? 
O9 Ni4 O8 85.01(17) 2_665 . ? 
O9 Ni4 O8 94.99(17) . . ? 
O10 Ni4 O8 81.43(17) 2_665 2_665 ? 
O10 Ni4 O8 98.57(17) . 2_665 ? 
O9 Ni4 O8 94.99(17) 2_665 2_665 ? 
O9 Ni4 O8 85.01(17) . 2_665 ? 
O8 Ni4 O8 180.0(2) . 2_665 ? 
O4 Ni5 O15 85.27(19) 1_455 . ? 
O4 Ni5 O10 90.46(18) 1_455 2_665 ? 
O15 Ni5 O10 167.21(18) . 2_665 ? 
O4 Ni5 O8 99.68(17) 1_455 2_665 ? 
O15 Ni5 O8 92.50(18) . 2_665 ? 
O10 Ni5 O8 76.32(16) 2_665 2_665 ? 
O4 Ni5 Cl4 162.23(14) 1_455 . ? 
O15 Ni5 Cl4 79.20(14) . . ? 
O10 Ni5 Cl4 106.51(13) 2_665 . ? 
O8 Ni5 Cl4 89.65(13) 2_665 . ? 
O4 Ni5 Cl2 92.73(13) 1_455 . ? 
O15 Ni5 Cl2 112.37(15) . . ? 
O10 Ni5 Cl2 79.83(12) 2_665 . ? 
O8 Ni5 Cl2 153.10(12) 2_665 . ? 
Cl4 Ni5 Cl2 85.33(7) . . ? 
O11 Ni6 O14 90.98(18) . . ? 
O11 Ni6 O9 77.06(17) . . ? 
O14 Ni6 O9 160.20(18) . . ? 
O11 Ni6 O8 89.68(18) . 2_665 ? 
O14 Ni6 O8 84.21(18) . 2_665 ? 
O9 Ni6 O8 80.05(17) . 2_665 ? 
O11 Ni6 Cl4 173.93(14) . . ? 
O14 Ni6 Cl4 83.08(14) . . ? 
O9 Ni6 Cl4 109.00(13) . . ? 
O8 Ni6 Cl4 91.01(12) 2_665 . ? 
O11 Ni6 Cl3 97.48(15) . . ? 
O14 Ni6 Cl3 120.69(15) . . ? 
O9 Ni6 Cl3 77.04(13) . . ? 
O8 Ni6 Cl3 153.74(12) 2_665 . ? 
Cl4 Ni6 Cl3 84.52(6) . . ? 
O11 Ni7 O12 98.38(18) . . ? 
O11 Ni7 O5 92.64(19) . 1_545 ? 
O12 Ni7 O5 98.0(2) . 1_545 ? 
O11 Ni7 O2 82.52(18) . 1_545 ? 
O12 Ni7 O2 169.5(2) . 1_545 ? 
O5 Ni7 O2 92.48(19) 1_545 1_545 ? 
O11 Ni7 O7 171.8(2) . 1_545 ? 
O12 Ni7 O7 82.06(18) . 1_545 ? 
O5 Ni7 O7 95.42(18) 1_545 1_545 ? 
O2 Ni7 O7 95.56(18) 1_545 1_545 ? 
O11 Ni7 O7 83.53(17) . 2_665 ? 
O12 Ni7 O7 88.00(18) . 2_665 ? 
O5 Ni7 O7 173.35(17) 1_545 2_665 ? 
O2 Ni7 O7 81.66(17) 1_545 2_665 ? 
O7 Ni7 O7 88.29(17) 1_545 2_665 ? 
O14 Ni8 O15 98.1(2) . . ? 
O14 Ni8 O13 92.8(2) . 2_656 ? 
O15 Ni8 O13 168.1(2) . 2_656 ? 
O14 Ni8 O17 172.9(2) . 2_566 ? 
O15 Ni8 O17 89.0(2) . 2_566 ? 
O13 Ni8 O17 80.17(19) 2_656 2_566 ? 
O14 Ni8 Cl4 81.93(14) . . ? 
O15 Ni8 Cl4 81.15(14) . . ? 
O13 Ni8 Cl4 105.37(15) 2_656 . ? 
O17 Ni8 Cl4 99.29(14) 2_566 . ? 
O14 Ni8 Cl5 84.71(14) . . ? 
O15 Ni8 Cl5 83.57(14) . . ? 
O13 Ni8 Cl5 92.59(15) 2_656 . ? 
O17 Ni8 Cl5 96.13(14) 2_566 . ? 
Cl4 Ni8 Cl5 158.03(7) . . ? 
 
_diffrn_measured_fraction_theta_max    0.962 
_diffrn_reflns_theta_full              26.37 
_diffrn_measured_fraction_theta_full   0.962 
_refine_diff_density_max    2.181 
_refine_diff_density_min   -1.133 
_refine_diff_density_rms    0.311 
