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NMR signal assignments of polymer ligands, synthetic procedures of monomers for polymer ligands (MA-Val-OPac, MA-β-Ala-OBzl, and MA-γ-Abu-OtBu) and model ligands for the polymer repeated unit (4H, 5H, and 6H), 1H NMR spectra of 4H, 4NMe4, 5H, 5NMe4, 6H, and 6NMe4, 13C CP/MAS spectra of model ligand–CaCO3 composites, FE/SEM images of model ligand–CaCO3 composites, and the calibration curve of the ratio of calcite to vaterite content on an XRD