# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C # This journal is © The Royal Society of Chemistry 2013 ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_fyz20120331_0m _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'B10 H6 O22 Sr4' _chemical_formula_weight 816.63 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sr Sr -1.5307 3.2498 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting Triclinic _symmetry_space_group_name_H-M 'P1 ' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' _cell_length_a 6.4991(6) _cell_length_b 6.5059(6) _cell_length_c 11.3175(11) _cell_angle_alpha 88.458(6) _cell_angle_beta 86.019(5) _cell_angle_gamma 61.351(5) _cell_volume 418.92(7) _cell_formula_units_Z 1 _cell_measurement_temperature 296(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour colourless _exptl_crystal_size_max 0.17 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.06 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 3.237 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 384 _exptl_absorpt_coefficient_mu 12.791 _exptl_absorpt_correction_type numerical _exptl_absorpt_correction_T_min 0.2157 _exptl_absorpt_correction_T_max 0.5344 _exptl_absorpt_process_details face-indexed _exptl_special_details ; ? ; _diffrn_ambient_temperature 296(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 8801 _diffrn_reflns_av_R_equivalents 0.0331 _diffrn_reflns_av_sigmaI/netI 0.0605 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_theta_min 1.80 _diffrn_reflns_theta_max 27.51 _reflns_number_total 3457 _reflns_number_gt 3215 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'Bruker SMART' _computing_cell_refinement 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0103P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.016(6) _refine_ls_number_reflns 3457 _refine_ls_number_parameters 325 _refine_ls_number_restraints 3 _refine_ls_R_factor_all 0.0324 _refine_ls_R_factor_gt 0.0288 _refine_ls_wR_factor_ref 0.0597 _refine_ls_wR_factor_gt 0.0587 _refine_ls_goodness_of_fit_ref 1.018 _refine_ls_restrained_S_all 1.018 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sr1 Sr 0.47985(8) 0.23922(8) 0.22349(5) 0.01283(13) Uani 1 1 d . . . Sr2 Sr 0.47062(8) 0.43005(8) 0.74251(5) 0.01272(13) Uani 1 1 d . . . Sr3 Sr 0.88262(8) 0.38101(8) 0.43665(5) 0.01128(12) Uani 1 1 d . . . Sr4 Sr 0.89332(8) -0.12186(8) -0.05823(5) 0.01224(12) Uani 1 1 d . . . B1 B 0.3461(11) -0.0494(11) 0.7418(6) 0.0105(13) Uani 1 1 d . . . B2 B 1.0047(10) -0.6572(10) -0.2360(5) 0.0072(12) Uani 1 1 d . . . B3 B -0.0344(10) 1.0302(10) 0.6578(6) 0.0099(13) Uani 1 1 d . . . B4 B 0.8938(10) -0.6534(11) -0.0117(6) 0.0101(13) Uani 1 1 d . . . B5 B 0.3789(11) 0.7592(11) 0.2226(6) 0.0113(13) Uani 1 1 d . . . B6 B 0.8802(11) -0.1603(11) 0.4967(6) 0.0116(13) Uani 1 1 d . . . B7 B 0.8296(10) -0.4128(10) 0.1651(6) 0.0090(12) Uani 1 1 d . . . B8 B 0.7850(10) -0.2292(10) -0.2955(5) 0.0073(12) Uani 1 1 d . . . B9 B 0.0490(11) 1.1521(11) 0.1818(6) 0.0086(13) Uani 1 1 d . . . B10 B 0.9700(10) 0.8354(11) 0.2705(6) 0.0082(13) Uani 1 1 d . . . O1 O 0.0258(6) 0.3792(6) 0.2105(3) 0.0075(8) Uani 1 1 d . . . O2 O 0.3286(7) 0.2110(7) 0.4331(4) 0.0210(10) Uani 1 1 d . . . O3 O 0.9122(6) 0.2773(6) 0.6639(3) 0.0064(8) Uani 1 1 d . . . O4 O 0.9830(6) -0.4259(6) -0.2427(4) 0.0090(9) Uani 1 1 d . . . O5 O 0.8185(7) -0.4394(6) 0.0333(3) 0.0120(8) Uani 1 1 d . . . O6 O 0.7893(6) -0.0081(7) -0.2747(3) 0.0089(8) Uani 1 1 d . . . O7 O 0.9757(6) 0.1531(6) 0.0610(3) 0.0113(8) Uani 1 1 d . . . O8 O 0.8785(6) 0.7808(6) 0.3817(3) 0.0099(8) Uani 1 1 d . . . O9 O 0.2258(6) 0.6794(6) 0.2588(4) 0.0102(8) Uani 1 1 d . . . O10 O 0.5717(6) 0.7812(6) 0.7609(3) 0.0094(8) Uani 1 1 d . . . O11 O 0.7883(6) 0.7382(7) 0.5750(3) 0.0122(8) Uani 1 1 d . . . O12 O 0.9159(6) 0.0842(6) 0.2693(4) 0.0085(8) Uani 1 1 d . . . O13 O 0.4668(7) 0.4652(7) 0.5148(4) 0.0239(10) Uani 1 1 d . . . O14 O 0.9698(6) -0.0214(6) 0.5294(3) 0.0109(8) Uani 1 1 d . . . O15 O 0.2019(6) 0.8740(6) 0.7002(4) 0.0123(8) Uani 1 1 d . . . O16 O 0.6143(6) 0.5951(7) 0.2255(4) 0.0123(9) Uani 1 1 d . . . O17 O 0.8817(7) 0.3027(6) -0.1285(3) 0.0125(8) Uani 1 1 d . . . O18 O 0.2611(6) 0.1819(6) 0.7687(4) 0.0134(9) Uani 1 1 d . . . O19 O 0.8464(6) -0.1992(6) 0.1756(3) 0.0078(8) Uani 1 1 d . . . O20 O 1.3256(7) -0.3727(7) -0.0482(4) 0.0206(10) Uani 1 1 d . . . O21 O 0.3063(6) 0.9809(6) 0.1831(4) 0.0114(8) Uani 1 1 d . . . O22 O 0.4924(7) 0.2095(7) -0.0013(4) 0.0202(9) Uani 1 1 d . . . H1 H 0.3976 0.3361 0.4740 0.024 Uiso 1 1 d R . . H2 H 0.3370 0.5980 0.5183 0.024 Uiso 1 1 d R . . H3 H 0.2987 0.1348 0.4948 0.024 Uiso 1 1 d R . . H4 H 1.4098 -0.5827 -0.0245 0.024 Uiso 1 1 d R . . H5 H 1.3210 -0.2815 0.0123 0.024 Uiso 1 1 d R . . H6 H 0.3585 0.1964 0.0149 0.024 Uiso 1 1 d R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sr1 0.0077(2) 0.0095(3) 0.0196(3) 0.0001(2) -0.0031(2) -0.0025(2) Sr2 0.0088(3) 0.0090(3) 0.0188(3) -0.0013(2) 0.0006(2) -0.0031(2) Sr3 0.0136(3) 0.0105(2) 0.0101(3) -0.00024(19) -0.0010(2) -0.0061(2) Sr4 0.0147(3) 0.0103(2) 0.0107(3) 0.0014(2) -0.0033(2) -0.0050(2) B1 0.011(3) 0.010(3) 0.011(3) -0.001(3) 0.003(3) -0.006(3) B2 0.004(3) 0.004(3) 0.011(3) -0.001(2) 0.001(2) 0.000(2) B3 0.007(3) 0.005(3) 0.015(3) -0.001(3) -0.007(2) 0.000(2) B4 0.007(3) 0.015(3) 0.007(3) 0.002(3) -0.003(2) -0.005(3) B5 0.011(3) 0.006(3) 0.010(3) -0.004(2) -0.001(2) 0.002(3) B6 0.013(3) 0.006(3) 0.014(3) 0.002(3) -0.007(3) -0.001(3) B7 0.008(3) 0.008(3) 0.010(3) -0.002(2) -0.001(2) -0.003(3) B8 0.006(3) 0.003(3) 0.010(3) 0.000(2) -0.005(2) 0.001(2) B9 0.008(3) 0.012(3) 0.007(3) 0.005(3) -0.004(2) -0.005(3) B10 0.008(3) 0.008(3) 0.007(3) 0.001(2) -0.003(2) -0.003(3) O1 0.008(2) 0.007(2) 0.006(2) -0.0003(15) -0.0037(16) -0.0014(17) O2 0.016(2) 0.030(3) 0.018(3) 0.003(2) -0.0079(19) -0.012(2) O3 0.0068(19) 0.004(2) 0.009(2) 0.0010(16) -0.0030(16) -0.0028(16) O4 0.006(2) 0.006(2) 0.012(2) -0.0012(16) -0.0025(16) -0.0010(17) O5 0.018(2) 0.010(2) 0.008(2) 0.0011(16) -0.0050(16) -0.0066(17) O6 0.0077(19) 0.0083(19) 0.009(2) 0.0033(16) -0.0040(16) -0.0025(17) O7 0.019(2) 0.0088(19) 0.005(2) 0.0026(15) -0.0063(16) -0.0058(17) O8 0.015(2) 0.009(2) 0.007(2) -0.0012(16) -0.0017(16) -0.0063(17) O9 0.0065(19) 0.0070(19) 0.017(2) 0.0031(16) -0.0019(16) -0.0028(16) O10 0.0071(18) 0.0067(19) 0.014(2) 0.0037(16) -0.0029(16) -0.0031(16) O11 0.016(2) 0.015(2) 0.007(2) -0.0001(16) -0.0009(16) -0.0084(17) O12 0.0082(18) 0.0047(19) 0.013(2) -0.0006(16) -0.0004(17) -0.0032(16) O13 0.013(2) 0.026(2) 0.027(3) 0.001(2) -0.0032(19) -0.005(2) O14 0.016(2) 0.011(2) 0.008(2) -0.0005(16) 0.0004(16) -0.0078(17) O15 0.0065(19) 0.0083(19) 0.021(2) 0.0032(16) -0.0082(16) -0.0021(16) O16 0.0050(19) 0.009(2) 0.022(2) 0.0030(17) -0.0019(16) -0.0024(17) O17 0.017(2) 0.012(2) 0.009(2) -0.0002(17) -0.0026(16) -0.0070(18) O18 0.0083(19) 0.010(2) 0.022(2) 0.0016(17) -0.0042(17) -0.0045(17) O19 0.0094(19) 0.0056(19) 0.009(2) 0.0024(16) -0.0057(16) -0.0034(16) O20 0.016(2) 0.020(2) 0.021(3) -0.0021(19) -0.0046(18) -0.0042(19) O21 0.0050(18) 0.0071(19) 0.019(2) 0.0022(16) -0.0014(16) -0.0009(16) O22 0.014(2) 0.017(2) 0.026(3) 0.0039(19) -0.0024(18) -0.0042(19) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sr1 O21 2.497(4) 1_545 ? Sr1 O2 2.540(4) . ? Sr1 O22 2.550(4) . ? Sr1 O9 2.554(4) . ? Sr1 O12 2.598(4) . ? Sr1 O1 2.652(4) . ? Sr1 O19 2.737(4) . ? Sr1 O16 2.841(4) . ? Sr1 B10 3.077(6) 1_545 ? Sr1 B9 3.178(6) 1_545 ? Sr1 B9 3.463(6) 1_645 ? Sr1 Sr3 4.1379(8) 1_455 ? Sr1 H1 2.8777 . ? Sr1 H6 2.6031 . ? Sr2 O18 2.564(4) . ? Sr2 O13 2.581(5) . ? Sr2 O6 2.601(4) 1_556 ? Sr2 O15 2.612(4) . ? Sr2 O20 2.615(4) 1_466 ? Sr2 O3 2.641(3) . ? Sr2 O10 2.679(4) . ? Sr2 O4 2.835(3) 1_466 ? Sr2 O17 2.883(4) 1_556 ? Sr2 B1 3.082(6) 1_565 ? Sr2 B3 3.117(6) 1_645 ? Sr2 O22 3.181(4) 1_556 ? Sr2 H2 2.7632 . ? Sr3 O2 2.557(4) 1_655 ? Sr3 O13 2.581(4) . ? Sr3 O14 2.606(4) . ? Sr3 O11 2.631(4) . ? Sr3 O3 2.637(4) . ? Sr3 O8 2.646(4) . ? Sr3 O1 2.661(4) 1_655 ? Sr3 O12 2.665(4) . ? Sr3 O16 2.960(4) . ? Sr3 B6 3.071(6) 1_565 ? Sr3 B9 3.156(7) 1_645 ? Sr3 B3 3.235(7) 1_645 ? Sr4 O20 2.492(4) . ? Sr4 O22 2.511(4) . ? Sr4 O5 2.521(4) . ? Sr4 O7 2.541(3) . ? Sr4 O6 2.580(4) . ? Sr4 O19 2.704(4) . ? Sr4 O4 2.750(4) . ? Sr4 O17 2.821(4) . ? Sr4 B4 3.108(6) 1_565 ? Sr4 O15 3.269(4) 1_644 ? Sr4 O10 3.300(4) 1_544 ? Sr4 B3 3.405(7) 1_644 ? Sr4 H5 2.6339 . ? B1 O18 1.366(7) . ? B1 O15 1.368(7) 1_545 ? B1 O10 1.375(7) 1_545 ? B1 Sr2 3.082(6) 1_545 ? B2 O4 1.442(7) . ? B2 O3 1.481(7) 1_544 ? B2 O18 1.487(6) 1_644 ? B2 O17 1.495(7) 1_545 ? B2 Sr2 3.264(6) 1_544 ? B2 Sr2 3.330(6) 1_644 ? B3 O6 1.449(7) 1_466 ? B3 O3 1.475(7) 1_465 ? B3 O15 1.484(7) . ? B3 O14 1.496(7) 1_465 ? B3 Sr2 3.117(6) 1_465 ? B3 Sr3 3.235(7) 1_465 ? B3 Sr4 3.405(7) 1_466 ? B4 O5 1.337(7) . ? B4 O17 1.375(7) 1_545 ? B4 O7 1.381(7) 1_545 ? B4 Sr4 3.108(6) 1_545 ? B5 O21 1.358(7) . ? B5 O9 1.362(7) . ? B5 O16 1.386(7) . ? B6 O14 1.358(7) . ? B6 O11 1.360(7) 1_545 ? B6 O8 1.369(7) 1_545 ? B6 Sr3 3.071(6) 1_545 ? B7 O19 1.453(7) . ? B7 O1 1.456(7) 1_645 ? B7 O16 1.493(7) 1_545 ? B7 O5 1.517(7) . ? B7 Sr3 3.293(6) 1_545 ? B8 O10 1.457(7) 1_544 ? B8 O4 1.462(7) . ? B8 O6 1.478(7) . ? B8 O11 1.484(7) 1_544 ? B9 O1 1.454(7) 1_565 ? B9 O12 1.466(7) 1_465 ? B9 O7 1.478(7) 1_465 ? B9 O21 1.501(7) . ? B9 Sr3 3.156(7) 1_465 ? B9 Sr1 3.178(6) 1_565 ? B9 Sr1 3.463(6) 1_465 ? B10 O8 1.462(7) . ? B10 O19 1.468(7) 1_565 ? B10 O9 1.473(7) 1_655 ? B10 O12 1.483(7) 1_565 ? B10 Sr1 3.077(6) 1_565 ? O1 B9 1.454(7) 1_545 ? O1 B7 1.456(7) 1_465 ? O1 Sr3 2.661(4) 1_455 ? O2 Sr3 2.557(4) 1_455 ? O2 H1 1.2153 . ? O2 H3 0.9087 . ? O3 B3 1.475(7) 1_645 ? O3 B2 1.481(7) 1_566 ? O4 Sr2 2.835(3) 1_644 ? O6 B3 1.449(7) 1_644 ? O6 Sr2 2.601(4) 1_554 ? O7 B4 1.381(7) 1_565 ? O7 B9 1.478(7) 1_645 ? O8 B6 1.369(7) 1_565 ? O9 B10 1.473(7) 1_455 ? O10 B1 1.375(7) 1_565 ? O10 B8 1.457(7) 1_566 ? O10 Sr4 3.300(4) 1_566 ? O11 B6 1.360(7) 1_565 ? O11 B8 1.484(7) 1_566 ? O12 B9 1.466(7) 1_645 ? O12 B10 1.483(7) 1_545 ? O13 H1 1.2380 . ? O13 H2 0.8707 . ? O14 B3 1.496(7) 1_645 ? O15 B1 1.368(7) 1_565 ? O15 Sr4 3.269(4) 1_466 ? O16 B7 1.493(7) 1_565 ? O17 B4 1.375(7) 1_565 ? O17 B2 1.495(7) 1_565 ? O17 Sr2 2.883(4) 1_554 ? O18 B2 1.487(6) 1_466 ? O19 B10 1.468(7) 1_545 ? O20 Sr2 2.615(4) 1_644 ? O20 H4 1.2335 . ? O20 H5 0.9076 . ? O21 Sr1 2.497(4) 1_565 ? O22 Sr2 3.181(4) 1_554 ? O22 H6 0.9202 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O21 Sr1 O2 81.27(13) 1_545 . ? O21 Sr1 O22 74.05(13) 1_545 . ? O2 Sr1 O22 153.76(13) . . ? O21 Sr1 O9 122.04(11) 1_545 . ? O2 Sr1 O9 83.60(13) . . ? O22 Sr1 O9 101.91(13) . . ? O21 Sr1 O12 123.89(12) 1_545 . ? O2 Sr1 O12 96.79(13) . . ? O22 Sr1 O12 104.21(13) . . ? O9 Sr1 O12 113.28(11) . . ? O21 Sr1 O1 54.45(11) 1_545 . ? O2 Sr1 O1 74.53(12) . . ? O22 Sr1 O1 83.83(12) . . ? O9 Sr1 O1 67.60(11) . . ? O12 Sr1 O1 171.23(12) . . ? O21 Sr1 O19 72.95(11) 1_545 . ? O2 Sr1 O19 104.33(12) . . ? O22 Sr1 O19 77.02(12) . . ? O9 Sr1 O19 164.41(10) . . ? O12 Sr1 O19 53.08(10) . . ? O1 Sr1 O19 127.17(11) . . ? O21 Sr1 O16 166.63(12) 1_545 . ? O2 Sr1 O16 106.98(12) . . ? O22 Sr1 O16 95.84(12) . . ? O9 Sr1 O16 50.53(10) . . ? O12 Sr1 O16 66.50(11) . . ? O1 Sr1 O16 116.73(11) . . ? O19 Sr1 O16 113.90(10) . . ? O21 Sr1 B10 95.23(14) 1_545 1_545 ? O2 Sr1 B10 90.82(15) . 1_545 ? O22 Sr1 B10 100.03(15) . 1_545 ? O9 Sr1 B10 140.66(14) . 1_545 ? O12 Sr1 B10 28.74(13) . 1_545 ? O1 Sr1 B10 147.47(14) . 1_545 ? O19 Sr1 B10 28.49(13) . 1_545 ? O16 Sr1 B10 95.15(14) . 1_545 ? O21 Sr1 B9 27.46(14) 1_545 1_545 ? O2 Sr1 B9 77.21(15) . 1_545 ? O22 Sr1 B9 76.78(14) . 1_545 ? O9 Sr1 B9 94.59(14) . 1_545 ? O12 Sr1 B9 150.84(14) . 1_545 ? O1 Sr1 B9 27.01(14) . 1_545 ? O19 Sr1 B9 100.22(14) . 1_545 ? O16 Sr1 B9 142.64(14) . 1_545 ? B10 Sr1 B9 122.13(16) 1_545 1_545 ? O21 Sr1 B9 131.51(14) 1_545 1_645 ? O2 Sr1 B9 117.81(14) . 1_645 ? O22 Sr1 B9 85.89(14) . 1_645 ? O9 Sr1 B9 104.92(13) . 1_645 ? O12 Sr1 B9 22.77(14) . 1_645 ? O1 Sr1 B9 165.61(14) . 1_645 ? O19 Sr1 B9 59.54(13) . 1_645 ? O16 Sr1 B9 54.40(13) . 1_645 ? B10 Sr1 B9 44.86(15) 1_545 1_645 ? B9 Sr1 B9 156.2(2) 1_545 1_645 ? O21 Sr1 Sr3 66.22(9) 1_545 1_455 ? O2 Sr1 Sr3 35.86(9) . 1_455 ? O22 Sr1 Sr3 122.15(9) . 1_455 ? O9 Sr1 Sr3 69.12(8) . 1_455 ? O12 Sr1 Sr3 132.52(9) . 1_455 ? O1 Sr1 Sr3 38.92(8) . 1_455 ? O19 Sr1 Sr3 124.88(8) . 1_455 ? O16 Sr1 Sr3 114.27(8) . 1_455 ? B10 Sr1 Sr3 123.21(12) 1_545 1_455 ? B9 Sr1 Sr3 48.98(12) 1_545 1_455 ? B9 Sr1 Sr3 151.83(11) 1_645 1_455 ? O21 Sr1 H1 106.2 1_545 . ? O2 Sr1 H1 24.9 . . ? O22 Sr1 H1 171.2 . . ? O9 Sr1 H1 70.3 . . ? O12 Sr1 H1 83.1 . . ? O1 Sr1 H1 89.3 . . ? O19 Sr1 H1 111.6 . . ? O16 Sr1 H1 82.4 . . ? B10 Sr1 H1 88.7 1_545 . ? B9 Sr1 H1 99.3 1_545 . ? B9 Sr1 H1 99.9 1_645 . ? Sr3 Sr1 H1 51.9 1_455 . ? O21 Sr1 H6 57.0 1_545 . ? O2 Sr1 H6 133.4 . . ? O22 Sr1 H6 20.5 . . ? O9 Sr1 H6 100.7 . . ? O12 Sr1 H6 122.2 . . ? O1 Sr1 H6 65.1 . . ? O19 Sr1 H6 83.7 . . ? O16 Sr1 H6 111.2 . . ? B10 Sr1 H6 110.9 1_545 . ? B9 Sr1 H6 56.3 1_545 . ? B9 Sr1 H6 105.9 1_645 . ? Sr3 Sr1 H6 102.3 1_455 . ? H1 Sr1 H6 154.1 . . ? O18 Sr2 O13 97.56(13) . . ? O18 Sr2 O6 72.30(11) . 1_556 ? O13 Sr2 O6 90.98(13) . 1_556 ? O18 Sr2 O15 115.72(11) . . ? O13 Sr2 O15 74.34(13) . . ? O6 Sr2 O15 163.79(12) 1_556 . ? O18 Sr2 O20 94.54(13) . 1_466 ? O13 Sr2 O20 149.47(13) . 1_466 ? O6 Sr2 O20 119.44(13) 1_556 1_466 ? O15 Sr2 O20 75.16(13) . 1_466 ? O18 Sr2 O3 125.85(11) . . ? O13 Sr2 O3 74.06(12) . . ? O6 Sr2 O3 54.92(10) 1_556 . ? O15 Sr2 O3 112.98(11) . . ? O20 Sr2 O3 119.85(12) 1_466 . ? O18 Sr2 O10 161.60(12) . . ? O13 Sr2 O10 92.15(13) . . ? O6 Sr2 O10 123.32(11) 1_556 . ? O15 Sr2 O10 52.22(11) . . ? O20 Sr2 O10 69.76(12) 1_466 . ? O3 Sr2 O10 71.87(10) . . ? O18 Sr2 O4 50.61(11) . 1_466 ? O13 Sr2 O4 89.95(12) . 1_466 ? O6 Sr2 O4 122.45(10) 1_556 1_466 ? O15 Sr2 O4 65.48(10) . 1_466 ? O20 Sr2 O4 76.38(12) 1_466 1_466 ? O3 Sr2 O4 163.37(11) . 1_466 ? O10 Sr2 O4 114.13(10) . 1_466 ? O18 Sr2 O17 118.69(12) . 1_556 ? O13 Sr2 O17 123.71(12) . 1_556 ? O6 Sr2 O17 64.71(11) 1_556 1_556 ? O15 Sr2 O17 117.74(11) . 1_556 ? O20 Sr2 O17 72.74(11) 1_466 1_556 ? O3 Sr2 O17 50.09(11) . 1_556 ? O10 Sr2 O17 66.97(11) . 1_556 ? O4 Sr2 O17 146.27(12) 1_466 1_556 ? O18 Sr2 B1 138.76(14) . 1_565 ? O13 Sr2 B1 85.71(15) . 1_565 ? O6 Sr2 B1 148.94(14) 1_556 1_565 ? O15 Sr2 B1 26.17(13) . 1_565 ? O20 Sr2 B1 67.03(15) 1_466 1_565 ? O3 Sr2 B1 94.70(13) . 1_565 ? O10 Sr2 B1 26.46(13) . 1_565 ? O4 Sr2 B1 88.47(13) 1_466 1_565 ? O17 Sr2 B1 91.74(14) 1_556 1_565 ? O18 Sr2 B3 97.76(14) . 1_645 ? O13 Sr2 B3 77.22(15) . 1_645 ? O6 Sr2 B3 27.52(14) 1_556 1_645 ? O15 Sr2 B3 138.20(15) . 1_645 ? O20 Sr2 B3 128.67(14) 1_466 1_645 ? O3 Sr2 B3 28.17(13) . 1_645 ? O10 Sr2 B3 99.62(13) . 1_645 ? O4 Sr2 B3 144.37(13) 1_466 1_645 ? O17 Sr2 B3 57.65(13) 1_556 1_645 ? B1 Sr2 B3 122.83(16) 1_565 1_645 ? O18 Sr2 O22 65.36(12) . 1_556 ? O13 Sr2 O22 159.28(13) . 1_556 ? O6 Sr2 O22 73.13(11) 1_556 1_556 ? O15 Sr2 O22 122.73(11) . 1_556 ? O20 Sr2 O22 48.90(12) 1_466 1_556 ? O3 Sr2 O22 105.64(11) . 1_556 ? O10 Sr2 O22 107.59(11) . 1_556 ? O4 Sr2 O22 87.67(11) 1_466 1_556 ? O17 Sr2 O22 61.78(11) 1_556 1_556 ? B1 Sr2 O22 114.78(14) 1_565 1_556 ? B3 Sr2 O22 92.94(14) 1_645 1_556 ? O18 Sr2 H2 98.4 . . ? O13 Sr2 H2 18.3 . . ? O6 Sr2 H2 108.8 1_556 . ? O15 Sr2 H2 57.4 . . ? O20 Sr2 H2 131.8 1_466 . ? O3 Sr2 H2 88.5 . . ? O10 Sr2 H2 86.0 . . ? O4 Sr2 H2 76.8 1_466 . ? O17 Sr2 H2 135.1 1_556 . ? B1 Sr2 H2 72.9 1_565 . ? B3 Sr2 H2 95.3 1_645 . ? O22 Sr2 H2 162.7 1_556 . ? O2 Sr3 O13 158.06(15) 1_655 . ? O2 Sr3 O14 83.64(12) 1_655 . ? O13 Sr3 O14 78.89(13) . . ? O2 Sr3 O11 95.01(12) 1_655 . ? O13 Sr3 O11 82.48(12) . . ? O14 Sr3 O11 119.88(12) . . ? O2 Sr3 O3 84.88(12) 1_655 . ? O13 Sr3 O3 74.12(12) . . ? O14 Sr3 O3 53.74(11) . . ? O11 Sr3 O3 66.24(11) . . ? O2 Sr3 O8 84.99(12) 1_655 . ? O13 Sr3 O8 109.36(13) . . ? O14 Sr3 O8 164.59(11) . . ? O11 Sr3 O8 50.94(11) . . ? O3 Sr3 O8 114.85(10) . . ? O2 Sr3 O1 74.11(12) 1_655 1_655 ? O13 Sr3 O1 125.91(12) . 1_655 ? O14 Sr3 O1 117.05(11) . 1_655 ? O11 Sr3 O1 120.14(11) . 1_655 ? O3 Sr3 O1 158.30(11) . 1_655 ? O8 Sr3 O1 69.35(11) . 1_655 ? O2 Sr3 O12 92.38(12) 1_655 . ? O13 Sr3 O12 93.87(12) . . ? O14 Sr3 O12 69.65(12) . . ? O11 Sr3 O12 168.53(12) . . ? O3 Sr3 O12 123.31(11) . . ? O8 Sr3 O12 121.29(12) . . ? O1 Sr3 O12 53.86(11) 1_655 . ? O2 Sr3 O16 122.31(12) 1_655 . ? O13 Sr3 O16 79.16(12) . . ? O14 Sr3 O16 126.51(11) . . ? O11 Sr3 O16 104.62(11) . . ? O3 Sr3 O16 152.60(10) . . ? O8 Sr3 O16 68.64(11) . . ? O1 Sr3 O16 48.98(10) 1_655 . ? O12 Sr3 O16 63.95(11) . . ? O2 Sr3 B6 83.45(15) 1_655 1_565 ? O13 Sr3 B6 101.94(15) . 1_565 ? O14 Sr3 B6 140.97(15) . 1_565 ? O11 Sr3 B6 26.17(14) . 1_565 ? O3 Sr3 B6 88.49(14) . 1_565 ? O8 Sr3 B6 26.40(15) . 1_565 ? O1 Sr3 B6 94.34(15) 1_655 1_565 ? O12 Sr3 B6 147.54(15) . 1_565 ? O16 Sr3 B6 91.21(14) . 1_565 ? O2 Sr3 B9 77.41(14) 1_655 1_645 ? O13 Sr3 B9 115.82(15) . 1_645 ? O14 Sr3 B9 91.06(14) . 1_645 ? O11 Sr3 B9 147.44(14) . 1_645 ? O3 Sr3 B9 142.32(14) . 1_645 ? O8 Sr3 B9 96.59(14) . 1_645 ? O1 Sr3 B9 27.30(14) 1_655 1_645 ? O12 Sr3 B9 27.56(13) . 1_645 ? O16 Sr3 B9 57.23(13) . 1_645 ? B6 Sr3 B9 121.53(17) 1_565 1_645 ? O2 Sr3 B3 83.34(14) 1_655 1_645 ? O13 Sr3 B3 75.06(15) . 1_645 ? O14 Sr3 B3 27.04(13) . 1_645 ? O11 Sr3 B3 92.91(13) . 1_645 ? O3 Sr3 B3 26.70(12) . 1_645 ? O8 Sr3 B3 140.66(13) . 1_645 ? O1 Sr3 B3 140.88(13) 1_655 1_645 ? O12 Sr3 B3 96.66(13) . 1_645 ? O16 Sr3 B3 146.50(13) . 1_645 ? B6 Sr3 B3 114.67(16) 1_565 1_645 ? B9 Sr3 B3 117.09(16) 1_645 1_645 ? O20 Sr4 O22 156.55(14) . . ? O20 Sr4 O5 91.21(13) . . ? O22 Sr4 O5 95.68(12) . . ? O20 Sr4 O7 81.45(12) . . ? O22 Sr4 O7 76.05(13) . . ? O5 Sr4 O7 123.54(12) . . ? O20 Sr4 O6 110.31(13) . . ? O22 Sr4 O6 86.11(13) . . ? O5 Sr4 O6 117.95(12) . . ? O7 Sr4 O6 117.02(12) . . ? O20 Sr4 O19 88.12(12) . . ? O22 Sr4 O19 78.28(12) . . ? O5 Sr4 O19 53.29(11) . . ? O7 Sr4 O19 70.49(11) . . ? O6 Sr4 O19 160.57(11) . . ? O20 Sr4 O4 79.98(12) . . ? O22 Sr4 O4 123.44(12) . . ? O5 Sr4 O4 75.81(11) . . ? O7 Sr4 O4 153.41(11) . . ? O6 Sr4 O4 53.78(12) . . ? O19 Sr4 O4 127.43(11) . . ? O20 Sr4 O17 99.36(13) . . ? O22 Sr4 O17 71.45(12) . . ? O5 Sr4 O17 166.67(11) . . ? O7 Sr4 O17 51.13(11) . . ? O6 Sr4 O17 65.89(11) . . ? O19 Sr4 O17 118.56(10) . . ? O4 Sr4 O17 113.87(11) . . ? O20 Sr4 B4 95.30(14) . 1_565 ? O22 Sr4 B4 66.71(14) . 1_565 ? O5 Sr4 B4 145.12(14) . 1_565 ? O7 Sr4 B4 25.88(14) . 1_565 ? O6 Sr4 B4 91.71(15) . 1_565 ? O19 Sr4 B4 92.65(13) . 1_565 ? O4 Sr4 B4 139.07(14) . 1_565 ? O17 Sr4 B4 26.25(14) . 1_565 ? O20 Sr4 O15 65.59(12) . 1_644 ? O22 Sr4 O15 123.34(12) . 1_644 ? O5 Sr4 O15 130.41(10) . 1_644 ? O7 Sr4 O15 96.89(10) . 1_644 ? O6 Sr4 O15 46.78(10) . 1_644 ? O19 Sr4 O15 152.64(10) . 1_644 ? O4 Sr4 O15 57.98(9) . 1_644 ? O17 Sr4 O15 62.17(10) . 1_644 ? B4 Sr4 O15 82.87(13) 1_565 1_644 ? O20 Sr4 O10 124.17(11) . 1_544 ? O22 Sr4 O10 79.27(11) . 1_544 ? O5 Sr4 O10 73.00(11) . 1_544 ? O7 Sr4 O10 151.36(10) . 1_544 ? O6 Sr4 O10 46.35(10) . 1_544 ? O19 Sr4 O10 118.25(10) . 1_544 ? O4 Sr4 O10 44.46(9) . 1_544 ? O17 Sr4 O10 106.95(10) . 1_544 ? B4 Sr4 O10 128.01(13) 1_565 1_544 ? O15 Sr4 O10 84.67(9) 1_644 1_544 ? O20 Sr4 B3 91.17(14) . 1_644 ? O22 Sr4 B3 99.95(14) . 1_644 ? O5 Sr4 B3 133.86(13) . 1_644 ? O7 Sr4 B3 102.36(13) . 1_644 ? O6 Sr4 B3 23.20(13) . 1_644 ? O19 Sr4 B3 172.84(12) . 1_644 ? O4 Sr4 B3 59.34(13) . 1_644 ? O17 Sr4 B3 54.56(12) . 1_644 ? B4 Sr4 B3 80.33(15) 1_565 1_644 ? O15 Sr4 B3 25.59(11) 1_644 1_644 ? O10 Sr4 B3 67.83(11) 1_544 1_644 ? O20 Sr4 H5 20.2 . . ? O22 Sr4 H5 136.4 . . ? O5 Sr4 H5 96.8 . . ? O7 Sr4 H5 62.3 . . ? O6 Sr4 H5 123.0 . . ? O19 Sr4 H5 76.4 . . ? O4 Sr4 H5 100.1 . . ? O17 Sr4 H5 90.5 . . ? B4 Sr4 H5 79.6 1_565 . ? O15 Sr4 H5 76.2 1_644 . ? O10 Sr4 H5 144.3 1_544 . ? B3 Sr4 H5 100.8 1_644 . ? O18 B1 O15 120.3(5) . 1_545 ? O18 B1 O10 123.3(5) . 1_545 ? O15 B1 O10 116.2(5) 1_545 1_545 ? O18 B1 Sr2 165.2(4) . 1_545 ? O15 B1 Sr2 57.4(3) 1_545 1_545 ? O10 B1 Sr2 60.2(3) 1_545 1_545 ? O4 B2 O3 115.1(5) . 1_544 ? O4 B2 O18 104.8(4) . 1_644 ? O3 B2 O18 110.1(4) 1_544 1_644 ? O4 B2 O17 114.4(4) . 1_545 ? O3 B2 O17 104.2(4) 1_544 1_545 ? O18 B2 O17 108.3(4) 1_644 1_545 ? O4 B2 Sr2 104.4(3) . 1_544 ? O3 B2 Sr2 52.6(2) 1_544 1_544 ? O18 B2 Sr2 150.6(3) 1_644 1_544 ? O17 B2 Sr2 62.0(2) 1_545 1_544 ? O4 B2 Sr2 57.7(2) . 1_644 ? O3 B2 Sr2 124.7(3) 1_544 1_644 ? O18 B2 Sr2 47.2(2) 1_644 1_644 ? O17 B2 Sr2 129.6(3) 1_545 1_644 ? Sr2 B2 Sr2 160.6(2) 1_544 1_644 ? O6 B3 O3 111.5(4) 1_466 1_465 ? O6 B3 O15 110.3(5) 1_466 . ? O3 B3 O15 110.5(4) 1_465 . ? O6 B3 O14 110.4(4) 1_466 1_465 ? O3 B3 O14 105.8(5) 1_465 1_465 ? O15 B3 O14 108.2(4) . 1_465 ? O6 B3 Sr2 56.0(2) 1_466 1_465 ? O3 B3 Sr2 57.7(2) 1_465 1_465 ? O15 B3 Sr2 141.9(4) . 1_465 ? O14 B3 Sr2 109.9(3) 1_465 1_465 ? O6 B3 Sr3 127.0(4) 1_466 1_465 ? O3 B3 Sr3 53.4(2) 1_465 1_465 ? O15 B3 Sr3 122.7(4) . 1_465 ? O14 B3 Sr3 52.4(3) 1_465 1_465 ? Sr2 B3 Sr3 81.52(15) 1_465 1_465 ? O6 B3 Sr4 44.5(3) 1_466 1_466 ? O3 B3 Sr4 105.6(3) 1_465 1_466 ? O15 B3 Sr4 72.1(3) . 1_466 ? O14 B3 Sr4 146.0(4) 1_465 1_466 ? Sr2 B3 Sr4 76.88(14) 1_465 1_466 ? Sr3 B3 Sr4 156.3(2) 1_465 1_466 ? O5 B4 O17 124.0(5) . 1_545 ? O5 B4 O7 120.6(5) . 1_545 ? O17 B4 O7 115.2(5) 1_545 1_545 ? O5 B4 Sr4 157.6(4) . 1_545 ? O17 B4 Sr4 65.1(3) 1_545 1_545 ? O7 B4 Sr4 53.4(3) 1_545 1_545 ? O21 B5 O9 122.5(5) . . ? O21 B5 O16 122.5(5) . . ? O9 B5 O16 115.0(5) . . ? O14 B6 O11 123.7(5) . 1_545 ? O14 B6 O8 123.8(5) . 1_545 ? O11 B6 O8 112.5(5) 1_545 1_545 ? O14 B6 Sr3 157.0(4) . 1_545 ? O11 B6 Sr3 58.5(3) 1_545 1_545 ? O8 B6 Sr3 59.2(3) 1_545 1_545 ? O19 B7 O1 114.4(5) . 1_645 ? O19 B7 O16 114.8(4) . 1_545 ? O1 B7 O16 105.4(4) 1_645 1_545 ? O19 B7 O5 104.5(4) . . ? O1 B7 O5 110.3(4) 1_645 . ? O16 B7 O5 107.4(4) 1_545 . ? O19 B7 Sr3 104.1(3) . 1_545 ? O1 B7 Sr3 52.1(3) 1_645 1_545 ? O16 B7 Sr3 64.0(3) 1_545 1_545 ? O5 B7 Sr3 151.0(3) . 1_545 ? O10 B8 O4 106.9(4) 1_544 . ? O10 B8 O6 110.2(4) 1_544 . ? O4 B8 O6 110.5(4) . . ? O10 B8 O11 109.0(4) 1_544 1_544 ? O4 B8 O11 111.8(4) . 1_544 ? O6 B8 O11 108.6(4) . 1_544 ? O1 B9 O12 111.4(5) 1_565 1_465 ? O1 B9 O7 110.5(5) 1_565 1_465 ? O12 B9 O7 111.1(4) 1_465 1_465 ? O1 B9 O21 105.9(4) 1_565 . ? O12 B9 O21 109.9(5) 1_465 . ? O7 B9 O21 107.9(5) 1_465 . ? O1 B9 Sr3 57.0(3) 1_565 1_465 ? O12 B9 Sr3 57.2(3) 1_465 1_465 ? O7 B9 Sr3 144.8(4) 1_465 1_465 ? O21 B9 Sr3 107.3(3) . 1_465 ? O1 B9 Sr1 55.9(2) 1_565 1_565 ? O12 B9 Sr1 127.9(4) 1_465 1_565 ? O7 B9 Sr1 120.7(3) 1_465 1_565 ? O21 B9 Sr1 50.1(2) . 1_565 ? Sr3 B9 Sr1 81.57(15) 1_465 1_565 ? O1 B9 Sr1 103.5(3) 1_565 1_465 ? O12 B9 Sr1 43.3(2) 1_465 1_465 ? O7 B9 Sr1 75.3(3) 1_465 1_465 ? O21 B9 Sr1 146.7(4) . 1_465 ? Sr3 B9 Sr1 76.46(13) 1_465 1_465 ? Sr1 B9 Sr1 156.2(2) 1_565 1_465 ? O8 B10 O19 106.7(4) . 1_565 ? O8 B10 O9 108.1(4) . 1_655 ? O19 B10 O9 112.9(4) 1_565 1_655 ? O8 B10 O12 110.5(5) . 1_565 ? O19 B10 O12 108.0(5) 1_565 1_565 ? O9 B10 O12 110.6(4) 1_655 1_565 ? O8 B10 Sr1 91.0(3) . 1_565 ? O19 B10 Sr1 62.8(3) 1_565 1_565 ? O9 B10 Sr1 160.6(4) 1_655 1_565 ? O12 B10 Sr1 57.4(2) 1_565 1_565 ? B9 O1 B7 117.9(4) 1_545 1_465 ? B9 O1 Sr1 97.1(3) 1_545 . ? B7 O1 Sr1 134.4(3) 1_465 . ? B9 O1 Sr3 95.7(3) 1_545 1_455 ? B7 O1 Sr3 102.3(3) 1_465 1_455 ? Sr1 O1 Sr3 102.31(13) . 1_455 ? Sr1 O2 Sr3 108.55(16) . 1_455 ? Sr1 O2 H1 93.3 . . ? Sr3 O2 H1 115.8 1_455 . ? Sr1 O2 H3 153.9 . . ? Sr3 O2 H3 77.4 1_455 . ? H1 O2 H3 107.2 . . ? B3 O3 B2 116.4(4) 1_645 1_566 ? B3 O3 Sr3 99.9(3) 1_645 . ? B2 O3 Sr3 134.1(3) 1_566 . ? B3 O3 Sr2 94.1(3) 1_645 . ? B2 O3 Sr2 100.9(3) 1_566 . ? Sr3 O3 Sr2 103.60(12) . . ? B2 O4 B8 122.2(4) . . ? B2 O4 Sr4 127.4(3) . . ? B8 O4 Sr4 85.2(3) . . ? B2 O4 Sr2 96.8(3) . 1_644 ? B8 O4 Sr2 131.8(3) . 1_644 ? Sr4 O4 Sr2 92.77(11) . 1_644 ? B4 O5 B7 119.0(4) . . ? B4 O5 Sr4 126.3(3) . . ? B7 O5 Sr4 103.9(3) . . ? B3 O6 B8 117.6(4) 1_644 . ? B3 O6 Sr4 112.3(3) 1_644 . ? B8 O6 Sr4 91.4(3) . . ? B3 O6 Sr2 96.5(3) 1_644 1_554 ? B8 O6 Sr2 134.4(3) . 1_554 ? Sr4 O6 Sr2 103.20(13) . 1_554 ? B4 O7 B9 123.6(4) 1_565 1_645 ? B4 O7 Sr4 100.7(3) 1_565 . ? B9 O7 Sr4 135.0(3) 1_645 . ? B6 O8 B10 131.7(5) 1_565 . ? B6 O8 Sr3 94.4(3) 1_565 . ? B10 O8 Sr3 126.7(3) . . ? B5 O9 B10 122.0(4) . 1_455 ? B5 O9 Sr1 101.4(3) . . ? B10 O9 Sr1 133.2(3) 1_455 . ? B1 O10 B8 125.5(4) 1_565 1_566 ? B1 O10 Sr2 93.3(3) 1_565 . ? B8 O10 Sr2 122.0(3) 1_566 . ? B1 O10 Sr4 120.9(3) 1_565 1_566 ? B8 O10 Sr4 65.6(3) 1_566 1_566 ? Sr2 O10 Sr4 132.57(13) . 1_566 ? B6 O11 B8 120.8(4) 1_565 1_566 ? B6 O11 Sr3 95.3(3) 1_565 . ? B8 O11 Sr3 134.8(3) 1_566 . ? B9 O12 B10 117.5(4) 1_645 1_545 ? B9 O12 Sr1 113.9(3) 1_645 . ? B10 O12 Sr1 93.9(3) 1_545 . ? B9 O12 Sr3 95.2(3) 1_645 . ? B10 O12 Sr3 133.5(3) 1_545 . ? Sr1 O12 Sr3 102.43(13) . . ? Sr3 O13 Sr2 106.94(15) . . ? Sr3 O13 H1 114.9 . . ? Sr2 O13 H1 110.3 . . ? Sr3 O13 H2 128.8 . . ? Sr2 O13 H2 92.7 . . ? H1 O13 H2 100.5 . . ? B6 O14 B3 119.6(5) . 1_645 ? B6 O14 Sr3 125.9(3) . . ? B3 O14 Sr3 100.6(3) 1_645 . ? B1 O15 B3 124.3(4) 1_565 . ? B1 O15 Sr2 96.4(3) 1_565 . ? B3 O15 Sr2 139.1(3) . . ? B1 O15 Sr4 101.6(3) 1_565 1_466 ? B3 O15 Sr4 82.3(3) . 1_466 ? Sr2 O15 Sr4 86.11(11) . 1_466 ? B5 O16 B7 131.5(5) . 1_565 ? B5 O16 Sr1 88.2(3) . . ? B7 O16 Sr1 126.7(3) 1_565 . ? B5 O16 Sr3 127.7(3) . . ? B7 O16 Sr3 89.1(3) 1_565 . ? Sr1 O16 Sr3 90.01(11) . . ? B4 O17 B2 128.7(4) 1_565 1_565 ? B4 O17 Sr4 88.6(3) 1_565 . ? B2 O17 Sr4 127.1(3) 1_565 . ? B4 O17 Sr2 128.6(3) 1_565 1_554 ? B2 O17 Sr2 90.7(3) 1_565 1_554 ? Sr4 O17 Sr2 90.79(10) . 1_554 ? B1 O18 B2 118.7(4) . 1_466 ? B1 O18 Sr2 128.5(3) . . ? B2 O18 Sr2 107.6(3) 1_466 . ? B7 O19 B10 122.0(5) . 1_545 ? B7 O19 Sr4 97.8(3) . . ? B10 O19 Sr4 126.9(3) 1_545 . ? B7 O19 Sr1 126.1(3) . . ? B10 O19 Sr1 88.7(3) 1_545 . ? Sr4 O19 Sr1 94.89(12) . . ? Sr4 O20 Sr2 104.70(15) . 1_644 ? Sr4 O20 H4 120.7 . . ? Sr2 O20 H4 77.8 1_644 . ? Sr4 O20 H5 88.8 . . ? Sr2 O20 H5 154.2 1_644 . ? H4 O20 H5 114.5 . . ? B5 O21 B9 120.4(4) . . ? B5 O21 Sr1 126.8(4) . 1_565 ? B9 O21 Sr1 102.4(3) . 1_565 ? Sr4 O22 Sr1 104.73(15) . . ? Sr4 O22 Sr2 90.23(12) . 1_554 ? Sr1 O22 Sr2 150.82(16) . 1_554 ? Sr4 O22 H6 125.6 . . ? Sr1 O22 H6 83.0 . . ? Sr2 O22 H6 108.7 1_554 . ? _diffrn_measured_fraction_theta_max 0.994 _diffrn_reflns_theta_full 27.51 _diffrn_measured_fraction_theta_full 0.994 _refine_diff_density_max 1.070 _refine_diff_density_min -0.841 _refine_diff_density_rms 0.144 _database_code_depnum_ccdc_archive 'CCDC 951534'