# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2015

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_p
_database_code_depnum_ccdc_archive 'CCDC 1057255'
_audit_update_record             
;
2015-05-05 deposited with the CCDC.
2015-05-06 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            (C4O4)2@Ag24(C6H9)16(CF3COO)4.2CH3CN
_chemical_melting_point          ?
_chemical_formula_moiety         'C112 H144 Ag24 F12 O16, 2CH3CN'
_chemical_formula_sum            'C116 H150 Ag24 F12 N2 O16'
_chemical_formula_weight         4645.25

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   P21/n

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   23.5527(7)
_cell_length_b                   20.9694(8)
_cell_length_c                   29.3460(9)
_cell_angle_alpha                90.00
_cell_angle_beta                 95.231(3)
_cell_angle_gamma                90.00
_cell_volume                     14433.2(8)
_cell_formula_units_Z            4
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    6365
_cell_measurement_theta_min      3.2040
_cell_measurement_theta_max      27.1420

_exptl_crystal_description       block
_exptl_crystal_colour            YELLOW
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.26
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.135
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             8872
_exptl_absorpt_coefficient_mu    3.238
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.4334
_exptl_absorpt_correction_T_max  0.4865
_exptl_absorpt_process_details   
;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.32.4 (release 27-04-2006 CrysAlis171 .NET)
(compiled Apr 27 2007,17:53:11)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Oxford Gemini S Ultra'
_diffrn_measurement_method       'w scans'
_diffrn_detector_area_resol_mean 16.1903
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            68602
_diffrn_reflns_av_R_equivalents  0.0437
_diffrn_reflns_av_unetI/netI     0.0592
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_h_max       29
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_theta_min         2.92
_diffrn_reflns_theta_max         26.00
_reflns_number_total             28306
_reflns_number_gt                20984
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'CrysAlis CCD, Oxford Diffraction Ltd.'
_computing_cell_refinement       'CrysAlis RED, Oxford Diffraction Ltd.'
_computing_data_reduction        'CrysAlis RED, Oxford Diffraction Ltd.'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'ORTEPII(Johnson,1976)and PLUTON(Spek,1990)'
_computing_publication_material  'SHELXL97(Sheldrick, 1997)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0251P)²+41.7147P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         28306
_refine_ls_number_parameters     1720
_refine_ls_number_restraints     490
_refine_ls_R_factor_all          0.0762
_refine_ls_R_factor_gt           0.0489
_refine_ls_wR_factor_ref         0.0937
_refine_ls_wR_factor_gt          0.0860
_refine_ls_goodness_of_fit_ref   1.054
_refine_ls_restrained_S_all      1.072
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.42403(2) 0.93864(3) 0.208150(17) 0.03299(13) Uani 1 1 d . A .
Ag2 Ag 0.64218(2) 0.58200(3) 0.360115(18) 0.03498(13) Uani 1 1 d . A .
Ag3 Ag 0.53148(2) 0.78712(3) 0.398723(18) 0.03610(13) Uani 1 1 d . A .
Ag4 Ag 0.41038(2) 0.58881(3) 0.309852(17) 0.03614(13) Uani 1 1 d . A .
Ag5 Ag 0.29782(2) 0.80741(3) 0.288478(17) 0.03698(14) Uani 1 1 d . A .
Ag6 Ag 0.33963(2) 0.84130(3) 0.196536(19) 0.04025(14) Uani 1 1 d . A .
Ag7 Ag 0.38401(2) 0.90737(3) 0.299423(19) 0.03948(14) Uani 1 1 d . A .
Ag8 Ag 0.61855(2) 0.84629(3) 0.212168(18) 0.03896(14) Uani 1 1 d . A .
Ag9 Ag 0.46177(3) 0.70690(3) 0.129319(17) 0.03733(14) Uani 1 1 d . A .
Ag10 Ag 0.51415(2) 0.56827(3) 0.375765(19) 0.03746(14) Uani 1 1 d . A .
Ag11 Ag 0.64264(2) 0.57759(3) 0.198673(19) 0.03895(14) Uani 1 1 d . . .
Ag12 Ag 0.39660(2) 0.59209(3) 0.192437(17) 0.03999(14) Uani 1 1 d . A .
Ag13 Ag 0.61191(2) 0.85655(3) 0.330921(18) 0.03944(14) Uani 1 1 d . A .
Ag14 Ag 0.69229(2) 0.63696(3) 0.282700(19) 0.04115(15) Uani 1 1 d . A .
Ag15 Ag 0.37661(2) 0.80741(3) 0.376140(18) 0.03934(14) Uani 1 1 d . A .
Ag16 Ag 0.59318(2) 0.52280(3) 0.275319(18) 0.03890(14) Uani 1 1 d . A .
Ag17 Ag 0.45763(3) 0.84456(3) 0.129463(18) 0.04202(15) Uani 1 1 d . A .
Ag18 Ag 0.53677(2) 0.94486(3) 0.268029(19) 0.03829(14) Uani 1 1 d . A .
Ag19 Ag 0.64499(2) 0.73181(3) 0.37754(2) 0.04097(14) Uani 1 1 d . A .
Ag20 Ag 0.32110(3) 0.67772(3) 0.24162(2) 0.04611(15) Uani 1 1 d . A .
Ag21 Ag 0.44201(3) 0.68513(3) 0.39324(2) 0.04392(15) Uani 1 1 d . A .
Ag22 Ag 0.66951(3) 0.72209(3) 0.17633(2) 0.05290(17) Uani 1 1 d . . .
Ag23 Ag 0.51254(3) 0.56616(3) 0.16744(2) 0.05503(18) Uani 1 1 d . . .
Ag24 Ag 0.57872(3) 0.79220(4) 0.12201(2) 0.0659(2) Uani 1 1 d . A .
C1 C 0.4310(3) 0.7556(3) 0.2795(2) 0.0243(14) Uani 1 1 d . . .
C2 C 0.4374(3) 0.7560(3) 0.2307(2) 0.0244(14) Uani 1 1 d . . .
C3 C 0.4807(3) 0.8046(3) 0.2373(2) 0.0243(14) Uani 1 1 d . . .
C4 C 0.4751(3) 0.8038(3) 0.2863(2) 0.0241(14) Uani 1 1 d . . .
O1 O 0.39953(18) 0.7256(2) 0.30471(14) 0.0298(11) Uani 1 1 d . . .
O2 O 0.41298(18) 0.7259(2) 0.19701(14) 0.0307(11) Uani 1 1 d . . .
O3 O 0.51061(18) 0.8346(2) 0.21054(14) 0.0287(11) Uani 1 1 d . . .
O4 O 0.49943(19) 0.8338(2) 0.31996(14) 0.0320(11) Uani 1 1 d . . .
C5 C 0.5512(3) 0.6800(3) 0.3023(2) 0.0247(14) Uani 1 1 d . . .
C6 C 0.5231(3) 0.6432(3) 0.2640(2) 0.0251(15) Uani 1 1 d . . .
C7 C 0.5551(3) 0.6792(3) 0.2323(2) 0.0250(14) Uani 1 1 d . . .
C8 C 0.5827(3) 0.7165(3) 0.2709(2) 0.0254(14) Uani 1 1 d . . .
O5 O 0.54931(18) 0.6792(2) 0.34515(14) 0.0282(10) Uani 1 1 d . . .
O6 O 0.48724(19) 0.5990(2) 0.25984(14) 0.0314(11) Uani 1 1 d . . .
O7 O 0.55777(18) 0.6786(2) 0.18969(14) 0.0287(10) Uani 1 1 d . . .
O8 O 0.61922(19) 0.7601(2) 0.27483(15) 0.0335(11) Uani 1 1 d . . .
C11 C 0.5940(4) 0.6344(4) 0.4571(3) 0.048(2) Uani 1 1 d U A .
C12 C 0.6055(4) 0.6699(4) 0.5031(3) 0.068(2) Uani 1 1 d DU . .
O11 O 0.5446(2) 0.6186(3) 0.44679(18) 0.0543(15) Uani 1 1 d . . .
O12 O 0.6370(3) 0.6276(4) 0.43721(19) 0.0681(19) Uani 1 1 d . . .
F11 F 0.6546(6) 0.6481(8) 0.5254(4) 0.112(5) Uani 0.608(11) 1 d PDU A 1
F12 F 0.5666(7) 0.6618(8) 0.5303(4) 0.105(5) Uani 0.608(11) 1 d PDU A 1
F13 F 0.6146(7) 0.7299(5) 0.4975(5) 0.087(4) Uani 0.608(11) 1 d PDU A 1
F14 F 0.6156(11) 0.6351(8) 0.5388(5) 0.083(6) Uani 0.392(11) 1 d PDU A 2
F15 F 0.6457(9) 0.7133(11) 0.5047(8) 0.089(7) Uani 0.392(11) 1 d PDU A 2
F16 F 0.5595(8) 0.7047(12) 0.5131(7) 0.098(6) Uani 0.392(11) 1 d PDU A 2
C21 C 0.2573(4) 0.7299(5) 0.3746(3) 0.067(3) Uani 1 1 d U A .
C22 C 0.2091(5) 0.7095(6) 0.4035(4) 0.101(3) Uani 1 1 d DU . .
O21 O 0.2419(3) 0.7433(4) 0.3342(2) 0.078(2) Uani 1 1 d . . .
O22 O 0.3046(3) 0.7331(3) 0.3957(2) 0.0626(17) Uani 1 1 d . . .
F21 F 0.1607(6) 0.6986(10) 0.3821(6) 0.138(6) Uani 0.608(11) 1 d PDU A 1
F22 F 0.2246(6) 0.6546(7) 0.4272(5) 0.116(5) Uani 0.608(11) 1 d PDU A 1
F23 F 0.2049(7) 0.7518(7) 0.4373(5) 0.130(6) Uani 0.608(11) 1 d PDU A 1
F24 F 0.1874(10) 0.6558(11) 0.3890(10) 0.135(8) Uani 0.392(11) 1 d PDU A 2
F25 F 0.2168(11) 0.7095(14) 0.4462(6) 0.127(8) Uani 0.392(11) 1 d PDU A 2
F26 F 0.1645(8) 0.7495(11) 0.3934(8) 0.114(7) Uani 0.392(11) 1 d PDU A 2
C31 C 0.6534(5) 0.6154(5) 0.0949(3) 0.072(2) Uani 1 1 d U . .
C32 C 0.6812(4) 0.5980(6) 0.0517(4) 0.072(3) Uani 1 1 d . . .
O31 O 0.6506(3) 0.6723(4) 0.1008(2) 0.083(2) Uani 1 1 d U . .
O32 O 0.6382(4) 0.5715(4) 0.1176(2) 0.098(2) Uani 1 1 d U . .
F31 F 0.6929(3) 0.5365(4) 0.0487(3) 0.134(3) Uani 1 1 d . . .
F32 F 0.7251(4) 0.6270(6) 0.0461(4) 0.219(7) Uani 1 1 d . . .
F33 F 0.6441(3) 0.6039(4) 0.0151(2) 0.122(3) Uani 1 1 d . . .
C41 C 0.5294(4) 0.9766(4) 0.1439(3) 0.049(2) Uani 1 1 d . A .
C42 C 0.5717(4) 1.0253(5) 0.1302(3) 0.078(3) Uani 1 1 d DU . .
O41 O 0.5043(3) 0.9916(3) 0.17709(19) 0.0582(16) Uani 1 1 d . . .
O42 O 0.5273(3) 0.9274(3) 0.1218(2) 0.077(2) Uani 1 1 d . . .
F41 F 0.6245(5) 1.0136(7) 0.1498(5) 0.103(5) Uani 0.608(11) 1 d PDU A 1
F42 F 0.5776(8) 1.0285(9) 0.0864(4) 0.110(6) Uani 0.608(11) 1 d PDU A 1
F43 F 0.5614(7) 1.0846(6) 0.1430(6) 0.103(5) Uani 0.608(11) 1 d PDU A 1
F44 F 0.6012(11) 1.0071(12) 0.0963(8) 0.097(7) Uani 0.392(11) 1 d PDU A 2
F45 F 0.5424(9) 1.0762(10) 0.1137(8) 0.102(6) Uani 0.392(11) 1 d PDU A 2
F46 F 0.6084(11) 1.0468(13) 0.1622(7) 0.115(7) Uani 0.392(11) 1 d PDU A 2
C51 C 0.3770(3) 0.9007(4) 0.1483(2) 0.0395(18) Uani 1 1 d . . .
C52 C 0.3692(3) 0.9180(4) 0.1088(2) 0.045(2) Uani 1 1 d . A .
C53 C 0.3555(4) 0.9440(5) 0.0622(3) 0.074(3) Uani 1 1 d DU . .
C56 C 0.3540(7) 1.0168(6) 0.0656(5) 0.090(4) Uani 0.695(6) 1 d PDU A 1
H56A H 0.3450 1.0350 0.0351 0.135 Uiso 0.695(6) 1 calc PR A 1
H56B H 0.3914 1.0324 0.0784 0.135 Uiso 0.695(6) 1 calc PR A 1
H56C H 0.3249 1.0296 0.0856 0.135 Uiso 0.695(6) 1 calc PR A 1
C54 C 0.3957(7) 0.9220(9) 0.0296(4) 0.098(5) Uani 0.695(6) 1 d PDU A 1
H54A H 0.3847 0.9402 -0.0006 0.148 Uiso 0.695(6) 1 calc PR A 1
H54B H 0.3946 0.8753 0.0277 0.148 Uiso 0.695(6) 1 calc PR A 1
H54C H 0.4344 0.9358 0.0403 0.148 Uiso 0.695(6) 1 calc PR A 1
C55 C 0.2929(6) 0.9237(7) 0.0454(4) 0.082(4) Uani 0.695(6) 1 d PDU A 1
H55A H 0.2829 0.9405 0.0146 0.123 Uiso 0.695(6) 1 calc PR A 1
H55B H 0.2666 0.9409 0.0664 0.123 Uiso 0.695(6) 1 calc PR A 1
H55C H 0.2902 0.8771 0.0449 0.123 Uiso 0.695(6) 1 calc PR A 1
C57 C 0.4059(13) 0.9857(16) 0.0522(11) 0.098(6) Uani 0.305(6) 1 d PDU A 2
H57A H 0.3987 1.0046 0.0217 0.148 Uiso 0.305(6) 1 calc PR A 2
H57B H 0.4406 0.9597 0.0534 0.148 Uiso 0.305(6) 1 calc PR A 2
H57C H 0.4109 1.0198 0.0751 0.148 Uiso 0.305(6) 1 calc PR A 2
C58 C 0.3572(15) 0.8864(15) 0.0305(9) 0.084(7) Uani 0.305(6) 1 d PDU A 2
H58A H 0.3487 0.9001 -0.0013 0.126 Uiso 0.305(6) 1 calc PR A 2
H58B H 0.3289 0.8549 0.0383 0.126 Uiso 0.305(6) 1 calc PR A 2
H58C H 0.3953 0.8671 0.0342 0.126 Uiso 0.305(6) 1 calc PR A 2
C59 C 0.3018(13) 0.9788(16) 0.0530(11) 0.094(6) Uani 0.305(6) 1 d PDU A 2
H59A H 0.2983 0.9940 0.0212 0.141 Uiso 0.305(6) 1 calc PR A 2
H59B H 0.3013 1.0153 0.0738 0.141 Uiso 0.305(6) 1 calc PR A 2
H59C H 0.2697 0.9505 0.0576 0.141 Uiso 0.305(6) 1 calc PR A 2
C61 C 0.2800(3) 0.7711(4) 0.2218(3) 0.0371(18) Uani 1 1 d . . .
C62 C 0.2618(3) 0.7521(4) 0.1839(3) 0.046(2) Uani 1 1 d . A .
C63 C 0.2378(5) 0.7308(6) 0.1375(3) 0.099(4) Uani 1 1 d DU . .
C64 C 0.2848(5) 0.7198(7) 0.1074(4) 0.136(5) Uani 1 1 d DU A .
H64A H 0.2689 0.7178 0.0754 0.204 Uiso 1 1 calc R . .
H64B H 0.3041 0.6795 0.1159 0.204 Uiso 1 1 calc R . .
H64C H 0.3123 0.7549 0.1112 0.204 Uiso 1 1 calc R . .
C65 C 0.2056(6) 0.6702(6) 0.1428(4) 0.152(6) Uani 1 1 d DU A .
H65A H 0.1787 0.6760 0.1661 0.228 Uiso 1 1 calc R . .
H65B H 0.2324 0.6359 0.1522 0.228 Uiso 1 1 calc R . .
H65C H 0.1845 0.6590 0.1135 0.228 Uiso 1 1 calc R . .
C66 C 0.1981(6) 0.7806(7) 0.1190(4) 0.164(6) Uani 1 1 d DU A .
H66A H 0.1728 0.7927 0.1422 0.246 Uiso 1 1 calc R . .
H66B H 0.1754 0.7643 0.0918 0.246 Uiso 1 1 calc R . .
H66C H 0.2198 0.8180 0.1105 0.246 Uiso 1 1 calc R . .
C71 C 0.3183(3) 0.8796(4) 0.3412(2) 0.0333(17) Uani 1 1 d . . .
C72 C 0.2825(3) 0.9071(4) 0.3602(2) 0.0340(17) Uani 1 1 d . A .
C73 C 0.2374(3) 0.9401(4) 0.3827(2) 0.051(2) Uani 1 1 d DU . .
C74 C 0.2420(6) 0.9278(7) 0.4320(4) 0.083(5) Uani 0.695(6) 1 d PDU A 1
H74A H 0.2115 0.9505 0.4458 0.125 Uiso 0.695(6) 1 calc PR A 1
H74B H 0.2791 0.9428 0.4457 0.125 Uiso 0.695(6) 1 calc PR A 1
H74C H 0.2385 0.8820 0.4374 0.125 Uiso 0.695(6) 1 calc PR A 1
C75 C 0.2462(6) 1.0137(6) 0.3766(4) 0.072(4) Uani 0.695(6) 1 d PDU A 1
H75A H 0.2168 1.0369 0.3913 0.108 Uiso 0.695(6) 1 calc PR A 1
H75B H 0.2433 1.0241 0.3439 0.108 Uiso 0.695(6) 1 calc PR A 1
H75C H 0.2839 1.0259 0.3907 0.108 Uiso 0.695(6) 1 calc PR A 1
C76 C 0.1809(5) 0.9257(7) 0.3585(5) 0.085(5) Uani 0.695(6) 1 d PDU A 1
H76A H 0.1512 0.9478 0.3737 0.128 Uiso 0.695(6) 1 calc PR A 1
H76B H 0.1741 0.8796 0.3592 0.128 Uiso 0.695(6) 1 calc PR A 1
H76C H 0.1801 0.9401 0.3267 0.128 Uiso 0.695(6) 1 calc PR A 1
C77 C 0.2005(9) 0.8860(10) 0.4049(7) 0.041(6) Uani 0.305(6) 1 d PDU A 2
H77A H 0.1700 0.9060 0.4204 0.061 Uiso 0.305(6) 1 calc PR A 2
H77B H 0.2252 0.8614 0.4271 0.061 Uiso 0.305(6) 1 calc PR A 2
H77C H 0.1839 0.8575 0.3808 0.061 Uiso 0.305(6) 1 calc PR A 2
C78 C 0.2629(11) 0.9803(11) 0.4227(7) 0.053(6) Uani 0.305(6) 1 d PDU A 2
H78A H 0.2323 1.0018 0.4372 0.080 Uiso 0.305(6) 1 calc PR A 2
H78B H 0.2887 1.0122 0.4116 0.080 Uiso 0.305(6) 1 calc PR A 2
H78C H 0.2843 0.9527 0.4452 0.080 Uiso 0.305(6) 1 calc PR A 2
C79 C 0.1967(11) 0.9774(12) 0.3503(9) 0.063(7) Uani 0.305(6) 1 d PDU A 2
H79A H 0.1681 0.9981 0.3674 0.095 Uiso 0.305(6) 1 calc PR A 2
H79B H 0.1777 0.9485 0.3275 0.095 Uiso 0.305(6) 1 calc PR A 2
H79C H 0.2179 1.0099 0.3348 0.095 Uiso 0.305(6) 1 calc PR A 2
C81 C 0.4329(3) 0.5994(4) 0.1306(2) 0.0339(17) Uani 1 1 d . . .
C82 C 0.4344(3) 0.6017(3) 0.0891(2) 0.0339(17) Uani 1 1 d . . .
C83 C 0.4344(4) 0.5965(4) 0.0383(2) 0.046(2) Uani 1 1 d . . .
C84 C 0.3978(4) 0.6500(5) 0.0162(3) 0.068(3) Uani 1 1 d . . .
H84A H 0.3577 0.6426 0.0213 0.103 Uiso 1 1 calc R . .
H84B H 0.4017 0.6510 -0.0167 0.103 Uiso 1 1 calc R . .
H84C H 0.4102 0.6909 0.0299 0.103 Uiso 1 1 calc R . .
C85 C 0.4104(5) 0.5310(5) 0.0242(3) 0.086(4) Uani 1 1 d . . .
H85A H 0.4312 0.4980 0.0425 0.128 Uiso 1 1 calc R . .
H85B H 0.4147 0.5239 -0.0083 0.128 Uiso 1 1 calc R . .
H85C H 0.3699 0.5292 0.0294 0.128 Uiso 1 1 calc R . .
C86 C 0.4958(4) 0.6032(5) 0.0263(3) 0.066(3) Uani 1 1 d . . .
H86A H 0.5106 0.6452 0.0361 0.100 Uiso 1 1 calc R . .
H86B H 0.4969 0.5989 -0.0069 0.100 Uiso 1 1 calc R . .
H86C H 0.5193 0.5698 0.0419 0.100 Uiso 1 1 calc R . .
C91 C 0.5805(3) 0.5018(4) 0.2032(2) 0.0378(18) Uani 1 1 d . . .
C92 C 0.5569(3) 0.4592(4) 0.1821(2) 0.0381(18) Uani 1 1 d . . .
C93 C 0.5344(3) 0.4028(4) 0.1558(3) 0.054(2) Uani 1 1 d DU . .
C94 C 0.5647(5) 0.3449(5) 0.1762(4) 0.101(4) Uani 1 1 d DU . .
H94A H 0.6053 0.3474 0.1715 0.151 Uiso 1 1 calc R . .
H94B H 0.5483 0.3064 0.1613 0.151 Uiso 1 1 calc R . .
H94C H 0.5602 0.3430 0.2090 0.151 Uiso 1 1 calc R . .
C95 C 0.5488(6) 0.4094(7) 0.1074(3) 0.126(5) Uani 1 1 d DU . .
H95A H 0.5265 0.4444 0.0926 0.189 Uiso 1 1 calc R . .
H95B H 0.5397 0.3696 0.0909 0.189 Uiso 1 1 calc R . .
H95C H 0.5895 0.4186 0.1072 0.189 Uiso 1 1 calc R . .
C96 C 0.4720(4) 0.3957(6) 0.1581(4) 0.106(4) Uani 1 1 d DU . .
H96A H 0.4645 0.3828 0.1891 0.159 Uiso 1 1 calc R . .
H96B H 0.4573 0.3631 0.1362 0.159 Uiso 1 1 calc R . .
H96C H 0.4531 0.4364 0.1505 0.159 Uiso 1 1 calc R . .
C101 C 0.7146(3) 0.6392(4) 0.2128(2) 0.0399(18) Uani 1 1 d . . .
C102 C 0.7640(3) 0.6518(4) 0.2104(3) 0.0414(18) Uani 1 1 d . . .
C103 C 0.8257(3) 0.6612(4) 0.2060(3) 0.057(2) Uani 1 1 d . . .
C104 C 0.8580(4) 0.6075(5) 0.2312(4) 0.076(3) Uani 1 1 d . . .
H10A H 0.8484 0.6062 0.2629 0.114 Uiso 1 1 calc R . .
H10B H 0.8991 0.6147 0.2307 0.114 Uiso 1 1 calc R . .
H10C H 0.8476 0.5669 0.2162 0.114 Uiso 1 1 calc R . .
C105 C 0.8430(4) 0.7253(6) 0.2251(5) 0.120(5) Uani 1 1 d . . .
H10D H 0.8217 0.7586 0.2074 0.180 Uiso 1 1 calc R . .
H10E H 0.8839 0.7315 0.2232 0.180 Uiso 1 1 calc R . .
H10F H 0.8346 0.7277 0.2572 0.180 Uiso 1 1 calc R . .
C106 C 0.8368(5) 0.6579(7) 0.1552(4) 0.113(5) Uani 1 1 d . . .
H10G H 0.8204 0.6186 0.1417 0.170 Uiso 1 1 calc R . .
H10H H 0.8780 0.6584 0.1526 0.170 Uiso 1 1 calc R . .
H10I H 0.8191 0.6948 0.1390 0.170 Uiso 1 1 calc R . .
C111 C 0.6199(3) 0.8232(4) 0.4026(2) 0.0369(17) Uani 1 1 d . . .
C112 C 0.6373(3) 0.8637(4) 0.4291(2) 0.0351(17) Uani 1 1 d . . .
C113 C 0.6595(4) 0.9113(4) 0.4632(3) 0.059(3) Uani 1 1 d . . .
C114 C 0.6163(5) 0.9205(6) 0.4981(3) 0.096(4) Uani 1 1 d . . .
H11A H 0.5816 0.9400 0.4832 0.143 Uiso 1 1 calc R . .
H11B H 0.6325 0.9483 0.5228 0.143 Uiso 1 1 calc R . .
H11C H 0.6068 0.8790 0.5109 0.143 Uiso 1 1 calc R . .
C115 C 0.7157(6) 0.8862(7) 0.4869(5) 0.157(8) Uani 1 1 d . . .
H11D H 0.7083 0.8476 0.5042 0.235 Uiso 1 1 calc R . .
H11E H 0.7327 0.9188 0.5078 0.235 Uiso 1 1 calc R . .
H11F H 0.7419 0.8762 0.4638 0.235 Uiso 1 1 calc R . .
C116 C 0.6672(5) 0.9743(5) 0.4396(4) 0.092(4) Uani 1 1 d . . .
H11G H 0.6943 0.9691 0.4165 0.139 Uiso 1 1 calc R . .
H11H H 0.6818 1.0060 0.4622 0.139 Uiso 1 1 calc R . .
H11I H 0.6304 0.9886 0.4248 0.139 Uiso 1 1 calc R . .
C121 C 0.4469(3) 0.9745(3) 0.2746(2) 0.0324(16) Uani 1 1 d . . .
C122 C 0.4607(3) 0.9992(4) 0.3116(2) 0.0350(17) Uani 1 1 d . A .
C123 C 0.4730(4) 1.0305(4) 0.3564(3) 0.052(2) Uani 1 1 d . . .
C124 C 0.4891(5) 0.9793(6) 0.3933(3) 0.093(4) Uani 1 1 d . A .
H12A H 0.4558 0.9523 0.3971 0.140 Uiso 1 1 calc R . .
H12B H 0.5013 1.0002 0.4224 0.140 Uiso 1 1 calc R . .
H12C H 0.5202 0.9528 0.3838 0.140 Uiso 1 1 calc R . .
C125 C 0.4207(5) 1.0650(6) 0.3689(4) 0.107(5) Uani 1 1 d . A .
H12D H 0.4086 1.0958 0.3448 0.161 Uiso 1 1 calc R . .
H12E H 0.4295 1.0876 0.3979 0.161 Uiso 1 1 calc R . .
H12F H 0.3901 1.0342 0.3721 0.161 Uiso 1 1 calc R . .
C126 C 0.5229(6) 1.0738(7) 0.3536(4) 0.132(6) Uani 1 1 d . A .
H12G H 0.5543 1.0501 0.3420 0.198 Uiso 1 1 calc R . .
H12H H 0.5350 1.0905 0.3842 0.198 Uiso 1 1 calc R . .
H12I H 0.5120 1.1093 0.3330 0.198 Uiso 1 1 calc R . .
C201 C 0.6619(3) 0.8219(4) 0.1522(2) 0.0358(17) Uani 1 1 d . . .
C202 C 0.6964(3) 0.8417(4) 0.1272(2) 0.0385(18) Uani 1 1 d . . .
C203 C 0.7379(3) 0.8651(5) 0.0968(3) 0.059(3) Uani 1 1 d . . .
C204 C 0.7963(4) 0.8696(7) 0.1220(4) 0.107(5) Uani 1 1 d . . .
H20A H 0.7931 0.8867 0.1528 0.160 Uiso 1 1 calc R . .
H20B H 0.8202 0.8981 0.1053 0.160 Uiso 1 1 calc R . .
H20C H 0.8137 0.8272 0.1244 0.160 Uiso 1 1 calc R . .
C205 C 0.7408(6) 0.8192(8) 0.0576(4) 0.156(8) Uani 1 1 d . . .
H20D H 0.7435 0.7755 0.0694 0.234 Uiso 1 1 calc R . .
H20E H 0.7744 0.8288 0.0414 0.234 Uiso 1 1 calc R . .
H20F H 0.7063 0.8235 0.0364 0.234 Uiso 1 1 calc R . .
C206 C 0.7205(6) 0.9309(8) 0.0806(6) 0.176(9) Uani 1 1 d . . .
H20G H 0.6876 0.9280 0.0577 0.264 Uiso 1 1 calc R . .
H20H H 0.7523 0.9514 0.0669 0.264 Uiso 1 1 calc R . .
H20I H 0.7103 0.9564 0.1066 0.264 Uiso 1 1 calc R . .
C301 C 0.4944(3) 0.7742(4) 0.0830(2) 0.0355(17) Uani 1 1 d . . .
C302 C 0.5156(3) 0.7865(4) 0.0479(2) 0.0354(17) Uani 1 1 d . A .
C303 C 0.5370(3) 0.8012(5) 0.0024(3) 0.054(2) Uani 1 1 d . . .
C304 C 0.5855(5) 0.7553(6) -0.0049(3) 0.099(4) Uani 1 1 d . A .
H30A H 0.6037 0.7679 -0.0323 0.148 Uiso 1 1 calc R . .
H30B H 0.5704 0.7119 -0.0089 0.148 Uiso 1 1 calc R . .
H30C H 0.6138 0.7566 0.0218 0.148 Uiso 1 1 calc R . .
C305 C 0.5577(6) 0.8687(6) 0.0031(4) 0.106(4) Uani 1 1 d . A .
H30D H 0.5254 0.8976 0.0056 0.159 Uiso 1 1 calc R . .
H30E H 0.5752 0.8778 -0.0252 0.159 Uiso 1 1 calc R . .
H30F H 0.5859 0.8749 0.0294 0.159 Uiso 1 1 calc R . .
C306 C 0.4879(4) 0.7917(7) -0.0344(3) 0.095(4) Uani 1 1 d . A .
H30G H 0.4567 0.8207 -0.0287 0.143 Uiso 1 1 calc R . .
H30H H 0.4744 0.7475 -0.0336 0.143 Uiso 1 1 calc R . .
H30I H 0.5009 0.8007 -0.0645 0.143 Uiso 1 1 calc R . .
C401 C 0.5839(3) 0.5056(3) 0.3490(2) 0.0327(16) Uani 1 1 d . . .
C402 C 0.5502(3) 0.4626(4) 0.3456(2) 0.0319(16) Uani 1 1 d . A .
C403 C 0.5137(3) 0.4050(4) 0.3411(3) 0.049(2) Uani 1 1 d DU . .
C404 C 0.5471(4) 0.3504(5) 0.3241(4) 0.097(4) Uani 1 1 d DU A .
H40A H 0.5622 0.3624 0.2953 0.146 Uiso 1 1 calc R . .
H40B H 0.5221 0.3132 0.3190 0.146 Uiso 1 1 calc R . .
H40C H 0.5787 0.3399 0.3469 0.146 Uiso 1 1 calc R . .
C405 C 0.4638(4) 0.4182(5) 0.3059(4) 0.093(4) Uani 1 1 d DU A .
H40D H 0.4407 0.4529 0.3168 0.139 Uiso 1 1 calc R . .
H40E H 0.4404 0.3796 0.3014 0.139 Uiso 1 1 calc R . .
H40F H 0.4781 0.4305 0.2769 0.139 Uiso 1 1 calc R . .
C406 C 0.4915(5) 0.3903(6) 0.3861(3) 0.119(5) Uani 1 1 d DU A .
H40G H 0.5233 0.3777 0.4081 0.178 Uiso 1 1 calc R . .
H40H H 0.4639 0.3553 0.3822 0.178 Uiso 1 1 calc R . .
H40I H 0.4729 0.4282 0.3973 0.178 Uiso 1 1 calc R . .
C501 C 0.4205(3) 0.5821(3) 0.3827(2) 0.0313(16) Uani 1 1 d . . .
C502 C 0.4051(3) 0.5769(3) 0.4206(2) 0.0324(16) Uani 1 1 d . A .
C503 C 0.3852(3) 0.5651(4) 0.4667(3) 0.054(2) Uani 1 1 d DU . .
C504 C 0.4339(5) 0.5257(6) 0.4944(4) 0.070(4) Uani 0.695(6) 1 d PDU A 1
H50A H 0.4229 0.5167 0.5252 0.105 Uiso 0.695(6) 1 calc PR A 1
H50B H 0.4694 0.5504 0.4967 0.105 Uiso 0.695(6) 1 calc PR A 1
H50C H 0.4398 0.4854 0.4785 0.105 Uiso 0.695(6) 1 calc PR A 1
C505 C 0.3312(5) 0.5281(7) 0.4644(5) 0.080(5) Uani 0.695(6) 1 d PDU A 1
H50D H 0.3199 0.5215 0.4953 0.119 Uiso 0.695(6) 1 calc PR A 1
H50E H 0.3369 0.4866 0.4500 0.119 Uiso 0.695(6) 1 calc PR A 1
H50F H 0.3012 0.5516 0.4462 0.119 Uiso 0.695(6) 1 calc PR A 1
C506 C 0.3810(6) 0.6295(6) 0.4918(4) 0.067(4) Uani 0.695(6) 1 d PDU A 1
H50G H 0.3681 0.6220 0.5222 0.101 Uiso 0.695(6) 1 calc PR A 1
H50H H 0.3538 0.6572 0.4741 0.101 Uiso 0.695(6) 1 calc PR A 1
H50I H 0.4186 0.6499 0.4951 0.101 Uiso 0.695(6) 1 calc PR A 1
C507 C 0.3244(9) 0.5932(13) 0.4616(8) 0.061(7) Uani 0.305(6) 1 d PDU A 2
H50J H 0.3015 0.5709 0.4369 0.091 Uiso 0.305(6) 1 calc PR A 2
H50K H 0.3263 0.6387 0.4542 0.091 Uiso 0.305(6) 1 calc PR A 2
H50L H 0.3068 0.5878 0.4903 0.091 Uiso 0.305(6) 1 calc PR A 2
C508 C 0.3793(12) 0.4947(10) 0.4730(10) 0.065(7) Uani 0.305(6) 1 d PDU A 2
H50M H 0.3557 0.4768 0.4468 0.098 Uiso 0.305(6) 1 calc PR A 2
H50N H 0.3613 0.4863 0.5012 0.098 Uiso 0.305(6) 1 calc PR A 2
H50O H 0.4172 0.4749 0.4751 0.098 Uiso 0.305(6) 1 calc PR A 2
C509 C 0.4194(12) 0.5971(13) 0.5041(9) 0.069(7) Uani 0.305(6) 1 d PDU A 2
H50P H 0.4040 0.5871 0.5332 0.103 Uiso 0.305(6) 1 calc PR A 2
H50Q H 0.4182 0.6433 0.4991 0.103 Uiso 0.305(6) 1 calc PR A 2
H50R H 0.4589 0.5822 0.5051 0.103 Uiso 0.305(6) 1 calc PR A 2
C601 C 0.3459(3) 0.5757(4) 0.2462(2) 0.0357(17) Uani 1 1 d . . .
C602 C 0.3118(3) 0.5550(4) 0.2707(2) 0.0362(18) Uani 1 1 d . A .
C603 C 0.2664(4) 0.5250(5) 0.2950(3) 0.062(3) Uani 1 1 d . . .
C604 C 0.2880(6) 0.4671(7) 0.3175(5) 0.132(5) Uani 1 1 d U A .
H60A H 0.2951 0.4350 0.2945 0.197 Uiso 1 1 calc R . .
H60B H 0.2597 0.4508 0.3372 0.197 Uiso 1 1 calc R . .
H60C H 0.3236 0.4765 0.3363 0.197 Uiso 1 1 calc R . .
C605 C 0.2151(5) 0.5181(8) 0.2644(4) 0.130(6) Uani 1 1 d . A .
H60D H 0.2211 0.4855 0.2414 0.196 Uiso 1 1 calc R . .
H60E H 0.2060 0.5589 0.2491 0.196 Uiso 1 1 calc R . .
H60F H 0.1835 0.5053 0.2819 0.196 Uiso 1 1 calc R . .
C606 C 0.2525(5) 0.5698(8) 0.3344(4) 0.138(7) Uani 1 1 d . A .
H60G H 0.2238 0.5497 0.3519 0.207 Uiso 1 1 calc R . .
H60H H 0.2376 0.6103 0.3216 0.207 Uiso 1 1 calc R . .
H60I H 0.2872 0.5777 0.3546 0.207 Uiso 1 1 calc R . .
C701 C 0.6232(3) 0.9216(3) 0.2719(2) 0.0316(16) Uani 1 1 d . . .
C702 C 0.6746(3) 0.9170(3) 0.2735(2) 0.0321(16) Uani 1 1 d . A .
C703 C 0.7378(3) 0.9197(4) 0.2744(3) 0.052(2) Uani 1 1 d . . .
C704 C 0.7614(3) 0.9475(4) 0.3205(3) 0.056(2) Uani 1 1 d . A .
H70A H 0.7442 0.9895 0.3247 0.085 Uiso 1 1 calc R . .
H70B H 0.8028 0.9520 0.3211 0.085 Uiso 1 1 calc R . .
H70C H 0.7521 0.9190 0.3452 0.085 Uiso 1 1 calc R . .
C705 C 0.7533(4) 0.9634(5) 0.2349(3) 0.073(3) Uani 1 1 d . A .
H70D H 0.7366 0.9460 0.2057 0.109 Uiso 1 1 calc R . .
H70E H 0.7948 0.9654 0.2347 0.109 Uiso 1 1 calc R . .
H70F H 0.7382 1.0063 0.2393 0.109 Uiso 1 1 calc R . .
C706 C 0.7615(4) 0.8526(5) 0.2681(4) 0.090(4) Uani 1 1 d . A .
H70G H 0.7492 0.8244 0.2920 0.135 Uiso 1 1 calc R . .
H70H H 0.8032 0.8542 0.2704 0.135 Uiso 1 1 calc R . .
H70I H 0.7472 0.8362 0.2380 0.135 Uiso 1 1 calc R . .
C801 C 0.7055(3) 0.6549(4) 0.3540(2) 0.0370(17) Uani 1 1 d . . .
C802 C 0.7412(3) 0.6850(3) 0.3768(2) 0.0343(17) Uani 1 1 d . A .
C803 C 0.7894(3) 0.7140(5) 0.4064(3) 0.055(2) Uani 1 1 d . . .
C804 C 0.8396(5) 0.6737(7) 0.4024(5) 0.130(5) Uani 1 1 d U A .
H80A H 0.8315 0.6302 0.4120 0.195 Uiso 1 1 calc R . .
H80B H 0.8720 0.6908 0.4220 0.195 Uiso 1 1 calc R . .
H80C H 0.8489 0.6734 0.3705 0.195 Uiso 1 1 calc R . .
C805 C 0.7989(5) 0.7825(6) 0.3920(4) 0.107(4) Uani 1 1 d . A .
H80D H 0.8298 0.8015 0.4123 0.160 Uiso 1 1 calc R . .
H80E H 0.7639 0.8071 0.3939 0.160 Uiso 1 1 calc R . .
H80F H 0.8094 0.7832 0.3604 0.160 Uiso 1 1 calc R . .
C806 C 0.7734(5) 0.7167(6) 0.4558(3) 0.086(4) Uani 1 1 d . A .
H80G H 0.7665 0.6734 0.4666 0.130 Uiso 1 1 calc R . .
H80H H 0.7387 0.7423 0.4570 0.130 Uiso 1 1 calc R . .
H80I H 0.8046 0.7362 0.4754 0.130 Uiso 1 1 calc R . .
C901 C 0.4504(3) 0.7760(3) 0.4266(2) 0.0295(15) Uani 1 1 d . . .
C902 C 0.4325(3) 0.8007(3) 0.4595(2) 0.0383(18) Uani 1 1 d . A .
C903 C 0.4142(4) 0.8274(4) 0.5025(3) 0.062(2) Uani 1 1 d DU . .
C904 C 0.4503(5) 0.7968(5) 0.5426(3) 0.107(4) Uani 1 1 d DU A .
H90A H 0.4421 0.7510 0.5434 0.160 Uiso 1 1 calc R . .
H90B H 0.4411 0.8165 0.5713 0.160 Uiso 1 1 calc R . .
H90C H 0.4908 0.8031 0.5388 0.160 Uiso 1 1 calc R . .
C905 C 0.4241(5) 0.8992(5) 0.5028(3) 0.091(4) Uani 1 1 d DU A .
H90D H 0.4033 0.9183 0.4757 0.137 Uiso 1 1 calc R . .
H90E H 0.4649 0.9079 0.5024 0.137 Uiso 1 1 calc R . .
H90F H 0.4103 0.9177 0.5304 0.137 Uiso 1 1 calc R . .
C906 C 0.3510(4) 0.8125(6) 0.5048(4) 0.105(4) Uani 1 1 d DU A .
H90G H 0.3284 0.8352 0.4802 0.158 Uiso 1 1 calc R . .
H90H H 0.3394 0.8264 0.5345 0.158 Uiso 1 1 calc R . .
H90I H 0.3448 0.7665 0.5013 0.158 Uiso 1 1 calc R . .
C1S C 0.1351(6) 0.7893(7) 0.2686(5) 0.116(5) Uiso 1 1 d D . .
C2S C 0.1487(12) 0.7230(9) 0.2543(10) 0.130(10) Uiso 0.50 1 d PD . .
C3S C 0.1002(11) 0.7555(12) 0.2308(8) 0.140(11) Uiso 0.50 1 d PD . .
N1S N 0.1515(16) 0.6720(11) 0.2351(12) 0.221(16) Uiso 0.50 1 d PD . .
N2S N 0.0697(14) 0.7196(16) 0.2075(11) 0.228(16) Uiso 0.50 1 d PD . .
N10S N 0.4401(9) 0.1207(11) 0.1962(7) 0.231(8) Uiso 1 1 d D . .
C10S C 0.4728(13) 0.1586(16) 0.2162(11) 0.153(13) Uiso 0.50 1 d PD . .
C40S C 0.4598(17) 0.1660(18) 0.1775(16) 0.22(2) Uiso 0.50 1 d PD . .
C20S C 0.4991(13) 0.2088(14) 0.2473(10) 0.151(12) Uiso 0.50 1 d PD . .
C30S C 0.4704(16) 0.2241(15) 0.1501(12) 0.177(15) Uiso 0.50 1 d PD . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C121 2.114(7) . ?
Ag1 C51 2.142(7) . ?
Ag1 O41 2.440(5) . ?
Ag1 Ag6 2.8479(8) . ?
Ag1 Ag7 2.9922(7) . ?
Ag1 Ag18 3.0504(8) . ?
Ag1 Ag17 3.1912(8) . ?
Ag2 C401 2.116(7) . ?
Ag2 C801 2.155(7) . ?
Ag2 O12 2.470(6) . ?
Ag2 Ag14 2.8933(8) . ?
Ag2 Ag16 2.9226(7) . ?
Ag2 Ag10 3.1047(8) . ?
Ag2 Ag19 3.1825(8) . ?
Ag3 C901 2.157(7) . ?
Ag3 C111 2.209(7) . ?
Ag3 O4 2.560(4) . ?
Ag3 Ag21 2.9963(8) . ?
Ag3 Ag19 3.0303(8) . ?
Ag3 Ag13 3.2178(8) . ?
Ag4 C501 2.134(7) . ?
Ag4 C601 2.315(7) . ?
Ag4 O6 2.442(4) . ?
Ag4 C602 2.594(7) . ?
Ag4 Ag10 3.0063(8) . ?
Ag4 Ag21 3.2078(8) . ?
Ag4 Ag20 3.3376(8) . ?
Ag5 C61 2.107(7) . ?
Ag5 C71 2.186(7) . ?
Ag5 O21 2.379(6) . ?
Ag5 Ag7 2.9155(8) . ?
Ag5 Ag15 3.0317(7) . ?
Ag5 Ag6 3.0397(8) . ?
Ag5 Ag20 3.1183(9) . ?
Ag6 C51 2.133(7) . ?
Ag6 C61 2.209(7) . ?
Ag6 C62 2.622(8) . ?
Ag7 C71 2.140(7) . ?
Ag7 C121 2.214(7) . ?
Ag7 C122 2.642(7) . ?
Ag7 Ag15 3.0927(8) . ?
Ag8 C201 2.176(7) . ?
Ag8 C701 2.355(7) . ?
Ag8 O3 2.550(4) . ?
Ag8 O8 2.578(5) . ?
Ag8 C702 2.596(7) . ?
Ag8 Ag24 2.9520(8) . ?
Ag8 Ag22 3.0918(9) . ?
Ag8 Ag18 3.3535(8) . ?
Ag9 C301 2.149(7) . ?
Ag9 C81 2.356(7) . ?
Ag9 O2 2.417(4) . ?
Ag9 C82 2.558(7) . ?
Ag9 Ag17 2.8883(8) . ?
Ag9 Ag24 3.3076(9) . ?
Ag9 Ag23 3.3388(9) . ?
Ag10 C501 2.253(7) . ?
Ag10 C401 2.297(7) . ?
Ag10 O11 2.387(5) . ?
Ag10 C402 2.561(7) . ?
Ag10 Ag21 3.0517(8) . ?
Ag11 C101 2.140(8) . ?
Ag11 C91 2.174(8) . ?
Ag11 O32 2.375(6) . ?
Ag11 Ag16 2.8659(8) . ?
Ag11 Ag14 2.9107(8) . ?
Ag11 Ag23 3.1264(8) . ?
Ag11 Ag22 3.1762(9) . ?
Ag12 C81 2.081(7) . ?
Ag12 C601 2.091(7) . ?
Ag12 Ag23 2.9419(9) . ?
Ag12 Ag20 2.9897(9) . ?
Ag13 C111 2.207(7) . ?
Ag13 C701 2.239(7) . ?
Ag13 C702 2.662(7) . ?
Ag13 Ag19 3.0209(9) . ?
Ag13 Ag18 3.0614(8) . ?
Ag14 C801 2.122(7) . ?
Ag14 C101 2.163(7) . ?
Ag14 Ag16 3.3368(9) . ?
Ag15 C71 2.230(7) . ?
Ag15 C901 2.275(6) . ?
Ag15 O22 2.410(6) . ?
Ag15 C902 2.673(7) . ?
Ag15 Ag21 3.0097(9) . ?
Ag16 C91 2.157(7) . ?
Ag16 C401 2.221(7) . ?
Ag16 C402 2.693(7) . ?
Ag17 C301 2.235(7) . ?
Ag17 C51 2.343(7) . ?
Ag17 O42 2.413(6) . ?
Ag17 O3 2.592(4) . ?
Ag17 C52 2.617(8) . ?
Ag17 Ag24 3.0824(9) . ?
Ag18 C701 2.087(7) . ?
Ag18 C121 2.232(7) . ?
Ag18 C122 2.561(7) . ?
Ag19 C111 2.154(8) . ?
Ag19 C801 2.300(7) . ?
Ag19 C802 2.472(7) . ?
Ag20 C601 2.218(8) . ?
Ag20 C61 2.238(8) . ?
Ag20 C62 2.613(8) . ?
Ag21 C901 2.143(7) . ?
Ag21 C501 2.233(7) . ?
Ag21 C502 2.584(7) . ?
Ag22 C201 2.211(8) . ?
Ag22 C101 2.256(8) . ?
Ag22 O31 2.453(6) . ?
Ag22 Ag24 2.9417(10) . ?
Ag23 C81 2.191(7) . ?
Ag23 C91 2.275(7) . ?
Ag23 C92 2.494(8) . ?
Ag24 C201 2.167(7) . ?
Ag24 C301 2.231(7) . ?
Ag24 C302 2.523(7) . ?
C1 O1 1.263(7) . ?
C1 C4 1.450(9) . ?
C1 C2 1.453(8) . ?
C2 O2 1.265(7) . ?
C2 C3 1.442(9) . ?
C3 O3 1.269(7) . ?
C3 C4 1.456(8) . ?
C4 O4 1.263(7) . ?
C5 O5 1.263(7) . ?
C5 C8 1.451(9) . ?
C5 C6 1.468(9) . ?
C6 O6 1.254(8) . ?
C6 C7 1.460(9) . ?
C7 O7 1.257(7) . ?
C7 C8 1.480(9) . ?
C8 O8 1.253(8) . ?
C11 O11 1.222(10) . ?
C11 O12 1.222(10) . ?
C11 C12 1.543(12) . ?
C12 F12 1.279(12) . ?
C12 F14 1.282(14) . ?
C12 F13 1.288(13) . ?
C12 F15 1.312(16) . ?
C12 F11 1.355(11) . ?
C12 F16 1.359(15) . ?
C21 O22 1.227(11) . ?
C21 O21 1.240(11) . ?
C21 C22 1.540(14) . ?
C22 F25 1.249(18) . ?
C22 F21 1.270(14) . ?
C22 F24 1.293(19) . ?
C22 F23 1.342(14) . ?
C22 F26 1.354(19) . ?
C22 F22 1.377(14) . ?
C31 O32 1.208(11) . ?
C31 O31 1.209(12) . ?
C31 C32 1.522(13) . ?
C32 F32 1.223(12) . ?
C32 F31 1.322(13) . ?
C32 F33 1.326(11) . ?
C41 O42 1.218(10) . ?
C41 O41 1.224(9) . ?
C41 C42 1.506(12) . ?
C42 F46 1.301(18) . ?
C42 F42 1.306(14) . ?
C42 F44 1.320(18) . ?
C42 F43 1.327(13) . ?
C42 F45 1.337(17) . ?
C42 F41 1.345(13) . ?
C51 C52 1.215(10) . ?
C52 C53 1.479(11) . ?
C53 C59 1.46(2) . ?
C53 C54 1.479(13) . ?
C53 C57 1.53(2) . ?
C53 C58 1.53(2) . ?
C53 C56 1.531(13) . ?
C53 C55 1.569(13) . ?
C61 C62 1.222(10) . ?
C62 C63 1.494(12) . ?
C63 C66 1.472(12) . ?
C63 C65 1.494(12) . ?
C63 C64 1.497(12) . ?
C71 C72 1.201(9) . ?
C72 C73 1.473(10) . ?
C73 C74 1.463(11) . ?
C73 C76 1.480(12) . ?
C73 C79 1.507(19) . ?
C73 C78 1.526(19) . ?
C73 C75 1.570(12) . ?
C73 C77 1.602(18) . ?
C81 C82 1.224(9) . ?
C82 C83 1.494(9) . ?
C83 C84 1.523(12) . ?
C83 C86 1.526(11) . ?
C83 C85 1.528(12) . ?
C91 C92 1.193(10) . ?
C92 C93 1.485(11) . ?
C93 C96 1.483(10) . ?
C93 C95 1.495(11) . ?
C93 C94 1.505(10) . ?
C101 C102 1.202(10) . ?
C102 C103 1.484(11) . ?
C103 C105 1.498(13) . ?
C103 C104 1.513(12) . ?
C103 C106 1.539(13) . ?
C111 C112 1.199(9) . ?
C112 C113 1.474(10) . ?
C113 C116 1.511(14) . ?
C113 C114 1.521(13) . ?
C113 C115 1.531(13) . ?
C121 C122 1.220(9) . ?
C122 C123 1.474(10) . ?
C123 C126 1.492(12) . ?
C123 C125 1.502(13) . ?
C123 C124 1.549(13) . ?
C201 C202 1.216(9) . ?
C202 C203 1.467(10) . ?
C203 C204 1.504(12) . ?
C203 C205 1.505(14) . ?
C203 C206 1.506(16) . ?
C301 C302 1.213(9) . ?
C302 C303 1.503(9) . ?
C303 C305 1.497(14) . ?
C303 C306 1.521(12) . ?
C303 C304 1.523(13) . ?
C401 C402 1.199(9) . ?
C402 C403 1.482(11) . ?
C403 C406 1.496(10) . ?
C403 C404 1.500(10) . ?
C403 C405 1.515(10) . ?
C501 C502 1.206(9) . ?
C502 C503 1.493(10) . ?
C503 C509 1.46(2) . ?
C503 C505 1.486(12) . ?
C503 C508 1.49(2) . ?
C503 C507 1.54(2) . ?
C503 C506 1.544(12) . ?
C503 C504 1.578(12) . ?
C601 C602 1.208(9) . ?
C602 C603 1.477(10) . ?
C603 C605 1.446(12) . ?
C603 C604 1.452(16) . ?
C603 C606 1.548(15) . ?
C701 C702 1.210(9) . ?
C702 C703 1.488(10) . ?
C703 C704 1.530(11) . ?
C703 C706 1.531(12) . ?
C703 C705 1.547(12) . ?
C801 C802 1.204(9) . ?
C802 C803 1.494(10) . ?
C803 C804 1.467(14) . ?
C803 C805 1.522(14) . ?
C803 C806 1.531(13) . ?
C901 C902 1.204(9) . ?
C902 C903 1.480(10) . ?
C903 C905 1.524(11) . ?
C903 C906 1.528(11) . ?
C903 C904 1.530(10) . ?
C1S C2S 1.496(9) . ?
C1S C3S 1.497(9) . ?
C2S N1S 1.213(8) . ?
C3S N2S 1.209(8) . ?
N10S C40S 1.210(9) . ?
N10S C10S 1.220(8) . ?
C10S C20S 1.492(8) . ?
C40S C30S 1.494(9) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C121 Ag1 C51 163.3(3) . . ?
C121 Ag1 O41 92.4(2) . . ?
C51 Ag1 O41 102.9(2) . . ?
C121 Ag1 Ag6 118.80(19) . . ?
C51 Ag1 Ag6 48.1(2) . . ?
O41 Ag1 Ag6 146.90(13) . . ?
C121 Ag1 Ag7 47.66(19) . . ?
C51 Ag1 Ag7 118.1(2) . . ?
O41 Ag1 Ag7 138.78(13) . . ?
Ag6 Ag1 Ag7 71.14(2) . . ?
C121 Ag1 Ag18 47.02(18) . . ?
C51 Ag1 Ag18 147.8(2) . . ?
O41 Ag1 Ag18 62.10(14) . . ?
Ag6 Ag1 Ag18 131.38(2) . . ?
Ag7 Ag1 Ag18 79.77(2) . . ?
C121 Ag1 Ag17 145.96(18) . . ?
C51 Ag1 Ag17 47.2(2) . . ?
O41 Ag1 Ag17 76.07(14) . . ?
Ag6 Ag1 Ag17 71.74(2) . . ?
Ag7 Ag1 Ag17 129.15(2) . . ?
Ag18 Ag1 Ag17 100.55(2) . . ?
C401 Ag2 C801 165.6(3) . . ?
C401 Ag2 O12 110.5(2) . . ?
C801 Ag2 O12 83.9(2) . . ?
C401 Ag2 Ag14 119.04(18) . . ?
C801 Ag2 Ag14 46.9(2) . . ?
O12 Ag2 Ag14 128.52(16) . . ?
C401 Ag2 Ag16 49.18(18) . . ?
C801 Ag2 Ag16 117.0(2) . . ?
O12 Ag2 Ag16 153.62(14) . . ?
Ag14 Ag2 Ag16 70.02(2) . . ?
C401 Ag2 Ag10 47.72(19) . . ?
C801 Ag2 Ag10 140.1(2) . . ?
O12 Ag2 Ag10 76.73(14) . . ?
Ag14 Ag2 Ag10 128.63(2) . . ?
Ag16 Ag2 Ag10 76.88(2) . . ?
C401 Ag2 Ag19 140.88(19) . . ?
C801 Ag2 Ag19 46.3(2) . . ?
O12 Ag2 Ag19 58.15(17) . . ?
Ag14 Ag2 Ag19 74.27(2) . . ?
Ag16 Ag2 Ag19 123.84(2) . . ?
Ag10 Ag2 Ag19 94.24(2) . . ?
C901 Ag3 C111 151.7(3) . . ?
C901 Ag3 O4 100.7(2) . . ?
C111 Ag3 O4 96.6(2) . . ?
C901 Ag3 Ag21 45.65(18) . . ?
C111 Ag3 Ag21 154.5(2) . . ?
O4 Ag3 Ag21 94.37(11) . . ?
C901 Ag3 Ag19 149.82(19) . . ?
C111 Ag3 Ag19 45.3(2) . . ?
O4 Ag3 Ag19 98.86(10) . . ?
Ag21 Ag3 Ag19 110.19(2) . . ?
C901 Ag3 Ag13 151.00(18) . . ?
C111 Ag3 Ag13 43.21(19) . . ?
O4 Ag3 Ag13 53.88(10) . . ?
Ag21 Ag3 Ag13 137.77(2) . . ?
Ag19 Ag3 Ag13 57.733(19) . . ?
C501 Ag4 C601 143.7(3) . . ?
C501 Ag4 O6 126.0(2) . . ?
C601 Ag4 O6 89.6(2) . . ?
C501 Ag4 C602 116.1(2) . . ?
C601 Ag4 C602 27.7(2) . . ?
O6 Ag4 C602 116.13(18) . . ?
C501 Ag4 Ag10 48.43(18) . . ?
C601 Ag4 Ag10 159.66(19) . . ?
O6 Ag4 Ag10 78.20(10) . . ?
C602 Ag4 Ag10 152.64(17) . . ?
C501 Ag4 Ag21 43.95(19) . . ?
C601 Ag4 Ag21 141.28(19) . . ?
O6 Ag4 Ag21 105.67(10) . . ?
C602 Ag4 Ag21 130.28(16) . . ?
Ag10 Ag4 Ag21 58.717(18) . . ?
C501 Ag4 Ag20 130.09(19) . . ?
C601 Ag4 Ag20 41.46(19) . . ?
O6 Ag4 Ag20 92.96(11) . . ?
C602 Ag4 Ag20 52.96(17) . . ?
Ag10 Ag4 Ag20 153.74(3) . . ?
Ag21 Ag4 Ag20 101.29(2) . . ?
C61 Ag5 C71 156.9(3) . . ?
C61 Ag5 O21 104.2(3) . . ?
C71 Ag5 O21 95.2(2) . . ?
C61 Ag5 Ag7 116.1(2) . . ?
C71 Ag5 Ag7 46.95(18) . . ?
O21 Ag5 Ag7 139.43(15) . . ?
C61 Ag5 Ag15 147.5(2) . . ?
C71 Ag5 Ag15 47.25(18) . . ?
O21 Ag5 Ag15 81.31(15) . . ?
Ag7 Ag5 Ag15 62.632(19) . . ?
C61 Ag5 Ag6 46.6(2) . . ?
C71 Ag5 Ag6 113.40(18) . . ?
O21 Ag5 Ag6 150.84(16) . . ?
Ag7 Ag5 Ag6 69.57(2) . . ?
Ag15 Ag5 Ag6 122.03(2) . . ?
C61 Ag5 Ag20 45.9(2) . . ?
C71 Ag5 Ag20 151.56(18) . . ?
O21 Ag5 Ag20 83.37(19) . . ?
Ag7 Ag5 Ag20 121.80(2) . . ?
Ag15 Ag5 Ag20 104.80(2) . . ?
Ag6 Ag5 Ag20 74.23(2) . . ?
C51 Ag6 C61 157.6(3) . . ?
C51 Ag6 C62 130.4(3) . . ?
C61 Ag6 C62 27.7(2) . . ?
C51 Ag6 Ag1 48.4(2) . . ?
C61 Ag6 Ag1 153.62(19) . . ?
C62 Ag6 Ag1 178.71(17) . . ?
C51 Ag6 Ag5 155.7(2) . . ?
C61 Ag6 Ag5 43.87(19) . . ?
C62 Ag6 Ag5 71.35(17) . . ?
Ag1 Ag6 Ag5 109.91(2) . . ?
C71 Ag7 C121 154.4(3) . . ?
C71 Ag7 C122 130.0(3) . . ?
C121 Ag7 C122 27.3(2) . . ?
C71 Ag7 Ag5 48.3(2) . . ?
C121 Ag7 Ag5 154.27(18) . . ?
C122 Ag7 Ag5 178.25(16) . . ?
C71 Ag7 Ag1 151.08(18) . . ?
C121 Ag7 Ag1 44.89(18) . . ?
C122 Ag7 Ag1 72.18(16) . . ?
Ag5 Ag7 Ag1 109.39(2) . . ?
C71 Ag7 Ag15 46.14(19) . . ?
C121 Ag7 Ag15 138.96(17) . . ?
C122 Ag7 Ag15 118.61(16) . . ?
Ag5 Ag7 Ag15 60.523(19) . . ?
Ag1 Ag7 Ag15 147.51(3) . . ?
C201 Ag8 C701 140.1(3) . . ?
C201 Ag8 O3 120.2(2) . . ?
C701 Ag8 O3 93.29(19) . . ?
C201 Ag8 O8 116.1(2) . . ?
C701 Ag8 O8 86.7(2) . . ?
O3 Ag8 O8 83.52(14) . . ?
C201 Ag8 C702 116.6(2) . . ?
C701 Ag8 C702 27.7(2) . . ?
O3 Ag8 C702 120.72(19) . . ?
O8 Ag8 C702 86.37(18) . . ?
C201 Ag8 Ag24 47.04(18) . . ?
C701 Ag8 Ag24 156.13(18) . . ?
O3 Ag8 Ag24 73.22(9) . . ?
O8 Ag8 Ag24 110.53(10) . . ?
C702 Ag8 Ag24 160.08(16) . . ?
C201 Ag8 Ag22 45.7(2) . . ?
C701 Ag8 Ag22 145.59(18) . . ?
O3 Ag8 Ag22 109.25(11) . . ?
O8 Ag8 Ag22 71.01(11) . . ?
C702 Ag8 Ag22 121.88(16) . . ?
Ag24 Ag8 Ag22 58.20(2) . . ?
C201 Ag8 Ag18 150.9(2) . . ?
C701 Ag8 Ag18 38.05(17) . . ?
O3 Ag8 Ag18 56.81(10) . . ?
O8 Ag8 Ag18 92.87(11) . . ?
C702 Ag8 Ag18 65.65(16) . . ?
Ag24 Ag8 Ag18 121.68(3) . . ?
Ag22 Ag8 Ag18 160.66(3) . . ?
C301 Ag9 C81 139.4(2) . . ?
C301 Ag9 O2 129.5(2) . . ?
C81 Ag9 O2 89.1(2) . . ?
C301 Ag9 C82 111.4(2) . . ?
C81 Ag9 C82 28.5(2) . . ?
O2 Ag9 C82 113.75(19) . . ?
C301 Ag9 Ag17 50.1(2) . . ?
C81 Ag9 Ag17 161.18(17) . . ?
O2 Ag9 Ag17 79.38(11) . . ?
C82 Ag9 Ag17 148.85(16) . . ?
C301 Ag9 Ag24 41.91(18) . . ?
C81 Ag9 Ag24 139.61(17) . . ?
O2 Ag9 Ag24 115.18(11) . . ?
C82 Ag9 Ag24 127.82(15) . . ?
Ag17 Ag9 Ag24 59.21(2) . . ?
C301 Ag9 Ag23 130.9(2) . . ?
C81 Ag9 Ag23 40.86(17) . . ?
O2 Ag9 Ag23 93.02(11) . . ?
C82 Ag9 Ag23 57.30(16) . . ?
Ag17 Ag9 Ag23 153.38(3) . . ?
Ag24 Ag9 Ag23 102.99(2) . . ?
C501 Ag10 C401 147.3(3) . . ?
C501 Ag10 O11 94.8(2) . . ?
C401 Ag10 O11 112.6(2) . . ?
C501 Ag10 C402 120.1(2) . . ?
C401 Ag10 C402 27.9(2) . . ?
O11 Ag10 C402 127.0(2) . . ?
C501 Ag10 Ag4 45.10(17) . . ?
C401 Ag10 Ag4 115.22(17) . . ?
O11 Ag10 Ag4 131.34(14) . . ?
C402 Ag10 Ag4 100.22(15) . . ?
C501 Ag10 Ag21 46.87(18) . . ?
C401 Ag10 Ag21 160.58(18) . . ?
O11 Ag10 Ag21 68.05(14) . . ?
C402 Ag10 Ag21 163.86(15) . . ?
Ag4 Ag10 Ag21 63.940(19) . . ?
C501 Ag10 Ag2 166.84(18) . . ?
C401 Ag10 Ag2 42.96(19) . . ?
O11 Ag10 Ag2 82.50(14) . . ?
C402 Ag10 Ag2 70.84(17) . . ?
Ag4 Ag10 Ag2 129.43(2) . . ?
Ag21 Ag10 Ag2 120.90(2) . . ?
C101 Ag11 C91 162.8(3) . . ?
C101 Ag11 O32 100.8(3) . . ?
C91 Ag11 O32 93.1(3) . . ?
C101 Ag11 Ag16 117.4(2) . . ?
C91 Ag11 Ag16 48.32(19) . . ?
O32 Ag11 Ag16 141.35(19) . . ?
C101 Ag11 Ag14 47.76(19) . . ?
C91 Ag11 Ag14 118.85(19) . . ?
O32 Ag11 Ag14 148.08(19) . . ?
Ag16 Ag11 Ag14 70.56(2) . . ?
C101 Ag11 Ag23 147.2(2) . . ?
C91 Ag11 Ag23 46.68(19) . . ?
O32 Ag11 Ag23 75.5(2) . . ?
Ag16 Ag11 Ag23 75.03(2) . . ?
Ag14 Ag11 Ag23 126.05(2) . . ?
C101 Ag11 Ag22 45.2(2) . . ?
C91 Ag11 Ag22 149.13(19) . . ?
O32 Ag11 Ag22 80.53(19) . . ?
Ag16 Ag11 Ag22 130.34(2) . . ?
Ag14 Ag11 Ag22 72.22(2) . . ?
Ag23 Ag11 Ag22 102.77(2) . . ?
C81 Ag12 C601 167.9(3) . . ?
C81 Ag12 Ag23 48.05(19) . . ?
C601 Ag12 Ag23 139.9(2) . . ?
C81 Ag12 Ag20 133.4(2) . . ?
C601 Ag12 Ag20 47.8(2) . . ?
Ag23 Ag12 Ag20 146.91(3) . . ?
C111 Ag13 C701 157.5(3) . . ?
C111 Ag13 C702 138.6(2) . . ?
C701 Ag13 C702 26.9(2) . . ?
C111 Ag13 Ag19 45.4(2) . . ?
C701 Ag13 Ag19 146.49(18) . . ?
C702 Ag13 Ag19 124.35(15) . . ?
C111 Ag13 Ag18 139.50(19) . . ?
C701 Ag13 Ag18 42.97(18) . . ?
C702 Ag13 Ag18 69.72(15) . . ?
Ag19 Ag13 Ag18 155.21(3) . . ?
C111 Ag13 Ag3 43.26(18) . . ?
C701 Ag13 Ag3 150.69(18) . . ?
C702 Ag13 Ag3 177.52(15) . . ?
Ag19 Ag13 Ag3 58.018(18) . . ?
Ag18 Ag13 Ag3 107.82(2) . . ?
C801 Ag14 C101 154.8(3) . . ?
C801 Ag14 Ag2 47.9(2) . . ?
C101 Ag14 Ag2 154.8(2) . . ?
C801 Ag14 Ag11 157.4(2) . . ?
C101 Ag14 Ag11 47.1(2) . . ?
Ag2 Ag14 Ag11 109.49(3) . . ?
C801 Ag14 Ag16 103.3(2) . . ?
C101 Ag14 Ag16 100.5(2) . . ?
Ag2 Ag14 Ag16 55.402(17) . . ?
Ag11 Ag14 Ag16 54.090(18) . . ?
C71 Ag15 C901 153.8(3) . . ?
C71 Ag15 O22 97.6(2) . . ?
C901 Ag15 O22 99.8(2) . . ?
C71 Ag15 C902 133.5(2) . . ?
C901 Ag15 C902 26.7(2) . . ?
O22 Ag15 C902 92.7(2) . . ?
C71 Ag15 Ag21 159.94(18) . . ?
C901 Ag15 Ag21 45.26(17) . . ?
O22 Ag15 Ag21 76.70(16) . . ?
C902 Ag15 Ag21 66.48(15) . . ?
C71 Ag15 Ag5 46.05(18) . . ?
C901 Ag15 Ag5 157.57(17) . . ?
O22 Ag15 Ag5 79.18(14) . . ?
C902 Ag15 Ag5 171.33(17) . . ?
Ag21 Ag15 Ag5 113.95(3) . . ?
C71 Ag15 Ag7 43.77(17) . . ?
C901 Ag15 Ag7 125.41(17) . . ?
O22 Ag15 Ag7 134.34(15) . . ?
C902 Ag15 Ag7 130.22(16) . . ?
Ag21 Ag15 Ag7 129.56(2) . . ?
Ag5 Ag15 Ag7 56.845(18) . . ?
C91 Ag16 C401 154.8(3) . . ?
C91 Ag16 C402 128.9(3) . . ?
C401 Ag16 C402 26.1(2) . . ?
C91 Ag16 Ag11 48.8(2) . . ?
C401 Ag16 Ag11 155.75(19) . . ?
C402 Ag16 Ag11 175.53(15) . . ?
C91 Ag16 Ag2 158.7(2) . . ?
C401 Ag16 Ag2 46.13(19) . . ?
C402 Ag16 Ag2 72.18(15) . . ?
Ag11 Ag16 Ag2 109.92(3) . . ?
C91 Ag16 Ag14 104.1(2) . . ?
C401 Ag16 Ag14 100.59(19) . . ?
C402 Ag16 Ag14 126.60(15) . . ?
Ag11 Ag16 Ag14 55.345(18) . . ?
Ag2 Ag16 Ag14 54.577(18) . . ?
C301 Ag17 C51 147.5(3) . . ?
C301 Ag17 O42 96.5(2) . . ?
C51 Ag17 O42 103.5(3) . . ?
C301 Ag17 O3 109.0(2) . . ?
C51 Ag17 O3 99.0(2) . . ?
O42 Ag17 O3 82.5(2) . . ?
C301 Ag17 C52 126.3(2) . . ?
C51 Ag17 C52 27.6(2) . . ?
O42 Ag17 C52 95.0(3) . . ?
O3 Ag17 C52 124.52(19) . . ?
C301 Ag17 Ag9 47.52(19) . . ?
C51 Ag17 Ag9 122.03(19) . . ?
O42 Ag17 Ag9 134.10(17) . . ?
O3 Ag17 Ag9 84.67(11) . . ?
C52 Ag17 Ag9 127.91(18) . . ?
C301 Ag17 Ag24 46.30(18) . . ?
C51 Ag17 Ag24 166.12(18) . . ?
O42 Ag17 Ag24 66.97(17) . . ?
O3 Ag17 Ag24 70.44(10) . . ?
C52 Ag17 Ag24 156.22(17) . . ?
Ag9 Ag17 Ag24 67.19(2) . . ?
C301 Ag17 Ag1 169.84(17) . . ?
C51 Ag17 Ag1 42.16(18) . . ?
O42 Ag17 Ag1 80.65(16) . . ?
O3 Ag17 Ag1 61.07(10) . . ?
C52 Ag17 Ag1 63.85(16) . . ?
Ag9 Ag17 Ag1 129.02(2) . . ?
Ag24 Ag17 Ag1 124.31(3) . . ?
C701 Ag18 C121 171.5(3) . . ?
C701 Ag18 C122 143.1(2) . . ?
C121 Ag18 C122 28.4(2) . . ?
C701 Ag18 Ag1 144.63(18) . . ?
C121 Ag18 Ag1 43.85(18) . . ?
C122 Ag18 Ag1 72.23(16) . . ?
C701 Ag18 Ag13 47.01(19) . . ?
C121 Ag18 Ag13 128.11(18) . . ?
C122 Ag18 Ag13 111.12(16) . . ?
Ag1 Ag18 Ag13 138.28(3) . . ?
C701 Ag18 Ag8 44.09(18) . . ?
C121 Ag18 Ag8 143.68(18) . . ?
C122 Ag18 Ag8 167.77(17) . . ?
Ag1 Ag18 Ag8 101.58(2) . . ?
Ag13 Ag18 Ag8 66.148(19) . . ?
C111 Ag19 C801 157.4(3) . . ?
C111 Ag19 C802 129.5(2) . . ?
C801 Ag19 C802 28.9(2) . . ?
C111 Ag19 Ag13 46.89(19) . . ?
C801 Ag19 Ag13 127.78(18) . . ?
C802 Ag19 Ag13 122.59(17) . . ?
C111 Ag19 Ag3 46.77(19) . . ?
C801 Ag19 Ag3 155.88(19) . . ?
C802 Ag19 Ag3 168.72(16) . . ?
Ag13 Ag19 Ag3 64.248(19) . . ?
C111 Ag19 Ag2 158.5(2) . . ?
C801 Ag19 Ag2 42.61(19) . . ?
C802 Ag19 Ag2 67.19(17) . . ?
Ag13 Ag19 Ag2 141.37(2) . . ?
Ag3 Ag19 Ag2 113.89(2) . . ?
C601 Ag20 C61 164.7(3) . . ?
C601 Ag20 C62 137.5(2) . . ?
C61 Ag20 C62 27.8(2) . . ?
C601 Ag20 Ag12 44.34(18) . . ?
C61 Ag20 Ag12 131.48(19) . . ?
C62 Ag20 Ag12 110.60(18) . . ?
C601 Ag20 Ag5 150.51(17) . . ?
C61 Ag20 Ag5 42.47(19) . . ?
C62 Ag20 Ag5 70.14(18) . . ?
Ag12 Ag20 Ag5 150.80(3) . . ?
C601 Ag20 Ag4 43.72(17) . . ?
C61 Ag20 Ag4 151.52(19) . . ?
C62 Ag20 Ag4 173.26(18) . . ?
Ag12 Ag20 Ag4 65.428(19) . . ?
Ag5 Ag20 Ag4 110.43(2) . . ?
C901 Ag21 C501 159.0(2) . . ?
C901 Ag21 C502 131.2(2) . . ?
C501 Ag21 C502 27.8(2) . . ?
C901 Ag21 Ag3 46.03(18) . . ?
C501 Ag21 Ag3 147.93(17) . . ?
C502 Ag21 Ag3 149.89(15) . . ?
C901 Ag21 Ag15 48.93(17) . . ?
C501 Ag21 Ag15 133.96(17) . . ?
C502 Ag21 Ag15 128.18(15) . . ?
Ag3 Ag21 Ag15 75.38(2) . . ?
C901 Ag21 Ag10 139.57(17) . . ?
C501 Ag21 Ag10 47.42(17) . . ?
C502 Ag21 Ag10 63.62(15) . . ?
Ag3 Ag21 Ag10 100.52(2) . . ?
Ag15 Ag21 Ag10 160.12(3) . . ?
C901 Ag21 Ag4 156.00(18) . . ?
C501 Ag21 Ag4 41.53(17) . . ?
C502 Ag21 Ag4 67.85(15) . . ?
Ag3 Ag21 Ag4 127.13(2) . . ?
Ag15 Ag21 Ag4 109.24(2) . . ?
Ag10 Ag21 Ag4 57.342(18) . . ?
C201 Ag22 C101 154.5(3) . . ?
C201 Ag22 O31 96.3(2) . . ?
C101 Ag22 O31 98.0(3) . . ?
C201 Ag22 Ag24 47.14(18) . . ?
C101 Ag22 Ag24 158.4(2) . . ?
O31 Ag22 Ag24 70.14(18) . . ?
C201 Ag22 Ag8 44.73(18) . . ?
C101 Ag22 Ag8 131.92(19) . . ?
O31 Ag22 Ag8 128.45(18) . . ?
Ag24 Ag22 Ag8 58.52(2) . . ?
C201 Ag22 Ag11 163.16(18) . . ?
C101 Ag22 Ag11 42.3(2) . . ?
O31 Ag22 Ag11 75.95(17) . . ?
Ag24 Ag22 Ag11 116.10(3) . . ?
Ag8 Ag22 Ag11 129.98(3) . . ?
C81 Ag23 C91 161.9(3) . . ?
C81 Ag23 C92 134.2(3) . . ?
C91 Ag23 C92 28.5(2) . . ?
C81 Ag23 Ag12 44.93(17) . . ?
C91 Ag23 Ag12 128.65(19) . . ?
C92 Ag23 Ag12 120.48(17) . . ?
C81 Ag23 Ag11 153.13(19) . . ?
C91 Ag23 Ag11 44.0(2) . . ?
C92 Ag23 Ag11 68.55(18) . . ?
Ag12 Ag23 Ag11 145.08(3) . . ?
C81 Ag23 Ag9 44.70(19) . . ?
C91 Ag23 Ag9 153.4(2) . . ?
C92 Ag23 Ag9 169.67(16) . . ?
Ag12 Ag23 Ag9 66.92(2) . . ?
Ag11 Ag23 Ag9 110.00(3) . . ?
C201 Ag24 C301 170.9(3) . . ?
C201 Ag24 C302 143.7(2) . . ?
C301 Ag24 C302 28.7(2) . . ?
C201 Ag24 Ag22 48.4(2) . . ?
C301 Ag24 Ag22 139.7(2) . . ?
C302 Ag24 Ag22 141.80(18) . . ?
C201 Ag24 Ag8 47.31(18) . . ?
C301 Ag24 Ag8 136.02(18) . . ?
C302 Ag24 Ag8 154.80(17) . . ?
Ag22 Ag24 Ag8 63.28(2) . . ?
C201 Ag24 Ag17 132.6(2) . . ?
C301 Ag24 Ag17 46.42(19) . . ?
C302 Ag24 Ag17 66.51(16) . . ?
Ag22 Ag24 Ag17 140.46(3) . . ?
Ag8 Ag24 Ag17 91.15(3) . . ?
C201 Ag24 Ag9 148.91(19) . . ?
C301 Ag24 Ag9 40.04(18) . . ?
C302 Ag24 Ag9 66.51(17) . . ?
Ag22 Ag24 Ag9 105.26(3) . . ?
Ag8 Ag24 Ag9 110.37(3) . . ?
Ag17 Ag24 Ag9 53.604(19) . . ?
O1 C1 C4 135.8(6) . . ?
O1 C1 C2 134.4(6) . . ?
C4 C1 C2 89.8(5) . . ?
O2 C2 C3 136.3(6) . . ?
O2 C2 C1 133.3(6) . . ?
C3 C2 C1 90.4(5) . . ?
O3 C3 C2 133.9(6) . . ?
O3 C3 C4 136.2(6) . . ?
C2 C3 C4 89.9(5) . . ?
O4 C4 C1 136.4(6) . . ?
O4 C4 C3 133.7(6) . . ?
C1 C4 C3 89.9(5) . . ?
C2 O2 Ag9 120.5(4) . . ?
C3 O3 Ag8 130.2(4) . . ?
C3 O3 Ag17 111.1(4) . . ?
Ag8 O3 Ag17 113.90(15) . . ?
C4 O4 Ag3 126.3(4) . . ?
O5 C5 C8 134.8(6) . . ?
O5 C5 C6 134.4(6) . . ?
C8 C5 C6 90.8(5) . . ?
O6 C6 C7 134.6(6) . . ?
O6 C6 C5 135.8(6) . . ?
C7 C6 C5 89.7(5) . . ?
O7 C7 C6 134.8(6) . . ?
O7 C7 C8 135.2(6) . . ?
C6 C7 C8 89.9(5) . . ?
O8 C8 C5 135.5(6) . . ?
O8 C8 C7 134.8(6) . . ?
C5 C8 C7 89.6(5) . . ?
C6 O6 Ag4 122.4(4) . . ?
C8 O8 Ag8 119.1(4) . . ?
O11 C11 O12 131.4(8) . . ?
O11 C11 C12 115.8(8) . . ?
O12 C11 C12 112.8(8) . . ?
F12 C12 F14 60.3(9) . . ?
F12 C12 F13 110.4(10) . . ?
F14 C12 F13 129.8(12) . . ?
F12 C12 F15 128.8(15) . . ?
F14 C12 F15 106.6(11) . . ?
F13 C12 F15 36.8(9) . . ?
F12 C12 F11 106.3(9) . . ?
F14 C12 F11 47.6(8) . . ?
F13 C12 F11 104.2(9) . . ?
F15 C12 F11 68.5(10) . . ?
F12 C12 F16 46.2(9) . . ?
F14 C12 F16 102.8(11) . . ?
F13 C12 F16 69.6(11) . . ?
F15 C12 F16 102.1(12) . . ?
F11 C12 F16 137.5(11) . . ?
F12 C12 C11 113.8(9) . . ?
F14 C12 C11 116.4(11) . . ?
F13 C12 C11 112.1(9) . . ?
F15 C12 C11 115.7(13) . . ?
F11 C12 C11 109.4(9) . . ?
F16 C12 C11 111.7(10) . . ?
C11 O11 Ag10 122.7(5) . . ?
C11 O12 Ag2 126.5(5) . . ?
O22 C21 O21 130.0(8) . . ?
O22 C21 C22 114.8(9) . . ?
O21 C21 C22 115.2(9) . . ?
F25 C22 F21 122.6(18) . . ?
F25 C22 F24 110.3(14) . . ?
F21 C22 F24 51.1(10) . . ?
F25 C22 F23 43.4(11) . . ?
F21 C22 F23 111.1(12) . . ?
F24 C22 F23 140.1(16) . . ?
F25 C22 F26 105.0(13) . . ?
F21 C22 F26 50.3(10) . . ?
F24 C22 F26 101.2(13) . . ?
F23 C22 F26 69.1(11) . . ?
F25 C22 F22 59.0(12) . . ?
F21 C22 F22 106.6(11) . . ?
F24 C22 F22 61.1(11) . . ?
F23 C22 F22 102.4(10) . . ?
F26 C22 F22 142.4(13) . . ?
F25 C22 C21 120.4(15) . . ?
F21 C22 C21 116.7(11) . . ?
F24 C22 C21 110.4(14) . . ?
F23 C22 C21 109.4(10) . . ?
F26 C22 C21 107.6(12) . . ?
F22 C22 C21 109.6(10) . . ?
C21 O21 Ag5 122.6(6) . . ?
C21 O22 Ag15 122.9(6) . . ?
O32 C31 O31 130.4(10) . . ?
O32 C31 C32 116.7(10) . . ?
O31 C31 C32 112.9(10) . . ?
F32 C32 F31 106.9(11) . . ?
F32 C32 F33 110.3(12) . . ?
F31 C32 F33 99.4(9) . . ?
F32 C32 C31 115.2(9) . . ?
F31 C32 C31 113.4(11) . . ?
F33 C32 C31 110.5(9) . . ?
C31 O31 Ag22 122.9(6) . . ?
C31 O32 Ag11 121.6(6) . . ?
O42 C41 O41 129.9(8) . . ?
O42 C41 C42 115.3(8) . . ?
O41 C41 C42 114.7(8) . . ?
F46 C42 F42 124.8(16) . . ?
F46 C42 F44 106.4(13) . . ?
F42 C42 F44 33.3(11) . . ?
F46 C42 F43 66.2(11) . . ?
F42 C42 F43 105.6(10) . . ?
F44 C42 F43 127.4(15) . . ?
F46 C42 F45 105.8(12) . . ?
F42 C42 F45 72.6(10) . . ?
F44 C42 F45 104.4(12) . . ?
F43 C42 F45 41.8(9) . . ?
F46 C42 F41 39.2(11) . . ?
F42 C42 F41 104.6(10) . . ?
F44 C42 F41 74.8(12) . . ?
F43 C42 F41 103.5(10) . . ?
F45 C42 F41 136.5(13) . . ?
F46 C42 C41 117.0(13) . . ?
F42 C42 C41 115.5(11) . . ?
F44 C42 C41 114.3(14) . . ?
F43 C42 C41 114.6(9) . . ?
F45 C42 C41 107.9(12) . . ?
F41 C42 C41 111.7(10) . . ?
C41 O41 Ag1 128.8(6) . . ?
C41 O42 Ag17 123.8(6) . . ?
C52 C51 Ag6 140.6(7) . . ?
C52 C51 Ag1 133.9(7) . . ?
Ag6 C51 Ag1 83.5(2) . . ?
C52 C51 Ag17 88.8(5) . . ?
Ag6 C51 Ag17 104.8(3) . . ?
Ag1 C51 Ag17 90.6(3) . . ?
C51 C52 C53 174.1(9) . . ?
C51 C52 Ag17 63.5(5) . . ?
C53 C52 Ag17 122.2(5) . . ?
C59 C53 C52 117.9(15) . . ?
C59 C53 C54 128.9(16) . . ?
C52 C53 C54 112.6(9) . . ?
C59 C53 C57 110.6(12) . . ?
C52 C53 C57 106.3(14) . . ?
C54 C53 C57 59.9(12) . . ?
C59 C53 C58 110.7(12) . . ?
C52 C53 C58 104.8(14) . . ?
C54 C53 C58 46.0(12) . . ?
C57 C53 C58 105.8(12) . . ?
C59 C53 C56 59.4(13) . . ?
C52 C53 C56 108.1(8) . . ?
C54 C53 C56 111.8(9) . . ?
C57 C53 C56 57.5(13) . . ?
C58 C53 C56 146.2(14) . . ?
C59 C53 C55 46.1(13) . . ?
C52 C53 C55 108.1(8) . . ?
C54 C53 C55 110.6(8) . . ?
C57 C53 C55 145.1(14) . . ?
C58 C53 C55 70.8(12) . . ?
C56 C53 C55 105.4(8) . . ?
C62 C61 Ag5 171.0(6) . . ?
C62 C61 Ag6 95.3(6) . . ?
Ag5 C61 Ag6 89.5(3) . . ?
C62 C61 Ag20 93.4(6) . . ?
Ag5 C61 Ag20 91.7(3) . . ?
Ag6 C61 Ag20 113.4(3) . . ?
C61 C62 C63 177.8(9) . . ?
C61 C62 Ag20 58.8(5) . . ?
C63 C62 Ag20 123.2(6) . . ?
C61 C62 Ag6 57.0(5) . . ?
C63 C62 Ag6 123.0(6) . . ?
Ag20 C62 Ag6 90.5(2) . . ?
C66 C63 C62 107.4(9) . . ?
C66 C63 C65 109.3(9) . . ?
C62 C63 C65 108.3(9) . . ?
C66 C63 C64 111.7(9) . . ?
C62 C63 C64 110.1(8) . . ?
C65 C63 C64 109.9(10) . . ?
C72 C71 Ag7 135.3(6) . . ?
C72 C71 Ag5 122.7(6) . . ?
Ag7 C71 Ag5 84.7(2) . . ?
C72 C71 Ag15 122.8(5) . . ?
Ag7 C71 Ag15 90.1(3) . . ?
Ag5 C71 Ag15 86.7(3) . . ?
C71 C72 C73 178.6(8) . . ?
C74 C73 C72 111.7(7) . . ?
C74 C73 C76 114.9(8) . . ?
C72 C73 C76 110.0(8) . . ?
C74 C73 C79 134.5(14) . . ?
C72 C73 C79 113.8(13) . . ?
C76 C73 C79 46.5(10) . . ?
C74 C73 C78 49.2(10) . . ?
C72 C73 C78 110.8(11) . . ?
C76 C73 C78 139.1(13) . . ?
C79 C73 C78 112.5(11) . . ?
C74 C73 C75 106.6(8) . . ?
C72 C73 C75 107.6(7) . . ?
C76 C73 C75 105.5(8) . . ?
C79 C73 C75 60.0(10) . . ?
C78 C73 C75 59.8(10) . . ?
C74 C73 C77 57.9(9) . . ?
C72 C73 C77 106.8(10) . . ?
C76 C73 C77 63.5(9) . . ?
C79 C73 C77 106.7(11) . . ?
C78 C73 C77 105.6(10) . . ?
C75 C73 C77 145.5(11) . . ?
C82 C81 Ag12 157.3(6) . . ?
C82 C81 Ag23 113.8(6) . . ?
Ag12 C81 Ag23 87.0(2) . . ?
C82 C81 Ag9 85.0(5) . . ?
Ag12 C81 Ag9 103.1(3) . . ?
Ag23 C81 Ag9 94.4(2) . . ?
C81 C82 C83 173.5(8) . . ?
C81 C82 Ag9 66.5(5) . . ?
C83 C82 Ag9 120.0(5) . . ?
C82 C83 C84 108.6(7) . . ?
C82 C83 C86 108.1(6) . . ?
C84 C83 C86 110.3(7) . . ?
C82 C83 C85 107.5(7) . . ?
C84 C83 C85 111.5(8) . . ?
C86 C83 C85 110.7(8) . . ?
C92 C91 Ag16 132.7(7) . . ?
C92 C91 Ag11 143.0(6) . . ?
Ag16 C91 Ag11 82.9(3) . . ?
C92 C91 Ag23 86.0(5) . . ?
Ag16 C91 Ag23 111.1(3) . . ?
Ag11 C91 Ag23 89.3(3) . . ?
C91 C92 C93 173.2(8) . . ?
C91 C92 Ag23 65.5(5) . . ?
C93 C92 Ag23 120.2(5) . . ?
C96 C93 C92 111.4(7) . . ?
C96 C93 C95 111.3(8) . . ?
C92 C93 C95 108.5(8) . . ?
C96 C93 C94 109.7(8) . . ?
C92 C93 C94 107.6(7) . . ?
C95 C93 C94 108.2(8) . . ?
C102 C101 Ag11 151.0(7) . . ?
C102 C101 Ag14 112.4(6) . . ?
Ag11 C101 Ag14 85.1(3) . . ?
C102 C101 Ag22 102.6(6) . . ?
Ag11 C101 Ag22 92.5(3) . . ?
Ag14 C101 Ag22 108.8(3) . . ?
C101 C102 C103 174.7(8) . . ?
C102 C103 C105 108.8(7) . . ?
C102 C103 C104 108.3(7) . . ?
C105 C103 C104 112.2(9) . . ?
C102 C103 C106 109.4(8) . . ?
C105 C103 C106 109.7(10) . . ?
C104 C103 C106 108.5(9) . . ?
C112 C111 Ag19 139.7(6) . . ?
C112 C111 Ag13 112.9(6) . . ?
Ag19 C111 Ag13 87.7(3) . . ?
C112 C111 Ag3 122.8(6) . . ?
Ag19 C111 Ag3 88.0(3) . . ?
Ag13 C111 Ag3 93.5(3) . . ?
C111 C112 C113 177.5(8) . . ?
C112 C113 C116 109.3(8) . . ?
C112 C113 C114 109.1(8) . . ?
C116 C113 C114 108.3(8) . . ?
C112 C113 C115 108.3(7) . . ?
C116 C113 C115 111.9(10) . . ?
C114 C113 C115 110.0(10) . . ?
C122 C121 Ag1 175.6(6) . . ?
C122 C121 Ag7 96.3(5) . . ?
Ag1 C121 Ag7 87.5(3) . . ?
C122 C121 Ag18 90.9(5) . . ?
Ag1 C121 Ag18 89.1(3) . . ?
Ag7 C121 Ag18 121.3(3) . . ?
C121 C122 C123 175.7(7) . . ?
C121 C122 Ag18 60.6(4) . . ?
C123 C122 Ag18 123.6(5) . . ?
C121 C122 Ag7 56.4(4) . . ?
C123 C122 Ag7 121.4(5) . . ?
Ag18 C122 Ag7 96.3(3) . . ?
C122 C123 C126 108.3(7) . . ?
C122 C123 C125 109.5(7) . . ?
C126 C123 C125 112.7(10) . . ?
C122 C123 C124 109.3(7) . . ?
C126 C123 C124 108.5(9) . . ?
C125 C123 C124 108.4(8) . . ?
C202 C201 Ag24 118.8(5) . . ?
C202 C201 Ag8 142.7(6) . . ?
Ag24 C201 Ag8 85.7(2) . . ?
C202 C201 Ag22 118.6(6) . . ?
Ag24 C201 Ag22 84.4(3) . . ?
Ag8 C201 Ag22 89.6(3) . . ?
C201 C202 C203 179.4(9) . . ?
C202 C203 C204 110.6(7) . . ?
C202 C203 C205 109.3(8) . . ?
C204 C203 C205 108.3(10) . . ?
C202 C203 C206 108.7(8) . . ?
C204 C203 C206 107.9(11) . . ?
C205 C203 C206 112.0(11) . . ?
C302 C301 Ag9 151.1(7) . . ?
C302 C301 Ag24 89.1(5) . . ?
Ag9 C301 Ag24 98.1(3) . . ?
C302 C301 Ag17 126.1(6) . . ?
Ag9 C301 Ag17 82.4(2) . . ?
Ag24 C301 Ag17 87.3(2) . . ?
C301 C302 C303 175.3(8) . . ?
C301 C302 Ag24 62.2(4) . . ?
C303 C302 Ag24 122.5(5) . . ?
C305 C303 C302 108.3(8) . . ?
C305 C303 C306 111.0(9) . . ?
C302 C303 C306 107.9(7) . . ?
C305 C303 C304 110.6(9) . . ?
C302 C303 C304 108.3(7) . . ?
C306 C303 C304 110.5(9) . . ?
C402 C401 Ag2 175.7(6) . . ?
C402 C401 Ag16 99.5(5) . . ?
Ag2 C401 Ag16 84.7(3) . . ?
C402 C401 Ag10 88.4(5) . . ?
Ag2 C401 Ag10 89.3(3) . . ?
Ag16 C401 Ag10 112.2(3) . . ?
C401 C402 C403 174.2(7) . . ?
C401 C402 Ag10 63.7(5) . . ?
C403 C402 Ag10 121.9(5) . . ?
C401 C402 Ag16 54.4(4) . . ?
C403 C402 Ag16 124.7(5) . . ?
Ag10 C402 Ag16 91.1(2) . . ?
C402 C403 C406 109.6(7) . . ?
C402 C403 C404 109.5(7) . . ?
C406 C403 C404 111.8(8) . . ?
C402 C403 C405 108.7(7) . . ?
C406 C403 C405 109.1(7) . . ?
C404 C403 C405 108.1(7) . . ?
C502 C501 Ag4 156.2(6) . . ?
C502 C501 Ag21 92.5(5) . . ?
Ag4 C501 Ag21 94.5(3) . . ?
C502 C501 Ag10 116.8(5) . . ?
Ag4 C501 Ag10 86.5(2) . . ?
Ag21 C501 Ag10 85.7(2) . . ?
C501 C502 C503 175.5(8) . . ?
C501 C502 Ag21 59.7(5) . . ?
C503 C502 Ag21 124.8(5) . . ?
C509 C503 C505 133.2(14) . . ?
C509 C503 C502 114.0(14) . . ?
C505 C503 C502 112.5(8) . . ?
C509 C503 C508 114.2(12) . . ?
C505 C503 C508 53.3(10) . . ?
C502 C503 C508 108.4(13) . . ?
C509 C503 C507 110.0(11) . . ?
C505 C503 C507 54.0(10) . . ?
C502 C503 C507 102.3(10) . . ?
C508 C503 C507 107.1(11) . . ?
C509 C503 C506 45.3(11) . . ?
C505 C503 C506 112.8(8) . . ?
C502 C503 C506 109.0(7) . . ?
C508 C503 C506 142.5(13) . . ?
C507 C503 C506 67.3(10) . . ?
C509 C503 C504 61.9(11) . . ?
C505 C503 C504 109.2(8) . . ?
C502 C503 C504 106.2(7) . . ?
C508 C503 C504 59.3(11) . . ?
C507 C503 C504 151.1(11) . . ?
C506 C503 C504 106.7(7) . . ?
C602 C601 Ag12 164.8(6) . . ?
C602 C601 Ag20 101.4(6) . . ?
Ag12 C601 Ag20 87.8(3) . . ?
C602 C601 Ag4 89.1(5) . . ?
Ag12 C601 Ag4 102.2(3) . . ?
Ag20 C601 Ag4 94.8(3) . . ?
C601 C602 C603 172.0(7) . . ?
C601 C602 Ag4 63.2(4) . . ?
C603 C602 Ag4 124.1(5) . . ?
C605 C603 C604 115.9(11) . . ?
C605 C603 C602 110.1(8) . . ?
C604 C603 C602 109.7(9) . . ?
C605 C603 C606 107.6(10) . . ?
C604 C603 C606 104.8(10) . . ?
C602 C603 C606 108.3(8) . . ?
C702 C701 Ag18 171.0(6) . . ?
C702 C701 Ag13 96.4(5) . . ?
Ag18 C701 Ag13 90.0(3) . . ?
C702 C701 Ag8 87.3(5) . . ?
Ag18 C701 Ag8 97.9(3) . . ?
Ag13 C701 Ag8 99.6(3) . . ?
C701 C702 C703 173.2(8) . . ?
C701 C702 Ag8 65.0(4) . . ?
C703 C702 Ag8 118.7(5) . . ?
C701 C702 Ag13 56.7(4) . . ?
C703 C702 Ag13 128.1(5) . . ?
Ag8 C702 Ag13 83.7(2) . . ?
C702 C703 C704 108.2(6) . . ?
C702 C703 C706 109.7(7) . . ?
C704 C703 C706 110.6(8) . . ?
C702 C703 C705 108.1(7) . . ?
C704 C703 C705 110.2(7) . . ?
C706 C703 C705 109.9(8) . . ?
C802 C801 Ag14 132.3(6) . . ?
C802 C801 Ag2 141.3(6) . . ?
Ag14 C801 Ag2 85.1(3) . . ?
C802 C801 Ag19 83.5(5) . . ?
Ag14 C801 Ag19 112.4(3) . . ?
Ag2 C801 Ag19 91.1(3) . . ?
C801 C802 C803 172.3(8) . . ?
C801 C802 Ag19 67.6(5) . . ?
C803 C802 Ag19 118.8(5) . . ?
C804 C803 C802 107.1(8) . . ?
C804 C803 C805 112.3(10) . . ?
C802 C803 C805 110.2(7) . . ?
C804 C803 C806 111.6(9) . . ?
C802 C803 C806 109.1(7) . . ?
C805 C803 C806 106.5(9) . . ?
C902 C901 Ag21 136.4(6) . . ?
C902 C901 Ag3 130.1(6) . . ?
Ag21 C901 Ag3 88.3(2) . . ?
C902 C901 Ag15 95.4(5) . . ?
Ag21 C901 Ag15 85.8(2) . . ?
Ag3 C901 Ag15 111.8(3) . . ?
C901 C902 C903 174.8(8) . . ?
C901 C902 Ag15 57.9(4) . . ?
C903 C902 Ag15 127.1(5) . . ?
C902 C903 C905 108.8(7) . . ?
C902 C903 C906 108.8(7) . . ?
C905 C903 C906 110.5(7) . . ?
C902 C903 C904 108.3(7) . . ?
C905 C903 C904 109.7(7) . . ?
C906 C903 C904 110.8(8) . . ?
C2S C1S C3S 57.9(8) . . ?
N1S C2S C1S 166(3) . . ?
N2S C3S C1S 166(3) . . ?
C40S N10S C10S 57(3) . . ?
N10S C10S C20S 165(3) . . ?
N10S C40S C30S 167(4) . . ?

_diffrn_measured_fraction_theta_max 0.998
_diffrn_reflns_theta_full        26.00
_diffrn_measured_fraction_theta_full 0.998
_refine_diff_density_max         2.783
_refine_diff_density_min         -1.671
_refine_diff_density_rms         0.138
