# Electronic Supplementary Material (ESI) for CrystEngComm.
# This journal is © The Royal Society of Chemistry 2015

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 1059082'
_audit_update_record             
;
2015-04-13 deposited with the CCDC.
2015-06-25 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C42.50 H35 Dy N3 O11'
_chemical_formula_weight         926.24

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Orthorhombic
_symmetry_space_group_name_H-M   Pbcn

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z+1/2'
'-x, y, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x-1/2, y-1/2, -z-1/2'
'x, -y, z-1/2'
'-x-1/2, y-1/2, z'

_cell_length_a                   35.022(3)
_cell_length_b                   10.7640(10)
_cell_length_c                   20.158(2)
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_volume                     7599.1(12)
_cell_formula_units_Z            8
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    9195
_cell_measurement_theta_min      2.33
_cell_measurement_theta_max      27.37

_exptl_crystal_description       needle
_exptl_crystal_colour            yellow
_exptl_crystal_size_max          0.54
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.04
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.619
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3720
_exptl_absorpt_coefficient_mu    2.035
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.4063
_exptl_absorpt_correction_T_max  0.9230
_exptl_absorpt_process_details   SADABS

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            49156
_diffrn_reflns_av_R_equivalents  0.0571
_diffrn_reflns_av_sigmaI/netI    0.0399
_diffrn_reflns_limit_h_min       -45
_diffrn_reflns_limit_h_max       45
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_theta_min         3.47
_diffrn_reflns_theta_max         27.48
_reflns_number_total             8693
_reflns_number_gt                6826
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker SMART'
_computing_cell_refinement       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'


_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0166P)²+8.4070P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         8693
_refine_ls_number_parameters     532
_refine_ls_number_restraints     4
_refine_ls_R_factor_all          0.0459
_refine_ls_R_factor_gt           0.0301
_refine_ls_wR_factor_ref         0.0599
_refine_ls_wR_factor_gt          0.0553
_refine_ls_goodness_of_fit_ref   1.014
_refine_ls_restrained_S_all      1.014
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.15661(9) 0.3771(3) 1.15050(16) 0.0289(7) Uani 1 1 d . . .
H1 H 0.1526 0.4447 1.1227 0.035 Uiso 1 1 calc R . .
C2 C 0.17904(10) 0.3904(4) 1.20725(18) 0.0366(9) Uani 1 1 d . . .
H2 H 0.1901 0.4669 1.2169 0.044 Uiso 1 1 calc R . .
C3 C 0.18497(9) 0.2908(4) 1.24919(17) 0.0365(9) Uani 1 1 d . . .
H3 H 0.1993 0.3008 1.2876 0.044 Uiso 1 1 calc R . .
C4 C 0.16965(9) 0.1769(4) 1.23412(15) 0.0308(8) Uani 1 1 d . . .
H4 H 0.1738 0.1096 1.2621 0.037 Uiso 1 1 calc R . .
C5 C 0.14792(8) 0.1620(3) 1.17710(14) 0.0224(7) Uani 1 1 d . . .
H5 H 0.1383 0.0839 1.1664 0.027 Uiso 1 1 calc R . .
C6 C 0.14031(8) 0.2626(3) 1.13561(14) 0.0193(6) Uani 1 1 d . . .
C7 C 0.11387(8) 0.2424(3) 1.07726(13) 0.0173(6) Uani 1 1 d . . .
C8 C 0.09602(8) 0.3451(3) 1.04706(14) 0.0206(6) Uani 1 1 d . . .
H8 H 0.1023 0.4244 1.0618 0.025 Uiso 1 1 calc R . .
C9 C 0.06933(8) 0.3329(3) 0.99591(14) 0.0176(6) Uani 1 1 d . . .
C10 C 0.05008(8) 0.4467(3) 0.96904(13) 0.0169(6) Uani 1 1 d . . .
C11 C 0.04944(8) 0.5615(3) 1.00070(14) 0.0190(6) Uani 1 1 d . . .
H11 H 0.0608 0.5695 1.0422 0.023 Uiso 1 1 calc R . .
C12 C 0.03245(8) 0.6631(3) 0.97229(14) 0.0198(6) Uani 1 1 d . . .
H12 H 0.0322 0.7386 0.9947 0.024 Uiso 1 1 calc R . .
C13 C 0.01508(8) 0.5427(3) 0.87971(14) 0.0188(6) Uani 1 1 d . . .
H13 H 0.0031 0.5360 0.8387 0.023 Uiso 1 1 calc R . .
C14 C 0.03176(8) 0.4400(3) 0.90764(14) 0.0203(7) Uani 1 1 d . . .
H14 H 0.0309 0.3645 0.8853 0.024 Uiso 1 1 calc R . .
C15 C 0.21261(10) 0.3385(4) 0.84241(18) 0.0385(9) Uani 1 1 d . . .
H15 H 0.2047 0.3275 0.7988 0.046 Uiso 1 1 calc R . .
C16 C 0.24316(11) 0.4160(4) 0.8561(2) 0.0529(12) Uani 1 1 d . . .
H16 H 0.2556 0.4569 0.8217 0.063 Uiso 1 1 calc R . .
C17 C 0.25526(11) 0.4327(4) 0.9204(2) 0.0451(10) Uani 1 1 d . . .
H17 H 0.2759 0.4843 0.9295 0.054 Uiso 1 1 calc R . .
C18 C 0.23663(10) 0.3729(4) 0.97119(19) 0.0423(10) Uani 1 1 d . . .
H18 H 0.2447 0.3842 1.0147 0.051 Uiso 1 1 calc R . .
C19 C 0.20591(9) 0.2962(3) 0.95799(16) 0.0303(8) Uani 1 1 d . . .
H19 H 0.1933 0.2570 0.9928 0.036 Uiso 1 1 calc R . .
C20 C 0.19374(8) 0.2771(3) 0.89318(15) 0.0213(6) Uani 1 1 d . . .
C21 C 0.15946(8) 0.1963(3) 0.88264(14) 0.0179(6) Uani 1 1 d . . .
C22 C 0.14534(8) 0.1737(3) 0.81755(14) 0.0187(6) Uani 1 1 d . . .
H22 H 0.1605 0.1949 0.7814 0.022 Uiso 1 1 calc R . .
C23 C 0.10997(8) 0.1214(3) 0.80597(13) 0.0161(6) Uani 1 1 d . . .
C24 C 0.09552(8) 0.1110(3) 0.73578(13) 0.0146(6) Uani 1 1 d . . .
C25 C 0.10792(8) 0.1851(3) 0.68396(13) 0.0170(6) Uani 1 1 d . . .
H25 H 0.1267 0.2446 0.6912 0.020 Uiso 1 1 calc R . .
C26 C 0.09232(8) 0.1707(3) 0.62149(13) 0.0166(6) Uani 1 1 d . . .
H26 H 0.0998 0.2232 0.5872 0.020 Uiso 1 1 calc R . .
C27 C 0.05386(8) 0.0071(3) 0.65955(13) 0.0179(6) Uani 1 1 d . . .
H27 H 0.0363 -0.0555 0.6507 0.022 Uiso 1 1 calc R . .
C28 C 0.06715(8) 0.0245(3) 0.72294(13) 0.0171(6) Uani 1 1 d . . .
H28 H 0.0570 -0.0222 0.7576 0.021 Uiso 1 1 calc R . .
C29 C 0.19092(9) -0.1392(3) 1.09791(15) 0.0271(7) Uani 1 1 d . . .
H29 H 0.1792 -0.0616 1.0978 0.032 Uiso 1 1 calc R . .
C30 C 0.21714(10) -0.1682(4) 1.14727(17) 0.0356(9) Uani 1 1 d . . .
H30 H 0.2229 -0.1103 1.1800 0.043 Uiso 1 1 calc R . .
C31 C 0.23453(11) -0.2828(4) 1.1477(2) 0.0491(11) Uani 1 1 d . . .
H31 H 0.2521 -0.3025 1.1807 0.059 Uiso 1 1 calc R . .
C32 C 0.22588(13) -0.3683(4) 1.0991(2) 0.0618(14) Uani 1 1 d . . .
H32 H 0.2378 -0.4455 1.0991 0.074 Uiso 1 1 calc R . .
C33 C 0.19948(11) -0.3399(4) 1.0502(2) 0.0453(10) Uani 1 1 d . . .
H33 H 0.1935 -0.3987 1.0180 0.054 Uiso 1 1 calc R . .
C34 C 0.18199(9) -0.2247(3) 1.04881(15) 0.0246(7) Uani 1 1 d . . .
C35 C 0.15290(8) -0.1886(3) 0.99773(14) 0.0192(6) Uani 1 1 d . . .
C36 C 0.14224(9) -0.2720(3) 0.94729(15) 0.0237(7) Uani 1 1 d . . .
H36 H 0.1555 -0.3464 0.9429 0.028 Uiso 1 1 calc R . .
C37 C 0.11231(8) -0.2465(3) 0.90357(14) 0.0181(6) Uani 1 1 d . . .
C38 C 0.10341(8) -0.3350(3) 0.84845(14) 0.0188(6) Uani 1 1 d . . .
C39 C 0.11469(9) -0.4586(3) 0.84581(15) 0.0246(7) Uani 1 1 d . . .
H39 H 0.1285 -0.4926 0.8808 0.030 Uiso 1 1 calc R . .
C40 C 0.10566(10) -0.5309(3) 0.79223(16) 0.0296(8) Uani 1 1 d . . .
H40 H 0.1132 -0.6137 0.7916 0.036 Uiso 1 1 calc R . .
C41 C 0.07411(9) -0.3643(3) 0.74149(15) 0.0231(7) Uani 1 1 d . . .
H41 H 0.0604 -0.3318 0.7061 0.028 Uiso 1 1 calc R . .
C42 C 0.08235(8) -0.2910(3) 0.79504(14) 0.0213(7) Uani 1 1 d . . .
H42 H 0.0736 -0.2094 0.7957 0.026 Uiso 1 1 calc R . .
C43 C 0.0000 0.2645(6) 0.7500 0.0627(18) Uani 1 2 d S . .
H43A H 0.0187 0.2348 0.7190 0.094 Uiso 0.50 1 calc PR . .
H43B H -0.0248 0.2348 0.7374 0.094 Uiso 0.50 1 calc PR . .
H43C H 0.0061 0.2348 0.7936 0.094 Uiso 0.50 1 calc PR . .
Dy1 Dy 0.088730(4) 0.038578(12) 0.962135(6) 0.01375(4) Uani 1 1 d . . .
N1 N 0.01585(7) 0.6541(2) 0.91129(11) 0.0180(5) Uani 1 1 d . . .
N2 N 0.06647(7) 0.0815(2) 0.60998(11) 0.0148(5) Uani 1 1 d . . .
N3 N 0.08591(8) -0.4842(2) 0.73980(13) 0.0258(6) Uani 1 1 d . . .
O1 O 0.00081(6) 0.75307(18) 0.88281(10) 0.0243(5) Uani 1 1 d . . .
O2 O 0.05978(6) 0.23076(18) 0.96820(9) 0.0210(4) Uani 1 1 d . . .
O3 O 0.10795(6) 0.13125(19) 1.06144(9) 0.0208(5) Uani 1 1 d . . .
O4 O 0.05245(5) 0.06677(18) 0.54901(8) 0.0163(4) Uani 1 1 d . . .
O5 O 0.08691(6) 0.0836(2) 0.84962(9) 0.0235(5) Uani 1 1 d . . .
O6 O 0.14325(6) 0.1536(2) 0.93382(9) 0.0230(5) Uani 1 1 d . . .
O7 O 0.07892(7) -0.5534(2) 0.68787(12) 0.0389(6) Uani 1 1 d . . .
O8 O 0.09126(6) -0.15091(19) 0.90619(10) 0.0218(5) Uani 1 1 d . . .
O9 O 0.13817(6) -0.08222(19) 1.00472(10) 0.0222(5) Uani 1 1 d . . .
O10 O 0.02432(6) -0.01126(19) 0.92800(10) 0.0181(4) Uani 1 1 d D . .
O11 O 0.0000 0.8340(3) 0.7500 0.0347(8) Uani 1 2 d SD . .
O12 O 0.0000 0.3847(4) 0.7500 0.111(3) Uani 1 2 d S . .
H12A H -0.0161 0.4101 0.7762 0.167 Uiso 0.50 1 calc PR . .
H10A H 0.0199(11) -0.093(2) 0.914(2) 0.076(9) Uiso 1 1 d D . .
H10B H 0.0016(8) 0.025(3) 0.941(2) 0.076(9) Uiso 1 1 d D . .
H11A H -0.0022(13) 0.779(3) 0.7107(14) 0.076(9) Uiso 1 1 d D . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C6 1.392(4) . ?
C1 C2 1.395(4) . ?
C2 C3 1.382(5) . ?
C3 C4 1.372(5) . ?
C4 C5 1.388(4) . ?
C5 C6 1.394(4) . ?
C6 C7 1.513(4) . ?
C7 O3 1.256(3) . ?
C7 C8 1.408(4) . ?
C8 C9 1.398(4) . ?
C9 O2 1.278(3) . ?
C9 C10 1.499(4) . ?
C10 C11 1.391(4) . ?
C10 C14 1.396(4) . ?
C11 C12 1.370(4) . ?
C12 N1 1.364(4) . ?
C13 N1 1.357(4) . ?
C13 C14 1.371(4) . ?
C15 C16 1.384(5) . ?
C15 C20 1.386(4) . ?
C16 C17 1.376(5) . ?
C17 C18 1.374(5) . ?
C18 C19 1.382(5) . ?
C19 C20 1.390(4) . ?
C20 C21 1.498(4) . ?
C21 O6 1.264(3) . ?
C21 C22 1.423(4) . ?
C22 C23 1.380(4) . ?
C23 O5 1.262(3) . ?
C23 C24 1.507(4) . ?
C24 C25 1.384(4) . ?
C24 C28 1.386(4) . ?
C25 C26 1.382(4) . ?
C26 N2 1.340(3) . ?
C27 N2 1.355(3) . ?
C27 C28 1.373(4) . ?
C29 C34 1.388(4) . ?
C29 C30 1.390(4) . ?
C30 C31 1.375(5) . ?
C31 C32 1.379(6) . ?
C32 C33 1.386(5) . ?
C33 C34 1.383(5) . ?
C34 C35 1.500(4) . ?
C35 O9 1.264(3) . ?
C35 C36 1.407(4) . ?
C36 C37 1.397(4) . ?
C37 O8 1.266(3) . ?
C37 C38 1.497(4) . ?
C38 C42 1.388(4) . ?
C38 C39 1.389(4) . ?
C39 C40 1.368(4) . ?
C40 N3 1.359(4) . ?
C41 N3 1.355(4) . ?
C41 C42 1.368(4) . ?
C43 O12 1.294(7) . ?
Dy1 O2 2.307(2) . ?
Dy1 O5 2.3202(19) . ?
Dy1 O9 2.329(2) . ?
Dy1 O8 2.3324(19) . ?
Dy1 O3 2.3356(19) . ?
Dy1 O6 2.346(2) . ?
Dy1 O10 2.419(2) . ?
Dy1 O4 2.4427(18) 7_556 ?
N1 O1 1.320(3) . ?
N2 O4 1.333(3) . ?
N3 O7 1.308(3) . ?
O4 Dy1 2.4427(18) 7 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C6 C1 C2 119.9(3) . . ?
C3 C2 C1 120.4(3) . . ?
C4 C3 C2 120.0(3) . . ?
C3 C4 C5 120.1(3) . . ?
C4 C5 C6 120.8(3) . . ?
C1 C6 C5 118.7(3) . . ?
C1 C6 C7 123.1(3) . . ?
C5 C6 C7 118.2(3) . . ?
O3 C7 C8 124.4(3) . . ?
O3 C7 C6 115.8(3) . . ?
C8 C7 C6 119.7(3) . . ?
C9 C8 C7 122.8(3) . . ?
O2 C9 C8 125.3(3) . . ?
O2 C9 C10 115.3(2) . . ?
C8 C9 C10 119.4(3) . . ?
C11 C10 C14 116.4(3) . . ?
C11 C10 C9 124.6(3) . . ?
C14 C10 C9 119.0(3) . . ?
C12 C11 C10 121.6(3) . . ?
N1 C12 C11 120.3(3) . . ?
N1 C13 C14 120.7(3) . . ?
C13 C14 C10 121.2(3) . . ?
C16 C15 C20 120.6(3) . . ?
C17 C16 C15 120.3(4) . . ?
C18 C17 C16 119.6(3) . . ?
C17 C18 C19 120.4(3) . . ?
C18 C19 C20 120.5(3) . . ?
C15 C20 C19 118.5(3) . . ?
C15 C20 C21 123.7(3) . . ?
C19 C20 C21 117.7(3) . . ?
O6 C21 C22 122.3(3) . . ?
O6 C21 C20 117.1(3) . . ?
C22 C21 C20 120.6(3) . . ?
C23 C22 C21 122.5(3) . . ?
O5 C23 C22 126.0(3) . . ?
O5 C23 C24 114.6(2) . . ?
C22 C23 C24 119.4(2) . . ?
C25 C24 C28 118.1(2) . . ?
C25 C24 C23 124.1(3) . . ?
C28 C24 C23 117.8(2) . . ?
C26 C25 C24 119.9(3) . . ?
N2 C26 C25 120.4(3) . . ?
N2 C27 C28 119.7(3) . . ?
C27 C28 C24 120.6(3) . . ?
C34 C29 C30 120.7(3) . . ?
C31 C30 C29 120.0(4) . . ?
C30 C31 C32 119.8(3) . . ?
C31 C32 C33 120.3(4) . . ?
C34 C33 C32 120.5(4) . . ?
C33 C34 C29 118.8(3) . . ?
C33 C34 C35 123.2(3) . . ?
C29 C34 C35 118.1(3) . . ?
O9 C35 C36 123.4(3) . . ?
O9 C35 C34 115.8(3) . . ?
C36 C35 C34 120.7(3) . . ?
C37 C36 C35 121.9(3) . . ?
O8 C37 C36 124.8(3) . . ?
O8 C37 C38 115.3(3) . . ?
C36 C37 C38 119.9(3) . . ?
C42 C38 C39 116.6(3) . . ?
C42 C38 C37 118.0(3) . . ?
C39 C38 C37 125.4(3) . . ?
C40 C39 C38 120.6(3) . . ?
N3 C40 C39 121.4(3) . . ?
N3 C41 C42 120.3(3) . . ?
C41 C42 C38 121.8(3) . . ?
O2 Dy1 O5 81.51(7) . . ?
O2 Dy1 O9 143.87(7) . . ?
O5 Dy1 O9 119.82(7) . . ?
O2 Dy1 O8 145.74(7) . . ?
O5 Dy1 O8 73.20(7) . . ?
O9 Dy1 O8 70.23(7) . . ?
O2 Dy1 O3 72.44(7) . . ?
O5 Dy1 O3 139.16(7) . . ?
O9 Dy1 O3 73.04(7) . . ?
O8 Dy1 O3 140.98(7) . . ?
O2 Dy1 O6 84.11(7) . . ?
O5 Dy1 O6 71.00(7) . . ?
O9 Dy1 O6 77.25(7) . . ?
O8 Dy1 O6 108.24(7) . . ?
O3 Dy1 O6 75.43(7) . . ?
O2 Dy1 O10 78.70(7) . . ?
O5 Dy1 O10 75.08(7) . . ?
O9 Dy1 O10 132.40(7) . . ?
O8 Dy1 O10 72.78(7) . . ?
O3 Dy1 O10 127.40(7) . . ?
O6 Dy1 O10 143.80(7) . . ?
O2 Dy1 O4 98.61(7) . 7_556 ?
O5 Dy1 O4 141.58(7) . 7_556 ?
O9 Dy1 O4 82.14(7) . 7_556 ?
O8 Dy1 O4 87.73(7) . 7_556 ?
O3 Dy1 O4 74.56(7) . 7_556 ?
O6 Dy1 O4 147.42(6) . 7_556 ?
O10 Dy1 O4 67.41(6) . 7_556 ?
O1 N1 C13 120.1(2) . . ?
O1 N1 C12 120.3(2) . . ?
C13 N1 C12 119.6(2) . . ?
O4 N2 C26 119.6(2) . . ?
O4 N2 C27 119.3(2) . . ?
C26 N2 C27 121.1(2) . . ?
O7 N3 C41 120.3(3) . . ?
O7 N3 C40 120.5(3) . . ?
C41 N3 C40 119.2(3) . . ?
C9 O2 Dy1 132.83(18) . . ?
C7 O3 Dy1 132.24(18) . . ?
N2 O4 Dy1 121.64(15) . 7 ?
C23 O5 Dy1 137.00(18) . . ?
C21 O6 Dy1 139.10(19) . . ?
C37 O8 Dy1 138.80(19) . . ?
C35 O9 Dy1 140.18(19) . . ?

_diffrn_measured_fraction_theta_max 0.998
_diffrn_reflns_theta_full        27.48
_diffrn_measured_fraction_theta_full 0.998
_refine_diff_density_max         0.678
_refine_diff_density_min         -0.695
_refine_diff_density_rms         0.090
