# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2015

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_x82895m
_database_code_depnum_ccdc_archive 'CCDC 1042151'
_audit_update_record             
;
2015-01-08 deposited with the CCDC.
2015-02-09 downloaded from the CCDC.
;
_audit_creation_date             2015-01-08
_audit_creation_method           
;
Olex2 1.2
(compiled 2013.12.10 svn.r2850 for OlexSys, GUI svn.r4736)
;
_shelxl_version_number           2014/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C4 H21 B19, C10 H16 N'
_chemical_formula_sum            'C14 H38 B19 N'
_chemical_formula_weight         425.84
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   18.851(9)
_cell_length_b                   10.072(4)
_cell_length_c                   13.477(6)
_cell_angle_alpha                90
_cell_angle_beta                 97.068(13)
_cell_angle_gamma                90
_cell_volume                     2540(2)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    453
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      16.296
_cell_measurement_theta_min      2.829
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    0.052
_exptl_absorpt_correction_T_max  0.7446
_exptl_absorpt_correction_T_min  0.4484
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.1145 before and 0.0877 after correction.
The Ratio of minimum to maximum transmission is 0.6022.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.114
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             896
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.2172
_diffrn_reflns_av_unetI/netI     0.1915
_diffrn_reflns_Laue_measured_fraction_full 0.594
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            14879
_diffrn_reflns_point_group_measured_fraction_full 0.594
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         20.838
_diffrn_reflns_theta_min         1.088
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.594
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                1229
_reflns_number_total             2651
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         0.265
_refine_diff_density_min         -0.261
_refine_diff_density_rms         0.057
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.005
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     308
_refine_ls_number_reflns         2651
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.2026
_refine_ls_R_factor_gt           0.0867
_refine_ls_restrained_S_all      1.005
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1143P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1912
_refine_ls_wR_factor_ref         0.2451
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Others
 Sof(B12)=Sof(H12)=1-FVAR(1)
 Sof(B3)=Sof(H3)=FVAR(1)
 Fixed Uiso: B3(0.03) B12(0.03)
3.a Secondary CH2 refined with riding coordinates:
 C103(H10J,H10K)
3.b Aromatic/amide H refined with riding coordinates:
 C107(H107), C106(H106), C108(H108), C105(H105), C109(H109)
3.c Idealised Me refined as rotating group:
 C102(H10A,H10B,H10C), C101(H10D,H10E,H10F), C100(H10G,H10H,H10I)
3.d Boron cage BH refined with riding coordinates:
 B1(H1), B2(H2), B3(H3), B4(H4), B5(H5), B6(H6), C8(H8), B9(H9), B10(H10),
 B11(H11), B12(H12), C2'(H2'), B3'(H3'), B4'(H4'), B5'(H5'), B6'(H6'), B7'(H7'),
  B8'(H8'), B9'(H9'), B10'(H10'), B11'(H11'), B12'(H12')
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
B1 B 0.5925(5) 0.3550(8) 0.3127(5) 0.037(2) Uani 1 1 d . . . . .
H1 H 0.5602 0.4267 0.3522 0.044 Uiso 1 1 calc R . . . .
B2 B 0.6813(4) 0.3149(8) 0.3582(6) 0.033(2) Uani 1 1 d . . . . .
H2 H 0.7097 0.3619 0.4273 0.039 Uiso 1 1 calc R . . . .
B3 B 0.6623(7) 0.4033(15) 0.2507(10) 0.030 Uiso 0.548(10) 1 d . . P . .
H3 H 0.6783 0.5102 0.2482 0.036 Uiso 0.548(10) 1 calc R . P . .
B4 B 0.5848(4) 0.3442(9) 0.1781(6) 0.036(2) Uani 1 1 d . . . . .
H4 H 0.5494 0.4109 0.1272 0.043 Uiso 1 1 calc R . . . .
B5 B 0.5520(5) 0.2123(8) 0.2480(5) 0.039(3) Uani 1 1 d . . . . .
H5 H 0.4933 0.1918 0.2438 0.046 Uiso 1 1 calc R . . . .
B6 B 0.6142(4) 0.1942(8) 0.3606(6) 0.034(2) Uani 1 1 d . . . . .
H6 H 0.5968 0.1605 0.4330 0.041 Uiso 1 1 calc R . . . .
C7 C 0.7194(3) 0.2719(7) 0.2539(4) 0.0320(19) Uani 1 1 d . . . . .
C8 C 0.6649(4) 0.2848(8) 0.1572(6) 0.061(3) Uani 1 1 d . . . . .
H8 H 0.6847 0.3164 0.0858 0.074 Uiso 1 1 calc R . . . .
B9 B 0.6018(4) 0.1745(8) 0.1467(6) 0.035(2) Uani 1 1 d . . . . .
H9 H 0.5773 0.1296 0.0745 0.042 Uiso 1 1 calc R . . . .
B10 B 0.6159(4) 0.0809(9) 0.2613(5) 0.039(3) Uani 1 1 d . . . . .
H10 H 0.5993 -0.0252 0.2677 0.047 Uiso 1 1 calc R . . . .
B11 B 0.6976(4) 0.1459(8) 0.3260(5) 0.035(2) Uani 1 1 d . . . . .
H11 H 0.7370 0.0823 0.3735 0.042 Uiso 1 1 calc R . . . .
B12 B 0.6852(9) 0.1359(18) 0.1968(12) 0.030 Uiso 0.452(10) 1 d . . P . .
H12 H 0.7169 0.0628 0.1577 0.036 Uiso 0.452(10) 1 calc R . P . .
C1' C 0.7970(4) 0.2998(7) 0.2430(5) 0.034(2) Uani 1 1 d . . . . .
C2' C 0.8580(4) 0.2800(8) 0.3441(5) 0.057(3) Uani 1 1 d . . . . .
H2' H 0.8417 0.2457 0.4171 0.068 Uiso 1 1 calc R . . . .
B3' B 0.8572(4) 0.1677(9) 0.2458(5) 0.034(2) Uani 1 1 d . . . . .
H3' H 0.8419 0.0607 0.2509 0.041 Uiso 1 1 calc R . . . .
B4' B 0.8338(4) 0.2619(8) 0.1346(6) 0.035(2) Uani 1 1 d . . . . .
H4' H 0.8029 0.2172 0.0664 0.042 Uiso 1 1 calc R . . . .
B5' B 0.8203(5) 0.4308(9) 0.1702(6) 0.041(3) Uani 1 1 d . . . . .
H5' H 0.7805 0.4968 0.1256 0.049 Uiso 1 1 calc R . . . .
B6' B 0.8371(4) 0.4363(8) 0.2990(5) 0.032(2) Uani 1 1 d . . . . .
H6' H 0.8073 0.5091 0.3412 0.038 Uiso 1 1 calc R . . . .
B7' B 0.9382(4) 0.2301(9) 0.3095(6) 0.044(3) Uani 1 1 d . . . . .
H7' H 0.9766 0.1648 0.3571 0.052 Uiso 1 1 calc R . . . .
B8' B 0.9249(4) 0.2193(9) 0.1740(6) 0.038(3) Uani 1 1 d . . . . .
H8' H 0.9548 0.1470 0.1315 0.046 Uiso 1 1 calc R . . . .
B9' B 0.9026(4) 0.3824(9) 0.1279(6) 0.042(3) Uani 1 1 d . . . . .
H9' H 0.9180 0.4171 0.0546 0.050 Uiso 1 1 calc R . . . .
B10' B 0.9024(5) 0.4917(9) 0.2314(6) 0.039(2) Uani 1 1 d . . . . .
H10' H 0.9174 0.5989 0.2271 0.047 Uiso 1 1 calc R . . . .
B11' B 0.9245(5) 0.3971(9) 0.3423(6) 0.044(3) Uani 1 1 d . . . . .
H11' H 0.9539 0.4414 0.4117 0.053 Uiso 1 1 calc R . . . .
B12' B 0.9667(5) 0.3625(9) 0.2338(5) 0.039(3) Uani 1 1 d . . . . .
H12' H 1.0246 0.3840 0.2303 0.047 Uiso 1 1 calc R . . . .
C107 C 0.1045(5) 0.2531(9) 0.5317(6) 0.054(2) Uani 1 1 d . . . . .
H107 H 0.0554 0.2326 0.5331 0.065 Uiso 1 1 calc R . . . .
C106 C 0.1550(5) 0.1958(8) 0.5984(6) 0.049(2) Uani 1 1 d . . . . .
H106 H 0.1405 0.1348 0.6457 0.059 Uiso 1 1 calc R . . . .
C108 C 0.1240(4) 0.3402(8) 0.4627(6) 0.049(2) Uani 1 1 d . . . . .
H108 H 0.0889 0.3805 0.4156 0.058 Uiso 1 1 calc R . . . .
C102 C 0.3312(4) 0.2514(8) 0.3580(4) 0.048(2) Uani 1 1 d . . . . .
H10A H 0.3303 0.3413 0.3301 0.073 Uiso 1 1 calc GR . . . .
H10B H 0.2822 0.2182 0.3560 0.073 Uiso 1 1 calc GR . . . .
H10C H 0.3584 0.1928 0.3186 0.073 Uiso 1 1 calc GR . . . .
C101 C 0.3693(4) 0.1174(7) 0.5063(5) 0.045(2) Uani 1 1 d . . . . .
H10D H 0.3946 0.0595 0.4639 0.068 Uiso 1 1 calc GR . . . .
H10E H 0.3206 0.0842 0.5079 0.068 Uiso 1 1 calc GR . . . .
H10F H 0.3947 0.1182 0.5743 0.068 Uiso 1 1 calc GR . . . .
C100 C 0.4407(4) 0.3060(7) 0.4689(5) 0.046(2) Uani 1 1 d . . . . .
H10G H 0.4628 0.3099 0.5386 0.070 Uiso 1 1 calc GR . . . .
H10H H 0.4396 0.3952 0.4398 0.070 Uiso 1 1 calc GR . . . .
H10I H 0.4686 0.2469 0.4309 0.070 Uiso 1 1 calc GR . . . .
C105 C 0.2264(4) 0.2229(7) 0.5998(5) 0.043(2) Uani 1 1 d . . . . .
H105 H 0.2607 0.1820 0.6477 0.051 Uiso 1 1 calc R . . . .
C104 C 0.2479(4) 0.3129(8) 0.5286(5) 0.037(2) Uani 1 1 d . . . . .
C103 C 0.3260(4) 0.3463(7) 0.5271(5) 0.039(2) Uani 1 1 d . . . . .
H10J H 0.3500 0.3456 0.5967 0.047 Uiso 1 1 calc R . . . .
H10K H 0.3294 0.4378 0.5011 0.047 Uiso 1 1 calc R . . . .
C109 C 0.1958(4) 0.3691(8) 0.4619(5) 0.044(2) Uani 1 1 d . . . . .
H109 H 0.2093 0.4299 0.4137 0.052 Uiso 1 1 calc R . . . .
N1 N 0.3664(3) 0.2544(6) 0.4652(4) 0.0339(16) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
B1 H1 1.1200 . ?
B1 B2 1.758(11) . ?
B1 B3 1.715(16) . ?
B1 B4 1.806(10) . ?
B1 B5 1.801(12) . ?
B1 B6 1.772(12) . ?
B2 H2 1.1200 . ?
B2 B3 1.700(16) . ?
B2 B6 1.758(11) . ?
B2 C7 1.710(9) . ?
B2 B11 1.793(11) . ?
B3 H3 1.1200 . ?
B3 B4 1.761(16) . ?
B3 C7 1.702(16) . ?
B3 C8 1.741(16) . ?
B4 H4 1.1200 . ?
B4 B5 1.782(12) . ?
B4 C8 1.680(11) . ?
B4 B9 1.799(12) . ?
B5 H5 1.1200 . ?
B5 B6 1.809(11) . ?
B5 B9 1.791(10) . ?
B5 B10 1.784(12) . ?
B6 H6 1.1200 . ?
B6 B10 1.762(11) . ?
B6 B11 1.763(11) . ?
C7 C8 1.563(10) . ?
C7 B11 1.680(10) . ?
C7 B12 1.662(19) . ?
C7 C1' 1.514(9) . ?
C8 H8 1.1200 . ?
C8 B9 1.620(11) . ?
C8 B12 1.622(19) . ?
B9 H9 1.1200 . ?
B9 B10 1.801(11) . ?
B9 B12 1.678(19) . ?
B10 H10 1.1200 . ?
B10 B11 1.796(12) . ?
B10 B12 1.745(18) . ?
B11 H11 1.1200 . ?
B11 B12 1.730(18) . ?
B12 H12 1.1200 . ?
C1' C2' 1.683(10) . ?
C1' B3' 1.746(10) . ?
C1' B4' 1.736(10) . ?
C1' B5' 1.734(10) . ?
C1' B6' 1.701(10) . ?
C2' H2' 1.1200 . ?
C2' B3' 1.740(10) . ?
C2' B6' 1.716(11) . ?
C2' B7' 1.712(11) . ?
C2' B11' 1.724(11) . ?
B3' H3' 1.1200 . ?
B3' B4' 1.783(11) . ?
B3' B7' 1.772(11) . ?
B3' B8' 1.772(11) . ?
B4' H4' 1.1200 . ?
B4' B5' 1.795(12) . ?
B4' B8' 1.786(11) . ?
B4' B9' 1.787(12) . ?
B5' H5' 1.1200 . ?
B5' B6' 1.727(11) . ?
B5' B9' 1.786(11) . ?
B5' B10' 1.771(12) . ?
B6' H6' 1.1200 . ?
B6' B10' 1.712(11) . ?
B6' B11' 1.725(12) . ?
B7' H7' 1.1200 . ?
B7' B8' 1.817(11) . ?
B7' B11' 1.766(12) . ?
B7' B12' 1.802(12) . ?
B8' H8' 1.1200 . ?
B8' B9' 1.787(12) . ?
B8' B12' 1.787(12) . ?
B9' H9' 1.1200 . ?
B9' B10' 1.778(12) . ?
B9' B12' 1.763(12) . ?
B10' H10' 1.1200 . ?
B10' B11' 1.778(12) . ?
B10' B12' 1.776(12) . ?
B11' H11' 1.1200 . ?
B11' B12' 1.783(11) . ?
B12' H12' 1.1200 . ?
C107 H107 0.9500 . ?
C107 C106 1.356(10) . ?
C107 C108 1.362(10) . ?
C106 H106 0.9500 . ?
C106 C105 1.370(9) . ?
C108 H108 0.9500 . ?
C108 C109 1.385(9) . ?
C102 H10A 0.9800 . ?
C102 H10B 0.9800 . ?
C102 H10C 0.9800 . ?
C102 N1 1.513(8) . ?
C101 H10D 0.9800 . ?
C101 H10E 0.9800 . ?
C101 H10F 0.9800 . ?
C101 N1 1.485(8) . ?
C100 H10G 0.9800 . ?
C100 H10H 0.9800 . ?
C100 H10I 0.9800 . ?
C100 N1 1.490(8) . ?
C105 H105 0.9500 . ?
C105 C104 1.416(9) . ?
C104 C103 1.512(9) . ?
C104 C109 1.370(10) . ?
C103 H10J 0.9900 . ?
C103 H10K 0.9900 . ?
C103 N1 1.513(8) . ?
C109 H109 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
B2 B1 H1 122.2 . . ?
B2 B1 B4 107.0(5) . . ?
B2 B1 B5 108.3(6) . . ?
B2 B1 B6 59.7(5) . . ?
B3 B1 H1 122.9 . . ?
B3 B1 B2 58.6(6) . . ?
B3 B1 B4 59.9(6) . . ?
B3 B1 B5 107.2(7) . . ?
B3 B1 B6 106.3(7) . . ?
B4 B1 H1 122.3 . . ?
B5 B1 H1 121.5 . . ?
B5 B1 B4 59.2(4) . . ?
B6 B1 H1 122.1 . . ?
B6 B1 B4 107.3(6) . . ?
B6 B1 B5 60.8(5) . . ?
B1 B2 H2 122.0 . . ?
B1 B2 B6 60.5(5) . . ?
B1 B2 B11 108.5(6) . . ?
B3 B2 B1 59.4(6) . . ?
B3 B2 H2 121.0 . . ?
B3 B2 B6 107.5(7) . . ?
B3 B2 C7 59.9(6) . . ?
B3 B2 B11 108.4(7) . . ?
B6 B2 H2 123.3 . . ?
B6 B2 B11 59.5(4) . . ?
C7 B2 B1 104.5(5) . . ?
C7 B2 H2 125.7 . . ?
C7 B2 B6 102.4(5) . . ?
C7 B2 B11 57.2(4) . . ?
B11 B2 H2 121.6 . . ?
B1 B3 H3 120.9 . . ?
B1 B3 B4 62.6(6) . . ?
B1 B3 C8 104.4(9) . . ?
B2 B3 B1 62.0(6) . . ?
B2 B3 H3 120.0 . . ?
B2 B3 B4 111.7(9) . . ?
B2 B3 C7 60.4(6) . . ?
B2 B3 C8 103.7(9) . . ?
B4 B3 H3 121.1 . . ?
C7 B3 B1 106.7(9) . . ?
C7 B3 H3 125.2 . . ?
C7 B3 B4 103.3(9) . . ?
C7 B3 C8 54.0(6) . . ?
C8 B3 H3 127.3 . . ?
C8 B3 B4 57.3(6) . . ?
B1 B4 H4 123.2 . . ?
B3 B4 B1 57.5(6) . . ?
B3 B4 H4 122.0 . . ?
B3 B4 B5 106.0(7) . . ?
B3 B4 B9 107.0(7) . . ?
B5 B4 B1 60.3(4) . . ?
B5 B4 H4 123.5 . . ?
B5 B4 B9 60.0(4) . . ?
C8 B4 B1 103.1(6) . . ?
C8 B4 B3 60.8(6) . . ?
C8 B4 H4 126.2 . . ?
C8 B4 B5 101.6(6) . . ?
C8 B4 B9 55.4(4) . . ?
B9 B4 B1 107.4(6) . . ?
B9 B4 H4 122.4 . . ?
B1 B5 H5 121.9 . . ?
B1 B5 B6 58.8(5) . . ?
B4 B5 B1 60.5(4) . . ?
B4 B5 H5 121.0 . . ?
B4 B5 B6 106.7(6) . . ?
B4 B5 B9 60.5(4) . . ?
B4 B5 B10 109.4(6) . . ?
B6 B5 H5 123.9 . . ?
B9 B5 B1 107.9(6) . . ?
B9 B5 H5 122.0 . . ?
B9 B5 B6 105.8(6) . . ?
B10 B5 B1 107.6(6) . . ?
B10 B5 H5 121.3 . . ?
B10 B5 B6 58.7(5) . . ?
B10 B5 B9 60.5(4) . . ?
B1 B6 B5 60.4(5) . . ?
B1 B6 H6 121.0 . . ?
B2 B6 B1 59.7(5) . . ?
B2 B6 B5 108.0(6) . . ?
B2 B6 H6 120.9 . . ?
B2 B6 B10 110.7(5) . . ?
B2 B6 B11 61.2(5) . . ?
B5 B6 H6 122.2 . . ?
B10 B6 B1 109.9(6) . . ?
B10 B6 B5 59.9(4) . . ?
B10 B6 H6 120.0 . . ?
B10 B6 B11 61.3(4) . . ?
B11 B6 B1 109.2(6) . . ?
B11 B6 B5 108.2(5) . . ?
B11 B6 H6 120.8 . . ?
B3 C7 B2 59.8(6) . . ?
C8 C7 B2 111.4(6) . . ?
C8 C7 B3 64.3(6) . . ?
C8 C7 B11 111.3(6) . . ?
C8 C7 B12 60.3(7) . . ?
B11 C7 B2 63.9(4) . . ?
B11 C7 B3 113.8(6) . . ?
B12 C7 B2 114.3(7) . . ?
B12 C7 B3 115.0(9) . . ?
B12 C7 B11 62.4(7) . . ?
C1' C7 B2 122.7(5) . . ?
C1' C7 B3 117.9(7) . . ?
C1' C7 C8 116.6(5) . . ?
C1' C7 B11 120.2(6) . . ?
C1' C7 B12 115.6(8) . . ?
B3 C8 H8 117.9 . . ?
B4 C8 B3 61.9(6) . . ?
B4 C8 H8 116.4 . . ?
C7 C8 B3 61.7(6) . . ?
C7 C8 B4 113.7(6) . . ?
C7 C8 H8 119.0 . . ?
C7 C8 B9 114.6(6) . . ?
C7 C8 B12 62.9(7) . . ?
B9 C8 B3 116.6(7) . . ?
B9 C8 B4 66.1(5) . . ?
B9 C8 H8 116.0 . . ?
B9 C8 B12 62.4(7) . . ?
B12 C8 B3 114.9(9) . . ?
B12 C8 B4 117.1(8) . . ?
B12 C8 H8 117.1 . . ?
B4 B9 H9 121.5 . . ?
B4 B9 B10 107.9(5) . . ?
B5 B9 B4 59.5(4) . . ?
B5 B9 H9 123.3 . . ?
B5 B9 B10 59.6(4) . . ?
C8 B9 B4 58.6(5) . . ?
C8 B9 B5 103.6(6) . . ?
C8 B9 H9 125.0 . . ?
C8 B9 B10 104.8(6) . . ?
C8 B9 B12 58.9(7) . . ?
B10 B9 H9 122.3 . . ?
B12 B9 B4 108.1(8) . . ?
B12 B9 B5 107.2(8) . . ?
B12 B9 H9 121.4 . . ?
B12 B9 B10 60.1(7) . . ?
B5 B10 B9 59.9(4) . . ?
B5 B10 H10 121.5 . . ?
B5 B10 B11 107.8(6) . . ?
B6 B10 B5 61.3(5) . . ?
B6 B10 B9 107.3(6) . . ?
B6 B10 H10 121.8 . . ?
B6 B10 B11 59.4(4) . . ?
B9 B10 H10 123.6 . . ?
B11 B10 B9 104.6(6) . . ?
B11 B10 H10 122.8 . . ?
B12 B10 B5 104.6(8) . . ?
B12 B10 B6 104.9(8) . . ?
B12 B10 B9 56.5(7) . . ?
B12 B10 H10 125.1 . . ?
B12 B10 B11 58.5(7) . . ?
B2 B11 B10 107.6(6) . . ?
B2 B11 H11 121.7 . . ?
B6 B11 B2 59.3(5) . . ?
B6 B11 B10 59.4(5) . . ?
B6 B11 H11 123.8 . . ?
C7 B11 B2 58.9(4) . . ?
C7 B11 B6 103.5(6) . . ?
C7 B11 B10 104.5(6) . . ?
C7 B11 H11 124.8 . . ?
C7 B11 B12 58.3(7) . . ?
B10 B11 H11 122.5 . . ?
B12 B11 B2 107.0(8) . . ?
B12 B11 B6 105.5(8) . . ?
B12 B11 B10 59.3(7) . . ?
B12 B11 H11 122.7 . . ?
C7 B12 B9 106.6(11) . . ?
C7 B12 B10 107.6(10) . . ?
C7 B12 B11 59.3(7) . . ?
C7 B12 H12 124.1 . . ?
C8 B12 C7 56.8(7) . . ?
C8 B12 B9 58.7(7) . . ?
C8 B12 B10 107.2(10) . . ?
C8 B12 B11 105.9(11) . . ?
C8 B12 H12 124.8 . . ?
B9 B12 B10 63.5(7) . . ?
B9 B12 B11 113.3(10) . . ?
B9 B12 H12 119.4 . . ?
B10 B12 H12 120.1 . . ?
B11 B12 B10 62.2(6) . . ?
B11 B12 H12 119.9 . . ?
C7 C1' C2' 118.1(5) . . ?
C7 C1' B3' 119.4(6) . . ?
C7 C1' B4' 122.1(6) . . ?
C7 C1' B5' 120.8(6) . . ?
C7 C1' B6' 119.3(5) . . ?
C2' C1' B3' 61.0(4) . . ?
C2' C1' B4' 110.6(5) . . ?
C2' C1' B5' 110.7(6) . . ?
C2' C1' B6' 61.0(4) . . ?
B4' C1' B3' 61.6(4) . . ?
B5' C1' B3' 112.5(5) . . ?
B5' C1' B4' 62.3(4) . . ?
B6' C1' B3' 110.7(5) . . ?
B6' C1' B4' 110.4(5) . . ?
B6' C1' B5' 60.4(4) . . ?
C1' C2' H2' 120.9 . . ?
C1' C2' B3' 61.3(4) . . ?
C1' C2' B6' 60.1(4) . . ?
C1' C2' B7' 110.7(5) . . ?
C1' C2' B11' 109.5(6) . . ?
B3' C2' H2' 119.4 . . ?
B6' C2' H2' 121.2 . . ?
B6' C2' B3' 110.3(6) . . ?
B6' C2' B11' 60.2(5) . . ?
B7' C2' H2' 119.7 . . ?
B7' C2' B3' 61.7(4) . . ?
B7' C2' B6' 110.2(6) . . ?
B7' C2' B11' 61.9(5) . . ?
B11' C2' H2' 120.1 . . ?
B11' C2' B3' 111.8(5) . . ?
C1' B3' H3' 124.3 . . ?
C1' B3' B4' 58.9(4) . . ?
C1' B3' B7' 105.1(6) . . ?
C1' B3' B8' 105.9(6) . . ?
C2' B3' C1' 57.7(4) . . ?
C2' B3' H3' 123.9 . . ?
C2' B3' B4' 105.8(6) . . ?
C2' B3' B7' 58.3(4) . . ?
C2' B3' B8' 106.6(6) . . ?
B4' B3' H3' 121.6 . . ?
B7' B3' H3' 121.6 . . ?
B7' B3' B4' 109.2(6) . . ?
B7' B3' B8' 61.7(5) . . ?
B8' B3' H3' 121.6 . . ?
B8' B3' B4' 60.3(4) . . ?
C1' B4' B3' 59.5(4) . . ?
C1' B4' H4' 123.9 . . ?
C1' B4' B5' 58.8(4) . . ?
C1' B4' B8' 105.8(6) . . ?
C1' B4' B9' 105.1(5) . . ?
B3' B4' H4' 121.8 . . ?
B3' B4' B5' 107.9(5) . . ?
B3' B4' B8' 59.5(5) . . ?
B3' B4' B9' 107.3(6) . . ?
B5' B4' H4' 121.6 . . ?
B8' B4' H4' 122.1 . . ?
B8' B4' B5' 108.1(6) . . ?
B8' B4' B9' 60.0(5) . . ?
B9' B4' H4' 122.6 . . ?
B9' B4' B5' 59.8(5) . . ?
C1' B5' B4' 58.9(4) . . ?
C1' B5' H5' 123.7 . . ?
C1' B5' B9' 105.3(6) . . ?
C1' B5' B10' 105.5(6) . . ?
B4' B5' H5' 121.8 . . ?
B6' B5' C1' 58.9(4) . . ?
B6' B5' B4' 106.6(6) . . ?
B6' B5' H5' 123.2 . . ?
B6' B5' B9' 105.7(6) . . ?
B6' B5' B10' 58.6(5) . . ?
B9' B5' B4' 59.9(5) . . ?
B9' B5' H5' 122.9 . . ?
B10' B5' B4' 108.0(6) . . ?
B10' B5' H5' 122.3 . . ?
B10' B5' B9' 60.0(5) . . ?
C1' B6' C2' 59.0(4) . . ?
C1' B6' B5' 60.8(4) . . ?
C1' B6' H6' 122.0 . . ?
C1' B6' B10' 109.7(6) . . ?
C1' B6' B11' 108.6(6) . . ?
C2' B6' B5' 109.4(6) . . ?
C2' B6' H6' 121.9 . . ?
C2' B6' B11' 60.1(5) . . ?
B5' B6' H6' 119.3 . . ?
B10' B6' C2' 109.8(6) . . ?
B10' B6' B5' 62.0(5) . . ?
B10' B6' H6' 119.7 . . ?
B10' B6' B11' 62.3(5) . . ?
B11' B6' B5' 112.4(6) . . ?
B11' B6' H6' 119.8 . . ?
C2' B7' B3' 59.9(4) . . ?
C2' B7' H7' 123.1 . . ?
C2' B7' B8' 105.9(6) . . ?
C2' B7' B11' 59.4(5) . . ?
C2' B7' B12' 105.8(6) . . ?
B3' B7' H7' 121.8 . . ?
B3' B7' B8' 59.2(4) . . ?
B3' B7' B12' 106.7(6) . . ?
B8' B7' H7' 122.7 . . ?
B11' B7' B3' 108.4(6) . . ?
B11' B7' H7' 121.3 . . ?
B11' B7' B8' 107.6(6) . . ?
B11' B7' B12' 60.0(5) . . ?
B12' B7' H7' 122.9 . . ?
B12' B7' B8' 59.2(5) . . ?
B3' B8' B4' 60.2(4) . . ?
B3' B8' B7' 59.1(4) . . ?
B3' B8' H8' 121.9 . . ?
B3' B8' B9' 107.8(6) . . ?
B3' B8' B12' 107.3(6) . . ?
B4' B8' B7' 107.1(5) . . ?
B4' B8' H8' 122.0 . . ?
B4' B8' B9' 60.0(5) . . ?
B4' B8' B12' 107.2(6) . . ?
B7' B8' H8' 122.5 . . ?
B9' B8' B7' 107.0(6) . . ?
B9' B8' H8' 122.1 . . ?
B9' B8' B12' 59.1(5) . . ?
B12' B8' B7' 60.0(5) . . ?
B12' B8' H8' 122.3 . . ?
B4' B9' H9' 121.7 . . ?
B5' B9' B4' 60.3(4) . . ?
B5' B9' B8' 108.5(6) . . ?
B5' B9' H9' 121.7 . . ?
B8' B9' B4' 60.0(5) . . ?
B8' B9' H9' 121.2 . . ?
B10' B9' B4' 108.0(5) . . ?
B10' B9' B5' 59.6(4) . . ?
B10' B9' B8' 108.7(6) . . ?
B10' B9' H9' 121.7 . . ?
B12' B9' B4' 108.2(6) . . ?
B12' B9' B5' 108.0(6) . . ?
B12' B9' B8' 60.4(5) . . ?
B12' B9' H9' 121.6 . . ?
B12' B9' B10' 60.2(5) . . ?
B5' B10' B9' 60.4(5) . . ?
B5' B10' H10' 121.5 . . ?
B5' B10' B11' 107.9(6) . . ?
B5' B10' B12' 108.0(6) . . ?
B6' B10' B5' 59.4(4) . . ?
B6' B10' B9' 106.7(6) . . ?
B6' B10' H10' 123.0 . . ?
B6' B10' B11' 59.2(4) . . ?
B6' B10' B12' 106.6(6) . . ?
B9' B10' H10' 122.1 . . ?
B11' B10' B9' 107.7(6) . . ?
B11' B10' H10' 121.7 . . ?
B12' B10' B9' 59.5(5) . . ?
B12' B10' H10' 122.0 . . ?
B12' B10' B11' 60.2(5) . . ?
C2' B11' B6' 59.7(5) . . ?
C2' B11' B7' 58.7(5) . . ?
C2' B11' B10' 106.4(6) . . ?
C2' B11' H11' 123.2 . . ?
C2' B11' B12' 106.1(6) . . ?
B6' B11' B7' 107.3(6) . . ?
B6' B11' B10' 58.5(5) . . ?
B6' B11' H11' 123.0 . . ?
B6' B11' B12' 105.8(6) . . ?
B7' B11' B10' 109.1(6) . . ?
B7' B11' H11' 121.1 . . ?
B7' B11' B12' 61.0(5) . . ?
B10' B11' H11' 121.9 . . ?
B10' B11' B12' 59.8(4) . . ?
B12' B11' H11' 122.5 . . ?
B7' B12' H12' 121.8 . . ?
B8' B12' B7' 60.8(5) . . ?
B8' B12' H12' 121.0 . . ?
B9' B12' B7' 108.7(6) . . ?
B9' B12' B8' 60.4(5) . . ?
B9' B12' B10' 60.3(5) . . ?
B9' B12' B11' 108.1(6) . . ?
B9' B12' H12' 121.2 . . ?
B10' B12' B7' 107.6(6) . . ?
B10' B12' B8' 108.7(6) . . ?
B10' B12' B11' 59.9(5) . . ?
B10' B12' H12' 121.6 . . ?
B11' B12' B7' 59.0(4) . . ?
B11' B12' B8' 108.1(6) . . ?
B11' B12' H12' 122.2 . . ?
C106 C107 H107 120.0 . . ?
C106 C107 C108 120.0(8) . . ?
C108 C107 H107 120.0 . . ?
C107 C106 H106 118.9 . . ?
C107 C106 C105 122.2(7) . . ?
C105 C106 H106 118.9 . . ?
C107 C108 H108 120.4 . . ?
C107 C108 C109 119.2(7) . . ?
C109 C108 H108 120.4 . . ?
H10A C102 H10B 109.5 . . ?
H10A C102 H10C 109.5 . . ?
H10B C102 H10C 109.5 . . ?
N1 C102 H10A 109.5 . . ?
N1 C102 H10B 109.5 . . ?
N1 C102 H10C 109.5 . . ?
H10D C101 H10E 109.5 . . ?
H10D C101 H10F 109.5 . . ?
H10E C101 H10F 109.5 . . ?
N1 C101 H10D 109.5 . . ?
N1 C101 H10E 109.5 . . ?
N1 C101 H10F 109.5 . . ?
H10G C100 H10H 109.5 . . ?
H10G C100 H10I 109.5 . . ?
H10H C100 H10I 109.5 . . ?
N1 C100 H10G 109.5 . . ?
N1 C100 H10H 109.5 . . ?
N1 C100 H10I 109.5 . . ?
C106 C105 H105 120.6 . . ?
C106 C105 C104 118.8(7) . . ?
C104 C105 H105 120.6 . . ?
C105 C104 C103 120.8(7) . . ?
C109 C104 C105 117.8(7) . . ?
C109 C104 C103 121.3(7) . . ?
C104 C103 H10J 108.5 . . ?
C104 C103 H10K 108.5 . . ?
C104 C103 N1 115.3(6) . . ?
H10J C103 H10K 107.5 . . ?
N1 C103 H10J 108.5 . . ?
N1 C103 H10K 108.5 . . ?
C108 C109 H109 119.0 . . ?
C104 C109 C108 122.1(7) . . ?
C104 C109 H109 119.0 . . ?
C101 N1 C102 109.2(6) . . ?
C101 N1 C100 108.7(5) . . ?
C101 N1 C103 111.2(5) . . ?
C100 N1 C102 109.8(5) . . ?
C100 N1 C103 107.6(5) . . ?
C103 N1 C102 110.4(5) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
B1 B2 B3 B4 -39.4(7) . . . . ?
B1 B2 B3 C7 -132.7(8) . . . . ?
B1 B2 B3 C8 -99.3(8) . . . . ?
B1 B2 B6 B5 37.7(5) . . . . ?
B1 B2 B6 B10 101.6(6) . . . . ?
B1 B2 B6 B11 139.1(5) . . . . ?
B1 B2 C7 B3 40.8(7) . . . . ?
B1 B2 C7 C8 1.0(8) . . . . ?
B1 B2 C7 B11 -102.9(6) . . . . ?
B1 B2 C7 B12 -65.0(9) . . . . ?
B1 B2 C7 C1' 146.5(6) . . . . ?
B1 B2 B11 B6 -37.0(5) . . . . ?
B1 B2 B11 C7 95.6(6) . . . . ?
B1 B2 B11 B10 -1.1(6) . . . . ?
B1 B2 B11 B12 61.3(8) . . . . ?
B1 B3 B4 B5 -37.3(7) . . . . ?
B1 B3 B4 C8 -131.7(8) . . . . ?
B1 B3 B4 B9 -100.1(6) . . . . ?
B1 B3 C7 B2 -42.7(7) . . . . ?
B1 B3 C7 C8 95.9(9) . . . . ?
B1 B3 C7 B11 -7.2(11) . . . . ?
B1 B3 C7 B12 62.1(11) . . . . ?
B1 B3 C7 C1' -156.2(7) . . . . ?
B1 B3 C8 B4 43.2(7) . . . . ?
B1 B3 C8 C7 -100.4(8) . . . . ?
B1 B3 C8 B9 4.6(11) . . . . ?
B1 B3 C8 B12 -65.5(11) . . . . ?
B1 B4 B5 B6 -37.7(5) . . . . ?
B1 B4 B5 B9 -136.7(6) . . . . ?
B1 B4 B5 B10 -99.7(6) . . . . ?
B1 B4 C8 B3 -40.2(7) . . . . ?
B1 B4 C8 C7 -5.3(8) . . . . ?
B1 B4 C8 B9 102.2(6) . . . . ?
B1 B4 C8 B12 65.1(10) . . . . ?
B1 B4 B9 B5 38.6(5) . . . . ?
B1 B4 B9 C8 -94.2(6) . . . . ?
B1 B4 B9 B10 2.5(7) . . . . ?
B1 B4 B9 B12 -61.0(8) . . . . ?
B1 B5 B6 B2 -37.4(5) . . . . ?
B1 B5 B6 B10 -141.4(6) . . . . ?
B1 B5 B6 B11 -102.2(6) . . . . ?
B1 B5 B9 B4 -38.9(5) . . . . ?
B1 B5 B9 C8 1.2(8) . . . . ?
B1 B5 B9 B10 100.5(6) . . . . ?
B1 B5 B9 B12 62.4(9) . . . . ?
B1 B5 B10 B6 34.0(5) . . . . ?
B1 B5 B10 B9 -101.1(6) . . . . ?
B1 B5 B10 B11 -4.2(7) . . . . ?
B1 B5 B10 B12 -65.2(8) . . . . ?
B1 B6 B10 B5 -35.2(5) . . . . ?
B1 B6 B10 B9 4.5(8) . . . . ?
B1 B6 B10 B11 101.6(6) . . . . ?
B1 B6 B10 B12 63.5(9) . . . . ?
B1 B6 B11 B2 36.8(5) . . . . ?
B1 B6 B11 C7 -3.7(7) . . . . ?
B1 B6 B11 B10 -102.7(6) . . . . ?
B1 B6 B11 B12 -64.1(9) . . . . ?
B2 B1 B3 B4 138.4(8) . . . . ?
B2 B1 B3 C7 41.9(6) . . . . ?
B2 B1 B3 C8 98.0(9) . . . . ?
B2 B1 B4 B3 -36.3(7) . . . . ?
B2 B1 B4 B5 101.6(7) . . . . ?
B2 B1 B4 C8 5.6(8) . . . . ?
B2 B1 B4 B9 63.1(7) . . . . ?
B2 B1 B5 B4 -99.3(6) . . . . ?
B2 B1 B5 B6 37.5(5) . . . . ?
B2 B1 B5 B9 -60.4(7) . . . . ?
B2 B1 B5 B10 3.5(7) . . . . ?
B2 B1 B6 B5 -138.0(5) . . . . ?
B2 B1 B6 B10 -102.9(6) . . . . ?
B2 B1 B6 B11 -37.4(5) . . . . ?
B2 B3 B4 B1 39.1(7) . . . . ?
B2 B3 B4 B5 1.8(10) . . . . ?
B2 B3 B4 C8 -92.7(9) . . . . ?
B2 B3 B4 B9 -61.1(9) . . . . ?
B2 B3 C7 C8 138.6(7) . . . . ?
B2 B3 C7 B11 35.5(7) . . . . ?
B2 B3 C7 B12 104.7(8) . . . . ?
B2 B3 C7 C1' -113.5(7) . . . . ?
B2 B3 C8 B4 107.2(8) . . . . ?
B2 B3 C8 C7 -36.3(6) . . . . ?
B2 B3 C8 B9 68.7(10) . . . . ?
B2 B3 C8 B12 -1.5(12) . . . . ?
B2 B6 B10 B5 -99.3(6) . . . . ?
B2 B6 B10 B9 -59.6(7) . . . . ?
B2 B6 B10 B11 37.5(5) . . . . ?
B2 B6 B10 B12 -0.6(9) . . . . ?
B2 B6 B11 C7 -40.4(5) . . . . ?
B2 B6 B11 B10 -139.5(6) . . . . ?
B2 B6 B11 B12 -100.9(8) . . . . ?
B2 C7 C8 B3 37.9(7) . . . . ?
B2 C7 C8 B4 2.9(9) . . . . ?
B2 C7 C8 B9 -70.4(8) . . . . ?
B2 C7 C8 B12 -106.6(8) . . . . ?
B2 C7 B11 B6 40.6(5) . . . . ?
B2 C7 B11 B10 102.0(6) . . . . ?
B2 C7 B11 B12 140.8(8) . . . . ?
B2 C7 B12 C8 101.8(7) . . . . ?
B2 C7 B12 B9 69.1(10) . . . . ?
B2 C7 B12 B10 2.3(12) . . . . ?
B2 C7 B12 B11 -38.6(8) . . . . ?
B2 C7 C1' C2' 39.0(9) . . . . ?
B2 C7 C1' B3' 109.7(7) . . . . ?
B2 C7 C1' B4' -177.2(6) . . . . ?
B2 C7 C1' B5' -102.6(7) . . . . ?
B2 C7 C1' B6' -31.6(9) . . . . ?
B2 B11 B12 C7 34.5(7) . . . . ?
B2 B11 B12 C8 0.7(11) . . . . ?
B2 B11 B12 B9 -61.6(11) . . . . ?
B2 B11 B12 B10 -100.7(7) . . . . ?
B3 B1 B2 B6 -137.4(8) . . . . ?
B3 B1 B2 C7 -41.1(7) . . . . ?
B3 B1 B2 B11 -100.9(8) . . . . ?
B3 B1 B4 B5 137.9(8) . . . . ?
B3 B1 B4 C8 42.0(7) . . . . ?
B3 B1 B4 B9 99.4(8) . . . . ?
B3 B1 B5 B4 -37.4(7) . . . . ?
B3 B1 B5 B6 99.4(7) . . . . ?
B3 B1 B5 B9 1.5(9) . . . . ?
B3 B1 B5 B10 65.4(8) . . . . ?
B3 B1 B6 B2 37.0(7) . . . . ?
B3 B1 B6 B5 -100.9(7) . . . . ?
B3 B1 B6 B10 -65.9(8) . . . . ?
B3 B1 B6 B11 -0.4(8) . . . . ?
B3 B2 B6 B1 -37.7(7) . . . . ?
B3 B2 B6 B5 0.0(8) . . . . ?
B3 B2 B6 B10 63.9(8) . . . . ?
B3 B2 B6 B11 101.4(7) . . . . ?
B3 B2 C7 C8 -39.8(8) . . . . ?
B3 B2 C7 B11 -143.8(8) . . . . ?
B3 B2 C7 B12 -105.8(10) . . . . ?
B3 B2 C7 C1' 105.6(8) . . . . ?
B3 B2 B11 B6 -100.0(7) . . . . ?
B3 B2 B11 C7 32.6(7) . . . . ?
B3 B2 B11 B10 -64.1(7) . . . . ?
B3 B2 B11 B12 -1.7(10) . . . . ?
B3 B4 B5 B1 36.0(7) . . . . ?
B3 B4 B5 B6 -1.7(8) . . . . ?
B3 B4 B5 B9 -100.6(7) . . . . ?
B3 B4 B5 B10 -63.7(8) . . . . ?
B3 B4 C8 C7 34.9(7) . . . . ?
B3 B4 C8 B9 142.5(7) . . . . ?
B3 B4 C8 B12 105.3(10) . . . . ?
B3 B4 B9 B5 99.0(7) . . . . ?
B3 B4 B9 C8 -33.8(6) . . . . ?
B3 B4 B9 B10 62.9(7) . . . . ?
B3 B4 B9 B12 -0.6(9) . . . . ?
B3 C7 C8 B4 -35.0(7) . . . . ?
B3 C7 C8 B9 -108.3(8) . . . . ?
B3 C7 C8 B12 -144.4(9) . . . . ?
B3 C7 B11 B2 -33.9(7) . . . . ?
B3 C7 B11 B6 6.7(9) . . . . ?
B3 C7 B11 B10 68.1(8) . . . . ?
B3 C7 B11 B12 106.8(10) . . . . ?
B3 C7 B12 C8 35.3(8) . . . . ?
B3 C7 B12 B9 2.6(12) . . . . ?
B3 C7 B12 B10 -64.1(12) . . . . ?
B3 C7 B12 B11 -105.0(8) . . . . ?
B3 C7 C1' C2' 109.3(8) . . . . ?
B3 C7 C1' B3' -180.0(7) . . . . ?
B3 C7 C1' B4' -106.9(8) . . . . ?
B3 C7 C1' B5' -32.3(9) . . . . ?
B3 C7 C1' B6' 38.7(9) . . . . ?
B3 C8 B9 B4 37.0(7) . . . . ?
B3 C8 B9 B5 -3.6(10) . . . . ?
B3 C8 B9 B10 -65.2(9) . . . . ?
B3 C8 B9 B12 -105.7(10) . . . . ?
B3 C8 B12 C7 -34.4(8) . . . . ?
B3 C8 B12 B9 108.3(8) . . . . ?
B3 C8 B12 B10 65.7(12) . . . . ?
B3 C8 B12 B11 0.4(13) . . . . ?
B4 B1 B2 B3 36.9(7) . . . . ?
B4 B1 B2 B6 -100.5(6) . . . . ?
B4 B1 B2 C7 -4.2(7) . . . . ?
B4 B1 B2 B11 -64.0(7) . . . . ?
B4 B1 B3 B2 -138.4(8) . . . . ?
B4 B1 B3 C7 -96.6(9) . . . . ?
B4 B1 B3 C8 -40.4(6) . . . . ?
B4 B1 B5 B6 136.8(6) . . . . ?
B4 B1 B5 B9 38.9(5) . . . . ?
B4 B1 B5 B10 102.8(6) . . . . ?
B4 B1 B6 B2 99.9(6) . . . . ?
B4 B1 B6 B5 -38.0(5) . . . . ?
B4 B1 B6 B10 -3.0(8) . . . . ?
B4 B1 B6 B11 62.5(7) . . . . ?
B4 B3 C7 B2 -107.6(8) . . . . ?
B4 B3 C7 C8 30.9(6) . . . . ?
B4 B3 C7 B11 -72.2(8) . . . . ?
B4 B3 C7 B12 -2.9(11) . . . . ?
B4 B3 C7 C1' 138.8(6) . . . . ?
B4 B3 C8 C7 -143.5(7) . . . . ?
B4 B3 C8 B9 -38.5(7) . . . . ?
B4 B3 C8 B12 -108.7(9) . . . . ?
B4 B5 B6 B1 38.5(5) . . . . ?
B4 B5 B6 B2 1.0(7) . . . . ?
B4 B5 B6 B10 -102.9(6) . . . . ?
B4 B5 B6 B11 -63.8(7) . . . . ?
B4 B5 B9 C8 40.1(6) . . . . ?
B4 B5 B9 B10 139.4(6) . . . . ?
B4 B5 B9 B12 101.3(8) . . . . ?
B4 B5 B10 B6 98.2(6) . . . . ?
B4 B5 B10 B9 -36.9(5) . . . . ?
B4 B5 B10 B11 60.0(6) . . . . ?
B4 B5 B10 B12 -1.0(9) . . . . ?
B4 C8 B9 B5 -40.6(5) . . . . ?
B4 C8 B9 B10 -102.2(6) . . . . ?
B4 C8 B9 B12 -142.6(8) . . . . ?
B4 C8 B12 C7 -104.2(8) . . . . ?
B4 C8 B12 B9 38.5(8) . . . . ?
B4 C8 B12 B10 -4.1(13) . . . . ?
B4 C8 B12 B11 -69.4(11) . . . . ?
B4 B9 B10 B5 36.1(6) . . . . ?
B4 B9 B10 B6 -4.3(7) . . . . ?
B4 B9 B10 B11 -66.3(7) . . . . ?
B4 B9 B10 B12 -101.0(9) . . . . ?
B4 B9 B12 C7 -1.1(11) . . . . ?
B4 B9 B12 C8 -33.0(7) . . . . ?
B4 B9 B12 B10 100.7(7) . . . . ?
B4 B9 B12 B11 62.1(11) . . . . ?
B5 B1 B2 B3 99.4(8) . . . . ?
B5 B1 B2 B6 -38.0(5) . . . . ?
B5 B1 B2 C7 58.3(6) . . . . ?
B5 B1 B2 B11 -1.5(7) . . . . ?
B5 B1 B3 B2 -101.4(7) . . . . ?
B5 B1 B3 B4 37.1(7) . . . . ?
B5 B1 B3 C7 -59.5(9) . . . . ?
B5 B1 B3 C8 -3.3(10) . . . . ?
B5 B1 B4 B3 -137.9(8) . . . . ?
B5 B1 B4 C8 -95.9(6) . . . . ?
B5 B1 B4 B9 -38.5(5) . . . . ?
B5 B1 B6 B2 138.0(5) . . . . ?
B5 B1 B6 B10 35.0(5) . . . . ?
B5 B1 B6 B11 100.5(6) . . . . ?
B5 B4 C8 B3 -102.0(7) . . . . ?
B5 B4 C8 C7 -67.2(8) . . . . ?
B5 B4 C8 B9 40.4(5) . . . . ?
B5 B4 C8 B12 3.3(10) . . . . ?
B5 B4 B9 C8 -132.8(6) . . . . ?
B5 B4 B9 B10 -36.1(6) . . . . ?
B5 B4 B9 B12 -99.7(8) . . . . ?
B5 B6 B10 B9 39.8(5) . . . . ?
B5 B6 B10 B11 136.8(6) . . . . ?
B5 B6 B10 B12 98.7(8) . . . . ?
B5 B6 B11 B2 100.9(6) . . . . ?
B5 B6 B11 C7 60.5(7) . . . . ?
B5 B6 B11 B10 -38.6(5) . . . . ?
B5 B6 B11 B12 0.1(9) . . . . ?
B5 B9 B10 B6 -40.4(6) . . . . ?
B5 B9 B10 B11 -102.4(6) . . . . ?
B5 B9 B10 B12 -137.2(9) . . . . ?
B5 B9 B12 C7 -63.9(10) . . . . ?
B5 B9 B12 C8 -95.8(7) . . . . ?
B5 B9 B12 B10 37.8(7) . . . . ?
B5 B9 B12 B11 -0.7(13) . . . . ?
B5 B10 B11 B2 3.3(6) . . . . ?
B5 B10 B11 B6 39.1(5) . . . . ?
B5 B10 B11 C7 -58.2(6) . . . . ?
B5 B10 B11 B12 -96.5(9) . . . . ?
B5 B10 B12 C7 62.7(10) . . . . ?
B5 B10 B12 C8 2.9(12) . . . . ?
B5 B10 B12 B9 -37.4(7) . . . . ?
B5 B10 B12 B11 102.2(7) . . . . ?
B6 B1 B2 B3 137.4(8) . . . . ?
B6 B1 B2 C7 96.3(5) . . . . ?
B6 B1 B2 B11 36.5(5) . . . . ?
B6 B1 B3 B2 -37.6(6) . . . . ?
B6 B1 B3 B4 100.9(7) . . . . ?
B6 B1 B3 C7 4.3(10) . . . . ?
B6 B1 B3 C8 60.5(9) . . . . ?
B6 B1 B4 B3 -99.1(8) . . . . ?
B6 B1 B4 B5 38.8(6) . . . . ?
B6 B1 B4 C8 -57.2(7) . . . . ?
B6 B1 B4 B9 0.2(7) . . . . ?
B6 B1 B5 B4 -136.8(6) . . . . ?
B6 B1 B5 B9 -97.9(6) . . . . ?
B6 B1 B5 B10 -34.0(5) . . . . ?
B6 B2 B3 B1 38.2(6) . . . . ?
B6 B2 B3 B4 -1.2(10) . . . . ?
B6 B2 B3 C7 -94.5(6) . . . . ?
B6 B2 B3 C8 -61.1(8) . . . . ?
B6 B2 C7 B3 103.2(8) . . . . ?
B6 B2 C7 C8 63.4(7) . . . . ?
B6 B2 C7 B11 -40.5(5) . . . . ?
B6 B2 C7 B12 -2.6(10) . . . . ?
B6 B2 C7 C1' -151.1(6) . . . . ?
B6 B2 B11 C7 132.6(6) . . . . ?
B6 B2 B11 B10 35.9(5) . . . . ?
B6 B2 B11 B12 98.3(8) . . . . ?
B6 B5 B9 B4 -100.6(6) . . . . ?
B6 B5 B9 C8 -60.5(7) . . . . ?
B6 B5 B9 B10 38.8(6) . . . . ?
B6 B5 B9 B12 0.7(9) . . . . ?
B6 B5 B10 B9 -135.1(6) . . . . ?
B6 B5 B10 B11 -38.2(5) . . . . ?
B6 B5 B10 B12 -99.3(8) . . . . ?
B6 B10 B11 B2 -35.8(5) . . . . ?
B6 B10 B11 C7 -97.3(6) . . . . ?
B6 B10 B11 B12 -135.6(9) . . . . ?
B6 B10 B12 C7 -0.9(11) . . . . ?
B6 B10 B12 C8 -60.8(11) . . . . ?
B6 B10 B12 B9 -101.1(7) . . . . ?
B6 B10 B12 B11 38.6(7) . . . . ?
B6 B11 B12 C7 96.5(7) . . . . ?
B6 B11 B12 C8 62.7(10) . . . . ?
B6 B11 B12 B9 0.4(13) . . . . ?
B6 B11 B12 B10 -38.7(7) . . . . ?
C7 B2 B3 B1 132.7(8) . . . . ?
C7 B2 B3 B4 93.3(9) . . . . ?
C7 B2 B3 C8 33.4(6) . . . . ?
C7 B2 B6 B1 -99.7(6) . . . . ?
C7 B2 B6 B5 -62.0(6) . . . . ?
C7 B2 B6 B10 1.9(7) . . . . ?
C7 B2 B6 B11 39.4(5) . . . . ?
C7 B2 B11 B6 -132.6(6) . . . . ?
C7 B2 B11 B10 -96.7(5) . . . . ?
C7 B2 B11 B12 -34.3(7) . . . . ?
C7 B3 B4 B1 102.1(8) . . . . ?
C7 B3 B4 B5 64.9(8) . . . . ?
C7 B3 B4 C8 -29.6(6) . . . . ?
C7 B3 B4 B9 2.0(8) . . . . ?
C7 B3 C8 B4 143.5(7) . . . . ?
C7 B3 C8 B9 105.0(8) . . . . ?
C7 B3 C8 B12 34.8(9) . . . . ?
C7 C8 B9 B4 106.3(7) . . . . ?
C7 C8 B9 B5 65.7(8) . . . . ?
C7 C8 B9 B10 4.1(8) . . . . ?
C7 C8 B9 B12 -36.3(8) . . . . ?
C7 C8 B12 B9 142.7(8) . . . . ?
C7 C8 B12 B10 100.1(10) . . . . ?
C7 C8 B12 B11 34.8(7) . . . . ?
C7 B11 B12 C8 -33.8(7) . . . . ?
C7 B11 B12 B9 -96.1(11) . . . . ?
C7 B11 B12 B10 -135.2(9) . . . . ?
C7 C1' C2' B3' 109.8(6) . . . . ?
C7 C1' C2' B6' -109.7(6) . . . . ?
C7 C1' C2' B7' 148.3(6) . . . . ?
C7 C1' C2' B11' -145.4(6) . . . . ?
C7 C1' B3' C2' -107.8(6) . . . . ?
C7 C1' B3' B4' 112.9(7) . . . . ?
C7 C1' B3' B7' -143.5(6) . . . . ?
C7 C1' B3' B8' 152.3(6) . . . . ?
C7 C1' B4' B3' -108.6(7) . . . . ?
C7 C1' B4' B5' 110.6(7) . . . . ?
C7 C1' B4' B8' -147.5(6) . . . . ?
C7 C1' B4' B9' 150.0(6) . . . . ?
C7 C1' B5' B4' -112.8(7) . . . . ?
C7 C1' B5' B6' 108.4(7) . . . . ?
C7 C1' B5' B9' -152.2(6) . . . . ?
C7 C1' B5' B10' 145.3(6) . . . . ?
C7 C1' B6' C2' 107.9(6) . . . . ?
C7 C1' B6' B5' -110.8(7) . . . . ?
C7 C1' B6' B10' -150.3(6) . . . . ?
C7 C1' B6' B11' 143.3(6) . . . . ?
C8 B3 B4 B1 131.7(8) . . . . ?
C8 B3 B4 B5 94.5(7) . . . . ?
C8 B3 B4 B9 31.6(6) . . . . ?
C8 B3 C7 B2 -138.6(7) . . . . ?
C8 B3 C7 B11 -103.1(7) . . . . ?
C8 B3 C7 B12 -33.9(8) . . . . ?
C8 B3 C7 C1' 107.9(7) . . . . ?
C8 B4 B5 B1 98.6(6) . . . . ?
C8 B4 B5 B6 60.9(6) . . . . ?
C8 B4 B5 B9 -38.0(5) . . . . ?
C8 B4 B5 B10 -1.1(7) . . . . ?
C8 B4 B9 B5 132.8(6) . . . . ?
C8 B4 B9 B10 96.7(6) . . . . ?
C8 B4 B9 B12 33.2(7) . . . . ?
C8 C7 B11 B2 -104.2(6) . . . . ?
C8 C7 B11 B6 -63.6(7) . . . . ?
C8 C7 B11 B10 -2.2(7) . . . . ?
C8 C7 B11 B12 36.5(8) . . . . ?
C8 C7 B12 B9 -32.7(7) . . . . ?
C8 C7 B12 B10 -99.5(10) . . . . ?
C8 C7 B12 B11 -140.3(8) . . . . ?
C8 C7 C1' C2' -177.1(6) . . . . ?
C8 C7 C1' B3' -106.5(7) . . . . ?
C8 C7 C1' B4' -33.4(9) . . . . ?
C8 C7 C1' B5' 41.3(9) . . . . ?
C8 C7 C1' B6' 112.2(7) . . . . ?
C8 B9 B10 B5 97.3(6) . . . . ?
C8 B9 B10 B6 56.9(7) . . . . ?
C8 B9 B10 B11 -5.0(7) . . . . ?
C8 B9 B10 B12 -39.8(8) . . . . ?
C8 B9 B12 C7 31.9(7) . . . . ?
C8 B9 B12 B10 133.7(9) . . . . ?
C8 B9 B12 B11 95.1(11) . . . . ?
B9 B4 B5 B1 136.7(6) . . . . ?
B9 B4 B5 B6 99.0(6) . . . . ?
B9 B4 B5 B10 36.9(5) . . . . ?
B9 B4 C8 B3 -142.5(7) . . . . ?
B9 B4 C8 C7 -107.6(7) . . . . ?
B9 B4 C8 B12 -37.1(9) . . . . ?
B9 B5 B6 B1 101.7(6) . . . . ?
B9 B5 B6 B2 64.3(7) . . . . ?
B9 B5 B6 B10 -39.7(5) . . . . ?
B9 B5 B6 B11 -0.5(8) . . . . ?
B9 B5 B10 B6 135.1(6) . . . . ?
B9 B5 B10 B11 96.9(6) . . . . ?
B9 B5 B10 B12 35.8(7) . . . . ?
B9 C8 B12 C7 -142.7(8) . . . . ?
B9 C8 B12 B10 -42.6(8) . . . . ?
B9 C8 B12 B11 -107.9(10) . . . . ?
B9 B10 B11 B2 65.8(6) . . . . ?
B9 B10 B11 B6 101.7(6) . . . . ?
B9 B10 B11 C7 4.4(7) . . . . ?
B9 B10 B11 B12 -33.9(8) . . . . ?
B9 B10 B12 C7 100.2(11) . . . . ?
B9 B10 B12 C8 40.3(8) . . . . ?
B9 B10 B12 B11 139.6(9) . . . . ?
B10 B5 B6 B1 141.4(6) . . . . ?
B10 B5 B6 B2 104.0(6) . . . . ?
B10 B5 B6 B11 39.2(5) . . . . ?
B10 B5 B9 B4 -139.4(6) . . . . ?
B10 B5 B9 C8 -99.3(7) . . . . ?
B10 B5 B9 B12 -38.1(8) . . . . ?
B10 B6 B11 B2 139.5(6) . . . . ?
B10 B6 B11 C7 99.1(6) . . . . ?
B10 B6 B11 B12 38.6(8) . . . . ?
B10 B9 B12 C7 -101.8(10) . . . . ?
B10 B9 B12 C8 -133.7(9) . . . . ?
B10 B9 B12 B11 -38.6(8) . . . . ?
B10 B11 B12 C7 135.2(9) . . . . ?
B10 B11 B12 C8 101.4(10) . . . . ?
B10 B11 B12 B9 39.1(8) . . . . ?
B11 B2 B3 B1 101.1(7) . . . . ?
B11 B2 B3 B4 61.7(9) . . . . ?
B11 B2 B3 C7 -31.6(6) . . . . ?
B11 B2 B3 C8 1.8(9) . . . . ?
B11 B2 B6 B1 -139.1(5) . . . . ?
B11 B2 B6 B5 -101.4(6) . . . . ?
B11 B2 B6 B10 -37.5(5) . . . . ?
B11 B2 C7 B3 143.8(8) . . . . ?
B11 B2 C7 C8 104.0(7) . . . . ?
B11 B2 C7 B12 38.0(8) . . . . ?
B11 B2 C7 C1' -110.6(7) . . . . ?
B11 B6 B10 B5 -136.8(6) . . . . ?
B11 B6 B10 B9 -97.1(6) . . . . ?
B11 B6 B10 B12 -38.1(8) . . . . ?
B11 C7 C8 B3 107.1(7) . . . . ?
B11 C7 C8 B4 72.1(8) . . . . ?
B11 C7 C8 B9 -1.2(9) . . . . ?
B11 C7 C8 B12 -37.4(8) . . . . ?
B11 C7 B12 C8 140.3(8) . . . . ?
B11 C7 B12 B9 107.6(10) . . . . ?
B11 C7 B12 B10 40.9(8) . . . . ?
B11 C7 C1' C2' -37.6(8) . . . . ?
B11 C7 C1' B3' 33.1(8) . . . . ?
B11 C7 C1' B4' 106.2(7) . . . . ?
B11 C7 C1' B5' -179.2(6) . . . . ?
B11 C7 C1' B6' -108.2(7) . . . . ?
B11 B10 B12 C7 -39.5(8) . . . . ?
B11 B10 B12 C8 -99.3(11) . . . . ?
B11 B10 B12 B9 -139.6(9) . . . . ?
B12 C7 C8 B3 144.4(9) . . . . ?
B12 C7 C8 B4 109.5(9) . . . . ?
B12 C7 C8 B9 36.2(8) . . . . ?
B12 C7 B11 B2 -140.8(8) . . . . ?
B12 C7 B11 B6 -100.1(9) . . . . ?
B12 C7 B11 B10 -38.8(8) . . . . ?
B12 C7 C1' C2' -109.1(9) . . . . ?
B12 C7 C1' B3' -38.5(10) . . . . ?
B12 C7 C1' B4' 34.6(10) . . . . ?
B12 C7 C1' B5' 109.3(9) . . . . ?
B12 C7 C1' B6' -179.8(8) . . . . ?
B12 C8 B9 B4 142.6(8) . . . . ?
B12 C8 B9 B5 102.0(8) . . . . ?
B12 C8 B9 B10 40.4(8) . . . . ?
B12 B9 B10 B5 137.2(9) . . . . ?
B12 B9 B10 B6 96.7(9) . . . . ?
B12 B9 B10 B11 34.8(8) . . . . ?
B12 B10 B11 B2 99.8(9) . . . . ?
B12 B10 B11 B6 135.6(9) . . . . ?
B12 B10 B11 C7 38.3(8) . . . . ?
C1' C7 C8 B3 -109.9(8) . . . . ?
C1' C7 C8 B4 -144.8(6) . . . . ?
C1' C7 C8 B9 141.8(6) . . . . ?
C1' C7 C8 B12 105.7(9) . . . . ?
C1' C7 B11 B2 114.3(7) . . . . ?
C1' C7 B11 B6 154.9(6) . . . . ?
C1' C7 B11 B10 -143.7(6) . . . . ?
C1' C7 B11 B12 -105.0(9) . . . . ?
C1' C7 B12 C8 -107.4(7) . . . . ?
C1' C7 B12 B9 -140.1(7) . . . . ?
C1' C7 B12 B10 153.2(7) . . . . ?
C1' C7 B12 B11 112.3(7) . . . . ?
C1' C2' B3' B4' 35.6(5) . . . . ?
C1' C2' B3' B7' 138.6(6) . . . . ?
C1' C2' B3' B8' 98.6(6) . . . . ?
C1' C2' B6' B5' -35.4(5) . . . . ?
C1' C2' B6' B10' -101.6(6) . . . . ?
C1' C2' B6' B11' -140.7(5) . . . . ?
C1' C2' B7' B3' -38.3(6) . . . . ?
C1' C2' B7' B8' 0.4(8) . . . . ?
C1' C2' B7' B11' 101.7(7) . . . . ?
C1' C2' B7' B12' 62.1(7) . . . . ?
C1' C2' B11' B6' 35.6(5) . . . . ?
C1' C2' B11' B7' -103.6(6) . . . . ?
C1' C2' B11' B10' -0.9(7) . . . . ?
C1' C2' B11' B12' -63.5(7) . . . . ?
C1' B3' B4' B5' 34.6(5) . . . . ?
C1' B3' B4' B8' 135.5(6) . . . . ?
C1' B3' B4' B9' 97.7(6) . . . . ?
C1' B3' B7' C2' 35.4(5) . . . . ?
C1' B3' B7' B8' -100.3(6) . . . . ?
C1' B3' B7' B11' -0.3(7) . . . . ?
C1' B3' B7' B12' -63.5(6) . . . . ?
C1' B3' B8' B4' -38.7(5) . . . . ?
C1' B3' B8' B7' 98.8(6) . . . . ?
C1' B3' B8' B9' -0.7(7) . . . . ?
C1' B3' B8' B12' 61.6(7) . . . . ?
C1' B4' B5' B6' 36.0(5) . . . . ?
C1' B4' B5' B9' 134.9(6) . . . . ?
C1' B4' B5' B10' 97.6(6) . . . . ?
C1' B4' B8' B3' 38.9(5) . . . . ?
C1' B4' B8' B7' 1.5(7) . . . . ?
C1' B4' B8' B9' -98.6(6) . . . . ?
C1' B4' B8' B12' -61.6(6) . . . . ?
C1' B4' B9' B5' -38.9(5) . . . . ?
C1' B4' B9' B8' 99.7(6) . . . . ?
C1' B4' B9' B10' -1.8(8) . . . . ?
C1' B4' B9' B12' 61.9(7) . . . . ?
C1' B5' B6' C2' 34.6(5) . . . . ?
C1' B5' B6' B10' 137.3(6) . . . . ?
C1' B5' B6' B11' 99.4(6) . . . . ?
C1' B5' B9' B4' 39.0(5) . . . . ?
C1' B5' B9' B8' 1.9(7) . . . . ?
C1' B5' B9' B10' -99.4(6) . . . . ?
C1' B5' B9' B12' -62.1(7) . . . . ?
C1' B5' B10' B6' -37.0(5) . . . . ?
C1' B5' B10' B9' 98.9(6) . . . . ?
C1' B5' B10' B11' -1.7(7) . . . . ?
C1' B5' B10' B12' 62.0(7) . . . . ?
C1' B6' B10' B5' 38.9(6) . . . . ?
C1' B6' B10' B9' -0.2(8) . . . . ?
C1' B6' B10' B11' -101.2(6) . . . . ?
C1' B6' B10' B12' -62.6(7) . . . . ?
C1' B6' B11' C2' -35.0(5) . . . . ?
C1' B6' B11' B7' 0.8(7) . . . . ?
C1' B6' B11' B10' 103.0(6) . . . . ?
C1' B6' B11' B12' 64.7(7) . . . . ?
C2' C1' B3' B4' -139.2(6) . . . . ?
C2' C1' B3' B7' -35.6(5) . . . . ?
C2' C1' B3' B8' -99.9(6) . . . . ?
C2' C1' B4' B3' 37.6(6) . . . . ?
C2' C1' B4' B5' -103.2(6) . . . . ?
C2' C1' B4' B8' -1.3(7) . . . . ?
C2' C1' B4' B9' -63.8(7) . . . . ?
C2' C1' B5' B4' 103.1(6) . . . . ?
C2' C1' B5' B6' -35.8(5) . . . . ?
C2' C1' B5' B9' 63.6(7) . . . . ?
C2' C1' B5' B10' 1.2(7) . . . . ?
C2' C1' B6' B5' 141.3(6) . . . . ?
C2' C1' B6' B10' 101.8(6) . . . . ?
C2' C1' B6' B11' 35.4(5) . . . . ?
C2' B3' B4' C1' -35.0(5) . . . . ?
C2' B3' B4' B5' -0.4(7) . . . . ?
C2' B3' B4' B8' 100.4(6) . . . . ?
C2' B3' B4' B9' 62.6(6) . . . . ?
C2' B3' B7' B8' -135.6(7) . . . . ?
C2' B3' B7' B11' -35.7(5) . . . . ?
C2' B3' B7' B12' -98.9(7) . . . . ?
C2' B3' B8' B4' -99.0(6) . . . . ?
C2' B3' B8' B7' 38.4(5) . . . . ?
C2' B3' B8' B9' -61.1(7) . . . . ?
C2' B3' B8' B12' 1.2(7) . . . . ?
C2' B6' B10' B5' 102.0(6) . . . . ?
C2' B6' B10' B9' 62.9(7) . . . . ?
C2' B6' B10' B11' -38.1(5) . . . . ?
C2' B6' B10' B12' 0.5(8) . . . . ?
C2' B6' B11' B7' 35.8(5) . . . . ?
C2' B6' B11' B10' 137.9(6) . . . . ?
C2' B6' B11' B12' 99.7(6) . . . . ?
C2' B7' B8' B3' -39.0(6) . . . . ?
C2' B7' B8' B4' -1.1(8) . . . . ?
C2' B7' B8' B9' 61.9(7) . . . . ?
C2' B7' B8' B12' 99.2(7) . . . . ?
C2' B7' B11' B6' -36.2(5) . . . . ?
C2' B7' B11' B10' -98.1(7) . . . . ?
C2' B7' B11' B12' -135.0(6) . . . . ?
C2' B7' B12' B8' -99.4(6) . . . . ?
C2' B7' B12' B9' -61.1(7) . . . . ?
C2' B7' B12' B10' 2.7(7) . . . . ?
C2' B7' B12' B11' 39.3(5) . . . . ?
C2' B11' B12' B7' -39.0(6) . . . . ?
C2' B11' B12' B8' -1.6(8) . . . . ?
C2' B11' B12' B9' 62.3(8) . . . . ?
C2' B11' B12' B10' 100.0(7) . . . . ?
B3' C1' C2' B6' 140.5(6) . . . . ?
B3' C1' C2' B7' 38.5(6) . . . . ?
B3' C1' C2' B11' 104.8(6) . . . . ?
B3' C1' B4' B5' -140.8(6) . . . . ?
B3' C1' B4' B8' -38.9(5) . . . . ?
B3' C1' B4' B9' -101.4(6) . . . . ?
B3' C1' B5' B4' 37.0(6) . . . . ?
B3' C1' B5' B6' -101.8(6) . . . . ?
B3' C1' B5' B9' -2.5(7) . . . . ?
B3' C1' B5' B10' -64.9(7) . . . . ?
B3' C1' B6' C2' -36.5(5) . . . . ?
B3' C1' B6' B5' 104.8(6) . . . . ?
B3' C1' B6' B10' 65.3(7) . . . . ?
B3' C1' B6' B11' -1.1(7) . . . . ?
B3' C2' B6' C1' 36.5(5) . . . . ?
B3' C2' B6' B5' 1.2(8) . . . . ?
B3' C2' B6' B10' -65.1(7) . . . . ?
B3' C2' B6' B11' -104.2(6) . . . . ?
B3' C2' B7' B8' 38.6(6) . . . . ?
B3' C2' B7' B11' 140.0(6) . . . . ?
B3' C2' B7' B12' 100.4(6) . . . . ?
B3' C2' B11' B6' 101.6(6) . . . . ?
B3' C2' B11' B7' -37.6(6) . . . . ?
B3' C2' B11' B10' 65.1(7) . . . . ?
B3' C2' B11' B12' 2.5(8) . . . . ?
B3' B4' B5' C1' -34.9(5) . . . . ?
B3' B4' B5' B6' 1.1(8) . . . . ?
B3' B4' B5' B9' 100.0(6) . . . . ?
B3' B4' B5' B10' 62.7(7) . . . . ?
B3' B4' B8' B7' -37.4(5) . . . . ?
B3' B4' B8' B9' -137.5(6) . . . . ?
B3' B4' B8' B12' -100.5(6) . . . . ?
B3' B4' B9' B5' -101.1(6) . . . . ?
B3' B4' B9' B8' 37.6(5) . . . . ?
B3' B4' B9' B10' -64.0(7) . . . . ?
B3' B4' B9' B12' -0.3(7) . . . . ?
B3' B7' B8' B4' 37.8(6) . . . . ?
B3' B7' B8' B9' 100.9(6) . . . . ?
B3' B7' B8' B12' 138.2(6) . . . . ?
B3' B7' B11' C2' 35.9(5) . . . . ?
B3' B7' B11' B6' -0.3(7) . . . . ?
B3' B7' B11' B10' -62.2(7) . . . . ?
B3' B7' B11' B12' -99.1(6) . . . . ?
B3' B7' B12' B8' -36.7(5) . . . . ?
B3' B7' B12' B9' 1.5(7) . . . . ?
B3' B7' B12' B10' 65.3(7) . . . . ?
B3' B7' B12' B11' 101.9(6) . . . . ?
B3' B8' B9' B4' -38.0(5) . . . . ?
B3' B8' B9' B5' -0.7(8) . . . . ?
B3' B8' B9' B10' 62.5(7) . . . . ?
B3' B8' B9' B12' 99.9(6) . . . . ?
B3' B8' B12' B7' 36.8(6) . . . . ?
B3' B8' B12' B9' -100.7(6) . . . . ?
B3' B8' B12' B10' -63.3(7) . . . . ?
B3' B8' B12' B11' 0.3(8) . . . . ?
B4' C1' C2' B3' -37.9(5) . . . . ?
B4' C1' C2' B6' 102.6(6) . . . . ?
B4' C1' C2' B7' 0.6(8) . . . . ?
B4' C1' C2' B11' 66.9(7) . . . . ?
B4' C1' B3' C2' 139.2(6) . . . . ?
B4' C1' B3' B7' 103.6(6) . . . . ?
B4' C1' B3' B8' 39.3(5) . . . . ?
B4' C1' B5' B6' -138.8(6) . . . . ?
B4' C1' B5' B9' -39.4(5) . . . . ?
B4' C1' B5' B10' -101.9(6) . . . . ?
B4' C1' B6' C2' -102.8(6) . . . . ?
B4' C1' B6' B5' 38.5(6) . . . . ?
B4' C1' B6' B10' -1.0(8) . . . . ?
B4' C1' B6' B11' -67.4(7) . . . . ?
B4' B3' B7' C2' 97.2(6) . . . . ?
B4' B3' B7' B8' -38.5(5) . . . . ?
B4' B3' B7' B11' 61.5(7) . . . . ?
B4' B3' B7' B12' -1.7(7) . . . . ?
B4' B3' B8' B7' 137.4(6) . . . . ?
B4' B3' B8' B9' 37.9(5) . . . . ?
B4' B3' B8' B12' 100.2(6) . . . . ?
B4' B5' B6' C1' -36.0(5) . . . . ?
B4' B5' B6' C2' -1.4(8) . . . . ?
B4' B5' B6' B10' 101.3(7) . . . . ?
B4' B5' B6' B11' 63.4(7) . . . . ?
B4' B5' B9' B8' -37.1(5) . . . . ?
B4' B5' B9' B10' -138.3(6) . . . . ?
B4' B5' B9' B12' -101.1(7) . . . . ?
B4' B5' B10' B6' -98.8(6) . . . . ?
B4' B5' B10' B9' 37.2(5) . . . . ?
B4' B5' B10' B11' -63.5(7) . . . . ?
B4' B5' B10' B12' 0.2(7) . . . . ?
B4' B8' B9' B5' 37.3(5) . . . . ?
B4' B8' B9' B10' 100.5(6) . . . . ?
B4' B8' B9' B12' 137.9(5) . . . . ?
B4' B8' B12' B7' 100.1(6) . . . . ?
B4' B8' B12' B9' -37.4(5) . . . . ?
B4' B8' B12' B10' 0.0(7) . . . . ?
B4' B8' B12' B11' 63.6(7) . . . . ?
B4' B9' B10' B5' -37.4(6) . . . . ?
B4' B9' B10' B6' 1.3(8) . . . . ?
B4' B9' B10' B11' 63.5(7) . . . . ?
B4' B9' B10' B12' 101.0(7) . . . . ?
B4' B9' B12' B7' -0.8(7) . . . . ?
B4' B9' B12' B8' 37.7(5) . . . . ?
B4' B9' B12' B10' -100.8(6) . . . . ?
B4' B9' B12' B11' -63.3(7) . . . . ?
B5' C1' C2' B3' -105.0(6) . . . . ?
B5' C1' C2' B6' 35.5(5) . . . . ?
B5' C1' C2' B7' -66.5(7) . . . . ?
B5' C1' C2' B11' -0.1(7) . . . . ?
B5' C1' B3' C2' 101.9(6) . . . . ?
B5' C1' B3' B4' -37.3(6) . . . . ?
B5' C1' B3' B7' 66.3(7) . . . . ?
B5' C1' B3' B8' 2.0(7) . . . . ?
B5' C1' B4' B3' 140.8(6) . . . . ?
B5' C1' B4' B8' 101.9(6) . . . . ?
B5' C1' B4' B9' 39.4(6) . . . . ?
B5' C1' B6' C2' -141.3(6) . . . . ?
B5' C1' B6' B10' -39.5(6) . . . . ?
B5' C1' B6' B11' -105.8(6) . . . . ?
B5' B4' B8' B3' 100.6(6) . . . . ?
B5' B4' B8' B7' 63.2(7) . . . . ?
B5' B4' B8' B9' -36.9(5) . . . . ?
B5' B4' B8' B12' 0.1(7) . . . . ?
B5' B4' B9' B8' 138.6(6) . . . . ?
B5' B4' B9' B10' 37.1(6) . . . . ?
B5' B4' B9' B12' 100.8(6) . . . . ?
B5' B6' B10' B9' -39.1(6) . . . . ?
B5' B6' B10' B11' -140.1(6) . . . . ?
B5' B6' B10' B12' -101.5(6) . . . . ?
B5' B6' B11' C2' -100.2(6) . . . . ?
B5' B6' B11' B7' -64.4(7) . . . . ?
B5' B6' B11' B10' 37.7(6) . . . . ?
B5' B6' B11' B12' -0.5(8) . . . . ?
B5' B9' B10' B6' 38.7(6) . . . . ?
B5' B9' B10' B11' 100.9(6) . . . . ?
B5' B9' B10' B12' 138.4(6) . . . . ?
B5' B9' B12' B7' 63.0(7) . . . . ?
B5' B9' B12' B8' 101.5(6) . . . . ?
B5' B9' B12' B10' -37.0(5) . . . . ?
B5' B9' B12' B11' 0.5(8) . . . . ?
B5' B10' B11' C2' 1.6(7) . . . . ?
B5' B10' B11' B6' -35.4(5) . . . . ?
B5' B10' B11' B7' 63.6(7) . . . . ?
B5' B10' B11' B12' 101.0(6) . . . . ?
B5' B10' B12' B7' -64.5(7) . . . . ?
B5' B10' B12' B8' -0.2(7) . . . . ?
B5' B10' B12' B9' 37.4(5) . . . . ?
B5' B10' B12' B11' -100.7(6) . . . . ?
B6' C1' C2' B3' -140.5(6) . . . . ?
B6' C1' C2' B7' -102.0(7) . . . . ?
B6' C1' C2' B11' -35.7(5) . . . . ?
B6' C1' B3' C2' 36.5(5) . . . . ?
B6' C1' B3' B4' -102.7(6) . . . . ?
B6' C1' B3' B7' 0.9(7) . . . . ?
B6' C1' B3' B8' -63.4(6) . . . . ?
B6' C1' B4' B3' 103.2(6) . . . . ?
B6' C1' B4' B5' -37.6(6) . . . . ?
B6' C1' B4' B8' 64.3(7) . . . . ?
B6' C1' B4' B9' 1.7(7) . . . . ?
B6' C1' B5' B4' 138.8(6) . . . . ?
B6' C1' B5' B9' 99.4(6) . . . . ?
B6' C1' B5' B10' 36.9(5) . . . . ?
B6' C2' B3' C1' -36.0(5) . . . . ?
B6' C2' B3' B4' -0.4(7) . . . . ?
B6' C2' B3' B7' 102.6(6) . . . . ?
B6' C2' B3' B8' 62.6(7) . . . . ?
B6' C2' B7' B3' -102.8(6) . . . . ?
B6' C2' B7' B8' -64.2(7) . . . . ?
B6' C2' B7' B11' 37.1(6) . . . . ?
B6' C2' B7' B12' -2.4(7) . . . . ?
B6' C2' B11' B7' -139.2(6) . . . . ?
B6' C2' B11' B10' -36.6(5) . . . . ?
B6' C2' B11' B12' -99.2(6) . . . . ?
B6' B5' B9' B4' 100.3(6) . . . . ?
B6' B5' B9' B8' 63.2(7) . . . . ?
B6' B5' B9' B10' -38.0(6) . . . . ?
B6' B5' B9' B12' -0.8(8) . . . . ?
B6' B5' B10' B9' 136.0(7) . . . . ?
B6' B5' B10' B11' 35.3(5) . . . . ?
B6' B5' B10' B12' 99.0(6) . . . . ?
B6' B10' B11' C2' 37.1(5) . . . . ?
B6' B10' B11' B7' 99.0(6) . . . . ?
B6' B10' B11' B12' 136.4(6) . . . . ?
B6' B10' B12' B7' -2.0(8) . . . . ?
B6' B10' B12' B8' 62.4(7) . . . . ?
B6' B10' B12' B9' 99.9(6) . . . . ?
B6' B10' B12' B11' -38.2(6) . . . . ?
B6' B11' B12' B7' -101.3(6) . . . . ?
B6' B11' B12' B8' -63.9(7) . . . . ?
B6' B11' B12' B9' 0.0(8) . . . . ?
B6' B11' B12' B10' 37.6(6) . . . . ?
B7' C2' B3' C1' -138.6(6) . . . . ?
B7' C2' B3' B4' -103.1(6) . . . . ?
B7' C2' B3' B8' -40.0(6) . . . . ?
B7' C2' B6' C1' 102.8(6) . . . . ?
B7' C2' B6' B5' 67.5(7) . . . . ?
B7' C2' B6' B10' 1.2(8) . . . . ?
B7' C2' B6' B11' -37.8(5) . . . . ?
B7' C2' B11' B6' 139.2(6) . . . . ?
B7' C2' B11' B10' 102.7(6) . . . . ?
B7' C2' B11' B12' 40.1(6) . . . . ?
B7' B3' B4' C1' -96.4(6) . . . . ?
B7' B3' B4' B5' -61.8(7) . . . . ?
B7' B3' B4' B8' 39.1(6) . . . . ?
B7' B3' B4' B9' 1.3(7) . . . . ?
B7' B3' B8' B4' -137.4(6) . . . . ?
B7' B3' B8' B9' -99.5(7) . . . . ?
B7' B3' B8' B12' -37.2(6) . . . . ?
B7' B8' B9' B4' -100.2(6) . . . . ?
B7' B8' B9' B5' -63.0(7) . . . . ?
B7' B8' B9' B10' 0.2(7) . . . . ?
B7' B8' B9' B12' 37.6(5) . . . . ?
B7' B8' B12' B9' -137.6(6) . . . . ?
B7' B8' B12' B10' -100.1(6) . . . . ?
B7' B8' B12' B11' -36.6(6) . . . . ?
B7' B11' B12' B8' 37.4(6) . . . . ?
B7' B11' B12' B9' 101.3(7) . . . . ?
B7' B11' B12' B10' 139.0(6) . . . . ?
B8' B3' B4' C1' -135.5(6) . . . . ?
B8' B3' B4' B5' -100.9(6) . . . . ?
B8' B3' B4' B9' -37.8(5) . . . . ?
B8' B3' B7' C2' 135.6(7) . . . . ?
B8' B3' B7' B11' 99.9(6) . . . . ?
B8' B3' B7' B12' 36.7(5) . . . . ?
B8' B4' B5' C1' -97.8(6) . . . . ?
B8' B4' B5' B6' -61.8(7) . . . . ?
B8' B4' B5' B9' 37.0(5) . . . . ?
B8' B4' B5' B10' -0.2(7) . . . . ?
B8' B4' B9' B5' -138.6(6) . . . . ?
B8' B4' B9' B10' -101.6(7) . . . . ?
B8' B4' B9' B12' -37.9(5) . . . . ?
B8' B7' B11' C2' 98.5(6) . . . . ?
B8' B7' B11' B6' 62.3(7) . . . . ?
B8' B7' B11' B10' 0.4(8) . . . . ?
B8' B7' B11' B12' -36.5(6) . . . . ?
B8' B7' B12' B9' 38.3(5) . . . . ?
B8' B7' B12' B10' 102.1(6) . . . . ?
B8' B7' B12' B11' 138.6(6) . . . . ?
B8' B9' B10' B5' -100.9(6) . . . . ?
B8' B9' B10' B6' -62.3(7) . . . . ?
B8' B9' B10' B11' 0.0(8) . . . . ?
B8' B9' B10' B12' 37.5(5) . . . . ?
B8' B9' B12' B7' -38.4(5) . . . . ?
B8' B9' B12' B10' -138.5(6) . . . . ?
B8' B9' B12' B11' -101.0(6) . . . . ?
B9' B4' B5' C1' -134.9(6) . . . . ?
B9' B4' B5' B6' -98.9(6) . . . . ?
B9' B4' B5' B10' -37.2(5) . . . . ?
B9' B4' B8' B3' 137.5(6) . . . . ?
B9' B4' B8' B7' 100.1(6) . . . . ?
B9' B4' B8' B12' 37.0(5) . . . . ?
B9' B5' B6' C1' -98.6(6) . . . . ?
B9' B5' B6' C2' -64.0(7) . . . . ?
B9' B5' B6' B10' 38.7(6) . . . . ?
B9' B5' B6' B11' 0.8(8) . . . . ?
B9' B5' B10' B6' -136.0(7) . . . . ?
B9' B5' B10' B11' -100.6(7) . . . . ?
B9' B5' B10' B12' -37.0(5) . . . . ?
B9' B8' B12' B7' 137.6(6) . . . . ?
B9' B8' B12' B10' 37.5(5) . . . . ?
B9' B8' B12' B11' 101.0(6) . . . . ?
B9' B10' B11' C2' -62.2(7) . . . . ?
B9' B10' B11' B6' -99.2(6) . . . . ?
B9' B10' B11' B7' -0.2(8) . . . . ?
B9' B10' B11' B12' 37.2(5) . . . . ?
B9' B10' B12' B7' -101.9(6) . . . . ?
B9' B10' B12' B8' -37.5(5) . . . . ?
B9' B10' B12' B11' -138.1(6) . . . . ?
B10' B5' B6' C1' -137.3(6) . . . . ?
B10' B5' B6' C2' -102.7(6) . . . . ?
B10' B5' B6' B11' -37.9(6) . . . . ?
B10' B5' B9' B4' 138.3(6) . . . . ?
B10' B5' B9' B8' 101.2(6) . . . . ?
B10' B5' B9' B12' 37.3(6) . . . . ?
B10' B6' B11' C2' -137.9(6) . . . . ?
B10' B6' B11' B7' -102.2(6) . . . . ?
B10' B6' B11' B12' -38.3(6) . . . . ?
B10' B9' B12' B7' 100.0(6) . . . . ?
B10' B9' B12' B8' 138.5(6) . . . . ?
B10' B9' B12' B11' 37.5(6) . . . . ?
B10' B11' B12' B7' -139.0(6) . . . . ?
B10' B11' B12' B8' -101.6(7) . . . . ?
B10' B11' B12' B9' -37.6(6) . . . . ?
B11' C2' B3' C1' -101.0(7) . . . . ?
B11' C2' B3' B4' -65.4(7) . . . . ?
B11' C2' B3' B7' 37.7(6) . . . . ?
B11' C2' B3' B8' -2.3(8) . . . . ?
B11' C2' B6' C1' 140.7(5) . . . . ?
B11' C2' B6' B5' 105.3(6) . . . . ?
B11' C2' B6' B10' 39.1(5) . . . . ?
B11' C2' B7' B3' -140.0(6) . . . . ?
B11' C2' B7' B8' -101.3(7) . . . . ?
B11' C2' B7' B12' -39.5(5) . . . . ?
B11' B6' B10' B5' 140.1(6) . . . . ?
B11' B6' B10' B9' 101.0(6) . . . . ?
B11' B6' B10' B12' 38.6(6) . . . . ?
B11' B7' B8' B3' -101.3(6) . . . . ?
B11' B7' B8' B4' -63.5(7) . . . . ?
B11' B7' B8' B9' -0.4(7) . . . . ?
B11' B7' B8' B12' 36.9(6) . . . . ?
B11' B7' B12' B8' -138.6(6) . . . . ?
B11' B7' B12' B9' -100.4(6) . . . . ?
B11' B7' B12' B10' -36.6(6) . . . . ?
B11' B10' B12' B7' 36.2(5) . . . . ?
B11' B10' B12' B8' 100.6(6) . . . . ?
B11' B10' B12' B9' 138.1(6) . . . . ?
B12' B7' B8' B3' -138.2(6) . . . . ?
B12' B7' B8' B4' -100.3(6) . . . . ?
B12' B7' B8' B9' -37.3(5) . . . . ?
B12' B7' B11' C2' 135.0(6) . . . . ?
B12' B7' B11' B6' 98.8(6) . . . . ?
B12' B7' B11' B10' 36.9(6) . . . . ?
B12' B8' B9' B4' -137.9(5) . . . . ?
B12' B8' B9' B5' -100.6(6) . . . . ?
B12' B8' B9' B10' -37.4(5) . . . . ?
B12' B9' B10' B5' -138.4(6) . . . . ?
B12' B9' B10' B6' -99.8(6) . . . . ?
B12' B9' B10' B11' -37.5(6) . . . . ?
B12' B10' B11' C2' -99.3(6) . . . . ?
B12' B10' B11' B6' -136.4(6) . . . . ?
B12' B10' B11' B7' -37.4(6) . . . . ?
C107 C106 C105 C104 -0.6(11) . . . . ?
C107 C108 C109 C104 0.0(12) . . . . ?
C106 C107 C108 C109 -0.2(12) . . . . ?
C106 C105 C104 C103 179.9(6) . . . . ?
C106 C105 C104 C109 0.4(10) . . . . ?
C108 C107 C106 C105 0.4(12) . . . . ?
C105 C104 C103 N1 87.7(8) . . . . ?
C105 C104 C109 C108 -0.1(11) . . . . ?
C104 C103 N1 C102 57.7(8) . . . . ?
C104 C103 N1 C101 -63.6(8) . . . . ?
C104 C103 N1 C100 177.5(6) . . . . ?
C103 C104 C109 C108 -179.6(7) . . . . ?
C109 C104 C103 N1 -92.8(8) . . . . ?

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_x82820
_database_code_depnum_ccdc_archive 'CCDC 1042152'
_audit_update_record             
;
2015-01-05 deposited with the CCDC.
2015-02-09 downloaded from the CCDC.
;
_audit_creation_date             2014-06-05
_audit_creation_method           
;
Olex2 1.2
(compiled 2013.12.10 svn.r2850 for OlexSys, GUI svn.r4736)
;
_shelxl_version_number           2013-4
_chemical_name_common            ?
_chemical_name_systematic        
;
 ?
;
_chemical_formula_moiety         'C14 H35 B19 Ru'
_chemical_formula_sum            'C14 H35 B19 Ru'
_chemical_formula_weight         509.88
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   11.5653(7)
_cell_length_b                   14.1222(9)
_cell_length_c                   15.1116(10)
_cell_angle_alpha                90
_cell_angle_beta                 91.611(4)
_cell_angle_gamma                90
_cell_volume                     2467.2(3)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9918
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27.318
_cell_measurement_theta_min      2.188
_shelx_estimated_absorpt_T_max   0.939
_shelx_estimated_absorpt_T_min   0.775
_exptl_absorpt_coefficient_mu    0.640
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.6192
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.0662 before and 0.0513 after correction.
The Ratio of minimum to maximum transmission is 0.8305.
The λ/2 correction factor is Not present.
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.373
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       plate
_exptl_crystal_F_000             1032
_exptl_crystal_size_max          0.42
_exptl_crystal_size_mid          0.38
_exptl_crystal_size_min          0.1
_exptl_special_details           
;
 ?
;
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0431
_diffrn_reflns_av_unetI/netI     0.0371
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.991
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            34686
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.991
_diffrn_reflns_theta_full        25.000
_diffrn_reflns_theta_max         27.468
_diffrn_reflns_theta_min         1.974
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4326
_reflns_number_total             5604
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.60A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         0.681
_refine_diff_density_min         -0.714
_refine_diff_density_rms         0.078
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     373
_refine_ls_number_reflns         5604
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0492
_refine_ls_R_factor_gt           0.0309
_refine_ls_restrained_S_all      1.029
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0310P)²+2.3852P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0689
_refine_ls_wR_factor_ref         0.0766
_refine_special_details          
;
 ?
;
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Ternary CH refined with riding coordinates:
 C31(H31), C32(H32), C34(H34), C35(H35), C37(H37)
2.b Idealised Me refined as rotating group:
 C36(H36A,H36B,H36C), C38(H38A,H38B,H38C), C39(H39A,H39B,H39C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru3 Ru 0.70115(2) 0.19197(2) 0.78645(2) 0.01778(7) Uani 1 1 d . . . . .
C1 C 0.5647(2) 0.13084(17) 0.69172(15) 0.0201(5) Uani 1 1 d . . . . .
C2 C 0.5683(2) 0.24711(19) 0.69209(16) 0.0234(5) Uani 1 1 d . . . . .
H2 H 0.507(2) 0.2789(19) 0.7215(18) 0.028 Uiso 1 1 d R . . . .
B4 B 0.7047(2) 0.0884(2) 0.67690(18) 0.0230(6) Uani 1 1 d . . . . .
H4 H 0.728(2) 0.0181(19) 0.7004(17) 0.028 Uiso 1 1 d R . . . .
B5 B 0.5988(3) 0.0896(2) 0.58732(19) 0.0264(6) Uani 1 1 d . . . . .
H5 H 0.560(2) 0.024(2) 0.5655(18) 0.032 Uiso 1 1 d R . . . .
B6 B 0.5108(3) 0.1908(2) 0.59757(19) 0.0258(6) Uani 1 1 d . . . . .
H6 H 0.422(2) 0.1933(18) 0.5845(18) 0.031 Uiso 1 1 d R . . . .
B7 B 0.7058(3) 0.2938(2) 0.6765(2) 0.0262(6) Uani 1 1 d . . . . .
H7 H 0.722(2) 0.364(2) 0.7004(17) 0.031 Uiso 1 1 d R . . . .
B8 B 0.7981(2) 0.1908(2) 0.66209(19) 0.0256(6) Uani 1 1 d . . . . .
H8 H 0.890(2) 0.1873(18) 0.6651(18) 0.031 Uiso 1 1 d R . . . .
B9 B 0.7412(3) 0.1278(2) 0.5688(2) 0.0293(7) Uani 1 1 d . . . . .
H9 H 0.799(2) 0.083(2) 0.5313(18) 0.035 Uiso 1 1 d R . . . .
B10 B 0.6223(3) 0.1912(2) 0.5213(2) 0.0314(7) Uani 1 1 d . . . . .
H10 H 0.603(2) 0.1903(19) 0.452(2) 0.038 Uiso 1 1 d R . . . .
B11 B 0.5983(3) 0.2914(2) 0.5889(2) 0.0297(7) Uani 1 1 d . . . . .
H11 H 0.556(2) 0.355(2) 0.5677(18) 0.036 Uiso 1 1 d R . . . .
B12 B 0.7416(3) 0.2539(2) 0.5686(2) 0.0321(7) Uani 1 1 d . . . . .
H12 H 0.795(3) 0.293(2) 0.529(2) 0.038 Uiso 1 1 d R . . . .
C30 C 0.6666(2) 0.25951(19) 0.92275(16) 0.0231(5) Uani 1 1 d . . . . .
C31 C 0.6647(2) 0.16083(18) 0.93321(15) 0.0212(5) Uani 1 1 d . . . . .
H31 H 0.5896 0.1301 0.9475 0.025 Uiso 1 1 calc R . . . .
C32 C 0.7558(2) 0.10275(18) 0.90558(16) 0.0230(5) Uani 1 1 d . . . . .
H32 H 0.7436 0.0327 0.9030 0.028 Uiso 1 1 calc R . . . .
C33 C 0.8546(2) 0.14120(19) 0.86751(17) 0.0236(5) Uani 1 1 d . . . . .
C34 C 0.8574(2) 0.24128(19) 0.85711(17) 0.0253(6) Uani 1 1 d . . . . .
H34 H 0.9208 0.2700 0.8224 0.030 Uiso 1 1 calc R . . . .
C35 C 0.7656(2) 0.29942(18) 0.88333(16) 0.0247(5) Uani 1 1 d . . . . .
H35 H 0.7650 0.3679 0.8663 0.030 Uiso 1 1 calc R . . . .
C36 C 0.9518(2) 0.0789(2) 0.83929(19) 0.0324(6) Uani 1 1 d . . . . .
H36A H 0.9950 0.1110 0.7931 0.049 Uiso 1 1 calc GR . . . .
H36B H 0.9204 0.0192 0.8161 0.049 Uiso 1 1 calc GR . . . .
H36C H 1.0037 0.0660 0.8903 0.049 Uiso 1 1 calc GR . . . .
C37 C 0.5703(2) 0.31993(18) 0.95887(17) 0.0266(6) Uani 1 1 d . . . . .
H37 H 0.5026 0.2776 0.9691 0.032 Uiso 1 1 calc R . . . .
C38 C 0.6110(3) 0.3595(2) 1.04838(18) 0.0333(6) Uani 1 1 d . . . . .
H38A H 0.6394 0.3077 1.0862 0.050 Uiso 1 1 calc GR . . . .
H38B H 0.5462 0.3911 1.0767 0.050 Uiso 1 1 calc GR . . . .
H38C H 0.6734 0.4053 1.0397 0.050 Uiso 1 1 calc GR . . . .
C39 C 0.5300(2) 0.3988(2) 0.89658(18) 0.0326(6) Uani 1 1 d . . . . .
H39A H 0.4677 0.4345 0.9238 0.049 Uiso 1 1 calc GR . . . .
H39B H 0.5015 0.3712 0.8406 0.049 Uiso 1 1 calc GR . . . .
H39C H 0.5949 0.4413 0.8853 0.049 Uiso 1 1 calc GR . . . .
C1' C 0.4656(2) 0.07657(17) 0.73583(16) 0.0212(5) Uani 1 1 d . . . . .
C2' C 0.4947(2) 0.0140(2) 0.82762(18) 0.0301(6) Uani 1 1 d . . . . .
H2' H 0.582(2) 0.013(2) 0.8497(19) 0.036 Uiso 1 1 d R . . . .
B3' B 0.4130(2) 0.1167(2) 0.83406(19) 0.0222(6) Uani 1 1 d . . . . .
H3' H 0.446(2) 0.1785(19) 0.8592(18) 0.027 Uiso 1 1 d R . . . .
B4' B 0.3255(2) 0.1198(2) 0.73769(19) 0.0244(6) Uani 1 1 d . . . . .
H4' H 0.309(2) 0.1848(19) 0.7062(17) 0.029 Uiso 1 1 d R . . . .
B5' B 0.3585(3) 0.0191(2) 0.6766(2) 0.0262(6) Uani 1 1 d . . . . .
H5' H 0.361(2) 0.028(2) 0.6198(19) 0.031 Uiso 1 1 d R . . . .
B6' B 0.4672(3) -0.0465(2) 0.7298(2) 0.0297(7) Uani 1 1 d . . . . .
H6' H 0.539(2) -0.078(2) 0.6966(18) 0.036 Uiso 1 1 d R . . . .
B7' B 0.3777(3) 0.0150(2) 0.8962(2) 0.0283(7) Uani 1 1 d . . . . .
H7' H 0.392(2) 0.016(2) 0.9667(19) 0.034 Uiso 1 1 d R . . . .
B8' B 0.2683(2) 0.0804(2) 0.83872(19) 0.0249(6) Uani 1 1 d . . . . .
H8' H 0.211(2) 0.1255(19) 0.8705(17) 0.030 Uiso 1 1 d R . . . .
B9' B 0.2341(3) 0.0189(3) 0.7389(2) 0.0313(7) Uani 1 1 d . . . . .
H9' H 0.151(2) 0.028(2) 0.7035(19) 0.038 Uiso 1 1 d R . . . .
B10' B 0.3222(3) -0.0838(3) 0.7338(2) 0.0387(8) Uani 1 1 d . . . . .
H10' H 0.294(3) -0.143(2) 0.693(2) 0.046 Uiso 1 1 d R . . . .
B11' B 0.4103(3) -0.0867(2) 0.8311(2) 0.0362(8) Uani 1 1 d . . . . .
H11' H 0.445(3) -0.146(2) 0.863(2) 0.043 Uiso 1 1 d R . . . .
B12' B 0.2660(3) -0.0460(2) 0.8369(2) 0.0342(7) Uani 1 1 d . . . . .
H12' H 0.198(2) -0.084(2) 0.8693(19) 0.041 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru3 C1 2.271(2) . ?
Ru3 C2 2.208(3) . ?
Ru3 B4 2.210(3) . ?
Ru3 B7 2.200(3) . ?
Ru3 B8 2.215(3) . ?
Ru3 C30 2.315(2) . ?
Ru3 C31 2.311(2) . ?
Ru3 C32 2.272(2) . ?
Ru3 C33 2.246(2) . ?
Ru3 C34 2.187(2) . ?
Ru3 C35 2.223(2) . ?
C1 C2 1.643(3) . ?
C1 B4 1.747(4) . ?
C1 B5 1.737(4) . ?
C1 B6 1.755(4) . ?
C1 C1' 1.545(3) . ?
C2 H2 0.96(3) . ?
C2 B6 1.749(4) . ?
C2 B7 1.743(4) . ?
C2 B11 1.725(4) . ?
B4 H4 1.09(3) . ?
B4 B5 1.800(4) . ?
B4 B8 1.821(4) . ?
B4 B9 1.788(4) . ?
B5 H5 1.08(3) . ?
B5 B6 1.764(4) . ?
B5 B9 1.763(4) . ?
B5 B10 1.773(5) . ?
B6 H6 1.04(3) . ?
B6 B10 1.753(4) . ?
B6 B11 1.751(4) . ?
B7 H7 1.07(3) . ?
B7 B8 1.821(4) . ?
B7 B11 1.790(4) . ?
B7 B12 1.785(4) . ?
B8 H8 1.06(3) . ?
B8 B9 1.777(4) . ?
B8 B12 1.779(4) . ?
B9 H9 1.08(3) . ?
B9 B10 1.775(5) . ?
B9 B12 1.780(5) . ?
B10 H10 1.07(3) . ?
B10 B11 1.771(5) . ?
B10 B12 1.773(5) . ?
B11 H11 1.07(3) . ?
B11 B12 1.775(5) . ?
B12 H12 1.03(3) . ?
C30 C31 1.403(4) . ?
C30 C35 1.422(4) . ?
C30 C37 1.517(3) . ?
C31 H31 1.0000 . ?
C31 C32 1.407(3) . ?
C32 H32 1.0000 . ?
C32 C33 1.404(3) . ?
C33 C34 1.422(4) . ?
C33 C36 1.499(3) . ?
C34 H34 1.0000 . ?
C34 C35 1.408(4) . ?
C35 H35 1.0000 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 H37 1.0000 . ?
C37 C38 1.526(4) . ?
C37 C39 1.522(4) . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 H38C 0.9800 . ?
C39 H39A 0.9800 . ?
C39 H39B 0.9800 . ?
C39 H39C 0.9800 . ?
C1' C2' 1.671(4) . ?
C1' B3' 1.716(4) . ?
C1' B4' 1.733(4) . ?
C1' B5' 1.712(4) . ?
C1' B6' 1.741(4) . ?
C2' H2' 1.05(3) . ?
C2' B3' 1.735(4) . ?
C2' B6' 1.729(4) . ?
C2' B7' 1.727(4) . ?
C2' B11' 1.726(4) . ?
B3' H3' 1.02(3) . ?
B3' B4' 1.751(4) . ?
B3' B7' 1.770(4) . ?
B3' B8' 1.754(4) . ?
B4' H4' 1.05(3) . ?
B4' B5' 1.744(4) . ?
B4' B8' 1.771(4) . ?
B4' B9' 1.775(4) . ?
B5' H5' 0.87(3) . ?
B5' B6' 1.741(5) . ?
B5' B9' 1.742(4) . ?
B5' B10' 1.748(5) . ?
B6' H6' 1.07(3) . ?
B6' B10' 1.761(5) . ?
B6' B11' 1.775(4) . ?
B7' H7' 1.07(3) . ?
B7' B8' 1.775(4) . ?
B7' B11' 1.787(4) . ?
B7' B12' 1.775(5) . ?
B8' H8' 1.05(3) . ?
B8' B9' 1.775(4) . ?
B8' B12' 1.785(5) . ?
B9' H9' 1.09(3) . ?
B9' B10' 1.775(5) . ?
B9' B12' 1.771(5) . ?
B10' H10' 1.08(3) . ?
B10' B11' 1.766(5) . ?
B10' B12' 1.786(4) . ?
B11' H11' 1.04(3) . ?
B11' B12' 1.770(5) . ?
B12' H12' 1.08(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Ru3 C30 125.67(8) . . ?
C1 Ru3 C31 112.97(9) . . ?
C1 Ru3 C32 117.47(9) . . ?
C2 Ru3 C1 42.99(9) . . ?
C2 Ru3 B4 77.11(10) . . ?
C2 Ru3 B8 79.31(10) . . ?
C2 Ru3 C30 107.15(9) . . ?
C2 Ru3 C31 122.98(9) . . ?
C2 Ru3 C32 151.63(9) . . ?
C2 Ru3 C33 171.76(9) . . ?
C2 Ru3 C35 113.51(10) . . ?
B4 Ru3 C1 45.87(9) . . ?
B4 Ru3 B8 48.61(11) . . ?
B4 Ru3 C30 161.18(10) . . ?
B4 Ru3 C31 126.92(10) . . ?
B4 Ru3 C32 102.48(10) . . ?
B4 Ru3 C33 99.57(10) . . ?
B4 Ru3 C35 158.77(10) . . ?
B7 Ru3 C1 78.66(10) . . ?
B7 Ru3 C2 46.59(10) . . ?
B7 Ru3 B4 82.24(11) . . ?
B7 Ru3 B8 48.73(11) . . ?
B7 Ru3 C30 114.30(11) . . ?
B7 Ru3 C31 149.15(10) . . ?
B7 Ru3 C32 161.63(10) . . ?
B7 Ru3 C33 125.83(10) . . ?
B7 Ru3 C35 92.11(11) . . ?
B8 Ru3 C1 79.73(10) . . ?
B8 Ru3 C30 149.56(10) . . ?
B8 Ru3 C31 157.34(10) . . ?
B8 Ru3 C32 122.13(10) . . ?
B8 Ru3 C33 92.82(10) . . ?
B8 Ru3 C35 113.31(11) . . ?
C31 Ru3 C30 35.30(9) . . ?
C32 Ru3 C30 64.82(9) . . ?
C32 Ru3 C31 35.74(9) . . ?
C33 Ru3 C1 138.33(9) . . ?
C33 Ru3 C30 78.45(9) . . ?
C33 Ru3 C31 65.06(9) . . ?
C33 Ru3 C32 36.19(9) . . ?
C34 Ru3 C1 168.19(9) . . ?
C34 Ru3 C2 138.89(10) . . ?
C34 Ru3 B4 122.94(10) . . ?
C34 Ru3 B7 97.10(11) . . ?
C34 Ru3 B8 89.17(11) . . ?
C34 Ru3 C30 66.13(9) . . ?
C34 Ru3 C31 76.26(9) . . ?
C34 Ru3 C32 65.31(9) . . ?
C34 Ru3 C33 37.41(9) . . ?
C34 Ru3 C35 37.24(9) . . ?
C35 Ru3 C1 152.73(9) . . ?
C35 Ru3 C30 36.45(9) . . ?
C35 Ru3 C31 64.19(9) . . ?
C35 Ru3 C32 77.06(10) . . ?
C35 Ru3 C33 67.26(9) . . ?
C2 C1 Ru3 66.47(12) . . ?
C2 C1 B4 108.63(19) . . ?
C2 C1 B5 109.38(19) . . ?
C2 C1 B6 61.88(16) . . ?
B4 C1 Ru3 65.21(12) . . ?
B4 C1 B6 111.76(18) . . ?
B5 C1 Ru3 121.90(16) . . ?
B5 C1 B4 62.22(16) . . ?
B5 C1 B6 60.66(16) . . ?
B6 C1 Ru3 123.51(16) . . ?
C1' C1 Ru3 115.29(15) . . ?
C1' C1 C2 120.9(2) . . ?
C1' C1 B4 125.9(2) . . ?
C1' C1 B5 114.5(2) . . ?
C1' C1 B6 109.78(19) . . ?
Ru3 C2 H2 112.0(16) . . ?
C1 C2 Ru3 70.54(12) . . ?
C1 C2 H2 116.9(16) . . ?
C1 C2 B6 62.22(16) . . ?
C1 C2 B7 113.6(2) . . ?
C1 C2 B11 111.4(2) . . ?
B6 C2 Ru3 127.48(17) . . ?
B6 C2 H2 108.9(16) . . ?
B7 C2 Ru3 66.44(13) . . ?
B7 C2 H2 125.0(17) . . ?
B7 C2 B6 112.8(2) . . ?
B11 C2 Ru3 123.89(17) . . ?
B11 C2 H2 114.8(16) . . ?
B11 C2 B6 60.51(17) . . ?
B11 C2 B7 62.15(17) . . ?
Ru3 B4 H4 111.7(14) . . ?
C1 B4 Ru3 68.92(12) . . ?
C1 B4 H4 119.5(14) . . ?
C1 B4 B5 58.63(15) . . ?
C1 B4 B8 107.4(2) . . ?
C1 B4 B9 104.7(2) . . ?
B5 B4 Ru3 122.05(17) . . ?
B5 B4 H4 114.2(14) . . ?
B5 B4 B8 107.1(2) . . ?
B8 B4 Ru3 65.85(13) . . ?
B8 B4 H4 128.6(14) . . ?
B9 B4 Ru3 119.26(19) . . ?
B9 B4 H4 121.4(14) . . ?
B9 B4 B5 58.87(17) . . ?
B9 B4 B8 59.00(17) . . ?
C1 B5 B4 59.15(15) . . ?
C1 B5 H5 117.5(14) . . ?
C1 B5 B6 60.16(15) . . ?
C1 B5 B9 106.2(2) . . ?
C1 B5 B10 106.4(2) . . ?
B4 B5 H5 119.4(15) . . ?
B6 B5 B4 108.9(2) . . ?
B6 B5 H5 119.2(14) . . ?
B6 B5 B10 59.44(17) . . ?
B9 B5 B4 60.20(16) . . ?
B9 B5 H5 126.7(14) . . ?
B9 B5 B6 108.0(2) . . ?
B9 B5 B10 60.27(18) . . ?
B10 B5 B4 108.6(2) . . ?
B10 B5 H5 126.5(15) . . ?
C1 B6 B5 59.18(15) . . ?
C1 B6 H6 119.7(15) . . ?
C2 B6 C1 55.90(14) . . ?
C2 B6 B5 103.5(2) . . ?
C2 B6 H6 119.3(15) . . ?
C2 B6 B10 105.4(2) . . ?
C2 B6 B11 59.05(16) . . ?
B5 B6 H6 125.4(15) . . ?
B10 B6 C1 106.5(2) . . ?
B10 B6 B5 60.54(18) . . ?
B10 B6 H6 128.0(16) . . ?
B11 B6 C1 105.0(2) . . ?
B11 B6 B5 108.3(2) . . ?
B11 B6 H6 121.9(15) . . ?
B11 B6 B10 60.70(18) . . ?
Ru3 B7 H7 111.1(14) . . ?
C2 B7 Ru3 66.97(12) . . ?
C2 B7 H7 116.9(14) . . ?
C2 B7 B8 104.7(2) . . ?
C2 B7 B11 58.42(16) . . ?
C2 B7 B12 103.9(2) . . ?
B8 B7 Ru3 66.09(13) . . ?
B8 B7 H7 133.4(15) . . ?
B11 B7 Ru3 121.01(18) . . ?
B11 B7 H7 112.0(15) . . ?
B11 B7 B8 107.1(2) . . ?
B12 B7 Ru3 119.67(19) . . ?
B12 B7 H7 124.0(14) . . ?
B12 B7 B8 59.12(17) . . ?
B12 B7 B11 59.54(18) . . ?
Ru3 B8 H8 119.5(15) . . ?
B4 B8 Ru3 65.54(12) . . ?
B4 B8 H8 123.6(14) . . ?
B7 B8 Ru3 65.19(13) . . ?
B7 B8 B4 105.51(19) . . ?
B7 B8 H8 128.3(14) . . ?
B9 B8 Ru3 119.47(18) . . ?
B9 B8 B4 59.55(17) . . ?
B9 B8 B7 106.8(2) . . ?
B9 B8 H8 111.0(15) . . ?
B9 B8 B12 60.06(18) . . ?
B12 B8 Ru3 119.13(18) . . ?
B12 B8 B4 106.8(2) . . ?
B12 B8 B7 59.42(17) . . ?
B12 B8 H8 113.7(15) . . ?
B4 B9 H9 117.5(15) . . ?
B5 B9 B4 60.93(17) . . ?
B5 B9 B8 110.7(2) . . ?
B5 B9 H9 119.6(15) . . ?
B5 B9 B10 60.13(18) . . ?
B5 B9 B12 108.0(2) . . ?
B8 B9 B4 61.45(16) . . ?
B8 B9 H9 119.0(15) . . ?
B8 B9 B12 60.03(18) . . ?
B10 B9 B4 109.0(2) . . ?
B10 B9 B8 109.5(2) . . ?
B10 B9 H9 124.0(15) . . ?
B10 B9 B12 59.81(19) . . ?
B12 B9 B4 108.3(2) . . ?
B12 B9 H9 125.1(15) . . ?
B5 B10 B9 59.60(18) . . ?
B5 B10 H10 120.7(15) . . ?
B6 B10 B5 60.02(17) . . ?
B6 B10 B9 108.0(2) . . ?
B6 B10 H10 120.4(16) . . ?
B6 B10 B11 59.57(18) . . ?
B6 B10 B12 108.4(2) . . ?
B9 B10 H10 122.1(16) . . ?
B11 B10 B5 107.0(2) . . ?
B11 B10 B9 107.6(2) . . ?
B11 B10 H10 123.0(15) . . ?
B11 B10 B12 60.13(19) . . ?
B12 B10 B5 107.9(2) . . ?
B12 B10 B9 60.22(19) . . ?
B12 B10 H10 122.9(16) . . ?
C2 B11 B6 60.44(16) . . ?
C2 B11 B7 59.43(16) . . ?
C2 B11 B10 105.7(2) . . ?
C2 B11 H11 118.3(15) . . ?
C2 B11 B12 105.1(2) . . ?
B6 B11 B7 110.5(2) . . ?
B6 B11 B10 59.73(18) . . ?
B6 B11 H11 116.5(15) . . ?
B6 B11 B12 108.4(2) . . ?
B7 B11 H11 120.4(15) . . ?
B10 B11 B7 108.9(2) . . ?
B10 B11 H11 125.3(15) . . ?
B10 B11 B12 59.99(19) . . ?
B12 B11 B7 60.08(18) . . ?
B12 B11 H11 128.4(15) . . ?
B7 B12 H12 121.1(16) . . ?
B8 B12 B7 61.46(17) . . ?
B8 B12 H12 121.4(17) . . ?
B9 B12 B7 108.3(2) . . ?
B9 B12 B8 59.92(18) . . ?
B9 B12 H12 122.8(16) . . ?
B10 B12 B7 109.1(2) . . ?
B10 B12 B8 109.5(2) . . ?
B10 B12 B9 59.97(19) . . ?
B10 B12 B11 59.88(18) . . ?
B10 B12 H12 120.2(17) . . ?
B11 B12 B7 60.38(17) . . ?
B11 B12 B8 109.6(2) . . ?
B11 B12 B9 107.2(2) . . ?
B11 B12 H12 120.8(16) . . ?
C31 C30 Ru3 72.21(14) . . ?
C31 C30 C35 117.1(2) . . ?
C31 C30 C37 120.3(2) . . ?
C35 C30 Ru3 68.24(13) . . ?
C35 C30 C37 122.4(2) . . ?
C37 C30 Ru3 134.34(17) . . ?
Ru3 C31 H31 118.2 . . ?
C30 C31 Ru3 72.48(14) . . ?
C30 C31 H31 118.2 . . ?
C30 C31 C32 122.1(2) . . ?
C32 C31 Ru3 70.62(13) . . ?
C32 C31 H31 118.2 . . ?
Ru3 C32 H32 118.8 . . ?
C31 C32 Ru3 73.64(14) . . ?
C31 C32 H32 118.8 . . ?
C33 C32 Ru3 70.86(14) . . ?
C33 C32 C31 121.4(2) . . ?
C33 C32 H32 118.8 . . ?
C32 C33 Ru3 72.94(13) . . ?
C32 C33 C34 116.8(2) . . ?
C32 C33 C36 121.1(2) . . ?
C34 C33 Ru3 69.06(14) . . ?
C34 C33 C36 122.1(2) . . ?
C36 C33 Ru3 128.31(18) . . ?
Ru3 C34 H34 118.7 . . ?
C33 C34 Ru3 73.53(14) . . ?
C33 C34 H34 118.7 . . ?
C35 C34 Ru3 72.75(14) . . ?
C35 C34 C33 121.9(2) . . ?
C35 C34 H34 118.7 . . ?
Ru3 C35 H35 119.4 . . ?
C30 C35 Ru3 75.31(14) . . ?
C30 C35 H35 119.4 . . ?
C34 C35 Ru3 70.01(14) . . ?
C34 C35 C30 120.6(2) . . ?
C34 C35 H35 119.4 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36B 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C30 C37 H37 107.8 . . ?
C30 C37 C38 108.3(2) . . ?
C30 C37 C39 113.8(2) . . ?
C38 C37 H37 107.8 . . ?
C39 C37 H37 107.8 . . ?
C39 C37 C38 111.2(2) . . ?
C37 C38 H38A 109.5 . . ?
C37 C38 H38B 109.5 . . ?
C37 C38 H38C 109.5 . . ?
H38A C38 H38B 109.5 . . ?
H38A C38 H38C 109.5 . . ?
H38B C38 H38C 109.5 . . ?
C37 C39 H39A 109.5 . . ?
C37 C39 H39B 109.5 . . ?
C37 C39 H39C 109.5 . . ?
H39A C39 H39B 109.5 . . ?
H39A C39 H39C 109.5 . . ?
H39B C39 H39C 109.5 . . ?
C1 C1' C2' 119.09(19) . . ?
C1 C1' B3' 119.6(2) . . ?
C1 C1' B4' 122.5(2) . . ?
C1 C1' B5' 122.9(2) . . ?
C1 C1' B6' 117.6(2) . . ?
C2' C1' B3' 61.61(16) . . ?
C2' C1' B4' 109.83(19) . . ?
C2' C1' B5' 108.0(2) . . ?
C2' C1' B6' 60.84(17) . . ?
B3' C1' B4' 61.00(15) . . ?
B3' C1' B6' 112.3(2) . . ?
B4' C1' B6' 111.4(2) . . ?
B5' C1' B3' 109.90(19) . . ?
B5' C1' B4' 60.83(16) . . ?
B5' C1' B6' 60.53(17) . . ?
C1' C2' H2' 116.1(16) . . ?
C1' C2' B3' 60.47(16) . . ?
C1' C2' B6' 61.58(16) . . ?
C1' C2' B7' 110.6(2) . . ?
C1' C2' B11' 111.1(2) . . ?
B3' C2' H2' 120.8(16) . . ?
B6' C2' H2' 114.5(16) . . ?
B6' C2' B3' 112.0(2) . . ?
B7' C2' H2' 124.7(16) . . ?
B7' C2' B3' 61.52(17) . . ?
B7' C2' B6' 112.9(2) . . ?
B11' C2' H2' 120.9(16) . . ?
B11' C2' B3' 112.2(2) . . ?
B11' C2' B6' 61.85(18) . . ?
B11' C2' B7' 62.34(17) . . ?
C1' B3' C2' 57.91(15) . . ?
C1' B3' H3' 117.8(15) . . ?
C1' B3' B4' 59.97(15) . . ?
C1' B3' B7' 106.5(2) . . ?
C1' B3' B8' 107.5(2) . . ?
C2' B3' H3' 122.4(15) . . ?
C2' B3' B4' 106.1(2) . . ?
C2' B3' B7' 59.01(17) . . ?
C2' B3' B8' 106.2(2) . . ?
B4' B3' H3' 119.4(15) . . ?
B4' B3' B7' 109.0(2) . . ?
B4' B3' B8' 60.69(16) . . ?
B7' B3' H3' 125.8(15) . . ?
B8' B3' H3' 125.6(15) . . ?
B8' B3' B7' 60.46(17) . . ?
C1' B4' B3' 59.03(15) . . ?
C1' B4' H4' 117.5(15) . . ?
C1' B4' B5' 59.00(16) . . ?
C1' B4' B8' 106.0(2) . . ?
C1' B4' B9' 105.9(2) . . ?
B3' B4' H4' 119.6(15) . . ?
B3' B4' B8' 59.76(16) . . ?
B3' B4' B9' 107.6(2) . . ?
B5' B4' B3' 106.9(2) . . ?
B5' B4' H4' 120.9(15) . . ?
B5' B4' B8' 107.0(2) . . ?
B5' B4' B9' 59.35(17) . . ?
B8' B4' H4' 126.6(15) . . ?
B8' B4' B9' 60.10(17) . . ?
B9' B4' H4' 127.2(15) . . ?
C1' B5' B4' 60.16(16) . . ?
C1' B5' H5' 114.0(19) . . ?
C1' B5' B6' 60.54(16) . . ?
C1' B5' B9' 108.3(2) . . ?
C1' B5' B10' 108.4(2) . . ?
B4' B5' H5' 114.6(19) . . ?
B4' B5' B10' 110.9(2) . . ?
B6' B5' B4' 110.8(2) . . ?
B6' B5' H5' 119.7(19) . . ?
B6' B5' B9' 110.2(2) . . ?
B6' B5' B10' 60.6(2) . . ?
B9' B5' B4' 61.20(18) . . ?
B9' B5' H5' 125.5(19) . . ?
B9' B5' B10' 61.1(2) . . ?
B10' B5' H5' 128.6(19) . . ?
C1' B6' B5' 58.92(16) . . ?
C1' B6' H6' 116.3(15) . . ?
C1' B6' B10' 106.6(2) . . ?
C1' B6' B11' 105.7(2) . . ?
C2' B6' C1' 57.58(15) . . ?
C2' B6' B5' 104.2(2) . . ?
C2' B6' H6' 118.5(15) . . ?
C2' B6' B10' 105.7(2) . . ?
C2' B6' B11' 59.01(18) . . ?
B5' B6' H6' 123.9(15) . . ?
B5' B6' B10' 59.9(2) . . ?
B5' B6' B11' 106.8(2) . . ?
B10' B6' H6' 129.8(15) . . ?
B10' B6' B11' 59.9(2) . . ?
B11' B6' H6' 125.5(15) . . ?
C2' B7' B3' 59.47(16) . . ?
C2' B7' H7' 119.6(15) . . ?
C2' B7' B8' 105.7(2) . . ?
C2' B7' B11' 58.81(17) . . ?
C2' B7' B12' 105.3(2) . . ?
B3' B7' H7' 119.1(15) . . ?
B3' B7' B8' 59.32(17) . . ?
B3' B7' B11' 107.7(2) . . ?
B3' B7' B12' 107.5(2) . . ?
B8' B7' H7' 124.6(15) . . ?
B8' B7' B11' 107.9(2) . . ?
B11' B7' H7' 121.7(15) . . ?
B12' B7' H7' 126.6(15) . . ?
B12' B7' B8' 60.40(18) . . ?
B12' B7' B11' 59.6(2) . . ?
B3' B8' B4' 59.55(16) . . ?
B3' B8' B7' 60.22(17) . . ?
B3' B8' H8' 117.5(15) . . ?
B3' B8' B9' 107.4(2) . . ?
B3' B8' B12' 107.8(2) . . ?
B4' B8' B7' 107.9(2) . . ?
B4' B8' H8' 117.5(15) . . ?
B4' B8' B9' 60.06(17) . . ?
B4' B8' B12' 107.8(2) . . ?
B7' B8' H8' 123.2(15) . . ?
B7' B8' B9' 107.4(2) . . ?
B7' B8' B12' 59.79(19) . . ?
B9' B8' H8' 123.8(15) . . ?
B9' B8' B12' 59.65(19) . . ?
B12' B8' H8' 127.3(15) . . ?
B4' B9' B8' 59.84(17) . . ?
B4' B9' H9' 114.5(15) . . ?
B5' B9' B4' 59.45(17) . . ?
B5' B9' B8' 106.9(2) . . ?
B5' B9' H9' 117.4(15) . . ?
B5' B9' B10' 59.60(18) . . ?
B5' B9' B12' 107.3(2) . . ?
B8' B9' H9' 122.1(15) . . ?
B10' B9' B4' 108.2(2) . . ?
B10' B9' B8' 108.8(2) . . ?
B10' B9' H9' 124.9(15) . . ?
B12' B9' B4' 108.3(2) . . ?
B12' B9' B8' 60.46(18) . . ?
B12' B9' H9' 129.2(15) . . ?
B12' B9' B10' 60.49(19) . . ?
B5' B10' B6' 59.48(18) . . ?
B5' B10' B9' 59.27(19) . . ?
B5' B10' H10' 115.2(17) . . ?
B5' B10' B11' 106.9(2) . . ?
B5' B10' B12' 106.4(2) . . ?
B6' B10' B9' 107.8(2) . . ?
B6' B10' H10' 118.9(16) . . ?
B6' B10' B11' 60.45(19) . . ?
B6' B10' B12' 108.1(2) . . ?
B9' B10' H10' 119.1(17) . . ?
B9' B10' B12' 59.64(19) . . ?
B11' B10' B9' 107.6(2) . . ?
B11' B10' H10' 128.2(17) . . ?
B11' B10' B12' 59.8(2) . . ?
B12' B10' H10' 128.2(16) . . ?
C2' B11' B6' 59.14(17) . . ?
C2' B11' B7' 58.85(17) . . ?
C2' B11' B10' 105.6(2) . . ?
C2' B11' H11' 118.1(17) . . ?
C2' B11' B12' 105.5(2) . . ?
B6' B11' B7' 107.8(2) . . ?
B6' B11' H11' 120.5(17) . . ?
B7' B11' H11' 118.7(17) . . ?
B10' B11' B6' 59.63(19) . . ?
B10' B11' B7' 108.3(2) . . ?
B10' B11' H11' 127.3(17) . . ?
B10' B11' B12' 60.7(2) . . ?
B12' B11' B6' 108.1(3) . . ?
B12' B11' B7' 59.84(18) . . ?
B12' B11' H11' 126.1(17) . . ?
B7' B12' B8' 59.81(17) . . ?
B7' B12' B10' 107.9(2) . . ?
B7' B12' H12' 122.8(15) . . ?
B8' B12' B10' 107.9(2) . . ?
B8' B12' H12' 120.3(16) . . ?
B9' B12' B7' 107.6(2) . . ?
B9' B12' B8' 59.89(18) . . ?
B9' B12' B10' 59.9(2) . . ?
B9' B12' H12' 120.0(15) . . ?
B10' B12' H12' 122.0(16) . . ?
B11' B12' B7' 60.55(19) . . ?
B11' B12' B8' 108.2(2) . . ?
B11' B12' B9' 107.5(2) . . ?
B11' B12' B10' 59.5(2) . . ?
B11' B12' H12' 123.8(16) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ru3 C1 C2 B6 156.27(15) . . . . ?
Ru3 C1 C2 B7 51.88(17) . . . . ?
Ru3 C1 C2 B11 119.79(19) . . . . ?
Ru3 C1 B4 B5 -154.30(17) . . . . ?
Ru3 C1 B4 B8 -54.54(15) . . . . ?
Ru3 C1 B4 B9 -116.12(19) . . . . ?
Ru3 C1 B5 B4 27.63(18) . . . . ?
Ru3 C1 B5 B6 -113.3(2) . . . . ?
Ru3 C1 B5 B9 -11.5(3) . . . . ?
Ru3 C1 B5 B10 -74.5(2) . . . . ?
Ru3 C1 B6 C2 -26.26(17) . . . . ?
Ru3 C1 B6 B5 110.8(2) . . . . ?
Ru3 C1 B6 B10 71.5(2) . . . . ?
Ru3 C1 B6 B11 8.1(3) . . . . ?
Ru3 C1 C1' C2' -34.7(3) . . . . ?
Ru3 C1 C1' B3' 37.3(3) . . . . ?
Ru3 C1 C1' B4' 109.9(2) . . . . ?
Ru3 C1 C1' B5' -176.09(18) . . . . ?
Ru3 C1 C1' B6' -104.9(2) . . . . ?
Ru3 C2 B6 C1 28.56(18) . . . . ?
Ru3 C2 B6 B5 -8.4(3) . . . . ?
Ru3 C2 B6 B10 -71.1(3) . . . . ?
Ru3 C2 B6 B11 -111.9(2) . . . . ?
Ru3 C2 B7 B8 55.45(15) . . . . ?
Ru3 C2 B7 B11 156.70(18) . . . . ?
Ru3 C2 B7 B12 116.66(19) . . . . ?
Ru3 C2 B11 B6 117.5(2) . . . . ?
Ru3 C2 B11 B7 -25.9(2) . . . . ?
Ru3 C2 B11 B10 77.1(3) . . . . ?
Ru3 C2 B11 B12 14.7(3) . . . . ?
Ru3 B4 B5 C1 -28.51(18) . . . . ?
Ru3 B4 B5 B6 6.7(3) . . . . ?
Ru3 B4 B5 B9 107.2(2) . . . . ?
Ru3 B4 B5 B10 69.9(2) . . . . ?
Ru3 B4 B8 B7 -52.79(15) . . . . ?
Ru3 B4 B8 B9 -153.42(18) . . . . ?
Ru3 B4 B8 B12 -114.91(19) . . . . ?
Ru3 B4 B9 B5 -111.8(2) . . . . ?
Ru3 B4 B9 B8 27.90(18) . . . . ?
Ru3 B4 B9 B10 -74.5(3) . . . . ?
Ru3 B4 B9 B12 -11.0(3) . . . . ?
Ru3 B7 B8 B4 53.00(15) . . . . ?
Ru3 B7 B8 B9 115.25(18) . . . . ?
Ru3 B7 B8 B12 153.65(19) . . . . ?
Ru3 B7 B11 C2 25.13(19) . . . . ?
Ru3 B7 B11 B6 -8.5(3) . . . . ?
Ru3 B7 B11 B10 -72.3(3) . . . . ?
Ru3 B7 B11 B12 -108.4(2) . . . . ?
Ru3 B7 B12 B8 -27.8(2) . . . . ?
Ru3 B7 B12 B9 10.9(3) . . . . ?
Ru3 B7 B12 B10 74.5(3) . . . . ?
Ru3 B7 B12 B11 110.7(2) . . . . ?
Ru3 B8 B9 B4 -27.89(19) . . . . ?
Ru3 B8 B9 B5 9.3(3) . . . . ?
Ru3 B8 B9 B10 73.7(3) . . . . ?
Ru3 B8 B9 B12 108.6(2) . . . . ?
Ru3 B8 B12 B7 27.5(2) . . . . ?
Ru3 B8 B12 B9 -109.2(2) . . . . ?
Ru3 B8 B12 B10 -74.2(3) . . . . ?
Ru3 B8 B12 B11 -10.2(3) . . . . ?
Ru3 C30 C31 C32 52.5(2) . . . . ?
Ru3 C30 C35 C34 -55.5(2) . . . . ?
Ru3 C30 C37 C38 -167.8(2) . . . . ?
Ru3 C30 C37 C39 -43.6(3) . . . . ?
Ru3 C31 C32 C33 54.6(2) . . . . ?
Ru3 C32 C33 C34 55.0(2) . . . . ?
Ru3 C32 C33 C36 -124.9(2) . . . . ?
Ru3 C33 C34 C35 56.8(2) . . . . ?
Ru3 C34 C35 C30 58.1(2) . . . . ?
C1 C2 B6 B5 -37.00(18) . . . . ?
C1 C2 B6 B10 -99.7(2) . . . . ?
C1 C2 B6 B11 -140.5(2) . . . . ?
C1 C2 B7 Ru3 -54.03(17) . . . . ?
C1 C2 B7 B8 1.4(3) . . . . ?
C1 C2 B7 B11 102.7(2) . . . . ?
C1 C2 B7 B12 62.6(3) . . . . ?
C1 C2 B11 B6 37.2(2) . . . . ?
C1 C2 B11 B7 -106.2(2) . . . . ?
C1 C2 B11 B10 -3.2(3) . . . . ?
C1 C2 B11 B12 -65.7(3) . . . . ?
C1 B4 B5 B6 35.26(19) . . . . ?
C1 B4 B5 B9 135.7(2) . . . . ?
C1 B4 B5 B10 98.4(2) . . . . ?
C1 B4 B8 Ru3 56.39(15) . . . . ?
C1 B4 B8 B7 3.6(2) . . . . ?
C1 B4 B8 B9 -97.0(2) . . . . ?
C1 B4 B8 B12 -58.5(2) . . . . ?
C1 B4 B9 B5 -38.06(19) . . . . ?
C1 B4 B9 B8 101.7(2) . . . . ?
C1 B4 B9 B10 -0.7(3) . . . . ?
C1 B4 B9 B12 62.8(3) . . . . ?
C1 B5 B6 C2 35.47(17) . . . . ?
C1 B5 B6 B10 135.7(2) . . . . ?
C1 B5 B6 B11 96.9(2) . . . . ?
C1 B5 B9 B4 38.62(19) . . . . ?
C1 B5 B9 B8 1.3(3) . . . . ?
C1 B5 B9 B10 -99.9(2) . . . . ?
C1 B5 B9 B12 -62.7(3) . . . . ?
C1 B5 B10 B6 -39.13(19) . . . . ?
C1 B5 B10 B9 99.6(2) . . . . ?
C1 B5 B10 B11 -1.2(3) . . . . ?
C1 B5 B10 B12 62.2(3) . . . . ?
C1 B6 B10 B5 38.7(2) . . . . ?
C1 B6 B10 B9 1.9(3) . . . . ?
C1 B6 B10 B11 -98.3(2) . . . . ?
C1 B6 B10 B12 -61.8(3) . . . . ?
C1 B6 B11 C2 -33.05(18) . . . . ?
C1 B6 B11 B7 0.2(3) . . . . ?
C1 B6 B11 B10 100.7(2) . . . . ?
C1 B6 B11 B12 64.3(2) . . . . ?
C1 C1' C2' B3' 110.0(2) . . . . ?
C1 C1' C2' B6' -107.3(2) . . . . ?
C1 C1' C2' B7' 147.1(2) . . . . ?
C1 C1' C2' B11' -145.7(2) . . . . ?
C1 C1' B3' C2' -109.2(2) . . . . ?
C1 C1' B3' B4' 113.1(2) . . . . ?
C1 C1' B3' B7' -144.2(2) . . . . ?
C1 C1' B3' B8' 152.3(2) . . . . ?
C1 C1' B4' B3' -108.5(2) . . . . ?
C1 C1' B4' B5' 112.5(2) . . . . ?
C1 C1' B4' B8' -146.9(2) . . . . ?
C1 C1' B4' B9' 150.3(2) . . . . ?
C1 C1' B5' B4' -111.8(3) . . . . ?
C1 C1' B5' B6' 105.6(3) . . . . ?
C1 C1' B5' B9' -151.0(2) . . . . ?
C1 C1' B5' B10' 144.2(2) . . . . ?
C1 C1' B6' C2' 109.7(2) . . . . ?
C1 C1' B6' B5' -114.1(2) . . . . ?
C1 C1' B6' B10' -151.9(2) . . . . ?
C1 C1' B6' B11' 145.4(2) . . . . ?
C2 C1 B4 Ru3 51.70(15) . . . . ?
C2 C1 B4 B5 -102.6(2) . . . . ?
C2 C1 B4 B8 -2.8(2) . . . . ?
C2 C1 B4 B9 -64.4(2) . . . . ?
C2 C1 B5 B4 101.4(2) . . . . ?
C2 C1 B5 B6 -39.6(2) . . . . ?
C2 C1 B5 B9 62.3(3) . . . . ?
C2 C1 B5 B10 -0.8(3) . . . . ?
C2 C1 B6 B5 137.0(2) . . . . ?
C2 C1 B6 B10 97.7(2) . . . . ?
C2 C1 B6 B11 34.39(19) . . . . ?
C2 C1 C1' C2' -111.3(2) . . . . ?
C2 C1 C1' B3' -39.3(3) . . . . ?
C2 C1 C1' B4' 33.3(3) . . . . ?
C2 C1 C1' B5' 107.3(3) . . . . ?
C2 C1 C1' B6' 178.5(2) . . . . ?
C2 B6 B10 B5 97.0(2) . . . . ?
C2 B6 B10 B9 60.3(3) . . . . ?
C2 B6 B10 B11 -40.0(2) . . . . ?
C2 B6 B10 B12 -3.5(3) . . . . ?
C2 B6 B11 B7 33.2(2) . . . . ?
C2 B6 B11 B10 133.8(2) . . . . ?
C2 B6 B11 B12 97.3(2) . . . . ?
C2 B7 B8 Ru3 -56.02(15) . . . . ?
C2 B7 B8 B4 -3.0(2) . . . . ?
C2 B7 B8 B9 59.2(2) . . . . ?
C2 B7 B8 B12 97.6(2) . . . . ?
C2 B7 B11 B6 -33.6(2) . . . . ?
C2 B7 B11 B10 -97.5(2) . . . . ?
C2 B7 B11 B12 -133.6(2) . . . . ?
C2 B7 B12 B8 -99.0(2) . . . . ?
C2 B7 B12 B9 -60.3(3) . . . . ?
C2 B7 B12 B10 3.4(3) . . . . ?
C2 B7 B12 B11 39.5(2) . . . . ?
C2 B11 B12 B7 -40.2(2) . . . . ?
C2 B11 B12 B8 -2.1(3) . . . . ?
C2 B11 B12 B9 61.4(3) . . . . ?
C2 B11 B12 B10 99.7(2) . . . . ?
B4 C1 C2 Ru3 -51.00(15) . . . . ?
B4 C1 C2 B6 105.3(2) . . . . ?
B4 C1 C2 B7 0.9(3) . . . . ?
B4 C1 C2 B11 68.8(2) . . . . ?
B4 C1 B5 B6 -141.0(2) . . . . ?
B4 C1 B5 B9 -39.1(2) . . . . ?
B4 C1 B5 B10 -102.2(2) . . . . ?
B4 C1 B6 C2 -100.2(2) . . . . ?
B4 C1 B6 B5 36.9(2) . . . . ?
B4 C1 B6 B10 -2.5(3) . . . . ?
B4 C1 B6 B11 -65.8(2) . . . . ?
B4 C1 C1' C2' 42.0(3) . . . . ?
B4 C1 C1' B3' 114.0(3) . . . . ?
B4 C1 C1' B4' -173.4(2) . . . . ?
B4 C1 C1' B5' -99.4(3) . . . . ?
B4 C1 C1' B6' -28.2(3) . . . . ?
B4 B5 B6 C1 -34.85(18) . . . . ?
B4 B5 B6 C2 0.6(3) . . . . ?
B4 B5 B6 B10 100.9(2) . . . . ?
B4 B5 B6 B11 62.1(3) . . . . ?
B4 B5 B9 B8 -37.4(2) . . . . ?
B4 B5 B9 B10 -138.6(2) . . . . ?
B4 B5 B9 B12 -101.3(2) . . . . ?
B4 B5 B10 B6 -101.4(2) . . . . ?
B4 B5 B10 B9 37.3(2) . . . . ?
B4 B5 B10 B11 -63.4(3) . . . . ?
B4 B5 B10 B12 -0.1(3) . . . . ?
B4 B8 B9 B5 37.1(2) . . . . ?
B4 B8 B9 B10 101.6(2) . . . . ?
B4 B8 B9 B12 136.5(2) . . . . ?
B4 B8 B12 B7 98.4(2) . . . . ?
B4 B8 B12 B9 -38.28(19) . . . . ?
B4 B8 B12 B10 -3.3(3) . . . . ?
B4 B8 B12 B11 60.7(3) . . . . ?
B4 B9 B10 B5 -37.7(2) . . . . ?
B4 B9 B10 B6 -0.8(3) . . . . ?
B4 B9 B10 B11 62.1(3) . . . . ?
B4 B9 B10 B12 100.5(2) . . . . ?
B4 B9 B12 B7 0.1(3) . . . . ?
B4 B9 B12 B8 39.5(2) . . . . ?
B4 B9 B12 B10 -101.9(2) . . . . ?
B4 B9 B12 B11 -63.6(3) . . . . ?
B5 C1 C2 Ru3 -117.25(17) . . . . ?
B5 C1 C2 B6 39.03(19) . . . . ?
B5 C1 C2 B7 -65.4(2) . . . . ?
B5 C1 C2 B11 2.5(3) . . . . ?
B5 C1 B4 Ru3 154.30(17) . . . . ?
B5 C1 B4 B8 99.8(2) . . . . ?
B5 C1 B4 B9 38.2(2) . . . . ?
B5 C1 B6 C2 -137.0(2) . . . . ?
B5 C1 B6 B10 -39.3(2) . . . . ?
B5 C1 B6 B11 -102.7(2) . . . . ?
B5 C1 C1' C2' 114.5(2) . . . . ?
B5 C1 C1' B3' -173.6(2) . . . . ?
B5 C1 C1' B4' -101.0(3) . . . . ?
B5 C1 C1' B5' -27.0(3) . . . . ?
B5 C1 C1' B6' 44.2(3) . . . . ?
B5 B4 B8 Ru3 118.07(18) . . . . ?
B5 B4 B8 B7 65.3(2) . . . . ?
B5 B4 B8 B9 -35.35(19) . . . . ?
B5 B4 B8 B12 3.2(3) . . . . ?
B5 B4 B9 B8 139.8(2) . . . . ?
B5 B4 B9 B10 37.4(2) . . . . ?
B5 B4 B9 B12 100.9(2) . . . . ?
B5 B6 B10 B9 -36.8(2) . . . . ?
B5 B6 B10 B11 -137.0(2) . . . . ?
B5 B6 B10 B12 -100.5(2) . . . . ?
B5 B6 B11 C2 -95.0(2) . . . . ?
B5 B6 B11 B7 -61.8(3) . . . . ?
B5 B6 B11 B10 38.7(2) . . . . ?
B5 B6 B11 B12 2.3(3) . . . . ?
B5 B9 B10 B6 36.9(2) . . . . ?
B5 B9 B10 B11 99.8(2) . . . . ?
B5 B9 B10 B12 138.3(2) . . . . ?
B5 B9 B12 B7 64.6(3) . . . . ?
B5 B9 B12 B8 104.0(2) . . . . ?
B5 B9 B12 B10 -37.4(2) . . . . ?
B5 B9 B12 B11 0.9(3) . . . . ?
B5 B10 B11 C2 2.6(3) . . . . ?
B5 B10 B11 B6 -38.2(2) . . . . ?
B5 B10 B11 B7 65.1(3) . . . . ?
B5 B10 B11 B12 101.2(2) . . . . ?
B5 B10 B12 B7 -63.4(3) . . . . ?
B5 B10 B12 B8 2.1(3) . . . . ?
B5 B10 B12 B9 37.1(2) . . . . ?
B5 B10 B12 B11 -99.8(2) . . . . ?
B6 C1 C2 Ru3 -156.27(15) . . . . ?
B6 C1 C2 B7 -104.4(2) . . . . ?
B6 C1 C2 B11 -36.5(2) . . . . ?
B6 C1 B4 Ru3 118.06(18) . . . . ?
B6 C1 B4 B5 -36.2(2) . . . . ?
B6 C1 B4 B8 63.5(2) . . . . ?
B6 C1 B4 B9 1.9(3) . . . . ?
B6 C1 B5 B4 141.0(2) . . . . ?
B6 C1 B5 B9 101.8(2) . . . . ?
B6 C1 B5 B10 38.8(2) . . . . ?
B6 C1 C1' C2' -179.6(2) . . . . ?
B6 C1 C1' B3' -107.7(2) . . . . ?
B6 C1 C1' B4' -35.0(3) . . . . ?
B6 C1 C1' B5' 38.9(3) . . . . ?
B6 C1 C1' B6' 110.1(2) . . . . ?
B6 C2 B7 Ru3 -122.45(19) . . . . ?
B6 C2 B7 B8 -67.0(2) . . . . ?
B6 C2 B7 B11 34.2(2) . . . . ?
B6 C2 B7 B12 -5.8(3) . . . . ?
B6 C2 B11 B7 -143.4(2) . . . . ?
B6 C2 B11 B10 -40.4(2) . . . . ?
B6 C2 B11 B12 -102.9(2) . . . . ?
B6 B5 B9 B4 101.9(2) . . . . ?
B6 B5 B9 B8 64.5(3) . . . . ?
B6 B5 B9 B10 -36.7(2) . . . . ?
B6 B5 B9 B12 0.5(3) . . . . ?
B6 B5 B10 B9 138.7(2) . . . . ?
B6 B5 B10 B11 38.0(2) . . . . ?
B6 B5 B10 B12 101.3(2) . . . . ?
B6 B10 B11 C2 40.7(2) . . . . ?
B6 B10 B11 B7 103.2(2) . . . . ?
B6 B10 B11 B12 139.4(2) . . . . ?
B6 B10 B12 B7 0.1(3) . . . . ?
B6 B10 B12 B8 65.6(3) . . . . ?
B6 B10 B12 B9 100.6(2) . . . . ?
B6 B10 B12 B11 -36.3(2) . . . . ?
B6 B11 B12 B7 -103.6(2) . . . . ?
B6 B11 B12 B8 -65.4(3) . . . . ?
B6 B11 B12 B9 -2.0(3) . . . . ?
B6 B11 B12 B10 36.3(2) . . . . ?
B7 C2 B6 C1 105.6(2) . . . . ?
B7 C2 B6 B5 68.6(2) . . . . ?
B7 C2 B6 B10 5.9(3) . . . . ?
B7 C2 B6 B11 -34.9(2) . . . . ?
B7 C2 B11 B6 143.4(2) . . . . ?
B7 C2 B11 B10 103.0(2) . . . . ?
B7 C2 B11 B12 40.6(2) . . . . ?
B7 B8 B9 B4 -98.4(2) . . . . ?
B7 B8 B9 B5 -61.3(3) . . . . ?
B7 B8 B9 B10 3.2(3) . . . . ?
B7 B8 B9 B12 38.10(19) . . . . ?
B7 B8 B12 B9 -136.7(2) . . . . ?
B7 B8 B12 B10 -101.7(2) . . . . ?
B7 B8 B12 B11 -37.7(2) . . . . ?
B7 B11 B12 B8 38.2(2) . . . . ?
B7 B11 B12 B9 101.6(2) . . . . ?
B7 B11 B12 B10 139.9(2) . . . . ?
B8 B4 B5 C1 -100.3(2) . . . . ?
B8 B4 B5 B6 -65.0(2) . . . . ?
B8 B4 B5 B9 35.4(2) . . . . ?
B8 B4 B5 B10 -1.9(3) . . . . ?
B8 B4 B9 B5 -139.8(2) . . . . ?
B8 B4 B9 B10 -102.4(2) . . . . ?
B8 B4 B9 B12 -38.9(2) . . . . ?
B8 B7 B11 C2 97.1(2) . . . . ?
B8 B7 B11 B6 63.5(3) . . . . ?
B8 B7 B11 B10 -0.4(3) . . . . ?
B8 B7 B11 B12 -36.5(2) . . . . ?
B8 B7 B12 B9 38.7(2) . . . . ?
B8 B7 B12 B10 102.4(2) . . . . ?
B8 B7 B12 B11 138.5(2) . . . . ?
B8 B9 B10 B5 -103.3(2) . . . . ?
B8 B9 B10 B6 -66.3(3) . . . . ?
B8 B9 B10 B11 -3.4(3) . . . . ?
B8 B9 B10 B12 35.0(2) . . . . ?
B8 B9 B12 B7 -39.4(2) . . . . ?
B8 B9 B12 B10 -141.4(2) . . . . ?
B8 B9 B12 B11 -103.1(2) . . . . ?
B9 B4 B5 C1 -135.7(2) . . . . ?
B9 B4 B5 B6 -100.4(2) . . . . ?
B9 B4 B5 B10 -37.3(2) . . . . ?
B9 B4 B8 Ru3 153.42(18) . . . . ?
B9 B4 B8 B7 100.6(2) . . . . ?
B9 B4 B8 B12 38.5(2) . . . . ?
B9 B5 B6 C1 -98.7(2) . . . . ?
B9 B5 B6 C2 -63.2(2) . . . . ?
B9 B5 B6 B10 37.1(2) . . . . ?
B9 B5 B6 B11 -1.7(3) . . . . ?
B9 B5 B10 B6 -138.7(2) . . . . ?
B9 B5 B10 B11 -100.7(2) . . . . ?
B9 B5 B10 B12 -37.4(2) . . . . ?
B9 B8 B12 B7 136.7(2) . . . . ?
B9 B8 B12 B10 35.0(2) . . . . ?
B9 B8 B12 B11 99.0(3) . . . . ?
B9 B10 B11 C2 -60.2(3) . . . . ?
B9 B10 B11 B6 -100.9(2) . . . . ?
B9 B10 B11 B7 2.3(3) . . . . ?
B9 B10 B11 B12 38.5(2) . . . . ?
B9 B10 B12 B7 -100.5(2) . . . . ?
B9 B10 B12 B8 -35.0(2) . . . . ?
B9 B10 B12 B11 -136.9(2) . . . . ?
B10 B5 B6 C1 -135.7(2) . . . . ?
B10 B5 B6 C2 -100.3(2) . . . . ?
B10 B5 B6 B11 -38.8(2) . . . . ?
B10 B5 B9 B4 138.6(2) . . . . ?
B10 B5 B9 B8 101.2(2) . . . . ?
B10 B5 B9 B12 37.2(2) . . . . ?
B10 B6 B11 C2 -133.8(2) . . . . ?
B10 B6 B11 B7 -100.5(2) . . . . ?
B10 B6 B11 B12 -36.4(2) . . . . ?
B10 B9 B12 B7 102.0(2) . . . . ?
B10 B9 B12 B8 141.4(2) . . . . ?
B10 B9 B12 B11 38.2(2) . . . . ?
B10 B11 B12 B7 -139.9(2) . . . . ?
B10 B11 B12 B8 -101.7(3) . . . . ?
B10 B11 B12 B9 -38.3(2) . . . . ?
B11 C2 B6 C1 140.5(2) . . . . ?
B11 C2 B6 B5 103.5(2) . . . . ?
B11 C2 B6 B10 40.8(2) . . . . ?
B11 C2 B7 Ru3 -156.70(18) . . . . ?
B11 C2 B7 B8 -101.2(2) . . . . ?
B11 C2 B7 B12 -40.0(2) . . . . ?
B11 B6 B10 B5 137.0(2) . . . . ?
B11 B6 B10 B9 100.2(3) . . . . ?
B11 B6 B10 B12 36.5(2) . . . . ?
B11 B7 B8 Ru3 -116.95(19) . . . . ?
B11 B7 B8 B4 -64.0(2) . . . . ?
B11 B7 B8 B9 -1.7(3) . . . . ?
B11 B7 B8 B12 36.7(2) . . . . ?
B11 B7 B12 B8 -138.5(2) . . . . ?
B11 B7 B12 B9 -99.8(2) . . . . ?
B11 B7 B12 B10 -36.1(2) . . . . ?
B11 B10 B12 B7 36.3(2) . . . . ?
B11 B10 B12 B8 101.9(2) . . . . ?
B11 B10 B12 B9 136.9(2) . . . . ?
B12 B7 B8 Ru3 -153.65(19) . . . . ?
B12 B7 B8 B4 -100.6(2) . . . . ?
B12 B7 B8 B9 -38.4(2) . . . . ?
B12 B7 B11 C2 133.6(2) . . . . ?
B12 B7 B11 B6 100.0(2) . . . . ?
B12 B7 B11 B10 36.1(2) . . . . ?
B12 B8 B9 B4 -136.5(2) . . . . ?
B12 B8 B9 B5 -99.4(2) . . . . ?
B12 B8 B9 B10 -34.9(2) . . . . ?
B12 B9 B10 B5 -138.3(2) . . . . ?
B12 B9 B10 B6 -101.3(2) . . . . ?
B12 B9 B10 B11 -38.5(2) . . . . ?
B12 B10 B11 C2 -98.6(2) . . . . ?
B12 B10 B11 B6 -139.4(2) . . . . ?
B12 B10 B11 B7 -36.2(2) . . . . ?
C30 C31 C32 Ru3 -53.3(2) . . . . ?
C30 C31 C32 C33 1.3(4) . . . . ?
C31 C30 C35 Ru3 55.0(2) . . . . ?
C31 C30 C35 C34 -0.6(3) . . . . ?
C31 C30 C37 C38 97.8(3) . . . . ?
C31 C30 C37 C39 -138.0(2) . . . . ?
C31 C32 C33 Ru3 -55.9(2) . . . . ?
C31 C32 C33 C34 -0.9(4) . . . . ?
C31 C32 C33 C36 179.2(2) . . . . ?
C32 C33 C34 Ru3 -57.0(2) . . . . ?
C32 C33 C34 C35 -0.2(4) . . . . ?
C33 C34 C35 Ru3 -57.1(2) . . . . ?
C33 C34 C35 C30 0.9(4) . . . . ?
C35 C30 C31 Ru3 -53.00(19) . . . . ?
C35 C30 C31 C32 -0.5(3) . . . . ?
C35 C30 C37 C38 -77.5(3) . . . . ?
C35 C30 C37 C39 46.7(3) . . . . ?
C36 C33 C34 Ru3 122.9(2) . . . . ?
C36 C33 C34 C35 179.7(2) . . . . ?
C37 C30 C31 Ru3 131.5(2) . . . . ?
C37 C30 C31 C32 -176.0(2) . . . . ?
C37 C30 C35 Ru3 -129.6(2) . . . . ?
C37 C30 C35 C34 174.8(2) . . . . ?
C1' C1 C2 Ru3 106.4(2) . . . . ?
C1' C1 C2 B6 -97.3(2) . . . . ?
C1' C1 C2 B7 158.3(2) . . . . ?
C1' C1 C2 B11 -133.8(2) . . . . ?
C1' C1 B4 Ru3 -104.3(2) . . . . ?
C1' C1 B4 B5 101.4(3) . . . . ?
C1' C1 B4 B8 -158.8(2) . . . . ?
C1' C1 B4 B9 139.6(2) . . . . ?
C1' C1 B5 B4 -119.2(2) . . . . ?
C1' C1 B5 B6 99.8(2) . . . . ?
C1' C1 B5 B9 -158.4(2) . . . . ?
C1' C1 B5 B10 138.6(2) . . . . ?
C1' C1 B6 C2 115.2(2) . . . . ?
C1' C1 B6 B5 -107.7(2) . . . . ?
C1' C1 B6 B10 -147.0(2) . . . . ?
C1' C1 B6 B11 149.6(2) . . . . ?
C1' C2' B3' B4' 37.27(18) . . . . ?
C1' C2' B3' B7' 140.0(2) . . . . ?
C1' C2' B3' B8' 100.7(2) . . . . ?
C1' C2' B6' B5' -37.69(18) . . . . ?
C1' C2' B6' B10' -99.9(2) . . . . ?
C1' C2' B6' B11' -139.0(2) . . . . ?
C1' C2' B7' B3' -36.64(19) . . . . ?
C1' C2' B7' B8' 2.0(3) . . . . ?
C1' C2' B7' B11' 103.8(2) . . . . ?
C1' C2' B7' B12' 65.0(3) . . . . ?
C1' C2' B11' B6' 38.2(2) . . . . ?
C1' C2' B11' B7' -102.9(2) . . . . ?
C1' C2' B11' B10' -0.7(3) . . . . ?
C1' C2' B11' B12' -63.9(3) . . . . ?
C1' B3' B4' B5' 35.97(19) . . . . ?
C1' B3' B4' B8' 136.2(2) . . . . ?
C1' B3' B4' B9' 98.4(2) . . . . ?
C1' B3' B7' C2' 34.56(18) . . . . ?
C1' B3' B7' B8' -101.1(2) . . . . ?
C1' B3' B7' B11' -0.4(3) . . . . ?
C1' B3' B7' B12' -63.2(2) . . . . ?
C1' B3' B8' B4' -38.9(2) . . . . ?
C1' B3' B8' B7' 99.4(2) . . . . ?
C1' B3' B8' B9' -1.1(3) . . . . ?
C1' B3' B8' B12' 61.8(3) . . . . ?
C1' B4' B5' B6' 34.5(2) . . . . ?
C1' B4' B5' B9' 136.8(2) . . . . ?
C1' B4' B5' B10' 99.8(2) . . . . ?
C1' B4' B8' B3' 38.11(19) . . . . ?
C1' B4' B8' B7' 0.7(3) . . . . ?
C1' B4' B8' B9' -99.5(2) . . . . ?
C1' B4' B8' B12' -62.4(3) . . . . ?
C1' B4' B9' B5' -37.63(19) . . . . ?
C1' B4' B9' B8' 99.6(2) . . . . ?
C1' B4' B9' B10' -2.0(3) . . . . ?
C1' B4' B9' B12' 62.0(3) . . . . ?
C1' B5' B6' C2' 37.06(18) . . . . ?
C1' B5' B6' B10' 137.2(2) . . . . ?
C1' B5' B6' B11' 98.5(2) . . . . ?
C1' B5' B9' B4' 38.7(2) . . . . ?
C1' B5' B9' B8' 0.9(3) . . . . ?
C1' B5' B9' B10' -101.4(2) . . . . ?
C1' B5' B9' B12' -62.7(3) . . . . ?
C1' B5' B10' B6' -38.5(2) . . . . ?
C1' B5' B10' B9' 101.2(2) . . . . ?
C1' B5' B10' B11' 0.5(3) . . . . ?
C1' B5' B10' B12' 63.1(3) . . . . ?
C1' B6' B10' B5' 37.4(2) . . . . ?
C1' B6' B10' B9' 1.7(3) . . . . ?
C1' B6' B10' B11' -98.8(2) . . . . ?
C1' B6' B10' B12' -61.3(3) . . . . ?
C1' B6' B11' C2' -35.1(2) . . . . ?
C1' B6' B11' B7' -0.8(3) . . . . ?
C1' B6' B11' B10' 100.4(2) . . . . ?
C1' B6' B11' B12' 62.5(3) . . . . ?
C2' C1' B3' B4' -137.8(2) . . . . ?
C2' C1' B3' B7' -35.03(19) . . . . ?
C2' C1' B3' B8' -98.5(2) . . . . ?
C2' C1' B4' B3' 38.9(2) . . . . ?
C2' C1' B4' B5' -100.1(2) . . . . ?
C2' C1' B4' B8' 0.5(3) . . . . ?
C2' C1' B4' B9' -62.3(2) . . . . ?
C2' C1' B5' B4' 103.1(2) . . . . ?
C2' C1' B5' B6' -39.46(19) . . . . ?
C2' C1' B5' B9' 63.9(3) . . . . ?
C2' C1' B5' B10' -0.9(3) . . . . ?
C2' C1' B6' B5' 136.2(2) . . . . ?
C2' C1' B6' B10' 98.4(2) . . . . ?
C2' C1' B6' B11' 35.8(2) . . . . ?
C2' B3' B4' C1' -36.35(18) . . . . ?
C2' B3' B4' B5' -0.4(3) . . . . ?
C2' B3' B4' B8' 99.9(2) . . . . ?
C2' B3' B4' B9' 62.1(2) . . . . ?
C2' B3' B7' B8' -135.6(2) . . . . ?
C2' B3' B7' B11' -34.9(2) . . . . ?
C2' B3' B7' B12' -97.8(2) . . . . ?
C2' B3' B8' B4' -99.7(2) . . . . ?
C2' B3' B8' B7' 38.63(19) . . . . ?
C2' B3' B8' B9' -61.9(3) . . . . ?
C2' B3' B8' B12' 1.0(3) . . . . ?
C2' B6' B10' B5' 97.5(2) . . . . ?
C2' B6' B10' B9' 61.9(3) . . . . ?
C2' B6' B10' B11' -38.6(2) . . . . ?
C2' B6' B10' B12' -1.2(3) . . . . ?
C2' B6' B11' B7' 34.4(2) . . . . ?
C2' B6' B11' B10' 135.5(2) . . . . ?
C2' B6' B11' B12' 97.6(2) . . . . ?
C2' B7' B8' B3' -38.73(19) . . . . ?
C2' B7' B8' B4' -1.7(3) . . . . ?
C2' B7' B8' B9' 61.7(3) . . . . ?
C2' B7' B8' B12' 99.0(2) . . . . ?
C2' B7' B11' B6' -34.5(2) . . . . ?
C2' B7' B11' B10' -97.6(2) . . . . ?
C2' B7' B11' B12' -135.5(2) . . . . ?
C2' B7' B12' B8' -99.6(2) . . . . ?
C2' B7' B12' B9' -62.2(3) . . . . ?
C2' B7' B12' B10' 1.1(3) . . . . ?
C2' B7' B12' B11' 38.4(2) . . . . ?
C2' B11' B12' B7' -38.5(2) . . . . ?
C2' B11' B12' B8' -1.0(3) . . . . ?
C2' B11' B12' B9' 62.2(3) . . . . ?
C2' B11' B12' B10' 99.4(2) . . . . ?
B3' C1' C2' B6' 142.7(2) . . . . ?
B3' C1' C2' B7' 37.1(2) . . . . ?
B3' C1' C2' B11' 104.3(2) . . . . ?
B3' C1' B4' B5' -139.0(2) . . . . ?
B3' C1' B4' B8' -38.45(19) . . . . ?
B3' C1' B4' B9' -101.2(2) . . . . ?
B3' C1' B5' B4' 37.6(2) . . . . ?
B3' C1' B5' B6' -105.0(2) . . . . ?
B3' C1' B5' B9' -1.6(3) . . . . ?
B3' C1' B5' B10' -66.4(3) . . . . ?
B3' C1' B6' C2' -35.20(19) . . . . ?
B3' C1' B6' B5' 101.0(2) . . . . ?
B3' C1' B6' B10' 63.2(3) . . . . ?
B3' C1' B6' B11' 0.6(3) . . . . ?
B3' C2' B6' C1' 34.67(19) . . . . ?
B3' C2' B6' B5' -3.0(3) . . . . ?
B3' C2' B6' B10' -65.2(3) . . . . ?
B3' C2' B6' B11' -104.3(2) . . . . ?
B3' C2' B7' B8' 38.65(19) . . . . ?
B3' C2' B7' B11' 140.4(2) . . . . ?
B3' C2' B7' B12' 101.6(2) . . . . ?
B3' C2' B11' B6' 103.9(2) . . . . ?
B3' C2' B11' B7' -37.2(2) . . . . ?
B3' C2' B11' B10' 65.0(3) . . . . ?
B3' C2' B11' B12' 1.7(3) . . . . ?
B3' B4' B5' C1' -35.98(19) . . . . ?
B3' B4' B5' B6' -1.5(3) . . . . ?
B3' B4' B5' B9' 100.8(2) . . . . ?
B3' B4' B5' B10' 63.9(3) . . . . ?
B3' B4' B8' B7' -37.4(2) . . . . ?
B3' B4' B8' B9' -137.6(2) . . . . ?
B3' B4' B8' B12' -100.5(2) . . . . ?
B3' B4' B9' B5' -99.5(2) . . . . ?
B3' B4' B9' B8' 37.7(2) . . . . ?
B3' B4' B9' B10' -63.9(3) . . . . ?
B3' B4' B9' B12' 0.1(3) . . . . ?
B3' B7' B8' B4' 37.1(2) . . . . ?
B3' B7' B8' B9' 100.4(2) . . . . ?
B3' B7' B8' B12' 137.7(2) . . . . ?
B3' B7' B11' C2' 35.2(2) . . . . ?
B3' B7' B11' B6' 0.7(3) . . . . ?
B3' B7' B11' B10' -62.3(3) . . . . ?
B3' B7' B11' B12' -100.3(2) . . . . ?
B3' B7' B12' B8' -37.4(2) . . . . ?
B3' B7' B12' B9' 0.1(3) . . . . ?
B3' B7' B12' B10' 63.3(3) . . . . ?
B3' B7' B12' B11' 100.7(2) . . . . ?
B3' B8' B9' B4' -37.5(2) . . . . ?
B3' B8' B9' B5' 0.2(3) . . . . ?
B3' B8' B9' B10' 63.1(3) . . . . ?
B3' B8' B9' B12' 100.8(2) . . . . ?
B3' B8' B12' B7' 37.8(2) . . . . ?
B3' B8' B12' B9' -100.1(2) . . . . ?
B3' B8' B12' B10' -62.9(3) . . . . ?
B3' B8' B12' B11' 0.0(3) . . . . ?
B4' C1' C2' B3' -38.68(19) . . . . ?
B4' C1' C2' B6' 104.0(2) . . . . ?
B4' C1' C2' B7' -1.6(3) . . . . ?
B4' C1' C2' B11' 65.6(3) . . . . ?
B4' C1' B3' C2' 137.8(2) . . . . ?
B4' C1' B3' B7' 102.7(2) . . . . ?
B4' C1' B3' B8' 39.2(2) . . . . ?
B4' C1' B5' B6' -142.6(2) . . . . ?
B4' C1' B5' B9' -39.2(2) . . . . ?
B4' C1' B5' B10' -104.0(2) . . . . ?
B4' C1' B6' C2' -101.5(2) . . . . ?
B4' C1' B6' B5' 34.7(2) . . . . ?
B4' C1' B6' B10' -3.1(3) . . . . ?
B4' C1' B6' B11' -65.7(3) . . . . ?
B4' B3' B7' C2' 97.8(2) . . . . ?
B4' B3' B7' B8' -37.85(19) . . . . ?
B4' B3' B7' B11' 62.9(3) . . . . ?
B4' B3' B7' B12' 0.0(3) . . . . ?
B4' B3' B8' B7' 138.3(2) . . . . ?
B4' B3' B8' B9' 37.8(2) . . . . ?
B4' B3' B8' B12' 100.7(2) . . . . ?
B4' B5' B6' C1' -34.3(2) . . . . ?
B4' B5' B6' C2' 2.7(3) . . . . ?
B4' B5' B6' B10' 102.9(2) . . . . ?
B4' B5' B6' B11' 64.2(3) . . . . ?
B4' B5' B9' B8' -37.9(2) . . . . ?
B4' B5' B9' B10' -140.1(2) . . . . ?
B4' B5' B9' B12' -101.4(2) . . . . ?
B4' B5' B10' B6' -102.8(2) . . . . ?
B4' B5' B10' B9' 37.0(2) . . . . ?
B4' B5' B10' B11' -63.8(3) . . . . ?
B4' B5' B10' B12' -1.1(3) . . . . ?
B4' B8' B9' B5' 37.7(2) . . . . ?
B4' B8' B9' B10' 100.6(2) . . . . ?
B4' B8' B9' B12' 138.3(2) . . . . ?
B4' B8' B12' B7' 100.7(2) . . . . ?
B4' B8' B12' B9' -37.3(2) . . . . ?
B4' B8' B12' B10' -0.1(3) . . . . ?
B4' B8' B12' B11' 62.9(3) . . . . ?
B4' B9' B10' B5' -35.5(2) . . . . ?
B4' B9' B10' B6' 0.2(3) . . . . ?
B4' B9' B10' B11' 64.0(3) . . . . ?
B4' B9' B10' B12' 101.2(2) . . . . ?
B4' B9' B12' B7' -0.1(3) . . . . ?
B4' B9' B12' B8' 37.3(2) . . . . ?
B4' B9' B12' B10' -101.0(2) . . . . ?
B4' B9' B12' B11' -64.0(3) . . . . ?
B5' C1' C2' B3' -103.4(2) . . . . ?
B5' C1' C2' B6' 39.3(2) . . . . ?
B5' C1' C2' B7' -66.3(3) . . . . ?
B5' C1' C2' B11' 1.0(3) . . . . ?
B5' C1' B3' C2' 100.3(2) . . . . ?
B5' C1' B3' B4' -37.5(2) . . . . ?
B5' C1' B3' B7' 65.2(2) . . . . ?
B5' C1' B3' B8' 1.7(3) . . . . ?
B5' C1' B4' B3' 139.0(2) . . . . ?
B5' C1' B4' B8' 100.6(2) . . . . ?
B5' C1' B4' B9' 37.8(2) . . . . ?
B5' C1' B6' C2' -136.2(2) . . . . ?
B5' C1' B6' B10' -37.8(2) . . . . ?
B5' C1' B6' B11' -100.4(2) . . . . ?
B5' B4' B8' B3' 99.9(2) . . . . ?
B5' B4' B8' B7' 62.6(3) . . . . ?
B5' B4' B8' B9' -37.7(2) . . . . ?
B5' B4' B8' B12' -0.6(3) . . . . ?
B5' B4' B9' B8' 137.2(2) . . . . ?
B5' B4' B9' B10' 35.6(2) . . . . ?
B5' B4' B9' B12' 99.7(3) . . . . ?
B5' B6' B10' B9' -35.7(2) . . . . ?
B5' B6' B10' B11' -136.2(2) . . . . ?
B5' B6' B10' B12' -98.7(3) . . . . ?
B5' B6' B11' C2' -96.8(2) . . . . ?
B5' B6' B11' B7' -62.4(3) . . . . ?
B5' B6' B11' B10' 38.7(2) . . . . ?
B5' B6' B11' B12' 0.9(3) . . . . ?
B5' B9' B10' B6' 35.8(2) . . . . ?
B5' B9' B10' B11' 99.5(2) . . . . ?
B5' B9' B10' B12' 136.7(2) . . . . ?
B5' B9' B12' B7' 62.6(3) . . . . ?
B5' B9' B12' B8' 100.0(2) . . . . ?
B5' B9' B12' B10' -38.3(2) . . . . ?
B5' B9' B12' B11' -1.2(3) . . . . ?
B5' B10' B11' C2' 0.1(3) . . . . ?
B5' B10' B11' B6' -38.6(2) . . . . ?
B5' B10' B11' B7' 61.8(3) . . . . ?
B5' B10' B11' B12' 99.4(3) . . . . ?
B5' B10' B12' B7' -62.5(3) . . . . ?
B5' B10' B12' B8' 0.7(3) . . . . ?
B5' B10' B12' B9' 37.9(2) . . . . ?
B5' B10' B12' B11' -100.3(3) . . . . ?
B6' C1' C2' B3' -142.7(2) . . . . ?
B6' C1' C2' B7' -105.6(2) . . . . ?
B6' C1' C2' B11' -38.4(2) . . . . ?
B6' C1' B3' C2' 34.9(2) . . . . ?
B6' C1' B3' B4' -102.9(2) . . . . ?
B6' C1' B3' B7' -0.1(3) . . . . ?
B6' C1' B3' B8' -63.6(3) . . . . ?
B6' C1' B4' B3' 104.4(2) . . . . ?
B6' C1' B4' B5' -34.6(2) . . . . ?
B6' C1' B4' B8' 66.0(2) . . . . ?
B6' C1' B4' B9' 3.2(3) . . . . ?
B6' C1' B5' B4' 142.6(2) . . . . ?
B6' C1' B5' B9' 103.4(3) . . . . ?
B6' C1' B5' B10' 38.6(2) . . . . ?
B6' C2' B3' C1' -35.09(19) . . . . ?
B6' C2' B3' B4' 2.2(3) . . . . ?
B6' C2' B3' B7' 105.0(2) . . . . ?
B6' C2' B3' B8' 65.6(3) . . . . ?
B6' C2' B7' B3' -103.5(2) . . . . ?
B6' C2' B7' B8' -64.8(3) . . . . ?
B6' C2' B7' B11' 36.9(2) . . . . ?
B6' C2' B7' B12' -1.9(3) . . . . ?
B6' C2' B11' B7' -141.1(2) . . . . ?
B6' C2' B11' B10' -38.9(2) . . . . ?
B6' C2' B11' B12' -102.1(3) . . . . ?
B6' B5' B9' B4' 103.3(2) . . . . ?
B6' B5' B9' B8' 65.4(3) . . . . ?
B6' B5' B9' B10' -36.9(2) . . . . ?
B6' B5' B9' B12' 1.8(3) . . . . ?
B6' B5' B10' B9' 139.8(2) . . . . ?
B6' B5' B10' B11' 39.0(2) . . . . ?
B6' B5' B10' B12' 101.7(3) . . . . ?
B6' B10' B11' C2' 38.7(2) . . . . ?
B6' B10' B11' B7' 100.4(2) . . . . ?
B6' B10' B11' B12' 138.0(2) . . . . ?
B6' B10' B12' B7' 0.1(3) . . . . ?
B6' B10' B12' B8' 63.3(3) . . . . ?
B6' B10' B12' B9' 100.5(3) . . . . ?
B6' B10' B12' B11' -37.8(2) . . . . ?
B6' B11' B12' B7' -100.5(2) . . . . ?
B6' B11' B12' B8' -63.0(3) . . . . ?
B6' B11' B12' B9' 0.2(3) . . . . ?
B6' B11' B12' B10' 37.4(2) . . . . ?
B7' C2' B3' C1' -140.0(2) . . . . ?
B7' C2' B3' B4' -102.8(2) . . . . ?
B7' C2' B3' B8' -39.3(2) . . . . ?
B7' C2' B6' C1' 101.8(2) . . . . ?
B7' C2' B6' B5' 64.1(3) . . . . ?
B7' C2' B6' B10' 1.9(3) . . . . ?
B7' C2' B6' B11' -37.1(2) . . . . ?
B7' C2' B11' B6' 141.1(2) . . . . ?
B7' C2' B11' B10' 102.2(2) . . . . ?
B7' C2' B11' B12' 39.0(2) . . . . ?
B7' B3' B4' C1' -98.5(2) . . . . ?
B7' B3' B4' B5' -62.5(3) . . . . ?
B7' B3' B4' B8' 37.8(2) . . . . ?
B7' B3' B4' B9' -0.1(3) . . . . ?
B7' B3' B8' B4' -138.3(2) . . . . ?
B7' B3' B8' B9' -100.5(2) . . . . ?
B7' B3' B8' B12' -37.6(2) . . . . ?
B7' B8' B9' B4' -101.0(2) . . . . ?
B7' B8' B9' B5' -63.3(3) . . . . ?
B7' B8' B9' B10' -0.3(3) . . . . ?
B7' B8' B9' B12' 37.4(2) . . . . ?
B7' B8' B12' B9' -137.9(2) . . . . ?
B7' B8' B12' B10' -100.8(3) . . . . ?
B7' B8' B12' B11' -37.8(2) . . . . ?
B7' B11' B12' B8' 37.5(2) . . . . ?
B7' B11' B12' B9' 100.7(2) . . . . ?
B7' B11' B12' B10' 137.9(2) . . . . ?
B8' B3' B4' C1' -136.2(2) . . . . ?
B8' B3' B4' B5' -100.3(2) . . . . ?
B8' B3' B4' B9' -37.8(2) . . . . ?
B8' B3' B7' C2' 135.6(2) . . . . ?
B8' B3' B7' B11' 100.7(2) . . . . ?
B8' B3' B7' B12' 37.8(2) . . . . ?
B8' B4' B5' C1' -98.8(2) . . . . ?
B8' B4' B5' B6' -64.3(3) . . . . ?
B8' B4' B5' B9' 38.0(2) . . . . ?
B8' B4' B5' B10' 1.1(3) . . . . ?
B8' B4' B9' B5' -137.2(2) . . . . ?
B8' B4' B9' B10' -101.6(2) . . . . ?
B8' B4' B9' B12' -37.5(2) . . . . ?
B8' B7' B11' C2' 97.8(2) . . . . ?
B8' B7' B11' B6' 63.4(3) . . . . ?
B8' B7' B11' B10' 0.3(3) . . . . ?
B8' B7' B11' B12' -37.7(2) . . . . ?
B8' B7' B12' B9' 37.4(2) . . . . ?
B8' B7' B12' B10' 100.7(3) . . . . ?
B8' B7' B12' B11' 138.0(2) . . . . ?
B8' B9' B10' B5' -99.0(2) . . . . ?
B8' B9' B10' B6' -63.3(3) . . . . ?
B8' B9' B10' B11' 0.5(3) . . . . ?
B8' B9' B10' B12' 37.7(2) . . . . ?
B8' B9' B12' B7' -37.4(2) . . . . ?
B8' B9' B12' B10' -138.3(2) . . . . ?
B8' B9' B12' B11' -101.3(2) . . . . ?
B9' B4' B5' C1' -136.8(2) . . . . ?
B9' B4' B5' B6' -102.3(3) . . . . ?
B9' B4' B5' B10' -36.9(2) . . . . ?
B9' B4' B8' B3' 137.6(2) . . . . ?
B9' B4' B8' B7' 100.2(2) . . . . ?
B9' B4' B8' B12' 37.1(2) . . . . ?
B9' B5' B6' C1' -100.2(2) . . . . ?
B9' B5' B6' C2' -63.1(3) . . . . ?
B9' B5' B6' B10' 37.1(2) . . . . ?
B9' B5' B6' B11' -1.7(3) . . . . ?
B9' B5' B10' B6' -139.8(2) . . . . ?
B9' B5' B10' B11' -100.8(2) . . . . ?
B9' B5' B10' B12' -38.1(2) . . . . ?
B9' B8' B12' B7' 137.9(2) . . . . ?
B9' B8' B12' B10' 37.2(2) . . . . ?
B9' B8' B12' B11' 100.1(2) . . . . ?
B9' B10' B11' C2' -62.2(3) . . . . ?
B9' B10' B11' B6' -100.9(2) . . . . ?
B9' B10' B11' B7' -0.5(3) . . . . ?
B9' B10' B11' B12' 37.1(2) . . . . ?
B9' B10' B12' B7' -100.4(2) . . . . ?
B9' B10' B12' B8' -37.2(2) . . . . ?
B9' B10' B12' B11' -138.2(2) . . . . ?
B10' B5' B6' C1' -137.2(2) . . . . ?
B10' B5' B6' C2' -100.2(2) . . . . ?
B10' B5' B6' B11' -38.7(2) . . . . ?
B10' B5' B9' B4' 140.1(2) . . . . ?
B10' B5' B9' B8' 102.3(3) . . . . ?
B10' B5' B9' B12' 38.7(2) . . . . ?
B10' B6' B11' C2' -135.5(2) . . . . ?
B10' B6' B11' B7' -101.1(3) . . . . ?
B10' B6' B11' B12' -37.9(2) . . . . ?
B10' B9' B12' B7' 100.9(2) . . . . ?
B10' B9' B12' B8' 138.3(2) . . . . ?
B10' B9' B12' B11' 37.0(2) . . . . ?
B10' B11' B12' B7' -137.9(2) . . . . ?
B10' B11' B12' B8' -100.5(2) . . . . ?
B10' B11' B12' B9' -37.2(2) . . . . ?
B11' C2' B3' C1' -102.5(2) . . . . ?
B11' C2' B3' B4' -65.2(3) . . . . ?
B11' C2' B3' B7' 37.6(2) . . . . ?
B11' C2' B3' B8' -1.7(3) . . . . ?
B11' C2' B6' C1' 139.0(2) . . . . ?
B11' C2' B6' B5' 101.3(2) . . . . ?
B11' C2' B6' B10' 39.1(2) . . . . ?
B11' C2' B7' B3' -140.4(2) . . . . ?
B11' C2' B7' B8' -101.7(2) . . . . ?
B11' C2' B7' B12' -38.8(2) . . . . ?
B11' B6' B10' B5' 136.2(2) . . . . ?
B11' B6' B10' B9' 100.5(3) . . . . ?
B11' B6' B10' B12' 37.5(2) . . . . ?
B11' B7' B8' B3' -100.4(2) . . . . ?
B11' B7' B8' B4' -63.3(3) . . . . ?
B11' B7' B8' B9' 0.0(3) . . . . ?
B11' B7' B8' B12' 37.3(2) . . . . ?
B11' B7' B12' B8' -138.0(2) . . . . ?
B11' B7' B12' B9' -100.6(2) . . . . ?
B11' B7' B12' B10' -37.4(2) . . . . ?
B11' B10' B12' B7' 37.8(2) . . . . ?
B11' B10' B12' B8' 101.0(2) . . . . ?
B11' B10' B12' B9' 138.2(2) . . . . ?
B12' B7' B8' B3' -137.7(2) . . . . ?
B12' B7' B8' B4' -100.6(2) . . . . ?
B12' B7' B8' B9' -37.3(2) . . . . ?
B12' B7' B11' C2' 135.5(2) . . . . ?
B12' B7' B11' B6' 101.0(3) . . . . ?
B12' B7' B11' B10' 38.0(2) . . . . ?
B12' B8' B9' B4' -138.3(2) . . . . ?
B12' B8' B9' B5' -100.6(3) . . . . ?
B12' B8' B9' B10' -37.7(2) . . . . ?
B12' B9' B10' B5' -136.7(2) . . . . ?
B12' B9' B10' B6' -100.9(3) . . . . ?
B12' B9' B10' B11' -37.2(2) . . . . ?
B12' B10' B11' C2' -99.3(2) . . . . ?
B12' B10' B11' B6' -138.0(2) . . . . ?
B12' B10' B11' B7' -37.6(2) . . . . ?

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_4583
_database_code_depnum_ccdc_archive 'CCDC 1042153'
_audit_update_record             
;
2015-01-05 deposited with the CCDC.
2015-02-09 downloaded from the CCDC.
;
_audit_creation_date             2014-12-10
_audit_creation_method           
;
Olex2 1.2
(compiled 2013.12.10 svn.r2850 for OlexSys, GUI svn.r4736)
;
_shelxl_version_number           2014/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C14 H35 B19 Ru'
_chemical_formula_sum            'C14 H35 B19 Ru'
_chemical_formula_weight         509.88
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   10.9051(9)
_cell_length_b                   16.9528(14)
_cell_length_c                   13.8437(11)
_cell_angle_alpha                90
_cell_angle_beta                 105.039(4)
_cell_angle_gamma                90
_cell_volume                     2471.7(4)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9935
_cell_measurement_temperature    100.0(2)
_cell_measurement_theta_max      31.901
_cell_measurement_theta_min      2.845
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    0.639
_exptl_absorpt_correction_T_max  0.7466
_exptl_absorpt_correction_T_min  0.6969
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.0618 before and 0.0487 after correction.
The Ratio of minimum to maximum transmission is 0.9334.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.370
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1032
_exptl_crystal_size_max          0.56
_exptl_crystal_size_mid          0.42
_exptl_crystal_size_min          0.36
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0388
_diffrn_reflns_av_unetI/netI     0.0336
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.989
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            52456
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.989
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         33.530
_diffrn_reflns_theta_min         1.940
_diffrn_ambient_temperature      100.0(2)
_diffrn_detector_area_resol_mean 8
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'sealed tube'
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                7975
_reflns_number_total             9614
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         0.956
_refine_diff_density_min         -1.368
_refine_diff_density_rms         0.075
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.031
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     374
_refine_ls_number_reflns         9614
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0392
_refine_ls_R_factor_gt           0.0288
_refine_ls_restrained_S_all      1.031
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0288P)²+0.8417P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0639
_refine_ls_wR_factor_ref         0.0680
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Shared sites
{C3', B3'}
{B2', C2'}
3. Uiso/Uaniso restraints and constraints
Uanis(C3') = Uanis(B3')
Uanis(B2') = Uanis(C2')
4. Others
 Sof(B3')=Sof(C2')=1-FVAR(1)
 Sof(C3')=Sof(B2')=FVAR(1)
5.a Ternary CH refined with riding coordinates:
 C21(H21), C22(H22), C24(H24), C25(H25), C27(H27)
5.b Idealised Me refined as rotating group:
 C26(H26A,H26B,H26C), C28(H28A,H28B,H28C), C29(H29A,H29B,H29C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C -0.19819(13) -0.24169(8) -0.47864(10) 0.0188(2) Uani 1 1 d . . . . .
H1 H -0.1632(16) -0.1902(11) -0.4832(12) 0.023 Uiso 1 1 d R . . . .
Ru2 Ru -0.39170(2) -0.23548(2) -0.46496(2) 0.01662(3) Uani 1 1 d . . . . .
B3 B -0.31010(13) -0.27948(8) -0.57985(11) 0.0172(3) Uani 1 1 d . . . . .
H3 H -0.3369(17) -0.2534(10) -0.6530(13) 0.021 Uiso 1 1 d R . . . .
B4 B -0.14572(13) -0.31072(9) -0.54694(11) 0.0179(3) Uani 1 1 d . . . . .
H4 H -0.0926(15) -0.2985(10) -0.5980(12) 0.021 Uiso 1 1 d R . . . .
B5 B -0.08692(15) -0.30853(10) -0.41588(12) 0.0218(3) Uani 1 1 d . . . . .
H5 H 0.0107(16) -0.2906(11) -0.3831(13) 0.026 Uiso 1 1 d R . . . .
B6 B -0.21445(15) -0.27690(9) -0.36474(12) 0.0211(3) Uani 1 1 d . . . . .
H6 H -0.1815(18) -0.2432(10) -0.2984(14) 0.025 Uiso 1 1 d R . . . .
B7 B -0.39861(14) -0.35360(9) -0.52830(11) 0.0173(3) Uani 1 1 d . . . . .
H7 H -0.4867(16) -0.3785(10) -0.5736(12) 0.021 Uiso 1 1 d R . . . .
C8 C -0.26535(11) -0.37864(7) -0.57186(9) 0.0152(2) Uani 1 1 d . . . . .
B9 B -0.12992(14) -0.39913(9) -0.47659(11) 0.0198(3) Uani 1 1 d . . . . .
H9 H -0.0630(16) -0.4431(10) -0.4883(12) 0.024 Uiso 1 1 d R . . . .
B10 B -0.17326(15) -0.37889(10) -0.36480(11) 0.0222(3) Uani 1 1 d . . . . .
H10 H -0.1278(16) -0.4103(11) -0.2970(12) 0.027 Uiso 1 1 d R . . . .
B11 B -0.33813(15) -0.35173(9) -0.39478(12) 0.0208(3) Uani 1 1 d . . . . .
H11 H -0.3938(16) -0.3735(10) -0.3454(12) 0.025 Uiso 1 1 d R . . . .
B12 B -0.28421(15) -0.42493(9) -0.46556(11) 0.0191(3) Uani 1 1 d . . . . .
H12 H -0.3083(16) -0.4860(10) -0.4681(12) 0.023 Uiso 1 1 d R . . . .
C20 C -0.40262(14) -0.11302(9) -0.40158(14) 0.0317(3) Uani 1 1 d . . . . .
C21 C -0.46328(14) -0.16814(9) -0.35222(11) 0.0258(3) Uani 1 1 d . . . . .
H21 H -0.4263 -0.1789 -0.2794 0.031 Uiso 1 1 calc R . . . .
C22 C -0.56144(13) -0.21719(8) -0.40747(10) 0.0200(2) Uani 1 1 d . . . . .
H22 H -0.5925 -0.2617 -0.3726 0.024 Uiso 1 1 calc R . . . .
C23 C -0.60313(12) -0.21201(8) -0.51289(10) 0.0186(2) Uani 1 1 d . . . . .
C24 C -0.54025(14) -0.15764(8) -0.56223(11) 0.0240(3) Uani 1 1 d . . . . .
H24 H -0.5555 -0.1607 -0.6365 0.029 Uiso 1 1 calc R . . . .
C25 C -0.44231(15) -0.10934(9) -0.50744(14) 0.0303(3) Uani 1 1 d . . . . .
H25 H -0.3894 -0.0792 -0.5439 0.036 Uiso 1 1 calc R . . . .
C26 C -0.29715(18) -0.06123(12) -0.34400(19) 0.0531(6) Uani 1 1 d . . . . .
H26A H -0.3319 -0.0100 -0.3317 0.080 Uiso 1 1 calc GR . . . .
H26B H -0.2345 -0.0536 -0.3827 0.080 Uiso 1 1 calc GR . . . .
H26C H -0.2562 -0.0863 -0.2800 0.080 Uiso 1 1 calc GR . . . .
C27 C -0.71372(14) -0.25910(9) -0.57497(11) 0.0240(3) Uani 1 1 d . . . . .
H27 H -0.6892 -0.2796 -0.6351 0.029 Uiso 1 1 calc R . . . .
C28 C -0.75094(15) -0.32916(9) -0.51999(13) 0.0318(3) Uani 1 1 d . . . . .
H28A H -0.7855 -0.3102 -0.4656 0.048 Uiso 1 1 calc GR . . . .
H28B H -0.6759 -0.3619 -0.4923 0.048 Uiso 1 1 calc GR . . . .
H28C H -0.8154 -0.3606 -0.5667 0.048 Uiso 1 1 calc GR . . . .
C29 C -0.82584(15) -0.20221(11) -0.61113(13) 0.0345(4) Uani 1 1 d . . . . .
H29A H -0.8018 -0.1603 -0.6514 0.052 Uiso 1 1 calc GR . . . .
H29B H -0.8483 -0.1789 -0.5532 0.052 Uiso 1 1 calc GR . . . .
H29C H -0.8990 -0.2311 -0.6518 0.052 Uiso 1 1 calc GR . . . .
C1' C -0.28482(12) -0.42523(7) -0.66928(9) 0.0164(2) Uani 1 1 d . . . . .
C3' C -0.39482(15) -0.49762(9) -0.69079(11) 0.0233(3) Uani 0.554(19) 1 d . . P
A 1
H3' H -0.4405(17) -0.5063(11) -0.6361(13) 0.028 Uiso 1 1 d R . . B 1
B2' B -0.23755(15) -0.52118(9) -0.66132(12) 0.0229(3) Uani 0.554(19) 1 d . . P
A 1
H2' H -0.1964(17) -0.5430(11) -0.5878(13) 0.027 Uiso 1 1 d R . . C 1
B3' B -0.39482(15) -0.49762(9) -0.69079(11) 0.0233(3) Uani 0.446(19) 1 d . . P
A 2
C2' C -0.23755(15) -0.52118(9) -0.66132(12) 0.0229(3) Uani 0.446(19) 1 d . . P
A 2
B6' B -0.15649(14) -0.45159(9) -0.71472(11) 0.0187(3) Uani 1 1 d . . . . .
H6' H -0.0664(16) -0.4330(10) -0.6747(12) 0.022 Uiso 1 1 d R . . . .
B5' B -0.27275(14) -0.38322(9) -0.77973(11) 0.0181(3) Uani 1 1 d . . . . .
H5' H -0.2492(15) -0.3212(10) -0.7783(12) 0.022 Uiso 1 1 d R . . . .
B4' B -0.42284(14) -0.41191(9) -0.76330(11) 0.0193(3) Uani 1 1 d . . . . .
H4' H -0.4868(16) -0.3688(10) -0.7499(12) 0.023 Uiso 1 1 d R . . . .
B11' B -0.19446(14) -0.54636(9) -0.76935(12) 0.0211(3) Uani 1 1 d . . . . .
H11' H -0.1195(16) -0.5905(11) -0.7666(12) 0.025 Uiso 1 1 d R . . . .
B7' B -0.34462(15) -0.57508(9) -0.75266(12) 0.0213(3) Uani 1 1 d . . . . .
H7' H -0.3655(16) -0.6337(11) -0.7332(12) 0.026 Uiso 1 1 d R . . . .
B8' B -0.46080(15) -0.50692(10) -0.81817(12) 0.0227(3) Uani 1 1 d . . . . .
H8' H -0.5547(17) -0.5242(11) -0.8420(12) 0.027 Uiso 1 1 d R . . . .
B9' B -0.38294(15) -0.43532(10) -0.87553(12) 0.0225(3) Uani 1 1 d . . . . .
H9' H -0.4333(16) -0.4045(11) -0.9444(12) 0.027 Uiso 1 1 d R . . . .
B10' B -0.21843(15) -0.46014(9) -0.84580(12) 0.0211(3) Uani 1 1 d . . . . .
H10' H -0.1597(16) -0.4489(10) -0.8933(12) 0.025 Uiso 1 1 d R . . . .
B12' B -0.33433(15) -0.53630(9) -0.86963(12) 0.0211(3) Uani 1 1 d . . . . .
H12' H -0.3486(16) -0.5729(11) -0.9344(13) 0.025 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 H1 0.961(18) . ?
C1 Ru2 2.1696(13) . ?
C1 B3 1.725(2) . ?
C1 B4 1.695(2) . ?
C1 B5 1.722(2) . ?
C1 B6 1.738(2) . ?
Ru2 B3 2.1477(15) . ?
Ru2 B6 2.1823(16) . ?
Ru2 B7 2.1796(15) . ?
Ru2 B11 2.2078(16) . ?
Ru2 C20 2.2688(15) . ?
Ru2 C21 2.2317(14) . ?
Ru2 C22 2.2182(13) . ?
Ru2 C23 2.2629(13) . ?
Ru2 C24 2.2465(14) . ?
Ru2 C25 2.2483(15) . ?
B3 H3 1.074(17) . ?
B3 B4 1.810(2) . ?
B3 B7 1.838(2) . ?
B3 C8 1.7458(19) . ?
B4 H4 1.045(16) . ?
B4 B5 1.761(2) . ?
B4 C8 1.7068(19) . ?
B4 B9 1.771(2) . ?
B5 H5 1.086(17) . ?
B5 B6 1.798(2) . ?
B5 B9 1.755(2) . ?
B5 B10 1.776(2) . ?
B6 H6 1.063(18) . ?
B6 B10 1.787(2) . ?
B6 B11 1.819(2) . ?
B7 H7 1.087(16) . ?
B7 C8 1.7636(19) . ?
B7 B11 1.794(2) . ?
B7 B12 1.792(2) . ?
C8 B9 1.7409(19) . ?
C8 B12 1.7265(19) . ?
C8 C1' 1.5294(17) . ?
B9 H9 1.084(17) . ?
B9 B10 1.765(2) . ?
B9 B12 1.783(2) . ?
B10 H10 1.081(17) . ?
B10 B11 1.797(2) . ?
B10 B12 1.773(2) . ?
B11 H11 1.090(17) . ?
B11 B12 1.773(2) . ?
B12 H12 1.066(17) . ?
C20 C21 1.418(2) . ?
C20 C25 1.418(3) . ?
C20 C26 1.501(2) . ?
C21 H21 1.0000 . ?
C21 C22 1.413(2) . ?
C22 H22 1.0000 . ?
C22 C23 1.4142(19) . ?
C23 C24 1.4246(19) . ?
C23 C27 1.514(2) . ?
C24 H24 1.0000 . ?
C24 C25 1.402(2) . ?
C25 H25 1.0000 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 H27 1.0000 . ?
C27 C28 1.522(2) . ?
C27 C29 1.536(2) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C1' C3' 1.6878(19) . ?
C1' B2' 1.701(2) . ?
C1' B3' 1.6878(19) . ?
C1' C2' 1.701(2) . ?
C1' B6' 1.7352(19) . ?
C1' B5' 1.7225(19) . ?
C1' B4' 1.7303(19) . ?
C3' H3' 1.020(18) . ?
C3' B2' 1.704(2) . ?
C3' B4' 1.747(2) . ?
C3' B7' 1.732(2) . ?
C3' B8' 1.730(2) . ?
B2' H2' 1.066(18) . ?
B2' B6' 1.749(2) . ?
B2' B11' 1.733(2) . ?
B2' B7' 1.741(2) . ?
B3' C2' 1.704(2) . ?
B3' B4' 1.747(2) . ?
B3' B7' 1.732(2) . ?
B3' B8' 1.730(2) . ?
C2' B6' 1.749(2) . ?
C2' B11' 1.733(2) . ?
C2' B7' 1.741(2) . ?
B6' H6' 1.043(17) . ?
B6' B5' 1.780(2) . ?
B6' B11' 1.778(2) . ?
B6' B10' 1.770(2) . ?
B5' H5' 1.082(17) . ?
B5' B4' 1.778(2) . ?
B5' B9' 1.776(2) . ?
B5' B10' 1.780(2) . ?
B4' H4' 1.059(17) . ?
B4' B8' 1.783(2) . ?
B4' B9' 1.764(2) . ?
B11' H11' 1.102(17) . ?
B11' B7' 1.780(2) . ?
B11' B10' 1.784(2) . ?
B11' B12' 1.784(2) . ?
B7' H7' 1.070(18) . ?
B7' B8' 1.779(2) . ?
B7' B12' 1.778(2) . ?
B8' H8' 1.033(18) . ?
B8' B9' 1.782(2) . ?
B8' B12' 1.780(2) . ?
B9' H9' 1.101(17) . ?
B9' B10' 1.784(2) . ?
B9' B12' 1.788(2) . ?
B10' H10' 1.047(17) . ?
B10' B12' 1.777(2) . ?
B12' H12' 1.068(17) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ru2 C1 H1 111.9(10) . . ?
B3 C1 H1 119.5(10) . . ?
B3 C1 Ru2 65.78(7) . . ?
B3 C1 B6 113.09(10) . . ?
B4 C1 H1 113.1(10) . . ?
B4 C1 Ru2 124.00(9) . . ?
B4 C1 B3 63.93(8) . . ?
B4 C1 B5 62.05(9) . . ?
B4 C1 B6 113.44(11) . . ?
B5 C1 H1 113.0(10) . . ?
B5 C1 Ru2 124.20(9) . . ?
B5 C1 B3 115.02(10) . . ?
B5 C1 B6 62.64(9) . . ?
B6 C1 H1 120.5(10) . . ?
B6 C1 Ru2 66.85(7) . . ?
C1 Ru2 B6 47.06(6) . . ?
C1 Ru2 B7 81.55(5) . . ?
C1 Ru2 B11 80.95(6) . . ?
C1 Ru2 C20 103.18(5) . . ?
C1 Ru2 C21 127.63(5) . . ?
C1 Ru2 C22 163.57(5) . . ?
C1 Ru2 C23 157.37(5) . . ?
C1 Ru2 C24 122.86(5) . . ?
C1 Ru2 C25 101.64(5) . . ?
B3 Ru2 C1 47.10(5) . . ?
B3 Ru2 B6 83.70(6) . . ?
B3 Ru2 B7 50.25(5) . . ?
B3 Ru2 B11 84.41(6) . . ?
B3 Ru2 C20 132.66(6) . . ?
B3 Ru2 C21 169.39(6) . . ?
B3 Ru2 C22 149.19(5) . . ?
B3 Ru2 C23 115.49(5) . . ?
B3 Ru2 C24 97.64(5) . . ?
B3 Ru2 C25 104.92(6) . . ?
B6 Ru2 B11 48.96(6) . . ?
B6 Ru2 C20 100.10(6) . . ?
B6 Ru2 C21 97.63(6) . . ?
B6 Ru2 C22 120.05(5) . . ?
B6 Ru2 C23 155.50(5) . . ?
B6 Ru2 C24 162.19(6) . . ?
B6 Ru2 C25 126.10(6) . . ?
B7 Ru2 B6 83.83(6) . . ?
B7 Ru2 B11 48.28(6) . . ?
B7 Ru2 C20 175.16(5) . . ?
B7 Ru2 C21 140.31(6) . . ?
B7 Ru2 C22 109.13(5) . . ?
B7 Ru2 C23 96.74(5) . . ?
B7 Ru2 C24 110.75(6) . . ?
B7 Ru2 C25 142.01(6) . . ?
B11 Ru2 C20 132.92(6) . . ?
B11 Ru2 C21 104.45(6) . . ?
B11 Ru2 C22 96.72(5) . . ?
B11 Ru2 C23 114.78(5) . . ?
B11 Ru2 C24 148.80(6) . . ?
B11 Ru2 C25 169.44(6) . . ?
C21 Ru2 C20 36.73(6) . . ?
C21 Ru2 C23 66.45(5) . . ?
C21 Ru2 C24 77.88(5) . . ?
C21 Ru2 C25 65.78(6) . . ?
C22 Ru2 C20 66.48(5) . . ?
C22 Ru2 C21 37.04(5) . . ?
C22 Ru2 C23 36.78(5) . . ?
C22 Ru2 C24 66.04(5) . . ?
C22 Ru2 C25 77.87(5) . . ?
C23 Ru2 C20 78.51(5) . . ?
C24 Ru2 C20 65.94(6) . . ?
C24 Ru2 C23 36.83(5) . . ?
C24 Ru2 C25 36.36(6) . . ?
C25 Ru2 C20 36.58(7) . . ?
C25 Ru2 C23 66.03(5) . . ?
C1 B3 Ru2 67.12(7) . . ?
C1 B3 H3 125.1(9) . . ?
C1 B3 B4 57.22(8) . . ?
C1 B3 B7 105.71(10) . . ?
C1 B3 C8 100.31(9) . . ?
Ru2 B3 H3 119.5(9) . . ?
B4 B3 Ru2 119.26(9) . . ?
B4 B3 H3 111.5(10) . . ?
B4 B3 B7 106.73(10) . . ?
B7 B3 Ru2 65.78(7) . . ?
B7 B3 H3 127.3(9) . . ?
C8 B3 Ru2 116.76(9) . . ?
C8 B3 H3 117.4(9) . . ?
C8 B3 B4 57.33(7) . . ?
C8 B3 B7 58.90(8) . . ?
C1 B4 B3 58.85(8) . . ?
C1 B4 H4 124.6(10) . . ?
C1 B4 B5 59.73(8) . . ?
C1 B4 C8 103.15(10) . . ?
C1 B4 B9 106.04(10) . . ?
B3 B4 H4 117.3(9) . . ?
B5 B4 B3 108.98(10) . . ?
B5 B4 H4 125.1(9) . . ?
B5 B4 B9 59.59(9) . . ?
C8 B4 B3 59.43(8) . . ?
C8 B4 H4 121.7(9) . . ?
C8 B4 B5 106.11(11) . . ?
C8 B4 B9 60.04(8) . . ?
B9 B4 B3 109.55(10) . . ?
B9 B4 H4 123.2(10) . . ?
C1 B5 B4 58.22(8) . . ?
C1 B5 H5 120.8(10) . . ?
C1 B5 B6 59.11(8) . . ?
C1 B5 B9 105.58(10) . . ?
C1 B5 B10 105.42(11) . . ?
B4 B5 H5 119.5(9) . . ?
B4 B5 B6 107.45(10) . . ?
B4 B5 B10 107.89(11) . . ?
B6 B5 H5 121.7(9) . . ?
B9 B5 B4 60.50(9) . . ?
B9 B5 H5 123.8(10) . . ?
B9 B5 B6 108.16(11) . . ?
B9 B5 B10 59.98(9) . . ?
B10 B5 H5 125.7(9) . . ?
B10 B5 B6 59.97(9) . . ?
C1 B6 Ru2 66.09(7) . . ?
C1 B6 B5 58.25(8) . . ?
C1 B6 H6 120.6(10) . . ?
C1 B6 B10 104.32(10) . . ?
C1 B6 B11 106.03(10) . . ?
Ru2 B6 H6 114.9(10) . . ?
B5 B6 Ru2 119.58(9) . . ?
B5 B6 H6 112.2(10) . . ?
B5 B6 B11 107.77(11) . . ?
B10 B6 Ru2 119.51(9) . . ?
B10 B6 B5 59.41(9) . . ?
B10 B6 H6 119.5(10) . . ?
B10 B6 B11 59.78(9) . . ?
B11 B6 Ru2 66.25(7) . . ?
B11 B6 H6 129.6(10) . . ?
Ru2 B7 H7 121.5(9) . . ?
B3 B7 Ru2 63.97(6) . . ?
B3 B7 H7 121.1(9) . . ?
C8 B7 Ru2 114.40(8) . . ?
C8 B7 B3 57.95(7) . . ?
C8 B7 H7 113.1(9) . . ?
C8 B7 B11 103.96(10) . . ?
C8 B7 B12 58.10(8) . . ?
B11 B7 Ru2 66.68(7) . . ?
B11 B7 B3 107.35(10) . . ?
B11 B7 H7 129.4(9) . . ?
B12 B7 Ru2 118.55(9) . . ?
B12 B7 B3 106.25(10) . . ?
B12 B7 H7 114.7(9) . . ?
B12 B7 B11 59.27(8) . . ?
B3 C8 B7 63.15(8) . . ?
B4 C8 B3 63.24(8) . . ?
B4 C8 B7 115.02(10) . . ?
B4 C8 B9 61.82(8) . . ?
B4 C8 B12 112.84(10) . . ?
B9 C8 B3 114.10(10) . . ?
B9 C8 B7 113.66(10) . . ?
B12 C8 B3 113.48(10) . . ?
B12 C8 B7 61.77(8) . . ?
B12 C8 B9 61.89(8) . . ?
C1' C8 B3 117.96(10) . . ?
C1' C8 B4 116.78(10) . . ?
C1' C8 B7 119.18(10) . . ?
C1' C8 B9 117.48(10) . . ?
C1' C8 B12 119.79(10) . . ?
B4 B9 H9 118.2(9) . . ?
B4 B9 B12 107.18(10) . . ?
B5 B9 B4 59.91(9) . . ?
B5 B9 H9 124.5(9) . . ?
B5 B9 B10 60.61(9) . . ?
B5 B9 B12 108.33(11) . . ?
C8 B9 B4 58.14(8) . . ?
C8 B9 B5 104.89(10) . . ?
C8 B9 H9 119.7(9) . . ?
C8 B9 B10 104.95(10) . . ?
C8 B9 B12 58.66(8) . . ?
B10 B9 B4 107.92(11) . . ?
B10 B9 H9 127.5(9) . . ?
B10 B9 B12 59.95(9) . . ?
B12 B9 H9 122.1(9) . . ?
B5 B10 B6 60.63(9) . . ?
B5 B10 H10 120.4(9) . . ?
B5 B10 B11 109.74(11) . . ?
B6 B10 H10 122.4(9) . . ?
B6 B10 B11 61.02(9) . . ?
B9 B10 B5 59.42(9) . . ?
B9 B10 B6 108.24(11) . . ?
B9 B10 H10 119.9(9) . . ?
B9 B10 B11 109.07(10) . . ?
B9 B10 B12 60.52(9) . . ?
B11 B10 H10 122.2(9) . . ?
B12 B10 B5 107.84(11) . . ?
B12 B10 B6 107.82(11) . . ?
B12 B10 H10 122.1(10) . . ?
B12 B10 B11 59.56(9) . . ?
Ru2 B11 H11 116.8(9) . . ?
B6 B11 Ru2 64.79(7) . . ?
B6 B11 H11 126.4(9) . . ?
B7 B11 Ru2 65.04(7) . . ?
B7 B11 B6 107.48(10) . . ?
B7 B11 B10 108.16(11) . . ?
B7 B11 H11 121.6(9) . . ?
B10 B11 Ru2 117.71(9) . . ?
B10 B11 B6 59.20(9) . . ?
B10 B11 H11 117.1(9) . . ?
B12 B11 Ru2 117.99(9) . . ?
B12 B11 B6 106.37(11) . . ?
B12 B11 B7 60.29(8) . . ?
B12 B11 B10 59.54(9) . . ?
B12 B11 H11 115.3(9) . . ?
B7 B12 H12 120.3(9) . . ?
C8 B12 B7 60.13(8) . . ?
C8 B12 B9 59.45(8) . . ?
C8 B12 B10 105.23(11) . . ?
C8 B12 B11 106.43(10) . . ?
C8 B12 H12 119.7(9) . . ?
B9 B12 B7 110.29(10) . . ?
B9 B12 H12 117.7(9) . . ?
B10 B12 B7 109.36(11) . . ?
B10 B12 B9 59.52(9) . . ?
B10 B12 B11 60.90(9) . . ?
B10 B12 H12 124.4(9) . . ?
B11 B12 B7 60.44(9) . . ?
B11 B12 B9 109.34(11) . . ?
B11 B12 H12 125.7(9) . . ?
C21 C20 Ru2 70.21(8) . . ?
C21 C20 C26 121.21(17) . . ?
C25 C20 Ru2 70.92(8) . . ?
C25 C20 C21 118.14(14) . . ?
C25 C20 C26 120.63(17) . . ?
C26 C20 Ru2 129.10(11) . . ?
Ru2 C21 H21 119.3 . . ?
C20 C21 Ru2 73.06(8) . . ?
C20 C21 H21 119.3 . . ?
C22 C21 Ru2 70.97(8) . . ?
C22 C21 C20 120.61(14) . . ?
C22 C21 H21 119.3 . . ?
Ru2 C22 H22 119.1 . . ?
C21 C22 Ru2 72.00(8) . . ?
C21 C22 H22 119.1 . . ?
C21 C22 C23 121.16(13) . . ?
C23 C22 Ru2 73.33(7) . . ?
C23 C22 H22 119.1 . . ?
C22 C23 Ru2 69.89(7) . . ?
C22 C23 C24 117.98(13) . . ?
C22 C23 C27 123.26(12) . . ?
C24 C23 Ru2 70.96(8) . . ?
C24 C23 C27 118.72(12) . . ?
C27 C23 Ru2 132.43(10) . . ?
Ru2 C24 H24 119.1 . . ?
C23 C24 Ru2 72.21(8) . . ?
C23 C24 H24 119.1 . . ?
C25 C24 Ru2 71.89(9) . . ?
C25 C24 C23 120.82(14) . . ?
C25 C24 H24 119.1 . . ?
Ru2 C25 H25 118.9 . . ?
C20 C25 Ru2 72.50(9) . . ?
C20 C25 H25 118.9 . . ?
C24 C25 Ru2 71.75(8) . . ?
C24 C25 C20 121.25(14) . . ?
C24 C25 H25 118.9 . . ?
C20 C26 H26A 109.5 . . ?
C20 C26 H26B 109.5 . . ?
C20 C26 H26C 109.5 . . ?
H26A C26 H26B 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C23 C27 H27 108.0 . . ?
C23 C27 C28 113.84(12) . . ?
C23 C27 C29 107.67(12) . . ?
C28 C27 H27 108.0 . . ?
C28 C27 C29 111.11(13) . . ?
C29 C27 H27 108.0 . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28B 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29B 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C8 C1' C3' 117.44(10) . . ?
C8 C1' B2' 117.79(10) . . ?
C8 C1' B3' 117.44(10) . . ?
C8 C1' C2' 117.79(10) . . ?
C8 C1' B6' 120.81(10) . . ?
C8 C1' B5' 122.97(10) . . ?
C8 C1' B4' 119.38(10) . . ?
C3' C1' B2' 60.37(9) . . ?
C3' C1' B6' 110.60(10) . . ?
C3' C1' B5' 111.01(10) . . ?
C3' C1' B4' 61.48(8) . . ?
B2' C1' B6' 61.18(8) . . ?
B2' C1' B5' 111.17(10) . . ?
B2' C1' B4' 111.30(10) . . ?
B3' C1' C2' 60.37(9) . . ?
B3' C1' B6' 110.60(10) . . ?
B3' C1' B5' 111.01(10) . . ?
B3' C1' B4' 61.48(8) . . ?
C2' C1' B6' 61.18(8) . . ?
C2' C1' B5' 111.17(10) . . ?
C2' C1' B4' 111.30(10) . . ?
B5' C1' B6' 61.97(8) . . ?
B5' C1' B4' 61.98(8) . . ?
B4' C1' B6' 112.76(10) . . ?
C1' C3' H3' 115.9(10) . . ?
C1' C3' B2' 60.21(9) . . ?
C1' C3' B4' 60.46(8) . . ?
C1' C3' B7' 109.70(11) . . ?
C1' C3' B8' 109.55(11) . . ?
B2' C3' H3' 116.3(10) . . ?
B2' C3' B4' 110.34(11) . . ?
B2' C3' B7' 60.87(9) . . ?
B2' C3' B8' 110.44(12) . . ?
B4' C3' H3' 120.1(10) . . ?
B7' C3' H3' 122.4(10) . . ?
B7' C3' B4' 112.15(11) . . ?
B8' C3' H3' 126.1(10) . . ?
B8' C3' B4' 61.69(9) . . ?
B8' C3' B7' 61.85(9) . . ?
C1' B2' C3' 59.42(8) . . ?
C1' B2' H2' 116.0(10) . . ?
C1' B2' B6' 60.36(8) . . ?
C1' B2' B11' 108.96(11) . . ?
C1' B2' B7' 108.66(11) . . ?
C3' B2' H2' 117.2(9) . . ?
C3' B2' B6' 109.17(11) . . ?
C3' B2' B11' 109.41(11) . . ?
C3' B2' B7' 60.36(9) . . ?
B6' B2' H2' 120.2(10) . . ?
B11' B2' H2' 126.7(10) . . ?
B11' B2' B6' 61.41(9) . . ?
B11' B2' B7' 61.64(9) . . ?
B7' B2' H2' 123.3(10) . . ?
B7' B2' B6' 111.36(11) . . ?
C1' B3' C2' 60.21(9) . . ?
C1' B3' B4' 60.46(8) . . ?
C1' B3' B7' 109.70(11) . . ?
C1' B3' B8' 109.55(11) . . ?
C2' B3' B4' 110.34(11) . . ?
C2' B3' B7' 60.87(9) . . ?
C2' B3' B8' 110.44(12) . . ?
B7' B3' B4' 112.15(11) . . ?
B8' B3' B4' 61.69(9) . . ?
B8' B3' B7' 61.85(9) . . ?
C1' C2' B3' 59.42(8) . . ?
C1' C2' B6' 60.36(8) . . ?
C1' C2' B11' 108.96(11) . . ?
C1' C2' B7' 108.66(11) . . ?
B3' C2' B6' 109.17(11) . . ?
B3' C2' B11' 109.41(11) . . ?
B3' C2' B7' 60.36(9) . . ?
B11' C2' B6' 61.41(9) . . ?
B11' C2' B7' 61.64(9) . . ?
B7' C2' B6' 111.36(11) . . ?
C1' B6' B2' 58.45(8) . . ?
C1' B6' C2' 58.45(8) . . ?
C1' B6' H6' 117.8(9) . . ?
C1' B6' B5' 58.67(8) . . ?
C1' B6' B11' 105.44(10) . . ?
C1' B6' B10' 105.28(10) . . ?
B2' B6' H6' 119.2(9) . . ?
B2' B6' B5' 106.33(10) . . ?
B2' B6' B11' 58.86(9) . . ?
B2' B6' B10' 106.13(11) . . ?
C2' B6' H6' 119.2(9) . . ?
C2' B6' B5' 106.33(10) . . ?
C2' B6' B11' 58.86(9) . . ?
C2' B6' B10' 106.13(11) . . ?
B5' B6' H6' 121.4(10) . . ?
B11' B6' H6' 125.6(10) . . ?
B11' B6' B5' 108.45(10) . . ?
B10' B6' H6' 128.7(9) . . ?
B10' B6' B5' 60.18(9) . . ?
B10' B6' B11' 60.35(9) . . ?
C1' B5' B6' 59.37(8) . . ?
C1' B5' H5' 117.3(9) . . ?
C1' B5' B4' 59.22(8) . . ?
C1' B5' B9' 105.34(10) . . ?
C1' B5' B10' 105.40(10) . . ?
B6' B5' H5' 119.3(9) . . ?
B6' B5' B10' 59.64(9) . . ?
B4' B5' B6' 108.41(10) . . ?
B4' B5' H5' 119.1(9) . . ?
B4' B5' B10' 107.79(11) . . ?
B9' B5' B6' 107.99(11) . . ?
B9' B5' H5' 127.5(9) . . ?
B9' B5' B4' 59.51(9) . . ?
B9' B5' B10' 60.20(9) . . ?
B10' B5' H5' 127.8(9) . . ?
C1' B4' C3' 58.06(8) . . ?
C1' B4' B3' 58.06(8) . . ?
C1' B4' B5' 58.80(8) . . ?
C1' B4' H4' 116.2(9) . . ?
C1' B4' B8' 105.25(10) . . ?
C1' B4' B9' 105.54(10) . . ?
C3' B4' B5' 105.75(11) . . ?
C3' B4' H4' 119.8(9) . . ?
C3' B4' B8' 58.68(9) . . ?
C3' B4' B9' 105.81(11) . . ?
B3' B4' B5' 105.75(11) . . ?
B3' B4' H4' 119.8(9) . . ?
B3' B4' B8' 58.68(9) . . ?
B3' B4' B9' 105.81(11) . . ?
B5' B4' H4' 120.3(9) . . ?
B5' B4' B8' 108.19(11) . . ?
B8' B4' H4' 127.4(9) . . ?
B9' B4' B5' 60.20(9) . . ?
B9' B4' H4' 129.3(9) . . ?
B9' B4' B8' 60.31(9) . . ?
B2' B11' B6' 59.73(9) . . ?
B2' B11' H11' 120.2(9) . . ?
B2' B11' B7' 59.39(9) . . ?
B2' B11' B10' 106.22(11) . . ?
B2' B11' B12' 106.22(11) . . ?
C2' B11' B6' 59.73(9) . . ?
C2' B11' H11' 120.2(9) . . ?
C2' B11' B7' 59.39(9) . . ?
C2' B11' B10' 106.22(11) . . ?
C2' B11' B12' 106.22(11) . . ?
B6' B11' H11' 120.7(9) . . ?
B6' B11' B7' 108.21(11) . . ?
B6' B11' B10' 59.60(9) . . ?
B6' B11' B12' 107.59(11) . . ?
B7' B11' H11' 120.6(9) . . ?
B7' B11' B10' 107.64(11) . . ?
B7' B11' B12' 59.85(9) . . ?
B10' B11' H11' 124.8(9) . . ?
B10' B11' B12' 59.73(9) . . ?
B12' B11' H11' 124.7(9) . . ?
C3' B7' B2' 58.77(9) . . ?
C3' B7' B11' 106.03(11) . . ?
C3' B7' H7' 117.7(9) . . ?
C3' B7' B8' 59.02(9) . . ?
C3' B7' B12' 105.82(11) . . ?
B2' B7' B11' 58.97(9) . . ?
B2' B7' H7' 116.9(9) . . ?
B2' B7' B8' 106.50(11) . . ?
B2' B7' B12' 106.17(11) . . ?
B3' B7' C2' 58.77(9) . . ?
B3' B7' B11' 106.03(11) . . ?
B3' B7' H7' 117.7(9) . . ?
B3' B7' B8' 59.02(9) . . ?
B3' B7' B12' 105.82(11) . . ?
C2' B7' B11' 58.97(9) . . ?
C2' B7' H7' 116.9(9) . . ?
C2' B7' B8' 106.50(11) . . ?
C2' B7' B12' 106.17(11) . . ?
B11' B7' H7' 123.4(9) . . ?
B8' B7' B11' 108.27(11) . . ?
B8' B7' H7' 124.2(9) . . ?
B12' B7' B11' 60.20(9) . . ?
B12' B7' H7' 129.8(9) . . ?
B12' B7' B8' 60.04(9) . . ?
C3' B8' B4' 59.63(9) . . ?
C3' B8' B7' 59.13(9) . . ?
C3' B8' H8' 117.8(9) . . ?
C3' B8' B9' 105.78(11) . . ?
C3' B8' B12' 105.84(11) . . ?
B3' B8' B4' 59.63(9) . . ?
B3' B8' B7' 59.13(9) . . ?
B3' B8' H8' 117.8(9) . . ?
B3' B8' B9' 105.78(11) . . ?
B3' B8' B12' 105.84(11) . . ?
B4' B8' H8' 119.6(10) . . ?
B7' B8' B4' 108.28(10) . . ?
B7' B8' H8' 119.6(10) . . ?
B7' B8' B9' 108.12(11) . . ?
B7' B8' B12' 59.94(9) . . ?
B9' B8' B4' 59.32(9) . . ?
B9' B8' H8' 126.7(10) . . ?
B12' B8' B4' 107.76(11) . . ?
B12' B8' H8' 126.8(10) . . ?
B12' B8' B9' 60.26(9) . . ?
B5' B9' B8' 108.31(11) . . ?
B5' B9' H9' 120.0(9) . . ?
B5' B9' B10' 60.00(9) . . ?
B5' B9' B12' 107.87(11) . . ?
B4' B9' B5' 60.28(8) . . ?
B4' B9' B8' 60.38(9) . . ?
B4' B9' H9' 118.3(9) . . ?
B4' B9' B10' 108.24(10) . . ?
B4' B9' B12' 108.25(11) . . ?
B8' B9' H9' 121.4(9) . . ?
B8' B9' B10' 107.67(11) . . ?
B8' B9' B12' 59.81(9) . . ?
B10' B9' H9' 123.9(9) . . ?
B10' B9' B12' 59.67(9) . . ?
B12' B9' H9' 124.7(9) . . ?
B6' B10' B5' 60.18(8) . . ?
B6' B10' B11' 60.05(9) . . ?
B6' B10' B9' 108.10(11) . . ?
B6' B10' H10' 119.7(9) . . ?
B6' B10' B12' 108.28(11) . . ?
B5' B10' B11' 108.21(11) . . ?
B5' B10' B9' 59.80(9) . . ?
B5' B10' H10' 121.9(10) . . ?
B11' B10' B9' 108.30(11) . . ?
B11' B10' H10' 120.2(10) . . ?
B9' B10' H10' 123.7(9) . . ?
B12' B10' B5' 108.19(11) . . ?
B12' B10' B11' 60.15(9) . . ?
B12' B10' B9' 60.28(9) . . ?
B12' B10' H10' 122.5(10) . . ?
B11' B12' B9' 108.09(11) . . ?
B11' B12' H12' 120.4(10) . . ?
B7' B12' B11' 59.95(9) . . ?
B7' B12' B8' 60.02(9) . . ?
B7' B12' B9' 107.92(11) . . ?
B7' B12' H12' 121.3(10) . . ?
B8' B12' B11' 108.06(11) . . ?
B8' B12' B9' 59.93(9) . . ?
B8' B12' H12' 122.6(9) . . ?
B9' B12' H12' 122.8(10) . . ?
B10' B12' B11' 60.11(9) . . ?
B10' B12' B7' 108.03(11) . . ?
B10' B12' B8' 108.07(11) . . ?
B10' B12' B9' 60.05(9) . . ?
B10' B12' H12' 121.3(9) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 B3 B4 B5 33.83(10) . . . . ?
C1 B3 B4 C8 131.74(11) . . . . ?
C1 B3 B4 B9 97.35(11) . . . . ?
C1 B3 B7 Ru2 55.29(8) . . . . ?
C1 B3 B7 C8 -92.72(10) . . . . ?
C1 B3 B7 B11 3.17(13) . . . . ?
C1 B3 B7 B12 -59.02(12) . . . . ?
C1 B3 C8 B4 -39.61(9) . . . . ?
C1 B3 C8 B7 102.22(10) . . . . ?
C1 B3 C8 B9 -3.22(13) . . . . ?
C1 B3 C8 B12 65.16(12) . . . . ?
C1 B3 C8 C1' -147.29(10) . . . . ?
C1 B4 B5 B6 34.13(10) . . . . ?
C1 B4 B5 B9 135.52(11) . . . . ?
C1 B4 B5 B10 97.39(11) . . . . ?
C1 B4 C8 B3 40.98(9) . . . . ?
C1 B4 C8 B7 3.50(13) . . . . ?
C1 B4 C8 B9 -101.11(11) . . . . ?
C1 B4 C8 B12 -64.79(12) . . . . ?
C1 B4 C8 C1' 150.47(10) . . . . ?
C1 B4 B9 B5 -39.03(10) . . . . ?
C1 B4 B9 C8 96.18(10) . . . . ?
C1 B4 B9 B10 -0.61(13) . . . . ?
C1 B4 B9 B12 62.59(12) . . . . ?
C1 B5 B6 Ru2 25.92(9) . . . . ?
C1 B5 B6 B10 134.73(11) . . . . ?
C1 B5 B6 B11 98.21(11) . . . . ?
C1 B5 B9 B4 38.20(10) . . . . ?
C1 B5 B9 C8 -0.06(14) . . . . ?
C1 B5 B9 B10 -99.07(11) . . . . ?
C1 B5 B9 B12 -61.45(13) . . . . ?
C1 B5 B10 B6 -39.23(10) . . . . ?
C1 B5 B10 B9 99.34(11) . . . . ?
C1 B5 B10 B11 -1.67(14) . . . . ?
C1 B5 B10 B12 61.59(13) . . . . ?
C1 B6 B10 B5 38.57(10) . . . . ?
C1 B6 B10 B9 1.72(14) . . . . ?
C1 B6 B10 B11 -100.44(11) . . . . ?
C1 B6 B10 B12 -62.29(13) . . . . ?
C1 B6 B11 Ru2 -54.04(8) . . . . ?
C1 B6 B11 B7 -3.63(13) . . . . ?
C1 B6 B11 B10 97.49(11) . . . . ?
C1 B6 B11 B12 59.69(13) . . . . ?
Ru2 C1 B3 B4 -154.51(9) . . . . ?
Ru2 C1 B3 B7 -54.46(8) . . . . ?
Ru2 C1 B3 C8 -114.84(8) . . . . ?
Ru2 C1 B4 B3 28.26(10) . . . . ?
Ru2 C1 B4 B5 -114.18(12) . . . . ?
Ru2 C1 B4 C8 -13.02(14) . . . . ?
Ru2 C1 B4 B9 -75.22(12) . . . . ?
Ru2 C1 B5 B4 113.87(11) . . . . ?
Ru2 C1 B5 B6 -27.54(10) . . . . ?
Ru2 C1 B5 B9 74.59(13) . . . . ?
Ru2 C1 B5 B10 12.10(14) . . . . ?
Ru2 C1 B6 B5 155.42(9) . . . . ?
Ru2 C1 B6 B10 116.29(10) . . . . ?
Ru2 C1 B6 B11 54.14(8) . . . . ?
Ru2 B3 B4 C1 -27.03(9) . . . . ?
Ru2 B3 B4 B5 6.80(14) . . . . ?
Ru2 B3 B4 C8 104.71(10) . . . . ?
Ru2 B3 B4 B9 70.32(12) . . . . ?
Ru2 B3 B7 C8 -148.01(8) . . . . ?
Ru2 B3 B7 B11 -52.12(8) . . . . ?
Ru2 B3 B7 B12 -114.31(9) . . . . ?
Ru2 B3 C8 B4 -109.07(10) . . . . ?
Ru2 B3 C8 B7 32.76(8) . . . . ?
Ru2 B3 C8 B9 -72.68(12) . . . . ?
Ru2 B3 C8 B12 -4.30(13) . . . . ?
Ru2 B3 C8 C1' 143.25(9) . . . . ?
Ru2 B6 B10 B5 108.92(11) . . . . ?
Ru2 B6 B10 B9 72.07(13) . . . . ?
Ru2 B6 B10 B11 -30.09(10) . . . . ?
Ru2 B6 B10 B12 8.06(15) . . . . ?
Ru2 B6 B11 B7 50.41(8) . . . . ?
Ru2 B6 B11 B10 151.53(9) . . . . ?
Ru2 B6 B11 B12 113.73(10) . . . . ?
Ru2 B7 C8 B3 -31.52(8) . . . . ?
Ru2 B7 C8 B4 5.99(13) . . . . ?
Ru2 B7 C8 B9 74.62(11) . . . . ?
Ru2 B7 C8 B12 109.62(10) . . . . ?
Ru2 B7 C8 C1' -140.13(10) . . . . ?
Ru2 B7 B11 B6 -50.27(8) . . . . ?
Ru2 B7 B11 B10 -112.78(10) . . . . ?
Ru2 B7 B11 B12 -149.50(9) . . . . ?
Ru2 B7 B12 C8 -102.43(10) . . . . ?
Ru2 B7 B12 B9 -69.27(12) . . . . ?
Ru2 B7 B12 B10 -5.58(14) . . . . ?
Ru2 B7 B12 B11 32.04(9) . . . . ?
Ru2 B11 B12 B7 -31.40(9) . . . . ?
Ru2 B11 B12 C8 8.77(14) . . . . ?
Ru2 B11 B12 B9 71.51(13) . . . . ?
Ru2 B11 B12 B10 107.36(11) . . . . ?
Ru2 C20 C21 C22 -54.80(12) . . . . ?
Ru2 C20 C25 C24 54.87(12) . . . . ?
Ru2 C21 C22 C23 -56.70(11) . . . . ?
Ru2 C22 C23 C24 -54.00(11) . . . . ?
Ru2 C22 C23 C27 128.25(13) . . . . ?
Ru2 C23 C24 C25 -55.14(12) . . . . ?
Ru2 C23 C27 C28 75.16(16) . . . . ?
Ru2 C23 C27 C29 -161.19(11) . . . . ?
Ru2 C24 C25 C20 -55.22(13) . . . . ?
B3 C1 B4 B5 -142.44(11) . . . . ?
B3 C1 B4 C8 -41.28(9) . . . . ?
B3 C1 B4 B9 -103.48(11) . . . . ?
B3 C1 B5 B4 37.18(11) . . . . ?
B3 C1 B5 B6 -104.23(12) . . . . ?
B3 C1 B5 B9 -2.10(15) . . . . ?
B3 C1 B5 B10 -64.59(13) . . . . ?
B3 C1 B6 Ru2 -48.14(9) . . . . ?
B3 C1 B6 B5 107.28(12) . . . . ?
B3 C1 B6 B10 68.14(13) . . . . ?
B3 C1 B6 B11 5.99(14) . . . . ?
B3 B4 B5 C1 -33.49(10) . . . . ?
B3 B4 B5 B6 0.64(14) . . . . ?
B3 B4 B5 B9 102.03(11) . . . . ?
B3 B4 B5 B10 63.91(13) . . . . ?
B3 B4 C8 B7 -37.48(10) . . . . ?
B3 B4 C8 B9 -142.09(10) . . . . ?
B3 B4 C8 B12 -105.77(11) . . . . ?
B3 B4 C8 C1' 109.49(12) . . . . ?
B3 B4 B9 B5 -101.05(11) . . . . ?
B3 B4 B9 C8 34.15(9) . . . . ?
B3 B4 B9 B10 -62.64(13) . . . . ?
B3 B4 B9 B12 0.56(14) . . . . ?
B3 B7 C8 B4 37.51(10) . . . . ?
B3 B7 C8 B9 106.14(11) . . . . ?
B3 B7 C8 B12 141.14(10) . . . . ?
B3 B7 C8 C1' -108.61(12) . . . . ?
B3 B7 B11 Ru2 50.56(8) . . . . ?
B3 B7 B11 B6 0.29(13) . . . . ?
B3 B7 B11 B10 -62.22(13) . . . . ?
B3 B7 B11 B12 -98.94(11) . . . . ?
B3 B7 B12 C8 -33.64(9) . . . . ?
B3 B7 B12 B9 -0.48(13) . . . . ?
B3 B7 B12 B10 63.21(13) . . . . ?
B3 B7 B12 B11 100.83(11) . . . . ?
B3 C8 B9 B4 -36.94(10) . . . . ?
B3 C8 B9 B5 2.17(14) . . . . ?
B3 C8 B9 B10 65.13(13) . . . . ?
B3 C8 B9 B12 104.83(11) . . . . ?
B3 C8 B12 B7 37.61(10) . . . . ?
B3 C8 B12 B9 -105.83(11) . . . . ?
B3 C8 B12 B10 -66.27(12) . . . . ?
B3 C8 B12 B11 -2.71(14) . . . . ?
B3 C8 C1' C3' -112.40(12) . . . . ?
B3 C8 C1' B2' 178.45(10) . . . . ?
B3 C8 C1' B3' -112.40(12) . . . . ?
B3 C8 C1' C2' 178.45(10) . . . . ?
B3 C8 C1' B6' 107.12(13) . . . . ?
B3 C8 C1' B5' 32.52(16) . . . . ?
B3 C8 C1' B4' -41.38(15) . . . . ?
B4 C1 B3 Ru2 154.51(9) . . . . ?
B4 C1 B3 B7 100.05(10) . . . . ?
B4 C1 B3 C8 39.67(9) . . . . ?
B4 C1 B5 B6 -141.41(11) . . . . ?
B4 C1 B5 B9 -39.28(10) . . . . ?
B4 C1 B5 B10 -101.77(11) . . . . ?
B4 C1 B6 Ru2 -118.52(10) . . . . ?
B4 C1 B6 B5 36.90(10) . . . . ?
B4 C1 B6 B10 -2.23(14) . . . . ?
B4 C1 B6 B11 -64.38(13) . . . . ?
B4 B3 B7 Ru2 115.11(9) . . . . ?
B4 B3 B7 C8 -32.90(9) . . . . ?
B4 B3 B7 B11 62.99(12) . . . . ?
B4 B3 B7 B12 0.80(13) . . . . ?
B4 B3 C8 B7 141.83(10) . . . . ?
B4 B3 C8 B9 36.39(10) . . . . ?
B4 B3 C8 B12 104.77(11) . . . . ?
B4 B3 C8 C1' -107.68(12) . . . . ?
B4 B5 B6 C1 -33.76(10) . . . . ?
B4 B5 B6 Ru2 -7.84(15) . . . . ?
B4 B5 B6 B10 100.96(12) . . . . ?
B4 B5 B6 B11 64.44(13) . . . . ?
B4 B5 B9 C8 -38.26(9) . . . . ?
B4 B5 B9 B10 -137.27(11) . . . . ?
B4 B5 B9 B12 -99.65(11) . . . . ?
B4 B5 B10 B6 -100.22(11) . . . . ?
B4 B5 B10 B9 38.36(10) . . . . ?
B4 B5 B10 B11 -62.66(13) . . . . ?
B4 B5 B10 B12 0.61(14) . . . . ?
B4 C8 B9 B5 39.11(10) . . . . ?
B4 C8 B9 B10 102.07(11) . . . . ?
B4 C8 B9 B12 141.77(11) . . . . ?
B4 C8 B12 B7 107.14(11) . . . . ?
B4 C8 B12 B9 -36.29(10) . . . . ?
B4 C8 B12 B10 3.26(14) . . . . ?
B4 C8 B12 B11 66.82(13) . . . . ?
B4 C8 C1' C3' 175.24(10) . . . . ?
B4 C8 C1' B2' 106.10(13) . . . . ?
B4 C8 C1' B3' 175.24(10) . . . . ?
B4 C8 C1' C2' 106.10(13) . . . . ?
B4 C8 C1' B6' 34.77(16) . . . . ?
B4 C8 C1' B5' -39.84(16) . . . . ?
B4 C8 C1' B4' -113.73(12) . . . . ?
B4 B9 B10 B5 -38.10(10) . . . . ?
B4 B9 B10 B6 -0.72(14) . . . . ?
B4 B9 B10 B11 64.08(14) . . . . ?
B4 B9 B10 B12 99.88(11) . . . . ?
B4 B9 B12 B7 -0.04(14) . . . . ?
B4 B9 B12 C8 33.38(9) . . . . ?
B4 B9 B12 B10 -101.14(11) . . . . ?
B4 B9 B12 B11 -64.72(13) . . . . ?
B5 C1 B3 Ru2 118.05(11) . . . . ?
B5 C1 B3 B4 -36.46(11) . . . . ?
B5 C1 B3 B7 63.59(13) . . . . ?
B5 C1 B3 C8 3.21(13) . . . . ?
B5 C1 B4 B3 142.44(11) . . . . ?
B5 C1 B4 C8 101.16(11) . . . . ?
B5 C1 B4 B9 38.96(10) . . . . ?
B5 C1 B6 Ru2 -155.42(9) . . . . ?
B5 C1 B6 B10 -39.14(10) . . . . ?
B5 C1 B6 B11 -101.28(11) . . . . ?
B5 B4 C8 B3 102.86(11) . . . . ?
B5 B4 C8 B7 65.38(13) . . . . ?
B5 B4 C8 B9 -39.23(10) . . . . ?
B5 B4 C8 B12 -2.91(13) . . . . ?
B5 B4 C8 C1' -147.65(11) . . . . ?
B5 B4 B9 C8 135.20(11) . . . . ?
B5 B4 B9 B10 38.41(10) . . . . ?
B5 B4 B9 B12 101.61(11) . . . . ?
B5 B6 B10 B9 -36.85(10) . . . . ?
B5 B6 B10 B11 -139.01(11) . . . . ?
B5 B6 B10 B12 -100.86(12) . . . . ?
B5 B6 B11 Ru2 -115.16(10) . . . . ?
B5 B6 B11 B7 -64.75(13) . . . . ?
B5 B6 B11 B10 36.36(10) . . . . ?
B5 B6 B11 B12 -1.44(14) . . . . ?
B5 B9 B10 B6 37.38(10) . . . . ?
B5 B9 B10 B11 102.18(12) . . . . ?
B5 B9 B10 B12 137.98(11) . . . . ?
B5 B9 B12 B7 63.19(13) . . . . ?
B5 B9 B12 C8 96.61(11) . . . . ?
B5 B9 B12 B10 -37.91(10) . . . . ?
B5 B9 B12 B11 -1.49(14) . . . . ?
B5 B10 B11 Ru2 -8.23(14) . . . . ?
B5 B10 B11 B6 -37.39(10) . . . . ?
B5 B10 B11 B7 62.54(13) . . . . ?
B5 B10 B11 B12 99.59(12) . . . . ?
B5 B10 B12 B7 -65.43(13) . . . . ?
B5 B10 B12 C8 -2.26(14) . . . . ?
B5 B10 B12 B9 37.26(10) . . . . ?
B5 B10 B12 B11 -102.86(12) . . . . ?
B6 C1 B3 Ru2 48.67(9) . . . . ?
B6 C1 B3 B4 -105.83(12) . . . . ?
B6 C1 B3 B7 -5.79(13) . . . . ?
B6 C1 B3 C8 -66.16(12) . . . . ?
B6 C1 B4 B3 105.30(12) . . . . ?
B6 C1 B4 B5 -37.14(11) . . . . ?
B6 C1 B4 C8 64.01(13) . . . . ?
B6 C1 B4 B9 1.82(14) . . . . ?
B6 C1 B5 B4 141.41(11) . . . . ?
B6 C1 B5 B9 102.13(12) . . . . ?
B6 C1 B5 B10 39.65(10) . . . . ?
B6 B5 B9 B4 100.20(11) . . . . ?
B6 B5 B9 C8 61.94(13) . . . . ?
B6 B5 B9 B10 -37.07(10) . . . . ?
B6 B5 B9 B12 0.55(14) . . . . ?
B6 B5 B10 B9 138.57(11) . . . . ?
B6 B5 B10 B11 37.56(10) . . . . ?
B6 B5 B10 B12 100.82(12) . . . . ?
B6 B10 B11 Ru2 29.16(9) . . . . ?
B6 B10 B11 B7 99.93(11) . . . . ?
B6 B10 B11 B12 136.99(11) . . . . ?
B6 B10 B12 B7 -1.39(15) . . . . ?
B6 B10 B12 C8 61.78(13) . . . . ?
B6 B10 B12 B9 101.30(12) . . . . ?
B6 B10 B12 B11 -38.82(10) . . . . ?
B6 B11 B12 B7 -101.12(11) . . . . ?
B6 B11 B12 C8 -60.94(12) . . . . ?
B6 B11 B12 B9 1.79(14) . . . . ?
B6 B11 B12 B10 37.64(10) . . . . ?
B7 B3 B4 C1 -98.21(11) . . . . ?
B7 B3 B4 B5 -64.37(13) . . . . ?
B7 B3 B4 C8 33.54(9) . . . . ?
B7 B3 B4 B9 -0.85(13) . . . . ?
B7 B3 C8 B4 -141.83(10) . . . . ?
B7 B3 C8 B9 -105.44(11) . . . . ?
B7 B3 C8 B12 -37.06(10) . . . . ?
B7 B3 C8 C1' 110.49(12) . . . . ?
B7 C8 B9 B4 -106.81(11) . . . . ?
B7 C8 B9 B5 -67.70(13) . . . . ?
B7 C8 B9 B10 -4.74(14) . . . . ?
B7 C8 B9 B12 34.96(10) . . . . ?
B7 C8 B12 B9 -143.44(10) . . . . ?
B7 C8 B12 B10 -103.88(11) . . . . ?
B7 C8 B12 B11 -40.32(10) . . . . ?
B7 C8 C1' C3' -39.21(15) . . . . ?
B7 C8 C1' B2' -108.36(12) . . . . ?
B7 C8 C1' B3' -39.21(15) . . . . ?
B7 C8 C1' C2' -108.36(12) . . . . ?
B7 C8 C1' B6' -179.69(10) . . . . ?
B7 C8 C1' B5' 105.70(13) . . . . ?
B7 C8 C1' B4' 31.81(16) . . . . ?
B7 B11 B12 C8 40.18(9) . . . . ?
B7 B11 B12 B9 102.91(11) . . . . ?
B7 B11 B12 B10 138.76(11) . . . . ?
C8 B3 B4 C1 -131.74(11) . . . . ?
C8 B3 B4 B5 -97.91(11) . . . . ?
C8 B3 B4 B9 -34.39(9) . . . . ?
C8 B3 B7 Ru2 148.01(8) . . . . ?
C8 B3 B7 B11 95.89(10) . . . . ?
C8 B3 B7 B12 33.70(9) . . . . ?
C8 B4 B5 C1 -96.07(11) . . . . ?
C8 B4 B5 B6 -61.94(13) . . . . ?
C8 B4 B5 B9 39.45(10) . . . . ?
C8 B4 B5 B10 1.32(14) . . . . ?
C8 B4 B9 B5 -135.20(11) . . . . ?
C8 B4 B9 B10 -96.79(11) . . . . ?
C8 B4 B9 B12 -33.59(9) . . . . ?
C8 B7 B11 Ru2 110.88(8) . . . . ?
C8 B7 B11 B6 60.61(12) . . . . ?
C8 B7 B11 B10 -1.90(13) . . . . ?
C8 B7 B11 B12 -38.63(9) . . . . ?
C8 B7 B12 B9 33.16(9) . . . . ?
C8 B7 B12 B10 96.85(11) . . . . ?
C8 B7 B12 B11 134.47(11) . . . . ?
C8 B9 B10 B5 -98.90(11) . . . . ?
C8 B9 B10 B6 -61.52(13) . . . . ?
C8 B9 B10 B11 3.27(14) . . . . ?
C8 B9 B10 B12 39.07(10) . . . . ?
C8 B9 B12 B7 -33.42(9) . . . . ?
C8 B9 B12 B10 -134.52(11) . . . . ?
C8 B9 B12 B11 -98.10(11) . . . . ?
C8 C1' C3' B2' -108.00(12) . . . . ?
C8 C1' C3' B4' 110.30(12) . . . . ?
C8 C1' C3' B7' -144.79(11) . . . . ?
C8 C1' C3' B8' 149.07(11) . . . . ?
C8 C1' B2' C3' 107.43(12) . . . . ?
C8 C1' B2' B6' -111.77(12) . . . . ?
C8 C1' B2' B11' -150.73(11) . . . . ?
C8 C1' B2' B7' 143.74(11) . . . . ?
C8 C1' B3' C2' -108.00(12) . . . . ?
C8 C1' B3' B4' 110.30(12) . . . . ?
C8 C1' B3' B7' -144.79(11) . . . . ?
C8 C1' B3' B8' 149.07(11) . . . . ?
C8 C1' C2' B3' 107.43(12) . . . . ?
C8 C1' C2' B6' -111.77(12) . . . . ?
C8 C1' C2' B11' -150.73(11) . . . . ?
C8 C1' C2' B7' 143.74(11) . . . . ?
C8 C1' B6' B2' 106.95(13) . . . . ?
C8 C1' B6' C2' 106.95(13) . . . . ?
C8 C1' B6' B5' -113.59(13) . . . . ?
C8 C1' B6' B11' 143.91(11) . . . . ?
C8 C1' B6' B10' -153.26(11) . . . . ?
C8 C1' B5' B6' 110.26(12) . . . . ?
C8 C1' B5' B4' -108.49(13) . . . . ?
C8 C1' B5' B9' -147.63(11) . . . . ?
C8 C1' B5' B10' 149.69(11) . . . . ?
C8 C1' B4' C3' -107.21(13) . . . . ?
C8 C1' B4' B3' -107.21(13) . . . . ?
C8 C1' B4' B5' 114.07(12) . . . . ?
C8 C1' B4' B8' -143.62(11) . . . . ?
C8 C1' B4' B9' 153.58(11) . . . . ?
B9 B4 B5 C1 -135.52(11) . . . . ?
B9 B4 B5 B6 -101.39(12) . . . . ?
B9 B4 B5 B10 -38.12(10) . . . . ?
B9 B4 C8 B3 142.09(10) . . . . ?
B9 B4 C8 B7 104.62(11) . . . . ?
B9 B4 C8 B12 36.32(10) . . . . ?
B9 B4 C8 C1' -108.42(12) . . . . ?
B9 B5 B6 C1 -97.65(11) . . . . ?
B9 B5 B6 Ru2 -71.73(13) . . . . ?
B9 B5 B6 B10 37.08(10) . . . . ?
B9 B5 B6 B11 0.55(14) . . . . ?
B9 B5 B10 B6 -138.57(11) . . . . ?
B9 B5 B10 B11 -101.01(11) . . . . ?
B9 B5 B10 B12 -37.75(10) . . . . ?
B9 C8 B12 B7 143.44(10) . . . . ?
B9 C8 B12 B10 39.56(10) . . . . ?
B9 C8 B12 B11 103.12(11) . . . . ?
B9 C8 C1' C3' 104.74(13) . . . . ?
B9 C8 C1' B2' 35.60(15) . . . . ?
B9 C8 C1' B3' 104.74(13) . . . . ?
B9 C8 C1' C2' 35.60(15) . . . . ?
B9 C8 C1' B6' -35.73(16) . . . . ?
B9 C8 C1' B5' -110.34(13) . . . . ?
B9 C8 C1' B4' 175.77(11) . . . . ?
B9 B10 B11 Ru2 -71.62(13) . . . . ?
B9 B10 B11 B6 -100.78(12) . . . . ?
B9 B10 B11 B7 -0.85(15) . . . . ?
B9 B10 B11 B12 36.20(11) . . . . ?
B9 B10 B12 B7 -102.69(11) . . . . ?
B9 B10 B12 C8 -39.52(10) . . . . ?
B9 B10 B12 B11 -140.12(11) . . . . ?
B10 B5 B6 C1 -134.73(11) . . . . ?
B10 B5 B6 Ru2 -108.80(11) . . . . ?
B10 B5 B6 B11 -36.52(10) . . . . ?
B10 B5 B9 B4 137.27(11) . . . . ?
B10 B5 B9 C8 99.01(11) . . . . ?
B10 B5 B9 B12 37.62(10) . . . . ?
B10 B6 B11 Ru2 -151.53(9) . . . . ?
B10 B6 B11 B7 -101.11(11) . . . . ?
B10 B6 B11 B12 -37.80(10) . . . . ?
B10 B9 B12 B7 101.10(12) . . . . ?
B10 B9 B12 C8 134.52(11) . . . . ?
B10 B9 B12 B11 36.43(10) . . . . ?
B10 B11 B12 B7 -138.76(11) . . . . ?
B10 B11 B12 C8 -98.58(11) . . . . ?
B10 B11 B12 B9 -35.85(10) . . . . ?
B11 B6 B10 B5 139.01(11) . . . . ?
B11 B6 B10 B9 102.16(11) . . . . ?
B11 B6 B10 B12 38.16(10) . . . . ?
B11 B7 C8 B3 -101.94(10) . . . . ?
B11 B7 C8 B4 -64.43(12) . . . . ?
B11 B7 C8 B9 4.20(13) . . . . ?
B11 B7 C8 B12 39.20(9) . . . . ?
B11 B7 C8 C1' 149.45(11) . . . . ?
B11 B7 B12 C8 -134.47(11) . . . . ?
B11 B7 B12 B9 -101.32(12) . . . . ?
B11 B7 B12 B10 -37.63(10) . . . . ?
B11 B10 B12 B7 37.43(10) . . . . ?
B11 B10 B12 C8 100.60(11) . . . . ?
B11 B10 B12 B9 140.12(11) . . . . ?
B12 B7 C8 B3 -141.14(10) . . . . ?
B12 B7 C8 B4 -103.63(11) . . . . ?
B12 B7 C8 B9 -35.00(10) . . . . ?
B12 B7 C8 C1' 110.25(12) . . . . ?
B12 B7 B11 Ru2 149.50(9) . . . . ?
B12 B7 B11 B6 99.24(11) . . . . ?
B12 B7 B11 B10 36.73(10) . . . . ?
B12 C8 B9 B4 -141.77(11) . . . . ?
B12 C8 B9 B5 -102.66(11) . . . . ?
B12 C8 B9 B10 -39.70(10) . . . . ?
B12 C8 C1' C3' 33.06(16) . . . . ?
B12 C8 C1' B2' -36.09(15) . . . . ?
B12 C8 C1' B3' 33.06(16) . . . . ?
B12 C8 C1' C2' -36.09(15) . . . . ?
B12 C8 C1' B6' -107.42(13) . . . . ?
B12 C8 C1' B5' 177.97(11) . . . . ?
B12 C8 C1' B4' 104.08(13) . . . . ?
B12 B9 B10 B5 -137.98(11) . . . . ?
B12 B9 B10 B6 -100.60(12) . . . . ?
B12 B9 B10 B11 -35.80(10) . . . . ?
B12 B10 B11 Ru2 -107.83(11) . . . . ?
B12 B10 B11 B6 -136.99(11) . . . . ?
B12 B10 B11 B7 -37.05(10) . . . . ?
C20 C21 C22 Ru2 55.78(12) . . . . ?
C20 C21 C22 C23 -0.9(2) . . . . ?
C21 C20 C25 Ru2 -53.76(12) . . . . ?
C21 C20 C25 C24 1.1(2) . . . . ?
C21 C22 C23 Ru2 56.08(12) . . . . ?
C21 C22 C23 C24 2.08(19) . . . . ?
C21 C22 C23 C27 -175.67(12) . . . . ?
C22 C23 C24 Ru2 53.48(11) . . . . ?
C22 C23 C24 C25 -1.7(2) . . . . ?
C22 C23 C27 C28 -17.28(19) . . . . ?
C22 C23 C27 C29 106.37(16) . . . . ?
C23 C24 C25 Ru2 55.29(12) . . . . ?
C23 C24 C25 C20 0.1(2) . . . . ?
C24 C23 C27 C28 164.99(13) . . . . ?
C24 C23 C27 C29 -71.37(16) . . . . ?
C25 C20 C21 Ru2 54.10(12) . . . . ?
C25 C20 C21 C22 -0.7(2) . . . . ?
C26 C20 C21 Ru2 -124.45(14) . . . . ?
C26 C20 C21 C22 -179.25(14) . . . . ?
C26 C20 C25 Ru2 124.80(14) . . . . ?
C26 C20 C25 C24 179.68(14) . . . . ?
C27 C23 C24 Ru2 -128.67(12) . . . . ?
C27 C23 C24 C25 176.19(13) . . . . ?
C1' C8 B9 B4 107.31(12) . . . . ?
C1' C8 B9 B5 146.42(11) . . . . ?
C1' C8 B9 B10 -150.63(11) . . . . ?
C1' C8 B9 B12 -110.93(12) . . . . ?
C1' C8 B12 B7 -109.29(12) . . . . ?
C1' C8 B12 B9 107.27(12) . . . . ?
C1' C8 B12 B10 146.83(11) . . . . ?
C1' C8 B12 B11 -149.61(11) . . . . ?
C1' C3' B2' B6' -35.56(10) . . . . ?
C1' C3' B2' B11' -101.06(12) . . . . ?
C1' C3' B2' B7' -139.80(11) . . . . ?
C1' C3' B4' B5' 35.90(9) . . . . ?
C1' C3' B4' B8' 137.91(11) . . . . ?
C1' C3' B4' B9' 98.72(11) . . . . ?
C1' C3' B7' B2' 36.51(10) . . . . ?
C1' C3' B7' B11' -0.21(14) . . . . ?
C1' C3' B7' B8' -102.21(12) . . . . ?
C1' C3' B7' B12' -63.08(13) . . . . ?
C1' C3' B8' B4' -38.23(10) . . . . ?
C1' C3' B8' B7' 102.46(12) . . . . ?
C1' C3' B8' B9' 0.48(15) . . . . ?
C1' C3' B8' B12' 63.37(14) . . . . ?
C1' B2' B6' B5' -35.35(9) . . . . ?
C1' B2' B6' B11' -137.38(11) . . . . ?
C1' B2' B6' B10' -98.31(11) . . . . ?
C1' B2' B11' B6' 38.49(10) . . . . ?
C1' B2' B11' B7' -101.48(12) . . . . ?
C1' B2' B11' B10' -0.25(14) . . . . ?
C1' B2' B11' B12' -62.73(13) . . . . ?
C1' B2' B7' C3' -35.91(10) . . . . ?
C1' B2' B7' B11' 101.97(12) . . . . ?
C1' B2' B7' B8' 0.24(14) . . . . ?
C1' B2' B7' B12' 63.07(13) . . . . ?
C1' B3' C2' B6' -35.56(10) . . . . ?
C1' B3' C2' B11' -101.06(12) . . . . ?
C1' B3' C2' B7' -139.80(11) . . . . ?
C1' B3' B4' B5' 35.90(9) . . . . ?
C1' B3' B4' B8' 137.91(11) . . . . ?
C1' B3' B4' B9' 98.72(11) . . . . ?
C1' B3' B7' C2' 36.51(10) . . . . ?
C1' B3' B7' B11' -0.21(14) . . . . ?
C1' B3' B7' B8' -102.21(12) . . . . ?
C1' B3' B7' B12' -63.08(13) . . . . ?
C1' B3' B8' B4' -38.23(10) . . . . ?
C1' B3' B8' B7' 102.46(12) . . . . ?
C1' B3' B8' B9' 0.48(15) . . . . ?
C1' B3' B8' B12' 63.37(14) . . . . ?
C1' C2' B6' B5' -35.35(9) . . . . ?
C1' C2' B6' B11' -137.38(11) . . . . ?
C1' C2' B6' B10' -98.31(11) . . . . ?
C1' C2' B11' B6' 38.49(10) . . . . ?
C1' C2' B11' B7' -101.48(12) . . . . ?
C1' C2' B11' B10' -0.25(14) . . . . ?
C1' C2' B11' B12' -62.73(13) . . . . ?
C1' C2' B7' B3' -35.91(10) . . . . ?
C1' C2' B7' B11' 101.97(12) . . . . ?
C1' C2' B7' B8' 0.24(14) . . . . ?
C1' C2' B7' B12' 63.07(13) . . . . ?
C1' B6' B5' B4' -34.53(9) . . . . ?
C1' B6' B5' B9' -97.52(11) . . . . ?
C1' B6' B5' B10' -134.80(11) . . . . ?
C1' B6' B11' B2' -36.78(10) . . . . ?
C1' B6' B11' C2' -36.78(10) . . . . ?
C1' B6' B11' B7' -1.13(14) . . . . ?
C1' B6' B11' B10' 99.06(11) . . . . ?
C1' B6' B11' B12' 62.10(13) . . . . ?
C1' B6' B10' B5' 38.93(9) . . . . ?
C1' B6' B10' B11' -99.32(11) . . . . ?
C1' B6' B10' B9' 1.81(14) . . . . ?
C1' B6' B10' B12' -62.00(13) . . . . ?
C1' B5' B4' C3' -35.57(9) . . . . ?
C1' B5' B4' B3' -35.57(9) . . . . ?
C1' B5' B4' B8' -97.16(11) . . . . ?
C1' B5' B4' B9' -135.06(11) . . . . ?
C1' B5' B9' B4' 39.00(10) . . . . ?
C1' B5' B9' B8' 1.03(14) . . . . ?
C1' B5' B9' B10' -99.22(11) . . . . ?
C1' B5' B9' B12' -62.24(13) . . . . ?
C1' B5' B10' B6' -39.30(9) . . . . ?
C1' B5' B10' B11' -1.90(13) . . . . ?
C1' B5' B10' B9' 99.11(11) . . . . ?
C1' B5' B10' B12' 61.78(13) . . . . ?
C1' B4' B8' C3' 36.13(10) . . . . ?
C1' B4' B8' B3' 36.13(10) . . . . ?
C1' B4' B8' B7' 1.19(14) . . . . ?
C1' B4' B8' B9' -99.46(11) . . . . ?
C1' B4' B8' B12' -62.18(13) . . . . ?
C1' B4' B9' B5' -38.84(10) . . . . ?
C1' B4' B9' B8' 98.95(11) . . . . ?
C1' B4' B9' B10' -1.43(14) . . . . ?
C1' B4' B9' B12' 61.75(13) . . . . ?
C3' C1' B2' B6' 140.80(11) . . . . ?
C3' C1' B2' B11' 101.84(12) . . . . ?
C3' C1' B2' B7' 36.31(11) . . . . ?
C3' C1' B6' B2' -35.94(10) . . . . ?
C3' C1' B6' B5' 103.52(11) . . . . ?
C3' C1' B6' B11' 1.02(13) . . . . ?
C3' C1' B6' B10' 63.86(13) . . . . ?
C3' C1' B5' B6' -102.86(11) . . . . ?
C3' C1' B5' B4' 38.39(10) . . . . ?
C3' C1' B5' B9' -0.75(14) . . . . ?
C3' C1' B5' B10' -63.43(13) . . . . ?
C3' C1' B4' B5' -138.72(11) . . . . ?
C3' C1' B4' B8' -36.41(10) . . . . ?
C3' C1' B4' B9' -99.20(12) . . . . ?
C3' B2' B6' C1' 35.17(10) . . . . ?
C3' B2' B6' B5' -0.17(14) . . . . ?
C3' B2' B6' B11' -102.20(12) . . . . ?
C3' B2' B6' B10' -63.13(13) . . . . ?
C3' B2' B11' B6' 101.79(12) . . . . ?
C3' B2' B11' B7' -38.17(11) . . . . ?
C3' B2' B11' B10' 63.05(13) . . . . ?
C3' B2' B11' B12' 0.57(15) . . . . ?
C3' B2' B7' B11' 137.88(12) . . . . ?
C3' B2' B7' B8' 36.15(11) . . . . ?
C3' B2' B7' B12' 98.98(12) . . . . ?
C3' B4' B8' B7' -34.93(11) . . . . ?
C3' B4' B8' B9' -135.58(12) . . . . ?
C3' B4' B8' B12' -98.31(12) . . . . ?
C3' B4' B9' B5' -99.37(11) . . . . ?
C3' B4' B9' B8' 38.42(10) . . . . ?
C3' B4' B9' B10' -61.96(13) . . . . ?
C3' B4' B9' B12' 1.22(14) . . . . ?
C3' B7' B8' B4' 35.14(11) . . . . ?
C3' B7' B8' B9' 97.92(12) . . . . ?
C3' B7' B8' B12' 135.51(11) . . . . ?
C3' B7' B12' B11' 99.70(11) . . . . ?
C3' B7' B12' B8' -38.64(10) . . . . ?
C3' B7' B12' B9' -1.25(14) . . . . ?
C3' B7' B12' B10' 62.23(13) . . . . ?
C3' B8' B9' B5' -0.94(15) . . . . ?
C3' B8' B9' B4' -38.86(10) . . . . ?
C3' B8' B9' B10' 62.49(14) . . . . ?
C3' B8' B9' B12' 99.51(12) . . . . ?
C3' B8' B12' B11' 1.47(15) . . . . ?
C3' B8' B12' B7' 38.70(10) . . . . ?
C3' B8' B12' B9' -99.41(12) . . . . ?
C3' B8' B12' B10' -62.12(14) . . . . ?
B2' C1' C3' B4' -141.70(11) . . . . ?
B2' C1' C3' B7' -36.79(10) . . . . ?
B2' C1' C3' B8' -102.93(12) . . . . ?
B2' C1' B6' B5' 139.46(11) . . . . ?
B2' C1' B6' B11' 36.96(10) . . . . ?
B2' C1' B6' B10' 99.80(11) . . . . ?
B2' C1' B5' B6' -37.64(10) . . . . ?
B2' C1' B5' B4' 103.61(11) . . . . ?
B2' C1' B5' B9' 64.47(13) . . . . ?
B2' C1' B5' B10' 1.79(13) . . . . ?
B2' C1' B4' C3' 35.33(10) . . . . ?
B2' C1' B4' B5' -103.39(11) . . . . ?
B2' C1' B4' B8' -1.08(14) . . . . ?
B2' C1' B4' B9' -63.88(13) . . . . ?
B2' C3' B4' C1' -35.00(10) . . . . ?
B2' C3' B4' B5' 0.89(14) . . . . ?
B2' C3' B4' B8' 102.91(12) . . . . ?
B2' C3' B4' B9' 63.72(13) . . . . ?
B2' C3' B7' B11' -36.72(10) . . . . ?
B2' C3' B7' B8' -138.72(12) . . . . ?
B2' C3' B7' B12' -99.59(11) . . . . ?
B2' C3' B8' B4' -102.74(12) . . . . ?
B2' C3' B8' B7' 37.95(11) . . . . ?
B2' C3' B8' B9' -64.03(14) . . . . ?
B2' C3' B8' B12' -1.14(15) . . . . ?
B2' B6' B5' C1' 35.25(9) . . . . ?
B2' B6' B5' B4' 0.73(14) . . . . ?
B2' B6' B5' B9' -62.27(13) . . . . ?
B2' B6' B5' B10' -99.54(11) . . . . ?
B2' B6' B11' B7' 35.65(11) . . . . ?
B2' B6' B11' B10' 135.84(11) . . . . ?
B2' B6' B11' B12' 98.87(12) . . . . ?
B2' B6' B10' B5' 99.88(11) . . . . ?
B2' B6' B10' B11' -38.37(10) . . . . ?
B2' B6' B10' B9' 62.76(13) . . . . ?
B2' B6' B10' B12' -1.05(14) . . . . ?
B2' B11' B7' C3' 36.63(10) . . . . ?
B2' B11' B7' B8' 98.65(12) . . . . ?
B2' B11' B7' B12' 135.97(12) . . . . ?
B2' B11' B10' B6' 38.80(10) . . . . ?
B2' B11' B10' B5' 1.35(14) . . . . ?
B2' B11' B10' B9' -61.97(13) . . . . ?
B2' B11' B10' B12' -99.61(11) . . . . ?
B2' B11' B12' B7' -38.53(10) . . . . ?
B2' B11' B12' B8' -1.26(15) . . . . ?
B2' B11' B12' B9' 62.13(14) . . . . ?
B2' B11' B12' B10' 99.62(12) . . . . ?
B2' B7' B8' C3' -36.04(11) . . . . ?
B2' B7' B8' B4' -0.90(15) . . . . ?
B2' B7' B8' B9' 61.88(14) . . . . ?
B2' B7' B8' B12' 99.47(12) . . . . ?
B2' B7' B12' B11' 38.32(10) . . . . ?
B2' B7' B12' B8' -100.03(12) . . . . ?
B2' B7' B12' B9' -62.63(13) . . . . ?
B2' B7' B12' B10' 0.85(14) . . . . ?
B3' C1' C2' B6' 140.80(11) . . . . ?
B3' C1' C2' B11' 101.84(12) . . . . ?
B3' C1' C2' B7' 36.31(11) . . . . ?
B3' C1' B6' C2' -35.94(10) . . . . ?
B3' C1' B6' B5' 103.52(11) . . . . ?
B3' C1' B6' B11' 1.02(13) . . . . ?
B3' C1' B6' B10' 63.86(13) . . . . ?
B3' C1' B5' B6' -102.86(11) . . . . ?
B3' C1' B5' B4' 38.39(10) . . . . ?
B3' C1' B5' B9' -0.75(14) . . . . ?
B3' C1' B5' B10' -63.43(13) . . . . ?
B3' C1' B4' B5' -138.72(11) . . . . ?
B3' C1' B4' B8' -36.41(10) . . . . ?
B3' C1' B4' B9' -99.20(12) . . . . ?
B3' C2' B6' C1' 35.17(10) . . . . ?
B3' C2' B6' B5' -0.17(14) . . . . ?
B3' C2' B6' B11' -102.20(12) . . . . ?
B3' C2' B6' B10' -63.13(13) . . . . ?
B3' C2' B11' B6' 101.79(12) . . . . ?
B3' C2' B11' B7' -38.17(11) . . . . ?
B3' C2' B11' B10' 63.05(13) . . . . ?
B3' C2' B11' B12' 0.57(15) . . . . ?
B3' C2' B7' B11' 137.88(12) . . . . ?
B3' C2' B7' B8' 36.15(11) . . . . ?
B3' C2' B7' B12' 98.98(12) . . . . ?
B3' B4' B8' B7' -34.93(11) . . . . ?
B3' B4' B8' B9' -135.58(12) . . . . ?
B3' B4' B8' B12' -98.31(12) . . . . ?
B3' B4' B9' B5' -99.37(11) . . . . ?
B3' B4' B9' B8' 38.42(10) . . . . ?
B3' B4' B9' B10' -61.96(13) . . . . ?
B3' B4' B9' B12' 1.22(14) . . . . ?
B3' B7' B8' B4' 35.14(11) . . . . ?
B3' B7' B8' B9' 97.92(12) . . . . ?
B3' B7' B8' B12' 135.51(11) . . . . ?
B3' B7' B12' B11' 99.70(11) . . . . ?
B3' B7' B12' B8' -38.64(10) . . . . ?
B3' B7' B12' B9' -1.25(14) . . . . ?
B3' B7' B12' B10' 62.23(13) . . . . ?
B3' B8' B9' B5' -0.94(15) . . . . ?
B3' B8' B9' B4' -38.86(10) . . . . ?
B3' B8' B9' B10' 62.49(14) . . . . ?
B3' B8' B9' B12' 99.51(12) . . . . ?
B3' B8' B12' B11' 1.47(15) . . . . ?
B3' B8' B12' B7' 38.70(10) . . . . ?
B3' B8' B12' B9' -99.41(12) . . . . ?
B3' B8' B12' B10' -62.12(14) . . . . ?
C2' C1' B3' B4' -141.70(11) . . . . ?
C2' C1' B3' B7' -36.79(10) . . . . ?
C2' C1' B3' B8' -102.93(12) . . . . ?
C2' C1' B6' B5' 139.46(11) . . . . ?
C2' C1' B6' B11' 36.96(10) . . . . ?
C2' C1' B6' B10' 99.80(11) . . . . ?
C2' C1' B5' B6' -37.64(10) . . . . ?
C2' C1' B5' B4' 103.61(11) . . . . ?
C2' C1' B5' B9' 64.47(13) . . . . ?
C2' C1' B5' B10' 1.79(13) . . . . ?
C2' C1' B4' B3' 35.33(10) . . . . ?
C2' C1' B4' B5' -103.39(11) . . . . ?
C2' C1' B4' B8' -1.08(14) . . . . ?
C2' C1' B4' B9' -63.88(13) . . . . ?
C2' B3' B4' C1' -35.00(10) . . . . ?
C2' B3' B4' B5' 0.89(14) . . . . ?
C2' B3' B4' B8' 102.91(12) . . . . ?
C2' B3' B4' B9' 63.72(13) . . . . ?
C2' B3' B7' B11' -36.72(10) . . . . ?
C2' B3' B7' B8' -138.72(12) . . . . ?
C2' B3' B7' B12' -99.59(11) . . . . ?
C2' B3' B8' B4' -102.74(12) . . . . ?
C2' B3' B8' B7' 37.95(11) . . . . ?
C2' B3' B8' B9' -64.03(14) . . . . ?
C2' B3' B8' B12' -1.14(15) . . . . ?
C2' B6' B5' C1' 35.25(9) . . . . ?
C2' B6' B5' B4' 0.73(14) . . . . ?
C2' B6' B5' B9' -62.27(13) . . . . ?
C2' B6' B5' B10' -99.54(11) . . . . ?
C2' B6' B11' B7' 35.65(11) . . . . ?
C2' B6' B11' B10' 135.84(11) . . . . ?
C2' B6' B11' B12' 98.87(12) . . . . ?
C2' B6' B10' B5' 99.88(11) . . . . ?
C2' B6' B10' B11' -38.37(10) . . . . ?
C2' B6' B10' B9' 62.76(13) . . . . ?
C2' B6' B10' B12' -1.05(14) . . . . ?
C2' B11' B7' B3' 36.63(10) . . . . ?
C2' B11' B7' B8' 98.65(12) . . . . ?
C2' B11' B7' B12' 135.97(12) . . . . ?
C2' B11' B10' B6' 38.80(10) . . . . ?
C2' B11' B10' B5' 1.35(14) . . . . ?
C2' B11' B10' B9' -61.97(13) . . . . ?
C2' B11' B10' B12' -99.61(11) . . . . ?
C2' B11' B12' B7' -38.53(10) . . . . ?
C2' B11' B12' B8' -1.26(15) . . . . ?
C2' B11' B12' B9' 62.13(14) . . . . ?
C2' B11' B12' B10' 99.62(12) . . . . ?
C2' B7' B8' B3' -36.04(11) . . . . ?
C2' B7' B8' B4' -0.90(15) . . . . ?
C2' B7' B8' B9' 61.88(14) . . . . ?
C2' B7' B8' B12' 99.47(12) . . . . ?
C2' B7' B12' B11' 38.32(10) . . . . ?
C2' B7' B12' B8' -100.03(12) . . . . ?
C2' B7' B12' B9' -62.63(13) . . . . ?
C2' B7' B12' B10' 0.85(14) . . . . ?
B6' C1' C3' B2' 36.27(10) . . . . ?
B6' C1' C3' B4' -105.43(11) . . . . ?
B6' C1' C3' B7' -0.52(14) . . . . ?
B6' C1' C3' B8' -66.66(13) . . . . ?
B6' C1' B2' C3' -140.80(11) . . . . ?
B6' C1' B2' B11' -38.96(10) . . . . ?
B6' C1' B2' B7' -104.49(12) . . . . ?
B6' C1' B3' C2' 36.27(10) . . . . ?
B6' C1' B3' B4' -105.43(11) . . . . ?
B6' C1' B3' B7' -0.52(14) . . . . ?
B6' C1' B3' B8' -66.66(13) . . . . ?
B6' C1' C2' B3' -140.80(11) . . . . ?
B6' C1' C2' B11' -38.96(10) . . . . ?
B6' C1' C2' B7' -104.49(12) . . . . ?
B6' C1' B5' B4' 141.25(11) . . . . ?
B6' C1' B5' B9' 102.11(11) . . . . ?
B6' C1' B5' B10' 39.43(10) . . . . ?
B6' C1' B4' C3' 101.91(11) . . . . ?
B6' C1' B4' B3' 101.91(11) . . . . ?
B6' C1' B4' B5' -36.81(10) . . . . ?
B6' C1' B4' B8' 65.50(13) . . . . ?
B6' C1' B4' B9' 2.70(14) . . . . ?
B6' B2' B11' B7' -139.97(11) . . . . ?
B6' B2' B11' B10' -38.74(10) . . . . ?
B6' B2' B11' B12' -101.22(12) . . . . ?
B6' B2' B7' C3' -100.55(12) . . . . ?
B6' B2' B7' B11' 37.33(11) . . . . ?
B6' B2' B7' B8' -64.40(14) . . . . ?
B6' B2' B7' B12' -1.56(15) . . . . ?
B6' C2' B11' B7' -139.97(11) . . . . ?
B6' C2' B11' B10' -38.74(10) . . . . ?
B6' C2' B11' B12' -101.22(12) . . . . ?
B6' C2' B7' B3' -100.55(12) . . . . ?
B6' C2' B7' B11' 37.33(11) . . . . ?
B6' C2' B7' B8' -64.40(14) . . . . ?
B6' C2' B7' B12' -1.56(15) . . . . ?
B6' B5' B4' C1' 34.59(9) . . . . ?
B6' B5' B4' C3' -0.99(14) . . . . ?
B6' B5' B4' B3' -0.99(14) . . . . ?
B6' B5' B4' B8' -62.57(13) . . . . ?
B6' B5' B4' B9' -100.47(12) . . . . ?
B6' B5' B9' B4' 101.20(11) . . . . ?
B6' B5' B9' B8' 63.23(13) . . . . ?
B6' B5' B9' B10' -37.03(10) . . . . ?
B6' B5' B9' B12' -0.04(14) . . . . ?
B6' B5' B10' B11' 37.40(10) . . . . ?
B6' B5' B10' B9' 138.41(11) . . . . ?
B6' B5' B10' B12' 101.08(12) . . . . ?
B6' B11' B7' C3' 0.84(14) . . . . ?
B6' B11' B7' B2' -35.79(10) . . . . ?
B6' B11' B7' B3' 0.84(14) . . . . ?
B6' B11' B7' C2' -35.79(10) . . . . ?
B6' B11' B7' B8' 62.86(14) . . . . ?
B6' B11' B7' B12' 100.18(12) . . . . ?
B6' B11' B10' B5' -37.46(10) . . . . ?
B6' B11' B10' B9' -100.78(11) . . . . ?
B6' B11' B10' B12' -138.42(11) . . . . ?
B6' B11' B12' B7' -101.24(12) . . . . ?
B6' B11' B12' B8' -63.97(14) . . . . ?
B6' B11' B12' B9' -0.58(15) . . . . ?
B6' B11' B12' B10' 36.91(10) . . . . ?
B6' B10' B12' B11' -37.27(10) . . . . ?
B6' B10' B12' B7' 0.13(15) . . . . ?
B6' B10' B12' B8' 63.61(14) . . . . ?
B6' B10' B12' B9' 100.84(12) . . . . ?
B5' C1' C3' B2' 103.10(11) . . . . ?
B5' C1' C3' B4' -38.60(10) . . . . ?
B5' C1' C3' B7' 66.31(13) . . . . ?
B5' C1' C3' B8' 0.17(15) . . . . ?
B5' C1' B2' C3' -102.83(11) . . . . ?
B5' C1' B2' B6' 37.97(10) . . . . ?
B5' C1' B2' B11' -0.99(14) . . . . ?
B5' C1' B2' B7' -66.52(13) . . . . ?
B5' C1' B3' C2' 103.10(11) . . . . ?
B5' C1' B3' B4' -38.60(10) . . . . ?
B5' C1' B3' B7' 66.31(13) . . . . ?
B5' C1' B3' B8' 0.17(15) . . . . ?
B5' C1' C2' B3' -102.83(11) . . . . ?
B5' C1' C2' B6' 37.97(10) . . . . ?
B5' C1' C2' B11' -0.99(14) . . . . ?
B5' C1' C2' B7' -66.52(13) . . . . ?
B5' C1' B6' B2' -139.46(11) . . . . ?
B5' C1' B6' C2' -139.46(11) . . . . ?
B5' C1' B6' B11' -102.50(11) . . . . ?
B5' C1' B6' B10' -39.66(10) . . . . ?
B5' C1' B4' C3' 138.72(11) . . . . ?
B5' C1' B4' B3' 138.72(11) . . . . ?
B5' C1' B4' B8' 102.31(11) . . . . ?
B5' C1' B4' B9' 39.51(10) . . . . ?
B5' B6' B11' B2' -98.32(11) . . . . ?
B5' B6' B11' C2' -98.32(11) . . . . ?
B5' B6' B11' B7' -62.67(13) . . . . ?
B5' B6' B11' B10' 37.52(10) . . . . ?
B5' B6' B11' B12' 0.56(14) . . . . ?
B5' B6' B10' B11' -138.25(11) . . . . ?
B5' B6' B10' B9' -37.12(10) . . . . ?
B5' B6' B10' B12' -100.93(12) . . . . ?
B5' B4' B8' C3' 97.73(12) . . . . ?
B5' B4' B8' B3' 97.73(12) . . . . ?
B5' B4' B8' B7' 62.79(14) . . . . ?
B5' B4' B8' B9' -37.86(10) . . . . ?
B5' B4' B8' B12' -0.59(14) . . . . ?
B5' B4' B9' B8' 137.79(11) . . . . ?
B5' B4' B9' B10' 37.41(10) . . . . ?
B5' B4' B9' B12' 100.59(12) . . . . ?
B5' B9' B10' B6' 37.29(10) . . . . ?
B5' B9' B10' B11' 100.85(12) . . . . ?
B5' B9' B10' B12' 138.44(11) . . . . ?
B5' B9' B12' B11' 0.38(15) . . . . ?
B5' B9' B12' B7' 63.77(13) . . . . ?
B5' B9' B12' B8' 101.21(12) . . . . ?
B5' B9' B12' B10' -37.13(10) . . . . ?
B5' B10' B12' B11' -100.99(12) . . . . ?
B5' B10' B12' B7' -63.59(14) . . . . ?
B5' B10' B12' B8' -0.11(15) . . . . ?
B5' B10' B12' B9' 37.12(10) . . . . ?
B4' C1' C3' B2' 141.70(11) . . . . ?
B4' C1' C3' B7' 104.91(12) . . . . ?
B4' C1' C3' B8' 38.77(11) . . . . ?
B4' C1' B2' C3' -35.77(10) . . . . ?
B4' C1' B2' B6' 105.03(11) . . . . ?
B4' C1' B2' B11' 66.08(13) . . . . ?
B4' C1' B2' B7' 0.54(14) . . . . ?
B4' C1' B3' C2' 141.70(11) . . . . ?
B4' C1' B3' B7' 104.91(12) . . . . ?
B4' C1' B3' B8' 38.77(11) . . . . ?
B4' C1' C2' B3' -35.77(10) . . . . ?
B4' C1' C2' B6' 105.03(11) . . . . ?
B4' C1' C2' B11' 66.08(13) . . . . ?
B4' C1' C2' B7' 0.54(14) . . . . ?
B4' C1' B6' B2' -102.64(11) . . . . ?
B4' C1' B6' C2' -102.64(11) . . . . ?
B4' C1' B6' B5' 36.82(10) . . . . ?
B4' C1' B6' B11' -65.68(13) . . . . ?
B4' C1' B6' B10' -2.85(14) . . . . ?
B4' C1' B5' B6' -141.25(11) . . . . ?
B4' C1' B5' B9' -39.14(10) . . . . ?
B4' C1' B5' B10' -101.82(11) . . . . ?
B4' C3' B2' C1' 35.10(10) . . . . ?
B4' C3' B2' B6' -0.46(15) . . . . ?
B4' C3' B2' B11' -65.96(14) . . . . ?
B4' C3' B2' B7' -104.70(12) . . . . ?
B4' C3' B7' B2' 101.70(12) . . . . ?
B4' C3' B7' B11' 64.97(14) . . . . ?
B4' C3' B7' B8' -37.02(11) . . . . ?
B4' C3' B7' B12' 2.10(14) . . . . ?
B4' C3' B8' B7' 140.69(12) . . . . ?
B4' C3' B8' B9' 38.72(11) . . . . ?
B4' C3' B8' B12' 101.60(12) . . . . ?
B4' B3' C2' C1' 35.10(10) . . . . ?
B4' B3' C2' B6' -0.46(15) . . . . ?
B4' B3' C2' B11' -65.96(14) . . . . ?
B4' B3' C2' B7' -104.70(12) . . . . ?
B4' B3' B7' C2' 101.70(12) . . . . ?
B4' B3' B7' B11' 64.97(14) . . . . ?
B4' B3' B7' B8' -37.02(11) . . . . ?
B4' B3' B7' B12' 2.10(14) . . . . ?
B4' B3' B8' B7' 140.69(12) . . . . ?
B4' B3' B8' B9' 38.72(11) . . . . ?
B4' B3' B8' B12' 101.60(12) . . . . ?
B4' B5' B9' B8' -37.97(10) . . . . ?
B4' B5' B9' B10' -138.22(11) . . . . ?
B4' B5' B9' B12' -101.23(12) . . . . ?
B4' B5' B10' B6' -101.33(11) . . . . ?
B4' B5' B10' B11' -63.93(13) . . . . ?
B4' B5' B10' B9' 37.08(10) . . . . ?
B4' B5' B10' B12' -0.25(14) . . . . ?
B4' B8' B9' B5' 37.92(10) . . . . ?
B4' B8' B9' B10' 101.35(11) . . . . ?
B4' B8' B9' B12' 138.37(11) . . . . ?
B4' B8' B12' B11' 64.01(14) . . . . ?
B4' B8' B12' B7' 101.25(12) . . . . ?
B4' B8' B12' B9' -36.86(10) . . . . ?
B4' B8' B12' B10' 0.43(15) . . . . ?
B4' B9' B10' B6' -0.24(15) . . . . ?
B4' B9' B10' B5' -37.53(10) . . . . ?
B4' B9' B10' B11' 63.32(14) . . . . ?
B4' B9' B10' B12' 100.91(12) . . . . ?
B4' B9' B12' B11' -63.38(14) . . . . ?
B4' B9' B12' B7' 0.01(14) . . . . ?
B4' B9' B12' B8' 37.45(10) . . . . ?
B4' B9' B12' B10' -100.89(11) . . . . ?
B11' B2' B6' C1' 137.38(11) . . . . ?
B11' B2' B6' B5' 102.03(11) . . . . ?
B11' B2' B6' B10' 39.07(10) . . . . ?
B11' B2' B7' C3' -137.88(12) . . . . ?
B11' B2' B7' B8' -101.74(12) . . . . ?
B11' B2' B7' B12' -38.90(10) . . . . ?
B11' C2' B6' C1' 137.38(11) . . . . ?
B11' C2' B6' B5' 102.03(11) . . . . ?
B11' C2' B6' B10' 39.07(10) . . . . ?
B11' C2' B7' B3' -137.88(12) . . . . ?
B11' C2' B7' B8' -101.74(12) . . . . ?
B11' C2' B7' B12' -38.90(10) . . . . ?
B11' B6' B5' C1' 97.20(11) . . . . ?
B11' B6' B5' B4' 62.67(13) . . . . ?
B11' B6' B5' B9' -0.32(14) . . . . ?
B11' B6' B5' B10' -37.60(10) . . . . ?
B11' B6' B10' B5' 138.25(11) . . . . ?
B11' B6' B10' B9' 101.13(12) . . . . ?
B11' B6' B10' B12' 37.32(10) . . . . ?
B11' B7' B8' C3' -98.11(12) . . . . ?
B11' B7' B8' B3' -98.11(12) . . . . ?
B11' B7' B8' B4' -62.97(14) . . . . ?
B11' B7' B8' B9' -0.19(15) . . . . ?
B11' B7' B8' B12' 37.40(10) . . . . ?
B11' B7' B12' B8' -138.35(11) . . . . ?
B11' B7' B12' B9' -100.95(12) . . . . ?
B11' B7' B12' B10' -37.47(10) . . . . ?
B11' B10' B12' B7' 37.40(10) . . . . ?
B11' B10' B12' B8' 100.88(12) . . . . ?
B11' B10' B12' B9' 138.11(11) . . . . ?
B7' C3' B2' C1' 139.80(11) . . . . ?
B7' C3' B2' B6' 104.24(12) . . . . ?
B7' C3' B2' B11' 38.74(11) . . . . ?
B7' C3' B4' C1' -100.82(12) . . . . ?
B7' C3' B4' B5' -64.92(13) . . . . ?
B7' C3' B4' B8' 37.09(11) . . . . ?
B7' C3' B4' B9' -2.10(14) . . . . ?
B7' C3' B8' B4' -140.69(12) . . . . ?
B7' C3' B8' B9' -101.98(12) . . . . ?
B7' C3' B8' B12' -39.09(11) . . . . ?
B7' B2' B6' C1' 99.95(12) . . . . ?
B7' B2' B6' B5' 64.60(13) . . . . ?
B7' B2' B6' B11' -37.43(11) . . . . ?
B7' B2' B6' B10' 1.64(15) . . . . ?
B7' B2' B11' B6' 139.97(11) . . . . ?
B7' B2' B11' B10' 101.22(12) . . . . ?
B7' B2' B11' B12' 38.74(10) . . . . ?
B7' B3' C2' C1' 139.80(11) . . . . ?
B7' B3' C2' B6' 104.24(12) . . . . ?
B7' B3' C2' B11' 38.74(11) . . . . ?
B7' B3' B4' C1' -100.82(12) . . . . ?
B7' B3' B4' B5' -64.92(13) . . . . ?
B7' B3' B4' B8' 37.09(11) . . . . ?
B7' B3' B4' B9' -2.10(14) . . . . ?
B7' B3' B8' B4' -140.69(12) . . . . ?
B7' B3' B8' B9' -101.98(12) . . . . ?
B7' B3' B8' B12' -39.09(11) . . . . ?
B7' C2' B6' C1' 99.95(12) . . . . ?
B7' C2' B6' B5' 64.60(13) . . . . ?
B7' C2' B6' B11' -37.43(11) . . . . ?
B7' C2' B6' B10' 1.64(15) . . . . ?
B7' C2' B11' B6' 139.97(11) . . . . ?
B7' C2' B11' B10' 101.22(12) . . . . ?
B7' C2' B11' B12' 38.74(10) . . . . ?
B7' B11' B10' B6' 101.16(12) . . . . ?
B7' B11' B10' B5' 63.71(13) . . . . ?
B7' B11' B10' B9' 0.39(14) . . . . ?
B7' B11' B10' B12' -37.25(10) . . . . ?
B7' B11' B12' B8' 37.27(11) . . . . ?
B7' B11' B12' B9' 100.66(12) . . . . ?
B7' B11' B12' B10' 138.15(11) . . . . ?
B7' B8' B9' B5' -63.00(14) . . . . ?
B7' B8' B9' B4' -100.93(12) . . . . ?
B7' B8' B9' B10' 0.42(14) . . . . ?
B7' B8' B9' B12' 37.45(10) . . . . ?
B7' B8' B12' B11' -37.24(10) . . . . ?
B7' B8' B12' B9' -138.11(11) . . . . ?
B7' B8' B12' B10' -100.82(12) . . . . ?
B8' C3' B2' C1' 101.43(12) . . . . ?
B8' C3' B2' B6' 65.87(14) . . . . ?
B8' C3' B2' B11' 0.36(15) . . . . ?
B8' C3' B2' B7' -38.37(11) . . . . ?
B8' C3' B4' C1' -137.91(11) . . . . ?
B8' C3' B4' B5' -102.01(12) . . . . ?
B8' C3' B4' B9' -39.19(10) . . . . ?
B8' C3' B7' B2' 138.72(12) . . . . ?
B8' C3' B7' B11' 102.00(12) . . . . ?
B8' C3' B7' B12' 39.13(10) . . . . ?
B8' B3' C2' C1' 101.43(12) . . . . ?
B8' B3' C2' B6' 65.87(14) . . . . ?
B8' B3' C2' B11' 0.36(15) . . . . ?
B8' B3' C2' B7' -38.37(11) . . . . ?
B8' B3' B4' C1' -137.91(11) . . . . ?
B8' B3' B4' B5' -102.01(12) . . . . ?
B8' B3' B4' B9' -39.19(10) . . . . ?
B8' B3' B7' C2' 138.72(12) . . . . ?
B8' B3' B7' B11' 102.00(12) . . . . ?
B8' B3' B7' B12' 39.13(10) . . . . ?
B8' B4' B9' B5' -137.79(11) . . . . ?
B8' B4' B9' B10' -100.38(12) . . . . ?
B8' B4' B9' B12' -37.20(10) . . . . ?
B8' B7' B12' B11' 138.35(11) . . . . ?
B8' B7' B12' B9' 37.40(10) . . . . ?
B8' B7' B12' B10' 100.88(12) . . . . ?
B8' B9' B10' B6' -64.06(13) . . . . ?
B8' B9' B10' B5' -101.35(12) . . . . ?
B8' B9' B10' B11' -0.50(14) . . . . ?
B8' B9' B10' B12' 37.09(10) . . . . ?
B8' B9' B12' B11' -100.82(12) . . . . ?
B8' B9' B12' B7' -37.44(10) . . . . ?
B8' B9' B12' B10' -138.34(11) . . . . ?
B9' B5' B4' C1' 135.06(11) . . . . ?
B9' B5' B4' C3' 99.49(12) . . . . ?
B9' B5' B4' B3' 99.49(12) . . . . ?
B9' B5' B4' B8' 37.90(10) . . . . ?
B9' B5' B10' B6' -138.41(11) . . . . ?
B9' B5' B10' B11' -101.01(12) . . . . ?
B9' B5' B10' B12' -37.33(11) . . . . ?
B9' B4' B8' C3' 135.58(12) . . . . ?
B9' B4' B8' B3' 135.58(12) . . . . ?
B9' B4' B8' B7' 100.65(12) . . . . ?
B9' B4' B8' B12' 37.27(10) . . . . ?
B9' B8' B12' B11' 100.87(12) . . . . ?
B9' B8' B12' B7' 138.11(11) . . . . ?
B9' B8' B12' B10' 37.29(10) . . . . ?
B9' B10' B12' B11' -138.11(11) . . . . ?
B9' B10' B12' B7' -100.72(12) . . . . ?
B9' B10' B12' B8' -37.24(11) . . . . ?
B10' B6' B5' C1' 134.80(11) . . . . ?
B10' B6' B5' B4' 100.27(11) . . . . ?
B10' B6' B5' B9' 37.27(10) . . . . ?
B10' B6' B11' B2' -135.84(11) . . . . ?
B10' B6' B11' C2' -135.84(11) . . . . ?
B10' B6' B11' B7' -100.19(12) . . . . ?
B10' B6' B11' B12' -36.97(10) . . . . ?
B10' B5' B4' C1' 97.67(11) . . . . ?
B10' B5' B4' C3' 62.10(13) . . . . ?
B10' B5' B4' B3' 62.10(13) . . . . ?
B10' B5' B4' B8' 0.52(14) . . . . ?
B10' B5' B4' B9' -37.39(10) . . . . ?
B10' B5' B9' B4' 138.22(11) . . . . ?
B10' B5' B9' B8' 100.26(12) . . . . ?
B10' B5' B9' B12' 36.99(10) . . . . ?
B10' B11' B7' C3' -62.14(13) . . . . ?
B10' B11' B7' B2' -98.77(12) . . . . ?
B10' B11' B7' B3' -62.14(13) . . . . ?
B10' B11' B7' C2' -98.77(12) . . . . ?
B10' B11' B7' B8' -0.12(14) . . . . ?
B10' B11' B7' B12' 37.20(10) . . . . ?
B10' B11' B12' B7' -138.15(11) . . . . ?
B10' B11' B12' B8' -100.88(12) . . . . ?
B10' B11' B12' B9' -37.49(11) . . . . ?
B10' B9' B12' B11' 37.52(10) . . . . ?
B10' B9' B12' B7' 100.90(11) . . . . ?
B10' B9' B12' B8' 138.34(11) . . . . ?
B12' B11' B7' C3' -99.34(12) . . . . ?
B12' B11' B7' B2' -135.97(12) . . . . ?
B12' B11' B7' B3' -99.34(12) . . . . ?
B12' B11' B7' C2' -135.97(12) . . . . ?
B12' B11' B7' B8' -37.33(10) . . . . ?
B12' B11' B10' B6' 138.42(11) . . . . ?
B12' B11' B10' B5' 100.96(12) . . . . ?
B12' B11' B10' B9' 37.64(10) . . . . ?
B12' B7' B8' C3' -135.51(11) . . . . ?
B12' B7' B8' B3' -135.51(11) . . . . ?
B12' B7' B8' B4' -100.37(12) . . . . ?
B12' B7' B8' B9' -37.59(10) . . . . ?
B12' B8' B9' B5' -100.45(12) . . . . ?
B12' B8' B9' B4' -138.37(11) . . . . ?
B12' B8' B9' B10' -37.02(10) . . . . ?
B12' B9' B10' B6' -101.15(12) . . . . ?
B12' B9' B10' B5' -138.44(11) . . . . ?
B12' B9' B10' B11' -37.59(10) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_ac018a
_database_code_depnum_ccdc_archive 'CCDC 1042154'
_audit_update_record             
;
2015-01-05 deposited with the CCDC.
2015-02-09 downloaded from the CCDC.
;
_audit_creation_date             2014-12-12
_audit_creation_method           
;
Olex2 1.2
(compiled 2013.12.10 svn.r2850 for OlexSys, GUI svn.r4736)
;
_shelxl_version_number           2014/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C9 H26 B19 Co'
_chemical_formula_sum            'C9 H26 B19 Co'
_chemical_formula_weight         398.62
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   6.7993(5)
_cell_length_b                   14.4533(10)
_cell_length_c                   20.3575(14)
_cell_angle_alpha                89.609(3)
_cell_angle_beta                 85.554(3)
_cell_angle_gamma                89.158(3)
_cell_volume                     1994.3(2)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    ?
_cell_measurement_temperature    100.0
_cell_measurement_theta_max      ?
_cell_measurement_theta_min      ?
_shelx_estimated_absorpt_T_max   0.967
_shelx_estimated_absorpt_T_min   0.927
_exptl_absorpt_coefficient_mu    0.853
_exptl_absorpt_correction_T_max  1.00
_exptl_absorpt_correction_T_min  0.817
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.1202 before and 0.0853 after correction.
The Ratio of minimum to maximum transmission is 0.7824.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            red
_exptl_crystal_colour_primary    red
_exptl_crystal_density_diffrn    1.328
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             808
_exptl_crystal_size_max          0.09
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0378
_diffrn_reflns_av_unetI/netI     0.0355
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            26471
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         27.481
_diffrn_reflns_theta_min         2.819
_diffrn_ambient_temperature      100.0
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  ?
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                7965
_reflns_number_total             9102
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         0.655
_refine_diff_density_min         -0.343
_refine_diff_density_rms         0.061
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.070
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     649
_refine_ls_number_reflns         9102
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0403
_refine_ls_R_factor_gt           0.0334
_refine_ls_restrained_S_all      1.070
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0343P)²+1.3633P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0821
_refine_ls_wR_factor_ref         0.0850
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2.a Ternary CH refined with riding coordinates:
 C31A(H31A), C32A(H32A), C33A(H33A), C34A(H34A), C35A(H35A), C31C(H31C),
 C32C(H32C), C33C(H33C), C34C(H34C), C35C(H35C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1A C 0.7697(2) 0.10690(11) 0.36878(8) 0.0120(3) Uani 1 1 d . . . . .
C2A C 0.5600(3) 0.05300(12) 0.35755(8) 0.0141(3) Uani 1 1 d . . . . .
H2A H 0.434(3) 0.0880(15) 0.3706(10) 0.017 Uiso 1 1 d R . . . .
Co3A Co 0.68713(3) 0.10276(2) 0.27064(2) 0.01255(6) Uani 1 1 d . . . . .
B4A B 0.9500(3) 0.06647(14) 0.31237(10) 0.0159(4) Uani 1 1 d . . . . .
H4A H 1.071(3) 0.1088(15) 0.2987(10) 0.019 Uiso 1 1 d R . . . .
B5A B 0.9386(3) 0.02734(13) 0.39647(10) 0.0157(4) Uani 1 1 d . . . . .
H5A H 1.042(3) 0.0498(15) 0.4289(10) 0.019 Uiso 1 1 d R . . . .
B6A B 0.6871(3) 0.02093(13) 0.42497(10) 0.0151(4) Uani 1 1 d . . . . .
H6A H 0.631(3) 0.0412(15) 0.4725(10) 0.018 Uiso 1 1 d R . . . .
B7A B 0.5870(3) -0.02837(13) 0.29435(10) 0.0149(4) Uani 1 1 d . . . . .
H7A H 0.463(3) -0.0519(15) 0.2694(10) 0.018 Uiso 1 1 d R . . . .
B8A B 0.8460(3) -0.02253(14) 0.26479(11) 0.0182(4) Uani 1 1 d . . . . .
H8A H 0.904(3) -0.0429(15) 0.2182(11) 0.022 Uiso 1 1 d R . . . .
B9A B 0.9843(3) -0.05307(14) 0.33259(11) 0.0190(4) Uani 1 1 d . . . . .
H9A H 1.130(3) -0.0856(15) 0.3252(11) 0.023 Uiso 1 1 d R . . . .
B10A B 0.8189(3) -0.08057(14) 0.40158(11) 0.0180(4) Uani 1 1 d . . . . .
H10A H 0.855(3) -0.1322(15) 0.4420(10) 0.022 Uiso 1 1 d R . . . .
B11A B 0.5743(3) -0.06236(13) 0.37841(10) 0.0162(4) Uani 1 1 d . . . . .
H11A H 0.445(3) -0.0947(15) 0.4001(10) 0.019 Uiso 1 1 d R . . . .
B12A B 0.7584(3) -0.11065(14) 0.32153(11) 0.0183(4) Uani 1 1 d . . . . .
H12A H 0.753(3) -0.1834(15) 0.3063(11) 0.022 Uiso 1 1 d R . . . .
C31A C 0.4781(3) 0.11649(13) 0.20250(9) 0.0199(4) Uani 1 1 d . . . . .
H31A H 0.3578 0.0779 0.2007 0.024 Uiso 1 1 calc R . . . .
C32A C 0.4873(3) 0.20183(13) 0.23514(9) 0.0232(4) Uani 1 1 d . . . . .
H32A H 0.3762 0.2332 0.2618 0.028 Uiso 1 1 calc R . . . .
C33A C 0.6827(3) 0.23473(13) 0.22431(9) 0.0252(4) Uani 1 1 d . . . . .
H33A H 0.7332 0.2933 0.2423 0.030 Uiso 1 1 calc R . . . .
C34A C 0.7953(3) 0.16947(15) 0.18594(9) 0.0259(4) Uani 1 1 d . . . . .
H34A H 0.9374 0.1751 0.1700 0.031 Uiso 1 1 calc R . . . .
C35A C 0.6676(3) 0.09552(14) 0.17151(9) 0.0223(4) Uani 1 1 d . . . . .
H35A H 0.7036 0.0409 0.1429 0.027 Uiso 1 1 calc R . . . .
C1B C 0.7713(2) 0.20325(11) 0.40161(8) 0.0121(3) Uani 1 1 d . . . . .
C2B C 0.8194(3) 0.20787(12) 0.48128(8) 0.0148(3) Uani 1 1 d . . . . .
H2B H 0.838(3) 0.1514(15) 0.5014(10) 0.018 Uiso 1 1 d R . . . .
B3B B 1.0010(3) 0.24218(13) 0.42350(10) 0.0146(4) Uani 1 1 d . . . . .
H3B H 1.127(3) 0.1987(15) 0.4128(10) 0.017 Uiso 1 1 d R . . . .
B4B B 0.8712(3) 0.29937(13) 0.36265(10) 0.0148(4) Uani 1 1 d . . . . .
H4B H 0.933(3) 0.2930(14) 0.3134(10) 0.018 Uiso 1 1 d R . . . .
B5B B 0.6124(3) 0.29317(13) 0.38592(10) 0.0147(4) Uani 1 1 d . . . . .
H5B H 0.506(3) 0.2833(15) 0.3505(10) 0.018 Uiso 1 1 d R . . . .
B6B B 0.5815(3) 0.23090(14) 0.46154(10) 0.0151(4) Uani 1 1 d . . . . .
H6B H 0.472(3) 0.1821(15) 0.4716(10) 0.018 Uiso 1 1 d R . . . .
B7B B 0.9518(3) 0.30259(14) 0.49939(10) 0.0166(4) Uani 1 1 d . . . . .
H7B H 1.058(3) 0.2947(15) 0.5345(10) 0.020 Uiso 1 1 d R . . . .
B8B B 0.9820(3) 0.36418(14) 0.42338(10) 0.0162(4) Uani 1 1 d . . . . .
H8B H 1.112(3) 0.4058(15) 0.4101(10) 0.019 Uiso 1 1 d R . . . .
B9B B 0.7421(3) 0.39610(14) 0.40030(10) 0.0168(4) Uani 1 1 d . . . . .
H9B H 0.717(3) 0.4601(15) 0.3710(10) 0.020 Uiso 1 1 d R . . . .
B10B B 0.5640(3) 0.35288(14) 0.46171(10) 0.0178(4) Uani 1 1 d . . . . .
H10B H 0.424(3) 0.3834(15) 0.4753(10) 0.021 Uiso 1 1 d R . . . .
B11B B 0.6945(3) 0.29480(15) 0.52246(10) 0.0182(4) Uani 1 1 d . . . . .
H11B H 0.636(3) 0.2829(15) 0.5703(11) 0.022 Uiso 1 1 d R . . . .
B12B B 0.7920(3) 0.39758(14) 0.48514(10) 0.0184(4) Uani 1 1 d . . . . .
H12B H 0.799(3) 0.4614(15) 0.5130(11) 0.022 Uiso 1 1 d R . . . .
C1C C 0.2113(2) 0.60371(11) 0.13229(8) 0.0117(3) Uani 1 1 d . . . . .
C2C C 0.3975(3) 0.53698(12) 0.15096(9) 0.0144(3) Uani 1 1 d . . . . .
H2C H 0.528(3) 0.5623(15) 0.1430(10) 0.017 Uiso 1 1 d R . . . .
Co3C Co 0.25101(3) 0.59165(2) 0.23445(2) 0.01219(6) Uani 1 1 d . . . . .
B4C B 0.0040(3) 0.57354(14) 0.18181(10) 0.0144(4) Uani 1 1 d . . . . .
H4C H -0.107(3) 0.6242(15) 0.1922(10) 0.017 Uiso 1 1 d R . . . .
B5C B 0.0364(3) 0.53662(13) 0.09765(10) 0.0148(4) Uani 1 1 d . . . . .
H5C H -0.051(3) 0.5677(15) 0.0614(10) 0.018 Uiso 1 1 d R . . . .
B6C B 0.2898(3) 0.51461(13) 0.07792(10) 0.0144(4) Uani 1 1 d . . . . .
H6C H 0.368(3) 0.5322(14) 0.0335(10) 0.017 Uiso 1 1 d R . . . .
B7C B 0.3345(3) 0.45650(13) 0.21224(10) 0.0154(4) Uani 1 1 d . . . . .
H7C H 0.448(3) 0.4286(15) 0.2417(10) 0.018 Uiso 1 1 d R . . . .
B8C B 0.0715(3) 0.47613(14) 0.23240(10) 0.0160(4) Uani 1 1 d . . . . .
H8C H -0.009(3) 0.4569(15) 0.2780(10) 0.019 Uiso 1 1 d R . . . .
B9C B -0.0476(3) 0.45721(14) 0.15927(10) 0.0169(4) Uani 1 1 d . . . . .
H9C H -0.198(3) 0.4332(15) 0.1600(10) 0.020 Uiso 1 1 d R . . . .
B10C B 0.1311(3) 0.42150(13) 0.09584(10) 0.0161(4) Uani 1 1 d . . . . .
H10C H 0.098(3) 0.3756(15) 0.0572(10) 0.019 Uiso 1 1 d R . . . .
B11C B 0.3671(3) 0.42407(13) 0.12793(10) 0.0158(4) Uani 1 1 d . . . . .
H11C H 0.497(3) 0.3861(15) 0.1096(10) 0.019 Uiso 1 1 d R . . . .
B12C B 0.1575(3) 0.38551(13) 0.17796(10) 0.0164(4) Uani 1 1 d . . . . .
H12C H 0.142(3) 0.3142(15) 0.1946(10) 0.020 Uiso 1 1 d R . . . .
C31C C 0.3420(3) 0.57188(13) 0.32685(9) 0.0203(4) Uani 1 1 d . . . . .
H31C H 0.3830 0.5114 0.3461 0.024 Uiso 1 1 calc R . . . .
C32C C 0.4696(3) 0.63632(14) 0.29288(9) 0.0214(4) Uani 1 1 d . . . . .
H32C H 0.6153 0.6287 0.2830 0.026 Uiso 1 1 calc R . . . .
C33C C 0.3532(3) 0.71435(13) 0.27707(9) 0.0225(4) Uani 1 1 d . . . . .
H33C H 0.4019 0.7705 0.2523 0.027 Uiso 1 1 calc R . . . .
C34C C 0.1555(3) 0.69729(13) 0.29935(9) 0.0226(4) Uani 1 1 d . . . . .
H34C H 0.0408 0.7402 0.2943 0.027 Uiso 1 1 calc R . . . .
C35C C 0.1474(3) 0.60963(14) 0.33089(9) 0.0206(4) Uani 1 1 d . . . . .
H35C H 0.0274 0.5806 0.3534 0.025 Uiso 1 1 calc R . . . .
C1D C 0.2478(2) 0.70029(11) 0.10049(8) 0.0120(3) Uani 1 1 d . . . . .
C2D C 0.2161(3) 0.71128(12) 0.01996(8) 0.0140(3) Uani 1 1 d . . . . .
H2D H 0.179(3) 0.6581(15) -0.0012(10) 0.017 Uiso 1 1 d R . . . .
B3D B 0.0389(3) 0.75771(14) 0.07555(10) 0.0151(4) Uani 1 1 d . . . . .
H3D H -0.097(3) 0.7245(15) 0.0832(10) 0.018 Uiso 1 1 d R . . . .
B4D B 0.1755(3) 0.80206(13) 0.13897(10) 0.0160(4) Uani 1 1 d . . . . .
H4D H 0.105(3) 0.7990(15) 0.1887(10) 0.019 Uiso 1 1 d R . . . .
B5D B 0.4306(3) 0.77457(13) 0.11903(10) 0.0154(4) Uani 1 1 d . . . . .
H5D H 0.530(3) 0.7527(15) 0.1542(10) 0.018 Uiso 1 1 d R . . . .
B6D B 0.4533(3) 0.71452(14) 0.04339(10) 0.0154(4) Uani 1 1 d . . . . .
H6D H 0.548(3) 0.6582(15) 0.0334(10) 0.019 Uiso 1 1 d R . . . .
B7D B 0.1165(3) 0.81565(14) 0.00058(10) 0.0163(4) Uani 1 1 d . . . . .
H7D H 0.014(3) 0.8165(15) -0.0352(10) 0.020 Uiso 1 1 d R . . . .
B8D B 0.0937(3) 0.87698(14) 0.07645(10) 0.0164(4) Uani 1 1 d . . . . .
H8D H -0.020(3) 0.9277(15) 0.0860(10) 0.020 Uiso 1 1 d R . . . .
B9D B 0.3363(3) 0.88770(14) 0.10365(10) 0.0187(4) Uani 1 1 d . . . . .
H9D H 0.376(3) 0.9472(15) 0.1336(11) 0.022 Uiso 1 1 d R . . . .
B10D B 0.5070(3) 0.83343(14) 0.04445(11) 0.0186(4) Uani 1 1 d . . . . .
H10D H 0.653(3) 0.8528(15) 0.0354(11) 0.022 Uiso 1 1 d R . . . .
B11D B 0.3705(3) 0.78919(14) -0.01907(10) 0.0170(4) Uani 1 1 d . . . . .
H11D H 0.422(3) 0.7749(15) -0.0674(11) 0.020 Uiso 1 1 d R . . . .
B12D B 0.2990(3) 0.89674(14) 0.01783(10) 0.0179(4) Uani 1 1 d . . . . .
H12D H 0.316(3) 0.9623(15) -0.0089(10) 0.021 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1A C2A 1.667(2) . ?
C1A Co3A 2.1182(16) . ?
C1A B4A 1.713(3) . ?
C1A B5A 1.735(3) . ?
C1A B6A 1.752(3) . ?
C1A C1B 1.549(2) . ?
C2A H2A 1.01(2) . ?
C2A Co3A 2.0393(17) . ?
C2A B6A 1.735(3) . ?
C2A B7A 1.746(3) . ?
C2A B11A 1.721(3) . ?
Co3A B4A 2.096(2) . ?
Co3A B7A 2.0647(19) . ?
Co3A B8A 2.094(2) . ?
Co3A C31A 2.0682(18) . ?
Co3A C32A 2.1211(19) . ?
Co3A C33A 2.1229(18) . ?
Co3A C34A 2.0602(19) . ?
Co3A C35A 2.0360(18) . ?
B4A H4A 1.05(2) . ?
B4A B5A 1.796(3) . ?
B4A B8A 1.801(3) . ?
B4A B9A 1.789(3) . ?
B5A H5A 1.06(2) . ?
B5A B6A 1.766(3) . ?
B5A B9A 1.757(3) . ?
B5A B10A 1.768(3) . ?
B6A H6A 1.05(2) . ?
B6A B10A 1.757(3) . ?
B6A B11A 1.758(3) . ?
B7A H7A 1.08(2) . ?
B7A B8A 1.819(3) . ?
B7A B11A 1.773(3) . ?
B7A B12A 1.769(3) . ?
B8A H8A 1.04(2) . ?
B8A B9A 1.779(3) . ?
B8A B12A 1.791(3) . ?
B9A H9A 1.09(2) . ?
B9A B10A 1.777(3) . ?
B9A B12A 1.788(3) . ?
B10A H10A 1.15(2) . ?
B10A B11A 1.779(3) . ?
B10A B12A 1.770(3) . ?
B11A H11A 1.06(2) . ?
B11A B12A 1.777(3) . ?
B12A H12A 1.10(2) . ?
C31A H31A 1.0000 . ?
C31A C32A 1.409(3) . ?
C31A C35A 1.420(3) . ?
C32A H32A 1.0000 . ?
C32A C33A 1.418(3) . ?
C33A H33A 1.0000 . ?
C33A C34A 1.408(3) . ?
C34A H34A 1.0000 . ?
C34A C35A 1.433(3) . ?
C35A H35A 1.0000 . ?
C1B C2B 1.681(2) . ?
C1B B3B 1.758(3) . ?
C1B B4B 1.717(3) . ?
C1B B5B 1.722(3) . ?
C1B B6B 1.749(3) . ?
C2B H2B 0.92(2) . ?
C2B B3B 1.714(3) . ?
C2B B6B 1.724(3) . ?
C2B B7B 1.707(3) . ?
C2B B11B 1.696(3) . ?
B3B H3B 1.06(2) . ?
B3B B4B 1.769(3) . ?
B3B B7B 1.786(3) . ?
B3B B8B 1.766(3) . ?
B4B H4B 1.06(2) . ?
B4B B5B 1.789(3) . ?
B4B B8B 1.776(3) . ?
B4B B9B 1.785(3) . ?
B5B H5B 1.07(2) . ?
B5B B6B 1.778(3) . ?
B5B B9B 1.778(3) . ?
B5B B10B 1.779(3) . ?
B6B H6B 1.04(2) . ?
B6B B10B 1.765(3) . ?
B6B B11B 1.779(3) . ?
B7B H7B 1.06(2) . ?
B7B B8B 1.780(3) . ?
B7B B11B 1.780(3) . ?
B7B B12B 1.775(3) . ?
B8B H8B 1.09(2) . ?
B8B B9B 1.786(3) . ?
B8B B12B 1.795(3) . ?
B9B H9B 1.12(2) . ?
B9B B10B 1.788(3) . ?
B9B B12B 1.786(3) . ?
B10B H10B 1.06(2) . ?
B10B B11B 1.776(3) . ?
B10B B12B 1.787(3) . ?
B11B H11B 1.04(2) . ?
B11B B12B 1.777(3) . ?
B12B H12B 1.09(2) . ?
C1C C2C 1.646(2) . ?
C1C Co3C 2.1235(16) . ?
C1C B4C 1.728(3) . ?
C1C B5C 1.740(2) . ?
C1C B6C 1.754(2) . ?
C1C C1D 1.550(2) . ?
C2C H2C 0.97(2) . ?
C2C Co3C 2.0586(18) . ?
C2C B6C 1.742(3) . ?
C2C B7C 1.734(3) . ?
C2C B11C 1.721(3) . ?
Co3C B4C 2.082(2) . ?
Co3C B7C 2.0693(19) . ?
Co3C B8C 2.085(2) . ?
Co3C C31C 2.0424(17) . ?
Co3C C32C 2.0866(18) . ?
Co3C C33C 2.1285(18) . ?
Co3C C34C 2.0891(18) . ?
Co3C C35C 2.0508(18) . ?
B4C H4C 1.05(2) . ?
B4C B5C 1.794(3) . ?
B4C B8C 1.813(3) . ?
B4C B9C 1.793(3) . ?
B5C H5C 1.08(2) . ?
B5C B6C 1.764(3) . ?
B5C B9C 1.762(3) . ?
B5C B10C 1.775(3) . ?
B6C H6C 1.04(2) . ?
B6C B10C 1.756(3) . ?
B6C B11C 1.752(3) . ?
B7C H7C 1.08(2) . ?
B7C B8C 1.822(3) . ?
B7C B11C 1.779(3) . ?
B7C B12C 1.779(3) . ?
B8C H8C 1.08(2) . ?
B8C B9C 1.774(3) . ?
B8C B12C 1.784(3) . ?
B9C H9C 1.09(2) . ?
B9C B10C 1.777(3) . ?
B9C B12C 1.788(3) . ?
B10C H10C 1.07(2) . ?
B10C B11C 1.779(3) . ?
B10C B12C 1.769(3) . ?
B11C H11C 1.08(2) . ?
B11C B12C 1.780(3) . ?
B12C H12C 1.09(2) . ?
C31C H31C 1.0000 . ?
C31C C32C 1.421(3) . ?
C31C C35C 1.421(3) . ?
C32C H32C 1.0000 . ?
C32C C33C 1.418(3) . ?
C33C H33C 1.0000 . ?
C33C C34C 1.410(3) . ?
C34C H34C 1.0000 . ?
C34C C35C 1.416(3) . ?
C35C H35C 1.0000 . ?
C1D C2D 1.676(2) . ?
C1D B3D 1.742(3) . ?
C1D B4D 1.719(3) . ?
C1D B5D 1.720(3) . ?
C1D B6D 1.760(3) . ?
C2D H2D 0.93(2) . ?
C2D B3D 1.720(3) . ?
C2D B6D 1.718(3) . ?
C2D B7D 1.701(3) . ?
C2D B11D 1.701(3) . ?
B3D H3D 1.05(2) . ?
B3D B4D 1.777(3) . ?
B3D B7D 1.783(3) . ?
B3D B8D 1.770(3) . ?
B4D H4D 1.09(2) . ?
B4D B5D 1.790(3) . ?
B4D B8D 1.782(3) . ?
B4D B9D 1.775(3) . ?
B5D H5D 1.06(2) . ?
B5D B6D 1.768(3) . ?
B5D B9D 1.782(3) . ?
B5D B10D 1.781(3) . ?
B6D H6D 1.04(2) . ?
B6D B10D 1.763(3) . ?
B6D B11D 1.781(3) . ?
B7D H7D 1.05(2) . ?
B7D B8D 1.781(3) . ?
B7D B11D 1.778(3) . ?
B7D B12D 1.775(3) . ?
B8D H8D 1.06(2) . ?
B8D B9D 1.790(3) . ?
B8D B12D 1.790(3) . ?
B9D H9D 1.11(2) . ?
B9D B10D 1.785(3) . ?
B9D B12D 1.788(3) . ?
B10D H10D 1.04(2) . ?
B10D B11D 1.777(3) . ?
B10D B12D 1.790(3) . ?
B11D H11D 1.04(2) . ?
B11D B12D 1.776(3) . ?
B12D H12D 1.09(2) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2A C1A Co3A 63.90(8) . . ?
C2A C1A B4A 108.80(13) . . ?
C2A C1A B5A 109.03(13) . . ?
C2A C1A B6A 60.92(10) . . ?
B4A C1A Co3A 65.35(9) . . ?
B4A C1A B5A 62.76(11) . . ?
B4A C1A B6A 112.11(13) . . ?
B5A C1A Co3A 120.77(11) . . ?
B5A C1A B6A 60.85(11) . . ?
B6A C1A Co3A 119.57(11) . . ?
C1B C1A C2A 121.84(14) . . ?
C1B C1A Co3A 116.93(11) . . ?
C1B C1A B4A 124.27(14) . . ?
C1B C1A B5A 114.83(13) . . ?
C1B C1A B6A 111.76(13) . . ?
C1A C2A H2A 116.5(12) . . ?
C1A C2A Co3A 68.88(8) . . ?
C1A C2A B6A 61.97(10) . . ?
C1A C2A B7A 112.60(13) . . ?
C1A C2A B11A 111.46(13) . . ?
Co3A C2A H2A 110.4(12) . . ?
B6A C2A H2A 112.5(12) . . ?
B6A C2A Co3A 124.93(12) . . ?
B6A C2A B7A 112.34(13) . . ?
B7A C2A H2A 124.5(12) . . ?
B7A C2A Co3A 65.57(9) . . ?
B11A C2A H2A 118.3(12) . . ?
B11A C2A Co3A 121.81(12) . . ?
B11A C2A B6A 61.17(11) . . ?
B11A C2A B7A 61.51(11) . . ?
C1A Co3A C32A 121.28(7) . . ?
C1A Co3A C33A 113.47(7) . . ?
C2A Co3A C1A 47.22(6) . . ?
C2A Co3A B4A 83.27(8) . . ?
C2A Co3A B7A 50.36(7) . . ?
C2A Co3A B8A 85.91(8) . . ?
C2A Co3A C31A 110.09(7) . . ?
C2A Co3A C32A 106.86(8) . . ?
C2A Co3A C33A 132.98(8) . . ?
C2A Co3A C34A 172.26(8) . . ?
B4A Co3A C1A 47.95(7) . . ?
B4A Co3A C32A 151.96(8) . . ?
B4A Co3A C33A 115.61(8) . . ?
B7A Co3A C1A 85.51(7) . . ?
B7A Co3A B4A 87.98(8) . . ?
B7A Co3A B8A 51.86(8) . . ?
B7A Co3A C31A 90.03(8) . . ?
B7A Co3A C32A 118.85(8) . . ?
B7A Co3A C33A 155.90(8) . . ?
B8A Co3A C1A 85.04(7) . . ?
B8A Co3A B4A 50.91(8) . . ?
B8A Co3A C32A 152.93(8) . . ?
B8A Co3A C33A 140.13(9) . . ?
C31A Co3A C1A 151.10(7) . . ?
C31A Co3A B4A 160.51(8) . . ?
C31A Co3A B8A 114.18(8) . . ?
C31A Co3A C32A 39.29(7) . . ?
C31A Co3A C33A 66.12(7) . . ?
C32A Co3A C33A 39.05(8) . . ?
C34A Co3A C1A 131.90(7) . . ?
C34A Co3A B4A 100.88(8) . . ?
C34A Co3A B7A 135.74(8) . . ?
C34A Co3A B8A 101.79(9) . . ?
C34A Co3A C31A 67.67(8) . . ?
C34A Co3A C32A 66.50(9) . . ?
C34A Co3A C33A 39.30(9) . . ?
C35A Co3A C1A 168.35(8) . . ?
C35A Co3A C2A 141.56(7) . . ?
C35A Co3A B4A 120.72(8) . . ?
C35A Co3A B7A 97.57(8) . . ?
C35A Co3A B8A 88.04(8) . . ?
C35A Co3A C31A 40.47(8) . . ?
C35A Co3A C32A 66.98(8) . . ?
C35A Co3A C33A 66.95(8) . . ?
C35A Co3A C34A 40.94(8) . . ?
C1A B4A Co3A 66.70(9) . . ?
C1A B4A H4A 118.9(12) . . ?
C1A B4A B5A 59.23(11) . . ?
C1A B4A B8A 108.22(14) . . ?
C1A B4A B9A 105.52(14) . . ?
Co3A B4A H4A 115.2(12) . . ?
B5A B4A Co3A 118.92(12) . . ?
B5A B4A H4A 114.3(12) . . ?
B5A B4A B8A 107.41(14) . . ?
B8A B4A Co3A 64.48(9) . . ?
B8A B4A H4A 128.1(12) . . ?
B9A B4A Co3A 116.72(12) . . ?
B9A B4A H4A 121.2(12) . . ?
B9A B4A B5A 58.68(11) . . ?
B9A B4A B8A 59.42(11) . . ?
C1A B5A B4A 58.00(10) . . ?
C1A B5A H5A 118.8(12) . . ?
C1A B5A B6A 60.05(11) . . ?
C1A B5A B9A 105.99(14) . . ?
C1A B5A B10A 106.51(13) . . ?
B4A B5A H5A 121.0(12) . . ?
B6A B5A B4A 107.62(14) . . ?
B6A B5A H5A 119.2(12) . . ?
B6A B5A B10A 59.61(11) . . ?
B9A B5A B4A 60.49(12) . . ?
B9A B5A H5A 126.1(12) . . ?
B9A B5A B6A 108.18(14) . . ?
B9A B5A B10A 60.53(12) . . ?
B10A B5A B4A 108.45(14) . . ?
B10A B5A H5A 125.0(12) . . ?
C1A B6A B5A 59.11(10) . . ?
C1A B6A H6A 118.5(12) . . ?
C1A B6A B10A 106.29(14) . . ?
C1A B6A B11A 105.79(13) . . ?
C2A B6A C1A 57.11(10) . . ?
C2A B6A B5A 104.63(13) . . ?
C2A B6A H6A 119.2(11) . . ?
C2A B6A B10A 105.75(14) . . ?
C2A B6A B11A 59.03(11) . . ?
B5A B6A H6A 123.9(11) . . ?
B10A B6A B5A 60.26(12) . . ?
B10A B6A H6A 128.4(12) . . ?
B10A B6A B11A 60.82(11) . . ?
B11A B6A B5A 108.62(14) . . ?
B11A B6A H6A 123.0(12) . . ?
C2A B7A Co3A 64.07(8) . . ?
C2A B7A H7A 122.0(11) . . ?
C2A B7A B8A 104.38(13) . . ?
C2A B7A B11A 58.54(11) . . ?
C2A B7A B12A 104.54(14) . . ?
Co3A B7A H7A 116.8(12) . . ?
B8A B7A Co3A 64.90(9) . . ?
B8A B7A H7A 129.4(11) . . ?
B11A B7A Co3A 117.78(12) . . ?
B11A B7A H7A 112.5(11) . . ?
B11A B7A B8A 108.00(14) . . ?
B12A B7A Co3A 117.94(12) . . ?
B12A B7A H7A 119.1(12) . . ?
B12A B7A B8A 59.87(12) . . ?
B12A B7A B11A 60.21(12) . . ?
Co3A B8A H8A 116.9(12) . . ?
B4A B8A Co3A 64.60(9) . . ?
B4A B8A B7A 105.94(14) . . ?
B4A B8A H8A 123.9(12) . . ?
B7A B8A Co3A 63.24(9) . . ?
B7A B8A H8A 125.0(12) . . ?
B9A B8A Co3A 117.30(12) . . ?
B9A B8A B4A 59.97(11) . . ?
B9A B8A B7A 106.61(14) . . ?
B9A B8A H8A 117.0(12) . . ?
B9A B8A B12A 60.11(12) . . ?
B12A B8A Co3A 115.43(13) . . ?
B12A B8A B4A 107.03(14) . . ?
B12A B8A B7A 58.67(11) . . ?
B12A B8A H8A 118.0(12) . . ?
B4A B9A H9A 120.2(12) . . ?
B5A B9A B4A 60.84(11) . . ?
B5A B9A B8A 110.13(14) . . ?
B5A B9A H9A 119.1(11) . . ?
B5A B9A B10A 60.06(12) . . ?
B5A B9A B12A 107.85(15) . . ?
B8A B9A B4A 60.62(11) . . ?
B8A B9A H9A 121.4(11) . . ?
B8A B9A B12A 60.26(12) . . ?
B10A B9A B4A 108.36(14) . . ?
B10A B9A B8A 109.04(15) . . ?
B10A B9A H9A 121.8(12) . . ?
B10A B9A B12A 59.54(12) . . ?
B12A B9A B4A 107.65(14) . . ?
B12A B9A H9A 124.2(12) . . ?
B5A B10A B9A 59.41(12) . . ?
B5A B10A H10A 119.4(11) . . ?
B5A B10A B11A 107.58(14) . . ?
B5A B10A B12A 108.14(15) . . ?
B6A B10A B5A 60.12(11) . . ?
B6A B10A B9A 107.69(14) . . ?
B6A B10A H10A 118.2(11) . . ?
B6A B10A B11A 59.63(11) . . ?
B6A B10A B12A 108.14(14) . . ?
B9A B10A H10A 123.8(11) . . ?
B9A B10A B11A 107.93(14) . . ?
B11A B10A H10A 122.2(11) . . ?
B12A B10A B9A 60.55(12) . . ?
B12A B10A H10A 125.1(11) . . ?
B12A B10A B11A 60.07(12) . . ?
C2A B11A B6A 59.80(11) . . ?
C2A B11A B7A 59.95(11) . . ?
C2A B11A B10A 105.37(13) . . ?
C2A B11A H11A 118.4(12) . . ?
C2A B11A B12A 105.27(14) . . ?
B6A B11A B7A 109.93(14) . . ?
B6A B11A B10A 59.55(11) . . ?
B6A B11A H11A 117.9(11) . . ?
B6A B11A B12A 107.78(14) . . ?
B7A B11A B10A 108.34(15) . . ?
B7A B11A H11A 119.9(11) . . ?
B7A B11A B12A 59.77(12) . . ?
B10A B11A H11A 126.0(12) . . ?
B12A B11A B10A 59.71(12) . . ?
B12A B11A H11A 127.9(12) . . ?
B7A B12A B8A 61.46(12) . . ?
B7A B12A B9A 108.43(14) . . ?
B7A B12A B10A 108.97(14) . . ?
B7A B12A B11A 60.02(11) . . ?
B7A B12A H12A 120.6(11) . . ?
B8A B12A H12A 121.1(11) . . ?
B9A B12A B8A 59.63(12) . . ?
B9A B12A H12A 122.7(11) . . ?
B10A B12A B8A 108.83(14) . . ?
B10A B12A B9A 59.91(12) . . ?
B10A B12A B11A 60.22(12) . . ?
B10A B12A H12A 121.2(11) . . ?
B11A B12A B8A 109.11(14) . . ?
B11A B12A B9A 107.55(14) . . ?
B11A B12A H12A 121.2(11) . . ?
Co3A C31A H31A 125.8 . . ?
C32A C31A Co3A 72.38(10) . . ?
C32A C31A H31A 125.8 . . ?
C32A C31A C35A 108.42(17) . . ?
C35A C31A Co3A 68.54(10) . . ?
C35A C31A H31A 125.8 . . ?
Co3A C32A H32A 126.0 . . ?
C31A C32A Co3A 68.33(11) . . ?
C31A C32A H32A 126.0 . . ?
C31A C32A C33A 107.94(19) . . ?
C33A C32A Co3A 70.55(11) . . ?
C33A C32A H32A 126.0 . . ?
Co3A C33A H33A 125.7 . . ?
C32A C33A Co3A 70.41(10) . . ?
C32A C33A H33A 125.7 . . ?
C34A C33A Co3A 67.95(11) . . ?
C34A C33A C32A 108.47(17) . . ?
C34A C33A H33A 125.7 . . ?
Co3A C34A H34A 126.1 . . ?
C33A C34A Co3A 72.76(11) . . ?
C33A C34A H34A 126.1 . . ?
C33A C34A C35A 107.78(18) . . ?
C35A C34A Co3A 68.62(10) . . ?
C35A C34A H34A 126.1 . . ?
Co3A C35A H35A 126.3 . . ?
C31A C35A Co3A 70.99(10) . . ?
C31A C35A C34A 107.37(17) . . ?
C31A C35A H35A 126.3 . . ?
C34A C35A Co3A 70.44(10) . . ?
C34A C35A H35A 126.3 . . ?
C1A C1B C2B 117.96(13) . . ?
C1A C1B B3B 116.56(14) . . ?
C1A C1B B4B 123.25(14) . . ?
C1A C1B B5B 124.47(13) . . ?
C1A C1B B6B 118.17(13) . . ?
C2B C1B B3B 59.73(10) . . ?
C2B C1B B4B 107.82(12) . . ?
C2B C1B B5B 108.31(13) . . ?
C2B C1B B6B 60.29(11) . . ?
B4B C1B B3B 61.19(11) . . ?
B4B C1B B5B 62.71(11) . . ?
B4B C1B B6B 112.68(13) . . ?
B5B C1B B3B 112.33(13) . . ?
B5B C1B B6B 61.62(11) . . ?
B6B C1B B3B 111.73(13) . . ?
C1B C2B H2B 115.4(13) . . ?
C1B C2B B3B 62.37(10) . . ?
C1B C2B B6B 61.81(10) . . ?
C1B C2B B7B 113.17(13) . . ?
C1B C2B B11B 112.68(14) . . ?
B3B C2B H2B 116.5(13) . . ?
B3B C2B B6B 115.23(14) . . ?
B6B C2B H2B 115.1(13) . . ?
B7B C2B H2B 121.6(13) . . ?
B7B C2B B3B 62.95(11) . . ?
B7B C2B B6B 115.20(14) . . ?
B11B C2B H2B 120.7(13) . . ?
B11B C2B B3B 115.35(14) . . ?
B11B C2B B6B 62.70(12) . . ?
B11B C2B B7B 63.10(12) . . ?
C1B B3B H3B 118.0(11) . . ?
C1B B3B B4B 58.27(10) . . ?
C1B B3B B7B 105.85(14) . . ?
C1B B3B B8B 105.49(13) . . ?
C2B B3B C1B 57.90(10) . . ?
C2B B3B H3B 119.6(11) . . ?
C2B B3B B4B 104.07(14) . . ?
C2B B3B B7B 58.33(11) . . ?
C2B B3B B8B 104.27(14) . . ?
B4B B3B H3B 123.9(11) . . ?
B4B B3B B7B 108.14(14) . . ?
B7B B3B H3B 123.8(11) . . ?
B8B B3B H3B 129.6(11) . . ?
B8B B3B B4B 60.31(11) . . ?
B8B B3B B7B 60.12(11) . . ?
C1B B4B B3B 60.55(10) . . ?
C1B B4B H4B 118.6(11) . . ?
C1B B4B B5B 58.76(10) . . ?
C1B B4B B8B 106.82(13) . . ?
C1B B4B B9B 105.67(14) . . ?
B3B B4B H4B 116.0(11) . . ?
B3B B4B B5B 108.63(14) . . ?
B3B B4B B8B 59.76(11) . . ?
B3B B4B B9B 108.01(14) . . ?
B5B B4B H4B 123.7(11) . . ?
B8B B4B H4B 123.1(11) . . ?
B8B B4B B5B 108.10(14) . . ?
B8B B4B B9B 60.18(11) . . ?
B9B B4B H4B 128.3(11) . . ?
B9B B4B B5B 59.64(11) . . ?
C1B B5B B4B 58.53(10) . . ?
C1B B5B H5B 118.7(11) . . ?
C1B B5B B6B 59.95(11) . . ?
C1B B5B B9B 105.82(13) . . ?
C1B B5B B10B 106.21(13) . . ?
B4B B5B H5B 122.1(11) . . ?
B6B B5B B4B 107.97(14) . . ?
B6B B5B H5B 117.9(11) . . ?
B6B B5B B10B 59.52(11) . . ?
B9B B5B B4B 60.06(11) . . ?
B9B B5B H5B 127.2(12) . . ?
B9B B5B B6B 107.98(14) . . ?
B9B B5B B10B 60.35(12) . . ?
B10B B5B B4B 108.12(14) . . ?
B10B B5B H5B 124.5(11) . . ?
C1B B6B B5B 58.43(10) . . ?
C1B B6B H6B 117.6(12) . . ?
C1B B6B B10B 105.61(14) . . ?
C1B B6B B11B 105.62(14) . . ?
C2B B6B C1B 57.90(10) . . ?
C2B B6B B5B 103.94(14) . . ?
C2B B6B H6B 120.3(12) . . ?
C2B B6B B10B 103.96(14) . . ?
C2B B6B B11B 57.88(11) . . ?
B5B B6B H6B 123.3(12) . . ?
B5B B6B B11B 107.99(14) . . ?
B10B B6B B5B 60.27(11) . . ?
B10B B6B H6B 129.5(12) . . ?
B10B B6B B11B 60.16(12) . . ?
B11B B6B H6B 124.6(11) . . ?
C2B B7B B3B 58.72(11) . . ?
C2B B7B H7B 117.9(12) . . ?
C2B B7B B8B 104.00(13) . . ?
C2B B7B B11B 58.14(11) . . ?
C2B B7B B12B 104.15(14) . . ?
B3B B7B H7B 116.5(12) . . ?
B8B B7B B3B 59.38(11) . . ?
B8B B7B H7B 126.5(12) . . ?
B8B B7B B11B 108.18(14) . . ?
B11B B7B B3B 107.77(13) . . ?
B11B B7B H7B 121.5(12) . . ?
B12B B7B B3B 108.08(14) . . ?
B12B B7B H7B 129.8(12) . . ?
B12B B7B B8B 60.67(12) . . ?
B12B B7B B11B 59.99(12) . . ?
B3B B8B B4B 59.93(11) . . ?
B3B B8B B7B 60.50(11) . . ?
B3B B8B H8B 120.1(11) . . ?
B3B B8B B9B 108.13(14) . . ?
B3B B8B B12B 108.07(14) . . ?
B4B B8B B7B 108.15(14) . . ?
B4B B8B H8B 120.6(11) . . ?
B4B B8B B9B 60.16(11) . . ?
B4B B8B B12B 107.95(14) . . ?
B7B B8B H8B 121.9(11) . . ?
B7B B8B B9B 107.64(14) . . ?
B7B B8B B12B 59.53(12) . . ?
B9B B8B H8B 122.6(11) . . ?
B9B B8B B12B 59.85(12) . . ?
B12B B8B H8B 123.4(11) . . ?
B4B B9B B8B 59.65(11) . . ?
B4B B9B H9B 120.2(11) . . ?
B4B B9B B10B 107.93(14) . . ?
B4B B9B B12B 107.93(14) . . ?
B5B B9B B4B 60.30(11) . . ?
B5B B9B B8B 108.20(14) . . ?
B5B B9B H9B 120.6(11) . . ?
B5B B9B B10B 59.86(11) . . ?
B5B B9B B12B 108.11(14) . . ?
B8B B9B H9B 121.5(11) . . ?
B8B B9B B10B 108.22(14) . . ?
B8B B9B B12B 60.34(12) . . ?
B10B B9B H9B 122.8(11) . . ?
B12B B9B H9B 123.2(11) . . ?
B12B B9B B10B 60.02(12) . . ?
B5B B10B B9B 59.79(11) . . ?
B5B B10B H10B 121.7(12) . . ?
B5B B10B B12B 108.01(14) . . ?
B6B B10B B5B 60.21(11) . . ?
B6B B10B B9B 108.10(14) . . ?
B6B B10B H10B 117.6(12) . . ?
B6B B10B B11B 60.31(11) . . ?
B6B B10B B12B 108.42(14) . . ?
B9B B10B H10B 125.7(12) . . ?
B11B B10B B5B 108.07(14) . . ?
B11B B10B B9B 107.61(14) . . ?
B11B B10B H10B 119.4(12) . . ?
B11B B10B B12B 59.82(12) . . ?
B12B B10B B9B 59.95(12) . . ?
B12B B10B H10B 123.9(12) . . ?
C2B B11B B6B 59.43(11) . . ?
C2B B11B B7B 58.77(11) . . ?
C2B B11B B10B 104.66(14) . . ?
C2B B11B H11B 118.9(12) . . ?
C2B B11B B12B 104.53(14) . . ?
B6B B11B B7B 108.95(14) . . ?
B6B B11B H11B 114.4(12) . . ?
B7B B11B H11B 123.8(12) . . ?
B10B B11B B6B 59.54(11) . . ?
B10B B11B B7B 108.34(15) . . ?
B10B B11B H11B 123.7(12) . . ?
B10B B11B B12B 60.39(12) . . ?
B12B B11B B6B 108.26(14) . . ?
B12B B11B B7B 59.84(12) . . ?
B12B B11B H11B 130.0(12) . . ?
B7B B12B B8B 59.80(12) . . ?
B7B B12B B9B 107.83(14) . . ?
B7B B12B B10B 108.11(14) . . ?
B7B B12B B11B 60.17(12) . . ?
B7B B12B H12B 120.8(12) . . ?
B8B B12B H12B 122.1(12) . . ?
B9B B12B B8B 59.82(11) . . ?
B9B B12B B10B 60.03(12) . . ?
B9B B12B H12B 122.8(12) . . ?
B10B B12B B8B 107.81(14) . . ?
B10B B12B H12B 122.2(12) . . ?
B11B B12B B8B 107.64(14) . . ?
B11B B12B B9B 107.64(14) . . ?
B11B B12B B10B 59.78(12) . . ?
B11B B12B H12B 121.3(12) . . ?
C2C C1C Co3C 64.76(8) . . ?
C2C C1C B4C 108.85(13) . . ?
C2C C1C B5C 109.20(13) . . ?
C2C C1C B6C 61.52(10) . . ?
B4C C1C Co3C 64.48(8) . . ?
B4C C1C B5C 62.32(11) . . ?
B4C C1C B6C 111.82(13) . . ?
B5C C1C Co3C 119.86(11) . . ?
B5C C1C B6C 60.64(11) . . ?
B6C C1C Co3C 120.56(11) . . ?
C1D C1C C2C 120.74(14) . . ?
C1D C1C Co3C 116.54(11) . . ?
C1D C1C B4C 125.10(14) . . ?
C1D C1C B5C 115.87(13) . . ?
C1D C1C B6C 111.48(13) . . ?
C1C C2C H2C 116.7(13) . . ?
C1C C2C Co3C 68.91(8) . . ?
C1C C2C B6C 62.28(10) . . ?
C1C C2C B7C 113.48(13) . . ?
C1C C2C B11C 111.83(13) . . ?
Co3C C2C H2C 111.5(12) . . ?
B6C C2C H2C 112.1(12) . . ?
B6C C2C Co3C 124.90(12) . . ?
B7C C2C H2C 123.7(13) . . ?
B7C C2C Co3C 65.49(9) . . ?
B7C C2C B6C 112.66(13) . . ?
B11C C2C H2C 117.1(13) . . ?
B11C C2C Co3C 121.89(12) . . ?
B11C C2C B6C 60.79(11) . . ?
B11C C2C B7C 61.98(11) . . ?
C1C Co3C C33C 114.05(7) . . ?
C2C Co3C C1C 46.33(6) . . ?
C2C Co3C B4C 83.05(7) . . ?
C2C Co3C B7C 49.66(7) . . ?
C2C Co3C B8C 85.43(7) . . ?
C2C Co3C C32C 105.91(7) . . ?
C2C Co3C C33C 120.38(7) . . ?
C2C Co3C C34C 155.28(8) . . ?
B4C Co3C C1C 48.51(7) . . ?
B4C Co3C B8C 51.59(8) . . ?
B4C Co3C C32C 167.89(8) . . ?
B4C Co3C C33C 129.06(8) . . ?
B4C Co3C C34C 101.82(8) . . ?
B7C Co3C C1C 84.76(7) . . ?
B7C Co3C B4C 88.46(8) . . ?
B7C Co3C B8C 52.02(8) . . ?
B7C Co3C C32C 103.53(8) . . ?
B7C Co3C C33C 141.99(8) . . ?
B7C Co3C C34C 153.20(8) . . ?
B8C Co3C C1C 85.47(7) . . ?
B8C Co3C C32C 135.83(8) . . ?
B8C Co3C C33C 153.98(8) . . ?
B8C Co3C C34C 116.76(8) . . ?
C31C Co3C C1C 169.13(7) . . ?
C31C Co3C C2C 123.32(7) . . ?
C31C Co3C B4C 140.35(8) . . ?
C31C Co3C B7C 88.98(8) . . ?
C31C Co3C B8C 97.67(8) . . ?
C31C Co3C C32C 40.25(8) . . ?
C31C Co3C C33C 66.51(7) . . ?
C31C Co3C C34C 67.26(7) . . ?
C31C Co3C C35C 40.63(8) . . ?
C32C Co3C C1C 133.21(7) . . ?
C32C Co3C C33C 39.30(8) . . ?
C32C Co3C C34C 66.62(8) . . ?
C34C Co3C C1C 120.59(7) . . ?
C34C Co3C C33C 39.04(8) . . ?
C35C Co3C C1C 150.21(7) . . ?
C35C Co3C C2C 161.40(7) . . ?
C35C Co3C B4C 106.24(8) . . ?
C35C Co3C B7C 113.45(8) . . ?
C35C Co3C B8C 87.97(8) . . ?
C35C Co3C C32C 67.66(8) . . ?
C35C Co3C C33C 66.48(8) . . ?
C35C Co3C C34C 40.00(8) . . ?
C1C B4C Co3C 67.01(8) . . ?
C1C B4C H4C 118.5(12) . . ?
C1C B4C B5C 59.15(10) . . ?
C1C B4C B8C 107.49(13) . . ?
C1C B4C B9C 105.25(14) . . ?
Co3C B4C H4C 113.1(11) . . ?
B5C B4C Co3C 119.33(12) . . ?
B5C B4C H4C 115.6(11) . . ?
B5C B4C B8C 106.99(14) . . ?
B8C B4C Co3C 64.30(9) . . ?
B8C B4C H4C 128.4(11) . . ?
B9C B4C Co3C 116.51(12) . . ?
B9C B4C H4C 123.2(11) . . ?
B9C B4C B5C 58.85(11) . . ?
B9C B4C B8C 58.92(11) . . ?
C1C B5C B4C 58.52(10) . . ?
C1C B5C H5C 118.6(11) . . ?
C1C B5C B6C 60.08(10) . . ?
C1C B5C B9C 106.07(13) . . ?
C1C B5C B10C 106.36(13) . . ?
B4C B5C H5C 120.0(11) . . ?
B6C B5C B4C 108.27(13) . . ?
B6C B5C H5C 119.6(11) . . ?
B6C B5C B10C 59.50(11) . . ?
B9C B5C B4C 60.53(11) . . ?
B9C B5C H5C 126.0(11) . . ?
B9C B5C B6C 108.06(14) . . ?
B9C B5C B10C 60.32(12) . . ?
B10C B5C B4C 108.60(14) . . ?
B10C B5C H5C 125.6(11) . . ?
C1C B6C B5C 59.28(10) . . ?
C1C B6C H6C 118.4(12) . . ?
C1C B6C B10C 106.56(14) . . ?
C2C B6C C1C 56.20(10) . . ?
C2C B6C B5C 103.90(13) . . ?
C2C B6C H6C 118.2(11) . . ?
C2C B6C B10C 105.53(14) . . ?
C2C B6C B11C 59.02(11) . . ?
B5C B6C H6C 125.3(11) . . ?
B10C B6C B5C 60.57(11) . . ?
B10C B6C H6C 129.2(11) . . ?
B11C B6C C1C 105.41(13) . . ?
B11C B6C B5C 108.84(14) . . ?
B11C B6C H6C 122.0(12) . . ?
B11C B6C B10C 60.97(11) . . ?
C2C B7C Co3C 64.85(9) . . ?
C2C B7C H7C 119.5(11) . . ?
C2C B7C B8C 104.47(13) . . ?
C2C B7C B11C 58.65(11) . . ?
C2C B7C B12C 104.44(13) . . ?
Co3C B7C H7C 114.2(11) . . ?
B8C B7C Co3C 64.44(9) . . ?
B8C B7C H7C 130.7(11) . . ?
B11C B7C Co3C 118.35(12) . . ?
B11C B7C H7C 113.5(11) . . ?
B11C B7C B8C 107.60(14) . . ?
B12C B7C Co3C 117.28(12) . . ?
B12C B7C H7C 122.5(11) . . ?
B12C B7C B8C 59.40(11) . . ?
B12C B7C B11C 60.05(11) . . ?
Co3C B8C H8C 116.9(11) . . ?
B4C B8C Co3C 64.11(9) . . ?
B4C B8C B7C 105.61(13) . . ?
B4C B8C H8C 123.7(12) . . ?
B7C B8C Co3C 63.54(9) . . ?
B7C B8C H8C 125.6(11) . . ?
B9C B8C Co3C 117.24(12) . . ?
B9C B8C B4C 59.96(11) . . ?
B9C B8C B7C 106.92(14) . . ?
B9C B8C H8C 116.4(11) . . ?
B9C B8C B12C 60.36(11) . . ?
B12C B8C Co3C 116.23(12) . . ?
B12C B8C B4C 107.25(14) . . ?
B12C B8C B7C 59.10(11) . . ?
B12C B8C H8C 117.7(12) . . ?
B4C B9C H9C 120.9(11) . . ?
B5C B9C B4C 60.62(11) . . ?
B5C B9C B8C 110.19(14) . . ?
B5C B9C H9C 118.7(11) . . ?
B5C B9C B10C 60.19(11) . . ?
B5C B9C B12C 107.78(14) . . ?
B8C B9C B4C 61.12(11) . . ?
B8C B9C H9C 122.4(11) . . ?
B8C B9C B10C 109.06(14) . . ?
B8C B9C B12C 60.11(11) . . ?
B10C B9C B4C 108.58(14) . . ?
B10C B9C H9C 120.4(11) . . ?
B10C B9C B12C 59.49(11) . . ?
B12C B9C B4C 107.96(14) . . ?
B12C B9C H9C 124.0(12) . . ?
B5C B10C B9C 59.49(11) . . ?
B5C B10C H10C 120.2(12) . . ?
B5C B10C B11C 107.11(13) . . ?
B6C B10C B5C 59.93(11) . . ?
B6C B10C B9C 107.73(13) . . ?
B6C B10C H10C 119.7(11) . . ?
B6C B10C B11C 59.40(11) . . ?
B6C B10C B12C 108.18(14) . . ?
B9C B10C H10C 122.7(11) . . ?
B9C B10C B11C 107.93(14) . . ?
B11C B10C H10C 122.7(11) . . ?
B12C B10C B5C 108.08(14) . . ?
B12C B10C B9C 60.58(12) . . ?
B12C B10C H10C 123.8(12) . . ?
B12C B10C B11C 60.21(11) . . ?
C2C B11C B6C 60.19(11) . . ?
C2C B11C B7C 59.36(11) . . ?
C2C B11C B10C 105.41(14) . . ?
C2C B11C H11C 117.3(11) . . ?
C2C B11C B12C 104.92(14) . . ?
B6C B11C B7C 110.00(14) . . ?
B6C B11C B10C 59.63(11) . . ?
B6C B11C H11C 116.3(11) . . ?
B6C B11C B12C 107.88(14) . . ?
B7C B11C B10C 108.40(14) . . ?
B7C B11C H11C 120.5(11) . . ?
B7C B11C B12C 59.97(11) . . ?
B10C B11C H11C 126.4(11) . . ?
B10C B11C B12C 59.61(11) . . ?
B12C B11C H11C 129.5(12) . . ?
B7C B12C B8C 61.51(11) . . ?
B7C B12C B9C 108.16(14) . . ?
B7C B12C B11C 59.98(11) . . ?
B7C B12C H12C 119.1(11) . . ?
B8C B12C B9C 59.53(11) . . ?
B8C B12C H12C 118.9(11) . . ?
B9C B12C H12C 123.2(11) . . ?
B10C B12C B7C 108.87(14) . . ?
B10C B12C B8C 108.95(14) . . ?
B10C B12C B9C 59.93(11) . . ?
B10C B12C B11C 60.18(11) . . ?
B10C B12C H12C 123.5(11) . . ?
B11C B12C B8C 109.23(13) . . ?
B11C B12C B9C 107.40(14) . . ?
B11C B12C H12C 122.3(11) . . ?
Co3C C31C H31C 125.8 . . ?
C32C C31C Co3C 71.55(10) . . ?
C32C C31C H31C 125.8 . . ?
C35C C31C Co3C 70.00(10) . . ?
C35C C31C H31C 125.8 . . ?
C35C C31C C32C 108.29(17) . . ?
Co3C C32C H32C 126.3 . . ?
C31C C32C Co3C 68.20(10) . . ?
C31C C32C H32C 126.3 . . ?
C33C C32C Co3C 71.94(11) . . ?
C33C C32C C31C 107.41(17) . . ?
C33C C32C H32C 126.3 . . ?
Co3C C33C H33C 125.8 . . ?
C32C C33C Co3C 68.76(10) . . ?
C32C C33C H33C 125.8 . . ?
C34C C33C Co3C 68.97(10) . . ?
C34C C33C C32C 108.39(17) . . ?
C34C C33C H33C 125.8 . . ?
Co3C C34C H34C 125.8 . . ?
C33C C34C Co3C 71.99(10) . . ?
C33C C34C H34C 125.8 . . ?
C33C C34C C35C 108.37(17) . . ?
C35C C34C Co3C 68.54(10) . . ?
C35C C34C H34C 125.8 . . ?
Co3C C35C H35C 126.2 . . ?
C31C C35C Co3C 69.37(10) . . ?
C31C C35C H35C 126.2 . . ?
C34C C35C Co3C 71.46(10) . . ?
C34C C35C C31C 107.52(17) . . ?
C34C C35C H35C 126.2 . . ?
C1C C1D C2D 117.23(13) . . ?
C1C C1D B3D 115.48(13) . . ?
C1C C1D B4D 123.24(14) . . ?
C1C C1D B5D 125.18(14) . . ?
C1C C1D B6D 118.72(14) . . ?
C2D C1D B3D 60.38(10) . . ?
C2D C1D B4D 108.56(13) . . ?
C2D C1D B5D 108.04(13) . . ?
C2D C1D B6D 59.94(10) . . ?
B3D C1D B6D 111.93(13) . . ?
B4D C1D B3D 61.76(11) . . ?
B4D C1D B5D 62.74(11) . . ?
B4D C1D B6D 112.29(13) . . ?
B5D C1D B3D 112.90(13) . . ?
B5D C1D B6D 61.05(11) . . ?
C1D C2D H2D 116.1(13) . . ?
C1D C2D B3D 61.72(10) . . ?
C1D C2D B6D 62.47(11) . . ?
C1D C2D B7D 112.73(13) . . ?
C1D C2D B11D 113.14(13) . . ?
B3D C2D H2D 115.1(13) . . ?
B6D C2D H2D 117.1(13) . . ?
B6D C2D B3D 115.19(13) . . ?
B7D C2D H2D 119.9(13) . . ?
B7D C2D B3D 62.83(11) . . ?
B7D C2D B6D 115.19(14) . . ?
B7D C2D B11D 63.03(12) . . ?
B11D C2D H2D 121.2(13) . . ?
B11D C2D B3D 115.21(14) . . ?
B11D C2D B6D 62.79(11) . . ?
C1D B3D H3D 117.9(12) . . ?
C1D B3D B4D 58.46(10) . . ?
C1D B3D B7D 105.77(14) . . ?
C1D B3D B8D 105.77(14) . . ?
C2D B3D C1D 57.90(10) . . ?
C2D B3D H3D 118.8(12) . . ?
C2D B3D B4D 104.04(14) . . ?
C2D B3D B7D 58.06(11) . . ?
C2D B3D B8D 104.19(14) . . ?
B4D B3D H3D 124.9(11) . . ?
B4D B3D B7D 108.08(14) . . ?
B7D B3D H3D 123.1(12) . . ?
B8D B3D H3D 129.9(12) . . ?
B8D B3D B4D 60.33(11) . . ?
B8D B3D B7D 60.19(11) . . ?
C1D B4D B3D 59.77(10) . . ?
C1D B4D H4D 118.7(11) . . ?
C1D B4D B5D 58.66(10) . . ?
C1D B4D B8D 106.25(13) . . ?
C1D B4D B9D 105.75(14) . . ?
B3D B4D H4D 116.3(11) . . ?
B3D B4D B5D 108.00(14) . . ?
B3D B4D B8D 59.64(11) . . ?
B5D B4D H4D 123.6(11) . . ?
B8D B4D H4D 123.3(11) . . ?
B8D B4D B5D 108.29(14) . . ?
B9D B4D B3D 107.98(14) . . ?
B9D B4D H4D 128.3(11) . . ?
B9D B4D B5D 59.99(12) . . ?
B9D B4D B8D 60.42(12) . . ?
C1D B5D B4D 58.60(11) . . ?
C1D B5D H5D 118.3(12) . . ?
C1D B5D B6D 60.60(11) . . ?
C1D B5D B9D 105.38(14) . . ?
C1D B5D B10D 106.49(14) . . ?
B4D B5D H5D 124.1(11) . . ?
B6D B5D B4D 108.59(14) . . ?
B6D B5D H5D 115.4(12) . . ?
B6D B5D B9D 107.87(14) . . ?
B6D B5D B10D 59.57(11) . . ?
B9D B5D B4D 59.58(12) . . ?
B9D B5D H5D 129.1(12) . . ?
B10D B5D B4D 107.89(14) . . ?
B10D B5D H5D 123.4(11) . . ?
B10D B5D B9D 60.12(12) . . ?
C1D B6D B5D 58.35(10) . . ?
C1D B6D H6D 118.6(12) . . ?
C1D B6D B10D 105.54(14) . . ?
C1D B6D B11D 105.46(14) . . ?
C2D B6D C1D 57.59(10) . . ?
C2D B6D B5D 104.04(14) . . ?
C2D B6D H6D 119.4(12) . . ?
C2D B6D B10D 104.20(14) . . ?
C2D B6D B11D 58.14(11) . . ?
B5D B6D H6D 124.4(12) . . ?
B5D B6D B11D 108.36(14) . . ?
B10D B6D B5D 60.58(12) . . ?
B10D B6D H6D 129.4(12) . . ?
B10D B6D B11D 60.18(12) . . ?
B11D B6D H6D 123.1(12) . . ?
C2D B7D B3D 59.10(11) . . ?
C2D B7D H7D 117.2(12) . . ?
C2D B7D B8D 104.48(13) . . ?
C2D B7D B11D 58.49(11) . . ?
C2D B7D B12D 104.36(14) . . ?
B3D B7D H7D 115.1(12) . . ?
B8D B7D B3D 59.52(11) . . ?
B8D B7D H7D 125.9(12) . . ?
B11D B7D B3D 108.40(14) . . ?
B11D B7D H7D 122.0(12) . . ?
B11D B7D B8D 108.33(14) . . ?
B12D B7D B3D 108.07(14) . . ?
B12D B7D H7D 130.8(12) . . ?
B12D B7D B8D 60.43(12) . . ?
B12D B7D B11D 59.96(12) . . ?
B3D B8D B4D 60.03(11) . . ?
B3D B8D B7D 60.29(11) . . ?
B3D B8D H8D 121.0(12) . . ?
B3D B8D B9D 107.63(14) . . ?
B3D B8D B12D 108.04(14) . . ?
B4D B8D H8D 122.5(12) . . ?
B4D B8D B9D 59.59(11) . . ?
B4D B8D B12D 107.77(15) . . ?
B7D B8D B4D 107.92(14) . . ?
B7D B8D H8D 120.9(11) . . ?
B7D B8D B9D 107.40(14) . . ?
B7D B8D B12D 59.62(11) . . ?
B9D B8D H8D 123.1(11) . . ?
B9D B8D B12D 59.95(12) . . ?
B12D B8D H8D 121.7(12) . . ?
B4D B9D B5D 60.43(11) . . ?
B4D B9D B8D 59.99(11) . . ?
B4D B9D H9D 119.9(11) . . ?
B4D B9D B10D 108.41(14) . . ?
B4D B9D B12D 108.15(14) . . ?
B5D B9D B8D 108.30(14) . . ?
B5D B9D H9D 120.8(12) . . ?
B5D B9D B10D 59.91(12) . . ?
B5D B9D B12D 108.08(14) . . ?
B8D B9D H9D 121.4(12) . . ?
B10D B9D B8D 108.27(14) . . ?
B10D B9D H9D 122.7(11) . . ?
B10D B9D B12D 60.15(12) . . ?
B12D B9D B8D 60.03(12) . . ?
B12D B9D H9D 123.2(12) . . ?
B5D B10D B9D 59.97(12) . . ?
B5D B10D H10D 119.8(12) . . ?
B5D B10D B12D 108.04(15) . . ?
B6D B10D B5D 59.85(11) . . ?
B6D B10D B9D 107.98(14) . . ?
B6D B10D H10D 118.0(12) . . ?
B6D B10D B11D 60.42(11) . . ?
B6D B10D B12D 108.26(14) . . ?
B9D B10D H10D 124.1(12) . . ?
B9D B10D B12D 60.03(12) . . ?
B11D B10D B5D 107.98(14) . . ?
B11D B10D B9D 107.70(15) . . ?
B11D B10D H10D 121.5(12) . . ?
B11D B10D B12D 59.70(12) . . ?
B12D B10D H10D 125.0(12) . . ?
C2D B11D B6D 59.07(11) . . ?
C2D B11D B7D 58.48(11) . . ?
C2D B11D B10D 104.30(14) . . ?
C2D B11D H11D 117.3(12) . . ?
C2D B11D B12D 104.34(14) . . ?
B6D B11D H11D 116.9(12) . . ?
B7D B11D B6D 108.37(14) . . ?
B7D B11D H11D 120.3(12) . . ?
B10D B11D B6D 59.40(11) . . ?
B10D B11D B7D 108.30(15) . . ?
B10D B11D H11D 127.2(12) . . ?
B12D B11D B6D 108.10(14) . . ?
B12D B11D B7D 59.94(12) . . ?
B12D B11D B10D 60.53(12) . . ?
B12D B11D H11D 129.6(12) . . ?
B7D B12D B8D 59.95(11) . . ?
B7D B12D B9D 107.71(14) . . ?
B7D B12D B10D 107.83(14) . . ?
B7D B12D B11D 60.11(11) . . ?
B7D B12D H12D 122.0(11) . . ?
B8D B12D B10D 108.00(14) . . ?
B8D B12D H12D 121.5(12) . . ?
B9D B12D B8D 60.02(12) . . ?
B9D B12D B10D 59.82(12) . . ?
B9D B12D H12D 121.7(11) . . ?
B10D B12D H12D 121.8(11) . . ?
B11D B12D B8D 108.07(14) . . ?
B11D B12D B9D 107.59(14) . . ?
B11D B12D B10D 59.77(12) . . ?
B11D B12D H12D 122.1(11) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1A C2A B6A B5A -36.80(12) . . . . ?
C1A C2A B6A B10A -99.48(14) . . . . ?
C1A C2A B6A B11A -140.00(14) . . . . ?
C1A C2A B7A Co3A -51.85(11) . . . . ?
C1A C2A B7A B8A 0.45(18) . . . . ?
C1A C2A B7A B11A 103.00(15) . . . . ?
C1A C2A B7A B12A 62.49(17) . . . . ?
C1A C2A B11A B6A 37.56(13) . . . . ?
C1A C2A B11A B7A -104.86(14) . . . . ?
C1A C2A B11A B10A -2.26(18) . . . . ?
C1A C2A B11A B12A -64.40(16) . . . . ?
C1A B4A B5A B6A 35.30(12) . . . . ?
C1A B4A B5A B9A 136.63(14) . . . . ?
C1A B4A B5A B10A 98.33(15) . . . . ?
C1A B4A B8A Co3A 51.79(11) . . . . ?
C1A B4A B8A B7A 2.64(18) . . . . ?
C1A B4A B8A B9A -97.63(15) . . . . ?
C1A B4A B8A B12A -58.81(17) . . . . ?
C1A B4A B9A B5A -37.77(13) . . . . ?
C1A B4A B9A B8A 102.28(15) . . . . ?
C1A B4A B9A B10A 0.30(18) . . . . ?
C1A B4A B9A B12A 63.23(17) . . . . ?
C1A B5A B6A C2A 35.89(11) . . . . ?
C1A B5A B6A B10A 135.91(14) . . . . ?
C1A B5A B6A B11A 97.64(14) . . . . ?
C1A B5A B9A B4A 37.29(12) . . . . ?
C1A B5A B9A B8A 0.71(19) . . . . ?
C1A B5A B9A B10A -100.24(14) . . . . ?
C1A B5A B9A B12A -63.37(17) . . . . ?
C1A B5A B10A B6A -38.96(13) . . . . ?
C1A B5A B10A B9A 99.35(15) . . . . ?
C1A B5A B10A B11A -1.48(19) . . . . ?
C1A B5A B10A B12A 61.97(18) . . . . ?
C1A B6A B10A B5A 38.47(12) . . . . ?
C1A B6A B10A B9A 1.53(18) . . . . ?
C1A B6A B10A B11A -99.29(14) . . . . ?
C1A B6A B10A B12A -62.46(17) . . . . ?
C1A B6A B11A C2A -34.12(12) . . . . ?
C1A B6A B11A B7A 0.05(18) . . . . ?
C1A B6A B11A B10A 100.13(15) . . . . ?
C1A B6A B11A B12A 63.55(17) . . . . ?
C1A C1B C2B B3B 106.04(16) . . . . ?
C1A C1B C2B B6B -108.21(16) . . . . ?
C1A C1B C2B B7B 144.57(15) . . . . ?
C1A C1B C2B B11B -146.20(15) . . . . ?
C1A C1B B3B C2B -108.37(15) . . . . ?
C1A C1B B3B B4B 115.13(16) . . . . ?
C1A C1B B3B B7B -143.04(14) . . . . ?
C1A C1B B3B B8B 154.26(14) . . . . ?
C1A C1B B4B B3B -104.45(17) . . . . ?
C1A C1B B4B B5B 115.04(17) . . . . ?
C1A C1B B4B B8B -143.64(15) . . . . ?
C1A C1B B4B B9B 153.40(15) . . . . ?
C1A C1B B5B B4B -113.22(17) . . . . ?
C1A C1B B5B B6B 106.26(17) . . . . ?
C1A C1B B5B B9B -151.81(15) . . . . ?
C1A C1B B5B B10B 145.14(15) . . . . ?
C1A C1B B6B C2B 107.87(16) . . . . ?
C1A C1B B6B B5B -116.13(16) . . . . ?
C1A C1B B6B B10B -155.22(14) . . . . ?
C1A C1B B6B B11B 142.06(15) . . . . ?
C2A C1A B4A Co3A 48.13(10) . . . . ?
C2A C1A B4A B5A -102.25(14) . . . . ?
C2A C1A B4A B8A -2.41(18) . . . . ?
C2A C1A B4A B9A -64.74(16) . . . . ?
C2A C1A B5A B4A 101.88(14) . . . . ?
C2A C1A B5A B6A -38.65(13) . . . . ?
C2A C1A B5A B9A 63.44(16) . . . . ?
C2A C1A B5A B10A 0.11(18) . . . . ?
C2A C1A B6A B5A 137.51(14) . . . . ?
C2A C1A B6A B10A 98.50(14) . . . . ?
C2A C1A B6A B11A 34.94(13) . . . . ?
C2A C1A C1B C2B 100.84(17) . . . . ?
C2A C1A C1B B3B 168.97(14) . . . . ?
C2A C1A C1B B4B -119.49(17) . . . . ?
C2A C1A C1B B5B -41.9(2) . . . . ?
C2A C1A C1B B6B 31.5(2) . . . . ?
C2A B6A B10A B5A 98.11(14) . . . . ?
C2A B6A B10A B9A 61.17(17) . . . . ?
C2A B6A B10A B11A -39.65(13) . . . . ?
C2A B6A B10A B12A -2.82(18) . . . . ?
C2A B6A B11A B7A 34.16(13) . . . . ?
C2A B6A B11A B10A 134.25(15) . . . . ?
C2A B6A B11A B12A 97.67(15) . . . . ?
C2A B7A B8A Co3A -51.79(10) . . . . ?
C2A B7A B8A B4A -1.85(17) . . . . ?
C2A B7A B8A B9A 60.89(16) . . . . ?
C2A B7A B8A B12A 98.68(14) . . . . ?
C2A B7A B11A B6A -34.11(13) . . . . ?
C2A B7A B11A B10A -97.51(14) . . . . ?
C2A B7A B11A B12A -133.58(14) . . . . ?
C2A B7A B12A B8A -98.40(14) . . . . ?
C2A B7A B12A B9A -60.38(17) . . . . ?
C2A B7A B12A B10A 3.24(18) . . . . ?
C2A B7A B12A B11A 39.67(12) . . . . ?
C2A B11A B12A B7A -40.54(12) . . . . ?
C2A B11A B12A B8A -2.14(18) . . . . ?
C2A B11A B12A B9A 61.01(17) . . . . ?
C2A B11A B12A B10A 99.13(14) . . . . ?
Co3A C1A C2A B6A 154.31(11) . . . . ?
Co3A C1A C2A B7A 50.13(11) . . . . ?
Co3A C1A C2A B11A 117.08(13) . . . . ?
Co3A C1A B4A B5A -150.37(11) . . . . ?
Co3A C1A B4A B8A -50.54(11) . . . . ?
Co3A C1A B4A B9A -112.86(12) . . . . ?
Co3A C1A B5A B4A 31.53(12) . . . . ?
Co3A C1A B5A B6A -109.00(13) . . . . ?
Co3A C1A B5A B9A -6.91(18) . . . . ?
Co3A C1A B5A B10A -70.24(16) . . . . ?
Co3A C1A B6A C2A -26.59(12) . . . . ?
Co3A C1A B6A B5A 110.92(13) . . . . ?
Co3A C1A B6A B10A 71.91(15) . . . . ?
Co3A C1A B6A B11A 8.35(18) . . . . ?
Co3A C1A C1B C2B 175.46(11) . . . . ?
Co3A C1A C1B B3B -116.42(13) . . . . ?
Co3A C1A C1B B4B -44.87(19) . . . . ?
Co3A C1A C1B B5B 32.7(2) . . . . ?
Co3A C1A C1B B6B 106.07(14) . . . . ?
Co3A C2A B6A C1A 29.55(12) . . . . ?
Co3A C2A B6A B5A -7.25(18) . . . . ?
Co3A C2A B6A B10A -69.93(16) . . . . ?
Co3A C2A B6A B11A -110.45(15) . . . . ?
Co3A C2A B7A B8A 52.30(10) . . . . ?
Co3A C2A B7A B11A 154.84(12) . . . . ?
Co3A C2A B7A B12A 114.34(13) . . . . ?
Co3A C2A B11A B6A 115.33(14) . . . . ?
Co3A C2A B11A B7A -27.09(12) . . . . ?
Co3A C2A B11A B10A 75.51(16) . . . . ?
Co3A C2A B11A B12A 13.36(18) . . . . ?
Co3A B4A B5A C1A -31.25(11) . . . . ?
Co3A B4A B5A B6A 4.05(18) . . . . ?
Co3A B4A B5A B9A 105.38(14) . . . . ?
Co3A B4A B5A B10A 67.08(17) . . . . ?
Co3A B4A B8A B7A -49.15(11) . . . . ?
Co3A B4A B8A B9A -149.42(13) . . . . ?
Co3A B4A B8A B12A -110.60(13) . . . . ?
Co3A B4A B9A B5A -109.12(14) . . . . ?
Co3A B4A B9A B8A 30.93(13) . . . . ?
Co3A B4A B9A B10A -71.05(17) . . . . ?
Co3A B4A B9A B12A -8.11(19) . . . . ?
Co3A B7A B8A B4A 49.94(11) . . . . ?
Co3A B7A B8A B9A 112.68(13) . . . . ?
Co3A B7A B8A B12A 150.47(12) . . . . ?
Co3A B7A B11A C2A 25.60(12) . . . . ?
Co3A B7A B11A B6A -8.51(19) . . . . ?
Co3A B7A B11A B10A -71.91(16) . . . . ?
Co3A B7A B11A B12A -107.98(14) . . . . ?
Co3A B7A B12A B8A -30.35(13) . . . . ?
Co3A B7A B12A B9A 7.7(2) . . . . ?
Co3A B7A B12A B10A 71.28(18) . . . . ?
Co3A B7A B12A B11A 107.72(14) . . . . ?
Co3A B8A B9A B4A -31.14(13) . . . . ?
Co3A B8A B9A B5A 5.5(2) . . . . ?
Co3A B8A B9A B10A 69.69(17) . . . . ?
Co3A B8A B9A B12A 105.12(15) . . . . ?
Co3A B8A B12A B7A 29.17(12) . . . . ?
Co3A B8A B12A B9A -108.21(14) . . . . ?
Co3A B8A B12A B10A -72.68(17) . . . . ?
Co3A B8A B12A B11A -8.61(18) . . . . ?
Co3A C31A C32A C33A 59.64(13) . . . . ?
Co3A C31A C35A C34A -61.38(12) . . . . ?
Co3A C32A C33A C34A 57.38(13) . . . . ?
Co3A C33A C34A C35A 59.98(13) . . . . ?
Co3A C34A C35A C31A 61.74(12) . . . . ?
B4A C1A C2A Co3A -48.90(11) . . . . ?
B4A C1A C2A B6A 105.41(14) . . . . ?
B4A C1A C2A B7A 1.23(18) . . . . ?
B4A C1A C2A B11A 68.18(17) . . . . ?
B4A C1A B5A B6A -140.53(14) . . . . ?
B4A C1A B5A B9A -38.44(13) . . . . ?
B4A C1A B5A B10A -101.77(15) . . . . ?
B4A C1A B6A C2A -99.91(14) . . . . ?
B4A C1A B6A B5A 37.60(13) . . . . ?
B4A C1A B6A B10A -1.41(18) . . . . ?
B4A C1A B6A B11A -64.97(17) . . . . ?
B4A C1A C1B C2B -107.24(18) . . . . ?
B4A C1A C1B B3B -39.1(2) . . . . ?
B4A C1A C1B B4B 32.4(2) . . . . ?
B4A C1A C1B B5B 110.02(19) . . . . ?
B4A C1A C1B B6B -176.63(15) . . . . ?
B4A B5A B6A C1A -34.45(12) . . . . ?
B4A B5A B6A C2A 1.44(17) . . . . ?
B4A B5A B6A B10A 101.46(15) . . . . ?
B4A B5A B6A B11A 63.19(17) . . . . ?
B4A B5A B9A B8A -36.58(14) . . . . ?
B4A B5A B9A B10A -137.53(14) . . . . ?
B4A B5A B9A B12A -100.66(15) . . . . ?
B4A B5A B10A B6A -100.03(15) . . . . ?
B4A B5A B10A B9A 38.28(14) . . . . ?
B4A B5A B10A B11A -62.55(18) . . . . ?
B4A B5A B10A B12A 0.90(19) . . . . ?
B4A B8A B9A B5A 36.67(14) . . . . ?
B4A B8A B9A B10A 100.84(15) . . . . ?
B4A B8A B9A B12A 136.26(15) . . . . ?
B4A B8A B12A B7A 98.62(15) . . . . ?
B4A B8A B12A B9A -38.76(13) . . . . ?
B4A B8A B12A B10A -3.23(19) . . . . ?
B4A B8A B12A B11A 60.85(18) . . . . ?
B4A B9A B10A B5A -38.41(13) . . . . ?
B4A B9A B10A B6A -1.15(19) . . . . ?
B4A B9A B10A B11A 61.82(17) . . . . ?
B4A B9A B10A B12A 100.10(15) . . . . ?
B4A B9A B12A B7A 0.4(2) . . . . ?
B4A B9A B12A B8A 39.21(14) . . . . ?
B4A B9A B12A B10A -101.32(16) . . . . ?
B4A B9A B12A B11A -63.07(18) . . . . ?
B5A C1A C2A Co3A -115.70(12) . . . . ?
B5A C1A C2A B6A 38.61(13) . . . . ?
B5A C1A C2A B7A -65.57(17) . . . . ?
B5A C1A C2A B11A 1.38(18) . . . . ?
B5A C1A B4A Co3A 150.37(11) . . . . ?
B5A C1A B4A B8A 99.83(15) . . . . ?
B5A C1A B4A B9A 37.51(13) . . . . ?
B5A C1A B6A C2A -137.51(14) . . . . ?
B5A C1A B6A B10A -39.01(13) . . . . ?
B5A C1A B6A B11A -102.57(15) . . . . ?
B5A C1A C1B C2B -34.4(2) . . . . ?
B5A C1A C1B B3B 33.73(19) . . . . ?
B5A C1A C1B B4B 105.27(17) . . . . ?
B5A C1A C1B B5B -177.14(14) . . . . ?
B5A C1A C1B B6B -103.78(17) . . . . ?
B5A B4A B8A Co3A 114.33(13) . . . . ?
B5A B4A B8A B7A 65.18(17) . . . . ?
B5A B4A B8A B9A -35.09(13) . . . . ?
B5A B4A B8A B12A 3.73(18) . . . . ?
B5A B4A B9A B8A 140.05(15) . . . . ?
B5A B4A B9A B10A 38.06(13) . . . . ?
B5A B4A B9A B12A 101.00(16) . . . . ?
B5A B6A B10A B9A -36.94(13) . . . . ?
B5A B6A B10A B11A -137.76(15) . . . . ?
B5A B6A B10A B12A -100.93(16) . . . . ?
B5A B6A B11A C2A -96.23(14) . . . . ?
B5A B6A B11A B7A -62.06(18) . . . . ?
B5A B6A B11A B10A 38.02(14) . . . . ?
B5A B6A B11A B12A 1.44(18) . . . . ?
B5A B9A B10A B6A 37.26(13) . . . . ?
B5A B9A B10A B11A 100.22(15) . . . . ?
B5A B9A B10A B12A 138.51(15) . . . . ?
B5A B9A B12A B7A 64.61(19) . . . . ?
B5A B9A B12A B8A 103.44(16) . . . . ?
B5A B9A B12A B10A -37.10(14) . . . . ?
B5A B9A B12A B11A 1.16(19) . . . . ?
B5A B10A B11A C2A 2.25(19) . . . . ?
B5A B10A B11A B6A -37.70(14) . . . . ?
B5A B10A B11A B7A 65.12(18) . . . . ?
B5A B10A B11A B12A 101.21(16) . . . . ?
B5A B10A B12A B7A -63.91(18) . . . . ?
B5A B10A B12A B8A 1.47(19) . . . . ?
B5A B10A B12A B9A 36.88(14) . . . . ?
B5A B10A B12A B11A -100.27(15) . . . . ?
B6A C1A C2A Co3A -154.31(11) . . . . ?
B6A C1A C2A B7A -104.18(15) . . . . ?
B6A C1A C2A B11A -37.23(13) . . . . ?
B6A C1A B4A Co3A 113.56(12) . . . . ?
B6A C1A B4A B5A -36.82(13) . . . . ?
B6A C1A B4A B8A 63.02(17) . . . . ?
B6A C1A B4A B9A 0.69(18) . . . . ?
B6A C1A B5A B4A 140.53(14) . . . . ?
B6A C1A B5A B9A 102.09(15) . . . . ?
B6A C1A B5A B10A 38.76(13) . . . . ?
B6A C1A C1B C2B 32.44(19) . . . . ?
B6A C1A C1B B3B 100.57(16) . . . . ?
B6A C1A C1B B4B 172.11(14) . . . . ?
B6A C1A C1B B5B -110.30(17) . . . . ?
B6A C1A C1B B6B -36.94(19) . . . . ?
B6A C2A B7A Co3A -119.56(13) . . . . ?
B6A C2A B7A B8A -67.26(16) . . . . ?
B6A C2A B7A B11A 35.29(13) . . . . ?
B6A C2A B7A B12A -5.22(18) . . . . ?
B6A C2A B11A B7A -142.42(14) . . . . ?
B6A C2A B11A B10A -39.82(13) . . . . ?
B6A C2A B11A B12A -101.96(15) . . . . ?
B6A B5A B9A B4A 100.38(15) . . . . ?
B6A B5A B9A B8A 63.80(18) . . . . ?
B6A B5A B9A B10A -37.15(13) . . . . ?
B6A B5A B9A B12A -0.28(19) . . . . ?
B6A B5A B10A B9A 138.31(15) . . . . ?
B6A B5A B10A B11A 37.48(14) . . . . ?
B6A B5A B10A B12A 100.93(15) . . . . ?
B6A B10A B11A C2A 39.94(13) . . . . ?
B6A B10A B11A B7A 102.81(15) . . . . ?
B6A B10A B11A B12A 138.90(15) . . . . ?
B6A B10A B12A B7A -0.29(19) . . . . ?
B6A B10A B12A B8A 65.09(18) . . . . ?
B6A B10A B12A B9A 100.50(15) . . . . ?
B6A B10A B12A B11A -36.64(13) . . . . ?
B6A B11A B12A B7A -103.15(15) . . . . ?
B6A B11A B12A B8A -64.75(17) . . . . ?
B6A B11A B12A B9A -1.60(19) . . . . ?
B6A B11A B12A B10A 36.52(13) . . . . ?
B7A C2A B6A C1A 104.58(14) . . . . ?
B7A C2A B6A B5A 67.78(16) . . . . ?
B7A C2A B6A B10A 5.10(18) . . . . ?
B7A C2A B6A B11A -35.42(13) . . . . ?
B7A C2A B11A B6A 142.42(14) . . . . ?
B7A C2A B11A B10A 102.60(15) . . . . ?
B7A C2A B11A B12A 40.45(13) . . . . ?
B7A B8A B9A B4A -99.13(14) . . . . ?
B7A B8A B9A B5A -62.46(17) . . . . ?
B7A B8A B9A B10A 1.71(18) . . . . ?
B7A B8A B9A B12A 37.13(13) . . . . ?
B7A B8A B12A B9A -137.38(15) . . . . ?
B7A B8A B12A B10A -101.85(16) . . . . ?
B7A B8A B12A B11A -37.77(13) . . . . ?
B7A B11A B12A B8A 38.40(13) . . . . ?
B7A B11A B12A B9A 101.56(15) . . . . ?
B7A B11A B12A B10A 139.67(14) . . . . ?
B8A B4A B5A C1A -101.22(14) . . . . ?
B8A B4A B5A B6A -65.92(17) . . . . ?
B8A B4A B5A B9A 35.41(13) . . . . ?
B8A B4A B5A B10A -2.89(18) . . . . ?
B8A B4A B9A B5A -140.05(15) . . . . ?
B8A B4A B9A B10A -101.98(16) . . . . ?
B8A B4A B9A B12A -39.05(14) . . . . ?
B8A B7A B11A C2A 96.16(14) . . . . ?
B8A B7A B11A B6A 62.05(18) . . . . ?
B8A B7A B11A B10A -1.35(18) . . . . ?
B8A B7A B11A B12A -37.42(13) . . . . ?
B8A B7A B12A B9A 38.01(14) . . . . ?
B8A B7A B12A B10A 101.63(15) . . . . ?
B8A B7A B12A B11A 138.07(14) . . . . ?
B8A B9A B10A B5A -102.79(15) . . . . ?
B8A B9A B10A B6A -65.54(17) . . . . ?
B8A B9A B10A B11A -2.57(18) . . . . ?
B8A B9A B10A B12A 35.72(13) . . . . ?
B8A B9A B12A B7A -38.83(14) . . . . ?
B8A B9A B12A B10A -140.53(15) . . . . ?
B8A B9A B12A B11A -102.28(15) . . . . ?
B9A B4A B5A C1A -136.63(14) . . . . ?
B9A B4A B5A B6A -101.32(15) . . . . ?
B9A B4A B5A B10A -38.30(14) . . . . ?
B9A B4A B8A Co3A 149.42(13) . . . . ?
B9A B4A B8A B7A 100.27(15) . . . . ?
B9A B4A B8A B12A 38.82(14) . . . . ?
B9A B5A B6A C1A -98.36(15) . . . . ?
B9A B5A B6A C2A -62.47(17) . . . . ?
B9A B5A B6A B10A 37.55(14) . . . . ?
B9A B5A B6A B11A -0.72(18) . . . . ?
B9A B5A B10A B6A -138.31(15) . . . . ?
B9A B5A B10A B11A -100.83(16) . . . . ?
B9A B5A B10A B12A -37.38(14) . . . . ?
B9A B8A B12A B7A 137.38(15) . . . . ?
B9A B8A B12A B10A 35.52(14) . . . . ?
B9A B8A B12A B11A 99.60(15) . . . . ?
B9A B10A B11A C2A -60.46(17) . . . . ?
B9A B10A B11A B6A -100.40(15) . . . . ?
B9A B10A B11A B7A 2.41(18) . . . . ?
B9A B10A B11A B12A 38.50(13) . . . . ?
B9A B10A B12A B7A -100.79(15) . . . . ?
B9A B10A B12A B8A -35.41(14) . . . . ?
B9A B10A B12A B11A -137.14(14) . . . . ?
B10A B5A B6A C1A -135.91(14) . . . . ?
B10A B5A B6A C2A -100.02(14) . . . . ?
B10A B5A B6A B11A -38.27(13) . . . . ?
B10A B5A B9A B4A 137.53(14) . . . . ?
B10A B5A B9A B8A 100.95(16) . . . . ?
B10A B5A B9A B12A 36.87(14) . . . . ?
B10A B6A B11A C2A -134.25(15) . . . . ?
B10A B6A B11A B7A -100.09(16) . . . . ?
B10A B6A B11A B12A -36.59(14) . . . . ?
B10A B9A B12A B7A 101.70(16) . . . . ?
B10A B9A B12A B8A 140.53(15) . . . . ?
B10A B9A B12A B11A 38.26(13) . . . . ?
B10A B11A B12A B7A -139.67(14) . . . . ?
B10A B11A B12A B8A -101.27(15) . . . . ?
B10A B11A B12A B9A -38.11(13) . . . . ?
B11A C2A B6A C1A 140.00(14) . . . . ?
B11A C2A B6A B5A 103.20(15) . . . . ?
B11A C2A B6A B10A 40.52(13) . . . . ?
B11A C2A B7A Co3A -154.84(12) . . . . ?
B11A C2A B7A B8A -102.55(14) . . . . ?
B11A C2A B7A B12A -40.51(13) . . . . ?
B11A B6A B10A B5A 137.76(15) . . . . ?
B11A B6A B10A B9A 100.82(15) . . . . ?
B11A B6A B10A B12A 36.83(13) . . . . ?
B11A B7A B8A Co3A -112.89(13) . . . . ?
B11A B7A B8A B4A -62.96(17) . . . . ?
B11A B7A B8A B9A -0.21(18) . . . . ?
B11A B7A B8A B12A 37.57(13) . . . . ?
B11A B7A B12A B8A -138.07(14) . . . . ?
B11A B7A B12A B9A -100.06(16) . . . . ?
B11A B7A B12A B10A -36.44(14) . . . . ?
B11A B10A B12A B7A 36.35(13) . . . . ?
B11A B10A B12A B8A 101.73(15) . . . . ?
B11A B10A B12A B9A 137.14(14) . . . . ?
B12A B7A B8A Co3A -150.47(12) . . . . ?
B12A B7A B8A B4A -100.53(15) . . . . ?
B12A B7A B8A B9A -37.78(13) . . . . ?
B12A B7A B11A C2A 133.58(14) . . . . ?
B12A B7A B11A B6A 99.47(16) . . . . ?
B12A B7A B11A B10A 36.07(13) . . . . ?
B12A B8A B9A B4A -136.26(15) . . . . ?
B12A B8A B9A B5A -99.59(16) . . . . ?
B12A B8A B9A B10A -35.42(13) . . . . ?
B12A B9A B10A B5A -138.51(15) . . . . ?
B12A B9A B10A B6A -101.25(15) . . . . ?
B12A B9A B10A B11A -38.29(13) . . . . ?
B12A B10A B11A C2A -98.96(15) . . . . ?
B12A B10A B11A B6A -138.90(15) . . . . ?
B12A B10A B11A B7A -36.09(13) . . . . ?
C31A C32A C33A Co3A -58.26(12) . . . . ?
C31A C32A C33A C34A -0.9(2) . . . . ?
C32A C31A C35A Co3A 61.72(13) . . . . ?
C32A C31A C35A C34A 0.3(2) . . . . ?
C32A C33A C34A Co3A -58.88(13) . . . . ?
C32A C33A C34A C35A 1.1(2) . . . . ?
C33A C34A C35A Co3A -62.62(13) . . . . ?
C33A C34A C35A C31A -0.9(2) . . . . ?
C35A C31A C32A Co3A -59.31(13) . . . . ?
C35A C31A C32A C33A 0.3(2) . . . . ?
C1B C1A C2A Co3A 106.83(14) . . . . ?
C1B C1A C2A B6A -98.86(16) . . . . ?
C1B C1A C2A B7A 156.96(14) . . . . ?
C1B C1A C2A B11A -136.09(15) . . . . ?
C1B C1A B4A Co3A -106.88(15) . . . . ?
C1B C1A B4A B5A 102.75(17) . . . . ?
C1B C1A B4A B8A -157.42(15) . . . . ?
C1B C1A B4A B9A 140.26(15) . . . . ?
C1B C1A B5A B4A -117.37(15) . . . . ?
C1B C1A B5A B6A 102.10(15) . . . . ?
C1B C1A B5A B9A -155.81(14) . . . . ?
C1B C1A B5A B10A 140.86(15) . . . . ?
C1B C1A B6A C2A 115.33(15) . . . . ?
C1B C1A B6A B5A -107.16(15) . . . . ?
C1B C1A B6A B10A -146.17(14) . . . . ?
C1B C1A B6A B11A 150.28(14) . . . . ?
C1B C2B B3B B4B 37.13(12) . . . . ?
C1B C2B B3B B7B 139.99(14) . . . . ?
C1B C2B B3B B8B 99.53(14) . . . . ?
C1B C2B B6B B5B -37.57(12) . . . . ?
C1B C2B B6B B10B -99.87(14) . . . . ?
C1B C2B B6B B11B -140.27(14) . . . . ?
C1B C2B B7B B3B -38.29(13) . . . . ?
C1B C2B B7B B8B 1.74(19) . . . . ?
C1B C2B B7B B11B 104.67(16) . . . . ?
C1B C2B B7B B12B 64.50(17) . . . . ?
C1B C2B B11B B6B 37.63(13) . . . . ?
C1B C2B B11B B7B -105.43(15) . . . . ?
C1B C2B B11B B10B -2.62(18) . . . . ?
C1B C2B B11B B12B -65.25(17) . . . . ?
C1B B3B B4B B5B 35.02(12) . . . . ?
C1B B3B B4B B8B 135.56(14) . . . . ?
C1B B3B B4B B9B 98.19(14) . . . . ?
C1B B3B B7B C2B 34.48(12) . . . . ?
C1B B3B B7B B8B -99.03(14) . . . . ?
C1B B3B B7B B11B 1.98(18) . . . . ?
C1B B3B B7B B12B -61.41(17) . . . . ?
C1B B3B B8B B4B -38.16(12) . . . . ?
C1B B3B B8B B7B 99.66(14) . . . . ?
C1B B3B B8B B9B -0.77(18) . . . . ?
C1B B3B B8B B12B 62.54(16) . . . . ?
C1B B4B B5B B6B 35.35(12) . . . . ?
C1B B4B B5B B9B 136.17(14) . . . . ?
C1B B4B B5B B10B 98.29(14) . . . . ?
C1B B4B B8B B3B 39.56(13) . . . . ?
C1B B4B B8B B7B 1.61(18) . . . . ?
C1B B4B B8B B9B -98.74(15) . . . . ?
C1B B4B B8B B12B -61.34(17) . . . . ?
C1B B4B B9B B5B -37.95(12) . . . . ?
C1B B4B B9B B8B 100.70(14) . . . . ?
C1B B4B B9B B10B -0.33(17) . . . . ?
C1B B4B B9B B12B 63.10(16) . . . . ?
C1B B5B B6B C2B 37.32(12) . . . . ?
C1B B5B B6B B10B 135.62(14) . . . . ?
C1B B5B B6B B11B 97.62(15) . . . . ?
C1B B5B B9B B4B 37.87(12) . . . . ?
C1B B5B B9B B8B 0.99(18) . . . . ?
C1B B5B B9B B10B -99.94(14) . . . . ?
C1B B5B B9B B12B -62.87(17) . . . . ?
C1B B5B B10B B6B -39.09(13) . . . . ?
C1B B5B B10B B9B 99.28(14) . . . . ?
C1B B5B B10B B11B -1.00(18) . . . . ?
C1B B5B B10B B12B 62.26(17) . . . . ?
C1B B6B B10B B5B 38.22(12) . . . . ?
C1B B6B B10B B9B 1.06(18) . . . . ?
C1B B6B B10B B11B -99.32(15) . . . . ?
C1B B6B B10B B12B -62.43(17) . . . . ?
C1B B6B B11B C2B -34.21(12) . . . . ?
C1B B6B B11B B7B -1.30(18) . . . . ?
C1B B6B B11B B10B 99.31(15) . . . . ?
C1B B6B B11B B12B 62.22(17) . . . . ?
C2B C1B B3B B4B -136.50(14) . . . . ?
C2B C1B B3B B7B -34.67(12) . . . . ?
C2B C1B B3B B8B -97.36(15) . . . . ?
C2B C1B B4B B3B 38.65(13) . . . . ?
C2B C1B B4B B5B -101.86(14) . . . . ?
C2B C1B B4B B8B -0.55(17) . . . . ?
C2B C1B B4B B9B -63.50(16) . . . . ?
C2B C1B B5B B4B 101.07(14) . . . . ?
C2B C1B B5B B6B -39.46(12) . . . . ?
C2B C1B B5B B9B 62.48(16) . . . . ?
C2B C1B B5B B10B -0.58(17) . . . . ?
C2B C1B B6B B5B 136.01(14) . . . . ?
C2B C1B B6B B10B 96.91(14) . . . . ?
C2B C1B B6B B11B 34.20(12) . . . . ?
C2B B3B B4B C1B -36.95(12) . . . . ?
C2B B3B B4B B5B -1.93(17) . . . . ?
C2B B3B B4B B8B 98.61(14) . . . . ?
C2B B3B B4B B9B 61.24(16) . . . . ?
C2B B3B B7B B8B -133.51(14) . . . . ?
C2B B3B B7B B11B -32.50(13) . . . . ?
C2B B3B B7B B12B -95.89(15) . . . . ?
C2B B3B B8B B4B -98.26(14) . . . . ?
C2B B3B B8B B7B 39.56(12) . . . . ?
C2B B3B B8B B9B -60.87(17) . . . . ?
C2B B3B B8B B12B 2.44(17) . . . . ?
C2B B6B B10B B5B 98.28(14) . . . . ?
C2B B6B B10B B9B 61.12(17) . . . . ?
C2B B6B B10B B11B -39.26(13) . . . . ?
C2B B6B B10B B12B -2.37(18) . . . . ?
C2B B6B B11B B7B 32.91(13) . . . . ?
C2B B6B B11B B10B 133.52(15) . . . . ?
C2B B6B B11B B12B 96.42(16) . . . . ?
C2B B7B B8B B3B -39.70(13) . . . . ?
C2B B7B B8B B4B -2.00(18) . . . . ?
C2B B7B B8B B9B 61.57(17) . . . . ?
C2B B7B B8B B12B 98.57(15) . . . . ?
C2B B7B B11B B6B -33.17(13) . . . . ?
C2B B7B B11B B10B -96.37(15) . . . . ?
C2B B7B B11B B12B -133.75(14) . . . . ?
C2B B7B B12B B8B -98.30(14) . . . . ?
C2B B7B B12B B9B -61.27(17) . . . . ?
C2B B7B B12B B10B 2.19(18) . . . . ?
C2B B7B B12B B11B 39.25(13) . . . . ?
C2B B11B B12B B7B -39.65(13) . . . . ?
C2B B11B B12B B8B -1.90(18) . . . . ?
C2B B11B B12B B9B 61.19(17) . . . . ?
C2B B11B B12B B10B 98.83(14) . . . . ?
B3B C1B C2B B6B 145.75(14) . . . . ?
B3B C1B C2B B7B 38.52(14) . . . . ?
B3B C1B C2B B11B 107.76(15) . . . . ?
B3B C1B B4B B5B -140.51(14) . . . . ?
B3B C1B B4B B8B -39.19(13) . . . . ?
B3B C1B B4B B9B -102.15(14) . . . . ?
B3B C1B B5B B4B 37.04(13) . . . . ?
B3B C1B B5B B6B -103.48(14) . . . . ?
B3B C1B B5B B9B -1.55(18) . . . . ?
B3B C1B B5B B10B -64.60(17) . . . . ?
B3B C1B B6B C2B -31.56(13) . . . . ?
B3B C1B B6B B5B 104.45(14) . . . . ?
B3B C1B B6B B10B 65.36(16) . . . . ?
B3B C1B B6B B11B 2.64(18) . . . . ?
B3B C2B B6B C1B 33.45(13) . . . . ?
B3B C2B B6B B5B -4.12(18) . . . . ?
B3B C2B B6B B10B -66.42(17) . . . . ?
B3B C2B B6B B11B -106.82(16) . . . . ?
B3B C2B B7B B8B 40.03(13) . . . . ?
B3B C2B B7B B11B 142.95(15) . . . . ?
B3B C2B B7B B12B 102.78(15) . . . . ?
B3B C2B B11B B6B 106.64(15) . . . . ?
B3B C2B B11B B7B -36.42(14) . . . . ?
B3B C2B B11B B10B 66.39(18) . . . . ?
B3B C2B B11B B12B 3.76(19) . . . . ?
B3B B4B B5B C1B -35.76(12) . . . . ?
B3B B4B B5B B6B -0.41(18) . . . . ?
B3B B4B B5B B9B 100.41(15) . . . . ?
B3B B4B B5B B10B 62.53(17) . . . . ?
B3B B4B B8B B7B -37.95(14) . . . . ?
B3B B4B B8B B9B -138.30(15) . . . . ?
B3B B4B B8B B12B -100.91(15) . . . . ?
B3B B4B B9B B5B -101.47(15) . . . . ?
B3B B4B B9B B8B 37.18(13) . . . . ?
B3B B4B B9B B10B -63.85(17) . . . . ?
B3B B4B B9B B12B -0.43(18) . . . . ?
B3B B7B B8B B4B 37.70(13) . . . . ?
B3B B7B B8B B9B 101.27(15) . . . . ?
B3B B7B B8B B12B 138.27(14) . . . . ?
B3B B7B B11B C2B 32.73(13) . . . . ?
B3B B7B B11B B6B -0.44(19) . . . . ?
B3B B7B B11B B10B -63.64(17) . . . . ?
B3B B7B B11B B12B -101.02(15) . . . . ?
B3B B7B B12B B8B -37.06(13) . . . . ?
B3B B7B B12B B9B -0.02(19) . . . . ?
B3B B7B B12B B10B 63.43(18) . . . . ?
B3B B7B B12B B11B 100.50(15) . . . . ?
B3B B8B B9B B4B -37.29(13) . . . . ?
B3B B8B B9B B5B -0.13(19) . . . . ?
B3B B8B B9B B10B 63.25(17) . . . . ?
B3B B8B B9B B12B 100.79(15) . . . . ?
B3B B8B B12B B7B 37.55(13) . . . . ?
B3B B8B B12B B9B -100.90(15) . . . . ?
B3B B8B B12B B10B -63.45(18) . . . . ?
B3B B8B B12B B11B -0.36(18) . . . . ?
B4B C1B C2B B3B -39.31(13) . . . . ?
B4B C1B C2B B6B 106.44(14) . . . . ?
B4B C1B C2B B7B -0.79(18) . . . . ?
B4B C1B C2B B11B 68.44(17) . . . . ?
B4B C1B B3B C2B 136.50(14) . . . . ?
B4B C1B B3B B7B 101.83(15) . . . . ?
B4B C1B B3B B8B 39.13(13) . . . . ?
B4B C1B B5B B6B -140.52(14) . . . . ?
B4B C1B B5B B9B -38.59(13) . . . . ?
B4B C1B B5B B10B -101.64(15) . . . . ?
B4B C1B B6B C2B -98.25(14) . . . . ?
B4B C1B B6B B5B 37.76(13) . . . . ?
B4B C1B B6B B10B -1.33(18) . . . . ?
B4B C1B B6B B11B -64.05(17) . . . . ?
B4B B3B B7B C2B 95.65(14) . . . . ?
B4B B3B B7B B8B -37.87(13) . . . . ?
B4B B3B B7B B11B 63.15(17) . . . . ?
B4B B3B B7B B12B -0.24(18) . . . . ?
B4B B3B B8B B7B 137.82(15) . . . . ?
B4B B3B B8B B9B 37.39(13) . . . . ?
B4B B3B B8B B12B 100.70(15) . . . . ?
B4B B5B B6B C1B -34.76(12) . . . . ?
B4B B5B B6B C2B 2.56(17) . . . . ?
B4B B5B B6B B10B 100.86(15) . . . . ?
B4B B5B B6B B11B 62.86(17) . . . . ?
B4B B5B B9B B8B -36.88(13) . . . . ?
B4B B5B B9B B10B -137.81(14) . . . . ?
B4B B5B B9B B12B -100.74(15) . . . . ?
B4B B5B B10B B6B -100.61(15) . . . . ?
B4B B5B B10B B9B 37.76(13) . . . . ?
B4B B5B B10B B11B -62.52(17) . . . . ?
B4B B5B B10B B12B 0.74(19) . . . . ?
B4B B8B B9B B5B 37.16(13) . . . . ?
B4B B8B B9B B10B 100.53(15) . . . . ?
B4B B8B B9B B12B 138.08(14) . . . . ?
B4B B8B B12B B7B 100.92(15) . . . . ?
B4B B8B B12B B9B -37.53(13) . . . . ?
B4B B8B B12B B10B -0.09(19) . . . . ?
B4B B8B B12B B11B 63.01(17) . . . . ?
B4B B9B B10B B5B -37.82(13) . . . . ?
B4B B9B B10B B6B -0.47(18) . . . . ?
B4B B9B B10B B11B 63.23(17) . . . . ?
B4B B9B B10B B12B 100.77(15) . . . . ?
B4B B9B B12B B7B 0.27(19) . . . . ?
B4B B9B B12B B8B 37.30(13) . . . . ?
B4B B9B B12B B10B -100.77(15) . . . . ?
B4B B9B B12B B11B -63.24(18) . . . . ?
B5B C1B C2B B3B -105.68(14) . . . . ?
B5B C1B C2B B6B 40.07(13) . . . . ?
B5B C1B C2B B7B -67.15(17) . . . . ?
B5B C1B C2B B11B 2.08(18) . . . . ?
B5B C1B B3B C2B 98.84(14) . . . . ?
B5B C1B B3B B4B -37.66(13) . . . . ?
B5B C1B B3B B7B 64.17(16) . . . . ?
B5B C1B B3B B8B 1.47(18) . . . . ?
B5B C1B B4B B3B 140.51(14) . . . . ?
B5B C1B B4B B8B 101.32(15) . . . . ?
B5B C1B B4B B9B 38.36(12) . . . . ?
B5B C1B B6B C2B -136.01(14) . . . . ?
B5B C1B B6B B10B -39.09(13) . . . . ?
B5B C1B B6B B11B -101.81(15) . . . . ?
B5B B4B B8B B3B 101.45(15) . . . . ?
B5B B4B B8B B7B 63.49(17) . . . . ?
B5B B4B B8B B9B -36.85(13) . . . . ?
B5B B4B B8B B12B 0.54(18) . . . . ?
B5B B4B B9B B8B 138.65(14) . . . . ?
B5B B4B B9B B10B 37.62(13) . . . . ?
B5B B4B B9B B12B 101.05(15) . . . . ?
B5B B6B B10B B9B -37.16(13) . . . . ?
B5B B6B B10B B11B -137.54(15) . . . . ?
B5B B6B B10B B12B -100.65(16) . . . . ?
B5B B6B B11B C2B -95.47(15) . . . . ?
B5B B6B B11B B7B -62.56(18) . . . . ?
B5B B6B B11B B10B 38.05(14) . . . . ?
B5B B6B B11B B12B 0.96(19) . . . . ?
B5B B9B B10B B6B 37.35(13) . . . . ?
B5B B9B B10B B11B 101.05(15) . . . . ?
B5B B9B B10B B12B 138.59(15) . . . . ?
B5B B9B B12B B7B 64.04(18) . . . . ?
B5B B9B B12B B8B 101.07(15) . . . . ?
B5B B9B B12B B10B -37.00(13) . . . . ?
B5B B9B B12B B11B 0.53(19) . . . . ?
B5B B10B B11B C2B 2.15(18) . . . . ?
B5B B10B B11B B6B -38.04(13) . . . . ?
B5B B10B B11B B7B 63.60(17) . . . . ?
B5B B10B B11B B12B 100.75(16) . . . . ?
B5B B10B B12B B7B -63.61(18) . . . . ?
B5B B10B B12B B8B -0.41(19) . . . . ?
B5B B10B B12B B9B 36.95(13) . . . . ?
B5B B10B B12B B11B -100.85(15) . . . . ?
B6B C1B C2B B3B -145.75(14) . . . . ?
B6B C1B C2B B7B -107.22(16) . . . . ?
B6B C1B C2B B11B -37.99(14) . . . . ?
B6B C1B B3B C2B 31.76(13) . . . . ?
B6B C1B B3B B4B -104.74(14) . . . . ?
B6B C1B B3B B7B -2.92(17) . . . . ?
B6B C1B B3B B8B -65.61(16) . . . . ?
B6B C1B B4B B3B 103.19(14) . . . . ?
B6B C1B B4B B5B -37.32(13) . . . . ?
B6B C1B B4B B8B 64.00(17) . . . . ?
B6B C1B B4B B9B 1.04(18) . . . . ?
B6B C1B B5B B4B 140.52(14) . . . . ?
B6B C1B B5B B9B 101.93(14) . . . . ?
B6B C1B B5B B10B 38.88(13) . . . . ?
B6B C2B B3B C1B -33.26(13) . . . . ?
B6B C2B B3B B4B 3.87(18) . . . . ?
B6B C2B B3B B7B 106.73(16) . . . . ?
B6B C2B B3B B8B 66.28(17) . . . . ?
B6B C2B B7B B3B -106.78(15) . . . . ?
B6B C2B B7B B8B -66.75(18) . . . . ?
B6B C2B B7B B11B 36.17(14) . . . . ?
B6B C2B B7B B12B -4.00(19) . . . . ?
B6B C2B B11B B7B -143.06(14) . . . . ?
B6B C2B B11B B10B -40.25(13) . . . . ?
B6B C2B B11B B12B -102.88(15) . . . . ?
B6B B5B B9B B4B 100.80(15) . . . . ?
B6B B5B B9B B8B 63.92(17) . . . . ?
B6B B5B B9B B10B -37.01(13) . . . . ?
B6B B5B B9B B12B 0.06(19) . . . . ?
B6B B5B B10B B9B 138.36(14) . . . . ?
B6B B5B B10B B11B 38.09(14) . . . . ?
B6B B5B B10B B12B 101.35(15) . . . . ?
B6B B10B B11B C2B 40.19(13) . . . . ?
B6B B10B B11B B7B 101.65(15) . . . . ?
B6B B10B B11B B12B 138.79(15) . . . . ?
B6B B10B B12B B7B 0.13(19) . . . . ?
B6B B10B B12B B8B 63.34(18) . . . . ?
B6B B10B B12B B9B 100.70(15) . . . . ?
B6B B10B B12B B11B -37.10(14) . . . . ?
B6B B11B B12B B7B -101.76(15) . . . . ?
B6B B11B B12B B8B -64.01(18) . . . . ?
B6B B11B B12B B9B -0.92(19) . . . . ?
B6B B11B B12B B10B 36.72(14) . . . . ?
B7B C2B B3B C1B -139.99(14) . . . . ?
B7B C2B B3B B4B -102.86(14) . . . . ?
B7B C2B B3B B8B -40.45(13) . . . . ?
B7B C2B B6B C1B 103.95(15) . . . . ?
B7B C2B B6B B5B 66.38(17) . . . . ?
B7B C2B B6B B10B 4.08(19) . . . . ?
B7B C2B B6B B11B -36.32(14) . . . . ?
B7B C2B B11B B6B 143.06(14) . . . . ?
B7B C2B B11B B10B 102.81(15) . . . . ?
B7B C2B B11B B12B 40.18(13) . . . . ?
B7B B3B B4B C1B -97.78(14) . . . . ?
B7B B3B B4B B5B -62.76(17) . . . . ?
B7B B3B B4B B8B 37.78(13) . . . . ?
B7B B3B B4B B9B 0.41(18) . . . . ?
B7B B3B B8B B4B -137.82(15) . . . . ?
B7B B3B B8B B9B -100.43(15) . . . . ?
B7B B3B B8B B12B -37.12(13) . . . . ?
B7B B8B B9B B4B -101.21(15) . . . . ?
B7B B8B B9B B5B -64.05(17) . . . . ?
B7B B8B B9B B10B -0.68(18) . . . . ?
B7B B8B B9B B12B 36.86(13) . . . . ?
B7B B8B B12B B9B -138.45(14) . . . . ?
B7B B8B B12B B10B -101.00(15) . . . . ?
B7B B8B B12B B11B -37.91(13) . . . . ?
B7B B11B B12B B8B 37.74(13) . . . . ?
B7B B11B B12B B9B 100.84(15) . . . . ?
B7B B11B B12B B10B 138.48(14) . . . . ?
B8B B3B B4B C1B -135.56(14) . . . . ?
B8B B3B B4B B5B -100.54(15) . . . . ?
B8B B3B B4B B9B -37.37(13) . . . . ?
B8B B3B B7B C2B 133.51(14) . . . . ?
B8B B3B B7B B11B 101.01(15) . . . . ?
B8B B3B B7B B12B 37.62(14) . . . . ?
B8B B4B B5B C1B -99.08(14) . . . . ?
B8B B4B B5B B6B -63.73(17) . . . . ?
B8B B4B B5B B9B 37.09(13) . . . . ?
B8B B4B B5B B10B -0.80(18) . . . . ?
B8B B4B B9B B5B -138.65(14) . . . . ?
B8B B4B B9B B10B -101.03(15) . . . . ?
B8B B4B B9B B12B -37.61(13) . . . . ?
B8B B7B B11B C2B 95.49(14) . . . . ?
B8B B7B B11B B6B 62.32(18) . . . . ?
B8B B7B B11B B10B -0.88(18) . . . . ?
B8B B7B B11B B12B -38.26(13) . . . . ?
B8B B7B B12B B9B 37.03(13) . . . . ?
B8B B7B B12B B10B 100.49(15) . . . . ?
B8B B7B B12B B11B 137.55(14) . . . . ?
B8B B9B B10B B5B -100.91(15) . . . . ?
B8B B9B B10B B6B -63.56(17) . . . . ?
B8B B9B B10B B11B 0.14(18) . . . . ?
B8B B9B B10B B12B 37.68(13) . . . . ?
B8B B9B B12B B7B -37.03(13) . . . . ?
B8B B9B B12B B10B -138.07(14) . . . . ?
B8B B9B B12B B11B -100.54(15) . . . . ?
B9B B4B B5B C1B -136.17(14) . . . . ?
B9B B4B B5B B6B -100.82(15) . . . . ?
B9B B4B B5B B10B -37.88(13) . . . . ?
B9B B4B B8B B3B 138.30(15) . . . . ?
B9B B4B B8B B7B 100.35(16) . . . . ?
B9B B4B B8B B12B 37.39(13) . . . . ?
B9B B5B B6B C1B -98.25(14) . . . . ?
B9B B5B B6B C2B -60.93(16) . . . . ?
B9B B5B B6B B10B 37.37(13) . . . . ?
B9B B5B B6B B11B -0.63(18) . . . . ?
B9B B5B B10B B6B -138.36(14) . . . . ?
B9B B5B B10B B11B -100.28(15) . . . . ?
B9B B5B B10B B12B -37.02(13) . . . . ?
B9B B8B B12B B7B 138.45(14) . . . . ?
B9B B8B B12B B10B 37.45(13) . . . . ?
B9B B8B B12B B11B 100.54(15) . . . . ?
B9B B10B B11B C2B -61.00(17) . . . . ?
B9B B10B B11B B6B -101.19(15) . . . . ?
B9B B10B B11B B7B 0.45(18) . . . . ?
B9B B10B B11B B12B 37.60(13) . . . . ?
B9B B10B B12B B7B -100.56(15) . . . . ?
B9B B10B B12B B8B -37.35(13) . . . . ?
B9B B10B B12B B11B -137.79(15) . . . . ?
B10B B5B B6B C1B -135.62(14) . . . . ?
B10B B5B B6B C2B -98.30(14) . . . . ?
B10B B5B B6B B11B -38.00(14) . . . . ?
B10B B5B B9B B4B 137.81(14) . . . . ?
B10B B5B B9B B8B 100.93(15) . . . . ?
B10B B5B B9B B12B 37.07(14) . . . . ?
B10B B6B B11B C2B -133.52(15) . . . . ?
B10B B6B B11B B7B -100.61(16) . . . . ?
B10B B6B B11B B12B -37.09(14) . . . . ?
B10B B9B B12B B7B 101.04(15) . . . . ?
B10B B9B B12B B8B 138.07(14) . . . . ?
B10B B9B B12B B11B 37.53(14) . . . . ?
B10B B11B B12B B7B -138.48(14) . . . . ?
B10B B11B B12B B8B -100.74(15) . . . . ?
B10B B11B B12B B9B -37.64(14) . . . . ?
B11B C2B B3B C1B -103.51(15) . . . . ?
B11B C2B B3B B4B -66.39(17) . . . . ?
B11B C2B B3B B7B 36.48(14) . . . . ?
B11B C2B B3B B8B -3.98(18) . . . . ?
B11B C2B B6B C1B 140.27(14) . . . . ?
B11B C2B B6B B5B 102.70(14) . . . . ?
B11B C2B B6B B10B 40.40(13) . . . . ?
B11B C2B B7B B3B -142.95(15) . . . . ?
B11B C2B B7B B8B -102.92(15) . . . . ?
B11B C2B B7B B12B -40.17(13) . . . . ?
B11B B6B B10B B5B 137.54(15) . . . . ?
B11B B6B B10B B9B 100.38(15) . . . . ?
B11B B6B B10B B12B 36.89(14) . . . . ?
B11B B7B B8B B3B -100.31(15) . . . . ?
B11B B7B B8B B4B -62.61(17) . . . . ?
B11B B7B B8B B9B 0.96(18) . . . . ?
B11B B7B B8B B12B 37.96(13) . . . . ?
B11B B7B B12B B8B -137.55(14) . . . . ?
B11B B7B B12B B9B -100.52(15) . . . . ?
B11B B7B B12B B10B -37.06(14) . . . . ?
B11B B10B B12B B7B 37.23(14) . . . . ?
B11B B10B B12B B8B 100.44(15) . . . . ?
B11B B10B B12B B9B 137.79(15) . . . . ?
B12B B7B B8B B3B -138.27(14) . . . . ?
B12B B7B B8B B4B -100.57(15) . . . . ?
B12B B7B B8B B9B -37.00(13) . . . . ?
B12B B7B B11B C2B 133.75(14) . . . . ?
B12B B7B B11B B6B 100.58(16) . . . . ?
B12B B7B B11B B10B 37.39(13) . . . . ?
B12B B8B B9B B4B -138.08(14) . . . . ?
B12B B8B B9B B5B -100.91(15) . . . . ?
B12B B8B B9B B10B -37.54(13) . . . . ?
B12B B9B B10B B5B -138.59(15) . . . . ?
B12B B9B B10B B6B -101.24(15) . . . . ?
B12B B9B B10B B11B -37.54(13) . . . . ?
B12B B10B B11B C2B -98.60(15) . . . . ?
B12B B10B B11B B6B -138.79(15) . . . . ?
B12B B10B B11B B7B -37.15(13) . . . . ?
C1C C2C B6C B5C -36.96(12) . . . . ?
C1C C2C B6C B10C -99.79(14) . . . . ?
C1C C2C B6C B11C -140.81(14) . . . . ?
C1C C2C B7C Co3C -51.01(11) . . . . ?
C1C C2C B7C B8C 1.15(17) . . . . ?
C1C C2C B7C B11C 103.19(15) . . . . ?
C1C C2C B7C B12C 62.69(17) . . . . ?
C1C C2C B11C B6C 37.05(13) . . . . ?
C1C C2C B11C B7C -105.84(15) . . . . ?
C1C C2C B11C B10C -3.29(18) . . . . ?
C1C C2C B11C B12C -65.28(17) . . . . ?
C1C B4C B5C B6C 35.10(12) . . . . ?
C1C B4C B5C B9C 135.96(14) . . . . ?
C1C B4C B5C B10C 98.18(14) . . . . ?
C1C B4C B8C Co3C 52.69(10) . . . . ?
C1C B4C B8C B7C 3.22(17) . . . . ?
C1C B4C B8C B9C -97.58(15) . . . . ?
C1C B4C B8C B12C -58.64(16) . . . . ?
C1C B4C B9C B5C -38.22(12) . . . . ?
C1C B4C B9C B8C 101.51(14) . . . . ?
C1C B4C B9C B10C -0.50(17) . . . . ?
C1C B4C B9C B12C 62.50(17) . . . . ?
C1C B5C B6C C2C 35.53(11) . . . . ?
C1C B5C B6C B10C 135.73(14) . . . . ?
C1C B5C B6C B11C 97.12(14) . . . . ?
C1C B5C B9C B4C 38.10(13) . . . . ?
C1C B5C B9C B8C 1.00(19) . . . . ?
C1C B5C B9C B10C -99.97(14) . . . . ?
C1C B5C B9C B12C -62.92(17) . . . . ?
C1C B5C B10C B6C -39.09(13) . . . . ?
C1C B5C B10C B9C 99.48(14) . . . . ?
C1C B5C B10C B11C -1.62(18) . . . . ?
C1C B5C B10C B12C 61.88(17) . . . . ?
C1C B6C B10C B5C 38.76(12) . . . . ?
C1C B6C B10C B9C 1.99(17) . . . . ?
C1C B6C B10C B11C -98.75(14) . . . . ?
C1C B6C B10C B12C -62.04(17) . . . . ?
C1C B6C B11C C2C -33.00(12) . . . . ?
C1C B6C B11C B7C 0.54(18) . . . . ?
C1C B6C B11C B10C 100.67(14) . . . . ?
C1C B6C B11C B12C 64.29(16) . . . . ?
C1C C1D C2D B3D 105.30(16) . . . . ?
C1C C1D C2D B6D -109.06(16) . . . . ?
C1C C1D C2D B7D 143.35(15) . . . . ?
C1C C1D C2D B11D -147.48(15) . . . . ?
C1C C1D B3D C2D -108.19(15) . . . . ?
C1C C1D B3D B4D 115.68(16) . . . . ?
C1C C1D B3D B7D -142.49(14) . . . . ?
C1C C1D B3D B8D 154.71(14) . . . . ?
C1C C1D B4D B3D -103.40(17) . . . . ?
C1C C1D B4D B5D 115.93(17) . . . . ?
C1C C1D B4D B8D -142.22(15) . . . . ?
C1C C1D B4D B9D 154.65(15) . . . . ?
C1C C1D B5D B4D -113.03(18) . . . . ?
C1C C1D B5D B6D 106.37(18) . . . . ?
C1C C1D B5D B9D -151.48(15) . . . . ?
C1C C1D B5D B10D 145.74(16) . . . . ?
C1C C1D B6D C2D 106.60(15) . . . . ?
C1C C1D B6D B5D -116.60(16) . . . . ?
C1C C1D B6D B10D -156.22(14) . . . . ?
C1C C1D B6D B11D 141.08(14) . . . . ?
C2C C1C B4C Co3C 48.52(10) . . . . ?
C2C C1C B4C B5C -102.31(14) . . . . ?
C2C C1C B4C B8C -2.60(17) . . . . ?
C2C C1C B4C B9C -64.24(16) . . . . ?
C2C C1C B5C B4C 101.76(14) . . . . ?
C2C C1C B5C B6C -39.19(13) . . . . ?
C2C C1C B5C B9C 62.72(17) . . . . ?
C2C C1C B5C B10C -0.37(18) . . . . ?
C2C C1C B6C B5C 137.24(14) . . . . ?
C2C C1C B6C B10C 97.88(14) . . . . ?
C2C C1C B6C B11C 34.19(12) . . . . ?
C2C C1C C1D C2D 105.21(16) . . . . ?
C2C C1C C1D B3D 173.47(13) . . . . ?
C2C C1C C1D B4D -114.85(17) . . . . ?
C2C C1C C1D B5D -36.9(2) . . . . ?
C2C C1C C1D B6D 36.3(2) . . . . ?
C2C B6C B10C B5C 97.44(14) . . . . ?
C2C B6C B10C B9C 60.67(17) . . . . ?
C2C B6C B10C B11C -40.07(13) . . . . ?
C2C B6C B10C B12C -3.36(18) . . . . ?
C2C B6C B11C B7C 33.53(13) . . . . ?
C2C B6C B11C B10C 133.67(14) . . . . ?
C2C B6C B11C B12C 97.29(14) . . . . ?
C2C B7C B8C Co3C -52.41(10) . . . . ?
C2C B7C B8C B4C -2.61(17) . . . . ?
C2C B7C B8C B9C 60.11(16) . . . . ?
C2C B7C B8C B12C 98.43(14) . . . . ?
C2C B7C B11C B6C -33.86(13) . . . . ?
C2C B7C B11C B10C -97.38(15) . . . . ?
C2C B7C B11C B12C -133.47(14) . . . . ?
C2C B7C B12C B8C -98.48(14) . . . . ?
C2C B7C B12C B9C -60.22(17) . . . . ?
C2C B7C B12C B10C 3.35(18) . . . . ?
C2C B7C B12C B11C 39.80(13) . . . . ?
C2C B11C B12C B7C -40.26(12) . . . . ?
C2C B11C B12C B8C -1.98(18) . . . . ?
C2C B11C B12C B9C 61.05(16) . . . . ?
C2C B11C B12C B10C 99.35(14) . . . . ?
Co3C C1C C2C B6C 153.55(11) . . . . ?
Co3C C1C C2C B7C 49.29(11) . . . . ?
Co3C C1C C2C B11C 117.10(13) . . . . ?
Co3C C1C B4C B5C -150.84(11) . . . . ?
Co3C C1C B4C B8C -51.12(10) . . . . ?
Co3C C1C B4C B9C -112.76(12) . . . . ?
Co3C C1C B5C B4C 30.47(12) . . . . ?
Co3C C1C B5C B6C -110.48(13) . . . . ?
Co3C C1C B5C B9C -8.57(18) . . . . ?
Co3C C1C B5C B10C -71.66(16) . . . . ?
Co3C C1C B6C C2C -27.90(11) . . . . ?
Co3C C1C B6C B5C 109.34(13) . . . . ?
Co3C C1C B6C B10C 69.98(15) . . . . ?
Co3C C1C B6C B11C 6.29(17) . . . . ?
Co3C C1C C1D C2D -179.71(11) . . . . ?
Co3C C1C C1D B3D -111.45(13) . . . . ?
Co3C C1C C1D B4D -39.77(19) . . . . ?
Co3C C1C C1D B5D 38.2(2) . . . . ?
Co3C C1C C1D B6D 111.42(14) . . . . ?
Co3C C2C B6C C1C 30.45(12) . . . . ?
Co3C C2C B6C B5C -6.51(18) . . . . ?
Co3C C2C B6C B10C -69.33(17) . . . . ?
Co3C C2C B6C B11C -110.36(15) . . . . ?
Co3C C2C B7C B8C 52.16(10) . . . . ?
Co3C C2C B7C B11C 154.20(12) . . . . ?
Co3C C2C B7C B12C 113.71(13) . . . . ?
Co3C C2C B11C B6C 115.09(14) . . . . ?
Co3C C2C B11C B7C -27.80(13) . . . . ?
Co3C C2C B11C B10C 74.75(16) . . . . ?
Co3C C2C B11C B12C 12.76(18) . . . . ?
Co3C B4C B5C C1C -30.97(12) . . . . ?
Co3C B4C B5C B6C 4.14(18) . . . . ?
Co3C B4C B5C B9C 104.99(14) . . . . ?
Co3C B4C B5C B10C 67.21(16) . . . . ?
Co3C B4C B8C B7C -49.47(10) . . . . ?
Co3C B4C B8C B9C -150.27(12) . . . . ?
Co3C B4C B8C B12C -111.33(13) . . . . ?
Co3C B4C B9C B5C -109.77(14) . . . . ?
Co3C B4C B9C B8C 29.96(12) . . . . ?
Co3C B4C B9C B10C -72.05(16) . . . . ?
Co3C B4C B9C B12C -9.05(18) . . . . ?
Co3C B7C B8C B4C 49.80(10) . . . . ?
Co3C B7C B8C B9C 112.52(12) . . . . ?
Co3C B7C B8C B12C 150.84(12) . . . . ?
Co3C B7C B11C C2C 26.59(12) . . . . ?
Co3C B7C B11C B6C -7.26(19) . . . . ?
Co3C B7C B11C B10C -70.78(17) . . . . ?
Co3C B7C B11C B12C -106.87(14) . . . . ?
Co3C B7C B12C B8C -29.64(12) . . . . ?
Co3C B7C B12C B9C 8.61(19) . . . . ?
Co3C B7C B12C B10C 72.18(17) . . . . ?
Co3C B7C B12C B11C 108.63(14) . . . . ?
Co3C B8C B9C B4C -30.12(12) . . . . ?
Co3C B8C B9C B5C 6.8(2) . . . . ?
Co3C B8C B9C B10C 71.10(16) . . . . ?
Co3C B8C B9C B12C 106.20(14) . . . . ?
Co3C B8C B12C B7C 29.10(12) . . . . ?
Co3C B8C B12C B9C -107.86(14) . . . . ?
Co3C B8C B12C B10C -72.60(16) . . . . ?
Co3C B8C B12C B11C -8.51(18) . . . . ?
Co3C C31C C32C C33C 61.62(12) . . . . ?
Co3C C31C C35C C34C -61.63(12) . . . . ?
Co3C C32C C33C C34C 57.66(12) . . . . ?
Co3C C33C C34C C35C 59.12(12) . . . . ?
Co3C C34C C35C C31C 60.29(12) . . . . ?
B4C C1C C2C Co3C -48.38(10) . . . . ?
B4C C1C C2C B6C 105.17(14) . . . . ?
B4C C1C C2C B7C 0.91(18) . . . . ?
B4C C1C C2C B11C 68.72(17) . . . . ?
B4C C1C B5C B6C -140.95(14) . . . . ?
B4C C1C B5C B9C -39.04(13) . . . . ?
B4C C1C B5C B10C -102.13(15) . . . . ?
B4C C1C B6C C2C -100.30(14) . . . . ?
B4C C1C B6C B5C 36.94(13) . . . . ?
B4C C1C B6C B10C -2.42(18) . . . . ?
B4C C1C B6C B11C -66.11(16) . . . . ?
B4C C1C C1D C2D -103.45(18) . . . . ?
B4C C1C C1D B3D -35.2(2) . . . . ?
B4C C1C C1D B4D 36.5(2) . . . . ?
B4C C1C C1D B5D 114.48(18) . . . . ?
B4C C1C C1D B6D -172.32(14) . . . . ?
B4C B5C B6C C1C -34.46(12) . . . . ?
B4C B5C B6C C2C 1.07(17) . . . . ?
B4C B5C B6C B10C 101.27(15) . . . . ?
B4C B5C B6C B11C 62.66(17) . . . . ?
B4C B5C B9C B8C -37.10(14) . . . . ?
B4C B5C B9C B10C -138.07(14) . . . . ?
B4C B5C B9C B12C -101.02(15) . . . . ?
B4C B5C B10C B6C -100.70(14) . . . . ?
B4C B5C B10C B9C 37.87(13) . . . . ?
B4C B5C B10C B11C -63.23(17) . . . . ?
B4C B5C B10C B12C 0.26(18) . . . . ?
B4C B8C B9C B5C 36.89(14) . . . . ?
B4C B8C B9C B10C 101.21(15) . . . . ?
B4C B8C B9C B12C 136.32(14) . . . . ?
B4C B8C B12C B7C 98.20(14) . . . . ?
B4C B8C B12C B9C -38.76(13) . . . . ?
B4C B8C B12C B10C -3.50(18) . . . . ?
B4C B8C B12C B11C 60.59(17) . . . . ?
B4C B9C B10C B5C -37.90(13) . . . . ?
B4C B9C B10C B6C -0.94(18) . . . . ?
B4C B9C B10C B11C 61.78(17) . . . . ?
B4C B9C B10C B12C 100.34(15) . . . . ?
B4C B9C B12C B7C 0.32(19) . . . . ?
B4C B9C B12C B8C 39.47(13) . . . . ?
B4C B9C B12C B10C -101.41(15) . . . . ?
B4C B9C B12C B11C -63.00(17) . . . . ?
B5C C1C C2C Co3C -114.75(12) . . . . ?
B5C C1C C2C B6C 38.80(13) . . . . ?
B5C C1C C2C B7C -65.46(17) . . . . ?
B5C C1C C2C B11C 2.35(18) . . . . ?
B5C C1C B4C Co3C 150.84(11) . . . . ?
B5C C1C B4C B8C 99.71(14) . . . . ?
B5C C1C B4C B9C 38.07(12) . . . . ?
B5C C1C B6C C2C -137.24(14) . . . . ?
B5C C1C B6C B10C -39.36(13) . . . . ?
B5C C1C B6C B11C -103.05(15) . . . . ?
B5C C1C C1D C2D -30.3(2) . . . . ?
B5C C1C C1D B3D 37.94(19) . . . . ?
B5C C1C C1D B4D 109.62(17) . . . . ?
B5C C1C C1D B5D -172.38(15) . . . . ?
B5C C1C C1D B6D -99.18(17) . . . . ?
B5C B4C B8C Co3C 114.92(12) . . . . ?
B5C B4C B8C B7C 65.45(16) . . . . ?
B5C B4C B8C B9C -35.35(13) . . . . ?
B5C B4C B8C B12C 3.59(17) . . . . ?
B5C B4C B9C B8C 139.72(15) . . . . ?
B5C B4C B9C B10C 37.71(13) . . . . ?
B5C B4C B9C B12C 100.71(15) . . . . ?
B5C B6C B10C B9C -36.77(13) . . . . ?
B5C B6C B10C B11C -137.51(14) . . . . ?
B5C B6C B10C B12C -100.80(15) . . . . ?
B5C B6C B11C C2C -95.23(14) . . . . ?
B5C B6C B11C B7C -61.70(17) . . . . ?
B5C B6C B11C B10C 38.44(13) . . . . ?
B5C B6C B11C B12C 2.06(18) . . . . ?
B5C B9C B10C B6C 36.96(13) . . . . ?
B5C B9C B10C B11C 99.68(14) . . . . ?
B5C B9C B10C B12C 138.24(14) . . . . ?
B5C B9C B12C B7C 64.37(18) . . . . ?
B5C B9C B12C B8C 103.52(15) . . . . ?
B5C B9C B12C B10C -37.36(13) . . . . ?
B5C B9C B12C B11C 1.05(18) . . . . ?
B5C B10C B11C C2C 2.91(18) . . . . ?
B5C B10C B11C B6C -37.71(13) . . . . ?
B5C B10C B11C B7C 65.17(17) . . . . ?
B5C B10C B11C B12C 101.42(15) . . . . ?
B5C B10C B12C B7C -63.41(18) . . . . ?
B5C B10C B12C B8C 2.03(19) . . . . ?
B5C B10C B12C B9C 37.13(13) . . . . ?
B5C B10C B12C B11C -99.77(15) . . . . ?
B6C C1C C2C Co3C -153.55(11) . . . . ?
B6C C1C C2C B7C -104.26(15) . . . . ?
B6C C1C C2C B11C -36.45(13) . . . . ?
B6C C1C B4C Co3C 114.57(12) . . . . ?
B6C C1C B4C B5C -36.26(13) . . . . ?
B6C C1C B4C B8C 63.45(16) . . . . ?
B6C C1C B4C B9C 1.81(17) . . . . ?
B6C C1C B5C B4C 140.95(14) . . . . ?
B6C C1C B5C B9C 101.91(15) . . . . ?
B6C C1C B5C B10C 38.82(13) . . . . ?
B6C C1C C1D C2D 36.44(19) . . . . ?
B6C C1C C1D B3D 104.70(15) . . . . ?
B6C C1C C1D B4D 176.38(14) . . . . ?
B6C C1C C1D B5D -105.63(17) . . . . ?
B6C C1C C1D B6D -32.43(19) . . . . ?
B6C C2C B7C Co3C -119.41(13) . . . . ?
B6C C2C B7C B8C -67.25(16) . . . . ?
B6C C2C B7C B11C 34.79(13) . . . . ?
B6C C2C B7C B12C -5.70(18) . . . . ?
B6C C2C B11C B7C -142.89(14) . . . . ?
B6C C2C B11C B10C -40.35(13) . . . . ?
B6C C2C B11C B12C -102.33(15) . . . . ?
B6C B5C B9C B4C 101.22(14) . . . . ?
B6C B5C B9C B8C 64.12(18) . . . . ?
B6C B5C B9C B10C -36.85(13) . . . . ?
B6C B5C B9C B12C 0.20(18) . . . . ?
B6C B5C B10C B9C 138.57(14) . . . . ?
B6C B5C B10C B11C 37.47(13) . . . . ?
B6C B5C B10C B12C 100.96(15) . . . . ?
B6C B10C B11C C2C 40.62(13) . . . . ?
B6C B10C B11C B7C 102.88(15) . . . . ?
B6C B10C B11C B12C 139.13(14) . . . . ?
B6C B10C B12C B7C 0.01(19) . . . . ?
B6C B10C B12C B8C 65.45(18) . . . . ?
B6C B10C B12C B9C 100.54(15) . . . . ?
B6C B10C B12C B11C -36.36(13) . . . . ?
B6C B11C B12C B7C -103.22(14) . . . . ?
B6C B11C B12C B8C -64.94(17) . . . . ?
B6C B11C B12C B9C -1.91(18) . . . . ?
B6C B11C B12C B10C 36.39(13) . . . . ?
B7C C2C B6C C1C 105.56(15) . . . . ?
B7C C2C B6C B5C 68.61(16) . . . . ?
B7C C2C B6C B10C 5.78(18) . . . . ?
B7C C2C B6C B11C -35.25(14) . . . . ?
B7C C2C B11C B6C 142.89(14) . . . . ?
B7C C2C B11C B10C 102.55(15) . . . . ?
B7C C2C B11C B12C 40.56(13) . . . . ?
B7C B8C B9C B4C -98.57(14) . . . . ?
B7C B8C B9C B5C -61.69(17) . . . . ?
B7C B8C B9C B10C 2.64(18) . . . . ?
B7C B8C B9C B12C 37.75(13) . . . . ?
B7C B8C B12C B9C -136.95(14) . . . . ?
B7C B8C B12C B10C -101.70(15) . . . . ?
B7C B8C B12C B11C -37.61(13) . . . . ?
B7C B11C B12C B8C 38.28(13) . . . . ?
B7C B11C B12C B9C 101.31(15) . . . . ?
B7C B11C B12C B10C 139.61(14) . . . . ?
B8C B4C B5C C1C -100.58(14) . . . . ?
B8C B4C B5C B6C -65.47(16) . . . . ?
B8C B4C B5C B9C 35.38(13) . . . . ?
B8C B4C B5C B10C -2.39(18) . . . . ?
B8C B4C B9C B5C -139.72(15) . . . . ?
B8C B4C B9C B10C -102.01(15) . . . . ?
B8C B4C B9C B12C -39.01(13) . . . . ?
B8C B7C B11C C2C 96.53(14) . . . . ?
B8C B7C B11C B6C 62.67(17) . . . . ?
B8C B7C B11C B10C -0.85(18) . . . . ?
B8C B7C B11C B12C -36.94(13) . . . . ?
B8C B7C B12C B9C 38.26(13) . . . . ?
B8C B7C B12C B10C 101.82(15) . . . . ?
B8C B7C B12C B11C 138.28(14) . . . . ?
B8C B9C B10C B5C -102.88(15) . . . . ?
B8C B9C B10C B6C -65.92(17) . . . . ?
B8C B9C B10C B11C -3.20(18) . . . . ?
B8C B9C B10C B12C 35.36(13) . . . . ?
B8C B9C B12C B7C -39.15(13) . . . . ?
B8C B9C B12C B10C -140.89(14) . . . . ?
B8C B9C B12C B11C -102.47(14) . . . . ?
B9C B4C B5C C1C -135.96(14) . . . . ?
B9C B4C B5C B6C -100.85(15) . . . . ?
B9C B4C B5C B10C -37.77(13) . . . . ?
B9C B4C B8C Co3C 150.27(12) . . . . ?
B9C B4C B8C B7C 100.80(15) . . . . ?
B9C B4C B8C B12C 38.94(13) . . . . ?
B9C B5C B6C C1C -98.53(14) . . . . ?
B9C B5C B6C C2C -62.99(16) . . . . ?
B9C B5C B6C B10C 37.21(13) . . . . ?
B9C B5C B6C B11C -1.41(18) . . . . ?
B9C B5C B10C B6C -138.57(14) . . . . ?
B9C B5C B10C B11C -101.10(15) . . . . ?
B9C B5C B10C B12C -37.60(13) . . . . ?
B9C B8C B12C B7C 136.95(14) . . . . ?
B9C B8C B12C B10C 35.26(13) . . . . ?
B9C B8C B12C B11C 99.34(15) . . . . ?
B9C B10C B11C C2C -59.78(17) . . . . ?
B9C B10C B11C B6C -100.41(15) . . . . ?
B9C B10C B11C B7C 2.48(18) . . . . ?
B9C B10C B11C B12C 38.72(13) . . . . ?
B9C B10C B12C B7C -100.53(15) . . . . ?
B9C B10C B12C B8C -35.09(13) . . . . ?
B9C B10C B12C B11C -136.90(14) . . . . ?
B10C B5C B6C C1C -135.73(14) . . . . ?
B10C B5C B6C C2C -100.20(14) . . . . ?
B10C B5C B6C B11C -38.61(13) . . . . ?
B10C B5C B9C B4C 138.07(14) . . . . ?
B10C B5C B9C B8C 100.97(16) . . . . ?
B10C B5C B9C B12C 37.05(13) . . . . ?
B10C B6C B11C C2C -133.67(14) . . . . ?
B10C B6C B11C B7C -100.13(16) . . . . ?
B10C B6C B11C B12C -36.38(13) . . . . ?
B10C B9C B12C B7C 101.73(15) . . . . ?
B10C B9C B12C B8C 140.89(14) . . . . ?
B10C B9C B12C B11C 38.41(13) . . . . ?
B10C B11C B12C B7C -139.61(14) . . . . ?
B10C B11C B12C B8C -101.33(15) . . . . ?
B10C B11C B12C B9C -38.30(13) . . . . ?
B11C C2C B6C C1C 140.81(14) . . . . ?
B11C C2C B6C B5C 103.86(15) . . . . ?
B11C C2C B6C B10C 41.03(13) . . . . ?
B11C C2C B7C Co3C -154.20(12) . . . . ?
B11C C2C B7C B8C -102.04(14) . . . . ?
B11C C2C B7C B12C -40.50(13) . . . . ?
B11C B6C B10C B5C 137.51(14) . . . . ?
B11C B6C B10C B9C 100.74(15) . . . . ?
B11C B6C B10C B12C 36.71(13) . . . . ?
B11C B7C B8C Co3C -113.61(12) . . . . ?
B11C B7C B8C B4C -63.81(16) . . . . ?
B11C B7C B8C B9C -1.09(17) . . . . ?
B11C B7C B8C B12C 37.23(13) . . . . ?
B11C B7C B12C B8C -138.28(14) . . . . ?
B11C B7C B12C B9C -100.02(15) . . . . ?
B11C B7C B12C B10C -36.45(14) . . . . ?
B11C B10C B12C B7C 36.36(13) . . . . ?
B11C B10C B12C B8C 101.80(15) . . . . ?
B11C B10C B12C B9C 136.90(14) . . . . ?
B12C B7C B8C Co3C -150.84(12) . . . . ?
B12C B7C B8C B4C -101.04(14) . . . . ?
B12C B7C B8C B9C -38.32(13) . . . . ?
B12C B7C B11C C2C 133.47(14) . . . . ?
B12C B7C B11C B6C 99.61(15) . . . . ?
B12C B7C B11C B10C 36.09(13) . . . . ?
B12C B8C B9C B4C -136.32(14) . . . . ?
B12C B8C B9C B5C -99.43(16) . . . . ?
B12C B8C B9C B10C -35.11(13) . . . . ?
B12C B9C B10C B5C -138.24(14) . . . . ?
B12C B9C B10C B6C -101.28(15) . . . . ?
B12C B9C B10C B11C -38.56(13) . . . . ?
B12C B10C B11C C2C -98.51(15) . . . . ?
B12C B10C B11C B6C -139.13(14) . . . . ?
B12C B10C B11C B7C -36.24(13) . . . . ?
C31C C32C C33C Co3C -59.23(12) . . . . ?
C31C C32C C33C C34C -1.6(2) . . . . ?
C32C C31C C35C Co3C 61.64(12) . . . . ?
C32C C31C C35C C34C 0.0(2) . . . . ?
C32C C33C C34C Co3C -57.53(12) . . . . ?
C32C C33C C34C C35C 1.6(2) . . . . ?
C33C C34C C35C Co3C -61.28(12) . . . . ?
C33C C34C C35C C31C -1.0(2) . . . . ?
C35C C31C C32C Co3C -60.66(12) . . . . ?
C35C C31C C32C C33C 1.0(2) . . . . ?
C1D C1C C2C Co3C 107.12(14) . . . . ?
C1D C1C C2C B6C -99.33(16) . . . . ?
C1D C1C C2C B7C 156.41(14) . . . . ?
C1D C1C C2C B11C -135.78(15) . . . . ?
C1D C1C B4C Co3C -105.65(15) . . . . ?
C1D C1C B4C B5C 103.51(17) . . . . ?
C1D C1C B4C B8C -156.78(14) . . . . ?
C1D C1C B4C B9C 141.59(15) . . . . ?
C1D C1C B5C B4C -117.85(16) . . . . ?
C1D C1C B5C B6C 101.20(15) . . . . ?
C1D C1C B5C B9C -156.89(14) . . . . ?
C1D C1C B5C B10C 140.01(15) . . . . ?
C1D C1C B6C C2C 114.30(15) . . . . ?
C1D C1C B6C B5C -108.46(15) . . . . ?
C1D C1C B6C B10C -147.82(14) . . . . ?
C1D C1C B6C B11C 148.49(14) . . . . ?
C1D C2D B3D B4D 37.51(12) . . . . ?
C1D C2D B3D B7D 140.28(14) . . . . ?
C1D C2D B3D B8D 99.92(14) . . . . ?
C1D C2D B6D B5D -36.91(12) . . . . ?
C1D C2D B6D B10D -99.59(14) . . . . ?
C1D C2D B6D B11D -140.02(14) . . . . ?
C1D C2D B7D B3D -37.60(13) . . . . ?
C1D C2D B7D B8D 2.50(18) . . . . ?
C1D C2D B7D B11D 105.37(15) . . . . ?
C1D C2D B7D B12D 65.11(17) . . . . ?
C1D C2D B11D B6D 38.29(13) . . . . ?
C1D C2D B11D B7D -104.71(15) . . . . ?
C1D C2D B11D B10D -1.78(19) . . . . ?
C1D C2D B11D B12D -64.46(17) . . . . ?
C1D B3D B4D B5D 34.69(12) . . . . ?
C1D B3D B4D B8D 135.78(14) . . . . ?
C1D B3D B4D B9D 98.12(15) . . . . ?
C1D B3D B7D C2D 34.23(12) . . . . ?
C1D B3D B7D B8D -99.42(14) . . . . ?
C1D B3D B7D B11D 1.46(17) . . . . ?
C1D B3D B7D B12D -62.02(17) . . . . ?
C1D B3D B8D B4D -38.15(13) . . . . ?
C1D B3D B8D B7D 99.42(14) . . . . ?
C1D B3D B8D B9D -0.94(18) . . . . ?
C1D B3D B8D B12D 62.38(17) . . . . ?
C1D B4D B5D B6D 35.70(12) . . . . ?
C1D B4D B5D B9D 135.95(14) . . . . ?
C1D B4D B5D B10D 98.77(14) . . . . ?
C1D B4D B8D B3D 38.88(13) . . . . ?
C1D B4D B8D B7D 0.87(18) . . . . ?
C1D B4D B8D B9D -99.19(15) . . . . ?
C1D B4D B8D B12D -62.10(17) . . . . ?
C1D B4D B9D B5D -38.10(12) . . . . ?
C1D B4D B9D B8D 100.03(14) . . . . ?
C1D B4D B9D B10D -0.88(18) . . . . ?
C1D B4D B9D B12D 62.82(17) . . . . ?
C1D B5D B6D C2D 36.56(12) . . . . ?
C1D B5D B6D B10D 135.14(14) . . . . ?
C1D B5D B6D B11D 97.20(15) . . . . ?
C1D B5D B9D B4D 37.99(13) . . . . ?
C1D B5D B9D B8D 0.49(18) . . . . ?
C1D B5D B9D B10D -100.46(15) . . . . ?
C1D B5D B9D B12D -63.05(17) . . . . ?
C1D B5D B10D B6D -39.86(13) . . . . ?
C1D B5D B10D B9D 98.56(15) . . . . ?
C1D B5D B10D B11D -1.91(19) . . . . ?
C1D B5D B10D B12D 61.21(17) . . . . ?
C1D B6D B10D B5D 38.55(12) . . . . ?
C1D B6D B10D B9D 1.38(18) . . . . ?
C1D B6D B10D B11D -99.19(15) . . . . ?
C1D B6D B10D B12D -62.14(17) . . . . ?
C1D B6D B11D C2D -34.25(12) . . . . ?
C1D B6D B11D B7D -1.52(18) . . . . ?
C1D B6D B11D B10D 99.31(15) . . . . ?
C1D B6D B11D B12D 61.94(17) . . . . ?
C2D C1D B3D B4D -136.13(14) . . . . ?
C2D C1D B3D B7D -34.30(12) . . . . ?
C2D C1D B3D B8D -97.10(14) . . . . ?
C2D C1D B4D B3D 39.46(13) . . . . ?
C2D C1D B4D B5D -101.21(14) . . . . ?
C2D C1D B4D B8D 0.64(17) . . . . ?
C2D C1D B4D B9D -62.48(16) . . . . ?
C2D C1D B5D B4D 102.06(14) . . . . ?
C2D C1D B5D B6D -38.54(13) . . . . ?
C2D C1D B5D B9D 63.60(16) . . . . ?
C2D C1D B5D B10D 0.83(17) . . . . ?
C2D C1D B6D B5D 136.80(14) . . . . ?
C2D C1D B6D B10D 97.18(14) . . . . ?
C2D C1D B6D B11D 34.48(12) . . . . ?
C2D B3D B4D C1D -37.24(12) . . . . ?
C2D B3D B4D B5D -2.54(17) . . . . ?
C2D B3D B4D B8D 98.54(14) . . . . ?
C2D B3D B4D B9D 60.88(16) . . . . ?
C2D B3D B7D B8D -133.65(14) . . . . ?
C2D B3D B7D B11D -32.76(13) . . . . ?
C2D B3D B7D B12D -96.24(15) . . . . ?
C2D B3D B8D B4D -98.27(14) . . . . ?
C2D B3D B8D B7D 39.30(12) . . . . ?
C2D B3D B8D B9D -61.06(17) . . . . ?
C2D B3D B8D B12D 2.25(18) . . . . ?
C2D B6D B10D B5D 98.32(14) . . . . ?
C2D B6D B10D B9D 61.16(17) . . . . ?
C2D B6D B10D B11D -39.41(13) . . . . ?
C2D B6D B10D B12D -2.36(18) . . . . ?
C2D B6D B11D B7D 32.73(13) . . . . ?
C2D B6D B11D B10D 133.56(15) . . . . ?
C2D B6D B11D B12D 96.19(15) . . . . ?
C2D B7D B8D B3D -39.89(13) . . . . ?
C2D B7D B8D B4D -1.99(18) . . . . ?
C2D B7D B8D B9D 60.87(17) . . . . ?
C2D B7D B8D B12D 98.51(15) . . . . ?
C2D B7D B11D B6D -32.96(13) . . . . ?
C2D B7D B11D B10D -95.88(15) . . . . ?
C2D B7D B11D B12D -133.68(14) . . . . ?
C2D B7D B12D B8D -98.71(14) . . . . ?
C2D B7D B12D B9D -60.97(17) . . . . ?
C2D B7D B12D B10D 2.18(18) . . . . ?
C2D B7D B12D B11D 39.53(13) . . . . ?
C2D B11D B12D B7D -39.52(13) . . . . ?
C2D B11D B12D B8D -2.19(18) . . . . ?
C2D B11D B12D B9D 61.19(17) . . . . ?
C2D B11D B12D B10D 98.54(15) . . . . ?
B3D C1D C2D B6D 145.64(14) . . . . ?
B3D C1D C2D B7D 38.05(13) . . . . ?
B3D C1D C2D B11D 107.22(15) . . . . ?
B3D C1D B4D B5D -140.67(14) . . . . ?
B3D C1D B4D B8D -38.82(13) . . . . ?
B3D C1D B4D B9D -101.94(15) . . . . ?
B3D C1D B5D B4D 37.31(13) . . . . ?
B3D C1D B5D B6D -103.28(15) . . . . ?
B3D C1D B5D B9D -1.14(18) . . . . ?
B3D C1D B5D B10D -63.92(17) . . . . ?
B3D C1D B6D C2D -31.94(13) . . . . ?
B3D C1D B6D B5D 104.87(15) . . . . ?
B3D C1D B6D B10D 65.25(17) . . . . ?
B3D C1D B6D B11D 2.55(18) . . . . ?
B3D C2D B6D C1D 33.32(13) . . . . ?
B3D C2D B6D B5D -3.60(18) . . . . ?
B3D C2D B6D B10D -66.27(17) . . . . ?
B3D C2D B6D B11D -106.71(16) . . . . ?
B3D C2D B7D B8D 40.10(13) . . . . ?
B3D C2D B7D B11D 142.96(14) . . . . ?
B3D C2D B7D B12D 102.70(15) . . . . ?
B3D C2D B11D B6D 106.68(15) . . . . ?
B3D C2D B11D B7D -36.32(14) . . . . ?
B3D C2D B11D B10D 66.61(18) . . . . ?
B3D C2D B11D B12D 3.92(19) . . . . ?
B3D B4D B5D C1D -35.16(12) . . . . ?
B3D B4D B5D B6D 0.54(18) . . . . ?
B3D B4D B5D B9D 100.79(15) . . . . ?
B3D B4D B5D B10D 63.61(17) . . . . ?
B3D B4D B8D B7D -38.02(13) . . . . ?
B3D B4D B8D B9D -138.07(15) . . . . ?
B3D B4D B8D B12D -100.98(15) . . . . ?
B3D B4D B9D B5D -100.82(15) . . . . ?
B3D B4D B9D B8D 37.32(13) . . . . ?
B3D B4D B9D B10D -63.60(18) . . . . ?
B3D B4D B9D B12D 0.10(19) . . . . ?
B3D B7D B8D B4D 37.90(13) . . . . ?
B3D B7D B8D B9D 100.76(15) . . . . ?
B3D B7D B8D B12D 138.39(15) . . . . ?
B3D B7D B11D C2D 33.00(13) . . . . ?
B3D B7D B11D B6D 0.05(18) . . . . ?
B3D B7D B11D B10D -62.88(17) . . . . ?
B3D B7D B11D B12D -100.68(15) . . . . ?
B3D B7D B12D B8D -37.01(13) . . . . ?
B3D B7D B12D B9D 0.73(19) . . . . ?
B3D B7D B12D B10D 63.88(18) . . . . ?
B3D B7D B12D B11D 101.23(15) . . . . ?
B3D B8D B9D B4D -37.40(13) . . . . ?
B3D B8D B9D B5D 0.29(19) . . . . ?
B3D B8D B9D B10D 63.75(17) . . . . ?
B3D B8D B9D B12D 101.04(15) . . . . ?
B3D B8D B12D B7D 37.34(13) . . . . ?
B3D B8D B12D B9D -100.35(15) . . . . ?
B3D B8D B12D B10D -63.26(18) . . . . ?
B3D B8D B12D B11D -0.06(19) . . . . ?
B4D C1D C2D B3D -40.10(13) . . . . ?
B4D C1D C2D B6D 105.54(14) . . . . ?
B4D C1D C2D B7D -2.04(18) . . . . ?
B4D C1D C2D B11D 67.12(17) . . . . ?
B4D C1D B3D C2D 136.13(14) . . . . ?
B4D C1D B3D B7D 101.83(15) . . . . ?
B4D C1D B3D B8D 39.03(13) . . . . ?
B4D C1D B5D B6D -140.59(14) . . . . ?
B4D C1D B5D B9D -38.45(13) . . . . ?
B4D C1D B5D B10D -101.23(15) . . . . ?
B4D C1D B6D C2D -99.22(14) . . . . ?
B4D C1D B6D B5D 37.58(13) . . . . ?
B4D C1D B6D B10D -2.04(18) . . . . ?
B4D C1D B6D B11D -64.74(17) . . . . ?
B4D B3D B7D C2D 95.57(14) . . . . ?
B4D B3D B7D B8D -38.08(13) . . . . ?
B4D B3D B7D B11D 62.81(17) . . . . ?
B4D B3D B7D B12D -0.67(18) . . . . ?
B4D B3D B8D B7D 137.57(15) . . . . ?
B4D B3D B8D B9D 37.21(14) . . . . ?
B4D B3D B8D B12D 100.53(16) . . . . ?
B4D B5D B6D C1D -34.87(12) . . . . ?
B4D B5D B6D C2D 1.70(17) . . . . ?
B4D B5D B6D B10D 100.28(15) . . . . ?
B4D B5D B6D B11D 62.34(17) . . . . ?
B4D B5D B9D B8D -37.50(13) . . . . ?
B4D B5D B9D B10D -138.45(14) . . . . ?
B4D B5D B9D B12D -101.04(15) . . . . ?
B4D B5D B10D B6D -101.47(15) . . . . ?
B4D B5D B10D B9D 36.95(13) . . . . ?
B4D B5D B10D B11D -63.52(17) . . . . ?
B4D B5D B10D B12D -0.40(18) . . . . ?
B4D B8D B9D B5D 37.69(13) . . . . ?
B4D B8D B9D B10D 101.15(15) . . . . ?
B4D B8D B9D B12D 138.44(15) . . . . ?
B4D B8D B12D B7D 100.76(15) . . . . ?
B4D B8D B12D B9D -36.93(13) . . . . ?
B4D B8D B12D B10D 0.16(18) . . . . ?
B4D B8D B12D B11D 63.37(17) . . . . ?
B4D B9D B10D B5D -37.44(13) . . . . ?
B4D B9D B10D B6D -0.33(19) . . . . ?
B4D B9D B10D B11D 63.49(18) . . . . ?
B4D B9D B10D B12D 100.81(15) . . . . ?
B4D B9D B12D B7D -0.52(19) . . . . ?
B4D B9D B12D B8D 37.19(14) . . . . ?
B4D B9D B12D B10D -101.24(15) . . . . ?
B4D B9D B12D B11D -63.93(18) . . . . ?
B5D C1D C2D B3D -106.59(14) . . . . ?
B5D C1D C2D B6D 39.04(13) . . . . ?
B5D C1D C2D B7D -68.54(17) . . . . ?
B5D C1D C2D B11D 0.63(18) . . . . ?
B5D C1D B3D C2D 98.43(14) . . . . ?
B5D C1D B3D B4D -37.70(14) . . . . ?
B5D C1D B3D B7D 64.13(17) . . . . ?
B5D C1D B3D B8D 1.33(18) . . . . ?
B5D C1D B4D B3D 140.67(14) . . . . ?
B5D C1D B4D B8D 101.85(15) . . . . ?
B5D C1D B4D B9D 38.73(13) . . . . ?
B5D C1D B6D C2D -136.80(14) . . . . ?
B5D C1D B6D B10D -39.62(13) . . . . ?
B5D C1D B6D B11D -102.32(15) . . . . ?
B5D B4D B8D B3D 100.57(15) . . . . ?
B5D B4D B8D B7D 62.56(17) . . . . ?
B5D B4D B8D B9D -37.49(13) . . . . ?
B5D B4D B8D B12D -0.41(18) . . . . ?
B5D B4D B9D B8D 138.13(14) . . . . ?
B5D B4D B9D B10D 37.22(13) . . . . ?
B5D B4D B9D B12D 100.92(16) . . . . ?
B5D B6D B10D B9D -37.17(14) . . . . ?
B5D B6D B10D B11D -137.73(15) . . . . ?
B5D B6D B10D B12D -100.68(16) . . . . ?
B5D B6D B11D C2D -95.44(15) . . . . ?
B5D B6D B11D B7D -62.71(17) . . . . ?
B5D B6D B11D B10D 38.12(14) . . . . ?
B5D B6D B11D B12D 0.75(19) . . . . ?
B5D B9D B10D B6D 37.11(13) . . . . ?
B5D B9D B10D B11D 100.93(15) . . . . ?
B5D B9D B10D B12D 138.25(14) . . . . ?
B5D B9D B12D B7D 63.42(18) . . . . ?
B5D B9D B12D B8D 101.14(15) . . . . ?
B5D B9D B12D B10D -37.30(14) . . . . ?
B5D B9D B12D B11D 0.02(19) . . . . ?
B5D B10D B11D C2D 2.21(18) . . . . ?
B5D B10D B11D B6D -37.69(14) . . . . ?
B5D B10D B11D B7D 63.27(18) . . . . ?
B5D B10D B11D B12D 100.81(16) . . . . ?
B5D B10D B12D B7D -63.20(18) . . . . ?
B5D B10D B12D B8D 0.15(19) . . . . ?
B5D B10D B12D B9D 37.32(13) . . . . ?
B5D B10D B12D B11D -100.70(15) . . . . ?
B6D C1D C2D B3D -145.64(14) . . . . ?
B6D C1D C2D B7D -107.59(15) . . . . ?
B6D C1D C2D B11D -38.42(14) . . . . ?
B6D C1D B3D C2D 31.78(13) . . . . ?
B6D C1D B3D B4D -104.35(15) . . . . ?
B6D C1D B3D B7D -2.52(17) . . . . ?
B6D C1D B3D B8D -65.32(17) . . . . ?
B6D C1D B4D B3D 103.77(14) . . . . ?
B6D C1D B4D B5D -36.90(13) . . . . ?
B6D C1D B4D B8D 64.95(17) . . . . ?
B6D C1D B4D B9D 1.83(18) . . . . ?
B6D C1D B5D B4D 140.59(14) . . . . ?
B6D C1D B5D B9D 102.14(15) . . . . ?
B6D C1D B5D B10D 39.37(13) . . . . ?
B6D C2D B3D C1D -33.58(13) . . . . ?
B6D C2D B3D B4D 3.93(18) . . . . ?
B6D C2D B3D B7D 106.70(16) . . . . ?
B6D C2D B3D B8D 66.34(17) . . . . ?
B6D C2D B7D B3D -106.69(15) . . . . ?
B6D C2D B7D B8D -66.60(18) . . . . ?
B6D C2D B7D B11D 36.27(14) . . . . ?
B6D C2D B7D B12D -3.99(19) . . . . ?
B6D C2D B11D B7D -143.00(14) . . . . ?
B6D C2D B11D B10D -40.07(13) . . . . ?
B6D C2D B11D B12D -102.75(15) . . . . ?
B6D B5D B9D B4D 101.49(15) . . . . ?
B6D B5D B9D B8D 63.99(18) . . . . ?
B6D B5D B9D B10D -36.96(13) . . . . ?
B6D B5D B9D B12D 0.45(19) . . . . ?
B6D B5D B10D B9D 138.42(15) . . . . ?
B6D B5D B10D B11D 37.95(14) . . . . ?
B6D B5D B10D B12D 101.07(15) . . . . ?
B6D B10D B11D C2D 39.90(13) . . . . ?
B6D B10D B11D B7D 100.96(15) . . . . ?
B6D B10D B11D B12D 138.50(15) . . . . ?
B6D B10D B12D B7D 0.13(19) . . . . ?
B6D B10D B12D B8D 63.48(18) . . . . ?
B6D B10D B12D B9D 100.66(16) . . . . ?
B6D B10D B12D B11D -37.36(14) . . . . ?
B6D B11D B12D B7D -101.18(15) . . . . ?
B6D B11D B12D B8D -63.85(18) . . . . ?
B6D B11D B12D B9D -0.47(19) . . . . ?
B6D B11D B12D B10D 36.87(14) . . . . ?
B7D C2D B3D C1D -140.28(14) . . . . ?
B7D C2D B3D B4D -102.78(14) . . . . ?
B7D C2D B3D B8D -40.36(13) . . . . ?
B7D C2D B6D C1D 103.67(15) . . . . ?
B7D C2D B6D B5D 66.75(17) . . . . ?
B7D C2D B6D B10D 4.07(19) . . . . ?
B7D C2D B6D B11D -36.36(14) . . . . ?
B7D C2D B11D B6D 143.00(14) . . . . ?
B7D C2D B11D B10D 102.93(15) . . . . ?
B7D C2D B11D B12D 40.24(13) . . . . ?
B7D B3D B4D C1D -97.77(14) . . . . ?
B7D B3D B4D B5D -63.07(17) . . . . ?
B7D B3D B4D B8D 38.01(13) . . . . ?
B7D B3D B4D B9D 0.35(18) . . . . ?
B7D B3D B8D B4D -137.57(15) . . . . ?
B7D B3D B8D B9D -100.36(15) . . . . ?
B7D B3D B8D B12D -37.04(13) . . . . ?
B7D B8D B9D B4D -100.95(15) . . . . ?
B7D B8D B9D B5D -63.26(18) . . . . ?
B7D B8D B9D B10D 0.19(18) . . . . ?
B7D B8D B9D B12D 37.49(13) . . . . ?
B7D B8D B12D B9D -137.69(14) . . . . ?
B7D B8D B12D B10D -100.60(15) . . . . ?
B7D B8D B12D B11D -37.40(13) . . . . ?
B7D B11D B12D B8D 37.33(13) . . . . ?
B7D B11D B12D B9D 100.71(15) . . . . ?
B7D B11D B12D B10D 138.05(15) . . . . ?
B8D B3D B4D C1D -135.78(14) . . . . ?
B8D B3D B4D B5D -101.08(15) . . . . ?
B8D B3D B4D B9D -37.66(14) . . . . ?
B8D B3D B7D C2D 133.65(14) . . . . ?
B8D B3D B7D B11D 100.89(15) . . . . ?
B8D B3D B7D B12D 37.40(14) . . . . ?
B8D B4D B5D C1D -98.26(14) . . . . ?
B8D B4D B5D B6D -62.56(17) . . . . ?
B8D B4D B5D B9D 37.68(13) . . . . ?
B8D B4D B5D B10D 0.50(18) . . . . ?
B8D B4D B9D B5D -138.13(14) . . . . ?
B8D B4D B9D B10D -100.92(15) . . . . ?
B8D B4D B9D B12D -37.21(14) . . . . ?
B8D B7D B11D C2D 96.08(14) . . . . ?
B8D B7D B11D B6D 63.12(17) . . . . ?
B8D B7D B11D B10D 0.20(18) . . . . ?
B8D B7D B11D B12D -37.60(13) . . . . ?
B8D B7D B12D B9D 37.74(14) . . . . ?
B8D B7D B12D B10D 100.89(15) . . . . ?
B8D B7D B12D B11D 138.24(15) . . . . ?
B8D B9D B10D B5D -101.01(15) . . . . ?
B8D B9D B10D B6D -63.90(18) . . . . ?
B8D B9D B10D B11D -0.07(18) . . . . ?
B8D B9D B10D B12D 37.24(13) . . . . ?
B8D B9D B12D B7D -37.71(13) . . . . ?
B8D B9D B12D B10D -138.44(14) . . . . ?
B8D B9D B12D B11D -101.12(15) . . . . ?
B9D B4D B5D C1D -135.95(14) . . . . ?
B9D B4D B5D B6D -100.25(15) . . . . ?
B9D B4D B5D B10D -37.18(13) . . . . ?
B9D B4D B8D B3D 138.07(15) . . . . ?
B9D B4D B8D B7D 100.05(16) . . . . ?
B9D B4D B8D B12D 37.09(13) . . . . ?
B9D B5D B6D C1D -97.94(15) . . . . ?
B9D B5D B6D C2D -61.38(16) . . . . ?
B9D B5D B6D B10D 37.20(14) . . . . ?
B9D B5D B6D B11D -0.74(19) . . . . ?
B9D B5D B10D B6D -138.42(15) . . . . ?
B9D B5D B10D B11D -100.47(16) . . . . ?
B9D B5D B10D B12D -37.35(13) . . . . ?
B9D B8D B12D B7D 137.69(14) . . . . ?
B9D B8D B12D B10D 37.09(13) . . . . ?
B9D B8D B12D B11D 100.29(15) . . . . ?
B9D B10D B11D C2D -61.13(17) . . . . ?
B9D B10D B11D B6D -101.03(15) . . . . ?
B9D B10D B11D B7D -0.08(18) . . . . ?
B9D B10D B11D B12D 37.46(13) . . . . ?
B9D B10D B12D B7D -100.52(15) . . . . ?
B9D B10D B12D B8D -37.17(13) . . . . ?
B9D B10D B12D B11D -138.02(15) . . . . ?
B10D B5D B6D C1D -135.14(14) . . . . ?
B10D B5D B6D C2D -98.58(15) . . . . ?
B10D B5D B6D B11D -37.94(13) . . . . ?
B10D B5D B9D B4D 138.45(14) . . . . ?
B10D B5D B9D B8D 100.95(15) . . . . ?
B10D B5D B9D B12D 37.41(14) . . . . ?
B10D B6D B11D C2D -133.56(15) . . . . ?
B10D B6D B11D B7D -100.83(16) . . . . ?
B10D B6D B11D B12D -37.37(14) . . . . ?
B10D B9D B12D B7D 100.73(15) . . . . ?
B10D B9D B12D B8D 138.44(14) . . . . ?
B10D B9D B12D B11D 37.32(13) . . . . ?
B10D B11D B12D B7D -138.05(15) . . . . ?
B10D B11D B12D B8D -100.72(15) . . . . ?
B10D B11D B12D B9D -37.34(14) . . . . ?
B11D C2D B3D C1D -103.89(15) . . . . ?
B11D C2D B3D B4D -66.38(17) . . . . ?
B11D C2D B3D B7D 36.39(14) . . . . ?
B11D C2D B3D B8D -3.96(18) . . . . ?
B11D C2D B6D C1D 140.02(14) . . . . ?
B11D C2D B6D B5D 103.11(15) . . . . ?
B11D C2D B6D B10D 40.43(13) . . . . ?
B11D C2D B7D B3D -142.96(14) . . . . ?
B11D C2D B7D B8D -102.87(15) . . . . ?
B11D C2D B7D B12D -40.26(13) . . . . ?
B11D B6D B10D B5D 137.73(15) . . . . ?
B11D B6D B10D B9D 100.57(16) . . . . ?
B11D B6D B10D B12D 37.05(14) . . . . ?
B11D B7D B8D B3D -101.00(15) . . . . ?
B11D B7D B8D B4D -63.10(17) . . . . ?
B11D B7D B8D B9D -0.24(18) . . . . ?
B11D B7D B8D B12D 37.40(13) . . . . ?
B11D B7D B12D B8D -138.24(15) . . . . ?
B11D B7D B12D B9D -100.50(15) . . . . ?
B11D B7D B12D B10D -37.35(14) . . . . ?
B11D B10D B12D B7D 37.50(14) . . . . ?
B11D B10D B12D B8D 100.85(15) . . . . ?
B11D B10D B12D B9D 138.02(15) . . . . ?
B12D B7D B8D B3D -138.39(15) . . . . ?
B12D B7D B8D B4D -100.50(16) . . . . ?
B12D B7D B8D B9D -37.64(13) . . . . ?
B12D B7D B11D C2D 133.68(14) . . . . ?
B12D B7D B11D B6D 100.72(15) . . . . ?
B12D B7D B11D B10D 37.80(13) . . . . ?
B12D B8D B9D B4D -138.44(15) . . . . ?
B12D B8D B9D B5D -100.75(16) . . . . ?
B12D B8D B9D B10D -37.29(13) . . . . ?
B12D B9D B10D B5D -138.25(14) . . . . ?
B12D B9D B10D B6D -101.14(15) . . . . ?
B12D B9D B10D B11D -37.32(13) . . . . ?
B12D B10D B11D C2D -98.59(15) . . . . ?
B12D B10D B11D B6D -138.50(15) . . . . ?
B12D B10D B11D B7D -37.54(13) . . . . ?

_olex2_computing_structure_solution_long 'ShelXS (Sheldrick, 2008)'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_4953
_database_code_depnum_ccdc_archive 'CCDC 1042155'
_audit_update_record             
;
2015-01-05 deposited with the CCDC.
2015-02-09 downloaded from the CCDC.
;
_audit_creation_date             2014-12-16
_audit_creation_method           
;
Olex2 1.2
(compiled 2013.12.10 svn.r2850 for OlexSys, GUI svn.r4736)
;
_shelxl_version_number           2014/6
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C9 H26 B19 Co'
_chemical_formula_sum            'C9 H26 B19 Co'
_chemical_formula_weight         398.62
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   12.6472(6)
_cell_length_b                   6.6422(3)
_cell_length_c                   23.8175(10)
_cell_angle_alpha                90
_cell_angle_beta                 95.642(2)
_cell_angle_gamma                90
_cell_volume                     1991.10(16)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9947
_cell_measurement_temperature    100.0(2)
_cell_measurement_theta_max      29.319
_cell_measurement_theta_min      3.185
_shelx_estimated_absorpt_T_max   0.935
_shelx_estimated_absorpt_T_min   0.726
_exptl_absorpt_coefficient_mu    0.855
_exptl_absorpt_correction_T_max  0.7459
_exptl_absorpt_correction_T_min  0.6612
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.0594 before and 0.0475 after correction.
The Ratio of minimum to maximum transmission is 0.8864.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.330
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    ?
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             808
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.08
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0368
_diffrn_reflns_av_unetI/netI     0.0273
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            37451
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         29.576
_diffrn_reflns_theta_min         1.718
_diffrn_ambient_temperature      100.0(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_special_details          ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4897
_reflns_number_total             5581
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'XS (Sheldrick, 2008)'
_refine_diff_density_max         0.364
_refine_diff_density_min         -0.243
_refine_diff_density_rms         0.055
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.086
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     325
_refine_ls_number_reflns         5581
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0404
_refine_ls_R_factor_gt           0.0325
_refine_ls_restrained_S_all      1.086
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0314P)²+0.8956P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0732
_refine_ls_wR_factor_ref         0.0764
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2.a Ternary CH refined with riding coordinates:
 C21(H21), C22(H22), C23(H23), C24(H24), C25(H25)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C -0.37554(11) -0.4009(2) -0.39983(6) 0.0186(3) Uani 1 1 d . . . . .
H1 H -0.3985(14) -0.267(3) -0.4165(7) 0.022 Uiso 1 1 d R . . . .
Co2 Co -0.24871(2) -0.52608(3) -0.43197(2) 0.01431(6) Uani 1 1 d . . . . .
B3 B -0.26112(12) -0.4060(2) -0.35532(6) 0.0136(3) Uani 1 1 d . . . . .
H3 H -0.2150(13) -0.276(2) -0.3406(7) 0.016 Uiso 1 1 d R . . . .
B4 B -0.38978(12) -0.4087(2) -0.32971(6) 0.0159(3) Uani 1 1 d . . . . .
H4 H -0.4110(13) -0.284(3) -0.3056(7) 0.019 Uiso 1 1 d R . . . .
B5 B -0.47702(13) -0.5435(3) -0.37825(7) 0.0208(3) Uani 1 1 d . . . . .
H5 H -0.5557(15) -0.494(3) -0.3861(8) 0.025 Uiso 1 1 d R . . . .
B6 B -0.40293(13) -0.6276(3) -0.43406(7) 0.0198(3) Uani 1 1 d . . . . .
H6 H -0.4468(13) -0.637(3) -0.4744(7) 0.024 Uiso 1 1 d R . . . .
B7 B -0.21432(12) -0.6657(2) -0.35576(6) 0.0146(3) Uani 1 1 d . . . . .
H7 H -0.1343(13) -0.703(2) -0.3398(7) 0.017 Uiso 1 1 d R . . . .
C8 C -0.29346(10) -0.5773(2) -0.30514(5) 0.0122(2) Uani 1 1 d . . . . .
B9 B -0.42362(12) -0.6607(3) -0.31518(7) 0.0182(3) Uani 1 1 d . . . . .
H9 H -0.4654(13) -0.691(3) -0.2792(7) 0.022 Uiso 1 1 d R . . . .
B10 B -0.43239(14) -0.7966(3) -0.37954(7) 0.0216(3) Uani 1 1 d . . . . .
H10 H -0.4863(14) -0.921(3) -0.3876(7) 0.026 Uiso 1 1 d R . . . .
B11 B -0.30341(13) -0.8001(2) -0.40413(7) 0.0188(3) Uani 1 1 d . . . . .
H11 H -0.2819(14) -0.934(3) -0.4252(7) 0.023 Uiso 1 1 d R . . . .
B12 B -0.31628(13) -0.8166(2) -0.33117(7) 0.0171(3) Uani 1 1 d . . . . .
H12 H -0.2946(13) -0.939(3) -0.3038(7) 0.021 Uiso 1 1 d R . . . .
C21 C -0.22962(15) -0.3288(3) -0.49705(6) 0.0298(4) Uani 1 1 d . . . . .
H21 H -0.2780 -0.2142 -0.5090 0.036 Uiso 1 1 calc R . . . .
C22 C -0.23916(14) -0.5272(3) -0.51767(6) 0.0265(3) Uani 1 1 d . . . . .
H22 H -0.2946 -0.5781 -0.5471 0.032 Uiso 1 1 calc R . . . .
C23 C -0.15586(14) -0.6411(3) -0.48959(7) 0.0303(4) Uani 1 1 d . . . . .
H23 H -0.1413 -0.7870 -0.4958 0.036 Uiso 1 1 calc R . . . .
C24 C -0.09540(13) -0.5111(3) -0.45175(7) 0.0361(5) Uani 1 1 d . . . . .
H24 H -0.0308 -0.5494 -0.4264 0.043 Uiso 1 1 calc R . . . .
C25 C -0.14108(15) -0.3191(3) -0.45644(7) 0.0343(4) Uani 1 1 d . . . . .
H25 H -0.1153 -0.1966 -0.4348 0.041 Uiso 1 1 calc R . . . .
C1' C -0.24113(10) -0.55593(19) -0.24460(5) 0.0116(2) Uani 1 1 d . . . . .
C2' C -0.22055(11) -0.3230(2) -0.21927(6) 0.0174(3) Uani 1 1 d . . . . .
H2' H -0.2494(13) -0.207(3) -0.2467(7) 0.021 Uiso 1 1 d R . . . .
B3' B -0.11285(12) -0.4640(2) -0.23571(6) 0.0143(3) Uani 1 1 d . . . . .
H3' H -0.0786(13) -0.426(3) -0.2725(7) 0.017 Uiso 1 1 d R . . . .
B4' B -0.14217(12) -0.7155(2) -0.21758(6) 0.0140(3) Uani 1 1 d . . . . .
H4' H -0.1209(13) -0.834(2) -0.2442(7) 0.017 Uiso 1 1 d R . . . .
B5' B -0.26957(13) -0.7187(2) -0.19170(6) 0.0153(3) Uani 1 1 d . . . . .
H5' H -0.3203(13) -0.838(3) -0.2018(7) 0.018 Uiso 1 1 d R . . . .
B6' B -0.31684(12) -0.4696(2) -0.19381(6) 0.0141(3) Uani 1 1 d . . . . .
H6' H -0.3911(13) -0.436(2) -0.2067(7) 0.017 Uiso 1 1 d R . . . .
B7' B -0.10631(13) -0.3138(2) -0.17404(7) 0.0168(3) Uani 1 1 d . . . . .
H7' H -0.0620(13) -0.179(3) -0.1728(7) 0.020 Uiso 1 1 d R . . . .
B8' B -0.05578(13) -0.5641(2) -0.17147(6) 0.0165(3) Uani 1 1 d . . . . .
H8' H 0.0286(13) -0.594(3) -0.1658(7) 0.020 Uiso 1 1 d R . . . .
B9' B -0.15240(13) -0.7218(2) -0.14379(6) 0.0174(3) Uani 1 1 d . . . . .
H9' H -0.1297(13) -0.855(3) -0.1196(7) 0.021 Uiso 1 1 d R . . . .
B10' B -0.26234(13) -0.5687(2) -0.12940(6) 0.0174(3) Uani 1 1 d . . . . .
H10' H -0.3142(13) -0.603(3) -0.0979(7) 0.021 Uiso 1 1 d R . . . .
B11' B -0.23368(13) -0.3169(2) -0.14809(6) 0.0168(3) Uani 1 1 d . . . . .
H11' H -0.2666(13) -0.188(3) -0.1320(7) 0.020 Uiso 1 1 d R . . . .
B12' B -0.12994(13) -0.4734(3) -0.11665(7) 0.0185(3) Uani 1 1 d . . . . .
H12' H -0.0908(14) -0.443(3) -0.0741(7) 0.022 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 H1 1.003(18) . ?
C1 Co2 2.0226(14) . ?
C1 B3 1.708(2) . ?
C1 B4 1.698(2) . ?
C1 B5 1.714(2) . ?
C1 B6 1.731(2) . ?
Co2 B3 2.0124(15) . ?
Co2 B6 2.0597(17) . ?
Co2 B7 2.0464(15) . ?
Co2 B11 2.0787(16) . ?
Co2 C21 2.0622(15) . ?
Co2 C22 2.0566(14) . ?
Co2 C23 2.0404(15) . ?
Co2 C24 2.0423(16) . ?
Co2 C25 2.0590(16) . ?
B3 H3 1.080(16) . ?
B3 B4 1.793(2) . ?
B3 B7 1.824(2) . ?
B3 C8 1.7279(19) . ?
B4 H4 1.058(17) . ?
B4 B5 1.762(2) . ?
B4 C8 1.715(2) . ?
B4 B9 1.771(2) . ?
B5 H5 1.048(18) . ?
B5 B6 1.789(2) . ?
B5 B9 1.766(2) . ?
B5 B10 1.775(3) . ?
B6 H6 1.063(17) . ?
B6 B10 1.783(2) . ?
B6 B11 1.797(2) . ?
B7 H7 1.075(16) . ?
B7 C8 1.743(2) . ?
B7 B11 1.772(2) . ?
B7 B12 1.778(2) . ?
C8 B9 1.731(2) . ?
C8 B12 1.720(2) . ?
C8 C1' 1.5329(17) . ?
B9 H9 1.070(17) . ?
B9 B10 1.773(2) . ?
B9 B12 1.778(2) . ?
B10 H10 1.077(18) . ?
B10 B11 1.787(2) . ?
B10 B12 1.780(2) . ?
B11 H11 1.070(18) . ?
B11 B12 1.765(2) . ?
B12 H12 1.061(17) . ?
C21 H21 1.0000 . ?
C21 C22 1.408(2) . ?
C21 C25 1.407(3) . ?
C22 H22 1.0000 . ?
C22 C23 1.411(2) . ?
C23 H23 1.0000 . ?
C23 C24 1.417(3) . ?
C24 H24 1.0000 . ?
C24 C25 1.400(3) . ?
C25 H25 1.0000 . ?
C1' C2' 1.6716(19) . ?
C1' B3' 1.727(2) . ?
C1' B4' 1.7160(19) . ?
C1' B5' 1.7247(19) . ?
C1' B6' 1.7137(19) . ?
C2' H2' 1.052(17) . ?
C2' B3' 1.729(2) . ?
C2' B6' 1.716(2) . ?
C2' B7' 1.716(2) . ?
C2' B11' 1.720(2) . ?
B3' H3' 1.046(16) . ?
B3' B4' 1.774(2) . ?
B3' B7' 1.771(2) . ?
B3' B8' 1.757(2) . ?
B4' H4' 1.061(16) . ?
B4' B5' 1.781(2) . ?
B4' B8' 1.782(2) . ?
B4' B9' 1.775(2) . ?
B5' H5' 1.034(17) . ?
B5' B6' 1.758(2) . ?
B5' B9' 1.779(2) . ?
B5' B10' 1.782(2) . ?
B6' H6' 0.985(17) . ?
B6' B10' 1.748(2) . ?
B6' B11' 1.760(2) . ?
B7' H7' 1.058(17) . ?
B7' B8' 1.780(2) . ?
B7' B11' 1.781(2) . ?
B7' B12' 1.778(2) . ?
B8' H8' 1.081(16) . ?
B8' B9' 1.785(2) . ?
B8' B12' 1.786(2) . ?
B9' H9' 1.080(17) . ?
B9' B10' 1.783(2) . ?
B9' B12' 1.785(2) . ?
B10' H10' 1.067(17) . ?
B10' B11' 1.778(2) . ?
B10' B12' 1.788(2) . ?
B11' H11' 1.043(17) . ?
B11' B12' 1.780(2) . ?
B12' H12' 1.102(17) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Co2 C1 H1 115.0(10) . . ?
B3 C1 H1 117.3(10) . . ?
B3 C1 Co2 64.65(7) . . ?
B3 C1 B5 114.62(11) . . ?
B3 C1 B6 113.16(11) . . ?
B4 C1 H1 111.2(10) . . ?
B4 C1 Co2 121.64(9) . . ?
B4 C1 B3 63.53(9) . . ?
B4 C1 B5 62.18(9) . . ?
B4 C1 B6 113.66(12) . . ?
B5 C1 H1 114.3(10) . . ?
B5 C1 Co2 122.11(10) . . ?
B5 C1 B6 62.59(10) . . ?
B6 C1 H1 123.1(10) . . ?
B6 C1 Co2 66.03(7) . . ?
C1 Co2 B6 50.16(6) . . ?
C1 Co2 B7 87.59(6) . . ?
C1 Co2 B11 86.44(7) . . ?
C1 Co2 C21 100.32(6) . . ?
C1 Co2 C22 120.22(6) . . ?
C1 Co2 C23 159.83(7) . . ?
C1 Co2 C24 150.86(8) . . ?
C1 Co2 C25 113.81(7) . . ?
B3 Co2 C1 50.09(6) . . ?
B3 Co2 B6 89.63(6) . . ?
B3 Co2 B7 53.39(6) . . ?
B3 Co2 B11 89.97(6) . . ?
B3 Co2 C21 117.10(7) . . ?
B3 Co2 C22 156.82(7) . . ?
B3 Co2 C23 149.31(7) . . ?
B3 Co2 C24 110.51(7) . . ?
B3 Co2 C25 96.02(6) . . ?
B6 Co2 B11 51.47(7) . . ?
B6 Co2 C21 111.74(7) . . ?
B7 Co2 B6 89.51(6) . . ?
B7 Co2 B11 50.87(6) . . ?
B7 Co2 C21 157.55(7) . . ?
B7 Co2 C22 148.27(7) . . ?
B7 Co2 C25 117.70(7) . . ?
C21 Co2 B11 149.71(7) . . ?
C22 Co2 B6 97.05(7) . . ?
C22 Co2 B11 111.54(7) . . ?
C22 Co2 C21 39.97(7) . . ?
C22 Co2 C25 67.45(7) . . ?
C23 Co2 B6 117.86(7) . . ?
C23 Co2 B7 109.92(7) . . ?
C23 Co2 B11 96.79(7) . . ?
C23 Co2 C21 67.34(7) . . ?
C23 Co2 C22 40.29(7) . . ?
C23 Co2 C24 40.61(8) . . ?
C23 Co2 C25 67.63(7) . . ?
C24 Co2 B6 158.22(8) . . ?
C24 Co2 B7 95.90(7) . . ?
C24 Co2 B11 118.00(8) . . ?
C24 Co2 C21 67.15(7) . . ?
C24 Co2 C22 67.76(7) . . ?
C24 Co2 C25 39.92(8) . . ?
C25 Co2 B6 149.61(8) . . ?
C25 Co2 B11 157.67(8) . . ?
C25 Co2 C21 39.93(7) . . ?
C1 B3 Co2 65.26(7) . . ?
C1 B3 H3 125.7(9) . . ?
C1 B3 B4 57.96(8) . . ?
C1 B3 B7 105.71(11) . . ?
C1 B3 C8 101.46(10) . . ?
Co2 B3 H3 121.5(9) . . ?
B4 B3 Co2 117.32(9) . . ?
B4 B3 H3 112.2(9) . . ?
B4 B3 B7 107.38(10) . . ?
B7 B3 Co2 64.26(7) . . ?
B7 B3 H3 126.3(9) . . ?
C8 B3 Co2 114.30(9) . . ?
C8 B3 H3 117.3(8) . . ?
C8 B3 B4 58.26(8) . . ?
C8 B3 B7 58.71(8) . . ?
C1 B4 B3 58.51(8) . . ?
C1 B4 H4 124.6(9) . . ?
C1 B4 B5 59.35(9) . . ?
C1 B4 C8 102.41(10) . . ?
C1 B4 B9 105.78(11) . . ?
B3 B4 H4 117.7(9) . . ?
B5 B4 B3 108.21(11) . . ?
B5 B4 H4 125.4(9) . . ?
B5 B4 B9 59.99(9) . . ?
C8 B4 B3 58.97(8) . . ?
C8 B4 H4 122.4(9) . . ?
C8 B4 B5 105.66(11) . . ?
C8 B4 B9 59.53(9) . . ?
B9 B4 B3 108.70(11) . . ?
B9 B4 H4 123.7(9) . . ?
C1 B5 B4 58.46(9) . . ?
C1 B5 H5 120.0(10) . . ?
C1 B5 B6 59.17(9) . . ?
C1 B5 B9 105.29(11) . . ?
C1 B5 B10 105.63(11) . . ?
B4 B5 H5 118.7(10) . . ?
B4 B5 B6 107.83(11) . . ?
B4 B5 B9 60.24(9) . . ?
B4 B5 B10 108.25(12) . . ?
B6 B5 H5 121.6(10) . . ?
B9 B5 H5 124.6(10) . . ?
B9 B5 B6 108.05(12) . . ?
B9 B5 B10 60.09(10) . . ?
B10 B5 H5 126.3(10) . . ?
B10 B5 B6 60.05(10) . . ?
C1 B6 Co2 63.81(7) . . ?
C1 B6 B5 58.24(9) . . ?
C1 B6 H6 122.7(10) . . ?
C1 B6 B10 104.54(11) . . ?
C1 B6 B11 105.53(11) . . ?
Co2 B6 H6 116.7(9) . . ?
B5 B6 Co2 116.33(10) . . ?
B5 B6 H6 115.2(9) . . ?
B5 B6 B11 107.57(11) . . ?
B10 B6 Co2 116.97(10) . . ?
B10 B6 B5 59.57(10) . . ?
B10 B6 H6 119.5(10) . . ?
B10 B6 B11 59.87(10) . . ?
B11 B6 Co2 64.81(7) . . ?
B11 B6 H6 127.1(10) . . ?
Co2 B7 H7 122.0(9) . . ?
B3 B7 Co2 62.35(7) . . ?
B3 B7 H7 120.8(9) . . ?
C8 B7 Co2 112.00(9) . . ?
C8 B7 B3 57.90(8) . . ?
C8 B7 H7 114.7(9) . . ?
C8 B7 B11 104.34(11) . . ?
C8 B7 B12 58.49(8) . . ?
B11 B7 Co2 65.51(7) . . ?
B11 B7 B3 107.12(11) . . ?
B11 B7 H7 129.0(9) . . ?
B11 B7 B12 59.63(9) . . ?
B12 B7 Co2 116.74(9) . . ?
B12 B7 B3 106.56(10) . . ?
B12 B7 H7 116.2(9) . . ?
B3 C8 B7 63.39(8) . . ?
B3 C8 B9 113.69(10) . . ?
B4 C8 B3 62.77(8) . . ?
B4 C8 B7 114.89(10) . . ?
B4 C8 B9 61.84(9) . . ?
B4 C8 B12 113.09(10) . . ?
B9 C8 B7 113.55(10) . . ?
B12 C8 B3 113.69(10) . . ?
B12 C8 B7 61.77(9) . . ?
B12 C8 B9 62.02(9) . . ?
C1' C8 B3 118.68(10) . . ?
C1' C8 B4 119.16(11) . . ?
C1' C8 B7 117.24(10) . . ?
C1' C8 B9 118.45(10) . . ?
C1' C8 B12 117.78(11) . . ?
B4 B9 H9 119.0(9) . . ?
B4 B9 B10 107.95(11) . . ?
B4 B9 B12 107.73(11) . . ?
B5 B9 B4 59.76(9) . . ?
B5 B9 H9 126.0(9) . . ?
B5 B9 B10 60.19(10) . . ?
B5 B9 B12 108.11(11) . . ?
C8 B9 B4 58.63(8) . . ?
C8 B9 B5 104.79(11) . . ?
C8 B9 H9 119.3(9) . . ?
C8 B9 B10 105.09(11) . . ?
C8 B9 B12 58.69(8) . . ?
B10 B9 H9 127.0(9) . . ?
B10 B9 B12 60.18(10) . . ?
B12 B9 H9 120.5(9) . . ?
B5 B10 B6 60.38(10) . . ?
B5 B10 H10 122.3(10) . . ?
B5 B10 B11 108.67(12) . . ?
B5 B10 B12 107.64(11) . . ?
B6 B10 H10 121.8(9) . . ?
B6 B10 B11 60.44(9) . . ?
B9 B10 B5 59.72(10) . . ?
B9 B10 B6 108.02(12) . . ?
B9 B10 H10 122.0(9) . . ?
B9 B10 B11 107.97(11) . . ?
B9 B10 B12 60.05(9) . . ?
B11 B10 H10 120.9(10) . . ?
B12 B10 B6 107.47(11) . . ?
B12 B10 H10 121.7(9) . . ?
B12 B10 B11 59.31(9) . . ?
Co2 B11 H11 118.1(10) . . ?
B6 B11 Co2 63.72(7) . . ?
B6 B11 H11 123.0(9) . . ?
B7 B11 Co2 63.62(7) . . ?
B7 B11 B6 108.21(11) . . ?
B7 B11 B10 108.85(11) . . ?
B7 B11 H11 123.4(9) . . ?
B10 B11 Co2 115.88(10) . . ?
B10 B11 B6 59.69(10) . . ?
B10 B11 H11 116.5(10) . . ?
B12 B11 Co2 115.74(10) . . ?
B12 B11 B6 107.55(12) . . ?
B12 B11 B7 60.35(9) . . ?
B12 B11 B10 60.16(9) . . ?
B12 B11 H11 117.6(9) . . ?
B7 B12 B9 109.63(11) . . ?
B7 B12 B10 108.88(11) . . ?
B7 B12 H12 118.9(9) . . ?
C8 B12 B7 59.74(8) . . ?
C8 B12 B9 59.29(8) . . ?
C8 B12 B10 105.23(11) . . ?
C8 B12 B11 105.60(11) . . ?
C8 B12 H12 117.5(9) . . ?
B9 B12 B10 59.77(10) . . ?
B9 B12 H12 118.1(9) . . ?
B10 B12 H12 127.0(9) . . ?
B11 B12 B7 60.02(9) . . ?
B11 B12 B9 108.71(12) . . ?
B11 B12 B10 60.53(9) . . ?
B11 B12 H12 127.6(9) . . ?
Co2 C21 H21 125.7 . . ?
C22 C21 Co2 69.80(9) . . ?
C22 C21 H21 125.7 . . ?
C25 C21 Co2 69.91(9) . . ?
C25 C21 H21 125.7 . . ?
C25 C21 C22 108.52(16) . . ?
Co2 C22 H22 126.2 . . ?
C21 C22 Co2 70.23(8) . . ?
C21 C22 H22 126.2 . . ?
C21 C22 C23 107.60(15) . . ?
C23 C22 Co2 69.24(9) . . ?
C23 C22 H22 126.2 . . ?
Co2 C23 H23 126.1 . . ?
C22 C23 Co2 70.47(9) . . ?
C22 C23 H23 126.1 . . ?
C22 C23 C24 107.80(16) . . ?
C24 C23 Co2 69.76(9) . . ?
C24 C23 H23 126.1 . . ?
Co2 C24 H24 125.9 . . ?
C23 C24 Co2 69.62(9) . . ?
C23 C24 H24 125.9 . . ?
C25 C24 Co2 70.68(10) . . ?
C25 C24 C23 108.17(15) . . ?
C25 C24 H24 125.9 . . ?
Co2 C25 H25 126.0 . . ?
C21 C25 Co2 70.15(9) . . ?
C21 C25 H25 126.0 . . ?
C24 C25 Co2 69.40(10) . . ?
C24 C25 C21 107.90(15) . . ?
C24 C25 H25 126.0 . . ?
C8 C1' C2' 117.56(10) . . ?
C8 C1' B3' 117.49(10) . . ?
C8 C1' B4' 121.81(10) . . ?
C8 C1' B5' 121.82(11) . . ?
C8 C1' B6' 118.38(10) . . ?
C2' C1' B3' 61.15(8) . . ?
C2' C1' B4' 110.74(10) . . ?
C2' C1' B5' 110.65(10) . . ?
C2' C1' B6' 60.89(8) . . ?
B4' C1' B3' 62.01(8) . . ?
B4' C1' B5' 62.34(8) . . ?
B5' C1' B3' 113.15(10) . . ?
B6' C1' B3' 112.25(10) . . ?
B6' C1' B4' 112.30(10) . . ?
B6' C1' B5' 61.51(8) . . ?
C1' C2' H2' 114.9(9) . . ?
C1' C2' B3' 61.01(8) . . ?
C1' C2' B6' 60.77(8) . . ?
C1' C2' B7' 110.55(10) . . ?
C1' C2' B11' 110.55(10) . . ?
B3' C2' H2' 119.2(9) . . ?
B6' C2' H2' 114.9(9) . . ?
B6' C2' B3' 112.03(11) . . ?
B6' C2' B7' 112.42(11) . . ?
B6' C2' B11' 61.61(9) . . ?
B7' C2' H2' 125.7(9) . . ?
B7' C2' B3' 61.85(9) . . ?
B7' C2' B11' 62.45(9) . . ?
B11' C2' H2' 122.3(9) . . ?
B11' C2' B3' 113.00(11) . . ?
C1' B3' C2' 57.85(8) . . ?
C1' B3' H3' 116.4(9) . . ?
C1' B3' B4' 58.69(8) . . ?
C1' B3' B7' 105.51(10) . . ?
C1' B3' B8' 105.87(10) . . ?
C2' B3' H3' 117.2(9) . . ?
C2' B3' B4' 105.46(10) . . ?
C2' B3' B7' 58.71(8) . . ?
C2' B3' B8' 105.83(10) . . ?
B4' B3' H3' 123.2(9) . . ?
B7' B3' H3' 124.6(9) . . ?
B7' B3' B4' 108.80(11) . . ?
B8' B3' H3' 130.8(9) . . ?
B8' B3' B4' 60.62(9) . . ?
B8' B3' B7' 60.59(9) . . ?
C1' B4' B3' 59.30(8) . . ?
C1' B4' H4' 116.8(9) . . ?
C1' B4' B5' 59.07(8) . . ?
C1' B4' B8' 105.25(10) . . ?
C1' B4' B9' 105.34(10) . . ?
B3' B4' H4' 118.7(9) . . ?
B3' B4' B5' 108.28(10) . . ?
B3' B4' B8' 59.23(9) . . ?
B3' B4' B9' 107.51(11) . . ?
B5' B4' H4' 119.3(9) . . ?
B5' B4' B8' 108.32(11) . . ?
B8' B4' H4' 127.6(9) . . ?
B9' B4' H4' 128.4(9) . . ?
B9' B4' B5' 60.05(9) . . ?
B9' B4' B8' 60.22(9) . . ?
C1' B5' B4' 58.59(8) . . ?
C1' B5' H5' 118.7(9) . . ?
C1' B5' B6' 58.94(8) . . ?
C1' B5' B9' 104.80(11) . . ?
C1' B5' B10' 105.10(10) . . ?
B4' B5' H5' 119.4(9) . . ?
B4' B5' B10' 107.89(11) . . ?
B6' B5' B4' 107.18(10) . . ?
B6' B5' H5' 120.9(9) . . ?
B6' B5' B9' 106.78(11) . . ?
B6' B5' B10' 59.16(9) . . ?
B9' B5' B4' 59.82(9) . . ?
B9' B5' H5' 126.8(9) . . ?
B9' B5' B10' 60.08(9) . . ?
B10' B5' H5' 127.1(9) . . ?
C1' B6' C2' 58.34(8) . . ?
C1' B6' B5' 59.55(8) . . ?
C1' B6' H6' 116.0(9) . . ?
C1' B6' B10' 107.10(10) . . ?
C1' B6' B11' 106.76(11) . . ?
C2' B6' B5' 107.03(10) . . ?
C2' B6' H6' 116.7(10) . . ?
C2' B6' B10' 106.95(11) . . ?
C2' B6' B11' 59.32(9) . . ?
B5' B6' H6' 122.3(10) . . ?
B5' B6' B11' 110.12(11) . . ?
B10' B6' B5' 61.10(9) . . ?
B10' B6' H6' 129.9(10) . . ?
B10' B6' B11' 60.90(9) . . ?
B11' B6' H6' 123.7(10) . . ?
C2' B7' B3' 59.44(8) . . ?
C2' B7' H7' 117.3(9) . . ?
C2' B7' B8' 105.41(11) . . ?
C2' B7' B11' 58.88(9) . . ?
C2' B7' B12' 105.46(11) . . ?
B3' B7' H7' 118.8(9) . . ?
B3' B7' B8' 59.33(9) . . ?
B3' B7' B11' 108.15(11) . . ?
B3' B7' B12' 107.73(11) . . ?
B8' B7' H7' 127.2(9) . . ?
B8' B7' B11' 108.15(11) . . ?
B11' B7' H7' 119.7(9) . . ?
B12' B7' H7' 127.9(9) . . ?
B12' B7' B8' 60.26(9) . . ?
B12' B7' B11' 60.02(9) . . ?
B3' B8' B4' 60.15(8) . . ?
B3' B8' B7' 60.08(9) . . ?
B3' B8' H8' 119.6(9) . . ?
B3' B8' B9' 107.84(11) . . ?
B3' B8' B12' 107.99(11) . . ?
B4' B8' H8' 120.7(9) . . ?
B4' B8' B9' 59.71(9) . . ?
B4' B8' B12' 107.86(11) . . ?
B7' B8' B4' 108.03(10) . . ?
B7' B8' H8' 121.6(10) . . ?
B7' B8' B9' 107.73(11) . . ?
B7' B8' B12' 59.82(9) . . ?
B9' B8' H8' 123.3(9) . . ?
B9' B8' B12' 59.99(9) . . ?
B12' B8' H8' 123.7(9) . . ?
B4' B9' B5' 60.13(8) . . ?
B4' B9' B8' 60.07(9) . . ?
B4' B9' H9' 120.4(9) . . ?
B4' B9' B10' 108.11(11) . . ?
B4' B9' B12' 108.17(11) . . ?
B5' B9' B8' 108.27(10) . . ?
B5' B9' H9' 120.8(9) . . ?
B5' B9' B10' 60.04(9) . . ?
B5' B9' B12' 108.31(11) . . ?
B8' B9' H9' 121.6(9) . . ?
B8' B9' B12' 60.03(9) . . ?
B10' B9' B8' 108.14(11) . . ?
B10' B9' H9' 122.5(9) . . ?
B10' B9' B12' 60.15(9) . . ?
B12' B9' H9' 122.8(9) . . ?
B5' B10' B9' 59.88(9) . . ?
B5' B10' H10' 118.8(9) . . ?
B5' B10' B12' 108.05(11) . . ?
B6' B10' B5' 59.74(9) . . ?
B6' B10' B9' 107.09(10) . . ?
B6' B10' H10' 118.7(9) . . ?
B6' B10' B11' 59.88(9) . . ?
B6' B10' B12' 107.31(11) . . ?
B9' B10' H10' 124.0(9) . . ?
B9' B10' B12' 59.98(9) . . ?
B11' B10' B5' 108.21(10) . . ?
B11' B10' B9' 107.86(11) . . ?
B11' B10' H10' 122.0(10) . . ?
B11' B10' B12' 59.90(9) . . ?
B12' B10' H10' 125.8(9) . . ?
C2' B11' B6' 59.07(8) . . ?
C2' B11' B7' 58.66(8) . . ?
C2' B11' B10' 105.44(11) . . ?
C2' B11' H11' 117.6(9) . . ?
C2' B11' B12' 105.19(11) . . ?
B6' B11' B7' 107.31(11) . . ?
B6' B11' B10' 59.22(9) . . ?
B6' B11' H11' 117.8(9) . . ?
B6' B11' B12' 107.14(11) . . ?
B7' B11' H11' 121.7(9) . . ?
B10' B11' B7' 108.13(11) . . ?
B10' B11' H11' 125.7(9) . . ?
B10' B11' B12' 60.34(9) . . ?
B12' B11' B7' 59.89(9) . . ?
B12' B11' H11' 129.0(9) . . ?
B7' B12' B8' 59.92(9) . . ?
B7' B12' B9' 107.79(11) . . ?
B7' B12' B10' 107.82(11) . . ?
B7' B12' B11' 60.09(9) . . ?
B7' B12' H12' 120.1(9) . . ?
B8' B12' B10' 107.87(11) . . ?
B8' B12' H12' 120.9(9) . . ?
B9' B12' B8' 59.98(9) . . ?
B9' B12' B10' 59.87(9) . . ?
B9' B12' H12' 123.0(9) . . ?
B10' B12' H12' 123.4(9) . . ?
B11' B12' B8' 107.93(11) . . ?
B11' B12' B9' 107.65(11) . . ?
B11' B12' B10' 59.75(9) . . ?
B11' B12' H12' 121.6(9) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 B3 B4 B5 33.82(11) . . . . ?
C1 B3 B4 C8 131.50(11) . . . . ?
C1 B3 B4 B9 97.43(12) . . . . ?
C1 B3 B7 Co2 51.82(8) . . . . ?
C1 B3 B7 C8 -94.04(11) . . . . ?
C1 B3 B7 B11 2.43(13) . . . . ?
C1 B3 B7 B12 -60.16(12) . . . . ?
C1 B3 C8 B4 -40.37(10) . . . . ?
C1 B3 C8 B7 101.54(11) . . . . ?
C1 B3 C8 B9 -4.02(14) . . . . ?
C1 B3 C8 B12 64.45(13) . . . . ?
C1 B3 C8 C1' -150.43(11) . . . . ?
C1 B4 B5 B6 33.99(11) . . . . ?
C1 B4 B5 B9 135.00(12) . . . . ?
C1 B4 B5 B10 97.49(12) . . . . ?
C1 B4 C8 B3 40.84(10) . . . . ?
C1 B4 C8 B7 3.40(14) . . . . ?
C1 B4 C8 B9 -101.16(12) . . . . ?
C1 B4 C8 B12 -64.94(13) . . . . ?
C1 B4 C8 C1' 150.17(11) . . . . ?
C1 B4 B9 B5 -39.21(10) . . . . ?
C1 B4 B9 C8 95.33(11) . . . . ?
C1 B4 B9 B10 -1.73(14) . . . . ?
C1 B4 B9 B12 61.83(13) . . . . ?
C1 B5 B6 Co2 27.68(10) . . . . ?
C1 B5 B6 B10 134.91(12) . . . . ?
C1 B5 B6 B11 97.72(12) . . . . ?
C1 B5 B9 B4 38.67(10) . . . . ?
C1 B5 B9 C8 -0.34(15) . . . . ?
C1 B5 B9 B10 -99.49(12) . . . . ?
C1 B5 B9 B12 -61.71(14) . . . . ?
C1 B5 B10 B6 -39.16(10) . . . . ?
C1 B5 B10 B9 98.91(12) . . . . ?
C1 B5 B10 B11 -1.44(15) . . . . ?
C1 B5 B10 B12 61.30(14) . . . . ?
C1 B6 B10 B5 38.47(10) . . . . ?
C1 B6 B10 B9 1.11(15) . . . . ?
C1 B6 B10 B11 -99.75(12) . . . . ?
C1 B6 B10 B12 -62.28(14) . . . . ?
C1 B6 B11 Co2 -50.43(8) . . . . ?
C1 B6 B11 B7 -3.59(14) . . . . ?
C1 B6 B11 B10 98.05(12) . . . . ?
C1 B6 B11 B12 60.17(13) . . . . ?
Co2 C1 B3 B4 -152.18(10) . . . . ?
Co2 C1 B3 B7 -51.22(8) . . . . ?
Co2 C1 B3 C8 -111.65(9) . . . . ?
Co2 C1 B4 B3 29.70(10) . . . . ?
Co2 C1 B4 B5 -112.39(13) . . . . ?
Co2 C1 B4 C8 -11.38(15) . . . . ?
Co2 C1 B4 B9 -72.87(13) . . . . ?
Co2 C1 B5 B4 111.66(11) . . . . ?
Co2 C1 B5 B6 -30.04(10) . . . . ?
Co2 C1 B5 B9 72.14(13) . . . . ?
Co2 C1 B5 B10 9.54(15) . . . . ?
Co2 C1 B6 B5 152.35(10) . . . . ?
Co2 C1 B6 B10 113.24(10) . . . . ?
Co2 C1 B6 B11 51.02(9) . . . . ?
Co2 B3 B4 C1 -28.50(10) . . . . ?
Co2 B3 B4 B5 5.32(15) . . . . ?
Co2 B3 B4 C8 103.00(11) . . . . ?
Co2 B3 B4 B9 68.93(13) . . . . ?
Co2 B3 B7 C8 -145.86(9) . . . . ?
Co2 B3 B7 B11 -49.38(8) . . . . ?
Co2 B3 B7 B12 -111.98(10) . . . . ?
Co2 B3 C8 B4 -108.23(10) . . . . ?
Co2 B3 C8 B7 33.69(9) . . . . ?
Co2 B3 C8 B9 -71.87(12) . . . . ?
Co2 B3 C8 B12 -3.40(14) . . . . ?
Co2 B3 C8 C1' 141.71(10) . . . . ?
Co2 B6 B10 B5 106.16(12) . . . . ?
Co2 B6 B10 B9 68.80(14) . . . . ?
Co2 B6 B10 B11 -32.06(10) . . . . ?
Co2 B6 B10 B12 5.41(16) . . . . ?
Co2 B6 B11 B7 46.84(9) . . . . ?
Co2 B6 B11 B10 148.48(10) . . . . ?
Co2 B6 B11 B12 110.60(10) . . . . ?
Co2 B7 C8 B3 -32.42(9) . . . . ?
Co2 B7 C8 B4 4.78(14) . . . . ?
Co2 B7 C8 B9 73.35(12) . . . . ?
Co2 B7 C8 B12 108.76(10) . . . . ?
Co2 B7 C8 C1' -142.66(10) . . . . ?
Co2 B7 B11 B6 -46.89(9) . . . . ?
Co2 B7 B11 B10 -110.21(11) . . . . ?
Co2 B7 B11 B12 -147.15(10) . . . . ?
Co2 B7 B12 C8 -100.55(10) . . . . ?
Co2 B7 B12 B9 -67.24(13) . . . . ?
Co2 B7 B12 B10 -3.54(15) . . . . ?
Co2 B7 B12 B11 33.56(10) . . . . ?
Co2 B11 B12 B7 -32.65(10) . . . . ?
Co2 B11 B12 C8 7.43(14) . . . . ?
Co2 B11 B12 B9 69.71(13) . . . . ?
Co2 B11 B12 B10 106.38(12) . . . . ?
Co2 C21 C22 C23 -59.39(11) . . . . ?
Co2 C21 C25 C24 59.35(11) . . . . ?
Co2 C22 C23 C24 -60.04(11) . . . . ?
Co2 C23 C24 C25 -60.44(11) . . . . ?
Co2 C24 C25 C21 -59.83(11) . . . . ?
B3 C1 B4 B5 -142.08(12) . . . . ?
B3 C1 B4 C8 -41.08(10) . . . . ?
B3 C1 B4 B9 -102.57(11) . . . . ?
B3 C1 B5 B4 37.23(11) . . . . ?
B3 C1 B5 B6 -104.46(13) . . . . ?
B3 C1 B5 B9 -2.29(16) . . . . ?
B3 C1 B5 B10 -64.88(14) . . . . ?
B3 C1 B6 Co2 -45.58(9) . . . . ?
B3 C1 B6 B5 106.77(12) . . . . ?
B3 C1 B6 B10 67.66(14) . . . . ?
B3 C1 B6 B11 5.44(15) . . . . ?
B3 B4 B5 C1 -33.48(10) . . . . ?
B3 B4 B5 B6 0.51(15) . . . . ?
B3 B4 B5 B9 101.52(12) . . . . ?
B3 B4 B5 B10 64.01(14) . . . . ?
B3 B4 C8 B7 -37.44(11) . . . . ?
B3 B4 C8 B9 -141.99(11) . . . . ?
B3 B4 C8 B12 -105.78(11) . . . . ?
B3 B4 C8 C1' 109.33(12) . . . . ?
B3 B4 B9 B5 -100.69(12) . . . . ?
B3 B4 B9 C8 33.85(10) . . . . ?
B3 B4 B9 B10 -63.21(14) . . . . ?
B3 B4 B9 B12 0.34(14) . . . . ?
B3 B7 C8 B4 37.20(11) . . . . ?
B3 B7 C8 B9 105.77(11) . . . . ?
B3 B7 C8 B12 141.19(11) . . . . ?
B3 B7 C8 C1' -110.24(12) . . . . ?
B3 B7 B11 Co2 47.64(8) . . . . ?
B3 B7 B11 B6 0.74(14) . . . . ?
B3 B7 B11 B10 -62.57(13) . . . . ?
B3 B7 B11 B12 -99.51(11) . . . . ?
B3 B7 B12 C8 -33.64(9) . . . . ?
B3 B7 B12 B9 -0.34(14) . . . . ?
B3 B7 B12 B10 63.37(13) . . . . ?
B3 B7 B12 B11 100.47(11) . . . . ?
B3 C8 B9 B4 -36.72(11) . . . . ?
B3 C8 B9 B5 2.84(15) . . . . ?
B3 C8 B9 B10 65.37(14) . . . . ?
B3 C8 B9 B12 105.29(11) . . . . ?
B3 C8 B12 B7 37.73(10) . . . . ?
B3 C8 B12 B9 -105.29(12) . . . . ?
B3 C8 B12 B10 -65.53(13) . . . . ?
B3 C8 B12 B11 -2.49(15) . . . . ?
B3 C8 C1' C2' 37.05(16) . . . . ?
B3 C8 C1' B3' -32.95(16) . . . . ?
B3 C8 C1' B4' -105.51(13) . . . . ?
B3 C8 C1' B5' 179.44(11) . . . . ?
B3 C8 C1' B6' 107.06(13) . . . . ?
B4 C1 B3 Co2 152.18(10) . . . . ?
B4 C1 B3 B7 100.95(11) . . . . ?
B4 C1 B3 C8 40.53(10) . . . . ?
B4 C1 B5 B6 -141.70(12) . . . . ?
B4 C1 B5 B9 -39.52(11) . . . . ?
B4 C1 B5 B10 -102.11(12) . . . . ?
B4 C1 B6 Co2 -115.59(10) . . . . ?
B4 C1 B6 B5 36.76(11) . . . . ?
B4 C1 B6 B10 -2.35(15) . . . . ?
B4 C1 B6 B11 -64.57(14) . . . . ?
B4 B3 B7 Co2 112.52(9) . . . . ?
B4 B3 B7 C8 -33.34(9) . . . . ?
B4 B3 B7 B11 63.13(13) . . . . ?
B4 B3 B7 B12 0.54(13) . . . . ?
B4 B3 C8 B7 141.91(11) . . . . ?
B4 B3 C8 B9 36.36(11) . . . . ?
B4 B3 C8 B12 104.83(12) . . . . ?
B4 B3 C8 C1' -110.06(13) . . . . ?
B4 B5 B6 C1 -33.71(11) . . . . ?
B4 B5 B6 Co2 -6.03(16) . . . . ?
B4 B5 B6 B10 101.20(13) . . . . ?
B4 B5 B6 B11 64.01(14) . . . . ?
B4 B5 B9 C8 -39.01(10) . . . . ?
B4 B5 B9 B10 -138.16(11) . . . . ?
B4 B5 B9 B12 -100.38(12) . . . . ?
B4 B5 B10 B6 -100.50(12) . . . . ?
B4 B5 B10 B9 37.57(10) . . . . ?
B4 B5 B10 B11 -62.78(14) . . . . ?
B4 B5 B10 B12 -0.03(15) . . . . ?
B4 C8 B9 B5 39.56(11) . . . . ?
B4 C8 B9 B10 102.09(12) . . . . ?
B4 C8 B9 B12 142.02(11) . . . . ?
B4 C8 B12 B7 106.88(11) . . . . ?
B4 C8 B12 B9 -36.15(10) . . . . ?
B4 C8 B12 B10 3.62(14) . . . . ?
B4 C8 B12 B11 66.66(13) . . . . ?
B4 C8 C1' C2' -35.98(16) . . . . ?
B4 C8 C1' B3' -105.98(13) . . . . ?
B4 C8 C1' B4' -178.53(11) . . . . ?
B4 C8 C1' B5' 106.41(14) . . . . ?
B4 C8 C1' B6' 34.04(16) . . . . ?
B4 B9 B10 B5 -37.29(11) . . . . ?
B4 B9 B10 B6 0.37(15) . . . . ?
B4 B9 B10 B11 64.27(14) . . . . ?
B4 B9 B10 B12 100.56(12) . . . . ?
B4 B9 B12 B7 0.00(15) . . . . ?
B4 B9 B12 C8 33.48(10) . . . . ?
B4 B9 B12 B10 -100.93(12) . . . . ?
B4 B9 B12 B11 -63.94(14) . . . . ?
B5 C1 B3 Co2 115.46(12) . . . . ?
B5 C1 B3 B4 -36.72(12) . . . . ?
B5 C1 B3 B7 64.24(14) . . . . ?
B5 C1 B3 C8 3.81(15) . . . . ?
B5 C1 B4 B3 142.08(12) . . . . ?
B5 C1 B4 C8 101.00(12) . . . . ?
B5 C1 B4 B9 39.52(11) . . . . ?
B5 C1 B6 Co2 -152.35(10) . . . . ?
B5 C1 B6 B10 -39.11(11) . . . . ?
B5 C1 B6 B11 -101.33(12) . . . . ?
B5 B4 C8 B3 102.13(11) . . . . ?
B5 B4 C8 B7 64.68(13) . . . . ?
B5 B4 C8 B9 -39.87(10) . . . . ?
B5 B4 C8 B12 -3.65(14) . . . . ?
B5 B4 C8 C1' -148.54(11) . . . . ?
B5 B4 B9 C8 134.54(11) . . . . ?
B5 B4 B9 B10 37.48(11) . . . . ?
B5 B4 B9 B12 101.04(12) . . . . ?
B5 B6 B10 B9 -37.36(11) . . . . ?
B5 B6 B10 B11 -138.22(12) . . . . ?
B5 B6 B10 B12 -100.75(13) . . . . ?
B5 B6 B11 Co2 -111.42(11) . . . . ?
B5 B6 B11 B7 -64.58(14) . . . . ?
B5 B6 B11 B10 37.06(11) . . . . ?
B5 B6 B11 B12 -0.82(15) . . . . ?
B5 B9 B10 B6 37.65(11) . . . . ?
B5 B9 B10 B11 101.56(12) . . . . ?
B5 B9 B10 B12 137.84(11) . . . . ?
B5 B9 B12 B7 63.15(14) . . . . ?
B5 B9 B12 C8 96.63(12) . . . . ?
B5 B9 B12 B10 -37.79(11) . . . . ?
B5 B9 B12 B11 -0.79(15) . . . . ?
B5 B10 B11 Co2 -6.29(15) . . . . ?
B5 B10 B11 B6 -37.69(11) . . . . ?
B5 B10 B11 B7 62.85(14) . . . . ?
B5 B10 B11 B12 99.87(12) . . . . ?
B5 B10 B12 B7 -64.77(14) . . . . ?
B5 B10 B12 C8 -2.07(14) . . . . ?
B5 B10 B12 B9 37.46(11) . . . . ?
B5 B10 B12 B11 -101.65(12) . . . . ?
B6 C1 B3 Co2 46.24(9) . . . . ?
B6 C1 B3 B4 -105.94(13) . . . . ?
B6 C1 B3 B7 -4.98(14) . . . . ?
B6 C1 B3 C8 -65.41(13) . . . . ?
B6 C1 B4 B3 105.16(13) . . . . ?
B6 C1 B4 B5 -36.92(12) . . . . ?
B6 C1 B4 C8 64.08(13) . . . . ?
B6 C1 B4 B9 2.59(15) . . . . ?
B6 C1 B5 B4 141.70(12) . . . . ?
B6 C1 B5 B9 102.17(13) . . . . ?
B6 C1 B5 B10 39.58(11) . . . . ?
B6 B5 B9 B4 100.65(12) . . . . ?
B6 B5 B9 C8 61.64(14) . . . . ?
B6 B5 B9 B10 -37.51(11) . . . . ?
B6 B5 B9 B12 0.27(15) . . . . ?
B6 B5 B10 B9 138.07(12) . . . . ?
B6 B5 B10 B11 37.72(11) . . . . ?
B6 B5 B10 B12 100.46(12) . . . . ?
B6 B10 B11 Co2 31.40(10) . . . . ?
B6 B10 B11 B7 100.54(12) . . . . ?
B6 B10 B11 B12 137.56(12) . . . . ?
B6 B10 B12 B7 -1.10(15) . . . . ?
B6 B10 B12 C8 61.59(14) . . . . ?
B6 B10 B12 B9 101.13(13) . . . . ?
B6 B10 B12 B11 -37.98(11) . . . . ?
B6 B11 B12 B7 -101.37(12) . . . . ?
B6 B11 B12 C8 -61.28(13) . . . . ?
B6 B11 B12 B9 0.99(15) . . . . ?
B6 B11 B12 B10 37.66(11) . . . . ?
B7 B3 B4 C1 -97.98(11) . . . . ?
B7 B3 B4 B5 -64.16(13) . . . . ?
B7 B3 B4 C8 33.53(9) . . . . ?
B7 B3 B4 B9 -0.55(14) . . . . ?
B7 B3 C8 B4 -141.91(11) . . . . ?
B7 B3 C8 B9 -105.56(12) . . . . ?
B7 B3 C8 B12 -37.09(10) . . . . ?
B7 B3 C8 C1' 108.02(12) . . . . ?
B7 C8 B9 B4 -106.70(11) . . . . ?
B7 C8 B9 B5 -67.14(14) . . . . ?
B7 C8 B9 B10 -4.61(15) . . . . ?
B7 C8 B9 B12 35.32(11) . . . . ?
B7 C8 B12 B9 -143.02(11) . . . . ?
B7 C8 B12 B10 -103.26(11) . . . . ?
B7 C8 B12 B11 -40.22(10) . . . . ?
B7 C8 C1' C2' 110.03(12) . . . . ?
B7 C8 C1' B3' 40.03(15) . . . . ?
B7 C8 C1' B4' -32.52(16) . . . . ?
B7 C8 C1' B5' -107.58(13) . . . . ?
B7 C8 C1' B6' -179.95(10) . . . . ?
B7 B11 B12 C8 40.09(10) . . . . ?
B7 B11 B12 B9 102.36(12) . . . . ?
B7 B11 B12 B10 139.03(12) . . . . ?
C8 B3 B4 C1 -131.50(11) . . . . ?
C8 B3 B4 B5 -97.69(12) . . . . ?
C8 B3 B4 B9 -34.08(10) . . . . ?
C8 B3 B7 Co2 145.86(9) . . . . ?
C8 B3 B7 B11 96.48(11) . . . . ?
C8 B3 B7 B12 33.88(9) . . . . ?
C8 B4 B5 C1 -95.36(11) . . . . ?
C8 B4 B5 B6 -61.36(14) . . . . ?
C8 B4 B5 B9 39.64(10) . . . . ?
C8 B4 B5 B10 2.14(14) . . . . ?
C8 B4 B9 B5 -134.54(11) . . . . ?
C8 B4 B9 B10 -97.07(12) . . . . ?
C8 B4 B9 B12 -33.51(10) . . . . ?
C8 B7 B11 Co2 107.96(9) . . . . ?
C8 B7 B11 B6 61.07(13) . . . . ?
C8 B7 B11 B10 -2.25(14) . . . . ?
C8 B7 B11 B12 -39.19(10) . . . . ?
C8 B7 B12 B9 33.30(10) . . . . ?
C8 B7 B12 B10 97.01(12) . . . . ?
C8 B7 B12 B11 134.11(11) . . . . ?
C8 B9 B10 B5 -98.64(11) . . . . ?
C8 B9 B10 B6 -60.99(14) . . . . ?
C8 B9 B10 B11 2.92(15) . . . . ?
C8 B9 B10 B12 39.20(10) . . . . ?
C8 B9 B12 B7 -33.48(10) . . . . ?
C8 B9 B12 B10 -134.41(11) . . . . ?
C8 B9 B12 B11 -97.42(11) . . . . ?
C8 C1' C2' B3' -107.87(12) . . . . ?
C8 C1' C2' B6' 108.85(12) . . . . ?
C8 C1' C2' B7' -146.26(11) . . . . ?
C8 C1' C2' B11' 146.51(11) . . . . ?
C8 C1' B3' C2' 107.99(12) . . . . ?
C8 C1' B3' B4' -113.36(12) . . . . ?
C8 C1' B3' B7' 143.78(11) . . . . ?
C8 C1' B3' B8' -153.02(11) . . . . ?
C8 C1' B4' B3' 106.58(13) . . . . ?
C8 C1' B4' B5' -112.05(13) . . . . ?
C8 C1' B4' B8' 145.44(11) . . . . ?
C8 C1' B4' B9' -151.88(11) . . . . ?
C8 C1' B5' B4' 112.04(13) . . . . ?
C8 C1' B5' B6' -107.44(13) . . . . ?
C8 C1' B5' B9' 151.64(11) . . . . ?
C8 C1' B5' B10' -145.95(12) . . . . ?
C8 C1' B6' C2' -107.52(12) . . . . ?
C8 C1' B6' B5' 112.88(13) . . . . ?
C8 C1' B6' B10' 152.77(11) . . . . ?
C8 C1' B6' B11' -143.26(11) . . . . ?
B9 B4 B5 C1 -135.00(12) . . . . ?
B9 B4 B5 B6 -101.01(13) . . . . ?
B9 B4 B5 B10 -37.51(11) . . . . ?
B9 B4 C8 B3 141.99(11) . . . . ?
B9 B4 C8 B7 104.55(12) . . . . ?
B9 B4 C8 B12 36.22(11) . . . . ?
B9 B4 C8 C1' -108.67(13) . . . . ?
B9 B5 B6 C1 -97.38(12) . . . . ?
B9 B5 B6 Co2 -69.70(14) . . . . ?
B9 B5 B6 B10 37.53(11) . . . . ?
B9 B5 B6 B11 0.34(15) . . . . ?
B9 B5 B10 B6 -138.07(12) . . . . ?
B9 B5 B10 B11 -100.35(12) . . . . ?
B9 B5 B10 B12 -37.61(10) . . . . ?
B9 C8 B12 B7 143.02(11) . . . . ?
B9 C8 B12 B10 39.76(10) . . . . ?
B9 C8 B12 B11 102.80(12) . . . . ?
B9 C8 C1' C2' -107.78(13) . . . . ?
B9 C8 C1' B3' -177.77(11) . . . . ?
B9 C8 C1' B4' 109.67(13) . . . . ?
B9 C8 C1' B5' 34.61(17) . . . . ?
B9 C8 C1' B6' -37.76(16) . . . . ?
B9 B10 B11 Co2 -69.55(13) . . . . ?
B9 B10 B11 B6 -100.95(13) . . . . ?
B9 B10 B11 B7 -0.41(15) . . . . ?
B9 B10 B11 B12 36.61(11) . . . . ?
B9 B10 B12 B7 -102.22(12) . . . . ?
B9 B10 B12 C8 -39.53(10) . . . . ?
B9 B10 B12 B11 -139.10(12) . . . . ?
B10 B5 B6 C1 -134.91(12) . . . . ?
B10 B5 B6 Co2 -107.23(12) . . . . ?
B10 B5 B6 B11 -37.19(11) . . . . ?
B10 B5 B9 B4 138.16(11) . . . . ?
B10 B5 B9 C8 99.15(12) . . . . ?
B10 B5 B9 B12 37.78(11) . . . . ?
B10 B6 B11 Co2 -148.48(10) . . . . ?
B10 B6 B11 B7 -101.64(12) . . . . ?
B10 B6 B11 B12 -37.88(11) . . . . ?
B10 B9 B12 B7 100.93(12) . . . . ?
B10 B9 B12 C8 134.41(11) . . . . ?
B10 B9 B12 B11 37.00(11) . . . . ?
B10 B11 B12 B7 -139.03(12) . . . . ?
B10 B11 B12 C8 -98.95(12) . . . . ?
B10 B11 B12 B9 -36.67(11) . . . . ?
B11 B6 B10 B5 138.22(12) . . . . ?
B11 B6 B10 B9 100.86(12) . . . . ?
B11 B6 B10 B12 37.47(11) . . . . ?
B11 B7 C8 B3 -101.44(11) . . . . ?
B11 B7 C8 B4 -64.23(13) . . . . ?
B11 B7 C8 B9 4.34(14) . . . . ?
B11 B7 C8 B12 39.75(10) . . . . ?
B11 B7 C8 C1' 148.33(11) . . . . ?
B11 B7 B12 C8 -134.11(11) . . . . ?
B11 B7 B12 B9 -100.81(12) . . . . ?
B11 B7 B12 B10 -37.10(11) . . . . ?
B11 B10 B12 B7 36.88(11) . . . . ?
B11 B10 B12 C8 99.57(11) . . . . ?
B11 B10 B12 B9 139.10(12) . . . . ?
B12 B7 C8 B3 -141.19(11) . . . . ?
B12 B7 C8 B4 -103.98(12) . . . . ?
B12 B7 C8 B9 -35.41(11) . . . . ?
B12 B7 C8 C1' 108.58(12) . . . . ?
B12 B7 B11 Co2 147.15(10) . . . . ?
B12 B7 B11 B6 100.25(12) . . . . ?
B12 B7 B11 B10 36.94(11) . . . . ?
B12 C8 B9 B4 -142.02(11) . . . . ?
B12 C8 B9 B5 -102.46(12) . . . . ?
B12 C8 B9 B10 -39.93(11) . . . . ?
B12 C8 C1' C2' -179.25(11) . . . . ?
B12 C8 C1' B3' 110.75(13) . . . . ?
B12 C8 C1' B4' 38.20(16) . . . . ?
B12 C8 C1' B5' -36.86(16) . . . . ?
B12 C8 C1' B6' -109.24(13) . . . . ?
B12 B9 B10 B5 -137.84(11) . . . . ?
B12 B9 B10 B6 -100.19(12) . . . . ?
B12 B9 B10 B11 -36.29(11) . . . . ?
B12 B10 B11 Co2 -106.16(11) . . . . ?
B12 B10 B11 B6 -137.56(12) . . . . ?
B12 B10 B11 B7 -37.02(11) . . . . ?
C21 C22 C23 Co2 60.01(11) . . . . ?
C21 C22 C23 C24 -0.03(17) . . . . ?
C22 C21 C25 Co2 -59.32(11) . . . . ?
C22 C21 C25 C24 0.03(18) . . . . ?
C22 C23 C24 Co2 60.49(11) . . . . ?
C22 C23 C24 C25 0.05(18) . . . . ?
C23 C24 C25 Co2 59.78(11) . . . . ?
C23 C24 C25 C21 -0.05(18) . . . . ?
C25 C21 C22 Co2 59.39(11) . . . . ?
C25 C21 C22 C23 0.00(17) . . . . ?
C1' C8 B9 B4 109.78(13) . . . . ?
C1' C8 B9 B5 149.34(12) . . . . ?
C1' C8 B9 B10 -148.13(12) . . . . ?
C1' C8 B9 B12 -108.20(13) . . . . ?
C1' C8 B12 B7 -107.71(12) . . . . ?
C1' C8 B12 B9 109.26(12) . . . . ?
C1' C8 B12 B10 149.03(11) . . . . ?
C1' C8 B12 B11 -147.93(11) . . . . ?
C1' C2' B3' B4' -35.84(9) . . . . ?
C1' C2' B3' B7' -138.74(11) . . . . ?
C1' C2' B3' B8' -99.06(11) . . . . ?
C1' C2' B6' B5' 35.76(10) . . . . ?
C1' C2' B6' B10' 99.97(11) . . . . ?
C1' C2' B6' B11' 139.44(11) . . . . ?
C1' C2' B7' B3' 38.03(10) . . . . ?
C1' C2' B7' B8' -0.96(14) . . . . ?
C1' C2' B7' B11' -103.14(11) . . . . ?
C1' C2' B7' B12' -63.72(13) . . . . ?
C1' C2' B11' B6' -37.30(10) . . . . ?
C1' C2' B11' B7' 103.14(12) . . . . ?
C1' C2' B11' B10' 1.03(14) . . . . ?
C1' C2' B11' B12' 63.84(14) . . . . ?
C1' B3' B4' B5' -34.33(10) . . . . ?
C1' B3' B4' B8' -135.21(11) . . . . ?
C1' B3' B4' B9' -97.77(11) . . . . ?
C1' B3' B7' C2' -35.41(9) . . . . ?
C1' B3' B7' B8' 99.75(11) . . . . ?
C1' B3' B7' B11' -1.01(14) . . . . ?
C1' B3' B7' B12' 62.42(13) . . . . ?
C1' B3' B8' B4' 38.74(9) . . . . ?
C1' B3' B8' B7' -99.15(11) . . . . ?
C1' B3' B8' B9' 1.45(14) . . . . ?
C1' B3' B8' B12' -61.95(13) . . . . ?
C1' B4' B5' B6' -34.76(10) . . . . ?
C1' B4' B5' B9' -134.53(11) . . . . ?
C1' B4' B5' B10' -97.10(11) . . . . ?
C1' B4' B8' B3' -38.89(10) . . . . ?
C1' B4' B8' B7' -1.21(14) . . . . ?
C1' B4' B8' B9' 99.20(11) . . . . ?
C1' B4' B8' B12' 62.01(13) . . . . ?
C1' B4' B9' B5' 39.35(10) . . . . ?
C1' B4' B9' B8' -99.05(11) . . . . ?
C1' B4' B9' B10' 1.88(14) . . . . ?
C1' B4' B9' B12' -61.77(13) . . . . ?
C1' B5' B6' C2' -35.24(9) . . . . ?
C1' B5' B6' B10' -135.56(11) . . . . ?
C1' B5' B6' B11' -98.10(11) . . . . ?
C1' B5' B9' B4' -39.00(9) . . . . ?
C1' B5' B9' B8' -1.71(13) . . . . ?
C1' B5' B9' B10' 99.14(11) . . . . ?
C1' B5' B9' B12' 61.88(13) . . . . ?
C1' B5' B10' B6' 38.41(10) . . . . ?
C1' B5' B10' B9' -98.63(11) . . . . ?
C1' B5' B10' B11' 1.88(14) . . . . ?
C1' B5' B10' B12' -61.51(13) . . . . ?
C1' B6' B10' B5' -39.16(10) . . . . ?
C1' B6' B10' B9' -1.08(15) . . . . ?
C1' B6' B10' B11' 100.02(11) . . . . ?
C1' B6' B10' B12' 62.02(13) . . . . ?
C1' B6' B11' C2' 35.31(9) . . . . ?
C1' B6' B11' B7' 0.57(14) . . . . ?
C1' B6' B11' B10' -100.59(11) . . . . ?
C1' B6' B11' B12' -62.44(13) . . . . ?
C2' C1' B3' B4' 138.65(10) . . . . ?
C2' C1' B3' B7' 35.79(10) . . . . ?
C2' C1' B3' B8' 98.99(11) . . . . ?
C2' C1' B4' B3' -38.22(10) . . . . ?
C2' C1' B4' B5' 103.14(11) . . . . ?
C2' C1' B4' B8' 0.64(13) . . . . ?
C2' C1' B4' B9' 63.32(13) . . . . ?
C2' C1' B5' B4' -103.28(11) . . . . ?
C2' C1' B5' B6' 37.24(10) . . . . ?
C2' C1' B5' B9' -63.68(12) . . . . ?
C2' C1' B5' B10' -1.27(14) . . . . ?
C2' C1' B6' B5' -139.60(11) . . . . ?
C2' C1' B6' B10' -99.71(12) . . . . ?
C2' C1' B6' B11' -35.73(10) . . . . ?
C2' B3' B4' C1' 35.47(9) . . . . ?
C2' B3' B4' B5' 1.13(13) . . . . ?
C2' B3' B4' B8' -99.74(11) . . . . ?
C2' B3' B4' B9' -62.30(13) . . . . ?
C2' B3' B7' B8' 135.16(11) . . . . ?
C2' B3' B7' B11' 34.40(10) . . . . ?
C2' B3' B7' B12' 97.83(12) . . . . ?
C2' B3' B8' B4' 99.10(11) . . . . ?
C2' B3' B8' B7' -38.78(10) . . . . ?
C2' B3' B8' B9' 61.81(13) . . . . ?
C2' B3' B8' B12' -1.58(14) . . . . ?
C2' B6' B10' B5' -100.46(11) . . . . ?
C2' B6' B10' B9' -62.37(14) . . . . ?
C2' B6' B10' B11' 38.73(10) . . . . ?
C2' B6' B10' B12' 0.73(14) . . . . ?
C2' B6' B11' B7' -34.74(10) . . . . ?
C2' B6' B11' B10' -135.90(11) . . . . ?
C2' B6' B11' B12' -97.75(12) . . . . ?
C2' B7' B8' B3' 39.04(10) . . . . ?
C2' B7' B8' B4' 1.33(14) . . . . ?
C2' B7' B8' B9' -61.75(13) . . . . ?
C2' B7' B8' B12' -99.26(12) . . . . ?
C2' B7' B11' B6' 34.91(10) . . . . ?
C2' B7' B11' B10' 97.40(12) . . . . ?
C2' B7' B11' B12' 135.05(11) . . . . ?
C2' B7' B12' B8' 99.18(11) . . . . ?
C2' B7' B12' B9' 61.65(13) . . . . ?
C2' B7' B12' B10' -1.56(14) . . . . ?
C2' B7' B12' B11' -38.87(10) . . . . ?
C2' B11' B12' B7' 38.71(10) . . . . ?
C2' B11' B12' B8' 1.26(15) . . . . ?
C2' B11' B12' B9' -62.06(14) . . . . ?
C2' B11' B12' B10' -99.38(11) . . . . ?
B3' C1' C2' B6' -143.28(11) . . . . ?
B3' C1' C2' B7' -38.39(10) . . . . ?
B3' C1' C2' B11' -105.62(12) . . . . ?
B3' C1' B4' B5' 141.36(11) . . . . ?
B3' C1' B4' B8' 38.86(10) . . . . ?
B3' C1' B4' B9' 101.54(11) . . . . ?
B3' C1' B5' B4' -36.84(10) . . . . ?
B3' C1' B5' B6' 103.68(11) . . . . ?
B3' C1' B5' B9' 2.76(14) . . . . ?
B3' C1' B5' B10' 65.17(13) . . . . ?
B3' C1' B6' C2' 34.46(10) . . . . ?
B3' C1' B6' B5' -105.14(11) . . . . ?
B3' C1' B6' B10' -65.25(13) . . . . ?
B3' C1' B6' B11' -1.28(14) . . . . ?
B3' C2' B6' C1' -34.35(10) . . . . ?
B3' C2' B6' B5' 1.41(14) . . . . ?
B3' C2' B6' B10' 65.63(13) . . . . ?
B3' C2' B6' B11' 105.09(12) . . . . ?
B3' C2' B7' B8' -38.98(10) . . . . ?
B3' C2' B7' B11' -141.17(11) . . . . ?
B3' C2' B7' B12' -101.75(11) . . . . ?
B3' C2' B11' B6' -103.52(12) . . . . ?
B3' C2' B11' B7' 36.91(11) . . . . ?
B3' C2' B11' B10' -65.19(14) . . . . ?
B3' C2' B11' B12' -2.38(15) . . . . ?
B3' B4' B5' C1' 34.43(10) . . . . ?
B3' B4' B5' B6' -0.33(14) . . . . ?
B3' B4' B5' B9' -100.10(11) . . . . ?
B3' B4' B5' B10' -62.67(13) . . . . ?
B3' B4' B8' B7' 37.68(10) . . . . ?
B3' B4' B8' B9' 138.09(11) . . . . ?
B3' B4' B8' B12' 100.90(12) . . . . ?
B3' B4' B9' B5' 101.40(11) . . . . ?
B3' B4' B9' B8' -37.00(10) . . . . ?
B3' B4' B9' B10' 63.94(14) . . . . ?
B3' B4' B9' B12' 0.28(14) . . . . ?
B3' B7' B8' B4' -37.71(10) . . . . ?
B3' B7' B8' B9' -100.78(12) . . . . ?
B3' B7' B8' B12' -138.30(12) . . . . ?
B3' B7' B11' C2' -34.63(10) . . . . ?
B3' B7' B11' B6' 0.28(14) . . . . ?
B3' B7' B11' B10' 62.77(13) . . . . ?
B3' B7' B11' B12' 100.42(12) . . . . ?
B3' B7' B12' B8' 36.92(10) . . . . ?
B3' B7' B12' B9' -0.61(15) . . . . ?
B3' B7' B12' B10' -63.82(13) . . . . ?
B3' B7' B12' B11' -101.14(12) . . . . ?
B3' B8' B9' B4' 37.49(10) . . . . ?
B3' B8' B9' B5' 0.17(14) . . . . ?
B3' B8' B9' B10' -63.39(13) . . . . ?
B3' B8' B9' B12' -100.88(12) . . . . ?
B3' B8' B12' B7' -37.31(11) . . . . ?
B3' B8' B12' B9' 100.63(12) . . . . ?
B3' B8' B12' B10' 63.33(14) . . . . ?
B3' B8' B12' B11' 0.20(15) . . . . ?
B4' C1' C2' B3' 38.59(10) . . . . ?
B4' C1' C2' B6' -104.69(11) . . . . ?
B4' C1' C2' B7' 0.20(14) . . . . ?
B4' C1' C2' B11' -67.03(13) . . . . ?
B4' C1' B3' C2' -138.65(10) . . . . ?
B4' C1' B3' B7' -102.86(11) . . . . ?
B4' C1' B3' B8' -39.66(10) . . . . ?
B4' C1' B5' B6' 140.52(11) . . . . ?
B4' C1' B5' B9' 39.60(10) . . . . ?
B4' C1' B5' B10' 102.01(11) . . . . ?
B4' C1' B6' C2' 102.11(11) . . . . ?
B4' C1' B6' B5' -37.49(11) . . . . ?
B4' C1' B6' B10' 2.40(14) . . . . ?
B4' C1' B6' B11' 66.37(13) . . . . ?
B4' B3' B7' C2' -97.04(11) . . . . ?
B4' B3' B7' B8' 38.12(10) . . . . ?
B4' B3' B7' B11' -62.64(13) . . . . ?
B4' B3' B7' B12' 0.79(14) . . . . ?
B4' B3' B8' B7' -137.89(11) . . . . ?
B4' B3' B8' B9' -37.29(10) . . . . ?
B4' B3' B8' B12' -100.69(12) . . . . ?
B4' B5' B6' C1' 34.61(9) . . . . ?
B4' B5' B6' C2' -0.63(14) . . . . ?
B4' B5' B6' B10' -100.95(12) . . . . ?
B4' B5' B6' B11' -63.49(13) . . . . ?
B4' B5' B9' B8' 37.29(10) . . . . ?
B4' B5' B9' B10' 138.14(11) . . . . ?
B4' B5' B9' B12' 100.88(12) . . . . ?
B4' B5' B10' B6' 99.72(11) . . . . ?
B4' B5' B10' B9' -37.32(10) . . . . ?
B4' B5' B10' B11' 63.19(13) . . . . ?
B4' B5' B10' B12' -0.20(14) . . . . ?
B4' B8' B9' B5' -37.32(10) . . . . ?
B4' B8' B9' B10' -100.88(11) . . . . ?
B4' B8' B9' B12' -138.37(11) . . . . ?
B4' B8' B12' B7' -100.88(11) . . . . ?
B4' B8' B12' B9' 37.06(10) . . . . ?
B4' B8' B12' B10' -0.23(14) . . . . ?
B4' B8' B12' B11' -63.36(14) . . . . ?
B4' B9' B10' B5' 37.51(10) . . . . ?
B4' B9' B10' B6' -0.51(15) . . . . ?
B4' B9' B10' B11' -63.61(14) . . . . ?
B4' B9' B10' B12' -100.99(12) . . . . ?
B4' B9' B12' B7' 0.20(15) . . . . ?
B4' B9' B12' B8' -37.30(10) . . . . ?
B4' B9' B12' B10' 100.88(12) . . . . ?
B4' B9' B12' B11' 63.62(14) . . . . ?
B5' C1' C2' B3' 105.78(11) . . . . ?
B5' C1' C2' B6' -37.50(10) . . . . ?
B5' C1' C2' B7' 67.39(13) . . . . ?
B5' C1' C2' B11' 0.16(14) . . . . ?
B5' C1' B3' C2' -101.68(11) . . . . ?
B5' C1' B3' B4' 36.97(10) . . . . ?
B5' C1' B3' B7' -65.88(13) . . . . ?
B5' C1' B3' B8' -2.69(14) . . . . ?
B5' C1' B4' B3' -141.36(11) . . . . ?
B5' C1' B4' B8' -102.50(11) . . . . ?
B5' C1' B4' B9' -39.83(10) . . . . ?
B5' C1' B6' C2' 139.60(11) . . . . ?
B5' C1' B6' B10' 39.89(11) . . . . ?
B5' C1' B6' B11' 103.87(12) . . . . ?
B5' B4' B8' B3' -100.80(11) . . . . ?
B5' B4' B8' B7' -63.11(13) . . . . ?
B5' B4' B8' B9' 37.30(10) . . . . ?
B5' B4' B8' B12' 0.11(14) . . . . ?
B5' B4' B9' B8' -138.40(11) . . . . ?
B5' B4' B9' B10' -37.47(11) . . . . ?
B5' B4' B9' B12' -101.12(12) . . . . ?
B5' B6' B10' B9' 38.08(11) . . . . ?
B5' B6' B10' B11' 139.18(11) . . . . ?
B5' B6' B10' B12' 101.19(11) . . . . ?
B5' B6' B11' C2' 98.35(11) . . . . ?
B5' B6' B11' B7' 63.62(13) . . . . ?
B5' B6' B11' B10' -37.55(10) . . . . ?
B5' B6' B11' B12' 0.60(14) . . . . ?
B5' B9' B10' B6' -38.02(10) . . . . ?
B5' B9' B10' B11' -101.11(11) . . . . ?
B5' B9' B10' B12' -138.50(11) . . . . ?
B5' B9' B12' B7' -63.47(14) . . . . ?
B5' B9' B12' B8' -100.97(11) . . . . ?
B5' B9' B12' B10' 37.21(10) . . . . ?
B5' B9' B12' B11' -0.05(14) . . . . ?
B5' B10' B11' C2' -1.80(14) . . . . ?
B5' B10' B11' B6' 36.47(10) . . . . ?
B5' B10' B11' B7' -63.29(14) . . . . ?
B5' B10' B11' B12' -100.74(12) . . . . ?
B5' B10' B12' B7' 63.55(13) . . . . ?
B5' B10' B12' B8' 0.26(14) . . . . ?
B5' B10' B12' B9' -37.08(10) . . . . ?
B5' B10' B12' B11' 101.01(11) . . . . ?
B6' C1' C2' B3' 143.28(11) . . . . ?
B6' C1' C2' B7' 104.89(12) . . . . ?
B6' C1' C2' B11' 37.66(10) . . . . ?
B6' C1' B3' C2' -34.36(10) . . . . ?
B6' C1' B3' B4' 104.29(11) . . . . ?
B6' C1' B3' B7' 1.43(14) . . . . ?
B6' C1' B3' B8' 64.63(13) . . . . ?
B6' C1' B4' B3' -104.21(11) . . . . ?
B6' C1' B4' B5' 37.16(10) . . . . ?
B6' C1' B4' B8' -65.35(13) . . . . ?
B6' C1' B4' B9' -2.67(14) . . . . ?
B6' C1' B5' B4' -140.52(11) . . . . ?
B6' C1' B5' B9' -100.92(11) . . . . ?
B6' C1' B5' B10' -38.51(10) . . . . ?
B6' C2' B3' C1' 34.25(10) . . . . ?
B6' C2' B3' B4' -1.59(14) . . . . ?
B6' C2' B3' B7' -104.49(12) . . . . ?
B6' C2' B3' B8' -64.81(13) . . . . ?
B6' C2' B7' B3' 103.85(12) . . . . ?
B6' C2' B7' B8' 64.87(13) . . . . ?
B6' C2' B7' B11' -37.31(11) . . . . ?
B6' C2' B7' B12' 2.11(14) . . . . ?
B6' C2' B11' B7' 140.44(11) . . . . ?
B6' C2' B11' B10' 38.33(10) . . . . ?
B6' C2' B11' B12' 101.14(12) . . . . ?
B6' B5' B9' B4' -100.46(11) . . . . ?
B6' B5' B9' B8' -63.17(13) . . . . ?
B6' B5' B9' B10' 37.68(10) . . . . ?
B6' B5' B9' B12' 0.42(14) . . . . ?
B6' B5' B10' B9' -137.03(11) . . . . ?
B6' B5' B10' B11' -36.53(10) . . . . ?
B6' B5' B10' B12' -99.91(12) . . . . ?
B6' B10' B11' C2' -38.27(10) . . . . ?
B6' B10' B11' B7' -99.76(11) . . . . ?
B6' B10' B11' B12' -137.21(11) . . . . ?
B6' B10' B12' B7' 0.52(14) . . . . ?
B6' B10' B12' B8' -62.76(13) . . . . ?
B6' B10' B12' B9' -100.11(11) . . . . ?
B6' B10' B12' B11' 37.99(10) . . . . ?
B6' B11' B12' B7' 100.44(11) . . . . ?
B6' B11' B12' B8' 63.00(14) . . . . ?
B6' B11' B12' B9' -0.33(14) . . . . ?
B6' B11' B12' B10' -37.64(10) . . . . ?
B7' C2' B3' C1' 138.74(11) . . . . ?
B7' C2' B3' B4' 102.90(11) . . . . ?
B7' C2' B3' B8' 39.68(10) . . . . ?
B7' C2' B6' C1' -101.79(12) . . . . ?
B7' C2' B6' B5' -66.03(13) . . . . ?
B7' C2' B6' B10' -1.81(14) . . . . ?
B7' C2' B6' B11' 37.65(11) . . . . ?
B7' C2' B11' B6' -140.44(11) . . . . ?
B7' C2' B11' B10' -102.10(12) . . . . ?
B7' C2' B11' B12' -39.29(11) . . . . ?
B7' B3' B4' C1' 97.11(11) . . . . ?
B7' B3' B4' B5' 62.77(13) . . . . ?
B7' B3' B4' B8' -38.10(10) . . . . ?
B7' B3' B4' B9' -0.67(14) . . . . ?
B7' B3' B8' B4' 137.89(11) . . . . ?
B7' B3' B8' B9' 100.59(11) . . . . ?
B7' B3' B8' B12' 37.20(11) . . . . ?
B7' B8' B9' B4' 100.93(11) . . . . ?
B7' B8' B9' B5' 63.60(13) . . . . ?
B7' B8' B9' B10' 0.04(14) . . . . ?
B7' B8' B9' B12' -37.44(10) . . . . ?
B7' B8' B12' B9' 137.94(11) . . . . ?
B7' B8' B12' B10' 100.65(12) . . . . ?
B7' B8' B12' B11' 37.52(11) . . . . ?
B7' B11' B12' B8' -37.44(11) . . . . ?
B7' B11' B12' B9' -100.77(12) . . . . ?
B7' B11' B12' B10' -138.08(11) . . . . ?
B8' B3' B4' C1' 135.21(11) . . . . ?
B8' B3' B4' B5' 100.88(11) . . . . ?
B8' B3' B4' B9' 37.44(10) . . . . ?
B8' B3' B7' C2' -135.16(11) . . . . ?
B8' B3' B7' B11' -100.76(12) . . . . ?
B8' B3' B7' B12' -37.33(11) . . . . ?
B8' B4' B5' C1' 97.16(11) . . . . ?
B8' B4' B5' B6' 62.40(13) . . . . ?
B8' B4' B5' B9' -37.37(10) . . . . ?
B8' B4' B5' B10' 0.05(14) . . . . ?
B8' B4' B9' B5' 138.40(11) . . . . ?
B8' B4' B9' B10' 100.94(12) . . . . ?
B8' B4' B9' B12' 37.28(10) . . . . ?
B8' B7' B11' C2' -97.40(11) . . . . ?
B8' B7' B11' B6' -62.49(13) . . . . ?
B8' B7' B11' B10' -0.01(14) . . . . ?
B8' B7' B11' B12' 37.64(10) . . . . ?
B8' B7' B12' B9' -37.53(10) . . . . ?
B8' B7' B12' B10' -100.74(12) . . . . ?
B8' B7' B12' B11' -138.05(12) . . . . ?
B8' B9' B10' B5' 101.06(11) . . . . ?
B8' B9' B10' B6' 63.04(14) . . . . ?
B8' B9' B10' B11' -0.05(14) . . . . ?
B8' B9' B10' B12' -37.43(10) . . . . ?
B8' B9' B12' B7' 37.50(10) . . . . ?
B8' B9' B12' B10' 138.18(11) . . . . ?
B8' B9' B12' B11' 100.92(12) . . . . ?
B9' B4' B5' C1' 134.53(11) . . . . ?
B9' B4' B5' B6' 99.78(12) . . . . ?
B9' B4' B5' B10' 37.43(10) . . . . ?
B9' B4' B8' B3' -138.09(11) . . . . ?
B9' B4' B8' B7' -100.41(12) . . . . ?
B9' B4' B8' B12' -37.19(10) . . . . ?
B9' B5' B6' C1' 97.46(11) . . . . ?
B9' B5' B6' C2' 62.22(13) . . . . ?
B9' B5' B6' B10' -38.10(10) . . . . ?
B9' B5' B6' B11' -0.63(14) . . . . ?
B9' B5' B10' B6' 137.03(11) . . . . ?
B9' B5' B10' B11' 100.51(12) . . . . ?
B9' B5' B10' B12' 37.12(10) . . . . ?
B9' B8' B12' B7' -137.94(11) . . . . ?
B9' B8' B12' B10' -37.29(10) . . . . ?
B9' B8' B12' B11' -100.43(12) . . . . ?
B9' B10' B11' C2' 61.53(13) . . . . ?
B9' B10' B11' B6' 99.79(11) . . . . ?
B9' B10' B11' B7' 0.03(14) . . . . ?
B9' B10' B11' B12' -37.42(10) . . . . ?
B9' B10' B12' B7' 100.63(11) . . . . ?
B9' B10' B12' B8' 37.34(10) . . . . ?
B9' B10' B12' B11' 138.09(11) . . . . ?
B10' B5' B6' C1' 135.56(11) . . . . ?
B10' B5' B6' C2' 100.32(12) . . . . ?
B10' B5' B6' B11' 37.46(10) . . . . ?
B10' B5' B9' B4' -138.14(11) . . . . ?
B10' B5' B9' B8' -100.84(12) . . . . ?
B10' B5' B9' B12' -37.26(10) . . . . ?
B10' B6' B11' C2' 135.90(11) . . . . ?
B10' B6' B11' B7' 101.16(12) . . . . ?
B10' B6' B11' B12' 38.15(10) . . . . ?
B10' B9' B12' B7' -100.68(12) . . . . ?
B10' B9' B12' B8' -138.18(11) . . . . ?
B10' B9' B12' B11' -37.26(10) . . . . ?
B10' B11' B12' B7' 138.08(11) . . . . ?
B10' B11' B12' B8' 100.64(12) . . . . ?
B10' B11' B12' B9' 37.31(10) . . . . ?
B11' C2' B3' C1' 101.58(12) . . . . ?
B11' C2' B3' B4' 65.74(13) . . . . ?
B11' C2' B3' B7' -37.16(11) . . . . ?
B11' C2' B3' B8' 2.52(15) . . . . ?
B11' C2' B6' C1' -139.44(11) . . . . ?
B11' C2' B6' B5' -103.68(11) . . . . ?
B11' C2' B6' B10' -39.47(10) . . . . ?
B11' C2' B7' B3' 141.17(11) . . . . ?
B11' C2' B7' B8' 102.18(12) . . . . ?
B11' C2' B7' B12' 39.42(10) . . . . ?
B11' B6' B10' B5' -139.18(11) . . . . ?
B11' B6' B10' B9' -101.10(12) . . . . ?
B11' B6' B10' B12' -38.00(10) . . . . ?
B11' B7' B8' B3' 100.76(12) . . . . ?
B11' B7' B8' B4' 63.05(13) . . . . ?
B11' B7' B8' B9' -0.02(14) . . . . ?
B11' B7' B8' B12' -37.54(11) . . . . ?
B11' B7' B12' B8' 138.05(12) . . . . ?
B11' B7' B12' B9' 100.53(12) . . . . ?
B11' B7' B12' B10' 37.31(10) . . . . ?
B11' B10' B12' B7' -37.46(10) . . . . ?
B11' B10' B12' B8' -100.75(12) . . . . ?
B11' B10' B12' B9' -138.09(11) . . . . ?
B12' B7' B8' B3' 138.30(12) . . . . ?
B12' B7' B8' B4' 100.59(12) . . . . ?
B12' B7' B8' B9' 37.52(10) . . . . ?
B12' B7' B11' C2' -135.05(11) . . . . ?
B12' B7' B11' B6' -100.14(12) . . . . ?
B12' B7' B11' B10' -37.65(10) . . . . ?
B12' B8' B9' B4' 138.37(11) . . . . ?
B12' B8' B9' B5' 101.05(12) . . . . ?
B12' B8' B9' B10' 37.49(10) . . . . ?
B12' B9' B10' B5' 138.50(11) . . . . ?
B12' B9' B10' B6' 100.48(12) . . . . ?
B12' B9' B10' B11' 37.38(10) . . . . ?
B12' B10' B11' C2' 98.94(11) . . . . ?
B12' B10' B11' B6' 137.21(11) . . . . ?
B12' B10' B11' B7' 37.45(10) . . . . ?

