 
data_1 
 
_audit_creation_method            SHELXL-97 
_chemical_name_systematic 
; 
 ? 
; 
_chemical_name_common             K4MgW3O12 
_chemical_melting_point           ? 
_chemical_formula_moiety          ? 
_chemical_formula_sum 
 'K4 Mg O12 W3' 
_chemical_formula_weight          924.26 
 
loop_ 
 _atom_type_symbol 
 _atom_type_description 
 _atom_type_scat_dispersion_real 
 _atom_type_scat_dispersion_imag 
 _atom_type_scat_source 
 'K'  'K'   0.2009   0.2494 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Mg'  'Mg'   0.0486   0.0363 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'O'  'O'   0.0106   0.0060 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'W'  'W'  -0.8490   6.8722 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 
_symmetry_cell_setting            Triclinic 
_symmetry_space_group_name_H-M    P-1 
 
loop_ 
 _symmetry_equiv_pos_as_xyz 
 'x, y, z' 
 '-x, -y, -z' 
 
_cell_length_a                    7.7255(14) 
_cell_length_b                    9.9119(19) 
_cell_length_c                    10.0401(18) 
_cell_angle_alpha                 93.249(10) 
_cell_angle_beta                  106.624(10) 
_cell_angle_gamma                 105.781(11) 
_cell_volume                      701.3(2) 
_cell_formula_units_Z             2 
_cell_measurement_temperature     293(2) 
_cell_measurement_reflns_used     4673 
_cell_measurement_theta_min       2.16 
_cell_measurement_theta_max       27.55 
 
_exptl_crystal_description        block 
_exptl_crystal_colour             colorless 
_exptl_crystal_size_max           0.195 
_exptl_crystal_size_mid           0.071 
_exptl_crystal_size_min           0.063 
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_diffrn     4.377 
_exptl_crystal_density_method     'not measured' 
_exptl_crystal_F_000              812 
_exptl_absorpt_coefficient_mu     25.824 
_exptl_absorpt_correction_type    'numerical'
_exptl_absorpt_correction_T_min   0.16343 
_exptl_absorpt_correction_T_max   0.36439 
_exptl_absorpt_process_details    "Face-indexed" 
 
_exptl_special_details 
; 
 ? 
; 
 
_diffrn_ambient_temperature       293(2) 
_diffrn_radiation_wavelength      0.71073 
_diffrn_radiation_type            MoK\a 
_diffrn_radiation_source          'fine-focus sealed tube' 
_diffrn_radiation_monochromator   graphite 
_diffrn_measurement_device_type   'CCD area detector' 
_diffrn_measurement_method        'phi and omega scans' 
_diffrn_detector_area_resol_mean  ? 
_diffrn_standards_number          ? 
_diffrn_standards_interval_count  ? 
_diffrn_standards_interval_time   ? 
_diffrn_standards_decay_%         ? 
_diffrn_reflns_number             13490 
_diffrn_reflns_av_R_equivalents   0.0405 
_diffrn_reflns_av_sigmaI/netI     0.0409 
_diffrn_reflns_limit_h_min        -10 
_diffrn_reflns_limit_h_max        10 
_diffrn_reflns_limit_k_min        -12 
_diffrn_reflns_limit_k_max        11 
_diffrn_reflns_limit_l_min        -13 
_diffrn_reflns_limit_l_max        12 
_diffrn_reflns_theta_min          2.14 
_diffrn_reflns_theta_max          27.59 
_reflns_number_total              3192 
_reflns_number_gt                 2662 
_reflns_threshold_expression      >2sigma(I) 
 
_computing_data_collection        'Bruker SMART' 
_computing_cell_refinement        'Bruker SMART' 
_computing_data_reduction         'Bruker SAINT' 
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)' 
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)' 
_computing_molecular_graphics     'Bruker SHELXTL' 
_computing_publication_material   'Bruker SHELXTL' 
 
_refine_special_details 
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
; 
 
_refine_ls_structure_factor_coef  Fsqd  
_refine_ls_matrix_type            full 
_refine_ls_weighting_scheme       calc  
_refine_ls_weighting_details 
 'calc w=1/[σ²(Fo²)+(0.0233P)²+4.0465P] where P=(Fo²+2Fc²)/3' 
_atom_sites_solution_primary      direct 
_atom_sites_solution_secondary    difmap 
_atom_sites_solution_hydrogens    ? 
_refine_ls_hydrogen_treatment     ? 
_refine_ls_extinction_method      SHELXL 
_refine_ls_extinction_coef        0.00114(11) 
_refine_ls_extinction_expression 
 'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^' 
_refine_ls_number_reflns          3192 
_refine_ls_number_parameters      125 
_refine_ls_number_restraints      0 
_refine_ls_R_factor_all           0.0411 
_refine_ls_R_factor_gt            0.0303 
_refine_ls_wR_factor_ref          0.0658 
_refine_ls_wR_factor_gt           0.0619 
_refine_ls_goodness_of_fit_ref    1.089 
_refine_ls_restrained_S_all       1.089 
_refine_ls_shift/su_max           0.000 
_refine_ls_shift/su_mean          0.000 
 
loop_ 
 _atom_site_label 
 _atom_site_type_symbol 
 _atom_site_fract_x 
 _atom_site_fract_y 
 _atom_site_fract_z 
 _atom_site_U_iso_or_equiv 
 _atom_site_adp_type 
 _atom_site_occupancy 
 _atom_site_symmetry_multiplicity 
 _atom_site_calc_flag 
 _atom_site_refinement_flags 
 _atom_site_disorder_assembly 
 _atom_site_disorder_group 
W1 W 0.87816(4) 0.35632(4) 0.18603(3) 0.01914(11) Uani 1 1 d . . . 
W2 W 0.76250(5) -0.18861(4) 0.25581(3) 0.01976(11) Uani 1 1 d . . . 
W3 W 0.38113(5) 0.14969(4) 0.38866(4) 0.02706(11) Uani 1 1 d . . . 
K1 K 0.3513(3) 0.4325(2) 0.1129(2) 0.0274(4) Uani 1 1 d . . . 
K2 K 0.0000 0.0000 0.0000 0.0320(7) Uani 1 2 d S . . 
K3 K 0.2204(3) 0.7615(2) 0.22388(19) 0.0242(4) Uani 1 1 d . . . 
K4 K 0.2551(3) 0.4792(2) 0.5264(2) 0.0345(5) Uani 1 1 d . . . 
K5 K 0.5000 0.0000 0.0000 0.0385(7) Uani 1 2 d S . . 
Mg1 Mg 0.8431(5) 0.1219(3) 0.4479(3) 0.0365(8) Uani 1 1 d . . . 
O1 O 0.7566(8) -0.0090(6) 0.2683(6) 0.0266(13) Uiso 1 1 d . . . 
O2 O 0.5538(9) -0.3080(7) 0.2680(6) 0.0319(15) Uiso 1 1 d . . . 
O3 O 0.3890(8) 0.3248(7) 0.3676(6) 0.0315(14) Uiso 1 1 d . . . 
O4 O 1.0921(9) 0.4880(7) 0.2096(7) 0.0361(16) Uiso 1 1 d . . . 
O5 O 0.9645(8) -0.2212(7) 0.3715(6) 0.0300(14) Uiso 1 1 d . . . 
O6 O 0.6114(9) 0.1502(7) 0.4916(7) 0.0375(16) Uiso 1 1 d . . . 
O7 O 0.8871(10) 0.3000(8) 0.3531(7) 0.0432(17) Uiso 1 1 d . . . 
O8 O 0.8443(9) 0.2162(8) 0.0563(7) 0.0417(17) Uiso 1 1 d . . . 
O9 O 0.3216(9) 0.0525(7) 0.2217(6) 0.0331(15) Uiso 1 1 d . . . 
O10 O 0.8017(10) -0.0750(8) 0.5337(8) 0.0479(19) Uiso 1 1 d . . . 
O11 O 0.7760(10) -0.2189(8) 0.0869(8) 0.0490(19) Uiso 1 1 d . . . 
O12 O 0.6964(11) 0.4346(9) 0.1355(8) 0.052(2) Uiso 1 1 d . . . 
 
 
_geom_special_details 
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
; 
 
loop_ 
 _geom_bond_atom_site_label_1 
 _geom_bond_atom_site_label_2 
 _geom_bond_distance 
 _geom_bond_site_symmetry_2 
 _geom_bond_publ_flag 
W1 O4 1.749(7) . ? 
W1 O12 1.750(7) . ? 
W1 O8 1.759(7) . ? 
W1 O7 1.786(7) . ? 
W1 K4 3.681(2) 1_655 ? 
W1 K4 3.759(2) 2_666 ? 
W1 K1 3.8165(19) 1_655 ? 
W1 K5 3.8749(9) . ? 
W1 K3 4.0074(19) 2_665 ? 
W1 K1 4.027(2) 2_665 ? 
W1 K3 4.091(2) 1_655 ? 
W2 O11 1.743(7) . ? 
W2 O2 1.762(6) . ? 
W2 O5 1.779(6) . ? 
W2 O1 1.792(6) . ? 
W2 Mg1 3.343(3) . ? 
W2 K4 3.710(2) 2_656 ? 
W2 K5 3.7189(7) . ? 
W2 K3 3.8004(19) 1_645 ? 
W2 K2 3.8514(6) 1_655 ? 
W2 K3 3.997(2) 1_545 ? 
W2 K1 4.036(2) 2_655 ? 
W2 K1 4.068(2) 1_545 ? 
W3 O3 1.747(6) . ? 
W3 O9 1.756(6) . ? 
W3 O6 1.782(6) . ? 
W3 O10 1.811(7) 2_656 ? 
W3 K3 3.820(2) 1_545 ? 
W3 K4 3.848(2) 2_666 ? 
W3 K4 3.939(2) . ? 
W3 K1 4.055(2) . ? 
W3 K2 4.0609(9) . ? 
W3 K3 4.083(2) 2_666 ? 
K1 O11 2.594(8) 2_655 ? 
K1 O12 2.605(8) . ? 
K1 O4 2.628(6) 1_455 ? 
K1 O2 2.730(7) 1_565 ? 
K1 O3 2.796(7) . ? 
K1 O12 2.864(8) 2_665 ? 
K1 K1 3.724(4) 2_665 ? 
K1 W1 3.8165(19) 1_455 ? 
K1 K3 3.863(3) . ? 
K1 K4 3.875(3) 2_666 ? 
K1 W1 4.027(2) 2_665 ? 
K1 W2 4.036(2) 2_655 ? 
K2 O9 2.720(6) 2 ? 
K2 O9 2.720(6) . ? 
K2 O11 2.738(8) 2_655 ? 
K2 O11 2.738(8) 1_455 ? 
K2 O8 2.831(7) 1_455 ? 
K2 O8 2.831(7) 2_655 ? 
K2 K3 3.761(2) 2_565 ? 
K2 K3 3.761(2) 1_545 ? 
K2 W2 3.8514(6) 2_655 ? 
K2 W2 3.8514(6) 1_455 ? 
K2 K5 3.8627(7) 1_455 ? 
K2 K5 3.8628(7) . ? 
K3 O4 2.601(7) 1_455 ? 
K3 O8 2.745(7) 2_665 ? 
K3 O6 2.755(7) 2_666 ? 
K3 O2 2.766(6) 1_565 ? 
K3 O9 2.779(7) 1_565 ? 
K3 O5 2.822(6) 1_465 ? 
K3 O11 3.377(7) 1_465 ? 
K3 Mg1 3.638(3) 2_666 ? 
K3 K2 3.761(2) 1_565 ? 
K3 W2 3.8004(19) 1_465 ? 
K3 W3 3.820(2) 1_565 ? 
K4 O3 2.735(6) . ? 
K4 O3 2.766(7) 2_666 ? 
K4 O7 2.888(7) 1_455 ? 
K4 O7 3.037(7) 2_666 ? 
K4 O2 3.055(7) 2_656 ? 
K4 O5 3.066(7) 2_656 ? 
K4 O4 3.084(7) 1_455 ? 
K4 O12 3.341(8) 2_666 ? 
K4 W1 3.681(2) 1_455 ? 
K4 W2 3.710(2) 2_656 ? 
K4 W1 3.759(2) 2_666 ? 
K4 W3 3.848(2) 2_666 ? 
K5 O8 2.809(7) . ? 
K5 O8 2.809(7) 2_655 ? 
K5 O1 2.874(6) 2_655 ? 
K5 O1 2.874(6) . ? 
K5 O9 3.023(6) . ? 
K5 O9 3.023(6) 2_655 ? 
K5 O11 3.418(7) 2_655 ? 
K5 O11 3.418(7) . ? 
K5 W2 3.7189(6) 2_655 ? 
K5 K2 3.8628(7) 1_655 ? 
Mg1 O5 1.982(7) 2_756 ? 
Mg1 O1 1.989(6) . ? 
Mg1 O6 2.046(7) . ? 
Mg1 O7 2.047(8) . ? 
Mg1 O10 2.159(8) . ? 
Mg1 K3 3.638(3) 2_666 ? 
Mg1 K4 3.926(4) 1_655 ? 
Mg1 K4 4.231(4) 2_666 ? 
O2 K1 2.730(7) 1_545 ? 
O2 K3 2.766(6) 1_545 ? 
O2 K4 3.055(7) 2_656 ? 
O3 K4 2.766(7) 2_666 ? 
O4 K3 2.601(7) 1_655 ? 
O4 K1 2.628(6) 1_655 ? 
O4 K4 3.084(7) 1_655 ? 
O5 Mg1 1.982(7) 2_756 ? 
O5 K3 2.822(6) 1_645 ? 
O5 K4 3.066(7) 2_656 ? 
O6 K3 2.755(7) 2_666 ? 
O7 K4 2.888(7) 1_655 ? 
O7 K4 3.037(7) 2_666 ? 
O8 K3 2.745(7) 2_665 ? 
O8 K2 2.831(7) 1_655 ? 
O9 K3 2.779(7) 1_545 ? 
O10 W3 1.811(7) 2_656 ? 
O11 K1 2.594(8) 2_655 ? 
O11 K2 2.738(8) 1_655 ? 
O11 K3 3.377(7) 1_645 ? 
O12 K1 2.864(8) 2_665 ? 
O12 K4 3.341(8) 2_666 ? 
 
loop_ 
 _geom_angle_atom_site_label_1 
 _geom_angle_atom_site_label_2 
 _geom_angle_atom_site_label_3 
 _geom_angle 
 _geom_angle_site_symmetry_1 
 _geom_angle_site_symmetry_3 
 _geom_angle_publ_flag 
O4 W1 O12 107.4(3) . . ? 
O4 W1 O8 110.7(3) . . ? 
O12 W1 O8 110.3(3) . . ? 
O4 W1 O7 106.9(3) . . ? 
O12 W1 O7 108.9(3) . . ? 
O8 W1 O7 112.5(3) . . ? 
O4 W1 K4 56.6(2) . 1_655 ? 
O12 W1 K4 121.3(3) . 1_655 ? 
O8 W1 K4 128.4(2) . 1_655 ? 
O7 W1 K4 50.3(2) . 1_655 ? 
O4 W1 K4 96.9(2) . 2_666 ? 
O12 W1 K4 62.7(2) . 2_666 ? 
O8 W1 K4 152.1(2) . 2_666 ? 
O7 W1 K4 52.9(2) . 2_666 ? 
K4 W1 K4 64.35(5) 1_655 2_666 ? 
O4 W1 K1 36.6(2) . 1_655 ? 
O12 W1 K1 130.9(3) . 1_655 ? 
O8 W1 K1 75.4(2) . 1_655 ? 
O7 W1 K1 113.3(2) . 1_655 ? 
K4 W1 K1 72.65(4) 1_655 1_655 ? 
K4 W1 K1 130.68(4) 2_666 1_655 ? 
O4 W1 K5 152.1(2) . . ? 
O12 W1 K5 86.8(3) . . ? 
O8 W1 K5 41.4(2) . . ? 
O7 W1 K5 90.2(2) . . ? 
K4 W1 K5 135.67(4) 1_655 . ? 
K4 W1 K5 111.01(4) 2_666 . ? 
K1 W1 K5 116.46(3) 1_655 . ? 
O4 W1 K3 95.2(2) . 2_665 ? 
O12 W1 K3 87.2(2) . 2_665 ? 
O8 W1 K3 34.5(2) . 2_665 ? 
O7 W1 K3 146.5(2) . 2_665 ? 
K4 W1 K3 143.41(4) 1_655 2_665 ? 
K4 W1 K3 149.67(4) 2_666 2_665 ? 
K1 W1 K3 71.13(4) 1_655 2_665 ? 
K5 W1 K3 60.78(3) . 2_665 ? 
O4 W1 K1 85.8(2) . 2_665 ? 
O12 W1 K1 38.2(2) . 2_665 ? 
O8 W1 K1 90.2(2) . 2_665 ? 
O7 W1 K1 146.8(2) . 2_665 ? 
K4 W1 K1 131.93(5) 1_655 2_665 ? 
K4 W1 K1 95.84(4) 2_666 2_665 ? 
K1 W1 K1 95.34(4) 1_655 2_665 ? 
K5 W1 K1 91.78(3) . 2_665 ? 
K3 W1 K1 57.48(4) 2_665 2_665 ? 
O4 W1 K3 24.4(2) . 1_655 ? 
O12 W1 K3 83.4(3) . 1_655 ? 
O8 W1 K3 125.1(2) . 1_655 ? 
O7 W1 K3 112.0(2) . 1_655 ? 
K4 W1 K3 65.99(5) 1_655 1_655 ? 
K4 W1 K3 82.11(4) 2_666 1_655 ? 
K1 W1 K3 58.37(4) 1_655 1_655 ? 
K5 W1 K3 157.58(3) . 1_655 ? 
K3 W1 K3 98.55(4) 2_665 1_655 ? 
K1 W1 K3 68.22(4) 2_665 1_655 ? 
O11 W2 O2 109.3(3) . . ? 
O11 W2 O5 106.1(3) . . ? 
O2 W2 O5 109.9(3) . . ? 
O11 W2 O1 102.2(3) . . ? 
O2 W2 O1 112.3(3) . . ? 
O5 W2 O1 116.4(3) . . ? 
O11 W2 Mg1 128.1(3) . . ? 
O2 W2 Mg1 108.6(2) . . ? 
O5 W2 Mg1 92.6(2) . . ? 
O1 W2 Mg1 29.44(19) . . ? 
O11 W2 K4 119.2(3) . 2_656 ? 
O2 W2 K4 54.8(2) . 2_656 ? 
O5 W2 K4 55.2(2) . 2_656 ? 
O1 W2 K4 138.57(19) . 2_656 ? 
Mg1 W2 K4 111.33(6) . 2_656 ? 
O11 W2 K5 66.4(2) . . ? 
O2 W2 K5 93.4(2) . . ? 
O5 W2 K5 156.5(2) . . ? 
O1 W2 K5 48.80(19) . . ? 
Mg1 W2 K5 77.27(6) . . ? 
K4 W2 K5 148.19(3) 2_656 . ? 
O11 W2 K3 62.7(2) . 1_645 ? 
O2 W2 K3 132.5(2) . 1_645 ? 
O5 W2 K3 44.52(19) . 1_645 ? 
O1 W2 K3 115.19(18) . 1_645 ? 
Mg1 W2 K3 111.23(7) . 1_645 ? 
K4 W2 K3 86.83(4) 2_656 1_645 ? 
K5 W2 K3 119.55(3) . 1_645 ? 
O11 W2 K2 39.4(3) . 1_655 ? 
O2 W2 K2 144.3(2) . 1_655 ? 
O5 W2 K2 98.3(2) . 1_655 ? 
O1 W2 K2 71.38(18) . 1_655 ? 
Mg1 W2 K2 90.98(6) . 1_655 ? 
K4 W2 K2 144.56(3) 2_656 1_655 ? 
K5 W2 K2 61.332(13) . 1_655 ? 
K3 W2 K2 58.87(3) 1_645 1_655 ? 
O11 W2 K3 108.0(2) . 1_545 ? 
O2 W2 K3 35.8(2) . 1_545 ? 
O5 W2 K3 138.7(2) . 1_545 ? 
O1 W2 K3 78.12(18) . 1_545 ? 
Mg1 W2 K3 84.33(7) . 1_545 ? 
K4 W2 K3 87.64(4) 2_656 1_545 ? 
K5 W2 K3 62.14(3) . 1_545 ? 
K3 W2 K3 164.43(6) 1_645 1_545 ? 
K2 W2 K3 122.88(3) 1_655 1_545 ? 
O11 W2 K1 26.5(3) . 2_655 ? 
O2 W2 K1 85.4(2) . 2_655 ? 
O5 W2 K1 105.39(19) . 2_655 ? 
O1 W2 K1 123.19(19) . 2_655 ? 
Mg1 W2 K1 152.12(6) . 2_655 ? 
K4 W2 K1 96.48(5) 2_656 2_655 ? 
K5 W2 K1 77.95(3) . 2_655 ? 
K3 W2 K1 70.98(4) 1_645 2_655 ? 
K2 W2 K1 65.82(3) 1_655 2_655 ? 
K3 W2 K1 95.23(4) 1_545 2_655 ? 
O11 W2 K1 80.3(3) . 1_545 ? 
O2 W2 K1 31.7(2) . 1_545 ? 
O5 W2 K1 107.5(2) . 1_545 ? 
O1 W2 K1 132.92(18) . 1_545 ? 
Mg1 W2 K1 139.49(7) . 1_545 ? 
K4 W2 K1 59.55(4) 2_656 1_545 ? 
K5 W2 K1 93.45(3) . 1_545 ? 
K3 W2 K1 107.63(4) 1_645 1_545 ? 
K2 W2 K1 119.24(3) 1_655 1_545 ? 
K3 W2 K1 57.24(4) 1_545 1_545 ? 
K1 W2 K1 54.71(5) 2_655 1_545 ? 
O3 W3 O9 108.2(3) . . ? 
O3 W3 O6 107.8(3) . . ? 
O9 W3 O6 109.5(3) . . ? 
O3 W3 O10 109.2(3) . 2_656 ? 
O9 W3 O10 108.5(3) . 2_656 ? 
O6 W3 O10 113.5(3) . 2_656 ? 
O3 W3 K3 148.4(2) . 1_545 ? 
O9 W3 K3 42.1(2) . 1_545 ? 
O6 W3 K3 95.4(2) . 1_545 ? 
O10 W3 K3 79.2(2) 2_656 1_545 ? 
O3 W3 K4 40.6(2) . 2_666 ? 
O9 W3 K4 118.4(2) . 2_666 ? 
O6 W3 K4 67.4(2) . 2_666 ? 
O10 W3 K4 129.8(2) 2_656 2_666 ? 
K3 W3 K4 149.84(4) 1_545 2_666 ? 
O3 W3 K4 36.33(19) . . ? 
O9 W3 K4 133.5(2) . . ? 
O6 W3 K4 110.6(2) . . ? 
O10 W3 K4 75.5(2) 2_656 . ? 
K3 W3 K4 149.20(4) 1_545 . ? 
K4 W3 K4 59.84(5) 2_666 . ? 
O3 W3 K1 34.5(2) . . ? 
O9 W3 K1 73.9(2) . . ? 
O6 W3 K1 117.2(2) . . ? 
O10 W3 K1 124.7(2) 2_656 . ? 
K3 W3 K1 115.42(4) 1_545 . ? 
K4 W3 K1 58.67(4) 2_666 . ? 
K4 W3 K1 67.51(4) . . ? 
O3 W3 K2 92.1(2) . . ? 
O9 W3 K2 31.38(19) . . ? 
O6 W3 K2 140.9(2) . . ? 
O10 W3 K2 89.7(2) 2_656 . ? 
K3 W3 K2 56.91(3) 1_545 . ? 
K4 W3 K2 121.82(4) 2_666 . ? 
K4 W3 K2 105.36(3) . . ? 
K1 W3 K2 63.79(3) . . ? 
O3 W3 K3 96.7(2) . 2_666 ? 
O9 W3 K3 141.2(2) . 2_666 ? 
O6 W3 K3 32.6(2) . 2_666 ? 
O10 W3 K3 90.0(2) 2_656 2_666 ? 
K3 W3 K3 114.06(3) 1_545 2_666 ? 
K4 W3 K3 64.67(4) 2_666 2_666 ? 
K4 W3 K3 83.45(4) . 2_666 ? 
K1 W3 K3 123.30(4) . 2_666 ? 
K2 W3 K3 170.81(3) . 2_666 ? 
O11 K1 O12 89.6(2) 2_655 . ? 
O11 K1 O4 114.7(2) 2_655 1_455 ? 
O12 K1 O4 153.3(2) . 1_455 ? 
O11 K1 O2 161.2(2) 2_655 1_565 ? 
O12 K1 O2 78.8(2) . 1_565 ? 
O4 K1 O2 80.1(2) 1_455 1_565 ? 
O11 K1 O3 107.7(2) 2_655 . ? 
O12 K1 O3 88.8(2) . . ? 
O4 K1 O3 73.79(19) 1_455 . ? 
O2 K1 O3 87.06(19) 1_565 . ? 
O11 K1 O12 77.1(2) 2_655 2_665 ? 
O12 K1 O12 94.3(2) . 2_665 ? 
O4 K1 O12 101.5(2) 1_455 2_665 ? 
O2 K1 O12 88.9(2) 1_565 2_665 ? 
O3 K1 O12 174.3(2) . 2_665 ? 
O11 K1 K1 79.90(17) 2_655 2_665 ? 
O12 K1 K1 50.09(18) . 2_665 ? 
O4 K1 K1 141.14(18) 1_455 2_665 ? 
O2 K1 K1 81.31(15) 1_565 2_665 ? 
O3 K1 K1 138.70(15) . 2_665 ? 
O12 K1 K1 44.23(15) 2_665 2_665 ? 
O11 K1 W1 92.75(17) 2_655 1_455 ? 
O12 K1 W1 159.99(19) . 1_455 ? 
O4 K1 W1 23.37(15) 1_455 1_455 ? 
O2 K1 W1 103.20(13) 1_565 1_455 ? 
O3 K1 W1 71.51(13) . 1_455 ? 
O12 K1 W1 105.59(16) 2_665 1_455 ? 
K1 K1 W1 149.76(9) 2_665 1_455 ? 
O11 K1 K3 139.47(17) 2_655 . ? 
O12 K1 K3 123.54(19) . . ? 
O4 K1 K3 42.09(16) 1_455 . ? 
O2 K1 K3 45.73(13) 1_565 . ? 
O3 K1 K3 96.56(13) . . ? 
O12 K1 K3 77.73(16) 2_665 . ? 
K1 K1 K3 102.88(8) 2_665 . ? 
W1 K1 K3 64.37(4) 1_455 . ? 
O11 K1 K4 132.75(18) 2_655 2_666 ? 
O12 K1 K4 58.18(17) . 2_666 ? 
O4 K1 K4 95.65(15) 1_455 2_666 ? 
O2 K1 K4 51.62(14) 1_565 2_666 ? 
O3 K1 K4 45.52(14) . 2_666 ? 
O12 K1 K4 133.18(17) 2_665 2_666 ? 
K1 K1 K4 99.07(8) 2_665 2_666 ? 
W1 K1 K4 107.13(5) 1_455 2_666 ? 
K3 K1 K4 87.27(6) . 2_666 ? 
O11 K1 W1 85.14(18) 2_655 2_665 ? 
O12 K1 W1 115.34(18) . 2_665 ? 
O4 K1 W1 79.41(15) 1_455 2_665 ? 
O2 K1 W1 86.49(14) 1_565 2_665 ? 
O3 K1 W1 153.13(13) . 2_665 ? 
O12 K1 W1 22.19(15) 2_665 2_665 ? 
K1 K1 W1 65.61(6) 2_665 2_665 ? 
W1 K1 W1 84.66(4) 1_455 2_665 ? 
K3 K1 W1 61.00(4) . 2_665 ? 
K4 K1 W1 137.83(7) 2_666 2_665 ? 
O11 K1 W2 17.43(17) 2_655 2_655 ? 
O12 K1 W2 82.14(17) . 2_655 ? 
O4 K1 W2 124.30(16) 1_455 2_655 ? 
O2 K1 W2 143.99(15) 1_565 2_655 ? 
O3 K1 W2 122.92(14) . 2_655 ? 
O12 K1 W2 62.36(16) 2_665 2_655 ? 
K1 K1 W2 63.09(5) 2_665 2_655 ? 
W1 K1 W2 105.09(5) 1_455 2_655 ? 
K3 K1 W2 134.65(6) . 2_655 ? 
K4 K1 W2 135.61(6) 2_666 2_655 ? 
W1 K1 W2 74.51(4) 2_665 2_655 ? 
O9 K2 O9 180.0(2) 2 . ? 
O9 K2 O11 98.1(2) 2 2_655 ? 
O9 K2 O11 81.9(2) . 2_655 ? 
O9 K2 O11 81.9(2) 2 1_455 ? 
O9 K2 O11 98.1(2) . 1_455 ? 
O11 K2 O11 180.0(3) 2_655 1_455 ? 
O9 K2 O8 76.36(19) 2 1_455 ? 
O9 K2 O8 103.64(19) . 1_455 ? 
O11 K2 O8 80.9(2) 2_655 1_455 ? 
O11 K2 O8 99.1(2) 1_455 1_455 ? 
O9 K2 O8 103.64(19) 2 2_655 ? 
O9 K2 O8 76.36(19) . 2_655 ? 
O11 K2 O8 99.1(2) 2_655 2_655 ? 
O11 K2 O8 80.9(2) 1_455 2_655 ? 
O8 K2 O8 180.0(4) 1_455 2_655 ? 
O9 K2 K3 47.52(14) 2 2_565 ? 
O9 K2 K3 132.48(14) . 2_565 ? 
O11 K2 K3 60.21(15) 2_655 2_565 ? 
O11 K2 K3 119.79(15) 1_455 2_565 ? 
O8 K2 K3 46.64(14) 1_455 2_565 ? 
O8 K2 K3 133.36(14) 2_655 2_565 ? 
O9 K2 K3 132.48(14) 2 1_545 ? 
O9 K2 K3 47.52(14) . 1_545 ? 
O11 K2 K3 119.79(15) 2_655 1_545 ? 
O11 K2 K3 60.21(15) 1_455 1_545 ? 
O8 K2 K3 133.36(14) 1_455 1_545 ? 
O8 K2 K3 46.64(14) 2_655 1_545 ? 
K3 K2 K3 180.0 2_565 1_545 ? 
O9 K2 W2 83.37(13) 2 2_655 ? 
O9 K2 W2 96.63(13) . 2_655 ? 
O11 K2 W2 23.84(15) 2_655 2_655 ? 
O11 K2 W2 156.16(15) 1_455 2_655 ? 
O8 K2 W2 95.46(14) 1_455 2_655 ? 
O8 K2 W2 84.54(14) 2_655 2_655 ? 
K3 K2 W2 59.89(3) 2_565 2_655 ? 
K3 K2 W2 120.11(3) 1_545 2_655 ? 
O9 K2 W2 96.63(13) 2 1_455 ? 
O9 K2 W2 83.37(13) . 1_455 ? 
O11 K2 W2 156.16(15) 2_655 1_455 ? 
O11 K2 W2 23.84(15) 1_455 1_455 ? 
O8 K2 W2 84.54(14) 1_455 1_455 ? 
O8 K2 W2 95.46(14) 2_655 1_455 ? 
K3 K2 W2 120.11(3) 2_565 1_455 ? 
K3 K2 W2 59.89(3) 1_545 1_455 ? 
W2 K2 W2 180.0 2_655 1_455 ? 
O9 K2 K5 51.15(12) 2 1_455 ? 
O9 K2 K5 128.85(12) . 1_455 ? 
O11 K2 K5 120.51(15) 2_655 1_455 ? 
O11 K2 K5 59.49(15) 1_455 1_455 ? 
O8 K2 K5 46.53(14) 1_455 1_455 ? 
O8 K2 K5 133.47(14) 2_655 1_455 ? 
K3 K2 K5 63.08(3) 2_565 1_455 ? 
K3 K2 K5 116.92(3) 1_545 1_455 ? 
W2 K2 K5 122.356(10) 2_655 1_455 ? 
W2 K2 K5 57.644(10) 1_455 1_455 ? 
O9 K2 K5 128.85(12) 2 . ? 
O9 K2 K5 51.15(12) . . ? 
O11 K2 K5 59.49(15) 2_655 . ? 
O11 K2 K5 120.51(15) 1_455 . ? 
O8 K2 K5 133.47(14) 1_455 . ? 
O8 K2 K5 46.53(14) 2_655 . ? 
K3 K2 K5 116.92(3) 2_565 . ? 
K3 K2 K5 63.08(3) 1_545 . ? 
W2 K2 K5 57.644(11) 2_655 . ? 
W2 K2 K5 122.356(10) 1_455 . ? 
K5 K2 K5 180.0 1_455 . ? 
O4 K3 O8 100.1(2) 1_455 2_665 ? 
O4 K3 O6 102.6(2) 1_455 2_666 ? 
O8 K3 O6 155.7(2) 2_665 2_666 ? 
O4 K3 O2 79.9(2) 1_455 1_565 ? 
O8 K3 O2 96.90(19) 2_665 1_565 ? 
O6 K3 O2 78.94(19) 2_666 1_565 ? 
O4 K3 O9 174.2(2) 1_455 1_565 ? 
O8 K3 O9 76.8(2) 2_665 1_565 ? 
O6 K3 O9 81.2(2) 2_666 1_565 ? 
O2 K3 O9 105.18(19) 1_565 1_565 ? 
O4 K3 O5 86.6(2) 1_455 1_465 ? 
O8 K3 O5 124.3(2) 2_665 1_465 ? 
O6 K3 O5 65.81(18) 2_666 1_465 ? 
O2 K3 O5 138.34(19) 1_565 1_465 ? 
O9 K3 O5 91.12(18) 1_565 1_465 ? 
O4 K3 O11 91.0(2) 1_455 1_465 ? 
O8 K3 O11 71.46(19) 2_665 1_465 ? 
O6 K3 O11 116.28(19) 2_666 1_465 ? 
O2 K3 O11 163.88(19) 1_565 1_465 ? 
O9 K3 O11 83.44(19) 1_565 1_465 ? 
O5 K3 O11 53.11(18) 1_465 1_465 ? 
O4 K3 Mg1 100.61(16) 1_455 2_666 ? 
O8 K3 Mg1 146.86(16) 2_665 2_666 ? 
O6 K3 Mg1 33.88(14) 2_666 2_666 ? 
O2 K3 Mg1 111.98(15) 1_565 2_666 ? 
O9 K3 Mg1 80.09(14) 1_565 2_666 ? 
O5 K3 Mg1 32.74(14) 1_465 2_666 ? 
O11 K3 Mg1 82.63(14) 1_465 2_666 ? 
O4 K3 K2 128.21(15) 1_455 1_565 ? 
O8 K3 K2 48.57(14) 2_665 1_565 ? 
O6 K3 K2 119.11(15) 2_666 1_565 ? 
O2 K3 K2 134.25(14) 1_565 1_565 ? 
O9 K3 K2 46.19(13) 1_565 1_565 ? 
O5 K3 K2 84.23(13) 1_465 1_565 ? 
O11 K3 K2 44.71(13) 1_465 1_565 ? 
Mg1 K3 K2 98.38(7) 2_666 1_565 ? 
O4 K3 W2 92.08(14) 1_455 1_465 ? 
O8 K3 W2 98.11(14) 2_665 1_465 ? 
O6 K3 W2 89.49(14) 2_666 1_465 ? 
O2 K3 W2 164.03(14) 1_565 1_465 ? 
O9 K3 W2 83.59(13) 1_565 1_465 ? 
O5 K3 W2 26.24(12) 1_465 1_465 ? 
O11 K3 W2 27.30(12) 1_465 1_465 ? 
Mg1 K3 W2 55.63(7) 2_666 1_465 ? 
K2 K3 W2 61.24(3) 1_565 1_465 ? 
O4 K3 W3 156.96(15) 1_455 1_565 ? 
O8 K3 W3 101.82(16) 2_665 1_565 ? 
O6 K3 W3 57.09(15) 2_666 1_565 ? 
O2 K3 W3 104.18(15) 1_565 1_565 ? 
O9 K3 W3 25.09(13) 1_565 1_565 ? 
O5 K3 W3 75.28(14) 1_465 1_565 ? 
O11 K3 W3 89.41(14) 1_465 1_565 ? 
Mg1 K3 W3 56.61(6) 2_666 1_565 ? 
K2 K3 W3 64.78(3) 1_565 1_565 ? 
W2 K3 W3 77.99(4) 1_465 1_565 ? 
O4 K3 K1 42.63(14) 1_455 . ? 
O8 K3 K1 81.58(15) 2_665 . ? 
O6 K3 K1 109.99(15) 2_666 . ? 
O2 K3 K1 44.96(14) 1_565 . ? 
O9 K3 K1 140.28(14) 1_565 . ? 
O5 K3 K1 128.49(15) 1_465 . ? 
O11 K3 K1 120.44(14) 1_465 . ? 
Mg1 K3 K1 130.44(8) 2_666 . ? 
K2 K3 K1 129.52(6) 1_565 . ? 
W2 K3 K1 132.67(6) 1_465 . ? 
W3 K3 K1 148.83(6) 1_565 . ? 
O3 K4 O3 90.1(2) . 2_666 ? 
O3 K4 O7 84.37(19) . 1_455 ? 
O3 K4 O7 166.1(2) 2_666 1_455 ? 
O3 K4 O7 165.5(2) . 2_666 ? 
O3 K4 O7 86.05(19) 2_666 2_666 ? 
O7 K4 O7 96.1(2) 1_455 2_666 ? 
O3 K4 O2 76.06(18) . 2_656 ? 
O3 K4 O2 81.50(19) 2_666 2_656 ? 
O7 K4 O2 109.3(2) 1_455 2_656 ? 
O7 K4 O2 117.08(19) 2_666 2_656 ? 
O3 K4 O5 94.66(19) . 2_656 ? 
O3 K4 O5 134.85(19) 2_666 2_656 ? 
O7 K4 O5 58.52(19) 1_455 2_656 ? 
O7 K4 O5 97.96(18) 2_666 2_656 ? 
O2 K4 O5 56.56(17) 2_656 2_656 ? 
O3 K4 O4 67.80(18) . 1_455 ? 
O3 K4 O4 109.49(19) 2_666 1_455 ? 
O7 K4 O4 56.66(19) 1_455 1_455 ? 
O7 K4 O4 100.30(19) 2_666 1_455 ? 
O2 K4 O4 141.92(18) 2_656 1_455 ? 
O5 K4 O4 113.85(18) 2_656 1_455 ? 
O3 K4 O12 138.8(2) . 2_666 ? 
O3 K4 O12 75.89(19) 2_666 2_666 ? 
O7 K4 O12 116.3(2) 1_455 2_666 ? 
O7 K4 O12 53.37(19) 2_666 2_666 ? 
O2 K4 O12 63.77(18) 2_656 2_666 ? 
O5 K4 O12 71.24(19) 2_656 2_666 ? 
O4 K4 O12 153.37(19) 1_455 2_666 ? 
O3 K4 W1 74.40(14) . 1_455 ? 
O3 K4 W1 137.74(15) 2_666 1_455 ? 
O7 K4 W1 28.41(14) 1_455 1_455 ? 
O7 K4 W1 99.21(14) 2_666 1_455 ? 
O2 K4 W1 129.57(14) 2_656 1_455 ? 
O5 K4 W1 86.27(13) 2_656 1_455 ? 
O4 K4 W1 28.24(13) 1_455 1_455 ? 
O12 K4 W1 139.40(14) 2_666 1_455 ? 
O3 K4 W2 85.74(15) . 2_656 ? 
O3 K4 W2 107.95(15) 2_666 2_656 ? 
O7 K4 W2 84.37(16) 1_455 2_656 ? 
O7 K4 W2 108.77(15) 2_666 2_656 ? 
O2 K4 W2 28.12(12) 2_656 2_656 ? 
O5 K4 W2 28.47(11) 2_656 2_656 ? 
O4 K4 W2 133.55(15) 1_455 2_656 ? 
O12 K4 W2 63.24(14) 2_666 2_656 ? 
W1 K4 W2 109.74(6) 1_455 2_656 ? 
O3 K4 W1 165.97(15) . 2_666 ? 
O3 K4 W1 88.03(13) 2_666 2_666 ? 
O7 K4 W1 100.30(14) 1_455 2_666 ? 
O7 K4 W1 27.97(14) 2_666 2_666 ? 
O2 K4 W1 89.91(12) 2_656 2_666 ? 
O5 K4 W1 76.97(12) 2_656 2_666 ? 
O4 K4 W1 125.79(13) 1_455 2_666 ? 
O12 K4 W1 27.73(13) 2_666 2_666 ? 
W1 K4 W1 115.65(5) 1_455 2_666 ? 
W2 K4 W1 81.61(5) 2_656 2_666 ? 
O3 K4 W3 103.81(15) . 2_666 ? 
O3 K4 W3 24.29(13) 2_666 2_666 ? 
O7 K4 W3 146.48(16) 1_455 2_666 ? 
O7 K4 W3 68.11(14) 2_666 2_666 ? 
O2 K4 W3 104.19(13) 2_656 2_666 ? 
O5 K4 W3 149.34(13) 2_656 2_666 ? 
O4 K4 W3 95.87(14) 1_455 2_666 ? 
O12 K4 W3 78.82(15) 2_666 2_666 ? 
W1 K4 W3 122.00(6) 1_455 2_666 ? 
W2 K4 W3 128.14(6) 2_656 2_666 ? 
W1 K4 W3 79.65(4) 2_666 2_666 ? 
O8 K5 O8 180.0(3) . 2_655 ? 
O8 K5 O1 110.43(19) . 2_655 ? 
O8 K5 O1 69.57(19) 2_655 2_655 ? 
O8 K5 O1 69.57(19) . . ? 
O8 K5 O1 110.43(19) 2_655 . ? 
O1 K5 O1 180.00(16) 2_655 . ? 
O8 K5 O9 108.00(18) . . ? 
O8 K5 O9 72.00(18) 2_655 . ? 
O1 K5 O9 107.65(16) 2_655 . ? 
O1 K5 O9 72.35(16) . . ? 
O8 K5 O9 72.00(18) . 2_655 ? 
O8 K5 O9 108.00(18) 2_655 2_655 ? 
O1 K5 O9 72.35(16) 2_655 2_655 ? 
O1 K5 O9 107.65(16) . 2_655 ? 
O9 K5 O9 180.0(4) . 2_655 ? 
O8 K5 O11 94.76(19) . 2_655 ? 
O8 K5 O11 85.24(19) 2_655 2_655 ? 
O1 K5 O11 50.96(17) 2_655 2_655 ? 
O1 K5 O11 129.04(17) . 2_655 ? 
O9 K5 O11 67.17(17) . 2_655 ? 
O9 K5 O11 112.83(17) 2_655 2_655 ? 
O8 K5 O11 85.24(19) . . ? 
O8 K5 O11 94.76(19) 2_655 . ? 
O1 K5 O11 129.04(17) 2_655 . ? 
O1 K5 O11 50.96(17) . . ? 
O9 K5 O11 112.83(17) . . ? 
O9 K5 O11 67.17(17) 2_655 . ? 
O11 K5 O11 180.00(19) 2_655 . ? 
O8 K5 W2 92.60(14) . 2_655 ? 
O8 K5 W2 87.40(14) 2_655 2_655 ? 
O1 K5 W2 27.97(12) 2_655 2_655 ? 
O1 K5 W2 152.03(12) . 2_655 ? 
O9 K5 W2 94.29(12) . 2_655 ? 
O9 K5 W2 85.71(12) 2_655 2_655 ? 
O11 K5 W2 27.87(12) 2_655 2_655 ? 
O11 K5 W2 152.13(12) . 2_655 ? 
O8 K5 W2 87.40(14) . . ? 
O8 K5 W2 92.60(14) 2_655 . ? 
O1 K5 W2 152.03(12) 2_655 . ? 
O1 K5 W2 27.97(12) . . ? 
O9 K5 W2 85.71(12) . . ? 
O9 K5 W2 94.29(12) 2_655 . ? 
O11 K5 W2 152.13(12) 2_655 . ? 
O11 K5 W2 27.87(12) . . ? 
W2 K5 W2 180.0 2_655 . ? 
O8 K5 K2 132.99(14) . . ? 
O8 K5 K2 47.01(14) 2_655 . ? 
O1 K5 K2 64.54(11) 2_655 . ? 
O1 K5 K2 115.46(11) . . ? 
O9 K5 K2 44.48(12) . . ? 
O9 K5 K2 135.52(12) 2_655 . ? 
O11 K5 K2 43.65(13) 2_655 . ? 
O11 K5 K2 136.35(13) . . ? 
W2 K5 K2 61.024(11) 2_655 . ? 
W2 K5 K2 118.976(11) . . ? 
O8 K5 K2 47.01(14) . 1_655 ? 
O8 K5 K2 132.99(14) 2_655 1_655 ? 
O1 K5 K2 115.46(11) 2_655 1_655 ? 
O1 K5 K2 64.54(11) . 1_655 ? 
O9 K5 K2 135.52(12) . 1_655 ? 
O9 K5 K2 44.48(12) 2_655 1_655 ? 
O11 K5 K2 136.35(13) 2_655 1_655 ? 
O11 K5 K2 43.65(13) . 1_655 ? 
W2 K5 K2 118.976(11) 2_655 1_655 ? 
W2 K5 K2 61.024(11) . 1_655 ? 
K2 K5 K2 180.0 . 1_655 ? 
O5 Mg1 O1 152.3(3) 2_756 . ? 
O5 Mg1 O6 97.6(3) 2_756 . ? 
O1 Mg1 O6 108.9(3) . . ? 
O5 Mg1 O7 92.7(3) 2_756 . ? 
O1 Mg1 O7 93.6(3) . . ? 
O6 Mg1 O7 93.5(3) . . ? 
O5 Mg1 O10 90.1(3) 2_756 . ? 
O1 Mg1 O10 82.1(3) . . ? 
O6 Mg1 O10 90.1(3) . . ? 
O7 Mg1 O10 175.1(3) . . ? 
O5 Mg1 W2 132.5(2) 2_756 . ? 
O1 Mg1 W2 26.29(18) . . ? 
O6 Mg1 W2 114.6(2) . . ? 
O7 Mg1 W2 117.7(2) . . ? 
O10 Mg1 W2 57.7(2) . . ? 
O5 Mg1 K3 50.37(18) 2_756 2_666 ? 
O1 Mg1 K3 151.2(2) . 2_666 ? 
O6 Mg1 K3 48.7(2) . 2_666 ? 
O7 Mg1 K3 104.4(2) . 2_666 ? 
O10 Mg1 K3 80.4(2) . 2_666 ? 
W2 Mg1 K3 136.38(10) . 2_666 ? 
O5 Mg1 K4 50.3(2) 2_756 1_655 ? 
O1 Mg1 K4 122.2(2) . 1_655 ? 
O6 Mg1 K4 111.7(2) . 1_655 ? 
O7 Mg1 K4 45.5(2) . 1_655 ? 
O10 Mg1 K4 135.5(2) . 1_655 ? 
W2 Mg1 K4 131.61(11) . 1_655 ? 
K3 Mg1 K4 85.99(8) 2_666 1_655 ? 
O5 Mg1 K4 78.3(2) 2_756 2_666 ? 
O1 Mg1 K4 122.8(2) . 2_666 ? 
O6 Mg1 K4 57.2(2) . 2_666 ? 
O7 Mg1 K4 42.0(2) . 2_666 ? 
O10 Mg1 K4 142.7(2) . 2_666 ? 
W2 Mg1 K4 148.45(10) . 2_666 ? 
K3 Mg1 K4 64.80(7) 2_666 2_666 ? 
K4 Mg1 K4 57.98(6) 1_655 2_666 ? 
W2 O1 Mg1 124.3(3) . . ? 
W2 O1 K5 103.2(2) . . ? 
Mg1 O1 K5 129.8(3) . . ? 
W2 O2 K1 128.5(3) . 1_545 ? 
W2 O2 K3 122.3(3) . 1_545 ? 
K1 O2 K3 89.31(19) 1_545 1_545 ? 
W2 O2 K4 97.1(2) . 2_656 ? 
K1 O2 K4 83.91(18) 1_545 2_656 ? 
K3 O2 K4 133.0(2) 1_545 2_656 ? 
W3 O3 K4 121.4(3) . . ? 
W3 O3 K4 115.1(3) . 2_666 ? 
K4 O3 K4 89.85(19) . 2_666 ? 
W3 O3 K1 124.8(3) . . ? 
K4 O3 K1 106.9(2) . . ? 
K4 O3 K1 88.34(19) 2_666 . ? 
W1 O4 K3 139.5(3) . 1_655 ? 
W1 O4 K1 120.1(3) . 1_655 ? 
K3 O4 K1 95.3(2) 1_655 1_655 ? 
W1 O4 K4 95.2(3) . 1_655 ? 
K3 O4 K4 96.3(2) 1_655 1_655 ? 
K1 O4 K4 101.8(2) 1_655 1_655 ? 
W2 O5 Mg1 134.8(4) . 2_756 ? 
W2 O5 K3 109.2(3) . 1_645 ? 
Mg1 O5 K3 96.9(2) 2_756 1_645 ? 
W2 O5 K4 96.3(2) . 2_656 ? 
Mg1 O5 K4 99.9(2) 2_756 2_656 ? 
K3 O5 K4 122.4(2) 1_645 2_656 ? 
W3 O6 Mg1 134.9(4) . . ? 
W3 O6 K3 127.0(3) . 2_666 ? 
Mg1 O6 K3 97.5(3) . 2_666 ? 
W1 O7 Mg1 142.0(4) . . ? 
W1 O7 K4 101.3(3) . 1_655 ? 
Mg1 O7 K4 104.1(3) . 1_655 ? 
W1 O7 K4 99.1(3) . 2_666 ? 
Mg1 O7 K4 111.2(3) . 2_666 ? 
K4 O7 K4 83.90(19) 1_655 2_666 ? 
W1 O8 K3 124.2(3) . 2_665 ? 
W1 O8 K5 114.1(3) . . ? 
K3 O8 K5 91.8(2) 2_665 . ? 
W1 O8 K2 141.6(3) . 1_655 ? 
K3 O8 K2 84.80(19) 2_665 1_655 ? 
K5 O8 K2 86.5(2) . 1_655 ? 
W3 O9 K2 129.0(3) . . ? 
W3 O9 K3 112.8(3) . 1_545 ? 
K2 O9 K3 86.29(19) . 1_545 ? 
W3 O9 K5 140.4(3) . . ? 
K2 O9 K5 84.37(16) . . ? 
K3 O9 K5 86.75(17) 1_545 . ? 
W3 O10 Mg1 125.9(4) 2_656 . ? 
W2 O11 K1 136.1(4) . 2_655 ? 
W2 O11 K2 116.8(4) . 1_655 ? 
K1 O11 K2 107.0(3) 2_655 1_655 ? 
W2 O11 K3 90.0(3) . 1_645 ? 
K1 O11 K3 98.5(2) 2_655 1_645 ? 
K2 O11 K3 75.08(17) 1_655 1_645 ? 
W2 O11 K5 85.7(3) . . ? 
K1 O11 K5 107.9(2) 2_655 . ? 
K2 O11 K5 76.86(18) 1_655 . ? 
K3 O11 K5 146.0(3) 1_645 . ? 
W1 O12 K1 149.5(4) . . ? 
W1 O12 K1 119.6(3) . 2_665 ? 
K1 O12 K1 85.7(2) . 2_665 ? 
W1 O12 K4 89.6(3) . 2_666 ? 
K1 O12 K4 80.3(2) . 2_666 ? 
K1 O12 K4 137.3(3) 2_665 2_666 ? 
 
loop_ 
 _geom_torsion_atom_site_label_1 
 _geom_torsion_atom_site_label_2 
 _geom_torsion_atom_site_label_3 
 _geom_torsion_atom_site_label_4 
 _geom_torsion 
 _geom_torsion_site_symmetry_1 
 _geom_torsion_site_symmetry_2 
 _geom_torsion_site_symmetry_3 
 _geom_torsion_site_symmetry_4 
 _geom_torsion_publ_flag 
O11 K1 K3 O4 70.3(3) 2_655 . . 1_455 ? 
O12 K1 K3 O4 -149.9(3) . . . 1_455 ? 
O2 K1 K3 O4 -136.3(3) 1_565 . . 1_455 ? 
O3 K1 K3 O4 -56.9(2) . . . 1_455 ? 
O12 K1 K3 O4 123.1(3) 2_665 . . 1_455 ? 
K1 K1 K3 O4 159.8(2) 2_665 . . 1_455 ? 
W1 K1 K3 O4 9.0(2) 1_455 . . 1_455 ? 
K4 K1 K3 O4 -101.5(2) 2_666 . . 1_455 ? 
W1 K1 K3 O4 107.5(2) 2_665 . . 1_455 ? 
W2 K1 K3 O4 95.1(2) 2_655 . . 1_455 ? 
O11 K1 K3 O8 -44.7(3) 2_655 . . 2_665 ? 
O12 K1 K3 O8 95.1(3) . . . 2_665 ? 
O4 K1 K3 O8 -115.1(3) 1_455 . . 2_665 ? 
O2 K1 K3 O8 108.7(2) 1_565 . . 2_665 ? 
O3 K1 K3 O8 -171.9(2) . . . 2_665 ? 
O12 K1 K3 O8 8.1(2) 2_665 . . 2_665 ? 
K1 K1 K3 O8 44.74(17) 2_665 . . 2_665 ? 
W1 K1 K3 O8 -106.10(15) 1_455 . . 2_665 ? 
K4 K1 K3 O8 143.42(16) 2_666 . . 2_665 ? 
W1 K1 K3 O8 -7.60(15) 2_665 . . 2_665 ? 
W2 K1 K3 O8 -20.01(17) 2_655 . . 2_665 ? 
O11 K1 K3 O6 157.4(3) 2_655 . . 2_666 ? 
O12 K1 K3 O6 -62.8(3) . . . 2_666 ? 
O4 K1 K3 O6 87.1(3) 1_455 . . 2_666 ? 
O2 K1 K3 O6 -49.2(2) 1_565 . . 2_666 ? 
O3 K1 K3 O6 30.2(2) . . . 2_666 ? 
O12 K1 K3 O6 -149.8(2) 2_665 . . 2_666 ? 
K1 K1 K3 O6 -113.15(17) 2_665 . . 2_666 ? 
W1 K1 K3 O6 96.01(16) 1_455 . . 2_666 ? 
K4 K1 K3 O6 -14.47(16) 2_666 . . 2_666 ? 
W1 K1 K3 O6 -165.49(16) 2_665 . . 2_666 ? 
W2 K1 K3 O6 -177.89(16) 2_655 . . 2_666 ? 
O11 K1 K3 O2 -153.4(3) 2_655 . . 1_565 ? 
O12 K1 K3 O2 -13.6(3) . . . 1_565 ? 
O4 K1 K3 O2 136.3(3) 1_455 . . 1_565 ? 
O3 K1 K3 O2 79.4(2) . . . 1_565 ? 
O12 K1 K3 O2 -100.6(2) 2_665 . . 1_565 ? 
K1 K1 K3 O2 -63.93(19) 2_665 . . 1_565 ? 
W1 K1 K3 O2 145.23(19) 1_455 . . 1_565 ? 
K4 K1 K3 O2 34.75(19) 2_666 . . 1_565 ? 
W1 K1 K3 O2 -116.27(19) 2_665 . . 1_565 ? 
W2 K1 K3 O2 -128.7(2) 2_655 . . 1_565 ? 
O11 K1 K3 O9 -102.1(3) 2_655 . . 1_565 ? 
O12 K1 K3 O9 37.7(3) . . . 1_565 ? 
O4 K1 K3 O9 -172.4(3) 1_455 . . 1_565 ? 
O2 K1 K3 O9 51.3(3) 1_565 . . 1_565 ? 
O3 K1 K3 O9 130.7(3) . . . 1_565 ? 
O12 K1 K3 O9 -49.3(3) 2_665 . . 1_565 ? 
K1 K1 K3 O9 -12.6(2) 2_665 . . 1_565 ? 
W1 K1 K3 O9 -163.5(2) 1_455 . . 1_565 ? 
K4 K1 K3 O9 86.0(2) 2_666 . . 1_565 ? 
W1 K1 K3 O9 -65.0(2) 2_665 . . 1_565 ? 
W2 K1 K3 O9 -77.4(2) 2_655 . . 1_565 ? 
O11 K1 K3 O5 82.9(3) 2_655 . . 1_465 ? 
O12 K1 K3 O5 -137.3(3) . . . 1_465 ? 
O4 K1 K3 O5 12.6(3) 1_455 . . 1_465 ? 
O2 K1 K3 O5 -123.7(3) 1_565 . . 1_465 ? 
O3 K1 K3 O5 -44.3(2) . . . 1_465 ? 
O12 K1 K3 O5 135.7(2) 2_665 . . 1_465 ? 
K1 K1 K3 O5 172.38(18) 2_665 . . 1_465 ? 
W1 K1 K3 O5 21.54(17) 1_455 . . 1_465 ? 
K4 K1 K3 O5 -88.93(18) 2_666 . . 1_465 ? 
W1 K1 K3 O5 120.05(18) 2_665 . . 1_465 ? 
W2 K1 K3 O5 107.64(18) 2_655 . . 1_465 ? 
O11 K1 K3 O11 17.9(4) 2_655 . . 1_465 ? 
O12 K1 K3 O11 157.7(3) . . . 1_465 ? 
O4 K1 K3 O11 -52.4(3) 1_455 . . 1_465 ? 
O2 K1 K3 O11 171.3(2) 1_565 . . 1_465 ? 
O3 K1 K3 O11 -109.3(2) . . . 1_465 ? 
O12 K1 K3 O11 70.7(2) 2_665 . . 1_465 ? 
K1 K1 K3 O11 107.35(17) 2_665 . . 1_465 ? 
W1 K1 K3 O11 -43.48(16) 1_455 . . 1_465 ? 
K4 K1 K3 O11 -153.96(16) 2_666 . . 1_465 ? 
W1 K1 K3 O11 55.02(16) 2_665 . . 1_465 ? 
W2 K1 K3 O11 42.61(18) 2_655 . . 1_465 ? 
O11 K1 K3 Mg1 125.7(3) 2_655 . . 2_666 ? 
O12 K1 K3 Mg1 -94.5(2) . . . 2_666 ? 
O4 K1 K3 Mg1 55.3(2) 1_455 . . 2_666 ? 
O2 K1 K3 Mg1 -80.9(2) 1_565 . . 2_666 ? 
O3 K1 K3 Mg1 -1.55(18) . . . 2_666 ? 
O12 K1 K3 Mg1 178.46(19) 2_665 . . 2_666 ? 
K1 K1 K3 Mg1 -144.87(11) 2_665 . . 2_666 ? 
W1 K1 K3 Mg1 64.29(10) 1_455 . . 2_666 ? 
K4 K1 K3 Mg1 -46.19(12) 2_666 . . 2_666 ? 
W1 K1 K3 Mg1 162.80(11) 2_665 . . 2_666 ? 
W2 K1 K3 Mg1 150.39(10) 2_655 . . 2_666 ? 
O11 K1 K3 K2 -36.4(3) 2_655 . . 1_565 ? 
O12 K1 K3 K2 103.4(2) . . . 1_565 ? 
O4 K1 K3 K2 -106.7(2) 1_455 . . 1_565 ? 
O2 K1 K3 K2 117.0(2) 1_565 . . 1_565 ? 
O3 K1 K3 K2 -163.61(14) . . . 1_565 ? 
O12 K1 K3 K2 16.40(17) 2_665 . . 1_565 ? 
K1 K1 K3 K2 53.07(10) 2_665 . . 1_565 ? 
W1 K1 K3 K2 -97.77(7) 1_455 . . 1_565 ? 
K4 K1 K3 K2 151.76(7) 2_666 . . 1_565 ? 
W1 K1 K3 K2 0.74(6) 2_665 . . 1_565 ? 
W2 K1 K3 K2 -11.67(12) 2_655 . . 1_565 ? 
O11 K1 K3 W2 48.6(3) 2_655 . . 1_465 ? 
O12 K1 K3 W2 -171.6(2) . . . 1_465 ? 
O4 K1 K3 W2 -21.8(2) 1_455 . . 1_465 ? 
O2 K1 K3 W2 -158.0(2) 1_565 . . 1_465 ? 
O3 K1 K3 W2 -78.65(15) . . . 1_465 ? 
O12 K1 K3 W2 101.36(17) 2_665 . . 1_465 ? 
K1 K1 K3 W2 138.04(8) 2_665 . . 1_465 ? 
W1 K1 K3 W2 -12.80(7) 1_455 . . 1_465 ? 
K4 K1 K3 W2 -123.28(8) 2_666 . . 1_465 ? 
W1 K1 K3 W2 85.70(7) 2_665 . . 1_465 ? 
W2 K1 K3 W2 73.29(11) 2_655 . . 1_465 ? 
O11 K1 K3 W3 -143.6(3) 2_655 . . 1_565 ? 
O12 K1 K3 W3 -3.8(3) . . . 1_565 ? 
O4 K1 K3 W3 146.0(2) 1_455 . . 1_565 ? 
O2 K1 K3 W3 9.7(2) 1_565 . . 1_565 ? 
O3 K1 K3 W3 89.13(17) . . . 1_565 ? 
O12 K1 K3 W3 -90.86(19) 2_665 . . 1_565 ? 
K1 K1 K3 W3 -54.19(14) 2_665 . . 1_565 ? 
W1 K1 K3 W3 154.97(11) 1_455 . . 1_565 ? 
K4 K1 K3 W3 44.50(12) 2_666 . . 1_565 ? 
W1 K1 K3 W3 -106.52(11) 2_665 . . 1_565 ? 
W2 K1 K3 W3 -118.93(11) 2_655 . . 1_565 ? 
O11 W2 K5 O8 -84.7(3) . . . . ? 
O2 W2 K5 O8 165.6(2) . . . . ? 
O5 W2 K5 O8 -8.9(5) . . . . ? 
O1 W2 K5 O8 48.7(3) . . . . ? 
Mg1 W2 K5 O8 57.28(15) . . . . ? 
K4 W2 K5 O8 167.36(15) 2_656 . . . ? 
K3 W2 K5 O8 -50.10(14) 1_645 . . . ? 
K2 W2 K5 O8 -40.97(13) 1_655 . . . ? 
K3 W2 K5 O8 147.56(14) 1_545 . . . ? 
K1 W2 K5 O8 -109.83(14) 2_655 . . . ? 
K1 W2 K5 O8 -162.62(14) 1_545 . . . ? 
O11 W2 K5 O8 95.3(3) . . . 2_655 ? 
O2 W2 K5 O8 -14.4(2) . . . 2_655 ? 
O5 W2 K5 O8 171.1(5) . . . 2_655 ? 
O1 W2 K5 O8 -131.3(3) . . . 2_655 ? 
Mg1 W2 K5 O8 -122.72(15) . . . 2_655 ? 
K4 W2 K5 O8 -12.64(15) 2_656 . . 2_655 ? 
K3 W2 K5 O8 129.90(14) 1_645 . . 2_655 ? 
K2 W2 K5 O8 139.03(13) 1_655 . . 2_655 ? 
K3 W2 K5 O8 -32.44(14) 1_545 . . 2_655 ? 
K1 W2 K5 O8 70.17(14) 2_655 . . 2_655 ? 
K1 W2 K5 O8 17.38(14) 1_545 . . 2_655 ? 
O11 W2 K5 O1 46.5(4) . . . 2_655 ? 
O2 W2 K5 O1 -63.1(3) . . . 2_655 ? 
O5 W2 K5 O1 122.4(5) . . . 2_655 ? 
O1 W2 K5 O1 180.0 . . . 2_655 ? 
Mg1 W2 K5 O1 -171.5(2) . . . 2_655 ? 
K4 W2 K5 O1 -61.4(2) 2_656 . . 2_655 ? 
K3 W2 K5 O1 81.2(2) 1_645 . . 2_655 ? 
K2 W2 K5 O1 90.3(2) 1_655 . . 2_655 ? 
K3 W2 K5 O1 -81.2(2) 1_545 . . 2_655 ? 
K1 W2 K5 O1 21.4(2) 2_655 . . 2_655 ? 
K1 W2 K5 O1 -31.4(2) 1_545 . . 2_655 ? 
O11 W2 K5 O1 -133.5(4) . . . . ? 
O2 W2 K5 O1 116.9(3) . . . . ? 
O5 W2 K5 O1 -57.6(5) . . . . ? 
Mg1 W2 K5 O1 8.5(2) . . . . ? 
K4 W2 K5 O1 118.6(2) 2_656 . . . ? 
K3 W2 K5 O1 -98.8(2) 1_645 . . . ? 
K2 W2 K5 O1 -89.7(2) 1_655 . . . ? 
K3 W2 K5 O1 98.8(2) 1_545 . . . ? 
K1 W2 K5 O1 -158.6(2) 2_655 . . . ? 
K1 W2 K5 O1 148.6(2) 1_545 . . . ? 
O11 W2 K5 O9 167.0(3) . . . . ? 
O2 W2 K5 O9 57.4(2) . . . . ? 
O5 W2 K5 O9 -117.2(5) . . . . ? 
O1 W2 K5 O9 -59.5(3) . . . . ? 
Mg1 W2 K5 O9 -50.99(14) . . . . ? 
K4 W2 K5 O9 59.09(14) 2_656 . . . ? 
K3 W2 K5 O9 -158.37(13) 1_645 . . . ? 
K2 W2 K5 O9 -149.25(12) 1_655 . . . ? 
K3 W2 K5 O9 39.29(13) 1_545 . . . ? 
K1 W2 K5 O9 141.90(13) 2_655 . . . ? 
K1 W2 K5 O9 89.11(13) 1_545 . . . ? 
O11 W2 K5 O9 -13.0(3) . . . 2_655 ? 
O2 W2 K5 O9 -122.6(2) . . . 2_655 ? 
O5 W2 K5 O9 62.8(5) . . . 2_655 ? 
O1 W2 K5 O9 120.5(3) . . . 2_655 ? 
Mg1 W2 K5 O9 129.01(14) . . . 2_655 ? 
K4 W2 K5 O9 -120.91(14) 2_656 . . 2_655 ? 
K3 W2 K5 O9 21.63(13) 1_645 . . 2_655 ? 
K2 W2 K5 O9 30.75(12) 1_655 . . 2_655 ? 
K3 W2 K5 O9 -140.71(13) 1_545 . . 2_655 ? 
K1 W2 K5 O9 -38.10(13) 2_655 . . 2_655 ? 
K1 W2 K5 O9 -90.89(13) 1_545 . . 2_655 ? 
O11 W2 K5 O11 180.0 . . . 2_655 ? 
O2 W2 K5 O11 70.4(3) . . . 2_655 ? 
O5 W2 K5 O11 -104.1(5) . . . 2_655 ? 
O1 W2 K5 O11 -46.5(4) . . . 2_655 ? 
Mg1 W2 K5 O11 -38.0(3) . . . 2_655 ? 
K4 W2 K5 O11 72.1(3) 2_656 . . 2_655 ? 
K3 W2 K5 O11 -145.4(3) 1_645 . . 2_655 ? 
K2 W2 K5 O11 -136.2(3) 1_655 . . 2_655 ? 
K3 W2 K5 O11 52.3(3) 1_545 . . 2_655 ? 
K1 W2 K5 O11 154.9(3) 2_655 . . 2_655 ? 
K1 W2 K5 O11 102.1(3) 1_545 . . 2_655 ? 
O2 W2 K5 O11 -109.6(3) . . . . ? 
O5 W2 K5 O11 75.9(5) . . . . ? 
O1 W2 K5 O11 133.5(4) . . . . ? 
Mg1 W2 K5 O11 142.0(3) . . . . ? 
K4 W2 K5 O11 -107.9(3) 2_656 . . . ? 
K3 W2 K5 O11 34.6(3) 1_645 . . . ? 
K2 W2 K5 O11 43.8(3) 1_655 . . . ? 
K3 W2 K5 O11 -127.7(3) 1_545 . . . ? 
K1 W2 K5 O11 -25.1(3) 2_655 . . . ? 
K1 W2 K5 O11 -77.9(3) 1_545 . . . ? 
O11 W2 K5 W2 80(100) . . . 2_655 ? 
O2 W2 K5 W2 -30(100) . . . 2_655 ? 
O5 W2 K5 W2 156(100) . . . 2_655 ? 
O1 W2 K5 W2 -147(100) . . . 2_655 ? 
Mg1 W2 K5 W2 -138(100) . . . 2_655 ? 
K4 W2 K5 W2 -28(100) 2_656 . . 2_655 ? 
K3 W2 K5 W2 114(100) 1_645 . . 2_655 ? 
K2 W2 K5 W2 124(100) 1_655 . . 2_655 ? 
K3 W2 K5 W2 -48(100) 1_545 . . 2_655 ? 
K1 W2 K5 W2 55(100) 2_655 . . 2_655 ? 
K1 W2 K5 W2 2(100) 1_545 . . 2_655 ? 
O11 W2 K5 K2 136.2(3) . . . . ? 
O2 W2 K5 K2 26.6(2) . . . . ? 
O5 W2 K5 K2 -147.9(5) . . . . ? 
O1 W2 K5 K2 -90.3(2) . . . . ? 
Mg1 W2 K5 K2 -81.75(6) . . . . ? 
K4 W2 K5 K2 28.34(6) 2_656 . . . ? 
K3 W2 K5 K2 170.87(3) 1_645 . . . ? 
K2 W2 K5 K2 180.0 1_655 . . . ? 
K3 W2 K5 K2 8.53(3) 1_545 . . . ? 
K1 W2 K5 K2 111.15(3) 2_655 . . . ? 
K1 W2 K5 K2 58.36(3) 1_545 . . . ? 
O11 W2 K5 K2 -43.8(3) . . . 1_655 ? 
O2 W2 K5 K2 -153.4(2) . . . 1_655 ? 
O5 W2 K5 K2 32.1(5) . . . 1_655 ? 
O1 W2 K5 K2 89.7(2) . . . 1_655 ? 
Mg1 W2 K5 K2 98.25(6) . . . 1_655 ? 
K4 W2 K5 K2 -151.66(6) 2_656 . . 1_655 ? 
K3 W2 K5 K2 -9.13(3) 1_645 . . 1_655 ? 
K3 W2 K5 K2 -171.47(3) 1_545 . . 1_655 ? 
K1 W2 K5 K2 -68.85(3) 2_655 . . 1_655 ? 
K1 W2 K5 K2 -121.64(3) 1_545 . . 1_655 ? 
O9 K2 K5 O8 110.3(3) 2 . . . ? 
O9 K2 K5 O8 -69.7(3) . . . . ? 
O11 K2 K5 O8 35.6(3) 2_655 . . . ? 
O11 K2 K5 O8 -144.4(3) 1_455 . . . ? 
O8 K2 K5 O8 0.0 1_455 . . . ? 
O8 K2 K5 O8 180.0 2_655 . . . ? 
K3 K2 K5 O8 54.56(19) 2_565 . . . ? 
K3 K2 K5 O8 -125.44(19) 1_545 . . . ? 
W2 K2 K5 O8 63.56(19) 2_655 . . . ? 
W2 K2 K5 O8 -116.44(19) 1_455 . . . ? 
K5 K2 K5 O8 -164.89(19) 1_455 . . . ? 
O9 K2 K5 O8 -69.7(3) 2 . . 2_655 ? 
O9 K2 K5 O8 110.3(3) . . . 2_655 ? 
O11 K2 K5 O8 -144.4(3) 2_655 . . 2_655 ? 
O11 K2 K5 O8 35.6(3) 1_455 . . 2_655 ? 
O8 K2 K5 O8 180.0 1_455 . . 2_655 ? 
K3 K2 K5 O8 -125.44(19) 2_565 . . 2_655 ? 
K3 K2 K5 O8 54.56(19) 1_545 . . 2_655 ? 
W2 K2 K5 O8 -116.44(19) 2_655 . . 2_655 ? 
W2 K2 K5 O8 63.56(19) 1_455 . . 2_655 ? 
K5 K2 K5 O8 15.11(19) 1_455 . . 2_655 ? 
O9 K2 K5 O1 15.4(2) 2 . . 2_655 ? 
O9 K2 K5 O1 -164.6(2) . . . 2_655 ? 
O11 K2 K5 O1 -59.2(2) 2_655 . . 2_655 ? 
O11 K2 K5 O1 120.8(2) 1_455 . . 2_655 ? 
O8 K2 K5 O1 -94.9(2) 1_455 . . 2_655 ? 
O8 K2 K5 O1 85.1(2) 2_655 . . 2_655 ? 
K3 K2 K5 O1 -40.29(14) 2_565 . . 2_655 ? 
K3 K2 K5 O1 139.71(14) 1_545 . . 2_655 ? 
W2 K2 K5 O1 -31.29(13) 2_655 . . 2_655 ? 
W2 K2 K5 O1 148.70(13) 1_455 . . 2_655 ? 
K5 K2 K5 O1 100.26(13) 1_455 . . 2_655 ? 
O9 K2 K5 O1 -164.6(2) 2 . . . ? 
O9 K2 K5 O1 15.4(2) . . . . ? 
O11 K2 K5 O1 120.8(2) 2_655 . . . ? 
O11 K2 K5 O1 -59.2(2) 1_455 . . . ? 
O8 K2 K5 O1 85.1(2) 1_455 . . . ? 
O8 K2 K5 O1 -94.9(2) 2_655 . . . ? 
K3 K2 K5 O1 139.71(14) 2_565 . . . ? 
K3 K2 K5 O1 -40.29(14) 1_545 . . . ? 
W2 K2 K5 O1 148.71(13) 2_655 . . . ? 
W2 K2 K5 O1 -31.29(13) 1_455 . . . ? 
K5 K2 K5 O1 -79.74(13) 1_455 . . . ? 
O9 K2 K5 O9 180.0 2 . . . ? 
O11 K2 K5 O9 105.4(3) 2_655 . . . ? 
O11 K2 K5 O9 -74.6(3) 1_455 . . . ? 
O8 K2 K5 O9 69.7(3) 1_455 . . . ? 
O8 K2 K5 O9 -110.3(3) 2_655 . . . ? 
K3 K2 K5 O9 124.31(18) 2_565 . . . ? 
K3 K2 K5 O9 -55.69(18) 1_545 . . . ? 
W2 K2 K5 O9 133.30(18) 2_655 . . . ? 
W2 K2 K5 O9 -46.70(18) 1_455 . . . ? 
K5 K2 K5 O9 -95.15(18) 1_455 . . . ? 
O9 K2 K5 O9 0.0 2 . . 2_655 ? 
O9 K2 K5 O9 180.0 . . . 2_655 ? 
O11 K2 K5 O9 -74.6(3) 2_655 . . 2_655 ? 
O11 K2 K5 O9 105.4(3) 1_455 . . 2_655 ? 
O8 K2 K5 O9 -110.3(3) 1_455 . . 2_655 ? 
O8 K2 K5 O9 69.7(3) 2_655 . . 2_655 ? 
K3 K2 K5 O9 -55.69(18) 2_565 . . 2_655 ? 
K3 K2 K5 O9 124.31(18) 1_545 . . 2_655 ? 
W2 K2 K5 O9 -46.70(18) 2_655 . . 2_655 ? 
W2 K2 K5 O9 133.30(18) 1_455 . . 2_655 ? 
K5 K2 K5 O9 84.85(18) 1_455 . . 2_655 ? 
O9 K2 K5 O11 74.6(3) 2 . . 2_655 ? 
O9 K2 K5 O11 -105.4(3) . . . 2_655 ? 
O11 K2 K5 O11 180.0 1_455 . . 2_655 ? 
O8 K2 K5 O11 -35.6(3) 1_455 . . 2_655 ? 
O8 K2 K5 O11 144.4(3) 2_655 . . 2_655 ? 
K3 K2 K5 O11 18.94(18) 2_565 . . 2_655 ? 
K3 K2 K5 O11 -161.06(18) 1_545 . . 2_655 ? 
W2 K2 K5 O11 27.93(18) 2_655 . . 2_655 ? 
W2 K2 K5 O11 -152.07(18) 1_455 . . 2_655 ? 
K5 K2 K5 O11 159.49(18) 1_455 . . 2_655 ? 
O9 K2 K5 O11 -105.4(3) 2 . . . ? 
O9 K2 K5 O11 74.6(3) . . . . ? 
O11 K2 K5 O11 180.0 2_655 . . . ? 
O11 K2 K5 O11 0.0 1_455 . . . ? 
O8 K2 K5 O11 144.4(3) 1_455 . . . ? 
O8 K2 K5 O11 -35.6(3) 2_655 . . . ? 
K3 K2 K5 O11 -161.06(18) 2_565 . . . ? 
K3 K2 K5 O11 18.94(18) 1_545 . . . ? 
W2 K2 K5 O11 -152.07(18) 2_655 . . . ? 
W2 K2 K5 O11 27.93(18) 1_455 . . . ? 
K5 K2 K5 O11 -20.51(18) 1_455 . . . ? 
O9 K2 K5 W2 46.70(18) 2 . . 2_655 ? 
O9 K2 K5 W2 -133.30(18) . . . 2_655 ? 
O11 K2 K5 W2 -27.93(18) 2_655 . . 2_655 ? 
O11 K2 K5 W2 152.07(18) 1_455 . . 2_655 ? 
O8 K2 K5 W2 -63.56(19) 1_455 . . 2_655 ? 
O8 K2 K5 W2 116.44(19) 2_655 . . 2_655 ? 
K3 K2 K5 W2 -9.00(3) 2_565 . . 2_655 ? 
K3 K2 K5 W2 171.00(3) 1_545 . . 2_655 ? 
W2 K2 K5 W2 180.0 1_455 . . 2_655 ? 
K5 K2 K5 W2 131.551(12) 1_455 . . 2_655 ? 
O9 K2 K5 W2 -133.30(18) 2 . . . ? 
O9 K2 K5 W2 46.70(18) . . . . ? 
O11 K2 K5 W2 152.07(18) 2_655 . . . ? 
O11 K2 K5 W2 -27.93(18) 1_455 . . . ? 
O8 K2 K5 W2 116.44(19) 1_455 . . . ? 
O8 K2 K5 W2 -63.56(19) 2_655 . . . ? 
K3 K2 K5 W2 171.00(3) 2_565 . . . ? 
K3 K2 K5 W2 -9.00(3) 1_545 . . . ? 
W2 K2 K5 W2 180.0 2_655 . . . ? 
W2 K2 K5 W2 0.0 1_455 . . . ? 
K5 K2 K5 W2 -48.449(12) 1_455 . . . ? 
O9 K2 K5 K2 -84.85(18) 2 . . 1_655 ? 
O9 K2 K5 K2 95.15(18) . . . 1_655 ? 
O11 K2 K5 K2 -159.49(18) 2_655 . . 1_655 ? 
O11 K2 K5 K2 20.51(18) 1_455 . . 1_655 ? 
O8 K2 K5 K2 164.89(19) 1_455 . . 1_655 ? 
O8 K2 K5 K2 -15.11(19) 2_655 . . 1_655 ? 
K3 K2 K5 K2 -140.55(3) 2_565 . . 1_655 ? 
K3 K2 K5 K2 39.45(3) 1_545 . . 1_655 ? 
W2 K2 K5 K2 -131.551(12) 2_655 . . 1_655 ? 
W2 K2 K5 K2 48.449(12) 1_455 . . 1_655 ? 
K5 K2 K5 K2 0.0 1_455 . . 1_655 ? 
O11 W2 Mg1 O5 -116.4(4) . . . 2_756 ? 
O2 W2 Mg1 O5 108.5(4) . . . 2_756 ? 
O5 W2 Mg1 O5 -3.5(5) . . . 2_756 ? 
O1 W2 Mg1 O5 -149.0(5) . . . 2_756 ? 
K4 W2 Mg1 O5 50.0(3) 2_656 . . 2_756 ? 
K5 W2 Mg1 O5 -162.1(3) . . . 2_756 ? 
K3 W2 Mg1 O5 -45.1(3) 1_645 . . 2_756 ? 
K2 W2 Mg1 O5 -101.9(3) 1_655 . . 2_756 ? 
K3 W2 Mg1 O5 135.2(3) 1_545 . . 2_756 ? 
K1 W2 Mg1 O5 -134.3(3) 2_655 . . 2_756 ? 
K1 W2 Mg1 O5 117.6(3) 1_545 . . 2_756 ? 
O11 W2 Mg1 O1 32.6(5) . . . . ? 
O2 W2 Mg1 O1 -102.5(4) . . . . ? 
O5 W2 Mg1 O1 145.5(4) . . . . ? 
K4 W2 Mg1 O1 -161.0(4) 2_656 . . . ? 
K5 W2 Mg1 O1 -13.1(4) . . . . ? 
K3 W2 Mg1 O1 103.9(4) 1_645 . . . ? 
K2 W2 Mg1 O1 47.1(4) 1_655 . . . ? 
K3 W2 Mg1 O1 -75.8(4) 1_545 . . . ? 
K1 W2 Mg1 O1 14.7(4) 2_655 . . . ? 
K1 W2 Mg1 O1 -93.4(4) 1_545 . . . ? 
O11 W2 Mg1 O6 115.5(4) . . . . ? 
O2 W2 Mg1 O6 -19.5(3) . . . . ? 
O5 W2 Mg1 O6 -131.6(3) . . . . ? 
O1 W2 Mg1 O6 82.9(5) . . . . ? 
K4 W2 Mg1 O6 -78.1(2) 2_656 . . . ? 
K5 W2 Mg1 O6 69.8(2) . . . . ? 
K3 W2 Mg1 O6 -173.1(2) 1_645 . . . ? 
K2 W2 Mg1 O6 130.1(2) 1_655 . . . ? 
K3 W2 Mg1 O6 7.1(2) 1_545 . . . ? 
K1 W2 Mg1 O6 97.6(3) 2_655 . . . ? 
K1 W2 Mg1 O6 -10.4(3) 1_545 . . . ? 
O11 W2 Mg1 O7 7.1(4) . . . . ? 
O2 W2 Mg1 O7 -128.0(3) . . . . ? 
O5 W2 Mg1 O7 120.0(3) . . . . ? 
O1 W2 Mg1 O7 -25.5(4) . . . . ? 
K4 W2 Mg1 O7 173.5(3) 2_656 . . . ? 
K5 W2 Mg1 O7 -38.7(3) . . . . ? 
K3 W2 Mg1 O7 78.4(3) 1_645 . . . ? 
K2 W2 Mg1 O7 21.6(3) 1_655 . . . ? 
K3 W2 Mg1 O7 -101.3(3) 1_545 . . . ? 
K1 W2 Mg1 O7 -10.8(4) 2_655 . . . ? 
K1 W2 Mg1 O7 -118.9(3) 1_545 . . . ? 
O11 W2 Mg1 O10 -171.2(4) . . . . ? 
O2 W2 Mg1 O10 53.8(3) . . . . ? 
O5 W2 Mg1 O10 -58.3(3) . . . . ? 
O1 W2 Mg1 O10 156.2(5) . . . . ? 
K4 W2 Mg1 O10 -4.8(2) 2_656 . . . ? 
K5 W2 Mg1 O10 143.1(2) . . . . ? 
K3 W2 Mg1 O10 -99.9(2) 1_645 . . . ? 
K2 W2 Mg1 O10 -156.6(2) 1_655 . . . ? 
K3 W2 Mg1 O10 80.4(2) 1_545 . . . ? 
K1 W2 Mg1 O10 170.9(2) 2_655 . . . ? 
K1 W2 Mg1 O10 62.8(3) 1_545 . . . ? 
O11 W2 Mg1 K3 170.6(3) . . . 2_666 ? 
O2 W2 Mg1 K3 35.6(3) . . . 2_666 ? 
O5 W2 Mg1 K3 -76.5(3) . . . 2_666 ? 
O1 W2 Mg1 K3 138.0(4) . . . 2_666 ? 
K4 W2 Mg1 K3 -23.00(19) 2_656 . . 2_666 ? 
K5 W2 Mg1 K3 124.90(17) . . . 2_666 ? 
K3 W2 Mg1 K3 -118.05(15) 1_645 . . 2_666 ? 
K2 W2 Mg1 K3 -174.82(16) 1_655 . . 2_666 ? 
K3 W2 Mg1 K3 62.23(17) 1_545 . . 2_666 ? 
K1 W2 Mg1 K3 152.71(9) 2_655 . . 2_666 ? 
K1 W2 Mg1 K3 44.6(2) 1_545 . . 2_666 ? 
O11 W2 Mg1 K4 -46.6(3) . . . 1_655 ? 
O2 W2 Mg1 K4 178.4(2) . . . 1_655 ? 
O5 W2 Mg1 K4 66.3(2) . . . 1_655 ? 
O1 W2 Mg1 K4 -79.2(4) . . . 1_655 ? 
K4 W2 Mg1 K4 119.77(11) 2_656 . . 1_655 ? 
K5 W2 Mg1 K4 -92.33(12) . . . 1_655 ? 
K3 W2 Mg1 K4 24.72(15) 1_645 . . 1_655 ? 
K2 W2 Mg1 K4 -32.05(13) 1_655 . . 1_655 ? 
K3 W2 Mg1 K4 -155.00(13) 1_545 . . 1_655 ? 
K1 W2 Mg1 K4 -64.5(2) 2_655 . . 1_655 ? 
K1 W2 Mg1 K4 -172.58(8) 1_545 . . 1_655 ? 
O11 W2 Mg1 K4 48.7(4) . . . 2_666 ? 
O2 W2 Mg1 K4 -86.4(3) . . . 2_666 ? 
O5 W2 Mg1 K4 161.5(3) . . . 2_666 ? 
O1 W2 Mg1 K4 16.0(4) . . . 2_666 ? 
K4 W2 Mg1 K4 -144.98(18) 2_656 . . 2_666 ? 
K5 W2 Mg1 K4 2.91(18) . . . 2_666 ? 
K3 W2 Mg1 K4 119.96(19) 1_645 . . 2_666 ? 
K2 W2 Mg1 K4 63.2(2) 1_655 . . 2_666 ? 
K3 W2 Mg1 K4 -59.8(2) 1_545 . . 2_666 ? 
K1 W2 Mg1 K4 30.7(3) 2_655 . . 2_666 ? 
K1 W2 Mg1 K4 -77.3(2) 1_545 . . 2_666 ? 
O11 W2 O1 Mg1 -154.3(4) . . . . ? 
O2 W2 O1 Mg1 88.7(4) . . . . ? 
O5 W2 O1 Mg1 -39.2(5) . . . . ? 
K4 W2 O1 Mg1 27.2(5) 2_656 . . . ? 
K5 W2 O1 Mg1 162.9(5) . . . . ? 
K3 W2 O1 Mg1 -88.9(4) 1_645 . . . ? 
K2 W2 O1 Mg1 -129.3(4) 1_655 . . . ? 
K3 W2 O1 Mg1 99.6(3) 1_545 . . . ? 
K1 W2 O1 Mg1 -171.9(2) 2_655 . . . ? 
K1 W2 O1 Mg1 117.7(3) 1_545 . . . ? 
O11 W2 O1 K5 42.9(3) . . . . ? 
O2 W2 O1 K5 -74.2(3) . . . . ? 
O5 W2 O1 K5 158.0(2) . . . . ? 
Mg1 W2 O1 K5 -162.9(5) . . . . ? 
K4 W2 O1 K5 -135.64(16) 2_656 . . . ? 
K3 W2 O1 K5 108.22(16) 1_645 . . . ? 
K2 W2 O1 K5 67.80(15) 1_655 . . . ? 
K3 W2 O1 K5 -63.22(15) 1_545 . . . ? 
K1 W2 O1 K5 25.3(3) 2_655 . . . ? 
K1 W2 O1 K5 -45.2(3) 1_545 . . . ? 
O5 Mg1 O1 W2 54.8(8) 2_756 . . . ? 
O6 Mg1 O1 W2 -107.5(4) . . . . ? 
O7 Mg1 O1 W2 157.5(4) . . . . ? 
O10 Mg1 O1 W2 -20.1(4) . . . . ? 
K3 Mg1 O1 W2 -73.2(6) 2_666 . . . ? 
K4 Mg1 O1 W2 119.7(3) 1_655 . . . ? 
K4 Mg1 O1 W2 -170.1(2) 2_666 . . . ? 
O5 Mg1 O1 K5 -147.1(5) 2_756 . . . ? 
O6 Mg1 O1 K5 50.6(4) . . . . ? 
O7 Mg1 O1 K5 -44.4(4) . . . . ? 
O10 Mg1 O1 K5 138.0(4) . . . . ? 
W2 Mg1 O1 K5 158.1(6) . . . . ? 
K3 Mg1 O1 K5 84.9(5) 2_666 . . . ? 
K4 Mg1 O1 K5 -82.2(4) 1_655 . . . ? 
K4 Mg1 O1 K5 -12.0(4) 2_666 . . . ? 
O8 K5 O1 W2 -126.7(3) . . . . ? 
O8 K5 O1 W2 53.3(3) 2_655 . . . ? 
O1 K5 O1 W2 29(100) 2_655 . . . ? 
O9 K5 O1 W2 115.6(3) . . . . ? 
O9 K5 O1 W2 -64.4(3) 2_655 . . . ? 
O11 K5 O1 W2 154.1(2) 2_655 . . . ? 
O11 K5 O1 W2 -25.9(2) . . . . ? 
W2 K5 O1 W2 180.0 2_655 . . . ? 
K2 K5 O1 W2 104.3(2) . . . . ? 
K2 K5 O1 W2 -75.7(2) 1_655 . . . ? 
O8 K5 O1 Mg1 71.7(4) . . . . ? 
O8 K5 O1 Mg1 -108.3(4) 2_655 . . . ? 
O1 K5 O1 Mg1 -132(100) 2_655 . . . ? 
O9 K5 O1 Mg1 -45.9(3) . . . . ? 
O9 K5 O1 Mg1 134.1(3) 2_655 . . . ? 
O11 K5 O1 Mg1 -7.4(5) 2_655 . . . ? 
O11 K5 O1 Mg1 172.6(5) . . . . ? 
W2 K5 O1 Mg1 18.5(5) 2_655 . . . ? 
W2 K5 O1 Mg1 -161.5(5) . . . . ? 
K2 K5 O1 Mg1 -57.2(4) . . . . ? 
K2 K5 O1 Mg1 122.8(4) 1_655 . . . ? 
O11 W2 O2 K1 24.9(5) . . . 1_545 ? 
O5 W2 O2 K1 -91.3(4) . . . 1_545 ? 
O1 W2 O2 K1 137.5(3) . . . 1_545 ? 
Mg1 W2 O2 K1 168.8(3) . . . 1_545 ? 
K4 W2 O2 K1 -87.8(4) 2_656 . . 1_545 ? 
K5 W2 O2 K1 91.1(3) . . . 1_545 ? 
K3 W2 O2 K1 -45.4(5) 1_645 . . 1_545 ? 
K2 W2 O2 K1 48.8(6) 1_655 . . 1_545 ? 
K3 W2 O2 K1 119.0(5) 1_545 . . 1_545 ? 
K1 W2 O2 K1 13.4(3) 2_655 . . 1_545 ? 
O11 W2 O2 K3 -94.1(4) . . . 1_545 ? 
O5 W2 O2 K3 149.7(3) . . . 1_545 ? 
O1 W2 O2 K3 18.5(4) . . . 1_545 ? 
Mg1 W2 O2 K3 49.7(3) . . . 1_545 ? 
K4 W2 O2 K3 153.1(4) 2_656 . . 1_545 ? 
K5 W2 O2 K3 -28.0(3) . . . 1_545 ? 
K3 W2 O2 K3 -164.41(14) 1_645 . . 1_545 ? 
K2 W2 O2 K3 -70.2(5) 1_655 . . 1_545 ? 
K1 W2 O2 K3 -105.6(3) 2_655 . . 1_545 ? 
K1 W2 O2 K3 -119.0(5) 1_545 . . 1_545 ? 
O11 W2 O2 K4 112.7(3) . . . 2_656 ? 
O5 W2 O2 K4 -3.4(3) . . . 2_656 ? 
O1 W2 O2 K4 -134.6(2) . . . 2_656 ? 
Mg1 W2 O2 K4 -103.40(16) . . . 2_656 ? 
K5 W2 O2 K4 178.88(13) . . . 2_656 ? 
K3 W2 O2 K4 42.4(3) 1_645 . . 2_656 ? 
K2 W2 O2 K4 136.6(2) 1_655 . . 2_656 ? 
K3 W2 O2 K4 -153.1(4) 1_545 . . 2_656 ? 
K1 W2 O2 K4 101.27(15) 2_655 . . 2_656 ? 
K1 W2 O2 K4 87.8(4) 1_545 . . 2_656 ? 
O9 W3 O3 K4 140.9(3) . . . . ? 
O6 W3 O3 K4 -100.8(3) . . . . ? 
O10 W3 O3 K4 23.0(4) 2_656 . . . ? 
K3 W3 O3 K4 123.8(3) 1_545 . . . ? 
K4 W3 O3 K4 -106.4(4) 2_666 . . . ? 
K1 W3 O3 K4 147.0(5) . . . . ? 
K2 W3 O3 K4 113.4(3) . . . . ? 
K3 W3 O3 K4 -69.4(3) 2_666 . . . ? 
O9 W3 O3 K4 -112.7(3) . . . 2_666 ? 
O6 W3 O3 K4 5.7(4) . . . 2_666 ? 
O10 W3 O3 K4 129.4(3) 2_656 . . 2_666 ? 
K3 W3 O3 K4 -129.8(3) 1_545 . . 2_666 ? 
K4 W3 O3 K4 106.4(4) . . . 2_666 ? 
K1 W3 O3 K4 -106.6(4) . . . 2_666 ? 
K2 W3 O3 K4 -140.1(2) . . . 2_666 ? 
K3 W3 O3 K4 37.1(3) 2_666 . . 2_666 ? 
O9 W3 O3 K1 -6.1(4) . . . . ? 
O6 W3 O3 K1 112.3(3) . . . . ? 
O10 W3 O3 K1 -124.0(3) 2_656 . . . ? 
K3 W3 O3 K1 -23.1(6) 1_545 . . . ? 
K4 W3 O3 K1 106.6(4) 2_666 . . . ? 
K4 W3 O3 K1 -147.0(5) . . . . ? 
K2 W3 O3 K1 -33.5(3) . . . . ? 
K3 W3 O3 K1 143.7(3) 2_666 . . . ? 
O3 K4 O3 W3 119.7(4) 2_666 . . . ? 
O7 K4 O3 W3 -73.0(3) 1_455 . . . ? 
O7 K4 O3 W3 -165.6(6) 2_666 . . . ? 
O2 K4 O3 W3 38.5(3) 2_656 . . . ? 
O5 K4 O3 W3 -15.4(3) 2_656 . . . ? 
O4 K4 O3 W3 -129.2(4) 1_455 . . . ? 
O12 K4 O3 W3 51.3(5) 2_666 . . . ? 
W1 K4 O3 W3 -100.2(3) 1_455 . . . ? 
W2 K4 O3 W3 11.7(3) 2_656 . . . ? 
W1 K4 O3 W3 37.3(9) 2_666 . . . ? 
W3 K4 O3 W3 140.0(3) 2_666 . . . ? 
O3 K4 O3 K4 0.0 2_666 . . 2_666 ? 
O7 K4 O3 K4 167.3(2) 1_455 . . 2_666 ? 
O7 K4 O3 K4 74.7(8) 2_666 . . 2_666 ? 
O2 K4 O3 K4 -81.20(18) 2_656 . . 2_666 ? 
O5 K4 O3 K4 -135.05(19) 2_656 . . 2_666 ? 
O4 K4 O3 K4 111.1(2) 1_455 . . 2_666 ? 
O12 K4 O3 K4 -68.4(3) 2_666 . . 2_666 ? 
W1 K4 O3 K4 140.14(18) 1_455 . . 2_666 ? 
W2 K4 O3 K4 -107.99(15) 2_656 . . 2_666 ? 
W1 K4 O3 K4 -82.4(6) 2_666 . . 2_666 ? 
W3 K4 O3 K4 20.28(16) 2_666 . . 2_666 ? 
O3 K4 O3 K1 -88.2(2) 2_666 . . . ? 
O7 K4 O3 K1 79.0(2) 1_455 . . . ? 
O7 K4 O3 K1 -13.6(9) 2_666 . . . ? 
O2 K4 O3 K1 -169.4(2) 2_656 . . . ? 
O5 K4 O3 K1 136.7(2) 2_656 . . . ? 
O4 K4 O3 K1 22.84(19) 1_455 . . . ? 
O12 K4 O3 K1 -156.7(2) 2_666 . . . ? 
W1 K4 O3 K1 51.93(16) 1_455 . . . ? 
W2 K4 O3 K1 163.79(19) 2_656 . . . ? 
W1 K4 O3 K1 -170.7(5) 2_666 . . . ? 
W3 K4 O3 K1 -67.9(2) 2_666 . . . ? 
O11 K1 O3 W3 13.5(4) 2_655 . . . ? 
O12 K1 O3 W3 -75.7(4) . . . . ? 
O4 K1 O3 W3 124.8(4) 1_455 . . . ? 
O2 K1 O3 W3 -154.6(3) 1_565 . . . ? 
O12 K1 O3 W3 161(2) 2_665 . . . ? 
K1 K1 O3 W3 -81.3(4) 2_665 . . . ? 
W1 K1 O3 W3 100.5(3) 1_455 . . . ? 
K3 K1 O3 W3 160.6(3) . . . . ? 
K4 K1 O3 W3 -119.8(4) 2_666 . . . ? 
W1 K1 O3 W3 129.1(3) 2_665 . . . ? 
W2 K1 O3 W3 4.1(4) 2_655 . . . ? 
O11 K1 O3 K4 -137.4(2) 2_655 . . . ? 
O12 K1 O3 K4 133.4(3) . . . . ? 
O4 K1 O3 K4 -26.1(2) 1_455 . . . ? 
O2 K1 O3 K4 54.5(2) 1_565 . . . ? 
O12 K1 O3 K4 10(2) 2_665 . . . ? 
K1 K1 O3 K4 127.80(19) 2_665 . . . ? 
W1 K1 O3 K4 -50.45(16) 1_455 . . . ? 
K3 K1 O3 K4 9.7(2) . . . . ? 
K4 K1 O3 K4 89.3(2) 2_666 . . . ? 
W1 K1 O3 K4 -21.8(5) 2_665 . . . ? 
W2 K1 O3 K4 -146.79(14) 2_655 . . . ? 
O11 K1 O3 K4 133.3(2) 2_655 . . 2_666 ? 
O12 K1 O3 K4 44.0(2) . . . 2_666 ? 
O4 K1 O3 K4 -115.4(2) 1_455 . . 2_666 ? 
O2 K1 O3 K4 -34.82(18) 1_565 . . 2_666 ? 
O12 K1 O3 K4 -80(2) 2_665 . . 2_666 ? 
K1 K1 O3 K4 38.5(3) 2_665 . . 2_666 ? 
W1 K1 O3 K4 -139.79(16) 1_455 . . 2_666 ? 
K3 K1 O3 K4 -79.63(14) . . . 2_666 ? 
W1 K1 O3 K4 -111.1(3) 2_665 . . 2_666 ? 
W2 K1 O3 K4 123.87(13) 2_655 . . 2_666 ? 
O12 W1 O4 K3 10.5(6) . . . 1_655 ? 
O8 W1 O4 K3 131.0(5) . . . 1_655 ? 
O7 W1 O4 K3 -106.3(5) . . . 1_655 ? 
K4 W1 O4 K3 -106.0(5) 1_655 . . 1_655 ? 
K4 W1 O4 K3 -53.0(5) 2_666 . . 1_655 ? 
K1 W1 O4 K3 147.2(7) 1_655 . . 1_655 ? 
K5 W1 O4 K3 128.3(4) . . . 1_655 ? 
K3 W1 O4 K3 99.1(5) 2_665 . . 1_655 ? 
K1 W1 O4 K3 42.4(5) 2_665 . . 1_655 ? 
O12 W1 O4 K1 -136.7(4) . . . 1_655 ? 
O8 W1 O4 K1 -16.2(4) . . . 1_655 ? 
O7 W1 O4 K1 106.5(4) . . . 1_655 ? 
K4 W1 O4 K1 106.9(4) 1_655 . . 1_655 ? 
K4 W1 O4 K1 159.8(3) 2_666 . . 1_655 ? 
K5 W1 O4 K1 -18.9(7) . . . 1_655 ? 
K3 W1 O4 K1 -48.0(3) 2_665 . . 1_655 ? 
K1 W1 O4 K1 -104.8(3) 2_665 . . 1_655 ? 
K3 W1 O4 K1 -147.2(7) 1_655 . . 1_655 ? 
O12 W1 O4 K4 116.4(3) . . . 1_655 ? 
O8 W1 O4 K4 -123.1(3) . . . 1_655 ? 
O7 W1 O4 K4 -0.3(3) . . . 1_655 ? 
K4 W1 O4 K4 52.95(17) 2_666 . . 1_655 ? 
K1 W1 O4 K4 -106.9(4) 1_655 . . 1_655 ? 
K5 W1 O4 K4 -125.8(3) . . . 1_655 ? 
K3 W1 O4 K4 -154.89(13) 2_665 . . 1_655 ? 
K1 W1 O4 K4 148.34(15) 2_665 . . 1_655 ? 
K3 W1 O4 K4 106.0(5) 1_655 . . 1_655 ? 
O11 W2 O5 Mg1 134.6(5) . . . 2_756 ? 
O2 W2 O5 Mg1 -107.2(5) . . . 2_756 ? 
O1 W2 O5 Mg1 21.8(6) . . . 2_756 ? 
Mg1 W2 O5 Mg1 3.7(5) . . . 2_756 ? 
K4 W2 O5 Mg1 -110.7(5) 2_656 . . 2_756 ? 
K5 W2 O5 Mg1 66.9(7) . . . 2_756 ? 
K3 W2 O5 Mg1 121.8(6) 1_645 . . 2_756 ? 
K2 W2 O5 Mg1 95.0(5) 1_655 . . 2_756 ? 
K3 W2 O5 Mg1 -80.7(6) 1_545 . . 2_756 ? 
K1 W2 O5 Mg1 162.1(4) 2_655 . . 2_756 ? 
K1 W2 O5 Mg1 -140.7(4) 1_545 . . 2_756 ? 
O11 W2 O5 K3 12.9(4) . . . 1_645 ? 
O2 W2 O5 K3 131.0(3) . . . 1_645 ? 
O1 W2 O5 K3 -100.0(3) . . . 1_645 ? 
Mg1 W2 O5 K3 -118.1(2) . . . 1_645 ? 
K4 W2 O5 K3 127.6(3) 2_656 . . 1_645 ? 
K5 W2 O5 K3 -54.8(6) . . . 1_645 ? 
K2 W2 O5 K3 -26.7(2) 1_655 . . 1_645 ? 
K3 W2 O5 K3 157.54(12) 1_545 . . 1_645 ? 
K1 W2 O5 K3 40.4(3) 2_655 . . 1_645 ? 
K1 W2 O5 K3 97.6(2) 1_545 . . 1_645 ? 
O11 W2 O5 K4 -114.7(3) . . . 2_656 ? 
O2 W2 O5 K4 3.4(3) . . . 2_656 ? 
O1 W2 O5 K4 132.4(2) . . . 2_656 ? 
Mg1 W2 O5 K4 114.32(15) . . . 2_656 ? 
K5 W2 O5 K4 177.6(3) . . . 2_656 ? 
K3 W2 O5 K4 -127.6(3) 1_645 . . 2_656 ? 
K2 W2 O5 K4 -154.31(11) 1_655 . . 2_656 ? 
K3 W2 O5 K4 30.0(4) 1_545 . . 2_656 ? 
K1 W2 O5 K4 -87.22(15) 2_655 . . 2_656 ? 
K1 W2 O5 K4 -30.00(19) 1_545 . . 2_656 ? 
O3 W3 O6 Mg1 -94.7(6) . . . . ? 
O9 W3 O6 Mg1 22.8(6) . . . . ? 
O10 W3 O6 Mg1 144.2(5) 2_656 . . . ? 
K3 W3 O6 Mg1 63.6(5) 1_545 . . . ? 
K4 W3 O6 Mg1 -90.8(5) 2_666 . . . ? 
K4 W3 O6 Mg1 -133.2(5) . . . . ? 
K1 W3 O6 Mg1 -58.6(6) . . . . ? 
K2 W3 O6 Mg1 22.4(8) . . . . ? 
K3 W3 O6 Mg1 -168.7(9) 2_666 . . . ? 
O3 W3 O6 K3 73.9(4) . . . 2_666 ? 
O9 W3 O6 K3 -168.6(4) . . . 2_666 ? 
O10 W3 O6 K3 -47.1(5) 2_656 . . 2_666 ? 
K3 W3 O6 K3 -127.7(3) 1_545 . . 2_666 ? 
K4 W3 O6 K3 77.9(3) 2_666 . . 2_666 ? 
K4 W3 O6 K3 35.5(4) . . . 2_666 ? 
K1 W3 O6 K3 110.0(3) . . . 2_666 ? 
K2 W3 O6 K3 -168.92(11) . . . 2_666 ? 
O5 Mg1 O6 W3 157.9(5) 2_756 . . . ? 
O1 Mg1 O6 W3 -30.3(6) . . . . ? 
O7 Mg1 O6 W3 64.7(6) . . . . ? 
O10 Mg1 O6 W3 -112.0(6) . . . . ? 
W2 Mg1 O6 W3 -58.0(6) . . . . ? 
K3 Mg1 O6 W3 170.9(7) 2_666 . . . ? 
K4 Mg1 O6 W3 107.7(5) 1_655 . . . ? 
K4 Mg1 O6 W3 87.1(5) 2_666 . . . ? 
O5 Mg1 O6 K3 -13.0(3) 2_756 . . 2_666 ? 
O1 Mg1 O6 K3 158.8(2) . . . 2_666 ? 
O7 Mg1 O6 K3 -106.2(3) . . . 2_666 ? 
O10 Mg1 O6 K3 77.1(3) . . . 2_666 ? 
W2 Mg1 O6 K3 131.10(17) . . . 2_666 ? 
K4 Mg1 O6 K3 -63.2(2) 1_655 . . 2_666 ? 
K4 Mg1 O6 K3 -83.8(2) 2_666 . . 2_666 ? 
O4 W1 O7 Mg1 -131.0(6) . . . . ? 
O12 W1 O7 Mg1 113.2(6) . . . . ? 
O8 W1 O7 Mg1 -9.4(7) . . . . ? 
K4 W1 O7 Mg1 -131.3(7) 1_655 . . . ? 
K4 W1 O7 Mg1 143.1(7) 2_666 . . . ? 
K1 W1 O7 Mg1 -92.5(6) 1_655 . . . ? 
K5 W1 O7 Mg1 26.6(6) . . . . ? 
K3 W1 O7 Mg1 -1.8(9) 2_665 . . . ? 
K1 W1 O7 Mg1 120.1(5) 2_665 . . . ? 
K3 W1 O7 Mg1 -156.3(5) 1_655 . . . ? 
O4 W1 O7 K4 0.3(3) . . . 1_655 ? 
O12 W1 O7 K4 -115.4(3) . . . 1_655 ? 
O8 W1 O7 K4 122.0(3) . . . 1_655 ? 
K4 W1 O7 K4 -85.5(3) 2_666 . . 1_655 ? 
K1 W1 O7 K4 38.8(3) 1_655 . . 1_655 ? 
K5 W1 O7 K4 157.93(19) . . . 1_655 ? 
K3 W1 O7 K4 129.5(3) 2_665 . . 1_655 ? 
K1 W1 O7 K4 -108.5(3) 2_665 . . 1_655 ? 
K3 W1 O7 K4 -25.0(3) 1_655 . . 1_655 ? 
O4 W1 O7 K4 85.9(3) . . . 2_666 ? 
O12 W1 O7 K4 -29.9(4) . . . 2_666 ? 
O8 W1 O7 K4 -152.5(3) . . . 2_666 ? 
K4 W1 O7 K4 85.5(3) 1_655 . . 2_666 ? 
K1 W1 O7 K4 124.35(14) 1_655 . . 2_666 ? 
K5 W1 O7 K4 -116.53(18) . . . 2_666 ? 
K3 W1 O7 K4 -144.9(2) 2_665 . . 2_666 ? 
K1 W1 O7 K4 -23.0(5) 2_665 . . 2_666 ? 
K3 W1 O7 K4 60.6(2) 1_655 . . 2_666 ? 
O5 Mg1 O7 W1 150.2(6) 2_756 . . . ? 
O1 Mg1 O7 W1 -2.8(7) . . . . ? 
O6 Mg1 O7 W1 -112.0(6) . . . . ? 
O10 Mg1 O7 W1 26(5) . . . . ? 
W2 Mg1 O7 W1 8.2(7) . . . . ? 
K3 Mg1 O7 W1 -160.1(5) 2_666 . . . ? 
K4 Mg1 O7 W1 130.6(7) 1_655 . . . ? 
K4 Mg1 O7 W1 -140.5(8) 2_666 . . . ? 
O5 Mg1 O7 K4 19.6(3) 2_756 . . 1_655 ? 
O1 Mg1 O7 K4 -133.4(3) . . . 1_655 ? 
O6 Mg1 O7 K4 117.4(3) . . . 1_655 ? 
O10 Mg1 O7 K4 -105(4) . . . 1_655 ? 
W2 Mg1 O7 K4 -122.4(2) . . . 1_655 ? 
K3 Mg1 O7 K4 69.3(2) 2_666 . . 1_655 ? 
K4 Mg1 O7 K4 88.9(3) 2_666 . . 1_655 ? 
O5 Mg1 O7 K4 -69.3(3) 2_756 . . 2_666 ? 
O1 Mg1 O7 K4 137.7(3) . . . 2_666 ? 
O6 Mg1 O7 K4 28.5(3) . . . 2_666 ? 
O10 Mg1 O7 K4 166(4) . . . 2_666 ? 
W2 Mg1 O7 K4 148.77(18) . . . 2_666 ? 
K3 Mg1 O7 K4 -19.6(3) 2_666 . . 2_666 ? 
K4 Mg1 O7 K4 -88.9(3) 1_655 . . 2_666 ? 
O4 W1 O8 K3 -67.9(4) . . . 2_665 ? 
O12 W1 O8 K3 50.8(5) . . . 2_665 ? 
O7 W1 O8 K3 172.7(3) . . . 2_665 ? 
K4 W1 O8 K3 -131.0(2) 1_655 . . 2_665 ? 
K4 W1 O8 K3 120.6(4) 2_666 . . 2_665 ? 
K1 W1 O8 K3 -77.8(3) 1_655 . . 2_665 ? 
K5 W1 O8 K3 110.2(5) . . . 2_665 ? 
K1 W1 O8 K3 17.7(3) 2_665 . . 2_665 ? 
K3 W1 O8 K3 -45.5(4) 1_655 . . 2_665 ? 
O4 W1 O8 K5 -178.1(3) . . . . ? 
O12 W1 O8 K5 -59.3(4) . . . . ? 
O7 W1 O8 K5 62.5(4) . . . . ? 
K4 W1 O8 K5 118.8(2) 1_655 . . . ? 
K4 W1 O8 K5 10.4(7) 2_666 . . . ? 
K1 W1 O8 K5 172.0(3) 1_655 . . . ? 
K3 W1 O8 K5 -110.2(5) 2_665 . . . ? 
K1 W1 O8 K5 -92.5(3) 2_665 . . . ? 
K3 W1 O8 K5 -155.67(14) 1_655 . . . ? 
O4 W1 O8 K2 64.9(6) . . . 1_655 ? 
O12 W1 O8 K2 -176.3(5) . . . 1_655 ? 
O7 W1 O8 K2 -54.5(6) . . . 1_655 ? 
K4 W1 O8 K2 1.8(7) 1_655 . . 1_655 ? 
K4 W1 O8 K2 -106.6(5) 2_666 . . 1_655 ? 
K1 W1 O8 K2 55.0(5) 1_655 . . 1_655 ? 
K5 W1 O8 K2 -117.0(7) . . . 1_655 ? 
K3 W1 O8 K2 132.8(8) 2_665 . . 1_655 ? 
K1 W1 O8 K2 150.5(5) 2_665 . . 1_655 ? 
K3 W1 O8 K2 87.3(6) 1_655 . . 1_655 ? 
O8 K5 O8 W1 -125(100) 2_655 . . . ? 
O1 K5 O8 W1 107.4(3) 2_655 . . . ? 
O1 K5 O8 W1 -72.6(3) . . . . ? 
O9 K5 O8 W1 -10.0(4) . . . . ? 
O9 K5 O8 W1 170.0(4) 2_655 . . . ? 
O11 K5 O8 W1 57.5(3) 2_655 . . . ? 
O11 K5 O8 W1 -122.5(3) . . . . ? 
W2 K5 O8 W1 85.3(3) 2_655 . . . ? 
W2 K5 O8 W1 -94.7(3) . . . . ? 
K2 K5 O8 W1 33.7(4) . . . . ? 
K2 K5 O8 W1 -146.3(4) 1_655 . . . ? 
O8 K5 O8 K3 106(100) 2_655 . . 2_665 ? 
O1 K5 O8 K3 -21.6(2) 2_655 . . 2_665 ? 
O1 K5 O8 K3 158.4(2) . . . 2_665 ? 
O9 K5 O8 K3 -139.05(17) . . . 2_665 ? 
O9 K5 O8 K3 40.95(17) 2_655 . . 2_665 ? 
O11 K5 O8 K3 -71.5(2) 2_655 . . 2_665 ? 
O11 K5 O8 K3 108.5(2) . . . 2_665 ? 
W2 K5 O8 K3 -43.69(15) 2_655 . . 2_665 ? 
W2 K5 O8 K3 136.31(15) . . . 2_665 ? 
K2 K5 O8 K3 -95.33(18) . . . 2_665 ? 
K2 K5 O8 K3 84.67(18) 1_655 . . 2_665 ? 
O8 K5 O8 K2 22(100) 2_655 . . 1_655 ? 
O1 K5 O8 K2 -106.26(17) 2_655 . . 1_655 ? 
O1 K5 O8 K2 73.74(17) . . . 1_655 ? 
O9 K5 O8 K2 136.28(16) . . . 1_655 ? 
O9 K5 O8 K2 -43.72(16) 2_655 . . 1_655 ? 
O11 K5 O8 K2 -156.21(17) 2_655 . . 1_655 ? 
O11 K5 O8 K2 23.79(17) . . . 1_655 ? 
W2 K5 O8 K2 -128.36(13) 2_655 . . 1_655 ? 
W2 K5 O8 K2 51.64(13) . . . 1_655 ? 
K2 K5 O8 K2 180.0 . . . 1_655 ? 
O3 W3 O9 K2 -62.3(4) . . . . ? 
O6 W3 O9 K2 -179.6(4) . . . . ? 
O10 W3 O9 K2 56.1(5) 2_656 . . . ? 
K3 W3 O9 K2 104.4(5) 1_545 . . . ? 
K4 W3 O9 K2 -105.4(3) 2_666 . . . ? 
K4 W3 O9 K2 -31.3(5) . . . . ? 
K1 W3 O9 K2 -65.9(3) . . . . ? 
K3 W3 O9 K2 170.62(11) 2_666 . . . ? 
O3 W3 O9 K3 -166.7(3) . . . 1_545 ? 
O6 W3 O9 K3 76.0(3) . . . 1_545 ? 
O10 W3 O9 K3 -48.4(4) 2_656 . . 1_545 ? 
K4 W3 O9 K3 150.19(15) 2_666 . . 1_545 ? 
K4 W3 O9 K3 -135.74(17) . . . 1_545 ? 
K1 W3 O9 K3 -170.3(3) . . . 1_545 ? 
K2 W3 O9 K3 -104.4(5) . . . 1_545 ? 
K3 W3 O9 K3 66.2(4) 2_666 . . 1_545 ? 
O3 W3 O9 K5 79.0(5) . . . . ? 
O6 W3 O9 K5 -38.3(6) . . . . ? 
O10 W3 O9 K5 -162.7(5) 2_656 . . . ? 
K3 W3 O9 K5 -114.3(6) 1_545 . . . ? 
K4 W3 O9 K5 35.9(5) 2_666 . . . ? 
K4 W3 O9 K5 110.0(4) . . . . ? 
K1 W3 O9 K5 75.4(4) . . . . ? 
K2 W3 O9 K5 141.3(8) . . . . ? 
K3 W3 O9 K5 -48.1(7) 2_666 . . . ? 
O9 K2 O9 W3 -142(100) 2 . . . ? 
O11 K2 O9 W3 99.3(4) 2_655 . . . ? 
O11 K2 O9 W3 -80.7(4) 1_455 . . . ? 
O8 K2 O9 W3 20.9(4) 1_455 . . . ? 
O8 K2 O9 W3 -159.1(4) 2_655 . . . ? 
K3 K2 O9 W3 63.5(4) 2_565 . . . ? 
K3 K2 O9 W3 -116.5(4) 1_545 . . . ? 
W2 K2 O9 W3 118.1(4) 2_655 . . . ? 
W2 K2 O9 W3 -61.9(4) 1_455 . . . ? 
K5 K2 O9 W3 -23.6(5) 1_455 . . . ? 
K5 K2 O9 W3 156.4(5) . . . . ? 
O9 K2 O9 K3 -26(100) 2 . . 1_545 ? 
O11 K2 O9 K3 -144.1(2) 2_655 . . 1_545 ? 
O11 K2 O9 K3 35.9(2) 1_455 . . 1_545 ? 
O8 K2 O9 K3 137.38(18) 1_455 . . 1_545 ? 
O8 K2 O9 K3 -42.62(18) 2_655 . . 1_545 ? 
K3 K2 O9 K3 180.0 2_565 . . 1_545 ? 
W2 K2 O9 K3 -125.33(11) 2_655 . . 1_545 ? 
W2 K2 O9 K3 54.67(11) 1_455 . . 1_545 ? 
K5 K2 O9 K3 92.90(16) 1_455 . . 1_545 ? 
K5 K2 O9 K3 -87.10(16) . . . 1_545 ? 
O9 K2 O9 K5 61(100) 2 . . . ? 
O11 K2 O9 K5 -57.04(18) 2_655 . . . ? 
O11 K2 O9 K5 122.96(18) 1_455 . . . ? 
O8 K2 O9 K5 -135.52(17) 1_455 . . . ? 
O8 K2 O9 K5 44.48(17) 2_655 . . . ? 
K3 K2 O9 K5 -92.90(16) 2_565 . . . ? 
K3 K2 O9 K5 87.10(16) 1_545 . . . ? 
W2 K2 O9 K5 -38.24(13) 2_655 . . . ? 
W2 K2 O9 K5 141.76(13) 1_455 . . . ? 
K5 K2 O9 K5 180.0 1_455 . . . ? 
O8 K5 O9 W3 -16.9(5) . . . . ? 
O8 K5 O9 W3 163.1(5) 2_655 . . . ? 
O1 K5 O9 W3 -136.2(5) 2_655 . . . ? 
O1 K5 O9 W3 43.8(5) . . . . ? 
O9 K5 O9 W3 106(100) 2_655 . . . ? 
O11 K5 O9 W3 -104.5(5) 2_655 . . . ? 
O11 K5 O9 W3 75.5(5) . . . . ? 
W2 K5 O9 W3 -111.1(5) 2_655 . . . ? 
W2 K5 O9 W3 68.9(5) . . . . ? 
K2 K5 O9 W3 -150.7(6) . . . . ? 
K2 K5 O9 W3 29.3(6) 1_655 . . . ? 
O8 K5 O9 K2 133.81(18) . . . . ? 
O8 K5 O9 K2 -46.19(18) 2_655 . . . ? 
O1 K5 O9 K2 14.6(2) 2_655 . . . ? 
O1 K5 O9 K2 -165.4(2) . . . . ? 
O9 K5 O9 K2 -103(100) 2_655 . . . ? 
O11 K5 O9 K2 46.23(17) 2_655 . . . ? 
O11 K5 O9 K2 -133.77(17) . . . . ? 
W2 K5 O9 K2 39.67(14) 2_655 . . . ? 
W2 K5 O9 K2 -140.33(14) . . . . ? 
K2 K5 O9 K2 180.0 1_655 . . . ? 
O8 K5 O9 K3 -139.60(18) . . . 1_545 ? 
O8 K5 O9 K3 40.40(18) 2_655 . . 1_545 ? 
O1 K5 O9 K3 101.16(18) 2_655 . . 1_545 ? 
O1 K5 O9 K3 -78.84(18) . . . 1_545 ? 
O9 K5 O9 K3 -16(100) 2_655 . . 1_545 ? 
O11 K5 O9 K3 132.8(2) 2_655 . . 1_545 ? 
O11 K5 O9 K3 -47.2(2) . . . 1_545 ? 
W2 K5 O9 K3 126.26(12) 2_655 . . 1_545 ? 
W2 K5 O9 K3 -53.74(12) . . . 1_545 ? 
K2 K5 O9 K3 86.58(17) . . . 1_545 ? 
K2 K5 O9 K3 -93.42(17) 1_655 . . 1_545 ? 
O5 Mg1 O10 W3 95.9(5) 2_756 . . 2_656 ? 
O1 Mg1 O10 W3 -110.7(5) . . . 2_656 ? 
O6 Mg1 O10 W3 -1.7(5) . . . 2_656 ? 
O7 Mg1 O10 W3 -140(4) . . . 2_656 ? 
W2 Mg1 O10 W3 -121.1(5) . . . 2_656 ? 
K3 Mg1 O10 W3 46.3(4) 2_666 . . 2_656 ? 
K4 Mg1 O10 W3 120.4(4) 1_655 . . 2_656 ? 
K4 Mg1 O10 W3 25.3(7) 2_666 . . 2_656 ? 
O2 W2 O11 K1 -26.3(6) . . . 2_655 ? 
O5 W2 O11 K1 92.2(5) . . . 2_655 ? 
O1 W2 O11 K1 -145.4(5) . . . 2_655 ? 
Mg1 W2 O11 K1 -161.2(3) . . . 2_655 ? 
K4 W2 O11 K1 33.4(6) 2_656 . . 2_655 ? 
K5 W2 O11 K1 -111.5(5) . . . 2_655 ? 
K3 W2 O11 K1 102.3(5) 1_645 . . 2_655 ? 
K2 W2 O11 K1 175.6(8) 1_655 . . 2_655 ? 
K3 W2 O11 K1 -64.2(5) 1_545 . . 2_655 ? 
K1 W2 O11 K1 -13.4(4) 1_545 . . 2_655 ? 
O2 W2 O11 K2 158.1(3) . . . 1_655 ? 
O5 W2 O11 K2 -83.3(4) . . . 1_655 ? 
O1 W2 O11 K2 39.0(4) . . . 1_655 ? 
Mg1 W2 O11 K2 23.3(5) . . . 1_655 ? 
K4 W2 O11 K2 -142.1(2) 2_656 . . 1_655 ? 
K5 W2 O11 K2 73.0(3) . . . 1_655 ? 
K3 W2 O11 K2 -73.2(3) 1_645 . . 1_655 ? 
K3 W2 O11 K2 120.3(3) 1_545 . . 1_655 ? 
K1 W2 O11 K2 -175.6(8) 2_655 . . 1_655 ? 
K1 W2 O11 K2 171.1(3) 1_545 . . 1_655 ? 
O2 W2 O11 K3 -128.7(2) . . . 1_645 ? 
O5 W2 O11 K3 -10.1(3) . . . 1_645 ? 
O1 W2 O11 K3 112.2(2) . . . 1_645 ? 
Mg1 W2 O11 K3 96.5(2) . . . 1_645 ? 
K4 W2 O11 K3 -68.9(2) 2_656 . . 1_645 ? 
K5 W2 O11 K3 146.2(2) . . . 1_645 ? 
K2 W2 O11 K3 73.2(3) 1_655 . . 1_645 ? 
K3 W2 O11 K3 -166.47(8) 1_545 . . 1_645 ? 
K1 W2 O11 K3 -102.3(5) 2_655 . . 1_645 ? 
K1 W2 O11 K3 -115.69(16) 1_545 . . 1_645 ? 
O2 W2 O11 K5 85.2(3) . . . . ? 
O5 W2 O11 K5 -156.3(2) . . . . ? 
O1 W2 O11 K5 -33.9(2) . . . . ? 
Mg1 W2 O11 K5 -49.7(3) . . . . ? 
K4 W2 O11 K5 144.91(9) 2_656 . . . ? 
K3 W2 O11 K5 -146.2(2) 1_645 . . . ? 
K2 W2 O11 K5 -73.0(3) 1_655 . . . ? 
K3 W2 O11 K5 47.34(18) 1_545 . . . ? 
K1 W2 O11 K5 111.5(5) 2_655 . . . ? 
K1 W2 O11 K5 98.11(12) 1_545 . . . ? 
O8 K5 O11 W2 93.4(3) . . . . ? 
O8 K5 O11 W2 -86.6(3) 2_655 . . . ? 
O1 K5 O11 W2 -154.0(2) 2_655 . . . ? 
O1 K5 O11 W2 26.0(2) . . . . ? 
O9 K5 O11 W2 -14.1(3) . . . . ? 
O9 K5 O11 W2 165.9(3) 2_655 . . . ? 
O11 K5 O11 W2 -99(100) 2_655 . . . ? 
W2 K5 O11 W2 180.000(1) 2_655 . . . ? 
K2 K5 O11 W2 -61.2(3) . . . . ? 
K2 K5 O11 W2 118.8(3) 1_655 . . . ? 
O8 K5 O11 K1 -129.2(3) . . . 2_655 ? 
O8 K5 O11 K1 50.8(3) 2_655 . . 2_655 ? 
O1 K5 O11 K1 -16.7(3) 2_655 . . 2_655 ? 
O1 K5 O11 K1 163.3(3) . . . 2_655 ? 
O9 K5 O11 K1 123.2(2) . . . 2_655 ? 
O9 K5 O11 K1 -56.8(2) 2_655 . . 2_655 ? 
O11 K5 O11 K1 38(100) 2_655 . . 2_655 ? 
W2 K5 O11 K1 -42.7(4) 2_655 . . 2_655 ? 
W2 K5 O11 K1 137.3(4) . . . 2_655 ? 
K2 K5 O11 K1 76.1(3) . . . 2_655 ? 
K2 K5 O11 K1 -103.9(3) 1_655 . . 2_655 ? 
O8 K5 O11 K2 -25.31(18) . . . 1_655 ? 
O8 K5 O11 K2 154.69(18) 2_655 . . 1_655 ? 
O1 K5 O11 K2 87.2(2) 2_655 . . 1_655 ? 
O1 K5 O11 K2 -92.8(2) . . . 1_655 ? 
O9 K5 O11 K2 -132.85(17) . . . 1_655 ? 
O9 K5 O11 K2 47.15(17) 2_655 . . 1_655 ? 
O11 K5 O11 K2 142(100) 2_655 . . 1_655 ? 
W2 K5 O11 K2 61.2(3) 2_655 . . 1_655 ? 
W2 K5 O11 K2 -118.8(3) . . . 1_655 ? 
K2 K5 O11 K2 180.0 . . . 1_655 ? 
O8 K5 O11 K3 9.8(4) . . . 1_645 ? 
O8 K5 O11 K3 -170.2(4) 2_655 . . 1_645 ? 
O1 K5 O11 K3 122.4(4) 2_655 . . 1_645 ? 
O1 K5 O11 K3 -57.6(4) . . . 1_645 ? 
O9 K5 O11 K3 -97.7(4) . . . 1_645 ? 
O9 K5 O11 K3 82.3(4) 2_655 . . 1_645 ? 
O11 K5 O11 K3 177(100) 2_655 . . 1_645 ? 
W2 K5 O11 K3 96.4(5) 2_655 . . 1_645 ? 
W2 K5 O11 K3 -83.6(5) . . . 1_645 ? 
K2 K5 O11 K3 -144.9(3) . . . 1_645 ? 
K2 K5 O11 K3 35.1(3) 1_655 . . 1_645 ? 
O4 W1 O12 K1 -158.7(7) . . . . ? 
O8 W1 O12 K1 80.6(8) . . . . ? 
O7 W1 O12 K1 -43.3(9) . . . . ? 
K4 W1 O12 K1 -97.7(8) 1_655 . . . ? 
K4 W1 O12 K1 -69.9(7) 2_666 . . . ? 
K1 W1 O12 K1 168.6(6) 1_655 . . . ? 
K5 W1 O12 K1 45.8(8) . . . . ? 
K3 W1 O12 K1 106.7(8) 2_665 . . . ? 
K1 W1 O12 K1 142.8(10) 2_665 . . . ? 
K3 W1 O12 K1 -154.4(8) 1_655 . . . ? 
O4 W1 O12 K1 58.5(4) . . . 2_665 ? 
O8 W1 O12 K1 -62.2(5) . . . 2_665 ? 
O7 W1 O12 K1 173.9(4) . . . 2_665 ? 
K4 W1 O12 K1 119.5(3) 1_655 . . 2_665 ? 
K4 W1 O12 K1 147.3(5) 2_666 . . 2_665 ? 
K1 W1 O12 K1 25.8(5) 1_655 . . 2_665 ? 
K5 W1 O12 K1 -97.0(3) . . . 2_665 ? 
K3 W1 O12 K1 -36.1(3) 2_665 . . 2_665 ? 
K3 W1 O12 K1 62.8(3) 1_655 . . 2_665 ? 
O4 W1 O12 K4 -88.8(3) . . . 2_666 ? 
O8 W1 O12 K4 150.4(3) . . . 2_666 ? 
O7 W1 O12 K4 26.6(3) . . . 2_666 ? 
K4 W1 O12 K4 -27.9(3) 1_655 . . 2_666 ? 
K1 W1 O12 K4 -121.56(19) 1_655 . . 2_666 ? 
K5 W1 O12 K4 115.67(15) . . . 2_666 ? 
K3 W1 O12 K4 176.54(16) 2_665 . . 2_666 ? 
K1 W1 O12 K4 -147.3(5) 2_665 . . 2_666 ? 
K3 W1 O12 K4 -84.51(14) 1_655 . . 2_666 ? 
O11 K1 O12 W1 -71.1(8) 2_655 . . . ? 
O4 K1 O12 W1 85.2(10) 1_455 . . . ? 
O2 K1 O12 W1 123.8(8) 1_565 . . . ? 
O3 K1 O12 W1 36.6(8) . . . . ? 
O12 K1 O12 W1 -148.2(9) 2_665 . . . ? 
K1 K1 O12 W1 -148.2(9) 2_665 . . . ? 
W1 K1 O12 W1 26.0(12) 1_455 . . . ? 
K3 K1 O12 W1 133.7(7) . . . . ? 
K4 K1 O12 W1 72.2(8) 2_666 . . . ? 
W1 K1 O12 W1 -155.6(7) 2_665 . . . ? 
W2 K1 O12 W1 -86.9(8) 2_655 . . . ? 
O11 K1 O12 K1 77.1(2) 2_655 . . 2_665 ? 
O4 K1 O12 K1 -126.6(5) 1_455 . . 2_665 ? 
O2 K1 O12 K1 -88.0(2) 1_565 . . 2_665 ? 
O3 K1 O12 K1 -175.2(2) . . . 2_665 ? 
O12 K1 O12 K1 0.0 2_665 . . 2_665 ? 
W1 K1 O12 K1 174.2(4) 1_455 . . 2_665 ? 
K3 K1 O12 K1 -78.1(2) . . . 2_665 ? 
K4 K1 O12 K1 -139.5(3) 2_666 . . 2_665 ? 
W1 K1 O12 K1 -7.4(2) 2_665 . . 2_665 ? 
W2 K1 O12 K1 61.31(14) 2_655 . . 2_665 ? 
O11 K1 O12 K4 -143.4(2) 2_655 . . 2_666 ? 
O4 K1 O12 K4 13.0(6) 1_455 . . 2_666 ? 
O2 K1 O12 K4 51.54(17) 1_565 . . 2_666 ? 
O3 K1 O12 K4 -35.69(18) . . . 2_666 ? 
O12 K1 O12 K4 139.5(3) 2_665 . . 2_666 ? 
K1 K1 O12 K4 139.5(3) 2_665 . . 2_666 ? 
W1 K1 O12 K4 -46.3(6) 1_455 . . 2_666 ? 
K3 K1 O12 K4 61.4(2) . . . 2_666 ? 
W1 K1 O12 K4 132.17(11) 2_665 . . 2_666 ? 
W2 K1 O12 K4 -159.16(14) 2_655 . . 2_666 ? 
 
_diffrn_measured_fraction_theta_max    0.985 
_diffrn_reflns_theta_full              27.59 
_diffrn_measured_fraction_theta_full   0.985 
_refine_diff_density_max    2.109 
_refine_diff_density_min   -2.444 
_refine_diff_density_rms    0.316 
