# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2016

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_4
_database_code_depnum_ccdc_archive 'CCDC 1439435'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C48.50 H95 Cl16 N4 O12.50 Pt9 Sn7'
_chemical_formula_weight         4088.12

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 2/c'
_space_group_name_Hall           '-C 2yc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   44.6369(16)
_cell_length_b                   13.2659(4)
_cell_length_c                   31.3491(10)
_cell_angle_alpha                90
_cell_angle_beta                 96.774(2)
_cell_angle_gamma                90
_cell_volume                     18433.7(10)
_cell_formula_units_Z            8
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9868
_cell_measurement_theta_min      2.3545
_cell_measurement_theta_max      28.1935

_exptl_crystal_description       prism
_exptl_crystal_colour            black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.946
_exptl_crystal_F_000             14704
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.210
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.130
_exptl_absorpt_coefficient_mu    15.967
_shelx_estimated_absorpt_T_min   0.134
_shelx_estimated_absorpt_T_max   0.231
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.1344
_exptl_absorpt_correction_T_max  0.2307
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1660 (selected reflections only, before parameter refinement)
 R(int) = 0.0686 (selected reflections only, after parameter refinement)
;
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            141262
_diffrn_reflns_av_unetI/netI     0.0511
_diffrn_reflns_av_R_equivalents  0.0808
_diffrn_reflns_limit_h_min       -56
_diffrn_reflns_limit_h_max       56
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_l_min       -40
_diffrn_reflns_limit_l_max       40
_diffrn_reflns_theta_min         1.308
_diffrn_reflns_theta_max         27.000
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             20115
_reflns_number_gt                15054
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
 The asymmetric unit of the unit cell contains one cluster 
 anion, four [NEt4]+ cations and two CH3COCH3 molecules 
 (all located on general positions) as well as half of a
  CH3COCH3 molecule equally disordered over two symmetry 
 related (by 2) positions.
;

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0301P)²+664.4301P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         20115
_refine_ls_number_parameters     824
_refine_ls_number_restraints     232
_refine_ls_R_factor_all          0.0683
_refine_ls_R_factor_gt           0.0417
_refine_ls_wR_factor_ref         0.1032
_refine_ls_wR_factor_gt          0.0887
_refine_ls_goodness_of_fit_ref   1.071
_refine_ls_restrained_S_all      1.068
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.14924(2) 0.67771(3) 0.22662(2) 0.02395(10) Uani 1 1 d . . . . .
Pt2 Pt 0.09084(2) 0.56610(3) 0.20286(2) 0.02583(10) Uani 1 1 d . . . . .
Pt3 Pt 0.09617(2) 0.78265(3) 0.23762(2) 0.02294(10) Uani 1 1 d . . . . .
Pt4 Pt 0.08569(2) 0.68460(3) 0.06836(2) 0.02841(11) Uani 1 1 d . . . . .
Pt5 Pt 0.09245(2) 0.90054(3) 0.10174(2) 0.02239(10) Uani 1 1 d . . . . .
Pt6 Pt 0.14593(2) 0.79966(3) 0.09162(2) 0.02445(10) Uani 1 1 d . . . . .
Pt7 Pt 0.07452(2) 0.73368(3) 0.15147(2) 0.02235(10) Uani 1 1 d . . . . .
Pt8 Pt 0.12664(2) 0.63381(3) 0.13931(2) 0.02383(10) Uani 1 1 d . . . . .
Pt9 Pt 0.12824(2) 0.82352(3) 0.17089(2) 0.02154(9) Uani 1 1 d . . . . .
Sn1 Sn 0.18116(2) 0.73070(6) 0.16176(2) 0.02616(17) Uani 1 1 d . . . . .
Sn2 Sn 0.07138(2) 0.53909(6) 0.12038(2) 0.02609(18) Uani 1 1 d . . . . .
Sn3 Sn 0.07804(2) 0.93124(5) 0.18175(2) 0.02209(16) Uani 1 1 d . . . . .
Sn4 Sn 0.10998(2) 0.60674(6) 0.28531(2) 0.02653(18) Uani 1 1 d . . . . .
Sn5 Sn 0.10049(2) 0.83703(6) 0.01990(2) 0.02594(17) Uani 1 1 d . . . . .
Sn6 Sn 0.14535(2) 0.99892(6) 0.10220(3) 0.02814(18) Uani 1 1 d . . . . .
Sn7 Sn 0.14996(2) 0.84497(6) 0.27588(2) 0.02849(18) Uani 1 1 d . . . . .
Cl1 Cl 0.22132(7) 0.8448(2) 0.18614(11) 0.0376(7) Uani 1 1 d . . . . .
Cl2 Cl 0.21665(8) 0.6028(3) 0.14560(11) 0.0425(8) Uani 1 1 d . . . . .
Cl3 Cl 0.08338(8) 0.3736(2) 0.09845(10) 0.0402(8) Uani 1 1 d . . . . .
Cl4 Cl 0.01852(7) 0.5078(2) 0.10237(10) 0.0378(7) Uani 1 1 d . . . . .
Cl5 Cl 0.09249(7) 1.0965(2) 0.20681(10) 0.0339(7) Uani 1 1 d . . . . .
Cl6 Cl 0.02535(7) 0.9684(2) 0.17802(10) 0.0319(6) Uani 1 1 d . . . . .
Cl7 Cl 0.13686(9) 0.6929(3) 0.34704(12) 0.0491(9) Uani 1 1 d . . . . .
Cl8 Cl 0.06650(8) 0.5869(2) 0.32232(10) 0.0401(8) Uani 1 1 d . . . . .
Cl9 Cl 0.13169(8) 0.4483(2) 0.31045(10) 0.0372(7) Uani 1 1 d . . . . .
Cl10 Cl 0.12042(8) 0.7488(2) -0.03716(9) 0.0354(7) Uani 1 1 d . . . . .
Cl11 Cl 0.05222(7) 0.8736(2) -0.02144(9) 0.0316(7) Uani 1 1 d . . . . .
Cl12 Cl 0.12316(7) 0.9949(2) -0.00069(9) 0.0328(7) Uani 1 1 d . . . . .
Cl13 Cl 0.19387(8) 1.0419(3) 0.08348(11) 0.0462(8) Uani 1 1 d . . . . .
Cl14 Cl 0.12796(8) 1.1669(2) 0.09512(10) 0.0398(8) Uani 1 1 d . . . . .
Cl15 Cl 0.20075(7) 0.8424(3) 0.30965(10) 0.0380(7) Uani 1 1 d . . . . .
Cl16 Cl 0.13438(7) 0.9665(2) 0.32463(9) 0.0348(7) Uani 1 1 d . . . . .
C1 C 0.1781(3) 0.5862(9) 0.2525(4) 0.032(3) Uani 1 1 d . . . . .
C2 C 0.0788(3) 0.4392(9) 0.2186(4) 0.035(3) Uani 1 1 d . . . . .
C3 C 0.0679(3) 0.8159(9) 0.2744(4) 0.029(3) Uani 1 1 d . . . . .
C4 C 0.0685(3) 0.6171(9) 0.0194(4) 0.034(3) Uani 1 1 d . . . . .
C5 C 0.0640(3) 0.9991(9) 0.0811(4) 0.032(3) Uani 1 1 d . . . . .
C6 C 0.1747(3) 0.7842(9) 0.0531(4) 0.030(3) Uani 1 1 d . . . . .
C7 C 0.0317(3) 0.7343(9) 0.1487(4) 0.028(3) Uani 1 1 d . . . . .
C8 C 0.1457(3) 0.5205(10) 0.1170(4) 0.036(3) Uani 1 1 d . . . . .
C9 C 0.1522(3) 0.9459(9) 0.1938(4) 0.029(3) Uani 1 1 d . . . . .
O1 O 0.1955(2) 0.5326(7) 0.2685(3) 0.042(2) Uani 1 1 d . . . . .
O2 O 0.0707(2) 0.3609(7) 0.2276(3) 0.052(3) Uani 1 1 d . . . . .
O3 O 0.0509(2) 0.8413(7) 0.2973(3) 0.048(3) Uani 1 1 d . . . . .
O4 O 0.0580(3) 0.5705(7) -0.0087(3) 0.058(3) Uani 1 1 d . . . . .
O5 O 0.0473(2) 1.0612(7) 0.0697(3) 0.038(2) Uani 1 1 d . . . . .
O6 O 0.1930(3) 0.7788(9) 0.0324(3) 0.056(3) Uani 1 1 d . . . . .
O7 O 0.0069(2) 0.7354(6) 0.1471(3) 0.039(2) Uani 1 1 d . . . . .
O8 O 0.1569(2) 0.4530(7) 0.1036(4) 0.053(3) Uani 1 1 d . . . . .
O9 O 0.16086(18) 0.9609(6) 0.2337(2) 0.0255(17) Uani 1 1 d . . . . .
O10 O 0.15985(19) 1.0158(6) 0.1676(3) 0.0300(19) Uani 1 1 d . . . . .
N1 N 0.0438(2) 0.2271(7) 0.3430(3) 0.025(2) Uani 1 1 d . U . . .
C101 C 0.0467(3) 0.3395(8) 0.3481(4) 0.030(3) Uani 1 1 d . U . . .
H10A H 0.0281 0.3712 0.3338 0.036 Uiso 1 1 calc R U . . .
H10B H 0.0637 0.3626 0.3330 0.036 Uiso 1 1 calc R U . . .
C102 C 0.0519(3) 0.3771(9) 0.3944(4) 0.036(3) Uani 1 1 d . U . . .
H10C H 0.0534 0.4507 0.3945 0.053 Uiso 1 1 calc R U . . .
H10D H 0.0349 0.3566 0.4096 0.053 Uiso 1 1 calc R U . . .
H10E H 0.0706 0.3480 0.4087 0.053 Uiso 1 1 calc R U . . .
C103 C 0.0175(3) 0.1902(9) 0.3641(4) 0.033(3) Uani 1 1 d . U . . .
H10F H 0.0217 0.2028 0.3954 0.039 Uiso 1 1 calc R U . . .
H10G H 0.0159 0.1163 0.3600 0.039 Uiso 1 1 calc R U . . .
C104 C -0.0132(3) 0.2369(11) 0.3482(5) 0.048(4) Uani 1 1 d . U . . .
H10H H -0.0287 0.2076 0.3641 0.072 Uiso 1 1 calc R U . . .
H10I H -0.0123 0.3099 0.3530 0.072 Uiso 1 1 calc R U . . .
H10J H -0.0181 0.2231 0.3175 0.072 Uiso 1 1 calc R U . . .
C105 C 0.0402(3) 0.2079(9) 0.2951(3) 0.034(3) Uani 1 1 d . U . . .
H10K H 0.0575 0.2387 0.2828 0.040 Uiso 1 1 calc R U . . .
H10L H 0.0216 0.2419 0.2821 0.040 Uiso 1 1 calc R U . . .
C106 C 0.0384(3) 0.0962(10) 0.2828(4) 0.043(3) Uani 1 1 d . U . . .
H10M H 0.0361 0.0898 0.2515 0.064 Uiso 1 1 calc R U . . .
H10N H 0.0570 0.0621 0.2949 0.064 Uiso 1 1 calc R U . . .
H10O H 0.0211 0.0653 0.2942 0.064 Uiso 1 1 calc R U . . .
C107 C 0.0717(3) 0.1739(8) 0.3650(4) 0.030(3) Uani 1 1 d . U . . .
H10P H 0.0688 0.1002 0.3614 0.036 Uiso 1 1 calc R U . . .
H10Q H 0.0735 0.1889 0.3961 0.036 Uiso 1 1 calc R U . . .
C108 C 0.1011(3) 0.2033(10) 0.3480(4) 0.039(3) Uani 1 1 d . U . . .
H10R H 0.1179 0.1659 0.3638 0.058 Uiso 1 1 calc R U . . .
H10S H 0.0999 0.1870 0.3174 0.058 Uiso 1 1 calc R U . . .
H10T H 0.1045 0.2758 0.3521 0.058 Uiso 1 1 calc R U . . .
N2 N 0.9456(2) 0.7649(7) 0.0417(3) 0.031(2) Uani 1 1 d . U . . .
C201 C 0.9186(3) 0.7554(10) 0.0067(4) 0.043(3) Uani 1 1 d . U . . .
H20A H 0.9072 0.8196 0.0052 0.051 Uiso 1 1 calc R U . . .
H20B H 0.9263 0.7454 -0.0213 0.051 Uiso 1 1 calc R U . . .
C202 C 0.8974(4) 0.6718(13) 0.0134(6) 0.062(5) Uani 1 1 d . U . . .
H20C H 0.8809 0.6712 -0.0103 0.093 Uiso 1 1 calc R U . . .
H20D H 0.9082 0.6074 0.0141 0.093 Uiso 1 1 calc R U . . .
H20E H 0.8891 0.6818 0.0406 0.093 Uiso 1 1 calc R U . . .
C203 C 0.9659(3) 0.6729(10) 0.0429(4) 0.041(3) Uani 1 1 d . U . . .
H20F H 0.9820 0.6803 0.0673 0.050 Uiso 1 1 calc R U . . .
H20G H 0.9538 0.6129 0.0487 0.050 Uiso 1 1 calc R U . . .
C204 C 0.9804(4) 0.6539(12) 0.0028(5) 0.057(4) Uani 1 1 d . U . . .
H20H H 0.9930 0.5933 0.0066 0.086 Uiso 1 1 calc R U . . .
H20I H 0.9647 0.6442 -0.0215 0.086 Uiso 1 1 calc R U . . .
H20J H 0.9930 0.7118 -0.0029 0.086 Uiso 1 1 calc R U . . .
C205 C 0.9620(3) 0.8576(9) 0.0303(4) 0.041(3) Uani 1 1 d . U . . .
H20K H 0.9478 0.9152 0.0291 0.049 Uiso 1 1 calc R U . . .
H20L H 0.9679 0.8487 0.0011 0.049 Uiso 1 1 calc R U . . .
C206 C 0.9899(4) 0.8849(11) 0.0603(5) 0.053(4) Uani 1 1 d . U . . .
H20M H 0.9989 0.9464 0.0501 0.080 Uiso 1 1 calc R U . . .
H20N H 0.9843 0.8963 0.0892 0.080 Uiso 1 1 calc R U . . .
H20O H 1.0045 0.8296 0.0611 0.080 Uiso 1 1 calc R U . . .
C207 C 0.9356(3) 0.7736(10) 0.0859(4) 0.038(3) Uani 1 1 d . U . . .
H20P H 0.9250 0.7108 0.0921 0.046 Uiso 1 1 calc R U . . .
H20Q H 0.9538 0.7789 0.1072 0.046 Uiso 1 1 calc R U . . .
C208 C 0.9155(4) 0.8609(13) 0.0921(4) 0.054(4) Uani 1 1 d . U . . .
H20R H 0.9102 0.8605 0.1215 0.080 Uiso 1 1 calc R U . . .
H20S H 0.9259 0.9239 0.0869 0.080 Uiso 1 1 calc R U . . .
H20T H 0.8970 0.8556 0.0718 0.080 Uiso 1 1 calc R U . . .
N3 N 0.2176(3) 0.9707(9) 0.4430(3) 0.043(3) Uani 1 1 d . U . . .
C301 C 0.1963(4) 0.9017(12) 0.4629(5) 0.053(4) Uani 1 1 d . U . . .
H30A H 0.1822 0.9435 0.4775 0.063 Uiso 1 1 calc R U . . .
H30B H 0.2082 0.8603 0.4851 0.063 Uiso 1 1 calc R U . . .
C302 C 0.1778(5) 0.8309(14) 0.4313(6) 0.076(6) Uani 1 1 d . U . . .
H30C H 0.1646 0.7891 0.4470 0.114 Uiso 1 1 calc R U . . .
H30D H 0.1654 0.8709 0.4096 0.114 Uiso 1 1 calc DR U . . .
H30E H 0.1914 0.7876 0.4172 0.114 Uiso 1 1 calc R U . . .
C303 C 0.2406(3) 0.9097(12) 0.4223(4) 0.048(4) Uani 1 1 d . U . . .
H30F H 0.2546 0.9571 0.4105 0.057 Uiso 1 1 calc R U . . .
H30G H 0.2299 0.8720 0.3979 0.057 Uiso 1 1 calc R U . . .
C304 C 0.2594(4) 0.8341(14) 0.4516(5) 0.067(5) Uani 1 1 d . U . . .
H30H H 0.2735 0.7989 0.4350 0.101 Uiso 1 1 calc R U . . .
H30I H 0.2708 0.8704 0.4755 0.101 Uiso 1 1 calc R U . . .
H30J H 0.2460 0.7851 0.4629 0.101 Uiso 1 1 calc R U . . .
C305 C 0.2296(4) 1.0406(14) 0.4767(5) 0.069(5) Uani 1 1 d . U . . .
H30K H 0.2401 1.0007 0.5008 0.083 Uiso 1 1 calc DR U . . .
H30L H 0.2124 1.0751 0.4877 0.083 Uiso 1 1 calc DR U . . .
C306 C 0.2520(5) 1.1230(17) 0.4642(7) 0.098(7) Uani 1 1 d . U . . .
H30M H 0.2585 1.1651 0.4893 0.148 Uiso 1 1 calc R U . . .
H30N H 0.2696 1.0905 0.4542 0.148 Uiso 1 1 calc R U . . .
H30O H 0.2419 1.1651 0.4411 0.148 Uiso 1 1 calc R U . . .
C307 C 0.2008(3) 1.0346(11) 0.4067(4) 0.044(3) Uani 1 1 d . U . . .
H30P H 0.2156 1.0764 0.3936 0.053 Uiso 1 1 calc R U . . .
H30Q H 0.1911 0.9888 0.3842 0.053 Uiso 1 1 calc R U . . .
C308 C 0.1773(4) 1.1016(13) 0.4211(5) 0.059(4) Uani 1 1 d . U . . .
H30R H 0.1676 1.1398 0.3965 0.089 Uiso 1 1 calc R U . . .
H30S H 0.1622 1.0608 0.4334 0.089 Uiso 1 1 calc DR U . . .
H30T H 0.1867 1.1485 0.4429 0.089 Uiso 1 1 calc R U . . .
N4 N 0.1964(2) 0.2447(7) 0.2261(3) 0.032(2) Uani 1 1 d . U . . .
C401 C 0.2104(3) 0.1406(9) 0.2218(4) 0.033(3) Uani 1 1 d . U . . .
H40A H 0.1975 0.0902 0.2342 0.039 Uiso 1 1 calc R U . . .
H40B H 0.2100 0.1249 0.1908 0.039 Uiso 1 1 calc R U . . .
C402 C 0.2420(3) 0.1288(11) 0.2428(5) 0.053(4) Uani 1 1 d . U . . .
H40C H 0.2489 0.0599 0.2384 0.080 Uiso 1 1 calc R U . . .
H40D H 0.2551 0.1768 0.2303 0.080 Uiso 1 1 calc R U . . .
H40E H 0.2426 0.1419 0.2737 0.080 Uiso 1 1 calc R U . . .
C403 C 0.2148(3) 0.3258(10) 0.2085(4) 0.037(3) Uani 1 1 d . U . . .
H40F H 0.2349 0.3270 0.2256 0.045 Uiso 1 1 calc R U . . .
H40G H 0.2050 0.3914 0.2128 0.045 Uiso 1 1 calc R U . . .
C404 C 0.2192(4) 0.3163(12) 0.1616(5) 0.051(4) Uani 1 1 d . U . . .
H40H H 0.2314 0.3728 0.1534 0.077 Uiso 1 1 calc R U . . .
H40I H 0.2295 0.2527 0.1570 0.077 Uiso 1 1 calc R U . . .
H40J H 0.1995 0.3173 0.1441 0.077 Uiso 1 1 calc R U . . .
C405 C 0.1652(3) 0.2408(10) 0.2015(5) 0.040(3) Uani 1 1 d . U . . .
H40K H 0.1673 0.2258 0.1711 0.048 Uiso 1 1 calc R U . . .
H40L H 0.1542 0.1837 0.2128 0.048 Uiso 1 1 calc R U . . .
C406 C 0.1460(4) 0.3334(11) 0.2028(5) 0.051(4) Uani 1 1 d . U . . .
H40M H 0.1264 0.3219 0.1858 0.076 Uiso 1 1 calc R U . . .
H40N H 0.1430 0.3483 0.2326 0.076 Uiso 1 1 calc R U . . .
H40O H 0.1561 0.3906 0.1907 0.076 Uiso 1 1 calc R U . . .
C407 C 0.1943(3) 0.2689(11) 0.2726(4) 0.044(3) Uani 1 1 d . U . . .
H40P H 0.1843 0.3352 0.2740 0.053 Uiso 1 1 calc R U . . .
H40Q H 0.2151 0.2759 0.2874 0.053 Uiso 1 1 calc R U . . .
C408 C 0.1774(4) 0.1926(11) 0.2973(5) 0.055(4) Uani 1 1 d . U . . .
H40R H 0.1774 0.2156 0.3270 0.083 Uiso 1 1 calc R U . . .
H40S H 0.1566 0.1864 0.2837 0.083 Uiso 1 1 calc R U . . .
H40T H 0.1875 0.1269 0.2971 0.083 Uiso 1 1 calc R U . . .
C501 C 0.1660(7) 0.527(2) 1.0104(9) 0.161(12) Uiso 1 1 d D U . . .
H50A H 0.1506 0.4740 1.0097 0.241 Uiso 1 1 calc R U . . .
H50B H 0.1854 0.4999 1.0235 0.241 Uiso 1 1 calc R U . . .
H50C H 0.1602 0.5841 1.0273 0.241 Uiso 1 1 calc R U . . .
C502 C 0.1689(6) 0.561(2) 0.9654(8) 0.229(12) Uiso 1 1 d D U . . .
C503 C 0.1488(6) 0.513(2) 0.9295(9) 0.167(12) Uiso 1 1 d D U . . .
H50D H 0.1360 0.4623 0.9412 0.251 Uiso 1 1 calc R U . . .
H50E H 0.1361 0.5647 0.9142 0.251 Uiso 1 1 calc R U . . .
H50F H 0.1611 0.4804 0.9096 0.251 Uiso 1 1 calc DR U . . .
O502 O 0.1874(7) 0.628(2) 0.9590(10) 0.291(14) Uiso 1 1 d D U . . .
C601 C 0.2175(4) 0.4181(18) 0.9405(7) 0.141(10) Uiso 1 1 d D U . . .
H60A H 0.2191 0.4667 0.9642 0.211 Uiso 1 1 calc R U . . .
H60B H 0.1971 0.3896 0.9366 0.211 Uiso 1 1 calc DR U . . .
H60C H 0.2322 0.3640 0.9471 0.211 Uiso 1 1 calc R U . . .
C602 C 0.2235(5) 0.470(2) 0.9007(8) 0.184(11) Uiso 1 1 d D U . . .
C603 C 0.2294(9) 0.580(2) 0.9017(12) 0.229(16) Uiso 1 1 d D U . . .
H60D H 0.2294 0.6047 0.9311 0.344 Uiso 1 1 calc R U . . .
H60E H 0.2491 0.5929 0.8919 0.344 Uiso 1 1 calc R U . . .
H60F H 0.2136 0.6141 0.8827 0.344 Uiso 1 1 calc R U . . .
O602 O 0.2222(6) 0.417(2) 0.8680(9) 0.221(11) Uiso 1 1 d D U . . .
C701 C 0.0096(5) 0.5566(15) 0.2138(6) 0.083(6) Uiso 1 1 d D U . . .
H70A H 0.0080 0.6288 0.2198 0.125 Uiso 1 1 calc R U . . .
H70B H 0.0306 0.5399 0.2103 0.125 Uiso 1 1 calc R U . . .
H70C H -0.0034 0.5399 0.1874 0.125 Uiso 1 1 calc R U . . .
C702 C 0.0000 0.4980(14) 0.2500 0.049(5) Uiso 1 2 d DS U P . .
O702 O 0.0000 0.4072(13) 0.2500 0.077(5) Uiso 1 2 d DS U P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.882(13) . ?
Pt1 Pt9 2.6993(6) . ?
Pt1 Sn7 2.7015(9) . ?
Pt1 Sn1 2.7094(10) . ?
Pt1 Pt3 2.8040(7) . ?
Pt1 Sn4 2.8466(10) . ?
Pt1 Pt8 2.8629(6) . ?
Pt1 Pt2 3.0141(6) . ?
Pt2 C2 1.851(12) . ?
Pt2 Sn2 2.6529(9) . ?
Pt2 Sn4 2.6797(9) . ?
Pt2 Pt7 2.7912(6) . ?
Pt2 Pt8 2.8425(7) . ?
Pt2 Pt3 3.0718(6) . ?
Pt3 C3 1.859(13) . ?
Pt3 Sn7 2.6849(9) . ?
Pt3 Sn3 2.6969(8) . ?
Pt3 Pt9 2.7252(6) . ?
Pt3 Sn4 2.8006(9) . ?
Pt3 Pt7 2.8344(6) . ?
Pt4 C4 1.861(12) . ?
Pt4 Sn2 2.6531(9) . ?
Pt4 Sn5 2.6588(9) . ?
Pt4 Pt7 2.7871(6) . ?
Pt4 Pt8 2.7900(6) . ?
Pt4 Pt5 3.0526(6) . ?
Pt4 Pt6 3.1035(7) . ?
Pt5 C5 1.883(13) . ?
Pt5 Sn3 2.6927(9) . ?
Pt5 Sn6 2.6967(10) . ?
Pt5 Pt9 2.7347(6) . ?
Pt5 Sn5 2.7636(9) . ?
Pt5 Pt6 2.7875(7) . ?
Pt5 Pt7 2.8749(6) . ?
Pt6 C6 1.873(12) . ?
Pt6 Sn6 2.6646(9) . ?
Pt6 Sn1 2.7069(9) . ?
Pt6 Pt9 2.7132(6) . ?
Pt6 Pt8 2.8498(6) . ?
Pt6 Sn5 2.8879(9) . ?
Pt7 C7 1.905(12) . ?
Pt7 Pt9 2.6827(6) . ?
Pt7 Pt8 2.7425(7) . ?
Pt7 Sn2 2.7569(9) . ?
Pt7 Sn3 2.7855(8) . ?
Pt8 C8 1.903(13) . ?
Pt8 Pt9 2.7022(6) . ?
Pt8 Sn1 2.7686(9) . ?
Pt8 Sn2 2.7692(9) . ?
Pt9 C9 2.029(11) . ?
Pt9 Sn1 2.7086(9) . ?
Pt9 Sn3 2.7126(9) . ?
Sn1 Cl1 2.402(3) . ?
Sn1 Cl2 2.415(3) . ?
Sn2 Cl3 2.380(3) . ?
Sn2 Cl4 2.397(3) . ?
Sn3 Cl5 2.392(3) . ?
Sn3 Cl6 2.393(3) . ?
Sn4 Cl8 2.390(4) . ?
Sn4 Cl9 2.408(3) . ?
Sn4 Cl7 2.438(4) . ?
Sn5 Cl10 2.395(3) . ?
Sn5 Cl11 2.428(3) . ?
Sn5 Cl12 2.445(3) . ?
Sn6 O10 2.088(8) . ?
Sn6 Cl14 2.361(3) . ?
Sn6 Cl13 2.379(4) . ?
Sn7 O9 2.121(8) . ?
Sn7 Cl16 2.381(3) . ?
Sn7 Cl15 2.387(3) . ?
C1 O1 1.127(14) . ?
C2 O2 1.147(14) . ?
C3 O3 1.154(15) . ?
C4 O4 1.133(14) . ?
C5 O5 1.139(14) . ?
C6 O6 1.107(15) . ?
C7 O7 1.100(14) . ?
C8 O8 1.127(15) . ?
C9 O9 1.280(13) . ?
C9 O10 1.310(14) . ?
N1 C103 1.499(16) . ?
N1 C101 1.503(14) . ?
N1 C105 1.512(14) . ?
N1 C107 1.522(15) . ?
C101 C102 1.525(16) . ?
C101 H10A 0.9900 . ?
C101 H10B 0.9900 . ?
C102 H10C 0.9800 . ?
C102 H10D 0.9800 . ?
C102 H10E 0.9800 . ?
C103 C104 1.530(19) . ?
C103 H10F 0.9900 . ?
C103 H10G 0.9900 . ?
C104 H10H 0.9800 . ?
C104 H10I 0.9800 . ?
C104 H10J 0.9800 . ?
C105 C106 1.530(17) . ?
C105 H10K 0.9900 . ?
C105 H10L 0.9900 . ?
C106 H10M 0.9800 . ?
C106 H10N 0.9800 . ?
C106 H10O 0.9800 . ?
C107 C108 1.524(18) . ?
C107 H10P 0.9900 . ?
C107 H10Q 0.9900 . ?
C108 H10R 0.9800 . ?
C108 H10S 0.9800 . ?
C108 H10T 0.9800 . ?
N2 C205 1.496(16) . ?
N2 C207 1.511(16) . ?
N2 C203 1.516(16) . ?
N2 C201 1.535(15) . ?
C201 C202 1.49(2) . ?
C201 H20A 0.9900 . ?
C201 H20B 0.9900 . ?
C202 H20C 0.9800 . ?
C202 H20D 0.9800 . ?
C202 H20E 0.9800 . ?
C203 C204 1.50(2) . ?
C203 H20F 0.9900 . ?
C203 H20G 0.9900 . ?
C204 H20H 0.9800 . ?
C204 H20I 0.9800 . ?
C204 H20J 0.9800 . ?
C205 C206 1.513(19) . ?
C205 H20K 0.9900 . ?
C205 H20L 0.9900 . ?
C206 H20M 0.9800 . ?
C206 H20N 0.9800 . ?
C206 H20O 0.9800 . ?
C207 C208 1.493(19) . ?
C207 H20P 0.9900 . ?
C207 H20Q 0.9900 . ?
C208 H20R 0.9800 . ?
C208 H20S 0.9800 . ?
C208 H20T 0.9800 . ?
N3 C305 1.460(18) . ?
N3 C301 1.507(18) . ?
N3 C303 1.511(19) . ?
N3 C307 1.543(18) . ?
C301 C302 1.53(2) . ?
C301 H30A 0.9900 . ?
C301 H30B 0.9900 . ?
C302 H30C 0.9800 . ?
C302 H30D 0.9800 . ?
C302 H30E 0.9800 . ?
C303 C304 1.54(2) . ?
C303 H30F 0.9900 . ?
C303 H30G 0.9900 . ?
C304 H30H 0.9800 . ?
C304 H30I 0.9800 . ?
C304 H30J 0.9800 . ?
C305 C306 1.56(3) . ?
C305 H30K 0.9900 . ?
C305 H30L 0.9900 . ?
C306 H30M 0.9800 . ?
C306 H30N 0.9800 . ?
C306 H30O 0.9800 . ?
C307 C308 1.48(2) . ?
C307 H30P 0.9900 . ?
C307 H30Q 0.9900 . ?
C308 H30R 0.9800 . ?
C308 H30S 0.9800 . ?
C308 H30T 0.9800 . ?
N4 C403 1.495(16) . ?
N4 C407 1.506(16) . ?
N4 C405 1.513(16) . ?
N4 C401 1.527(16) . ?
C401 C402 1.494(18) . ?
C401 H40A 0.9900 . ?
C401 H40B 0.9900 . ?
C402 H40C 0.9800 . ?
C402 H40D 0.9800 . ?
C402 H40E 0.9800 . ?
C403 C404 1.511(18) . ?
C403 H40F 0.9900 . ?
C403 H40G 0.9900 . ?
C404 H40H 0.9800 . ?
C404 H40I 0.9800 . ?
C404 H40J 0.9800 . ?
C405 C406 1.500(19) . ?
C405 H40K 0.9900 . ?
C405 H40L 0.9900 . ?
C406 H40M 0.9800 . ?
C406 H40N 0.9800 . ?
C406 H40O 0.9800 . ?
C407 C408 1.527(19) . ?
C407 H40P 0.9900 . ?
C407 H40Q 0.9900 . ?
C408 H40R 0.9800 . ?
C408 H40S 0.9800 . ?
C408 H40T 0.9800 . ?
C501 C502 1.501(13) . ?
C501 H50A 0.9800 . ?
C501 H50B 0.9800 . ?
C501 H50C 0.9800 . ?
C502 O502 1.245(15) . ?
C502 C503 1.495(13) . ?
C503 H50D 0.9800 . ?
C503 H50E 0.9800 . ?
C503 H50F 0.9800 . ?
C601 C602 1.475(13) . ?
C601 H60A 0.9800 . ?
C601 H60B 0.9800 . ?
C601 H60C 0.9800 . ?
C602 O602 1.238(15) . ?
C602 C603 1.483(13) . ?
C603 H60D 0.9800 . ?
C603 H60E 0.9800 . ?
C603 H60F 0.9800 . ?
C701 C702 1.479(15) . ?
C701 H70A 0.9800 . ?
C701 H70B 0.9800 . ?
C701 H70C 0.9800 . ?
C702 O702 1.204(16) . ?
C702 C701 1.480(15) 2 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 Pt9 155.4(4) . . ?
C1 Pt1 Sn7 108.7(4) . . ?
Pt9 Pt1 Sn7 76.18(2) . . ?
C1 Pt1 Sn1 95.6(4) . . ?
Pt9 Pt1 Sn1 60.10(2) . . ?
Sn7 Pt1 Sn1 104.12(3) . . ?
C1 Pt1 Pt3 144.3(4) . . ?
Pt9 Pt1 Pt3 59.329(16) . . ?
Sn7 Pt1 Pt3 58.34(2) . . ?
Sn1 Pt1 Pt3 119.35(2) . . ?
C1 Pt1 Sn4 87.1(4) . . ?
Pt9 Pt1 Sn4 117.52(3) . . ?
Sn7 Pt1 Sn4 82.47(3) . . ?
Sn1 Pt1 Sn4 171.54(3) . . ?
Pt3 Pt1 Sn4 59.42(2) . . ?
C1 Pt1 Pt8 115.3(4) . . ?
Pt9 Pt1 Pt8 58.043(15) . . ?
Sn7 Pt1 Pt8 133.84(2) . . ?
Sn1 Pt1 Pt8 59.51(2) . . ?
Pt3 Pt1 Pt8 90.632(18) . . ?
Sn4 Pt1 Pt8 112.10(2) . . ?
C1 Pt1 Pt2 108.5(4) . . ?
Pt9 Pt1 Pt2 88.161(17) . . ?
Sn7 Pt1 Pt2 119.76(3) . . ?
Sn1 Pt1 Pt2 117.26(2) . . ?
Pt3 Pt1 Pt2 63.617(16) . . ?
Sn4 Pt1 Pt2 54.327(19) . . ?
Pt8 Pt1 Pt2 57.782(15) . . ?
C2 Pt2 Sn2 93.8(4) . . ?
C2 Pt2 Sn4 89.7(4) . . ?
Sn2 Pt2 Sn4 176.14(3) . . ?
C2 Pt2 Pt7 144.5(4) . . ?
Sn2 Pt2 Pt7 60.79(2) . . ?
Sn4 Pt2 Pt7 115.36(2) . . ?
C2 Pt2 Pt8 132.8(4) . . ?
Sn2 Pt2 Pt8 60.40(2) . . ?
Sn4 Pt2 Pt8 118.08(3) . . ?
Pt7 Pt2 Pt8 58.254(16) . . ?
C2 Pt2 Pt1 130.5(4) . . ?
Sn2 Pt2 Pt1 118.77(3) . . ?
Sn4 Pt2 Pt1 59.65(2) . . ?
Pt7 Pt2 Pt1 84.870(17) . . ?
Pt8 Pt2 Pt1 58.440(15) . . ?
C2 Pt2 Pt3 140.2(4) . . ?
Sn2 Pt2 Pt3 118.35(2) . . ?
Sn4 Pt2 Pt3 57.80(2) . . ?
Pt7 Pt2 Pt3 57.582(14) . . ?
Pt8 Pt2 Pt3 85.796(17) . . ?
Pt1 Pt2 Pt3 54.859(14) . . ?
C3 Pt3 Sn7 106.6(4) . . ?
C3 Pt3 Sn3 93.2(3) . . ?
Sn7 Pt3 Sn3 104.42(3) . . ?
C3 Pt3 Pt9 152.2(3) . . ?
Sn7 Pt3 Pt9 76.02(2) . . ?
Sn3 Pt3 Pt9 60.04(2) . . ?
C3 Pt3 Sn4 89.4(3) . . ?
Sn7 Pt3 Sn4 83.63(3) . . ?
Sn3 Pt3 Sn4 170.40(3) . . ?
Pt9 Pt3 Sn4 118.23(3) . . ?
C3 Pt3 Pt1 147.0(3) . . ?
Sn7 Pt3 Pt1 58.92(2) . . ?
Sn3 Pt3 Pt1 118.43(3) . . ?
Pt9 Pt3 Pt1 58.422(16) . . ?
Sn4 Pt3 Pt1 61.05(2) . . ?
C3 Pt3 Pt7 117.7(4) . . ?
Sn7 Pt3 Pt7 133.05(3) . . ?
Sn3 Pt3 Pt7 60.416(19) . . ?
Pt9 Pt3 Pt7 57.662(15) . . ?
Sn4 Pt3 Pt7 110.27(2) . . ?
Pt1 Pt3 Pt7 88.108(18) . . ?
C3 Pt3 Pt2 114.3(4) . . ?
Sn7 Pt3 Pt2 118.31(2) . . ?
Sn3 Pt3 Pt2 116.64(2) . . ?
Pt9 Pt3 Pt2 86.528(17) . . ?
Sn4 Pt3 Pt2 54.062(19) . . ?
Pt1 Pt3 Pt2 61.524(15) . . ?
Pt7 Pt3 Pt2 56.232(14) . . ?
C4 Pt4 Sn2 92.9(4) . . ?
C4 Pt4 Sn5 90.1(4) . . ?
Sn2 Pt4 Sn5 176.88(3) . . ?
C4 Pt4 Pt7 141.3(4) . . ?
Sn2 Pt4 Pt7 60.84(2) . . ?
Sn5 Pt4 Pt7 116.12(2) . . ?
C4 Pt4 Pt8 135.1(4) . . ?
Sn2 Pt4 Pt8 61.10(2) . . ?
Sn5 Pt4 Pt8 117.10(3) . . ?
Pt7 Pt4 Pt8 58.912(16) . . ?
C4 Pt4 Pt5 138.4(4) . . ?
Sn2 Pt4 Pt5 119.55(2) . . ?
Sn5 Pt4 Pt5 57.38(2) . . ?
Pt7 Pt4 Pt5 58.775(14) . . ?
Pt8 Pt4 Pt5 85.659(16) . . ?
C4 Pt4 Pt6 133.8(4) . . ?
Sn2 Pt4 Pt6 118.56(2) . . ?
Sn5 Pt4 Pt6 59.56(2) . . ?
Pt7 Pt4 Pt6 84.890(17) . . ?
Pt8 Pt4 Pt6 57.541(15) . . ?
Pt5 Pt4 Pt6 53.841(14) . . ?
C5 Pt5 Sn3 89.4(4) . . ?
C5 Pt5 Sn6 102.7(4) . . ?
Sn3 Pt5 Sn6 103.12(3) . . ?
C5 Pt5 Pt9 147.0(4) . . ?
Sn3 Pt5 Pt9 59.97(2) . . ?
Sn6 Pt5 Pt9 75.36(2) . . ?
C5 Pt5 Sn5 92.8(4) . . ?
Sn3 Pt5 Sn5 169.18(3) . . ?
Sn6 Pt5 Sn5 86.73(3) . . ?
Pt9 Pt5 Sn5 119.62(2) . . ?
C5 Pt5 Pt6 147.8(4) . . ?
Sn3 Pt5 Pt6 118.71(2) . . ?
Sn6 Pt5 Pt6 58.11(2) . . ?
Pt9 Pt5 Pt6 58.845(16) . . ?
Sn5 Pt5 Pt6 62.69(2) . . ?
C5 Pt5 Pt7 120.1(4) . . ?
Sn3 Pt5 Pt7 59.93(2) . . ?
Sn6 Pt5 Pt7 132.01(2) . . ?
Pt9 Pt5 Pt7 57.074(15) . . ?
Sn5 Pt5 Pt7 110.09(2) . . ?
Pt6 Pt5 Pt7 89.367(17) . . ?
C5 Pt5 Pt4 119.9(4) . . ?
Sn3 Pt5 Pt4 115.88(2) . . ?
Sn6 Pt5 Pt4 120.47(3) . . ?
Pt9 Pt5 Pt4 86.907(16) . . ?
Sn5 Pt5 Pt4 54.13(2) . . ?
Pt6 Pt5 Pt4 64.013(16) . . ?
Pt7 Pt5 Pt4 55.997(14) . . ?
C6 Pt6 Sn6 101.9(4) . . ?
C6 Pt6 Sn1 96.3(4) . . ?
Sn6 Pt6 Sn1 104.33(3) . . ?
C6 Pt6 Pt9 153.9(4) . . ?
Sn6 Pt6 Pt9 76.24(2) . . ?
Sn1 Pt6 Pt9 59.97(2) . . ?
C6 Pt6 Pt5 141.9(4) . . ?
Sn6 Pt6 Pt5 59.24(2) . . ?
Sn1 Pt6 Pt5 119.54(3) . . ?
Pt9 Pt6 Pt5 59.606(16) . . ?
C6 Pt6 Pt8 121.7(4) . . ?
Sn6 Pt6 Pt8 133.84(3) . . ?
Sn1 Pt6 Pt8 59.70(2) . . ?
Pt9 Pt6 Pt8 58.062(15) . . ?
Pt5 Pt6 Pt8 89.716(19) . . ?
C6 Pt6 Sn5 89.3(4) . . ?
Sn6 Pt6 Sn5 84.86(3) . . ?
Sn1 Pt6 Sn5 167.88(3) . . ?
Pt9 Pt6 Sn5 116.06(3) . . ?
Pt5 Pt6 Sn5 58.25(2) . . ?
Pt8 Pt6 Sn5 108.23(2) . . ?
C6 Pt6 Pt4 115.8(4) . . ?
Sn6 Pt6 Pt4 119.75(3) . . ?
Sn1 Pt6 Pt4 115.39(2) . . ?
Pt9 Pt6 Pt4 86.265(18) . . ?
Pt5 Pt6 Pt4 62.147(16) . . ?
Pt8 Pt6 Pt4 55.696(14) . . ?
Sn5 Pt6 Pt4 52.54(2) . . ?
C7 Pt7 Pt9 151.0(3) . . ?
C7 Pt7 Pt8 149.3(3) . . ?
Pt9 Pt7 Pt8 59.735(16) . . ?
C7 Pt7 Sn2 88.8(3) . . ?
Pt9 Pt7 Sn2 120.20(3) . . ?
Pt8 Pt7 Sn2 60.47(2) . . ?
C7 Pt7 Sn3 91.5(3) . . ?
Pt9 Pt7 Sn3 59.45(2) . . ?
Pt8 Pt7 Sn3 119.15(2) . . ?
Sn2 Pt7 Sn3 179.12(3) . . ?
C7 Pt7 Pt4 104.4(4) . . ?
Pt9 Pt7 Pt4 93.57(2) . . ?
Pt8 Pt7 Pt4 60.597(16) . . ?
Sn2 Pt7 Pt4 57.18(2) . . ?
Sn3 Pt7 Pt4 121.95(2) . . ?
C7 Pt7 Pt2 102.8(4) . . ?
Pt9 Pt7 Pt2 93.296(18) . . ?
Pt8 Pt7 Pt2 61.810(17) . . ?
Sn2 Pt7 Pt2 57.127(19) . . ?
Sn3 Pt7 Pt2 123.53(2) . . ?
Pt4 Pt7 Pt2 106.873(19) . . ?
C7 Pt7 Pt3 105.6(4) . . ?
Pt9 Pt7 Pt3 59.126(15) . . ?
Pt8 Pt7 Pt3 92.508(18) . . ?
Sn2 Pt7 Pt3 123.29(2) . . ?
Sn3 Pt7 Pt3 57.347(19) . . ?
Pt4 Pt7 Pt3 149.98(2) . . ?
Pt2 Pt7 Pt3 66.186(15) . . ?
C7 Pt7 Pt5 108.3(4) . . ?
Pt9 Pt7 Pt5 58.831(15) . . ?
Pt8 Pt7 Pt5 90.094(19) . . ?
Sn2 Pt7 Pt5 122.34(2) . . ?
Sn3 Pt7 Pt5 56.784(19) . . ?
Pt4 Pt7 Pt5 65.228(16) . . ?
Pt2 Pt7 Pt5 148.85(2) . . ?
Pt3 Pt7 Pt5 104.762(18) . . ?
C8 Pt8 Pt9 151.3(4) . . ?
C8 Pt8 Pt7 149.0(4) . . ?
Pt9 Pt8 Pt7 59.032(16) . . ?
C8 Pt8 Sn1 92.4(4) . . ?
Pt9 Pt8 Sn1 59.34(2) . . ?
Pt7 Pt8 Sn1 118.36(2) . . ?
C8 Pt8 Sn2 89.4(4) . . ?
Pt9 Pt8 Sn2 119.05(3) . . ?
Pt7 Pt8 Sn2 60.02(2) . . ?
Sn1 Pt8 Sn2 177.47(3) . . ?
C8 Pt8 Pt4 100.2(4) . . ?
Pt9 Pt8 Pt4 93.079(18) . . ?
Pt7 Pt8 Pt4 60.491(17) . . ?
Sn1 Pt8 Pt4 124.34(2) . . ?
Sn2 Pt8 Pt4 57.01(2) . . ?
C8 Pt8 Pt2 108.8(4) . . ?
Pt9 Pt8 Pt2 91.740(19) . . ?
Pt7 Pt8 Pt2 59.936(16) . . ?
Sn1 Pt8 Pt2 121.23(2) . . ?
Sn2 Pt8 Pt2 56.41(2) . . ?
Pt4 Pt8 Pt2 105.39(2) . . ?
C8 Pt8 Pt6 103.9(4) . . ?
Pt9 Pt8 Pt6 58.436(15) . . ?
Pt7 Pt8 Pt6 90.790(18) . . ?
Sn1 Pt8 Pt6 57.58(2) . . ?
Sn2 Pt8 Pt6 123.68(2) . . ?
Pt4 Pt8 Pt6 66.763(16) . . ?
Pt2 Pt8 Pt6 147.28(2) . . ?
C8 Pt8 Pt1 113.0(4) . . ?
Pt9 Pt8 Pt1 57.943(14) . . ?
Pt7 Pt8 Pt1 88.734(18) . . ?
Sn1 Pt8 Pt1 57.49(2) . . ?
Sn2 Pt8 Pt1 120.11(3) . . ?
Pt4 Pt8 Pt1 146.82(2) . . ?
Pt2 Pt8 Pt1 63.778(16) . . ?
Pt6 Pt8 Pt1 104.490(18) . . ?
C9 Pt9 Pt7 148.9(3) . . ?
C9 Pt9 Pt1 102.4(3) . . ?
Pt7 Pt9 Pt1 93.516(18) . . ?
C9 Pt9 Pt8 149.9(3) . . ?
Pt7 Pt9 Pt8 61.234(16) . . ?
Pt1 Pt9 Pt8 64.014(16) . . ?
C9 Pt9 Sn1 88.3(3) . . ?
Pt7 Pt9 Sn1 122.77(2) . . ?
Pt1 Pt9 Sn1 60.13(2) . . ?
Pt8 Pt9 Sn1 61.55(2) . . ?
C9 Pt9 Sn3 86.8(3) . . ?
Pt7 Pt9 Sn3 62.16(2) . . ?
Pt1 Pt9 Sn3 121.68(2) . . ?
Pt8 Pt9 Sn3 123.37(2) . . ?
Sn1 Pt9 Sn3 175.04(3) . . ?
C9 Pt9 Pt6 102.7(4) . . ?
Pt7 Pt9 Pt6 95.125(18) . . ?
Pt1 Pt9 Pt6 113.13(2) . . ?
Pt8 Pt9 Pt6 63.503(16) . . ?
Sn1 Pt9 Pt6 59.90(2) . . ?
Sn3 Pt9 Pt6 120.69(2) . . ?
C9 Pt9 Pt3 101.0(4) . . ?
Pt7 Pt9 Pt3 63.212(16) . . ?
Pt1 Pt9 Pt3 62.248(16) . . ?
Pt8 Pt9 Pt3 95.872(19) . . ?
Sn1 Pt9 Pt3 122.30(2) . . ?
Sn3 Pt9 Pt3 59.46(2) . . ?
Pt6 Pt9 Pt3 156.33(2) . . ?
C9 Pt9 Pt5 102.5(3) . . ?
Pt7 Pt9 Pt5 64.095(16) . . ?
Pt1 Pt9 Pt5 155.04(2) . . ?
Pt8 Pt9 Pt5 94.004(17) . . ?
Sn1 Pt9 Pt5 121.42(2) . . ?
Sn3 Pt9 Pt5 59.25(2) . . ?
Pt6 Pt9 Pt5 61.549(16) . . ?
Pt3 Pt9 Pt5 111.84(2) . . ?
Cl1 Sn1 Cl2 91.49(12) . . ?
Cl1 Sn1 Pt6 112.68(8) . . ?
Cl2 Sn1 Pt6 113.55(8) . . ?
Cl1 Sn1 Pt9 107.90(8) . . ?
Cl2 Sn1 Pt9 160.60(9) . . ?
Pt6 Sn1 Pt9 60.13(2) . . ?
Cl1 Sn1 Pt1 111.32(9) . . ?
Cl2 Sn1 Pt1 113.03(9) . . ?
Pt6 Sn1 Pt1 113.00(3) . . ?
Pt9 Sn1 Pt1 59.76(2) . . ?
Cl1 Sn1 Pt8 167.00(9) . . ?
Cl2 Sn1 Pt8 101.50(9) . . ?
Pt6 Sn1 Pt8 62.71(2) . . ?
Pt9 Sn1 Pt8 59.11(2) . . ?
Pt1 Sn1 Pt8 63.00(2) . . ?
Cl3 Sn2 Cl4 91.19(12) . . ?
Cl3 Sn2 Pt2 110.31(8) . . ?
Cl4 Sn2 Pt2 116.93(9) . . ?
Cl3 Sn2 Pt4 114.51(9) . . ?
Cl4 Sn2 Pt4 106.43(8) . . ?
Pt2 Sn2 Pt4 115.22(3) . . ?
Cl3 Sn2 Pt7 164.14(9) . . ?
Cl4 Sn2 Pt7 104.66(8) . . ?
Pt2 Sn2 Pt7 62.09(2) . . ?
Pt4 Sn2 Pt7 61.98(2) . . ?
Cl3 Sn2 Pt8 104.80(9) . . ?
Cl4 Sn2 Pt8 163.00(8) . . ?
Pt2 Sn2 Pt8 63.19(2) . . ?
Pt4 Sn2 Pt8 61.89(2) . . ?
Pt7 Sn2 Pt8 59.51(2) . . ?
Cl5 Sn3 Cl6 93.02(11) . . ?
Cl5 Sn3 Pt5 111.09(8) . . ?
Cl6 Sn3 Pt5 109.09(8) . . ?
Cl5 Sn3 Pt3 114.09(8) . . ?
Cl6 Sn3 Pt3 113.59(8) . . ?
Pt5 Sn3 Pt3 114.09(3) . . ?
Cl5 Sn3 Pt9 109.23(8) . . ?
Cl6 Sn3 Pt9 157.55(8) . . ?
Pt5 Sn3 Pt9 60.78(2) . . ?
Pt3 Sn3 Pt9 60.50(2) . . ?
Cl5 Sn3 Pt7 167.58(9) . . ?
Cl6 Sn3 Pt7 99.29(7) . . ?
Pt5 Sn3 Pt7 63.28(2) . . ?
Pt3 Sn3 Pt7 62.24(2) . . ?
Pt9 Sn3 Pt7 58.39(2) . . ?
Cl8 Sn4 Cl9 93.64(12) . . ?
Cl8 Sn4 Cl7 91.04(13) . . ?
Cl9 Sn4 Cl7 90.45(12) . . ?
Cl8 Sn4 Pt2 105.14(9) . . ?
Cl9 Sn4 Pt2 102.14(8) . . ?
Cl7 Sn4 Pt2 158.61(10) . . ?
Cl8 Sn4 Pt3 102.15(8) . . ?
Cl9 Sn4 Pt3 163.11(9) . . ?
Cl7 Sn4 Pt3 95.16(9) . . ?
Pt2 Sn4 Pt3 68.14(2) . . ?
Cl8 Sn4 Pt1 161.28(9) . . ?
Cl9 Sn4 Pt1 104.22(9) . . ?
Cl7 Sn4 Pt1 94.32(10) . . ?
Pt2 Sn4 Pt1 66.02(2) . . ?
Pt3 Sn4 Pt1 59.53(2) . . ?
Cl10 Sn5 Cl11 94.78(11) . . ?
Cl10 Sn5 Cl12 91.10(11) . . ?
Cl11 Sn5 Cl12 93.26(10) . . ?
Cl10 Sn5 Pt4 101.21(8) . . ?
Cl11 Sn5 Pt4 101.08(8) . . ?
Cl12 Sn5 Pt4 160.14(8) . . ?
Cl10 Sn5 Pt5 160.50(8) . . ?
Cl11 Sn5 Pt5 103.32(8) . . ?
Cl12 Sn5 Pt5 95.00(8) . . ?
Pt4 Sn5 Pt5 68.49(2) . . ?
Cl10 Sn5 Pt6 102.06(8) . . ?
Cl11 Sn5 Pt6 161.31(8) . . ?
Cl12 Sn5 Pt6 94.47(7) . . ?
Pt4 Sn5 Pt6 67.90(2) . . ?
Pt5 Sn5 Pt6 59.06(2) . . ?
O10 Sn6 Cl14 92.9(2) . . ?
O10 Sn6 Cl13 91.8(3) . . ?
Cl14 Sn6 Cl13 92.85(13) . . ?
O10 Sn6 Pt6 102.8(2) . . ?
Cl14 Sn6 Pt6 158.79(9) . . ?
Cl13 Sn6 Pt6 100.62(10) . . ?
O10 Sn6 Pt5 103.1(2) . . ?
Cl14 Sn6 Pt5 100.27(9) . . ?
Cl13 Sn6 Pt5 159.50(10) . . ?
Pt6 Sn6 Pt5 62.65(2) . . ?
O9 Sn7 Cl16 90.9(2) . . ?
O9 Sn7 Cl15 90.6(2) . . ?
Cl16 Sn7 Cl15 93.39(11) . . ?
O9 Sn7 Pt3 101.7(2) . . ?
Cl16 Sn7 Pt3 100.46(8) . . ?
Cl15 Sn7 Pt3 161.18(9) . . ?
O9 Sn7 Pt1 103.1(2) . . ?
Cl16 Sn7 Pt1 159.79(9) . . ?
Cl15 Sn7 Pt1 100.87(8) . . ?
Pt3 Sn7 Pt1 62.74(2) . . ?
O1 C1 Pt1 178.9(12) . . ?
O2 C2 Pt2 178.2(13) . . ?
O3 C3 Pt3 176.6(11) . . ?
O4 C4 Pt4 175.4(11) . . ?
O5 C5 Pt5 177.4(11) . . ?
O6 C6 Pt6 175.0(12) . . ?
O7 C7 Pt7 179.5(13) . . ?
O8 C8 Pt8 179.5(14) . . ?
O9 C9 O10 115.6(10) . . ?
O9 C9 Pt9 123.8(8) . . ?
O10 C9 Pt9 120.7(8) . . ?
C9 O9 Sn7 115.6(7) . . ?
C9 O10 Sn6 117.8(7) . . ?
C103 N1 C101 109.8(9) . . ?
C103 N1 C105 112.6(9) . . ?
C101 N1 C105 105.7(9) . . ?
C103 N1 C107 106.9(9) . . ?
C101 N1 C107 110.9(9) . . ?
C105 N1 C107 110.9(9) . . ?
N1 C101 C102 115.3(10) . . ?
N1 C101 H10A 108.5 . . ?
C102 C101 H10A 108.5 . . ?
N1 C101 H10B 108.5 . . ?
C102 C101 H10B 108.5 . . ?
H10A C101 H10B 107.5 . . ?
C101 C102 H10C 109.5 . . ?
C101 C102 H10D 109.5 . . ?
H10C C102 H10D 109.5 . . ?
C101 C102 H10E 109.5 . . ?
H10C C102 H10E 109.5 . . ?
H10D C102 H10E 109.5 . . ?
N1 C103 C104 116.2(11) . . ?
N1 C103 H10F 108.2 . . ?
C104 C103 H10F 108.2 . . ?
N1 C103 H10G 108.2 . . ?
C104 C103 H10G 108.2 . . ?
H10F C103 H10G 107.4 . . ?
C103 C104 H10H 109.5 . . ?
C103 C104 H10I 109.5 . . ?
H10H C104 H10I 109.5 . . ?
C103 C104 H10J 109.5 . . ?
H10H C104 H10J 109.5 . . ?
H10I C104 H10J 109.5 . . ?
N1 C105 C106 114.2(10) . . ?
N1 C105 H10K 108.7 . . ?
C106 C105 H10K 108.7 . . ?
N1 C105 H10L 108.7 . . ?
C106 C105 H10L 108.7 . . ?
H10K C105 H10L 107.6 . . ?
C105 C106 H10M 109.5 . . ?
C105 C106 H10N 109.5 . . ?
H10M C106 H10N 109.5 . . ?
C105 C106 H10O 109.5 . . ?
H10M C106 H10O 109.5 . . ?
H10N C106 H10O 109.5 . . ?
N1 C107 C108 114.6(9) . . ?
N1 C107 H10P 108.6 . . ?
C108 C107 H10P 108.6 . . ?
N1 C107 H10Q 108.6 . . ?
C108 C107 H10Q 108.6 . . ?
H10P C107 H10Q 107.6 . . ?
C107 C108 H10R 109.5 . . ?
C107 C108 H10S 109.5 . . ?
H10R C108 H10S 109.5 . . ?
C107 C108 H10T 109.5 . . ?
H10R C108 H10T 109.5 . . ?
H10S C108 H10T 109.5 . . ?
C205 N2 C207 111.2(10) . . ?
C205 N2 C203 111.2(11) . . ?
C207 N2 C203 106.1(9) . . ?
C205 N2 C201 105.2(9) . . ?
C207 N2 C201 111.7(11) . . ?
C203 N2 C201 111.6(9) . . ?
C202 C201 N2 114.9(12) . . ?
C202 C201 H20A 108.5 . . ?
N2 C201 H20A 108.5 . . ?
C202 C201 H20B 108.5 . . ?
N2 C201 H20B 108.5 . . ?
H20A C201 H20B 107.5 . . ?
C201 C202 H20C 109.5 . . ?
C201 C202 H20D 109.5 . . ?
H20C C202 H20D 109.5 . . ?
C201 C202 H20E 109.5 . . ?
H20C C202 H20E 109.5 . . ?
H20D C202 H20E 109.5 . . ?
C204 C203 N2 115.3(11) . . ?
C204 C203 H20F 108.4 . . ?
N2 C203 H20F 108.4 . . ?
C204 C203 H20G 108.4 . . ?
N2 C203 H20G 108.4 . . ?
H20F C203 H20G 107.5 . . ?
C203 C204 H20H 109.5 . . ?
C203 C204 H20I 109.5 . . ?
H20H C204 H20I 109.5 . . ?
C203 C204 H20J 109.5 . . ?
H20H C204 H20J 109.5 . . ?
H20I C204 H20J 109.5 . . ?
N2 C205 C206 115.9(10) . . ?
N2 C205 H20K 108.3 . . ?
C206 C205 H20K 108.3 . . ?
N2 C205 H20L 108.3 . . ?
C206 C205 H20L 108.3 . . ?
H20K C205 H20L 107.4 . . ?
C205 C206 H20M 109.5 . . ?
C205 C206 H20N 109.5 . . ?
H20M C206 H20N 109.5 . . ?
C205 C206 H20O 109.5 . . ?
H20M C206 H20O 109.5 . . ?
H20N C206 H20O 109.5 . . ?
C208 C207 N2 115.2(10) . . ?
C208 C207 H20P 108.5 . . ?
N2 C207 H20P 108.5 . . ?
C208 C207 H20Q 108.5 . . ?
N2 C207 H20Q 108.5 . . ?
H20P C207 H20Q 107.5 . . ?
C207 C208 H20R 109.5 . . ?
C207 C208 H20S 109.5 . . ?
H20R C208 H20S 109.5 . . ?
C207 C208 H20T 109.5 . . ?
H20R C208 H20T 109.5 . . ?
H20S C208 H20T 109.5 . . ?
C305 N3 C301 106.5(12) . . ?
C305 N3 C303 116.2(12) . . ?
C301 N3 C303 110.2(12) . . ?
C305 N3 C307 106.9(12) . . ?
C301 N3 C307 111.3(11) . . ?
C303 N3 C307 105.9(10) . . ?
N3 C301 C302 115.1(12) . . ?
N3 C301 H30A 108.5 . . ?
C302 C301 H30A 108.5 . . ?
N3 C301 H30B 108.5 . . ?
C302 C301 H30B 108.5 . . ?
H30A C301 H30B 107.5 . . ?
C301 C302 H30C 109.5 . . ?
C301 C302 H30D 109.5 . . ?
H30C C302 H30D 109.5 . . ?
C301 C302 H30E 109.5 . . ?
H30C C302 H30E 109.5 . . ?
H30D C302 H30E 109.5 . . ?
N3 C303 C304 116.3(12) . . ?
N3 C303 H30F 108.2 . . ?
C304 C303 H30F 108.2 . . ?
N3 C303 H30G 108.2 . . ?
C304 C303 H30G 108.2 . . ?
H30F C303 H30G 107.4 . . ?
C303 C304 H30H 109.5 . . ?
C303 C304 H30I 109.5 . . ?
H30H C304 H30I 109.5 . . ?
C303 C304 H30J 109.5 . . ?
H30H C304 H30J 109.5 . . ?
H30I C304 H30J 109.5 . . ?
N3 C305 C306 117.0(14) . . ?
N3 C305 H30K 108.1 . . ?
C306 C305 H30K 108.1 . . ?
N3 C305 H30L 108.1 . . ?
C306 C305 H30L 108.1 . . ?
H30K C305 H30L 107.3 . . ?
C305 C306 H30M 109.5 . . ?
C305 C306 H30N 109.5 . . ?
H30M C306 H30N 109.5 . . ?
C305 C306 H30O 109.5 . . ?
H30M C306 H30O 109.5 . . ?
H30N C306 H30O 109.5 . . ?
C308 C307 N3 113.9(12) . . ?
C308 C307 H30P 108.8 . . ?
N3 C307 H30P 108.8 . . ?
C308 C307 H30Q 108.8 . . ?
N3 C307 H30Q 108.8 . . ?
H30P C307 H30Q 107.7 . . ?
C307 C308 H30R 109.5 . . ?
C307 C308 H30S 109.5 . . ?
H30R C308 H30S 109.5 . . ?
C307 C308 H30T 109.5 . . ?
H30R C308 H30T 109.5 . . ?
H30S C308 H30T 109.5 . . ?
C403 N4 C407 107.6(9) . . ?
C403 N4 C405 110.5(10) . . ?
C407 N4 C405 109.9(11) . . ?
C403 N4 C401 111.9(10) . . ?
C407 N4 C401 110.5(10) . . ?
C405 N4 C401 106.5(9) . . ?
C402 C401 N4 115.4(10) . . ?
C402 C401 H40A 108.4 . . ?
N4 C401 H40A 108.4 . . ?
C402 C401 H40B 108.4 . . ?
N4 C401 H40B 108.4 . . ?
H40A C401 H40B 107.5 . . ?
C401 C402 H40C 109.5 . . ?
C401 C402 H40D 109.5 . . ?
H40C C402 H40D 109.5 . . ?
C401 C402 H40E 109.5 . . ?
H40C C402 H40E 109.5 . . ?
H40D C402 H40E 109.5 . . ?
N4 C403 C404 116.0(11) . . ?
N4 C403 H40F 108.3 . . ?
C404 C403 H40F 108.3 . . ?
N4 C403 H40G 108.3 . . ?
C404 C403 H40G 108.3 . . ?
H40F C403 H40G 107.4 . . ?
C403 C404 H40H 109.5 . . ?
C403 C404 H40I 109.5 . . ?
H40H C404 H40I 109.5 . . ?
C403 C404 H40J 109.5 . . ?
H40H C404 H40J 109.5 . . ?
H40I C404 H40J 109.5 . . ?
C406 C405 N4 116.9(11) . . ?
C406 C405 H40K 108.1 . . ?
N4 C405 H40K 108.1 . . ?
C406 C405 H40L 108.1 . . ?
N4 C405 H40L 108.1 . . ?
H40K C405 H40L 107.3 . . ?
C405 C406 H40M 109.5 . . ?
C405 C406 H40N 109.5 . . ?
H40M C406 H40N 109.5 . . ?
C405 C406 H40O 109.5 . . ?
H40M C406 H40O 109.5 . . ?
H40N C406 H40O 109.5 . . ?
N4 C407 C408 116.2(11) . . ?
N4 C407 H40P 108.2 . . ?
C408 C407 H40P 108.2 . . ?
N4 C407 H40Q 108.2 . . ?
C408 C407 H40Q 108.2 . . ?
H40P C407 H40Q 107.4 . . ?
C407 C408 H40R 109.5 . . ?
C407 C408 H40S 109.5 . . ?
H40R C408 H40S 109.5 . . ?
C407 C408 H40T 109.5 . . ?
H40R C408 H40T 109.5 . . ?
H40S C408 H40T 109.5 . . ?
C502 C501 H50A 109.5 . . ?
C502 C501 H50B 109.5 . . ?
H50A C501 H50B 109.5 . . ?
C502 C501 H50C 109.5 . . ?
H50A C501 H50C 109.5 . . ?
H50B C501 H50C 109.5 . . ?
O502 C502 C503 122(2) . . ?
O502 C502 C501 120(2) . . ?
C503 C502 C501 118(2) . . ?
C502 C503 H50D 109.5 . . ?
C502 C503 H50E 109.5 . . ?
H50D C503 H50E 109.5 . . ?
C502 C503 H50F 109.5 . . ?
H50D C503 H50F 109.5 . . ?
H50E C503 H50F 109.5 . . ?
C602 C601 H60A 109.5 . . ?
C602 C601 H60B 109.5 . . ?
H60A C601 H60B 109.5 . . ?
C602 C601 H60C 109.5 . . ?
H60A C601 H60C 109.5 . . ?
H60B C601 H60C 109.5 . . ?
O602 C602 C601 116.4(19) . . ?
O602 C602 C603 124(2) . . ?
C601 C602 C603 119(2) . . ?
C602 C603 H60D 109.5 . . ?
C602 C603 H60E 109.5 . . ?
H60D C603 H60E 109.5 . . ?
C602 C603 H60F 109.5 . . ?
H60D C603 H60F 109.5 . . ?
H60E C603 H60F 109.5 . . ?
C702 C701 H70A 109.5 . . ?
C702 C701 H70B 109.5 . . ?
H70A C701 H70B 109.5 . . ?
C702 C701 H70C 109.5 . . ?
H70A C701 H70C 109.5 . . ?
H70B C701 H70C 109.5 . . ?
O702 C702 C701 121.7(10) . . ?
O702 C702 C701 121.7(10) . 2 ?
C701 C702 C701 117(2) . 2 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O10 C9 O9 Sn7 -177.8(8) . . . . ?
Pt9 C9 O9 Sn7 2.4(12) . . . . ?
O9 C9 O10 Sn6 -178.0(8) . . . . ?
Pt9 C9 O10 Sn6 1.8(12) . . . . ?
C103 N1 C101 C102 60.5(13) . . . . ?
C105 N1 C101 C102 -177.7(11) . . . . ?
C107 N1 C101 C102 -57.5(14) . . . . ?
C101 N1 C103 C104 57.4(13) . . . . ?
C105 N1 C103 C104 -60.2(13) . . . . ?
C107 N1 C103 C104 177.8(10) . . . . ?
C103 N1 C105 C106 -62.9(14) . . . . ?
C101 N1 C105 C106 177.2(11) . . . . ?
C107 N1 C105 C106 56.9(14) . . . . ?
C103 N1 C107 C108 -179.2(10) . . . . ?
C101 N1 C107 C108 -59.5(13) . . . . ?
C105 N1 C107 C108 57.7(13) . . . . ?
C205 N2 C201 C202 -175.4(12) . . . . ?
C207 N2 C201 C202 -54.6(15) . . . . ?
C203 N2 C201 C202 63.9(16) . . . . ?
C205 N2 C203 C204 -54.6(15) . . . . ?
C207 N2 C203 C204 -175.7(12) . . . . ?
C201 N2 C203 C204 62.5(16) . . . . ?
C207 N2 C205 C206 58.5(16) . . . . ?
C203 N2 C205 C206 -59.5(15) . . . . ?
C201 N2 C205 C206 179.5(12) . . . . ?
C205 N2 C207 C208 58.4(16) . . . . ?
C203 N2 C207 C208 179.5(12) . . . . ?
C201 N2 C207 C208 -58.8(15) . . . . ?
C305 N3 C301 C302 172.1(15) . . . . ?
C303 N3 C301 C302 -61.2(17) . . . . ?
C307 N3 C301 C302 55.9(18) . . . . ?
C305 N3 C303 C304 64.9(18) . . . . ?
C301 N3 C303 C304 -56.2(16) . . . . ?
C307 N3 C303 C304 -176.6(13) . . . . ?
C301 N3 C305 C306 -178.5(16) . . . . ?
C303 N3 C305 C306 58(2) . . . . ?
C307 N3 C305 C306 -59.5(19) . . . . ?
C305 N3 C307 C308 -54.7(16) . . . . ?
C301 N3 C307 C308 61.2(16) . . . . ?
C303 N3 C307 C308 -179.1(12) . . . . ?
C403 N4 C401 C402 57.5(15) . . . . ?
C407 N4 C401 C402 -62.4(15) . . . . ?
C405 N4 C401 C402 178.3(12) . . . . ?
C407 N4 C403 C404 -179.0(12) . . . . ?
C405 N4 C403 C404 -59.1(15) . . . . ?
C401 N4 C403 C404 59.4(15) . . . . ?
C403 N4 C405 C406 -61.5(16) . . . . ?
C407 N4 C405 C406 57.1(16) . . . . ?
C401 N4 C405 C406 176.8(12) . . . . ?
C403 N4 C407 C408 -177.6(13) . . . . ?
C405 N4 C407 C408 62.1(16) . . . . ?
C401 N4 C407 C408 -55.2(16) . . . . ?

_refine_diff_density_max         4.097
_refine_diff_density_min         -1.716
_refine_diff_density_rms         0.285

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_Me
_database_code_depnum_ccdc_archive 'CCDC 1439436'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C80 H69 Cl12 O8 P3 Pt5 Sn6'
_chemical_formula_weight         3364.25

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   P2(1)/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   14.0022(2)
_cell_length_b                   14.5742(3)
_cell_length_c                   47.1561(8)
_cell_angle_alpha                90.00
_cell_angle_beta                 92.2750(10)
_cell_angle_gamma                90.00
_cell_volume                     9615.6(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    9974
_cell_measurement_theta_min      2.1725
_cell_measurement_theta_max      28.8085

_exptl_crystal_description       prism
_exptl_crystal_colour            red
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.11
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.324
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             6208
_exptl_absorpt_coefficient_mu    9.204
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.3206
_exptl_absorpt_correction_T_max  0.4309
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1215 (selected reflections only, before parameter refinement)
 R(int) = 0.0583 (selected reflections only, after parameter refinement)
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            140848
_diffrn_reflns_av_R_equivalents  0.0634
_diffrn_reflns_av_unetI/netI     0.0461
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_l_min       -62
_diffrn_reflns_limit_l_max       62
_diffrn_reflns_theta_min         1.46
_diffrn_reflns_theta_max         28.00
_reflns_number_total             23071
_reflns_number_gt                17957
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
 The asymmetric unit of the unit cell contains one cluster anion and three 
 [PPh4]+ cations (all located on general positions).
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0192P)²+55.2685P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         23071
_refine_ls_number_parameters     1027
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0591
_refine_ls_R_factor_gt           0.0376
_refine_ls_wR_factor_ref         0.0738
_refine_ls_wR_factor_gt          0.0667
_refine_ls_goodness_of_fit_ref   1.063
_refine_ls_restrained_S_all      1.063
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.850170(18) 0.506169(18) 0.123880(5) 0.01809(6) Uani 1 1 d . . .
Pt2 Pt 0.974612(17) 0.660935(18) 0.119625(5) 0.01648(5) Uani 1 1 d . . .
Pt3 Pt 0.808139(18) 0.675652(18) 0.151647(5) 0.01646(5) Uani 1 1 d . . .
Pt4 Pt 0.792929(17) 0.666191(18) 0.091796(5) 0.01645(5) Uani 1 1 d . . .
Pt5 Pt 0.869553(18) 0.829551(18) 0.118523(5) 0.01764(6) Uani 1 1 d . . .
Sn1 Sn 0.96003(3) 0.55192(3) 0.168631(9) 0.01866(10) Uani 1 1 d . . .
Sn2 Sn 0.96702(3) 0.78528(3) 0.166072(9) 0.01772(10) Uani 1 1 d . . .
Sn3 Sn 0.92976(3) 0.53740(3) 0.074643(9) 0.01981(10) Uani 1 1 d . . .
Sn4 Sn 0.93904(3) 0.77183(3) 0.069838(9) 0.02144(10) Uani 1 1 d . . .
Sn5 Sn 0.66961(3) 0.56021(3) 0.124589(9) 0.01872(10) Uani 1 1 d . . .
Sn6 Sn 0.68327(3) 0.79436(3) 0.119801(9) 0.01809(10) Uani 1 1 d . . .
Cl1 Cl 1.11481(12) 0.48065(12) 0.17148(4) 0.0265(4) Uani 1 1 d . . .
Cl2 Cl 0.91033(14) 0.47872(14) 0.21122(4) 0.0337(4) Uani 1 1 d . . .
Cl3 Cl 0.91943(13) 0.86867(13) 0.20704(4) 0.0302(4) Uani 1 1 d . . .
Cl4 Cl 1.12771(12) 0.84587(12) 0.16880(4) 0.0261(4) Uani 1 1 d . . .
Cl5 Cl 0.84611(14) 0.45575(14) 0.03716(4) 0.0336(4) Uani 1 1 d . . .
Cl6 Cl 1.07650(14) 0.45985(15) 0.06770(4) 0.0380(5) Uani 1 1 d . . .
Cl7 Cl 0.86447(16) 0.83800(16) 0.02828(4) 0.0429(5) Uani 1 1 d . . .
Cl8 Cl 1.09141(14) 0.84027(14) 0.06099(4) 0.0366(5) Uani 1 1 d . . .
Cl9 Cl 0.58317(13) 0.49214(14) 0.16249(4) 0.0315(4) Uani 1 1 d . . .
Cl10 Cl 0.56881(14) 0.49175(14) 0.08812(4) 0.0326(4) Uani 1 1 d . . .
Cl11 Cl 0.60044(13) 0.88253(13) 0.15453(4) 0.0293(4) Uani 1 1 d . . .
Cl12 Cl 0.58994(13) 0.86548(13) 0.08132(4) 0.0290(4) Uani 1 1 d . . .
C1 C 0.8361(5) 0.3803(5) 0.12573(16) 0.0288(17) Uani 1 1 d . . .
C2 C 1.1080(5) 0.6576(5) 0.11588(14) 0.0235(15) Uani 1 1 d . . .
C3 C 0.7486(5) 0.6843(5) 0.18641(14) 0.0225(15) Uani 1 1 d . . .
C4 C 0.7129(5) 0.6618(5) 0.05892(14) 0.0225(15) Uani 1 1 d . . .
C5 C 0.8815(5) 0.9561(5) 0.11678(16) 0.0287(17) Uani 1 1 d . . .
O1 O 0.8257(4) 0.3024(4) 0.12729(13) 0.0447(15) Uani 1 1 d . . .
O2 O 1.1883(3) 0.6566(4) 0.11331(11) 0.0355(13) Uani 1 1 d . . .
O3 O 0.7104(4) 0.6896(4) 0.20737(10) 0.0370(14) Uani 1 1 d . . .
O4 O 0.6632(4) 0.6597(4) 0.03923(10) 0.0331(13) Uani 1 1 d . . .
O5 O 0.8885(5) 1.0347(4) 0.11563(13) 0.0476(16) Uani 1 1 d . . .
C11 C 1.0622(6) 0.6713(6) 0.21768(14) 0.0354(19) Uani 1 1 d . . .
H11A H 1.0768 0.7350 0.2229 0.053 Uiso 1 1 calc R . .
H11B H 1.1218 0.6367 0.2163 0.053 Uiso 1 1 calc R . .
H11C H 1.0231 0.6434 0.2322 0.053 Uiso 1 1 calc R . .
C12 C 1.0104(6) 0.6384(6) 0.02093(15) 0.0335(19) Uani 1 1 d . . .
H12A H 1.0236 0.6993 0.0132 0.050 Uiso 1 1 calc R . .
H12B H 0.9646 0.6063 0.0082 0.050 Uiso 1 1 calc R . .
H12C H 1.0699 0.6031 0.0226 0.050 Uiso 1 1 calc R . .
C13 C 0.4842(6) 0.6837(6) 0.1203(2) 0.053(3) Uani 1 1 d . . .
H13A H 0.4617 0.7474 0.1205 0.079 Uiso 1 1 calc R . .
H13B H 0.4562 0.6497 0.1358 0.079 Uiso 1 1 calc R . .
H13C H 0.4648 0.6551 0.1021 0.079 Uiso 1 1 calc R . .
O11 O 1.0108(3) 0.6696(3) 0.19089(9) 0.0239(10) Uani 1 1 d . . .
O12 O 0.9707(3) 0.6481(3) 0.04850(10) 0.0261(11) Uani 1 1 d . . .
O13 O 0.5870(3) 0.6822(3) 0.12374(10) 0.0243(11) Uani 1 1 d . . .
P1 P 0.40169(13) 0.52405(13) 0.24892(4) 0.0201(4) Uani 1 1 d . . .
C101 C 0.3988(5) 0.6008(5) 0.21953(14) 0.0223(15) Uani 1 1 d . . .
C102 C 0.3204(6) 0.5993(5) 0.20033(16) 0.0311(17) Uani 1 1 d . . .
H102 H 0.2763 0.5499 0.2006 0.037 Uiso 1 1 calc R . .
C103 C 0.3068(7) 0.6692(6) 0.18100(17) 0.045(2) Uani 1 1 d . . .
H103 H 0.2534 0.6679 0.1679 0.054 Uiso 1 1 calc R . .
C104 C 0.3706(7) 0.7413(6) 0.18068(19) 0.047(2) Uani 1 1 d . . .
H104 H 0.3601 0.7905 0.1677 0.057 Uiso 1 1 calc R . .
C105 C 0.4492(7) 0.7422(6) 0.19896(18) 0.045(2) Uani 1 1 d . . .
H105 H 0.4936 0.7913 0.1982 0.054 Uiso 1 1 calc R . .
C106 C 0.4646(5) 0.6732(5) 0.21839(15) 0.0316(17) Uani 1 1 d . . .
H106 H 0.5193 0.6744 0.2310 0.038 Uiso 1 1 calc R . .
C107 C 0.3330(5) 0.5745(5) 0.27635(14) 0.0245(15) Uani 1 1 d . . .
C108 C 0.3200(6) 0.6692(6) 0.27734(19) 0.042(2) Uani 1 1 d . . .
H108 H 0.3466 0.7072 0.2633 0.050 Uiso 1 1 calc R . .
C109 C 0.2678(7) 0.7085(7) 0.2990(2) 0.056(3) Uani 1 1 d . . .
H109 H 0.2607 0.7732 0.3002 0.067 Uiso 1 1 calc R . .
C110 C 0.2272(6) 0.6517(8) 0.31841(18) 0.049(3) Uani 1 1 d . . .
H110 H 0.1901 0.6774 0.3329 0.059 Uiso 1 1 calc R . .
C111 C 0.2393(6) 0.5605(7) 0.31724(16) 0.043(2) Uani 1 1 d . . .
H111 H 0.2117 0.5231 0.3312 0.052 Uiso 1 1 calc R . .
C112 C 0.2908(5) 0.5190(6) 0.29627(14) 0.0320(18) Uani 1 1 d . . .
H112 H 0.2971 0.4542 0.2955 0.038 Uiso 1 1 calc R . .
C113 C 0.5223(5) 0.5073(5) 0.26150(14) 0.0226(15) Uani 1 1 d . . .
C114 C 0.5942(5) 0.4968(6) 0.24166(15) 0.0328(18) Uani 1 1 d . . .
H114 H 0.5791 0.5020 0.2219 0.039 Uiso 1 1 calc R . .
C115 C 0.6861(6) 0.4791(6) 0.25113(17) 0.041(2) Uani 1 1 d . . .
H115 H 0.7343 0.4710 0.2377 0.049 Uiso 1 1 calc R . .
C116 C 0.7105(5) 0.4727(6) 0.27980(17) 0.0348(19) Uani 1 1 d . . .
H116 H 0.7746 0.4605 0.2860 0.042 Uiso 1 1 calc R . .
C117 C 0.6403(5) 0.4843(5) 0.29912(15) 0.0300(17) Uani 1 1 d . . .
H117 H 0.6565 0.4803 0.3188 0.036 Uiso 1 1 calc R . .
C118 C 0.5468(5) 0.5016(5) 0.29037(14) 0.0267(16) Uani 1 1 d . . .
H118 H 0.4994 0.5097 0.3040 0.032 Uiso 1 1 calc R . .
C119 C 0.3488(5) 0.4160(5) 0.23931(13) 0.0240(15) Uani 1 1 d . . .
C120 C 0.4052(6) 0.3413(6) 0.23203(15) 0.0351(19) Uani 1 1 d . . .
H120 H 0.4729 0.3472 0.2325 0.042 Uiso 1 1 calc R . .
C121 C 0.3628(8) 0.2582(6) 0.22415(18) 0.050(3) Uani 1 1 d . . .
H121 H 0.4014 0.2076 0.2191 0.060 Uiso 1 1 calc R . .
C122 C 0.2645(8) 0.2495(6) 0.22367(16) 0.048(3) Uani 1 1 d . . .
H122 H 0.2356 0.1926 0.2186 0.058 Uiso 1 1 calc R . .
C123 C 0.2096(7) 0.3216(7) 0.23046(16) 0.046(2) Uani 1 1 d . . .
H123 H 0.1420 0.3150 0.2299 0.055 Uiso 1 1 calc R . .
C124 C 0.2500(6) 0.4052(6) 0.23823(15) 0.0338(19) Uani 1 1 d . . .
H124 H 0.2101 0.4553 0.2428 0.041 Uiso 1 1 calc R . .
P2 P 0.17157(13) 0.17433(13) 0.12146(4) 0.0213(4) Uani 1 1 d . . .
C201 C 0.1039(5) 0.1684(5) 0.15314(14) 0.0208(14) Uani 1 1 d . . .
C202 C 0.0970(5) 0.0868(5) 0.16833(14) 0.0230(15) Uani 1 1 d . . .
H202 H 0.1274 0.0328 0.1619 0.028 Uiso 1 1 calc R . .
C203 C 0.0457(5) 0.0848(5) 0.19279(14) 0.0270(16) Uani 1 1 d . . .
H203 H 0.0408 0.0297 0.2034 0.032 Uiso 1 1 calc R . .
C204 C 0.0016(5) 0.1646(5) 0.20165(15) 0.0286(17) Uani 1 1 d . . .
H204 H -0.0342 0.1630 0.2184 0.034 Uiso 1 1 calc R . .
C205 C 0.0080(5) 0.2455(5) 0.18700(15) 0.0298(17) Uani 1 1 d . . .
H205 H -0.0227 0.2992 0.1935 0.036 Uiso 1 1 calc R . .
C206 C 0.0602(5) 0.2478(5) 0.16251(15) 0.0254(16) Uani 1 1 d . . .
H206 H 0.0659 0.3035 0.1522 0.030 Uiso 1 1 calc R . .
C207 C 0.2394(5) 0.2787(5) 0.12354(14) 0.0214(15) Uani 1 1 d . . .
C208 C 0.2871(5) 0.3012(5) 0.14914(15) 0.0260(16) Uani 1 1 d . . .
H208 H 0.2818 0.2625 0.1652 0.031 Uiso 1 1 calc R . .
C209 C 0.3417(5) 0.3796(5) 0.15110(16) 0.0322(18) Uani 1 1 d . . .
H209 H 0.3740 0.3955 0.1685 0.039 Uiso 1 1 calc R . .
C210 C 0.3490(6) 0.4344(5) 0.12767(16) 0.0329(18) Uani 1 1 d . . .
H210 H 0.3870 0.4884 0.1291 0.039 Uiso 1 1 calc R . .
C211 C 0.3029(5) 0.4133(5) 0.10219(17) 0.0326(18) Uani 1 1 d . . .
H211 H 0.3092 0.4524 0.0863 0.039 Uiso 1 1 calc R . .
C212 C 0.2473(5) 0.3351(5) 0.09986(15) 0.0259(15) Uani 1 1 d . . .
H212 H 0.2149 0.3200 0.0824 0.031 Uiso 1 1 calc R . .
C213 C 0.0938(5) 0.1727(5) 0.09015(14) 0.0262(16) Uani 1 1 d . . .
C214 C 0.0075(6) 0.2173(6) 0.09008(19) 0.040(2) Uani 1 1 d . . .
H214 H -0.0120 0.2485 0.1066 0.048 Uiso 1 1 calc R . .
C215 C -0.0518(7) 0.2163(7) 0.0653(2) 0.057(3) Uani 1 1 d . . .
H215 H -0.1115 0.2472 0.0649 0.069 Uiso 1 1 calc R . .
C216 C -0.0239(7) 0.1716(7) 0.04199(19) 0.052(3) Uani 1 1 d . . .
H216 H -0.0639 0.1720 0.0252 0.062 Uiso 1 1 calc R . .
C217 C 0.0624(8) 0.1252(9) 0.04215(19) 0.065(3) Uani 1 1 d . . .
H217 H 0.0805 0.0924 0.0258 0.078 Uiso 1 1 calc R . .
C218 C 0.1215(7) 0.1266(7) 0.06596(18) 0.051(2) Uani 1 1 d . . .
H218 H 0.1815 0.0962 0.0660 0.061 Uiso 1 1 calc R . .
C219 C 0.2511(5) 0.0776(5) 0.11985(14) 0.0240(16) Uani 1 1 d . . .
C220 C 0.3500(5) 0.0907(5) 0.12379(14) 0.0261(16) Uani 1 1 d . . .
H220 H 0.3757 0.1501 0.1275 0.031 Uiso 1 1 calc R . .
C221 C 0.4090(6) 0.0156(6) 0.12218(16) 0.0353(19) Uani 1 1 d . . .
H221 H 0.4761 0.0235 0.1247 0.042 Uiso 1 1 calc R . .
C222 C 0.3726(6) -0.0704(6) 0.11701(17) 0.037(2) Uani 1 1 d . . .
H222 H 0.4147 -0.1213 0.1159 0.044 Uiso 1 1 calc R . .
C223 C 0.2759(6) -0.0834(6) 0.11341(16) 0.036(2) Uani 1 1 d . . .
H223 H 0.2512 -0.1433 0.1100 0.043 Uiso 1 1 calc R . .
C224 C 0.2148(6) -0.0098(5) 0.11475(15) 0.0312(18) Uani 1 1 d . . .
H224 H 0.1478 -0.0187 0.1122 0.037 Uiso 1 1 calc R . .
P3 P 0.48498(13) 0.21311(13) 0.03055(4) 0.0227(4) Uani 1 1 d . . .
C301 C 0.5359(5) 0.2036(5) 0.06613(15) 0.0294(17) Uani 1 1 d . . .
C302 C 0.5123(6) 0.2656(5) 0.08645(16) 0.0322(18) Uani 1 1 d . . .
H302 H 0.4684 0.3137 0.0820 0.039 Uiso 1 1 calc R . .
C303 C 0.5531(6) 0.2578(6) 0.11368(17) 0.037(2) Uani 1 1 d . . .
H303 H 0.5380 0.3013 0.1278 0.045 Uiso 1 1 calc R . .
C304 C 0.6143(7) 0.1881(7) 0.1202(2) 0.056(3) Uani 1 1 d . . .
H304 H 0.6412 0.1828 0.1389 0.067 Uiso 1 1 calc R . .
C305 C 0.6381(7) 0.1249(8) 0.0998(2) 0.065(3) Uani 1 1 d . . .
H305 H 0.6810 0.0762 0.1046 0.078 Uiso 1 1 calc R . .
C306 C 0.5995(7) 0.1329(7) 0.07277(19) 0.051(3) Uani 1 1 d . . .
H306 H 0.6162 0.0902 0.0586 0.061 Uiso 1 1 calc R . .
C307 C 0.4049(5) 0.3086(5) 0.02777(13) 0.0223(15) Uani 1 1 d . . .
C308 C 0.4434(5) 0.3971(5) 0.02726(14) 0.0259(16) Uani 1 1 d . . .
H308 H 0.5107 0.4061 0.0286 0.031 Uiso 1 1 calc R . .
C309 C 0.3823(6) 0.4711(5) 0.02480(15) 0.0334(19) Uani 1 1 d . . .
H309 H 0.4078 0.5314 0.0241 0.040 Uiso 1 1 calc R . .
C310 C 0.2846(6) 0.4587(6) 0.02332(15) 0.036(2) Uani 1 1 d . . .
H310 H 0.2434 0.5104 0.0220 0.043 Uiso 1 1 calc R . .
C311 C 0.2464(6) 0.3716(6) 0.02381(15) 0.0311(18) Uani 1 1 d . . .
H311 H 0.1791 0.3633 0.0224 0.037 Uiso 1 1 calc R . .
C312 C 0.3065(5) 0.2961(5) 0.02634(14) 0.0259(16) Uani 1 1 d . . .
H312 H 0.2804 0.2360 0.0271 0.031 Uiso 1 1 calc R . .
C313 C 0.4176(5) 0.1109(5) 0.02266(17) 0.0315(18) Uani 1 1 d . . .
C314 C 0.3944(8) 0.0522(6) 0.0439(2) 0.058(3) Uani 1 1 d . . .
H314 H 0.4213 0.0609 0.0625 0.069 Uiso 1 1 calc R . .
C315 C 0.3318(9) -0.0203(8) 0.0384(3) 0.082(4) Uani 1 1 d . . .
H315 H 0.3161 -0.0607 0.0533 0.098 Uiso 1 1 calc R . .
C316 C 0.2927(7) -0.0337(7) 0.0118(3) 0.064(3) Uani 1 1 d . . .
H316 H 0.2493 -0.0828 0.0082 0.077 Uiso 1 1 calc R . .
C317 C 0.3158(7) 0.0225(6) -0.0092(3) 0.063(3) Uani 1 1 d . . .
H317 H 0.2885 0.0131 -0.0277 0.076 Uiso 1 1 calc R . .
C318 C 0.3789(8) 0.0941(6) -0.0043(2) 0.062(3) Uani 1 1 d . . .
H318 H 0.3959 0.1323 -0.0196 0.075 Uiso 1 1 calc R . .
C319 C 0.5789(5) 0.2362(5) 0.00632(15) 0.0244(15) Uani 1 1 d . . .
C320 C 0.6693(6) 0.2577(6) 0.01652(17) 0.0367(19) Uani 1 1 d . . .
H320 H 0.6838 0.2569 0.0364 0.044 Uiso 1 1 calc R . .
C321 C 0.7398(6) 0.2808(5) -0.00227(18) 0.037(2) Uani 1 1 d . . .
H321 H 0.8023 0.2960 0.0048 0.045 Uiso 1 1 calc R . .
C322 C 0.7191(6) 0.2816(6) -0.03056(19) 0.044(2) Uani 1 1 d . . .
H322 H 0.7679 0.2948 -0.0434 0.053 Uiso 1 1 calc R . .
C323 C 0.6286(7) 0.2635(9) -0.04071(19) 0.069(4) Uani 1 1 d . . .
H323 H 0.6136 0.2672 -0.0605 0.083 Uiso 1 1 calc R . .
C324 C 0.5590(6) 0.2399(8) -0.02230(18) 0.058(3) Uani 1 1 d . . .
H324 H 0.4964 0.2261 -0.0295 0.069 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.848(8) . ?
Pt1 Sn1 2.6470(5) . ?
Pt1 Sn5 2.6496(5) . ?
Pt1 Sn3 2.6543(5) . ?
Pt1 Pt2 2.8621(4) . ?
Pt1 Pt3 2.8676(4) . ?
Pt1 Pt4 2.8765(4) . ?
Pt2 C2 1.883(7) . ?
Pt2 Pt4 2.8169(4) . ?
Pt2 Sn1 2.8184(5) . ?
Pt2 Sn3 2.8337(5) . ?
Pt2 Pt3 2.8353(3) . ?
Pt2 Sn2 2.8480(5) . ?
Pt2 Pt5 2.8635(4) . ?
Pt2 Sn4 2.8774(5) . ?
Pt3 C3 1.873(7) . ?
Pt3 Sn2 2.8008(5) . ?
Pt3 Pt4 2.8253(3) . ?
Pt3 Sn5 2.8328(5) . ?
Pt3 Sn6 2.8455(5) . ?
Pt3 Sn1 2.8777(5) . ?
Pt3 Pt5 2.8839(4) . ?
Pt4 C4 1.877(7) . ?
Pt4 Sn6 2.7842(5) . ?
Pt4 Sn4 2.7922(5) . ?
Pt4 Sn5 2.8232(5) . ?
Pt4 Sn3 2.8234(5) . ?
Pt4 Pt5 2.8811(4) . ?
Pt5 C5 1.854(8) . ?
Pt5 Sn2 2.6577(5) . ?
Pt5 Sn6 2.6613(5) . ?
Pt5 Sn4 2.6650(5) . ?
Sn1 O11 2.119(5) . ?
Sn1 Cl2 2.4015(18) . ?
Sn1 Cl1 2.4023(17) . ?
Sn2 O11 2.129(5) . ?
Sn2 Cl3 2.3989(17) . ?
Sn2 Cl4 2.4158(17) . ?
Sn3 O12 2.123(5) . ?
Sn3 Cl6 2.3789(19) . ?
Sn3 Cl5 2.3974(19) . ?
Sn4 O12 2.121(5) . ?
Sn4 Cl7 2.3872(19) . ?
Sn4 Cl8 2.4066(19) . ?
Sn5 O13 2.120(5) . ?
Sn5 Cl10 2.3984(18) . ?
Sn5 Cl9 2.4113(17) . ?
Sn6 O13 2.132(5) . ?
Sn6 Cl11 2.4143(17) . ?
Sn6 Cl12 2.4262(18) . ?
C1 O1 1.147(9) . ?
C2 O2 1.136(8) . ?
C3 O3 1.145(8) . ?
C4 O4 1.138(8) . ?
C5 O5 1.152(9) . ?
C11 O11 1.429(8) . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 O12 1.441(8) . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 O13 1.443(9) . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 H13C 0.9800 . ?
P1 C101 1.781(7) . ?
P1 C113 1.785(7) . ?
P1 C119 1.791(7) . ?
P1 C107 1.799(7) . ?
C101 C102 1.395(10) . ?
C101 C106 1.403(10) . ?
C102 C103 1.375(11) . ?
C102 H102 0.9500 . ?
C103 C104 1.380(12) . ?
C103 H103 0.9500 . ?
C104 C105 1.370(12) . ?
C104 H104 0.9500 . ?
C105 C106 1.372(11) . ?
C105 H105 0.9500 . ?
C106 H106 0.9500 . ?
C107 C112 1.389(10) . ?
C107 C108 1.393(11) . ?
C108 C109 1.402(12) . ?
C108 H108 0.9500 . ?
C109 C110 1.374(14) . ?
C109 H109 0.9500 . ?
C110 C111 1.342(13) . ?
C110 H110 0.9500 . ?
C111 C112 1.385(10) . ?
C111 H111 0.9500 . ?
C112 H112 0.9500 . ?
C113 C118 1.393(9) . ?
C113 C114 1.409(9) . ?
C114 C115 1.370(11) . ?
C114 H114 0.9500 . ?
C115 C116 1.384(11) . ?
C115 H115 0.9500 . ?
C116 C117 1.377(10) . ?
C116 H116 0.9500 . ?
C117 C118 1.380(10) . ?
C117 H117 0.9500 . ?
C118 H118 0.9500 . ?
C119 C124 1.392(10) . ?
C119 C120 1.396(10) . ?
C120 C121 1.393(12) . ?
C120 H120 0.9500 . ?
C121 C122 1.381(13) . ?
C121 H121 0.9500 . ?
C122 C123 1.349(13) . ?
C122 H122 0.9500 . ?
C123 C124 1.386(11) . ?
C123 H123 0.9500 . ?
C124 H124 0.9500 . ?
P2 C207 1.794(7) . ?
P2 C213 1.800(7) . ?
P2 C219 1.800(7) . ?
P2 C201 1.803(7) . ?
C201 C206 1.390(9) . ?
C201 C202 1.393(9) . ?
C202 C203 1.383(9) . ?
C202 H202 0.9500 . ?
C203 C204 1.389(10) . ?
C203 H203 0.9500 . ?
C204 C205 1.372(11) . ?
C204 H204 0.9500 . ?
C205 C206 1.391(9) . ?
C205 H205 0.9500 . ?
C206 H206 0.9500 . ?
C207 C212 1.394(9) . ?
C207 C208 1.395(10) . ?
C208 C209 1.375(10) . ?
C208 H208 0.9500 . ?
C209 C210 1.371(10) . ?
C209 H209 0.9500 . ?
C210 C211 1.376(11) . ?
C210 H210 0.9500 . ?
C211 C212 1.382(10) . ?
C211 H211 0.9500 . ?
C212 H212 0.9500 . ?
C213 C214 1.373(10) . ?
C213 C218 1.391(11) . ?
C214 C215 1.407(12) . ?
C214 H214 0.9500 . ?
C215 C216 1.348(13) . ?
C215 H215 0.9500 . ?
C216 C217 1.385(14) . ?
C216 H216 0.9500 . ?
C217 C218 1.368(12) . ?
C217 H217 0.9500 . ?
C218 H218 0.9500 . ?
C219 C224 1.389(10) . ?
C219 C220 1.403(10) . ?
C220 C221 1.375(10) . ?
C220 H220 0.9500 . ?
C221 C222 1.371(11) . ?
C221 H221 0.9500 . ?
C222 C223 1.371(11) . ?
C222 H222 0.9500 . ?
C223 C224 1.376(10) . ?
C223 H223 0.9500 . ?
C224 H224 0.9500 . ?
P3 C307 1.788(7) . ?
P3 C313 1.795(8) . ?
P3 C301 1.803(7) . ?
P3 C319 1.807(7) . ?
C301 C302 1.367(10) . ?
C301 C306 1.390(11) . ?
C302 C303 1.389(10) . ?
C302 H302 0.9500 . ?
C303 C304 1.355(12) . ?
C303 H303 0.9500 . ?
C304 C305 1.380(15) . ?
C304 H304 0.9500 . ?
C305 C306 1.371(13) . ?
C305 H305 0.9500 . ?
C306 H306 0.9500 . ?
C307 C312 1.390(10) . ?
C307 C308 1.398(10) . ?
C308 C309 1.380(10) . ?
C308 H308 0.9500 . ?
C309 C310 1.378(11) . ?
C309 H309 0.9500 . ?
C310 C311 1.378(11) . ?
C310 H310 0.9500 . ?
C311 C312 1.387(10) . ?
C311 H311 0.9500 . ?
C312 H312 0.9500 . ?
C313 C314 1.365(12) . ?
C313 C318 1.383(12) . ?
C314 C315 1.390(13) . ?
C314 H314 0.9500 . ?
C315 C316 1.362(16) . ?
C315 H315 0.9500 . ?
C316 C317 1.334(15) . ?
C316 H316 0.9500 . ?
C317 C318 1.381(12) . ?
C317 H317 0.9500 . ?
C318 H318 0.9500 . ?
C319 C324 1.368(11) . ?
C319 C320 1.373(10) . ?
C320 C321 1.393(11) . ?
C320 H320 0.9500 . ?
C321 C322 1.354(12) . ?
C321 H321 0.9500 . ?
C322 C323 1.362(13) . ?
C322 H322 0.9500 . ?
C323 C324 1.374(12) . ?
C323 H323 0.9500 . ?
C324 H324 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 Sn1 105.8(2) . . ?
C1 Pt1 Sn5 101.0(2) . . ?
Sn1 Pt1 Sn5 116.083(16) . . ?
C1 Pt1 Sn3 105.1(2) . . ?
Sn1 Pt1 Sn3 113.783(17) . . ?
Sn5 Pt1 Sn3 113.207(17) . . ?
C1 Pt1 Pt2 148.5(2) . . ?
Sn1 Pt1 Pt2 61.393(12) . . ?
Sn5 Pt1 Pt2 110.518(14) . . ?
Sn3 Pt1 Pt2 61.682(13) . . ?
C1 Pt1 Pt3 144.1(2) . . ?
Sn1 Pt1 Pt3 62.760(12) . . ?
Sn5 Pt1 Pt3 61.638(12) . . ?
Sn3 Pt1 Pt3 110.648(14) . . ?
Pt2 Pt1 Pt3 59.318(9) . . ?
C1 Pt1 Pt4 143.3(2) . . ?
Sn1 Pt1 Pt4 110.858(14) . . ?
Sn5 Pt1 Pt4 61.284(12) . . ?
Sn3 Pt1 Pt4 61.236(12) . . ?
Pt2 Pt1 Pt4 58.794(9) . . ?
Pt3 Pt1 Pt4 58.925(9) . . ?
C2 Pt2 Pt4 146.9(2) . . ?
C2 Pt2 Sn1 99.6(2) . . ?
Pt4 Pt2 Sn1 107.688(13) . . ?
C2 Pt2 Sn3 96.0(2) . . ?
Pt4 Pt2 Sn3 59.956(12) . . ?
Sn1 Pt2 Sn3 103.561(16) . . ?
C2 Pt2 Pt3 153.0(2) . . ?
Pt4 Pt2 Pt3 59.980(8) . . ?
Sn1 Pt2 Pt3 61.192(12) . . ?
Sn3 Pt2 Pt3 106.516(13) . . ?
C2 Pt2 Sn2 99.0(2) . . ?
Pt4 Pt2 Sn2 106.283(13) . . ?
Sn1 Pt2 Sn2 73.859(14) . . ?
Sn3 Pt2 Sn2 165.028(16) . . ?
Pt3 Pt2 Sn2 59.050(11) . . ?
C2 Pt2 Pt1 126.5(2) . . ?
Pt4 Pt2 Pt1 60.858(9) . . ?
Sn1 Pt2 Pt1 55.540(12) . . ?
Sn3 Pt2 Pt1 55.549(12) . . ?
Pt3 Pt2 Pt1 60.437(9) . . ?
Sn2 Pt2 Pt1 113.963(13) . . ?
C2 Pt2 Pt5 122.1(2) . . ?
Pt4 Pt2 Pt5 60.948(9) . . ?
Sn1 Pt2 Pt5 116.408(13) . . ?
Sn3 Pt2 Pt5 115.675(14) . . ?
Pt3 Pt2 Pt5 60.799(9) . . ?
Sn2 Pt2 Pt5 55.461(11) . . ?
Pt1 Pt2 Pt5 111.337(11) . . ?
C2 Pt2 Sn4 94.5(2) . . ?
Pt4 Pt2 Sn4 58.715(12) . . ?
Sn1 Pt2 Sn4 165.883(17) . . ?
Sn3 Pt2 Sn4 73.744(15) . . ?
Pt3 Pt2 Sn4 105.824(13) . . ?
Sn2 Pt2 Sn4 105.042(16) . . ?
Pt1 Pt2 Sn4 114.438(14) . . ?
Pt5 Pt2 Sn4 55.318(11) . . ?
C3 Pt3 Sn2 97.2(2) . . ?
C3 Pt3 Pt4 149.2(2) . . ?
Sn2 Pt3 Pt4 107.345(13) . . ?
C3 Pt3 Sn5 96.5(2) . . ?
Sn2 Pt3 Sn5 166.236(15) . . ?
Pt4 Pt3 Sn5 59.864(11) . . ?
C3 Pt3 Pt2 151.1(2) . . ?
Sn2 Pt3 Pt2 60.701(11) . . ?
Pt4 Pt3 Pt2 59.686(8) . . ?
Sn5 Pt3 Pt2 106.135(13) . . ?
C3 Pt3 Sn6 97.8(2) . . ?
Sn2 Pt3 Sn6 104.290(16) . . ?
Pt4 Pt3 Sn6 58.808(11) . . ?
Sn5 Pt3 Sn6 74.215(15) . . ?
Pt2 Pt3 Sn6 105.418(13) . . ?
C3 Pt3 Pt1 124.4(2) . . ?
Sn2 Pt3 Pt1 115.268(13) . . ?
Pt4 Pt3 Pt1 60.694(9) . . ?
Sn5 Pt3 Pt1 55.391(12) . . ?
Pt2 Pt3 Pt1 60.244(9) . . ?
Sn6 Pt3 Pt1 114.562(13) . . ?
C3 Pt3 Sn1 98.5(2) . . ?
Sn2 Pt3 Sn1 73.665(14) . . ?
Pt4 Pt3 Sn1 105.844(13) . . ?
Sn5 Pt3 Sn1 103.797(16) . . ?
Pt2 Pt3 Sn1 59.115(11) . . ?
Sn6 Pt3 Sn1 163.682(15) . . ?
Pt1 Pt3 Sn1 54.867(11) . . ?
C3 Pt3 Pt5 125.1(2) . . ?
Sn2 Pt3 Pt5 55.724(11) . . ?
Pt4 Pt3 Pt5 60.605(9) . . ?
Sn5 Pt3 Pt5 115.565(13) . . ?
Pt2 Pt3 Pt5 60.083(9) . . ?
Sn6 Pt3 Pt5 55.352(11) . . ?
Pt1 Pt3 Pt5 110.586(10) . . ?
Sn1 Pt3 Pt5 113.900(13) . . ?
C4 Pt4 Sn6 95.3(2) . . ?
C4 Pt4 Sn4 97.7(2) . . ?
Sn6 Pt4 Sn4 103.411(16) . . ?
C4 Pt4 Pt2 151.9(2) . . ?
Sn6 Pt4 Pt2 107.586(14) . . ?
Sn4 Pt4 Pt2 61.725(12) . . ?
C4 Pt4 Sn5 94.3(2) . . ?
Sn6 Pt4 Sn5 75.312(15) . . ?
Sn4 Pt4 Sn5 167.923(17) . . ?
Pt2 Pt4 Sn5 106.897(13) . . ?
C4 Pt4 Sn3 97.5(2) . . ?
Sn6 Pt4 Sn3 167.215(17) . . ?
Sn4 Pt4 Sn3 75.215(15) . . ?
Pt2 Pt4 Sn3 60.318(12) . . ?
Sn5 Pt4 Sn3 103.295(16) . . ?
C4 Pt4 Pt3 147.7(2) . . ?
Sn6 Pt4 Pt3 60.958(12) . . ?
Sn4 Pt4 Pt3 108.436(14) . . ?
Pt2 Pt4 Pt3 60.334(8) . . ?
Sn5 Pt4 Pt3 60.201(12) . . ?
Sn3 Pt4 Pt3 107.069(13) . . ?
C4 Pt4 Pt1 123.4(2) . . ?
Sn6 Pt4 Pt1 116.224(13) . . ?
Sn4 Pt4 Pt1 116.689(14) . . ?
Pt2 Pt4 Pt1 60.349(9) . . ?
Sn5 Pt4 Pt1 55.393(12) . . ?
Sn3 Pt4 Pt1 55.499(11) . . ?
Pt3 Pt4 Pt1 60.381(9) . . ?
C4 Pt4 Pt5 126.1(2) . . ?
Sn6 Pt4 Pt5 56.006(12) . . ?
Sn4 Pt4 Pt5 56.009(12) . . ?
Pt2 Pt4 Pt5 60.325(9) . . ?
Sn5 Pt4 Pt5 115.960(13) . . ?
Sn3 Pt4 Pt5 115.439(14) . . ?
Pt3 Pt4 Pt5 60.704(9) . . ?
Pt1 Pt4 Pt5 110.412(11) . . ?
C5 Pt5 Sn2 103.6(2) . . ?
C5 Pt5 Sn6 106.4(2) . . ?
Sn2 Pt5 Sn6 113.893(16) . . ?
C5 Pt5 Sn4 103.8(2) . . ?
Sn2 Pt5 Sn4 117.217(17) . . ?
Sn6 Pt5 Sn4 110.507(17) . . ?
C5 Pt5 Pt2 143.8(2) . . ?
Sn2 Pt5 Pt2 61.974(12) . . ?
Sn6 Pt5 Pt2 109.722(14) . . ?
Sn4 Pt5 Pt2 62.605(12) . . ?
C5 Pt5 Pt4 146.7(2) . . ?
Sn2 Pt5 Pt4 109.773(14) . . ?
Sn6 Pt5 Pt4 60.155(12) . . ?
Sn4 Pt5 Pt4 60.307(13) . . ?
Pt2 Pt5 Pt4 58.726(9) . . ?
C5 Pt5 Pt3 145.8(2) . . ?
Sn2 Pt5 Pt3 60.555(12) . . ?
Sn6 Pt5 Pt3 61.592(12) . . ?
Sn4 Pt5 Pt3 110.364(14) . . ?
Pt2 Pt5 Pt3 59.117(9) . . ?
Pt4 Pt5 Pt3 58.691(9) . . ?
O11 Sn1 Cl2 92.74(14) . . ?
O11 Sn1 Cl1 92.17(14) . . ?
Cl2 Sn1 Cl1 92.97(7) . . ?
O11 Sn1 Pt1 140.53(12) . . ?
Cl2 Sn1 Pt1 112.11(5) . . ?
Cl1 Sn1 Pt1 115.47(5) . . ?
O11 Sn1 Pt2 85.20(12) . . ?
Cl2 Sn1 Pt2 165.69(5) . . ?
Cl1 Sn1 Pt2 101.25(4) . . ?
Pt1 Sn1 Pt2 63.067(12) . . ?
O11 Sn1 Pt3 81.99(13) . . ?
Cl2 Sn1 Pt3 106.00(5) . . ?
Cl1 Sn1 Pt3 160.33(5) . . ?
Pt1 Sn1 Pt3 62.373(12) . . ?
Pt2 Sn1 Pt3 59.693(11) . . ?
O11 Sn2 Cl3 92.40(13) . . ?
O11 Sn2 Cl4 90.74(14) . . ?
Cl3 Sn2 Cl4 93.43(6) . . ?
O11 Sn2 Pt5 141.55(12) . . ?
Cl3 Sn2 Pt5 113.99(5) . . ?
Cl4 Sn2 Pt5 113.71(5) . . ?
O11 Sn2 Pt3 83.71(13) . . ?
Cl3 Sn2 Pt3 103.96(5) . . ?
Cl4 Sn2 Pt3 161.91(5) . . ?
Pt5 Sn2 Pt3 63.722(13) . . ?
O11 Sn2 Pt2 84.26(12) . . ?
Cl3 Sn2 Pt2 164.09(5) . . ?
Cl4 Sn2 Pt2 102.15(4) . . ?
Pt5 Sn2 Pt2 62.565(12) . . ?
Pt3 Sn2 Pt2 60.249(11) . . ?
O12 Sn3 Cl6 91.52(14) . . ?
O12 Sn3 Cl5 94.84(14) . . ?
Cl6 Sn3 Cl5 93.56(7) . . ?
O12 Sn3 Pt1 140.41(12) . . ?
Cl6 Sn3 Pt1 115.71(5) . . ?
Cl5 Sn3 Pt1 110.48(5) . . ?
O12 Sn3 Pt4 82.13(13) . . ?
Cl6 Sn3 Pt4 162.72(6) . . ?
Cl5 Sn3 Pt4 102.94(5) . . ?
Pt1 Sn3 Pt4 63.265(12) . . ?
O12 Sn3 Pt2 83.97(13) . . ?
Cl6 Sn3 Pt2 103.76(5) . . ?
Cl5 Sn3 Pt2 162.65(5) . . ?
Pt1 Sn3 Pt2 62.770(12) . . ?
Pt4 Sn3 Pt2 59.727(11) . . ?
O12 Sn4 Cl7 92.69(14) . . ?
O12 Sn4 Cl8 93.83(14) . . ?
Cl7 Sn4 Cl8 92.99(7) . . ?
O12 Sn4 Pt5 140.13(12) . . ?
Cl7 Sn4 Pt5 114.65(5) . . ?
Cl8 Sn4 Pt5 112.02(5) . . ?
O12 Sn4 Pt4 82.94(13) . . ?
Cl7 Sn4 Pt4 102.96(6) . . ?
Cl8 Sn4 Pt4 163.84(5) . . ?
Pt5 Sn4 Pt4 63.684(12) . . ?
O12 Sn4 Pt2 82.92(13) . . ?
Cl7 Sn4 Pt2 162.31(6) . . ?
Cl8 Sn4 Pt2 104.37(5) . . ?
Pt5 Sn4 Pt2 62.077(12) . . ?
Pt4 Sn4 Pt2 59.560(11) . . ?
O13 Sn5 Cl10 91.73(14) . . ?
O13 Sn5 Cl9 93.98(14) . . ?
Cl10 Sn5 Cl9 93.55(6) . . ?
O13 Sn5 Pt1 140.27(12) . . ?
Cl10 Sn5 Pt1 113.70(5) . . ?
Cl9 Sn5 Pt1 113.22(5) . . ?
O13 Sn5 Pt4 82.88(12) . . ?
Cl10 Sn5 Pt4 100.96(5) . . ?
Cl9 Sn5 Pt4 165.22(5) . . ?
Pt1 Sn5 Pt4 63.323(12) . . ?
O13 Sn5 Pt3 82.75(13) . . ?
Cl10 Sn5 Pt3 160.56(5) . . ?
Cl9 Sn5 Pt3 105.39(5) . . ?
Pt1 Sn5 Pt3 62.971(13) . . ?
Pt4 Sn5 Pt3 59.935(11) . . ?
O13 Sn6 Cl11 91.53(13) . . ?
O13 Sn6 Cl12 93.97(14) . . ?
Cl11 Sn6 Cl12 91.19(6) . . ?
O13 Sn6 Pt5 140.67(13) . . ?
Cl11 Sn6 Pt5 114.23(5) . . ?
Cl12 Sn6 Pt5 113.58(5) . . ?
O13 Sn6 Pt4 83.64(12) . . ?
Cl11 Sn6 Pt4 165.38(5) . . ?
Cl12 Sn6 Pt4 102.87(4) . . ?
Pt5 Sn6 Pt4 63.839(12) . . ?
O13 Sn6 Pt3 82.25(13) . . ?
Cl11 Sn6 Pt3 105.50(5) . . ?
Cl12 Sn6 Pt3 162.92(5) . . ?
Pt5 Sn6 Pt3 63.056(12) . . ?
Pt4 Sn6 Pt3 60.233(11) . . ?
O1 C1 Pt1 178.4(7) . . ?
O2 C2 Pt2 178.9(7) . . ?
O3 C3 Pt3 178.6(6) . . ?
O4 C4 Pt4 178.9(6) . . ?
O5 C5 Pt5 179.7(9) . . ?
O11 C11 H11A 109.5 . . ?
O11 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
O11 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
O12 C12 H12A 109.5 . . ?
O12 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
O12 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
O13 C13 H13A 109.5 . . ?
O13 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
O13 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
C11 O11 Sn1 126.9(4) . . ?
C11 O11 Sn2 126.6(4) . . ?
Sn1 O11 Sn2 106.56(19) . . ?
C12 O12 Sn4 127.3(4) . . ?
C12 O12 Sn3 124.9(4) . . ?
Sn4 O12 Sn3 107.72(19) . . ?
C13 O13 Sn5 123.8(4) . . ?
C13 O13 Sn6 127.6(5) . . ?
Sn5 O13 Sn6 107.4(2) . . ?
C101 P1 C113 109.7(3) . . ?
C101 P1 C119 111.1(3) . . ?
C113 P1 C119 109.9(3) . . ?
C101 P1 C107 107.9(3) . . ?
C113 P1 C107 110.1(3) . . ?
C119 P1 C107 108.3(3) . . ?
C102 C101 C106 119.2(7) . . ?
C102 C101 P1 119.2(5) . . ?
C106 C101 P1 120.5(5) . . ?
C103 C102 C101 120.2(8) . . ?
C103 C102 H102 119.9 . . ?
C101 C102 H102 119.9 . . ?
C102 C103 C104 119.9(8) . . ?
C102 C103 H103 120.1 . . ?
C104 C103 H103 120.1 . . ?
C105 C104 C103 120.3(8) . . ?
C105 C104 H104 119.8 . . ?
C103 C104 H104 119.8 . . ?
C104 C105 C106 121.0(8) . . ?
C104 C105 H105 119.5 . . ?
C106 C105 H105 119.5 . . ?
C105 C106 C101 119.4(7) . . ?
C105 C106 H106 120.3 . . ?
C101 C106 H106 120.3 . . ?
C112 C107 C108 119.6(7) . . ?
C112 C107 P1 120.1(6) . . ?
C108 C107 P1 120.2(6) . . ?
C107 C108 C109 120.1(9) . . ?
C107 C108 H108 119.9 . . ?
C109 C108 H108 119.9 . . ?
C110 C109 C108 118.7(9) . . ?
C110 C109 H109 120.6 . . ?
C108 C109 H109 120.6 . . ?
C111 C110 C109 120.9(8) . . ?
C111 C110 H110 119.6 . . ?
C109 C110 H110 119.6 . . ?
C110 C111 C112 122.1(9) . . ?
C110 C111 H111 118.9 . . ?
C112 C111 H111 118.9 . . ?
C111 C112 C107 118.5(8) . . ?
C111 C112 H112 120.8 . . ?
C107 C112 H112 120.8 . . ?
C118 C113 C114 119.2(7) . . ?
C118 C113 P1 121.7(5) . . ?
C114 C113 P1 119.1(5) . . ?
C115 C114 C113 119.4(7) . . ?
C115 C114 H114 120.3 . . ?
C113 C114 H114 120.3 . . ?
C114 C115 C116 121.6(7) . . ?
C114 C115 H115 119.2 . . ?
C116 C115 H115 119.2 . . ?
C117 C116 C115 118.9(7) . . ?
C117 C116 H116 120.6 . . ?
C115 C116 H116 120.6 . . ?
C116 C117 C118 121.2(7) . . ?
C116 C117 H117 119.4 . . ?
C118 C117 H117 119.4 . . ?
C117 C118 C113 119.8(7) . . ?
C117 C118 H118 120.1 . . ?
C113 C118 H118 120.1 . . ?
C124 C119 C120 118.3(7) . . ?
C124 C119 P1 120.6(6) . . ?
C120 C119 P1 121.0(6) . . ?
C121 C120 C119 120.3(8) . . ?
C121 C120 H120 119.9 . . ?
C119 C120 H120 119.9 . . ?
C122 C121 C120 119.9(9) . . ?
C122 C121 H121 120.1 . . ?
C120 C121 H121 120.1 . . ?
C123 C122 C121 120.2(8) . . ?
C123 C122 H122 119.9 . . ?
C121 C122 H122 119.9 . . ?
C122 C123 C124 121.1(9) . . ?
C122 C123 H123 119.5 . . ?
C124 C123 H123 119.5 . . ?
C123 C124 C119 120.3(8) . . ?
C123 C124 H124 119.9 . . ?
C119 C124 H124 119.9 . . ?
C207 P2 C213 111.0(3) . . ?
C207 P2 C219 109.8(3) . . ?
C213 P2 C219 108.1(3) . . ?
C207 P2 C201 106.9(3) . . ?
C213 P2 C201 111.0(3) . . ?
C219 P2 C201 110.1(3) . . ?
C206 C201 C202 120.5(6) . . ?
C206 C201 P2 118.4(5) . . ?
C202 C201 P2 121.1(5) . . ?
C203 C202 C201 119.7(7) . . ?
C203 C202 H202 120.1 . . ?
C201 C202 H202 120.1 . . ?
C202 C203 C204 119.0(7) . . ?
C202 C203 H203 120.5 . . ?
C204 C203 H203 120.5 . . ?
C205 C204 C203 122.0(6) . . ?
C205 C204 H204 119.0 . . ?
C203 C204 H204 119.0 . . ?
C204 C205 C206 119.1(7) . . ?
C204 C205 H205 120.5 . . ?
C206 C205 H205 120.5 . . ?
C201 C206 C205 119.8(7) . . ?
C201 C206 H206 120.1 . . ?
C205 C206 H206 120.1 . . ?
C212 C207 C208 120.3(7) . . ?
C212 C207 P2 121.0(6) . . ?
C208 C207 P2 118.7(5) . . ?
C209 C208 C207 119.9(7) . . ?
C209 C208 H208 120.0 . . ?
C207 C208 H208 120.0 . . ?
C210 C209 C208 119.3(7) . . ?
C210 C209 H209 120.4 . . ?
C208 C209 H209 120.4 . . ?
C209 C210 C211 121.7(7) . . ?
C209 C210 H210 119.2 . . ?
C211 C210 H210 119.2 . . ?
C210 C211 C212 119.8(7) . . ?
C210 C211 H211 120.1 . . ?
C212 C211 H211 120.1 . . ?
C211 C212 C207 119.0(7) . . ?
C211 C212 H212 120.5 . . ?
C207 C212 H212 120.5 . . ?
C214 C213 C218 120.0(7) . . ?
C214 C213 P2 120.0(6) . . ?
C218 C213 P2 120.0(6) . . ?
C213 C214 C215 119.2(8) . . ?
C213 C214 H214 120.4 . . ?
C215 C214 H214 120.4 . . ?
C216 C215 C214 120.2(9) . . ?
C216 C215 H215 119.9 . . ?
C214 C215 H215 119.9 . . ?
C215 C216 C217 120.8(9) . . ?
C215 C216 H216 119.6 . . ?
C217 C216 H216 119.6 . . ?
C218 C217 C216 119.7(10) . . ?
C218 C217 H217 120.1 . . ?
C216 C217 H217 120.1 . . ?
C217 C218 C213 120.1(9) . . ?
C217 C218 H218 120.0 . . ?
C213 C218 H218 120.0 . . ?
C224 C219 C220 120.0(7) . . ?
C224 C219 P2 120.2(6) . . ?
C220 C219 P2 119.8(6) . . ?
C221 C220 C219 118.4(7) . . ?
C221 C220 H220 120.8 . . ?
C219 C220 H220 120.8 . . ?
C222 C221 C220 121.2(8) . . ?
C222 C221 H221 119.4 . . ?
C220 C221 H221 119.4 . . ?
C223 C222 C221 120.5(7) . . ?
C223 C222 H222 119.8 . . ?
C221 C222 H222 119.8 . . ?
C222 C223 C224 120.0(8) . . ?
C222 C223 H223 120.0 . . ?
C224 C223 H223 120.0 . . ?
C223 C224 C219 119.9(7) . . ?
C223 C224 H224 120.0 . . ?
C219 C224 H224 120.0 . . ?
C307 P3 C313 107.9(3) . . ?
C307 P3 C301 110.6(3) . . ?
C313 P3 C301 108.3(4) . . ?
C307 P3 C319 106.2(3) . . ?
C313 P3 C319 114.4(4) . . ?
C301 P3 C319 109.4(3) . . ?
C302 C301 C306 120.2(7) . . ?
C302 C301 P3 120.3(6) . . ?
C306 C301 P3 119.5(6) . . ?
C301 C302 C303 119.4(8) . . ?
C301 C302 H302 120.3 . . ?
C303 C302 H302 120.3 . . ?
C304 C303 C302 120.2(9) . . ?
C304 C303 H303 119.9 . . ?
C302 C303 H303 119.9 . . ?
C303 C304 C305 120.8(9) . . ?
C303 C304 H304 119.6 . . ?
C305 C304 H304 119.6 . . ?
C306 C305 C304 119.5(9) . . ?
C306 C305 H305 120.3 . . ?
C304 C305 H305 120.3 . . ?
C305 C306 C301 119.9(9) . . ?
C305 C306 H306 120.1 . . ?
C301 C306 H306 120.1 . . ?
C312 C307 C308 120.2(6) . . ?
C312 C307 P3 121.3(6) . . ?
C308 C307 P3 118.6(5) . . ?
C309 C308 C307 119.0(7) . . ?
C309 C308 H308 120.5 . . ?
C307 C308 H308 120.5 . . ?
C310 C309 C308 120.9(8) . . ?
C310 C309 H309 119.6 . . ?
C308 C309 H309 119.6 . . ?
C309 C310 C311 120.3(7) . . ?
C309 C310 H310 119.8 . . ?
C311 C310 H310 119.8 . . ?
C310 C311 C312 119.9(7) . . ?
C310 C311 H311 120.1 . . ?
C312 C311 H311 120.1 . . ?
C311 C312 C307 119.8(7) . . ?
C311 C312 H312 120.1 . . ?
C307 C312 H312 120.1 . . ?
C314 C313 C318 117.8(8) . . ?
C314 C313 P3 120.4(7) . . ?
C318 C313 P3 121.4(7) . . ?
C313 C314 C315 120.4(10) . . ?
C313 C314 H314 119.8 . . ?
C315 C314 H314 119.8 . . ?
C316 C315 C314 120.5(11) . . ?
C316 C315 H315 119.8 . . ?
C314 C315 H315 119.8 . . ?
C317 C316 C315 119.7(10) . . ?
C317 C316 H316 120.2 . . ?
C315 C316 H316 120.2 . . ?
C316 C317 C318 120.8(10) . . ?
C316 C317 H317 119.6 . . ?
C318 C317 H317 119.6 . . ?
C317 C318 C313 120.8(10) . . ?
C317 C318 H318 119.6 . . ?
C313 C318 H318 119.6 . . ?
C324 C319 C320 119.0(7) . . ?
C324 C319 P3 120.4(6) . . ?
C320 C319 P3 120.3(6) . . ?
C319 C320 C321 119.9(8) . . ?
C319 C320 H320 120.0 . . ?
C321 C320 H320 120.0 . . ?
C322 C321 C320 120.0(8) . . ?
C322 C321 H321 120.0 . . ?
C320 C321 H321 120.0 . . ?
C321 C322 C323 120.3(8) . . ?
C321 C322 H322 119.9 . . ?
C323 C322 H322 119.9 . . ?
C322 C323 C324 120.0(9) . . ?
C322 C323 H323 120.0 . . ?
C324 C323 H323 120.0 . . ?
C319 C324 C323 120.8(8) . . ?
C319 C324 H324 119.6 . . ?
C323 C324 H324 119.6 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 Pt2 C2 2.3(5) . . . . ?
Sn1 Pt1 Pt2 C2 75.1(3) . . . . ?
Sn5 Pt1 Pt2 C2 -175.5(3) . . . . ?
Sn3 Pt1 Pt2 C2 -69.5(3) . . . . ?
Pt3 Pt1 Pt2 C2 148.7(3) . . . . ?
Pt4 Pt1 Pt2 C2 -141.3(3) . . . . ?
C1 Pt1 Pt2 Pt4 143.6(5) . . . . ?
Sn1 Pt1 Pt2 Pt4 -143.565(15) . . . . ?
Sn5 Pt1 Pt2 Pt4 -34.258(14) . . . . ?
Sn3 Pt1 Pt2 Pt4 71.780(14) . . . . ?
Pt3 Pt1 Pt2 Pt4 -69.983(9) . . . . ?
C1 Pt1 Pt2 Sn1 -72.8(5) . . . . ?
Sn5 Pt1 Pt2 Sn1 109.308(18) . . . . ?
Sn3 Pt1 Pt2 Sn1 -144.654(18) . . . . ?
Pt3 Pt1 Pt2 Sn1 73.582(14) . . . . ?
Pt4 Pt1 Pt2 Sn1 143.565(15) . . . . ?
C1 Pt1 Pt2 Sn3 71.8(5) . . . . ?
Sn1 Pt1 Pt2 Sn3 144.654(18) . . . . ?
Sn5 Pt1 Pt2 Sn3 -106.038(18) . . . . ?
Pt3 Pt1 Pt2 Sn3 -141.764(15) . . . . ?
Pt4 Pt1 Pt2 Sn3 -71.780(14) . . . . ?
C1 Pt1 Pt2 Pt3 -146.4(5) . . . . ?
Sn1 Pt1 Pt2 Pt3 -73.582(13) . . . . ?
Sn5 Pt1 Pt2 Pt3 35.726(14) . . . . ?
Sn3 Pt1 Pt2 Pt3 141.764(15) . . . . ?
Pt4 Pt1 Pt2 Pt3 69.983(9) . . . . ?
C1 Pt1 Pt2 Sn2 -120.4(5) . . . . ?
Sn1 Pt1 Pt2 Sn2 -47.625(17) . . . . ?
Sn5 Pt1 Pt2 Sn2 61.682(19) . . . . ?
Sn3 Pt1 Pt2 Sn2 167.720(18) . . . . ?
Pt3 Pt1 Pt2 Sn2 25.956(14) . . . . ?
Pt4 Pt1 Pt2 Sn2 95.940(15) . . . . ?
C1 Pt1 Pt2 Pt5 179.1(5) . . . . ?
Sn1 Pt1 Pt2 Pt5 -108.122(15) . . . . ?
Sn5 Pt1 Pt2 Pt5 1.186(17) . . . . ?
Sn3 Pt1 Pt2 Pt5 107.224(15) . . . . ?
Pt3 Pt1 Pt2 Pt5 -34.540(10) . . . . ?
Pt4 Pt1 Pt2 Pt5 35.444(10) . . . . ?
C1 Pt1 Pt2 Sn4 118.6(5) . . . . ?
Sn1 Pt1 Pt2 Sn4 -168.550(18) . . . . ?
Sn5 Pt1 Pt2 Sn4 -59.243(19) . . . . ?
Sn3 Pt1 Pt2 Sn4 46.796(17) . . . . ?
Pt3 Pt1 Pt2 Sn4 -94.968(15) . . . . ?
Pt4 Pt1 Pt2 Sn4 -24.985(13) . . . . ?
C2 Pt2 Pt3 C3 -5.1(6) . . . . ?
Pt4 Pt2 Pt3 C3 179.4(4) . . . . ?
Sn1 Pt2 Pt3 C3 43.5(4) . . . . ?
Sn3 Pt2 Pt3 C3 140.2(4) . . . . ?
Sn2 Pt2 Pt3 C3 -44.2(4) . . . . ?
Pt1 Pt2 Pt3 C3 108.0(4) . . . . ?
Pt5 Pt2 Pt3 C3 -109.2(4) . . . . ?
Sn4 Pt2 Pt3 C3 -142.5(4) . . . . ?
C2 Pt2 Pt3 Sn2 39.0(5) . . . . ?
Pt4 Pt2 Pt3 Sn2 -136.393(15) . . . . ?
Sn1 Pt2 Pt3 Sn2 87.699(16) . . . . ?
Sn3 Pt2 Pt3 Sn2 -175.637(17) . . . . ?
Pt1 Pt2 Pt3 Sn2 152.201(15) . . . . ?
Pt5 Pt2 Pt3 Sn2 -65.028(13) . . . . ?
Sn4 Pt2 Pt3 Sn2 -98.312(17) . . . . ?
C2 Pt2 Pt3 Pt4 175.4(5) . . . . ?
Sn1 Pt2 Pt3 Pt4 -135.909(15) . . . . ?
Sn3 Pt2 Pt3 Pt4 -39.244(13) . . . . ?
Sn2 Pt2 Pt3 Pt4 136.393(15) . . . . ?
Pt1 Pt2 Pt3 Pt4 -71.406(10) . . . . ?
Pt5 Pt2 Pt3 Pt4 71.365(10) . . . . ?
Sn4 Pt2 Pt3 Pt4 38.080(14) . . . . ?
C2 Pt2 Pt3 Sn5 -145.3(5) . . . . ?
Pt4 Pt2 Pt3 Sn5 39.234(13) . . . . ?
Sn1 Pt2 Pt3 Sn5 -96.675(17) . . . . ?
Sn3 Pt2 Pt3 Sn5 -0.010(18) . . . . ?
Sn2 Pt2 Pt3 Sn5 175.626(18) . . . . ?
Pt1 Pt2 Pt3 Sn5 -32.172(13) . . . . ?
Pt5 Pt2 Pt3 Sn5 110.599(14) . . . . ?
Sn4 Pt2 Pt3 Sn5 77.314(18) . . . . ?
C2 Pt2 Pt3 Sn6 137.0(5) . . . . ?
Pt4 Pt2 Pt3 Sn6 -38.411(13) . . . . ?
Sn1 Pt2 Pt3 Sn6 -174.320(18) . . . . ?
Sn3 Pt2 Pt3 Sn6 -77.655(17) . . . . ?
Sn2 Pt2 Pt3 Sn6 97.981(17) . . . . ?
Pt1 Pt2 Pt3 Sn6 -109.818(14) . . . . ?
Pt5 Pt2 Pt3 Sn6 32.954(13) . . . . ?
Sn4 Pt2 Pt3 Sn6 -0.331(18) . . . . ?
C2 Pt2 Pt3 Pt1 -113.2(5) . . . . ?
Pt4 Pt2 Pt3 Pt1 71.406(10) . . . . ?
Sn1 Pt2 Pt3 Pt1 -64.503(13) . . . . ?
Sn3 Pt2 Pt3 Pt1 32.162(13) . . . . ?
Sn2 Pt2 Pt3 Pt1 -152.201(15) . . . . ?
Pt5 Pt2 Pt3 Pt1 142.771(11) . . . . ?
Sn4 Pt2 Pt3 Pt1 109.487(15) . . . . ?
C2 Pt2 Pt3 Sn1 -48.7(5) . . . . ?
Pt4 Pt2 Pt3 Sn1 135.909(15) . . . . ?
Sn3 Pt2 Pt3 Sn1 96.665(17) . . . . ?
Sn2 Pt2 Pt3 Sn1 -87.699(16) . . . . ?
Pt1 Pt2 Pt3 Sn1 64.503(13) . . . . ?
Pt5 Pt2 Pt3 Sn1 -152.726(15) . . . . ?
Sn4 Pt2 Pt3 Sn1 173.989(18) . . . . ?
C2 Pt2 Pt3 Pt5 104.1(5) . . . . ?
Pt4 Pt2 Pt3 Pt5 -71.365(10) . . . . ?
Sn1 Pt2 Pt3 Pt5 152.726(15) . . . . ?
Sn3 Pt2 Pt3 Pt5 -110.609(14) . . . . ?
Sn2 Pt2 Pt3 Pt5 65.028(13) . . . . ?
Pt1 Pt2 Pt3 Pt5 -142.771(11) . . . . ?
Sn4 Pt2 Pt3 Pt5 -33.284(13) . . . . ?
C1 Pt1 Pt3 C3 4.3(5) . . . . ?
Sn1 Pt1 Pt3 C3 -74.9(3) . . . . ?
Sn5 Pt1 Pt3 C3 72.3(3) . . . . ?
Sn3 Pt1 Pt3 C3 178.2(3) . . . . ?
Pt2 Pt1 Pt3 C3 -146.1(3) . . . . ?
Pt4 Pt1 Pt3 C3 144.1(3) . . . . ?
C1 Pt1 Pt3 Sn2 123.7(4) . . . . ?
Sn1 Pt1 Pt3 Sn2 44.567(17) . . . . ?
Sn5 Pt1 Pt3 Sn2 -168.304(18) . . . . ?
Sn3 Pt1 Pt3 Sn2 -62.33(2) . . . . ?
Pt2 Pt1 Pt3 Sn2 -26.727(14) . . . . ?
Pt4 Pt1 Pt3 Sn2 -96.494(15) . . . . ?
C1 Pt1 Pt3 Pt4 -139.8(4) . . . . ?
Sn1 Pt1 Pt3 Pt4 141.060(15) . . . . ?
Sn5 Pt1 Pt3 Pt4 -71.810(13) . . . . ?
Sn3 Pt1 Pt3 Pt4 34.159(15) . . . . ?
Pt2 Pt1 Pt3 Pt4 69.767(9) . . . . ?
C1 Pt1 Pt3 Sn5 -68.0(4) . . . . ?
Sn1 Pt1 Pt3 Sn5 -147.129(17) . . . . ?
Sn3 Pt1 Pt3 Sn5 105.969(18) . . . . ?
Pt2 Pt1 Pt3 Sn5 141.577(15) . . . . ?
Pt4 Pt1 Pt3 Sn5 71.810(13) . . . . ?
C1 Pt1 Pt3 Pt2 150.4(4) . . . . ?
Sn1 Pt1 Pt3 Pt2 71.293(13) . . . . ?
Sn5 Pt1 Pt3 Pt2 -141.577(15) . . . . ?
Sn3 Pt1 Pt3 Pt2 -35.608(15) . . . . ?
Pt4 Pt1 Pt3 Pt2 -69.767(9) . . . . ?
C1 Pt1 Pt3 Sn6 -115.2(4) . . . . ?
Sn1 Pt1 Pt3 Sn6 165.619(18) . . . . ?
Sn5 Pt1 Pt3 Sn6 -47.252(17) . . . . ?
Sn3 Pt1 Pt3 Sn6 58.72(2) . . . . ?
Pt2 Pt1 Pt3 Sn6 94.325(15) . . . . ?
Pt4 Pt1 Pt3 Sn6 24.558(13) . . . . ?
C1 Pt1 Pt3 Sn1 79.2(4) . . . . ?
Sn5 Pt1 Pt3 Sn1 147.129(17) . . . . ?
Sn3 Pt1 Pt3 Sn1 -106.901(19) . . . . ?
Pt2 Pt1 Pt3 Sn1 -71.293(13) . . . . ?
Pt4 Pt1 Pt3 Sn1 -141.060(15) . . . . ?
C1 Pt1 Pt3 Pt5 -175.5(4) . . . . ?
Sn1 Pt1 Pt3 Pt5 105.360(15) . . . . ?
Sn5 Pt1 Pt3 Pt5 -107.511(15) . . . . ?
Sn3 Pt1 Pt3 Pt5 -1.542(18) . . . . ?
Pt2 Pt1 Pt3 Pt5 34.066(10) . . . . ?
Pt4 Pt1 Pt3 Pt5 -35.701(10) . . . . ?
C2 Pt2 Pt4 C4 6.8(6) . . . . ?
Sn1 Pt2 Pt4 C4 -137.2(5) . . . . ?
Sn3 Pt2 Pt4 C4 -41.5(5) . . . . ?
Pt3 Pt2 Pt4 C4 -177.0(5) . . . . ?
Sn2 Pt2 Pt4 C4 145.0(5) . . . . ?
Pt1 Pt2 Pt4 C4 -106.3(5) . . . . ?
Pt5 Pt2 Pt4 C4 111.9(5) . . . . ?
Sn4 Pt2 Pt4 C4 47.0(5) . . . . ?
C2 Pt2 Pt4 Sn6 -136.3(4) . . . . ?
Sn1 Pt2 Pt4 Sn6 79.739(18) . . . . ?
Sn3 Pt2 Pt4 Sn6 175.471(18) . . . . ?
Pt3 Pt2 Pt4 Sn6 39.951(13) . . . . ?
Sn2 Pt2 Pt4 Sn6 1.910(18) . . . . ?
Pt1 Pt2 Pt4 Sn6 110.669(14) . . . . ?
Pt5 Pt2 Pt4 Sn6 -31.169(13) . . . . ?
Sn4 Pt2 Pt4 Sn6 -96.073(17) . . . . ?
C2 Pt2 Pt4 Sn4 -40.2(4) . . . . ?
Sn1 Pt2 Pt4 Sn4 175.812(17) . . . . ?
Sn3 Pt2 Pt4 Sn4 -88.456(16) . . . . ?
Pt3 Pt2 Pt4 Sn4 136.024(15) . . . . ?
Sn2 Pt2 Pt4 Sn4 97.983(17) . . . . ?
Pt1 Pt2 Pt4 Sn4 -153.259(14) . . . . ?
Pt5 Pt2 Pt4 Sn4 64.904(13) . . . . ?
C2 Pt2 Pt4 Sn5 144.2(4) . . . . ?
Sn1 Pt2 Pt4 Sn5 0.209(18) . . . . ?
Sn3 Pt2 Pt4 Sn5 95.941(17) . . . . ?
Pt3 Pt2 Pt4 Sn5 -39.579(13) . . . . ?
Sn2 Pt2 Pt4 Sn5 -77.620(17) . . . . ?
Pt1 Pt2 Pt4 Sn5 31.138(13) . . . . ?
Pt5 Pt2 Pt4 Sn5 -110.699(14) . . . . ?
Sn4 Pt2 Pt4 Sn5 -175.603(18) . . . . ?
C2 Pt2 Pt4 Sn3 48.3(4) . . . . ?
Sn1 Pt2 Pt4 Sn3 -95.732(17) . . . . ?
Pt3 Pt2 Pt4 Sn3 -135.519(15) . . . . ?
Sn2 Pt2 Pt4 Sn3 -173.560(17) . . . . ?
Pt1 Pt2 Pt4 Sn3 -64.802(13) . . . . ?
Pt5 Pt2 Pt4 Sn3 153.360(14) . . . . ?
Sn4 Pt2 Pt4 Sn3 88.456(16) . . . . ?
C2 Pt2 Pt4 Pt3 -176.2(4) . . . . ?
Sn1 Pt2 Pt4 Pt3 39.788(13) . . . . ?
Sn3 Pt2 Pt4 Pt3 135.519(15) . . . . ?
Sn2 Pt2 Pt4 Pt3 -38.041(13) . . . . ?
Pt1 Pt2 Pt4 Pt3 70.717(9) . . . . ?
Pt5 Pt2 Pt4 Pt3 -71.120(9) . . . . ?
Sn4 Pt2 Pt4 Pt3 -136.024(15) . . . . ?
C2 Pt2 Pt4 Pt1 113.1(4) . . . . ?
Sn1 Pt2 Pt4 Pt1 -30.930(13) . . . . ?
Sn3 Pt2 Pt4 Pt1 64.802(13) . . . . ?
Pt3 Pt2 Pt4 Pt1 -70.717(9) . . . . ?
Sn2 Pt2 Pt4 Pt1 -108.758(14) . . . . ?
Pt5 Pt2 Pt4 Pt1 -141.837(10) . . . . ?
Sn4 Pt2 Pt4 Pt1 153.259(14) . . . . ?
C2 Pt2 Pt4 Pt5 -105.1(4) . . . . ?
Sn1 Pt2 Pt4 Pt5 110.908(14) . . . . ?
Sn3 Pt2 Pt4 Pt5 -153.360(14) . . . . ?
Pt3 Pt2 Pt4 Pt5 71.120(9) . . . . ?
Sn2 Pt2 Pt4 Pt5 33.079(12) . . . . ?
Pt1 Pt2 Pt4 Pt5 141.837(10) . . . . ?
Sn4 Pt2 Pt4 Pt5 -64.904(13) . . . . ?
C3 Pt3 Pt4 C4 -2.1(6) . . . . ?
Sn2 Pt3 Pt4 C4 -143.6(4) . . . . ?
Sn5 Pt3 Pt4 C4 42.0(4) . . . . ?
Pt2 Pt3 Pt4 C4 177.3(4) . . . . ?
Sn6 Pt3 Pt4 C4 -47.1(4) . . . . ?
Pt1 Pt3 Pt4 C4 106.7(4) . . . . ?
Sn1 Pt3 Pt4 C4 139.0(4) . . . . ?
Pt5 Pt3 Pt4 C4 -112.1(4) . . . . ?
C3 Pt3 Pt4 Sn6 45.0(4) . . . . ?
Sn2 Pt3 Pt4 Sn6 -96.500(17) . . . . ?
Sn5 Pt3 Pt4 Sn6 89.070(16) . . . . ?
Pt2 Pt3 Pt4 Sn6 -135.560(15) . . . . ?
Pt1 Pt3 Pt4 Sn6 153.775(15) . . . . ?
Sn1 Pt3 Pt4 Sn6 -173.928(18) . . . . ?
Pt5 Pt3 Pt4 Sn6 -65.055(13) . . . . ?
C3 Pt3 Pt4 Sn4 140.4(4) . . . . ?
Sn2 Pt3 Pt4 Sn4 -1.074(19) . . . . ?
Sn5 Pt3 Pt4 Sn4 -175.505(18) . . . . ?
Pt2 Pt3 Pt4 Sn4 -40.135(14) . . . . ?
Sn6 Pt3 Pt4 Sn4 95.425(18) . . . . ?
Pt1 Pt3 Pt4 Sn4 -110.799(15) . . . . ?
Sn1 Pt3 Pt4 Sn4 -78.503(18) . . . . ?
Pt5 Pt3 Pt4 Sn4 30.371(14) . . . . ?
C3 Pt3 Pt4 Pt2 -179.5(4) . . . . ?
Sn2 Pt3 Pt4 Pt2 39.060(13) . . . . ?
Sn5 Pt3 Pt4 Pt2 -135.370(15) . . . . ?
Sn6 Pt3 Pt4 Pt2 135.560(15) . . . . ?
Pt1 Pt3 Pt4 Pt2 -70.665(10) . . . . ?
Sn1 Pt3 Pt4 Pt2 -38.368(13) . . . . ?
Pt5 Pt3 Pt4 Pt2 70.505(10) . . . . ?
C3 Pt3 Pt4 Sn5 -44.1(4) . . . . ?
Sn2 Pt3 Pt4 Sn5 174.430(18) . . . . ?
Pt2 Pt3 Pt4 Sn5 135.370(15) . . . . ?
Sn6 Pt3 Pt4 Sn5 -89.070(16) . . . . ?
Pt1 Pt3 Pt4 Sn5 64.706(13) . . . . ?
Sn1 Pt3 Pt4 Sn5 97.002(17) . . . . ?
Pt5 Pt3 Pt4 Sn5 -154.124(15) . . . . ?
C3 Pt3 Pt4 Sn3 -139.9(4) . . . . ?
Sn2 Pt3 Pt4 Sn3 78.612(18) . . . . ?
Sn5 Pt3 Pt4 Sn3 -95.818(17) . . . . ?
Pt2 Pt3 Pt4 Sn3 39.552(14) . . . . ?
Sn6 Pt3 Pt4 Sn3 175.112(18) . . . . ?
Pt1 Pt3 Pt4 Sn3 -31.112(13) . . . . ?
Sn1 Pt3 Pt4 Sn3 1.184(18) . . . . ?
Pt5 Pt3 Pt4 Sn3 110.058(15) . . . . ?
C3 Pt3 Pt4 Pt1 -108.8(4) . . . . ?
Sn2 Pt3 Pt4 Pt1 109.725(14) . . . . ?
Sn5 Pt3 Pt4 Pt1 -64.706(13) . . . . ?
Pt2 Pt3 Pt4 Pt1 70.665(10) . . . . ?
Sn6 Pt3 Pt4 Pt1 -153.775(15) . . . . ?
Sn1 Pt3 Pt4 Pt1 32.296(13) . . . . ?
Pt5 Pt3 Pt4 Pt1 141.170(11) . . . . ?
C3 Pt3 Pt4 Pt5 110.0(4) . . . . ?
Sn2 Pt3 Pt4 Pt5 -31.445(13) . . . . ?
Sn5 Pt3 Pt4 Pt5 154.124(15) . . . . ?
Pt2 Pt3 Pt4 Pt5 -70.505(10) . . . . ?
Sn6 Pt3 Pt4 Pt5 65.055(13) . . . . ?
Pt1 Pt3 Pt4 Pt5 -141.170(11) . . . . ?
Sn1 Pt3 Pt4 Pt5 -108.874(14) . . . . ?
C1 Pt1 Pt4 C4 -1.5(4) . . . . ?
Sn1 Pt1 Pt4 C4 -178.9(2) . . . . ?
Sn5 Pt1 Pt4 C4 -69.8(2) . . . . ?
Sn3 Pt1 Pt4 C4 74.6(2) . . . . ?
Pt2 Pt1 Pt4 C4 147.2(2) . . . . ?
Pt3 Pt1 Pt4 C4 -142.2(2) . . . . ?
C1 Pt1 Pt4 Sn6 115.1(4) . . . . ?
Sn1 Pt1 Pt4 Sn6 -62.23(2) . . . . ?
Sn5 Pt1 Pt4 Sn6 46.898(18) . . . . ?
Sn3 Pt1 Pt4 Sn6 -168.684(19) . . . . ?
Pt2 Pt1 Pt4 Sn6 -96.151(15) . . . . ?
Pt3 Pt1 Pt4 Sn6 -25.509(14) . . . . ?
C1 Pt1 Pt4 Sn4 -122.4(4) . . . . ?
Sn1 Pt1 Pt4 Sn4 60.245(19) . . . . ?
Sn5 Pt1 Pt4 Sn4 169.378(19) . . . . ?
Sn3 Pt1 Pt4 Sn4 -46.204(18) . . . . ?
Pt2 Pt1 Pt4 Sn4 26.329(14) . . . . ?
Pt3 Pt1 Pt4 Sn4 96.971(16) . . . . ?
C1 Pt1 Pt4 Pt2 -148.7(4) . . . . ?
Sn1 Pt1 Pt4 Pt2 33.916(14) . . . . ?
Sn5 Pt1 Pt4 Pt2 143.048(15) . . . . ?
Sn3 Pt1 Pt4 Pt2 -72.533(14) . . . . ?
Pt3 Pt1 Pt4 Pt2 70.641(9) . . . . ?
C1 Pt1 Pt4 Sn5 68.2(4) . . . . ?
Sn1 Pt1 Pt4 Sn5 -109.133(18) . . . . ?
Sn3 Pt1 Pt4 Sn5 144.419(18) . . . . ?
Pt2 Pt1 Pt4 Sn5 -143.048(15) . . . . ?
Pt3 Pt1 Pt4 Sn5 -72.407(14) . . . . ?
C1 Pt1 Pt4 Sn3 -76.2(4) . . . . ?
Sn1 Pt1 Pt4 Sn3 106.449(19) . . . . ?
Sn5 Pt1 Pt4 Sn3 -144.419(18) . . . . ?
Pt2 Pt1 Pt4 Sn3 72.533(14) . . . . ?
Pt3 Pt1 Pt4 Sn3 143.174(16) . . . . ?
C1 Pt1 Pt4 Pt3 140.6(4) . . . . ?
Sn1 Pt1 Pt4 Pt3 -36.726(14) . . . . ?
Sn5 Pt1 Pt4 Pt3 72.407(14) . . . . ?
Sn3 Pt1 Pt4 Pt3 -143.174(16) . . . . ?
Pt2 Pt1 Pt4 Pt3 -70.641(9) . . . . ?
C1 Pt1 Pt4 Pt5 176.3(4) . . . . ?
Sn1 Pt1 Pt4 Pt5 -1.032(17) . . . . ?
Sn5 Pt1 Pt4 Pt5 108.101(15) . . . . ?
Sn3 Pt1 Pt4 Pt5 -107.481(16) . . . . ?
Pt2 Pt1 Pt4 Pt5 -34.948(10) . . . . ?
Pt3 Pt1 Pt4 Pt5 35.694(10) . . . . ?
C2 Pt2 Pt5 C5 -4.1(5) . . . . ?
Pt4 Pt2 Pt5 C5 -145.6(4) . . . . ?
Sn1 Pt2 Pt5 C5 117.9(4) . . . . ?
Sn3 Pt2 Pt5 C5 -120.1(4) . . . . ?
Pt3 Pt2 Pt5 C5 144.6(4) . . . . ?
Sn2 Pt2 Pt5 C5 73.9(4) . . . . ?
Pt1 Pt2 Pt5 C5 179.0(4) . . . . ?
Sn4 Pt2 Pt5 C5 -75.4(4) . . . . ?
C2 Pt2 Pt5 Sn2 -78.0(2) . . . . ?
Pt4 Pt2 Pt5 Sn2 140.505(14) . . . . ?
Sn1 Pt2 Pt5 Sn2 44.063(18) . . . . ?
Sn3 Pt2 Pt5 Sn2 166.014(18) . . . . ?
Pt3 Pt2 Pt5 Sn2 70.698(13) . . . . ?
Pt1 Pt2 Pt5 Sn2 105.098(15) . . . . ?
Sn4 Pt2 Pt5 Sn2 -149.250(18) . . . . ?
C2 Pt2 Pt5 Sn6 174.7(2) . . . . ?
Pt4 Pt2 Pt5 Sn6 33.252(13) . . . . ?
Sn1 Pt2 Pt5 Sn6 -63.191(19) . . . . ?
Sn3 Pt2 Pt5 Sn6 58.761(19) . . . . ?
Pt3 Pt2 Pt5 Sn6 -36.556(13) . . . . ?
Sn2 Pt2 Pt5 Sn6 -107.254(17) . . . . ?
Pt1 Pt2 Pt5 Sn6 -2.156(17) . . . . ?
Sn4 Pt2 Pt5 Sn6 103.497(18) . . . . ?
C2 Pt2 Pt5 Sn4 71.3(2) . . . . ?
Pt4 Pt2 Pt5 Sn4 -70.245(14) . . . . ?
Sn1 Pt2 Pt5 Sn4 -166.688(19) . . . . ?
Sn3 Pt2 Pt5 Sn4 -44.736(18) . . . . ?
Pt3 Pt2 Pt5 Sn4 -140.053(16) . . . . ?
Sn2 Pt2 Pt5 Sn4 149.250(18) . . . . ?
Pt1 Pt2 Pt5 Sn4 -105.653(16) . . . . ?
C2 Pt2 Pt5 Pt4 141.5(2) . . . . ?
Sn1 Pt2 Pt5 Pt4 -96.443(15) . . . . ?
Sn3 Pt2 Pt5 Pt4 25.509(14) . . . . ?
Pt3 Pt2 Pt5 Pt4 -69.808(9) . . . . ?
Sn2 Pt2 Pt5 Pt4 -140.505(14) . . . . ?
Pt1 Pt2 Pt5 Pt4 -35.408(10) . . . . ?
Sn4 Pt2 Pt5 Pt4 70.245(14) . . . . ?
C2 Pt2 Pt5 Pt3 -148.7(2) . . . . ?
Pt4 Pt2 Pt5 Pt3 69.808(9) . . . . ?
Sn1 Pt2 Pt5 Pt3 -26.635(14) . . . . ?
Sn3 Pt2 Pt5 Pt3 95.317(15) . . . . ?
Sn2 Pt2 Pt5 Pt3 -70.698(13) . . . . ?
Pt1 Pt2 Pt5 Pt3 34.400(10) . . . . ?
Sn4 Pt2 Pt5 Pt3 140.053(16) . . . . ?
C4 Pt4 Pt5 C5 -4.6(5) . . . . ?
Sn6 Pt4 Pt5 C5 -73.9(4) . . . . ?
Sn4 Pt4 Pt5 C5 68.5(4) . . . . ?
Pt2 Pt4 Pt5 C5 142.7(4) . . . . ?
Sn5 Pt4 Pt5 C5 -121.9(4) . . . . ?
Sn3 Pt4 Pt5 C5 117.1(4) . . . . ?
Pt3 Pt4 Pt5 C5 -146.8(4) . . . . ?
Pt1 Pt4 Pt5 C5 177.6(4) . . . . ?
C4 Pt4 Pt5 Sn2 176.1(2) . . . . ?
Sn6 Pt4 Pt5 Sn2 106.855(18) . . . . ?
Sn4 Pt4 Pt5 Sn2 -110.762(18) . . . . ?
Pt2 Pt4 Pt5 Sn2 -36.627(13) . . . . ?
Sn5 Pt4 Pt5 Sn2 58.805(19) . . . . ?
Sn3 Pt4 Pt5 Sn2 -62.181(19) . . . . ?
Pt3 Pt4 Pt5 Sn2 33.893(13) . . . . ?
Pt1 Pt4 Pt5 Sn2 -1.670(17) . . . . ?
C4 Pt4 Pt5 Sn6 69.3(2) . . . . ?
Sn4 Pt4 Pt5 Sn6 142.383(18) . . . . ?
Pt2 Pt4 Pt5 Sn6 -143.482(15) . . . . ?
Sn5 Pt4 Pt5 Sn6 -48.051(18) . . . . ?
Sn3 Pt4 Pt5 Sn6 -169.036(18) . . . . ?
Pt3 Pt4 Pt5 Sn6 -72.962(13) . . . . ?
Pt1 Pt4 Pt5 Sn6 -108.525(15) . . . . ?
C4 Pt4 Pt5 Sn4 -73.1(2) . . . . ?
Sn6 Pt4 Pt5 Sn4 -142.383(18) . . . . ?
Pt2 Pt4 Pt5 Sn4 74.135(14) . . . . ?
Sn5 Pt4 Pt5 Sn4 169.566(19) . . . . ?
Sn3 Pt4 Pt5 Sn4 48.581(18) . . . . ?
Pt3 Pt4 Pt5 Sn4 144.655(16) . . . . ?
Pt1 Pt4 Pt5 Sn4 109.092(16) . . . . ?
C4 Pt4 Pt5 Pt2 -147.2(2) . . . . ?
Sn6 Pt4 Pt5 Pt2 143.482(15) . . . . ?
Sn4 Pt4 Pt5 Pt2 -74.135(14) . . . . ?
Sn5 Pt4 Pt5 Pt2 95.431(15) . . . . ?
Sn3 Pt4 Pt5 Pt2 -25.554(13) . . . . ?
Pt3 Pt4 Pt5 Pt2 70.520(9) . . . . ?
Pt1 Pt4 Pt5 Pt2 34.957(10) . . . . ?
C4 Pt4 Pt5 Pt3 142.2(2) . . . . ?
Sn6 Pt4 Pt5 Pt3 72.962(13) . . . . ?
Sn4 Pt4 Pt5 Pt3 -144.655(16) . . . . ?
Pt2 Pt4 Pt5 Pt3 -70.520(9) . . . . ?
Sn5 Pt4 Pt5 Pt3 24.911(14) . . . . ?
Sn3 Pt4 Pt5 Pt3 -96.074(15) . . . . ?
Pt1 Pt4 Pt5 Pt3 -35.563(10) . . . . ?
C3 Pt3 Pt5 C5 3.6(5) . . . . ?
Sn2 Pt3 Pt5 C5 -69.4(4) . . . . ?
Pt4 Pt3 Pt5 C5 147.6(4) . . . . ?
Sn5 Pt3 Pt5 C5 122.9(4) . . . . ?
Pt2 Pt3 Pt5 C5 -142.5(4) . . . . ?
Sn6 Pt3 Pt5 C5 77.1(4) . . . . ?
Pt1 Pt3 Pt5 C5 -176.6(4) . . . . ?
Sn1 Pt3 Pt5 C5 -117.0(4) . . . . ?
C3 Pt3 Pt5 Sn2 73.0(3) . . . . ?
Pt4 Pt3 Pt5 Sn2 -142.943(15) . . . . ?
Sn5 Pt3 Pt5 Sn2 -167.676(18) . . . . ?
Pt2 Pt3 Pt5 Sn2 -73.077(13) . . . . ?
Sn6 Pt3 Pt5 Sn2 146.523(17) . . . . ?
Pt1 Pt3 Pt5 Sn2 -107.206(15) . . . . ?
Sn1 Pt3 Pt5 Sn2 -47.600(17) . . . . ?
C3 Pt3 Pt5 Sn6 -73.5(3) . . . . ?
Sn2 Pt3 Pt5 Sn6 -146.523(17) . . . . ?
Pt4 Pt3 Pt5 Sn6 70.534(13) . . . . ?
Sn5 Pt3 Pt5 Sn6 45.801(17) . . . . ?
Pt2 Pt3 Pt5 Sn6 140.400(15) . . . . ?
Pt1 Pt3 Pt5 Sn6 106.271(15) . . . . ?
Sn1 Pt3 Pt5 Sn6 165.876(18) . . . . ?
C3 Pt3 Pt5 Sn4 -176.5(3) . . . . ?
Sn2 Pt3 Pt5 Sn4 110.528(19) . . . . ?
Pt4 Pt3 Pt5 Sn4 -32.414(15) . . . . ?
Sn5 Pt3 Pt5 Sn4 -57.15(2) . . . . ?
Pt2 Pt3 Pt5 Sn4 37.451(15) . . . . ?
Sn6 Pt3 Pt5 Sn4 -102.949(18) . . . . ?
Pt1 Pt3 Pt5 Sn4 3.322(18) . . . . ?
Sn1 Pt3 Pt5 Sn4 62.928(19) . . . . ?
C3 Pt3 Pt5 Pt2 146.1(3) . . . . ?
Sn2 Pt3 Pt5 Pt2 73.077(13) . . . . ?
Pt4 Pt3 Pt5 Pt2 -69.865(9) . . . . ?
Sn5 Pt3 Pt5 Pt2 -94.599(15) . . . . ?
Sn6 Pt3 Pt5 Pt2 -140.400(15) . . . . ?
Pt1 Pt3 Pt5 Pt2 -34.129(10) . . . . ?
Sn1 Pt3 Pt5 Pt2 25.477(13) . . . . ?
C3 Pt3 Pt5 Pt4 -144.0(3) . . . . ?
Sn2 Pt3 Pt5 Pt4 142.943(15) . . . . ?
Sn5 Pt3 Pt5 Pt4 -24.733(14) . . . . ?
Pt2 Pt3 Pt5 Pt4 69.865(9) . . . . ?
Sn6 Pt3 Pt5 Pt4 -70.534(13) . . . . ?
Pt1 Pt3 Pt5 Pt4 35.737(10) . . . . ?
Sn1 Pt3 Pt5 Pt4 95.342(14) . . . . ?
C1 Pt1 Sn1 O11 -171.2(3) . . . . ?
Sn5 Pt1 Sn1 O11 -60.1(2) . . . . ?
Sn3 Pt1 Sn1 O11 73.9(2) . . . . ?
Pt2 Pt1 Sn1 O11 40.1(2) . . . . ?
Pt3 Pt1 Sn1 O11 -28.0(2) . . . . ?
Pt4 Pt1 Sn1 O11 7.2(2) . . . . ?
C1 Pt1 Sn1 Cl2 -46.1(2) . . . . ?
Sn5 Pt1 Sn1 Cl2 64.96(6) . . . . ?
Sn3 Pt1 Sn1 Cl2 -161.00(5) . . . . ?
Pt2 Pt1 Sn1 Cl2 165.18(5) . . . . ?
Pt3 Pt1 Sn1 Cl2 97.08(5) . . . . ?
Pt4 Pt1 Sn1 Cl2 132.25(5) . . . . ?
C1 Pt1 Sn1 Cl1 58.7(2) . . . . ?
Sn5 Pt1 Sn1 Cl1 169.76(5) . . . . ?
Sn3 Pt1 Sn1 Cl1 -56.20(5) . . . . ?
Pt2 Pt1 Sn1 Cl1 -90.01(5) . . . . ?
Pt3 Pt1 Sn1 Cl1 -158.12(5) . . . . ?
Pt4 Pt1 Sn1 Cl1 -122.94(5) . . . . ?
C1 Pt1 Sn1 Pt2 148.7(2) . . . . ?
Sn5 Pt1 Sn1 Pt2 -100.226(17) . . . . ?
Sn3 Pt1 Sn1 Pt2 33.817(17) . . . . ?
Pt3 Pt1 Sn1 Pt2 -68.102(10) . . . . ?
Pt4 Pt1 Sn1 Pt2 -32.929(13) . . . . ?
C1 Pt1 Sn1 Pt3 -143.2(2) . . . . ?
Sn5 Pt1 Sn1 Pt3 -32.124(17) . . . . ?
Sn3 Pt1 Sn1 Pt3 101.919(17) . . . . ?
Pt2 Pt1 Sn1 Pt3 68.102(10) . . . . ?
Pt4 Pt1 Sn1 Pt3 35.174(12) . . . . ?
C2 Pt2 Sn1 O11 76.3(3) . . . . ?
Pt4 Pt2 Sn1 O11 -122.74(13) . . . . ?
Sn3 Pt2 Sn1 O11 174.88(13) . . . . ?
Pt3 Pt2 Sn1 O11 -83.52(13) . . . . ?
Sn2 Pt2 Sn1 O11 -20.38(13) . . . . ?
Pt1 Pt2 Sn1 O11 -155.73(13) . . . . ?
Pt5 Pt2 Sn1 O11 -56.99(13) . . . . ?
Sn4 Pt2 Sn1 O11 -107.92(15) . . . . ?
C2 Pt2 Sn1 Cl2 158.5(3) . . . . ?
Pt4 Pt2 Sn1 Cl2 -40.5(2) . . . . ?
Sn3 Pt2 Sn1 Cl2 -102.9(2) . . . . ?
Pt3 Pt2 Sn1 Cl2 -1.3(2) . . . . ?
Sn2 Pt2 Sn1 Cl2 61.9(2) . . . . ?
Pt1 Pt2 Sn1 Cl2 -73.5(2) . . . . ?
Pt5 Pt2 Sn1 Cl2 25.2(2) . . . . ?
Sn4 Pt2 Sn1 Cl2 -25.7(2) . . . . ?
C2 Pt2 Sn1 Cl1 -15.0(2) . . . . ?
Pt4 Pt2 Sn1 Cl1 145.99(5) . . . . ?
Sn3 Pt2 Sn1 Cl1 83.62(5) . . . . ?
Pt3 Pt2 Sn1 Cl1 -174.78(5) . . . . ?
Sn2 Pt2 Sn1 Cl1 -111.64(5) . . . . ?
Pt1 Pt2 Sn1 Cl1 113.01(5) . . . . ?
Pt5 Pt2 Sn1 Cl1 -148.25(5) . . . . ?
Sn4 Pt2 Sn1 Cl1 160.82(7) . . . . ?
C2 Pt2 Sn1 Pt1 -128.0(2) . . . . ?
Pt4 Pt2 Sn1 Pt1 32.988(13) . . . . ?
Sn3 Pt2 Sn1 Pt1 -29.388(15) . . . . ?
Pt3 Pt2 Sn1 Pt1 72.212(11) . . . . ?
Sn2 Pt2 Sn1 Pt1 135.349(16) . . . . ?
Pt5 Pt2 Sn1 Pt1 98.738(14) . . . . ?
Sn4 Pt2 Sn1 Pt1 47.81(7) . . . . ?
C2 Pt2 Sn1 Pt3 159.8(2) . . . . ?
Pt4 Pt2 Sn1 Pt3 -39.224(12) . . . . ?
Sn3 Pt2 Sn1 Pt3 -101.600(15) . . . . ?
Sn2 Pt2 Sn1 Pt3 63.137(13) . . . . ?
Pt1 Pt2 Sn1 Pt3 -72.212(11) . . . . ?
Pt5 Pt2 Sn1 Pt3 26.526(14) . . . . ?
Sn4 Pt2 Sn1 Pt3 -24.40(7) . . . . ?
C3 Pt3 Sn1 O11 -71.2(3) . . . . ?
Sn2 Pt3 Sn1 O11 23.87(13) . . . . ?
Pt4 Pt3 Sn1 O11 127.74(13) . . . . ?
Sn5 Pt3 Sn1 O11 -170.15(13) . . . . ?
Pt2 Pt3 Sn1 O11 89.10(13) . . . . ?
Sn6 Pt3 Sn1 O11 108.95(14) . . . . ?
Pt1 Pt3 Sn1 O11 162.47(13) . . . . ?
Pt5 Pt3 Sn1 O11 63.35(13) . . . . ?
C3 Pt3 Sn1 Cl2 19.4(2) . . . . ?
Sn2 Pt3 Sn1 Cl2 114.43(5) . . . . ?
Pt4 Pt3 Sn1 Cl2 -141.69(5) . . . . ?
Sn5 Pt3 Sn1 Cl2 -79.58(5) . . . . ?
Pt2 Pt3 Sn1 Cl2 179.67(6) . . . . ?
Sn6 Pt3 Sn1 Cl2 -160.48(7) . . . . ?
Pt1 Pt3 Sn1 Cl2 -106.96(5) . . . . ?
Pt5 Pt3 Sn1 Cl2 153.92(5) . . . . ?
C3 Pt3 Sn1 Cl1 -144.9(3) . . . . ?
Sn2 Pt3 Sn1 Cl1 -49.86(14) . . . . ?
Pt4 Pt3 Sn1 Cl1 54.01(14) . . . . ?
Sn5 Pt3 Sn1 Cl1 116.12(14) . . . . ?
Pt2 Pt3 Sn1 Cl1 15.37(14) . . . . ?
Sn6 Pt3 Sn1 Cl1 35.22(16) . . . . ?
Pt1 Pt3 Sn1 Cl1 88.74(14) . . . . ?
Pt5 Pt3 Sn1 Cl1 -10.38(14) . . . . ?
C3 Pt3 Sn1 Pt1 126.3(2) . . . . ?
Sn2 Pt3 Sn1 Pt1 -138.601(15) . . . . ?
Pt4 Pt3 Sn1 Pt1 -34.730(13) . . . . ?
Sn5 Pt3 Sn1 Pt1 27.386(14) . . . . ?
Pt2 Pt3 Sn1 Pt1 -73.367(11) . . . . ?
Sn6 Pt3 Sn1 Pt1 -53.52(6) . . . . ?
Pt5 Pt3 Sn1 Pt1 -99.116(13) . . . . ?
C3 Pt3 Sn1 Pt2 -160.3(2) . . . . ?
Sn2 Pt3 Sn1 Pt2 -65.235(12) . . . . ?
Pt4 Pt3 Sn1 Pt2 38.637(12) . . . . ?
Sn5 Pt3 Sn1 Pt2 100.752(14) . . . . ?
Sn6 Pt3 Sn1 Pt2 19.85(6) . . . . ?
Pt1 Pt3 Sn1 Pt2 73.367(11) . . . . ?
Pt5 Pt3 Sn1 Pt2 -25.749(13) . . . . ?
C5 Pt5 Sn2 O11 -177.7(3) . . . . ?
Sn6 Pt5 Sn2 O11 67.1(2) . . . . ?
Sn4 Pt5 Sn2 O11 -64.1(2) . . . . ?
Pt2 Pt5 Sn2 O11 -33.4(2) . . . . ?
Pt4 Pt5 Sn2 O11 1.9(2) . . . . ?
Pt3 Pt5 Sn2 O11 35.1(2) . . . . ?
C5 Pt5 Sn2 Cl3 52.9(2) . . . . ?
Sn6 Pt5 Sn2 Cl3 -62.23(5) . . . . ?
Sn4 Pt5 Sn2 Cl3 166.57(5) . . . . ?
Pt2 Pt5 Sn2 Cl3 -162.74(5) . . . . ?
Pt4 Pt5 Sn2 Cl3 -127.45(5) . . . . ?
Pt3 Pt5 Sn2 Cl3 -94.28(5) . . . . ?
C5 Pt5 Sn2 Cl4 -52.5(2) . . . . ?
Sn6 Pt5 Sn2 Cl4 -167.72(5) . . . . ?
Sn4 Pt5 Sn2 Cl4 61.08(5) . . . . ?
Pt2 Pt5 Sn2 Cl4 91.77(5) . . . . ?
Pt4 Pt5 Sn2 Cl4 127.06(5) . . . . ?
Pt3 Pt5 Sn2 Cl4 160.23(5) . . . . ?
C5 Pt5 Sn2 Pt3 147.2(2) . . . . ?
Sn6 Pt5 Sn2 Pt3 32.049(16) . . . . ?
Sn4 Pt5 Sn2 Pt3 -99.151(18) . . . . ?
Pt2 Pt5 Sn2 Pt3 -68.455(10) . . . . ?
Pt4 Pt5 Sn2 Pt3 -33.170(12) . . . . ?
C5 Pt5 Sn2 Pt2 -144.3(2) . . . . ?
Sn6 Pt5 Sn2 Pt2 100.504(17) . . . . ?
Sn4 Pt5 Sn2 Pt2 -30.696(18) . . . . ?
Pt4 Pt5 Sn2 Pt2 35.285(12) . . . . ?
Pt3 Pt5 Sn2 Pt2 68.455(11) . . . . ?
C3 Pt3 Sn2 O11 73.2(2) . . . . ?
Pt4 Pt3 Sn2 O11 -125.56(13) . . . . ?
Sn5 Pt3 Sn2 O11 -104.90(14) . . . . ?
Pt2 Pt3 Sn2 O11 -86.97(13) . . . . ?
Sn6 Pt3 Sn2 O11 173.15(13) . . . . ?
Pt1 Pt3 Sn2 O11 -60.37(13) . . . . ?
Sn1 Pt3 Sn2 O11 -23.64(13) . . . . ?
Pt5 Pt3 Sn2 O11 -158.93(13) . . . . ?
C3 Pt3 Sn2 Cl3 -17.7(2) . . . . ?
Pt4 Pt3 Sn2 Cl3 143.53(5) . . . . ?
Sn5 Pt3 Sn2 Cl3 164.18(8) . . . . ?
Pt2 Pt3 Sn2 Cl3 -177.88(5) . . . . ?
Sn6 Pt3 Sn2 Cl3 82.23(5) . . . . ?
Pt1 Pt3 Sn2 Cl3 -151.29(5) . . . . ?
Sn1 Pt3 Sn2 Cl3 -114.56(5) . . . . ?
Pt5 Pt3 Sn2 Cl3 110.16(5) . . . . ?
C3 Pt3 Sn2 Cl4 146.0(3) . . . . ?
Pt4 Pt3 Sn2 Cl4 -52.78(15) . . . . ?
Sn5 Pt3 Sn2 Cl4 -32.12(18) . . . . ?
Pt2 Pt3 Sn2 Cl4 -14.19(15) . . . . ?
Sn6 Pt3 Sn2 Cl4 -114.07(15) . . . . ?
Pt1 Pt3 Sn2 Cl4 12.41(15) . . . . ?
Sn1 Pt3 Sn2 Cl4 49.14(15) . . . . ?
Pt5 Pt3 Sn2 Cl4 -86.15(15) . . . . ?
C3 Pt3 Sn2 Pt5 -127.9(2) . . . . ?
Pt4 Pt3 Sn2 Pt5 33.370(13) . . . . ?
Sn5 Pt3 Sn2 Pt5 54.03(7) . . . . ?
Pt2 Pt3 Sn2 Pt5 71.962(11) . . . . ?
Sn6 Pt3 Sn2 Pt5 -27.922(14) . . . . ?
Pt1 Pt3 Sn2 Pt5 98.559(14) . . . . ?
Sn1 Pt3 Sn2 Pt5 135.288(15) . . . . ?
C3 Pt3 Sn2 Pt2 160.1(2) . . . . ?
Pt4 Pt3 Sn2 Pt2 -38.592(12) . . . . ?
Sn5 Pt3 Sn2 Pt2 -17.93(7) . . . . ?
Sn6 Pt3 Sn2 Pt2 -99.884(14) . . . . ?
Pt1 Pt3 Sn2 Pt2 26.597(13) . . . . ?
Sn1 Pt3 Sn2 Pt2 63.326(12) . . . . ?
Pt5 Pt3 Sn2 Pt2 -71.962(11) . . . . ?
C2 Pt2 Sn2 O11 -77.2(3) . . . . ?
Pt4 Pt2 Sn2 O11 124.49(13) . . . . ?
Sn1 Pt2 Sn2 O11 20.31(13) . . . . ?
Sn3 Pt2 Sn2 O11 102.42(15) . . . . ?
Pt3 Pt2 Sn2 O11 86.02(13) . . . . ?
Pt1 Pt2 Sn2 O11 59.66(13) . . . . ?
Pt5 Pt2 Sn2 O11 159.88(13) . . . . ?
Sn4 Pt2 Sn2 O11 -174.31(13) . . . . ?
C2 Pt2 Sn2 Cl3 -155.7(3) . . . . ?
Pt4 Pt2 Sn2 Cl3 45.99(19) . . . . ?
Sn1 Pt2 Sn2 Cl3 -58.19(19) . . . . ?
Sn3 Pt2 Sn2 Cl3 23.9(2) . . . . ?
Pt3 Pt2 Sn2 Cl3 7.51(19) . . . . ?
Pt1 Pt2 Sn2 Cl3 -18.84(19) . . . . ?
Pt5 Pt2 Sn2 Cl3 81.38(19) . . . . ?
Sn4 Pt2 Sn2 Cl3 107.19(19) . . . . ?
C2 Pt2 Sn2 Cl4 12.4(2) . . . . ?
Pt4 Pt2 Sn2 Cl4 -145.99(5) . . . . ?
Sn1 Pt2 Sn2 Cl4 109.83(5) . . . . ?
Sn3 Pt2 Sn2 Cl4 -168.06(7) . . . . ?
Pt3 Pt2 Sn2 Cl4 175.54(5) . . . . ?
Pt1 Pt2 Sn2 Cl4 149.18(5) . . . . ?
Pt5 Pt2 Sn2 Cl4 -110.60(5) . . . . ?
Sn4 Pt2 Sn2 Cl4 -84.79(5) . . . . ?
C2 Pt2 Sn2 Pt5 123.0(2) . . . . ?
Pt4 Pt2 Sn2 Pt5 -35.396(13) . . . . ?
Sn1 Pt2 Sn2 Pt5 -139.576(16) . . . . ?
Sn3 Pt2 Sn2 Pt5 -57.47(6) . . . . ?
Pt3 Pt2 Sn2 Pt5 -73.868(12) . . . . ?
Pt1 Pt2 Sn2 Pt5 -100.222(14) . . . . ?
Sn4 Pt2 Sn2 Pt5 25.809(15) . . . . ?
C2 Pt2 Sn2 Pt3 -163.2(2) . . . . ?
Pt4 Pt2 Sn2 Pt3 38.473(12) . . . . ?
Sn1 Pt2 Sn2 Pt3 -65.708(13) . . . . ?
Sn3 Pt2 Sn2 Pt3 16.40(6) . . . . ?
Pt1 Pt2 Sn2 Pt3 -26.354(13) . . . . ?
Pt5 Pt2 Sn2 Pt3 73.868(12) . . . . ?
Sn4 Pt2 Sn2 Pt3 99.677(15) . . . . ?
C1 Pt1 Sn3 O12 174.9(3) . . . . ?
Sn1 Pt1 Sn3 O12 -69.8(2) . . . . ?
Sn5 Pt1 Sn3 O12 65.5(2) . . . . ?
Pt2 Pt1 Sn3 O12 -36.1(2) . . . . ?
Pt3 Pt1 Sn3 O12 -1.4(2) . . . . ?
Pt4 Pt1 Sn3 O12 31.8(2) . . . . ?
C1 Pt1 Sn3 Cl6 -56.2(3) . . . . ?
Sn1 Pt1 Sn3 Cl6 59.11(6) . . . . ?
Sn5 Pt1 Sn3 Cl6 -165.52(6) . . . . ?
Pt2 Pt1 Sn3 Cl6 92.82(6) . . . . ?
Pt3 Pt1 Sn3 Cl6 127.49(6) . . . . ?
Pt4 Pt1 Sn3 Cl6 160.76(6) . . . . ?
C1 Pt1 Sn3 Cl5 48.5(3) . . . . ?
Sn1 Pt1 Sn3 Cl5 163.79(5) . . . . ?
Sn5 Pt1 Sn3 Cl5 -60.83(6) . . . . ?
Pt2 Pt1 Sn3 Cl5 -162.50(6) . . . . ?
Pt3 Pt1 Sn3 Cl5 -127.83(5) . . . . ?
Pt4 Pt1 Sn3 Cl5 -94.56(5) . . . . ?
C1 Pt1 Sn3 Pt4 143.1(2) . . . . ?
Sn1 Pt1 Sn3 Pt4 -101.651(17) . . . . ?
Sn5 Pt1 Sn3 Pt4 33.726(17) . . . . ?
Pt2 Pt1 Sn3 Pt4 -67.938(11) . . . . ?
Pt3 Pt1 Sn3 Pt4 -33.271(13) . . . . ?
C1 Pt1 Sn3 Pt2 -149.0(2) . . . . ?
Sn1 Pt1 Sn3 Pt2 -33.712(17) . . . . ?
Sn5 Pt1 Sn3 Pt2 101.664(17) . . . . ?
Pt3 Pt1 Sn3 Pt2 34.667(13) . . . . ?
Pt4 Pt1 Sn3 Pt2 67.938(11) . . . . ?
C4 Pt4 Sn3 O12 74.1(2) . . . . ?
Sn6 Pt4 Sn3 O12 -107.47(15) . . . . ?
Sn4 Pt4 Sn3 O12 -22.01(13) . . . . ?
Pt2 Pt4 Sn3 O12 -87.58(13) . . . . ?
Sn5 Pt4 Sn3 O12 170.35(13) . . . . ?
Pt3 Pt4 Sn3 O12 -127.14(13) . . . . ?
Pt1 Pt4 Sn3 O12 -160.17(14) . . . . ?
Pt5 Pt4 Sn3 O12 -62.02(14) . . . . ?
C4 Pt4 Sn3 Cl6 143.3(3) . . . . ?
Sn6 Pt4 Sn3 Cl6 -38.2(2) . . . . ?
Sn4 Pt4 Sn3 Cl6 47.25(18) . . . . ?
Pt2 Pt4 Sn3 Cl6 -18.33(18) . . . . ?
Sn5 Pt4 Sn3 Cl6 -120.40(18) . . . . ?
Pt3 Pt4 Sn3 Cl6 -57.89(18) . . . . ?
Pt1 Pt4 Sn3 Cl6 -90.92(18) . . . . ?
Pt5 Pt4 Sn3 Cl6 7.23(19) . . . . ?
C4 Pt4 Sn3 Cl5 -19.1(2) . . . . ?
Sn6 Pt4 Sn3 Cl5 159.34(8) . . . . ?
Sn4 Pt4 Sn3 Cl5 -115.20(5) . . . . ?
Pt2 Pt4 Sn3 Cl5 179.23(5) . . . . ?
Sn5 Pt4 Sn3 Cl5 77.16(5) . . . . ?
Pt3 Pt4 Sn3 Cl5 139.67(5) . . . . ?
Pt1 Pt4 Sn3 Cl5 106.64(5) . . . . ?
Pt5 Pt4 Sn3 Cl5 -155.22(5) . . . . ?
C4 Pt4 Sn3 Pt1 -125.8(2) . . . . ?
Sn6 Pt4 Sn3 Pt1 52.70(8) . . . . ?
Sn4 Pt4 Sn3 Pt1 138.165(16) . . . . ?
Pt2 Pt4 Sn3 Pt1 72.590(12) . . . . ?
Sn5 Pt4 Sn3 Pt1 -29.479(15) . . . . ?
Pt3 Pt4 Sn3 Pt1 33.030(14) . . . . ?
Pt5 Pt4 Sn3 Pt1 98.146(14) . . . . ?
C4 Pt4 Sn3 Pt2 161.7(2) . . . . ?
Sn6 Pt4 Sn3 Pt2 -19.89(8) . . . . ?
Sn4 Pt4 Sn3 Pt2 65.576(13) . . . . ?
Sn5 Pt4 Sn3 Pt2 -102.068(14) . . . . ?
Pt3 Pt4 Sn3 Pt2 -39.560(12) . . . . ?
Pt1 Pt4 Sn3 Pt2 -72.590(12) . . . . ?
Pt5 Pt4 Sn3 Pt2 25.557(13) . . . . ?
C2 Pt2 Sn3 O12 -71.4(3) . . . . ?
Pt4 Pt2 Sn3 O12 84.39(13) . . . . ?
Sn1 Pt2 Sn3 O12 -172.81(13) . . . . ?
Pt3 Pt2 Sn3 O12 123.65(13) . . . . ?
Sn2 Pt2 Sn3 O12 109.02(15) . . . . ?
Pt1 Pt2 Sn3 O12 157.81(13) . . . . ?
Pt5 Pt2 Sn3 O12 58.61(13) . . . . ?
Sn4 Pt2 Sn3 O12 21.54(13) . . . . ?
C2 Pt2 Sn3 Cl6 18.7(2) . . . . ?
Pt4 Pt2 Sn3 Cl6 174.48(6) . . . . ?
Sn1 Pt2 Sn3 Cl6 -82.72(6) . . . . ?
Pt3 Pt2 Sn3 Cl6 -146.26(6) . . . . ?
Sn2 Pt2 Sn3 Cl6 -160.89(8) . . . . ?
Pt1 Pt2 Sn3 Cl6 -112.10(6) . . . . ?
Pt5 Pt2 Sn3 Cl6 148.70(5) . . . . ?
Sn4 Pt2 Sn3 Cl6 111.63(6) . . . . ?
C2 Pt2 Sn3 Cl5 -158.3(3) . . . . ?
Pt4 Pt2 Sn3 Cl5 -2.53(17) . . . . ?
Sn1 Pt2 Sn3 Cl5 100.27(17) . . . . ?
Pt3 Pt2 Sn3 Cl5 36.73(18) . . . . ?
Sn2 Pt2 Sn3 Cl5 22.1(2) . . . . ?
Pt1 Pt2 Sn3 Cl5 70.89(17) . . . . ?
Pt5 Pt2 Sn3 Cl5 -28.31(18) . . . . ?
Sn4 Pt2 Sn3 Cl5 -65.38(17) . . . . ?
C2 Pt2 Sn3 Pt1 130.8(2) . . . . ?
Pt4 Pt2 Sn3 Pt1 -73.415(12) . . . . ?
Sn1 Pt2 Sn3 Pt1 29.385(15) . . . . ?
Pt3 Pt2 Sn3 Pt1 -34.160(13) . . . . ?
Sn2 Pt2 Sn3 Pt1 -48.79(6) . . . . ?
Pt5 Pt2 Sn3 Pt1 -99.194(14) . . . . ?
Sn4 Pt2 Sn3 Pt1 -136.271(16) . . . . ?
C2 Pt2 Sn3 Pt4 -155.8(2) . . . . ?
Sn1 Pt2 Sn3 Pt4 102.800(14) . . . . ?
Pt3 Pt2 Sn3 Pt4 39.256(12) . . . . ?
Sn2 Pt2 Sn3 Pt4 24.63(6) . . . . ?
Pt1 Pt2 Sn3 Pt4 73.415(12) . . . . ?
Pt5 Pt2 Sn3 Pt4 -25.779(13) . . . . ?
Sn4 Pt2 Sn3 Pt4 -62.856(13) . . . . ?
C5 Pt5 Sn4 O12 175.5(3) . . . . ?
Sn2 Pt5 Sn4 O12 62.0(2) . . . . ?
Sn6 Pt5 Sn4 O12 -70.7(2) . . . . ?
Pt2 Pt5 Sn4 O12 31.5(2) . . . . ?
Pt4 Pt5 Sn4 O12 -36.3(2) . . . . ?
Pt3 Pt5 Sn4 O12 -4.5(2) . . . . ?
C5 Pt5 Sn4 Cl7 -55.4(3) . . . . ?
Sn2 Pt5 Sn4 Cl7 -168.92(7) . . . . ?
Sn6 Pt5 Sn4 Cl7 58.35(7) . . . . ?
Pt2 Pt5 Sn4 Cl7 160.58(7) . . . . ?
Pt4 Pt5 Sn4 Cl7 92.77(7) . . . . ?
Pt3 Pt5 Sn4 Cl7 124.58(7) . . . . ?
C5 Pt5 Sn4 Cl8 48.9(3) . . . . ?
Sn2 Pt5 Sn4 Cl8 -64.59(6) . . . . ?
Sn6 Pt5 Sn4 Cl8 162.67(6) . . . . ?
Pt2 Pt5 Sn4 Cl8 -95.09(6) . . . . ?
Pt4 Pt5 Sn4 Cl8 -162.91(6) . . . . ?
Pt3 Pt5 Sn4 Cl8 -131.09(6) . . . . ?
C5 Pt5 Sn4 Pt4 -148.2(2) . . . . ?
Sn2 Pt5 Sn4 Pt4 98.316(18) . . . . ?
Sn6 Pt5 Sn4 Pt4 -34.420(16) . . . . ?
Pt2 Pt5 Sn4 Pt4 67.817(11) . . . . ?
Pt3 Pt5 Sn4 Pt4 31.817(13) . . . . ?
C5 Pt5 Sn4 Pt2 144.0(2) . . . . ?
Sn2 Pt5 Sn4 Pt2 30.500(18) . . . . ?
Sn6 Pt5 Sn4 Pt2 -102.237(16) . . . . ?
Pt4 Pt5 Sn4 Pt2 -67.817(11) . . . . ?
Pt3 Pt5 Sn4 Pt2 -36.000(13) . . . . ?
C4 Pt4 Sn4 O12 -73.7(3) . . . . ?
Sn6 Pt4 Sn4 O12 -171.12(14) . . . . ?
Pt2 Pt4 Sn4 O12 85.91(14) . . . . ?
Sn5 Pt4 Sn4 O12 106.44(16) . . . . ?
Sn3 Pt4 Sn4 O12 21.99(14) . . . . ?
Pt3 Pt4 Sn4 O12 125.40(14) . . . . ?
Pt1 Pt4 Sn4 O12 59.96(14) . . . . ?
Pt5 Pt4 Sn4 O12 157.53(14) . . . . ?
C4 Pt4 Sn4 Cl7 17.4(2) . . . . ?
Sn6 Pt4 Sn4 Cl7 -79.97(6) . . . . ?
Pt2 Pt4 Sn4 Cl7 177.06(6) . . . . ?
Sn5 Pt4 Sn4 Cl7 -162.42(9) . . . . ?
Sn3 Pt4 Sn4 Cl7 113.14(6) . . . . ?
Pt3 Pt4 Sn4 Cl7 -143.45(6) . . . . ?
Pt1 Pt4 Sn4 Cl7 151.10(6) . . . . ?
Pt5 Pt4 Sn4 Cl7 -111.32(6) . . . . ?
C4 Pt4 Sn4 Cl8 -153.0(3) . . . . ?
Sn6 Pt4 Sn4 Cl8 109.59(19) . . . . ?
Pt2 Pt4 Sn4 Cl8 6.62(19) . . . . ?
Sn5 Pt4 Sn4 Cl8 27.1(2) . . . . ?
Sn3 Pt4 Sn4 Cl8 -57.30(19) . . . . ?
Pt3 Pt4 Sn4 Cl8 46.12(19) . . . . ?
Pt1 Pt4 Sn4 Cl8 -19.33(19) . . . . ?
Pt5 Pt4 Sn4 Cl8 78.24(19) . . . . ?
C4 Pt4 Sn4 Pt5 128.7(2) . . . . ?
Sn6 Pt4 Sn4 Pt5 31.349(15) . . . . ?
Pt2 Pt4 Sn4 Pt5 -71.620(11) . . . . ?
Sn5 Pt4 Sn4 Pt5 -51.10(8) . . . . ?
Sn3 Pt4 Sn4 Pt5 -135.543(16) . . . . ?
Pt3 Pt4 Sn4 Pt5 -32.127(14) . . . . ?
Pt1 Pt4 Sn4 Pt5 -97.576(14) . . . . ?
C4 Pt4 Sn4 Pt2 -159.7(2) . . . . ?
Sn6 Pt4 Sn4 Pt2 102.969(14) . . . . ?
Sn5 Pt4 Sn4 Pt2 20.52(8) . . . . ?
Sn3 Pt4 Sn4 Pt2 -63.923(13) . . . . ?
Pt3 Pt4 Sn4 Pt2 39.493(12) . . . . ?
Pt1 Pt4 Sn4 Pt2 -25.956(14) . . . . ?
Pt5 Pt4 Sn4 Pt2 71.620(11) . . . . ?
C2 Pt2 Sn4 O12 73.3(3) . . . . ?
Pt4 Pt2 Sn4 O12 -85.95(13) . . . . ?
Sn1 Pt2 Sn4 O12 -102.52(15) . . . . ?
Sn3 Pt2 Sn4 O12 -21.61(13) . . . . ?
Pt3 Pt2 Sn4 O12 -124.62(13) . . . . ?
Sn2 Pt2 Sn4 O12 173.89(13) . . . . ?
Pt1 Pt2 Sn4 O12 -60.37(13) . . . . ?
Pt5 Pt2 Sn4 O12 -160.25(13) . . . . ?
C2 Pt2 Sn4 Cl7 149.8(3) . . . . ?
Pt4 Pt2 Sn4 Cl7 -9.47(18) . . . . ?
Sn1 Pt2 Sn4 Cl7 -26.0(2) . . . . ?
Sn3 Pt2 Sn4 Cl7 54.87(19) . . . . ?
Pt3 Pt2 Sn4 Cl7 -48.14(19) . . . . ?
Sn2 Pt2 Sn4 Cl7 -109.63(19) . . . . ?
Pt1 Pt2 Sn4 Cl7 16.10(19) . . . . ?
Pt5 Pt2 Sn4 Cl7 -83.77(19) . . . . ?
C2 Pt2 Sn4 Cl8 -18.8(2) . . . . ?
Pt4 Pt2 Sn4 Cl8 -178.10(5) . . . . ?
Sn1 Pt2 Sn4 Cl8 165.32(8) . . . . ?
Sn3 Pt2 Sn4 Cl8 -113.76(5) . . . . ?
Pt3 Pt2 Sn4 Cl8 143.23(5) . . . . ?
Sn2 Pt2 Sn4 Cl8 81.74(5) . . . . ?
Pt1 Pt2 Sn4 Cl8 -152.53(5) . . . . ?
Pt5 Pt2 Sn4 Cl8 107.59(5) . . . . ?
C2 Pt2 Sn4 Pt5 -126.4(2) . . . . ?
Pt4 Pt2 Sn4 Pt5 74.305(12) . . . . ?
Sn1 Pt2 Sn4 Pt5 57.73(7) . . . . ?
Sn3 Pt2 Sn4 Pt5 138.642(16) . . . . ?
Pt3 Pt2 Sn4 Pt5 35.631(13) . . . . ?
Sn2 Pt2 Sn4 Pt5 -25.857(15) . . . . ?
Pt1 Pt2 Sn4 Pt5 99.879(14) . . . . ?
C2 Pt2 Sn4 Pt4 159.3(2) . . . . ?
Sn1 Pt2 Sn4 Pt4 -16.58(7) . . . . ?
Sn3 Pt2 Sn4 Pt4 64.337(13) . . . . ?
Pt3 Pt2 Sn4 Pt4 -38.674(12) . . . . ?
Sn2 Pt2 Sn4 Pt4 -100.162(15) . . . . ?
Pt1 Pt2 Sn4 Pt4 25.574(13) . . . . ?
Pt5 Pt2 Sn4 Pt4 -74.305(12) . . . . ?
C1 Pt1 Sn5 O13 179.7(3) . . . . ?
Sn1 Pt1 Sn5 O13 65.8(2) . . . . ?
Sn3 Pt1 Sn5 O13 -68.5(2) . . . . ?
Pt2 Pt1 Sn5 O13 -1.5(2) . . . . ?
Pt3 Pt1 Sn5 O13 33.3(2) . . . . ?
Pt4 Pt1 Sn5 O13 -34.8(2) . . . . ?
C1 Pt1 Sn5 Cl10 -54.9(2) . . . . ?
Sn1 Pt1 Sn5 Cl10 -168.73(5) . . . . ?
Sn3 Pt1 Sn5 Cl10 56.97(6) . . . . ?
Pt2 Pt1 Sn5 Cl10 123.98(5) . . . . ?
Pt3 Pt1 Sn5 Cl10 158.77(5) . . . . ?
Pt4 Pt1 Sn5 Cl10 90.68(5) . . . . ?
C1 Pt1 Sn5 Cl9 50.3(2) . . . . ?
Sn1 Pt1 Sn5 Cl9 -63.55(5) . . . . ?
Sn3 Pt1 Sn5 Cl9 162.15(5) . . . . ?
Pt2 Pt1 Sn5 Cl9 -130.84(5) . . . . ?
Pt3 Pt1 Sn5 Cl9 -96.04(5) . . . . ?
Pt4 Pt1 Sn5 Cl9 -164.14(5) . . . . ?
C1 Pt1 Sn5 Pt4 -145.6(2) . . . . ?
Sn1 Pt1 Sn5 Pt4 100.592(17) . . . . ?
Sn3 Pt1 Sn5 Pt4 -33.708(17) . . . . ?
Pt2 Pt1 Sn5 Pt4 33.298(13) . . . . ?
Pt3 Pt1 Sn5 Pt4 68.094(10) . . . . ?
C1 Pt1 Sn5 Pt3 146.3(2) . . . . ?
Sn1 Pt1 Sn5 Pt3 32.498(17) . . . . ?
Sn3 Pt1 Sn5 Pt3 -101.803(17) . . . . ?
Pt2 Pt1 Sn5 Pt3 -34.797(12) . . . . ?
Pt4 Pt1 Sn5 Pt3 -68.094(10) . . . . ?
C4 Pt4 Sn5 O13 -73.3(2) . . . . ?
Sn6 Pt4 Sn5 O13 21.08(13) . . . . ?
Sn4 Pt4 Sn5 O13 106.54(15) . . . . ?
Pt2 Pt4 Sn5 O13 125.36(13) . . . . ?
Sn3 Pt4 Sn5 O13 -172.02(13) . . . . ?
Pt3 Pt4 Sn5 O13 85.72(13) . . . . ?
Pt1 Pt4 Sn5 O13 158.46(13) . . . . ?
Pt5 Pt4 Sn5 O13 60.68(13) . . . . ?
C4 Pt4 Sn5 Cl10 17.1(2) . . . . ?
Sn6 Pt4 Sn5 Cl10 111.46(5) . . . . ?
Sn4 Pt4 Sn5 Cl10 -163.07(9) . . . . ?
Pt2 Pt4 Sn5 Cl10 -144.25(5) . . . . ?
Sn3 Pt4 Sn5 Cl10 -81.63(5) . . . . ?
Pt3 Pt4 Sn5 Cl10 176.11(5) . . . . ?
Pt1 Pt4 Sn5 Cl10 -111.15(5) . . . . ?
Pt5 Pt4 Sn5 Cl10 151.07(5) . . . . ?
C4 Pt4 Sn5 Cl9 -151.8(3) . . . . ?
Sn6 Pt4 Sn5 Cl9 -57.4(2) . . . . ?
Sn4 Pt4 Sn5 Cl9 28.0(2) . . . . ?
Pt2 Pt4 Sn5 Cl9 46.9(2) . . . . ?
Sn3 Pt4 Sn5 Cl9 109.5(2) . . . . ?
Pt3 Pt4 Sn5 Cl9 7.2(2) . . . . ?
Pt1 Pt4 Sn5 Cl9 79.9(2) . . . . ?
Pt5 Pt4 Sn5 Cl9 -17.8(2) . . . . ?
C4 Pt4 Sn5 Pt1 128.3(2) . . . . ?
Sn6 Pt4 Sn5 Pt1 -137.381(16) . . . . ?
Sn4 Pt4 Sn5 Pt1 -51.92(8) . . . . ?
Pt2 Pt4 Sn5 Pt1 -33.093(13) . . . . ?
Sn3 Pt4 Sn5 Pt1 29.520(15) . . . . ?
Pt3 Pt4 Sn5 Pt1 -72.735(12) . . . . ?
Pt5 Pt4 Sn5 Pt1 -97.778(14) . . . . ?
C4 Pt4 Sn5 Pt3 -159.0(2) . . . . ?
Sn6 Pt4 Sn5 Pt3 -64.647(13) . . . . ?
Sn4 Pt4 Sn5 Pt3 20.82(8) . . . . ?
Pt2 Pt4 Sn5 Pt3 39.642(12) . . . . ?
Sn3 Pt4 Sn5 Pt3 102.254(15) . . . . ?
Pt1 Pt4 Sn5 Pt3 72.735(12) . . . . ?
Pt5 Pt4 Sn5 Pt3 -25.044(14) . . . . ?
C3 Pt3 Sn5 O13 73.1(2) . . . . ?
Sn2 Pt3 Sn5 O13 -108.86(15) . . . . ?
Pt4 Pt3 Sn5 O13 -85.94(13) . . . . ?
Pt2 Pt3 Sn5 O13 -125.09(13) . . . . ?
Sn6 Pt3 Sn5 O13 -23.21(13) . . . . ?
Pt1 Pt3 Sn5 O13 -159.26(13) . . . . ?
Sn1 Pt3 Sn5 O13 173.54(13) . . . . ?
Pt5 Pt3 Sn5 O13 -61.01(13) . . . . ?
C3 Pt3 Sn5 Cl10 147.5(3) . . . . ?
Sn2 Pt3 Sn5 Cl10 -34.45(19) . . . . ?
Pt4 Pt3 Sn5 Cl10 -11.54(16) . . . . ?
Pt2 Pt3 Sn5 Cl10 -50.69(16) . . . . ?
Sn6 Pt3 Sn5 Cl10 51.19(16) . . . . ?
Pt1 Pt3 Sn5 Cl10 -84.86(16) . . . . ?
Sn1 Pt3 Sn5 Cl10 -112.05(16) . . . . ?
Pt5 Pt3 Sn5 Cl10 13.39(16) . . . . ?
C3 Pt3 Sn5 Cl9 -19.1(2) . . . . ?
Sn2 Pt3 Sn5 Cl9 158.99(8) . . . . ?
Pt4 Pt3 Sn5 Cl9 -178.10(5) . . . . ?
Pt2 Pt3 Sn5 Cl9 142.75(5) . . . . ?
Sn6 Pt3 Sn5 Cl9 -115.37(5) . . . . ?
Pt1 Pt3 Sn5 Cl9 108.58(5) . . . . ?
Sn1 Pt3 Sn5 Cl9 81.39(5) . . . . ?
Pt5 Pt3 Sn5 Cl9 -153.17(5) . . . . ?
C3 Pt3 Sn5 Pt1 -127.7(2) . . . . ?
Sn2 Pt3 Sn5 Pt1 50.40(7) . . . . ?
Pt4 Pt3 Sn5 Pt1 73.319(11) . . . . ?
Pt2 Pt3 Sn5 Pt1 34.170(13) . . . . ?
Sn6 Pt3 Sn5 Pt1 136.047(15) . . . . ?
Sn1 Pt3 Sn5 Pt1 -27.197(14) . . . . ?
Pt5 Pt3 Sn5 Pt1 98.248(14) . . . . ?
C3 Pt3 Sn5 Pt4 159.0(2) . . . . ?
Sn2 Pt3 Sn5 Pt4 -22.92(7) . . . . ?
Pt2 Pt3 Sn5 Pt4 -39.149(12) . . . . ?
Sn6 Pt3 Sn5 Pt4 62.728(12) . . . . ?
Pt1 Pt3 Sn5 Pt4 -73.319(11) . . . . ?
Sn1 Pt3 Sn5 Pt4 -100.516(14) . . . . ?
Pt5 Pt3 Sn5 Pt4 24.929(13) . . . . ?
C5 Pt5 Sn6 O13 -176.0(3) . . . . ?
Sn2 Pt5 Sn6 O13 -62.5(2) . . . . ?
Sn4 Pt5 Sn6 O13 71.9(2) . . . . ?
Pt2 Pt5 Sn6 O13 4.7(2) . . . . ?
Pt4 Pt5 Sn6 O13 37.4(2) . . . . ?
Pt3 Pt5 Sn6 O13 -30.8(2) . . . . ?
C5 Pt5 Sn6 Cl11 -49.4(2) . . . . ?
Sn2 Pt5 Sn6 Cl11 64.05(5) . . . . ?
Sn4 Pt5 Sn6 Cl11 -161.54(5) . . . . ?
Pt2 Pt5 Sn6 Cl11 131.27(5) . . . . ?
Pt4 Pt5 Sn6 Cl11 163.98(5) . . . . ?
Pt3 Pt5 Sn6 Cl11 95.74(5) . . . . ?
C5 Pt5 Sn6 Cl12 53.4(2) . . . . ?
Sn2 Pt5 Sn6 Cl12 166.84(5) . . . . ?
Sn4 Pt5 Sn6 Cl12 -58.75(5) . . . . ?
Pt2 Pt5 Sn6 Cl12 -125.94(5) . . . . ?
Pt4 Pt5 Sn6 Cl12 -93.23(5) . . . . ?
Pt3 Pt5 Sn6 Cl12 -161.47(5) . . . . ?
C5 Pt5 Sn6 Pt4 146.6(2) . . . . ?
Sn2 Pt5 Sn6 Pt4 -99.928(16) . . . . ?
Sn4 Pt5 Sn6 Pt4 34.480(16) . . . . ?
Pt2 Pt5 Sn6 Pt4 -32.704(12) . . . . ?
Pt3 Pt5 Sn6 Pt4 -68.235(10) . . . . ?
C5 Pt5 Sn6 Pt3 -145.2(2) . . . . ?
Sn2 Pt5 Sn6 Pt3 -31.693(16) . . . . ?
Sn4 Pt5 Sn6 Pt3 102.715(16) . . . . ?
Pt2 Pt5 Sn6 Pt3 35.531(12) . . . . ?
Pt4 Pt5 Sn6 Pt3 68.235(10) . . . . ?
C4 Pt4 Sn6 O13 72.2(2) . . . . ?
Sn4 Pt4 Sn6 O13 171.46(13) . . . . ?
Pt2 Pt4 Sn6 O13 -124.34(13) . . . . ?
Sn5 Pt4 Sn6 O13 -20.92(13) . . . . ?
Sn3 Pt4 Sn6 O13 -106.28(15) . . . . ?
Pt3 Pt4 Sn6 O13 -84.68(13) . . . . ?
Pt1 Pt4 Sn6 O13 -59.33(13) . . . . ?
Pt5 Pt4 Sn6 O13 -157.19(13) . . . . ?
C4 Pt4 Sn6 Cl11 143.5(3) . . . . ?
Sn4 Pt4 Sn6 Cl11 -117.3(2) . . . . ?
Pt2 Pt4 Sn6 Cl11 -53.1(2) . . . . ?
Sn5 Pt4 Sn6 Cl11 50.4(2) . . . . ?
Sn3 Pt4 Sn6 Cl11 -35.0(2) . . . . ?
Pt3 Pt4 Sn6 Cl11 -13.4(2) . . . . ?
Pt1 Pt4 Sn6 Cl11 12.0(2) . . . . ?
Pt5 Pt4 Sn6 Cl11 -85.9(2) . . . . ?
C4 Pt4 Sn6 Cl12 -20.4(2) . . . . ?
Sn4 Pt4 Sn6 Cl12 78.83(5) . . . . ?
Pt2 Pt4 Sn6 Cl12 143.02(5) . . . . ?
Sn5 Pt4 Sn6 Cl12 -113.55(5) . . . . ?
Sn3 Pt4 Sn6 Cl12 161.09(8) . . . . ?
Pt3 Pt4 Sn6 Cl12 -177.32(5) . . . . ?
Pt1 Pt4 Sn6 Cl12 -151.96(5) . . . . ?
Pt5 Pt4 Sn6 Cl12 110.18(5) . . . . ?
C4 Pt4 Sn6 Pt5 -130.6(2) . . . . ?
Sn4 Pt4 Sn6 Pt5 -31.351(15) . . . . ?
Pt2 Pt4 Sn6 Pt5 32.846(13) . . . . ?
Sn5 Pt4 Sn6 Pt5 136.268(15) . . . . ?
Sn3 Pt4 Sn6 Pt5 50.91(8) . . . . ?
Pt3 Pt4 Sn6 Pt5 72.505(11) . . . . ?
Pt1 Pt4 Sn6 Pt5 97.860(14) . . . . ?
C4 Pt4 Sn6 Pt3 156.9(2) . . . . ?
Sn4 Pt4 Sn6 Pt3 -103.855(15) . . . . ?
Pt2 Pt4 Sn6 Pt3 -39.659(12) . . . . ?
Sn5 Pt4 Sn6 Pt3 63.763(13) . . . . ?
Sn3 Pt4 Sn6 Pt3 -21.60(8) . . . . ?
Pt1 Pt4 Sn6 Pt3 25.355(14) . . . . ?
Pt5 Pt4 Sn6 Pt3 -72.505(11) . . . . ?
C3 Pt3 Sn6 O13 -71.5(2) . . . . ?
Sn2 Pt3 Sn6 O13 -171.06(13) . . . . ?
Pt4 Pt3 Sn6 O13 87.09(13) . . . . ?
Sn5 Pt3 Sn6 O13 23.11(13) . . . . ?
Pt2 Pt3 Sn6 O13 125.91(13) . . . . ?
Pt1 Pt3 Sn6 O13 62.02(13) . . . . ?
Sn1 Pt3 Sn6 O13 108.32(14) . . . . ?
Pt5 Pt3 Sn6 O13 160.88(13) . . . . ?
C3 Pt3 Sn6 Cl11 17.9(2) . . . . ?
Sn2 Pt3 Sn6 Cl11 -81.62(5) . . . . ?
Pt4 Pt3 Sn6 Cl11 176.52(5) . . . . ?
Sn5 Pt3 Sn6 Cl11 112.55(5) . . . . ?
Pt2 Pt3 Sn6 Cl11 -144.65(5) . . . . ?
Pt1 Pt3 Sn6 Cl11 151.45(5) . . . . ?
Sn1 Pt3 Sn6 Cl11 -162.25(7) . . . . ?
Pt5 Pt3 Sn6 Cl11 -109.68(5) . . . . ?
C3 Pt3 Sn6 Cl12 -149.7(3) . . . . ?
Sn2 Pt3 Sn6 Cl12 110.80(17) . . . . ?
Pt4 Pt3 Sn6 Cl12 8.94(17) . . . . ?
Sn5 Pt3 Sn6 Cl12 -55.03(17) . . . . ?
Pt2 Pt3 Sn6 Cl12 47.77(17) . . . . ?
Pt1 Pt3 Sn6 Cl12 -16.12(17) . . . . ?
Sn1 Pt3 Sn6 Cl12 30.17(19) . . . . ?
Pt5 Pt3 Sn6 Cl12 82.74(17) . . . . ?
C3 Pt3 Sn6 Pt5 127.6(2) . . . . ?
Sn2 Pt3 Sn6 Pt5 28.058(14) . . . . ?
Pt4 Pt3 Sn6 Pt5 -73.796(11) . . . . ?
Sn5 Pt3 Sn6 Pt5 -137.772(15) . . . . ?
Pt2 Pt3 Sn6 Pt5 -34.968(13) . . . . ?
Pt1 Pt3 Sn6 Pt5 -98.863(14) . . . . ?
Sn1 Pt3 Sn6 Pt5 -52.56(6) . . . . ?
C3 Pt3 Sn6 Pt4 -158.6(2) . . . . ?
Sn2 Pt3 Sn6 Pt4 101.854(14) . . . . ?
Sn5 Pt3 Sn6 Pt4 -63.976(13) . . . . ?
Pt2 Pt3 Sn6 Pt4 38.829(12) . . . . ?
Pt1 Pt3 Sn6 Pt4 -25.067(14) . . . . ?
Sn1 Pt3 Sn6 Pt4 21.23(6) . . . . ?
Pt5 Pt3 Sn6 Pt4 73.796(11) . . . . ?
Sn1 Pt1 C1 O1 83(35) . . . . ?
Sn5 Pt1 C1 O1 -38(35) . . . . ?
Sn3 Pt1 C1 O1 -156(35) . . . . ?
Pt2 Pt1 C1 O1 144(34) . . . . ?
Pt3 Pt1 C1 O1 18(35) . . . . ?
Pt4 Pt1 C1 O1 -94(35) . . . . ?
Pt4 Pt2 C2 O2 45(48) . . . . ?
Sn1 Pt2 C2 O2 -170(100) . . . . ?
Sn3 Pt2 C2 O2 85(47) . . . . ?
Pt3 Pt2 C2 O2 -128(47) . . . . ?
Sn2 Pt2 C2 O2 -95(47) . . . . ?
Pt1 Pt2 C2 O2 136(100) . . . . ?
Pt5 Pt2 C2 O2 -40(47) . . . . ?
Sn4 Pt2 C2 O2 11(47) . . . . ?
Sn2 Pt3 C3 O3 144(25) . . . . ?
Pt4 Pt3 C3 O3 1(25) . . . . ?
Sn5 Pt3 C3 O3 -37(25) . . . . ?
Pt2 Pt3 C3 O3 -179(100) . . . . ?
Sn6 Pt3 C3 O3 38(25) . . . . ?
Pt1 Pt3 C3 O3 -89(25) . . . . ?
Sn1 Pt3 C3 O3 -142(25) . . . . ?
Pt5 Pt3 C3 O3 91(25) . . . . ?
Sn6 Pt4 C4 O4 -17(37) . . . . ?
Sn4 Pt4 C4 O4 -121(37) . . . . ?
Pt2 Pt4 C4 O4 -162(37) . . . . ?
Sn5 Pt4 C4 O4 59(37) . . . . ?
Sn3 Pt4 C4 O4 163(100) . . . . ?
Pt3 Pt4 C4 O4 23(37) . . . . ?
Pt1 Pt4 C4 O4 109(37) . . . . ?
Pt5 Pt4 C4 O4 -68(37) . . . . ?
Sn2 Pt5 C5 O5 -150(100) . . . . ?
Sn6 Pt5 C5 O5 -30(100) . . . . ?
Sn4 Pt5 C5 O5 87(100) . . . . ?
Pt2 Pt5 C5 O5 149(100) . . . . ?
Pt4 Pt5 C5 O5 31(100) . . . . ?
Pt3 Pt5 C5 O5 -93(100) . . . . ?
Cl2 Sn1 O11 C11 40.5(6) . . . . ?
Cl1 Sn1 O11 C11 -52.6(6) . . . . ?
Pt1 Sn1 O11 C11 171.1(5) . . . . ?
Pt2 Sn1 O11 C11 -153.7(6) . . . . ?
Pt3 Sn1 O11 C11 146.2(6) . . . . ?
Cl2 Sn1 O11 Sn2 -137.98(18) . . . . ?
Cl1 Sn1 O11 Sn2 128.94(18) . . . . ?
Pt1 Sn1 O11 Sn2 -7.4(3) . . . . ?
Pt2 Sn1 O11 Sn2 27.83(17) . . . . ?
Pt3 Sn1 O11 Sn2 -32.20(16) . . . . ?
Cl3 Sn2 O11 C11 -41.6(6) . . . . ?
Cl4 Sn2 O11 C11 51.9(5) . . . . ?
Pt5 Sn2 O11 C11 -176.6(5) . . . . ?
Pt3 Sn2 O11 C11 -145.4(6) . . . . ?
Pt2 Sn2 O11 C11 154.0(6) . . . . ?
Cl3 Sn2 O11 Sn1 136.84(18) . . . . ?
Cl4 Sn2 O11 Sn1 -129.70(18) . . . . ?
Pt5 Sn2 O11 Sn1 1.8(3) . . . . ?
Pt3 Sn2 O11 Sn1 33.05(16) . . . . ?
Pt2 Sn2 O11 Sn1 -27.56(16) . . . . ?
Cl7 Sn4 O12 C12 45.3(5) . . . . ?
Cl8 Sn4 O12 C12 -47.8(6) . . . . ?
Pt5 Sn4 O12 C12 -179.6(5) . . . . ?
Pt4 Sn4 O12 C12 148.1(6) . . . . ?
Pt2 Sn4 O12 C12 -151.9(6) . . . . ?
Cl7 Sn4 O12 Sn3 -133.09(19) . . . . ?
Cl8 Sn4 O12 Sn3 133.73(19) . . . . ?
Pt5 Sn4 O12 Sn3 1.9(4) . . . . ?
Pt4 Sn4 O12 Sn3 -30.36(17) . . . . ?
Pt2 Sn4 O12 Sn3 29.70(17) . . . . ?
Cl6 Sn3 O12 C12 47.7(5) . . . . ?
Cl5 Sn3 O12 C12 -46.0(5) . . . . ?
Pt1 Sn3 O12 C12 -176.8(4) . . . . ?
Pt4 Sn3 O12 C12 -148.4(5) . . . . ?
Pt2 Sn3 O12 C12 151.4(5) . . . . ?
Cl6 Sn3 O12 Sn4 -133.82(19) . . . . ?
Cl5 Sn3 O12 Sn4 132.48(19) . . . . ?
Pt1 Sn3 O12 Sn4 1.7(4) . . . . ?
Pt4 Sn3 O12 Sn4 30.05(17) . . . . ?
Pt2 Sn3 O12 Sn4 -30.14(18) . . . . ?
Cl10 Sn5 O13 C13 38.7(6) . . . . ?
Cl9 Sn5 O13 C13 -55.0(6) . . . . ?
Pt1 Sn5 O13 C13 170.4(5) . . . . ?
Pt4 Sn5 O13 C13 139.5(6) . . . . ?
Pt3 Sn5 O13 C13 -160.0(6) . . . . ?
Cl10 Sn5 O13 Sn6 -129.26(18) . . . . ?
Cl9 Sn5 O13 Sn6 137.07(17) . . . . ?
Pt1 Sn5 O13 Sn6 2.5(3) . . . . ?
Pt4 Sn5 O13 Sn6 -28.42(16) . . . . ?
Pt3 Sn5 O13 Sn6 32.04(16) . . . . ?
Cl11 Sn6 O13 C13 55.3(6) . . . . ?
Cl12 Sn6 O13 C13 -36.0(6) . . . . ?
Pt5 Sn6 O13 C13 -171.9(6) . . . . ?
Pt4 Sn6 O13 C13 -138.6(6) . . . . ?
Pt3 Sn6 O13 C13 160.7(6) . . . . ?
Cl11 Sn6 O13 Sn5 -137.36(18) . . . . ?
Cl12 Sn6 O13 Sn5 131.34(17) . . . . ?
Pt5 Sn6 O13 Sn5 -4.5(3) . . . . ?
Pt4 Sn6 O13 Sn5 28.81(16) . . . . ?
Pt3 Sn6 O13 Sn5 -31.92(16) . . . . ?
C113 P1 C101 C102 157.5(6) . . . . ?
C119 P1 C101 C102 35.9(7) . . . . ?
C107 P1 C101 C102 -82.7(6) . . . . ?
C113 P1 C101 C106 -34.4(7) . . . . ?
C119 P1 C101 C106 -156.0(6) . . . . ?
C107 P1 C101 C106 85.5(6) . . . . ?
C106 C101 C102 C103 -1.6(11) . . . . ?
P1 C101 C102 C103 166.7(6) . . . . ?
C101 C102 C103 C104 -0.3(13) . . . . ?
C102 C103 C104 C105 1.9(14) . . . . ?
C103 C104 C105 C106 -1.8(15) . . . . ?
C104 C105 C106 C101 -0.1(13) . . . . ?
C102 C101 C106 C105 1.7(11) . . . . ?
P1 C101 C106 C105 -166.4(6) . . . . ?
C101 P1 C107 C112 154.2(6) . . . . ?
C113 P1 C107 C112 -86.2(6) . . . . ?
C119 P1 C107 C112 33.9(7) . . . . ?
C101 P1 C107 C108 -24.3(7) . . . . ?
C113 P1 C107 C108 95.3(7) . . . . ?
C119 P1 C107 C108 -144.5(6) . . . . ?
C112 C107 C108 C109 2.6(12) . . . . ?
P1 C107 C108 C109 -178.9(7) . . . . ?
C107 C108 C109 C110 -2.4(13) . . . . ?
C108 C109 C110 C111 1.9(14) . . . . ?
C109 C110 C111 C112 -1.6(14) . . . . ?
C110 C111 C112 C107 1.7(12) . . . . ?
C108 C107 C112 C111 -2.2(11) . . . . ?
P1 C107 C112 C111 179.3(6) . . . . ?
C101 P1 C113 C118 140.5(6) . . . . ?
C119 P1 C113 C118 -97.2(6) . . . . ?
C107 P1 C113 C118 22.0(7) . . . . ?
C101 P1 C113 C114 -41.4(7) . . . . ?
C119 P1 C113 C114 81.0(7) . . . . ?
C107 P1 C113 C114 -159.9(6) . . . . ?
C118 C113 C114 C115 1.6(12) . . . . ?
P1 C113 C114 C115 -176.6(7) . . . . ?
C113 C114 C115 C116 -1.1(14) . . . . ?
C114 C115 C116 C117 0.1(14) . . . . ?
C115 C116 C117 C118 0.3(13) . . . . ?
C116 C117 C118 C113 0.3(12) . . . . ?
C114 C113 C118 C117 -1.2(11) . . . . ?
P1 C113 C118 C117 176.9(6) . . . . ?
C101 P1 C119 C124 -80.5(6) . . . . ?
C113 P1 C119 C124 158.0(5) . . . . ?
C107 P1 C119 C124 37.7(6) . . . . ?
C101 P1 C119 C120 97.8(6) . . . . ?
C113 P1 C119 C120 -23.7(7) . . . . ?
C107 P1 C119 C120 -143.9(6) . . . . ?
C124 C119 C120 C121 -0.5(11) . . . . ?
P1 C119 C120 C121 -178.9(6) . . . . ?
C119 C120 C121 C122 -0.3(12) . . . . ?
C120 C121 C122 C123 0.9(12) . . . . ?
C121 C122 C123 C124 -0.5(12) . . . . ?
C122 C123 C124 C119 -0.4(12) . . . . ?
C120 C119 C124 C123 0.9(10) . . . . ?
P1 C119 C124 C123 179.3(6) . . . . ?
C207 P2 C201 C206 42.2(6) . . . . ?
C213 P2 C201 C206 -78.9(6) . . . . ?
C219 P2 C201 C206 161.5(6) . . . . ?
C207 P2 C201 C202 -136.3(6) . . . . ?
C213 P2 C201 C202 102.5(6) . . . . ?
C219 P2 C201 C202 -17.1(7) . . . . ?
C206 C201 C202 C203 0.5(11) . . . . ?
P2 C201 C202 C203 179.0(5) . . . . ?
C201 C202 C203 C204 0.3(11) . . . . ?
C202 C203 C204 C205 -0.6(11) . . . . ?
C203 C204 C205 C206 0.1(11) . . . . ?
C202 C201 C206 C205 -1.0(11) . . . . ?
P2 C201 C206 C205 -179.6(6) . . . . ?
C204 C205 C206 C201 0.7(11) . . . . ?
C213 P2 C207 C212 -16.2(7) . . . . ?
C219 P2 C207 C212 103.2(6) . . . . ?
C201 P2 C207 C212 -137.4(6) . . . . ?
C213 P2 C207 C208 165.9(6) . . . . ?
C219 P2 C207 C208 -74.7(6) . . . . ?
C201 P2 C207 C208 44.8(6) . . . . ?
C212 C207 C208 C209 0.3(11) . . . . ?
P2 C207 C208 C209 178.2(6) . . . . ?
C207 C208 C209 C210 -0.4(11) . . . . ?
C208 C209 C210 C211 0.2(12) . . . . ?
C209 C210 C211 C212 0.1(12) . . . . ?
C210 C211 C212 C207 -0.2(11) . . . . ?
C208 C207 C212 C211 0.0(10) . . . . ?
P2 C207 C212 C211 -177.8(5) . . . . ?
C207 P2 C213 C214 -81.7(7) . . . . ?
C219 P2 C213 C214 157.8(6) . . . . ?
C201 P2 C213 C214 36.9(8) . . . . ?
C207 P2 C213 C218 97.9(7) . . . . ?
C219 P2 C213 C218 -22.6(8) . . . . ?
C201 P2 C213 C218 -143.4(7) . . . . ?
C218 C213 C214 C215 -0.5(13) . . . . ?
P2 C213 C214 C215 179.1(7) . . . . ?
C213 C214 C215 C216 0.3(15) . . . . ?
C214 C215 C216 C217 0.8(16) . . . . ?
C215 C216 C217 C218 -1.8(17) . . . . ?
C216 C217 C218 C213 1.6(16) . . . . ?
C214 C213 C218 C217 -0.5(14) . . . . ?
P2 C213 C218 C217 179.9(8) . . . . ?
C207 P2 C219 C224 -172.3(5) . . . . ?
C213 P2 C219 C224 -51.2(6) . . . . ?
C201 P2 C219 C224 70.2(6) . . . . ?
C207 P2 C219 C220 7.7(6) . . . . ?
C213 P2 C219 C220 128.9(5) . . . . ?
C201 P2 C219 C220 -109.7(6) . . . . ?
C224 C219 C220 C221 0.7(10) . . . . ?
P2 C219 C220 C221 -179.4(5) . . . . ?
C219 C220 C221 C222 -0.4(11) . . . . ?
C220 C221 C222 C223 -0.2(12) . . . . ?
C221 C222 C223 C224 0.6(12) . . . . ?
C222 C223 C224 C219 -0.3(11) . . . . ?
C220 C219 C224 C223 -0.3(10) . . . . ?
P2 C219 C224 C223 179.7(6) . . . . ?
C307 P3 C301 C302 -0.7(8) . . . . ?
C313 P3 C301 C302 -118.8(7) . . . . ?
C319 P3 C301 C302 115.9(7) . . . . ?
C307 P3 C301 C306 179.4(7) . . . . ?
C313 P3 C301 C306 61.2(8) . . . . ?
C319 P3 C301 C306 -64.1(8) . . . . ?
C306 C301 C302 C303 0.6(12) . . . . ?
P3 C301 C302 C303 -179.3(6) . . . . ?
C301 C302 C303 C304 -1.2(12) . . . . ?
C302 C303 C304 C305 0.9(14) . . . . ?
C303 C304 C305 C306 0.2(16) . . . . ?
C304 C305 C306 C301 -0.9(16) . . . . ?
C302 C301 C306 C305 0.5(14) . . . . ?
P3 C301 C306 C305 -179.6(8) . . . . ?
C313 P3 C307 C312 13.3(7) . . . . ?
C301 P3 C307 C312 -105.1(6) . . . . ?
C319 P3 C307 C312 136.4(6) . . . . ?
C313 P3 C307 C308 -167.2(5) . . . . ?
C301 P3 C307 C308 74.5(6) . . . . ?
C319 P3 C307 C308 -44.0(6) . . . . ?
C312 C307 C308 C309 -1.1(10) . . . . ?
P3 C307 C308 C309 179.3(5) . . . . ?
C307 C308 C309 C310 1.0(11) . . . . ?
C308 C309 C310 C311 -1.1(11) . . . . ?
C309 C310 C311 C312 1.2(11) . . . . ?
C310 C311 C312 C307 -1.3(10) . . . . ?
C308 C307 C312 C311 1.3(10) . . . . ?
P3 C307 C312 C311 -179.1(5) . . . . ?
C307 P3 C313 C314 -105.5(7) . . . . ?
C301 P3 C313 C314 14.3(8) . . . . ?
C319 P3 C313 C314 136.6(7) . . . . ?
C307 P3 C313 C318 67.4(8) . . . . ?
C301 P3 C313 C318 -172.8(8) . . . . ?
C319 P3 C313 C318 -50.5(9) . . . . ?
C318 C313 C314 C315 -1.8(15) . . . . ?
P3 C313 C314 C315 171.4(8) . . . . ?
C313 C314 C315 C316 0.1(17) . . . . ?
C314 C315 C316 C317 0.8(18) . . . . ?
C315 C316 C317 C318 0.0(17) . . . . ?
C316 C317 C318 C313 -1.8(17) . . . . ?
C314 C313 C318 C317 2.6(15) . . . . ?
P3 C313 C318 C317 -170.4(8) . . . . ?
C307 P3 C319 C324 -65.2(8) . . . . ?
C313 P3 C319 C324 53.7(9) . . . . ?
C301 P3 C319 C324 175.4(8) . . . . ?
C307 P3 C319 C320 109.2(7) . . . . ?
C313 P3 C319 C320 -131.8(7) . . . . ?
C301 P3 C319 C320 -10.1(8) . . . . ?
C324 C319 C320 C321 -1.5(13) . . . . ?
P3 C319 C320 C321 -176.1(6) . . . . ?
C319 C320 C321 C322 -0.3(13) . . . . ?
C320 C321 C322 C323 2.7(14) . . . . ?
C321 C322 C323 C324 -3.2(17) . . . . ?
C320 C319 C324 C323 1.0(16) . . . . ?
P3 C319 C324 C323 175.6(9) . . . . ?
C322 C323 C324 C319 1.4(18) . . . . ?

_diffrn_measured_fraction_theta_max 0.993
_diffrn_reflns_theta_full        28.00
_diffrn_measured_fraction_theta_full 0.993
_refine_diff_density_max         2.142
_refine_diff_density_min         -1.342
_refine_diff_density_rms         0.208
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1_Me_4acetone
_database_code_depnum_ccdc_archive 'CCDC 1439437'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C92 H93 Cl12 O12 P3 Pt5 Sn6'
_chemical_formula_weight         3596.56

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Orthorhombic
_symmetry_space_group_name_H-M   Pna2(1)

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x+1/2, -y+1/2, z'
'-x+1/2, y+1/2, z+1/2'

_cell_length_a                   29.225(5)
_cell_length_b                   14.528(3)
_cell_length_c                   27.190(5)
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_volume                     11545(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    291(2)
_cell_measurement_reflns_used    9907
_cell_measurement_theta_min      2.1665
_cell_measurement_theta_max      23.997

_exptl_crystal_description       plate
_exptl_crystal_colour            orange
_exptl_crystal_size_max          0.24
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.16
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.069
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             6720
_exptl_absorpt_coefficient_mu    7.676
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.2602
_exptl_absorpt_correction_T_max  0.3731
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1795 (selected reflections only, before parameter refinement)
 R(int) = 0.0998 (selected reflections only, after parameter refinement)
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      291(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            103341
_diffrn_reflns_av_R_equivalents  0.0937
_diffrn_reflns_av_unetI/netI     0.0919
_diffrn_reflns_limit_h_min       -34
_diffrn_reflns_limit_h_max       34
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_theta_min         1.39
_diffrn_reflns_theta_max         25.03
_reflns_number_total             20291
_reflns_number_gt                14865
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. The following restraints
 were applied (given as SHELXL lines): 
 isor .02 cl1 cl3 cl6
 isor .02 c12 c13 o1 o5 c105 c109 c110 c111 c115 c116 c117 c118
 isor .02 c122 c123 c203 c204 c205 c206 c208 c209 c210 c211 c212
 isor .02 c214 c215 c216 c217 c219 c220 c221 c222 c223 c224 c303
 isor .02 c304 c305 c306 c308 c309 c310 c315 c321 c322 c323 c324
 simu p1 > c124
 simu p2 > c224
 AFIX 66 on all Ph rings
 simu .01 p3 > c324
 delu p3 c319 c320 c321 c322 c323
 delu c303 c304
 simu .01 c401 > o402
 dfix 1.51 c401 c402 c402 c403
 dfix 1.21 c402 o402
 dfix 2.58 c401 c403
 same c411 > o412
 same c421 > o422
 same c431 > o432
 flat c401 > o402
 simu .01 c411 > o412
 dfix 1.51 c411 c412 c412 c413
 dfix 1.21 c412 o412
 dfix 2.58 c411 c413
 flat c411 > o412
 simu .01 c421 > o422
 dfix 1.51 c421 c422 c422 c423
 dfix 1.21 c422 o422
 dfix 2.58 c421 c423
 flat c421 > o422
 simu .01 c431 > o432
 dfix 1.51 c431 c432 c432 c433
 dfix 1.21 c432 o432
 dfix 2.58 c431 c433
 flat c431 > o432
 The asymmetric unit of the unit cell contains one cluster anion, three 
 [PPh4]+ cations and four acetone molecules (all located on general positions). 
 Some C-atoms have been restrained to isotropic behaviour (ISOR command in 
 SHELXL, s.u. 0.02). The C-atoms of the Ph-rings have been constrained to fit 
 regular hexagons (AFIX 66 command in SHELXL). Similar U restraints have been 
 applied to the [PPh4]+ cations (SIMU command in SHELXL, s.u. 0.02). The 
 acetone molecules have been refined isotropically and restrained to have 
 similar geometries (SAME command in SHELXL, s.u. 0.02). Restraints to bond 
 distances were applied as follow (s.u. 0.02): 1.21 Å for C O and 1.51 Å 
 for C C in acetone.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0738P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.051(5)
_refine_ls_number_reflns         20291
_refine_ls_number_parameters     947
_refine_ls_number_restraints     799
_refine_ls_R_factor_all          0.0886
_refine_ls_R_factor_gt           0.0589
_refine_ls_wR_factor_ref         0.1437
_refine_ls_wR_factor_gt          0.1303
_refine_ls_goodness_of_fit_ref   1.009
_refine_ls_restrained_S_all      1.001
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.31055(2) 0.51858(4) 0.42744(2) 0.05017(17) Uani 1 1 d . . .
Pt2 Pt 0.39913(2) 0.47850(4) 0.38950(2) 0.04699(16) Uani 1 1 d . . .
Pt3 Pt 0.35389(2) 0.64300(4) 0.35995(3) 0.04983(16) Uani 1 1 d . . .
Pt4 Pt 0.32270(2) 0.46971(4) 0.32588(2) 0.04778(16) Uani 1 1 d . . .
Pt5 Pt 0.40719(2) 0.54251(5) 0.29019(2) 0.05447(18) Uani 1 1 d . . .
Sn1 Sn 0.38004(4) 0.61630(7) 0.46100(4) 0.0514(3) Uani 1 1 d . . .
Sn2 Sn 0.45006(4) 0.63680(8) 0.36082(5) 0.0613(3) Uani 1 1 d . . .
Sn3 Sn 0.25975(4) 0.60297(8) 0.35973(5) 0.0604(3) Uani 1 1 d . . .
Sn4 Sn 0.32948(4) 0.61827(8) 0.25869(4) 0.0590(3) Uani 1 1 d . . .
Sn5 Sn 0.33261(4) 0.34447(7) 0.40651(4) 0.0538(3) Uani 1 1 d . . .
Sn6 Sn 0.39810(4) 0.36148(8) 0.30234(4) 0.0548(3) Uani 1 1 d . . .
Cl1 Cl 0.3565(2) 0.7547(3) 0.5031(2) 0.0927(17) Uani 1 1 d U . .
Cl2 Cl 0.41572(18) 0.5550(3) 0.53389(18) 0.0775(14) Uani 1 1 d . . .
Cl3 Cl 0.52590(19) 0.5864(5) 0.3755(3) 0.116(2) Uani 1 1 d U . .
Cl4 Cl 0.4734(2) 0.7884(3) 0.3364(2) 0.0961(17) Uani 1 1 d . . .
Cl5 Cl 0.2251(2) 0.7418(4) 0.3893(2) 0.0970(17) Uani 1 1 d . . .
Cl6 Cl 0.18791(19) 0.5278(4) 0.3495(3) 0.112(2) Uani 1 1 d U . .
Cl7 Cl 0.3391(2) 0.7665(4) 0.2218(3) 0.114(2) Uani 1 1 d . . .
Cl8 Cl 0.2998(2) 0.5532(4) 0.18354(18) 0.0895(16) Uani 1 1 d . . .
Cl9 Cl 0.3658(2) 0.2492(3) 0.46957(17) 0.0784(14) Uani 1 1 d . . .
Cl10 Cl 0.26413(19) 0.2566(3) 0.4029(2) 0.0901(16) Uani 1 1 d . . .
Cl11 Cl 0.46995(19) 0.2807(4) 0.3006(2) 0.0924(16) Uani 1 1 d . . .
Cl12 Cl 0.3723(2) 0.2824(4) 0.22981(17) 0.0878(16) Uani 1 1 d . . .
O11 O 0.4424(4) 0.6768(8) 0.4349(4) 0.072(3) Uani 1 1 d . . .
O12 O 0.2628(4) 0.6477(8) 0.2858(4) 0.072(3) Uani 1 1 d . . .
O13 O 0.3676(4) 0.2670(7) 0.3511(4) 0.065(3) Uani 1 1 d . . .
C11 C 0.4719(6) 0.7313(12) 0.4639(8) 0.083(6) Uani 1 1 d . . .
H11A H 0.4590 0.7388 0.4961 0.125 Uiso 1 1 calc R . .
H11B H 0.4755 0.7906 0.4488 0.125 Uiso 1 1 calc R . .
H11C H 0.5011 0.7018 0.4665 0.125 Uiso 1 1 calc R . .
C12 C 0.2258(8) 0.6825(17) 0.2572(8) 0.115(8) Uani 1 1 d U . .
H12A H 0.1993 0.6902 0.2777 0.172 Uiso 1 1 calc R . .
H12B H 0.2188 0.6400 0.2312 0.172 Uiso 1 1 calc R . .
H12C H 0.2342 0.7409 0.2433 0.172 Uiso 1 1 calc R . .
C13 C 0.3748(8) 0.1675(12) 0.3502(8) 0.098(7) Uani 1 1 d U . .
H13A H 0.3577 0.1395 0.3764 0.147 Uiso 1 1 calc R . .
H13B H 0.4068 0.1545 0.3545 0.147 Uiso 1 1 calc R . .
H13C H 0.3647 0.1432 0.3192 0.147 Uiso 1 1 calc R . .
C1 C 0.2686(7) 0.5112(14) 0.4759(7) 0.076(6) Uani 1 1 d . . .
C2 C 0.4446(7) 0.4201(13) 0.4238(7) 0.070(5) Uani 1 1 d . . .
C3 C 0.3472(5) 0.7751(13) 0.3626(7) 0.058(4) Uani 1 1 d . . .
C4 C 0.2813(5) 0.3987(12) 0.2911(7) 0.060(5) Uani 1 1 d . . .
C5 C 0.4470(6) 0.5446(15) 0.2377(8) 0.083(6) Uani 1 1 d . . .
O1 O 0.2423(6) 0.5058(12) 0.5077(7) 0.119(6) Uani 1 1 d U . .
O2 O 0.4731(5) 0.3833(10) 0.4448(5) 0.095(5) Uani 1 1 d . . .
O3 O 0.3452(5) 0.8505(9) 0.3645(6) 0.098(5) Uani 1 1 d . . .
O4 O 0.2536(5) 0.3555(11) 0.2707(6) 0.108(5) Uani 1 1 d . . .
O5 O 0.4738(6) 0.5452(12) 0.2057(6) 0.121(6) Uani 1 1 d U . .
P1 P 0.14536(17) 0.0957(3) 0.49763(18) 0.0637(12) Uani 1 1 d . . .
C101 C 0.2009(4) 0.0455(8) 0.4962(5) 0.068(5) Uani 1 1 d GU . .
C102 C 0.2044(5) -0.0495(8) 0.4914(6) 0.094(6) Uani 1 1 d GU . .
H102 H 0.1782 -0.0858 0.4928 0.112 Uiso 1 1 calc R . .
C103 C 0.2470(6) -0.0902(7) 0.4847(5) 0.103(7) Uani 1 1 d GU . .
H103 H 0.2493 -0.1537 0.4815 0.124 Uiso 1 1 calc R . .
C104 C 0.2861(4) -0.0359(11) 0.4827(6) 0.094(6) Uani 1 1 d GU . .
H104 H 0.3146 -0.0631 0.4781 0.113 Uiso 1 1 calc R . .
C105 C 0.2826(4) 0.0591(10) 0.4874(6) 0.103(7) Uani 1 1 d GU . .
H105 H 0.3088 0.0955 0.4860 0.123 Uiso 1 1 calc R . .
C106 C 0.2400(5) 0.0998(6) 0.4941(5) 0.080(5) Uani 1 1 d GU . .
H106 H 0.2377 0.1634 0.4973 0.096 Uiso 1 1 calc R . .
C107 C 0.1455(5) 0.2124(7) 0.5191(6) 0.082(6) Uani 1 1 d GU . .
C108 C 0.1565(5) 0.2825(10) 0.4864(4) 0.085(6) Uani 1 1 d GU . .
H108 H 0.1656 0.2683 0.4545 0.102 Uiso 1 1 calc R . .
C109 C 0.1539(5) 0.3739(9) 0.5013(6) 0.108(7) Uani 1 1 d GU . .
H109 H 0.1612 0.4208 0.4794 0.130 Uiso 1 1 calc R . .
C110 C 0.1402(6) 0.3952(8) 0.5489(6) 0.121(8) Uani 1 1 d GU . .
H110 H 0.1385 0.4563 0.5589 0.146 Uiso 1 1 calc R . .
C111 C 0.1292(6) 0.3251(12) 0.5817(5) 0.120(8) Uani 1 1 d GU . .
H111 H 0.1201 0.3394 0.6135 0.144 Uiso 1 1 calc R . .
C112 C 0.1318(5) 0.2337(10) 0.5668(5) 0.109(7) Uani 1 1 d GU . .
H112 H 0.1245 0.1869 0.5887 0.131 Uiso 1 1 calc R . .
C113 C 0.1222(5) 0.1051(10) 0.4375(4) 0.081(5) Uani 1 1 d GU . .
C114 C 0.0822(5) 0.1550(9) 0.4303(5) 0.084(5) Uani 1 1 d GU . .
H114 H 0.0680 0.1837 0.4568 0.101 Uiso 1 1 calc R . .
C115 C 0.0634(5) 0.1620(10) 0.3835(6) 0.115(7) Uani 1 1 d GU . .
H115 H 0.0366 0.1954 0.3787 0.138 Uiso 1 1 calc R . .
C116 C 0.0846(6) 0.1191(12) 0.3439(4) 0.132(9) Uani 1 1 d GU . .
H116 H 0.0720 0.1238 0.3126 0.158 Uiso 1 1 calc R . .
C117 C 0.1246(6) 0.0692(11) 0.3511(5) 0.144(9) Uani 1 1 d GU . .
H117 H 0.1388 0.0405 0.3246 0.173 Uiso 1 1 calc R . .
C118 C 0.1434(5) 0.0622(10) 0.3979(6) 0.114(7) Uani 1 1 d GU . .
H118 H 0.1702 0.0288 0.4027 0.137 Uiso 1 1 calc R . .
C119 C 0.1104(4) 0.0253(8) 0.5356(4) 0.063(4) Uani 1 1 d GU . .
C120 C 0.0679(4) -0.0062(8) 0.5201(4) 0.068(5) Uani 1 1 d GU . .
H120 H 0.0571 0.0093 0.4890 0.082 Uiso 1 1 calc R . .
C121 C 0.0416(4) -0.0611(8) 0.5509(6) 0.085(6) Uani 1 1 d GU . .
H121 H 0.0132 -0.0823 0.5405 0.103 Uiso 1 1 calc R . .
C122 C 0.0578(5) -0.0844(8) 0.5974(5) 0.096(6) Uani 1 1 d GU . .
H122 H 0.0401 -0.1211 0.6180 0.115 Uiso 1 1 calc R . .
C123 C 0.1002(5) -0.0528(9) 0.6129(4) 0.094(6) Uani 1 1 d GU . .
H123 H 0.1111 -0.0684 0.6440 0.113 Uiso 1 1 calc R . .
C124 C 0.1266(4) 0.0021(9) 0.5821(4) 0.078(5) Uani 1 1 d GU . .
H124 H 0.1550 0.0232 0.5925 0.094 Uiso 1 1 calc R . .
P2 P 0.2940(2) 0.5614(3) 0.6741(2) 0.0771(15) Uani 1 1 d . . .
C201 C 0.2944(5) 0.4575(8) 0.6401(5) 0.076(5) Uani 1 1 d GU . .
C202 C 0.3295(4) 0.4418(9) 0.6066(5) 0.088(6) Uani 1 1 d GU . .
H202 H 0.3544 0.4817 0.6053 0.105 Uiso 1 1 calc R . .
C203 C 0.3274(5) 0.3666(10) 0.5752(5) 0.109(7) Uani 1 1 d GU . .
H203 H 0.3508 0.3561 0.5527 0.131 Uiso 1 1 calc R . .
C204 C 0.2902(6) 0.3070(8) 0.5772(5) 0.104(7) Uani 1 1 d GU . .
H204 H 0.2888 0.2567 0.5561 0.125 Uiso 1 1 calc R . .
C205 C 0.2552(5) 0.3227(9) 0.6107(6) 0.119(7) Uani 1 1 d GU . .
H205 H 0.2303 0.2829 0.6121 0.142 Uiso 1 1 calc R . .
C206 C 0.2573(4) 0.3980(10) 0.6422(5) 0.104(7) Uani 1 1 d GU . .
H206 H 0.2338 0.4085 0.6646 0.125 Uiso 1 1 calc R . .
C207 C 0.2775(6) 0.5385(12) 0.7366(5) 0.092(6) Uani 1 1 d GU . .
C208 C 0.2824(6) 0.4504(10) 0.7558(7) 0.132(8) Uani 1 1 d GU . .
H208 H 0.2961 0.4044 0.7371 0.158 Uiso 1 1 calc R . .
C209 C 0.2666(7) 0.4309(11) 0.8029(7) 0.151(9) Uani 1 1 d GU . .
H209 H 0.2699 0.3719 0.8157 0.182 Uiso 1 1 calc R . .
C210 C 0.2461(6) 0.4995(15) 0.8308(5) 0.125(8) Uani 1 1 d GU . .
H210 H 0.2356 0.4865 0.8624 0.150 Uiso 1 1 calc R . .
C211 C 0.2413(6) 0.5877(13) 0.8117(6) 0.145(9) Uani 1 1 d GU . .
H211 H 0.2275 0.6336 0.8303 0.174 Uiso 1 1 calc R . .
C212 C 0.2570(6) 0.6072(9) 0.7646(7) 0.133(8) Uani 1 1 d GU . .
H212 H 0.2538 0.6662 0.7517 0.159 Uiso 1 1 calc R . .
C213 C 0.3520(4) 0.6039(10) 0.6743(5) 0.077(5) Uani 1 1 d GU . .
C214 C 0.3807(6) 0.5641(9) 0.7090(5) 0.108(7) Uani 1 1 d GU . .
H214 H 0.3697 0.5185 0.7299 0.130 Uiso 1 1 calc R . .
C215 C 0.4260(5) 0.5925(12) 0.7127(6) 0.135(8) Uani 1 1 d GU . .
H215 H 0.4452 0.5659 0.7359 0.162 Uiso 1 1 calc R . .
C216 C 0.4426(4) 0.6607(12) 0.6815(7) 0.123(8) Uani 1 1 d GU . .
H216 H 0.4729 0.6798 0.6839 0.148 Uiso 1 1 calc R . .
C217 C 0.4138(6) 0.7005(10) 0.6468(6) 0.117(8) Uani 1 1 d GU . .
H217 H 0.4249 0.7461 0.6260 0.140 Uiso 1 1 calc R . .
C218 C 0.3685(5) 0.6721(9) 0.6432(5) 0.095(6) Uani 1 1 d GU . .
H218 H 0.3493 0.6987 0.6199 0.114 Uiso 1 1 calc R . .
C219 C 0.2585(6) 0.6457(11) 0.6459(7) 0.101(7) Uani 1 1 d GU . .
C220 C 0.2557(6) 0.7358(12) 0.6628(6) 0.122(8) Uani 1 1 d GU . .
H220 H 0.2749 0.7557 0.6879 0.147 Uiso 1 1 calc R . .
C221 C 0.2242(7) 0.7962(10) 0.6421(7) 0.137(9) Uani 1 1 d GU . .
H221 H 0.2224 0.8565 0.6533 0.164 Uiso 1 1 calc R . .
C222 C 0.1956(6) 0.7665(15) 0.6045(7) 0.171(11) Uani 1 1 d GU . .
H222 H 0.1745 0.8069 0.5906 0.205 Uiso 1 1 calc R . .
C223 C 0.1983(6) 0.6763(17) 0.5876(6) 0.185(11) Uani 1 1 d GU . .
H223 H 0.1792 0.6564 0.5625 0.222 Uiso 1 1 calc R . .
C224 C 0.2298(7) 0.6159(11) 0.6083(7) 0.159(10) Uani 1 1 d GU . .
H224 H 0.2317 0.5556 0.5971 0.190 Uiso 1 1 calc R . .
P3 P 0.4575(2) 0.0502(3) 0.5668(2) 0.0723(14) Uani 1 1 d U . .
C301 C 0.4896(5) -0.0395(7) 0.5954(5) 0.087(4) Uani 1 1 d GU . .
C302 C 0.4817(4) -0.0592(8) 0.6447(5) 0.091(4) Uani 1 1 d GU . .
H302 H 0.4582 -0.0296 0.6615 0.109 Uiso 1 1 calc R . .
C303 C 0.5089(5) -0.1232(9) 0.6690(4) 0.097(4) Uani 1 1 d GU . .
H303 H 0.5036 -0.1364 0.7020 0.116 Uiso 1 1 calc R . .
C304 C 0.5440(5) -0.1676(8) 0.6439(6) 0.103(4) Uani 1 1 d GU . .
H304 H 0.5622 -0.2104 0.6602 0.123 Uiso 1 1 calc R . .
C305 C 0.5519(4) -0.1479(9) 0.5946(6) 0.108(5) Uani 1 1 d GU . .
H305 H 0.5754 -0.1776 0.5779 0.130 Uiso 1 1 calc R . .
C306 C 0.5247(5) -0.0839(9) 0.5704(4) 0.104(5) Uani 1 1 d GU . .
H306 H 0.5300 -0.0707 0.5374 0.125 Uiso 1 1 calc R . .
C307 C 0.4005(4) 0.0334(10) 0.5870(6) 0.093(4) Uani 1 1 d GU . .
C308 C 0.3751(5) 0.1060(7) 0.6059(6) 0.106(5) Uani 1 1 d GU . .
H308 H 0.3876 0.1649 0.6069 0.127 Uiso 1 1 calc R . .
C309 C 0.3311(5) 0.0907(9) 0.6234(6) 0.115(5) Uani 1 1 d GU . .
H309 H 0.3140 0.1393 0.6360 0.138 Uiso 1 1 calc R . .
C310 C 0.3124(4) 0.0027(11) 0.6219(6) 0.108(5) Uani 1 1 d GU . .
H310 H 0.2830 -0.0076 0.6335 0.129 Uiso 1 1 calc R . .
C311 C 0.3379(5) -0.0700(8) 0.6030(6) 0.098(4) Uani 1 1 d GU . .
H311 H 0.3254 -0.1289 0.6020 0.118 Uiso 1 1 calc R . .
C312 C 0.3819(5) -0.0546(8) 0.5855(5) 0.094(4) Uani 1 1 d GU . .
H312 H 0.3990 -0.1033 0.5729 0.113 Uiso 1 1 calc R . .
C313 C 0.4625(6) 0.0418(9) 0.5015(4) 0.093(4) Uani 1 1 d GU . .
C314 C 0.4308(5) -0.0081(9) 0.4741(5) 0.097(4) Uani 1 1 d GU . .
H314 H 0.4060 -0.0357 0.4897 0.117 Uiso 1 1 calc R . .
C315 C 0.4363(5) -0.0167(9) 0.4236(5) 0.104(5) Uani 1 1 d GU . .
H315 H 0.4151 -0.0500 0.4053 0.124 Uiso 1 1 calc R . .
C316 C 0.4733(6) 0.0246(10) 0.4003(4) 0.110(5) Uani 1 1 d GU . .
H316 H 0.4770 0.0189 0.3665 0.132 Uiso 1 1 calc R . .
C317 C 0.5050(5) 0.0745(10) 0.4277(6) 0.112(5) Uani 1 1 d GU . .
H317 H 0.5298 0.1021 0.4121 0.135 Uiso 1 1 calc R . .
C318 C 0.4995(5) 0.0830(9) 0.4782(6) 0.105(5) Uani 1 1 d GU . .
H318 H 0.5207 0.1164 0.4965 0.126 Uiso 1 1 calc R . .
C319 C 0.4784(5) 0.1620(6) 0.5838(5) 0.082(4) Uani 1 1 d GU . .
C320 C 0.4615(4) 0.2385(8) 0.5590(4) 0.088(4) Uani 1 1 d GU . .
H320 H 0.4406 0.2309 0.5336 0.106 Uiso 1 1 calc R . .
C321 C 0.4759(5) 0.3262(7) 0.5723(5) 0.091(4) Uani 1 1 d GU . .
H321 H 0.4646 0.3774 0.5558 0.110 Uiso 1 1 calc R . .
C322 C 0.5072(5) 0.3375(6) 0.6104(5) 0.093(4) Uani 1 1 d GU . .
H322 H 0.5168 0.3962 0.6193 0.112 Uiso 1 1 calc R . .
C323 C 0.5241(4) 0.2610(9) 0.6352(4) 0.090(4) Uani 1 1 d GU . .
H323 H 0.5450 0.2686 0.6606 0.108 Uiso 1 1 calc R . .
C324 C 0.5097(5) 0.1733(7) 0.6219(4) 0.087(4) Uani 1 1 d GU . .
H324 H 0.5210 0.1221 0.6384 0.104 Uiso 1 1 calc R . .
C401 C 0.3534(8) 1.0154(19) 0.2198(10) 0.155(10) Uiso 1 1 d DU . .
H40A H 0.3390 1.0189 0.1881 0.233 Uiso 1 1 calc R . .
H40B H 0.3558 1.0761 0.2336 0.233 Uiso 1 1 calc R . .
H40C H 0.3354 0.9773 0.2412 0.233 Uiso 1 1 calc R . .
C402 C 0.3993(7) 0.9756(12) 0.2146(7) 0.112(7) Uiso 1 1 d DU . .
C403 C 0.4293(9) 0.966(2) 0.2582(10) 0.184(12) Uiso 1 1 d DU . .
H40D H 0.4134 0.9880 0.2869 0.276 Uiso 1 1 calc R . .
H40E H 0.4566 1.0021 0.2534 0.276 Uiso 1 1 calc R . .
H40F H 0.4374 0.9028 0.2626 0.276 Uiso 1 1 calc R . .
O402 O 0.4137(7) 0.9504(13) 0.1761(7) 0.159(7) Uiso 1 1 d DU . .
C411 C 0.0881(15) 0.372(3) 0.3228(13) 0.310(19) Uiso 1 1 d DU . .
H41A H 0.1116 0.3322 0.3356 0.465 Uiso 1 1 calc R . .
H41B H 0.0595 0.3389 0.3221 0.465 Uiso 1 1 calc R . .
H41C H 0.0851 0.4250 0.3433 0.465 Uiso 1 1 calc R . .
C412 C 0.1003(10) 0.4004(19) 0.2725(12) 0.284(15) Uiso 1 1 d DU . .
C413 C 0.1421(12) 0.365(3) 0.2487(14) 0.269(18) Uiso 1 1 d DU . .
H41D H 0.1482 0.4005 0.2195 0.404 Uiso 1 1 calc R . .
H41E H 0.1379 0.3018 0.2400 0.404 Uiso 1 1 calc R . .
H41F H 0.1674 0.3708 0.2710 0.404 Uiso 1 1 calc R . .
O412 O 0.0766(12) 0.453(2) 0.2517(13) 0.325(16) Uiso 1 1 d DU . .
C421 C 0.6131(17) 0.712(4) 0.2922(13) 0.39(2) Uiso 1 1 d DU . .
H42A H 0.6301 0.6561 0.2978 0.589 Uiso 1 1 calc R . .
H42B H 0.5842 0.7080 0.3089 0.589 Uiso 1 1 calc R . .
H42C H 0.6301 0.7632 0.3046 0.589 Uiso 1 1 calc R . .
C422 C 0.6053(11) 0.7236(19) 0.2390(12) 0.352(17) Uiso 1 1 d DU . .
C423 C 0.5612(13) 0.754(4) 0.2185(17) 0.37(2) Uiso 1 1 d DU . .
H42D H 0.5662 0.7830 0.1872 0.552 Uiso 1 1 calc R . .
H42E H 0.5472 0.7974 0.2406 0.552 Uiso 1 1 calc R . .
H42F H 0.5414 0.7020 0.2144 0.552 Uiso 1 1 calc R . .
O422 O 0.6352(12) 0.708(3) 0.2111(13) 0.332(16) Uiso 1 1 d DU . .
C431 C 0.1190(13) 0.7614(19) 0.4620(13) 0.203(13) Uiso 1 1 d DU . .
H43A H 0.1367 0.7716 0.4912 0.304 Uiso 1 1 calc R . .
H43B H 0.0912 0.7966 0.4637 0.304 Uiso 1 1 calc R . .
H43C H 0.1363 0.7802 0.4337 0.304 Uiso 1 1 calc R . .
C432 C 0.1078(9) 0.6631(19) 0.4579(10) 0.228(12) Uiso 1 1 d DU . .
C433 C 0.0833(13) 0.623(2) 0.4157(12) 0.237(15) Uiso 1 1 d DU . .
H43D H 0.0801 0.5575 0.4206 0.355 Uiso 1 1 calc R . .
H43E H 0.1002 0.6338 0.3861 0.355 Uiso 1 1 calc R . .
H43F H 0.0535 0.6502 0.4131 0.355 Uiso 1 1 calc R . .
O432 O 0.1200(12) 0.614(2) 0.4900(11) 0.303(14) Uiso 1 1 d DU . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.80(2) . ?
Pt1 Sn1 2.6404(13) . ?
Pt1 Sn3 2.6642(14) . ?
Pt1 Sn5 2.6717(13) . ?
Pt1 Pt2 2.8469(10) . ?
Pt1 Pt3 2.8704(9) . ?
Pt1 Pt4 2.8734(10) . ?
Pt2 C2 1.83(2) . ?
Pt2 Sn5 2.7903(13) . ?
Pt2 Pt4 2.8280(9) . ?
Pt2 Sn1 2.8459(13) . ?
Pt2 Pt3 2.8470(9) . ?
Pt2 Sn2 2.8482(13) . ?
Pt2 Pt5 2.8655(10) . ?
Pt2 Sn6 2.9167(13) . ?
Pt3 C3 1.931(19) . ?
Pt3 Sn3 2.8121(14) . ?
Pt3 Sn2 2.8122(14) . ?
Pt3 Pt4 2.8333(9) . ?
Pt3 Pt5 2.8559(10) . ?
Pt3 Sn4 2.8668(14) . ?
Pt3 Sn1 2.8781(14) . ?
Pt4 C4 1.85(2) . ?
Pt4 Sn6 2.7814(14) . ?
Pt4 Sn3 2.8251(13) . ?
Pt4 Sn4 2.8347(14) . ?
Pt4 Pt5 2.8560(10) . ?
Pt4 Sn5 2.8636(13) . ?
Pt5 C5 1.84(2) . ?
Pt5 Sn6 2.6639(14) . ?
Pt5 Sn4 2.6652(14) . ?
Pt5 Sn2 2.6712(14) . ?
Sn1 O11 2.143(12) . ?
Sn1 Cl2 2.410(5) . ?
Sn1 Cl1 2.415(5) . ?
Sn2 O11 2.108(11) . ?
Sn2 Cl3 2.368(6) . ?
Sn2 Cl4 2.400(5) . ?
Sn3 O12 2.114(12) . ?
Sn3 Cl6 2.383(6) . ?
Sn3 Cl5 2.395(5) . ?
Sn4 O12 2.128(12) . ?
Sn4 Cl7 2.391(5) . ?
Sn4 Cl8 2.412(5) . ?
Sn5 O13 2.142(10) . ?
Sn5 Cl10 2.376(5) . ?
Sn5 Cl9 2.408(5) . ?
Sn6 O13 2.106(11) . ?
Sn6 Cl12 2.404(5) . ?
Sn6 Cl11 2.406(5) . ?
O11 C11 1.41(2) . ?
O12 C12 1.43(2) . ?
O13 C13 1.460(19) . ?
C11 H11A 0.9600 . ?
C11 H11B 0.9600 . ?
C11 H11C 0.9600 . ?
C12 H12A 0.9600 . ?
C12 H12B 0.9600 . ?
C12 H12C 0.9600 . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C1 O1 1.16(2) . ?
C2 O2 1.14(2) . ?
C3 O3 1.098(18) . ?
C4 O4 1.16(2) . ?
C5 O5 1.17(2) . ?
P1 C113 1.774(12) . ?
P1 C119 1.776(10) . ?
P1 C101 1.780(12) . ?
P1 C107 1.794(11) . ?
C101 C102 1.3900 . ?
C101 C106 1.3900 . ?
C102 C103 1.3900 . ?
C102 H102 0.9300 . ?
C103 C104 1.3900 . ?
C103 H103 0.9300 . ?
C104 C105 1.3900 . ?
C104 H104 0.9300 . ?
C105 C106 1.3900 . ?
C105 H105 0.9300 . ?
C106 H106 0.9300 . ?
C107 C108 1.3900 . ?
C107 C112 1.3900 . ?
C108 C109 1.3900 . ?
C108 H108 0.9300 . ?
C109 C110 1.3900 . ?
C109 H109 0.9300 . ?
C110 C111 1.3900 . ?
C110 H110 0.9300 . ?
C111 C112 1.3900 . ?
C111 H111 0.9300 . ?
C112 H112 0.9300 . ?
C113 C114 1.3900 . ?
C113 C118 1.3900 . ?
C114 C115 1.3900 . ?
C114 H114 0.9300 . ?
C115 C116 1.3900 . ?
C115 H115 0.9300 . ?
C116 C117 1.3900 . ?
C116 H116 0.9300 . ?
C117 C118 1.3900 . ?
C117 H117 0.9300 . ?
C118 H118 0.9300 . ?
C119 C120 1.3900 . ?
C119 C124 1.3900 . ?
C120 C121 1.3900 . ?
C120 H120 0.9300 . ?
C121 C122 1.3900 . ?
C121 H121 0.9300 . ?
C122 C123 1.3900 . ?
C122 H122 0.9300 . ?
C123 C124 1.3900 . ?
C123 H123 0.9300 . ?
C124 H124 0.9300 . ?
P2 C201 1.768(10) . ?
P2 C219 1.778(15) . ?
P2 C207 1.799(14) . ?
P2 C213 1.804(12) . ?
C201 C202 1.3900 . ?
C201 C206 1.3900 . ?
C202 C203 1.3900 . ?
C202 H202 0.9300 . ?
C203 C204 1.3900 . ?
C203 H203 0.9300 . ?
C204 C205 1.3900 . ?
C204 H204 0.9300 . ?
C205 C206 1.3900 . ?
C205 H205 0.9300 . ?
C206 H206 0.9300 . ?
C207 C208 1.3900 . ?
C207 C212 1.3900 . ?
C208 C209 1.3900 . ?
C208 H208 0.9300 . ?
C209 C210 1.3900 . ?
C209 H209 0.9300 . ?
C210 C211 1.3900 . ?
C210 H210 0.9300 . ?
C211 C212 1.3900 . ?
C211 H211 0.9300 . ?
C212 H212 0.9300 . ?
C213 C214 1.3900 . ?
C213 C218 1.3900 . ?
C214 C215 1.3900 . ?
C214 H214 0.9300 . ?
C215 C216 1.3900 . ?
C215 H215 0.9300 . ?
C216 C217 1.3900 . ?
C216 H216 0.9300 . ?
C217 C218 1.3900 . ?
C217 H217 0.9300 . ?
C218 H218 0.9300 . ?
C219 C220 1.3900 . ?
C219 C224 1.3900 . ?
C220 C221 1.3900 . ?
C220 H220 0.9300 . ?
C221 C222 1.3900 . ?
C221 H221 0.9300 . ?
C222 C223 1.3900 . ?
C222 H222 0.9300 . ?
C223 C224 1.3900 . ?
C223 H223 0.9300 . ?
C224 H224 0.9300 . ?
P3 C307 1.771(13) . ?
P3 C301 1.785(11) . ?
P3 C313 1.786(11) . ?
P3 C319 1.796(10) . ?
C301 C302 1.3900 . ?
C301 C306 1.3900 . ?
C302 C303 1.3900 . ?
C302 H302 0.9300 . ?
C303 C304 1.3900 . ?
C303 H303 0.9300 . ?
C304 C305 1.3900 . ?
C304 H304 0.9300 . ?
C305 C306 1.3900 . ?
C305 H305 0.9300 . ?
C306 H306 0.9300 . ?
C307 C308 1.3900 . ?
C307 C312 1.3900 . ?
C308 C309 1.3900 . ?
C308 H308 0.9300 . ?
C309 C310 1.3900 . ?
C309 H309 0.9300 . ?
C310 C311 1.3900 . ?
C310 H310 0.9300 . ?
C311 C312 1.3900 . ?
C311 H311 0.9300 . ?
C312 H312 0.9300 . ?
C313 C314 1.3900 . ?
C313 C318 1.3900 . ?
C314 C315 1.3900 . ?
C314 H314 0.9300 . ?
C315 C316 1.3900 . ?
C315 H315 0.9300 . ?
C316 C317 1.3900 . ?
C316 H316 0.9300 . ?
C317 C318 1.3900 . ?
C317 H317 0.9300 . ?
C318 H318 0.9300 . ?
C319 C320 1.3900 . ?
C319 C324 1.3900 . ?
C320 C321 1.3900 . ?
C320 H320 0.9300 . ?
C321 C322 1.3900 . ?
C321 H321 0.9300 . ?
C322 C323 1.3900 . ?
C322 H322 0.9300 . ?
C323 C324 1.3900 . ?
C323 H323 0.9300 . ?
C324 H324 0.9300 . ?
C401 C402 1.468(13) . ?
C401 H40A 0.9600 . ?
C401 H40B 0.9600 . ?
C401 H40C 0.9600 . ?
C402 O402 1.186(12) . ?
C402 C403 1.481(13) . ?
C403 H40D 0.9600 . ?
C403 H40E 0.9600 . ?
C403 H40F 0.9600 . ?
C411 C412 1.473(13) . ?
C411 H41A 0.9600 . ?
C411 H41B 0.9600 . ?
C411 H41C 0.9600 . ?
C412 O412 1.181(13) . ?
C412 C413 1.473(13) . ?
C413 H41D 0.9600 . ?
C413 H41E 0.9600 . ?
C413 H41F 0.9600 . ?
C421 C422 1.475(13) . ?
C421 H42A 0.9600 . ?
C421 H42B 0.9600 . ?
C421 H42C 0.9600 . ?
C422 O422 1.178(13) . ?
C422 C423 1.472(13) . ?
C423 H42D 0.9600 . ?
C423 H42E 0.9600 . ?
C423 H42F 0.9600 . ?
C431 C432 1.469(13) . ?
C431 H43A 0.9600 . ?
C431 H43B 0.9600 . ?
C431 H43C 0.9600 . ?
C432 O432 1.183(13) . ?
C432 C433 1.475(13) . ?
C433 H43D 0.9600 . ?
C433 H43E 0.9600 . ?
C433 H43F 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 Sn1 107.6(5) . . ?
C1 Pt1 Sn3 98.8(7) . . ?
Sn1 Pt1 Sn3 114.83(4) . . ?
C1 Pt1 Sn5 105.3(7) . . ?
Sn1 Pt1 Sn5 113.40(4) . . ?
Sn3 Pt1 Sn5 115.02(4) . . ?
C1 Pt1 Pt2 150.6(7) . . ?
Sn1 Pt1 Pt2 62.35(3) . . ?
Sn3 Pt1 Pt2 110.52(4) . . ?
Sn5 Pt1 Pt2 60.65(3) . . ?
C1 Pt1 Pt3 143.6(7) . . ?
Sn1 Pt1 Pt3 62.81(3) . . ?
Sn3 Pt1 Pt3 60.94(3) . . ?
Sn5 Pt1 Pt3 110.71(4) . . ?
Pt2 Pt1 Pt3 59.73(2) . . ?
C1 Pt1 Pt4 140.5(5) . . ?
Sn1 Pt1 Pt4 111.71(4) . . ?
Sn3 Pt1 Pt4 61.21(3) . . ?
Sn5 Pt1 Pt4 62.06(3) . . ?
Pt2 Pt1 Pt4 59.26(2) . . ?
Pt3 Pt1 Pt4 59.11(2) . . ?
C2 Pt2 Sn5 95.6(5) . . ?
C2 Pt2 Pt4 149.7(5) . . ?
Sn5 Pt2 Pt4 61.28(3) . . ?
C2 Pt2 Sn1 96.9(6) . . ?
Sn5 Pt2 Sn1 103.95(4) . . ?
Pt4 Pt2 Sn1 107.14(3) . . ?
C2 Pt2 Pt1 124.7(6) . . ?
Sn5 Pt2 Pt1 56.57(3) . . ?
Pt4 Pt2 Pt1 60.84(2) . . ?
Sn1 Pt2 Pt1 55.27(3) . . ?
C2 Pt2 Pt3 150.4(5) . . ?
Sn5 Pt2 Pt3 108.00(4) . . ?
Pt4 Pt2 Pt3 59.90(2) . . ?
Sn1 Pt2 Pt3 60.74(3) . . ?
Pt1 Pt2 Pt3 60.55(2) . . ?
C2 Pt2 Sn2 97.7(5) . . ?
Sn5 Pt2 Sn2 166.65(4) . . ?
Pt4 Pt2 Sn2 106.37(4) . . ?
Sn1 Pt2 Sn2 73.83(4) . . ?
Pt1 Pt2 Sn2 114.16(4) . . ?
Pt3 Pt2 Sn2 59.18(3) . . ?
C2 Pt2 Pt5 124.8(6) . . ?
Sn5 Pt2 Pt5 116.10(3) . . ?
Pt4 Pt2 Pt5 60.21(2) . . ?
Sn1 Pt2 Pt5 115.57(4) . . ?
Pt1 Pt2 Pt5 110.48(3) . . ?
Pt3 Pt2 Pt5 59.99(2) . . ?
Sn2 Pt2 Pt5 55.75(3) . . ?
C2 Pt2 Sn6 98.7(6) . . ?
Sn5 Pt2 Sn6 73.78(4) . . ?
Pt4 Pt2 Sn6 57.89(3) . . ?
Sn1 Pt2 Sn6 164.38(4) . . ?
Pt1 Pt2 Sn6 113.84(3) . . ?
Pt3 Pt2 Sn6 104.78(3) . . ?
Sn2 Pt2 Sn6 104.70(4) . . ?
Pt5 Pt2 Sn6 54.86(3) . . ?
C3 Pt3 Sn3 96.1(4) . . ?
C3 Pt3 Sn2 97.6(5) . . ?
Sn3 Pt3 Sn2 166.23(4) . . ?
C3 Pt3 Pt4 149.7(5) . . ?
Sn3 Pt3 Pt4 60.06(3) . . ?
Sn2 Pt3 Pt4 107.21(3) . . ?
C3 Pt3 Pt2 150.5(5) . . ?
Sn3 Pt3 Pt2 106.35(3) . . ?
Sn2 Pt3 Pt2 60.43(3) . . ?
Pt4 Pt3 Pt2 59.72(2) . . ?
C3 Pt3 Pt5 126.0(5) . . ?
Sn3 Pt3 Pt5 115.25(4) . . ?
Sn2 Pt3 Pt5 56.23(3) . . ?
Pt4 Pt3 Pt5 60.26(2) . . ?
Pt2 Pt3 Pt5 60.33(2) . . ?
C3 Pt3 Sn4 97.8(5) . . ?
Sn3 Pt3 Sn4 74.25(4) . . ?
Sn2 Pt3 Sn4 104.65(4) . . ?
Pt4 Pt3 Sn4 59.64(3) . . ?
Pt2 Pt3 Sn4 106.34(3) . . ?
Pt5 Pt3 Sn4 55.51(3) . . ?
C3 Pt3 Pt1 123.9(5) . . ?
Sn3 Pt3 Pt1 55.91(3) . . ?
Sn2 Pt3 Pt1 114.54(3) . . ?
Pt4 Pt3 Pt1 60.50(2) . . ?
Pt2 Pt3 Pt1 59.73(2) . . ?
Pt5 Pt3 Pt1 110.08(3) . . ?
Sn4 Pt3 Pt1 115.17(4) . . ?
C3 Pt3 Sn1 97.2(5) . . ?
Sn3 Pt3 Sn1 103.53(4) . . ?
Sn2 Pt3 Sn1 73.87(4) . . ?
Pt4 Pt3 Sn1 106.13(3) . . ?
Pt2 Pt3 Sn1 59.61(3) . . ?
Pt5 Pt3 Sn1 114.86(3) . . ?
Sn4 Pt3 Sn1 165.02(4) . . ?
Pt1 Pt3 Sn1 54.69(3) . . ?
C4 Pt4 Sn6 94.9(5) . . ?
C4 Pt4 Sn3 97.1(5) . . ?
Sn6 Pt4 Sn3 168.04(4) . . ?
C4 Pt4 Pt2 148.7(5) . . ?
Sn6 Pt4 Pt2 62.65(3) . . ?
Sn3 Pt4 Pt2 106.51(3) . . ?
C4 Pt4 Pt3 150.8(5) . . ?
Sn6 Pt4 Pt3 108.83(4) . . ?
Sn3 Pt4 Pt3 59.60(3) . . ?
Pt2 Pt4 Pt3 60.38(2) . . ?
C4 Pt4 Sn4 98.1(5) . . ?
Sn6 Pt4 Sn4 103.11(4) . . ?
Sn3 Pt4 Sn4 74.55(4) . . ?
Pt2 Pt4 Sn4 107.74(4) . . ?
Pt3 Pt4 Sn4 60.77(3) . . ?
C4 Pt4 Pt5 126.7(5) . . ?
Sn6 Pt4 Pt5 56.38(3) . . ?
Sn3 Pt4 Pt5 114.83(4) . . ?
Pt2 Pt4 Pt5 60.55(2) . . ?
Pt3 Pt4 Pt5 60.26(2) . . ?
Sn4 Pt4 Pt5 55.85(3) . . ?
C4 Pt4 Sn5 95.9(5) . . ?
Sn6 Pt4 Sn5 74.75(4) . . ?
Sn3 Pt4 Sn5 104.59(4) . . ?
Pt2 Pt4 Sn5 58.71(3) . . ?
Pt3 Pt4 Sn5 106.37(3) . . ?
Sn4 Pt4 Sn5 165.96(4) . . ?
Pt5 Pt4 Sn5 114.08(4) . . ?
C4 Pt4 Pt1 123.3(5) . . ?
Sn6 Pt4 Pt1 117.30(3) . . ?
Sn3 Pt4 Pt1 55.74(3) . . ?
Pt2 Pt4 Pt1 59.91(2) . . ?
Pt3 Pt4 Pt1 60.39(2) . . ?
Sn4 Pt4 Pt1 116.09(3) . . ?
Pt5 Pt4 Pt1 109.99(3) . . ?
Sn5 Pt4 Pt1 55.51(3) . . ?
C5 Pt5 Sn6 100.1(7) . . ?
C5 Pt5 Sn4 106.4(6) . . ?
Sn6 Pt5 Sn4 111.26(5) . . ?
C5 Pt5 Sn2 104.6(6) . . ?
Sn6 Pt5 Sn2 117.64(4) . . ?
Sn4 Pt5 Sn2 114.77(5) . . ?
C5 Pt5 Pt3 148.3(7) . . ?
Sn6 Pt5 Pt3 111.59(4) . . ?
Sn4 Pt5 Pt3 62.45(3) . . ?
Sn2 Pt5 Pt3 61.06(3) . . ?
C5 Pt5 Pt4 144.7(6) . . ?
Sn6 Pt5 Pt4 60.40(3) . . ?
Sn4 Pt5 Pt4 61.67(3) . . ?
Sn2 Pt5 Pt4 110.56(4) . . ?
Pt3 Pt5 Pt4 59.48(2) . . ?
C5 Pt5 Pt2 141.9(6) . . ?
Sn6 Pt5 Pt2 63.55(3) . . ?
Sn4 Pt5 Pt2 111.52(4) . . ?
Sn2 Pt5 Pt2 61.80(3) . . ?
Pt3 Pt5 Pt2 59.68(2) . . ?
Pt4 Pt5 Pt2 59.24(2) . . ?
O11 Sn1 Cl2 93.2(3) . . ?
O11 Sn1 Cl1 93.3(3) . . ?
Cl2 Sn1 Cl1 92.37(19) . . ?
O11 Sn1 Pt1 139.4(3) . . ?
Cl2 Sn1 Pt1 114.72(13) . . ?
Cl1 Sn1 Pt1 113.10(15) . . ?
O11 Sn1 Pt2 84.0(3) . . ?
Cl2 Sn1 Pt2 102.53(13) . . ?
Cl1 Sn1 Pt2 164.97(15) . . ?
Pt1 Sn1 Pt2 62.39(3) . . ?
O11 Sn1 Pt3 81.6(3) . . ?
Cl2 Sn1 Pt3 161.75(13) . . ?
Cl1 Sn1 Pt3 105.35(15) . . ?
Pt1 Sn1 Pt3 62.51(3) . . ?
Pt2 Sn1 Pt3 59.65(3) . . ?
O11 Sn2 Cl3 91.3(4) . . ?
O11 Sn2 Cl4 92.4(3) . . ?
Cl3 Sn2 Cl4 93.8(2) . . ?
O11 Sn2 Pt5 141.1(3) . . ?
Cl3 Sn2 Pt5 113.69(18) . . ?
Cl4 Sn2 Pt5 113.86(15) . . ?
O11 Sn2 Pt3 83.9(3) . . ?
Cl3 Sn2 Pt3 161.19(16) . . ?
Cl4 Sn2 Pt3 104.58(15) . . ?
Pt5 Sn2 Pt3 62.71(3) . . ?
O11 Sn2 Pt2 84.6(3) . . ?
Cl3 Sn2 Pt2 101.12(15) . . ?
Cl4 Sn2 Pt2 164.88(16) . . ?
Pt5 Sn2 Pt2 62.46(3) . . ?
Pt3 Sn2 Pt2 60.39(3) . . ?
O12 Sn3 Cl6 93.8(4) . . ?
O12 Sn3 Cl5 94.4(3) . . ?
Cl6 Sn3 Cl5 93.0(2) . . ?
O12 Sn3 Pt1 140.8(3) . . ?
Cl6 Sn3 Pt1 111.17(19) . . ?
Cl5 Sn3 Pt1 113.04(15) . . ?
O12 Sn3 Pt3 84.1(3) . . ?
Cl6 Sn3 Pt3 163.14(15) . . ?
Cl5 Sn3 Pt3 103.79(16) . . ?
Pt1 Sn3 Pt3 63.15(3) . . ?
O12 Sn3 Pt4 82.7(3) . . ?
Cl6 Sn3 Pt4 102.80(15) . . ?
Cl5 Sn3 Pt4 164.04(16) . . ?
Pt1 Sn3 Pt4 63.05(3) . . ?
Pt3 Sn3 Pt4 60.34(3) . . ?
O12 Sn4 Cl7 94.1(4) . . ?
O12 Sn4 Cl8 92.5(3) . . ?
Cl7 Sn4 Cl8 92.3(2) . . ?
O12 Sn4 Pt5 138.8(3) . . ?
Cl7 Sn4 Pt5 113.99(18) . . ?
Cl8 Sn4 Pt5 114.60(15) . . ?
O12 Sn4 Pt4 82.3(3) . . ?
Cl7 Sn4 Pt4 164.56(18) . . ?
Cl8 Sn4 Pt4 102.85(15) . . ?
Pt5 Sn4 Pt4 62.48(3) . . ?
O12 Sn4 Pt3 82.5(3) . . ?
Cl7 Sn4 Pt3 105.11(17) . . ?
Cl8 Sn4 Pt3 162.17(15) . . ?
Pt5 Sn4 Pt3 62.04(3) . . ?
Pt4 Sn4 Pt3 59.59(3) . . ?
O13 Sn5 Cl10 95.2(3) . . ?
O13 Sn5 Cl9 90.4(3) . . ?
Cl10 Sn5 Cl9 93.40(19) . . ?
O13 Sn5 Pt1 139.7(3) . . ?
Cl10 Sn5 Pt1 108.32(15) . . ?
Cl9 Sn5 Pt1 119.32(12) . . ?
O13 Sn5 Pt2 85.3(3) . . ?
Cl10 Sn5 Pt2 162.79(15) . . ?
Cl9 Sn5 Pt2 103.81(13) . . ?
Pt1 Sn5 Pt2 62.78(3) . . ?
O13 Sn5 Pt4 81.0(3) . . ?
Cl10 Sn5 Pt4 103.01(14) . . ?
Cl9 Sn5 Pt4 162.04(14) . . ?
Pt1 Sn5 Pt4 62.43(3) . . ?
Pt2 Sn5 Pt4 60.01(3) . . ?
O13 Sn6 Cl12 94.1(3) . . ?
O13 Sn6 Cl11 93.7(3) . . ?
Cl12 Sn6 Cl11 91.39(19) . . ?
O13 Sn6 Pt5 139.8(3) . . ?
Cl12 Sn6 Pt5 113.67(14) . . ?
Cl11 Sn6 Pt5 113.08(15) . . ?
O13 Sn6 Pt4 83.6(3) . . ?
Cl12 Sn6 Pt4 102.14(14) . . ?
Cl11 Sn6 Pt4 166.34(14) . . ?
Pt5 Sn6 Pt4 63.22(3) . . ?
O13 Sn6 Pt2 82.7(3) . . ?
Cl12 Sn6 Pt2 161.52(14) . . ?
Cl11 Sn6 Pt2 106.95(14) . . ?
Pt5 Sn6 Pt2 61.59(3) . . ?
Pt4 Sn6 Pt2 59.46(3) . . ?
C11 O11 Sn2 128.5(11) . . ?
C11 O11 Sn1 124.4(11) . . ?
Sn2 O11 Sn1 107.1(5) . . ?
C12 O12 Sn3 126.7(13) . . ?
C12 O12 Sn4 125.2(12) . . ?
Sn3 O12 Sn4 107.8(5) . . ?
C13 O13 Sn6 125.0(10) . . ?
C13 O13 Sn5 126.9(10) . . ?
Sn6 O13 Sn5 107.6(4) . . ?
O11 C11 H11A 109.5 . . ?
O11 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
O11 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
O12 C12 H12A 109.5 . . ?
O12 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
O12 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
O13 C13 H13A 109.5 . . ?
O13 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
O13 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
O1 C1 Pt1 179(2) . . ?
O2 C2 Pt2 179.3(19) . . ?
O3 C3 Pt3 177.3(15) . . ?
O4 C4 Pt4 176.7(17) . . ?
O5 C5 Pt5 177.3(19) . . ?
C113 P1 C119 111.2(7) . . ?
C113 P1 C101 111.0(7) . . ?
C119 P1 C101 107.6(6) . . ?
C113 P1 C107 103.2(7) . . ?
C119 P1 C107 110.8(7) . . ?
C101 P1 C107 113.1(6) . . ?
C102 C101 C106 120.0 . . ?
C102 C101 P1 118.4(8) . . ?
C106 C101 P1 121.2(8) . . ?
C103 C102 C101 120.0 . . ?
C103 C102 H102 120.0 . . ?
C101 C102 H102 120.0 . . ?
C102 C103 C104 120.0 . . ?
C102 C103 H103 120.0 . . ?
C104 C103 H103 120.0 . . ?
C103 C104 C105 120.0 . . ?
C103 C104 H104 120.0 . . ?
C105 C104 H104 120.0 . . ?
C104 C105 C106 120.0 . . ?
C104 C105 H105 120.0 . . ?
C106 C105 H105 120.0 . . ?
C105 C106 C101 120.0 . . ?
C105 C106 H106 120.0 . . ?
C101 C106 H106 120.0 . . ?
C108 C107 C112 120.0 . . ?
C108 C107 P1 119.0(9) . . ?
C112 C107 P1 120.9(9) . . ?
C109 C108 C107 120.0 . . ?
C109 C108 H108 120.0 . . ?
C107 C108 H108 120.0 . . ?
C110 C109 C108 120.0 . . ?
C110 C109 H109 120.0 . . ?
C108 C109 H109 120.0 . . ?
C109 C110 C111 120.0 . . ?
C109 C110 H110 120.0 . . ?
C111 C110 H110 120.0 . . ?
C112 C111 C110 120.0 . . ?
C112 C111 H111 120.0 . . ?
C110 C111 H111 120.0 . . ?
C111 C112 C107 120.0 . . ?
C111 C112 H112 120.0 . . ?
C107 C112 H112 120.0 . . ?
C114 C113 C118 120.0 . . ?
C114 C113 P1 119.4(9) . . ?
C118 C113 P1 120.6(9) . . ?
C115 C114 C113 120.0 . . ?
C115 C114 H114 120.0 . . ?
C113 C114 H114 120.0 . . ?
C114 C115 C116 120.0 . . ?
C114 C115 H115 120.0 . . ?
C116 C115 H115 120.0 . . ?
C117 C116 C115 120.0 . . ?
C117 C116 H116 120.0 . . ?
C115 C116 H116 120.0 . . ?
C118 C117 C116 120.0 . . ?
C118 C117 H117 120.0 . . ?
C116 C117 H117 120.0 . . ?
C117 C118 C113 120.0 . . ?
C117 C118 H118 120.0 . . ?
C113 C118 H118 120.0 . . ?
C120 C119 C124 120.0 . . ?
C120 C119 P1 121.8(8) . . ?
C124 C119 P1 118.2(8) . . ?
C119 C120 C121 120.0 . . ?
C119 C120 H120 120.0 . . ?
C121 C120 H120 120.0 . . ?
C122 C121 C120 120.0 . . ?
C122 C121 H121 120.0 . . ?
C120 C121 H121 120.0 . . ?
C121 C122 C123 120.0 . . ?
C121 C122 H122 120.0 . . ?
C123 C122 H122 120.0 . . ?
C124 C123 C122 120.0 . . ?
C124 C123 H123 120.0 . . ?
C122 C123 H123 120.0 . . ?
C123 C124 C119 120.0 . . ?
C123 C124 H124 120.0 . . ?
C119 C124 H124 120.0 . . ?
C201 P2 C219 111.6(9) . . ?
C201 P2 C207 109.7(7) . . ?
C219 P2 C207 112.2(8) . . ?
C201 P2 C213 106.6(7) . . ?
C219 P2 C213 108.3(8) . . ?
C207 P2 C213 108.1(8) . . ?
C202 C201 C206 120.0 . . ?
C202 C201 P2 119.2(8) . . ?
C206 C201 P2 120.3(8) . . ?
C203 C202 C201 120.0 . . ?
C203 C202 H202 120.0 . . ?
C201 C202 H202 120.0 . . ?
C202 C203 C204 120.0 . . ?
C202 C203 H203 120.0 . . ?
C204 C203 H203 120.0 . . ?
C205 C204 C203 120.0 . . ?
C205 C204 H204 120.0 . . ?
C203 C204 H204 120.0 . . ?
C204 C205 C206 120.0 . . ?
C204 C205 H205 120.0 . . ?
C206 C205 H205 120.0 . . ?
C205 C206 C201 120.0 . . ?
C205 C206 H206 120.0 . . ?
C201 C206 H206 120.0 . . ?
C208 C207 C212 120.0 . . ?
C208 C207 P2 119.9(11) . . ?
C212 C207 P2 120.0(11) . . ?
C209 C208 C207 120.0 . . ?
C209 C208 H208 120.0 . . ?
C207 C208 H208 120.0 . . ?
C208 C209 C210 120.0 . . ?
C208 C209 H209 120.0 . . ?
C210 C209 H209 120.0 . . ?
C211 C210 C209 120.0 . . ?
C211 C210 H210 120.0 . . ?
C209 C210 H210 120.0 . . ?
C212 C211 C210 120.0 . . ?
C212 C211 H211 120.0 . . ?
C210 C211 H211 120.0 . . ?
C211 C212 C207 120.0 . . ?
C211 C212 H212 120.0 . . ?
C207 C212 H212 120.0 . . ?
C214 C213 C218 120.0 . . ?
C214 C213 P2 115.4(9) . . ?
C218 C213 P2 124.6(9) . . ?
C213 C214 C215 120.0 . . ?
C213 C214 H214 120.0 . . ?
C215 C214 H214 120.0 . . ?
C216 C215 C214 120.0 . . ?
C216 C215 H215 120.0 . . ?
C214 C215 H215 120.0 . . ?
C215 C216 C217 120.0 . . ?
C215 C216 H216 120.0 . . ?
C217 C216 H216 120.0 . . ?
C218 C217 C216 120.0 . . ?
C218 C217 H217 120.0 . . ?
C216 C217 H217 120.0 . . ?
C217 C218 C213 120.0 . . ?
C217 C218 H218 120.0 . . ?
C213 C218 H218 120.0 . . ?
C220 C219 C224 120.0 . . ?
C220 C219 P2 122.8(12) . . ?
C224 C219 P2 117.0(12) . . ?
C221 C220 C219 120.0 . . ?
C221 C220 H220 120.0 . . ?
C219 C220 H220 120.0 . . ?
C222 C221 C220 120.0 . . ?
C222 C221 H221 120.0 . . ?
C220 C221 H221 120.0 . . ?
C221 C222 C223 120.0 . . ?
C221 C222 H222 120.0 . . ?
C223 C222 H222 120.0 . . ?
C224 C223 C222 120.0 . . ?
C224 C223 H223 120.0 . . ?
C222 C223 H223 120.0 . . ?
C223 C224 C219 120.0 . . ?
C223 C224 H224 120.0 . . ?
C219 C224 H224 120.0 . . ?
C307 P3 C301 104.9(7) . . ?
C307 P3 C313 112.0(8) . . ?
C301 P3 C313 110.0(7) . . ?
C307 P3 C319 111.4(7) . . ?
C301 P3 C319 111.7(6) . . ?
C313 P3 C319 106.9(7) . . ?
C302 C301 C306 120.0 . . ?
C302 C301 P3 118.9(9) . . ?
C306 C301 P3 120.8(9) . . ?
C303 C302 C301 120.0 . . ?
C303 C302 H302 120.0 . . ?
C301 C302 H302 120.0 . . ?
C302 C303 C304 120.0 . . ?
C302 C303 H303 120.0 . . ?
C304 C303 H303 120.0 . . ?
C305 C304 C303 120.0 . . ?
C305 C304 H304 120.0 . . ?
C303 C304 H304 120.0 . . ?
C304 C305 C306 120.0 . . ?
C304 C305 H305 120.0 . . ?
C306 C305 H305 120.0 . . ?
C305 C306 C301 120.0 . . ?
C305 C306 H306 120.0 . . ?
C301 C306 H306 120.0 . . ?
C308 C307 C312 120.0 . . ?
C308 C307 P3 120.9(9) . . ?
C312 C307 P3 119.1(9) . . ?
C309 C308 C307 120.0 . . ?
C309 C308 H308 120.0 . . ?
C307 C308 H308 120.0 . . ?
C308 C309 C310 120.0 . . ?
C308 C309 H309 120.0 . . ?
C310 C309 H309 120.0 . . ?
C311 C310 C309 120.0 . . ?
C311 C310 H310 120.0 . . ?
C309 C310 H310 120.0 . . ?
C312 C311 C310 120.0 . . ?
C312 C311 H311 120.0 . . ?
C310 C311 H311 120.0 . . ?
C311 C312 C307 120.0 . . ?
C311 C312 H312 120.0 . . ?
C307 C312 H312 120.0 . . ?
C314 C313 C318 120.0 . . ?
C314 C313 P3 120.9(10) . . ?
C318 C313 P3 119.0(10) . . ?
C315 C314 C313 120.0 . . ?
C315 C314 H314 120.0 . . ?
C313 C314 H314 120.0 . . ?
C314 C315 C316 120.0 . . ?
C314 C315 H315 120.0 . . ?
C316 C315 H315 120.0 . . ?
C315 C316 C317 120.0 . . ?
C315 C316 H316 120.0 . . ?
C317 C316 H316 120.0 . . ?
C318 C317 C316 120.0 . . ?
C318 C317 H317 120.0 . . ?
C316 C317 H317 120.0 . . ?
C317 C318 C313 120.0 . . ?
C317 C318 H318 120.0 . . ?
C313 C318 H318 120.0 . . ?
C320 C319 C324 120.0 . . ?
C320 C319 P3 118.5(7) . . ?
C324 C319 P3 121.5(7) . . ?
C319 C320 C321 120.0 . . ?
C319 C320 H320 120.0 . . ?
C321 C320 H320 120.0 . . ?
C322 C321 C320 120.0 . . ?
C322 C321 H321 120.0 . . ?
C320 C321 H321 120.0 . . ?
C321 C322 C323 120.0 . . ?
C321 C322 H322 120.0 . . ?
C323 C322 H322 120.0 . . ?
C324 C323 C322 120.0 . . ?
C324 C323 H323 120.0 . . ?
C322 C323 H323 120.0 . . ?
C323 C324 C319 120.0 . . ?
C323 C324 H324 120.0 . . ?
C319 C324 H324 120.0 . . ?
C402 C401 H40A 109.5 . . ?
C402 C401 H40B 109.5 . . ?
H40A C401 H40B 109.5 . . ?
C402 C401 H40C 109.5 . . ?
H40A C401 H40C 109.5 . . ?
H40B C401 H40C 109.5 . . ?
O402 C402 C401 122(2) . . ?
O402 C402 C403 118.0(19) . . ?
C401 C402 C403 120.0(14) . . ?
C402 C403 H40D 109.5 . . ?
C402 C403 H40E 109.5 . . ?
H40D C403 H40E 109.5 . . ?
C402 C403 H40F 109.5 . . ?
H40D C403 H40F 109.5 . . ?
H40E C403 H40F 109.5 . . ?
C412 C411 H41A 109.5 . . ?
C412 C411 H41B 109.5 . . ?
H41A C411 H41B 109.5 . . ?
C412 C411 H41C 109.5 . . ?
H41A C411 H41C 109.5 . . ?
H41B C411 H41C 109.5 . . ?
O412 C412 C411 119(2) . . ?
O412 C412 C413 120(2) . . ?
C411 C412 C413 120.7(16) . . ?
C412 C413 H41D 109.5 . . ?
C412 C413 H41E 109.5 . . ?
H41D C413 H41E 109.5 . . ?
C412 C413 H41F 109.5 . . ?
H41D C413 H41F 109.5 . . ?
H41E C413 H41F 109.5 . . ?
C422 C421 H42A 109.5 . . ?
C422 C421 H42B 109.5 . . ?
H42A C421 H42B 109.5 . . ?
C422 C421 H42C 109.5 . . ?
H42A C421 H42C 109.5 . . ?
H42B C421 H42C 109.5 . . ?
O422 C422 C423 118(3) . . ?
O422 C422 C421 120(3) . . ?
C423 C422 C421 122.8(17) . . ?
C422 C423 H42D 109.5 . . ?
C422 C423 H42E 109.5 . . ?
H42D C423 H42E 109.5 . . ?
C422 C423 H42F 109.5 . . ?
H42D C423 H42F 109.5 . . ?
H42E C423 H42F 109.5 . . ?
C432 C431 H43A 109.5 . . ?
C432 C431 H43B 109.5 . . ?
H43A C431 H43B 109.5 . . ?
C432 C431 H43C 109.5 . . ?
H43A C431 H43C 109.5 . . ?
H43B C431 H43C 109.5 . . ?
O432 C432 C431 118(2) . . ?
O432 C432 C433 119(2) . . ?
C431 C432 C433 123.7(16) . . ?
C432 C433 H43D 109.5 . . ?
C432 C433 H43E 109.5 . . ?
H43D C433 H43E 109.5 . . ?
C432 C433 H43F 109.5 . . ?
H43D C433 H43F 109.5 . . ?
H43E C433 H43F 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 Pt2 C2 -4.1(13) . . . . ?
Sn1 Pt1 Pt2 C2 72.3(6) . . . . ?
Sn3 Pt1 Pt2 C2 -179.6(6) . . . . ?
Sn5 Pt1 Pt2 C2 -71.7(6) . . . . ?
Pt3 Pt1 Pt2 C2 145.4(6) . . . . ?
Pt4 Pt1 Pt2 C2 -144.8(6) . . . . ?
C1 Pt1 Pt2 Sn5 67.5(11) . . . . ?
Sn1 Pt1 Pt2 Sn5 144.01(5) . . . . ?
Sn3 Pt1 Pt2 Sn5 -107.92(5) . . . . ?
Pt3 Pt1 Pt2 Sn5 -142.94(4) . . . . ?
Pt4 Pt1 Pt2 Sn5 -73.09(3) . . . . ?
C1 Pt1 Pt2 Pt4 140.6(11) . . . . ?
Sn1 Pt1 Pt2 Pt4 -142.90(4) . . . . ?
Sn3 Pt1 Pt2 Pt4 -34.83(4) . . . . ?
Sn5 Pt1 Pt2 Pt4 73.09(3) . . . . ?
Pt3 Pt1 Pt2 Pt4 -69.85(2) . . . . ?
C1 Pt1 Pt2 Sn1 -76.5(11) . . . . ?
Sn3 Pt1 Pt2 Sn1 108.07(5) . . . . ?
Sn5 Pt1 Pt2 Sn1 -144.01(5) . . . . ?
Pt3 Pt1 Pt2 Sn1 73.05(4) . . . . ?
Pt4 Pt1 Pt2 Sn1 142.90(4) . . . . ?
C1 Pt1 Pt2 Pt3 -149.5(11) . . . . ?
Sn1 Pt1 Pt2 Pt3 -73.05(4) . . . . ?
Sn3 Pt1 Pt2 Pt3 35.02(4) . . . . ?
Sn5 Pt1 Pt2 Pt3 142.94(4) . . . . ?
Pt4 Pt1 Pt2 Pt3 69.85(2) . . . . ?
C1 Pt1 Pt2 Sn2 -123.4(11) . . . . ?
Sn1 Pt1 Pt2 Sn2 -46.97(4) . . . . ?
Sn3 Pt1 Pt2 Sn2 61.10(5) . . . . ?
Sn5 Pt1 Pt2 Sn2 169.02(5) . . . . ?
Pt3 Pt1 Pt2 Sn2 26.08(4) . . . . ?
Pt4 Pt1 Pt2 Sn2 95.94(4) . . . . ?
C1 Pt1 Pt2 Pt5 176.0(11) . . . . ?
Sn1 Pt1 Pt2 Pt5 -107.56(4) . . . . ?
Sn3 Pt1 Pt2 Pt5 0.51(4) . . . . ?
Sn5 Pt1 Pt2 Pt5 108.43(4) . . . . ?
Pt3 Pt1 Pt2 Pt5 -34.51(3) . . . . ?
Pt4 Pt1 Pt2 Pt5 35.34(3) . . . . ?
C1 Pt1 Pt2 Sn6 116.4(11) . . . . ?
Sn1 Pt1 Pt2 Sn6 -167.11(5) . . . . ?
Sn3 Pt1 Pt2 Sn6 -59.04(5) . . . . ?
Sn5 Pt1 Pt2 Sn6 48.88(4) . . . . ?
Pt3 Pt1 Pt2 Sn6 -94.06(4) . . . . ?
Pt4 Pt1 Pt2 Sn6 -24.21(3) . . . . ?
C2 Pt2 Pt3 C3 -3.1(16) . . . . ?
Sn5 Pt2 Pt3 C3 138.1(10) . . . . ?
Pt4 Pt2 Pt3 C3 177.6(10) . . . . ?
Sn1 Pt2 Pt3 C3 41.9(10) . . . . ?
Pt1 Pt2 Pt3 C3 106.2(10) . . . . ?
Sn2 Pt2 Pt3 C3 -46.0(10) . . . . ?
Pt5 Pt2 Pt3 C3 -111.6(10) . . . . ?
Sn6 Pt2 Pt3 C3 -144.5(10) . . . . ?
C2 Pt2 Pt3 Sn3 -141.3(12) . . . . ?
Sn5 Pt2 Pt3 Sn3 -0.12(5) . . . . ?
Pt4 Pt2 Pt3 Sn3 39.32(3) . . . . ?
Sn1 Pt2 Pt3 Sn3 -96.35(4) . . . . ?
Pt1 Pt2 Pt3 Sn3 -32.05(3) . . . . ?
Sn2 Pt2 Pt3 Sn3 175.80(5) . . . . ?
Pt5 Pt2 Pt3 Sn3 110.15(4) . . . . ?
Sn6 Pt2 Pt3 Sn3 77.28(4) . . . . ?
C2 Pt2 Pt3 Sn2 42.9(12) . . . . ?
Sn5 Pt2 Pt3 Sn2 -175.92(5) . . . . ?
Pt4 Pt2 Pt3 Sn2 -136.48(4) . . . . ?
Sn1 Pt2 Pt3 Sn2 87.85(4) . . . . ?
Pt1 Pt2 Pt3 Sn2 152.15(4) . . . . ?
Pt5 Pt2 Pt3 Sn2 -65.65(4) . . . . ?
Sn6 Pt2 Pt3 Sn2 -98.52(4) . . . . ?
C2 Pt2 Pt3 Pt4 179.4(12) . . . . ?
Sn5 Pt2 Pt3 Pt4 -39.44(3) . . . . ?
Sn1 Pt2 Pt3 Pt4 -135.67(4) . . . . ?
Pt1 Pt2 Pt3 Pt4 -71.37(3) . . . . ?
Sn2 Pt2 Pt3 Pt4 136.48(4) . . . . ?
Pt5 Pt2 Pt3 Pt4 70.83(3) . . . . ?
Sn6 Pt2 Pt3 Pt4 37.96(3) . . . . ?
C2 Pt2 Pt3 Pt5 108.5(12) . . . . ?
Sn5 Pt2 Pt3 Pt5 -110.27(4) . . . . ?
Pt4 Pt2 Pt3 Pt5 -70.83(3) . . . . ?
Sn1 Pt2 Pt3 Pt5 153.50(4) . . . . ?
Pt1 Pt2 Pt3 Pt5 -142.20(3) . . . . ?
Sn2 Pt2 Pt3 Pt5 65.65(4) . . . . ?
Sn6 Pt2 Pt3 Pt5 -32.87(3) . . . . ?
C2 Pt2 Pt3 Sn4 140.7(12) . . . . ?
Sn5 Pt2 Pt3 Sn4 -78.07(4) . . . . ?
Pt4 Pt2 Pt3 Sn4 -38.63(3) . . . . ?
Sn1 Pt2 Pt3 Sn4 -174.30(4) . . . . ?
Pt1 Pt2 Pt3 Sn4 -110.00(4) . . . . ?
Sn2 Pt2 Pt3 Sn4 97.85(4) . . . . ?
Pt5 Pt2 Pt3 Sn4 32.20(4) . . . . ?
Sn6 Pt2 Pt3 Sn4 -0.67(5) . . . . ?
C2 Pt2 Pt3 Pt1 -109.3(12) . . . . ?
Sn5 Pt2 Pt3 Pt1 31.93(3) . . . . ?
Pt4 Pt2 Pt3 Pt1 71.37(3) . . . . ?
Sn1 Pt2 Pt3 Pt1 -64.30(3) . . . . ?
Sn2 Pt2 Pt3 Pt1 -152.15(4) . . . . ?
Pt5 Pt2 Pt3 Pt1 142.20(3) . . . . ?
Sn6 Pt2 Pt3 Pt1 109.33(4) . . . . ?
C2 Pt2 Pt3 Sn1 -45.0(12) . . . . ?
Sn5 Pt2 Pt3 Sn1 96.23(4) . . . . ?
Pt4 Pt2 Pt3 Sn1 135.67(4) . . . . ?
Pt1 Pt2 Pt3 Sn1 64.30(3) . . . . ?
Sn2 Pt2 Pt3 Sn1 -87.85(4) . . . . ?
Pt5 Pt2 Pt3 Sn1 -153.50(4) . . . . ?
Sn6 Pt2 Pt3 Sn1 173.63(4) . . . . ?
C1 Pt1 Pt3 C3 9.8(11) . . . . ?
Sn1 Pt1 Pt3 C3 -73.0(6) . . . . ?
Sn3 Pt1 Pt3 C3 72.6(6) . . . . ?
Sn5 Pt1 Pt3 C3 -179.5(6) . . . . ?
Pt2 Pt1 Pt3 C3 -145.3(6) . . . . ?
Pt4 Pt1 Pt3 C3 144.6(6) . . . . ?
C1 Pt1 Pt3 Sn3 -62.8(10) . . . . ?
Sn1 Pt1 Pt3 Sn3 -145.66(4) . . . . ?
Sn5 Pt1 Pt3 Sn3 107.89(5) . . . . ?
Pt2 Pt1 Pt3 Sn3 142.06(4) . . . . ?
Pt4 Pt1 Pt3 Sn3 71.97(3) . . . . ?
C1 Pt1 Pt3 Sn2 128.6(10) . . . . ?
Sn1 Pt1 Pt3 Sn2 45.76(4) . . . . ?
Sn3 Pt1 Pt3 Sn2 -168.59(5) . . . . ?
Sn5 Pt1 Pt3 Sn2 -60.69(5) . . . . ?
Pt2 Pt1 Pt3 Sn2 -26.53(4) . . . . ?
Pt4 Pt1 Pt3 Sn2 -96.62(4) . . . . ?
C1 Pt1 Pt3 Pt4 -134.8(10) . . . . ?
Sn1 Pt1 Pt3 Pt4 142.37(4) . . . . ?
Sn3 Pt1 Pt3 Pt4 -71.97(3) . . . . ?
Sn5 Pt1 Pt3 Pt4 35.93(4) . . . . ?
Pt2 Pt1 Pt3 Pt4 70.09(2) . . . . ?
C1 Pt1 Pt3 Pt2 155.1(10) . . . . ?
Sn1 Pt1 Pt3 Pt2 72.29(3) . . . . ?
Sn3 Pt1 Pt3 Pt2 -142.06(4) . . . . ?
Sn5 Pt1 Pt3 Pt2 -34.16(4) . . . . ?
Pt4 Pt1 Pt3 Pt2 -70.09(2) . . . . ?
C1 Pt1 Pt3 Pt5 -170.3(10) . . . . ?
Sn1 Pt1 Pt3 Pt5 106.83(4) . . . . ?
Sn3 Pt1 Pt3 Pt5 -107.51(4) . . . . ?
Sn5 Pt1 Pt3 Pt5 0.38(5) . . . . ?
Pt2 Pt1 Pt3 Pt5 34.54(3) . . . . ?
Pt4 Pt1 Pt3 Pt5 -35.55(3) . . . . ?
C1 Pt1 Pt3 Sn4 -109.9(10) . . . . ?
Sn1 Pt1 Pt3 Sn4 167.20(5) . . . . ?
Sn3 Pt1 Pt3 Sn4 -47.14(4) . . . . ?
Sn5 Pt1 Pt3 Sn4 60.75(5) . . . . ?
Pt2 Pt1 Pt3 Sn4 94.92(4) . . . . ?
Pt4 Pt1 Pt3 Sn4 24.83(4) . . . . ?
C1 Pt1 Pt3 Sn1 82.9(10) . . . . ?
Sn3 Pt1 Pt3 Sn1 145.66(4) . . . . ?
Sn5 Pt1 Pt3 Sn1 -106.45(5) . . . . ?
Pt2 Pt1 Pt3 Sn1 -72.29(3) . . . . ?
Pt4 Pt1 Pt3 Sn1 -142.37(4) . . . . ?
C2 Pt2 Pt4 C4 4.2(15) . . . . ?
Sn5 Pt2 Pt4 C4 -39.9(10) . . . . ?
Sn1 Pt2 Pt4 C4 -136.7(10) . . . . ?
Pt1 Pt2 Pt4 C4 -105.5(10) . . . . ?
Pt3 Pt2 Pt4 C4 -176.4(10) . . . . ?
Sn2 Pt2 Pt4 C4 145.6(10) . . . . ?
Pt5 Pt2 Pt4 C4 113.2(10) . . . . ?
Sn6 Pt2 Pt4 C4 48.2(10) . . . . ?
C2 Pt2 Pt4 Sn6 -44.0(12) . . . . ?
Sn5 Pt2 Pt4 Sn6 -88.15(4) . . . . ?
Sn1 Pt2 Pt4 Sn6 175.04(4) . . . . ?
Pt1 Pt2 Pt4 Sn6 -153.72(4) . . . . ?
Pt3 Pt2 Pt4 Sn6 135.40(4) . . . . ?
Sn2 Pt2 Pt4 Sn6 97.35(5) . . . . ?
Pt5 Pt2 Pt4 Sn6 64.92(3) . . . . ?
C2 Pt2 Pt4 Sn3 141.5(12) . . . . ?
Sn5 Pt2 Pt4 Sn3 97.31(5) . . . . ?
Sn1 Pt2 Pt4 Sn3 0.50(5) . . . . ?
Pt1 Pt2 Pt4 Sn3 31.75(3) . . . . ?
Pt3 Pt2 Pt4 Sn3 -39.14(3) . . . . ?
Sn2 Pt2 Pt4 Sn3 -77.19(5) . . . . ?
Pt5 Pt2 Pt4 Sn3 -109.61(4) . . . . ?
Sn6 Pt2 Pt4 Sn3 -174.54(5) . . . . ?
C2 Pt2 Pt4 Pt3 -179.4(12) . . . . ?
Sn5 Pt2 Pt4 Pt3 136.45(4) . . . . ?
Sn1 Pt2 Pt4 Pt3 39.64(3) . . . . ?
Pt1 Pt2 Pt4 Pt3 70.89(2) . . . . ?
Sn2 Pt2 Pt4 Pt3 -38.05(3) . . . . ?
Pt5 Pt2 Pt4 Pt3 -70.47(3) . . . . ?
Sn6 Pt2 Pt4 Pt3 -135.40(4) . . . . ?
C2 Pt2 Pt4 Sn4 -139.9(12) . . . . ?
Sn5 Pt2 Pt4 Sn4 175.95(4) . . . . ?
Sn1 Pt2 Pt4 Sn4 79.14(4) . . . . ?
Pt1 Pt2 Pt4 Sn4 110.39(4) . . . . ?
Pt3 Pt2 Pt4 Sn4 39.50(3) . . . . ?
Sn2 Pt2 Pt4 Sn4 1.45(5) . . . . ?
Pt5 Pt2 Pt4 Sn4 -30.97(3) . . . . ?
Sn6 Pt2 Pt4 Sn4 -95.89(4) . . . . ?
C2 Pt2 Pt4 Pt5 -108.9(12) . . . . ?
Sn5 Pt2 Pt4 Pt5 -153.08(4) . . . . ?
Sn1 Pt2 Pt4 Pt5 110.11(4) . . . . ?
Pt1 Pt2 Pt4 Pt5 141.36(3) . . . . ?
Pt3 Pt2 Pt4 Pt5 70.47(3) . . . . ?
Sn2 Pt2 Pt4 Pt5 32.42(3) . . . . ?
Sn6 Pt2 Pt4 Pt5 -64.92(3) . . . . ?
C2 Pt2 Pt4 Sn5 44.2(12) . . . . ?
Sn1 Pt2 Pt4 Sn5 -96.81(4) . . . . ?
Pt1 Pt2 Pt4 Sn5 -65.57(3) . . . . ?
Pt3 Pt2 Pt4 Sn5 -136.45(4) . . . . ?
Sn2 Pt2 Pt4 Sn5 -174.50(4) . . . . ?
Pt5 Pt2 Pt4 Sn5 153.08(4) . . . . ?
Sn6 Pt2 Pt4 Sn5 88.15(4) . . . . ?
C2 Pt2 Pt4 Pt1 109.7(12) . . . . ?
Sn5 Pt2 Pt4 Pt1 65.57(3) . . . . ?
Sn1 Pt2 Pt4 Pt1 -31.25(3) . . . . ?
Pt3 Pt2 Pt4 Pt1 -70.89(2) . . . . ?
Sn2 Pt2 Pt4 Pt1 -108.94(4) . . . . ?
Pt5 Pt2 Pt4 Pt1 -141.36(3) . . . . ?
Sn6 Pt2 Pt4 Pt1 153.72(4) . . . . ?
C3 Pt3 Pt4 C4 -1.5(15) . . . . ?
Sn3 Pt3 Pt4 C4 40.7(11) . . . . ?
Sn2 Pt3 Pt4 C4 -145.0(11) . . . . ?
Pt2 Pt3 Pt4 C4 176.1(11) . . . . ?
Pt5 Pt3 Pt4 C4 -112.9(11) . . . . ?
Sn4 Pt3 Pt4 C4 -47.8(11) . . . . ?
Pt1 Pt3 Pt4 C4 106.0(11) . . . . ?
Sn1 Pt3 Pt4 C4 137.3(11) . . . . ?
C3 Pt3 Pt4 Sn6 141.2(10) . . . . ?
Sn3 Pt3 Pt4 Sn6 -176.66(5) . . . . ?
Sn2 Pt3 Pt4 Sn6 -2.40(5) . . . . ?
Pt2 Pt3 Pt4 Sn6 -41.22(4) . . . . ?
Pt5 Pt3 Pt4 Sn6 29.71(4) . . . . ?
Sn4 Pt3 Pt4 Sn6 94.81(4) . . . . ?
Pt1 Pt3 Pt4 Sn6 -111.33(4) . . . . ?
Sn1 Pt3 Pt4 Sn6 -80.09(4) . . . . ?
C3 Pt3 Pt4 Sn3 -42.2(10) . . . . ?
Sn2 Pt3 Pt4 Sn3 174.26(5) . . . . ?
Pt2 Pt3 Pt4 Sn3 135.44(4) . . . . ?
Pt5 Pt3 Pt4 Sn3 -153.63(4) . . . . ?
Sn4 Pt3 Pt4 Sn3 -88.53(4) . . . . ?
Pt1 Pt3 Pt4 Sn3 65.33(3) . . . . ?
Sn1 Pt3 Pt4 Sn3 96.57(4) . . . . ?
C3 Pt3 Pt4 Pt2 -177.6(10) . . . . ?
Sn3 Pt3 Pt4 Pt2 -135.44(4) . . . . ?
Sn2 Pt3 Pt4 Pt2 38.83(3) . . . . ?
Pt5 Pt3 Pt4 Pt2 70.93(3) . . . . ?
Sn4 Pt3 Pt4 Pt2 136.03(4) . . . . ?
Pt1 Pt3 Pt4 Pt2 -70.10(3) . . . . ?
Sn1 Pt3 Pt4 Pt2 -38.87(3) . . . . ?
C3 Pt3 Pt4 Sn4 46.3(10) . . . . ?
Sn3 Pt3 Pt4 Sn4 88.53(4) . . . . ?
Sn2 Pt3 Pt4 Sn4 -97.20(4) . . . . ?
Pt2 Pt3 Pt4 Sn4 -136.03(4) . . . . ?
Pt5 Pt3 Pt4 Sn4 -65.10(4) . . . . ?
Pt1 Pt3 Pt4 Sn4 153.87(4) . . . . ?
Sn1 Pt3 Pt4 Sn4 -174.90(5) . . . . ?
C3 Pt3 Pt4 Pt5 111.4(10) . . . . ?
Sn3 Pt3 Pt4 Pt5 153.63(4) . . . . ?
Sn2 Pt3 Pt4 Pt5 -32.11(4) . . . . ?
Pt2 Pt3 Pt4 Pt5 -70.93(3) . . . . ?
Sn4 Pt3 Pt4 Pt5 65.10(4) . . . . ?
Pt1 Pt3 Pt4 Pt5 -141.04(3) . . . . ?
Sn1 Pt3 Pt4 Pt5 -109.80(4) . . . . ?
C3 Pt3 Pt4 Sn5 -139.8(10) . . . . ?
Sn3 Pt3 Pt4 Sn5 -97.59(4) . . . . ?
Sn2 Pt3 Pt4 Sn5 76.68(4) . . . . ?
Pt2 Pt3 Pt4 Sn5 37.85(3) . . . . ?
Pt5 Pt3 Pt4 Sn5 108.78(4) . . . . ?
Sn4 Pt3 Pt4 Sn5 173.88(5) . . . . ?
Pt1 Pt3 Pt4 Sn5 -32.25(3) . . . . ?
Sn1 Pt3 Pt4 Sn5 -1.02(5) . . . . ?
C3 Pt3 Pt4 Pt1 -107.5(10) . . . . ?
Sn3 Pt3 Pt4 Pt1 -65.33(3) . . . . ?
Sn2 Pt3 Pt4 Pt1 108.93(4) . . . . ?
Pt2 Pt3 Pt4 Pt1 70.10(3) . . . . ?
Pt5 Pt3 Pt4 Pt1 141.04(3) . . . . ?
Sn4 Pt3 Pt4 Pt1 -153.87(4) . . . . ?
Sn1 Pt3 Pt4 Pt1 31.24(3) . . . . ?
C1 Pt1 Pt4 C4 -7.4(12) . . . . ?
Sn1 Pt1 Pt4 C4 178.3(6) . . . . ?
Sn3 Pt1 Pt4 C4 -74.4(6) . . . . ?
Sn5 Pt1 Pt4 C4 72.5(6) . . . . ?
Pt2 Pt1 Pt4 C4 143.2(6) . . . . ?
Pt3 Pt1 Pt4 C4 -145.9(6) . . . . ?
C1 Pt1 Pt4 Sn6 -124.4(11) . . . . ?
Sn1 Pt1 Pt4 Sn6 61.38(5) . . . . ?
Sn3 Pt1 Pt4 Sn6 168.65(5) . . . . ?
Sn5 Pt1 Pt4 Sn6 -44.45(5) . . . . ?
Pt2 Pt1 Pt4 Sn6 26.27(4) . . . . ?
Pt3 Pt1 Pt4 Sn6 97.14(4) . . . . ?
C1 Pt1 Pt4 Sn3 67.0(11) . . . . ?
Sn1 Pt1 Pt4 Sn3 -107.28(5) . . . . ?
Sn5 Pt1 Pt4 Sn3 146.90(5) . . . . ?
Pt2 Pt1 Pt4 Sn3 -142.38(4) . . . . ?
Pt3 Pt1 Pt4 Sn3 -71.51(4) . . . . ?
C1 Pt1 Pt4 Pt2 -150.6(11) . . . . ?
Sn1 Pt1 Pt4 Pt2 35.10(4) . . . . ?
Sn3 Pt1 Pt4 Pt2 142.38(4) . . . . ?
Sn5 Pt1 Pt4 Pt2 -70.72(3) . . . . ?
Pt3 Pt1 Pt4 Pt2 70.87(2) . . . . ?
C1 Pt1 Pt4 Pt3 138.5(11) . . . . ?
Sn1 Pt1 Pt4 Pt3 -35.77(3) . . . . ?
Sn3 Pt1 Pt4 Pt3 71.51(4) . . . . ?
Sn5 Pt1 Pt4 Pt3 -141.59(4) . . . . ?
Pt2 Pt1 Pt4 Pt3 -70.87(2) . . . . ?
C1 Pt1 Pt4 Sn4 113.2(11) . . . . ?
Sn1 Pt1 Pt4 Sn4 -61.11(5) . . . . ?
Sn3 Pt1 Pt4 Sn4 46.17(5) . . . . ?
Sn5 Pt1 Pt4 Sn4 -166.93(5) . . . . ?
Pt2 Pt1 Pt4 Sn4 -96.21(4) . . . . ?
Pt3 Pt1 Pt4 Sn4 -25.34(4) . . . . ?
C1 Pt1 Pt4 Pt5 174.0(11) . . . . ?
Sn1 Pt1 Pt4 Pt5 -0.25(4) . . . . ?
Sn3 Pt1 Pt4 Pt5 107.03(4) . . . . ?
Sn5 Pt1 Pt4 Pt5 -106.07(4) . . . . ?
Pt2 Pt1 Pt4 Pt5 -35.35(3) . . . . ?
Pt3 Pt1 Pt4 Pt5 35.52(3) . . . . ?
C1 Pt1 Pt4 Sn5 -79.9(11) . . . . ?
Sn1 Pt1 Pt4 Sn5 105.83(5) . . . . ?
Sn3 Pt1 Pt4 Sn5 -146.90(5) . . . . ?
Pt2 Pt1 Pt4 Sn5 70.72(3) . . . . ?
Pt3 Pt1 Pt4 Sn5 141.59(4) . . . . ?
C3 Pt3 Pt5 C5 3.5(13) . . . . ?
Sn3 Pt3 Pt5 C5 122.8(12) . . . . ?
Sn2 Pt3 Pt5 C5 -69.6(12) . . . . ?
Pt4 Pt3 Pt5 C5 148.0(12) . . . . ?
Pt2 Pt3 Pt5 C5 -142.0(12) . . . . ?
Sn4 Pt3 Pt5 C5 76.3(12) . . . . ?
Pt1 Pt3 Pt5 C5 -176.3(12) . . . . ?
Sn1 Pt3 Pt5 C5 -116.9(12) . . . . ?
C3 Pt3 Pt5 Sn6 -176.3(6) . . . . ?
Sn3 Pt3 Pt5 Sn6 -56.97(5) . . . . ?
Sn2 Pt3 Pt5 Sn6 110.57(5) . . . . ?
Pt4 Pt3 Pt5 Sn6 -31.79(4) . . . . ?
Pt2 Pt3 Pt5 Sn6 38.16(4) . . . . ?
Sn4 Pt3 Pt5 Sn6 -103.50(5) . . . . ?
Pt1 Pt3 Pt5 Sn6 3.86(5) . . . . ?
Sn1 Pt3 Pt5 Sn6 63.26(5) . . . . ?
C3 Pt3 Pt5 Sn4 -72.8(6) . . . . ?
Sn3 Pt3 Pt5 Sn4 46.53(5) . . . . ?
Sn2 Pt3 Pt5 Sn4 -145.94(5) . . . . ?
Pt4 Pt3 Pt5 Sn4 71.71(4) . . . . ?
Pt2 Pt3 Pt5 Sn4 141.66(4) . . . . ?
Pt1 Pt3 Pt5 Sn4 107.35(4) . . . . ?
Sn1 Pt3 Pt5 Sn4 166.76(5) . . . . ?
C3 Pt3 Pt5 Sn2 73.2(6) . . . . ?
Sn3 Pt3 Pt5 Sn2 -167.54(5) . . . . ?
Pt4 Pt3 Pt5 Sn2 -142.35(4) . . . . ?
Pt2 Pt3 Pt5 Sn2 -72.41(4) . . . . ?
Sn4 Pt3 Pt5 Sn2 145.94(5) . . . . ?
Pt1 Pt3 Pt5 Sn2 -106.71(4) . . . . ?
Sn1 Pt3 Pt5 Sn2 -47.31(4) . . . . ?
C3 Pt3 Pt5 Pt4 -144.5(6) . . . . ?
Sn3 Pt3 Pt5 Pt4 -25.18(4) . . . . ?
Sn2 Pt3 Pt5 Pt4 142.35(4) . . . . ?
Pt2 Pt3 Pt5 Pt4 69.95(3) . . . . ?
Sn4 Pt3 Pt5 Pt4 -71.71(4) . . . . ?
Pt1 Pt3 Pt5 Pt4 35.64(3) . . . . ?
Sn1 Pt3 Pt5 Pt4 95.05(4) . . . . ?
C3 Pt3 Pt5 Pt2 145.6(6) . . . . ?
Sn3 Pt3 Pt5 Pt2 -95.13(4) . . . . ?
Sn2 Pt3 Pt5 Pt2 72.41(4) . . . . ?
Pt4 Pt3 Pt5 Pt2 -69.95(3) . . . . ?
Sn4 Pt3 Pt5 Pt2 -141.66(4) . . . . ?
Pt1 Pt3 Pt5 Pt2 -34.30(3) . . . . ?
Sn1 Pt3 Pt5 Pt2 25.10(3) . . . . ?
C4 Pt4 Pt5 C5 -5.3(13) . . . . ?
Sn6 Pt4 Pt5 C5 63.1(11) . . . . ?
Sn3 Pt4 Pt5 C5 -126.2(11) . . . . ?
Pt2 Pt4 Pt5 C5 138.1(11) . . . . ?
Pt3 Pt4 Pt5 C5 -151.2(11) . . . . ?
Sn4 Pt4 Pt5 C5 -78.2(11) . . . . ?
Sn5 Pt4 Pt5 C5 113.1(11) . . . . ?
Pt1 Pt4 Pt5 C5 173.2(11) . . . . ?
C4 Pt4 Pt5 Sn6 -68.4(6) . . . . ?
Sn3 Pt4 Pt5 Sn6 170.68(5) . . . . ?
Pt2 Pt4 Pt5 Sn6 75.05(3) . . . . ?
Pt3 Pt4 Pt5 Sn6 145.71(4) . . . . ?
Sn4 Pt4 Pt5 Sn6 -141.27(5) . . . . ?
Sn5 Pt4 Pt5 Sn6 49.97(4) . . . . ?
Pt1 Pt4 Pt5 Sn6 110.14(4) . . . . ?
C4 Pt4 Pt5 Sn4 72.9(6) . . . . ?
Sn6 Pt4 Pt5 Sn4 141.27(5) . . . . ?
Sn3 Pt4 Pt5 Sn4 -48.05(5) . . . . ?
Pt2 Pt4 Pt5 Sn4 -143.68(4) . . . . ?
Pt3 Pt4 Pt5 Sn4 -73.02(4) . . . . ?
Sn5 Pt4 Pt5 Sn4 -168.76(4) . . . . ?
Pt1 Pt4 Pt5 Sn4 -108.59(4) . . . . ?
C4 Pt4 Pt5 Sn2 -179.3(6) . . . . ?
Sn6 Pt4 Pt5 Sn2 -110.90(5) . . . . ?
Sn3 Pt4 Pt5 Sn2 59.78(5) . . . . ?
Pt2 Pt4 Pt5 Sn2 -35.86(4) . . . . ?
Pt3 Pt4 Pt5 Sn2 34.81(4) . . . . ?
Sn4 Pt4 Pt5 Sn2 107.83(5) . . . . ?
Sn5 Pt4 Pt5 Sn2 -60.94(5) . . . . ?
Pt1 Pt4 Pt5 Sn2 -0.77(5) . . . . ?
C4 Pt4 Pt5 Pt3 145.9(6) . . . . ?
Sn6 Pt4 Pt5 Pt3 -145.71(4) . . . . ?
Sn3 Pt4 Pt5 Pt3 24.97(4) . . . . ?
Pt2 Pt4 Pt5 Pt3 -70.67(3) . . . . ?
Sn4 Pt4 Pt5 Pt3 73.02(4) . . . . ?
Sn5 Pt4 Pt5 Pt3 -95.74(4) . . . . ?
Pt1 Pt4 Pt5 Pt3 -35.57(3) . . . . ?
C4 Pt4 Pt5 Pt2 -143.4(6) . . . . ?
Sn6 Pt4 Pt5 Pt2 -75.05(3) . . . . ?
Sn3 Pt4 Pt5 Pt2 95.64(4) . . . . ?
Pt3 Pt4 Pt5 Pt2 70.67(3) . . . . ?
Sn4 Pt4 Pt5 Pt2 143.68(4) . . . . ?
Sn5 Pt4 Pt5 Pt2 -25.08(3) . . . . ?
Pt1 Pt4 Pt5 Pt2 35.09(3) . . . . ?
C2 Pt2 Pt5 C5 3.2(12) . . . . ?
Sn5 Pt2 Pt5 C5 -115.1(11) . . . . ?
Pt4 Pt2 Pt5 C5 -141.3(11) . . . . ?
Sn1 Pt2 Pt5 C5 122.8(11) . . . . ?
Pt1 Pt2 Pt5 C5 -176.9(11) . . . . ?
Pt3 Pt2 Pt5 C5 148.4(11) . . . . ?
Sn2 Pt2 Pt5 C5 77.2(11) . . . . ?
Sn6 Pt2 Pt5 C5 -71.5(11) . . . . ?
C2 Pt2 Pt5 Sn6 74.7(6) . . . . ?
Sn5 Pt2 Pt5 Sn6 -43.51(5) . . . . ?
Pt4 Pt2 Pt5 Sn6 -69.76(4) . . . . ?
Sn1 Pt2 Pt5 Sn6 -165.65(5) . . . . ?
Pt1 Pt2 Pt5 Sn6 -105.35(4) . . . . ?
Pt3 Pt2 Pt5 Sn6 -140.08(4) . . . . ?
Sn2 Pt2 Pt5 Sn6 148.73(5) . . . . ?
C2 Pt2 Pt5 Sn4 178.6(6) . . . . ?
Sn5 Pt2 Pt5 Sn4 60.32(5) . . . . ?
Pt4 Pt2 Pt5 Sn4 34.08(4) . . . . ?
Sn1 Pt2 Pt5 Sn4 -61.81(5) . . . . ?
Pt1 Pt2 Pt5 Sn4 -1.52(5) . . . . ?
Pt3 Pt2 Pt5 Sn4 -36.25(4) . . . . ?
Sn2 Pt2 Pt5 Sn4 -107.43(5) . . . . ?
Sn6 Pt2 Pt5 Sn4 103.84(5) . . . . ?
C2 Pt2 Pt5 Sn2 -74.0(6) . . . . ?
Sn5 Pt2 Pt5 Sn2 167.76(5) . . . . ?
Pt4 Pt2 Pt5 Sn2 141.51(4) . . . . ?
Sn1 Pt2 Pt5 Sn2 45.62(5) . . . . ?
Pt1 Pt2 Pt5 Sn2 105.91(4) . . . . ?
Pt3 Pt2 Pt5 Sn2 71.19(4) . . . . ?
Sn6 Pt2 Pt5 Sn2 -148.73(5) . . . . ?
C2 Pt2 Pt5 Pt3 -145.2(6) . . . . ?
Sn5 Pt2 Pt5 Pt3 96.57(4) . . . . ?
Pt4 Pt2 Pt5 Pt3 70.33(3) . . . . ?
Sn1 Pt2 Pt5 Pt3 -25.57(4) . . . . ?
Pt1 Pt2 Pt5 Pt3 34.73(3) . . . . ?
Sn2 Pt2 Pt5 Pt3 -71.19(4) . . . . ?
Sn6 Pt2 Pt5 Pt3 140.08(4) . . . . ?
C2 Pt2 Pt5 Pt4 144.5(6) . . . . ?
Sn5 Pt2 Pt5 Pt4 26.24(4) . . . . ?
Sn1 Pt2 Pt5 Pt4 -95.89(4) . . . . ?
Pt1 Pt2 Pt5 Pt4 -35.60(3) . . . . ?
Pt3 Pt2 Pt5 Pt4 -70.33(3) . . . . ?
Sn2 Pt2 Pt5 Pt4 -141.51(4) . . . . ?
Sn6 Pt2 Pt5 Pt4 69.76(4) . . . . ?
C1 Pt1 Sn1 O11 -172.5(9) . . . . ?
Sn3 Pt1 Sn1 O11 -63.6(5) . . . . ?
Sn5 Pt1 Sn1 O11 71.5(5) . . . . ?
Pt2 Pt1 Sn1 O11 37.6(5) . . . . ?
Pt3 Pt1 Sn1 O11 -30.7(5) . . . . ?
Pt4 Pt1 Sn1 O11 3.7(5) . . . . ?
C1 Pt1 Sn1 Cl2 58.3(7) . . . . ?
Sn3 Pt1 Sn1 Cl2 167.20(15) . . . . ?
Sn5 Pt1 Sn1 Cl2 -57.72(15) . . . . ?
Pt2 Pt1 Sn1 Cl2 -91.64(15) . . . . ?
Pt3 Pt1 Sn1 Cl2 -159.89(15) . . . . ?
Pt4 Pt1 Sn1 Cl2 -125.56(15) . . . . ?
C1 Pt1 Sn1 Cl1 -46.0(8) . . . . ?
Sn3 Pt1 Sn1 Cl1 62.96(17) . . . . ?
Sn5 Pt1 Sn1 Cl1 -161.95(16) . . . . ?
Pt2 Pt1 Sn1 Cl1 164.12(17) . . . . ?
Pt3 Pt1 Sn1 Cl1 95.88(17) . . . . ?
Pt4 Pt1 Sn1 Cl1 130.21(16) . . . . ?
C1 Pt1 Sn1 Pt2 149.9(7) . . . . ?
Sn3 Pt1 Sn1 Pt2 -101.16(4) . . . . ?
Sn5 Pt1 Sn1 Pt2 33.92(4) . . . . ?
Pt3 Pt1 Sn1 Pt2 -68.25(3) . . . . ?
Pt4 Pt1 Sn1 Pt2 -33.92(3) . . . . ?
C1 Pt1 Sn1 Pt3 -141.9(7) . . . . ?
Sn3 Pt1 Sn1 Pt3 -32.91(4) . . . . ?
Sn5 Pt1 Sn1 Pt3 102.17(4) . . . . ?
Pt2 Pt1 Sn1 Pt3 68.25(3) . . . . ?
Pt4 Pt1 Sn1 Pt3 34.33(3) . . . . ?
C2 Pt2 Sn1 O11 75.6(7) . . . . ?
Sn5 Pt2 Sn1 O11 173.1(3) . . . . ?
Pt4 Pt2 Sn1 O11 -123.1(3) . . . . ?
Pt1 Pt2 Sn1 O11 -156.5(3) . . . . ?
Pt3 Pt2 Sn1 O11 -83.8(3) . . . . ?
Sn2 Pt2 Sn1 O11 -20.5(3) . . . . ?
Pt5 Pt2 Sn1 O11 -58.4(3) . . . . ?
Sn6 Pt2 Sn1 O11 -107.3(3) . . . . ?
C2 Pt2 Sn1 Cl2 -16.4(6) . . . . ?
Sn5 Pt2 Sn1 Cl2 81.19(14) . . . . ?
Pt4 Pt2 Sn1 Cl2 144.99(13) . . . . ?
Pt1 Pt2 Sn1 Cl2 111.54(14) . . . . ?
Pt3 Pt2 Sn1 Cl2 -175.76(14) . . . . ?
Sn2 Pt2 Sn1 Cl2 -112.44(14) . . . . ?
Pt5 Pt2 Sn1 Cl2 -150.40(13) . . . . ?
Sn6 Pt2 Sn1 Cl2 160.78(19) . . . . ?
C2 Pt2 Sn1 Cl1 156.0(8) . . . . ?
Sn5 Pt2 Sn1 Cl1 -106.4(6) . . . . ?
Pt4 Pt2 Sn1 Cl1 -42.6(6) . . . . ?
Pt1 Pt2 Sn1 Cl1 -76.1(6) . . . . ?
Pt3 Pt2 Sn1 Cl1 -3.4(6) . . . . ?
Sn2 Pt2 Sn1 Cl1 60.0(6) . . . . ?
Pt5 Pt2 Sn1 Cl1 22.0(6) . . . . ?
Sn6 Pt2 Sn1 Cl1 -26.8(6) . . . . ?
C2 Pt2 Sn1 Pt1 -127.9(6) . . . . ?
Sn5 Pt2 Sn1 Pt1 -30.35(4) . . . . ?
Pt4 Pt2 Sn1 Pt1 33.45(3) . . . . ?
Pt3 Pt2 Sn1 Pt1 72.70(3) . . . . ?
Sn2 Pt2 Sn1 Pt1 136.02(4) . . . . ?
Pt5 Pt2 Sn1 Pt1 98.06(4) . . . . ?
Sn6 Pt2 Sn1 Pt1 49.24(16) . . . . ?
C2 Pt2 Sn1 Pt3 159.4(6) . . . . ?
Sn5 Pt2 Sn1 Pt3 -103.05(4) . . . . ?
Pt4 Pt2 Sn1 Pt3 -39.25(3) . . . . ?
Pt1 Pt2 Sn1 Pt3 -72.70(3) . . . . ?
Sn2 Pt2 Sn1 Pt3 63.32(3) . . . . ?
Pt5 Pt2 Sn1 Pt3 25.36(3) . . . . ?
Sn6 Pt2 Sn1 Pt3 -23.46(16) . . . . ?
C3 Pt3 Sn1 O11 -72.8(6) . . . . ?
Sn3 Pt3 Sn1 O11 -170.9(3) . . . . ?
Sn2 Pt3 Sn1 O11 23.1(3) . . . . ?
Pt4 Pt3 Sn1 O11 126.8(3) . . . . ?
Pt2 Pt3 Sn1 O11 87.9(3) . . . . ?
Pt5 Pt3 Sn1 O11 62.6(3) . . . . ?
Sn4 Pt3 Sn1 O11 109.6(4) . . . . ?
Pt1 Pt3 Sn1 O11 160.4(3) . . . . ?
C3 Pt3 Sn1 Cl2 -147.3(6) . . . . ?
Sn3 Pt3 Sn1 Cl2 114.5(4) . . . . ?
Sn2 Pt3 Sn1 Cl2 -51.5(4) . . . . ?
Pt4 Pt3 Sn1 Cl2 52.2(4) . . . . ?
Pt2 Pt3 Sn1 Cl2 13.3(4) . . . . ?
Pt5 Pt3 Sn1 Cl2 -12.0(4) . . . . ?
Sn4 Pt3 Sn1 Cl2 35.0(5) . . . . ?
Pt1 Pt3 Sn1 Cl2 85.8(4) . . . . ?
C3 Pt3 Sn1 Cl1 18.4(5) . . . . ?
Sn3 Pt3 Sn1 Cl1 -79.69(16) . . . . ?
Sn2 Pt3 Sn1 Cl1 114.31(16) . . . . ?
Pt4 Pt3 Sn1 Cl1 -141.99(16) . . . . ?
Pt2 Pt3 Sn1 Cl1 179.10(16) . . . . ?
Pt5 Pt3 Sn1 Cl1 153.80(15) . . . . ?
Sn4 Pt3 Sn1 Cl1 -159.3(2) . . . . ?
Pt1 Pt3 Sn1 Cl1 -108.41(16) . . . . ?
C3 Pt3 Sn1 Pt1 126.8(5) . . . . ?
Sn3 Pt3 Sn1 Pt1 28.72(4) . . . . ?
Sn2 Pt3 Sn1 Pt1 -137.29(4) . . . . ?
Pt4 Pt3 Sn1 Pt1 -33.58(3) . . . . ?
Pt2 Pt3 Sn1 Pt1 -72.50(3) . . . . ?
Pt5 Pt3 Sn1 Pt1 -97.79(4) . . . . ?
Sn4 Pt3 Sn1 Pt1 -50.86(17) . . . . ?
C3 Pt3 Sn1 Pt2 -160.7(5) . . . . ?
Sn3 Pt3 Sn1 Pt2 101.21(4) . . . . ?
Sn2 Pt3 Sn1 Pt2 -64.79(3) . . . . ?
Pt4 Pt3 Sn1 Pt2 38.92(3) . . . . ?
Pt5 Pt3 Sn1 Pt2 -25.29(3) . . . . ?
Sn4 Pt3 Sn1 Pt2 21.64(17) . . . . ?
Pt1 Pt3 Sn1 Pt2 72.50(3) . . . . ?
C5 Pt5 Sn2 O11 -176.8(8) . . . . ?
Sn6 Pt5 Sn2 O11 -66.9(5) . . . . ?
Sn4 Pt5 Sn2 O11 66.9(5) . . . . ?
Pt3 Pt5 Sn2 O11 33.8(5) . . . . ?
Pt4 Pt5 Sn2 O11 -0.4(5) . . . . ?
Pt2 Pt5 Sn2 O11 -35.2(5) . . . . ?
C5 Pt5 Sn2 Cl3 -51.1(7) . . . . ?
Sn6 Pt5 Sn2 Cl3 58.86(18) . . . . ?
Sn4 Pt5 Sn2 Cl3 -167.32(17) . . . . ?
Pt3 Pt5 Sn2 Cl3 159.52(18) . . . . ?
Pt4 Pt5 Sn2 Cl3 125.33(17) . . . . ?
Pt2 Pt5 Sn2 Cl3 90.50(17) . . . . ?
C5 Pt5 Sn2 Cl4 54.7(7) . . . . ?
Sn6 Pt5 Sn2 Cl4 164.66(17) . . . . ?
Sn4 Pt5 Sn2 Cl4 -61.53(17) . . . . ?
Pt3 Pt5 Sn2 Cl4 -94.68(17) . . . . ?
Pt4 Pt5 Sn2 Cl4 -128.87(17) . . . . ?
Pt2 Pt5 Sn2 Cl4 -163.71(17) . . . . ?
C5 Pt5 Sn2 Pt3 149.4(7) . . . . ?
Sn6 Pt5 Sn2 Pt3 -100.66(5) . . . . ?
Sn4 Pt5 Sn2 Pt3 33.16(4) . . . . ?
Pt4 Pt5 Sn2 Pt3 -34.19(3) . . . . ?
Pt2 Pt5 Sn2 Pt3 -69.02(3) . . . . ?
C5 Pt5 Sn2 Pt2 -141.6(7) . . . . ?
Sn6 Pt5 Sn2 Pt2 -31.64(5) . . . . ?
Sn4 Pt5 Sn2 Pt2 102.18(4) . . . . ?
Pt3 Pt5 Sn2 Pt2 69.02(3) . . . . ?
Pt4 Pt5 Sn2 Pt2 34.83(3) . . . . ?
C3 Pt3 Sn2 O11 71.9(6) . . . . ?
Sn3 Pt3 Sn2 O11 -104.4(4) . . . . ?
Pt4 Pt3 Sn2 O11 -125.7(3) . . . . ?
Pt2 Pt3 Sn2 O11 -87.2(3) . . . . ?
Pt5 Pt3 Sn2 O11 -159.4(3) . . . . ?
Sn4 Pt3 Sn2 O11 172.1(3) . . . . ?
Pt1 Pt3 Sn2 O11 -60.9(3) . . . . ?
Sn1 Pt3 Sn2 O11 -23.4(3) . . . . ?
C3 Pt3 Sn2 Cl3 147.8(8) . . . . ?
Sn3 Pt3 Sn2 Cl3 -28.5(7) . . . . ?
Pt4 Pt3 Sn2 Cl3 -49.8(6) . . . . ?
Pt2 Pt3 Sn2 Cl3 -11.3(6) . . . . ?
Pt5 Pt3 Sn2 Cl3 -83.5(6) . . . . ?
Sn4 Pt3 Sn2 Cl3 -112.0(6) . . . . ?
Pt1 Pt3 Sn2 Cl3 15.0(6) . . . . ?
Sn1 Pt3 Sn2 Cl3 52.5(6) . . . . ?
C3 Pt3 Sn2 Cl4 -19.0(6) . . . . ?
Sn3 Pt3 Sn2 Cl4 164.7(2) . . . . ?
Pt4 Pt3 Sn2 Cl4 143.36(15) . . . . ?
Pt2 Pt3 Sn2 Cl4 -178.14(16) . . . . ?
Pt5 Pt3 Sn2 Cl4 109.64(15) . . . . ?
Sn4 Pt3 Sn2 Cl4 81.13(15) . . . . ?
Pt1 Pt3 Sn2 Cl4 -151.81(15) . . . . ?
Sn1 Pt3 Sn2 Cl4 -114.33(15) . . . . ?
C3 Pt3 Sn2 Pt5 -128.7(5) . . . . ?
Sn3 Pt3 Sn2 Pt5 55.05(19) . . . . ?
Pt4 Pt3 Sn2 Pt5 33.72(3) . . . . ?
Pt2 Pt3 Sn2 Pt5 72.22(3) . . . . ?
Sn4 Pt3 Sn2 Pt5 -28.50(4) . . . . ?
Pt1 Pt3 Sn2 Pt5 98.55(4) . . . . ?
Sn1 Pt3 Sn2 Pt5 136.03(4) . . . . ?
C3 Pt3 Sn2 Pt2 159.1(5) . . . . ?
Sn3 Pt3 Sn2 Pt2 -17.17(19) . . . . ?
Pt4 Pt3 Sn2 Pt2 -38.50(3) . . . . ?
Pt5 Pt3 Sn2 Pt2 -72.22(3) . . . . ?
Sn4 Pt3 Sn2 Pt2 -100.73(4) . . . . ?
Pt1 Pt3 Sn2 Pt2 26.33(3) . . . . ?
Sn1 Pt3 Sn2 Pt2 63.81(3) . . . . ?
C2 Pt2 Sn2 O11 -74.1(7) . . . . ?
Sn5 Pt2 Sn2 O11 103.0(4) . . . . ?
Pt4 Pt2 Sn2 O11 124.4(3) . . . . ?
Sn1 Pt2 Sn2 O11 20.8(3) . . . . ?
Pt1 Pt2 Sn2 O11 59.5(3) . . . . ?
Pt3 Pt2 Sn2 O11 86.0(3) . . . . ?
Pt5 Pt2 Sn2 O11 158.7(3) . . . . ?
Sn6 Pt2 Sn2 O11 -175.3(3) . . . . ?
C2 Pt2 Sn2 Cl3 16.2(6) . . . . ?
Sn5 Pt2 Sn2 Cl3 -166.7(2) . . . . ?
Pt4 Pt2 Sn2 Cl3 -145.32(19) . . . . ?
Sn1 Pt2 Sn2 Cl3 111.11(19) . . . . ?
Pt1 Pt2 Sn2 Cl3 149.83(19) . . . . ?
Pt3 Pt2 Sn2 Cl3 176.30(19) . . . . ?
Pt5 Pt2 Sn2 Cl3 -111.06(19) . . . . ?
Sn6 Pt2 Sn2 Cl3 -85.03(19) . . . . ?
C2 Pt2 Sn2 Cl4 -153.2(8) . . . . ?
Sn5 Pt2 Sn2 Cl4 24.0(6) . . . . ?
Pt4 Pt2 Sn2 Cl4 45.3(6) . . . . ?
Sn1 Pt2 Sn2 Cl4 -58.3(6) . . . . ?
Pt1 Pt2 Sn2 Cl4 -19.6(6) . . . . ?
Pt3 Pt2 Sn2 Cl4 6.9(6) . . . . ?
Pt5 Pt2 Sn2 Cl4 79.6(6) . . . . ?
Sn6 Pt2 Sn2 Cl4 105.6(6) . . . . ?
C2 Pt2 Sn2 Pt5 127.2(6) . . . . ?
Sn5 Pt2 Sn2 Pt5 -55.61(19) . . . . ?
Pt4 Pt2 Sn2 Pt5 -34.26(3) . . . . ?
Sn1 Pt2 Sn2 Pt5 -137.83(4) . . . . ?
Pt1 Pt2 Sn2 Pt5 -99.12(4) . . . . ?
Pt3 Pt2 Sn2 Pt5 -72.64(3) . . . . ?
Sn6 Pt2 Sn2 Pt5 26.03(4) . . . . ?
C2 Pt2 Sn2 Pt3 -160.1(6) . . . . ?
Sn5 Pt2 Sn2 Pt3 17.04(19) . . . . ?
Pt4 Pt2 Sn2 Pt3 38.38(3) . . . . ?
Sn1 Pt2 Sn2 Pt3 -65.19(3) . . . . ?
Pt1 Pt2 Sn2 Pt3 -26.47(3) . . . . ?
Pt5 Pt2 Sn2 Pt3 72.64(3) . . . . ?
Sn6 Pt2 Sn2 Pt3 98.67(4) . . . . ?
C1 Pt1 Sn3 O12 -175.7(8) . . . . ?
Sn1 Pt1 Sn3 O12 70.2(5) . . . . ?
Sn5 Pt1 Sn3 O12 -64.2(5) . . . . ?
Pt2 Pt1 Sn3 O12 2.1(5) . . . . ?
Pt3 Pt1 Sn3 O12 36.6(5) . . . . ?
Pt4 Pt1 Sn3 O12 -32.0(5) . . . . ?
C1 Pt1 Sn3 Cl6 -49.7(6) . . . . ?
Sn1 Pt1 Sn3 Cl6 -163.83(17) . . . . ?
Sn5 Pt1 Sn3 Cl6 61.82(17) . . . . ?
Pt2 Pt1 Sn3 Cl6 128.06(17) . . . . ?
Pt3 Pt1 Sn3 Cl6 162.60(17) . . . . ?
Pt4 Pt1 Sn3 Cl6 94.00(17) . . . . ?
C1 Pt1 Sn3 Cl5 53.4(6) . . . . ?
Sn1 Pt1 Sn3 Cl5 -60.73(18) . . . . ?
Sn5 Pt1 Sn3 Cl5 164.92(17) . . . . ?
Pt2 Pt1 Sn3 Cl5 -128.84(17) . . . . ?
Pt3 Pt1 Sn3 Cl5 -94.30(17) . . . . ?
Pt4 Pt1 Sn3 Cl5 -162.91(18) . . . . ?
C1 Pt1 Sn3 Pt3 147.7(6) . . . . ?
Sn1 Pt1 Sn3 Pt3 33.57(4) . . . . ?
Sn5 Pt1 Sn3 Pt3 -100.78(4) . . . . ?
Pt2 Pt1 Sn3 Pt3 -34.54(3) . . . . ?
Pt4 Pt1 Sn3 Pt3 -68.61(3) . . . . ?
C1 Pt1 Sn3 Pt4 -143.7(6) . . . . ?
Sn1 Pt1 Sn3 Pt4 102.17(4) . . . . ?
Sn5 Pt1 Sn3 Pt4 -32.17(4) . . . . ?
Pt2 Pt1 Sn3 Pt4 34.07(3) . . . . ?
Pt3 Pt1 Sn3 Pt4 68.61(3) . . . . ?
C3 Pt3 Sn3 O12 75.1(6) . . . . ?
Sn2 Pt3 Sn3 O12 -108.6(4) . . . . ?
Pt4 Pt3 Sn3 O12 -85.0(3) . . . . ?
Pt2 Pt3 Sn3 O12 -124.1(3) . . . . ?
Pt5 Pt3 Sn3 O12 -59.7(3) . . . . ?
Sn4 Pt3 Sn3 O12 -21.3(3) . . . . ?
Pt1 Pt3 Sn3 O12 -157.7(3) . . . . ?
Sn1 Pt3 Sn3 O12 174.0(3) . . . . ?
C3 Pt3 Sn3 Cl6 158.8(9) . . . . ?
Sn2 Pt3 Sn3 Cl6 -24.9(7) . . . . ?
Pt4 Pt3 Sn3 Cl6 -1.3(7) . . . . ?
Pt2 Pt3 Sn3 Cl6 -40.4(7) . . . . ?
Pt5 Pt3 Sn3 Cl6 24.0(7) . . . . ?
Sn4 Pt3 Sn3 Cl6 62.4(7) . . . . ?
Pt1 Pt3 Sn3 Cl6 -74.0(7) . . . . ?
Sn1 Pt3 Sn3 Cl6 -102.3(7) . . . . ?
C3 Pt3 Sn3 Cl5 -18.0(6) . . . . ?
Sn2 Pt3 Sn3 Cl5 158.2(2) . . . . ?
Pt4 Pt3 Sn3 Cl5 -178.12(15) . . . . ?
Pt2 Pt3 Sn3 Cl5 142.72(15) . . . . ?
Pt5 Pt3 Sn3 Cl5 -152.88(15) . . . . ?
Sn4 Pt3 Sn3 Cl5 -114.46(15) . . . . ?
Pt1 Pt3 Sn3 Cl5 109.12(15) . . . . ?
Sn1 Pt3 Sn3 Cl5 80.86(15) . . . . ?
C3 Pt3 Sn3 Pt1 -127.2(5) . . . . ?
Sn2 Pt3 Sn3 Pt1 49.12(19) . . . . ?
Pt4 Pt3 Sn3 Pt1 72.76(3) . . . . ?
Pt2 Pt3 Sn3 Pt1 33.60(3) . . . . ?
Pt5 Pt3 Sn3 Pt1 98.00(4) . . . . ?
Sn4 Pt3 Sn3 Pt1 136.43(4) . . . . ?
Sn1 Pt3 Sn3 Pt1 -28.26(4) . . . . ?
C3 Pt3 Sn3 Pt4 160.1(5) . . . . ?
Sn2 Pt3 Sn3 Pt4 -23.64(19) . . . . ?
Pt2 Pt3 Sn3 Pt4 -39.16(3) . . . . ?
Pt5 Pt3 Sn3 Pt4 25.24(4) . . . . ?
Sn4 Pt3 Sn3 Pt4 63.67(3) . . . . ?
Pt1 Pt3 Sn3 Pt4 -72.76(3) . . . . ?
Sn1 Pt3 Sn3 Pt4 -101.02(4) . . . . ?
C4 Pt4 Sn3 O12 -74.0(6) . . . . ?
Sn6 Pt4 Sn3 O12 102.8(4) . . . . ?
Pt2 Pt4 Sn3 O12 126.9(3) . . . . ?
Pt3 Pt4 Sn3 O12 87.4(3) . . . . ?
Sn4 Pt4 Sn3 O12 22.5(3) . . . . ?
Pt5 Pt4 Sn3 O12 62.2(3) . . . . ?
Sn5 Pt4 Sn3 O12 -172.0(3) . . . . ?
Pt1 Pt4 Sn3 O12 160.3(3) . . . . ?
C4 Pt4 Sn3 Cl6 18.3(6) . . . . ?
Sn6 Pt4 Sn3 Cl6 -165.0(3) . . . . ?
Pt2 Pt4 Sn3 Cl6 -140.87(19) . . . . ?
Pt3 Pt4 Sn3 Cl6 179.6(2) . . . . ?
Sn4 Pt4 Sn3 Cl6 114.8(2) . . . . ?
Pt5 Pt4 Sn3 Cl6 154.47(19) . . . . ?
Sn5 Pt4 Sn3 Cl6 -79.7(2) . . . . ?
Pt1 Pt4 Sn3 Cl6 -107.4(2) . . . . ?
C4 Pt4 Sn3 Cl5 -154.7(8) . . . . ?
Sn6 Pt4 Sn3 Cl5 22.1(6) . . . . ?
Pt2 Pt4 Sn3 Cl5 46.1(5) . . . . ?
Pt3 Pt4 Sn3 Cl5 6.6(5) . . . . ?
Sn4 Pt4 Sn3 Cl5 -58.2(5) . . . . ?
Pt5 Pt4 Sn3 Cl5 -18.5(5) . . . . ?
Sn5 Pt4 Sn3 Cl5 107.3(5) . . . . ?
Pt1 Pt4 Sn3 Cl5 79.6(5) . . . . ?
C4 Pt4 Sn3 Pt1 125.7(5) . . . . ?
Sn6 Pt4 Sn3 Pt1 -57.5(2) . . . . ?
Pt2 Pt4 Sn3 Pt1 -33.42(3) . . . . ?
Pt3 Pt4 Sn3 Pt1 -72.93(3) . . . . ?
Sn4 Pt4 Sn3 Pt1 -137.77(4) . . . . ?
Pt5 Pt4 Sn3 Pt1 -98.08(4) . . . . ?
Sn5 Pt4 Sn3 Pt1 27.72(4) . . . . ?
C4 Pt4 Sn3 Pt3 -161.3(5) . . . . ?
Sn6 Pt4 Sn3 Pt3 15.4(2) . . . . ?
Pt2 Pt4 Sn3 Pt3 39.51(3) . . . . ?
Sn4 Pt4 Sn3 Pt3 -64.83(4) . . . . ?
Pt5 Pt4 Sn3 Pt3 -25.15(4) . . . . ?
Sn5 Pt4 Sn3 Pt3 100.65(4) . . . . ?
Pt1 Pt4 Sn3 Pt3 72.93(3) . . . . ?
C5 Pt5 Sn4 O12 178.3(8) . . . . ?
Sn6 Pt5 Sn4 O12 70.1(5) . . . . ?
Sn2 Pt5 Sn4 O12 -66.6(5) . . . . ?
Pt3 Pt5 Sn4 O12 -33.9(5) . . . . ?
Pt4 Pt5 Sn4 O12 34.4(5) . . . . ?
Pt2 Pt5 Sn4 O12 1.2(5) . . . . ?
C5 Pt5 Sn4 Cl7 -52.8(7) . . . . ?
Sn6 Pt5 Sn4 Cl7 -161.0(2) . . . . ?
Sn2 Pt5 Sn4 Cl7 62.3(2) . . . . ?
Pt3 Pt5 Sn4 Cl7 95.0(2) . . . . ?
Pt4 Pt5 Sn4 Cl7 163.3(2) . . . . ?
Pt2 Pt5 Sn4 Cl7 130.1(2) . . . . ?
C5 Pt5 Sn4 Cl8 51.7(7) . . . . ?
Sn6 Pt5 Sn4 Cl8 -56.42(17) . . . . ?
Sn2 Pt5 Sn4 Cl8 166.88(16) . . . . ?
Pt3 Pt5 Sn4 Cl8 -160.45(17) . . . . ?
Pt4 Pt5 Sn4 Cl8 -92.14(17) . . . . ?
Pt2 Pt5 Sn4 Cl8 -125.30(16) . . . . ?
C5 Pt5 Sn4 Pt4 143.9(7) . . . . ?
Sn6 Pt5 Sn4 Pt4 35.71(4) . . . . ?
Sn2 Pt5 Sn4 Pt4 -100.98(4) . . . . ?
Pt3 Pt5 Sn4 Pt4 -68.31(3) . . . . ?
Pt2 Pt5 Sn4 Pt4 -33.17(3) . . . . ?
C5 Pt5 Sn4 Pt3 -147.8(7) . . . . ?
Sn6 Pt5 Sn4 Pt3 104.02(4) . . . . ?
Sn2 Pt5 Sn4 Pt3 -32.67(4) . . . . ?
Pt4 Pt5 Sn4 Pt3 68.31(3) . . . . ?
Pt2 Pt5 Sn4 Pt3 35.15(3) . . . . ?
C4 Pt4 Sn4 O12 72.8(6) . . . . ?
Sn6 Pt4 Sn4 O12 169.7(3) . . . . ?
Sn3 Pt4 Sn4 O12 -22.4(3) . . . . ?
Pt2 Pt4 Sn4 O12 -125.2(3) . . . . ?
Pt3 Pt4 Sn4 O12 -85.8(3) . . . . ?
Pt5 Pt4 Sn4 O12 -157.9(3) . . . . ?
Sn5 Pt4 Sn4 O12 -110.8(3) . . . . ?
Pt1 Pt4 Sn4 O12 -60.6(3) . . . . ?
C4 Pt4 Sn4 Cl7 150.2(9) . . . . ?
Sn6 Pt4 Sn4 Cl7 -112.9(7) . . . . ?
Sn3 Pt4 Sn4 Cl7 55.0(7) . . . . ?
Pt2 Pt4 Sn4 Cl7 -47.8(7) . . . . ?
Pt3 Pt4 Sn4 Cl7 -8.4(7) . . . . ?
Pt5 Pt4 Sn4 Cl7 -80.5(7) . . . . ?
Sn5 Pt4 Sn4 Cl7 -33.4(7) . . . . ?
Pt1 Pt4 Sn4 Cl7 16.8(7) . . . . ?
C4 Pt4 Sn4 Cl8 -18.0(5) . . . . ?
Sn6 Pt4 Sn4 Cl8 78.92(15) . . . . ?
Sn3 Pt4 Sn4 Cl8 -113.19(15) . . . . ?
Pt2 Pt4 Sn4 Cl8 144.04(15) . . . . ?
Pt3 Pt4 Sn4 Cl8 -176.64(15) . . . . ?
Pt5 Pt4 Sn4 Cl8 111.26(15) . . . . ?
Sn5 Pt4 Sn4 Cl8 158.4(2) . . . . ?
Pt1 Pt4 Sn4 Cl8 -151.40(15) . . . . ?
C4 Pt4 Sn4 Pt5 -129.3(5) . . . . ?
Sn6 Pt4 Sn4 Pt5 -32.34(4) . . . . ?
Sn3 Pt4 Sn4 Pt5 135.55(4) . . . . ?
Pt2 Pt4 Sn4 Pt5 32.78(3) . . . . ?
Pt3 Pt4 Sn4 Pt5 72.10(3) . . . . ?
Sn5 Pt4 Sn4 Pt5 47.17(18) . . . . ?
Pt1 Pt4 Sn4 Pt5 97.34(4) . . . . ?
C4 Pt4 Sn4 Pt3 158.6(5) . . . . ?
Sn6 Pt4 Sn4 Pt3 -104.44(4) . . . . ?
Sn3 Pt4 Sn4 Pt3 63.45(3) . . . . ?
Pt2 Pt4 Sn4 Pt3 -39.32(3) . . . . ?
Pt5 Pt4 Sn4 Pt3 -72.10(3) . . . . ?
Sn5 Pt4 Sn4 Pt3 -24.94(17) . . . . ?
Pt1 Pt4 Sn4 Pt3 25.24(4) . . . . ?
C3 Pt3 Sn4 O12 -73.0(6) . . . . ?
Sn3 Pt3 Sn4 O12 21.2(3) . . . . ?
Sn2 Pt3 Sn4 O12 -173.0(3) . . . . ?
Pt4 Pt3 Sn4 O12 85.4(3) . . . . ?
Pt2 Pt3 Sn4 O12 124.1(3) . . . . ?
Pt5 Pt3 Sn4 O12 158.2(3) . . . . ?
Pt1 Pt3 Sn4 O12 60.3(3) . . . . ?
Sn1 Pt3 Sn4 O12 104.7(4) . . . . ?
C3 Pt3 Sn4 Cl7 19.3(5) . . . . ?
Sn3 Pt3 Sn4 Cl7 113.52(19) . . . . ?
Sn2 Pt3 Sn4 Cl7 -80.71(19) . . . . ?
Pt4 Pt3 Sn4 Cl7 177.68(19) . . . . ?
Pt2 Pt3 Sn4 Cl7 -143.65(19) . . . . ?
Pt5 Pt3 Sn4 Cl7 -109.48(19) . . . . ?
Pt1 Pt3 Sn4 Cl7 152.62(19) . . . . ?
Sn1 Pt3 Sn4 Cl7 -163.0(2) . . . . ?
C3 Pt3 Sn4 Cl8 -147.6(7) . . . . ?
Sn3 Pt3 Sn4 Cl8 -53.4(5) . . . . ?
Sn2 Pt3 Sn4 Cl8 112.4(5) . . . . ?
Pt4 Pt3 Sn4 Cl8 10.8(5) . . . . ?
Pt2 Pt3 Sn4 Cl8 49.4(5) . . . . ?
Pt5 Pt3 Sn4 Cl8 83.6(5) . . . . ?
Pt1 Pt3 Sn4 Cl8 -14.3(5) . . . . ?
Sn1 Pt3 Sn4 Cl8 30.1(5) . . . . ?
C3 Pt3 Sn4 Pt5 128.8(5) . . . . ?
Sn3 Pt3 Sn4 Pt5 -137.00(4) . . . . ?
Sn2 Pt3 Sn4 Pt5 28.77(4) . . . . ?
Pt4 Pt3 Sn4 Pt5 -72.84(3) . . . . ?
Pt2 Pt3 Sn4 Pt5 -34.18(3) . . . . ?
Pt1 Pt3 Sn4 Pt5 -97.90(4) . . . . ?
Sn1 Pt3 Sn4 Pt5 -53.53(17) . . . . ?
C3 Pt3 Sn4 Pt4 -158.4(5) . . . . ?
Sn3 Pt3 Sn4 Pt4 -64.16(3) . . . . ?
Sn2 Pt3 Sn4 Pt4 101.61(4) . . . . ?
Pt2 Pt3 Sn4 Pt4 38.67(3) . . . . ?
Pt5 Pt3 Sn4 Pt4 72.84(3) . . . . ?
Pt1 Pt3 Sn4 Pt4 -25.06(4) . . . . ?
Sn1 Pt3 Sn4 Pt4 19.31(17) . . . . ?
C1 Pt1 Sn5 O13 166.7(8) . . . . ?
Sn1 Pt1 Sn5 O13 -75.9(5) . . . . ?
Sn3 Pt1 Sn5 O13 59.1(5) . . . . ?
Pt2 Pt1 Sn5 O13 -41.4(5) . . . . ?
Pt3 Pt1 Sn5 O13 -7.6(5) . . . . ?
Pt4 Pt1 Sn5 O13 27.2(5) . . . . ?
C1 Pt1 Sn5 Cl10 44.1(6) . . . . ?
Sn1 Pt1 Sn5 Cl10 161.46(15) . . . . ?
Sn3 Pt1 Sn5 Cl10 -63.54(15) . . . . ?
Pt2 Pt1 Sn5 Cl10 -163.98(15) . . . . ?
Pt3 Pt1 Sn5 Cl10 -130.18(15) . . . . ?
Pt4 Pt1 Sn5 Cl10 -95.43(15) . . . . ?
C1 Pt1 Sn5 Cl9 -60.8(6) . . . . ?
Sn1 Pt1 Sn5 Cl9 56.54(17) . . . . ?
Sn3 Pt1 Sn5 Cl9 -168.47(16) . . . . ?
Pt2 Pt1 Sn5 Cl9 91.09(16) . . . . ?
Pt3 Pt1 Sn5 Cl9 124.90(16) . . . . ?
Pt4 Pt1 Sn5 Cl9 159.64(17) . . . . ?
C1 Pt1 Sn5 Pt2 -151.9(6) . . . . ?
Sn1 Pt1 Sn5 Pt2 -34.55(4) . . . . ?
Sn3 Pt1 Sn5 Pt2 100.44(4) . . . . ?
Pt3 Pt1 Sn5 Pt2 33.81(3) . . . . ?
Pt4 Pt1 Sn5 Pt2 68.56(3) . . . . ?
C1 Pt1 Sn5 Pt4 139.5(6) . . . . ?
Sn1 Pt1 Sn5 Pt4 -103.11(4) . . . . ?
Sn3 Pt1 Sn5 Pt4 31.89(4) . . . . ?
Pt2 Pt1 Sn5 Pt4 -68.56(3) . . . . ?
Pt3 Pt1 Sn5 Pt4 -34.75(3) . . . . ?
C2 Pt2 Sn5 O13 -77.0(7) . . . . ?
Pt4 Pt2 Sn5 O13 82.3(3) . . . . ?
Sn1 Pt2 Sn5 O13 -175.6(3) . . . . ?
Pt1 Pt2 Sn5 O13 154.6(3) . . . . ?
Pt3 Pt2 Sn5 O13 121.1(3) . . . . ?
Sn2 Pt2 Sn5 O13 105.8(4) . . . . ?
Pt5 Pt2 Sn5 O13 56.4(3) . . . . ?
Sn6 Pt2 Sn5 O13 20.5(3) . . . . ?
C2 Pt2 Sn5 Cl10 -169.4(8) . . . . ?
Pt4 Pt2 Sn5 Cl10 -10.0(5) . . . . ?
Sn1 Pt2 Sn5 Cl10 92.1(5) . . . . ?
Pt1 Pt2 Sn5 Cl10 62.3(5) . . . . ?
Pt3 Pt2 Sn5 Cl10 28.8(5) . . . . ?
Sn2 Pt2 Sn5 Cl10 13.4(5) . . . . ?
Pt5 Pt2 Sn5 Cl10 -36.0(5) . . . . ?
Sn6 Pt2 Sn5 Cl10 -71.9(5) . . . . ?
C2 Pt2 Sn5 Cl9 12.2(6) . . . . ?
Pt4 Pt2 Sn5 Cl9 171.56(13) . . . . ?
Sn1 Pt2 Sn5 Cl9 -86.31(13) . . . . ?
Pt1 Pt2 Sn5 Cl9 -116.15(13) . . . . ?
Pt3 Pt2 Sn5 Cl9 -149.64(13) . . . . ?
Sn2 Pt2 Sn5 Cl9 -165.0(2) . . . . ?
Pt5 Pt2 Sn5 Cl9 145.61(13) . . . . ?
Sn6 Pt2 Sn5 Cl9 109.71(13) . . . . ?
C2 Pt2 Sn5 Pt1 128.4(6) . . . . ?
Pt4 Pt2 Sn5 Pt1 -72.30(3) . . . . ?
Sn1 Pt2 Sn5 Pt1 29.84(4) . . . . ?
Pt3 Pt2 Sn5 Pt1 -33.49(3) . . . . ?
Sn2 Pt2 Sn5 Pt1 -48.83(19) . . . . ?
Pt5 Pt2 Sn5 Pt1 -98.25(4) . . . . ?
Sn6 Pt2 Sn5 Pt1 -134.14(4) . . . . ?
C2 Pt2 Sn5 Pt4 -159.3(6) . . . . ?
Sn1 Pt2 Sn5 Pt4 102.14(4) . . . . ?
Pt1 Pt2 Sn5 Pt4 72.30(3) . . . . ?
Pt3 Pt2 Sn5 Pt4 38.81(3) . . . . ?
Sn2 Pt2 Sn5 Pt4 23.47(19) . . . . ?
Pt5 Pt2 Sn5 Pt4 -25.95(3) . . . . ?
Sn6 Pt2 Sn5 Pt4 -61.85(3) . . . . ?
C4 Pt4 Sn5 O13 70.7(6) . . . . ?
Sn6 Pt4 Sn5 O13 -22.8(3) . . . . ?
Sn3 Pt4 Sn5 O13 169.6(3) . . . . ?
Pt2 Pt4 Sn5 O13 -89.7(3) . . . . ?
Pt3 Pt4 Sn5 O13 -128.4(3) . . . . ?
Sn4 Pt4 Sn5 O13 -105.8(4) . . . . ?
Pt5 Pt4 Sn5 O13 -64.1(3) . . . . ?
Pt1 Pt4 Sn5 O13 -162.6(3) . . . . ?
C4 Pt4 Sn5 Cl10 -22.6(5) . . . . ?
Sn6 Pt4 Sn5 Cl10 -116.08(14) . . . . ?
Sn3 Pt4 Sn5 Cl10 76.28(14) . . . . ?
Pt2 Pt4 Sn5 Cl10 176.97(14) . . . . ?
Pt3 Pt4 Sn5 Cl10 138.34(14) . . . . ?
Sn4 Pt4 Sn5 Cl10 160.9(2) . . . . ?
Pt5 Pt4 Sn5 Cl10 -157.45(14) . . . . ?
Pt1 Pt4 Sn5 Cl10 104.08(14) . . . . ?
C4 Pt4 Sn5 Cl9 132.9(6) . . . . ?
Sn6 Pt4 Sn5 Cl9 39.4(4) . . . . ?
Sn3 Pt4 Sn5 Cl9 -128.2(4) . . . . ?
Pt2 Pt4 Sn5 Cl9 -27.5(4) . . . . ?
Pt3 Pt4 Sn5 Cl9 -66.2(4) . . . . ?
Sn4 Pt4 Sn5 Cl9 -43.6(4) . . . . ?
Pt5 Pt4 Sn5 Cl9 -2.0(4) . . . . ?
Pt1 Pt4 Sn5 Cl9 -100.4(4) . . . . ?
C4 Pt4 Sn5 Pt1 -126.7(5) . . . . ?
Sn6 Pt4 Sn5 Pt1 139.84(4) . . . . ?
Sn3 Pt4 Sn5 Pt1 -27.80(4) . . . . ?
Pt2 Pt4 Sn5 Pt1 72.88(3) . . . . ?
Pt3 Pt4 Sn5 Pt1 34.26(3) . . . . ?
Sn4 Pt4 Sn5 Pt1 56.80(18) . . . . ?
Pt5 Pt4 Sn5 Pt1 98.47(4) . . . . ?
C4 Pt4 Sn5 Pt2 160.4(5) . . . . ?
Sn6 Pt4 Sn5 Pt2 66.95(4) . . . . ?
Sn3 Pt4 Sn5 Pt2 -100.68(4) . . . . ?
Pt3 Pt4 Sn5 Pt2 -38.62(3) . . . . ?
Sn4 Pt4 Sn5 Pt2 -16.08(18) . . . . ?
Pt5 Pt4 Sn5 Pt2 25.59(3) . . . . ?
Pt1 Pt4 Sn5 Pt2 -72.88(3) . . . . ?
C5 Pt5 Sn6 O13 173.8(8) . . . . ?
Sn4 Pt5 Sn6 O13 -73.9(5) . . . . ?
Sn2 Pt5 Sn6 O13 61.4(5) . . . . ?
Pt3 Pt5 Sn6 O13 -6.3(5) . . . . ?
Pt4 Pt5 Sn6 O13 -37.7(5) . . . . ?
Pt2 Pt5 Sn6 O13 30.3(5) . . . . ?
C5 Pt5 Sn6 Cl12 -56.4(6) . . . . ?
Sn4 Pt5 Sn6 Cl12 55.85(17) . . . . ?
Sn2 Pt5 Sn6 Cl12 -168.82(16) . . . . ?
Pt3 Pt5 Sn6 Cl12 123.53(16) . . . . ?
Pt4 Pt5 Sn6 Cl12 92.07(16) . . . . ?
Pt2 Pt5 Sn6 Cl12 160.09(16) . . . . ?
C5 Pt5 Sn6 Cl11 46.1(6) . . . . ?
Sn4 Pt5 Sn6 Cl11 158.29(15) . . . . ?
Sn2 Pt5 Sn6 Cl11 -66.38(16) . . . . ?
Pt3 Pt5 Sn6 Cl11 -134.03(15) . . . . ?
Pt4 Pt5 Sn6 Cl11 -165.49(16) . . . . ?
Pt2 Pt5 Sn6 Cl11 -97.46(15) . . . . ?
C5 Pt5 Sn6 Pt4 -148.4(6) . . . . ?
Sn4 Pt5 Sn6 Pt4 -36.22(4) . . . . ?
Sn2 Pt5 Sn6 Pt4 99.11(5) . . . . ?
Pt3 Pt5 Sn6 Pt4 31.46(4) . . . . ?
Pt2 Pt5 Sn6 Pt4 68.02(3) . . . . ?
C5 Pt5 Sn6 Pt2 143.5(6) . . . . ?
Sn4 Pt5 Sn6 Pt2 -104.24(4) . . . . ?
Sn2 Pt5 Sn6 Pt2 31.09(5) . . . . ?
Pt3 Pt5 Sn6 Pt2 -36.56(3) . . . . ?
Pt4 Pt5 Sn6 Pt2 -68.02(3) . . . . ?
C4 Pt4 Sn6 O13 -71.8(6) . . . . ?
Sn3 Pt4 Sn6 O13 111.5(4) . . . . ?
Pt2 Pt4 Sn6 O13 85.3(3) . . . . ?
Pt3 Pt4 Sn6 O13 125.5(3) . . . . ?
Sn4 Pt4 Sn6 O13 -171.3(3) . . . . ?
Pt5 Pt4 Sn6 O13 156.6(3) . . . . ?
Sn5 Pt4 Sn6 O13 23.0(3) . . . . ?
Pt1 Pt4 Sn6 O13 59.8(3) . . . . ?
C4 Pt4 Sn6 Cl12 21.0(6) . . . . ?
Sn3 Pt4 Sn6 Cl12 -155.7(2) . . . . ?
Pt2 Pt4 Sn6 Cl12 178.15(15) . . . . ?
Pt3 Pt4 Sn6 Cl12 -141.69(15) . . . . ?
Sn4 Pt4 Sn6 Cl12 -78.45(15) . . . . ?
Pt5 Pt4 Sn6 Cl12 -110.57(15) . . . . ?
Sn5 Pt4 Sn6 Cl12 115.86(15) . . . . ?
Pt1 Pt4 Sn6 Cl12 152.61(15) . . . . ?
C4 Pt4 Sn6 Cl11 -150.9(8) . . . . ?
Sn3 Pt4 Sn6 Cl11 32.3(7) . . . . ?
Pt2 Pt4 Sn6 Cl11 6.2(6) . . . . ?
Pt3 Pt4 Sn6 Cl11 46.4(7) . . . . ?
Sn4 Pt4 Sn6 Cl11 109.6(6) . . . . ?
Pt5 Pt4 Sn6 Cl11 77.5(6) . . . . ?
Sn5 Pt4 Sn6 Cl11 -56.1(6) . . . . ?
Pt1 Pt4 Sn6 Cl11 -19.3(7) . . . . ?
C4 Pt4 Sn6 Pt5 131.6(5) . . . . ?
Sn3 Pt4 Sn6 Pt5 -45.1(2) . . . . ?
Pt2 Pt4 Sn6 Pt5 -71.28(3) . . . . ?
Pt3 Pt4 Sn6 Pt5 -31.12(4) . . . . ?
Sn4 Pt4 Sn6 Pt5 32.12(4) . . . . ?
Sn5 Pt4 Sn6 Pt5 -133.57(4) . . . . ?
Pt1 Pt4 Sn6 Pt5 -96.82(4) . . . . ?
C4 Pt4 Sn6 Pt2 -157.1(5) . . . . ?
Sn3 Pt4 Sn6 Pt2 26.1(2) . . . . ?
Pt3 Pt4 Sn6 Pt2 40.16(3) . . . . ?
Sn4 Pt4 Sn6 Pt2 103.40(4) . . . . ?
Pt5 Pt4 Sn6 Pt2 71.28(3) . . . . ?
Sn5 Pt4 Sn6 Pt2 -62.29(3) . . . . ?
Pt1 Pt4 Sn6 Pt2 -25.54(3) . . . . ?
C2 Pt2 Sn6 O13 72.4(6) . . . . ?
Sn5 Pt2 Sn6 O13 -20.9(3) . . . . ?
Pt4 Pt2 Sn6 O13 -86.8(3) . . . . ?
Sn1 Pt2 Sn6 O13 -104.7(4) . . . . ?
Pt1 Pt2 Sn6 O13 -61.8(3) . . . . ?
Pt3 Pt2 Sn6 O13 -125.8(3) . . . . ?
Sn2 Pt2 Sn6 O13 172.8(3) . . . . ?
Pt5 Pt2 Sn6 O13 -160.8(3) . . . . ?
C2 Pt2 Sn6 Cl12 153.5(7) . . . . ?
Sn5 Pt2 Sn6 Cl12 60.2(5) . . . . ?
Pt4 Pt2 Sn6 Cl12 -5.7(5) . . . . ?
Sn1 Pt2 Sn6 Cl12 -23.6(5) . . . . ?
Pt1 Pt2 Sn6 Cl12 19.3(5) . . . . ?
Pt3 Pt2 Sn6 Cl12 -44.6(5) . . . . ?
Sn2 Pt2 Sn6 Cl12 -106.0(5) . . . . ?
Pt5 Pt2 Sn6 Cl12 -79.7(5) . . . . ?
C2 Pt2 Sn6 Cl11 -19.2(6) . . . . ?
Sn5 Pt2 Sn6 Cl11 -112.56(16) . . . . ?
Pt4 Pt2 Sn6 Cl11 -178.47(16) . . . . ?
Sn1 Pt2 Sn6 Cl11 163.7(2) . . . . ?
Pt1 Pt2 Sn6 Cl11 -153.46(15) . . . . ?
Pt3 Pt2 Sn6 Cl11 142.60(15) . . . . ?
Sn2 Pt2 Sn6 Cl11 81.19(16) . . . . ?
Pt5 Pt2 Sn6 Cl11 107.52(16) . . . . ?
C2 Pt2 Sn6 Pt5 -126.7(6) . . . . ?
Sn5 Pt2 Sn6 Pt5 139.91(4) . . . . ?
Pt4 Pt2 Sn6 Pt5 74.01(3) . . . . ?
Sn1 Pt2 Sn6 Pt5 56.13(16) . . . . ?
Pt1 Pt2 Sn6 Pt5 99.01(4) . . . . ?
Pt3 Pt2 Sn6 Pt5 35.08(3) . . . . ?
Sn2 Pt2 Sn6 Pt5 -26.33(4) . . . . ?
C2 Pt2 Sn6 Pt4 159.3(6) . . . . ?
Sn5 Pt2 Sn6 Pt4 65.91(4) . . . . ?
Sn1 Pt2 Sn6 Pt4 -17.88(16) . . . . ?
Pt1 Pt2 Sn6 Pt4 25.01(3) . . . . ?
Pt3 Pt2 Sn6 Pt4 -38.93(3) . . . . ?
Sn2 Pt2 Sn6 Pt4 -100.33(4) . . . . ?
Pt5 Pt2 Sn6 Pt4 -74.01(3) . . . . ?
Cl3 Sn2 O11 C11 49.7(14) . . . . ?
Cl4 Sn2 O11 C11 -44.2(14) . . . . ?
Pt5 Sn2 O11 C11 -178.4(12) . . . . ?
Pt3 Sn2 O11 C11 -148.6(14) . . . . ?
Pt2 Sn2 O11 C11 150.7(14) . . . . ?
Cl3 Sn2 O11 Sn1 -129.3(5) . . . . ?
Cl4 Sn2 O11 Sn1 136.8(4) . . . . ?
Pt5 Sn2 O11 Sn1 2.6(8) . . . . ?
Pt3 Sn2 O11 Sn1 32.4(4) . . . . ?
Pt2 Sn2 O11 Sn1 -28.3(4) . . . . ?
Cl2 Sn1 O11 C11 -48.4(14) . . . . ?
Cl1 Sn1 O11 C11 44.1(13) . . . . ?
Pt1 Sn1 O11 C11 176.4(11) . . . . ?
Pt2 Sn1 O11 C11 -150.7(13) . . . . ?
Pt3 Sn1 O11 C11 149.2(14) . . . . ?
Cl2 Sn1 O11 Sn2 130.6(4) . . . . ?
Cl1 Sn1 O11 Sn2 -136.8(4) . . . . ?
Pt1 Sn1 O11 Sn2 -4.6(8) . . . . ?
Pt2 Sn1 O11 Sn2 28.4(4) . . . . ?
Pt3 Sn1 O11 Sn2 -31.8(4) . . . . ?
Cl6 Sn3 O12 C12 40.4(15) . . . . ?
Cl5 Sn3 O12 C12 -52.9(15) . . . . ?
Pt1 Sn3 O12 C12 171.3(13) . . . . ?
Pt3 Sn3 O12 C12 -156.3(15) . . . . ?
Pt4 Sn3 O12 C12 142.9(15) . . . . ?
Cl6 Sn3 O12 Sn4 -133.5(4) . . . . ?
Cl5 Sn3 O12 Sn4 133.1(4) . . . . ?
Pt1 Sn3 O12 Sn4 -2.7(8) . . . . ?
Pt3 Sn3 O12 Sn4 29.7(4) . . . . ?
Pt4 Sn3 O12 Sn4 -31.1(4) . . . . ?
Cl7 Sn4 O12 C12 52.0(15) . . . . ?
Cl8 Sn4 O12 C12 -40.4(15) . . . . ?
Pt5 Sn4 O12 C12 -173.4(13) . . . . ?
Pt4 Sn4 O12 C12 -143.1(15) . . . . ?
Pt3 Sn4 O12 C12 156.7(15) . . . . ?
Cl7 Sn4 O12 Sn3 -133.9(5) . . . . ?
Cl8 Sn4 O12 Sn3 133.7(4) . . . . ?
Pt5 Sn4 O12 Sn3 0.7(8) . . . . ?
Pt4 Sn4 O12 Sn3 31.0(4) . . . . ?
Pt3 Sn4 O12 Sn3 -29.2(4) . . . . ?
Cl12 Sn6 O13 C13 53.9(15) . . . . ?
Cl11 Sn6 O13 C13 -37.8(15) . . . . ?
Pt5 Sn6 O13 C13 -171.0(13) . . . . ?
Pt4 Sn6 O13 C13 155.7(15) . . . . ?
Pt2 Sn6 O13 C13 -144.4(15) . . . . ?
Cl12 Sn6 O13 Sn5 -133.8(5) . . . . ?
Cl11 Sn6 O13 Sn5 134.6(5) . . . . ?
Pt5 Sn6 O13 Sn5 1.4(9) . . . . ?
Pt4 Sn6 O13 Sn5 -32.0(4) . . . . ?
Pt2 Sn6 O13 Sn5 27.9(4) . . . . ?
Cl10 Sn5 O13 C13 -54.3(15) . . . . ?
Cl9 Sn5 O13 C13 39.2(15) . . . . ?
Pt1 Sn5 O13 C13 179.2(13) . . . . ?
Pt2 Sn5 O13 C13 143.0(15) . . . . ?
Pt4 Sn5 O13 C13 -156.6(15) . . . . ?
Cl10 Sn5 O13 Sn6 133.5(5) . . . . ?
Cl9 Sn5 O13 Sn6 -133.0(5) . . . . ?
Pt1 Sn5 O13 Sn6 7.0(8) . . . . ?
Pt2 Sn5 O13 Sn6 -29.2(4) . . . . ?
Pt4 Sn5 O13 Sn6 31.2(4) . . . . ?
Sn1 Pt1 C1 O1 -53(83) . . . . ?
Sn3 Pt1 C1 O1 -173(100) . . . . ?
Sn5 Pt1 C1 O1 68(83) . . . . ?
Pt2 Pt1 C1 O1 11(83) . . . . ?
Pt3 Pt1 C1 O1 -121(82) . . . . ?
Pt4 Pt1 C1 O1 132(82) . . . . ?
Sn5 Pt2 C2 O2 93(100) . . . . ?
Pt4 Pt2 C2 O2 55(100) . . . . ?
Sn1 Pt2 C2 O2 -162(100) . . . . ?
Pt1 Pt2 C2 O2 146(100) . . . . ?
Pt3 Pt2 C2 O2 -124(100) . . . . ?
Sn2 Pt2 C2 O2 -87(100) . . . . ?
Pt5 Pt2 C2 O2 -34(100) . . . . ?
Sn6 Pt2 C2 O2 19(100) . . . . ?
Sn3 Pt3 C3 O3 170(100) . . . . ?
Sn2 Pt3 C3 O3 -9(39) . . . . ?
Pt4 Pt3 C3 O3 -154(38) . . . . ?
Pt2 Pt3 C3 O3 30(39) . . . . ?
Pt5 Pt3 C3 O3 -63(39) . . . . ?
Sn4 Pt3 C3 O3 -115(39) . . . . ?
Pt1 Pt3 C3 O3 117(39) . . . . ?
Sn1 Pt3 C3 O3 65(39) . . . . ?
Sn6 Pt4 C4 O4 156(29) . . . . ?
Sn3 Pt4 C4 O4 -25(29) . . . . ?
Pt2 Pt4 C4 O4 114(29) . . . . ?
Pt3 Pt4 C4 O4 -59(30) . . . . ?
Sn4 Pt4 C4 O4 -100(29) . . . . ?
Pt5 Pt4 C4 O4 -153(29) . . . . ?
Sn5 Pt4 C4 O4 81(29) . . . . ?
Pt1 Pt4 C4 O4 28(29) . . . . ?
Sn6 Pt5 C5 O5 -78(43) . . . . ?
Sn4 Pt5 C5 O5 166(43) . . . . ?
Sn2 Pt5 C5 O5 44(43) . . . . ?
Pt3 Pt5 C5 O5 102(43) . . . . ?
Pt4 Pt5 C5 O5 -130(42) . . . . ?
Pt2 Pt5 C5 O5 -18(44) . . . . ?
C113 P1 C101 C102 -79.4(9) . . . . ?
C119 P1 C101 C102 42.4(9) . . . . ?
C107 P1 C101 C102 165.1(8) . . . . ?
C113 P1 C101 C106 93.4(10) . . . . ?
C119 P1 C101 C106 -144.8(8) . . . . ?
C107 P1 C101 C106 -22.0(11) . . . . ?
C106 C101 C102 C103 0.0 . . . . ?
P1 C101 C102 C103 172.9(11) . . . . ?
C101 C102 C103 C104 0.0 . . . . ?
C102 C103 C104 C105 0.0 . . . . ?
C103 C104 C105 C106 0.0 . . . . ?
C104 C105 C106 C101 0.0 . . . . ?
C102 C101 C106 C105 0.0 . . . . ?
P1 C101 C106 C105 -172.7(11) . . . . ?
C113 P1 C107 C108 -38.3(10) . . . . ?
C119 P1 C107 C108 -157.4(8) . . . . ?
C101 P1 C107 C108 81.7(10) . . . . ?
C113 P1 C107 C112 137.4(9) . . . . ?
C119 P1 C107 C112 18.3(10) . . . . ?
C101 P1 C107 C112 -102.6(9) . . . . ?
C112 C107 C108 C109 0.0 . . . . ?
P1 C107 C108 C109 175.7(10) . . . . ?
C107 C108 C109 C110 0.0 . . . . ?
C108 C109 C110 C111 0.0 . . . . ?
C109 C110 C111 C112 0.0 . . . . ?
C110 C111 C112 C107 0.0 . . . . ?
C108 C107 C112 C111 0.0 . . . . ?
P1 C107 C112 C111 -175.7(10) . . . . ?
C119 P1 C113 C114 69.9(10) . . . . ?
C101 P1 C113 C114 -170.4(8) . . . . ?
C107 P1 C113 C114 -48.9(10) . . . . ?
C119 P1 C113 C118 -109.3(9) . . . . ?
C101 P1 C113 C118 10.4(10) . . . . ?
C107 P1 C113 C118 131.9(9) . . . . ?
C118 C113 C114 C115 0.0 . . . . ?
P1 C113 C114 C115 -179.2(12) . . . . ?
C113 C114 C115 C116 0.0 . . . . ?
C114 C115 C116 C117 0.0 . . . . ?
C115 C116 C117 C118 0.0 . . . . ?
C116 C117 C118 C113 0.0 . . . . ?
C114 C113 C118 C117 0.0 . . . . ?
P1 C113 C118 C117 179.2(12) . . . . ?
C113 P1 C119 C120 -7.6(10) . . . . ?
C101 P1 C119 C120 -129.3(7) . . . . ?
C107 P1 C119 C120 106.5(8) . . . . ?
C113 P1 C119 C124 172.4(7) . . . . ?
C101 P1 C119 C124 50.7(8) . . . . ?
C107 P1 C119 C124 -73.4(8) . . . . ?
C124 C119 C120 C121 0.0 . . . . ?
P1 C119 C120 C121 -179.9(9) . . . . ?
C119 C120 C121 C122 0.0 . . . . ?
C120 C121 C122 C123 0.0 . . . . ?
C121 C122 C123 C124 0.0 . . . . ?
C122 C123 C124 C119 0.0 . . . . ?
C120 C119 C124 C123 0.0 . . . . ?
P1 C119 C124 C123 179.9(9) . . . . ?
C219 P2 C201 C202 95.8(11) . . . . ?
C207 P2 C201 C202 -139.2(9) . . . . ?
C213 P2 C201 C202 -22.4(10) . . . . ?
C219 P2 C201 C206 -75.9(11) . . . . ?
C207 P2 C201 C206 49.2(11) . . . . ?
C213 P2 C201 C206 166.0(9) . . . . ?
C206 C201 C202 C203 0.0 . . . . ?
P2 C201 C202 C203 -171.7(11) . . . . ?
C201 C202 C203 C204 0.0 . . . . ?
C202 C203 C204 C205 0.0 . . . . ?
C203 C204 C205 C206 0.0 . . . . ?
C204 C205 C206 C201 0.0 . . . . ?
C202 C201 C206 C205 0.0 . . . . ?
P2 C201 C206 C205 171.6(11) . . . . ?
C201 P2 C207 C208 21.5(12) . . . . ?
C219 P2 C207 C208 146.2(11) . . . . ?
C213 P2 C207 C208 -94.4(10) . . . . ?
C201 P2 C207 C212 -153.8(10) . . . . ?
C219 P2 C207 C212 -29.2(13) . . . . ?
C213 P2 C207 C212 90.2(11) . . . . ?
C212 C207 C208 C209 0.0 . . . . ?
P2 C207 C208 C209 -175.3(13) . . . . ?
C207 C208 C209 C210 0.0 . . . . ?
C208 C209 C210 C211 0.0 . . . . ?
C209 C210 C211 C212 0.0 . . . . ?
C210 C211 C212 C207 0.0 . . . . ?
C208 C207 C212 C211 0.0 . . . . ?
P2 C207 C212 C211 175.3(13) . . . . ?
C201 P2 C213 C214 -81.5(9) . . . . ?
C219 P2 C213 C214 158.3(9) . . . . ?
C207 P2 C213 C214 36.4(10) . . . . ?
C201 P2 C213 C218 99.2(10) . . . . ?
C219 P2 C213 C218 -21.1(11) . . . . ?
C207 P2 C213 C218 -142.9(9) . . . . ?
C218 C213 C214 C215 0.0 . . . . ?
P2 C213 C214 C215 -179.4(10) . . . . ?
C213 C214 C215 C216 0.0 . . . . ?
C214 C215 C216 C217 0.0 . . . . ?
C215 C216 C217 C218 0.0 . . . . ?
C216 C217 C218 C213 0.0 . . . . ?
C214 C213 C218 C217 0.0 . . . . ?
P2 C213 C218 C217 179.3(11) . . . . ?
C201 P2 C219 C220 -173.7(10) . . . . ?
C207 P2 C219 C220 62.6(13) . . . . ?
C213 P2 C219 C220 -56.7(12) . . . . ?
C201 P2 C219 C224 11.9(12) . . . . ?
C207 P2 C219 C224 -111.7(11) . . . . ?
C213 P2 C219 C224 129.0(9) . . . . ?
C224 C219 C220 C221 0.0 . . . . ?
P2 C219 C220 C221 -174.1(14) . . . . ?
C219 C220 C221 C222 0.0 . . . . ?
C220 C221 C222 C223 0.0 . . . . ?
C221 C222 C223 C224 0.0 . . . . ?
C222 C223 C224 C219 0.0 . . . . ?
C220 C219 C224 C223 0.0 . . . . ?
P2 C219 C224 C223 174.5(13) . . . . ?
C307 P3 C301 C302 -44.0(9) . . . . ?
C313 P3 C301 C302 -164.6(8) . . . . ?
C319 P3 C301 C302 76.9(9) . . . . ?
C307 P3 C301 C306 141.6(8) . . . . ?
C313 P3 C301 C306 21.0(10) . . . . ?
C319 P3 C301 C306 -97.5(9) . . . . ?
C306 C301 C302 C303 0.0 . . . . ?
P3 C301 C302 C303 -174.5(10) . . . . ?
C301 C302 C303 C304 0.0 . . . . ?
C302 C303 C304 C305 0.0 . . . . ?
C303 C304 C305 C306 0.0 . . . . ?
C304 C305 C306 C301 0.0 . . . . ?
C302 C301 C306 C305 0.0 . . . . ?
P3 C301 C306 C305 174.3(10) . . . . ?
C301 P3 C307 C308 130.8(9) . . . . ?
C313 P3 C307 C308 -109.9(9) . . . . ?
C319 P3 C307 C308 9.8(11) . . . . ?
C301 P3 C307 C312 -46.7(10) . . . . ?
C313 P3 C307 C312 72.6(10) . . . . ?
C319 P3 C307 C312 -167.7(8) . . . . ?
C312 C307 C308 C309 0.0 . . . . ?
P3 C307 C308 C309 -177.5(12) . . . . ?
C307 C308 C309 C310 0.0 . . . . ?
C308 C309 C310 C311 0.0 . . . . ?
C309 C310 C311 C312 0.0 . . . . ?
C310 C311 C312 C307 0.0 . . . . ?
C308 C307 C312 C311 0.0 . . . . ?
P3 C307 C312 C311 177.5(12) . . . . ?
C307 P3 C313 C314 -24.4(11) . . . . ?
C301 P3 C313 C314 91.9(9) . . . . ?
C319 P3 C313 C314 -146.7(8) . . . . ?
C307 P3 C313 C318 158.0(8) . . . . ?
C301 P3 C313 C318 -85.7(9) . . . . ?
C319 P3 C313 C318 35.7(10) . . . . ?
C318 C313 C314 C315 0.0 . . . . ?
P3 C313 C314 C315 -177.6(11) . . . . ?
C313 C314 C315 C316 0.0 . . . . ?
C314 C315 C316 C317 0.0 . . . . ?
C315 C316 C317 C318 0.0 . . . . ?
C316 C317 C318 C313 0.0 . . . . ?
C314 C313 C318 C317 0.0 . . . . ?
P3 C313 C318 C317 177.6(10) . . . . ?
C307 P3 C319 C320 -72.4(10) . . . . ?
C301 P3 C319 C320 170.6(8) . . . . ?
C313 P3 C319 C320 50.3(10) . . . . ?
C307 P3 C319 C324 105.5(9) . . . . ?
C301 P3 C319 C324 -11.5(11) . . . . ?
C313 P3 C319 C324 -131.8(9) . . . . ?
C324 C319 C320 C321 0.0 . . . . ?
P3 C319 C320 C321 177.9(10) . . . . ?
C319 C320 C321 C322 0.0 . . . . ?
C320 C321 C322 C323 0.0 . . . . ?
C321 C322 C323 C324 0.0 . . . . ?
C322 C323 C324 C319 0.0 . . . . ?
C320 C319 C324 C323 0.0 . . . . ?
P3 C319 C324 C323 -177.9(11) . . . . ?

_diffrn_measured_fraction_theta_max 1.000
_diffrn_reflns_theta_full        25.03
_diffrn_measured_fraction_theta_full 1.000
_refine_diff_density_max         1.560
_refine_diff_density_min         -2.461
_refine_diff_density_rms         0.237
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_3_6MeCN
_database_code_depnum_ccdc_archive 'CCDC 1439438'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C114 H98 Cl16 N6 O6 P4 Pt6 Sn6'
_chemical_formula_weight         4221.74

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Triclinic
_symmetry_space_group_name_H-M   P-1

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   13.2558(12)
_cell_length_b                   15.6328(14)
_cell_length_c                   18.5341(17)
_cell_angle_alpha                69.384(5)
_cell_angle_beta                 69.584(5)
_cell_angle_gamma                85.050(5)
_cell_volume                     3366.0(5)
_cell_formula_units_Z            1
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    9777
_cell_measurement_theta_min      2.168
_cell_measurement_theta_max      25.015

_exptl_crystal_description       prism
_exptl_crystal_colour            black
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.10
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.083
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1972
_exptl_absorpt_coefficient_mu    7.713
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.3716
_exptl_absorpt_correction_T_max  0.5126
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1822 (selected reflections only, before parameter refinement)
 R(int) = 0.0865 (selected reflections only, after parameter refinement)
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            46912
_diffrn_reflns_av_R_equivalents  0.1013
_diffrn_reflns_av_unetI/netI     0.1063
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_theta_min         1.39
_diffrn_reflns_theta_max         25.03
_reflns_number_total             11887
_reflns_number_gt                8825
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. The following restraints
 were applied (given as SHELXL lines): 
 isor .02 cl3 cl6 cl7 o1 o2 c103 c104 c120 c121 c122 c123 c124
 isor .02 c203 c204 c205 c220 c221 c222 c223
 simu c101 > c124
 simu c201 > c224
 same n2 > c402
 same n3 > c502
 simu n1 > c502
 AFIX 66 on all Ph rings
 The asymmetric unit of the unit cell contains one half of a cluster anion 
 (located on an inversion centre), two [PPh4]+ cations and three CH3CN 
 molecules (all located on general positions). Similar U restraints have 
 been applied to the [PPh4]+ cations and the CH3CN molecules (SIMU command 
 in SHELXL, s.u. 0.02). The C-atoms of the Ph-rings have been constrained 
 to fit regular hexagons (AFIX 66 command in SHELXL). The CH3CN molecules 
 have been refined isotropically and their geometries restrained to be 
 similar (SAME command in SHELXL, s.u. 0.02).
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0439P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         11887
_refine_ls_number_parameters     571
_refine_ls_number_restraints     417
_refine_ls_R_factor_all          0.0746
_refine_ls_R_factor_gt           0.0511
_refine_ls_wR_factor_ref         0.1421
_refine_ls_wR_factor_gt          0.1271
_refine_ls_goodness_of_fit_ref   1.024
_refine_ls_restrained_S_all      1.016
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.63880(3) 0.11543(2) 0.37318(2) 0.03661(12) Uani 1 1 d . . .
Pt2 Pt 0.44790(3) 0.07271(2) 0.51205(2) 0.03534(12) Uani 1 1 d . . .
Pt3 Pt 0.46669(3) 0.05129(2) 0.35950(3) 0.03828(13) Uani 1 1 d . . .
Sn1 Sn 0.66946(6) 0.06429(5) 0.51214(5) 0.0445(2) Uani 1 1 d . . .
Sn2 Sn 0.66530(6) -0.04252(5) 0.32732(5) 0.0430(2) Uani 1 1 d . . .
Sn3 Sn 0.56579(6) 0.21163(5) 0.24791(5) 0.0443(2) Uani 1 1 d . . .
Cl1 Cl 0.6860(3) 0.2002(2) 0.5382(2) 0.0721(9) Uani 1 1 d . . .
Cl2 Cl 0.8505(2) 0.0207(2) 0.5002(2) 0.0692(9) Uani 1 1 d . . .
Cl3 Cl 0.7432(3) 0.0440(2) 0.1845(2) 0.0850(12) Uani 1 1 d U . .
Cl4 Cl 0.6148(3) -0.1723(2) 0.3050(2) 0.0661(8) Uani 1 1 d . . .
Cl5 Cl 0.8347(3) -0.0980(2) 0.3404(3) 0.0792(11) Uani 1 1 d . . .
Cl6 Cl 0.4722(3) 0.3386(2) 0.2791(2) 0.0934(13) Uani 1 1 d U . .
Cl7 Cl 0.4935(3) 0.2297(3) 0.1410(2) 0.0928(13) Uani 1 1 d U . .
Cl8 Cl 0.7242(2) 0.2998(2) 0.15089(19) 0.0681(9) Uani 1 1 d . . .
C1 C 0.7718(10) 0.1800(8) 0.3219(7) 0.054(3) Uani 1 1 d . . .
C2 C 0.4036(9) 0.1932(8) 0.4957(7) 0.055(3) Uani 1 1 d . . .
C3 C 0.3923(9) 0.0307(8) 0.2958(8) 0.052(3) Uani 1 1 d . . .
O1 O 0.8528(8) 0.2169(7) 0.2925(7) 0.096(3) Uani 1 1 d U . .
O2 O 0.3775(8) 0.2669(6) 0.4835(6) 0.087(3) Uani 1 1 d U . .
O3 O 0.3517(7) 0.0156(7) 0.2582(6) 0.076(3) Uani 1 1 d . . .
P1 P 0.1667(3) 0.5150(2) 0.3037(2) 0.0539(8) Uani 1 1 d . . .
C101 C 0.0513(6) 0.5840(5) 0.3124(6) 0.068(4) Uani 1 1 d GU . .
C102 C 0.0143(8) 0.6208(6) 0.3748(5) 0.080(4) Uani 1 1 d GU . .
H102 H 0.0518 0.6121 0.4108 0.096 Uiso 1 1 calc R . .
C103 C -0.0786(8) 0.6706(6) 0.3834(6) 0.094(5) Uani 1 1 d GU . .
H103 H -0.1033 0.6952 0.4251 0.113 Uiso 1 1 calc R . .
C104 C -0.1345(7) 0.6835(6) 0.3296(7) 0.105(5) Uani 1 1 d GU . .
H104 H -0.1967 0.7168 0.3354 0.127 Uiso 1 1 calc R . .
C105 C -0.0975(8) 0.6467(7) 0.2672(7) 0.103(5) Uani 1 1 d GU . .
H105 H -0.1350 0.6554 0.2313 0.124 Uiso 1 1 calc R . .
C106 C -0.0046(8) 0.5970(6) 0.2586(5) 0.080(4) Uani 1 1 d GU . .
H106 H 0.0201 0.5724 0.2169 0.097 Uiso 1 1 calc R . .
C107 C 0.2333(6) 0.5301(5) 0.1990(4) 0.052(3) Uani 1 1 d GU . .
C108 C 0.2428(7) 0.6170(4) 0.1405(5) 0.070(4) Uani 1 1 d GU . .
H108 H 0.2119 0.6660 0.1564 0.084 Uiso 1 1 calc R . .
C109 C 0.2985(7) 0.6304(5) 0.0581(4) 0.072(4) Uani 1 1 d GU . .
H109 H 0.3049 0.6885 0.0190 0.087 Uiso 1 1 calc R . .
C110 C 0.3447(7) 0.5571(6) 0.0343(4) 0.082(4) Uani 1 1 d GU . .
H110 H 0.3820 0.5661 -0.0208 0.099 Uiso 1 1 calc R . .
C111 C 0.3352(7) 0.4702(5) 0.0928(5) 0.074(4) Uani 1 1 d GU . .
H111 H 0.3661 0.4212 0.0769 0.088 Uiso 1 1 calc R . .
C112 C 0.2795(7) 0.4567(4) 0.1751(5) 0.063(3) Uani 1 1 d GU . .
H112 H 0.2731 0.3986 0.2143 0.076 Uiso 1 1 calc R . .
C113 C 0.1214(6) 0.3981(4) 0.3605(5) 0.050(3) Uani 1 1 d GU . .
C114 C 0.0154(6) 0.3718(5) 0.3784(6) 0.072(4) Uani 1 1 d GU . .
H114 H -0.0323 0.4151 0.3622 0.087 Uiso 1 1 calc R . .
C115 C -0.0193(5) 0.2806(6) 0.4204(6) 0.083(4) Uani 1 1 d GU . .
H115 H -0.0902 0.2629 0.4324 0.100 Uiso 1 1 calc R . .
C116 C 0.0520(7) 0.2157(4) 0.4446(5) 0.074(4) Uani 1 1 d GU . .
H116 H 0.0288 0.1547 0.4728 0.089 Uiso 1 1 calc R . .
C117 C 0.1580(7) 0.2420(5) 0.4268(5) 0.071(4) Uani 1 1 d GU . .
H117 H 0.2056 0.1986 0.4430 0.085 Uiso 1 1 calc R . .
C118 C 0.1927(5) 0.3332(5) 0.3847(5) 0.061(3) Uani 1 1 d GU . .
H118 H 0.2636 0.3509 0.3728 0.073 Uiso 1 1 calc R . .
C119 C 0.2549(8) 0.5459(6) 0.3438(6) 0.065(3) Uani 1 1 d GU . .
C120 C 0.3392(9) 0.6097(7) 0.2923(5) 0.095(5) Uani 1 1 d GU . .
H120 H 0.3520 0.6330 0.2361 0.114 Uiso 1 1 calc R . .
C121 C 0.4045(8) 0.6386(7) 0.3246(8) 0.120(6) Uani 1 1 d GU . .
H121 H 0.4608 0.6813 0.2901 0.145 Uiso 1 1 calc R . .
C122 C 0.3854(10) 0.6038(9) 0.4085(9) 0.125(6) Uani 1 1 d GU . .
H122 H 0.4291 0.6232 0.4301 0.150 Uiso 1 1 calc R . .
C123 C 0.3011(11) 0.5400(9) 0.4601(6) 0.140(7) Uani 1 1 d GU . .
H123 H 0.2884 0.5167 0.5162 0.167 Uiso 1 1 calc R . .
C124 C 0.2359(9) 0.5111(7) 0.4277(6) 0.110(5) Uani 1 1 d GU . .
H124 H 0.1795 0.4684 0.4622 0.132 Uiso 1 1 calc R . .
P2 P 0.2099(3) 0.1671(2) 0.0109(2) 0.0535(8) Uani 1 1 d . . .
C201 C 0.2777(7) 0.2774(4) -0.0465(5) 0.056(3) Uani 1 1 d GU . .
C202 C 0.3841(7) 0.2907(6) -0.0548(6) 0.075(4) Uani 1 1 d GU . .
H202 H 0.4226 0.2414 -0.0340 0.090 Uiso 1 1 calc R . .
C203 C 0.4329(6) 0.3780(7) -0.0941(6) 0.091(5) Uani 1 1 d GU . .
H203 H 0.5040 0.3869 -0.0996 0.109 Uiso 1 1 calc R . .
C204 C 0.3753(9) 0.4518(5) -0.1252(6) 0.096(5) Uani 1 1 d GU . .
H204 H 0.4080 0.5101 -0.1515 0.116 Uiso 1 1 calc R . .
C205 C 0.2690(9) 0.4384(5) -0.1169(6) 0.109(5) Uani 1 1 d GU . .
H205 H 0.2305 0.4878 -0.1377 0.131 Uiso 1 1 calc R . .
C206 C 0.2202(6) 0.3512(6) -0.0776(6) 0.083(4) Uani 1 1 d GU . .
H206 H 0.1491 0.3422 -0.0721 0.100 Uiso 1 1 calc R . .
C207 C 0.0977(6) 0.1586(6) -0.0190(6) 0.060(3) Uani 1 1 d GU . .
C208 C 0.1115(6) 0.1220(6) -0.0800(6) 0.071(4) Uani 1 1 d GU . .
H208 H 0.1773 0.0986 -0.1023 0.085 Uiso 1 1 calc R . .
C209 C 0.0271(8) 0.1203(7) -0.1077(5) 0.087(4) Uani 1 1 d GU . .
H209 H 0.0364 0.0958 -0.1485 0.105 Uiso 1 1 calc R . .
C210 C -0.0713(7) 0.1552(7) -0.0744(6) 0.087(4) Uani 1 1 d GU . .
H210 H -0.1278 0.1541 -0.0929 0.104 Uiso 1 1 calc R . .
C211 C -0.0851(5) 0.1918(6) -0.0133(6) 0.087(4) Uani 1 1 d GU . .
H211 H -0.1509 0.2152 0.0090 0.105 Uiso 1 1 calc R . .
C212 C -0.0007(7) 0.1935(6) 0.0143(5) 0.073(4) Uani 1 1 d GU . .
H212 H -0.0100 0.2180 0.0551 0.088 Uiso 1 1 calc R . .
C213 C 0.1642(6) 0.1506(5) 0.1176(4) 0.054(3) Uani 1 1 d GU . .
C214 C 0.2193(6) 0.1944(5) 0.1472(5) 0.064(3) Uani 1 1 d GU . .
H214 H 0.2785 0.2335 0.1111 0.077 Uiso 1 1 calc R . .
C215 C 0.1860(7) 0.1797(6) 0.2307(5) 0.074(4) Uani 1 1 d GU . .
H215 H 0.2229 0.2090 0.2505 0.089 Uiso 1 1 calc R . .
C216 C 0.0976(8) 0.1212(6) 0.2846(4) 0.078(4) Uani 1 1 d GU . .
H216 H 0.0753 0.1114 0.3404 0.093 Uiso 1 1 calc R . .
C217 C 0.0425(6) 0.0775(6) 0.2550(5) 0.088(4) Uani 1 1 d GU . .
H217 H -0.0167 0.0384 0.2911 0.106 Uiso 1 1 calc R . .
C218 C 0.0758(6) 0.0922(5) 0.1715(6) 0.075(4) Uani 1 1 d GU . .
H218 H 0.0389 0.0629 0.1517 0.089 Uiso 1 1 calc R . .
C219 C 0.3034(7) 0.0838(5) -0.0117(6) 0.064(3) Uani 1 1 d GU . .
C220 C 0.3738(8) 0.1022(6) -0.0917(5) 0.093(5) Uani 1 1 d GU . .
H220 H 0.3755 0.1592 -0.1313 0.112 Uiso 1 1 calc R . .
C221 C 0.4417(8) 0.0353(8) -0.1126(6) 0.110(5) Uani 1 1 d GU . .
H221 H 0.4888 0.0476 -0.1661 0.132 Uiso 1 1 calc R . .
C222 C 0.4392(8) -0.0500(7) -0.0535(8) 0.103(5) Uani 1 1 d GU . .
H222 H 0.4846 -0.0947 -0.0674 0.124 Uiso 1 1 calc R . .
C223 C 0.3688(8) -0.0683(5) 0.0265(7) 0.097(5) Uani 1 1 d GU . .
H223 H 0.3671 -0.1254 0.0661 0.116 Uiso 1 1 calc R . .
C224 C 0.3009(7) -0.0015(6) 0.0474(5) 0.081(4) Uani 1 1 d GU . .
H224 H 0.2538 -0.0138 0.1009 0.098 Uiso 1 1 calc R . .
N1 N 0.9726(17) 0.4444(14) 0.9332(13) 0.170(8) Uiso 1 1 d DU . .
C301 C 0.9775(16) 0.5212(14) 0.9044(13) 0.119(6) Uiso 1 1 d DU . .
C302 C 0.9854(18) 0.6146(14) 0.8681(14) 0.157(9) Uiso 1 1 d DU . .
H30A H 1.0600 0.6346 0.8431 0.236 Uiso 1 1 calc R . .
H30B H 0.9499 0.6421 0.9089 0.236 Uiso 1 1 calc R . .
H30C H 0.9519 0.6324 0.8270 0.236 Uiso 1 1 calc R . .
N2 N 0.2110(16) 0.8080(14) 0.2194(12) 0.162(7) Uiso 1 1 d DU . .
C401 C 0.1726(15) 0.8287(13) 0.2749(12) 0.113(6) Uiso 1 1 d DU . .
C402 C 0.1276(14) 0.8508(12) 0.3453(11) 0.116(6) Uiso 1 1 d DU . .
H40A H 0.1162 0.7963 0.3926 0.174 Uiso 1 1 calc R . .
H40B H 0.0600 0.8786 0.3461 0.174 Uiso 1 1 calc R . .
H40C H 0.1755 0.8929 0.3461 0.174 Uiso 1 1 calc R . .
N3 N 0.803(2) 0.427(2) 0.3066(19) 0.254(13) Uiso 1 1 d DU . .
C501 C 0.714(2) 0.4246(18) 0.3396(17) 0.153(8) Uiso 1 1 d DU . .
C502 C 0.604(2) 0.417(2) 0.3782(19) 0.242(15) Uiso 1 1 d DU . .
H50A H 0.5707 0.3980 0.3473 0.364 Uiso 1 1 calc R . .
H50B H 0.5774 0.4747 0.3819 0.364 Uiso 1 1 calc R . .
H50C H 0.5865 0.3720 0.4323 0.364 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.869(13) . ?
Pt1 Sn1 2.5810(9) . ?
Pt1 Pt3 2.6929(6) . ?
Pt1 Sn3 2.7289(8) . ?
Pt1 Pt2 2.8305(6) . ?
Pt1 Sn2 2.8395(8) . ?
Pt1 Pt2 2.9947(6) 2_656 ?
Pt2 C2 1.875(11) . ?
Pt2 Pt2 2.6492(7) 2_656 ?
Pt2 Sn2 2.7117(9) 2_656 ?
Pt2 Pt3 2.8861(6) . ?
Pt2 Sn1 2.9291(8) . ?
Pt2 Sn1 2.9909(8) 2_656 ?
Pt2 Pt3 2.9932(6) 2_656 ?
Pt2 Pt1 2.9947(6) 2_656 ?
Pt3 C3 1.899(14) . ?
Pt3 Sn1 2.5927(8) 2_656 ?
Pt3 Sn3 2.7033(8) . ?
Pt3 Sn2 2.8795(8) . ?
Pt3 Pt2 2.9932(6) 2_656 ?
Sn1 Cl1 2.382(3) . ?
Sn1 Cl2 2.393(3) . ?
Sn1 Pt3 2.5927(8) 2_656 ?
Sn1 Pt2 2.9909(8) 2_656 ?
Sn2 Cl3 2.391(3) . ?
Sn2 Cl5 2.397(3) . ?
Sn2 Cl4 2.398(3) . ?
Sn2 Pt2 2.7117(9) 2_656 ?
Sn3 Cl8 2.379(3) . ?
Sn3 Cl6 2.387(3) . ?
Sn3 Cl7 2.410(4) . ?
C1 O1 1.122(13) . ?
C2 O2 1.141(13) . ?
C3 O3 1.110(13) . ?
P1 C119 1.764(8) . ?
P1 C107 1.767(7) . ?
P1 C101 1.787(7) . ?
P1 C113 1.790(6) . ?
C101 C102 1.3900 . ?
C101 C106 1.3900 . ?
C102 C103 1.3900 . ?
C102 H102 0.9300 . ?
C103 C104 1.3900 . ?
C103 H103 0.9300 . ?
C104 C105 1.3900 . ?
C104 H104 0.9300 . ?
C105 C106 1.3900 . ?
C105 H105 0.9300 . ?
C106 H106 0.9300 . ?
C107 C108 1.3900 . ?
C107 C112 1.3900 . ?
C108 C109 1.3900 . ?
C108 H108 0.9300 . ?
C109 C110 1.3900 . ?
C109 H109 0.9300 . ?
C110 C111 1.3900 . ?
C110 H110 0.9300 . ?
C111 C112 1.3900 . ?
C111 H111 0.9300 . ?
C112 H112 0.9300 . ?
C113 C114 1.3900 . ?
C113 C118 1.3900 . ?
C114 C115 1.3900 . ?
C114 H114 0.9300 . ?
C115 C116 1.3900 . ?
C115 H115 0.9300 . ?
C116 C117 1.3900 . ?
C116 H116 0.9300 . ?
C117 C118 1.3900 . ?
C117 H117 0.9300 . ?
C118 H118 0.9300 . ?
C119 C120 1.3900 . ?
C119 C124 1.3900 . ?
C120 C121 1.3900 . ?
C120 H120 0.9300 . ?
C121 C122 1.3900 . ?
C121 H121 0.9300 . ?
C122 C123 1.3900 . ?
C122 H122 0.9300 . ?
C123 C124 1.3900 . ?
C123 H123 0.9300 . ?
C124 H124 0.9300 . ?
P2 C219 1.775(7) . ?
P2 C213 1.783(7) . ?
P2 C207 1.789(7) . ?
P2 C201 1.794(7) . ?
C201 C202 1.3900 . ?
C201 C206 1.3900 . ?
C202 C203 1.3900 . ?
C202 H202 0.9300 . ?
C203 C204 1.3900 . ?
C203 H203 0.9300 . ?
C204 C205 1.3900 . ?
C204 H204 0.9300 . ?
C205 C206 1.3900 . ?
C205 H205 0.9300 . ?
C206 H206 0.9300 . ?
C207 C208 1.3900 . ?
C207 C212 1.3900 . ?
C208 C209 1.3900 . ?
C208 H208 0.9300 . ?
C209 C210 1.3900 . ?
C209 H209 0.9300 . ?
C210 C211 1.3900 . ?
C210 H210 0.9300 . ?
C211 C212 1.3900 . ?
C211 H211 0.9300 . ?
C212 H212 0.9300 . ?
C213 C214 1.3900 . ?
C213 C218 1.3900 . ?
C214 C215 1.3900 . ?
C214 H214 0.9300 . ?
C215 C216 1.3900 . ?
C215 H215 0.9300 . ?
C216 C217 1.3900 . ?
C216 H216 0.9300 . ?
C217 C218 1.3900 . ?
C217 H217 0.9300 . ?
C218 H218 0.9300 . ?
C219 C220 1.3900 . ?
C219 C224 1.3900 . ?
C220 C221 1.3900 . ?
C220 H220 0.9300 . ?
C221 C222 1.3900 . ?
C221 H221 0.9300 . ?
C222 C223 1.3900 . ?
C222 H222 0.9300 . ?
C223 C224 1.3900 . ?
C223 H223 0.9300 . ?
C224 H224 0.9300 . ?
N1 C301 1.126(18) . ?
C301 C302 1.371(18) . ?
C302 H30A 0.9600 . ?
C302 H30B 0.9600 . ?
C302 H30C 0.9600 . ?
N2 C401 1.124(17) . ?
C401 C402 1.385(17) . ?
C402 H40A 0.9600 . ?
C402 H40B 0.9600 . ?
C402 H40C 0.9600 . ?
N3 C501 1.117(19) . ?
C501 C502 1.377(19) . ?
C502 H50A 0.9600 . ?
C502 H50B 0.9600 . ?
C502 H50C 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 Sn1 89.9(4) . . ?
C1 Pt1 Pt3 148.7(4) . . ?
Sn1 Pt1 Pt3 121.00(2) . . ?
C1 Pt1 Sn3 93.1(3) . . ?
Sn1 Pt1 Sn3 160.45(3) . . ?
Pt3 Pt1 Sn3 59.811(19) . . ?
C1 Pt1 Pt2 145.2(4) . . ?
Sn1 Pt1 Pt2 65.35(2) . . ?
Pt3 Pt1 Pt2 62.946(16) . . ?
Sn3 Pt1 Pt2 102.82(2) . . ?
C1 Pt1 Sn2 106.7(4) . . ?
Sn1 Pt1 Sn2 105.74(3) . . ?
Pt3 Pt1 Sn2 62.663(19) . . ?
Sn3 Pt1 Sn2 91.90(3) . . ?
Pt2 Pt1 Sn2 103.53(2) . . ?
C1 Pt1 Pt2 137.6(3) . 2_656 ?
Sn1 Pt1 Pt2 64.38(2) . 2_656 ?
Pt3 Pt1 Pt2 63.245(14) . 2_656 ?
Sn3 Pt1 Pt2 122.66(2) . 2_656 ?
Pt2 Pt1 Pt2 54.014(15) . 2_656 ?
Sn2 Pt1 Pt2 55.317(19) . 2_656 ?
C2 Pt2 Pt2 162.1(4) . 2_656 ?
C2 Pt2 Sn2 85.0(4) . 2_656 ?
Pt2 Pt2 Sn2 112.35(3) 2_656 2_656 ?
C2 Pt2 Pt1 96.4(4) . . ?
Pt2 Pt2 Pt1 66.158(18) 2_656 . ?
Sn2 Pt2 Pt1 153.37(2) 2_656 . ?
C2 Pt2 Pt3 102.3(4) . . ?
Pt2 Pt2 Pt3 65.304(18) 2_656 . ?
Sn2 Pt2 Pt3 149.49(2) 2_656 . ?
Pt1 Pt2 Pt3 56.198(15) . . ?
C2 Pt2 Sn1 108.9(4) . . ?
Pt2 Pt2 Sn1 64.62(2) 2_656 . ?
Sn2 Pt2 Sn1 101.12(3) 2_656 . ?
Pt1 Pt2 Sn1 53.214(19) . . ?
Pt3 Pt2 Sn1 104.26(2) . . ?
C2 Pt2 Sn1 121.7(4) . 2_656 ?
Pt2 Pt2 Sn1 62.23(2) 2_656 2_656 ?
Sn2 Pt2 Sn1 98.51(3) 2_656 2_656 ?
Pt1 Pt2 Sn1 103.20(2) . 2_656 ?
Pt3 Pt2 Sn1 52.318(18) . 2_656 ?
Sn1 Pt2 Sn1 126.845(18) . 2_656 ?
C2 Pt2 Pt3 129.6(4) . 2_656 ?
Pt2 Pt2 Pt3 61.169(17) 2_656 2_656 ?
Sn2 Pt2 Pt3 60.389(19) 2_656 2_656 ?
Pt1 Pt2 Pt3 100.292(17) . 2_656 ?
Pt3 Pt2 Pt3 126.473(15) . 2_656 ?
Sn1 Pt2 Pt3 51.912(18) . 2_656 ?
Sn1 Pt2 Pt3 100.194(19) 2_656 2_656 ?
C2 Pt2 Pt1 137.5(4) . 2_656 ?
Pt2 Pt2 Pt1 59.828(17) 2_656 2_656 ?
Sn2 Pt2 Pt1 59.436(19) 2_656 2_656 ?
Pt1 Pt2 Pt1 125.986(15) . 2_656 ?
Pt3 Pt2 Pt1 98.988(17) . 2_656 ?
Sn1 Pt2 Pt1 100.767(19) . 2_656 ?
Sn1 Pt2 Pt1 51.088(18) 2_656 2_656 ?
Pt3 Pt2 Pt1 53.453(13) 2_656 2_656 ?
C3 Pt3 Sn1 88.1(3) . 2_656 ?
C3 Pt3 Pt1 151.5(3) . . ?
Sn1 Pt3 Pt1 119.38(2) 2_656 . ?
C3 Pt3 Sn3 96.1(3) . . ?
Sn1 Pt3 Sn3 160.52(3) 2_656 . ?
Pt1 Pt3 Sn3 60.75(2) . . ?
C3 Pt3 Sn2 106.7(3) . . ?
Sn1 Pt3 Sn2 105.47(3) 2_656 . ?
Pt1 Pt3 Sn2 61.160(19) . . ?
Sn3 Pt3 Sn2 91.56(2) . . ?
C3 Pt3 Pt2 146.2(3) . . ?
Sn1 Pt3 Pt2 65.92(2) 2_656 . ?
Pt1 Pt3 Pt2 60.856(15) . . ?
Sn3 Pt3 Pt2 102.02(2) . . ?
Sn2 Pt3 Pt2 101.15(2) . . ?
C3 Pt3 Pt2 133.6(3) . 2_656 ?
Sn1 Pt3 Pt2 62.77(2) 2_656 2_656 ?
Pt1 Pt3 Pt2 63.301(15) . 2_656 ?
Sn3 Pt3 Pt2 123.65(2) . 2_656 ?
Sn2 Pt3 Pt2 54.958(19) . 2_656 ?
Pt2 Pt3 Pt2 53.527(15) . 2_656 ?
Cl1 Sn1 Cl2 94.98(12) . . ?
Cl1 Sn1 Pt1 106.56(9) . . ?
Cl2 Sn1 Pt1 112.15(9) . . ?
Cl1 Sn1 Pt3 109.87(9) . 2_656 ?
Cl2 Sn1 Pt3 110.72(8) . 2_656 ?
Pt1 Sn1 Pt3 119.62(3) . 2_656 ?
Cl1 Sn1 Pt2 101.37(9) . . ?
Cl2 Sn1 Pt2 163.55(9) . . ?
Pt1 Sn1 Pt2 61.44(2) . . ?
Pt3 Sn1 Pt2 65.32(2) 2_656 . ?
Cl1 Sn1 Pt2 154.51(9) . 2_656 ?
Cl2 Sn1 Pt2 110.51(9) . 2_656 ?
Pt1 Sn1 Pt2 64.53(2) . 2_656 ?
Pt3 Sn1 Pt2 61.76(2) 2_656 2_656 ?
Pt2 Sn1 Pt2 53.155(18) . 2_656 ?
Cl3 Sn2 Cl5 93.72(15) . . ?
Cl3 Sn2 Cl4 94.36(13) . . ?
Cl5 Sn2 Cl4 96.15(12) . . ?
Cl3 Sn2 Pt2 157.05(9) . 2_656 ?
Cl5 Sn2 Pt2 98.51(10) . 2_656 ?
Cl4 Sn2 Pt2 103.49(9) . 2_656 ?
Cl3 Sn2 Pt1 93.03(9) . . ?
Cl5 Sn2 Pt1 103.86(9) . . ?
Cl4 Sn2 Pt1 158.15(9) . . ?
Pt2 Sn2 Pt1 65.25(2) 2_656 . ?
Cl3 Sn2 Pt3 97.75(10) . . ?
Cl5 Sn2 Pt3 157.31(10) . . ?
Cl4 Sn2 Pt3 102.39(9) . . ?
Pt2 Sn2 Pt3 64.65(2) 2_656 . ?
Pt1 Sn2 Pt3 56.177(17) . . ?
Cl8 Sn3 Cl6 94.77(13) . . ?
Cl8 Sn3 Cl7 91.10(13) . . ?
Cl6 Sn3 Cl7 92.50(16) . . ?
Cl8 Sn3 Pt3 150.75(8) . . ?
Cl6 Sn3 Pt3 111.19(9) . . ?
Cl7 Sn3 Pt3 100.64(9) . . ?
Cl8 Sn3 Pt1 100.66(8) . . ?
Cl6 Sn3 Pt1 108.00(11) . . ?
Cl7 Sn3 Pt1 155.20(10) . . ?
Pt3 Sn3 Pt1 59.435(19) . . ?
O1 C1 Pt1 178.1(11) . . ?
O2 C2 Pt2 178.1(11) . . ?
O3 C3 Pt3 176.9(11) . . ?
C119 P1 C107 110.0(5) . . ?
C119 P1 C101 110.9(5) . . ?
C107 P1 C101 108.4(4) . . ?
C119 P1 C113 109.2(4) . . ?
C107 P1 C113 110.1(4) . . ?
C101 P1 C113 108.2(4) . . ?
C102 C101 C106 120.0 . . ?
C102 C101 P1 120.6(6) . . ?
C106 C101 P1 119.4(6) . . ?
C101 C102 C103 120.0 . . ?
C101 C102 H102 120.0 . . ?
C103 C102 H102 120.0 . . ?
C104 C103 C102 120.0 . . ?
C104 C103 H103 120.0 . . ?
C102 C103 H103 120.0 . . ?
C105 C104 C103 120.0 . . ?
C105 C104 H104 120.0 . . ?
C103 C104 H104 120.0 . . ?
C104 C105 C106 120.0 . . ?
C104 C105 H105 120.0 . . ?
C106 C105 H105 120.0 . . ?
C105 C106 C101 120.0 . . ?
C105 C106 H106 120.0 . . ?
C101 C106 H106 120.0 . . ?
C108 C107 C112 120.0 . . ?
C108 C107 P1 119.4(5) . . ?
C112 C107 P1 120.6(5) . . ?
C107 C108 C109 120.0 . . ?
C107 C108 H108 120.0 . . ?
C109 C108 H108 120.0 . . ?
C108 C109 C110 120.0 . . ?
C108 C109 H109 120.0 . . ?
C110 C109 H109 120.0 . . ?
C109 C110 C111 120.0 . . ?
C109 C110 H110 120.0 . . ?
C111 C110 H110 120.0 . . ?
C112 C111 C110 120.0 . . ?
C112 C111 H111 120.0 . . ?
C110 C111 H111 120.0 . . ?
C111 C112 C107 120.0 . . ?
C111 C112 H112 120.0 . . ?
C107 C112 H112 120.0 . . ?
C114 C113 C118 120.0 . . ?
C114 C113 P1 119.8(5) . . ?
C118 C113 P1 120.2(5) . . ?
C115 C114 C113 120.0 . . ?
C115 C114 H114 120.0 . . ?
C113 C114 H114 120.0 . . ?
C114 C115 C116 120.0 . . ?
C114 C115 H115 120.0 . . ?
C116 C115 H115 120.0 . . ?
C117 C116 C115 120.0 . . ?
C117 C116 H116 120.0 . . ?
C115 C116 H116 120.0 . . ?
C118 C117 C116 120.0 . . ?
C118 C117 H117 120.0 . . ?
C116 C117 H117 120.0 . . ?
C117 C118 C113 120.0 . . ?
C117 C118 H118 120.0 . . ?
C113 C118 H118 120.0 . . ?
C120 C119 C124 120.0 . . ?
C120 C119 P1 119.9(6) . . ?
C124 C119 P1 119.9(6) . . ?
C121 C120 C119 120.0 . . ?
C121 C120 H120 120.0 . . ?
C119 C120 H120 120.0 . . ?
C120 C121 C122 120.0 . . ?
C120 C121 H121 120.0 . . ?
C122 C121 H121 120.0 . . ?
C123 C122 C121 120.0 . . ?
C123 C122 H122 120.0 . . ?
C121 C122 H122 120.0 . . ?
C124 C123 C122 120.0 . . ?
C124 C123 H123 120.0 . . ?
C122 C123 H123 120.0 . . ?
C123 C124 C119 120.0 . . ?
C123 C124 H124 120.0 . . ?
C119 C124 H124 120.0 . . ?
C219 P2 C213 110.9(4) . . ?
C219 P2 C207 109.0(4) . . ?
C213 P2 C207 109.6(4) . . ?
C219 P2 C201 107.5(4) . . ?
C213 P2 C201 109.4(4) . . ?
C207 P2 C201 110.4(4) . . ?
C202 C201 C206 120.0 . . ?
C202 C201 P2 120.7(5) . . ?
C206 C201 P2 119.1(5) . . ?
C201 C202 C203 120.0 . . ?
C201 C202 H202 120.0 . . ?
C203 C202 H202 120.0 . . ?
C202 C203 C204 120.0 . . ?
C202 C203 H203 120.0 . . ?
C204 C203 H203 120.0 . . ?
C205 C204 C203 120.0 . . ?
C205 C204 H204 120.0 . . ?
C203 C204 H204 120.0 . . ?
C204 C205 C206 120.0 . . ?
C204 C205 H205 120.0 . . ?
C206 C205 H205 120.0 . . ?
C205 C206 C201 120.0 . . ?
C205 C206 H206 120.0 . . ?
C201 C206 H206 120.0 . . ?
C208 C207 C212 120.0 . . ?
C208 C207 P2 119.3(5) . . ?
C212 C207 P2 120.6(5) . . ?
C209 C208 C207 120.0 . . ?
C209 C208 H208 120.0 . . ?
C207 C208 H208 120.0 . . ?
C210 C209 C208 120.0 . . ?
C210 C209 H209 120.0 . . ?
C208 C209 H209 120.0 . . ?
C209 C210 C211 120.0 . . ?
C209 C210 H210 120.0 . . ?
C211 C210 H210 120.0 . . ?
C212 C211 C210 120.0 . . ?
C212 C211 H211 120.0 . . ?
C210 C211 H211 120.0 . . ?
C211 C212 C207 120.0 . . ?
C211 C212 H212 120.0 . . ?
C207 C212 H212 120.0 . . ?
C214 C213 C218 120.0 . . ?
C214 C213 P2 119.7(5) . . ?
C218 C213 P2 120.3(5) . . ?
C213 C214 C215 120.0 . . ?
C213 C214 H214 120.0 . . ?
C215 C214 H214 120.0 . . ?
C216 C215 C214 120.0 . . ?
C216 C215 H215 120.0 . . ?
C214 C215 H215 120.0 . . ?
C215 C216 C217 120.0 . . ?
C215 C216 H216 120.0 . . ?
C217 C216 H216 120.0 . . ?
C218 C217 C216 120.0 . . ?
C218 C217 H217 120.0 . . ?
C216 C217 H217 120.0 . . ?
C217 C218 C213 120.0 . . ?
C217 C218 H218 120.0 . . ?
C213 C218 H218 120.0 . . ?
C220 C219 C224 120.0 . . ?
C220 C219 P2 118.8(6) . . ?
C224 C219 P2 121.0(6) . . ?
C221 C220 C219 120.0 . . ?
C221 C220 H220 120.0 . . ?
C219 C220 H220 120.0 . . ?
C220 C221 C222 120.0 . . ?
C220 C221 H221 120.0 . . ?
C222 C221 H221 120.0 . . ?
C223 C222 C221 120.0 . . ?
C223 C222 H222 120.0 . . ?
C221 C222 H222 120.0 . . ?
C224 C223 C222 120.0 . . ?
C224 C223 H223 120.0 . . ?
C222 C223 H223 120.0 . . ?
C223 C224 C219 120.0 . . ?
C223 C224 H224 120.0 . . ?
C219 C224 H224 120.0 . . ?
N1 C301 C302 179(3) . . ?
C301 C302 H30A 109.5 . . ?
C301 C302 H30B 109.5 . . ?
H30A C302 H30B 109.5 . . ?
C301 C302 H30C 109.5 . . ?
H30A C302 H30C 109.5 . . ?
H30B C302 H30C 109.5 . . ?
N2 C401 C402 177(2) . . ?
C401 C402 H40A 109.5 . . ?
C401 C402 H40B 109.5 . . ?
H40A C402 H40B 109.5 . . ?
C401 C402 H40C 109.5 . . ?
H40A C402 H40C 109.5 . . ?
H40B C402 H40C 109.5 . . ?
N3 C501 C502 176(4) . . ?
C501 C502 H50A 109.5 . . ?
C501 C502 H50B 109.5 . . ?
H50A C502 H50B 109.5 . . ?
C501 C502 H50C 109.5 . . ?
H50A C502 H50C 109.5 . . ?
H50B C502 H50C 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 Pt2 C2 60.5(7) . . . . ?
Sn1 Pt1 Pt2 C2 108.9(4) . . . . ?
Pt3 Pt1 Pt2 C2 -100.5(4) . . . . ?
Sn3 Pt1 Pt2 C2 -54.6(4) . . . . ?
Sn2 Pt1 Pt2 C2 -149.7(4) . . . . ?
Pt2 Pt1 Pt2 C2 -175.8(4) 2_656 . . . ?
C1 Pt1 Pt2 Pt2 -123.7(6) . . . 2_656 ?
Sn1 Pt1 Pt2 Pt2 -75.24(2) . . . 2_656 ?
Pt3 Pt1 Pt2 Pt2 75.296(19) . . . 2_656 ?
Sn3 Pt1 Pt2 Pt2 121.24(2) . . . 2_656 ?
Sn2 Pt1 Pt2 Pt2 26.09(2) . . . 2_656 ?
C1 Pt1 Pt2 Sn2 -31.0(6) . . . 2_656 ?
Sn1 Pt1 Pt2 Sn2 17.41(5) . . . 2_656 ?
Pt3 Pt1 Pt2 Sn2 167.95(5) . . . 2_656 ?
Sn3 Pt1 Pt2 Sn2 -146.11(5) . . . 2_656 ?
Sn2 Pt1 Pt2 Sn2 118.74(4) . . . 2_656 ?
Pt2 Pt1 Pt2 Sn2 92.65(5) 2_656 . . 2_656 ?
C1 Pt1 Pt2 Pt3 161.0(6) . . . . ?
Sn1 Pt1 Pt2 Pt3 -150.54(2) . . . . ?
Sn3 Pt1 Pt2 Pt3 45.95(2) . . . . ?
Sn2 Pt1 Pt2 Pt3 -49.21(2) . . . . ?
Pt2 Pt1 Pt2 Pt3 -75.296(19) 2_656 . . . ?
C1 Pt1 Pt2 Sn1 -48.4(6) . . . . ?
Pt3 Pt1 Pt2 Sn1 150.54(2) . . . . ?
Sn3 Pt1 Pt2 Sn1 -163.51(3) . . . . ?
Sn2 Pt1 Pt2 Sn1 101.33(3) . . . . ?
Pt2 Pt1 Pt2 Sn1 75.24(2) 2_656 . . . ?
C1 Pt1 Pt2 Sn1 -174.8(6) . . . 2_656 ?
Sn1 Pt1 Pt2 Sn1 -126.417(19) . . . 2_656 ?
Pt3 Pt1 Pt2 Sn1 24.123(18) . . . 2_656 ?
Sn3 Pt1 Pt2 Sn1 70.07(3) . . . 2_656 ?
Sn2 Pt1 Pt2 Sn1 -25.09(3) . . . 2_656 ?
Pt2 Pt1 Pt2 Sn1 -51.173(19) 2_656 . . 2_656 ?
C1 Pt1 Pt2 Pt3 -71.7(6) . . . 2_656 ?
Sn1 Pt1 Pt2 Pt3 -23.28(2) . . . 2_656 ?
Pt3 Pt1 Pt2 Pt3 127.265(15) . . . 2_656 ?
Sn3 Pt1 Pt2 Pt3 173.21(2) . . . 2_656 ?
Sn2 Pt1 Pt2 Pt3 78.06(2) . . . 2_656 ?
Pt2 Pt1 Pt2 Pt3 51.969(14) 2_656 . . 2_656 ?
C1 Pt1 Pt2 Pt1 -123.7(6) . . . 2_656 ?
Sn1 Pt1 Pt2 Pt1 -75.24(2) . . . 2_656 ?
Pt3 Pt1 Pt2 Pt1 75.296(19) . . . 2_656 ?
Sn3 Pt1 Pt2 Pt1 121.24(2) . . . 2_656 ?
Sn2 Pt1 Pt2 Pt1 26.09(2) . . . 2_656 ?
Pt2 Pt1 Pt2 Pt1 0.0 2_656 . . 2_656 ?
C1 Pt1 Pt3 C3 5.9(9) . . . . ?
Sn1 Pt1 Pt3 C3 -163.5(7) . . . . ?
Sn3 Pt1 Pt3 C3 39.2(7) . . . . ?
Pt2 Pt1 Pt3 C3 165.0(7) . . . . ?
Sn2 Pt1 Pt3 C3 -70.9(7) . . . . ?
Pt2 Pt1 Pt3 C3 -133.7(7) 2_656 . . . ?
C1 Pt1 Pt3 Sn1 169.1(7) . . . 2_656 ?
Sn1 Pt1 Pt3 Sn1 -0.35(5) . . . 2_656 ?
Sn3 Pt1 Pt3 Sn1 -157.62(3) . . . 2_656 ?
Pt2 Pt1 Pt3 Sn1 -31.79(3) . . . 2_656 ?
Sn2 Pt1 Pt3 Sn1 92.26(3) . . . 2_656 ?
Pt2 Pt1 Pt3 Sn1 29.44(3) 2_656 . . 2_656 ?
C1 Pt1 Pt3 Sn3 -33.3(7) . . . . ?
Sn1 Pt1 Pt3 Sn3 157.27(3) . . . . ?
Pt2 Pt1 Pt3 Sn3 125.83(2) . . . . ?
Sn2 Pt1 Pt3 Sn3 -110.12(3) . . . . ?
Pt2 Pt1 Pt3 Sn3 -172.94(2) 2_656 . . . ?
C1 Pt1 Pt3 Sn2 76.9(7) . . . . ?
Sn1 Pt1 Pt3 Sn2 -92.61(3) . . . . ?
Sn3 Pt1 Pt3 Sn2 110.12(3) . . . . ?
Pt2 Pt1 Pt3 Sn2 -124.04(2) . . . . ?
Pt2 Pt1 Pt3 Sn2 -62.82(2) 2_656 . . . ?
C1 Pt1 Pt3 Pt2 -159.1(7) . . . . ?
Sn1 Pt1 Pt3 Pt2 31.43(3) . . . . ?
Sn3 Pt1 Pt3 Pt2 -125.83(2) . . . . ?
Sn2 Pt1 Pt3 Pt2 124.04(2) . . . . ?
Pt2 Pt1 Pt3 Pt2 61.222(16) 2_656 . . . ?
C1 Pt1 Pt3 Pt2 139.7(7) . . . 2_656 ?
Sn1 Pt1 Pt3 Pt2 -29.79(3) . . . 2_656 ?
Sn3 Pt1 Pt3 Pt2 172.94(2) . . . 2_656 ?
Pt2 Pt1 Pt3 Pt2 -61.222(16) . . . 2_656 ?
Sn2 Pt1 Pt3 Pt2 62.82(2) . . . 2_656 ?
C2 Pt2 Pt3 C3 -77.7(7) . . . . ?
Pt2 Pt2 Pt3 C3 115.9(6) 2_656 . . . ?
Sn2 Pt2 Pt3 C3 23.4(6) 2_656 . . . ?
Pt1 Pt2 Pt3 C3 -167.2(6) . . . . ?
Sn1 Pt2 Pt3 C3 168.8(6) . . . . ?
Sn1 Pt2 Pt3 C3 43.0(6) 2_656 . . . ?
Pt3 Pt2 Pt3 C3 115.9(6) 2_656 . . . ?
Pt1 Pt2 Pt3 C3 65.2(6) 2_656 . . . ?
C2 Pt2 Pt3 Sn1 -120.7(4) . . . 2_656 ?
Pt2 Pt2 Pt3 Sn1 72.97(2) 2_656 . . 2_656 ?
Sn2 Pt2 Pt3 Sn1 -19.56(4) 2_656 . . 2_656 ?
Pt1 Pt2 Pt3 Sn1 149.82(2) . . . 2_656 ?
Sn1 Pt2 Pt3 Sn1 125.84(2) . . . 2_656 ?
Pt3 Pt2 Pt3 Sn1 72.97(2) 2_656 . . 2_656 ?
Pt1 Pt2 Pt3 Sn1 22.23(2) 2_656 . . 2_656 ?
C2 Pt2 Pt3 Pt1 89.5(4) . . . . ?
Pt2 Pt2 Pt3 Pt1 -76.848(19) 2_656 . . . ?
Sn2 Pt2 Pt3 Pt1 -169.38(4) 2_656 . . . ?
Sn1 Pt2 Pt3 Pt1 -23.979(19) . . . . ?
Sn1 Pt2 Pt3 Pt1 -149.82(2) 2_656 . . . ?
Pt3 Pt2 Pt3 Pt1 -76.848(19) 2_656 . . . ?
Pt1 Pt2 Pt3 Pt1 -127.591(14) 2_656 . . . ?
C2 Pt2 Pt3 Sn3 43.2(4) . . . . ?
Pt2 Pt2 Pt3 Sn3 -123.17(2) 2_656 . . . ?
Sn2 Pt2 Pt3 Sn3 144.30(4) 2_656 . . . ?
Pt1 Pt2 Pt3 Sn3 -46.32(2) . . . . ?
Sn1 Pt2 Pt3 Sn3 -70.30(3) . . . . ?
Sn1 Pt2 Pt3 Sn3 163.86(3) 2_656 . . . ?
Pt3 Pt2 Pt3 Sn3 -123.17(2) 2_656 . . . ?
Pt1 Pt2 Pt3 Sn3 -173.912(19) 2_656 . . . ?
C2 Pt2 Pt3 Sn2 137.2(4) . . . . ?
Pt2 Pt2 Pt3 Sn2 -29.13(2) 2_656 . . . ?
Sn2 Pt2 Pt3 Sn2 -121.66(4) 2_656 . . . ?
Pt1 Pt2 Pt3 Sn2 47.715(19) . . . . ?
Sn1 Pt2 Pt3 Sn2 23.74(2) . . . . ?
Sn1 Pt2 Pt3 Sn2 -102.10(3) 2_656 . . . ?
Pt3 Pt2 Pt3 Sn2 -29.13(2) 2_656 . . . ?
Pt1 Pt2 Pt3 Sn2 -79.88(2) 2_656 . . . ?
C2 Pt2 Pt3 Pt2 166.3(4) . . . 2_656 ?
Sn2 Pt2 Pt3 Pt2 -92.53(4) 2_656 . . 2_656 ?
Pt1 Pt2 Pt3 Pt2 76.848(19) . . . 2_656 ?
Sn1 Pt2 Pt3 Pt2 52.869(19) . . . 2_656 ?
Sn1 Pt2 Pt3 Pt2 -72.97(2) 2_656 . . 2_656 ?
Pt3 Pt2 Pt3 Pt2 0.0 2_656 . . 2_656 ?
Pt1 Pt2 Pt3 Pt2 -50.743(15) 2_656 . . 2_656 ?
C1 Pt1 Sn1 Cl1 60.6(4) . . . . ?
Pt3 Pt1 Sn1 Cl1 -124.88(9) . . . . ?
Sn3 Pt1 Sn1 Cl1 -38.37(13) . . . . ?
Pt2 Pt1 Sn1 Cl1 -94.15(9) . . . . ?
Sn2 Pt1 Sn1 Cl1 167.91(9) . . . . ?
Pt2 Pt1 Sn1 Cl1 -154.35(9) 2_656 . . . ?
C1 Pt1 Sn1 Cl2 -42.1(4) . . . . ?
Pt3 Pt1 Sn1 Cl2 132.48(9) . . . . ?
Sn3 Pt1 Sn1 Cl2 -141.01(11) . . . . ?
Pt2 Pt1 Sn1 Cl2 163.21(9) . . . . ?
Sn2 Pt1 Sn1 Cl2 65.27(9) . . . . ?
Pt2 Pt1 Sn1 Cl2 103.01(9) 2_656 . . . ?
C1 Pt1 Sn1 Pt3 -174.2(3) . . . 2_656 ?
Pt3 Pt1 Sn1 Pt3 0.35(5) . . . 2_656 ?
Sn3 Pt1 Sn1 Pt3 86.86(8) . . . 2_656 ?
Pt2 Pt1 Sn1 Pt3 31.08(3) . . . 2_656 ?
Sn2 Pt1 Sn1 Pt3 -66.86(4) . . . 2_656 ?
Pt2 Pt1 Sn1 Pt3 -29.12(3) 2_656 . . 2_656 ?
C1 Pt1 Sn1 Pt2 154.7(3) . . . . ?
Pt3 Pt1 Sn1 Pt2 -30.73(2) . . . . ?
Sn3 Pt1 Sn1 Pt2 55.78(8) . . . . ?
Sn2 Pt1 Sn1 Pt2 -97.94(2) . . . . ?
Pt2 Pt1 Sn1 Pt2 -60.202(17) 2_656 . . . ?
C1 Pt1 Sn1 Pt2 -145.1(3) . . . 2_656 ?
Pt3 Pt1 Sn1 Pt2 29.47(2) . . . 2_656 ?
Sn3 Pt1 Sn1 Pt2 115.98(8) . . . 2_656 ?
Pt2 Pt1 Sn1 Pt2 60.202(17) . . . 2_656 ?
Sn2 Pt1 Sn1 Pt2 -37.74(2) . . . 2_656 ?
C2 Pt2 Sn1 Cl1 19.1(4) . . . . ?
Pt2 Pt2 Sn1 Cl1 -178.97(10) 2_656 . . . ?
Sn2 Pt2 Sn1 Cl1 -69.35(9) 2_656 . . . ?
Pt1 Pt2 Sn1 Cl1 102.79(9) . . . . ?
Pt3 Pt2 Sn1 Cl1 127.73(9) . . . . ?
Sn1 Pt2 Sn1 Cl1 -178.97(10) 2_656 . . . ?
Pt3 Pt2 Sn1 Cl1 -106.81(10) 2_656 . . . ?
Pt1 Pt2 Sn1 Cl1 -130.00(9) 2_656 . . . ?
C2 Pt2 Sn1 Cl2 -154.5(5) . . . . ?
Pt2 Pt2 Sn1 Cl2 7.4(3) 2_656 . . . ?
Sn2 Pt2 Sn1 Cl2 117.0(3) 2_656 . . . ?
Pt1 Pt2 Sn1 Cl2 -70.9(3) . . . . ?
Pt3 Pt2 Sn1 Cl2 -45.9(3) . . . . ?
Sn1 Pt2 Sn1 Cl2 7.4(3) 2_656 . . . ?
Pt3 Pt2 Sn1 Cl2 79.5(3) 2_656 . . . ?
Pt1 Pt2 Sn1 Cl2 56.3(3) 2_656 . . . ?
C2 Pt2 Sn1 Pt1 -83.7(4) . . . . ?
Pt2 Pt2 Sn1 Pt1 78.24(2) 2_656 . . . ?
Sn2 Pt2 Sn1 Pt1 -172.15(2) 2_656 . . . ?
Pt3 Pt2 Sn1 Pt1 24.94(2) . . . . ?
Sn1 Pt2 Sn1 Pt1 78.24(2) 2_656 . . . ?
Pt3 Pt2 Sn1 Pt1 150.40(3) 2_656 . . . ?
Pt1 Pt2 Sn1 Pt1 127.203(17) 2_656 . . . ?
C2 Pt2 Sn1 Pt3 125.9(4) . . . 2_656 ?
Pt2 Pt2 Sn1 Pt3 -72.16(2) 2_656 . . 2_656 ?
Sn2 Pt2 Sn1 Pt3 37.46(2) 2_656 . . 2_656 ?
Pt1 Pt2 Sn1 Pt3 -150.40(3) . . . 2_656 ?
Pt3 Pt2 Sn1 Pt3 -125.458(19) . . . 2_656 ?
Sn1 Pt2 Sn1 Pt3 -72.16(2) 2_656 . . 2_656 ?
Pt1 Pt2 Sn1 Pt3 -23.19(2) 2_656 . . 2_656 ?
C2 Pt2 Sn1 Pt2 -161.9(4) . . . 2_656 ?
Sn2 Pt2 Sn1 Pt2 109.62(3) 2_656 . . 2_656 ?
Pt1 Pt2 Sn1 Pt2 -78.24(2) . . . 2_656 ?
Pt3 Pt2 Sn1 Pt2 -53.295(18) . . . 2_656 ?
Sn1 Pt2 Sn1 Pt2 0.0 2_656 . . 2_656 ?
Pt3 Pt2 Sn1 Pt2 72.16(2) 2_656 . . 2_656 ?
Pt1 Pt2 Sn1 Pt2 48.968(17) 2_656 . . 2_656 ?
C1 Pt1 Sn2 Cl3 -50.8(4) . . . . ?
Sn1 Pt1 Sn2 Cl3 -145.53(11) . . . . ?
Pt3 Pt1 Sn2 Cl3 97.30(11) . . . . ?
Sn3 Pt1 Sn2 Cl3 43.00(11) . . . . ?
Pt2 Pt1 Sn2 Cl3 146.67(11) . . . . ?
Pt2 Pt1 Sn2 Cl3 172.31(11) 2_656 . . . ?
C1 Pt1 Sn2 Cl5 43.8(4) . . . . ?
Sn1 Pt1 Sn2 Cl5 -50.94(11) . . . . ?
Pt3 Pt1 Sn2 Cl5 -168.11(11) . . . . ?
Sn3 Pt1 Sn2 Cl5 137.59(10) . . . . ?
Pt2 Pt1 Sn2 Cl5 -118.74(10) . . . . ?
Pt2 Pt1 Sn2 Cl5 -93.10(10) 2_656 . . . ?
C1 Pt1 Sn2 Cl4 -160.5(4) . . . . ?
Sn1 Pt1 Sn2 Cl4 104.8(2) . . . . ?
Pt3 Pt1 Sn2 Cl4 -12.4(2) . . . . ?
Sn3 Pt1 Sn2 Cl4 -66.7(2) . . . . ?
Pt2 Pt1 Sn2 Cl4 37.0(2) . . . . ?
Pt2 Pt1 Sn2 Cl4 62.6(2) 2_656 . . . ?
C1 Pt1 Sn2 Pt2 136.9(4) . . . 2_656 ?
Sn1 Pt1 Sn2 Pt2 42.16(3) . . . 2_656 ?
Pt3 Pt1 Sn2 Pt2 -75.017(19) . . . 2_656 ?
Sn3 Pt1 Sn2 Pt2 -129.32(2) . . . 2_656 ?
Pt2 Pt1 Sn2 Pt2 -25.64(2) . . . 2_656 ?
C1 Pt1 Sn2 Pt3 -148.1(4) . . . . ?
Sn1 Pt1 Sn2 Pt3 117.18(3) . . . . ?
Sn3 Pt1 Sn2 Pt3 -54.30(2) . . . . ?
Pt2 Pt1 Sn2 Pt3 49.377(18) . . . . ?
Pt2 Pt1 Sn2 Pt3 75.017(19) 2_656 . . . ?
C3 Pt3 Sn2 Cl3 63.5(4) . . . . ?
Sn1 Pt3 Sn2 Cl3 156.15(10) 2_656 . . . ?
Pt1 Pt3 Sn2 Cl3 -88.46(10) . . . . ?
Sn3 Pt3 Sn2 Cl3 -33.42(10) . . . . ?
Pt2 Pt3 Sn2 Cl3 -135.99(10) . . . . ?
Pt2 Pt3 Sn2 Cl3 -164.56(10) 2_656 . . . ?
C3 Pt3 Sn2 Cl5 -176.9(4) . . . . ?
Sn1 Pt3 Sn2 Cl5 -84.2(2) 2_656 . . . ?
Pt1 Pt3 Sn2 Cl5 31.2(2) . . . . ?
Sn3 Pt3 Sn2 Cl5 86.3(2) . . . . ?
Pt2 Pt3 Sn2 Cl5 -16.3(2) . . . . ?
Pt2 Pt3 Sn2 Cl5 -44.9(2) 2_656 . . . ?
C3 Pt3 Sn2 Cl4 -32.8(4) . . . . ?
Sn1 Pt3 Sn2 Cl4 59.92(9) 2_656 . . . ?
Pt1 Pt3 Sn2 Cl4 175.31(9) . . . . ?
Sn3 Pt3 Sn2 Cl4 -129.65(9) . . . . ?
Pt2 Pt3 Sn2 Cl4 127.78(9) . . . . ?
Pt2 Pt3 Sn2 Cl4 99.21(9) 2_656 . . . ?
C3 Pt3 Sn2 Pt2 -132.0(4) . . . 2_656 ?
Sn1 Pt3 Sn2 Pt2 -39.29(3) 2_656 . . 2_656 ?
Pt1 Pt3 Sn2 Pt2 76.10(2) . . . 2_656 ?
Sn3 Pt3 Sn2 Pt2 131.14(2) . . . 2_656 ?
Pt2 Pt3 Sn2 Pt2 28.57(2) . . . 2_656 ?
C3 Pt3 Sn2 Pt1 151.9(4) . . . . ?
Sn1 Pt3 Sn2 Pt1 -115.39(3) 2_656 . . . ?
Sn3 Pt3 Sn2 Pt1 55.04(2) . . . . ?
Pt2 Pt3 Sn2 Pt1 -47.530(18) . . . . ?
Pt2 Pt3 Sn2 Pt1 -76.10(2) 2_656 . . . ?
C3 Pt3 Sn3 Cl8 -110.3(4) . . . . ?
Sn1 Pt3 Sn3 Cl8 148.0(2) 2_656 . . . ?
Pt1 Pt3 Sn3 Cl8 52.05(19) . . . . ?
Sn2 Pt3 Sn3 Cl8 -3.3(2) . . . . ?
Pt2 Pt3 Sn3 Cl8 98.4(2) . . . . ?
Pt2 Pt3 Sn3 Cl8 44.5(2) 2_656 . . . ?
C3 Pt3 Sn3 Cl6 98.7(4) . . . . ?
Sn1 Pt3 Sn3 Cl6 -3.05(16) 2_656 . . . ?
Pt1 Pt3 Sn3 Cl6 -98.97(13) . . . . ?
Sn2 Pt3 Sn3 Cl6 -154.33(13) . . . . ?
Pt2 Pt3 Sn3 Cl6 -52.59(13) . . . . ?
Pt2 Pt3 Sn3 Cl6 -106.54(13) 2_656 . . . ?
C3 Pt3 Sn3 Cl7 1.8(3) . . . . ?
Sn1 Pt3 Sn3 Cl7 -99.97(14) 2_656 . . . ?
Pt1 Pt3 Sn3 Cl7 164.11(12) . . . . ?
Sn2 Pt3 Sn3 Cl7 108.74(12) . . . . ?
Pt2 Pt3 Sn3 Cl7 -149.51(12) . . . . ?
Pt2 Pt3 Sn3 Cl7 156.53(12) 2_656 . . . ?
C3 Pt3 Sn3 Pt1 -162.3(3) . . . . ?
Sn1 Pt3 Sn3 Pt1 95.92(8) 2_656 . . . ?
Sn2 Pt3 Sn3 Pt1 -55.37(2) . . . . ?
Pt2 Pt3 Sn3 Pt1 46.381(18) . . . . ?
Pt2 Pt3 Sn3 Pt1 -7.58(3) 2_656 . . . ?
C1 Pt1 Sn3 Cl8 6.5(4) . . . . ?
Sn1 Pt1 Sn3 Cl8 104.89(12) . . . . ?
Pt3 Pt1 Sn3 Cl8 -156.92(10) . . . . ?
Pt2 Pt1 Sn3 Cl8 155.31(9) . . . . ?
Sn2 Pt1 Sn3 Cl8 -100.35(10) . . . . ?
Pt2 Pt1 Sn3 Cl8 -149.43(9) 2_656 . . . ?
C1 Pt1 Sn3 Cl6 -92.1(4) . . . . ?
Sn1 Pt1 Sn3 Cl6 6.26(14) . . . . ?
Pt3 Pt1 Sn3 Cl6 104.45(11) . . . . ?
Pt2 Pt1 Sn3 Cl6 56.68(11) . . . . ?
Sn2 Pt1 Sn3 Cl6 161.02(11) . . . . ?
Pt2 Pt1 Sn3 Cl6 111.94(11) 2_656 . . . ?
C1 Pt1 Sn3 Cl7 123.5(4) . . . . ?
Sn1 Pt1 Sn3 Cl7 -138.1(3) . . . . ?
Pt3 Pt1 Sn3 Cl7 -39.9(3) . . . . ?
Pt2 Pt1 Sn3 Cl7 -87.7(3) . . . . ?
Sn2 Pt1 Sn3 Cl7 16.7(3) . . . . ?
Pt2 Pt1 Sn3 Cl7 -32.4(3) 2_656 . . . ?
C1 Pt1 Sn3 Pt3 163.4(4) . . . . ?
Sn1 Pt1 Sn3 Pt3 -98.19(8) . . . . ?
Pt2 Pt1 Sn3 Pt3 -47.77(2) . . . . ?
Sn2 Pt1 Sn3 Pt3 56.57(2) . . . . ?
Pt2 Pt1 Sn3 Pt3 7.49(2) 2_656 . . . ?
Sn1 Pt1 C1 O1 38(41) . . . . ?
Pt3 Pt1 C1 O1 -133(40) . . . . ?
Sn3 Pt1 C1 O1 -161(41) . . . . ?
Pt2 Pt1 C1 O1 81(41) . . . . ?
Sn2 Pt1 C1 O1 -68(41) . . . . ?
Pt2 Pt1 C1 O1 -11(41) 2_656 . . . ?
Pt2 Pt2 C2 O2 30(35) 2_656 . . . ?
Sn2 Pt2 C2 O2 -165(34) 2_656 . . . ?
Pt1 Pt2 C2 O2 42(34) . . . . ?
Pt3 Pt2 C2 O2 -15(34) . . . . ?
Sn1 Pt2 C2 O2 95(34) . . . . ?
Sn1 Pt2 C2 O2 -68(34) 2_656 . . . ?
Pt3 Pt2 C2 O2 151(34) 2_656 . . . ?
Pt1 Pt2 C2 O2 -133(34) 2_656 . . . ?
Sn1 Pt3 C3 O3 -90(21) 2_656 . . . ?
Pt1 Pt3 C3 O3 76(21) . . . . ?
Sn3 Pt3 C3 O3 110(21) . . . . ?
Sn2 Pt3 C3 O3 16(21) . . . . ?
Pt2 Pt3 C3 O3 -128(21) . . . . ?
Pt2 Pt3 C3 O3 -41(21) 2_656 . . . ?
C119 P1 C101 C102 -28.2(7) . . . . ?
C107 P1 C101 C102 -149.1(5) . . . . ?
C113 P1 C101 C102 91.4(6) . . . . ?
C119 P1 C101 C106 154.9(6) . . . . ?
C107 P1 C101 C106 34.0(6) . . . . ?
C113 P1 C101 C106 -85.4(6) . . . . ?
C106 C101 C102 C103 0.0 . . . . ?
P1 C101 C102 C103 -176.8(7) . . . . ?
C101 C102 C103 C104 0.0 . . . . ?
C102 C103 C104 C105 0.0 . . . . ?
C103 C104 C105 C106 0.0 . . . . ?
C104 C105 C106 C101 0.0 . . . . ?
C102 C101 C106 C105 0.0 . . . . ?
P1 C101 C106 C105 176.8(7) . . . . ?
C119 P1 C107 C108 -81.1(6) . . . . ?
C101 P1 C107 C108 40.4(6) . . . . ?
C113 P1 C107 C108 158.5(5) . . . . ?
C119 P1 C107 C112 96.5(6) . . . . ?
C101 P1 C107 C112 -142.1(5) . . . . ?
C113 P1 C107 C112 -23.9(6) . . . . ?
C112 C107 C108 C109 0.0 . . . . ?
P1 C107 C108 C109 177.6(6) . . . . ?
C107 C108 C109 C110 0.0 . . . . ?
C108 C109 C110 C111 0.0 . . . . ?
C109 C110 C111 C112 0.0 . . . . ?
C110 C111 C112 C107 0.0 . . . . ?
C108 C107 C112 C111 0.0 . . . . ?
P1 C107 C112 C111 -177.6(6) . . . . ?
C119 P1 C113 C114 141.7(6) . . . . ?
C107 P1 C113 C114 -97.4(5) . . . . ?
C101 P1 C113 C114 20.9(6) . . . . ?
C119 P1 C113 C118 -40.2(6) . . . . ?
C107 P1 C113 C118 80.8(6) . . . . ?
C101 P1 C113 C118 -160.9(5) . . . . ?
C118 C113 C114 C115 0.0 . . . . ?
P1 C113 C114 C115 178.2(6) . . . . ?
C113 C114 C115 C116 0.0 . . . . ?
C114 C115 C116 C117 0.0 . . . . ?
C115 C116 C117 C118 0.0 . . . . ?
C116 C117 C118 C113 0.0 . . . . ?
C114 C113 C118 C117 0.0 . . . . ?
P1 C113 C118 C117 -178.2(6) . . . . ?
C107 P1 C119 C120 26.9(7) . . . . ?
C101 P1 C119 C120 -93.0(7) . . . . ?
C113 P1 C119 C120 147.9(6) . . . . ?
C107 P1 C119 C124 -157.4(6) . . . . ?
C101 P1 C119 C124 82.7(7) . . . . ?
C113 P1 C119 C124 -36.4(7) . . . . ?
C124 C119 C120 C121 0.0 . . . . ?
P1 C119 C120 C121 175.7(8) . . . . ?
C119 C120 C121 C122 0.0 . . . . ?
C120 C121 C122 C123 0.0 . . . . ?
C121 C122 C123 C124 0.0 . . . . ?
C122 C123 C124 C119 0.0 . . . . ?
C120 C119 C124 C123 0.0 . . . . ?
P1 C119 C124 C123 -175.7(8) . . . . ?
C219 P2 C201 C202 -40.0(7) . . . . ?
C213 P2 C201 C202 80.5(6) . . . . ?
C207 P2 C201 C202 -158.8(5) . . . . ?
C219 P2 C201 C206 144.8(6) . . . . ?
C213 P2 C201 C206 -94.7(6) . . . . ?
C207 P2 C201 C206 26.0(7) . . . . ?
C206 C201 C202 C203 0.0 . . . . ?
P2 C201 C202 C203 -175.1(7) . . . . ?
C201 C202 C203 C204 0.0 . . . . ?
C202 C203 C204 C205 0.0 . . . . ?
C203 C204 C205 C206 0.0 . . . . ?
C204 C205 C206 C201 0.0 . . . . ?
C202 C201 C206 C205 0.0 . . . . ?
P2 C201 C206 C205 175.2(7) . . . . ?
C219 P2 C207 C208 -24.9(6) . . . . ?
C213 P2 C207 C208 -146.5(5) . . . . ?
C201 P2 C207 C208 93.0(6) . . . . ?
C219 P2 C207 C212 159.3(5) . . . . ?
C213 P2 C207 C212 37.7(6) . . . . ?
C201 P2 C207 C212 -82.8(6) . . . . ?
C212 C207 C208 C209 0.0 . . . . ?
P2 C207 C208 C209 -175.8(7) . . . . ?
C207 C208 C209 C210 0.0 . . . . ?
C208 C209 C210 C211 0.0 . . . . ?
C209 C210 C211 C212 0.0 . . . . ?
C210 C211 C212 C207 0.0 . . . . ?
C208 C207 C212 C211 0.0 . . . . ?
P2 C207 C212 C211 175.8(7) . . . . ?
C219 P2 C213 C214 90.3(5) . . . . ?
C207 P2 C213 C214 -149.3(5) . . . . ?
C201 P2 C213 C214 -28.1(6) . . . . ?
C219 P2 C213 C218 -87.8(5) . . . . ?
C207 P2 C213 C218 32.6(6) . . . . ?
C201 P2 C213 C218 153.8(5) . . . . ?
C218 C213 C214 C215 0.0 . . . . ?
P2 C213 C214 C215 -178.1(6) . . . . ?
C213 C214 C215 C216 0.0 . . . . ?
C214 C215 C216 C217 0.0 . . . . ?
C215 C216 C217 C218 0.0 . . . . ?
C216 C217 C218 C213 0.0 . . . . ?
C214 C213 C218 C217 0.0 . . . . ?
P2 C213 C218 C217 178.1(6) . . . . ?
C213 P2 C219 C220 -158.7(5) . . . . ?
C207 P2 C219 C220 80.5(6) . . . . ?
C201 P2 C219 C220 -39.2(6) . . . . ?
C213 P2 C219 C224 26.7(7) . . . . ?
C207 P2 C219 C224 -94.1(6) . . . . ?
C201 P2 C219 C224 146.2(5) . . . . ?
C224 C219 C220 C221 0.0 . . . . ?
P2 C219 C220 C221 -174.7(7) . . . . ?
C219 C220 C221 C222 0.0 . . . . ?
C220 C221 C222 C223 0.0 . . . . ?
C221 C222 C223 C224 0.0 . . . . ?
C222 C223 C224 C219 0.0 . . . . ?
C220 C219 C224 C223 0.0 . . . . ?
P2 C219 C224 C223 174.6(7) . . . . ?

_diffrn_measured_fraction_theta_max 0.999
_diffrn_reflns_theta_full        25.03
_diffrn_measured_fraction_theta_full 0.999
_refine_diff_density_max         3.210
_refine_diff_density_min         -2.852
_refine_diff_density_rms         0.239
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_3_4MeCN_1
_database_code_depnum_ccdc_archive 'CCDC 1439439'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C110 H92 Cl16 N4 O6 P4 Pt6 Sn6'
_chemical_formula_weight         4139.64

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   P2(1)/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   13.0696(5)
_cell_length_b                   18.9114(7)
_cell_length_c                   26.3812(10)
_cell_angle_alpha                90.00
_cell_angle_beta                 91.697(2)
_cell_angle_gamma                90.00
_cell_volume                     6517.6(4)
_cell_formula_units_Z            2
_cell_measurement_temperature    298(2)
_cell_measurement_reflns_used    9917
_cell_measurement_theta_min      2.154
_cell_measurement_theta_max      25.646

_exptl_crystal_description       prism
_exptl_crystal_colour            black
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.12
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.109
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3856
_exptl_absorpt_coefficient_mu    7.964
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.2856
_exptl_absorpt_correction_T_max  0.4483
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1734 (selected reflections only, before parameter refinement)
 R(int) = 0.0762 (selected reflections only, after parameter refinement)
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      298(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            100318
_diffrn_reflns_av_R_equivalents  0.0984
_diffrn_reflns_av_unetI/netI     0.0535
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_theta_min         1.54
_diffrn_reflns_theta_max         26.00
_reflns_number_total             12808
_reflns_number_gt                9356
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. The following restraints
 were applied (given as SHELXL lines): 
 isor .01 cl6 cl8 c204
 simu .01 p1 > c124
 simu .01 p2 > c224
 isor .01 n1 > c402
 simu .01 n1 > c402
 same n2 > c402
 dfix 1.14 n1 c301 n2 c401
 dfix 1.47 c301 c302 c401 c402
 The asymmetric unit of the unit cell contains one half of a cluster anion 
 (located on an inversion centre), two [PPh4]+ cations and two CH3CN molecules 
 (all located on general positions). Similar U restraints have been applied 
 to the [PPh4]+ cations (SIMU command in SHELXL, s.u. 0.01). The CH3CN 
 molecules have been restrained to isotropic behaviour (ISOR command in 
 SHELXL, s.u. 0.01), to have similar geometries (SAME command in SHELXL, 
 s.u. 0.02) and similar U parameters (SIMU command in SHELXL, s.u. 0.01). 
 Restraints to bond distances were applied as follow (s.u. 0.01): 1.14 Å 
 for C N and 1.47 Å for C C in CH3CN.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0338P)²+29.7216P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         12808
_refine_ls_number_parameters     685
_refine_ls_number_restraints     373
_refine_ls_R_factor_all          0.0702
_refine_ls_R_factor_gt           0.0399
_refine_ls_wR_factor_ref         0.1038
_refine_ls_wR_factor_gt          0.0855
_refine_ls_goodness_of_fit_ref   1.084
_refine_ls_restrained_S_all      1.083
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.08262(3) 0.624867(17) 0.497137(13) 0.03843(9) Uani 1 1 d . . .
Pt2 Pt 0.04096(3) 0.478280(17) 0.457458(12) 0.03661(9) Uani 1 1 d . . .
Pt3 Pt -0.10092(3) 0.601819(17) 0.451451(14) 0.04079(9) Uani 1 1 d . . .
Sn1 Sn 0.18056(5) 0.52338(3) 0.54365(2) 0.04431(16) Uani 1 1 d . . .
Sn2 Sn 0.08668(5) 0.58731(3) 0.39495(2) 0.04312(15) Uani 1 1 d . . .
Sn3 Sn -0.05172(5) 0.73495(3) 0.47764(3) 0.04814(17) Uani 1 1 d . . .
Cl1 Cl 0.3493(2) 0.51166(16) 0.51380(11) 0.0659(7) Uani 1 1 d . . .
Cl2 Cl 0.2268(2) 0.56485(16) 0.62686(10) 0.0656(7) Uani 1 1 d . . .
Cl3 Cl 0.0958(2) 0.70841(14) 0.36633(11) 0.0691(8) Uani 1 1 d . . .
Cl4 Cl 0.0167(2) 0.54545(16) 0.31595(10) 0.0698(8) Uani 1 1 d . . .
Cl5 Cl 0.2617(2) 0.56393(16) 0.37675(11) 0.0664(7) Uani 1 1 d . . .
Cl6 Cl 0.0667(3) 0.82885(14) 0.49278(15) 0.0853(10) Uani 1 1 d U . .
Cl7 Cl -0.1390(3) 0.80182(16) 0.41187(13) 0.0853(10) Uani 1 1 d . . .
Cl8 Cl -0.1624(3) 0.76814(18) 0.54297(15) 0.1060(13) Uani 1 1 d U . .
C1 C 0.1942(8) 0.6851(5) 0.5072(4) 0.061(3) Uani 1 1 d . . .
C2 C 0.0772(8) 0.4163(5) 0.4069(4) 0.055(3) Uani 1 1 d . . .
C3 C -0.2057(8) 0.6288(5) 0.4061(5) 0.063(3) Uani 1 1 d . . .
O1 O 0.2643(7) 0.7200(5) 0.5126(4) 0.107(3) Uani 1 1 d . . .
O2 O 0.0963(7) 0.3784(4) 0.3743(3) 0.077(2) Uani 1 1 d . . .
O3 O -0.2675(7) 0.6450(5) 0.3770(4) 0.110(4) Uani 1 1 d . . .
P1 P 0.3797(2) 0.30081(13) 0.28080(9) 0.0479(6) Uani 1 1 d . . .
C101 C 0.3357(8) 0.3770(5) 0.2462(4) 0.056(2) Uani 1 1 d U . .
C102 C 0.2887(9) 0.4319(6) 0.2710(4) 0.063(2) Uani 1 1 d U . .
H102 H 0.2870 0.4321 0.3062 0.075 Uiso 1 1 calc R . .
C103 C 0.2441(9) 0.4866(6) 0.2432(4) 0.069(3) Uani 1 1 d U . .
H103 H 0.2144 0.5247 0.2596 0.083 Uiso 1 1 calc R . .
C104 C 0.2443(10) 0.4839(6) 0.1917(4) 0.074(3) Uani 1 1 d U . .
H104 H 0.2122 0.5199 0.1732 0.089 Uiso 1 1 calc R . .
C105 C 0.2901(10) 0.4301(6) 0.1662(4) 0.073(3) Uani 1 1 d U . .
H105 H 0.2892 0.4293 0.1309 0.087 Uiso 1 1 calc R . .
C106 C 0.3373(9) 0.3775(6) 0.1939(4) 0.065(2) Uani 1 1 d U . .
H106 H 0.3710 0.3414 0.1771 0.078 Uiso 1 1 calc R . .
C107 C 0.4137(8) 0.3234(5) 0.3454(4) 0.048(2) Uani 1 1 d U . .
C108 C 0.5143(8) 0.3294(5) 0.3620(4) 0.058(2) Uani 1 1 d U . .
H108 H 0.5669 0.3208 0.3398 0.069 Uiso 1 1 calc R . .
C109 C 0.5369(10) 0.3482(6) 0.4112(4) 0.068(3) Uani 1 1 d U . .
H109 H 0.6048 0.3521 0.4224 0.081 Uiso 1 1 calc R . .
C110 C 0.4600(10) 0.3612(6) 0.4438(4) 0.071(3) Uani 1 1 d U . .
H110 H 0.4766 0.3742 0.4771 0.085 Uiso 1 1 calc R . .
C111 C 0.3595(10) 0.3558(6) 0.4288(4) 0.069(3) Uani 1 1 d U . .
H111 H 0.3075 0.3647 0.4512 0.083 Uiso 1 1 calc R . .
C112 C 0.3377(9) 0.3365(6) 0.3792(4) 0.062(2) Uani 1 1 d U . .
H112 H 0.2697 0.3322 0.3683 0.074 Uiso 1 1 calc R . .
C113 C 0.4906(8) 0.2655(5) 0.2510(4) 0.055(2) Uani 1 1 d U . .
C114 C 0.5022(9) 0.1932(5) 0.2453(4) 0.061(2) Uani 1 1 d U . .
H114 H 0.4495 0.1628 0.2538 0.073 Uiso 1 1 calc R . .
C115 C 0.5919(9) 0.1666(6) 0.2272(4) 0.069(3) Uani 1 1 d U . .
H115 H 0.5993 0.1182 0.2226 0.083 Uiso 1 1 calc R . .
C116 C 0.6701(10) 0.2113(6) 0.2159(4) 0.073(3) Uani 1 1 d U . .
H116 H 0.7314 0.1929 0.2047 0.087 Uiso 1 1 calc R . .
C117 C 0.6594(10) 0.2826(6) 0.2208(4) 0.072(3) Uani 1 1 d U . .
H117 H 0.7127 0.3127 0.2127 0.087 Uiso 1 1 calc R . .
C118 C 0.5682(9) 0.3103(6) 0.2382(4) 0.064(2) Uani 1 1 d U . .
H118 H 0.5599 0.3589 0.2410 0.077 Uiso 1 1 calc R . .
C119 C 0.2777(8) 0.2384(6) 0.2809(4) 0.059(2) Uani 1 1 d U . .
C120 C 0.2664(9) 0.1922(6) 0.3207(4) 0.068(3) Uani 1 1 d U . .
H120 H 0.3138 0.1920 0.3477 0.082 Uiso 1 1 calc R . .
C121 C 0.1832(10) 0.1455(6) 0.3203(5) 0.079(3) Uani 1 1 d U . .
H121 H 0.1744 0.1151 0.3475 0.094 Uiso 1 1 calc R . .
C122 C 0.1152(11) 0.1447(7) 0.2803(5) 0.085(3) Uani 1 1 d U . .
H122 H 0.0597 0.1139 0.2802 0.102 Uiso 1 1 calc R . .
C123 C 0.1283(11) 0.1885(7) 0.2407(5) 0.088(3) Uani 1 1 d U . .
H123 H 0.0831 0.1861 0.2128 0.106 Uiso 1 1 calc R . .
C124 C 0.2072(10) 0.2365(6) 0.2408(4) 0.075(3) Uani 1 1 d U . .
H124 H 0.2133 0.2678 0.2138 0.090 Uiso 1 1 calc R . .
P2 P 0.3243(2) 0.95530(14) 0.41050(10) 0.0551(7) Uani 1 1 d . . .
C201 C 0.4039(10) 0.8784(6) 0.4166(4) 0.067(3) Uani 1 1 d U . .
C202 C 0.5064(11) 0.8843(7) 0.4314(4) 0.078(3) Uani 1 1 d U . .
H202 H 0.5351 0.9286 0.4375 0.094 Uiso 1 1 calc R . .
C203 C 0.5660(12) 0.8236(8) 0.4372(5) 0.092(3) Uani 1 1 d U . .
H203 H 0.6348 0.8273 0.4468 0.110 Uiso 1 1 calc R . .
C204 C 0.5242(12) 0.7601(8) 0.4288(5) 0.094(3) Uani 1 1 d U . .
H204 H 0.5652 0.7201 0.4323 0.113 Uiso 1 1 calc R . .
C205 C 0.4225(12) 0.7520(7) 0.4151(5) 0.091(3) Uani 1 1 d U . .
H205 H 0.3944 0.7072 0.4102 0.109 Uiso 1 1 calc R . .
C206 C 0.3636(11) 0.8116(6) 0.4088(5) 0.079(3) Uani 1 1 d U . .
H206 H 0.2949 0.8069 0.3990 0.095 Uiso 1 1 calc R . .
C207 C 0.4050(9) 1.0304(6) 0.4004(4) 0.063(2) Uani 1 1 d U . .
C208 C 0.3986(9) 1.0903(6) 0.4308(4) 0.067(3) Uani 1 1 d U . .
H208 H 0.3505 1.0925 0.4561 0.080 Uiso 1 1 calc R . .
C209 C 0.4640(10) 1.1466(6) 0.4233(5) 0.077(3) Uani 1 1 d U . .
H209 H 0.4604 1.1866 0.4436 0.093 Uiso 1 1 calc R . .
C210 C 0.5338(11) 1.1434(7) 0.3860(5) 0.082(3) Uani 1 1 d U . .
H210 H 0.5773 1.1816 0.3811 0.098 Uiso 1 1 calc R . .
C211 C 0.5412(10) 1.0853(7) 0.3556(5) 0.080(3) Uani 1 1 d U . .
H211 H 0.5898 1.0838 0.3306 0.096 Uiso 1 1 calc R . .
C212 C 0.4760(10) 1.0287(6) 0.3623(5) 0.074(3) Uani 1 1 d U . .
H212 H 0.4796 0.9894 0.3412 0.089 Uiso 1 1 calc R . .
C213 C 0.2561(8) 0.9680(5) 0.4674(4) 0.053(2) Uani 1 1 d U . .
C214 C 0.2852(9) 0.9330(5) 0.5112(4) 0.059(2) Uani 1 1 d U . .
H214 H 0.3399 0.9015 0.5114 0.071 Uiso 1 1 calc R . .
C215 C 0.2321(9) 0.9452(6) 0.5553(4) 0.069(3) Uani 1 1 d U . .
H215 H 0.2486 0.9198 0.5846 0.082 Uiso 1 1 calc R . .
C216 C 0.1557(10) 0.9945(6) 0.5554(5) 0.072(3) Uani 1 1 d U . .
H216 H 0.1226 1.0046 0.5853 0.087 Uiso 1 1 calc R . .
C217 C 0.1282(10) 1.0284(6) 0.5123(5) 0.071(3) Uani 1 1 d U . .
H217 H 0.0745 1.0606 0.5125 0.085 Uiso 1 1 calc R . .
C218 C 0.1776(9) 1.0165(6) 0.4684(4) 0.065(2) Uani 1 1 d U . .
H218 H 0.1584 1.0410 0.4391 0.078 Uiso 1 1 calc R . .
C219 C 0.2323(9) 0.9446(5) 0.3595(4) 0.063(2) Uani 1 1 d U . .
C220 C 0.1410(10) 0.9098(6) 0.3680(5) 0.075(3) Uani 1 1 d U . .
H220 H 0.1271 0.8943 0.4006 0.089 Uiso 1 1 calc R . .
C221 C 0.0711(11) 0.8980(7) 0.3296(5) 0.083(3) Uani 1 1 d U . .
H221 H 0.0112 0.8733 0.3356 0.100 Uiso 1 1 calc R . .
C222 C 0.0900(11) 0.9226(7) 0.2820(5) 0.085(3) Uani 1 1 d U . .
H222 H 0.0411 0.9161 0.2560 0.102 Uiso 1 1 calc R . .
C223 C 0.1791(11) 0.9566(6) 0.2719(4) 0.078(3) Uani 1 1 d U . .
H223 H 0.1916 0.9721 0.2393 0.094 Uiso 1 1 calc R . .
C224 C 0.2505(10) 0.9676(6) 0.3105(4) 0.068(3) Uani 1 1 d U . .
H224 H 0.3115 0.9907 0.3037 0.082 Uiso 1 1 calc R . .
N1 N 0.7854(18) 0.1691(12) 0.3369(9) 0.212(8) Uani 1 1 d DU . .
C301 C 0.844(2) 0.2106(14) 0.3423(11) 0.199(8) Uani 1 1 d DU . .
C302 C 0.9202(19) 0.2654(13) 0.3461(10) 0.214(9) Uani 1 1 d DU . .
H30A H 0.9777 0.2488 0.3663 0.322 Uiso 1 1 calc R . .
H30B H 0.8916 0.3064 0.3618 0.322 Uiso 1 1 calc R . .
H30C H 0.9422 0.2774 0.3128 0.322 Uiso 1 1 calc R . .
N2 N 0.4480(11) -0.0024(7) 0.2299(5) 0.110(4) Uani 1 1 d DU . .
C401 C 0.4570(11) 0.0119(7) 0.1893(5) 0.083(3) Uani 1 1 d DU . .
C402 C 0.4752(11) 0.0300(7) 0.1374(5) 0.092(4) Uani 1 1 d DU . .
H40A H 0.4685 0.0802 0.1330 0.137 Uiso 1 1 calc R . .
H40B H 0.4263 0.0062 0.1156 0.137 Uiso 1 1 calc R . .
H40C H 0.5431 0.0157 0.1290 0.137 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.863(11) . ?
Pt1 Sn1 2.5951(7) . ?
Pt1 Pt3 2.6880(5) . ?
Pt1 Sn3 2.7618(7) . ?
Pt1 Sn2 2.7899(7) . ?
Pt1 Pt2 2.8219(5) 3_566 ?
Pt1 Pt2 3.0072(5) . ?
Pt2 C2 1.847(11) . ?
Pt2 Pt2 2.6461(7) 3_566 ?
Pt2 Sn2 2.7178(7) . ?
Pt2 Pt1 2.8219(5) 3_566 ?
Pt2 Sn1 2.8946(7) 3_566 ?
Pt2 Pt3 2.9278(5) 3_566 ?
Pt2 Pt3 2.9840(5) . ?
Pt2 Sn1 2.9968(7) . ?
Pt3 C3 1.864(11) . ?
Pt3 Sn1 2.5912(7) 3_566 ?
Pt3 Sn3 2.6838(7) . ?
Pt3 Sn2 2.9198(7) . ?
Pt3 Pt2 2.9278(5) 3_566 ?
Sn1 Cl1 2.374(3) . ?
Sn1 Cl2 2.392(3) . ?
Sn1 Pt3 2.5912(7) 3_566 ?
Sn1 Pt2 2.8946(7) 3_566 ?
Sn2 Cl4 2.386(3) . ?
Sn2 Cl5 2.392(3) . ?
Sn2 Cl3 2.416(3) . ?
Sn3 Cl8 2.368(3) . ?
Sn3 Cl6 2.381(3) . ?
Sn3 Cl7 2.407(3) . ?
C1 O1 1.135(12) . ?
C2 O2 1.154(11) . ?
C3 O3 1.140(12) . ?
P1 C119 1.781(11) . ?
P1 C101 1.790(10) . ?
P1 C113 1.798(11) . ?
P1 C107 1.800(9) . ?
C101 C102 1.381(14) . ?
C101 C106 1.382(14) . ?
C102 C103 1.388(15) . ?
C102 H102 0.9300 . ?
C103 C104 1.359(15) . ?
C103 H103 0.9300 . ?
C104 C105 1.369(16) . ?
C104 H104 0.9300 . ?
C105 C106 1.371(15) . ?
C105 H105 0.9300 . ?
C106 H106 0.9300 . ?
C107 C112 1.376(14) . ?
C107 C108 1.379(13) . ?
C108 C109 1.368(14) . ?
C108 H108 0.9300 . ?
C109 C110 1.364(16) . ?
C109 H109 0.9300 . ?
C110 C111 1.365(16) . ?
C110 H110 0.9300 . ?
C111 C112 1.380(14) . ?
C111 H111 0.9300 . ?
C112 H112 0.9300 . ?
C113 C118 1.371(14) . ?
C113 C114 1.384(13) . ?
C114 C115 1.374(15) . ?
C114 H114 0.9300 . ?
C115 C116 1.367(16) . ?
C115 H115 0.9300 . ?
C116 C117 1.362(15) . ?
C116 H116 0.9300 . ?
C117 C118 1.391(15) . ?
C117 H117 0.9300 . ?
C118 H118 0.9300 . ?
C119 C120 1.376(14) . ?
C119 C124 1.383(14) . ?
C120 C121 1.400(15) . ?
C120 H120 0.9300 . ?
C121 C122 1.360(17) . ?
C121 H121 0.9300 . ?
C122 C123 1.348(17) . ?
C122 H122 0.9300 . ?
C123 C124 1.375(16) . ?
C123 H123 0.9300 . ?
C124 H124 0.9300 . ?
P2 C213 1.785(10) . ?
P2 C219 1.788(11) . ?
P2 C201 1.792(11) . ?
P2 C207 1.795(11) . ?
C201 C206 1.382(16) . ?
C201 C202 1.390(17) . ?
C202 C203 1.394(17) . ?
C202 H202 0.9300 . ?
C203 C204 1.334(19) . ?
C203 H203 0.9300 . ?
C204 C205 1.38(2) . ?
C204 H204 0.9300 . ?
C205 C206 1.372(16) . ?
C205 H205 0.9300 . ?
C206 H206 0.9300 . ?
C207 C212 1.388(16) . ?
C207 C208 1.392(15) . ?
C208 C209 1.384(16) . ?
C208 H208 0.9300 . ?
C209 C210 1.362(18) . ?
C209 H209 0.9300 . ?
C210 C211 1.366(18) . ?
C210 H210 0.9300 . ?
C211 C212 1.383(16) . ?
C211 H211 0.9300 . ?
C212 H212 0.9300 . ?
C213 C214 1.375(13) . ?
C213 C218 1.377(14) . ?
C214 C215 1.390(15) . ?
C214 H214 0.9300 . ?
C215 C216 1.366(16) . ?
C215 H215 0.9300 . ?
C216 C217 1.346(16) . ?
C216 H216 0.9300 . ?
C217 C218 1.361(15) . ?
C217 H217 0.9300 . ?
C218 H218 0.9300 . ?
C219 C220 1.387(16) . ?
C219 C224 1.392(14) . ?
C220 C221 1.363(16) . ?
C220 H220 0.9300 . ?
C221 C222 1.368(17) . ?
C221 H221 0.9300 . ?
C222 C223 1.363(18) . ?
C222 H222 0.9300 . ?
C223 C224 1.376(16) . ?
C223 H223 0.9300 . ?
C224 H224 0.9300 . ?
N1 C301 1.103(13) . ?
C301 C302 1.439(14) . ?
C302 H30A 0.9600 . ?
C302 H30B 0.9600 . ?
C302 H30C 0.9600 . ?
N2 C401 1.115(11) . ?
C401 C402 1.437(12) . ?
C402 H40A 0.9600 . ?
C402 H40B 0.9600 . ?
C402 H40C 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 Sn1 90.7(3) . . ?
C1 Pt1 Pt3 147.9(3) . . ?
Sn1 Pt1 Pt3 120.877(19) . . ?
C1 Pt1 Sn3 93.2(3) . . ?
Sn1 Pt1 Sn3 161.35(3) . . ?
Pt3 Pt1 Sn3 58.986(17) . . ?
C1 Pt1 Sn2 104.8(4) . . ?
Sn1 Pt1 Sn2 104.20(2) . . ?
Pt3 Pt1 Sn2 64.388(17) . . ?
Sn3 Pt1 Sn2 92.41(2) . . ?
C1 Pt1 Pt2 144.8(3) . 3_566 ?
Sn1 Pt1 Pt2 64.442(17) . 3_566 ?
Pt3 Pt1 Pt2 64.142(13) . 3_566 ?
Sn3 Pt1 Pt2 103.380(19) . 3_566 ?
Sn2 Pt1 Pt2 105.170(18) . 3_566 ?
C1 Pt1 Pt2 138.2(3) . . ?
Sn1 Pt1 Pt2 64.183(17) . . ?
Pt3 Pt1 Pt2 62.901(12) . . ?
Sn3 Pt1 Pt2 121.497(19) . . ?
Sn2 Pt1 Pt2 55.762(15) . . ?
Pt2 Pt1 Pt2 53.880(13) 3_566 . ?
C2 Pt2 Pt2 158.1(3) . 3_566 ?
C2 Pt2 Sn2 88.7(3) . . ?
Pt2 Pt2 Sn2 112.39(2) 3_566 . ?
C2 Pt2 Pt1 91.7(3) . 3_566 ?
Pt2 Pt2 Pt1 66.639(15) 3_566 3_566 ?
Sn2 Pt2 Pt1 157.06(2) . 3_566 ?
C2 Pt2 Sn1 105.3(3) . 3_566 ?
Pt2 Pt2 Sn1 65.305(19) 3_566 3_566 ?
Sn2 Pt2 Sn1 103.88(2) . 3_566 ?
Pt1 Pt2 Sn1 53.978(15) 3_566 3_566 ?
C2 Pt2 Pt3 101.3(3) . 3_566 ?
Pt2 Pt2 Pt3 64.504(15) 3_566 3_566 ?
Sn2 Pt2 Pt3 146.33(2) . 3_566 ?
Pt1 Pt2 Pt3 55.708(12) 3_566 3_566 ?
Sn1 Pt2 Pt3 104.238(18) 3_566 3_566 ?
C2 Pt2 Pt3 129.1(3) . . ?
Pt2 Pt2 Pt3 62.327(14) 3_566 . ?
Sn2 Pt2 Pt3 61.396(17) . . ?
Pt1 Pt2 Pt3 101.606(14) 3_566 . ?
Sn1 Pt2 Pt3 52.280(15) 3_566 . ?
Pt3 Pt2 Pt3 126.831(13) 3_566 . ?
C2 Pt2 Sn1 124.4(3) . . ?
Pt2 Pt2 Sn1 61.352(18) 3_566 . ?
Sn2 Pt2 Sn1 96.00(2) . . ?
Pt1 Pt2 Sn1 102.588(17) 3_566 . ?
Sn1 Pt2 Sn1 126.657(16) 3_566 . ?
Pt3 Pt2 Sn1 51.855(15) 3_566 . ?
Pt3 Pt2 Sn1 100.421(17) . . ?
C2 Pt2 Pt1 142.0(3) . . ?
Pt2 Pt2 Pt1 59.481(14) 3_566 . ?
Sn2 Pt2 Pt1 58.066(16) . . ?
Pt1 Pt2 Pt1 126.120(13) 3_566 . ?
Sn1 Pt2 Pt1 100.617(17) 3_566 . ?
Pt3 Pt2 Pt1 98.623(14) 3_566 . ?
Pt3 Pt2 Pt1 53.314(11) . . ?
Sn1 Pt2 Pt1 51.217(14) . . ?
C3 Pt3 Sn1 89.6(3) . 3_566 ?
C3 Pt3 Sn3 94.3(3) . . ?
Sn1 Pt3 Sn3 159.70(3) 3_566 . ?
C3 Pt3 Pt1 150.8(3) . . ?
Sn1 Pt3 Pt1 118.70(2) 3_566 . ?
Sn3 Pt3 Pt1 61.878(18) . . ?
C3 Pt3 Sn2 108.1(4) . . ?
Sn1 Pt3 Sn2 106.51(2) 3_566 . ?
Sn3 Pt3 Sn2 91.21(2) . . ?
Pt1 Pt3 Sn2 59.498(16) . . ?
C3 Pt3 Pt2 147.4(3) . 3_566 ?
Sn1 Pt3 Pt2 65.444(17) 3_566 3_566 ?
Sn3 Pt3 Pt2 102.581(19) . 3_566 ?
Pt1 Pt3 Pt2 60.150(12) . 3_566 ?
Sn2 Pt3 Pt2 99.323(17) . 3_566 ?
C3 Pt3 Pt2 133.8(3) . . ?
Sn1 Pt3 Pt2 62.086(17) 3_566 . ?
Sn3 Pt3 Pt2 125.24(2) . . ?
Pt1 Pt3 Pt2 63.785(12) . . ?
Sn2 Pt3 Pt2 54.805(15) . . ?
Pt2 Pt3 Pt2 53.169(13) 3_566 . ?
Cl1 Sn1 Cl2 97.08(10) . . ?
Cl1 Sn1 Pt3 108.04(7) . 3_566 ?
Cl2 Sn1 Pt3 110.16(8) . 3_566 ?
Cl1 Sn1 Pt1 111.24(8) . . ?
Cl2 Sn1 Pt1 107.40(7) . . ?
Pt3 Sn1 Pt1 120.41(3) 3_566 . ?
Cl1 Sn1 Pt2 159.13(7) . 3_566 ?
Cl2 Sn1 Pt2 103.77(7) . 3_566 ?
Pt3 Sn1 Pt2 65.634(17) 3_566 3_566 ?
Pt1 Sn1 Pt2 61.580(17) . 3_566 ?
Cl1 Sn1 Pt2 105.81(7) . . ?
Cl2 Sn1 Pt2 157.11(7) . . ?
Pt3 Sn1 Pt2 62.701(16) 3_566 . ?
Pt1 Sn1 Pt2 64.599(17) . . ?
Pt2 Sn1 Pt2 53.343(16) 3_566 . ?
Cl4 Sn2 Cl5 96.18(11) . . ?
Cl4 Sn2 Cl3 93.60(10) . . ?
Cl5 Sn2 Cl3 93.22(10) . . ?
Cl4 Sn2 Pt2 101.11(8) . . ?
Cl5 Sn2 Pt2 102.14(7) . . ?
Cl3 Sn2 Pt2 157.33(7) . . ?
Cl4 Sn2 Pt1 155.59(8) . . ?
Cl5 Sn2 Pt1 106.66(7) . . ?
Cl3 Sn2 Pt1 93.62(7) . . ?
Pt2 Sn2 Pt1 66.172(17) . . ?
Cl4 Sn2 Pt3 99.84(8) . . ?
Cl5 Sn2 Pt3 160.42(7) . . ?
Cl3 Sn2 Pt3 96.92(7) . . ?
Pt2 Sn2 Pt3 63.799(16) . . ?
Pt1 Sn2 Pt3 56.115(15) . . ?
Cl8 Sn3 Cl6 95.06(14) . . ?
Cl8 Sn3 Cl7 95.66(14) . . ?
Cl6 Sn3 Cl7 91.19(12) . . ?
Cl8 Sn3 Pt3 106.81(10) . . ?
Cl6 Sn3 Pt3 153.16(9) . . ?
Cl7 Sn3 Pt3 101.69(8) . . ?
Cl8 Sn3 Pt1 117.59(10) . . ?
Cl6 Sn3 Pt1 97.15(8) . . ?
Cl7 Sn3 Pt1 144.63(9) . . ?
Pt3 Sn3 Pt1 59.136(16) . . ?
O1 C1 Pt1 177.6(12) . . ?
O2 C2 Pt2 177.3(10) . . ?
O3 C3 Pt3 177.6(12) . . ?
C119 P1 C101 107.8(5) . . ?
C119 P1 C113 111.6(5) . . ?
C101 P1 C113 109.1(5) . . ?
C119 P1 C107 108.6(5) . . ?
C101 P1 C107 111.0(5) . . ?
C113 P1 C107 108.8(5) . . ?
C102 C101 C106 119.2(10) . . ?
C102 C101 P1 120.3(8) . . ?
C106 C101 P1 120.0(8) . . ?
C101 C102 C103 119.8(10) . . ?
C101 C102 H102 120.1 . . ?
C103 C102 H102 120.1 . . ?
C104 C103 C102 119.1(11) . . ?
C104 C103 H103 120.4 . . ?
C102 C103 H103 120.4 . . ?
C103 C104 C105 122.3(11) . . ?
C103 C104 H104 118.9 . . ?
C105 C104 H104 118.9 . . ?
C104 C105 C106 118.3(11) . . ?
C104 C105 H105 120.9 . . ?
C106 C105 H105 120.9 . . ?
C105 C106 C101 121.2(11) . . ?
C105 C106 H106 119.4 . . ?
C101 C106 H106 119.4 . . ?
C112 C107 C108 118.6(9) . . ?
C112 C107 P1 119.6(8) . . ?
C108 C107 P1 121.8(8) . . ?
C109 C108 C107 119.9(10) . . ?
C109 C108 H108 120.0 . . ?
C107 C108 H108 120.0 . . ?
C110 C109 C108 120.2(11) . . ?
C110 C109 H109 119.9 . . ?
C108 C109 H109 119.9 . . ?
C109 C110 C111 121.6(11) . . ?
C109 C110 H110 119.2 . . ?
C111 C110 H110 119.2 . . ?
C110 C111 C112 117.7(11) . . ?
C110 C111 H111 121.2 . . ?
C112 C111 H111 121.2 . . ?
C107 C112 C111 121.9(11) . . ?
C107 C112 H112 119.0 . . ?
C111 C112 H112 119.0 . . ?
C118 C113 C114 120.0(10) . . ?
C118 C113 P1 119.3(8) . . ?
C114 C113 P1 120.4(8) . . ?
C115 C114 C113 119.7(11) . . ?
C115 C114 H114 120.1 . . ?
C113 C114 H114 120.1 . . ?
C116 C115 C114 120.1(11) . . ?
C116 C115 H115 120.0 . . ?
C114 C115 H115 120.0 . . ?
C117 C116 C115 120.8(12) . . ?
C117 C116 H116 119.6 . . ?
C115 C116 H116 119.6 . . ?
C116 C117 C118 119.7(12) . . ?
C116 C117 H117 120.2 . . ?
C118 C117 H117 120.2 . . ?
C113 C118 C117 119.7(10) . . ?
C113 C118 H118 120.1 . . ?
C117 C118 H118 120.1 . . ?
C120 C119 C124 118.9(11) . . ?
C120 C119 P1 121.3(8) . . ?
C124 C119 P1 119.8(9) . . ?
C119 C120 C121 119.7(11) . . ?
C119 C120 H120 120.1 . . ?
C121 C120 H120 120.1 . . ?
C122 C121 C120 120.2(12) . . ?
C122 C121 H121 119.9 . . ?
C120 C121 H121 119.9 . . ?
C123 C122 C121 120.0(13) . . ?
C123 C122 H122 120.0 . . ?
C121 C122 H122 120.0 . . ?
C122 C123 C124 121.1(12) . . ?
C122 C123 H123 119.4 . . ?
C124 C123 H123 119.4 . . ?
C123 C124 C119 120.0(12) . . ?
C123 C124 H124 120.0 . . ?
C119 C124 H124 120.0 . . ?
C213 P2 C219 107.9(5) . . ?
C213 P2 C201 109.6(5) . . ?
C219 P2 C201 110.6(5) . . ?
C213 P2 C207 109.2(5) . . ?
C219 P2 C207 111.3(5) . . ?
C201 P2 C207 108.3(6) . . ?
C206 C201 C202 118.4(11) . . ?
C206 C201 P2 120.7(10) . . ?
C202 C201 P2 120.8(10) . . ?
C201 C202 C203 119.7(13) . . ?
C201 C202 H202 120.2 . . ?
C203 C202 H202 120.2 . . ?
C204 C203 C202 119.9(15) . . ?
C204 C203 H203 120.1 . . ?
C202 C203 H203 120.1 . . ?
C203 C204 C205 122.2(14) . . ?
C203 C204 H204 118.9 . . ?
C205 C204 H204 118.9 . . ?
C206 C205 C204 118.3(14) . . ?
C206 C205 H205 120.9 . . ?
C204 C205 H205 120.9 . . ?
C205 C206 C201 121.5(14) . . ?
C205 C206 H206 119.2 . . ?
C201 C206 H206 119.2 . . ?
C212 C207 C208 119.4(11) . . ?
C212 C207 P2 119.8(9) . . ?
C208 C207 P2 120.8(9) . . ?
C209 C208 C207 119.7(12) . . ?
C209 C208 H208 120.2 . . ?
C207 C208 H208 120.2 . . ?
C210 C209 C208 119.9(13) . . ?
C210 C209 H209 120.0 . . ?
C208 C209 H209 120.0 . . ?
C209 C210 C211 121.4(13) . . ?
C209 C210 H210 119.3 . . ?
C211 C210 H210 119.3 . . ?
C210 C211 C212 119.6(13) . . ?
C210 C211 H211 120.2 . . ?
C212 C211 H211 120.2 . . ?
C211 C212 C207 120.0(12) . . ?
C211 C212 H212 120.0 . . ?
C207 C212 H212 120.0 . . ?
C214 C213 C218 119.5(10) . . ?
C214 C213 P2 120.7(8) . . ?
C218 C213 P2 119.7(8) . . ?
C213 C214 C215 119.4(10) . . ?
C213 C214 H214 120.3 . . ?
C215 C214 H214 120.3 . . ?
C216 C215 C214 119.9(11) . . ?
C216 C215 H215 120.1 . . ?
C214 C215 H215 120.1 . . ?
C217 C216 C215 120.0(11) . . ?
C217 C216 H216 120.0 . . ?
C215 C216 H216 120.0 . . ?
C216 C217 C218 121.2(12) . . ?
C216 C217 H217 119.4 . . ?
C218 C217 H217 119.4 . . ?
C217 C218 C213 119.9(11) . . ?
C217 C218 H218 120.0 . . ?
C213 C218 H218 120.0 . . ?
C220 C219 C224 118.0(11) . . ?
C220 C219 P2 119.6(8) . . ?
C224 C219 P2 122.3(10) . . ?
C221 C220 C219 121.2(12) . . ?
C221 C220 H220 119.4 . . ?
C219 C220 H220 119.4 . . ?
C220 C221 C222 119.5(14) . . ?
C220 C221 H221 120.3 . . ?
C222 C221 H221 120.3 . . ?
C223 C222 C221 121.1(13) . . ?
C223 C222 H222 119.5 . . ?
C221 C222 H222 119.5 . . ?
C222 C223 C224 119.6(12) . . ?
C222 C223 H223 120.2 . . ?
C224 C223 H223 120.2 . . ?
C223 C224 C219 120.5(12) . . ?
C223 C224 H224 119.7 . . ?
C219 C224 H224 119.7 . . ?
N1 C301 C302 177(4) . . ?
C301 C302 H30A 109.5 . . ?
C301 C302 H30B 109.5 . . ?
H30A C302 H30B 109.5 . . ?
C301 C302 H30C 109.5 . . ?
H30A C302 H30C 109.5 . . ?
H30B C302 H30C 109.5 . . ?
N2 C401 C402 176.5(17) . . ?
C401 C402 H40A 109.5 . . ?
C401 C402 H40B 109.5 . . ?
H40A C402 H40B 109.5 . . ?
C401 C402 H40C 109.5 . . ?
H40A C402 H40C 109.5 . . ?
H40B C402 H40C 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 Pt2 C2 -40.0(7) . . . . ?
Sn1 Pt1 Pt2 C2 -98.5(5) . . . . ?
Pt3 Pt1 Pt2 C2 108.9(5) . . . . ?
Sn3 Pt1 Pt2 C2 101.8(5) . . . . ?
Sn2 Pt1 Pt2 C2 32.7(5) . . . . ?
Pt2 Pt1 Pt2 C2 -174.6(5) 3_566 . . . ?
C1 Pt1 Pt2 Pt2 134.6(5) . . . 3_566 ?
Sn1 Pt1 Pt2 Pt2 76.10(2) . . . 3_566 ?
Pt3 Pt1 Pt2 Pt2 -76.521(16) . . . 3_566 ?
Sn3 Pt1 Pt2 Pt2 -83.62(3) . . . 3_566 ?
Sn2 Pt1 Pt2 Pt2 -152.69(2) . . . 3_566 ?
C1 Pt1 Pt2 Sn2 -72.7(5) . . . . ?
Sn1 Pt1 Pt2 Sn2 -131.22(3) . . . . ?
Pt3 Pt1 Pt2 Sn2 76.17(2) . . . . ?
Sn3 Pt1 Pt2 Sn2 69.07(3) . . . . ?
Pt2 Pt1 Pt2 Sn2 152.69(2) 3_566 . . . ?
C1 Pt1 Pt2 Pt1 134.6(5) . . . 3_566 ?
Sn1 Pt1 Pt2 Pt1 76.10(2) . . . 3_566 ?
Pt3 Pt1 Pt2 Pt1 -76.520(16) . . . 3_566 ?
Sn3 Pt1 Pt2 Pt1 -83.62(3) . . . 3_566 ?
Sn2 Pt1 Pt2 Pt1 -152.69(2) . . . 3_566 ?
Pt2 Pt1 Pt2 Pt1 0.0 3_566 . . 3_566 ?
C1 Pt1 Pt2 Sn1 -172.6(5) . . . 3_566 ?
Sn1 Pt1 Pt2 Sn1 128.946(16) . . . 3_566 ?
Pt3 Pt1 Pt2 Sn1 -23.672(18) . . . 3_566 ?
Sn3 Pt1 Pt2 Sn1 -30.77(3) . . . 3_566 ?
Sn2 Pt1 Pt2 Sn1 -99.84(2) . . . 3_566 ?
Pt2 Pt1 Pt2 Sn1 52.848(17) 3_566 . . 3_566 ?
C1 Pt1 Pt2 Pt3 81.1(5) . . . 3_566 ?
Sn1 Pt1 Pt2 Pt3 22.59(2) . . . 3_566 ?
Pt3 Pt1 Pt2 Pt3 -130.023(13) . . . 3_566 ?
Sn3 Pt1 Pt2 Pt3 -137.12(2) . . . 3_566 ?
Sn2 Pt1 Pt2 Pt3 153.81(2) . . . 3_566 ?
Pt2 Pt1 Pt2 Pt3 -53.503(14) 3_566 . . 3_566 ?
C1 Pt1 Pt2 Pt3 -148.9(5) . . . . ?
Sn1 Pt1 Pt2 Pt3 152.62(2) . . . . ?
Sn3 Pt1 Pt2 Pt3 -7.10(2) . . . . ?
Sn2 Pt1 Pt2 Pt3 -76.17(2) . . . . ?
Pt2 Pt1 Pt2 Pt3 76.521(16) 3_566 . . . ?
C1 Pt1 Pt2 Sn1 58.5(5) . . . . ?
Pt3 Pt1 Pt2 Sn1 -152.62(2) . . . . ?
Sn3 Pt1 Pt2 Sn1 -159.72(3) . . . . ?
Sn2 Pt1 Pt2 Sn1 131.22(3) . . . . ?
Pt2 Pt1 Pt2 Sn1 -76.10(2) 3_566 . . . ?
C1 Pt1 Pt3 C3 5.1(10) . . . . ?
Sn1 Pt1 Pt3 C3 -163.3(8) . . . . ?
Sn3 Pt1 Pt3 C3 38.5(8) . . . . ?
Sn2 Pt1 Pt3 C3 -71.6(8) . . . . ?
Pt2 Pt1 Pt3 C3 164.7(8) 3_566 . . . ?
Pt2 Pt1 Pt3 C3 -134.5(8) . . . . ?
C1 Pt1 Pt3 Sn1 169.8(7) . . . 3_566 ?
Sn1 Pt1 Pt3 Sn1 1.33(4) . . . 3_566 ?
Sn3 Pt1 Pt3 Sn1 -156.89(3) . . . 3_566 ?
Sn2 Pt1 Pt3 Sn1 93.07(3) . . . 3_566 ?
Pt2 Pt1 Pt3 Sn1 -30.63(2) 3_566 . . 3_566 ?
Pt2 Pt1 Pt3 Sn1 30.17(2) . . . 3_566 ?
C1 Pt1 Pt3 Sn3 -33.3(7) . . . . ?
Sn1 Pt1 Pt3 Sn3 158.22(3) . . . . ?
Sn2 Pt1 Pt3 Sn3 -110.04(2) . . . . ?
Pt2 Pt1 Pt3 Sn3 126.26(2) 3_566 . . . ?
Pt2 Pt1 Pt3 Sn3 -172.94(2) . . . . ?
C1 Pt1 Pt3 Sn2 76.7(7) . . . . ?
Sn1 Pt1 Pt3 Sn2 -91.74(3) . . . . ?
Sn3 Pt1 Pt3 Sn2 110.04(2) . . . . ?
Pt2 Pt1 Pt3 Sn2 -123.700(18) 3_566 . . . ?
Pt2 Pt1 Pt3 Sn2 -62.898(17) . . . . ?
C1 Pt1 Pt3 Pt2 -159.6(7) . . . 3_566 ?
Sn1 Pt1 Pt3 Pt2 31.96(2) . . . 3_566 ?
Sn3 Pt1 Pt3 Pt2 -126.26(2) . . . 3_566 ?
Sn2 Pt1 Pt3 Pt2 123.700(18) . . . 3_566 ?
Pt2 Pt1 Pt3 Pt2 60.802(14) . . . 3_566 ?
C1 Pt1 Pt3 Pt2 139.6(7) . . . . ?
Sn1 Pt1 Pt3 Pt2 -28.84(2) . . . . ?
Sn3 Pt1 Pt3 Pt2 172.94(2) . . . . ?
Sn2 Pt1 Pt3 Pt2 62.898(17) . . . . ?
Pt2 Pt1 Pt3 Pt2 -60.802(14) 3_566 . . . ?
C2 Pt2 Pt3 C3 19.7(6) . . . . ?
Pt2 Pt2 Pt3 C3 -137.8(5) 3_566 . . . ?
Sn2 Pt2 Pt3 C3 81.3(5) . . . . ?
Pt1 Pt2 Pt3 C3 -82.2(5) 3_566 . . . ?
Sn1 Pt2 Pt3 C3 -58.8(5) 3_566 . . . ?
Pt3 Pt2 Pt3 C3 -137.8(5) 3_566 . . . ?
Sn1 Pt2 Pt3 C3 172.5(5) . . . . ?
Pt1 Pt2 Pt3 C3 151.1(5) . . . . ?
C2 Pt2 Pt3 Sn1 78.5(4) . . . 3_566 ?
Pt2 Pt2 Pt3 Sn1 -79.00(2) 3_566 . . 3_566 ?
Sn2 Pt2 Pt3 Sn1 140.11(3) . . . 3_566 ?
Pt1 Pt2 Pt3 Sn1 -23.39(2) 3_566 . . 3_566 ?
Pt3 Pt2 Pt3 Sn1 -79.00(2) 3_566 . . 3_566 ?
Sn1 Pt2 Pt3 Sn1 -128.694(16) . . . 3_566 ?
Pt1 Pt2 Pt3 Sn1 -150.07(2) . . . 3_566 ?
C2 Pt2 Pt3 Sn3 -123.8(4) . . . . ?
Pt2 Pt2 Pt3 Sn3 78.70(3) 3_566 . . . ?
Sn2 Pt2 Pt3 Sn3 -62.19(3) . . . . ?
Pt1 Pt2 Pt3 Sn3 134.31(2) 3_566 . . . ?
Sn1 Pt2 Pt3 Sn3 157.70(3) 3_566 . . . ?
Pt3 Pt2 Pt3 Sn3 78.70(3) 3_566 . . . ?
Sn1 Pt2 Pt3 Sn3 29.01(3) . . . . ?
Pt1 Pt2 Pt3 Sn3 7.63(2) . . . . ?
C2 Pt2 Pt3 Pt1 -131.4(4) . . . . ?
Pt2 Pt2 Pt3 Pt1 71.072(16) 3_566 . . . ?
Sn2 Pt2 Pt3 Pt1 -69.815(19) . . . . ?
Pt1 Pt2 Pt3 Pt1 126.685(13) 3_566 . . . ?
Sn1 Pt2 Pt3 Pt1 150.07(2) 3_566 . . . ?
Pt3 Pt2 Pt3 Pt1 71.072(16) 3_566 . . . ?
Sn1 Pt2 Pt3 Pt1 21.379(17) . . . . ?
C2 Pt2 Pt3 Sn2 -61.6(4) . . . . ?
Pt2 Pt2 Pt3 Sn2 140.89(2) 3_566 . . . ?
Pt1 Pt2 Pt3 Sn2 -163.50(2) 3_566 . . . ?
Sn1 Pt2 Pt3 Sn2 -140.11(3) 3_566 . . . ?
Pt3 Pt2 Pt3 Sn2 140.89(2) 3_566 . . . ?
Sn1 Pt2 Pt3 Sn2 91.19(2) . . . . ?
Pt1 Pt2 Pt3 Sn2 69.815(19) . . . . ?
C2 Pt2 Pt3 Pt2 157.5(4) . . . 3_566 ?
Sn2 Pt2 Pt3 Pt2 -140.89(2) . . . 3_566 ?
Pt1 Pt2 Pt3 Pt2 55.613(13) 3_566 . . 3_566 ?
Sn1 Pt2 Pt3 Pt2 79.00(2) 3_566 . . 3_566 ?
Pt3 Pt2 Pt3 Pt2 0.0 3_566 . . 3_566 ?
Sn1 Pt2 Pt3 Pt2 -49.694(17) . . . 3_566 ?
Pt1 Pt2 Pt3 Pt2 -71.072(16) . . . 3_566 ?
C1 Pt1 Sn1 Cl1 -47.4(4) . . . . ?
Pt3 Pt1 Sn1 Cl1 126.49(7) . . . . ?
Sn3 Pt1 Sn1 Cl1 -149.58(9) . . . . ?
Sn2 Pt1 Sn1 Cl1 58.09(7) . . . . ?
Pt2 Pt1 Sn1 Cl1 158.36(7) 3_566 . . . ?
Pt2 Pt1 Sn1 Cl1 97.99(7) . . . . ?
C1 Pt1 Sn1 Cl2 57.7(4) . . . . ?
Pt3 Pt1 Sn1 Cl2 -128.42(8) . . . . ?
Sn3 Pt1 Sn1 Cl2 -44.49(11) . . . . ?
Sn2 Pt1 Sn1 Cl2 163.19(8) . . . . ?
Pt2 Pt1 Sn1 Cl2 -96.55(8) 3_566 . . . ?
Pt2 Pt1 Sn1 Cl2 -156.91(8) . . . . ?
C1 Pt1 Sn1 Pt3 -175.2(4) . . . 3_566 ?
Pt3 Pt1 Sn1 Pt3 -1.35(4) . . . 3_566 ?
Sn3 Pt1 Sn1 Pt3 82.58(8) . . . 3_566 ?
Sn2 Pt1 Sn1 Pt3 -69.75(3) . . . 3_566 ?
Pt2 Pt1 Sn1 Pt3 30.52(3) 3_566 . . 3_566 ?
Pt2 Pt1 Sn1 Pt3 -29.85(2) . . . 3_566 ?
C1 Pt1 Sn1 Pt2 154.2(4) . . . 3_566 ?
Pt3 Pt1 Sn1 Pt2 -31.87(2) . . . 3_566 ?
Sn3 Pt1 Sn1 Pt2 52.06(7) . . . 3_566 ?
Sn2 Pt1 Sn1 Pt2 -100.26(2) . . . 3_566 ?
Pt2 Pt1 Sn1 Pt2 -60.363(15) . . . 3_566 ?
C1 Pt1 Sn1 Pt2 -145.4(4) . . . . ?
Pt3 Pt1 Sn1 Pt2 28.49(2) . . . . ?
Sn3 Pt1 Sn1 Pt2 112.43(7) . . . . ?
Sn2 Pt1 Sn1 Pt2 -39.902(19) . . . . ?
Pt2 Pt1 Sn1 Pt2 60.363(15) 3_566 . . . ?
C2 Pt2 Sn1 Cl1 26.1(4) . . . . ?
Pt2 Pt2 Sn1 Cl1 -178.74(8) 3_566 . . . ?
Sn2 Pt2 Sn1 Cl1 -66.47(8) . . . . ?
Pt1 Pt2 Sn1 Cl1 127.06(8) 3_566 . . . ?
Sn1 Pt2 Sn1 Cl1 -178.74(8) 3_566 . . . ?
Pt3 Pt2 Sn1 Cl1 102.48(8) 3_566 . . . ?
Pt3 Pt2 Sn1 Cl1 -128.43(8) . . . . ?
Pt1 Pt2 Sn1 Cl1 -106.40(8) . . . . ?
C2 Pt2 Sn1 Cl2 -153.4(4) . . . . ?
Pt2 Pt2 Sn1 Cl2 1.79(19) 3_566 . . . ?
Sn2 Pt2 Sn1 Cl2 114.1(2) . . . . ?
Pt1 Pt2 Sn1 Cl2 -52.4(2) 3_566 . . . ?
Sn1 Pt2 Sn1 Cl2 1.79(19) 3_566 . . . ?
Pt3 Pt2 Sn1 Cl2 -77.0(2) 3_566 . . . ?
Pt3 Pt2 Sn1 Cl2 52.1(2) . . . . ?
Pt1 Pt2 Sn1 Cl2 74.13(19) . . . . ?
C2 Pt2 Sn1 Pt3 -76.4(4) . . . 3_566 ?
Pt2 Pt2 Sn1 Pt3 78.777(19) 3_566 . . 3_566 ?
Sn2 Pt2 Sn1 Pt3 -168.95(2) . . . 3_566 ?
Pt1 Pt2 Sn1 Pt3 24.577(18) 3_566 . . 3_566 ?
Sn1 Pt2 Sn1 Pt3 78.777(19) 3_566 . . 3_566 ?
Pt3 Pt2 Sn1 Pt3 129.093(15) . . . 3_566 ?
Pt1 Pt2 Sn1 Pt3 151.12(2) . . . 3_566 ?
C2 Pt2 Sn1 Pt1 132.5(4) . . . . ?
Pt2 Pt2 Sn1 Pt1 -72.341(18) 3_566 . . . ?
Sn2 Pt2 Sn1 Pt1 39.93(2) . . . . ?
Pt1 Pt2 Sn1 Pt1 -126.541(15) 3_566 . . . ?
Sn1 Pt2 Sn1 Pt1 -72.341(18) 3_566 . . . ?
Pt3 Pt2 Sn1 Pt1 -151.12(2) 3_566 . . . ?
Pt3 Pt2 Sn1 Pt1 -22.025(17) . . . . ?
C2 Pt2 Sn1 Pt2 -155.1(4) . . . 3_566 ?
Sn2 Pt2 Sn1 Pt2 112.27(2) . . . 3_566 ?
Pt1 Pt2 Sn1 Pt2 -54.200(15) 3_566 . . 3_566 ?
Sn1 Pt2 Sn1 Pt2 0.0 3_566 . . 3_566 ?
Pt3 Pt2 Sn1 Pt2 -78.777(19) 3_566 . . 3_566 ?
Pt3 Pt2 Sn1 Pt2 50.316(14) . . . 3_566 ?
Pt1 Pt2 Sn1 Pt2 72.341(18) . . . 3_566 ?
C2 Pt2 Sn2 Cl4 41.3(3) . . . . ?
Pt2 Pt2 Sn2 Cl4 -132.77(8) 3_566 . . . ?
Pt1 Pt2 Sn2 Cl4 -50.06(10) 3_566 . . . ?
Sn1 Pt2 Sn2 Cl4 -64.09(8) 3_566 . . . ?
Pt3 Pt2 Sn2 Cl4 150.01(8) 3_566 . . . ?
Pt3 Pt2 Sn2 Cl4 -95.60(8) . . . . ?
Sn1 Pt2 Sn2 Cl4 165.79(8) . . . . ?
Pt1 Pt2 Sn2 Cl4 -158.08(8) . . . . ?
C2 Pt2 Sn2 Cl5 -57.6(3) . . . . ?
Pt2 Pt2 Sn2 Cl5 128.35(8) 3_566 . . . ?
Pt1 Pt2 Sn2 Cl5 -148.94(8) 3_566 . . . ?
Sn1 Pt2 Sn2 Cl5 -162.98(8) 3_566 . . . ?
Pt3 Pt2 Sn2 Cl5 51.13(9) 3_566 . . . ?
Pt3 Pt2 Sn2 Cl5 165.52(8) . . . . ?
Sn1 Pt2 Sn2 Cl5 66.90(8) . . . . ?
Pt1 Pt2 Sn2 Cl5 103.03(8) . . . . ?
C2 Pt2 Sn2 Cl3 170.8(4) . . . . ?
Pt2 Pt2 Sn2 Cl3 -3.3(2) 3_566 . . . ?
Pt1 Pt2 Sn2 Cl3 79.5(2) 3_566 . . . ?
Sn1 Pt2 Sn2 Cl3 65.4(2) 3_566 . . . ?
Pt3 Pt2 Sn2 Cl3 -80.5(2) 3_566 . . . ?
Pt3 Pt2 Sn2 Cl3 33.9(2) . . . . ?
Sn1 Pt2 Sn2 Cl3 -64.7(2) . . . . ?
Pt1 Pt2 Sn2 Cl3 -28.6(2) . . . . ?
C2 Pt2 Sn2 Pt1 -160.6(3) . . . . ?
Pt2 Pt2 Sn2 Pt1 25.31(2) 3_566 . . . ?
Pt1 Pt2 Sn2 Pt1 108.03(5) 3_566 . . . ?
Sn1 Pt2 Sn2 Pt1 93.99(2) 3_566 . . . ?
Pt3 Pt2 Sn2 Pt1 -51.91(4) 3_566 . . . ?
Pt3 Pt2 Sn2 Pt1 62.486(14) . . . . ?
Sn1 Pt2 Sn2 Pt1 -36.129(18) . . . . ?
C2 Pt2 Sn2 Pt3 136.9(3) . . . . ?
Pt2 Pt2 Sn2 Pt3 -37.17(2) 3_566 . . . ?
Pt1 Pt2 Sn2 Pt3 45.54(5) 3_566 . . . ?
Sn1 Pt2 Sn2 Pt3 31.503(19) 3_566 . . . ?
Pt3 Pt2 Sn2 Pt3 -114.39(3) 3_566 . . . ?
Sn1 Pt2 Sn2 Pt3 -98.616(19) . . . . ?
Pt1 Pt2 Sn2 Pt3 -62.486(14) . . . . ?
C1 Pt1 Sn2 Cl4 -158.7(4) . . . . ?
Sn1 Pt1 Sn2 Cl4 106.71(18) . . . . ?
Pt3 Pt1 Sn2 Cl4 -11.05(18) . . . . ?
Sn3 Pt1 Sn2 Cl4 -64.74(18) . . . . ?
Pt2 Pt1 Sn2 Cl4 39.82(18) 3_566 . . . ?
Pt2 Pt1 Sn2 Cl4 62.40(18) . . . . ?
C1 Pt1 Sn2 Cl5 42.7(3) . . . . ?
Sn1 Pt1 Sn2 Cl5 -51.88(8) . . . . ?
Pt3 Pt1 Sn2 Cl5 -169.64(8) . . . . ?
Sn3 Pt1 Sn2 Cl5 136.66(8) . . . . ?
Pt2 Pt1 Sn2 Cl5 -118.77(8) 3_566 . . . ?
Pt2 Pt1 Sn2 Cl5 -96.19(8) . . . . ?
C1 Pt1 Sn2 Cl3 -51.8(3) . . . . ?
Sn1 Pt1 Sn2 Cl3 -146.34(8) . . . . ?
Pt3 Pt1 Sn2 Cl3 95.90(8) . . . . ?
Sn3 Pt1 Sn2 Cl3 42.21(8) . . . . ?
Pt2 Pt1 Sn2 Cl3 146.77(8) 3_566 . . . ?
Pt2 Pt1 Sn2 Cl3 169.36(8) . . . . ?
C1 Pt1 Sn2 Pt2 138.9(3) . . . . ?
Sn1 Pt1 Sn2 Pt2 44.31(2) . . . . ?
Pt3 Pt1 Sn2 Pt2 -73.452(15) . . . . ?
Sn3 Pt1 Sn2 Pt2 -127.15(2) . . . . ?
Pt2 Pt1 Sn2 Pt2 -22.59(2) 3_566 . . . ?
C1 Pt1 Sn2 Pt3 -147.7(3) . . . . ?
Sn1 Pt1 Sn2 Pt3 117.76(2) . . . . ?
Sn3 Pt1 Sn2 Pt3 -53.693(18) . . . . ?
Pt2 Pt1 Sn2 Pt3 50.867(15) 3_566 . . . ?
Pt2 Pt1 Sn2 Pt3 73.452(15) . . . . ?
C3 Pt3 Sn2 Cl4 -33.8(3) . . . . ?
Sn1 Pt3 Sn2 Cl4 61.39(8) 3_566 . . . ?
Sn3 Pt3 Sn2 Cl4 -128.64(7) . . . . ?
Pt1 Pt3 Sn2 Cl4 175.39(8) . . . . ?
Pt2 Pt3 Sn2 Cl4 128.40(7) 3_566 . . . ?
Pt2 Pt3 Sn2 Cl4 97.62(7) . . . . ?
C3 Pt3 Sn2 Cl5 -178.2(4) . . . . ?
Sn1 Pt3 Sn2 Cl5 -83.1(2) 3_566 . . . ?
Sn3 Pt3 Sn2 Cl5 86.9(2) . . . . ?
Pt1 Pt3 Sn2 Cl5 30.9(2) . . . . ?
Pt2 Pt3 Sn2 Cl5 -16.1(2) 3_566 . . . ?
Pt2 Pt3 Sn2 Cl5 -46.8(2) . . . . ?
C3 Pt3 Sn2 Cl3 61.1(3) . . . . ?
Sn1 Pt3 Sn2 Cl3 156.28(8) 3_566 . . . ?
Sn3 Pt3 Sn2 Cl3 -33.75(8) . . . . ?
Pt1 Pt3 Sn2 Cl3 -89.72(8) . . . . ?
Pt2 Pt3 Sn2 Cl3 -136.71(8) 3_566 . . . ?
Pt2 Pt3 Sn2 Cl3 -167.49(8) . . . . ?
C3 Pt3 Sn2 Pt2 -131.4(3) . . . . ?
Sn1 Pt3 Sn2 Pt2 -36.23(2) 3_566 . . . ?
Sn3 Pt3 Sn2 Pt2 133.74(2) . . . . ?
Pt1 Pt3 Sn2 Pt2 77.767(16) . . . . ?
Pt2 Pt3 Sn2 Pt2 30.776(18) 3_566 . . . ?
C3 Pt3 Sn2 Pt1 150.9(3) . . . . ?
Sn1 Pt3 Sn2 Pt1 -114.00(2) 3_566 . . . ?
Sn3 Pt3 Sn2 Pt1 55.969(19) . . . . ?
Pt2 Pt3 Sn2 Pt1 -46.990(15) 3_566 . . . ?
Pt2 Pt3 Sn2 Pt1 -77.767(16) . . . . ?
C3 Pt3 Sn3 Cl8 85.2(4) . . . . ?
Sn1 Pt3 Sn3 Cl8 -15.35(15) 3_566 . . . ?
Pt1 Pt3 Sn3 Cl8 -112.52(12) . . . . ?
Sn2 Pt3 Sn3 Cl8 -166.58(12) . . . . ?
Pt2 Pt3 Sn3 Cl8 -66.75(12) 3_566 . . . ?
Pt2 Pt3 Sn3 Cl8 -120.28(12) . . . . ?
C3 Pt3 Sn3 Cl6 -131.6(4) . . . . ?
Sn1 Pt3 Sn3 Cl6 127.9(2) 3_566 . . . ?
Pt1 Pt3 Sn3 Cl6 30.7(2) . . . . ?
Sn2 Pt3 Sn3 Cl6 -23.4(2) . . . . ?
Pt2 Pt3 Sn3 Cl6 76.5(2) 3_566 . . . ?
Pt2 Pt3 Sn3 Cl6 22.9(2) . . . . ?
C3 Pt3 Sn3 Cl7 -14.4(4) . . . . ?
Sn1 Pt3 Sn3 Cl7 -115.01(11) 3_566 . . . ?
Pt1 Pt3 Sn3 Cl7 147.82(10) . . . . ?
Sn2 Pt3 Sn3 Cl7 93.76(10) . . . . ?
Pt2 Pt3 Sn3 Cl7 -166.41(10) 3_566 . . . ?
Pt2 Pt3 Sn3 Cl7 140.06(10) . . . . ?
C3 Pt3 Sn3 Pt1 -162.3(4) . . . . ?
Sn1 Pt3 Sn3 Pt1 97.17(7) 3_566 . . . ?
Sn2 Pt3 Sn3 Pt1 -54.059(18) . . . . ?
Pt2 Pt3 Sn3 Pt1 45.773(16) 3_566 . . . ?
Pt2 Pt3 Sn3 Pt1 -7.76(2) . . . . ?
C1 Pt1 Sn3 Cl8 -103.1(4) . . . . ?
Sn1 Pt1 Sn3 Cl8 -1.35(15) . . . . ?
Pt3 Pt1 Sn3 Cl8 93.89(13) . . . . ?
Sn2 Pt1 Sn3 Cl8 151.87(13) . . . . ?
Pt2 Pt1 Sn3 Cl8 45.65(13) 3_566 . . . ?
Pt2 Pt1 Sn3 Cl8 101.26(13) . . . . ?
C1 Pt1 Sn3 Cl6 -3.6(4) . . . . ?
Sn1 Pt1 Sn3 Cl6 98.20(12) . . . . ?
Pt3 Pt1 Sn3 Cl6 -166.57(10) . . . . ?
Sn2 Pt1 Sn3 Cl6 -108.58(10) . . . . ?
Pt2 Pt1 Sn3 Cl6 145.20(10) 3_566 . . . ?
Pt2 Pt1 Sn3 Cl6 -159.19(10) . . . . ?
C1 Pt1 Sn3 Cl7 98.7(4) . . . . ?
Sn1 Pt1 Sn3 Cl7 -159.51(16) . . . . ?
Pt3 Pt1 Sn3 Cl7 -64.28(16) . . . . ?
Sn2 Pt1 Sn3 Cl7 -6.29(16) . . . . ?
Pt2 Pt1 Sn3 Cl7 -112.51(16) 3_566 . . . ?
Pt2 Pt1 Sn3 Cl7 -56.90(16) . . . . ?
C1 Pt1 Sn3 Pt3 163.0(4) . . . . ?
Sn1 Pt1 Sn3 Pt3 -95.24(7) . . . . ?
Sn2 Pt1 Sn3 Pt3 57.983(19) . . . . ?
Pt2 Pt1 Sn3 Pt3 -48.233(17) 3_566 . . . ?
Pt2 Pt1 Sn3 Pt3 7.37(2) . . . . ?
Sn1 Pt1 C1 O1 52(27) . . . . ?
Pt3 Pt1 C1 O1 -118(27) . . . . ?
Sn3 Pt1 C1 O1 -146(27) . . . . ?
Sn2 Pt1 C1 O1 -52(27) . . . . ?
Pt2 Pt1 C1 O1 95(27) 3_566 . . . ?
Pt2 Pt1 C1 O1 2(28) . . . . ?
Pt2 Pt2 C2 O2 94(20) 3_566 . . . ?
Sn2 Pt2 C2 O2 -71(20) . . . . ?
Pt1 Pt2 C2 O2 86(20) 3_566 . . . ?
Sn1 Pt2 C2 O2 33(21) 3_566 . . . ?
Pt3 Pt2 C2 O2 142(20) 3_566 . . . ?
Pt3 Pt2 C2 O2 -20(21) . . . . ?
Sn1 Pt2 C2 O2 -167(20) . . . . ?
Pt1 Pt2 C2 O2 -98(20) . . . . ?
Sn1 Pt3 C3 O3 -101(24) 3_566 . . . ?
Sn3 Pt3 C3 O3 99(24) . . . . ?
Pt1 Pt3 C3 O3 65(24) . . . . ?
Sn2 Pt3 C3 O3 6(24) . . . . ?
Pt2 Pt3 C3 O3 -140(24) 3_566 . . . ?
Pt2 Pt3 C3 O3 -52(24) . . . . ?
C119 P1 C101 C102 90.0(10) . . . . ?
C113 P1 C101 C102 -148.7(9) . . . . ?
C107 P1 C101 C102 -28.8(11) . . . . ?
C119 P1 C101 C106 -82.1(10) . . . . ?
C113 P1 C101 C106 39.2(11) . . . . ?
C107 P1 C101 C106 159.1(9) . . . . ?
C106 C101 C102 C103 -0.2(17) . . . . ?
P1 C101 C102 C103 -172.3(9) . . . . ?
C101 C102 C103 C104 2.3(18) . . . . ?
C102 C103 C104 C105 -2(2) . . . . ?
C103 C104 C105 C106 0(2) . . . . ?
C104 C105 C106 C101 2.4(19) . . . . ?
C102 C101 C106 C105 -2.3(18) . . . . ?
P1 C101 C106 C105 169.9(10) . . . . ?
C119 P1 C107 C112 -43.9(10) . . . . ?
C101 P1 C107 C112 74.4(9) . . . . ?
C113 P1 C107 C112 -165.6(8) . . . . ?
C119 P1 C107 C108 137.5(9) . . . . ?
C101 P1 C107 C108 -104.2(9) . . . . ?
C113 P1 C107 C108 15.8(10) . . . . ?
C112 C107 C108 C109 -0.1(16) . . . . ?
P1 C107 C108 C109 178.5(8) . . . . ?
C107 C108 C109 C110 -0.2(17) . . . . ?
C108 C109 C110 C111 0.3(19) . . . . ?
C109 C110 C111 C112 0.0(18) . . . . ?
C108 C107 C112 C111 0.4(16) . . . . ?
P1 C107 C112 C111 -178.3(9) . . . . ?
C110 C111 C112 C107 -0.3(18) . . . . ?
C119 P1 C113 C118 166.7(9) . . . . ?
C101 P1 C113 C118 47.7(10) . . . . ?
C107 P1 C113 C118 -73.5(10) . . . . ?
C119 P1 C113 C114 -19.4(10) . . . . ?
C101 P1 C113 C114 -138.3(9) . . . . ?
C107 P1 C113 C114 100.4(9) . . . . ?
C118 C113 C114 C115 0.5(17) . . . . ?
P1 C113 C114 C115 -173.4(9) . . . . ?
C113 C114 C115 C116 1.5(18) . . . . ?
C114 C115 C116 C117 -2.1(19) . . . . ?
C115 C116 C117 C118 0.8(19) . . . . ?
C114 C113 C118 C117 -1.8(17) . . . . ?
P1 C113 C118 C117 172.2(9) . . . . ?
C116 C117 C118 C113 1.2(18) . . . . ?
C101 P1 C119 C120 -149.4(9) . . . . ?
C113 P1 C119 C120 90.9(10) . . . . ?
C107 P1 C119 C120 -29.1(11) . . . . ?
C101 P1 C119 C124 29.8(11) . . . . ?
C113 P1 C119 C124 -90.0(10) . . . . ?
C107 P1 C119 C124 150.1(9) . . . . ?
C124 C119 C120 C121 -1.4(18) . . . . ?
P1 C119 C120 C121 177.8(9) . . . . ?
C119 C120 C121 C122 2(2) . . . . ?
C120 C121 C122 C123 0(2) . . . . ?
C121 C122 C123 C124 -3(2) . . . . ?
C122 C123 C124 C119 3(2) . . . . ?
C120 C119 C124 C123 -0.8(19) . . . . ?
P1 C119 C124 C123 -180.0(10) . . . . ?
C213 P2 C201 C206 81.4(10) . . . . ?
C219 P2 C201 C206 -37.4(11) . . . . ?
C207 P2 C201 C206 -159.5(9) . . . . ?
C213 P2 C201 C202 -95.8(10) . . . . ?
C219 P2 C201 C202 145.4(9) . . . . ?
C207 P2 C201 C202 23.3(11) . . . . ?
C206 C201 C202 C203 1.1(17) . . . . ?
P2 C201 C202 C203 178.3(9) . . . . ?
C201 C202 C203 C204 -0.5(19) . . . . ?
C202 C203 C204 C205 -1(2) . . . . ?
C203 C204 C205 C206 2(2) . . . . ?
C204 C205 C206 C201 -1(2) . . . . ?
C202 C201 C206 C205 -0.3(18) . . . . ?
P2 C201 C206 C205 -177.6(10) . . . . ?
C213 P2 C207 C212 171.2(9) . . . . ?
C219 P2 C207 C212 -69.8(11) . . . . ?
C201 P2 C207 C212 51.9(11) . . . . ?
C213 P2 C207 C208 -7.8(11) . . . . ?
C219 P2 C207 C208 111.1(10) . . . . ?
C201 P2 C207 C208 -127.2(9) . . . . ?
C212 C207 C208 C209 -1.1(17) . . . . ?
P2 C207 C208 C209 177.9(9) . . . . ?
C207 C208 C209 C210 0.5(18) . . . . ?
C208 C209 C210 C211 -0.3(19) . . . . ?
C209 C210 C211 C212 0.7(19) . . . . ?
C210 C211 C212 C207 -1.4(19) . . . . ?
C208 C207 C212 C211 1.6(18) . . . . ?
P2 C207 C212 C211 -177.4(9) . . . . ?
C219 P2 C213 C214 135.5(9) . . . . ?
C201 P2 C213 C214 15.1(11) . . . . ?
C207 P2 C213 C214 -103.4(9) . . . . ?
C219 P2 C213 C218 -48.5(10) . . . . ?
C201 P2 C213 C218 -169.0(9) . . . . ?
C207 P2 C213 C218 72.5(10) . . . . ?
C218 C213 C214 C215 2.6(16) . . . . ?
P2 C213 C214 C215 178.5(8) . . . . ?
C213 C214 C215 C216 -3.7(17) . . . . ?
C214 C215 C216 C217 3.6(18) . . . . ?
C215 C216 C217 C218 -2.3(19) . . . . ?
C216 C217 C218 C213 1.2(18) . . . . ?
C214 C213 C218 C217 -1.3(17) . . . . ?
P2 C213 C218 C217 -177.3(9) . . . . ?
C213 P2 C219 C220 -35.0(11) . . . . ?
C201 P2 C219 C220 84.8(11) . . . . ?
C207 P2 C219 C220 -154.8(10) . . . . ?
C213 P2 C219 C224 147.6(9) . . . . ?
C201 P2 C219 C224 -92.5(10) . . . . ?
C207 P2 C219 C224 27.9(11) . . . . ?
C224 C219 C220 C221 0.4(19) . . . . ?
P2 C219 C220 C221 -177.0(10) . . . . ?
C219 C220 C221 C222 -2(2) . . . . ?
C220 C221 C222 C223 2(2) . . . . ?
C221 C222 C223 C224 -1(2) . . . . ?
C222 C223 C224 C219 -0.2(19) . . . . ?
C220 C219 C224 C223 0.7(17) . . . . ?
P2 C219 C224 C223 178.0(9) . . . . ?

_diffrn_measured_fraction_theta_max 1.000
_diffrn_reflns_theta_full        26.00
_diffrn_measured_fraction_theta_full 1.000
_refine_diff_density_max         2.632
_refine_diff_density_min         -1.590
_refine_diff_density_rms         0.177
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_3_4MeCN_2
_database_code_depnum_ccdc_archive 'CCDC 1439440'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C110 H92 Cl16 N4 O6 P4 Pt6 Sn6'
_chemical_formula_weight         4139.64

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   P2(1)/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   13.707(7)
_cell_length_b                   28.016(14)
_cell_length_c                   17.266(9)
_cell_angle_alpha                90.00
_cell_angle_beta                 92.377(6)
_cell_angle_gamma                90.00
_cell_volume                     6624(6)
_cell_formula_units_Z            2
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    9828
_cell_measurement_theta_min      2.361
_cell_measurement_theta_max      27.108

_exptl_crystal_description       prism
_exptl_crystal_colour            black
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.16
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.075
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3856
_exptl_absorpt_coefficient_mu    7.836
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.2659
_exptl_absorpt_correction_T_max  0.3670
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1739 (selected reflections only, before parameter refinement)
 R(int) = 0.0725 (selected reflections only, after parameter refinement)
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            67162
_diffrn_reflns_av_R_equivalents  0.0589
_diffrn_reflns_av_unetI/netI     0.0438
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -34
_diffrn_reflns_limit_k_max       34
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_theta_min         1.45
_diffrn_reflns_theta_max         26.00
_reflns_number_total             13012
_reflns_number_gt                10822
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. The following restraints
 were applied (given as SHELXL lines): 
 delu .005 p2 c59 c41
 simu .01 c1 > o3
 simu .01 c11 > c34
 isor .005 c41 > c64
 simu .01 p2 > c64
 AFIX 66 on Ph rings
 same n2 > c202
 simu .01 n1 > c202
 dfix 1.14 .01 n1 c101 n2 c201
 dfix 1.47 .01 c101 c102 c201 c202
 The asymmetric unit of the unit cell contains one half of a cluster anion 
 (located on an inversion centre), two [PPh4]+ cations and two CH3CN 
 molecules (all located on general positions). Similar U restraints have 
 been applied to the C and O atoms of the CO ligands and to the C atoms of 
 the Ph-rings (SIMU command in SHELXL, s.u. 0.01). The C-atoms of the Ph 
 rings bonded to P(2) have been restrained to isotropic behaviour (ISOR 
 command in SHELXL, s.u. 0.005) as well as constrained to fit regular 
 hexagons (AFIX 66 command in SHELXL). The CH3CN molecules have been 
 restrained to have similar geometries (SAME command in SHELXL, s.u. 
 0.02) and similar U parameters (SIMU command in SHELXL, s.u. 0.01). 
 Restraints to bond distances were applied as follow (s.u. 0.02): 1.14
  Å for C N and 1.47 Å for C C in CH3CN.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0434P)²+18.3437P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         13012
_refine_ls_number_parameters     607
_refine_ls_number_restraints     464
_refine_ls_R_factor_all          0.0493
_refine_ls_R_factor_gt           0.0383
_refine_ls_wR_factor_ref         0.1019
_refine_ls_wR_factor_gt          0.0959
_refine_ls_goodness_of_fit_ref   1.053
_refine_ls_restrained_S_all      1.066
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.45721(2) 0.029826(10) 0.547784(14) 0.04226(8) Uani 1 1 d . . .
Pt2 Pt 0.34487(2) 0.009601(10) 0.412158(15) 0.04510(8) Uani 1 1 d . . .
Pt3 Pt 0.49896(2) 0.068297(11) 0.396343(16) 0.04854(8) Uani 1 1 d . . .
Sn1 Sn 0.52039(4) 0.020080(18) 0.69591(3) 0.04759(12) Uani 1 1 d . . .
Sn2 Sn 0.32112(4) 0.09771(2) 0.34404(3) 0.05515(14) Uani 1 1 d . . .
Sn3 Sn 0.65318(4) 0.05850(2) 0.48644(3) 0.05831(15) Uani 1 1 d . . .
Cl1 Cl 0.61424(18) -0.01513(8) 0.80207(11) 0.0685(6) Uani 1 1 d . . .
Cl2 Cl 0.37450(17) 0.01654(9) 0.76746(13) 0.0746(6) Uani 1 1 d . . .
Cl3 Cl 0.56238(18) 0.10061(7) 0.72973(11) 0.0677(6) Uani 1 1 d . . .
Cl4 Cl 0.3661(2) 0.15617(10) 0.24969(15) 0.0881(7) Uani 1 1 d . . .
Cl5 Cl 0.2588(2) 0.15245(9) 0.43519(15) 0.0868(7) Uani 1 1 d . . .
Cl6 Cl 0.1689(2) 0.08591(12) 0.27531(18) 0.1011(9) Uani 1 1 d . . .
Cl7 Cl 0.7094(2) 0.13262(10) 0.5401(2) 0.1041(9) Uani 1 1 d . . .
Cl8 Cl 0.7947(2) 0.04656(12) 0.41260(16) 0.0954(8) Uani 1 1 d . . .
C1 C 0.3617(7) 0.0731(3) 0.5806(4) 0.0564(19) Uani 1 1 d U . .
C2 C 0.2211(7) -0.0106(3) 0.3767(6) 0.073(2) Uani 1 1 d U . .
C3 C 0.5679(7) 0.1107(4) 0.3357(6) 0.076(3) Uani 1 1 d U . .
O1 O 0.3016(5) 0.0956(2) 0.6024(4) 0.0814(18) Uani 1 1 d U . .
O2 O 0.1476(6) -0.0239(3) 0.3563(5) 0.116(3) Uani 1 1 d U . .
O3 O 0.6149(6) 0.1331(3) 0.2974(5) 0.113(3) Uani 1 1 d U . .
P1 P 0.47062(17) 0.30124(8) 0.43691(12) 0.0580(5) Uani 1 1 d . . .
C11 C 0.5154(6) 0.3545(3) 0.4842(5) 0.0607(18) Uani 1 1 d U . .
C12 C 0.5130(6) 0.3608(3) 0.5636(5) 0.0641(19) Uani 1 1 d U . .
H12 H 0.4894 0.3366 0.5945 0.077 Uiso 1 1 calc R . .
C13 C 0.5454(7) 0.4027(4) 0.5969(5) 0.073(2) Uani 1 1 d U . .
H13 H 0.5440 0.4068 0.6503 0.088 Uiso 1 1 calc R . .
C14 C 0.5794(8) 0.4381(4) 0.5519(6) 0.081(2) Uani 1 1 d U . .
H14 H 0.5987 0.4669 0.5747 0.097 Uiso 1 1 calc R . .
C15 C 0.5857(8) 0.4323(4) 0.4735(6) 0.080(2) Uani 1 1 d U . .
H15 H 0.6115 0.4565 0.4437 0.096 Uiso 1 1 calc R . .
C16 C 0.5546(7) 0.3913(3) 0.4396(5) 0.072(2) Uani 1 1 d U . .
H16 H 0.5591 0.3873 0.3864 0.086 Uiso 1 1 calc R . .
C17 C 0.3607(6) 0.3117(3) 0.3777(5) 0.0596(18) Uani 1 1 d U . .
C18 C 0.3019(7) 0.2733(4) 0.3612(6) 0.077(2) Uani 1 1 d U . .
H18 H 0.3174 0.2435 0.3817 0.092 Uiso 1 1 calc R . .
C19 C 0.2192(8) 0.2795(4) 0.3139(6) 0.088(3) Uani 1 1 d U . .
H19 H 0.1786 0.2536 0.3026 0.106 Uiso 1 1 calc R . .
C20 C 0.1967(8) 0.3234(4) 0.2836(6) 0.082(2) Uani 1 1 d U . .
H20 H 0.1408 0.3274 0.2519 0.099 Uiso 1 1 calc R . .
C21 C 0.2570(8) 0.3614(4) 0.3002(6) 0.078(2) Uani 1 1 d U . .
H21 H 0.2414 0.3913 0.2798 0.094 Uiso 1 1 calc R . .
C22 C 0.3396(7) 0.3559(3) 0.3462(5) 0.069(2) Uani 1 1 d U . .
H22 H 0.3811 0.3816 0.3562 0.083 Uiso 1 1 calc R . .
C23 C 0.5646(8) 0.2796(4) 0.3769(6) 0.077(2) Uani 1 1 d U . .
C24 C 0.5446(9) 0.2644(4) 0.3016(6) 0.093(3) Uani 1 1 d U . .
H24 H 0.4807 0.2657 0.2815 0.111 Uiso 1 1 calc R . .
C25 C 0.6145(10) 0.2476(5) 0.2565(8) 0.114(3) Uani 1 1 d U . .
H25 H 0.5995 0.2371 0.2063 0.136 Uiso 1 1 calc R . .
C26 C 0.7083(11) 0.2465(5) 0.2866(8) 0.122(3) Uani 1 1 d U . .
H26 H 0.7576 0.2369 0.2548 0.146 Uiso 1 1 calc R . .
C27 C 0.7326(10) 0.2589(5) 0.3610(9) 0.121(3) Uani 1 1 d U . .
H27 H 0.7961 0.2553 0.3813 0.145 Uiso 1 1 calc R . .
C28 C 0.6591(9) 0.2771(5) 0.4057(7) 0.102(3) Uani 1 1 d U . .
H28 H 0.6743 0.2877 0.4558 0.123 Uiso 1 1 calc R . .
C29 C 0.4417(7) 0.2587(3) 0.5100(5) 0.0639(19) Uani 1 1 d U . .
C30 C 0.3614(8) 0.2675(4) 0.5530(5) 0.076(2) Uani 1 1 d U . .
H30 H 0.3207 0.2932 0.5407 0.091 Uiso 1 1 calc R . .
C31 C 0.3415(8) 0.2381(4) 0.6146(6) 0.084(2) Uani 1 1 d U . .
H31 H 0.2899 0.2450 0.6460 0.101 Uiso 1 1 calc R . .
C32 C 0.3979(9) 0.1988(4) 0.6289(6) 0.087(3) Uani 1 1 d U . .
H32 H 0.3828 0.1783 0.6690 0.105 Uiso 1 1 calc R . .
C33 C 0.4757(9) 0.1892(4) 0.5856(6) 0.086(2) Uani 1 1 d U . .
H33 H 0.5142 0.1625 0.5960 0.103 Uiso 1 1 calc R . .
C34 C 0.4968(8) 0.2197(3) 0.5259(5) 0.074(2) Uani 1 1 d U . .
H34 H 0.5502 0.2133 0.4960 0.089 Uiso 1 1 calc R . .
P2 P -0.00427(19) 0.12101(12) 0.02144(16) 0.0832(8) Uani 1 1 d U . .
C41 C 0.0104(10) 0.1823(3) 0.0401(7) 0.136(3) Uani 1 1 d GU . .
C42 C -0.0388(9) 0.2046(5) 0.0989(7) 0.186(5) Uani 1 1 d GU . .
H42 H -0.0824 0.1873 0.1278 0.224 Uiso 1 1 calc R . .
C43 C -0.0227(10) 0.2527(5) 0.1145(7) 0.208(5) Uani 1 1 d GU . .
H43 H -0.0557 0.2676 0.1539 0.249 Uiso 1 1 calc R . .
C44 C 0.0424(11) 0.2785(4) 0.0713(9) 0.200(5) Uani 1 1 d GU . .
H44 H 0.0532 0.3107 0.0818 0.240 Uiso 1 1 calc R . .
C45 C 0.0916(9) 0.2562(5) 0.0125(8) 0.182(5) Uani 1 1 d GU . .
H45 H 0.1352 0.2734 -0.0164 0.219 Uiso 1 1 calc R . .
C46 C 0.0756(9) 0.2081(5) -0.0030(6) 0.155(4) Uani 1 1 d GU . .
H46 H 0.1085 0.1931 -0.0424 0.187 Uiso 1 1 calc R . .
C47 C -0.0572(7) 0.0886(3) 0.1001(4) 0.101(3) Uani 1 1 d GU . .
C48 C -0.1518(6) 0.0986(3) 0.1212(5) 0.125(3) Uani 1 1 d GU . .
H48 H -0.1876 0.1225 0.0956 0.150 Uiso 1 1 calc R . .
C49 C -0.1929(5) 0.0729(4) 0.1805(6) 0.127(3) Uani 1 1 d GU . .
H49 H -0.2562 0.0796 0.1946 0.153 Uiso 1 1 calc R . .
C50 C -0.1395(7) 0.0372(3) 0.2187(5) 0.128(4) Uani 1 1 d GU . .
H50 H -0.1670 0.0200 0.2584 0.154 Uiso 1 1 calc R . .
C51 C -0.0449(7) 0.0272(3) 0.1976(5) 0.122(3) Uani 1 1 d GU . .
H51 H -0.0091 0.0033 0.2231 0.146 Uiso 1 1 calc R . .
C52 C -0.0037(5) 0.0529(3) 0.1382(5) 0.108(3) Uani 1 1 d GU . .
H52 H 0.0596 0.0462 0.1241 0.130 Uiso 1 1 calc R . .
C53 C 0.1135(4) 0.0976(2) 0.0099(4) 0.075(2) Uani 1 1 d GU . .
C54 C 0.1852(5) 0.1087(2) 0.0664(3) 0.080(2) Uani 1 1 d GU . .
H54 H 0.1708 0.1290 0.1069 0.095 Uiso 1 1 calc R . .
C55 C 0.2783(4) 0.0895(3) 0.0622(4) 0.087(2) Uani 1 1 d GU . .
H55 H 0.3262 0.0969 0.0999 0.105 Uiso 1 1 calc R . .
C56 C 0.2997(4) 0.0591(3) 0.0015(4) 0.092(3) Uani 1 1 d GU . .
H56 H 0.3620 0.0462 -0.0013 0.110 Uiso 1 1 calc R . .
C57 C 0.2281(5) 0.0480(2) -0.0549(4) 0.095(3) Uani 1 1 d GU . .
H57 H 0.2424 0.0277 -0.0955 0.114 Uiso 1 1 calc R . .
C58 C 0.1350(5) 0.0672(2) -0.0507(3) 0.086(2) Uani 1 1 d GU . .
H58 H 0.0870 0.0598 -0.0885 0.103 Uiso 1 1 calc R . .
C59 C -0.0756(7) 0.1126(4) -0.0654(5) 0.106(3) Uani 1 1 d GU . .
C60 C -0.1309(8) 0.0714(3) -0.0762(6) 0.135(4) Uani 1 1 d GU . .
H60 H -0.1323 0.0486 -0.0371 0.162 Uiso 1 1 calc R . .
C61 C -0.1842(7) 0.0642(3) -0.1455(7) 0.150(4) Uani 1 1 d GU . .
H61 H -0.2212 0.0366 -0.1527 0.180 Uiso 1 1 calc R . .
C62 C -0.1821(7) 0.0982(4) -0.2039(5) 0.150(4) Uani 1 1 d GU . .
H62 H -0.2178 0.0934 -0.2503 0.180 Uiso 1 1 calc R . .
C63 C -0.1268(8) 0.1395(4) -0.1931(5) 0.151(4) Uani 1 1 d GU . .
H63 H -0.1255 0.1622 -0.2322 0.182 Uiso 1 1 calc R . .
C64 C -0.0736(7) 0.1466(3) -0.1238(6) 0.131(4) Uani 1 1 d GU . .
H64 H -0.0366 0.1742 -0.1166 0.158 Uiso 1 1 calc R . .
N1 N 0.9668(14) 0.2312(6) 0.3059(11) 0.201(7) Uiso 1 1 d DU . .
C101 C 0.9658(15) 0.1943(7) 0.3323(11) 0.164(6) Uiso 1 1 d DU . .
C102 C 0.9585(15) 0.1472(7) 0.3679(12) 0.193(8) Uiso 1 1 d DU . .
H10A H 0.9925 0.1474 0.4176 0.290 Uiso 1 1 calc R . .
H10B H 0.9871 0.1238 0.3352 0.290 Uiso 1 1 calc R . .
H10C H 0.8910 0.1396 0.3742 0.290 Uiso 1 1 calc R . .
N2 N 0.940(2) 0.9099(10) 0.3259(14) 0.279(10) Uiso 1 1 d DU . .
C201 C 0.947(2) 0.9122(9) 0.3917(13) 0.226(9) Uiso 1 1 d DU . .
C202 C 0.9442(18) 0.9394(9) 0.4641(13) 0.226(10) Uiso 1 1 d DU . .
H20A H 1.0086 0.9409 0.4881 0.339 Uiso 1 1 calc R . .
H20B H 0.9009 0.9240 0.4985 0.339 Uiso 1 1 calc R . .
H20C H 0.9212 0.9712 0.4531 0.339 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.888(8) . ?
Pt1 Pt1 2.6556(9) 3_656 ?
Pt1 Sn1 2.6798(13) . ?
Pt1 Pt2 2.8064(11) . ?
Pt1 Pt3 2.9069(13) . ?
Pt1 Sn3 2.9475(13) 3_656 ?
Pt1 Pt3 2.9666(13) 3_656 ?
Pt1 Pt2 2.9837(13) 3_656 ?
Pt1 Sn3 3.0362(14) . ?
Pt2 C2 1.867(9) . ?
Pt2 Sn3 2.5889(11) 3_656 ?
Pt2 Pt3 2.6995(10) . ?
Pt2 Sn2 2.7477(13) . ?
Pt2 Sn1 2.8052(11) 3_656 ?
Pt2 Pt1 2.9837(13) 3_656 ?
Pt3 C3 1.866(9) . ?
Pt3 Sn3 2.5866(11) . ?
Pt3 Sn2 2.6932(12) . ?
Pt3 Sn1 2.9500(12) 3_656 ?
Pt3 Pt1 2.9666(13) 3_656 ?
Sn1 Cl3 2.395(2) . ?
Sn1 Cl2 2.396(2) . ?
Sn1 Cl1 2.407(2) . ?
Sn1 Pt2 2.8052(11) 3_656 ?
Sn1 Pt3 2.9500(12) 3_656 ?
Sn2 Cl6 2.380(3) . ?
Sn2 Cl5 2.381(3) . ?
Sn2 Cl4 2.408(3) . ?
Sn3 Cl7 2.388(3) . ?
Sn3 Cl8 2.389(3) . ?
Sn3 Pt2 2.5889(11) 3_656 ?
Sn3 Pt1 2.9475(13) 3_656 ?
C1 O1 1.115(9) . ?
C2 O2 1.117(10) . ?
C3 O3 1.132(10) . ?
P1 C23 1.791(10) . ?
P1 C29 1.793(8) . ?
P1 C11 1.797(9) . ?
P1 C17 1.810(9) . ?
C11 C12 1.383(11) . ?
C11 C16 1.406(12) . ?
C12 C13 1.372(12) . ?
C12 H12 0.9300 . ?
C13 C14 1.354(13) . ?
C13 H13 0.9300 . ?
C14 C15 1.371(14) . ?
C14 H14 0.9300 . ?
C15 C16 1.349(13) . ?
C15 H15 0.9300 . ?
C16 H16 0.9300 . ?
C17 C18 1.367(12) . ?
C17 C22 1.376(12) . ?
C18 C19 1.380(14) . ?
C18 H18 0.9300 . ?
C19 C20 1.367(15) . ?
C19 H19 0.9300 . ?
C20 C21 1.371(14) . ?
C20 H20 0.9300 . ?
C21 C22 1.366(13) . ?
C21 H21 0.9300 . ?
C22 H22 0.9300 . ?
C23 C28 1.369(15) . ?
C23 C24 1.386(14) . ?
C24 C25 1.344(15) . ?
C24 H24 0.9300 . ?
C25 C26 1.367(19) . ?
C25 H25 0.9300 . ?
C26 C27 1.357(19) . ?
C26 H26 0.9300 . ?
C27 C28 1.392(16) . ?
C27 H27 0.9300 . ?
C28 H28 0.9300 . ?
C29 C34 1.350(12) . ?
C29 C30 1.376(13) . ?
C30 C31 1.382(13) . ?
C30 H30 0.9300 . ?
C31 C32 1.361(15) . ?
C31 H31 0.9300 . ?
C32 C33 1.354(15) . ?
C32 H32 0.9300 . ?
C33 C34 1.379(13) . ?
C33 H33 0.9300 . ?
C34 H34 0.9300 . ?
P2 C41 1.756(10) . ?
P2 C53 1.762(6) . ?
P2 C59 1.771(8) . ?
P2 C47 1.810(7) . ?
C41 C42 1.3900 . ?
C41 C46 1.3900 . ?
C42 C43 1.3900 . ?
C42 H42 0.9300 . ?
C43 C44 1.3900 . ?
C43 H43 0.9300 . ?
C44 C45 1.3900 . ?
C44 H44 0.9300 . ?
C45 C46 1.3900 . ?
C45 H45 0.9300 . ?
C46 H46 0.9300 . ?
C47 C48 1.3900 . ?
C47 C52 1.3900 . ?
C48 C49 1.3900 . ?
C48 H48 0.9300 . ?
C49 C50 1.3900 . ?
C49 H49 0.9300 . ?
C50 C51 1.3900 . ?
C50 H50 0.9300 . ?
C51 C52 1.3900 . ?
C51 H51 0.9300 . ?
C52 H52 0.9300 . ?
C53 C54 1.3900 . ?
C53 C58 1.3900 . ?
C54 C55 1.3900 . ?
C54 H54 0.9300 . ?
C55 C56 1.3900 . ?
C55 H55 0.9300 . ?
C56 C57 1.3900 . ?
C56 H56 0.9300 . ?
C57 C58 1.3900 . ?
C57 H57 0.9300 . ?
C58 H58 0.9300 . ?
C59 C60 1.3900 . ?
C59 C64 1.3900 . ?
C60 C61 1.3900 . ?
C60 H60 0.9300 . ?
C61 C62 1.3900 . ?
C61 H61 0.9300 . ?
C62 C63 1.3900 . ?
C62 H62 0.9300 . ?
C63 C64 1.3900 . ?
C63 H63 0.9300 . ?
C64 H64 0.9300 . ?
N1 C101 1.132(9) . ?
C101 C102 1.459(9) . ?
C102 H10A 0.9600 . ?
C102 H10B 0.9600 . ?
C102 H10C 0.9600 . ?
N2 C201 1.138(9) . ?
C201 C202 1.465(9) . ?
C202 H20A 0.9600 . ?
C202 H20B 0.9600 . ?
C202 H20C 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 Pt1 157.0(2) . 3_656 ?
C1 Pt1 Sn1 88.8(2) . . ?
Pt1 Pt1 Sn1 113.28(3) 3_656 . ?
C1 Pt1 Pt2 91.0(2) . . ?
Pt1 Pt1 Pt2 66.15(3) 3_656 . ?
Sn1 Pt1 Pt2 156.95(2) . . ?
C1 Pt1 Pt3 101.4(2) . . ?
Pt1 Pt1 Pt3 64.27(3) 3_656 . ?
Sn1 Pt1 Pt3 145.92(3) . . ?
Pt2 Pt1 Pt3 56.36(3) . . ?
C1 Pt1 Sn3 104.0(3) . 3_656 ?
Pt1 Pt1 Sn3 65.38(3) 3_656 3_656 ?
Sn1 Pt1 Sn3 104.40(2) . 3_656 ?
Pt2 Pt1 Sn3 53.410(16) . 3_656 ?
Pt3 Pt1 Sn3 104.45(3) . 3_656 ?
C1 Pt1 Pt3 129.1(2) . 3_656 ?
Pt1 Pt1 Pt3 61.98(3) 3_656 3_656 ?
Sn1 Pt1 Pt3 62.753(16) . 3_656 ?
Pt2 Pt1 Pt3 100.42(2) . 3_656 ?
Pt3 Pt1 Pt3 126.250(12) . 3_656 ?
Sn3 Pt1 Pt3 51.87(3) 3_656 3_656 ?
C1 Pt1 Pt2 143.4(2) . 3_656 ?
Pt1 Pt1 Pt2 59.35(2) 3_656 3_656 ?
Sn1 Pt1 Pt2 59.089(15) . 3_656 ?
Pt2 Pt1 Pt2 125.505(18) . 3_656 ?
Pt3 Pt1 Pt2 97.74(2) . 3_656 ?
Sn3 Pt1 Pt2 100.95(3) 3_656 3_656 ?
Pt3 Pt1 Pt2 53.958(11) 3_656 3_656 ?
C1 Pt1 Sn3 124.7(3) . . ?
Pt1 Pt1 Sn3 61.95(3) 3_656 . ?
Sn1 Pt1 Sn3 95.99(3) . . ?
Pt2 Pt1 Sn3 103.01(3) . . ?
Pt3 Pt1 Sn3 51.544(15) . . ?
Sn3 Pt1 Sn3 127.331(18) 3_656 . ?
Pt3 Pt1 Sn3 100.86(2) 3_656 . ?
Pt2 Pt1 Sn3 50.93(3) 3_656 . ?
C2 Pt2 Sn3 89.0(3) . 3_656 ?
C2 Pt2 Pt3 148.8(3) . . ?
Sn3 Pt2 Pt3 122.08(2) 3_656 . ?
C2 Pt2 Sn2 92.4(3) . . ?
Sn3 Pt2 Sn2 161.66(2) 3_656 . ?
Pt3 Pt2 Sn2 59.25(3) . . ?
C2 Pt2 Sn1 107.8(3) . 3_656 ?
Sn3 Pt2 Sn1 104.05(3) 3_656 3_656 ?
Pt3 Pt2 Sn1 64.78(3) . 3_656 ?
Sn2 Pt2 Sn1 92.93(3) . 3_656 ?
C2 Pt2 Pt1 142.6(3) . . ?
Sn3 Pt2 Pt1 66.08(3) 3_656 . ?
Pt3 Pt2 Pt1 63.70(2) . . ?
Sn2 Pt2 Pt1 103.12(3) . . ?
Sn1 Pt2 Pt1 105.15(4) 3_656 . ?
C2 Pt2 Pt1 140.2(3) . 3_656 ?
Sn3 Pt2 Pt1 65.58(2) 3_656 3_656 ?
Pt3 Pt2 Pt1 62.70(3) . 3_656 ?
Sn2 Pt2 Pt1 121.481(19) . 3_656 ?
Sn1 Pt2 Pt1 55.05(3) 3_656 3_656 ?
Pt1 Pt2 Pt1 54.495(18) . 3_656 ?
C3 Pt3 Sn3 89.1(3) . . ?
C3 Pt3 Sn2 95.2(3) . . ?
Sn3 Pt3 Sn2 160.02(2) . . ?
C3 Pt3 Pt2 149.4(3) . . ?
Sn3 Pt3 Pt2 119.86(3) . . ?
Sn2 Pt3 Pt2 61.27(3) . . ?
C3 Pt3 Pt1 149.8(3) . . ?
Sn3 Pt3 Pt1 66.81(3) . . ?
Sn2 Pt3 Pt1 101.88(3) . . ?
Pt2 Pt3 Pt1 59.941(14) . . ?
C3 Pt3 Sn1 105.5(3) . 3_656 ?
Sn3 Pt3 Sn1 106.77(3) . 3_656 ?
Sn2 Pt3 Sn1 90.91(3) . 3_656 ?
Pt2 Pt3 Sn1 59.34(2) . 3_656 ?
Pt1 Pt3 Sn1 99.08(3) . 3_656 ?
C3 Pt3 Pt1 132.2(3) . 3_656 ?
Sn3 Pt3 Pt1 63.685(17) . 3_656 ?
Sn2 Pt3 Pt1 124.112(17) . 3_656 ?
Pt2 Pt3 Pt1 63.34(3) . 3_656 ?
Pt1 Pt3 Pt1 53.750(12) . 3_656 ?
Sn1 Pt3 Pt1 53.86(3) 3_656 3_656 ?
Cl3 Sn1 Cl2 96.35(9) . . ?
Cl3 Sn1 Cl1 94.88(8) . . ?
Cl2 Sn1 Cl1 91.23(9) . . ?
Cl3 Sn1 Pt1 101.63(5) . . ?
Cl2 Sn1 Pt1 104.64(7) . . ?
Cl1 Sn1 Pt1 155.50(6) . . ?
Cl3 Sn1 Pt2 106.46(6) . 3_656 ?
Cl2 Sn1 Pt2 156.54(7) . 3_656 ?
Cl1 Sn1 Pt2 92.25(7) . 3_656 ?
Pt1 Sn1 Pt2 65.86(3) . 3_656 ?
Cl3 Sn1 Pt3 159.67(6) . 3_656 ?
Cl2 Sn1 Pt3 100.68(7) . 3_656 ?
Cl1 Sn1 Pt3 95.76(6) . 3_656 ?
Pt1 Sn1 Pt3 63.38(3) . 3_656 ?
Pt2 Sn1 Pt3 55.88(2) 3_656 3_656 ?
Cl6 Sn2 Cl5 95.05(12) . . ?
Cl6 Sn2 Cl4 90.03(11) . . ?
Cl5 Sn2 Cl4 96.76(10) . . ?
Cl6 Sn2 Pt3 152.51(9) . . ?
Cl5 Sn2 Pt3 108.66(8) . . ?
Cl4 Sn2 Pt3 100.46(8) . . ?
Cl6 Sn2 Pt2 100.05(8) . . ?
Cl5 Sn2 Pt2 109.58(7) . . ?
Cl4 Sn2 Pt2 150.63(7) . . ?
Pt3 Sn2 Pt2 59.480(16) . . ?
Cl7 Sn3 Cl8 94.17(12) . . ?
Cl7 Sn3 Pt3 112.55(9) . . ?
Cl8 Sn3 Pt3 110.82(8) . . ?
Cl7 Sn3 Pt2 112.60(9) . 3_656 ?
Cl8 Sn3 Pt2 105.77(8) . 3_656 ?
Pt3 Sn3 Pt2 118.04(3) . 3_656 ?
Cl7 Sn3 Pt1 164.22(9) . 3_656 ?
Cl8 Sn3 Pt1 101.36(9) . 3_656 ?
Pt3 Sn3 Pt1 64.44(3) . 3_656 ?
Pt2 Sn3 Pt1 60.51(3) 3_656 3_656 ?
Cl7 Sn3 Pt1 111.75(9) . . ?
Cl8 Sn3 Pt1 154.02(9) . . ?
Pt3 Sn3 Pt1 61.65(4) . . ?
Pt2 Sn3 Pt1 63.48(2) 3_656 . ?
Pt1 Sn3 Pt1 52.669(18) 3_656 . ?
O1 C1 Pt1 174.5(8) . . ?
O2 C2 Pt2 178.1(10) . . ?
O3 C3 Pt3 174.0(10) . . ?
C23 P1 C29 111.6(5) . . ?
C23 P1 C11 107.7(5) . . ?
C29 P1 C11 108.3(4) . . ?
C23 P1 C17 109.3(4) . . ?
C29 P1 C17 107.6(4) . . ?
C11 P1 C17 112.5(4) . . ?
C12 C11 C16 118.3(8) . . ?
C12 C11 P1 122.3(7) . . ?
C16 C11 P1 119.4(6) . . ?
C13 C12 C11 120.2(8) . . ?
C13 C12 H12 119.9 . . ?
C11 C12 H12 119.9 . . ?
C14 C13 C12 120.0(9) . . ?
C14 C13 H13 120.0 . . ?
C12 C13 H13 120.0 . . ?
C13 C14 C15 121.1(9) . . ?
C13 C14 H14 119.5 . . ?
C15 C14 H14 119.5 . . ?
C16 C15 C14 119.8(9) . . ?
C16 C15 H15 120.1 . . ?
C14 C15 H15 120.1 . . ?
C15 C16 C11 120.5(8) . . ?
C15 C16 H16 119.8 . . ?
C11 C16 H16 119.8 . . ?
C18 C17 C22 120.8(9) . . ?
C18 C17 P1 117.3(7) . . ?
C22 C17 P1 121.7(7) . . ?
C17 C18 C19 119.2(10) . . ?
C17 C18 H18 120.4 . . ?
C19 C18 H18 120.4 . . ?
C20 C19 C18 120.3(10) . . ?
C20 C19 H19 119.8 . . ?
C18 C19 H19 119.8 . . ?
C19 C20 C21 119.7(10) . . ?
C19 C20 H20 120.2 . . ?
C21 C20 H20 120.2 . . ?
C22 C21 C20 120.7(10) . . ?
C22 C21 H21 119.6 . . ?
C20 C21 H21 119.6 . . ?
C21 C22 C17 119.2(9) . . ?
C21 C22 H22 120.4 . . ?
C17 C22 H22 120.4 . . ?
C28 C23 C24 118.1(10) . . ?
C28 C23 P1 120.0(8) . . ?
C24 C23 P1 121.9(8) . . ?
C25 C24 C23 122.3(12) . . ?
C25 C24 H24 118.9 . . ?
C23 C24 H24 118.9 . . ?
C24 C25 C26 117.9(13) . . ?
C24 C25 H25 121.0 . . ?
C26 C25 H25 121.0 . . ?
C27 C26 C25 123.0(12) . . ?
C27 C26 H26 118.5 . . ?
C25 C26 H26 118.5 . . ?
C26 C27 C28 117.5(14) . . ?
C26 C27 H27 121.2 . . ?
C28 C27 H27 121.2 . . ?
C23 C28 C27 120.9(12) . . ?
C23 C28 H28 119.5 . . ?
C27 C28 H28 119.5 . . ?
C34 C29 C30 119.3(8) . . ?
C34 C29 P1 122.9(7) . . ?
C30 C29 P1 117.8(7) . . ?
C29 C30 C31 119.7(10) . . ?
C29 C30 H30 120.1 . . ?
C31 C30 H30 120.1 . . ?
C32 C31 C30 119.5(10) . . ?
C32 C31 H31 120.2 . . ?
C30 C31 H31 120.2 . . ?
C33 C32 C31 121.0(10) . . ?
C33 C32 H32 119.5 . . ?
C31 C32 H32 119.5 . . ?
C32 C33 C34 119.0(10) . . ?
C32 C33 H33 120.5 . . ?
C34 C33 H33 120.5 . . ?
C29 C34 C33 121.3(10) . . ?
C29 C34 H34 119.3 . . ?
C33 C34 H34 119.3 . . ?
C41 P2 C53 106.6(5) . . ?
C41 P2 C59 109.9(5) . . ?
C53 P2 C59 109.4(4) . . ?
C41 P2 C47 113.5(6) . . ?
C53 P2 C47 107.2(4) . . ?
C59 P2 C47 110.1(5) . . ?
C42 C41 C46 120.0 . . ?
C42 C41 P2 121.2(9) . . ?
C46 C41 P2 118.7(9) . . ?
C43 C42 C41 120.0 . . ?
C43 C42 H42 120.0 . . ?
C41 C42 H42 120.0 . . ?
C42 C43 C44 120.0 . . ?
C42 C43 H43 120.0 . . ?
C44 C43 H43 120.0 . . ?
C45 C44 C43 120.0 . . ?
C45 C44 H44 120.0 . . ?
C43 C44 H44 120.0 . . ?
C44 C45 C46 120.0 . . ?
C44 C45 H45 120.0 . . ?
C46 C45 H45 120.0 . . ?
C45 C46 C41 120.0 . . ?
C45 C46 H46 120.0 . . ?
C41 C46 H46 120.0 . . ?
C48 C47 C52 120.0 . . ?
C48 C47 P2 120.2(6) . . ?
C52 C47 P2 119.8(6) . . ?
C47 C48 C49 120.0 . . ?
C47 C48 H48 120.0 . . ?
C49 C48 H48 120.0 . . ?
C50 C49 C48 120.0 . . ?
C50 C49 H49 120.0 . . ?
C48 C49 H49 120.0 . . ?
C49 C50 C51 120.0 . . ?
C49 C50 H50 120.0 . . ?
C51 C50 H50 120.0 . . ?
C52 C51 C50 120.0 . . ?
C52 C51 H51 120.0 . . ?
C50 C51 H51 120.0 . . ?
C51 C52 C47 120.0 . . ?
C51 C52 H52 120.0 . . ?
C47 C52 H52 120.0 . . ?
C54 C53 C58 120.0 . . ?
C54 C53 P2 117.5(4) . . ?
C58 C53 P2 122.4(4) . . ?
C53 C54 C55 120.0 . . ?
C53 C54 H54 120.0 . . ?
C55 C54 H54 120.0 . . ?
C56 C55 C54 120.0 . . ?
C56 C55 H55 120.0 . . ?
C54 C55 H55 120.0 . . ?
C55 C56 C57 120.0 . . ?
C55 C56 H56 120.0 . . ?
C57 C56 H56 120.0 . . ?
C58 C57 C56 120.0 . . ?
C58 C57 H57 120.0 . . ?
C56 C57 H57 120.0 . . ?
C57 C58 C53 120.0 . . ?
C57 C58 H58 120.0 . . ?
C53 C58 H58 120.0 . . ?
C60 C59 C64 120.0 . . ?
C60 C59 P2 120.2(7) . . ?
C64 C59 P2 119.8(7) . . ?
C59 C60 C61 120.0 . . ?
C59 C60 H60 120.0 . . ?
C61 C60 H60 120.0 . . ?
C60 C61 C62 120.0 . . ?
C60 C61 H61 120.0 . . ?
C62 C61 H61 120.0 . . ?
C63 C62 C61 120.0 . . ?
C63 C62 H62 120.0 . . ?
C61 C62 H62 120.0 . . ?
C62 C63 C64 120.0 . . ?
C62 C63 H63 120.0 . . ?
C64 C63 H63 120.0 . . ?
C63 C64 C59 120.0 . . ?
C63 C64 H64 120.0 . . ?
C59 C64 H64 120.0 . . ?
N1 C101 C102 176(3) . . ?
C101 C102 H10A 109.5 . . ?
C101 C102 H10B 109.5 . . ?
H10A C102 H10B 109.5 . . ?
C101 C102 H10C 109.5 . . ?
H10A C102 H10C 109.5 . . ?
H10B C102 H10C 109.5 . . ?
N2 C201 C202 151(3) . . ?
C201 C202 H20A 109.5 . . ?
C201 C202 H20B 109.5 . . ?
H20A C202 H20B 109.5 . . ?
C201 C202 H20C 109.5 . . ?
H20A C202 H20C 109.5 . . ?
H20B C202 H20C 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 Pt2 C2 -54.6(6) . . . . ?
Pt1 Pt1 Pt2 C2 128.4(5) 3_656 . . . ?
Sn1 Pt1 Pt2 C2 34.7(5) . . . . ?
Pt3 Pt1 Pt2 C2 -157.6(5) . . . . ?
Sn3 Pt1 Pt2 C2 52.3(5) 3_656 . . . ?
Pt3 Pt1 Pt2 C2 75.6(5) 3_656 . . . ?
Pt2 Pt1 Pt2 C2 128.4(5) 3_656 . . . ?
Sn3 Pt1 Pt2 C2 179.4(5) . . . . ?
C1 Pt1 Pt2 Sn3 -106.8(3) . . . 3_656 ?
Pt1 Pt1 Pt2 Sn3 76.16(3) 3_656 . . 3_656 ?
Sn1 Pt1 Pt2 Sn3 -17.56(4) . . . 3_656 ?
Pt3 Pt1 Pt2 Sn3 150.15(2) . . . 3_656 ?
Pt3 Pt1 Pt2 Sn3 23.30(2) 3_656 . . 3_656 ?
Pt2 Pt1 Pt2 Sn3 76.17(3) 3_656 . . 3_656 ?
Sn3 Pt1 Pt2 Sn3 127.133(15) . . . 3_656 ?
C1 Pt1 Pt2 Pt3 103.0(3) . . . . ?
Pt1 Pt1 Pt2 Pt3 -73.98(4) 3_656 . . . ?
Sn1 Pt1 Pt2 Pt3 -167.70(4) . . . . ?
Sn3 Pt1 Pt2 Pt3 -150.15(2) 3_656 . . . ?
Pt3 Pt1 Pt2 Pt3 -126.85(2) 3_656 . . . ?
Pt2 Pt1 Pt2 Pt3 -73.98(4) 3_656 . . . ?
Sn3 Pt1 Pt2 Pt3 -23.015(18) . . . . ?
C1 Pt1 Pt2 Sn2 57.5(2) . . . . ?
Pt1 Pt1 Pt2 Sn2 -119.50(3) 3_656 . . . ?
Sn1 Pt1 Pt2 Sn2 146.78(4) . . . . ?
Pt3 Pt1 Pt2 Sn2 -45.52(2) . . . . ?
Sn3 Pt1 Pt2 Sn2 164.33(2) 3_656 . . . ?
Pt3 Pt1 Pt2 Sn2 -172.372(16) 3_656 . . . ?
Pt2 Pt1 Pt2 Sn2 -119.50(3) 3_656 . . . ?
Sn3 Pt1 Pt2 Sn2 -68.53(2) . . . . ?
C1 Pt1 Pt2 Sn1 154.2(2) . . . 3_656 ?
Pt1 Pt1 Pt2 Sn1 -22.753(19) 3_656 . . 3_656 ?
Sn1 Pt1 Pt2 Sn1 -116.47(5) . . . 3_656 ?
Pt3 Pt1 Pt2 Sn1 51.23(3) . . . 3_656 ?
Sn3 Pt1 Pt2 Sn1 -98.92(3) 3_656 . . 3_656 ?
Pt3 Pt1 Pt2 Sn1 -75.622(19) 3_656 . . 3_656 ?
Pt2 Pt1 Pt2 Sn1 -22.753(19) 3_656 . . 3_656 ?
Sn3 Pt1 Pt2 Sn1 28.21(3) . . . 3_656 ?
C1 Pt1 Pt2 Pt1 177.0(2) . . . 3_656 ?
Sn1 Pt1 Pt2 Pt1 -93.72(5) . . . 3_656 ?
Pt3 Pt1 Pt2 Pt1 73.98(4) . . . 3_656 ?
Sn3 Pt1 Pt2 Pt1 -76.16(3) 3_656 . . 3_656 ?
Pt3 Pt1 Pt2 Pt1 -52.87(2) 3_656 . . 3_656 ?
Pt2 Pt1 Pt2 Pt1 0.0 3_656 . . 3_656 ?
Sn3 Pt1 Pt2 Pt1 50.97(3) . . . 3_656 ?
C2 Pt2 Pt3 C3 -16.0(9) . . . . ?
Sn3 Pt2 Pt3 C3 158.1(7) 3_656 . . . ?
Sn2 Pt2 Pt3 C3 -43.4(7) . . . . ?
Sn1 Pt2 Pt3 C3 66.9(7) 3_656 . . . ?
Pt1 Pt2 Pt3 C3 -169.4(7) . . . . ?
Pt1 Pt2 Pt3 C3 128.9(7) 3_656 . . . ?
C2 Pt2 Pt3 Sn3 -175.5(6) . . . . ?
Sn3 Pt2 Pt3 Sn3 -1.45(4) 3_656 . . . ?
Sn2 Pt2 Pt3 Sn3 157.09(3) . . . . ?
Sn1 Pt2 Pt3 Sn3 -92.67(4) 3_656 . . . ?
Pt1 Pt2 Pt3 Sn3 31.04(2) . . . . ?
Pt1 Pt2 Pt3 Sn3 -30.67(2) 3_656 . . . ?
C2 Pt2 Pt3 Sn2 27.4(6) . . . . ?
Sn3 Pt2 Pt3 Sn2 -158.53(3) 3_656 . . . ?
Sn1 Pt2 Pt3 Sn2 110.24(4) 3_656 . . . ?
Pt1 Pt2 Pt3 Sn2 -126.049(19) . . . . ?
Pt1 Pt2 Pt3 Sn2 172.241(17) 3_656 . . . ?
C2 Pt2 Pt3 Pt1 153.4(6) . . . . ?
Sn3 Pt2 Pt3 Pt1 -32.48(2) 3_656 . . . ?
Sn2 Pt2 Pt3 Pt1 126.049(19) . . . . ?
Sn1 Pt2 Pt3 Pt1 -123.71(3) 3_656 . . . ?
Pt1 Pt2 Pt3 Pt1 -61.710(13) 3_656 . . . ?
C2 Pt2 Pt3 Sn1 -82.9(6) . . . 3_656 ?
Sn3 Pt2 Pt3 Sn1 91.22(4) 3_656 . . 3_656 ?
Sn2 Pt2 Pt3 Sn1 -110.24(4) . . . 3_656 ?
Pt1 Pt2 Pt3 Sn1 123.71(3) . . . 3_656 ?
Pt1 Pt2 Pt3 Sn1 62.00(3) 3_656 . . 3_656 ?
C2 Pt2 Pt3 Pt1 -144.9(6) . . . 3_656 ?
Sn3 Pt2 Pt3 Pt1 29.23(2) 3_656 . . 3_656 ?
Sn2 Pt2 Pt3 Pt1 -172.241(17) . . . 3_656 ?
Sn1 Pt2 Pt3 Pt1 -62.00(3) 3_656 . . 3_656 ?
Pt1 Pt2 Pt3 Pt1 61.710(13) . . . 3_656 ?
C1 Pt1 Pt3 C3 85.8(7) . . . . ?
Pt1 Pt1 Pt3 C3 -113.3(6) 3_656 . . . ?
Sn1 Pt1 Pt3 C3 -19.2(6) . . . . ?
Pt2 Pt1 Pt3 C3 169.3(6) . . . . ?
Sn3 Pt1 Pt3 C3 -166.3(6) 3_656 . . . ?
Pt3 Pt1 Pt3 C3 -113.3(6) 3_656 . . . ?
Pt2 Pt1 Pt3 C3 -62.8(6) 3_656 . . . ?
Sn3 Pt1 Pt3 C3 -39.8(6) . . . . ?
C1 Pt1 Pt3 Sn3 125.6(3) . . . . ?
Pt1 Pt1 Pt3 Sn3 -73.51(3) 3_656 . . . ?
Sn1 Pt1 Pt3 Sn3 20.55(3) . . . . ?
Pt2 Pt1 Pt3 Sn3 -150.89(2) . . . . ?
Sn3 Pt1 Pt3 Sn3 -126.52(2) 3_656 . . . ?
Pt3 Pt1 Pt3 Sn3 -73.51(3) 3_656 . . . ?
Pt2 Pt1 Pt3 Sn3 -23.05(2) 3_656 . . . ?
C1 Pt1 Pt3 Sn2 -37.1(3) . . . . ?
Pt1 Pt1 Pt3 Sn2 123.808(19) 3_656 . . . ?
Sn1 Pt1 Pt3 Sn2 -142.14(4) . . . . ?
Pt2 Pt1 Pt3 Sn2 46.42(3) . . . . ?
Sn3 Pt1 Pt3 Sn2 70.80(3) 3_656 . . . ?
Pt3 Pt1 Pt3 Sn2 123.808(19) 3_656 . . . ?
Pt2 Pt1 Pt3 Sn2 174.270(16) 3_656 . . . ?
Sn3 Pt1 Pt3 Sn2 -162.68(2) . . . . ?
C1 Pt1 Pt3 Pt2 -83.5(3) . . . . ?
Pt1 Pt1 Pt3 Pt2 77.38(3) 3_656 . . . ?
Sn1 Pt1 Pt3 Pt2 171.44(3) . . . . ?
Sn3 Pt1 Pt3 Pt2 24.376(16) 3_656 . . . ?
Pt3 Pt1 Pt3 Pt2 77.38(3) 3_656 . . . ?
Pt2 Pt1 Pt3 Pt2 127.85(3) 3_656 . . . ?
Sn3 Pt1 Pt3 Pt2 150.89(2) . . . . ?
C1 Pt1 Pt3 Sn1 -130.0(3) . . . 3_656 ?
Pt1 Pt1 Pt3 Sn1 30.94(2) 3_656 . . 3_656 ?
Sn1 Pt1 Pt3 Sn1 124.99(3) . . . 3_656 ?
Pt2 Pt1 Pt3 Sn1 -46.444(18) . . . 3_656 ?
Sn3 Pt1 Pt3 Sn1 -22.07(2) 3_656 . . 3_656 ?
Pt3 Pt1 Pt3 Sn1 30.94(2) 3_656 . . 3_656 ?
Pt2 Pt1 Pt3 Sn1 81.40(2) 3_656 . . 3_656 ?
Sn3 Pt1 Pt3 Sn1 104.45(2) . . . 3_656 ?
C1 Pt1 Pt3 Pt1 -160.9(3) . . . 3_656 ?
Sn1 Pt1 Pt3 Pt1 94.05(4) . . . 3_656 ?
Pt2 Pt1 Pt3 Pt1 -77.38(3) . . . 3_656 ?
Sn3 Pt1 Pt3 Pt1 -53.01(3) 3_656 . . 3_656 ?
Pt3 Pt1 Pt3 Pt1 0.0 3_656 . . 3_656 ?
Pt2 Pt1 Pt3 Pt1 50.461(12) 3_656 . . 3_656 ?
Sn3 Pt1 Pt3 Pt1 73.51(3) . . . 3_656 ?
C1 Pt1 Sn1 Cl3 -58.5(3) . . . . ?
Pt1 Pt1 Sn1 Cl3 128.24(7) 3_656 . . . ?
Pt2 Pt1 Sn1 Cl3 -148.25(7) . . . . ?
Pt3 Pt1 Sn1 Cl3 50.20(7) . . . . ?
Sn3 Pt1 Sn1 Cl3 -162.73(6) 3_656 . . . ?
Pt3 Pt1 Sn1 Cl3 165.40(7) 3_656 . . . ?
Pt2 Pt1 Sn1 Cl3 102.99(7) 3_656 . . . ?
Sn3 Pt1 Sn1 Cl3 66.24(7) . . . . ?
C1 Pt1 Sn1 Cl2 41.3(3) . . . . ?
Pt1 Pt1 Sn1 Cl2 -131.95(7) 3_656 . . . ?
Pt2 Pt1 Sn1 Cl2 -48.44(8) . . . . ?
Pt3 Pt1 Sn1 Cl2 150.01(7) . . . . ?
Sn3 Pt1 Sn1 Cl2 -62.91(7) 3_656 . . . ?
Pt3 Pt1 Sn1 Cl2 -94.79(7) 3_656 . . . ?
Pt2 Pt1 Sn1 Cl2 -157.20(7) 3_656 . . . ?
Sn3 Pt1 Sn1 Cl2 166.06(7) . . . . ?
C1 Pt1 Sn1 Cl1 170.1(3) . . . . ?
Pt1 Pt1 Sn1 Cl1 -3.15(16) 3_656 . . . ?
Pt2 Pt1 Sn1 Cl1 80.37(16) . . . . ?
Pt3 Pt1 Sn1 Cl1 -81.18(16) . . . . ?
Sn3 Pt1 Sn1 Cl1 65.89(16) 3_656 . . . ?
Pt3 Pt1 Sn1 Cl1 34.02(15) 3_656 . . . ?
Pt2 Pt1 Sn1 Cl1 -28.40(15) 3_656 . . . ?
Sn3 Pt1 Sn1 Cl1 -65.14(16) . . . . ?
C1 Pt1 Sn1 Pt2 -161.5(3) . . . 3_656 ?
Pt1 Pt1 Sn1 Pt2 25.251(19) 3_656 . . 3_656 ?
Pt2 Pt1 Sn1 Pt2 108.77(5) . . . 3_656 ?
Pt3 Pt1 Sn1 Pt2 -52.78(4) . . . 3_656 ?
Sn3 Pt1 Sn1 Pt2 94.29(3) 3_656 . . 3_656 ?
Pt3 Pt1 Sn1 Pt2 62.417(15) 3_656 . . 3_656 ?
Sn3 Pt1 Sn1 Pt2 -36.74(3) . . . 3_656 ?
C1 Pt1 Sn1 Pt3 136.1(3) . . . 3_656 ?
Pt1 Pt1 Sn1 Pt3 -37.17(2) 3_656 . . 3_656 ?
Pt2 Pt1 Sn1 Pt3 46.35(5) . . . 3_656 ?
Pt3 Pt1 Sn1 Pt3 -115.20(3) . . . 3_656 ?
Sn3 Pt1 Sn1 Pt3 31.87(3) 3_656 . . 3_656 ?
Pt2 Pt1 Sn1 Pt3 -62.417(15) 3_656 . . 3_656 ?
Sn3 Pt1 Sn1 Pt3 -99.16(2) . . . 3_656 ?
C3 Pt3 Sn2 Cl6 113.4(4) . . . . ?
Sn3 Pt3 Sn2 Cl6 -144.86(19) . . . . ?
Pt2 Pt3 Sn2 Cl6 -46.03(19) . . . . ?
Pt1 Pt3 Sn2 Cl6 -91.68(19) . . . . ?
Sn1 Pt3 Sn2 Cl6 7.80(19) 3_656 . . . ?
Pt1 Pt3 Sn2 Cl6 -37.65(19) 3_656 . . . ?
C3 Pt3 Sn2 Cl5 -98.3(4) . . . . ?
Sn3 Pt3 Sn2 Cl5 3.38(10) . . . . ?
Pt2 Pt3 Sn2 Cl5 102.22(8) . . . . ?
Pt1 Pt3 Sn2 Cl5 56.56(8) . . . . ?
Sn1 Pt3 Sn2 Cl5 156.04(7) 3_656 . . . ?
Pt1 Pt3 Sn2 Cl5 110.60(8) 3_656 . . . ?
C3 Pt3 Sn2 Cl4 2.6(4) . . . . ?
Sn3 Pt3 Sn2 Cl4 104.26(10) . . . . ?
Pt2 Pt3 Sn2 Cl4 -156.91(8) . . . . ?
Pt1 Pt3 Sn2 Cl4 157.44(7) . . . . ?
Sn1 Pt3 Sn2 Cl4 -103.08(8) 3_656 . . . ?
Pt1 Pt3 Sn2 Cl4 -148.53(7) 3_656 . . . ?
C3 Pt3 Sn2 Pt2 159.5(3) . . . . ?
Sn3 Pt3 Sn2 Pt2 -98.83(6) . . . . ?
Pt1 Pt3 Sn2 Pt2 -45.650(14) . . . . ?
Sn1 Pt3 Sn2 Pt2 53.82(3) 3_656 . . . ?
Pt1 Pt3 Sn2 Pt2 8.380(19) 3_656 . . . ?
C2 Pt2 Sn2 Cl6 -5.9(3) . . . . ?
Sn3 Pt2 Sn2 Cl6 -99.94(11) 3_656 . . . ?
Pt3 Pt2 Sn2 Cl6 160.29(9) . . . . ?
Sn1 Pt2 Sn2 Cl6 102.08(10) 3_656 . . . ?
Pt1 Pt2 Sn2 Cl6 -151.62(9) . . . . ?
Pt1 Pt2 Sn2 Cl6 152.20(9) 3_656 . . . ?
C2 Pt2 Sn2 Cl5 93.2(3) . . . . ?
Sn3 Pt2 Sn2 Cl5 -0.85(11) 3_656 . . . ?
Pt3 Pt2 Sn2 Cl5 -100.63(9) . . . . ?
Sn1 Pt2 Sn2 Cl5 -158.83(8) 3_656 . . . ?
Pt1 Pt2 Sn2 Cl5 -52.53(9) . . . . ?
Pt1 Pt2 Sn2 Cl5 -108.71(8) 3_656 . . . ?
C2 Pt2 Sn2 Cl4 -114.3(4) . . . . ?
Sn3 Pt2 Sn2 Cl4 151.63(16) 3_656 . . . ?
Pt3 Pt2 Sn2 Cl4 51.86(16) . . . . ?
Sn1 Pt2 Sn2 Cl4 -6.34(16) 3_656 . . . ?
Pt1 Pt2 Sn2 Cl4 99.95(16) . . . . ?
Pt1 Pt2 Sn2 Cl4 43.77(16) 3_656 . . . ?
C2 Pt2 Sn2 Pt3 -166.2(3) . . . . ?
Sn3 Pt2 Sn2 Pt3 99.78(7) 3_656 . . . ?
Sn1 Pt2 Sn2 Pt3 -58.20(3) 3_656 . . . ?
Pt1 Pt2 Sn2 Pt3 48.094(18) . . . . ?
Pt1 Pt2 Sn2 Pt3 -8.087(18) 3_656 . . . ?
C3 Pt3 Sn3 Cl7 57.8(4) . . . . ?
Sn2 Pt3 Sn3 Cl7 -44.94(11) . . . . ?
Pt2 Pt3 Sn3 Cl7 -132.45(10) . . . . ?
Pt1 Pt3 Sn3 Cl7 -103.40(10) . . . . ?
Sn1 Pt3 Sn3 Cl7 163.72(9) 3_656 . . . ?
Pt1 Pt3 Sn3 Cl7 -163.02(10) 3_656 . . . ?
C3 Pt3 Sn3 Cl8 -46.2(4) . . . . ?
Sn2 Pt3 Sn3 Cl8 -148.96(10) . . . . ?
Pt2 Pt3 Sn3 Cl8 123.54(9) . . . . ?
Pt1 Pt3 Sn3 Cl8 152.58(9) . . . . ?
Sn1 Pt3 Sn3 Cl8 59.71(9) 3_656 . . . ?
Pt1 Pt3 Sn3 Cl8 92.96(9) 3_656 . . . ?
C3 Pt3 Sn3 Pt2 -168.4(3) . . . 3_656 ?
Sn2 Pt3 Sn3 Pt2 88.90(7) . . . 3_656 ?
Pt2 Pt3 Sn3 Pt2 1.39(4) . . . 3_656 ?
Pt1 Pt3 Sn3 Pt2 30.43(2) . . . 3_656 ?
Sn1 Pt3 Sn3 Pt2 -62.44(4) 3_656 . . 3_656 ?
Pt1 Pt3 Sn3 Pt2 -29.18(2) 3_656 . . 3_656 ?
C3 Pt3 Sn3 Pt1 -139.2(3) . . . 3_656 ?
Sn2 Pt3 Sn3 Pt1 118.08(6) . . . 3_656 ?
Pt2 Pt3 Sn3 Pt1 30.57(2) . . . 3_656 ?
Pt1 Pt3 Sn3 Pt1 59.617(14) . . . 3_656 ?
Sn1 Pt3 Sn3 Pt1 -33.26(2) 3_656 . . 3_656 ?
C3 Pt3 Sn3 Pt1 161.2(3) . . . . ?
Sn2 Pt3 Sn3 Pt1 58.46(7) . . . . ?
Pt2 Pt3 Sn3 Pt1 -29.043(19) . . . . ?
Sn1 Pt3 Sn3 Pt1 -92.87(3) 3_656 . . . ?
Pt1 Pt3 Sn3 Pt1 -59.617(14) 3_656 . . . ?
C1 Pt1 Sn3 Cl7 28.8(3) . . . . ?
Pt1 Pt1 Sn3 Cl7 -177.12(9) 3_656 . . . ?
Sn1 Pt1 Sn3 Cl7 -63.89(9) . . . . ?
Pt2 Pt1 Sn3 Cl7 129.27(9) . . . . ?
Pt3 Pt1 Sn3 Cl7 104.70(10) . . . . ?
Sn3 Pt1 Sn3 Cl7 -177.12(9) 3_656 . . . ?
Pt3 Pt1 Sn3 Cl7 -127.24(10) 3_656 . . . ?
Pt2 Pt1 Sn3 Cl7 -105.27(10) 3_656 . . . ?
C1 Pt1 Sn3 Cl8 -155.2(3) . . . . ?
Pt1 Pt1 Sn3 Cl8 -1.14(17) 3_656 . . . ?
Sn1 Pt1 Sn3 Cl8 112.09(18) . . . . ?
Pt2 Pt1 Sn3 Cl8 -54.76(18) . . . . ?
Pt3 Pt1 Sn3 Cl8 -79.32(18) . . . . ?
Sn3 Pt1 Sn3 Cl8 -1.14(17) 3_656 . . . ?
Pt3 Pt1 Sn3 Cl8 48.74(18) 3_656 . . . ?
Pt2 Pt1 Sn3 Cl8 70.71(18) 3_656 . . . ?
C1 Pt1 Sn3 Pt3 -75.9(3) . . . . ?
Pt1 Pt1 Sn3 Pt3 78.17(3) 3_656 . . . ?
Sn1 Pt1 Sn3 Pt3 -168.596(19) . . . . ?
Pt2 Pt1 Sn3 Pt3 24.56(2) . . . . ?
Sn3 Pt1 Sn3 Pt3 78.17(3) 3_656 . . . ?
Pt3 Pt1 Sn3 Pt3 128.059(14) 3_656 . . . ?
Pt2 Pt1 Sn3 Pt3 150.03(2) 3_656 . . . ?
C1 Pt1 Sn3 Pt2 134.1(3) . . . 3_656 ?
Pt1 Pt1 Sn3 Pt2 -71.85(4) 3_656 . . 3_656 ?
Sn1 Pt1 Sn3 Pt2 41.38(2) . . . 3_656 ?
Pt2 Pt1 Sn3 Pt2 -125.47(3) . . . 3_656 ?
Pt3 Pt1 Sn3 Pt2 -150.03(2) . . . 3_656 ?
Sn3 Pt1 Sn3 Pt2 -71.85(4) 3_656 . . 3_656 ?
Pt3 Pt1 Sn3 Pt2 -21.967(16) 3_656 . . 3_656 ?
C1 Pt1 Sn3 Pt1 -154.1(3) . . . 3_656 ?
Sn1 Pt1 Sn3 Pt1 113.23(3) . . . 3_656 ?
Pt2 Pt1 Sn3 Pt1 -53.614(18) . . . 3_656 ?
Pt3 Pt1 Sn3 Pt1 -78.17(3) . . . 3_656 ?
Sn3 Pt1 Sn3 Pt1 0.0 3_656 . . 3_656 ?
Pt3 Pt1 Sn3 Pt1 49.88(3) 3_656 . . 3_656 ?
Pt2 Pt1 Sn3 Pt1 71.85(4) 3_656 . . 3_656 ?
Pt1 Pt1 C1 O1 91(8) 3_656 . . . ?
Sn1 Pt1 C1 O1 -73(8) . . . . ?
Pt2 Pt1 C1 O1 84(8) . . . . ?
Pt3 Pt1 C1 O1 140(8) . . . . ?
Sn3 Pt1 C1 O1 32(8) 3_656 . . . ?
Pt3 Pt1 C1 O1 -20(8) 3_656 . . . ?
Pt2 Pt1 C1 O1 -100(8) 3_656 . . . ?
Sn3 Pt1 C1 O1 -169(8) . . . . ?
Sn3 Pt2 C2 O2 -23(34) 3_656 . . . ?
Pt3 Pt2 C2 O2 152(33) . . . . ?
Sn2 Pt2 C2 O2 175(100) . . . . ?
Sn1 Pt2 C2 O2 82(34) 3_656 . . . ?
Pt1 Pt2 C2 O2 -69(34) . . . . ?
Pt1 Pt2 C2 O2 25(34) 3_656 . . . ?
Sn3 Pt3 C3 O3 65(10) . . . . ?
Sn2 Pt3 C3 O3 -135(10) . . . . ?
Pt2 Pt3 C3 O3 -98(9) . . . . ?
Pt1 Pt3 C3 O3 101(10) . . . . ?
Sn1 Pt3 C3 O3 -43(10) 3_656 . . . ?
Pt1 Pt3 C3 O3 12(10) 3_656 . . . ?
C23 P1 C11 C12 -128.4(8) . . . . ?
C29 P1 C11 C12 -7.7(9) . . . . ?
C17 P1 C11 C12 111.1(8) . . . . ?
C23 P1 C11 C16 51.4(9) . . . . ?
C29 P1 C11 C16 172.1(7) . . . . ?
C17 P1 C11 C16 -69.1(8) . . . . ?
C16 C11 C12 C13 2.1(14) . . . . ?
P1 C11 C12 C13 -178.1(7) . . . . ?
C11 C12 C13 C14 0.3(15) . . . . ?
C12 C13 C14 C15 -2.6(17) . . . . ?
C13 C14 C15 C16 2.4(18) . . . . ?
C14 C15 C16 C11 0.2(16) . . . . ?
C12 C11 C16 C15 -2.4(15) . . . . ?
P1 C11 C16 C15 177.8(8) . . . . ?
C23 P1 C17 C18 82.8(8) . . . . ?
C29 P1 C17 C18 -38.5(8) . . . . ?
C11 P1 C17 C18 -157.7(7) . . . . ?
C23 P1 C17 C22 -93.3(8) . . . . ?
C29 P1 C17 C22 145.4(7) . . . . ?
C11 P1 C17 C22 26.2(8) . . . . ?
C22 C17 C18 C19 -1.5(14) . . . . ?
P1 C17 C18 C19 -177.7(8) . . . . ?
C17 C18 C19 C20 0.3(16) . . . . ?
C18 C19 C20 C21 0.3(17) . . . . ?
C19 C20 C21 C22 0.4(16) . . . . ?
C20 C21 C22 C17 -1.7(15) . . . . ?
C18 C17 C22 C21 2.2(13) . . . . ?
P1 C17 C22 C21 178.2(7) . . . . ?
C29 P1 C23 C28 -72.7(11) . . . . ?
C11 P1 C23 C28 46.0(11) . . . . ?
C17 P1 C23 C28 168.5(9) . . . . ?
C29 P1 C23 C24 106.2(10) . . . . ?
C11 P1 C23 C24 -135.1(9) . . . . ?
C17 P1 C23 C24 -12.7(11) . . . . ?
C28 C23 C24 C25 -0.4(19) . . . . ?
P1 C23 C24 C25 -179.2(10) . . . . ?
C23 C24 C25 C26 -1(2) . . . . ?
C24 C25 C26 C27 4(2) . . . . ?
C25 C26 C27 C28 -5(2) . . . . ?
C24 C23 C28 C27 -1.2(19) . . . . ?
P1 C23 C28 C27 177.7(11) . . . . ?
C26 C27 C28 C23 4(2) . . . . ?
C23 P1 C29 C34 11.5(10) . . . . ?
C11 P1 C29 C34 -106.8(8) . . . . ?
C17 P1 C29 C34 131.3(8) . . . . ?
C23 P1 C29 C30 -170.9(8) . . . . ?
C11 P1 C29 C30 70.8(8) . . . . ?
C17 P1 C29 C30 -51.0(8) . . . . ?
C34 C29 C30 C31 3.7(15) . . . . ?
P1 C29 C30 C31 -174.1(8) . . . . ?
C29 C30 C31 C32 -4.2(16) . . . . ?
C30 C31 C32 C33 2.7(17) . . . . ?
C31 C32 C33 C34 -0.5(17) . . . . ?
C30 C29 C34 C33 -1.5(15) . . . . ?
P1 C29 C34 C33 176.1(8) . . . . ?
C32 C33 C34 C29 0.0(17) . . . . ?
C53 P2 C41 C42 -134.7(6) . . . . ?
C59 P2 C41 C42 106.9(7) . . . . ?
C47 P2 C41 C42 -16.9(8) . . . . ?
C53 P2 C41 C46 42.7(8) . . . . ?
C59 P2 C41 C46 -75.7(8) . . . . ?
C47 P2 C41 C46 160.5(7) . . . . ?
C46 C41 C42 C43 0.0 . . . . ?
P2 C41 C42 C43 177.4(9) . . . . ?
C41 C42 C43 C44 0.0 . . . . ?
C42 C43 C44 C45 0.0 . . . . ?
C43 C44 C45 C46 0.0 . . . . ?
C44 C45 C46 C41 0.0 . . . . ?
C42 C41 C46 C45 0.0 . . . . ?
P2 C41 C46 C45 -177.4(9) . . . . ?
C41 P2 C47 C48 64.2(7) . . . . ?
C53 P2 C47 C48 -178.4(5) . . . . ?
C59 P2 C47 C48 -59.5(6) . . . . ?
C41 P2 C47 C52 -117.2(6) . . . . ?
C53 P2 C47 C52 0.3(6) . . . . ?
C59 P2 C47 C52 119.1(6) . . . . ?
C52 C47 C48 C49 0.0 . . . . ?
P2 C47 C48 C49 178.6(7) . . . . ?
C47 C48 C49 C50 0.0 . . . . ?
C48 C49 C50 C51 0.0 . . . . ?
C49 C50 C51 C52 0.0 . . . . ?
C50 C51 C52 C47 0.0 . . . . ?
C48 C47 C52 C51 0.0 . . . . ?
P2 C47 C52 C51 -178.6(6) . . . . ?
C41 P2 C53 C54 49.5(6) . . . . ?
C59 P2 C53 C54 168.3(5) . . . . ?
C47 P2 C53 C54 -72.4(5) . . . . ?
C41 P2 C53 C58 -133.5(6) . . . . ?
C59 P2 C53 C58 -14.7(6) . . . . ?
C47 P2 C53 C58 104.6(5) . . . . ?
C58 C53 C54 C55 0.0 . . . . ?
P2 C53 C54 C55 177.1(5) . . . . ?
C53 C54 C55 C56 0.0 . . . . ?
C54 C55 C56 C57 0.0 . . . . ?
C55 C56 C57 C58 0.0 . . . . ?
C56 C57 C58 C53 0.0 . . . . ?
C54 C53 C58 C57 0.0 . . . . ?
P2 C53 C58 C57 -176.9(5) . . . . ?
C41 P2 C59 C60 -152.9(7) . . . . ?
C53 P2 C59 C60 90.4(6) . . . . ?
C47 P2 C59 C60 -27.1(7) . . . . ?
C41 P2 C59 C64 29.3(8) . . . . ?
C53 P2 C59 C64 -87.4(6) . . . . ?
C47 P2 C59 C64 155.1(6) . . . . ?
C64 C59 C60 C61 0.0 . . . . ?
P2 C59 C60 C61 -177.8(7) . . . . ?
C59 C60 C61 C62 0.0 . . . . ?
C60 C61 C62 C63 0.0 . . . . ?
C61 C62 C63 C64 0.0 . . . . ?
C62 C63 C64 C59 0.0 . . . . ?
C60 C59 C64 C63 0.0 . . . . ?
P2 C59 C64 C63 177.8(7) . . . . ?

_diffrn_measured_fraction_theta_max 0.999
_diffrn_reflns_theta_full        26.00
_diffrn_measured_fraction_theta_full 0.999
_refine_diff_density_max         1.651
_refine_diff_density_min         -1.037
_refine_diff_density_rms         0.135
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_5
_database_code_depnum_ccdc_archive 'CCDC 1439441'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C70 H58 Cl8 O18 P2 Pt10 Sn4'
_chemical_formula_weight         3958.36

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   P2(1)/n

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   12.596(4)
_cell_length_b                   18.116(5)
_cell_length_c                   20.422(6)
_cell_angle_alpha                90.00
_cell_angle_beta                 103.388(3)
_cell_angle_gamma                90.00
_cell_volume                     4534(2)
_cell_formula_units_Z            2
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    9321
_cell_measurement_theta_min      2.3385
_cell_measurement_theta_max      25.505

_exptl_crystal_description       plate
_exptl_crystal_colour            black
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.11
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.900
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3536
_exptl_absorpt_coefficient_mu    16.769
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.1523
_exptl_absorpt_correction_T_max  0.2599
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1653 (selected reflections only, before parameter refinement)
 R(int) = 0.0960 (selected reflections only, after parameter refinement)
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            31091
_diffrn_reflns_av_R_equivalents  0.1189
_diffrn_reflns_av_unetI/netI     0.0893
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_theta_min         1.52
_diffrn_reflns_theta_max         23.53
_reflns_number_total             6630
_reflns_number_gt                4164
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. The following restraints
 were applied (given as SHELXL lines): 
 isor .01 c2 c119 c5 c109 c115 c110 c111
 simu .01 c101 > c106
 simu .01 o1 > c8
 AFIX 66 on Ph rings
 dfix 1.43 .01 o200 c201 o200 c204
 dfix 1.53 .01 c201 c202 c202 c203 c203 c204
 simu .01 o200 > c204 
 The asymmetric unit of the unit cell contains one half of a cluster anion 
 (located on an inversion centre), one [PPh4]+ cation and one thf molecule 
 (all located on general positions). Similar U restraints have been applied 
 to the C and O atoms of the CO ligands (SIMU command in SHELXL, s.u. 0.01). 
 The C-atoms of the Ph-rings have been constrained to fit regular hexagons 
 (AFIX 66 command in SHELXL). Similar U restraints have been applied to 
 the thf molecule (SIMU command in SHELXL, s.u. 0.01). Restraints to bond 
 distances were applied as follow (s.u. 0.02): 1.43 Å for C O and 1.53 Å 
 for C C in thf. Due to the poor quality of these crystals, the data 
 have been cut at 2? = 47.06° and some high residual electron densities 
 remain close to the Pt atoms. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.1515P)²+629.2802P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         6630
_refine_ls_number_parameters     432
_refine_ls_number_restraints     130
_refine_ls_R_factor_all          0.1667
_refine_ls_R_factor_gt           0.0997
_refine_ls_wR_factor_ref         0.3130
_refine_ls_wR_factor_gt          0.2465
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_restrained_S_all      1.040
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.68439(13) 0.96118(9) 0.05965(9) 0.0402(5) Uani 1 1 d . . .
Pt2 Pt 0.47270(12) 0.91855(8) -0.00052(8) 0.0371(4) Uani 1 1 d . . .
Pt3 Pt 0.70315(13) 1.04200(9) -0.05923(9) 0.0445(5) Uani 1 1 d . . .
Pt4 Pt 0.64052(14) 0.89833(9) -0.06904(9) 0.0451(5) Uani 1 1 d . . .
Pt5 Pt 0.51448(13) 0.98762(9) 0.12273(9) 0.0424(5) Uani 1 1 d . . .
Sn1 Sn 0.4252(3) 0.84472(17) 0.11045(17) 0.0518(8) Uani 1 1 d . . .
Sn2 Sn 0.6406(2) 0.81192(16) 0.03777(17) 0.0479(8) Uani 1 1 d . . .
Cl1 Cl 0.4152(15) 0.8226(9) 0.2237(8) 0.094(5) Uani 1 1 d . . .
Cl2 Cl 0.3239(12) 0.7368(7) 0.0644(9) 0.084(4) Uani 1 1 d . . .
Cl3 Cl 0.5743(11) 0.6957(6) -0.0111(7) 0.068(4) Uani 1 1 d . . .
Cl4 Cl 0.8184(10) 0.7663(7) 0.0890(7) 0.068(3) Uani 1 1 d . . .
O1 O 0.572(2) 0.7948(18) 0.1218(15) 0.059(9) Uani 1 1 d . . .
H1 H 0.6057 0.7675 0.1596 0.070 Uiso 1 1 calc R . .
O2 O 0.486(3) 1.034(2) 0.259(2) 0.086(10) Uani 1 1 d U . .
O3 O 0.332(3) 0.819(2) -0.103(2) 0.089(11) Uani 1 1 d U . .
O4 O 0.826(3) 0.9390(19) -0.127(2) 0.081(10) Uani 1 1 d U . .
O5 O 0.932(3) 0.966(2) 0.079(2) 0.076(9) Uani 1 1 d U . .
O6 O 0.599(4) 0.775(2) -0.1698(19) 0.092(11) Uani 1 1 d U . .
O7 O 0.908(3) 1.132(2) -0.029(2) 0.089(11) Uani 1 1 d U . .
O8 O 0.737(3) 0.966(2) 0.2061(18) 0.081(10) Uani 1 1 d U . .
C2 C 0.502(5) 1.013(4) 0.208(3) 0.086(13) Uani 1 1 d U . .
C3 C 0.383(4) 0.852(3) -0.063(3) 0.071(12) Uani 1 1 d U . .
C4 C 0.758(4) 0.948(3) -0.097(3) 0.077(12) Uani 1 1 d U . .
C5 C 0.839(4) 0.965(3) 0.074(3) 0.065(10) Uani 1 1 d U . .
C6 C 0.617(6) 0.814(3) -0.130(3) 0.085(13) Uani 1 1 d U . .
C7 C 0.829(4) 1.103(3) -0.041(3) 0.083(12) Uani 1 1 d U . .
C8 C 0.677(5) 0.972(3) 0.151(3) 0.078(12) Uani 1 1 d U . .
P1 P 0.2772(10) 0.9622(7) 0.3944(7) 0.055(3) Uani 1 1 d . . .
C101 C 0.382(2) 0.8949(19) 0.398(2) 0.083(8) Uani 1 1 d GU . .
C102 C 0.489(3) 0.9105(17) 0.395(2) 0.084(8) Uani 1 1 d GU . .
H102 H 0.5082 0.9584 0.3860 0.101 Uiso 1 1 calc R . .
C103 C 0.567(2) 0.855(2) 0.406(2) 0.085(8) Uani 1 1 d GU . .
H103 H 0.6381 0.8652 0.4036 0.102 Uiso 1 1 calc R . .
C104 C 0.538(3) 0.7833(19) 0.419(2) 0.087(8) Uani 1 1 d GU . .
H104 H 0.5898 0.7459 0.4261 0.104 Uiso 1 1 calc R . .
C105 C 0.431(3) 0.7676(17) 0.422(2) 0.087(8) Uani 1 1 d GU . .
H105 H 0.4115 0.7198 0.4310 0.105 Uiso 1 1 calc R . .
C106 C 0.353(2) 0.823(2) 0.411(2) 0.084(8) Uani 1 1 d GU . .
H106 H 0.2815 0.8129 0.4134 0.101 Uiso 1 1 calc R . .
C107 C 0.160(2) 0.9286(18) 0.3351(14) 0.072(16) Uani 1 1 d G . .
C108 C 0.175(2) 0.9124(19) 0.2712(16) 0.066(15) Uani 1 1 d G . .
H108 H 0.2427 0.9195 0.2614 0.080 Uiso 1 1 calc R . .
C109 C 0.088(3) 0.886(2) 0.2220(13) 0.093(19) Uani 1 1 d GU . .
H109 H 0.0979 0.8748 0.1793 0.112 Uiso 1 1 calc R . .
C110 C -0.013(2) 0.875(2) 0.2366(16) 0.077(16) Uani 1 1 d GU . .
H110 H -0.0713 0.8571 0.2037 0.092 Uiso 1 1 calc R . .
C111 C -0.028(2) 0.8912(19) 0.3005(18) 0.083(17) Uani 1 1 d GU . .
H111 H -0.0956 0.8841 0.3102 0.100 Uiso 1 1 calc R . .
C112 C 0.059(3) 0.9180(18) 0.3497(14) 0.053(12) Uani 1 1 d G . .
H112 H 0.0492 0.9289 0.3924 0.063 Uiso 1 1 calc R . .
C113 C 0.249(3) 0.9756(18) 0.4745(14) 0.063(14) Uani 1 1 d G . .
C114 C 0.185(2) 1.0358(16) 0.4823(15) 0.054(12) Uani 1 1 d G . .
H114 H 0.1572 1.0667 0.4459 0.065 Uiso 1 1 calc R . .
C115 C 0.162(3) 1.0499(17) 0.5444(19) 0.079(16) Uani 1 1 d GU . .
H115 H 0.1186 1.0903 0.5496 0.094 Uiso 1 1 calc R . .
C116 C 0.203(3) 1.004(2) 0.5987(14) 0.09(2) Uani 1 1 d G . .
H116 H 0.1872 1.0133 0.6403 0.113 Uiso 1 1 calc R . .
C117 C 0.267(3) 0.944(2) 0.5910(15) 0.10(2) Uani 1 1 d G . .
H117 H 0.2945 0.9127 0.6273 0.115 Uiso 1 1 calc R . .
C118 C 0.290(3) 0.9294(17) 0.5288(19) 0.072(15) Uani 1 1 d G . .
H118 H 0.3332 0.8891 0.5236 0.086 Uiso 1 1 calc R . .
C119 C 0.313(2) 1.0499(13) 0.3666(14) 0.048(11) Uani 1 1 d GU . .
C120 C 0.263(2) 1.0787(18) 0.3039(14) 0.080(19) Uani 1 1 d G . .
H120 H 0.2095 1.0517 0.2748 0.096 Uiso 1 1 calc R . .
C121 C 0.293(3) 1.1478(19) 0.2849(17) 0.09(2) Uani 1 1 d G . .
H121 H 0.2600 1.1671 0.2430 0.103 Uiso 1 1 calc R . .
C122 C 0.374(3) 1.1881(14) 0.329(2) 0.12(3) Uani 1 1 d G . .
H122 H 0.3940 1.2344 0.3158 0.143 Uiso 1 1 calc R . .
C123 C 0.424(3) 1.1593(17) 0.391(2) 0.09(2) Uani 1 1 d G . .
H123 H 0.4775 1.1863 0.4203 0.107 Uiso 1 1 calc R . .
C124 C 0.394(3) 1.0903(17) 0.4102(14) 0.067(15) Uani 1 1 d G . .
H124 H 0.4270 1.0710 0.4521 0.080 Uiso 1 1 calc R . .
O200 O 0.608(4) 0.670(3) 0.186(3) 0.126(12) Uiso 1 1 d DU . .
C201 C 0.677(5) 0.675(5) 0.252(3) 0.130(13) Uiso 1 1 d DU . .
H20A H 0.7030 0.7255 0.2611 0.156 Uiso 1 1 calc R . .
H20B H 0.7394 0.6429 0.2564 0.156 Uiso 1 1 calc R . .
C202 C 0.609(6) 0.653(4) 0.302(4) 0.133(13) Uiso 1 1 d DU . .
H20C H 0.6534 0.6277 0.3408 0.160 Uiso 1 1 calc R . .
H20D H 0.5739 0.6949 0.3170 0.160 Uiso 1 1 calc R . .
C203 C 0.524(6) 0.600(4) 0.261(3) 0.132(13) Uiso 1 1 d DU . .
H20E H 0.4536 0.6069 0.2708 0.158 Uiso 1 1 calc R . .
H20F H 0.5467 0.5489 0.2694 0.158 Uiso 1 1 calc R . .
C204 C 0.521(6) 0.620(4) 0.187(3) 0.131(13) Uiso 1 1 d DU . .
H20G H 0.5276 0.5764 0.1618 0.157 Uiso 1 1 calc R . .
H20H H 0.4514 0.6438 0.1673 0.157 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C8 1.90(5) . ?
Pt1 C5 1.90(5) . ?
Pt1 Pt2 2.775(2) . ?
Pt1 Sn2 2.775(3) . ?
Pt1 Pt5 2.783(2) . ?
Pt1 Pt4 2.799(2) . ?
Pt1 Pt3 2.891(2) . ?
Pt1 Pt2 3.002(2) 3_675 ?
Pt2 C3 1.92(5) . ?
Pt2 Pt5 2.750(2) . ?
Pt2 Sn1 2.813(3) . ?
Pt2 Pt4 2.816(2) . ?
Pt2 Sn2 2.837(3) . ?
Pt2 Pt3 2.856(2) 3_675 ?
Pt2 Pt1 3.002(2) 3_675 ?
Pt2 Pt2 3.029(3) 3_675 ?
Pt2 Pt5 3.055(2) 3_675 ?
Pt3 C7 1.90(5) . ?
Pt3 C4 2.06(4) . ?
Pt3 Sn1 2.671(3) 3_675 ?
Pt3 Pt4 2.713(2) . ?
Pt3 Pt5 2.800(2) 3_675 ?
Pt3 Pt2 2.856(2) 3_675 ?
Pt4 C4 1.93(5) . ?
Pt4 C6 1.95(5) . ?
Pt4 Sn2 2.685(4) . ?
Pt4 Pt5 2.879(2) 3_675 ?
Pt5 C2 1.85(7) . ?
Pt5 C8 2.02(6) . ?
Pt5 Pt3 2.800(2) 3_675 ?
Pt5 Sn1 2.810(4) . ?
Pt5 Pt4 2.879(2) 3_675 ?
Pt5 Pt2 3.055(2) 3_675 ?
Sn1 O1 2.03(3) . ?
Sn1 Cl1 2.380(15) . ?
Sn1 Cl2 2.405(14) . ?
Sn1 Pt3 2.671(3) 3_675 ?
Sn2 O1 2.11(3) . ?
Sn2 Cl4 2.389(12) . ?
Sn2 Cl3 2.396(12) . ?
O1 H1 0.9300 . ?
O2 C2 1.15(7) . ?
O3 C3 1.09(6) . ?
O4 C4 1.17(5) . ?
O5 C5 1.16(6) . ?
O6 C6 1.06(6) . ?
O7 C7 1.11(6) . ?
O8 C8 1.21(6) . ?
P1 C113 1.77(3) . ?
P1 C119 1.78(2) . ?
P1 C107 1.78(3) . ?
P1 C101 1.79(3) . ?
C101 C102 1.3900 . ?
C101 C106 1.3900 . ?
C102 C103 1.3900 . ?
C102 H102 0.9300 . ?
C103 C104 1.3900 . ?
C103 H103 0.9300 . ?
C104 C105 1.3900 . ?
C104 H104 0.9300 . ?
C105 C106 1.3900 . ?
C105 H105 0.9300 . ?
C106 H106 0.9300 . ?
C107 C108 1.3900 . ?
C107 C112 1.3900 . ?
C108 C109 1.3900 . ?
C108 H108 0.9300 . ?
C109 C110 1.3900 . ?
C109 H109 0.9300 . ?
C110 C111 1.3900 . ?
C110 H110 0.9300 . ?
C111 C112 1.3900 . ?
C111 H111 0.9300 . ?
C112 H112 0.9300 . ?
C113 C114 1.3900 . ?
C113 C118 1.3900 . ?
C114 C115 1.3900 . ?
C114 H114 0.9300 . ?
C115 C116 1.3900 . ?
C115 H115 0.9300 . ?
C116 C117 1.3900 . ?
C116 H116 0.9300 . ?
C117 C118 1.3900 . ?
C117 H117 0.9300 . ?
C118 H118 0.9300 . ?
C119 C120 1.3900 . ?
C119 C124 1.3900 . ?
C120 C121 1.3900 . ?
C120 H120 0.9300 . ?
C121 C122 1.3900 . ?
C121 H121 0.9300 . ?
C122 C123 1.3900 . ?
C122 H122 0.9300 . ?
C123 C124 1.3900 . ?
C123 H123 0.9300 . ?
C124 H124 0.9300 . ?
O200 C204 1.428(10) . ?
O200 C201 1.428(10) . ?
C201 C202 1.531(10) . ?
C201 H20A 0.9700 . ?
C201 H20B 0.9700 . ?
C202 C203 1.529(10) . ?
C202 H20C 0.9700 . ?
C202 H20D 0.9700 . ?
C203 C204 1.529(10) . ?
C203 H20E 0.9700 . ?
C203 H20F 0.9700 . ?
C204 H20G 0.9700 . ?
C204 H20H 0.9700 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C8 Pt1 C5 97(2) . . ?
C8 Pt1 Pt2 101.8(18) . . ?
C5 Pt1 Pt2 157.3(16) . . ?
C8 Pt1 Sn2 101.8(18) . . ?
C5 Pt1 Sn2 102.4(16) . . ?
Pt2 Pt1 Sn2 61.50(8) . . ?
C8 Pt1 Pt5 46.5(18) . . ?
C5 Pt1 Pt5 142.3(16) . . ?
Pt2 Pt1 Pt5 59.32(6) . . ?
Sn2 Pt1 Pt5 95.55(9) . . ?
C8 Pt1 Pt4 157.0(18) . . ?
C5 Pt1 Pt4 97.6(16) . . ?
Pt2 Pt1 Pt4 60.69(6) . . ?
Sn2 Pt1 Pt4 57.58(8) . . ?
Pt5 Pt1 Pt4 119.92(7) . . ?
C8 Pt1 Pt3 143.6(18) . . ?
C5 Pt1 Pt3 80.5(16) . . ?
Pt2 Pt1 Pt3 91.49(7) . . ?
Sn2 Pt1 Pt3 114.21(9) . . ?
Pt5 Pt1 Pt3 121.51(7) . . ?
Pt4 Pt1 Pt3 56.93(6) . . ?
C8 Pt1 Pt2 98.3(18) . 3_675 ?
C5 Pt1 Pt2 126.5(16) . 3_675 ?
Pt2 Pt1 Pt2 63.10(6) . 3_675 ?
Sn2 Pt1 Pt2 123.67(9) . 3_675 ?
Pt5 Pt1 Pt2 63.61(6) . 3_675 ?
Pt4 Pt1 Pt2 87.08(7) . 3_675 ?
Pt3 Pt1 Pt2 57.94(5) . 3_675 ?
C3 Pt2 Pt5 148.7(17) . . ?
C3 Pt2 Pt1 145.6(16) . . ?
Pt5 Pt2 Pt1 60.50(6) . . ?
C3 Pt2 Sn1 92.3(17) . . ?
Pt5 Pt2 Sn1 60.67(8) . . ?
Pt1 Pt2 Sn1 97.90(9) . . ?
C3 Pt2 Pt4 88.8(17) . . ?
Pt5 Pt2 Pt4 120.49(7) . . ?
Pt1 Pt2 Pt4 60.09(6) . . ?
Sn1 Pt2 Pt4 131.51(9) . . ?
C3 Pt2 Sn2 92.5(16) . . ?
Pt5 Pt2 Sn2 94.88(9) . . ?
Pt1 Pt2 Sn2 59.26(8) . . ?
Sn1 Pt2 Sn2 74.82(10) . . ?
Pt4 Pt2 Sn2 56.70(8) . . ?
C3 Pt2 Pt3 92.8(16) . 3_675 ?
Pt5 Pt2 Pt3 59.88(6) . 3_675 ?
Pt1 Pt2 Pt3 120.13(7) . 3_675 ?
Sn1 Pt2 Pt3 56.22(8) . 3_675 ?
Pt4 Pt2 Pt3 172.07(8) . 3_675 ?
Sn2 Pt2 Pt3 130.92(9) . 3_675 ?
C3 Pt2 Pt1 87.4(16) . 3_675 ?
Pt5 Pt2 Pt1 90.38(6) . 3_675 ?
Pt1 Pt2 Pt1 116.90(6) . 3_675 ?
Sn1 Pt2 Pt1 115.20(9) . 3_675 ?
Pt4 Pt2 Pt1 113.28(7) . 3_675 ?
Sn2 Pt2 Pt1 169.97(9) . 3_675 ?
Pt3 Pt2 Pt1 59.08(6) 3_675 3_675 ?
C3 Pt2 Pt2 135.3(16) . 3_675 ?
Pt5 Pt2 Pt2 63.60(6) . 3_675 ?
Pt1 Pt2 Pt2 62.12(6) . 3_675 ?
Sn1 Pt2 Pt2 123.23(10) . 3_675 ?
Pt4 Pt2 Pt2 86.27(7) . 3_675 ?
Sn2 Pt2 Pt2 120.52(10) . 3_675 ?
Pt3 Pt2 Pt2 87.16(7) 3_675 3_675 ?
Pt1 Pt2 Pt2 54.78(6) 3_675 3_675 ?
C3 Pt2 Pt5 86.3(17) . 3_675 ?
Pt5 Pt2 Pt5 117.36(7) . 3_675 ?
Pt1 Pt2 Pt5 88.84(6) . 3_675 ?
Sn1 Pt2 Pt5 169.84(9) . 3_675 ?
Pt4 Pt2 Pt5 58.58(6) . 3_675 ?
Sn2 Pt2 Pt5 115.28(9) . 3_675 ?
Pt3 Pt2 Pt5 113.75(7) 3_675 3_675 ?
Pt1 Pt2 Pt5 54.70(5) 3_675 3_675 ?
Pt2 Pt2 Pt5 53.76(6) 3_675 3_675 ?
C7 Pt3 C4 102(2) . . ?
C7 Pt3 Sn1 91.8(19) . 3_675 ?
C4 Pt3 Sn1 135.6(18) . 3_675 ?
C7 Pt3 Pt4 142.1(18) . . ?
C4 Pt3 Pt4 45.2(15) . . ?
Sn1 Pt3 Pt4 124.66(10) 3_675 . ?
C7 Pt3 Pt5 152(2) . 3_675 ?
C4 Pt3 Pt5 92.6(16) . 3_675 ?
Sn1 Pt3 Pt5 61.76(9) 3_675 3_675 ?
Pt4 Pt3 Pt5 62.95(6) . 3_675 ?
C7 Pt3 Pt2 117.9(17) . 3_675 ?
C4 Pt3 Pt2 137.0(15) . 3_675 ?
Sn1 Pt3 Pt2 61.06(8) 3_675 3_675 ?
Pt4 Pt3 Pt2 91.75(7) . 3_675 ?
Pt5 Pt3 Pt2 58.18(6) 3_675 3_675 ?
C7 Pt3 Pt1 111(2) . . ?
C4 Pt3 Pt1 89.9(17) . . ?
Sn1 Pt3 Pt1 123.92(9) 3_675 . ?
Pt4 Pt3 Pt1 59.83(6) . . ?
Pt5 Pt3 Pt1 91.74(7) 3_675 . ?
Pt2 Pt3 Pt1 62.98(6) 3_675 . ?
C4 Pt4 C6 101(2) . . ?
C4 Pt4 Sn2 131(2) . . ?
C6 Pt4 Sn2 92.2(17) . . ?
C4 Pt4 Pt3 49.1(13) . . ?
C6 Pt4 Pt3 142.6(17) . . ?
Sn2 Pt4 Pt3 123.63(10) . . ?
C4 Pt4 Pt1 95.3(16) . . ?
C6 Pt4 Pt1 152.6(18) . . ?
Sn2 Pt4 Pt1 60.76(8) . . ?
Pt3 Pt4 Pt1 63.24(6) . . ?
C4 Pt4 Pt2 143.4(13) . . ?
C6 Pt4 Pt2 113.8(19) . . ?
Sn2 Pt4 Pt2 62.05(8) . . ?
Pt3 Pt4 Pt2 94.44(7) . . ?
Pt1 Pt4 Pt2 59.22(6) . . ?
C4 Pt4 Pt5 93.0(18) . 3_675 ?
C6 Pt4 Pt5 109(2) . 3_675 ?
Sn2 Pt4 Pt5 126.91(9) . 3_675 ?
Pt3 Pt4 Pt5 59.99(6) . 3_675 ?
Pt1 Pt4 Pt5 91.99(7) . 3_675 ?
Pt2 Pt4 Pt5 64.86(6) . 3_675 ?
C2 Pt5 C8 94(3) . . ?
C2 Pt5 Pt2 160(2) . . ?
C8 Pt5 Pt2 99.4(18) . . ?
C2 Pt5 Pt1 136(2) . . ?
C8 Pt5 Pt1 42.9(15) . . ?
Pt2 Pt5 Pt1 60.18(6) . . ?
C2 Pt5 Pt3 101(2) . 3_675 ?
C8 Pt5 Pt3 157.9(19) . 3_675 ?
Pt2 Pt5 Pt3 61.94(6) . 3_675 ?
Pt1 Pt5 Pt3 121.87(8) . 3_675 ?
C2 Pt5 Sn1 101(2) . . ?
C8 Pt5 Sn1 104.8(17) . . ?
Pt2 Pt5 Sn1 60.76(8) . . ?
Pt1 Pt5 Sn1 97.75(9) . . ?
Pt3 Pt5 Sn1 56.87(8) 3_675 . ?
C2 Pt5 Pt4 89(2) . 3_675 ?
C8 Pt5 Pt4 139.9(16) . 3_675 ?
Pt2 Pt5 Pt4 90.50(7) . 3_675 ?
Pt1 Pt5 Pt4 118.26(8) . 3_675 ?
Pt3 Pt5 Pt4 57.06(6) 3_675 3_675 ?
Sn1 Pt5 Pt4 113.89(9) . 3_675 ?
C2 Pt5 Pt2 132(2) . 3_675 ?
C8 Pt5 Pt2 93.9(13) . 3_675 ?
Pt2 Pt5 Pt2 62.64(7) . 3_675 ?
Pt1 Pt5 Pt2 61.69(6) . 3_675 ?
Pt3 Pt5 Pt2 87.68(7) 3_675 3_675 ?
Sn1 Pt5 Pt2 122.37(9) . 3_675 ?
Pt4 Pt5 Pt2 56.57(5) 3_675 3_675 ?
O1 Sn1 Cl1 93.8(9) . . ?
O1 Sn1 Cl2 94.0(10) . . ?
Cl1 Sn1 Cl2 95.8(6) . . ?
O1 Sn1 Pt3 147.4(9) . 3_675 ?
Cl1 Sn1 Pt3 110.3(4) . 3_675 ?
Cl2 Sn1 Pt3 104.7(4) . 3_675 ?
O1 Sn1 Pt5 93.7(9) . . ?
Cl1 Sn1 Pt5 100.3(5) . . ?
Cl2 Sn1 Pt5 161.7(4) . . ?
Pt3 Sn1 Pt5 61.36(8) 3_675 . ?
O1 Sn1 Pt2 86.9(8) . . ?
Cl1 Sn1 Pt2 158.8(5) . . ?
Cl2 Sn1 Pt2 105.3(4) . . ?
Pt3 Sn1 Pt2 62.71(8) 3_675 . ?
Pt5 Sn1 Pt2 58.57(7) . . ?
O1 Sn2 Cl4 96.3(8) . . ?
O1 Sn2 Cl3 92.3(10) . . ?
Cl4 Sn2 Cl3 94.6(5) . . ?
O1 Sn2 Pt4 145.3(8) . . ?
Cl4 Sn2 Pt4 112.4(4) . . ?
Cl3 Sn2 Pt4 103.9(4) . . ?
O1 Sn2 Pt1 96.6(9) . . ?
Cl4 Sn2 Pt1 97.8(3) . . ?
Cl3 Sn2 Pt1 163.8(4) . . ?
Pt4 Sn2 Pt1 61.66(8) . . ?
O1 Sn2 Pt2 84.6(8) . . ?
Cl4 Sn2 Pt2 156.8(3) . . ?
Cl3 Sn2 Pt2 108.5(4) . . ?
Pt4 Sn2 Pt2 61.25(8) . . ?
Pt1 Sn2 Pt2 59.24(7) . . ?
Sn1 O1 Sn2 112.0(13) . . ?
Sn1 O1 H1 124.0 . . ?
Sn2 O1 H1 124.0 . . ?
O2 C2 Pt5 173(6) . . ?
O3 C3 Pt2 175(5) . . ?
O4 C4 Pt4 142(4) . . ?
O4 C4 Pt3 132(4) . . ?
Pt4 C4 Pt3 85.7(17) . . ?
O5 C5 Pt1 176(5) . . ?
O6 C6 Pt4 171(6) . . ?
O7 C7 Pt3 173(6) . . ?
O8 C8 Pt1 138(5) . . ?
O8 C8 Pt5 131(4) . . ?
Pt1 C8 Pt5 91(2) . . ?
C113 P1 C119 107.0(16) . . ?
C113 P1 C107 111.4(16) . . ?
C119 P1 C107 108.6(16) . . ?
C113 P1 C101 111.1(18) . . ?
C119 P1 C101 112.4(17) . . ?
C107 P1 C101 106.3(18) . . ?
C102 C101 C106 120.0 . . ?
C102 C101 P1 125(2) . . ?
C106 C101 P1 115(2) . . ?
C101 C102 C103 120.0 . . ?
C101 C102 H102 120.0 . . ?
C103 C102 H102 120.0 . . ?
C102 C103 C104 120.0 . . ?
C102 C103 H103 120.0 . . ?
C104 C103 H103 120.0 . . ?
C105 C104 C103 120.0 . . ?
C105 C104 H104 120.0 . . ?
C103 C104 H104 120.0 . . ?
C104 C105 C106 120.0 . . ?
C104 C105 H105 120.0 . . ?
C106 C105 H105 120.0 . . ?
C105 C106 C101 120.0 . . ?
C105 C106 H106 120.0 . . ?
C101 C106 H106 120.0 . . ?
C108 C107 C112 120.0 . . ?
C108 C107 P1 116.2(18) . . ?
C112 C107 P1 123.8(18) . . ?
C107 C108 C109 120.0 . . ?
C107 C108 H108 120.0 . . ?
C109 C108 H108 120.0 . . ?
C108 C109 C110 120.0 . . ?
C108 C109 H109 120.0 . . ?
C110 C109 H109 120.0 . . ?
C111 C110 C109 120.0 . . ?
C111 C110 H110 120.0 . . ?
C109 C110 H110 120.0 . . ?
C110 C111 C112 120.0 . . ?
C110 C111 H111 120.0 . . ?
C112 C111 H111 120.0 . . ?
C111 C112 C107 120.0 . . ?
C111 C112 H112 120.0 . . ?
C107 C112 H112 120.0 . . ?
C114 C113 C118 120.0 . . ?
C114 C113 P1 117(2) . . ?
C118 C113 P1 123(2) . . ?
C113 C114 C115 120.0 . . ?
C113 C114 H114 120.0 . . ?
C115 C114 H114 120.0 . . ?
C116 C115 C114 120.0 . . ?
C116 C115 H115 120.0 . . ?
C114 C115 H115 120.0 . . ?
C115 C116 C117 120.0 . . ?
C115 C116 H116 120.0 . . ?
C117 C116 H116 120.0 . . ?
C118 C117 C116 120.0 . . ?
C118 C117 H117 120.0 . . ?
C116 C117 H117 120.0 . . ?
C117 C118 C113 120.0 . . ?
C117 C118 H118 120.0 . . ?
C113 C118 H118 120.0 . . ?
C120 C119 C124 120.0 . . ?
C120 C119 P1 122.2(17) . . ?
C124 C119 P1 117.8(17) . . ?
C121 C120 C119 120.0 . . ?
C121 C120 H120 120.0 . . ?
C119 C120 H120 120.0 . . ?
C120 C121 C122 120.0 . . ?
C120 C121 H121 120.0 . . ?
C122 C121 H121 120.0 . . ?
C121 C122 C123 120.0 . . ?
C121 C122 H122 120.0 . . ?
C123 C122 H122 120.0 . . ?
C124 C123 C122 120.0 . . ?
C124 C123 H123 120.0 . . ?
C122 C123 H123 120.0 . . ?
C123 C124 C119 120.0 . . ?
C123 C124 H124 120.0 . . ?
C119 C124 H124 120.0 . . ?
C204 O200 C201 109(5) . . ?
O200 C201 C202 107(5) . . ?
O200 C201 H20A 110.2 . . ?
C202 C201 H20A 110.2 . . ?
O200 C201 H20B 110.2 . . ?
C202 C201 H20B 110.2 . . ?
H20A C201 H20B 108.5 . . ?
C203 C202 C201 103(6) . . ?
C203 C202 H20C 111.2 . . ?
C201 C202 H20C 111.2 . . ?
C203 C202 H20D 111.2 . . ?
C201 C202 H20D 111.2 . . ?
H20C C202 H20D 109.1 . . ?
C202 C203 C204 104(6) . . ?
C202 C203 H20E 110.9 . . ?
C204 C203 H20E 110.9 . . ?
C202 C203 H20F 110.9 . . ?
C204 C203 H20F 110.9 . . ?
H20E C203 H20F 108.9 . . ?
O200 C204 C203 109(5) . . ?
O200 C204 H20G 109.9 . . ?
C203 C204 H20G 109.9 . . ?
O200 C204 H20H 109.9 . . ?
C203 C204 H20H 109.9 . . ?
H20G C204 H20H 108.3 . . ?

_diffrn_measured_fraction_theta_max 0.985
_diffrn_reflns_theta_full        23.53
_diffrn_measured_fraction_theta_full 0.985
_refine_diff_density_max         7.174
_refine_diff_density_min         -4.743
_refine_diff_density_rms         0.586
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_PtSn6
_database_code_depnum_ccdc_archive 'CCDC 1439442'
_audit_update_record             
;
2015-12-25 deposited with the CCDC.
2016-01-04 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C54 H52 Cl14 O2 P2 Pt Sn5'
_chemical_formula_weight         2079.74

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   C2/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   20.3822(7)
_cell_length_b                   14.5461(5)
_cell_length_c                   26.2602(11)
_cell_angle_alpha                90.00
_cell_angle_beta                 112.334(2)
_cell_angle_gamma                90.00
_cell_volume                     7201.6(5)
_cell_formula_units_Z            4
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    7759
_cell_measurement_theta_min      2.1605
_cell_measurement_theta_max      22.1465

_exptl_crystal_description       needle
_exptl_crystal_colour            orange
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.11
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.918
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3952
_exptl_absorpt_coefficient_mu    4.242
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.5686
_exptl_absorpt_correction_T_max  0.6526
_exptl_absorpt_process_details   
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1391 (selected reflections only, before parameter refinement)
 R(int) = 0.0599 (selected reflections only, after parameter refinement)
;

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            56014
_diffrn_reflns_av_R_equivalents  0.0759
_diffrn_reflns_av_unetI/netI     0.0434
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_theta_min         1.68
_diffrn_reflns_theta_max         26.00
_reflns_number_total             7084
_reflns_number_gt                5160
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. The following restraints
 were applied (given as SHELXL lines): 
 simu .01 c121 c122 c123
 simu .01 o1 > c3
 isor .01 o1 c1 c2 c3 c105 c106 c115 c116 c117 c121 c122 c123 c124
 AFIX 66 on all Ph rings
 The asymmetric unit of the unit cell contains half of a cluster anion 
 (on 2) and one [PPh4]+ cation (on a general position). Some C-atoms have 
 been restrained to isotropic behaviour (ISOR command in SHELXL, s.u. 0.01). 
 The C-atoms of the Ph-rings have been constrained to fit regular hexagons 
 (AFIX 66 command in SHELXL). Similar U restraints have been applied to 
 the acetone molecules (SIMU command in SHELXL, s.u. 0.01).
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0374P)²+65.7748P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         7084
_refine_ls_number_parameters     305
_refine_ls_number_restraints     108
_refine_ls_R_factor_all          0.0741
_refine_ls_R_factor_gt           0.0472
_refine_ls_wR_factor_ref         0.1129
_refine_ls_wR_factor_gt          0.1013
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_restrained_S_all      1.095
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.0000 0.75728(3) 0.7500 0.03763(12) Uani 1 2 d S . .
Sn1 Sn 0.05013(3) 0.75200(5) 0.85534(2) 0.05525(18) Uani 1 1 d . . .
Sn2 Sn 0.10479(3) 0.85369(4) 0.74879(3) 0.05148(17) Uani 1 1 d . . .
Sn3 Sn 0.0000 0.58043(6) 0.7500 0.0528(2) Uani 1 2 d S . .
Cl1 Cl -0.02136(15) 0.6709(2) 0.89263(11) 0.0914(9) Uani 1 1 d . . .
Cl2 Cl 0.15926(14) 0.6811(2) 0.90458(12) 0.0889(9) Uani 1 1 d . . .
Cl3 Cl 0.06475(19) 0.8849(2) 0.90870(11) 0.0973(10) Uani 1 1 d . . .
Cl4 Cl 0.18842(15) 0.9096(2) 0.83379(12) 0.0984(10) Uani 1 1 d . . .
Cl5 Cl 0.18849(19) 0.8000(3) 0.7135(2) 0.1317(16) Uani 1 1 d . . .
Cl6 Cl 0.08189(15) 0.99793(18) 0.70313(11) 0.0753(7) Uani 1 1 d . . .
Cl7 Cl 0.0424(2) 0.4765(2) 0.82336(14) 0.1094(11) Uani 1 1 d . . .
O1 O 0.1151(4) 0.5695(6) 0.7520(4) 0.103(2) Uani 1 1 d U . .
C1 C 0.1581(7) 0.5364(10) 0.7382(6) 0.104(3) Uani 1 1 d U . .
C2 C 0.1395(10) 0.4664(14) 0.6970(8) 0.182(7) Uani 1 1 d U . .
H2A H 0.0897 0.4538 0.6847 0.273 Uiso 1 1 calc R . .
H2B H 0.1658 0.4115 0.7122 0.273 Uiso 1 1 calc R . .
H2C H 0.1506 0.4869 0.6665 0.273 Uiso 1 1 calc R . .
C3 C 0.2330(10) 0.5592(13) 0.7614(8) 0.172(6) Uani 1 1 d U . .
H3A H 0.2407 0.6091 0.7869 0.257 Uiso 1 1 calc R . .
H3B H 0.2482 0.5769 0.7324 0.257 Uiso 1 1 calc R . .
H3C H 0.2596 0.5065 0.7803 0.257 Uiso 1 1 calc R . .
P1 P 0.92266(13) 0.76873(16) 0.04455(9) 0.0501(5) Uani 1 1 d . . .
C101 C 1.0180(3) 0.7649(5) 0.0706(3) 0.054(2) Uani 1 1 d G . .
C102 C 1.0512(4) 0.7562(5) 0.0334(2) 0.089(4) Uani 1 1 d G . .
H102 H 1.0243 0.7541 -0.0042 0.106 Uiso 1 1 calc R . .
C103 C 1.1247(4) 0.7508(6) 0.0524(3) 0.094(4) Uani 1 1 d G . .
H103 H 1.1470 0.7450 0.0276 0.113 Uiso 1 1 calc R . .
C104 C 1.1650(3) 0.7539(5) 0.1086(4) 0.088(4) Uani 1 1 d G . .
H104 H 1.2142 0.7503 0.1213 0.105 Uiso 1 1 calc R . .
C105 C 1.1317(4) 0.7626(6) 0.1458(2) 0.101(4) Uani 1 1 d GU . .
H105 H 1.1586 0.7648 0.1834 0.122 Uiso 1 1 calc R . .
C106 C 1.0582(4) 0.7681(5) 0.1268(2) 0.089(3) Uani 1 1 d GU . .
H106 H 1.0359 0.7739 0.1516 0.106 Uiso 1 1 calc R . .
C107 C 0.8911(3) 0.6663(4) 0.0056(2) 0.053(2) Uani 1 1 d G . .
C108 C 0.8322(3) 0.6683(4) -0.0436(2) 0.070(3) Uani 1 1 d G . .
H108 H 0.8104 0.7240 -0.0576 0.085 Uiso 1 1 calc R . .
C109 C 0.8057(3) 0.5870(5) -0.0718(2) 0.087(4) Uani 1 1 d G . .
H109 H 0.7663 0.5884 -0.1046 0.104 Uiso 1 1 calc R . .
C110 C 0.8383(4) 0.5038(4) -0.0508(3) 0.095(4) Uani 1 1 d G . .
H110 H 0.8206 0.4494 -0.0696 0.114 Uiso 1 1 calc R . .
C111 C 0.8972(4) 0.5018(3) -0.0016(3) 0.086(3) Uani 1 1 d G . .
H111 H 0.9190 0.4461 0.0124 0.103 Uiso 1 1 calc R . .
C112 C 0.9237(3) 0.5831(4) 0.0265(2) 0.074(3) Uani 1 1 d G . .
H112 H 0.9631 0.5818 0.0594 0.088 Uiso 1 1 calc R . .
C113 C 0.8937(3) 0.7731(4) 0.1005(2) 0.056(2) Uani 1 1 d G . .
C114 C 0.8510(3) 0.7040(4) 0.1079(3) 0.065(3) Uani 1 1 d G . .
H114 H 0.8375 0.6547 0.0836 0.078 Uiso 1 1 calc R . .
C115 C 0.8284(4) 0.7088(5) 0.1515(3) 0.095(4) Uani 1 1 d GU . .
H115 H 0.7998 0.6626 0.1564 0.114 Uiso 1 1 calc R . .
C116 C 0.8485(4) 0.7826(6) 0.1878(3) 0.099(4) Uani 1 1 d GU . .
H116 H 0.8333 0.7858 0.2170 0.119 Uiso 1 1 calc R . .
C117 C 0.8912(4) 0.8516(5) 0.1805(3) 0.111(4) Uani 1 1 d GU . .
H117 H 0.9046 0.9010 0.2048 0.134 Uiso 1 1 calc R . .
C118 C 0.9138(4) 0.8469(4) 0.1368(3) 0.088(4) Uani 1 1 d G . .
H118 H 0.9424 0.8931 0.1319 0.106 Uiso 1 1 calc R . .
C119 C 0.8868(4) 0.8671(5) 0.0025(3) 0.067(3) Uani 1 1 d G . .
C120 C 0.8263(4) 0.9082(5) 0.0045(3) 0.088(3) Uani 1 1 d G . .
H120 H 0.8075 0.8877 0.0297 0.105 Uiso 1 1 calc R . .
C121 C 0.7939(4) 0.9800(6) -0.0311(4) 0.106(4) Uani 1 1 d GU . .
H121 H 0.7534 1.0076 -0.0297 0.127 Uiso 1 1 calc R . .
C122 C 0.8219(5) 1.0107(5) -0.0687(3) 0.123(4) Uani 1 1 d GU . .
H122 H 0.8002 1.0588 -0.0925 0.147 Uiso 1 1 calc R . .
C123 C 0.8824(5) 0.9696(7) -0.0708(3) 0.134(4) Uani 1 1 d GU . .
H123 H 0.9012 0.9901 -0.0959 0.161 Uiso 1 1 calc R . .
C124 C 0.9149(4) 0.8977(6) -0.0352(4) 0.124(5) Uani 1 1 d GU . .
H124 H 0.9553 0.8702 -0.0365 0.149 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 Sn1 2.5600(6) 2_556 ?
Pt1 Sn1 2.5600(6) . ?
Pt1 Sn2 2.5654(6) . ?
Pt1 Sn2 2.5654(6) 2_556 ?
Pt1 Sn3 2.5724(10) . ?
Sn1 Cl3 2.339(3) . ?
Sn1 Cl2 2.344(3) . ?
Sn1 Cl1 2.357(3) . ?
Sn2 Cl5 2.362(3) . ?
Sn2 Cl6 2.373(3) . ?
Sn2 Cl4 2.378(3) . ?
Sn3 O1 2.332(8) . ?
Sn3 O1 2.332(8) 2_556 ?
Sn3 Cl7 2.341(3) 2_556 ?
Sn3 Cl7 2.341(3) . ?
O1 C1 1.172(13) . ?
C1 C2 1.43(2) . ?
C1 C3 1.45(2) . ?
C2 H2A 0.9600 . ?
C2 H2B 0.9600 . ?
C2 H2C 0.9600 . ?
C3 H3A 0.9600 . ?
C3 H3B 0.9600 . ?
C3 H3C 0.9600 . ?
P1 C113 1.782(5) . ?
P1 C107 1.783(5) . ?
P1 C119 1.786(6) . ?
P1 C101 1.798(5) . ?
C101 C102 1.3900 . ?
C101 C106 1.3900 . ?
C102 C103 1.3900 . ?
C102 H102 0.9300 . ?
C103 C104 1.3900 . ?
C103 H103 0.9300 . ?
C104 C105 1.3900 . ?
C104 H104 0.9300 . ?
C105 C106 1.3900 . ?
C105 H105 0.9300 . ?
C106 H106 0.9300 . ?
C107 C108 1.3900 . ?
C107 C112 1.3900 . ?
C108 C109 1.3900 . ?
C108 H108 0.9300 . ?
C109 C110 1.3900 . ?
C109 H109 0.9300 . ?
C110 C111 1.3900 . ?
C110 H110 0.9300 . ?
C111 C112 1.3900 . ?
C111 H111 0.9300 . ?
C112 H112 0.9300 . ?
C113 C114 1.3900 . ?
C113 C118 1.3900 . ?
C114 C115 1.3900 . ?
C114 H114 0.9300 . ?
C115 C116 1.3900 . ?
C115 H115 0.9300 . ?
C116 C117 1.3900 . ?
C116 H116 0.9300 . ?
C117 C118 1.3900 . ?
C117 H117 0.9300 . ?
C118 H118 0.9300 . ?
C119 C120 1.3900 . ?
C119 C124 1.3900 . ?
C120 C121 1.3900 . ?
C120 H120 0.9300 . ?
C121 C122 1.3900 . ?
C121 H121 0.9300 . ?
C122 C123 1.3900 . ?
C122 H122 0.9300 . ?
C123 C124 1.3900 . ?
C123 H123 0.9300 . ?
C124 H124 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Sn1 Pt1 Sn1 176.57(4) 2_556 . ?
Sn1 Pt1 Sn2 89.73(2) 2_556 . ?
Sn1 Pt1 Sn2 92.14(2) . . ?
Sn1 Pt1 Sn2 92.14(2) 2_556 2_556 ?
Sn1 Pt1 Sn2 89.73(2) . 2_556 ?
Sn2 Pt1 Sn2 113.72(3) . 2_556 ?
Sn1 Pt1 Sn3 88.283(18) 2_556 . ?
Sn1 Pt1 Sn3 88.283(18) . . ?
Sn2 Pt1 Sn3 123.139(16) . . ?
Sn2 Pt1 Sn3 123.139(16) 2_556 . ?
Cl3 Sn1 Cl2 98.90(12) . . ?
Cl3 Sn1 Cl1 97.04(12) . . ?
Cl2 Sn1 Cl1 99.07(11) . . ?
Cl3 Sn1 Pt1 122.03(8) . . ?
Cl2 Sn1 Pt1 120.97(8) . . ?
Cl1 Sn1 Pt1 114.07(7) . . ?
Cl5 Sn2 Cl6 97.27(13) . . ?
Cl5 Sn2 Cl4 96.56(14) . . ?
Cl6 Sn2 Cl4 96.04(10) . . ?
Cl5 Sn2 Pt1 123.57(10) . . ?
Cl6 Sn2 Pt1 118.99(7) . . ?
Cl4 Sn2 Pt1 118.58(8) . . ?
O1 Sn3 O1 172.2(4) . 2_556 ?
O1 Sn3 Cl7 91.7(2) . 2_556 ?
O1 Sn3 Cl7 83.3(2) 2_556 2_556 ?
O1 Sn3 Cl7 83.3(2) . . ?
O1 Sn3 Cl7 91.7(2) 2_556 . ?
Cl7 Sn3 Cl7 99.5(2) 2_556 . ?
O1 Sn3 Pt1 93.9(2) . . ?
O1 Sn3 Pt1 93.9(2) 2_556 . ?
Cl7 Sn3 Pt1 130.25(10) 2_556 . ?
Cl7 Sn3 Pt1 130.25(10) . . ?
C1 O1 Sn3 152.3(10) . . ?
O1 C1 C2 120.9(15) . . ?
O1 C1 C3 124.6(16) . . ?
C2 C1 C3 114.5(14) . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C1 C3 H3A 109.5 . . ?
C1 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C1 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C113 P1 C107 110.1(3) . . ?
C113 P1 C119 107.2(3) . . ?
C107 P1 C119 109.9(3) . . ?
C113 P1 C101 109.7(3) . . ?
C107 P1 C101 107.1(3) . . ?
C119 P1 C101 112.9(4) . . ?
C102 C101 C106 120.0 . . ?
C102 C101 P1 118.7(4) . . ?
C106 C101 P1 121.3(4) . . ?
C103 C102 C101 120.0 . . ?
C103 C102 H102 120.0 . . ?
C101 C102 H102 120.0 . . ?
C102 C103 C104 120.0 . . ?
C102 C103 H103 120.0 . . ?
C104 C103 H103 120.0 . . ?
C103 C104 C105 120.0 . . ?
C103 C104 H104 120.0 . . ?
C105 C104 H104 120.0 . . ?
C106 C105 C104 120.0 . . ?
C106 C105 H105 120.0 . . ?
C104 C105 H105 120.0 . . ?
C105 C106 C101 120.0 . . ?
C105 C106 H106 120.0 . . ?
C101 C106 H106 120.0 . . ?
C108 C107 C112 120.0 . . ?
C108 C107 P1 120.8(4) . . ?
C112 C107 P1 119.1(4) . . ?
C107 C108 C109 120.0 . . ?
C107 C108 H108 120.0 . . ?
C109 C108 H108 120.0 . . ?
C108 C109 C110 120.0 . . ?
C108 C109 H109 120.0 . . ?
C110 C109 H109 120.0 . . ?
C109 C110 C111 120.0 . . ?
C109 C110 H110 120.0 . . ?
C111 C110 H110 120.0 . . ?
C112 C111 C110 120.0 . . ?
C112 C111 H111 120.0 . . ?
C110 C111 H111 120.0 . . ?
C111 C112 C107 120.0 . . ?
C111 C112 H112 120.0 . . ?
C107 C112 H112 120.0 . . ?
C114 C113 C118 120.0 . . ?
C114 C113 P1 120.7(4) . . ?
C118 C113 P1 119.3(4) . . ?
C113 C114 C115 120.0 . . ?
C113 C114 H114 120.0 . . ?
C115 C114 H114 120.0 . . ?
C114 C115 C116 120.0 . . ?
C114 C115 H115 120.0 . . ?
C116 C115 H115 120.0 . . ?
C115 C116 C117 120.0 . . ?
C115 C116 H116 120.0 . . ?
C117 C116 H116 120.0 . . ?
C118 C117 C116 120.0 . . ?
C118 C117 H117 120.0 . . ?
C116 C117 H117 120.0 . . ?
C117 C118 C113 120.0 . . ?
C117 C118 H118 120.0 . . ?
C113 C118 H118 120.0 . . ?
C120 C119 C124 120.0 . . ?
C120 C119 P1 118.8(5) . . ?
C124 C119 P1 121.0(5) . . ?
C121 C120 C119 120.0 . . ?
C121 C120 H120 120.0 . . ?
C119 C120 H120 120.0 . . ?
C122 C121 C120 120.0 . . ?
C122 C121 H121 120.0 . . ?
C120 C121 H121 120.0 . . ?
C123 C122 C121 120.0 . . ?
C123 C122 H122 120.0 . . ?
C121 C122 H122 120.0 . . ?
C122 C123 C124 120.0 . . ?
C122 C123 H123 120.0 . . ?
C124 C123 H123 120.0 . . ?
C123 C124 C119 120.0 . . ?
C123 C124 H124 120.0 . . ?
C119 C124 H124 120.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Sn1 Pt1 Sn1 Cl3 -173.64(11) 2_556 . . . ?
Sn2 Pt1 Sn1 Cl3 63.26(11) . . . . ?
Sn2 Pt1 Sn1 Cl3 -50.47(11) 2_556 . . . ?
Sn3 Pt1 Sn1 Cl3 -173.64(11) . . . . ?
Sn1 Pt1 Sn1 Cl2 60.33(10) 2_556 . . . ?
Sn2 Pt1 Sn1 Cl2 -62.78(10) . . . . ?
Sn2 Pt1 Sn1 Cl2 -176.51(10) 2_556 . . . ?
Sn3 Pt1 Sn1 Cl2 60.33(10) . . . . ?
Sn1 Pt1 Sn1 Cl1 -57.68(10) 2_556 . . . ?
Sn2 Pt1 Sn1 Cl1 179.21(10) . . . . ?
Sn2 Pt1 Sn1 Cl1 65.49(10) 2_556 . . . ?
Sn3 Pt1 Sn1 Cl1 -57.68(10) . . . . ?
Sn1 Pt1 Sn2 Cl5 -62.86(15) 2_556 . . . ?
Sn1 Pt1 Sn2 Cl5 114.27(15) . . . . ?
Sn2 Pt1 Sn2 Cl5 -155.08(15) 2_556 . . . ?
Sn3 Pt1 Sn2 Cl5 24.92(15) . . . . ?
Sn1 Pt1 Sn2 Cl6 59.93(8) 2_556 . . . ?
Sn1 Pt1 Sn2 Cl6 -122.95(8) . . . . ?
Sn2 Pt1 Sn2 Cl6 -32.30(8) 2_556 . . . ?
Sn3 Pt1 Sn2 Cl6 147.70(8) . . . . ?
Sn1 Pt1 Sn2 Cl4 175.95(10) 2_556 . . . ?
Sn1 Pt1 Sn2 Cl4 -6.92(10) . . . . ?
Sn2 Pt1 Sn2 Cl4 83.73(10) 2_556 . . . ?
Sn3 Pt1 Sn2 Cl4 -96.27(10) . . . . ?
Sn1 Pt1 Sn3 O1 90.6(2) 2_556 . . . ?
Sn1 Pt1 Sn3 O1 -89.4(2) . . . . ?
Sn2 Pt1 Sn3 O1 2.0(2) . . . . ?
Sn2 Pt1 Sn3 O1 -178.0(2) 2_556 . . . ?
Sn1 Pt1 Sn3 O1 -89.4(2) 2_556 . . 2_556 ?
Sn1 Pt1 Sn3 O1 90.6(2) . . . 2_556 ?
Sn2 Pt1 Sn3 O1 -178.0(2) . . . 2_556 ?
Sn2 Pt1 Sn3 O1 2.0(2) 2_556 . . 2_556 ?
Sn1 Pt1 Sn3 Cl7 -4.93(12) 2_556 . . 2_556 ?
Sn1 Pt1 Sn3 Cl7 175.07(12) . . . 2_556 ?
Sn2 Pt1 Sn3 Cl7 -93.49(12) . . . 2_556 ?
Sn2 Pt1 Sn3 Cl7 86.51(12) 2_556 . . 2_556 ?
Sn1 Pt1 Sn3 Cl7 175.07(12) 2_556 . . . ?
Sn1 Pt1 Sn3 Cl7 -4.93(12) . . . . ?
Sn2 Pt1 Sn3 Cl7 86.51(12) . . . . ?
Sn2 Pt1 Sn3 Cl7 -93.49(12) 2_556 . . . ?
O1 Sn3 O1 C1 41(2) 2_556 . . . ?
Cl7 Sn3 O1 C1 -9(2) 2_556 . . . ?
Cl7 Sn3 O1 C1 91(2) . . . . ?
Pt1 Sn3 O1 C1 -139(2) . . . . ?
Sn3 O1 C1 C2 4(3) . . . . ?
Sn3 O1 C1 C3 -173.8(14) . . . . ?
C113 P1 C101 C102 176.6(4) . . . . ?
C107 P1 C101 C102 57.1(5) . . . . ?
C119 P1 C101 C102 -63.9(5) . . . . ?
C113 P1 C101 C106 -1.8(5) . . . . ?
C107 P1 C101 C106 -121.2(4) . . . . ?
C119 P1 C101 C106 117.7(5) . . . . ?
C106 C101 C102 C103 0.0 . . . . ?
P1 C101 C102 C103 -178.4(5) . . . . ?
C101 C102 C103 C104 0.0 . . . . ?
C102 C103 C104 C105 0.0 . . . . ?
C103 C104 C105 C106 0.0 . . . . ?
C104 C105 C106 C101 0.0 . . . . ?
C102 C101 C106 C105 0.0 . . . . ?
P1 C101 C106 C105 178.3(5) . . . . ?
C113 P1 C107 C108 100.6(4) . . . . ?
C119 P1 C107 C108 -17.3(5) . . . . ?
C101 P1 C107 C108 -140.2(4) . . . . ?
C113 P1 C107 C112 -75.5(4) . . . . ?
C119 P1 C107 C112 166.6(4) . . . . ?
C101 P1 C107 C112 43.6(5) . . . . ?
C112 C107 C108 C109 0.0 . . . . ?
P1 C107 C108 C109 -176.1(5) . . . . ?
C107 C108 C109 C110 0.0 . . . . ?
C108 C109 C110 C111 0.0 . . . . ?
C109 C110 C111 C112 0.0 . . . . ?
C110 C111 C112 C107 0.0 . . . . ?
C108 C107 C112 C111 0.0 . . . . ?
P1 C107 C112 C111 176.2(5) . . . . ?
C107 P1 C113 C114 -1.7(5) . . . . ?
C119 P1 C113 C114 117.8(5) . . . . ?
C101 P1 C113 C114 -119.3(4) . . . . ?
C107 P1 C113 C118 178.8(4) . . . . ?
C119 P1 C113 C118 -61.7(5) . . . . ?
C101 P1 C113 C118 61.2(5) . . . . ?
C118 C113 C114 C115 0.0 . . . . ?
P1 C113 C114 C115 -179.5(5) . . . . ?
C113 C114 C115 C116 0.0 . . . . ?
C114 C115 C116 C117 0.0 . . . . ?
C115 C116 C117 C118 0.0 . . . . ?
C116 C117 C118 C113 0.0 . . . . ?
C114 C113 C118 C117 0.0 . . . . ?
P1 C113 C118 C117 179.5(5) . . . . ?
C113 P1 C119 C120 -23.6(6) . . . . ?
C107 P1 C119 C120 96.0(5) . . . . ?
C101 P1 C119 C120 -144.5(5) . . . . ?
C113 P1 C119 C124 161.8(5) . . . . ?
C107 P1 C119 C124 -78.6(5) . . . . ?
C101 P1 C119 C124 40.9(6) . . . . ?
C124 C119 C120 C121 0.0 . . . . ?
P1 C119 C120 C121 -174.7(6) . . . . ?
C119 C120 C121 C122 0.0 . . . . ?
C120 C121 C122 C123 0.0 . . . . ?
C121 C122 C123 C124 0.0 . . . . ?
C122 C123 C124 C119 0.0 . . . . ?
C120 C119 C124 C123 0.0 . . . . ?
P1 C119 C124 C123 174.6(6) . . . . ?

_diffrn_measured_fraction_theta_max 0.999
_diffrn_reflns_theta_full        26.00
_diffrn_measured_fraction_theta_full 0.999
_refine_diff_density_max         0.988
_refine_diff_density_min         -0.754
_refine_diff_density_rms         0.132

