# Electronic Supplementary Material (ESI) for RSC Advances.
# This journal is © The Royal Society of Chemistry 2015

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
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# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_shelxl
_database_code_depnum_ccdc_archive 'CCDC 1049866'
_audit_update_record             
;
2015-02-16 deposited with the CCDC.
2015-06-16 downloaded from the CCDC.
;
_audit_creation_date             2015-02-16
_audit_creation_method           
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_shelxl_version_number           2013-4
_chemical_name_common            ?
_chemical_name_systematic        
;
 ?
;
_chemical_formula_moiety         'C44 H32'
_chemical_formula_sum            'C44 H32'
_chemical_formula_weight         560.69
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   21.779(11)
_cell_length_b                   4.904(2)
_cell_length_c                   27.269(12)
_cell_angle_alpha                90
_cell_angle_beta                 97.075(8)
_cell_angle_gamma                90
_cell_volume                     2891(2)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    5409
_cell_measurement_temperature    153(2)
_cell_measurement_theta_max      30.7132
_cell_measurement_theta_min      2.5529
_shelx_estimated_absorpt_T_max   0.997
_shelx_estimated_absorpt_T_min   0.976
_exptl_absorpt_coefficient_mu    0.073
_exptl_absorpt_correction_T_max  0.9975
_exptl_absorpt_correction_T_min  0.9849
_exptl_absorpt_correction_type   Numerical
_exptl_absorpt_process_details   '(T. Higashi, 2000)'
_exptl_crystal_colour            Green
_exptl_crystal_density_diffrn    1.288
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       Platelet
_exptl_crystal_F_000             1184
_exptl_crystal_size_max          0.33
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.04
_exptl_special_details           
;
 ?
;
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0484
_diffrn_reflns_av_unetI/netI     0.0321
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -6
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_number            16217
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.492
_diffrn_reflns_theta_min         2.553
_diffrn_ambient_temperature      153(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_details      
;
scan:
	Number of images: 360
	           Slice: -75.0000 - 105.0000
	     Image width: 0.5000
	        Exp time: 35.0000
	   Rotation axis: Omega
	           Omega: 0.0000
	             Chi: 45.0000
	             Phi: 90.0000
	             XTD: 40.0573
	          2theta: 15.0966
scan:
	Number of images: 360
	           Slice: -75.0000 - 105.0000
	     Image width: 0.5000
	        Exp time: 35.0000
	   Rotation axis: Omega
	           Omega: 0.0000
	             Chi: 0.0000
	             Phi: 0.0000
	             XTD: 40.0573
	          2theta: 15.0966
scan:
	Number of images: 286
	           Slice: -40.0000 - 103.0000
	     Image width: 0.5000
	        Exp time: 35.0000
	   Rotation axis: Omega
	           Omega: 0.0000
	             Chi: 45.0000
	             Phi: 0.0000
	             XTD: 40.0573
	          2theta: 15.0966
;
_diffrn_measurement_device       
;
Saturn70 (2x2 bin mode)
;
_diffrn_measurement_device_details 
;
AFC8: Eulerian 3 circle
;
_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       dtprofit.ref
_diffrn_number_total             4591
_diffrn_orient_matrix_type       d*Trek
_diffrn_orient_matrix_UB_11      0.0364
_diffrn_orient_matrix_UB_12      0.0068
_diffrn_orient_matrix_UB_13      0.0277
_diffrn_orient_matrix_UB_21      -0.1254
_diffrn_orient_matrix_UB_22      0.0520
_diffrn_orient_matrix_UB_23      0.1521
_diffrn_orient_matrix_UB_31      0.0020
_diffrn_orient_matrix_UB_32      -0.0344
_diffrn_orient_matrix_UB_33      0.0134
_diffrn_radiation_detector       CCD
_diffrn_radiation_monochromator  Other
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71075
_diffrn_source                   'Sealed Tube'
_diffrn_source_current           40.0000
_diffrn_source_power             2.0000
_diffrn_source_voltage           50.0000
_diffrn_special_details          
;
 ?
;
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2647
_reflns_number_total             2982
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2008)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL-2014 (Sheldrick, 2008)'
_computing_structure_solution    
;
ShelXS-97 (Sheldrick, 2008)
;
_refine_diff_density_max         0.188
_refine_diff_density_min         -0.191
_refine_diff_density_rms         0.041
_refine_ls_extinction_coef       0.0008(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.179
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     200
_refine_ls_number_reflns         2982
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0751
_refine_ls_R_factor_gt           0.0658
_refine_ls_restrained_S_all      1.179
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0410P)²+3.3521P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1361
_refine_ls_wR_factor_ref         0.1415
_refine_special_details          
;
 ?
;
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 C11(H11A,H11B), C22(H22A,H22B)
2.b Aromatic/amide H refined with riding coordinates:
 C1(H1), C4(H4), C5(H5), C6(H6), C7(H7), C8(H8), C14(H14), C15(H15), C16(H16),
 C17(H17), C18(H18), C21(H21)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.32512(9) 1.1352(4) 0.54095(7) 0.0350(5) Uani 1 1 d . . . . .
H1 H 0.3007 1.2734 0.5255 0.042 Uiso 1 1 calc R . . . .
C2 C 0.37415(9) 1.0107(4) 0.52107(7) 0.0336(5) Uani 1 1 d . . . . .
C3 C 0.40002(9) 0.8161(4) 0.55551(7) 0.0327(4) Uani 1 1 d . . . . .
C4 C 0.44937(9) 0.6447(4) 0.55050(7) 0.0376(5) Uani 1 1 d . . . . .
H4 H 0.4660 0.6600 0.5208 0.045 Uiso 1 1 calc R . . . .
C5 C 0.47767(10) 0.4538(5) 0.58326(8) 0.0421(5) Uani 1 1 d . . . . .
H5 H 0.5105 0.3597 0.5724 0.050 Uiso 1 1 calc R . . . .
C6 C 0.46397(10) 0.3834(5) 0.62987(8) 0.0443(5) Uani 1 1 d . . . . .
H6 H 0.4893 0.2503 0.6460 0.053 Uiso 1 1 calc R . . . .
C7 C 0.41790(10) 0.4823(5) 0.65613(8) 0.0449(5) Uani 1 1 d . . . . .
H7 H 0.4173 0.4100 0.6876 0.054 Uiso 1 1 calc R . . . .
C8 C 0.37257(10) 0.6758(4) 0.64135(7) 0.0370(5) Uani 1 1 d . . . . .
H8 H 0.3444 0.7080 0.6637 0.044 Uiso 1 1 calc R . . . .
C9 C 0.36329(9) 0.8266(4) 0.59839(7) 0.0324(4) Uani 1 1 d . . . . .
C10 C 0.31742(9) 1.0260(4) 0.58688(7) 0.0333(5) Uani 1 1 d . . . . .
C11 C 0.26662(9) 1.0977(4) 0.61738(7) 0.0371(5) Uani 1 1 d . . . . .
H11A H 0.2503 1.2765 0.6078 0.045 Uiso 1 1 calc R . . . .
H11B H 0.2834 1.1052 0.6520 0.045 Uiso 1 1 calc R . . . .
C12 C 0.21510(9) 0.8901(4) 0.61040(7) 0.0332(5) Uani 1 1 d . . . . .
C13 C 0.18345(9) 0.7712(4) 0.64672(7) 0.0341(5) Uani 1 1 d . . . . .
C14 C 0.19272(10) 0.8262(5) 0.69715(7) 0.0404(5) Uani 1 1 d . . . . .
H14 H 0.2233 0.9541 0.7071 0.049 Uiso 1 1 calc R . . . .
C15 C 0.16280(10) 0.7171(5) 0.73452(7) 0.0455(6) Uani 1 1 d . . . . .
H15 H 0.1754 0.7850 0.7660 0.055 Uiso 1 1 calc R . . . .
C16 C 0.11662(11) 0.5205(5) 0.73172(8) 0.0484(6) Uani 1 1 d . . . . .
H16 H 0.1029 0.4754 0.7617 0.058 Uiso 1 1 calc R . . . .
C17 C 0.08803(11) 0.3819(5) 0.69100(8) 0.0460(6) Uani 1 1 d . . . . .
H17 H 0.0586 0.2536 0.6975 0.055 Uiso 1 1 calc R . . . .
C18 C 0.09725(10) 0.4084(5) 0.64153(8) 0.0393(5) Uani 1 1 d . . . . .
H18 H 0.0728 0.2967 0.6195 0.047 Uiso 1 1 calc R . . . .
C19 C 0.13750(9) 0.5769(4) 0.62068(7) 0.0336(5) Uani 1 1 d . . . . .
C20 C 0.14346(9) 0.5929(4) 0.56975(7) 0.0326(4) Uani 1 1 d . . . . .
C21 C 0.19027(9) 0.7802(4) 0.56461(7) 0.0335(5) Uani 1 1 d . . . . .
H21 H 0.2035 0.8268 0.5346 0.040 Uiso 1 1 calc R . . . .
C22 C 0.10720(9) 0.4314(5) 0.52896(7) 0.0379(5) Uani 1 1 d . . . . .
H22A H 0.1128 0.2385 0.5360 0.046 Uiso 1 1 calc R . . . .
H22B H 0.0636 0.4724 0.5285 0.046 Uiso 1 1 calc R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 H1 0.9300 . ?
C1 C2 1.396(3) . ?
C1 C10 1.391(3) . ?
C2 C3 1.407(3) . ?
C2 C22 1.498(3) 7_566 ?
C3 C4 1.384(3) . ?
C3 C9 1.497(3) . ?
C4 H4 0.9300 . ?
C4 C5 1.385(3) . ?
C5 H5 0.9300 . ?
C5 C6 1.385(3) . ?
C6 H6 0.9300 . ?
C6 C7 1.390(3) . ?
C7 H7 0.9300 . ?
C7 C8 1.393(3) . ?
C8 H8 0.9300 . ?
C8 C9 1.379(3) . ?
C9 C10 1.406(3) . ?
C10 C11 1.505(3) . ?
C11 H11A 0.9700 . ?
C11 H11B 0.9700 . ?
C11 C12 1.510(3) . ?
C12 C13 1.401(3) . ?
C12 C21 1.406(3) . ?
C13 C14 1.392(3) . ?
C13 C19 1.496(3) . ?
C14 H14 0.9300 . ?
C14 C15 1.383(3) . ?
C15 H15 0.9300 . ?
C15 C16 1.388(4) . ?
C16 H16 0.9300 . ?
C16 C17 1.383(3) . ?
C17 H17 0.9300 . ?
C17 C18 1.394(3) . ?
C18 H18 0.9300 . ?
C18 C19 1.378(3) . ?
C19 C20 1.413(3) . ?
C20 C21 1.392(3) . ?
C20 C22 1.507(3) . ?
C21 H21 0.9300 . ?
C22 C2 1.498(3) 7_566 ?
C22 H22A 0.9700 . ?
C22 H22B 0.9700 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 H1 124.3 . . ?
C10 C1 H1 124.3 . . ?
C10 C1 C2 111.35(19) . . ?
C1 C2 C3 107.46(17) . . ?
C1 C2 C22 125.23(19) . 7_566 ?
C3 C2 C22 127.25(19) . 7_566 ?
C2 C3 C9 106.82(17) . . ?
C4 C3 C2 126.73(18) . . ?
C4 C3 C9 126.45(19) . . ?
C3 C4 H4 115.3 . . ?
C3 C4 C5 129.5(2) . . ?
C5 C4 H4 115.3 . . ?
C4 C5 H5 115.4 . . ?
C6 C5 C4 129.2(2) . . ?
C6 C5 H5 115.4 . . ?
C5 C6 H6 115.2 . . ?
C5 C6 C7 129.6(2) . . ?
C7 C6 H6 115.2 . . ?
C6 C7 H7 115.9 . . ?
C6 C7 C8 128.3(2) . . ?
C8 C7 H7 115.9 . . ?
C7 C8 H8 115.3 . . ?
C9 C8 C7 129.5(2) . . ?
C9 C8 H8 115.3 . . ?
C8 C9 C3 127.49(19) . . ?
C8 C9 C10 126.05(18) . . ?
C10 C9 C3 106.45(17) . . ?
C1 C10 C9 107.91(17) . . ?
C1 C10 C11 125.86(19) . . ?
C9 C10 C11 126.14(18) . . ?
C10 C11 H11A 109.4 . . ?
C10 C11 H11B 109.4 . . ?
C10 C11 C12 110.99(17) . . ?
H11A C11 H11B 108.0 . . ?
C12 C11 H11A 109.4 . . ?
C12 C11 H11B 109.4 . . ?
C13 C12 C11 127.88(18) . . ?
C13 C12 C21 107.42(18) . . ?
C21 C12 C11 124.70(18) . . ?
C12 C13 C19 106.74(16) . . ?
C14 C13 C12 126.4(2) . . ?
C14 C13 C19 126.84(19) . . ?
C13 C14 H14 115.5 . . ?
C15 C14 C13 129.0(2) . . ?
C15 C14 H14 115.5 . . ?
C14 C15 H15 115.4 . . ?
C14 C15 C16 129.2(2) . . ?
C16 C15 H15 115.4 . . ?
C15 C16 H16 115.2 . . ?
C17 C16 C15 129.6(2) . . ?
C17 C16 H16 115.2 . . ?
C16 C17 H17 115.6 . . ?
C16 C17 C18 128.8(2) . . ?
C18 C17 H17 115.6 . . ?
C17 C18 H18 115.5 . . ?
C19 C18 C17 129.1(2) . . ?
C19 C18 H18 115.5 . . ?
C18 C19 C13 127.50(18) . . ?
C18 C19 C20 125.4(2) . . ?
C20 C19 C13 107.10(17) . . ?
C19 C20 C22 126.37(18) . . ?
C21 C20 C19 107.02(17) . . ?
C21 C20 C22 126.59(18) . . ?
C12 C21 H21 124.1 . . ?
C20 C21 C12 111.71(18) . . ?
C20 C21 H21 124.1 . . ?
C2 C22 C20 113.35(17) 7_566 . ?
C2 C22 H22A 108.9 7_566 . ?
C2 C22 H22B 108.9 7_566 . ?
C20 C22 H22A 108.9 . . ?
C20 C22 H22B 108.9 . . ?
H22A C22 H22B 107.7 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 C2 C3 C4 179.47(19) . . . . ?
C1 C2 C3 C9 0.3(2) . . . . ?
C1 C10 C11 C12 98.1(2) . . . . ?
C2 C1 C10 C9 1.1(2) . . . . ?
C2 C1 C10 C11 -175.66(18) . . . . ?
C2 C3 C4 C5 178.5(2) . . . . ?
C2 C3 C9 C8 -178.63(19) . . . . ?
C2 C3 C9 C10 0.3(2) . . . . ?
C3 C4 C5 C6 0.1(4) . . . . ?
C3 C9 C10 C1 -0.8(2) . . . . ?
C3 C9 C10 C11 175.91(18) . . . . ?
C4 C3 C9 C8 2.2(3) . . . . ?
C4 C3 C9 C10 -178.85(19) . . . . ?
C4 C5 C6 C7 0.8(4) . . . . ?
C5 C6 C7 C8 1.5(4) . . . . ?
C6 C7 C8 C9 -3.2(4) . . . . ?
C7 C8 C9 C3 1.1(4) . . . . ?
C7 C8 C9 C10 -177.6(2) . . . . ?
C8 C9 C10 C1 178.14(19) . . . . ?
C8 C9 C10 C11 -5.1(3) . . . . ?
C9 C3 C4 C5 -2.5(3) . . . . ?
C9 C10 C11 C12 -78.1(2) . . . . ?
C10 C1 C2 C3 -0.9(2) . . . . ?
C10 C1 C2 C22 176.48(18) . . . 7_566 ?
C10 C11 C12 C13 136.2(2) . . . . ?
C10 C11 C12 C21 -43.6(3) . . . . ?
C11 C12 C13 C14 1.3(3) . . . . ?
C11 C12 C13 C19 -179.29(18) . . . . ?
C11 C12 C21 C20 179.79(18) . . . . ?
C12 C13 C14 C15 179.6(2) . . . . ?
C12 C13 C19 C18 178.1(2) . . . . ?
C12 C13 C19 C20 -0.9(2) . . . . ?
C13 C12 C21 C20 -0.1(2) . . . . ?
C13 C14 C15 C16 1.4(4) . . . . ?
C13 C19 C20 C21 0.8(2) . . . . ?
C13 C19 C20 C22 179.19(19) . . . . ?
C14 C13 C19 C18 -2.6(3) . . . . ?
C14 C13 C19 C20 178.5(2) . . . . ?
C14 C15 C16 C17 -0.2(4) . . . . ?
C15 C16 C17 C18 -1.6(4) . . . . ?
C16 C17 C18 C19 0.7(4) . . . . ?
C17 C18 C19 C13 2.0(4) . . . . ?
C17 C18 C19 C20 -179.3(2) . . . . ?
C18 C19 C20 C21 -178.14(19) . . . . ?
C18 C19 C20 C22 0.2(3) . . . . ?
C19 C13 C14 C15 0.3(4) . . . . ?
C19 C20 C21 C12 -0.5(2) . . . . ?
C19 C20 C22 C2 -178.22(19) . . . 7_566 ?
C21 C12 C13 C14 -178.79(19) . . . . ?
C21 C12 C13 C19 0.6(2) . . . . ?
C21 C20 C22 C2 -0.2(3) . . . 7_566 ?
C22 C2 C3 C4 2.2(3) 7_566 . . . ?
C22 C2 C3 C9 -176.95(18) 7_566 . . . ?
C22 C20 C21 C12 -178.85(19) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'

# start Validation Reply Form
_vrf_PLAT031_shelxl              
;
PROBLEM: Refined Extinction Parameter within Range ......      2.667 Sigma 
RESPONSE: Refining the extinction parameter yielded slightly better
refinement values, and so it was included with its standard uncertainty.
;
_vrf_PLAT906_shelxl              
;
PROBLEM: Large K value in the Analysis of Variance ......     13.349 Check 
RESPONSE: The large value of K was for Fc/Fc(max) = 0.007. All others were
between 0.871 and 1.866.

;
_vrf_PLAT911_shelxl              
;
PROBLEM: Missing # FCF Refl Between THmin & STh/L=  0.600          2 Report
RESPONSE: These may have been obscured by the beamstop.
;
# end Validation Reply Form
