# Electronic Supplementary Material (ESI) for RSC Advances.
# This journal is © The Royal Society of Chemistry 2015

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_aa
_audit_block_doi                 10.5517/cc1jgc9n
_database_code_depnum_ccdc_archive 'CCDC 1413981'
_audit_update_record             
;
2015-07-20 deposited with the CCDC.
2015-07-27 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2013
_chemical_name_systematic        'Au11 nanocluster'
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C128 H130 Au11 P8 Se2, F6 Sb'
_chemical_formula_sum            'C128 H130 Au11 F6 P8 Sb Se2'
_chemical_formula_weight         4476.37

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   17.7943(19)
_cell_length_b                   19.9153(17)
_cell_length_c                   20.554(14)
_cell_angle_alpha                75.999(2)
_cell_angle_beta                 77.498(3)
_cell_angle_gamma                85.011(2)
_cell_volume                     6895(5)
_cell_formula_units_Z            2
_cell_measurement_temperature    291(2)
_cell_measurement_reflns_used    3861
_cell_measurement_theta_min      2.11
_cell_measurement_theta_max      25.86

_exptl_crystal_description       block
_exptl_crystal_colour            darkred
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.156
_exptl_crystal_F_000             4120
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.240
_exptl_crystal_size_mid          0.220
_exptl_crystal_size_min          0.200
_exptl_absorpt_coefficient_mu    12.515
_shelx_estimated_absorpt_T_min   0.153
_shelx_estimated_absorpt_T_max   0.189
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.151
_exptl_absorpt_correction_T_max  0.185
_exptl_absorpt_process_details   'SADABS, Bruker, 2013'

_exptl_special_details           
;
 ?
;

_diffrn_ambient_temperature      291(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'sealed tube'
_diffrn_measurement_device_type  'Bruker Smart Aepex CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            83014
_diffrn_reflns_av_unetI/netI     0.0955
_diffrn_reflns_av_R_equivalents  0.0153
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_theta_min         1.043
_diffrn_reflns_theta_max         27.000
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             30079
_reflns_number_gt                23629
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

# SQUEEZE RESULTS
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.137 0.711 0.220 22 8 ' '
2 0.197 0.535 0.855 13 1 ' '
3 0.202 0.885 0.111 7 3 ' '
4 0.500 0.500 0.500 913 151 ' '
5 0.315 0.786 0.046 8 1 ' '
6 0.406 0.562 0.829 21 1 ' '
7 0.594 0.438 0.171 21 1 ' '
8 0.684 0.214 0.954 8 1 ' '
9 0.802 0.465 0.145 13 1 ' '
10 0.798 0.115 0.889 7 3 ' '
11 0.863 0.289 0.780 22 8 ' '

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
;
 ?
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           fullcycle
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
;
 w=1/[σ²(Fo²)+(0.095P)²+1.99P]
 where P=(Fo²+2Fc²)/3
;
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         30079
_refine_ls_number_parameters     1399
_refine_ls_number_restraints     4
_refine_ls_R_factor_all          0.0579
_refine_ls_R_factor_gt           0.0561
_refine_ls_wR_factor_ref         0.1390
_refine_ls_wR_factor_gt          0.1385
_refine_ls_goodness_of_fit_ref   1.087
_refine_ls_restrained_S_all      1.088
_refine_ls_shift/su_max          0.038
_refine_ls_shift/su_mean         0.003

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.95076(2) 0.78431(2) 0.81757(2) 0.04224(6) Uani 1 1 d . . . . .
Au2 Au 0.77556(2) 0.84129(2) 0.86375(2) 0.04257(6) Uani 1 1 d . . . . .
Au3 Au 0.69141(2) 0.70914(2) 0.86929(2) 0.04340(6) Uani 1 1 d . . . . .
Au4 Au 0.87143(2) 0.62100(2) 0.81429(2) 0.04223(6) Uani 1 1 d . . . . .
Au5 Au 0.86406(2) 0.88755(2) 0.72984(2) 0.04230(6) Uani 1 1 d . . . . .
Au6 Au 0.69135(2) 0.81123(2) 0.74335(2) 0.04377(6) Uani 1 1 d . . . . .
Au7 Au 0.77081(2) 0.67124(2) 0.72004(2) 0.04275(6) Uani 1 1 d . . . . .
Au8 Au 0.95333(2) 0.72154(2) 0.69891(2) 0.04208(6) Uani 1 1 d . . . . .
Au9 Au 0.83349(2) 0.70182(2) 0.91657(2) 0.04216(6) Uani 1 1 d . . . . .
Au10 Au 0.83172(2) 0.80536(2) 0.64292(2) 0.04260(6) Uani 1 1 d . . . . .
Au11 Au 0.82331(2) 0.75503(2) 0.78161(2) 0.03988(5) Uani 1 1 d . . . . .
P1 P 1.07223(8) 0.78655(8) 0.84391(7) 0.0412(2) Uani 1 1 d . . . . .
P2 P 0.73623(10) 0.92334(8) 0.92446(9) 0.0463(3) Uani 1 1 d . U . . .
P3 P 0.57638(9) 0.67380(9) 0.94075(9) 0.0471(3) Uani 1 1 d . . . . .
P4 P 0.91516(9) 0.51017(8) 0.85873(8) 0.0428(3) Uani 1 1 d . . . . .
P5 P 0.90107(9) 0.99782(8) 0.67217(8) 0.0446(3) Uani 1 1 d . . . . .
P6 P 0.57507(10) 0.86066(9) 0.71436(9) 0.0487(3) Uani 1 1 d . . . . .
P7 P 0.72171(8) 0.59005(8) 0.67855(7) 0.0412(2) Uani 1 1 d . . . . .
P8 P 1.07237(10) 0.71659(9) 0.62627(9) 0.0481(3) Uani 1 1 d . . . . .
Sb1 Sb 0.35356(3) 0.71610(3) 0.21362(3) 0.05607(10) Uani 1 1 d . . . . .
Se1 Se 0.86346(3) 0.63565(3) 1.02561(3) 0.04239(10) Uani 1 1 d . . . . .
Se2 Se 0.86111(3) 0.86772(3) 0.52301(3) 0.04332(11) Uani 1 1 d . . . . .
C1 C 1.0789(4) 0.7918(3) 0.9298(3) 0.0448(11) Uani 1 1 d . . . . .
C2 C 1.0283(3) 0.7601(2) 0.9843(2) 0.0341(9) Uani 1 1 d . . . . .
H2 H 0.9877 0.7381 0.9774 0.041 Uiso 1 1 calc R U . . .
C3 C 1.0341(4) 0.7589(3) 1.0501(3) 0.0468(12) Uani 1 1 d . . . . .
H3 H 0.9996 0.7350 1.0875 0.056 Uiso 1 1 calc R U . . .
C4 C 1.0965(4) 0.7964(5) 1.0594(3) 0.0555(16) Uani 1 1 d . . . . .
H4 H 1.1009 0.7996 1.1028 0.067 Uiso 1 1 calc R U . . .
C5 C 1.1483(4) 0.8269(3) 1.0024(3) 0.0436(11) Uani 1 1 d . . . . .
H5 H 1.1901 0.8494 1.0065 0.052 Uiso 1 1 calc R U . . .
C6 C 1.1374(4) 0.8237(3) 0.9384(3) 0.0451(11) Uani 1 1 d . . . . .
H6 H 1.1725 0.8449 0.8999 0.054 Uiso 1 1 calc R U . . .
C7 C 1.1295(4) 0.8639(4) 0.7931(3) 0.0479(12) Uani 1 1 d . . . . .
C8 C 1.1013(4) 0.9289(4) 0.7988(4) 0.0549(14) Uani 1 1 d . . . . .
H8 H 1.0542 0.9346 0.8275 0.066 Uiso 1 1 calc R U . . .
C9 C 1.1437(4) 0.9863(4) 0.7612(3) 0.0469(11) Uani 1 1 d . . . . .
H9 H 1.1253 1.0304 0.7658 0.056 Uiso 1 1 calc R U . . .
C10 C 1.2128(4) 0.9782(3) 0.7173(3) 0.0490(13) Uani 1 1 d . . . . .
H10 H 1.2401 1.0168 0.6914 0.059 Uiso 1 1 calc R U . . .
C11 C 1.2410(4) 0.9135(4) 0.7121(3) 0.0465(12) Uani 1 1 d . . . . .
H11 H 1.2879 0.9083 0.6829 0.056 Uiso 1 1 calc R U . . .
C12 C 1.2005(3) 0.8549(4) 0.7498(4) 0.0496(14) Uani 1 1 d . . . . .
H12 H 1.2201 0.8108 0.7463 0.060 Uiso 1 1 calc R U . . .
C13 C 0.7955(3) 0.9411(3) 0.9790(3) 0.0420(10) Uani 1 1 d . U . . .
C14 C 0.8678(5) 0.9144(4) 0.9736(4) 0.0560(17) Uani 1 1 d . . . . .
H14 H 0.8876 0.8886 0.9412 0.067 Uiso 1 1 calc R U . . .
C15 C 0.9146(5) 0.9261(4) 1.0187(5) 0.0602(17) Uani 1 1 d . . . . .
H15 H 0.9645 0.9072 1.0165 0.072 Uiso 1 1 calc R U . . .
C16 C 0.8850(3) 0.9646(3) 1.0635(3) 0.0427(10) Uani 1 1 d . . . . .
H16 H 0.9146 0.9714 1.0934 0.051 Uiso 1 1 calc R U . . .
C17 C 0.8099(4) 0.9955(3) 1.0672(3) 0.0454(12) Uani 1 1 d . . . . .
H17 H 0.7909 1.0252 1.0960 0.054 Uiso 1 1 calc R U . . .
C18 C 0.7664(3) 0.9788(3) 1.0252(3) 0.0389(9) Uani 1 1 d . . . . .
H18 H 0.7152 0.9944 1.0293 0.047 Uiso 1 1 calc R U . . .
C19 C 0.6559(4) 0.8932(3) 0.9894(4) 0.0479(12) Uani 1 1 d . . . . .
C20 C 0.5991(5) 0.9412(3) 1.0123(3) 0.0482(13) Uani 1 1 d . . . . .
H20 H 0.6041 0.9881 0.9916 0.058 Uiso 1 1 calc R U . . .
C21 C 0.5367(3) 0.9207(4) 1.0640(3) 0.0459(12) Uani 1 1 d . . . . .
H21 H 0.4992 0.9526 1.0782 0.055 Uiso 1 1 calc R U . . .
C22 C 0.5315(4) 0.8482(3) 1.0955(4) 0.0500(13) Uani 1 1 d . . . . .
H22 H 0.4909 0.8331 1.1318 0.060 Uiso 1 1 calc R U . . .
C23 C 0.5839(4) 0.8016(4) 1.0738(4) 0.0544(15) Uani 1 1 d . . . . .
H23 H 0.5774 0.7547 1.0932 0.065 Uiso 1 1 calc R U . . .
C24 C 0.6473(5) 0.8227(4) 1.0232(4) 0.0553(15) Uani 1 1 d . . . . .
H24 H 0.6850 0.7901 1.0111 0.066 Uiso 1 1 calc R U . . .
C25 C 0.5120(5) 0.7521(4) 0.9355(4) 0.0525(14) Uani 1 1 d . . . . .
C26 C 0.5343(4) 0.8105(3) 0.9546(4) 0.0457(12) Uani 1 1 d . . . . .
H26 H 0.5804 0.8107 0.9690 0.055 Uiso 1 1 calc R U . . .
C27 C 0.4818(4) 0.8679(4) 0.9501(4) 0.0543(15) Uani 1 1 d . . . . .
H27 H 0.4911 0.9062 0.9651 0.065 Uiso 1 1 calc R U . . .
C28 C 0.4210(4) 0.8681(4) 0.9254(4) 0.0529(14) Uani 1 1 d . . . . .
H28 H 0.3879 0.9069 0.9242 0.063 Uiso 1 1 calc R U . . .
C29 C 0.4013(3) 0.8144(3) 0.9003(4) 0.0501(14) Uani 1 1 d . . . . .
H29 H 0.3588 0.8184 0.8799 0.060 Uiso 1 1 calc R U . . .
C30 C 0.4473(4) 0.7558(4) 0.9073(4) 0.0524(13) Uani 1 1 d . . . . .
H30 H 0.4351 0.7179 0.8929 0.063 Uiso 1 1 calc R U . . .
C31 C 0.5903(4) 0.6412(4) 1.0249(4) 0.0560(16) Uani 1 1 d . . . . .
C32 C 0.6664(4) 0.6169(4) 1.0390(4) 0.0545(15) Uani 1 1 d . . . . .
H32 H 0.7091 0.6191 1.0034 0.065 Uiso 1 1 calc R U . . .
C33 C 0.6734(4) 0.5916(4) 1.1041(4) 0.0551(15) Uani 1 1 d . . . . .
H33 H 0.7220 0.5778 1.1133 0.066 Uiso 1 1 calc R U . . .
C34 C 0.6104(4) 0.5852(4) 1.1582(3) 0.0493(13) Uani 1 1 d . . . . .
H34 H 0.6173 0.5650 1.2024 0.059 Uiso 1 1 calc R U . . .
C35 C 0.5411(4) 0.6072(3) 1.1480(3) 0.0487(13) Uani 1 1 d . . . . .
H35 H 0.5008 0.6063 1.1856 0.058 Uiso 1 1 calc R U . . .
C36 C 0.5264(4) 0.6321(3) 1.0818(3) 0.0460(12) Uani 1 1 d . . . . .
H36 H 0.4763 0.6425 1.0751 0.055 Uiso 1 1 calc R U . . .
C37 C 0.8348(6) 0.4650(4) 0.9188(4) 0.0589(16) Uani 1 1 d . . . . .
C38 C 0.7924(4) 0.4898(3) 0.9718(3) 0.0450(11) Uani 1 1 d . . . . .
H38 H 0.8033 0.5330 0.9764 0.054 Uiso 1 1 calc R U . . .
C39 C 0.7339(5) 0.4539(4) 1.0192(4) 0.0571(15) Uani 1 1 d . . . . .
H39 H 0.7086 0.4720 1.0561 0.068 Uiso 1 1 calc R U . . .
C40 C 0.7122(3) 0.3906(3) 1.0124(3) 0.0421(11) Uani 1 1 d . . . . .
H40 H 0.6727 0.3655 1.0436 0.051 Uiso 1 1 calc R U . . .
C41 C 0.7531(6) 0.3676(5) 0.9564(5) 0.0637(18) Uani 1 1 d . . . . .
H41 H 0.7376 0.3272 0.9489 0.076 Uiso 1 1 calc R U . . .
C42 C 0.8152(5) 0.3998(4) 0.9106(4) 0.0517(13) Uani 1 1 d . . . . .
H42 H 0.8432 0.3799 0.8758 0.062 Uiso 1 1 calc R U . . .
C43 C 0.9514(3) 0.4571(3) 0.7980(3) 0.0416(10) Uani 1 1 d . . . . .
C44 C 0.9284(4) 0.4751(4) 0.7346(4) 0.0471(12) Uani 1 1 d . . . . .
H44 H 0.8950 0.5130 0.7244 0.056 Uiso 1 1 calc R U . . .
C45 C 0.9561(4) 0.4359(4) 0.6891(3) 0.0477(13) Uani 1 1 d . . . . .
H45 H 0.9394 0.4465 0.6478 0.057 Uiso 1 1 calc R U . . .
C46 C 1.0083(4) 0.3804(3) 0.7008(4) 0.0485(12) Uani 1 1 d . . . . .
H46 H 1.0280 0.3562 0.6670 0.058 Uiso 1 1 calc R U . . .
C47 C 1.0317(5) 0.3607(3) 0.7665(4) 0.0508(14) Uani 1 1 d . . . . .
H47 H 1.0638 0.3221 0.7778 0.061 Uiso 1 1 calc R U . . .
C48 C 1.0027(4) 0.4037(4) 0.8120(3) 0.0512(13) Uani 1 1 d . . . . .
H48 H 1.0193 0.3953 0.8533 0.061 Uiso 1 1 calc R U . . .
C49 C 0.9325(3) 1.0512(2) 0.7182(3) 0.0375(9) Uani 1 1 d . U . . .
C50 C 0.9313(3) 1.0272(3) 0.7893(3) 0.0401(9) Uani 1 1 d . U . . .
H50 H 0.9152 0.9829 0.8117 0.048 Uiso 1 1 calc R U . . .
C51 C 0.9534(4) 1.0680(3) 0.8240(4) 0.0497(12) Uani 1 1 d . . . . .
H51 H 0.9531 1.0516 0.8704 0.060 Uiso 1 1 calc R U . . .
C52 C 0.9768(5) 1.1350(4) 0.7915(4) 0.0546(15) Uani 1 1 d . . . . .
H52 H 0.9902 1.1639 0.8163 0.066 Uiso 1 1 calc R U . . .
C53 C 0.9798(5) 1.1580(4) 0.7217(3) 0.0548(16) Uani 1 1 d . . . . .
H53 H 1.0011 1.2002 0.6981 0.066 Uiso 1 1 calc R U . . .
C54 C 0.9512(4) 1.1181(3) 0.6880(3) 0.0492(13) Uani 1 1 d . . . . .
H54 H 0.9443 1.1369 0.6435 0.059 Uiso 1 1 calc R U . . .
C55 C 0.8283(3) 1.0574(3) 0.6405(3) 0.0447(12) Uani 1 1 d . . . . .
C56 C 0.7875(4) 1.0417(4) 0.5958(5) 0.0572(18) Uani 1 1 d . . . . .
H56 H 0.7977 0.9996 0.5828 0.069 Uiso 1 1 calc R U . . .
C57 C 0.7320(5) 1.0873(5) 0.5702(4) 0.0579(16) Uani 1 1 d . . . . .
H57 H 0.7090 1.0774 0.5372 0.069 Uiso 1 1 calc R U . . .
C58 C 0.7095(4) 1.1495(4) 0.5937(3) 0.0525(14) Uani 1 1 d . . . . .
H58 H 0.6704 1.1797 0.5791 0.063 Uiso 1 1 calc R U . . .
C59 C 0.7505(5) 1.1611(4) 0.6400(6) 0.0631(19) Uani 1 1 d . . . . .
H59 H 0.7389 1.2014 0.6561 0.076 Uiso 1 1 calc R U . . .
C60 C 0.8080(4) 1.1162(4) 0.6636(4) 0.0535(14) Uani 1 1 d . . . . .
H60 H 0.8327 1.1264 0.6954 0.064 Uiso 1 1 calc R U . . .
C61 C 0.5694(4) 0.8910(4) 0.6288(3) 0.0470(12) Uani 1 1 d . . . . .
C62 C 0.6347(4) 0.8988(4) 0.5778(4) 0.0557(17) Uani 1 1 d . . . . .
H62 H 0.6828 0.8872 0.5890 0.067 Uiso 1 1 calc R U . . .
C63 C 0.6293(5) 0.9234(5) 0.5105(4) 0.0611(19) Uani 1 1 d . . . . .
H63 H 0.6739 0.9313 0.4767 0.073 Uiso 1 1 calc R U . . .
C64 C 0.5580(7) 0.9367(5) 0.4925(4) 0.071 Uani 1 1 d . . . . .
H64 H 0.5544 0.9512 0.4467 0.086 Uiso 1 1 calc R U . . .
C65 C 0.4909(3) 0.9280(4) 0.5442(4) 0.0540(15) Uani 1 1 d . U . . .
H65 H 0.4428 0.9378 0.5326 0.065 Uiso 1 1 calc R U . . .
C66 C 0.4963(4) 0.9053(4) 0.6112(3) 0.0544(16) Uani 1 1 d . U . . .
H66 H 0.4519 0.8992 0.6453 0.065 Uiso 1 1 calc R U . . .
C67 C 0.4930(4) 0.8017(4) 0.7356(5) 0.064(2) Uani 1 1 d . . . . .
C68 C 0.4224(6) 0.8218(4) 0.7700(5) 0.0606(18) Uani 1 1 d . . . . .
H68 H 0.4164 0.8637 0.7834 0.073 Uiso 1 1 calc R U . . .
C69 C 0.3592(4) 0.7783(4) 0.7848(5) 0.0603(18) Uani 1 1 d . . . . .
H69 H 0.3112 0.7917 0.8073 0.072 Uiso 1 1 calc R U . . .
C70 C 0.3696(5) 0.7148(5) 0.7653(4) 0.0596(17) Uani 1 1 d . . . . .
H70 H 0.3287 0.6853 0.7759 0.072 Uiso 1 1 calc R U . . .
C71 C 0.4412(5) 0.6958(5) 0.7300(5) 0.065(2) Uani 1 1 d . . . . .
H71 H 0.4477 0.6544 0.7158 0.078 Uiso 1 1 calc R U . . .
C72 C 0.5029(4) 0.7389(4) 0.7160(5) 0.0572(17) Uani 1 1 d . . . . .
H72 H 0.5510 0.7257 0.6935 0.069 Uiso 1 1 calc R U . . .
C73 C 0.6353(3) 0.6157(3) 0.6438(3) 0.0397(10) Uani 1 1 d . . . . .
C74 C 0.6313(4) 0.6798(3) 0.6023(5) 0.0534(15) Uani 1 1 d . . . . .
H74 H 0.6721 0.7094 0.5922 0.064 Uiso 1 1 calc R U . . .
C75 C 0.5659(4) 0.7009(4) 0.5750(4) 0.0539(16) Uani 1 1 d . . . . .
H75 H 0.5622 0.7447 0.5467 0.065 Uiso 1 1 calc R U . . .
C76 C 0.5049(4) 0.6546(5) 0.5909(4) 0.0568(16) Uani 1 1 d . . . . .
H76 H 0.4606 0.6682 0.5732 0.068 Uiso 1 1 calc R U . . .
C77 C 0.5110(4) 0.5906(4) 0.6317(5) 0.0543(15) Uani 1 1 d . . . . .
H77 H 0.4713 0.5600 0.6411 0.065 Uiso 1 1 calc R U . . .
C78 C 0.5761(4) 0.5705(4) 0.6594(3) 0.0480(12) Uani 1 1 d . . . . .
H78 H 0.5798 0.5269 0.6882 0.058 Uiso 1 1 calc R U . . .
C79 C 0.7826(4) 0.5596(3) 0.6154(4) 0.0493(12) Uani 1 1 d . . . . .
C80 C 0.7531(3) 0.5189(3) 0.5820(4) 0.0477(13) Uani 1 1 d . . . . .
H80 H 0.7023 0.5056 0.5970 0.057 Uiso 1 1 calc R U . . .
C81 C 0.7985(5) 0.4976(4) 0.5262(4) 0.0532(14) Uani 1 1 d . . . . .
H81 H 0.7780 0.4701 0.5042 0.064 Uiso 1 1 calc R U . . .
C82 C 0.8733(6) 0.5169(4) 0.5034(3) 0.060(2) Uani 1 1 d . . . . .
H82 H 0.9021 0.5036 0.4648 0.072 Uiso 1 1 calc R U . . .
C83 C 0.9074(4) 0.5556(3) 0.5358(4) 0.0532(15) Uani 1 1 d . . . . .
H83 H 0.9592 0.5660 0.5212 0.064 Uiso 1 1 calc R U . . .
C84 C 0.8617(4) 0.5786(3) 0.5915(2) 0.0458(12) Uani 1 1 d . . . . .
H84 H 0.8826 0.6062 0.6131 0.055 Uiso 1 1 calc R U . . .
C85 C 1.0823(4) 0.7049(2) 0.5402(3) 0.0444(12) Uani 1 1 d . . . . .
C86 C 1.0204(5) 0.7214(4) 0.5065(3) 0.0515(14) Uani 1 1 d . . . . .
H86 H 0.9740 0.7388 0.5282 0.062 Uiso 1 1 calc R U . . .
C87 C 1.0283(5) 0.7118(4) 0.4404(3) 0.0527(14) Uani 1 1 d . . . . .
H87 H 0.9873 0.7221 0.4178 0.063 Uiso 1 1 calc R U . . .
C88 C 1.0991(4) 0.6862(4) 0.4082(4) 0.0533(14) Uani 1 1 d . U . . .
H88 H 1.1052 0.6801 0.3639 0.064 Uiso 1 1 calc R U . . .
C89 C 1.1592(5) 0.6702(4) 0.4419(3) 0.0504(13) Uani 1 1 d . U . . .
H89 H 1.2058 0.6532 0.4201 0.060 Uiso 1 1 calc R U . . .
C90 C 1.1516(4) 0.6788(4) 0.5077(3) 0.0475(12) Uani 1 1 d . . . . .
H90 H 1.1926 0.6672 0.5302 0.057 Uiso 1 1 calc R U . . .
C91 C 1.1324(5) 0.6417(3) 0.6578(3) 0.0511(14) Uani 1 1 d . . . . .
C92 C 1.1099(5) 0.5752(4) 0.6597(3) 0.0517(14) Uani 1 1 d . . . . .
H92 H 1.0663 0.5679 0.6447 0.062 Uiso 1 1 calc R U . . .
C93 C 1.1579(4) 0.5209(4) 0.6858(4) 0.0545(15) Uani 1 1 d . . . . .
H93 H 1.1436 0.4758 0.6907 0.065 Uiso 1 1 calc R U . . .
C94 C 1.2247(4) 0.5300(3) 0.7047(3) 0.0483(12) Uani 1 1 d . . . . .
H94 H 1.2550 0.4921 0.7217 0.058 Uiso 1 1 calc R U . . .
C95 C 1.2460(4) 0.5950(4) 0.6983(3) 0.0487(13) Uani 1 1 d . . . . .
H95 H 1.2914 0.6017 0.7110 0.058 Uiso 1 1 calc R U . . .
C96 C 1.2009(5) 0.6531(4) 0.6728(4) 0.0560(15) Uani 1 1 d . . . . .
H96 H 1.2171 0.6978 0.6664 0.067 Uiso 1 1 calc R U . . .
C97 C 0.8304(3) 0.6881(3) 1.0913(3) 0.0444(11) Uani 1 1 d . . . . .
C98 C 0.8036(4) 0.6517(3) 1.1565(4) 0.0551(16) Uani 1 1 d . . . . .
H98 H 0.7988 0.6039 1.1675 0.066 Uiso 1 1 calc R U . . .
C99 C 0.7834(3) 0.6925(3) 1.2066(3) 0.0452(13) Uani 1 1 d . . . . .
H99 H 0.7704 0.6710 1.2528 0.054 Uiso 1 1 calc R U . . .
C100 C 0.7831(3) 0.7628(4) 1.1864(4) 0.0472(12) Uani 1 1 d . . . . .
H100 H 0.7646 0.7892 1.2186 0.057 Uiso 1 1 calc R U . . .
C101 C 0.8100(4) 0.7957(4) 1.1185(4) 0.0551(16) Uani 1 1 d . . . . .
H101 H 0.8128 0.8436 1.1055 0.066 Uiso 1 1 calc R U . . .
C102 C 0.8315(4) 0.7574(4) 1.0730(3) 0.0489(13) Uani 1 1 d . . . . .
H102 H 0.8479 0.7790 1.0272 0.059 Uiso 1 1 calc R U . . .
C103 C 0.8383(3) 0.8117(3) 0.4625(3) 0.0397(9) Uani 1 1 d . . . . .
C104 C 0.8576(4) 0.8322(3) 0.3911(3) 0.0465(13) Uani 1 1 d . . . . .
H104 H 0.8867 0.8713 0.3716 0.056 Uiso 1 1 calc R U . . .
C105 C 0.8373(6) 0.7999(5) 0.3509(4) 0.0614(18) Uani 1 1 d . . . . .
H105 H 0.8441 0.8194 0.3042 0.074 Uiso 1 1 calc R U . . .
C106 C 0.8043(5) 0.7339(3) 0.3787(4) 0.0543(16) Uani 1 1 d . . . . .
H106 H 0.7953 0.7076 0.3495 0.065 Uiso 1 1 calc R U . . .
C107 C 0.7863(7) 0.7097(5) 0.4454(5) 0.070(3) Uani 1 1 d . . . . .
H107 H 0.7619 0.6677 0.4629 0.083 Uiso 1 1 calc R U . . .
C108 C 0.8038(6) 0.7471(4) 0.4918(4) 0.0560(15) Uani 1 1 d . . . . .
H108 H 0.7928 0.7296 0.5389 0.067 Uiso 1 1 calc R U . . .
C109 C 1.1291(4) 0.7118(4) 0.8252(4) 0.0538(14) Uani 1 1 d . . . . .
H10A H 1.1596 0.7224 0.7790 0.065 Uiso 1 1 calc R U . . .
H10B H 1.1634 0.6959 0.8571 0.065 Uiso 1 1 calc R U . . .
C110 C 1.0705(4) 0.6571(3) 0.8331(4) 0.0504(13) Uani 1 1 d . . . . .
H11A H 1.0255 0.6786 0.8158 0.060 Uiso 1 1 calc R U . . .
H11B H 1.0930 0.6228 0.8073 0.060 Uiso 1 1 calc R U . . .
C111 C 1.0480(5) 0.6231(6) 0.9082(4) 0.0630(19) Uani 1 1 d . . . . .
H11C H 1.0428 0.6585 0.9342 0.076 Uiso 1 1 calc R U . . .
H11D H 1.0895 0.5911 0.9210 0.076 Uiso 1 1 calc R U . . .
C112 C 0.9710(4) 0.5827(4) 0.9291(4) 0.0529(14) Uani 1 1 d . . . . .
H11E H 0.9517 0.5773 0.9779 0.063 Uiso 1 1 calc R U . . .
H11F H 0.9330 0.6103 0.9056 0.063 Uiso 1 1 calc R U . . .
C113 C 0.9799(4) 0.5094(4) 0.9122(3) 0.0498(12) Uani 1 1 d . . . . .
H11G H 0.9676 0.4735 0.9538 0.060 Uiso 1 1 calc R U . . .
H11H H 1.0322 0.5009 0.8891 0.060 Uiso 1 1 calc R U . . .
C114 C 0.7002(4) 1.0037(4) 0.8814(4) 0.0529(13) Uani 1 1 d . . . . .
H11I H 0.6897 1.0356 0.9116 0.064 Uiso 1 1 calc R U . . .
H11J H 0.7384 1.0237 0.8415 0.064 Uiso 1 1 calc R U . . .
C115 C 0.6269(5) 0.9926(4) 0.8598(5) 0.0613(18) Uani 1 1 d . . . . .
H11K H 0.5904 0.9703 0.8999 0.074 Uiso 1 1 calc R U . . .
H11L H 0.6044 1.0373 0.8411 0.074 Uiso 1 1 calc R U . . .
C116 C 0.6385(4) 0.9500(4) 0.8083(5) 0.0571(16) Uani 1 1 d . . . . .
H11M H 0.6170 0.9051 0.8306 0.069 Uiso 1 1 calc R U . . .
H11N H 0.6934 0.9425 0.7930 0.069 Uiso 1 1 calc R U . . .
C117 C 0.6020(4) 0.9809(3) 0.7430(3) 0.0516(17) Uani 1 1 d . . . . .
H11O H 0.5839 1.0285 0.7421 0.062 Uiso 1 1 calc R U . . .
H11P H 0.6402 0.9803 0.7015 0.062 Uiso 1 1 calc R U . . .
C118 C 0.5344(5) 0.9360(3) 0.7471(3) 0.0536(15) Uani 1 1 d . . . . .
H11Q H 0.4987 0.9618 0.7198 0.064 Uiso 1 1 calc R U . . .
H11R H 0.5069 0.9217 0.7942 0.064 Uiso 1 1 calc R U . . .
C119 C 0.5408(4) 0.6228(5) 0.8952(3) 0.0532(13) Uani 1 1 d . . . . .
H11S H 0.4899 0.6081 0.9202 0.064 Uiso 1 1 calc R U . . .
H11T H 0.5348 0.6520 0.8513 0.064 Uiso 1 1 calc R U . . .
C120 C 0.5870(7) 0.5618(6) 0.8829(5) 0.069(2) Uani 1 1 d . . . . .
H12A H 0.6252 0.5522 0.9115 0.082 Uiso 1 1 d R U . . .
H12B H 0.5583 0.5205 0.8900 0.082 Uiso 1 1 d R U . . .
C121 C 0.6350(5) 0.5784(7) 0.8119(6) 0.073(3) Uani 1 1 d . . . . .
H12C H 0.6607 0.6216 0.8036 0.087 Uiso 1 1 calc R U . . .
H12D H 0.6030 0.5828 0.7783 0.087 Uiso 1 1 calc R U . . .
C122 C 0.6952(7) 0.5172(4) 0.8072(4) 0.066(2) Uani 1 1 d . . . . .
H12E H 0.6634 0.4786 0.8328 0.079 Uiso 1 1 d R U . . .
H12F H 0.7358 0.5193 0.8314 0.079 Uiso 1 1 d R U . . .
C123 C 0.7207(4) 0.5052(3) 0.7369(3) 0.0474(12) Uani 1 1 d . . . . .
H12G H 0.6853 0.4758 0.7279 0.057 Uiso 1 1 calc R U . . .
H12H H 0.7717 0.4831 0.7315 0.057 Uiso 1 1 calc R U . . .
C124 C 0.9783(3) 0.9898(3) 0.5912(3) 0.0408(9) Uani 1 1 d . . . . .
H12I H 0.9602 0.9615 0.5657 0.049 Uiso 1 1 calc R U . . .
H12J H 0.9899 1.0351 0.5615 0.049 Uiso 1 1 calc R U . . .
C125 C 1.0498(5) 0.9554(4) 0.6177(4) 0.0556(17) Uani 1 1 d . . . . .
H12K H 1.0696 0.9875 0.6381 0.067 Uiso 1 1 calc R U . . .
H12L H 1.0337 0.9151 0.6539 0.067 Uiso 1 1 calc R U . . .
C126 C 1.1137(3) 0.9334(4) 0.5677(3) 0.0471(12) Uani 1 1 d . . . . .
H12M H 1.1616 0.9267 0.5841 0.057 Uiso 1 1 calc R U . . .
H12N H 1.1207 0.9665 0.5238 0.057 Uiso 1 1 calc R U . . .
C127 C 1.0837(4) 0.8633(4) 0.5634(5) 0.0564(15) Uani 1 1 d . . . . .
H12O H 1.0280 0.8632 0.5772 0.068 Uiso 1 1 calc R U . . .
H12P H 1.0978 0.8575 0.5167 0.068 Uiso 1 1 calc R U . . .
C128 C 1.1189(3) 0.8052(3) 0.6099(3) 0.0460(11) Uani 1 1 d . . . . .
H12Q H 1.1148 0.8173 0.6535 0.055 Uiso 1 1 calc R U . . .
H12R H 1.1732 0.8004 0.5903 0.055 Uiso 1 1 calc R U . . .
F1 F 0.4161(3) 0.6408(3) 0.2515(3) 0.0621(10) Uani 1 1 d . . . . .
F2 F 0.2703(3) 0.6809(3) 0.2865(3) 0.0640(11) Uani 1 1 d . . . . .
F3 F 0.2907(3) 0.7869(4) 0.1801(2) 0.0664(15) Uani 1 1 d . . . . .
F4 F 0.4370(3) 0.7489(3) 0.1422(3) 0.0593(10) Uani 1 1 d . . . . .
F5 F 0.4020(3) 0.7618(3) 0.2637(2) 0.0567(10) Uani 1 1 d . . . . .
F6 F 0.3065(3) 0.6704(3) 0.1644(3) 0.0627(11) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 P1 2.3457(15) . ?
Au1 Au11 2.6821(19) . ?
Au1 Au9 2.887(2) . ?
Au1 Au5 2.953(2) . ?
Au1 Au8 2.9882(15) . ?
Au1 Au2 3.245(2) . ?
Au2 P2 2.2644(17) . ?
Au2 Au11 2.6556(19) . ?
Au2 Au5 2.8378(15) . ?
Au2 Au9 2.913(2) . ?
Au2 Au3 3.106(2) . ?
Au2 Au6 3.3476(15) . ?
Au3 P3 2.3003(16) . ?
Au3 Au11 2.7086(19) . ?
Au3 Au6 2.8789(13) . ?
Au3 Au9 2.879(2) . ?
Au3 Au7 3.3218(19) . ?
Au4 P4 2.3119(16) . ?
Au4 Au11 2.7006(19) . ?
Au4 Au7 2.8657(11) . ?
Au4 Au9 2.8810(13) . ?
Au4 Au8 2.910(2) . ?
Au5 P5 2.3055(15) . ?
Au5 Au11 2.6950(19) . ?
Au5 Au10 2.8681(11) . ?
Au6 P6 2.3454(17) . ?
Au6 Au11 2.7021(19) . ?
Au6 Au10 2.889(2) . ?
Au6 Au7 3.110(2) . ?
Au7 P7 2.3111(14) . ?
Au7 Au11 2.6578(19) . ?
Au7 Au10 2.921(2) . ?
Au8 P8 2.3220(17) . ?
Au8 Au11 2.6953(19) . ?
Au8 Au10 2.883(2) . ?
Au9 Se1 2.4515(14) . ?
Au9 Au11 2.7592(18) . ?
Au10 Se2 2.4422(15) . ?
Au10 Au11 2.7591(19) . ?
P1 C109 1.798(7) . ?
P1 C1 1.823(7) . ?
P1 C7 1.881(7) . ?
P2 C19 1.766(6) . ?
P2 C114 1.771(8) . ?
P2 C13 1.806(6) . ?
P3 C31 1.758(9) . ?
P3 C119 1.772(8) . ?
P3 C25 1.848(8) . ?
P4 C113 1.752(7) . ?
P4 C43 1.807(6) . ?
P4 C37 1.816(9) . ?
P5 C49 1.776(6) . ?
P5 C55 1.798(6) . ?
P5 C124 1.946(6) . ?
P6 C61 1.739(6) . ?
P6 C118 1.821(6) . ?
P6 C67 1.865(9) . ?
P7 C79 1.698(7) . ?
P7 C73 1.816(6) . ?
P7 C123 1.819(6) . ?
P8 C85 1.808(6) . ?
P8 C91 1.828(7) . ?
P8 C128 1.938(6) . ?
Sb1 F3 1.818(6) . ?
Sb1 F6 1.871(5) . ?
Sb1 F4 1.884(6) . ?
Sb1 F5 1.898(5) . ?
Sb1 F1 1.901(6) . ?
Sb1 F2 1.908(6) . ?
Se1 C97 1.868(6) . ?
Se2 C103 1.981(6) . ?
C1 C6 1.331(9) . ?
C1 C2 1.335(8) . ?
C2 C3 1.374(7) . ?
C2 H2 0.9300 . ?
C3 C4 1.460(9) . ?
C3 H3 0.9300 . ?
C4 C5 1.370(9) . ?
C4 H4 0.9300 . ?
C5 C6 1.386(7) . ?
C5 H5 0.9300 . ?
C6 H6 0.9300 . ?
C7 C8 1.369(11) . ?
C7 C12 1.403(8) . ?
C8 C9 1.394(10) . ?
C8 H8 0.9300 . ?
C9 C10 1.382(7) . ?
C9 H9 0.9300 . ?
C10 C11 1.360(9) . ?
C10 H10 0.9300 . ?
C11 C12 1.397(10) . ?
C11 H11 0.9300 . ?
C12 H12 0.9300 . ?
C13 C18 1.341(8) . ?
C13 C14 1.341(9) . ?
C14 C15 1.441(12) . ?
C14 H14 0.9300 . ?
C15 C16 1.333(10) . ?
C15 H15 0.9300 . ?
C16 C17 1.416(7) . ?
C16 H16 0.9300 . ?
C17 C18 1.388(7) . ?
C17 H17 0.9300 . ?
C18 H18 0.9300 . ?
C19 C24 1.413(8) . ?
C19 C20 1.415(8) . ?
C20 C21 1.375(10) . ?
C20 H20 0.9300 . ?
C21 C22 1.434(9) . ?
C21 H21 0.9300 . ?
C22 C23 1.341(9) . ?
C22 H22 0.9300 . ?
C23 C24 1.377(10) . ?
C23 H23 0.9300 . ?
C24 H24 0.9300 . ?
C25 C30 1.387(10) . ?
C25 C26 1.425(9) . ?
C26 C27 1.411(8) . ?
C26 H26 0.9300 . ?
C27 C28 1.289(12) . ?
C27 H27 0.9300 . ?
C28 C29 1.393(11) . ?
C28 H28 0.9300 . ?
C29 C30 1.363(10) . ?
C29 H29 0.9300 . ?
C30 H30 0.9300 . ?
C31 C36 1.433(7) . ?
C31 C32 1.461(9) . ?
C32 C33 1.340(12) . ?
C32 H32 0.9300 . ?
C33 C34 1.388(10) . ?
C33 H33 0.9300 . ?
C34 C35 1.316(10) . ?
C34 H34 0.9300 . ?
C35 C36 1.403(9) . ?
C35 H35 0.9300 . ?
C36 H36 0.9300 . ?
C37 C38 1.357(10) . ?
C37 C42 1.431(9) . ?
C38 C39 1.376(9) . ?
C38 H38 0.9300 . ?
C39 C40 1.398(10) . ?
C39 H39 0.9300 . ?
C40 C41 1.377(10) . ?
C40 H40 0.9300 . ?
C41 C42 1.378(11) . ?
C41 H41 0.9300 . ?
C42 H42 0.9300 . ?
C43 C48 1.358(9) . ?
C43 C44 1.404(9) . ?
C44 C45 1.347(10) . ?
C44 H44 0.9300 . ?
C45 C46 1.391(10) . ?
C45 H45 0.9300 . ?
C46 C47 1.453(9) . ?
C46 H46 0.9300 . ?
C47 C48 1.406(10) . ?
C47 H47 0.9300 . ?
C48 H48 0.9300 . ?
C49 C54 1.363(5) . ?
C49 C50 1.419(7) . ?
C50 C51 1.334(8) . ?
C50 H50 0.9300 . ?
C51 C52 1.394(8) . ?
C51 H51 0.9300 . ?
C52 C53 1.388(9) . ?
C52 H52 0.9300 . ?
C53 C54 1.364(10) . ?
C53 H53 0.9300 . ?
C54 H54 0.9300 . ?
C55 C60 1.359(11) . ?
C55 C56 1.394(11) . ?
C56 C57 1.383(10) . ?
C56 H56 0.9300 . ?
C57 C58 1.429(13) . ?
C57 H57 0.9300 . ?
C58 C59 1.391(13) . ?
C58 H58 0.9300 . ?
C59 C60 1.388(11) . ?
C59 H59 0.9300 . ?
C60 H60 0.9300 . ?
C61 C62 1.378(10) . ?
C61 C66 1.412(8) . ?
C62 C63 1.373(11) . ?
C62 H62 0.9300 . ?
C63 C64 1.383(13) . ?
C63 H63 0.9300 . ?
C64 C65 1.408(11) . ?
C64 H64 0.9300 . ?
C65 C66 1.363(10) . ?
C65 H65 0.9300 . ?
C66 H66 0.9300 . ?
C67 C68 1.379(9) . ?
C67 C72 1.389(13) . ?
C68 C69 1.415(12) . ?
C68 H68 0.9300 . ?
C69 C70 1.403(10) . ?
C69 H69 0.9300 . ?
C70 C71 1.393(10) . ?
C70 H70 0.9300 . ?
C71 C72 1.391(12) . ?
C71 H71 0.9300 . ?
C72 H72 0.9300 . ?
C73 C74 1.359(9) . ?
C73 C78 1.381(9) . ?
C74 C75 1.389(8) . ?
C74 H74 0.9300 . ?
C75 C76 1.418(10) . ?
C75 H75 0.9300 . ?
C76 C77 1.356(11) . ?
C76 H76 0.9300 . ?
C77 C78 1.386(9) . ?
C77 H77 0.9300 . ?
C78 H78 0.9300 . ?
C79 C80 1.379(10) . ?
C79 C84 1.438(10) . ?
C80 C81 1.386(9) . ?
C80 H80 0.9300 . ?
C81 C82 1.367(12) . ?
C81 H81 0.9300 . ?
C82 C83 1.383(14) . ?
C82 H82 0.9300 . ?
C83 C84 1.403(10) . ?
C83 H83 0.9300 . ?
C84 H84 0.9300 . ?
C85 C90 1.392(8) . ?
C85 C86 1.401(11) . ?
C86 C87 1.395(8) . ?
C86 H86 0.9300 . ?
C87 C88 1.405(9) . ?
C87 H87 0.9300 . ?
C88 C89 1.370(11) . ?
C88 H88 0.9300 . ?
C89 C90 1.381(8) . ?
C89 H89 0.9300 . ?
C90 H90 0.9300 . ?
C91 C96 1.370(13) . ?
C91 C92 1.406(10) . ?
C92 C93 1.394(8) . ?
C92 H92 0.9300 . ?
C93 C94 1.367(10) . ?
C93 H93 0.9300 . ?
C94 C95 1.349(10) . ?
C94 H94 0.9300 . ?
C95 C96 1.408(9) . ?
C95 H95 0.9300 . ?
C96 H96 0.9300 . ?
C97 C102 1.341(10) . ?
C97 C98 1.366(9) . ?
C98 C99 1.429(9) . ?
C98 H98 0.9300 . ?
C99 C100 1.360(9) . ?
C99 H99 0.9300 . ?
C100 C101 1.388(9) . ?
C100 H100 0.9300 . ?
C101 C102 1.320(9) . ?
C101 H101 0.9300 . ?
C102 H102 0.9300 . ?
C103 C104 1.399(8) . ?
C103 C108 1.412(8) . ?
C104 C105 1.286(11) . ?
C104 H104 0.9300 . ?
C105 C106 1.423(9) . ?
C105 H105 0.9300 . ?
C106 C107 1.317(12) . ?
C106 H106 0.9300 . ?
C107 C108 1.441(10) . ?
C107 H107 0.9300 . ?
C108 H108 0.9300 . ?
C109 C110 1.531(10) . ?
C109 H10A 0.9700 . ?
C109 H10B 0.9700 . ?
C110 C111 1.509(10) . ?
C110 H11A 0.9700 . ?
C110 H11B 0.9700 . ?
C111 C112 1.574(11) . ?
C111 H11C 0.9700 . ?
C111 H11D 0.9700 . ?
C112 C113 1.568(11) . ?
C112 H11E 0.9700 . ?
C112 H11F 0.9700 . ?
C113 H11G 0.9700 . ?
C113 H11H 0.9700 . ?
C114 C115 1.516(11) . ?
C114 H11I 0.9700 . ?
C114 H11J 0.9700 . ?
C115 C116 1.479(12) . ?
C115 H11K 0.9700 . ?
C115 H11L 0.9700 . ?
C116 C117 1.586(12) . ?
C116 H11M 0.9700 . ?
C116 H11N 0.9700 . ?
C117 C118 1.537(12) . ?
C117 H11O 0.9700 . ?
C117 H11P 0.9700 . ?
C118 H11Q 0.9700 . ?
C118 H11R 0.9700 . ?
C119 C120 1.449(12) . ?
C119 H11S 0.9700 . ?
C119 H11T 0.9700 . ?
C120 C121 1.498(13) . ?
C120 H12A 0.9700 . ?
C120 H12B 0.9700 . ?
C121 C122 1.560(11) . ?
C121 H12C 0.9700 . ?
C121 H12D 0.9700 . ?
C122 C123 1.488(10) . ?
C122 H12E 0.9700 . ?
C122 H12F 0.9700 . ?
C123 H12G 0.9700 . ?
C123 H12H 0.9700 . ?
C124 C125 1.535(8) . ?
C124 H12I 0.9700 . ?
C124 H12J 0.9700 . ?
C125 C126 1.471(8) . ?
C125 H12K 0.9700 . ?
C125 H12L 0.9700 . ?
C126 C127 1.566(10) . ?
C126 H12M 0.9700 . ?
C126 H12N 0.9700 . ?
C127 C128 1.497(9) . ?
C127 H12O 0.9700 . ?
C127 H12P 0.9700 . ?
C128 H12Q 0.9700 . ?
C128 H12R 0.9700 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Au1 Au11 167.51(4) . . ?
P1 Au1 Au9 119.02(5) . . ?
Au11 Au1 Au9 59.26(3) . . ?
P1 Au1 Au5 131.76(4) . . ?
Au11 Au1 Au5 56.906(13) . . ?
Au9 Au1 Au5 104.38(2) . . ?
P1 Au1 Au8 113.88(4) . . ?
Au11 Au1 Au8 56.449(11) . . ?
Au9 Au1 Au8 98.73(3) . . ?
Au5 Au1 Au8 76.49(3) . . ?
P1 Au1 Au2 138.88(4) . . ?
Au11 Au1 Au2 52.184(18) . . ?
Au9 Au1 Au2 56.352(9) . . ?
Au5 Au1 Au2 54.25(3) . . ?
Au8 Au1 Au2 106.993(12) . . ?
P2 Au2 Au11 174.39(4) . . ?
P2 Au2 Au5 116.14(5) . . ?
Au11 Au2 Au5 58.65(3) . . ?
P2 Au2 Au9 126.10(6) . . ?
Au11 Au2 Au9 59.19(3) . . ?
Au5 Au2 Au9 106.694(16) . . ?
P2 Au2 Au3 128.04(4) . . ?
Au11 Au2 Au3 55.418(10) . . ?
Au5 Au2 Au3 108.98(2) . . ?
Au9 Au2 Au3 57.046(11) . . ?
P2 Au2 Au1 127.18(5) . . ?
Au11 Au2 Au1 52.928(7) . . ?
Au5 Au2 Au1 57.607(8) . . ?
Au9 Au2 Au1 55.598(12) . . ?
Au3 Au2 Au1 97.972(11) . . ?
P2 Au2 Au6 125.32(5) . . ?
Au11 Au2 Au6 51.96(2) . . ?
Au5 Au2 Au6 67.77(4) . . ?
Au9 Au2 Au6 99.798(17) . . ?
Au3 Au2 Au6 52.825(13) . . ?
Au1 Au2 Au6 101.70(2) . . ?
P3 Au3 Au11 177.45(5) . . ?
P3 Au3 Au6 119.72(5) . . ?
Au11 Au3 Au6 57.746(19) . . ?
P3 Au3 Au9 123.11(6) . . ?
Au11 Au3 Au9 59.09(3) . . ?
Au6 Au3 Au9 112.83(2) . . ?
P3 Au3 Au2 125.64(4) . . ?
Au11 Au3 Au2 53.822(17) . . ?
Au6 Au3 Au2 67.90(2) . . ?
Au9 Au3 Au2 58.093(8) . . ?
P3 Au3 Au7 128.49(5) . . ?
Au11 Au3 Au7 51.070(16) . . ?
Au6 Au3 Au7 59.69(3) . . ?
Au9 Au3 Au7 95.61(3) . . ?
Au2 Au3 Au7 102.642(9) . . ?
P4 Au4 Au11 170.63(4) . . ?
P4 Au4 Au7 131.44(4) . . ?
Au11 Au4 Au7 56.947(8) . . ?
P4 Au4 Au9 111.72(5) . . ?
Au11 Au4 Au9 59.15(3) . . ?
Au7 Au4 Au9 106.46(3) . . ?
P4 Au4 Au8 126.46(4) . . ?
Au11 Au4 Au8 57.268(9) . . ?
Au7 Au4 Au8 71.85(3) . . ?
Au9 Au4 Au8 100.69(4) . . ?
P5 Au5 Au11 172.78(4) . . ?
P5 Au5 Au2 129.41(4) . . ?
Au11 Au5 Au2 57.296(8) . . ?
P5 Au5 Au10 113.59(6) . . ?
Au11 Au5 Au10 59.37(3) . . ?
Au2 Au5 Au10 109.06(4) . . ?
P5 Au5 Au1 126.52(4) . . ?
Au11 Au5 Au1 56.485(10) . . ?
Au2 Au5 Au1 68.14(3) . . ?
Au10 Au5 Au1 100.25(3) . . ?
P6 Au6 Au11 177.83(4) . . ?
P6 Au6 Au3 120.53(5) . . ?
Au11 Au6 Au3 57.963(11) . . ?
P6 Au6 Au10 123.00(5) . . ?
Au11 Au6 Au10 59.02(3) . . ?
Au3 Au6 Au10 112.65(3) . . ?
P6 Au6 Au7 127.52(5) . . ?
Au11 Au6 Au7 53.875(14) . . ?
Au3 Au6 Au7 67.25(3) . . ?
Au10 Au6 Au7 58.143(8) . . ?
P6 Au6 Au2 127.36(4) . . ?
Au11 Au6 Au2 50.712(8) . . ?
Au3 Au6 Au2 59.28(3) . . ?
Au10 Au6 Au2 96.06(4) . . ?
Au7 Au6 Au2 101.987(12) . . ?
P7 Au7 Au11 173.53(4) . . ?
P7 Au7 Au4 117.16(4) . . ?
Au11 Au7 Au4 58.40(2) . . ?
P7 Au7 Au10 127.41(5) . . ?
Au11 Au7 Au10 59.06(4) . . ?
Au4 Au7 Au10 103.86(2) . . ?
P7 Au7 Au6 126.62(4) . . ?
Au11 Au7 Au6 55.209(9) . . ?
Au4 Au7 Au6 110.03(2) . . ?
Au10 Au7 Au6 57.150(16) . . ?
P7 Au7 Au3 122.60(4) . . ?
Au11 Au7 Au3 52.45(2) . . ?
Au4 Au7 Au3 70.96(4) . . ?
Au10 Au7 Au3 100.32(2) . . ?
Au6 Au7 Au3 53.060(10) . . ?
P8 Au8 Au11 167.76(4) . . ?
P8 Au8 Au10 117.65(6) . . ?
Au11 Au8 Au10 59.17(3) . . ?
P8 Au8 Au4 132.45(5) . . ?
Au11 Au8 Au4 57.448(18) . . ?
Au10 Au8 Au4 103.69(2) . . ?
P8 Au8 Au1 115.69(5) . . ?
Au11 Au8 Au1 56.03(2) . . ?
Au10 Au8 Au1 99.06(2) . . ?
Au4 Au8 Au1 77.11(4) . . ?
Se1 Au9 Au11 166.951(19) . . ?
Se1 Au9 Au3 128.276(19) . . ?
Au11 Au9 Au3 57.375(14) . . ?
Se1 Au9 Au4 110.73(4) . . ?
Au11 Au9 Au4 57.17(3) . . ?
Au3 Au9 Au4 77.63(2) . . ?
Se1 Au9 Au1 119.26(3) . . ?
Au11 Au9 Au1 56.67(2) . . ?
Au3 Au9 Au1 112.47(3) . . ?
Au4 Au9 Au1 79.21(3) . . ?
Se1 Au9 Au2 136.382(18) . . ?
Au11 Au9 Au2 55.756(8) . . ?
Au3 Au9 Au2 64.861(11) . . ?
Au4 Au9 Au2 112.83(3) . . ?
Au1 Au9 Au2 68.050(12) . . ?
Se2 Au10 Au11 166.578(19) . . ?
Se2 Au10 Au5 110.71(4) . . ?
Au11 Au10 Au5 57.19(3) . . ?
Se2 Au10 Au8 117.98(2) . . ?
Au11 Au10 Au8 57.012(12) . . ?
Au5 Au10 Au8 79.49(2) . . ?
Se2 Au10 Au6 128.54(3) . . ?
Au11 Au10 Au6 57.11(3) . . ?
Au5 Au10 Au6 74.24(3) . . ?
Au8 Au10 Au6 113.31(3) . . ?
Se2 Au10 Au7 136.828(17) . . ?
Au11 Au10 Au7 55.706(10) . . ?
Au5 Au10 Au7 112.45(4) . . ?
Au8 Au10 Au7 71.439(14) . . ?
Au6 Au10 Au7 64.707(14) . . ?
Au2 Au11 Au7 141.741(17) . . ?
Au2 Au11 Au1 74.888(18) . . ?
Au7 Au11 Au1 142.448(12) . . ?
Au2 Au11 Au5 64.06(3) . . ?
Au7 Au11 Au5 128.07(3) . . ?
Au1 Au11 Au5 66.609(16) . . ?
Au2 Au11 Au8 139.062(15) . . ?
Au7 Au11 Au8 78.56(3) . . ?
Au1 Au11 Au8 67.52(3) . . ?
Au5 Au11 Au8 86.038(14) . . ?
Au2 Au11 Au4 128.61(3) . . ?
Au7 Au11 Au4 64.657(19) . . ?
Au1 Au11 Au4 86.176(12) . . ?
Au5 Au11 Au4 146.740(12) . . ?
Au8 Au11 Au4 65.285(16) . . ?
Au2 Au11 Au6 77.33(3) . . ?
Au7 Au11 Au6 70.916(14) . . ?
Au1 Au11 Au6 143.483(12) . . ?
Au5 Au11 Au6 80.141(12) . . ?
Au8 Au11 Au6 126.62(3) . . ?
Au4 Au11 Au6 130.052(11) . . ?
Au2 Au11 Au3 70.76(2) . . ?
Au7 Au11 Au3 76.48(3) . . ?
Au1 Au11 Au3 125.54(3) . . ?
Au5 Au11 Au3 127.246(11) . . ?
Au8 Au11 Au3 146.400(14) . . ?
Au4 Au11 Au3 83.743(12) . . ?
Au6 Au11 Au3 64.29(3) . . ?
Au2 Au11 Au10 118.23(3) . . ?
Au7 Au11 Au10 65.24(3) . . ?
Au1 Au11 Au10 110.375(19) . . ?
Au5 Au11 Au10 63.441(8) . . ?
Au8 Au11 Au10 63.82(3) . . ?
Au4 Au11 Au10 113.118(11) . . ?
Au6 Au11 Au10 63.872(12) . . ?
Au3 Au11 Au10 122.79(2) . . ?
Au2 Au11 Au9 65.05(3) . . ?
Au7 Au11 Au9 116.38(3) . . ?
Au1 Au11 Au9 64.069(16) . . ?
Au5 Au11 Au9 115.529(10) . . ?
Au8 Au11 Au9 109.66(3) . . ?
Au4 Au11 Au9 63.686(10) . . ?
Au6 Au11 Au9 122.874(12) . . ?
Au3 Au11 Au9 63.54(2) . . ?
Au10 Au11 Au9 173.223(12) . . ?
C109 P1 C1 107.5(3) . . ?
C109 P1 C7 106.1(2) . . ?
C1 P1 C7 99.1(3) . . ?
C109 P1 Au1 109.1(2) . . ?
C1 P1 Au1 119.6(2) . . ?
C7 P1 Au1 114.4(2) . . ?
C19 P2 C114 102.1(2) . . ?
C19 P2 C13 97.5(3) . . ?
C114 P2 C13 107.7(3) . . ?
C19 P2 Au2 108.6(2) . . ?
C114 P2 Au2 117.7(3) . . ?
C13 P2 Au2 119.8(2) . . ?
C31 P3 C119 122.4(3) . . ?
C31 P3 C25 110.7(3) . . ?
C119 P3 C25 104.5(3) . . ?
C31 P3 Au3 109.9(2) . . ?
C119 P3 Au3 102.3(2) . . ?
C25 P3 Au3 105.5(2) . . ?
C113 P4 C43 111.4(2) . . ?
C113 P4 C37 101.6(3) . . ?
C43 P4 C37 106.2(3) . . ?
C113 P4 Au4 112.3(2) . . ?
C43 P4 Au4 116.3(2) . . ?
C37 P4 Au4 107.8(3) . . ?
C49 P5 C55 96.8(2) . . ?
C49 P5 C124 111.08(18) . . ?
C55 P5 C124 105.0(2) . . ?
C49 P5 Au5 118.23(19) . . ?
C55 P5 Au5 117.3(2) . . ?
C124 P5 Au5 107.53(15) . . ?
C61 P6 C118 99.8(3) . . ?
C61 P6 C67 95.1(4) . . ?
C118 P6 C67 104.3(4) . . ?
C61 P6 Au6 119.8(2) . . ?
C118 P6 Au6 117.6(3) . . ?
C67 P6 Au6 116.6(2) . . ?
C79 P7 C73 103.3(3) . . ?
C79 P7 C123 91.3(3) . . ?
C73 P7 C123 115.5(3) . . ?
C79 P7 Au7 115.9(3) . . ?
C73 P7 Au7 116.85(17) . . ?
C123 P7 Au7 111.1(2) . . ?
C85 P8 C91 97.6(3) . . ?
C85 P8 C128 101.9(3) . . ?
C91 P8 C128 114.6(3) . . ?
C85 P8 Au8 122.5(2) . . ?
C91 P8 Au8 112.66(19) . . ?
C128 P8 Au8 107.4(2) . . ?
F3 Sb1 F6 81.3(3) . . ?
F3 Sb1 F4 91.5(3) . . ?
F6 Sb1 F4 96.7(2) . . ?
F3 Sb1 F5 99.2(3) . . ?
F6 Sb1 F5 179.5(3) . . ?
F4 Sb1 F5 83.2(2) . . ?
F3 Sb1 F1 177.8(3) . . ?
F6 Sb1 F1 98.4(3) . . ?
F4 Sb1 F1 90.7(2) . . ?
F5 Sb1 F1 81.1(3) . . ?
F3 Sb1 F2 89.9(3) . . ?
F6 Sb1 F2 83.2(2) . . ?
F4 Sb1 F2 178.7(3) . . ?
F5 Sb1 F2 96.9(2) . . ?
F1 Sb1 F2 87.9(3) . . ?
C97 Se1 Au9 108.54(16) . . ?
C103 Se2 Au10 111.07(16) . . ?
C6 C1 C2 119.8(6) . . ?
C6 C1 P1 119.6(5) . . ?
C2 C1 P1 120.5(5) . . ?
C1 C2 C3 122.4(6) . . ?
C1 C2 H2 118.8 . . ?
C3 C2 H2 118.8 . . ?
C2 C3 C4 117.7(6) . . ?
C2 C3 H3 121.2 . . ?
C4 C3 H3 121.2 . . ?
C5 C4 C3 118.2(6) . . ?
C5 C4 H4 120.9 . . ?
C3 C4 H4 120.9 . . ?
C4 C5 C6 119.0(6) . . ?
C4 C5 H5 120.5 . . ?
C6 C5 H5 120.5 . . ?
C1 C6 C5 122.9(6) . . ?
C1 C6 H6 118.6 . . ?
C5 C6 H6 118.6 . . ?
C8 C7 C12 120.5(7) . . ?
C8 C7 P1 119.3(5) . . ?
C12 C7 P1 120.1(6) . . ?
C7 C8 C9 119.5(7) . . ?
C7 C8 H8 120.3 . . ?
C9 C8 H8 120.3 . . ?
C10 C9 C8 120.6(6) . . ?
C10 C9 H9 119.7 . . ?
C8 C9 H9 119.7 . . ?
C11 C10 C9 119.8(6) . . ?
C11 C10 H10 120.1 . . ?
C9 C10 H10 120.1 . . ?
C10 C11 C12 121.0(5) . . ?
C10 C11 H11 119.5 . . ?
C12 C11 H11 119.5 . . ?
C11 C12 C7 118.6(6) . . ?
C11 C12 H12 120.7 . . ?
C7 C12 H12 120.7 . . ?
C18 C13 C14 121.0(6) . . ?
C18 C13 P2 120.1(5) . . ?
C14 C13 P2 118.9(5) . . ?
C13 C14 C15 119.3(6) . . ?
C13 C14 H14 120.4 . . ?
C15 C14 H14 120.4 . . ?
C16 C15 C14 118.8(7) . . ?
C16 C15 H15 120.6 . . ?
C14 C15 H15 120.6 . . ?
C15 C16 C17 122.0(6) . . ?
C15 C16 H16 119.0 . . ?
C17 C16 H16 119.0 . . ?
C18 C17 C16 116.2(5) . . ?
C18 C17 H17 121.9 . . ?
C16 C17 H17 121.9 . . ?
C13 C18 C17 122.5(5) . . ?
C13 C18 H18 118.8 . . ?
C17 C18 H18 118.8 . . ?
C24 C19 C20 117.3(6) . . ?
C24 C19 P2 123.0(5) . . ?
C20 C19 P2 119.6(5) . . ?
C21 C20 C19 121.9(5) . . ?
C21 C20 H20 119.0 . . ?
C19 C20 H20 119.0 . . ?
C20 C21 C22 117.6(6) . . ?
C20 C21 H21 121.2 . . ?
C22 C21 H21 121.2 . . ?
C23 C22 C21 121.5(6) . . ?
C23 C22 H22 119.2 . . ?
C21 C22 H22 119.2 . . ?
C22 C23 C24 120.5(7) . . ?
C22 C23 H23 119.7 . . ?
C24 C23 H23 119.7 . . ?
C23 C24 C19 121.0(7) . . ?
C23 C24 H24 119.5 . . ?
C19 C24 H24 119.5 . . ?
C30 C25 C26 121.0(7) . . ?
C30 C25 P3 120.0(6) . . ?
C26 C25 P3 118.7(5) . . ?
C27 C26 C25 115.3(6) . . ?
C27 C26 H26 122.3 . . ?
C25 C26 H26 122.3 . . ?
C28 C27 C26 121.1(8) . . ?
C28 C27 H27 119.4 . . ?
C26 C27 H27 119.4 . . ?
C27 C28 C29 124.8(7) . . ?
C27 C28 H28 117.6 . . ?
C29 C28 H28 117.6 . . ?
C30 C29 C28 116.7(6) . . ?
C30 C29 H29 121.6 . . ?
C28 C29 H29 121.6 . . ?
C29 C30 C25 120.5(7) . . ?
C29 C30 H30 119.7 . . ?
C25 C30 H30 119.7 . . ?
C36 C31 C32 117.5(7) . . ?
C36 C31 P3 121.0(6) . . ?
C32 C31 P3 121.3(5) . . ?
C33 C32 C31 118.8(7) . . ?
C33 C32 H32 120.6 . . ?
C31 C32 H32 120.6 . . ?
C32 C33 C34 122.1(8) . . ?
C32 C33 H33 118.9 . . ?
C34 C33 H33 118.9 . . ?
C35 C34 C33 121.1(7) . . ?
C35 C34 H34 119.4 . . ?
C33 C34 H34 119.4 . . ?
C34 C35 C36 121.6(6) . . ?
C34 C35 H35 119.2 . . ?
C36 C35 H35 119.2 . . ?
C35 C36 C31 118.5(7) . . ?
C35 C36 H36 120.7 . . ?
C31 C36 H36 120.7 . . ?
C38 C37 C42 117.9(7) . . ?
C38 C37 P4 123.2(6) . . ?
C42 C37 P4 118.9(6) . . ?
C37 C38 C39 123.1(7) . . ?
C37 C38 H38 118.5 . . ?
C39 C38 H38 118.5 . . ?
C38 C39 C40 120.7(7) . . ?
C38 C39 H39 119.6 . . ?
C40 C39 H39 119.6 . . ?
C41 C40 C39 115.6(6) . . ?
C41 C40 H40 122.2 . . ?
C39 C40 H40 122.2 . . ?
C40 C41 C42 125.2(7) . . ?
C40 C41 H41 117.4 . . ?
C42 C41 H41 117.4 . . ?
C41 C42 C37 117.3(7) . . ?
C41 C42 H42 121.4 . . ?
C37 C42 H42 121.4 . . ?
C48 C43 C44 121.2(6) . . ?
C48 C43 P4 120.6(5) . . ?
C44 C43 P4 118.0(5) . . ?
C45 C44 C43 118.0(7) . . ?
C45 C44 H44 121.0 . . ?
C43 C44 H44 121.0 . . ?
C44 C45 C46 123.3(6) . . ?
C44 C45 H45 118.3 . . ?
C46 C45 H45 118.3 . . ?
C45 C46 C47 119.1(7) . . ?
C45 C46 H46 120.4 . . ?
C47 C46 H46 120.4 . . ?
C48 C47 C46 115.6(6) . . ?
C48 C47 H47 122.2 . . ?
C46 C47 H47 122.2 . . ?
C43 C48 C47 122.5(6) . . ?
C43 C48 H48 118.8 . . ?
C47 C48 H48 118.8 . . ?
C54 C49 C50 118.2(5) . . ?
C54 C49 P5 121.0(4) . . ?
C50 C49 P5 120.5(4) . . ?
C51 C50 C49 120.3(4) . . ?
C51 C50 H50 119.9 . . ?
C49 C50 H50 119.9 . . ?
C50 C51 C52 120.9(6) . . ?
C50 C51 H51 119.6 . . ?
C52 C51 H51 119.6 . . ?
C53 C52 C51 119.0(7) . . ?
C53 C52 H52 120.5 . . ?
C51 C52 H52 120.5 . . ?
C54 C53 C52 119.4(6) . . ?
C54 C53 H53 120.3 . . ?
C52 C53 H53 120.3 . . ?
C49 C54 C53 121.3(5) . . ?
C49 C54 H54 119.4 . . ?
C53 C54 H54 119.4 . . ?
C60 C55 C56 118.5(6) . . ?
C60 C55 P5 120.8(5) . . ?
C56 C55 P5 120.5(6) . . ?
C57 C56 C55 121.3(8) . . ?
C57 C56 H56 119.4 . . ?
C55 C56 H56 119.4 . . ?
C56 C57 C58 121.1(8) . . ?
C56 C57 H57 119.4 . . ?
C58 C57 H57 119.4 . . ?
C59 C58 C57 114.6(7) . . ?
C59 C58 H58 122.7 . . ?
C57 C58 H58 122.7 . . ?
C58 C59 C60 123.8(9) . . ?
C58 C59 H59 118.1 . . ?
C60 C59 H59 118.1 . . ?
C55 C60 C59 120.4(7) . . ?
C55 C60 H60 119.8 . . ?
C59 C60 H60 119.8 . . ?
C62 C61 C66 119.6(6) . . ?
C62 C61 P6 121.2(5) . . ?
C66 C61 P6 119.2(5) . . ?
C63 C62 C61 120.4(6) . . ?
C63 C62 H62 119.8 . . ?
C61 C62 H62 119.8 . . ?
C62 C63 C64 120.4(6) . . ?
C62 C63 H63 119.8 . . ?
C64 C63 H63 119.8 . . ?
C63 C64 C65 119.4(7) . . ?
C63 C64 H64 120.3 . . ?
C65 C64 H64 120.3 . . ?
C66 C65 C64 120.2(7) . . ?
C66 C65 H65 119.9 . . ?
C64 C65 H65 119.9 . . ?
C65 C66 C61 119.8(5) . . ?
C65 C66 H66 120.1 . . ?
C61 C66 H66 120.1 . . ?
C68 C67 C72 120.8(8) . . ?
C68 C67 P6 119.1(8) . . ?
C72 C67 P6 120.1(5) . . ?
C67 C68 C69 119.6(8) . . ?
C67 C68 H68 120.2 . . ?
C69 C68 H68 120.2 . . ?
C70 C69 C68 119.5(7) . . ?
C70 C69 H69 120.3 . . ?
C68 C69 H69 120.3 . . ?
C71 C70 C69 120.0(9) . . ?
C71 C70 H70 120.0 . . ?
C69 C70 H70 120.0 . . ?
C72 C71 C70 119.9(9) . . ?
C72 C71 H71 120.0 . . ?
C70 C71 H71 120.0 . . ?
C67 C72 C71 120.2(8) . . ?
C67 C72 H72 119.9 . . ?
C71 C72 H72 119.9 . . ?
C74 C73 C78 121.7(6) . . ?
C74 C73 P7 118.2(4) . . ?
C78 C73 P7 120.1(5) . . ?
C73 C74 C75 119.4(6) . . ?
C73 C74 H74 120.3 . . ?
C75 C74 H74 120.3 . . ?
C74 C75 C76 119.1(6) . . ?
C74 C75 H75 120.5 . . ?
C76 C75 H75 120.5 . . ?
C77 C76 C75 120.1(6) . . ?
C77 C76 H76 119.9 . . ?
C75 C76 H76 119.9 . . ?
C76 C77 C78 120.3(7) . . ?
C76 C77 H77 119.8 . . ?
C78 C77 H77 119.8 . . ?
C73 C78 C77 119.3(7) . . ?
C73 C78 H78 120.4 . . ?
C77 C78 H78 120.4 . . ?
C80 C79 C84 118.4(6) . . ?
C80 C79 P7 118.2(6) . . ?
C84 C79 P7 123.2(5) . . ?
C79 C80 C81 120.7(7) . . ?
C79 C80 H80 119.7 . . ?
C81 C80 H80 119.7 . . ?
C82 C81 C80 120.3(7) . . ?
C82 C81 H81 119.9 . . ?
C80 C81 H81 119.9 . . ?
C81 C82 C83 122.2(6) . . ?
C81 C82 H82 118.9 . . ?
C83 C82 H82 118.9 . . ?
C82 C83 C84 118.0(6) . . ?
C82 C83 H83 121.0 . . ?
C84 C83 H83 121.0 . . ?
C83 C84 C79 120.4(6) . . ?
C83 C84 H84 119.8 . . ?
C79 C84 H84 119.8 . . ?
C90 C85 C86 119.9(6) . . ?
C90 C85 P8 119.8(6) . . ?
C86 C85 P8 120.2(4) . . ?
C87 C86 C85 119.9(6) . . ?
C87 C86 H86 120.1 . . ?
C85 C86 H86 120.1 . . ?
C86 C87 C88 119.1(8) . . ?
C86 C87 H87 120.4 . . ?
C88 C87 H87 120.4 . . ?
C89 C88 C87 120.4(7) . . ?
C89 C88 H88 119.8 . . ?
C87 C88 H88 119.8 . . ?
C88 C89 C90 120.9(7) . . ?
C88 C89 H89 119.6 . . ?
C90 C89 H89 119.6 . . ?
C89 C90 C85 119.8(7) . . ?
C89 C90 H90 120.1 . . ?
C85 C90 H90 120.1 . . ?
C96 C91 C92 122.6(6) . . ?
C96 C91 P8 118.5(5) . . ?
C92 C91 P8 118.7(6) . . ?
C93 C92 C91 115.1(7) . . ?
C93 C92 H92 122.5 . . ?
C91 C92 H92 122.5 . . ?
C94 C93 C92 123.8(8) . . ?
C94 C93 H93 118.1 . . ?
C92 C93 H93 118.1 . . ?
C95 C94 C93 118.8(6) . . ?
C95 C94 H94 120.6 . . ?
C93 C94 H94 120.6 . . ?
C94 C95 C96 121.4(7) . . ?
C94 C95 H95 119.3 . . ?
C96 C95 H95 119.3 . . ?
C91 C96 C95 118.0(7) . . ?
C91 C96 H96 121.0 . . ?
C95 C96 H96 121.0 . . ?
C102 C97 C98 123.6(6) . . ?
C102 C97 Se1 120.3(5) . . ?
C98 C97 Se1 116.0(5) . . ?
C97 C98 C99 114.9(6) . . ?
C97 C98 H98 122.5 . . ?
C99 C98 H98 122.5 . . ?
C100 C99 C98 119.9(5) . . ?
C100 C99 H99 120.1 . . ?
C98 C99 H99 120.1 . . ?
C99 C100 C101 121.0(6) . . ?
C99 C100 H100 119.5 . . ?
C101 C100 H100 119.5 . . ?
C102 C101 C100 118.5(7) . . ?
C102 C101 H101 120.7 . . ?
C100 C101 H101 120.7 . . ?
C101 C102 C97 121.6(7) . . ?
C101 C102 H102 119.2 . . ?
C97 C102 H102 119.2 . . ?
C104 C103 C108 117.9(5) . . ?
C104 C103 Se2 122.6(4) . . ?
C108 C103 Se2 119.5(4) . . ?
C105 C104 C103 123.6(6) . . ?
C105 C104 H104 118.2 . . ?
C103 C104 H104 118.2 . . ?
C104 C105 C106 119.3(7) . . ?
C104 C105 H105 120.4 . . ?
C106 C105 H105 120.4 . . ?
C107 C106 C105 120.4(7) . . ?
C107 C106 H106 119.8 . . ?
C105 C106 H106 119.8 . . ?
C106 C107 C108 121.0(6) . . ?
C106 C107 H107 119.5 . . ?
C108 C107 H107 119.5 . . ?
C103 C108 C107 117.0(6) . . ?
C103 C108 H108 121.5 . . ?
C107 C108 H108 121.5 . . ?
C110 C109 P1 104.9(4) . . ?
C110 C109 H10A 110.8 . . ?
P1 C109 H10A 110.8 . . ?
C110 C109 H10B 110.8 . . ?
P1 C109 H10B 110.8 . . ?
H10A C109 H10B 108.8 . . ?
C111 C110 C109 107.8(7) . . ?
C111 C110 H11A 110.1 . . ?
C109 C110 H11A 110.1 . . ?
C111 C110 H11B 110.1 . . ?
C109 C110 H11B 110.1 . . ?
H11A C110 H11B 108.5 . . ?
C110 C111 C112 114.9(6) . . ?
C110 C111 H11C 108.6 . . ?
C112 C111 H11C 108.6 . . ?
C110 C111 H11D 108.6 . . ?
C112 C111 H11D 108.6 . . ?
H11C C111 H11D 107.5 . . ?
C113 C112 C111 114.1(6) . . ?
C113 C112 H11E 108.7 . . ?
C111 C112 H11E 108.7 . . ?
C113 C112 H11F 108.7 . . ?
C111 C112 H11F 108.7 . . ?
H11E C112 H11F 107.6 . . ?
C112 C113 P4 106.1(5) . . ?
C112 C113 H11G 110.5 . . ?
P4 C113 H11G 110.5 . . ?
C112 C113 H11H 110.5 . . ?
P4 C113 H11H 110.5 . . ?
H11G C113 H11H 108.7 . . ?
C115 C114 P2 109.4(6) . . ?
C115 C114 H11I 109.8 . . ?
P2 C114 H11I 109.8 . . ?
C115 C114 H11J 109.8 . . ?
P2 C114 H11J 109.8 . . ?
H11I C114 H11J 108.2 . . ?
C116 C115 C114 113.9(6) . . ?
C116 C115 H11K 108.8 . . ?
C114 C115 H11K 108.8 . . ?
C116 C115 H11L 108.8 . . ?
C114 C115 H11L 108.8 . . ?
H11K C115 H11L 107.7 . . ?
C115 C116 C117 116.0(7) . . ?
C115 C116 H11M 108.3 . . ?
C117 C116 H11M 108.3 . . ?
C115 C116 H11N 108.3 . . ?
C117 C116 H11N 108.3 . . ?
H11M C116 H11N 107.4 . . ?
C118 C117 C116 107.7(5) . . ?
C118 C117 H11O 110.2 . . ?
C116 C117 H11O 110.2 . . ?
C118 C117 H11P 110.2 . . ?
C116 C117 H11P 110.2 . . ?
H11O C117 H11P 108.5 . . ?
C117 C118 P6 107.0(5) . . ?
C117 C118 H11Q 110.3 . . ?
P6 C118 H11Q 110.3 . . ?
C117 C118 H11R 110.3 . . ?
P6 C118 H11R 110.3 . . ?
H11Q C118 H11R 108.6 . . ?
C120 C119 P3 116.5(6) . . ?
C120 C119 H11S 108.2 . . ?
P3 C119 H11S 108.2 . . ?
C120 C119 H11T 108.2 . . ?
P3 C119 H11T 108.2 . . ?
H11S C119 H11T 107.3 . . ?
C119 C120 C121 109.0(9) . . ?
C119 C120 H12A 109.4 . . ?
C121 C120 H12A 103.0 . . ?
C119 C120 H12B 115.2 . . ?
C121 C120 H12B 110.3 . . ?
H12A C120 H12B 109.3 . . ?
C120 C121 C122 106.5(10) . . ?
C120 C121 H12C 110.4 . . ?
C122 C121 H12C 110.4 . . ?
C120 C121 H12D 110.4 . . ?
C122 C121 H12D 110.4 . . ?
H12C C121 H12D 108.6 . . ?
C123 C122 C121 113.7(7) . . ?
C123 C122 H12E 105.6 . . ?
C121 C122 H12E 100.0 . . ?
C123 C122 H12F 116.1 . . ?
C121 C122 H12F 111.5 . . ?
H12E C122 H12F 108.3 . . ?
C122 C123 P7 106.3(4) . . ?
C122 C123 H12G 110.5 . . ?
P7 C123 H12G 110.5 . . ?
C122 C123 H12H 110.5 . . ?
P7 C123 H12H 110.5 . . ?
H12G C123 H12H 108.7 . . ?
C125 C124 P5 105.7(4) . . ?
C125 C124 H12I 110.6 . . ?
P5 C124 H12I 110.6 . . ?
C125 C124 H12J 110.6 . . ?
P5 C124 H12J 110.6 . . ?
H12I C124 H12J 108.7 . . ?
C126 C125 C124 117.2(6) . . ?
C126 C125 H12K 108.0 . . ?
C124 C125 H12K 108.0 . . ?
C126 C125 H12L 108.0 . . ?
C124 C125 H12L 108.0 . . ?
H12K C125 H12L 107.2 . . ?
C125 C126 C127 100.8(6) . . ?
C125 C126 H12M 111.6 . . ?
C127 C126 H12M 111.6 . . ?
C125 C126 H12N 111.6 . . ?
C127 C126 H12N 111.6 . . ?
H12M C126 H12N 109.4 . . ?
C128 C127 C126 108.8(6) . . ?
C128 C127 H12O 109.9 . . ?
C126 C127 H12O 109.9 . . ?
C128 C127 H12P 109.9 . . ?
C126 C127 H12P 109.9 . . ?
H12O C127 H12P 108.3 . . ?
C127 C128 P8 114.5(4) . . ?
C127 C128 H12Q 108.6 . . ?
P8 C128 H12Q 108.6 . . ?
C127 C128 H12R 108.6 . . ?
P8 C128 H12R 108.6 . . ?
H12Q C128 H12R 107.6 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C109 P1 C1 C6 85.8(6) . . . . ?
C7 P1 C1 C6 -24.3(6) . . . . ?
Au1 P1 C1 C6 -149.2(5) . . . . ?
C109 P1 C1 C2 -90.0(5) . . . . ?
C7 P1 C1 C2 159.9(5) . . . . ?
Au1 P1 C1 C2 35.0(6) . . . . ?
C6 C1 C2 C3 -0.1(9) . . . . ?
P1 C1 C2 C3 175.7(4) . . . . ?
C1 C2 C3 C4 2.6(9) . . . . ?
C2 C3 C4 C5 -4.0(11) . . . . ?
C3 C4 C5 C6 3.0(11) . . . . ?
C2 C1 C6 C5 -1.0(11) . . . . ?
P1 C1 C6 C5 -176.9(5) . . . . ?
C4 C5 C6 C1 -0.5(11) . . . . ?
C109 P1 C7 C8 -178.0(5) . . . . ?
C1 P1 C7 C8 -66.7(6) . . . . ?
Au1 P1 C7 C8 61.7(6) . . . . ?
C109 P1 C7 C12 2.1(6) . . . . ?
C1 P1 C7 C12 113.4(6) . . . . ?
Au1 P1 C7 C12 -118.2(5) . . . . ?
C12 C7 C8 C9 -0.1(11) . . . . ?
P1 C7 C8 C9 180.0(6) . . . . ?
C7 C8 C9 C10 1.5(12) . . . . ?
C8 C9 C10 C11 -1.9(12) . . . . ?
C9 C10 C11 C12 0.9(12) . . . . ?
C10 C11 C12 C7 0.5(10) . . . . ?
C8 C7 C12 C11 -0.9(10) . . . . ?
P1 C7 C12 C11 179.1(5) . . . . ?
C19 P2 C13 C18 -50.1(5) . . . . ?
C114 P2 C13 C18 55.2(5) . . . . ?
Au2 P2 C13 C18 -166.5(4) . . . . ?
C19 P2 C13 C14 128.1(6) . . . . ?
C114 P2 C13 C14 -126.6(6) . . . . ?
Au2 P2 C13 C14 11.7(7) . . . . ?
C18 C13 C14 C15 0.5(12) . . . . ?
P2 C13 C14 C15 -177.7(6) . . . . ?
C13 C14 C15 C16 -1.5(13) . . . . ?
C14 C15 C16 C17 -1.4(12) . . . . ?
C15 C16 C17 C18 5.1(11) . . . . ?
C14 C13 C18 C17 3.5(10) . . . . ?
P2 C13 C18 C17 -178.3(5) . . . . ?
C16 C17 C18 C13 -6.1(10) . . . . ?
C114 P2 C19 C24 159.2(7) . . . . ?
C13 P2 C19 C24 -90.9(8) . . . . ?
Au2 P2 C19 C24 34.1(8) . . . . ?
C114 P2 C19 C20 -24.7(7) . . . . ?
C13 P2 C19 C20 85.3(7) . . . . ?
Au2 P2 C19 C20 -149.8(6) . . . . ?
C24 C19 C20 C21 -1.6(12) . . . . ?
P2 C19 C20 C21 -178.0(5) . . . . ?
C19 C20 C21 C22 1.1(10) . . . . ?
C20 C21 C22 C23 -2.4(11) . . . . ?
C21 C22 C23 C24 4.2(13) . . . . ?
C22 C23 C24 C19 -4.7(14) . . . . ?
C20 C19 C24 C23 3.4(13) . . . . ?
P2 C19 C24 C23 179.6(7) . . . . ?
C31 P3 C25 C30 -126.7(7) . . . . ?
C119 P3 C25 C30 6.9(7) . . . . ?
Au3 P3 C25 C30 114.4(6) . . . . ?
C31 P3 C25 C26 59.5(7) . . . . ?
C119 P3 C25 C26 -166.9(5) . . . . ?
Au3 P3 C25 C26 -59.4(6) . . . . ?
C30 C25 C26 C27 7.0(11) . . . . ?
P3 C25 C26 C27 -179.2(5) . . . . ?
C25 C26 C27 C28 -4.9(11) . . . . ?
C26 C27 C28 C29 -1.0(12) . . . . ?
C27 C28 C29 C30 4.9(12) . . . . ?
C28 C29 C30 C25 -2.5(11) . . . . ?
C26 C25 C30 C29 -3.4(12) . . . . ?
P3 C25 C30 C29 -177.0(6) . . . . ?
C119 P3 C31 C36 -76.1(6) . . . . ?
C25 P3 C31 C36 47.8(8) . . . . ?
Au3 P3 C31 C36 164.1(5) . . . . ?
C119 P3 C31 C32 98.8(7) . . . . ?
C25 P3 C31 C32 -137.3(7) . . . . ?
Au3 P3 C31 C32 -21.1(8) . . . . ?
C36 C31 C32 C33 -3.9(12) . . . . ?
P3 C31 C32 C33 -179.0(7) . . . . ?
C31 C32 C33 C34 2.5(12) . . . . ?
C32 C33 C34 C35 -3.5(12) . . . . ?
C33 C34 C35 C36 6.0(12) . . . . ?
C34 C35 C36 C31 -7.5(11) . . . . ?
C32 C31 C36 C35 6.3(11) . . . . ?
P3 C31 C36 C35 -178.7(6) . . . . ?
C113 P4 C37 C38 64.0(8) . . . . ?
C43 P4 C37 C38 -179.4(7) . . . . ?
Au4 P4 C37 C38 -54.1(9) . . . . ?
C113 P4 C37 C42 -115.4(7) . . . . ?
C43 P4 C37 C42 1.2(8) . . . . ?
Au4 P4 C37 C42 126.5(7) . . . . ?
C42 C37 C38 C39 2.7(13) . . . . ?
P4 C37 C38 C39 -176.7(7) . . . . ?
C37 C38 C39 C40 -3.8(12) . . . . ?
C38 C39 C40 C41 0.4(11) . . . . ?
C39 C40 C41 C42 4.2(14) . . . . ?
C40 C41 C42 C37 -5.2(15) . . . . ?
C38 C37 C42 C41 1.6(13) . . . . ?
P4 C37 C42 C41 -178.9(8) . . . . ?
C113 P4 C43 C48 25.2(6) . . . . ?
C37 P4 C43 C48 -84.6(7) . . . . ?
Au4 P4 C43 C48 155.6(5) . . . . ?
C113 P4 C43 C44 -151.2(4) . . . . ?
C37 P4 C43 C44 99.0(6) . . . . ?
Au4 P4 C43 C44 -20.8(5) . . . . ?
C48 C43 C44 C45 3.0(9) . . . . ?
P4 C43 C44 C45 179.3(5) . . . . ?
C43 C44 C45 C46 -2.6(9) . . . . ?
C44 C45 C46 C47 3.4(9) . . . . ?
C45 C46 C47 C48 -4.3(9) . . . . ?
C44 C43 C48 C47 -4.4(11) . . . . ?
P4 C43 C48 C47 179.3(6) . . . . ?
C46 C47 C48 C43 4.9(11) . . . . ?
C55 P5 C49 C54 -50.5(4) . . . . ?
C124 P5 C49 C54 58.6(4) . . . . ?
Au5 P5 C49 C54 -176.5(4) . . . . ?
C55 P5 C49 C50 123.2(4) . . . . ?
C124 P5 C49 C50 -127.7(4) . . . . ?
Au5 P5 C49 C50 -2.8(5) . . . . ?
C54 C49 C50 C51 -4.6(7) . . . . ?
P5 C49 C50 C51 -178.5(4) . . . . ?
C49 C50 C51 C52 0.9(8) . . . . ?
C50 C51 C52 C53 -2.5(12) . . . . ?
C51 C52 C53 C54 7.9(13) . . . . ?
C50 C49 C54 C53 10.2(9) . . . . ?
P5 C49 C54 C53 -175.9(6) . . . . ?
C52 C53 C54 C49 -12.0(13) . . . . ?
C49 P5 C55 C60 -9.0(5) . . . . ?
C124 P5 C55 C60 -123.0(5) . . . . ?
Au5 P5 C55 C60 117.7(5) . . . . ?
C49 P5 C55 C56 175.9(5) . . . . ?
C124 P5 C55 C56 61.9(5) . . . . ?
Au5 P5 C55 C56 -57.4(5) . . . . ?
C60 C55 C56 C57 5.7(10) . . . . ?
P5 C55 C56 C57 -179.1(6) . . . . ?
C55 C56 C57 C58 -5.9(11) . . . . ?
C56 C57 C58 C59 3.6(10) . . . . ?
C57 C58 C59 C60 -1.4(12) . . . . ?
C56 C55 C60 C59 -3.4(11) . . . . ?
P5 C55 C60 C59 -178.6(6) . . . . ?
C58 C59 C60 C55 1.4(13) . . . . ?
C118 P6 C61 C62 117.4(7) . . . . ?
C67 P6 C61 C62 -137.1(7) . . . . ?
Au6 P6 C61 C62 -12.4(8) . . . . ?
C118 P6 C61 C66 -65.0(7) . . . . ?
C67 P6 C61 C66 40.4(7) . . . . ?
Au6 P6 C61 C66 165.1(5) . . . . ?
C66 C61 C62 C63 3.1(13) . . . . ?
P6 C61 C62 C63 -179.4(7) . . . . ?
C61 C62 C63 C64 -4.1(15) . . . . ?
C62 C63 C64 C65 3.2(17) . . . . ?
C63 C64 C65 C66 -1.4(16) . . . . ?
C64 C65 C66 C61 0.5(14) . . . . ?
C62 C61 C66 C65 -1.4(12) . . . . ?
P6 C61 C66 C65 -178.9(7) . . . . ?
C61 P6 C67 C68 -102.3(8) . . . . ?
C118 P6 C67 C68 -0.9(9) . . . . ?
Au6 P6 C67 C68 130.5(7) . . . . ?
C61 P6 C67 C72 76.7(7) . . . . ?
C118 P6 C67 C72 178.1(7) . . . . ?
Au6 P6 C67 C72 -50.4(8) . . . . ?
C72 C67 C68 C69 -0.7(15) . . . . ?
P6 C67 C68 C69 178.3(7) . . . . ?
C67 C68 C69 C70 1.1(15) . . . . ?
C68 C69 C70 C71 -1.7(15) . . . . ?
C69 C70 C71 C72 2.0(15) . . . . ?
C68 C67 C72 C71 1.0(14) . . . . ?
P6 C67 C72 C71 -178.0(8) . . . . ?
C70 C71 C72 C67 -1.6(15) . . . . ?
C79 P7 C73 C74 -84.9(6) . . . . ?
C123 P7 C73 C74 177.2(5) . . . . ?
Au7 P7 C73 C74 43.7(6) . . . . ?
C79 P7 C73 C78 94.7(5) . . . . ?
C123 P7 C73 C78 -3.3(5) . . . . ?
Au7 P7 C73 C78 -136.8(4) . . . . ?
C78 C73 C74 C75 0.5(11) . . . . ?
P7 C73 C74 C75 -180.0(6) . . . . ?
C73 C74 C75 C76 -0.4(13) . . . . ?
C74 C75 C76 C77 -0.5(14) . . . . ?
C75 C76 C77 C78 1.4(14) . . . . ?
C74 C73 C78 C77 0.4(10) . . . . ?
P7 C73 C78 C77 -179.1(5) . . . . ?
C76 C77 C78 C73 -1.4(12) . . . . ?
C73 P7 C79 C80 -41.6(6) . . . . ?
C123 P7 C79 C80 75.0(6) . . . . ?
Au7 P7 C79 C80 -170.7(4) . . . . ?
C73 P7 C79 C84 133.3(6) . . . . ?
C123 P7 C79 C84 -110.0(6) . . . . ?
Au7 P7 C79 C84 4.2(7) . . . . ?
C84 C79 C80 C81 -0.8(9) . . . . ?
P7 C79 C80 C81 174.4(5) . . . . ?
C79 C80 C81 C82 -0.2(10) . . . . ?
C80 C81 C82 C83 2.5(12) . . . . ?
C81 C82 C83 C84 -3.7(11) . . . . ?
C82 C83 C84 C79 2.6(9) . . . . ?
C80 C79 C84 C83 -0.4(9) . . . . ?
P7 C79 C84 C83 -175.4(5) . . . . ?
C91 P8 C85 C90 -34.8(5) . . . . ?
C128 P8 C85 C90 82.4(5) . . . . ?
Au8 P8 C85 C90 -157.8(4) . . . . ?
C91 P8 C85 C86 144.6(5) . . . . ?
C128 P8 C85 C86 -98.3(5) . . . . ?
Au8 P8 C85 C86 21.6(6) . . . . ?
C90 C85 C86 C87 -0.1(10) . . . . ?
P8 C85 C86 C87 -179.5(6) . . . . ?
C85 C86 C87 C88 -0.7(11) . . . . ?
C86 C87 C88 C89 0.8(11) . . . . ?
C87 C88 C89 C90 -0.1(11) . . . . ?
C88 C89 C90 C85 -0.8(11) . . . . ?
C86 C85 C90 C89 0.9(10) . . . . ?
P8 C85 C90 C89 -179.7(5) . . . . ?
C85 P8 C91 C96 112.3(6) . . . . ?
C128 P8 C91 C96 5.5(6) . . . . ?
Au8 P8 C91 C96 -117.8(5) . . . . ?
C85 P8 C91 C92 -62.1(5) . . . . ?
C128 P8 C91 C92 -168.9(5) . . . . ?
Au8 P8 C91 C92 67.8(5) . . . . ?
C96 C91 C92 C93 7.2(10) . . . . ?
P8 C91 C92 C93 -178.6(5) . . . . ?
C91 C92 C93 C94 -3.8(11) . . . . ?
C92 C93 C94 C95 0.4(12) . . . . ?
C93 C94 C95 C96 0.1(11) . . . . ?
C92 C91 C96 C95 -7.0(11) . . . . ?
P8 C91 C96 C95 178.8(5) . . . . ?
C94 C95 C96 C91 3.2(11) . . . . ?
Au9 Se1 C97 C102 -32.1(6) . . . . ?
Au9 Se1 C97 C98 146.0(5) . . . . ?
C102 C97 C98 C99 -6.0(11) . . . . ?
Se1 C97 C98 C99 176.1(5) . . . . ?
C97 C98 C99 C100 7.5(10) . . . . ?
C98 C99 C100 C101 -6.9(10) . . . . ?
C99 C100 C101 C102 4.1(11) . . . . ?
C100 C101 C102 C97 -2.3(11) . . . . ?
C98 C97 C102 C101 3.6(11) . . . . ?
Se1 C97 C102 C101 -178.6(6) . . . . ?
C108 C103 C104 C105 8.8(12) . . . . ?
Se2 C103 C104 C105 -173.6(8) . . . . ?
C103 C104 C105 C106 -10.5(15) . . . . ?
C104 C105 C106 C107 7.9(16) . . . . ?
C105 C106 C107 C108 -3.8(17) . . . . ?
C104 C103 C108 C107 -4.2(12) . . . . ?
Se2 C103 C108 C107 178.1(8) . . . . ?
C106 C107 C108 C103 2.2(16) . . . . ?
C1 P1 C109 C110 103.8(5) . . . . ?
C7 P1 C109 C110 -150.9(4) . . . . ?
Au1 P1 C109 C110 -27.3(6) . . . . ?
P1 C109 C110 C111 -82.3(6) . . . . ?
C109 C110 C111 C112 161.9(7) . . . . ?
C110 C111 C112 C113 78.8(9) . . . . ?
C111 C112 C113 P4 -122.3(6) . . . . ?
C43 P4 C113 C112 147.4(3) . . . . ?
C37 P4 C113 C112 -99.9(4) . . . . ?
Au4 P4 C113 C112 15.0(5) . . . . ?
C19 P2 C114 C115 -54.3(6) . . . . ?
C13 P2 C114 C115 -156.3(5) . . . . ?
Au2 P2 C114 C115 64.5(6) . . . . ?
P2 C114 C115 C116 -65.1(9) . . . . ?
C114 C115 C116 C117 -130.1(7) . . . . ?
C115 C116 C117 C118 -110.5(7) . . . . ?
C116 C117 C118 P6 -82.3(5) . . . . ?
C61 P6 C118 C117 -92.1(5) . . . . ?
C67 P6 C118 C117 170.1(5) . . . . ?
Au6 P6 C118 C117 39.2(5) . . . . ?
C31 P3 C119 C120 -61.4(7) . . . . ?
C25 P3 C119 C120 171.9(6) . . . . ?
Au3 P3 C119 C120 62.0(7) . . . . ?
P3 C119 C120 C121 -98.2(8) . . . . ?
C119 C120 C121 C122 168.2(9) . . . . ?
C120 C121 C122 C123 151.3(9) . . . . ?
C121 C122 C123 P7 34.5(11) . . . . ?
C79 P7 C123 C122 159.4(7) . . . . ?
C73 P7 C123 C122 -95.2(7) . . . . ?
Au7 P7 C123 C122 40.9(7) . . . . ?
P5 C124 C125 C126 171.0(6) . . . . ?
C124 C125 C126 C127 -80.2(7) . . . . ?
C125 C126 C127 C128 -96.9(6) . . . . ?
C126 C127 C128 P8 167.6(4) . . . . ?

_refine_diff_density_max         1.679
_refine_diff_density_min         -1.348
_refine_diff_density_rms         0.320

_shelxl_version_number           2013-2

