# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2016

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 1447181'
_audit_update_record             
;
2016-01-14 deposited with the CCDC.
2016-03-03 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C15 H9 Dy N2 O6.50'
_chemical_formula_weight         483.74

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   C2/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   13.666(3)
_cell_length_b                   15.154(3)
_cell_length_c                   15.228(3)
_cell_angle_alpha                90.00
_cell_angle_beta                 101.24(3)
_cell_angle_gamma                90.00
_cell_volume                     3093.3(11)
_cell_formula_units_Z            8
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    5668
_cell_measurement_theta_min      1.3634
_cell_measurement_theta_max      31.0571

_exptl_crystal_description       rod
_exptl_crystal_colour            'light yellow'
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.05
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.077
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1848
_exptl_absorpt_coefficient_mu    4.869
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.7139
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_process_details   ?

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area dtetector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean '15x15 microns'
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            10844
_diffrn_reflns_av_R_equivalents  0.0378
_diffrn_reflns_av_sigmaI/netI    0.0345
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_theta_min         2.27
_diffrn_reflns_theta_max         27.47
_reflns_number_total             3537
_reflns_number_gt                3345
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'SMART (Bruker, 2000)'
_computing_cell_refinement       SMART
_computing_data_reduction        'SAINT (Bruker, 2000)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'SHELXL-97 (Sheldrick, 1997)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0190P)²+18.6355P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         3537
_refine_ls_number_parameters     222
_refine_ls_number_restraints     6
_refine_ls_R_factor_all          0.0337
_refine_ls_R_factor_gt           0.0308
_refine_ls_wR_factor_ref         0.0654
_refine_ls_wR_factor_gt          0.0638
_refine_ls_goodness_of_fit_ref   1.106
_refine_ls_restrained_S_all      1.109
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.577423(13) 0.176158(11) 0.578215(11) 0.01552(7) Uani 1 1 d . . .
C1 C 0.7214(4) 0.3268(3) 0.7154(3) 0.0327(11) Uani 1 1 d . . .
H1 H 0.7610 0.2767 0.7281 0.039 Uiso 1 1 calc R . .
C2 C 0.7557(4) 0.4051(3) 0.7585(4) 0.0397(12) Uani 1 1 d . . .
H2 H 0.8164 0.4068 0.7987 0.048 Uiso 1 1 calc R . .
C3 C 0.6990(4) 0.4790(3) 0.7410(3) 0.0407(13) Uani 1 1 d . . .
H3 H 0.7212 0.5322 0.7683 0.049 Uiso 1 1 calc R . .
C4 C 0.6065(4) 0.4749(3) 0.6813(3) 0.0331(11) Uani 1 1 d . . .
C5 C 0.5413(5) 0.5480(3) 0.6611(4) 0.0420(13) Uani 1 1 d . . .
H5 H 0.5610 0.6028 0.6859 0.050 Uiso 1 1 calc R . .
C6 C 0.4520(4) 0.5395(3) 0.6071(4) 0.0397(13) Uani 1 1 d . . .
H6 H 0.4104 0.5885 0.5962 0.048 Uiso 1 1 calc R . .
C7 C 0.4186(4) 0.4569(3) 0.5654(3) 0.0347(12) Uani 1 1 d . . .
C8 C 0.3251(4) 0.4444(4) 0.5085(4) 0.0417(13) Uani 1 1 d . . .
H8 H 0.2794 0.4906 0.4982 0.050 Uiso 1 1 calc R . .
C9 C 0.3019(4) 0.3649(4) 0.4688(4) 0.0438(14) Uani 1 1 d . . .
H9 H 0.2406 0.3564 0.4306 0.053 Uiso 1 1 calc R . .
C10 C 0.3711(3) 0.2956(4) 0.4860(4) 0.0357(11) Uani 1 1 d . . .
H10 H 0.3549 0.2419 0.4572 0.043 Uiso 1 1 calc R . .
C11 C 0.4824(3) 0.3833(3) 0.5805(3) 0.0246(9) Uani 1 1 d . . .
C12 C 0.5768(3) 0.3920(3) 0.6410(3) 0.0261(9) Uani 1 1 d . . .
C13 C 0.4598(3) 0.0246(3) 0.4648(2) 0.0183(8) Uani 1 1 d . . .
C14 C 0.7874(3) 0.2287(3) 0.5391(3) 0.0180(8) Uani 1 1 d . . .
C15 C 0.4453(3) 0.1429(3) 0.7229(3) 0.0182(8) Uani 1 1 d . . .
N1 N 0.6354(3) 0.3190(2) 0.6570(2) 0.0246(8) Uani 1 1 d . . .
N2 N 0.4583(3) 0.3031(2) 0.5411(2) 0.0242(8) Uani 1 1 d . . .
O1 O 0.4682(2) 0.10649(18) 0.46023(19) 0.0236(6) Uani 1 1 d . . .
O2 O 0.3938(2) -0.02340(19) 0.41945(19) 0.0235(6) Uani 1 1 d . . .
O3 O 0.7520(2) 0.17653(18) 0.58863(19) 0.0213(6) Uani 1 1 d . . .
O4 O 0.8768(2) 0.2505(2) 0.54580(19) 0.0245(6) Uani 1 1 d . . .
O5 O 0.4361(2) 0.1423(2) 0.63951(18) 0.0228(6) Uani 1 1 d . . .
O6 O 0.3775(2) 0.1454(2) 0.76720(18) 0.0220(6) Uani 1 1 d . . .
O1W O 0.5000 0.2474(8) 0.2500 0.210(7) Uani 1 2 d SU . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O2 2.347(3) 5_656 ?
Dy1 O1 2.350(3) . ?
Dy1 O5 2.360(3) . ?
Dy1 O3 2.361(3) . ?
Dy1 O6 2.361(3) 2_656 ?
Dy1 O4 2.378(3) 7_656 ?
Dy1 N2 2.512(4) . ?
Dy1 N1 2.527(3) . ?
C1 N1 1.334(6) . ?
C1 C2 1.394(6) . ?
C1 H1 0.9300 . ?
C2 C3 1.358(8) . ?
C2 H2 0.9300 . ?
C3 C4 1.408(8) . ?
C3 H3 0.9300 . ?
C4 C5 1.417(7) . ?
C4 C12 1.422(6) . ?
C5 C6 1.339(8) . ?
C5 H5 0.9300 . ?
C6 C7 1.438(8) . ?
C6 H6 0.9300 . ?
C7 C11 1.406(6) . ?
C7 C8 1.410(8) . ?
C8 C9 1.358(8) . ?
C8 H8 0.9300 . ?
C9 C10 1.404(7) . ?
C9 H9 0.9300 . ?
C10 N2 1.323(6) . ?
C10 H10 0.9300 . ?
C11 N2 1.366(6) . ?
C11 C12 1.438(6) . ?
C12 N1 1.360(5) . ?
C13 O1 1.249(5) . ?
C13 O2 1.256(5) . ?
C13 C13 1.567(7) 5_656 ?
C14 O4 1.250(5) . ?
C14 O3 1.253(5) . ?
C14 C14 1.551(7) 7_656 ?
C15 O6 1.249(5) . ?
C15 O5 1.251(5) . ?
C15 C15 1.560(8) 2_656 ?
O2 Dy1 2.347(3) 5_656 ?
O4 Dy1 2.378(3) 7_656 ?
O6 Dy1 2.361(3) 2_656 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Dy1 O1 69.40(10) 5_656 . ?
O2 Dy1 O5 85.82(11) 5_656 . ?
O1 Dy1 O5 75.99(10) . . ?
O2 Dy1 O3 80.61(10) 5_656 . ?
O1 Dy1 O3 122.37(11) . . ?
O5 Dy1 O3 150.30(10) . . ?
O2 Dy1 O6 77.27(10) 5_656 2_656 ?
O1 Dy1 O6 132.61(10) . 2_656 ?
O5 Dy1 O6 68.74(10) . 2_656 ?
O3 Dy1 O6 82.50(10) . 2_656 ?
O2 Dy1 O4 113.80(11) 5_656 7_656 ?
O1 Dy1 O4 80.15(10) . 7_656 ?
O5 Dy1 O4 141.10(10) . 7_656 ?
O3 Dy1 O4 68.48(10) . 7_656 ?
O6 Dy1 O4 145.73(10) 2_656 7_656 ?
O2 Dy1 N2 149.10(11) 5_656 . ?
O1 Dy1 N2 83.40(11) . . ?
O5 Dy1 N2 73.21(11) . . ?
O3 Dy1 N2 127.99(11) . . ?
O6 Dy1 N2 114.03(11) 2_656 . ?
O4 Dy1 N2 73.91(11) 7_656 . ?
O2 Dy1 N1 143.29(11) 5_656 . ?
O1 Dy1 N1 147.30(11) . . ?
O5 Dy1 N1 101.74(12) . . ?
O3 Dy1 N1 75.34(11) . . ?
O6 Dy1 N1 72.48(11) 2_656 . ?
O4 Dy1 N1 82.55(12) 7_656 . ?
N2 Dy1 N1 65.17(12) . . ?
N1 C1 C2 124.1(5) . . ?
N1 C1 H1 117.9 . . ?
C2 C1 H1 117.9 . . ?
C3 C2 C1 118.9(5) . . ?
C3 C2 H2 120.5 . . ?
C1 C2 H2 120.5 . . ?
C2 C3 C4 119.8(5) . . ?
C2 C3 H3 120.1 . . ?
C4 C3 H3 120.1 . . ?
C3 C4 C5 123.5(5) . . ?
C3 C4 C12 117.6(4) . . ?
C5 C4 C12 118.8(5) . . ?
C6 C5 C4 121.2(5) . . ?
C6 C5 H5 119.4 . . ?
C4 C5 H5 119.4 . . ?
C5 C6 C7 121.8(5) . . ?
C5 C6 H6 119.1 . . ?
C7 C6 H6 119.1 . . ?
C11 C7 C8 116.9(5) . . ?
C11 C7 C6 119.1(5) . . ?
C8 C7 C6 124.0(5) . . ?
C9 C8 C7 119.8(5) . . ?
C9 C8 H8 120.1 . . ?
C7 C8 H8 120.1 . . ?
C8 C9 C10 119.4(5) . . ?
C8 C9 H9 120.3 . . ?
C10 C9 H9 120.3 . . ?
N2 C10 C9 123.0(5) . . ?
N2 C10 H10 118.5 . . ?
C9 C10 H10 118.5 . . ?
N2 C11 C7 123.0(4) . . ?
N2 C11 C12 118.2(4) . . ?
C7 C11 C12 118.8(4) . . ?
N1 C12 C4 122.2(4) . . ?
N1 C12 C11 117.6(4) . . ?
C4 C12 C11 120.2(4) . . ?
O1 C13 O2 127.5(4) . . ?
O1 C13 C13 116.8(4) . 5_656 ?
O2 C13 C13 115.7(4) . 5_656 ?
O4 C14 O3 127.1(4) . . ?
O4 C14 C14 116.1(4) . 7_656 ?
O3 C14 C14 116.8(4) . 7_656 ?
O6 C15 O5 127.6(4) . . ?
O6 C15 C15 116.7(4) . 2_656 ?
O5 C15 C15 115.7(4) . 2_656 ?
C1 N1 C12 117.4(4) . . ?
C1 N1 Dy1 123.1(3) . . ?
C12 N1 Dy1 119.5(3) . . ?
C10 N2 C11 117.7(4) . . ?
C10 N2 Dy1 122.8(3) . . ?
C11 N2 Dy1 119.5(3) . . ?
C13 O1 Dy1 117.1(2) . . ?
C13 O2 Dy1 117.5(3) . 5_656 ?
C14 O3 Dy1 117.7(2) . . ?
C14 O4 Dy1 117.6(2) . 7_656 ?
C15 O5 Dy1 118.1(2) . . ?
C15 O6 Dy1 117.9(2) . 2_656 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
N1 C1 C2 C3 0.0(8) . . . . ?
C1 C2 C3 C4 1.2(8) . . . . ?
C2 C3 C4 C5 178.1(5) . . . . ?
C2 C3 C4 C12 -0.5(7) . . . . ?
C3 C4 C5 C6 -176.8(5) . . . . ?
C12 C4 C5 C6 1.8(7) . . . . ?
C4 C5 C6 C7 -1.4(8) . . . . ?
C5 C6 C7 C11 -1.2(7) . . . . ?
C5 C6 C7 C8 179.5(5) . . . . ?
C11 C7 C8 C9 -2.3(7) . . . . ?
C6 C7 C8 C9 176.9(5) . . . . ?
C7 C8 C9 C10 0.8(8) . . . . ?
C8 C9 C10 N2 1.5(8) . . . . ?
C8 C7 C11 N2 1.7(7) . . . . ?
C6 C7 C11 N2 -177.6(4) . . . . ?
C8 C7 C11 C12 -177.4(4) . . . . ?
C6 C7 C11 C12 3.3(6) . . . . ?
C3 C4 C12 N1 -1.4(7) . . . . ?
C5 C4 C12 N1 179.9(4) . . . . ?
C3 C4 C12 C11 179.0(4) . . . . ?
C5 C4 C12 C11 0.4(7) . . . . ?
N2 C11 C12 N1 -1.6(6) . . . . ?
C7 C11 C12 N1 177.6(4) . . . . ?
N2 C11 C12 C4 177.9(4) . . . . ?
C7 C11 C12 C4 -2.9(6) . . . . ?
C2 C1 N1 C12 -1.8(8) . . . . ?
C2 C1 N1 Dy1 178.9(4) . . . . ?
C4 C12 N1 C1 2.5(7) . . . . ?
C11 C12 N1 C1 -177.9(4) . . . . ?
C4 C12 N1 Dy1 -178.2(3) . . . . ?
C11 C12 N1 Dy1 1.4(5) . . . . ?
O2 Dy1 N1 C1 14.7(5) 5_656 . . . ?
O1 Dy1 N1 C1 -164.1(3) . . . . ?
O5 Dy1 N1 C1 113.6(4) . . . . ?
O3 Dy1 N1 C1 -36.1(4) . . . . ?
O6 Dy1 N1 C1 50.6(4) 2_656 . . . ?
O4 Dy1 N1 C1 -105.7(4) 7_656 . . . ?
N2 Dy1 N1 C1 178.6(4) . . . . ?
O2 Dy1 N1 C12 -164.6(3) 5_656 . . . ?
O1 Dy1 N1 C12 16.6(4) . . . . ?
O5 Dy1 N1 C12 -65.7(3) . . . . ?
O3 Dy1 N1 C12 144.7(3) . . . . ?
O6 Dy1 N1 C12 -128.7(3) 2_656 . . . ?
O4 Dy1 N1 C12 75.1(3) 7_656 . . . ?
N2 Dy1 N1 C12 -0.6(3) . . . . ?
C9 C10 N2 C11 -2.2(7) . . . . ?
C9 C10 N2 Dy1 176.3(4) . . . . ?
C7 C11 N2 C10 0.5(6) . . . . ?
C12 C11 N2 C10 179.6(4) . . . . ?
C7 C11 N2 Dy1 -178.1(3) . . . . ?
C12 C11 N2 Dy1 1.1(5) . . . . ?
O2 Dy1 N2 C10 -17.5(5) 5_656 . . . ?
O1 Dy1 N2 C10 10.5(4) . . . . ?
O5 Dy1 N2 C10 -66.8(4) . . . . ?
O3 Dy1 N2 C10 136.9(3) . . . . ?
O6 Dy1 N2 C10 -123.5(4) 2_656 . . . ?
O4 Dy1 N2 C10 92.1(4) 7_656 . . . ?
N1 Dy1 N2 C10 -178.8(4) . . . . ?
O2 Dy1 N2 C11 161.0(3) 5_656 . . . ?
O1 Dy1 N2 C11 -171.0(3) . . . . ?
O5 Dy1 N2 C11 111.7(3) . . . . ?
O3 Dy1 N2 C11 -44.6(3) . . . . ?
O6 Dy1 N2 C11 55.0(3) 2_656 . . . ?
O4 Dy1 N2 C11 -89.4(3) 7_656 . . . ?
N1 Dy1 N2 C11 -0.3(3) . . . . ?
O2 C13 O1 Dy1 165.7(3) . . . . ?
C13 C13 O1 Dy1 -14.1(6) 5_656 . . . ?
O2 Dy1 O1 C13 15.5(3) 5_656 . . . ?
O5 Dy1 O1 C13 -75.3(3) . . . . ?
O3 Dy1 O1 C13 79.1(3) . . . . ?
O6 Dy1 O1 C13 -32.8(4) 2_656 . . . ?
O4 Dy1 O1 C13 135.7(3) 7_656 . . . ?
N2 Dy1 O1 C13 -149.6(3) . . . . ?
N1 Dy1 O1 C13 -165.3(3) . . . . ?
O1 C13 O2 Dy1 165.8(3) . . . 5_656 ?
C13 C13 O2 Dy1 -14.5(5) 5_656 . . 5_656 ?
O4 C14 O3 Dy1 165.7(3) . . . . ?
C14 C14 O3 Dy1 -14.0(5) 7_656 . . . ?
O2 Dy1 O3 C14 135.6(3) 5_656 . . . ?
O1 Dy1 O3 C14 77.3(3) . . . . ?
O5 Dy1 O3 C14 -160.5(3) . . . . ?
O6 Dy1 O3 C14 -146.2(3) 2_656 . . . ?
O4 Dy1 O3 C14 15.2(3) 7_656 . . . ?
N2 Dy1 O3 C14 -31.5(3) . . . . ?
N1 Dy1 O3 C14 -72.4(3) . . . . ?
O3 C14 O4 Dy1 166.0(3) . . . 7_656 ?
C14 C14 O4 Dy1 -14.2(5) 7_656 . . 7_656 ?
O6 C15 O5 Dy1 163.6(3) . . . . ?
C15 C15 O5 Dy1 -14.7(3) 2_656 . . . ?
O2 Dy1 O5 C15 92.8(3) 5_656 . . . ?
O1 Dy1 O5 C15 162.6(3) . . . . ?
O3 Dy1 O5 C15 30.1(4) . . . . ?
O6 Dy1 O5 C15 14.8(3) 2_656 . . . ?
O4 Dy1 O5 C15 -143.6(3) 7_656 . . . ?
N2 Dy1 O5 C15 -110.2(3) . . . . ?
N1 Dy1 O5 C15 -50.9(3) . . . . ?
O5 C15 O6 Dy1 -167.2(3) . . . 2_656 ?
C15 C15 O6 Dy1 11.1(3) 2_656 . . 2_656 ?

_diffrn_measured_fraction_theta_max 0.998
_diffrn_reflns_theta_full        27.47
_diffrn_measured_fraction_theta_full 0.998
_refine_diff_density_max         1.635
_refine_diff_density_min         -0.857
_refine_diff_density_rms         0.130
_exptl_crystal_recrystallization_method 'hydrothermal synthesize'
_exptl_crystal_preparation       'Magnetic properties'
