data_MN-0P4CD4_publ

_pd_block_id                     2016-03-05T14:58|MN-0P4CD4|CMB|BT-1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-03-05T14:58
_audit_author_name               CMB
_audit_update_record             
; 2016-03-05T14:58  Initial CIF as created by GSAS2CIF
;

#=============================================================================
# this information describes the project, paper etc. for the CIF             #
# Acta Cryst. Section C papers and editorial correspondence is generated     #
# from the information in this section                                       #
#                                                                            #
#   (from)   CIF submission form for Rietveld refinements (Acta Cryst. C)    #
#                                                 Version 14 December 1998   #
#=============================================================================

# 1. SUBMISSION DETAILS
_publ_contact_author_name            'J.R. Long'  
_publ_contact_author_address        
; 
Department of Chemistry, University of California, Berkeley, Berkeley, 
California 94720, United States.
;
_publ_contact_author_email           'jrlong@berkeley.edu'
_publ_contact_author_phone           '510-642-0860'
_publ_contact_author_fax             'none'
_publ_requested_journal 			 'Chem. Commun.'
_publ_section_title 				 
;
Adsorption of Two Hydrogen Molecules 
at a Single Metal Site in a Metal-Organic Framework
;
loop_
_publ_author_name
'Tomče Runčevski'
'Matthew T. Kapelewski'
'Rodolfo M. Torres-Gavosto'
'Jacob D. Tarver'
'Craig M. Brown'
'Jeffrey R. Long'


_publ_author_address
;
Department of Chemistry, University of California, Berkeley, 
Berkeley, California 94720.
;
 _publ_section_abstract
;
In order to drastically increase the gas storage capacity of 
metal-organic frameworks, coordinatively unsaturated metal centers 
able to bind multiple gas molecules must be 
introduced. Herein, we report the first example of two gas molecules 
(of either deuterium, methane, or carbon dioxide) binding to a 
single metal center (Mn2+) in a metal organic framework.
;
 
#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; 
Rietveld refinement of neutron scattering powder diffraction data using
the GSAS/EXPGUI software, with R values and definitions given in
https://subversion.xor.aps.anl.gov/EXPGUI/gsas/all/GSAS%20Manual.pdf 
;

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

_pd_char_colour                  'orange' # use ICDD colour descriptions
_refine_ls_shift/su_max          0.49
_refine_ls_shift/su_mean         0.49
_refine_ls_number_parameters     21
_refine_ls_goodness_of_fit_all   1.21
_refine_ls_number_restraints     29
_refine_ls_matrix_type           full
_refine_ls_hydrogen_treatment    'refall'
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     powder

_chemical_name_systematic        'Metal-organic framework'
_chemical_name_common            'Mn2(DSBDC)'
_chemical_formula_moiety         'C4 H Mn O2 S'

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C4.29 H D1.18 Mn O2 S'
_chemical_properties_physical    'air-sensitive, oxygen-sensitive'

_diffrn_ambient_temperature      5

_cell_measurement_temperature    5

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_refinement  'GSAS/EXPGUI'
_computing_molecular_graphics    'VESTA'
_computing_publication_material  'GSAS'

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from C:/GSAS/data/Coprime/0p5CO2/CO_PRIME_R3M_R.cif'
_cell_length_a                   27.316(4)
_cell_length_b                   27.316
_cell_length_c                   15.0891(25)
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                120.0
_cell_volume                     9750.8(27)
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_H-M   'R -3 c'
_symmetry_space_group_name_Hall  '-r 3 2" c'
_symmetry_int_tables_number      167
_chemical_absolute_configuration ?
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -y,x-y,+z
3 y-x,-x,+z
4 y-x,+y,+z+1/2
5 -y,-x,+z+1/2
6 +x,x-y,+z+1/2
-1 -x,-y,-z
-2 +y,y-x,-z
-3 x-y,+x,-z
-4 x-y,-y,-z+1/2
-5 +y,+x,-z+1/2
-6 -x,y-x,-z+1/2
101 +x+1/3,+y+2/3,+z+2/3
102 -y+1/3,x-y+2/3,+z+2/3
103 y-x+1/3,-x+2/3,+z+2/3
104 y-x+1/3,+y+2/3,+z+1/6
105 -y+1/3,-x+2/3,+z+1/6
106 +x+1/3,x-y+2/3,+z+1/6
-101 -x+2/3,-y+1/3,-z+1/3
-102 +y+2/3,y-x+1/3,-z+1/3
-103 x-y+2/3,+x+1/3,-z+1/3
-104 x-y+2/3,-y+1/3,-z+5/6
-105 +y+2/3,+x+1/3,-z+5/6
-106 -x+2/3,y-x+1/3,-z+5/6
201 +x+2/3,+y+1/3,+z+1/3
202 -y+2/3,x-y+1/3,+z+1/3
203 y-x+2/3,-x+1/3,+z+1/3
204 y-x+2/3,+y+1/3,+z+5/6
205 -y+2/3,-x+1/3,+z+5/6
206 +x+2/3,x-y+1/3,+z+5/6
-201 -x+1/3,-y+2/3,-z+2/3
-202 +y+1/3,y-x+2/3,-z+2/3
-203 x-y+1/3,+x+2/3,-z+2/3
-204 x-y+1/3,-y+2/3,-z+1/6
-205 +y+1/3,+x+2/3,-z+1/6
-206 -x+1/3,y-x+2/3,-z+1/6

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Mn Mn1 0.31252 0.3333 0.08333 1.0 Uiso 0.05221 18
Mn Mn2 0.40265 0.40265 0.25 1.0 Uiso 0.03921 18
S S3 0.28777 0.2291 0.05245 1.0 Uiso 0.09589 36
O O1 0.37124 0.31847 0.19226 1.0 Uiso 0.06064 36
O O2 0.3381 0.27943 0.32524 1.0 Uiso 0.06403 36
C C1 0.33953 0.21811 0.19745 1.0 Uiso 0.03963 36
C C4 0.31639 0.19715 0.11383 1.0 Uiso 0.04261 36
C C2 0.3578 0.18761 0.24514 1.0 Uiso 0.04078 36
C C3 0.34435 0.26815 0.23467 1.0 Uiso 0.02684 36
H H 0.37321 0.20306 0.30851 1.0 Uiso 0.03301 36
C CD1 0.0598(13) 0.2064(10) 0.1815(17) 0.294(8) Uiso 0.006(6) 36
D D1 0.0628(17) 0.1929(18) 0.2482(22) 0.294(8) Uiso 0.006(6) 36
D D2 0.0967(14) 0.2121(14) 0.1450(26) 0.294(8) Uiso 0.006(6) 36
D D3 0.0596(16) 0.2461(13) 0.1838(27) 0.294(8) Uiso 0.006(6) 36
D D4 0.0217(14) 0.1741(15) 0.1490(24) 0.294(8) Uiso 0.006(6) 36
_chemical_formula_weight         173.95
_cell_formula_units_Z            36

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Mn1 Mn2 3.3633(4) . 1_555 N
Mn1 Mn2 3.3624(4) . 103_554 N
Mn1 S3 2.61747(35) . 1_555 N
Mn1 S3 2.61897(35) . -104_443 N
Mn1 O1 2.46740(26) . 1_555 N
Mn1 O1 2.46756(26) . -104_443 N
Mn1 O2 1.68993(20) . -5_555 N
Mn1 O2 1.68974(20) . 103_554 N
Mn1 C3 3.26890(35) . 1_555 N
Mn1 C3 3.0769(4) . -5_555 N
Mn1 C3 3.0767(4) . 103_554 N
Mn1 C3 3.26958(35) . -104_443 N
Mn2 Mn1 3.3633(4) . 1_555 N
Mn2 Mn1 3.3633(4) . -5_555 N
Mn2 S3 2.33869(31) . -104_443 N
Mn2 S3 2.33869(31) . 202_555 N
Mn2 O1 2.19316(26) . 1_555 N
Mn2 O1 2.19316(26) . -5_555 N
Mn2 O2 3.1294(4) . 1_555 N
Mn2 O2 3.1294(4) . -5_555 N
Mn2 C4 3.3993(4) . -104_443 N
Mn2 C4 3.3993(4) . 202_555 N
Mn2 C3 3.1996(4) . 1_555 N
Mn2 C3 3.1996(4) . -5_555 N
Mn2 D3 2.723(30) . 106_555 N
Mn2 D3 2.723(30) . -203_444 N
S3 Mn1 2.61747(35) . 1_555 N
S3 Mn2 2.33869(31) . 103_554 N
S3 O1 3.16888(34) . 1_555 N
S3 O1 3.4936(4) . 103_554 N
S3 O1 3.2320(4) . -104_443 N
S3 O2 3.0525(4) . 103_554 N
S3 C1 2.70203(32) . 1_555 N
S3 C4 1.70685(19) . 1_555 N
S3 C2 2.66911(35) . -201_444 N
S3 C3 3.0721(4) . 1_555 N
S3 H 2.8117(4) . -201_444 N
S3 D3 3.241(28) . 205_554 N
O1 Mn1 2.46740(26) . 1_555 N
O1 Mn2 2.19316(26) . 1_555 N
O1 S3 3.16888(34) . 1_555 N
O1 S3 3.2320(4) . -104_443 N
O1 S3 3.4936(4) . 202_555 N
O1 O1 3.04448(33) . -5_555 N
O1 O1 3.3615(5) . -104_443 N
O1 O2 2.24006(31) . 1_555 N
O1 O2 2.8268(4) . -5_555 N
O1 C1 2.42858(33) . 1_555 N
O1 C4 3.1085(4) . 1_555 N
O1 C2 3.4981(5) . 1_555 N
O1 C3 1.35237(15) . 1_555 N
O1 C3 3.4111(4) . -5_555 N
O1 D3 3.455(33) . 205_554 N
O1 D3 2.712(30) . -203_444 N
O2 Mn1 1.68993(20) . -5_555 N
O2 Mn2 3.1294(4) . 1_555 N
O2 S3 3.0525(4) . 202_555 N
O2 O1 2.24006(31) . 1_555 N
O2 O1 2.8268(4) . -5_555 N
O2 O2 2.7683(5) . -206_445 N
O2 C1 2.56725(29) . 1_555 N
O2 C2 3.0644(4) . 1_555 N
O2 C3 1.42980(22) . 1_555 N
O2 C3 3.3168(4) . -5_555 N
O2 H 2.7087(4) . 1_555 N
C1 S3 2.70203(32) . 1_555 N
C1 O1 2.42858(33) . 1_555 N
C1 O2 2.56725(29) . 1_555 N
C1 C1 2.81507(35) . -201_444 N
C1 C4 1.39910(19) . 1_555 N
C1 C4 2.42115(33) . -201_444 N
C1 C2 1.36977(15) . 1_555 N
C1 C2 2.38185(26) . -201_444 N
C1 C3 1.42174(17) . 1_555 N
C1 H 2.04992(25) . 1_555 N
C1 H 3.3326(4) . -201_444 N
C1 D3 3.35(4) . 205_554 N
C4 Mn2 3.3993(4) . 103_554 N
C4 S3 1.70685(19) . 1_555 N
C4 O1 3.1085(4) . 1_555 N
C4 C1 1.39910(19) . 1_555 N
C4 C1 2.42115(33) . -201_444 N
C4 C4 2.77747(30) . -201_444 N
C4 C2 2.35954(29) . 1_555 N
C4 C2 1.37001(17) . -201_444 N
C4 C3 2.48761(27) . 1_555 N
C4 H 3.2885(4) . 1_555 N
C4 H 2.09501(22) . -201_444 N
C4 D3 2.94(4) . 205_554 N
C2 S3 2.66911(35) . -201_444 N
C2 O1 3.4981(5) . 1_555 N
C2 O2 3.0644(4) . 1_555 N
C2 C1 1.36977(15) . 1_555 N
C2 C1 2.38185(26) . -201_444 N
C2 C4 2.35954(29) . 1_555 N
C2 C4 1.37001(17) . -201_444 N
C2 C2 2.6785(4) . -201_444 N
C2 C3 2.40995(33) . 1_555 N
C2 H 1.04506(15) . 1_555 N
C2 D3 3.47(4) . -5_555 N
C3 Mn1 3.26890(35) . 1_555 N
C3 Mn1 3.0769(4) . -5_555 N
C3 Mn2 3.1996(4) . 1_555 N
C3 S3 3.0721(4) . 1_555 N
C3 O1 1.35237(15) . 1_555 N
C3 O1 3.4111(4) . -5_555 N
C3 O2 1.42980(22) . 1_555 N
C3 O2 3.3168(4) . -5_555 N
C3 C1 1.42174(17) . 1_555 N
C3 C4 2.48761(27) . 1_555 N
C3 C2 2.40995(33) . 1_555 N
C3 H 2.53506(29) . 1_555 N
H S3 2.8117(4) . -201_444 N
H O2 2.7087(4) . 1_555 N
H C1 2.04992(25) . 1_555 N
H C1 3.3326(4) . -201_444 N
H C4 3.2885(4) . 1_555 N
H C4 2.09501(22) . -201_444 N
H C2 1.04506(15) . 1_555 N
H C3 2.53506(29) . 1_555 N
H D2 3.280(32) . 202_555 N
CD1 D1 1.08930(26) . 1_555 N
CD1 D1 3.12(6) . -6_555 N
CD1 D2 1.08882(26) . 1_555 N
CD1 D3 1.08914(24) . 1_555 N
CD1 D4 1.08902(23) . 1_555 N
CD1 D4 3.22(4) . -6_555 N
D1 CD1 1.08930(26) . 1_555 N
D1 CD1 3.12(6) . -6_555 N
D1 D1 2.97(8) . -6_555 N
D1 D2 1.753(19) . 1_555 N
D1 D3 1.788(16) . 1_555 N
D1 D3 3.42(5) . -6_555 N
D1 D4 1.787(13) . 1_555 N
D1 D4 2.53(5) . -6_555 N
D2 H 3.280(32) . 103_554 N
D2 CD1 1.08882(26) . 1_555 N
D2 D1 1.753(19) . 1_555 N
D2 D3 1.781(12) . 1_555 N
D2 D4 1.777(5) . 1_555 N
D3 Mn2 2.723(30) . 206_454 N
D3 S3 3.241(28) . 105_555 N
D3 O1 3.455(33) . 105_555 N
D3 O1 2.712(30) . -202_344 N
D3 C1 3.35(4) . 105_555 N
D3 C4 2.94(4) . 105_555 N
D3 C2 3.47(4) . -5_555 N
D3 CD1 1.08914(24) . 1_555 N
D3 D1 1.788(16) . 1_555 N
D3 D1 3.42(5) . -6_555 N
D3 D2 1.781(12) . 1_555 N
D3 D3 3.46(7) . -6_555 N
D3 D4 1.784(8) . 1_555 N
D3 D4 3.49(5) . -6_555 N
D4 CD1 1.08902(23) . 1_555 N
D4 CD1 3.22(4) . -6_555 N
D4 D1 1.787(13) . 1_555 N
D4 D1 2.53(5) . -6_555 N
D4 D2 1.777(5) . 1_555 N
D4 D3 1.784(8) . 1_555 N
D4 D3 3.49(5) . -6_555 N
D4 D4 3.22(7) . -6_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 Mn1 O2 109.990(12) -5_557 . 103_554 N
S3 Mn2 S3 163.7104(27) -104_554 . 202_555 N
Mn2 S3 C4 113.416(7) 103_554 . 1_555 N
Mn1 O2 C3 160.9252(25) -5_445 . 1_555 N
C4 C1 C2 116.892(6) 1_555 . 1_555 N
C4 C1 C3 123.7354(26) 1_555 . 1_555 N
C2 C1 C3 119.370(9) 1_555 . 1_555 N
S3 C4 C1 120.585(6) 1_555 . 1_555 N
S3 C4 C2 119.936(7) 1_555 . -201_444 N
C1 C4 C2 118.6627(11) 1_555 . -201_444 N
C1 C2 C4 124.184(7) 1_555 . -201_444 N
C1 C2 H 115.527(7) 1_555 . 1_555 N
C4 C2 H 119.7284(9) -201_443 . 1_555 N
O1 C3 O2 107.216(7) 1_555 . 1_555 N
O1 C3 C1 122.175(8) 1_555 . 1_555 N
O2 C3 C1 128.3962(14) 1_555 . 1_555 N
D1 CD1 D2 107.2(17) 1_555 . 1_555 N
D1 CD1 D3 110.3(15) 1_555 . 1_555 N
D1 CD1 D4 110.2(12) 1_555 . 1_555 N
D2 CD1 D3 109.8(11) 1_555 . 1_555 N
D2 CD1 D4 109.4(5) 1_555 . 1_555 N
D3 CD1 D4 110.0(7) 1_555 . 1_555 N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

 

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; 
NCNR
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
;

;
_diffrn_radiation_probe          'neutron'
_diffrn_radiation_type           'Neutron'
_diffrn_radiation_wavelength     2.0772
_diffrn_source                   'Nuclear Reactor'
_diffrn_source_type              'BT-1'
_diffrn_detector                 'BT-1'
_diffrn_detector_type            'Helium' # make or model of detector
_diffrn_measurement_device_type  'neutron'

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;


# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  Ge311

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

 
_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; 
Vanadium cell
;

_pd_spec_mount_mode              transmission # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   cylinder # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Mn 36.0 -0.3730 International_Tables_Vol_C
S 36.0 0.2847 International_Tables_Vol_C
O 72.0 0.5803 International_Tables_Vol_C
C 154.582 0.6646 International_Tables_Vol_C
H 36.0 -0.3739 International_Tables_Vol_C
D 42.329 0.6671 International_Tables_Vol_C
_pd_proc_ls_prof_R_factor        0.0268
_pd_proc_ls_prof_wR_factor       0.0322
_pd_proc_ls_prof_wR_expected     0.0288
_refine_ls_R_Fsqd_factor         0.12572

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 18 terms.
 Shifted Chebyshev function of 1st kind
      1:    1266.01     2:   -370.800     3:    297.713     4:   -71.8825    
      5:    68.8716     6:   -53.6997     7:    40.3767     8:   -56.2019    
      9:    27.8143    10:   -37.6709    11:    15.5191    12:   -12.7108    
     13:    18.5105    14:   -12.3040    15:    12.2822    16:   3.281450E-02
     17:   -3.64411    18:    10.5059    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

 _cell_measurement_reflns_used   840
 _cell_measurement_theta_min 	 1.9475
 _cell_measurement_theta_max     161.7475

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  199.235 #2(GV)   =   -0.100 #3(GW)   =   46.703
 #4(GP)   =    0.000 #5(LX)   =   14.845 #6(LY)   =   18.651
 #7(S/L)  =   0.0443 #8(H/L)  =   0.0318
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0001 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00010
_pd_proc_info_datetime           2016-03-05T14:58:56
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.94
_pd_meas_2theta_range_max        161.74
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.9475
_pd_proc_2theta_range_max        161.7475
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
7800(170) 0.0 3528. .
7330(170) 0.0 3513. .
7120(160) 0.0 3498. .
7000(160) 0.0 3483. .
6530(160) 0.0 3467. .
6380(160) 0.0 3451. .
6760(160) 0.0 3434. .
6430(160) 0.0 3417. .
6390(160) 0.0 3400. .
6410(160) 0.0 3383. .
6340(150) 0.0 3365. .
5870(150) 0.0 3347. .
5930(150) 0.0 3329. .
5770(150) 0.0 3311. .
5480(140) 0.0 3293. .
5110(140) 0.0 3274. .
5180(140) 0.0 3255. .
4830(130) 0.0 3236. .
4710(130) 0.0 3217. .
4590(130) 0.0 3198. .
4450(130) 0.0 3179. .
4160(120) 0.0 3159. .
4080(120) 0.0 3140. .
3910(120) 0.0 3120. .
3670(120) 0.0 3101. .
4030(120) 0.0 3081. .
3740(120) 0.0 3062. .
3500(110) 0.0 3042. .
3470(110) 0.0 3023. .
3570(110) 0.0 3003. .
3400(110) 0.0 2984. .
3460(110) 0.0 2964. .
3270(110) 0.0 2945. .
3180(110) 0.0 2925. .
3250(110) 0.0 2906. .
2990(100) 0.0 2886. .
3270(110) 0.0 2867. .
2990(100) 0.0 2848. .
3030(110) 0.0 2829. .
3200(110) 0.0 2810. .
3140(110) 0.0 2791. .
3070(110) 0.0 2772. .
2990(100) 0.0 2753. .
2970(100) 0.0 2735. .
3030(110) 0.0 2716. .
2870(100) 0.0 2698. .
2712(99) 0.0 2680. .
2870(100) 0.0 2662. .
2860(100) 0.0 2644. .
2850(100) 0.0 2626. .
2693(98) 0.0 2608. .
2706(99) 0.0 2591. .
2720(99) 0.0 2573. .
2681(98) 0.0 2556. .
2605(96) 0.0 2539. .
2642(97) 0.0 2522. .
2657(98) 0.0 2505. .
2607(97) 0.0 2489. .
2498(94) 0.0 2473. .
2521(95) 0.0 2456. .
2341(91) 0.0 2440. .
2368(92) 0.0 2425. .
2384(92) 0.0 2409. .
2381(92) 0.0 2393. .
2476(94) 0.0 2378. .
2383(92) 0.0 2363. .
2432(93) 0.0001156 2348. 2356.
2110(86) 0.0001352 2333. 2342.
2381(92) 0.0001181 2319. 2328.
2145(87) 0.0001321 2305. 2314.
2406(92) 0.0001181 2290. 2300.
2252(89) 0.0001262 2276. 2286.
2356(91) 0.0001208 2263. 2273.
2136(87) 0.0001321 2249. 2260.
2191(88) 0.0001291 2236. 2247.
2274(90) 0.0001235 2223. 2234.
2090(85) 0.0001384 2210. 2221.
2192(88) 0.0001291 2197. 2209.
2118(86) 0.0001352 2184. 2197.
2201(88) 0.0001291 2172. 2185.
2177(87) 0.0001321 2159. 2173.
2018(84) 0.0001417 2147. 2161.
2278(90) 0.0001235 2136. 2150.
2075(85) 0.0001384 2124. 2139.
2044(84) 0.0001417 2112. 2128.
2178(87) 0.0001321 2101. 2118.
2278(90) 0.0001235 2090. 2108.
2040(84) 0.0001417 2079. 2097.
2100(86) 0.0001352 2068. 2088.
2105(86) 0.0001352 2058. 2078.
2101(86) 0.0001352 2047. 2069.
2030(84) 0.0001417 2037. 2060.
2070(85) 0.0001384 2027. 2051.
2063(85) 0.0001384 2017. 2042.
1934(82) 0.0001487 2008. 2034.
1957(82) 0.0001487 1998. 2026.
2070(100) 0.0000925 1989. 2019.
1960(100) 0.0000980 1980. 2012.
1920(100) 0.0001000 1971. 2005.
2127(64) 0.0002441 1962. 1998.
1999(62) 0.0002601 1954. 1992.
2067(63) 0.0002520 1945. 1987.
2075(64) 0.0002441 1937. 1982.
2054(63) 0.0002520 1929. 1978.
2053(63) 0.0002520 1921. 1974.
1947(61) 0.0002687 1913. 1971.
2037(63) 0.0002520 1906. 1969.
2101(64) 0.0002441 1898. 1969.
2052(63) 0.0002520 1891. 1970.
2100(64) 0.0002441 1884. 1974.
2028(63) 0.0002520 1877. 1983.
2153(65) 0.0002367 1870. 1997.
2150(65) 0.0002367 1863. 2021.
2115(64) 0.0002441 1857. 2053.
2170(65) 0.0002367 1850. 2094.
2242(66) 0.0002296 1844. 2144.
2324(68) 0.0002163 1838. 2207.
2371(68) 0.0002163 1832. 2280.
2396(69) 0.0002100 1826. 2355.
2447(70) 0.0002041 1820. 2443.
2564(71) 0.0001984 1815. 2547.
2586(72) 0.0001929 1809. 2652.
2700(74) 0.0001826 1804. 2773.
2824(75) 0.0001778 1799. 2918.
2992(78) 0.0001644 1794. 3070.
3158(80) 0.0001562 1789. 3249.
3382(83) 0.0001452 1784. 3463.
3578(86) 0.0001352 1780. 3701.
3876(90) 0.0001235 1775. 3998.
4419(96) 0.0001085 1771. 4356.
4920(100) 0.0000961 1766. 4799.
5570(110) 0.0000857 1762. 5338.
6020(110) 0.0000783 1758. 5939.
6480(120) 0.0000731 1754. 6493.
6460(120) 0.0000731 1750. 6785.
6140(110) 0.0000769 1746. 6534.
5460(110) 0.0000873 1743. 5670.
4644(98) 0.0001041 1739. 4560.
3771(88) 0.0001291 1736. 3603.
3078(79) 0.0001602 1732. 2933.
2651(73) 0.0001877 1729. 2518.
2312(67) 0.0002228 1726. 2277.
2084(64) 0.0002441 1723. 2136.
1985(62) 0.0002601 1720. 2047.
1945(61) 0.0002687 1717. 1985.
1799(58) 0.0002973 1714. 1939.
1906(60) 0.0002778 1711. 1903.
1775(58) 0.0002973 1708. 1874.
1869(60) 0.0002778 1706. 1850.
1772(58) 0.0002973 1703. 1830.
1837(59) 0.0002873 1701. 1813.
1688(56) 0.0003189 1698. 1799.
1755(58) 0.0002973 1696. 1786.
1706(57) 0.0003078 1694. 1776.
1713(57) 0.0003078 1692. 1766.
1705(57) 0.0003078 1690. 1758.
1680(56) 0.0003189 1688. 1750.
1713(57) 0.0003078 1686. 1743.
1761(58) 0.0002973 1684. 1737.
1621(55) 0.0003306 1682. 1731.
1737(57) 0.0003078 1680. 1726.
1691(56) 0.0003189 1678. 1721.
1780(58) 0.0002973 1677. 1717.
1734(57) 0.0003078 1675. 1713.
1698(57) 0.0003078 1674. 1709.
1690(56) 0.0003189 1672. 1705.
1655(56) 0.0003189 1671. 1702.
1649(56) 0.0003189 1669. 1699.
1645(56) 0.0003189 1668. 1696.
1640(55) 0.0003306 1667. 1693.
1599(55) 0.0003306 1665. 1690.
1727(57) 0.0003078 1664. 1688.
1685(56) 0.0003189 1663. 1686.
1681(56) 0.0003189 1662. 1684.
1634(55) 0.0003306 1661. 1681.
1629(55) 0.0003306 1659. 1680.
1620(55) 0.0003306 1658. 1678.
1677(56) 0.0003189 1657. 1676.
1604(55) 0.0003306 1656. 1674.
1677(56) 0.0003189 1656. 1673.
1630(55) 0.0003306 1655. 1671.
1651(56) 0.0003189 1654. 1670.
1583(54) 0.0003429 1653. 1668.
1710(57) 0.0003078 1652. 1667.
1587(54) 0.0003429 1651. 1666.
1622(55) 0.0003306 1650. 1664.
1729(57) 0.0003078 1650. 1663.
1672(70) 0.0002041 1649. 1662.
1668(70) 0.0002041 1648. 1661.
1704(71) 0.0001984 1648. 1660.
1717(72) 0.0001929 1647. 1659.
1692(71) 0.0001984 1646. 1658.
1679(71) 0.0001984 1646. 1657.
1677(71) 0.0001984 1645. 1656.
1647(70) 0.0002041 1644. 1655.
1584(68) 0.0002163 1644. 1654.
1536(82) 0.0001487 1643. 1654.
1640(85) 0.0001384 1643. 1653.
1687(87) 0.0001321 1642. 1652.
1689(57) 0.0003078 1642. 1651.
1644(56) 0.0003189 1641. 1651.
1695(57) 0.0003078 1641. 1650.
1630(56) 0.0003189 1640. 1649.
1641(56) 0.0003189 1640. 1649.
1657(57) 0.0003078 1639. 1648.
1609(56) 0.0003189 1639. 1647.
1679(57) 0.0003078 1638. 1647.
1701(57) 0.0003078 1638. 1646.
1693(57) 0.0003078 1637. 1646.
1726(58) 0.0002973 1637. 1645.
1676(57) 0.0003078 1636. 1645.
1682(57) 0.0003078 1636. 1644.
1729(58) 0.0002973 1635. 1643.
1740(58) 0.0002973 1635. 1643.
1657(57) 0.0003078 1634. 1642.
1717(58) 0.0002973 1634. 1642.
1722(58) 0.0002973 1633. 1641.
1684(57) 0.0003078 1633. 1641.
1646(56) 0.0003189 1633. 1640.
1694(57) 0.0003078 1632. 1640.
1679(57) 0.0003078 1632. 1639.
1717(58) 0.0002973 1631. 1639.
1640(56) 0.0003189 1631. 1638.
1702(58) 0.0002973 1630. 1638.
1650(56) 0.0003189 1630. 1638.
1705(58) 0.0002973 1629. 1637.
1708(58) 0.0002973 1629. 1637.
1709(58) 0.0002973 1628. 1636.
1729(58) 0.0002973 1628. 1636.
1688(57) 0.0003078 1627. 1635.
1713(58) 0.0002973 1627. 1635.
1682(57) 0.0003078 1626. 1635.
1683(57) 0.0003078 1626. 1634.
1682(57) 0.0003078 1625. 1634.
1601(56) 0.0003189 1625. 1633.
1615(56) 0.0003189 1624. 1633.
1670(57) 0.0003078 1623. 1632.
1631(56) 0.0003189 1623. 1632.
1582(55) 0.0003306 1622. 1632.
1638(56) 0.0003189 1622. 1631.
1790(59) 0.0002873 1621. 1631.
1628(56) 0.0003189 1621. 1631.
1569(55) 0.0003306 1620. 1631.
1622(56) 0.0003189 1619. 1630.
1650(56) 0.0003189 1619. 1630.
1684(57) 0.0003078 1618. 1630.
1682(57) 0.0003078 1617. 1630.
1625(56) 0.0003189 1617. 1630.
1705(58) 0.0002973 1616. 1631.
1701(57) 0.0003078 1615. 1631.
1705(58) 0.0002973 1615. 1633.
1649(56) 0.0003189 1614. 1635.
1710(58) 0.0002973 1613. 1637.
1767(59) 0.0002873 1613. 1641.
1760(59) 0.0002873 1612. 1645.
1725(58) 0.0002973 1611. 1651.
1691(57) 0.0003078 1610. 1659.
1731(58) 0.0002973 1610. 1669.
1725(58) 0.0002973 1609. 1681.
1727(58) 0.0002973 1608. 1697.
1738(58) 0.0002973 1607. 1716.
1775(59) 0.0002873 1606. 1735.
1755(59) 0.0002873 1606. 1751.
1798(59) 0.0002873 1605. 1758.
1710(58) 0.0002973 1604. 1754.
1659(57) 0.0003078 1603. 1744.
1684(57) 0.0003078 1602. 1737.
1698(57) 0.0003078 1601. 1739.
1718(58) 0.0002973 1600. 1748.
1672(57) 0.0003078 1600. 1759.
1618(56) 0.0003189 1599. 1766.
1639(56) 0.0003189 1598. 1758.
1607(56) 0.0003189 1597. 1734.
1578(55) 0.0003306 1596. 1704.
1642(56) 0.0003189 1595. 1678.
1641(56) 0.0003189 1594. 1660.
1602(56) 0.0003189 1593. 1650.
1625(56) 0.0003189 1592. 1646.
1747(58) 0.0002973 1591. 1645.
1722(58) 0.0002973 1590. 1648.
1626(56) 0.0003189 1589. 1655.
1607(56) 0.0003189 1588. 1666.
1599(55) 0.0003306 1587. 1684.
1701(58) 0.0002973 1586. 1708.
1813(60) 0.0002778 1585. 1739.
1791(59) 0.0002873 1584. 1780.
1794(59) 0.0002873 1583. 1834.
1717(77) 0.0001687 1582. 1902.
2045(57) 0.0003078 1581. 1983.
2256(61) 0.0002687 1580. 2082.
2271(61) 0.0002687 1579. 2191.
2357(62) 0.0002601 1577. 2286.
2401(63) 0.0002520 1576. 2337.
2254(61) 0.0002687 1575. 2302.
2287(61) 0.0002687 1574. 2178.
2100(58) 0.0002973 1573. 2023.
2002(62) 0.0002601 1572. 1890.
1902(60) 0.0002778 1571. 1797.
1803(58) 0.0002973 1570. 1742.
1771(57) 0.0003078 1568. 1715.
1760(57) 0.0003078 1567. 1709.
1851(59) 0.0002873 1566. 1716.
1860(59) 0.0002873 1565. 1733.
1830(59) 0.0002873 1564. 1760.
1877(59) 0.0002873 1563. 1799.
1877(59) 0.0002873 1562. 1855.
1873(59) 0.0002873 1560. 1923.
1935(60) 0.0002778 1559. 1998.
2097(63) 0.0002520 1558. 2077.
2085(63) 0.0002520 1557. 2139.
2058(62) 0.0002601 1556. 2149.
2004(62) 0.0002601 1554. 2088.
2009(62) 0.0002601 1553. 1977.
1855(59) 0.0002873 1552. 1862.
1829(59) 0.0002873 1551. 1773.
1739(57) 0.0003078 1550. 1713.
1690(56) 0.0003189 1548. 1677.
1639(55) 0.0003306 1547. 1658.
1685(56) 0.0003189 1546. 1648.
1624(55) 0.0003306 1545. 1644.
1594(54) 0.0003429 1543. 1644.
1613(54) 0.0003429 1542. 1648.
1598(54) 0.0003429 1541. 1656.
1572(54) 0.0003429 1540. 1669.
1715(56) 0.0003189 1538. 1689.
1691(56) 0.0003189 1537. 1722.
1774(58) 0.0002973 1536. 1771.
1823(58) 0.0002973 1535. 1844.
1944(61) 0.0002687 1534. 1943.
1975(61) 0.0002687 1532. 2072.
2296(66) 0.0002296 1531. 2239.
2567(71) 0.0001984 1530. 2466.
2863(75) 0.0001778 1529. 2749.
3189(79) 0.0001602 1527. 3060.
3464(83) 0.0001452 1526. 3378.
3711(86) 0.0001352 1525. 3630.
3749(86) 0.0001352 1524. 3681.
3460(83) 0.0001452 1522. 3455.
3072(78) 0.0001644 1521. 3029.
2706(73) 0.0001877 1520. 2586.
2320(67) 0.0002228 1519. 2236.
1944(61) 0.0002687 1518. 1997.
1817(58) 0.0002973 1516. 1849.
1695(56) 0.0003189 1515. 1761.
1720(57) 0.0003078 1514. 1709.
1612(54) 0.0003429 1513. 1677.
1524(53) 0.000356 1512. 1656.
1666(56) 0.0003189 1510. 1644.
1640(55) 0.0003306 1509. 1639.
1574(54) 0.0003429 1508. 1642.
1612(54) 0.0003429 1507. 1653.
1572(54) 0.0003429 1506. 1673.
1609(54) 0.0003429 1504. 1703.
1660(55) 0.0003306 1503. 1746.
1750(57) 0.0003078 1502. 1801.
1686(56) 0.0003189 1501. 1862.
1736(57) 0.0003078 1500. 1921.
1803(58) 0.0002973 1499. 1960.
1763(57) 0.0003078 1497. 1953.
1722(57) 0.0003078 1496. 1890.
1642(55) 0.0003306 1495. 1799.
1559(53) 0.000356 1494. 1712.
1583(54) 0.0003429 1493. 1646.
1609(54) 0.0003429 1492. 1602.
1533(53) 0.000356 1491. 1574.
1494(52) 0.000370 1489. 1558.
1604(54) 0.0003429 1488. 1549.
1612(54) 0.0003429 1487. 1544.
1559(53) 0.000356 1486. 1543.
1439(51) 0.000384 1485. 1544.
1647(55) 0.0003306 1484. 1548.
1678(56) 0.0003189 1483. 1555.
1631(55) 0.0003306 1482. 1565.
1602(54) 0.0003429 1481. 1575.
1681(56) 0.0003189 1480. 1583.
1598(54) 0.0003429 1479. 1586.
1574(54) 0.0003429 1478. 1577.
1573(54) 0.0003429 1476. 1559.
1539(53) 0.000356 1475. 1540.
1561(53) 0.000356 1474. 1523.
1437(51) 0.000384 1473. 1511.
1513(53) 0.000356 1472. 1503.
1508(52) 0.000370 1471. 1497.
1574(54) 0.0003429 1470. 1493.
1581(54) 0.0003429 1469. 1490.
1476(52) 0.000370 1468. 1488.
1496(52) 0.000370 1467. 1486.
1497(46) 0.000473 1466. 1484.
1496(46) 0.000473 1466. 1482.
1468(46) 0.000473 1465. 1481.
1495(46) 0.000473 1464. 1479.
1510(46) 0.000473 1463. 1478.
1471(46) 0.000473 1462. 1477.
1477(46) 0.000473 1461. 1476.
1479(46) 0.000473 1460. 1475.
1490(46) 0.000473 1459. 1474.
1421(45) 0.000494 1458. 1473.
1411(49) 0.000416 1457. 1472.
1378(48) 0.000434 1456. 1471.
1420(49) 0.000416 1456. 1470.
1513(51) 0.000384 1455. 1470.
1457(50) 0.000400 1454. 1469.
1501(51) 0.000384 1453. 1468.
1512(51) 0.000384 1452. 1468.
1479(50) 0.000400 1451. 1468.
1455(50) 0.000400 1450. 1467.
1483(50) 0.000400 1450. 1467.
1429(49) 0.000416 1449. 1467.
1415(49) 0.000416 1448. 1468.
1556(52) 0.000370 1447. 1468.
1452(50) 0.000400 1447. 1469.
1484(50) 0.000400 1446. 1470.
1563(52) 0.000370 1445. 1472.
1479(50) 0.000400 1444. 1475.
1464(50) 0.000400 1443. 1479.
1489(50) 0.000400 1443. 1485.
1562(52) 0.000370 1442. 1495.
1523(51) 0.000384 1441. 1510.
1547(52) 0.000370 1441. 1531.
1563(52) 0.000370 1440. 1560.
1556(52) 0.000370 1439. 1596.
1539(51) 0.000384 1438. 1642.
1608(53) 0.000356 1438. 1694.
1577(52) 0.000370 1437. 1738.
1564(52) 0.000370 1436. 1760.
1498(51) 0.000384 1436. 1747.
1601(52) 0.000370 1435. 1699.
1568(52) 0.000370 1435. 1640.
1530(51) 0.000384 1434. 1589.
1481(50) 0.000400 1433. 1553.
1516(51) 0.000384 1433. 1529.
1542(51) 0.000384 1432. 1515.
1591(52) 0.000370 1431. 1508.
1594(52) 0.000370 1431. 1507.
1538(51) 0.000384 1430. 1511.
1587(52) 0.000370 1430. 1521.
1677(54) 0.0003429 1429. 1540.
1730(55) 0.0003306 1429. 1571.
1736(55) 0.0003306 1428. 1617.
1745(55) 0.0003306 1428. 1684.
1873(57) 0.0003078 1427. 1770.
1900(58) 0.0002973 1426. 1876.
1943(58) 0.0002973 1426. 2000.
2047(60) 0.0002778 1425. 2112.
2051(60) 0.0002778 1425. 2173.
2048(60) 0.0002778 1424. 2150.
1949(58) 0.0002973 1424. 2038.
1854(57) 0.0003078 1423. 1888.
1778(56) 0.0003189 1423. 1752.
1734(55) 0.0003306 1422. 1650.
1587(52) 0.000370 1422. 1583.
1573(52) 0.000370 1422. 1542.
1549(52) 0.000370 1421. 1517.
1598(52) 0.000370 1421. 1503.
1475(50) 0.000400 1420. 1494.
1561(52) 0.000370 1420. 1488.
1561(52) 0.000370 1419. 1486.
1512(51) 0.000384 1419. 1485.
1438(49) 0.000416 1418. 1486.
1519(51) 0.000384 1418. 1490.
1497(51) 0.000384 1418. 1498.
1500(51) 0.000384 1417. 1510.
1548(52) 0.000370 1417. 1530.
1681(54) 0.0003429 1416. 1558.
1702(54) 0.0003429 1416. 1596.
1762(55) 0.0003306 1416. 1644.
1802(56) 0.0003189 1415. 1704.
1867(57) 0.0003078 1415. 1769.
1987(59) 0.0002873 1415. 1829.
2094(61) 0.0002687 1414. 1876.
2097(61) 0.0002687 1414. 1914.
2067(60) 0.0002778 1414. 1962.
2046(60) 0.0002778 1413. 2041.
2017(60) 0.0002778 1413. 2156.
2131(61) 0.0002687 1412. 2288.
2195(62) 0.0002601 1412. 2386.
2089(61) 0.0002687 1412. 2395.
2173(62) 0.0002601 1411. 2286.
1993(59) 0.0002873 1411. 2101.
1905(58) 0.0002973 1411. 1912.
1876(57) 0.0003078 1411. 1763.
1707(54) 0.0003429 1410. 1661.
1677(54) 0.0003429 1410. 1599.
1625(53) 0.000356 1410. 1566.
1608(53) 0.000356 1409. 1552.
1596(52) 0.000370 1409. 1549.
1577(52) 0.000370 1409. 1550.
1555(52) 0.000370 1408. 1549.
1648(48) 0.000434 1408. 1541.
1606(48) 0.000434 1408. 1525.
1571(47) 0.000453 1408. 1504.
1544(47) 0.000453 1407. 1485.
1541(47) 0.000453 1407. 1470.
1469(45) 0.000494 1407. 1459.
1448(45) 0.000494 1406. 1453.
1498(46) 0.000473 1406. 1449.
1520(51) 0.000384 1406. 1447.
1481(50) 0.000400 1406. 1447.
1465(50) 0.000400 1405. 1449.
1488(50) 0.000400 1405. 1453.
1510(50) 0.000400 1405. 1461.
1459(49) 0.000416 1405. 1472.
1536(51) 0.000384 1404. 1485.
1517(51) 0.000384 1404. 1499.
1493(50) 0.000400 1404. 1513.
1446(49) 0.000416 1404. 1522.
1508(50) 0.000400 1403. 1519.
1533(51) 0.000384 1403. 1506.
1494(50) 0.000400 1403. 1488.
1467(50) 0.000400 1403. 1473.
1577(52) 0.000370 1402. 1464.
1473(50) 0.000400 1402. 1461.
1538(51) 0.000384 1402. 1463.
1504(50) 0.000400 1402. 1473.
1461(49) 0.000416 1401. 1491.
1593(52) 0.000370 1401. 1519.
1555(51) 0.000384 1401. 1561.
1629(53) 0.000356 1401. 1614.
1610(52) 0.000370 1400. 1673.
1640(53) 0.000356 1400. 1731.
1651(53) 0.000356 1400. 1779.
1628(53) 0.000356 1400. 1793.
1683(54) 0.0003429 1399. 1754.
1611(52) 0.000370 1399. 1680.
1577(52) 0.000370 1399. 1604.
1632(53) 0.000356 1399. 1543.
1568(52) 0.000370 1398. 1499.
1517(51) 0.000384 1398. 1471.
1452(49) 0.000416 1398. 1454.
1484(50) 0.000400 1397. 1443.
1528(51) 0.000384 1397. 1436.
1460(49) 0.000416 1397. 1432.
1503(50) 0.000400 1397. 1428.
1479(50) 0.000400 1396. 1426.
1494(50) 0.000400 1396. 1424.
1466(50) 0.000400 1396. 1423.
1446(49) 0.000416 1396. 1422.
1520(51) 0.000384 1395. 1422.
1402(48) 0.000434 1395. 1422.
1468(50) 0.000400 1395. 1423.
1496(50) 0.000400 1394. 1425.
1469(50) 0.000400 1394. 1427.
1468(50) 0.000400 1394. 1432.
1431(49) 0.000416 1394. 1439.
1367(48) 0.000434 1393. 1448.
1405(48) 0.000434 1393. 1461.
1424(49) 0.000416 1393. 1476.
1450(49) 0.000416 1392. 1494.
1470(50) 0.000400 1392. 1515.
1507(50) 0.000400 1392. 1536.
1510(50) 0.000400 1391. 1558.
1517(51) 0.000384 1391. 1585.
1539(51) 0.000384 1391. 1615.
1580(52) 0.000370 1391. 1646.
1641(53) 0.000356 1390. 1669.
1689(54) 0.0003429 1390. 1670.
1617(52) 0.000370 1390. 1646.
1574(52) 0.000370 1389. 1615.
1581(52) 0.000370 1389. 1591.
1593(52) 0.000370 1388. 1577.
1595(52) 0.000370 1388. 1568.
1542(51) 0.000384 1388. 1556.
1490(50) 0.000400 1387. 1534.
1506(50) 0.000400 1387. 1506.
1465(50) 0.000400 1387. 1482.
1372(48) 0.000434 1386. 1464.
1455(49) 0.000416 1386. 1454.
1465(50) 0.000400 1386. 1450.
1382(48) 0.000434 1385. 1451.
1433(49) 0.000416 1385. 1455.
1452(49) 0.000416 1384. 1458.
1466(50) 0.000400 1384. 1458.
1431(49) 0.000416 1384. 1453.
1426(49) 0.000416 1383. 1443.
1392(48) 0.000434 1383. 1434.
1404(48) 0.000434 1382. 1425.
1427(49) 0.000416 1382. 1420.
1466(50) 0.000400 1382. 1417.
1430(49) 0.000416 1381. 1415.
1441(49) 0.000416 1381. 1415.
1452(49) 0.000416 1380. 1416.
1443(49) 0.000416 1380. 1419.
1458(49) 0.000416 1379. 1422.
1451(49) 0.000416 1379. 1428.
1492(50) 0.000400 1378. 1434.
1533(51) 0.000384 1378. 1442.
1569(52) 0.000370 1378. 1450.
1555(46) 0.000473 1377. 1458.
1566(46) 0.000473 1377. 1467.
1540(45) 0.000494 1376. 1481.
1500(45) 0.000494 1376. 1505.
1522(45) 0.000494 1375. 1544.
1596(46) 0.000473 1375. 1602.
1684(48) 0.000434 1374. 1678.
1707(48) 0.000434 1374. 1765.
1738(48) 0.000434 1373. 1849.
1857(50) 0.000400 1373. 1914.
1875(55) 0.0003306 1372. 1929.
1807(54) 0.0003429 1372. 1884.
1793(54) 0.0003429 1371. 1807.
1762(53) 0.000356 1370. 1730.
1768(53) 0.000356 1370. 1666.
1733(53) 0.000356 1369. 1616.
1673(52) 0.000370 1369. 1586.
1672(52) 0.000370 1368. 1579.
1663(51) 0.000384 1368. 1596.
1665(52) 0.000370 1367. 1640.
1706(52) 0.000370 1367. 1711.
1784(53) 0.000356 1366. 1807.
1903(55) 0.0003306 1365. 1916.
1871(55) 0.0003306 1365. 2020.
1926(56) 0.0003189 1364. 2097.
2011(57) 0.0003078 1364. 2107.
1973(56) 0.0003189 1363. 2027.
1866(55) 0.0003306 1362. 1891.
1776(53) 0.000356 1362. 1753.
1724(53) 0.000356 1361. 1639.
1591(50) 0.000400 1361. 1558.
1501(49) 0.000416 1360. 1503.
1509(49) 0.000416 1359. 1469.
1515(49) 0.000416 1359. 1448.
1519(49) 0.000416 1358. 1436.
1505(49) 0.000416 1357. 1428.
1472(48) 0.000434 1357. 1426.
1444(48) 0.000434 1356. 1427.
1422(47) 0.000453 1355. 1434.
1393(47) 0.000453 1355. 1446.
1478(48) 0.000434 1354. 1464.
1507(49) 0.000416 1353. 1484.
1494(49) 0.000416 1353. 1502.
1502(49) 0.000416 1352. 1512.
1569(50) 0.000400 1351. 1506.
1508(49) 0.000416 1350. 1485.
1515(49) 0.000416 1350. 1458.
1514(49) 0.000416 1349. 1434.
1373(46) 0.000473 1348. 1414.
1452(48) 0.000434 1348. 1401.
1499(49) 0.000416 1347. 1392.
1381(46) 0.000473 1346. 1387.
1349(46) 0.000473 1345. 1385.
1391(47) 0.000453 1345. 1385.
1458(48) 0.000434 1344. 1387.
1457(48) 0.000434 1343. 1392.
1476(48) 0.000434 1342. 1402.
1449(48) 0.000434 1341. 1416.
1434(47) 0.000453 1341. 1437.
1512(49) 0.000416 1340. 1461.
1548(49) 0.000416 1339. 1487.
1564(50) 0.000400 1338. 1509.
1491(48) 0.000434 1338. 1520.
1526(49) 0.000416 1337. 1517.
1487(48) 0.000434 1336. 1507.
1503(49) 0.000416 1335. 1501.
1514(49) 0.000416 1334. 1504.
1536(49) 0.000416 1334. 1514.
1522(49) 0.000416 1333. 1524.
1446(48) 0.000434 1332. 1528.
1473(48) 0.000434 1331. 1520.
1439(48) 0.000434 1330. 1503.
1410(47) 0.000453 1329. 1484.
1367(46) 0.000473 1329. 1461.
1404(47) 0.000453 1328. 1436.
1432(47) 0.000453 1327. 1412.
1349(46) 0.000473 1326. 1391.
1311(45) 0.000494 1325. 1376.
1344(46) 0.000473 1324. 1366.
1324(45) 0.000494 1323. 1359.
1345(46) 0.000473 1323. 1354.
1349(46) 0.000473 1322. 1350.
1344(46) 0.000473 1321. 1348.
1273(44) 0.000517 1320. 1345.
1343(46) 0.000473 1319. 1343.
1407(47) 0.000453 1318. 1342.
1356(46) 0.000473 1317. 1341.
1299(45) 0.000494 1316. 1342.
1295(45) 0.000494 1316. 1342.
1317(45) 0.000494 1315. 1343.
1297(45) 0.000494 1314. 1342.
1367(46) 0.000473 1313. 1340.
1365(46) 0.000473 1312. 1337.
1306(45) 0.000494 1311. 1334.
1297(45) 0.000494 1310. 1332.
1289(45) 0.000494 1309. 1330.
1314(45) 0.000494 1308. 1328.
1334(46) 0.000473 1307. 1328.
1346(46) 0.000473 1306. 1328.
1339(46) 0.000473 1305. 1329.
1322(35) 0.000816 1304.5 1331.2
1301(39) 0.000657 1304. 1335.
1363(40) 0.000625 1303. 1341.
1369(40) 0.000625 1302. 1351.
1343(40) 0.000625 1301. 1363.
1300(39) 0.000657 1300. 1377.
1323(39) 0.000657 1299. 1391.
1330(39) 0.000657 1298. 1401.
1349(40) 0.000625 1297. 1405.
1398(44) 0.000517 1296. 1402.
1398(44) 0.000517 1295. 1397.
1361(44) 0.000517 1294. 1395.
1429(45) 0.000494 1293. 1397.
1462(45) 0.000494 1292. 1400.
1497(46) 0.000473 1291. 1401.
1493(46) 0.000473 1290. 1396.
1434(45) 0.000494 1289. 1387.
1446(45) 0.000494 1288. 1376.
1415(44) 0.000517 1287. 1367.
1377(44) 0.000517 1286. 1361.
1447(45) 0.000494 1285. 1361.
1392(44) 0.000517 1285. 1368.
1499(46) 0.000473 1284. 1385.
1514(46) 0.000473 1283. 1415.
1486(46) 0.000473 1282. 1463.
1521(46) 0.000473 1281. 1531.
1549(47) 0.000453 1280. 1614.
1574(47) 0.000453 1279. 1700.
1644(48) 0.000434 1278. 1756.
1627(48) 0.000434 1277. 1750.
1666(48) 0.000434 1276. 1686.
1636(48) 0.000434 1275. 1601.
1591(47) 0.000453 1274. 1521.
1513(46) 0.000473 1273. 1460.
1426(45) 0.000494 1272. 1416.
1448(45) 0.000494 1271. 1386.
1461(45) 0.000494 1270. 1364.
1457(45) 0.000494 1269. 1349.
1396(44) 0.000517 1268. 1339.
1406(44) 0.000517 1267. 1333.
1421(45) 0.000494 1266. 1332.
1327(43) 0.000541 1265. 1336.
1292(42) 0.000567 1264. 1346.
1376(44) 0.000517 1263. 1362.
1353(43) 0.000541 1262. 1384.
1357(43) 0.000541 1261. 1408.
1417(44) 0.000517 1260. 1426.
1430(45) 0.000494 1259. 1431.
1387(44) 0.000517 1258. 1421.
1447(45) 0.000494 1257. 1406.
1414(44) 0.000517 1256. 1398.
1485(46) 0.000473 1255. 1401.
1509(46) 0.000473 1254. 1421.
1465(45) 0.000494 1253. 1457.
1460(45) 0.000494 1252. 1507.
1542(47) 0.000453 1251. 1559.
1549(47) 0.000453 1250. 1597.
1575(47) 0.000453 1249. 1609.
1629(48) 0.000434 1248. 1601.
1570(47) 0.000453 1247. 1578.
1542(47) 0.000453 1246. 1539.
1498(46) 0.000473 1245. 1486.
1464(45) 0.000494 1245. 1432.
1375(44) 0.000517 1244. 1387.
1352(43) 0.000541 1243. 1353.
1394(44) 0.000517 1242. 1329.
1378(44) 0.000517 1241. 1314.
1402(44) 0.000517 1240. 1306.
1422(45) 0.000494 1239. 1302.
1393(44) 0.000517 1238. 1304.
1317(43) 0.000541 1237. 1310.
1418(45) 0.000494 1236. 1322.
1378(44) 0.000517 1235. 1340.
1431(45) 0.000494 1234. 1365.
1378(44) 0.000517 1233. 1392.
1381(44) 0.000517 1232. 1415.
1528(46) 0.000473 1231. 1429.
1523(46) 0.000473 1230. 1434.
1551(47) 0.000453 1229. 1438.
1590(47) 0.000453 1228. 1443.
1649(48) 0.000434 1227. 1443.
1625(48) 0.000434 1227. 1433.
1527(46) 0.000473 1226. 1415.
1514(46) 0.000473 1225. 1402.
1503(46) 0.000473 1224. 1401.
1528(46) 0.000473 1223. 1416.
1537(46) 0.000473 1222. 1444.
1508(46) 0.000473 1221. 1478.
1429(45) 0.000494 1220. 1502.
1490(46) 0.000473 1219. 1505.
1495(46) 0.000473 1218. 1486.
1509(46) 0.000473 1217. 1456.
1415(44) 0.000517 1217. 1417.
1414(44) 0.000517 1216. 1375.
1376(44) 0.000517 1215. 1337.
1423(45) 0.000494 1214. 1308.
1317(43) 0.000541 1213. 1286.
1332(43) 0.000541 1212. 1270.
1324(43) 0.000541 1211. 1260.
1331(43) 0.000541 1210. 1252.
1255(36) 0.000772 1210. 1247.
1254(36) 0.000772 1209. 1243.
1237(36) 0.000772 1208. 1241.
1281(36) 0.000772 1207. 1239.
1280(36) 0.000772 1206. 1238.
1289(37) 0.000730 1205. 1237.
1283(36) 0.000772 1204. 1238.
1261(36) 0.000772 1204. 1239.
1262(36) 0.000772 1203. 1242.
1341(41) 0.000595 1202. 1246.
1310(40) 0.000625 1201. 1254.
1292(40) 0.000625 1200. 1267.
1269(40) 0.000625 1199. 1287.
1301(40) 0.000625 1199. 1315.
1348(41) 0.000595 1198. 1351.
1371(41) 0.000595 1197. 1394.
1391(42) 0.000567 1196. 1434.
1373(41) 0.000595 1195. 1456.
1396(42) 0.000567 1195. 1451.
1422(42) 0.000567 1194. 1428.
1370(41) 0.000595 1193. 1403.
1344(41) 0.000595 1192. 1388.
1370(41) 0.000595 1191. 1386.
1372(41) 0.000595 1191. 1393.
1352(41) 0.000595 1190. 1399.
1342(41) 0.000595 1189. 1394.
1337(41) 0.000595 1188. 1377.
1361(41) 0.000595 1188. 1358.
1360(41) 0.000595 1187. 1344.
1352(41) 0.000595 1186. 1338.
1284(40) 0.000625 1185. 1338.
1285(40) 0.000625 1185. 1336.
1289(40) 0.000625 1184. 1330.
1313(40) 0.000625 1183. 1319.
1363(41) 0.000595 1182. 1308.
1334(41) 0.000595 1182. 1298.
1302(40) 0.000625 1181. 1285.
1340(41) 0.000595 1180. 1271.
1308(40) 0.000625 1179. 1255.
1229(39) 0.000657 1179. 1240.
1266(39) 0.000657 1178. 1227.
1212(39) 0.000657 1177. 1217.
1207(38) 0.000693 1177. 1210.
1208(38) 0.000693 1176. 1204.
1185(38) 0.000693 1175. 1200.
1181(38) 0.000693 1175. 1196.
1192(38) 0.000693 1174. 1194.
1181(38) 0.000693 1173. 1192.
1177(38) 0.000693 1173. 1191.
1203(38) 0.000693 1172. 1190.
1194(38) 0.000693 1171. 1189.
1159(38) 0.000693 1171. 1188.
1158(38) 0.000693 1170. 1188.
1192(38) 0.000693 1169. 1188.
1187(38) 0.000693 1169. 1189.
1197(38) 0.000693 1168. 1190.
1196(38) 0.000693 1167. 1192.
1224(39) 0.000657 1167. 1197.
1216(39) 0.000657 1166. 1203.
1206(38) 0.000693 1166. 1212.
1189(38) 0.000693 1165. 1224.
1150(37) 0.000730 1164. 1238.
1232(39) 0.000657 1164. 1252.
1240(39) 0.000657 1163. 1263.
1244(39) 0.000657 1163. 1268.
1211(39) 0.000657 1162. 1271.
1239(39) 0.000657 1161. 1277.
1234(39) 0.000657 1161. 1285.
1274(40) 0.000625 1160. 1295.
1258(39) 0.000657 1160. 1299.
1252(39) 0.000657 1159. 1293.
1245(39) 0.000657 1159. 1275.
1181(38) 0.000693 1158. 1254.
1214(39) 0.000657 1158. 1233.
1194(38) 0.000693 1157. 1217.
1154(37) 0.000730 1156. 1204.
1215(39) 0.000657 1156. 1195.
1226(39) 0.000657 1155. 1189.
1227(39) 0.000657 1155. 1184.
1215(39) 0.000657 1154. 1181.
1199(38) 0.000693 1154. 1180.
1207(38) 0.000693 1153. 1180.
1234(39) 0.000657 1153. 1182.
1168(38) 0.000693 1152. 1186.
1135(37) 0.000730 1152. 1192.
1180(38) 0.000693 1151. 1201.
1204(38) 0.000693 1151. 1211.
1192(38) 0.000693 1150. 1221.
1202(38) 0.000693 1150. 1225.
1202(38) 0.000693 1149. 1223.
1178(38) 0.000693 1149. 1216.
1175(38) 0.000693 1149. 1206.
1200(38) 0.000693 1148. 1197.
1177(38) 0.000693 1148. 1189.
1172(38) 0.000693 1147. 1182.
1145(37) 0.000730 1147. 1176.
1164(38) 0.000693 1146. 1172.
1174(38) 0.000693 1146. 1169.
1180(38) 0.000693 1145. 1168.
1151(37) 0.000730 1145. 1168.
1179(33) 0.000918 1144.6 1169.3
1145(32) 0.000977 1144.1 1171.9
1182(33) 0.000918 1143.7 1175.9
1222(34) 0.000865 1143.3 1181.3
1226(34) 0.000865 1142.9 1187.8
1179(33) 0.000918 1142.5 1194.9
1178(33) 0.000918 1142.1 1201.6
1209(33) 0.000918 1141.7 1207.1
1204(33) 0.000918 1141.4 1212.0
1182(36) 0.000772 1141. 1218.
1206(36) 0.000772 1141. 1227.
1192(36) 0.000772 1140. 1237.
1218(37) 0.000730 1140. 1247.
1245(37) 0.000730 1139. 1253.
1276(38) 0.000693 1139. 1257.
1276(37) 0.000730 1139. 1256.
1244(37) 0.000730 1138. 1252.
1253(37) 0.000730 1138. 1248.
1257(37) 0.000730 1138. 1249.
1286(38) 0.000693 1137. 1255.
1304(38) 0.000693 1137. 1266.
1293(38) 0.000693 1137. 1276.
1273(37) 0.000730 1136. 1279.
1267(37) 0.000730 1136. 1273.
1218(37) 0.000730 1136. 1261.
1256(37) 0.000730 1135. 1250.
1249(37) 0.000730 1135. 1243.
1179(36) 0.000772 1135. 1239.
1187(36) 0.000772 1134. 1237.
1223(37) 0.000730 1134. 1230.
1185(36) 0.000772 1134. 1219.
1166(36) 0.000772 1134. 1205.
1195(36) 0.000772 1133. 1193.
1136(35) 0.000816 1133.0 1181.8
1138(35) 0.000816 1132.7 1173.5
1204(36) 0.000772 1132. 1168.
1219(37) 0.000730 1132. 1164.
1230(37) 0.000730 1132. 1162.
1191(36) 0.000772 1132. 1162.
1158(36) 0.000772 1131. 1163.
1127(35) 0.000816 1131.1 1166.7
1198(36) 0.000772 1131. 1173.
1224(37) 0.000730 1131. 1183.
1307(38) 0.000693 1130. 1198.
1262(37) 0.000730 1130. 1218.
1267(37) 0.000730 1130. 1243.
1313(38) 0.000693 1130. 1268.
1275(37) 0.000730 1129. 1289.
1339(39) 0.000657 1129. 1298.
1325(38) 0.000693 1129. 1292.
1278(38) 0.000693 1129. 1276.
1300(38) 0.000693 1128. 1254.
1275(38) 0.000693 1128. 1231.
1219(37) 0.000730 1128. 1209.
1210(36) 0.000772 1128. 1191.
1216(37) 0.000730 1127. 1177.
1192(36) 0.000772 1127. 1167.
1174(36) 0.000772 1127. 1160.
1145(35) 0.000816 1126.8 1154.8
1180(36) 0.000772 1127. 1152.
1234(37) 0.000730 1126. 1151.
1206(36) 0.000772 1126. 1150.
1145(35) 0.000816 1126.0 1150.8
1154(36) 0.000772 1126. 1152.
1136(35) 0.000816 1125.6 1153.4
1128(35) 0.000816 1125.4 1154.5
1128(35) 0.000816 1125.2 1154.9
1164(36) 0.000772 1125. 1155.
1218(37) 0.000730 1125. 1156.
1133(35) 0.000816 1124.6 1159.3
1150(35) 0.000816 1124.4 1164.3
1228(37) 0.000730 1124. 1172.
1193(36) 0.000772 1124. 1181.
1196(36) 0.000772 1124. 1192.
1171(36) 0.000772 1124. 1202.
1163(36) 0.000772 1124. 1209.
1173(36) 0.000772 1123. 1209.
1178(36) 0.000772 1123. 1204.
1200(36) 0.000772 1123. 1195.
1132(35) 0.000816 1122.8 1184.1
1132(35) 0.000816 1122.7 1172.7
1140(35) 0.000816 1122.5 1162.8
1137(35) 0.000816 1122.4 1155.1
1160(36) 0.000772 1122. 1150.
1180(36) 0.000772 1122. 1146.
1171(36) 0.000772 1122. 1143.
1133(35) 0.000816 1121.7 1141.9
1157(36) 0.000772 1122. 1141.
1168(36) 0.000772 1121. 1141.
1125(35) 0.000816 1121.3 1141.5
1134(35) 0.000816 1121.1 1142.5
1149(35) 0.000816 1121.0 1144.2
1155(36) 0.000772 1121. 1147.
1165(36) 0.000772 1121. 1151.
1169(36) 0.000772 1121. 1158.
1190(36) 0.000772 1120. 1167.
1172(36) 0.000772 1120. 1179.
1200(36) 0.000772 1120. 1195.
1235(37) 0.000730 1120. 1213.
1246(37) 0.000730 1120. 1230.
1253(33) 0.000918 1119.7 1241.9
1245(33) 0.000918 1119.5 1242.9
1225(32) 0.000977 1119.4 1233.7
1242(32) 0.000977 1119.3 1219.5
1243(32) 0.000977 1119.1 1205.4
1277(33) 0.000918 1119.0 1194.5
1203(32) 0.000977 1118.9 1188.0
1185(32) 0.000977 1118.7 1186.2
1231(32) 0.000977 1118.6 1189.5
1173(34) 0.000865 1118.5 1197.7
1173(34) 0.000865 1118.3 1210.9
1194(35) 0.000816 1118.2 1228.8
1258(36) 0.000772 1118. 1251.
1269(36) 0.000772 1118. 1279.
1293(36) 0.000772 1118. 1314.
1338(37) 0.000730 1118. 1353.
1388(38) 0.000693 1118. 1392.
1387(38) 0.000693 1117. 1417.
1383(37) 0.000730 1117. 1416.
1354(37) 0.000730 1117. 1390.
1325(37) 0.000730 1117. 1348.
1276(36) 0.000772 1117. 1303.
1320(37) 0.000730 1117. 1262.
1193(35) 0.000816 1116.7 1228.3
1201(35) 0.000816 1116.5 1203.1
1214(35) 0.000816 1116.4 1185.5
1173(34) 0.000865 1116.3 1174.1
1173(34) 0.000865 1116.2 1167.3
1159(34) 0.000865 1116.0 1163.9
1207(35) 0.000816 1115.9 1163.0
1155(34) 0.000865 1115.8 1164.1
1163(34) 0.000865 1115.7 1166.4
1176(34) 0.000865 1115.5 1169.1
1200(35) 0.000816 1115.4 1171.1
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1144(34) 0.000865 1115.0 1172.7
1221(35) 0.000816 1114.9 1175.6
1228(35) 0.000816 1114.8 1182.0
1260(36) 0.000772 1115. 1193.
1192(35) 0.000816 1114.5 1209.6
1206(35) 0.000816 1114.4 1232.7
1256(36) 0.000772 1114. 1262.
1315(37) 0.000730 1114. 1298.
1322(37) 0.000730 1114. 1334.
1312(36) 0.000772 1114. 1365.
1329(37) 0.000730 1114. 1388.
1382(37) 0.000730 1114. 1406.
1412(38) 0.000693 1113. 1419.
1418(38) 0.000693 1113. 1423.
1403(38) 0.000693 1113. 1411.
1377(37) 0.000730 1113. 1379.
1364(37) 0.000730 1113. 1337.
1297(36) 0.000772 1113. 1294.
1249(36) 0.000772 1113. 1258.
1329(37) 0.000730 1112. 1229.
1247(36) 0.000772 1112. 1209.
1250(36) 0.000772 1112. 1195.
1200(35) 0.000816 1112.1 1186.6
1208(35) 0.000816 1111.9 1180.9
1154(34) 0.000865 1111.8 1176.9
1136(34) 0.000865 1111.6 1174.4
1214(35) 0.000816 1111.5 1174.2
1191(35) 0.000816 1111.3 1176.5
1130(34) 0.000865 1111.2 1181.3
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1170(34) 0.000865 1110.9 1194.3
1172(34) 0.000865 1110.7 1198.3
1172(34) 0.000865 1110.6 1198.4
1213(35) 0.000816 1110.4 1195.3
1198(35) 0.000816 1110.3 1191.0
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1173(34) 0.000865 1109.8 1182.4
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1187(35) 0.000816 1109.5 1185.5
1206(35) 0.000816 1109.3 1192.3
1237(35) 0.000816 1109.2 1204.2
1264(36) 0.000772 1109. 1222.
1272(36) 0.000772 1109. 1247.
1354(37) 0.000730 1109. 1278.
1329(37) 0.000730 1109. 1311.
1272(36) 0.000772 1108. 1339.
1293(36) 0.000772 1108. 1355.
1359(37) 0.000730 1108. 1357.
1406(38) 0.000693 1108. 1344.
1316(37) 0.000730 1108. 1319.
1323(37) 0.000730 1107. 1288.
1345(37) 0.000730 1107. 1257.
1257(36) 0.000772 1107. 1231.
1247(36) 0.000772 1107. 1212.
1276(36) 0.000772 1107. 1201.
1303(36) 0.000772 1107. 1197.
1238(35) 0.000816 1106.4 1199.1
1263(36) 0.000772 1106. 1205.
1276(36) 0.000772 1106. 1214.
1213(35) 0.000816 1105.8 1223.0
1271(36) 0.000772 1106. 1231.
1236(35) 0.000816 1105.4 1233.5
1264(36) 0.000772 1105. 1230.
1239(31) 0.001041 1105.0 1220.4
1215(31) 0.001041 1104.8 1208.0
1244(31) 0.001041 1104.6 1196.4
1194(31) 0.001041 1104.4 1187.8
1209(31) 0.001041 1104.2 1183.1
1229(31) 0.001041 1104.0 1181.7
1264(32) 0.000977 1103.8 1181.7
1198(31) 0.001041 1103.6 1180.3
1182(31) 0.001041 1103.4 1175.5
1199(34) 0.000865 1103.2 1167.7
1179(33) 0.000918 1103.0 1158.7
1192(33) 0.000918 1102.8 1150.3
1192(33) 0.000918 1102.5 1143.3
1191(33) 0.000918 1102.3 1137.7
1164(33) 0.000918 1102.1 1133.2
1113(32) 0.000977 1101.9 1129.4
1154(33) 0.000918 1101.7 1126.2
1152(33) 0.000918 1101.4 1123.4
1080(32) 0.000977 1101.2 1121.2
1157(33) 0.000918 1101.0 1119.5
1107(32) 0.000977 1100.8 1118.3
1119(32) 0.000977 1100.5 1117.6
1139(33) 0.000918 1100.3 1117.4
1183(33) 0.000918 1100.1 1117.7
1128(33) 0.000918 1099.8 1118.8
1173(33) 0.000918 1099.6 1120.8
1097(32) 0.000977 1099.3 1124.0
1105(32) 0.000977 1099.1 1128.6
1158(33) 0.000918 1098.9 1135.0
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1139(33) 0.000918 1098.4 1151.8
1207(34) 0.000865 1098.1 1160.4
1174(33) 0.000918 1097.9 1166.2
1194(34) 0.000865 1097.6 1166.9
1241(34) 0.000865 1097.4 1162.2
1259(34) 0.000865 1097.1 1154.1
1295(35) 0.000816 1096.9 1145.0
1244(34) 0.000865 1096.6 1136.7
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1232(34) 0.000865 1095.5 1120.2
1119(32) 0.000977 1095.3 1120.3
1184(33) 0.000918 1095.0 1121.5
1087(32) 0.000977 1094.7 1123.5
1032(31) 0.001041 1094.5 1125.5
1122(32) 0.000977 1094.2 1126.6
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1068(32) 0.000977 1093.4 1120.9
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1129(33) 0.000918 1092.5 1114.0
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1076(32) 0.000977 1092.0 1114.2
1078(32) 0.000977 1091.7 1116.2
1089(32) 0.000977 1091.4 1119.6
1134(33) 0.000918 1091.1 1124.5
1151(33) 0.000918 1090.8 1130.8
1076(32) 0.000977 1090.5 1138.2
1104(32) 0.000977 1090.2 1145.7
1167(33) 0.000918 1089.9 1151.9
1147(33) 0.000918 1089.6 1154.7
1164(33) 0.000918 1089.3 1153.6
1116(32) 0.000977 1089.0 1150.1
1087(32) 0.000977 1088.7 1146.2
1165(33) 0.000918 1088.4 1143.4
1085(32) 0.000977 1088.1 1142.2
1142(33) 0.000918 1087.8 1142.6
1103(32) 0.000977 1087.5 1143.6
1121(32) 0.000977 1087.2 1144.5
1122(32) 0.000977 1086.9 1144.9
1166(33) 0.000918 1086.6 1145.7
1153(33) 0.000918 1086.2 1147.6
1228(34) 0.000865 1085.9 1150.4
1179(33) 0.000918 1085.6 1153.2
1110(32) 0.000977 1085.3 1154.3
1121(32) 0.000977 1085.0 1152.1
1166(33) 0.000918 1084.7 1146.7
1141(33) 0.000918 1084.3 1139.6
1145(33) 0.000918 1084.0 1132.6
1182(33) 0.000918 1083.7 1126.9
1103(32) 0.000977 1083.4 1123.0
1084(32) 0.000977 1083.0 1121.3
1159(33) 0.000918 1082.7 1122.1
1134(33) 0.000918 1082.4 1125.4
1130(33) 0.000918 1082.1 1131.3
1178(33) 0.000918 1081.7 1139.7
1205(34) 0.000865 1081.4 1150.4
1141(33) 0.000918 1081.1 1162.2
1216(34) 0.000865 1080.7 1173.4
1178(33) 0.000918 1080.4 1181.6
1125(32) 0.000977 1080.1 1185.0
1197(34) 0.000865 1079.7 1183.5
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1122(32) 0.000977 1078.7 1170.2
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1238(34) 0.000865 1078.0 1176.1
1205(34) 0.000865 1077.7 1186.5
1207(30) 0.001111 1077.4 1201.1
1226(30) 0.001111 1077.0 1217.4
1283(31) 0.001041 1076.7 1231.9
1272(31) 0.001041 1076.3 1241.3
1230(30) 0.001111 1076.0 1245.5
1221(30) 0.001111 1075.6 1246.3
1258(30) 0.001111 1075.3 1245.1
1255(30) 0.001111 1074.9 1240.5
1212(30) 0.001111 1074.6 1231.1
1225(33) 0.000918 1074.2 1217.5
1202(32) 0.000977 1073.9 1202.4
1243(33) 0.000918 1073.5 1188.5
1242(33) 0.000918 1073.2 1177.1
1168(32) 0.000977 1072.8 1168.7
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1219(33) 0.000918 1071.4 1180.4
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1253(33) 0.000918 1070.7 1216.7
1275(33) 0.000918 1070.4 1236.7
1207(32) 0.000977 1070.0 1251.2
1182(32) 0.000977 1069.6 1254.3
1187(32) 0.000977 1069.3 1244.2
1239(33) 0.000918 1068.9 1224.6
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1184(32) 0.000977 1068.2 1179.9
1126(31) 0.001041 1067.9 1161.5
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1147(32) 0.000977 1067.1 1137.0
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1107(31) 0.001041 1065.3 1128.2
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1122(31) 0.001041 1064.6 1134.4
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1149(32) 0.000977 1062.8 1130.3
1122(31) 0.001041 1062.5 1122.9
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1105(31) 0.001041 1061.7 1109.6
1121(31) 0.001041 1061.4 1104.6
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1135(31) 0.001041 1058.1 1107.8
1091(31) 0.001041 1057.8 1112.8
1103(31) 0.001041 1057.4 1119.3
1165(32) 0.000977 1057.1 1127.4
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1145(32) 0.000977 1056.4 1144.0
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1112(31) 0.001041 1049.6 1125.6
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1181(32) 0.000977 1048.6 1150.7
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1122(31) 0.001041 1047.6 1145.4
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1089(31) 0.001041 1046.6 1123.1
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1080(31) 0.001041 1045.5 1095.1
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1065(30) 0.001111 1044.9 1081.1
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1056(30) 0.001111 1043.9 1068.2
1067(30) 0.001111 1043.5 1065.8
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1056(30) 0.001111 1042.9 1062.8
1085(31) 0.001041 1042.5 1062.2
1066(39) 0.000657 1042. 1062.
1072(27) 0.001372 1041.9 1062.2
1081(27) 0.001372 1041.6 1062.7
1045(27) 0.001372 1041.2 1063.6
1055(27) 0.001372 1040.9 1064.9
1072(27) 0.001372 1040.6 1066.6
1089(27) 0.001372 1040.3 1069.0
1090(27) 0.001372 1039.9 1072.4
1042(27) 0.001372 1039.6 1076.7
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1066(30) 0.001111 1038.7 1093.7
1084(30) 0.001111 1038.4 1098.7
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1119(30) 0.001111 1037.7 1104.4
1135(31) 0.001041 1037.4 1105.1
1128(30) 0.001111 1037.1 1105.4
1138(31) 0.001041 1036.8 1106.4
1121(30) 0.001111 1036.5 1109.1
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1186(31) 0.001041 1035.3 1145.4
1196(31) 0.001041 1035.0 1160.2
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1172(31) 0.001041 1031.8 1125.3
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1159(31) 0.001041 1029.8 1098.3
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1125(30) 0.001111 1028.5 1085.3
1109(30) 0.001111 1028.2 1079.6
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1104(30) 0.001111 1027.7 1070.8
1102(30) 0.001111 1027.4 1068.0
1104(30) 0.001111 1027.1 1066.4
1107(30) 0.001111 1026.9 1065.8
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1106(30) 0.001111 1025.1 1063.7
1116(30) 0.001111 1024.8 1064.9
1077(30) 0.001111 1024.6 1067.5
1097(30) 0.001111 1024.4 1071.8
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1183(31) 0.001041 1020.6 1199.3
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1204(31) 0.001041 1020.2 1242.7
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1242(32) 0.000977 1019.8 1249.3
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1078(30) 0.001111 1017.9 1080.5
1086(30) 0.001111 1017.7 1073.7
1104(30) 0.001111 1017.5 1068.3
1078(30) 0.001111 1017.3 1064.2
1084(30) 0.001111 1017.1 1061.5
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1073(27) 0.001372 1015.4 1055.1
1103(28) 0.001276 1015.2 1055.3
1065(27) 0.001372 1015.0 1056.4
1064(27) 0.001372 1014.9 1058.4
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1054(27) 0.001372 1014.5 1064.1
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1191(31) 0.001041 1151.7 1205.3
1189(31) 0.001041 1151.1 1204.4
1135(30) 0.001111 1150.3 1203.7
1165(31) 0.001041 1149.6 1203.0
1181(31) 0.001041 1148.9 1202.5
1198(31) 0.001041 1148.1 1202.0
1211(31) 0.001041 1147.4 1201.6
1253(32) 0.000977 1146.6 1201.2
1234(32) 0.000977 1145.8 1200.8
1201(31) 0.001041 1145.0 1200.4
1211(31) 0.001041 1144.2 1200.0
1201(31) 0.001041 1143.4 1199.6
1191(31) 0.001041 1142.6 1199.1
1216(31) 0.001041 1141.8 1198.6
1216(31) 0.001041 1141.0 1198.0
1217(31) 0.001041 1140.1 1197.4
1202(31) 0.001041 1139.3 1196.7
1194(31) 0.001041 1138.5 1195.9
1204(31) 0.001041 1137.7 1195.1
1196(31) 0.001041 1136.9 1194.3
1176(31) 0.001041 1136.1 1193.5
1202(31) 0.001041 1135.3 1192.7
1163(31) 0.001041 1134.6 1191.9
1146(30) 0.001111 1133.8 1191.0
1147(30) 0.001111 1133.1 1190.2
1153(31) 0.001041 1132.4 1189.3
1193(31) 0.001041 1131.7 1188.4
1163(31) 0.001041 1131.0 1187.4
1186(31) 0.001041 1130.4 1186.4
1205(31) 0.001041 1129.7 1185.3
1224(31) 0.001041 1129.2 1184.2
1129(30) 0.001111 1128.6 1183.0
1170(31) 0.001041 1128.1 1181.8
1186(31) 0.001041 1127.6 1180.5
1168(31) 0.001041 1127.2 1179.2
1136(30) 0.001111 1126.8 1177.8
1137(30) 0.001111 1126.5 1176.4
1180(31) 0.001041 1126.2 1175.1
1154(31) 0.001041 1126.0 1173.8
1154(31) 0.001041 1125.8 1172.6
1163(31) 0.001041 1125.8 1171.4
1166(31) 0.001041 1125.7 1170.4
1166(31) 0.001041 1125.8 1169.6
1163(31) 0.001041 1125.9 1169.0
1175(31) 0.001041 1126.1 1168.5
1183(31) 0.001041 1126.4 1168.3
1183(31) 0.001041 1126.8 1168.3
1164(31) 0.001041 1127.3 1168.5
1185(31) 0.001041 1127.9 1169.0
1194(31) 0.001041 1128.6 1169.8
1158(31) 0.001041 1129.4 1170.8
1129(30) 0.001111 1130.3 1172.1
1109(30) 0.001111 1131.4 1173.6
1193(31) 0.001041 1132.6 1175.4
1211(31) 0.001041 1133.9 1177.5
1157(31) 0.001041 1135.4 1179.7
1171(31) 0.001041 1137.0 1182.2
1177(31) 0.001041 1138.7 1184.9
1156(31) . . .
1175(31) . . .
1181(31) . . .
1120(30) . . .
1068(29) . . .
1143(30) . . .
1157(31) . . .
1161(31) . . .
1206(31) . . .
1126(30) . . .
1159(31) . . .
1200(31) . . .
1166(31) . . .
1155(31) . . .
1190(31) . . .
1195(31) . . .
1221(31) . . .
1201(31) . . .
1173(31) . . .
1207(31) . . .
1181(31) . . .
1176(31) . . .
1152(31) . . .
1178(31) . . .
1218(31) . . .
1209(31) . . .
1166(31) . . .
1170(29) . . .
1209(29) . . .
1227(29) . . .
1232(29) . . .
1177(29) . . .
1164(29) . . .
1166(29) . . .
1151(28) . . .
1172(31) . . .
1167(31) . . .
1193(32) . . .
1184(31) . . .
1163(31) . . .
1183(31) . . .
1184(31) . . .
1179(31) . . .
1194(32) . . .
1201(32) . . .
1198(32) . . .
1199(32) . . .
1214(32) . . .
1180(31) . . .
1153(31) . . .
1151(31) . . .
1187(32) . . .
1220(32) . . .
1148(31) . . .
1160(31) . . .
1199(32) . . .
1212(32) . . .
1224(32) . . .
1148(31) . . .
1208(32) . . .
1212(32) . . .
1234(32) . . .
1200(32) . . .
1177(31) . . .
1149(31) . . .
1174(31) . . .
1173(31) . . .
1191(32) . . .
1211(32) . . .
1175(31) . . .
1130(31) . . .
1180(31) . . .
1250(32) . . .
1188(32) . . .
1213(32) . . .
1184(31) . . .
1214(32) . . .
1228(32) . . .
1196(32) . . .
1237(32) . . .
1249(32) . . .
1174(31) . . .
1187(32) . . .
1176(31) . . .
1232(32) . . .
1221(32) . . .
1203(32) . . .
1252(32) . . .
1224(32) . . .
1213(32) . . .
1215(32) . . .
1251(32) . . .
1251(32) . . .
1197(32) . . .
1244(32) . . .
1206(32) . . .
1219(32) . . .
1219(32) . . .
1280(33) . . .
1284(33) . . .
1241(32) . . .
1218(32) . . .
1236(32) . . .
1224(32) . . .
1246(32) . . .
1244(32) . . .
1250(32) . . .
1227(32) . . .
1241(32) . . .
1217(32) . . .
1244(32) . . .
1281(33) . . .
1272(33) . . .
1223(32) . . .
1200(32) . . .
1216(32) . . .
1235(32) . . .
1209(32) . . .
1232(32) . . .
1258(32) . . .
1234(32) . . .
1220(32) . . .
1239(32) . . .
1262(32) . . .
1272(33) . . .
1258(32) . . .
1201(30) . . .
1212(30) . . .
1244(30) . . .
1220(30) . . .
1251(30) . . .
1223(30) . . .
1246(30) . . .
1282(31) . . .
1278(30) . . .
1237(30) . . .
1253(33) . . .
1279(34) . . .
1231(33) . . .
1288(34) . . .
1300(34) . . .
1258(33) . . .
1286(34) . . .
1289(34) . . .
1254(33) . . .
1277(34) . . .
1249(33) . . .
1242(33) . . .
1233(33) . . .
1250(33) . . .
1268(33) . . .
1227(33) . . .
1235(33) . . .
1255(33) . . .
1235(33) . . .
1258(33) . . .
1210(33) . . .
1270(33) . . .
1304(34) . . .
1236(33) . . .
1188(32) . . .
1182(32) . . .
1258(33) . . .
1284(34) . . .
1287(34) . . .
1251(33) . . .
1238(33) . . .
1254(33) . . .
1209(33) . . .
1244(33) . . .
1241(33) . . .
1269(33) . . .
1274(34) . . .
1264(33) . . .
1323(34) . . .
1337(34) . . .
1275(34) . . .
1290(34) . . .
1326(34) . . .
1288(34) . . .
1320(34) . . .
1331(34) . . .
1302(34) . . .
1303(34) . . .
1291(34) . . .
1332(34) . . .
1338(34) . . .
1335(34) . . .
1334(34) . . .
1330(34) . . .
1313(34) . . .
1298(34) . . .
1275(33) . . .
1283(34) . . .
1308(34) . . .
1324(34) . . .
1339(34) . . .
1340(34) . . .
1328(34) . . .
1321(34) . . .
1336(34) . . .
1336(34) . . .
1351(34) . . .
1356(34) . . .
1365(35) . . .
1332(34) . . .
1328(34) . . .
1361(35) . . .
1333(34) . . .
1355(34) . . .
1403(35) . . .
1388(35) . . .
1358(34) . . .
1333(34) . . .
1336(34) . . .
1364(35) . . .
1400(35) . . .
1375(35) . . .
1369(35) . . .
1373(35) . . .
1406(35) . . .
1359(34) . . .
1354(34) . . .
1352(34) . . .
1392(35) . . .
1445(35) . . .
1430(28) . . .
1408(33) . . .
1402(33) . . .
1419(33) . . .
1426(33) . . .
1445(33) . . .
1453(33) . . .
1439(33) . . .
1435(33) . . .
1442(37) . . .
1460(37) . . .
1471(37) . . .
1468(37) . . .
1426(37) . . .
1441(37) . . .
1455(37) . . .
1440(37) . . .
1482(37) . . .
1475(37) . . .
1437(37) . . .
1426(36) . . .
1430(37) . . .
1483(37) . . .
1510(37) . . .
1471(37) . . .
1470(37) . . .
1499(37) . . .
1528(38) . . .
1512(37) . . .
1483(37) . . .
1525(38) . . .
1523(38) . . .
1518(37) . . .
1564(38) . . .
1536(38) . . .
1539(38) . . .
1538(38) . . .
1532(38) . . .
1503(37) . . .
1527(38) . . .
1562(38) . . .
1556(38) . . .
1551(38) . . .
1584(38) . . .
1579(38) . . .
1551(38) . . .
1545(38) . . .
1564(38) . . .
1573(38) . . .
1582(38) . . .
1592(38) . . .
1595(38) . . .
1610(38) . . .
1607(38) . . .
1591(38) . . .
1571(38) . . .
1638(39) . . .
1633(39) . . .
1638(39) . . .
1620(39) . . .
1669(39) . . .
1674(39) . . .
1678(39) . . .
1718(40) . . .
1697(39) . . .
1637(39) . . .
1629(39) . . .
1648(39) . . .
1709(39) . . .
1698(39) . . .
1708(39) . . .
1725(40) . . .
1694(39) . . .
1681(39) . . .
1696(39) . . .
1713(40) . . .
1720(40) . . .
1714(40) . . .
1723(40) . . .
1732(40) . . .
1711(39) . . .
1752(40) . . .
1732(40) . . .
1696(39) . . .
1733(40) . . .
1769(40) . . .
1799(40) . . .
1802(40) . . .
1815(41) . . .
1820(41) . . .
1817(41) . . .
1798(40) . . .
1787(40) . . .
1813(41) . . .
1886(41) . . .
1893(41) . . .
1870(41) . . .
1858(41) . . .
1867(41) . . .
1887(41) . . .
1914(39) . . .
1907(39) . . .
1989(40) . . .
1950(40) . . .
1955(40) . . .
1930(39) . . .
2019(40) . . .
1962(40) . . .
1919(39) . . .
1932(43) . . .
1910(43) . . .
1994(44) . . .
2027(44) . . .
2021(44) . . .
2018(44) . . .
2109(45) . . .
2085(45) . . .
2106(45) . . .
2042(45) . . .
2084(45) . . .
2009(44) . . .
2064(45) . . .
2044(45) . . .
2103(45) . . .
2121(45) . . .
2146(45) . . .
2135(45) . . .
2098(45) . . .
2143(45) . . .
2172(46) . . .
2139(45) . . .
2157(46) . . .
2213(46) . . .
2267(47) . . .
2285(47) . . .
2266(47) . . .
2297(47) . . .
2261(46) . . .
2275(47) . . .
2293(47) . . .
2238(46) . . .
2312(47) . . .
2364(47) . . .
2321(47) . . .
2367(47) . . .
2373(47) . . .
2338(47) . . .
2308(47) . . .
2405(48) . . .
2341(47) . . .
2345(47) . . .
2371(47) . . .
2401(48) . . .
2486(48) . . .
2428(48) . . .
2443(48) . . .
2503(49) . . .
2526(49) . . .
2536(49) . . .
2438(48) . . .
2420(48) . . .
2544(49) . . .
2531(49) . . .
2537(49) . . .
2597(49) . . .
2619(49) . . .
2561(49) . . .
2621(50) . . .
2636(50) . . .
2655(50) . . .
2728(50) . . .
2737(50) . . .
2626(50) . . .
2721(50) . . .
2753(51) . . .
2721(50) . . .
2682(50) . . .
2794(51) . . .
2796(51) . . .
2800(51) . . .
2842(51) . . .
2823(51) . . .
2871(52) . . .
2825(51) . . .
2893(52) . . .
2901(52) . . .
2957(52) . . .
2835(51) . . .
2880(52) . . .
2880(52) . . .
2979(52) . . .
3014(53) . . .
3103(53) . . .
3029(53) . . .
3061(53) . . .
3038(53) . . .
3095(53) . . .
3094(53) . . .
3096(53) . . .
3077(53) . . .
3087(70) . . .
3054(69) . . .
3084(70) . . .
3009(69) . . .
3133(70) . . .
3122(70) . . .
3291(72) . . .
3219(71) . . .
3212(71) . . .
3198(87) . . .
_pd_meas_number_of_points        3197
_pd_proc_number_of_points        3197

_reflns_number_total             840
_reflns_limit_h_min              0
_reflns_limit_h_max              22
_reflns_limit_k_min              0
_reflns_limit_k_max              13
_reflns_limit_l_min              -14
_reflns_limit_l_max              14
_reflns_d_resolution_high        1.106
_reflns_d_resolution_low         13.658

# start Validation Reply Form
_vrf_SHFSU01_I
;
PROBLEM: The absolute value of parameter shift to su ratio > 0.20
RESPONSE: Small occupancy values for methane and relative = large ratio
;
_vrf_PLAT044_I
;
PROBLEM: Calculated and Reported Density Dx  Differ by ..     1.0664 Check 
RESPONSE: Adsorbed density of gas
;
_vrf_PLAT080_I
;
PROBLEM: Maximum Shift/Error ............................       0.49 Why ? 
RESPONSE: Small occupancy values for methane
;
_vrf_PLAT602_I
;
PROBLEM: VERY LARGE Solvent Accessible VOID(S) in Structure        ! Info 
RESPONSE: Thats the idea of MOFs
;
_vrf_PLAT701_I
;
PROBLEM: Bond    Calc   35.103(7), Rep   2.6190(3), Dev..    4640.58 Sigma 
RESPONSE: irrelevant
;
_vrf_PLAT721_I
;
PROBLEM: Bond    Calc    33.22000, Rep   2.8117(4) Dev...      30.41 Ang.  
RESPONSE: irrelevant
;
_vrf_PLAT722_I
;
PROBLEM: Angle   Calc      143.00, Rep   109.99(1) Dev...      33.01 Degree
RESPONSE: irrelevant
;
_vrf_PLAT770_I
;
PROBLEM: Suspect C-H Bond in CIF:   C1     --  H       ..       2.05 Ang.  
RESPONSE: irrelevant
;
_vrf_PLAT772_I
;
PROBLEM: Suspect O-H Bond in CIF:   O2     --  H       ..       2.71 Ang.  
RESPONSE: irrelevant
;
# end Validation Reply Form
 
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
