# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2016

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_ss16095
_database_code_depnum_ccdc_archive 'CCDC 1495857'
_audit_update_record             
;
2016-07-25 deposited with the CCDC.
2016-09-06 downloaded from the CCDC.
;
# start Validation Reply Form
_vrf_PLAT213_ss16095             
;
PROBLEM: Atom O6AA            has ADP max/min Ratio .....       12.0 oblate
RESPONSE: Strongly disordered H2O molecule
;
_vrf_PLAT043_ss16095             
;
PROBLEM: Calculated and Reported Mol. Weight Differ by ..      26.21 Check
RESPONSE: No H atoms added due to refinement instability and disordered solvent
;
_vrf_PLAT201_ss16095             
;
PROBLEM: Isotropic non-H Atoms in Main Residue(s) .......          1 Report
RESPONSE: disordered O atom
;
_vrf_PLAT213_ss16095_2           
;
PROBLEM: Atom C3AA            has ADP max/min Ratio .....        4.5 oblate
RESPONSE: disordered C atom
;
_vrf_PLAT214_ss16095             
;
PROBLEM: Atom O4CA    (Anion/Solvent) ADP max/min Ratio          5.4 prolat
RESPONSE: disordered oxygen atom (solvent)
;
_vrf_PLAT306_ss16095             
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......       O0CA Check
RESPONSE: water oxygen atom
;
_vrf_PLAT306_ss16095_2           
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......       O1CA Check
RESPONSE: water oxygen atom
;
_vrf_PLAT306_ss16095_3           
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......       O2CA Check
RESPONSE: water oxygen atom
;
_vrf_PLAT306_ss16095_4           
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......       O3CA Check
RESPONSE: water oxygen atom
;
_vrf_PLAT306_ss16095_5           
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......       O4CA Check
RESPONSE: water oxygen atom
;
_vrf_PLAT306_ss16095_6           
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......       O5CA Check
RESPONSE: water oxygen atom
;
_vrf_PLAT306_ss16095_7           
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......       O6CA Check
RESPONSE: water oxygen atom
;
_vrf_CHEMW03_ss16095             
;
PROBLEM: The ratio of given/expected molecular weight as
RESPONSE: Hydrogen atoms not added, see above
;
_vrf_PLAT041_ss16095             
;
PROBLEM: Calc. and Reported SumFormula    Strings  Differ     Please Check
RESPONSE: Hydrogen atoms not added, see above
;
_vrf_PLAT068_ss16095             
;
PROBLEM: Reported F000 Differs from Calcd (or Missing)...     Please Check
RESPONSE: Hydrogen atoms not added, see above
;
_vrf_PLAT090_ss16095             
;
PROBLEM: Poor Data / Parameter Ratio (Zmax &gt; 18) ........       8.01 Note
RESPONSE: crystal quality low, despite several measurements on different samples
;
_vrf_PLAT213_ss16095_3           
;
PROBLEM: Atom C0BA            has ADP max/min Ratio .....        3.2 prolat
RESPONSE: disorder
;
_vrf_PLAT234_ss16095             
;
PROBLEM: Large Hirshfeld Difference N1AA   --  N2AA    ..       0.16 Ang.
RESPONSE: disorder
;
_audit_creation_date             2016-07-20
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_moiety         'C14 Mo5 N6 O27 P2 Rb4, O'
_chemical_formula_sum            'C14 H26 Mo5 N6 O28 P2 Rb4'
_chemical_formula_weight         1609.93
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_h-m   'P 1 21 1'
_symmetry_int_tables_number      4
_chemical_absolute_configuration unk
_chemical_melting_point          ?
_exptl_crystal_description       block
_exptl_crystal_colour            yellow
_diffrn_ambient_temperature      150(2)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_H-M_alt        'P 21 '
_space_group_name_Hall           'P 2yb'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   10.7278(3)
_cell_length_b                   14.7418(3)
_cell_length_c                   13.2364(3)
_cell_angle_alpha                90
_cell_angle_beta                 107.779(2)
_cell_angle_gamma                90
_cell_volume                     1993.32(8)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    5021
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      24.5
_cell_measurement_theta_min      6.2
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    6.564
_exptl_absorpt_correction_T_max  0.789
_exptl_absorpt_correction_T_min  0.491
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details   'Agilent Crysalis software'
_exptl_absorpt_special_details   'Agilent Crysalis software'
_exptl_crystal_density_diffrn    2.682
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_F_000             1528
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0251
_diffrn_reflns_av_unetI/netI     0.0449
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            10336
_diffrn_reflns_point_group_measured_fraction_full 0.985
_diffrn_reflns_point_group_measured_fraction_max 0.953
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.301
_diffrn_reflns_theta_min         3.408
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Agilent SuperNova'
_diffrn_measurement_method       ?
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   microfocus
_diffrn_special_details          ?
_reflns_Friedel_coverage         0.992
_reflns_Friedel_fraction_full    0.981
_reflns_Friedel_fraction_max     0.961
_reflns_number_gt                5972
_reflns_number_total             6485
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         1.584
_refine_diff_density_min         -1.346
_refine_diff_density_rms         0.192
_refine_ls_abs_structure_details 
;
 Flack x determined using 1891 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.003(5)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     527
_refine_ls_number_reflns         6485
_refine_ls_number_restraints     1
_refine_ls_R_factor_all          0.0513
_refine_ls_R_factor_gt           0.0465
_refine_ls_restrained_S_all      1.038
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0604P)²+18.7323P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1147
_refine_ls_wR_factor_ref         0.1188
_refine_special_details          ?
_olex2_refinement_description    
;
1. Uiso/Uaniso restraints and constraints
: with sigma of 0.01 and sigma for terminal atoms of 0.1
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Mo1 Mo 0.00244(9) 0.31153(8) 0.25779(7) 0.0090(2) Uani 1 1 d . . . . .
Mo0A Mo -0.15692(10) -0.03804(8) 0.13912(8) 0.0091(2) Uani 1 1 d . . . . .
Mo1A Mo 0.16209(10) -0.04265(7) 0.35006(8) 0.0091(2) Uani 1 1 d . . . . .
Mo2A Mo 0.26165(10) 0.17597(8) 0.38393(8) 0.0091(2) Uani 1 1 d . . . . .
Mo3A Mo -0.25434(10) 0.18059(8) 0.12134(8) 0.0089(2) Uani 1 1 d . . . . .
Rb6 Rb -0.57753(14) -0.18307(13) -0.29476(11) 0.0258(3) Uani 1 1 d . . . . .
Rb7 Rb -0.12717(13) 0.36441(9) -0.06443(10) 0.0172(3) Uani 1 1 d . . . . .
Rb9 Rb -0.41546(16) 0.08106(15) -0.15968(12) 0.0351(4) Uani 1 1 d . . . . .
P1 P 0.0683(3) 0.1200(2) 0.1338(2) 0.0084(6) Uani 1 1 d . . . . .
P0AA P -0.0611(3) 0.1115(2) 0.3671(2) 0.0094(7) Uani 1 1 d . . . . .
Rb8 Rb 0.13281(13) 0.35744(10) 0.58291(10) 0.0180(3) Uani 1 1 d . . . . .
O1 O -0.0281(8) 0.1970(6) 0.1339(6) 0.0086(18) Uani 1 1 d . . . . .
O0AA O -0.0012(10) 0.3869(7) 0.1597(7) 0.019(2) Uani 1 1 d . . . . .
O1AA O -0.1641(9) -0.1121(7) 0.0382(7) 0.016(2) Uani 1 1 d . . . . .
O2AA O -0.1439(8) 0.0899(6) 0.2523(6) 0.0092(18) Uani 1 1 d . . . . .
O3AA O 0.1487(8) 0.0927(6) 0.2473(6) 0.0107(18) Uani 1 1 d . . . . .
O4AA O 0.1717(9) -0.1241(7) 0.4435(7) 0.016(2) Uani 1 1 d . . . . .
O5AA O 0.1813(8) 0.2741(6) 0.2879(6) 0.0094(18) Uiso 1 1 d . U . . .
O6AA O -0.1766(8) 0.2748(6) 0.2240(7) 0.0102(18) Uani 1 1 d . . . . .
O7AA O 0.4065(9) 0.1800(7) 0.3567(7) 0.016(2) Uani 1 1 d . . . . .
O8AA O -0.2553(8) 0.0622(7) 0.0608(6) 0.0113(19) Uani 1 1 d . . . . .
O9AA O -0.2656(9) -0.0816(7) 0.1962(7) 0.0130(19) Uani 1 1 d . . . . .
O0BA O 0.0338(8) 0.1906(6) 0.3716(6) 0.0091(18) Uani 1 1 d . . . . .
O1BA O -0.3978(8) 0.1777(7) 0.1504(7) 0.0145(19) Uani 1 1 d . . . . .
O2BA O 0.0109(9) 0.0267(7) 0.4175(6) 0.0119(19) Uani 1 1 d . . . . .
O3BA O 0.0013(9) -0.0705(7) 0.2437(6) 0.014(2) Uani 1 1 d . . . . .
O4BA O -0.0034(8) 0.0373(6) 0.0769(7) 0.0112(19) Uani 1 1 d . . . . .
O5BA O 0.2641(8) 0.0532(6) 0.4351(6) 0.0103(18) Uani 1 1 d . . . . .
O6BA O -0.2899(9) 0.2389(7) 0.0046(7) 0.015(2) Uani 1 1 d . . . . .
O7BA O 0.2907(9) 0.2288(6) 0.5038(7) 0.014(2) Uani 1 1 d . . . . .
C1 C 0.1792(13) 0.1589(9) 0.0661(10) 0.014(3) Uani 1 1 d . . . . .
C0AA C -0.1685(13) 0.1462(9) 0.4403(10) 0.014(3) Uani 1 1 d . . . . .
C1AA C 0.2588(12) 0.0854(9) 0.0370(10) 0.013(3) Uani 1 1 d . . . . .
O8BA O 0.2647(9) -0.0819(7) 0.2844(7) 0.014(2) Uani 1 1 d . . . . .
C2AA C 0.4002(13) -0.0518(9) -0.0242(10) 0.015(3) Uani 1 1 d . . . . .
C3AA C 0.4310(13) -0.0257(10) 0.0819(11) 0.018(3) Uani 1 1 d . . . . .
C4AA C -0.2590(13) 0.0722(10) 0.4569(10) 0.014(3) Uani 1 1 d . . . . .
C5AA C 0.3606(14) 0.0420(11) 0.1120(10) 0.020(3) Uani 1 1 d . . . . .
C6AA C -0.2467(13) 0.0413(10) 0.5589(11) 0.017(3) Uani 1 1 d . . . . .
C7AA C -0.4344(14) -0.0358(11) 0.3856(11) 0.021(3) Uani 1 1 d . . . . .
C8AA C 0.2990(13) -0.0098(10) -0.0997(11) 0.016(3) Uani 1 1 d . . . . .
C9AA C 0.2279(14) 0.0589(10) -0.0690(10) 0.018(3) Uani 1 1 d . . . . .
C0BA C -0.4204(14) -0.0657(10) 0.4888(12) 0.020(3) Uani 1 1 d . . . . .
C1BA C -0.3293(16) -0.0282(11) 0.5734(11) 0.023(3) Uani 1 1 d . . . . .
C2BA C -0.3533(13) 0.0341(11) 0.3709(10) 0.019(3) Uani 1 1 d . . . . .
N1 N -0.5003(13) -0.1362(9) 0.5120(10) 0.023(3) Uani 1 1 d . . . . .
N0AA N -0.5497(12) -0.1935(10) 0.4416(10) 0.026(3) Uani 1 1 d . . . . .
N1AA N 0.5371(12) -0.1741(10) -0.0005(11) 0.026(3) Uani 1 1 d . . . . .
N2AA N 0.4700(13) -0.1169(9) -0.0656(10) 0.024(3) Uani 1 1 d . . . . .
N3AA N -0.6014(14) -0.2510(11) 0.3886(12) 0.034(3) Uani 1 1 d . . . . .
N4AA N 0.5992(14) -0.2308(10) 0.0449(11) 0.032(3) Uani 1 1 d . . . . .
O9BA O 0.0089(9) 0.3808(6) 0.3635(7) 0.016(2) Uani 1 1 d . . . . .
O0CA O -0.1338(11) 0.0531(7) -0.1388(8) 0.024(2) Uani 1 1 d . . . . .
O1CA O 0.1229(11) 0.0404(8) 0.6343(8) 0.026(2) Uani 1 1 d . . . . .
O2CA O -0.1165(12) 0.2221(8) -0.2146(9) 0.033(3) Uani 1 1 d . . . . .
O3CA O -0.3171(10) -0.1283(8) -0.1812(8) 0.027(2) Uani 1 1 d . . . . .
O4CA O -0.6098(11) 0.0162(12) -0.3453(8) 0.048(4) Uani 1 1 d . . . A 2
O5CA O 0.1057(13) 0.2135(8) 0.7109(10) 0.038(3) Uani 1 1 d . . . . .
O6CA O -0.6069(15) 0.2206(11) -0.2619(10) 0.058(4) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Mo1 Rb7 4.1364(16) . ?
Mo1 Rb8 4.1543(16) . ?
Mo1 O1 2.306(9) . ?
Mo1 O0AA 1.700(10) . ?
Mo1 O5AA 1.918(9) . ?
Mo1 O6AA 1.912(8) . ?
Mo1 O0BA 2.291(9) . ?
Mo1 O9BA 1.717(9) . ?
Mo0A Rb7 3.7647(17) 2_545 ?
Mo0A Rb8 3.9239(16) 2_546 ?
Mo0A O1AA 1.709(9) . ?
Mo0A O2AA 2.385(9) . ?
Mo0A O8AA 1.925(9) . ?
Mo0A O9AA 1.697(9) . ?
Mo0A O3BA 1.895(9) . ?
Mo0A O4BA 2.335(9) . ?
Mo1A Rb7 3.9302(16) 2_545 ?
Mo1A Rb8 3.8314(17) 2_546 ?
Mo1A O3AA 2.395(9) . ?
Mo1A O4AA 1.705(9) . ?
Mo1A O2BA 2.314(9) . ?
Mo1A O3BA 1.909(9) . ?
Mo1A O5BA 1.925(9) . ?
Mo1A O8BA 1.699(9) . ?
Mo2A Rb8 4.2694(17) . ?
Mo2A O3AA 2.215(8) . ?
Mo2A O5AA 1.945(9) . ?
Mo2A O7AA 1.700(9) . ?
Mo2A O0BA 2.409(8) . ?
Mo2A O5BA 1.930(9) . ?
Mo2A O7BA 1.709(9) . ?
Mo3A Rb6 3.8847(19) 2_455 ?
Mo3A Rb7 4.1593(17) . ?
Mo3A Rb9 3.8795(19) . ?
Mo3A O1 2.394(8) . ?
Mo3A O2AA 2.223(9) . ?
Mo3A O6AA 1.944(9) . ?
Mo3A O8AA 1.919(10) . ?
Mo3A O1BA 1.697(9) . ?
Mo3A O6BA 1.706(9) . ?
Rb6 Mo3A 3.8847(19) 2_445 ?
Rb6 Rb9 4.414(2) . ?
Rb6 O6AA 3.119(9) 2_445 ?
Rb6 O7AA 3.006(10) 2_545 ?
Rb6 O1BA 2.871(10) 2_445 ?
Rb6 N1 3.000(12) 1_554 ?
Rb6 N0AA 3.596(13) 1_554 ?
Rb6 N2AA 3.077(12) 1_455 ?
Rb6 O3CA 2.855(11) . ?
Rb6 O4CA 3.009(17) . ?
Rb7 O1 3.522(9) . ?
Rb7 O0AA 2.879(10) . ?
Rb7 O1AA 3.056(9) 2 ?
Rb7 O3BA 3.214(8) 2 ?
Rb7 O4BA 2.936(10) 2 ?
Rb7 O6BA 2.878(10) . ?
Rb7 C1AA 3.612(14) 2 ?
Rb7 O8BA 2.942(9) 2 ?
Rb7 C2AA 3.686(14) 2 ?
Rb7 C3AA 3.583(14) 2 ?
Rb7 C5AA 3.544(15) 2 ?
Rb7 O2CA 2.917(12) . ?
Rb9 O8AA 2.912(8) . ?
Rb9 O6BA 3.188(9) . ?
Rb9 C2AA 3.622(14) 1_455 ?
Rb9 C8AA 3.646(13) 1_455 ?
Rb9 N2AA 3.538(13) 1_455 ?
Rb9 O0CA 2.977(11) . ?
Rb9 O3CA 3.303(11) . ?
Rb9 O4CA 2.858(12) . ?
Rb9 O6CA 2.929(15) . ?
P1 Rb7 3.974(4) 2_545 ?
P1 O1 1.536(9) . ?
P1 O3AA 1.540(9) . ?
P1 O4BA 1.514(9) . ?
P1 C1 1.788(12) . ?
P0AA Rb8 3.920(4) 2_546 ?
P0AA O2AA 1.542(8) . ?
P0AA O0BA 1.538(9) . ?
P0AA O2BA 1.513(10) . ?
P0AA C0AA 1.791(13) . ?
Rb8 O4AA 3.188(9) 2_556 ?
Rb8 O9AA 2.974(9) 2_556 ?
Rb8 O0BA 3.631(9) . ?
Rb8 O2BA 2.932(10) 2_556 ?
Rb8 O3BA 3.237(9) 2_556 ?
Rb8 O7BA 2.940(9) . ?
Rb8 C4AA 3.545(14) 2_556 ?
Rb8 C7AA 3.507(15) 2_556 ?
Rb8 C2BA 3.445(15) 2_556 ?
Rb8 O9BA 2.821(9) . ?
Rb8 O5CA 2.785(12) . ?
Rb8 O6CA 3.548(14) 1_656 ?
O1AA Rb7 3.056(9) 2_545 ?
O4AA Rb8 3.189(9) 2_546 ?
O6AA Rb6 3.119(9) 2_455 ?
O7AA Rb6 3.006(10) 2 ?
O9AA Rb8 2.974(9) 2_546 ?
O1BA Rb6 2.871(10) 2_455 ?
O2BA Rb8 2.932(10) 2_546 ?
O3BA Rb7 3.214(8) 2_545 ?
O3BA Rb8 3.237(9) 2_546 ?
O4BA Rb7 2.936(10) 2_545 ?
C1 C1AA 1.502(19) . ?
C0AA C4AA 1.521(19) . ?
C1AA Rb7 3.612(14) 2_545 ?
C1AA C5AA 1.388(18) . ?
C1AA C9AA 1.395(18) . ?
O8BA Rb7 2.942(9) 2_545 ?
C2AA Rb7 3.686(14) 2_545 ?
C2AA Rb9 3.623(14) 1_655 ?
C2AA C3AA 1.396(19) . ?
C2AA C8AA 1.38(2) . ?
C2AA N2AA 1.426(18) . ?
C3AA Rb7 3.583(14) 2_545 ?
C3AA C5AA 1.38(2) . ?
C4AA Rb8 3.545(14) 2_546 ?
C4AA C6AA 1.392(18) . ?
C4AA C2BA 1.389(19) . ?
C5AA Rb7 3.544(15) 2_545 ?
C6AA Rb8 3.709(14) 2_546 ?
C6AA C1BA 1.41(2) . ?
C7AA Rb8 3.506(15) 2_546 ?
C7AA C0BA 1.40(2) . ?
C7AA C2BA 1.40(2) . ?
C8AA Rb7 3.743(14) 2_545 ?
C8AA Rb9 3.646(13) 1_655 ?
C8AA C9AA 1.40(2) . ?
C9AA Rb7 3.697(15) 2_545 ?
C0BA Rb8 3.673(14) 2_546 ?
C0BA C1BA 1.36(2) . ?
C0BA N1 1.438(19) . ?
C2BA Rb8 3.445(15) 2_546 ?
N1 Rb6 3.000(12) 1_556 ?
N1 N0AA 1.250(19) . ?
N0AA Rb6 3.596(13) 1_556 ?
N0AA N3AA 1.13(2) . ?
N1AA N2AA 1.262(19) . ?
N1AA N4AA 1.12(2) . ?
N2AA Rb6 3.077(12) 1_655 ?
N2AA Rb9 3.538(13) 1_655 ?
O6CA Rb8 3.547(14) 1_454 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Rb7 Mo1 Rb8 159.76(4) . . ?
O1 Mo1 Rb7 58.3(2) . . ?
O1 Mo1 Rb8 141.8(2) . . ?
O0AA Mo1 Rb7 33.6(3) . . ?
O0AA Mo1 Rb8 127.3(3) . . ?
O0AA Mo1 O1 88.3(4) . . ?
O0AA Mo1 O5AA 97.7(4) . . ?
O0AA Mo1 O6AA 102.7(4) . . ?
O0AA Mo1 O0BA 167.1(4) . . ?
O0AA Mo1 O9BA 102.7(5) . . ?
O5AA Mo1 Rb7 105.6(2) . . ?
O5AA Mo1 Rb8 80.4(2) . . ?
O5AA Mo1 O1 81.5(3) . . ?
O5AA Mo1 O0BA 72.7(3) . . ?
O6AA Mo1 Rb7 79.3(3) . . ?
O6AA Mo1 Rb8 106.5(3) . . ?
O6AA Mo1 O1 73.3(3) . . ?
O6AA Mo1 O5AA 146.8(4) . . ?
O6AA Mo1 O0BA 82.5(3) . . ?
O0BA Mo1 Rb7 139.5(2) . . ?
O0BA Mo1 Rb8 60.7(2) . . ?
O0BA Mo1 O1 81.9(3) . . ?
O9BA Mo1 Rb7 130.2(3) . . ?
O9BA Mo1 Rb8 30.8(3) . . ?
O9BA Mo1 O1 167.6(4) . . ?
O9BA Mo1 O5AA 102.3(4) . . ?
O9BA Mo1 O6AA 98.4(4) . . ?
O9BA Mo1 O0BA 88.0(4) . . ?
Rb7 Mo0A Rb8 105.63(4) 2_545 2_546 ?
O1AA Mo0A Rb7 52.9(3) . 2_545 ?
O1AA Mo0A Rb8 117.2(3) . 2_546 ?
O1AA Mo0A O2AA 167.4(4) . . ?
O1AA Mo0A O8AA 100.5(4) . . ?
O1AA Mo0A O3BA 103.1(4) . . ?
O1AA Mo0A O4BA 84.0(4) . . ?
O2AA Mo0A Rb7 124.7(2) . 2_545 ?
O2AA Mo0A Rb8 75.4(2) . 2_546 ?
O8AA Mo0A Rb7 120.4(3) . 2_545 ?
O8AA Mo0A Rb8 132.5(3) . 2_546 ?
O8AA Mo0A O2AA 69.4(3) . . ?
O8AA Mo0A O4BA 77.0(3) . . ?
O9AA Mo0A Rb7 133.9(3) . 2_545 ?
O9AA Mo0A Rb8 44.9(3) . 2_546 ?
O9AA Mo0A O1AA 103.5(5) . . ?
O9AA Mo0A O2AA 86.4(4) . . ?
O9AA Mo0A O8AA 101.1(4) . . ?
O9AA Mo0A O3BA 99.4(4) . . ?
O9AA Mo0A O4BA 172.5(4) . . ?
O3BA Mo0A Rb7 58.6(3) . 2_545 ?
O3BA Mo0A Rb8 55.1(3) . 2_546 ?
O3BA Mo0A O2AA 82.7(3) . . ?
O3BA Mo0A O8AA 144.0(4) . . ?
O3BA Mo0A O4BA 78.9(3) . . ?
O4BA Mo0A Rb7 51.3(2) . 2_545 ?
O4BA Mo0A Rb8 131.7(2) . 2_546 ?
O4BA Mo0A O2AA 86.2(3) . . ?
Rb8 Mo1A Rb7 104.23(4) 2_546 2_545 ?
O3AA Mo1A Rb7 76.9(2) . 2_545 ?
O3AA Mo1A Rb8 122.8(2) . 2_546 ?
O4AA Mo1A Rb7 114.8(3) . 2_545 ?
O4AA Mo1A Rb8 55.4(3) . 2_546 ?
O4AA Mo1A O3AA 168.3(4) . . ?
O4AA Mo1A O2BA 85.7(4) . . ?
O4AA Mo1A O3BA 103.0(4) . . ?
O4AA Mo1A O5BA 101.3(4) . . ?
O2BA Mo1A Rb7 130.8(2) . 2_545 ?
O2BA Mo1A Rb8 49.8(2) . 2_546 ?
O2BA Mo1A O3AA 85.6(3) . . ?
O3BA Mo1A Rb7 54.3(3) . 2_545 ?
O3BA Mo1A Rb8 57.6(3) . 2_546 ?
O3BA Mo1A O3AA 82.9(4) . . ?
O3BA Mo1A O2BA 78.3(3) . . ?
O3BA Mo1A O5BA 144.4(4) . . ?
O5BA Mo1A Rb7 133.5(3) . 2_545 ?
O5BA Mo1A Rb8 120.6(3) . 2_546 ?
O5BA Mo1A O3AA 69.2(3) . . ?
O5BA Mo1A O2BA 77.9(4) . . ?
O8BA Mo1A Rb7 43.5(3) . 2_545 ?
O8BA Mo1A Rb8 134.2(3) . 2_546 ?
O8BA Mo1A O3AA 85.9(4) . . ?
O8BA Mo1A O4AA 103.1(5) . . ?
O8BA Mo1A O2BA 171.0(4) . . ?
O8BA Mo1A O3BA 97.5(4) . . ?
O8BA Mo1A O5BA 102.0(4) . . ?
O3AA Mo2A Rb8 130.7(2) . . ?
O3AA Mo2A O0BA 72.8(3) . . ?
O5AA Mo2A Rb8 77.0(3) . . ?
O5AA Mo2A O3AA 81.7(3) . . ?
O5AA Mo2A O0BA 69.6(3) . . ?
O7AA Mo2A Rb8 126.7(3) . . ?
O7AA Mo2A O3AA 98.8(4) . . ?
O7AA Mo2A O5AA 95.0(4) . . ?
O7AA Mo2A O0BA 163.1(4) . . ?
O7AA Mo2A O5BA 101.1(4) . . ?
O7AA Mo2A O7BA 105.2(4) . . ?
O0BA Mo2A Rb8 58.2(2) . . ?
O5BA Mo2A Rb8 110.1(3) . . ?
O5BA Mo2A O3AA 73.3(3) . . ?
O5BA Mo2A O5AA 152.0(4) . . ?
O5BA Mo2A O0BA 90.7(3) . . ?
O7BA Mo2A Rb8 31.0(3) . . ?
O7BA Mo2A O3AA 155.5(4) . . ?
O7BA Mo2A O5AA 100.8(4) . . ?
O7BA Mo2A O0BA 85.1(4) . . ?
O7BA Mo2A O5BA 97.0(4) . . ?
Rb6 Mo3A Rb7 107.91(4) 2_455 . ?
Rb9 Mo3A Rb6 127.66(4) . 2_455 ?
Rb9 Mo3A Rb7 79.05(4) . . ?
O1 Mo3A Rb6 123.4(2) . 2_455 ?
O1 Mo3A Rb7 57.8(2) . . ?
O1 Mo3A Rb9 104.5(2) . . ?
O2AA Mo3A Rb6 94.8(2) . 2_455 ?
O2AA Mo3A Rb7 131.3(2) . . ?
O2AA Mo3A Rb9 119.7(2) . . ?
O2AA Mo3A O1 73.7(3) . . ?
O6AA Mo3A Rb6 52.8(3) . 2_455 ?
O6AA Mo3A Rb7 78.4(3) . . ?
O6AA Mo3A Rb9 155.6(3) . . ?
O6AA Mo3A O1 70.7(3) . . ?
O6AA Mo3A O2AA 82.7(3) . . ?
O8AA Mo3A Rb6 140.6(3) . 2_455 ?
O8AA Mo3A Rb7 107.8(3) . . ?
O8AA Mo3A Rb9 46.5(2) . . ?
O8AA Mo3A O1 89.8(3) . . ?
O8AA Mo3A O2AA 73.3(3) . . ?
O8AA Mo3A O6AA 152.6(4) . . ?
O1BA Mo3A Rb6 42.4(3) . 2_455 ?
O1BA Mo3A Rb7 129.4(3) . . ?
O1BA Mo3A Rb9 92.2(3) . . ?
O1BA Mo3A O1 163.2(4) . . ?
O1BA Mo3A O2AA 96.5(4) . . ?
O1BA Mo3A O6AA 94.8(4) . . ?
O1BA Mo3A O8AA 100.5(4) . . ?
O1BA Mo3A O6BA 104.5(4) . . ?
O6BA Mo3A Rb6 105.0(3) . 2_455 ?
O6BA Mo3A Rb7 32.8(3) . . ?
O6BA Mo3A Rb9 53.9(3) . . ?
O6BA Mo3A O1 87.3(4) . . ?
O6BA Mo3A O2AA 158.0(4) . . ?
O6BA Mo3A O6AA 101.7(4) . . ?
O6BA Mo3A O8AA 96.2(4) . . ?
Mo3A Rb6 Rb9 114.43(4) 2_445 . ?
O6AA Rb6 Mo3A 29.75(16) 2_445 2_445 ?
O6AA Rb6 Rb9 108.58(18) 2_445 . ?
O6AA Rb6 N0AA 127.7(3) 2_445 1_554 ?
O7AA Rb6 Mo3A 104.2(2) 2_545 2_445 ?
O7AA Rb6 Rb9 120.35(19) 2_545 . ?
O7AA Rb6 O6AA 126.2(3) 2_545 2_445 ?
O7AA Rb6 N0AA 57.8(3) 2_545 1_554 ?
O7AA Rb6 N2AA 123.4(3) 2_545 1_455 ?
O7AA Rb6 O4CA 129.3(3) 2_545 . ?
O1BA Rb6 Mo3A 23.51(18) 2_445 2_445 ?
O1BA Rb6 Rb9 117.8(2) 2_445 . ?
O1BA Rb6 O6AA 53.1(2) 2_445 2_445 ?
O1BA Rb6 O7AA 83.7(3) 2_445 2_545 ?
O1BA Rb6 N1 146.9(3) 2_445 1_554 ?
O1BA Rb6 N0AA 131.8(3) 2_445 1_554 ?
O1BA Rb6 N2AA 65.9(3) 2_445 1_455 ?
O1BA Rb6 O4CA 144.9(3) 2_445 . ?
N1 Rb6 Mo3A 157.2(3) 1_554 2_445 ?
N1 Rb6 Rb9 88.0(3) 1_554 . ?
N1 Rb6 O6AA 141.3(3) 1_554 2_445 ?
N1 Rb6 O7AA 64.6(3) 1_554 2_545 ?
N1 Rb6 N0AA 19.3(3) 1_554 1_554 ?
N1 Rb6 N2AA 139.6(4) 1_554 1_455 ?
N1 Rb6 O4CA 68.2(3) 1_554 . ?
N0AA Rb6 Mo3A 137.9(2) 1_554 2_445 ?
N0AA Rb6 Rb9 107.0(2) 1_554 . ?
N2AA Rb6 Mo3A 63.2(2) 1_455 2_445 ?
N2AA Rb6 Rb9 52.8(2) 1_455 . ?
N2AA Rb6 O6AA 70.6(3) 1_455 2_445 ?
N2AA Rb6 N0AA 158.8(3) 1_455 1_554 ?
O3CA Rb6 Mo3A 113.0(2) . 2_445 ?
O3CA Rb6 Rb9 48.4(2) . . ?
O3CA Rb6 O6AA 132.8(2) . 2_445 ?
O3CA Rb6 O7AA 75.7(3) . 2_545 ?
O3CA Rb6 O1BA 97.2(3) . 2_445 ?
O3CA Rb6 N1 84.4(3) . 1_554 ?
O3CA Rb6 N0AA 99.5(3) . 1_554 ?
O3CA Rb6 N2AA 63.3(3) . 1_455 ?
O3CA Rb6 O4CA 82.5(3) . . ?
O4CA Rb6 Mo3A 126.4(2) . 2_445 ?
O4CA Rb6 Rb9 39.9(2) . . ?
O4CA Rb6 O6AA 102.1(3) . 2_445 ?
O4CA Rb6 N0AA 82.2(3) . 1_554 ?
O4CA Rb6 N2AA 83.3(3) . 1_455 ?
O1 Rb7 C1AA 126.5(2) . 2 ?
O1 Rb7 C2AA 94.9(2) . 2 ?
O1 Rb7 C3AA 115.2(3) . 2 ?
O1 Rb7 C5AA 133.3(3) . 2 ?
O0AA Rb7 O1 51.2(2) . . ?
O0AA Rb7 O1AA 74.2(3) . 2 ?
O0AA Rb7 O3BA 123.7(3) . 2 ?
O0AA Rb7 O4BA 82.9(3) . 2 ?
O0AA Rb7 C1AA 82.4(3) . 2 ?
O0AA Rb7 O8BA 157.6(3) . 2 ?
O0AA Rb7 C2AA 78.6(3) . 2 ?
O0AA Rb7 C3AA 98.4(3) . 2 ?
O0AA Rb7 C5AA 100.5(3) . 2 ?
O0AA Rb7 O2CA 133.0(3) . . ?
O1AA Rb7 O1 85.9(2) 2 . ?
O1AA Rb7 O3BA 53.5(2) 2 2 ?
O1AA Rb7 C1AA 107.7(3) 2 2 ?
O1AA Rb7 C2AA 144.1(3) 2 2 ?
O1AA Rb7 C3AA 146.5(3) 2 2 ?
O1AA Rb7 C5AA 125.4(3) 2 2 ?
O3BA Rb7 O1 131.3(2) 2 . ?
O3BA Rb7 C1AA 94.0(3) 2 2 ?
O3BA Rb7 C2AA 133.5(3) 2 2 ?
O3BA Rb7 C3AA 113.3(3) 2 2 ?
O3BA Rb7 C5AA 94.7(3) 2 2 ?
O4BA Rb7 O1 127.5(2) 2 . ?
O4BA Rb7 O1AA 54.5(3) 2 2 ?
O4BA Rb7 O3BA 52.0(2) 2 2 ?
O4BA Rb7 C1AA 55.3(3) 2 2 ?
O4BA Rb7 O8BA 79.3(2) 2 2 ?
O4BA Rb7 C2AA 99.6(3) 2 2 ?
O4BA Rb7 C3AA 92.5(3) 2 2 ?
O4BA Rb7 C5AA 70.9(3) 2 2 ?
O6BA Rb7 O1 52.2(2) . . ?
O6BA Rb7 O0AA 83.5(3) . . ?
O6BA Rb7 O1AA 137.3(3) . 2 ?
O6BA Rb7 O3BA 149.2(3) . 2 ?
O6BA Rb7 O4BA 157.2(3) . 2 ?
O6BA Rb7 C1AA 104.7(3) . 2 ?
O6BA Rb7 O8BA 108.5(2) . 2 ?
O6BA Rb7 C2AA 59.8(3) . 2 ?
O6BA Rb7 C3AA 71.5(3) . 2 ?
O6BA Rb7 C5AA 93.8(3) . 2 ?
O6BA Rb7 O2CA 84.7(3) . . ?
C1AA Rb7 C2AA 45.0(3) 2 2 ?
O8BA Rb7 O1 150.7(2) 2 . ?
O8BA Rb7 O1AA 105.6(2) 2 2 ?
O8BA Rb7 O3BA 52.1(2) 2 2 ?
O8BA Rb7 C1AA 76.3(3) 2 2 ?
O8BA Rb7 C2AA 91.0(3) 2 2 ?
O8BA Rb7 C3AA 69.1(3) 2 2 ?
O8BA Rb7 C5AA 60.8(3) 2 2 ?
C3AA Rb7 C1AA 39.0(3) 2 2 ?
C3AA Rb7 C2AA 22.1(3) 2 2 ?
C5AA Rb7 C1AA 22.3(3) 2 2 ?
C5AA Rb7 C2AA 38.9(3) 2 2 ?
C5AA Rb7 C3AA 22.3(3) 2 2 ?
O2CA Rb7 O1 86.5(3) . . ?
O2CA Rb7 O1AA 84.7(3) . 2 ?
O2CA Rb7 O3BA 66.3(3) . 2 ?
O2CA Rb7 O4BA 117.9(3) . 2 ?
O2CA Rb7 C1AA 144.6(3) . 2 ?
O2CA Rb7 O8BA 68.3(3) . 2 ?
O2CA Rb7 C2AA 131.2(3) . 2 ?
O2CA Rb7 C3AA 120.4(3) . 2 ?
O2CA Rb7 C5AA 125.7(3) . 2 ?
Mo3A Rb9 Rb6 136.64(5) . . ?
Mo3A Rb9 Rb7 52.89(3) . . ?
Rb6 Rb9 Rb7 162.35(5) . . ?
O8AA Rb9 Mo3A 28.55(19) . . ?
O8AA Rb9 Rb6 111.1(2) . . ?
O8AA Rb9 Rb7 72.77(19) . . ?
O8AA Rb9 O6BA 52.3(3) . . ?
O8AA Rb9 C2AA 72.4(3) . 1_455 ?
O8AA Rb9 C8AA 91.4(3) . 1_455 ?
O8AA Rb9 N2AA 74.4(3) . 1_455 ?
O8AA Rb9 O0CA 67.8(2) . . ?
O8AA Rb9 O3CA 83.7(3) . . ?
O8AA Rb9 O6CA 130.2(3) . . ?
O6BA Rb9 Mo3A 25.63(17) . . ?
O6BA Rb9 Rb6 162.18(18) . . ?
O6BA Rb9 Rb7 30.60(17) . . ?
O6BA Rb9 C2AA 103.7(3) . 1_455 ?
O6BA Rb9 C8AA 109.1(3) . 1_455 ?
O6BA Rb9 N2AA 118.8(3) . 1_455 ?
O6BA Rb9 O3CA 131.4(3) . . ?
C2AA Rb9 Mo3A 83.1(2) 1_455 . ?
C2AA Rb9 Rb6 61.1(2) 1_455 . ?
C2AA Rb9 Rb7 134.3(2) 1_455 . ?
C2AA Rb9 C8AA 21.9(3) 1_455 1_455 ?
C8AA Rb9 Mo3A 95.1(2) 1_455 . ?
C8AA Rb9 Rb6 60.7(2) 1_455 . ?
C8AA Rb9 Rb7 136.9(2) 1_455 . ?
N2AA Rb9 Mo3A 94.3(2) 1_455 . ?
N2AA Rb9 Rb6 43.8(2) 1_455 . ?
N2AA Rb9 Rb7 146.6(2) 1_455 . ?
N2AA Rb9 C2AA 22.9(3) 1_455 1_455 ?
N2AA Rb9 C8AA 38.3(3) 1_455 1_455 ?
O0CA Rb9 Mo3A 79.69(19) . . ?
O0CA Rb9 Rb6 100.3(2) . . ?
O0CA Rb9 Rb7 64.6(2) . . ?
O0CA Rb9 O6BA 80.3(3) . . ?
O0CA Rb9 C2AA 124.8(3) . 1_455 ?
O0CA Rb9 C8AA 145.6(3) . 1_455 ?
O0CA Rb9 N2AA 107.8(3) . 1_455 ?
O0CA Rb9 O3CA 62.4(3) . . ?
O3CA Rb9 Mo3A 112.07(18) . . ?
O3CA Rb9 Rb6 40.29(19) . . ?
O3CA Rb9 Rb7 126.8(2) . . ?
O3CA Rb9 C2AA 77.0(3) . 1_455 ?
O3CA Rb9 C8AA 89.3(3) . 1_455 ?
O3CA Rb9 N2AA 54.1(3) . 1_455 ?
O4CA Rb9 Mo3A 160.9(2) . . ?
O4CA Rb9 Rb6 42.5(3) . . ?
O4CA Rb9 Rb7 135.4(3) . . ?
O4CA Rb9 O8AA 151.8(4) . . ?
O4CA Rb9 O6BA 151.1(4) . . ?
O4CA Rb9 C2AA 83.1(4) . 1_455 ?
O4CA Rb9 C8AA 67.9(3) . 1_455 ?
O4CA Rb9 N2AA 77.6(4) . 1_455 ?
O4CA Rb9 O0CA 119.1(3) . . ?
O4CA Rb9 O3CA 77.4(4) . . ?
O4CA Rb9 O6CA 67.3(4) . . ?
O6CA Rb9 Mo3A 102.8(3) . . ?
O6CA Rb9 Rb6 107.4(3) . . ?
O6CA Rb9 Rb7 80.0(3) . . ?
O6CA Rb9 O6BA 83.9(3) . . ?
O6CA Rb9 C2AA 101.3(4) . 1_455 ?
O6CA Rb9 C8AA 80.9(4) . 1_455 ?
O6CA Rb9 N2AA 118.2(4) . 1_455 ?
O6CA Rb9 O0CA 133.5(4) . . ?
O6CA Rb9 O3CA 144.5(4) . . ?
O1 P1 Rb7 148.8(3) . 2_545 ?
O1 P1 O3AA 111.7(5) . . ?
O1 P1 C1 108.3(6) . . ?
O3AA P1 Rb7 84.1(4) . 2_545 ?
O3AA P1 C1 108.2(6) . . ?
O4BA P1 Rb7 38.2(4) . 2_545 ?
O4BA P1 O1 110.9(5) . . ?
O4BA P1 O3AA 108.9(5) . . ?
O4BA P1 C1 108.9(6) . . ?
C1 P1 Rb7 90.7(5) . 2_545 ?
O2AA P0AA Rb8 83.4(4) . 2_546 ?
O2AA P0AA C0AA 108.7(6) . . ?
O0BA P0AA Rb8 151.6(4) . 2_546 ?
O0BA P0AA O2AA 111.7(5) . . ?
O0BA P0AA C0AA 106.9(6) . . ?
O2BA P0AA Rb8 40.2(4) . 2_546 ?
O2BA P0AA O2AA 109.1(5) . . ?
O2BA P0AA O0BA 111.5(5) . . ?
O2BA P0AA C0AA 108.9(6) . . ?
C0AA P0AA Rb8 89.5(5) . 2_546 ?
O4AA Rb8 O0BA 85.7(2) 2_556 . ?
O4AA Rb8 O3BA 52.2(2) 2_556 2_556 ?
O4AA Rb8 C4AA 109.4(3) 2_556 2_556 ?
O4AA Rb8 C7AA 148.4(3) 2_556 2_556 ?
O4AA Rb8 C2BA 125.4(3) 2_556 2_556 ?
O4AA Rb8 O6CA 135.3(3) 2_556 1_656 ?
O9AA Rb8 O4AA 104.4(2) 2_556 2_556 ?
O9AA Rb8 O0BA 154.4(2) 2_556 . ?
O9AA Rb8 O3BA 52.2(2) 2_556 2_556 ?
O9AA Rb8 C4AA 77.7(3) 2_556 2_556 ?
O9AA Rb8 C7AA 66.4(3) 2_556 2_556 ?
O9AA Rb8 C2BA 60.0(3) 2_556 2_556 ?
O9AA Rb8 O6CA 63.0(3) 2_556 1_656 ?
O2BA Rb8 O4AA 53.6(3) 2_556 2_556 ?
O2BA Rb8 O9AA 80.7(2) 2_556 2_556 ?
O2BA Rb8 O0BA 123.0(2) 2_556 . ?
O2BA Rb8 O3BA 51.3(2) 2_556 2_556 ?
O2BA Rb8 O7BA 155.2(3) 2_556 . ?
O2BA Rb8 C4AA 57.6(3) 2_556 2_556 ?
O2BA Rb8 C7AA 94.8(3) 2_556 2_556 ?
O2BA Rb8 C2BA 71.9(3) 2_556 2_556 ?
O2BA Rb8 O6CA 143.7(3) 2_556 1_656 ?
O3BA Rb8 O0BA 132.8(2) 2_556 . ?
O3BA Rb8 C4AA 94.9(3) 2_556 2_556 ?
O3BA Rb8 C7AA 111.2(3) 2_556 2_556 ?
O3BA Rb8 C2BA 93.2(3) 2_556 2_556 ?
O3BA Rb8 O6CA 102.6(3) 2_556 1_656 ?
O7BA Rb8 O4AA 134.3(2) . 2_556 ?
O7BA Rb8 O9AA 113.0(3) . 2_556 ?
O7BA Rb8 O0BA 49.7(2) . . ?
O7BA Rb8 O3BA 153.3(3) . 2_556 ?
O7BA Rb8 C4AA 103.6(3) . 2_556 ?
O7BA Rb8 C7AA 73.8(3) . 2_556 ?
O7BA Rb8 C2BA 96.4(3) . 2_556 ?
O7BA Rb8 O6CA 53.3(3) . 1_656 ?
C4AA Rb8 O0BA 121.7(2) 2_556 . ?
C4AA Rb8 O6CA 109.0(4) 2_556 1_656 ?
C7AA Rb8 O0BA 116.0(3) 2_556 . ?
C7AA Rb8 C4AA 40.2(3) 2_556 2_556 ?
C7AA Rb8 O6CA 69.6(4) 2_556 1_656 ?
C2BA Rb8 O0BA 132.2(3) 2_556 . ?
C2BA Rb8 C4AA 22.9(3) 2_556 2_556 ?
C2BA Rb8 C7AA 23.2(4) 2_556 2_556 ?
C2BA Rb8 O6CA 87.2(4) 2_556 1_656 ?
O9BA Rb8 O4AA 74.4(3) . 2_556 ?
O9BA Rb8 O9AA 155.4(3) . 2_556 ?
O9BA Rb8 O0BA 49.8(2) . . ?
O9BA Rb8 O2BA 79.2(2) . 2_556 ?
O9BA Rb8 O3BA 121.2(3) . 2_556 ?
O9BA Rb8 O7BA 81.6(3) . . ?
O9BA Rb8 C4AA 79.6(3) . 2_556 ?
O9BA Rb8 C7AA 101.3(3) . 2_556 ?
O9BA Rb8 C2BA 99.9(3) . 2_556 ?
O9BA Rb8 O6CA 134.9(3) . 1_656 ?
O5CA Rb8 O4AA 80.7(3) . 2_556 ?
O5CA Rb8 O9AA 74.9(3) . 2_556 ?
O5CA Rb8 O0BA 83.8(3) . . ?
O5CA Rb8 O2BA 119.8(3) . 2_556 ?
O5CA Rb8 O3BA 70.6(3) . 2_556 ?
O5CA Rb8 O7BA 84.5(3) . . ?
O5CA Rb8 C4AA 152.4(3) . 2_556 ?
O5CA Rb8 C7AA 122.2(4) . 2_556 ?
O5CA Rb8 C2BA 131.4(4) . 2_556 ?
O5CA Rb8 O9BA 128.0(3) . . ?
O5CA Rb8 O6CA 54.9(4) . 1_656 ?
O6CA Rb8 O0BA 93.1(3) 1_656 . ?
Mo1 O1 Mo3A 92.5(3) . . ?
Mo1 O1 Rb7 87.8(3) . . ?
Mo3A O1 Rb7 87.1(2) . . ?
P1 O1 Mo1 126.3(5) . . ?
P1 O1 Mo3A 126.4(5) . . ?
P1 O1 Rb7 124.6(4) . . ?
Mo1 O0AA Rb7 127.3(5) . . ?
Mo0A O1AA Rb7 100.6(4) . 2_545 ?
Mo3A O2AA Mo0A 94.1(3) . . ?
P0AA O2AA Mo0A 133.5(5) . . ?
P0AA O2AA Mo3A 130.8(5) . . ?
Mo2A O3AA Mo1A 94.3(3) . . ?
P1 O3AA Mo1A 133.6(5) . . ?
P1 O3AA Mo2A 131.0(5) . . ?
Mo1A O4AA Rb8 98.5(4) . 2_546 ?
Mo1 O5AA Mo2A 124.4(5) . . ?
Mo1 O6AA Mo3A 123.5(5) . . ?
Mo1 O6AA Rb6 139.0(4) . 2_455 ?
Mo3A O6AA Rb6 97.5(3) . 2_455 ?
Mo2A O7AA Rb6 139.0(5) . 2 ?
Mo0A O8AA Rb9 132.2(4) . . ?
Mo3A O8AA Mo0A 122.8(4) . . ?
Mo3A O8AA Rb9 105.0(4) . . ?
Mo0A O9AA Rb8 111.4(4) . 2_546 ?
Mo1 O0BA Mo2A 93.2(3) . . ?
Mo1 O0BA Rb8 85.9(3) . . ?
Mo2A O0BA Rb8 87.5(2) . . ?
P0AA O0BA Mo1 127.0(5) . . ?
P0AA O0BA Mo2A 125.5(5) . . ?
P0AA O0BA Rb8 125.3(4) . . ?
Mo3A O1BA Rb6 114.0(4) . 2_455 ?
Mo1A O2BA Rb8 93.1(3) . 2_546 ?
P0AA O2BA Mo1A 121.3(5) . . ?
P0AA O2BA Rb8 120.3(5) . 2_546 ?
Mo0A O3BA Mo1A 153.0(6) . . ?
Mo0A O3BA Rb7 91.2(3) . 2_545 ?
Mo0A O3BA Rb8 96.2(3) . 2_546 ?
Mo1A O3BA Rb7 96.9(3) . 2_545 ?
Mo1A O3BA Rb8 92.6(3) . 2_546 ?
Rb7 O3BA Rb8 143.4(3) 2_545 2_546 ?
Mo0A O4BA Rb7 90.4(3) . 2_545 ?
P1 O4BA Mo0A 120.9(5) . . ?
P1 O4BA Rb7 123.3(5) . 2_545 ?
Mo1A O5BA Mo2A 122.6(4) . . ?
Mo3A O6BA Rb7 128.5(4) . . ?
Mo3A O6BA Rb9 100.4(4) . . ?
Rb7 O6BA Rb9 115.1(3) . . ?
Mo2A O7BA Rb8 131.5(4) . . ?
C1AA C1 P1 114.5(10) . . ?
C4AA C0AA P0AA 114.6(10) . . ?
C1 C1AA Rb7 110.8(8) . 2_545 ?
C5AA C1AA Rb7 76.1(9) . 2_545 ?
C5AA C1AA C1 122.4(12) . . ?
C5AA C1AA C9AA 118.9(13) . . ?
C9AA C1AA Rb7 82.4(8) . 2_545 ?
C9AA C1AA C1 118.7(12) . . ?
Mo1A O8BA Rb7 113.0(4) . 2_545 ?
Rb9 C2AA Rb7 161.1(4) 1_655 2_545 ?
C3AA C2AA Rb7 74.8(8) . 2_545 ?
C3AA C2AA Rb9 110.6(9) . 1_655 ?
C3AA C2AA N2AA 125.6(13) . . ?
C8AA C2AA Rb7 81.6(8) . 2_545 ?
C8AA C2AA Rb9 80.0(8) . 1_655 ?
C8AA C2AA C3AA 119.9(12) . . ?
C8AA C2AA N2AA 114.5(12) . . ?
N2AA C2AA Rb7 117.2(8) . 2_545 ?
N2AA C2AA Rb9 75.2(7) . 1_655 ?
C2AA C3AA Rb7 83.1(8) . 2_545 ?
C5AA C3AA Rb7 77.2(8) . 2_545 ?
C5AA C3AA C2AA 120.5(12) . . ?
C0AA C4AA Rb8 109.3(8) . 2_546 ?
C6AA C4AA Rb8 85.7(8) . 2_546 ?
C6AA C4AA C0AA 120.0(12) . . ?
C2BA C4AA Rb8 74.5(8) . 2_546 ?
C2BA C4AA C0AA 120.6(12) . . ?
C2BA C4AA C6AA 119.4(13) . . ?
C1AA C5AA Rb7 81.6(8) . 2_545 ?
C3AA C5AA Rb7 80.4(9) . 2_545 ?
C3AA C5AA C1AA 120.5(12) . . ?
C4AA C6AA Rb8 72.4(8) . 2_546 ?
C4AA C6AA C1BA 119.6(13) . . ?
C1BA C6AA Rb8 81.7(9) . 2_546 ?
C0BA C7AA Rb8 85.5(8) . 2_546 ?
C0BA C7AA C2BA 118.7(13) . . ?
C2BA C7AA Rb8 75.9(8) . 2_546 ?
Rb9 C8AA Rb7 154.7(4) 1_655 2_545 ?
C2AA C8AA Rb7 77.0(8) . 2_545 ?
C2AA C8AA Rb9 78.1(8) . 1_655 ?
C2AA C8AA C9AA 119.5(12) . . ?
C9AA C8AA Rb7 77.3(8) . 2_545 ?
C9AA C8AA Rb9 111.5(9) . 1_655 ?
C1AA C9AA Rb7 75.6(8) . 2_545 ?
C1AA C9AA C8AA 120.8(13) . . ?
C8AA C9AA Rb7 81.0(9) . 2_545 ?
C7AA C0BA Rb8 72.1(8) . 2_546 ?
C7AA C0BA N1 122.8(14) . . ?
C1BA C0BA Rb8 83.6(9) . 2_546 ?
C1BA C0BA C7AA 120.8(13) . . ?
C1BA C0BA N1 116.3(13) . . ?
N1 C0BA Rb8 115.8(9) . 2_546 ?
C0BA C1BA C6AA 120.6(13) . . ?
C4AA C2BA Rb8 82.6(8) . 2_546 ?
C4AA C2BA C7AA 120.8(13) . . ?
C7AA C2BA Rb8 80.8(9) . 2_546 ?
C0BA N1 Rb6 133.3(9) . 1_556 ?
N0AA N1 Rb6 108.4(9) . 1_556 ?
N0AA N1 C0BA 118.3(12) . . ?
N1 N0AA Rb6 52.3(7) . 1_556 ?
N3AA N0AA Rb6 117.6(11) . 1_556 ?
N3AA N0AA N1 169.9(15) . . ?
N4AA N1AA N2AA 170.0(15) . . ?
Rb6 N2AA Rb9 83.4(3) 1_655 1_655 ?
C2AA N2AA Rb6 130.1(9) . 1_655 ?
C2AA N2AA Rb9 81.9(8) . 1_655 ?
N1AA N2AA Rb6 110.5(9) . 1_655 ?
N1AA N2AA Rb9 127.2(9) . 1_655 ?
N1AA N2AA C2AA 116.4(12) . . ?
Mo1 O9BA Rb8 131.0(5) . . ?
Rb6 O3CA Rb9 91.3(3) . . ?
Rb9 O4CA Rb6 97.5(3) . . ?
Rb9 O6CA Rb8 169.6(6) . 1_454 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Rb6 Mo3A O6BA Rb7 99.9(5) 2_455 . . . ?
Rb6 Mo3A O6BA Rb9 -126.0(2) 2_455 . . . ?
Rb6 N1 N0AA N3AA -1(10) 1_556 . . . ?
Rb7 Mo1 O9BA Rb8 -168.6(3) . . . . ?
Rb7 Mo0A O9AA Rb8 64.1(5) 2_545 . . 2_546 ?
Rb7 Mo0A O3BA Mo1A 107.7(11) 2_545 . . . ?
Rb7 Mo0A O3BA Rb8 -144.1(4) 2_545 . . 2_546 ?
Rb7 Mo1A O4AA Rb8 -90.6(3) 2_545 . . 2_546 ?
Rb7 Mo3A O1BA Rb6 -72.1(5) . . . 2_455 ?
Rb7 Mo3A O6BA Rb9 134.1(7) . . . . ?
Rb7 P1 O1 Mo1 147.9(3) 2_545 . . . ?
Rb7 P1 O1 Mo3A 20.3(10) 2_545 . . . ?
Rb7 P1 O1 Rb7 -95.3(7) 2_545 . . . ?
Rb7 P1 O3AA Mo1A -37.1(6) 2_545 . . . ?
Rb7 P1 O3AA Mo2A 157.9(6) 2_545 . . . ?
Rb7 P1 O4BA Mo0A 113.7(7) 2_545 . . . ?
Rb7 P1 C1 C1AA -11.5(9) 2_545 . . . ?
Rb7 C1AA C5AA C3AA 73.6(13) 2_545 . . . ?
Rb7 C1AA C9AA C8AA -70.1(13) 2_545 . . . ?
Rb7 C2AA C3AA C5AA -70.8(13) 2_545 . . . ?
Rb7 C2AA C8AA Rb9 175.2(3) 2_545 . . 1_655 ?
Rb7 C2AA C8AA C9AA 67.1(12) 2_545 . . . ?
Rb7 C2AA N2AA Rb6 90.4(10) 2_545 . . 1_655 ?
Rb7 C2AA N2AA Rb9 164.6(6) 2_545 . . 1_655 ?
Rb7 C2AA N2AA N1AA -67.8(14) 2_545 . . . ?
Rb7 C3AA C5AA C1AA -74.3(13) 2_545 . . . ?
Rb7 C8AA C9AA C1AA 67.2(13) 2_545 . . . ?
Rb9 Mo3A O1BA Rb6 -149.7(3) . . . 2_455 ?
Rb9 Mo3A O6BA Rb7 -134.1(7) . . . . ?
Rb9 C2AA C3AA Rb7 160.9(5) 1_655 . . 2_545 ?
Rb9 C2AA C3AA C5AA 90.2(14) 1_655 . . . ?
Rb9 C2AA C8AA Rb7 -175.2(3) 1_655 . . 2_545 ?
Rb9 C2AA C8AA C9AA -108.1(13) 1_655 . . . ?
Rb9 C2AA N2AA Rb6 -74.2(9) 1_655 . . 1_655 ?
Rb9 C2AA N2AA N1AA 127.6(12) 1_655 . . . ?
Rb9 C8AA C9AA Rb7 -155.1(6) 1_655 . . 2_545 ?
Rb9 C8AA C9AA C1AA -87.9(14) 1_655 . . . ?
P1 C1 C1AA Rb7 13.6(11) . . . 2_545 ?
P1 C1 C1AA C5AA -72.7(15) . . . . ?
P1 C1 C1AA C9AA 106.4(13) . . . . ?
P0AA C0AA C4AA Rb8 19.0(11) . . . 2_546 ?
P0AA C0AA C4AA C6AA 115.3(13) . . . . ?
P0AA C0AA C4AA C2BA -64.0(15) . . . . ?
Rb8 Mo1 O0AA Rb7 -169.7(3) . . . . ?
Rb8 Mo0A O1AA Rb7 -89.5(3) 2_546 . . 2_545 ?
Rb8 Mo0A O3BA Mo1A -108.2(11) 2_546 . . . ?
Rb8 Mo0A O3BA Rb7 144.1(4) 2_546 . . 2_545 ?
Rb8 Mo1A O8BA Rb7 58.3(6) 2_546 . . 2_545 ?
Rb8 Mo2A O7AA Rb6 -46.1(8) . . . 2 ?
Rb8 P0AA O2AA Mo0A -40.6(6) 2_546 . . . ?
Rb8 P0AA O2AA Mo3A 157.8(6) 2_546 . . . ?
Rb8 P0AA O0BA Mo1 149.6(4) 2_546 . . . ?
Rb8 P0AA O0BA Mo2A 20.9(11) 2_546 . . . ?
Rb8 P0AA O0BA Rb8 -95.2(7) 2_546 . . . ?
Rb8 P0AA O2BA Mo1A 115.3(7) 2_546 . . . ?
Rb8 P0AA C0AA C4AA -16.1(9) 2_546 . . . ?
Rb8 C4AA C6AA C1BA -69.2(13) 2_546 . . . ?
Rb8 C4AA C2BA C7AA 74.7(13) 2_546 . . . ?
Rb8 C6AA C1BA C0BA -63.8(14) 2_546 . . . ?
Rb8 C7AA C0BA C1BA 70.8(14) 2_546 . . . ?
Rb8 C7AA C0BA N1 -109.6(13) 2_546 . . . ?
Rb8 C7AA C2BA C4AA -75.7(13) 2_546 . . . ?
Rb8 C0BA C1BA C6AA 64.5(14) 2_546 . . . ?
Rb8 C0BA N1 Rb6 119.6(9) 2_546 . . 1_556 ?
Rb8 C0BA N1 N0AA -58.9(16) 2_546 . . . ?
O1 Mo1 O0AA Rb7 25.3(5) . . . . ?
O1 Mo1 O9BA Rb8 61(2) . . . . ?
O1 Mo3A O1BA Rb6 37.1(17) . . . 2_455 ?
O1 Mo3A O6BA Rb7 -24.0(5) . . . . ?
O1 Mo3A O6BA Rb9 110.1(3) . . . . ?
O1 P1 O3AA Mo1A 115.0(7) . . . . ?
O1 P1 O3AA Mo2A -49.9(8) . . . . ?
O1 P1 O4BA Mo0A -61.8(7) . . . . ?
O1 P1 O4BA Rb7 -175.5(4) . . . 2_545 ?
O1 P1 C1 C1AA -166.4(9) . . . . ?
O0AA Mo1 O9BA Rb8 -146.6(6) . . . . ?
O1AA Mo0A O9AA Rb8 115.1(4) . . . 2_546 ?
O1AA Mo0A O3BA Mo1A 137.6(10) . . . . ?
O1AA Mo0A O3BA Rb7 29.9(4) . . . 2_545 ?
O1AA Mo0A O3BA Rb8 -114.2(4) . . . 2_546 ?
O2AA Mo0A O1AA Rb7 84.0(17) . . . 2_545 ?
O2AA Mo0A O9AA Rb8 -72.9(4) . . . 2_546 ?
O2AA Mo0A O3BA Mo1A -31.0(10) . . . . ?
O2AA Mo0A O3BA Rb7 -138.7(3) . . . 2_545 ?
O2AA Mo0A O3BA Rb8 77.2(3) . . . 2_546 ?
O2AA Mo3A O1BA Rb6 90.1(4) . . . 2_455 ?
O2AA Mo3A O6BA Rb7 -53.8(13) . . . . ?
O2AA Mo3A O6BA Rb9 80.3(10) . . . . ?
O2AA P0AA O0BA Mo1 31.1(8) . . . . ?
O2AA P0AA O0BA Mo2A -97.6(6) . . . . ?
O2AA P0AA O0BA Rb8 146.3(5) . . . . ?
O2AA P0AA O2BA Mo1A 61.9(7) . . . . ?
O2AA P0AA O2BA Rb8 -53.4(6) . . . 2_546 ?
O2AA P0AA C0AA C4AA 66.7(11) . . . . ?
O3AA Mo1A O4AA Rb8 84.9(18) . . . 2_546 ?
O3AA Mo1A O8BA Rb7 -75.1(4) . . . 2_545 ?
O3AA Mo2A O7AA Rb6 113.7(7) . . . 2 ?
O3AA Mo2A O7BA Rb8 -53.2(13) . . . . ?
O3AA P1 O1 Mo1 31.7(7) . . . . ?
O3AA P1 O1 Mo3A -95.9(6) . . . . ?
O3AA P1 O1 Rb7 148.5(5) . . . . ?
O3AA P1 O4BA Mo0A 61.4(7) . . . . ?
O3AA P1 O4BA Rb7 -52.3(6) . . . 2_545 ?
O3AA P1 C1 C1AA 72.4(11) . . . . ?
O4AA Mo1A O8BA Rb7 112.4(5) . . . 2_545 ?
O5AA Mo1 O0AA Rb7 106.5(6) . . . . ?
O5AA Mo1 O9BA Rb8 -45.6(7) . . . . ?
O5AA Mo2A O7AA Rb6 31.4(7) . . . 2 ?
O5AA Mo2A O7BA Rb8 40.4(6) . . . . ?
O6AA Mo1 O0AA Rb7 -47.1(6) . . . . ?
O6AA Mo1 O9BA Rb8 108.3(6) . . . . ?
O6AA Mo3A O1BA Rb6 6.9(5) . . . 2_455 ?
O6AA Mo3A O6BA Rb7 45.6(6) . . . . ?
O6AA Mo3A O6BA Rb9 179.8(3) . . . . ?
O7AA Mo2A O7BA Rb8 138.7(6) . . . . ?
O8AA Mo0A O1AA Rb7 120.3(3) . . . 2_545 ?
O8AA Mo0A O9AA Rb8 -141.1(4) . . . 2_546 ?
O8AA Mo0A O3BA Mo1A 7.9(14) . . . . ?
O8AA Mo0A O3BA Rb7 -99.8(6) . . . 2_545 ?
O8AA Mo0A O3BA Rb8 116.1(6) . . . 2_546 ?
O8AA Mo3A O1BA Rb6 164.2(4) . . . 2_455 ?
O8AA Mo3A O6BA Rb7 -113.6(6) . . . . ?
O8AA Mo3A O6BA Rb9 20.6(4) . . . . ?
O9AA Mo0A O1AA Rb7 -135.4(4) . . . 2_545 ?
O9AA Mo0A O3BA Mo1A -116.0(11) . . . . ?
O9AA Mo0A O3BA Rb7 136.3(4) . . . 2_545 ?
O9AA Mo0A O3BA Rb8 -7.9(4) . . . 2_546 ?
O0BA Mo1 O0AA Rb7 65(2) . . . . ?
O0BA Mo1 O9BA Rb8 26.2(6) . . . . ?
O0BA Mo2A O7AA Rb6 55.0(18) . . . 2 ?
O0BA Mo2A O7BA Rb8 -27.7(6) . . . . ?
O0BA P0AA O2AA Mo0A 114.6(7) . . . . ?
O0BA P0AA O2AA Mo3A -47.1(8) . . . . ?
O0BA P0AA O2BA Mo1A -61.9(7) . . . . ?
O0BA P0AA O2BA Rb8 -177.2(4) . . . 2_546 ?
O0BA P0AA C0AA C4AA -172.6(9) . . . . ?
O1BA Mo3A O6BA Rb7 143.9(6) . . . . ?
O1BA Mo3A O6BA Rb9 -82.0(4) . . . . ?
O2BA Mo1A O4AA Rb8 42.8(3) . . . 2_546 ?
O2BA P0AA O2AA Mo0A -9.1(8) . . . . ?
O2BA P0AA O2AA Mo3A -170.7(6) . . . . ?
O2BA P0AA O0BA Mo1 153.4(5) . . . . ?
O2BA P0AA O0BA Mo2A 24.7(7) . . . . ?
O2BA P0AA O0BA Rb8 -91.4(6) . . . . ?
O2BA P0AA C0AA C4AA -52.0(11) . . . . ?
O3BA Mo0A O1AA Rb7 -32.3(4) . . . 2_545 ?
O3BA Mo0A O9AA Rb8 9.1(5) . . . 2_546 ?
O3BA Mo1A O4AA Rb8 -34.2(4) . . . 2_546 ?
O3BA Mo1A O8BA Rb7 7.1(5) . . . 2_545 ?
O4BA Mo0A O1AA Rb7 44.8(3) . . . 2_545 ?
O4BA Mo0A O3BA Mo1A 56.5(10) . . . . ?
O4BA Mo0A O3BA Rb7 -51.2(3) . . . 2_545 ?
O4BA Mo0A O3BA Rb8 164.7(4) . . . 2_546 ?
O4BA P1 O1 Mo1 153.3(5) . . . . ?
O4BA P1 O1 Mo3A 25.7(7) . . . . ?
O4BA P1 O1 Rb7 -90.0(6) . . . . ?
O4BA P1 O3AA Mo1A -7.7(8) . . . . ?
O4BA P1 O3AA Mo2A -172.7(6) . . . . ?
O4BA P1 C1 C1AA -45.7(11) . . . . ?
O5BA Mo1A O4AA Rb8 119.5(3) . . . 2_546 ?
O5BA Mo1A O8BA Rb7 -142.9(4) . . . 2_545 ?
O5BA Mo2A O7AA Rb6 -171.7(6) . . . 2 ?
O5BA Mo2A O7BA Rb8 -117.8(6) . . . . ?
O6BA Mo3A O1BA Rb6 -96.5(5) . . . 2_455 ?
O7BA Mo2A O7AA Rb6 -71.2(7) . . . 2 ?
C1 P1 O1 Mo1 -87.3(7) . . . . ?
C1 P1 O1 Mo3A 145.1(6) . . . . ?
C1 P1 O1 Rb7 29.4(7) . . . . ?
C1 P1 O3AA Mo1A -125.9(7) . . . . ?
C1 P1 O3AA Mo2A 69.2(8) . . . . ?
C1 P1 O4BA Mo0A 179.2(6) . . . . ?
C1 P1 O4BA Rb7 65.4(7) . . . 2_545 ?
C1 C1AA C5AA Rb7 106.0(12) . . . 2_545 ?
C1 C1AA C5AA C3AA 179.7(13) . . . . ?
C1 C1AA C9AA Rb7 -109.6(11) . . . 2_545 ?
C1 C1AA C9AA C8AA -179.7(13) . . . . ?
C0AA P0AA O2AA Mo0A -127.8(7) . . . . ?
C0AA P0AA O2AA Mo3A 70.6(8) . . . . ?
C0AA P0AA O0BA Mo1 -87.6(7) . . . . ?
C0AA P0AA O0BA Mo2A 143.6(6) . . . . ?
C0AA P0AA O0BA Rb8 27.5(7) . . . . ?
C0AA P0AA O2BA Mo1A -179.6(6) . . . . ?
C0AA P0AA O2BA Rb8 65.1(7) . . . 2_546 ?
C0AA C4AA C6AA Rb8 -109.8(12) . . . 2_546 ?
C0AA C4AA C6AA C1BA -179.0(13) . . . . ?
C0AA C4AA C2BA Rb8 103.5(12) . . . 2_546 ?
C0AA C4AA C2BA C7AA 178.2(13) . . . . ?
O8BA Mo1A O4AA Rb8 -135.2(4) . . . 2_546 ?
C2AA C3AA C5AA Rb7 74.0(13) . . . 2_545 ?
C2AA C3AA C5AA C1AA 0(2) . . . . ?
C2AA C8AA C9AA Rb7 -66.9(12) . . . 2_545 ?
C2AA C8AA C9AA C1AA 0(2) . . . . ?
C3AA C2AA C8AA Rb7 -67.1(12) . . . 2_545 ?
C3AA C2AA C8AA Rb9 108.2(13) . . . 1_655 ?
C3AA C2AA C8AA C9AA 0(2) . . . . ?
C3AA C2AA N2AA Rb6 -179.3(11) . . . 1_655 ?
C3AA C2AA N2AA Rb9 -105.0(14) . . . 1_655 ?
C3AA C2AA N2AA N1AA 23(2) . . . . ?
C4AA C6AA C1BA C0BA 0(2) . . . . ?
C5AA C1AA C9AA Rb7 69.5(12) . . . 2_545 ?
C5AA C1AA C9AA C8AA -1(2) . . . . ?
C6AA C4AA C2BA Rb8 -75.7(12) . . . 2_546 ?
C6AA C4AA C2BA C7AA -1(2) . . . . ?
C7AA C0BA C1BA C6AA 0(2) . . . . ?
C7AA C0BA N1 Rb6 -155.8(11) . . . 1_556 ?
C7AA C0BA N1 N0AA 26(2) . . . . ?
C8AA C2AA C3AA Rb7 70.7(12) . . . 2_545 ?
C8AA C2AA C3AA C5AA 0(2) . . . . ?
C8AA C2AA N2AA Rb6 -2.7(18) . . . 1_655 ?
C8AA C2AA N2AA Rb9 71.5(11) . . . 1_655 ?
C8AA C2AA N2AA N1AA -160.9(13) . . . . ?
C9AA C1AA C5AA Rb7 -73.0(12) . . . 2_545 ?
C9AA C1AA C5AA C3AA 1(2) . . . . ?
C0BA C7AA C2BA Rb8 76.8(13) . . . 2_546 ?
C0BA C7AA C2BA C4AA 1(2) . . . . ?
C0BA N1 N0AA Rb6 178.8(17) . . . 1_556 ?
C0BA N1 N0AA N3AA 178(9) . . . . ?
C1BA C0BA N1 Rb6 24(2) . . . 1_556 ?
C1BA C0BA N1 N0AA -154.7(14) . . . . ?
C2BA C4AA C6AA Rb8 69.5(12) . . . 2_546 ?
C2BA C4AA C6AA C1BA 0(2) . . . . ?
C2BA C7AA C0BA Rb8 -71.3(12) . . . 2_546 ?
C2BA C7AA C0BA C1BA 0(2) . . . . ?
C2BA C7AA C0BA N1 179.1(13) . . . . ?
N1 C0BA C1BA C6AA -179.8(13) . . . . ?
N2AA C2AA C3AA Rb7 -112.9(13) . . . 2_545 ?
N2AA C2AA C3AA C5AA 176.4(14) . . . . ?
N2AA C2AA C8AA Rb7 116.2(11) . . . 2_545 ?
N2AA C2AA C8AA Rb9 -68.6(11) . . . 1_655 ?
N2AA C2AA C8AA C9AA -176.7(13) . . . . ?
N4AA N1AA N2AA Rb6 10(9) . . . 1_655 ?
N4AA N1AA N2AA Rb9 -88(9) . . . 1_655 ?
N4AA N1AA N2AA C2AA 172(8) . . . . ?
O9BA Mo1 O0AA Rb7 -148.9(6) . . . . ?

_shelx_SHELXL_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
