 
data_1 
 
_audit_creation_method            SHELXL-97 
_chemical_name_systematic 
; 
 ? 
; 
_chemical_name_common             ? 
_chemical_melting_point           ? 
_chemical_formula_moiety          ? 
_chemical_formula_sum 
 'B10 O23 Sr3 V2' 
_chemical_formula_weight          840.84 
 
loop_ 
 _atom_type_symbol 
 _atom_type_description 
 _atom_type_scat_dispersion_real 
 _atom_type_scat_dispersion_imag 
 _atom_type_scat_source 
 'O'  'O'   0.0106   0.0060 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'B'  'B'   0.0013   0.0007 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'V'  'V'   0.3005   0.5294 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Sr'  'Sr'  -1.5307   3.2498 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 
_symmetry_cell_setting            Triclinic 
_symmetry_space_group_name_H-M     P-1 
 
loop_ 
 _symmetry_equiv_pos_as_xyz 
 'x, y, z' 
 '-x, -y, -z' 
 
_cell_length_a                    6.639(2) 
_cell_length_b                    11.571(4) 
_cell_length_c                    12.998(4) 
_cell_angle_alpha                 114.333(3) 
_cell_angle_beta                  103.334(3) 
_cell_angle_gamma                 90.432(3) 
_cell_volume                      879.3(5) 
_cell_formula_units_Z             2 
_cell_measurement_temperature     296(2) 
_cell_measurement_reflns_used     1942 
_cell_measurement_theta_min       3.15 
_cell_measurement_theta_max       27.68 
 
_exptl_crystal_description        block
_exptl_crystal_colour             colorless 
_exptl_crystal_size_max           0.20 
_exptl_crystal_size_mid           0.15 
_exptl_crystal_size_min           0.10 
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_diffrn     3.176 
_exptl_crystal_density_method     'not measured' 
_exptl_crystal_F_000              788 
_exptl_absorpt_coefficient_mu     10.193 
_exptl_absorpt_correction_type     numerical 
_exptl_absorpt_correction_T_min   0.2350 
_exptl_absorpt_correction_T_max   0.4288 
_exptl_absorpt_process_details    'face-indexed'
 
_exptl_special_details 
; 
 ? 
; 
 
_diffrn_ambient_temperature       296(2) 
_diffrn_radiation_wavelength      0.71073 
_diffrn_radiation_type            MoK\a 
_diffrn_radiation_source          'fine-focus sealed tube' 
_diffrn_radiation_monochromator   graphite 
_diffrn_measurement_device_type   'multiwire proportional' 
_diffrn_measurement_method         'phi and omega scans' 
_diffrn_detector_area_resol_mean  ? 
_diffrn_standards_number          ? 
_diffrn_standards_interval_count  ? 
_diffrn_standards_interval_time   ? 
_diffrn_standards_decay_%         ? 
_diffrn_reflns_number             6431 
_diffrn_reflns_av_R_equivalents   0.0432 
_diffrn_reflns_av_sigmaI/netI     0.0756 
_diffrn_reflns_limit_h_min        -8 
_diffrn_reflns_limit_h_max        8 
_diffrn_reflns_limit_k_min        -15 
_diffrn_reflns_limit_k_max        14 
_diffrn_reflns_limit_l_min        -12 
_diffrn_reflns_limit_l_max        16 
_diffrn_reflns_theta_min          3.15 
_diffrn_reflns_theta_max          27.68 
_reflns_number_total              3951 
_reflns_number_gt                 3022 
_reflns_threshold_expression      >2sigma(I) 
 
_computing_data_collection         'Bruker FRAMBO' 
_computing_cell_refinement         'Bruker FRAMBO' 
_computing_data_reduction         'Bruker SAINT' 
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)' 
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)' 
_computing_molecular_graphics      'Bruker SHELXTL' 
_computing_publication_material   'Bruker SHELXTL' 
 
_refine_special_details 
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
; 
 
_refine_ls_structure_factor_coef  Fsqd  
_refine_ls_matrix_type            full 
_refine_ls_weighting_scheme       calc  
_refine_ls_weighting_details 
 'calc w=1/[σ²(Fo²)+(0.0645P)²+6.2160P] where P=(Fo²+2Fc²)/3' 
_atom_sites_solution_primary      direct 
_atom_sites_solution_secondary    difmap 
_atom_sites_solution_hydrogens    ? 
_refine_ls_hydrogen_treatment     ? 
_refine_ls_extinction_method      none 
_refine_ls_extinction_coef        ? 
_refine_ls_number_reflns          3951 
_refine_ls_number_parameters      388 
_refine_ls_number_restraints      18 
_refine_ls_R_factor_all           0.0722 
_refine_ls_R_factor_gt            0.0516 
_refine_ls_wR_factor_ref          0.1406 
_refine_ls_wR_factor_gt           0.1245 
_refine_ls_goodness_of_fit_ref    1.018 
_refine_ls_restrained_S_all       1.016 
_refine_ls_shift/su_max           0.000 
_refine_ls_shift/su_mean          0.000 
 
loop_ 
 _atom_site_label 
 _atom_site_type_symbol 
 _atom_site_fract_x 
 _atom_site_fract_y 
 _atom_site_fract_z 
 _atom_site_U_iso_or_equiv 
 _atom_site_adp_type 
 _atom_site_occupancy 
 _atom_site_symmetry_multiplicity 
 _atom_site_calc_flag 
 _atom_site_refinement_flags 
 _atom_site_disorder_assembly 
 _atom_site_disorder_group 
B1 B 0.2026(12) 0.8741(7) 0.3213(7) 0.0106(15) Uani 1 1 d . . . 
B2 B 0.9183(11) 0.7577(7) 0.3443(7) 0.0086(15) Uani 1 1 d . . . 
B3 B 0.2642(12) 0.6064(8) 0.6385(7) 0.0103(15) Uani 1 1 d . . . 
B4 B -0.0837(11) 0.6598(7) 0.6707(7) 0.0081(14) Uani 1 1 d . . . 
B5 B -0.4204(12) 0.7496(7) 0.6609(7) 0.0094(15) Uani 1 1 d . . . 
B6 B -0.4729(12) 0.9480(8) 0.6326(7) 0.0104(15) Uani 1 1 d . . . 
B7 B 0.0438(14) 0.2908(9) -0.1524(8) 0.0183(18) Uani 1 1 d . . . 
B8 B -0.0157(12) 0.5591(8) 0.3804(7) 0.0111(15) Uani 1 1 d . . . 
B9 B 0.4173(12) 1.1435(8) 0.6280(7) 0.0112(15) Uani 1 1 d . . . 
B10 B -0.1936(13) 0.7946(9) -0.1509(8) 0.0157(17) Uani 1 1 d . . . 
O1 O 0.1369(9) 1.1449(7) 0.0312(5) 0.0318(16) Uani 1 1 d . . . 
O2 O -0.3675(7) 0.8172(5) -0.2132(4) 0.0135(11) Uani 1 1 d . . . 
O3 O 0.1193(8) 0.8020(5) 0.1946(5) 0.0163(11) Uani 1 1 d . . . 
O4 O 0.1064(10) 0.3587(6) -0.0331(5) 0.0312(16) Uani 1 1 d . . . 
O5 O 0.7332(7) 0.7836(5) 0.3939(4) 0.0096(10) Uani 1 1 d . . . 
O6 O 0.3859(7) 0.8151(5) 0.3599(5) 0.0132(11) Uani 1 1 d . . . 
O7 O 0.0462(7) 0.8770(4) 0.3825(4) 0.0089(10) Uani 1 1 d . . . 
O8 O 0.3708(7) 1.0273(5) 0.6267(5) 0.0140(11) Uani 1 1 d . . . 
O9 O -0.2713(7) 0.9928(4) 0.6524(4) 0.0109(10) Uani 1 1 d . . . 
O10 O -0.2360(7) 0.7195(5) 0.6165(4) 0.0081(9) Uani 1 1 d . . . 
O11 O 0.1179(7) 0.6887(5) 0.6508(5) 0.0124(10) Uani 1 1 d . . . 
O12 O 0.4492(7) 0.6246(5) 0.6183(4) 0.0106(10) Uani 1 1 d . . . 
O13 O 0.1357(7) 0.4812(5) 0.3799(5) 0.0125(10) Uani 1 1 d . . . 
O14 O 0.0417(7) 0.6806(5) 0.4006(4) 0.0109(10) Uani 1 1 d . . . 
O15 O 0.7816(7) 0.5135(5) 0.3652(5) 0.0116(10) Uani 1 1 d . . . 
O16 O -0.0597(8) 0.7110(5) -0.2015(5) 0.0173(11) Uani 1 1 d . . . 
O17 O -0.5431(7) 0.8282(4) 0.6098(4) 0.0102(10) Uani 1 1 d . . . 
O18 O 0.1446(8) 0.3148(5) -0.2213(4) 0.0166(12) Uani 1 1 d . . . 
O20 O 0.1438(17) 0.9600(10) -0.1855(10) 0.019(2) Uani 0.50 1 d PU . . 
O21 O 0.5880(15) 1.0701(10) 0.0054(10) 0.017(2) Uani 0.50 1 d P . . 
O22 O 0.4212(16) 0.5707(10) 0.0094(10) 0.018(2) Uani 0.50 1 d P . . 
O23 O 0.304(2) 0.5453(11) 0.1903(10) 0.027(3) Uani 0.50 1 d P . . 
O24 O 0.455(2) 1.1367(13) -0.0734(13) 0.038(3) Uani 0.50 1 d P . . 
O26 O 0.516(2) 0.3685(13) 0.0816(13) 0.037(3) Uani 0.50 1 d P . . 
O27 O 0.419(2) 0.4403(13) 0.1819(12) 0.038(3) Uani 0.50 1 d P . . 
O28 O 0.305(2) 0.5970(15) 0.0892(14) 0.047(4) Uani 0.50 1 d P . . 
O29 O 0.260(3) 1.0642(19) -0.1765(18) 0.070(5) Uani 0.50 1 d PU . . 
O30 O 0.218(3) 0.906(2) -0.0891(18) 0.074(6) Uani 0.50 1 d PU . . 
Sr1 Sr 0.19418(10) 0.74734(7) -0.00453(6) 0.01318(18) Uani 1 1 d . . . 
Sr2 Sr 0.45438(10) 0.61765(6) 0.40101(6) 0.01179(18) Uani 1 1 d . . . 
Sr3 Sr 0.04839(10) 0.88400(6) 0.60341(6) 0.01154(18) Uani 1 1 d . . . 
V4 V 0.3502(2) 0.45652(13) 0.06112(12) 0.0199(3) Uani 1 1 d . . . 
V5 V 0.2991(2) 1.04872(15) -0.05912(12) 0.0260(4) Uani 1 1 d . . . 
 
 
_geom_special_details 
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
; 
 
loop_ 
 _geom_bond_atom_site_label_1 
 _geom_bond_atom_site_label_2 
 _geom_bond_distance 
 _geom_bond_site_symmetry_2 
 _geom_bond_publ_flag 
B1 O7 1.440(9) . ? 
B1 O3 1.467(9) . ? 
B1 O9 1.477(9) 2_576 ? 
B1 O6 1.488(9) . ? 
B1 Sr3 3.183(8) 2_576 ? 
B2 O18 1.420(9) 2_665 ? 
B2 O7 1.448(9) 1_655 ? 
B2 O5 1.492(8) . ? 
B2 O14 1.507(9) 1_655 ? 
B2 Sr3 2.967(8) 1_655 ? 
B3 O12 1.346(9) . ? 
B3 O11 1.355(9) . ? 
B3 O15 1.397(10) 2_666 ? 
B3 Sr2 3.145(8) 2_666 ? 
B4 O10 1.442(9) . ? 
B4 O11 1.481(8) . ? 
B4 O16 1.485(9) 1_556 ? 
B4 O13 1.489(9) 2_566 ? 
B4 Sr3 3.233(8) . ? 
B5 O2 1.445(9) 1_556 ? 
B5 O10 1.456(9) . ? 
B5 O17 1.480(9) . ? 
B5 O12 1.499(9) 1_455 ? 
B5 Sr2 2.978(8) 1_455 ? 
B6 O17 1.348(9) . ? 
B6 O9 1.359(9) . ? 
B6 O8 1.400(9) 1_455 ? 
B6 Sr3 3.158(8) 1_455 ? 
B7 O18 1.344(10) . ? 
B7 O3 1.360(10) 2_565 ? 
B7 O4 1.375(11) . ? 
B7 Sr1 3.012(9) 2_565 ? 
B8 O14 1.354(9) . ? 
B8 O13 1.354(9) . ? 
B8 O15 1.382(9) 1_455 ? 
B8 Sr2 3.115(8) . ? 
B9 O6 1.340(9) 2_676 ? 
B9 O5 1.367(9) 2_676 ? 
B9 O8 1.370(10) . ? 
B9 Sr2 3.079(8) 2_676 ? 
B10 O2 1.344(10) . ? 
B10 O1 1.371(10) 2_575 ? 
B10 O16 1.384(9) . ? 
B10 Sr1 3.027(9) . ? 
O1 B10 1.371(10) 2_575 ? 
O1 V5 1.817(6) . ? 
O1 Sr1 2.559(6) 2_575 ? 
O2 B5 1.445(9) 1_554 ? 
O3 B7 1.360(10) 2_565 ? 
O3 Sr1 2.568(5) . ? 
O4 V4 1.821(6) . ? 
O4 Sr1 2.576(6) 2_565 ? 
O5 B9 1.367(9) 2_676 ? 
O5 Sr2 2.701(5) . ? 
O5 Sr3 2.806(5) 1_655 ? 
O6 B9 1.340(9) 2_676 ? 
O6 Sr2 2.573(5) . ? 
O7 B2 1.448(9) 1_455 ? 
O7 Sr3 2.781(5) 2_576 ? 
O7 Sr3 2.835(5) . ? 
O8 B6 1.400(9) 1_655 ? 
O8 Sr3 2.579(5) . ? 
O9 B1 1.477(9) 2_576 ? 
O9 Sr3 2.549(5) . ? 
O10 Sr3 2.752(5) . ? 
O10 Sr2 2.837(5) 1_455 ? 
O11 Sr3 2.595(5) . ? 
O12 B5 1.499(9) 1_655 ? 
O12 Sr2 2.800(5) . ? 
O12 Sr2 2.802(5) 2_666 ? 
O13 B4 1.489(9) 2_566 ? 
O13 Sr2 2.523(5) . ? 
O14 B2 1.507(9) 1_455 ? 
O14 Sr3 2.706(5) . ? 
O14 Sr2 2.839(5) . ? 
O15 B8 1.382(9) 1_655 ? 
O15 B3 1.397(10) 2_666 ? 
O15 Sr2 2.536(5) . ? 
O16 B4 1.485(9) 1_554 ? 
O16 Sr1 2.585(5) . ? 
O17 Sr3 2.783(5) 1_455 ? 
O17 Sr2 2.798(5) 1_455 ? 
O18 B2 1.420(10) 2_665 ? 
O20 O29 1.37(2) . ? 
O20 O30 1.60(2) . ? 
O20 V5 1.621(11) . ? 
O20 Sr3 2.431(11) 1_554 ? 
O21 O30 1.42(2) 2_675 ? 
O21 O24 1.632(19) . ? 
O21 V5 1.872(11) 2_675 ? 
O21 V5 1.877(10) . ? 
O21 Sr1 2.557(11) 2_675 ? 
O22 O28 1.372(17) . ? 
O22 O26 1.726(17) 2_665 ? 
O22 V4 1.813(10) . ? 
O22 V4 1.912(10) 2_665 ? 
O22 Sr1 2.590(11) . ? 
O23 O27 1.417(19) . ? 
O23 O28 1.65(2) . ? 
O23 V4 1.669(12) . ? 
O23 Sr2 2.456(11) . ? 
O24 V5 1.541(13) . ? 
O24 O29 1.56(2) . ? 
O24 Sr1 2.447(13) 2_675 ? 
O26 O27 1.52(2) . ? 
O26 V4 1.556(13) . ? 
O26 O22 1.726(17) 2_665 ? 
O26 Sr1 2.517(14) 2_665 ? 
O27 V4 1.619(14) . ? 
O27 Sr2 2.692(14) . ? 
O28 V4 1.560(16) . ? 
O28 Sr1 2.530(17) . ? 
O29 V5 1.57(2) . ? 
O29 Sr3 2.77(2) 1_554 ? 
O30 O21 1.42(2) 2_675 ? 
O30 V5 1.59(2) . ? 
O30 Sr1 2.52(2) . ? 
Sr1 O24 2.447(14) 2_675 ? 
Sr1 O26 2.517(14) 2_665 ? 
Sr1 O21 2.557(11) 2_675 ? 
Sr1 O1 2.559(6) 2_575 ? 
Sr1 O4 2.576(6) 2_565 ? 
Sr1 B7 3.012(9) 2_565 ? 
Sr2 O17 2.798(5) 1_655 ? 
Sr2 O12 2.802(5) 2_666 ? 
Sr2 O10 2.837(5) 1_655 ? 
Sr2 B5 2.978(8) 1_655 ? 
Sr3 O20 2.431(11) 1_556 ? 
Sr3 O29 2.77(2) 1_556 ? 
Sr3 O7 2.781(5) 2_576 ? 
Sr3 O17 2.783(5) 1_655 ? 
Sr3 O5 2.806(5) 1_455 ? 
Sr3 B2 2.967(8) 1_455 ? 
V4 O22 1.912(10) 2_665 ? 
V4 Sr1 3.8679(19) 2_665 ? 
V5 O21 1.872(11) 2_675 ? 
V5 Sr1 3.815(2) 2_675 ? 
V5 Sr3 3.9166(19) 1_554 ? 
 
loop_ 
 _geom_angle_atom_site_label_1 
 _geom_angle_atom_site_label_2 
 _geom_angle_atom_site_label_3 
 _geom_angle 
 _geom_angle_site_symmetry_1 
 _geom_angle_site_symmetry_3 
 _geom_angle_publ_flag 
O7 B1 O3 111.3(6) . . ? 
O7 B1 O9 107.8(6) . 2_576 ? 
O3 B1 O9 109.2(6) . 2_576 ? 
O7 B1 O6 111.3(6) . . ? 
O3 B1 O6 108.4(6) . . ? 
O9 B1 O6 108.8(5) 2_576 . ? 
O7 B1 Sr3 60.8(3) . 2_576 ? 
O3 B1 Sr3 106.1(5) . 2_576 ? 
O9 B1 Sr3 51.8(3) 2_576 2_576 ? 
O6 B1 Sr3 144.7(5) . 2_576 ? 
O18 B2 O7 114.6(6) 2_665 1_655 ? 
O18 B2 O5 110.6(6) 2_665 . ? 
O7 B2 O5 109.2(6) 1_655 . ? 
O18 B2 O14 109.7(6) 2_665 1_655 ? 
O7 B2 O14 107.2(6) 1_655 1_655 ? 
O5 B2 O14 105.0(5) . 1_655 ? 
O18 B2 Sr3 174.1(5) 2_665 1_655 ? 
O7 B2 Sr3 70.5(4) 1_655 1_655 ? 
O5 B2 Sr3 69.1(4) . 1_655 ? 
O14 B2 Sr3 65.2(3) 1_655 1_655 ? 
O12 B3 O11 125.4(7) . . ? 
O12 B3 O15 114.9(6) . 2_666 ? 
O11 B3 O15 119.5(6) . 2_666 ? 
O12 B3 Sr2 62.9(4) . 2_666 ? 
O11 B3 Sr2 171.0(5) . 2_666 ? 
O15 B3 Sr2 52.0(3) 2_666 2_666 ? 
O10 B4 O11 106.8(6) . . ? 
O10 B4 O16 112.1(6) . 1_556 ? 
O11 B4 O16 108.4(5) . 1_556 ? 
O10 B4 O13 112.5(5) . 2_566 ? 
O11 B4 O13 109.1(5) . 2_566 ? 
O16 B4 O13 107.8(6) 1_556 2_566 ? 
O10 B4 Sr3 57.9(3) . . ? 
O11 B4 Sr3 51.8(3) . . ? 
O16 B4 Sr3 110.1(4) 1_556 . ? 
O13 B4 Sr3 141.5(5) 2_566 . ? 
O2 B5 O10 112.0(6) 1_556 . ? 
O2 B5 O17 109.0(6) 1_556 . ? 
O10 B5 O17 110.1(6) . . ? 
O2 B5 O12 111.9(6) 1_556 1_455 ? 
O10 B5 O12 106.2(5) . 1_455 ? 
O17 B5 O12 107.6(6) . 1_455 ? 
O2 B5 Sr2 177.3(5) 1_556 1_455 ? 
O10 B5 Sr2 70.2(4) . 1_455 ? 
O17 B5 Sr2 68.5(3) . 1_455 ? 
O12 B5 Sr2 68.5(3) 1_455 1_455 ? 
O17 B6 O9 125.9(7) . . ? 
O17 B6 O8 114.5(6) . 1_455 ? 
O9 B6 O8 119.4(6) . 1_455 ? 
O17 B6 Sr3 61.7(3) . 1_455 ? 
O9 B6 Sr3 172.0(5) . 1_455 ? 
O8 B6 Sr3 53.4(3) 1_455 1_455 ? 
O18 B7 O3 123.0(8) . 2_565 ? 
O18 B7 O4 120.5(7) . . ? 
O3 B7 O4 116.4(7) 2_565 . ? 
O18 B7 Sr1 176.3(6) . 2_565 ? 
O3 B7 Sr1 58.2(4) 2_565 2_565 ? 
O4 B7 Sr1 58.5(4) . 2_565 ? 
O14 B8 O13 117.7(6) . . ? 
O14 B8 O15 123.1(7) . 1_455 ? 
O13 B8 O15 119.2(7) . 1_455 ? 
O14 B8 Sr2 65.7(4) . . ? 
O13 B8 Sr2 52.2(3) . . ? 
O15 B8 Sr2 171.1(5) 1_455 . ? 
O6 B9 O5 116.8(7) 2_676 2_676 ? 
O6 B9 O8 120.4(7) 2_676 . ? 
O5 B9 O8 122.4(6) 2_676 . ? 
O6 B9 Sr2 55.7(4) 2_676 2_676 ? 
O5 B9 Sr2 61.2(4) 2_676 2_676 ? 
O8 B9 Sr2 171.6(5) . 2_676 ? 
O2 B10 O1 121.2(7) . 2_575 ? 
O2 B10 O16 123.2(7) . . ? 
O1 B10 O16 115.6(7) 2_575 . ? 
O2 B10 Sr1 178.4(6) . . ? 
O1 B10 Sr1 57.2(4) 2_575 . ? 
O16 B10 Sr1 58.3(4) . . ? 
B10 O1 V5 125.2(5) 2_575 . ? 
B10 O1 Sr1 96.0(5) 2_575 2_575 ? 
V5 O1 Sr1 137.7(3) . 2_575 ? 
B10 O2 B5 118.7(6) . 1_554 ? 
B7 O3 B1 119.7(6) 2_565 . ? 
B7 O3 Sr1 95.1(5) 2_565 . ? 
B1 O3 Sr1 144.2(4) . . ? 
B7 O4 V4 130.7(5) . . ? 
B7 O4 Sr1 94.4(5) . 2_565 ? 
V4 O4 Sr1 133.3(3) . 2_565 ? 
B9 O5 B2 125.6(6) 2_676 . ? 
B9 O5 Sr2 92.4(4) 2_676 . ? 
B2 O5 Sr2 129.1(4) . . ? 
B9 O5 Sr3 120.3(4) 2_676 1_655 ? 
B2 O5 Sr3 81.1(4) . 1_655 ? 
Sr2 O5 Sr3 109.87(17) . 1_655 ? 
B9 O6 B1 123.3(6) 2_676 . ? 
B9 O6 Sr2 98.9(4) 2_676 . ? 
B1 O6 Sr2 137.5(4) . . ? 
B1 O7 B2 116.3(5) . 1_455 ? 
B1 O7 Sr3 92.3(4) . 2_576 ? 
B2 O7 Sr3 132.7(4) 1_455 2_576 ? 
B1 O7 Sr3 135.1(4) . . ? 
B2 O7 Sr3 80.7(4) 1_455 . ? 
Sr3 O7 Sr3 105.62(15) 2_576 . ? 
B9 O8 B6 120.2(6) . 1_655 ? 
B9 O8 Sr3 138.8(4) . . ? 
B6 O8 Sr3 100.8(4) 1_655 . ? 
B6 O9 B1 123.6(6) . 2_576 ? 
B6 O9 Sr3 133.1(4) . . ? 
B1 O9 Sr3 101.2(4) 2_576 . ? 
B4 O10 B5 117.0(6) . . ? 
B4 O10 Sr3 95.8(4) . . ? 
B5 O10 Sr3 127.9(4) . . ? 
B4 O10 Sr2 131.4(4) . 1_455 ? 
B5 O10 Sr2 81.0(4) . 1_455 ? 
Sr3 O10 Sr2 107.51(16) . 1_455 ? 
B3 O11 B4 121.8(6) . . ? 
B3 O11 Sr3 135.2(4) . . ? 
B4 O11 Sr3 101.5(4) . . ? 
B3 O12 B5 126.9(6) . 1_655 ? 
B3 O12 Sr2 118.6(4) . . ? 
B5 O12 Sr2 81.6(4) 1_655 . ? 
B3 O12 Sr2 91.7(4) . 2_666 ? 
B5 O12 Sr2 133.1(4) 1_655 2_666 ? 
Sr2 O12 Sr2 103.97(16) . 2_666 ? 
B8 O13 B4 121.1(6) . 2_566 ? 
B8 O13 Sr2 102.7(4) . . ? 
B4 O13 Sr2 131.8(4) 2_566 . ? 
B8 O14 B2 125.9(6) . 1_455 ? 
B8 O14 Sr3 123.0(4) . . ? 
B2 O14 Sr3 84.4(4) 1_455 . ? 
B8 O14 Sr2 88.6(4) . . ? 
B2 O14 Sr2 128.8(4) 1_455 . ? 
Sr3 O14 Sr2 109.03(16) . . ? 
B8 O15 B3 120.6(6) 1_655 2_666 ? 
B8 O15 Sr2 134.2(5) 1_655 . ? 
B3 O15 Sr2 102.3(4) 2_666 . ? 
B10 O16 B4 119.8(6) . 1_554 ? 
B10 O16 Sr1 94.6(5) . . ? 
B4 O16 Sr1 144.1(4) 1_554 . ? 
B6 O17 B5 123.0(6) . . ? 
B6 O17 Sr3 93.1(4) . 1_455 ? 
B5 O17 Sr3 130.1(4) . 1_455 ? 
B6 O17 Sr2 122.7(4) . 1_455 ? 
B5 O17 Sr2 82.0(4) . 1_455 ? 
Sr3 O17 Sr2 108.03(16) 1_455 1_455 ? 
B7 O18 B2 120.1(6) . 2_665 ? 
O29 O20 O30 118.7(14) . . ? 
O29 O20 V5 62.6(10) . . ? 
O30 O20 V5 59.1(8) . . ? 
O29 O20 Sr3 89.1(10) . 1_554 ? 
O30 O20 Sr3 139.4(10) . 1_554 ? 
V5 O20 Sr3 149.7(6) . 1_554 ? 
O30 O21 O24 138.8(13) 2_675 . ? 
O30 O21 V5 55.8(9) 2_675 2_675 ? 
O24 O21 V5 163.6(9) . 2_675 ? 
O30 O21 V5 160.1(11) 2_675 . ? 
O24 O21 V5 51.5(5) . . ? 
V5 O21 V5 118.1(6) 2_675 . ? 
O30 O21 Sr1 72.3(10) 2_675 2_675 ? 
O24 O21 Sr1 67.4(6) . 2_675 ? 
V5 O21 Sr1 123.9(5) 2_675 2_675 ? 
V5 O21 Sr1 118.0(5) . 2_675 ? 
O28 O22 O26 139.4(11) . 2_665 ? 
O28 O22 V4 56.6(8) . . ? 
O26 O22 V4 160.3(8) 2_665 . ? 
O28 O22 V4 162.7(11) . 2_665 ? 
O26 O22 V4 50.3(5) 2_665 2_665 ? 
V4 O22 V4 118.4(6) . 2_665 ? 
O28 O22 Sr1 72.1(8) . . ? 
O26 O22 Sr1 68.0(6) 2_665 . ? 
V4 O22 Sr1 123.2(5) . . ? 
V4 O22 Sr1 117.7(5) 2_665 . ? 
O27 O23 O28 114.9(11) . . ? 
O27 O23 V4 62.7(7) . . ? 
O28 O23 V4 56.0(7) . . ? 
O27 O23 Sr2 83.5(8) . . ? 
O28 O23 Sr2 138.1(8) . . ? 
V4 O23 Sr2 141.7(7) . . ? 
V5 O24 O29 60.8(9) . . ? 
V5 O24 O21 72.5(7) . . ? 
O29 O24 O21 122.3(12) . . ? 
V5 O24 Sr1 145.2(9) . 2_675 ? 
O29 O24 Sr1 151.7(11) . 2_675 ? 
O21 O24 Sr1 74.6(6) . 2_675 ? 
O27 O26 V4 63.5(8) . . ? 
O27 O26 O22 124.9(10) . 2_665 ? 
V4 O26 O22 71.0(7) . 2_665 ? 
O27 O26 Sr1 151.0(10) . 2_665 ? 
V4 O26 Sr1 142.4(8) . 2_665 ? 
O22 O26 Sr1 72.5(6) 2_665 2_665 ? 
O23 O27 O26 124.1(12) . . ? 
O23 O27 V4 66.3(8) . . ? 
O26 O27 V4 59.4(7) . . ? 
O23 O27 Sr2 65.0(7) . . ? 
O26 O27 Sr2 150.2(9) . . ? 
V4 O27 Sr2 128.2(8) . . ? 
O22 O28 V4 76.1(8) . . ? 
O22 O28 O23 131.6(13) . . ? 
V4 O28 O23 62.5(7) . . ? 
O22 O28 Sr1 76.9(9) . . ? 
V4 O28 Sr1 142.9(9) . . ? 
O23 O28 Sr1 151.1(9) . . ? 
O20 O29 O24 123.1(16) . . ? 
O20 O29 V5 66.4(10) . . ? 
O24 O29 V5 58.9(9) . . ? 
O20 O29 Sr3 61.2(9) . 1_554 ? 
O24 O29 Sr3 155.6(12) . 1_554 ? 
V5 O29 Sr3 126.5(11) . 1_554 ? 
O21 O30 V5 76.7(11) 2_675 . ? 
O21 O30 O20 130.3(16) 2_675 . ? 
V5 O30 O20 61.0(9) . . ? 
O21 O30 Sr1 75.2(10) 2_675 . ? 
V5 O30 Sr1 144.4(12) . . ? 
O20 O30 Sr1 153.2(12) . . ? 
O24 Sr1 O26 62.2(5) 2_675 2_665 ? 
O24 Sr1 O30 70.3(6) 2_675 . ? 
O26 Sr1 O30 93.6(6) 2_665 . ? 
O24 Sr1 O28 91.3(5) 2_675 . ? 
O26 Sr1 O28 70.4(5) 2_665 . ? 
O30 Sr1 O28 160.1(6) . . ? 
O24 Sr1 O21 38.0(4) 2_675 2_675 ? 
O26 Sr1 O21 79.7(4) 2_665 2_675 ? 
O30 Sr1 O21 32.5(5) . 2_675 ? 
O28 Sr1 O21 129.3(4) . 2_675 ? 
O24 Sr1 O1 123.1(4) 2_675 2_575 ? 
O26 Sr1 O1 150.9(4) 2_665 2_575 ? 
O30 Sr1 O1 65.9(5) . 2_575 ? 
O28 Sr1 O1 133.2(4) . 2_575 ? 
O21 Sr1 O1 90.9(3) 2_675 2_575 ? 
O24 Sr1 O3 96.0(4) 2_675 . ? 
O26 Sr1 O3 128.1(4) 2_665 . ? 
O30 Sr1 O3 124.4(5) . . ? 
O28 Sr1 O3 63.3(4) . . ? 
O21 Sr1 O3 112.6(3) 2_675 . ? 
O1 Sr1 O3 80.98(19) 2_575 . ? 
O24 Sr1 O4 147.4(4) 2_675 2_565 ? 
O26 Sr1 O4 123.8(3) 2_665 2_565 ? 
O30 Sr1 O4 134.3(5) . 2_565 ? 
O28 Sr1 O4 65.6(4) . 2_565 ? 
O21 Sr1 O4 156.5(3) 2_675 2_565 ? 
O1 Sr1 O4 69.2(2) 2_575 2_565 ? 
O3 Sr1 O4 53.72(17) . 2_565 ? 
O24 Sr1 O16 125.8(4) 2_675 . ? 
O26 Sr1 O16 98.6(4) 2_665 . ? 
O30 Sr1 O16 60.5(5) . . ? 
O28 Sr1 O16 131.8(4) . . ? 
O21 Sr1 O16 91.7(3) 2_675 . ? 
O1 Sr1 O16 53.88(17) 2_575 . ? 
O3 Sr1 O16 129.45(17) . . ? 
O4 Sr1 O16 86.48(19) 2_565 . ? 
O24 Sr1 O22 78.4(4) 2_675 . ? 
O26 Sr1 O22 39.5(4) 2_665 . ? 
O30 Sr1 O22 132.6(5) . . ? 
O28 Sr1 O22 31.0(4) . . ? 
O21 Sr1 O22 110.9(3) 2_675 . ? 
O1 Sr1 O22 158.0(3) 2_575 . ? 
O3 Sr1 O22 92.9(3) . . ? 
O4 Sr1 O22 90.1(3) 2_565 . ? 
O16 Sr1 O22 119.8(3) . . ? 
O24 Sr1 B7 121.5(4) 2_675 2_565 ? 
O26 Sr1 B7 129.6(4) 2_665 2_565 ? 
O30 Sr1 B7 136.5(5) . 2_565 ? 
O28 Sr1 B7 59.6(4) . 2_565 ? 
O21 Sr1 B7 137.4(3) 2_675 2_565 ? 
O1 Sr1 B7 74.8(2) 2_575 2_565 ? 
O3 Sr1 B7 26.7(2) . 2_565 ? 
O4 Sr1 B7 27.1(2) 2_565 2_565 ? 
O16 Sr1 B7 109.8(2) . 2_565 ? 
O22 Sr1 B7 90.2(3) . 2_565 ? 
O24 Sr1 B10 129.6(4) 2_675 . ? 
O26 Sr1 B10 125.2(4) 2_665 . ? 
O30 Sr1 B10 59.9(5) . . ? 
O28 Sr1 B10 139.1(4) . . ? 
O21 Sr1 B10 91.7(3) 2_675 . ? 
O1 Sr1 B10 26.78(19) 2_575 . ? 
O3 Sr1 B10 105.3(2) . . ? 
O4 Sr1 B10 76.2(2) 2_565 . ? 
O16 Sr1 B10 27.11(19) . . ? 
O22 Sr1 B10 143.0(3) . . ? 
B7 Sr1 B10 92.2(2) 2_565 . ? 
O23 Sr2 O13 81.8(3) . . ? 
O23 Sr2 O15 91.2(3) . . ? 
O13 Sr2 O15 118.86(16) . . ? 
O23 Sr2 O6 71.5(3) . . ? 
O13 Sr2 O6 115.99(16) . . ? 
O15 Sr2 O6 118.76(16) . . ? 
O23 Sr2 O27 31.5(4) . . ? 
O13 Sr2 O27 81.6(3) . . ? 
O15 Sr2 O27 64.8(3) . . ? 
O6 Sr2 O27 99.6(3) . . ? 
O23 Sr2 O5 89.0(3) . . ? 
O13 Sr2 O5 166.98(16) . . ? 
O15 Sr2 O5 70.34(15) . . ? 
O6 Sr2 O5 51.79(15) . . ? 
O27 Sr2 O5 95.5(3) . . ? 
O23 Sr2 O17 138.6(3) . 1_655 ? 
O13 Sr2 O17 99.95(15) . 1_655 ? 
O15 Sr2 O17 121.85(15) . 1_655 ? 
O6 Sr2 O17 70.68(16) . 1_655 ? 
O27 Sr2 O17 169.9(3) . 1_655 ? 
O5 Sr2 O17 80.80(14) . 1_655 ? 
O23 Sr2 O12 152.1(3) . . ? 
O13 Sr2 O12 70.21(16) . . ? 
O15 Sr2 O12 102.10(15) . . ? 
O6 Sr2 O12 120.51(15) . . ? 
O27 Sr2 O12 137.8(3) . . ? 
O5 Sr2 O12 118.51(14) . . ? 
O17 Sr2 O12 50.84(14) 1_655 . ? 
O23 Sr2 O12 94.4(3) . 2_666 ? 
O13 Sr2 O12 68.95(15) . 2_666 ? 
O15 Sr2 O12 51.04(14) . 2_666 ? 
O6 Sr2 O12 163.40(16) . 2_666 ? 
O27 Sr2 O12 64.7(3) . 2_666 ? 
O5 Sr2 O12 121.30(14) . 2_666 ? 
O17 Sr2 O12 125.22(15) 1_655 2_666 ? 
O12 Sr2 O12 76.03(16) . 2_666 ? 
O23 Sr2 O10 157.7(3) . 1_655 ? 
O13 Sr2 O10 119.13(16) . 1_655 ? 
O15 Sr2 O10 72.40(15) . 1_655 ? 
O6 Sr2 O10 102.66(15) . 1_655 ? 
O27 Sr2 O10 137.1(3) . 1_655 ? 
O5 Sr2 O10 71.43(14) . 1_655 ? 
O17 Sr2 O10 50.56(13) 1_655 1_655 ? 
O12 Sr2 O10 49.57(13) . 1_655 ? 
O12 Sr2 O10 87.05(14) 2_666 1_655 ? 
O23 Sr2 O14 80.0(3) . . ? 
O13 Sr2 O14 50.79(15) . . ? 
O15 Sr2 O14 167.05(15) . . ? 
O6 Sr2 O14 67.55(15) . . ? 
O27 Sr2 O14 103.8(3) . . ? 
O5 Sr2 O14 118.55(14) . . ? 
O17 Sr2 O14 70.37(14) 1_655 . ? 
O12 Sr2 O14 82.24(14) . . ? 
O12 Sr2 O14 119.73(14) 2_666 . ? 
O10 Sr2 O14 118.49(14) 1_655 . ? 
O23 Sr2 B5 167.9(3) . 1_655 ? 
O13 Sr2 B5 97.6(2) . 1_655 ? 
O15 Sr2 B5 99.57(19) . 1_655 ? 
O6 Sr2 B5 98.20(19) . 1_655 ? 
O27 Sr2 B5 160.5(4) . 1_655 ? 
O5 Sr2 B5 89.40(18) . 1_655 ? 
O17 Sr2 B5 29.48(18) 1_655 1_655 ? 
O12 Sr2 B5 29.87(17) . 1_655 ? 
O12 Sr2 B5 96.71(19) 2_666 1_655 ? 
O10 Sr2 B5 28.87(17) 1_655 1_655 ? 
O14 Sr2 B5 90.23(18) . 1_655 ? 
O20 Sr3 O9 79.6(3) 1_556 . ? 
O20 Sr3 O8 87.8(3) 1_556 . ? 
O9 Sr3 O8 117.29(16) . . ? 
O20 Sr3 O11 71.9(3) 1_556 . ? 
O9 Sr3 O11 116.64(15) . . ? 
O8 Sr3 O11 116.79(16) . . ? 
O20 Sr3 O14 143.6(3) 1_556 . ? 
O9 Sr3 O14 124.26(15) . . ? 
O8 Sr3 O14 101.21(16) . . ? 
O11 Sr3 O14 72.52(16) . . ? 
O20 Sr3 O10 82.4(3) 1_556 . ? 
O9 Sr3 O10 69.31(15) . . ? 
O8 Sr3 O10 167.08(16) . . ? 
O11 Sr3 O10 51.96(14) . . ? 
O14 Sr3 O10 82.05(14) . . ? 
O20 Sr3 O29 29.7(5) 1_556 1_556 ? 
O9 Sr3 O29 84.7(4) . 1_556 ? 
O8 Sr3 O29 60.3(4) . 1_556 ? 
O11 Sr3 O29 95.2(5) . 1_556 ? 
O14 Sr3 O29 151.0(4) . 1_556 ? 
O10 Sr3 O29 111.4(4) . 1_556 ? 
O20 Sr3 O7 92.5(3) 1_556 2_576 ? 
O9 Sr3 O7 52.24(14) . 2_576 ? 
O8 Sr3 O7 67.54(15) . 2_576 ? 
O11 Sr3 O7 163.19(15) . 2_576 ? 
O14 Sr3 O7 123.64(15) . 2_576 ? 
O10 Sr3 O7 121.16(14) . 2_576 ? 
O29 Sr3 O7 72.4(4) 1_556 2_576 ? 
O20 Sr3 O17 87.2(3) 1_556 1_655 ? 
O9 Sr3 O17 162.97(15) . 1_655 ? 
O8 Sr3 O17 50.90(15) . 1_655 ? 
O11 Sr3 O17 68.39(14) . 1_655 ? 
O14 Sr3 O17 72.56(14) . 1_655 ? 
O10 Sr3 O17 119.79(14) . 1_655 ? 
O29 Sr3 O17 78.5(4) 1_556 1_655 ? 
O7 Sr3 O17 118.41(14) 2_576 1_655 ? 
O20 Sr3 O5 147.9(3) 1_556 1_455 ? 
O9 Sr3 O5 74.29(15) . 1_455 ? 
O8 Sr3 O5 120.64(16) . 1_455 ? 
O11 Sr3 O5 103.54(15) . 1_455 ? 
O14 Sr3 O5 51.11(14) . 1_455 ? 
O10 Sr3 O5 71.17(14) . 1_455 ? 
O29 Sr3 O5 156.5(4) 1_556 1_455 ? 
O7 Sr3 O5 86.13(14) 2_576 1_455 ? 
O17 Sr3 O5 121.49(14) 1_655 1_455 ? 
O20 Sr3 O7 158.2(3) 1_556 . ? 
O9 Sr3 O7 104.36(15) . . ? 
O8 Sr3 O7 71.21(16) . . ? 
O11 Sr3 O7 122.37(15) . . ? 
O14 Sr3 O7 50.79(14) . . ? 
O10 Sr3 O7 119.18(14) . . ? 
O29 Sr3 O7 128.6(4) 1_556 . ? 
O7 Sr3 O7 74.38(15) 2_576 . ? 
O17 Sr3 O7 84.12(14) 1_655 . ? 
O5 Sr3 O7 50.29(13) 1_455 . ? 
O20 Sr3 B2 172.5(3) 1_556 1_455 ? 
O9 Sr3 B2 101.89(19) . 1_455 ? 
O8 Sr3 B2 97.90(19) . 1_455 ? 
O11 Sr3 B2 100.96(19) . 1_455 ? 
O14 Sr3 B2 30.37(18) . 1_455 ? 
O10 Sr3 B2 91.16(17) . 1_455 ? 
O29 Sr3 B2 157.3(5) 1_556 1_455 ? 
O7 Sr3 B2 94.22(18) 2_576 1_455 ? 
O17 Sr3 B2 92.62(18) 1_655 1_455 ? 
O5 Sr3 B2 29.79(17) 1_455 1_455 ? 
O7 Sr3 B2 28.79(17) . 1_455 ? 
O26 V4 O28 145.6(8) . . ? 
O26 V4 O27 57.1(8) . . ? 
O28 V4 O27 109.1(8) . . ? 
O26 V4 O23 107.0(7) . . ? 
O28 V4 O23 61.5(7) . . ? 
O27 V4 O23 51.0(7) . . ? 
O26 V4 O22 117.4(6) . . ? 
O28 V4 O22 47.2(6) . . ? 
O27 V4 O22 135.6(6) . . ? 
O23 V4 O22 104.8(6) . . ? 
O26 V4 O4 109.3(6) . . ? 
O28 V4 O4 105.1(6) . . ? 
O27 V4 O4 111.8(5) . . ? 
O23 V4 O4 106.7(5) . . ? 
O22 V4 O4 110.9(4) . . ? 
O26 V4 O22 58.6(6) . 2_665 ? 
O28 V4 O22 106.7(6) . 2_665 ? 
O27 V4 O22 109.0(6) . 2_665 ? 
O23 V4 O22 138.3(5) . 2_665 ? 
O22 V4 O22 61.6(6) . 2_665 ? 
O4 V4 O22 114.9(4) . 2_665 ? 
O26 V4 Sr1 23.4(5) . 2_665 ? 
O28 V4 Sr1 138.5(6) . 2_665 ? 
O27 V4 Sr1 79.6(6) . 2_665 ? 
O23 V4 Sr1 127.0(4) . 2_665 ? 
O22 V4 Sr1 97.5(4) . 2_665 ? 
O4 V4 Sr1 108.9(2) . 2_665 ? 
O22 V4 Sr1 36.4(3) 2_665 2_665 ? 
O26 V4 Sr1 150.6(5) . . ? 
O28 V4 Sr1 23.1(6) . . ? 
O27 V4 Sr1 132.2(5) . . ? 
O23 V4 Sr1 83.6(4) . . ? 
O22 V4 Sr1 33.9(3) . . ? 
O4 V4 Sr1 93.0(2) . . ? 
O22 V4 Sr1 95.0(3) 2_665 . ? 
Sr1 V4 Sr1 131.28(4) 2_665 . ? 
O26 V4 Sr2 85.1(6) . . ? 
O28 V4 Sr2 76.3(6) . . ? 
O27 V4 Sr2 32.8(5) . . ? 
O23 V4 Sr2 22.9(4) . . ? 
O22 V4 Sr2 110.3(4) . . ? 
O4 V4 Sr2 121.97(19) . . ? 
O22 V4 Sr2 120.0(3) 2_665 . ? 
Sr1 V4 Sr2 104.14(4) 2_665 . ? 
Sr1 V4 Sr2 99.45(4) . . ? 
O24 V5 O29 60.2(9) . . ? 
O24 V5 O30 146.4(9) . . ? 
O29 V5 O30 108.3(11) . . ? 
O24 V5 O20 109.5(7) . . ? 
O29 V5 O20 51.0(8) . . ? 
O30 V5 O20 59.9(9) . . ? 
O24 V5 O1 109.5(6) . . ? 
O29 V5 O1 110.5(8) . . ? 
O30 V5 O1 104.0(8) . . ? 
O20 V5 O1 106.5(4) . . ? 
O24 V5 O21 116.3(6) . 2_675 ? 
O29 V5 O21 136.1(8) . 2_675 ? 
O30 V5 O21 47.6(8) . 2_675 ? 
O20 V5 O21 103.3(5) . 2_675 ? 
O1 V5 O21 111.0(4) . 2_675 ? 
O24 V5 O21 56.0(7) . . ? 
O29 V5 O21 108.2(8) . . ? 
O30 V5 O21 106.6(8) . . ? 
O20 V5 O21 134.8(5) . . ? 
O1 V5 O21 118.6(4) . . ? 
O21 V5 O21 61.9(6) 2_675 . ? 
O24 V5 Sr1 21.5(6) . 2_675 ? 
O29 V5 Sr1 81.0(7) . 2_675 ? 
O30 V5 Sr1 139.7(7) . 2_675 ? 
O20 V5 Sr1 127.8(4) . 2_675 ? 
O1 V5 Sr1 109.0(2) . 2_675 ? 
O21 V5 Sr1 98.2(3) 2_675 2_675 ? 
O21 V5 Sr1 36.3(3) . 2_675 ? 
O24 V5 Sr3 91.4(6) . 1_554 ? 
O29 V5 Sr3 34.7(7) . 1_554 ? 
O30 V5 Sr3 73.8(8) . 1_554 ? 
O20 V5 Sr3 18.2(4) . 1_554 ? 
O1 V5 Sr3 116.59(19) . 1_554 ? 
O21 V5 Sr3 110.8(3) 2_675 1_554 ? 
O21 V5 Sr3 122.4(3) . 1_554 ? 
Sr1 V5 Sr3 109.60(4) 2_675 1_554 ? 
O24 V5 Sr1 148.2(6) . . ? 
O29 V5 Sr1 130.2(7) . . ? 
O30 V5 Sr1 22.0(8) . . ? 
O20 V5 Sr1 81.4(4) . . ? 
O1 V5 Sr1 94.8(3) . . ? 
O21 V5 Sr1 32.8(3) 2_675 . ? 
O21 V5 Sr1 94.7(3) . . ? 
Sr1 V5 Sr1 130.93(4) 2_675 . ? 
Sr3 V5 Sr1 95.75(4) 1_554 . ? 
 
_diffrn_measured_fraction_theta_max    0.964 
_diffrn_reflns_theta_full              27.68 
_diffrn_measured_fraction_theta_full   0.964 
_refine_diff_density_max    2.915 
_refine_diff_density_min   -2.101 
_refine_diff_density_rms    0.247 
