# Electronic Supplementary Material (ESI) for RSC Advances.
# This journal is © The Royal Society of Chemistry 2016

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_MA_publ
_database_code_depnum_ccdc_archive 'CCDC 1479625'
_audit_update_record             
;
2016-05-13 deposited with the CCDC.
2016-05-17 downloaded from the CCDC.
;

_pd_block_id                     2015-08-04T11:23|MA|ma|bruker

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2015-08-04T11:23

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.00
_refine_ls_shift/su_mean         0.00
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     41
_refine_ls_goodness_of_fit_all   2.91
_refine_ls_number_restraints     186
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    293

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from C:/Users/SOUMEN/Desktop/sdas/expo with prev result/rietveld/M'
_cell_length_a                   15.748(12)
_cell_length_b                   12.735(9)
_cell_length_c                   7.2909(17)
_cell_angle_alpha                90.0
_cell_angle_beta                 106.47(8)
_cell_angle_gamma                90.0
_cell_volume                     1402.2(9)
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21 1'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x,+y+1/2,-z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
C C1 0.0821 1.0623 0.5417 1.0 Uiso 0.04 2
C C2 0.0102 0.9938 0.4982 1.0 Uiso 0.04 2
C C3 0.0237 0.8852 0.4967 1.0 Uiso 0.04 2
C C4 0.1085 0.8442 0.5382 1.0 Uiso 0.04 2
C C5 0.181 0.913 0.5807 1.0 Uiso 0.04 2
C C6 0.1667 1.0228 0.5821 1.0 Uiso 0.04 2
C C7 0.1208 0.7279 0.5377 1.0 Uiso 0.04 2
C C8 0.2115 0.6888 0.5764 1.0 Uiso 0.04 2
C C9 0.2844 0.7599 0.6138 1.0 Uiso 0.04 2
C C10 0.2685 0.8704 0.623 1.0 Uiso 0.04 2
C C11 0.2264 0.5801 0.5755 1.0 Uiso 0.04 2
C C12 0.3111 0.5357 0.6096 1.0 Uiso 0.04 2
C C13 0.3808 0.6044 0.6421 1.0 Uiso 0.04 2
C C14 0.3685 0.7165 0.6414 1.0 Uiso 0.04 2
O O15 0.3312 0.9425 0.6755 1.0 Uiso 0.04 2
O O16 0.4438 0.7692 0.6605 1.0 Uiso 0.04 2
Mn Mn1 0.4505 0.91 0.7377 1.0 Uiso 0.04 2
O O18 0.4566 1.0514 0.8127 1.0 Uiso 0.04 2
O O19 0.5701 0.8782 0.7987 1.0 Uiso 0.04 2
C C20 0.6317 0.952 0.8454 1.0 Uiso 0.04 2
C C21 0.7199 0.9113 0.8956 1.0 Uiso 0.04 2
C C22 0.7909 0.9816 0.9191 1.0 Uiso 0.04 2
C C23 0.7764 1.0973 0.8951 1.0 Uiso 0.04 2
C C24 0.6854 1.1349 0.8589 1.0 Uiso 0.04 2
C C25 0.6141 1.0627 0.8395 1.0 Uiso 0.04 2
C C26 0.6686 1.2433 0.8438 1.0 Uiso 0.04 2
C C27 0.5834 1.2863 0.8103 1.0 Uiso 0.04 2
C C28 0.5154 1.2166 0.7956 1.0 Uiso 0.04 2
C C29 0.5297 1.105 0.8137 1.0 Uiso 0.04 2
C C30 0.7366 0.8021 0.9196 1.0 Uiso 0.04 2
C C31 0.822 0.7648 0.9637 1.0 Uiso 0.04 2
C C32 0.8922 0.8348 0.9861 1.0 Uiso 0.04 2
C C33 0.8765 0.9428 0.9642 1.0 Uiso 0.04 2
O O34 0.0582 0.6691 0.5065 1.0 Uiso 0.04 2
O O35 0.1549 0.5169 0.5402 1.0 Uiso 0.04 2
O O36 0.4628 0.5644 0.6742 1.0 Uiso 0.04 2
O O37 0.4329 1.2553 0.7644 1.0 Uiso 0.04 2
O O38 0.7386 1.3076 0.8624 1.0 Uiso 0.04 2
O O39 0.8374 1.1567 0.9059 1.0 Uiso 0.04 2
O O40 0.4027 0.9399 1.0133 1.0 Uiso 0.04 2
O O41 0.4978 0.8824 0.4604 1.0 Uiso 0.04 2
H H42 0.07296 1.13439 0.54342 1.0 Uiso 0.06 2
H H43 -0.04707 1.02035 0.47001 1.0 Uiso 0.06 2
H H44 -0.02475 0.84013 0.46755 1.0 Uiso 0.06 2
H H45 0.21478 1.06842 0.61049 1.0 Uiso 0.06 2
H H46 0.31947 0.4634 0.6101 1.0 Uiso 0.06 2
H H47 0.57362 1.35833 0.79869 1.0 Uiso 0.06 2
H H48 0.6897 0.75552 0.9055 1.0 Uiso 0.06 2
H H49 0.83284 0.69307 0.97852 1.0 Uiso 0.06 2
H H50 0.94991 0.80953 1.01583 1.0 Uiso 0.06 2
H H51 0.92386 0.98887 0.98003 1.0 Uiso 0.06 2
H H52 0.10396 0.5386 0.51784 1.0 Uiso 0.06 2
H H53 0.46759 0.50041 0.66947 1.0 Uiso 0.06 2
H H54 0.42059 1.31698 0.77667 1.0 Uiso 0.06 2
H H55 0.78508 1.28933 0.84225 1.0 Uiso 0.06 2
H H56 0.36364 0.8918 1.02817 1.0 Uiso 0.06 2
H H57 0.4196 0.97018 1.10217 1.0 Uiso 0.06 2
H H58 0.54549 0.9201 0.44518 1.0 Uiso 0.06 2
H H59 0.4721 0.86326 0.37199 1.0 Uiso 0.06 2

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C28 H18 Mn O12'
_chemical_formula_weight         601.38
_cell_formula_units_Z            2

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.3929(8) . 1_555 N
C1 C6 1.3756(10) . 1_555 N
C1 H42 0.9299(6) . 1_555 N
C2 C1 1.3929(8) . 1_555 N
C2 C3 1.3998(9) . 1_555 N
C2 H43 0.9300(7) . 1_555 N
C3 C2 1.3998(9) . 1_555 N
C3 C4 1.3851(10) . 1_555 N
C3 H44 0.9300(6) . 1_555 N
C4 C3 1.3851(10) . 1_555 N
C4 C5 1.4024(8) . 1_555 N
C4 C7 1.4939(10) . 1_555 N
C5 C4 1.4024(8) . 1_555 N
C5 C6 1.4168(9) . 1_555 N
C5 C10 1.4308(11) . 1_555 N
C6 C1 1.3756(10) . 1_555 N
C6 C5 1.4168(9) . 1_555 N
C6 H45 0.9300(5) . 1_555 N
C7 C4 1.4939(10) . 1_555 N
C7 C8 1.4626(11) . 1_555 N
C7 O34 1.2071(7) . 1_555 N
C8 C7 1.4626(11) . 1_555 N
C8 C9 1.4264(8) . 1_555 N
C8 C11 1.4044(9) . 1_555 N
C9 C8 1.4264(8) . 1_555 N
C9 C10 1.4342(9) . 1_555 N
C9 C14 1.3960(10) . 1_555 N
C10 C5 1.4308(11) . 1_555 N
C10 C9 1.4342(9) . 1_555 N
C10 O15 1.3230(8) . 1_555 N
C11 C8 1.4044(9) . 1_555 N
C11 C12 1.4045(10) . 1_555 N
C11 O35 1.3482(8) . 1_555 N
C12 C11 1.4045(10) . 1_555 N
C12 C13 1.3707(8) . 1_555 N
C12 H46 0.9300(6) . 1_555 N
C13 C12 1.3707(8) . 1_555 N
C13 C14 1.4405(10) . 1_555 N
C13 O36 1.3455(10) . 1_555 N
C14 C9 1.3960(10) . 1_555 N
C14 C13 1.4405(10) . 1_555 N
C14 O16 1.3351(8) . 1_555 N
O15 C10 1.3230(8) . 1_555 N
O15 Mn1 1.8503(15) . 1_555 N
O16 C14 1.3351(8) . 1_555 N
O16 Mn1 1.8734(12) . 1_555 N
Mn1 O15 1.8503(15) . 1_555 N
Mn1 O16 1.8734(12) . 1_555 N
Mn1 O18 1.8765(12) . 1_555 N
Mn1 O19 1.8532(15) . 1_555 N
Mn1 O40 2.3679(10) . 1_555 N
Mn1 O41 2.3707(10) . 1_555 N
O18 Mn1 1.8765(12) . 1_555 N
O18 C29 1.3366(8) . 1_555 N
O19 Mn1 1.8532(15) . 1_555 N
O19 C20 1.3240(8) . 1_555 N
C20 O19 1.3240(8) . 1_555 N
C20 C21 1.4296(11) . 1_555 N
C20 C25 1.4351(9) . 1_555 N
C21 C20 1.4296(11) . 1_555 N
C21 C22 1.4044(8) . 1_555 N
C21 C30 1.4169(9) . 1_555 N
C22 C21 1.4044(8) . 1_555 N
C22 C23 1.4937(10) . 1_555 N
C22 C33 1.3850(10) . 1_555 N
C23 C22 1.4937(10) . 1_555 N
C23 C24 1.4623(11) . 1_555 N
C23 O39 1.2076(7) . 1_555 N
C24 C23 1.4623(11) . 1_555 N
C24 C25 1.4269(8) . 1_555 N
C24 C26 1.4041(9) . 1_555 N
C25 C20 1.4351(9) . 1_555 N
C25 C24 1.4269(8) . 1_555 N
C25 C29 1.3966(10) . 1_555 N
C26 C24 1.4041(9) . 1_555 N
C26 C27 1.4050(10) . 1_555 N
C26 O38 1.3489(8) . 1_555 N
C27 C26 1.4050(10) . 1_555 N
C27 C28 1.3715(8) . 1_555 N
C27 H47 0.9300(6) . 1_555 N
C28 C27 1.3715(8) . 1_555 N
C28 C29 1.4392(9) . 1_555 N
C28 O37 1.3472(10) . 1_555 N
C29 O18 1.3366(8) . 1_555 N
C29 C25 1.3966(10) . 1_555 N
C29 C28 1.4392(9) . 1_555 N
C30 C21 1.4169(9) . 1_555 N
C30 C31 1.3757(10) . 1_555 N
C30 H48 0.9300(5) . 1_555 N
C31 C30 1.3757(10) . 1_555 N
C31 C32 1.3933(8) . 1_555 N
C31 H49 0.9300(6) . 1_555 N
C32 C31 1.3933(8) . 1_555 N
C32 C33 1.3986(9) . 1_555 N
C32 H50 0.9299(7) . 1_555 N
C33 C22 1.3850(10) . 1_555 N
C33 C32 1.3986(9) . 1_555 N
C33 H51 0.9301(5) . 1_555 N
O34 C7 1.2071(7) . 1_555 N
O35 C11 1.3482(8) . 1_555 N
O35 H52 0.8200(6) . 1_555 N
O36 C13 1.3455(10) . 1_555 N
O36 H53 0.8200(5) . 1_555 N
O37 C28 1.3472(10) . 1_555 N
O37 H54 0.8200(5) . 1_555 N
O38 C26 1.3489(8) . 1_555 N
O38 H55 0.8201(6) . 1_555 N
O39 C23 1.2076(7) . 1_555 N
O40 Mn1 2.3679(10) . 1_555 N
O40 H56 0.8962(5) . 1_555 N
O40 H57 0.7359(4) . 1_555 N
O41 Mn1 2.3707(10) . 1_555 N
O41 H58 0.9242(5) . 1_555 N
O41 H59 0.7005(5) . 1_555 N
H42 C1 0.9299(6) . 1_555 N
H43 C2 0.9300(7) . 1_555 N
H44 C3 0.9300(6) . 1_555 N
H45 C6 0.9300(5) . 1_555 N
H46 C12 0.9300(6) . 1_555 N
H47 C27 0.9300(6) . 1_555 N
H48 C30 0.9300(5) . 1_555 N
H49 C31 0.9300(6) . 1_555 N
H50 C32 0.9299(7) . 1_555 N
H51 C33 0.9301(5) . 1_555 N
H52 O35 0.8200(6) . 1_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 H42 120.16(4) 1_555 . 1_555 N
C6 C1 H42 120.156(13) 1_555 . 1_555 N
C1 C2 H43 119.83(5) 1_555 . 1_555 N
C3 C2 H43 119.830(13) 1_555 . 1_555 N
C2 C3 H44 119.67(4) 1_555 . 1_555 N
C4 C3 H44 119.67(5) 1_555 . 1_555 N
C1 C6 H45 119.82(5) 1_555 . 1_555 N
C5 C6 H45 119.81(4) 1_555 . 1_555 N
C4 C7 O34 121.06(4) 1_555 . 1_555 N
C8 C7 O34 121.73(5) 1_555 . 1_555 N
C5 C10 O15 113.16(5) 1_555 . 1_555 N
C9 C10 O15 124.66(4) 1_555 . 1_555 N
C8 C11 O35 117.24(4) 1_555 . 1_555 N
C12 C11 O35 119.56(5) 1_555 . 1_555 N
C11 C12 H46 121.716(15) 1_555 . 1_555 N
C13 C12 H46 121.71(4) 1_555 . 1_555 N
C12 C13 O36 118.06(5) 1_555 . 1_555 N
C14 C13 O36 119.820(14) 1_555 . 1_555 N
C9 C14 O16 126.46(5) 1_555 . 1_555 N
C13 C14 O16 112.536(34) 1_555 . 1_555 N
C10 O15 Mn1 122.57(5) 1_555 . 1_555 N
C14 O16 Mn1 119.025(32) 1_555 . 1_555 N
O15 Mn1 O16 100.004(32) 1_555 . 1_555 N
O15 Mn1 O18 79.704(31) 1_555 . 1_555 N
O15 Mn1 O19 180.0 1_555 . 1_555 N
O16 Mn1 O18 180.0 1_555 . 1_555 N
O16 Mn1 O19 80.198(32) 1_555 . 1_555 N
O18 Mn1 O19 100.092(31) 1_555 . 1_555 N
Mn1 O18 C29 117.679(33) 1_555 . 1_555 N
Mn1 O19 C20 121.82(5) 1_555 . 1_555 N
O19 C20 C21 113.35(5) 1_555 . 1_555 N
O19 C20 C25 124.64(4) 1_555 . 1_555 N
C22 C23 O39 121.19(4) 1_555 . 1_555 N
C24 C23 O39 121.83(5) 1_555 . 1_555 N
C24 C26 O38 117.29(4) 1_555 . 1_555 N
C27 C26 O38 119.59(5) 1_555 . 1_555 N
C26 C27 H47 121.708(13) 1_555 . 1_555 N
C26 C27 H59 128.37(5) 1_555 . 2_656 N
C28 C27 H47 121.72(4) 1_555 . 1_555 N
C28 C27 H59 95.51(7) 1_555 . 2_656 N
H47 C27 H59 47.013(19) 1_555 . 2_656 N
C27 C28 O37 118.08(5) 1_555 . 1_555 N
C29 C28 O37 119.675(12) 1_555 . 1_555 N
O18 C29 C25 126.09(5) 1_555 . 1_555 N
O18 C29 C28 113.061(35) 1_555 . 1_555 N
C21 C30 H48 119.91(4) 1_555 . 1_555 N
C31 C30 H48 119.91(5) 1_555 . 1_555 N
C30 C31 H49 120.094(10) 1_555 . 1_555 N
C32 C31 H49 120.10(4) 1_555 . 1_555 N
C31 C32 H50 119.76(5) 1_555 . 1_555 N
C33 C32 H50 119.761(10) 1_555 . 1_555 N
C22 C33 H51 119.78(5) 1_555 . 1_555 N
C32 C33 H51 119.78(4) 1_555 . 1_555 N
C11 O35 H52 123.63(5) 1_555 . 1_555 N
C13 O36 H53 117.653(18) 1_555 . 1_555 N
C28 O37 H54 125.346(15) 1_555 . 1_555 N
C26 O38 H55 123.73(4) 1_555 . 1_555 N


# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_diffrn_ambient_temperature      293
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  ?
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
C 56.0 0.000 0.000 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500
51.6512 0.21560 International_Tables_Vol_C
O 24.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
Mn 2.0 0.000 0.000 11.2819 5.34090 7.35730 0.34320 3.01930 17.8674 2.24410
83.7543 1.08960 International_Tables_Vol_C
H 36.0 0.000 0.000 0.49300 10.5109 0.32291 26.1257 0.14019 3.14236 0.04081
57.7997 0.00304 International_Tables_Vol_C
_diffrn_radiation_probe          x-ray
_diffrn_radiation_polarisn_ratio ?
_diffrn_radiation_wavelength     1.54184
_pd_proc_ls_prof_R_factor        0.0328
_pd_proc_ls_prof_wR_factor       0.0483
_pd_proc_ls_prof_wR_expected     0.0166
_refine_ls_R_Fsqd_factor         0.61754

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 36 terms.
 Shifted Chebyshev function of 1st kind
      1:    3463.86     2:   -2187.35     3:    517.309     4:   -449.379    
      5:    530.583     6:   -540.957     7:    529.344     8:   -390.452    
      9:    169.251    10:    11.0940    11:   -29.7060    12:   -41.7389    
     13:    16.1836    14:    73.5229    15:   -112.543    16:    79.3951    
     17:    20.3101    18:   -114.031    19:    78.5418    20:    23.5690    
     21:   -23.7230    22:   -30.4694    23:    59.2493    24:   -45.8852    
     25:    25.5976    26:   -16.4599    27:    17.7247    28:   -35.8641    
     29:    46.5553    30:    3.71981    31:   -53.5824    32:    27.0247    
     33:    38.0511    34:   -52.5618    35:    30.6667    36:    13.2683    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  905.975 #2(GV)   =  -72.292 #3(GW)   =   23.889
 #4(GP)   =    1.484 #5(LX)   =    5.384 #6(LY)   =   64.790
 #7(S/L)  =   0.0132 #8(H/L)  =   0.0279
 #9(trns) =    -2.08 #10(shft)=   0.4671
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.329 #15(L22) =    1.140 #16(L33) =    0.147
 #17(L12) =   -0.381 #18(L13) =    0.205 #19(L23) =   -0.166
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2015-08-04T11:23:29
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        4.0
_pd_meas_2theta_range_max        79.98
_pd_meas_2theta_range_inc        0.02
_pd_proc_2theta_range_min        4.00007
_pd_proc_2theta_range_max        79.98007
_pd_proc_2theta_range_inc        0.02

loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
8454.0 0.0001183 8997.22754 8997.22754
8592.0 0.0001164 8856.87109 8856.87109
8601.0 0.0001163 8730.10645 8730.10645
8540.0 0.0001171 8615.76367 8615.76367
8365.0 0.0001195 8512.74902 8512.74902
8466.0 0.0001181 8420.04688 8420.04688
8478.0 0.0001180 8336.71387 8336.71387
8421.0 0.0001188 8261.87500 8261.87500
8450.0 0.0001183 8194.71582 8194.71582
8361.0 0.0001196 8134.48486 8134.48486
8280.0 0.0001208 8080.48389 8080.48389
8219.0 0.0001217 8032.07178 8032.07178
8338.0 0.0001199 7988.65137 7988.65137
8169.0 0.0001224 7949.67432 7949.67432
8189.0 0.0001221 7914.63916 7996.63965
8158.0 0.0001226 7883.08008 7967.39014
8092.0 0.0001236 7854.57373 7941.29199
8021.0 0.0001247 7828.72949 7917.96143
8067.0 0.0001240 7805.18945 7897.04736
7972.0 0.0001254 7783.63037 7878.23242
7906.0 0.0001265 7763.75488 7861.22656
7952.0 0.0001258 7745.29590 7845.77100
7978.0 0.0001253 7728.00684 7831.62744
7891.0 0.0001267 7711.66846 7818.58545
7731.0 0.0001293 7696.08350 7806.45801
7735.0 0.0001293 7681.07031 7795.07422
7808.0 0.0001281 7666.47168 7784.28906
7717.0 0.0001296 7652.14355 7773.97021
7632.0 0.0001310 7637.96045 7764.00684
7598.0 0.0001316 7623.80908 7754.30078
7563.0 0.0001322 7609.59131 7744.76953
7626.0 0.0001311 7595.22314 7735.34863
7633.0 0.0001310 7580.62842 7725.98047
7575.0 0.0001320 7565.74316 7716.62305
7551.0 0.0001324 7550.51416 7707.24756
7556.0 0.0001323 7534.89551 7697.83447
7576.0 0.0001320 7518.85010 7688.37598
7462.0 0.0001340 7502.34717 7678.87402
7437.0 0.0001345 7485.36230 7669.33887
7672.0 0.0001303 7467.87891 7659.79541
7533.0 0.0001327 7449.88428 7650.27588
7474.0 0.0001338 7431.37158 7640.82178
7455.0 0.0001341 7412.33594 7631.48633
7419.0 0.0001348 7392.77832 7622.33350
7535.0 0.0001327 7372.70264 7613.43799
7424.0 0.0001347 7352.11621 7604.88818
7437.0 0.0001345 7331.02686 7596.78613
7377.0 0.0001356 7309.44678 7589.24805
7265.0 0.0001376 7287.39014 7582.41064
7463.0 0.0001340 7264.87109 7576.42725
7282.0 0.0001373 7241.90527 7571.47656
7427.0 0.0001346 7218.51221 7567.76807
7259.0 0.0001378 7194.70752 7565.54199
7395.0 0.0001352 7170.51367 7565.08887
7522.0 0.0001329 7145.94727 7566.75195
7580.0 0.0001319 7121.02930 7570.96143
7683.0 0.0001302 7095.77930 7578.26270
7660.0 0.0001305 7070.21826 7589.37646
7697.0 0.0001299 7044.36523 7605.27197
7707.0 0.0001298 7018.24023 7627.27539
7767.0 0.0001287 6991.86230 7657.18701
7900.0 0.0001266 6965.25293 7697.40332
7941.0 0.0001259 6938.42773 7750.99707
8092.0 0.0001236 6911.40625 7821.75781
8091.0 0.0001236 6884.20703 7914.14453
8242.0 0.0001213 6856.84668 8033.15283
8346.0 0.0001198 6829.34180 8184.05127
8693.0 0.0001150 6801.70752 8371.79785
8934.0 0.0001119 6773.96045 8599.84082
9024.0 0.0001108 6746.11377 8868.39746
9362.0 0.0001068 6718.18359 9174.15234
9753.0 0.0001025 6690.17969 9514.90625
10107.0 0.0000989 6662.11719 9897.87402
10628.0 0.0000941 6634.00732 10340.94727
11147.0 0.0000897 6605.86084 10861.12012
11731.0 0.0000852 6577.68945 11459.36328
12340.0 0.0000810 6549.50146 12116.42285
13089.0 0.0000764 6521.30615 12810.78418
14151.0 0.0000707 6493.11230 13550.53906
15113.0 0.0000662 6464.92969 14380.75586
16130.0 0.0000620 6436.76270 15347.56836
17319.0 0.0000577 6408.61963 16456.18555
18722.0 0.0000534 6380.50684 17670.41602
20399.0 0.0000490 6352.43115 18960.51953
21961.0 0.0000455 6324.39551 20339.29297
23703.0 0.0000422 6296.40674 21820.18555
25164.0 0.0000397 6268.46826 23342.67188
26498.0 0.0000377 6240.58496 24768.58789
27248.0 0.0000367 6212.75928 25946.05273
27612.0 0.0000362 6184.99561 26727.95898
27384.0 0.0000365 6157.29688 26933.94922
26681.0 0.0000375 6129.66553 26383.54492
25020.0 0.0000400 6102.10498 25012.79883
22875.0 0.0000437 6074.61572 22953.56641
20784.0 0.0000481 6047.20020 20500.99414
18552.0 0.0000539 6019.86133 17986.45313
16258.0 0.0000615 5992.60059 15658.63965
14798.0 0.0000676 5965.41797 13649.34277
12906.0 0.0000775 5938.31592 11999.08594
11739.0 0.0000852 5911.29639 10692.95410
10556.0 0.0000947 5884.36035 9687.11328
9803.0 0.0001020 5857.50684 8926.15234
9223.0 0.0001084 5830.73926 8354.30957
8601.0 0.0001163 5804.05811 7922.23535
7882.0 0.0001269 5777.46436 7590.15527
7586.0 0.0001318 5750.95850 7328.29883
7242.0 0.0001381 5724.54248 7115.65186
6971.0 0.0001435 5698.21680 6937.98975
6805.0 0.0001470 5671.98291 6785.90332
6655.0 0.0001503 5645.84131 6653.17334
6480.0 0.0001543 5619.79395 6535.60547
6301.0 0.0001587 5593.84229 6430.25879
6145.0 0.0001627 5567.98779 6334.98145
5961.0 0.0001678 5542.22998 6248.12793
5889.0 0.0001698 5516.57275 6168.40869
5795.0 0.0001726 5491.01709 6094.78027
5782.0 0.0001730 5465.56396 6026.39111
5686.0 0.0001759 5440.21729 5962.53809
5637.0 0.0001774 5414.97705 5902.63330
5579.0 0.0001792 5389.84521 5846.18408
5452.0 0.0001834 5364.82568 5792.77686
5411.0 0.0001848 5339.91943 5742.05908
5339.0 0.0001873 5315.12939 5693.72949
5216.0 0.0001917 5290.45752 5647.53174
5134.0 0.0001948 5265.90723 5603.24609
5098.0 0.0001962 5241.48145 5560.68115
5080.0 0.0001969 5217.18164 5519.67090
5085.0 0.0001967 5193.01221 5480.07422
5084.0 0.0001967 5168.97510 5441.76318
4989.0 0.0002004 5145.07471 5145.07471
4938.0 0.0002025 5121.31299 5121.31299
4978.0 0.0002009 5097.69385 5097.69385
4958.0 0.0002017 5074.22070 5074.22070
4894.0 0.0002043 5050.89697 5050.89697
4947.0 0.0002021 5027.72754 5027.72754
4902.0 0.0002040 5004.71338 5004.71338
4773.0 0.0002095 4981.85986 4981.85986
4796.0 0.0002085 4959.17041 4959.17041
4822.0 0.0002074 4936.64893 4936.64893
4889.0 0.0002045 4914.29883 4914.29883
4821.0 0.0002074 4892.12402 4892.12402
4815.0 0.0002077 4870.12842 4870.12842
4777.0 0.0002093 4848.31689 4848.31689
4602.0 0.0002173 4826.69189 4826.69189
4733.0 0.0002113 4805.25781 4805.25781
4694.0 0.0002130 4784.01904 4784.01904
4629.0 0.0002160 4762.97803 4762.97803
4799.0 0.0002084 4742.14063 4742.14063
4645.0 0.0002153 4721.50879 4721.50879
4628.0 0.0002161 4701.08691 4701.08691
4728.0 0.0002115 4680.87939 4680.87939
4642.0 0.0002154 4660.88965 4660.88965
4595.0 0.0002176 4641.12012 4641.12012
4648.0 0.0002151 4621.57568 4621.57568
4498.0 0.0002223 4602.25928 4602.25928
4582.0 0.0002182 4583.17480 4583.17480
4560.0 0.0002193 4564.32520 4564.32520
4608.0 0.0002170 4545.71338 4545.71338
4553.0 0.0002196 4527.34277 4527.34277
4685.0 0.0002134 4509.21680 4509.21680
4508.0 0.0002218 4491.33838 4491.33838
4461.0 0.0002242 4473.70898 4473.70898
4456.0 0.0002244 4456.33301 4456.33301
4522.0 0.0002211 4439.21191 4439.21191
4570.0 0.0002188 4422.34961 4422.34961
4596.0 0.0002176 4405.74658 4405.74658
4444.0 0.0002250 4389.40576 4389.40576
4430.0 0.0002257 4373.33008 4373.33008
4443.0 0.0002251 4357.52051 4357.52051
4439.0 0.0002253 4341.97852 4341.97852
4386.0 0.0002280 4326.70654 4326.70654
4419.0 0.0002263 4311.70508 4311.70508
4423.0 0.0002261 4296.97705 4296.97705
4395.0 0.0002275 4282.52197 4282.52197
4510.0 0.0002217 4268.34082 4268.34082
4493.0 0.0002226 4254.43555 4254.43555
4382.0 0.0002282 4240.80615 4240.80615
4395.0 0.0002275 4227.45361 4227.45361
4399.0 0.0002273 4214.37695 4214.37695
4407.0 0.0002269 4201.57813 4201.57813
4398.0 0.0002274 4189.05664 4189.05664
4419.0 0.0002263 4176.81104 4176.81104
4438.0 0.0002253 4164.84229 4164.84229
4369.0 0.0002289 4153.14941 4153.14941
4358.0 0.0002295 4141.73242 4141.73242
4345.0 0.0002301 4130.58936 4130.58936
4327.0 0.0002311 4119.72021 4119.72021
4390.0 0.0002278 4109.12305 4109.12305
4203.0 0.0002379 4098.79688 4098.79688
4337.0 0.0002306 4088.74097 4088.74097
4260.0 0.0002347 4078.95288 4142.16943
4252.0 0.0002352 4069.43091 4134.80127
4232.0 0.0002363 4060.17334 4160.23584
4321.0 0.0002314 4051.17822 4154.74805
4179.0 0.0002393 4042.44263 4149.70752
4213.0 0.0002374 4033.96509 4145.12695
4281.0 0.0002336 4025.74243 4141.01709
4218.0 0.0002371 4017.77271 4137.39404
4288.0 0.0002332 4010.05249 4134.27100
4287.0 0.0002333 4002.57861 4131.66455
4153.0 0.0002408 3995.34937 4129.59521
4221.0 0.0002369 3988.35986 4128.08154
4238.0 0.0002360 3981.60840 4127.14844
4277.0 0.0002338 3975.09058 4126.82080
4315.0 0.0002317 3968.80347 4127.12793
4241.0 0.0002358 3962.74268 4128.10205
4249.0 0.0002353 3956.90576 4129.78076
4299.0 0.0002326 3951.28735 4132.20264
4294.0 0.0002329 3945.88525 4135.41650
4275.0 0.0002339 3940.69385 4139.47314
4278.0 0.0002338 3935.71045 4144.43359
4191.0 0.0002386 3930.92993 4150.36377
4227.0 0.0002366 3926.34839 4157.34180
4216.0 0.0002372 3921.96143 4165.45459
4208.0 0.0002376 3917.76514 4174.80518
4269.0 0.0002342 3913.75464 4185.50732
4308.0 0.0002321 3909.92554 4197.69678
4315.0 0.0002317 3906.27319 4211.52734
4336.0 0.0002306 3902.79370 4227.18115
4287.0 0.0002333 3899.48169 4244.86816
4236.0 0.0002361 3896.33252 4264.83740
4314.0 0.0002318 3893.34180 4287.38525
4346.0 0.0002301 3890.50537 4312.86670
4366.0 0.0002290 3887.81738 4341.71240
4465.0 0.0002240 3885.27393 4374.46240
4477.0 0.0002234 3882.87012 4411.79785
4433.0 0.0002256 3880.60083 4454.60254
4462.0 0.0002241 3878.46167 4504.04102
4538.0 0.0002204 3876.44775 4561.66455
4577.0 0.0002185 3874.55444 4629.54053
4589.0 0.0002179 3872.77710 4710.40137
4699.0 0.0002128 3871.11108 4807.79639
4883.0 0.0002048 3869.55103 4926.23438
4910.0 0.0002037 3868.09277 5071.29980
4911.0 0.0002036 3866.73193 5249.72949
5105.0 0.0001959 3865.46362 5469.43408
5265.0 0.0001899 3864.28345 5739.41650
5537.0 0.0001806 3863.18652 6069.42529
5747.0 0.0001740 3862.16870 6469.02393
6039.0 0.0001656 3861.22583 6945.72119
6271.0 0.0001595 3860.35303 7502.43945
6845.0 0.0001461 3859.54590 8136.48828
7476.0 0.0001338 3858.80103 8843.78906
8095.0 0.0001235 3858.11353 9628.12207
9067.0 0.0001103 3857.47949 10505.65820
10035.0 0.0000997 3856.89502 11494.00098
11152.0 0.0000897 3856.35571 12588.41406
12465.0 0.0000802 3855.85864 13740.40527
14278.0 0.0000700 3855.39893 14856.26758
15650.0 0.0000639 3854.97363 15824.21973
16576.0 0.0000603 3854.57861 16550.60938
17444.0 0.0000573 3854.21069 16965.90820
17619.0 0.0000568 3853.86621 17001.63281
17068.0 0.0000586 3853.54199 16594.26563
15524.0 0.0000644 3853.23462 15739.09668
13576.0 0.0000737 3852.94116 14531.26660
11889.0 0.0000841 3852.65845 13135.93848
10325.0 0.0000969 3852.38354 11718.23340
9174.0 0.0001090 3852.11328 10395.65820
8267.0 0.0001210 3851.84521 9230.92676
7422.0 0.0001347 3851.57715 8245.84668
6852.0 0.0001459 3851.30566 7437.27246
6331.0 0.0001580 3851.02905 6788.56104
5913.0 0.0001691 3850.74414 6276.80127
5676.0 0.0001762 3850.44971 5877.36914
5358.0 0.0001866 3850.14307 5566.81641
5134.0 0.0001948 3849.82227 5324.57520
5051.0 0.0001980 3849.48584 5133.72461
5001.0 0.0002000 3849.13159 4981.05664
4822.0 0.0002074 3848.75830 4856.69580
4768.0 0.0002097 3848.36377 4753.48389
4732.0 0.0002113 3847.94702 4666.34033
4659.0 0.0002146 3847.50684 4591.67578
4644.0 0.0002153 3847.04224 4526.93750
4538.0 0.0002204 3846.55151 4470.27002
4474.0 0.0002235 3846.03345 4420.28906
4498.0 0.0002223 3845.48804 4375.92969
4449.0 0.0002248 3844.91431 4336.34814
4346.0 0.0002301 3844.31152 4300.86182
4228.0 0.0002365 3843.67871 4268.90918
4194.0 0.0002384 3843.01636 4240.02393
4191.0 0.0002386 3842.32300 4213.81104
4181.0 0.0002392 3841.59961 4189.93945
4123.0 0.0002425 3840.84546 4168.12500
4092.0 0.0002444 3840.06030 4148.12500
4163.0 0.0002402 3839.24463 4129.73145
4059.0 0.0002464 3838.39844 4112.76465
4041.0 0.0002475 3837.52222 4097.06934
4051.0 0.0002469 3836.61621 4082.50928
4004.0 0.0002498 3835.68091 4068.96680
3987.0 0.0002508 3834.71704 4056.33838
3984.0 0.0002510 3833.72510 4044.53320
3996.0 0.0002503 3832.70557 4033.47119
4061.0 0.0002462 3831.65967 3897.60791
4198.0 0.0002382 3830.58862 3830.58862
4075.0 0.0002454 3829.49292 3829.49292
3965.0 0.0002522 3828.37354 3828.37354
3971.0 0.0002518 3827.23218 3827.23218
4099.0 0.0002440 3826.06958 3826.06958
4003.0 0.0002498 3824.88770 3824.88770
3864.0 0.0002588 3823.68701 3823.68701
4028.0 0.0002483 3822.46997 3822.46997
3856.0 0.0002593 3821.23730 3821.23730
3844.0 0.0002601 3819.99097 3819.99097
3971.0 0.0002518 3818.73267 3818.73267
3930.0 0.0002545 3817.46362 3817.46362
3846.0 0.0002600 3816.18628 3816.18628
3799.0 0.0002632 3814.90186 3814.90186
3859.0 0.0002591 3813.61279 3813.61279
3790.0 0.0002639 3812.32056 3812.32056
3813.0 0.0002623 3811.02710 3811.02710
3880.0 0.0002577 3809.73486 3809.73486
3901.0 0.0002563 3808.44556 3808.44556
3838.0 0.0002606 3807.16089 3807.16089
3838.0 0.0002606 3805.88379 3805.88379
3863.0 0.0002589 3804.61548 3804.61548
3857.0 0.0002593 3803.35913 3803.35913
3815.0 0.0002621 3802.11597 3802.11597
3827.0 0.0002613 3800.88892 3800.88892
3856.0 0.0002593 3799.67993 3799.67993
3840.0 0.0002604 3798.49146 3798.49146
3837.0 0.0002606 3797.32520 3797.32520
3873.0 0.0002582 3796.18384 3796.18384
3831.0 0.0002610 3795.06982 3795.06982
3818.0 0.0002619 3793.98511 3793.98511
3871.0 0.0002583 3792.93213 3792.93213
3814.0 0.0002622 3791.91333 3791.91333
3802.0 0.0002630 3790.93042 3790.93042
3845.0 0.0002601 3789.98657 3793.31738
3829.0 0.0002612 3789.08350 3794.17139
3876.0 0.0002580 3788.22363 3793.50366
3943.0 0.0002536 3787.40894 3792.89233
3935.0 0.0002541 3786.64233 3792.34082
3878.0 0.0002579 3785.92505 3791.85156
3906.0 0.0002560 3785.26050 3791.42896
3819.0 0.0002618 3784.64966 3791.07495
3808.0 0.0002626 3784.09546 3790.79443
3906.0 0.0002560 3783.60010 3790.59009
3841.0 0.0002603 3783.16528 3790.46582
3776.0 0.0002648 3782.79297 3790.42505
3794.0 0.0002636 3782.48560 3790.47241
3899.0 0.0002565 3782.24512 3790.61157
3912.0 0.0002556 3782.07349 3790.84741
3894.0 0.0002568 3781.97241 3791.18433
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2186.0 0.000457 2120.79321 2152.73608
2191.0 0.000456 2119.15576 2150.43506
2146.0 0.000466 2117.51050 2145.39526
2153.0 0.000464 2115.85620 2142.74243
2115.0 0.000473 2114.19434 2140.26636
2179.0 0.000459 2112.52490 2137.53442
2134.0 0.000469 2110.84717 2135.10254
2159.0 0.000463 2109.16284 2132.41699
2126.0 0.000470 2107.47119 2129.55859
2144.0 0.000466 2105.77319 2127.28687
2144.0 0.000466 2104.06836 2124.66357
2112.0 0.000473 2102.35791 2121.03198
2091.0 0.000478 2100.64160 2117.35010
2116.0 0.000473 2098.91919 2115.42944
2084.0 0.000480 2097.19214 2113.19214
2106.0 0.000475 2095.45972 2111.09766
2052.0 0.000487 2093.72314 2109.18359
2162.0 0.000463 2091.98193 2107.82959
2091.0 0.000478 2090.23706 2105.95337
2148.0 0.000466 2088.48804 2104.21484
2086.0 0.000479 2086.73633 2102.68164
2080.0 0.000481 2084.98169 2100.07178
2060.0 0.000485 2083.22363 2098.65918
2068.0 0.000484 2081.46387 2097.37793
2055.0 0.000487 2079.70142 2096.01245
2083.0 0.000480 2077.93799 2094.78662
2035.0 0.000491 2076.17285 2091.61987
2067.0 0.000484 2074.40698 2090.57178
2113.0 0.000473 2072.64014 2089.55176
2108.0 0.000474 2070.87354 2084.54736
2086.0 0.000479 2069.10693 2085.19263
2054.0 0.000487 2067.34033 2084.48071
2043.0 0.000489 2065.57495 2083.89136
2060.0 0.000485 2063.81006 2083.25806
2076.0 0.000482 2062.04736 2082.58618
2066.0 0.000484 2060.28564 2087.40942
2111.0 0.000474 2058.52686 2086.41479
2118.0 0.000472 2056.77075 2085.55566
2081.0 0.000481 2055.01685 2082.71313
2079.0 0.000481 2053.26685 2082.93896
2113.0 0.000473 2051.51978 2082.84961
2128.0 0.000470 2049.77734 2081.92163
2117.0 0.000472 2048.03882 2080.92700
2105.0 0.000475 2046.30530 2080.11475
2109.0 0.000474 2044.57642 2086.15405
2104.0 0.000475 2042.85339 2084.91431
2072.0 0.000483 2041.13623 2083.67822
2080.0 0.000481 2039.42468 2082.34619
2076.0 0.000482 2037.71997 2082.62231
2116.0 0.000473 2036.02161 2081.72778
2144.0 0.000466 2034.33093 2080.24805
2122.0 0.000471 2032.64734 2081.55664
2103.0 0.000476 2030.97192 2079.82080
2157.0 0.000464 2029.30444 2080.25366
2058.0 0.000486 2027.64587 2078.66846
2046.0 0.000489 2025.99622 2085.75439
2072.0 0.000483 2024.35535 2083.81226
2144.0 0.000466 2022.72437 2082.54053
2084.0 0.000480 2021.10291 2077.33301
2044.0 0.000489 2019.49207 2075.25513
2038.0 0.000491 2017.89124 2070.89087
2076.0 0.000482 2016.30176 2070.37354
2067.0 0.000484 2014.72351 2068.19263
2070.0 0.000483 2013.15613 2066.38208
2089.0 0.000479 2011.60107 2067.96484
2017.0 0.000496 2010.05762 2066.39380
2109.0 0.000474 2008.52698 2065.98267
2136.0 0.000468 2007.00842 2064.01221
2052.0 0.000487 2005.50342 2060.87207
2053.0 0.000487 2004.01111 2058.06958
2061.0 0.000485 2002.53271 2053.20313
2069.0 0.000483 2001.06824 2051.69116
2068.0 0.000484 1999.61719 2050.39087
2078.0 0.000481 1998.18103 2050.69678
2005.0 0.000499 1996.75867 2050.87891
1999.0 0.000500 1995.35193 2049.77466
2048.0 0.000488 1993.95959 2049.43848
2031.0 0.000492 1992.58289 2050.13525
2053.0 0.000487 1991.22131 2049.07935
2032.0 0.000492 1989.87573 2049.67139
2043.0 0.000489 1988.54626 2047.07190
2042.0 0.000490 1987.23242 2045.31824
2078.0 0.000481 1985.93530 2044.47229
2012.0 0.000497 1984.65417 2045.25317
1996.0 0.000501 1983.39038 2044.43591
2037.0 0.000491 1982.14294 2043.63330
2040.0 0.000490 1980.91284 2042.78979
2026.0 0.000494 1979.70007 2042.77563
2026.0 0.000494 1978.50415 2041.48853
2031.0 0.000492 1977.32617 2041.33044
2003.0 0.000499 1976.16528 2037.69360
2024.0 0.000494 1975.02271 2038.35107
2035.0 0.000491 1973.89746 2037.32983
2028.0 0.000493 1972.79077 2036.46533
2046.0 0.000489 1971.70166 2040.05859
1990.0 0.000503 1970.63098 2039.06201
2013.0 0.000497 1969.57861 2038.03015
2050.0 0.000488 1968.54419 2036.96045
2022.0 0.000495 1967.52856 2035.61169
2026.0 0.000494 1966.53088 2033.81372
2045.0 0.000489 1965.55212 2032.65100
2045.0 0.000489 1964.59143 2031.71387
2028.0 0.000493 1963.64978 2029.77734
2102.0 0.000476 1962.72632 2028.61768
2126.0 0.000470 1961.82166 2028.17224
2075.0 0.000482 1960.93567 2026.96619
2018.0 0.000496 1960.06775 2025.62793
2017.0 0.000496 1959.21875 2024.10205
2047.0 0.000489 1958.38794 2022.99048
1998.0 0.000501 1957.57593 2021.58655
1961.0 0.000510 1956.78186 2020.02234
1972.0 0.000507 1956.00659 2006.10168
2007.0 0.000498 1955.24951 2005.20984
2041.0 0.000490 1954.51038 2003.49634
2026.0 0.000494 1953.78967 2001.55237
2107.0 0.000475 1953.08655 2000.31030
2041.0 0.000490 1952.40173 1999.31433
1965.0 0.000509 1951.73438 1998.21375
1985.0 0.000504 1951.08484 1997.20459
1952.0 0.000512 1950.45264 1996.54102
1980.0 0.000505 1949.83801 1995.73450
1999.0 0.000500 1949.24072 1988.70117
1983.0 0.000504 1948.66003 1984.69995
2007.0 0.000498 1948.09656 1983.71912
2018.0 0.000496 1947.54944 1982.51929
2047.0 0.000489 1947.01917 1979.71924
2038.0 0.000491 1946.50476 1979.15955
1985.0 0.000504 1946.00671 1978.59705
1995.0 0.000501 1945.52429 1978.05737
2009.0 0.000498 1945.05774 1977.23486
2037.0 0.000491 1944.60657 1976.53552
1962.0 0.000510 1944.17017 1973.56519
1952.0 0.000512 1943.74902 1973.02673
1969.0 0.000508 1943.34216 1972.28821
1983.0 0.000504 1942.94983 1966.68726
1989.0 0.000503 1942.57129 1962.20569
1991.0 0.000502 1942.20667 1961.79102
2002.0 0.000500 1941.85559 1961.45166
1961.0 0.000510 1941.51746 1961.01196
1982.0 0.000505 1941.19226 1960.71753
2059.0 0.000486 1940.87952 1959.84155
2021.0 0.000495 1940.57898 1959.47449
1982.0 0.000505 1940.29016 1959.33679
2016.0 0.000496 1940.01306 1956.49695
1994.0 0.000502 1939.74683 1952.27576
1969.0 0.000508 1939.49170 1952.79468
1959.0 0.000510 1939.24683 1952.62500
1941.0 0.000515 1939.01196 1952.45715
1964.0 0.000509 1938.78687 1952.37524
1973.0 0.000507 1938.57092 1960.49866
2052.0 0.000487 1938.36401 1960.06531
2020.0 0.000495 1938.16553 1962.35815
2054.0 0.000487 1937.97534 1960.60083
2004.0 0.000499 1937.79260 1960.56482
1990.0 0.000503 1937.61743 1960.04614
1955.0 0.000512 1937.44910 1959.94141
1952.0 0.000512 1937.28711 1959.39417
1967.0 0.000508 1937.13135 1959.60645
1973.0 0.000507 1936.98096 1961.36365
1912.0 0.000523 1936.83606 1961.13721
1951.0 0.000513 1936.69568 1961.20129
1980.0 0.000505 1936.55981 1963.12256
1936.0 0.000517 1936.42786 1962.55847
1956.0 0.000511 1936.29932 1962.21753
1991.0 0.000502 1936.17383 1961.64111
1926.0 0.000519 1936.05078 1952.29016
1924.0 0.000520 1935.93005 1952.02820
1940.0 0.000515 1935.81079 1951.13013
2002.0 0.000500 1935.69299 1951.06616
1966.0 0.000509 1935.57581 1950.82617
2007.0 0.000498 1935.45911 1949.52417
1909.0 0.000524 1935.34229 1949.90369
1964.0 0.000509 1935.22473 1949.72485
1963.0 0.000509 1935.10632 1949.54370
2002.0 0.000500 1934.98645 1944.88647
1969.0 0.000508 1934.86462 1944.85767
1970.0 0.000508 1934.74048 1944.93762
1938.0 0.000516 1934.61365 1944.95374
1887.0 0.000530 1934.48340 1944.92761
1950.0 0.000513 1934.34961 1946.12769
1884.0 0.000531 1934.21167 1945.40808
1902.0 0.000526 1934.06921 1951.19727
1986.0 0.000504 1933.92175 1951.17419
2016.0 0.000496 1933.76880 1949.78015
2000.0 0.000500 1933.61023 1949.79968
1946.0 0.000514 1933.44519 1950.30298
1959.0 0.000510 1933.27356 1950.39465
1965.0 0.000509 1933.09497 1950.45691
1922.0 0.000520 1932.90869 1950.49353
1937.0 0.000516 1932.71472 1951.20581
1963.0 0.000509 1932.51221 1948.08789
1955.0 0.000512 1932.30127 1949.12866
1960.0 0.000510 1932.08105 1948.51599
1956.0 0.000511 1931.85168 1948.67249
1955.0 0.000512 1931.61218 1949.02087
1961.0 0.000510 1931.36279 1948.48682
1899.0 0.000527 1931.10278 1948.65234
1884.0 0.000531 1930.83179 1948.81152
1928.0 0.000519 1930.54968 1949.27002
1948.0 0.000513 1930.25586 1949.27014
1907.0 0.000524 1929.95032 1951.68811
1968.0 0.000508 1929.63232 1950.41357
1902.0 0.000526 1929.30212 1950.35925
1923.0 0.000520 1928.95886 1951.39734
1908.0 0.000524 1928.60266 1951.26184
1859.0 0.000538 1928.23315 1951.52063
1879.0 0.000532 1927.84973 1952.21558
1822.0 0.000549 1927.45264 1952.39429
1854.0 0.000539 1927.04102 1952.67419
1913.0 0.000523 1926.61536 1952.69580
1922.0 0.000520 1926.17480 1953.82483
1944.0 0.000514 1925.71960 1953.58801
1959.0 0.000510 1925.24939 1953.28296
1940.0 0.000515 1924.76355 1953.65222
1922.0 0.000520 1924.26257 1955.46265
1896.0 0.000527 1923.74573 1955.20337
1927.0 0.000519 1923.21338 1957.24231
1881.0 0.000532 1922.66479 1956.85815
1891.0 0.000529 1922.10046 1955.72925
1972.0 0.000507 1921.51953 1954.84583
1960.0 0.000510 1920.92273 1948.84998
1947.0 0.000514 1920.30933 1948.05273
1914.0 0.000522 1919.67932 1947.19141
1882.0 0.000531 1919.03284 1942.36694
1955.0 0.000512 1918.36951 1941.49731
1882.0 0.000531 1917.68982 1942.16138
1903.0 0.000525 1916.99316 1942.25061
1969.0 0.000508 1916.27991 1941.16150
1938.0 0.000516 1915.54968 1939.77844
1931.0 0.000518 1914.80298 1938.90320
1907.0 0.000524 1914.03967 1935.04688
1897.0 0.000527 1913.25916 1933.69775
1867.0 0.000536 1912.46240 1932.33960
1908.0 0.000524 1911.64868 1927.99329
1939.0 0.000516 1910.81873 1926.59399
1926.0 0.000519 1909.97205 1925.70081
1958.0 0.000511 1909.10925 1924.74854
1932.0 0.000518 1908.23022 1923.31177
1896.0 0.000527 1907.33484 1921.54492
1915.0 0.000522 1906.42383 1920.19495
1896.0 0.000527 1905.49658 1918.75610
1863.0 0.000537 1904.55408 1917.27295
1873.0 0.000534 1903.59558 1917.02112
1910.0 0.000524 1902.62231 1915.20264
1918.0 0.000521 1901.63354 1914.22742
1930.0 0.000518 1900.63025 1912.94727
1956.0 0.000511 1899.61218 1911.00208
1917.0 0.000522 1898.57959 1909.50037
1914.0 0.000522 1897.53320 1907.82056
1974.0 0.000507 1896.47229 1910.20850
1902.0 0.000526 1895.39844 1908.64868
1856.0 0.000539 1894.31067 1907.11609
1893.0 0.000528 1893.21045 1903.62744
1844.0 0.000542 1892.09705 1902.16919
1900.0 0.000526 1890.97180 1900.66296
1895.0 0.000528 1889.83435 1899.79993
1913.0 0.000523 1888.68494 1898.20630
1893.0 0.000528 1887.52454 1896.73901
1816.0 0.000551 1886.35291 1895.38379
1861.0 0.000537 1885.17102 1895.84583
1913.0 0.000523 1883.97852 1894.34546
1860.0 0.000538 1882.77673 1892.85913
1895.0 0.000528 1881.56543 1889.42090
1890.0 0.000529 1880.34497 1888.00220
1938.0 0.000516 1879.11621 1886.58496
1909.0 0.000524 1877.87903 1885.16577
1923.0 0.000520 1876.63464 1884.52502
1882.0 0.000531 1875.38269 1883.12866
1847.0 0.000541 1874.12439 1880.35388
1892.0 0.000529 1872.85925 1879.02808
1906.0 0.000525 1871.58899 1877.65051
1907.0 0.000524 1870.31323 1876.59583
1887.0 0.000530 1869.03235 1875.48450
1835.0 0.000545 1867.74744 1874.14722
1897.0 0.000527 1866.45850 1872.77417
1875.0 0.000533 1865.16638 1871.47974
1866.0 0.000536 1863.87109 1876.31628
1825.0 0.000548 1862.57410 1875.17358
1864.0 0.000536 1861.27466 1873.89563
1909.0 0.000524 1859.97449 1872.09143
1902.0 0.000526 1858.67334 1870.98169
1845.0 0.000542 1857.37170 1869.92346
1849.0 0.000541 1856.07068 1868.71094
1909.0 0.000524 1854.77014 1867.77893
1934.0 0.000517 1853.47131 1866.35217
1920.0 0.000521 1852.17395 1862.40161
1872.0 0.000534 1850.87939 1864.15295
1855.0 0.000539 1849.58765 1863.03308
1852.0 0.000540 1848.29907 1861.98083
1824.0 0.000548 1847.01477 1860.87207
1861.0 0.000537 1845.73462 1859.98840
1916.0 0.000522 1844.45972 1854.76147
1861.0 0.000537 1843.19006 1853.74841
1819.0 0.000550 1841.92676 1852.52612
1849.0 0.000541 1840.66956 1850.24939
1873.0 0.000534 1839.42004 1847.92017
1919.0 0.000521 1838.17786 1847.03113
1924.0 0.000520 1836.94336 1846.17981
1872.0 0.000534 1835.71765 1845.35303
1863.0 0.000537 1834.50073 1844.15698
1807.0 0.000553 1833.29358 1843.26160
1905.0 0.000525 1832.09607 1840.52209
1897.0 0.000527 1830.90930 1839.69189
1852.0 0.000540 1829.73303 1839.73425
1830.0 0.000546 1828.56848 1838.42627
1882.0 0.000531 1827.41553 1837.04358
1937.0 0.000516 1826.27454 1836.34277
1832.0 0.000546 1825.14636 1837.69824
1850.0 0.000541 1824.03076 1837.14392
1782.0 0.000561 1822.92896 1836.47229
1755.0 0.000570 1821.84058 1835.68420
1815.0 0.000551 1820.76648 1842.16272
1903.0 0.000525 1819.70703 1841.36011
1867.0 0.000536 1818.66211 1840.74451
1889.0 0.000529 1817.63245 1839.63806
1814.0 0.000551 1816.61804 1838.85486
1865.0 0.000536 1815.61963 1837.80481
1796.0 0.000557 1814.63708 1834.30676
1784.0 0.000561 1813.67102 1833.72986
1828.0 0.000547 1812.72119 1837.61719
1826.0 0.000548 1811.78857 1837.17371
1741.0 0.000574 1810.87292 1840.25244
1833.0 0.000546 1809.97437 1839.70776
1885.0 0.000531 1809.09326 1839.19739
1870.0 0.000535 1808.22974 1838.24121
1852.0 0.000540 1807.38403 1838.17310
1920.0 0.000521 1806.55615 1836.18616
1897.0 0.000527 1805.74646 1833.43127
1837.0 0.000544 1804.95471 1832.88733
1809.0 0.000553 1804.18127 1839.72217
1823.0 0.000549 1803.42627 1839.17444
1851.0 0.000540 1802.68933 1837.30835
1873.0 0.000534 1801.97083 1836.59949
1847.0 0.000541 1801.27063 1836.77454
1875.0 0.000533 1800.58887 1836.00964
1898.0 0.000527 1799.92542 1835.18457
1862.0 0.000537 1799.28027 1823.96289
1860.0 0.000538 1798.65344 1822.94226
1837.0 0.000544 1798.04443 1821.99780
1794.0 0.000557 1797.45374 1823.46851
1802.0 0.000555 1796.88062 1822.54492
1835.0 0.000545 1796.32556 1821.76282
1849.0 0.000541 1795.78796 1820.74475
1848.0 0.000541 1795.26770 1819.71057
1872.0 0.000534 1794.76465 1817.95459
1859.0 0.000538 1794.27844 1817.23389
1801.0 0.000555 1793.80920 1811.47107
1835.0 0.000545 1793.35608 1807.26233
1818.0 0.000550 1792.91943 1806.29126
1812.0 0.000552 1792.49829 1805.23425
1825.0 0.000548 1792.09302 1803.95740
1833.0 0.000546 1791.70276 1803.47766
1773.0 0.000564 1791.32727 1802.64417
1800.0 0.000556 1790.96631 1801.88232
1841.0 0.000543 1790.61938 1800.75891
1855.0 0.000539 1790.28613 1800.55151
1870.0 0.000535 1789.96582 1800.21082
1754.0 0.000570 1789.65857 1793.27722
1806.0 0.000554 1789.36340 1792.18335
1874.0 0.000534 1789.08020 1791.89880
1826.0 0.000548 1788.80811 1816.46960
1827.0 0.000547 1788.54688 1816.29028
1850.0 0.000541 1788.29590 1817.32263
1826.0 0.000548 1788.05457 1817.20032
1775.0 0.000563 1787.82239 1815.97693
1863.0 0.000537 1787.59863 1815.98657
1802.0 0.000555 1787.38306 1816.15015
1853.0 0.000540 1787.17468 1816.30493
1758.0 0.000569 1786.97327 1813.64331
1758.0 0.000569 1786.77783 1813.66577
1787.0 0.000560 1786.58789 1826.06006
1818.0 0.000550 1786.40283 1825.96716
1776.0 0.000563 1786.22180 1826.44983
1783.0 0.000561 1786.04456 1826.45752
1761.0 0.000568 1785.86987 1825.68713
1771.0 0.000565 1785.69763 1825.67310
1776.0 0.000563 1785.52661 1825.46179
1833.0 0.000546 1785.35657 1825.22363
1826.0 0.000548 1785.18652 1825.11194
1841.0 0.000543 1785.01575 1823.62915
1877.0 0.000533 1784.84387 1823.23926
1837.0 0.000544 1784.66968 1822.74561
1801.0 0.000555 1784.49292 1822.24377
1816.0 0.000551 1784.31250 1821.68347
1814.0 0.000551 1784.12805 1822.27014
1802.0 0.000555 1783.93848 1821.61414
1798.0 0.000556 1783.74341 1820.93115
1791.0 0.000558 1783.54211 1820.18530
1798.0 0.000556 1783.33350 1818.72388
1804.0 0.000554 1783.11731 1817.91125
1763.0 0.000567 1782.89246 1819.66943
1759.0 0.000569 1782.65869 1818.88245
1798.0 0.000556 1782.41479 1818.00208
1817.0 0.000550 1782.16052 1817.23059
1830.0 0.000546 1781.89490 1810.31970
1769.0 0.000565 1781.61755 1813.11316
1793.0 0.000558 1781.32776 1812.21338
1807.0 0.000553 1781.02454 1811.29858
1781.0 0.000561 1780.70764 1810.35083
1785.0 0.000560 1780.37622 1809.09021
1747.0 0.000572 1780.02991 1807.95447
1733.0 0.000577 1779.66772 1808.59204
1789.0 0.000559 1779.28955 1808.13477
1816.0 0.000551 1778.89453 1807.22290
1828.0 0.000547 1778.48230 1805.16187
1770.0 0.000565 1778.05225 1800.51880
1837.0 0.000544 1777.60376 1801.36035
1762.0 0.000568 1777.13660 1800.37854
1704.0 0.000587 1776.65002 1799.38550
1734.0 0.000577 1776.14392 1798.37244
1874.0 0.000534 1775.61755 1791.94739
1742.0 0.000574 1775.07092 1791.14026
1824.0 0.000548 1774.50342 1791.11572
1776.0 0.000563 1773.91431 1790.46313
1768.0 0.000566 1773.30408 1789.53589
1783.0 0.000561 1772.67175 1788.07019
1789.0 0.000559 1772.01770 1786.96948
1749.0 0.000572 1771.34106 1784.03210
1760.0 0.000568 1770.64221 1783.16895
1823.0 0.000549 1769.92029 1782.25049
1811.0 0.000552 1769.17603 1780.03577
1734.0 0.000577 1768.40869 1776.49609
1704.0 0.000587 1767.61816 1776.21338
1819.0 0.000550 1766.80493 1775.85010
1811.0 0.000552 1765.96826 1774.23779
1729.0 0.000578 1765.10889 1773.55713
1727.0 0.000579 1764.22620 1772.62830
1780.0 0.000562 1763.32104 1770.50500
1759.0 0.000569 1762.39270 1769.36230
1735.0 0.000576 1761.44214 1768.79150
1745.0 0.000573 1760.46924 1767.89197
1804.0 0.000554 1759.47363 1767.09473
1763.0 0.000567 1758.45654 1766.67883
1718.0 0.000582 1757.41748 1765.78992
1758.0 0.000569 1756.35742 1764.92053
1774.0 0.000564 1755.27612 1766.49438
1763.0 0.000567 1754.17468 1765.39978
1777.0 0.000563 1753.05322 1764.01782
1806.0 0.000554 1751.91162 1762.97302
1826.0 0.000548 1750.75159 1762.09583
1809.0 0.000553 1749.57239 1761.17993
1791.0 0.000558 1748.37573 1760.27539
1784.0 0.000561 1747.16125 1759.71704
1748.0 0.000572 1745.93066 1759.82837
1740.0 0.000575 1744.68347 1759.06995
1791.0 0.000558 1743.42163 1762.01245
1801.0 0.000555 1742.14526 1761.48987
1793.0 0.000558 1740.85449 1760.53186
1726.0 0.000579 1739.55151 1759.57556
1735.0 0.000576 1738.23584 1758.85168
1770.0 0.000565 1736.90955 1757.99939
1815.0 0.000551 1735.57239 1757.87500
1814.0 0.000551 1734.22656 1757.27087
1810.0 0.000552 1732.87170 1755.93237
1743.0 0.000574 1731.51013 1755.75391
1718.0 0.000582 1730.14221 1754.90686
1818.0 0.000550 1728.76831 1756.92798
1730.0 0.000578 1727.39087 1756.99316
1754.0 0.000570 1726.00964 1756.28760
1719.0 0.000582 1724.62695 1755.91003
1706.0 0.000586 1723.24280 1755.48706
1756.0 0.000569 1721.85950 1754.98315
1820.0 0.000549 1720.47766 1754.88904
1797.0 0.000556 1719.09778 1754.53162
1786.0 0.000560 1717.72229 1753.94543
1835.0 0.000545 1716.35132 1753.88464
1697.0 0.000589 1714.98706 1753.51440
1741.0 0.000574 1713.62988 1753.77649
1750.0 0.000571 1712.28186 1753.77075
1683.0 0.000594 1710.94324 1753.08093
1755.0 0.000570 1709.61646 1753.89319
1798.0 0.000556 1708.30225 1754.49536
1746.0 0.000573 1707.00110 1754.15125
1730.0 0.000578 1705.71545 1753.78784
1807.0 0.000553 1704.44556 1753.42139
1790.0 0.000559 1703.19373 1753.13293
1746.0 0.000573 1701.96008 1753.05664
1719.0 0.000582 1700.74683 1752.71326
1733.0 0.000577 1699.55420 1752.42932
1762.0 0.000568 1698.38464 1751.97449
1774.0 0.000564 1697.23840 1753.35999
1742.0 0.000574 1696.11658 1753.24182
1765.0 0.000567 1695.02100 1753.08569
1793.0 0.000558 1693.95190 1752.63330
1771.0 0.000565 1692.91138 1752.86169
1759.0 0.000569 1691.89966 1752.37573
1800.0 0.000556 1690.91858 1751.95483
1808.0 0.000553 1689.96875 1751.77502
1775.0 0.000563 1689.05066 1751.23364
1764.0 0.000567 1688.16614 1747.04224
1738.0 0.000575 1687.31531 1746.35535
1720.0 0.000581 1686.49976 1746.51782
1733.0 0.000577 1685.71960 1747.08765
1758.0 0.000569 1684.97632 1745.62720
1758.0 0.000569 1684.27002 1745.01245
1752.0 0.000571 1683.60193 1744.38782
1739.0 0.000575 1682.97253 1743.15869
1708.0 0.000585 1682.38196 1742.50708
1722.0 0.000581 1681.83130 1742.01819
1736.0 0.000576 1681.32056 1741.37158
1778.0 0.000562 1680.85071 1738.92908
1744.0 0.000573 1680.42151 1738.25269
1742.0 0.000574 1680.03381 1736.42773
1765.0 0.000567 1679.68738 1733.03064
1641.0 0.000609 1679.38269 1728.61328
1795.0 0.000557 1679.11963 1728.28760
1805.0 0.000554 1678.89819 1727.99023
1698.0 0.000589 1678.71863 1727.17102
1759.0 0.000569 1678.58044 1726.92920
1743.0 0.000574 1678.48376 1726.66638
1733.0 0.000577 1678.42810 1725.91699
1713.0 0.000584 1678.41333 1725.60706
1716.0 0.000583 1678.43872 1725.52124
1767.0 0.000566 1678.50427 1724.59570
1729.0 0.000578 1678.60901 1719.67175
1693.0 0.000591 1678.75232 1719.66089
1728.0 0.000579 1678.93372 1716.95996
1739.0 0.000575 1679.15222 1717.03674
1735.0 0.000576 1679.40698 1719.37024
1661.0 0.000602 1679.69714 1719.69434
1649.0 0.000606 1680.02148 1720.65088
1723.0 0.000580 1680.37903 1720.87183
1743.0 0.000574 1680.76880 1720.31458
1710.0 0.000585 1681.18896 1717.41089
1709.0 0.000585 1681.63904 1718.70410
1736.0 0.000576 1682.11670 1718.34766
1706.0 0.000586 1682.62122 1718.28491
1715.0 0.000583 1683.15039 1717.52454
1728.0 0.000579 1683.70313 1718.39026
1685.0 0.000593 1684.27747 1720.41418
1672.0 0.000598 1684.87146 1720.95056
1720.0 0.000581 1685.48401 1721.41748
1714.0 0.000583 1686.11230 1722.23059
1682.0 0.000595 1686.75525 1722.63159
1719.0 0.000582 1687.41016 1720.38440
1746.0 0.000573 1688.07532 1720.80774
1767.0 0.000566 1688.74854 1718.60510
1783.0 0.000561 1689.42749 1718.30981
1731.0 0.000578 1690.11047 1718.96887
1696.0 0.000590 1690.79468 1719.87891
1748.0 0.000572 1691.47839 1720.68176
1754.0 0.000570 1692.15857 1720.99329
1699.0 0.000589 1692.83374 1721.22668
1735.0 0.000576 1693.50073 1721.12683
1708.0 0.000585 1694.15771 1721.76355
1691.0 0.000591 1694.80188 1721.71948
1732.0 0.000577 1695.43091 1722.18762
1741.0 0.000574 1696.04272 1720.20447
1706.0 0.000586 1696.63440 1720.40454
1716.0 0.000583 1697.20410 1721.40857
1752.0 0.000571 1697.74878 1721.82068
1746.0 0.000573 1698.26672 1722.37854
1706.0 0.000586 1698.75488 1724.44226
1694.0 0.000590 1699.21143 1724.72778
1700.0 0.000588 1699.63367 1724.84241
1680.0 0.000595 1700.01953 1725.04810
1736.0 0.000576 1700.36694 1724.66553
1679.0 0.000596 1700.67346 1724.56982
1711.0 0.000584 1700.93726 1724.75476
1592.0 0.000628 1701.15588 1724.60205
1733.0 0.000577 1701.32788 1724.78503
1744.0 0.000573 1701.45093 1725.06445
1704.0 0.000587 1701.52332 1724.34900
1680.0 0.000595 1701.54358 1724.40869
1727.0 0.000579 1701.50977 1725.39441
1794.0 0.000557 1701.42053 1725.47302
1753.0 0.000570 1701.27441 1725.36536
1732.0 0.000577 1701.07031 1724.36096
1695.0 0.000590 1700.80676 1723.92444
1717.0 0.000582 1700.48303 1722.39624
1675.0 0.000597 1700.09814 1722.01526
1689.0 0.000592 1699.65125 1714.70337
1729.0 0.000578 1699.14172 1714.34668
1751.0 0.000571 1698.56934 1715.53040
1692.0 0.000591 1697.93347 1715.11963
1696.0 0.000590 1697.23450 1714.60754
1731.0 0.000578 1696.47192 1705.49023
1701.0 0.000588 1695.64648 1704.09412
1669.0 0.000599 1694.75818 1703.53186
1718.0 0.000582 1693.80798 1702.55872
1740.0 0.000575 1692.79651 1708.85767
1735.0 0.000576 1691.72437 1707.34729
1711.0 0.000584 1690.59338 1702.83276
1709.0 0.000585 1689.40417 1700.86243
1712.0 0.000584 1688.15906 1699.51624
1708.0 0.000585 1686.85901 1699.46252
1690.0 0.000592 1685.50684 1699.11877
1681.0 0.000595 1684.10437 1695.77380
1658.0 0.000603 1682.65320 1694.14258
1651.0 0.000606 1681.15710 1692.80542
1713.0 0.000584 1679.61780 1691.82947
1700.0 0.000588 1678.03906 1693.91687
1720.0 0.000581 1676.42322 1693.27393
1789.0 0.000559 1674.77441 1691.84033
1785.0 0.000560 1673.09534 1689.86584
1747.0 0.000572 1671.39063 1691.53687
1687.0 0.000593 1669.66370 1690.29150
1630.0 0.000613 1667.91785 1689.21399
1695.0 0.000590 1666.15845 1688.78369
1728.0 0.000579 1664.38855 1687.67346
1810.0 0.000552 1662.61401 1686.30237
1686.0 0.000593 1660.83813 1692.44873
1657.0 0.000604 1659.06665 1691.03503
1670.0 0.000599 1657.30334 1690.03455
1605.0 0.000623 1655.55432 1689.25720
1647.0 0.000607 1653.82385 1687.89124
1646.0 0.000608 1652.11633 1686.53198
1602.0 0.000624 1650.43811 1686.85242
1706.0 0.000586 1648.79309 1685.68689
1710.0 0.000585 1647.18738 1684.43420
1691.0 0.000591 1645.62500 1683.03967
1659.0 0.000603 1644.11206 1682.52136
1723.0 0.000580 1642.65295 1677.70972
1620.0 0.000617 1641.25208 1685.10474
1674.0 0.000597 1639.91528 1684.33728
1715.0 0.000583 1638.64624 1683.62915
1731.0 0.000578 1637.45032 1683.30774
1685.0 0.000593 1636.33093 1682.74231
1731.0 0.000578 1635.29285 1682.23828
1724.0 0.000580 1634.33960 1681.66125
1671.0 0.000598 1633.47498 1681.27820
1720.0 0.000581 1632.70227 1680.87744
1662.0 0.000602 1632.02405 1680.62915
1693.0 0.000591 1631.44336 1678.54504
1689.0 0.000592 1630.96216 1677.09534
1677.0 0.000596 1630.58264 1679.64709
1669.0 0.000599 1630.30579 1679.89050
1654.0 0.000605 1630.13245 1679.71472
1680.0 0.000595 1630.06348 1683.08374
1716.0 0.000583 1630.09802 1683.62134
1704.0 0.000587 1630.23596 1684.16150
1685.0 0.000593 1630.47571 1684.70557
1656.0 0.000604 1630.81531 1680.73132
1650.0 0.000606 1631.25232 1682.03113
1695.0 0.000590 1631.78320 1682.81689
1676.0 0.000597 1632.40466 1682.80542
1636.0 0.000611 1633.11108 1683.66956
1669.0 0.000599 1633.89771 1684.58301
1697.0 0.000589 1634.75842 1685.57251
1696.0 0.000590 1635.68604 1688.00757
1696.0 0.000590 1636.67346 1686.31104
1723.0 0.000580 1637.71155 1687.53711
1747.0 0.000572 1638.79199 1690.31104
1688.0 0.000592 1639.90393 1687.70093
1729.0 0.000578 1641.03772 1686.99768
1781.0 0.000561 1642.18091 1688.12634
1703.0 0.000587 1643.32202 1690.05408
1712.0 0.000584 1644.44861 1690.86951
1671.0 0.000598 1645.54663 1692.16089
1684.0 0.000594 1646.60278 1693.11462
1705.0 0.000587 1647.60181 1694.17285
1642.0 0.000609 1648.52966 1696.14246
1665.0 0.000601 1649.37036 1696.69153
1610.0 0.000621 1650.10901 1697.50647
1732.0 0.000577 1650.72900 1698.85046
1718.0 0.000582 1651.21533 1697.35071
1687.0 0.000593 1651.55200 1697.69238
1717.0 0.000582 1651.72363 1697.89307
1666.0 0.000600 1651.71497 1697.88782
1705.0 0.000587 1651.51184 1697.53833
1743.0 0.000574 1651.10034 1697.15601
1676.0 0.000597 1650.46814 1696.50781
1712.0 0.000584 1649.60364 1695.47961
1649.0 0.000606 1648.49670 1694.99146
1657.0 0.000604 1647.14026 1691.28638
1687.0 0.000593 1645.52734 1689.55005
1689.0 0.000592 1643.65613 1687.70972
1655.0 0.000604 1641.52466 1685.54443
1641.0 0.000609 1639.13794 1691.25537
1627.0 0.000615 1636.50073 1688.65088
1705.0 0.000587 1633.62634 1685.90723
1757.0 0.000569 1630.52991 1683.63525
1651.0 0.000606 1627.23132 1680.43896
1633.0 0.000612 1623.76086 1675.32825
1657.0 0.000604 1620.14990 1671.84229
1673.0 0.000598 1616.44312 1668.40015
1657.0 0.000604 1612.68713 1663.64124
1607.0 0.000622 1608.94397 1659.56421
1626.0 0.000615 1605.27954 1656.36414
1659.0 0.000603 1601.77625 1657.09595
1722.0 0.000581 1598.52429 1654.17908
1751.0 0.000571 1595.62708 1651.31885
1737.0 0.000576 1593.20557 1648.50720
1684.0 0.000594 1591.39172 1647.20911
1634.0 0.000612 1590.33801 1645.70325
1645.0 0.000608 1590.21216 1647.26746
1644.0 0.000608 1591.20288 1649.01721
1674.0 0.000597 1593.51929 1651.66431
1719.0 0.000582 1597.39539 1656.17664
1678.0 0.000596 1603.08533 1662.14063
1675.0 0.000597 1610.87708 1670.44373
1667.0 0.000600 1621.07690 1681.09583
1649.0 0.000606 1634.03540 1694.84778
1647.0 0.000607 1650.11841 1711.41125
1645.0 . . .
_pd_meas_number_of_points        3800
_pd_proc_number_of_points        3800

_reflns_number_total             1515
_reflns_limit_h_min              0
_reflns_limit_h_max              13
_reflns_limit_k_min              0
_reflns_limit_k_max              10
_reflns_limit_l_min              -6
_reflns_limit_l_max              5
_reflns_d_resolution_high        1.203
_reflns_d_resolution_low         15.102
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
