# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2017

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 1513036'
_audit_update_record             
;
2016-12-18 deposited with the CCDC.
2017-01-19 downloaded from the CCDC.
;

# start Validation Reply Form
_vrf_PLAT043_1                   
;
PROBLEM: Calculated and Reported Mol. Weight Differ by ..      189.82 Check
RESPONSE: Hydrogen atoms on the water molecules and ammonium ions are not 
present in the refined structure but they obvioulsy must be counted.
;

_vrf_PLAT201_1                   
;
PROBLEM: Isotropic non-H Atoms in Main Residue(s) ....... 5 Report 
RESPONSE: Due to the large structure and the existence of a large 
 amount of weight atoms, the intensity data are not very good, 
 leading to the ADP max/min ratio of some O atoms and water O atoms, 
 and it is very difficult to refine this large structure, therefore,
 in the final refinement, all the W, Sb, Mn and Na atoms were 
 refined anisotropically; some O atoms and water O atoms were 
 refined isotropically.
;

_vrf_PLAT220_1                   
;
PROBLEM: Non-Solvent Resd 1  Mn   Ueq(max)/Ueq(min) Range       10.0 Ratio
RESPONSE: In this structure, the Mn6 atom is disordered over two positions 
(Mn6 and Mn6'), the Mn6 position is refined anisotropically while 
the Mn6' position is refined isotropically, which lead to the large
of the Mn Ueq(max)/Ueq(min) range. For Non-Solvent Resd 1  O  
Ueq(max)/Ueq(min) Range 8.0 Ratio, tn polyoxometalate (POM) compounds, 
the Ueq of oxygen atoms in the POM skeleton is small due to multiple 
covalent bonds, whereas the Ueq of these discrete water oxygen atoms 
is biggish without the constraint of covalent bonds. 
;

_vrf_PLAT306_1                   
;
PROBLEM: Isolated Oxygen Atom (H-atoms Missing ?) .......  O9W Check
RESPONSE: The hydrogen atoms of the water molecules could not be directly 
 located from the difference Fourier maps because of the presence of too many
 heavy atoms in the structure.
;

_vrf_PLAT342_1                   
;
PROBLEM: Low Bond Precision on C-C Bonds ............... 0.025 Ang.
RESPONSE: The alert derives from shading of reciprocal space
 by the pressure cell, and it is unavoidable in the high pressure
 crystal structure determination.
;
# end Validation Reply Form


_audit_creation_date             2016-12-18
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_chemical_name_common            ?
_chemical_name_systematic        
;
 ? 
;
_chemical_formula_moiety         '0.5(C12 Mn18 Na4 O212 Sb4 W36), 17(O)'
_chemical_formula_sum            'C6 H94 Mn9 Na2 O123 Sb2 W18'
_chemical_formula_weight         6228.05
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x, y, -z+1/2'
3 'x+1/2, y+1/2, z'
4 '-x+1/2, y+1/2, -z+1/2'
5 '-x, -y, -z'
6 'x, -y, z-1/2'
7 '-x+1/2, -y+1/2, -z'
8 'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   18.061(4)
_cell_length_b                   27.381(6)
_cell_length_c                   23.825(5)
_cell_angle_alpha                90.00
_cell_angle_beta                 106.140(4)
_cell_angle_gamma                90.00
_cell_volume                     11318(4)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    6984
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.083
_cell_measurement_theta_min      2.522
_exptl_absorpt_coefficient_mu    19.777
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.3707
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.1559 before and 0.0610 after correction. The Ratio of minimum to maximum transmission is 0.4971. The λ/2 correction factor is 0.0015.'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    3.655
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       rhombus
_exptl_crystal_F_000             11180
_exptl_crystal_size_max          0.48
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.22
_exptl_special_details           
;
Because of the large structure of 1 and the existence of a 
large amount of weight atoms, the intensity data are not 
very good, leading to the ADP max/min ratio of some atoms, and 
it is very difficult to refine this large structure, therefore, 
some unit-occupancy atoms have been refined isotropically and
restrainedly refined. The ISOR instruction is used for 
C3 and MN6 atoms. The Mn6 atom is disordered over two positions 
(Mn6 and Mn6'), the Mn6 position is refined anisotropically while 
the Mn6' position is refined isotropically, which lead to the large
of the Mn Ueq(max)/Ueq(min) range. O35, O3W, O5W, O7W-O8W, 
O10W-O13W and O15W-O25W are refined isostropicallly. 
658 parameters and 12 restraints are used in the refinement. 
;
_diffrn_reflns_av_R_equivalents  0.0621
_diffrn_reflns_av_unetI/netI     0.0696
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            28233
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.73
_diffrn_ambient_temperature      296.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'fine-focus sealed tube'
_diffrn_standards_decay_%        ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_number         ?
_reflns_number_gt                7145
_reflns_number_total             9863
_reflns_threshold_expression     >2sigma(I)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XH (Sheldrick, 2008)'
_computing_structure_solution    'SIR2004 (Burla et al., 2007)'
_refine_diff_density_max         2.774
_refine_diff_density_min         -2.631
_refine_diff_density_rms         0.372
_refine_ls_extinction_coef       ?
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     658
_refine_ls_number_reflns         9863
_refine_ls_number_restraints     12
_refine_ls_R_factor_all          0.0727
_refine_ls_R_factor_gt           0.0459
_refine_ls_restrained_S_all      1.023
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0665P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1148
_refine_ls_wR_factor_ref         0.1243
_refine_special_details          
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;
_olex2_refinement_description    
;
1. Uiso/Uaniso restraints and constraints
Uanis(C3) \\sim Ueq, Uanis(Mn6) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
2. Others
 Fixed Sof: Mn6(0.25) Mn6'(0.25) O8W(0.15) O8W'(0.35) O15W(0.5) O16W(0.5)
 O17W(0.5) O18W(0.5) O20W(0.5) O24W(0.5)
 Fixed Uiso: O7W(0.07907) O10W(0.09602) O11W(0.09866) O12W(0.09785)
 O13W(0.09083) O19W(0.08711)
;
_atom_sites_solution_hydrogens   constr
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_site_symmetry_order
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Sb1 Sb 0.36670(6) -0.30138(3) 0.25685(4) 0.0131(2) Uani 1 d . . 1 . . .
Na1 Na 0.4546(4) -0.2762(2) 0.5763(3) 0.0271(14) Uani 1 d . . 1 . . .
W1 W 0.36554(4) -0.41128(2) 0.33920(3) 0.01788(15) Uani 1 d . . 1 . . .
W2 W 0.29451(4) -0.41087(2) 0.17674(3) 0.01911(16) Uani 1 d . . 1 . . .
W3 W 0.26401(4) -0.30521(2) 0.10502(3) 0.01747(15) Uani 1 d . . 1 . . .
W4 W 0.30070(4) -0.18806(2) 0.18570(3) 0.01854(15) Uani 1 d . . 1 . . .
W5 W 0.36468(4) -0.18808(2) 0.33153(3) 0.02083(16) Uani 1 d . . 1 . . .
W6 W 0.39903(4) -0.30560(2) 0.41217(3) 0.01936(16) Uani 1 d . . 1 . . .
W7 W 0.21708(4) -0.33955(2) 0.34651(3) 0.02115(16) Uani 1 d . . 1 . . .
W8 W 0.14608(4) -0.33915(2) 0.18450(3) 0.02205(16) Uani 1 d . . 1 . . .
W9 W 0.18263(4) -0.22193(2) 0.26562(3) 0.02193(16) Uani 1 d . . 1 . . .
Mn1 Mn 0.55729(13) -0.23980(7) 0.37900(10) 0.0183(5) Uani 1 d . . 1 . . .
Mn2 Mn 0.5000 -0.17993(11) 0.2500 0.0197(7) Uani 1 d . . 2 S T P
Mn3 Mn 0.5000 -0.42056(12) 0.2500 0.0227(7) Uani 1 d . . 2 S T P
Mn4 Mn 0.44268(14) -0.36476(8) 0.12149(10) 0.0223(5) Uani 1 d . . 1 . . .
Mn5 Mn 0.39132(17) -0.54480(9) 0.39647(11) 0.0360(7) Uani 1 d . . 1 . . .
Mn6 Mn 0.5000 0.0275(4) 0.2500 0.069(4) Uani 0.50 d . . 2 S TU P
Mn6' Mn 0.4913(6) 0.0290(3) 0.2218(4) 0.0051(19) Uiso 0.25 d . . 1 . . .
O1 O 0.3809(6) -0.4705(3) 0.3653(4) 0.021(2) Uani 1 d . . 1 . . .
O2 O 0.4077(6) -0.3768(3) 0.4135(4) 0.018(2) Uani 1 d . . 1 . . .
O3 O 0.3319(5) -0.3316(3) 0.3212(4) 0.016(2) Uani 1 d . . 1 . . .
O4 O 0.2633(6) -0.4022(4) 0.3546(4) 0.026(2) Uani 1 d . . 1 . . .
O5 O 0.4517(6) -0.3953(3) 0.3181(4) 0.021(2) Uani 1 d . . 1 . . .
O6 O 0.3105(6) -0.4222(3) 0.2589(4) 0.020(2) Uani 1 d . . 1 . . .
O7 O 0.2885(6) -0.4700(4) 0.1507(4) 0.029(3) Uani 1 d . . 1 . . .
O8 O 0.1849(6) -0.4025(3) 0.1718(5) 0.027(3) Uani 1 d . . 1 . . .
O9 O 0.3970(6) -0.3950(3) 0.1905(4) 0.019(2) Uani 1 d . . 1 . . .
O10 O 0.2777(5) -0.3311(3) 0.1981(4) 0.017(2) Uani 1 d . . 1 . . .
O11 O 0.2711(6) -0.3773(3) 0.1027(4) 0.025(2) Uani 1 d . . 1 . . .
O12 O 0.2391(7) -0.2954(4) 0.0312(4) 0.028(3) Uani 1 d . . 1 . . .
O13 O 0.1565(6) -0.3169(4) 0.1119(5) 0.027(3) Uani 1 d . . 1 . . .
O14 O 0.3685(5) -0.3014(3) 0.1281(4) 0.015(2) Uani 1 d . . 1 . . .
O15 O 0.2553(6) -0.2406(3) 0.1340(4) 0.020(2) Uani 1 d . . 1 . . .
O16 O 0.2883(6) -0.1393(4) 0.1379(5) 0.027(3) Uani 1 d . . 1 . . .
O17 O 0.2002(6) -0.1819(3) 0.2047(4) 0.020(2) Uani 1 d . . 1 . . .
O18 O 0.3055(5) -0.2420(3) 0.2604(4) 0.012(2) Uani 1 d . . 1 . . .
O19 O 0.3970(5) -0.2114(3) 0.1897(4) 0.018(2) Uani 1 d . . 1 . . .
O20 O 0.3422(6) -0.1520(3) 0.2574(5) 0.027(3) Uani 1 d . . 1 . . .
O21 O 0.3944(7) -0.1401(4) 0.3803(5) 0.032(3) Uani 1 d . . 1 . . .
O22 O 0.2511(6) -0.1829(4) 0.3218(5) 0.026(3) Uani 1 d . . 1 . . .
O23 O 0.4546(6) -0.2114(4) 0.3189(4) 0.023(2) Uani 1 d . . 1 . . .
O24 O 0.3660(6) -0.2401(4) 0.3838(4) 0.025(2) Uani 1 d . . 1 . . .
O25 O 0.4369(7) -0.2948(4) 0.4849(4) 0.029(3) Uani 1 d . . 1 . . .
O26 O 0.4811(6) -0.3015(3) 0.3811(4) 0.016(2) Uani 1 d . . 1 . . .
O27 O 0.2909(6) -0.3173(4) 0.4147(4) 0.024(2) Uani 1 d . . 1 . . .
O28 O 0.1409(6) -0.3517(4) 0.3747(5) 0.035(3) Uani 1 d . . 1 . . .
O29 O 0.1966(6) -0.2737(4) 0.3215(4) 0.027(3) Uani 1 d . . 1 . . .
O30 O 0.1705(6) -0.3556(4) 0.2653(4) 0.028(3) Uani 1 d . . 1 . . .
O31 O 0.0481(6) -0.3503(4) 0.1630(5) 0.033(3) Uani 1 d . . 1 . . .
O32 O 0.1471(6) -0.2732(4) 0.2094(4) 0.021(2) Uani 1 d . . 1 . . .
O33 O 0.0943(7) -0.1984(4) 0.2677(5) 0.040(3) Uani 1 d . . 1 . . .
O34 O 0.5251(7) -0.1155(4) 0.3083(5) 0.037(3) Uani 1 d . . 1 . . .
O35 O 0.5243(9) -0.0340(6) 0.3112(7) 0.075(5) Uiso 1 d . . 1 . . .
O36 O 0.4054(6) -0.3504(4) 0.0276(4) 0.028(3) Uani 1 d . . 1 . . .
O37 O 0.4254(7) -0.4379(4) 0.0777(5) 0.034(3) Uani 1 d . . 1 . . .
O38 O 0.4061(9) -0.4724(4) -0.0113(5) 0.050(4) Uani 1 d . . 1 . . .
O39 O 0.3965(9) -0.3840(4) -0.0604(5) 0.046(4) Uani 1 d . . 1 . . .
O1W O 0.5991(6) -0.2503(4) 0.4744(5) 0.034(3) Uani 1 d . . 1 . . .
O2W O 0.5749(7) -0.1646(4) 0.4134(5) 0.042(3) Uani 1 d . . 1 . . .
O3W O 0.5000 -0.4974(10) 0.2500 0.094(8) Uiso 1 d . . 2 S T P
O4W O 0.2682(8) -0.5468(4) 0.3736(8) 0.072(5) Uani 1 d . . 1 . . .
O5W O 0.5133(11) -0.5384(7) 0.4056(8) 0.096(6) Uiso 1 d . . 1 . . .
O6W O 0.3842(10) -0.5934(5) 0.3206(6) 0.070(5) Uani 1 d . . 1 . . .
O7W O 0.3822(10) 0.0315(6) 0.2561(7) 0.079 Uiso 1 d . . 1 . . .
O8W O 0.5000 0.108(3) 0.2500 0.07(2) Uiso 0.30 d . . 2 S T P
O8W' O 0.535(2) 0.0913(12) 0.2812(15) 0.034(8) Uiso 0.35 d . . 1 . . .
O9W O 0.5780(8) -0.2903(5) 0.5960(6) 0.053(4) Uani 1 d . . 1 . . .
O10W O 0.4405(12) -0.2002(7) 0.5526(9) 0.096 Uiso 1 d . . 1 . . .
O11W O 0.4739(11) -0.2437(7) 0.6597(8) 0.099 Uiso 1 d . . 1 . . .
O12W O 0.3181(12) -0.2744(7) 0.5697(8) 0.098 Uiso 1 d . . 1 . . .
O13W O 0.4486(11) -0.3479(7) 0.6090(8) 0.091 Uiso 1 d . . 1 . . .
O14W O 0.5285(9) -0.2281(6) 0.5454(6) 0.071(5) Uani 1 d . . 1 . . .
O15W O 0.5724(17) -0.0378(11) 0.4411(12) 0.062(8) Uiso 0.50 d . . 1 . . .
O16W O 0.564(2) 0.0588(13) 0.0773(15) 0.087(11) Uiso 0.50 d . . 1 . . .
O17W O 0.878(2) 0.0811(12) 0.5091(14) 0.079(10) Uiso 0.50 d . . 1 . . .
O18W O 0.6871(18) 0.3911(11) 0.3722(13) 0.068(9) Uiso 0.50 d . . 1 . . .
O19W O 0.4543(11) 0.0623(6) 0.1412(8) 0.087 Uiso 1 d . . 1 . . .
O20W O 0.6346(17) 0.4498(10) 0.2832(12) 0.060(8) Uiso 0.50 d . . 1 . . .
O21W O 1.0285(14) 0.3525(9) 0.5127(10) 0.128(8) Uiso 1 d . . 1 . . .
O22W O 0.8018(12) 0.4464(7) 0.2585(8) 0.099(6) Uiso 1 d . . 1 . . .
O23W O 0.6958(11) 0.0309(7) 0.4112(8) 0.095(6) Uiso 1 d . . 1 . . .
O24W O 0.763(2) 0.0155(14) 0.5368(16) 0.094(12) Uiso 0.50 d . . 1 . . .
O25W O 0.5000 0.0000 0.5000 0.095(8) Uiso 1 d . . 2 S T P
O26W O 0.7148(10) 0.0975(7) -0.0214(6) 0.083(5) Uani 1 d . . 1 . . .
O27W O 0.6558(9) 0.0405(5) 0.4868(6) 0.068(4) Uani 1 d . . 1 . . .
C1 C 0.4040(10) -0.3855(5) -0.0052(8) 0.034(4) Uani 1 d . . 1 . . .
C2 C 0.4145(10) -0.4373(5) 0.0249(7) 0.025(4) Uani 1 d . . 1 . . .
C3 C 0.5141(10) -0.0764(6) 0.2832(8) 0.036(4) Uani 1 d . . 1 . U .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb1 O3 1.993(9) . ?
Sb1 O10 1.988(9) . ?
Sb1 O18 1.980(9) . ?
Na1 O25 2.172(11) . ?
Na1 O9W 2.180(15) . ?
Na1 O10W 2.155(19) . ?
Na1 O11W 2.116(19) . ?
Na1 O12W 2.43(2) . ?
Na1 O13W 2.126(19) . ?
Na1 O14W 2.145(17) . ?
W1 O1 1.731(9) . ?
W1 O2 1.963(9) . ?
W1 O3 2.272(8) . ?
W1 O4 1.995(10) . ?
W1 O5 1.817(10) . ?
W1 O6 1.919(9) . ?
W2 O6 1.922(9) . ?
W2 O7 1.727(10) . ?
W2 O8 1.964(10) . ?
W2 O9 1.839(10) . ?
W2 O10 2.281(9) . ?
W2 O11 1.929(10) . ?
W3 O10 2.275(10) . ?
W3 O11 1.981(9) . ?
W3 O12 1.710(10) . ?
W3 O13 2.019(11) . ?
W3 O14 1.816(9) . ?
W3 O15 1.921(9) . ?
W4 O15 1.923(10) . ?
W4 O16 1.729(10) . ?
W4 O17 1.996(10) . ?
W4 O18 2.296(8) . ?
W4 O19 1.831(9) . ?
W4 O20 1.934(10) . ?
W5 O18 2.279(8) . ?
W5 O20 1.966(11) . ?
W5 O21 1.737(10) . ?
W5 O22 2.004(10) . ?
W5 O23 1.846(10) . ?
W5 O24 1.888(10) . ?
W6 O2 1.957(9) . ?
W6 O3 2.283(9) . ?
W6 O24 1.951(10) . ?
W6 O25 1.703(10) . ?
W6 O26 1.835(9) . ?
W6 O27 1.995(10) . ?
W7 O3 2.325(10) . ?
W7 O4 1.894(11) . ?
W7 O27 1.893(11) . ?
W7 O28 1.723(10) . ?
W7 O29 1.904(10) . ?
W7 O30 1.933(10) . ?
W8 O8 1.925(10) . ?
W8 O10 2.319(9) . ?
W8 O13 1.892(11) . ?
W8 O30 1.906(10) . ?
W8 O31 1.727(10) . ?
W8 O32 1.900(10) . ?
W9 O17 1.915(9) . ?
W9 O18 2.323(9) . ?
W9 O22 1.881(10) . ?
W9 O29 1.912(10) . ?
W9 O32 1.922(10) . ?
W9 O33 1.735(11) . ?
Mn1 O14 2.190(9) 2_655 ?
Mn1 O19 2.171(10) 2_655 ?
Mn1 O23 2.149(11) . ?
Mn1 O26 2.189(9) . ?
Mn1 O1W 2.206(11) . ?
Mn1 O2W 2.205(10) . ?
Mn2 O19 2.186(9) 2_655 ?
Mn2 O19 2.186(9) . ?
Mn2 O23 2.204(10) 2_655 ?
Mn2 O23 2.204(10) . ?
Mn2 O34 2.214(11) 2_655 ?
Mn2 O34 2.214(11) . ?
Mn3 O5 2.158(9) 2_655 ?
Mn3 O5 2.158(9) . ?
Mn3 O9 2.120(10) . ?
Mn3 O9 2.120(10) 2_655 ?
Mn3 O3W 2.10(3) . ?
Mn4 O5 2.210(10) 2_655 ?
Mn4 O9 2.197(10) . ?
Mn4 O14 2.223(9) . ?
Mn4 O26 2.224(9) 2_655 ?
Mn4 O36 2.184(10) . ?
Mn4 O37 2.238(10) . ?
Mn5 O1 2.156(9) . ?
Mn5 O38 2.190(11) 6_546 ?
Mn5 O39 2.195(11) 6_546 ?
Mn5 O4W 2.138(15) . ?
Mn5 O5W 2.16(2) . ?
Mn5 O6W 2.220(13) . ?
Mn6 Mn6' 0.648(10) 2_655 ?
Mn6 Mn6' 0.648(10) . ?
Mn6 O35 2.192(18) . ?
Mn6 O35 2.192(18) 2_655 ?
Mn6 O7W 2.174(17) . ?
Mn6 O7W 2.174(17) 2_655 ?
Mn6 O8W 2.21(8) . ?
Mn6 O8W' 1.94(3) 2_655 ?
Mn6 O8W' 1.94(3) . ?
Mn6' Mn6' 1.29(2) 2_655 ?
Mn6' O35 1.885(19) 2_655 ?
Mn6' O7W 2.33(2) . ?
Mn6' O7W 2.20(2) 2_655 ?
Mn6' O8W 2.26(8) . ?
Mn6' O8W' 1.77(3) 2_655 ?
Mn6' O8W' 2.22(3) . ?
Mn6' O19W 2.06(2) . ?
O5 Mn4 2.210(10) 2_655 ?
O14 Mn1 2.190(9) 2_655 ?
O19 Mn1 2.171(10) 2_655 ?
O26 Mn4 2.224(9) 2_655 ?
O34 C3 1.215(19) . ?
O35 Mn6' 1.885(19) 2_655 ?
O35 C3 1.33(2) . ?
O36 C1 1.234(18) . ?
O37 C2 1.220(18) . ?
O38 Mn5 2.190(11) 6_545 ?
O38 C2 1.271(18) . ?
O39 Mn5 2.195(11) 6_545 ?
O39 C1 1.28(2) . ?
O7W Mn6' 2.20(2) 2_655 ?
O8W Mn6' 2.26(8) 2_655 ?
O8W O8W' 0.96(4) . ?
O8W O8W' 0.96(4) 2_655 ?
O8W' Mn6' 1.77(3) 2_655 ?
O8W' O8W' 1.67(7) 2_655 ?
O10W O14W 1.81(2) . ?
C1 C2 1.58(2) . ?
C3 C3 1.52(4) 2_655 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O10 Sb1 O3 90.3(4) . . ?
O18 Sb1 O3 90.5(4) . . ?
O18 Sb1 O10 90.8(4) . . ?
O25 Na1 O9W 91.7(5) . . ?
O25 Na1 O12W 94.4(6) . . ?
O9W Na1 O12W 167.6(7) . . ?
O10W Na1 O25 89.4(6) . . ?
O10W Na1 O9W 105.4(7) . . ?
O10W Na1 O12W 85.4(7) . . ?
O11W Na1 O25 168.6(7) . . ?
O11W Na1 O9W 88.9(7) . . ?
O11W Na1 O10W 79.4(8) . . ?
O11W Na1 O12W 87.3(7) . . ?
O11W Na1 O13W 93.2(7) . . ?
O11W Na1 O14W 96.2(7) . . ?
O13W Na1 O25 98.2(6) . . ?
O13W Na1 O9W 84.9(7) . . ?
O13W Na1 O10W 167.0(8) . . ?
O13W Na1 O12W 83.6(7) . . ?
O13W Na1 O14W 142.4(7) . . ?
O14W Na1 O25 74.4(5) . . ?
O14W Na1 O9W 59.0(6) . . ?
O14W Na1 O10W 49.9(7) . . ?
O14W Na1 O12W 133.1(7) . . ?
O1 W1 O2 98.2(4) . . ?
O1 W1 O3 167.0(4) . . ?
O1 W1 O4 96.6(4) . . ?
O1 W1 O5 105.1(4) . . ?
O1 W1 O6 101.4(4) . . ?
O2 W1 O3 74.1(3) . . ?
O2 W1 O4 85.5(4) . . ?
O4 W1 O3 72.7(4) . . ?
O5 W1 O2 89.2(4) . . ?
O5 W1 O3 85.5(4) . . ?
O5 W1 O4 158.2(4) . . ?
O5 W1 O6 90.4(4) . . ?
O6 W1 O2 159.7(4) . . ?
O6 W1 O3 85.7(4) . . ?
O6 W1 O4 87.3(4) . . ?
O6 W2 O8 86.8(4) . . ?
O6 W2 O10 85.4(4) . . ?
O6 W2 O11 160.2(4) . . ?
O7 W2 O6 101.0(4) . . ?
O7 W2 O8 97.3(5) . . ?
O7 W2 O9 104.2(5) . . ?
O7 W2 O10 168.2(4) . . ?
O7 W2 O11 98.2(4) . . ?
O8 W2 O10 73.0(4) . . ?
O9 W2 O6 89.9(4) . . ?
O9 W2 O8 158.5(4) . . ?
O9 W2 O10 85.7(4) . . ?
O9 W2 O11 90.3(4) . . ?
O11 W2 O8 85.9(4) . . ?
O11 W2 O10 74.9(4) . . ?
O11 W3 O10 74.1(4) . . ?
O11 W3 O13 85.1(4) . . ?
O12 W3 O10 167.7(4) . . ?
O12 W3 O11 97.3(5) . . ?
O12 W3 O13 97.1(5) . . ?
O12 W3 O14 104.8(5) . . ?
O12 W3 O15 101.6(4) . . ?
O13 W3 O10 73.6(4) . . ?
O14 W3 O10 84.3(4) . . ?
O14 W3 O11 89.8(4) . . ?
O14 W3 O13 157.9(4) . . ?
O14 W3 O15 91.2(4) . . ?
O15 W3 O10 86.2(4) . . ?
O15 W3 O11 160.1(4) . . ?
O15 W3 O13 86.6(4) . . ?
O15 W4 O17 87.5(4) . . ?
O15 W4 O18 86.1(3) . . ?
O15 W4 O20 159.8(4) . . ?
O16 W4 O15 101.7(4) . . ?
O16 W4 O17 97.1(4) . . ?
O16 W4 O18 167.9(4) . . ?
O16 W4 O19 104.6(5) . . ?
O16 W4 O20 97.8(5) . . ?
O17 W4 O18 73.7(3) . . ?
O19 W4 O15 90.1(4) . . ?
O19 W4 O17 158.2(4) . . ?
O19 W4 O18 84.5(4) . . ?
O19 W4 O20 90.2(4) . . ?
O20 W4 O17 84.9(4) . . ?
O20 W4 O18 73.9(4) . . ?
O20 W5 O18 73.7(4) . . ?
O20 W5 O22 84.9(4) . . ?
O21 W5 O18 169.1(4) . . ?
O21 W5 O20 99.8(5) . . ?
O21 W5 O22 98.0(5) . . ?
O21 W5 O23 104.4(5) . . ?
O21 W5 O24 100.6(5) . . ?
O22 W5 O18 72.9(4) . . ?
O23 W5 O18 84.7(4) . . ?
O23 W5 O20 89.9(4) . . ?
O23 W5 O22 157.5(4) . . ?
O23 W5 O24 89.8(4) . . ?
O24 W5 O18 85.4(4) . . ?
O24 W5 O20 159.0(4) . . ?
O24 W5 O22 87.4(4) . . ?
O2 W6 O3 73.9(3) . . ?
O2 W6 O27 85.1(4) . . ?
O24 W6 O2 159.7(4) . . ?
O24 W6 O3 85.9(4) . . ?
O24 W6 O27 87.1(4) . . ?
O25 W6 O2 98.6(4) . . ?
O25 W6 O3 167.7(4) . . ?
O25 W6 O24 101.0(4) . . ?
O25 W6 O26 105.0(5) . . ?
O25 W6 O27 96.7(5) . . ?
O26 W6 O2 89.8(4) . . ?
O26 W6 O3 84.9(4) . . ?
O26 W6 O24 90.5(4) . . ?
O26 W6 O27 158.2(4) . . ?
O27 W6 O3 73.3(4) . . ?
O4 W7 O3 73.2(4) . . ?
O4 W7 O29 158.7(4) . . ?
O4 W7 O30 87.3(4) . . ?
O27 W7 O3 74.1(4) . . ?
O27 W7 O4 91.1(4) . . ?
O27 W7 O29 89.6(4) . . ?
O27 W7 O30 159.8(4) . . ?
O28 W7 O3 170.2(4) . . ?
O28 W7 O4 99.4(5) . . ?
O28 W7 O27 100.1(5) . . ?
O28 W7 O29 101.4(5) . . ?
O28 W7 O30 100.0(5) . . ?
O29 W7 O3 86.6(4) . . ?
O29 W7 O30 84.8(4) . . ?
O30 W7 O3 86.2(4) . . ?
O8 W8 O10 72.7(4) . . ?
O13 W8 O8 90.7(4) . . ?
O13 W8 O10 74.8(4) . . ?
O13 W8 O30 161.0(4) . . ?
O13 W8 O32 89.2(4) . . ?
O30 W8 O8 87.4(4) . . ?
O30 W8 O10 86.6(4) . . ?
O31 W8 O8 100.5(5) . . ?
O31 W8 O10 169.8(4) . . ?
O31 W8 O13 98.0(5) . . ?
O31 W8 O30 100.8(5) . . ?
O31 W8 O32 100.4(5) . . ?
O32 W8 O8 158.9(4) . . ?
O32 W8 O10 86.9(4) . . ?
O32 W8 O30 85.9(4) . . ?
O17 W9 O18 74.5(4) . . ?
O17 W9 O32 89.0(4) . . ?
O22 W9 O17 90.0(5) . . ?
O22 W9 O18 74.0(4) . . ?
O22 W9 O29 89.6(4) . . ?
O22 W9 O32 159.3(4) . . ?
O29 W9 O17 159.1(4) . . ?
O29 W9 O18 85.3(4) . . ?
O29 W9 O32 84.1(4) . . ?
O32 W9 O18 85.9(4) . . ?
O33 W9 O17 99.0(5) . . ?
O33 W9 O18 171.8(4) . . ?
O33 W9 O22 101.4(5) . . ?
O33 W9 O29 101.5(5) . . ?
O33 W9 O32 99.2(5) . . ?
O14 Mn1 O1W 86.4(4) 2_655 . ?
O14 Mn1 O2W 136.0(4) 2_655 . ?
O19 Mn1 O14 81.3(4) 2_655 2_655 ?
O19 Mn1 O26 131.8(4) 2_655 . ?
O19 Mn1 O1W 136.9(4) 2_655 . ?
O19 Mn1 O2W 84.3(4) 2_655 . ?
O23 Mn1 O14 131.4(4) . 2_655 ?
O23 Mn1 O19 78.8(4) . 2_655 ?
O23 Mn1 O26 82.1(4) . . ?
O23 Mn1 O1W 135.9(4) . . ?
O23 Mn1 O2W 85.3(4) . . ?
O26 Mn1 O14 79.0(3) . 2_655 ?
O26 Mn1 O1W 85.0(4) . . ?
O26 Mn1 O2W 137.6(4) . . ?
O2W Mn1 O1W 76.5(4) . . ?
O19 Mn2 O19 133.6(5) . 2_655 ?
O19 Mn2 O23 77.3(4) 2_655 . ?
O19 Mn2 O23 84.9(4) 2_655 2_655 ?
O19 Mn2 O23 84.9(4) . . ?
O19 Mn2 O23 77.3(4) . 2_655 ?
O19 Mn2 O34 135.6(4) 2_655 2_655 ?
O19 Mn2 O34 85.1(4) 2_655 . ?
O19 Mn2 O34 135.6(4) . . ?
O19 Mn2 O34 85.1(4) . 2_655 ?
O23 Mn2 O23 134.0(5) 2_655 . ?
O23 Mn2 O34 84.1(4) 2_655 2_655 ?
O23 Mn2 O34 84.1(4) . . ?
O23 Mn2 O34 136.5(4) 2_655 . ?
O23 Mn2 O34 136.5(4) . 2_655 ?
O34 Mn2 O34 74.2(7) 2_655 . ?
O5 Mn3 O5 142.6(5) 2_655 . ?
O9 Mn3 O5 81.6(4) . 2_655 ?
O9 Mn3 O5 86.2(4) 2_655 2_655 ?
O9 Mn3 O5 86.2(4) . . ?
O9 Mn3 O5 81.6(4) 2_655 . ?
O9 Mn3 O9 141.5(5) 2_655 . ?
O3W Mn3 O5 108.7(2) . . ?
O3W Mn3 O5 108.7(2) . 2_655 ?
O3W Mn3 O9 109.2(3) . . ?
O3W Mn3 O9 109.2(3) . 2_655 ?
O5 Mn4 O14 132.6(3) 2_655 . ?
O5 Mn4 O26 83.3(4) 2_655 2_655 ?
O5 Mn4 O37 87.0(4) 2_655 . ?
O9 Mn4 O5 78.8(4) . 2_655 ?
O9 Mn4 O14 83.3(3) . . ?
O9 Mn4 O26 132.8(4) . 2_655 ?
O9 Mn4 O37 88.7(4) . . ?
O14 Mn4 O26 77.5(3) . 2_655 ?
O14 Mn4 O37 136.2(4) . . ?
O26 Mn4 O37 133.7(4) 2_655 . ?
O36 Mn4 O5 134.4(4) . 2_655 ?
O36 Mn4 O9 139.5(4) . . ?
O36 Mn4 O14 84.9(4) . . ?
O36 Mn4 O26 81.3(4) . 2_655 ?
O36 Mn4 O37 73.8(4) . . ?
O1 Mn5 O38 96.7(4) . 6_546 ?
O1 Mn5 O39 171.2(4) . 6_546 ?
O1 Mn5 O5W 86.9(6) . . ?
O1 Mn5 O6W 107.8(5) . . ?
O38 Mn5 O39 75.2(4) 6_546 6_546 ?
O38 Mn5 O6W 155.5(5) 6_546 . ?
O39 Mn5 O6W 80.4(5) 6_546 . ?
O4W Mn5 O1 87.2(4) . . ?
O4W Mn5 O38 95.1(6) . 6_546 ?
O4W Mn5 O39 90.1(5) . 6_546 ?
O4W Mn5 O5W 170.8(7) . . ?
O4W Mn5 O6W 87.5(6) . . ?
O5W Mn5 O38 92.6(6) . 6_546 ?
O5W Mn5 O39 96.6(6) . 6_546 ?
O5W Mn5 O6W 87.5(7) . . ?
Mn6' Mn6 Mn6' 173(3) . 2_655 ?
Mn6' Mn6 O35 133.2(17) . . ?
Mn6' Mn6 O35 54.0(14) 2_655 . ?
Mn6' Mn6 O35 54.0(14) . 2_655 ?
Mn6' Mn6 O35 133.2(17) 2_655 2_655 ?
Mn6' Mn6 O7W 83.6(10) . 2_655 ?
Mn6' Mn6 O7W 83.6(10) 2_655 . ?
Mn6' Mn6 O7W 96.1(10) 2_655 2_655 ?
Mn6' Mn6 O7W 96.1(10) . . ?
Mn6' Mn6 O8W 86.4(15) 2_655 . ?
Mn6' Mn6 O8W 86.4(15) . . ?
Mn6' Mn6 O8W' 107.5(18) . . ?
Mn6' Mn6 O8W' 107.5(18) 2_655 2_655 ?
Mn6' Mn6 O8W' 65.5(16) 2_655 . ?
Mn6' Mn6 O8W' 65.5(16) . 2_655 ?
O35 Mn6 O35 79.5(9) 2_655 . ?
O35 Mn6 O8W 140.3(5) 2_655 . ?
O35 Mn6 O8W 140.3(5) . . ?
O7W Mn6 O35 93.7(6) 2_655 . ?
O7W Mn6 O35 93.7(6) . 2_655 ?
O7W Mn6 O35 90.8(6) 2_655 2_655 ?
O7W Mn6 O35 90.8(6) . . ?
O7W Mn6 O7W 174.2(10) . 2_655 ?
O7W Mn6 O8W 87.1(5) . . ?
O7W Mn6 O8W 87.1(5) 2_655 . ?
O8W' Mn6 O35 158.9(11) 2_655 . ?
O8W' Mn6 O35 117.0(11) 2_655 2_655 ?
O8W' Mn6 O35 158.9(11) . 2_655 ?
O8W' Mn6 O35 117.0(11) . . ?
O8W' Mn6 O7W 98.8(11) 2_655 2_655 ?
O8W' Mn6 O7W 98.8(11) . . ?
O8W' Mn6 O7W 75.8(11) 2_655 . ?
O8W' Mn6 O7W 75.8(11) . 2_655 ?
O8W' Mn6 O8W 25.6(11) . . ?
O8W' Mn6 O8W 25.6(11) 2_655 . ?
O8W' Mn6 O8W' 51(2) . 2_655 ?
Mn6 Mn6' Mn6' 3.6(15) . 2_655 ?
Mn6 Mn6' O35 109.9(16) . 2_655 ?
Mn6 Mn6' O7W 67.9(9) . . ?
Mn6 Mn6' O7W 79.4(11) . 2_655 ?
Mn6 Mn6' O8W 77.0(16) . . ?
Mn6 Mn6' O8W' 95.0(18) . 2_655 ?
Mn6 Mn6' O8W' 56.3(16) . . ?
Mn6 Mn6' O19W 156.5(17) . . ?
Mn6' Mn6' O35 113.5(6) 2_655 2_655 ?
Mn6' Mn6' O7W 79.3(11) 2_655 2_655 ?
Mn6' Mn6' O7W 67.7(9) 2_655 . ?
Mn6' Mn6' O8W 73.4(6) 2_655 . ?
Mn6' Mn6' O8W' 52.8(9) 2_655 . ?
Mn6' Mn6' O8W' 91.5(12) 2_655 2_655 ?
Mn6' Mn6' O19W 153.0(6) 2_655 . ?
O35 Mn6' O7W 97.5(8) 2_655 . ?
O35 Mn6' O7W 98.9(8) 2_655 2_655 ?
O35 Mn6' O8W 172.5(9) 2_655 . ?
O35 Mn6' O8W' 162.9(12) 2_655 . ?
O35 Mn6' O19W 92.5(8) 2_655 . ?
O7W Mn6' O7W 146.8(6) 2_655 . ?
O7W Mn6' O8W 85.2(6) 2_655 . ?
O7W Mn6' O8W' 70.0(10) 2_655 . ?
O8W Mn6' O7W 82.1(6) . . ?
O8W' Mn6' O35 149.2(14) 2_655 2_655 ?
O8W' Mn6' O7W 86.7(10) . . ?
O8W' Mn6' O7W 103.4(13) 2_655 2_655 ?
O8W' Mn6' O7W 74.8(12) 2_655 . ?
O8W' Mn6' O8W 24.6(9) . . ?
O8W' Mn6' O8W 23.6(14) 2_655 . ?
O8W' Mn6' O8W' 48(2) 2_655 . ?
O8W' Mn6' O19W 61.4(12) 2_655 . ?
O19W Mn6' O7W 104.8(8) . 2_655 ?
O19W Mn6' O7W 103.1(8) . . ?
O19W Mn6' O8W 80.3(8) . . ?
O19W Mn6' O8W' 102.7(11) . . ?
W1 O1 Mn5 176.0(6) . . ?
W6 O2 W1 117.1(4) . . ?
Sb1 O3 W1 114.8(4) . . ?
Sb1 O3 W6 113.7(4) . . ?
Sb1 O3 W7 137.1(4) . . ?
W1 O3 W6 94.4(3) . . ?
W1 O3 W7 94.2(3) . . ?
W6 O3 W7 93.4(3) . . ?
W7 O4 W1 119.9(5) . . ?
W1 O5 Mn3 133.4(5) . . ?
W1 O5 Mn4 124.2(5) . 2_655 ?
Mn3 O5 Mn4 98.9(4) . 2_655 ?
W1 O6 W2 151.6(5) . . ?
W8 O8 W2 120.1(5) . . ?
W2 O9 Mn3 134.0(5) . . ?
W2 O9 Mn4 121.6(5) . . ?
Mn3 O9 Mn4 100.5(4) . . ?
Sb1 O10 W2 114.7(4) . . ?
Sb1 O10 W3 114.0(4) . . ?
Sb1 O10 W8 137.2(5) . . ?
W2 O10 W8 94.2(3) . . ?
W3 O10 W2 93.8(3) . . ?
W3 O10 W8 93.6(4) . . ?
W2 O11 W3 116.6(5) . . ?
W8 O13 W3 117.9(5) . . ?
W3 O14 Mn1 128.9(5) . 2_655 ?
W3 O14 Mn4 122.0(4) . . ?
Mn1 O14 Mn4 101.7(4) 2_655 . ?
W3 O15 W4 148.9(6) . . ?
W9 O17 W4 118.4(5) . . ?
Sb1 O18 W4 113.4(4) . . ?
Sb1 O18 W5 114.3(4) . . ?
Sb1 O18 W9 138.6(4) . . ?
W4 O18 W9 93.4(3) . . ?
W5 O18 W4 93.9(3) . . ?
W5 O18 W9 93.7(3) . . ?
W4 O19 Mn1 129.8(5) . 2_655 ?
W4 O19 Mn2 121.2(5) . . ?
Mn1 O19 Mn2 101.8(4) 2_655 . ?
W4 O20 W5 118.0(5) . . ?
W9 O22 W5 119.5(5) . . ?
W5 O23 Mn1 130.7(5) . . ?
W5 O23 Mn2 120.8(5) . . ?
Mn1 O23 Mn2 101.9(4) . . ?
W5 O24 W6 150.3(6) . . ?
W6 O25 Na1 165.1(7) . . ?
W6 O26 Mn1 129.8(5) . . ?
W6 O26 Mn4 122.7(4) . 2_655 ?
Mn1 O26 Mn4 101.7(4) . 2_655 ?
W7 O27 W6 119.2(5) . . ?
W7 O29 W9 153.7(6) . . ?
W8 O30 W7 150.6(6) . . ?
W8 O32 W9 152.2(6) . . ?
C3 O34 Mn2 114.6(11) . . ?
Mn6' O35 Mn6 16.1(4) 2_655 . ?
C3 O35 Mn6 111.3(12) . . ?
C3 O35 Mn6' 127.4(14) . 2_655 ?
C1 O36 Mn4 117.1(10) . . ?
C2 O37 Mn4 115.6(9) . . ?
C2 O38 Mn5 118.4(10) . 6_545 ?
C1 O39 Mn5 115.4(9) . 6_545 ?
Mn6 O7W Mn6' 16.0(3) . . ?
Mn6 O7W Mn6' 17.0(3) . 2_655 ?
Mn6' O7W Mn6' 33.0(5) 2_655 . ?
Mn6 O8W Mn6' 16.6(6) . 2_655 ?
Mn6 O8W Mn6' 16.6(6) . . ?
Mn6' O8W Mn6' 33.2(13) . 2_655 ?
O8W' O8W Mn6 61(5) . . ?
O8W' O8W Mn6 61(5) 2_655 . ?
O8W' O8W Mn6' 75(6) 2_655 2_655 ?
O8W' O8W Mn6' 75(6) . . ?
O8W' O8W Mn6' 48(5) 2_655 . ?
O8W' O8W Mn6' 48(5) . 2_655 ?
O8W' O8W O8W' 122(10) 2_655 . ?
Mn6 O8W' Mn6' 16.2(4) . . ?
Mn6' O8W' Mn6 19.5(5) 2_655 . ?
Mn6' O8W' Mn6' 35.6(8) 2_655 . ?
O8W O8W' Mn6 93(6) . . ?
O8W O8W' Mn6' 80(5) . . ?
O8W O8W' Mn6' 109(6) . 2_655 ?
O8W O8W' O8W' 29(5) . 2_655 ?
O8W' O8W' Mn6 64.4(11) 2_655 . ?
O8W' O8W' Mn6' 80.3(13) 2_655 2_655 ?
O8W' O8W' Mn6' 51.8(10) 2_655 . ?
O14W O10W Na1 64.8(8) . . ?
O10W O14W Na1 65.3(8) . . ?
O36 C1 O39 127.0(15) . . ?
O36 C1 C2 115.6(15) . . ?
O39 C1 C2 117.3(13) . . ?
O37 C2 O38 130.2(15) . . ?
O37 C2 C1 116.4(13) . . ?
O38 C2 C1 113.3(14) . . ?
O34 C3 O35 122.8(17) . . ?
O34 C3 C3 118.3(10) . 2_655 ?
O35 C3 C3 118.9(11) . 2_655 ?

_olex2_submission_special_instructions 'No special instructions were received'

