# Electronic Supplementary Material (ESI) for Chemical Communications.
# This journal is © The Royal Society of Chemistry 2017

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_p-1
_database_code_depnum_ccdc_archive 'CCDC 1540839'
_audit_update_record             
;
2017-03-29 deposited with the CCDC.
2017-06-20 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/6
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C124 Cl12 Cr N7 O70 Si2 W18'
_chemical_formula_weight         6550.19

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.6870(3)
_cell_length_b                   18.7174(5)
_cell_length_c                   19.0467(4)
_cell_angle_alpha                106.2000(10)
_cell_angle_beta                 92.3250(10)
_cell_angle_gamma                97.7920(10)
_cell_volume                     4964.7(2)
_cell_formula_units_Z            1
_cell_measurement_temperature    123(2)
_cell_measurement_reflns_used    24083
_cell_measurement_theta_min      1.117
_cell_measurement_theta_max      29.488

_exptl_crystal_description       prism
_exptl_crystal_colour            green
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_density_diffrn    2.191
_exptl_crystal_F_000             2941
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.01
_exptl_crystal_size_mid          0.01
_exptl_crystal_size_min          0.01
_exptl_absorpt_coefficient_mu    10.675
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_correction_T_min  0.722
_exptl_absorpt_correction_T_max  0.900
_exptl_absorpt_process_details   'HKL2000 DENZO SCALEPACK'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      123(2)
_diffrn_radiation_wavelength     0.71069
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  CCD
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            27164
_diffrn_reflns_av_unetI/netI     0.0670
_diffrn_reflns_v_R_equivalents   ?
_diffrn_reflns_limit_h_min       ?
_diffrn_reflns_limit_h_max       ?
_diffrn_reflns_limit_k_min       ?
_diffrn_reflns_limit_k_max       ?
_diffrn_reflns_limit_l_min       ?
_diffrn_reflns_limit_l_max       ?
_diffrn_reflns_theta_min         1.117
_diffrn_reflns_theta_max         29.488
_diffrn_reflns_theta_full        25.240
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.982
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.982
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             27164
_reflns_number_gt                19236
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Rigaku CrystalClear'
_computing_cell_refinement       HKL2000
_computing_data_reduction        HKL2000
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-2014/6 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1538P)²+217.9433P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   none
_refine_ls_hydrogen_treatment    none
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         27164
_refine_ls_number_parameters     692
_refine_ls_number_restraints     8
_refine_ls_R_factor_all          0.1331
_refine_ls_R_factor_gt           0.0899
_refine_ls_wR_factor_ref         0.2950
_refine_ls_wR_factor_gt          0.2459
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_restrained_S_all      1.066
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
N1 N 0.7798(13) 0.6770(11) -0.3194(10) 0.045(4) Uiso 1 1 d . . . . .
C111 C 0.7759(19) 0.5950(15) -0.3544(15) 0.055(6) Uiso 1 1 d . . . . .
C112 C 0.807(2) 0.5734(18) -0.4349(18) 0.070(8) Uiso 1 1 d . . . . .
C113 C 0.796(3) 0.489(2) -0.464(2) 0.090(10) Uiso 1 1 d . . . . .
C114 C 0.818(3) 0.459(3) -0.545(3) 0.113(14) Uiso 1 1 d . . . . .
C121 C 0.8766(16) 0.7219(13) -0.3233(13) 0.045(5) Uiso 1 1 d . . . . .
C122 C 0.9541(16) 0.6917(14) -0.2980(13) 0.047(5) Uiso 1 1 d . . . . .
C123 C 1.0477(19) 0.7411(16) -0.3044(15) 0.059(6) Uiso 1 1 d . . . . .
C124 C 1.1281(17) 0.7090(14) -0.2812(14) 0.049(5) Uiso 1 1 d . . . . .
C131 C 0.7671(16) 0.6916(13) -0.2372(13) 0.045(5) Uiso 1 1 d . . . . .
C132 C 0.674(2) 0.6532(18) -0.2216(18) 0.070(8) Uiso 1 1 d . . . . .
C133 C 0.6710(17) 0.6598(14) -0.1414(13) 0.049(5) Uiso 1 1 d . . . . .
C134 C 0.591(2) 0.6080(18) -0.1245(17) 0.067(7) Uiso 1 1 d . . . . .
C141 C 0.7048(16) 0.7024(13) -0.3613(12) 0.044(5) Uiso 1 1 d . . . . .
C142 C 0.7029(19) 0.7872(15) -0.3344(15) 0.056(6) Uiso 1 1 d . . . . .
C143 C 0.618(2) 0.8078(17) -0.3761(16) 0.062(7) Uiso 1 1 d . . . . .
C144 C 0.624(2) 0.8905(18) -0.3626(17) 0.068(7) Uiso 1 1 d . . . . .
N2 N 0.7871(11) 0.4817(9) 0.1370(9) 0.035(3) Uiso 1 1 d . . . . .
C211 C 0.7386(15) 0.4095(12) 0.1491(12) 0.041(4) Uiso 1 1 d . . . . .
C212 C 0.7075(19) 0.4145(16) 0.2271(15) 0.059(6) Uiso 1 1 d . . . . .
C213 C 0.652(2) 0.3342(17) 0.2211(17) 0.065(7) Uiso 1 1 d . . . . .
C214 C 0.611(3) 0.337(3) 0.295(2) 0.101(12) Uiso 1 1 d . . . . .
C221 C 0.8712(14) 0.5156(11) 0.1915(11) 0.036(4) Uiso 1 1 d . . . . .
C222 C 0.9448(14) 0.4649(12) 0.1874(11) 0.038(4) Uiso 1 1 d . . . . .
C223 C 1.0293(15) 0.5092(13) 0.2381(12) 0.043(5) Uiso 1 1 d . . . . .
C224 C 1.009(2) 0.5322(18) 0.3154(18) 0.071(8) Uiso 1 1 d . . . . .
C231 C 0.7217(14) 0.5447(11) 0.1533(11) 0.036(4) Uiso 1 1 d . . . . .
C232 C 0.6333(17) 0.5224(14) 0.1021(13) 0.047(5) Uiso 1 1 d . . . . .
C233 C 0.5681(17) 0.5826(14) 0.1385(14) 0.050(5) Uiso 1 1 d . . . . .
C234 C 0.483(2) 0.5772(16) 0.0865(16) 0.060(7) Uiso 1 1 d . . . . .
C241 C 0.8108(15) 0.4639(12) 0.0585(12) 0.041(4) Uiso 1 1 d . . . . .
C242 C 0.8659(15) 0.5279(12) 0.0360(12) 0.039(4) Uiso 1 1 d . . . . .
C243 C 0.8766(16) 0.5049(13) -0.0469(12) 0.044(5) Uiso 1 1 d . . . . .
C244 C 0.7866(17) 0.4999(14) -0.0911(13) 0.049(5) Uiso 1 1 d . . . . .
N3 N 0.5469(13) 0.9673(11) 0.2100(10) 0.043(4) Uiso 1 1 d . . . . .
C311 C 0.5704(17) 0.8959(14) 0.1530(13) 0.047(5) Uiso 1 1 d . . . . .
C312 C 0.4883(18) 0.8450(15) 0.1078(15) 0.055(6) Uiso 1 1 d . . . . .
C313 C 0.519(2) 0.7789(17) 0.0510(16) 0.062(7) Uiso 1 1 d . . . . .
C314 C 0.437(2) 0.7293(19) 0.0040(18) 0.073(8) Uiso 1 1 d . . . . .
C321 C 0.4954(16) 1.0119(13) 0.1738(13) 0.045(5) Uiso 1 1 d . . . . .
C322 C 0.5459(17) 1.0395(14) 0.1160(14) 0.050(5) Uiso 1 1 d . . . . .
C323 C 0.4888(18) 1.0927(15) 0.0886(15) 0.055(6) Uiso 1 1 d . . . . .
C324 C 0.491(3) 1.167(2) 0.147(2) 0.085(10) Uiso 1 1 d . . . . .
C331 C 0.6411(15) 1.0120(13) 0.2501(12) 0.043(5) Uiso 1 1 d . . . . .
C332 C 0.6307(18) 1.0806(15) 0.3132(14) 0.053(6) Uiso 1 1 d . . . . .
C333 C 0.7273(16) 1.1311(14) 0.3439(13) 0.048(5) Uiso 1 1 d . . . . .
C334 C 0.721(3) 1.205(2) 0.404(2) 0.087(10) Uiso 1 1 d . . . . .
C341 C 0.4910(17) 0.9434(14) 0.2662(13) 0.049(5) Uiso 1 1 d . . . . .
C342 C 0.528(2) 0.8894(17) 0.3043(16) 0.062(7) Uiso 1 1 d . . . . .
C343 C 0.476(3) 0.893(2) 0.374(2) 0.083(10) Uiso 1 1 d . . . . .
C344 C 0.505(2) 0.8334(19) 0.4123(19) 0.075(8) Uiso 1 1 d . . . . .
N4 N 1.0000 1.0000 0.5000 0.114(5) Uiso 1 2 d S U P . .
C411 C 0.980(3) 1.064(3) 0.468(3) 0.114(5) Uiso 1 1 d . U . . .
C412 C 0.998(3) 1.145(3) 0.518(3) 0.114(5) Uiso 1 1 d . U . . .
C413 C 0.953(3) 1.199(3) 0.476(3) 0.114(5) Uiso 1 1 d . U . . .
C414 C 0.983(3) 1.276(3) 0.533(3) 0.114(5) Uiso 1 1 d . U . . .
C421 C 0.898(3) 0.964(3) 0.454(3) 0.114(5) Uiso 1 1 d . U . . .
C422 C 0.825(3) 0.978(3) 0.520(3) 0.114(5) Uiso 1 1 d . U . . .
C423 C 0.783(3) 1.054(3) 0.526(3) 0.114(5) Uiso 1 1 d . U . . .
C424 C 0.697(4) 1.019(3) 0.493(3) 0.116(5) Uiso 1 1 d . U . . .
O1 O 0.9247(8) 1.0689(6) 0.0591(6) 0.022(2) Uani 1 1 d . . . . .
O2 O 0.8906(8) 0.9481(7) -0.0643(6) 0.026(2) Uani 1 1 d . . . . .
O3 O 1.0629(8) 0.7812(7) -0.1048(7) 0.027(2) Uani 1 1 d . . . . .
O4 O 1.2160(9) 0.7887(7) -0.0089(7) 0.033(3) Uani 1 1 d . . . . .
O5 O 1.2674(9) 0.9815(8) 0.1877(7) 0.035(3) Uani 1 1 d . . . . .
O6 O 1.1502(8) 1.0895(7) 0.2079(7) 0.028(2) Uani 1 1 d . . . . .
O7 O 0.7931(9) 1.0942(7) 0.1601(7) 0.034(3) Uani 1 1 d . . . . .
O8 O 0.7257(9) 0.8515(8) -0.0926(8) 0.038(3) Uani 1 1 d . . . . .
O9 O 0.9241(10) 0.6571(8) -0.1281(8) 0.038(3) Uani 1 1 d . . . . .
O10 O 1.2128(9) 0.6828(7) 0.0692(8) 0.036(3) Uani 1 1 d . . . . .
O11 O 1.2718(9) 0.8947(8) 0.2862(8) 0.037(3) Uani 1 1 d . . . . .
O12 O 1.0549(9) 1.1145(7) 0.3347(7) 0.033(3) Uani 1 1 d . . . . .
O13 O 0.7741(8) 0.9614(7) 0.0454(6) 0.026(2) Uani 1 1 d . . . . .
O14 O 0.8959(8) 0.8042(6) -0.0635(6) 0.023(2) Uani 1 1 d . . . . .
O15 O 1.0611(8) 0.6842(7) -0.0204(6) 0.027(2) Uani 1 1 d . . . . .
O16 O 1.1983(9) 0.8344(7) 0.1387(7) 0.029(3) Uani 1 1 d . . . . .
O17 O 1.1483(8) 0.9944(7) 0.2937(6) 0.027(2) Uani 1 1 d . . . . .
O18 O 0.9637(9) 1.0560(7) 0.1915(6) 0.027(2) Uani 1 1 d . . . . .
O19 O 0.9447(7) 0.9335(6) 0.0616(6) 0.020(2) Uani 1 1 d . . . . .
O20 O 1.0435(8) 0.8210(6) 0.0423(6) 0.023(2) Uani 1 1 d . . . . .
O21 O 1.0773(7) 0.9401(6) 0.1653(6) 0.021(2) Uani 1 1 d . . . . .
O22 O 0.9289(8) 0.8395(6) 0.1454(6) 0.023(2) Uani 1 1 d . . . . .
O23 O 0.8233(8) 0.9549(7) 0.1803(6) 0.024(2) Uani 1 1 d . . . . .
O24 O 0.7817(8) 0.8177(7) 0.0389(7) 0.028(2) Uani 1 1 d . . . . .
O25 O 0.8835(9) 0.7096(7) 0.0162(7) 0.029(3) Uani 1 1 d . . . . .
O26 O 1.0530(8) 0.7257(7) 0.1315(7) 0.032(3) Uani 1 1 d . . . . .
O27 O 1.0860(9) 0.8384(8) 0.2504(7) 0.033(3) Uani 1 1 d . . . . .
O28 O 0.9600(8) 0.9677(7) 0.2788(6) 0.026(2) Uani 1 1 d . . . . .
O29 O 0.7602(8) 0.8130(7) 0.1791(6) 0.025(2) Uani 1 1 d . . . . .
O30 O 0.8688(8) 0.7030(7) 0.1521(6) 0.025(2) Uani 1 1 d . . . . .
O31 O 0.9076(8) 0.8225(7) 0.2749(7) 0.030(3) Uani 1 1 d . . . . .
O32 O 0.7810(10) 0.9225(8) 0.3136(8) 0.039(3) Uani 1 1 d . . . . .
O33 O 0.7039(10) 0.6811(8) 0.0648(9) 0.042(3) Uani 1 1 d . . . . .
O34 O 1.0001(9) 0.6965(8) 0.2597(8) 0.035(3) Uani 1 1 d . . . . .
Si1 Si 1.0022(3) 0.8838(2) 0.1026(2) 0.0197(8) Uani 1 1 d . . . . .
W1 W 0.85757(5) 1.02583(4) 0.12462(4) 0.02383(15) Uani 1 1 d . . . . .
W2 W 0.81666(5) 0.87798(4) -0.02745(4) 0.02748(16) Uani 1 1 d . . . . .
W3 W 0.96360(5) 0.72925(4) -0.05212(4) 0.03051(17) Uani 1 1 d . . . . .
W4 W 1.14845(7) 0.74992(5) 0.05934(5) 0.0421(2) Uani 1 1 d . . . . .
W5 W 1.18335(6) 0.90623(5) 0.22938(5) 0.0400(2) Uani 1 1 d . . . . .
W6 W 1.05390(5) 1.03955(5) 0.25739(4) 0.03443(18) Uani 1 1 d . . . . .
W7 W 0.85014(5) 0.89550(4) 0.24231(4) 0.02974(17) Uani 1 1 d . . . . .
W8 W 0.80140(5) 0.74947(4) 0.09216(4) 0.03081(17) Uani 1 1 d . . . . .
W9 W 0.98260(5) 0.75767(4) 0.20893(5) 0.03180(18) Uani 1 1 d . . . . .
Cr1 Cr 1.0000 1.0000 0.0000 0.0209(7) Uani 1 2 d S . P . .
O1W O 1.2892(10) 0.9388(8) 0.0444(8) 0.037(3) Uiso 1 1 d . . . . .
Cl11 Cl 0.4739(14) 0.6082(12) 0.5167(11) 0.181(7) Uiso 1 1 d . . . . .
Cl12 Cl 0.4929(14) 0.5157(12) 0.3457(11) 0.178(7) Uiso 1 1 d . . . . .
C11 C 0.504(4) 0.645(3) 0.441(3) 0.142(19) Uiso 1 1 d . . . . .
C12 C 0.476(4) 0.599(3) 0.374(3) 0.135(18) Uiso 1 1 d . . . . .
Cl21 Cl 0.7521(8) 0.6132(6) 0.3598(6) 0.098(3) Uiso 1 1 d . . . . .
Cl22 Cl 0.7402(9) 0.7762(7) 0.4645(7) 0.115(4) Uiso 1 1 d . . . . .
C21 C 0.793(2) 0.6974(17) 0.3373(16) 0.061(7) Uiso 1 1 d . . . . .
C22 C 0.741(2) 0.758(2) 0.3663(19) 0.077(9) Uiso 1 1 d . . . . .
Cl31 Cl 0.6296(8) 1.3004(6) 0.7585(6) 0.102(3) Uiso 1 1 d . . . . .
Cl32 Cl 0.7454(8) 1.3060(7) 0.6095(7) 0.108(3) Uiso 1 1 d . . . . .
C31 C 0.750(3) 1.305(2) 0.754(2) 0.091(11) Uiso 1 1 d . . . . .
C32 C 0.781(3) 1.270(2) 0.682(2) 0.085(10) Uiso 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
N1 C111 1.49(3) . ?
N1 C141 1.54(3) . ?
N1 C131 1.54(3) . ?
N1 C121 1.57(3) . ?
C111 C112 1.57(4) . ?
C112 C113 1.51(5) . ?
C113 C114 1.55(6) . ?
C121 C122 1.46(3) . ?
C122 C123 1.58(4) . ?
C123 C124 1.50(4) . ?
C131 C132 1.54(4) . ?
C132 C133 1.50(4) . ?
C133 C134 1.52(4) . ?
C141 C142 1.53(3) . ?
C142 C143 1.60(4) . ?
C143 C144 1.49(4) . ?
N2 C241 1.50(3) . ?
N2 C211 1.52(3) . ?
N2 C221 1.52(3) . ?
N2 C231 1.59(3) . ?
C211 C212 1.55(3) . ?
C212 C213 1.58(4) . ?
C213 C214 1.55(5) . ?
C221 C222 1.52(3) . ?
C222 C223 1.53(3) . ?
C223 C224 1.47(4) . ?
C231 C232 1.53(3) . ?
C232 C233 1.61(3) . ?
C233 C234 1.53(4) . ?
C241 C242 1.52(3) . ?
C242 C243 1.54(3) . ?
C243 C244 1.52(3) . ?
N3 C321 1.48(3) . ?
N3 C341 1.50(3) . ?
N3 C331 1.56(3) . ?
N3 C311 1.56(3) . ?
C311 C312 1.50(4) . ?
C312 C313 1.53(4) . ?
C313 C314 1.50(4) . ?
C321 C322 1.52(3) . ?
C322 C323 1.57(4) . ?
C323 C324 1.51(5) . ?
C331 C332 1.52(3) . ?
C332 C333 1.58(3) . ?
C333 C334 1.55(4) . ?
C341 C342 1.54(4) . ?
C342 C343 1.55(5) . ?
C343 C344 1.59(5) . ?
N4 C411 1.54(5) . ?
N4 C411 1.54(5) 2_776 ?
N4 C421 1.66(5) . ?
N4 C421 1.66(5) 2_776 ?
C411 C412 1.52(6) . ?
C411 C421 2.03(7) . ?
C412 C413 1.65(6) . ?
C413 C414 1.54(6) . ?
C421 C422 1.68(7) . ?
C422 C423 1.61(7) . ?
C423 C424 1.38(6) . ?
O1 W1 1.903(11) . ?
O1 Cr1 1.958(11) . ?
O2 W2 1.894(11) . ?
O2 Cr1 1.943(11) . ?
O3 W3 2.088(11) . ?
O4 W4 1.907(11) . ?
O5 W5 2.089(14) . ?
O6 W6 2.001(12) . ?
O7 W1 1.699(13) . ?
O8 W2 1.707(14) . ?
O9 W3 1.699(14) . ?
O10 W4 1.716(14) . ?
O11 W5 1.732(13) . ?
O12 W6 1.725(13) . ?
O13 W1 1.916(12) . ?
O13 W2 1.969(12) . ?
O14 W3 1.880(11) . ?
O14 W2 1.925(11) . ?
O15 W3 1.915(11) . ?
O15 W4 1.958(11) . ?
O16 W4 1.894(12) . ?
O16 W5 1.911(12) . ?
O17 W5 1.909(12) . ?
O17 W6 1.918(12) . ?
O18 W1 1.890(12) . ?
O18 W6 1.900(11) . ?
O19 Si1 1.659(12) . ?
O19 Cr1 2.050(11) . ?
O19 W1 2.373(10) . ?
O19 W2 2.392(10) . ?
O20 Si1 1.602(12) . ?
O20 W4 2.238(11) . ?
O20 W3 2.263(11) . ?
O21 Si1 1.621(11) . ?
O21 W5 2.205(11) . ?
O21 W6 2.250(11) . ?
O22 Si1 1.650(12) . ?
O22 W7 2.295(11) . ?
O22 W8 2.326(11) . ?
O22 W9 2.390(11) . ?
O23 W7 1.898(11) . ?
O23 W1 1.945(11) . ?
O24 W8 1.882(12) . ?
O24 W2 1.956(13) . ?
O25 W3 1.868(12) . ?
O25 W8 1.971(12) . ?
O26 W9 1.844(13) . ?
O26 W4 2.096(13) . ?
O27 W5 1.911(13) . ?
O27 W9 1.957(13) . ?
O28 W7 1.925(12) . ?
O28 W6 1.931(11) . ?
O29 W8 1.924(12) . ?
O29 W7 1.964(12) . ?
O30 W8 1.933(11) . ?
O30 W9 1.945(13) . ?
O31 W7 1.926(12) . ?
O31 W9 1.971(12) . ?
O32 W7 1.731(14) . ?
O33 W8 1.741(15) . ?
O34 W9 1.729(12) . ?
Cr1 O2 1.943(11) 2_775 ?
Cr1 O1 1.958(11) 2_775 ?
Cr1 O19 2.050(11) 2_775 ?
Cl11 C11 1.81(6) . ?
Cl12 C12 1.56(6) . ?
C11 C12 1.33(8) . ?
Cl21 C21 1.78(3) . ?
Cl22 C22 1.81(4) . ?
C21 C22 1.45(4) . ?
Cl31 C31 1.76(4) . ?
Cl32 C32 1.79(4) . ?
C31 C32 1.46(5) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C111 N1 C141 106.5(18) . . ?
C111 N1 C131 109.7(18) . . ?
C141 N1 C131 113.6(17) . . ?
C111 N1 C121 111.6(18) . . ?
C141 N1 C121 110.2(17) . . ?
C131 N1 C121 105.3(17) . . ?
N1 C111 C112 115(2) . . ?
C113 C112 C111 109(3) . . ?
C112 C113 C114 114(3) . . ?
C122 C121 N1 114.3(19) . . ?
C121 C122 C123 110(2) . . ?
C124 C123 C122 110(2) . . ?
C132 C131 N1 113(2) . . ?
C133 C132 C131 111(2) . . ?
C132 C133 C134 114(2) . . ?
C142 C141 N1 113.1(19) . . ?
C141 C142 C143 110(2) . . ?
C144 C143 C142 111(2) . . ?
C241 N2 C211 107.8(16) . . ?
C241 N2 C221 112.7(15) . . ?
C211 N2 C221 111.3(15) . . ?
C241 N2 C231 110.3(15) . . ?
C211 N2 C231 110.3(15) . . ?
C221 N2 C231 104.4(14) . . ?
N2 C211 C212 116.9(19) . . ?
C211 C212 C213 105(2) . . ?
C214 C213 C212 109(3) . . ?
C222 C221 N2 114.6(16) . . ?
C221 C222 C223 108.9(17) . . ?
C224 C223 C222 112(2) . . ?
C232 C231 N2 112.7(16) . . ?
C231 C232 C233 104.7(18) . . ?
C234 C233 C232 111(2) . . ?
N2 C241 C242 116.3(18) . . ?
C241 C242 C243 111.0(18) . . ?
C244 C243 C242 111.8(19) . . ?
C321 N3 C341 110.2(18) . . ?
C321 N3 C331 112.9(17) . . ?
C341 N3 C331 107.5(17) . . ?
C321 N3 C311 111.0(17) . . ?
C341 N3 C311 109.1(17) . . ?
C331 N3 C311 106.0(16) . . ?
C312 C311 N3 114(2) . . ?
C311 C312 C313 111(2) . . ?
C314 C313 C312 111(2) . . ?
N3 C321 C322 114.7(19) . . ?
C321 C322 C323 109(2) . . ?
C324 C323 C322 111(2) . . ?
C332 C331 N3 113.3(19) . . ?
C331 C332 C333 111(2) . . ?
C334 C333 C332 114(2) . . ?
N3 C341 C342 118(2) . . ?
C341 C342 C343 107(2) . . ?
C342 C343 C344 110(3) . . ?
C411 N4 C411 180(3) . 2_776 ?
C411 N4 C421 79(2) . . ?
C411 N4 C421 101(2) 2_776 . ?
C411 N4 C421 101(2) . 2_776 ?
C411 N4 C421 79(2) 2_776 2_776 ?
C421 N4 C421 180.0 . 2_776 ?
C412 C411 N4 119(4) . . ?
C412 C411 C421 142(4) . . ?
N4 C411 C421 53(2) . . ?
C411 C412 C413 109(4) . . ?
C414 C413 C412 99(4) . . ?
C422 C421 N4 103(3) . . ?
C422 C421 C411 106(3) . . ?
N4 C421 C411 48.1(19) . . ?
C421 C422 C423 110(4) . . ?
C424 C423 C422 96(4) . . ?
W1 O1 Cr1 112.2(5) . . ?
W2 O2 Cr1 113.4(6) . . ?
W1 O13 W2 120.2(6) . . ?
W3 O14 W2 151.6(7) . . ?
W3 O15 W4 116.2(6) . . ?
W4 O16 W5 149.6(7) . . ?
W5 O17 W6 118.0(6) . . ?
W1 O18 W6 153.6(7) . . ?
Si1 O19 Cr1 125.8(6) . . ?
Si1 O19 W1 123.6(6) . . ?
Cr1 O19 W1 92.6(4) . . ?
Si1 O19 W2 123.0(6) . . ?
Cr1 O19 W2 92.1(4) . . ?
W1 O19 W2 90.0(3) . . ?
Si1 O20 W4 128.4(6) . . ?
Si1 O20 W3 126.9(7) . . ?
W4 O20 W3 93.9(4) . . ?
Si1 O21 W5 126.0(6) . . ?
Si1 O21 W6 128.1(6) . . ?
W5 O21 W6 94.8(4) . . ?
Si1 O22 W7 125.8(6) . . ?
Si1 O22 W8 126.8(6) . . ?
W7 O22 W8 92.3(4) . . ?
Si1 O22 W9 119.3(6) . . ?
W7 O22 W9 92.1(4) . . ?
W8 O22 W9 90.8(4) . . ?
W7 O23 W1 153.3(6) . . ?
W8 O24 W2 153.9(7) . . ?
W3 O25 W8 147.3(7) . . ?
W9 O26 W4 150.2(7) . . ?
W5 O27 W9 145.6(7) . . ?
W7 O28 W6 146.3(6) . . ?
W8 O29 W7 118.0(6) . . ?
W8 O30 W9 120.0(6) . . ?
W7 O31 W9 120.0(6) . . ?
O20 Si1 O21 115.1(6) . . ?
O20 Si1 O22 107.3(6) . . ?
O21 Si1 O22 106.4(6) . . ?
O20 Si1 O19 109.8(6) . . ?
O21 Si1 O19 109.7(6) . . ?
O22 Si1 O19 108.2(6) . . ?
O7 W1 O18 101.6(6) . . ?
O7 W1 O1 100.6(5) . . ?
O18 W1 O1 88.5(5) . . ?
O7 W1 O13 100.7(6) . . ?
O18 W1 O13 157.3(5) . . ?
O1 W1 O13 91.3(5) . . ?
O7 W1 O23 101.5(5) . . ?
O18 W1 O23 83.7(5) . . ?
O1 W1 O23 157.6(5) . . ?
O13 W1 O23 87.9(5) . . ?
O7 W1 O19 173.2(5) . . ?
O18 W1 O19 82.7(4) . . ?
O1 W1 O19 74.1(4) . . ?
O13 W1 O19 75.5(4) . . ?
O23 W1 O19 84.1(4) . . ?
O8 W2 O2 99.7(6) . . ?
O8 W2 O14 103.1(6) . . ?
O2 W2 O14 90.4(5) . . ?
O8 W2 O24 102.8(6) . . ?
O2 W2 O24 157.5(5) . . ?
O14 W2 O24 84.3(5) . . ?
O8 W2 O13 101.0(6) . . ?
O2 W2 O13 90.0(5) . . ?
O14 W2 O13 155.5(5) . . ?
O24 W2 O13 86.0(5) . . ?
O8 W2 O19 171.4(5) . . ?
O2 W2 O19 73.4(4) . . ?
O14 W2 O19 82.5(4) . . ?
O24 W2 O19 84.2(4) . . ?
O13 W2 O19 74.1(4) . . ?
O9 W3 O25 101.7(6) . . ?
O9 W3 O14 101.8(6) . . ?
O25 W3 O14 89.1(5) . . ?
O9 W3 O15 96.8(6) . . ?
O25 W3 O15 95.3(5) . . ?
O14 W3 O15 159.5(5) . . ?
O9 W3 O3 94.6(6) . . ?
O25 W3 O3 163.2(5) . . ?
O14 W3 O3 84.0(5) . . ?
O15 W3 O3 86.3(5) . . ?
O9 W3 O20 168.9(5) . . ?
O25 W3 O20 86.7(5) . . ?
O14 W3 O20 85.4(4) . . ?
O15 W3 O20 75.0(5) . . ?
O3 W3 O20 77.5(4) . . ?
O10 W4 O16 102.5(6) . . ?
O10 W4 O4 100.5(6) . . ?
O16 W4 O4 92.1(6) . . ?
O10 W4 O15 97.1(5) . . ?
O16 W4 O15 159.4(5) . . ?
O4 W4 O15 90.7(6) . . ?
O10 W4 O26 93.4(6) . . ?
O16 W4 O26 85.5(5) . . ?
O4 W4 O26 166.1(5) . . ?
O15 W4 O26 86.9(5) . . ?
O10 W4 O20 169.9(5) . . ?
O16 W4 O20 85.0(5) . . ?
O4 W4 O20 85.8(5) . . ?
O15 W4 O20 74.8(5) . . ?
O26 W4 O20 80.4(4) . . ?
O11 W5 O17 98.2(6) . . ?
O11 W5 O16 101.6(6) . . ?
O17 W5 O16 158.0(5) . . ?
O11 W5 O27 99.0(6) . . ?
O17 W5 O27 94.8(6) . . ?
O16 W5 O27 91.4(5) . . ?
O11 W5 O5 94.1(6) . . ?
O17 W5 O5 85.0(5) . . ?
O16 W5 O5 84.2(5) . . ?
O27 W5 O5 166.8(5) . . ?
O11 W5 O21 170.9(5) . . ?
O17 W5 O21 74.2(5) . . ?
O16 W5 O21 85.1(5) . . ?
O27 W5 O21 86.7(5) . . ?
O5 W5 O21 80.5(5) . . ?
O12 W6 O18 103.0(6) . . ?
O12 W6 O17 97.3(6) . . ?
O18 W6 O17 159.7(5) . . ?
O12 W6 O28 99.8(5) . . ?
O18 W6 O28 87.4(5) . . ?
O17 W6 O28 90.4(5) . . ?
O12 W6 O6 97.1(5) . . ?
O18 W6 O6 88.0(5) . . ?
O17 W6 O6 88.3(5) . . ?
O28 W6 O6 163.1(5) . . ?
O12 W6 O21 169.8(5) . . ?
O18 W6 O21 86.7(5) . . ?
O17 W6 O21 73.0(4) . . ?
O28 W6 O21 83.7(4) . . ?
O6 W6 O21 79.8(4) . . ?
O32 W7 O23 103.1(5) . . ?
O32 W7 O28 100.5(6) . . ?
O23 W7 O28 87.0(5) . . ?
O32 W7 O31 99.4(6) . . ?
O23 W7 O31 157.6(5) . . ?
O28 W7 O31 89.1(5) . . ?
O32 W7 O29 97.0(6) . . ?
O23 W7 O29 88.1(5) . . ?
O28 W7 O29 162.4(5) . . ?
O31 W7 O29 89.0(5) . . ?
O32 W7 O22 170.2(6) . . ?
O23 W7 O22 82.3(4) . . ?
O28 W7 O22 87.8(5) . . ?
O31 W7 O22 75.4(5) . . ?
O29 W7 O22 74.9(4) . . ?
O33 W8 O24 102.9(6) . . ?
O33 W8 O29 99.4(6) . . ?
O24 W8 O29 91.5(5) . . ?
O33 W8 O30 99.1(6) . . ?
O24 W8 O30 157.4(5) . . ?
O29 W8 O30 89.8(5) . . ?
O33 W8 O25 100.7(6) . . ?
O24 W8 O25 85.9(5) . . ?
O29 W8 O25 159.8(5) . . ?
O30 W8 O25 85.2(5) . . ?
O33 W8 O22 171.9(6) . . ?
O24 W8 O22 83.1(5) . . ?
O29 W8 O22 74.8(4) . . ?
O30 W8 O22 75.5(5) . . ?
O25 W8 O22 85.0(5) . . ?
O34 W9 O26 101.4(6) . . ?
O34 W9 O30 98.9(6) . . ?
O26 W9 O30 92.7(5) . . ?
O34 W9 O27 100.5(6) . . ?
O26 W9 O27 86.4(6) . . ?
O30 W9 O27 160.3(5) . . ?
O34 W9 O31 99.6(6) . . ?
O26 W9 O31 158.7(5) . . ?
O30 W9 O31 88.1(5) . . ?
O27 W9 O31 85.7(6) . . ?
O34 W9 O22 169.0(5) . . ?
O26 W9 O22 87.3(5) . . ?
O30 W9 O22 73.8(4) . . ?
O27 W9 O22 86.6(5) . . ?
O31 W9 O22 72.4(4) . . ?
O2 Cr1 O2 180.0(6) . 2_775 ?
O2 Cr1 O1 90.7(5) . 2_775 ?
O2 Cr1 O1 89.3(5) 2_775 2_775 ?
O2 Cr1 O1 89.3(5) . . ?
O2 Cr1 O1 90.7(5) 2_775 . ?
O1 Cr1 O1 180.0 2_775 . ?
O2 Cr1 O19 81.0(4) . . ?
O2 Cr1 O19 99.0(4) 2_775 . ?
O1 Cr1 O19 99.0(4) 2_775 . ?
O1 Cr1 O19 81.0(4) . . ?
O2 Cr1 O19 99.0(4) . 2_775 ?
O2 Cr1 O19 81.0(4) 2_775 2_775 ?
O1 Cr1 O19 81.0(4) 2_775 2_775 ?
O1 Cr1 O19 99.0(4) . 2_775 ?
O19 Cr1 O19 180.0(4) . 2_775 ?
C12 C11 Cl11 115(5) . . ?
C11 C12 Cl12 125(5) . . ?
C22 C21 Cl21 113(2) . . ?
C21 C22 Cl22 110(2) . . ?
C32 C31 Cl31 116(3) . . ?
C31 C32 Cl32 115(3) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C141 N1 C111 C112 68(3) . . . . ?
C131 N1 C111 C112 -169(2) . . . . ?
C121 N1 C111 C112 -53(3) . . . . ?
N1 C111 C112 C113 -178(2) . . . . ?
C111 C112 C113 C114 177(3) . . . . ?
C111 N1 C121 C122 -50(3) . . . . ?
C141 N1 C121 C122 -168.4(19) . . . . ?
C131 N1 C121 C122 69(2) . . . . ?
N1 C121 C122 C123 180.0(19) . . . . ?
C121 C122 C123 C124 -178(2) . . . . ?
C111 N1 C131 C132 -61(3) . . . . ?
C141 N1 C131 C132 58(3) . . . . ?
C121 N1 C131 C132 179(2) . . . . ?
N1 C131 C132 C133 172(2) . . . . ?
C131 C132 C133 C134 -166(2) . . . . ?
C111 N1 C141 C142 -177(2) . . . . ?
C131 N1 C141 C142 62(2) . . . . ?
C121 N1 C141 C142 -56(2) . . . . ?
N1 C141 C142 C143 -175.2(19) . . . . ?
C141 C142 C143 C144 -169(2) . . . . ?
C241 N2 C211 C212 179.9(19) . . . . ?
C221 N2 C211 C212 56(2) . . . . ?
C231 N2 C211 C212 -59(2) . . . . ?
N2 C211 C212 C213 174.9(19) . . . . ?
C211 C212 C213 C214 -175(3) . . . . ?
C241 N2 C221 C222 -61(2) . . . . ?
C211 N2 C221 C222 60(2) . . . . ?
C231 N2 C221 C222 179.4(16) . . . . ?
N2 C221 C222 C223 173.3(16) . . . . ?
C221 C222 C223 C224 63(3) . . . . ?
C241 N2 C231 C232 57(2) . . . . ?
C211 N2 C231 C232 -62(2) . . . . ?
C221 N2 C231 C232 178.3(16) . . . . ?
N2 C231 C232 C233 167.3(16) . . . . ?
C231 C232 C233 C234 170(2) . . . . ?
C211 N2 C241 C242 -176.0(17) . . . . ?
C221 N2 C241 C242 -53(2) . . . . ?
C231 N2 C241 C242 63(2) . . . . ?
N2 C241 C242 C243 -174.0(17) . . . . ?
C241 C242 C243 C244 72(2) . . . . ?
C321 N3 C311 C312 -57(3) . . . . ?
C341 N3 C311 C312 65(2) . . . . ?
C331 N3 C311 C312 -179.7(19) . . . . ?
N3 C311 C312 C313 177(2) . . . . ?
C311 C312 C313 C314 -178(2) . . . . ?
C341 N3 C321 C322 179.6(19) . . . . ?
C331 N3 C321 C322 59(2) . . . . ?
C311 N3 C321 C322 -59(2) . . . . ?
N3 C321 C322 C323 -173.9(19) . . . . ?
C321 C322 C323 C324 71(3) . . . . ?
C321 N3 C331 C332 63(2) . . . . ?
C341 N3 C331 C332 -58(2) . . . . ?
C311 N3 C331 C332 -174.8(19) . . . . ?
N3 C331 C332 C333 -171.0(18) . . . . ?
C331 C332 C333 C334 176(2) . . . . ?
C321 N3 C341 C342 174(2) . . . . ?
C331 N3 C341 C342 -63(3) . . . . ?
C311 N3 C341 C342 52(3) . . . . ?
N3 C341 C342 C343 163(2) . . . . ?
C341 C342 C343 C344 175(2) . . . . ?
C421 N4 C411 C412 136(5) . . . . ?
C421 N4 C411 C412 -44(5) 2_776 . . . ?
C421 N4 C411 C421 180.001(9) 2_776 . . . ?
N4 C411 C412 C413 -170(3) . . . . ?
C421 C411 C412 C413 -103(6) . . . . ?
C411 C412 C413 C414 -178(4) . . . . ?
C411 N4 C421 C422 -100(4) . . . . ?
C411 N4 C421 C422 80(4) 2_776 . . . ?
C411 N4 C421 C411 180.001(11) 2_776 . . . ?
N4 C421 C422 C423 95(4) . . . . ?
C411 C421 C422 C423 46(4) . . . . ?
C421 C422 C423 C424 106(4) . . . . ?
W4 O20 Si1 O21 43.2(10) . . . . ?
W3 O20 Si1 O21 177.8(6) . . . . ?
W4 O20 Si1 O22 -75.0(9) . . . . ?
W3 O20 Si1 O22 59.6(9) . . . . ?
W4 O20 Si1 O19 167.5(7) . . . . ?
W3 O20 Si1 O19 -57.8(9) . . . . ?
W5 O21 Si1 O20 -48.7(9) . . . . ?
W6 O21 Si1 O20 176.8(6) . . . . ?
W5 O21 Si1 O22 70.1(8) . . . . ?
W6 O21 Si1 O22 -64.5(8) . . . . ?
W5 O21 Si1 O19 -173.0(6) . . . . ?
W6 O21 Si1 O19 52.4(8) . . . . ?
W7 O22 Si1 O20 176.8(7) . . . . ?
W8 O22 Si1 O20 -56.3(9) . . . . ?
W9 O22 Si1 O20 59.6(8) . . . . ?
W7 O22 Si1 O21 53.1(9) . . . . ?
W8 O22 Si1 O21 180.0(7) . . . . ?
W9 O22 Si1 O21 -64.1(7) . . . . ?
W7 O22 Si1 O19 -64.8(9) . . . . ?
W8 O22 Si1 O19 62.1(8) . . . . ?
W9 O22 Si1 O19 178.0(6) . . . . ?
Cr1 O19 Si1 O20 -63.1(9) . . . . ?
W1 O19 Si1 O20 173.8(6) . . . . ?
W2 O19 Si1 O20 58.4(8) . . . . ?
Cr1 O19 Si1 O21 64.3(9) . . . . ?
W1 O19 Si1 O21 -58.8(8) . . . . ?
W2 O19 Si1 O21 -174.2(6) . . . . ?
Cr1 O19 Si1 O22 -179.9(6) . . . . ?
W1 O19 Si1 O22 57.0(8) . . . . ?
W2 O19 Si1 O22 -58.5(8) . . . . ?
W6 O18 W1 O7 127.9(16) . . . . ?
W6 O18 W1 O1 -131.6(16) . . . . ?
W6 O18 W1 O13 -42(2) . . . . ?
W6 O18 W1 O23 27.4(16) . . . . ?
W6 O18 W1 O19 -57.4(16) . . . . ?
Cr1 O2 W2 O8 174.9(7) . . . . ?
Cr1 O2 W2 O14 -81.8(7) . . . . ?
Cr1 O2 W2 O24 -5.8(17) . . . . ?
Cr1 O2 W2 O13 73.7(7) . . . . ?
Cr1 O2 W2 O19 0.3(5) . . . . ?
W8 O25 W3 O9 -131.8(13) . . . . ?
W8 O25 W3 O14 -29.9(13) . . . . ?
W8 O25 W3 O15 130.1(13) . . . . ?
W8 O25 W3 O3 35(3) . . . . ?
W8 O25 W3 O20 55.5(13) . . . . ?
W2 O14 W3 O9 127.9(13) . . . . ?
W2 O14 W3 O25 26.1(13) . . . . ?
W2 O14 W3 O15 -77(2) . . . . ?
W2 O14 W3 O3 -138.6(14) . . . . ?
W2 O14 W3 O20 -60.6(13) . . . . ?
W5 O16 W4 O10 -115.5(15) . . . . ?
W5 O16 W4 O4 143.3(14) . . . . ?
W5 O16 W4 O15 46(2) . . . . ?
W5 O16 W4 O26 -23.0(14) . . . . ?
W5 O16 W4 O20 57.7(14) . . . . ?
W1 O23 W7 O32 126.4(15) . . . . ?
W1 O23 W7 O28 26.3(15) . . . . ?
W1 O23 W7 O31 -54(2) . . . . ?
W1 O23 W7 O29 -136.8(15) . . . . ?
W1 O23 W7 O22 -61.8(15) . . . . ?
W2 O24 W8 O33 -126.9(16) . . . . ?
W2 O24 W8 O29 133.1(16) . . . . ?
W2 O24 W8 O30 40(3) . . . . ?
W2 O24 W8 O25 -26.9(16) . . . . ?
W2 O24 W8 O22 58.6(16) . . . . ?
W4 O26 W9 O34 -136.0(14) . . . . ?
W4 O26 W9 O30 124.4(14) . . . . ?
W4 O26 W9 O27 -36.0(14) . . . . ?
W4 O26 W9 O31 33(2) . . . . ?
W4 O26 W9 O22 50.8(14) . . . . ?
Cl11 C11 C12 Cl12 -52(8) . . . . ?
Cl21 C21 C22 Cl22 56(3) . . . . ?
Cl31 C31 C32 Cl32 58(4) . . . . ?

_refine_diff_density_max         5.526
_refine_diff_density_min         -9.520
_refine_diff_density_rms         0.852

_shelxl_version_number           2014/6



