# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2017

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_5075
_database_code_depnum_ccdc_archive 'CCDC 1527028'
_audit_update_record             
;
2017-01-12 deposited with the CCDC.
2017-03-07 downloaded from the CCDC.
;
_audit_creation_date             2016-05-27
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C10 H25 B20 P'
_chemical_formula_sum            'C10 H25 B20 P'
_chemical_formula_weight         392.47
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   7.1139(10)
_cell_length_b                   11.4378(14)
_cell_length_c                   13.3912(15)
_cell_angle_alpha                81.884(5)
_cell_angle_beta                 84.954(5)
_cell_angle_gamma                81.231(6)
_cell_volume                     1063.6(2)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    2475
_cell_measurement_temperature    100.0(2)
_cell_measurement_theta_max      26.058
_cell_measurement_theta_min      2.224
_shelx_estimated_absorpt_T_max   0.990
_shelx_estimated_absorpt_T_min   0.951
_exptl_absorpt_coefficient_mu    0.127
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_correction_T_min  0.6919
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.0704 before and 0.0615 after correction.
The Ratio of minimum to maximum transmission is 0.9282.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.225
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    ?
_exptl_crystal_description       PLATE
_exptl_crystal_F_000             400
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.08
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0636
_diffrn_reflns_av_unetI/netI     0.0780
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.987
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            15395
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.987
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         26.464
_diffrn_reflns_theta_min         2.904
_diffrn_ambient_temperature      100.0(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3563
_reflns_number_total             4334
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v7.68A (Bruker, 2009)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'XS (Sheldrick, 2008)'
_refine_diff_density_max         0.312
_refine_diff_density_min         -0.350
_refine_diff_density_rms         0.065
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.135
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     340
_refine_ls_number_reflns         4334
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0871
_refine_ls_R_factor_gt           0.0685
_refine_ls_restrained_S_all      1.135
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0347P)²+0.9539P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1260
_refine_ls_wR_factor_ref         0.1342
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C12(H12), C13(H13), C14(H14), C15(H15), C16(H16)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     heavy
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P 0.54074(10) 0.78360(6) 0.67791(5) 0.01170(18) Uani 1 1 d . . . . .
C1 C 0.7501(4) 0.5711(2) 0.78898(18) 0.0116(5) Uani 1 1 d . . . . .
C2 C 0.6263(4) 0.6175(2) 0.68943(18) 0.0125(5) Uani 1 1 d . . . . .
B3 B 0.8688(4) 0.5708(3) 0.6677(2) 0.0143(6) Uani 1 1 d . . . . .
H3 H 0.958(4) 0.635(2) 0.640(2) 0.017 Uiso 1 1 d R . . . .
B4 B 0.9225(4) 0.4524(3) 0.7669(2) 0.0149(6) Uani 1 1 d . . . . .
H4 H 1.054(4) 0.444(2) 0.801(2) 0.018 Uiso 1 1 d R . . . .
B5 B 0.7062(4) 0.4312(3) 0.8423(2) 0.0147(6) Uani 1 1 d . . . . .
H5 H 0.706(4) 0.411(2) 0.923(2) 0.018 Uiso 1 1 d R . . . .
B6 B 0.5174(4) 0.5358(3) 0.7916(2) 0.0141(6) Uani 1 1 d . . . . .
H6 H 0.406(4) 0.581(2) 0.836(2) 0.017 Uiso 1 1 d R . . . .
B7 B 0.7019(4) 0.5339(3) 0.5919(2) 0.0162(7) Uani 1 1 d . . . . .
H7 H 0.698(4) 0.576(2) 0.518(2) 0.019 Uiso 1 1 d R . . . .
B8 B 0.8899(5) 0.4247(3) 0.6419(2) 0.0166(7) Uani 1 1 d . . . . .
H8 H 1.008(4) 0.392(2) 0.594(2) 0.020 Uiso 1 1 d R . . . .
B9 B 0.7916(5) 0.3369(3) 0.7482(2) 0.0178(7) Uani 1 1 d . . . . .
H9 H 0.849(4) 0.244(3) 0.771(2) 0.021 Uiso 1 1 d R . . . .
B10 B 0.5433(5) 0.3907(3) 0.7631(2) 0.0165(7) Uani 1 1 d . . . . .
H10 H 0.438(4) 0.336(2) 0.795(2) 0.020 Uiso 1 1 d R . . . .
C11 C 0.6554(4) 0.8368(2) 0.55671(19) 0.0135(6) Uani 1 1 d . . . . .
B11 B 0.4886(4) 0.5130(3) 0.6669(2) 0.0141(6) Uani 1 1 d . . . . .
H11 H 0.353(4) 0.541(2) 0.639(2) 0.017 Uiso 1 1 d R . . . .
C12 C 0.5312(4) 0.8522(2) 0.47918(19) 0.0165(6) Uani 1 1 d . . . . .
H12 H 0.4019 0.8408 0.4950 0.020 Uiso 1 1 calc R . . . .
B12 B 0.6570(5) 0.3877(3) 0.6399(2) 0.0175(7) Uani 1 1 d . . . . .
H12A H 0.622(4) 0.327(2) 0.591(2) 0.021 Uiso 1 1 d R . . . .
C13 C 0.5942(4) 0.8839(2) 0.3797(2) 0.0196(6) Uani 1 1 d . . . . .
H13 H 0.5097 0.8908 0.3273 0.024 Uiso 1 1 calc R . . . .
C14 C 0.7796(4) 0.9055(2) 0.3565(2) 0.0214(6) Uani 1 1 d . . . . .
H14 H 0.8229 0.9277 0.2883 0.026 Uiso 1 1 calc R . . . .
C15 C 0.9029(4) 0.8947(2) 0.4332(2) 0.0220(6) Uani 1 1 d . . . . .
H15 H 1.0299 0.9109 0.4173 0.026 Uiso 1 1 calc R . . . .
C16 C 0.8425(4) 0.8606(2) 0.5326(2) 0.0172(6) Uani 1 1 d . . . . .
H16 H 0.9280 0.8533 0.5845 0.021 Uiso 1 1 calc R . . . .
C1' C 0.7731(3) 0.6755(2) 0.84513(18) 0.0108(5) Uani 1 1 d . . . . .
C2' C 0.6853(4) 0.8053(2) 0.78374(18) 0.0119(5) Uani 1 1 d . . . . .
B3' B 0.5621(4) 0.7545(3) 0.8958(2) 0.0139(6) Uani 1 1 d . . . . .
H3' H 0.429(4) 0.725(2) 0.890(2) 0.017 Uiso 1 1 d R . . . .
B4' B 0.7419(4) 0.6775(3) 0.9738(2) 0.0144(6) Uani 1 1 d . . . . .
H4' H 0.717(4) 0.596(2) 1.018(2) 0.017 Uiso 1 1 d R . . . .
B5' B 0.9683(4) 0.6884(3) 0.9081(2) 0.0156(6) Uani 1 1 d . . . . .
H5' H 1.080(4) 0.616(2) 0.913(2) 0.019 Uiso 1 1 d R . . . .
B6' B 0.9329(4) 0.7707(3) 0.7872(2) 0.0133(6) Uani 1 1 d . . . . .
H6' H 1.023(4) 0.746(2) 0.721(2) 0.016 Uiso 1 1 d R . . . .
B7' B 0.5912(4) 0.9052(3) 0.8675(2) 0.0131(6) Uani 1 1 d . . . . .
H7' H 0.471(4) 0.963(2) 0.844(2) 0.016 Uiso 1 1 d R . . . .
B8' B 0.6297(4) 0.8257(3) 0.9902(2) 0.0158(6) Uani 1 1 d . . . . .
H8' H 0.531(4) 0.841(2) 1.053(2) 0.019 Uiso 1 1 d R . . . .
B9' B 0.8805(5) 0.7860(3) 0.9986(2) 0.0178(7) Uani 1 1 d . . . . .
H9' H 0.945(4) 0.780(2) 1.065(2) 0.021 Uiso 1 1 d R . . . .
B10' B 0.9948(4) 0.8427(3) 0.8826(2) 0.0165(7) Uani 1 1 d . . . . .
H10' H 1.130(4) 0.871(2) 0.875(2) 0.020 Uiso 1 1 d R . . . .
B11' B 0.8152(4) 0.9155(3) 0.8003(2) 0.0147(6) Uani 1 1 d . . . . .
H11' H 0.831(4) 0.984(2) 0.738(2) 0.018 Uiso 1 1 d R . . . .
B12' B 0.7871(4) 0.9272(3) 0.9324(2) 0.0161(6) Uani 1 1 d . . . . .
H12' H 0.796(4) 1.012(2) 0.961(2) 0.019 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
P1 C2 1.893(3) . ?
P1 C11 1.819(3) . ?
P1 C2' 1.887(3) . ?
C1 C2 1.643(3) . ?
C1 B3 1.764(4) . ?
C1 B4 1.726(4) . ?
C1 B5 1.721(4) . ?
C1 B6 1.760(4) . ?
C1 C1' 1.534(3) . ?
C2 B3 1.738(4) . ?
C2 B6 1.737(4) . ?
C2 B7 1.726(4) . ?
C2 B11 1.729(4) . ?
B3 H3 1.05(3) . ?
B3 B4 1.780(4) . ?
B3 B7 1.761(4) . ?
B3 B8 1.735(4) . ?
B4 H4 1.06(3) . ?
B4 B5 1.794(4) . ?
B4 B8 1.788(4) . ?
B4 B9 1.784(4) . ?
B5 H5 1.07(3) . ?
B5 B6 1.772(4) . ?
B5 B9 1.780(4) . ?
B5 B10 1.790(4) . ?
B6 H6 1.06(3) . ?
B6 B10 1.734(4) . ?
B6 B11 1.760(4) . ?
B7 H7 1.04(3) . ?
B7 B8 1.791(5) . ?
B7 B11 1.772(4) . ?
B7 B12 1.770(4) . ?
B8 H8 1.06(3) . ?
B8 B9 1.778(4) . ?
B8 B12 1.774(4) . ?
B9 H9 1.09(3) . ?
B9 B10 1.783(4) . ?
B9 B12 1.787(4) . ?
B10 H10 1.07(3) . ?
B10 B11 1.783(4) . ?
B10 B12 1.774(4) . ?
C11 C12 1.397(4) . ?
C11 C16 1.401(4) . ?
B11 H11 1.05(3) . ?
B11 B12 1.779(5) . ?
C12 H12 0.9500 . ?
C12 C13 1.384(4) . ?
B12 H12A 1.08(3) . ?
C13 H13 0.9500 . ?
C13 C14 1.380(4) . ?
C14 H14 0.9500 . ?
C14 C15 1.389(4) . ?
C15 H15 0.9500 . ?
C15 C16 1.382(4) . ?
C16 H16 0.9500 . ?
C1' C2' 1.653(3) . ?
C1' B3' 1.764(4) . ?
C1' B4' 1.721(4) . ?
C1' B5' 1.722(4) . ?
C1' B6' 1.750(4) . ?
C2' B3' 1.743(4) . ?
C2' B6' 1.749(4) . ?
C2' B7' 1.735(4) . ?
C2' B11' 1.721(4) . ?
B3' H3' 1.06(3) . ?
B3' B4' 1.770(4) . ?
B3' B7' 1.752(4) . ?
B3' B8' 1.734(4) . ?
B4' H4' 1.06(3) . ?
B4' B5' 1.779(4) . ?
B4' B8' 1.795(4) . ?
B4' B9' 1.781(5) . ?
B5' H5' 1.06(3) . ?
B5' B6' 1.773(4) . ?
B5' B9' 1.772(4) . ?
B5' B10' 1.785(4) . ?
B6' H6' 1.10(3) . ?
B6' B10' 1.735(4) . ?
B6' B11' 1.763(4) . ?
B7' H7' 1.04(3) . ?
B7' B8' 1.785(4) . ?
B7' B11' 1.771(4) . ?
B7' B12' 1.773(4) . ?
B8' H8' 1.07(3) . ?
B8' B9' 1.782(4) . ?
B8' B12' 1.787(4) . ?
B9' H9' 1.03(3) . ?
B9' B10' 1.775(5) . ?
B9' B12' 1.791(4) . ?
B10' H10' 1.05(3) . ?
B10' B11' 1.790(4) . ?
B10' B12' 1.771(4) . ?
B11' H11' 1.07(3) . ?
B11' B12' 1.784(4) . ?
B12' H12' 1.10(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11 P1 C2 102.02(11) . . ?
C11 P1 C2' 109.84(12) . . ?
C2' P1 C2 93.00(11) . . ?
C2 C1 B3 61.24(15) . . ?
C2 C1 B4 110.92(19) . . ?
C2 C1 B5 110.7(2) . . ?
C2 C1 B6 61.29(15) . . ?
B4 C1 B3 61.33(16) . . ?
B4 C1 B6 112.6(2) . . ?
B5 C1 B3 112.4(2) . . ?
B5 C1 B4 62.74(17) . . ?
B5 C1 B6 61.19(16) . . ?
B6 C1 B3 112.18(19) . . ?
C1' C1 C2 111.09(19) . . ?
C1' C1 B3 115.8(2) . . ?
C1' C1 B4 126.4(2) . . ?
C1' C1 B5 126.8(2) . . ?
C1' C1 B6 116.0(2) . . ?
C1 C2 P1 111.87(16) . . ?
C1 C2 B3 62.81(16) . . ?
C1 C2 B6 62.67(15) . . ?
C1 C2 B7 111.8(2) . . ?
C1 C2 B11 111.77(19) . . ?
B3 C2 P1 118.01(17) . . ?
B6 C2 P1 113.81(17) . . ?
B6 C2 B3 114.6(2) . . ?
B7 C2 P1 126.96(18) . . ?
B7 C2 B3 61.09(17) . . ?
B7 C2 B6 112.2(2) . . ?
B7 C2 B11 61.71(17) . . ?
B11 C2 P1 123.92(18) . . ?
B11 C2 B3 112.4(2) . . ?
B11 C2 B6 61.04(16) . . ?
C1 B3 H3 120.3(15) . . ?
C1 B3 B4 58.28(15) . . ?
C2 B3 C1 55.95(15) . . ?
C2 B3 H3 118.6(15) . . ?
C2 B3 B4 104.1(2) . . ?
C2 B3 B7 59.12(16) . . ?
B4 B3 H3 124.6(15) . . ?
B7 B3 C1 104.6(2) . . ?
B7 B3 H3 121.4(14) . . ?
B7 B3 B4 109.9(2) . . ?
B8 B3 C1 105.5(2) . . ?
B8 B3 C2 106.2(2) . . ?
B8 B3 H3 128.2(15) . . ?
B8 B3 B4 61.15(18) . . ?
B8 B3 B7 61.62(18) . . ?
C1 B4 B3 60.39(16) . . ?
C1 B4 H4 118.4(15) . . ?
C1 B4 B5 58.49(16) . . ?
C1 B4 B8 104.8(2) . . ?
C1 B4 B9 104.5(2) . . ?
B3 B4 H4 119.3(14) . . ?
B3 B4 B5 108.3(2) . . ?
B3 B4 B8 58.17(17) . . ?
B3 B4 B9 106.4(2) . . ?
B5 B4 H4 120.5(14) . . ?
B8 B4 H4 127.0(15) . . ?
B8 B4 B5 107.3(2) . . ?
B9 B4 H4 128.0(15) . . ?
B9 B4 B5 59.67(17) . . ?
B9 B4 B8 59.68(17) . . ?
C1 B5 B4 58.77(16) . . ?
C1 B5 H5 117.4(14) . . ?
C1 B5 B6 60.49(16) . . ?
C1 B5 B9 104.9(2) . . ?
C1 B5 B10 105.1(2) . . ?
B4 B5 H5 120.8(14) . . ?
B6 B5 B4 108.8(2) . . ?
B6 B5 H5 117.6(15) . . ?
B6 B5 B9 106.9(2) . . ?
B6 B5 B10 58.28(17) . . ?
B9 B5 B4 59.89(17) . . ?
B9 B5 H5 129.2(15) . . ?
B9 B5 B10 59.92(18) . . ?
B10 B5 B4 107.9(2) . . ?
B10 B5 H5 126.7(14) . . ?
C1 B6 B5 58.32(16) . . ?
C1 B6 H6 119.5(15) . . ?
C1 B6 B11 105.0(2) . . ?
C2 B6 C1 56.04(14) . . ?
C2 B6 B5 104.1(2) . . ?
C2 B6 H6 118.4(14) . . ?
C2 B6 B11 59.26(16) . . ?
B5 B6 H6 124.3(14) . . ?
B10 B6 C1 105.8(2) . . ?
B10 B6 C2 106.1(2) . . ?
B10 B6 B5 61.38(18) . . ?
B10 B6 H6 128.7(15) . . ?
B10 B6 B11 61.36(18) . . ?
B11 B6 B5 110.0(2) . . ?
B11 B6 H6 121.8(14) . . ?
C2 B7 B3 59.79(16) . . ?
C2 B7 H7 118.9(15) . . ?
C2 B7 B8 104.3(2) . . ?
C2 B7 B11 59.23(16) . . ?
C2 B7 B12 104.9(2) . . ?
B3 B7 H7 117.5(15) . . ?
B3 B7 B8 58.47(17) . . ?
B3 B7 B11 109.3(2) . . ?
B3 B7 B12 107.1(2) . . ?
B8 B7 H7 126.0(15) . . ?
B11 B7 H7 120.9(15) . . ?
B11 B7 B8 108.2(2) . . ?
B12 B7 H7 128.4(15) . . ?
B12 B7 B8 59.77(18) . . ?
B12 B7 B11 60.29(17) . . ?
B3 B8 B4 60.68(17) . . ?
B3 B8 B7 59.91(17) . . ?
B3 B8 H8 118.7(15) . . ?
B3 B8 B9 108.7(2) . . ?
B3 B8 B12 108.1(2) . . ?
B4 B8 B7 108.2(2) . . ?
B4 B8 H8 120.7(15) . . ?
B7 B8 H8 120.9(15) . . ?
B9 B8 B4 60.05(17) . . ?
B9 B8 B7 107.9(2) . . ?
B9 B8 H8 123.7(15) . . ?
B12 B8 B4 108.4(2) . . ?
B12 B8 B7 59.53(18) . . ?
B12 B8 H8 123.6(15) . . ?
B12 B8 B9 60.41(18) . . ?
B4 B9 H9 119.7(15) . . ?
B4 B9 B12 108.0(2) . . ?
B5 B9 B4 60.43(17) . . ?
B5 B9 H9 119.5(15) . . ?
B5 B9 B10 60.30(18) . . ?
B5 B9 B12 107.9(2) . . ?
B8 B9 B4 60.27(17) . . ?
B8 B9 B5 108.4(2) . . ?
B8 B9 H9 122.6(15) . . ?
B8 B9 B10 107.8(2) . . ?
B8 B9 B12 59.70(17) . . ?
B10 B9 B4 108.6(2) . . ?
B10 B9 H9 122.1(15) . . ?
B10 B9 B12 59.61(18) . . ?
B12 B9 H9 124.2(15) . . ?
B5 B10 H10 119.8(15) . . ?
B6 B10 B5 60.34(17) . . ?
B6 B10 B9 108.4(2) . . ?
B6 B10 H10 117.9(15) . . ?
B6 B10 B11 60.04(17) . . ?
B6 B10 B12 108.2(2) . . ?
B9 B10 B5 59.78(17) . . ?
B9 B10 H10 123.8(15) . . ?
B9 B10 B11 108.3(2) . . ?
B11 B10 B5 108.1(2) . . ?
B11 B10 H10 121.3(15) . . ?
B12 B10 B5 108.0(2) . . ?
B12 B10 B9 60.30(18) . . ?
B12 B10 H10 124.9(15) . . ?
B12 B10 B11 59.99(17) . . ?
C12 C11 P1 111.57(19) . . ?
C12 C11 C16 118.6(2) . . ?
C16 C11 P1 129.8(2) . . ?
C2 B11 B6 59.70(16) . . ?
C2 B11 B7 59.06(16) . . ?
C2 B11 B10 104.3(2) . . ?
C2 B11 H11 119.8(15) . . ?
C2 B11 B12 104.4(2) . . ?
B6 B11 B7 108.9(2) . . ?
B6 B11 B10 58.60(17) . . ?
B6 B11 H11 117.0(15) . . ?
B6 B11 B12 106.9(2) . . ?
B7 B11 B10 107.8(2) . . ?
B7 B11 H11 122.5(14) . . ?
B7 B11 B12 59.79(17) . . ?
B10 B11 H11 124.6(14) . . ?
B12 B11 B10 59.75(17) . . ?
B12 B11 H11 128.6(15) . . ?
C11 C12 H12 119.6 . . ?
C13 C12 C11 120.9(3) . . ?
C13 C12 H12 119.6 . . ?
B7 B12 B8 60.69(18) . . ?
B7 B12 B9 108.4(2) . . ?
B7 B12 B10 108.3(2) . . ?
B7 B12 B11 59.93(17) . . ?
B7 B12 H12A 121.8(14) . . ?
B8 B12 B9 59.89(18) . . ?
B8 B12 B10 108.3(2) . . ?
B8 B12 B11 108.6(2) . . ?
B8 B12 H12A 123.1(15) . . ?
B9 B12 H12A 122.3(15) . . ?
B10 B12 B9 60.09(17) . . ?
B10 B12 B11 60.25(17) . . ?
B10 B12 H12A 120.2(15) . . ?
B11 B12 B9 108.3(2) . . ?
B11 B12 H12A 119.9(15) . . ?
C12 C13 H13 120.0 . . ?
C14 C13 C12 120.0(3) . . ?
C14 C13 H13 120.0 . . ?
C13 C14 H14 120.1 . . ?
C13 C14 C15 119.8(3) . . ?
C15 C14 H14 120.1 . . ?
C14 C15 H15 119.7 . . ?
C16 C15 C14 120.7(3) . . ?
C16 C15 H15 119.7 . . ?
C11 C16 H16 120.0 . . ?
C15 C16 C11 120.0(3) . . ?
C15 C16 H16 120.0 . . ?
C1 C1' C2' 111.78(19) . . ?
C1 C1' B3' 116.6(2) . . ?
C1 C1' B4' 125.9(2) . . ?
C1 C1' B5' 126.1(2) . . ?
C1 C1' B6' 116.2(2) . . ?
C2' C1' B3' 61.23(15) . . ?
C2' C1' B4' 110.96(19) . . ?
C2' C1' B5' 111.21(19) . . ?
C2' C1' B6' 61.77(15) . . ?
B4' C1' B3' 61.05(16) . . ?
B4' C1' B5' 62.24(17) . . ?
B4' C1' B6' 112.4(2) . . ?
B5' C1' B3' 111.8(2) . . ?
B5' C1' B6' 61.40(16) . . ?
B6' C1' B3' 112.22(19) . . ?
C1' C2' P1 110.94(16) . . ?
C1' C2' B3' 62.54(15) . . ?
C1' C2' B6' 61.85(15) . . ?
C1' C2' B7' 110.88(19) . . ?
C1' C2' B11' 111.0(2) . . ?
B3' C2' P1 106.26(16) . . ?
B3' C2' B6' 113.34(19) . . ?
B6' C2' P1 125.77(17) . . ?
B7' C2' P1 119.74(17) . . ?
B7' C2' B3' 60.50(16) . . ?
B7' C2' B6' 111.6(2) . . ?
B11' C2' P1 132.77(18) . . ?
B11' C2' B3' 111.6(2) . . ?
B11' C2' B6' 61.07(16) . . ?
B11' C2' B7' 61.66(16) . . ?
C1' B3' H3' 119.4(15) . . ?
C1' B3' B4' 58.26(15) . . ?
C2' B3' C1' 56.24(14) . . ?
C2' B3' H3' 117.5(14) . . ?
C2' B3' B4' 104.6(2) . . ?
C2' B3' B7' 59.53(16) . . ?
B4' B3' H3' 124.4(14) . . ?
B7' B3' C1' 105.0(2) . . ?
B7' B3' H3' 121.7(15) . . ?
B7' B3' B4' 110.1(2) . . ?
B8' B3' C1' 106.2(2) . . ?
B8' B3' C2' 107.1(2) . . ?
B8' B3' H3' 128.4(15) . . ?
B8' B3' B4' 61.60(17) . . ?
B8' B3' B7' 61.59(18) . . ?
C1' B4' B3' 60.69(16) . . ?
C1' B4' H4' 116.7(15) . . ?
C1' B4' B5' 58.92(16) . . ?
C1' B4' B8' 105.4(2) . . ?
C1' B4' B9' 104.9(2) . . ?
B3' B4' H4' 118.7(15) . . ?
B3' B4' B5' 108.8(2) . . ?
B3' B4' B8' 58.21(17) . . ?
B3' B4' B9' 106.5(2) . . ?
B5' B4' H4' 119.6(15) . . ?
B5' B4' B8' 107.9(2) . . ?
B5' B4' B9' 59.71(18) . . ?
B8' B4' H4' 127.8(15) . . ?
B9' B4' H4' 129.1(15) . . ?
B9' B4' B8' 59.79(18) . . ?
C1' B5' B4' 58.84(16) . . ?
C1' B5' H5' 117.7(15) . . ?
C1' B5' B6' 60.08(16) . . ?
C1' B5' B9' 105.2(2) . . ?
C1' B5' B10' 104.8(2) . . ?
B4' B5' H5' 121.4(15) . . ?
B4' B5' B10' 107.9(2) . . ?
B6' B5' B4' 108.6(2) . . ?
B6' B5' H5' 117.3(15) . . ?
B6' B5' B10' 58.39(17) . . ?
B9' B5' B4' 60.20(18) . . ?
B9' B5' H5' 129.0(15) . . ?
B9' B5' B6' 107.0(2) . . ?
B9' B5' B10' 59.86(18) . . ?
B10' B5' H5' 126.3(15) . . ?
C1' B6' B5' 58.52(15) . . ?
C1' B6' H6' 119.3(14) . . ?
C1' B6' B11' 104.7(2) . . ?
C2' B6' C1' 56.38(14) . . ?
C2' B6' B5' 104.5(2) . . ?
C2' B6' H6' 121.5(14) . . ?
C2' B6' B11' 58.68(16) . . ?
B5' B6' H6' 120.8(14) . . ?
B10' B6' C1' 105.7(2) . . ?
B10' B6' C2' 106.0(2) . . ?
B10' B6' B5' 61.17(18) . . ?
B10' B6' H6' 126.8(14) . . ?
B10' B6' B11' 61.53(18) . . ?
B11' B6' B5' 109.8(2) . . ?
B11' B6' H6' 124.7(14) . . ?
C2' B7' B3' 59.97(16) . . ?
C2' B7' H7' 114.7(15) . . ?
C2' B7' B8' 105.2(2) . . ?
C2' B7' B11' 58.78(16) . . ?
C2' B7' B12' 105.3(2) . . ?
B3' B7' H7' 115.8(15) . . ?
B3' B7' B8' 58.71(17) . . ?
B3' B7' B11' 108.8(2) . . ?
B3' B7' B12' 107.5(2) . . ?
B8' B7' H7' 127.8(15) . . ?
B11' B7' H7' 120.1(15) . . ?
B11' B7' B8' 108.7(2) . . ?
B11' B7' B12' 60.45(17) . . ?
B12' B7' H7' 131.4(15) . . ?
B12' B7' B8' 60.29(17) . . ?
B3' B8' B4' 60.19(17) . . ?
B3' B8' B7' 59.69(17) . . ?
B3' B8' H8' 118.5(15) . . ?
B3' B8' B9' 108.0(2) . . ?
B3' B8' B12' 107.6(2) . . ?
B4' B8' H8' 120.9(15) . . ?
B7' B8' B4' 107.5(2) . . ?
B7' B8' H8' 121.1(15) . . ?
B7' B8' B12' 59.53(17) . . ?
B9' B8' B4' 59.73(17) . . ?
B9' B8' B7' 107.6(2) . . ?
B9' B8' H8' 124.4(15) . . ?
B9' B8' B12' 60.25(18) . . ?
B12' B8' B4' 107.8(2) . . ?
B12' B8' H8' 124.5(15) . . ?
B4' B9' B8' 60.47(17) . . ?
B4' B9' H9' 122.5(16) . . ?
B4' B9' B12' 108.2(2) . . ?
B5' B9' B4' 60.09(17) . . ?
B5' B9' B8' 108.7(2) . . ?
B5' B9' H9' 120.8(16) . . ?
B5' B9' B10' 60.43(18) . . ?
B5' B9' B12' 108.2(2) . . ?
B8' B9' H9' 122.5(16) . . ?
B8' B9' B12' 59.99(17) . . ?
B10' B9' B4' 108.2(2) . . ?
B10' B9' B8' 108.0(2) . . ?
B10' B9' H9' 120.5(16) . . ?
B10' B9' B12' 59.54(17) . . ?
B12' B9' H9' 121.5(16) . . ?
B5' B10' H10' 121.8(15) . . ?
B5' B10' B11' 108.1(2) . . ?
B6' B10' B5' 60.45(17) . . ?
B6' B10' B9' 108.6(2) . . ?
B6' B10' H10' 118.0(15) . . ?
B6' B10' B11' 59.99(17) . . ?
B6' B10' B12' 108.8(2) . . ?
B9' B10' B5' 59.71(17) . . ?
B9' B10' H10' 124.8(15) . . ?
B9' B10' B11' 108.4(2) . . ?
B11' B10' H10' 119.5(15) . . ?
B12' B10' B5' 108.5(2) . . ?
B12' B10' B9' 60.68(18) . . ?
B12' B10' H10' 123.0(15) . . ?
B12' B10' B11' 60.14(17) . . ?
C2' B11' B6' 60.25(16) . . ?
C2' B11' B7' 59.56(16) . . ?
C2' B11' B10' 104.9(2) . . ?
C2' B11' H11' 117.3(14) . . ?
C2' B11' B12' 105.4(2) . . ?
B6' B11' B7' 109.2(2) . . ?
B6' B11' B10' 58.48(17) . . ?
B6' B11' H11' 117.5(15) . . ?
B6' B11' B12' 107.0(2) . . ?
B7' B11' B10' 107.4(2) . . ?
B7' B11' H11' 120.8(15) . . ?
B7' B11' B12' 59.83(17) . . ?
B10' B11' H11' 127.0(15) . . ?
B12' B11' B10' 59.41(17) . . ?
B12' B11' H11' 129.0(15) . . ?
B7' B12' B8' 60.19(17) . . ?
B7' B12' B9' 107.7(2) . . ?
B7' B12' B11' 59.72(17) . . ?
B7' B12' H12' 122.9(14) . . ?
B8' B12' B9' 59.76(17) . . ?
B8' B12' H12' 122.9(14) . . ?
B9' B12' H12' 121.6(14) . . ?
B10' B12' B7' 108.1(2) . . ?
B10' B12' B8' 108.0(2) . . ?
B10' B12' B9' 59.78(18) . . ?
B10' B12' B11' 60.46(17) . . ?
B10' B12' H12' 120.2(15) . . ?
B11' B12' B8' 108.0(2) . . ?
B11' B12' B9' 107.9(2) . . ?
B11' B12' H12' 121.2(14) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P1 C2 B3 C1 101.60(19) . . . . ?
P1 C2 B3 B4 136.04(18) . . . . ?
P1 C2 B3 B7 -119.0(2) . . . . ?
P1 C2 B3 B8 -160.38(17) . . . . ?
P1 C2 B6 C1 -103.31(19) . . . . ?
P1 C2 B6 B5 -137.98(18) . . . . ?
P1 C2 B6 B10 158.22(18) . . . . ?
P1 C2 B6 B11 116.9(2) . . . . ?
P1 C2 B7 B3 104.8(2) . . . . ?
P1 C2 B7 B8 144.3(2) . . . . ?
P1 C2 B7 B11 -112.8(2) . . . . ?
P1 C2 B7 B12 -153.77(19) . . . . ?
P1 C2 B11 B6 -100.6(2) . . . . ?
P1 C2 B11 B7 117.4(2) . . . . ?
P1 C2 B11 B10 -140.11(19) . . . . ?
P1 C2 B11 B12 158.01(17) . . . . ?
P1 C11 C12 C13 -175.3(2) . . . . ?
P1 C11 C16 C15 176.5(2) . . . . ?
P1 C2' B3' C1' 105.55(17) . . . . ?
P1 C2' B3' B4' 139.64(18) . . . . ?
P1 C2' B3' B7' -115.38(18) . . . . ?
P1 C2' B3' B8' -156.10(17) . . . . ?
P1 C2' B6' C1' -96.6(2) . . . . ?
P1 C2' B6' B5' -131.5(2) . . . . ?
P1 C2' B6' B10' 164.91(18) . . . . ?
P1 C2' B6' B11' 123.9(2) . . . . ?
P1 C2' B7' B3' 92.7(2) . . . . ?
P1 C2' B7' B8' 131.59(19) . . . . ?
P1 C2' B7' B11' -125.5(2) . . . . ?
P1 C2' B7' B12' -165.68(17) . . . . ?
P1 C2' B11' B6' -113.5(2) . . . . ?
P1 C2' B11' B7' 105.6(2) . . . . ?
P1 C2' B11' B10' -152.7(2) . . . . ?
P1 C2' B11' B12' 145.5(2) . . . . ?
C1 C2 B3 B4 34.44(18) . . . . ?
C1 C2 B3 B7 139.4(2) . . . . ?
C1 C2 B3 B8 98.0(2) . . . . ?
C1 C2 B6 B5 -34.67(19) . . . . ?
C1 C2 B6 B10 -98.5(2) . . . . ?
C1 C2 B6 B11 -139.8(2) . . . . ?
C1 C2 B7 B3 -38.5(2) . . . . ?
C1 C2 B7 B8 0.9(3) . . . . ?
C1 C2 B7 B11 103.8(2) . . . . ?
C1 C2 B7 B12 62.9(3) . . . . ?
C1 C2 B11 B6 38.2(2) . . . . ?
C1 C2 B11 B7 -103.8(2) . . . . ?
C1 C2 B11 B10 -1.3(3) . . . . ?
C1 C2 B11 B12 -63.2(2) . . . . ?
C1 B3 B4 B5 34.85(19) . . . . ?
C1 B3 B4 B8 134.3(2) . . . . ?
C1 B3 B4 B9 97.7(2) . . . . ?
C1 B3 B7 C2 33.84(18) . . . . ?
C1 B3 B7 B8 -99.9(2) . . . . ?
C1 B3 B7 B11 0.0(3) . . . . ?
C1 B3 B7 B12 -63.7(3) . . . . ?
C1 B3 B8 B4 -39.16(19) . . . . ?
C1 B3 B8 B7 98.5(2) . . . . ?
C1 B3 B8 B9 -1.8(3) . . . . ?
C1 B3 B8 B12 62.3(3) . . . . ?
C1 B4 B5 B6 35.36(19) . . . . ?
C1 B4 B5 B9 134.4(2) . . . . ?
C1 B4 B5 B10 97.1(2) . . . . ?
C1 B4 B8 B3 40.05(19) . . . . ?
C1 B4 B8 B7 2.2(3) . . . . ?
C1 B4 B8 B9 -98.4(2) . . . . ?
C1 B4 B8 B12 -60.8(3) . . . . ?
C1 B4 B9 B5 -39.03(19) . . . . ?
C1 B4 B9 B8 98.9(2) . . . . ?
C1 B4 B9 B10 -1.4(3) . . . . ?
C1 B4 B9 B12 61.7(3) . . . . ?
C1 B5 B6 C2 33.67(18) . . . . ?
C1 B5 B6 B10 134.5(2) . . . . ?
C1 B5 B6 B11 95.7(2) . . . . ?
C1 B5 B9 B4 39.25(19) . . . . ?
C1 B5 B9 B8 1.4(3) . . . . ?
C1 B5 B9 B10 -99.0(2) . . . . ?
C1 B5 B9 B12 -61.8(3) . . . . ?
C1 B5 B10 B6 -40.02(19) . . . . ?
C1 B5 B10 B9 98.7(2) . . . . ?
C1 B5 B10 B11 -2.3(3) . . . . ?
C1 B5 B10 B12 61.1(3) . . . . ?
C1 B6 B10 B5 39.11(18) . . . . ?
C1 B6 B10 B9 2.2(3) . . . . ?
C1 B6 B10 B11 -98.7(2) . . . . ?
C1 B6 B10 B12 -61.7(3) . . . . ?
C1 B6 B11 C2 -33.69(18) . . . . ?
C1 B6 B11 B7 0.3(3) . . . . ?
C1 B6 B11 B10 100.0(2) . . . . ?
C1 B6 B11 B12 63.4(2) . . . . ?
C1 C1' C2' P1 11.4(2) . . . . ?
C1 C1' C2' B3' 109.4(2) . . . . ?
C1 C1' C2' B6' -109.0(2) . . . . ?
C1 C1' C2' B7' 147.0(2) . . . . ?
C1 C1' C2' B11' -146.5(2) . . . . ?
C1 C1' B3' C2' -101.4(2) . . . . ?
C1 C1' B3' B4' 118.2(2) . . . . ?
C1 C1' B3' B7' -137.2(2) . . . . ?
C1 C1' B3' B8' 158.6(2) . . . . ?
C1 C1' B4' B3' -103.4(3) . . . . ?
C1 C1' B4' B5' 116.1(3) . . . . ?
C1 C1' B4' B8' -142.0(2) . . . . ?
C1 C1' B4' B9' 155.8(2) . . . . ?
C1 C1' B5' B4' -115.9(3) . . . . ?
C1 C1' B5' B6' 103.0(3) . . . . ?
C1 C1' B5' B9' -155.9(2) . . . . ?
C1 C1' B5' B10' 141.9(2) . . . . ?
C1 C1' B6' C2' 101.8(2) . . . . ?
C1 C1' B6' B5' -118.7(2) . . . . ?
C1 C1' B6' B10' -159.2(2) . . . . ?
C1 C1' B6' B11' 136.8(2) . . . . ?
C2 P1 C11 C12 98.2(2) . . . . ?
C2 P1 C11 C16 -80.5(3) . . . . ?
C2 P1 C2' C1' -10.91(17) . . . . ?
C2 P1 C2' B3' -77.16(17) . . . . ?
C2 P1 C2' B6' 58.8(2) . . . . ?
C2 P1 C2' B7' -142.07(19) . . . . ?
C2 P1 C2' B11' 140.4(2) . . . . ?
C2 C1 B3 B4 -139.9(2) . . . . ?
C2 C1 B3 B7 -35.23(19) . . . . ?
C2 C1 B3 B8 -99.3(2) . . . . ?
C2 C1 B4 B3 37.23(19) . . . . ?
C2 C1 B4 B5 -103.2(2) . . . . ?
C2 C1 B4 B8 -1.7(3) . . . . ?
C2 C1 B4 B9 -63.6(2) . . . . ?
C2 C1 B5 B4 103.6(2) . . . . ?
C2 C1 B5 B6 -37.4(2) . . . . ?
C2 C1 B5 B9 63.8(2) . . . . ?
C2 C1 B5 B10 1.5(3) . . . . ?
C2 C1 B6 B5 139.6(2) . . . . ?
C2 C1 B6 B10 99.0(2) . . . . ?
C2 C1 B6 B11 35.09(19) . . . . ?
C2 C1 C1' C2' -5.5(3) . . . . ?
C2 C1 C1' B3' 62.2(3) . . . . ?
C2 C1 C1' B4' 134.5(2) . . . . ?
C2 C1 C1' B5' -146.1(2) . . . . ?
C2 C1 C1' B6' -73.7(3) . . . . ?
C2 B3 B4 C1 -33.43(18) . . . . ?
C2 B3 B4 B5 1.4(3) . . . . ?
C2 B3 B4 B8 100.9(2) . . . . ?
C2 B3 B4 B9 64.2(2) . . . . ?
C2 B3 B7 B8 -133.8(2) . . . . ?
C2 B3 B7 B11 -33.80(19) . . . . ?
C2 B3 B7 B12 -97.6(2) . . . . ?
C2 B3 B8 B4 -97.5(2) . . . . ?
C2 B3 B8 B7 40.19(19) . . . . ?
C2 B3 B8 B9 -60.1(3) . . . . ?
C2 B3 B8 B12 3.9(3) . . . . ?
C2 B6 B10 B5 97.6(2) . . . . ?
C2 B6 B10 B9 60.7(3) . . . . ?
C2 B6 B10 B11 -40.26(19) . . . . ?
C2 B6 B10 B12 -3.2(3) . . . . ?
C2 B6 B11 B7 33.96(19) . . . . ?
C2 B6 B11 B10 133.7(2) . . . . ?
C2 B6 B11 B12 97.1(2) . . . . ?
C2 B7 B8 B3 -40.09(19) . . . . ?
C2 B7 B8 B4 -1.9(3) . . . . ?
C2 B7 B8 B9 61.6(3) . . . . ?
C2 B7 B8 B12 99.2(2) . . . . ?
C2 B7 B11 B6 -34.22(19) . . . . ?
C2 B7 B11 B10 -96.3(2) . . . . ?
C2 B7 B11 B12 -133.2(2) . . . . ?
C2 B7 B12 B8 -98.0(2) . . . . ?
C2 B7 B12 B9 -60.6(3) . . . . ?
C2 B7 B12 B10 3.1(3) . . . . ?
C2 B7 B12 B11 40.40(19) . . . . ?
C2 B11 B12 B7 -40.20(19) . . . . ?
C2 B11 B12 B8 -2.6(3) . . . . ?
C2 B11 B12 B9 60.9(2) . . . . ?
C2 B11 B12 B10 98.3(2) . . . . ?
B3 C1 C2 P1 -111.27(19) . . . . ?
B3 C1 C2 B6 142.3(2) . . . . ?
B3 C1 C2 B7 37.8(2) . . . . ?
B3 C1 C2 B11 104.8(2) . . . . ?
B3 C1 B4 B5 -140.5(2) . . . . ?
B3 C1 B4 B8 -38.96(19) . . . . ?
B3 C1 B4 B9 -100.9(2) . . . . ?
B3 C1 B5 B4 37.2(2) . . . . ?
B3 C1 B5 B6 -103.8(2) . . . . ?
B3 C1 B5 B9 -2.6(3) . . . . ?
B3 C1 B5 B10 -64.9(3) . . . . ?
B3 C1 B6 C2 -35.34(19) . . . . ?
B3 C1 B6 B5 104.3(2) . . . . ?
B3 C1 B6 B10 63.7(2) . . . . ?
B3 C1 B6 B11 -0.2(3) . . . . ?
B3 C1 C1' C2' 61.8(3) . . . . ?
B3 C1 C1' B3' 129.5(2) . . . . ?
B3 C1 C1' B4' -158.3(2) . . . . ?
B3 C1 C1' B5' -78.9(3) . . . . ?
B3 C1 C1' B6' -6.4(3) . . . . ?
B3 C2 B6 C1 36.7(2) . . . . ?
B3 C2 B6 B5 2.0(3) . . . . ?
B3 C2 B6 B10 -61.8(3) . . . . ?
B3 C2 B6 B11 -103.1(2) . . . . ?
B3 C2 B7 B8 39.43(19) . . . . ?
B3 C2 B7 B11 142.3(2) . . . . ?
B3 C2 B7 B12 101.4(2) . . . . ?
B3 C2 B11 B6 106.6(2) . . . . ?
B3 C2 B11 B7 -35.4(2) . . . . ?
B3 C2 B11 B10 67.1(2) . . . . ?
B3 C2 B11 B12 5.2(3) . . . . ?
B3 B4 B5 C1 -35.65(19) . . . . ?
B3 B4 B5 B6 -0.3(3) . . . . ?
B3 B4 B5 B9 98.7(2) . . . . ?
B3 B4 B5 B10 61.5(3) . . . . ?
B3 B4 B8 B7 -37.8(2) . . . . ?
B3 B4 B8 B9 -138.4(2) . . . . ?
B3 B4 B8 B12 -100.9(2) . . . . ?
B3 B4 B9 B5 -101.9(2) . . . . ?
B3 B4 B9 B8 36.0(2) . . . . ?
B3 B4 B9 B10 -64.3(3) . . . . ?
B3 B4 B9 B12 -1.2(3) . . . . ?
B3 B7 B8 B4 38.1(2) . . . . ?
B3 B7 B8 B9 101.7(2) . . . . ?
B3 B7 B8 B12 139.2(2) . . . . ?
B3 B7 B11 C2 34.0(2) . . . . ?
B3 B7 B11 B6 -0.2(3) . . . . ?
B3 B7 B11 B10 -62.3(3) . . . . ?
B3 B7 B11 B12 -99.2(2) . . . . ?
B3 B7 B12 B8 -35.6(2) . . . . ?
B3 B7 B12 B9 1.9(3) . . . . ?
B3 B7 B12 B10 65.6(3) . . . . ?
B3 B7 B12 B11 102.8(2) . . . . ?
B3 B8 B9 B4 -37.7(2) . . . . ?
B3 B8 B9 B5 0.3(3) . . . . ?
B3 B8 B9 B10 64.1(3) . . . . ?
B3 B8 B9 B12 100.7(2) . . . . ?
B3 B8 B12 B7 36.5(2) . . . . ?
B3 B8 B12 B9 -101.7(2) . . . . ?
B3 B8 B12 B10 -64.7(3) . . . . ?
B3 B8 B12 B11 -0.8(3) . . . . ?
B4 C1 C2 P1 -148.54(17) . . . . ?
B4 C1 C2 B3 -37.27(19) . . . . ?
B4 C1 C2 B6 105.1(2) . . . . ?
B4 C1 C2 B7 0.5(3) . . . . ?
B4 C1 C2 B11 67.6(2) . . . . ?
B4 C1 B3 C2 139.9(2) . . . . ?
B4 C1 B3 B7 104.6(2) . . . . ?
B4 C1 B3 B8 40.6(2) . . . . ?
B4 C1 B5 B6 -141.0(2) . . . . ?
B4 C1 B5 B9 -39.8(2) . . . . ?
B4 C1 B5 B10 -102.1(2) . . . . ?
B4 C1 B6 C2 -102.3(2) . . . . ?
B4 C1 B6 B5 37.3(2) . . . . ?
B4 C1 B6 B10 -3.3(3) . . . . ?
B4 C1 B6 B11 -67.2(2) . . . . ?
B4 C1 C1' C2' 134.0(2) . . . . ?
B4 C1 C1' B3' -158.3(2) . . . . ?
B4 C1 C1' B4' -86.1(3) . . . . ?
B4 C1 C1' B5' -6.7(4) . . . . ?
B4 C1 C1' B6' 65.8(3) . . . . ?
B4 B3 B7 C2 94.9(2) . . . . ?
B4 B3 B7 B8 -38.8(2) . . . . ?
B4 B3 B7 B11 61.1(3) . . . . ?
B4 B3 B7 B12 -2.6(3) . . . . ?
B4 B3 B8 B7 137.7(2) . . . . ?
B4 B3 B8 B9 37.4(2) . . . . ?
B4 B3 B8 B12 101.4(2) . . . . ?
B4 B5 B6 C1 -34.66(19) . . . . ?
B4 B5 B6 C2 -1.0(3) . . . . ?
B4 B5 B6 B10 99.8(2) . . . . ?
B4 B5 B6 B11 61.0(3) . . . . ?
B4 B5 B9 B8 -37.8(2) . . . . ?
B4 B5 B9 B10 -138.3(2) . . . . ?
B4 B5 B9 B12 -101.0(2) . . . . ?
B4 B5 B10 B6 -101.5(2) . . . . ?
B4 B5 B10 B9 37.2(2) . . . . ?
B4 B5 B10 B11 -63.8(3) . . . . ?
B4 B5 B10 B12 -0.3(3) . . . . ?
B4 B8 B9 B5 37.9(2) . . . . ?
B4 B8 B9 B10 101.7(2) . . . . ?
B4 B8 B9 B12 138.3(2) . . . . ?
B4 B8 B12 B7 100.7(2) . . . . ?
B4 B8 B12 B9 -37.4(2) . . . . ?
B4 B8 B12 B10 -0.5(3) . . . . ?
B4 B8 B12 B11 63.4(3) . . . . ?
B4 B9 B10 B5 -37.7(2) . . . . ?
B4 B9 B10 B6 -0.5(3) . . . . ?
B4 B9 B10 B11 63.1(3) . . . . ?
B4 B9 B10 B12 100.5(2) . . . . ?
B4 B9 B12 B7 -0.4(3) . . . . ?
B4 B9 B12 B8 37.4(2) . . . . ?
B4 B9 B12 B10 -101.4(2) . . . . ?
B4 B9 B12 B11 -63.9(3) . . . . ?
B5 C1 C2 P1 143.78(17) . . . . ?
B5 C1 C2 B3 -105.0(2) . . . . ?
B5 C1 C2 B6 37.4(2) . . . . ?
B5 C1 C2 B7 -67.2(2) . . . . ?
B5 C1 C2 B11 -0.1(3) . . . . ?
B5 C1 B3 C2 102.1(2) . . . . ?
B5 C1 B3 B4 -37.7(2) . . . . ?
B5 C1 B3 B7 66.9(3) . . . . ?
B5 C1 B3 B8 2.8(3) . . . . ?
B5 C1 B4 B3 140.5(2) . . . . ?
B5 C1 B4 B8 101.5(2) . . . . ?
B5 C1 B4 B9 39.61(19) . . . . ?
B5 C1 B6 C2 -139.6(2) . . . . ?
B5 C1 B6 B10 -40.60(19) . . . . ?
B5 C1 B6 B11 -104.5(2) . . . . ?
B5 C1 C1' C2' -145.1(2) . . . . ?
B5 C1 C1' B3' -77.4(3) . . . . ?
B5 C1 C1' B4' -5.2(4) . . . . ?
B5 C1 C1' B5' 74.2(3) . . . . ?
B5 C1 C1' B6' 146.7(2) . . . . ?
B5 B4 B8 B3 101.1(2) . . . . ?
B5 B4 B8 B7 63.3(3) . . . . ?
B5 B4 B8 B9 -37.3(2) . . . . ?
B5 B4 B8 B12 0.2(3) . . . . ?
B5 B4 B9 B8 137.9(2) . . . . ?
B5 B4 B9 B10 37.6(2) . . . . ?
B5 B4 B9 B12 100.8(2) . . . . ?
B5 B6 B10 B9 -36.9(2) . . . . ?
B5 B6 B10 B11 -137.9(2) . . . . ?
B5 B6 B10 B12 -100.8(2) . . . . ?
B5 B6 B11 C2 -94.9(2) . . . . ?
B5 B6 B11 B7 -61.0(3) . . . . ?
B5 B6 B11 B10 38.8(2) . . . . ?
B5 B6 B11 B12 2.2(3) . . . . ?
B5 B9 B10 B6 37.1(2) . . . . ?
B5 B9 B10 B11 100.8(2) . . . . ?
B5 B9 B10 B12 138.1(2) . . . . ?
B5 B9 B12 B7 63.4(3) . . . . ?
B5 B9 B12 B8 101.3(2) . . . . ?
B5 B9 B12 B10 -37.5(2) . . . . ?
B5 B9 B12 B11 -0.1(3) . . . . ?
B5 B10 B11 C2 2.2(3) . . . . ?
B5 B10 B11 B6 -37.8(2) . . . . ?
B5 B10 B11 B7 63.8(3) . . . . ?
B5 B10 B11 B12 100.8(2) . . . . ?
B5 B10 B12 B7 -63.8(3) . . . . ?
B5 B10 B12 B8 0.5(3) . . . . ?
B5 B10 B12 B9 37.4(2) . . . . ?
B5 B10 B12 B11 -100.9(2) . . . . ?
B6 C1 C2 P1 106.39(19) . . . . ?
B6 C1 C2 B3 -142.3(2) . . . . ?
B6 C1 C2 B7 -104.5(2) . . . . ?
B6 C1 C2 B11 -37.5(2) . . . . ?
B6 C1 B3 C2 35.36(19) . . . . ?
B6 C1 B3 B4 -104.5(2) . . . . ?
B6 C1 B3 B7 0.1(3) . . . . ?
B6 C1 B3 B8 -63.9(3) . . . . ?
B6 C1 B4 B3 103.8(2) . . . . ?
B6 C1 B4 B5 -36.7(2) . . . . ?
B6 C1 B4 B8 64.8(2) . . . . ?
B6 C1 B4 B9 2.9(3) . . . . ?
B6 C1 B5 B4 141.0(2) . . . . ?
B6 C1 B5 B9 101.2(2) . . . . ?
B6 C1 B5 B10 38.94(19) . . . . ?
B6 C1 C1' C2' -72.8(2) . . . . ?
B6 C1 C1' B3' -5.1(3) . . . . ?
B6 C1 C1' B4' 67.1(3) . . . . ?
B6 C1 C1' B5' 146.5(2) . . . . ?
B6 C1 C1' B6' -141.1(2) . . . . ?
B6 C2 B3 C1 -36.6(2) . . . . ?
B6 C2 B3 B4 -2.2(3) . . . . ?
B6 C2 B3 B7 102.8(2) . . . . ?
B6 C2 B3 B8 61.4(3) . . . . ?
B6 C2 B7 B3 -106.7(2) . . . . ?
B6 C2 B7 B8 -67.3(2) . . . . ?
B6 C2 B7 B11 35.6(2) . . . . ?
B6 C2 B7 B12 -5.3(3) . . . . ?
B6 C2 B11 B7 -142.0(2) . . . . ?
B6 C2 B11 B10 -39.52(19) . . . . ?
B6 C2 B11 B12 -101.4(2) . . . . ?
B6 B5 B9 B4 102.4(2) . . . . ?
B6 B5 B9 B8 64.5(3) . . . . ?
B6 B5 B9 B10 -35.88(19) . . . . ?
B6 B5 B9 B12 1.4(3) . . . . ?
B6 B5 B10 B9 138.7(2) . . . . ?
B6 B5 B10 B11 37.7(2) . . . . ?
B6 B5 B10 B12 101.2(2) . . . . ?
B6 B10 B11 C2 40.07(19) . . . . ?
B6 B10 B11 B7 101.7(2) . . . . ?
B6 B10 B11 B12 138.6(2) . . . . ?
B6 B10 B12 B7 0.0(3) . . . . ?
B6 B10 B12 B8 64.3(3) . . . . ?
B6 B10 B12 B9 101.2(2) . . . . ?
B6 B10 B12 B11 -37.1(2) . . . . ?
B6 B11 B12 B7 -102.4(2) . . . . ?
B6 B11 B12 B8 -64.8(3) . . . . ?
B6 B11 B12 B9 -1.3(3) . . . . ?
B6 B11 B12 B10 36.1(2) . . . . ?
B7 C2 B3 C1 -139.4(2) . . . . ?
B7 C2 B3 B4 -105.0(2) . . . . ?
B7 C2 B3 B8 -41.4(2) . . . . ?
B7 C2 B6 C1 103.9(2) . . . . ?
B7 C2 B6 B5 69.2(3) . . . . ?
B7 C2 B6 B10 5.4(3) . . . . ?
B7 C2 B6 B11 -35.9(2) . . . . ?
B7 C2 B11 B6 142.0(2) . . . . ?
B7 C2 B11 B10 102.4(2) . . . . ?
B7 C2 B11 B12 40.57(19) . . . . ?
B7 B3 B4 C1 -95.3(2) . . . . ?
B7 B3 B4 B5 -60.4(3) . . . . ?
B7 B3 B4 B8 39.0(2) . . . . ?
B7 B3 B4 B9 2.4(3) . . . . ?
B7 B3 B8 B4 -137.7(2) . . . . ?
B7 B3 B8 B9 -100.3(2) . . . . ?
B7 B3 B8 B12 -36.3(2) . . . . ?
B7 B8 B9 B4 -101.1(2) . . . . ?
B7 B8 B9 B5 -63.2(3) . . . . ?
B7 B8 B9 B10 0.6(3) . . . . ?
B7 B8 B9 B12 37.2(2) . . . . ?
B7 B8 B12 B9 -138.1(2) . . . . ?
B7 B8 B12 B10 -101.2(2) . . . . ?
B7 B8 B12 B11 -37.3(2) . . . . ?
B7 B11 B12 B8 37.6(2) . . . . ?
B7 B11 B12 B9 101.1(2) . . . . ?
B7 B11 B12 B10 138.5(2) . . . . ?
B8 B3 B4 C1 -134.3(2) . . . . ?
B8 B3 B4 B5 -99.5(2) . . . . ?
B8 B3 B4 B9 -36.7(2) . . . . ?
B8 B3 B7 C2 133.8(2) . . . . ?
B8 B3 B7 B11 100.0(2) . . . . ?
B8 B3 B7 B12 36.2(2) . . . . ?
B8 B4 B5 C1 -97.0(2) . . . . ?
B8 B4 B5 B6 -61.7(3) . . . . ?
B8 B4 B5 B9 37.3(2) . . . . ?
B8 B4 B5 B10 0.1(3) . . . . ?
B8 B4 B9 B5 -137.9(2) . . . . ?
B8 B4 B9 B10 -100.3(2) . . . . ?
B8 B4 B9 B12 -37.2(2) . . . . ?
B8 B7 B11 C2 96.1(2) . . . . ?
B8 B7 B11 B6 61.9(3) . . . . ?
B8 B7 B11 B10 -0.2(3) . . . . ?
B8 B7 B11 B12 -37.1(2) . . . . ?
B8 B7 B12 B9 37.5(2) . . . . ?
B8 B7 B12 B10 101.2(2) . . . . ?
B8 B7 B12 B11 138.4(2) . . . . ?
B8 B9 B10 B5 -101.5(2) . . . . ?
B8 B9 B10 B6 -64.3(3) . . . . ?
B8 B9 B10 B11 -0.7(3) . . . . ?
B8 B9 B10 B12 36.6(2) . . . . ?
B8 B9 B12 B7 -37.8(2) . . . . ?
B8 B9 B12 B10 -138.8(2) . . . . ?
B8 B9 B12 B11 -101.3(2) . . . . ?
B9 B4 B5 C1 -134.4(2) . . . . ?
B9 B4 B5 B6 -99.0(2) . . . . ?
B9 B4 B5 B10 -37.3(2) . . . . ?
B9 B4 B8 B3 138.4(2) . . . . ?
B9 B4 B8 B7 100.6(2) . . . . ?
B9 B4 B8 B12 37.6(2) . . . . ?
B9 B5 B6 C1 -97.9(2) . . . . ?
B9 B5 B6 C2 -64.2(2) . . . . ?
B9 B5 B6 B10 36.6(2) . . . . ?
B9 B5 B6 B11 -2.2(3) . . . . ?
B9 B5 B10 B6 -138.7(2) . . . . ?
B9 B5 B10 B11 -101.0(2) . . . . ?
B9 B5 B10 B12 -37.6(2) . . . . ?
B9 B8 B12 B7 138.1(2) . . . . ?
B9 B8 B12 B10 36.9(2) . . . . ?
B9 B8 B12 B11 100.8(2) . . . . ?
B9 B10 B11 C2 -61.1(3) . . . . ?
B9 B10 B11 B6 -101.1(2) . . . . ?
B9 B10 B11 B7 0.6(3) . . . . ?
B9 B10 B11 B12 37.5(2) . . . . ?
B9 B10 B12 B7 -101.2(2) . . . . ?
B9 B10 B12 B8 -36.9(2) . . . . ?
B9 B10 B12 B11 -138.3(2) . . . . ?
B10 B5 B6 C1 -134.5(2) . . . . ?
B10 B5 B6 C2 -100.8(2) . . . . ?
B10 B5 B6 B11 -38.8(2) . . . . ?
B10 B5 B9 B4 138.3(2) . . . . ?
B10 B5 B9 B8 100.4(2) . . . . ?
B10 B5 B9 B12 37.2(2) . . . . ?
B10 B6 B11 C2 -133.7(2) . . . . ?
B10 B6 B11 B7 -99.8(2) . . . . ?
B10 B6 B11 B12 -36.6(2) . . . . ?
B10 B9 B12 B7 101.0(2) . . . . ?
B10 B9 B12 B8 138.8(2) . . . . ?
B10 B9 B12 B11 37.5(2) . . . . ?
B10 B11 B12 B7 -138.5(2) . . . . ?
B10 B11 B12 B8 -100.9(2) . . . . ?
B10 B11 B12 B9 -37.4(2) . . . . ?
C11 P1 C2 C1 118.98(17) . . . . ?
C11 P1 C2 B3 49.1(2) . . . . ?
C11 P1 C2 B6 -172.34(17) . . . . ?
C11 P1 C2 B7 -24.3(2) . . . . ?
C11 P1 C2 B11 -102.3(2) . . . . ?
C11 P1 C2' C1' -114.84(17) . . . . ?
C11 P1 C2' B3' 178.91(16) . . . . ?
C11 P1 C2' B6' -45.1(2) . . . . ?
C11 P1 C2' B7' 114.01(19) . . . . ?
C11 P1 C2' B11' 36.5(3) . . . . ?
C11 C12 C13 C14 -2.7(4) . . . . ?
B11 C2 B3 C1 -103.8(2) . . . . ?
B11 C2 B3 B4 -69.4(2) . . . . ?
B11 C2 B3 B7 35.6(2) . . . . ?
B11 C2 B3 B8 -5.8(3) . . . . ?
B11 C2 B6 C1 139.8(2) . . . . ?
B11 C2 B6 B5 105.1(2) . . . . ?
B11 C2 B6 B10 41.3(2) . . . . ?
B11 C2 B7 B3 -142.3(2) . . . . ?
B11 C2 B7 B8 -102.9(2) . . . . ?
B11 C2 B7 B12 -40.9(2) . . . . ?
B11 B6 B10 B5 137.9(2) . . . . ?
B11 B6 B10 B9 101.0(2) . . . . ?
B11 B6 B10 B12 37.1(2) . . . . ?
B11 B7 B8 B3 -101.9(2) . . . . ?
B11 B7 B8 B4 -63.8(3) . . . . ?
B11 B7 B8 B9 -0.3(3) . . . . ?
B11 B7 B8 B12 37.3(2) . . . . ?
B11 B7 B12 B8 -138.4(2) . . . . ?
B11 B7 B12 B9 -101.0(2) . . . . ?
B11 B7 B12 B10 -37.3(2) . . . . ?
B11 B10 B12 B7 37.1(2) . . . . ?
B11 B10 B12 B8 101.4(2) . . . . ?
B11 B10 B12 B9 138.3(2) . . . . ?
C12 C11 C16 C15 -2.1(4) . . . . ?
C12 C13 C14 C15 0.3(4) . . . . ?
B12 B7 B8 B3 -139.2(2) . . . . ?
B12 B7 B8 B4 -101.1(2) . . . . ?
B12 B7 B8 B9 -37.6(2) . . . . ?
B12 B7 B11 C2 133.2(2) . . . . ?
B12 B7 B11 B6 99.0(2) . . . . ?
B12 B7 B11 B10 36.9(2) . . . . ?
B12 B8 B9 B4 -138.3(2) . . . . ?
B12 B8 B9 B5 -100.4(2) . . . . ?
B12 B8 B9 B10 -36.6(2) . . . . ?
B12 B9 B10 B5 -138.1(2) . . . . ?
B12 B9 B10 B6 -101.0(2) . . . . ?
B12 B9 B10 B11 -37.4(2) . . . . ?
B12 B10 B11 C2 -98.5(2) . . . . ?
B12 B10 B11 B6 -138.6(2) . . . . ?
B12 B10 B11 B7 -36.9(2) . . . . ?
C13 C14 C15 C16 1.1(4) . . . . ?
C14 C15 C16 C11 -0.1(4) . . . . ?
C16 C11 C12 C13 3.5(4) . . . . ?
C1' C1 C2 P1 -2.6(2) . . . . ?
C1' C1 C2 B3 108.7(2) . . . . ?
C1' C1 C2 B6 -109.0(2) . . . . ?
C1' C1 C2 B7 146.5(2) . . . . ?
C1' C1 C2 B11 -146.5(2) . . . . ?
C1' C1 B3 C2 -101.0(2) . . . . ?
C1' C1 B3 B4 119.2(2) . . . . ?
C1' C1 B3 B7 -136.2(2) . . . . ?
C1' C1 B3 B8 159.7(2) . . . . ?
C1' C1 B4 B3 -102.3(3) . . . . ?
C1' C1 B4 B5 117.2(3) . . . . ?
C1' C1 B4 B8 -141.2(2) . . . . ?
C1' C1 B4 B9 156.9(2) . . . . ?
C1' C1 B5 B4 -116.6(3) . . . . ?
C1' C1 B5 B6 102.4(3) . . . . ?
C1' C1 B5 B9 -156.4(2) . . . . ?
C1' C1 B5 B10 141.3(2) . . . . ?
C1' C1 B6 C2 100.9(2) . . . . ?
C1' C1 B6 B5 -119.5(2) . . . . ?
C1' C1 B6 B10 -160.1(2) . . . . ?
C1' C1 B6 B11 136.0(2) . . . . ?
C1' C2' B3' B4' 34.09(18) . . . . ?
C1' C2' B3' B7' 139.1(2) . . . . ?
C1' C2' B3' B8' 98.4(2) . . . . ?
C1' C2' B6' B5' -34.90(19) . . . . ?
C1' C2' B6' B10' -98.5(2) . . . . ?
C1' C2' B6' B11' -139.5(2) . . . . ?
C1' C2' B7' B3' -38.5(2) . . . . ?
C1' C2' B7' B8' 0.4(3) . . . . ?
C1' C2' B7' B11' 103.3(2) . . . . ?
C1' C2' B7' B12' 63.1(2) . . . . ?
C1' C2' B11' B6' 37.82(19) . . . . ?
C1' C2' B11' B7' -103.1(2) . . . . ?
C1' C2' B11' B10' -1.4(3) . . . . ?
C1' C2' B11' B12' -63.2(2) . . . . ?
C1' B3' B4' B5' 35.20(19) . . . . ?
C1' B3' B4' B8' 135.0(2) . . . . ?
C1' B3' B4' B9' 98.1(2) . . . . ?
C1' B3' B7' C2' 34.33(17) . . . . ?
C1' B3' B7' B8' -100.5(2) . . . . ?
C1' B3' B7' B11' 0.4(3) . . . . ?
C1' B3' B7' B12' -63.6(2) . . . . ?
C1' B3' B8' B4' -38.79(18) . . . . ?
C1' B3' B8' B7' 98.6(2) . . . . ?
C1' B3' B8' B9' -1.6(3) . . . . ?
C1' B3' B8' B12' 62.0(2) . . . . ?
C1' B4' B5' B6' 35.04(19) . . . . ?
C1' B4' B5' B9' 134.4(2) . . . . ?
C1' B4' B5' B10' 96.8(2) . . . . ?
C1' B4' B8' B3' 39.78(19) . . . . ?
C1' B4' B8' B7' 2.0(3) . . . . ?
C1' B4' B8' B9' -98.5(2) . . . . ?
C1' B4' B8' B12' -60.8(3) . . . . ?
C1' B4' B9' B5' -39.27(19) . . . . ?
C1' B4' B9' B8' 99.4(2) . . . . ?
C1' B4' B9' B10' -1.3(3) . . . . ?
C1' B4' B9' B12' 61.7(3) . . . . ?
C1' B5' B6' C2' 33.96(18) . . . . ?
C1' B5' B6' B10' 134.5(2) . . . . ?
C1' B5' B6' B11' 95.4(2) . . . . ?
C1' B5' B9' B4' 39.31(18) . . . . ?
C1' B5' B9' B8' 2.0(3) . . . . ?
C1' B5' B9' B10' -98.5(2) . . . . ?
C1' B5' B9' B12' -61.6(3) . . . . ?
C1' B5' B10' B6' -39.78(19) . . . . ?
C1' B5' B10' B9' 99.2(2) . . . . ?
C1' B5' B10' B11' -1.9(3) . . . . ?
C1' B5' B10' B12' 61.8(3) . . . . ?
C1' B6' B10' B5' 39.22(19) . . . . ?
C1' B6' B10' B9' 2.5(3) . . . . ?
C1' B6' B10' B11' -98.4(2) . . . . ?
C1' B6' B10' B12' -61.9(3) . . . . ?
C1' B6' B11' C2' -33.97(17) . . . . ?
C1' B6' B11' B7' 1.2(3) . . . . ?
C1' B6' B11' B10' 100.2(2) . . . . ?
C1' B6' B11' B12' 64.4(2) . . . . ?
C2' P1 C2 C1 7.97(18) . . . . ?
C2' P1 C2 B3 -61.90(19) . . . . ?
C2' P1 C2 B6 76.65(18) . . . . ?
C2' P1 C2 B7 -135.3(2) . . . . ?
C2' P1 C2 B11 146.7(2) . . . . ?
C2' P1 C11 C12 -164.14(18) . . . . ?
C2' P1 C11 C16 17.2(3) . . . . ?
C2' C1' B3' B4' -140.4(2) . . . . ?
C2' C1' B3' B7' -35.78(18) . . . . ?
C2' C1' B3' B8' -100.0(2) . . . . ?
C2' C1' B4' B3' 36.8(2) . . . . ?
C2' C1' B4' B5' -103.7(2) . . . . ?
C2' C1' B4' B8' -1.8(3) . . . . ?
C2' C1' B4' B9' -64.0(2) . . . . ?
C2' C1' B5' B4' 103.3(2) . . . . ?
C2' C1' B5' B6' -37.86(19) . . . . ?
C2' C1' B5' B9' 63.3(2) . . . . ?
C2' C1' B5' B10' 1.1(3) . . . . ?
C2' C1' B6' B5' 139.5(2) . . . . ?
C2' C1' B6' B10' 99.0(2) . . . . ?
C2' C1' B6' B11' 34.98(18) . . . . ?
C2' B3' B4' C1' -33.22(18) . . . . ?
C2' B3' B4' B5' 2.0(3) . . . . ?
C2' B3' B4' B8' 101.8(2) . . . . ?
C2' B3' B4' B9' 64.9(2) . . . . ?
C2' B3' B7' B8' -134.9(2) . . . . ?
C2' B3' B7' B11' -33.96(19) . . . . ?
C2' B3' B7' B12' -97.9(2) . . . . ?
C2' B3' B8' B4' -97.7(2) . . . . ?
C2' B3' B8' B7' 39.73(19) . . . . ?
C2' B3' B8' B9' -60.5(3) . . . . ?
C2' B3' B8' B12' 3.1(3) . . . . ?
C2' B6' B10' B5' 98.0(2) . . . . ?
C2' B6' B10' B9' 61.4(3) . . . . ?
C2' B6' B10' B11' -39.59(19) . . . . ?
C2' B6' B10' B12' -3.1(3) . . . . ?
C2' B6' B11' B7' 35.15(19) . . . . ?
C2' B6' B11' B10' 134.2(2) . . . . ?
C2' B6' B11' B12' 98.4(2) . . . . ?
C2' B7' B8' B3' -39.49(19) . . . . ?
C2' B7' B8' B4' -1.5(3) . . . . ?
C2' B7' B8' B9' 61.5(3) . . . . ?
C2' B7' B8' B12' 99.2(2) . . . . ?
C2' B7' B11' B6' -35.43(19) . . . . ?
C2' B7' B11' B10' -97.3(2) . . . . ?
C2' B7' B11' B12' -134.3(2) . . . . ?
C2' B7' B12' B8' -99.0(2) . . . . ?
C2' B7' B12' B9' -61.4(2) . . . . ?
C2' B7' B12' B10' 1.7(3) . . . . ?
C2' B7' B12' B11' 39.37(19) . . . . ?
C2' B11' B12' B7' -39.78(19) . . . . ?
C2' B11' B12' B8' -2.5(3) . . . . ?
C2' B11' B12' B9' 60.7(3) . . . . ?
C2' B11' B12' B10' 98.4(2) . . . . ?
B3' C1' C2' P1 -97.99(18) . . . . ?
B3' C1' C2' B6' 141.7(2) . . . . ?
B3' C1' C2' B7' 37.6(2) . . . . ?
B3' C1' C2' B11' 104.2(2) . . . . ?
B3' C1' B4' B5' -140.4(2) . . . . ?
B3' C1' B4' B8' -38.59(19) . . . . ?
B3' C1' B4' B9' -100.8(2) . . . . ?
B3' C1' B5' B4' 36.9(2) . . . . ?
B3' C1' B5' B6' -104.2(2) . . . . ?
B3' C1' B5' B9' -3.1(3) . . . . ?
B3' C1' B5' B10' -65.3(2) . . . . ?
B3' C1' B6' C2' -35.95(19) . . . . ?
B3' C1' B6' B5' 103.5(2) . . . . ?
B3' C1' B6' B10' 63.0(2) . . . . ?
B3' C1' B6' B11' -1.0(3) . . . . ?
B3' C2' B6' C1' 36.82(19) . . . . ?
B3' C2' B6' B5' 1.9(3) . . . . ?
B3' C2' B6' B10' -61.7(3) . . . . ?
B3' C2' B6' B11' -102.7(2) . . . . ?
B3' C2' B7' B8' 38.88(19) . . . . ?
B3' C2' B7' B11' 141.8(2) . . . . ?
B3' C2' B7' B12' 101.6(2) . . . . ?
B3' C2' B11' B6' 105.5(2) . . . . ?
B3' C2' B11' B7' -35.4(2) . . . . ?
B3' C2' B11' B10' 66.3(3) . . . . ?
B3' C2' B11' B12' 4.5(3) . . . . ?
B3' B4' B5' C1' -35.93(19) . . . . ?
B3' B4' B5' B6' -0.9(3) . . . . ?
B3' B4' B5' B9' 98.5(2) . . . . ?
B3' B4' B5' B10' 60.9(3) . . . . ?
B3' B4' B8' B7' -37.8(2) . . . . ?
B3' B4' B8' B9' -138.3(2) . . . . ?
B3' B4' B8' B12' -100.6(2) . . . . ?
B3' B4' B9' B5' -102.6(2) . . . . ?
B3' B4' B9' B8' 36.13(19) . . . . ?
B3' B4' B9' B10' -64.6(3) . . . . ?
B3' B4' B9' B12' -1.6(3) . . . . ?
B3' B7' B8' B4' 38.0(2) . . . . ?
B3' B7' B8' B9' 101.0(2) . . . . ?
B3' B7' B8' B12' 138.7(2) . . . . ?
B3' B7' B11' C2' 34.44(19) . . . . ?
B3' B7' B11' B6' -1.0(3) . . . . ?
B3' B7' B11' B10' -62.9(3) . . . . ?
B3' B7' B11' B12' -99.9(2) . . . . ?
B3' B7' B12' B8' -36.24(19) . . . . ?
B3' B7' B12' B9' 1.3(3) . . . . ?
B3' B7' B12' B10' 64.5(3) . . . . ?
B3' B7' B12' B11' 102.1(2) . . . . ?
B3' B8' B9' B4' -37.4(2) . . . . ?
B3' B8' B9' B5' -0.2(3) . . . . ?
B3' B8' B9' B10' 63.8(3) . . . . ?
B3' B8' B9' B12' 100.5(2) . . . . ?
B3' B8' B12' B7' 36.7(2) . . . . ?
B3' B8' B12' B9' -101.0(2) . . . . ?
B3' B8' B12' B10' -64.3(3) . . . . ?
B3' B8' B12' B11' -0.4(3) . . . . ?
B4' C1' C2' P1 -134.68(17) . . . . ?
B4' C1' C2' B3' -36.7(2) . . . . ?
B4' C1' C2' B6' 105.0(2) . . . . ?
B4' C1' C2' B7' 0.9(3) . . . . ?
B4' C1' C2' B11' 67.5(2) . . . . ?
B4' C1' B3' C2' 140.4(2) . . . . ?
B4' C1' B3' B7' 104.6(2) . . . . ?
B4' C1' B3' B8' 40.4(2) . . . . ?
B4' C1' B5' B6' -141.1(2) . . . . ?
B4' C1' B5' B9' -40.0(2) . . . . ?
B4' C1' B5' B10' -102.2(2) . . . . ?
B4' C1' B6' C2' -102.6(2) . . . . ?
B4' C1' B6' B5' 36.9(2) . . . . ?
B4' C1' B6' B10' -3.6(3) . . . . ?
B4' C1' B6' B11' -67.6(2) . . . . ?
B4' B3' B7' C2' 95.5(2) . . . . ?
B4' B3' B7' B8' -39.3(2) . . . . ?
B4' B3' B7' B11' 61.6(3) . . . . ?
B4' B3' B7' B12' -2.4(3) . . . . ?
B4' B3' B8' B7' 137.4(2) . . . . ?
B4' B3' B8' B9' 37.2(2) . . . . ?
B4' B3' B8' B12' 100.8(2) . . . . ?
B4' B5' B6' C1' -34.53(19) . . . . ?
B4' B5' B6' C2' -0.6(3) . . . . ?
B4' B5' B6' B10' 99.9(2) . . . . ?
B4' B5' B6' B11' 60.9(3) . . . . ?
B4' B5' B9' B8' -37.3(2) . . . . ?
B4' B5' B9' B10' -137.8(2) . . . . ?
B4' B5' B9' B12' -100.9(2) . . . . ?
B4' B5' B10' B6' -101.3(2) . . . . ?
B4' B5' B10' B9' 37.7(2) . . . . ?
B4' B5' B10' B11' -63.4(3) . . . . ?
B4' B5' B10' B12' 0.3(3) . . . . ?
B4' B8' B9' B5' 37.2(2) . . . . ?
B4' B8' B9' B10' 101.2(2) . . . . ?
B4' B8' B9' B12' 137.8(2) . . . . ?
B4' B8' B12' B7' 100.2(2) . . . . ?
B4' B8' B12' B9' -37.5(2) . . . . ?
B4' B8' B12' B10' -0.8(3) . . . . ?
B4' B8' B12' B11' 63.1(3) . . . . ?
B4' B9' B10' B5' -37.8(2) . . . . ?
B4' B9' B10' B6' -0.8(3) . . . . ?
B4' B9' B10' B11' 62.8(3) . . . . ?
B4' B9' B10' B12' 100.8(2) . . . . ?
B4' B9' B12' B7' 0.2(3) . . . . ?
B4' B9' B12' B8' 37.9(2) . . . . ?
B4' B9' B12' B10' -100.9(2) . . . . ?
B4' B9' B12' B11' -62.9(3) . . . . ?
B5' C1' C2' P1 158.04(16) . . . . ?
B5' C1' C2' B3' -104.0(2) . . . . ?
B5' C1' C2' B6' 37.7(2) . . . . ?
B5' C1' C2' B7' -66.4(2) . . . . ?
B5' C1' C2' B11' 0.2(3) . . . . ?
B5' C1' B3' C2' 103.0(2) . . . . ?
B5' C1' B3' B4' -37.4(2) . . . . ?
B5' C1' B3' B7' 67.2(2) . . . . ?
B5' C1' B3' B8' 3.0(3) . . . . ?
B5' C1' B4' B3' 140.4(2) . . . . ?
B5' C1' B4' B8' 101.8(2) . . . . ?
B5' C1' B4' B9' 39.7(2) . . . . ?
B5' C1' B6' C2' -139.5(2) . . . . ?
B5' C1' B6' B10' -40.5(2) . . . . ?
B5' C1' B6' B11' -104.5(2) . . . . ?
B5' B4' B8' B3' 101.5(2) . . . . ?
B5' B4' B8' B7' 63.7(3) . . . . ?
B5' B4' B8' B9' -36.8(2) . . . . ?
B5' B4' B8' B12' 1.0(3) . . . . ?
B5' B4' B9' B8' 138.7(2) . . . . ?
B5' B4' B9' B10' 37.9(2) . . . . ?
B5' B4' B9' B12' 101.0(2) . . . . ?
B5' B6' B10' B9' -36.7(2) . . . . ?
B5' B6' B10' B11' -137.6(2) . . . . ?
B5' B6' B10' B12' -101.1(2) . . . . ?
B5' B6' B11' C2' -95.3(2) . . . . ?
B5' B6' B11' B7' -60.2(3) . . . . ?
B5' B6' B11' B10' 38.9(2) . . . . ?
B5' B6' B11' B12' 3.1(3) . . . . ?
B5' B9' B10' B6' 37.0(2) . . . . ?
B5' B9' B10' B11' 100.6(2) . . . . ?
B5' B9' B10' B12' 138.6(2) . . . . ?
B5' B9' B12' B7' 63.8(3) . . . . ?
B5' B9' B12' B8' 101.5(2) . . . . ?
B5' B9' B12' B10' -37.3(2) . . . . ?
B5' B9' B12' B11' 0.7(3) . . . . ?
B5' B10' B11' C2' 2.0(3) . . . . ?
B5' B10' B11' B6' -38.1(2) . . . . ?
B5' B10' B11' B7' 64.3(3) . . . . ?
B5' B10' B11' B12' 101.4(2) . . . . ?
B5' B10' B12' B7' -63.3(3) . . . . ?
B5' B10' B12' B8' 0.3(3) . . . . ?
B5' B10' B12' B9' 37.0(2) . . . . ?
B5' B10' B12' B11' -100.6(2) . . . . ?
B6' C1' C2' P1 120.34(19) . . . . ?
B6' C1' C2' B3' -141.7(2) . . . . ?
B6' C1' C2' B7' -104.1(2) . . . . ?
B6' C1' C2' B11' -37.5(2) . . . . ?
B6' C1' B3' C2' 36.17(19) . . . . ?
B6' C1' B3' B4' -104.2(2) . . . . ?
B6' C1' B3' B7' 0.4(3) . . . . ?
B6' C1' B3' B8' -63.8(2) . . . . ?
B6' C1' B4' B3' 103.8(2) . . . . ?
B6' C1' B4' B5' -36.6(2) . . . . ?
B6' C1' B4' B8' 65.2(2) . . . . ?
B6' C1' B4' B9' 3.1(3) . . . . ?
B6' C1' B5' B4' 141.1(2) . . . . ?
B6' C1' B5' B9' 101.2(2) . . . . ?
B6' C1' B5' B10' 38.95(19) . . . . ?
B6' C2' B3' C1' -36.55(19) . . . . ?
B6' C2' B3' B4' -2.5(3) . . . . ?
B6' C2' B3' B7' 102.5(2) . . . . ?
B6' C2' B3' B8' 61.8(3) . . . . ?
B6' C2' B7' B3' -105.4(2) . . . . ?
B6' C2' B7' B8' -66.5(2) . . . . ?
B6' C2' B7' B11' 36.40(19) . . . . ?
B6' C2' B7' B12' -3.8(3) . . . . ?
B6' C2' B11' B7' -140.9(2) . . . . ?
B6' C2' B11' B10' -39.23(19) . . . . ?
B6' C2' B11' B12' -101.0(2) . . . . ?
B6' B5' B9' B4' 102.1(2) . . . . ?
B6' B5' B9' B8' 64.8(3) . . . . ?
B6' B5' B9' B10' -35.7(2) . . . . ?
B6' B5' B9' B12' 1.2(3) . . . . ?
B6' B5' B10' B9' 139.0(2) . . . . ?
B6' B5' B10' B11' 37.9(2) . . . . ?
B6' B5' B10' B12' 101.6(2) . . . . ?
B6' B10' B11' C2' 40.10(19) . . . . ?
B6' B10' B11' B7' 102.3(2) . . . . ?
B6' B10' B11' B12' 139.5(2) . . . . ?
B6' B10' B12' B7' 0.9(3) . . . . ?
B6' B10' B12' B8' 64.5(3) . . . . ?
B6' B10' B12' B9' 101.2(2) . . . . ?
B6' B10' B12' B11' -36.5(2) . . . . ?
B6' B11' B12' B7' -102.8(2) . . . . ?
B6' B11' B12' B8' -65.5(3) . . . . ?
B6' B11' B12' B9' -2.3(3) . . . . ?
B6' B11' B12' B10' 35.4(2) . . . . ?
B7' C2' B3' C1' -139.1(2) . . . . ?
B7' C2' B3' B4' -105.0(2) . . . . ?
B7' C2' B3' B8' -40.7(2) . . . . ?
B7' C2' B6' C1' 102.9(2) . . . . ?
B7' C2' B6' B5' 68.0(2) . . . . ?
B7' C2' B6' B10' 4.3(3) . . . . ?
B7' C2' B6' B11' -36.6(2) . . . . ?
B7' C2' B11' B6' 140.9(2) . . . . ?
B7' C2' B11' B10' 101.7(2) . . . . ?
B7' C2' B11' B12' 39.91(19) . . . . ?
B7' B3' B4' C1' -95.7(2) . . . . ?
B7' B3' B4' B5' -60.5(3) . . . . ?
B7' B3' B4' B8' 39.3(2) . . . . ?
B7' B3' B4' B9' 2.5(3) . . . . ?
B7' B3' B8' B4' -137.4(2) . . . . ?
B7' B3' B8' B9' -100.3(2) . . . . ?
B7' B3' B8' B12' -36.6(2) . . . . ?
B7' B8' B9' B4' -100.4(2) . . . . ?
B7' B8' B9' B5' -63.2(3) . . . . ?
B7' B8' B9' B10' 0.8(3) . . . . ?
B7' B8' B9' B12' 37.4(2) . . . . ?
B7' B8' B12' B9' -137.8(2) . . . . ?
B7' B8' B12' B10' -101.0(2) . . . . ?
B7' B8' B12' B11' -37.1(2) . . . . ?
B7' B11' B12' B8' 37.3(2) . . . . ?
B7' B11' B12' B9' 100.5(2) . . . . ?
B7' B11' B12' B10' 138.2(2) . . . . ?
B8' B3' B4' C1' -135.0(2) . . . . ?
B8' B3' B4' B5' -99.8(2) . . . . ?
B8' B3' B4' B9' -36.8(2) . . . . ?
B8' B3' B7' C2' 134.9(2) . . . . ?
B8' B3' B7' B11' 100.9(2) . . . . ?
B8' B3' B7' B12' 36.9(2) . . . . ?
B8' B4' B5' C1' -97.6(2) . . . . ?
B8' B4' B5' B6' -62.5(3) . . . . ?
B8' B4' B5' B9' 36.8(2) . . . . ?
B8' B4' B5' B10' -0.8(3) . . . . ?
B8' B4' B9' B5' -138.7(2) . . . . ?
B8' B4' B9' B10' -100.8(2) . . . . ?
B8' B4' B9' B12' -37.7(2) . . . . ?
B8' B7' B11' C2' 96.8(2) . . . . ?
B8' B7' B11' B6' 61.4(3) . . . . ?
B8' B7' B11' B10' -0.5(3) . . . . ?
B8' B7' B11' B12' -37.5(2) . . . . ?
B8' B7' B12' B9' 37.6(2) . . . . ?
B8' B7' B12' B10' 100.7(2) . . . . ?
B8' B7' B12' B11' 138.4(2) . . . . ?
B8' B9' B10' B5' -101.8(2) . . . . ?
B8' B9' B10' B6' -64.8(3) . . . . ?
B8' B9' B10' B11' -1.1(3) . . . . ?
B8' B9' B10' B12' 36.8(2) . . . . ?
B8' B9' B12' B7' -37.8(2) . . . . ?
B8' B9' B12' B10' -138.8(2) . . . . ?
B8' B9' B12' B11' -100.8(2) . . . . ?
B9' B4' B5' C1' -134.4(2) . . . . ?
B9' B4' B5' B6' -99.4(2) . . . . ?
B9' B4' B5' B10' -37.6(2) . . . . ?
B9' B4' B8' B3' 138.3(2) . . . . ?
B9' B4' B8' B7' 100.5(2) . . . . ?
B9' B4' B8' B12' 37.7(2) . . . . ?
B9' B5' B6' C1' -98.1(2) . . . . ?
B9' B5' B6' C2' -64.1(2) . . . . ?
B9' B5' B6' B10' 36.4(2) . . . . ?
B9' B5' B6' B11' -2.6(3) . . . . ?
B9' B5' B10' B6' -139.0(2) . . . . ?
B9' B5' B10' B11' -101.2(2) . . . . ?
B9' B5' B10' B12' -37.5(2) . . . . ?
B9' B8' B12' B7' 137.8(2) . . . . ?
B9' B8' B12' B10' 36.7(2) . . . . ?
B9' B8' B12' B11' 100.7(2) . . . . ?
B9' B10' B11' C2' -61.2(3) . . . . ?
B9' B10' B11' B6' -101.3(2) . . . . ?
B9' B10' B11' B7' 1.0(3) . . . . ?
B9' B10' B11' B12' 38.2(2) . . . . ?
B9' B10' B12' B7' -100.4(2) . . . . ?
B9' B10' B12' B8' -36.7(2) . . . . ?
B9' B10' B12' B11' -137.7(2) . . . . ?
B10' B5' B6' C1' -134.5(2) . . . . ?
B10' B5' B6' C2' -100.5(2) . . . . ?
B10' B5' B6' B11' -39.0(2) . . . . ?
B10' B5' B9' B4' 137.8(2) . . . . ?
B10' B5' B9' B8' 100.5(2) . . . . ?
B10' B5' B9' B12' 36.9(2) . . . . ?
B10' B6' B11' C2' -134.2(2) . . . . ?
B10' B6' B11' B7' -99.0(2) . . . . ?
B10' B6' B11' B12' -35.8(2) . . . . ?
B10' B9' B12' B7' 101.1(2) . . . . ?
B10' B9' B12' B8' 138.8(2) . . . . ?
B10' B9' B12' B11' 38.0(2) . . . . ?
B10' B11' B12' B7' -138.2(2) . . . . ?
B10' B11' B12' B8' -100.9(2) . . . . ?
B10' B11' B12' B9' -37.7(2) . . . . ?
B11' C2' B3' C1' -103.2(2) . . . . ?
B11' C2' B3' B4' -69.1(2) . . . . ?
B11' C2' B3' B7' 35.8(2) . . . . ?
B11' C2' B3' B8' -4.9(3) . . . . ?
B11' C2' B6' C1' 139.5(2) . . . . ?
B11' C2' B6' B5' 104.6(2) . . . . ?
B11' C2' B6' B10' 41.0(2) . . . . ?
B11' C2' B7' B3' -141.8(2) . . . . ?
B11' C2' B7' B8' -102.9(2) . . . . ?
B11' C2' B7' B12' -40.19(19) . . . . ?
B11' B6' B10' B5' 137.6(2) . . . . ?
B11' B6' B10' B9' 101.0(2) . . . . ?
B11' B6' B10' B12' 36.5(2) . . . . ?
B11' B7' B8' B3' -101.1(2) . . . . ?
B11' B7' B8' B4' -63.1(3) . . . . ?
B11' B7' B8' B9' -0.2(3) . . . . ?
B11' B7' B8' B12' 37.6(2) . . . . ?
B11' B7' B12' B8' -138.4(2) . . . . ?
B11' B7' B12' B9' -100.8(2) . . . . ?
B11' B7' B12' B10' -37.6(2) . . . . ?
B11' B10' B12' B7' 37.3(2) . . . . ?
B11' B10' B12' B8' 101.0(2) . . . . ?
B11' B10' B12' B9' 137.7(2) . . . . ?
B12' B7' B8' B3' -138.7(2) . . . . ?
B12' B7' B8' B4' -100.7(2) . . . . ?
B12' B7' B8' B9' -37.8(2) . . . . ?
B12' B7' B11' C2' 134.3(2) . . . . ?
B12' B7' B11' B6' 98.9(2) . . . . ?
B12' B7' B11' B10' 37.0(2) . . . . ?
B12' B8' B9' B4' -137.8(2) . . . . ?
B12' B8' B9' B5' -100.7(2) . . . . ?
B12' B8' B9' B10' -36.6(2) . . . . ?
B12' B9' B10' B5' -138.6(2) . . . . ?
B12' B9' B10' B6' -101.6(2) . . . . ?
B12' B9' B10' B11' -38.0(2) . . . . ?
B12' B10' B11' C2' -99.4(2) . . . . ?
B12' B10' B11' B6' -139.5(2) . . . . ?
B12' B10' B11' B7' -37.2(2) . . . . ?

_shelx_SHELXL_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_5450
_database_code_depnum_ccdc_archive 'CCDC 1527033'
_audit_update_record             
;
2017-01-12 deposited with the CCDC.
2017-03-07 downloaded from the CCDC.
;
_audit_creation_date             2016-05-09
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C6 H25 B20 P Se'
_chemical_formula_sum            'C6 H25 B20 P Se'
_chemical_formula_weight         423.39
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   7.1663(7)
_cell_length_b                   11.0308(15)
_cell_length_c                   14.573(2)
_cell_angle_alpha                111.478(9)
_cell_angle_beta                 92.125(9)
_cell_angle_gamma                104.679(6)
_cell_volume                     1026.2(2)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    6562
_cell_measurement_temperature    100.0
_cell_measurement_theta_max      28.98
_cell_measurement_theta_min      2.94
_shelx_estimated_absorpt_T_max   0.726
_shelx_estimated_absorpt_T_min   0.450
_exptl_absorpt_coefficient_mu    1.898
_exptl_absorpt_correction_T_max  0.745975
_exptl_absorpt_correction_T_min  0.504496
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
 TWINABS-2008/4 (Bruker,2010) was used for absorption correction.
 
For component 1:
 wR2(int) was 0.0914 before and 0.0514 after correction.
 The Ratio of minimum to maximum transmission not present.
 The λ/2 correction factor is Not present
 
For component 2:
 wR2(int) was 0.1235 before and 0.0695 after correction.
 The Ratio of minimum to maximum transmission is 0.66.
 The λ/2 correction factor is Not present

Final HKLF 4 output contains 40190 reflections, Rint = 0.0763
 (18654 with I > 3sig(I), Rint = 0.0572)
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.370
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       BLOCK
_exptl_crystal_F_000             420
_exptl_crystal_size_max          0.5
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.18
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  ?
_diffrn_reflns_av_unetI/netI     0.0636
_diffrn_reflns_Laue_measured_fraction_full 0.976
_diffrn_reflns_Laue_measured_fraction_max 0.938
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            5691
_diffrn_reflns_point_group_measured_fraction_full 0.976
_diffrn_reflns_point_group_measured_fraction_max 0.938
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         30.136
_diffrn_reflns_theta_min         2.936
_diffrn_ambient_temperature      100.0
_diffrn_detector_area_resol_mean 8
_diffrn_measured_fraction_theta_full 0.976
_diffrn_measured_fraction_theta_max 0.938
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'sealed tube'
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4426
_reflns_number_total             5691
_reflns_special_details          
;
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v7.68A (Bruker, 2009)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'XT (Sheldrick, 2015)'
_refine_diff_density_max         0.612
_refine_diff_density_min         -0.583
_refine_diff_density_rms         0.100
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.036
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     315
_refine_ls_number_reflns         5691
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0634
_refine_ls_R_factor_gt           0.0410
_refine_ls_restrained_S_all      1.036
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0420P)²+0.2446P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0861
_refine_ls_wR_factor_ref         0.0939
_refine_special_details          
;
 Refined as a 2-component twin.
;
_olex2_refinement_description    
;
1. Twinned data refinement
 Scales: 0.688(2) 0.312(2)
2. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
3.a Secondary CH2 refined with riding coordinates:
 C11(H11A,H11B)
3.b Idealised Me refined as rotating group:
 C12(H12A,H12B,H12C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Se1 Se 0.40519(4) 0.66979(3) 0.51328(2) 0.01915(8) Uani 1 1 d . . . . .
P1 P 0.22050(9) 0.64096(6) 0.38886(4) 0.01283(13) Uani 1 1 d . . . . .
C1 C 0.2532(3) 0.4792(2) 0.18542(16) 0.0124(4) Uani 1 1 d . . . . .
C1' C 0.3452(3) 0.6282(2) 0.19879(16) 0.0126(4) Uani 1 1 d . . . . .
C2 C 0.1668(3) 0.4677(2) 0.28615(17) 0.0141(5) Uani 1 1 d . . . . .
C2' C 0.3314(3) 0.7371(2) 0.31059(16) 0.0126(4) Uani 1 1 d . . . . .
C11 C -0.0149(3) 0.6717(3) 0.41134(17) 0.0178(5) Uani 1 1 d . . . . .
H11A H -0.0796 0.6712 0.3499 0.021 Uiso 1 1 calc R . . . .
H11B H -0.0981 0.5966 0.4262 0.021 Uiso 1 1 calc R . . . .
C12 C 0.0004(4) 0.8068(3) 0.49739(19) 0.0218(5) Uani 1 1 d . . . . .
H12A H 0.0734 0.8823 0.4808 0.033 Uiso 1 1 calc GR . . . .
H12B H 0.0683 0.8096 0.5581 0.033 Uiso 1 1 calc GR . . . .
H12C H -0.1307 0.8152 0.5084 0.033 Uiso 1 1 calc GR . . . .
B3 B -0.0029(4) 0.4277(3) 0.18235(19) 0.0154(5) Uani 1 1 d . . . . .
H3 H -0.086(4) 0.495(3) 0.1858(19) 0.019 Uiso 1 1 d R . . . .
B3' B 0.5602(4) 0.7176(3) 0.2857(2) 0.0148(5) Uani 1 1 d . . . . .
H3' H 0.633(4) 0.665(3) 0.3176(19) 0.018 Uiso 1 1 d R . . . .
B4 B 0.1105(4) 0.3512(3) 0.0788(2) 0.0172(5) Uani 1 1 d . . . . .
H4 H 0.098(4) 0.374(3) 0.016(2) 0.021 Uiso 1 1 d R . . . .
B4' B 0.5580(4) 0.6872(3) 0.1569(2) 0.0162(5) Uani 1 1 d . . . . .
H4' H 0.623(4) 0.612(3) 0.1154(19) 0.019 Uiso 1 1 d R . . . .
B5 B 0.3427(4) 0.3441(3) 0.1240(2) 0.0172(6) Uani 1 1 d . . . . .
H5 H 0.475(4) 0.361(3) 0.0862(19) 0.021 Uiso 1 1 d R . . . .
B5' B 0.3281(4) 0.6939(3) 0.1093(2) 0.0166(5) Uani 1 1 d . . . . .
H5' H 0.255(4) 0.624(3) 0.035(2) 0.020 Uiso 1 1 d R . . . .
B6 B 0.3762(4) 0.4162(3) 0.2573(2) 0.0155(5) Uani 1 1 d . . . . .
H6 H 0.503(4) 0.476(3) 0.3046(19) 0.019 Uiso 1 1 d R . . . .
B6' B 0.1844(4) 0.7280(3) 0.20834(19) 0.0139(5) Uani 1 1 d . . . . .
H6' H 0.032(4) 0.685(3) 0.1995(19) 0.017 Uiso 1 1 d R . . . .
B7 B -0.0417(4) 0.3290(3) 0.2564(2) 0.0165(5) Uani 1 1 d . . . . .
H7 H -0.146(4) 0.340(3) 0.3032(19) 0.020 Uiso 1 1 d R . . . .
B7' B 0.5338(4) 0.8809(3) 0.3519(2) 0.0162(5) Uani 1 1 d . . . . .
H7' H 0.593(4) 0.930(3) 0.4313(19) 0.019 Uiso 1 1 d R . . . .
B8 B -0.0768(4) 0.2507(3) 0.1222(2) 0.0191(6) Uani 1 1 d . . . . .
H8 H -0.222(4) 0.199(3) 0.079(2) 0.023 Uiso 1 1 d R . . . .
B8' B 0.6797(4) 0.8517(3) 0.2532(2) 0.0167(5) Uani 1 1 d . . . . .
H8' H 0.848(4) 0.891(3) 0.2681(19) 0.020 Uiso 1 1 d R . . . .
B9 B 0.1349(4) 0.1966(3) 0.0858(2) 0.0204(6) Uani 1 1 d . . . . .
H9 H 0.128(4) 0.110(3) 0.018(2) 0.024 Uiso 1 1 d R . . . .
B9' B 0.5370(4) 0.8389(3) 0.1434(2) 0.0181(6) Uani 1 1 d . . . . .
H9' H 0.610(4) 0.874(3) 0.089(2) 0.022 Uiso 1 1 d R . . . .
B10 B 0.2968(4) 0.2391(3) 0.1962(2) 0.0207(6) Uani 1 1 d . . . . .
H10 H 0.397(4) 0.184(3) 0.202(2) 0.025 Uiso 1 1 d R . . . .
B10' B 0.3076(4) 0.8618(3) 0.1758(2) 0.0179(6) Uani 1 1 d . . . . .
H10' H 0.225(4) 0.910(3) 0.142(2) 0.021 Uiso 1 1 d R . . . .
B11 B 0.1885(4) 0.3222(3) 0.3013(2) 0.0176(6) Uani 1 1 d . . . . .
H11 H 0.219(4) 0.332(3) 0.375(2) 0.021 Uiso 1 1 d R . . . .
B11' B 0.3048(4) 0.8879(3) 0.3053(2) 0.0158(5) Uani 1 1 d . . . . .
H11' H 0.213(4) 0.938(3) 0.3535(19) 0.019 Uiso 1 1 d R . . . .
B12 B 0.0400(4) 0.1830(3) 0.1952(2) 0.0207(6) Uani 1 1 d . . . . .
H12 H -0.027(4) 0.092(3) 0.203(2) 0.025 Uiso 1 1 d R . . . .
B12' B 0.5241(4) 0.9589(3) 0.2647(2) 0.0170(6) Uani 1 1 d . . . . .
H12' H 0.576(4) 1.067(3) 0.2884(19) 0.020 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Se1 P1 2.0801(7) . ?
P1 C2 1.879(2) . ?
P1 C2' 1.893(2) . ?
P1 C11 1.822(2) . ?
C1 C1' 1.543(3) . ?
C1 C2 1.649(3) . ?
C1 B3 1.772(4) . ?
C1 B4 1.731(4) . ?
C1 B5 1.728(3) . ?
C1 B6 1.771(3) . ?
C1' C2' 1.657(3) . ?
C1' B3' 1.767(3) . ?
C1' B4' 1.726(4) . ?
C1' B5' 1.722(3) . ?
C1' B6' 1.761(3) . ?
C2 B3 1.751(3) . ?
C2 B6 1.748(3) . ?
C2 B7 1.751(4) . ?
C2 B11 1.741(4) . ?
C2' B3' 1.741(3) . ?
C2' B6' 1.749(3) . ?
C2' B7' 1.747(4) . ?
C2' B11' 1.750(4) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C11 C12 1.531(3) . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
B3 H3 1.05(3) . ?
B3 B4 1.776(4) . ?
B3 B7 1.777(4) . ?
B3 B8 1.746(4) . ?
B3' H3' 1.08(3) . ?
B3' B4' 1.781(4) . ?
B3' B7' 1.768(4) . ?
B3' B8' 1.746(4) . ?
B4 H4 1.03(3) . ?
B4 B5 1.798(4) . ?
B4 B8 1.804(4) . ?
B4 B9 1.797(4) . ?
B4' H4' 1.06(3) . ?
B4' B5' 1.793(4) . ?
B4' B8' 1.807(4) . ?
B4' B9' 1.796(4) . ?
B5 H5 1.12(3) . ?
B5 B6 1.789(4) . ?
B5 B9 1.795(4) . ?
B5 B10 1.810(4) . ?
B5' H5' 1.09(3) . ?
B5' B6' 1.787(4) . ?
B5' B9' 1.787(4) . ?
B5' B10' 1.796(4) . ?
B6 H6 1.03(3) . ?
B6 B10 1.748(4) . ?
B6 B11 1.772(4) . ?
B6' H6' 1.06(3) . ?
B6' B10' 1.751(4) . ?
B6' B11' 1.779(4) . ?
B7 H7 1.03(3) . ?
B7 B8 1.802(4) . ?
B7 B11 1.781(4) . ?
B7 B12 1.787(4) . ?
B7' H7' 1.09(3) . ?
B7' B8' 1.791(4) . ?
B7' B11' 1.783(4) . ?
B7' B12' 1.784(4) . ?
B8 H8 1.09(3) . ?
B8 B9 1.797(4) . ?
B8 B12 1.795(4) . ?
B8' H8' 1.15(3) . ?
B8' B9' 1.807(4) . ?
B8' B12' 1.791(4) . ?
B9 H9 1.09(3) . ?
B9 B10 1.785(4) . ?
B9 B12 1.797(4) . ?
B9' H9' 1.09(3) . ?
B9' B10' 1.780(4) . ?
B9' B12' 1.802(4) . ?
B10 H10 1.07(3) . ?
B10 B11 1.792(4) . ?
B10 B12 1.785(4) . ?
B10' H10' 1.10(3) . ?
B10' B11' 1.803(4) . ?
B10' B12' 1.795(4) . ?
B11 H11 1.05(3) . ?
B11 B12 1.787(4) . ?
B11' H11' 1.08(3) . ?
B11' B12' 1.793(4) . ?
B12 H12 1.05(3) . ?
B12' H12' 1.07(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 P1 Se1 114.43(8) . . ?
C2 P1 C2' 95.28(10) . . ?
C2' P1 Se1 115.05(8) . . ?
C11 P1 Se1 116.24(8) . . ?
C11 P1 C2 106.06(11) . . ?
C11 P1 C2' 107.48(11) . . ?
C1' C1 C2 112.14(18) . . ?
C1' C1 B3 116.31(18) . . ?
C1' C1 B4 125.58(19) . . ?
C1' C1 B5 125.76(19) . . ?
C1' C1 B6 116.57(18) . . ?
C2 C1 B3 61.43(14) . . ?
C2 C1 B4 110.84(18) . . ?
C2 C1 B5 111.19(18) . . ?
C2 C1 B6 61.37(14) . . ?
B4 C1 B3 60.92(15) . . ?
B4 C1 B6 112.56(19) . . ?
B5 C1 B3 112.28(18) . . ?
B5 C1 B4 62.63(16) . . ?
B5 C1 B6 61.51(15) . . ?
B6 C1 B3 112.22(18) . . ?
C1 C1' C2' 112.09(18) . . ?
C1 C1' B3' 116.14(18) . . ?
C1 C1' B4' 125.24(18) . . ?
C1 C1' B5' 125.73(19) . . ?
C1 C1' B6' 116.55(18) . . ?
C2' C1' B3' 61.03(14) . . ?
C2' C1' B4' 111.01(18) . . ?
C2' C1' B5' 111.45(18) . . ?
C2' C1' B6' 61.48(14) . . ?
B4' C1' B3' 61.29(15) . . ?
B4' C1' B6' 112.92(18) . . ?
B5' C1' B3' 112.51(19) . . ?
B5' C1' B4' 62.68(15) . . ?
B5' C1' B6' 61.75(15) . . ?
B6' C1' B3' 112.11(17) . . ?
C1 C2 P1 110.45(15) . . ?
C1 C2 B3 62.75(14) . . ?
C1 C2 B6 62.76(14) . . ?
C1 C2 B7 111.71(17) . . ?
C1 C2 B11 111.57(18) . . ?
B3 C2 P1 118.18(16) . . ?
B3 C2 B7 60.97(15) . . ?
B6 C2 P1 112.93(15) . . ?
B6 C2 B3 114.40(17) . . ?
B6 C2 B7 112.03(18) . . ?
B7 C2 P1 128.42(15) . . ?
B11 C2 P1 125.13(16) . . ?
B11 C2 B3 111.71(19) . . ?
B11 C2 B6 61.03(15) . . ?
B11 C2 B7 61.32(16) . . ?
C1' C2' P1 109.77(15) . . ?
C1' C2' B3' 62.60(14) . . ?
C1' C2' B6' 62.18(14) . . ?
C1' C2' B7' 111.15(17) . . ?
C1' C2' B11' 111.09(17) . . ?
B3' C2' P1 111.74(15) . . ?
B3' C2' B6' 113.95(17) . . ?
B3' C2' B7' 60.90(15) . . ?
B3' C2' B11' 111.72(18) . . ?
B6' C2' P1 118.78(16) . . ?
B6' C2' B11' 61.12(15) . . ?
B7' C2' P1 125.31(16) . . ?
B7' C2' B6' 111.78(18) . . ?
B7' C2' B11' 61.33(15) . . ?
B11' C2' P1 130.15(15) . . ?
P1 C11 H11A 108.9 . . ?
P1 C11 H11B 108.9 . . ?
H11A C11 H11B 107.7 . . ?
C12 C11 P1 113.26(17) . . ?
C12 C11 H11A 108.9 . . ?
C12 C11 H11B 108.9 . . ?
C11 C12 H12A 109.5 . . ?
C11 C12 H12B 109.5 . . ?
C11 C12 H12C 109.5 . . ?
H12A C12 H12B 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C1 B3 H3 120.7(15) . . ?
C1 B3 B4 58.41(14) . . ?
C1 B3 B7 104.98(18) . . ?
C2 B3 C1 55.82(13) . . ?
C2 B3 H3 118.2(14) . . ?
C2 B3 B4 104.22(18) . . ?
C2 B3 B7 59.54(15) . . ?
B4 B3 H3 125.1(14) . . ?
B4 B3 B7 110.1(2) . . ?
B7 B3 H3 120.6(15) . . ?
B8 B3 C1 106.18(19) . . ?
B8 B3 C2 106.68(19) . . ?
B8 B3 H3 127.5(15) . . ?
B8 B3 B4 61.61(16) . . ?
B8 B3 B7 61.52(16) . . ?
C1' B3' H3' 120.6(14) . . ?
C1' B3' B4' 58.22(14) . . ?
C1' B3' B7' 105.22(18) . . ?
C2' B3' C1' 56.37(13) . . ?
C2' B3' H3' 123.1(14) . . ?
C2' B3' B4' 104.69(18) . . ?
C2' B3' B7' 59.71(15) . . ?
C2' B3' B8' 106.99(19) . . ?
B4' B3' H3' 119.6(14) . . ?
B7' B3' H3' 124.6(14) . . ?
B7' B3' B4' 110.0(2) . . ?
B8' B3' C1' 106.13(19) . . ?
B8' B3' H3' 124.3(15) . . ?
B8' B3' B4' 61.63(16) . . ?
B8' B3' B7' 61.29(16) . . ?
C1 B4 B3 60.67(14) . . ?
C1 B4 H4 117.2(15) . . ?
C1 B4 B5 58.58(14) . . ?
C1 B4 B8 105.41(18) . . ?
C1 B4 B9 104.66(19) . . ?
B3 B4 H4 119.2(15) . . ?
B3 B4 B5 108.80(19) . . ?
B3 B4 B8 58.37(16) . . ?
B3 B4 B9 106.6(2) . . ?
B5 B4 H4 119.2(15) . . ?
B5 B4 B8 108.1(2) . . ?
B8 B4 H4 127.7(15) . . ?
B9 B4 H4 128.4(15) . . ?
B9 B4 B5 59.90(16) . . ?
B9 B4 B8 59.86(16) . . ?
C1' B4' B3' 60.49(14) . . ?
C1' B4' H4' 115.5(15) . . ?
C1' B4' B5' 58.55(14) . . ?
C1' B4' B8' 105.27(18) . . ?
C1' B4' B9' 104.68(18) . . ?
B3' B4' H4' 116.2(14) . . ?
B3' B4' B5' 108.52(18) . . ?
B3' B4' B8' 58.25(15) . . ?
B3' B4' B9' 106.74(19) . . ?
B5' B4' H4' 121.2(14) . . ?
B5' B4' B8' 108.06(19) . . ?
B5' B4' B9' 59.73(16) . . ?
B8' B4' H4' 127.2(15) . . ?
B9' B4' H4' 131.4(14) . . ?
B9' B4' B8' 60.21(16) . . ?
C1 B5 B4 58.79(14) . . ?
C1 B5 H5 119.3(14) . . ?
C1 B5 B6 60.44(14) . . ?
C1 B5 B9 104.92(19) . . ?
C1 B5 B10 104.77(18) . . ?
B4 B5 H5 122.5(14) . . ?
B4 B5 B10 107.4(2) . . ?
B6 B5 B4 108.60(19) . . ?
B6 B5 H5 117.7(14) . . ?
B6 B5 B9 106.3(2) . . ?
B6 B5 B10 58.11(16) . . ?
B9 B5 B4 60.03(16) . . ?
B9 B5 H5 128.3(14) . . ?
B9 B5 B10 59.35(17) . . ?
B10 B5 H5 125.0(14) . . ?
C1' B5' B4' 58.77(14) . . ?
C1' B5' H5' 117.8(14) . . ?
C1' B5' B6' 60.20(14) . . ?
C1' B5' B9' 105.24(19) . . ?
C1' B5' B10' 105.08(18) . . ?
B4' B5' H5' 120.6(14) . . ?
B4' B5' B10' 107.7(2) . . ?
B6' B5' B4' 108.52(18) . . ?
B6' B5' H5' 118.4(15) . . ?
B6' B5' B10' 58.51(15) . . ?
B9' B5' B4' 60.23(16) . . ?
B9' B5' H5' 128.4(14) . . ?
B9' B5' B6' 106.80(19) . . ?
B9' B5' B10' 59.58(16) . . ?
B10' B5' H5' 126.7(14) . . ?
C1 B6 B5 58.06(14) . . ?
C1 B6 H6 121.1(15) . . ?
C1 B6 B11 104.63(18) . . ?
C2 B6 C1 55.88(13) . . ?
C2 B6 B5 103.91(18) . . ?
C2 B6 H6 116.5(15) . . ?
C2 B6 B11 59.28(15) . . ?
B5 B6 H6 127.5(15) . . ?
B10 B6 C1 105.59(19) . . ?
B10 B6 C2 106.1(2) . . ?
B10 B6 B5 61.54(16) . . ?
B10 B6 H6 128.8(15) . . ?
B10 B6 B11 61.21(17) . . ?
B11 B6 B5 109.8(2) . . ?
B11 B6 H6 119.1(15) . . ?
C1' B6' B5' 58.05(14) . . ?
C1' B6' H6' 121.1(14) . . ?
C1' B6' B11' 105.05(18) . . ?
C2' B6' C1' 56.34(13) . . ?
C2' B6' B5' 104.27(18) . . ?
C2' B6' H6' 119.4(14) . . ?
C2' B6' B10' 106.33(19) . . ?
C2' B6' B11' 59.44(14) . . ?
B5' B6' H6' 124.2(14) . . ?
B10' B6' C1' 105.34(18) . . ?
B10' B6' B5' 60.99(16) . . ?
B10' B6' H6' 127.1(14) . . ?
B10' B6' B11' 61.43(16) . . ?
B11' B6' B5' 109.7(2) . . ?
B11' B6' H6' 121.4(14) . . ?
C2 B7 B3 59.49(14) . . ?
C2 B7 H7 116.8(15) . . ?
C2 B7 B8 104.25(18) . . ?
C2 B7 B11 59.05(15) . . ?
C2 B7 B12 104.78(18) . . ?
B3 B7 H7 118.4(15) . . ?
B3 B7 B8 58.41(15) . . ?
B3 B7 B11 108.63(19) . . ?
B3 B7 B12 106.96(19) . . ?
B8 B7 H7 128.3(15) . . ?
B11 B7 H7 119.2(15) . . ?
B11 B7 B8 108.1(2) . . ?
B11 B7 B12 60.09(16) . . ?
B12 B7 H7 129.2(15) . . ?
B12 B7 B8 60.01(16) . . ?
C2' B7' B3' 59.39(14) . . ?
C2' B7' H7' 119.2(15) . . ?
C2' B7' B8' 104.80(18) . . ?
C2' B7' B11' 59.41(15) . . ?
C2' B7' B12' 105.41(19) . . ?
B3' B7' H7' 117.0(14) . . ?
B3' B7' B8' 58.77(15) . . ?
B3' B7' B11' 108.91(19) . . ?
B3' B7' B12' 107.31(19) . . ?
B8' B7' H7' 124.4(14) . . ?
B11' B7' H7' 122.1(14) . . ?
B11' B7' B8' 108.6(2) . . ?
B11' B7' B12' 60.36(16) . . ?
B12' B7' H7' 128.3(14) . . ?
B12' B7' B8' 60.10(16) . . ?
B3 B8 B4 60.02(16) . . ?
B3 B8 B7 60.07(15) . . ?
B3 B8 H8 119.7(14) . . ?
B3 B8 B9 107.9(2) . . ?
B3 B8 B12 107.9(2) . . ?
B4 B8 H8 121.1(15) . . ?
B7 B8 B4 107.75(19) . . ?
B7 B8 H8 121.5(14) . . ?
B9 B8 B4 59.87(16) . . ?
B9 B8 B7 107.5(2) . . ?
B9 B8 H8 123.4(14) . . ?
B12 B8 B4 107.9(2) . . ?
B12 B8 B7 59.59(16) . . ?
B12 B8 H8 123.4(15) . . ?
B12 B8 B9 60.05(16) . . ?
B3' B8' B4' 60.12(15) . . ?
B3' B8' B7' 59.94(16) . . ?
B3' B8' H8' 119.8(13) . . ?
B3' B8' B9' 107.7(2) . . ?
B3' B8' B12' 107.97(19) . . ?
B4' B8' H8' 120.5(13) . . ?
B4' B8' B9' 59.60(16) . . ?
B7' B8' B4' 107.74(19) . . ?
B7' B8' H8' 122.2(13) . . ?
B7' B8' B9' 107.55(19) . . ?
B9' B8' H8' 123.1(13) . . ?
B12' B8' B4' 107.9(2) . . ?
B12' B8' B7' 59.76(15) . . ?
B12' B8' H8' 123.7(13) . . ?
B12' B8' B9' 60.11(16) . . ?
B4 B9 H9 119.6(15) . . ?
B4 B9 B12 108.1(2) . . ?
B5 B9 B4 60.07(16) . . ?
B5 B9 B8 108.6(2) . . ?
B5 B9 H9 119.6(15) . . ?
B5 B9 B12 108.5(2) . . ?
B8 B9 B4 60.27(16) . . ?
B8 B9 H9 121.9(15) . . ?
B8 B9 B12 59.93(16) . . ?
B10 B9 B4 108.5(2) . . ?
B10 B9 B5 60.76(16) . . ?
B10 B9 B8 108.1(2) . . ?
B10 B9 H9 122.4(15) . . ?
B10 B9 B12 59.77(17) . . ?
B12 B9 H9 123.9(15) . . ?
B4' B9' B8' 60.19(16) . . ?
B4' B9' H9' 121.6(14) . . ?
B4' B9' B12' 107.83(19) . . ?
B5' B9' B4' 60.05(16) . . ?
B5' B9' B8' 108.3(2) . . ?
B5' B9' H9' 123.4(14) . . ?
B5' B9' B12' 108.5(2) . . ?
B8' B9' H9' 119.7(14) . . ?
B10' B9' B4' 108.3(2) . . ?
B10' B9' B5' 60.45(16) . . ?
B10' B9' B8' 107.90(19) . . ?
B10' B9' H9' 122.9(14) . . ?
B10' B9' B12' 60.16(16) . . ?
B12' B9' B8' 59.48(15) . . ?
B12' B9' H9' 120.5(14) . . ?
B5 B10 H10 120.1(15) . . ?
B6 B10 B5 60.35(16) . . ?
B6 B10 B9 108.6(2) . . ?
B6 B10 H10 117.5(15) . . ?
B6 B10 B11 60.04(16) . . ?
B6 B10 B12 108.6(2) . . ?
B9 B10 B5 59.89(16) . . ?
B9 B10 H10 124.3(15) . . ?
B9 B10 B11 108.1(2) . . ?
B9 B10 B12 60.47(17) . . ?
B11 B10 B5 107.9(2) . . ?
B11 B10 H10 121.0(15) . . ?
B12 B10 B5 108.4(2) . . ?
B12 B10 H10 124.6(16) . . ?
B12 B10 B11 59.93(16) . . ?
B5' B10' H10' 122.5(14) . . ?
B5' B10' B11' 108.24(19) . . ?
B6' B10' B5' 60.50(15) . . ?
B6' B10' B9' 108.7(2) . . ?
B6' B10' H10' 120.0(15) . . ?
B6' B10' B11' 60.05(16) . . ?
B6' B10' B12' 108.3(2) . . ?
B9' B10' B5' 59.97(16) . . ?
B9' B10' H10' 123.2(15) . . ?
B9' B10' B11' 108.3(2) . . ?
B9' B10' B12' 60.52(16) . . ?
B11' B10' H10' 120.0(14) . . ?
B12' B10' B5' 108.36(19) . . ?
B12' B10' H10' 121.7(15) . . ?
B12' B10' B11' 59.78(16) . . ?
C2 B11 B6 59.69(15) . . ?
C2 B11 B7 59.63(15) . . ?
C2 B11 B10 104.49(19) . . ?
C2 B11 H11 115.6(15) . . ?
C2 B11 B12 105.25(19) . . ?
B6 B11 B7 109.53(19) . . ?
B6 B11 B10 58.75(16) . . ?
B6 B11 H11 115.7(15) . . ?
B6 B11 B12 107.5(2) . . ?
B7 B11 B10 108.2(2) . . ?
B7 B11 H11 120.3(15) . . ?
B7 B11 B12 60.13(16) . . ?
B10 B11 H11 127.7(14) . . ?
B12 B11 B10 59.83(16) . . ?
B12 B11 H11 131.0(15) . . ?
C2' B11' B6' 59.43(14) . . ?
C2' B11' B7' 59.26(15) . . ?
C2' B11' B10' 104.10(18) . . ?
C2' B11' H11' 118.1(14) . . ?
C2' B11' B12' 104.90(18) . . ?
B6' B11' B7' 108.70(18) . . ?
B6' B11' B10' 58.52(15) . . ?
B6' B11' H11' 116.1(14) . . ?
B6' B11' B12' 107.17(19) . . ?
B7' B11' B10' 107.63(19) . . ?
B7' B11' H11' 122.5(14) . . ?
B7' B11' B12' 59.86(16) . . ?
B10' B11' H11' 125.6(14) . . ?
B12' B11' B10' 59.89(16) . . ?
B12' B11' H11' 129.8(15) . . ?
B7 B12 B8 60.39(16) . . ?
B7 B12 B9 108.1(2) . . ?
B7 B12 H12 119.0(16) . . ?
B8 B12 B9 60.02(16) . . ?
B8 B12 H12 123.3(15) . . ?
B9 B12 H12 125.6(15) . . ?
B10 B12 B7 108.2(2) . . ?
B10 B12 B8 108.2(2) . . ?
B10 B12 B9 59.77(17) . . ?
B10 B12 B11 60.24(16) . . ?
B10 B12 H12 122.0(15) . . ?
B11 B12 B7 59.78(16) . . ?
B11 B12 B8 108.1(2) . . ?
B11 B12 B9 107.8(2) . . ?
B11 B12 H12 118.4(15) . . ?
B7' B12' B8' 60.15(15) . . ?
B7' B12' B9' 108.09(19) . . ?
B7' B12' B10' 107.9(2) . . ?
B7' B12' B11' 59.79(15) . . ?
B7' B12' H12' 120.3(14) . . ?
B8' B12' B9' 60.41(16) . . ?
B8' B12' B10' 107.97(19) . . ?
B8' B12' B11' 108.2(2) . . ?
B8' B12' H12' 123.7(15) . . ?
B9' B12' H12' 124.6(14) . . ?
B10' B12' B9' 59.32(16) . . ?
B10' B12' H12' 121.3(14) . . ?
B11' B12' B9' 107.8(2) . . ?
B11' B12' B10' 60.33(16) . . ?
B11' B12' H12' 118.6(15) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Se1 P1 C2 C1 -115.97(13) . . . . ?
Se1 P1 C2 B3 174.80(14) . . . . ?
Se1 P1 C2 B6 -47.86(17) . . . . ?
Se1 P1 C2 B7 100.93(19) . . . . ?
Se1 P1 C2 B11 21.9(2) . . . . ?
Se1 P1 C2' C1' 115.31(13) . . . . ?
Se1 P1 C2' B3' 47.84(17) . . . . ?
Se1 P1 C2' B6' -176.31(13) . . . . ?
Se1 P1 C2' B7' -21.11(19) . . . . ?
Se1 P1 C2' B11' -101.2(2) . . . . ?
Se1 P1 C11 C12 48.6(2) . . . . ?
P1 C2 B3 C1 99.79(18) . . . . ?
P1 C2 B3 B4 134.16(17) . . . . ?
P1 C2 B3 B7 -120.59(18) . . . . ?
P1 C2 B3 B8 -161.69(16) . . . . ?
P1 C2 B6 C1 -102.06(17) . . . . ?
P1 C2 B6 B5 -136.34(17) . . . . ?
P1 C2 B6 B10 159.74(16) . . . . ?
P1 C2 B6 B11 118.68(18) . . . . ?
P1 C2 B7 B3 104.4(2) . . . . ?
P1 C2 B7 B8 143.44(18) . . . . ?
P1 C2 B7 B11 -113.8(2) . . . . ?
P1 C2 B7 B12 -154.36(18) . . . . ?
P1 C2 B11 B6 -98.9(2) . . . . ?
P1 C2 B11 B7 118.8(2) . . . . ?
P1 C2 B11 B10 -138.41(18) . . . . ?
P1 C2 B11 B12 159.47(17) . . . . ?
P1 C2' B3' C1' 101.74(17) . . . . ?
P1 C2' B3' B4' 135.82(16) . . . . ?
P1 C2' B3' B7' -119.35(18) . . . . ?
P1 C2' B3' B8' -159.87(16) . . . . ?
P1 C2' B6' C1' -98.43(18) . . . . ?
P1 C2' B6' B5' -132.79(17) . . . . ?
P1 C2' B6' B10' 163.76(15) . . . . ?
P1 C2' B6' B11' 122.50(18) . . . . ?
P1 C2' B7' B3' 97.19(19) . . . . ?
P1 C2' B7' B8' 135.99(17) . . . . ?
P1 C2' B7' B11' -120.9(2) . . . . ?
P1 C2' B7' B12' -161.53(16) . . . . ?
P1 C2' B11' B6' -104.7(2) . . . . ?
P1 C2' B11' B7' 113.6(2) . . . . ?
P1 C2' B11' B10' -144.04(18) . . . . ?
P1 C2' B11' B12' 153.89(18) . . . . ?
C1 C1' C2' P1 3.7(2) . . . . ?
C1 C1' C2' B3' 108.6(2) . . . . ?
C1 C1' C2' B6' -109.2(2) . . . . ?
C1 C1' C2' B7' 146.60(18) . . . . ?
C1 C1' C2' B11' -147.12(18) . . . . ?
C1 C1' B3' C2' -102.0(2) . . . . ?
C1 C1' B3' B4' 117.7(2) . . . . ?
C1 C1' B3' B7' -137.99(19) . . . . ?
C1 C1' B3' B8' 158.08(19) . . . . ?
C1 C1' B4' B3' -103.2(2) . . . . ?
C1 C1' B4' B5' 116.1(2) . . . . ?
C1 C1' B4' B8' -141.8(2) . . . . ?
C1 C1' B4' B9' 155.6(2) . . . . ?
C1 C1' B5' B4' -115.4(2) . . . . ?
C1 C1' B5' B6' 103.8(2) . . . . ?
C1 C1' B5' B9' -155.3(2) . . . . ?
C1 C1' B5' B10' 142.8(2) . . . . ?
C1 C1' B6' C2' 101.9(2) . . . . ?
C1 C1' B6' B5' -118.2(2) . . . . ?
C1 C1' B6' B10' -158.40(19) . . . . ?
C1 C1' B6' B11' 137.69(19) . . . . ?
C1 C2 B3 B4 34.38(17) . . . . ?
C1 C2 B3 B7 139.62(19) . . . . ?
C1 C2 B3 B8 98.52(19) . . . . ?
C1 C2 B6 B5 -34.28(17) . . . . ?
C1 C2 B6 B10 -98.2(2) . . . . ?
C1 C2 B6 B11 -139.26(19) . . . . ?
C1 C2 B7 B3 -38.31(17) . . . . ?
C1 C2 B7 B8 0.7(2) . . . . ?
C1 C2 B7 B11 103.5(2) . . . . ?
C1 C2 B7 B12 62.9(2) . . . . ?
C1 C2 B11 B6 38.60(18) . . . . ?
C1 C2 B11 B7 -103.7(2) . . . . ?
C1 C2 B11 B10 -0.9(2) . . . . ?
C1 C2 B11 B12 -63.0(2) . . . . ?
C1 B3 B4 B5 34.62(17) . . . . ?
C1 B3 B4 B8 134.8(2) . . . . ?
C1 B3 B4 B9 97.8(2) . . . . ?
C1 B3 B7 C2 33.70(15) . . . . ?
C1 B3 B7 B8 -100.55(19) . . . . ?
C1 B3 B7 B11 -0.3(2) . . . . ?
C1 B3 B7 B12 -63.8(2) . . . . ?
C1 B3 B8 B4 -39.03(17) . . . . ?
C1 B3 B8 B7 98.55(19) . . . . ?
C1 B3 B8 B9 -1.7(2) . . . . ?
C1 B3 B8 B12 61.7(2) . . . . ?
C1 B4 B5 B6 35.65(18) . . . . ?
C1 B4 B5 B9 134.18(19) . . . . ?
C1 B4 B5 B10 97.0(2) . . . . ?
C1 B4 B8 B3 39.95(17) . . . . ?
C1 B4 B8 B7 2.1(3) . . . . ?
C1 B4 B8 B9 -98.3(2) . . . . ?
C1 B4 B8 B12 -60.8(2) . . . . ?
C1 B4 B9 B5 -39.24(17) . . . . ?
C1 B4 B9 B8 99.54(19) . . . . ?
C1 B4 B9 B10 -1.2(2) . . . . ?
C1 B4 B9 B12 62.1(2) . . . . ?
C1 B5 B6 C2 33.33(16) . . . . ?
C1 B5 B6 B10 134.3(2) . . . . ?
C1 B5 B6 B11 95.3(2) . . . . ?
C1 B5 B9 B4 39.40(17) . . . . ?
C1 B5 B9 B8 2.3(3) . . . . ?
C1 B5 B9 B10 -98.6(2) . . . . ?
C1 B5 B9 B12 -61.3(2) . . . . ?
C1 B5 B10 B6 -40.09(18) . . . . ?
C1 B5 B10 B9 98.8(2) . . . . ?
C1 B5 B10 B11 -2.1(3) . . . . ?
C1 B5 B10 B12 61.3(2) . . . . ?
C1 B6 B10 B5 39.10(17) . . . . ?
C1 B6 B10 B9 2.2(2) . . . . ?
C1 B6 B10 B11 -98.39(19) . . . . ?
C1 B6 B10 B12 -61.9(2) . . . . ?
C1 B6 B11 C2 -33.94(16) . . . . ?
C1 B6 B11 B7 0.1(2) . . . . ?
C1 B6 B11 B10 100.0(2) . . . . ?
C1 B6 B11 B12 63.8(2) . . . . ?
C1' C1 C2 P1 -3.1(2) . . . . ?
C1' C1 C2 B3 108.9(2) . . . . ?
C1' C1 C2 B6 -109.2(2) . . . . ?
C1' C1 C2 B7 146.43(18) . . . . ?
C1' C1 C2 B11 -147.03(19) . . . . ?
C1' C1 B3 C2 -102.1(2) . . . . ?
C1' C1 B3 B4 117.9(2) . . . . ?
C1' C1 B3 B7 -137.4(2) . . . . ?
C1' C1 B3 B8 158.46(19) . . . . ?
C1' C1 B4 B3 -103.0(2) . . . . ?
C1' C1 B4 B5 116.0(2) . . . . ?
C1' C1 B4 B8 -141.9(2) . . . . ?
C1' C1 B4 B9 155.9(2) . . . . ?
C1' C1 B5 B4 -115.8(2) . . . . ?
C1' C1 B5 B6 103.7(2) . . . . ?
C1' C1 B5 B9 -155.8(2) . . . . ?
C1' C1 B5 B10 142.6(2) . . . . ?
C1' C1 B6 C2 101.9(2) . . . . ?
C1' C1 B6 B5 -118.2(2) . . . . ?
C1' C1 B6 B10 -158.97(19) . . . . ?
C1' C1 B6 B11 137.4(2) . . . . ?
C1' C2' B3' B4' 34.07(17) . . . . ?
C1' C2' B3' B7' 138.90(19) . . . . ?
C1' C2' B3' B8' 98.4(2) . . . . ?
C1' C2' B6' B5' -34.36(17) . . . . ?
C1' C2' B6' B10' -97.81(19) . . . . ?
C1' C2' B6' B11' -139.07(19) . . . . ?
C1' C2' B7' B3' -38.73(17) . . . . ?
C1' C2' B7' B8' 0.1(2) . . . . ?
C1' C2' B7' B11' 103.19(19) . . . . ?
C1' C2' B7' B12' 62.5(2) . . . . ?
C1' C2' B11' B6' 38.39(17) . . . . ?
C1' C2' B11' B7' -103.29(19) . . . . ?
C1' C2' B11' B10' -0.9(2) . . . . ?
C1' C2' B11' B12' -63.0(2) . . . . ?
C1' B3' B4' B5' 34.72(17) . . . . ?
C1' B3' B4' B8' 134.92(19) . . . . ?
C1' B3' B4' B9' 97.7(2) . . . . ?
C1' B3' B7' C2' 34.56(16) . . . . ?
C1' B3' B7' B8' -100.3(2) . . . . ?
C1' B3' B7' B11' 0.4(2) . . . . ?
C1' B3' B7' B12' -63.4(2) . . . . ?
C1' B3' B8' B4' -38.80(16) . . . . ?
C1' B3' B8' B7' 98.81(19) . . . . ?
C1' B3' B8' B9' -1.6(2) . . . . ?
C1' B3' B8' B12' 61.9(2) . . . . ?
C1' B4' B5' B6' 35.32(17) . . . . ?
C1' B4' B5' B9' 134.50(19) . . . . ?
C1' B4' B5' B10' 97.21(19) . . . . ?
C1' B4' B8' B3' 39.70(17) . . . . ?
C1' B4' B8' B7' 1.9(2) . . . . ?
C1' B4' B8' B9' -98.4(2) . . . . ?
C1' B4' B8' B12' -61.2(2) . . . . ?
C1' B4' B9' B5' -38.97(17) . . . . ?
C1' B4' B9' B8' 99.43(19) . . . . ?
C1' B4' B9' B10' -1.2(2) . . . . ?
C1' B4' B9' B12' 62.5(2) . . . . ?
C1' B5' B6' C2' 33.62(16) . . . . ?
C1' B5' B6' B10' 134.6(2) . . . . ?
C1' B5' B6' B11' 95.8(2) . . . . ?
C1' B5' B9' B4' 39.21(16) . . . . ?
C1' B5' B9' B8' 1.9(2) . . . . ?
C1' B5' B9' B10' -98.79(19) . . . . ?
C1' B5' B9' B12' -61.2(2) . . . . ?
C1' B5' B10' B6' -39.77(17) . . . . ?
C1' B5' B10' B9' 99.1(2) . . . . ?
C1' B5' B10' B11' -2.0(3) . . . . ?
C1' B5' B10' B12' 61.3(2) . . . . ?
C1' B6' B10' B5' 38.78(17) . . . . ?
C1' B6' B10' B9' 1.8(2) . . . . ?
C1' B6' B10' B11' -99.05(19) . . . . ?
C1' B6' B10' B12' -62.4(2) . . . . ?
C1' B6' B11' C2' -34.38(16) . . . . ?
C1' B6' B11' B7' -0.1(2) . . . . ?
C1' B6' B11' B10' 99.52(19) . . . . ?
C1' B6' B11' B12' 63.1(2) . . . . ?
C2 P1 C2' C1' -4.80(15) . . . . ?
C2 P1 C2' B3' -72.27(16) . . . . ?
C2 P1 C2' B6' 63.59(17) . . . . ?
C2 P1 C2' B7' -141.22(18) . . . . ?
C2 P1 C2' B11' 138.7(2) . . . . ?
C2 P1 C11 C12 177.02(18) . . . . ?
C2 C1 C1' C2' -0.4(2) . . . . ?
C2 C1 C1' B3' 67.1(2) . . . . ?
C2 C1 C1' B4' 139.1(2) . . . . ?
C2 C1 C1' B5' -141.5(2) . . . . ?
C2 C1 C1' B6' -68.5(2) . . . . ?
C2 C1 B3 B4 -140.0(2) . . . . ?
C2 C1 B3 B7 -35.32(17) . . . . ?
C2 C1 B3 B8 -99.4(2) . . . . ?
C2 C1 B4 B3 37.14(18) . . . . ?
C2 C1 B4 B5 -103.8(2) . . . . ?
C2 C1 B4 B8 -1.7(2) . . . . ?
C2 C1 B4 B9 -63.9(2) . . . . ?
C2 C1 B5 B4 103.2(2) . . . . ?
C2 C1 B5 B6 -37.34(18) . . . . ?
C2 C1 B5 B9 63.2(2) . . . . ?
C2 C1 B5 B10 1.6(2) . . . . ?
C2 C1 B6 B5 139.9(2) . . . . ?
C2 C1 B6 B10 99.1(2) . . . . ?
C2 C1 B6 B11 35.44(17) . . . . ?
C2 B3 B4 C1 -33.25(16) . . . . ?
C2 B3 B4 B5 1.4(3) . . . . ?
C2 B3 B4 B8 101.5(2) . . . . ?
C2 B3 B4 B9 64.5(2) . . . . ?
C2 B3 B7 B8 -134.25(19) . . . . ?
C2 B3 B7 B11 -34.04(17) . . . . ?
C2 B3 B7 B12 -97.5(2) . . . . ?
C2 B3 B8 B4 -97.45(19) . . . . ?
C2 B3 B8 B7 40.14(17) . . . . ?
C2 B3 B8 B9 -60.2(2) . . . . ?
C2 B3 B8 B12 3.3(2) . . . . ?
C2 B6 B10 B5 97.38(19) . . . . ?
C2 B6 B10 B9 60.5(2) . . . . ?
C2 B6 B10 B11 -40.11(17) . . . . ?
C2 B6 B10 B12 -3.6(3) . . . . ?
C2 B6 B11 B7 34.03(18) . . . . ?
C2 B6 B11 B10 133.9(2) . . . . ?
C2 B6 B11 B12 97.8(2) . . . . ?
C2 B7 B8 B3 -39.55(17) . . . . ?
C2 B7 B8 B4 -1.7(2) . . . . ?
C2 B7 B8 B9 61.4(2) . . . . ?
C2 B7 B8 B12 99.1(2) . . . . ?
C2 B7 B11 B6 -34.05(17) . . . . ?
C2 B7 B11 B10 -96.5(2) . . . . ?
C2 B7 B11 B12 -133.48(19) . . . . ?
C2 B7 B12 B8 -98.1(2) . . . . ?
C2 B7 B12 B9 -60.4(2) . . . . ?
C2 B7 B12 B10 2.9(3) . . . . ?
C2 B7 B12 B11 40.06(17) . . . . ?
C2 B11 B12 B7 -40.46(17) . . . . ?
C2 B11 B12 B8 -2.9(2) . . . . ?
C2 B11 B12 B9 60.6(2) . . . . ?
C2 B11 B12 B10 98.1(2) . . . . ?
C2' P1 C2 C1 4.63(16) . . . . ?
C2' P1 C2 B3 -64.60(17) . . . . ?
C2' P1 C2 B6 72.74(16) . . . . ?
C2' P1 C2 B7 -138.5(2) . . . . ?
C2' P1 C2 B11 142.53(19) . . . . ?
C2' P1 C11 C12 -81.96(19) . . . . ?
C2' C1' B3' B4' -140.39(19) . . . . ?
C2' C1' B3' B7' -36.03(17) . . . . ?
C2' C1' B3' B8' -100.0(2) . . . . ?
C2' C1' B4' B3' 36.69(18) . . . . ?
C2' C1' B4' B5' -104.04(19) . . . . ?
C2' C1' B4' B8' -1.9(2) . . . . ?
C2' C1' B4' B9' -64.5(2) . . . . ?
C2' C1' B5' B4' 103.33(19) . . . . ?
C2' C1' B5' B6' -37.49(18) . . . . ?
C2' C1' B5' B9' 63.4(2) . . . . ?
C2' C1' B5' B10' 1.5(2) . . . . ?
C2' C1' B6' B5' 139.9(2) . . . . ?
C2' C1' B6' B10' 99.7(2) . . . . ?
C2' C1' B6' B11' 35.74(17) . . . . ?
C2' B3' B4' C1' -33.28(16) . . . . ?
C2' B3' B4' B5' 1.4(2) . . . . ?
C2' B3' B4' B8' 101.6(2) . . . . ?
C2' B3' B4' B9' 64.4(2) . . . . ?
C2' B3' B7' B8' -134.89(19) . . . . ?
C2' B3' B7' B11' -34.14(18) . . . . ?
C2' B3' B7' B12' -98.0(2) . . . . ?
C2' B3' B8' B4' -97.84(19) . . . . ?
C2' B3' B8' B7' 39.77(17) . . . . ?
C2' B3' B8' B9' -60.6(2) . . . . ?
C2' B3' B8' B12' 2.9(3) . . . . ?
C2' B6' B10' B5' 97.54(19) . . . . ?
C2' B6' B10' B9' 60.5(2) . . . . ?
C2' B6' B10' B11' -40.29(17) . . . . ?
C2' B6' B10' B12' -3.7(2) . . . . ?
C2' B6' B11' B7' 34.25(18) . . . . ?
C2' B6' B11' B10' 133.90(19) . . . . ?
C2' B6' B11' B12' 97.48(19) . . . . ?
C2' B7' B8' B3' -39.10(17) . . . . ?
C2' B7' B8' B4' -1.2(2) . . . . ?
C2' B7' B8' B9' 61.6(2) . . . . ?
C2' B7' B8' B12' 99.5(2) . . . . ?
C2' B7' B11' B6' -34.31(17) . . . . ?
C2' B7' B11' B10' -96.2(2) . . . . ?
C2' B7' B11' B12' -133.74(18) . . . . ?
C2' B7' B12' B8' -98.46(19) . . . . ?
C2' B7' B12' B9' -60.3(2) . . . . ?
C2' B7' B12' B10' 2.4(2) . . . . ?
C2' B7' B12' B11' 40.18(16) . . . . ?
C2' B11' B12' B7' -39.99(17) . . . . ?
C2' B11' B12' B8' -2.9(2) . . . . ?
C2' B11' B12' B9' 61.0(2) . . . . ?
C2' B11' B12' B10' 97.88(19) . . . . ?
C11 P1 C2 C1 114.53(16) . . . . ?
C11 P1 C2 B3 45.30(19) . . . . ?
C11 P1 C2 B6 -177.35(15) . . . . ?
C11 P1 C2 B7 -28.6(2) . . . . ?
C11 P1 C2 B11 -107.6(2) . . . . ?
C11 P1 C2' C1' -113.49(15) . . . . ?
C11 P1 C2' B3' 179.04(15) . . . . ?
C11 P1 C2' B6' -45.10(19) . . . . ?
C11 P1 C2' B7' 110.09(18) . . . . ?
C11 P1 C2' B11' 30.0(2) . . . . ?
B3 C1 C1' C2' 67.6(2) . . . . ?
B3 C1 C1' B3' 135.09(19) . . . . ?
B3 C1 C1' B4' -152.9(2) . . . . ?
B3 C1 C1' B5' -73.5(3) . . . . ?
B3 C1 C1' B6' -0.5(3) . . . . ?
B3 C1 C2 P1 -112.01(17) . . . . ?
B3 C1 C2 B6 141.99(19) . . . . ?
B3 C1 C2 B7 37.57(18) . . . . ?
B3 C1 C2 B11 104.1(2) . . . . ?
B3 C1 B4 B5 -140.9(2) . . . . ?
B3 C1 B4 B8 -38.84(18) . . . . ?
B3 C1 B4 B9 -101.0(2) . . . . ?
B3 C1 B5 B4 36.53(18) . . . . ?
B3 C1 B5 B6 -104.0(2) . . . . ?
B3 C1 B5 B9 -3.5(2) . . . . ?
B3 C1 B5 B10 -65.1(2) . . . . ?
B3 C1 B6 C2 -35.75(17) . . . . ?
B3 C1 B6 B5 104.1(2) . . . . ?
B3 C1 B6 B10 63.3(2) . . . . ?
B3 C1 B6 B11 -0.3(2) . . . . ?
B3 C2 B6 C1 36.95(18) . . . . ?
B3 C2 B6 B5 2.7(3) . . . . ?
B3 C2 B6 B10 -61.3(2) . . . . ?
B3 C2 B6 B11 -102.3(2) . . . . ?
B3 C2 B7 B8 39.02(17) . . . . ?
B3 C2 B7 B11 141.80(19) . . . . ?
B3 C2 B7 B12 101.2(2) . . . . ?
B3 C2 B11 B6 106.73(19) . . . . ?
B3 C2 B11 B7 -35.59(18) . . . . ?
B3 C2 B11 B10 67.2(2) . . . . ?
B3 C2 B11 B12 5.1(2) . . . . ?
B3 B4 B5 C1 -35.48(18) . . . . ?
B3 B4 B5 B6 0.2(3) . . . . ?
B3 B4 B5 B9 98.7(2) . . . . ?
B3 B4 B5 B10 61.6(2) . . . . ?
B3 B4 B8 B7 -37.86(18) . . . . ?
B3 B4 B8 B9 -138.2(2) . . . . ?
B3 B4 B8 B12 -100.8(2) . . . . ?
B3 B4 B9 B5 -102.5(2) . . . . ?
B3 B4 B9 B8 36.31(18) . . . . ?
B3 B4 B9 B10 -64.4(2) . . . . ?
B3 B4 B9 B12 -1.1(3) . . . . ?
B3 B7 B8 B4 37.84(18) . . . . ?
B3 B7 B8 B9 101.0(2) . . . . ?
B3 B7 B8 B12 138.6(2) . . . . ?
B3 B7 B11 C2 34.21(17) . . . . ?
B3 B7 B11 B6 0.2(3) . . . . ?
B3 B7 B11 B10 -62.3(2) . . . . ?
B3 B7 B11 B12 -99.3(2) . . . . ?
B3 B7 B12 B8 -36.08(18) . . . . ?
B3 B7 B12 B9 1.7(3) . . . . ?
B3 B7 B12 B10 64.9(2) . . . . ?
B3 B7 B12 B11 102.1(2) . . . . ?
B3 B8 B9 B4 -37.35(19) . . . . ?
B3 B8 B9 B5 -0.3(3) . . . . ?
B3 B8 B9 B10 64.1(2) . . . . ?
B3 B8 B9 B12 100.8(2) . . . . ?
B3 B8 B12 B7 37.04(18) . . . . ?
B3 B8 B12 B9 -100.8(2) . . . . ?
B3 B8 B12 B10 -64.0(2) . . . . ?
B3 B8 B12 B11 -0.3(3) . . . . ?
B3' C1' C2' P1 -104.89(16) . . . . ?
B3' C1' C2' B6' 142.23(19) . . . . ?
B3' C1' C2' B7' 38.01(17) . . . . ?
B3' C1' C2' B11' 104.3(2) . . . . ?
B3' C1' B4' B5' -140.73(19) . . . . ?
B3' C1' B4' B8' -38.62(17) . . . . ?
B3' C1' B4' B9' -101.2(2) . . . . ?
B3' C1' B5' B4' 36.94(18) . . . . ?
B3' C1' B5' B6' -103.88(19) . . . . ?
B3' C1' B5' B9' -3.0(2) . . . . ?
B3' C1' B5' B10' -64.9(2) . . . . ?
B3' C1' B6' C2' -35.34(17) . . . . ?
B3' C1' B6' B5' 104.5(2) . . . . ?
B3' C1' B6' B10' 64.3(2) . . . . ?
B3' C1' B6' B11' 0.4(2) . . . . ?
B3' C2' B6' C1' 36.51(18) . . . . ?
B3' C2' B6' B5' 2.1(3) . . . . ?
B3' C2' B6' B10' -61.3(2) . . . . ?
B3' C2' B6' B11' -102.6(2) . . . . ?
B3' C2' B7' B8' 38.80(17) . . . . ?
B3' C2' B7' B11' 141.92(19) . . . . ?
B3' C2' B7' B12' 101.28(19) . . . . ?
B3' C2' B11' B6' 106.21(19) . . . . ?
B3' C2' B11' B7' -35.46(18) . . . . ?
B3' C2' B11' B10' 66.9(2) . . . . ?
B3' C2' B11' B12' 4.8(2) . . . . ?
B3' B4' B5' C1' -35.52(18) . . . . ?
B3' B4' B5' B6' -0.2(3) . . . . ?
B3' B4' B5' B9' 99.0(2) . . . . ?
B3' B4' B5' B10' 61.7(2) . . . . ?
B3' B4' B8' B7' -37.78(18) . . . . ?
B3' B4' B8' B9' -138.1(2) . . . . ?
B3' B4' B8' B12' -100.9(2) . . . . ?
B3' B4' B9' B5' -102.0(2) . . . . ?
B3' B4' B9' B8' 36.36(18) . . . . ?
B3' B4' B9' B10' -64.2(2) . . . . ?
B3' B4' B9' B12' -0.6(3) . . . . ?
B3' B7' B8' B4' 37.86(18) . . . . ?
B3' B7' B8' B9' 100.7(2) . . . . ?
B3' B7' B8' B12' 138.6(2) . . . . ?
B3' B7' B11' C2' 34.13(17) . . . . ?
B3' B7' B11' B6' -0.2(3) . . . . ?
B3' B7' B11' B10' -62.1(2) . . . . ?
B3' B7' B11' B12' -99.6(2) . . . . ?
B3' B7' B12' B8' -36.32(18) . . . . ?
B3' B7' B12' B9' 1.8(3) . . . . ?
B3' B7' B12' B10' 64.5(2) . . . . ?
B3' B7' B12' B11' 102.3(2) . . . . ?
B3' B8' B9' B4' -37.43(18) . . . . ?
B3' B8' B9' B5' -0.1(2) . . . . ?
B3' B8' B9' B10' 63.8(2) . . . . ?
B3' B8' B9' B12' 100.9(2) . . . . ?
B3' B8' B12' B7' 36.99(19) . . . . ?
B3' B8' B12' B9' -100.5(2) . . . . ?
B3' B8' B12' B10' -63.8(2) . . . . ?
B3' B8' B12' B11' 0.0(3) . . . . ?
B4 C1 C1' C2' 139.4(2) . . . . ?
B4 C1 C1' B3' -153.1(2) . . . . ?
B4 C1 C1' B4' -81.1(3) . . . . ?
B4 C1 C1' B5' -1.7(3) . . . . ?
B4 C1 C1' B6' 71.3(3) . . . . ?
B4 C1 C2 P1 -148.94(16) . . . . ?
B4 C1 C2 B3 -36.93(18) . . . . ?
B4 C1 C2 B6 105.1(2) . . . . ?
B4 C1 C2 B7 0.6(2) . . . . ?
B4 C1 C2 B11 67.2(2) . . . . ?
B4 C1 B3 C2 140.0(2) . . . . ?
B4 C1 B3 B7 104.7(2) . . . . ?
B4 C1 B3 B8 40.57(18) . . . . ?
B4 C1 B5 B6 -140.6(2) . . . . ?
B4 C1 B5 B9 -40.01(18) . . . . ?
B4 C1 B5 B10 -101.6(2) . . . . ?
B4 C1 B6 C2 -102.25(19) . . . . ?
B4 C1 B6 B5 37.64(19) . . . . ?
B4 C1 B6 B10 -3.2(2) . . . . ?
B4 C1 B6 B11 -66.8(2) . . . . ?
B4 B3 B7 C2 95.0(2) . . . . ?
B4 B3 B7 B8 -39.20(19) . . . . ?
B4 B3 B7 B11 61.0(2) . . . . ?
B4 B3 B7 B12 -2.4(3) . . . . ?
B4 B3 B8 B7 137.6(2) . . . . ?
B4 B3 B8 B9 37.29(19) . . . . ?
B4 B3 B8 B12 100.8(2) . . . . ?
B4 B5 B6 C1 -34.96(18) . . . . ?
B4 B5 B6 C2 -1.6(2) . . . . ?
B4 B5 B6 B10 99.3(2) . . . . ?
B4 B5 B6 B11 60.3(2) . . . . ?
B4 B5 B9 B8 -37.13(19) . . . . ?
B4 B5 B9 B10 -138.0(2) . . . . ?
B4 B5 B9 B12 -100.7(2) . . . . ?
B4 B5 B10 B6 -101.5(2) . . . . ?
B4 B5 B10 B9 37.44(18) . . . . ?
B4 B5 B10 B11 -63.5(2) . . . . ?
B4 B5 B10 B12 -0.1(3) . . . . ?
B4 B8 B9 B5 37.04(19) . . . . ?
B4 B8 B9 B10 101.4(2) . . . . ?
B4 B8 B9 B12 138.2(2) . . . . ?
B4 B8 B12 B7 100.5(2) . . . . ?
B4 B8 B12 B9 -37.33(19) . . . . ?
B4 B8 B12 B10 -0.6(3) . . . . ?
B4 B8 B12 B11 63.2(2) . . . . ?
B4 B9 B10 B5 -37.75(19) . . . . ?
B4 B9 B10 B6 -0.7(3) . . . . ?
B4 B9 B10 B11 62.9(3) . . . . ?
B4 B9 B10 B12 100.6(2) . . . . ?
B4 B9 B12 B7 -0.4(3) . . . . ?
B4 B9 B12 B8 37.56(19) . . . . ?
B4 B9 B12 B10 -101.3(2) . . . . ?
B4 B9 B12 B11 -63.5(3) . . . . ?
B4' C1' C2' P1 -141.69(16) . . . . ?
B4' C1' C2' B3' -36.80(18) . . . . ?
B4' C1' C2' B6' 105.4(2) . . . . ?
B4' C1' C2' B7' 1.2(2) . . . . ?
B4' C1' C2' B11' 67.5(2) . . . . ?
B4' C1' B3' C2' 140.39(19) . . . . ?
B4' C1' B3' B7' 104.4(2) . . . . ?
B4' C1' B3' B8' 40.43(17) . . . . ?
B4' C1' B5' B6' -140.82(19) . . . . ?
B4' C1' B5' B9' -39.91(17) . . . . ?
B4' C1' B5' B10' -101.9(2) . . . . ?
B4' C1' B6' C2' -102.3(2) . . . . ?
B4' C1' B6' B5' 37.54(19) . . . . ?
B4' C1' B6' B10' -2.7(2) . . . . ?
B4' C1' B6' B11' -66.6(2) . . . . ?
B4' B3' B7' C2' 95.8(2) . . . . ?
B4' B3' B7' B8' -39.14(19) . . . . ?
B4' B3' B7' B11' 61.6(2) . . . . ?
B4' B3' B7' B12' -2.2(3) . . . . ?
B4' B3' B8' B7' 137.6(2) . . . . ?
B4' B3' B8' B9' 37.20(18) . . . . ?
B4' B3' B8' B12' 100.7(2) . . . . ?
B4' B5' B6' C1' -34.73(17) . . . . ?
B4' B5' B6' C2' -1.1(2) . . . . ?
B4' B5' B6' B10' 99.9(2) . . . . ?
B4' B5' B6' B11' 61.1(2) . . . . ?
B4' B5' B9' B8' -37.35(17) . . . . ?
B4' B5' B9' B10' -138.0(2) . . . . ?
B4' B5' B9' B12' -100.4(2) . . . . ?
B4' B5' B10' B6' -101.2(2) . . . . ?
B4' B5' B10' B9' 37.58(18) . . . . ?
B4' B5' B10' B11' -63.5(2) . . . . ?
B4' B5' B10' B12' -0.2(3) . . . . ?
B4' B8' B9' B5' 37.29(18) . . . . ?
B4' B8' B9' B10' 101.3(2) . . . . ?
B4' B8' B9' B12' 138.4(2) . . . . ?
B4' B8' B12' B7' 100.5(2) . . . . ?
B4' B8' B12' B9' -37.01(19) . . . . ?
B4' B8' B12' B10' -0.2(3) . . . . ?
B4' B8' B12' B11' 63.6(2) . . . . ?
B4' B9' B10' B5' -37.64(18) . . . . ?
B4' B9' B10' B6' -0.4(3) . . . . ?
B4' B9' B10' B11' 63.3(2) . . . . ?
B4' B9' B10' B12' 100.5(2) . . . . ?
B4' B9' B12' B7' -0.8(3) . . . . ?
B4' B9' B12' B8' 37.26(19) . . . . ?
B4' B9' B12' B10' -101.3(2) . . . . ?
B4' B9' B12' B11' -63.9(2) . . . . ?
B5 C1 C1' C2' -141.1(2) . . . . ?
B5 C1 C1' B3' -73.6(3) . . . . ?
B5 C1 C1' B4' -1.6(3) . . . . ?
B5 C1 C1' B5' 77.8(3) . . . . ?
B5 C1 C1' B6' 150.8(2) . . . . ?
B5 C1 C2 P1 143.40(16) . . . . ?
B5 C1 C2 B3 -104.6(2) . . . . ?
B5 C1 C2 B6 37.39(18) . . . . ?
B5 C1 C2 B7 -67.0(2) . . . . ?
B5 C1 C2 B11 -0.5(2) . . . . ?
B5 C1 B3 C2 102.8(2) . . . . ?
B5 C1 B3 B4 -37.22(19) . . . . ?
B5 C1 B3 B7 67.5(2) . . . . ?
B5 C1 B3 B8 3.4(2) . . . . ?
B5 C1 B4 B3 140.9(2) . . . . ?
B5 C1 B4 B8 102.1(2) . . . . ?
B5 C1 B4 B9 39.89(18) . . . . ?
B5 C1 B6 C2 -139.9(2) . . . . ?
B5 C1 B6 B10 -40.80(18) . . . . ?
B5 C1 B6 B11 -104.4(2) . . . . ?
B5 B4 B8 B3 101.3(2) . . . . ?
B5 B4 B8 B7 63.5(2) . . . . ?
B5 B4 B8 B9 -36.85(18) . . . . ?
B5 B4 B8 B12 0.6(3) . . . . ?
B5 B4 B9 B8 138.8(2) . . . . ?
B5 B4 B9 B10 38.05(19) . . . . ?
B5 B4 B9 B12 101.4(2) . . . . ?
B5 B6 B10 B9 -36.85(19) . . . . ?
B5 B6 B10 B11 -137.5(2) . . . . ?
B5 B6 B10 B12 -101.0(2) . . . . ?
B5 B6 B11 C2 -94.8(2) . . . . ?
B5 B6 B11 B7 -60.8(2) . . . . ?
B5 B6 B11 B10 39.14(19) . . . . ?
B5 B6 B11 B12 3.0(3) . . . . ?
B5 B9 B10 B6 37.05(18) . . . . ?
B5 B9 B10 B11 100.7(2) . . . . ?
B5 B9 B10 B12 138.4(2) . . . . ?
B5 B9 B12 B7 63.3(2) . . . . ?
B5 B9 B12 B8 101.2(2) . . . . ?
B5 B9 B12 B10 -37.67(19) . . . . ?
B5 B9 B12 B11 0.1(3) . . . . ?
B5 B10 B11 C2 1.8(3) . . . . ?
B5 B10 B11 B6 -38.11(19) . . . . ?
B5 B10 B11 B7 64.1(2) . . . . ?
B5 B10 B11 B12 101.3(2) . . . . ?
B5 B10 B12 B7 -63.5(2) . . . . ?
B5 B10 B12 B8 0.4(3) . . . . ?
B5 B10 B12 B9 37.26(19) . . . . ?
B5 B10 B12 B11 -100.5(2) . . . . ?
B5' C1' C2' P1 150.48(16) . . . . ?
B5' C1' C2' B3' -104.6(2) . . . . ?
B5' C1' C2' B6' 37.60(18) . . . . ?
B5' C1' C2' B7' -66.6(2) . . . . ?
B5' C1' C2' B11' -0.3(2) . . . . ?
B5' C1' B3' C2' 102.89(19) . . . . ?
B5' C1' B3' B4' -37.50(18) . . . . ?
B5' C1' B3' B7' 66.9(2) . . . . ?
B5' C1' B3' B8' 2.9(2) . . . . ?
B5' C1' B4' B3' 140.73(19) . . . . ?
B5' C1' B4' B8' 102.1(2) . . . . ?
B5' C1' B4' B9' 39.55(18) . . . . ?
B5' C1' B6' C2' -139.9(2) . . . . ?
B5' C1' B6' B10' -40.20(18) . . . . ?
B5' C1' B6' B11' -104.1(2) . . . . ?
B5' B4' B8' B3' 101.0(2) . . . . ?
B5' B4' B8' B7' 63.2(2) . . . . ?
B5' B4' B8' B9' -37.09(18) . . . . ?
B5' B4' B8' B12' 0.1(3) . . . . ?
B5' B4' B9' B8' 138.40(19) . . . . ?
B5' B4' B9' B10' 37.82(18) . . . . ?
B5' B4' B9' B12' 101.4(2) . . . . ?
B5' B6' B10' B9' -36.99(18) . . . . ?
B5' B6' B10' B11' -137.83(19) . . . . ?
B5' B6' B10' B12' -101.2(2) . . . . ?
B5' B6' B11' C2' -95.31(19) . . . . ?
B5' B6' B11' B7' -61.1(2) . . . . ?
B5' B6' B11' B10' 38.58(18) . . . . ?
B5' B6' B11' B12' 2.2(2) . . . . ?
B5' B9' B10' B6' 37.22(18) . . . . ?
B5' B9' B10' B11' 100.9(2) . . . . ?
B5' B9' B10' B12' 138.1(2) . . . . ?
B5' B9' B12' B7' 62.8(2) . . . . ?
B5' B9' B12' B8' 100.8(2) . . . . ?
B5' B9' B12' B10' -37.74(18) . . . . ?
B5' B9' B12' B11' -0.4(3) . . . . ?
B5' B10' B11' C2' 1.8(2) . . . . ?
B5' B10' B11' B6' -37.97(18) . . . . ?
B5' B10' B11' B7' 63.6(2) . . . . ?
B5' B10' B11' B12' 101.1(2) . . . . ?
B5' B10' B12' B7' -63.3(2) . . . . ?
B5' B10' B12' B8' 0.3(3) . . . . ?
B5' B10' B12' B9' 37.50(18) . . . . ?
B5' B10' B12' B11' -100.9(2) . . . . ?
B6 C1 C1' C2' -68.4(2) . . . . ?
B6 C1 C1' B3' -0.9(3) . . . . ?
B6 C1 C1' B4' 71.2(3) . . . . ?
B6 C1 C1' B5' 150.6(2) . . . . ?
B6 C1 C1' B6' -136.44(19) . . . . ?
B6 C1 C2 P1 106.00(17) . . . . ?
B6 C1 C2 B3 -141.99(19) . . . . ?
B6 C1 C2 B7 -104.4(2) . . . . ?
B6 C1 C2 B11 -37.88(18) . . . . ?
B6 C1 B3 C2 35.72(17) . . . . ?
B6 C1 B3 B4 -104.3(2) . . . . ?
B6 C1 B3 B7 0.4(2) . . . . ?
B6 C1 B3 B8 -63.7(2) . . . . ?
B6 C1 B4 B3 103.7(2) . . . . ?
B6 C1 B4 B5 -37.18(18) . . . . ?
B6 C1 B4 B8 64.9(2) . . . . ?
B6 C1 B4 B9 2.7(2) . . . . ?
B6 C1 B5 B4 140.6(2) . . . . ?
B6 C1 B5 B9 100.6(2) . . . . ?
B6 C1 B5 B10 38.95(18) . . . . ?
B6 C2 B3 C1 -36.96(18) . . . . ?
B6 C2 B3 B4 -2.6(3) . . . . ?
B6 C2 B3 B7 102.7(2) . . . . ?
B6 C2 B3 B8 61.6(2) . . . . ?
B6 C2 B7 B3 -106.57(19) . . . . ?
B6 C2 B7 B8 -67.5(2) . . . . ?
B6 C2 B7 B11 35.23(18) . . . . ?
B6 C2 B7 B12 -5.3(2) . . . . ?
B6 C2 B11 B7 -142.32(19) . . . . ?
B6 C2 B11 B10 -39.49(18) . . . . ?
B6 C2 B11 B12 -101.6(2) . . . . ?
B6 B5 B9 B4 102.4(2) . . . . ?
B6 B5 B9 B8 65.3(2) . . . . ?
B6 B5 B9 B10 -35.55(18) . . . . ?
B6 B5 B9 B12 1.7(3) . . . . ?
B6 B5 B10 B9 138.9(2) . . . . ?
B6 B5 B10 B11 37.97(19) . . . . ?
B6 B5 B10 B12 101.4(2) . . . . ?
B6 B10 B11 C2 39.96(18) . . . . ?
B6 B10 B11 B7 102.3(2) . . . . ?
B6 B10 B11 B12 139.4(2) . . . . ?
B6 B10 B12 B7 0.5(3) . . . . ?
B6 B10 B12 B8 64.4(3) . . . . ?
B6 B10 B12 B9 101.3(2) . . . . ?
B6 B10 B12 B11 -36.51(19) . . . . ?
B6 B11 B12 B7 -102.9(2) . . . . ?
B6 B11 B12 B8 -65.3(2) . . . . ?
B6 B11 B12 B9 -1.9(3) . . . . ?
B6 B11 B12 B10 35.68(19) . . . . ?
B6' C1' C2' P1 112.88(17) . . . . ?
B6' C1' C2' B3' -142.23(19) . . . . ?
B6' C1' C2' B7' -104.2(2) . . . . ?
B6' C1' C2' B11' -37.94(18) . . . . ?
B6' C1' B3' C2' 35.51(17) . . . . ?
B6' C1' B3' B4' -104.9(2) . . . . ?
B6' C1' B3' B7' -0.5(2) . . . . ?
B6' C1' B3' B8' -64.4(2) . . . . ?
B6' C1' B4' B3' 103.56(19) . . . . ?
B6' C1' B4' B5' -37.17(18) . . . . ?
B6' C1' B4' B8' 64.9(2) . . . . ?
B6' C1' B4' B9' 2.4(2) . . . . ?
B6' C1' B5' B4' 140.82(19) . . . . ?
B6' C1' B5' B9' 100.9(2) . . . . ?
B6' C1' B5' B10' 38.95(18) . . . . ?
B6' C2' B3' C1' -36.35(18) . . . . ?
B6' C2' B3' B4' -2.3(3) . . . . ?
B6' C2' B3' B7' 102.6(2) . . . . ?
B6' C2' B3' B8' 62.0(2) . . . . ?
B6' C2' B7' B3' -106.13(19) . . . . ?
B6' C2' B7' B8' -67.3(2) . . . . ?
B6' C2' B7' B11' 35.79(18) . . . . ?
B6' C2' B7' B12' -4.9(2) . . . . ?
B6' C2' B11' B7' -141.67(19) . . . . ?
B6' C2' B11' B10' -39.32(17) . . . . ?
B6' C2' B11' B12' -101.4(2) . . . . ?
B6' B5' B9' B4' 102.09(19) . . . . ?
B6' B5' B9' B8' 64.7(2) . . . . ?
B6' B5' B9' B10' -35.90(18) . . . . ?
B6' B5' B9' B12' 1.7(2) . . . . ?
B6' B5' B10' B9' 138.8(2) . . . . ?
B6' B5' B10' B11' 37.77(18) . . . . ?
B6' B5' B10' B12' 101.1(2) . . . . ?
B6' B10' B11' C2' 39.77(17) . . . . ?
B6' B10' B11' B7' 101.5(2) . . . . ?
B6' B10' B11' B12' 139.03(19) . . . . ?
B6' B10' B12' B7' 0.8(2) . . . . ?
B6' B10' B12' B8' 64.4(2) . . . . ?
B6' B10' B12' B9' 101.6(2) . . . . ?
B6' B10' B12' B11' -36.75(18) . . . . ?
B6' B11' B12' B7' -102.0(2) . . . . ?
B6' B11' B12' B8' -64.9(2) . . . . ?
B6' B11' B12' B9' -1.1(3) . . . . ?
B6' B11' B12' B10' 35.82(18) . . . . ?
B7 C2 B3 C1 -139.62(19) . . . . ?
B7 C2 B3 B4 -105.2(2) . . . . ?
B7 C2 B3 B8 -41.10(18) . . . . ?
B7 C2 B6 C1 103.91(19) . . . . ?
B7 C2 B6 B5 69.6(2) . . . . ?
B7 C2 B6 B10 5.7(2) . . . . ?
B7 C2 B6 B11 -35.35(19) . . . . ?
B7 C2 B11 B6 142.32(19) . . . . ?
B7 C2 B11 B10 102.8(2) . . . . ?
B7 C2 B11 B12 40.71(17) . . . . ?
B7 B3 B4 C1 -95.6(2) . . . . ?
B7 B3 B4 B5 -61.0(2) . . . . ?
B7 B3 B4 B8 39.16(19) . . . . ?
B7 B3 B4 B9 2.2(3) . . . . ?
B7 B3 B8 B4 -137.6(2) . . . . ?
B7 B3 B8 B9 -100.3(2) . . . . ?
B7 B3 B8 B12 -36.83(18) . . . . ?
B7 B8 B9 B4 -100.7(2) . . . . ?
B7 B8 B9 B5 -63.7(2) . . . . ?
B7 B8 B9 B10 0.7(3) . . . . ?
B7 B8 B9 B12 37.41(19) . . . . ?
B7 B8 B12 B9 -137.8(2) . . . . ?
B7 B8 B12 B10 -101.1(2) . . . . ?
B7 B8 B12 B11 -37.30(19) . . . . ?
B7 B11 B12 B8 37.58(19) . . . . ?
B7 B11 B12 B9 101.0(2) . . . . ?
B7 B11 B12 B10 138.6(2) . . . . ?
B7' C2' B3' C1' -138.90(19) . . . . ?
B7' C2' B3' B4' -104.8(2) . . . . ?
B7' C2' B3' B8' -40.52(18) . . . . ?
B7' C2' B6' C1' 103.21(19) . . . . ?
B7' C2' B6' B5' 68.8(2) . . . . ?
B7' C2' B6' B10' 5.4(2) . . . . ?
B7' C2' B6' B11' -35.87(18) . . . . ?
B7' C2' B11' B6' 141.67(19) . . . . ?
B7' C2' B11' B10' 102.4(2) . . . . ?
B7' C2' B11' B12' 40.28(17) . . . . ?
B7' B3' B4' C1' -95.93(19) . . . . ?
B7' B3' B4' B5' -61.2(2) . . . . ?
B7' B3' B4' B8' 38.99(18) . . . . ?
B7' B3' B4' B9' 1.8(3) . . . . ?
B7' B3' B8' B4' -137.6(2) . . . . ?
B7' B3' B8' B9' -100.4(2) . . . . ?
B7' B3' B8' B12' -36.91(18) . . . . ?
B7' B8' B9' B4' -100.7(2) . . . . ?
B7' B8' B9' B5' -63.4(2) . . . . ?
B7' B8' B9' B10' 0.6(3) . . . . ?
B7' B8' B9' B12' 37.71(19) . . . . ?
B7' B8' B12' B9' -137.5(2) . . . . ?
B7' B8' B12' B10' -100.8(2) . . . . ?
B7' B8' B12' B11' -36.95(18) . . . . ?
B7' B11' B12' B8' 37.10(18) . . . . ?
B7' B11' B12' B9' 101.0(2) . . . . ?
B7' B11' B12' B10' 137.9(2) . . . . ?
B8 B3 B4 C1 -134.8(2) . . . . ?
B8 B3 B4 B5 -100.1(2) . . . . ?
B8 B3 B4 B9 -36.97(19) . . . . ?
B8 B3 B7 C2 134.25(19) . . . . ?
B8 B3 B7 B11 100.2(2) . . . . ?
B8 B3 B7 B12 36.78(19) . . . . ?
B8 B4 B5 C1 -97.35(19) . . . . ?
B8 B4 B5 B6 -61.7(2) . . . . ?
B8 B4 B5 B9 36.84(18) . . . . ?
B8 B4 B5 B10 -0.3(2) . . . . ?
B8 B4 B9 B5 -138.8(2) . . . . ?
B8 B4 B9 B10 -100.7(2) . . . . ?
B8 B4 B9 B12 -37.41(19) . . . . ?
B8 B7 B11 C2 96.1(2) . . . . ?
B8 B7 B11 B6 62.0(2) . . . . ?
B8 B7 B11 B10 -0.4(3) . . . . ?
B8 B7 B11 B12 -37.40(19) . . . . ?
B8 B7 B12 B9 37.75(19) . . . . ?
B8 B7 B12 B10 101.0(2) . . . . ?
B8 B7 B12 B11 138.2(2) . . . . ?
B8 B9 B10 B5 -101.6(2) . . . . ?
B8 B9 B10 B6 -64.5(3) . . . . ?
B8 B9 B10 B11 -0.9(3) . . . . ?
B8 B9 B10 B12 36.8(2) . . . . ?
B8 B9 B12 B7 -37.92(19) . . . . ?
B8 B9 B12 B10 -138.9(2) . . . . ?
B8 B9 B12 B11 -101.1(2) . . . . ?
B8' B3' B4' C1' -134.92(19) . . . . ?
B8' B3' B4' B5' -100.2(2) . . . . ?
B8' B3' B4' B9' -37.24(18) . . . . ?
B8' B3' B7' C2' 134.89(19) . . . . ?
B8' B3' B7' B11' 100.7(2) . . . . ?
B8' B3' B7' B12' 36.90(19) . . . . ?
B8' B4' B5' C1' -97.20(19) . . . . ?
B8' B4' B5' B6' -61.9(2) . . . . ?
B8' B4' B5' B9' 37.30(18) . . . . ?
B8' B4' B5' B10' 0.0(2) . . . . ?
B8' B4' B9' B5' -138.40(19) . . . . ?
B8' B4' B9' B10' -100.6(2) . . . . ?
B8' B4' B9' B12' -36.95(18) . . . . ?
B8' B7' B11' C2' 96.6(2) . . . . ?
B8' B7' B11' B6' 62.2(2) . . . . ?
B8' B7' B11' B10' 0.3(3) . . . . ?
B8' B7' B11' B12' -37.19(18) . . . . ?
B8' B7' B12' B9' 38.14(19) . . . . ?
B8' B7' B12' B10' 100.9(2) . . . . ?
B8' B7' B12' B11' 138.6(2) . . . . ?
B8' B9' B10' B5' -101.3(2) . . . . ?
B8' B9' B10' B6' -64.1(2) . . . . ?
B8' B9' B10' B11' -0.4(3) . . . . ?
B8' B9' B10' B12' 36.82(19) . . . . ?
B8' B9' B12' B7' -38.02(19) . . . . ?
B8' B9' B12' B10' -138.5(2) . . . . ?
B8' B9' B12' B11' -101.2(2) . . . . ?
B9 B4 B5 C1 -134.18(19) . . . . ?
B9 B4 B5 B6 -98.5(2) . . . . ?
B9 B4 B5 B10 -37.14(18) . . . . ?
B9 B4 B8 B3 138.2(2) . . . . ?
B9 B4 B8 B7 100.3(2) . . . . ?
B9 B4 B8 B12 37.41(19) . . . . ?
B9 B5 B6 C1 -98.2(2) . . . . ?
B9 B5 B6 C2 -64.9(2) . . . . ?
B9 B5 B6 B10 36.10(18) . . . . ?
B9 B5 B6 B11 -2.9(2) . . . . ?
B9 B5 B10 B6 -138.9(2) . . . . ?
B9 B5 B10 B11 -100.9(2) . . . . ?
B9 B5 B10 B12 -37.51(19) . . . . ?
B9 B8 B12 B7 137.8(2) . . . . ?
B9 B8 B12 B10 36.74(19) . . . . ?
B9 B8 B12 B11 100.5(2) . . . . ?
B9 B10 B11 C2 -61.5(2) . . . . ?
B9 B10 B11 B6 -101.4(2) . . . . ?
B9 B10 B11 B7 0.8(3) . . . . ?
B9 B10 B11 B12 38.0(2) . . . . ?
B9 B10 B12 B7 -100.8(2) . . . . ?
B9 B10 B12 B8 -36.85(19) . . . . ?
B9 B10 B12 B11 -137.8(2) . . . . ?
B9' B4' B5' C1' -134.50(19) . . . . ?
B9' B4' B5' B6' -99.2(2) . . . . ?
B9' B4' B5' B10' -37.29(18) . . . . ?
B9' B4' B8' B3' 138.1(2) . . . . ?
B9' B4' B8' B7' 100.3(2) . . . . ?
B9' B4' B8' B12' 37.24(19) . . . . ?
B9' B5' B6' C1' -98.2(2) . . . . ?
B9' B5' B6' C2' -64.6(2) . . . . ?
B9' B5' B6' B10' 36.37(18) . . . . ?
B9' B5' B6' B11' -2.4(2) . . . . ?
B9' B5' B10' B6' -138.8(2) . . . . ?
B9' B5' B10' B11' -101.1(2) . . . . ?
B9' B5' B10' B12' -37.74(19) . . . . ?
B9' B8' B12' B7' 137.5(2) . . . . ?
B9' B8' B12' B10' 36.77(19) . . . . ?
B9' B8' B12' B11' 100.6(2) . . . . ?
B9' B10' B11' C2' -61.7(2) . . . . ?
B9' B10' B11' B6' -101.5(2) . . . . ?
B9' B10' B11' B7' 0.0(3) . . . . ?
B9' B10' B11' B12' 37.55(19) . . . . ?
B9' B10' B12' B7' -100.8(2) . . . . ?
B9' B10' B12' B8' -37.25(19) . . . . ?
B9' B10' B12' B11' -138.4(2) . . . . ?
B10 B5 B6 C1 -134.3(2) . . . . ?
B10 B5 B6 C2 -100.9(2) . . . . ?
B10 B5 B6 B11 -39.00(19) . . . . ?
B10 B5 B9 B4 138.0(2) . . . . ?
B10 B5 B9 B8 100.8(2) . . . . ?
B10 B5 B9 B12 37.24(19) . . . . ?
B10 B6 B11 C2 -133.9(2) . . . . ?
B10 B6 B11 B7 -99.9(2) . . . . ?
B10 B6 B11 B12 -36.15(19) . . . . ?
B10 B9 B12 B7 101.0(2) . . . . ?
B10 B9 B12 B8 138.9(2) . . . . ?
B10 B9 B12 B11 37.78(19) . . . . ?
B10 B11 B12 B7 -138.6(2) . . . . ?
B10 B11 B12 B8 -101.0(2) . . . . ?
B10 B11 B12 B9 -37.57(19) . . . . ?
B10' B5' B6' C1' -134.6(2) . . . . ?
B10' B5' B6' C2' -101.0(2) . . . . ?
B10' B5' B6' B11' -38.78(18) . . . . ?
B10' B5' B9' B4' 138.0(2) . . . . ?
B10' B5' B9' B8' 100.6(2) . . . . ?
B10' B5' B9' B12' 37.61(18) . . . . ?
B10' B6' B11' C2' -133.90(19) . . . . ?
B10' B6' B11' B7' -99.7(2) . . . . ?
B10' B6' B11' B12' -36.42(18) . . . . ?
B10' B9' B12' B7' 100.5(2) . . . . ?
B10' B9' B12' B8' 138.5(2) . . . . ?
B10' B9' B12' B11' 37.33(19) . . . . ?
B10' B11' B12' B7' -137.9(2) . . . . ?
B10' B11' B12' B8' -100.8(2) . . . . ?
B10' B11' B12' B9' -36.89(19) . . . . ?
B11 C2 B3 C1 -103.89(19) . . . . ?
B11 C2 B3 B4 -69.5(2) . . . . ?
B11 C2 B3 B7 35.73(18) . . . . ?
B11 C2 B3 B8 -5.4(2) . . . . ?
B11 C2 B6 C1 139.26(19) . . . . ?
B11 C2 B6 B5 105.0(2) . . . . ?
B11 C2 B6 B10 41.06(18) . . . . ?
B11 C2 B7 B3 -141.80(19) . . . . ?
B11 C2 B7 B8 -102.8(2) . . . . ?
B11 C2 B7 B12 -40.58(18) . . . . ?
B11 B6 B10 B5 137.5(2) . . . . ?
B11 B6 B10 B9 100.6(2) . . . . ?
B11 B6 B10 B12 36.46(19) . . . . ?
B11 B7 B8 B3 -101.2(2) . . . . ?
B11 B7 B8 B4 -63.3(2) . . . . ?
B11 B7 B8 B9 -0.2(3) . . . . ?
B11 B7 B8 B12 37.43(19) . . . . ?
B11 B7 B12 B8 -138.2(2) . . . . ?
B11 B7 B12 B9 -100.4(2) . . . . ?
B11 B7 B12 B10 -37.2(2) . . . . ?
B11 B10 B12 B7 36.99(19) . . . . ?
B11 B10 B12 B8 100.9(2) . . . . ?
B11 B10 B12 B9 137.8(2) . . . . ?
B11' C2' B3' C1' -103.28(19) . . . . ?
B11' C2' B3' B4' -69.2(2) . . . . ?
B11' C2' B3' B7' 35.62(18) . . . . ?
B11' C2' B3' B8' -4.9(2) . . . . ?
B11' C2' B6' C1' 139.07(19) . . . . ?
B11' C2' B6' B5' 104.7(2) . . . . ?
B11' C2' B6' B10' 41.26(18) . . . . ?
B11' C2' B7' B3' -141.92(19) . . . . ?
B11' C2' B7' B8' -103.1(2) . . . . ?
B11' C2' B7' B12' -40.64(17) . . . . ?
B11' B6' B10' B5' 137.83(19) . . . . ?
B11' B6' B10' B9' 100.8(2) . . . . ?
B11' B6' B10' B12' 36.63(18) . . . . ?
B11' B7' B8' B3' -101.3(2) . . . . ?
B11' B7' B8' B4' -63.4(2) . . . . ?
B11' B7' B8' B9' -0.6(3) . . . . ?
B11' B7' B8' B12' 37.30(19) . . . . ?
B11' B7' B12' B8' -138.6(2) . . . . ?
B11' B7' B12' B9' -100.5(2) . . . . ?
B11' B7' B12' B10' -37.78(18) . . . . ?
B11' B10' B12' B7' 37.54(18) . . . . ?
B11' B10' B12' B8' 101.1(2) . . . . ?
B11' B10' B12' B9' 138.4(2) . . . . ?
B12 B7 B8 B3 -138.6(2) . . . . ?
B12 B7 B8 B4 -100.8(2) . . . . ?
B12 B7 B8 B9 -37.61(19) . . . . ?
B12 B7 B11 C2 133.48(19) . . . . ?
B12 B7 B11 B6 99.4(2) . . . . ?
B12 B7 B11 B10 37.00(19) . . . . ?
B12 B8 B9 B4 -138.2(2) . . . . ?
B12 B8 B9 B5 -101.1(2) . . . . ?
B12 B8 B9 B10 -36.7(2) . . . . ?
B12 B9 B10 B5 -138.4(2) . . . . ?
B12 B9 B10 B6 -101.3(2) . . . . ?
B12 B9 B10 B11 -37.72(19) . . . . ?
B12 B10 B11 C2 -99.4(2) . . . . ?
B12 B10 B11 B6 -139.4(2) . . . . ?
B12 B10 B11 B7 -37.14(19) . . . . ?
B12' B7' B8' B3' -138.6(2) . . . . ?
B12' B7' B8' B4' -100.7(2) . . . . ?
B12' B7' B8' B9' -37.87(19) . . . . ?
B12' B7' B11' C2' 133.74(18) . . . . ?
B12' B7' B11' B6' 99.4(2) . . . . ?
B12' B7' B11' B10' 37.51(18) . . . . ?
B12' B8' B9' B4' -138.4(2) . . . . ?
B12' B8' B9' B5' -101.1(2) . . . . ?
B12' B8' B9' B10' -37.12(19) . . . . ?
B12' B9' B10' B5' -138.1(2) . . . . ?
B12' B9' B10' B6' -100.9(2) . . . . ?
B12' B9' B10' B11' -37.22(19) . . . . ?
B12' B10' B11' C2' -99.26(19) . . . . ?
B12' B10' B11' B6' -139.03(19) . . . . ?
B12' B10' B11' B7' -37.50(18) . . . . ?

_shelx_SHELXL_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_twin_individual_id
_twin_individual_mass_fraction_refined
1 0.688(2)
2 0.312(2)

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_5429
_database_code_depnum_ccdc_archive 'CCDC 1527030'
_audit_update_record             
;
2017-01-12 deposited with the CCDC.
2017-03-07 downloaded from the CCDC.
;
_audit_creation_date             2017-01-12
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.09.09 svn.r3337 for OlexSys, GUI svn.r5227)
;
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C10 H25 Au B20 Cl P'
_chemical_formula_sum            'C10 H25 Au B20 Cl P'
_chemical_formula_weight         624.89
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   17.0588(8)
_cell_length_b                   14.2499(7)
_cell_length_c                   20.0698(9)
_cell_angle_alpha                90
_cell_angle_beta                 102.497(3)
_cell_angle_gamma                90
_cell_volume                     4763.1(4)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    7273
_cell_measurement_temperature    100.0
_cell_measurement_theta_max      30.140
_cell_measurement_theta_min      2.446
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    6.357
_exptl_absorpt_correction_T_max  0.7463
_exptl_absorpt_correction_T_min  0.5223
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.1118 before and 0.0645 after correction.
The Ratio of minimum to maximum transmission is 0.6999.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.743
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       needle
_exptl_crystal_F_000             2368
_exptl_crystal_size_max          0.32
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.15
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0796
_diffrn_reflns_av_unetI/netI     0.0583
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            58934
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         32.011
_diffrn_reflns_theta_min         2.273
_diffrn_ambient_temperature      100.0
_diffrn_detector_area_resol_mean 8
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                6479
_reflns_number_total             8266
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v7.68A (Bruker, 2009)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         0.925
_refine_diff_density_min         -1.808
_refine_diff_density_rms         0.192
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.015
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     358
_refine_ls_number_reflns         8266
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0519
_refine_ls_R_factor_gt           0.0342
_refine_ls_restrained_S_all      1.015
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0242P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0602
_refine_ls_wR_factor_ref         0.0647
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C12(H12A), C13(H13), C14(H14), C15(H15), C16(H16)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.34661(2) 0.51583(2) 0.22043(2) 0.01221(4) Uani 1 1 d . . . . .
P1 P 0.28061(5) 0.43005(6) 0.28275(4) 0.01106(16) Uani 1 1 d . . . . .
Cl1 Cl 0.41169(5) 0.60504(6) 0.15584(4) 0.01902(17) Uani 1 1 d . . . . .
C1 C 0.30959(17) 0.4464(2) 0.42981(15) 0.0113(6) Uani 1 1 d . . . . .
C2 C 0.26036(18) 0.4957(2) 0.35846(16) 0.0119(6) Uani 1 1 d . . . . .
B3 B 0.2041(2) 0.4322(3) 0.40423(19) 0.0143(7) Uani 1 1 d . . . . .
H3 H 0.1766(19) 0.366(2) 0.3855(16) 0.017 Uiso 1 1 d R . . . .
B4 B 0.2530(2) 0.4514(3) 0.49091(19) 0.0143(7) Uani 1 1 d . . . . .
H4 H 0.2596(19) 0.391(2) 0.5264(16) 0.017 Uiso 1 1 d R . . . .
B5 B 0.3358(2) 0.5285(3) 0.49320(19) 0.0140(7) Uani 1 1 d . . . . .
H5 H 0.384(2) 0.519(2) 0.5272(19) 0.017 Uiso 1 1 d R . . . .
B6 B 0.3408(2) 0.5582(3) 0.40780(18) 0.0131(7) Uani 1 1 d . . . . .
H6 H 0.396(2) 0.564(2) 0.3923(16) 0.016 Uiso 1 1 d R . . . .
B7 B 0.1682(2) 0.5393(3) 0.3655(2) 0.0154(7) Uani 1 1 d . . . . .
H7 H 0.123(2) 0.535(2) 0.3222(18) 0.019 Uiso 1 1 d R . . . .
B8 B 0.1625(2) 0.5130(3) 0.4514(2) 0.0164(7) Uani 1 1 d . . . . .
H8 H 0.108(2) 0.501(2) 0.4668(19) 0.020 Uiso 1 1 d R . . . .
B9 B 0.2434(2) 0.5735(3) 0.5069(2) 0.0179(8) Uani 1 1 d . . . . .
H9 H 0.235(2) 0.598(2) 0.5579(17) 0.021 Uiso 1 1 d R . . . .
B10 B 0.2972(2) 0.6371(3) 0.45485(19) 0.0168(8) Uani 1 1 d . . . . .
H10 H 0.326(2) 0.699(3) 0.4652(16) 0.020 Uiso 1 1 d R . . . .
B11 B 0.2511(2) 0.6153(3) 0.36738(19) 0.0155(7) Uani 1 1 d . . . . .
H11 H 0.2535(19) 0.657(2) 0.3241(17) 0.019 Uiso 1 1 d R . . . .
B12 B 0.1911(2) 0.6276(3) 0.4293(2) 0.0179(8) Uani 1 1 d . . . . .
H12 H 0.154(2) 0.686(2) 0.4279(17) 0.022 Uiso 1 1 d R . . . .
C11 C 0.18733(17) 0.3833(2) 0.23516(15) 0.0124(6) Uani 1 1 d . . . . .
C12 C 0.1508(2) 0.4380(3) 0.17926(17) 0.0201(7) Uani 1 1 d . . . . .
H12A H 0.1757 0.4944 0.1693 0.024 Uiso 1 1 calc R . . . .
C13 C 0.0782(2) 0.4101(3) 0.13824(18) 0.0265(8) Uani 1 1 d . . . . .
H13 H 0.0524 0.4487 0.1014 0.032 Uiso 1 1 calc R . . . .
C14 C 0.0434(2) 0.3259(3) 0.15108(18) 0.0225(8) Uani 1 1 d . . . . .
H14 H -0.0057 0.3062 0.1224 0.027 Uiso 1 1 calc R . . . .
C15 C 0.08026(19) 0.2706(2) 0.20567(17) 0.0179(7) Uani 1 1 d . . . . .
H15 H 0.0566 0.2127 0.2141 0.021 Uiso 1 1 calc R . . . .
C16 C 0.15145(18) 0.2993(2) 0.24796(16) 0.0152(7) Uani 1 1 d . . . . .
H16 H 0.1759 0.2617 0.2858 0.018 Uiso 1 1 calc R . . . .
C1' C 0.36148(17) 0.3646(2) 0.41630(15) 0.0109(6) Uani 1 1 d . . . . .
C2' C 0.34443(17) 0.3372(2) 0.33462(15) 0.0110(6) Uani 1 1 d . . . . .
B3' B 0.4362(2) 0.3902(3) 0.36950(18) 0.0142(7) Uani 1 1 d . . . . .
H3' H 0.453(2) 0.460(2) 0.3548(17) 0.017 Uiso 1 1 d R . . . .
B4' B 0.4613(2) 0.3470(3) 0.4543(2) 0.0152(7) Uani 1 1 d . . . . .
H4' H 0.4868(19) 0.394(3) 0.4938(15) 0.018 Uiso 1 1 d R . . . .
B5' B 0.3854(2) 0.2674(3) 0.46689(19) 0.0139(7) Uani 1 1 d . . . . .
H5' H 0.369(2) 0.266(2) 0.5138(17) 0.017 Uiso 1 1 d R . . . .
B6' B 0.3101(2) 0.2597(3) 0.39069(18) 0.0129(7) Uani 1 1 d . . . . .
H6' H 0.249(2) 0.251(2) 0.3900(16) 0.015 Uiso 1 1 d R . . . .
B7' B 0.4292(2) 0.2970(3) 0.3112(2) 0.0150(7) Uani 1 1 d . . . . .
H7' H 0.4337(19) 0.317(2) 0.2574(17) 0.018 Uiso 1 1 d R . . . .
B8' B 0.5059(2) 0.3010(3) 0.38765(19) 0.0155(8) Uani 1 1 d . . . . .
H8' H 0.566(2) 0.316(2) 0.3861(16) 0.019 Uiso 1 1 d R . . . .
B9' B 0.4765(2) 0.2245(3) 0.44838(19) 0.0157(7) Uani 1 1 d . . . . .
H9' H 0.520(2) 0.188(2) 0.4857(16) 0.019 Uiso 1 1 d R . . . .
B10' B 0.3828(2) 0.1723(3) 0.40853(19) 0.0138(7) Uani 1 1 d . . . . .
H10' H 0.3630(19) 0.109(2) 0.4201(16) 0.017 Uiso 1 1 d R . . . .
B11' B 0.3534(2) 0.2179(3) 0.3236(2) 0.0157(7) Uani 1 1 d . . . . .
H11' H 0.315(2) 0.187(2) 0.2843(17) 0.019 Uiso 1 1 d R . . . .
B12' B 0.4567(2) 0.1930(3) 0.35990(19) 0.0153(7) Uani 1 1 d . . . . .
H12' H 0.4871(19) 0.137(2) 0.3406(16) 0.018 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 P1 2.2217(8) . ?
Au1 Cl1 2.2699(8) . ?
P1 C2 1.879(3) . ?
P1 C11 1.797(3) . ?
P1 C2' 1.878(3) . ?
C1 C2 1.652(4) . ?
C1 B3 1.773(5) . ?
C1 B4 1.718(4) . ?
C1 B5 1.715(5) . ?
C1 B6 1.766(5) . ?
C1 C1' 1.523(4) . ?
C2 B3 1.723(5) . ?
C2 B6 1.752(5) . ?
C2 B7 1.725(5) . ?
C2 B11 1.724(5) . ?
B3 H3 1.09(3) . ?
B3 B4 1.780(5) . ?
B3 B7 1.761(5) . ?
B3 B8 1.736(5) . ?
B4 H4 1.10(3) . ?
B4 B5 1.782(5) . ?
B4 B8 1.804(5) . ?
B4 B9 1.784(6) . ?
B5 H5 0.96(4) . ?
B5 B6 1.785(5) . ?
B5 B9 1.777(5) . ?
B5 B10 1.789(5) . ?
B6 H6 1.05(3) . ?
B6 B10 1.736(5) . ?
B6 B11 1.767(5) . ?
B7 H7 1.03(4) . ?
B7 B8 1.787(5) . ?
B7 B11 1.776(5) . ?
B7 B12 1.776(5) . ?
B8 H8 1.06(4) . ?
B8 B9 1.796(6) . ?
B8 B12 1.787(6) . ?
B9 H9 1.12(3) . ?
B9 B10 1.781(6) . ?
B9 B12 1.793(6) . ?
B10 H10 1.01(4) . ?
B10 B11 1.789(5) . ?
B10 B12 1.777(6) . ?
B11 H11 1.07(3) . ?
B11 B12 1.781(5) . ?
B12 H12 1.04(3) . ?
C11 C12 1.397(4) . ?
C11 C16 1.393(4) . ?
C12 H12A 0.9500 . ?
C12 C13 1.388(4) . ?
C13 H13 0.9500 . ?
C13 C14 1.388(5) . ?
C14 H14 0.9500 . ?
C14 C15 1.385(5) . ?
C15 H15 0.9500 . ?
C15 C16 1.385(4) . ?
C16 H16 0.9500 . ?
C1' C2' 1.649(4) . ?
C1' B3' 1.776(4) . ?
C1' B4' 1.728(5) . ?
C1' B5' 1.713(5) . ?
C1' B6' 1.752(5) . ?
C2' B3' 1.742(5) . ?
C2' B6' 1.764(5) . ?
C2' B7' 1.714(4) . ?
C2' B11' 1.725(5) . ?
B3' H3' 1.10(3) . ?
B3' B4' 1.774(5) . ?
B3' B7' 1.757(5) . ?
B3' B8' 1.724(5) . ?
B4' H4' 1.06(3) . ?
B4' B5' 1.780(5) . ?
B4' B8' 1.799(5) . ?
B4' B9' 1.772(5) . ?
B5' H5' 1.04(3) . ?
B5' B6' 1.775(5) . ?
B5' B9' 1.782(5) . ?
B5' B10' 1.786(5) . ?
B6' H6' 1.05(3) . ?
B6' B10' 1.739(5) . ?
B6' B11' 1.772(5) . ?
B7' H7' 1.13(3) . ?
B7' B8' 1.789(5) . ?
B7' B11' 1.774(5) . ?
B7' B12' 1.782(5) . ?
B8' H8' 1.06(3) . ?
B8' B9' 1.786(5) . ?
B8' B12' 1.784(5) . ?
B9' H9' 1.07(3) . ?
B9' B10' 1.787(5) . ?
B9' B12' 1.792(5) . ?
B10' H10' 1.01(3) . ?
B10' B11' 1.791(5) . ?
B10' B12' 1.778(5) . ?
B11' H11' 1.01(3) . ?
B11' B12' 1.792(5) . ?
B12' H12' 1.07(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Au1 Cl1 178.83(3) . . ?
C2 P1 Au1 112.68(10) . . ?
C11 P1 Au1 113.77(11) . . ?
C11 P1 C2 108.53(14) . . ?
C11 P1 C2' 111.95(15) . . ?
C2' P1 Au1 113.32(9) . . ?
C2' P1 C2 95.07(13) . . ?
C2 C1 B3 60.26(19) . . ?
C2 C1 B4 110.0(2) . . ?
C2 C1 B5 110.8(2) . . ?
C2 C1 B6 61.57(19) . . ?
B4 C1 B3 61.29(19) . . ?
B4 C1 B6 112.8(3) . . ?
B5 C1 B3 112.2(2) . . ?
B5 C1 B4 62.5(2) . . ?
B5 C1 B6 61.7(2) . . ?
B6 C1 B3 111.9(2) . . ?
C1' C1 C2 112.2(2) . . ?
C1' C1 B3 117.0(3) . . ?
C1' C1 B4 126.6(3) . . ?
C1' C1 B5 125.9(3) . . ?
C1' C1 B6 115.3(2) . . ?
C1 C2 P1 109.96(19) . . ?
C1 C2 B3 63.37(19) . . ?
C1 C2 B6 62.4(2) . . ?
C1 C2 B7 112.5(2) . . ?
C1 C2 B11 111.8(2) . . ?
B3 C2 P1 113.0(2) . . ?
B3 C2 B6 115.1(2) . . ?
B3 C2 B7 61.4(2) . . ?
B3 C2 B11 113.0(2) . . ?
B6 C2 P1 116.8(2) . . ?
B7 C2 P1 125.2(2) . . ?
B7 C2 B6 112.8(2) . . ?
B11 C2 P1 127.8(2) . . ?
B11 C2 B6 61.1(2) . . ?
B11 C2 B7 62.0(2) . . ?
C1 B3 H3 122.4(18) . . ?
C1 B3 B4 57.83(19) . . ?
C2 B3 C1 56.37(18) . . ?
C2 B3 H3 121.4(17) . . ?
C2 B3 B4 104.0(3) . . ?
C2 B3 B7 59.3(2) . . ?
C2 B3 B8 106.4(3) . . ?
B4 B3 H3 123.3(18) . . ?
B7 B3 C1 105.2(3) . . ?
B7 B3 H3 121.2(18) . . ?
B7 B3 B4 110.0(3) . . ?
B8 B3 C1 106.0(3) . . ?
B8 B3 H3 124.7(17) . . ?
B8 B3 B4 61.7(2) . . ?
B8 B3 B7 61.4(2) . . ?
C1 B4 B3 60.89(19) . . ?
C1 B4 H4 115.8(17) . . ?
C1 B4 B5 58.64(19) . . ?
C1 B4 B8 105.4(3) . . ?
C1 B4 B9 104.9(3) . . ?
B3 B4 H4 118.2(17) . . ?
B3 B4 B5 108.8(3) . . ?
B3 B4 B8 57.9(2) . . ?
B3 B4 B9 106.5(3) . . ?
B5 B4 H4 119.5(17) . . ?
B5 B4 B8 108.0(3) . . ?
B5 B4 B9 59.8(2) . . ?
B8 B4 H4 128.2(17) . . ?
B9 B4 H4 129.8(17) . . ?
B9 B4 B8 60.1(2) . . ?
C1 B5 B4 58.82(19) . . ?
C1 B5 H5 119(2) . . ?
C1 B5 B6 60.5(2) . . ?
C1 B5 B9 105.3(3) . . ?
C1 B5 B10 105.0(3) . . ?
B4 B5 H5 119(2) . . ?
B4 B5 B6 108.9(3) . . ?
B4 B5 B10 107.9(3) . . ?
B6 B5 H5 120(2) . . ?
B6 B5 B10 58.1(2) . . ?
B9 B5 B4 60.2(2) . . ?
B9 B5 H5 126(2) . . ?
B9 B5 B6 107.0(3) . . ?
B9 B5 B10 59.9(2) . . ?
B10 B5 H5 127(2) . . ?
C1 B6 B5 57.76(19) . . ?
C1 B6 H6 118.5(19) . . ?
C1 B6 B11 104.6(2) . . ?
C2 B6 C1 56.02(18) . . ?
C2 B6 B5 103.2(2) . . ?
C2 B6 H6 120.7(18) . . ?
C2 B6 B11 58.66(19) . . ?
B5 B6 H6 122.1(18) . . ?
B10 B6 C1 105.1(3) . . ?
B10 B6 C2 105.2(3) . . ?
B10 B6 B5 61.1(2) . . ?
B10 B6 H6 128.7(19) . . ?
B10 B6 B11 61.4(2) . . ?
B11 B6 B5 109.4(3) . . ?
B11 B6 H6 124.6(18) . . ?
C2 B7 B3 59.22(19) . . ?
C2 B7 H7 115.9(19) . . ?
C2 B7 B8 104.2(3) . . ?
C2 B7 B11 58.98(19) . . ?
C2 B7 B12 104.6(3) . . ?
B3 B7 H7 116.7(19) . . ?
B3 B7 B8 58.6(2) . . ?
B3 B7 B11 108.6(3) . . ?
B3 B7 B12 107.1(3) . . ?
B8 B7 H7 128(2) . . ?
B11 B7 H7 120(2) . . ?
B11 B7 B8 108.5(3) . . ?
B11 B7 B12 60.2(2) . . ?
B12 B7 H7 130.9(19) . . ?
B12 B7 B8 60.2(2) . . ?
B3 B8 B4 60.3(2) . . ?
B3 B8 B7 60.0(2) . . ?
B3 B8 H8 122.5(19) . . ?
B3 B8 B9 107.9(3) . . ?
B3 B8 B12 107.7(3) . . ?
B4 B8 H8 121(2) . . ?
B7 B8 B4 107.8(2) . . ?
B7 B8 H8 124(2) . . ?
B7 B8 B9 107.6(3) . . ?
B7 B8 B12 59.6(2) . . ?
B9 B8 B4 59.4(2) . . ?
B9 B8 H8 120(2) . . ?
B12 B8 B4 107.5(3) . . ?
B12 B8 H8 122.1(18) . . ?
B12 B8 B9 60.1(2) . . ?
B4 B9 B8 60.5(2) . . ?
B4 B9 H9 120.5(18) . . ?
B4 B9 B12 108.1(3) . . ?
B5 B9 B4 60.1(2) . . ?
B5 B9 B8 108.6(3) . . ?
B5 B9 H9 123.3(18) . . ?
B5 B9 B10 60.4(2) . . ?
B5 B9 B12 108.1(3) . . ?
B8 B9 H9 119.0(18) . . ?
B10 B9 B4 108.1(3) . . ?
B10 B9 B8 107.7(3) . . ?
B10 B9 H9 124.0(18) . . ?
B10 B9 B12 59.6(2) . . ?
B12 B9 B8 59.7(2) . . ?
B12 B9 H9 121.3(18) . . ?
B5 B10 H10 123(2) . . ?
B6 B10 B5 60.8(2) . . ?
B6 B10 B9 109.0(3) . . ?
B6 B10 H10 115.5(19) . . ?
B6 B10 B11 60.2(2) . . ?
B6 B10 B12 108.8(3) . . ?
B9 B10 B5 59.7(2) . . ?
B9 B10 H10 127.9(18) . . ?
B9 B10 B11 108.3(3) . . ?
B11 B10 B5 108.3(3) . . ?
B11 B10 H10 116.4(19) . . ?
B12 B10 B5 108.3(3) . . ?
B12 B10 B9 60.5(2) . . ?
B12 B10 H10 123(2) . . ?
B12 B10 B11 59.9(2) . . ?
C2 B11 B6 60.2(2) . . ?
C2 B11 B7 59.0(2) . . ?
C2 B11 B10 104.1(3) . . ?
C2 B11 H11 116.9(18) . . ?
C2 B11 B12 104.4(3) . . ?
B6 B11 B7 109.6(3) . . ?
B6 B11 B10 58.4(2) . . ?
B6 B11 H11 116.9(18) . . ?
B6 B11 B12 107.3(3) . . ?
B7 B11 B10 107.8(3) . . ?
B7 B11 H11 119.9(18) . . ?
B7 B11 B12 59.9(2) . . ?
B10 B11 H11 128.1(18) . . ?
B12 B11 B10 59.7(2) . . ?
B12 B11 H11 130.0(18) . . ?
B7 B12 B8 60.2(2) . . ?
B7 B12 B9 108.2(3) . . ?
B7 B12 B10 108.3(3) . . ?
B7 B12 B11 59.9(2) . . ?
B7 B12 H12 121(2) . . ?
B8 B12 B9 60.2(2) . . ?
B8 B12 H12 122.6(19) . . ?
B9 B12 H12 123.4(19) . . ?
B10 B12 B8 108.3(3) . . ?
B10 B12 B9 59.8(2) . . ?
B10 B12 B11 60.4(2) . . ?
B10 B12 H12 121.5(19) . . ?
B11 B12 B8 108.2(3) . . ?
B11 B12 B9 108.1(3) . . ?
B11 B12 H12 119.9(19) . . ?
C12 C11 P1 114.2(2) . . ?
C16 C11 P1 126.4(2) . . ?
C16 C11 C12 119.4(3) . . ?
C11 C12 H12A 119.9 . . ?
C13 C12 C11 120.1(3) . . ?
C13 C12 H12A 119.9 . . ?
C12 C13 H13 120.0 . . ?
C12 C13 C14 120.0(3) . . ?
C14 C13 H13 120.0 . . ?
C13 C14 H14 120.0 . . ?
C15 C14 C13 120.0(3) . . ?
C15 C14 H14 120.0 . . ?
C14 C15 H15 119.9 . . ?
C16 C15 C14 120.3(3) . . ?
C16 C15 H15 119.9 . . ?
C11 C16 H16 119.9 . . ?
C15 C16 C11 120.2(3) . . ?
C15 C16 H16 119.9 . . ?
C1 C1' C2' 111.9(2) . . ?
C1 C1' B3' 116.6(2) . . ?
C1 C1' B4' 126.0(3) . . ?
C1 C1' B5' 125.9(2) . . ?
C1 C1' B6' 115.6(2) . . ?
C2' C1' B3' 61.00(18) . . ?
C2' C1' B4' 110.5(2) . . ?
C2' C1' B5' 111.5(2) . . ?
C2' C1' B6' 62.42(19) . . ?
B4' C1' B3' 60.80(19) . . ?
B4' C1' B6' 112.8(2) . . ?
B5' C1' B3' 111.9(2) . . ?
B5' C1' B4' 62.3(2) . . ?
B5' C1' B6' 61.6(2) . . ?
B6' C1' B3' 113.0(2) . . ?
C1' C2' P1 109.9(2) . . ?
C1' C2' B3' 63.13(19) . . ?
C1' C2' B6' 61.67(19) . . ?
C1' C2' B7' 112.0(2) . . ?
C1' C2' B11' 111.0(2) . . ?
B3' C2' P1 106.3(2) . . ?
B3' C2' B6' 114.1(2) . . ?
B6' C2' P1 124.2(2) . . ?
B7' C2' P1 120.4(2) . . ?
B7' C2' B3' 61.1(2) . . ?
B7' C2' B6' 112.5(2) . . ?
B7' C2' B11' 62.1(2) . . ?
B11' C2' P1 132.8(2) . . ?
B11' C2' B3' 112.4(2) . . ?
B11' C2' B6' 61.0(2) . . ?
C1' B3' H3' 126.1(18) . . ?
C2' B3' C1' 55.87(17) . . ?
C2' B3' H3' 123.5(18) . . ?
C2' B3' B4' 104.2(2) . . ?
C2' B3' B7' 58.65(19) . . ?
B4' B3' C1' 58.24(19) . . ?
B4' B3' H3' 123.4(18) . . ?
B7' B3' C1' 104.2(2) . . ?
B7' B3' H3' 119.5(18) . . ?
B7' B3' B4' 110.2(3) . . ?
B8' B3' C1' 106.2(3) . . ?
B8' B3' C2' 106.5(3) . . ?
B8' B3' H3' 121.2(18) . . ?
B8' B3' B4' 61.9(2) . . ?
B8' B3' B7' 61.9(2) . . ?
C1' B4' B3' 60.96(19) . . ?
C1' B4' H4' 116.5(18) . . ?
C1' B4' B5' 58.46(19) . . ?
C1' B4' B8' 105.0(3) . . ?
C1' B4' B9' 104.9(3) . . ?
B3' B4' H4' 118.3(18) . . ?
B3' B4' B5' 108.9(3) . . ?
B3' B4' B8' 57.7(2) . . ?
B5' B4' H4' 119.4(17) . . ?
B5' B4' B8' 108.1(3) . . ?
B8' B4' H4' 128.1(17) . . ?
B9' B4' B3' 106.6(3) . . ?
B9' B4' H4' 129.2(19) . . ?
B9' B4' B5' 60.2(2) . . ?
B9' B4' B8' 60.0(2) . . ?
C1' B5' B4' 59.3(2) . . ?
C1' B5' H5' 118.9(19) . . ?
C1' B5' B6' 60.3(2) . . ?
C1' B5' B9' 105.1(2) . . ?
C1' B5' B10' 104.8(3) . . ?
B4' B5' H5' 119.2(19) . . ?
B4' B5' B9' 59.7(2) . . ?
B4' B5' B10' 107.8(3) . . ?
B6' B5' B4' 109.3(3) . . ?
B6' B5' H5' 119.9(19) . . ?
B6' B5' B9' 107.5(3) . . ?
B6' B5' B10' 58.5(2) . . ?
B9' B5' H5' 126.4(19) . . ?
B9' B5' B10' 60.1(2) . . ?
B10' B5' H5' 127.1(19) . . ?
C1' B6' C2' 55.91(18) . . ?
C1' B6' B5' 58.12(19) . . ?
C1' B6' H6' 122.5(18) . . ?
C1' B6' B11' 104.2(2) . . ?
C2' B6' B5' 103.5(2) . . ?
C2' B6' H6' 122.1(18) . . ?
C2' B6' B11' 58.40(19) . . ?
B5' B6' H6' 123.5(18) . . ?
B10' B6' C1' 105.2(2) . . ?
B10' B6' C2' 105.0(2) . . ?
B10' B6' B5' 61.1(2) . . ?
B10' B6' H6' 125.6(18) . . ?
B10' B6' B11' 61.3(2) . . ?
B11' B6' B5' 109.4(3) . . ?
B11' B6' H6' 121.9(18) . . ?
C2' B7' B3' 60.23(19) . . ?
C2' B7' H7' 114.5(16) . . ?
C2' B7' B8' 104.9(2) . . ?
C2' B7' B11' 59.27(19) . . ?
C2' B7' B12' 105.4(2) . . ?
B3' B7' H7' 116.0(17) . . ?
B3' B7' B8' 58.2(2) . . ?
B3' B7' B11' 109.4(3) . . ?
B3' B7' B12' 106.9(3) . . ?
B8' B7' H7' 128.4(17) . . ?
B11' B7' H7' 119.5(17) . . ?
B11' B7' B8' 108.6(3) . . ?
B11' B7' B12' 60.5(2) . . ?
B12' B7' H7' 131.6(17) . . ?
B12' B7' B8' 59.9(2) . . ?
B3' B8' B4' 60.4(2) . . ?
B3' B8' B7' 60.0(2) . . ?
B3' B8' H8' 118.3(18) . . ?
B3' B8' B9' 108.1(2) . . ?
B3' B8' B12' 108.3(3) . . ?
B4' B8' H8' 121.2(18) . . ?
B7' B8' B4' 107.6(2) . . ?
B7' B8' H8' 121.1(18) . . ?
B9' B8' B4' 59.2(2) . . ?
B9' B8' B7' 107.8(3) . . ?
B9' B8' H8' 124.3(18) . . ?
B12' B8' B4' 107.5(3) . . ?
B12' B8' B7' 59.8(2) . . ?
B12' B8' H8' 124.2(18) . . ?
B12' B8' B9' 60.2(2) . . ?
B4' B9' B5' 60.1(2) . . ?
B4' B9' B8' 60.8(2) . . ?
B4' B9' H9' 121.2(18) . . ?
B4' B9' B10' 108.1(3) . . ?
B4' B9' B12' 108.4(3) . . ?
B5' B9' B8' 108.6(3) . . ?
B5' B9' H9' 121.8(18) . . ?
B5' B9' B10' 60.0(2) . . ?
B5' B9' B12' 107.9(3) . . ?
B8' B9' H9' 121.2(18) . . ?
B8' B9' B10' 107.7(3) . . ?
B8' B9' B12' 59.8(2) . . ?
B10' B9' H9' 122.2(19) . . ?
B10' B9' B12' 59.6(2) . . ?
B12' B9' H9' 121.8(18) . . ?
B5' B10' B9' 59.9(2) . . ?
B5' B10' H10' 119.4(18) . . ?
B5' B10' B11' 108.1(3) . . ?
B6' B10' B5' 60.5(2) . . ?
B6' B10' B9' 108.8(3) . . ?
B6' B10' H10' 115.4(19) . . ?
B6' B10' B11' 60.2(2) . . ?
B6' B10' B12' 109.1(3) . . ?
B9' B10' H10' 125.6(19) . . ?
B9' B10' B11' 108.3(3) . . ?
B11' B10' H10' 120.2(19) . . ?
B12' B10' B5' 108.3(3) . . ?
B12' B10' B9' 60.3(2) . . ?
B12' B10' H10' 125.9(18) . . ?
B12' B10' B11' 60.3(2) . . ?
C2' B11' B6' 60.6(2) . . ?
C2' B11' B7' 58.6(2) . . ?
C2' B11' B10' 104.5(3) . . ?
C2' B11' H11' 118(2) . . ?
C2' B11' B12' 104.5(3) . . ?
B6' B11' B7' 109.2(3) . . ?
B6' B11' B10' 58.4(2) . . ?
B6' B11' H11' 115.4(19) . . ?
B6' B11' B12' 107.0(3) . . ?
B7' B11' B10' 107.5(3) . . ?
B7' B11' H11' 122.4(19) . . ?
B7' B11' B12' 60.0(2) . . ?
B10' B11' H11' 126(2) . . ?
B10' B11' B12' 59.5(2) . . ?
B12' B11' H11' 130.6(19) . . ?
B7' B12' B8' 60.2(2) . . ?
B7' B12' B9' 107.8(3) . . ?
B7' B12' B11' 59.5(2) . . ?
B7' B12' H12' 120.9(18) . . ?
B8' B12' B9' 59.9(2) . . ?
B8' B12' B11' 108.1(3) . . ?
B8' B12' H12' 121.7(18) . . ?
B9' B12' B11' 108.1(3) . . ?
B9' B12' H12' 123.0(18) . . ?
B10' B12' B7' 107.8(3) . . ?
B10' B12' B8' 108.2(3) . . ?
B10' B12' B9' 60.1(2) . . ?
B10' B12' B11' 60.3(2) . . ?
B10' B12' H12' 122.2(18) . . ?
B11' B12' H12' 120.8(18) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au1 P1 C2 C1 -114.95(17) . . . . ?
Au1 P1 C2 B3 176.39(17) . . . . ?
Au1 P1 C2 B6 -46.6(2) . . . . ?
Au1 P1 C2 B7 106.0(2) . . . . ?
Au1 P1 C2 B11 26.4(3) . . . . ?
Au1 P1 C11 C12 -28.8(3) . . . . ?
Au1 P1 C11 C16 149.4(2) . . . . ?
Au1 P1 C2' C1' 109.83(17) . . . . ?
Au1 P1 C2' B3' 43.1(2) . . . . ?
Au1 P1 C2' B6' 178.5(2) . . . . ?
Au1 P1 C2' B7' -22.6(3) . . . . ?
Au1 P1 C2' B11' -101.2(3) . . . . ?
P1 C2 B3 C1 101.7(2) . . . . ?
P1 C2 B3 B4 136.0(2) . . . . ?
P1 C2 B3 B7 -118.8(2) . . . . ?
P1 C2 B3 B8 -159.8(2) . . . . ?
P1 C2 B6 C1 -99.6(2) . . . . ?
P1 C2 B6 B5 -134.7(2) . . . . ?
P1 C2 B6 B10 162.2(2) . . . . ?
P1 C2 B6 B11 120.4(3) . . . . ?
P1 C2 B7 B3 99.3(3) . . . . ?
P1 C2 B7 B8 138.4(2) . . . . ?
P1 C2 B7 B11 -118.3(3) . . . . ?
P1 C2 B7 B12 -159.2(2) . . . . ?
P1 C2 B11 B6 -103.0(3) . . . . ?
P1 C2 B11 B7 114.4(3) . . . . ?
P1 C2 B11 B10 -143.0(2) . . . . ?
P1 C2 B11 B12 155.1(2) . . . . ?
P1 C11 C12 C13 -179.8(3) . . . . ?
P1 C11 C16 C15 -178.1(2) . . . . ?
P1 C2' B3' C1' 104.5(2) . . . . ?
P1 C2' B3' B4' 138.6(2) . . . . ?
P1 C2' B3' B7' -116.1(2) . . . . ?
P1 C2' B3' B8' -156.9(2) . . . . ?
P1 C2' B6' C1' -95.8(3) . . . . ?
P1 C2' B6' B5' -131.0(2) . . . . ?
P1 C2' B6' B10' 165.8(2) . . . . ?
P1 C2' B6' B11' 124.3(3) . . . . ?
P1 C2' B7' B3' 92.7(3) . . . . ?
P1 C2' B7' B8' 131.4(2) . . . . ?
P1 C2' B7' B11' -125.5(3) . . . . ?
P1 C2' B7' B12' -166.3(2) . . . . ?
P1 C2' B11' B6' -111.3(3) . . . . ?
P1 C2' B11' B7' 106.8(3) . . . . ?
P1 C2' B11' B10' -151.2(2) . . . . ?
P1 C2' B11' B12' 147.1(2) . . . . ?
C1 C2 B3 B4 34.4(2) . . . . ?
C1 C2 B3 B7 139.6(3) . . . . ?
C1 C2 B3 B8 98.5(3) . . . . ?
C1 C2 B6 B5 -35.1(2) . . . . ?
C1 C2 B6 B10 -98.2(3) . . . . ?
C1 C2 B6 B11 -140.0(3) . . . . ?
C1 C2 B7 B3 -38.9(3) . . . . ?
C1 C2 B7 B8 0.3(3) . . . . ?
C1 C2 B7 B11 103.5(3) . . . . ?
C1 C2 B7 B12 62.6(3) . . . . ?
C1 C2 B11 B6 37.8(2) . . . . ?
C1 C2 B11 B7 -104.8(3) . . . . ?
C1 C2 B11 B10 -2.2(3) . . . . ?
C1 C2 B11 B12 -64.0(3) . . . . ?
C1 B3 B4 B5 35.1(2) . . . . ?
C1 B3 B4 B8 135.0(3) . . . . ?
C1 B3 B4 B9 98.1(3) . . . . ?
C1 B3 B7 C2 34.0(2) . . . . ?
C1 B3 B7 B8 -100.2(3) . . . . ?
C1 B3 B7 B11 0.5(3) . . . . ?
C1 B3 B7 B12 -63.0(3) . . . . ?
C1 B3 B8 B4 -38.5(2) . . . . ?
C1 B3 B8 B7 98.9(3) . . . . ?
C1 B3 B8 B9 -1.5(3) . . . . ?
C1 B3 B8 B12 61.9(3) . . . . ?
C1 B4 B5 B6 35.5(2) . . . . ?
C1 B4 B5 B9 134.6(3) . . . . ?
C1 B4 B5 B10 97.0(3) . . . . ?
C1 B4 B8 B3 39.8(2) . . . . ?
C1 B4 B8 B7 1.8(3) . . . . ?
C1 B4 B8 B9 -98.5(3) . . . . ?
C1 B4 B8 B12 -61.0(3) . . . . ?
C1 B4 B9 B5 -39.0(2) . . . . ?
C1 B4 B9 B8 99.5(3) . . . . ?
C1 B4 B9 B10 -1.1(3) . . . . ?
C1 B4 B9 B12 62.0(3) . . . . ?
C1 B5 B6 C2 34.3(2) . . . . ?
C1 B5 B6 B10 134.5(3) . . . . ?
C1 B5 B6 B11 95.3(3) . . . . ?
C1 B5 B9 B4 39.1(2) . . . . ?
C1 B5 B9 B8 1.6(3) . . . . ?
C1 B5 B9 B10 -98.7(3) . . . . ?
C1 B5 B9 B12 -61.7(3) . . . . ?
C1 B5 B10 B6 -40.0(2) . . . . ?
C1 B5 B10 B9 99.2(3) . . . . ?
C1 B5 B10 B11 -1.7(3) . . . . ?
C1 B5 B10 B12 61.8(3) . . . . ?
C1 B6 B10 B5 38.7(2) . . . . ?
C1 B6 B10 B9 2.1(3) . . . . ?
C1 B6 B10 B11 -98.6(3) . . . . ?
C1 B6 B10 B12 -62.3(3) . . . . ?
C1 B6 B11 C2 -33.4(2) . . . . ?
C1 B6 B11 B7 0.1(3) . . . . ?
C1 B6 B11 B10 99.5(3) . . . . ?
C1 B6 B11 B12 63.6(3) . . . . ?
C1 C1' C2' P1 10.5(3) . . . . ?
C1 C1' C2' B3' 109.2(3) . . . . ?
C1 C1' C2' B6' -108.4(3) . . . . ?
C1 C1' C2' B7' 147.1(3) . . . . ?
C1 C1' C2' B11' -145.5(2) . . . . ?
C1 C1' B3' C2' -101.6(3) . . . . ?
C1 C1' B3' B4' 118.2(3) . . . . ?
C1 C1' B3' B7' -136.5(3) . . . . ?
C1 C1' B3' B8' 159.1(3) . . . . ?
C1 C1' B4' B3' -103.2(3) . . . . ?
C1 C1' B4' B5' 115.9(3) . . . . ?
C1 C1' B4' B8' -141.8(3) . . . . ?
C1 C1' B4' B9' 155.9(3) . . . . ?
C1 C1' B5' B4' -116.1(3) . . . . ?
C1 C1' B5' B6' 102.4(3) . . . . ?
C1 C1' B5' B9' -155.8(3) . . . . ?
C1 C1' B5' B10' 141.7(3) . . . . ?
C1 C1' B6' C2' 102.5(3) . . . . ?
C1 C1' B6' B5' -118.7(3) . . . . ?
C1 C1' B6' B10' -159.3(3) . . . . ?
C1 C1' B6' B11' 137.0(3) . . . . ?
C2 P1 C11 C12 97.5(3) . . . . ?
C2 P1 C11 C16 -84.4(3) . . . . ?
C2 P1 C2' C1' -7.5(2) . . . . ?
C2 P1 C2' B3' -74.3(2) . . . . ?
C2 P1 C2' B6' 61.1(3) . . . . ?
C2 P1 C2' B7' -139.9(2) . . . . ?
C2 P1 C2' B11' 141.4(3) . . . . ?
C2 C1 B3 B4 -139.7(3) . . . . ?
C2 C1 B3 B7 -35.3(2) . . . . ?
C2 C1 B3 B8 -99.4(3) . . . . ?
C2 C1 B4 B3 36.7(2) . . . . ?
C2 C1 B4 B5 -103.7(3) . . . . ?
C2 C1 B4 B8 -1.7(3) . . . . ?
C2 C1 B4 B9 -64.2(3) . . . . ?
C2 C1 B5 B4 102.4(3) . . . . ?
C2 C1 B5 B6 -38.5(2) . . . . ?
C2 C1 B5 B9 62.7(3) . . . . ?
C2 C1 B5 B10 0.3(3) . . . . ?
C2 C1 B6 B5 138.6(2) . . . . ?
C2 C1 B6 B10 98.3(3) . . . . ?
C2 C1 B6 B11 34.6(2) . . . . ?
C2 C1 C1' C2' -8.5(3) . . . . ?
C2 C1 C1' B3' 59.0(3) . . . . ?
C2 C1 C1' B4' 130.9(3) . . . . ?
C2 C1 C1' B5' -149.7(3) . . . . ?
C2 C1 C1' B6' -77.4(3) . . . . ?
C2 B3 B4 C1 -33.7(2) . . . . ?
C2 B3 B4 B5 1.4(3) . . . . ?
C2 B3 B4 B8 101.3(3) . . . . ?
C2 B3 B4 B9 64.4(3) . . . . ?
C2 B3 B7 B8 -134.2(3) . . . . ?
C2 B3 B7 B11 -33.5(2) . . . . ?
C2 B3 B7 B12 -97.1(3) . . . . ?
C2 B3 B8 B4 -97.4(3) . . . . ?
C2 B3 B8 B7 40.0(2) . . . . ?
C2 B3 B8 B9 -60.4(3) . . . . ?
C2 B3 B8 B12 3.0(3) . . . . ?
C2 B6 B10 B5 96.9(3) . . . . ?
C2 B6 B10 B9 60.3(3) . . . . ?
C2 B6 B10 B11 -40.4(2) . . . . ?
C2 B6 B10 B12 -4.1(3) . . . . ?
C2 B6 B11 B7 33.6(2) . . . . ?
C2 B6 B11 B10 132.9(3) . . . . ?
C2 B6 B11 B12 97.0(3) . . . . ?
C2 B7 B8 B3 -39.4(2) . . . . ?
C2 B7 B8 B4 -1.3(3) . . . . ?
C2 B7 B8 B9 61.4(3) . . . . ?
C2 B7 B8 B12 98.9(3) . . . . ?
C2 B7 B11 B6 -34.0(2) . . . . ?
C2 B7 B11 B10 -96.1(3) . . . . ?
C2 B7 B11 B12 -133.1(3) . . . . ?
C2 B7 B12 B8 -98.2(3) . . . . ?
C2 B7 B12 B9 -60.5(3) . . . . ?
C2 B7 B12 B10 2.9(3) . . . . ?
C2 B7 B12 B11 40.3(2) . . . . ?
C2 B11 B12 B7 -40.3(2) . . . . ?
C2 B11 B12 B8 -3.0(3) . . . . ?
C2 B11 B12 B9 60.7(3) . . . . ?
C2 B11 B12 B10 98.1(3) . . . . ?
B3 C1 C2 P1 -106.4(2) . . . . ?
B3 C1 C2 B6 142.9(3) . . . . ?
B3 C1 C2 B7 38.1(3) . . . . ?
B3 C1 C2 B11 105.6(3) . . . . ?
B3 C1 B4 B5 -140.4(3) . . . . ?
B3 C1 B4 B8 -38.4(2) . . . . ?
B3 C1 B4 B9 -100.9(3) . . . . ?
B3 C1 B5 B4 37.2(3) . . . . ?
B3 C1 B5 B6 -103.8(3) . . . . ?
B3 C1 B5 B9 -2.6(3) . . . . ?
B3 C1 B5 B10 -64.9(3) . . . . ?
B3 C1 B6 C2 -34.3(2) . . . . ?
B3 C1 B6 B5 104.3(3) . . . . ?
B3 C1 B6 B10 64.0(3) . . . . ?
B3 C1 B6 B11 0.2(3) . . . . ?
B3 C1 C1' C2' 58.3(3) . . . . ?
B3 C1 C1' B3' 125.8(3) . . . . ?
B3 C1 C1' B4' -162.3(3) . . . . ?
B3 C1 C1' B5' -82.8(4) . . . . ?
B3 C1 C1' B6' -10.5(4) . . . . ?
B3 C2 B6 C1 36.5(2) . . . . ?
B3 C2 B6 B5 1.5(3) . . . . ?
B3 C2 B6 B10 -61.7(3) . . . . ?
B3 C2 B6 B11 -103.5(3) . . . . ?
B3 C2 B7 B8 39.1(2) . . . . ?
B3 C2 B7 B11 142.4(3) . . . . ?
B3 C2 B7 B12 101.5(3) . . . . ?
B3 C2 B11 B6 107.0(3) . . . . ?
B3 C2 B11 B7 -35.6(3) . . . . ?
B3 C2 B11 B10 67.0(3) . . . . ?
B3 C2 B11 B12 5.2(3) . . . . ?
B3 B4 B5 C1 -36.0(2) . . . . ?
B3 B4 B5 B6 -0.6(3) . . . . ?
B3 B4 B5 B9 98.6(3) . . . . ?
B3 B4 B5 B10 61.0(3) . . . . ?
B3 B4 B8 B7 -38.0(3) . . . . ?
B3 B4 B8 B9 -138.3(3) . . . . ?
B3 B4 B8 B12 -100.9(3) . . . . ?
B3 B4 B9 B5 -102.5(3) . . . . ?
B3 B4 B9 B8 36.0(2) . . . . ?
B3 B4 B9 B10 -64.6(3) . . . . ?
B3 B4 B9 B12 -1.5(3) . . . . ?
B3 B7 B8 B4 38.2(3) . . . . ?
B3 B7 B8 B9 100.9(3) . . . . ?
B3 B7 B8 B12 138.3(3) . . . . ?
B3 B7 B11 C2 33.6(2) . . . . ?
B3 B7 B11 B6 -0.4(4) . . . . ?
B3 B7 B11 B10 -62.5(3) . . . . ?
B3 B7 B11 B12 -99.5(3) . . . . ?
B3 B7 B12 B8 -36.4(2) . . . . ?
B3 B7 B12 B9 1.3(3) . . . . ?
B3 B7 B12 B10 64.6(3) . . . . ?
B3 B7 B12 B11 102.1(3) . . . . ?
B3 B8 B9 B4 -37.4(2) . . . . ?
B3 B8 B9 B5 0.0(4) . . . . ?
B3 B8 B9 B10 63.9(3) . . . . ?
B3 B8 B9 B12 100.6(3) . . . . ?
B3 B8 B12 B7 37.2(3) . . . . ?
B3 B8 B12 B9 -100.8(3) . . . . ?
B3 B8 B12 B10 -63.9(3) . . . . ?
B3 B8 B12 B11 0.0(4) . . . . ?
B4 C1 C2 P1 -143.6(2) . . . . ?
B4 C1 C2 B3 -37.1(2) . . . . ?
B4 C1 C2 B6 105.8(3) . . . . ?
B4 C1 C2 B7 0.9(3) . . . . ?
B4 C1 C2 B11 68.5(3) . . . . ?
B4 C1 B3 C2 139.7(3) . . . . ?
B4 C1 B3 B7 104.4(3) . . . . ?
B4 C1 B3 B8 40.3(3) . . . . ?
B4 C1 B5 B6 -140.9(3) . . . . ?
B4 C1 B5 B9 -39.8(2) . . . . ?
B4 C1 B5 B10 -102.1(3) . . . . ?
B4 C1 B6 C2 -101.2(3) . . . . ?
B4 C1 B6 B5 37.4(2) . . . . ?
B4 C1 B6 B10 -2.9(3) . . . . ?
B4 C1 B6 B11 -66.7(3) . . . . ?
B4 C1 C1' C2' 131.3(3) . . . . ?
B4 C1 C1' B3' -161.2(3) . . . . ?
B4 C1 C1' B4' -89.3(4) . . . . ?
B4 C1 C1' B5' -9.9(5) . . . . ?
B4 C1 C1' B6' 62.4(4) . . . . ?
B4 B3 B7 C2 94.8(3) . . . . ?
B4 B3 B7 B8 -39.4(2) . . . . ?
B4 B3 B7 B11 61.3(3) . . . . ?
B4 B3 B7 B12 -2.2(3) . . . . ?
B4 B3 B8 B7 137.4(3) . . . . ?
B4 B3 B8 B9 37.0(3) . . . . ?
B4 B3 B8 B12 100.4(3) . . . . ?
B4 B5 B6 C1 -34.7(2) . . . . ?
B4 B5 B6 C2 -0.5(3) . . . . ?
B4 B5 B6 B10 99.8(3) . . . . ?
B4 B5 B6 B11 60.6(3) . . . . ?
B4 B5 B9 B8 -37.6(3) . . . . ?
B4 B5 B9 B10 -137.8(3) . . . . ?
B4 B5 B9 B12 -100.8(3) . . . . ?
B4 B5 B10 B6 -101.5(3) . . . . ?
B4 B5 B10 B9 37.7(2) . . . . ?
B4 B5 B10 B11 -63.2(3) . . . . ?
B4 B5 B10 B12 0.3(3) . . . . ?
B4 B8 B9 B5 37.3(3) . . . . ?
B4 B8 B9 B10 101.2(3) . . . . ?
B4 B8 B9 B12 138.0(3) . . . . ?
B4 B8 B12 B7 100.8(3) . . . . ?
B4 B8 B12 B9 -37.2(2) . . . . ?
B4 B8 B12 B10 -0.2(3) . . . . ?
B4 B8 B12 B11 63.7(3) . . . . ?
B4 B9 B10 B5 -37.7(2) . . . . ?
B4 B9 B10 B6 -0.6(4) . . . . ?
B4 B9 B10 B11 63.2(3) . . . . ?
B4 B9 B10 B12 100.7(3) . . . . ?
B4 B9 B12 B7 0.2(3) . . . . ?
B4 B9 B12 B8 37.8(2) . . . . ?
B4 B9 B12 B10 -100.9(3) . . . . ?
B4 B9 B12 B11 -63.2(3) . . . . ?
B5 C1 C2 P1 149.2(2) . . . . ?
B5 C1 C2 B3 -104.4(3) . . . . ?
B5 C1 C2 B6 38.5(2) . . . . ?
B5 C1 C2 B7 -66.3(3) . . . . ?
B5 C1 C2 B11 1.2(3) . . . . ?
B5 C1 B3 C2 102.0(3) . . . . ?
B5 C1 B3 B4 -37.7(3) . . . . ?
B5 C1 B3 B7 66.7(3) . . . . ?
B5 C1 B3 B8 2.7(3) . . . . ?
B5 C1 B4 B3 140.4(3) . . . . ?
B5 C1 B4 B8 102.0(3) . . . . ?
B5 C1 B4 B9 39.5(2) . . . . ?
B5 C1 B6 C2 -138.6(2) . . . . ?
B5 C1 B6 B10 -40.3(2) . . . . ?
B5 C1 B6 B11 -104.0(3) . . . . ?
B5 C1 C1' C2' -148.6(3) . . . . ?
B5 C1 C1' B3' -81.1(4) . . . . ?
B5 C1 C1' B4' -9.2(5) . . . . ?
B5 C1 C1' B5' 70.2(4) . . . . ?
B5 C1 C1' B6' 142.5(3) . . . . ?
B5 B4 B8 B3 101.3(3) . . . . ?
B5 B4 B8 B7 63.3(3) . . . . ?
B5 B4 B8 B9 -37.1(3) . . . . ?
B5 B4 B8 B12 0.4(3) . . . . ?
B5 B4 B9 B8 138.4(3) . . . . ?
B5 B4 B9 B10 37.9(2) . . . . ?
B5 B4 B9 B12 101.0(3) . . . . ?
B5 B6 B10 B9 -36.6(3) . . . . ?
B5 B6 B10 B11 -137.3(3) . . . . ?
B5 B6 B10 B12 -101.0(3) . . . . ?
B5 B6 B11 C2 -93.9(3) . . . . ?
B5 B6 B11 B7 -60.3(3) . . . . ?
B5 B6 B11 B10 39.0(3) . . . . ?
B5 B6 B11 B12 3.2(3) . . . . ?
B5 B9 B10 B6 37.1(3) . . . . ?
B5 B9 B10 B11 101.0(3) . . . . ?
B5 B9 B10 B12 138.5(3) . . . . ?
B5 B9 B12 B7 63.7(3) . . . . ?
B5 B9 B12 B8 101.4(3) . . . . ?
B5 B9 B12 B10 -37.3(3) . . . . ?
B5 B9 B12 B11 0.3(4) . . . . ?
B5 B10 B11 C2 2.4(3) . . . . ?
B5 B10 B11 B6 -38.6(2) . . . . ?
B5 B10 B11 B7 63.9(3) . . . . ?
B5 B10 B11 B12 101.0(3) . . . . ?
B5 B10 B12 B7 -63.8(3) . . . . ?
B5 B10 B12 B8 0.0(3) . . . . ?
B5 B10 B12 B9 37.1(2) . . . . ?
B5 B10 B12 B11 -101.0(3) . . . . ?
B6 C1 C2 P1 110.6(2) . . . . ?
B6 C1 C2 B3 -142.9(3) . . . . ?
B6 C1 C2 B7 -104.8(3) . . . . ?
B6 C1 C2 B11 -37.3(2) . . . . ?
B6 C1 B3 C2 34.8(2) . . . . ?
B6 C1 B3 B4 -104.9(3) . . . . ?
B6 C1 B3 B7 -0.5(3) . . . . ?
B6 C1 B3 B8 -64.5(3) . . . . ?
B6 C1 B4 B3 103.4(3) . . . . ?
B6 C1 B4 B5 -37.0(2) . . . . ?
B6 C1 B4 B8 64.9(3) . . . . ?
B6 C1 B4 B9 2.5(3) . . . . ?
B6 C1 B5 B4 140.9(3) . . . . ?
B6 C1 B5 B9 101.1(3) . . . . ?
B6 C1 B5 B10 38.8(2) . . . . ?
B6 C1 C1' C2' -76.4(3) . . . . ?
B6 C1 C1' B3' -8.9(4) . . . . ?
B6 C1 C1' B4' 63.0(4) . . . . ?
B6 C1 C1' B5' 142.4(3) . . . . ?
B6 C1 C1' B6' -145.3(2) . . . . ?
B6 C2 B3 C1 -36.2(2) . . . . ?
B6 C2 B3 B4 -1.8(3) . . . . ?
B6 C2 B3 B7 103.4(3) . . . . ?
B6 C2 B3 B8 62.4(3) . . . . ?
B6 C2 B7 B3 -107.2(3) . . . . ?
B6 C2 B7 B8 -68.1(3) . . . . ?
B6 C2 B7 B11 35.2(3) . . . . ?
B6 C2 B7 B12 -5.7(3) . . . . ?
B6 C2 B11 B7 -142.6(3) . . . . ?
B6 C2 B11 B10 -40.1(2) . . . . ?
B6 C2 B11 B12 -101.9(3) . . . . ?
B6 B5 B9 B4 102.4(3) . . . . ?
B6 B5 B9 B8 64.9(3) . . . . ?
B6 B5 B9 B10 -35.4(2) . . . . ?
B6 B5 B9 B12 1.6(3) . . . . ?
B6 B5 B10 B9 139.2(3) . . . . ?
B6 B5 B10 B11 38.3(2) . . . . ?
B6 B5 B10 B12 101.8(3) . . . . ?
B6 B10 B11 C2 41.0(2) . . . . ?
B6 B10 B11 B7 102.5(3) . . . . ?
B6 B10 B11 B12 139.6(3) . . . . ?
B6 B10 B12 B7 0.8(4) . . . . ?
B6 B10 B12 B8 64.6(3) . . . . ?
B6 B10 B12 B9 101.7(3) . . . . ?
B6 B10 B12 B11 -36.4(3) . . . . ?
B6 B11 B12 B7 -103.1(3) . . . . ?
B6 B11 B12 B8 -65.8(3) . . . . ?
B6 B11 B12 B9 -2.1(4) . . . . ?
B6 B11 B12 B10 35.3(3) . . . . ?
B7 C2 B3 C1 -139.6(3) . . . . ?
B7 C2 B3 B4 -105.2(3) . . . . ?
B7 C2 B3 B8 -41.0(2) . . . . ?
B7 C2 B6 C1 104.5(3) . . . . ?
B7 C2 B6 B5 69.4(3) . . . . ?
B7 C2 B6 B10 6.2(3) . . . . ?
B7 C2 B6 B11 -35.5(3) . . . . ?
B7 C2 B11 B6 142.6(3) . . . . ?
B7 C2 B11 B10 102.6(3) . . . . ?
B7 C2 B11 B12 40.7(2) . . . . ?
B7 B3 B4 C1 -95.8(3) . . . . ?
B7 B3 B4 B5 -60.7(3) . . . . ?
B7 B3 B4 B8 39.2(2) . . . . ?
B7 B3 B4 B9 2.3(3) . . . . ?
B7 B3 B8 B4 -137.4(3) . . . . ?
B7 B3 B8 B9 -100.5(3) . . . . ?
B7 B3 B8 B12 -37.0(3) . . . . ?
B7 B8 B9 B4 -100.7(3) . . . . ?
B7 B8 B9 B5 -63.3(3) . . . . ?
B7 B8 B9 B10 0.6(3) . . . . ?
B7 B8 B9 B12 37.3(2) . . . . ?
B7 B8 B12 B9 -138.0(3) . . . . ?
B7 B8 B12 B10 -101.0(3) . . . . ?
B7 B8 B12 B11 -37.1(2) . . . . ?
B7 B11 B12 B8 37.3(3) . . . . ?
B7 B11 B12 B9 101.0(3) . . . . ?
B7 B11 B12 B10 138.4(3) . . . . ?
B8 B3 B4 C1 -135.0(3) . . . . ?
B8 B3 B4 B5 -99.9(3) . . . . ?
B8 B3 B4 B9 -36.9(2) . . . . ?
B8 B3 B7 C2 134.2(3) . . . . ?
B8 B3 B7 B11 100.7(3) . . . . ?
B8 B3 B7 B12 37.1(3) . . . . ?
B8 B4 B5 C1 -97.4(3) . . . . ?
B8 B4 B5 B6 -62.0(3) . . . . ?
B8 B4 B5 B9 37.2(3) . . . . ?
B8 B4 B5 B10 -0.4(3) . . . . ?
B8 B4 B9 B5 -138.4(3) . . . . ?
B8 B4 B9 B10 -100.6(3) . . . . ?
B8 B4 B9 B12 -37.5(2) . . . . ?
B8 B7 B11 C2 95.7(3) . . . . ?
B8 B7 B11 B6 61.7(3) . . . . ?
B8 B7 B11 B10 -0.3(3) . . . . ?
B8 B7 B11 B12 -37.3(2) . . . . ?
B8 B7 B12 B9 37.7(3) . . . . ?
B8 B7 B12 B10 101.1(3) . . . . ?
B8 B7 B12 B11 138.5(3) . . . . ?
B8 B9 B10 B5 -101.7(3) . . . . ?
B8 B9 B10 B6 -64.6(3) . . . . ?
B8 B9 B10 B11 -0.8(3) . . . . ?
B8 B9 B10 B12 36.8(2) . . . . ?
B8 B9 B12 B7 -37.7(2) . . . . ?
B8 B9 B12 B10 -138.7(3) . . . . ?
B8 B9 B12 B11 -101.0(3) . . . . ?
B9 B4 B5 C1 -134.6(3) . . . . ?
B9 B4 B5 B6 -99.2(3) . . . . ?
B9 B4 B5 B10 -37.6(2) . . . . ?
B9 B4 B8 B3 138.3(3) . . . . ?
B9 B4 B8 B7 100.4(3) . . . . ?
B9 B4 B8 B12 37.5(2) . . . . ?
B9 B5 B6 C1 -98.3(3) . . . . ?
B9 B5 B6 C2 -64.0(3) . . . . ?
B9 B5 B6 B10 36.2(3) . . . . ?
B9 B5 B6 B11 -3.0(3) . . . . ?
B9 B5 B10 B6 -139.2(3) . . . . ?
B9 B5 B10 B11 -100.9(3) . . . . ?
B9 B5 B10 B12 -37.5(3) . . . . ?
B9 B8 B12 B7 138.0(3) . . . . ?
B9 B8 B12 B10 37.0(2) . . . . ?
B9 B8 B12 B11 100.9(3) . . . . ?
B9 B10 B11 C2 -60.9(3) . . . . ?
B9 B10 B11 B6 -101.8(3) . . . . ?
B9 B10 B11 B7 0.7(3) . . . . ?
B9 B10 B11 B12 37.8(3) . . . . ?
B9 B10 B12 B7 -100.9(3) . . . . ?
B9 B10 B12 B8 -37.1(3) . . . . ?
B9 B10 B12 B11 -138.1(3) . . . . ?
B10 B5 B6 C1 -134.5(3) . . . . ?
B10 B5 B6 C2 -100.2(3) . . . . ?
B10 B5 B6 B11 -39.2(3) . . . . ?
B10 B5 B9 B4 137.8(3) . . . . ?
B10 B5 B9 B8 100.3(3) . . . . ?
B10 B5 B9 B12 37.0(3) . . . . ?
B10 B6 B11 C2 -132.9(3) . . . . ?
B10 B6 B11 B7 -99.3(3) . . . . ?
B10 B6 B11 B12 -35.9(3) . . . . ?
B10 B9 B12 B7 101.0(3) . . . . ?
B10 B9 B12 B8 138.7(3) . . . . ?
B10 B9 B12 B11 37.7(3) . . . . ?
B10 B11 B12 B7 -138.4(3) . . . . ?
B10 B11 B12 B8 -101.2(3) . . . . ?
B10 B11 B12 B9 -37.4(3) . . . . ?
B11 C2 B3 C1 -103.8(3) . . . . ?
B11 C2 B3 B4 -69.4(3) . . . . ?
B11 C2 B3 B7 35.8(3) . . . . ?
B11 C2 B3 B8 -5.2(3) . . . . ?
B11 C2 B6 C1 140.0(3) . . . . ?
B11 C2 B6 B5 104.9(3) . . . . ?
B11 C2 B6 B10 41.8(2) . . . . ?
B11 C2 B7 B3 -142.4(3) . . . . ?
B11 C2 B7 B8 -103.3(3) . . . . ?
B11 C2 B7 B12 -40.9(2) . . . . ?
B11 B6 B10 B5 137.3(3) . . . . ?
B11 B6 B10 B9 100.7(3) . . . . ?
B11 B6 B10 B12 36.3(3) . . . . ?
B11 B7 B8 B3 -101.0(3) . . . . ?
B11 B7 B8 B4 -62.9(3) . . . . ?
B11 B7 B8 B9 -0.2(3) . . . . ?
B11 B7 B8 B12 37.3(2) . . . . ?
B11 B7 B12 B8 -138.5(3) . . . . ?
B11 B7 B12 B9 -100.8(3) . . . . ?
B11 B7 B12 B10 -37.4(3) . . . . ?
B11 B10 B12 B7 37.2(3) . . . . ?
B11 B10 B12 B8 101.0(3) . . . . ?
B11 B10 B12 B9 138.1(3) . . . . ?
B12 B7 B8 B3 -138.3(3) . . . . ?
B12 B7 B8 B4 -100.2(3) . . . . ?
B12 B7 B8 B9 -37.5(2) . . . . ?
B12 B7 B11 C2 133.1(3) . . . . ?
B12 B7 B11 B6 99.1(3) . . . . ?
B12 B7 B11 B10 37.0(2) . . . . ?
B12 B8 B9 B4 -138.0(3) . . . . ?
B12 B8 B9 B5 -100.6(3) . . . . ?
B12 B8 B9 B10 -36.7(2) . . . . ?
B12 B9 B10 B5 -138.5(3) . . . . ?
B12 B9 B10 B6 -101.4(3) . . . . ?
B12 B9 B10 B11 -37.5(2) . . . . ?
B12 B10 B11 C2 -98.7(3) . . . . ?
B12 B10 B11 B6 -139.6(3) . . . . ?
B12 B10 B11 B7 -37.1(2) . . . . ?
C11 P1 C2 C1 118.1(2) . . . . ?
C11 P1 C2 B3 49.5(2) . . . . ?
C11 P1 C2 B6 -173.5(2) . . . . ?
C11 P1 C2 B7 -20.9(3) . . . . ?
C11 P1 C2 B11 -100.5(3) . . . . ?
C11 P1 C2' C1' -119.9(2) . . . . ?
C11 P1 C2' B3' 173.41(18) . . . . ?
C11 P1 C2' B6' -51.2(3) . . . . ?
C11 P1 C2' B7' 107.7(2) . . . . ?
C11 P1 C2' B11' 29.1(3) . . . . ?
C11 C12 C13 C14 -2.6(6) . . . . ?
C12 C11 C16 C15 -0.1(5) . . . . ?
C12 C13 C14 C15 1.3(6) . . . . ?
C13 C14 C15 C16 0.6(5) . . . . ?
C14 C15 C16 C11 -1.2(5) . . . . ?
C16 C11 C12 C13 2.0(5) . . . . ?
C1' C1 C2 P1 2.9(3) . . . . ?
C1' C1 C2 B3 109.3(3) . . . . ?
C1' C1 C2 B6 -107.7(3) . . . . ?
C1' C1 C2 B7 147.4(3) . . . . ?
C1' C1 C2 B11 -145.0(3) . . . . ?
C1' C1 B3 C2 -101.3(3) . . . . ?
C1' C1 B3 B4 118.9(3) . . . . ?
C1' C1 B3 B7 -136.7(3) . . . . ?
C1' C1 B3 B8 159.3(3) . . . . ?
C1' C1 B4 B3 -103.7(3) . . . . ?
C1' C1 B4 B5 115.9(3) . . . . ?
C1' C1 B4 B8 -142.1(3) . . . . ?
C1' C1 B4 B9 155.4(3) . . . . ?
C1' C1 B5 B4 -117.0(3) . . . . ?
C1' C1 B5 B6 102.1(3) . . . . ?
C1' C1 B5 B9 -156.8(3) . . . . ?
C1' C1 B5 B10 140.9(3) . . . . ?
C1' C1 B6 C2 102.6(3) . . . . ?
C1' C1 B6 B5 -118.8(3) . . . . ?
C1' C1 B6 B10 -159.1(3) . . . . ?
C1' C1 B6 B11 137.2(3) . . . . ?
C1' C2' B3' B4' 34.2(2) . . . . ?
C1' C2' B3' B7' 139.4(3) . . . . ?
C1' C2' B3' B8' 98.6(3) . . . . ?
C1' C2' B6' B5' -35.1(2) . . . . ?
C1' C2' B6' B10' -98.3(3) . . . . ?
C1' C2' B6' B11' -139.9(3) . . . . ?
C1' C2' B7' B3' -38.8(2) . . . . ?
C1' C2' B7' B8' -0.1(3) . . . . ?
C1' C2' B7' B11' 103.0(3) . . . . ?
C1' C2' B7' B12' 62.2(3) . . . . ?
C1' C2' B11' B6' 37.4(2) . . . . ?
C1' C2' B11' B7' -104.5(3) . . . . ?
C1' C2' B11' B10' -2.5(3) . . . . ?
C1' C2' B11' B12' -64.2(3) . . . . ?
C1' B3' B4' B5' 34.6(2) . . . . ?
C1' B3' B4' B8' 134.5(3) . . . . ?
C1' B3' B4' B9' 98.2(3) . . . . ?
C1' B3' B7' C2' 33.8(2) . . . . ?
C1' B3' B7' B8' -101.0(3) . . . . ?
C1' B3' B7' B11' -0.6(3) . . . . ?
C1' B3' B7' B12' -64.6(3) . . . . ?
C1' B3' B8' B4' -39.1(2) . . . . ?
C1' B3' B8' B7' 97.7(3) . . . . ?
C1' B3' B8' B9' -2.7(3) . . . . ?
C1' B3' B8' B12' 61.0(3) . . . . ?
C1' B4' B5' B6' 34.9(2) . . . . ?
C1' B4' B5' B9' 134.4(3) . . . . ?
C1' B4' B5' B10' 97.0(3) . . . . ?
C1' B4' B8' B3' 40.2(2) . . . . ?
C1' B4' B8' B7' 1.8(3) . . . . ?
C1' B4' B8' B9' -98.8(3) . . . . ?
C1' B4' B8' B12' -61.3(3) . . . . ?
C1' B4' B9' B5' -39.1(2) . . . . ?
C1' B4' B9' B8' 98.9(3) . . . . ?
C1' B4' B9' B10' -1.7(3) . . . . ?
C1' B4' B9' B12' 61.4(3) . . . . ?
C1' B5' B6' C2' 34.1(2) . . . . ?
C1' B5' B6' B10' 134.1(3) . . . . ?
C1' B5' B6' B11' 95.0(3) . . . . ?
C1' B5' B9' B4' 39.5(2) . . . . ?
C1' B5' B9' B8' 1.5(3) . . . . ?
C1' B5' B9' B10' -98.7(3) . . . . ?
C1' B5' B9' B12' -61.8(3) . . . . ?
C1' B5' B10' B6' -40.2(2) . . . . ?
C1' B5' B10' B9' 99.1(3) . . . . ?
C1' B5' B10' B11' -2.0(3) . . . . ?
C1' B5' B10' B12' 61.8(3) . . . . ?
C1' B6' B10' B5' 39.2(2) . . . . ?
C1' B6' B10' B9' 2.6(3) . . . . ?
C1' B6' B10' B11' -98.2(3) . . . . ?
C1' B6' B10' B12' -61.6(3) . . . . ?
C1' B6' B11' C2' -33.4(2) . . . . ?
C1' B6' B11' B7' 0.5(3) . . . . ?
C1' B6' B11' B10' 99.7(3) . . . . ?
C1' B6' B11' B12' 63.9(3) . . . . ?
C2' P1 C2 C1 2.9(2) . . . . ?
C2' P1 C2 B3 -65.7(2) . . . . ?
C2' P1 C2 B6 71.3(2) . . . . ?
C2' P1 C2 B7 -136.1(3) . . . . ?
C2' P1 C2 B11 144.3(3) . . . . ?
C2' P1 C11 C12 -158.8(2) . . . . ?
C2' P1 C11 C16 19.3(3) . . . . ?
C2' C1' B3' B4' -140.2(3) . . . . ?
C2' C1' B3' B7' -35.0(2) . . . . ?
C2' C1' B3' B8' -99.3(3) . . . . ?
C2' C1' B4' B3' 36.7(2) . . . . ?
C2' C1' B4' B5' -104.2(3) . . . . ?
C2' C1' B4' B8' -1.9(3) . . . . ?
C2' C1' B4' B9' -64.2(3) . . . . ?
C2' C1' B5' B4' 102.6(3) . . . . ?
C2' C1' B5' B6' -38.9(2) . . . . ?
C2' C1' B5' B9' 62.9(3) . . . . ?
C2' C1' B5' B10' 0.4(3) . . . . ?
C2' C1' B6' B5' 138.8(2) . . . . ?
C2' C1' B6' B10' 98.1(3) . . . . ?
C2' C1' B6' B11' 34.5(2) . . . . ?
C2' B3' B4' C1' -33.1(2) . . . . ?
C2' B3' B4' B5' 1.5(3) . . . . ?
C2' B3' B4' B8' 101.4(3) . . . . ?
C2' B3' B4' B9' 65.0(3) . . . . ?
C2' B3' B7' B8' -134.7(3) . . . . ?
C2' B3' B7' B11' -34.4(2) . . . . ?
C2' B3' B7' B12' -98.3(3) . . . . ?
C2' B3' B8' B4' -97.6(3) . . . . ?
C2' B3' B8' B7' 39.3(2) . . . . ?
C2' B3' B8' B9' -61.2(3) . . . . ?
C2' B3' B8' B12' 2.6(3) . . . . ?
C2' B6' B10' B5' 97.3(3) . . . . ?
C2' B6' B10' B9' 60.7(3) . . . . ?
C2' B6' B10' B11' -40.1(2) . . . . ?
C2' B6' B10' B12' -3.5(3) . . . . ?
C2' B6' B11' B7' 33.9(2) . . . . ?
C2' B6' B11' B10' 133.1(3) . . . . ?
C2' B6' B11' B12' 97.3(3) . . . . ?
C2' B7' B8' B3' -39.6(2) . . . . ?
C2' B7' B8' B4' -1.0(3) . . . . ?
C2' B7' B8' B9' 61.5(3) . . . . ?
C2' B7' B8' B12' 99.4(3) . . . . ?
C2' B7' B11' B6' -34.7(2) . . . . ?
C2' B7' B11' B10' -96.6(3) . . . . ?
C2' B7' B11' B12' -133.7(3) . . . . ?
C2' B7' B12' B8' -98.6(3) . . . . ?
C2' B7' B12' B9' -60.8(3) . . . . ?
C2' B7' B12' B10' 2.7(3) . . . . ?
C2' B7' B12' B11' 40.2(2) . . . . ?
C2' B11' B12' B7' -39.6(2) . . . . ?
C2' B11' B12' B8' -2.6(3) . . . . ?
C2' B11' B12' B9' 60.8(3) . . . . ?
C2' B11' B12' B10' 98.5(3) . . . . ?
B3' C1' C2' P1 -98.7(2) . . . . ?
B3' C1' C2' B6' 142.4(2) . . . . ?
B3' C1' C2' B7' 37.9(2) . . . . ?
B3' C1' C2' B11' 105.3(3) . . . . ?
B3' C1' B4' B5' -140.9(3) . . . . ?
B3' C1' B4' B8' -38.6(2) . . . . ?
B3' C1' B4' B9' -100.9(3) . . . . ?
B3' C1' B5' B4' 36.4(2) . . . . ?
B3' C1' B5' B6' -105.1(3) . . . . ?
B3' C1' B5' B9' -3.3(3) . . . . ?
B3' C1' B5' B10' -65.8(3) . . . . ?
B3' C1' B6' C2' -35.4(2) . . . . ?
B3' C1' B6' B5' 103.4(3) . . . . ?
B3' C1' B6' B10' 62.7(3) . . . . ?
B3' C1' B6' B11' -0.9(3) . . . . ?
B3' C2' B6' C1' 36.6(2) . . . . ?
B3' C2' B6' B5' 1.4(3) . . . . ?
B3' C2' B6' B10' -61.8(3) . . . . ?
B3' C2' B6' B11' -103.3(3) . . . . ?
B3' C2' B7' B8' 38.6(2) . . . . ?
B3' C2' B7' B11' 141.7(3) . . . . ?
B3' C2' B7' B12' 101.0(3) . . . . ?
B3' C2' B11' B6' 106.0(3) . . . . ?
B3' C2' B11' B7' -35.9(2) . . . . ?
B3' C2' B11' B10' 66.0(3) . . . . ?
B3' C2' B11' B12' 4.4(3) . . . . ?
B3' B4' B5' C1' -35.7(2) . . . . ?
B3' B4' B5' B6' -0.7(3) . . . . ?
B3' B4' B5' B9' 98.7(3) . . . . ?
B3' B4' B5' B10' 61.3(3) . . . . ?
B3' B4' B8' B7' -38.4(3) . . . . ?
B3' B4' B8' B9' -139.0(3) . . . . ?
B3' B4' B8' B12' -101.5(3) . . . . ?
B3' B4' B9' B5' -102.7(3) . . . . ?
B3' B4' B9' B8' 35.3(2) . . . . ?
B3' B4' B9' B10' -65.3(3) . . . . ?
B3' B4' B9' B12' -2.2(3) . . . . ?
B3' B7' B8' B4' 38.6(3) . . . . ?
B3' B7' B8' B9' 101.1(3) . . . . ?
B3' B7' B8' B12' 139.0(3) . . . . ?
B3' B7' B11' C2' 34.7(2) . . . . ?
B3' B7' B11' B6' 0.1(4) . . . . ?
B3' B7' B11' B10' -61.8(3) . . . . ?
B3' B7' B11' B12' -98.9(3) . . . . ?
B3' B7' B12' B8' -35.6(2) . . . . ?
B3' B7' B12' B9' 2.2(3) . . . . ?
B3' B7' B12' B10' 65.6(3) . . . . ?
B3' B7' B12' B11' 103.1(3) . . . . ?
B3' B8' B9' B4' -36.9(3) . . . . ?
B3' B8' B9' B5' 0.8(4) . . . . ?
B3' B8' B9' B10' 64.3(3) . . . . ?
B3' B8' B9' B12' 101.1(3) . . . . ?
B3' B8' B12' B7' 36.7(2) . . . . ?
B3' B8' B12' B9' -100.9(3) . . . . ?
B3' B8' B12' B10' -63.8(3) . . . . ?
B3' B8' B12' B11' 0.0(3) . . . . ?
B4' C1' C2' P1 -135.3(2) . . . . ?
B4' C1' C2' B3' -36.6(2) . . . . ?
B4' C1' C2' B6' 105.8(3) . . . . ?
B4' C1' C2' B7' 1.3(3) . . . . ?
B4' C1' C2' B11' 68.7(3) . . . . ?
B4' C1' B3' C2' 140.2(3) . . . . ?
B4' C1' B3' B7' 105.2(3) . . . . ?
B4' C1' B3' B8' 40.9(2) . . . . ?
B4' C1' B5' B6' -141.5(3) . . . . ?
B4' C1' B5' B9' -39.7(2) . . . . ?
B4' C1' B5' B10' -102.2(3) . . . . ?
B4' C1' B6' C2' -102.0(3) . . . . ?
B4' C1' B6' B5' 36.7(2) . . . . ?
B4' C1' B6' B10' -3.9(3) . . . . ?
B4' C1' B6' B11' -67.6(3) . . . . ?
B4' B3' B7' C2' 94.7(3) . . . . ?
B4' B3' B7' B8' -40.0(2) . . . . ?
B4' B3' B7' B11' 60.4(3) . . . . ?
B4' B3' B7' B12' -3.6(3) . . . . ?
B4' B3' B8' B7' 136.8(3) . . . . ?
B4' B3' B8' B9' 36.4(3) . . . . ?
B4' B3' B8' B12' 100.2(3) . . . . ?
B4' B5' B6' C1' -34.5(2) . . . . ?
B4' B5' B6' C2' -0.4(3) . . . . ?
B4' B5' B6' B10' 99.5(3) . . . . ?
B4' B5' B6' B11' 60.5(3) . . . . ?
B4' B5' B9' B8' -38.0(3) . . . . ?
B4' B5' B9' B10' -138.2(3) . . . . ?
B4' B5' B9' B12' -101.3(3) . . . . ?
B4' B5' B10' B6' -102.1(3) . . . . ?
B4' B5' B10' B9' 37.2(2) . . . . ?
B4' B5' B10' B11' -63.9(3) . . . . ?
B4' B5' B10' B12' -0.1(3) . . . . ?
B4' B8' B9' B5' 37.7(2) . . . . ?
B4' B8' B9' B10' 101.2(3) . . . . ?
B4' B8' B9' B12' 138.0(3) . . . . ?
B4' B8' B12' B7' 100.5(3) . . . . ?
B4' B8' B12' B9' -37.1(2) . . . . ?
B4' B8' B12' B10' 0.1(3) . . . . ?
B4' B8' B12' B11' 63.8(3) . . . . ?
B4' B9' B10' B5' -37.4(2) . . . . ?
B4' B9' B10' B6' -0.6(3) . . . . ?
B4' B9' B10' B11' 63.3(3) . . . . ?
B4' B9' B10' B12' 101.1(3) . . . . ?
B4' B9' B12' B7' 0.1(3) . . . . ?
B4' B9' B12' B8' 38.0(2) . . . . ?
B4' B9' B12' B10' -100.6(3) . . . . ?
B4' B9' B12' B11' -62.9(3) . . . . ?
B5' C1' C2' P1 157.47(19) . . . . ?
B5' C1' C2' B3' -103.9(3) . . . . ?
B5' C1' C2' B6' 38.6(2) . . . . ?
B5' C1' C2' B7' -65.9(3) . . . . ?
B5' C1' C2' B11' 1.4(3) . . . . ?
B5' C1' B3' C2' 103.2(3) . . . . ?
B5' C1' B3' B4' -37.0(3) . . . . ?
B5' C1' B3' B7' 68.2(3) . . . . ?
B5' C1' B3' B8' 3.9(3) . . . . ?
B5' C1' B4' B3' 140.9(3) . . . . ?
B5' C1' B4' B8' 102.3(3) . . . . ?
B5' C1' B4' B9' 40.0(2) . . . . ?
B5' C1' B6' C2' -138.8(2) . . . . ?
B5' C1' B6' B10' -40.6(2) . . . . ?
B5' C1' B6' B11' -104.3(3) . . . . ?
B5' B4' B8' B3' 101.4(3) . . . . ?
B5' B4' B8' B7' 62.9(3) . . . . ?
B5' B4' B8' B9' -37.7(2) . . . . ?
B5' B4' B8' B12' -0.1(3) . . . . ?
B5' B4' B9' B8' 138.0(3) . . . . ?
B5' B4' B9' B10' 37.4(2) . . . . ?
B5' B4' B9' B12' 100.5(3) . . . . ?
B5' B6' B10' B9' -36.6(2) . . . . ?
B5' B6' B10' B11' -137.4(3) . . . . ?
B5' B6' B10' B12' -100.7(3) . . . . ?
B5' B6' B11' C2' -94.2(3) . . . . ?
B5' B6' B11' B7' -60.3(3) . . . . ?
B5' B6' B11' B10' 38.9(3) . . . . ?
B5' B6' B11' B12' 3.2(3) . . . . ?
B5' B9' B10' B6' 36.8(2) . . . . ?
B5' B9' B10' B11' 100.7(3) . . . . ?
B5' B9' B10' B12' 138.5(3) . . . . ?
B5' B9' B12' B7' 63.6(3) . . . . ?
B5' B9' B12' B8' 101.5(3) . . . . ?
B5' B9' B12' B10' -37.1(2) . . . . ?
B5' B9' B12' B11' 0.7(4) . . . . ?
B5' B10' B11' C2' 2.7(3) . . . . ?
B5' B10' B11' B6' -38.3(2) . . . . ?
B5' B10' B11' B7' 63.9(3) . . . . ?
B5' B10' B11' B12' 101.2(3) . . . . ?
B5' B10' B12' B7' -63.7(3) . . . . ?
B5' B10' B12' B8' 0.0(3) . . . . ?
B5' B10' B12' B9' 37.1(2) . . . . ?
B5' B10' B12' B11' -100.8(3) . . . . ?
B6' C1' C2' P1 118.9(2) . . . . ?
B6' C1' C2' B3' -142.4(2) . . . . ?
B6' C1' C2' B7' -104.5(3) . . . . ?
B6' C1' C2' B11' -37.2(2) . . . . ?
B6' C1' B3' C2' 35.9(2) . . . . ?
B6' C1' B3' B4' -104.3(3) . . . . ?
B6' C1' B3' B7' 0.9(3) . . . . ?
B6' C1' B3' B8' -63.4(3) . . . . ?
B6' C1' B4' B3' 104.4(3) . . . . ?
B6' C1' B4' B5' -36.5(2) . . . . ?
B6' C1' B4' B8' 65.8(3) . . . . ?
B6' C1' B4' B9' 3.5(3) . . . . ?
B6' C1' B5' B4' 141.5(3) . . . . ?
B6' C1' B5' B9' 101.8(3) . . . . ?
B6' C1' B5' B10' 39.3(2) . . . . ?
B6' C2' B3' C1' -36.0(2) . . . . ?
B6' C2' B3' B4' -1.8(3) . . . . ?
B6' C2' B3' B7' 103.4(3) . . . . ?
B6' C2' B3' B8' 62.6(3) . . . . ?
B6' C2' B7' B3' -106.0(3) . . . . ?
B6' C2' B7' B8' -67.4(3) . . . . ?
B6' C2' B7' B11' 35.7(3) . . . . ?
B6' C2' B7' B12' -5.1(3) . . . . ?
B6' C2' B11' B7' -141.9(3) . . . . ?
B6' C2' B11' B10' -40.0(2) . . . . ?
B6' C2' B11' B12' -101.6(3) . . . . ?
B6' B5' B9' B4' 102.6(3) . . . . ?
B6' B5' B9' B8' 64.6(3) . . . . ?
B6' B5' B9' B10' -35.6(2) . . . . ?
B6' B5' B9' B12' 1.2(3) . . . . ?
B6' B5' B10' B9' 139.3(3) . . . . ?
B6' B5' B10' B11' 38.2(2) . . . . ?
B6' B5' B10' B12' 102.0(3) . . . . ?
B6' B10' B11' C2' 41.0(2) . . . . ?
B6' B10' B11' B7' 102.2(3) . . . . ?
B6' B10' B11' B12' 139.5(3) . . . . ?
B6' B10' B12' B7' 0.6(4) . . . . ?
B6' B10' B12' B8' 64.3(3) . . . . ?
B6' B10' B12' B9' 101.3(3) . . . . ?
B6' B10' B12' B11' -36.6(3) . . . . ?
B6' B11' B12' B7' -102.8(3) . . . . ?
B6' B11' B12' B8' -65.8(3) . . . . ?
B6' B11' B12' B9' -2.4(3) . . . . ?
B6' B11' B12' B10' 35.3(2) . . . . ?
B7' C2' B3' C1' -139.4(3) . . . . ?
B7' C2' B3' B4' -105.2(3) . . . . ?
B7' C2' B3' B8' -40.8(2) . . . . ?
B7' C2' B6' C1' 103.7(3) . . . . ?
B7' C2' B6' B5' 68.6(3) . . . . ?
B7' C2' B6' B10' 5.4(3) . . . . ?
B7' C2' B6' B11' -36.1(3) . . . . ?
B7' C2' B11' B6' 141.9(3) . . . . ?
B7' C2' B11' B10' 102.0(3) . . . . ?
B7' C2' B11' B12' 40.3(2) . . . . ?
B7' B3' B4' C1' -94.5(3) . . . . ?
B7' B3' B4' B5' -59.9(3) . . . . ?
B7' B3' B4' B8' 40.0(2) . . . . ?
B7' B3' B4' B9' 3.7(3) . . . . ?
B7' B3' B8' B4' -136.8(3) . . . . ?
B7' B3' B8' B9' -100.4(3) . . . . ?
B7' B3' B8' B12' -36.7(2) . . . . ?
B7' B8' B9' B4' -100.3(3) . . . . ?
B7' B8' B9' B5' -62.6(3) . . . . ?
B7' B8' B9' B10' 0.9(3) . . . . ?
B7' B8' B9' B12' 37.7(2) . . . . ?
B7' B8' B12' B9' -137.6(3) . . . . ?
B7' B8' B12' B10' -100.5(3) . . . . ?
B7' B8' B12' B11' -36.7(2) . . . . ?
B7' B11' B12' B8' 37.0(2) . . . . ?
B7' B11' B12' B9' 100.4(3) . . . . ?
B7' B11' B12' B10' 138.1(3) . . . . ?
B8' B3' B4' C1' -134.5(3) . . . . ?
B8' B3' B4' B5' -99.9(3) . . . . ?
B8' B3' B4' B9' -36.4(2) . . . . ?
B8' B3' B7' C2' 134.7(3) . . . . ?
B8' B3' B7' B11' 100.4(3) . . . . ?
B8' B3' B7' B12' 36.4(2) . . . . ?
B8' B4' B5' C1' -96.8(3) . . . . ?
B8' B4' B5' B6' -61.9(3) . . . . ?
B8' B4' B5' B9' 37.5(2) . . . . ?
B8' B4' B5' B10' 0.1(3) . . . . ?
B8' B4' B9' B5' -138.0(3) . . . . ?
B8' B4' B9' B10' -100.6(3) . . . . ?
B8' B4' B9' B12' -37.6(2) . . . . ?
B8' B7' B11' C2' 96.6(3) . . . . ?
B8' B7' B11' B6' 61.9(3) . . . . ?
B8' B7' B11' B10' 0.1(3) . . . . ?
B8' B7' B11' B12' -37.0(2) . . . . ?
B8' B7' B12' B9' 37.8(2) . . . . ?
B8' B7' B12' B10' 101.3(3) . . . . ?
B8' B7' B12' B11' 138.7(3) . . . . ?
B8' B9' B10' B5' -101.7(3) . . . . ?
B8' B9' B10' B6' -64.8(3) . . . . ?
B8' B9' B10' B11' -0.9(3) . . . . ?
B8' B9' B10' B12' 36.9(2) . . . . ?
B8' B9' B12' B7' -37.9(2) . . . . ?
B8' B9' B12' B10' -138.6(3) . . . . ?
B8' B9' B12' B11' -100.8(3) . . . . ?
B9' B4' B5' C1' -134.4(3) . . . . ?
B9' B4' B5' B6' -99.4(3) . . . . ?
B9' B4' B5' B10' -37.4(2) . . . . ?
B9' B4' B8' B3' 139.0(3) . . . . ?
B9' B4' B8' B7' 100.6(3) . . . . ?
B9' B4' B8' B12' 37.5(2) . . . . ?
B9' B5' B6' C1' -97.7(3) . . . . ?
B9' B5' B6' C2' -63.6(3) . . . . ?
B9' B5' B6' B10' 36.3(2) . . . . ?
B9' B5' B6' B11' -2.7(3) . . . . ?
B9' B5' B10' B6' -139.3(3) . . . . ?
B9' B5' B10' B11' -101.1(3) . . . . ?
B9' B5' B10' B12' -37.3(2) . . . . ?
B9' B8' B12' B7' 137.6(3) . . . . ?
B9' B8' B12' B10' 37.1(2) . . . . ?
B9' B8' B12' B11' 100.9(3) . . . . ?
B9' B10' B11' C2' -60.6(3) . . . . ?
B9' B10' B11' B6' -101.7(3) . . . . ?
B9' B10' B11' B7' 0.5(3) . . . . ?
B9' B10' B11' B12' 37.8(2) . . . . ?
B9' B10' B12' B7' -100.7(3) . . . . ?
B9' B10' B12' B8' -37.1(2) . . . . ?
B9' B10' B12' B11' -137.9(3) . . . . ?
B10' B5' B6' C1' -134.1(3) . . . . ?
B10' B5' B6' C2' -99.9(3) . . . . ?
B10' B5' B6' B11' -39.1(3) . . . . ?
B10' B5' B9' B4' 138.2(3) . . . . ?
B10' B5' B9' B8' 100.2(3) . . . . ?
B10' B5' B9' B12' 36.9(2) . . . . ?
B10' B6' B11' C2' -133.1(3) . . . . ?
B10' B6' B11' B7' -99.2(3) . . . . ?
B10' B6' B11' B12' -35.8(2) . . . . ?
B10' B9' B12' B7' 100.7(3) . . . . ?
B10' B9' B12' B8' 138.6(3) . . . . ?
B10' B9' B12' B11' 37.8(2) . . . . ?
B10' B11' B12' B7' -138.1(3) . . . . ?
B10' B11' B12' B8' -101.1(3) . . . . ?
B10' B11' B12' B9' -37.7(3) . . . . ?
B11' C2' B3' C1' -103.1(3) . . . . ?
B11' C2' B3' B4' -68.9(3) . . . . ?
B11' C2' B3' B7' 36.3(3) . . . . ?
B11' C2' B3' B8' -4.5(3) . . . . ?
B11' C2' B6' C1' 139.9(3) . . . . ?
B11' C2' B6' B5' 104.7(3) . . . . ?
B11' C2' B6' B10' 41.6(2) . . . . ?
B11' C2' B7' B3' -141.7(3) . . . . ?
B11' C2' B7' B8' -103.1(3) . . . . ?
B11' C2' B7' B12' -40.8(2) . . . . ?
B11' B6' B10' B5' 137.4(3) . . . . ?
B11' B6' B10' B9' 100.8(3) . . . . ?
B11' B6' B10' B12' 36.6(3) . . . . ?
B11' B7' B8' B3' -101.7(3) . . . . ?
B11' B7' B8' B4' -63.1(3) . . . . ?
B11' B7' B8' B9' -0.6(3) . . . . ?
B11' B7' B8' B12' 37.3(2) . . . . ?
B11' B7' B12' B8' -138.7(3) . . . . ?
B11' B7' B12' B9' -101.0(3) . . . . ?
B11' B7' B12' B10' -37.5(2) . . . . ?
B11' B10' B12' B7' 37.2(2) . . . . ?
B11' B10' B12' B8' 100.9(3) . . . . ?
B11' B10' B12' B9' 137.9(3) . . . . ?
B12' B7' B8' B3' -139.0(3) . . . . ?
B12' B7' B8' B4' -100.4(3) . . . . ?
B12' B7' B8' B9' -37.9(2) . . . . ?
B12' B7' B11' C2' 133.7(3) . . . . ?
B12' B7' B11' B6' 99.0(3) . . . . ?
B12' B7' B11' B10' 37.1(2) . . . . ?
B12' B8' B9' B4' -138.0(3) . . . . ?
B12' B8' B9' B5' -100.3(3) . . . . ?
B12' B8' B9' B10' -36.8(2) . . . . ?
B12' B9' B10' B5' -138.5(3) . . . . ?
B12' B9' B10' B6' -101.7(3) . . . . ?
B12' B9' B10' B11' -37.8(2) . . . . ?
B12' B10' B11' C2' -98.5(3) . . . . ?
B12' B10' B11' B6' -139.5(3) . . . . ?
B12' B10' B11' B7' -37.3(2) . . . . ?

_shelx_SHELXL_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_x85454
_database_code_depnum_ccdc_archive 'CCDC 1527032'
_audit_update_record             
;
2017-01-12 deposited with the CCDC.
2017-03-07 downloaded from the CCDC.
;
_audit_creation_date             2016-05-27
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C10 H25 B20 P Se'
_chemical_formula_sum            'C10 H25 B20 P Se'
_chemical_formula_weight         471.43
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   10.3457(12)
_cell_length_b                   16.9431(17)
_cell_length_c                   13.6941(14)
_cell_angle_alpha                90
_cell_angle_beta                 105.612(6)
_cell_angle_gamma                90
_cell_volume                     2311.9(4)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    5567
_cell_measurement_temperature    100.0
_cell_measurement_theta_max      25.69
_cell_measurement_theta_min      2.512
_shelx_estimated_absorpt_T_max   0.849
_shelx_estimated_absorpt_T_min   0.551
_exptl_absorpt_coefficient_mu    1.693
_exptl_absorpt_correction_T_max  0.7458
_exptl_absorpt_correction_T_min  0.6160
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.0871 before and 0.0626 after correction.
The Ratio of minimum to maximum transmission is 0.8260.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.354
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       PLATE
_exptl_crystal_F_000             936
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0740
_diffrn_reflns_av_unetI/netI     0.0551
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            43105
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         28.950
_diffrn_reflns_theta_min         1.957
_diffrn_ambient_temperature      100.0
_diffrn_detector_area_resol_mean 8
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'sealed tube'
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4732
_reflns_number_total             6088
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v7.68A (Bruker, 2009)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'XT (Sheldrick, 2015)'
_refine_diff_density_max         0.353
_refine_diff_density_min         -0.425
_refine_diff_density_rms         0.082
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     349
_refine_ls_number_reflns         6088
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0554
_refine_ls_R_factor_gt           0.0365
_refine_ls_restrained_S_all      1.034
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0353P)²+0.5045P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0767
_refine_ls_wR_factor_ref         0.0827
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C12(H12A), C13(H13), C14(H14), C15(H15), C16(H16)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.3789(2) 0.31654(11) 0.45277(15) 0.0110(4) Uani 1 1 d . . . . .
P1 P 0.26580(5) 0.15797(3) 0.43453(4) 0.00994(11) Uani 1 1 d . . . . .
Se1 Se 0.15683(2) 0.10917(2) 0.29777(2) 0.01658(7) Uani 1 1 d . . . . .
C2 C 0.23840(19) 0.26730(11) 0.44547(15) 0.0105(4) Uani 1 1 d . . . . .
B3 B 0.3185(2) 0.30935(13) 0.56199(18) 0.0125(5) Uani 1 1 d . . . . .
H3 H 0.365(2) 0.2726(12) 0.6209(16) 0.015 Uiso 1 1 d R . . . .
B4 B 0.3891(2) 0.39844(13) 0.52939(19) 0.0140(5) Uani 1 1 d . . . . .
H4 H 0.485(2) 0.4161(13) 0.5730(17) 0.017 Uiso 1 1 d R . . . .
B5 B 0.3453(3) 0.40696(13) 0.39400(19) 0.0156(5) Uani 1 1 d . . . . .
H5 H 0.420(2) 0.4297(13) 0.3556(17) 0.019 Uiso 1 1 d R . . . .
B6 B 0.2473(2) 0.32298(14) 0.34050(18) 0.0135(5) Uani 1 1 d . . . . .
H6 H 0.258(2) 0.2960(12) 0.2765(16) 0.016 Uiso 1 1 d R . . . .
B7 B 0.1418(2) 0.31237(13) 0.51486(18) 0.0132(5) Uani 1 1 d . . . . .
H7 H 0.081(2) 0.2734(12) 0.5483(16) 0.016 Uiso 1 1 d R . . . .
B8 B 0.2358(2) 0.39850(13) 0.5676(2) 0.0159(5) Uani 1 1 d . . . . .
H8 H 0.237(2) 0.4198(13) 0.6408(17) 0.019 Uiso 1 1 d R . . . .
B9 B 0.2509(3) 0.45920(14) 0.4646(2) 0.0188(5) Uani 1 1 d . . . . .
H9 H 0.261(2) 0.5216(14) 0.4692(17) 0.023 Uiso 1 1 d R . . . .
B10 B 0.1651(3) 0.41181(14) 0.3492(2) 0.0168(5) Uani 1 1 d . . . . .
H10 H 0.119(2) 0.4444(13) 0.2767(17) 0.020 Uiso 1 1 d R . . . .
B11 B 0.0983(2) 0.32056(14) 0.38014(18) 0.0139(5) Uani 1 1 d . . . . .
H11 H 0.015(2) 0.2881(12) 0.3317(16) 0.017 Uiso 1 1 d R . . . .
C11 C 0.2309(2) 0.11464(11) 0.54553(15) 0.0114(4) Uani 1 1 d . . . . .
B12 B 0.0977(3) 0.40605(14) 0.4556(2) 0.0167(5) Uani 1 1 d . . . . .
H12 H 0.004(2) 0.4339(13) 0.4567(16) 0.020 Uiso 1 1 d R . . . .
C12 C 0.0949(2) 0.09731(11) 0.53491(16) 0.0131(4) Uani 1 1 d . . . . .
H12A H 0.0299 0.1081 0.4728 0.016 Uiso 1 1 calc R . . . .
C13 C 0.0558(2) 0.06440(11) 0.61528(16) 0.0146(4) Uani 1 1 d . . . . .
H13 H -0.0363 0.0536 0.6084 0.017 Uiso 1 1 calc R . . . .
C14 C 0.1507(2) 0.04714(11) 0.70571(16) 0.0143(4) Uani 1 1 d . . . . .
H14 H 0.1234 0.0244 0.7604 0.017 Uiso 1 1 calc R . . . .
C15 C 0.2857(2) 0.06309(12) 0.71631(16) 0.0158(4) Uani 1 1 d . . . . .
H15 H 0.3504 0.0507 0.7781 0.019 Uiso 1 1 calc R . . . .
C16 C 0.3265(2) 0.09709(11) 0.63686(16) 0.0134(4) Uani 1 1 d . . . . .
H16 H 0.4187 0.1083 0.6445 0.016 Uiso 1 1 calc R . . . .
C1' C 0.49519(19) 0.26149(11) 0.44867(15) 0.0102(4) Uani 1 1 d . . . . .
C2' C 0.4524(2) 0.16702(11) 0.44796(15) 0.0108(4) Uani 1 1 d . . . . .
B3' B 0.4752(2) 0.20631(14) 0.33563(18) 0.0135(5) Uani 1 1 d . . . . .
H3' H 0.388(2) 0.2127(12) 0.2714(16) 0.016 Uiso 1 1 d R . . . .
B4' B 0.6062(2) 0.27651(15) 0.37668(19) 0.0165(5) Uani 1 1 d . . . . .
H4' H 0.598(2) 0.3304(13) 0.3346(17) 0.020 Uiso 1 1 d R . . . .
B5' B 0.6613(2) 0.27609(14) 0.51265(18) 0.0135(5) Uani 1 1 d . . . . .
H5' H 0.689(2) 0.3311(13) 0.5530(16) 0.016 Uiso 1 1 d R . . . .
B6' B 0.5642(2) 0.20555(13) 0.55798(18) 0.0116(5) Uani 1 1 d . . . . .
H6' H 0.529(2) 0.2136(12) 0.6214(16) 0.014 Uiso 1 1 d R . . . .
B7' B 0.5352(2) 0.11091(14) 0.37742(18) 0.0140(5) Uani 1 1 d . . . . .
H7' H 0.481(2) 0.0646(13) 0.3353(16) 0.017 Uiso 1 1 d R . . . .
B8' B 0.6371(3) 0.18021(15) 0.3329(2) 0.0171(5) Uani 1 1 d . . . . .
H8' H 0.654(2) 0.1730(13) 0.2603(18) 0.021 Uiso 1 1 d R . . . .
B9' B 0.7529(3) 0.22271(14) 0.44003(19) 0.0167(5) Uani 1 1 d . . . . .
H9' H 0.849(2) 0.2429(13) 0.4374(16) 0.020 Uiso 1 1 d R . . . .
B10' B 0.7247(2) 0.17895(14) 0.55103(19) 0.0139(5) Uani 1 1 d . . . . .
H10' H 0.802(2) 0.1721(12) 0.6197(17) 0.017 Uiso 1 1 d R . . . .
B11' B 0.5892(2) 0.10996(13) 0.51177(18) 0.0133(5) Uani 1 1 d . . . . .
H11' H 0.571(2) 0.0607(13) 0.5526(16) 0.016 Uiso 1 1 d R . . . .
B12' B 0.7092(2) 0.12032(14) 0.44055(19) 0.0151(5) Uani 1 1 d . . . . .
H12' H 0.776(2) 0.0692(13) 0.4368(16) 0.018 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.655(3) . ?
C1 B3 1.774(3) . ?
C1 B4 1.726(3) . ?
C1 B5 1.722(3) . ?
C1 B6 1.761(3) . ?
C1 C1' 1.536(3) . ?
P1 Se1 2.0798(6) . ?
P1 C2 1.8860(19) . ?
P1 C11 1.810(2) . ?
P1 C2' 1.896(2) . ?
C2 B3 1.740(3) . ?
C2 B6 1.743(3) . ?
C2 B7 1.731(3) . ?
C2 B11 1.737(3) . ?
B3 H3 1.03(2) . ?
B3 B4 1.785(3) . ?
B3 B7 1.767(3) . ?
B3 B8 1.747(3) . ?
B4 H4 1.05(2) . ?
B4 B5 1.792(4) . ?
B4 B8 1.798(4) . ?
B4 B9 1.791(3) . ?
B5 H5 1.11(2) . ?
B5 B6 1.786(3) . ?
B5 B9 1.784(4) . ?
B5 B10 1.800(4) . ?
B6 H6 1.02(2) . ?
B6 B10 1.748(3) . ?
B6 B11 1.767(4) . ?
B7 H7 1.09(2) . ?
B7 B8 1.794(3) . ?
B7 B11 1.783(3) . ?
B7 B12 1.785(3) . ?
B8 H8 1.06(2) . ?
B8 B9 1.785(4) . ?
B8 B12 1.797(4) . ?
B9 H9 1.06(2) . ?
B9 B10 1.782(4) . ?
B9 B12 1.798(4) . ?
B10 H10 1.12(2) . ?
B10 B11 1.790(3) . ?
B10 B12 1.780(4) . ?
B11 H11 1.09(2) . ?
B11 B12 1.780(3) . ?
C11 C12 1.406(3) . ?
C11 C16 1.402(3) . ?
B12 H12 1.09(2) . ?
C12 H12A 0.9500 . ?
C12 C13 1.388(3) . ?
C13 H13 0.9500 . ?
C13 C14 1.389(3) . ?
C14 H14 0.9500 . ?
C14 C15 1.391(3) . ?
C15 H15 0.9500 . ?
C15 C16 1.393(3) . ?
C16 H16 0.9500 . ?
C1' C2' 1.660(3) . ?
C1' B3' 1.772(3) . ?
C1' B4' 1.722(3) . ?
C1' B5' 1.724(3) . ?
C1' B6' 1.753(3) . ?
C2' B3' 1.749(3) . ?
C2' B6' 1.760(3) . ?
C2' B7' 1.736(3) . ?
C2' B11' 1.742(3) . ?
B3' H3' 1.08(2) . ?
B3' B4' 1.777(3) . ?
B3' B7' 1.771(3) . ?
B3' B8' 1.743(3) . ?
B4' H4' 1.07(2) . ?
B4' B5' 1.795(3) . ?
B4' B8' 1.796(4) . ?
B4' B9' 1.782(4) . ?
B5' H5' 1.08(2) . ?
B5' B6' 1.777(3) . ?
B5' B9' 1.792(3) . ?
B5' B10' 1.797(3) . ?
B6' H6' 1.03(2) . ?
B6' B10' 1.747(3) . ?
B6' B11' 1.783(3) . ?
B7' H7' 1.04(2) . ?
B7' B8' 1.791(4) . ?
B7' B11' 1.773(3) . ?
B7' B12' 1.782(3) . ?
B8' H8' 1.06(2) . ?
B8' B9' 1.778(4) . ?
B8' B12' 1.780(4) . ?
B9' H9' 1.06(2) . ?
B9' B10' 1.785(4) . ?
B9' B12' 1.793(3) . ?
B10' H10' 1.06(2) . ?
B10' B11' 1.792(3) . ?
B10' B12' 1.781(3) . ?
B11' H11' 1.05(2) . ?
B11' B12' 1.781(3) . ?
B12' H12' 1.12(2) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 B3 60.88(12) . . ?
C2 C1 B4 110.57(16) . . ?
C2 C1 B5 110.91(15) . . ?
C2 C1 B6 61.25(12) . . ?
B4 C1 B3 61.34(13) . . ?
B4 C1 B6 112.81(15) . . ?
B5 C1 B3 112.51(16) . . ?
B5 C1 B4 62.64(13) . . ?
B5 C1 B6 61.68(13) . . ?
B6 C1 B3 112.06(16) . . ?
C1' C1 C2 112.06(15) . . ?
C1' C1 B3 116.53(15) . . ?
C1' C1 B4 126.17(16) . . ?
C1' C1 B5 125.79(17) . . ?
C1' C1 B6 115.77(16) . . ?
C2 P1 Se1 113.91(6) . . ?
C2 P1 C2' 94.81(8) . . ?
C11 P1 Se1 114.38(7) . . ?
C11 P1 C2 105.28(9) . . ?
C11 P1 C2' 112.30(9) . . ?
C2' P1 Se1 114.24(6) . . ?
C1 C2 P1 110.59(13) . . ?
C1 C2 B3 62.93(12) . . ?
C1 C2 B6 62.38(12) . . ?
C1 C2 B7 111.82(15) . . ?
C1 C2 B11 111.50(15) . . ?
B3 C2 P1 115.49(13) . . ?
B3 C2 B6 114.65(15) . . ?
B6 C2 P1 115.07(13) . . ?
B7 C2 P1 126.75(13) . . ?
B7 C2 B3 61.22(13) . . ?
B7 C2 B6 112.37(15) . . ?
B7 C2 B11 61.87(13) . . ?
B11 C2 P1 126.28(13) . . ?
B11 C2 B3 112.63(15) . . ?
B11 C2 B6 61.05(13) . . ?
C1 B3 H3 120.3(12) . . ?
C1 B3 B4 58.00(12) . . ?
C2 B3 C1 56.19(11) . . ?
C2 B3 H3 118.5(12) . . ?
C2 B3 B4 104.05(16) . . ?
C2 B3 B7 59.13(13) . . ?
C2 B3 B8 106.05(16) . . ?
B4 B3 H3 124.8(12) . . ?
B7 B3 C1 104.74(16) . . ?
B7 B3 H3 121.5(12) . . ?
B7 B3 B4 109.69(16) . . ?
B8 B3 C1 105.37(16) . . ?
B8 B3 H3 128.3(12) . . ?
B8 B3 B4 61.19(14) . . ?
B8 B3 B7 61.39(13) . . ?
C1 B4 B3 60.65(12) . . ?
C1 B4 H4 117.9(12) . . ?
C1 B4 B5 58.58(12) . . ?
C1 B4 B8 105.22(16) . . ?
C1 B4 B9 104.52(16) . . ?
B3 B4 H4 119.0(12) . . ?
B3 B4 B5 108.67(16) . . ?
B3 B4 B8 58.36(13) . . ?
B3 B4 B9 106.47(17) . . ?
B5 B4 H4 120.1(12) . . ?
B5 B4 B8 107.66(17) . . ?
B8 B4 H4 127.1(12) . . ?
B9 B4 H4 128.4(12) . . ?
B9 B4 B5 59.70(14) . . ?
B9 B4 B8 59.65(14) . . ?
C1 B5 B4 58.78(12) . . ?
C1 B5 H5 116.8(11) . . ?
C1 B5 B6 60.24(12) . . ?
C1 B5 B9 105.01(17) . . ?
C1 B5 B10 105.07(16) . . ?
B4 B5 H5 120.1(11) . . ?
B4 B5 B10 107.86(18) . . ?
B6 B5 B4 108.53(16) . . ?
B6 B5 H5 118.1(11) . . ?
B6 B5 B10 58.35(13) . . ?
B9 B5 B4 60.13(14) . . ?
B9 B5 H5 129.4(11) . . ?
B9 B5 B6 106.54(18) . . ?
B9 B5 B10 59.63(14) . . ?
B10 B5 H5 127.5(11) . . ?
C1 B6 B5 58.08(12) . . ?
C1 B6 H6 118.9(12) . . ?
C1 B6 B11 105.27(16) . . ?
C2 B6 C1 56.38(11) . . ?
C2 B6 B5 104.07(16) . . ?
C2 B6 H6 120.5(12) . . ?
C2 B6 B10 105.97(17) . . ?
C2 B6 B11 59.32(13) . . ?
B5 B6 H6 121.9(12) . . ?
B10 B6 C1 105.64(16) . . ?
B10 B6 B5 61.24(14) . . ?
B10 B6 H6 127.7(12) . . ?
B10 B6 B11 61.23(14) . . ?
B11 B6 B5 109.77(18) . . ?
B11 B6 H6 124.0(12) . . ?
C2 B7 B3 59.65(12) . . ?
C2 B7 H7 116.4(11) . . ?
C2 B7 B8 104.43(16) . . ?
C2 B7 B11 59.24(13) . . ?
C2 B7 B12 104.92(16) . . ?
B3 B7 H7 118.9(11) . . ?
B3 B7 B8 58.75(13) . . ?
B3 B7 B11 109.18(17) . . ?
B3 B7 B12 107.73(17) . . ?
B8 B7 H7 129.3(11) . . ?
B11 B7 H7 117.9(11) . . ?
B11 B7 B8 108.16(17) . . ?
B11 B7 B12 59.86(13) . . ?
B12 B7 H7 128.5(11) . . ?
B12 B7 B8 60.28(13) . . ?
B3 B8 B4 60.45(13) . . ?
B3 B8 B7 59.86(13) . . ?
B3 B8 H8 117.1(12) . . ?
B3 B8 B9 108.40(18) . . ?
B3 B8 B12 108.07(17) . . ?
B4 B8 H8 119.3(12) . . ?
B7 B8 B4 107.91(17) . . ?
B7 B8 H8 121.5(12) . . ?
B7 B8 B12 59.61(13) . . ?
B9 B8 B4 59.97(14) . . ?
B9 B8 B7 107.69(17) . . ?
B9 B8 H8 124.6(12) . . ?
B9 B8 B12 60.24(14) . . ?
B12 B8 B4 108.23(18) . . ?
B12 B8 H8 125.6(12) . . ?
B4 B9 H9 119.5(12) . . ?
B4 B9 B12 108.53(17) . . ?
B5 B9 B4 60.17(14) . . ?
B5 B9 B8 108.62(16) . . ?
B5 B9 H9 117.9(13) . . ?
B5 B9 B12 108.39(17) . . ?
B8 B9 B4 60.37(14) . . ?
B8 B9 H9 123.7(12) . . ?
B8 B9 B12 60.21(14) . . ?
B10 B9 B4 108.71(17) . . ?
B10 B9 B5 60.66(14) . . ?
B10 B9 B8 108.21(17) . . ?
B10 B9 H9 121.2(12) . . ?
B10 B9 B12 59.62(14) . . ?
B12 B9 H9 124.8(12) . . ?
B5 B10 H10 118.7(12) . . ?
B6 B10 B5 60.40(13) . . ?
B6 B10 B9 108.25(17) . . ?
B6 B10 H10 117.6(11) . . ?
B6 B10 B11 59.91(13) . . ?
B6 B10 B12 108.28(17) . . ?
B9 B10 B5 59.72(14) . . ?
B9 B10 H10 123.6(11) . . ?
B9 B10 B11 108.11(17) . . ?
B11 B10 B5 108.08(16) . . ?
B11 B10 H10 122.2(11) . . ?
B12 B10 B5 108.45(18) . . ?
B12 B10 B9 60.64(14) . . ?
B12 B10 H10 125.6(12) . . ?
B12 B10 B11 59.83(14) . . ?
C2 B11 B6 59.62(13) . . ?
C2 B11 B7 58.89(12) . . ?
C2 B11 B10 104.39(16) . . ?
C2 B11 H11 117.9(11) . . ?
C2 B11 B12 104.86(16) . . ?
B6 B11 B7 108.75(17) . . ?
B6 B11 B10 58.86(14) . . ?
B6 B11 H11 116.1(12) . . ?
B6 B11 B12 107.40(17) . . ?
B7 B11 B10 107.82(17) . . ?
B7 B11 H11 122.0(11) . . ?
B10 B11 H11 125.9(11) . . ?
B12 B11 B7 60.13(13) . . ?
B12 B11 B10 59.79(14) . . ?
B12 B11 H11 129.8(12) . . ?
C12 C11 P1 114.72(15) . . ?
C16 C11 P1 125.66(16) . . ?
C16 C11 C12 119.62(19) . . ?
B7 B12 B8 60.11(13) . . ?
B7 B12 B9 107.53(17) . . ?
B7 B12 H12 120.0(12) . . ?
B8 B12 B9 59.55(14) . . ?
B8 B12 H12 121.9(12) . . ?
B9 B12 H12 124.0(12) . . ?
B10 B12 B7 108.20(17) . . ?
B10 B12 B8 107.79(18) . . ?
B10 B12 B9 59.75(14) . . ?
B10 B12 B11 60.39(14) . . ?
B10 B12 H12 122.6(12) . . ?
B11 B12 B7 60.00(13) . . ?
B11 B12 B8 108.13(16) . . ?
B11 B12 B9 107.85(18) . . ?
B11 B12 H12 120.3(12) . . ?
C11 C12 H12A 120.0 . . ?
C13 C12 C11 119.95(19) . . ?
C13 C12 H12A 120.0 . . ?
C12 C13 H13 119.8 . . ?
C12 C13 C14 120.33(19) . . ?
C14 C13 H13 119.8 . . ?
C13 C14 H14 120.0 . . ?
C13 C14 C15 120.06(19) . . ?
C15 C14 H14 120.0 . . ?
C14 C15 H15 119.8 . . ?
C14 C15 C16 120.38(19) . . ?
C16 C15 H15 119.8 . . ?
C11 C16 H16 120.2 . . ?
C15 C16 C11 119.65(19) . . ?
C15 C16 H16 120.2 . . ?
C1 C1' C2' 112.07(15) . . ?
C1 C1' B3' 116.35(15) . . ?
C1 C1' B4' 125.54(16) . . ?
C1 C1' B5' 125.32(16) . . ?
C1 C1' B6' 116.13(16) . . ?
C2' C1' B3' 61.18(12) . . ?
C2' C1' B4' 110.91(15) . . ?
C2' C1' B5' 111.65(15) . . ?
C2' C1' B6' 62.00(12) . . ?
B4' C1' B3' 61.12(13) . . ?
B4' C1' B5' 62.77(14) . . ?
B4' C1' B6' 112.79(16) . . ?
B5' C1' B3' 112.69(15) . . ?
B5' C1' B6' 61.46(13) . . ?
B6' C1' B3' 112.69(15) . . ?
C1' C2' P1 109.96(12) . . ?
C1' C2' B3' 62.58(12) . . ?
C1' C2' B6' 61.61(12) . . ?
C1' C2' B7' 111.14(15) . . ?
C1' C2' B11' 110.67(15) . . ?
B3' C2' P1 108.66(13) . . ?
B3' C2' B6' 113.51(15) . . ?
B6' C2' P1 122.05(14) . . ?
B7' C2' P1 122.93(13) . . ?
B7' C2' B3' 61.06(13) . . ?
B7' C2' B6' 111.75(15) . . ?
B7' C2' B11' 61.29(13) . . ?
B11' C2' P1 132.25(14) . . ?
B11' C2' B3' 111.65(16) . . ?
B11' C2' B6' 61.21(12) . . ?
C1' B3' H3' 122.2(11) . . ?
C1' B3' B4' 58.05(13) . . ?
C2' B3' C1' 56.25(11) . . ?
C2' B3' H3' 118.2(12) . . ?
C2' B3' B4' 104.37(16) . . ?
C2' B3' B7' 59.11(13) . . ?
B4' B3' H3' 126.1(11) . . ?
B7' B3' C1' 104.53(16) . . ?
B7' B3' H3' 119.8(11) . . ?
B7' B3' B4' 109.71(17) . . ?
B8' B3' C1' 105.41(16) . . ?
B8' B3' C2' 106.26(16) . . ?
B8' B3' H3' 127.1(12) . . ?
B8' B3' B4' 61.36(14) . . ?
B8' B3' B7' 61.30(14) . . ?
C1' B4' B3' 60.83(13) . . ?
C1' B4' H4' 117.8(12) . . ?
C1' B4' B5' 58.67(13) . . ?
C1' B4' B8' 105.25(16) . . ?
C1' B4' B9' 104.92(17) . . ?
B3' B4' H4' 117.2(12) . . ?
B3' B4' B5' 109.14(16) . . ?
B3' B4' B8' 58.38(13) . . ?
B3' B4' B9' 106.79(17) . . ?
B5' B4' H4' 121.2(12) . . ?
B5' B4' B8' 107.91(17) . . ?
B8' B4' H4' 126.1(12) . . ?
B9' B4' H4' 129.1(12) . . ?
B9' B4' B5' 60.13(14) . . ?
B9' B4' B8' 59.57(14) . . ?
C1' B5' B4' 58.56(13) . . ?
C1' B5' H5' 118.3(12) . . ?
C1' B5' B6' 60.07(12) . . ?
C1' B5' B9' 104.42(16) . . ?
C1' B5' B10' 104.62(15) . . ?
B4' B5' H5' 119.5(11) . . ?
B4' B5' B10' 107.22(16) . . ?
B6' B5' B4' 108.27(16) . . ?
B6' B5' H5' 119.8(12) . . ?
B6' B5' B9' 106.70(16) . . ?
B6' B5' B10' 58.52(13) . . ?
B9' B5' B4' 59.60(14) . . ?
B9' B5' H5' 127.7(12) . . ?
B9' B5' B10' 59.63(13) . . ?
B10' B5' H5' 127.9(11) . . ?
C1' B6' C2' 56.40(11) . . ?
C1' B6' B5' 58.46(12) . . ?
C1' B6' H6' 119.4(12) . . ?
C1' B6' B11' 104.64(16) . . ?
C2' B6' B5' 104.68(16) . . ?
C2' B6' H6' 118.1(12) . . ?
C2' B6' B11' 58.91(12) . . ?
B5' B6' H6' 124.1(12) . . ?
B5' B6' B11' 109.71(17) . . ?
B10' B6' C1' 105.53(16) . . ?
B10' B6' C2' 105.83(16) . . ?
B10' B6' B5' 61.31(14) . . ?
B10' B6' H6' 129.0(12) . . ?
B10' B6' B11' 61.02(13) . . ?
B11' B6' H6' 122.3(11) . . ?
C2' B7' B3' 59.83(12) . . ?
C2' B7' H7' 116.7(12) . . ?
C2' B7' B8' 104.72(16) . . ?
C2' B7' B11' 59.52(12) . . ?
C2' B7' B12' 105.43(16) . . ?
B3' B7' H7' 114.8(12) . . ?
B3' B7' B8' 58.59(13) . . ?
B3' B7' B11' 109.20(16) . . ?
B3' B7' B12' 107.20(16) . . ?
B8' B7' H7' 125.5(12) . . ?
B11' B7' H7' 122.7(12) . . ?
B11' B7' B8' 108.01(17) . . ?
B11' B7' B12' 60.14(14) . . ?
B12' B7' H7' 131.0(12) . . ?
B12' B7' B8' 59.76(14) . . ?
B3' B8' B4' 60.26(14) . . ?
B3' B8' B7' 60.11(13) . . ?
B3' B8' H8' 116.6(12) . . ?
B3' B8' B9' 108.50(18) . . ?
B3' B8' B12' 108.51(17) . . ?
B4' B8' H8' 120.4(12) . . ?
B7' B8' B4' 107.92(17) . . ?
B7' B8' H8' 120.1(12) . . ?
B9' B8' B4' 59.82(14) . . ?
B9' B8' B7' 108.17(18) . . ?
B9' B8' H8' 125.3(12) . . ?
B9' B8' B12' 60.53(14) . . ?
B12' B8' B4' 108.27(17) . . ?
B12' B8' B7' 59.86(14) . . ?
B12' B8' H8' 125.0(12) . . ?
B4' B9' B5' 60.28(14) . . ?
B4' B9' H9' 120.0(12) . . ?
B4' B9' B10' 108.31(17) . . ?
B4' B9' B12' 108.31(17) . . ?
B5' B9' H9' 119.7(12) . . ?
B5' B9' B12' 108.33(17) . . ?
B8' B9' B4' 60.60(14) . . ?
B8' B9' B5' 108.86(17) . . ?
B8' B9' H9' 122.1(12) . . ?
B8' B9' B10' 107.85(17) . . ?
B8' B9' B12' 59.80(14) . . ?
B10' B9' B5' 60.32(13) . . ?
B10' B9' H9' 122.2(12) . . ?
B10' B9' B12' 59.70(14) . . ?
B12' B9' H9' 123.6(12) . . ?
B5' B10' H10' 119.1(11) . . ?
B6' B10' B5' 60.17(13) . . ?
B6' B10' B9' 108.35(17) . . ?
B6' B10' H10' 118.7(12) . . ?
B6' B10' B11' 60.48(13) . . ?
B6' B10' B12' 108.71(17) . . ?
B9' B10' B5' 60.04(13) . . ?
B9' B10' H10' 122.7(12) . . ?
B9' B10' B11' 108.02(17) . . ?
B11' B10' B5' 108.39(16) . . ?
B11' B10' H10' 122.4(12) . . ?
B12' B10' B5' 108.67(17) . . ?
B12' B10' B9' 60.39(14) . . ?
B12' B10' H10' 124.4(12) . . ?
B12' B10' B11' 59.81(13) . . ?
C2' B11' B6' 59.88(12) . . ?
C2' B11' B7' 59.19(13) . . ?
C2' B11' B10' 104.63(15) . . ?
C2' B11' H11' 118.0(12) . . ?
C2' B11' B12' 105.20(16) . . ?
B6' B11' B10' 58.50(13) . . ?
B6' B11' H11' 117.9(12) . . ?
B7' B11' B6' 108.95(16) . . ?
B7' B11' B10' 107.94(17) . . ?
B7' B11' H11' 120.5(12) . . ?
B7' B11' B12' 60.17(14) . . ?
B10' B11' H11' 126.7(12) . . ?
B12' B11' B6' 107.08(16) . . ?
B12' B11' B10' 59.77(13) . . ?
B12' B11' H11' 128.5(12) . . ?
B7' B12' B9' 107.91(17) . . ?
B7' B12' H12' 117.7(11) . . ?
B8' B12' B7' 60.38(14) . . ?
B8' B12' B9' 59.67(14) . . ?
B8' B12' B10' 107.92(17) . . ?
B8' B12' B11' 108.15(17) . . ?
B8' B12' H12' 122.0(11) . . ?
B9' B12' H12' 126.1(12) . . ?
B10' B12' B7' 108.07(17) . . ?
B10' B12' B9' 59.91(14) . . ?
B10' B12' B11' 60.42(13) . . ?
B10' B12' H12' 123.8(11) . . ?
B11' B12' B7' 59.68(13) . . ?
B11' B12' B9' 108.12(17) . . ?
B11' B12' H12' 118.6(12) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 C2 B3 B4 34.43(14) . . . . ?
C1 C2 B3 B7 139.20(16) . . . . ?
C1 C2 B3 B8 98.01(17) . . . . ?
C1 C2 B6 B5 -34.79(14) . . . . ?
C1 C2 B6 B10 -98.42(17) . . . . ?
C1 C2 B6 B11 -139.66(16) . . . . ?
C1 C2 B7 B3 -38.80(15) . . . . ?
C1 C2 B7 B8 0.7(2) . . . . ?
C1 C2 B7 B11 103.52(17) . . . . ?
C1 C2 B7 B12 63.27(19) . . . . ?
C1 C2 B11 B6 38.06(16) . . . . ?
C1 C2 B11 B7 -104.03(17) . . . . ?
C1 C2 B11 B10 -1.7(2) . . . . ?
C1 C2 B11 B12 -63.7(2) . . . . ?
C1 B3 B4 B5 34.78(15) . . . . ?
C1 B3 B4 B8 134.45(17) . . . . ?
C1 B3 B4 B9 97.69(17) . . . . ?
C1 B3 B7 C2 34.15(13) . . . . ?
C1 B3 B7 B8 -99.71(17) . . . . ?
C1 B3 B7 B11 0.36(19) . . . . ?
C1 B3 B7 B12 -63.10(19) . . . . ?
C1 B3 B8 B4 -38.90(15) . . . . ?
C1 B3 B8 B7 98.66(17) . . . . ?
C1 B3 B8 B9 -1.5(2) . . . . ?
C1 B3 B8 B12 62.3(2) . . . . ?
C1 B4 B5 B6 35.38(15) . . . . ?
C1 B4 B5 B9 134.22(17) . . . . ?
C1 B4 B5 B10 97.13(17) . . . . ?
C1 B4 B8 B3 40.16(15) . . . . ?
C1 B4 B8 B7 2.3(2) . . . . ?
C1 B4 B8 B9 -98.16(17) . . . . ?
C1 B4 B8 B12 -60.71(19) . . . . ?
C1 B4 B9 B5 -39.18(15) . . . . ?
C1 B4 B9 B8 99.36(17) . . . . ?
C1 B4 B9 B10 -1.4(2) . . . . ?
C1 B4 B9 B12 61.9(2) . . . . ?
C1 B5 B6 C2 34.04(14) . . . . ?
C1 B5 B6 B10 134.76(18) . . . . ?
C1 B5 B6 B11 96.08(18) . . . . ?
C1 B5 B9 B4 39.39(15) . . . . ?
C1 B5 B9 B8 2.0(2) . . . . ?
C1 B5 B9 B10 -98.90(17) . . . . ?
C1 B5 B9 B12 -61.9(2) . . . . ?
C1 B5 B10 B6 -39.67(16) . . . . ?
C1 B5 B10 B9 98.81(18) . . . . ?
C1 B5 B10 B11 -2.0(2) . . . . ?
C1 B5 B10 B12 61.3(2) . . . . ?
C1 B6 B10 B5 38.75(15) . . . . ?
C1 B6 B10 B9 1.7(2) . . . . ?
C1 B6 B10 B11 -99.11(17) . . . . ?
C1 B6 B10 B12 -62.5(2) . . . . ?
C1 B6 B11 C2 -33.97(14) . . . . ?
C1 B6 B11 B7 -0.2(2) . . . . ?
C1 B6 B11 B10 99.72(17) . . . . ?
C1 B6 B11 B12 63.37(19) . . . . ?
C1 C1' C2' P1 7.63(19) . . . . ?
C1 C1' C2' B3' 108.88(17) . . . . ?
C1 C1' C2' B6' -108.82(18) . . . . ?
C1 C1' C2' B7' 147.13(16) . . . . ?
C1 C1' C2' B11' -146.73(16) . . . . ?
C1 C1' B3' C2' -101.89(18) . . . . ?
C1 C1' B3' B4' 117.88(19) . . . . ?
C1 C1' B3' B7' -137.70(17) . . . . ?
C1 C1' B3' B8' 158.60(17) . . . . ?
C1 C1' B4' B3' -103.2(2) . . . . ?
C1 C1' B4' B5' 115.6(2) . . . . ?
C1 C1' B4' B8' -142.47(18) . . . . ?
C1 C1' B4' B9' 155.60(18) . . . . ?
C1 C1' B5' B4' -115.9(2) . . . . ?
C1 C1' B5' B6' 103.2(2) . . . . ?
C1 C1' B5' B9' -155.56(18) . . . . ?
C1 C1' B5' B10' 142.63(18) . . . . ?
C1 C1' B6' C2' 102.31(17) . . . . ?
C1 C1' B6' B5' -117.80(18) . . . . ?
C1 C1' B6' B10' -158.76(16) . . . . ?
C1 C1' B6' B11' 137.80(17) . . . . ?
P1 C2 B3 C1 101.17(15) . . . . ?
P1 C2 B3 B4 135.60(14) . . . . ?
P1 C2 B3 B7 -119.62(16) . . . . ?
P1 C2 B3 B8 -160.82(14) . . . . ?
P1 C2 B6 C1 -101.15(15) . . . . ?
P1 C2 B6 B5 -135.93(14) . . . . ?
P1 C2 B6 B10 160.43(14) . . . . ?
P1 C2 B6 B11 119.19(15) . . . . ?
P1 C2 B7 B3 101.69(17) . . . . ?
P1 C2 B7 B8 141.22(15) . . . . ?
P1 C2 B7 B11 -115.99(18) . . . . ?
P1 C2 B7 B12 -156.24(14) . . . . ?
P1 C2 B11 B6 -101.23(18) . . . . ?
P1 C2 B11 B7 116.69(18) . . . . ?
P1 C2 B11 B10 -140.94(16) . . . . ?
P1 C2 B11 B12 157.05(15) . . . . ?
P1 C11 C12 C13 -179.56(15) . . . . ?
P1 C11 C16 C15 -179.51(15) . . . . ?
P1 C2' B3' C1' 103.34(13) . . . . ?
P1 C2' B3' B4' 137.42(14) . . . . ?
P1 C2' B3' B7' -117.96(14) . . . . ?
P1 C2' B3' B8' -158.73(13) . . . . ?
P1 C2' B6' C1' -96.85(15) . . . . ?
P1 C2' B6' B5' -131.44(15) . . . . ?
P1 C2' B6' B10' 164.77(13) . . . . ?
P1 C2' B6' B11' 124.14(17) . . . . ?
P1 C2' B7' B3' 94.44(16) . . . . ?
P1 C2' B7' B8' 133.54(15) . . . . ?
P1 C2' B7' B11' -123.97(17) . . . . ?
P1 C2' B7' B12' -164.35(14) . . . . ?
P1 C2' B11' B6' -108.59(19) . . . . ?
P1 C2' B11' B7' 109.86(19) . . . . ?
P1 C2' B11' B10' -147.72(16) . . . . ?
P1 C2' B11' B12' 150.21(16) . . . . ?
Se1 P1 C2 C1 -115.36(11) . . . . ?
Se1 P1 C2 B3 175.71(12) . . . . ?
Se1 P1 C2 B6 -47.14(15) . . . . ?
Se1 P1 C2 B7 103.75(15) . . . . ?
Se1 P1 C2 B11 24.22(18) . . . . ?
Se1 P1 C11 C12 -40.03(16) . . . . ?
Se1 P1 C11 C16 139.14(15) . . . . ?
Se1 P1 C2' C1' 112.46(12) . . . . ?
Se1 P1 C2' B3' 45.70(13) . . . . ?
Se1 P1 C2' B6' -179.23(12) . . . . ?
Se1 P1 C2' B7' -21.35(17) . . . . ?
Se1 P1 C2' B11' -100.70(18) . . . . ?
C2 C1 B3 B4 -139.71(16) . . . . ?
C2 C1 B3 B7 -35.44(14) . . . . ?
C2 C1 B3 B8 -99.26(17) . . . . ?
C2 C1 B4 B3 37.12(15) . . . . ?
C2 C1 B4 B5 -103.60(17) . . . . ?
C2 C1 B4 B8 -1.9(2) . . . . ?
C2 C1 B4 B9 -63.86(19) . . . . ?
C2 C1 B5 B4 103.05(17) . . . . ?
C2 C1 B5 B6 -37.73(16) . . . . ?
C2 C1 B5 B9 63.0(2) . . . . ?
C2 C1 B5 B10 1.0(2) . . . . ?
C2 C1 B6 B5 139.31(17) . . . . ?
C2 C1 B6 B10 99.03(18) . . . . ?
C2 C1 B6 B11 35.25(14) . . . . ?
C2 C1 C1' C2' -4.9(2) . . . . ?
C2 C1 C1' B3' 62.8(2) . . . . ?
C2 C1 C1' B4' 134.83(18) . . . . ?
C2 C1 C1' B5' -145.72(17) . . . . ?
C2 C1 C1' B6' -73.45(19) . . . . ?
C2 P1 C11 C12 85.79(15) . . . . ?
C2 P1 C11 C16 -95.04(18) . . . . ?
C2 P1 C2' C1' -6.48(14) . . . . ?
C2 P1 C2' B3' -73.25(13) . . . . ?
C2 P1 C2' B6' 61.83(15) . . . . ?
C2 P1 C2' B7' -140.30(15) . . . . ?
C2 P1 C2' B11' 140.35(18) . . . . ?
C2 B3 B4 C1 -33.64(14) . . . . ?
C2 B3 B4 B5 1.1(2) . . . . ?
C2 B3 B4 B8 100.81(17) . . . . ?
C2 B3 B4 B9 64.05(19) . . . . ?
C2 B3 B7 B8 -133.86(17) . . . . ?
C2 B3 B7 B11 -33.79(14) . . . . ?
C2 B3 B7 B12 -97.25(17) . . . . ?
C2 B3 B8 B4 -97.47(17) . . . . ?
C2 B3 B8 B7 40.09(15) . . . . ?
C2 B3 B8 B9 -60.1(2) . . . . ?
C2 B3 B8 B12 3.7(2) . . . . ?
C2 B6 B10 B5 97.55(17) . . . . ?
C2 B6 B10 B9 60.5(2) . . . . ?
C2 B6 B10 B11 -40.31(15) . . . . ?
C2 B6 B10 B12 -3.7(2) . . . . ?
C2 B6 B11 B7 33.75(14) . . . . ?
C2 B6 B11 B10 133.69(17) . . . . ?
C2 B6 B11 B12 97.34(17) . . . . ?
C2 B7 B8 B3 -39.98(15) . . . . ?
C2 B7 B8 B4 -1.9(2) . . . . ?
C2 B7 B8 B9 61.45(19) . . . . ?
C2 B7 B8 B12 99.17(17) . . . . ?
C2 B7 B11 B6 -34.05(15) . . . . ?
C2 B7 B11 B10 -96.37(17) . . . . ?
C2 B7 B11 B12 -133.79(17) . . . . ?
C2 B7 B12 B8 -98.33(17) . . . . ?
C2 B7 B12 B9 -60.9(2) . . . . ?
C2 B7 B12 B10 2.2(2) . . . . ?
C2 B7 B12 B11 39.94(15) . . . . ?
C2 B11 B12 B7 -39.75(15) . . . . ?
C2 B11 B12 B8 -2.4(2) . . . . ?
C2 B11 B12 B9 60.6(2) . . . . ?
C2 B11 B12 B10 98.23(17) . . . . ?
B3 C1 C2 P1 -108.92(14) . . . . ?
B3 C1 C2 B6 142.76(16) . . . . ?
B3 C1 C2 B7 38.09(15) . . . . ?
B3 C1 C2 B11 105.25(17) . . . . ?
B3 C1 B4 B5 -140.71(17) . . . . ?
B3 C1 B4 B8 -39.04(15) . . . . ?
B3 C1 B4 B9 -100.98(18) . . . . ?
B3 C1 B5 B4 36.98(16) . . . . ?
B3 C1 B5 B6 -103.80(18) . . . . ?
B3 C1 B5 B9 -3.1(2) . . . . ?
B3 C1 B5 B10 -65.0(2) . . . . ?
B3 C1 B6 C2 -34.78(14) . . . . ?
B3 C1 B6 B5 104.52(17) . . . . ?
B3 C1 B6 B10 64.2(2) . . . . ?
B3 C1 B6 B11 0.5(2) . . . . ?
B3 C1 C1' C2' 62.5(2) . . . . ?
B3 C1 C1' B3' 130.18(17) . . . . ?
B3 C1 C1' B4' -157.79(17) . . . . ?
B3 C1 C1' B5' -78.3(2) . . . . ?
B3 C1 C1' B6' -6.1(2) . . . . ?
B3 C2 B6 C1 36.36(16) . . . . ?
B3 C2 B6 B5 1.6(2) . . . . ?
B3 C2 B6 B10 -62.1(2) . . . . ?
B3 C2 B6 B11 -103.30(18) . . . . ?
B3 C2 B7 B8 39.53(15) . . . . ?
B3 C2 B7 B11 142.32(16) . . . . ?
B3 C2 B7 B12 102.07(17) . . . . ?
B3 C2 B11 B6 106.60(17) . . . . ?
B3 C2 B11 B7 -35.48(16) . . . . ?
B3 C2 B11 B10 66.9(2) . . . . ?
B3 C2 B11 B12 4.9(2) . . . . ?
B3 B4 B5 C1 -35.64(15) . . . . ?
B3 B4 B5 B6 -0.3(2) . . . . ?
B3 B4 B5 B9 98.58(18) . . . . ?
B3 B4 B5 B10 61.5(2) . . . . ?
B3 B4 B8 B7 -37.83(15) . . . . ?
B3 B4 B8 B9 -138.31(18) . . . . ?
B3 B4 B8 B12 -100.87(17) . . . . ?
B3 B4 B9 B5 -102.35(17) . . . . ?
B3 B4 B9 B8 36.19(15) . . . . ?
B3 B4 B9 B10 -64.6(2) . . . . ?
B3 B4 B9 B12 -1.3(2) . . . . ?
B3 B7 B8 B4 38.09(16) . . . . ?
B3 B7 B8 B9 101.42(19) . . . . ?
B3 B7 B8 B12 139.14(19) . . . . ?
B3 B7 B11 C2 33.95(14) . . . . ?
B3 B7 B11 B6 -0.1(2) . . . . ?
B3 B7 B11 B10 -62.4(2) . . . . ?
B3 B7 B11 B12 -99.84(18) . . . . ?
B3 B7 B12 B8 -35.96(16) . . . . ?
B3 B7 B12 B9 1.4(2) . . . . ?
B3 B7 B12 B10 64.5(2) . . . . ?
B3 B7 B12 B11 102.31(18) . . . . ?
B3 B8 B9 B4 -37.57(16) . . . . ?
B3 B8 B9 B5 -0.3(2) . . . . ?
B3 B8 B9 B10 64.0(2) . . . . ?
B3 B8 B9 B12 100.74(18) . . . . ?
B3 B8 B12 B7 36.52(16) . . . . ?
B3 B8 B12 B9 -101.30(19) . . . . ?
B3 B8 B12 B10 -64.7(2) . . . . ?
B3 B8 B12 B11 -0.8(2) . . . . ?
B4 C1 C2 P1 -146.23(13) . . . . ?
B4 C1 C2 B3 -37.31(15) . . . . ?
B4 C1 C2 B6 105.45(17) . . . . ?
B4 C1 C2 B7 0.8(2) . . . . ?
B4 C1 C2 B11 67.95(19) . . . . ?
B4 C1 B3 C2 139.71(16) . . . . ?
B4 C1 B3 B7 104.27(17) . . . . ?
B4 C1 B3 B8 40.45(15) . . . . ?
B4 C1 B5 B6 -140.78(18) . . . . ?
B4 C1 B5 B9 -40.05(16) . . . . ?
B4 C1 B5 B10 -102.02(19) . . . . ?
B4 C1 B6 C2 -101.77(17) . . . . ?
B4 C1 B6 B5 37.54(17) . . . . ?
B4 C1 B6 B10 -2.7(2) . . . . ?
B4 C1 B6 B11 -66.5(2) . . . . ?
B4 C1 C1' C2' 135.09(18) . . . . ?
B4 C1 C1' B3' -157.22(17) . . . . ?
B4 C1 C1' B4' -85.2(3) . . . . ?
B4 C1 C1' B5' -5.7(3) . . . . ?
B4 C1 C1' B6' 66.5(2) . . . . ?
B4 B3 B7 C2 94.96(17) . . . . ?
B4 B3 B7 B8 -38.91(16) . . . . ?
B4 B3 B7 B11 61.2(2) . . . . ?
B4 B3 B7 B12 -2.3(2) . . . . ?
B4 B3 B8 B7 137.56(18) . . . . ?
B4 B3 B8 B9 37.36(16) . . . . ?
B4 B3 B8 B12 101.15(19) . . . . ?
B4 B5 B6 C1 -34.78(15) . . . . ?
B4 B5 B6 C2 -0.7(2) . . . . ?
B4 B5 B6 B10 99.98(19) . . . . ?
B4 B5 B6 B11 61.3(2) . . . . ?
B4 B5 B9 B8 -37.40(16) . . . . ?
B4 B5 B9 B10 -138.29(17) . . . . ?
B4 B5 B9 B12 -101.27(18) . . . . ?
B4 B5 B10 B6 -101.17(17) . . . . ?
B4 B5 B10 B9 37.31(15) . . . . ?
B4 B5 B10 B11 -63.5(2) . . . . ?
B4 B5 B10 B12 -0.2(2) . . . . ?
B4 B8 B9 B5 37.31(16) . . . . ?
B4 B8 B9 B10 101.62(18) . . . . ?
B4 B8 B9 B12 138.31(17) . . . . ?
B4 B8 B12 B7 100.49(17) . . . . ?
B4 B8 B12 B9 -37.33(16) . . . . ?
B4 B8 B12 B10 -0.7(2) . . . . ?
B4 B8 B12 B11 63.1(2) . . . . ?
B4 B9 B10 B5 -37.55(16) . . . . ?
B4 B9 B10 B6 -0.2(2) . . . . ?
B4 B9 B10 B11 63.2(2) . . . . ?
B4 B9 B10 B12 100.97(19) . . . . ?
B4 B9 B12 B7 0.0(2) . . . . ?
B4 B9 B12 B8 37.58(17) . . . . ?
B4 B9 B12 B10 -101.29(19) . . . . ?
B4 B9 B12 B11 -63.4(2) . . . . ?
B5 C1 C2 P1 146.23(14) . . . . ?
B5 C1 C2 B3 -104.85(17) . . . . ?
B5 C1 C2 B6 37.91(16) . . . . ?
B5 C1 C2 B7 -66.8(2) . . . . ?
B5 C1 C2 B11 0.4(2) . . . . ?
B5 C1 B3 C2 102.21(17) . . . . ?
B5 C1 B3 B4 -37.50(16) . . . . ?
B5 C1 B3 B7 66.76(19) . . . . ?
B5 C1 B3 B8 2.9(2) . . . . ?
B5 C1 B4 B3 140.71(17) . . . . ?
B5 C1 B4 B8 101.67(18) . . . . ?
B5 C1 B4 B9 39.73(16) . . . . ?
B5 C1 B6 C2 -139.31(17) . . . . ?
B5 C1 B6 B10 -40.28(16) . . . . ?
B5 C1 B6 B11 -104.06(18) . . . . ?
B5 C1 C1' C2' -144.97(18) . . . . ?
B5 C1 C1' B3' -77.3(2) . . . . ?
B5 C1 C1' B4' -5.3(3) . . . . ?
B5 C1 C1' B5' 74.2(3) . . . . ?
B5 C1 C1' B6' 146.47(18) . . . . ?
B5 B4 B8 B3 101.45(17) . . . . ?
B5 B4 B8 B7 63.62(19) . . . . ?
B5 B4 B8 B9 -36.87(15) . . . . ?
B5 B4 B8 B12 0.6(2) . . . . ?
B5 B4 B9 B8 138.54(17) . . . . ?
B5 B4 B9 B10 37.76(16) . . . . ?
B5 B4 B9 B12 101.03(19) . . . . ?
B5 B6 B10 B9 -37.07(17) . . . . ?
B5 B6 B10 B11 -137.86(18) . . . . ?
B5 B6 B10 B12 -101.29(19) . . . . ?
B5 B6 B11 C2 -95.01(17) . . . . ?
B5 B6 B11 B7 -61.3(2) . . . . ?
B5 B6 B11 B10 38.68(16) . . . . ?
B5 B6 B11 B12 2.3(2) . . . . ?
B5 B9 B10 B6 37.37(16) . . . . ?
B5 B9 B10 B11 100.78(18) . . . . ?
B5 B9 B10 B12 138.52(17) . . . . ?
B5 B9 B12 B7 63.8(2) . . . . ?
B5 B9 B12 B8 101.38(18) . . . . ?
B5 B9 B12 B10 -37.48(16) . . . . ?
B5 B9 B12 B11 0.4(2) . . . . ?
B5 B10 B11 C2 2.2(2) . . . . ?
B5 B10 B11 B6 -37.86(16) . . . . ?
B5 B10 B11 B7 63.7(2) . . . . ?
B5 B10 B11 B12 101.27(19) . . . . ?
B5 B10 B12 B7 -63.0(2) . . . . ?
B5 B10 B12 B8 0.5(2) . . . . ?
B5 B10 B12 B9 37.09(15) . . . . ?
B5 B10 B12 B11 -100.62(17) . . . . ?
B6 C1 C2 P1 108.32(15) . . . . ?
B6 C1 C2 B3 -142.76(16) . . . . ?
B6 C1 C2 B7 -104.67(17) . . . . ?
B6 C1 C2 B11 -37.50(16) . . . . ?
B6 C1 B3 C2 34.92(14) . . . . ?
B6 C1 B3 B4 -104.78(17) . . . . ?
B6 C1 B3 B7 -0.5(2) . . . . ?
B6 C1 B3 B8 -64.34(19) . . . . ?
B6 C1 B4 B3 103.56(18) . . . . ?
B6 C1 B4 B5 -37.15(16) . . . . ?
B6 C1 B4 B8 64.5(2) . . . . ?
B6 C1 B4 B9 2.6(2) . . . . ?
B6 C1 B5 B4 140.78(18) . . . . ?
B6 C1 B5 B9 100.73(18) . . . . ?
B6 C1 B5 B10 38.76(16) . . . . ?
B6 C1 C1' C2' -72.5(2) . . . . ?
B6 C1 C1' B3' -4.8(2) . . . . ?
B6 C1 C1' B4' 67.2(2) . . . . ?
B6 C1 C1' B5' 146.65(18) . . . . ?
B6 C1 C1' B6' -141.07(16) . . . . ?
B6 C2 B3 C1 -36.15(15) . . . . ?
B6 C2 B3 B4 -1.7(2) . . . . ?
B6 C2 B3 B7 103.05(18) . . . . ?
B6 C2 B3 B8 61.9(2) . . . . ?
B6 C2 B7 B3 -106.76(17) . . . . ?
B6 C2 B7 B8 -67.23(19) . . . . ?
B6 C2 B7 B11 35.56(16) . . . . ?
B6 C2 B7 B12 -4.7(2) . . . . ?
B6 C2 B11 B7 -142.08(17) . . . . ?
B6 C2 B11 B10 -39.71(15) . . . . ?
B6 C2 B11 B12 -101.72(18) . . . . ?
B6 B5 B9 B4 102.23(17) . . . . ?
B6 B5 B9 B8 64.8(2) . . . . ?
B6 B5 B9 B10 -36.06(15) . . . . ?
B6 B5 B9 B12 1.0(2) . . . . ?
B6 B5 B10 B9 138.48(18) . . . . ?
B6 B5 B10 B11 37.64(16) . . . . ?
B6 B5 B10 B12 100.99(18) . . . . ?
B6 B10 B11 C2 40.09(15) . . . . ?
B6 B10 B11 B7 101.55(18) . . . . ?
B6 B10 B11 B12 139.12(18) . . . . ?
B6 B10 B12 B7 1.0(2) . . . . ?
B6 B10 B12 B8 64.5(2) . . . . ?
B6 B10 B12 B9 101.10(18) . . . . ?
B6 B10 B12 B11 -36.61(16) . . . . ?
B6 B11 B12 B7 -102.03(18) . . . . ?
B6 B11 B12 B8 -64.6(2) . . . . ?
B6 B11 B12 B9 -1.7(2) . . . . ?
B6 B11 B12 B10 35.94(16) . . . . ?
B7 C2 B3 C1 -139.20(16) . . . . ?
B7 C2 B3 B4 -104.78(17) . . . . ?
B7 C2 B3 B8 -41.19(15) . . . . ?
B7 C2 B6 C1 103.78(17) . . . . ?
B7 C2 B6 B5 69.00(19) . . . . ?
B7 C2 B6 B10 5.4(2) . . . . ?
B7 C2 B6 B11 -35.88(16) . . . . ?
B7 C2 B11 B6 142.08(17) . . . . ?
B7 C2 B11 B10 102.37(17) . . . . ?
B7 C2 B11 B12 40.37(15) . . . . ?
B7 B3 B4 C1 -95.45(17) . . . . ?
B7 B3 B4 B5 -60.7(2) . . . . ?
B7 B3 B4 B8 38.99(16) . . . . ?
B7 B3 B4 B9 2.2(2) . . . . ?
B7 B3 B8 B4 -137.56(18) . . . . ?
B7 B3 B8 B9 -100.20(19) . . . . ?
B7 B3 B8 B12 -36.41(16) . . . . ?
B7 B8 B9 B4 -100.86(18) . . . . ?
B7 B8 B9 B5 -63.6(2) . . . . ?
B7 B8 B9 B10 0.8(2) . . . . ?
B7 B8 B9 B12 37.44(16) . . . . ?
B7 B8 B12 B9 -137.82(18) . . . . ?
B7 B8 B12 B10 -101.18(18) . . . . ?
B7 B8 B12 B11 -37.35(16) . . . . ?
B7 B11 B12 B8 37.39(16) . . . . ?
B7 B11 B12 B9 100.34(18) . . . . ?
B7 B11 B12 B10 137.97(18) . . . . ?
B8 B3 B4 C1 -134.45(17) . . . . ?
B8 B3 B4 B5 -99.67(18) . . . . ?
B8 B3 B4 B9 -36.76(16) . . . . ?
B8 B3 B7 C2 133.86(17) . . . . ?
B8 B3 B7 B11 100.08(18) . . . . ?
B8 B3 B7 B12 36.62(17) . . . . ?
B8 B4 B5 C1 -97.37(17) . . . . ?
B8 B4 B5 B6 -62.0(2) . . . . ?
B8 B4 B5 B9 36.85(15) . . . . ?
B8 B4 B5 B10 -0.2(2) . . . . ?
B8 B4 B9 B5 -138.54(17) . . . . ?
B8 B4 B9 B10 -100.78(19) . . . . ?
B8 B4 B9 B12 -37.50(17) . . . . ?
B8 B7 B11 C2 96.31(17) . . . . ?
B8 B7 B11 B6 62.3(2) . . . . ?
B8 B7 B11 B10 -0.1(2) . . . . ?
B8 B7 B11 B12 -37.48(16) . . . . ?
B8 B7 B12 B9 37.38(17) . . . . ?
B8 B7 B12 B10 100.48(19) . . . . ?
B8 B7 B12 B11 138.27(18) . . . . ?
B8 B9 B10 B5 -101.57(18) . . . . ?
B8 B9 B10 B6 -64.2(2) . . . . ?
B8 B9 B10 B11 -0.8(2) . . . . ?
B8 B9 B10 B12 36.95(16) . . . . ?
B8 B9 B12 B7 -37.63(16) . . . . ?
B8 B9 B12 B10 -138.86(17) . . . . ?
B8 B9 B12 B11 -100.94(18) . . . . ?
B9 B4 B5 C1 -134.22(17) . . . . ?
B9 B4 B5 B6 -98.84(19) . . . . ?
B9 B4 B5 B10 -37.09(15) . . . . ?
B9 B4 B8 B3 138.31(18) . . . . ?
B9 B4 B8 B7 100.49(18) . . . . ?
B9 B4 B8 B12 37.44(16) . . . . ?
B9 B5 B6 C1 -98.13(18) . . . . ?
B9 B5 B6 C2 -64.09(19) . . . . ?
B9 B5 B6 B10 36.63(16) . . . . ?
B9 B5 B6 B11 -2.1(2) . . . . ?
B9 B5 B10 B6 -138.48(18) . . . . ?
B9 B5 B10 B11 -100.84(19) . . . . ?
B9 B5 B10 B12 -37.49(16) . . . . ?
B9 B8 B12 B7 137.82(18) . . . . ?
B9 B8 B12 B10 36.64(16) . . . . ?
B9 B8 B12 B11 100.47(19) . . . . ?
B9 B10 B11 C2 -60.9(2) . . . . ?
B9 B10 B11 B6 -101.03(18) . . . . ?
B9 B10 B11 B7 0.5(2) . . . . ?
B9 B10 B11 B12 38.10(16) . . . . ?
B9 B10 B12 B7 -100.10(18) . . . . ?
B9 B10 B12 B8 -36.55(15) . . . . ?
B9 B10 B12 B11 -137.71(17) . . . . ?
B10 B5 B6 C1 -134.76(18) . . . . ?
B10 B5 B6 C2 -100.72(18) . . . . ?
B10 B5 B6 B11 -38.68(16) . . . . ?
B10 B5 B9 B4 138.29(17) . . . . ?
B10 B5 B9 B8 100.89(18) . . . . ?
B10 B5 B9 B12 37.03(16) . . . . ?
B10 B6 B11 C2 -133.69(17) . . . . ?
B10 B6 B11 B7 -99.94(18) . . . . ?
B10 B6 B11 B12 -36.35(16) . . . . ?
B10 B9 B12 B7 101.24(18) . . . . ?
B10 B9 B12 B8 138.86(17) . . . . ?
B10 B9 B12 B11 37.92(16) . . . . ?
B10 B11 B12 B7 -137.97(18) . . . . ?
B10 B11 B12 B8 -100.58(19) . . . . ?
B10 B11 B12 B9 -37.64(16) . . . . ?
B11 C2 B3 C1 -103.47(17) . . . . ?
B11 C2 B3 B4 -69.04(19) . . . . ?
B11 C2 B3 B7 35.74(16) . . . . ?
B11 C2 B3 B8 -5.5(2) . . . . ?
B11 C2 B6 C1 139.66(16) . . . . ?
B11 C2 B6 B5 104.87(18) . . . . ?
B11 C2 B6 B10 41.24(16) . . . . ?
B11 C2 B7 B3 -142.32(16) . . . . ?
B11 C2 B7 B8 -102.79(17) . . . . ?
B11 C2 B7 B12 -40.25(15) . . . . ?
B11 B6 B10 B5 137.86(18) . . . . ?
B11 B6 B10 B9 100.80(19) . . . . ?
B11 B6 B10 B12 36.57(16) . . . . ?
B11 B7 B8 B3 -101.85(18) . . . . ?
B11 B7 B8 B4 -63.8(2) . . . . ?
B11 B7 B8 B9 -0.4(2) . . . . ?
B11 B7 B8 B12 37.29(16) . . . . ?
B11 B7 B12 B8 -138.27(18) . . . . ?
B11 B7 B12 B9 -100.89(19) . . . . ?
B11 B7 B12 B10 -37.78(16) . . . . ?
B11 B10 B12 B7 37.61(16) . . . . ?
B11 B10 B12 B8 101.16(17) . . . . ?
B11 B10 B12 B9 137.71(17) . . . . ?
C11 P1 C2 C1 118.54(13) . . . . ?
C11 P1 C2 B3 49.61(16) . . . . ?
C11 P1 C2 B6 -173.24(14) . . . . ?
C11 P1 C2 B7 -22.35(18) . . . . ?
C11 P1 C2 B11 -101.87(17) . . . . ?
C11 P1 C2' C1' -115.16(13) . . . . ?
C11 P1 C2' B3' 178.08(12) . . . . ?
C11 P1 C2' B6' -46.85(16) . . . . ?
C11 P1 C2' B7' 111.02(16) . . . . ?
C11 P1 C2' B11' 31.7(2) . . . . ?
C11 C12 C13 C14 -1.2(3) . . . . ?
B12 B7 B8 B3 -139.14(19) . . . . ?
B12 B7 B8 B4 -101.05(19) . . . . ?
B12 B7 B8 B9 -37.72(16) . . . . ?
B12 B7 B11 C2 133.79(17) . . . . ?
B12 B7 B11 B6 99.74(18) . . . . ?
B12 B7 B11 B10 37.42(16) . . . . ?
B12 B8 B9 B4 -138.31(18) . . . . ?
B12 B8 B9 B5 -100.99(19) . . . . ?
B12 B8 B9 B10 -36.69(16) . . . . ?
B12 B9 B10 B5 -138.52(17) . . . . ?
B12 B9 B10 B6 -101.15(19) . . . . ?
B12 B9 B10 B11 -37.74(16) . . . . ?
B12 B10 B11 C2 -99.03(17) . . . . ?
B12 B10 B11 B6 -139.12(18) . . . . ?
B12 B10 B11 B7 -37.58(16) . . . . ?
C12 C11 C16 C15 -0.4(3) . . . . ?
C12 C13 C14 C15 0.3(3) . . . . ?
C13 C14 C15 C16 0.6(3) . . . . ?
C14 C15 C16 C11 -0.5(3) . . . . ?
C16 C11 C12 C13 1.2(3) . . . . ?
C1' C1 C2 P1 0.09(19) . . . . ?
C1' C1 C2 B3 109.02(17) . . . . ?
C1' C1 C2 B6 -108.23(18) . . . . ?
C1' C1 C2 B7 147.10(16) . . . . ?
C1' C1 C2 B11 -145.73(16) . . . . ?
C1' C1 B3 C2 -101.68(17) . . . . ?
C1' C1 B3 B4 118.61(18) . . . . ?
C1' C1 B3 B7 -137.12(16) . . . . ?
C1' C1 B3 B8 159.06(16) . . . . ?
C1' C1 B4 B3 -103.4(2) . . . . ?
C1' C1 B4 B5 115.9(2) . . . . ?
C1' C1 B4 B8 -142.39(19) . . . . ?
C1' C1 B4 B9 155.67(18) . . . . ?
C1' C1 B5 B4 -116.5(2) . . . . ?
C1' C1 B5 B6 102.7(2) . . . . ?
C1' C1 B5 B9 -156.54(18) . . . . ?
C1' C1 B5 B10 141.49(19) . . . . ?
C1' C1 B6 C2 102.17(17) . . . . ?
C1' C1 B6 B5 -118.52(19) . . . . ?
C1' C1 B6 B10 -158.80(17) . . . . ?
C1' C1 B6 B11 137.42(17) . . . . ?
C1' C2' B3' B4' 34.08(14) . . . . ?
C1' C2' B3' B7' 138.70(16) . . . . ?
C1' C2' B3' B8' 97.93(17) . . . . ?
C1' C2' B6' B5' -34.58(14) . . . . ?
C1' C2' B6' B10' -98.38(17) . . . . ?
C1' C2' B6' B11' -139.01(17) . . . . ?
C1' C2' B7' B3' -38.91(15) . . . . ?
C1' C2' B7' B8' 0.2(2) . . . . ?
C1' C2' B7' B11' 102.69(17) . . . . ?
C1' C2' B7' B12' 62.30(19) . . . . ?
C1' C2' B11' B6' 38.08(15) . . . . ?
C1' C2' B11' B7' -103.47(17) . . . . ?
C1' C2' B11' B10' -1.1(2) . . . . ?
C1' C2' B11' B12' -63.13(19) . . . . ?
C1' B3' B4' B5' 34.51(15) . . . . ?
C1' B3' B4' B8' 134.22(17) . . . . ?
C1' B3' B4' B9' 98.02(17) . . . . ?
C1' B3' B7' C2' 34.53(14) . . . . ?
C1' B3' B7' B8' -99.85(17) . . . . ?
C1' B3' B7' B11' 0.0(2) . . . . ?
C1' B3' B7' B12' -63.64(19) . . . . ?
C1' B3' B8' B4' -39.11(15) . . . . ?
C1' B3' B8' B7' 98.38(17) . . . . ?
C1' B3' B8' B9' -2.4(2) . . . . ?
C1' B3' B8' B12' 61.8(2) . . . . ?
C1' B4' B5' B6' 35.16(15) . . . . ?
C1' B4' B5' B9' 134.20(16) . . . . ?
C1' B4' B5' B10' 96.90(16) . . . . ?
C1' B4' B8' B3' 40.43(15) . . . . ?
C1' B4' B8' B7' 2.4(2) . . . . ?
C1' B4' B8' B9' -98.59(18) . . . . ?
C1' B4' B8' B12' -60.9(2) . . . . ?
C1' B4' B9' B5' -39.33(15) . . . . ?
C1' B4' B9' B8' 99.16(17) . . . . ?
C1' B4' B9' B10' -1.5(2) . . . . ?
C1' B4' B9' B12' 61.8(2) . . . . ?
C1' B5' B6' C2' 33.69(13) . . . . ?
C1' B5' B6' B10' 133.94(16) . . . . ?
C1' B5' B6' B11' 95.45(17) . . . . ?
C1' B5' B9' B4' 39.17(14) . . . . ?
C1' B5' B9' B8' 1.6(2) . . . . ?
C1' B5' B9' B10' -98.70(16) . . . . ?
C1' B5' B9' B12' -61.9(2) . . . . ?
C1' B5' B10' B6' -40.16(15) . . . . ?
C1' B5' B10' B9' 98.37(17) . . . . ?
C1' B5' B10' B11' -2.3(2) . . . . ?
C1' B5' B10' B12' 61.2(2) . . . . ?
C1' B6' B10' B5' 39.56(14) . . . . ?
C1' B6' B10' B9' 2.4(2) . . . . ?
C1' B6' B10' B11' -98.39(16) . . . . ?
C1' B6' B10' B12' -61.70(19) . . . . ?
C1' B6' B11' C2' -34.38(14) . . . . ?
C1' B6' B11' B7' 0.0(2) . . . . ?
C1' B6' B11' B10' 99.88(17) . . . . ?
C1' B6' B11' B12' 63.60(19) . . . . ?
C2' P1 C2 C1 3.85(14) . . . . ?
C2' P1 C2 B3 -65.08(15) . . . . ?
C2' P1 C2 B6 72.07(15) . . . . ?
C2' P1 C2 B7 -137.04(16) . . . . ?
C2' P1 C2 B11 143.44(17) . . . . ?
C2' P1 C11 C12 -172.33(14) . . . . ?
C2' P1 C11 C16 6.8(2) . . . . ?
C2' C1' B3' B4' -140.23(16) . . . . ?
C2' C1' B3' B7' -35.81(14) . . . . ?
C2' C1' B3' B8' -99.50(17) . . . . ?
C2' C1' B4' B3' 36.87(15) . . . . ?
C2' C1' B4' B5' -104.34(16) . . . . ?
C2' C1' B4' B8' -2.4(2) . . . . ?
C2' C1' B4' B9' -64.30(19) . . . . ?
C2' C1' B5' B4' 103.15(17) . . . . ?
C2' C1' B5' B6' -37.73(15) . . . . ?
C2' C1' B5' B9' 63.47(19) . . . . ?
C2' C1' B5' B10' 1.7(2) . . . . ?
C2' C1' B6' B5' 139.89(16) . . . . ?
C2' C1' B6' B10' 98.93(16) . . . . ?
C2' C1' B6' B11' 35.49(14) . . . . ?
C2' B3' B4' C1' -33.30(14) . . . . ?
C2' B3' B4' B5' 1.2(2) . . . . ?
C2' B3' B4' B8' 100.92(17) . . . . ?
C2' B3' B4' B9' 64.7(2) . . . . ?
C2' B3' B7' B8' -134.38(17) . . . . ?
C2' B3' B7' B11' -34.53(15) . . . . ?
C2' B3' B7' B12' -98.17(17) . . . . ?
C2' B3' B8' B4' -97.78(17) . . . . ?
C2' B3' B8' B7' 39.71(15) . . . . ?
C2' B3' B8' B9' -61.1(2) . . . . ?
C2' B3' B8' B12' 3.1(2) . . . . ?
C2' B6' B10' B5' 98.35(16) . . . . ?
C2' B6' B10' B9' 61.16(19) . . . . ?
C2' B6' B10' B11' -39.60(14) . . . . ?
C2' B6' B10' B12' -2.9(2) . . . . ?
C2' B6' B11' B7' 34.38(15) . . . . ?
C2' B6' B11' B10' 134.26(17) . . . . ?
C2' B6' B11' B12' 97.98(17) . . . . ?
C2' B7' B8' B3' -39.71(15) . . . . ?
C2' B7' B8' B4' -1.6(2) . . . . ?
C2' B7' B8' B9' 61.6(2) . . . . ?
C2' B7' B8' B12' 99.51(17) . . . . ?
C2' B7' B11' B6' -34.66(15) . . . . ?
C2' B7' B11' B10' -96.66(16) . . . . ?
C2' B7' B11' B12' -133.94(16) . . . . ?
C2' B7' B12' B8' -98.29(17) . . . . ?
C2' B7' B12' B9' -60.9(2) . . . . ?
C2' B7' B12' B10' 2.5(2) . . . . ?
C2' B7' B12' B11' 40.07(15) . . . . ?
C2' B11' B12' B7' -39.86(14) . . . . ?
C2' B11' B12' B8' -2.4(2) . . . . ?
C2' B11' B12' B9' 60.7(2) . . . . ?
C2' B11' B12' B10' 98.31(16) . . . . ?
B3' C1' C2' P1 -101.25(14) . . . . ?
B3' C1' C2' B6' 142.30(16) . . . . ?
B3' C1' C2' B7' 38.26(15) . . . . ?
B3' C1' C2' B11' 104.40(17) . . . . ?
B3' C1' B4' B5' -141.20(16) . . . . ?
B3' C1' B4' B8' -39.24(15) . . . . ?
B3' C1' B4' B9' -101.16(18) . . . . ?
B3' C1' B5' B4' 36.49(15) . . . . ?
B3' C1' B5' B6' -104.39(17) . . . . ?
B3' C1' B5' B9' -3.2(2) . . . . ?
B3' C1' B5' B10' -65.00(19) . . . . ?
B3' C1' B6' C2' -35.50(15) . . . . ?
B3' C1' B6' B5' 104.40(17) . . . . ?
B3' C1' B6' B10' 63.43(19) . . . . ?
B3' C1' B6' B11' 0.0(2) . . . . ?
B3' C2' B6' C1' 36.29(15) . . . . ?
B3' C2' B6' B5' 1.7(2) . . . . ?
B3' C2' B6' B10' -62.09(19) . . . . ?
B3' C2' B6' B11' -102.72(17) . . . . ?
B3' C2' B7' B8' 39.10(15) . . . . ?
B3' C2' B7' B11' 141.59(17) . . . . ?
B3' C2' B7' B12' 101.21(17) . . . . ?
B3' C2' B11' B6' 105.75(17) . . . . ?
B3' C2' B11' B7' -35.80(16) . . . . ?
B3' C2' B11' B10' 66.62(19) . . . . ?
B3' C2' B11' B12' 4.5(2) . . . . ?
B3' B4' B5' C1' -35.39(15) . . . . ?
B3' B4' B5' B6' -0.2(2) . . . . ?
B3' B4' B5' B9' 98.81(19) . . . . ?
B3' B4' B5' B10' 61.5(2) . . . . ?
B3' B4' B8' B7' -38.00(16) . . . . ?
B3' B4' B8' B9' -139.02(18) . . . . ?
B3' B4' B8' B12' -101.33(19) . . . . ?
B3' B4' B9' B5' -102.80(18) . . . . ?
B3' B4' B9' B8' 35.68(16) . . . . ?
B3' B4' B9' B10' -64.9(2) . . . . ?
B3' B4' B9' B12' -1.7(2) . . . . ?
B3' B7' B8' B4' 38.07(16) . . . . ?
B3' B7' B8' B9' 101.34(19) . . . . ?
B3' B7' B8' B12' 139.22(18) . . . . ?
B3' B7' B11' C2' 34.66(15) . . . . ?
B3' B7' B11' B6' 0.0(2) . . . . ?
B3' B7' B11' B10' -62.0(2) . . . . ?
B3' B7' B11' B12' -99.28(18) . . . . ?
B3' B7' B12' B8' -35.70(16) . . . . ?
B3' B7' B12' B9' 1.7(2) . . . . ?
B3' B7' B12' B10' 65.1(2) . . . . ?
B3' B7' B12' B11' 102.67(18) . . . . ?
B3' B8' B9' B4' -36.90(16) . . . . ?
B3' B8' B9' B5' 0.6(2) . . . . ?
B3' B8' B9' B10' 64.5(2) . . . . ?
B3' B8' B9' B12' 101.27(19) . . . . ?
B3' B8' B12' B7' 36.67(16) . . . . ?
B3' B8' B12' B9' -101.26(19) . . . . ?
B3' B8' B12' B10' -64.4(2) . . . . ?
B3' B8' B12' B11' -0.5(2) . . . . ?
B4' C1' C2' P1 -138.09(14) . . . . ?
B4' C1' C2' B3' -36.84(16) . . . . ?
B4' C1' C2' B6' 105.46(17) . . . . ?
B4' C1' C2' B7' 1.4(2) . . . . ?
B4' C1' C2' B11' 67.6(2) . . . . ?
B4' C1' B3' C2' 140.23(16) . . . . ?
B4' C1' B3' B7' 104.42(18) . . . . ?
B4' C1' B3' B8' 40.73(16) . . . . ?
B4' C1' B5' B6' -140.88(17) . . . . ?
B4' C1' B5' B9' -39.68(15) . . . . ?
B4' C1' B5' B10' -101.49(17) . . . . ?
B4' C1' B6' C2' -102.41(17) . . . . ?
B4' C1' B6' B5' 37.48(16) . . . . ?
B4' C1' B6' B10' -3.5(2) . . . . ?
B4' C1' B6' B11' -66.92(19) . . . . ?
B4' B3' B7' C2' 95.33(17) . . . . ?
B4' B3' B7' B8' -39.05(17) . . . . ?
B4' B3' B7' B11' 60.8(2) . . . . ?
B4' B3' B7' B12' -2.8(2) . . . . ?
B4' B3' B8' B7' 137.49(18) . . . . ?
B4' B3' B8' B9' 36.71(16) . . . . ?
B4' B3' B8' B12' 100.93(19) . . . . ?
B4' B5' B6' C1' -34.54(15) . . . . ?
B4' B5' B6' C2' -0.8(2) . . . . ?
B4' B5' B6' B10' 99.41(18) . . . . ?
B4' B5' B6' B11' 60.9(2) . . . . ?
B4' B5' B9' B8' -37.61(16) . . . . ?
B4' B5' B9' B10' -137.87(17) . . . . ?
B4' B5' B9' B12' -101.06(18) . . . . ?
B4' B5' B10' B6' -101.25(17) . . . . ?
B4' B5' B10' B9' 37.28(16) . . . . ?
B4' B5' B10' B11' -63.4(2) . . . . ?
B4' B5' B10' B12' 0.1(2) . . . . ?
B4' B8' B9' B5' 37.46(16) . . . . ?
B4' B8' B9' B10' 101.38(18) . . . . ?
B4' B8' B9' B12' 138.17(18) . . . . ?
B4' B8' B12' B7' 100.54(19) . . . . ?
B4' B8' B12' B9' -37.38(16) . . . . ?
B4' B8' B12' B10' -0.5(2) . . . . ?
B4' B8' B12' B11' 63.4(2) . . . . ?
B4' B9' B10' B5' -37.85(16) . . . . ?
B4' B9' B10' B6' -0.6(2) . . . . ?
B4' B9' B10' B11' 63.4(2) . . . . ?
B4' B9' B10' B12' 100.95(18) . . . . ?
B4' B9' B12' B7' 0.0(2) . . . . ?
B4' B9' B12' B8' 37.74(17) . . . . ?
B4' B9' B12' B10' -100.94(19) . . . . ?
B4' B9' B12' B11' -63.1(2) . . . . ?
B5' C1' C2' P1 153.96(13) . . . . ?
B5' C1' C2' B3' -104.79(17) . . . . ?
B5' C1' C2' B6' 37.51(16) . . . . ?
B5' C1' C2' B7' -66.5(2) . . . . ?
B5' C1' C2' B11' -0.4(2) . . . . ?
B5' C1' B3' C2' 103.08(16) . . . . ?
B5' C1' B3' B4' -37.15(16) . . . . ?
B5' C1' B3' B7' 67.28(19) . . . . ?
B5' C1' B3' B8' 3.6(2) . . . . ?
B5' C1' B4' B3' 141.20(16) . . . . ?
B5' C1' B4' B8' 101.97(18) . . . . ?
B5' C1' B4' B9' 40.04(15) . . . . ?
B5' C1' B6' C2' -139.89(16) . . . . ?
B5' C1' B6' B10' -40.96(15) . . . . ?
B5' C1' B6' B11' -104.40(17) . . . . ?
B5' B4' B8' B3' 101.86(18) . . . . ?
B5' B4' B8' B7' 63.9(2) . . . . ?
B5' B4' B8' B9' -37.16(16) . . . . ?
B5' B4' B8' B12' 0.5(2) . . . . ?
B5' B4' B9' B8' 138.48(17) . . . . ?
B5' B4' B9' B10' 37.87(15) . . . . ?
B5' B4' B9' B12' 101.11(18) . . . . ?
B5' B6' B10' B9' -37.19(16) . . . . ?
B5' B6' B10' B11' -137.95(17) . . . . ?
B5' B6' B10' B12' -101.27(18) . . . . ?
B5' B6' B11' C2' -95.65(17) . . . . ?
B5' B6' B11' B7' -61.3(2) . . . . ?
B5' B6' B11' B10' 38.62(16) . . . . ?
B5' B6' B11' B12' 2.3(2) . . . . ?
B5' B9' B10' B6' 37.25(15) . . . . ?
B5' B9' B10' B11' 101.27(17) . . . . ?
B5' B9' B10' B12' 138.80(17) . . . . ?
B5' B9' B12' B7' 63.8(2) . . . . ?
B5' B9' B12' B8' 101.60(19) . . . . ?
B5' B9' B12' B10' -37.08(16) . . . . ?
B5' B9' B12' B11' 0.7(2) . . . . ?
B5' B10' B11' C2' 2.0(2) . . . . ?
B5' B10' B11' B6' -37.76(16) . . . . ?
B5' B10' B11' B7' 63.9(2) . . . . ?
B5' B10' B11' B12' 101.35(18) . . . . ?
B5' B10' B12' B7' -63.6(2) . . . . ?
B5' B10' B12' B8' 0.2(2) . . . . ?
B5' B10' B12' B9' 37.04(16) . . . . ?
B5' B10' B12' B11' -100.88(17) . . . . ?
B6' C1' C2' P1 116.45(15) . . . . ?
B6' C1' C2' B3' -142.30(16) . . . . ?
B6' C1' C2' B7' -104.04(17) . . . . ?
B6' C1' C2' B11' -37.91(16) . . . . ?
B6' C1' B3' C2' 35.82(15) . . . . ?
B6' C1' B3' B4' -104.42(18) . . . . ?
B6' C1' B3' B7' 0.0(2) . . . . ?
B6' C1' B3' B8' -63.7(2) . . . . ?
B6' C1' B4' B3' 104.24(16) . . . . ?
B6' C1' B4' B5' -36.96(15) . . . . ?
B6' C1' B4' B8' 65.0(2) . . . . ?
B6' C1' B4' B9' 3.1(2) . . . . ?
B6' C1' B5' B4' 140.88(17) . . . . ?
B6' C1' B5' B9' 101.20(17) . . . . ?
B6' C1' B5' B10' 39.39(15) . . . . ?
B6' C2' B3' C1' -35.92(15) . . . . ?
B6' C2' B3' B4' -1.8(2) . . . . ?
B6' C2' B3' B7' 102.79(17) . . . . ?
B6' C2' B3' B8' 62.0(2) . . . . ?
B6' C2' B7' B3' -105.67(17) . . . . ?
B6' C2' B7' B8' -66.57(19) . . . . ?
B6' C2' B7' B11' 35.93(15) . . . . ?
B6' C2' B7' B12' -4.5(2) . . . . ?
B6' C2' B11' B7' -141.55(17) . . . . ?
B6' C2' B11' B10' -39.13(15) . . . . ?
B6' C2' B11' B12' -101.20(17) . . . . ?
B6' B5' B9' B4' 101.74(17) . . . . ?
B6' B5' B9' B8' 64.1(2) . . . . ?
B6' B5' B9' B10' -36.13(15) . . . . ?
B6' B5' B9' B12' 0.7(2) . . . . ?
B6' B5' B10' B9' 138.53(17) . . . . ?
B6' B5' B10' B11' 37.89(16) . . . . ?
B6' B5' B10' B12' 101.33(18) . . . . ?
B6' B10' B11' C2' 39.80(15) . . . . ?
B6' B10' B11' B7' 101.65(17) . . . . ?
B6' B10' B11' B12' 139.10(17) . . . . ?
B6' B10' B12' B7' 0.3(2) . . . . ?
B6' B10' B12' B8' 64.1(2) . . . . ?
B6' B10' B12' B9' 100.95(18) . . . . ?
B6' B10' B12' B11' -36.97(16) . . . . ?
B6' B11' B12' B7' -102.44(17) . . . . ?
B6' B11' B12' B8' -65.0(2) . . . . ?
B6' B11' B12' B9' -1.9(2) . . . . ?
B6' B11' B12' B10' 35.73(15) . . . . ?
B7' C2' B3' C1' -138.70(16) . . . . ?
B7' C2' B3' B4' -104.62(18) . . . . ?
B7' C2' B3' B8' -40.77(16) . . . . ?
B7' C2' B6' C1' 103.05(17) . . . . ?
B7' C2' B6' B5' 68.47(19) . . . . ?
B7' C2' B6' B10' 4.7(2) . . . . ?
B7' C2' B6' B11' -35.96(16) . . . . ?
B7' C2' B11' B6' 141.55(17) . . . . ?
B7' C2' B11' B10' 102.42(18) . . . . ?
B7' C2' B11' B12' 40.34(15) . . . . ?
B7' B3' B4' C1' -95.20(17) . . . . ?
B7' B3' B4' B5' -60.7(2) . . . . ?
B7' B3' B4' B8' 39.02(17) . . . . ?
B7' B3' B4' B9' 2.8(2) . . . . ?
B7' B3' B8' B4' -137.49(18) . . . . ?
B7' B3' B8' B9' -100.78(18) . . . . ?
B7' B3' B8' B12' -36.56(16) . . . . ?
B7' B8' B9' B4' -100.59(18) . . . . ?
B7' B8' B9' B5' -63.1(2) . . . . ?
B7' B8' B9' B10' 0.8(2) . . . . ?
B7' B8' B9' B12' 37.58(16) . . . . ?
B7' B8' B12' B9' -137.93(18) . . . . ?
B7' B8' B12' B10' -101.02(18) . . . . ?
B7' B8' B12' B11' -37.12(15) . . . . ?
B7' B11' B12' B8' 37.43(16) . . . . ?
B7' B11' B12' B9' 100.57(18) . . . . ?
B7' B11' B12' B10' 138.17(17) . . . . ?
B8' B3' B4' C1' -134.22(17) . . . . ?
B8' B3' B4' B5' -99.71(19) . . . . ?
B8' B3' B4' B9' -36.20(16) . . . . ?
B8' B3' B7' C2' 134.38(17) . . . . ?
B8' B3' B7' B11' 99.85(18) . . . . ?
B8' B3' B7' B12' 36.21(16) . . . . ?
B8' B4' B5' C1' -97.28(17) . . . . ?
B8' B4' B5' B6' -62.1(2) . . . . ?
B8' B4' B5' B9' 36.92(16) . . . . ?
B8' B4' B5' B10' -0.4(2) . . . . ?
B8' B4' B9' B5' -138.48(17) . . . . ?
B8' B4' B9' B10' -100.61(18) . . . . ?
B8' B4' B9' B12' -37.38(16) . . . . ?
B8' B7' B11' C2' 96.82(17) . . . . ?
B8' B7' B11' B6' 62.2(2) . . . . ?
B8' B7' B11' B10' 0.2(2) . . . . ?
B8' B7' B11' B12' -37.12(16) . . . . ?
B8' B7' B12' B9' 37.43(16) . . . . ?
B8' B7' B12' B10' 100.77(18) . . . . ?
B8' B7' B12' B11' 138.37(17) . . . . ?
B8' B9' B10' B5' -101.96(18) . . . . ?
B8' B9' B10' B6' -64.7(2) . . . . ?
B8' B9' B10' B11' -0.7(2) . . . . ?
B8' B9' B10' B12' 36.83(16) . . . . ?
B8' B9' B12' B7' -37.75(17) . . . . ?
B8' B9' B12' B10' -138.68(18) . . . . ?
B8' B9' B12' B11' -100.85(18) . . . . ?
B9' B4' B5' C1' -134.20(16) . . . . ?
B9' B4' B5' B6' -99.04(18) . . . . ?
B9' B4' B5' B10' -37.30(16) . . . . ?
B9' B4' B8' B3' 139.02(18) . . . . ?
B9' B4' B8' B7' 101.02(19) . . . . ?
B9' B4' B8' B12' 37.69(17) . . . . ?
B9' B5' B6' C1' -97.32(17) . . . . ?
B9' B5' B6' C2' -63.63(19) . . . . ?
B9' B5' B6' B10' 36.62(16) . . . . ?
B9' B5' B6' B11' -1.9(2) . . . . ?
B9' B5' B10' B6' -138.53(17) . . . . ?
B9' B5' B10' B11' -100.64(18) . . . . ?
B9' B5' B10' B12' -37.19(16) . . . . ?
B9' B8' B12' B7' 137.93(18) . . . . ?
B9' B8' B12' B10' 36.90(16) . . . . ?
B9' B8' B12' B11' 100.81(18) . . . . ?
B9' B10' B11' C2' -61.5(2) . . . . ?
B9' B10' B11' B6' -101.32(18) . . . . ?
B9' B10' B11' B7' 0.3(2) . . . . ?
B9' B10' B11' B12' 37.79(16) . . . . ?
B9' B10' B12' B7' -100.64(18) . . . . ?
B9' B10' B12' B8' -36.80(16) . . . . ?
B9' B10' B12' B11' -137.92(17) . . . . ?
B10' B5' B6' C1' -133.94(16) . . . . ?
B10' B5' B6' C2' -100.25(17) . . . . ?
B10' B5' B6' B11' -38.49(16) . . . . ?
B10' B5' B9' B4' 137.87(17) . . . . ?
B10' B5' B9' B8' 100.26(18) . . . . ?
B10' B5' B9' B12' 36.81(16) . . . . ?
B10' B6' B11' C2' -134.26(17) . . . . ?
B10' B6' B11' B7' -99.88(18) . . . . ?
B10' B6' B11' B12' -36.28(16) . . . . ?
B10' B9' B12' B7' 100.93(18) . . . . ?
B10' B9' B12' B8' 138.68(18) . . . . ?
B10' B9' B12' B11' 37.83(16) . . . . ?
B10' B11' B12' B7' -138.17(17) . . . . ?
B10' B11' B12' B8' -100.74(18) . . . . ?
B10' B11' B12' B9' -37.60(16) . . . . ?
B11' C2' B3' C1' -102.81(16) . . . . ?
B11' C2' B3' B4' -68.73(19) . . . . ?
B11' C2' B3' B7' 35.89(16) . . . . ?
B11' C2' B3' B8' -4.9(2) . . . . ?
B11' C2' B6' C1' 139.01(17) . . . . ?
B11' C2' B6' B5' 104.43(17) . . . . ?
B11' C2' B6' B10' 40.63(15) . . . . ?
B11' C2' B7' B3' -141.59(17) . . . . ?
B11' C2' B7' B8' -102.50(17) . . . . ?
B11' C2' B7' B12' -40.38(15) . . . . ?
B11' B6' B10' B5' 137.95(17) . . . . ?
B11' B6' B10' B9' 100.76(18) . . . . ?
B11' B6' B10' B12' 36.69(16) . . . . ?
B11' B7' B8' B3' -101.93(18) . . . . ?
B11' B7' B8' B4' -63.9(2) . . . . ?
B11' B7' B8' B9' -0.6(2) . . . . ?
B11' B7' B8' B12' 37.29(16) . . . . ?
B11' B7' B12' B8' -138.37(17) . . . . ?
B11' B7' B12' B9' -100.94(18) . . . . ?
B11' B7' B12' B10' -37.60(16) . . . . ?
B11' B10' B12' B7' 37.27(15) . . . . ?
B11' B10' B12' B8' 101.12(18) . . . . ?
B11' B10' B12' B9' 137.92(17) . . . . ?
B12' B7' B8' B3' -139.22(18) . . . . ?
B12' B7' B8' B4' -101.15(19) . . . . ?
B12' B7' B8' B9' -37.88(16) . . . . ?
B12' B7' B11' C2' 133.94(16) . . . . ?
B12' B7' B11' B6' 99.28(18) . . . . ?
B12' B7' B11' B10' 37.28(15) . . . . ?
B12' B8' B9' B4' -138.17(18) . . . . ?
B12' B8' B9' B5' -100.71(18) . . . . ?
B12' B8' B9' B10' -36.79(16) . . . . ?
B12' B9' B10' B5' -138.80(17) . . . . ?
B12' B9' B10' B6' -101.55(18) . . . . ?
B12' B9' B10' B11' -37.53(15) . . . . ?
B12' B10' B11' C2' -99.30(17) . . . . ?
B12' B10' B11' B6' -139.10(17) . . . . ?
B12' B10' B11' B7' -37.46(16) . . . . ?

_shelx_SHELXL_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_pbca
_database_code_depnum_ccdc_archive 'CCDC 1527031'
_audit_update_record             
;
2017-01-12 deposited with the CCDC.
2017-03-07 downloaded from the CCDC.
;
# start Validation Reply Form
_vrf_CHEMW03_pbca                
;
PROBLEM: ALERT: The ratio of given/expected molecular weight as
RESPONSE: Disordered solvent in lattice removed using BYPASS - see Experimental section in paper
;
# Added during the CSD deposition process: Thursday 12 January 2017 09:58 AM
# end Validation Reply Form

_audit_creation_date             2016-05-10
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.02.19 svn.r3266 for OlexSys, GUI svn.r5155)
;
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C6 H25 Au B20 Cl P'
_chemical_formula_sum            'C7.25 H27.50 Au B20 Cl3.50 P'
_chemical_formula_weight         683.00
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           61
_space_group_name_H-M_alt        'P b c a'
_space_group_name_Hall           '-P 2ac 2ab'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'x+1/2, -y+1/2, -z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'-x-1/2, y-1/2, z'
'x, -y-1/2, z-1/2'

_cell_length_a                   10.4380(13)
_cell_length_b                   17.711(2)
_cell_length_c                   27.475(3)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     5079.3(10)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    6037
_cell_measurement_temperature    100.0(2)
_cell_measurement_theta_max      27.113
_cell_measurement_theta_min      2.383
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    6.224
_exptl_absorpt_correction_T_max  0.7455
_exptl_absorpt_correction_T_min  0.5097
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.1580 before and 0.0524 after correction.
The Ratio of minimum to maximum transmission is 0.6837.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            orange
_exptl_crystal_colour_primary    orange
_exptl_crystal_density_diffrn    1.786
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             2596
_exptl_crystal_recrystallization_method ?
_exptl_crystal_size_max          0.36
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.12
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0526
_diffrn_reflns_av_unetI/netI     0.0418
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            33633
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         27.243
_diffrn_reflns_theta_min         2.300
_diffrn_ambient_temperature      100.0(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_special_details          ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3880
_reflns_number_total             5651
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v7.68A (Bruker, 2009)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'XS (Sheldrick, 2008)'
_refine_diff_density_max         0.692
_refine_diff_density_min         -0.649
_refine_diff_density_rms         0.127
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.020
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     323
_refine_ls_number_reflns         5651
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0476
_refine_ls_R_factor_gt           0.0297
_refine_ls_restrained_S_all      1.020
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0211P)²+2.3996P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0585
_refine_ls_wR_factor_ref         0.0622
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 C11(H11A,H11B)
2.b Idealised Me refined as rotating group:
 C12(H12A,H12B,H12C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.15369(2) 0.50218(2) 0.53118(2) 0.01338(5) Uani 1 1 d . . . . .
C1 C 0.2593(4) 0.3284(2) 0.64496(14) 0.0140(9) Uani 1 1 d . . . . .
Cl1 Cl 0.08773(10) 0.62279(6) 0.51444(4) 0.0201(2) Uani 1 1 d . . . . .
P1 P 0.23084(10) 0.38839(6) 0.54784(4) 0.0123(2) Uani 1 1 d . . . . .
C2 C 0.1552(4) 0.3382(2) 0.59989(14) 0.0134(9) Uani 1 1 d . . . . .
B3 B 0.2117(5) 0.2473(3) 0.61202(18) 0.0181(11) Uani 1 1 d . . . . .
H3 H 0.272(4) 0.221(2) 0.5880(15) 0.022 Uiso 1 1 d R . . . .
B4 B 0.2311(5) 0.2459(3) 0.67634(19) 0.0215(12) Uani 1 1 d . . . . .
H4 H 0.321(4) 0.219(2) 0.6910(15) 0.026 Uiso 1 1 d R . . . .
B5 B 0.1837(5) 0.3359(3) 0.70069(18) 0.0223(12) Uani 1 1 d . . . . .
H5 H 0.239(4) 0.355(2) 0.7306(14) 0.027 Uiso 1 1 d R . . . .
B6 B 0.1335(5) 0.3938(3) 0.65125(17) 0.0176(11) Uani 1 1 d . . . . .
H6 H 0.143(4) 0.449(2) 0.6462(14) 0.021 Uiso 1 1 d R . . . .
B7 B 0.0490(5) 0.2641(3) 0.59797(19) 0.0205(11) Uani 1 1 d . . . . .
H7 H 0.012(4) 0.255(2) 0.5621(13) 0.025 Uiso 1 1 d R . . . .
B8 B 0.0939(5) 0.2042(3) 0.64778(19) 0.0226(12) Uani 1 1 d . . . . .
H8 H 0.083(4) 0.139(2) 0.6459(14) 0.027 Uiso 1 1 d R . . . .
B9 B 0.0771(5) 0.2569(3) 0.70225(19) 0.0242(12) Uani 1 1 d . . . . .
H9 H 0.043(4) 0.228(2) 0.7358(15) 0.029 Uiso 1 1 d R . . . .
B10 B 0.0186(5) 0.3489(3) 0.68618(16) 0.0198(11) Uani 1 1 d . . . . .
H10 H -0.045(4) 0.382(2) 0.7080(14) 0.024 Uiso 1 1 d R . . . .
B11 B 0.0011(5) 0.3526(3) 0.62141(17) 0.0191(11) Uani 1 1 d . . . . .
H11 H -0.055(4) 0.392(2) 0.6008(14) 0.023 Uiso 1 1 d R . . . .
C11 C 0.2411(4) 0.3211(2) 0.49810(13) 0.0105(8) Uani 1 1 d . . . . .
H11A H 0.3047 0.2816 0.5061 0.013 Uiso 1 1 calc R . . . .
H11B H 0.1569 0.2964 0.4935 0.013 Uiso 1 1 calc R . . . .
B12 B -0.0360(5) 0.2684(3) 0.65342(17) 0.0176(11) Uani 1 1 d . . . . .
H12 H -0.134(4) 0.242(2) 0.6587(14) 0.021 Uiso 1 1 d R . . . .
C12 C 0.2809(4) 0.3615(2) 0.45069(14) 0.0190(10) Uani 1 1 d . . . . .
H12A H 0.3646 0.3855 0.4553 0.028 Uiso 1 1 calc GR . . . .
H12B H 0.2170 0.4000 0.4425 0.028 Uiso 1 1 calc GR . . . .
H12C H 0.2863 0.3246 0.4242 0.028 Uiso 1 1 calc GR . . . .
C1' C 0.3913(4) 0.3611(2) 0.63171(13) 0.0125(9) Uani 1 1 d . . . . .
C2' C 0.3947(4) 0.3955(2) 0.57615(13) 0.0144(9) Uani 1 1 d . . . . .
B3' B 0.3992(5) 0.4607(3) 0.62315(17) 0.0149(10) Uani 1 1 d . . . . .
H3' H 0.314(4) 0.490(2) 0.6284(14) 0.018 Uiso 1 1 d R . . . .
B4' B 0.4886(5) 0.4137(3) 0.66942(17) 0.0182(11) Uani 1 1 d . . . . .
H4' H 0.458(4) 0.418(2) 0.6998(14) 0.022 Uiso 1 1 d R . . . .
B5' B 0.5385(5) 0.3226(3) 0.64744(18) 0.0173(11) Uani 1 1 d . . . . .
H5' H 0.538(4) 0.272(2) 0.6708(13) 0.021 Uiso 1 1 d R . . . .
B6' B 0.4773(5) 0.3114(3) 0.58710(16) 0.0136(10) Uani 1 1 d . . . . .
H6' H 0.440(3) 0.260(2) 0.5715(13) 0.016 Uiso 1 1 d R . . . .
B7' B 0.4947(4) 0.4717(3) 0.57128(18) 0.0152(10) Uani 1 1 d . . . . .
H7' H 0.456(4) 0.520(2) 0.5456(14) 0.018 Uiso 1 1 d R . . . .
B8' B 0.5575(5) 0.4845(3) 0.63116(17) 0.0162(11) Uani 1 1 d . . . . .
H8' H 0.587(4) 0.536(2) 0.6441(14) 0.019 Uiso 1 1 d R . . . .
B9' B 0.6453(5) 0.4007(3) 0.64609(17) 0.0191(11) Uani 1 1 d . . . . .
H9' H 0.736(4) 0.405(2) 0.6699(14) 0.023 Uiso 1 1 d R . . . .
B10' B 0.6370(4) 0.3383(3) 0.59543(18) 0.0165(11) Uani 1 1 d . . . . .
H10' H 0.702(4) 0.292(2) 0.5876(14) 0.020 Uiso 1 1 d R . . . .
B11' B 0.5438(5) 0.3834(3) 0.54924(19) 0.0176(11) Uani 1 1 d . . . . .
H11' H 0.547(4) 0.375(2) 0.5125(14) 0.021 Uiso 1 1 d R . . . .
B12' B 0.6495(5) 0.4366(3) 0.58566(18) 0.0192(11) Uani 1 1 d . . . . .
H12' H 0.741(4) 0.460(2) 0.5695(14) 0.023 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 Cl1 2.2910(11) . ?
Au1 P1 2.2181(11) . ?
C1 C2 1.656(5) . ?
C1 B3 1.769(6) . ?
C1 B4 1.722(6) . ?
C1 B5 1.727(6) . ?
C1 B6 1.759(6) . ?
C1 C1' 1.538(5) . ?
P1 C2 1.860(4) . ?
P1 C11 1.816(4) . ?
P1 C2' 1.883(4) . ?
C2 B3 1.746(6) . ?
C2 B6 1.736(6) . ?
C2 B7 1.718(6) . ?
C2 B11 1.732(6) . ?
B3 H3 1.02(4) . ?
B3 B4 1.779(7) . ?
B3 B7 1.766(7) . ?
B3 B8 1.749(7) . ?
B4 H4 1.13(4) . ?
B4 B5 1.798(8) . ?
B4 B8 1.792(7) . ?
B4 B9 1.769(7) . ?
B5 H5 1.06(4) . ?
B5 B6 1.781(7) . ?
B5 B9 1.789(8) . ?
B5 B10 1.785(7) . ?
B6 H6 0.99(4) . ?
B6 B10 1.730(7) . ?
B6 B11 1.765(7) . ?
B7 H7 1.07(4) . ?
B7 B8 1.794(7) . ?
B7 B11 1.766(7) . ?
B7 B12 1.765(7) . ?
B8 H8 1.15(4) . ?
B8 B9 1.772(7) . ?
B8 B12 1.776(7) . ?
B9 H9 1.11(4) . ?
B9 B10 1.796(8) . ?
B9 B12 1.798(7) . ?
B10 H10 1.07(4) . ?
B10 B11 1.790(7) . ?
B10 B12 1.780(7) . ?
B11 H11 1.07(4) . ?
B11 B12 1.773(7) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C11 C12 1.543(5) . ?
B12 H12 1.13(4) . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C1' C2' 1.644(5) . ?
C1' B3' 1.782(6) . ?
C1' B4' 1.724(6) . ?
C1' B5' 1.736(6) . ?
C1' B6' 1.755(6) . ?
C2' B3' 1.733(6) . ?
C2' B6' 1.747(6) . ?
C2' B7' 1.711(6) . ?
C2' B11' 1.736(6) . ?
B3' H3' 1.04(4) . ?
B3' B4' 1.784(7) . ?
B3' B7' 1.750(7) . ?
B3' B8' 1.719(7) . ?
B4' H4' 0.90(4) . ?
B4' B5' 1.799(7) . ?
B4' B8' 1.788(7) . ?
B4' B9' 1.772(7) . ?
B5' H5' 1.10(4) . ?
B5' B6' 1.788(7) . ?
B5' B9' 1.777(7) . ?
B5' B10' 1.782(7) . ?
B6' H6' 1.07(4) . ?
B6' B10' 1.748(7) . ?
B6' B11' 1.786(7) . ?
B7' H7' 1.17(4) . ?
B7' B8' 1.785(7) . ?
B7' B11' 1.754(7) . ?
B7' B12' 1.776(7) . ?
B8' H8' 1.03(4) . ?
B8' B9' 1.793(7) . ?
B8' B12' 1.790(7) . ?
B9' H9' 1.15(4) . ?
B9' B10' 1.780(7) . ?
B9' B12' 1.779(7) . ?
B10' H10' 1.08(4) . ?
B10' B11' 1.787(7) . ?
B10' B12' 1.767(7) . ?
B11' H11' 1.02(4) . ?
B11' B12' 1.762(7) . ?
B12' H12' 1.13(4) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Au1 Cl1 176.16(4) . . ?
C2 C1 B3 61.2(2) . . ?
C2 C1 B4 110.5(3) . . ?
C2 C1 B5 110.8(3) . . ?
C2 C1 B6 61.0(2) . . ?
B4 C1 B3 61.3(3) . . ?
B4 C1 B5 62.8(3) . . ?
B4 C1 B6 112.5(3) . . ?
B5 C1 B3 112.8(3) . . ?
B5 C1 B6 61.4(3) . . ?
B6 C1 B3 112.0(3) . . ?
C1' C1 C2 111.8(3) . . ?
C1' C1 B3 115.9(3) . . ?
C1' C1 B4 126.2(3) . . ?
C1' C1 B5 126.1(3) . . ?
C1' C1 B6 116.3(3) . . ?
C2 P1 Au1 116.03(13) . . ?
C2 P1 C2' 95.74(18) . . ?
C11 P1 Au1 117.53(13) . . ?
C11 P1 C2 106.86(18) . . ?
C11 P1 C2' 107.53(18) . . ?
C2' P1 Au1 110.73(13) . . ?
C1 C2 P1 110.3(3) . . ?
C1 C2 B3 62.6(2) . . ?
C1 C2 B6 62.4(2) . . ?
C1 C2 B7 111.5(3) . . ?
C1 C2 B11 111.7(3) . . ?
B3 C2 P1 116.4(3) . . ?
B6 C2 P1 114.2(3) . . ?
B6 C2 B3 114.3(3) . . ?
B7 C2 P1 128.0(3) . . ?
B7 C2 B3 61.3(3) . . ?
B7 C2 B6 112.0(3) . . ?
B7 C2 B11 61.6(3) . . ?
B11 C2 P1 125.9(3) . . ?
B11 C2 B3 112.6(3) . . ?
B11 C2 B6 61.2(3) . . ?
C1 B3 H3 122(2) . . ?
C1 B3 B4 58.1(3) . . ?
C2 B3 C1 56.2(2) . . ?
C2 B3 H3 120(2) . . ?
C2 B3 B4 103.9(3) . . ?
C2 B3 B7 58.6(3) . . ?
C2 B3 B8 105.8(4) . . ?
B4 B3 H3 124(2) . . ?
B7 B3 C1 104.2(3) . . ?
B7 B3 H3 122(2) . . ?
B7 B3 B4 109.2(4) . . ?
B8 B3 C1 105.3(3) . . ?
B8 B3 H3 126(2) . . ?
B8 B3 B4 61.1(3) . . ?
B8 B3 B7 61.4(3) . . ?
C1 B4 B3 60.7(3) . . ?
C1 B4 H4 113(2) . . ?
C1 B4 B5 58.7(3) . . ?
C1 B4 B8 105.5(3) . . ?
C1 B4 B9 105.3(4) . . ?
B3 B4 H4 117(2) . . ?
B3 B4 B5 109.0(4) . . ?
B3 B4 B8 58.7(3) . . ?
B5 B4 H4 118(2) . . ?
B8 B4 H4 130(2) . . ?
B8 B4 B5 108.0(4) . . ?
B9 B4 B3 107.1(4) . . ?
B9 B4 H4 131(2) . . ?
B9 B4 B5 60.2(3) . . ?
B9 B4 B8 59.7(3) . . ?
C1 B5 B4 58.4(3) . . ?
C1 B5 H5 118(2) . . ?
C1 B5 B6 60.2(3) . . ?
C1 B5 B9 104.2(4) . . ?
C1 B5 B10 104.7(3) . . ?
B4 B5 H5 115(2) . . ?
B6 B5 B4 107.9(4) . . ?
B6 B5 H5 125(2) . . ?
B6 B5 B9 106.6(4) . . ?
B6 B5 B10 58.0(3) . . ?
B9 B5 B4 59.1(3) . . ?
B9 B5 H5 125(2) . . ?
B10 B5 B4 107.3(4) . . ?
B10 B5 H5 131(2) . . ?
B10 B5 B9 60.4(3) . . ?
C1 B6 B5 58.4(3) . . ?
C1 B6 H6 124(2) . . ?
C1 B6 B11 105.4(3) . . ?
C2 B6 C1 56.6(2) . . ?
C2 B6 B5 104.8(3) . . ?
C2 B6 H6 116(2) . . ?
C2 B6 B11 59.3(3) . . ?
B5 B6 H6 130(2) . . ?
B10 B6 C1 105.7(4) . . ?
B10 B6 C2 106.3(4) . . ?
B10 B6 B5 61.1(3) . . ?
B10 B6 H6 127(2) . . ?
B10 B6 B11 61.6(3) . . ?
B11 B6 B5 110.3(4) . . ?
B11 B6 H6 115(2) . . ?
C2 B7 B3 60.1(3) . . ?
C2 B7 H7 112(2) . . ?
C2 B7 B8 105.1(4) . . ?
C2 B7 B11 59.6(3) . . ?
C2 B7 B12 105.4(3) . . ?
B3 B7 H7 121(2) . . ?
B3 B7 B8 58.8(3) . . ?
B8 B7 H7 135(2) . . ?
B11 B7 B3 110.0(4) . . ?
B11 B7 H7 112(2) . . ?
B11 B7 B8 108.7(4) . . ?
B12 B7 B3 107.6(4) . . ?
B12 B7 H7 128(2) . . ?
B12 B7 B8 59.9(3) . . ?
B12 B7 B11 60.3(3) . . ?
B3 B8 B4 60.3(3) . . ?
B3 B8 B7 59.8(3) . . ?
B3 B8 H8 119(2) . . ?
B3 B8 B9 108.3(4) . . ?
B3 B8 B12 107.8(4) . . ?
B4 B8 B7 107.4(4) . . ?
B4 B8 H8 120(2) . . ?
B7 B8 H8 122(2) . . ?
B9 B8 B4 59.5(3) . . ?
B9 B8 B7 107.9(4) . . ?
B9 B8 H8 123(2) . . ?
B9 B8 B12 60.9(3) . . ?
B12 B8 B4 107.9(4) . . ?
B12 B8 B7 59.2(3) . . ?
B12 B8 H8 125(2) . . ?
B4 B9 B5 60.7(3) . . ?
B4 B9 B8 60.8(3) . . ?
B4 B9 H9 125(2) . . ?
B4 B9 B10 108.1(4) . . ?
B4 B9 B12 108.0(4) . . ?
B5 B9 H9 125(2) . . ?
B5 B9 B10 59.7(3) . . ?
B5 B9 B12 107.5(4) . . ?
B8 B9 B5 109.3(4) . . ?
B8 B9 H9 119(2) . . ?
B8 B9 B10 107.7(4) . . ?
B8 B9 B12 59.7(3) . . ?
B10 B9 H9 121(2) . . ?
B10 B9 B12 59.4(3) . . ?
B12 B9 H9 118(2) . . ?
B5 B10 B9 59.9(3) . . ?
B5 B10 H10 123(2) . . ?
B5 B10 B11 109.0(3) . . ?
B6 B10 B5 60.9(3) . . ?
B6 B10 B9 108.5(4) . . ?
B6 B10 H10 119(2) . . ?
B6 B10 B11 60.2(3) . . ?
B6 B10 B12 108.0(3) . . ?
B9 B10 H10 125(2) . . ?
B11 B10 B9 108.1(4) . . ?
B11 B10 H10 118(2) . . ?
B12 B10 B5 108.6(4) . . ?
B12 B10 B9 60.4(3) . . ?
B12 B10 H10 122(2) . . ?
B12 B10 B11 59.6(3) . . ?
C2 B11 B6 59.5(3) . . ?
C2 B11 B7 58.8(3) . . ?
C2 B11 B10 103.9(3) . . ?
C2 B11 H11 115(2) . . ?
C2 B11 B12 104.4(3) . . ?
B6 B11 B7 108.3(4) . . ?
B6 B11 B10 58.2(3) . . ?
B6 B11 H11 114(2) . . ?
B6 B11 B12 106.8(4) . . ?
B7 B11 B10 107.6(4) . . ?
B7 B11 H11 123(2) . . ?
B7 B11 B12 59.8(3) . . ?
B10 B11 H11 127(2) . . ?
B12 B11 B10 59.9(3) . . ?
B12 B11 H11 134(2) . . ?
P1 C11 H11A 109.6 . . ?
P1 C11 H11B 109.6 . . ?
H11A C11 H11B 108.1 . . ?
C12 C11 P1 110.3(3) . . ?
C12 C11 H11A 109.6 . . ?
C12 C11 H11B 109.6 . . ?
B7 B12 B8 60.9(3) . . ?
B7 B12 B9 108.0(4) . . ?
B7 B12 B10 108.1(3) . . ?
B7 B12 B11 59.9(3) . . ?
B7 B12 H12 123(2) . . ?
B8 B12 B9 59.4(3) . . ?
B8 B12 B10 108.3(4) . . ?
B8 B12 H12 116(2) . . ?
B9 B12 H12 117(2) . . ?
B10 B12 B9 60.3(3) . . ?
B10 B12 H12 123(2) . . ?
B11 B12 B8 109.2(3) . . ?
B11 B12 B9 108.8(4) . . ?
B11 B12 B10 60.5(3) . . ?
B11 B12 H12 127(2) . . ?
C11 C12 H12A 109.5 . . ?
C11 C12 H12B 109.5 . . ?
C11 C12 H12C 109.5 . . ?
H12A C12 H12B 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C1 C1' C2' 112.3(3) . . ?
C1 C1' B3' 116.5(3) . . ?
C1 C1' B4' 126.1(3) . . ?
C1 C1' B5' 125.9(3) . . ?
C1 C1' B6' 115.7(3) . . ?
C2' C1' B3' 60.6(2) . . ?
C2' C1' B4' 110.2(3) . . ?
C2' C1' B5' 110.9(3) . . ?
C2' C1' B6' 61.7(2) . . ?
B4' C1' B3' 61.2(3) . . ?
B4' C1' B5' 62.7(3) . . ?
B4' C1' B6' 112.9(3) . . ?
B5' C1' B3' 112.4(3) . . ?
B5' C1' B6' 61.6(3) . . ?
B6' C1' B3' 112.4(3) . . ?
C1' C2' P1 109.8(3) . . ?
C1' C2' B3' 63.6(2) . . ?
C1' C2' B6' 62.3(2) . . ?
C1' C2' B7' 112.2(3) . . ?
C1' C2' B11' 111.7(3) . . ?
B3' C2' P1 112.1(3) . . ?
B3' C2' B6' 115.3(3) . . ?
B3' C2' B11' 112.1(3) . . ?
B6' C2' P1 117.5(3) . . ?
B7' C2' P1 125.1(3) . . ?
B7' C2' B3' 61.1(3) . . ?
B7' C2' B6' 112.7(3) . . ?
B7' C2' B11' 61.2(3) . . ?
B11' C2' P1 129.1(3) . . ?
B11' C2' B6' 61.7(3) . . ?
C1' B3' H3' 116(2) . . ?
C1' B3' B4' 57.8(3) . . ?
C2' B3' C1' 55.7(2) . . ?
C2' B3' H3' 114(2) . . ?
C2' B3' B4' 103.5(3) . . ?
C2' B3' B7' 58.9(3) . . ?
B4' B3' H3' 125(2) . . ?
B7' B3' C1' 104.1(3) . . ?
B7' B3' H3' 123(2) . . ?
B7' B3' B4' 109.5(4) . . ?
B8' B3' C1' 105.7(3) . . ?
B8' B3' C2' 106.5(3) . . ?
B8' B3' H3' 133(2) . . ?
B8' B3' B4' 61.4(3) . . ?
B8' B3' B7' 61.9(3) . . ?
C1' B4' B3' 61.0(3) . . ?
C1' B4' H4' 113(3) . . ?
C1' B4' B5' 59.0(3) . . ?
C1' B4' B8' 105.2(3) . . ?
C1' B4' B9' 104.9(3) . . ?
B3' B4' H4' 116(3) . . ?
B3' B4' B5' 109.3(3) . . ?
B3' B4' B8' 57.5(3) . . ?
B5' B4' H4' 119(3) . . ?
B8' B4' H4' 129(3) . . ?
B8' B4' B5' 108.4(3) . . ?
B9' B4' B3' 106.6(3) . . ?
B9' B4' H4' 132(3) . . ?
B9' B4' B5' 59.7(3) . . ?
B9' B4' B8' 60.5(3) . . ?
C1' B5' B4' 58.3(3) . . ?
C1' B5' H5' 118(2) . . ?
C1' B5' B6' 59.7(2) . . ?
C1' B5' B9' 104.2(3) . . ?
C1' B5' B10' 104.5(3) . . ?
B4' B5' H5' 122(2) . . ?
B6' B5' B4' 107.9(3) . . ?
B6' B5' H5' 117(2) . . ?
B9' B5' B4' 59.4(3) . . ?
B9' B5' H5' 130(2) . . ?
B9' B5' B6' 107.0(3) . . ?
B9' B5' B10' 60.0(3) . . ?
B10' B5' B4' 107.3(3) . . ?
B10' B5' H5' 127(2) . . ?
B10' B5' B6' 58.7(3) . . ?
C1' B6' B5' 58.7(2) . . ?
C1' B6' H6' 121(2) . . ?
C1' B6' B11' 104.3(3) . . ?
C2' B6' C1' 56.0(2) . . ?
C2' B6' B5' 104.0(3) . . ?
C2' B6' H6' 118(2) . . ?
C2' B6' B10' 105.1(3) . . ?
C2' B6' B11' 58.9(3) . . ?
B5' B6' H6' 126(2) . . ?
B10' B6' C1' 105.1(3) . . ?
B10' B6' B5' 60.5(3) . . ?
B10' B6' H6' 129(2) . . ?
B10' B6' B11' 60.7(3) . . ?
B11' B6' B5' 108.8(3) . . ?
B11' B6' H6' 120.6(19) . . ?
C2' B7' B3' 60.1(3) . . ?
C2' B7' H7' 114.1(19) . . ?
C2' B7' B8' 104.6(3) . . ?
C2' B7' B11' 60.1(3) . . ?
C2' B7' B12' 105.1(3) . . ?
B3' B7' H7' 112(2) . . ?
B3' B7' B8' 58.2(3) . . ?
B3' B7' B11' 110.4(4) . . ?
B3' B7' B12' 107.4(4) . . ?
B8' B7' H7' 126(2) . . ?
B11' B7' H7' 122(2) . . ?
B11' B7' B8' 108.9(3) . . ?
B11' B7' B12' 59.9(3) . . ?
B12' B7' H7' 134(2) . . ?
B12' B7' B8' 60.4(3) . . ?
B3' B8' B4' 61.1(3) . . ?
B3' B8' B7' 59.9(3) . . ?
B3' B8' H8' 123(2) . . ?
B3' B8' B9' 108.5(3) . . ?
B3' B8' B12' 108.1(3) . . ?
B4' B8' H8' 123(2) . . ?
B4' B8' B9' 59.3(3) . . ?
B4' B8' B12' 107.1(3) . . ?
B7' B8' B4' 107.8(3) . . ?
B7' B8' H8' 123(2) . . ?
B7' B8' B9' 107.1(3) . . ?
B7' B8' B12' 59.6(3) . . ?
B9' B8' H8' 120(2) . . ?
B12' B8' H8' 120(2) . . ?
B12' B8' B9' 59.5(3) . . ?
B4' B9' B5' 60.9(3) . . ?
B4' B9' B8' 60.2(3) . . ?
B4' B9' H9' 122.9(19) . . ?
B4' B9' B10' 108.5(3) . . ?
B4' B9' B12' 108.3(4) . . ?
B5' B9' B8' 109.2(3) . . ?
B5' B9' H9' 124(2) . . ?
B5' B9' B10' 60.1(3) . . ?
B5' B9' B12' 108.2(3) . . ?
B8' B9' H9' 120(2) . . ?
B10' B9' B8' 108.1(3) . . ?
B10' B9' H9' 122(2) . . ?
B12' B9' B8' 60.2(3) . . ?
B12' B9' H9' 119(2) . . ?
B12' B9' B10' 59.6(3) . . ?
B5' B10' H10' 114(2) . . ?
B5' B10' B11' 109.0(3) . . ?
B6' B10' B5' 60.8(3) . . ?
B6' B10' B9' 108.6(3) . . ?
B6' B10' H10' 112(2) . . ?
B6' B10' B11' 60.7(3) . . ?
B6' B10' B12' 108.6(3) . . ?
B9' B10' B5' 59.9(3) . . ?
B9' B10' H10' 126(2) . . ?
B9' B10' B11' 107.7(3) . . ?
B11' B10' H10' 123(2) . . ?
B12' B10' B5' 108.5(4) . . ?
B12' B10' B9' 60.2(3) . . ?
B12' B10' H10' 132(2) . . ?
B12' B10' B11' 59.4(3) . . ?
C2' B11' B6' 59.4(3) . . ?
C2' B11' B7' 58.7(3) . . ?
C2' B11' B10' 103.9(3) . . ?
C2' B11' H11' 118(2) . . ?
C2' B11' B12' 104.7(3) . . ?
B6' B11' B10' 58.6(3) . . ?
B6' B11' H11' 118(2) . . ?
B7' B11' B6' 108.8(3) . . ?
B7' B11' B10' 108.2(4) . . ?
B7' B11' H11' 119(2) . . ?
B7' B11' B12' 60.7(3) . . ?
B10' B11' H11' 128(2) . . ?
B12' B11' B6' 107.1(3) . . ?
B12' B11' B10' 59.7(3) . . ?
B12' B11' H11' 129(2) . . ?
B7' B12' B8' 60.1(3) . . ?
B7' B12' B9' 108.1(4) . . ?
B7' B12' H12' 123(2) . . ?
B8' B12' H12' 124(2) . . ?
B9' B12' B8' 60.3(3) . . ?
B9' B12' H12' 121(2) . . ?
B10' B12' B7' 108.2(4) . . ?
B10' B12' B8' 108.7(4) . . ?
B10' B12' B9' 60.3(3) . . ?
B10' B12' H12' 119(2) . . ?
B11' B12' B7' 59.4(3) . . ?
B11' B12' B8' 108.3(4) . . ?
B11' B12' B9' 108.9(4) . . ?
B11' B12' B10' 60.9(3) . . ?
B11' B12' H12' 120(2) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au1 P1 C2 C1 -113.4(2) . . . . ?
Au1 P1 C2 B3 178.0(2) . . . . ?
Au1 P1 C2 B6 -45.5(3) . . . . ?
Au1 P1 C2 B7 105.0(3) . . . . ?
Au1 P1 C2 B11 25.4(4) . . . . ?
Au1 P1 C11 C12 37.7(3) . . . . ?
Au1 P1 C2' C1' 117.1(2) . . . . ?
Au1 P1 C2' B3' 48.4(3) . . . . ?
Au1 P1 C2' B6' -174.6(2) . . . . ?
Au1 P1 C2' B7' -21.0(4) . . . . ?
Au1 P1 C2' B11' -100.0(3) . . . . ?
C1 C2 B3 B4 34.8(3) . . . . ?
C1 C2 B3 B7 139.0(3) . . . . ?
C1 C2 B3 B8 98.1(4) . . . . ?
C1 C2 B6 B5 -34.6(3) . . . . ?
C1 C2 B6 B10 -98.3(4) . . . . ?
C1 C2 B6 B11 -139.7(3) . . . . ?
C1 C2 B7 B3 -38.8(3) . . . . ?
C1 C2 B7 B8 0.7(4) . . . . ?
C1 C2 B7 B11 103.8(4) . . . . ?
C1 C2 B7 B12 62.9(4) . . . . ?
C1 C2 B11 B6 38.1(3) . . . . ?
C1 C2 B11 B7 -103.5(4) . . . . ?
C1 C2 B11 B10 -1.1(4) . . . . ?
C1 C2 B11 B12 -63.1(4) . . . . ?
C1 B3 B4 B5 34.6(3) . . . . ?
C1 B3 B4 B8 134.5(4) . . . . ?
C1 B3 B4 B9 98.2(4) . . . . ?
C1 B3 B7 C2 34.2(3) . . . . ?
C1 B3 B7 B8 -100.0(4) . . . . ?
C1 B3 B7 B11 0.3(5) . . . . ?
C1 B3 B7 B12 -63.7(4) . . . . ?
C1 B3 B8 B4 -38.9(3) . . . . ?
C1 B3 B8 B7 98.0(4) . . . . ?
C1 B3 B8 B9 -2.4(5) . . . . ?
C1 B3 B8 B12 62.0(4) . . . . ?
C1 B4 B5 B6 35.7(3) . . . . ?
C1 B4 B5 B9 134.7(4) . . . . ?
C1 B4 B5 B10 96.9(3) . . . . ?
C1 B4 B8 B3 40.2(3) . . . . ?
C1 B4 B8 B7 2.0(5) . . . . ?
C1 B4 B8 B9 -98.9(4) . . . . ?
C1 B4 B8 B12 -60.5(4) . . . . ?
C1 B4 B9 B5 -39.0(3) . . . . ?
C1 B4 B9 B8 99.3(4) . . . . ?
C1 B4 B9 B10 -1.3(5) . . . . ?
C1 B4 B9 B12 61.4(4) . . . . ?
C1 B5 B6 C2 33.8(3) . . . . ?
C1 B5 B6 B10 134.6(4) . . . . ?
C1 B5 B6 B11 96.1(4) . . . . ?
C1 B5 B9 B4 38.7(3) . . . . ?
C1 B5 B9 B8 0.7(5) . . . . ?
C1 B5 B9 B10 -99.0(4) . . . . ?
C1 B5 B9 B12 -62.5(4) . . . . ?
C1 B5 B10 B6 -39.7(3) . . . . ?
C1 B5 B10 B9 98.2(4) . . . . ?
C1 B5 B10 B11 -2.3(5) . . . . ?
C1 B5 B10 B12 61.0(4) . . . . ?
C1 B6 B10 B5 39.1(3) . . . . ?
C1 B6 B10 B9 1.4(4) . . . . ?
C1 B6 B10 B11 -99.4(4) . . . . ?
C1 B6 B10 B12 -62.6(4) . . . . ?
C1 B6 B11 C2 -34.1(3) . . . . ?
C1 B6 B11 B7 0.0(4) . . . . ?
C1 B6 B11 B10 99.7(4) . . . . ?
C1 B6 B11 B12 63.0(4) . . . . ?
C1 C1' C2' P1 3.2(4) . . . . ?
C1 C1' C2' B3' 108.8(4) . . . . ?
C1 C1' C2' B6' -108.2(3) . . . . ?
C1 C1' C2' B7' 147.0(3) . . . . ?
C1 C1' C2' B11' -146.5(3) . . . . ?
C1 C1' B3' C2' -101.9(3) . . . . ?
C1 C1' B3' B4' 118.5(4) . . . . ?
C1 C1' B3' B7' -137.1(3) . . . . ?
C1 C1' B3' B8' 158.6(3) . . . . ?
C1 C1' B4' B3' -103.2(4) . . . . ?
C1 C1' B4' B5' 116.1(4) . . . . ?
C1 C1' B4' B8' -141.4(4) . . . . ?
C1 C1' B4' B9' 155.8(4) . . . . ?
C1 C1' B5' B4' -116.4(4) . . . . ?
C1 C1' B5' B6' 102.6(4) . . . . ?
C1 C1' B5' B9' -155.8(3) . . . . ?
C1 C1' B5' B10' 142.0(4) . . . . ?
C1 C1' B6' C2' 102.6(4) . . . . ?
C1 C1' B6' B5' -118.6(4) . . . . ?
C1 C1' B6' B10' -159.1(3) . . . . ?
C1 C1' B6' B11' 137.9(3) . . . . ?
P1 C2 B3 C1 100.3(3) . . . . ?
P1 C2 B3 B4 135.0(3) . . . . ?
P1 C2 B3 B7 -120.8(3) . . . . ?
P1 C2 B3 B8 -161.6(3) . . . . ?
P1 C2 B6 C1 -101.2(3) . . . . ?
P1 C2 B6 B5 -135.8(3) . . . . ?
P1 C2 B6 B10 160.6(3) . . . . ?
P1 C2 B6 B11 119.1(3) . . . . ?
P1 C2 B7 B3 102.4(4) . . . . ?
P1 C2 B7 B8 141.8(3) . . . . ?
P1 C2 B7 B11 -115.0(4) . . . . ?
P1 C2 B7 B12 -155.9(3) . . . . ?
P1 C2 B11 B6 -100.3(4) . . . . ?
P1 C2 B11 B7 118.1(4) . . . . ?
P1 C2 B11 B10 -139.5(3) . . . . ?
P1 C2 B11 B12 158.5(3) . . . . ?
P1 C2' B3' C1' 101.9(3) . . . . ?
P1 C2' B3' B4' 136.2(3) . . . . ?
P1 C2' B3' B7' -118.9(3) . . . . ?
P1 C2' B3' B8' -160.1(3) . . . . ?
P1 C2' B6' C1' -99.1(3) . . . . ?
P1 C2' B6' B5' -134.5(3) . . . . ?
P1 C2' B6' B10' 162.8(3) . . . . ?
P1 C2' B6' B11' 121.8(3) . . . . ?
P1 C2' B7' B3' 97.9(4) . . . . ?
P1 C2' B7' B8' 136.8(3) . . . . ?
P1 C2' B7' B11' -119.5(3) . . . . ?
P1 C2' B7' B12' -160.5(3) . . . . ?
P1 C2' B11' B6' -103.8(4) . . . . ?
P1 C2' B11' B7' 113.4(4) . . . . ?
P1 C2' B11' B10' -143.5(3) . . . . ?
P1 C2' B11' B12' 154.7(3) . . . . ?
C2 C1 B3 B4 -139.3(3) . . . . ?
C2 C1 B3 B7 -35.3(3) . . . . ?
C2 C1 B3 B8 -99.0(4) . . . . ?
C2 C1 B4 B3 37.6(3) . . . . ?
C2 C1 B4 B5 -103.5(4) . . . . ?
C2 C1 B4 B8 -1.6(4) . . . . ?
C2 C1 B4 B9 -63.8(4) . . . . ?
C2 C1 B5 B4 103.1(3) . . . . ?
C2 C1 B5 B6 -37.1(3) . . . . ?
C2 C1 B5 B9 64.1(4) . . . . ?
C2 C1 B5 B10 1.6(5) . . . . ?
C2 C1 B6 B5 139.8(4) . . . . ?
C2 C1 B6 B10 99.5(4) . . . . ?
C2 C1 B6 B11 35.2(3) . . . . ?
C2 C1 C1' C2' -1.1(4) . . . . ?
C2 C1 C1' B3' 66.1(4) . . . . ?
C2 C1 C1' B4' 138.4(4) . . . . ?
C2 C1 C1' B5' -141.7(4) . . . . ?
C2 C1 C1' B6' -69.3(4) . . . . ?
C2 P1 C11 C12 170.2(3) . . . . ?
C2 P1 C2' C1' -3.6(3) . . . . ?
C2 P1 C2' B3' -72.3(3) . . . . ?
C2 P1 C2' B6' 64.7(3) . . . . ?
C2 P1 C2' B7' -141.6(3) . . . . ?
C2 P1 C2' B11' 139.3(3) . . . . ?
C2 B3 B4 C1 -33.9(3) . . . . ?
C2 B3 B4 B5 0.6(4) . . . . ?
C2 B3 B4 B8 100.6(4) . . . . ?
C2 B3 B4 B9 64.3(4) . . . . ?
C2 B3 B7 B8 -134.2(4) . . . . ?
C2 B3 B7 B11 -33.9(3) . . . . ?
C2 B3 B7 B12 -98.0(4) . . . . ?
C2 B3 B8 B4 -97.5(4) . . . . ?
C2 B3 B8 B7 39.5(3) . . . . ?
C2 B3 B8 B9 -61.0(4) . . . . ?
C2 B3 B8 B12 3.4(4) . . . . ?
C2 B6 B10 B5 98.1(4) . . . . ?
C2 B6 B10 B9 60.4(4) . . . . ?
C2 B6 B10 B11 -40.3(3) . . . . ?
C2 B6 B10 B12 -3.5(5) . . . . ?
C2 B6 B11 B7 34.1(3) . . . . ?
C2 B6 B11 B10 133.8(4) . . . . ?
C2 B6 B11 B12 97.1(4) . . . . ?
C2 B7 B8 B3 -40.1(3) . . . . ?
C2 B7 B8 B4 -1.6(4) . . . . ?
C2 B7 B8 B9 61.1(4) . . . . ?
C2 B7 B8 B12 99.3(4) . . . . ?
C2 B7 B11 B6 -34.3(3) . . . . ?
C2 B7 B11 B10 -95.9(4) . . . . ?
C2 B7 B11 B12 -133.5(4) . . . . ?
C2 B7 B12 B8 -98.8(4) . . . . ?
C2 B7 B12 B9 -61.2(4) . . . . ?
C2 B7 B12 B10 2.5(5) . . . . ?
C2 B7 B12 B11 40.5(3) . . . . ?
C2 B11 B12 B7 -39.9(3) . . . . ?
C2 B11 B12 B8 -2.7(4) . . . . ?
C2 B11 B12 B9 60.5(4) . . . . ?
C2 B11 B12 B10 97.9(4) . . . . ?
B3 C1 C2 P1 -110.0(3) . . . . ?
B3 C1 C2 B6 142.6(3) . . . . ?
B3 C1 C2 B7 38.2(3) . . . . ?
B3 C1 C2 B11 105.0(4) . . . . ?
B3 C1 B4 B5 -141.1(4) . . . . ?
B3 C1 B4 B8 -39.2(3) . . . . ?
B3 C1 B4 B9 -101.4(4) . . . . ?
B3 C1 B5 B4 36.7(3) . . . . ?
B3 C1 B5 B6 -103.5(4) . . . . ?
B3 C1 B5 B9 -2.3(5) . . . . ?
B3 C1 B5 B10 -64.9(4) . . . . ?
B3 C1 B6 C2 -35.0(3) . . . . ?
B3 C1 B6 B5 104.8(4) . . . . ?
B3 C1 B6 B10 64.4(4) . . . . ?
B3 C1 B6 B11 0.2(4) . . . . ?
B3 C1 C1' C2' 66.4(4) . . . . ?
B3 C1 C1' B3' 133.6(3) . . . . ?
B3 C1 C1' B4' -154.2(4) . . . . ?
B3 C1 C1' B5' -74.2(5) . . . . ?
B3 C1 C1' B6' -1.8(5) . . . . ?
B3 C2 B6 C1 36.3(3) . . . . ?
B3 C2 B6 B5 1.7(5) . . . . ?
B3 C2 B6 B10 -62.0(4) . . . . ?
B3 C2 B6 B11 -103.4(4) . . . . ?
B3 C2 B7 B8 39.4(3) . . . . ?
B3 C2 B7 B11 142.5(4) . . . . ?
B3 C2 B7 B12 101.7(4) . . . . ?
B3 C2 B11 B6 106.3(4) . . . . ?
B3 C2 B11 B7 -35.3(3) . . . . ?
B3 C2 B11 B10 67.1(4) . . . . ?
B3 C2 B11 B12 5.1(4) . . . . ?
B3 B4 B5 C1 -35.4(3) . . . . ?
B3 B4 B5 B6 0.3(5) . . . . ?
B3 B4 B5 B9 99.3(4) . . . . ?
B3 B4 B5 B10 61.5(4) . . . . ?
B3 B4 B8 B7 -38.2(3) . . . . ?
B3 B4 B8 B9 -139.1(4) . . . . ?
B3 B4 B8 B12 -100.7(4) . . . . ?
B3 B4 B9 B5 -102.5(4) . . . . ?
B3 B4 B9 B8 35.8(3) . . . . ?
B3 B4 B9 B10 -64.8(4) . . . . ?
B3 B4 B9 B12 -2.0(5) . . . . ?
B3 B7 B8 B4 38.4(3) . . . . ?
B3 B7 B8 B9 101.2(4) . . . . ?
B3 B7 B8 B12 139.3(4) . . . . ?
B3 B7 B11 C2 34.1(3) . . . . ?
B3 B7 B11 B6 -0.2(5) . . . . ?
B3 B7 B11 B10 -61.7(4) . . . . ?
B3 B7 B11 B12 -99.3(4) . . . . ?
B3 B7 B12 B8 -35.8(3) . . . . ?
B3 B7 B12 B9 1.7(5) . . . . ?
B3 B7 B12 B10 65.5(4) . . . . ?
B3 B7 B12 B11 103.4(4) . . . . ?
B3 B8 B9 B4 -36.8(3) . . . . ?
B3 B8 B9 B5 1.1(5) . . . . ?
B3 B8 B9 B10 64.4(5) . . . . ?
B3 B8 B9 B12 100.6(4) . . . . ?
B3 B8 B12 B7 36.3(3) . . . . ?
B3 B8 B12 B9 -101.5(4) . . . . ?
B3 B8 B12 B10 -64.7(4) . . . . ?
B3 B8 B12 B11 -0.4(5) . . . . ?
B4 C1 C2 P1 -147.6(3) . . . . ?
B4 C1 C2 B3 -37.6(3) . . . . ?
B4 C1 C2 B6 105.0(4) . . . . ?
B4 C1 C2 B7 0.6(4) . . . . ?
B4 C1 C2 B11 67.4(4) . . . . ?
B4 C1 B3 C2 139.3(3) . . . . ?
B4 C1 B3 B7 104.0(4) . . . . ?
B4 C1 B3 B8 40.3(3) . . . . ?
B4 C1 B5 B6 -140.2(4) . . . . ?
B4 C1 B5 B9 -39.0(3) . . . . ?
B4 C1 B5 B10 -101.5(4) . . . . ?
B4 C1 B6 C2 -101.8(3) . . . . ?
B4 C1 B6 B5 38.0(4) . . . . ?
B4 C1 B6 B10 -2.3(4) . . . . ?
B4 C1 B6 B11 -66.6(4) . . . . ?
B4 C1 C1' C2' 138.5(4) . . . . ?
B4 C1 C1' B3' -154.3(4) . . . . ?
B4 C1 C1' B4' -82.1(5) . . . . ?
B4 C1 C1' B5' -2.1(6) . . . . ?
B4 C1 C1' B6' 70.3(5) . . . . ?
B4 B3 B7 C2 94.9(3) . . . . ?
B4 B3 B7 B8 -39.3(3) . . . . ?
B4 B3 B7 B11 61.0(4) . . . . ?
B4 B3 B7 B12 -3.0(5) . . . . ?
B4 B3 B8 B7 136.9(4) . . . . ?
B4 B3 B8 B9 36.5(3) . . . . ?
B4 B3 B8 B12 100.9(4) . . . . ?
B4 B5 B6 C1 -35.0(3) . . . . ?
B4 B5 B6 C2 -1.2(4) . . . . ?
B4 B5 B6 B10 99.6(4) . . . . ?
B4 B5 B6 B11 61.1(4) . . . . ?
B4 B5 B9 B8 -38.0(4) . . . . ?
B4 B5 B9 B10 -137.7(4) . . . . ?
B4 B5 B9 B12 -101.2(4) . . . . ?
B4 B5 B10 B6 -100.7(4) . . . . ?
B4 B5 B10 B9 37.2(3) . . . . ?
B4 B5 B10 B11 -63.2(4) . . . . ?
B4 B5 B10 B12 0.0(4) . . . . ?
B4 B8 B9 B5 37.9(4) . . . . ?
B4 B8 B9 B10 101.2(4) . . . . ?
B4 B8 B9 B12 137.4(4) . . . . ?
B4 B8 B12 B7 100.0(4) . . . . ?
B4 B8 B12 B9 -37.8(3) . . . . ?
B4 B8 B12 B10 -1.0(4) . . . . ?
B4 B8 B12 B11 63.2(4) . . . . ?
B4 B9 B10 B5 -38.1(3) . . . . ?
B4 B9 B10 B6 0.0(5) . . . . ?
B4 B9 B10 B11 63.7(4) . . . . ?
B4 B9 B10 B12 100.6(4) . . . . ?
B4 B9 B12 B7 0.2(5) . . . . ?
B4 B9 B12 B8 38.4(3) . . . . ?
B4 B9 B12 B10 -100.7(4) . . . . ?
B4 B9 B12 B11 -63.3(4) . . . . ?
B5 C1 C2 P1 144.7(3) . . . . ?
B5 C1 C2 B3 -105.3(4) . . . . ?
B5 C1 C2 B6 37.3(3) . . . . ?
B5 C1 C2 B7 -67.1(4) . . . . ?
B5 C1 C2 B11 -0.3(4) . . . . ?
B5 C1 B3 C2 102.0(4) . . . . ?
B5 C1 B3 B4 -37.3(3) . . . . ?
B5 C1 B3 B7 66.7(4) . . . . ?
B5 C1 B3 B8 3.0(5) . . . . ?
B5 C1 B4 B3 141.1(4) . . . . ?
B5 C1 B4 B8 101.9(4) . . . . ?
B5 C1 B4 B9 39.8(3) . . . . ?
B5 C1 B6 C2 -139.8(4) . . . . ?
B5 C1 B6 B10 -40.4(3) . . . . ?
B5 C1 B6 B11 -104.6(4) . . . . ?
B5 C1 C1' C2' -141.0(4) . . . . ?
B5 C1 C1' B3' -73.9(5) . . . . ?
B5 C1 C1' B4' -1.6(6) . . . . ?
B5 C1 C1' B5' 78.4(5) . . . . ?
B5 C1 C1' B6' 150.7(4) . . . . ?
B5 B4 B8 B3 101.7(4) . . . . ?
B5 B4 B8 B7 63.5(4) . . . . ?
B5 B4 B8 B9 -37.4(3) . . . . ?
B5 B4 B8 B12 1.0(4) . . . . ?
B5 B4 B9 B8 138.3(4) . . . . ?
B5 B4 B9 B10 37.7(3) . . . . ?
B5 B4 B9 B12 100.4(4) . . . . ?
B5 B6 B10 B9 -37.7(3) . . . . ?
B5 B6 B10 B11 -138.5(4) . . . . ?
B5 B6 B10 B12 -101.6(4) . . . . ?
B5 B6 B11 C2 -95.5(4) . . . . ?
B5 B6 B11 B7 -61.5(4) . . . . ?
B5 B6 B11 B10 38.2(3) . . . . ?
B5 B6 B11 B12 1.6(4) . . . . ?
B5 B9 B10 B6 38.1(3) . . . . ?
B5 B9 B10 B11 101.9(4) . . . . ?
B5 B9 B10 B12 138.8(4) . . . . ?
B5 B9 B12 B7 64.3(4) . . . . ?
B5 B9 B12 B8 102.5(4) . . . . ?
B5 B9 B12 B10 -36.7(3) . . . . ?
B5 B9 B12 B11 0.8(5) . . . . ?
B5 B10 B11 C2 2.1(4) . . . . ?
B5 B10 B11 B6 -37.8(3) . . . . ?
B5 B10 B11 B7 63.3(4) . . . . ?
B5 B10 B11 B12 100.9(4) . . . . ?
B5 B10 B12 B7 -63.9(4) . . . . ?
B5 B10 B12 B8 0.6(4) . . . . ?
B5 B10 B12 B9 37.0(3) . . . . ?
B5 B10 B12 B11 -101.6(4) . . . . ?
B6 C1 C2 P1 107.4(3) . . . . ?
B6 C1 C2 B3 -142.6(3) . . . . ?
B6 C1 C2 B7 -104.4(4) . . . . ?
B6 C1 C2 B11 -37.6(3) . . . . ?
B6 C1 B3 C2 35.0(3) . . . . ?
B6 C1 B3 B4 -104.4(4) . . . . ?
B6 C1 B3 B7 -0.3(4) . . . . ?
B6 C1 B3 B8 -64.0(4) . . . . ?
B6 C1 B4 B3 103.7(4) . . . . ?
B6 C1 B4 B5 -37.5(3) . . . . ?
B6 C1 B4 B8 64.5(4) . . . . ?
B6 C1 B4 B9 2.3(4) . . . . ?
B6 C1 B5 B4 140.2(4) . . . . ?
B6 C1 B5 B9 101.2(4) . . . . ?
B6 C1 B5 B10 38.7(3) . . . . ?
B6 C1 C1' C2' -68.4(4) . . . . ?
B6 C1 C1' B3' -1.3(5) . . . . ?
B6 C1 C1' B4' 71.0(5) . . . . ?
B6 C1 C1' B5' 150.9(4) . . . . ?
B6 C1 C1' B6' -136.7(3) . . . . ?
B6 C2 B3 C1 -36.2(3) . . . . ?
B6 C2 B3 B4 -1.5(4) . . . . ?
B6 C2 B3 B7 102.8(4) . . . . ?
B6 C2 B3 B8 61.9(4) . . . . ?
B6 C2 B7 B3 -106.6(4) . . . . ?
B6 C2 B7 B8 -67.2(4) . . . . ?
B6 C2 B7 B11 36.0(3) . . . . ?
B6 C2 B7 B12 -4.9(5) . . . . ?
B6 C2 B11 B7 -141.6(4) . . . . ?
B6 C2 B11 B10 -39.2(3) . . . . ?
B6 C2 B11 B12 -101.2(4) . . . . ?
B6 B5 B9 B4 101.3(4) . . . . ?
B6 B5 B9 B8 63.3(5) . . . . ?
B6 B5 B9 B10 -36.4(3) . . . . ?
B6 B5 B9 B12 0.1(5) . . . . ?
B6 B5 B10 B9 137.9(4) . . . . ?
B6 B5 B10 B11 37.5(3) . . . . ?
B6 B5 B10 B12 100.7(4) . . . . ?
B6 B10 B11 C2 39.8(3) . . . . ?
B6 B10 B11 B7 101.1(4) . . . . ?
B6 B10 B11 B12 138.6(4) . . . . ?
B6 B10 B12 B7 0.6(5) . . . . ?
B6 B10 B12 B8 65.1(4) . . . . ?
B6 B10 B12 B9 101.5(4) . . . . ?
B6 B10 B12 B11 -37.1(3) . . . . ?
B6 B11 B12 B7 -101.8(4) . . . . ?
B6 B11 B12 B8 -64.7(4) . . . . ?
B6 B11 B12 B9 -1.5(5) . . . . ?
B6 B11 B12 B10 35.9(3) . . . . ?
B7 C2 B3 C1 -139.0(3) . . . . ?
B7 C2 B3 B4 -104.2(4) . . . . ?
B7 C2 B3 B8 -40.8(3) . . . . ?
B7 C2 B6 C1 103.6(3) . . . . ?
B7 C2 B6 B5 69.0(4) . . . . ?
B7 C2 B6 B10 5.3(5) . . . . ?
B7 C2 B6 B11 -36.1(3) . . . . ?
B7 C2 B11 B6 141.6(4) . . . . ?
B7 C2 B11 B10 102.4(4) . . . . ?
B7 C2 B11 B12 40.4(3) . . . . ?
B7 B3 B4 C1 -95.1(4) . . . . ?
B7 B3 B4 B5 -60.5(4) . . . . ?
B7 B3 B4 B8 39.4(3) . . . . ?
B7 B3 B4 B9 3.1(5) . . . . ?
B7 B3 B8 B4 -136.9(4) . . . . ?
B7 B3 B8 B9 -100.4(4) . . . . ?
B7 B3 B8 B12 -36.0(3) . . . . ?
B7 B8 B9 B4 -100.0(4) . . . . ?
B7 B8 B9 B5 -62.1(5) . . . . ?
B7 B8 B9 B10 1.2(5) . . . . ?
B7 B8 B9 B12 37.4(3) . . . . ?
B7 B8 B12 B9 -137.7(4) . . . . ?
B7 B8 B12 B10 -101.0(4) . . . . ?
B7 B8 B12 B11 -36.7(3) . . . . ?
B7 B11 B12 B8 37.1(3) . . . . ?
B7 B11 B12 B9 100.4(4) . . . . ?
B7 B11 B12 B10 137.8(4) . . . . ?
B8 B3 B4 C1 -134.5(4) . . . . ?
B8 B3 B4 B5 -99.9(4) . . . . ?
B8 B3 B4 B9 -36.3(3) . . . . ?
B8 B3 B7 C2 134.2(4) . . . . ?
B8 B3 B7 B11 100.3(4) . . . . ?
B8 B3 B7 B12 36.2(3) . . . . ?
B8 B4 B5 C1 -97.5(4) . . . . ?
B8 B4 B5 B6 -61.9(4) . . . . ?
B8 B4 B5 B9 37.1(3) . . . . ?
B8 B4 B5 B10 -0.7(4) . . . . ?
B8 B4 B9 B5 -138.3(4) . . . . ?
B8 B4 B9 B10 -100.6(4) . . . . ?
B8 B4 B9 B12 -37.9(3) . . . . ?
B8 B7 B11 C2 96.9(4) . . . . ?
B8 B7 B11 B6 62.5(4) . . . . ?
B8 B7 B11 B10 1.0(5) . . . . ?
B8 B7 B11 B12 -36.6(3) . . . . ?
B8 B7 B12 B9 37.5(3) . . . . ?
B8 B7 B12 B10 101.3(4) . . . . ?
B8 B7 B12 B11 139.2(4) . . . . ?
B8 B9 B10 B5 -102.4(4) . . . . ?
B8 B9 B10 B6 -64.3(4) . . . . ?
B8 B9 B10 B11 -0.5(5) . . . . ?
B8 B9 B10 B12 36.4(3) . . . . ?
B8 B9 B12 B7 -38.2(3) . . . . ?
B8 B9 B12 B10 -139.1(4) . . . . ?
B8 B9 B12 B11 -101.6(4) . . . . ?
B9 B4 B5 C1 -134.7(4) . . . . ?
B9 B4 B5 B6 -99.0(4) . . . . ?
B9 B4 B5 B10 -37.8(3) . . . . ?
B9 B4 B8 B3 139.1(4) . . . . ?
B9 B4 B8 B7 100.9(4) . . . . ?
B9 B4 B8 B12 38.4(3) . . . . ?
B9 B5 B6 C1 -97.1(4) . . . . ?
B9 B5 B6 C2 -63.3(4) . . . . ?
B9 B5 B6 B10 37.4(3) . . . . ?
B9 B5 B6 B11 -1.1(5) . . . . ?
B9 B5 B10 B6 -137.9(4) . . . . ?
B9 B5 B10 B11 -100.5(4) . . . . ?
B9 B5 B10 B12 -37.2(3) . . . . ?
B9 B8 B12 B7 137.7(4) . . . . ?
B9 B8 B12 B10 36.8(3) . . . . ?
B9 B8 B12 B11 101.0(4) . . . . ?
B9 B10 B11 C2 -61.5(4) . . . . ?
B9 B10 B11 B6 -101.4(4) . . . . ?
B9 B10 B11 B7 -0.3(5) . . . . ?
B9 B10 B11 B12 37.3(3) . . . . ?
B9 B10 B12 B7 -100.9(4) . . . . ?
B9 B10 B12 B8 -36.4(3) . . . . ?
B9 B10 B12 B11 -138.6(4) . . . . ?
B10 B5 B6 C1 -134.6(4) . . . . ?
B10 B5 B6 C2 -100.7(4) . . . . ?
B10 B5 B6 B11 -38.5(3) . . . . ?
B10 B5 B9 B4 137.7(4) . . . . ?
B10 B5 B9 B8 99.7(4) . . . . ?
B10 B5 B9 B12 36.5(3) . . . . ?
B10 B6 B11 C2 -133.8(4) . . . . ?
B10 B6 B11 B7 -99.7(4) . . . . ?
B10 B6 B11 B12 -36.7(3) . . . . ?
B10 B9 B12 B7 100.9(4) . . . . ?
B10 B9 B12 B8 139.1(4) . . . . ?
B10 B9 B12 B11 37.5(3) . . . . ?
B10 B11 B12 B7 -137.8(4) . . . . ?
B10 B11 B12 B8 -100.6(4) . . . . ?
B10 B11 B12 B9 -37.4(3) . . . . ?
B11 C2 B3 C1 -103.6(3) . . . . ?
B11 C2 B3 B4 -68.8(4) . . . . ?
B11 C2 B3 B7 35.4(3) . . . . ?
B11 C2 B3 B8 -5.5(4) . . . . ?
B11 C2 B6 C1 139.7(3) . . . . ?
B11 C2 B6 B5 105.1(4) . . . . ?
B11 C2 B6 B10 41.4(3) . . . . ?
B11 C2 B7 B3 -142.5(4) . . . . ?
B11 C2 B7 B8 -103.1(4) . . . . ?
B11 C2 B7 B12 -40.8(3) . . . . ?
B11 B6 B10 B5 138.5(4) . . . . ?
B11 B6 B10 B9 100.8(4) . . . . ?
B11 B6 B10 B12 36.8(3) . . . . ?
B11 B7 B8 B3 -102.6(4) . . . . ?
B11 B7 B8 B4 -64.1(4) . . . . ?
B11 B7 B8 B9 -1.4(5) . . . . ?
B11 B7 B8 B12 36.8(3) . . . . ?
B11 B7 B12 B8 -139.2(4) . . . . ?
B11 B7 B12 B9 -101.7(4) . . . . ?
B11 B7 B12 B10 -38.0(3) . . . . ?
B11 B10 B12 B7 37.7(3) . . . . ?
B11 B10 B12 B8 102.2(4) . . . . ?
B11 B10 B12 B9 138.6(4) . . . . ?
C11 P1 C2 C1 113.3(3) . . . . ?
C11 P1 C2 B3 44.7(3) . . . . ?
C11 P1 C2 B6 -178.8(3) . . . . ?
C11 P1 C2 B7 -28.3(4) . . . . ?
C11 P1 C2 B11 -107.9(3) . . . . ?
C11 P1 C2' C1' -113.3(3) . . . . ?
C11 P1 C2' B3' 178.0(3) . . . . ?
C11 P1 C2' B6' -45.0(3) . . . . ?
C11 P1 C2' B7' 108.7(3) . . . . ?
C11 P1 C2' B11' 29.6(4) . . . . ?
B12 B7 B8 B3 -139.3(4) . . . . ?
B12 B7 B8 B4 -100.9(4) . . . . ?
B12 B7 B8 B9 -38.1(3) . . . . ?
B12 B7 B11 C2 133.5(4) . . . . ?
B12 B7 B11 B6 99.1(4) . . . . ?
B12 B7 B11 B10 37.6(3) . . . . ?
B12 B8 B9 B4 -137.4(4) . . . . ?
B12 B8 B9 B5 -99.5(4) . . . . ?
B12 B8 B9 B10 -36.2(3) . . . . ?
B12 B9 B10 B5 -138.8(4) . . . . ?
B12 B9 B10 B6 -100.6(4) . . . . ?
B12 B9 B10 B11 -36.9(3) . . . . ?
B12 B10 B11 C2 -98.8(4) . . . . ?
B12 B10 B11 B6 -138.6(4) . . . . ?
B12 B10 B11 B7 -37.6(3) . . . . ?
C1' C1 C2 P1 -1.5(4) . . . . ?
C1' C1 C2 B3 108.4(4) . . . . ?
C1' C1 C2 B6 -109.0(4) . . . . ?
C1' C1 C2 B7 146.7(3) . . . . ?
C1' C1 C2 B11 -146.5(3) . . . . ?
C1' C1 B3 C2 -101.8(4) . . . . ?
C1' C1 B3 B4 118.9(4) . . . . ?
C1' C1 B3 B7 -137.1(3) . . . . ?
C1' C1 B3 B8 159.2(3) . . . . ?
C1' C1 B4 B3 -102.4(4) . . . . ?
C1' C1 B4 B5 116.5(4) . . . . ?
C1' C1 B4 B8 -141.6(4) . . . . ?
C1' C1 B4 B9 156.2(4) . . . . ?
C1' C1 B5 B4 -116.6(4) . . . . ?
C1' C1 B5 B6 103.2(4) . . . . ?
C1' C1 B5 B9 -155.6(4) . . . . ?
C1' C1 B5 B10 141.9(4) . . . . ?
C1' C1 B6 C2 101.5(4) . . . . ?
C1' C1 B6 B5 -118.7(4) . . . . ?
C1' C1 B6 B10 -159.0(3) . . . . ?
C1' C1 B6 B11 136.7(3) . . . . ?
C1' C2' B3' B4' 34.3(3) . . . . ?
C1' C2' B3' B7' 139.1(3) . . . . ?
C1' C2' B3' B8' 98.0(3) . . . . ?
C1' C2' B6' B5' -35.5(3) . . . . ?
C1' C2' B6' B10' -98.2(3) . . . . ?
C1' C2' B6' B11' -139.2(3) . . . . ?
C1' C2' B7' B3' -39.3(3) . . . . ?
C1' C2' B7' B8' -0.4(4) . . . . ?
C1' C2' B7' B11' 103.3(4) . . . . ?
C1' C2' B7' B12' 62.3(4) . . . . ?
C1' C2' B11' B6' 38.5(3) . . . . ?
C1' C2' B11' B7' -104.2(3) . . . . ?
C1' C2' B11' B10' -1.1(4) . . . . ?
C1' C2' B11' B12' -62.9(4) . . . . ?
C1' B3' B4' B5' 35.1(3) . . . . ?
C1' B3' B4' B8' 135.0(3) . . . . ?
C1' B3' B4' B9' 98.1(4) . . . . ?
C1' B3' B7' C2' 33.9(3) . . . . ?
C1' B3' B7' B8' -100.5(3) . . . . ?
C1' B3' B7' B11' -0.3(4) . . . . ?
C1' B3' B7' B12' -63.9(4) . . . . ?
C1' B3' B8' B4' -38.4(3) . . . . ?
C1' B3' B8' B7' 97.9(3) . . . . ?
C1' B3' B8' B9' -1.5(4) . . . . ?
C1' B3' B8' B12' 61.5(4) . . . . ?
C1' B4' B5' B6' 34.8(3) . . . . ?
C1' B4' B5' B9' 134.3(3) . . . . ?
C1' B4' B5' B10' 96.6(3) . . . . ?
C1' B4' B8' B3' 39.8(3) . . . . ?
C1' B4' B8' B7' 1.0(4) . . . . ?
C1' B4' B8' B9' -98.7(4) . . . . ?
C1' B4' B8' B12' -61.8(4) . . . . ?
C1' B4' B9' B5' -39.4(3) . . . . ?
C1' B4' B9' B8' 99.3(3) . . . . ?
C1' B4' B9' B10' -1.4(4) . . . . ?
C1' B4' B9' B12' 61.8(4) . . . . ?
C1' B5' B6' C2' 34.3(3) . . . . ?
C1' B5' B6' B10' 133.9(3) . . . . ?
C1' B5' B6' B11' 95.7(3) . . . . ?
C1' B5' B9' B4' 38.9(3) . . . . ?
C1' B5' B9' B8' 1.6(4) . . . . ?
C1' B5' B9' B10' -98.7(3) . . . . ?
C1' B5' B9' B12' -62.3(4) . . . . ?
C1' B5' B10' B6' -40.0(3) . . . . ?
C1' B5' B10' B9' 98.2(3) . . . . ?
C1' B5' B10' B11' -1.7(4) . . . . ?
C1' B5' B10' B12' 61.5(4) . . . . ?
C1' B6' B10' B5' 39.6(3) . . . . ?
C1' B6' B10' B9' 2.1(4) . . . . ?
C1' B6' B10' B11' -98.2(3) . . . . ?
C1' B6' B10' B12' -61.8(4) . . . . ?
C1' B6' B11' C2' -34.0(3) . . . . ?
C1' B6' B11' B7' -0.9(4) . . . . ?
C1' B6' B11' B10' 99.4(3) . . . . ?
C1' B6' B11' B12' 63.2(4) . . . . ?
C2' P1 C2 C1 3.0(3) . . . . ?
C2' P1 C2 B3 -65.6(3) . . . . ?
C2' P1 C2 B6 71.0(3) . . . . ?
C2' P1 C2 B7 -138.6(4) . . . . ?
C2' P1 C2 B11 141.8(3) . . . . ?
C2' P1 C11 C12 -88.0(3) . . . . ?
C2' C1' B3' B4' -139.7(3) . . . . ?
C2' C1' B3' B7' -35.3(3) . . . . ?
C2' C1' B3' B8' -99.6(3) . . . . ?
C2' C1' B4' B3' 36.9(3) . . . . ?
C2' C1' B4' B5' -103.8(3) . . . . ?
C2' C1' B4' B8' -1.2(4) . . . . ?
C2' C1' B4' B9' -64.1(4) . . . . ?
C2' C1' B5' B4' 102.6(3) . . . . ?
C2' C1' B5' B6' -38.4(3) . . . . ?
C2' C1' B5' B9' 63.1(4) . . . . ?
C2' C1' B5' B10' 1.0(4) . . . . ?
C2' C1' B6' B5' 138.8(3) . . . . ?
C2' C1' B6' B10' 98.3(3) . . . . ?
C2' C1' B6' B11' 35.3(3) . . . . ?
C2' B3' B4' C1' -33.4(3) . . . . ?
C2' B3' B4' B5' 1.7(4) . . . . ?
C2' B3' B4' B8' 101.7(3) . . . . ?
C2' B3' B4' B9' 64.7(4) . . . . ?
C2' B3' B7' B8' -134.3(3) . . . . ?
C2' B3' B7' B11' -34.2(3) . . . . ?
C2' B3' B7' B12' -97.8(4) . . . . ?
C2' B3' B8' B4' -96.6(3) . . . . ?
C2' B3' B8' B7' 39.7(3) . . . . ?
C2' B3' B8' B9' -59.7(4) . . . . ?
C2' B3' B8' B12' 3.3(4) . . . . ?
C2' B6' B10' B5' 97.7(3) . . . . ?
C2' B6' B10' B9' 60.3(4) . . . . ?
C2' B6' B10' B11' -40.1(3) . . . . ?
C2' B6' B10' B12' -3.6(4) . . . . ?
C2' B6' B11' B7' 33.1(3) . . . . ?
C2' B6' B11' B10' 133.5(3) . . . . ?
C2' B6' B11' B12' 97.2(4) . . . . ?
C2' B7' B8' B3' -39.8(3) . . . . ?
C2' B7' B8' B4' -0.4(4) . . . . ?
C2' B7' B8' B9' 62.1(4) . . . . ?
C2' B7' B8' B12' 99.3(4) . . . . ?
C2' B7' B11' B6' -33.4(3) . . . . ?
C2' B7' B11' B10' -95.5(4) . . . . ?
C2' B7' B11' B12' -132.9(3) . . . . ?
C2' B7' B12' B8' -98.4(3) . . . . ?
C2' B7' B12' B9' -60.5(4) . . . . ?
C2' B7' B12' B10' 3.2(4) . . . . ?
C2' B7' B12' B11' 41.1(3) . . . . ?
C2' B11' B12' B7' -40.3(3) . . . . ?
C2' B11' B12' B8' -4.0(4) . . . . ?
C2' B11' B12' B9' 60.0(4) . . . . ?
C2' B11' B12' B10' 97.7(4) . . . . ?
B3' C1' C2' P1 -105.6(3) . . . . ?
B3' C1' C2' B6' 143.0(3) . . . . ?
B3' C1' C2' B7' 38.2(3) . . . . ?
B3' C1' C2' B11' 104.7(4) . . . . ?
B3' C1' B4' B5' -140.7(3) . . . . ?
B3' C1' B4' B8' -38.2(3) . . . . ?
B3' C1' B4' B9' -101.0(4) . . . . ?
B3' C1' B5' B4' 36.8(3) . . . . ?
B3' C1' B5' B6' -104.2(3) . . . . ?
B3' C1' B5' B9' -2.6(4) . . . . ?
B3' C1' B5' B10' -64.8(4) . . . . ?
B3' C1' B6' C2' -34.6(3) . . . . ?
B3' C1' B6' B5' 104.2(4) . . . . ?
B3' C1' B6' B10' 63.8(4) . . . . ?
B3' C1' B6' B11' 0.7(4) . . . . ?
B3' C2' B6' C1' 36.6(3) . . . . ?
B3' C2' B6' B5' 1.1(4) . . . . ?
B3' C2' B6' B10' -61.6(4) . . . . ?
B3' C2' B6' B11' -102.6(4) . . . . ?
B3' C2' B7' B8' 38.9(3) . . . . ?
B3' C2' B7' B11' 142.6(3) . . . . ?
B3' C2' B7' B12' 101.6(4) . . . . ?
B3' C2' B11' B6' 107.8(3) . . . . ?
B3' C2' B11' B7' -35.0(3) . . . . ?
B3' C2' B11' B10' 68.1(4) . . . . ?
B3' C2' B11' B12' 6.3(4) . . . . ?
B3' B4' B5' C1' -35.9(3) . . . . ?
B3' B4' B5' B6' -1.1(5) . . . . ?
B3' B4' B5' B9' 98.4(4) . . . . ?
B3' B4' B5' B10' 60.7(4) . . . . ?
B3' B4' B8' B7' -38.9(3) . . . . ?
B3' B4' B8' B9' -138.6(3) . . . . ?
B3' B4' B8' B12' -101.6(4) . . . . ?
B3' B4' B9' B5' -103.1(4) . . . . ?
B3' B4' B9' B8' 35.6(3) . . . . ?
B3' B4' B9' B10' -65.0(4) . . . . ?
B3' B4' B9' B12' -1.9(5) . . . . ?
B3' B7' B8' B4' 39.4(3) . . . . ?
B3' B7' B8' B9' 101.9(4) . . . . ?
B3' B7' B8' B12' 139.2(4) . . . . ?
B3' B7' B11' C2' 34.2(3) . . . . ?
B3' B7' B11' B6' 0.8(5) . . . . ?
B3' B7' B11' B10' -61.3(4) . . . . ?
B3' B7' B11' B12' -98.8(4) . . . . ?
B3' B7' B12' B8' -35.6(3) . . . . ?
B3' B7' B12' B9' 2.3(5) . . . . ?
B3' B7' B12' B10' 66.0(4) . . . . ?
B3' B7' B12' B11' 103.9(4) . . . . ?
B3' B8' B9' B4' -37.7(3) . . . . ?
B3' B8' B9' B5' 0.0(5) . . . . ?
B3' B8' B9' B10' 63.8(4) . . . . ?
B3' B8' B9' B12' 100.5(4) . . . . ?
B3' B8' B12' B7' 36.5(3) . . . . ?
B3' B8' B12' B9' -101.3(4) . . . . ?
B3' B8' B12' B10' -64.1(4) . . . . ?
B3' B8' B12' B11' 0.4(5) . . . . ?
B4' C1' C2' P1 -142.7(3) . . . . ?
B4' C1' C2' B3' -37.2(3) . . . . ?
B4' C1' C2' B6' 105.8(4) . . . . ?
B4' C1' C2' B7' 1.0(4) . . . . ?
B4' C1' C2' B11' 67.6(4) . . . . ?
B4' C1' B3' C2' 139.7(3) . . . . ?
B4' C1' B3' B7' 104.4(4) . . . . ?
B4' C1' B3' B8' 40.1(3) . . . . ?
B4' C1' B5' B6' -141.0(3) . . . . ?
B4' C1' B5' B9' -39.5(3) . . . . ?
B4' C1' B5' B10' -101.6(4) . . . . ?
B4' C1' B6' C2' -101.4(3) . . . . ?
B4' C1' B6' B5' 37.3(3) . . . . ?
B4' C1' B6' B10' -3.1(4) . . . . ?
B4' C1' B6' B11' -66.2(4) . . . . ?
B4' B3' B7' C2' 94.3(4) . . . . ?
B4' B3' B7' B8' -40.0(3) . . . . ?
B4' B3' B7' B11' 60.1(4) . . . . ?
B4' B3' B7' B12' -3.5(5) . . . . ?
B4' B3' B8' B7' 136.3(4) . . . . ?
B4' B3' B8' B9' 36.9(3) . . . . ?
B4' B3' B8' B12' 99.9(4) . . . . ?
B4' B5' B6' C1' -34.2(3) . . . . ?
B4' B5' B6' C2' 0.1(4) . . . . ?
B4' B5' B6' B10' 99.7(4) . . . . ?
B4' B5' B6' B11' 61.5(4) . . . . ?
B4' B5' B9' B8' -37.3(3) . . . . ?
B4' B5' B9' B10' -137.7(3) . . . . ?
B4' B5' B9' B12' -101.2(4) . . . . ?
B4' B5' B10' B6' -100.8(4) . . . . ?
B4' B5' B10' B9' 37.4(3) . . . . ?
B4' B5' B10' B11' -62.5(4) . . . . ?
B4' B5' B10' B12' 0.6(4) . . . . ?
B4' B8' B9' B5' 37.6(3) . . . . ?
B4' B8' B9' B10' 101.4(4) . . . . ?
B4' B8' B9' B12' 138.2(4) . . . . ?
B4' B8' B12' B7' 100.9(4) . . . . ?
B4' B8' B12' B9' -36.9(3) . . . . ?
B4' B8' B12' B10' 0.3(5) . . . . ?
B4' B8' B12' B11' 64.9(4) . . . . ?
B4' B9' B10' B5' -38.4(3) . . . . ?
B4' B9' B10' B6' -0.5(5) . . . . ?
B4' B9' B10' B11' 63.7(4) . . . . ?
B4' B9' B10' B12' 100.8(4) . . . . ?
B4' B9' B12' B7' -0.2(5) . . . . ?
B4' B9' B12' B8' 37.6(3) . . . . ?
B4' B9' B12' B10' -101.2(4) . . . . ?
B4' B9' B12' B11' -63.2(4) . . . . ?
B5' C1' C2' P1 149.8(3) . . . . ?
B5' C1' C2' B3' -104.6(3) . . . . ?
B5' C1' C2' B6' 38.4(3) . . . . ?
B5' C1' C2' B7' -66.4(4) . . . . ?
B5' C1' C2' B11' 0.1(4) . . . . ?
B5' C1' B3' C2' 102.2(3) . . . . ?
B5' C1' B3' B4' -37.4(3) . . . . ?
B5' C1' B3' B7' 67.0(4) . . . . ?
B5' C1' B3' B8' 2.7(4) . . . . ?
B5' C1' B4' B3' 140.7(3) . . . . ?
B5' C1' B4' B8' 102.6(4) . . . . ?
B5' C1' B4' B9' 39.7(3) . . . . ?
B5' C1' B6' C2' -138.8(3) . . . . ?
B5' C1' B6' B10' -40.5(3) . . . . ?
B5' C1' B6' B11' -103.5(3) . . . . ?
B5' B4' B8' B3' 101.7(4) . . . . ?
B5' B4' B8' B7' 62.8(4) . . . . ?
B5' B4' B8' B9' -36.9(3) . . . . ?
B5' B4' B8' B12' 0.1(5) . . . . ?
B5' B4' B9' B8' 138.7(3) . . . . ?
B5' B4' B9' B10' 38.0(3) . . . . ?
B5' B4' B9' B12' 101.2(4) . . . . ?
B5' B6' B10' B9' -37.5(3) . . . . ?
B5' B6' B10' B11' -137.8(4) . . . . ?
B5' B6' B10' B12' -101.3(4) . . . . ?
B5' B6' B11' C2' -95.3(3) . . . . ?
B5' B6' B11' B7' -62.2(4) . . . . ?
B5' B6' B11' B10' 38.1(3) . . . . ?
B5' B6' B11' B12' 1.9(4) . . . . ?
B5' B9' B10' B6' 37.9(3) . . . . ?
B5' B9' B10' B11' 102.1(4) . . . . ?
B5' B9' B10' B12' 139.1(4) . . . . ?
B5' B9' B12' B7' 64.3(4) . . . . ?
B5' B9' B12' B8' 102.1(4) . . . . ?
B5' B9' B12' B10' -36.7(3) . . . . ?
B5' B9' B12' B11' 1.3(5) . . . . ?
B5' B10' B11' C2' 1.7(4) . . . . ?
B5' B10' B11' B6' -38.4(3) . . . . ?
B5' B10' B11' B7' 62.9(4) . . . . ?
B5' B10' B11' B12' 100.8(4) . . . . ?
B5' B10' B12' B7' -64.3(4) . . . . ?
B5' B10' B12' B8' -0.6(4) . . . . ?
B5' B10' B12' B9' 36.6(3) . . . . ?
B5' B10' B12' B11' -101.6(4) . . . . ?
B6' C1' C2' P1 111.4(3) . . . . ?
B6' C1' C2' B3' -143.0(3) . . . . ?
B6' C1' C2' B7' -104.8(4) . . . . ?
B6' C1' C2' B11' -38.3(3) . . . . ?
B6' C1' B3' C2' 35.0(3) . . . . ?
B6' C1' B3' B4' -104.7(4) . . . . ?
B6' C1' B3' B7' -0.3(4) . . . . ?
B6' C1' B3' B8' -64.6(4) . . . . ?
B6' C1' B4' B3' 103.8(3) . . . . ?
B6' C1' B4' B5' -36.9(3) . . . . ?
B6' C1' B4' B8' 65.7(4) . . . . ?
B6' C1' B4' B9' 2.8(4) . . . . ?
B6' C1' B5' B4' 141.0(3) . . . . ?
B6' C1' B5' B9' 101.6(3) . . . . ?
B6' C1' B5' B10' 39.4(3) . . . . ?
B6' C2' B3' C1' -36.1(3) . . . . ?
B6' C2' B3' B4' -1.8(5) . . . . ?
B6' C2' B3' B7' 103.1(4) . . . . ?
B6' C2' B3' B8' 61.9(4) . . . . ?
B6' C2' B7' B3' -107.3(3) . . . . ?
B6' C2' B7' B8' -68.4(4) . . . . ?
B6' C2' B7' B11' 35.3(3) . . . . ?
B6' C2' B7' B12' -5.7(4) . . . . ?
B6' C2' B11' B7' -142.8(3) . . . . ?
B6' C2' B11' B10' -39.7(3) . . . . ?
B6' C2' B11' B12' -101.5(4) . . . . ?
B6' B5' B9' B4' 101.1(4) . . . . ?
B6' B5' B9' B8' 63.8(4) . . . . ?
B6' B5' B9' B10' -36.5(3) . . . . ?
B6' B5' B9' B12' -0.1(5) . . . . ?
B6' B5' B10' B9' 138.2(4) . . . . ?
B6' B5' B10' B11' 38.3(3) . . . . ?
B6' B5' B10' B12' 101.4(4) . . . . ?
B6' B10' B11' C2' 40.1(3) . . . . ?
B6' B10' B11' B7' 101.3(4) . . . . ?
B6' B10' B11' B12' 139.1(4) . . . . ?
B6' B10' B12' B7' 0.3(5) . . . . ?
B6' B10' B12' B8' 64.0(4) . . . . ?
B6' B10' B12' B9' 101.2(4) . . . . ?
B6' B10' B12' B11' -37.0(3) . . . . ?
B6' B11' B12' B7' -102.3(4) . . . . ?
B6' B11' B12' B8' -66.0(4) . . . . ?
B6' B11' B12' B9' -2.0(5) . . . . ?
B6' B11' B12' B10' 35.7(3) . . . . ?
B7' C2' B3' C1' -139.1(3) . . . . ?
B7' C2' B3' B4' -104.9(4) . . . . ?
B7' C2' B3' B8' -41.2(3) . . . . ?
B7' C2' B6' C1' 104.1(3) . . . . ?
B7' C2' B6' B5' 68.6(4) . . . . ?
B7' C2' B6' B10' 5.9(4) . . . . ?
B7' C2' B6' B11' -35.1(3) . . . . ?
B7' C2' B11' B6' 142.8(3) . . . . ?
B7' C2' B11' B10' 103.1(4) . . . . ?
B7' C2' B11' B12' 41.3(3) . . . . ?
B7' B3' B4' C1' -94.7(4) . . . . ?
B7' B3' B4' B5' -59.6(4) . . . . ?
B7' B3' B4' B8' 40.3(3) . . . . ?
B7' B3' B4' B9' 3.4(5) . . . . ?
B7' B3' B8' B4' -136.3(4) . . . . ?
B7' B3' B8' B9' -99.4(4) . . . . ?
B7' B3' B8' B12' -36.4(3) . . . . ?
B7' B8' B9' B4' -100.9(4) . . . . ?
B7' B8' B9' B5' -63.3(4) . . . . ?
B7' B8' B9' B10' 0.6(4) . . . . ?
B7' B8' B9' B12' 37.3(3) . . . . ?
B7' B8' B12' B9' -137.8(4) . . . . ?
B7' B8' B12' B10' -100.6(4) . . . . ?
B7' B8' B12' B11' -36.1(3) . . . . ?
B7' B11' B12' B8' 36.3(3) . . . . ?
B7' B11' B12' B9' 100.3(4) . . . . ?
B7' B11' B12' B10' 138.0(4) . . . . ?
B8' B3' B4' C1' -135.0(3) . . . . ?
B8' B3' B4' B5' -99.9(4) . . . . ?
B8' B3' B4' B9' -36.9(3) . . . . ?
B8' B3' B7' C2' 134.3(3) . . . . ?
B8' B3' B7' B11' 100.1(4) . . . . ?
B8' B3' B7' B12' 36.5(3) . . . . ?
B8' B4' B5' C1' -97.1(4) . . . . ?
B8' B4' B5' B6' -62.3(4) . . . . ?
B8' B4' B5' B9' 37.2(3) . . . . ?
B8' B4' B5' B10' -0.4(4) . . . . ?
B8' B4' B9' B5' -138.7(3) . . . . ?
B8' B4' B9' B10' -100.7(4) . . . . ?
B8' B4' B9' B12' -37.5(3) . . . . ?
B8' B7' B11' C2' 96.3(4) . . . . ?
B8' B7' B11' B6' 62.9(4) . . . . ?
B8' B7' B11' B10' 0.8(5) . . . . ?
B8' B7' B11' B12' -36.6(3) . . . . ?
B8' B7' B12' B9' 37.9(3) . . . . ?
B8' B7' B12' B10' 101.6(4) . . . . ?
B8' B7' B12' B11' 139.5(4) . . . . ?
B8' B9' B10' B5' -102.2(4) . . . . ?
B8' B9' B10' B6' -64.3(4) . . . . ?
B8' B9' B10' B11' -0.1(5) . . . . ?
B8' B9' B10' B12' 37.0(3) . . . . ?
B8' B9' B12' B7' -37.8(3) . . . . ?
B8' B9' B12' B10' -138.8(4) . . . . ?
B8' B9' B12' B11' -100.8(4) . . . . ?
B9' B4' B5' C1' -134.3(3) . . . . ?
B9' B4' B5' B6' -99.5(4) . . . . ?
B9' B4' B5' B10' -37.7(3) . . . . ?
B9' B4' B8' B3' 138.6(3) . . . . ?
B9' B4' B8' B7' 99.7(4) . . . . ?
B9' B4' B8' B12' 37.0(3) . . . . ?
B9' B5' B6' C1' -96.8(4) . . . . ?
B9' B5' B6' C2' -62.5(4) . . . . ?
B9' B5' B6' B10' 37.1(3) . . . . ?
B9' B5' B6' B11' -1.1(4) . . . . ?
B9' B5' B10' B6' -138.2(4) . . . . ?
B9' B5' B10' B11' -99.9(4) . . . . ?
B9' B5' B10' B12' -36.8(3) . . . . ?
B9' B8' B12' B7' 137.8(4) . . . . ?
B9' B8' B12' B10' 37.2(3) . . . . ?
B9' B8' B12' B11' 101.8(4) . . . . ?
B9' B10' B11' C2' -61.7(4) . . . . ?
B9' B10' B11' B6' -101.8(4) . . . . ?
B9' B10' B11' B7' -0.5(5) . . . . ?
B9' B10' B11' B12' 37.4(3) . . . . ?
B9' B10' B12' B7' -100.9(4) . . . . ?
B9' B10' B12' B8' -37.2(3) . . . . ?
B9' B10' B12' B11' -138.2(4) . . . . ?
B10' B5' B6' C1' -133.9(3) . . . . ?
B10' B5' B6' C2' -99.7(4) . . . . ?
B10' B5' B6' B11' -38.2(3) . . . . ?
B10' B5' B9' B4' 137.7(3) . . . . ?
B10' B5' B9' B8' 100.3(4) . . . . ?
B10' B5' B9' B12' 36.4(3) . . . . ?
B10' B6' B11' C2' -133.5(3) . . . . ?
B10' B6' B11' B7' -100.4(4) . . . . ?
B10' B6' B11' B12' -36.2(3) . . . . ?
B10' B9' B12' B7' 101.0(4) . . . . ?
B10' B9' B12' B8' 138.8(4) . . . . ?
B10' B9' B12' B11' 38.0(3) . . . . ?
B10' B11' B12' B7' -138.0(4) . . . . ?
B10' B11' B12' B8' -101.7(4) . . . . ?
B10' B11' B12' B9' -37.7(3) . . . . ?
B11' C2' B3' C1' -104.1(3) . . . . ?
B11' C2' B3' B4' -69.8(4) . . . . ?
B11' C2' B3' B7' 35.0(3) . . . . ?
B11' C2' B3' B8' -6.1(4) . . . . ?
B11' C2' B6' C1' 139.2(3) . . . . ?
B11' C2' B6' B5' 103.7(4) . . . . ?
B11' C2' B6' B10' 41.0(3) . . . . ?
B11' C2' B7' B3' -142.6(3) . . . . ?
B11' C2' B7' B8' -103.7(4) . . . . ?
B11' C2' B7' B12' -41.0(3) . . . . ?
B11' B6' B10' B5' 137.8(4) . . . . ?
B11' B6' B10' B9' 100.3(4) . . . . ?
B11' B6' B10' B12' 36.5(3) . . . . ?
B11' B7' B8' B3' -102.8(4) . . . . ?
B11' B7' B8' B4' -63.3(4) . . . . ?
B11' B7' B8' B9' -0.9(5) . . . . ?
B11' B7' B8' B12' 36.4(3) . . . . ?
B11' B7' B12' B8' -139.5(4) . . . . ?
B11' B7' B12' B9' -101.7(4) . . . . ?
B11' B7' B12' B10' -37.9(3) . . . . ?
B11' B10' B12' B7' 37.3(3) . . . . ?
B11' B10' B12' B8' 101.0(4) . . . . ?
B11' B10' B12' B9' 138.2(4) . . . . ?
B12' B7' B8' B3' -139.2(4) . . . . ?
B12' B7' B8' B4' -99.7(4) . . . . ?
B12' B7' B8' B9' -37.3(3) . . . . ?
B12' B7' B11' C2' 132.9(3) . . . . ?
B12' B7' B11' B6' 99.5(4) . . . . ?
B12' B7' B11' B10' 37.4(3) . . . . ?
B12' B8' B9' B4' -138.2(4) . . . . ?
B12' B8' B9' B5' -100.5(4) . . . . ?
B12' B8' B9' B10' -36.7(3) . . . . ?
B12' B9' B10' B5' -139.1(4) . . . . ?
B12' B9' B10' B6' -101.3(4) . . . . ?
B12' B9' B10' B11' -37.0(3) . . . . ?
B12' B10' B11' C2' -99.1(4) . . . . ?
B12' B10' B11' B6' -139.1(4) . . . . ?
B12' B10' B11' B7' -37.9(3) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.970 -0.081 0.250 269.6 104.1 ?
2 -0.775 0.081 0.750 269.6 105.0 ?
3 -0.715 0.419 0.250 269.6 105.0 ?
4 -0.383 0.581 0.750 269.6 104.2 ?

_shelx_SHELXL_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_5428
_database_code_depnum_ccdc_archive 'CCDC 1527029'
_audit_update_record             
;
2017-01-12 deposited with the CCDC.
2017-03-07 downloaded from the CCDC.
;
_audit_creation_date             2017-01-09
_audit_creation_method           
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C6 H25 B20 P'
_chemical_formula_sum            'C6 H25 B20 P'
_chemical_formula_weight         344.43
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   23.441(2)
_cell_length_b                   7.2690(6)
_cell_length_c                   24.083(2)
_cell_angle_alpha                90
_cell_angle_beta                 108.290(5)
_cell_angle_gamma                90
_cell_volume                     3896.2(6)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    1924
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      23.023
_cell_measurement_theta_min      2.607
_shelx_estimated_absorpt_T_max   0.995
_shelx_estimated_absorpt_T_min   0.948
_exptl_absorpt_coefficient_mu    0.129
_exptl_absorpt_correction_T_max  0.7450
_exptl_absorpt_correction_T_min  0.6011
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2008/1 (Bruker,2008) was used for absorption correction.
wR2(int) was 0.0989 before and 0.0760 after correction.
The Ratio of minimum to maximum transmission is 0.8068.
The λ/2 correction factor is 0.0015.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.174
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       needle
_exptl_crystal_F_000             1408
_exptl_crystal_size_max          0.42
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.1415
_diffrn_reflns_av_unetI/netI     0.1046
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       -6
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            44057
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        23.771
_diffrn_reflns_theta_max         23.771
_diffrn_reflns_theta_min         1.058
_diffrn_ambient_temperature      100.0
_diffrn_detector_area_resol_mean 8
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3517
_reflns_number_total             5928
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v7.68A (Bruker, 2009)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_refine_diff_density_max         0.482
_refine_diff_density_min         -0.407
_refine_diff_density_rms         0.071
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.053
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     609
_refine_ls_number_reflns         5928
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1435
_refine_ls_R_factor_gt           0.0795
_refine_ls_restrained_S_all      1.053
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0821P)²+9.4025P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1841
_refine_ls_wR_factor_ref         0.2133
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 C11C(H11X,H11Y), C11A(H11P,H11Q)
2.b Idealised Me refined as rotating group:
 C12C(H12X,H12Y,H12Z), C12A(H12P,H12Q,H12R)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
P1C P 0.58264(6) 0.37780(19) 0.73051(6) 0.0216(4) Uani 1 1 d . . . . .
C1D C 0.5867(2) 0.2671(6) 0.6150(2) 0.0171(11) Uani 1 1 d . . . . .
C2D C 0.6253(2) 0.3742(7) 0.6757(2) 0.0237(12) Uani 1 1 d . . . . .
B3D B 0.6460(3) 0.1493(9) 0.6663(3) 0.0223(14) Uani 1 1 d . . . . .
H3D H 0.637(2) 0.061(7) 0.693(2) 0.027 Uiso 1 1 d R . . . .
B4D B 0.6329(3) 0.1265(9) 0.5905(3) 0.0253(14) Uani 1 1 d . . . . .
H4D H 0.620(2) 0.003(7) 0.572(2) 0.030 Uiso 1 1 d R . . . .
B5D B 0.6062(3) 0.3431(8) 0.5560(3) 0.0218(14) Uani 1 1 d . . . . .
H5D H 0.571(2) 0.351(6) 0.510(2) 0.026 Uiso 1 1 d R . . . .
B6D B 0.6032(3) 0.5028(8) 0.6107(3) 0.0199(14) Uani 1 1 d . . . . .
H6D H 0.569(2) 0.607(7) 0.6062(19) 0.024 Uiso 1 1 d R . . . .
B7D B 0.7009(3) 0.3180(9) 0.6955(3) 0.0296(16) Uani 1 1 d . . . . .
H7D H 0.723(2) 0.309(7) 0.743(2) 0.036 Uiso 1 1 d R . . . .
B8D B 0.7071(3) 0.1629(9) 0.6399(3) 0.0271(15) Uani 1 1 d . . . . .
H8D H 0.733(2) 0.031(7) 0.653(2) 0.033 Uiso 1 1 d R . . . .
B9D B 0.6839(3) 0.2836(9) 0.5724(3) 0.0256(15) Uani 1 1 d . . . . .
H9D H 0.703(2) 0.257(7) 0.536(2) 0.031 Uiso 1 1 d R . . . .
B10D B 0.6644(3) 0.5104(9) 0.5857(3) 0.0257(15) Uani 1 1 d . . . . .
H10D H 0.671(2) 0.621(7) 0.562(2) 0.031 Uiso 1 1 d R . . . .
C11C C 0.5646(2) 0.6198(7) 0.7341(2) 0.0289(13) Uani 1 1 d . . . . .
H11X H 0.5597 0.6779 0.6957 0.035 Uiso 1 1 calc R . . . .
H11Y H 0.5260 0.6309 0.7424 0.035 Uiso 1 1 calc R . . . .
B11D B 0.6744(3) 0.5311(9) 0.6623(3) 0.0239(15) Uani 1 1 d . . . . .
H11D H 0.683(2) 0.671(7) 0.687(2) 0.029 Uiso 1 1 d R . . . .
B12D B 0.7259(3) 0.4007(9) 0.6377(3) 0.0270(15) Uani 1 1 d . . . . .
H12D H 0.772(2) 0.450(7) 0.644(2) 0.032 Uiso 1 1 d R . . . .
C12C C 0.6138(2) 0.7227(7) 0.7817(2) 0.0298(13) Uani 1 1 d . . . . .
H12X H 0.6508 0.7260 0.7709 0.045 Uiso 1 1 calc GR . . . .
H12Y H 0.6214 0.6589 0.8192 0.045 Uiso 1 1 calc GR . . . .
H12Z H 0.6004 0.8487 0.7852 0.045 Uiso 1 1 calc GR . . . .
C1C C 0.5229(2) 0.2240(6) 0.6151(2) 0.0160(11) Uani 1 1 d . . . . .
C2C C 0.5115(2) 0.2881(7) 0.6760(2) 0.0220(12) Uani 1 1 d . . . . .
B3C B 0.4748(3) 0.4119(9) 0.6133(3) 0.0229(14) Uani 1 1 d . . . . .
H3C H 0.492(2) 0.546(7) 0.609(2) 0.027 Uiso 1 1 d R . . . .
B4C B 0.4574(3) 0.2433(8) 0.5571(3) 0.0219(14) Uani 1 1 d . . . . .
H4C H 0.463(2) 0.265(7) 0.520(2) 0.026 Uiso 1 1 d R . . . .
B5C B 0.4834(3) 0.0248(8) 0.5880(3) 0.0271(15) Uani 1 1 d . . . . .
H5C H 0.507(2) -0.061(7) 0.565(2) 0.033 Uiso 1 1 d R . . . .
B6C B 0.5167(3) 0.0547(8) 0.6640(3) 0.0249(15) Uani 1 1 d . . . . .
H6C H 0.553(2) -0.007(7) 0.687(2) 0.030 Uiso 1 1 d R . . . .
B7C B 0.4380(3) 0.3553(9) 0.6644(3) 0.0252(15) Uani 1 1 d . . . . .
H7C H 0.431(2) 0.472(7) 0.691(2) 0.030 Uiso 1 1 d R . . . .
B8C B 0.4027(3) 0.3242(9) 0.5878(3) 0.0252(15) Uani 1 1 d . . . . .
H8C H 0.367(2) 0.401(7) 0.563(2) 0.030 Uiso 1 1 d R . . . .
B9C B 0.4060(3) 0.0849(9) 0.5723(3) 0.0275(15) Uani 1 1 d . . . . .
H9C H 0.372(2) 0.023(7) 0.541(2) 0.033 Uiso 1 1 d R . . . .
B10C B 0.4440(3) -0.0303(9) 0.6385(3) 0.0261(15) Uani 1 1 d . . . . .
H10C H 0.434(2) -0.177(7) 0.649(2) 0.031 Uiso 1 1 d R . . . .
B11C B 0.4638(3) 0.1373(9) 0.6956(3) 0.0256(14) Uani 1 1 d . . . . .
H11C H 0.474(2) 0.120(7) 0.741(2) 0.031 Uiso 1 1 d R . . . .
B12C B 0.3943(3) 0.1553(8) 0.6386(3) 0.0239(14) Uani 1 1 d . . . . .
H12C H 0.354(2) 0.143(7) 0.649(2) 0.029 Uiso 1 1 d R . . . .
P1A P 0.76522(6) 0.62232(19) 0.40765(6) 0.0235(4) Uani 1 1 d . . . . .
C1A C 0.8808(2) 0.7750(6) 0.4780(2) 0.0193(12) Uani 1 1 d . . . . .
C2A C 0.8150(2) 0.7005(7) 0.4808(2) 0.0222(12) Uani 1 1 d . . . . .
B3A B 0.8782(3) 0.5754(8) 0.5193(3) 0.0215(14) Uani 1 1 d . . . . .
H3A H 0.883(2) 0.440(7) 0.5042(19) 0.026 Uiso 1 1 d R . . . .
B4A B 0.9358(3) 0.7437(8) 0.5440(3) 0.0268(15) Uani 1 1 d . . . . .
H4A H 0.979(2) 0.721(7) 0.544(2) 0.032 Uiso 1 1 d R . . . .
B5A B 0.9047(3) 0.9631(9) 0.5211(3) 0.0269(15) Uani 1 1 d . . . . .
H5A H 0.931(2) 1.055(7) 0.505(2) 0.032 Uiso 1 1 d R . . . .
B6A B 0.8273(3) 0.9365(8) 0.4819(3) 0.0264(15) Uani 1 1 d . . . . .
H6A H 0.803(2) 0.999(7) 0.445(2) 0.032 Uiso 1 1 d R . . . .
B7A B 0.8200(3) 0.6201(9) 0.5492(3) 0.0252(14) Uani 1 1 d . . . . .
H7A H 0.792(2) 0.519(7) 0.549(2) 0.030 Uiso 1 1 d R . . . .
B8A B 0.8971(3) 0.6497(9) 0.5914(3) 0.0311(16) Uani 1 1 d . . . . .
H8A H 0.918(2) 0.553(8) 0.622(2) 0.037 Uiso 1 1 d R . . . .
B9A B 0.9139(3) 0.8876(10) 0.5941(3) 0.0322(16) Uani 1 1 d . . . . .
H9A H 0.948(2) 0.947(7) 0.633(2) 0.039 Uiso 1 1 d R . . . .
B10A B 0.8479(3) 1.0080(9) 0.5543(3) 0.0291(16) Uani 1 1 d . . . . .
H10A H 0.838(2) 1.151(7) 0.564(2) 0.035 Uiso 1 1 d R . . . .
B11A B 0.7891(3) 0.8399(8) 0.5272(3) 0.0254(15) Uani 1 1 d . . . . .
H11A H 0.743(2) 0.859(7) 0.517(2) 0.030 Uiso 1 1 d R . . . .
C11A C 0.7601(2) 0.3733(7) 0.4198(2) 0.0321(14) Uani 1 1 d . . . . .
H11P H 0.7995 0.3148 0.4244 0.039 Uiso 1 1 calc R . . . .
H11Q H 0.7500 0.3527 0.4563 0.039 Uiso 1 1 calc R . . . .
C12A C 0.7127(2) 0.2869(8) 0.3692(3) 0.0380(15) Uani 1 1 d . . . . .
H12P H 0.6739 0.3456 0.3645 0.057 Uiso 1 1 calc GR . . . .
H12Q H 0.7100 0.1552 0.3766 0.057 Uiso 1 1 calc GR . . . .
H12R H 0.7235 0.3036 0.3333 0.057 Uiso 1 1 calc GR . . . .
B12A B 0.8424(3) 0.8116(9) 0.5970(3) 0.0288(16) Uani 1 1 d . . . . .
H12A H 0.828(2) 0.814(7) 0.633(2) 0.035 Uiso 1 1 d R . . . .
C1B C 0.8872(2) 0.7416(7) 0.4174(2) 0.0216(12) Uani 1 1 d . . . . .
C2B C 0.8270(2) 0.6400(7) 0.3729(2) 0.0234(12) Uani 1 1 d . . . . .
B3B B 0.8399(3) 0.8698(9) 0.3591(3) 0.0276(15) Uani 1 1 d . . . . .
H3B H 0.813(2) 0.954(7) 0.370(2) 0.033 Uiso 1 1 d R . . . .
B4B B 0.9201(3) 0.8874(9) 0.3803(3) 0.0282(15) Uani 1 1 d . . . . .
H4B H 0.940(2) 1.006(7) 0.406(2) 0.034 Uiso 1 1 d R . . . .
B5B B 0.9515(3) 0.6675(9) 0.4041(3) 0.0264(15) Uani 1 1 d . . . . .
H5B H 0.995(2) 0.672(7) 0.441(2) 0.032 Uiso 1 1 d R . . . .
B6B B 0.8924(3) 0.5086(8) 0.3982(3) 0.0232(15) Uani 1 1 d . . . . .
H6B H 0.894(2) 0.406(7) 0.429(2) 0.028 Uiso 1 1 d R . . . .
B7B B 0.8136(3) 0.7102(10) 0.3012(3) 0.0339(17) Uani 1 1 d . . . . .
H7B H 0.766(2) 0.706(7) 0.271(2) 0.041 Uiso 1 1 d R . . . .
B8B B 0.8741(3) 0.8691(10) 0.3051(3) 0.0361(17) Uani 1 1 d . . . . .
H8B H 0.866(2) 0.988(8) 0.273(2) 0.043 Uiso 1 1 d R . . . .
B9B B 0.9430(3) 0.7428(10) 0.3314(3) 0.0332(17) Uani 1 1 d . . . . .
H9B H 0.980(2) 0.798(7) 0.320(2) 0.040 Uiso 1 1 d R . . . .
B10B B 0.9257(3) 0.5103(9) 0.3438(3) 0.0293(16) Uani 1 1 d . . . . .
H10B H 0.952(2) 0.389(7) 0.339(2) 0.035 Uiso 1 1 d R . . . .
B11B B 0.8455(3) 0.4915(9) 0.3255(3) 0.0288(16) Uani 1 1 d . . . . .
H11B H 0.820(2) 0.374(8) 0.313(2) 0.035 Uiso 1 1 d R . . . .
B12B B 0.8775(3) 0.6356(10) 0.2834(3) 0.0346(17) Uani 1 1 d . . . . .
H12B H 0.873(2) 0.611(8) 0.243(2) 0.042 Uiso 1 1 d R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
P1C C2D 1.890(5) . ?
P1C C11C 1.818(5) . ?
P1C C2C 1.886(5) . ?
C1D C2D 1.653(7) . ?
C1D B3D 1.764(7) . ?
C1D B4D 1.721(7) . ?
C1D B5D 1.714(8) . ?
C1D B6D 1.766(7) . ?
C1D C1C 1.530(6) . ?
C2D B3D 1.740(8) . ?
C2D B6D 1.756(7) . ?
C2D B7D 1.733(8) . ?
C2D B11D 1.722(8) . ?
B3D H3D 0.97(5) . ?
B3D B4D 1.762(9) . ?
B3D B7D 1.758(9) . ?
B3D B8D 1.743(9) . ?
B4D H4D 1.00(5) . ?
B4D B5D 1.799(8) . ?
B4D B8D 1.791(9) . ?
B4D B9D 1.802(9) . ?
B5D H5D 1.16(5) . ?
B5D B6D 1.774(8) . ?
B5D B9D 1.790(8) . ?
B5D B10D 1.800(8) . ?
B6D H6D 1.09(5) . ?
B6D B10D 1.724(9) . ?
B6D B11D 1.753(8) . ?
B7D H7D 1.10(5) . ?
B7D B8D 1.791(9) . ?
B7D B11D 1.765(9) . ?
B7D B12D 1.777(9) . ?
B8D H8D 1.13(5) . ?
B8D B9D 1.776(9) . ?
B8D B12D 1.789(9) . ?
B9D H9D 1.12(5) . ?
B9D B10D 1.767(9) . ?
B9D B12D 1.787(9) . ?
B10D H10D 1.02(5) . ?
B10D B11D 1.791(9) . ?
B10D B12D 1.773(9) . ?
C11C H11X 0.9900 . ?
C11C H11Y 0.9900 . ?
C11C C12C 1.539(7) . ?
B11D H11D 1.16(5) . ?
B11D B12D 1.776(9) . ?
B12D H12D 1.11(5) . ?
C12C H12X 0.9800 . ?
C12C H12Y 0.9800 . ?
C12C H12Z 0.9800 . ?
C1C C2C 1.639(7) . ?
C1C B3C 1.762(7) . ?
C1C B4C 1.725(7) . ?
C1C B5C 1.732(8) . ?
C1C B6C 1.742(8) . ?
C2C B3C 1.735(8) . ?
C2C B6C 1.732(8) . ?
C2C B7C 1.727(8) . ?
C2C B11C 1.735(8) . ?
B3C H3C 1.07(5) . ?
B3C B4C 1.776(8) . ?
B3C B7C 1.760(9) . ?
B3C B8C 1.729(9) . ?
B4C H4C 0.96(5) . ?
B4C B5C 1.778(8) . ?
B4C B8C 1.770(9) . ?
B4C B9C 1.787(9) . ?
B5C H5C 1.10(5) . ?
B5C B6C 1.763(9) . ?
B5C B9C 1.788(8) . ?
B5C B10C 1.787(9) . ?
B6C H6C 0.96(5) . ?
B6C B10C 1.732(9) . ?
B6C B11C 1.753(9) . ?
B7C H7C 1.10(5) . ?
B7C B8C 1.784(9) . ?
B7C B11C 1.777(9) . ?
B7C B12C 1.774(9) . ?
B8C H8C 1.04(5) . ?
B8C B9C 1.786(9) . ?
B8C B12C 1.788(8) . ?
B9C H9C 1.02(5) . ?
B9C B10C 1.774(9) . ?
B9C B12C 1.777(9) . ?
B10C H10C 1.13(5) . ?
B10C B11C 1.786(9) . ?
B10C B12C 1.783(9) . ?
B11C H11C 1.06(5) . ?
B11C B12C 1.774(9) . ?
B12C H12C 1.06(5) . ?
P1A C2A 1.870(5) . ?
P1A C11A 1.844(5) . ?
P1A C2B 1.890(5) . ?
C1A C2A 1.655(7) . ?
C1A B3A 1.771(7) . ?
C1A B4A 1.719(8) . ?
C1A B5A 1.701(8) . ?
C1A B6A 1.742(8) . ?
C1A C1B 1.533(7) . ?
C2A B3A 1.738(7) . ?
C2A B6A 1.738(8) . ?
C2A B7A 1.717(8) . ?
C2A B11A 1.752(8) . ?
B3A H3A 1.07(5) . ?
B3A B4A 1.779(9) . ?
B3A B7A 1.762(8) . ?
B3A B8A 1.738(9) . ?
B4A H4A 1.01(5) . ?
B4A B5A 1.768(9) . ?
B4A B8A 1.801(9) . ?
B4A B9A 1.790(9) . ?
B5A H5A 1.07(5) . ?
B5A B6A 1.775(9) . ?
B5A B9A 1.791(9) . ?
B5A B10A 1.787(9) . ?
B6A H6A 1.00(5) . ?
B6A B10A 1.737(9) . ?
B6A B11A 1.759(9) . ?
B7A H7A 0.99(5) . ?
B7A B8A 1.788(9) . ?
B7A B11A 1.766(9) . ?
B7A B12A 1.778(9) . ?
B8A H8A 1.03(5) . ?
B8A B9A 1.770(10) . ?
B8A B12A 1.776(9) . ?
B9A H9A 1.11(5) . ?
B9A B10A 1.774(9) . ?
B9A B12A 1.786(9) . ?
B10A H10A 1.11(5) . ?
B10A B11A 1.804(9) . ?
B10A B12A 1.788(9) . ?
B11A H11A 1.04(5) . ?
B11A B12A 1.766(9) . ?
C11A H11P 0.9900 . ?
C11A H11Q 0.9900 . ?
C11A C12A 1.505(7) . ?
C12A H12P 0.9800 . ?
C12A H12Q 0.9800 . ?
C12A H12R 0.9800 . ?
B12A H12A 1.02(5) . ?
C1B C2B 1.654(7) . ?
C1B B3B 1.759(8) . ?
C1B B4B 1.717(8) . ?
C1B B5B 1.723(8) . ?
C1B B6B 1.769(8) . ?
C2B B3B 1.748(8) . ?
C2B B6B 1.746(8) . ?
C2B B7B 1.732(8) . ?
C2B B11B 1.723(8) . ?
B3B H3B 0.99(5) . ?
B3B B4B 1.792(9) . ?
B3B B7B 1.769(9) . ?
B3B B8B 1.730(9) . ?
B4B H4B 1.07(5) . ?
B4B B5B 1.778(9) . ?
B4B B8B 1.798(9) . ?
B4B B9B 1.783(9) . ?
B5B H5B 1.11(5) . ?
B5B B6B 1.776(9) . ?
B5B B9B 1.785(9) . ?
B5B B10B 1.797(9) . ?
B6B H6B 1.05(5) . ?
B6B B10B 1.723(9) . ?
B6B B11B 1.755(9) . ?
B7B H7B 1.12(5) . ?
B7B B8B 1.809(10) . ?
B7B B11B 1.776(9) . ?
B7B B12B 1.767(9) . ?
B8B H8B 1.12(6) . ?
B8B B9B 1.792(10) . ?
B8B B12B 1.785(10) . ?
B9B H9B 1.07(5) . ?
B9B B10B 1.785(10) . ?
B9B B12B 1.785(10) . ?
B10B H10B 1.09(5) . ?
B10B B11B 1.796(9) . ?
B10B B12B 1.786(9) . ?
B11B H11B 1.03(5) . ?
B11B B12B 1.778(10) . ?
B12B H12B 0.97(5) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11C P1C C2D 103.2(2) . . ?
C11C P1C C2C 101.5(2) . . ?
C2C P1C C2D 93.2(2) . . ?
C2D C1D B3D 61.1(3) . . ?
C2D C1D B4D 110.8(4) . . ?
C2D C1D B5D 111.6(4) . . ?
C2D C1D B6D 61.7(3) . . ?
B3D C1D B6D 111.9(4) . . ?
B4D C1D B3D 60.7(3) . . ?
B4D C1D B6D 112.6(4) . . ?
B5D C1D B3D 112.5(4) . . ?
B5D C1D B4D 63.2(3) . . ?
B5D C1D B6D 61.3(3) . . ?
C1C C1D C2D 111.0(4) . . ?
C1C C1D B3D 117.0(4) . . ?
C1C C1D B4D 126.8(4) . . ?
C1C C1D B5D 125.6(4) . . ?
C1C C1D B6D 115.5(4) . . ?
C1D C2D P1C 111.2(3) . . ?
C1D C2D B3D 62.6(3) . . ?
C1D C2D B6D 62.3(3) . . ?
C1D C2D B7D 111.1(4) . . ?
C1D C2D B11D 111.0(4) . . ?
B3D C2D P1C 109.5(3) . . ?
B3D C2D B6D 113.6(4) . . ?
B6D C2D P1C 122.8(3) . . ?
B7D C2D P1C 122.1(3) . . ?
B7D C2D B3D 60.8(3) . . ?
B7D C2D B6D 111.2(4) . . ?
B11D C2D P1C 130.8(4) . . ?
B11D C2D B3D 111.6(4) . . ?
B11D C2D B6D 60.5(3) . . ?
B11D C2D B7D 61.4(3) . . ?
C1D B3D H3D 120(3) . . ?
C2D B3D C1D 56.3(3) . . ?
C2D B3D H3D 114(3) . . ?
C2D B3D B4D 105.0(4) . . ?
C2D B3D B7D 59.4(3) . . ?
C2D B3D B8D 106.7(4) . . ?
B4D B3D C1D 58.4(3) . . ?
B4D B3D H3D 128(3) . . ?
B7D B3D C1D 105.0(4) . . ?
B7D B3D H3D 119(3) . . ?
B7D B3D B4D 110.3(5) . . ?
B8D B3D C1D 105.8(4) . . ?
B8D B3D H3D 130(3) . . ?
B8D B3D B4D 61.4(4) . . ?
B8D B3D B7D 61.5(4) . . ?
C1D B4D B3D 60.8(3) . . ?
C1D B4D H4D 123(3) . . ?
C1D B4D B5D 58.2(3) . . ?
C1D B4D B8D 105.6(4) . . ?
C1D B4D B9D 104.0(4) . . ?
B3D B4D H4D 118(3) . . ?
B3D B4D B5D 108.6(4) . . ?
B3D B4D B8D 58.8(3) . . ?
B3D B4D B9D 106.2(5) . . ?
B5D B4D H4D 124(3) . . ?
B5D B4D B9D 59.6(3) . . ?
B8D B4D H4D 122(3) . . ?
B8D B4D B5D 107.6(4) . . ?
B8D B4D B9D 59.2(3) . . ?
B9D B4D H4D 127(3) . . ?
C1D B5D B4D 58.6(3) . . ?
C1D B5D H5D 121(2) . . ?
C1D B5D B6D 60.8(3) . . ?
C1D B5D B9D 104.8(4) . . ?
C1D B5D B10D 104.7(4) . . ?
B4D B5D H5D 122(2) . . ?
B4D B5D B10D 107.3(4) . . ?
B6D B5D B4D 108.6(4) . . ?
B6D B5D H5D 120(2) . . ?
B6D B5D B9D 105.6(4) . . ?
B6D B5D B10D 57.7(3) . . ?
B9D B5D B4D 60.3(3) . . ?
B9D B5D H5D 127(2) . . ?
B9D B5D B10D 58.9(3) . . ?
B10D B5D H5D 125(2) . . ?
C1D B6D B5D 57.9(3) . . ?
C1D B6D H6D 121(3) . . ?
C2D B6D C1D 56.0(3) . . ?
C2D B6D B5D 104.2(4) . . ?
C2D B6D H6D 118(2) . . ?
B5D B6D H6D 126(2) . . ?
B10D B6D C1D 105.8(4) . . ?
B10D B6D C2D 106.4(4) . . ?
B10D B6D B5D 61.9(3) . . ?
B10D B6D H6D 128(3) . . ?
B10D B6D B11D 62.0(4) . . ?
B11D B6D C1D 104.5(4) . . ?
B11D B6D C2D 58.8(3) . . ?
B11D B6D B5D 110.6(4) . . ?
B11D B6D H6D 120(2) . . ?
C2D B7D B3D 59.8(3) . . ?
C2D B7D H7D 114(3) . . ?
C2D B7D B8D 105.0(4) . . ?
C2D B7D B11D 59.0(3) . . ?
C2D B7D B12D 105.3(4) . . ?
B3D B7D H7D 115(3) . . ?
B3D B7D B8D 58.8(4) . . ?
B3D B7D B11D 108.8(4) . . ?
B3D B7D B12D 107.7(5) . . ?
B8D B7D H7D 128(3) . . ?
B11D B7D H7D 120(3) . . ?
B11D B7D B8D 108.3(4) . . ?
B11D B7D B12D 60.2(4) . . ?
B12D B7D H7D 133(3) . . ?
B12D B7D B8D 60.2(4) . . ?
B3D B8D B4D 59.8(3) . . ?
B3D B8D B7D 59.6(4) . . ?
B3D B8D H8D 107(3) . . ?
B3D B8D B9D 108.2(4) . . ?
B3D B8D B12D 107.7(5) . . ?
B4D B8D H8D 113(3) . . ?
B7D B8D B4D 107.5(4) . . ?
B7D B8D H8D 119(2) . . ?
B9D B8D B4D 60.7(3) . . ?
B9D B8D B7D 107.5(4) . . ?
B9D B8D H8D 131(3) . . ?
B9D B8D B12D 60.2(3) . . ?
B12D B8D B4D 108.6(4) . . ?
B12D B8D B7D 59.5(4) . . ?
B12D B8D H8D 135(3) . . ?
B4D B9D H9D 123(3) . . ?
B5D B9D B4D 60.1(3) . . ?
B5D B9D H9D 120(2) . . ?
B8D B9D B4D 60.1(3) . . ?
B8D B9D B5D 108.6(4) . . ?
B8D B9D H9D 123(3) . . ?
B8D B9D B12D 60.3(4) . . ?
B10D B9D B4D 108.6(4) . . ?
B10D B9D B5D 60.8(3) . . ?
B10D B9D B8D 108.5(5) . . ?
B10D B9D H9D 119(3) . . ?
B10D B9D B12D 59.8(4) . . ?
B12D B9D B4D 108.3(5) . . ?
B12D B9D B5D 108.7(4) . . ?
B12D B9D H9D 121(3) . . ?
B5D B10D H10D 122(3) . . ?
B6D B10D B5D 60.4(3) . . ?
B6D B10D B9D 108.9(4) . . ?
B6D B10D H10D 120(3) . . ?
B6D B10D B11D 59.8(3) . . ?
B6D B10D B12D 108.7(5) . . ?
B9D B10D B5D 60.2(3) . . ?
B9D B10D H10D 123(3) . . ?
B9D B10D B11D 107.9(5) . . ?
B9D B10D B12D 60.7(4) . . ?
B11D B10D B5D 107.7(4) . . ?
B11D B10D H10D 121(3) . . ?
B12D B10D B5D 108.9(4) . . ?
B12D B10D H10D 121(3) . . ?
B12D B10D B11D 59.8(3) . . ?
P1C C11C H11X 109.2 . . ?
P1C C11C H11Y 109.2 . . ?
H11X C11C H11Y 107.9 . . ?
C12C C11C P1C 112.0(4) . . ?
C12C C11C H11X 109.2 . . ?
C12C C11C H11Y 109.2 . . ?
C2D B11D B6D 60.7(3) . . ?
C2D B11D B7D 59.6(3) . . ?
C2D B11D B10D 105.0(4) . . ?
C2D B11D H11D 120(2) . . ?
C2D B11D B12D 105.9(4) . . ?
B6D B11D B7D 109.8(4) . . ?
B6D B11D B10D 58.2(3) . . ?
B6D B11D H11D 116(2) . . ?
B6D B11D B12D 107.2(4) . . ?
B7D B11D B10D 107.8(5) . . ?
B7D B11D H11D 124(2) . . ?
B7D B11D B12D 60.2(4) . . ?
B10D B11D H11D 123(2) . . ?
B12D B11D B10D 59.6(3) . . ?
B12D B11D H11D 127(2) . . ?
B7D B12D B8D 60.3(4) . . ?
B7D B12D B9D 107.6(5) . . ?
B7D B12D H12D 124(2) . . ?
B8D B12D H12D 123(3) . . ?
B9D B12D B8D 59.5(4) . . ?
B9D B12D H12D 121(3) . . ?
B10D B12D B7D 108.1(5) . . ?
B10D B12D B8D 107.6(4) . . ?
B10D B12D B9D 59.5(3) . . ?
B10D B12D B11D 60.6(4) . . ?
B10D B12D H12D 119(3) . . ?
B11D B12D B7D 59.6(4) . . ?
B11D B12D B8D 107.8(4) . . ?
B11D B12D B9D 107.7(4) . . ?
B11D B12D H12D 122(3) . . ?
C11C C12C H12X 109.5 . . ?
C11C C12C H12Y 109.5 . . ?
C11C C12C H12Z 109.5 . . ?
H12X C12C H12Y 109.5 . . ?
H12X C12C H12Z 109.5 . . ?
H12Y C12C H12Z 109.5 . . ?
C1D C1C C2C 112.1(4) . . ?
C1D C1C B3C 117.4(4) . . ?
C1D C1C B4C 127.2(4) . . ?
C1D C1C B5C 125.3(4) . . ?
C1D C1C B6C 115.8(4) . . ?
C2C C1C B3C 61.2(3) . . ?
C2C C1C B4C 110.3(4) . . ?
C2C C1C B5C 110.9(4) . . ?
C2C C1C B6C 61.5(3) . . ?
B4C C1C B3C 61.2(3) . . ?
B4C C1C B5C 61.9(3) . . ?
B4C C1C B6C 111.3(4) . . ?
B5C C1C B3C 112.1(4) . . ?
B5C C1C B6C 61.0(3) . . ?
B6C C1C B3C 112.0(4) . . ?
C1C C2C P1C 111.4(3) . . ?
C1C C2C B3C 62.9(3) . . ?
C1C C2C B6C 62.2(3) . . ?
C1C C2C B7C 111.7(4) . . ?
C1C C2C B11C 111.4(4) . . ?
B3C C2C P1C 121.0(4) . . ?
B6C C2C P1C 111.2(3) . . ?
B6C C2C B3C 113.9(4) . . ?
B6C C2C B11C 60.7(3) . . ?
B7C C2C P1C 129.3(4) . . ?
B7C C2C B3C 61.1(3) . . ?
B7C C2C B6C 111.6(4) . . ?
B7C C2C B11C 61.7(3) . . ?
B11C C2C P1C 122.2(3) . . ?
B11C C2C B3C 112.3(4) . . ?
C1C B3C H3C 117(3) . . ?
C1C B3C B4C 58.4(3) . . ?
C2C B3C C1C 55.9(3) . . ?
C2C B3C H3C 117(3) . . ?
C2C B3C B4C 103.7(4) . . ?
C2C B3C B7C 59.2(3) . . ?
B4C B3C H3C 124(3) . . ?
B7C B3C C1C 104.6(4) . . ?
B7C B3C H3C 124(3) . . ?
B7C B3C B4C 109.0(4) . . ?
B8C B3C C1C 105.6(4) . . ?
B8C B3C C2C 106.3(4) . . ?
B8C B3C H3C 131(3) . . ?
B8C B3C B4C 60.6(4) . . ?
B8C B3C B7C 61.5(4) . . ?
C1C B4C B3C 60.4(3) . . ?
C1C B4C H4C 115(3) . . ?
C1C B4C B5C 59.2(3) . . ?
C1C B4C B8C 105.4(4) . . ?
C1C B4C B9C 105.5(4) . . ?
B3C B4C H4C 122(3) . . ?
B3C B4C B5C 109.3(4) . . ?
B3C B4C B9C 107.3(4) . . ?
B5C B4C H4C 114(3) . . ?
B5C B4C B9C 60.2(3) . . ?
B8C B4C B3C 58.4(3) . . ?
B8C B4C H4C 132(3) . . ?
B8C B4C B5C 108.6(5) . . ?
B8C B4C B9C 60.3(4) . . ?
B9C B4C H4C 126(3) . . ?
C1C B5C B4C 58.9(3) . . ?
C1C B5C H5C 112(3) . . ?
C1C B5C B6C 59.8(3) . . ?
C1C B5C B9C 105.2(4) . . ?
C1C B5C B10C 105.1(4) . . ?
B4C B5C H5C 117(3) . . ?
B4C B5C B9C 60.1(3) . . ?
B4C B5C B10C 107.6(4) . . ?
B6C B5C B4C 107.8(4) . . ?
B6C B5C H5C 118(3) . . ?
B6C B5C B9C 106.2(5) . . ?
B6C B5C B10C 58.4(4) . . ?
B9C B5C H5C 132(3) . . ?
B10C B5C H5C 132(3) . . ?
B10C B5C B9C 59.5(4) . . ?
C1C B6C B5C 59.2(3) . . ?
C1C B6C H6C 118(3) . . ?
C1C B6C B11C 105.8(4) . . ?
C2C B6C C1C 56.3(3) . . ?
C2C B6C B5C 105.2(4) . . ?
C2C B6C H6C 117(3) . . ?
C2C B6C B10C 107.2(4) . . ?
C2C B6C B11C 59.7(3) . . ?
B5C B6C H6C 124(3) . . ?
B10C B6C C1C 107.1(4) . . ?
B10C B6C B5C 61.5(4) . . ?
B10C B6C H6C 129(3) . . ?
B10C B6C B11C 61.7(4) . . ?
B11C B6C B5C 110.5(4) . . ?
B11C B6C H6C 121(3) . . ?
C2C B7C B3C 59.7(3) . . ?
C2C B7C H7C 117(3) . . ?
C2C B7C B8C 104.2(4) . . ?
C2C B7C B11C 59.3(3) . . ?
C2C B7C B12C 105.1(4) . . ?
B3C B7C H7C 115(3) . . ?
B3C B7C B8C 58.4(3) . . ?
B3C B7C B11C 109.2(4) . . ?
B3C B7C B12C 107.6(5) . . ?
B8C B7C H7C 126(2) . . ?
B11C B7C H7C 123(3) . . ?
B11C B7C B8C 108.1(5) . . ?
B12C B7C H7C 131(3) . . ?
B12C B7C B8C 60.3(3) . . ?
B12C B7C B11C 59.9(3) . . ?
B3C B8C B4C 61.0(3) . . ?
B3C B8C B7C 60.1(3) . . ?
B3C B8C H8C 122(3) . . ?
B3C B8C B9C 109.4(4) . . ?
B3C B8C B12C 108.4(4) . . ?
B4C B8C B7C 108.2(4) . . ?
B4C B8C H8C 120(3) . . ?
B4C B8C B9C 60.3(3) . . ?
B4C B8C B12C 107.9(4) . . ?
B7C B8C H8C 124(3) . . ?
B7C B8C B9C 107.6(4) . . ?
B7C B8C B12C 59.6(3) . . ?
B9C B8C H8C 119(3) . . ?
B9C B8C B12C 59.6(4) . . ?
B12C B8C H8C 122(3) . . ?
B4C B9C B5C 59.7(3) . . ?
B4C B9C H9C 124(3) . . ?
B5C B9C H9C 124(3) . . ?
B8C B9C B4C 59.4(4) . . ?
B8C B9C B5C 107.5(4) . . ?
B8C B9C H9C 121(3) . . ?
B10C B9C B4C 107.9(4) . . ?
B10C B9C B5C 60.2(4) . . ?
B10C B9C B8C 108.4(5) . . ?
B10C B9C H9C 121(3) . . ?
B10C B9C B12C 60.3(4) . . ?
B12C B9C B4C 107.6(4) . . ?
B12C B9C B5C 108.2(4) . . ?
B12C B9C B8C 60.2(3) . . ?
B12C B9C H9C 120(3) . . ?
B5C B10C H10C 123(2) . . ?
B6C B10C B5C 60.1(3) . . ?
B6C B10C B9C 108.1(4) . . ?
B6C B10C H10C 120(2) . . ?
B6C B10C B11C 59.7(3) . . ?
B6C B10C B12C 107.4(4) . . ?
B9C B10C B5C 60.3(3) . . ?
B9C B10C H10C 124(2) . . ?
B9C B10C B11C 107.8(4) . . ?
B9C B10C B12C 60.0(4) . . ?
B11C B10C B5C 107.9(4) . . ?
B11C B10C H10C 120(2) . . ?
B12C B10C B5C 108.0(4) . . ?
B12C B10C H10C 122(2) . . ?
B12C B10C B11C 59.6(3) . . ?
C2C B11C B6C 59.5(3) . . ?
C2C B11C B7C 58.9(3) . . ?
C2C B11C B10C 104.7(4) . . ?
C2C B11C H11C 114(3) . . ?
C2C B11C B12C 104.8(4) . . ?
B6C B11C B7C 108.3(4) . . ?
B6C B11C B10C 58.6(3) . . ?
B6C B11C H11C 117(3) . . ?
B6C B11C B12C 106.9(5) . . ?
B7C B11C B10C 108.1(4) . . ?
B7C B11C H11C 119(3) . . ?
B10C B11C H11C 130(3) . . ?
B12C B11C B7C 60.0(3) . . ?
B12C B11C B10C 60.1(3) . . ?
B12C B11C H11C 132(3) . . ?
B7C B12C B8C 60.1(3) . . ?
B7C B12C B9C 108.4(5) . . ?
B7C B12C B10C 108.4(4) . . ?
B7C B12C H12C 117(3) . . ?
B8C B12C H12C 121(3) . . ?
B9C B12C B8C 60.1(4) . . ?
B9C B12C B10C 59.8(4) . . ?
B9C B12C H12C 126(3) . . ?
B10C B12C B8C 107.8(4) . . ?
B10C B12C H12C 125(3) . . ?
B11C B12C B7C 60.1(3) . . ?
B11C B12C B8C 108.0(4) . . ?
B11C B12C B9C 108.2(4) . . ?
B11C B12C B10C 60.3(3) . . ?
B11C B12C H12C 119(3) . . ?
C2A P1A C2B 93.3(2) . . ?
C11A P1A C2A 101.6(2) . . ?
C11A P1A C2B 103.5(2) . . ?
C2A C1A B3A 60.9(3) . . ?
C2A C1A B4A 110.9(4) . . ?
C2A C1A B5A 111.8(4) . . ?
C2A C1A B6A 61.5(3) . . ?
B4A C1A B3A 61.3(3) . . ?
B4A C1A B6A 112.5(4) . . ?
B5A C1A B3A 112.2(4) . . ?
B5A C1A B4A 62.2(3) . . ?
B5A C1A B6A 62.0(3) . . ?
B6A C1A B3A 111.7(4) . . ?
C1B C1A C2A 111.0(4) . . ?
C1B C1A B3A 115.9(4) . . ?
C1B C1A B4A 126.2(4) . . ?
C1B C1A B5A 126.5(4) . . ?
C1B C1A B6A 116.5(4) . . ?
C1A C2A P1A 112.0(3) . . ?
C1A C2A B3A 62.9(3) . . ?
C1A C2A B6A 61.7(3) . . ?
C1A C2A B7A 111.5(4) . . ?
C1A C2A B11A 110.5(4) . . ?
B3A C2A P1A 121.3(3) . . ?
B3A C2A B6A 113.5(4) . . ?
B3A C2A B11A 111.7(4) . . ?
B6A C2A P1A 111.4(4) . . ?
B6A C2A B11A 60.5(3) . . ?
B7A C2A P1A 129.4(4) . . ?
B7A C2A B3A 61.3(3) . . ?
B7A C2A B6A 111.1(4) . . ?
B7A C2A B11A 61.2(3) . . ?
B11A C2A P1A 122.5(3) . . ?
C1A B3A H3A 122(3) . . ?
C1A B3A B4A 57.9(3) . . ?
C2A B3A C1A 56.3(3) . . ?
C2A B3A H3A 118(2) . . ?
C2A B3A B4A 104.4(4) . . ?
C2A B3A B7A 58.7(3) . . ?
B4A B3A H3A 126(3) . . ?
B7A B3A C1A 104.2(4) . . ?
B7A B3A H3A 119(3) . . ?
B7A B3A B4A 109.9(5) . . ?
B8A B3A C1A 105.3(4) . . ?
B8A B3A C2A 106.1(4) . . ?
B8A B3A H3A 127(2) . . ?
B8A B3A B4A 61.6(4) . . ?
B8A B3A B7A 61.4(4) . . ?
C1A B4A B3A 60.8(3) . . ?
C1A B4A H4A 119(3) . . ?
C1A B4A B5A 58.4(3) . . ?
C1A B4A B8A 104.9(4) . . ?
C1A B4A B9A 104.8(4) . . ?
B3A B4A H4A 122(3) . . ?
B3A B4A B8A 58.1(4) . . ?
B3A B4A B9A 106.2(5) . . ?
B5A B4A B3A 108.8(4) . . ?
B5A B4A H4A 117(3) . . ?
B5A B4A B8A 107.5(5) . . ?
B5A B4A B9A 60.4(4) . . ?
B8A B4A H4A 129(3) . . ?
B9A B4A H4A 126(3) . . ?
B9A B4A B8A 59.0(4) . . ?
C1A B5A B4A 59.4(3) . . ?
C1A B5A H5A 114(3) . . ?
C1A B5A B6A 60.1(3) . . ?
C1A B5A B9A 105.5(4) . . ?
C1A B5A B10A 105.7(4) . . ?
B4A B5A H5A 117(3) . . ?
B4A B5A B6A 108.7(4) . . ?
B4A B5A B9A 60.4(4) . . ?
B4A B5A B10A 108.5(5) . . ?
B6A B5A H5A 119(3) . . ?
B6A B5A B9A 106.0(5) . . ?
B6A B5A B10A 58.4(4) . . ?
B9A B5A H5A 130(3) . . ?
B10A B5A H5A 131(3) . . ?
B10A B5A B9A 59.5(4) . . ?
C1A B6A B5A 57.9(3) . . ?
C1A B6A H6A 119(3) . . ?
C1A B6A B11A 106.2(4) . . ?
C2A B6A C1A 56.8(3) . . ?
C2A B6A B5A 104.6(4) . . ?
C2A B6A H6A 113(3) . . ?
C2A B6A B11A 60.1(3) . . ?
B5A B6A H6A 129(3) . . ?
B10A B6A C1A 106.1(4) . . ?
B10A B6A C2A 107.6(5) . . ?
B10A B6A B5A 61.2(4) . . ?
B10A B6A H6A 131(3) . . ?
B10A B6A B11A 62.1(4) . . ?
B11A B6A B5A 110.4(5) . . ?
B11A B6A H6A 118(3) . . ?
C2A B7A B3A 59.9(3) . . ?
C2A B7A H7A 114(3) . . ?
C2A B7A B8A 104.9(4) . . ?
C2A B7A B11A 60.4(3) . . ?
C2A B7A B12A 105.8(4) . . ?
B3A B7A H7A 118(3) . . ?
B3A B7A B8A 58.6(3) . . ?
B3A B7A B11A 110.0(5) . . ?
B3A B7A B12A 107.4(4) . . ?
B8A B7A H7A 130(3) . . ?
B11A B7A H7A 117(3) . . ?
B11A B7A B8A 107.9(5) . . ?
B11A B7A B12A 59.8(4) . . ?
B12A B7A H7A 130(3) . . ?
B12A B7A B8A 59.7(4) . . ?
B3A B8A B4A 60.3(3) . . ?
B3A B8A B7A 59.9(3) . . ?
B3A B8A H8A 115(3) . . ?
B3A B8A B9A 108.9(5) . . ?
B3A B8A B12A 108.6(4) . . ?
B4A B8A H8A 119(3) . . ?
B7A B8A B4A 107.8(4) . . ?
B7A B8A H8A 120(3) . . ?
B9A B8A B4A 60.2(4) . . ?
B9A B8A B7A 108.2(5) . . ?
B9A B8A H8A 126(3) . . ?
B9A B8A B12A 60.5(4) . . ?
B12A B8A B4A 108.4(5) . . ?
B12A B8A B7A 59.9(4) . . ?
B12A B8A H8A 127(3) . . ?
B4A B9A B5A 59.2(4) . . ?
B4A B9A H9A 121(3) . . ?
B5A B9A H9A 123(3) . . ?
B8A B9A B4A 60.8(4) . . ?
B8A B9A B5A 107.8(5) . . ?
B8A B9A H9A 120(3) . . ?
B8A B9A B10A 108.4(5) . . ?
B8A B9A B12A 60.0(4) . . ?
B10A B9A B4A 108.0(5) . . ?
B10A B9A B5A 60.2(4) . . ?
B10A B9A H9A 123(3) . . ?
B10A B9A B12A 60.3(4) . . ?
B12A B9A B4A 108.5(5) . . ?
B12A B9A B5A 108.0(5) . . ?
B12A B9A H9A 122(3) . . ?
B5A B10A H10A 120(3) . . ?
B5A B10A B11A 107.8(4) . . ?
B5A B10A B12A 108.1(5) . . ?
B6A B10A B5A 60.5(4) . . ?
B6A B10A B9A 108.4(5) . . ?
B6A B10A H10A 119(3) . . ?
B6A B10A B11A 59.6(4) . . ?
B6A B10A B12A 107.0(5) . . ?
B9A B10A B5A 60.4(4) . . ?
B9A B10A H10A 124(3) . . ?
B9A B10A B11A 107.4(5) . . ?
B9A B10A B12A 60.2(4) . . ?
B11A B10A H10A 122(3) . . ?
B12A B10A H10A 125(3) . . ?
B12A B10A B11A 58.9(4) . . ?
C2A B11A B6A 59.3(3) . . ?
C2A B11A B7A 58.4(3) . . ?
C2A B11A B10A 104.1(4) . . ?
C2A B11A H11A 118(3) . . ?
C2A B11A B12A 104.9(4) . . ?
B6A B11A B7A 107.9(4) . . ?
B6A B11A B10A 58.3(4) . . ?
B6A B11A H11A 119(3) . . ?
B6A B11A B12A 106.9(5) . . ?
B7A B11A B10A 108.0(4) . . ?
B7A B11A H11A 120(3) . . ?
B10A B11A H11A 128(3) . . ?
B12A B11A B7A 60.5(4) . . ?
B12A B11A B10A 60.1(4) . . ?
B12A B11A H11A 128(3) . . ?
P1A C11A H11P 109.6 . . ?
P1A C11A H11Q 109.6 . . ?
H11P C11A H11Q 108.1 . . ?
C12A C11A P1A 110.4(4) . . ?
C12A C11A H11P 109.6 . . ?
C12A C11A H11Q 109.6 . . ?
C11A C12A H12P 109.5 . . ?
C11A C12A H12Q 109.5 . . ?
C11A C12A H12R 109.5 . . ?
H12P C12A H12Q 109.5 . . ?
H12P C12A H12R 109.5 . . ?
H12Q C12A H12R 109.5 . . ?
B7A B12A B9A 107.9(5) . . ?
B7A B12A B10A 108.2(5) . . ?
B7A B12A H12A 117(3) . . ?
B8A B12A B7A 60.4(4) . . ?
B8A B12A B9A 59.6(4) . . ?
B8A B12A B10A 107.5(5) . . ?
B8A B12A H12A 121(3) . . ?
B9A B12A B10A 59.5(4) . . ?
B9A B12A H12A 126(3) . . ?
B10A B12A H12A 125(3) . . ?
B11A B12A B7A 59.8(3) . . ?
B11A B12A B8A 108.5(5) . . ?
B11A B12A B9A 108.6(5) . . ?
B11A B12A B10A 61.0(4) . . ?
B11A B12A H12A 119(3) . . ?
C1A C1B C2B 111.6(4) . . ?
C1A C1B B3B 116.7(4) . . ?
C1A C1B B4B 126.3(4) . . ?
C1A C1B B5B 125.4(4) . . ?
C1A C1B B6B 115.8(4) . . ?
C2B C1B B3B 61.5(3) . . ?
C2B C1B B4B 111.7(4) . . ?
C2B C1B B5B 111.1(4) . . ?
C2B C1B B6B 61.2(3) . . ?
B3B C1B B6B 112.1(4) . . ?
B4B C1B B3B 62.0(3) . . ?
B4B C1B B5B 62.3(3) . . ?
B4B C1B B6B 112.1(4) . . ?
B5B C1B B3B 112.8(4) . . ?
B5B C1B B6B 61.1(3) . . ?
C1B C2B P1A 111.2(3) . . ?
C1B C2B B3B 62.2(3) . . ?
C1B C2B B6B 62.7(3) . . ?
C1B C2B B7B 111.4(4) . . ?
C1B C2B B11B 111.5(4) . . ?
B3B C2B P1A 110.6(3) . . ?
B6B C2B P1A 121.3(4) . . ?
B6B C2B B3B 113.9(4) . . ?
B7B C2B P1A 122.5(4) . . ?
B7B C2B B3B 61.1(4) . . ?
B7B C2B B6B 111.9(4) . . ?
B11B C2B P1A 129.6(4) . . ?
B11B C2B B3B 112.2(4) . . ?
B11B C2B B6B 60.8(3) . . ?
B11B C2B B7B 61.8(4) . . ?
C1B B3B H3B 114(3) . . ?
C1B B3B B4B 57.8(3) . . ?
C1B B3B B7B 104.9(4) . . ?
C2B B3B C1B 56.3(3) . . ?
C2B B3B H3B 112(3) . . ?
C2B B3B B4B 104.0(4) . . ?
C2B B3B B7B 59.0(3) . . ?
B4B B3B H3B 126(3) . . ?
B7B B3B H3B 122(3) . . ?
B7B B3B B4B 110.2(5) . . ?
B8B B3B C1B 105.8(5) . . ?
B8B B3B C2B 106.8(5) . . ?
B8B B3B H3B 135(3) . . ?
B8B B3B B4B 61.4(4) . . ?
B8B B3B B7B 62.3(4) . . ?
C1B B4B B3B 60.1(3) . . ?
C1B B4B H4B 113(3) . . ?
C1B B4B B5B 59.0(3) . . ?
C1B B4B B8B 104.7(4) . . ?
C1B B4B B9B 104.9(5) . . ?
B3B B4B H4B 117(3) . . ?
B3B B4B B8B 57.6(4) . . ?
B5B B4B B3B 108.7(4) . . ?
B5B B4B H4B 118(3) . . ?
B5B B4B B8B 108.4(5) . . ?
B5B B4B B9B 60.2(4) . . ?
B8B B4B H4B 130(3) . . ?
B9B B4B B3B 106.1(5) . . ?
B9B B4B H4B 133(3) . . ?
B9B B4B B8B 60.0(4) . . ?
C1B B5B B4B 58.7(3) . . ?
C1B B5B H5B 118(3) . . ?
C1B B5B B6B 60.7(3) . . ?
C1B B5B B9B 104.6(4) . . ?
C1B B5B B10B 104.8(4) . . ?
B4B B5B H5B 114(3) . . ?
B4B B5B B9B 60.0(4) . . ?
B4B B5B B10B 108.1(5) . . ?
B6B B5B B4B 108.9(4) . . ?
B6B B5B H5B 125(3) . . ?
B6B B5B B9B 106.1(5) . . ?
B6B B5B B10B 57.7(4) . . ?
B9B B5B H5B 124(3) . . ?
B9B B5B B10B 59.8(4) . . ?
B10B B5B H5B 131(3) . . ?
C1B B6B B5B 58.1(3) . . ?
C1B B6B H6B 119(3) . . ?
C2B B6B C1B 56.1(3) . . ?
C2B B6B B5B 104.5(4) . . ?
C2B B6B H6B 117(3) . . ?
C2B B6B B11B 59.0(3) . . ?
B5B B6B H6B 124(3) . . ?
B10B B6B C1B 106.0(4) . . ?
B10B B6B C2B 106.8(4) . . ?
B10B B6B B5B 61.8(4) . . ?
B10B B6B H6B 129(3) . . ?
B10B B6B B11B 62.2(4) . . ?
B11B B6B C1B 104.8(4) . . ?
B11B B6B B5B 110.7(5) . . ?
B11B B6B H6B 122(3) . . ?
C2B B7B B3B 59.9(3) . . ?
C2B B7B H7B 118(3) . . ?
C2B B7B B8B 104.1(4) . . ?
C2B B7B B11B 58.8(3) . . ?
C2B B7B B12B 104.5(5) . . ?
B3B B7B H7B 124(3) . . ?
B3B B7B B8B 57.8(4) . . ?
B3B B7B B11B 108.8(4) . . ?
B8B B7B H7B 131(3) . . ?
B11B B7B H7B 115(3) . . ?
B11B B7B B8B 108.2(5) . . ?
B12B B7B B3B 106.3(5) . . ?
B12B B7B H7B 126(3) . . ?
B12B B7B B8B 59.9(4) . . ?
B12B B7B B11B 60.3(4) . . ?
B3B B8B B4B 61.0(4) . . ?
B3B B8B B7B 59.9(4) . . ?
B3B B8B H8B 119(3) . . ?
B3B B8B B9B 108.4(5) . . ?
B3B B8B B12B 107.2(5) . . ?
B4B B8B B7B 108.1(5) . . ?
B4B B8B H8B 123(3) . . ?
B7B B8B H8B 119(3) . . ?
B9B B8B B4B 59.5(4) . . ?
B9B B8B B7B 107.2(5) . . ?
B9B B8B H8B 125(3) . . ?
B12B B8B B4B 107.3(5) . . ?
B12B B8B B7B 58.9(4) . . ?
B12B B8B H8B 123(3) . . ?
B12B B8B B9B 59.9(4) . . ?
B4B B9B B5B 59.8(3) . . ?
B4B B9B B8B 60.4(4) . . ?
B4B B9B H9B 113(3) . . ?
B4B B9B B10B 108.4(5) . . ?
B4B B9B B12B 108.0(5) . . ?
B5B B9B B8B 108.4(5) . . ?
B5B B9B H9B 121(3) . . ?
B5B B9B B10B 60.4(4) . . ?
B5B B9B B12B 108.0(5) . . ?
B8B B9B H9B 116(3) . . ?
B10B B9B B8B 108.5(5) . . ?
B10B B9B H9B 130(3) . . ?
B10B B9B B12B 60.0(4) . . ?
B12B B9B B8B 59.9(4) . . ?
B12B B9B H9B 127(3) . . ?
B5B B10B H10B 122(3) . . ?
B6B B10B B5B 60.6(4) . . ?
B6B B10B B9B 108.4(5) . . ?
B6B B10B H10B 118(3) . . ?
B6B B10B B11B 59.8(4) . . ?
B6B B10B B12B 107.5(4) . . ?
B9B B10B B5B 59.8(4) . . ?
B9B B10B H10B 126(3) . . ?
B9B B10B B11B 107.8(5) . . ?
B9B B10B B12B 60.0(4) . . ?
B11B B10B B5B 107.9(4) . . ?
B11B B10B H10B 119(3) . . ?
B12B B10B B5B 107.5(5) . . ?
B12B B10B H10B 124(3) . . ?
B12B B10B B11B 59.5(4) . . ?
C2B B11B B6B 60.2(3) . . ?
C2B B11B B7B 59.3(3) . . ?
C2B B11B B10B 104.6(4) . . ?
C2B B11B H11B 118(3) . . ?
C2B B11B B12B 104.3(5) . . ?
B6B B11B B7B 109.4(5) . . ?
B6B B11B B10B 58.0(4) . . ?
B6B B11B H11B 119(3) . . ?
B6B B11B B12B 106.5(5) . . ?
B7B B11B B10B 108.2(5) . . ?
B7B B11B H11B 119(3) . . ?
B7B B11B B12B 59.6(4) . . ?
B10B B11B H11B 127(3) . . ?
B12B B11B B10B 60.0(4) . . ?
B12B B11B H11B 129(3) . . ?
B7B B12B B8B 61.2(4) . . ?
B7B B12B B9B 109.3(5) . . ?
B7B B12B B10B 109.1(5) . . ?
B7B B12B B11B 60.1(4) . . ?
B7B B12B H12B 118(3) . . ?
B8B B12B B9B 60.2(4) . . ?
B8B B12B B10B 108.8(5) . . ?
B8B B12B H12B 118(3) . . ?
B9B B12B B10B 60.0(4) . . ?
B9B B12B H12B 123(3) . . ?
B10B B12B H12B 125(3) . . ?
B11B B12B B8B 109.2(5) . . ?
B11B B12B B9B 108.6(5) . . ?
B11B B12B B10B 60.5(4) . . ?
B11B B12B H12B 122(3) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
P1C C2D B3D C1D 104.4(4) . . . . ?
P1C C2D B3D B4D 138.4(4) . . . . ?
P1C C2D B3D B7D -116.6(4) . . . . ?
P1C C2D B3D B8D -157.5(3) . . . . ?
P1C C2D B6D C1D -98.5(4) . . . . ?
P1C C2D B6D B5D -132.3(4) . . . . ?
P1C C2D B6D B10D 163.2(4) . . . . ?
P1C C2D B6D B11D 121.9(5) . . . . ?
P1C C2D B7D B3D 95.8(4) . . . . ?
P1C C2D B7D B8D 134.9(4) . . . . ?
P1C C2D B7D B11D -122.5(4) . . . . ?
P1C C2D B7D B12D -162.4(4) . . . . ?
P1C C2D B11D B6D -109.6(5) . . . . ?
P1C C2D B11D B7D 109.2(5) . . . . ?
P1C C2D B11D B10D -148.7(4) . . . . ?
P1C C2D B11D B12D 149.3(4) . . . . ?
P1C C2C B3C C1C 99.8(4) . . . . ?
P1C C2C B3C B4C 134.9(4) . . . . ?
P1C C2C B3C B7C -120.9(4) . . . . ?
P1C C2C B3C B8C -162.1(4) . . . . ?
P1C C2C B6C C1C -103.7(4) . . . . ?
P1C C2C B6C B5C -138.8(4) . . . . ?
P1C C2C B6C B10C 156.9(4) . . . . ?
P1C C2C B6C B11C 116.0(4) . . . . ?
P1C C2C B7C B3C 107.9(5) . . . . ?
P1C C2C B7C B8C 147.1(4) . . . . ?
P1C C2C B7C B11C -110.0(5) . . . . ?
P1C C2C B7C B12C -150.3(4) . . . . ?
P1C C2C B11C B6C -97.9(4) . . . . ?
P1C C2C B11C B7C 120.8(4) . . . . ?
P1C C2C B11C B10C -136.7(4) . . . . ?
P1C C2C B11C B12C 161.0(4) . . . . ?
C1D C2D B3D B4D 34.0(4) . . . . ?
C1D C2D B3D B7D 139.0(4) . . . . ?
C1D C2D B3D B8D 98.1(4) . . . . ?
C1D C2D B6D B5D -33.8(4) . . . . ?
C1D C2D B6D B10D -98.3(4) . . . . ?
C1D C2D B6D B11D -139.6(4) . . . . ?
C1D C2D B7D B3D -38.6(4) . . . . ?
C1D C2D B7D B8D 0.5(5) . . . . ?
C1D C2D B7D B11D 103.1(4) . . . . ?
C1D C2D B7D B12D 63.1(5) . . . . ?
C1D C2D B11D B6D 38.0(4) . . . . ?
C1D C2D B11D B7D -103.3(4) . . . . ?
C1D C2D B11D B10D -1.1(5) . . . . ?
C1D C2D B11D B12D -63.2(5) . . . . ?
C1D B3D B4D B5D 34.5(4) . . . . ?
C1D B3D B4D B8D 134.3(4) . . . . ?
C1D B3D B4D B9D 97.3(4) . . . . ?
C1D B3D B7D C2D 34.4(4) . . . . ?
C1D B3D B7D B8D -100.1(4) . . . . ?
C1D B3D B7D B11D 0.3(6) . . . . ?
C1D B3D B7D B12D -63.4(5) . . . . ?
C1D B3D B8D B4D -39.4(4) . . . . ?
C1D B3D B8D B7D 98.7(4) . . . . ?
C1D B3D B8D B9D -1.3(6) . . . . ?
C1D B3D B8D B12D 62.3(5) . . . . ?
C1D B4D B5D B6D 36.1(4) . . . . ?
C1D B4D B5D B9D 133.9(4) . . . . ?
C1D B4D B5D B10D 97.0(4) . . . . ?
C1D B4D B8D B3D 40.5(4) . . . . ?
C1D B4D B8D B7D 3.3(5) . . . . ?
C1D B4D B8D B9D -97.3(5) . . . . ?
C1D B4D B8D B12D -59.6(5) . . . . ?
C1D B4D B9D B5D -39.1(4) . . . . ?
C1D B4D B9D B8D 100.0(4) . . . . ?
C1D B4D B9D B10D -1.1(5) . . . . ?
C1D B4D B9D B12D 62.4(5) . . . . ?
C1D B5D B6D C2D 33.0(3) . . . . ?
C1D B5D B6D B10D 134.3(4) . . . . ?
C1D B5D B6D B11D 94.5(4) . . . . ?
C1D B5D B9D B4D 39.5(4) . . . . ?
C1D B5D B9D B8D 2.8(5) . . . . ?
C1D B5D B9D B10D -98.5(4) . . . . ?
C1D B5D B9D B12D -61.3(5) . . . . ?
C1D B5D B10D B6D -40.2(4) . . . . ?
C1D B5D B10D B9D 98.7(4) . . . . ?
C1D B5D B10D B11D -2.3(5) . . . . ?
C1D B5D B10D B12D 61.0(5) . . . . ?
C1D B6D B10D B5D 39.1(4) . . . . ?
C1D B6D B10D B9D 2.0(6) . . . . ?
C1D B6D B10D B11D -98.2(4) . . . . ?
C1D B6D B10D B12D -62.5(5) . . . . ?
C1D B6D B11D C2D -33.7(4) . . . . ?
C1D B6D B11D B7D 1.3(6) . . . . ?
C1D B6D B11D B10D 100.5(4) . . . . ?
C1D B6D B11D B12D 65.1(5) . . . . ?
C1D C1C C2C P1C -4.8(5) . . . . ?
C1D C1C C2C B3C 110.0(4) . . . . ?
C1D C1C C2C B6C -108.3(4) . . . . ?
C1D C1C C2C B7C 147.9(4) . . . . ?
C1D C1C C2C B11C -145.1(4) . . . . ?
C1D C1C B3C C2C -101.5(4) . . . . ?
C1D C1C B3C B4C 119.5(5) . . . . ?
C1D C1C B3C B7C -136.9(4) . . . . ?
C1D C1C B3C B8C 159.1(4) . . . . ?
C1D C1C B4C B3C -104.0(5) . . . . ?
C1D C1C B4C B5C 114.7(5) . . . . ?
C1D C1C B4C B8C -142.5(5) . . . . ?
C1D C1C B4C B9C 154.7(5) . . . . ?
C1D C1C B5C B4C -117.5(5) . . . . ?
C1D C1C B5C B6C 102.5(5) . . . . ?
C1D C1C B5C B9C -157.4(4) . . . . ?
C1D C1C B5C B10C 140.8(4) . . . . ?
C1D C1C B6C C2C 102.4(4) . . . . ?
C1D C1C B6C B5C -117.8(5) . . . . ?
C1D C1C B6C B10C -158.0(4) . . . . ?
C1D C1C B6C B11C 137.4(4) . . . . ?
C2D P1C C11C C12C -90.2(4) . . . . ?
C2D P1C C2C C1C 8.4(4) . . . . ?
C2D P1C C2C B3C -62.0(4) . . . . ?
C2D P1C C2C B6C 75.7(4) . . . . ?
C2D P1C C2C B7C -138.3(5) . . . . ?
C2D P1C C2C B11C 143.7(4) . . . . ?
C2D C1D B3D B4D -140.7(4) . . . . ?
C2D C1D B3D B7D -35.8(4) . . . . ?
C2D C1D B3D B8D -99.9(4) . . . . ?
C2D C1D B4D B3D 36.4(4) . . . . ?
C2D C1D B4D B5D -104.4(4) . . . . ?
C2D C1D B4D B8D -3.1(5) . . . . ?
C2D C1D B4D B9D -64.6(5) . . . . ?
C2D C1D B5D B4D 103.1(4) . . . . ?
C2D C1D B5D B6D -37.1(4) . . . . ?
C2D C1D B5D B9D 62.8(5) . . . . ?
C2D C1D B5D B10D 1.6(5) . . . . ?
C2D C1D B6D B5D 140.4(4) . . . . ?
C2D C1D B6D B10D 99.4(4) . . . . ?
C2D C1D B6D B11D 34.9(4) . . . . ?
C2D C1D C1C C2C -2.3(5) . . . . ?
C2D C1D C1C B3C 65.7(5) . . . . ?
C2D C1D C1C B4C 139.0(5) . . . . ?
C2D C1D C1C B5C -141.8(4) . . . . ?
C2D C1D C1C B6C -70.3(5) . . . . ?
C2D B3D B4D C1D -33.1(4) . . . . ?
C2D B3D B4D B5D 1.5(5) . . . . ?
C2D B3D B4D B8D 101.2(4) . . . . ?
C2D B3D B4D B9D 64.2(5) . . . . ?
C2D B3D B7D B8D -134.5(4) . . . . ?
C2D B3D B7D B11D -34.1(4) . . . . ?
C2D B3D B7D B12D -97.8(5) . . . . ?
C2D B3D B8D B4D -98.2(4) . . . . ?
C2D B3D B8D B7D 39.9(4) . . . . ?
C2D B3D B8D B9D -60.2(5) . . . . ?
C2D B3D B8D B12D 3.4(6) . . . . ?
C2D B6D B10D B5D 97.6(4) . . . . ?
C2D B6D B10D B9D 60.5(5) . . . . ?
C2D B6D B10D B11D -39.7(4) . . . . ?
C2D B6D B10D B12D -4.0(5) . . . . ?
C2D B6D B11D B7D 35.0(4) . . . . ?
C2D B6D B11D B10D 134.2(4) . . . . ?
C2D B6D B11D B12D 98.9(5) . . . . ?
C2D B7D B8D B3D -39.6(4) . . . . ?
C2D B7D B8D B4D -2.4(5) . . . . ?
C2D B7D B8D B9D 61.6(5) . . . . ?
C2D B7D B8D B12D 99.3(5) . . . . ?
C2D B7D B11D B6D -35.4(4) . . . . ?
C2D B7D B11D B10D -97.2(4) . . . . ?
C2D B7D B11D B12D -134.4(4) . . . . ?
C2D B7D B12D B8D -98.7(5) . . . . ?
C2D B7D B12D B9D -61.2(5) . . . . ?
C2D B7D B12D B10D 1.6(6) . . . . ?
C2D B7D B12D B11D 39.4(4) . . . . ?
C2D B11D B12D B7D -39.8(4) . . . . ?
C2D B11D B12D B8D -2.3(5) . . . . ?
C2D B11D B12D B9D 60.6(5) . . . . ?
C2D B11D B12D B10D 98.3(4) . . . . ?
B3D C1D C2D P1C -101.6(4) . . . . ?
B3D C1D C2D B6D 141.5(4) . . . . ?
B3D C1D C2D B7D 37.9(4) . . . . ?
B3D C1D C2D B11D 104.2(4) . . . . ?
B3D C1D B4D B5D -140.8(4) . . . . ?
B3D C1D B4D B8D -39.5(4) . . . . ?
B3D C1D B4D B9D -100.9(5) . . . . ?
B3D C1D B5D B4D 36.6(4) . . . . ?
B3D C1D B5D B6D -103.6(4) . . . . ?
B3D C1D B5D B9D -3.7(5) . . . . ?
B3D C1D B5D B10D -64.9(5) . . . . ?
B3D C1D B6D C2D -36.0(4) . . . . ?
B3D C1D B6D B5D 104.4(4) . . . . ?
B3D C1D B6D B10D 63.4(5) . . . . ?
B3D C1D B6D B11D -1.1(5) . . . . ?
B3D C1D C1C C2C 65.1(5) . . . . ?
B3D C1D C1C B3C 133.1(4) . . . . ?
B3D C1D C1C B4C -153.7(4) . . . . ?
B3D C1D C1C B5C -74.4(6) . . . . ?
B3D C1D C1C B6C -2.9(6) . . . . ?
B3D C2D B6D C1D 37.1(4) . . . . ?
B3D C2D B6D B5D 3.3(5) . . . . ?
B3D C2D B6D B10D -61.1(5) . . . . ?
B3D C2D B6D B11D -102.4(5) . . . . ?
B3D C2D B7D B8D 39.2(4) . . . . ?
B3D C2D B7D B11D 141.8(5) . . . . ?
B3D C2D B7D B12D 101.8(5) . . . . ?
B3D C2D B11D B6D 105.7(4) . . . . ?
B3D C2D B11D B7D -35.5(4) . . . . ?
B3D C2D B11D B10D 66.6(5) . . . . ?
B3D C2D B11D B12D 4.6(5) . . . . ?
B3D B4D B5D C1D -35.6(4) . . . . ?
B3D B4D B5D B6D 0.5(6) . . . . ?
B3D B4D B5D B9D 98.3(5) . . . . ?
B3D B4D B5D B10D 61.4(5) . . . . ?
B3D B4D B8D B7D -37.2(4) . . . . ?
B3D B4D B8D B9D -137.8(5) . . . . ?
B3D B4D B8D B12D -100.1(5) . . . . ?
B3D B4D B9D B5D -102.4(4) . . . . ?
B3D B4D B9D B8D 36.8(4) . . . . ?
B3D B4D B9D B10D -64.3(5) . . . . ?
B3D B4D B9D B12D -0.9(5) . . . . ?
B3D B7D B8D B4D 37.2(4) . . . . ?
B3D B7D B8D B9D 101.2(5) . . . . ?
B3D B7D B8D B12D 139.0(5) . . . . ?
B3D B7D B11D C2D 34.4(4) . . . . ?
B3D B7D B11D B6D -1.0(6) . . . . ?
B3D B7D B11D B10D -62.8(5) . . . . ?
B3D B7D B11D B12D -100.0(5) . . . . ?
B3D B7D B12D B8D -36.1(4) . . . . ?
B3D B7D B12D B9D 1.4(6) . . . . ?
B3D B7D B12D B10D 64.2(5) . . . . ?
B3D B7D B12D B11D 102.0(5) . . . . ?
B3D B8D B9D B4D -37.7(4) . . . . ?
B3D B8D B9D B5D -0.9(6) . . . . ?
B3D B8D B9D B10D 63.6(5) . . . . ?
B3D B8D B9D B12D 100.4(5) . . . . ?
B3D B8D B12D B7D 36.5(4) . . . . ?
B3D B8D B12D B9D -101.2(5) . . . . ?
B3D B8D B12D B10D -64.7(5) . . . . ?
B3D B8D B12D B11D -0.8(6) . . . . ?
B4D C1D C2D P1C -137.9(4) . . . . ?
B4D C1D C2D B3D -36.2(4) . . . . ?
B4D C1D C2D B6D 105.2(4) . . . . ?
B4D C1D C2D B7D 1.6(5) . . . . ?
B4D C1D C2D B11D 68.0(5) . . . . ?
B4D C1D B3D C2D 140.7(4) . . . . ?
B4D C1D B3D B7D 104.9(5) . . . . ?
B4D C1D B3D B8D 40.8(4) . . . . ?
B4D C1D B5D B6D -140.2(4) . . . . ?
B4D C1D B5D B9D -40.3(4) . . . . ?
B4D C1D B5D B10D -101.5(4) . . . . ?
B4D C1D B6D C2D -102.2(4) . . . . ?
B4D C1D B6D B5D 38.2(4) . . . . ?
B4D C1D B6D B10D -2.8(5) . . . . ?
B4D C1D B6D B11D -67.3(5) . . . . ?
B4D C1D C1C C2C 137.4(5) . . . . ?
B4D C1D C1C B3C -154.6(4) . . . . ?
B4D C1D C1C B4C -81.4(6) . . . . ?
B4D C1D C1C B5C -2.1(7) . . . . ?
B4D C1D C1C B6C 69.4(6) . . . . ?
B4D B3D B7D C2D 95.8(4) . . . . ?
B4D B3D B7D B8D -38.7(4) . . . . ?
B4D B3D B7D B11D 61.7(6) . . . . ?
B4D B3D B7D B12D -2.0(6) . . . . ?
B4D B3D B8D B7D 138.1(5) . . . . ?
B4D B3D B8D B9D 38.1(4) . . . . ?
B4D B3D B8D B12D 101.7(5) . . . . ?
B4D B5D B6D C1D -35.2(4) . . . . ?
B4D B5D B6D C2D -2.2(5) . . . . ?
B4D B5D B6D B10D 99.1(5) . . . . ?
B4D B5D B6D B11D 59.3(5) . . . . ?
B4D B5D B9D B8D -36.8(4) . . . . ?
B4D B5D B9D B10D -138.0(5) . . . . ?
B4D B5D B9D B12D -100.8(5) . . . . ?
B4D B5D B10D B6D -101.4(4) . . . . ?
B4D B5D B10D B9D 37.5(4) . . . . ?
B4D B5D B10D B11D -63.5(5) . . . . ?
B4D B5D B10D B12D -0.2(6) . . . . ?
B4D B8D B9D B5D 36.8(4) . . . . ?
B4D B8D B9D B10D 101.3(5) . . . . ?
B4D B8D B9D B12D 138.1(5) . . . . ?
B4D B8D B12D B7D 99.8(5) . . . . ?
B4D B8D B12D B9D -37.9(4) . . . . ?
B4D B8D B12D B10D -1.5(6) . . . . ?
B4D B8D B12D B11D 62.5(5) . . . . ?
B4D B9D B10D B5D -37.7(4) . . . . ?
B4D B9D B10D B6D -0.6(6) . . . . ?
B4D B9D B10D B11D 62.8(5) . . . . ?
B4D B9D B10D B12D 100.7(5) . . . . ?
B4D B9D B12D B7D -0.3(6) . . . . ?
B4D B9D B12D B8D 37.5(4) . . . . ?
B4D B9D B12D B10D -101.4(5) . . . . ?
B4D B9D B12D B11D -63.1(5) . . . . ?
B5D C1D C2D P1C 153.8(3) . . . . ?
B5D C1D C2D B3D -104.6(4) . . . . ?
B5D C1D C2D B6D 36.9(4) . . . . ?
B5D C1D C2D B7D -66.7(5) . . . . ?
B5D C1D C2D B11D -0.3(5) . . . . ?
B5D C1D B3D C2D 103.1(4) . . . . ?
B5D C1D B3D B4D -37.6(4) . . . . ?
B5D C1D B3D B7D 67.3(5) . . . . ?
B5D C1D B3D B8D 3.2(5) . . . . ?
B5D C1D B4D B3D 140.8(4) . . . . ?
B5D C1D B4D B8D 101.3(5) . . . . ?
B5D C1D B4D B9D 39.8(4) . . . . ?
B5D C1D B6D C2D -140.4(4) . . . . ?
B5D C1D B6D B10D -41.0(4) . . . . ?
B5D C1D B6D B11D -105.5(4) . . . . ?
B5D C1D C1C C2C -141.7(4) . . . . ?
B5D C1D C1C B3C -73.7(6) . . . . ?
B5D C1D C1C B4C -0.4(7) . . . . ?
B5D C1D C1C B5C 78.8(6) . . . . ?
B5D C1D C1C B6C 150.3(4) . . . . ?
B5D B4D B8D B3D 101.4(5) . . . . ?
B5D B4D B8D B7D 64.3(5) . . . . ?
B5D B4D B8D B9D -36.3(4) . . . . ?
B5D B4D B8D B12D 1.4(6) . . . . ?
B5D B4D B9D B8D 139.1(5) . . . . ?
B5D B4D B9D B10D 38.1(4) . . . . ?
B5D B4D B9D B12D 101.5(5) . . . . ?
B5D B6D B10D B9D -37.1(4) . . . . ?
B5D B6D B10D B11D -137.3(4) . . . . ?
B5D B6D B10D B12D -101.6(5) . . . . ?
B5D B6D B11D C2D -94.4(4) . . . . ?
B5D B6D B11D B7D -59.4(5) . . . . ?
B5D B6D B11D B10D 39.7(4) . . . . ?
B5D B6D B11D B12D 4.4(6) . . . . ?
B5D B9D B10D B6D 37.2(4) . . . . ?
B5D B9D B10D B11D 100.5(5) . . . . ?
B5D B9D B10D B12D 138.5(5) . . . . ?
B5D B9D B12D B7D 63.4(5) . . . . ?
B5D B9D B12D B8D 101.3(5) . . . . ?
B5D B9D B12D B10D -37.7(4) . . . . ?
B5D B9D B12D B11D 0.6(6) . . . . ?
B5D B10D B11D C2D 2.1(5) . . . . ?
B5D B10D B11D B6D -38.2(4) . . . . ?
B5D B10D B11D B7D 64.5(5) . . . . ?
B5D B10D B11D B12D 101.9(5) . . . . ?
B5D B10D B12D B7D -62.7(6) . . . . ?
B5D B10D B12D B8D 1.0(6) . . . . ?
B5D B10D B12D B9D 37.5(4) . . . . ?
B5D B10D B12D B11D -99.9(5) . . . . ?
B6D C1D C2D P1C 116.9(4) . . . . ?
B6D C1D C2D B3D -141.5(4) . . . . ?
B6D C1D C2D B7D -103.6(4) . . . . ?
B6D C1D C2D B11D -37.2(4) . . . . ?
B6D C1D B3D C2D 36.3(4) . . . . ?
B6D C1D B3D B4D -104.4(4) . . . . ?
B6D C1D B3D B7D 0.5(5) . . . . ?
B6D C1D B3D B8D -63.6(5) . . . . ?
B6D C1D B4D B3D 103.3(4) . . . . ?
B6D C1D B4D B5D -37.4(4) . . . . ?
B6D C1D B4D B8D 63.9(5) . . . . ?
B6D C1D B4D B9D 2.4(5) . . . . ?
B6D C1D B5D B4D 140.2(4) . . . . ?
B6D C1D B5D B9D 99.9(4) . . . . ?
B6D C1D B5D B10D 38.7(4) . . . . ?
B6D C1D C1C C2C -70.0(5) . . . . ?
B6D C1D C1C B3C -2.0(6) . . . . ?
B6D C1D C1C B4C 71.3(6) . . . . ?
B6D C1D C1C B5C 150.6(4) . . . . ?
B6D C1D C1C B6C -138.0(4) . . . . ?
B6D C2D B3D C1D -37.0(4) . . . . ?
B6D C2D B3D B4D -3.1(5) . . . . ?
B6D C2D B3D B7D 102.0(5) . . . . ?
B6D C2D B3D B8D 61.1(5) . . . . ?
B6D C2D B7D B3D -106.0(4) . . . . ?
B6D C2D B7D B8D -66.8(5) . . . . ?
B6D C2D B7D B11D 35.7(4) . . . . ?
B6D C2D B7D B12D -4.2(6) . . . . ?
B6D C2D B11D B7D -141.3(4) . . . . ?
B6D C2D B11D B10D -39.1(4) . . . . ?
B6D C2D B11D B12D -101.2(4) . . . . ?
B6D B5D B9D B4D 102.8(4) . . . . ?
B6D B5D B9D B8D 66.0(5) . . . . ?
B6D B5D B9D B10D -35.2(4) . . . . ?
B6D B5D B9D B12D 2.0(5) . . . . ?
B6D B5D B10D B9D 138.9(5) . . . . ?
B6D B5D B10D B11D 38.0(4) . . . . ?
B6D B5D B10D B12D 101.3(5) . . . . ?
B6D B10D B11D C2D 40.3(4) . . . . ?
B6D B10D B11D B7D 102.7(5) . . . . ?
B6D B10D B11D B12D 140.2(5) . . . . ?
B6D B10D B12D B7D 1.5(6) . . . . ?
B6D B10D B12D B8D 65.2(5) . . . . ?
B6D B10D B12D B9D 101.6(5) . . . . ?
B6D B10D B12D B11D -35.8(4) . . . . ?
B6D B11D B12D B7D -103.4(5) . . . . ?
B6D B11D B12D B8D -65.9(5) . . . . ?
B6D B11D B12D B9D -3.0(6) . . . . ?
B6D B11D B12D B10D 34.7(4) . . . . ?
B7D C2D B3D C1D -139.0(4) . . . . ?
B7D C2D B3D B4D -105.0(5) . . . . ?
B7D C2D B3D B8D -40.9(4) . . . . ?
B7D C2D B6D C1D 103.5(4) . . . . ?
B7D C2D B6D B5D 69.7(5) . . . . ?
B7D C2D B6D B10D 5.2(5) . . . . ?
B7D C2D B6D B11D -36.1(4) . . . . ?
B7D C2D B11D B6D 141.3(4) . . . . ?
B7D C2D B11D B10D 102.2(5) . . . . ?
B7D C2D B11D B12D 40.1(4) . . . . ?
B7D B3D B4D C1D -95.5(4) . . . . ?
B7D B3D B4D B5D -61.0(5) . . . . ?
B7D B3D B4D B8D 38.7(4) . . . . ?
B7D B3D B4D B9D 1.8(6) . . . . ?
B7D B3D B8D B4D -138.1(5) . . . . ?
B7D B3D B8D B9D -100.0(5) . . . . ?
B7D B3D B8D B12D -36.4(4) . . . . ?
B7D B8D B9D B4D -100.6(5) . . . . ?
B7D B8D B9D B5D -63.9(5) . . . . ?
B7D B8D B9D B10D 0.7(6) . . . . ?
B7D B8D B9D B12D 37.5(4) . . . . ?
B7D B8D B12D B9D -137.7(5) . . . . ?
B7D B8D B12D B10D -101.2(5) . . . . ?
B7D B8D B12D B11D -37.2(4) . . . . ?
B7D B11D B12D B8D 37.6(4) . . . . ?
B7D B11D B12D B9D 100.4(5) . . . . ?
B7D B11D B12D B10D 138.1(5) . . . . ?
B8D B3D B4D C1D -134.3(4) . . . . ?
B8D B3D B4D B5D -99.7(5) . . . . ?
B8D B3D B4D B9D -37.0(4) . . . . ?
B8D B3D B7D C2D 134.5(4) . . . . ?
B8D B3D B7D B11D 100.4(5) . . . . ?
B8D B3D B7D B12D 36.7(4) . . . . ?
B8D B4D B5D C1D -97.7(4) . . . . ?
B8D B4D B5D B6D -61.6(5) . . . . ?
B8D B4D B5D B9D 36.2(4) . . . . ?
B8D B4D B5D B10D -0.7(6) . . . . ?
B8D B4D B9D B5D -139.1(5) . . . . ?
B8D B4D B9D B10D -101.1(5) . . . . ?
B8D B4D B9D B12D -37.6(4) . . . . ?
B8D B7D B11D C2D 96.8(5) . . . . ?
B8D B7D B11D B6D 61.4(5) . . . . ?
B8D B7D B11D B10D -0.4(6) . . . . ?
B8D B7D B11D B12D -37.6(4) . . . . ?
B8D B7D B12D B9D 37.5(4) . . . . ?
B8D B7D B12D B10D 100.4(5) . . . . ?
B8D B7D B12D B11D 138.1(4) . . . . ?
B8D B9D B10D B5D -101.5(5) . . . . ?
B8D B9D B10D B6D -64.3(5) . . . . ?
B8D B9D B10D B11D -0.9(5) . . . . ?
B8D B9D B10D B12D 37.0(4) . . . . ?
B8D B9D B12D B7D -37.8(4) . . . . ?
B8D B9D B12D B10D -138.9(5) . . . . ?
B8D B9D B12D B11D -100.7(5) . . . . ?
B9D B4D B5D C1D -133.9(4) . . . . ?
B9D B4D B5D B6D -97.8(4) . . . . ?
B9D B4D B5D B10D -36.9(4) . . . . ?
B9D B4D B8D B3D 137.8(5) . . . . ?
B9D B4D B8D B7D 100.6(5) . . . . ?
B9D B4D B8D B12D 37.7(4) . . . . ?
B9D B5D B6D C1D -98.5(4) . . . . ?
B9D B5D B6D C2D -65.5(5) . . . . ?
B9D B5D B6D B10D 35.8(4) . . . . ?
B9D B5D B6D B11D -4.0(5) . . . . ?
B9D B5D B10D B6D -138.9(5) . . . . ?
B9D B5D B10D B11D -100.9(5) . . . . ?
B9D B5D B10D B12D -37.6(4) . . . . ?
B9D B8D B12D B7D 137.7(5) . . . . ?
B9D B8D B12D B10D 36.4(4) . . . . ?
B9D B8D B12D B11D 100.4(5) . . . . ?
B9D B10D B11D C2D -61.5(5) . . . . ?
B9D B10D B11D B6D -101.8(5) . . . . ?
B9D B10D B11D B7D 0.8(6) . . . . ?
B9D B10D B11D B12D 38.3(4) . . . . ?
B9D B10D B12D B7D -100.1(5) . . . . ?
B9D B10D B12D B8D -36.5(4) . . . . ?
B9D B10D B12D B11D -137.4(5) . . . . ?
B10D B5D B6D C1D -134.3(4) . . . . ?
B10D B5D B6D C2D -101.3(4) . . . . ?
B10D B5D B6D B11D -39.8(4) . . . . ?
B10D B5D B9D B4D 138.0(5) . . . . ?
B10D B5D B9D B8D 101.2(5) . . . . ?
B10D B5D B9D B12D 37.2(4) . . . . ?
B10D B6D B11D C2D -134.2(4) . . . . ?
B10D B6D B11D B7D -99.2(5) . . . . ?
B10D B6D B11D B12D -35.3(4) . . . . ?
B10D B9D B12D B7D 101.1(5) . . . . ?
B10D B9D B12D B8D 138.9(5) . . . . ?
B10D B9D B12D B11D 38.3(4) . . . . ?
B10D B11D B12D B7D -138.1(5) . . . . ?
B10D B11D B12D B8D -100.6(5) . . . . ?
B10D B11D B12D B9D -37.7(4) . . . . ?
C11C P1C C2D C1D -112.3(3) . . . . ?
C11C P1C C2D B3D -179.6(3) . . . . ?
C11C P1C C2D B6D -42.4(4) . . . . ?
C11C P1C C2D B7D 113.3(4) . . . . ?
C11C P1C C2D B11D 35.1(5) . . . . ?
C11C P1C C2C C1C 112.6(4) . . . . ?
C11C P1C C2C B3C 42.2(4) . . . . ?
C11C P1C C2C B6C 179.9(4) . . . . ?
C11C P1C C2C B7C -34.1(5) . . . . ?
C11C P1C C2C B11C -112.1(4) . . . . ?
B11D C2D B3D C1D -103.2(4) . . . . ?
B11D C2D B3D B4D -69.2(5) . . . . ?
B11D C2D B3D B7D 35.8(4) . . . . ?
B11D C2D B3D B8D -5.1(5) . . . . ?
B11D C2D B6D C1D 139.6(4) . . . . ?
B11D C2D B6D B5D 105.8(4) . . . . ?
B11D C2D B6D B10D 41.3(4) . . . . ?
B11D C2D B7D B3D -141.8(5) . . . . ?
B11D C2D B7D B8D -102.6(5) . . . . ?
B11D C2D B7D B12D -40.0(4) . . . . ?
B11D B6D B10D B5D 137.3(4) . . . . ?
B11D B6D B10D B9D 100.2(5) . . . . ?
B11D B6D B10D B12D 35.7(4) . . . . ?
B11D B7D B8D B3D -101.3(5) . . . . ?
B11D B7D B8D B4D -64.1(5) . . . . ?
B11D B7D B8D B9D -0.1(6) . . . . ?
B11D B7D B8D B12D 37.6(4) . . . . ?
B11D B7D B12D B8D -138.1(4) . . . . ?
B11D B7D B12D B9D -100.6(5) . . . . ?
B11D B7D B12D B10D -37.7(4) . . . . ?
B11D B10D B12D B7D 37.3(4) . . . . ?
B11D B10D B12D B8D 100.9(5) . . . . ?
B11D B10D B12D B9D 137.4(5) . . . . ?
B12D B7D B8D B3D -139.0(5) . . . . ?
B12D B7D B8D B4D -101.7(5) . . . . ?
B12D B7D B8D B9D -37.8(4) . . . . ?
B12D B7D B11D C2D 134.4(4) . . . . ?
B12D B7D B11D B6D 99.0(5) . . . . ?
B12D B7D B11D B10D 37.2(4) . . . . ?
B12D B8D B9D B4D -138.1(5) . . . . ?
B12D B8D B9D B5D -101.3(5) . . . . ?
B12D B8D B9D B10D -36.8(4) . . . . ?
B12D B9D B10D B5D -138.5(5) . . . . ?
B12D B9D B10D B6D -101.3(5) . . . . ?
B12D B9D B10D B11D -37.9(4) . . . . ?
B12D B10D B11D C2D -99.8(5) . . . . ?
B12D B10D B11D B6D -140.2(5) . . . . ?
B12D B10D B11D B7D -37.5(4) . . . . ?
C1C C1D C2D P1C 8.5(5) . . . . ?
C1C C1D C2D B3D 110.1(4) . . . . ?
C1C C1D C2D B6D -108.4(4) . . . . ?
C1C C1D C2D B7D 148.0(4) . . . . ?
C1C C1D C2D B11D -145.6(4) . . . . ?
C1C C1D B3D C2D -100.3(4) . . . . ?
C1C C1D B3D B4D 119.0(5) . . . . ?
C1C C1D B3D B7D -136.1(4) . . . . ?
C1C C1D B3D B8D 159.9(4) . . . . ?
C1C C1D B4D B3D -103.4(5) . . . . ?
C1C C1D B4D B5D 115.9(5) . . . . ?
C1C C1D B4D B8D -142.8(5) . . . . ?
C1C C1D B4D B9D 155.7(4) . . . . ?
C1C C1D B5D B4D -117.6(5) . . . . ?
C1C C1D B5D B6D 102.2(5) . . . . ?
C1C C1D B5D B9D -158.0(4) . . . . ?
C1C C1D B5D B10D 140.9(5) . . . . ?
C1C C1D B6D C2D 101.2(4) . . . . ?
C1C C1D B6D B5D -118.3(4) . . . . ?
C1C C1D B6D B10D -159.3(4) . . . . ?
C1C C1D B6D B11D 136.2(4) . . . . ?
C1C C2C B3C B4C 35.1(4) . . . . ?
C1C C2C B3C B7C 139.3(4) . . . . ?
C1C C2C B3C B8C 98.1(4) . . . . ?
C1C C2C B6C B5C -35.1(4) . . . . ?
C1C C2C B6C B10C -99.4(4) . . . . ?
C1C C2C B6C B11C -140.3(4) . . . . ?
C1C C2C B7C B3C -38.7(4) . . . . ?
C1C C2C B7C B8C 0.6(5) . . . . ?
C1C C2C B7C B11C 103.4(4) . . . . ?
C1C C2C B7C B12C 63.1(5) . . . . ?
C1C C2C B11C B6C 37.4(4) . . . . ?
C1C C2C B11C B7C -103.9(4) . . . . ?
C1C C2C B11C B10C -1.4(5) . . . . ?
C1C C2C B11C B12C -63.8(5) . . . . ?
C1C B3C B4C B5C 34.7(4) . . . . ?
C1C B3C B4C B8C 135.2(4) . . . . ?
C1C B3C B4C B9C 98.4(4) . . . . ?
C1C B3C B7C C2C 33.9(3) . . . . ?
C1C B3C B7C B8C -100.1(4) . . . . ?
C1C B3C B7C B11C -0.2(5) . . . . ?
C1C B3C B7C B12C -63.7(5) . . . . ?
C1C B3C B8C B4C -38.6(4) . . . . ?
C1C B3C B8C B7C 98.4(4) . . . . ?
C1C B3C B8C B9C -1.2(5) . . . . ?
C1C B3C B8C B12C 62.2(5) . . . . ?
C1C B4C B5C B6C 35.7(4) . . . . ?
C1C B4C B5C B9C 134.5(4) . . . . ?
C1C B4C B5C B10C 97.3(4) . . . . ?
C1C B4C B8C B3C 39.5(4) . . . . ?
C1C B4C B8C B7C 1.0(5) . . . . ?
C1C B4C B8C B9C -99.3(4) . . . . ?
C1C B4C B8C B12C -62.0(5) . . . . ?
C1C B4C B9C B5C -39.5(4) . . . . ?
C1C B4C B9C B8C 99.2(4) . . . . ?
C1C B4C B9C B10C -2.0(6) . . . . ?
C1C B4C B9C B12C 61.7(5) . . . . ?
C1C B5C B6C C2C 33.8(4) . . . . ?
C1C B5C B6C B10C 135.4(4) . . . . ?
C1C B5C B6C B11C 96.7(5) . . . . ?
C1C B5C B9C B4C 39.3(4) . . . . ?
C1C B5C B9C B8C 2.7(6) . . . . ?
C1C B5C B9C B10C -98.8(5) . . . . ?
C1C B5C B9C B12C -60.9(5) . . . . ?
C1C B5C B10C B6C -38.9(4) . . . . ?
C1C B5C B10C B9C 99.0(4) . . . . ?
C1C B5C B10C B11C -1.7(5) . . . . ?
C1C B5C B10C B12C 61.3(5) . . . . ?
C1C B6C B10C B5C 39.1(4) . . . . ?
C1C B6C B10C B9C 1.3(6) . . . . ?
C1C B6C B10C B11C -99.1(4) . . . . ?
C1C B6C B10C B12C -62.0(5) . . . . ?
C1C B6C B11C C2C -33.6(3) . . . . ?
C1C B6C B11C B7C 0.7(5) . . . . ?
C1C B6C B11C B10C 101.2(4) . . . . ?
C1C B6C B11C B12C 64.0(5) . . . . ?
C2C P1C C2D C1D -9.7(3) . . . . ?
C2C P1C C2D B3D -76.9(3) . . . . ?
C2C P1C C2D B6D 60.3(4) . . . . ?
C2C P1C C2D B7D -144.1(4) . . . . ?
C2C P1C C2D B11D 137.8(5) . . . . ?
C2C P1C C11C C12C 173.7(4) . . . . ?
C2C C1C B3C B4C -139.0(4) . . . . ?
C2C C1C B3C B7C -35.4(4) . . . . ?
C2C C1C B3C B8C -99.3(4) . . . . ?
C2C C1C B4C B3C 37.9(4) . . . . ?
C2C C1C B4C B5C -103.5(4) . . . . ?
C2C C1C B4C B8C -0.7(5) . . . . ?
C2C C1C B4C B9C -63.5(5) . . . . ?
C2C C1C B5C B4C 102.6(4) . . . . ?
C2C C1C B5C B6C -37.4(4) . . . . ?
C2C C1C B5C B9C 62.7(5) . . . . ?
C2C C1C B5C B10C 0.9(5) . . . . ?
C2C C1C B6C B5C 139.8(4) . . . . ?
C2C C1C B6C B10C 99.6(5) . . . . ?
C2C C1C B6C B11C 35.0(4) . . . . ?
C2C B3C B4C C1C -34.0(3) . . . . ?
C2C B3C B4C B5C 0.6(5) . . . . ?
C2C B3C B4C B8C 101.1(4) . . . . ?
C2C B3C B4C B9C 64.4(5) . . . . ?
C2C B3C B7C B8C -134.0(4) . . . . ?
C2C B3C B7C B11C -34.1(4) . . . . ?
C2C B3C B7C B12C -97.6(4) . . . . ?
C2C B3C B8C B4C -96.9(4) . . . . ?
C2C B3C B8C B7C 40.1(4) . . . . ?
C2C B3C B8C B9C -59.6(5) . . . . ?
C2C B3C B8C B12C 3.8(5) . . . . ?
C2C B6C B10C B5C 98.3(4) . . . . ?
C2C B6C B10C B9C 60.5(5) . . . . ?
C2C B6C B10C B11C -39.9(4) . . . . ?
C2C B6C B10C B12C -2.8(6) . . . . ?
C2C B6C B11C B7C 34.3(4) . . . . ?
C2C B6C B11C B10C 134.8(4) . . . . ?
C2C B6C B11C B12C 97.5(4) . . . . ?
C2C B7C B8C B3C -39.9(4) . . . . ?
C2C B7C B8C B4C -0.9(5) . . . . ?
C2C B7C B8C B9C 62.8(5) . . . . ?
C2C B7C B8C B12C 99.5(4) . . . . ?
C2C B7C B11C B6C -34.6(4) . . . . ?
C2C B7C B11C B10C -96.6(4) . . . . ?
C2C B7C B11C B12C -133.9(5) . . . . ?
C2C B7C B12C B8C -98.0(4) . . . . ?
C2C B7C B12C B9C -60.9(5) . . . . ?
C2C B7C B12C B10C 2.5(6) . . . . ?
C2C B7C B12C B11C 39.9(4) . . . . ?
C2C B11C B12C B7C -39.6(4) . . . . ?
C2C B11C B12C B8C -2.0(6) . . . . ?
C2C B11C B12C B9C 61.6(5) . . . . ?
C2C B11C B12C B10C 98.7(4) . . . . ?
B3C C1C C2C P1C -114.9(4) . . . . ?
B3C C1C C2C B6C 141.7(4) . . . . ?
B3C C1C C2C B7C 37.9(4) . . . . ?
B3C C1C C2C B11C 104.9(4) . . . . ?
B3C C1C B4C B5C -141.3(5) . . . . ?
B3C C1C B4C B8C -38.5(4) . . . . ?
B3C C1C B4C B9C -101.3(5) . . . . ?
B3C C1C B5C B4C 36.3(4) . . . . ?
B3C C1C B5C B6C -103.7(4) . . . . ?
B3C C1C B5C B9C -3.6(6) . . . . ?
B3C C1C B5C B10C -65.5(5) . . . . ?
B3C C1C B6C C2C -35.9(4) . . . . ?
B3C C1C B6C B5C 103.9(4) . . . . ?
B3C C1C B6C B10C 63.7(5) . . . . ?
B3C C1C B6C B11C -0.9(5) . . . . ?
B3C C2C B6C C1C 37.1(4) . . . . ?
B3C C2C B6C B5C 2.0(6) . . . . ?
B3C C2C B6C B10C -62.3(5) . . . . ?
B3C C2C B6C B11C -103.1(5) . . . . ?
B3C C2C B7C B8C 39.2(4) . . . . ?
B3C C2C B7C B11C 142.0(4) . . . . ?
B3C C2C B7C B12C 101.8(5) . . . . ?
B3C C2C B11C B6C 105.8(4) . . . . ?
B3C C2C B11C B7C -35.6(4) . . . . ?
B3C C2C B11C B10C 67.0(5) . . . . ?
B3C C2C B11C B12C 4.6(6) . . . . ?
B3C B4C B5C C1C -35.2(4) . . . . ?
B3C B4C B5C B6C 0.5(6) . . . . ?
B3C B4C B5C B9C 99.3(5) . . . . ?
B3C B4C B5C B10C 62.2(5) . . . . ?
B3C B4C B8C B7C -38.5(4) . . . . ?
B3C B4C B8C B9C -138.9(5) . . . . ?
B3C B4C B8C B12C -101.5(4) . . . . ?
B3C B4C B9C B5C -102.8(5) . . . . ?
B3C B4C B9C B8C 35.9(4) . . . . ?
B3C B4C B9C B10C -65.2(5) . . . . ?
B3C B4C B9C B12C -1.6(5) . . . . ?
B3C B7C B8C B4C 38.9(4) . . . . ?
B3C B7C B8C B9C 102.7(5) . . . . ?
B3C B7C B8C B12C 139.4(4) . . . . ?
B3C B7C B11C C2C 34.2(4) . . . . ?
B3C B7C B11C B6C -0.4(6) . . . . ?
B3C B7C B11C B10C -62.4(5) . . . . ?
B3C B7C B11C B12C -99.7(5) . . . . ?
B3C B7C B12C B8C -35.6(4) . . . . ?
B3C B7C B12C B9C 1.6(5) . . . . ?
B3C B7C B12C B10C 64.9(5) . . . . ?
B3C B7C B12C B11C 102.4(5) . . . . ?
B3C B8C B9C B4C -37.6(4) . . . . ?
B3C B8C B9C B5C -0.9(6) . . . . ?
B3C B8C B9C B10C 62.7(5) . . . . ?
B3C B8C B9C B12C 100.4(5) . . . . ?
B3C B8C B12C B7C 36.5(4) . . . . ?
B3C B8C B12C B9C -102.2(5) . . . . ?
B3C B8C B12C B10C -64.9(5) . . . . ?
B3C B8C B12C B11C -1.2(6) . . . . ?
B4C C1C C2C P1C -152.7(3) . . . . ?
B4C C1C C2C B3C -37.9(4) . . . . ?
B4C C1C C2C B6C 103.8(4) . . . . ?
B4C C1C C2C B7C 0.1(5) . . . . ?
B4C C1C C2C B11C 67.0(5) . . . . ?
B4C C1C B3C C2C 139.0(4) . . . . ?
B4C C1C B3C B7C 103.6(5) . . . . ?
B4C C1C B3C B8C 39.6(4) . . . . ?
B4C C1C B5C B6C -140.0(4) . . . . ?
B4C C1C B5C B9C -39.9(4) . . . . ?
B4C C1C B5C B10C -101.7(5) . . . . ?
B4C C1C B6C C2C -102.3(4) . . . . ?
B4C C1C B6C B5C 37.5(4) . . . . ?
B4C C1C B6C B10C -2.7(6) . . . . ?
B4C C1C B6C B11C -67.3(5) . . . . ?
B4C B3C B7C C2C 95.0(4) . . . . ?
B4C B3C B7C B8C -39.0(4) . . . . ?
B4C B3C B7C B11C 60.9(5) . . . . ?
B4C B3C B7C B12C -2.6(5) . . . . ?
B4C B3C B8C B7C 137.0(4) . . . . ?
B4C B3C B8C B9C 37.3(4) . . . . ?
B4C B3C B8C B12C 100.7(5) . . . . ?
B4C B5C B6C C1C -35.3(4) . . . . ?
B4C B5C B6C C2C -1.5(6) . . . . ?
B4C B5C B6C B10C 100.1(5) . . . . ?
B4C B5C B6C B11C 61.4(6) . . . . ?
B4C B5C B9C B8C -36.6(4) . . . . ?
B4C B5C B9C B10C -138.1(5) . . . . ?
B4C B5C B9C B12C -100.2(5) . . . . ?
B4C B5C B10C B6C -100.5(5) . . . . ?
B4C B5C B10C B9C 37.4(4) . . . . ?
B4C B5C B10C B11C -63.3(5) . . . . ?
B4C B5C B10C B12C -0.3(6) . . . . ?
B4C B8C B9C B5C 36.7(4) . . . . ?
B4C B8C B9C B10C 100.3(5) . . . . ?
B4C B8C B9C B12C 138.0(4) . . . . ?
B4C B8C B12C B7C 101.0(5) . . . . ?
B4C B8C B12C B9C -37.6(4) . . . . ?
B4C B8C B12C B10C -0.3(5) . . . . ?
B4C B8C B12C B11C 63.4(5) . . . . ?
B4C B9C B10C B5C -37.3(4) . . . . ?
B4C B9C B10C B6C 0.4(6) . . . . ?
B4C B9C B10C B11C 63.5(5) . . . . ?
B4C B9C B10C B12C 100.5(5) . . . . ?
B4C B9C B12C B7C 0.0(6) . . . . ?
B4C B9C B12C B8C 37.2(4) . . . . ?
B4C B9C B12C B10C -100.9(4) . . . . ?
B4C B9C B12C B11C -63.6(5) . . . . ?
B5C C1C C2C P1C 140.6(3) . . . . ?
B5C C1C C2C B3C -104.5(4) . . . . ?
B5C C1C C2C B6C 37.2(4) . . . . ?
B5C C1C C2C B7C -66.6(5) . . . . ?
B5C C1C C2C B11C 0.3(5) . . . . ?
B5C C1C B3C C2C 102.4(4) . . . . ?
B5C C1C B3C B4C -36.5(4) . . . . ?
B5C C1C B3C B7C 67.0(5) . . . . ?
B5C C1C B3C B8C 3.1(5) . . . . ?
B5C C1C B4C B3C 141.3(5) . . . . ?
B5C C1C B4C B8C 102.8(5) . . . . ?
B5C C1C B4C B9C 40.0(4) . . . . ?
B5C C1C B6C C2C -139.8(4) . . . . ?
B5C C1C B6C B10C -40.2(4) . . . . ?
B5C C1C B6C B11C -104.8(5) . . . . ?
B5C B4C B8C B3C 101.7(5) . . . . ?
B5C B4C B8C B7C 63.1(5) . . . . ?
B5C B4C B8C B9C -37.2(4) . . . . ?
B5C B4C B8C B12C 0.2(5) . . . . ?
B5C B4C B9C B8C 138.7(5) . . . . ?
B5C B4C B9C B10C 37.5(4) . . . . ?
B5C B4C B9C B12C 101.2(5) . . . . ?
B5C B6C B10C B9C -37.8(4) . . . . ?
B5C B6C B10C B11C -138.2(4) . . . . ?
B5C B6C B10C B12C -101.1(5) . . . . ?
B5C B6C B11C C2C -96.1(4) . . . . ?
B5C B6C B11C B7C -61.8(5) . . . . ?
B5C B6C B11C B10C 38.7(4) . . . . ?
B5C B6C B11C B12C 1.5(6) . . . . ?
B5C B9C B10C B6C 37.7(4) . . . . ?
B5C B9C B10C B11C 100.8(5) . . . . ?
B5C B9C B10C B12C 137.8(4) . . . . ?
B5C B9C B12C B7C 63.1(5) . . . . ?
B5C B9C B12C B8C 100.2(5) . . . . ?
B5C B9C B12C B10C -37.9(4) . . . . ?
B5C B9C B12C B11C -0.6(6) . . . . ?
B5C B10C B11C C2C 1.9(5) . . . . ?
B5C B10C B11C B6C -37.4(4) . . . . ?
B5C B10C B11C B7C 63.5(5) . . . . ?
B5C B10C B11C B12C 100.7(5) . . . . ?
B5C B10C B12C B7C -63.2(5) . . . . ?
B5C B10C B12C B8C 0.4(5) . . . . ?
B5C B10C B12C B9C 37.9(4) . . . . ?
B5C B10C B12C B11C -100.6(5) . . . . ?
B6C C1C C2C P1C 103.5(4) . . . . ?
B6C C1C C2C B3C -141.7(4) . . . . ?
B6C C1C C2C B7C -103.8(5) . . . . ?
B6C C1C C2C B11C -36.8(4) . . . . ?
B6C C1C B3C C2C 36.0(4) . . . . ?
B6C C1C B3C B4C -103.0(4) . . . . ?
B6C C1C B3C B7C 0.6(5) . . . . ?
B6C C1C B3C B8C -63.3(5) . . . . ?
B6C C1C B4C B3C 104.2(4) . . . . ?
B6C C1C B4C B5C -37.1(4) . . . . ?
B6C C1C B4C B8C 65.7(5) . . . . ?
B6C C1C B4C B9C 2.9(5) . . . . ?
B6C C1C B5C B4C 140.0(4) . . . . ?
B6C C1C B5C B9C 100.1(5) . . . . ?
B6C C1C B5C B10C 38.2(4) . . . . ?
B6C C2C B3C C1C -36.8(4) . . . . ?
B6C C2C B3C B4C -1.7(6) . . . . ?
B6C C2C B3C B7C 102.5(5) . . . . ?
B6C C2C B3C B8C 61.3(5) . . . . ?
B6C C2C B7C B3C -106.1(4) . . . . ?
B6C C2C B7C B8C -66.9(5) . . . . ?
B6C C2C B7C B11C 35.9(4) . . . . ?
B6C C2C B7C B12C -4.3(5) . . . . ?
B6C C2C B11C B7C -141.3(4) . . . . ?
B6C C2C B11C B10C -38.8(4) . . . . ?
B6C C2C B11C B12C -101.2(5) . . . . ?
B6C B5C B9C B4C 101.6(5) . . . . ?
B6C B5C B9C B8C 65.1(5) . . . . ?
B6C B5C B9C B10C -36.5(4) . . . . ?
B6C B5C B9C B12C 1.4(6) . . . . ?
B6C B5C B10C B9C 137.9(5) . . . . ?
B6C B5C B10C B11C 37.2(4) . . . . ?
B6C B5C B10C B12C 100.2(5) . . . . ?
B6C B10C B11C C2C 39.2(4) . . . . ?
B6C B10C B11C B7C 100.8(5) . . . . ?
B6C B10C B11C B12C 138.1(5) . . . . ?
B6C B10C B12C B7C 0.2(6) . . . . ?
B6C B10C B12C B8C 63.8(5) . . . . ?
B6C B10C B12C B9C 101.3(5) . . . . ?
B6C B10C B12C B11C -37.2(4) . . . . ?
B6C B11C B12C B7C -101.8(5) . . . . ?
B6C B11C B12C B8C -64.1(5) . . . . ?
B6C B11C B12C B9C -0.5(6) . . . . ?
B6C B11C B12C B10C 36.6(4) . . . . ?
B7C C2C B3C C1C -139.3(4) . . . . ?
B7C C2C B3C B4C -104.2(5) . . . . ?
B7C C2C B3C B8C -41.2(4) . . . . ?
B7C C2C B6C C1C 104.0(4) . . . . ?
B7C C2C B6C B5C 68.9(5) . . . . ?
B7C C2C B6C B10C 4.6(6) . . . . ?
B7C C2C B6C B11C -36.3(4) . . . . ?
B7C C2C B11C B6C 141.3(4) . . . . ?
B7C C2C B11C B10C 102.5(4) . . . . ?
B7C C2C B11C B12C 40.2(4) . . . . ?
B7C B3C B4C C1C -95.8(4) . . . . ?
B7C B3C B4C B5C -61.1(5) . . . . ?
B7C B3C B4C B8C 39.4(4) . . . . ?
B7C B3C B4C B9C 2.6(5) . . . . ?
B7C B3C B8C B4C -137.0(4) . . . . ?
B7C B3C B8C B9C -99.7(5) . . . . ?
B7C B3C B8C B12C -36.3(4) . . . . ?
B7C B8C B9C B4C -101.3(5) . . . . ?
B7C B8C B9C B5C -64.7(5) . . . . ?
B7C B8C B9C B10C -1.0(6) . . . . ?
B7C B8C B9C B12C 36.7(4) . . . . ?
B7C B8C B12C B9C -138.7(5) . . . . ?
B7C B8C B12C B10C -101.4(4) . . . . ?
B7C B8C B12C B11C -37.6(4) . . . . ?
B7C B11C B12C B8C 37.6(4) . . . . ?
B7C B11C B12C B9C 101.2(5) . . . . ?
B7C B11C B12C B10C 138.3(5) . . . . ?
B8C B3C B4C C1C -135.2(4) . . . . ?
B8C B3C B4C B5C -100.5(5) . . . . ?
B8C B3C B4C B9C -36.8(4) . . . . ?
B8C B3C B7C C2C 134.0(4) . . . . ?
B8C B3C B7C B11C 99.9(5) . . . . ?
B8C B3C B7C B12C 36.4(4) . . . . ?
B8C B4C B5C C1C -97.3(4) . . . . ?
B8C B4C B5C B6C -61.5(5) . . . . ?
B8C B4C B5C B9C 37.2(4) . . . . ?
B8C B4C B5C B10C 0.1(6) . . . . ?
B8C B4C B9C B5C -138.7(5) . . . . ?
B8C B4C B9C B10C -101.2(5) . . . . ?
B8C B4C B9C B12C -37.5(4) . . . . ?
B8C B7C B11C C2C 96.2(4) . . . . ?
B8C B7C B11C B6C 61.6(5) . . . . ?
B8C B7C B11C B10C -0.4(6) . . . . ?
B8C B7C B11C B12C -37.8(4) . . . . ?
B8C B7C B12C B9C 37.1(4) . . . . ?
B8C B7C B12C B10C 100.5(5) . . . . ?
B8C B7C B12C B11C 137.9(5) . . . . ?
B8C B9C B10C B5C -100.1(5) . . . . ?
B8C B9C B10C B6C -62.4(6) . . . . ?
B8C B9C B10C B11C 0.7(6) . . . . ?
B8C B9C B10C B12C 37.7(4) . . . . ?
B8C B9C B12C B7C -37.1(4) . . . . ?
B8C B9C B12C B10C -138.1(4) . . . . ?
B8C B9C B12C B11C -100.8(5) . . . . ?
B9C B4C B5C C1C -134.5(4) . . . . ?
B9C B4C B5C B6C -98.8(5) . . . . ?
B9C B4C B5C B10C -37.1(4) . . . . ?
B9C B4C B8C B3C 138.9(5) . . . . ?
B9C B4C B8C B7C 100.3(5) . . . . ?
B9C B4C B8C B12C 37.3(4) . . . . ?
B9C B5C B6C C1C -98.5(4) . . . . ?
B9C B5C B6C C2C -64.7(5) . . . . ?
B9C B5C B6C B10C 37.0(4) . . . . ?
B9C B5C B6C B11C -1.8(6) . . . . ?
B9C B5C B10C B6C -137.9(5) . . . . ?
B9C B5C B10C B11C -100.7(5) . . . . ?
B9C B5C B10C B12C -37.7(4) . . . . ?
B9C B8C B12C B7C 138.7(5) . . . . ?
B9C B8C B12C B10C 37.3(4) . . . . ?
B9C B8C B12C B11C 101.0(5) . . . . ?
B9C B10C B11C C2C -61.8(5) . . . . ?
B9C B10C B11C B6C -101.0(5) . . . . ?
B9C B10C B11C B7C -0.2(6) . . . . ?
B9C B10C B11C B12C 37.1(4) . . . . ?
B9C B10C B12C B7C -101.1(5) . . . . ?
B9C B10C B12C B8C -37.5(4) . . . . ?
B9C B10C B12C B11C -138.5(5) . . . . ?
B10C B5C B6C C1C -135.4(4) . . . . ?
B10C B5C B6C C2C -101.6(5) . . . . ?
B10C B5C B6C B11C -38.8(4) . . . . ?
B10C B5C B9C B4C 138.1(5) . . . . ?
B10C B5C B9C B8C 101.5(5) . . . . ?
B10C B5C B9C B12C 37.9(4) . . . . ?
B10C B6C B11C C2C -134.8(4) . . . . ?
B10C B6C B11C B7C -100.5(5) . . . . ?
B10C B6C B11C B12C -37.2(4) . . . . ?
B10C B9C B12C B7C 101.0(4) . . . . ?
B10C B9C B12C B8C 138.1(4) . . . . ?
B10C B9C B12C B11C 37.3(4) . . . . ?
B10C B11C B12C B7C -138.3(5) . . . . ?
B10C B11C B12C B8C -100.7(5) . . . . ?
B10C B11C B12C B9C -37.1(4) . . . . ?
B11C C2C B3C C1C -103.5(4) . . . . ?
B11C C2C B3C B4C -68.3(5) . . . . ?
B11C C2C B3C B7C 35.8(4) . . . . ?
B11C C2C B3C B8C -5.4(6) . . . . ?
B11C C2C B6C C1C 140.3(4) . . . . ?
B11C C2C B6C B5C 105.2(5) . . . . ?
B11C C2C B6C B10C 40.9(4) . . . . ?
B11C C2C B7C B3C -142.0(4) . . . . ?
B11C C2C B7C B8C -102.8(5) . . . . ?
B11C C2C B7C B12C -40.2(4) . . . . ?
B11C B6C B10C B5C 138.2(4) . . . . ?
B11C B6C B10C B9C 100.4(5) . . . . ?
B11C B6C B10C B12C 37.1(4) . . . . ?
B11C B7C B8C B3C -101.8(5) . . . . ?
B11C B7C B8C B4C -62.9(5) . . . . ?
B11C B7C B8C B9C 0.9(6) . . . . ?
B11C B7C B8C B12C 37.6(4) . . . . ?
B11C B7C B12C B8C -137.9(5) . . . . ?
B11C B7C B12C B9C -100.8(5) . . . . ?
B11C B7C B12C B10C -37.5(4) . . . . ?
B11C B10C B12C B7C 37.4(4) . . . . ?
B11C B10C B12C B8C 101.0(4) . . . . ?
B11C B10C B12C B9C 138.5(5) . . . . ?
B12C B7C B8C B3C -139.4(4) . . . . ?
B12C B7C B8C B4C -100.5(5) . . . . ?
B12C B7C B8C B9C -36.7(4) . . . . ?
B12C B7C B11C C2C 133.9(5) . . . . ?
B12C B7C B11C B6C 99.4(5) . . . . ?
B12C B7C B11C B10C 37.3(4) . . . . ?
B12C B8C B9C B4C -138.0(4) . . . . ?
B12C B8C B9C B5C -101.3(5) . . . . ?
B12C B8C B9C B10C -37.7(4) . . . . ?
B12C B9C B10C B5C -137.8(4) . . . . ?
B12C B9C B10C B6C -100.1(5) . . . . ?
B12C B9C B10C B11C -36.9(4) . . . . ?
B12C B10C B11C C2C -98.9(4) . . . . ?
B12C B10C B11C B6C -138.1(5) . . . . ?
B12C B10C B11C B7C -37.3(4) . . . . ?
P1A C2A B3A C1A 100.5(4) . . . . ?
P1A C2A B3A B4A 134.3(4) . . . . ?
P1A C2A B3A B7A -120.9(4) . . . . ?
P1A C2A B3A B8A -161.6(4) . . . . ?
P1A C2A B6A C1A -104.3(4) . . . . ?
P1A C2A B6A B5A -138.4(4) . . . . ?
P1A C2A B6A B10A 157.7(4) . . . . ?
P1A C2A B6A B11A 116.2(4) . . . . ?
P1A C2A B7A B3A 108.5(5) . . . . ?
P1A C2A B7A B8A 147.6(4) . . . . ?
P1A C2A B7A B11A -110.0(5) . . . . ?
P1A C2A B7A B12A -150.2(4) . . . . ?
P1A C2A B11A B6A -97.9(4) . . . . ?
P1A C2A B11A B7A 120.5(4) . . . . ?
P1A C2A B11A B10A -136.8(4) . . . . ?
P1A C2A B11A B12A 160.9(4) . . . . ?
P1A C2B B3B C1B 103.8(4) . . . . ?
P1A C2B B3B B4B 138.0(4) . . . . ?
P1A C2B B3B B7B -116.6(4) . . . . ?
P1A C2B B3B B8B -158.1(4) . . . . ?
P1A C2B B6B C1B -99.3(4) . . . . ?
P1A C2B B6B B5B -133.2(4) . . . . ?
P1A C2B B6B B10B 162.4(4) . . . . ?
P1A C2B B6B B11B 121.0(5) . . . . ?
P1A C2B B7B B3B 97.1(4) . . . . ?
P1A C2B B7B B8B 135.9(4) . . . . ?
P1A C2B B7B B11B -121.1(5) . . . . ?
P1A C2B B7B B12B -162.1(4) . . . . ?
P1A C2B B11B B6B -108.0(5) . . . . ?
P1A C2B B11B B7B 110.3(5) . . . . ?
P1A C2B B11B B10B -146.9(4) . . . . ?
P1A C2B B11B B12B 151.0(4) . . . . ?
C1A C2A B3A B4A 33.8(4) . . . . ?
C1A C2A B3A B7A 138.6(4) . . . . ?
C1A C2A B3A B8A 97.9(4) . . . . ?
C1A C2A B6A B5A -34.1(4) . . . . ?
C1A C2A B6A B10A -98.0(5) . . . . ?
C1A C2A B6A B11A -139.6(4) . . . . ?
C1A C2A B7A B3A -39.2(4) . . . . ?
C1A C2A B7A B8A -0.1(5) . . . . ?
C1A C2A B7A B11A 102.3(4) . . . . ?
C1A C2A B7A B12A 62.1(5) . . . . ?
C1A C2A B11A B6A 37.6(4) . . . . ?
C1A C2A B11A B7A -103.9(4) . . . . ?
C1A C2A B11A B10A -1.3(5) . . . . ?
C1A C2A B11A B12A -63.5(5) . . . . ?
C1A B3A B4A B5A 34.6(4) . . . . ?
C1A B3A B4A B8A 133.9(4) . . . . ?
C1A B3A B4A B9A 98.2(4) . . . . ?
C1A B3A B7A C2A 34.6(4) . . . . ?
C1A B3A B7A B8A -99.9(4) . . . . ?
C1A B3A B7A B11A -0.6(5) . . . . ?
C1A B3A B7A B12A -64.0(5) . . . . ?
C1A B3A B8A B4A -39.2(4) . . . . ?
C1A B3A B8A B7A 98.1(4) . . . . ?
C1A B3A B8A B9A -2.4(6) . . . . ?
C1A B3A B8A B12A 61.8(5) . . . . ?
C1A B4A B5A B6A 35.8(4) . . . . ?
C1A B4A B5A B9A 134.0(5) . . . . ?
C1A B4A B5A B10A 97.7(5) . . . . ?
C1A B4A B8A B3A 40.6(4) . . . . ?
C1A B4A B8A B7A 2.6(5) . . . . ?
C1A B4A B8A B9A -98.6(4) . . . . ?
C1A B4A B8A B12A -60.8(5) . . . . ?
C1A B4A B9A B5A -39.4(4) . . . . ?
C1A B4A B9A B8A 98.6(4) . . . . ?
C1A B4A B9A B10A -2.8(6) . . . . ?
C1A B4A B9A B12A 61.0(5) . . . . ?
C1A B5A B6A C2A 33.7(4) . . . . ?
C1A B5A B6A B10A 136.1(5) . . . . ?
C1A B5A B6A B11A 96.8(5) . . . . ?
C1A B5A B9A B4A 40.0(4) . . . . ?
C1A B5A B9A B8A 2.1(6) . . . . ?
C1A B5A B9A B10A -99.3(5) . . . . ?
C1A B5A B9A B12A -61.2(5) . . . . ?
C1A B5A B10A B6A -38.7(4) . . . . ?
C1A B5A B10A B9A 99.0(5) . . . . ?
C1A B5A B10A B11A -1.2(6) . . . . ?
C1A B5A B10A B12A 61.0(5) . . . . ?
C1A B6A B10A B5A 37.7(4) . . . . ?
C1A B6A B10A B9A -0.3(6) . . . . ?
C1A B6A B10A B11A -100.1(4) . . . . ?
C1A B6A B10A B12A -63.8(5) . . . . ?
C1A B6A B11A C2A -34.4(4) . . . . ?
C1A B6A B11A B7A -0.6(6) . . . . ?
C1A B6A B11A B10A 100.0(5) . . . . ?
C1A B6A B11A B12A 63.1(5) . . . . ?
C1A C1B C2B P1A 6.8(5) . . . . ?
C1A C1B C2B B3B 109.6(4) . . . . ?
C1A C1B C2B B6B -108.5(4) . . . . ?
C1A C1B C2B B7B 147.1(4) . . . . ?
C1A C1B C2B B11B -145.8(4) . . . . ?
C1A C1B B3B C2B -101.3(5) . . . . ?
C1A C1B B3B B4B 118.9(5) . . . . ?
C1A C1B B3B B7B -136.3(5) . . . . ?
C1A C1B B3B B8B 158.8(4) . . . . ?
C1A C1B B4B B3B -104.0(5) . . . . ?
C1A C1B B4B B5B 115.2(5) . . . . ?
C1A C1B B4B B8B -141.9(5) . . . . ?
C1A C1B B4B B9B 155.8(5) . . . . ?
C1A C1B B5B B4B -116.5(5) . . . . ?
C1A C1B B5B B6B 102.6(5) . . . . ?
C1A C1B B5B B9B -156.9(5) . . . . ?
C1A C1B B5B B10B 141.0(5) . . . . ?
C1A C1B B6B C2B 101.6(5) . . . . ?
C1A C1B B6B B5B -118.0(5) . . . . ?
C1A C1B B6B B10B -158.7(4) . . . . ?
C1A C1B B6B B11B 136.5(5) . . . . ?
C2A P1A C11A C12A 169.9(4) . . . . ?
C2A P1A C2B C1B -8.9(3) . . . . ?
C2A P1A C2B B3B -76.1(4) . . . . ?
C2A P1A C2B B6B 61.1(4) . . . . ?
C2A P1A C2B B7B -144.2(4) . . . . ?
C2A P1A C2B B11B 137.3(4) . . . . ?
C2A C1A B3A B4A -140.5(4) . . . . ?
C2A C1A B3A B7A -35.7(4) . . . . ?
C2A C1A B3A B8A -99.4(4) . . . . ?
C2A C1A B4A B3A 36.5(4) . . . . ?
C2A C1A B4A B5A -104.4(4) . . . . ?
C2A C1A B4A B8A -2.7(5) . . . . ?
C2A C1A B4A B9A -64.0(5) . . . . ?
C2A C1A B5A B4A 102.9(4) . . . . ?
C2A C1A B5A B6A -37.4(4) . . . . ?
C2A C1A B5A B9A 62.4(5) . . . . ?
C2A C1A B5A B10A 0.5(5) . . . . ?
C2A C1A B6A B5A 140.1(4) . . . . ?
C2A C1A B6A B10A 100.8(5) . . . . ?
C2A C1A B6A B11A 35.9(4) . . . . ?
C2A C1A C1B C2B -0.4(5) . . . . ?
C2A C1A C1B B3B 67.6(5) . . . . ?
C2A C1A C1B B4B 141.2(5) . . . . ?
C2A C1A C1B B5B -139.5(5) . . . . ?
C2A C1A C1B B6B -67.8(5) . . . . ?
C2A B3A B4A C1A -33.1(4) . . . . ?
C2A B3A B4A B5A 1.4(6) . . . . ?
C2A B3A B4A B8A 100.8(4) . . . . ?
C2A B3A B4A B9A 65.1(5) . . . . ?
C2A B3A B7A B8A -134.5(5) . . . . ?
C2A B3A B7A B11A -35.1(4) . . . . ?
C2A B3A B7A B12A -98.5(5) . . . . ?
C2A B3A B8A B4A -97.9(4) . . . . ?
C2A B3A B8A B7A 39.4(4) . . . . ?
C2A B3A B8A B9A -61.1(5) . . . . ?
C2A B3A B8A B12A 3.2(6) . . . . ?
C2A B6A B10A B5A 97.3(5) . . . . ?
C2A B6A B10A B9A 59.2(6) . . . . ?
C2A B6A B10A B11A -40.6(4) . . . . ?
C2A B6A B10A B12A -4.2(6) . . . . ?
C2A B6A B11A B7A 33.8(4) . . . . ?
C2A B6A B11A B10A 134.4(4) . . . . ?
C2A B6A B11A B12A 97.5(4) . . . . ?
C2A B7A B8A B3A -39.7(4) . . . . ?
C2A B7A B8A B4A -1.5(6) . . . . ?
C2A B7A B8A B9A 62.1(5) . . . . ?
C2A B7A B8A B12A 99.9(5) . . . . ?
C2A B7A B11A B6A -34.2(4) . . . . ?
C2A B7A B11A B10A -95.8(5) . . . . ?
C2A B7A B11A B12A -134.0(4) . . . . ?
C2A B7A B12A B8A -98.3(4) . . . . ?
C2A B7A B12A B9A -61.0(5) . . . . ?
C2A B7A B12A B10A 2.0(6) . . . . ?
C2A B7A B12A B11A 40.6(4) . . . . ?
C2A B11A B12A B7A -39.4(4) . . . . ?
C2A B11A B12A B8A -2.3(6) . . . . ?
C2A B11A B12A B9A 60.9(5) . . . . ?
C2A B11A B12A B10A 98.0(4) . . . . ?
B3A C1A C2A P1A -115.0(4) . . . . ?
B3A C1A C2A B6A 141.7(4) . . . . ?
B3A C1A C2A B7A 38.6(4) . . . . ?
B3A C1A C2A B11A 104.6(4) . . . . ?
B3A C1A B4A B5A -140.9(5) . . . . ?
B3A C1A B4A B8A -39.2(4) . . . . ?
B3A C1A B4A B9A -100.5(5) . . . . ?
B3A C1A B5A B4A 36.7(4) . . . . ?
B3A C1A B5A B6A -103.6(4) . . . . ?
B3A C1A B5A B9A -3.8(6) . . . . ?
B3A C1A B5A B10A -65.8(5) . . . . ?
B3A C1A B6A C2A -35.6(4) . . . . ?
B3A C1A B6A B5A 104.5(4) . . . . ?
B3A C1A B6A B10A 65.2(5) . . . . ?
B3A C1A B6A B11A 0.2(6) . . . . ?
B3A C1A C1B C2B 66.4(5) . . . . ?
B3A C1A C1B B3B 134.4(4) . . . . ?
B3A C1A C1B B4B -151.9(5) . . . . ?
B3A C1A C1B B5B -72.7(6) . . . . ?
B3A C1A C1B B6B -1.0(6) . . . . ?
B3A C2A B6A C1A 37.0(4) . . . . ?
B3A C2A B6A B5A 2.8(6) . . . . ?
B3A C2A B6A B10A -61.1(5) . . . . ?
B3A C2A B6A B11A -102.6(5) . . . . ?
B3A C2A B7A B8A 39.1(4) . . . . ?
B3A C2A B7A B11A 141.5(4) . . . . ?
B3A C2A B7A B12A 101.3(5) . . . . ?
B3A C2A B11A B6A 105.6(5) . . . . ?
B3A C2A B11A B7A -36.0(4) . . . . ?
B3A C2A B11A B10A 66.7(5) . . . . ?
B3A C2A B11A B12A 4.4(6) . . . . ?
B3A B4A B5A C1A -35.6(4) . . . . ?
B3A B4A B5A B6A 0.2(6) . . . . ?
B3A B4A B5A B9A 98.4(5) . . . . ?
B3A B4A B5A B10A 62.1(5) . . . . ?
B3A B4A B8A B7A -38.0(4) . . . . ?
B3A B4A B8A B9A -139.2(5) . . . . ?
B3A B4A B8A B12A -101.3(5) . . . . ?
B3A B4A B9A B5A -102.7(5) . . . . ?
B3A B4A B9A B8A 35.3(4) . . . . ?
B3A B4A B9A B10A -66.2(6) . . . . ?
B3A B4A B9A B12A -2.4(6) . . . . ?
B3A B7A B8A B4A 38.2(4) . . . . ?
B3A B7A B8A B9A 101.8(5) . . . . ?
B3A B7A B8A B12A 139.6(5) . . . . ?
B3A B7A B11A C2A 34.9(4) . . . . ?
B3A B7A B11A B6A 0.7(6) . . . . ?
B3A B7A B11A B10A -60.9(6) . . . . ?
B3A B7A B11A B12A -99.0(5) . . . . ?
B3A B7A B12A B8A -35.5(4) . . . . ?
B3A B7A B12A B9A 1.9(6) . . . . ?
B3A B7A B12A B10A 64.8(5) . . . . ?
B3A B7A B12A B11A 103.4(5) . . . . ?
B3A B8A B9A B4A -36.9(4) . . . . ?
B3A B8A B9A B5A 0.2(6) . . . . ?
B3A B8A B9A B10A 63.9(6) . . . . ?
B3A B8A B9A B12A 101.1(5) . . . . ?
B3A B8A B12A B7A 36.3(4) . . . . ?
B3A B8A B12A B9A -101.7(5) . . . . ?
B3A B8A B12A B10A -65.1(6) . . . . ?
B3A B8A B12A B11A -0.5(6) . . . . ?
B4A C1A C2A P1A -151.7(3) . . . . ?
B4A C1A C2A B3A -36.7(4) . . . . ?
B4A C1A C2A B6A 105.0(4) . . . . ?
B4A C1A C2A B7A 1.9(5) . . . . ?
B4A C1A C2A B11A 67.9(5) . . . . ?
B4A C1A B3A C2A 140.5(4) . . . . ?
B4A C1A B3A B7A 104.8(5) . . . . ?
B4A C1A B3A B8A 41.0(4) . . . . ?
B4A C1A B5A B6A -140.3(5) . . . . ?
B4A C1A B5A B9A -40.5(4) . . . . ?
B4A C1A B5A B10A -102.5(5) . . . . ?
B4A C1A B6A C2A -102.4(4) . . . . ?
B4A C1A B6A B5A 37.7(4) . . . . ?
B4A C1A B6A B10A -1.6(6) . . . . ?
B4A C1A B6A B11A -66.5(5) . . . . ?
B4A C1A C1B C2B 138.6(4) . . . . ?
B4A C1A C1B B3B -153.5(5) . . . . ?
B4A C1A C1B B4B -79.8(6) . . . . ?
B4A C1A C1B B5B -0.5(7) . . . . ?
B4A C1A C1B B6B 71.1(6) . . . . ?
B4A B3A B7A C2A 95.1(4) . . . . ?
B4A B3A B7A B8A -39.3(4) . . . . ?
B4A B3A B7A B11A 60.0(6) . . . . ?
B4A B3A B7A B12A -3.4(6) . . . . ?
B4A B3A B8A B7A 137.3(5) . . . . ?
B4A B3A B8A B9A 36.8(4) . . . . ?
B4A B3A B8A B12A 101.1(5) . . . . ?
B4A B5A B6A C1A -35.4(4) . . . . ?
B4A B5A B6A C2A -1.8(6) . . . . ?
B4A B5A B6A B10A 100.6(5) . . . . ?
B4A B5A B6A B11A 61.4(6) . . . . ?
B4A B5A B9A B8A -37.8(4) . . . . ?
B4A B5A B9A B10A -139.3(5) . . . . ?
B4A B5A B9A B12A -101.2(5) . . . . ?
B4A B5A B10A B6A -101.0(5) . . . . ?
B4A B5A B10A B9A 36.7(4) . . . . ?
B4A B5A B10A B11A -63.6(5) . . . . ?
B4A B5A B10A B12A -1.3(6) . . . . ?
B4A B8A B9A B5A 37.1(4) . . . . ?
B4A B8A B9A B10A 100.8(5) . . . . ?
B4A B8A B9A B12A 138.0(5) . . . . ?
B4A B8A B12A B7A 100.3(5) . . . . ?
B4A B8A B12A B9A -37.7(4) . . . . ?
B4A B8A B12A B10A -1.1(6) . . . . ?
B4A B8A B12A B11A 63.4(6) . . . . ?
B4A B9A B10A B5A -36.1(4) . . . . ?
B4A B9A B10A B6A 2.0(6) . . . . ?
B4A B9A B10A B11A 64.9(6) . . . . ?
B4A B9A B10A B12A 101.4(5) . . . . ?
B4A B9A B12A B7A 0.3(6) . . . . ?
B4A B9A B12A B8A 38.0(4) . . . . ?
B4A B9A B12A B10A -100.7(5) . . . . ?
B4A B9A B12A B11A -63.0(6) . . . . ?
B5A C1A C2A P1A 140.9(4) . . . . ?
B5A C1A C2A B3A -104.1(4) . . . . ?
B5A C1A C2A B6A 37.6(4) . . . . ?
B5A C1A C2A B7A -65.6(5) . . . . ?
B5A C1A C2A B11A 0.5(5) . . . . ?
B5A C1A B3A C2A 103.4(4) . . . . ?
B5A C1A B3A B4A -37.1(4) . . . . ?
B5A C1A B3A B7A 67.7(5) . . . . ?
B5A C1A B3A B8A 4.0(5) . . . . ?
B5A C1A B4A B3A 140.9(5) . . . . ?
B5A C1A B4A B8A 101.7(5) . . . . ?
B5A C1A B4A B9A 40.4(4) . . . . ?
B5A C1A B6A C2A -140.1(4) . . . . ?
B5A C1A B6A B10A -39.3(4) . . . . ?
B5A C1A B6A B11A -104.2(5) . . . . ?
B5A C1A C1B C2B -141.6(5) . . . . ?
B5A C1A C1B B3B -73.6(6) . . . . ?
B5A C1A C1B B4B 0.0(8) . . . . ?
B5A C1A C1B B5B 79.3(6) . . . . ?
B5A C1A C1B B6B 151.0(5) . . . . ?
B5A B4A B8A B3A 101.6(5) . . . . ?
B5A B4A B8A B7A 63.6(5) . . . . ?
B5A B4A B8A B9A -37.6(4) . . . . ?
B5A B4A B8A B12A 0.2(6) . . . . ?
B5A B4A B9A B8A 138.0(5) . . . . ?
B5A B4A B9A B10A 36.5(4) . . . . ?
B5A B4A B9A B12A 100.4(5) . . . . ?
B5A B6A B10A B9A -38.0(4) . . . . ?
B5A B6A B10A B11A -137.8(5) . . . . ?
B5A B6A B10A B12A -101.5(5) . . . . ?
B5A B6A B11A C2A -95.5(5) . . . . ?
B5A B6A B11A B7A -61.7(6) . . . . ?
B5A B6A B11A B10A 38.9(4) . . . . ?
B5A B6A B11A B12A 2.0(6) . . . . ?
B5A B9A B10A B6A 38.1(4) . . . . ?
B5A B9A B10A B11A 101.0(5) . . . . ?
B5A B9A B10A B12A 137.5(5) . . . . ?
B5A B9A B12A B7A 62.9(6) . . . . ?
B5A B9A B12A B8A 100.6(5) . . . . ?
B5A B9A B12A B10A -38.0(4) . . . . ?
B5A B9A B12A B11A -0.3(6) . . . . ?
B5A B10A B11A C2A 1.5(6) . . . . ?
B5A B10A B11A B6A -37.8(4) . . . . ?
B5A B10A B11A B7A 62.4(6) . . . . ?
B5A B10A B11A B12A 100.7(5) . . . . ?
B5A B10A B12A B7A -62.3(5) . . . . ?
B5A B10A B12A B8A 1.5(6) . . . . ?
B5A B10A B12A B9A 38.2(4) . . . . ?
B5A B10A B12A B11A -100.3(5) . . . . ?
B6A C1A C2A P1A 103.3(4) . . . . ?
B6A C1A C2A B3A -141.7(4) . . . . ?
B6A C1A C2A B7A -103.2(5) . . . . ?
B6A C1A C2A B11A -37.1(4) . . . . ?
B6A C1A B3A C2A 35.9(4) . . . . ?
B6A C1A B3A B4A -104.6(5) . . . . ?
B6A C1A B3A B7A 0.2(5) . . . . ?
B6A C1A B3A B8A -63.5(5) . . . . ?
B6A C1A B4A B3A 103.3(4) . . . . ?
B6A C1A B4A B5A -37.6(4) . . . . ?
B6A C1A B4A B8A 64.0(5) . . . . ?
B6A C1A B4A B9A 2.7(6) . . . . ?
B6A C1A B5A B4A 140.3(5) . . . . ?
B6A C1A B5A B9A 99.8(5) . . . . ?
B6A C1A B5A B10A 37.9(4) . . . . ?
B6A C1A C1B C2B -68.1(5) . . . . ?
B6A C1A C1B B3B -0.1(6) . . . . ?
B6A C1A C1B B4B 73.6(6) . . . . ?
B6A C1A C1B B5B 152.9(5) . . . . ?
B6A C1A C1B B6B -135.5(4) . . . . ?
B6A C2A B3A C1A -36.5(4) . . . . ?
B6A C2A B3A B4A -2.7(6) . . . . ?
B6A C2A B3A B7A 102.1(5) . . . . ?
B6A C2A B3A B8A 61.4(5) . . . . ?
B6A C2A B7A B3A -106.0(4) . . . . ?
B6A C2A B7A B8A -67.0(5) . . . . ?
B6A C2A B7A B11A 35.5(4) . . . . ?
B6A C2A B7A B12A -4.8(5) . . . . ?
B6A C2A B11A B7A -141.5(5) . . . . ?
B6A C2A B11A B10A -38.8(4) . . . . ?
B6A C2A B11A B12A -101.1(5) . . . . ?
B6A B5A B9A B4A 102.7(5) . . . . ?
B6A B5A B9A B8A 64.9(5) . . . . ?
B6A B5A B9A B10A -36.6(4) . . . . ?
B6A B5A B9A B12A 1.5(6) . . . . ?
B6A B5A B10A B9A 137.7(5) . . . . ?
B6A B5A B10A B11A 37.4(4) . . . . ?
B6A B5A B10A B12A 99.7(5) . . . . ?
B6A B10A B11A C2A 39.3(4) . . . . ?
B6A B10A B11A B7A 100.3(5) . . . . ?
B6A B10A B11A B12A 138.6(5) . . . . ?
B6A B10A B12A B7A 1.4(6) . . . . ?
B6A B10A B12A B8A 65.2(5) . . . . ?
B6A B10A B12A B9A 101.9(5) . . . . ?
B6A B10A B12A B11A -36.6(4) . . . . ?
B6A B11A B12A B7A -101.3(5) . . . . ?
B6A B11A B12A B8A -64.2(5) . . . . ?
B6A B11A B12A B9A -1.0(6) . . . . ?
B6A B11A B12A B10A 36.1(4) . . . . ?
B7A C2A B3A C1A -138.6(4) . . . . ?
B7A C2A B3A B4A -104.8(5) . . . . ?
B7A C2A B3A B8A -40.7(4) . . . . ?
B7A C2A B6A C1A 103.8(4) . . . . ?
B7A C2A B6A B5A 69.7(5) . . . . ?
B7A C2A B6A B10A 5.8(6) . . . . ?
B7A C2A B6A B11A -35.8(4) . . . . ?
B7A C2A B11A B6A 141.5(5) . . . . ?
B7A C2A B11A B10A 102.7(5) . . . . ?
B7A C2A B11A B12A 40.4(4) . . . . ?
B7A B3A B4A C1A -94.7(4) . . . . ?
B7A B3A B4A B5A -60.1(6) . . . . ?
B7A B3A B4A B8A 39.3(4) . . . . ?
B7A B3A B4A B9A 3.6(6) . . . . ?
B7A B3A B8A B4A -137.3(5) . . . . ?
B7A B3A B8A B9A -100.5(5) . . . . ?
B7A B3A B8A B12A -36.2(4) . . . . ?
B7A B8A B9A B4A -100.5(5) . . . . ?
B7A B8A B9A B5A -63.4(6) . . . . ?
B7A B8A B9A B10A 0.3(6) . . . . ?
B7A B8A B9A B12A 37.5(4) . . . . ?
B7A B8A B12A B9A -138.0(5) . . . . ?
B7A B8A B12A B10A -101.3(5) . . . . ?
B7A B8A B12A B11A -36.8(4) . . . . ?
B7A B11A B12A B8A 37.1(4) . . . . ?
B7A B11A B12A B9A 100.3(5) . . . . ?
B7A B11A B12A B10A 137.4(5) . . . . ?
B8A B3A B4A C1A -133.9(4) . . . . ?
B8A B3A B4A B5A -99.4(5) . . . . ?
B8A B3A B4A B9A -35.7(4) . . . . ?
B8A B3A B7A C2A 134.5(5) . . . . ?
B8A B3A B7A B11A 99.3(5) . . . . ?
B8A B3A B7A B12A 35.9(4) . . . . ?
B8A B4A B5A C1A -97.0(4) . . . . ?
B8A B4A B5A B6A -61.2(5) . . . . ?
B8A B4A B5A B9A 37.0(4) . . . . ?
B8A B4A B5A B10A 0.7(6) . . . . ?
B8A B4A B9A B5A -138.0(5) . . . . ?
B8A B4A B9A B10A -101.5(5) . . . . ?
B8A B4A B9A B12A -37.6(4) . . . . ?
B8A B7A B11A C2A 97.3(4) . . . . ?
B8A B7A B11A B6A 63.1(6) . . . . ?
B8A B7A B11A B10A 1.4(6) . . . . ?
B8A B7A B11A B12A -36.7(4) . . . . ?
B8A B7A B12A B9A 37.3(4) . . . . ?
B8A B7A B12A B10A 100.3(5) . . . . ?
B8A B7A B12A B11A 138.9(5) . . . . ?
B8A B9A B10A B5A -100.4(5) . . . . ?
B8A B9A B10A B6A -62.3(6) . . . . ?
B8A B9A B10A B11A 0.6(6) . . . . ?
B8A B9A B10A B12A 37.1(4) . . . . ?
B8A B9A B12A B7A -37.7(4) . . . . ?
B8A B9A B12A B10A -138.7(5) . . . . ?
B8A B9A B12A B11A -101.0(5) . . . . ?
B9A B4A B5A C1A -134.0(5) . . . . ?
B9A B4A B5A B6A -98.2(5) . . . . ?
B9A B4A B5A B10A -36.3(4) . . . . ?
B9A B4A B8A B3A 139.2(5) . . . . ?
B9A B4A B8A B7A 101.2(5) . . . . ?
B9A B4A B8A B12A 37.9(4) . . . . ?
B9A B5A B6A C1A -99.0(5) . . . . ?
B9A B5A B6A C2A -65.3(5) . . . . ?
B9A B5A B6A B10A 37.1(4) . . . . ?
B9A B5A B6A B11A -2.2(6) . . . . ?
B9A B5A B10A B6A -137.7(5) . . . . ?
B9A B5A B10A B11A -100.3(5) . . . . ?
B9A B5A B10A B12A -38.1(4) . . . . ?
B9A B8A B12A B7A 138.0(5) . . . . ?
B9A B8A B12A B10A 36.7(4) . . . . ?
B9A B8A B12A B11A 101.2(5) . . . . ?
B9A B10A B11A C2A -62.2(5) . . . . ?
B9A B10A B11A B6A -101.5(5) . . . . ?
B9A B10A B11A B7A -1.3(6) . . . . ?
B9A B10A B11A B12A 37.0(4) . . . . ?
B9A B10A B12A B7A -100.5(5) . . . . ?
B9A B10A B12A B8A -36.7(4) . . . . ?
B9A B10A B12A B11A -138.5(5) . . . . ?
B10A B5A B6A C1A -136.1(5) . . . . ?
B10A B5A B6A C2A -102.4(5) . . . . ?
B10A B5A B6A B11A -39.3(4) . . . . ?
B10A B5A B9A B4A 139.3(5) . . . . ?
B10A B5A B9A B8A 101.5(5) . . . . ?
B10A B5A B9A B12A 38.1(4) . . . . ?
B10A B6A B11A C2A -134.4(4) . . . . ?
B10A B6A B11A B7A -100.5(5) . . . . ?
B10A B6A B11A B12A -36.9(4) . . . . ?
B10A B9A B12A B7A 101.0(5) . . . . ?
B10A B9A B12A B8A 138.7(5) . . . . ?
B10A B9A B12A B11A 37.7(4) . . . . ?
B10A B11A B12A B7A -137.4(5) . . . . ?
B10A B11A B12A B8A -100.3(5) . . . . ?
B10A B11A B12A B9A -37.1(4) . . . . ?
B11A C2A B3A C1A -102.7(4) . . . . ?
B11A C2A B3A B4A -68.9(5) . . . . ?
B11A C2A B3A B7A 35.9(4) . . . . ?
B11A C2A B3A B8A -4.8(6) . . . . ?
B11A C2A B6A C1A 139.6(4) . . . . ?
B11A C2A B6A B5A 105.4(5) . . . . ?
B11A C2A B6A B10A 41.5(4) . . . . ?
B11A C2A B7A B3A -141.5(4) . . . . ?
B11A C2A B7A B8A -102.5(5) . . . . ?
B11A C2A B7A B12A -40.3(4) . . . . ?
B11A B6A B10A B5A 137.8(5) . . . . ?
B11A B6A B10A B9A 99.8(5) . . . . ?
B11A B6A B10A B12A 36.3(4) . . . . ?
B11A B7A B8A B3A -102.9(5) . . . . ?
B11A B7A B8A B4A -64.7(5) . . . . ?
B11A B7A B8A B9A -1.1(6) . . . . ?
B11A B7A B8A B12A 36.7(4) . . . . ?
B11A B7A B12A B8A -138.9(5) . . . . ?
B11A B7A B12A B9A -101.5(5) . . . . ?
B11A B7A B12A B10A -38.6(4) . . . . ?
B11A B10A B12A B7A 38.0(4) . . . . ?
B11A B10A B12A B8A 101.8(5) . . . . ?
B11A B10A B12A B9A 138.5(5) . . . . ?
C11A P1A C2A C1A 113.3(4) . . . . ?
C11A P1A C2A B3A 42.6(4) . . . . ?
C11A P1A C2A B6A -179.6(4) . . . . ?
C11A P1A C2A B7A -34.2(5) . . . . ?
C11A P1A C2A B11A -111.7(4) . . . . ?
C11A P1A C2B C1B -111.7(3) . . . . ?
C11A P1A C2B B3B -178.8(3) . . . . ?
C11A P1A C2B B6B -41.7(4) . . . . ?
C11A P1A C2B B7B 113.1(4) . . . . ?
C11A P1A C2B B11B 34.6(5) . . . . ?
B12A B7A B8A B3A -139.6(5) . . . . ?
B12A B7A B8A B4A -101.4(5) . . . . ?
B12A B7A B8A B9A -37.8(4) . . . . ?
B12A B7A B11A C2A 134.0(4) . . . . ?
B12A B7A B11A B6A 99.7(5) . . . . ?
B12A B7A B11A B10A 38.1(4) . . . . ?
B12A B8A B9A B4A -138.0(5) . . . . ?
B12A B8A B9A B5A -100.9(5) . . . . ?
B12A B8A B9A B10A -37.2(4) . . . . ?
B12A B9A B10A B5A -137.5(5) . . . . ?
B12A B9A B10A B6A -99.4(5) . . . . ?
B12A B9A B10A B11A -36.5(4) . . . . ?
B12A B10A B11A C2A -99.2(4) . . . . ?
B12A B10A B11A B6A -138.6(5) . . . . ?
B12A B10A B11A B7A -38.3(4) . . . . ?
C1B C1A C2A P1A -6.3(5) . . . . ?
C1B C1A C2A B3A 108.7(4) . . . . ?
C1B C1A C2A B6A -109.6(4) . . . . ?
C1B C1A C2A B7A 147.3(4) . . . . ?
C1B C1A C2A B11A -146.7(4) . . . . ?
C1B C1A B3A C2A -100.7(4) . . . . ?
C1B C1A B3A B4A 118.8(5) . . . . ?
C1B C1A B3A B7A -136.4(4) . . . . ?
C1B C1A B3A B8A 159.9(4) . . . . ?
C1B C1A B4A B3A -102.4(5) . . . . ?
C1B C1A B4A B5A 116.7(5) . . . . ?
C1B C1A B4A B8A -141.7(5) . . . . ?
C1B C1A B4A B9A 157.0(5) . . . . ?
C1B C1A B5A B4A -116.1(5) . . . . ?
C1B C1A B5A B6A 103.6(5) . . . . ?
C1B C1A B5A B9A -156.6(5) . . . . ?
C1B C1A B5A B10A 141.4(5) . . . . ?
C1B C1A B6A C2A 100.7(4) . . . . ?
C1B C1A B6A B5A -119.3(5) . . . . ?
C1B C1A B6A B10A -158.5(4) . . . . ?
C1B C1A B6A B11A 136.5(4) . . . . ?
C1B C2B B3B B4B 34.2(4) . . . . ?
C1B C2B B3B B7B 139.6(4) . . . . ?
C1B C2B B3B B8B 98.1(5) . . . . ?
C1B C2B B6B B5B -33.9(4) . . . . ?
C1B C2B B6B B10B -98.3(4) . . . . ?
C1B C2B B6B B11B -139.7(5) . . . . ?
C1B C2B B7B B3B -38.0(4) . . . . ?
C1B C2B B7B B8B 0.8(6) . . . . ?
C1B C2B B7B B11B 103.7(5) . . . . ?
C1B C2B B7B B12B 62.7(5) . . . . ?
C1B C2B B11B B6B 38.2(4) . . . . ?
C1B C2B B11B B7B -103.5(4) . . . . ?
C1B C2B B11B B10B -0.7(5) . . . . ?
C1B C2B B11B B12B -62.8(5) . . . . ?
C1B B3B B4B B5B 34.9(4) . . . . ?
C1B B3B B4B B8B 135.3(5) . . . . ?
C1B B3B B4B B9B 98.2(5) . . . . ?
C1B B3B B7B C2B 33.9(4) . . . . ?
C1B B3B B7B B8B -100.3(5) . . . . ?
C1B B3B B7B B11B -0.2(6) . . . . ?
C1B B3B B7B B12B -63.7(5) . . . . ?
C1B B3B B8B B4B -38.2(4) . . . . ?
C1B B3B B8B B7B 98.8(5) . . . . ?
C1B B3B B8B B9B -0.9(6) . . . . ?
C1B B3B B8B B12B 62.4(6) . . . . ?
C1B B4B B5B B6B 35.6(4) . . . . ?
C1B B4B B5B B9B 133.6(5) . . . . ?
C1B B4B B5B B10B 96.7(5) . . . . ?
C1B B4B B8B B3B 39.1(4) . . . . ?
C1B B4B B8B B7B 0.7(6) . . . . ?
C1B B4B B8B B9B -99.0(5) . . . . ?
C1B B4B B8B B12B -61.4(5) . . . . ?
C1B B4B B9B B5B -40.0(4) . . . . ?
C1B B4B B9B B8B 98.6(5) . . . . ?
C1B B4B B9B B10B -2.7(6) . . . . ?
C1B B4B B9B B12B 60.9(5) . . . . ?
C1B B5B B6B C2B 33.1(4) . . . . ?
C1B B5B B6B B10B 134.6(4) . . . . ?
C1B B5B B6B B11B 94.9(4) . . . . ?
C1B B5B B9B B4B 39.7(4) . . . . ?
C1B B5B B9B B8B 2.4(6) . . . . ?
C1B B5B B9B B10B -98.9(4) . . . . ?
C1B B5B B9B B12B -61.0(5) . . . . ?
C1B B5B B10B B6B -40.0(4) . . . . ?
C1B B5B B10B B9B 98.4(5) . . . . ?
C1B B5B B10B B11B -2.2(6) . . . . ?
C1B B5B B10B B12B 60.6(5) . . . . ?
C1B B6B B10B B5B 39.0(4) . . . . ?
C1B B6B B10B B9B 1.8(6) . . . . ?
C1B B6B B10B B11B -98.6(4) . . . . ?
C1B B6B B10B B12B -61.6(5) . . . . ?
C1B B6B B11B C2B -33.7(4) . . . . ?
C1B B6B B11B B7B 0.7(6) . . . . ?
C1B B6B B11B B10B 100.6(5) . . . . ?
C1B B6B B11B B12B 63.6(5) . . . . ?
C2B P1A C2A C1A 8.8(4) . . . . ?
C2B P1A C2A B3A -61.9(4) . . . . ?
C2B P1A C2A B6A 75.9(4) . . . . ?
C2B P1A C2A B7A -138.8(4) . . . . ?
C2B P1A C2A B11A 143.7(4) . . . . ?
C2B P1A C11A C12A -93.8(4) . . . . ?
C2B C1B B3B B4B -139.8(4) . . . . ?
C2B C1B B3B B7B -35.1(4) . . . . ?
C2B C1B B3B B8B -99.9(5) . . . . ?
C2B C1B B4B B3B 37.6(4) . . . . ?
C2B C1B B4B B5B -103.2(4) . . . . ?
C2B C1B B4B B8B -0.3(6) . . . . ?
C2B C1B B4B B9B -62.6(5) . . . . ?
C2B C1B B5B B4B 104.2(4) . . . . ?
C2B C1B B5B B6B -36.7(4) . . . . ?
C2B C1B B5B B9B 63.8(5) . . . . ?
C2B C1B B5B B10B 1.8(5) . . . . ?
C2B C1B B6B B5B 140.5(4) . . . . ?
C2B C1B B6B B10B 99.7(4) . . . . ?
C2B C1B B6B B11B 35.0(4) . . . . ?
C2B B3B B4B C1B -33.6(4) . . . . ?
C2B B3B B4B B5B 1.4(6) . . . . ?
C2B B3B B4B B8B 101.7(5) . . . . ?
C2B B3B B4B B9B 64.7(5) . . . . ?
C2B B3B B7B B8B -134.2(5) . . . . ?
C2B B3B B7B B11B -34.0(4) . . . . ?
C2B B3B B7B B12B -97.5(5) . . . . ?
C2B B3B B8B B4B -97.1(5) . . . . ?
C2B B3B B8B B7B 39.9(4) . . . . ?
C2B B3B B8B B9B -59.7(6) . . . . ?
C2B B3B B8B B12B 3.5(6) . . . . ?
C2B B6B B10B B5B 97.7(4) . . . . ?
C2B B6B B10B B9B 60.5(5) . . . . ?
C2B B6B B10B B11B -39.8(4) . . . . ?
C2B B6B B10B B12B -2.9(6) . . . . ?
C2B B6B B11B B7B 34.4(4) . . . . ?
C2B B6B B11B B10B 134.3(5) . . . . ?
C2B B6B B11B B12B 97.4(5) . . . . ?
C2B B7B B8B B3B -39.8(4) . . . . ?
C2B B7B B8B B4B -0.9(6) . . . . ?
C2B B7B B8B B9B 61.9(5) . . . . ?
C2B B7B B8B B12B 98.7(5) . . . . ?
C2B B7B B11B B6B -34.8(4) . . . . ?
C2B B7B B11B B10B -96.5(5) . . . . ?
C2B B7B B11B B12B -133.0(5) . . . . ?
C2B B7B B12B B8B -98.1(5) . . . . ?
C2B B7B B12B B9B -60.6(6) . . . . ?
C2B B7B B12B B10B 3.3(6) . . . . ?
C2B B7B B12B B11B 40.3(4) . . . . ?
C2B B11B B12B B7B -40.5(4) . . . . ?
C2B B11B B12B B8B -2.5(6) . . . . ?
C2B B11B B12B B9B 61.6(5) . . . . ?
C2B B11B B12B B10B 98.8(4) . . . . ?
B3B C1B C2B P1A -102.8(4) . . . . ?
B3B C1B C2B B6B 141.9(4) . . . . ?
B3B C1B C2B B7B 37.5(4) . . . . ?
B3B C1B C2B B11B 104.5(5) . . . . ?
B3B C1B B4B B5B -140.8(5) . . . . ?
B3B C1B B4B B8B -37.9(4) . . . . ?
B3B C1B B4B B9B -100.2(5) . . . . ?
B3B C1B B5B B4B 37.3(4) . . . . ?
B3B C1B B5B B6B -103.6(4) . . . . ?
B3B C1B B5B B9B -3.1(6) . . . . ?
B3B C1B B5B B10B -65.1(5) . . . . ?
B3B C1B B6B C2B -35.8(4) . . . . ?
B3B C1B B6B B5B 104.7(5) . . . . ?
B3B C1B B6B B10B 63.9(5) . . . . ?
B3B C1B B6B B11B -0.8(6) . . . . ?
B3B C2B B6B C1B 36.6(4) . . . . ?
B3B C2B B6B B5B 2.7(6) . . . . ?
B3B C2B B6B B10B -61.7(5) . . . . ?
B3B C2B B6B B11B -103.1(5) . . . . ?
B3B C2B B7B B8B 38.7(4) . . . . ?
B3B C2B B7B B11B 141.7(5) . . . . ?
B3B C2B B7B B12B 100.7(5) . . . . ?
B3B C2B B11B B6B 105.8(5) . . . . ?
B3B C2B B11B B7B -35.8(4) . . . . ?
B3B C2B B11B B10B 67.0(5) . . . . ?
B3B C2B B11B B12B 4.8(6) . . . . ?
B3B B4B B5B C1B -35.4(4) . . . . ?
B3B B4B B5B B6B 0.2(6) . . . . ?
B3B B4B B5B B9B 98.2(5) . . . . ?
B3B B4B B5B B10B 61.3(6) . . . . ?
B3B B4B B8B B7B -38.4(4) . . . . ?
B3B B4B B8B B9B -138.1(5) . . . . ?
B3B B4B B8B B12B -100.5(5) . . . . ?
B3B B4B B9B B5B -102.6(5) . . . . ?
B3B B4B B9B B8B 36.0(4) . . . . ?
B3B B4B B9B B10B -65.3(5) . . . . ?
B3B B4B B9B B12B -1.8(6) . . . . ?
B3B B7B B8B B4B 38.9(4) . . . . ?
B3B B7B B8B B9B 101.7(5) . . . . ?
B3B B7B B8B B12B 138.5(5) . . . . ?
B3B B7B B11B C2B 34.5(4) . . . . ?
B3B B7B B11B B6B -0.3(7) . . . . ?
B3B B7B B11B B10B -62.0(6) . . . . ?
B3B B7B B11B B12B -98.5(5) . . . . ?
B3B B7B B12B B8B -35.7(4) . . . . ?
B3B B7B B12B B9B 1.8(6) . . . . ?
B3B B7B B12B B10B 65.7(6) . . . . ?
B3B B7B B12B B11B 102.6(5) . . . . ?
B3B B8B B9B B4B -38.0(5) . . . . ?
B3B B8B B9B B5B -1.0(6) . . . . ?
B3B B8B B9B B10B 63.1(6) . . . . ?
B3B B8B B9B B12B 99.7(5) . . . . ?
B3B B8B B12B B7B 36.9(4) . . . . ?
B3B B8B B12B B9B -101.6(5) . . . . ?
B3B B8B B12B B10B -65.1(6) . . . . ?
B3B B8B B12B B11B -0.7(6) . . . . ?
B4B C1B C2B P1A -140.6(4) . . . . ?
B4B C1B C2B B3B -37.8(4) . . . . ?
B4B C1B C2B B6B 104.1(5) . . . . ?
B4B C1B C2B B7B -0.3(6) . . . . ?
B4B C1B C2B B11B 66.7(5) . . . . ?
B4B C1B B3B C2B 139.8(4) . . . . ?
B4B C1B B3B B7B 104.8(5) . . . . ?
B4B C1B B3B B8B 39.9(4) . . . . ?
B4B C1B B5B B6B -140.9(4) . . . . ?
B4B C1B B5B B9B -40.4(4) . . . . ?
B4B C1B B5B B10B -102.4(5) . . . . ?
B4B C1B B6B C2B -103.4(4) . . . . ?
B4B C1B B6B B5B 37.1(4) . . . . ?
B4B C1B B6B B10B -3.7(6) . . . . ?
B4B C1B B6B B11B -68.4(5) . . . . ?
B4B B3B B7B C2B 94.6(4) . . . . ?
B4B B3B B7B B8B -39.6(4) . . . . ?
B4B B3B B7B B11B 60.5(6) . . . . ?
B4B B3B B7B B12B -3.0(6) . . . . ?
B4B B3B B8B B7B 137.0(5) . . . . ?
B4B B3B B8B B9B 37.4(5) . . . . ?
B4B B3B B8B B12B 100.6(5) . . . . ?
B4B B5B B6B C1B -34.7(4) . . . . ?
B4B B5B B6B C2B -1.7(6) . . . . ?
B4B B5B B6B B10B 99.9(5) . . . . ?
B4B B5B B6B B11B 60.2(6) . . . . ?
B4B B5B B9B B8B -37.3(4) . . . . ?
B4B B5B B9B B10B -138.6(5) . . . . ?
B4B B5B B9B B12B -100.7(5) . . . . ?
B4B B5B B10B B6B -101.4(5) . . . . ?
B4B B5B B10B B9B 37.0(4) . . . . ?
B4B B5B B10B B11B -63.6(6) . . . . ?
B4B B5B B10B B12B -0.8(6) . . . . ?
B4B B8B B9B B5B 37.0(4) . . . . ?
B4B B8B B9B B10B 101.1(5) . . . . ?
B4B B8B B9B B12B 137.7(5) . . . . ?
B4B B8B B12B B7B 101.1(5) . . . . ?
B4B B8B B12B B9B -37.4(4) . . . . ?
B4B B8B B12B B10B -0.9(6) . . . . ?
B4B B8B B12B B11B 63.5(6) . . . . ?
B4B B9B B10B B5B -37.0(4) . . . . ?
B4B B9B B10B B6B 0.5(6) . . . . ?
B4B B9B B10B B11B 63.8(6) . . . . ?
B4B B9B B10B B12B 100.5(5) . . . . ?
B4B B9B B12B B7B 0.0(6) . . . . ?
B4B B9B B12B B8B 38.0(4) . . . . ?
B4B B9B B12B B10B -101.3(5) . . . . ?
B4B B9B B12B B11B -63.9(6) . . . . ?
B5B C1B C2B P1A 151.9(3) . . . . ?
B5B C1B C2B B3B -105.3(4) . . . . ?
B5B C1B C2B B6B 36.7(4) . . . . ?
B5B C1B C2B B7B -67.7(5) . . . . ?
B5B C1B C2B B11B -0.7(5) . . . . ?
B5B C1B B3B C2B 102.4(4) . . . . ?
B5B C1B B3B B4B -37.4(4) . . . . ?
B5B C1B B3B B7B 67.4(5) . . . . ?
B5B C1B B3B B8B 2.5(6) . . . . ?
B5B C1B B4B B3B 140.8(5) . . . . ?
B5B C1B B4B B8B 102.9(5) . . . . ?
B5B C1B B4B B9B 40.5(4) . . . . ?
B5B C1B B6B C2B -140.5(4) . . . . ?
B5B C1B B6B B10B -40.7(4) . . . . ?
B5B C1B B6B B11B -105.5(5) . . . . ?
B5B B4B B8B B3B 100.9(5) . . . . ?
B5B B4B B8B B7B 62.5(6) . . . . ?
B5B B4B B8B B9B -37.2(4) . . . . ?
B5B B4B B8B B12B 0.4(6) . . . . ?
B5B B4B B9B B8B 138.6(5) . . . . ?
B5B B4B B9B B10B 37.3(4) . . . . ?
B5B B4B B9B B12B 100.8(5) . . . . ?
B5B B6B B10B B9B -37.2(4) . . . . ?
B5B B6B B10B B11B -137.5(5) . . . . ?
B5B B6B B10B B12B -100.6(5) . . . . ?
B5B B6B B11B C2B -94.8(4) . . . . ?
B5B B6B B11B B7B -60.4(6) . . . . ?
B5B B6B B11B B10B 39.5(4) . . . . ?
B5B B6B B11B B12B 2.6(6) . . . . ?
B5B B9B B10B B6B 37.5(4) . . . . ?
B5B B9B B10B B11B 100.8(5) . . . . ?
B5B B9B B10B B12B 137.5(5) . . . . ?
B5B B9B B12B B7B 63.2(6) . . . . ?
B5B B9B B12B B8B 101.2(5) . . . . ?
B5B B9B B12B B10B -38.1(4) . . . . ?
B5B B9B B12B B11B -0.7(6) . . . . ?
B5B B10B B11B C2B 1.8(6) . . . . ?
B5B B10B B11B B6B -38.2(4) . . . . ?
B5B B10B B11B B7B 63.8(6) . . . . ?
B5B B10B B11B B12B 100.1(5) . . . . ?
B5B B10B B12B B7B -64.1(6) . . . . ?
B5B B10B B12B B8B 1.0(6) . . . . ?
B5B B10B B12B B9B 37.7(4) . . . . ?
B5B B10B B12B B11B -100.9(5) . . . . ?
B6B C1B C2B P1A 115.3(4) . . . . ?
B6B C1B C2B B3B -141.9(4) . . . . ?
B6B C1B C2B B7B -104.4(5) . . . . ?
B6B C1B C2B B11B -37.4(4) . . . . ?
B6B C1B B3B C2B 35.7(4) . . . . ?
B6B C1B B3B B4B -104.1(5) . . . . ?
B6B C1B B3B B7B 0.6(6) . . . . ?
B6B C1B B3B B8B -64.2(5) . . . . ?
B6B C1B B4B B3B 104.2(5) . . . . ?
B6B C1B B4B B5B -36.6(4) . . . . ?
B6B C1B B4B B8B 66.3(5) . . . . ?
B6B C1B B4B B9B 3.9(6) . . . . ?
B6B C1B B5B B4B 140.9(4) . . . . ?
B6B C1B B5B B9B 100.5(5) . . . . ?
B6B C1B B5B B10B 38.5(4) . . . . ?
B6B C2B B3B C1B -36.8(4) . . . . ?
B6B C2B B3B B4B -2.6(6) . . . . ?
B6B C2B B3B B7B 102.8(5) . . . . ?
B6B C2B B3B B8B 61.3(6) . . . . ?
B6B C2B B7B B3B -106.0(5) . . . . ?
B6B C2B B7B B8B -67.3(5) . . . . ?
B6B C2B B7B B11B 35.7(4) . . . . ?
B6B C2B B7B B12B -5.3(6) . . . . ?
B6B C2B B11B B7B -141.7(5) . . . . ?
B6B C2B B11B B10B -38.8(4) . . . . ?
B6B C2B B11B B12B -101.0(5) . . . . ?
B6B B5B B9B B4B 102.9(5) . . . . ?
B6B B5B B9B B8B 65.6(5) . . . . ?
B6B B5B B9B B10B -35.7(4) . . . . ?
B6B B5B B9B B12B 2.2(6) . . . . ?
B6B B5B B10B B9B 138.4(5) . . . . ?
B6B B5B B10B B11B 37.8(4) . . . . ?
B6B B5B B10B B12B 100.6(5) . . . . ?
B6B B10B B11B C2B 39.9(4) . . . . ?
B6B B10B B11B B7B 101.9(5) . . . . ?
B6B B10B B11B B12B 138.3(5) . . . . ?
B6B B10B B12B B7B -0.3(6) . . . . ?
B6B B10B B12B B8B 64.8(6) . . . . ?
B6B B10B B12B B9B 101.5(5) . . . . ?
B6B B10B B12B B11B -37.1(4) . . . . ?
B6B B11B B12B B7B -103.2(5) . . . . ?
B6B B11B B12B B8B -65.1(6) . . . . ?
B6B B11B B12B B9B -1.1(6) . . . . ?
B6B B11B B12B B10B 36.1(4) . . . . ?
B7B C2B B3B C1B -139.6(4) . . . . ?
B7B C2B B3B B4B -105.4(5) . . . . ?
B7B C2B B3B B8B -41.5(4) . . . . ?
B7B C2B B6B C1B 103.6(5) . . . . ?
B7B C2B B6B B5B 69.6(5) . . . . ?
B7B C2B B6B B10B 5.2(6) . . . . ?
B7B C2B B6B B11B -36.1(5) . . . . ?
B7B C2B B11B B6B 141.7(5) . . . . ?
B7B C2B B11B B10B 102.8(5) . . . . ?
B7B C2B B11B B12B 40.7(4) . . . . ?
B7B B3B B4B C1B -95.3(5) . . . . ?
B7B B3B B4B B5B -60.4(6) . . . . ?
B7B B3B B4B B8B 40.0(4) . . . . ?
B7B B3B B4B B9B 3.0(6) . . . . ?
B7B B3B B8B B4B -137.0(5) . . . . ?
B7B B3B B8B B9B -99.7(5) . . . . ?
B7B B3B B8B B12B -36.4(5) . . . . ?
B7B B8B B9B B4B -101.3(5) . . . . ?
B7B B8B B9B B5B -64.2(6) . . . . ?
B7B B8B B9B B10B -0.1(6) . . . . ?
B7B B8B B9B B12B 36.4(4) . . . . ?
B7B B8B B12B B9B -138.5(5) . . . . ?
B7B B8B B12B B10B -101.9(5) . . . . ?
B7B B8B B12B B11B -37.6(4) . . . . ?
B7B B11B B12B B8B 38.0(5) . . . . ?
B7B B11B B12B B9B 102.1(5) . . . . ?
B7B B11B B12B B10B 139.3(5) . . . . ?
B8B B3B B4B C1B -135.3(5) . . . . ?
B8B B3B B4B B5B -100.4(5) . . . . ?
B8B B3B B4B B9B -37.0(4) . . . . ?
B8B B3B B7B C2B 134.2(5) . . . . ?
B8B B3B B7B B11B 100.1(5) . . . . ?
B8B B3B B7B B12B 36.7(5) . . . . ?
B8B B4B B5B C1B -96.5(5) . . . . ?
B8B B4B B5B B6B -60.9(6) . . . . ?
B8B B4B B5B B9B 37.2(4) . . . . ?
B8B B4B B5B B10B 0.2(6) . . . . ?
B8B B4B B9B B5B -138.6(5) . . . . ?
B8B B4B B9B B10B -101.3(5) . . . . ?
B8B B4B B9B B12B -37.7(4) . . . . ?
B8B B7B B11B C2B 95.8(5) . . . . ?
B8B B7B B11B B6B 61.0(6) . . . . ?
B8B B7B B11B B10B -0.7(6) . . . . ?
B8B B7B B11B B12B -37.2(4) . . . . ?
B8B B7B B12B B9B 37.5(5) . . . . ?
B8B B7B B12B B10B 101.4(5) . . . . ?
B8B B7B B12B B11B 138.4(5) . . . . ?
B8B B9B B10B B5B -101.1(5) . . . . ?
B8B B9B B10B B6B -63.5(6) . . . . ?
B8B B9B B10B B11B -0.3(6) . . . . ?
B8B B9B B10B B12B 36.5(4) . . . . ?
B8B B9B B12B B7B -38.0(5) . . . . ?
B8B B9B B12B B10B -139.3(5) . . . . ?
B8B B9B B12B B11B -101.9(5) . . . . ?
B9B B4B B5B C1B -133.6(5) . . . . ?
B9B B4B B5B B6B -98.0(5) . . . . ?
B9B B4B B5B B10B -36.9(4) . . . . ?
B9B B4B B8B B3B 138.1(5) . . . . ?
B9B B4B B8B B7B 99.7(5) . . . . ?
B9B B4B B8B B12B 37.6(4) . . . . ?
B9B B5B B6B C1B -98.0(4) . . . . ?
B9B B5B B6B C2B -64.9(5) . . . . ?
B9B B5B B6B B10B 36.7(4) . . . . ?
B9B B5B B6B B11B -3.0(6) . . . . ?
B9B B5B B10B B6B -138.4(5) . . . . ?
B9B B5B B10B B11B -100.6(5) . . . . ?
B9B B5B B10B B12B -37.8(4) . . . . ?
B9B B8B B12B B7B 138.5(5) . . . . ?
B9B B8B B12B B10B 36.6(4) . . . . ?
B9B B8B B12B B11B 101.0(5) . . . . ?
B9B B10B B11B C2B -61.4(5) . . . . ?
B9B B10B B11B B6B -101.3(5) . . . . ?
B9B B10B B11B B7B 0.6(6) . . . . ?
B9B B10B B11B B12B 37.0(4) . . . . ?
B9B B10B B12B B7B -101.8(5) . . . . ?
B9B B10B B12B B8B -36.7(4) . . . . ?
B9B B10B B12B B11B -138.6(5) . . . . ?
B10B B5B B6B C1B -134.6(4) . . . . ?
B10B B5B B6B C2B -101.5(5) . . . . ?
B10B B5B B6B B11B -39.7(4) . . . . ?
B10B B5B B9B B4B 138.6(5) . . . . ?
B10B B5B B9B B8B 101.3(5) . . . . ?
B10B B5B B9B B12B 38.0(4) . . . . ?
B10B B6B B11B C2B -134.3(5) . . . . ?
B10B B6B B11B B7B -99.9(5) . . . . ?
B10B B6B B11B B12B -36.9(4) . . . . ?
B10B B9B B12B B7B 101.3(5) . . . . ?
B10B B9B B12B B8B 139.3(5) . . . . ?
B10B B9B B12B B11B 37.4(4) . . . . ?
B10B B11B B12B B7B -139.3(5) . . . . ?
B10B B11B B12B B8B -101.2(5) . . . . ?
B10B B11B B12B B9B -37.2(4) . . . . ?
B11B C2B B3B C1B -103.5(4) . . . . ?
B11B C2B B3B B4B -69.3(5) . . . . ?
B11B C2B B3B B7B 36.1(4) . . . . ?
B11B C2B B3B B8B -5.4(6) . . . . ?
B11B C2B B6B C1B 139.7(5) . . . . ?
B11B C2B B6B B5B 105.8(5) . . . . ?
B11B C2B B6B B10B 41.4(4) . . . . ?
B11B C2B B7B B3B -141.7(5) . . . . ?
B11B C2B B7B B8B -103.0(5) . . . . ?
B11B C2B B7B B12B -41.0(5) . . . . ?
B11B B6B B10B B5B 137.5(5) . . . . ?
B11B B6B B10B B9B 100.4(5) . . . . ?
B11B B6B B10B B12B 37.0(4) . . . . ?
B11B B7B B8B B3B -101.1(5) . . . . ?
B11B B7B B8B B4B -62.3(6) . . . . ?
B11B B7B B8B B9B 0.5(6) . . . . ?
B11B B7B B8B B12B 37.4(4) . . . . ?
B11B B7B B12B B8B -138.4(5) . . . . ?
B11B B7B B12B B9B -100.9(5) . . . . ?
B11B B7B B12B B10B -36.9(5) . . . . ?
B11B B10B B12B B7B 36.8(5) . . . . ?
B11B B10B B12B B8B 101.9(5) . . . . ?
B11B B10B B12B B9B 138.6(5) . . . . ?
B12B B7B B8B B3B -138.5(5) . . . . ?
B12B B7B B8B B4B -99.7(5) . . . . ?
B12B B7B B8B B9B -36.9(4) . . . . ?
B12B B7B B11B C2B 133.0(5) . . . . ?
B12B B7B B11B B6B 98.2(5) . . . . ?
B12B B7B B11B B10B 36.5(4) . . . . ?
B12B B8B B9B B4B -137.7(5) . . . . ?
B12B B8B B9B B5B -100.6(5) . . . . ?
B12B B8B B9B B10B -36.6(4) . . . . ?
B12B B9B B10B B5B -137.5(5) . . . . ?
B12B B9B B10B B6B -100.0(5) . . . . ?
B12B B9B B10B B11B -36.8(4) . . . . ?
B12B B10B B11B C2B -98.4(5) . . . . ?
B12B B10B B11B B6B -138.3(5) . . . . ?
B12B B10B B11B B7B -36.4(4) . . . . ?

_shelx_SHELXL_version_number     2014/7
_olex2_submission_special_instructions 'No special instructions were received'
