# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2017

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_2
_database_code_depnum_ccdc_archive 'CCDC 1538031'
_audit_update_record             
;
2017-03-15 deposited with the CCDC.
2017-04-19 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
 ?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C16 H6 Ag8 N8 O18'
_chemical_formula_weight         1461.25

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   Pna21

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x+1/2, -y+1/2, z'
'-x+1/2, y+1/2, z+1/2'

_cell_length_a                   7.7110(15)
_cell_length_b                   18.586(4)
_cell_length_c                   20.928(4)
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_volume                     2999.3(10)
_cell_formula_units_Z            4
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    6058
_cell_measurement_theta_min      1.95
_cell_measurement_theta_max      27.72

_exptl_crystal_description       needle
_exptl_crystal_colour            yellow
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.03
_exptl_crystal_size_min          0.03
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    3.236
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2712
_exptl_absorpt_coefficient_mu    5.202
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.826
_exptl_absorpt_correction_T_max  0.858
_exptl_absorpt_process_details   ?

_exptl_special_details           
;
 ?
;

_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            10443
_diffrn_reflns_av_R_equivalents  0.0848
_diffrn_reflns_av_sigmaI/netI    0.0608
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_theta_min         1.95
_diffrn_reflns_theta_max         27.72
_reflns_number_total             6642
_reflns_number_gt                6058
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker SMART'
_computing_cell_refinement       'Bruker SMART'
_computing_data_reduction        'Bruker SAIT'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.1261P)²+7.6636P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.51(6)
_refine_ls_number_reflns         6642
_refine_ls_number_parameters     501
_refine_ls_number_restraints     37
_refine_ls_R_factor_all          0.0682
_refine_ls_R_factor_gt           0.0636
_refine_ls_wR_factor_ref         0.1826
_refine_ls_wR_factor_gt          0.1747
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_restrained_S_all      1.026
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag3A Ag 1.069(2) -0.1876(7) 0.7539(9) 0.071(4) Uani 0.15 1 d P . .
Ag3 Ag 1.1347(2) -0.18993(14) 0.76038(13) 0.0498(4) Uani 0.85 1 d P . 1
Ag2 Ag 0.90048(14) -0.10165(6) 0.84258(7) 0.0643(3) Uani 1 1 d . . .
Ag1 Ag 1.29688(14) -0.09117(6) 0.85384(6) 0.0584(3) Uani 1 1 d . . 1
C9A C 1.104(4) 0.2546(17) 0.7774(14) 0.034(5) Uani 0.30 1 d PU . .
Ag4 Ag 0.76342(13) 0.58151(4) 0.66177(6) 0.0533(2) Uani 1 1 d . . .
Ag7 Ag 1.09550(14) 0.59489(6) 0.47139(6) 0.0597(3) Uani 1 1 d . . 1
Ag5 Ag 0.9785(3) 0.68442(12) 0.57555(10) 0.0525(4) Uani 0.80 1 d P . 1
Ag6 Ag 0.71648(14) 0.60521(7) 0.49231(8) 0.0739(4) Uani 1 1 d . . 1
O7 O 1.2232(12) -0.3127(5) 0.7567(6) 0.062(2) Uani 1 1 d . . .
O8 O 0.9769(12) -0.3091(5) 0.7048(5) 0.055(2) Uani 1 1 d . . .
O11 O 1.0661(12) 0.8218(6) 0.6181(5) 0.060(2) Uani 1 1 d . . .
N1 N 1.0376(12) 0.3429(5) 0.6941(5) 0.0456(19) Uani 1 1 d . . .
N4 N 0.8817(16) -0.2579(6) 0.9021(5) 0.055(2) Uani 1 1 d . . .
O12 O 0.7973(14) 0.7964(6) 0.5905(7) 0.075(3) Uani 1 1 d . . .
C14 C 1.0917(17) 0.1285(7) 0.7629(6) 0.054(3) Uani 1 1 d . . .
H14 H 1.1326 0.1210 0.8041 0.065 Uiso 1 1 d R . .
C11 C 1.0104(12) 0.2096(5) 0.6772(5) 0.0374(18) Uani 1 1 d . . .
N2 N 1.0703(13) 0.1982(5) 0.7400(5) 0.0454(19) Uani 1 1 d . . .
C12 C 0.9937(15) 0.0797(5) 0.6589(7) 0.049(2) Uani 1 1 d . . .
H12 H 0.9700 0.0397 0.6337 0.058 Uiso 1 1 d R . .
C3 C 0.9588(15) 0.4286(6) 0.6087(5) 0.043(2) Uani 1 1 d . . .
C7 C 1.0213(18) 0.4135(5) 0.6718(6) 0.051(3) Uani 1 1 d . . .
H7 H 1.0482 0.4509 0.6996 0.061 Uiso 1 1 d R . .
O13 O 0.6990(19) 0.6855(5) 0.3966(5) 0.069(3) Uani 1 1 d . . .
C6 C 0.9967(12) 0.2845(6) 0.6536(5) 0.041(2) Uani 1 1 d . . .
O16 O 0.4141(14) 0.5708(7) 0.4689(8) 0.085(4) Uani 1 1 d . . .
C1 C 0.9213(14) 0.5635(6) 0.5584(6) 0.047(2) Uani 1 1 d . . .
N6 N 0.9086(11) 0.8436(5) 0.6095(5) 0.046(2) Uani 1 1 d . . .
N8 N 0.4171(17) 0.5038(9) 0.4680(7) 0.078(4) Uani 1 1 d . . .
C2 C 0.9360(15) 0.5019(6) 0.5852(6) 0.047(2) Uani 1 1 d . . .
N3 N 1.6159(17) 0.0120(9) 0.8522(7) 0.073(4) Uani 1 1 d . . .
C13 C 1.0577(16) 0.0670(6) 0.7215(7) 0.053(3) Uani 1 1 d . . .
C5 C 0.9334(13) 0.2971(5) 0.5882(4) 0.0359(18) Uani 1 1 d U . .
O9 O 1.0860(16) -0.4163(5) 0.7312(6) 0.069(3) Uani 1 1 d . . .
O5 O 0.9447(18) -0.2669(5) 0.8478(6) 0.076(3) Uani 1 1 d . . .
O10 O 0.869(2) 0.9078(6) 0.6184(10) 0.094(5) Uani 1 1 d . . .
O18 O 0.2710(17) 0.4717(9) 0.4644(8) 0.103(5) Uani 1 1 d . . .
O2 O 1.4754(19) 0.0492(9) 0.8545(7) 0.095(4) Uani 1 1 d . . .
O3 O 1.6048(14) -0.0549(8) 0.8713(7) 0.077(3) Uani 1 1 d . . .
N5 N 1.0989(12) -0.3478(5) 0.7301(5) 0.0443(19) Uani 1 1 d . . .
C4 C 0.9179(13) 0.3688(6) 0.5671(6) 0.045(2) Uani 1 1 d . . .
H4 H 0.8849 0.3786 0.5253 0.054 Uiso 1 1 d R . .
O6 O 0.837(2) -0.3138(5) 0.9334(6) 0.084(4) Uani 1 1 d . . .
O4 O 0.867(3) -0.1951(6) 0.9258(7) 0.100(5) Uani 1 1 d . . .
O1 O 1.7579(19) 0.0371(7) 0.8357(14) 0.137(10) Uani 1 1 d . . .
C8 C 0.893(2) 0.2353(10) 0.5512(10) 0.054(4) Uani 0.70 1 d PU . .
H8 H 0.8641 0.2422 0.5085 0.065 Uiso 1 1 d R . .
C10 C 0.9674(15) 0.1519(6) 0.6337(6) 0.044(2) Uani 1 1 d . . .
O17 O 0.5623(18) 0.4701(9) 0.4703(11) 0.118(7) Uani 1 1 d U . .
C9 C 0.909(2) 0.1667(11) 0.5713(9) 0.053(4) Uani 0.70 1 d PU . .
H9 H 0.8664 0.1294 0.5461 0.064 Uiso 1 1 d R . .
C15 C 1.0937(16) -0.0060(7) 0.7440(8) 0.059(3) Uani 1 1 d . . .
C16 C 1.1192(17) -0.0683(6) 0.7692(6) 0.051(3) Uani 1 1 d . . .
N7 N 0.6428(14) 0.7437(5) 0.4254(5) 0.051(2) Uani 1 1 d . . .
O15 O 0.653(2) 0.8050(6) 0.3972(6) 0.088(4) Uani 1 1 d . . .
Ag8 Ag 1.1249(2) 0.31112(8) 0.80145(7) 0.0597(4) Uani 0.70 1 d P . 1
Ag8A Ag 0.8811(4) 0.18496(14) 0.52484(12) 0.0464(6) Uani 0.30 1 d P . 2
O14 O 0.5783(18) 0.7336(6) 0.4804(5) 0.075(3) Uani 1 1 d . . 2
Ag5A Ag 0.9029(14) 0.6871(4) 0.5688(5) 0.060(2) Uani 0.20 1 d P . .
C8A C 1.087(5) 0.325(2) 0.758(2) 0.049(8) Uani 0.30 1 d PU . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag3A Ag3 0.529(17) . ?
Ag3A C16 2.274(18) . ?
Ag3A O8 2.581(18) . ?
Ag3A Ag2 2.770(18) . ?
Ag3A Ag4 3.141(17) 3 ?
Ag3A Ag1 3.268(17) . ?
Ag3 C16 2.272(12) . ?
Ag3 O7 2.383(10) . ?
Ag3 Ag1 2.960(3) . ?
Ag3 Ag2 2.985(3) . ?
Ag3 Ag4 3.050(3) 3 ?
Ag2 C16 2.363(13) . ?
Ag2 O4 2.473(13) . ?
Ag2 O3 2.513(11) 1_455 ?
Ag2 Ag1 3.0718(17) . ?
Ag1 C16 2.279(13) . ?
Ag1 O6 2.447(12) 3_545 ?
Ag1 O3 2.495(12) . ?
C9A Ag8 1.18(3) . ?
C9A N2 1.33(3) . ?
C9A C8A 1.38(5) . ?
Ag4 C1 2.505(13) . ?
Ag4 C16 2.521(13) 3_455 ?
Ag4 O11 2.526(10) 3_465 ?
Ag4 C2 2.556(11) . ?
Ag4 C15 2.576(15) 3_455 ?
Ag4 Ag5A 2.965(10) . ?
Ag4 Ag3 3.050(3) 3_455 ?
Ag4 Ag5 3.109(2) . ?
Ag4 Ag3A 3.141(17) 3_455 ?
Ag7 C1 2.336(13) . ?
Ag7 O15 2.462(12) 3_565 ?
Ag7 O16 2.497(11) 1_655 ?
Ag7 Ag5 2.887(3) . ?
Ag7 Ag6 2.9615(16) . ?
Ag7 Ag5A 3.049(10) . ?
Ag5 Ag5A 0.602(9) . ?
Ag5 C1 2.317(12) . ?
Ag5 O12 2.504(12) 3_565 ?
Ag5 O12 2.527(12) . ?
Ag5 Ag6 3.047(3) . ?
Ag6 C1 2.237(11) . ?
Ag6 O16 2.467(12) . ?
Ag6 O13 2.501(10) . ?
Ag6 Ag5A 2.635(9) . ?
O7 N5 1.285(13) . ?
O8 N5 1.296(13) . ?
O11 N6 1.293(14) . ?
O11 Ag4 2.526(10) 3_565 ?
N1 C7 1.399(13) . ?
N1 C6 1.412(15) . ?
N1 C8A 1.42(5) . ?
N1 Ag8 2.418(10) . ?
N4 O5 1.246(16) . ?
N4 O4 1.273(15) . ?
N4 O6 1.275(15) . ?
O12 N6 1.290(14) . ?
O12 Ag5A 2.236(14) . ?
O12 Ag5 2.504(11) 3_465 ?
C14 N2 1.391(15) . ?
C14 C13 1.458(19) . ?
C14 H14 0.9298 . ?
C11 N2 1.408(13) . ?
C11 C10 1.444(15) . ?
C11 C6 1.482(13) . ?
N2 Ag8 2.497(10) . ?
C12 C13 1.42(2) . ?
C12 C10 1.456(14) . ?
C12 H12 0.9300 . ?
C3 C7 1.434(16) . ?
C3 C4 1.445(16) . ?
C3 C2 1.459(15) . ?
C7 H7 0.9299 . ?
O13 N7 1.312(13) . ?
O13 Ag8 2.411(11) 2_764 ?
C6 C5 1.473(13) . ?
O16 N8 1.245(19) . ?
O16 Ag7 2.497(11) 1_455 ?
C1 C2 1.281(16) . ?
C1 Ag5A 2.310(14) . ?
N6 O10 1.245(14) . ?
N8 O18 1.277(18) . ?
N8 O17 1.284(18) . ?
N3 O1 1.24(2) . ?
N3 O2 1.286(18) . ?
N3 O3 1.31(2) . ?
C13 C15 1.463(16) . ?
C5 C4 1.408(14) . ?
C5 C8 1.42(2) . ?
C5 Ag8A 2.503(10) . ?
O9 N5 1.278(13) . ?
O3 Ag2 2.513(11) 1_655 ?
C4 H4 0.9299 . ?
O6 Ag1 2.447(12) 3_445 ?
O6 Ag8A 2.550(12) 4_645 ?
C8 Ag8A 1.091(19) . ?
C8 C9 1.35(3) . ?
C8 H8 0.9300 . ?
C10 C9 1.41(2) . ?
C10 Ag8A 2.453(12) . ?
C9 Ag8A 1.05(2) . ?
C9 H9 0.9299 . ?
C15 C16 1.287(18) . ?
C15 Ag4 2.576(15) 3 ?
C16 Ag4 2.521(13) 3 ?
N7 O14 1.267(15) . ?
N7 O15 1.287(14) . ?
O15 Ag7 2.462(12) 3_465 ?
Ag8 C8A 1.00(5) . ?
Ag8 O13 2.411(11) 2_765 ?
Ag8A O6 2.550(12) 4_654 ?
Ag8A H8 1.1243 . ?
Ag8A H9 1.1291 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag3 Ag3A C16 83.1(18) . . ?
Ag3 Ag3A O8 107(2) . . ?
C16 Ag3A O8 163.0(9) . . ?
Ag3 Ag3A Ag2 109(2) . . ?
C16 Ag3A Ag2 54.8(5) . . ?
O8 Ag3A Ag2 130.1(7) . . ?
Ag3 Ag3A Ag4 75(2) . 3 ?
C16 Ag3A Ag4 52.6(5) . 3 ?
O8 Ag3A Ag4 115.8(7) . 3 ?
Ag2 Ag3A Ag4 105.9(4) . 3 ?
Ag3 Ag3A Ag1 50.4(19) . . ?
C16 Ag3A Ag1 44.2(4) . . ?
O8 Ag3A Ag1 151.9(7) . . ?
Ag2 Ag3A Ag1 60.5(3) . . ?
Ag4 Ag3A Ag1 77.9(3) 3 . ?
Ag3A Ag3 C16 83.6(18) . . ?
Ag3A Ag3 O7 110.3(18) . . ?
C16 Ag3 O7 166.1(4) . . ?
Ag3A Ag3 Ag1 122(2) . . ?
C16 Ag3 Ag1 49.5(3) . . ?
O7 Ag3 Ag1 119.6(3) . . ?
Ag3A Ag3 Ag2 61(2) . . ?
C16 Ag3 Ag2 51.3(3) . . ?
O7 Ag3 Ag2 135.9(3) . . ?
Ag1 Ag3 Ag2 62.22(7) . . ?
Ag3A Ag3 Ag4 95(2) . 3 ?
C16 Ag3 Ag4 54.2(3) . 3 ?
O7 Ag3 Ag4 121.2(3) . 3 ?
Ag1 Ag3 Ag4 84.25(7) . 3 ?
Ag2 Ag3 Ag4 102.93(8) . 3 ?
C16 Ag2 O4 135.7(6) . . ?
C16 Ag2 O3 135.4(4) . 1_455 ?
O4 Ag2 O3 88.9(6) . 1_455 ?
C16 Ag2 Ag3A 51.9(4) . . ?
O4 Ag2 Ag3A 96.6(5) . . ?
O3 Ag2 Ag3A 141.6(5) 1_455 . ?
C16 Ag2 Ag3 48.6(3) . . ?
O4 Ag2 Ag3 94.7(4) . . ?
O3 Ag2 Ag3 151.2(4) 1_455 . ?
Ag3A Ag2 Ag3 9.6(4) . . ?
C16 Ag2 Ag1 47.4(3) . . ?
O4 Ag2 Ag1 95.4(5) . . ?
O3 Ag2 Ag1 149.6(4) 1_455 . ?
Ag3A Ag2 Ag1 67.8(4) . . ?
Ag3 Ag2 Ag1 58.48(5) . . ?
C16 Ag1 O6 137.7(5) . 3_545 ?
C16 Ag1 O3 129.5(4) . . ?
O6 Ag1 O3 88.5(5) 3_545 . ?
C16 Ag1 Ag3 49.3(3) . . ?
O6 Ag1 Ag3 93.2(3) 3_545 . ?
O3 Ag1 Ag3 131.8(3) . . ?
C16 Ag1 Ag2 49.8(3) . . ?
O6 Ag1 Ag2 97.7(4) 3_545 . ?
O3 Ag1 Ag2 167.2(3) . . ?
Ag3 Ag1 Ag2 59.30(5) . . ?
C16 Ag1 Ag3A 44.1(4) . . ?
O6 Ag1 Ag3A 96.2(5) 3_545 . ?
O3 Ag1 Ag3A 139.0(5) . . ?
Ag3 Ag1 Ag3A 7.9(3) . . ?
Ag2 Ag1 Ag3A 51.7(3) . . ?
Ag8 C9A N2 169(3) . . ?
Ag8 C9A C8A 45(2) . . ?
N2 C9A C8A 124(3) . . ?
C1 Ag4 C16 166.4(3) . 3_455 ?
C1 Ag4 O11 94.3(4) . 3_465 ?
C16 Ag4 O11 97.3(4) 3_455 3_465 ?
C1 Ag4 C2 29.3(4) . . ?
C16 Ag4 C2 137.1(4) 3_455 . ?
O11 Ag4 C2 119.9(4) 3_465 . ?
C1 Ag4 C15 138.7(4) . 3_455 ?
C16 Ag4 C15 29.2(4) 3_455 3_455 ?
O11 Ag4 C15 108.8(4) 3_465 3_455 ?
C2 Ag4 C15 111.6(4) . 3_455 ?
C1 Ag4 Ag5A 49.1(3) . . ?
C16 Ag4 Ag5A 144.1(3) 3_455 . ?
O11 Ag4 Ag5A 60.7(3) 3_465 . ?
C2 Ag4 Ag5A 77.5(3) . . ?
C15 Ag4 Ag5A 169.3(3) 3_455 . ?
C1 Ag4 Ag3 146.2(3) . 3_455 ?
C16 Ag4 Ag3 46.9(3) 3_455 3_455 ?
O11 Ag4 Ag3 65.1(3) 3_465 3_455 ?
C2 Ag4 Ag3 167.5(3) . 3_455 ?
C15 Ag4 Ag3 75.1(3) 3_455 3_455 ?
Ag5A Ag4 Ag3 97.18(19) . 3_455 ?
C1 Ag4 Ag5 47.3(3) . . ?
C16 Ag4 Ag5 144.4(3) 3_455 . ?
O11 Ag4 Ag5 71.0(2) 3_465 . ?
C2 Ag4 Ag5 73.4(3) . . ?
C15 Ag4 Ag5 173.4(3) 3_455 . ?
Ag5A Ag4 Ag5 11.05(18) . . ?
Ag3 Ag4 Ag5 99.20(7) 3_455 . ?
C1 Ag4 Ag3A 147.8(4) . 3_455 ?
C16 Ag4 Ag3A 45.8(4) 3_455 3_455 ?
O11 Ag4 Ag3A 59.2(4) 3_465 3_455 ?
C2 Ag4 Ag3A 176.2(4) . 3_455 ?
C15 Ag4 Ag3A 71.9(4) 3_455 3_455 ?
Ag5A Ag4 Ag3A 99.3(3) . 3_455 ?
Ag3 Ag4 Ag3A 9.7(3) 3_455 3_455 ?
Ag5 Ag4 Ag3A 103.0(3) . 3_455 ?
C1 Ag7 O15 141.5(5) . 3_565 ?
C1 Ag7 O16 122.5(4) . 1_655 ?
O15 Ag7 O16 86.9(5) 3_565 1_655 ?
C1 Ag7 Ag5 51.4(3) . . ?
O15 Ag7 Ag5 95.6(3) 3_565 . ?
O16 Ag7 Ag5 115.3(4) 1_655 . ?
C1 Ag7 Ag6 48.2(3) . . ?
O15 Ag7 Ag6 102.7(4) 3_565 . ?
O16 Ag7 Ag6 170.2(3) 1_655 . ?
Ag5 Ag7 Ag6 62.78(5) . . ?
C1 Ag7 Ag5A 48.6(3) . . ?
O15 Ag7 Ag5A 94.8(3) 3_565 . ?
O16 Ag7 Ag5A 126.4(4) 1_655 . ?
Ag5 Ag7 Ag5A 11.22(17) . . ?
Ag6 Ag7 Ag5A 51.97(19) . . ?
Ag5A Ag5 C1 81.9(10) . . ?
Ag5A Ag5 O12 165.6(11) . 3_565 ?
C1 Ag5 O12 110.1(4) . 3_565 ?
Ag5A Ag5 O12 55.0(10) . . ?
C1 Ag5 O12 135.5(4) . . ?
O12 Ag5 O12 114.2(3) 3_565 . ?
Ag5A Ag5 Ag7 99.9(11) . . ?
C1 Ag5 Ag7 52.0(3) . . ?
O12 Ag5 Ag7 82.5(3) 3_565 . ?
O12 Ag5 Ag7 137.8(4) . . ?
Ag5A Ag5 Ag6 42.5(10) . . ?
C1 Ag5 Ag6 46.9(3) . . ?
O12 Ag5 Ag6 142.3(4) 3_565 . ?
O12 Ag5 Ag6 95.9(3) . . ?
Ag7 Ag5 Ag6 59.80(6) . . ?
Ag5A Ag5 Ag4 70.8(10) . . ?
C1 Ag5 Ag4 52.6(3) . . ?
O12 Ag5 Ag4 122.6(3) 3_565 . ?
O12 Ag5 Ag4 98.1(3) . . ?
Ag7 Ag5 Ag4 104.50(7) . . ?
Ag6 Ag5 Ag4 71.39(6) . . ?
C1 Ag6 O16 134.5(4) . . ?
C1 Ag6 O13 137.7(5) . . ?
O16 Ag6 O13 86.8(5) . . ?
C1 Ag6 Ag5A 55.9(4) . . ?
O16 Ag6 Ag5A 141.8(4) . . ?
O13 Ag6 Ag5A 99.9(3) . . ?
C1 Ag6 Ag7 51.1(3) . . ?
O16 Ag6 Ag7 152.4(4) . . ?
O13 Ag6 Ag7 88.5(3) . . ?
Ag5A Ag6 Ag7 65.7(2) . . ?
C1 Ag6 Ag5 49.1(3) . . ?
O16 Ag6 Ag5 149.9(4) . . ?
O13 Ag6 Ag5 101.9(3) . . ?
Ag5A Ag6 Ag5 8.9(2) . . ?
Ag7 Ag6 Ag5 57.42(5) . . ?
N5 O7 Ag3 106.6(7) . . ?
N5 O8 Ag3A 97.1(7) . . ?
N6 O11 Ag4 113.2(7) . 3_565 ?
C7 N1 C6 120.0(10) . . ?
C7 N1 C8A 123.6(19) . . ?
C6 N1 C8A 116.3(18) . . ?
C7 N1 Ag8 124.3(8) . . ?
C6 N1 Ag8 115.6(6) . . ?
C8A N1 Ag8 1.0(17) . . ?
O5 N4 O4 120.8(13) . . ?
O5 N4 O6 117.6(11) . . ?
O4 N4 O6 121.6(12) . . ?
N6 O12 Ag5A 116.0(8) . . ?
N6 O12 Ag5 126.5(8) . 3_465 ?
Ag5A O12 Ag5 117.5(5) . 3_465 ?
N6 O12 Ag5 103.3(8) . . ?
Ag5A O12 Ag5 12.7(3) . . ?
Ag5 O12 Ag5 130.1(4) 3_465 . ?
N2 C14 C13 120.3(11) . . ?
N2 C14 H14 120.0 . . ?
C13 C14 H14 119.6 . . ?
N2 C11 C10 123.5(9) . . ?
N2 C11 C6 118.3(9) . . ?
C10 C11 C6 118.1(9) . . ?
C9A N2 C14 120.5(16) . . ?
C9A N2 C11 119.6(16) . . ?
C14 N2 C11 120.0(10) . . ?
C9A N2 Ag8 5.4(13) . . ?
C14 N2 Ag8 125.8(8) . . ?
C11 N2 Ag8 114.2(7) . . ?
C13 C12 C10 122.4(10) . . ?
C13 C12 H12 117.3 . . ?
C10 C12 H12 120.3 . . ?
C7 C3 C4 118.5(10) . . ?
C7 C3 C2 122.3(10) . . ?
C4 C3 C2 119.2(10) . . ?
N1 C7 C3 121.4(11) . . ?
N1 C7 H7 118.2 . . ?
C3 C7 H7 120.3 . . ?
N7 O13 Ag8 123.0(7) . 2_764 ?
N7 O13 Ag6 98.1(7) . . ?
Ag8 O13 Ag6 130.3(5) 2_764 . ?
N1 C6 C5 120.6(9) . . ?
N1 C6 C11 120.4(9) . . ?
C5 C6 C11 118.9(9) . . ?
N8 O16 Ag6 104.1(9) . . ?
N8 O16 Ag7 101.4(9) . 1_455 ?
Ag6 O16 Ag7 151.5(7) . 1_455 ?
C2 C1 Ag6 130.0(9) . . ?
C2 C1 Ag5A 148.6(11) . . ?
Ag6 C1 Ag5A 70.8(4) . . ?
C2 C1 Ag5 141.5(10) . . ?
Ag6 C1 Ag5 84.0(4) . . ?
Ag5A C1 Ag5 14.9(2) . . ?
C2 C1 Ag7 120.9(9) . . ?
Ag6 C1 Ag7 80.7(4) . . ?
Ag5A C1 Ag7 82.0(4) . . ?
Ag5 C1 Ag7 76.7(3) . . ?
C2 C1 Ag4 77.5(8) . . ?
Ag6 C1 Ag4 98.3(4) . . ?
Ag5A C1 Ag4 75.9(5) . . ?
Ag5 C1 Ag4 80.2(4) . . ?
Ag7 C1 Ag4 156.8(5) . . ?
O10 N6 O12 122.3(12) . . ?
O10 N6 O11 120.6(11) . . ?
O12 N6 O11 117.0(10) . . ?
O16 N8 O18 116.9(15) . . ?
O16 N8 O17 120.2(14) . . ?
O18 N8 O17 122.9(17) . . ?
C1 C2 C3 173.5(13) . . ?
C1 C2 Ag4 73.2(8) . . ?
C3 C2 Ag4 113.1(7) . . ?
O1 N3 O2 123.6(19) . . ?
O1 N3 O3 120.0(14) . . ?
O2 N3 O3 116.4(15) . . ?
C12 C13 C14 118.7(10) . . ?
C12 C13 C15 121.1(12) . . ?
C14 C13 C15 120.2(13) . . ?
C4 C5 C8 125.3(11) . . ?
C4 C5 C6 118.0(9) . . ?
C8 C5 C6 116.7(11) . . ?
C4 C5 Ag8A 127.5(7) . . ?
C8 C5 Ag8A 3.7(8) . . ?
C6 C5 Ag8A 114.4(6) . . ?
N3 O3 Ag1 105.9(9) . . ?
N3 O3 Ag2 101.3(8) . 1_655 ?
Ag1 O3 Ag2 137.3(6) . 1_655 ?
O9 N5 O7 123.7(10) . . ?
O9 N5 O8 120.2(10) . . ?
O7 N5 O8 115.9(10) . . ?
C5 C4 C3 121.4(10) . . ?
C5 C4 H4 120.2 . . ?
C3 C4 H4 118.4 . . ?
N4 O6 Ag1 105.9(8) . 3_445 ?
N4 O6 Ag8A 124.7(9) . 4_645 ?
Ag1 O6 Ag8A 114.8(5) 3_445 4_645 ?
N4 O4 Ag2 111.1(10) . . ?
Ag8A C8 C9 49.7(12) . . ?
Ag8A C8 C5 171.6(17) . . ?
C9 C8 C5 125.2(18) . . ?
Ag8A C8 H8 67.1 . . ?
C9 C8 H8 116.8 . . ?
C5 C8 H8 117.7 . . ?
C9 C10 C11 120.9(12) . . ?
C9 C10 C12 124.0(12) . . ?
C11 C10 C12 115.1(10) . . ?
C9 C10 Ag8A 4.3(8) . . ?
C11 C10 Ag8A 117.5(7) . . ?
C12 C10 Ag8A 127.2(8) . . ?
Ag8A C9 C8 52.3(12) . . ?
Ag8A C9 C10 169.9(19) . . ?
C8 C9 C10 120.1(17) . . ?
Ag8A C9 H9 69.1 . . ?
C8 C9 H9 119.7 . . ?
C10 C9 H9 119.6 . . ?
C16 C15 C13 174.2(16) . . ?
C16 C15 Ag4 73.0(9) . 3 ?
C13 C15 Ag4 112.8(10) . 3 ?
C15 C16 Ag3 150.4(12) . . ?
C15 C16 Ag3A 142.4(13) . . ?
Ag3 C16 Ag3A 13.4(4) . . ?
C15 C16 Ag1 125.3(11) . . ?
Ag3 C16 Ag1 81.1(4) . . ?
Ag3A C16 Ag1 91.7(6) . . ?
C15 C16 Ag2 113.2(10) . . ?
Ag3 C16 Ag2 80.2(4) . . ?
Ag3A C16 Ag2 73.3(6) . . ?
Ag1 C16 Ag2 82.8(4) . . ?
C15 C16 Ag4 77.8(9) . 3 ?
Ag3 C16 Ag4 78.9(4) . 3 ?
Ag3A C16 Ag4 81.7(6) . 3 ?
Ag1 C16 Ag4 114.2(5) . 3 ?
Ag2 C16 Ag4 150.3(6) . 3 ?
O14 N7 O15 124.8(12) . . ?
O14 N7 O13 115.1(10) . . ?
O15 N7 O13 120.1(11) . . ?
N7 O15 Ag7 111.7(9) . 3_465 ?
C8A Ag8 C9A 78(3) . . ?
C8A Ag8 O13 157(2) . 2_765 ?
C9A Ag8 O13 117.0(15) . 2_765 ?
C8A Ag8 N1 1(2) . . ?
C9A Ag8 N1 77.4(15) . . ?
O13 Ag8 N1 156.6(4) 2_765 . ?
C8A Ag8 N2 72(2) . . ?
C9A Ag8 N2 6.1(15) . . ?
O13 Ag8 N2 122.8(3) 2_765 . ?
N1 Ag8 N2 71.3(3) . . ?
C9 Ag8A C8 78.0(15) . . ?
C9 Ag8A C10 5.8(11) . . ?
C8 Ag8A C10 73.8(11) . . ?
C9 Ag8A C5 75.3(11) . . ?
C8 Ag8A C5 4.8(10) . . ?
C10 Ag8A C5 70.9(3) . . ?
C9 Ag8A O6 146.1(11) . 4_654 ?
C8 Ag8A O6 115.4(10) . 4_654 ?
C10 Ag8A O6 151.5(5) . 4_654 ?
C5 Ag8A O6 119.8(3) . 4_654 ?
C9 Ag8A H8 127.5 . . ?
C8 Ag8A H8 49.6 . . ?
C10 Ag8A H8 123.4 . . ?
C5 Ag8A H8 52.5 . . ?
O6 Ag8A H8 71.8 4_654 . ?
C9 Ag8A H9 50.3 . . ?
C8 Ag8A H9 126.4 . . ?
C10 Ag8A H9 55.4 . . ?
C5 Ag8A H9 124.7 . . ?
O6 Ag8A H9 103.7 4_654 . ?
H8 Ag8A H9 166.4 . . ?
Ag5 Ag5A O12 112.3(11) . . ?
Ag5 Ag5A C1 83.2(10) . . ?
O12 Ag5A C1 160.9(7) . . ?
Ag5 Ag5A Ag6 128.6(12) . . ?
O12 Ag5A Ag6 116.7(5) . . ?
C1 Ag5A Ag6 53.3(3) . . ?
Ag5 Ag5A Ag4 98.2(11) . . ?
O12 Ag5A Ag4 109.6(5) . . ?
C1 Ag5A Ag4 55.0(4) . . ?
Ag6 Ag5A Ag4 79.6(2) . . ?
Ag5 Ag5A Ag7 68.9(10) . . ?
O12 Ag5A Ag7 145.5(6) . . ?
C1 Ag5A Ag7 49.4(4) . . ?
Ag6 Ag5A Ag7 62.3(2) . . ?
Ag4 Ag5A Ag7 104.1(3) . . ?
Ag8 C8A C9A 57(2) . . ?
Ag8 C8A N1 177(4) . . ?
C9A C8A N1 122(3) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O8 Ag3A Ag3 C16 166.1(14) . . . . ?
Ag2 Ag3A Ag3 C16 -49.0(10) . . . . ?
Ag4 Ag3A Ag3 C16 53.1(5) 3 . . . ?
Ag1 Ag3A Ag3 C16 -33.3(16) . . . . ?
C16 Ag3A Ag3 O7 -178.9(9) . . . . ?
O8 Ag3A Ag3 O7 -13(2) . . . . ?
Ag2 Ag3A Ag3 O7 132.1(8) . . . . ?
Ag4 Ag3A Ag3 O7 -125.9(12) 3 . . . ?
Ag1 Ag3A Ag3 O7 148(2) . . . . ?
C16 Ag3A Ag3 Ag1 33.3(16) . . . . ?
O8 Ag3A Ag3 Ag1 -160.7(5) . . . . ?
Ag2 Ag3A Ag3 Ag1 -16(2) . . . . ?
Ag4 Ag3A Ag3 Ag1 86.3(13) 3 . . . ?
C16 Ag3A Ag3 Ag2 49.0(10) . . . . ?
O8 Ag3A Ag3 Ag2 -145(2) . . . . ?
Ag4 Ag3A Ag3 Ag2 102.0(11) 3 . . . ?
Ag1 Ag3A Ag3 Ag2 16(2) . . . . ?
C16 Ag3A Ag3 Ag4 -53.1(5) . . . 3 ?
O8 Ag3A Ag3 Ag4 113.0(11) . . . 3 ?
Ag2 Ag3A Ag3 Ag4 -102.0(11) . . . 3 ?
Ag1 Ag3A Ag3 Ag4 -86.3(13) . . . 3 ?
Ag3 Ag3A Ag2 C16 66(2) . . . . ?
O8 Ag3A Ag2 C16 -159.4(12) . . . . ?
Ag4 Ag3A Ag2 C16 -13.3(4) 3 . . . ?
Ag1 Ag3A Ag2 C16 52.5(5) . . . . ?
Ag3 Ag3A Ag2 O4 -79(2) . . . . ?
C16 Ag3A Ag2 O4 -145.6(7) . . . . ?
O8 Ag3A Ag2 O4 54.9(10) . . . . ?
Ag4 Ag3A Ag2 O4 -158.9(6) 3 . . . ?
Ag1 Ag3A Ag2 O4 -93.1(5) . . . . ?
Ag3 Ag3A Ag2 O3 -175.8(19) . . . 1_455 ?
C16 Ag3A Ag2 O3 117.8(7) . . . 1_455 ?
O8 Ag3A Ag2 O3 -41.6(13) . . . 1_455 ?
Ag4 Ag3A Ag2 O3 104.5(7) 3 . . 1_455 ?
Ag1 Ag3A Ag2 O3 170.3(6) . . . 1_455 ?
C16 Ag3A Ag2 Ag3 -66(2) . . . . ?
O8 Ag3A Ag2 Ag3 134(3) . . . . ?
Ag4 Ag3A Ag2 Ag3 -80(2) 3 . . . ?
Ag1 Ag3A Ag2 Ag3 -14(2) . . . . ?
Ag3 Ag3A Ag2 Ag1 14(2) . . . . ?
C16 Ag3A Ag2 Ag1 -52.5(5) . . . . ?
O8 Ag3A Ag2 Ag1 148.1(10) . . . . ?
Ag4 Ag3A Ag2 Ag1 -65.8(4) 3 . . . ?
Ag3A Ag3 Ag2 C16 -106(2) . . . . ?
O7 Ag3 Ag2 C16 163.9(6) . . . . ?
Ag1 Ag3 Ag2 C16 58.8(4) . . . . ?
Ag4 Ag3 Ag2 C16 -17.5(4) 3 . . . ?
Ag3A Ag3 Ag2 O4 102(2) . . . . ?
C16 Ag3 Ag2 O4 -152.2(6) . . . . ?
O7 Ag3 Ag2 O4 11.6(6) . . . . ?
Ag1 Ag3 Ag2 O4 -93.4(4) . . . . ?
Ag4 Ag3 Ag2 O4 -169.7(4) 3 . . . ?
Ag3A Ag3 Ag2 O3 5(2) . . . 1_455 ?
C16 Ag3 Ag2 O3 111.5(7) . . . 1_455 ?
O7 Ag3 Ag2 O3 -84.7(7) . . . 1_455 ?
Ag1 Ag3 Ag2 O3 170.3(6) . . . 1_455 ?
Ag4 Ag3 Ag2 O3 94.0(6) 3 . . 1_455 ?
C16 Ag3 Ag2 Ag3A 106(2) . . . . ?
O7 Ag3 Ag2 Ag3A -90(2) . . . . ?
Ag1 Ag3 Ag2 Ag3A 165(2) . . . . ?
Ag4 Ag3 Ag2 Ag3A 89(2) 3 . . . ?
Ag3A Ag3 Ag2 Ag1 -165(2) . . . . ?
C16 Ag3 Ag2 Ag1 -58.8(4) . . . . ?
O7 Ag3 Ag2 Ag1 105.0(4) . . . . ?
Ag4 Ag3 Ag2 Ag1 -76.29(7) 3 . . . ?
Ag3A Ag3 Ag1 C16 -46(3) . . . . ?
O7 Ag3 Ag1 C16 169.3(5) . . . . ?
Ag2 Ag3 Ag1 C16 -61.3(4) . . . . ?
Ag4 Ag3 Ag1 C16 46.6(4) 3 . . . ?
Ag3A Ag3 Ag1 O6 113(3) . . . 3_545 ?
C16 Ag3 Ag1 O6 158.3(6) . . . 3_545 ?
O7 Ag3 Ag1 O6 -32.4(5) . . . 3_545 ?
Ag2 Ag3 Ag1 O6 97.0(3) . . . 3_545 ?
Ag4 Ag3 Ag1 O6 -155.1(3) 3 . . 3_545 ?
Ag3A Ag3 Ag1 O3 -157(3) . . . . ?
C16 Ag3 Ag1 O3 -110.8(6) . . . . ?
O7 Ag3 Ag1 O3 58.5(5) . . . . ?
Ag2 Ag3 Ag1 O3 -172.1(4) . . . . ?
Ag4 Ag3 Ag1 O3 -64.2(4) 3 . . . ?
Ag3A Ag3 Ag1 Ag2 16(3) . . . . ?
C16 Ag3 Ag1 Ag2 61.3(4) . . . . ?
O7 Ag3 Ag1 Ag2 -129.4(3) . . . . ?
Ag4 Ag3 Ag1 Ag2 107.89(6) 3 . . . ?
C16 Ag3 Ag1 Ag3A 46(3) . . . . ?
O7 Ag3 Ag1 Ag3A -145(3) . . . . ?
Ag2 Ag3 Ag1 Ag3A -16(3) . . . . ?
Ag4 Ag3 Ag1 Ag3A 92(3) 3 . . . ?
O4 Ag2 Ag1 C16 152.9(5) . . . . ?
O3 Ag2 Ag1 C16 -110.2(7) 1_455 . . . ?
Ag3A Ag2 Ag1 C16 57.9(5) . . . . ?
Ag3 Ag2 Ag1 C16 60.6(4) . . . . ?
C16 Ag2 Ag1 O6 -149.8(5) . . . 3_545 ?
O4 Ag2 Ag1 O6 3.1(4) . . . 3_545 ?
O3 Ag2 Ag1 O6 100.1(6) 1_455 . . 3_545 ?
Ag3A Ag2 Ag1 O6 -91.9(4) . . . 3_545 ?
Ag3 Ag2 Ag1 O6 -89.2(3) . . . 3_545 ?
C16 Ag2 Ag1 O3 91.9(14) . . . . ?
O4 Ag2 Ag1 O3 -115.3(14) . . . . ?
O3 Ag2 Ag1 O3 -18.3(9) 1_455 . . . ?
Ag3A Ag2 Ag1 O3 149.8(14) . . . . ?
Ag3 Ag2 Ag1 O3 152.5(14) . . . . ?
C16 Ag2 Ag1 Ag3 -60.6(4) . . . . ?
O4 Ag2 Ag1 Ag3 92.3(3) . . . . ?
O3 Ag2 Ag1 Ag3 -170.8(6) 1_455 . . . ?
Ag3A Ag2 Ag1 Ag3 -2.7(4) . . . . ?
C16 Ag2 Ag1 Ag3A -57.9(5) . . . . ?
O4 Ag2 Ag1 Ag3A 95.0(5) . . . . ?
O3 Ag2 Ag1 Ag3A -168.1(7) 1_455 . . . ?
Ag3 Ag2 Ag1 Ag3A 2.7(4) . . . . ?
Ag3 Ag3A Ag1 C16 129(3) . . . . ?
O8 Ag3A Ag1 C16 171(2) . . . . ?
Ag2 Ag3A Ag1 C16 -68.4(6) . . . . ?
Ag4 Ag3A Ag1 C16 47.8(5) 3 . . . ?
Ag3 Ag3A Ag1 O6 -68(3) . . . 3_545 ?
C16 Ag3A Ag1 O6 163.3(7) . . . 3_545 ?
O8 Ag3A Ag1 O6 -25.8(16) . . . 3_545 ?
Ag2 Ag3A Ag1 O6 94.9(4) . . . 3_545 ?
Ag4 Ag3A Ag1 O6 -148.9(4) 3 . . 3_545 ?
Ag3 Ag3A Ag1 O3 27(3) . . . . ?
C16 Ag3A Ag1 O3 -101.8(8) . . . . ?
O8 Ag3A Ag1 O3 69.1(18) . . . . ?
Ag2 Ag3A Ag1 O3 -170.2(5) . . . . ?
Ag4 Ag3A Ag1 O3 -54.0(7) 3 . . . ?
C16 Ag3A Ag1 Ag3 -129(3) . . . . ?
O8 Ag3A Ag1 Ag3 42.2(17) . . . . ?
Ag2 Ag3A Ag1 Ag3 163(3) . . . . ?
Ag4 Ag3A Ag1 Ag3 -81(3) 3 . . . ?
Ag3 Ag3A Ag1 Ag2 -163(3) . . . . ?
C16 Ag3A Ag1 Ag2 68.4(6) . . . . ?
O8 Ag3A Ag1 Ag2 -120.7(17) . . . . ?
Ag4 Ag3A Ag1 Ag2 116.2(4) 3 . . . ?
C1 Ag7 Ag5 Ag5A -71.4(11) . . . . ?
O15 Ag7 Ag5 Ag5A 86.8(11) 3_565 . . . ?
O16 Ag7 Ag5 Ag5A 176.1(11) 1_655 . . . ?
Ag6 Ag7 Ag5 Ag5A -14.6(10) . . . . ?
O15 Ag7 Ag5 C1 158.2(6) 3_565 . . . ?
O16 Ag7 Ag5 C1 -112.5(5) 1_655 . . . ?
Ag6 Ag7 Ag5 C1 56.7(3) . . . . ?
Ag5A Ag7 Ag5 C1 71.4(11) . . . . ?
C1 Ag7 Ag5 O12 122.9(4) . . . 3_565 ?
O15 Ag7 Ag5 O12 -78.8(5) 3_565 . . 3_565 ?
O16 Ag7 Ag5 O12 10.4(4) 1_655 . . 3_565 ?
Ag6 Ag7 Ag5 O12 179.7(3) . . . 3_565 ?
Ag5A Ag7 Ag5 O12 -165.7(11) . . . 3_565 ?
C1 Ag7 Ag5 O12 -119.0(5) . . . . ?
O15 Ag7 Ag5 O12 39.3(6) 3_565 . . . ?
O16 Ag7 Ag5 O12 128.5(5) 1_655 . . . ?
Ag6 Ag7 Ag5 O12 -62.2(4) . . . . ?
Ag5A Ag7 Ag5 O12 -47.6(10) . . . . ?
C1 Ag7 Ag5 Ag6 -56.7(3) . . . . ?
O15 Ag7 Ag5 Ag6 101.5(4) 3_565 . . . ?
O16 Ag7 Ag5 Ag6 -169.3(3) 1_655 . . . ?
Ag5A Ag7 Ag5 Ag6 14.6(10) . . . . ?
C1 Ag7 Ag5 Ag4 1.1(3) . . . . ?
O15 Ag7 Ag5 Ag4 159.4(4) 3_565 . . . ?
O16 Ag7 Ag5 Ag4 -111.4(3) 1_655 . . . ?
Ag6 Ag7 Ag5 Ag4 57.87(6) . . . . ?
Ag5A Ag7 Ag5 Ag4 72.5(10) . . . . ?
C1 Ag4 Ag5 Ag5A 94.5(11) . . . . ?
C16 Ag4 Ag5 Ag5A -96.1(12) 3_455 . . . ?
O11 Ag4 Ag5 Ag5A -20.8(11) 3_465 . . . ?
C2 Ag4 Ag5 Ag5A 110.0(11) . . . . ?
C15 Ag4 Ag5 Ag5A -110(3) 3_455 . . . ?
Ag3 Ag4 Ag5 Ag5A -80.3(11) 3_455 . . . ?
Ag3A Ag4 Ag5 Ag5A -71.3(11) 3_455 . . . ?
C16 Ag4 Ag5 C1 169.4(6) 3_455 . . . ?
O11 Ag4 Ag5 C1 -115.3(4) 3_465 . . . ?
C2 Ag4 Ag5 C1 15.5(5) . . . . ?
C15 Ag4 Ag5 C1 155(3) 3_455 . . . ?
Ag5A Ag4 Ag5 C1 -94.5(11) . . . . ?
Ag3 Ag4 Ag5 C1 -174.8(3) 3_455 . . . ?
Ag3A Ag4 Ag5 C1 -165.7(5) 3_455 . . . ?
C1 Ag4 Ag5 O12 -91.4(5) . . . 3_565 ?
C16 Ag4 Ag5 O12 78.0(7) 3_455 . . 3_565 ?
O11 Ag4 Ag5 O12 153.3(5) 3_465 . . 3_565 ?
C2 Ag4 Ag5 O12 -75.9(5) . . . 3_565 ?
C15 Ag4 Ag5 O12 64(3) 3_455 . . 3_565 ?
Ag5A Ag4 Ag5 O12 174.1(12) . . . 3_565 ?
Ag3 Ag4 Ag5 O12 93.8(4) 3_455 . . 3_565 ?
Ag3A Ag4 Ag5 O12 102.8(5) 3_455 . . 3_565 ?
C1 Ag4 Ag5 O12 143.0(5) . . . . ?
C16 Ag4 Ag5 O12 -47.7(6) 3_455 . . . ?
O11 Ag4 Ag5 O12 27.7(4) 3_465 . . . ?
C2 Ag4 Ag5 O12 158.5(4) . . . . ?
C15 Ag4 Ag5 O12 -62(3) 3_455 . . . ?
Ag5A Ag4 Ag5 O12 48.5(11) . . . . ?
Ag3 Ag4 Ag5 O12 -31.8(3) 3_455 . . . ?
Ag3A Ag4 Ag5 O12 -22.8(4) 3_455 . . . ?
C1 Ag4 Ag5 Ag7 -1.1(3) . . . . ?
C16 Ag4 Ag5 Ag7 168.2(5) 3_455 . . . ?
O11 Ag4 Ag5 Ag7 -116.4(3) 3_465 . . . ?
C2 Ag4 Ag5 Ag7 14.4(3) . . . . ?
C15 Ag4 Ag5 Ag7 154(3) 3_455 . . . ?
Ag5A Ag4 Ag5 Ag7 -95.6(11) . . . . ?
Ag3 Ag4 Ag5 Ag7 -175.91(7) 3_455 . . . ?
Ag3A Ag4 Ag5 Ag7 -166.9(3) 3_455 . . . ?
C1 Ag4 Ag5 Ag6 49.4(3) . . . . ?
C16 Ag4 Ag5 Ag6 -141.2(5) 3_455 . . . ?
O11 Ag4 Ag5 Ag6 -65.8(3) 3_465 . . . ?
C2 Ag4 Ag5 Ag6 65.0(3) . . . . ?
C15 Ag4 Ag5 Ag6 -155(3) 3_455 . . . ?
Ag5A Ag4 Ag5 Ag6 -45.0(11) . . . . ?
Ag3 Ag4 Ag5 Ag6 -125.34(6) 3_455 . . . ?
Ag3A Ag4 Ag5 Ag6 -116.3(3) 3_455 . . . ?
O15 Ag7 Ag6 C1 -150.9(5) 3_565 . . . ?
O16 Ag7 Ag6 C1 20(2) 1_655 . . . ?
Ag5 Ag7 Ag6 C1 -61.2(4) . . . . ?
Ag5A Ag7 Ag6 C1 -64.8(4) . . . . ?
C1 Ag7 Ag6 O16 -113.5(8) . . . . ?
O15 Ag7 Ag6 O16 95.5(7) 3_565 . . . ?
O16 Ag7 Ag6 O16 -94(2) 1_655 . . . ?
Ag5 Ag7 Ag6 O16 -174.7(7) . . . . ?
Ag5A Ag7 Ag6 O16 -178.3(7) . . . . ?
C1 Ag7 Ag6 O13 166.3(5) . . . . ?
O15 Ag7 Ag6 O13 15.4(4) 3_565 . . . ?
O16 Ag7 Ag6 O13 -174(2) 1_655 . . . ?
Ag5 Ag7 Ag6 O13 105.1(2) . . . . ?
Ag5A Ag7 Ag6 O13 101.5(3) . . . . ?
C1 Ag7 Ag6 Ag5A 64.8(4) . . . . ?
O15 Ag7 Ag6 Ag5A -86.1(4) 3_565 . . . ?
O16 Ag7 Ag6 Ag5A 84(2) 1_655 . . . ?
Ag5 Ag7 Ag6 Ag5A 3.6(3) . . . . ?
C1 Ag7 Ag6 Ag5 61.2(4) . . . . ?
O15 Ag7 Ag6 Ag5 -89.7(3) 3_565 . . . ?
O16 Ag7 Ag6 Ag5 81(2) 1_655 . . . ?
Ag5A Ag7 Ag6 Ag5 -3.6(2) . . . . ?
Ag5A Ag5 Ag6 C1 -137.2(16) . . . . ?
O12 Ag5 Ag6 C1 63.9(6) 3_565 . . . ?
O12 Ag5 Ag6 C1 -152.3(6) . . . . ?
Ag7 Ag5 Ag6 C1 64.4(4) . . . . ?
Ag4 Ag5 Ag6 C1 -55.7(4) . . . . ?
Ag5A Ag5 Ag6 O16 -26.5(17) . . . . ?
C1 Ag5 Ag6 O16 110.7(8) . . . . ?
O12 Ag5 Ag6 O16 174.6(7) 3_565 . . . ?
O12 Ag5 Ag6 O16 -41.5(7) . . . . ?
Ag7 Ag5 Ag6 O16 175.1(6) . . . . ?
Ag4 Ag5 Ag6 O16 55.0(6) . . . . ?
Ag5A Ag5 Ag6 O13 77.9(16) . . . . ?
C1 Ag5 Ag6 O13 -144.8(5) . . . . ?
O12 Ag5 Ag6 O13 -80.9(5) 3_565 . . . ?
O12 Ag5 Ag6 O13 62.9(4) . . . . ?
Ag7 Ag5 Ag6 O13 -80.4(3) . . . . ?
Ag4 Ag5 Ag6 O13 159.5(3) . . . . ?
C1 Ag5 Ag6 Ag5A 137.2(16) . . . . ?
O12 Ag5 Ag6 Ag5A -158.9(17) 3_565 . . . ?
O12 Ag5 Ag6 Ag5A -15.0(15) . . . . ?
Ag7 Ag5 Ag6 Ag5A -158.4(16) . . . . ?
Ag4 Ag5 Ag6 Ag5A 81.5(15) . . . . ?
Ag5A Ag5 Ag6 Ag7 158.4(16) . . . . ?
C1 Ag5 Ag6 Ag7 -64.4(4) . . . . ?
O12 Ag5 Ag6 Ag7 -0.5(4) 3_565 . . . ?
O12 Ag5 Ag6 Ag7 143.3(3) . . . . ?
Ag4 Ag5 Ag6 Ag7 -120.11(6) . . . . ?
Ag3A Ag3 O7 N5 10(3) . . . . ?
C16 Ag3 O7 N5 -165.8(17) . . . . ?
Ag1 Ag3 O7 N5 158.3(7) . . . . ?
Ag2 Ag3 O7 N5 78.9(10) . . . . ?
Ag4 Ag3 O7 N5 -99.6(8) 3 . . . ?
Ag3 Ag3A O8 N5 21(3) . . . . ?
C16 Ag3A O8 N5 146(3) . . . . ?
Ag2 Ag3A O8 N5 -113.7(10) . . . . ?
Ag4 Ag3A O8 N5 102.8(9) 3 . . . ?
Ag1 Ag3A O8 N5 -11.6(18) . . . . ?
Ag5A Ag5 O12 N6 -174.6(17) . . . . ?
C1 Ag5 O12 N6 168.7(8) . . . . ?
O12 Ag5 O12 N6 -5.6(14) 3_565 . . . ?
Ag7 Ag5 O12 N6 -112.1(9) . . . . ?
Ag6 Ag5 O12 N6 -162.3(9) . . . . ?
Ag4 Ag5 O12 N6 125.7(9) . . . . ?
C1 Ag5 O12 Ag5A -16.7(14) . . . . ?
O12 Ag5 O12 Ag5A 169.0(14) 3_565 . . . ?
Ag7 Ag5 O12 Ag5A 62.6(14) . . . . ?
Ag6 Ag5 O12 Ag5A 12.3(13) . . . . ?
Ag4 Ag5 O12 Ag5A -59.6(13) . . . . ?
Ag5A Ag5 O12 Ag5 6.5(15) . . . 3_465 ?
C1 Ag5 O12 Ag5 -10.2(12) . . . 3_465 ?
O12 Ag5 O12 Ag5 175.5(3) 3_565 . . 3_465 ?
Ag7 Ag5 O12 Ag5 69.1(9) . . . 3_465 ?
Ag6 Ag5 O12 Ag5 18.8(8) . . . 3_465 ?
Ag4 Ag5 O12 Ag5 -53.1(8) . . . 3_465 ?
Ag8 C9A N2 C14 -178(13) . . . . ?
C8A C9A N2 C14 180(3) . . . . ?
Ag8 C9A N2 C11 1(14) . . . . ?
C8A C9A N2 C11 -1(4) . . . . ?
C8A C9A N2 Ag8 -2(11) . . . . ?
C13 C14 N2 C9A -178.9(17) . . . . ?
C13 C14 N2 C11 2.0(18) . . . . ?
C13 C14 N2 Ag8 -179.0(8) . . . . ?
C10 C11 N2 C9A -178.8(16) . . . . ?
C6 C11 N2 C9A 3(2) . . . . ?
C10 C11 N2 C14 0.4(16) . . . . ?
C6 C11 N2 C14 -177.4(10) . . . . ?
C10 C11 N2 Ag8 -178.7(8) . . . . ?
C6 C11 N2 Ag8 3.5(11) . . . . ?
C6 N1 C7 C3 1.7(17) . . . . ?
C8A N1 C7 C3 -175(2) . . . . ?
Ag8 N1 C7 C3 -176.2(9) . . . . ?
C4 C3 C7 N1 -2.1(18) . . . . ?
C2 C3 C7 N1 178.1(11) . . . . ?
C1 Ag6 O13 N7 -101.2(10) . . . . ?
O16 Ag6 O13 N7 90.0(9) . . . . ?
Ag5A Ag6 O13 N7 -52.1(9) . . . . ?
Ag7 Ag6 O13 N7 -117.1(8) . . . . ?
Ag5 Ag6 O13 N7 -60.9(9) . . . . ?
C1 Ag6 O13 Ag8 46.1(9) . . . 2_764 ?
O16 Ag6 O13 Ag8 -122.6(7) . . . 2_764 ?
Ag5A Ag6 O13 Ag8 95.2(6) . . . 2_764 ?
Ag7 Ag6 O13 Ag8 30.2(6) . . . 2_764 ?
Ag5 Ag6 O13 Ag8 86.4(6) . . . 2_764 ?
C7 N1 C6 C5 -1.1(15) . . . . ?
C8A N1 C6 C5 176.1(19) . . . . ?
Ag8 N1 C6 C5 176.9(7) . . . . ?
C7 N1 C6 C11 -178.9(10) . . . . ?
C8A N1 C6 C11 -2(2) . . . . ?
Ag8 N1 C6 C11 -0.8(11) . . . . ?
N2 C11 C6 N1 -2.0(13) . . . . ?
C10 C11 C6 N1 -179.8(10) . . . . ?
N2 C11 C6 C5 -179.7(9) . . . . ?
C10 C11 C6 C5 2.4(13) . . . . ?
C1 Ag6 O16 N8 -41.1(16) . . . . ?
O13 Ag6 O16 N8 128.3(12) . . . . ?
Ag5A Ag6 O16 N8 -129.8(11) . . . . ?
Ag7 Ag6 O16 N8 47.7(16) . . . . ?
Ag5 Ag6 O16 N8 -123.4(11) . . . . ?
C1 Ag6 O16 Ag7 112.0(13) . . . 1_455 ?
O13 Ag6 O16 Ag7 -78.6(14) . . . 1_455 ?
Ag5A Ag6 O16 Ag7 23.4(18) . . . 1_455 ?
Ag7 Ag6 O16 Ag7 -159.1(9) . . . 1_455 ?
Ag5 Ag6 O16 Ag7 29.7(19) . . . 1_455 ?
O16 Ag6 C1 C2 20.8(16) . . . . ?
O13 Ag6 C1 C2 -143.3(11) . . . . ?
Ag5A Ag6 C1 C2 152.5(15) . . . . ?
Ag7 Ag6 C1 C2 -122.8(14) . . . . ?
Ag5 Ag6 C1 C2 159.8(15) . . . . ?
O16 Ag6 C1 Ag5A -131.7(6) . . . . ?
O13 Ag6 C1 Ag5A 64.1(7) . . . . ?
Ag7 Ag6 C1 Ag5A 84.7(4) . . . . ?
Ag5 Ag6 C1 Ag5A 7.3(3) . . . . ?
O16 Ag6 C1 Ag5 -139.0(6) . . . . ?
O13 Ag6 C1 Ag5 56.9(7) . . . . ?
Ag5A Ag6 C1 Ag5 -7.3(3) . . . . ?
Ag7 Ag6 C1 Ag5 77.5(3) . . . . ?
O16 Ag6 C1 Ag7 143.6(6) . . . . ?
O13 Ag6 C1 Ag7 -20.6(7) . . . . ?
Ag5A Ag6 C1 Ag7 -84.7(4) . . . . ?
Ag5 Ag6 C1 Ag7 -77.5(3) . . . . ?
O16 Ag6 C1 Ag4 -59.9(8) . . . . ?
O13 Ag6 C1 Ag4 136.0(4) . . . . ?
Ag5A Ag6 C1 Ag4 71.8(4) . . . . ?
Ag7 Ag6 C1 Ag4 156.6(5) . . . . ?
Ag5 Ag6 C1 Ag4 79.1(4) . . . . ?
Ag5A Ag5 C1 C2 -127.2(19) . . . . ?
O12 Ag5 C1 C2 61.0(16) 3_565 . . . ?
O12 Ag5 C1 C2 -113.5(15) . . . . ?
Ag7 Ag5 C1 C2 123.4(16) . . . . ?
Ag6 Ag5 C1 C2 -154.8(17) . . . . ?
Ag4 Ag5 C1 C2 -55.3(14) . . . . ?
Ag5A Ag5 C1 Ag6 27.6(12) . . . . ?
O12 Ag5 C1 Ag6 -144.2(4) 3_565 . . . ?
O12 Ag5 C1 Ag6 41.3(8) . . . . ?
Ag7 Ag5 C1 Ag6 -81.8(4) . . . . ?
Ag4 Ag5 C1 Ag6 99.6(4) . . . . ?
O12 Ag5 C1 Ag5A -171.8(12) 3_565 . . . ?
O12 Ag5 C1 Ag5A 13.7(12) . . . . ?
Ag7 Ag5 C1 Ag5A -109.4(12) . . . . ?
Ag6 Ag5 C1 Ag5A -27.6(12) . . . . ?
Ag4 Ag5 C1 Ag5A 72.0(11) . . . . ?
Ag5A Ag5 C1 Ag7 109.4(12) . . . . ?
O12 Ag5 C1 Ag7 -62.4(5) 3_565 . . . ?
O12 Ag5 C1 Ag7 123.1(6) . . . . ?
Ag6 Ag5 C1 Ag7 81.8(4) . . . . ?
Ag4 Ag5 C1 Ag7 -178.6(4) . . . . ?
Ag5A Ag5 C1 Ag4 -72.0(11) . . . . ?
O12 Ag5 C1 Ag4 116.2(4) 3_565 . . . ?
O12 Ag5 C1 Ag4 -58.2(7) . . . . ?
Ag7 Ag5 C1 Ag4 178.6(4) . . . . ?
Ag6 Ag5 C1 Ag4 -99.6(4) . . . . ?
O15 Ag7 C1 C2 -179.1(10) 3_565 . . . ?
O16 Ag7 C1 C2 -44.7(12) 1_655 . . . ?
Ag5 Ag7 C1 C2 -142.7(12) . . . . ?
Ag6 Ag7 C1 C2 131.4(12) . . . . ?
Ag5A Ag7 C1 C2 -156.9(13) . . . . ?
O15 Ag7 C1 Ag6 49.6(8) 3_565 . . . ?
O16 Ag7 C1 Ag6 -176.1(4) 1_655 . . . ?
Ag5 Ag7 C1 Ag6 85.9(3) . . . . ?
Ag5A Ag7 C1 Ag6 71.7(4) . . . . ?
O15 Ag7 C1 Ag5A -22.1(9) 3_565 . . . ?
O16 Ag7 C1 Ag5A 112.2(5) 1_655 . . . ?
Ag5 Ag7 C1 Ag5A 14.2(2) . . . . ?
Ag6 Ag7 C1 Ag5A -71.7(4) . . . . ?
O15 Ag7 C1 Ag5 -36.4(8) 3_565 . . . ?
O16 Ag7 C1 Ag5 98.0(5) 1_655 . . . ?
Ag6 Ag7 C1 Ag5 -85.9(3) . . . . ?
Ag5A Ag7 C1 Ag5 -14.2(2) . . . . ?
O15 Ag7 C1 Ag4 -39.8(17) 3_565 . . . ?
O16 Ag7 C1 Ag4 94.5(13) 1_655 . . . ?
Ag5 Ag7 C1 Ag4 -3.5(11) . . . . ?
Ag6 Ag7 C1 Ag4 -89.4(13) . . . . ?
Ag5A Ag7 C1 Ag4 -17.7(11) . . . . ?
C16 Ag4 C1 C2 -4(2) 3_455 . . . ?
O11 Ag4 C1 C2 -152.6(8) 3_465 . . . ?
C15 Ag4 C1 C2 -27.4(11) 3_455 . . . ?
Ag5A Ag4 C1 C2 163.1(9) . . . . ?
Ag3 Ag4 C1 C2 157.7(6) 3_455 . . . ?
Ag5 Ag4 C1 C2 148.4(9) . . . . ?
Ag3A Ag4 C1 C2 175.2(9) 3_455 . . . ?
C16 Ag4 C1 Ag6 124.8(15) 3_455 . . . ?
O11 Ag4 C1 Ag6 -23.3(4) 3_465 . . . ?
C2 Ag4 C1 Ag6 129.3(9) . . . . ?
C15 Ag4 C1 Ag6 101.8(6) 3_455 . . . ?
Ag5A Ag4 C1 Ag6 -67.7(4) . . . . ?
Ag3 Ag4 C1 Ag6 -73.1(6) 3_455 . . . ?
Ag5 Ag4 C1 Ag6 -82.3(4) . . . . ?
Ag3A Ag4 C1 Ag6 -55.6(9) 3_455 . . . ?
C16 Ag4 C1 Ag5A -167.5(15) 3_455 . . . ?
O11 Ag4 C1 Ag5A 44.3(4) 3_465 . . . ?
C2 Ag4 C1 Ag5A -163.1(9) . . . . ?
C15 Ag4 C1 Ag5A 169.5(6) 3_455 . . . ?
Ag3 Ag4 C1 Ag5A -5.4(7) 3_455 . . . ?
Ag5 Ag4 C1 Ag5A -14.6(2) . . . . ?
Ag3A Ag4 C1 Ag5A 12.1(9) 3_455 . . . ?
C16 Ag4 C1 Ag5 -152.8(15) 3_455 . . . ?
O11 Ag4 C1 Ag5 59.0(3) 3_465 . . . ?
C2 Ag4 C1 Ag5 -148.4(9) . . . . ?
C15 Ag4 C1 Ag5 -175.8(5) 3_455 . . . ?
Ag5A Ag4 C1 Ag5 14.6(2) . . . . ?
Ag3 Ag4 C1 Ag5 9.3(6) 3_455 . . . ?
Ag3A Ag4 C1 Ag5 26.8(9) 3_455 . . . ?
C16 Ag4 C1 Ag7 -149.4(14) 3_455 . . . ?
O11 Ag4 C1 Ag7 62.4(13) 3_465 . . . ?
C2 Ag4 C1 Ag7 -145.0(18) . . . . ?
C15 Ag4 C1 Ag7 -172.4(11) 3_455 . . . ?
Ag5A Ag4 C1 Ag7 18.1(11) . . . . ?
Ag3 Ag4 C1 Ag7 12.7(17) 3_455 . . . ?
Ag5 Ag4 C1 Ag7 3.4(10) . . . . ?
Ag3A Ag4 C1 Ag7 30.2(18) 3_455 . . . ?
Ag5A O12 N6 O10 174.4(14) . . . . ?
Ag5 O12 N6 O10 -5(2) 3_465 . . . ?
Ag5 O12 N6 O10 175.7(13) . . . . ?
Ag5A O12 N6 O11 -4.6(16) . . . . ?
Ag5 O12 N6 O11 175.6(9) 3_465 . . . ?
Ag5 O12 N6 O11 -3.3(14) . . . . ?
Ag4 O11 N6 O10 4.6(17) 3_565 . . . ?
Ag4 O11 N6 O12 -176.4(10) 3_565 . . . ?
Ag6 O16 N8 O18 171.8(13) . . . . ?
Ag7 O16 N8 O18 4.5(19) 1_455 . . . ?
Ag6 O16 N8 O17 -9(2) . . . . ?
Ag7 O16 N8 O17 -175.9(16) 1_455 . . . ?
Ag6 C1 C2 C3 75(11) . . . . ?
Ag5A C1 C2 C3 -161(10) . . . . ?
Ag5 C1 C2 C3 -138(11) . . . . ?
Ag7 C1 C2 C3 -30(12) . . . . ?
Ag4 C1 C2 C3 166(11) . . . . ?
Ag6 C1 C2 Ag4 -90.5(11) . . . . ?
Ag5A C1 C2 Ag4 32.8(17) . . . . ?
Ag5 C1 C2 Ag4 56.0(13) . . . . ?
Ag7 C1 C2 Ag4 164.7(8) . . . . ?
C7 C3 C2 C1 145(11) . . . . ?
C4 C3 C2 C1 -35(12) . . . . ?
C7 C3 C2 Ag4 -50.1(14) . . . . ?
C4 C3 C2 Ag4 130.1(9) . . . . ?
C16 Ag4 C2 C1 178.5(7) 3_455 . . . ?
O11 Ag4 C2 C1 32.0(9) 3_465 . . . ?
C15 Ag4 C2 C1 160.9(8) 3_455 . . . ?
Ag5A Ag4 C2 C1 -13.0(7) . . . . ?
Ag3 Ag4 C2 C1 -78.6(16) 3_455 . . . ?
Ag5 Ag4 C2 C1 -23.7(7) . . . . ?
Ag3A Ag4 C2 C1 -43(7) 3_455 . . . ?
C1 Ag4 C2 C3 -178.3(14) . . . . ?
C16 Ag4 C2 C3 0.2(12) 3_455 . . . ?
O11 Ag4 C2 C3 -146.3(8) 3_465 . . . ?
C15 Ag4 C2 C3 -17.4(10) 3_455 . . . ?
Ag5A Ag4 C2 C3 168.7(9) . . . . ?
Ag3 Ag4 C2 C3 103.1(13) 3_455 . . . ?
Ag5 Ag4 C2 C3 158.0(9) . . . . ?
Ag3A Ag4 C2 C3 139(6) 3_455 . . . ?
C10 C12 C13 C14 2.5(18) . . . . ?
C10 C12 C13 C15 -175.9(11) . . . . ?
N2 C14 C13 C12 -3.4(18) . . . . ?
N2 C14 C13 C15 175.0(12) . . . . ?
N1 C6 C5 C4 0.9(14) . . . . ?
C11 C6 C5 C4 178.7(8) . . . . ?
N1 C6 C5 C8 -179.1(11) . . . . ?
C11 C6 C5 C8 -1.3(14) . . . . ?
N1 C6 C5 Ag8A 177.8(7) . . . . ?
C11 C6 C5 Ag8A -4.5(11) . . . . ?
O1 N3 O3 Ag1 -156.6(18) . . . . ?
O2 N3 O3 Ag1 26.3(17) . . . . ?
O1 N3 O3 Ag2 -10(2) . . . 1_655 ?
O2 N3 O3 Ag2 173.1(12) . . . 1_655 ?
C16 Ag1 O3 N3 42.3(12) . . . . ?
O6 Ag1 O3 N3 -158.1(10) 3_545 . . . ?
Ag3 Ag1 O3 N3 109.0(10) . . . . ?
Ag2 Ag1 O3 N3 -39(2) . . . . ?
Ag3A Ag1 O3 N3 104.2(11) . . . . ?
C16 Ag1 O3 Ag2 -85.3(9) . . . 1_655 ?
O6 Ag1 O3 Ag2 74.3(8) 3_545 . . 1_655 ?
Ag3 Ag1 O3 Ag2 -18.7(10) . . . 1_655 ?
Ag2 Ag1 O3 Ag2 -166.4(7) . . . 1_655 ?
Ag3A Ag1 O3 Ag2 -23.5(12) . . . 1_655 ?
Ag3 O7 N5 O9 -165.9(11) . . . . ?
Ag3 O7 N5 O8 9.7(13) . . . . ?
Ag3A O8 N5 O9 164.1(11) . . . . ?
Ag3A O8 N5 O7 -11.7(12) . . . . ?
C8 C5 C4 C3 178.7(13) . . . . ?
C6 C5 C4 C3 -1.3(15) . . . . ?
Ag8A C5 C4 C3 -177.7(8) . . . . ?
C7 C3 C4 C5 1.9(16) . . . . ?
C2 C3 C4 C5 -178.3(10) . . . . ?
O5 N4 O6 Ag1 -21.5(17) . . . 3_445 ?
O4 N4 O6 Ag1 160.5(13) . . . 3_445 ?
O5 N4 O6 Ag8A -158.2(12) . . . 4_645 ?
O4 N4 O6 Ag8A 24(2) . . . 4_645 ?
O5 N4 O4 Ag2 15(2) . . . . ?
O6 N4 O4 Ag2 -166.7(12) . . . . ?
C16 Ag2 O4 N4 -59.2(15) . . . . ?
O3 Ag2 O4 N4 122.2(13) 1_455 . . . ?
Ag3A Ag2 O4 N4 -19.7(14) . . . . ?
Ag3 Ag2 O4 N4 -29.2(13) . . . . ?
Ag1 Ag2 O4 N4 -87.9(13) . . . . ?
C4 C5 C8 Ag8A 129(12) . . . . ?
C6 C5 C8 Ag8A -51(13) . . . . ?
C4 C5 C8 C9 179.8(14) . . . . ?
C6 C5 C8 C9 0(2) . . . . ?
Ag8A C5 C8 C9 51(12) . . . . ?
N2 C11 C10 C9 -179.8(12) . . . . ?
C6 C11 C10 C9 -2.0(16) . . . . ?
N2 C11 C10 C12 -1.2(15) . . . . ?
C6 C11 C10 C12 176.5(9) . . . . ?
N2 C11 C10 Ag8A -176.7(8) . . . . ?
C6 C11 C10 Ag8A 1.1(12) . . . . ?
C13 C12 C10 C9 178.2(13) . . . . ?
C13 C12 C10 C11 -0.3(16) . . . . ?
C13 C12 C10 Ag8A 174.7(9) . . . . ?
C5 C8 C9 Ag8A -171(2) . . . . ?
Ag8A C8 C9 C10 172(2) . . . . ?
C5 C8 C9 C10 1(3) . . . . ?
C11 C10 C9 Ag8A 40(11) . . . . ?
C12 C10 C9 Ag8A -139(10) . . . . ?
C11 C10 C9 C8 1(2) . . . . ?
C12 C10 C9 C8 -177.8(14) . . . . ?
Ag8A C10 C9 C8 -39(10) . . . . ?
C12 C13 C15 C16 -141(14) . . . . ?
C14 C13 C15 C16 40(15) . . . . ?
C12 C13 C15 Ag4 45.9(14) . . . 3 ?
C14 C13 C15 Ag4 -132.4(11) . . . 3 ?
C13 C15 C16 Ag3 148(13) . . . . ?
Ag4 C15 C16 Ag3 -38.8(19) 3 . . . ?
C13 C15 C16 Ag3A 128(14) . . . . ?
Ag4 C15 C16 Ag3A -58.4(17) 3 . . . ?
C13 C15 C16 Ag1 -62(15) . . . . ?
Ag4 C15 C16 Ag1 111.1(10) 3 . . . ?
C13 C15 C16 Ag2 36(15) . . . . ?
Ag4 C15 C16 Ag2 -151.0(8) 3 . . . ?
C13 C15 C16 Ag4 -173(14) . . . 3 ?
Ag3A Ag3 C16 C15 -62(3) . . . . ?
O7 Ag3 C16 C15 113(3) . . . . ?
Ag1 Ag3 C16 C15 156(2) . . . . ?
Ag2 Ag3 C16 C15 -120(2) . . . . ?
Ag4 Ag3 C16 C15 39(2) 3 . . . ?
O7 Ag3 C16 Ag3A 176(4) . . . . ?
Ag1 Ag3 C16 Ag3A -142(2) . . . . ?
Ag2 Ag3 C16 Ag3A -58(2) . . . . ?
Ag4 Ag3 C16 Ag3A 101(2) 3 . . . ?
Ag3A Ag3 C16 Ag1 142(2) . . . . ?
O7 Ag3 C16 Ag1 -42(2) . . . . ?
Ag2 Ag3 C16 Ag1 84.2(4) . . . . ?
Ag4 Ag3 C16 Ag1 -117.0(5) 3 . . . ?
Ag3A Ag3 C16 Ag2 58(2) . . . . ?
O7 Ag3 C16 Ag2 -126.3(19) . . . . ?
Ag1 Ag3 C16 Ag2 -84.2(4) . . . . ?
Ag4 Ag3 C16 Ag2 158.9(5) 3 . . . ?
Ag3A Ag3 C16 Ag4 -101(2) . . . 3 ?
O7 Ag3 C16 Ag4 75(2) . . . 3 ?
Ag1 Ag3 C16 Ag4 117.0(5) . . . 3 ?
Ag2 Ag3 C16 Ag4 -158.9(5) . . . 3 ?
Ag3 Ag3A C16 C15 134(3) . . . . ?
O8 Ag3A C16 C15 6(5) . . . . ?
Ag2 Ag3A C16 C15 -106.6(19) . . . . ?
Ag4 Ag3A C16 C15 57.3(17) 3 . . . ?
Ag1 Ag3A C16 C15 171(2) . . . . ?
O8 Ag3A C16 Ag3 -128(5) . . . . ?
Ag2 Ag3A C16 Ag3 119(2) . . . . ?
Ag4 Ag3A C16 Ag3 -77(2) 3 . . . ?
Ag1 Ag3A C16 Ag3 37(2) . . . . ?
Ag3 Ag3A C16 Ag1 -37(2) . . . . ?
O8 Ag3A C16 Ag1 -165(3) . . . . ?
Ag2 Ag3A C16 Ag1 82.0(4) . . . . ?
Ag4 Ag3A C16 Ag1 -114.2(5) 3 . . . ?
Ag3 Ag3A C16 Ag2 -119(2) . . . . ?
O8 Ag3A C16 Ag2 113(3) . . . . ?
Ag4 Ag3A C16 Ag2 163.8(5) 3 . . . ?
Ag1 Ag3A C16 Ag2 -82.0(4) . . . . ?
Ag3 Ag3A C16 Ag4 77(2) . . . 3 ?
O8 Ag3A C16 Ag4 -51(3) . . . 3 ?
Ag2 Ag3A C16 Ag4 -163.8(5) . . . 3 ?
Ag1 Ag3A C16 Ag4 114.2(5) . . . 3 ?
O6 Ag1 C16 C15 161.3(11) 3_545 . . . ?
O3 Ag1 C16 C15 -50.0(14) . . . . ?
Ag3 Ag1 C16 C15 -165.5(15) . . . . ?
Ag2 Ag1 C16 C15 113.4(13) . . . . ?
Ag3A Ag1 C16 C15 -173.6(16) . . . . ?
O6 Ag1 C16 Ag3 -33.3(8) 3_545 . . . ?
O3 Ag1 C16 Ag3 115.5(5) . . . . ?
Ag2 Ag1 C16 Ag3 -81.1(3) . . . . ?
Ag3A Ag1 C16 Ag3 -8.2(5) . . . . ?
O6 Ag1 C16 Ag3A -25.1(9) 3_545 . . . ?
O3 Ag1 C16 Ag3A 123.7(7) . . . . ?
Ag3 Ag1 C16 Ag3A 8.2(5) . . . . ?
Ag2 Ag1 C16 Ag3A -73.0(6) . . . . ?
O6 Ag1 C16 Ag2 47.8(7) 3_545 . . . ?
O3 Ag1 C16 Ag2 -163.4(4) . . . . ?
Ag3 Ag1 C16 Ag2 81.1(3) . . . . ?
Ag3A Ag1 C16 Ag2 73.0(6) . . . . ?
O6 Ag1 C16 Ag4 -106.8(7) 3_545 . . 3 ?
O3 Ag1 C16 Ag4 42.0(7) . . . 3 ?
Ag3 Ag1 C16 Ag4 -73.5(4) . . . 3 ?
Ag2 Ag1 C16 Ag4 -154.6(6) . . . 3 ?
Ag3A Ag1 C16 Ag4 -81.7(7) . . . 3 ?
O4 Ag2 C16 C15 -166.0(10) . . . . ?
O3 Ag2 C16 C15 12.0(14) 1_455 . . . ?
Ag3A Ag2 C16 C15 140.5(14) . . . . ?
Ag3 Ag2 C16 C15 152.3(13) . . . . ?
Ag1 Ag2 C16 C15 -125.5(13) . . . . ?
O4 Ag2 C16 Ag3 41.7(7) . . . . ?
O3 Ag2 C16 Ag3 -140.4(5) 1_455 . . . ?
Ag3A Ag2 C16 Ag3 -11.8(5) . . . . ?
Ag1 Ag2 C16 Ag3 82.2(3) . . . . ?
O4 Ag2 C16 Ag3A 53.5(8) . . . . ?
O3 Ag2 C16 Ag3A -128.6(7) 1_455 . . . ?
Ag3 Ag2 C16 Ag3A 11.8(5) . . . . ?
Ag1 Ag2 C16 Ag3A 94.0(6) . . . . ?
O4 Ag2 C16 Ag1 -40.5(7) . . . . ?
O3 Ag2 C16 Ag1 137.4(5) 1_455 . . . ?
Ag3A Ag2 C16 Ag1 -94.0(6) . . . . ?
Ag3 Ag2 C16 Ag1 -82.2(3) . . . . ?
O4 Ag2 C16 Ag4 87.3(12) . . . 3 ?
O3 Ag2 C16 Ag4 -94.7(11) 1_455 . . 3 ?
Ag3A Ag2 C16 Ag4 33.8(10) . . . 3 ?
Ag3 Ag2 C16 Ag4 45.6(9) . . . 3 ?
Ag1 Ag2 C16 Ag4 127.8(12) . . . 3 ?
Ag8 O13 N7 O14 -168.2(10) 2_764 . . . ?
Ag6 O13 N7 O14 -17.6(13) . . . . ?
Ag8 O13 N7 O15 13.1(19) 2_764 . . . ?
Ag6 O13 N7 O15 163.7(12) . . . . ?
O14 N7 O15 Ag7 13.5(18) . . . 3_465 ?
O13 N7 O15 Ag7 -167.9(10) . . . 3_465 ?
N2 C9A Ag8 C8A -2(13) . . . . ?
N2 C9A Ag8 O13 -164(13) . . . 2_765 ?
C8A C9A Ag8 O13 -161(2) . . . 2_765 ?
N2 C9A Ag8 N1 -3(13) . . . . ?
C8A C9A Ag8 N1 -1(2) . . . . ?
C8A C9A Ag8 N2 2(13) . . . . ?
C7 N1 Ag8 C8A 48(96) . . . . ?
C6 N1 Ag8 C8A -130(96) . . . . ?
C7 N1 Ag8 C9A -179.8(17) . . . . ?
C6 N1 Ag8 C9A 2.2(16) . . . . ?
C8A N1 Ag8 C9A 132(96) . . . . ?
C7 N1 Ag8 O13 -48.9(14) . . . 2_765 ?
C6 N1 Ag8 O13 133.1(9) . . . 2_765 ?
C8A N1 Ag8 O13 -97(96) . . . 2_765 ?
C7 N1 Ag8 N2 179.9(10) . . . . ?
C6 N1 Ag8 N2 1.9(7) . . . . ?
C8A N1 Ag8 N2 131(96) . . . . ?
C9A N2 Ag8 C8A 178(14) . . . . ?
C14 N2 Ag8 C8A 179(3) . . . . ?
C11 N2 Ag8 C8A -2(2) . . . . ?
C14 N2 Ag8 C9A 2(13) . . . . ?
C11 N2 Ag8 C9A -179(14) . . . . ?
C9A N2 Ag8 O13 17(14) . . . 2_765 ?
C14 N2 Ag8 O13 19.0(12) . . . 2_765 ?
C11 N2 Ag8 O13 -162.0(7) . . . 2_765 ?
C9A N2 Ag8 N1 176(14) . . . . ?
C14 N2 Ag8 N1 178.1(11) . . . . ?
C11 N2 Ag8 N1 -2.8(7) . . . . ?
C10 C9 Ag8A C8 -43(10) . . . . ?
C8 C9 Ag8A C10 43(10) . . . . ?
C8 C9 Ag8A C5 4.1(10) . . . . ?
C10 C9 Ag8A C5 -39(10) . . . . ?
C8 C9 Ag8A O6 -118.0(19) . . . 4_654 ?
C10 C9 Ag8A O6 -161(9) . . . 4_654 ?
C5 C8 Ag8A C9 56(13) . . . . ?
C9 C8 Ag8A C10 -4.1(10) . . . . ?
C5 C8 Ag8A C10 52(12) . . . . ?
C9 C8 Ag8A C5 -56(13) . . . . ?
C9 C8 Ag8A O6 147.0(11) . . . 4_654 ?
C5 C8 Ag8A O6 -157(12) . . . 4_654 ?
C11 C10 Ag8A C9 -142(11) . . . . ?
C12 C10 Ag8A C9 43(10) . . . . ?
C9 C10 Ag8A C8 136(11) . . . . ?
C11 C10 Ag8A C8 -6.4(12) . . . . ?
C12 C10 Ag8A C8 178.7(14) . . . . ?
C9 C10 Ag8A C5 140(11) . . . . ?
C11 C10 Ag8A C5 -2.4(7) . . . . ?
C12 C10 Ag8A C5 -177.3(10) . . . . ?
C9 C10 Ag8A O6 22(11) . . . 4_654 ?
C11 C10 Ag8A O6 -120.1(9) . . . 4_654 ?
C12 C10 Ag8A O6 65.0(14) . . . 4_654 ?
C4 C5 Ag8A C9 -176.2(13) . . . . ?
C8 C5 Ag8A C9 -123(13) . . . . ?
C6 C5 Ag8A C9 7.4(11) . . . . ?
C4 C5 Ag8A C8 -53(13) . . . . ?
C6 C5 Ag8A C8 130(13) . . . . ?
C4 C5 Ag8A C10 180.0(9) . . . . ?
C8 C5 Ag8A C10 -127(13) . . . . ?
C6 C5 Ag8A C10 3.5(7) . . . . ?
C4 C5 Ag8A O6 -29.1(10) . . . 4_654 ?
C8 C5 Ag8A O6 24(13) . . . 4_654 ?
C6 C5 Ag8A O6 154.4(7) . . . 4_654 ?
C1 Ag5 Ag5A O12 168.3(10) . . . . ?
O12 Ag5 Ag5A O12 -44(5) 3_565 . . . ?
Ag7 Ag5 Ag5A O12 -142.8(7) . . . . ?
Ag6 Ag5 Ag5A O12 -161.7(19) . . . . ?
Ag4 Ag5 Ag5A O12 115.2(10) . . . . ?
O12 Ag5 Ag5A C1 147(5) 3_565 . . . ?
O12 Ag5 Ag5A C1 -168.3(10) . . . . ?
Ag7 Ag5 Ag5A C1 48.9(4) . . . . ?
Ag6 Ag5 Ag5A C1 30.1(11) . . . . ?
Ag4 Ag5 Ag5A C1 -53.1(4) . . . . ?
C1 Ag5 Ag5A Ag6 -30.1(11) . . . . ?
O12 Ag5 Ag5A Ag6 117(4) 3_565 . . . ?
O12 Ag5 Ag5A Ag6 161.7(19) . . . . ?
Ag7 Ag5 Ag5A Ag6 18.9(13) . . . . ?
Ag4 Ag5 Ag5A Ag6 -83.1(11) . . . . ?
C1 Ag5 Ag5A Ag4 53.1(4) . . . . ?
O12 Ag5 Ag5A Ag4 -160(4) 3_565 . . . ?
O12 Ag5 Ag5A Ag4 -115.2(10) . . . . ?
Ag7 Ag5 Ag5A Ag4 102.0(4) . . . . ?
Ag6 Ag5 Ag5A Ag4 83.1(11) . . . . ?
C1 Ag5 Ag5A Ag7 -48.9(4) . . . . ?
O12 Ag5 Ag5A Ag7 98(5) 3_565 . . . ?
O12 Ag5 Ag5A Ag7 142.8(7) . . . . ?
Ag6 Ag5 Ag5A Ag7 -18.9(13) . . . . ?
Ag4 Ag5 Ag5A Ag7 -102.0(4) . . . . ?
N6 O12 Ag5A Ag5 5.8(19) . . . . ?
Ag5 O12 Ag5A Ag5 -174.4(13) 3_465 . . . ?
N6 O12 Ag5A C1 147.9(18) . . . . ?
Ag5 O12 Ag5A C1 -32(2) 3_465 . . . ?
Ag5 O12 Ag5A C1 142(3) . . . . ?
N6 O12 Ag5A Ag6 -158.2(10) . . . . ?
Ag5 O12 Ag5A Ag6 21.6(9) 3_465 . . . ?
Ag5 O12 Ag5A Ag6 -164.0(17) . . . . ?
N6 O12 Ag5A Ag4 113.8(11) . . . . ?
Ag5 O12 Ag5A Ag4 -66.4(7) 3_465 . . . ?
Ag5 O12 Ag5A Ag4 108.0(14) . . . . ?
N6 O12 Ag5A Ag7 -78.9(15) . . . . ?
Ag5 O12 Ag5A Ag7 100.9(9) 3_465 . . . ?
Ag5 O12 Ag5A Ag7 -84.7(15) . . . . ?
C2 C1 Ag5A Ag5 72(2) . . . . ?
Ag6 C1 Ag5A Ag5 -150.8(12) . . . . ?
Ag7 C1 Ag5A Ag5 -67.9(11) . . . . ?
Ag4 C1 Ag5A Ag5 105.0(11) . . . . ?
C2 C1 Ag5A O12 -73(3) . . . . ?
Ag6 C1 Ag5A O12 64(2) . . . . ?
Ag5 C1 Ag5A O12 -145(3) . . . . ?
Ag7 C1 Ag5A O12 147(2) . . . . ?
Ag4 C1 Ag5A O12 -40(2) . . . . ?
C2 C1 Ag5A Ag6 -137.3(19) . . . . ?
Ag5 C1 Ag5A Ag6 150.8(12) . . . . ?
Ag7 C1 Ag5A Ag6 82.9(3) . . . . ?
Ag4 C1 Ag5A Ag6 -104.2(4) . . . . ?
C2 C1 Ag5A Ag4 -33.1(17) . . . . ?
Ag6 C1 Ag5A Ag4 104.2(4) . . . . ?
Ag5 C1 Ag5A Ag4 -105.0(11) . . . . ?
Ag7 C1 Ag5A Ag4 -172.9(4) . . . . ?
C2 C1 Ag5A Ag7 139.8(19) . . . . ?
Ag6 C1 Ag5A Ag7 -82.9(3) . . . . ?
Ag5 C1 Ag5A Ag7 67.9(11) . . . . ?
Ag4 C1 Ag5A Ag7 172.9(4) . . . . ?
C1 Ag6 Ag5A Ag5 38.3(15) . . . . ?
O16 Ag6 Ag5A Ag5 158.8(14) . . . . ?
O13 Ag6 Ag5A Ag5 -103.7(15) . . . . ?
Ag7 Ag6 Ag5A Ag5 -19.9(15) . . . . ?
C1 Ag6 Ag5A O12 -160.7(8) . . . . ?
O16 Ag6 Ag5A O12 -40.2(9) . . . . ?
O13 Ag6 Ag5A O12 57.2(7) . . . . ?
Ag7 Ag6 Ag5A O12 141.0(6) . . . . ?
Ag5 Ag6 Ag5A O12 161(2) . . . . ?
O16 Ag6 Ag5A C1 120.5(7) . . . . ?
O13 Ag6 Ag5A C1 -142.1(5) . . . . ?
Ag7 Ag6 Ag5A C1 -58.3(4) . . . . ?
Ag5 Ag6 Ag5A C1 -38.3(15) . . . . ?
C1 Ag6 Ag5A Ag4 -53.9(4) . . . . ?
O16 Ag6 Ag5A Ag4 66.6(6) . . . . ?
O13 Ag6 Ag5A Ag4 164.1(3) . . . . ?
Ag7 Ag6 Ag5A Ag4 -112.1(2) . . . . ?
Ag5 Ag6 Ag5A Ag4 -92.2(15) . . . . ?
C1 Ag6 Ag5A Ag7 58.3(4) . . . . ?
O16 Ag6 Ag5A Ag7 178.7(5) . . . . ?
O13 Ag6 Ag5A Ag7 -83.8(3) . . . . ?
Ag5 Ag6 Ag5A Ag7 19.9(15) . . . . ?
C1 Ag4 Ag5A Ag5 -75.7(11) . . . . ?
C16 Ag4 Ag5A Ag5 99.3(12) 3_455 . . . ?
O11 Ag4 Ag5A Ag5 157.4(12) 3_465 . . . ?
C2 Ag4 Ag5A Ag5 -67.3(11) . . . . ?
C15 Ag4 Ag5A Ag5 145(2) 3_455 . . . ?
Ag3 Ag4 Ag5A Ag5 101.3(11) 3_455 . . . ?
Ag3A Ag4 Ag5A Ag5 110.8(11) 3_455 . . . ?
C1 Ag4 Ag5A O12 167.1(7) . . . . ?
C16 Ag4 Ag5A O12 -17.9(9) 3_455 . . . ?
O11 Ag4 Ag5A O12 40.1(5) 3_465 . . . ?
C2 Ag4 Ag5A O12 175.5(6) . . . . ?
C15 Ag4 Ag5A O12 27(2) 3_455 . . . ?
Ag3 Ag4 Ag5A O12 -16.0(5) 3_455 . . . ?
Ag5 Ag4 Ag5A O12 -117.2(13) . . . . ?
Ag3A Ag4 Ag5A O12 -6.4(6) 3_455 . . . ?
C16 Ag4 Ag5A C1 175.0(6) 3_455 . . . ?
O11 Ag4 Ag5A C1 -126.9(5) 3_465 . . . ?
C2 Ag4 Ag5A C1 8.4(5) . . . . ?
C15 Ag4 Ag5A C1 -140(2) 3_455 . . . ?
Ag3 Ag4 Ag5A C1 177.0(4) 3_455 . . . ?
Ag5 Ag4 Ag5A C1 75.7(11) . . . . ?
Ag3A Ag4 Ag5A C1 -173.5(5) 3_455 . . . ?
C1 Ag4 Ag5A Ag6 52.2(4) . . . . ?
C16 Ag4 Ag5A Ag6 -132.8(6) 3_455 . . . ?
O11 Ag4 Ag5A Ag6 -74.7(3) 3_465 . . . ?
C2 Ag4 Ag5A Ag6 60.6(3) . . . . ?
C15 Ag4 Ag5A Ag6 -88(2) 3_455 . . . ?
Ag3 Ag4 Ag5A Ag6 -130.79(18) 3_455 . . . ?
Ag5 Ag4 Ag5A Ag6 127.9(12) . . . . ?
Ag3A Ag4 Ag5A Ag6 -121.3(4) 3_455 . . . ?
C1 Ag4 Ag5A Ag7 -5.5(3) . . . . ?
C16 Ag4 Ag5A Ag7 169.5(5) 3_455 . . . ?
O11 Ag4 Ag5A Ag7 -132.5(4) 3_465 . . . ?
C2 Ag4 Ag5A Ag7 2.9(4) . . . . ?
C15 Ag4 Ag5A Ag7 -145(2) 3_455 . . . ?
Ag3 Ag4 Ag5A Ag7 171.5(2) 3_455 . . . ?
Ag5 Ag4 Ag5A Ag7 70.2(10) . . . . ?
Ag3A Ag4 Ag5A Ag7 -179.0(4) 3_455 . . . ?
C1 Ag7 Ag5A Ag5 99.4(11) . . . . ?
O15 Ag7 Ag5A Ag5 -94.2(11) 3_565 . . . ?
O16 Ag7 Ag5A Ag5 -4.4(12) 1_655 . . . ?
Ag6 Ag7 Ag5A Ag5 163.4(12) . . . . ?
C1 Ag7 Ag5A O12 -161.6(11) . . . . ?
O15 Ag7 Ag5A O12 4.7(10) 3_565 . . . ?
O16 Ag7 Ag5A O12 94.5(9) 1_655 . . . ?
Ag5 Ag7 Ag5A O12 98.9(14) . . . . ?
Ag6 Ag7 Ag5A O12 -97.7(9) . . . . ?
O15 Ag7 Ag5A C1 166.4(6) 3_565 . . . ?
O16 Ag7 Ag5A C1 -103.9(5) 1_655 . . . ?
Ag5 Ag7 Ag5A C1 -99.4(11) . . . . ?
Ag6 Ag7 Ag5A C1 64.0(4) . . . . ?
C1 Ag7 Ag5A Ag6 -64.0(4) . . . . ?
O15 Ag7 Ag5A Ag6 102.4(4) 3_565 . . . ?
O16 Ag7 Ag5A Ag6 -167.8(4) 1_655 . . . ?
Ag5 Ag7 Ag5A Ag6 -163.4(12) . . . . ?
C1 Ag7 Ag5A Ag4 6.0(4) . . . . ?
O15 Ag7 Ag5A Ag4 172.4(5) 3_565 . . . ?
O16 Ag7 Ag5A Ag4 -97.9(4) 1_655 . . . ?
Ag5 Ag7 Ag5A Ag4 -93.5(11) . . . . ?
Ag6 Ag7 Ag5A Ag4 69.9(2) . . . . ?
O13 Ag8 C8A C9A 134(5) 2_765 . . . ?
N1 Ag8 C8A C9A 48(96) . . . . ?
N2 Ag8 C8A C9A -0.3(15) . . . . ?
C9A Ag8 C8A N1 -48(96) . . . . ?
O13 Ag8 C8A N1 86(97) 2_765 . . . ?
N2 Ag8 C8A N1 -48(96) . . . . ?
N2 C9A C8A Ag8 179(3) . . . . ?
Ag8 C9A C8A N1 178(4) . . . . ?
N2 C9A C8A N1 -3(5) . . . . ?
C7 N1 C8A Ag8 -132(95) . . . . ?
C6 N1 C8A Ag8 51(96) . . . . ?
C7 N1 C8A C9A -179(2) . . . . ?
C6 N1 C8A C9A 4(4) . . . . ?
Ag8 N1 C8A C9A -47(94) . . . . ?

_diffrn_measured_fraction_theta_max 0.990
_diffrn_reflns_theta_full        27.72
_diffrn_measured_fraction_theta_full 0.990
_refine_diff_density_max         1.540
_refine_diff_density_min         -1.284
_refine_diff_density_rms         0.211
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 814054'
_audit_update_record             
;
2017-03-15 deposited with the CCDC.
2017-04-19 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
 ?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C8 H2 Ag5 N5 O9'
_chemical_formula_weight         851.50

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   P-1

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   8.4999(11)
_cell_length_b                   8.8716(11)
_cell_length_c                   10.0953(13)
_cell_angle_alpha                78.997(2)
_cell_angle_beta                 80.015(2)
_cell_angle_gamma                81.741(2)
_cell_volume                     731.12(16)
_cell_formula_units_Z            2
_cell_measurement_temperature    298(2)
_cell_measurement_reflns_used    1802
_cell_measurement_theta_min      2.27
_cell_measurement_theta_max      26.00

_exptl_crystal_description       block
_exptl_crystal_colour            black
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.06
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    3.868
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             784
_exptl_absorpt_coefficient_mu    6.643
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.460
_exptl_absorpt_correction_T_max  0.652
_exptl_absorpt_process_details   ?

_exptl_special_details           
;
 ?
;

_diffrn_ambient_temperature      298(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            5251
_diffrn_reflns_av_R_equivalents  0.1490
_diffrn_reflns_av_sigmaI/netI    0.1077
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_theta_min         2.08
_diffrn_reflns_theta_max         25.99
_reflns_number_total             2826
_reflns_number_gt                2488
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker SMART'
_computing_cell_refinement       'Bruker SMART'
_computing_data_reduction        'Bruker SAIT'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.1003P)²+10.2149P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         2826
_refine_ls_number_parameters     238
_refine_ls_number_restraints     6
_refine_ls_R_factor_all          0.0820
_refine_ls_R_factor_gt           0.0749
_refine_ls_wR_factor_ref         0.1972
_refine_ls_wR_factor_gt          0.1907
_refine_ls_goodness_of_fit_ref   1.061
_refine_ls_restrained_S_all      1.063
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag5 Ag 0.50654(19) 0.84338(14) 0.07465(11) 0.0590(4) Uani 1 1 d . . .
O3 O -0.2140(19) 0.4655(19) 0.2844(15) 0.085(3) Uani 1 1 d . . .
Ag4 Ag 0.37340(12) 0.52906(10) 0.12593(8) 0.0373(3) Uani 1 1 d . . .
Ag3 Ag 0.49273(14) 0.58918(12) 0.35372(10) 0.0450(3) Uani 1 1 d . . .
O9 O -0.0280(14) -0.1846(16) 0.8034(15) 0.070(4) Uani 1 1 d . . .
N5 N -0.1530(13) -0.1337(13) 0.8682(11) 0.039(2) Uani 1 1 d . . .
O7 O -0.1446(15) -0.0845(13) 0.9765(11) 0.059(3) Uani 1 1 d . . .
Ag2 Ag 0.08357(13) 0.38577(14) 0.33491(12) 0.0515(4) Uani 1 1 d . . .
Ag1 Ag 0.09996(14) -0.21082(15) 1.05268(13) 0.0562(4) Uani 1 1 d . . .
C1 C 0.3402(13) 0.1721(12) 0.5357(10) 0.026(2) Uani 1 1 d . . .
C2 C 0.2828(13) 0.0320(13) 0.5313(11) 0.029(2) Uani 1 1 d . . .
H2 H 0.2424 0.0178 0.4552 0.035 Uiso 1 1 calc R . .
C3 C 0.2885(14) -0.0810(12) 0.6417(11) 0.028(2) Uani 1 1 d . . .
H3 H 0.2503 -0.1748 0.6441 0.034 Uiso 1 1 calc R . .
C4 C 0.3536(13) -0.0539(11) 0.7532(10) 0.0230(19) Uani 1 1 d . . .
C7 C 0.3421(15) 0.3013(13) 0.4264(11) 0.031(2) Uani 1 1 d . . .
C8 C 0.3594(14) 0.4058(13) 0.3303(11) 0.032(2) Uani 1 1 d . . .
C5 C 0.3624(13) -0.1717(13) 0.8752(10) 0.026(2) Uani 1 1 d . . .
C6 C 0.3706(13) -0.2824(12) 0.9626(10) 0.027(2) Uani 1 1 d . . .
N1 N 0.4055(11) 0.1935(10) 0.6450(9) 0.0259(18) Uani 1 1 d . . .
N2 N 0.4084(11) 0.0813(10) 0.7536(9) 0.0256(18) Uani 1 1 d . . .
N3 N -0.1012(14) 0.2326(14) 0.6299(11) 0.043(3) Uani 1 1 d . . .
N4 N -0.1663(13) 0.5395(11) 0.1670(12) 0.040(2) Uani 1 1 d . . .
O5 O 0.011(2) 0.270(2) 0.672(2) 0.108(5) Uani 1 1 d U . .
O6 O -0.094(2) 0.2472(19) 0.5125(15) 0.085(3) Uani 1 1 d . . .
O4 O -0.214(2) 0.1761(19) 0.7079(17) 0.102(6) Uani 1 1 d . . .
O2 O -0.2616(15) 0.6054(14) 0.0920(14) 0.066(3) Uani 1 1 d . . .
O1 O -0.0186(13) 0.5392(14) 0.1348(13) 0.058(3) Uani 1 1 d . . .
O8 O -0.2834(13) -0.1296(18) 0.8327(14) 0.073(4) Uani 1 1 d . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag5 N2 2.235(9) 2_666 ?
Ag5 C6 2.273(11) 1_564 ?
Ag5 C5 2.565(11) 1_564 ?
Ag5 Ag5 2.894(2) 2_675 ?
Ag5 Ag4 3.0784(15) . ?
Ag5 Ag3 3.2516(15) . ?
O3 N4 1.270(17) . ?
Ag4 C6 2.114(10) 1_564 ?
Ag4 C8 2.135(10) . ?
Ag4 Ag3 2.8344(14) . ?
Ag4 Ag4 3.1059(18) 2_665 ?
Ag4 Ag1 3.1110(16) 1_564 ?
Ag3 C8 2.182(12) . ?
Ag3 N1 2.226(9) 2_666 ?
Ag3 Ag3 3.087(2) 2_666 ?
O9 N5 1.223(15) . ?
N5 O8 1.217(16) . ?
N5 O7 1.269(15) . ?
O7 Ag1 2.393(13) . ?
Ag2 C8 2.368(12) . ?
Ag2 O6 2.401(13) . ?
Ag2 O1 2.430(12) . ?
Ag2 C7 2.492(12) . ?
Ag1 C6 2.366(11) . ?
Ag1 O1 2.504(12) 1_546 ?
Ag1 C5 2.628(10) . ?
Ag1 Ag4 3.1109(16) 1_546 ?
C1 N1 1.373(14) . ?
C1 C2 1.411(16) . ?
C1 C7 1.431(15) . ?
C2 C3 1.352(15) . ?
C3 C4 1.410(15) . ?
C4 N2 1.349(14) . ?
C4 C5 1.460(13) . ?
C7 C8 1.212(16) . ?
C5 C6 1.191(15) . ?
C5 Ag5 2.565(11) 1_546 ?
C6 Ag4 2.114(10) 1_546 ?
C6 Ag5 2.273(11) 1_546 ?
N1 N2 1.333(12) . ?
N1 Ag3 2.226(9) 2_666 ?
N2 Ag5 2.235(9) 2_666 ?
N3 O6 1.160(18) . ?
N3 O5 1.22(2) . ?
N3 O4 1.230(19) . ?
N4 O2 1.216(16) . ?
N4 O1 1.241(15) . ?
O1 Ag1 2.504(12) 1_564 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N2 Ag5 C6 160.0(3) 2_666 1_564 ?
N2 Ag5 C5 164.4(3) 2_666 1_564 ?
C6 Ag5 C5 27.7(4) 1_564 1_564 ?
N2 Ag5 Ag5 90.5(2) 2_666 2_675 ?
C6 Ag5 Ag5 104.7(3) 1_564 2_675 ?
C5 Ag5 Ag5 77.2(2) 1_564 2_675 ?
N2 Ag5 Ag4 118.8(2) 2_666 . ?
C6 Ag5 Ag4 43.4(3) 1_564 . ?
C5 Ag5 Ag4 71.0(2) 1_564 . ?
Ag5 Ag5 Ag4 146.71(7) 2_675 . ?
N2 Ag5 Ag3 65.8(2) 2_666 . ?
C6 Ag5 Ag3 96.2(3) 1_564 . ?
C5 Ag5 Ag3 123.4(2) 1_564 . ?
Ag5 Ag5 Ag3 153.08(7) 2_675 . ?
Ag4 Ag5 Ag3 53.12(3) . . ?
C6 Ag4 C8 159.5(4) 1_564 . ?
C6 Ag4 Ag3 113.8(3) 1_564 . ?
C8 Ag4 Ag3 49.7(3) . . ?
C6 Ag4 Ag5 47.6(3) 1_564 . ?
C8 Ag4 Ag5 115.8(3) . . ?
Ag3 Ag4 Ag5 66.57(3) . . ?
C6 Ag4 Ag4 67.2(3) 1_564 2_665 ?
C8 Ag4 Ag4 128.4(3) . 2_665 ?
Ag3 Ag4 Ag4 116.47(6) . 2_665 ?
Ag5 Ag4 Ag4 83.41(4) . 2_665 ?
C6 Ag4 Ag1 49.5(3) 1_564 1_564 ?
C8 Ag4 Ag1 118.8(3) . 1_564 ?
Ag3 Ag4 Ag1 108.43(5) . 1_564 ?
Ag5 Ag4 Ag1 71.28(4) . 1_564 ?
Ag4 Ag4 Ag1 112.68(5) 2_665 1_564 ?
C8 Ag3 N1 168.9(4) . 2_666 ?
C8 Ag3 Ag4 48.3(3) . . ?
N1 Ag3 Ag4 123.4(2) 2_666 . ?
C8 Ag3 Ag3 85.4(3) . 2_666 ?
N1 Ag3 Ag3 103.0(2) 2_666 2_666 ?
Ag4 Ag3 Ag3 133.54(5) . 2_666 ?
C8 Ag3 Ag5 108.1(3) . . ?
N1 Ag3 Ag5 63.1(2) 2_666 . ?
Ag4 Ag3 Ag5 60.31(3) . . ?
Ag3 Ag3 Ag5 166.02(6) 2_666 . ?
O8 N5 O9 122.4(13) . . ?
O8 N5 O7 119.6(13) . . ?
O9 N5 O7 118.1(13) . . ?
N5 O7 Ag1 106.3(8) . . ?
C8 Ag2 O6 127.8(5) . . ?
C8 Ag2 O1 112.0(4) . . ?
O6 Ag2 O1 120.1(5) . . ?
C8 Ag2 C7 28.7(4) . . ?
O6 Ag2 C7 99.7(5) . . ?
O1 Ag2 C7 140.2(4) . . ?
C6 Ag1 O7 139.7(4) . . ?
C6 Ag1 O1 105.0(4) . 1_546 ?
O7 Ag1 O1 91.8(4) . 1_546 ?
C6 Ag1 C5 26.9(3) . . ?
O7 Ag1 C5 115.4(4) . . ?
O1 Ag1 C5 125.4(4) 1_546 . ?
C6 Ag1 Ag4 42.8(2) . 1_546 ?
O7 Ag1 Ag4 160.2(3) . 1_546 ?
O1 Ag1 Ag4 71.2(2) 1_546 1_546 ?
C5 Ag1 Ag4 69.7(2) . 1_546 ?
N1 C1 C2 122.1(9) . . ?
N1 C1 C7 114.1(9) . . ?
C2 C1 C7 123.7(10) . . ?
C3 C2 C1 117.6(10) . . ?
C2 C3 C4 118.7(10) . . ?
N2 C4 C3 122.1(9) . . ?
N2 C4 C5 116.9(9) . . ?
C3 C4 C5 121.0(9) . . ?
C8 C7 C1 173.6(13) . . ?
C8 C7 Ag2 70.0(8) . . ?
C1 C7 Ag2 115.6(8) . . ?
C7 C8 Ag4 160.0(11) . . ?
C7 C8 Ag3 116.7(10) . . ?
Ag4 C8 Ag3 82.1(4) . . ?
C7 C8 Ag2 81.3(8) . . ?
Ag4 C8 Ag2 90.2(4) . . ?
Ag3 C8 Ag2 134.1(5) . . ?
C6 C5 C4 170.7(11) . . ?
C6 C5 Ag5 62.4(7) . 1_546 ?
C4 C5 Ag5 125.3(7) . 1_546 ?
C6 C5 Ag1 64.2(7) . . ?
C4 C5 Ag1 118.6(7) . . ?
Ag5 C5 Ag1 88.0(3) 1_546 . ?
C5 C6 Ag4 176.3(9) . 1_546 ?
C5 C6 Ag5 90.0(8) . 1_546 ?
Ag4 C6 Ag5 89.1(4) 1_546 1_546 ?
C5 C6 Ag1 88.9(8) . . ?
Ag4 C6 Ag1 87.8(4) 1_546 . ?
Ag5 C6 Ag1 102.0(4) 1_546 . ?
N2 N1 C1 119.3(9) . . ?
N2 N1 Ag3 118.9(7) . 2_666 ?
C1 N1 Ag3 121.8(7) . 2_666 ?
N1 N2 C4 120.2(9) . . ?
N1 N2 Ag5 111.8(7) . 2_666 ?
C4 N2 Ag5 127.9(7) . 2_666 ?
O6 N3 O5 117.1(16) . . ?
O6 N3 O4 121.1(16) . . ?
O5 N3 O4 121.7(17) . . ?
O2 N4 O1 123.0(12) . . ?
O2 N4 O3 121.0(13) . . ?
O1 N4 O3 115.9(13) . . ?
N3 O6 Ag2 129.1(13) . . ?
N4 O1 Ag2 102.8(8) . . ?
N4 O1 Ag1 120.0(8) . 1_564 ?
Ag2 O1 Ag1 113.6(5) . 1_564 ?

_diffrn_measured_fraction_theta_max 0.989
_diffrn_reflns_theta_full        25.99
_diffrn_measured_fraction_theta_full 0.989
_refine_diff_density_max         3.517
_refine_diff_density_min         -3.671
_refine_diff_density_rms         0.390
