 
data_1 
 
_audit_creation_method            SHELXL-97 
_chemical_name_systematic 
; 
 ? 
; 
_chemical_name_common             ? 
_chemical_melting_point           ? 
_chemical_formula_moiety          'F6 Ga Na3' 
_chemical_formula_sum 
 'F6 Ga Na3' 
_chemical_formula_weight          252.69 
 
loop_ 
 _atom_type_symbol 
 _atom_type_description 
 _atom_type_scat_dispersion_real 
 _atom_type_scat_dispersion_imag 
 _atom_type_scat_source 
 'F'  'F'   0.0171   0.0103 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Na'  'Na'   0.0362   0.0249 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 'Ga'  'Ga'   0.2307   1.6083 
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 
 
_symmetry_cell_setting            Monoclinic 
_symmetry_space_group_name_H-M    P2(1)/n 
 
loop_ 
 _symmetry_equiv_pos_as_xyz 
 'x, y, z' 
 '-x+1/2, y+1/2, -z+1/2' 
 '-x, -y, -z' 
 'x-1/2, -y-1/2, z-1/2' 
 
_cell_length_a                    5.4760(2) 
_cell_length_b                    5.6862(2) 
_cell_length_c                    7.9009(3) 
_cell_angle_alpha                 90.00 
_cell_angle_beta                  90.309(2) 
_cell_angle_gamma                 90.00 
_cell_volume                      246.012(16) 
_cell_formula_units_Z             2 
_cell_measurement_temperature     296(2) 
_cell_measurement_reflns_used     2680 
_cell_measurement_theta_min       4.42 
_cell_measurement_theta_max       27.50 
 
_exptl_crystal_description        'block' 
_exptl_crystal_colour             'colourless' 
_exptl_crystal_size_max           0.078 
_exptl_crystal_size_mid           0.051 
_exptl_crystal_size_min           0.032 
_exptl_crystal_density_meas       ? 
_exptl_crystal_density_diffrn     3.411 
_exptl_crystal_density_method     'not measured' 
_exptl_crystal_F_000              236 
_exptl_absorpt_coefficient_mu     5.900 
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_correction_T_min   0.925
_exptl_absorpt_correction_T_max   0.948 
_exptl_absorpt_process_details    'SADABS (Sheldrick, 1996)'
_exptl_special_details 
; 
? 
; 
 
_diffrn_ambient_temperature       296(2) 
_diffrn_radiation_wavelength      0.71073 
_diffrn_radiation_type            MoK\a 
_diffrn_radiation_source          'fine-focus sealed tube' 
_diffrn_radiation_monochromator   graphite 
_diffrn_measurement_device_type   'Bruker APEX-II area-detector diffractometer' 
_diffrn_measurement_method        'phi and omega scans' 
_diffrn_detector_area_resol_mean  ? 
_diffrn_standards_number          none 
_diffrn_standards_interval_count  none 
_diffrn_standards_interval_time   none 
_diffrn_standards_decay_%         none 
_diffrn_reflns_number             3807 
_diffrn_reflns_av_R_equivalents   0.0254 
_diffrn_reflns_av_sigmaI/netI     0.0163 
_diffrn_reflns_limit_h_min        -7 
_diffrn_reflns_limit_h_max        7 
_diffrn_reflns_limit_k_min        -7 
_diffrn_reflns_limit_k_max        7 
_diffrn_reflns_limit_l_min        -9 
_diffrn_reflns_limit_l_max        10 
_diffrn_reflns_theta_min          4.42 
_diffrn_reflns_theta_max          27.50 
_reflns_number_total              566 
_reflns_number_gt                 544 
_reflns_threshold_expression      >2sigma(I) 
 
_computing_data_collection        'APEXII (Bruker, 2006)' 
_computing_cell_refinement        'SAINT (Bruker, 2006)' 
_computing_data_reduction         'SAINT' 
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)' 
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 1997)' 
_computing_molecular_graphics     'DIAMOND (Brandenburg, 1999)' 
_computing_publication_material   'SHELXTL (Sheldrick, 2008)' 
 
_refine_special_details 
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
; 
 
_refine_ls_structure_factor_coef  Fsqd  
_refine_ls_matrix_type            full 
_refine_ls_weighting_scheme       calc  
_refine_ls_weighting_details 
 'calc w=1/[σ²(Fo²)+(0.0444P)²+0.1337P] where P=(Fo²+2Fc²)/3' 
_atom_sites_solution_primary      direct 
_atom_sites_solution_secondary    difmap 
_atom_sites_solution_hydrogens    CONSTR 
_refine_ls_hydrogen_treatment     CONSTR 
_refine_ls_extinction_method      none 
_refine_ls_extinction_coef        ? 
_refine_ls_number_reflns          566 
_refine_ls_number_parameters      49 
_refine_ls_number_restraints      0 
_refine_ls_R_factor_all           0.0205 
_refine_ls_R_factor_gt            0.0197 
_refine_ls_wR_factor_ref          0.0579 
_refine_ls_wR_factor_gt           0.0573 
_refine_ls_goodness_of_fit_ref    1.008 
_refine_ls_restrained_S_all       1.008 
_refine_ls_shift/su_max           0.000 
_refine_ls_shift/su_mean          0.000 
 
loop_ 
 _atom_site_label 
 _atom_site_type_symbol 
 _atom_site_fract_x 
 _atom_site_fract_y 
 _atom_site_fract_z 
 _atom_site_U_iso_or_equiv 
 _atom_site_adp_type 
 _atom_site_occupancy 
 _atom_site_symmetry_multiplicity 
 _atom_site_calc_flag 
 _atom_site_refinement_flags 
 _atom_site_disorder_assembly 
 _atom_site_disorder_group 
Na1 Na 0.5000 -0.5000 0.0000 0.0125(3) Uani 1 2 d S . . 
Na2 Na -0.01450(17) 0.4456(2) 0.25335(11) 0.0199(2) Uani 1 1 d . . . 
Ga1 Ga 0.0000 0.0000 0.0000 0.00713(15) Uani 1 2 d S . . 
F1 F 0.2827(2) -0.1751(2) -0.04966(15) 0.0176(3) Uani 1 1 d . . . 
F2 F 0.1111(2) 0.0523(2) 0.22418(16) 0.0161(3) Uani 1 1 d . . . 
F3 F 0.1649(2) 0.2771(2) -0.06726(15) 0.0177(3) Uani 1 1 d . . . 
 
 
_geom_special_details 
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
; 
 
loop_ 
 _geom_bond_atom_site_label_1 
 _geom_bond_atom_site_label_2 
 _geom_bond_distance 
 _geom_bond_site_symmetry_2 
 _geom_bond_publ_flag 
Na1 F1 2.2311(12) 3_645 ? 
Na1 F1 2.2311(12) . ? 
Na1 F2 2.2851(13) 2_545 ? 
Na1 F2 2.2851(13) 4_655 ? 
Na1 F3 2.2904(12) 1_545 ? 
Na1 F3 2.2904(12) 3_655 ? 
Na1 Na2 3.1973(11) 4_655 ? 
Na1 Na2 3.1973(11) 2_545 ? 
Na1 Na2 3.3337(9) 3 ? 
Na1 Na2 3.3337(9) 1_645 ? 
Na1 Na2 3.4787(9) 1_545 ? 
Na1 Na2 3.4787(9) 3_655 ? 
Na2 F2 2.2966(17) 2 ? 
Na2 F3 2.3052(15) 3_565 ? 
Na2 F1 2.3187(15) 4_566 ? 
Na2 F2 2.3516(18) . ? 
Na2 F3 2.5925(17) 4_566 ? 
Na2 F1 2.6625(17) 3 ? 
Na2 F1 2.7441(15) 2 ? 
Na2 F3 2.8857(16) . ? 
Na2 Na1 3.1973(11) 2 ? 
Na2 Ga1 3.2303(11) . ? 
Na2 Ga1 3.3192(9) 2_455 ? 
Na2 Na1 3.3337(9) 1_465 ? 
Ga1 F1 1.8838(12) 3 ? 
Ga1 F1 1.8838(12) . ? 
Ga1 F2 1.8932(12) 3 ? 
Ga1 F2 1.8932(12) . ? 
Ga1 F3 1.8934(12) 3 ? 
Ga1 F3 1.8934(12) . ? 
Ga1 Na2 3.2303(11) 3 ? 
Ga1 Na2 3.3192(9) 2_445 ? 
Ga1 Na2 3.3192(9) 4_665 ? 
Ga1 Na2 3.4310(9) 4_565 ? 
Ga1 Na2 3.4310(9) 2_545 ? 
F1 Na2 2.3187(15) 4_665 ? 
F1 Na2 2.6625(17) 3 ? 
F1 Na2 2.7441(15) 2_545 ? 
F2 Na1 2.2851(13) 2 ? 
F2 Na2 2.2966(17) 2_545 ? 
F3 Na1 2.2904(12) 1_565 ? 
F3 Na2 2.3052(15) 3_565 ? 
F3 Na2 2.5925(17) 4_665 ? 
 
loop_ 
 _geom_angle_atom_site_label_1 
 _geom_angle_atom_site_label_2 
 _geom_angle_atom_site_label_3 
 _geom_angle 
 _geom_angle_site_symmetry_1 
 _geom_angle_site_symmetry_3 
 _geom_angle_publ_flag 
F1 Na1 F1 180.00(6) 3_645 . ? 
F1 Na1 F2 94.85(5) 3_645 2_545 ? 
F1 Na1 F2 85.15(5) . 2_545 ? 
F1 Na1 F2 85.15(5) 3_645 4_655 ? 
F1 Na1 F2 94.85(5) . 4_655 ? 
F2 Na1 F2 180.00(10) 2_545 4_655 ? 
F1 Na1 F3 90.47(4) 3_645 1_545 ? 
F1 Na1 F3 89.53(4) . 1_545 ? 
F2 Na1 F3 94.37(5) 2_545 1_545 ? 
F2 Na1 F3 85.63(5) 4_655 1_545 ? 
F1 Na1 F3 89.53(4) 3_645 3_655 ? 
F1 Na1 F3 90.47(4) . 3_655 ? 
F2 Na1 F3 85.63(5) 2_545 3_655 ? 
F2 Na1 F3 94.37(5) 4_655 3_655 ? 
F3 Na1 F3 180.0 1_545 3_655 ? 
F1 Na1 Na2 57.48(4) 3_645 4_655 ? 
F1 Na1 Na2 122.52(4) . 4_655 ? 
F2 Na1 Na2 132.72(4) 2_545 4_655 ? 
F2 Na1 Na2 47.28(4) 4_655 4_655 ? 
F3 Na1 Na2 53.33(4) 1_545 4_655 ? 
F3 Na1 Na2 126.67(4) 3_655 4_655 ? 
F1 Na1 Na2 122.52(4) 3_645 2_545 ? 
F1 Na1 Na2 57.48(4) . 2_545 ? 
F2 Na1 Na2 47.28(4) 2_545 2_545 ? 
F2 Na1 Na2 132.72(4) 4_655 2_545 ? 
F3 Na1 Na2 126.67(4) 1_545 2_545 ? 
F3 Na1 Na2 53.33(4) 3_655 2_545 ? 
Na2 Na1 Na2 180.0 4_655 2_545 ? 
F1 Na1 Na2 127.24(4) 3_645 3 ? 
F1 Na1 Na2 52.76(4) . 3 ? 
F2 Na1 Na2 110.18(4) 2_545 3 ? 
F2 Na1 Na2 69.82(4) 4_655 3 ? 
F3 Na1 Na2 43.67(4) 1_545 3 ? 
F3 Na1 Na2 136.33(4) 3_655 3 ? 
Na2 Na1 Na2 71.967(19) 4_655 3 ? 
Na2 Na1 Na2 108.033(19) 2_545 3 ? 
F1 Na1 Na2 52.76(4) 3_645 1_645 ? 
F1 Na1 Na2 127.24(4) . 1_645 ? 
F2 Na1 Na2 69.82(4) 2_545 1_645 ? 
F2 Na1 Na2 110.18(4) 4_655 1_645 ? 
F3 Na1 Na2 136.33(4) 1_545 1_645 ? 
F3 Na1 Na2 43.67(4) 3_655 1_645 ? 
Na2 Na1 Na2 108.033(19) 4_655 1_645 ? 
Na2 Na1 Na2 71.967(19) 2_545 1_645 ? 
Na2 Na1 Na2 180.00(4) 3 1_645 ? 
F1 Na1 Na2 104.95(4) 3_645 1_545 ? 
F1 Na1 Na2 75.05(4) . 1_545 ? 
F2 Na1 Na2 40.73(4) 2_545 1_545 ? 
F2 Na1 Na2 139.27(4) 4_655 1_545 ? 
F3 Na1 Na2 55.53(4) 1_545 1_545 ? 
F3 Na1 Na2 124.47(4) 3_655 1_545 ? 
Na2 Na1 Na2 105.23(2) 4_655 1_545 ? 
Na2 Na1 Na2 74.77(2) 2_545 1_545 ? 
Na2 Na1 Na2 73.02(2) 3 1_545 ? 
Na2 Na1 Na2 106.98(2) 1_645 1_545 ? 
F1 Na1 Na2 75.05(4) 3_645 3_655 ? 
F1 Na1 Na2 104.95(4) . 3_655 ? 
F2 Na1 Na2 139.27(4) 2_545 3_655 ? 
F2 Na1 Na2 40.73(4) 4_655 3_655 ? 
F3 Na1 Na2 124.47(4) 1_545 3_655 ? 
F3 Na1 Na2 55.53(4) 3_655 3_655 ? 
Na2 Na1 Na2 74.77(2) 4_655 3_655 ? 
Na2 Na1 Na2 105.23(2) 2_545 3_655 ? 
Na2 Na1 Na2 106.98(2) 3 3_655 ? 
Na2 Na1 Na2 73.02(2) 1_645 3_655 ? 
Na2 Na1 Na2 180.000(17) 1_545 3_655 ? 
F2 Na2 F3 102.05(6) 2 3_565 ? 
F2 Na2 F1 105.27(6) 2 4_566 ? 
F3 Na2 F1 82.67(6) 3_565 4_566 ? 
F2 Na2 F2 88.68(5) 2 . ? 
F3 Na2 F2 133.77(6) 3_565 . ? 
F1 Na2 F2 137.93(6) 4_566 . ? 
F2 Na2 F3 137.78(6) 2 4_566 ? 
F3 Na2 F3 116.24(4) 3_565 4_566 ? 
F1 Na2 F3 65.15(5) 4_566 4_566 ? 
F2 Na2 F3 77.78(5) . 4_566 ? 
F2 Na2 F1 136.60(6) 2 3 ? 
F3 Na2 F1 79.38(5) 3_565 3 ? 
F1 Na2 F1 117.79(4) 4_566 3 ? 
F2 Na2 F1 63.38(5) . 3 ? 
F3 Na2 F1 71.05(5) 4_566 3 ? 
F2 Na2 F1 63.89(5) 2 2 ? 
F3 Na2 F1 151.31(6) 3_565 2 ? 
F1 Na2 F1 77.82(5) 4_566 2 ? 
F2 Na2 F1 73.24(5) . 2 ? 
F3 Na2 F1 73.91(4) 4_566 2 ? 
F1 Na2 F1 128.49(5) 3 2 ? 
F2 Na2 F3 79.85(5) 2 . ? 
F3 Na2 F3 77.85(5) 3_565 . ? 
F1 Na2 F3 160.50(6) 4_566 . ? 
F2 Na2 F3 59.80(4) . . ? 
F3 Na2 F3 123.54(5) 4_566 . ? 
F1 Na2 F3 57.78(4) 3 . ? 
F1 Na2 F3 120.52(5) 2 . ? 
F2 Na2 Na1 98.13(5) 2 2 ? 
F3 Na2 Na1 159.80(5) 3_565 2 ? 
F1 Na2 Na1 92.71(4) 4_566 2 ? 
F2 Na2 Na1 45.55(4) . 2 ? 
F3 Na2 Na1 45.12(3) 4_566 2 ? 
F1 Na2 Na1 85.55(4) 3 2 ? 
F1 Na2 Na1 43.28(3) 2 2 ? 
F3 Na2 Na1 105.33(4) . 2 ? 
F2 Na2 Ga1 103.19(5) 2 . ? 
F3 Na2 Ga1 98.70(4) 3_565 . ? 
F1 Na2 Ga1 150.55(5) 4_566 . ? 
F2 Na2 Ga1 35.42(3) . . ? 
F3 Na2 Ga1 88.55(4) 4_566 . ? 
F1 Na2 Ga1 35.67(3) 3 . ? 
F1 Na2 Ga1 108.64(4) 2 . ? 
F3 Na2 Ga1 35.50(3) . . ? 
Na1 Na2 Ga1 75.84(3) 2 . ? 
F2 Na2 Ga1 134.68(5) 2 2_455 ? 
F3 Na2 Ga1 91.50(4) 3_565 2_455 ? 
F1 Na2 Ga1 33.44(3) 4_566 2_455 ? 
F2 Na2 Ga1 112.44(5) . 2_455 ? 
F3 Na2 Ga1 34.68(3) 4_566 2_455 ? 
F1 Na2 Ga1 88.15(4) 3 2_455 ? 
F1 Na2 Ga1 83.72(4) 2 2_455 ? 
F3 Na2 Ga1 145.47(4) . 2_455 ? 
Na1 Na2 Ga1 74.53(2) 2 2_455 ? 
Ga1 Na2 Ga1 117.34(3) . 2_455 ? 
F2 Na2 Na1 141.77(5) 2 1_465 ? 
F3 Na2 Na1 43.32(3) 3_565 1_465 ? 
F1 Na2 Na1 88.15(4) 4_566 1_465 ? 
F2 Na2 Na1 105.20(5) . 1_465 ? 
F3 Na2 Na1 80.41(4) 4_566 1_465 ? 
F1 Na2 Na1 41.84(3) 3 1_465 ? 
F1 Na2 Na1 154.04(4) 2 1_465 ? 
F3 Na2 Na1 77.17(3) . 1_465 ? 
Na1 Na2 Na1 117.17(3) 2 1_465 ? 
Ga1 Na2 Na1 73.91(2) . 1_465 ? 
Ga1 Na2 Na1 72.853(19) 2_455 1_465 ? 
F1 Ga1 F1 180.00(7) 3 . ? 
F1 Ga1 F2 91.00(5) 3 3 ? 
F1 Ga1 F2 89.00(5) . 3 ? 
F1 Ga1 F2 89.00(5) 3 . ? 
F1 Ga1 F2 91.00(6) . . ? 
F2 Ga1 F2 180.00(9) 3 . ? 
F1 Ga1 F3 89.28(5) 3 3 ? 
F1 Ga1 F3 90.72(5) . 3 ? 
F2 Ga1 F3 88.89(6) 3 3 ? 
F2 Ga1 F3 91.11(6) . 3 ? 
F1 Ga1 F3 90.72(5) 3 . ? 
F1 Ga1 F3 89.28(5) . . ? 
F2 Ga1 F3 91.11(6) 3 . ? 
F2 Ga1 F3 88.89(6) . . ? 
F3 Ga1 F3 180.00(8) 3 . ? 
F1 Ga1 Na2 55.49(4) 3 . ? 
F1 Ga1 Na2 124.51(4) . . ? 
F2 Ga1 Na2 133.95(5) 3 . ? 
F2 Ga1 Na2 46.05(5) . . ? 
F3 Ga1 Na2 117.73(4) 3 . ? 
F3 Ga1 Na2 62.27(4) . . ? 
F1 Ga1 Na2 124.51(4) 3 3 ? 
F1 Ga1 Na2 55.49(4) . 3 ? 
F2 Ga1 Na2 46.05(5) 3 3 ? 
F2 Ga1 Na2 133.95(5) . 3 ? 
F3 Ga1 Na2 62.27(4) 3 3 ? 
F3 Ga1 Na2 117.73(4) . 3 ? 
Na2 Ga1 Na2 180.00(2) . 3 ? 
F1 Ga1 Na2 42.71(4) 3 2_445 ? 
F1 Ga1 Na2 137.29(4) . 2_445 ? 
F2 Ga1 Na2 106.27(4) 3 2_445 ? 
F2 Ga1 Na2 73.73(4) . 2_445 ? 
F3 Ga1 Na2 51.17(4) 3 2_445 ? 
F3 Ga1 Na2 128.83(4) . 2_445 ? 
Na2 Ga1 Na2 71.750(19) . 2_445 ? 
Na2 Ga1 Na2 108.250(19) 3 2_445 ? 
F1 Ga1 Na2 137.29(4) 3 4_665 ? 
F1 Ga1 Na2 42.71(4) . 4_665 ? 
F2 Ga1 Na2 73.73(4) 3 4_665 ? 
F2 Ga1 Na2 106.27(4) . 4_665 ? 
F3 Ga1 Na2 128.83(4) 3 4_665 ? 
F3 Ga1 Na2 51.17(4) . 4_665 ? 
Na2 Ga1 Na2 108.250(19) . 4_665 ? 
Na2 Ga1 Na2 71.750(19) 3 4_665 ? 
Na2 Ga1 Na2 180.00(4) 2_445 4_665 ? 
F1 Ga1 Na2 52.94(4) 3 4_565 ? 
F1 Ga1 Na2 127.06(4) . 4_565 ? 
F2 Ga1 Na2 39.10(5) 3 4_565 ? 
F2 Ga1 Na2 140.90(5) . 4_565 ? 
F3 Ga1 Na2 80.97(4) 3 4_565 ? 
F3 Ga1 Na2 99.03(4) . 4_565 ? 
Na2 Ga1 Na2 104.97(2) . 4_565 ? 
Na2 Ga1 Na2 75.03(2) 3 4_565 ? 
Na2 Ga1 Na2 71.58(2) 2_445 4_565 ? 
Na2 Ga1 Na2 108.42(2) 4_665 4_565 ? 
F1 Ga1 Na2 127.06(4) 3 2_545 ? 
F1 Ga1 Na2 52.94(4) . 2_545 ? 
F2 Ga1 Na2 140.90(5) 3 2_545 ? 
F2 Ga1 Na2 39.10(5) . 2_545 ? 
F3 Ga1 Na2 99.03(4) 3 2_545 ? 
F3 Ga1 Na2 80.97(4) . 2_545 ? 
Na2 Ga1 Na2 75.03(2) . 2_545 ? 
Na2 Ga1 Na2 104.97(2) 3 2_545 ? 
Na2 Ga1 Na2 108.42(2) 2_445 2_545 ? 
Na2 Ga1 Na2 71.58(2) 4_665 2_545 ? 
Na2 Ga1 Na2 180.00(5) 4_565 2_545 ? 
Ga1 F1 Na1 147.04(6) . . ? 
Ga1 F1 Na2 103.86(6) . 4_665 ? 
Na1 F1 Na2 109.10(6) . 4_665 ? 
Ga1 F1 Na2 88.84(5) . 3 ? 
Na1 F1 Na2 85.40(5) . 3 ? 
Na2 F1 Na2 100.60(5) 4_665 3 ? 
Ga1 F1 Na2 93.84(5) . 2_545 ? 
Na1 F1 Na2 79.24(4) . 2_545 ? 
Na2 F1 Na2 102.18(5) 4_665 2_545 ? 
Na2 F1 Na2 155.68(6) 3 2_545 ? 
Ga1 F2 Na1 141.80(7) . 2 ? 
Ga1 F2 Na2 109.57(7) . 2_545 ? 
Na1 F2 Na2 98.79(5) 2 2_545 ? 
Ga1 F2 Na2 98.53(6) . . ? 
Na1 F2 Na2 87.18(5) 2 . ? 
Na2 F2 Na2 121.69(7) 2_545 . ? 
Ga1 F3 Na1 141.09(6) . 1_565 ? 
Ga1 F3 Na2 125.37(6) . 3_565 ? 
Na1 F3 Na2 93.00(5) 1_565 3_565 ? 
Ga1 F3 Na2 94.16(5) . 4_665 ? 
Na1 F3 Na2 81.55(5) 1_565 4_665 ? 
Na2 F3 Na2 103.07(5) 3_565 4_665 ? 
Ga1 F3 Na2 82.23(5) . . ? 
Na1 F3 Na2 83.61(4) 1_565 . ? 
Na2 F3 Na2 102.15(5) 3_565 . ? 
Na2 F3 Na2 151.27(6) 4_665 . ? 
 
_diffrn_measured_fraction_theta_max    1.000 
_diffrn_reflns_theta_full              27.50 
_diffrn_measured_fraction_theta_full   1.000 
_refine_diff_density_max    0.329 
_refine_diff_density_min   -1.077 
_refine_diff_density_rms    0.163 
