# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2017

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_shelxl
_database_code_depnum_ccdc_archive 'CCDC 1523304'
_audit_update_record             
;
2016-12-19 deposited with the CCDC.
2017-03-07 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C32 H28 O6'
_chemical_formula_weight         508.54

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Triclinic
_symmetry_space_group_name_H-M   P-1

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   7.5291(15)
_cell_length_b                   9.914(2)
_cell_length_c                   17.893(4)
_cell_angle_alpha                81.02(3)
_cell_angle_beta                 83.55(3)
_cell_angle_gamma                75.21(3)
_cell_volume                     1271.8(4)
_cell_formula_units_Z            2
_cell_measurement_temperature    113(2)
_cell_measurement_reflns_used    3878
_cell_measurement_theta_min      2.1436
_cell_measurement_theta_max      27.8465

_exptl_crystal_description       ?
_exptl_crystal_colour            ?
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.12
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.328
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             536
_exptl_absorpt_coefficient_mu    0.091
_exptl_absorpt_correction_type   MULTI-SCAN
_exptl_absorpt_correction_T_min  0.9820
_exptl_absorpt_correction_T_max  0.9891
_exptl_absorpt_process_details   crystalclear

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      113(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_monochromator  confocal
_diffrn_measurement_device_type  'rigaku saturn'
_diffrn_measurement_method       'ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_decay_%        0
_diffrn_reflns_number            12764
_diffrn_reflns_av_R_equivalents  0.0331
_diffrn_reflns_av_sigmaI/netI    0.0646
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         2.30
_diffrn_reflns_theta_max         27.86
_reflns_number_total             5947
_reflns_number_gt                3500
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       crystalclear
_computing_cell_refinement       crystalclear
_computing_data_reduction        crystalclear
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0310P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    CONSTR
_refine_ls_extinction_method     SHELXL
_refine_ls_extinction_coef       0.047(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_number_reflns         5947
_refine_ls_number_parameters     348
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0659
_refine_ls_R_factor_gt           0.0378
_refine_ls_wR_factor_ref         0.0855
_refine_ls_wR_factor_gt          0.0788
_refine_ls_goodness_of_fit_ref   1.072
_refine_ls_restrained_S_all      1.072
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
O1 O 0.21891(12) 0.14800(11) 0.74499(5) 0.0267(2) Uani 1 1 d . . .
O2 O 1.03404(12) -0.01179(10) 0.59548(5) 0.0262(2) Uani 1 1 d . . .
O3 O 0.24402(12) 0.41982(11) 0.62694(5) 0.0301(3) Uani 1 1 d . . .
O4 O -0.59615(11) 0.70769(11) 0.59847(5) 0.0253(2) Uani 1 1 d . . .
O5 O -0.05713(13) 0.92299(11) 0.92293(6) 0.0300(3) Uani 1 1 d . . .
O6 O 0.57933(13) 0.26332(11) 1.07050(5) 0.0301(3) Uani 1 1 d . . .
C1 C 0.30595(16) 0.33918(14) 0.78163(7) 0.0175(3) Uani 1 1 d . . .
C2 C 0.34225(18) 0.20972(15) 0.74180(7) 0.0189(3) Uani 1 1 d . . .
C3 C 0.52773(17) 0.15390(15) 0.70544(7) 0.0174(3) Uani 1 1 d . . .
C4 C 0.65737(17) 0.23445(15) 0.68975(7) 0.0213(3) Uani 1 1 d . . .
H4 H 0.6280 0.3261 0.7045 0.026 Uiso 1 1 calc R . .
C5 C 0.82847(17) 0.18392(15) 0.65311(8) 0.0213(3) Uani 1 1 d . . .
H5 H 0.9155 0.2403 0.6426 0.026 Uiso 1 1 calc R . .
C6 C 0.87065(17) 0.04948(15) 0.63201(7) 0.0190(3) Uani 1 1 d . . .
C7 C 0.74344(17) -0.03317(15) 0.64781(7) 0.0212(3) Uani 1 1 d . . .
H7 H 0.7734 -0.1253 0.6338 0.025 Uiso 1 1 calc R . .
C8 C 0.57361(18) 0.01927(15) 0.68392(7) 0.0195(3) Uani 1 1 d . . .
H8 H 0.4867 -0.0371 0.6943 0.023 Uiso 1 1 calc R . .
C9 C 1.16096(18) 0.07491(16) 0.56967(9) 0.0295(4) Uani 1 1 d . . .
H9A H 1.1022 0.1558 0.5344 0.044 Uiso 1 1 calc R . .
H9B H 1.2709 0.0199 0.5437 0.044 Uiso 1 1 calc R . .
H9C H 1.1964 0.1082 0.6132 0.044 Uiso 1 1 calc R . .
C10 C 0.19451(17) 0.46299(14) 0.75466(7) 0.0174(3) Uani 1 1 d . . .
C11 C 0.13423(17) 0.47452(14) 0.67609(7) 0.0196(3) Uani 1 1 d . . .
C12 C -0.05805(17) 0.54551(14) 0.65794(7) 0.0171(3) Uani 1 1 d . . .
C13 C -0.20710(17) 0.57153(14) 0.71247(7) 0.0192(3) Uani 1 1 d . . .
H13 H -0.1863 0.5518 0.7649 0.023 Uiso 1 1 calc R . .
C14 C -0.38422(17) 0.62567(15) 0.69043(7) 0.0198(3) Uani 1 1 d . . .
H14 H -0.4844 0.6436 0.7278 0.024 Uiso 1 1 calc R . .
C15 C -0.41682(17) 0.65418(14) 0.61369(7) 0.0182(3) Uani 1 1 d . . .
C16 C -0.27111(17) 0.62997(14) 0.55856(7) 0.0197(3) Uani 1 1 d . . .
H16 H -0.2924 0.6491 0.5062 0.024 Uiso 1 1 calc R . .
C17 C -0.09437(17) 0.57746(14) 0.58156(7) 0.0198(3) Uani 1 1 d . . .
H17 H 0.0059 0.5626 0.5440 0.024 Uiso 1 1 calc R . .
C18 C -0.64040(19) 0.72127(17) 0.52120(8) 0.0289(4) Uani 1 1 d . . .
H18A H -0.5756 0.7862 0.4893 0.043 Uiso 1 1 calc R . .
H18B H -0.7736 0.7580 0.5182 0.043 Uiso 1 1 calc R . .
H18C H -0.6022 0.6289 0.5033 0.043 Uiso 1 1 calc R . .
C19 C 0.12810(16) 0.58559(14) 0.79744(7) 0.0172(3) Uani 1 1 d . . .
C20 C 0.07336(17) 0.56846(15) 0.87537(7) 0.0211(3) Uani 1 1 d . . .
H20 H 0.0791 0.4764 0.9013 0.025 Uiso 1 1 calc R . .
C21 C 0.01163(17) 0.68219(15) 0.91487(8) 0.0230(3) Uani 1 1 d . . .
H21 H -0.0240 0.6679 0.9676 0.028 Uiso 1 1 calc R . .
C22 C 0.00111(17) 0.81824(15) 0.87787(8) 0.0200(3) Uani 1 1 d . . .
C23 C 0.04931(16) 0.83880(15) 0.80044(8) 0.0194(3) Uani 1 1 d . . .
H23 H 0.0394 0.9313 0.7744 0.023 Uiso 1 1 calc R . .
C24 C 0.11230(16) 0.72258(14) 0.76119(7) 0.0185(3) Uani 1 1 d . . .
H24 H 0.1453 0.7373 0.7083 0.022 Uiso 1 1 calc R . .
C25 C -0.0983(2) 1.06492(16) 0.88657(9) 0.0341(4) Uani 1 1 d . . .
H25A H 0.0088 1.0822 0.8535 0.051 Uiso 1 1 calc R . .
H25B H -0.1278 1.1292 0.9251 0.051 Uiso 1 1 calc R . .
H25C H -0.2040 1.0809 0.8562 0.051 Uiso 1 1 calc R . .
C26 C 0.38810(16) 0.31156(15) 0.85627(7) 0.0176(3) Uani 1 1 d . . .
C27 C 0.34607(17) 0.20769(14) 0.91224(7) 0.0197(3) Uani 1 1 d . . .
H27 H 0.2737 0.1489 0.9008 0.024 Uiso 1 1 calc R . .
C28 C 0.40744(17) 0.18775(15) 0.98461(7) 0.0206(3) Uani 1 1 d . . .
H28 H 0.3749 0.1176 1.0224 0.025 Uiso 1 1 calc R . .
C29 C 0.51610(17) 0.27090(15) 1.00099(7) 0.0205(3) Uani 1 1 d . . .
C30 C 0.56685(17) 0.37094(15) 0.94483(8) 0.0226(3) Uani 1 1 d . . .
H30 H 0.6464 0.4250 0.9554 0.027 Uiso 1 1 calc R . .
C31 C 0.50180(17) 0.39178(15) 0.87377(8) 0.0213(3) Uani 1 1 d . . .
H31 H 0.5349 0.4619 0.8362 0.026 Uiso 1 1 calc R . .
C32 C 0.5137(2) 0.17450(17) 1.13211(8) 0.0307(4) Uani 1 1 d . . .
H32A H 0.3795 0.2069 1.1402 0.046 Uiso 1 1 calc R . .
H32B H 0.5706 0.1780 1.1782 0.046 Uiso 1 1 calc R . .
H32C H 0.5457 0.0776 1.1203 0.046 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O1 C2 1.2277(16) . ?
O2 C6 1.3680(16) . ?
O2 C9 1.4357(17) . ?
O3 C11 1.2279(16) . ?
O4 C15 1.3604(15) . ?
O4 C18 1.4363(16) . ?
O5 C22 1.3677(17) . ?
O5 C25 1.4270(17) . ?
O6 C29 1.3655(16) . ?
O6 C32 1.4254(17) . ?
C1 C10 1.3505(18) . ?
C1 C26 1.4921(18) . ?
C1 C2 1.5141(19) . ?
C2 C3 1.4811(18) . ?
C3 C4 1.3912(19) . ?
C3 C8 1.3944(19) . ?
C4 C5 1.3869(18) . ?
C4 H4 0.9500 . ?
C5 C6 1.3907(19) . ?
C5 H5 0.9500 . ?
C6 C7 1.3915(19) . ?
C7 C8 1.3793(18) . ?
C7 H7 0.9500 . ?
C8 H8 0.9500 . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
C10 C19 1.4857(19) . ?
C10 C11 1.5040(18) . ?
C11 C12 1.4868(18) . ?
C12 C17 1.3956(18) . ?
C12 C13 1.4009(18) . ?
C13 C14 1.3815(18) . ?
C13 H13 0.9500 . ?
C14 C15 1.3944(18) . ?
C14 H14 0.9500 . ?
C15 C16 1.3895(18) . ?
C16 C17 1.3834(18) . ?
C16 H16 0.9500 . ?
C17 H17 0.9500 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C24 1.3925(19) . ?
C19 C20 1.4057(18) . ?
C20 C21 1.376(2) . ?
C20 H20 0.9500 . ?
C21 C22 1.3936(19) . ?
C21 H21 0.9500 . ?
C22 C23 1.3889(18) . ?
C23 C24 1.3945(19) . ?
C23 H23 0.9500 . ?
C24 H24 0.9500 . ?
C25 H25A 0.9800 . ?
C25 H25B 0.9800 . ?
C25 H25C 0.9800 . ?
C26 C27 1.3916(18) . ?
C26 C31 1.3961(19) . ?
C27 C28 1.3919(18) . ?
C27 H27 0.9500 . ?
C28 C29 1.3815(19) . ?
C28 H28 0.9500 . ?
C29 C30 1.3912(19) . ?
C30 C31 1.3803(19) . ?
C30 H30 0.9500 . ?
C31 H31 0.9500 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 H32C 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C6 O2 C9 117.24(11) . . ?
C15 O4 C18 117.63(11) . . ?
C22 O5 C25 117.74(11) . . ?
C29 O6 C32 117.88(11) . . ?
C10 C1 C26 124.11(13) . . ?
C10 C1 C2 122.14(12) . . ?
C26 C1 C2 113.44(12) . . ?
O1 C2 C3 121.44(13) . . ?
O1 C2 C1 118.43(12) . . ?
C3 C2 C1 119.95(12) . . ?
C4 C3 C8 118.50(13) . . ?
C4 C3 C2 121.56(13) . . ?
C8 C3 C2 119.92(12) . . ?
C5 C4 C3 121.45(14) . . ?
C5 C4 H4 119.3 . . ?
C3 C4 H4 119.3 . . ?
C4 C5 C6 118.94(13) . . ?
C4 C5 H5 120.5 . . ?
C6 C5 H5 120.5 . . ?
O2 C6 C5 124.43(12) . . ?
O2 C6 C7 115.11(13) . . ?
C5 C6 C7 120.46(12) . . ?
C8 C7 C6 119.73(14) . . ?
C8 C7 H7 120.1 . . ?
C6 C7 H7 120.1 . . ?
C7 C8 C3 120.92(13) . . ?
C7 C8 H8 119.5 . . ?
C3 C8 H8 119.5 . . ?
O2 C9 H9A 109.5 . . ?
O2 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
O2 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C1 C10 C19 124.45(12) . . ?
C1 C10 C11 116.68(13) . . ?
C19 C10 C11 118.87(12) . . ?
O3 C11 C12 119.54(12) . . ?
O3 C11 C10 119.30(12) . . ?
C12 C11 C10 121.11(12) . . ?
C17 C12 C13 118.01(12) . . ?
C17 C12 C11 117.64(12) . . ?
C13 C12 C11 124.13(12) . . ?
C14 C13 C12 120.35(12) . . ?
C14 C13 H13 119.8 . . ?
C12 C13 H13 119.8 . . ?
C13 C14 C15 120.40(12) . . ?
C13 C14 H14 119.8 . . ?
C15 C14 H14 119.8 . . ?
O4 C15 C16 124.25(12) . . ?
O4 C15 C14 115.44(12) . . ?
C16 C15 C14 120.30(12) . . ?
C17 C16 C15 118.57(12) . . ?
C17 C16 H16 120.7 . . ?
C15 C16 H16 120.7 . . ?
C16 C17 C12 122.35(12) . . ?
C16 C17 H17 118.8 . . ?
C12 C17 H17 118.8 . . ?
O4 C18 H18A 109.5 . . ?
O4 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
O4 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C24 C19 C20 117.36(13) . . ?
C24 C19 C10 121.11(12) . . ?
C20 C19 C10 121.51(13) . . ?
C21 C20 C19 121.41(13) . . ?
C21 C20 H20 119.3 . . ?
C19 C20 H20 119.3 . . ?
C20 C21 C22 120.29(13) . . ?
C20 C21 H21 119.9 . . ?
C22 C21 H21 119.9 . . ?
O5 C22 C23 124.98(13) . . ?
O5 C22 C21 115.40(12) . . ?
C23 C22 C21 119.62(14) . . ?
C22 C23 C24 119.45(13) . . ?
C22 C23 H23 120.3 . . ?
C24 C23 H23 120.3 . . ?
C19 C24 C23 121.82(13) . . ?
C19 C24 H24 119.1 . . ?
C23 C24 H24 119.1 . . ?
O5 C25 H25A 109.5 . . ?
O5 C25 H25B 109.5 . . ?
H25A C25 H25B 109.5 . . ?
O5 C25 H25C 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C27 C26 C31 117.81(12) . . ?
C27 C26 C1 120.31(12) . . ?
C31 C26 C1 121.82(12) . . ?
C26 C27 C28 121.62(13) . . ?
C26 C27 H27 119.2 . . ?
C28 C27 H27 119.2 . . ?
C29 C28 C27 119.35(13) . . ?
C29 C28 H28 120.3 . . ?
C27 C28 H28 120.3 . . ?
O6 C29 C28 124.31(12) . . ?
O6 C29 C30 115.74(12) . . ?
C28 C29 C30 119.95(13) . . ?
C31 C30 C29 120.10(13) . . ?
C31 C30 H30 120.0 . . ?
C29 C30 H30 120.0 . . ?
C30 C31 C26 121.07(13) . . ?
C30 C31 H31 119.5 . . ?
C26 C31 H31 119.5 . . ?
O6 C32 H32A 109.5 . . ?
O6 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
O6 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C10 C1 C2 O1 -72.93(17) . . . . ?
C26 C1 C2 O1 100.95(14) . . . . ?
C10 C1 C2 C3 111.89(14) . . . . ?
C26 C1 C2 C3 -74.24(15) . . . . ?
O1 C2 C3 C4 168.55(13) . . . . ?
C1 C2 C3 C4 -16.41(18) . . . . ?
O1 C2 C3 C8 -9.40(19) . . . . ?
C1 C2 C3 C8 165.65(12) . . . . ?
C8 C3 C4 C5 0.4(2) . . . . ?
C2 C3 C4 C5 -177.53(12) . . . . ?
C3 C4 C5 C6 -0.2(2) . . . . ?
C9 O2 C6 C5 -7.52(19) . . . . ?
C9 O2 C6 C7 172.60(12) . . . . ?
C4 C5 C6 O2 179.79(12) . . . . ?
C4 C5 C6 C7 -0.3(2) . . . . ?
O2 C6 C7 C8 -179.42(11) . . . . ?
C5 C6 C7 C8 0.7(2) . . . . ?
C6 C7 C8 C3 -0.5(2) . . . . ?
C4 C3 C8 C7 -0.1(2) . . . . ?
C2 C3 C8 C7 177.93(11) . . . . ?
C26 C1 C10 C19 -4.3(2) . . . . ?
C2 C1 C10 C19 168.93(12) . . . . ?
C26 C1 C10 C11 176.25(11) . . . . ?
C2 C1 C10 C11 -10.55(18) . . . . ?
C1 C10 C11 O3 -38.34(18) . . . . ?
C19 C10 C11 O3 142.15(13) . . . . ?
C1 C10 C11 C12 138.98(13) . . . . ?
C19 C10 C11 C12 -40.53(18) . . . . ?
O3 C11 C12 C17 -15.4(2) . . . . ?
C10 C11 C12 C17 167.26(13) . . . . ?
O3 C11 C12 C13 159.01(14) . . . . ?
C10 C11 C12 C13 -18.3(2) . . . . ?
C17 C12 C13 C14 0.7(2) . . . . ?
C11 C12 C13 C14 -173.67(13) . . . . ?
C12 C13 C14 C15 0.4(2) . . . . ?
C18 O4 C15 C16 9.19(19) . . . . ?
C18 O4 C15 C14 -171.86(13) . . . . ?
C13 C14 C15 O4 -179.77(12) . . . . ?
C13 C14 C15 C16 -0.8(2) . . . . ?
O4 C15 C16 C17 178.83(12) . . . . ?
C14 C15 C16 C17 -0.1(2) . . . . ?
C15 C16 C17 C12 1.3(2) . . . . ?
C13 C12 C17 C16 -1.6(2) . . . . ?
C11 C12 C17 C16 173.15(13) . . . . ?
C1 C10 C19 C24 141.78(13) . . . . ?
C11 C10 C19 C24 -38.75(17) . . . . ?
C1 C10 C19 C20 -40.24(19) . . . . ?
C11 C10 C19 C20 139.23(13) . . . . ?
C24 C19 C20 C21 -1.85(19) . . . . ?
C10 C19 C20 C21 -179.90(12) . . . . ?
C19 C20 C21 C22 0.3(2) . . . . ?
C25 O5 C22 C23 9.96(19) . . . . ?
C25 O5 C22 C21 -170.35(12) . . . . ?
C20 C21 C22 O5 -178.24(12) . . . . ?
C20 C21 C22 C23 1.5(2) . . . . ?
O5 C22 C23 C24 177.98(12) . . . . ?
C21 C22 C23 C24 -1.70(19) . . . . ?
C20 C19 C24 C23 1.60(18) . . . . ?
C10 C19 C24 C23 179.66(11) . . . . ?
C22 C23 C24 C19 0.15(19) . . . . ?
C10 C1 C26 C27 118.28(15) . . . . ?
C2 C1 C26 C27 -55.45(16) . . . . ?
C10 C1 C26 C31 -58.83(18) . . . . ?
C2 C1 C26 C31 127.44(13) . . . . ?
C31 C26 C27 C28 2.94(19) . . . . ?
C1 C26 C27 C28 -174.29(12) . . . . ?
C26 C27 C28 C29 -1.4(2) . . . . ?
C32 O6 C29 C28 -6.8(2) . . . . ?
C32 O6 C29 C30 172.78(12) . . . . ?
C27 C28 C29 O6 177.99(12) . . . . ?
C27 C28 C29 C30 -1.6(2) . . . . ?
O6 C29 C30 C31 -176.60(12) . . . . ?
C28 C29 C30 C31 3.0(2) . . . . ?
C29 C30 C31 C26 -1.5(2) . . . . ?
C27 C26 C31 C30 -1.5(2) . . . . ?
C1 C26 C31 C30 175.70(12) . . . . ?

_diffrn_measured_fraction_theta_max 0.982
_diffrn_reflns_theta_full        27.86
_diffrn_measured_fraction_theta_full 0.982
_refine_diff_density_max         0.280
_refine_diff_density_min         -0.254
_refine_diff_density_rms         0.048
