# Electronic Supplementary Material (ESI) for Chemical Communications.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_xxx_sq_sq
_database_code_depnum_ccdc_archive 'CCDC 1820449'
_audit_update_record             
;
2018-01-30 deposited with the CCDC.
2018-04-03 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         
;
C128 H288 Ag40.13 Cu13.87 O36 S51, C128 H288 Ag40.09 Cu13.91 O36 S51 [+ solvent]
;
_chemical_formula_sum            
'C256 H576 Ag80.22 Cu27.78 O72 S102 [+ solvent]'
_chemical_formula_weight         18497.50

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   21.0609(18)
_cell_length_b                   22.3168(12)
_cell_length_c                   34.112(2)
_cell_angle_alpha                79.041(2)
_cell_angle_beta                 78.4307(15)
_cell_angle_gamma                71.641(2)
_cell_volume                     14768.1(18)
_cell_formula_units_Z            1
_cell_measurement_temperature    130(2)
_cell_measurement_reflns_used    9874
_cell_measurement_theta_min      2.64
_cell_measurement_theta_max      22.61

_exptl_crystal_description       block
_exptl_crystal_colour            red
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.080
_exptl_crystal_F_000             8897
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.180
_exptl_absorpt_coefficient_mu    3.966
_shelx_estimated_absorpt_T_min   0.437
_shelx_estimated_absorpt_T_max   0.535
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.44
_exptl_absorpt_correction_T_max  0.54
_exptl_absorpt_process_details   'SADABS; Bruker, 2008'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      130(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            121300
_diffrn_reflns_av_unetI/netI     0.0887
_diffrn_reflns_av_R_equivalents  0.0650
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_limit_l_max       43
_diffrn_reflns_theta_min         0.615
_diffrn_reflns_theta_max         27.000
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measured_fraction_theta_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.985
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.985
_diffrn_reflns_point_group_measured_fraction_full 0.994
_reflns_number_total             63566
_reflns_number_gt                34948
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'SMART (Bruker, 2008)'
_computing_cell_refinement       SMART
_computing_data_reduction        'SAINT (Bruker, 2008)'
_computing_structure_solution    'SHELXTL (Bruker, 2008)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    'SHELXTL (Bruker, 2008)'
_computing_publication_material  'SHELXTL (Bruker, 2008)'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           fullcycle
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0200P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         63566
_refine_ls_number_parameters     2520
_refine_ls_number_restraints     1
_refine_ls_R_factor_all          0.0843
_refine_ls_R_factor_gt           0.0390
_refine_ls_wR_factor_ref         0.0800
_refine_ls_wR_factor_gt          0.0771
_refine_ls_goodness_of_fit_ref   1.006
_refine_ls_restrained_S_all      1.006
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.67308(3) 0.65948(2) -0.00067(2) 0.07430(15) Uani 1 1 d . . . . .
Ag2 Ag 0.77879(2) 0.51554(2) 0.00411(2) 0.06563(14) Uani 1 1 d . . . . .
Ag3 Ag 0.68101(2) 0.65809(2) -0.09789(2) 0.05664(12) Uani 1 1 d . . . . .
Ag4 Ag 0.54984(2) 0.75792(2) -0.01638(2) 0.05104(11) Uani 1 1 d . . . . .
Ag5 Ag 0.40311(2) 0.77312(2) -0.04307(2) 0.06185(13) Uani 1 1 d . . . . .
Ag6 Ag 0.33757(2) 0.75762(2) 0.05261(2) 0.05061(11) Uani 1 1 d . . . . .
Ag7 Ag 0.49541(2) 0.74039(2) -0.11522(2) 0.05699(12) Uani 1 1 d . . . . .
Ag8 Ag 0.61624(2) 0.61976(2) -0.15240(2) 0.06732(14) Uani 1 1 d . . . . .
Ag9 Ag 0.50001(2) 0.57240(2) -0.17922(2) 0.05716(12) Uani 1 1 d . . . . .
Ag10 Ag 0.78635(2) 0.37747(2) 0.02148(2) 0.06645(14) Uani 1 1 d . . . . .
Ag11 Ag 0.71965(2) 0.25676(2) 0.04493(2) 0.06243(14) Uani 1 1 d . . . . .
Ag12 Ag 0.71612(2) 0.42294(2) 0.10841(2) 0.05553(12) Uani 1 1 d . . . . .
Ag13 Ag 0.59183(2) 0.50589(2) 0.14828(2) 0.06542(14) Uani 1 1 d . . . . .
Ag14 Ag 0.65211(2) 0.60923(2) 0.08587(2) 0.05425(12) Uani 1 1 d . . . . .
Ag15 Ag 0.44055(2) 0.61308(2) 0.15783(2) 0.05661(12) Uani 1 1 d . . . . .
Ag16 Ag 0.31328(2) 0.51327(2) 0.16113(2) 0.05174(11) Uani 1 1 d . . . . .
Ag17 Ag 0.31962(2) 0.65704(2) 0.11813(2) 0.06211(13) Uani 1 1 d . . . . .
Ag18 Ag 0.21329(2) 0.65638(2) 0.05790(2) 0.05700(12) Uani 1 1 d . . . . .
Ag19 Ag 0.64907(2) 0.46086(2) -0.01170(2) 0.07232(15) Uani 1 1 d . . . . .
Ag20 Ag 0.63005(3) 0.31553(2) 0.13224(2) 0.0599(2) Uani 0.532(4) 1 d . . P A 1
Ag21 Ag 0.22934(3) 0.49855(2) 0.09048(2) 0.0579(2) Uani 0.533(4) 1 d . . P B 1
Cu7A Cu 0.63005(3) 0.31553(2) 0.13224(2) 0.0599(2) Uani 0.468(4) 1 d . . P A 1
Cu8A Cu 0.22934(3) 0.49855(2) 0.09048(2) 0.0579(2) Uani 0.467(4) 1 d . . P B 1
Cu1A Cu 0.44621(4) 0.63118(3) -0.04245(3) 0.0642(2) Uani 1 1 d . . . . .
Cu2A Cu 0.59141(3) 0.56386(3) -0.07086(3) 0.0624(2) Uani 1 1 d . . . . .
Cu3A Cu 0.43308(3) 0.59921(3) 0.05578(3) 0.0652(2) Uani 1 1 d . . . . .
Cu4A Cu 0.57648(3) 0.58436(3) 0.02275(3) 0.0562(2) Uani 1 1 d . . . . .
Cu5A Cu 0.49539(3) 0.71662(3) 0.08233(2) 0.05073(19) Uani 1 1 d . . . . .
Cu6A Cu 0.42741(4) 0.52979(3) -0.07531(3) 0.0714(2) Uani 1 1 d . . . . .
C1A C 0.8734(3) 0.6804(2) -0.0564(2) 0.0599(18) Uani 1 1 d . . . . .
C2A C 0.8564(3) 0.7464(2) -0.07947(19) 0.0578(17) Uani 1 1 d . . . . .
H2A1 H 0.8904 0.7484 -0.1035 0.087 Uiso 1 1 calc R U . . .
H2A2 H 0.8558 0.7772 -0.0623 0.087 Uiso 1 1 calc R U . . .
H2A3 H 0.8117 0.7567 -0.0877 0.087 Uiso 1 1 calc R U . . .
C3A C 0.8902(3) 0.6880(3) -0.01696(19) 0.0592(17) Uani 1 1 d . . . . .
H3A1 H 0.9028 0.6462 -0.0005 0.089 Uiso 1 1 calc R U . . .
H3A2 H 0.8506 0.7162 -0.0024 0.089 Uiso 1 1 calc R U . . .
H3A3 H 0.9280 0.7065 -0.0224 0.089 Uiso 1 1 calc R U . . .
C4A C 0.9382(2) 0.6423(2) -0.0777(2) 0.073(2) Uani 1 1 d . . . . .
H4AA H 0.9745 0.6608 -0.0773 0.109 Uiso 1 1 calc R U . . .
H4AB H 0.9334 0.6427 -0.1058 0.109 Uiso 1 1 calc R U . . .
H4AC H 0.9494 0.5982 -0.0641 0.109 Uiso 1 1 calc R U . . .
C5A C 0.3784(3) 0.9688(2) 0.0014(2) 0.0572(17) Uani 1 1 d . . . . .
C6A C 0.3032(3) 0.9929(2) -0.0023(2) 0.075(2) Uani 1 1 d . . . . .
H6A1 H 0.2884 1.0396 -0.0052 0.112 Uiso 1 1 calc R U . . .
H6A2 H 0.2772 0.9759 0.0220 0.112 Uiso 1 1 calc R U . . .
H6A3 H 0.2957 0.9788 -0.0260 0.112 Uiso 1 1 calc R U . . .
C7A C 0.3992(2) 0.9867(2) 0.03910(19) 0.0584(17) Uani 1 1 d . . . . .
H7A1 H 0.4478 0.9821 0.0342 0.088 Uiso 1 1 calc R U . . .
H7A2 H 0.3884 0.9582 0.0634 0.088 Uiso 1 1 calc R U . . .
H7A3 H 0.3740 1.0309 0.0428 0.088 Uiso 1 1 calc R U . . .
C8A C 0.4238(3) 0.9913(2) -0.0367(2) 0.0625(18) Uani 1 1 d . . . . .
H8A1 H 0.4152 1.0375 -0.0393 0.094 Uiso 1 1 calc R U . . .
H8A2 H 0.4134 0.9803 -0.0607 0.094 Uiso 1 1 calc R U . . .
H8A3 H 0.4715 0.9701 -0.0342 0.094 Uiso 1 1 calc R U . . .
C9A C 0.5513(3) 0.7626(2) -0.2641(2) 0.0603(17) Uani 1 1 d . . . . .
C10A C 0.4802(3) 0.8090(2) -0.2713(2) 0.0581(16) Uani 1 1 d . . . . .
H10A H 0.4577 0.8282 -0.2467 0.087 Uiso 1 1 calc R U . . .
H10B H 0.4527 0.7853 -0.2779 0.087 Uiso 1 1 calc R U . . .
H10C H 0.4858 0.8426 -0.2936 0.087 Uiso 1 1 calc R U . . .
C11A C 0.5905(3) 0.7157(3) -0.2923(2) 0.077(2) Uani 1 1 d . . . . .
H11A H 0.5627 0.6891 -0.2949 0.116 Uiso 1 1 calc R U . . .
H11B H 0.6028 0.7385 -0.3189 0.116 Uiso 1 1 calc R U . . .
H11C H 0.6316 0.6886 -0.2817 0.116 Uiso 1 1 calc R U . . .
C12A C 0.5962(2) 0.8008(2) -0.26172(17) 0.0426(13) Uani 1 1 d . . . . .
H12A H 0.6308 0.7755 -0.2450 0.064 Uiso 1 1 calc R U . . .
H12B H 0.5694 0.8393 -0.2496 0.064 Uiso 1 1 calc R U . . .
H12C H 0.6182 0.8131 -0.2889 0.064 Uiso 1 1 calc R U . . .
C13A C 0.9021(3) 0.2390(2) 0.11394(19) 0.0564(16) Uani 1 1 d . . . . .
C14A C 0.9180(3) 0.2882(2) 0.13492(19) 0.0588(17) Uani 1 1 d . . . . .
H14A H 0.9277 0.3228 0.1145 0.088 Uiso 1 1 calc R U . . .
H14B H 0.8788 0.3057 0.1546 0.088 Uiso 1 1 calc R U . . .
H14C H 0.9574 0.2668 0.1487 0.088 Uiso 1 1 calc R U . . .
C15A C 0.9590(2) 0.2073(2) 0.0817(2) 0.0603(18) Uani 1 1 d . . . . .
H15A H 1.0000 0.1851 0.0939 0.090 Uiso 1 1 calc R U . . .
H15B H 0.9684 0.2399 0.0596 0.090 Uiso 1 1 calc R U . . .
H15C H 0.9447 0.1765 0.0711 0.090 Uiso 1 1 calc R U . . .
C16A C 0.8851(3) 0.1802(2) 0.1355(2) 0.0631(19) Uani 1 1 d . . . . .
H16A H 0.9252 0.1498 0.1457 0.095 Uiso 1 1 calc R U . . .
H16B H 0.8700 0.1609 0.1169 0.095 Uiso 1 1 calc R U . . .
H16C H 0.8488 0.1911 0.1582 0.095 Uiso 1 1 calc R U . . .
C17A C 0.6104(3) 0.6488(3) 0.2252(2) 0.0679(19) Uani 1 1 d . . . . .
C18A C 0.5854(3) 0.7206(3) 0.2229(2) 0.087(2) Uani 1 1 d . . . . .
H18A H 0.5371 0.7335 0.2336 0.131 Uiso 1 1 calc R U . . .
H18B H 0.5926 0.7400 0.1947 0.131 Uiso 1 1 calc R U . . .
H18C H 0.6105 0.7347 0.2389 0.131 Uiso 1 1 calc R U . . .
C19A C 0.6873(3) 0.6179(3) 0.2257(2) 0.080(2) Uani 1 1 d . . . . .
H19A H 0.6984 0.6205 0.2518 0.120 Uiso 1 1 calc R U . . .
H19B H 0.7127 0.6406 0.2040 0.120 Uiso 1 1 calc R U . . .
H19C H 0.6994 0.5731 0.2217 0.120 Uiso 1 1 calc R U . . .
C20A C 0.5733(3) 0.6209(3) 0.26411(19) 0.0605(17) Uani 1 1 d . . . . .
H20A H 0.6002 0.6122 0.2860 0.091 Uiso 1 1 calc R U . . .
H20B H 0.5667 0.5811 0.2600 0.091 Uiso 1 1 calc R U . . .
H20C H 0.5292 0.6514 0.2713 0.091 Uiso 1 1 calc R U . . .
C21A C 0.1070(3) 0.6827(2) 0.1996(2) 0.0592(17) Uani 1 1 d . . . . .
C22A C 0.1406(4) 0.6734(3) 0.2361(2) 0.088(2) Uani 1 1 d . . . . .
H22A H 0.1276 0.7137 0.2472 0.132 Uiso 1 1 calc R U . . .
H22B H 0.1899 0.6593 0.2284 0.132 Uiso 1 1 calc R U . . .
H22C H 0.1264 0.6410 0.2566 0.132 Uiso 1 1 calc R U . . .
C23A C 0.0489(3) 0.6511(3) 0.2032(2) 0.077(2) Uani 1 1 d . . . . .
H23A H 0.0315 0.6608 0.1774 0.116 Uiso 1 1 calc R U . . .
H23B H 0.0667 0.6048 0.2099 0.116 Uiso 1 1 calc R U . . .
H23C H 0.0122 0.6678 0.2245 0.116 Uiso 1 1 calc R U . . .
C24A C 0.0783(3) 0.7535(2) 0.18397(19) 0.0578(16) Uani 1 1 d . . . . .
H24A H 0.0431 0.7742 0.2047 0.087 Uiso 1 1 calc R U . . .
H24B H 0.0587 0.7576 0.1595 0.087 Uiso 1 1 calc R U . . .
H24C H 0.1146 0.7740 0.1777 0.087 Uiso 1 1 calc R U . . .
C25A C 0.6443(2) 0.78277(18) 0.05909(17) 0.0373(13) Uani 1 1 d . . . . .
C26A C 0.6570(2) 0.82425(18) 0.01826(16) 0.0384(13) Uani 1 1 d . . . . .
H26A H 0.6905 0.8457 0.0195 0.058 Uiso 1 1 calc R U . . .
H26B H 0.6145 0.8562 0.0126 0.058 Uiso 1 1 calc R U . . .
H26C H 0.6740 0.7972 -0.0033 0.058 Uiso 1 1 calc R U . . .
C27A C 0.7044(2) 0.7488(2) 0.07950(18) 0.0497(15) Uani 1 1 d . . . . .
H27A H 0.7210 0.7044 0.0741 0.074 Uiso 1 1 calc R U . . .
H27B H 0.6917 0.7497 0.1087 0.074 Uiso 1 1 calc R U . . .
H27C H 0.7401 0.7697 0.0692 0.074 Uiso 1 1 calc R U . . .
C28A C 0.5852(2) 0.8231(2) 0.08984(16) 0.0448(13) Uani 1 1 d . . . . .
H28A H 0.5613 0.7947 0.1078 0.067 Uiso 1 1 calc R U . . .
H28B H 0.5533 0.8566 0.0745 0.067 Uiso 1 1 calc R U . . .
H28C H 0.6051 0.8424 0.1059 0.067 Uiso 1 1 calc R U . . .
C29A C 0.3458(3) 0.7874(2) 0.15485(17) 0.0515(15) Uani 1 1 d . . . . .
C30A C 0.2814(2) 0.8263(2) 0.14215(17) 0.0474(15) Uani 1 1 d . . . . .
H30A H 0.2647 0.8649 0.1553 0.071 Uiso 1 1 calc R U . . .
H30B H 0.2484 0.8019 0.1498 0.071 Uiso 1 1 calc R U . . .
H30C H 0.2880 0.8382 0.1128 0.071 Uiso 1 1 calc R U . . .
C31A C 0.3981(3) 0.8155(2) 0.15783(19) 0.0569(16) Uani 1 1 d . . . . .
H31A H 0.3962 0.8532 0.1374 0.085 Uiso 1 1 calc R U . . .
H31B H 0.4426 0.7843 0.1533 0.085 Uiso 1 1 calc R U . . .
H31C H 0.3906 0.8280 0.1848 0.085 Uiso 1 1 calc R U . . .
C32A C 0.3307(3) 0.7493(2) 0.19870(16) 0.0468(14) Uani 1 1 d . . . . .
H32A H 0.3719 0.7342 0.2113 0.070 Uiso 1 1 calc R U . . .
H32B H 0.3162 0.7128 0.1962 0.070 Uiso 1 1 calc R U . . .
H32C H 0.2949 0.7776 0.2155 0.070 Uiso 1 1 calc R U . . .
C33A C 0.8291(2) 0.5253(2) 0.10173(17) 0.0404(13) Uani 1 1 d . . . . .
C34A C 0.8451(3) 0.5856(2) 0.0810(2) 0.077(2) Uani 1 1 d . . . . .
H34A H 0.8859 0.5752 0.0610 0.116 Uiso 1 1 calc R U . . .
H34B H 0.8526 0.6078 0.1010 0.116 Uiso 1 1 calc R U . . .
H34C H 0.8071 0.6130 0.0675 0.116 Uiso 1 1 calc R U . . .
C35A C 0.8846(2) 0.4616(2) 0.0977(2) 0.074(2) Uani 1 1 d . . . . .
H35A H 0.9153 0.4656 0.0723 0.111 Uiso 1 1 calc R U . . .
H35B H 0.8637 0.4280 0.0979 0.111 Uiso 1 1 calc R U . . .
H35C H 0.9101 0.4507 0.1204 0.111 Uiso 1 1 calc R U . . .
C36A C 0.7956(3) 0.5495(3) 0.14248(19) 0.0622(17) Uani 1 1 d . . . . .
H36A H 0.7809 0.5156 0.1612 0.093 Uiso 1 1 calc R U . . .
H36B H 0.8282 0.5616 0.1538 0.093 Uiso 1 1 calc R U . . .
H36C H 0.7563 0.5865 0.1384 0.093 Uiso 1 1 calc R U . . .
C37A C 0.6699(2) 0.1424(2) 0.13342(19) 0.0485(16) Uani 1 1 d . . . . .
C38A C 0.7312(2) 0.1060(2) 0.10681(19) 0.0585(16) Uani 1 1 d . . . . .
H38A H 0.7406 0.0603 0.1165 0.088 Uiso 1 1 calc R U . . .
H38B H 0.7704 0.1200 0.1079 0.088 Uiso 1 1 calc R U . . .
H38C H 0.7221 0.1143 0.0789 0.088 Uiso 1 1 calc R U . . .
C39A C 0.6179(3) 0.1056(2) 0.1434(2) 0.0598(17) Uani 1 1 d . . . . .
H39A H 0.5759 0.1322 0.1335 0.090 Uiso 1 1 calc R U . . .
H39B H 0.6088 0.0939 0.1727 0.090 Uiso 1 1 calc R U . . .
H39C H 0.6354 0.0669 0.1303 0.090 Uiso 1 1 calc R U . . .
C40A C 0.6964(3) 0.1551(3) 0.1693(2) 0.076(2) Uani 1 1 d . . . . .
H40A H 0.6587 0.1671 0.1911 0.114 Uiso 1 1 calc R U . . .
H40B H 0.7174 0.1899 0.1604 0.114 Uiso 1 1 calc R U . . .
H40C H 0.7301 0.1165 0.1792 0.114 Uiso 1 1 calc R U . . .
C41A C 0.6630(3) 0.3762(4) 0.2184(2) 0.0710(19) Uani 1 1 d . . . . .
C42A C 0.6082(4) 0.4020(3) 0.2514(2) 0.084(2) Uani 1 1 d . . . . .
H42A H 0.5652 0.3981 0.2470 0.125 Uiso 1 1 calc R U . . .
H42B H 0.6042 0.4470 0.2513 0.125 Uiso 1 1 calc R U . . .
H42C H 0.6193 0.3778 0.2775 0.125 Uiso 1 1 calc R U . . .
C43A C 0.6779(3) 0.3064(3) 0.2233(2) 0.0714(19) Uani 1 1 d . . . . .
H43D H 0.7016 0.2874 0.2467 0.107 Uiso 1 1 calc R U . . .
H43E H 0.7067 0.2904 0.1989 0.107 Uiso 1 1 calc R U . . .
H43F H 0.6356 0.2950 0.2275 0.107 Uiso 1 1 calc R U . . .
C44A C 0.7310(3) 0.3900(4) 0.2097(2) 0.087(2) Uani 1 1 d . . . . .
H44A H 0.7478 0.3856 0.2352 0.130 Uiso 1 1 calc R U . . .
H44B H 0.7258 0.4335 0.1957 0.130 Uiso 1 1 calc R U . . .
H44C H 0.7633 0.3597 0.1927 0.130 Uiso 1 1 calc R U . . .
C45A C 0.2087(3) 0.3988(2) 0.19164(18) 0.0496(15) Uani 1 1 d . . . . .
C46A C 0.1383(3) 0.4399(3) 0.1805(2) 0.075(2) Uani 1 1 d . . . . .
H46A H 0.1427 0.4547 0.1514 0.113 Uiso 1 1 calc R U . . .
H46B H 0.1215 0.4768 0.1953 0.113 Uiso 1 1 calc R U . . .
H46C H 0.1065 0.4142 0.1877 0.113 Uiso 1 1 calc R U . . .
C47A C 0.2201(2) 0.33019(19) 0.19706(17) 0.0444(13) Uani 1 1 d . . . . .
H47A H 0.1969 0.3167 0.2236 0.067 Uiso 1 1 calc R U . . .
H47B H 0.2687 0.3087 0.1953 0.067 Uiso 1 1 calc R U . . .
H47C H 0.2023 0.3190 0.1759 0.067 Uiso 1 1 calc R U . . .
C48A C 0.2214(2) 0.4211(2) 0.22867(17) 0.0496(15) Uani 1 1 d . . . . .
H48A H 0.1876 0.4138 0.2519 0.074 Uiso 1 1 calc R U . . .
H48B H 0.2179 0.4666 0.2228 0.074 Uiso 1 1 calc R U . . .
H48C H 0.2668 0.3970 0.2348 0.074 Uiso 1 1 calc R U . . .
C49A C 0.0735(2) 0.5916(3) 0.05265(17) 0.0515(14) Uani 1 1 d . . . . .
C50A C 0.0441(3) 0.6647(2) 0.0504(2) 0.0579(17) Uani 1 1 d . . . . .
H50A H -0.0051 0.6765 0.0513 0.087 Uiso 1 1 calc R U . . .
H50B H 0.0643 0.6852 0.0251 0.087 Uiso 1 1 calc R U . . .
H50C H 0.0544 0.6788 0.0733 0.087 Uiso 1 1 calc R U . . .
C51A C 0.0482(3) 0.5624(3) 0.0216(2) 0.080(2) Uani 1 1 d . . . . .
H51A H 0.0260 0.5305 0.0364 0.119 Uiso 1 1 calc R U . . .
H51B H 0.0870 0.5423 0.0025 0.119 Uiso 1 1 calc R U . . .
H51C H 0.0160 0.5965 0.0067 0.119 Uiso 1 1 calc R U . . .
C52A C 0.0562(2) 0.5607(2) 0.09596(17) 0.0504(15) Uani 1 1 d . . . . .
H52A H 0.0786 0.5737 0.1141 0.076 Uiso 1 1 calc R U . . .
H52B H 0.0718 0.5142 0.0971 0.076 Uiso 1 1 calc R U . . .
H52C H 0.0071 0.5744 0.1044 0.076 Uiso 1 1 calc R U . . .
C53A C 0.3752(2) 0.5262(2) 0.25087(17) 0.0461(14) Uani 1 1 d . . . . .
C54A C 0.4320(3) 0.5450(3) 0.2636(2) 0.0651(18) Uani 1 1 d . . . . .
H54A H 0.4746 0.5110 0.2597 0.098 Uiso 1 1 calc R U . . .
H54B H 0.4371 0.5846 0.2470 0.098 Uiso 1 1 calc R U . . .
H54C H 0.4202 0.5513 0.2921 0.098 Uiso 1 1 calc R U . . .
C55A C 0.3756(3) 0.4556(2) 0.2701(2) 0.072(2) Uani 1 1 d . . . . .
H55A H 0.3452 0.4564 0.2960 0.108 Uiso 1 1 calc R U . . .
H55B H 0.4216 0.4305 0.2745 0.108 Uiso 1 1 calc R U . . .
H55C H 0.3601 0.4362 0.2517 0.108 Uiso 1 1 calc R U . . .
C56A C 0.3097(3) 0.5791(3) 0.2570(2) 0.0689(18) Uani 1 1 d . . . . .
H56A H 0.2919 0.5779 0.2859 0.103 Uiso 1 1 calc R U . . .
H56B H 0.2766 0.5734 0.2426 0.103 Uiso 1 1 calc R U . . .
H56C H 0.3182 0.6204 0.2465 0.103 Uiso 1 1 calc R U . . .
C57A C 0.1647(3) 0.8318(2) 0.0326(2) 0.0504(15) Uani 1 1 d . . . . .
C58A C 0.1427(3) 0.8199(3) 0.0759(2) 0.079(2) Uani 1 1 d . . . . .
H58A H 0.1559 0.8479 0.0897 0.119 Uiso 1 1 calc R U . . .
H58B H 0.1641 0.7753 0.0860 0.119 Uiso 1 1 calc R U . . .
H58C H 0.0934 0.8285 0.0812 0.119 Uiso 1 1 calc R U . . .
C59A C 0.1163(3) 0.8308(3) 0.0045(2) 0.0671(19) Uani 1 1 d . . . . .
H59A H 0.0852 0.8737 -0.0007 0.101 Uiso 1 1 calc R U . . .
H59B H 0.0902 0.8010 0.0174 0.101 Uiso 1 1 calc R U . . .
H59C H 0.1425 0.8173 -0.0211 0.101 Uiso 1 1 calc R U . . .
C60A C 0.1944(3) 0.8853(3) 0.0133(2) 0.073(2) Uani 1 1 d . . . . .
H60A H 0.1578 0.9251 0.0099 0.109 Uiso 1 1 calc R U . . .
H60B H 0.2205 0.8760 -0.0131 0.109 Uiso 1 1 calc R U . . .
H60C H 0.2241 0.8898 0.0306 0.109 Uiso 1 1 calc R U . . .
C61A C 0.6129(3) 0.8305(2) -0.1151(2) 0.0582(16) Uani 1 1 d . . . . .
C62A C 0.5595(3) 0.8886(2) -0.0950(2) 0.0669(19) Uani 1 1 d . . . . .
H62A H 0.5313 0.9159 -0.1149 0.100 Uiso 1 1 calc R U . . .
H62B H 0.5835 0.9134 -0.0860 0.100 Uiso 1 1 calc R U . . .
H62C H 0.5308 0.8724 -0.0718 0.100 Uiso 1 1 calc R U . . .
C63A C 0.6806(3) 0.8192(3) -0.1001(2) 0.075(2) Uani 1 1 d . . . . .
H63A H 0.7016 0.7733 -0.0937 0.112 Uiso 1 1 calc R U . . .
H63B H 0.6723 0.8396 -0.0758 0.112 Uiso 1 1 calc R U . . .
H63C H 0.7109 0.8374 -0.1213 0.112 Uiso 1 1 calc R U . . .
C64A C 0.6151(3) 0.8343(3) -0.1617(2) 0.0702(19) Uani 1 1 d . . . . .
H64A H 0.5890 0.8770 -0.1724 0.105 Uiso 1 1 calc R U . . .
H64B H 0.5954 0.8026 -0.1667 0.105 Uiso 1 1 calc R U . . .
H64C H 0.6621 0.8257 -0.1751 0.105 Uiso 1 1 calc R U . . .
O1A O 0.8436(2) 0.58191(19) -0.03132(15) 0.0783(14) Uani 1 1 d . . . . .
O2A O 0.7936(2) 0.6572(2) -0.08847(17) 0.0857(15) Uani 1 1 d . . . . .
O3A O 0.7587(2) 0.68830(18) -0.02217(14) 0.0709(12) Uani 1 1 d . . . . .
O4A O 0.47724(16) 0.85610(16) 0.00938(13) 0.0569(11) Uani 1 1 d . . . . .
O5A O 0.38933(18) 0.86767(17) -0.03050(13) 0.0579(11) Uani 1 1 d . . . . .
O6A O 0.35941(18) 0.86066(16) 0.04033(14) 0.0601(11) Uani 1 1 d . . . . .
O7A O 0.49901(18) 0.76274(18) -0.18871(13) 0.0616(11) Uani 1 1 d . . . . .
O8A O 0.5998(2) 0.68011(18) -0.20579(14) 0.0691(12) Uani 1 1 d . . . . .
O9A O 0.49838(17) 0.67446(15) -0.22341(13) 0.0551(10) Uani 1 1 d . . . . .
O10A O 0.8543(2) 0.32015(19) 0.05730(16) 0.0811(14) Uani 1 1 d . . . . .
O11A O 0.81060(18) 0.22760(17) 0.08106(14) 0.0647(12) Uani 1 1 d . . . . .
O12A O 0.7872(2) 0.3161(2) 0.12057(16) 0.0817(14) Uani 1 1 d . . . . .
O13A O 0.60534(17) 0.55969(19) 0.18998(13) 0.0627(11) Uani 1 1 d . . . . .
O14A O 0.62375(18) 0.65029(15) 0.14957(12) 0.0526(10) Uani 1 1 d . . . . .
O15A O 0.51170(16) 0.65400(15) 0.18807(12) 0.0504(10) Uani 1 1 d . . . . .
O16A O 0.19501(17) 0.58328(15) 0.17920(13) 0.0540(10) Uani 1 1 d . . . . .
O17A O 0.22737(18) 0.67995(16) 0.15940(13) 0.0585(11) Uani 1 1 d . . . . .
O18A O 0.14545(19) 0.65976(18) 0.12693(14) 0.0636(12) Uani 1 1 d . . . . .
S1A S 0.81454(8) 0.64767(8) -0.05190(6) 0.0642(5) Uani 1 1 d . . . . .
S2A S 0.40367(6) 0.87951(5) 0.00576(5) 0.0465(4) Uani 1 1 d . . . . .
S3A S 0.53546(6) 0.71638(6) -0.21464(5) 0.0465(4) Uani 1 1 d . . . . .
S4A S 0.82661(9) 0.28130(8) 0.09360(6) 0.0668(5) Uani 1 1 d . . . . .
S5A S 0.58496(7) 0.62696(6) 0.18438(5) 0.0535(4) Uani 1 1 d . . . . .
S6A S 0.17475(8) 0.64747(7) 0.16182(6) 0.0582(4) Uani 1 1 d . . . . .
S7A S 0.66408(7) 0.57324(6) -0.02889(5) 0.0506(4) Uani 1 1 d . . . . .
S8A S 0.45275(6) 0.69600(5) 0.00631(5) 0.0448(3) Uani 1 1 d . . . . .
S9A S 0.51591(7) 0.61304(6) -0.11260(5) 0.0511(4) Uani 1 1 d . . . . .
S10A S 0.66648(7) 0.38616(6) 0.05095(5) 0.0510(4) Uani 1 1 d . . . . .
S11A S 0.53872(7) 0.57210(6) 0.09485(5) 0.0494(4) Uani 1 1 d . . . . .
S12A S 0.32899(6) 0.57263(6) 0.08384(5) 0.0487(4) Uani 1 1 d . . . . .
S13A S 0.60623(6) 0.72188(5) 0.04820(5) 0.0407(3) Uani 1 1 d . . . . .
S14A S 0.38407(6) 0.72288(5) 0.12103(5) 0.0430(3) Uani 1 1 d . . . . .
S15A S 0.63577(6) 0.22208(5) 0.10298(5) 0.0462(4) Uani 1 1 d . . . . .
S16A S 0.62917(7) 0.39803(6) 0.17010(5) 0.0544(4) Uani 1 1 d . . . . .
S17A S 0.27049(6) 0.42431(6) 0.14778(5) 0.0467(4) Uani 1 1 d . . . . .
S18A S 0.16555(6) 0.57435(6) 0.03998(5) 0.0484(4) Uani 1 1 d . . . . .
S19A S 0.75338(7) 0.51801(6) 0.07744(5) 0.0535(4) Uani 1 1 d . . . . .
S20A S 0.40352(7) 0.52127(6) 0.19416(5) 0.0542(4) Uani 1 1 d . . . . .
S21A S 0.23933(6) 0.75540(5) 0.02561(5) 0.0498(4) Uani 1 1 d . . . . .
S22A S 0.54490(8) 0.48923(7) -0.08787(5) 0.0617(4) Uani 1 1 d . . . . .
S23A S 0.53834(8) 0.61760(7) -0.04090(5) 0.0577(4) Uani 1 1 d . . . . .
S24A S 0.58886(7) 0.75649(6) -0.08928(5) 0.0529(4) Uani 1 1 d . . . . .
S25A S 0.37860(9) 0.62209(8) 0.00830(7) 0.0852(6) Uani 1 1 d . . . . .
S1C S 0.5000 0.5000 0.0000 0.0736(7) Uani 1 2 d S . P . .
Ag23 Ag 0.71317(2) 0.07394(2) 0.46499(2) 0.05471(12) Uani 1 1 d . . . . .
Ag24 Ag 0.80770(2) 0.24196(2) 0.42946(2) 0.05307(12) Uani 1 1 d . . . . .
Ag25 Ag 0.80852(2) 0.12450(2) 0.38408(2) 0.06492(14) Uani 1 1 d . . . . .
Ag26 Ag 0.87995(2) 0.27206(2) 0.48316(2) 0.05468(12) Uani 1 1 d . . . . .
Ag27 Ag 1.00148(2) 0.25624(2) 0.53433(2) 0.05043(11) Uani 1 1 d . . . . .
Ag28 Ag 0.98877(2) 0.25656(2) 0.39948(2) 0.04772(11) Uani 1 1 d . . . . .
Ag29 Ag 1.07980(2) 0.15645(2) 0.35454(2) 0.05534(13) Uani 1 1 d . . . . .
Ag30 Ag 1.14136(2) 0.01237(2) 0.32674(2) 0.04990(11) Uani 1 1 d . . . . .
Ag31 Ag 0.93046(2) 0.15593(2) 0.33901(2) 0.04939(11) Uani 1 1 d . . . . .
Ag32 Ag 0.83343(2) -0.01215(2) 0.37503(2) 0.05207(12) Uani 1 1 d . . . . .
Ag33 Ag 1.04557(2) -0.15691(2) 0.36147(2) 0.05181(12) Uani 1 1 d . . . . .
Ag34 Ag 0.90143(2) -0.15597(2) 0.41992(2) 0.05552(13) Uani 1 1 d . . . . .
Ag35 Ag 0.72711(2) 0.07237(2) 0.60059(2) 0.05410(12) Uani 1 1 d . . . . .
Ag36 Ag 0.83258(2) 0.12013(2) 0.63865(2) 0.05940(13) Uani 1 1 d . . . . .
Ag37 Ag 0.81974(2) 0.24195(2) 0.56548(2) 0.05431(12) Uani 1 1 d . . . . .
Ag38 Ag 1.21695(2) 0.10915(2) 0.52118(2) 0.05525(12) Uani 1 1 d . . . . .
Ag39 Ag 1.27770(2) 0.00617(2) 0.45713(2) 0.06230(13) Uani 1 1 d . . . . .
Ag40 Ag 1.20552(2) 0.11066(2) 0.38592(2) 0.05457(12) Uani 1 1 d . . . . .
Ag41 Ag 1.14896(2) -0.03496(2) 0.48188(2) 0.07320(16) Uani 1 1 d . . . . .
Ag42 Ag 1.12309(3) 0.21486(2) 0.45365(2) 0.0496(2) Uani 0.521(4) 1 d . . P C 1
Ag43 Ag 0.98484(2) 0.00151(2) 0.32534(2) 0.0482(2) Uani 0.526(4) 1 d . . P D 1
Cu7B Cu 1.12309(3) 0.21486(2) 0.45365(2) 0.0496(2) Uani 0.479(4) 1 d . . P C 2
Cu8B Cu 0.98484(2) 0.00151(2) 0.32534(2) 0.0482(2) Uani 0.474(4) 1 d . . P D 2
Cu1B Cu 0.94538(3) 0.03842(3) 0.58291(3) 0.05548(19) Uani 1 1 d . . . . .
Cu2B Cu 0.90424(3) 0.13121(3) 0.49694(3) 0.0643(2) Uani 1 1 d . . . . .
Cu3B Cu 1.06225(4) 0.09037(3) 0.43569(3) 0.0668(2) Uani 1 1 d . . . . .
Cu4B Cu 0.90074(5) 0.02714(5) 0.43091(4) 0.1061(4) Uani 1 1 d . . . . .
Cu5B Cu 1.08061(4) 0.08426(4) 0.52385(3) 0.0761(3) Uani 1 1 d . . . . .
Cu6B Cu 0.72569(3) 0.18497(3) 0.51758(2) 0.05250(19) Uani 1 1 d . . . . .
C1B C 0.6191(3) 0.2604(2) 0.66896(19) 0.0526(15) Uani 1 1 d . . . . .
C2B C 0.6489(3) 0.3022(2) 0.68679(19) 0.0583(17) Uani 1 1 d . . . . .
H2B1 H 0.6196 0.3463 0.6842 0.088 Uiso 1 1 calc R U . . .
H2B2 H 0.6942 0.3009 0.6721 0.088 Uiso 1 1 calc R U . . .
H2B3 H 0.6517 0.2861 0.7154 0.088 Uiso 1 1 calc R U . . .
C3B C 0.6028(3) 0.2094(3) 0.7036(2) 0.072(2) Uani 1 1 d . . . . .
H3BA H 0.5618 0.2289 0.7215 0.107 Uiso 1 1 calc R U . . .
H3BB H 0.6408 0.1917 0.7190 0.107 Uiso 1 1 calc R U . . .
H3BC H 0.5956 0.1752 0.6924 0.107 Uiso 1 1 calc R U . . .
C4B C 0.5625(3) 0.3005(3) 0.6416(2) 0.070(2) Uani 1 1 d . . . . .
H4B1 H 0.5582 0.2736 0.6233 0.105 Uiso 1 1 calc R U . . .
H4B2 H 0.5755 0.3374 0.6258 0.105 Uiso 1 1 calc R U . . .
H4B3 H 0.5191 0.3150 0.6590 0.105 Uiso 1 1 calc R U . . .
C5B C 0.9357(3) 0.4620(3) 0.44947(19) 0.0530(15) Uani 1 1 d . . . . .
C6B C 0.9972(3) 0.4838(3) 0.4362(2) 0.073(2) Uani 1 1 d . . . . .
H6BA H 0.9842 0.5305 0.4312 0.110 Uiso 1 1 calc R U . . .
H6BB H 1.0220 0.4667 0.4113 0.110 Uiso 1 1 calc R U . . .
H6BC H 1.0263 0.4686 0.4573 0.110 Uiso 1 1 calc R U . . .
C7B C 0.9019(3) 0.4866(2) 0.4889(2) 0.072(2) Uani 1 1 d . . . . .
H7B1 H 0.9228 0.4572 0.5111 0.107 Uiso 1 1 calc R U . . .
H7B2 H 0.8536 0.4899 0.4929 0.107 Uiso 1 1 calc R U . . .
H7B3 H 0.9075 0.5288 0.4883 0.107 Uiso 1 1 calc R U . . .
C8B C 0.8886(3) 0.4912(3) 0.4146(2) 0.075(2) Uani 1 1 d . . . . .
H8B1 H 0.8710 0.5375 0.4139 0.112 Uiso 1 1 calc R U . . .
H8B2 H 0.8508 0.4726 0.4202 0.112 Uiso 1 1 calc R U . . .
H8B3 H 0.9155 0.4812 0.3884 0.112 Uiso 1 1 calc R U . . .
C9B C 1.0908(3) 0.1866(2) 0.21489(17) 0.0461(14) Uani 1 1 d . . . . .
C10B C 1.0516(3) 0.2559(2) 0.20997(19) 0.0530(16) Uani 1 1 d . . . . .
H10D H 1.0539 0.2727 0.1812 0.079 Uiso 1 1 calc R U . . .
H10E H 1.0710 0.2795 0.2235 0.079 Uiso 1 1 calc R U . . .
H10F H 1.0042 0.2608 0.2221 0.079 Uiso 1 1 calc R U . . .
C11B C 1.1673(2) 0.1782(2) 0.20503(19) 0.0503(15) Uani 1 1 d . . . . .
H11D H 1.1795 0.1910 0.1761 0.076 Uiso 1 1 calc R U . . .
H11E H 1.1919 0.1334 0.2123 0.076 Uiso 1 1 calc R U . . .
H11F H 1.1793 0.2048 0.2205 0.076 Uiso 1 1 calc R U . . .
C12B C 1.0689(3) 0.1522(3) 0.1868(2) 0.0604(17) Uani 1 1 d . . . . .
H12D H 1.0285 0.1397 0.2005 0.091 Uiso 1 1 calc R U . . .
H12E H 1.1057 0.1141 0.1803 0.091 Uiso 1 1 calc R U . . .
H12F H 1.0587 0.1809 0.1619 0.091 Uiso 1 1 calc R U . . .
C13B C 0.8722(3) -0.1825(3) 0.2939(2) 0.0681(18) Uani 1 1 d . . . . .
C14B C 0.8888(3) -0.1464(3) 0.2522(2) 0.077(2) Uani 1 1 d . . . . .
H14D H 0.9144 -0.1769 0.2334 0.115 Uiso 1 1 calc R U . . .
H14E H 0.9161 -0.1190 0.2542 0.115 Uiso 1 1 calc R U . . .
H14F H 0.8468 -0.1202 0.2423 0.115 Uiso 1 1 calc R U . . .
C15B C 0.7946(3) -0.1724(3) 0.3036(2) 0.083(2) Uani 1 1 d . . . . .
H15D H 0.7750 -0.1588 0.2785 0.124 Uiso 1 1 calc R U . . .
H15E H 0.7742 -0.1396 0.3215 0.124 Uiso 1 1 calc R U . . .
H15F H 0.7856 -0.2125 0.3170 0.124 Uiso 1 1 calc R U . . .
C16B C 0.9115(3) -0.2541(3) 0.2965(2) 0.0698(19) Uani 1 1 d . . . . .
H16D H 0.8984 -0.2734 0.2771 0.105 Uiso 1 1 calc R U . . .
H16E H 0.9009 -0.2753 0.3239 0.105 Uiso 1 1 calc R U . . .
H16F H 0.9602 -0.2589 0.2903 0.105 Uiso 1 1 calc R U . . .
C17B C 0.5956(3) 0.2670(3) 0.3854(2) 0.0655(18) Uani 1 1 d . . . . .
C18B C 0.6127(3) 0.3242(3) 0.3595(2) 0.068(2) Uani 1 1 d . . . . .
H18D H 0.6515 0.3100 0.3388 0.103 Uiso 1 1 calc R U . . .
H18E H 0.6240 0.3492 0.3764 0.103 Uiso 1 1 calc R U . . .
H18F H 0.5737 0.3507 0.3465 0.103 Uiso 1 1 calc R U . . .
C19B C 0.5407(3) 0.2933(3) 0.4205(2) 0.0704(19) Uani 1 1 d . . . . .
H19D H 0.4988 0.3182 0.4099 0.106 Uiso 1 1 calc R U . . .
H19E H 0.5564 0.3206 0.4333 0.106 Uiso 1 1 calc R U . . .
H19F H 0.5322 0.2577 0.4404 0.106 Uiso 1 1 calc R U . . .
C20B C 0.5791(3) 0.2251(3) 0.3615(2) 0.073(2) Uani 1 1 d . . . . .
H20D H 0.5867 0.2410 0.3327 0.109 Uiso 1 1 calc R U . . .
H20E H 0.5316 0.2256 0.3698 0.109 Uiso 1 1 calc R U . . .
H20F H 0.6083 0.1814 0.3666 0.109 Uiso 1 1 calc R U . . .
C21B C 1.3985(3) 0.1536(3) 0.42027(19) 0.0550(15) Uani 1 1 d . . . . .
C22B C 1.4415(4) 0.1247(3) 0.4551(2) 0.087(2) Uani 1 1 d . . . . .
H22D H 1.4874 0.1287 0.4459 0.131 Uiso 1 1 calc R U . . .
H22E H 1.4437 0.0796 0.4628 0.131 Uiso 1 1 calc R U . . .
H22F H 1.4206 0.1476 0.4784 0.131 Uiso 1 1 calc R U . . .
C23B C 1.3750(3) 0.2252(3) 0.4104(2) 0.0668(19) Uani 1 1 d . . . . .
H23D H 1.3689 0.2368 0.3819 0.100 Uiso 1 1 calc R U . . .
H23E H 1.4089 0.2434 0.4154 0.100 Uiso 1 1 calc R U . . .
H23F H 1.3318 0.2420 0.4274 0.100 Uiso 1 1 calc R U . . .
C24B C 1.4372(3) 0.1272(3) 0.3801(2) 0.0700(19) Uani 1 1 d . . . . .
H24D H 1.4763 0.1438 0.3704 0.105 Uiso 1 1 calc R U . . .
H24E H 1.4068 0.1408 0.3597 0.105 Uiso 1 1 calc R U . . .
H24F H 1.4527 0.0806 0.3850 0.105 Uiso 1 1 calc R U . . .
C25B C 0.5740(3) 0.1273(3) 0.5508(2) 0.0592(17) Uani 1 1 d . . . . .
C26B C 0.5584(4) 0.2014(3) 0.5430(2) 0.092(2) Uani 1 1 d . . . . .
H26D H 0.5110 0.2207 0.5390 0.137 Uiso 1 1 calc R U . . .
H26E H 0.5881 0.2137 0.5188 0.137 Uiso 1 1 calc R U . . .
H26F H 0.5662 0.2164 0.5663 0.137 Uiso 1 1 calc R U . . .
C27B C 0.5459(3) 0.1054(3) 0.5190(2) 0.0718(19) Uani 1 1 d . . . . .
H27D H 0.5288 0.0690 0.5316 0.108 Uiso 1 1 calc R U . . .
H27E H 0.5820 0.0927 0.4966 0.108 Uiso 1 1 calc R U . . .
H27F H 0.5089 0.1405 0.5089 0.108 Uiso 1 1 calc R U . . .
C28B C 0.5574(3) 0.0997(2) 0.59351(18) 0.0525(15) Uani 1 1 d . . . . .
H28D H 0.5841 0.1099 0.6104 0.079 Uiso 1 1 calc R U . . .
H28E H 0.5680 0.0533 0.5953 0.079 Uiso 1 1 calc R U . . .
H28F H 0.5091 0.1177 0.6030 0.079 Uiso 1 1 calc R U . . .
C29B C 1.3094(3) 0.0239(2) 0.3057(2) 0.0576(17) Uani 1 1 d . . . . .
C30B C 1.3671(3) 0.0369(4) 0.3186(3) 0.103(3) Uani 1 1 d . . . . .
H30D H 1.3878 0.0628 0.2964 0.155 Uiso 1 1 calc R U . . .
H30E H 1.4008 -0.0036 0.3257 0.155 Uiso 1 1 calc R U . . .
H30F H 1.3503 0.0599 0.3421 0.155 Uiso 1 1 calc R U . . .
C31B C 1.3444(3) -0.0414(3) 0.2933(2) 0.079(2) Uani 1 1 d . . . . .
H31D H 1.3178 -0.0509 0.2761 0.118 Uiso 1 1 calc R U . . .
H31E H 1.3487 -0.0734 0.3175 0.118 Uiso 1 1 calc R U . . .
H31F H 1.3895 -0.0424 0.2783 0.118 Uiso 1 1 calc R U . . .
C32B C 1.2843(3) 0.0740(3) 0.2725(2) 0.080(2) Uani 1 1 d . . . . .
H32D H 1.3188 0.0699 0.2483 0.120 Uiso 1 1 calc R U . . .
H32E H 1.2747 0.1161 0.2807 0.120 Uiso 1 1 calc R U . . .
H32F H 1.2428 0.0690 0.2664 0.120 Uiso 1 1 calc R U . . .
C33B C 1.1503(2) 0.2822(2) 0.34592(18) 0.0460(14) Uani 1 1 d . . . . .
C34B C 1.1720(3) 0.3242(3) 0.3678(2) 0.0676(19) Uani 1 1 d . . . . .
H34D H 1.1834 0.3591 0.3484 0.101 Uiso 1 1 calc R U . . .
H34E H 1.2116 0.2988 0.3805 0.101 Uiso 1 1 calc R U . . .
H34F H 1.1348 0.3419 0.3886 0.101 Uiso 1 1 calc R U . . .
C35B C 1.2117(2) 0.2501(2) 0.31619(18) 0.0518(15) Uani 1 1 d . . . . .
H35D H 1.2026 0.2149 0.3072 0.078 Uiso 1 1 calc R U . . .
H35E H 1.2519 0.2337 0.3297 0.078 Uiso 1 1 calc R U . . .
H35F H 1.2195 0.2815 0.2928 0.078 Uiso 1 1 calc R U . . .
C36B C 1.0945(2) 0.3229(2) 0.32293(17) 0.0434(14) Uani 1 1 d . . . . .
H36D H 1.0528 0.3364 0.3419 0.065 Uiso 1 1 calc R U . . .
H36E H 1.0874 0.2985 0.3040 0.065 Uiso 1 1 calc R U . . .
H36F H 1.1070 0.3606 0.3079 0.065 Uiso 1 1 calc R U . . .
C37B C 0.8589(3) 0.3305(2) 0.33304(19) 0.0507(15) Uani 1 1 d . . . . .
C38B C 0.8626(3) 0.3847(3) 0.3527(2) 0.0683(19) Uani 1 1 d . . . . .
H38D H 0.8736 0.4181 0.3317 0.102 Uiso 1 1 calc R U . . .
H38E H 0.8977 0.3687 0.3701 0.102 Uiso 1 1 calc R U . . .
H38F H 0.8188 0.4024 0.3688 0.102 Uiso 1 1 calc R U . . .
C39B C 0.9067(3) 0.3235(3) 0.2935(2) 0.0673(18) Uani 1 1 d . . . . .
H39D H 0.8988 0.3647 0.2761 0.101 Uiso 1 1 calc R U . . .
H39E H 0.8987 0.2921 0.2799 0.101 Uiso 1 1 calc R U . . .
H39F H 0.9536 0.3091 0.2988 0.101 Uiso 1 1 calc R U . . .
C40B C 0.7879(3) 0.3373(2) 0.33093(19) 0.0552(15) Uani 1 1 d . . . . .
H40D H 0.7583 0.3622 0.3519 0.083 Uiso 1 1 calc R U . . .
H40E H 0.7809 0.2950 0.3352 0.083 Uiso 1 1 calc R U . . .
H40F H 0.7771 0.3593 0.3043 0.083 Uiso 1 1 calc R U . . .
C41B C 0.8358(2) 0.1019(2) 0.27816(17) 0.0443(13) Uani 1 1 d . . . . .
C42B C 0.7656(3) 0.0866(3) 0.28775(19) 0.0595(16) Uani 1 1 d . . . . .
H42D H 0.7319 0.1194 0.3025 0.089 Uiso 1 1 calc R U . . .
H42E H 0.7705 0.0449 0.3043 0.089 Uiso 1 1 calc R U . . .
H42F H 0.7506 0.0862 0.2624 0.089 Uiso 1 1 calc R U . . .
C43B C 0.8274(3) 0.1716(3) 0.2673(2) 0.077(2) Uani 1 1 d . . . . .
H43A H 0.8720 0.1789 0.2591 0.116 Uiso 1 1 calc R U . . .
H43B H 0.8035 0.1934 0.2907 0.116 Uiso 1 1 calc R U . . .
H43C H 0.8011 0.1883 0.2449 0.116 Uiso 1 1 calc R U . . .
C44B C 0.8840(3) 0.0620(2) 0.24927(18) 0.0565(16) Uani 1 1 d . . . . .
H44D H 0.8612 0.0608 0.2272 0.085 Uiso 1 1 calc R U . . .
H44E H 0.9010 0.0187 0.2630 0.085 Uiso 1 1 calc R U . . .
H44F H 0.9219 0.0799 0.2384 0.085 Uiso 1 1 calc R U . . .
C45B C 0.6622(3) -0.0209(2) 0.41009(19) 0.0578(16) Uani 1 1 d D . . . .
C46B C 0.6097(3) -0.0202(4) 0.4474(2) 0.094(3) Uani 1 1 d . . . . .
H46D H 0.6044 -0.0630 0.4560 0.140 Uiso 1 1 calc R U . . .
H46E H 0.5664 0.0098 0.4413 0.140 Uiso 1 1 calc R U . . .
H46F H 0.6242 -0.0068 0.4691 0.140 Uiso 1 1 calc R U . . .
C47B C 0.6847(3) -0.0754(3) 0.3830(2) 0.078(2) Uani 1 1 d . . . . .
H47D H 0.6849 -0.1161 0.4001 0.118 Uiso 1 1 calc R U . . .
H47E H 0.7303 -0.0779 0.3683 0.118 Uiso 1 1 calc R U . . .
H47F H 0.6530 -0.0664 0.3637 0.118 Uiso 1 1 calc R U . . .
C48B C 0.6308(3) 0.0426(3) 0.3870(2) 0.098(3) Uani 1 1 d D . . . .
H48D H 0.5914 0.0405 0.3768 0.147 Uiso 1 1 calc R U . . .
H48E H 0.6640 0.0530 0.3643 0.147 Uiso 1 1 calc R U . . .
H48F H 0.6166 0.0755 0.4049 0.147 Uiso 1 1 calc R U . . .
C49B C 0.8864(2) 0.3290(2) 0.61937(17) 0.0425(13) Uani 1 1 d . . . . .
C50B C 1.0708(3) -0.0601(3) 0.23572(18) 0.0617(17) Uani 1 1 d . . . . .
H50D H 1.0827 -0.0714 0.2082 0.093 Uiso 1 1 calc R U . . .
H50E H 1.0639 -0.0143 0.2346 0.093 Uiso 1 1 calc R U . . .
H50F H 1.0291 -0.0707 0.2488 0.093 Uiso 1 1 calc R U . . .
C51B C 1.1453(2) -0.1677(2) 0.26472(17) 0.0471(15) Uani 1 1 d . . . . .
H51D H 1.1575 -0.1825 0.2382 0.071 Uiso 1 1 calc R U . . .
H51E H 1.1067 -0.1818 0.2800 0.071 Uiso 1 1 calc R U . . .
H51F H 1.1840 -0.1855 0.2795 0.071 Uiso 1 1 calc R U . . .
C52B C 1.1923(2) -0.07665(19) 0.24630(16) 0.0382(13) Uani 1 1 d . . . . .
H52D H 1.2314 -0.1147 0.2465 0.057 Uiso 1 1 calc R U . . .
H52E H 1.1948 -0.0495 0.2651 0.057 Uiso 1 1 calc R U . . .
H52F H 1.1924 -0.0530 0.2190 0.057 Uiso 1 1 calc R U . . .
C53B C 1.1268(2) -0.0966(2) 0.25933(17) 0.0426(13) Uani 1 1 d . . . . .
C54B C 1.1818(3) 0.3245(2) 0.4923(2) 0.0589(18) Uani 1 1 d . . . . .
H54D H 1.1401 0.3578 0.4870 0.088 Uiso 1 1 calc R U . . .
H54E H 1.1975 0.2980 0.4704 0.088 Uiso 1 1 calc R U . . .
H54F H 1.2167 0.3442 0.4937 0.088 Uiso 1 1 calc R U . . .
C55B C 1.2300(3) 0.2492(3) 0.5516(2) 0.078(2) Uani 1 1 d . . . . .
H55D H 1.2413 0.2790 0.5648 0.117 Uiso 1 1 calc R U . . .
H55E H 1.2679 0.2324 0.5310 0.117 Uiso 1 1 calc R U . . .
H55F H 1.2211 0.2140 0.5717 0.117 Uiso 1 1 calc R U . . .
C56B C 1.1182(3) 0.3248(2) 0.56078(19) 0.0527(16) Uani 1 1 d . . . . .
H56D H 1.1337 0.3149 0.5871 0.079 Uiso 1 1 calc R U . . .
H56E H 1.0740 0.3172 0.5638 0.079 Uiso 1 1 calc R U . . .
H56F H 1.1141 0.3697 0.5501 0.079 Uiso 1 1 calc R U . . .
C57B C 1.1682(2) 0.2833(2) 0.53216(18) 0.0429(14) Uani 1 1 d . . . . .
C58B C 0.9460(3) 0.3201(3) 0.6409(2) 0.073(2) Uani 1 1 d . . . . .
H58D H 0.9381 0.3573 0.6545 0.109 Uiso 1 1 calc R U . . .
H58E H 0.9874 0.3155 0.6212 0.109 Uiso 1 1 calc R U . . .
H58F H 0.9508 0.2818 0.6610 0.109 Uiso 1 1 calc R U . . .
C59B C 0.8249(3) 0.3258(3) 0.6487(2) 0.075(2) Uani 1 1 d . . . . .
H59D H 0.8321 0.2829 0.6640 0.112 Uiso 1 1 calc R U . . .
H59E H 0.7863 0.3354 0.6342 0.112 Uiso 1 1 calc R U . . .
H59F H 0.8155 0.3570 0.6674 0.112 Uiso 1 1 calc R U . . .
C60B C 0.8886(3) 0.3849(2) 0.58454(19) 0.0602(18) Uani 1 1 d . . . . .
H60D H 0.9204 0.4064 0.5884 0.090 Uiso 1 1 calc R U . . .
H60E H 0.8433 0.4153 0.5847 0.090 Uiso 1 1 calc R U . . .
H60F H 0.9033 0.3681 0.5586 0.090 Uiso 1 1 calc R U . . .
C61B C 0.7012(3) 0.3602(2) 0.4993(2) 0.0625(18) Uani 1 1 d . . . . .
C62B C 0.7143(3) 0.3919(3) 0.5297(2) 0.0667(18) Uani 1 1 d . . . . .
H62D H 0.6740 0.4267 0.5371 0.100 Uiso 1 1 calc R U . . .
H62E H 0.7526 0.4090 0.5186 0.100 Uiso 1 1 calc R U . . .
H62F H 0.7249 0.3610 0.5538 0.100 Uiso 1 1 calc R U . . .
C63B C 0.6318(3) 0.3494(3) 0.5122(2) 0.075(2) Uani 1 1 d . . . . .
H63D H 0.6121 0.3635 0.5387 0.112 Uiso 1 1 calc R U . . .
H63E H 0.6363 0.3039 0.5141 0.112 Uiso 1 1 calc R U . . .
H63F H 0.6023 0.3737 0.4923 0.112 Uiso 1 1 calc R U . . .
C64B C 0.7123(2) 0.3939(2) 0.45495(17) 0.0417(13) Uani 1 1 d . . . . .
H64D H 0.6700 0.4256 0.4488 0.063 Uiso 1 1 calc R U . . .
H64E H 0.7261 0.3621 0.4363 0.063 Uiso 1 1 calc R U . . .
H64F H 0.7477 0.4150 0.4520 0.063 Uiso 1 1 calc R U . . .
O1B O 0.64149(18) 0.17339(17) 0.43552(14) 0.0656(12) Uani 1 1 d . . . . .
O2B O 0.69012(17) 0.25833(16) 0.42538(13) 0.0567(11) Uani 1 1 d . . . . .
O3B O 0.70891(18) 0.19097(18) 0.37380(12) 0.0575(11) Uani 1 1 d . . . . .
O4B O 0.89169(14) 0.36527(14) 0.46725(12) 0.0456(10) Uani 1 1 d . . . . .
O5B O 0.9958(2) 0.35719(17) 0.48802(13) 0.0607(11) Uani 1 1 d . . . . .
O6B O 0.98776(17) 0.35772(15) 0.41606(12) 0.0512(10) Uani 1 1 d . . . . .
O7B O 1.08879(15) 0.18115(15) 0.29040(12) 0.0478(10) Uani 1 1 d . . . . .
O8B O 1.10823(17) 0.08383(15) 0.26487(12) 0.0500(9) Uani 1 1 d . . . . .
O9B O 0.99902(16) 0.15717(15) 0.27054(12) 0.0520(10) Uani 1 1 d . . . . .
O10B O 0.85923(19) -0.08350(18) 0.32401(13) 0.0629(11) Uani 1 1 d . . . . .
O11B O 0.96882(17) -0.15505(16) 0.31412(12) 0.0527(10) Uani 1 1 d . . . . .
O12B O 0.88236(19) -0.18252(16) 0.36552(14) 0.0619(12) Uani 1 1 d . . . . .
O13B O 0.66077(16) 0.17142(15) 0.62540(12) 0.0516(10) Uani 1 1 d . . . . .
O14B O 0.74077(19) 0.17867(18) 0.66317(13) 0.0633(12) Uani 1 1 d . . . . .
O15B O 0.71057(18) 0.26265(16) 0.60741(13) 0.0568(11) Uani 1 1 d . . . . .
O16B O 1.29308(17) 0.15207(16) 0.47132(13) 0.0534(10) Uani 1 1 d . . . . .
O17B O 1.34693(17) 0.05909(17) 0.44033(13) 0.0587(11) Uani 1 1 d . . . . .
O18B O 1.28842(16) 0.15516(14) 0.40053(13) 0.0499(10) Uani 1 1 d . . . . .
S1B S 0.66540(7) 0.21893(6) 0.40708(5) 0.0519(4) Uani 1 1 d . . . . .
S2B S 0.95459(7) 0.37919(5) 0.45622(5) 0.0433(3) Uani 1 1 d . . . . .
S3B S 1.07085(6) 0.14783(5) 0.26477(5) 0.0387(3) Uani 1 1 d . . . . .
S4B S 0.89886(7) -0.14603(6) 0.32670(5) 0.0513(4) Uani 1 1 d . . . . .
S5B S 0.68910(7) 0.21505(6) 0.63743(5) 0.0528(4) Uani 1 1 d . . . . .
S6B S 1.32368(8) 0.12746(6) 0.43462(5) 0.0527(4) Uani 1 1 d . . . . .
S7B S 0.66821(6) 0.10302(5) 0.53740(5) 0.0406(3) Uani 1 1 d . . . . .
S8B S 0.76718(6) 0.27855(5) 0.49943(5) 0.0402(3) Uani 1 1 d . . . . .
S9B S 1.13172(6) 0.22197(5) 0.52199(5) 0.0389(3) Uani 1 1 d . . . . .
S10B S 1.11955(6) 0.22213(5) 0.38182(5) 0.0394(3) Uani 1 1 d . . . . .
S11B S 1.09599(5) -0.07514(5) 0.31343(4) 0.0351(3) Uani 1 1 d . . . . .
S12B S 0.87247(6) 0.07673(5) 0.32649(4) 0.0379(3) Uani 1 1 d . . . . .
S13B S 0.89136(6) 0.25520(5) 0.37049(5) 0.0444(3) Uani 1 1 d . . . . .
S14B S 0.91276(7) 0.25450(6) 0.59357(5) 0.0500(4) Uani 1 1 d . . . . .
S15B S 1.24246(6) 0.02006(6) 0.34790(5) 0.0486(4) Uani 1 1 d . . . . .
S16B S 0.82647(7) 0.11499(6) 0.45357(5) 0.0558(4) Uani 1 1 d . . . . .
S17B S 0.83813(5) 0.11368(5) 0.57001(5) 0.0402(3) Uani 1 1 d . . . . .
S18B S 0.98218(7) 0.19576(6) 0.47744(5) 0.0522(4) Uani 1 1 d . . . . .
S19B S 0.96347(7) 0.11704(5) 0.54250(5) 0.0496(4) Uani 1 1 d . . . . .
S20B S 1.16377(7) 0.07165(6) 0.46596(5) 0.0471(3) Uani 1 1 d . . . . .
S21B S 0.73837(6) -0.01801(6) 0.42878(5) 0.0457(4) Uani 1 1 d . . . . .
S22B S 1.03164(6) 0.07307(5) 0.37651(4) 0.0365(3) Uani 1 1 d . . . . .
S23B S 0.94974(8) -0.07095(7) 0.40750(5) 0.0628(4) Uani 1 1 d . . . . .
S24B S 0.95130(8) 0.11696(7) 0.44169(6) 0.0643(4) Uani 1 1 d . . . . .
S25B S 1.11069(7) 0.00768(6) 0.43132(6) 0.0610(4) Uani 1 1 d . . . . .
S2C S 1.0000 0.0000 0.5000 0.0754(8) Uani 1 2 d S . P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O3A 2.056(4) . ?
Ag1 S13A 2.3252(13) . ?
Ag1 S7A 2.3820(14) . ?
Ag1 Ag4 2.8928(7) . ?
Ag1 Cu4A 2.9283(8) . ?
Ag1 Ag14 2.9491(8) . ?
Ag1 Ag2 3.2777(7) . ?
Ag1 Ag3 3.2926(8) . ?
Ag2 O1A 2.335(4) . ?
Ag2 S19A 2.4581(18) . ?
Ag2 S18A 2.5730(14) 2_665 ?
Ag2 S7A 2.7097(15) . ?
Ag2 Ag10 2.9843(6) . ?
Ag2 Ag21 3.3439(9) 2_665 ?
Ag3 O2A 2.450(5) . ?
Ag3 S24A 2.4508(14) . ?
Ag3 S17A 2.5749(14) 2_665 ?
Ag3 S7A 2.7652(15) . ?
Ag3 Ag8 2.8993(7) . ?
Ag3 Cu2A 3.1462(8) . ?
Ag4 O4A 2.448(3) . ?
Ag4 S24A 2.4606(17) . ?
Ag4 S13A 2.5854(15) . ?
Ag4 S8A 2.7256(12) . ?
Ag4 Ag5 3.2932(7) . ?
Ag5 O5A 2.151(4) . ?
Ag5 S8A 2.3160(15) . ?
Ag5 S15A 2.3217(16) 2_665 ?
Ag5 Ag7 2.8705(7) . ?
Ag5 Ag11 2.8813(7) 2_665 ?
Ag5 Cu1A 3.0049(8) . ?
Ag5 Ag6 3.2775(8) . ?
Ag6 O6A 2.428(3) . ?
Ag6 S21A 2.4449(14) . ?
Ag6 S14A 2.5995(16) . ?
Ag6 S8A 2.7308(12) . ?
Ag6 Ag17 2.9094(7) . ?
Ag7 O7A 2.452(4) . ?
Ag7 S24A 2.4600(15) . ?
Ag7 S15A 2.5926(12) 2_665 ?
Ag7 S9A 2.7236(13) . ?
Ag7 Ag8 3.3194(6) . ?
Ag8 O8A 2.068(5) . ?
Ag8 S9A 2.3027(14) . ?
Ag8 S17A 2.3016(14) 2_665 ?
Ag8 Cu2A 2.8414(10) . ?
Ag8 Ag16 2.9137(6) 2_665 ?
Ag8 Ag9 3.2927(7) . ?
Ag9 S20A 2.4641(13) 2_665 ?
Ag9 O9A 2.475(3) . ?
Ag9 S16A 2.5578(14) 2_665 ?
Ag9 S9A 2.7163(16) . ?
Ag9 Ag13 2.9183(6) 2_665 ?
Ag10 O10A 2.033(5) . ?
Ag10 S18A 2.3569(14) 2_665 ?
Ag10 S10A 2.4838(14) . ?
Ag10 Ag18 2.9443(8) 2_665 ?
Ag10 Ag19 3.1977(8) . ?
Ag10 Ag12 3.2329(7) . ?
Ag10 Ag11 3.3139(6) . ?
Ag11 O11A 2.338(4) . ?
Ag11 S21A 2.4241(17) 2_665 ?
Ag11 S15A 2.5529(13) . ?
Ag11 S10A 2.7805(13) . ?
Ag11 Ag5 2.8813(7) 2_665 ?
Ag12 O12A 2.393(4) . ?
Ag12 S19A 2.4692(13) . ?
Ag12 S16A 2.5963(16) . ?
Ag12 S10A 2.7539(15) . ?
Ag12 Ag13 2.9335(7) . ?
Ag12 Ag20 3.3314(6) . ?
Ag13 O13A 2.138(4) . ?
Ag13 S16A 2.3081(14) . ?
Ag13 S11A 2.3471(16) . ?
Ag13 Cu6A 2.8906(11) 2_665 ?
Ag13 Ag9 2.9183(6) 2_665 ?
Ag13 Ag14 3.2182(6) . ?
Ag13 Ag15 3.3254(6) . ?
Ag14 O14A 2.410(4) . ?
Ag14 S19A 2.4531(14) . ?
Ag14 S13A 2.5776(12) . ?
Ag14 S11A 2.7093(13) . ?
Ag14 Cu4A 3.1414(9) . ?
Ag15 O15A 2.446(3) . ?
Ag15 S20A 2.4487(13) . ?
Ag15 S14A 2.5668(13) . ?
Ag15 S11A 2.7387(14) . ?
Ag15 Ag17 2.9304(7) . ?
Ag16 S20A 2.4622(16) . ?
Ag16 O16A 2.515(3) . ?
Ag16 S17A 2.5684(12) . ?
Ag16 S12A 2.7229(16) . ?
Ag16 Ag8 2.9138(6) 2_665 ?
Ag16 Ag17 3.2964(6) . ?
Ag16 Ag21 3.3788(8) . ?
Ag17 O17A 2.137(4) . ?
Ag17 S14A 2.3186(12) . ?
Ag17 S12A 2.3380(14) . ?
Ag17 Cu3A 2.9936(9) . ?
Ag17 Ag18 3.3336(7) . ?
Ag18 S21A 2.4479(12) . ?
Ag18 O18A 2.498(4) . ?
Ag18 S18A 2.5627(11) . ?
Ag18 S12A 2.7533(14) . ?
Ag18 Ag10 2.9442(8) 2_665 ?
Ag19 S25A 2.0859(17) 2_665 ?
Ag19 S10A 2.4609(16) . ?
Ag19 S7A 2.5690(13) . ?
Ag19 S12A 2.6178(16) 2_665 ?
Ag19 Cu2A 2.8795(9) . ?
Ag19 S1C 2.9465(5) . ?
Ag19 Cu4A 3.0284(8) . ?
Ag19 Cu6A 3.0910(11) 2_665 ?
Ag19 Cu3A 3.2127(10) 2_665 ?
Ag20 S16A 2.4352(15) . ?
Ag20 S15A 2.4384(13) . ?
Ag21 S17A 2.4205(15) . ?
Ag21 S18A 2.4542(16) . ?
Ag21 Ag2 3.3440(9) 2_665 ?
Cu1A S23A 1.8772(15) . ?
Cu1A S25A 2.031(2) . ?
Cu1A S8A 2.4515(14) . ?
Cu1A S9A 2.5749(16) . ?
Cu1A S10A 2.6009(14) 2_665 ?
Cu1A Cu6A 2.8705(11) . ?
Cu1A Cu2A 3.0031(10) . ?
Cu2A S23A 1.7017(15) . ?
Cu2A S9A 2.2304(16) . ?
Cu2A S7A 2.3730(16) . ?
Cu2A S22A 2.3860(16) . ?
Cu3A S22A 2.0283(16) 2_665 ?
Cu3A S25A 2.064(2) . ?
Cu3A S12A 2.4156(13) . ?
Cu3A S8A 2.5655(13) . ?
Cu3A S11A 2.6698(16) . ?
Cu3A Cu4A 2.9406(9) . ?
Cu3A Ag19 3.2127(10) 2_665 ?
Cu4A S7A 2.2678(15) . ?
Cu4A S23A 2.3708(18) . ?
Cu4A S11A 2.4194(16) . ?
Cu4A Cu6A 2.8368(11) 2_665 ?
Cu5A S13A 2.4186(12) . ?
Cu5A S14A 2.4251(12) . ?
Cu6A S22A 2.3318(16) . ?
Cu6A S11A 2.3425(12) 2_665 ?
Cu6A S10A 2.3908(14) 2_665 ?
Cu6A Cu4A 2.8368(11) 2_665 ?
Cu6A Ag13 2.8907(11) 2_665 ?
Cu6A Ag19 3.0910(11) 2_665 ?
C1A C4A 1.491(8) . ?
C1A C2A 1.503(7) . ?
C1A C3A 1.508(9) . ?
C1A S1A 1.596(5) . ?
C2A H2A1 0.9800 . ?
C2A H2A2 0.9800 . ?
C2A H2A3 0.9800 . ?
C3A H3A1 0.9800 . ?
C3A H3A2 0.9800 . ?
C3A H3A3 0.9800 . ?
C4A H4AA 0.9800 . ?
C4A H4AB 0.9800 . ?
C4A H4AC 0.9800 . ?
C5A C6A 1.529(7) . ?
C5A C8A 1.554(8) . ?
C5A C7A 1.591(8) . ?
C5A S2A 1.878(5) . ?
C6A H6A1 0.9800 . ?
C6A H6A2 0.9800 . ?
C6A H6A3 0.9800 . ?
C7A H7A1 0.9800 . ?
C7A H7A2 0.9800 . ?
C7A H7A3 0.9800 . ?
C8A H8A1 0.9800 . ?
C8A H8A2 0.9800 . ?
C8A H8A3 0.9800 . ?
C9A C11A 1.490(8) . ?
C9A C12A 1.484(6) . ?
C9A C10A 1.564(7) . ?
C9A S3A 1.831(6) . ?
C10A H10A 0.9800 . ?
C10A H10B 0.9800 . ?
C10A H10C 0.9800 . ?
C11A H11A 0.9800 . ?
C11A H11B 0.9800 . ?
C11A H11C 0.9800 . ?
C12A H12A 0.9800 . ?
C12A H12B 0.9800 . ?
C12A H12C 0.9800 . ?
C13A C16A 1.490(7) . ?
C13A C15A 1.543(8) . ?
C13A C14A 1.566(7) . ?
C13A S4A 1.775(6) . ?
C14A H14A 0.9800 . ?
C14A H14B 0.9800 . ?
C14A H14C 0.9800 . ?
C15A H15A 0.9800 . ?
C15A H15B 0.9800 . ?
C15A H15C 0.9800 . ?
C16A H16A 0.9800 . ?
C16A H16B 0.9800 . ?
C16A H16C 0.9800 . ?
C17A C18A 1.512(8) . ?
C17A C20A 1.529(8) . ?
C17A C19A 1.550(8) . ?
C17A S5A 1.785(7) . ?
C18A H18A 0.9800 . ?
C18A H18B 0.9800 . ?
C18A H18C 0.9800 . ?
C19A H19A 0.9800 . ?
C19A H19B 0.9800 . ?
C19A H19C 0.9800 . ?
C20A H20A 0.9800 . ?
C20A H20B 0.9800 . ?
C20A H20C 0.9800 . ?
C21A C22A 1.504(9) . ?
C21A C24A 1.534(7) . ?
C21A C23A 1.569(8) . ?
C21A S6A 1.805(5) . ?
C22A H22A 0.9800 . ?
C22A H22B 0.9800 . ?
C22A H22C 0.9800 . ?
C23A H23A 0.9800 . ?
C23A H23B 0.9800 . ?
C23A H23C 0.9800 . ?
C24A H24A 0.9800 . ?
C24A H24B 0.9800 . ?
C24A H24C 0.9800 . ?
C25A C27A 1.487(7) . ?
C25A C26A 1.544(7) . ?
C25A C28A 1.608(7) . ?
C25A S13A 1.903(4) . ?
C26A H26A 0.9800 . ?
C26A H26B 0.9800 . ?
C26A H26C 0.9800 . ?
C27A H27A 0.9800 . ?
C27A H27B 0.9800 . ?
C27A H27C 0.9800 . ?
C28A H28A 0.9800 . ?
C28A H28B 0.9800 . ?
C28A H28C 0.9800 . ?
C29A C31A 1.457(7) . ?
C29A C30A 1.459(7) . ?
C29A C32A 1.599(7) . ?
C29A S14A 1.893(5) . ?
C30A H30A 0.9800 . ?
C30A H30B 0.9800 . ?
C30A H30C 0.9800 . ?
C31A H31A 0.9800 . ?
C31A H31B 0.9800 . ?
C31A H31C 0.9800 . ?
C32A H32A 0.9800 . ?
C32A H32B 0.9800 . ?
C32A H32C 0.9800 . ?
C33A C34A 1.499(7) . ?
C33A C36A 1.540(8) . ?
C33A C35A 1.539(6) . ?
C33A S19A 2.001(5) . ?
C34A H34A 0.9800 . ?
C34A H34B 0.9800 . ?
C34A H34C 0.9800 . ?
C35A H35A 0.9800 . ?
C35A H35B 0.9800 . ?
C35A H35C 0.9800 . ?
C36A H36A 0.9800 . ?
C36A H36B 0.9800 . ?
C36A H36C 0.9800 . ?
C37A C38A 1.516(7) . ?
C37A C39A 1.518(6) . ?
C37A C40A 1.549(9) . ?
C37A S15A 1.884(5) . ?
C38A H38A 0.9800 . ?
C38A H38B 0.9800 . ?
C38A H38C 0.9800 . ?
C39A H39A 0.9800 . ?
C39A H39B 0.9800 . ?
C39A H39C 0.9800 . ?
C40A H40A 0.9800 . ?
C40A H40B 0.9800 . ?
C40A H40C 0.9800 . ?
C41A C43A 1.471(9) . ?
C41A C42A 1.495(9) . ?
C41A C44A 1.518(8) . ?
C41A S16A 1.847(7) . ?
C42A H42A 0.9800 . ?
C42A H42B 0.9800 . ?
C42A H42C 0.9800 . ?
C43A H43D 0.9800 . ?
C43A H43E 0.9800 . ?
C43A H43F 0.9800 . ?
C44A H44A 0.9800 . ?
C44A H44B 0.9800 . ?
C44A H44C 0.9800 . ?
C45A C47A 1.454(6) . ?
C45A C48A 1.541(8) . ?
C45A C46A 1.555(8) . ?
C45A S17A 1.903(5) . ?
C46A H46A 0.9800 . ?
C46A H46B 0.9800 . ?
C46A H46C 0.9800 . ?
C47A H47A 0.9800 . ?
C47A H47B 0.9800 . ?
C47A H47C 0.9800 . ?
C48A H48A 0.9800 . ?
C48A H48B 0.9800 . ?
C48A H48C 0.9800 . ?
C49A C52A 1.532(7) . ?
C49A C50A 1.544(7) . ?
C49A C51A 1.594(8) . ?
C49A S18A 1.830(5) . ?
C50A H50A 0.9800 . ?
C50A H50B 0.9800 . ?
C50A H50C 0.9800 . ?
C51A H51A 0.9800 . ?
C51A H51B 0.9800 . ?
C51A H51C 0.9800 . ?
C52A H52A 0.9800 . ?
C52A H52B 0.9800 . ?
C52A H52C 0.9800 . ?
C53A C56A 1.516(7) . ?
C53A C54A 1.544(7) . ?
C53A C55A 1.586(6) . ?
C53A S20A 1.920(6) . ?
C54A H54A 0.9800 . ?
C54A H54B 0.9800 . ?
C54A H54C 0.9800 . ?
C55A H55A 0.9800 . ?
C55A H55B 0.9800 . ?
C55A H55C 0.9800 . ?
C56A H56A 0.9800 . ?
C56A H56B 0.9800 . ?
C56A H56C 0.9800 . ?
C57A C58A 1.456(9) . ?
C57A C60A 1.503(7) . ?
C57A C59A 1.540(8) . ?
C57A S21A 1.936(5) . ?
C58A H58A 0.9800 . ?
C58A H58B 0.9800 . ?
C58A H58C 0.9800 . ?
C59A H59A 0.9800 . ?
C59A H59B 0.9800 . ?
C59A H59C 0.9800 . ?
C60A H60A 0.9800 . ?
C60A H60B 0.9800 . ?
C60A H60C 0.9800 . ?
C61A C63A 1.540(8) . ?
C61A C64A 1.569(9) . ?
C61A C62A 1.590(8) . ?
C61A S24A 1.885(5) . ?
C62A H62A 0.9800 . ?
C62A H62B 0.9800 . ?
C62A H62C 0.9800 . ?
C63A H63A 0.9800 . ?
C63A H63B 0.9800 . ?
C63A H63C 0.9800 . ?
C64A H64A 0.9800 . ?
C64A H64B 0.9800 . ?
C64A H64C 0.9800 . ?
O1A S1A 1.495(5) . ?
O2A S1A 1.362(5) . ?
O3A S1A 1.560(5) . ?
O4A S2A 1.494(4) . ?
O5A S2A 1.420(4) . ?
O6A S2A 1.433(4) . ?
O7A S3A 1.420(4) . ?
O8A S3A 1.401(4) . ?
O9A S3A 1.495(4) . ?
O10A S4A 1.499(5) . ?
O11A S4A 1.497(4) . ?
O12A S4A 1.303(5) . ?
O13A S5A 1.412(4) . ?
O14A S5A 1.412(4) . ?
O15A S5A 1.458(4) . ?
O16A S6A 1.407(4) . ?
O17A S6A 1.486(4) . ?
O18A S6A 1.392(5) . ?
S10A Cu6A 2.3908(14) 2_665 ?
S10A S25A 2.458(3) 2_665 ?
S10A Cu1A 2.6008(14) 2_665 ?
S11A Cu6A 2.3426(12) 2_665 ?
S12A Ag19 2.6178(16) 2_665 ?
S15A Ag5 2.3219(16) 2_665 ?
S15A Ag7 2.5925(12) 2_665 ?
S16A Ag9 2.5579(14) 2_665 ?
S17A Ag8 2.3017(14) 2_665 ?
S17A Ag3 2.5748(14) 2_665 ?
S18A Ag10 2.3568(14) 2_665 ?
S18A Ag2 2.5730(14) 2_665 ?
S20A Ag9 2.4641(13) 2_665 ?
S21A Ag11 2.4241(17) 2_665 ?
S22A Cu3A 2.0283(16) 2_665 ?
S25A Ag19 2.0859(17) 2_665 ?
S25A S10A 2.458(3) 2_665 ?
S1C Ag19 2.9465(5) 2_665 ?
Ag23 O1B 2.422(4) . ?
Ag23 S21B 2.4563(14) . ?
Ag23 S7B 2.5890(16) . ?
Ag23 S16B 2.7483(15) . ?
Ag23 Ag39 2.9106(8) 2_756 ?
Ag23 Ag25 3.3082(7) . ?
Ag24 O2B 2.415(4) . ?
Ag24 S13B 2.4328(15) . ?
Ag24 S8B 2.5645(15) . ?
Ag24 S16B 2.7204(14) . ?
Ag24 Ag26 2.8900(7) . ?
Ag24 Ag25 3.2822(6) . ?
Ag25 O3B 2.205(4) . ?
Ag25 S12B 2.3748(14) . ?
Ag25 S16B 2.4342(19) . ?
Ag25 Cu4B 2.8831(12) . ?
Ag25 Ag31 2.9314(6) . ?
Ag25 Ag32 2.9925(6) . ?
Ag26 O4B 2.127(3) . ?
Ag26 S18B 2.2850(14) . ?
Ag26 S8B 2.2925(12) . ?
Ag26 Ag37 2.8873(7) . ?
Ag26 Cu2B 2.9809(8) . ?
Ag26 Ag27 3.2727(7) . ?
Ag26 Ag28 3.2822(7) . ?
Ag27 S14B 2.4654(16) . ?
Ag27 O5B 2.477(4) . ?
Ag27 S9B 2.5737(12) . ?
Ag27 S18B 2.7222(16) . ?
Ag27 Ag34 2.9487(7) 2_756 ?
Ag28 O6B 2.422(3) . ?
Ag28 S13B 2.4600(14) . ?
Ag28 S10B 2.5916(13) . ?
Ag28 S18B 2.7445(17) . ?
Ag28 Ag29 2.9053(6) . ?
Ag29 O7B 2.137(4) . ?
Ag29 S10B 2.3064(13) . ?
Ag29 S22B 2.3254(12) . ?
Ag29 Ag40 2.8665(7) . ?
Ag29 Cu3B 2.8903(10) . ?
Ag29 Ag31 3.2965(6) . ?
Ag29 Ag30 3.3104(6) . ?
Ag30 S15B 2.4449(15) . ?
Ag30 O8B 2.469(4) . ?
Ag30 S11B 2.5731(11) . ?
Ag30 S22B 2.7177(12) . ?
Ag30 Ag36 2.8894(6) 2_756 ?
Ag31 S13B 2.4781(13) . ?
Ag31 O9B 2.488(4) . ?
Ag31 S12B 2.5796(12) . ?
Ag31 S22B 2.7035(13) . ?
Ag31 Ag43 3.3638(6) . ?
Ag32 O10B 2.447(4) . ?
Ag32 S21B 2.4473(14) . ?
Ag32 S12B 2.5658(13) . ?
Ag32 S23B 2.7313(17) . ?
Ag32 Cu4B 2.9858(11) . ?
Ag32 Ag34 3.2884(6) . ?
Ag32 Ag43 3.3738(7) . ?
Ag33 S14B 2.4355(15) 2_756 ?
Ag33 O11B 2.490(4) . ?
Ag33 S11B 2.5551(12) . ?
Ag33 S23B 2.7668(16) . ?
Ag33 Ag36 2.9294(6) 2_756 ?
Ag33 Ag34 3.2772(6) . ?
Ag34 O12B 2.196(4) . ?
Ag34 S23B 2.3563(17) . ?
Ag34 S9B 2.3593(14) 2_756 ?
Ag34 Cu5B 2.8674(10) 2_756 ?
Ag34 Ag38 2.9142(7) 2_756 ?
Ag34 Ag27 2.9485(7) 2_756 ?
Ag35 O13B 2.418(3) . ?
Ag35 S15B 2.4482(15) 2_756 ?
Ag35 S7B 2.5750(16) . ?
Ag35 S17B 2.7237(12) . ?
Ag35 Ag39 2.9095(7) 2_756 ?
Ag35 Ag36 3.3060(7) . ?
Ag36 O14B 2.078(4) . ?
Ag36 S11B 2.3139(15) 2_756 ?
Ag36 S17B 2.3505(17) . ?
Ag36 Ag30 2.8895(6) 2_756 ?
Ag36 Ag33 2.9293(6) 2_756 ?
Ag36 Cu1B 3.0598(9) . ?
Ag36 Ag37 3.3048(7) . ?
Ag37 O15B 2.410(4) . ?
Ag37 S14B 2.4567(16) . ?
Ag37 S8B 2.5885(16) . ?
Ag37 S17B 2.7435(11) . ?
Ag38 O16B 2.374(4) . ?
Ag38 S21B 2.4605(15) 2_756 ?
Ag38 S9B 2.5926(11) . ?
Ag38 S20B 2.7457(16) . ?
Ag38 Ag34 2.9143(7) 2_756 ?
Ag38 Cu5B 3.0729(10) . ?
Ag38 Ag39 3.2598(7) . ?
Ag39 O17B 2.084(4) . ?
Ag39 S7B 2.3310(12) 2_756 ?
Ag39 S20B 2.3774(14) . ?
Ag39 Ag35 2.9093(7) 2_756 ?
Ag39 Ag23 2.9106(7) 2_756 ?
Ag39 Ag41 3.0433(7) . ?
Ag39 Ag40 3.2779(7) . ?
Ag40 O18B 2.431(3) . ?
Ag40 S15B 2.4450(15) . ?
Ag40 S10B 2.5725(12) . ?
Ag40 S20B 2.7568(16) . ?
Ag41 S25B 1.995(2) . ?
Ag41 S20B 2.4417(13) . ?
Ag41 S16B 2.5857(18) 2_756 ?
Ag41 S17B 2.6421(15) 2_756 ?
Ag41 Cu2B 2.6443(8) 2_756 ?
Ag41 S2C 2.9490(6) . ?
Ag41 Cu4B 2.9681(14) 2_756 ?
Ag41 Cu5B 3.0676(9) . ?
Ag41 Cu3B 3.1468(9) . ?
Ag42 S9B 2.4125(16) . ?
Ag42 S10B 2.4393(16) . ?
Ag43 S12B 2.4302(12) . ?
Ag43 S11B 2.4355(12) . ?
Cu7B S9B 2.4125(16) . ?
Cu7B S10B 2.4393(16) . ?
Cu8B S12B 2.4302(12) . ?
Cu8B S11B 2.4355(12) . ?
Cu1B S25B 1.9685(17) 2_756 ?
Cu1B S19B 2.1010(15) . ?
Cu1B S17B 2.4176(13) . ?
Cu1B S22B 2.5575(14) 2_756 ?
Cu1B S23B 2.6274(19) 2_756 ?
Cu2B S24B 1.979(2) . ?
Cu2B S19B 2.1010(19) . ?
Cu2B S18B 2.4288(15) . ?
Cu2B S16B 2.5597(19) . ?
Cu2B S17B 2.6239(17) . ?
Cu2B Ag41 2.6443(8) 2_756 ?
Cu3B S25B 1.8237(15) . ?
Cu3B S24B 2.1989(18) . ?
Cu3B S22B 2.3695(17) . ?
Cu3B S20B 2.4436(17) . ?
Cu4B S16B 2.2466(16) . ?
Cu4B S23B 2.3250(18) . ?
Cu4B Cu5B 2.6240(15) 2_756 ?
Cu4B S24B 2.6587(19) . ?
Cu4B Ag41 2.9682(14) 2_756 ?
Cu5B S23B 2.288(2) 2_756 ?
Cu5B S19B 2.3318(16) . ?
Cu5B S20B 2.3580(17) . ?
Cu5B Cu4B 2.6241(15) 2_756 ?
Cu5B Ag34 2.8675(10) 2_756 ?
Cu6B S7B 2.4216(13) . ?
Cu6B S8B 2.4389(12) . ?
C1B C3B 1.543(8) . ?
C1B C2B 1.541(8) . ?
C1B C4B 1.596(8) . ?
C1B S5B 1.787(6) . ?
C2B H2B1 0.9800 . ?
C2B H2B2 0.9800 . ?
C2B H2B3 0.9800 . ?
C3B H3BA 0.9800 . ?
C3B H3BB 0.9800 . ?
C3B H3BC 0.9800 . ?
C4B H4B1 0.9800 . ?
C4B H4B2 0.9800 . ?
C4B H4B3 0.9800 . ?
C5B C6B 1.484(7) . ?
C5B C7B 1.506(8) . ?
C5B C8B 1.610(9) . ?
C5B S2B 1.743(6) . ?
C6B H6BA 0.9800 . ?
C6B H6BB 0.9800 . ?
C6B H6BC 0.9800 . ?
C7B H7B1 0.9800 . ?
C7B H7B2 0.9800 . ?
C7B H7B3 0.9800 . ?
C8B H8B1 0.9800 . ?
C8B H8B2 0.9800 . ?
C8B H8B3 0.9800 . ?
C9B C10B 1.502(6) . ?
C9B C11B 1.538(7) . ?
C9B C12B 1.548(8) . ?
C9B S3B 1.789(6) . ?
C10B H10D 0.9800 . ?
C10B H10E 0.9800 . ?
C10B H10F 0.9800 . ?
C11B H11D 0.9800 . ?
C11B H11E 0.9800 . ?
C11B H11F 0.9800 . ?
C12B H12D 0.9800 . ?
C12B H12E 0.9800 . ?
C12B H12F 0.9800 . ?
C13B C14B 1.528(9) . ?
C13B C16B 1.544(8) . ?
C13B C15B 1.552(8) . ?
C13B S4B 1.767(7) . ?
C14B H14D 0.9800 . ?
C14B H14E 0.9800 . ?
C14B H14F 0.9800 . ?
C15B H15D 0.9800 . ?
C15B H15E 0.9800 . ?
C15B H15F 0.9800 . ?
C16B H16D 0.9800 . ?
C16B H16E 0.9800 . ?
C16B H16F 0.9800 . ?
C17B C18B 1.510(7) . ?
C17B C20B 1.505(8) . ?
C17B C19B 1.547(8) . ?
C17B S1B 1.732(7) . ?
C18B H18D 0.9800 . ?
C18B H18E 0.9800 . ?
C18B H18F 0.9800 . ?
C19B H19D 0.9800 . ?
C19B H19E 0.9800 . ?
C19B H19F 0.9800 . ?
C20B H20D 0.9800 . ?
C20B H20E 0.9800 . ?
C20B H20F 0.9800 . ?
C21B C23B 1.509(7) . ?
C21B C22B 1.555(9) . ?
C21B C24B 1.564(8) . ?
C21B S6B 1.796(6) . ?
C22B H22D 0.9800 . ?
C22B H22E 0.9800 . ?
C22B H22F 0.9800 . ?
C23B H23D 0.9800 . ?
C23B H23E 0.9800 . ?
C23B H23F 0.9800 . ?
C24B H24D 0.9800 . ?
C24B H24E 0.9800 . ?
C24B H24F 0.9800 . ?
C25B C28B 1.489(8) . ?
C25B C27B 1.551(9) . ?
C25B C26B 1.563(8) . ?
C25B S7B 1.868(5) . ?
C26B H26D 0.9800 . ?
C26B H26E 0.9800 . ?
C26B H26F 0.9800 . ?
C27B H27D 0.9800 . ?
C27B H27E 0.9800 . ?
C27B H27F 0.9800 . ?
C28B H28D 0.9800 . ?
C28B H28E 0.9800 . ?
C28B H28F 0.9800 . ?
C29B C32B 1.484(9) . ?
C29B C30B 1.494(9) . ?
C29B C31B 1.510(7) . ?
C29B S15B 1.812(6) . ?
C30B H30D 0.9800 . ?
C30B H30E 0.9800 . ?
C30B H30F 0.9800 . ?
C31B H31D 0.9800 . ?
C31B H31E 0.9800 . ?
C31B H31F 0.9800 . ?
C32B H32D 0.9800 . ?
C32B H32E 0.9800 . ?
C32B H32F 0.9800 . ?
C33B C36B 1.499(7) . ?
C33B C34B 1.523(8) . ?
C33B C35B 1.542(7) . ?
C33B S10B 1.822(5) . ?
C34B H34D 0.9800 . ?
C34B H34E 0.9800 . ?
C34B H34F 0.9800 . ?
C35B H35D 0.9800 . ?
C35B H35E 0.9800 . ?
C35B H35F 0.9800 . ?
C36B H36D 0.9800 . ?
C36B H36E 0.9800 . ?
C36B H36F 0.9800 . ?
C37B C40B 1.470(7) . ?
C37B C39B 1.515(8) . ?
C37B C38B 1.519(8) . ?
C37B S13B 1.932(6) . ?
C38B H38D 0.9800 . ?
C38B H38E 0.9800 . ?
C38B H38F 0.9800 . ?
C39B H39D 0.9800 . ?
C39B H39E 0.9800 . ?
C39B H39F 0.9800 . ?
C40B H40D 0.9800 . ?
C40B H40E 0.9800 . ?
C40B H40F 0.9800 . ?
C41B C44B 1.468(7) . ?
C41B C43B 1.491(7) . ?
C41B C42B 1.579(7) . ?
C41B S12B 1.875(6) . ?
C42B H42D 0.9800 . ?
C42B H42E 0.9800 . ?
C42B H42F 0.9800 . ?
C43B H43A 0.9800 . ?
C43B H43B 0.9800 . ?
C43B H43C 0.9800 . ?
C44B H44D 0.9800 . ?
C44B H44E 0.9800 . ?
C44B H44F 0.9800 . ?
C45B C46B 1.509(9) . ?
C45B C47B 1.565(8) . ?
C45B C48B 1.5021(15) . ?
C45B S21B 1.863(6) . ?
C46B H46D 0.9800 . ?
C46B H46E 0.9800 . ?
C46B H46F 0.9800 . ?
C47B H47D 0.9800 . ?
C47B H47E 0.9800 . ?
C47B H47F 0.9800 . ?
C48B H48D 0.9800 . ?
C48B H48E 0.9800 . ?
C48B H48F 0.9800 . ?
C49B C59B 1.482(8) . ?
C49B C58B 1.521(8) . ?
C49B C60B 1.556(8) . ?
C49B S14B 1.903(5) . ?
C50B C53B 1.493(8) . ?
C50B H50D 0.9800 . ?
C50B H50E 0.9800 . ?
C50B H50F 0.9800 . ?
C51B C53B 1.494(6) . ?
C51B H51D 0.9800 . ?
C51B H51E 0.9800 . ?
C51B H51F 0.9800 . ?
C52B C53B 1.538(6) . ?
C52B H52D 0.9800 . ?
C52B H52E 0.9800 . ?
C52B H52F 0.9800 . ?
C53B S11B 1.927(6) . ?
C54B C57B 1.521(8) . ?
C54B H54D 0.9800 . ?
C54B H54E 0.9800 . ?
C54B H54F 0.9800 . ?
C55B C57B 1.497(7) . ?
C55B H55D 0.9800 . ?
C55B H55E 0.9800 . ?
C55B H55F 0.9800 . ?
C56B C57B 1.496(7) . ?
C56B H56D 0.9800 . ?
C56B H56E 0.9800 . ?
C56B H56F 0.9800 . ?
C57B S9B 1.880(4) . ?
C58B H58D 0.9800 . ?
C58B H58E 0.9800 . ?
C58B H58F 0.9800 . ?
C59B H59D 0.9800 . ?
C59B H59E 0.9800 . ?
C59B H59F 0.9800 . ?
C60B H60D 0.9800 . ?
C60B H60E 0.9800 . ?
C60B H60F 0.9800 . ?
C61B C62B 1.472(8) . ?
C61B C63B 1.522(8) . ?
C61B C64B 1.564(8) . ?
C61B S8B 1.912(6) . ?
C62B H62D 0.9800 . ?
C62B H62E 0.9800 . ?
C62B H62F 0.9800 . ?
C63B H63D 0.9800 . ?
C63B H63E 0.9800 . ?
C63B H63F 0.9800 . ?
C64B H64D 0.9800 . ?
C64B H64E 0.9800 . ?
C64B H64F 0.9800 . ?
O1B S1B 1.407(4) . ?
O2B S1B 1.436(4) . ?
O3B S1B 1.418(4) . ?
O4B S2B 1.417(3) . ?
O5B S2B 1.441(4) . ?
O6B S2B 1.500(4) . ?
O7B S3B 1.420(4) . ?
O8B S3B 1.397(3) . ?
O9B S3B 1.438(3) . ?
O10B S4B 1.379(4) . ?
O11B S4B 1.410(4) . ?
O12B S4B 1.456(4) . ?
O13B S5B 1.445(3) . ?
O14B S5B 1.473(4) . ?
O15B S5B 1.444(4) . ?
O16B S6B 1.414(4) . ?
O17B S6B 1.435(4) . ?
O18B S6B 1.438(4) . ?
S7B Ag39 2.3311(12) 2_756 ?
S9B Ag34 2.3594(14) 2_756 ?
S11B Ag36 2.3139(15) 2_756 ?
S14B Ag33 2.4355(15) 2_756 ?
S15B Ag35 2.4481(15) 2_756 ?
S16B Ag41 2.5857(18) 2_756 ?
S17B Ag41 2.6421(15) 2_756 ?
S21B Ag38 2.4606(15) 2_756 ?
S22B Cu1B 2.5575(14) 2_756 ?
S23B Cu5B 2.288(2) 2_756 ?
S23B Cu1B 2.6272(19) 2_756 ?
S25B Cu1B 1.9685(17) 2_756 ?
S2C Ag41 2.9491(6) 2_756 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3A Ag1 S13A 108.80(12) . . ?
O3A Ag1 S7A 116.37(12) . . ?
S13A Ag1 S7A 134.82(4) . . ?
O3A Ag1 Ag4 113.14(11) . . ?
S13A Ag1 Ag4 58.19(3) . . ?
S7A Ag1 Ag4 102.26(3) . . ?
O3A Ag1 Cu4A 163.73(11) . . ?
S13A Ag1 Cu4A 85.90(3) . . ?
S7A Ag1 Cu4A 49.25(3) . . ?
Ag4 Ag1 Cu4A 80.22(2) . . ?
O3A Ag1 Ag14 117.07(13) . . ?
S13A Ag1 Ag14 57.05(3) . . ?
S7A Ag1 Ag14 99.57(4) . . ?
Ag4 Ag1 Ag14 106.55(2) . . ?
Cu4A Ag1 Ag14 64.62(2) . . ?
O3A Ag1 Ag2 84.42(11) . . ?
S13A Ag1 Ag2 133.14(3) . . ?
S7A Ag1 Ag2 54.47(3) . . ?
Ag4 Ag1 Ag2 156.35(2) . . ?
Cu4A Ag1 Ag2 80.29(2) . . ?
Ag14 Ag1 Ag2 76.679(18) . . ?
O3A Ag1 Ag3 80.61(13) . . ?
S13A Ag1 Ag3 137.18(3) . . ?
S7A Ag1 Ag3 55.57(4) . . ?
Ag4 Ag1 Ag3 79.460(19) . . ?
Cu4A Ag1 Ag3 93.41(2) . . ?
Ag14 Ag1 Ag3 155.02(2) . . ?
Ag2 Ag1 Ag3 88.467(18) . . ?
O1A Ag2 S19A 114.63(12) . . ?
O1A Ag2 S18A 95.04(11) . 2_665 ?
S19A Ag2 S18A 133.60(5) . 2_665 ?
O1A Ag2 S7A 98.54(12) . . ?
S19A Ag2 S7A 109.30(5) . . ?
S18A Ag2 S7A 99.87(5) 2_665 . ?
O1A Ag2 Ag10 139.72(10) . . ?
S19A Ag2 Ag10 87.61(3) . . ?
S18A Ag2 Ag10 49.51(3) 2_665 . ?
S7A Ag2 Ag10 105.26(3) . . ?
O1A Ag2 Ag1 75.09(10) . . ?
S19A Ag2 Ag1 84.25(3) . . ?
S18A Ag2 Ag1 139.77(4) 2_665 . ?
S7A Ag2 Ag1 45.67(3) . . ?
Ag10 Ag2 Ag1 143.27(2) . . ?
O1A Ag2 Ag21 80.36(12) . 2_665 ?
S19A Ag2 Ag21 163.21(3) . 2_665 ?
S18A Ag2 Ag21 46.80(4) 2_665 2_665 ?
S7A Ag2 Ag21 58.82(3) . 2_665 ?
Ag10 Ag2 Ag21 84.751(19) . 2_665 ?
Ag1 Ag2 Ag21 92.980(19) . 2_665 ?
O2A Ag3 S24A 117.26(11) . . ?
O2A Ag3 S17A 92.89(12) . 2_665 ?
S24A Ag3 S17A 139.25(5) . 2_665 ?
O2A Ag3 S7A 94.17(13) . . ?
S24A Ag3 S7A 106.49(5) . . ?
S17A Ag3 S7A 97.23(4) 2_665 . ?
O2A Ag3 Ag8 140.29(12) . . ?
S24A Ag3 Ag8 93.06(4) . . ?
S17A Ag3 Ag8 49.29(3) 2_665 . ?
S7A Ag3 Ag8 101.40(3) . . ?
O2A Ag3 Cu2A 135.66(12) . . ?
S24A Ag3 Cu2A 96.76(3) . . ?
S17A Ag3 Cu2A 75.87(3) 2_665 . ?
S7A Ag3 Cu2A 46.79(3) . . ?
Ag8 Ag3 Cu2A 55.89(2) . . ?
O2A Ag3 Ag1 73.80(13) . . ?
S24A Ag3 Ag1 80.60(4) . . ?
S17A Ag3 Ag1 136.97(3) 2_665 . ?
S7A Ag3 Ag1 45.28(3) . . ?
Ag8 Ag3 Ag1 140.14(2) . . ?
Cu2A Ag3 Ag1 85.61(2) . . ?
O4A Ag4 S24A 120.56(10) . . ?
O4A Ag4 S13A 91.08(10) . . ?
S24A Ag4 S13A 135.77(4) . . ?
O4A Ag4 S8A 94.06(9) . . ?
S24A Ag4 S8A 108.26(4) . . ?
S13A Ag4 S8A 98.38(4) . . ?
O4A Ag4 Ag1 138.61(9) . . ?
S24A Ag4 Ag1 89.15(3) . . ?
S13A Ag4 Ag1 49.84(3) . . ?
S8A Ag4 Ag1 103.58(3) . . ?
O4A Ag4 Ag5 77.21(9) . . ?
S24A Ag4 Ag5 82.42(3) . . ?
S13A Ag4 Ag5 138.13(3) . . ?
S8A Ag4 Ag5 44.02(3) . . ?
Ag1 Ag4 Ag5 139.362(19) . . ?
O5A Ag5 S8A 111.59(12) . . ?
O5A Ag5 S15A 110.25(12) . 2_665 ?
S8A Ag5 S15A 138.16(4) . 2_665 ?
O5A Ag5 Ag7 114.27(11) . . ?
S8A Ag5 Ag7 102.50(3) . . ?
S15A Ag5 Ag7 58.78(3) 2_665 . ?
O5A Ag5 Ag11 115.21(10) . 2_665 ?
S8A Ag5 Ag11 103.51(3) . 2_665 ?
S15A Ag5 Ag11 57.57(3) 2_665 2_665 ?
Ag7 Ag5 Ag11 108.50(2) . 2_665 ?
O5A Ag5 Cu1A 164.12(11) . . ?
S8A Ag5 Cu1A 52.96(3) . . ?
S15A Ag5 Cu1A 85.26(3) 2_665 . ?
Ag7 Ag5 Cu1A 70.23(2) . . ?
Ag11 Ag5 Cu1A 75.51(2) 2_665 . ?
O5A Ag5 Ag6 80.56(11) . . ?
S8A Ag5 Ag6 55.27(3) . . ?
S15A Ag5 Ag6 134.18(3) 2_665 . ?
Ag7 Ag5 Ag6 157.55(2) . . ?
Ag11 Ag5 Ag6 77.273(18) 2_665 . ?
Cu1A Ag5 Ag6 91.09(2) . . ?
O5A Ag5 Ag4 78.49(10) . . ?
S8A Ag5 Ag4 54.86(3) . . ?
S15A Ag5 Ag4 136.02(3) 2_665 . ?
Ag7 Ag5 Ag4 78.053(17) . . ?
Ag11 Ag5 Ag4 158.31(2) 2_665 . ?
Cu1A Ag5 Ag4 87.984(19) . . ?
Ag6 Ag5 Ag4 89.281(18) . . ?
O6A Ag6 S21A 114.85(9) . . ?
O6A Ag6 S14A 94.52(10) . . ?
S21A Ag6 S14A 137.46(4) . . ?
O6A Ag6 S8A 96.56(10) . . ?
S21A Ag6 S8A 109.01(5) . . ?
S14A Ag6 S8A 96.58(4) . . ?
O6A Ag6 Ag17 140.82(10) . . ?
S21A Ag6 Ag17 91.46(3) . . ?
S14A Ag6 Ag17 49.39(2) . . ?
S8A Ag6 Ag17 101.73(3) . . ?
O6A Ag6 Ag5 75.63(10) . . ?
S21A Ag6 Ag5 83.15(4) . . ?
S14A Ag6 Ag5 135.96(3) . . ?
S8A Ag6 Ag5 44.19(3) . . ?
Ag17 Ag6 Ag5 139.073(18) . . ?
O7A Ag7 S24A 115.92(9) . . ?
O7A Ag7 S15A 91.96(9) . 2_665 ?
S24A Ag7 S15A 137.69(5) . 2_665 ?
O7A Ag7 S9A 93.97(10) . . ?
S24A Ag7 S9A 108.86(4) . . ?
S15A Ag7 S9A 99.57(4) 2_665 . ?
O7A Ag7 Ag5 139.36(8) . . ?
S24A Ag7 Ag5 91.91(4) . . ?
S15A Ag7 Ag5 49.98(4) 2_665 . ?
S9A Ag7 Ag5 104.78(3) . . ?
O7A Ag7 Ag8 74.11(9) . . ?
S24A Ag7 Ag8 83.32(3) . . ?
S15A Ag7 Ag8 137.07(3) 2_665 . ?
S9A Ag7 Ag8 43.42(3) . . ?
Ag5 Ag7 Ag8 141.78(2) . . ?
O8A Ag8 S9A 111.51(12) . . ?
O8A Ag8 S17A 112.47(12) . 2_665 ?
S9A Ag8 S17A 136.02(5) . 2_665 ?
O8A Ag8 Cu2A 159.62(11) . . ?
S9A Ag8 Cu2A 50.06(4) . . ?
S17A Ag8 Cu2A 86.50(4) 2_665 . ?
O8A Ag8 Ag3 116.42(11) . . ?
S9A Ag8 Ag3 101.84(4) . . ?
S17A Ag8 Ag3 57.99(4) 2_665 . ?
Cu2A Ag8 Ag3 66.46(2) . . ?
O8A Ag8 Ag16 115.41(11) . 2_665 ?
S9A Ag8 Ag16 102.20(3) . 2_665 ?
S17A Ag8 Ag16 57.58(3) 2_665 2_665 ?
Cu2A Ag8 Ag16 80.51(2) . 2_665 ?
Ag3 Ag8 Ag16 107.71(2) . 2_665 ?
O8A Ag8 Ag9 79.37(11) . . ?
S9A Ag8 Ag9 54.68(4) . . ?
S17A Ag8 Ag9 134.97(3) 2_665 . ?
Cu2A Ag8 Ag9 92.58(2) . . ?
Ag3 Ag8 Ag9 156.33(2) . . ?
Ag16 Ag8 Ag9 77.833(16) 2_665 . ?
O8A Ag8 Ag7 81.14(11) . . ?
S9A Ag8 Ag7 54.38(3) . . ?
S17A Ag8 Ag7 134.32(3) 2_665 . ?
Cu2A Ag8 Ag7 80.08(2) . . ?
Ag3 Ag8 Ag7 76.691(17) . . ?
Ag16 Ag8 Ag7 156.18(2) 2_665 . ?
Ag9 Ag8 Ag7 89.389(16) . . ?
S20A Ag9 O9A 117.48(9) 2_665 . ?
S20A Ag9 S16A 137.34(4) 2_665 2_665 ?
O9A Ag9 S16A 90.59(9) . 2_665 ?
S20A Ag9 S9A 108.41(5) 2_665 . ?
O9A Ag9 S9A 94.55(10) . . ?
S16A Ag9 S9A 99.89(5) 2_665 . ?
S20A Ag9 Ag13 92.25(3) 2_665 2_665 ?
O9A Ag9 Ag13 137.63(8) . 2_665 ?
S16A Ag9 Ag13 49.32(3) 2_665 2_665 ?
S9A Ag9 Ag13 104.27(3) . 2_665 ?
S20A Ag9 Ag8 82.79(4) 2_665 . ?
O9A Ag9 Ag8 75.53(9) . . ?
S16A Ag9 Ag8 137.85(3) 2_665 . ?
S9A Ag9 Ag8 43.77(3) . . ?
Ag13 Ag9 Ag8 141.65(2) 2_665 . ?
O10A Ag10 S18A 114.73(14) . 2_665 ?
O10A Ag10 S10A 114.06(14) . . ?
S18A Ag10 S10A 131.20(5) 2_665 . ?
O10A Ag10 Ag18 119.73(13) . 2_665 ?
S18A Ag10 Ag18 56.52(3) 2_665 2_665 ?
S10A Ag10 Ag18 99.12(4) . 2_665 ?
O10A Ag10 Ag2 117.37(12) . . ?
S18A Ag10 Ag2 56.13(3) 2_665 . ?
S10A Ag10 Ag2 99.48(3) . . ?
Ag18 Ag10 Ag2 103.80(2) 2_665 . ?
O10A Ag10 Ag19 163.24(13) . . ?
S18A Ag10 Ag19 81.82(3) 2_665 . ?
S10A Ag10 Ag19 49.40(4) . . ?
Ag18 Ag10 Ag19 70.763(18) 2_665 . ?
Ag2 Ag10 Ag19 68.657(17) . . ?
O10A Ag10 Ag12 78.90(13) . . ?
S18A Ag10 Ag12 134.87(3) 2_665 . ?
S10A Ag10 Ag12 55.76(4) . . ?
Ag18 Ag10 Ag12 154.54(2) 2_665 . ?
Ag2 Ag10 Ag12 79.102(17) . . ?
Ag19 Ag10 Ag12 87.426(17) . . ?
O10A Ag10 Ag11 82.93(12) . . ?
S18A Ag10 Ag11 133.15(3) 2_665 . ?
S10A Ag10 Ag11 55.09(3) . . ?
Ag18 Ag10 Ag11 76.840(17) 2_665 . ?
Ag2 Ag10 Ag11 153.69(2) . . ?
Ag19 Ag10 Ag11 87.354(17) . . ?
Ag12 Ag10 Ag11 89.547(16) . . ?
O11A Ag11 S21A 110.14(11) . 2_665 ?
O11A Ag11 S15A 96.22(11) . . ?
S21A Ag11 S15A 139.32(4) 2_665 . ?
O11A Ag11 S10A 101.95(10) . . ?
S21A Ag11 S10A 108.33(4) 2_665 . ?
S15A Ag11 S10A 95.21(4) . . ?
O11A Ag11 Ag5 141.61(10) . 2_665 ?
S21A Ag11 Ag5 92.59(3) 2_665 2_665 ?
S15A Ag11 Ag5 50.14(3) . 2_665 ?
S10A Ag11 Ag5 99.43(3) . 2_665 ?
O11A Ag11 Ag10 74.60(9) . . ?
S21A Ag11 Ag10 82.76(3) 2_665 . ?
S15A Ag11 Ag10 135.35(3) . . ?
S10A Ag11 Ag10 47.10(3) . . ?
Ag5 Ag11 Ag10 140.81(2) 2_665 . ?
O12A Ag12 S19A 126.53(11) . . ?
O12A Ag12 S16A 89.53(12) . . ?
S19A Ag12 S16A 134.85(5) . . ?
O12A Ag12 S10A 88.90(13) . . ?
S19A Ag12 S10A 108.03(5) . . ?
S16A Ag12 S10A 97.55(5) . . ?
O12A Ag12 Ag13 137.94(12) . . ?
S19A Ag12 Ag13 89.29(3) . . ?
S16A Ag12 Ag13 48.87(3) . . ?
S10A Ag12 Ag13 100.99(3) . . ?
O12A Ag12 Ag10 72.60(13) . . ?
S19A Ag12 Ag10 82.03(4) . . ?
S16A Ag12 Ag10 140.07(3) . . ?
S10A Ag12 Ag10 48.21(3) . . ?
Ag13 Ag12 Ag10 141.58(2) . . ?
O12A Ag12 Ag20 67.07(11) . . ?
S19A Ag12 Ag20 162.59(4) . . ?
S16A Ag12 Ag20 46.50(3) . . ?
S10A Ag12 Ag20 58.18(3) . . ?
Ag13 Ag12 Ag20 83.666(16) . . ?
Ag10 Ag12 Ag20 93.630(17) . . ?
O13A Ag13 S16A 110.65(11) . . ?
O13A Ag13 S11A 111.83(11) . . ?
S16A Ag13 S11A 137.44(5) . . ?
O13A Ag13 Cu6A 161.97(11) . 2_665 ?
S16A Ag13 Cu6A 86.31(4) . 2_665 ?
S11A Ag13 Cu6A 51.88(3) . 2_665 ?
O13A Ag13 Ag9 116.23(10) . 2_665 ?
S16A Ag13 Ag9 57.18(4) . 2_665 ?
S11A Ag13 Ag9 100.55(3) . 2_665 ?
Cu6A Ag13 Ag9 77.66(2) 2_665 2_665 ?
O13A Ag13 Ag12 115.80(9) . . ?
S16A Ag13 Ag12 57.92(4) . . ?
S11A Ag13 Ag12 104.35(3) . . ?
Cu6A Ag13 Ag12 67.36(2) 2_665 . ?
Ag9 Ag13 Ag12 106.389(18) 2_665 . ?
O13A Ag13 Ag14 80.23(10) . . ?
S16A Ag13 Ag14 136.34(4) . . ?
S11A Ag13 Ag14 55.64(3) . . ?
Cu6A Ag13 Ag14 83.17(2) 2_665 . ?
Ag9 Ag13 Ag14 155.87(2) 2_665 . ?
Ag12 Ag13 Ag14 79.008(16) . . ?
O13A Ag13 Ag15 79.72(10) . . ?
S16A Ag13 Ag15 133.14(4) . . ?
S11A Ag13 Ag15 54.49(3) . . ?
Cu6A Ag13 Ag15 93.27(2) 2_665 . ?
Ag9 Ag13 Ag15 76.933(16) 2_665 . ?
Ag12 Ag13 Ag15 158.47(3) . . ?
Ag14 Ag13 Ag15 89.792(16) . . ?
O14A Ag14 S19A 117.10(10) . . ?
O14A Ag14 S13A 91.06(9) . . ?
S19A Ag14 S13A 137.13(5) . . ?
O14A Ag14 S11A 94.98(9) . . ?
S19A Ag14 S11A 110.47(4) . . ?
S13A Ag14 S11A 97.43(4) . . ?
O14A Ag14 Ag1 137.48(8) . . ?
S19A Ag14 Ag1 91.81(4) . . ?
S13A Ag14 Ag1 49.20(3) . . ?
S11A Ag14 Ag1 103.58(4) . . ?
O14A Ag14 Cu4A 138.06(9) . . ?
S19A Ag14 Cu4A 97.19(4) . . ?
S13A Ag14 Cu4A 77.50(3) . . ?
S11A Ag14 Cu4A 48.16(3) . . ?
Ag1 Ag14 Cu4A 57.370(19) . . ?
O14A Ag14 Ag13 75.46(8) . . ?
S19A Ag14 Ag13 83.27(3) . . ?
S13A Ag14 Ag13 137.49(3) . . ?
S11A Ag14 Ag13 45.66(3) . . ?
Ag1 Ag14 Ag13 142.33(2) . . ?
Cu4A Ag14 Ag13 86.117(19) . . ?
O15A Ag15 S20A 119.27(10) . . ?
O15A Ag15 S14A 93.53(9) . . ?
S20A Ag15 S14A 135.93(4) . . ?
O15A Ag15 S11A 94.79(9) . . ?
S20A Ag15 S11A 107.71(4) . . ?
S14A Ag15 S11A 96.99(4) . . ?
O15A Ag15 Ag17 140.91(8) . . ?
S20A Ag15 Ag17 89.70(4) . . ?
S14A Ag15 Ag17 49.35(3) . . ?
S11A Ag15 Ag17 100.85(3) . . ?
O15A Ag15 Ag13 75.21(8) . . ?
S20A Ag15 Ag13 83.30(3) . . ?
S14A Ag15 Ag13 136.51(3) . . ?
S11A Ag15 Ag13 44.24(3) . . ?
Ag17 Ag15 Ag13 138.17(2) . . ?
S20A Ag16 O16A 118.33(9) . . ?
S20A Ag16 S17A 137.17(4) . . ?
O16A Ag16 S17A 92.45(8) . . ?
S20A Ag16 S12A 107.62(5) . . ?
O16A Ag16 S12A 94.40(10) . . ?
S17A Ag16 S12A 98.08(5) . . ?
S20A Ag16 Ag8 91.30(3) . 2_665 ?
O16A Ag16 Ag8 139.41(7) . 2_665 ?
S17A Ag16 Ag8 49.15(3) . 2_665 ?
S12A Ag16 Ag8 102.65(3) . 2_665 ?
S20A Ag16 Ag17 81.42(3) . . ?
O16A Ag16 Ag17 75.94(8) . . ?
S17A Ag16 Ag17 137.95(3) . . ?
S12A Ag16 Ag17 44.45(3) . . ?
Ag8 Ag16 Ag17 139.59(2) 2_665 . ?
S20A Ag16 Ag21 161.73(4) . . ?
O16A Ag16 Ag21 76.22(9) . . ?
S17A Ag16 Ag21 45.55(3) . . ?
S12A Ag16 Ag21 57.86(3) . . ?
Ag8 Ag16 Ag21 82.201(17) 2_665 . ?
Ag17 Ag16 Ag21 92.458(18) . . ?
O17A Ag17 S14A 109.81(10) . . ?
O17A Ag17 S12A 112.53(10) . . ?
S14A Ag17 S12A 137.64(4) . . ?
O17A Ag17 Ag6 115.58(10) . . ?
S14A Ag17 Ag6 58.33(4) . . ?
S12A Ag17 Ag6 102.74(4) . . ?
O17A Ag17 Ag15 113.25(11) . . ?
S14A Ag17 Ag15 57.13(3) . . ?
S12A Ag17 Ag15 103.64(3) . . ?
Ag6 Ag17 Ag15 107.943(18) . . ?
O17A Ag17 Cu3A 164.66(9) . . ?
S14A Ag17 Cu3A 85.53(3) . . ?
S12A Ag17 Cu3A 52.13(3) . . ?
Ag6 Ag17 Cu3A 71.91(2) . . ?
Ag15 Ag17 Cu3A 74.63(2) . . ?
O17A Ag17 Ag16 79.36(9) . . ?
S14A Ag17 Ag16 135.35(4) . . ?
S12A Ag17 Ag16 54.65(4) . . ?
Ag6 Ag17 Ag16 157.29(2) . . ?
Ag15 Ag17 Ag16 78.807(16) . . ?
Cu3A Ag17 Ag16 89.776(19) . . ?
O17A Ag17 Ag18 81.41(11) . . ?
S14A Ag17 Ag18 135.20(4) . . ?
S12A Ag17 Ag18 54.74(4) . . ?
Ag6 Ag17 Ag18 77.466(18) . . ?
Ag15 Ag17 Ag18 158.180(19) . . ?
Cu3A Ag17 Ag18 87.60(2) . . ?
Ag16 Ag17 Ag18 88.741(15) . . ?
S21A Ag18 O18A 115.62(10) . . ?
S21A Ag18 S18A 137.94(5) . . ?
O18A Ag18 S18A 94.20(10) . . ?
S21A Ag18 S12A 107.91(4) . . ?
O18A Ag18 S12A 94.73(10) . . ?
S18A Ag18 S12A 97.74(4) . . ?
S21A Ag18 Ag10 90.69(4) . 2_665 ?
O18A Ag18 Ag10 140.80(10) . 2_665 ?
S18A Ag18 Ag10 50.09(3) . 2_665 ?
S12A Ag18 Ag10 104.55(3) . 2_665 ?
S21A Ag18 Ag17 81.90(4) . . ?
O18A Ag18 Ag17 74.76(10) . . ?
S18A Ag18 Ag17 136.88(3) . . ?
S12A Ag18 Ag17 43.90(3) . . ?
Ag10 Ag18 Ag17 140.795(19) 2_665 . ?
S25A Ag19 S10A 64.84(7) 2_665 . ?
S25A Ag19 S7A 166.12(7) 2_665 . ?
S10A Ag19 S7A 128.06(5) . . ?
S25A Ag19 S12A 70.25(7) 2_665 2_665 ?
S10A Ag19 S12A 124.83(4) . 2_665 ?
S7A Ag19 S12A 101.11(5) . 2_665 ?
S25A Ag19 Cu2A 114.88(6) 2_665 . ?
S10A Ag19 Cu2A 163.17(3) . . ?
S7A Ag19 Cu2A 51.25(4) . . ?
S12A Ag19 Cu2A 67.12(3) 2_665 . ?
S25A Ag19 S1C 74.06(5) 2_665 . ?
S10A Ag19 S1C 98.67(3) . . ?
S7A Ag19 S1C 97.14(3) . . ?
S12A Ag19 S1C 98.19(3) 2_665 . ?
Cu2A Ag19 S1C 66.223(16) . . ?
S25A Ag19 Cu4A 131.86(5) 2_665 . ?
S10A Ag19 Cu4A 100.39(3) . . ?
S7A Ag19 Cu4A 46.92(3) . . ?
S12A Ag19 Cu4A 133.83(3) 2_665 . ?
Cu2A Ag19 Cu4A 66.71(3) . . ?
S1C Ag19 Cu4A 62.845(15) . . ?
S25A Ag19 Cu6A 86.68(6) 2_665 2_665 ?
S10A Ag19 Cu6A 49.43(3) . 2_665 ?
S7A Ag19 Cu6A 98.75(4) . 2_665 ?
S12A Ag19 Cu6A 153.53(3) 2_665 2_665 ?
Cu2A Ag19 Cu6A 114.24(3) . 2_665 ?
S1C Ag19 Cu6A 61.928(19) . 2_665 ?
Cu4A Ag19 Cu6A 55.22(2) . 2_665 ?
S25A Ag19 Ag10 89.63(5) 2_665 . ?
S10A Ag19 Ag10 50.02(3) . . ?
S7A Ag19 Ag10 102.94(3) . . ?
S12A Ag19 Ag10 101.17(3) 2_665 . ?
Cu2A Ag19 Ag10 144.60(2) . . ?
S1C Ag19 Ag10 148.68(2) . . ?
Cu4A Ag19 Ag10 116.37(3) . . ?
Cu6A Ag19 Ag10 91.17(2) 2_665 . ?
S25A Ag19 Cu3A 39.03(6) 2_665 2_665 ?
S10A Ag19 Cu3A 103.01(3) . 2_665 ?
S7A Ag19 Cu3A 127.17(4) . 2_665 ?
S12A Ag19 Cu3A 47.61(3) 2_665 2_665 ?
Cu2A Ag19 Cu3A 76.00(3) . 2_665 ?
S1C Ag19 Cu3A 58.349(16) . 2_665 ?
Cu4A Ag19 Cu3A 118.93(2) . 2_665 ?
Cu6A Ag19 Cu3A 106.07(3) 2_665 2_665 ?
Ag10 Ag19 Cu3A 121.95(2) . 2_665 ?
S16A Ag20 S15A 171.68(5) . . ?
S16A Ag20 Ag12 50.65(4) . . ?
S15A Ag20 Ag12 133.43(3) . . ?
S17A Ag21 S18A 168.72(4) . . ?
S17A Ag21 Ag2 134.35(3) . 2_665 ?
S18A Ag21 Ag2 49.84(3) . 2_665 ?
S17A Ag21 Ag16 49.24(3) . . ?
S18A Ag21 Ag16 134.00(3) . . ?
Ag2 Ag21 Ag16 151.70(2) 2_665 . ?
S23A Cu1A S25A 122.37(8) . . ?
S23A Cu1A S8A 72.88(5) . . ?
S25A Cu1A S8A 69.83(6) . . ?
S23A Cu1A S9A 69.73(6) . . ?
S25A Cu1A S9A 159.88(6) . . ?
S8A Cu1A S9A 130.21(4) . . ?
S23A Cu1A S10A 161.81(5) . 2_665 ?
S25A Cu1A S10A 62.69(7) . 2_665 ?
S8A Cu1A S10A 122.96(4) . 2_665 ?
S9A Cu1A S10A 100.82(5) . 2_665 ?
S23A Cu1A Cu6A 110.48(4) . . ?
S25A Cu1A Cu6A 93.90(5) . . ?
S8A Cu1A Cu6A 161.09(4) . . ?
S9A Cu1A Cu6A 66.07(3) . . ?
S10A Cu1A Cu6A 51.53(3) 2_665 . ?
S23A Cu1A Cu2A 31.18(5) . . ?
S25A Cu1A Cu2A 135.73(5) . . ?
S8A Cu1A Cu2A 104.03(3) . . ?
S9A Cu1A Cu2A 46.36(3) . . ?
S10A Cu1A Cu2A 131.81(3) 2_665 . ?
Cu6A Cu1A Cu2A 80.59(3) . . ?
S23A Cu1A Ag5 96.97(4) . . ?
S25A Cu1A Ag5 90.14(5) . . ?
S8A Cu1A Ag5 48.95(3) . . ?
S9A Cu1A Ag5 104.93(3) . . ?
S10A Cu1A Ag5 100.56(3) 2_665 . ?
Cu6A Cu1A Ag5 144.16(3) . . ?
Cu2A Cu1A Ag5 119.53(3) . . ?
S23A Cu2A S9A 81.93(7) . . ?
S23A Cu2A S7A 77.58(7) . . ?
S9A Cu2A S7A 147.61(5) . . ?
S23A Cu2A S22A 116.41(6) . . ?
S9A Cu2A S22A 69.71(5) . . ?
S7A Cu2A S22A 142.34(5) . . ?
S23A Cu2A Ag8 112.28(6) . . ?
S9A Cu2A Ag8 52.33(4) . . ?
S7A Cu2A Ag8 114.15(4) . . ?
S22A Cu2A Ag8 93.45(4) . . ?
S23A Cu2A Ag19 101.46(6) . . ?
S9A Cu2A Ag19 152.62(3) . . ?
S7A Cu2A Ag19 57.60(3) . . ?
S22A Cu2A Ag19 84.85(4) . . ?
Ag8 Cu2A Ag19 142.82(3) . . ?
S23A Cu2A Cu1A 34.82(5) . . ?
S9A Cu2A Cu1A 56.66(4) . . ?
S7A Cu2A Cu1A 111.30(3) . . ?
S22A Cu2A Cu1A 83.88(4) . . ?
Ag8 Cu2A Cu1A 104.47(3) . . ?
Ag19 Cu2A Cu1A 112.23(3) . . ?
S23A Cu2A Ag3 87.48(4) . . ?
S9A Cu2A Ag3 96.44(3) . . ?
S7A Cu2A Ag3 58.13(3) . . ?
S22A Cu2A Ag3 148.98(4) . . ?
Ag8 Cu2A Ag3 57.653(19) . . ?
Ag19 Cu2A Ag3 110.79(3) . . ?
Cu1A Cu2A Ag3 112.27(3) . . ?
S22A Cu3A S25A 121.91(7) 2_665 . ?
S22A Cu3A S12A 70.90(6) 2_665 . ?
S25A Cu3A S12A 74.99(7) . . ?
S22A Cu3A S8A 158.55(5) 2_665 . ?
S25A Cu3A S8A 66.98(6) . . ?
S12A Cu3A S8A 129.82(4) . . ?
S22A Cu3A S11A 66.03(5) 2_665 . ?
S25A Cu3A S11A 159.36(7) . . ?
S12A Cu3A S11A 124.57(5) . . ?
S8A Cu3A S11A 99.24(4) . . ?
S22A Cu3A Cu4A 91.85(5) 2_665 . ?
S25A Cu3A Cu4A 108.57(6) . . ?
S12A Cu3A Cu4A 160.51(3) . . ?
S8A Cu3A Cu4A 66.77(3) . . ?
S11A Cu3A Cu4A 50.81(3) . . ?
S22A Cu3A Ag17 94.81(5) 2_665 . ?
S25A Cu3A Ag17 97.42(5) . . ?
S12A Cu3A Ag17 49.82(3) . . ?
S8A Cu3A Ag17 103.58(3) . . ?
S11A Cu3A Ag17 100.89(3) . . ?
Cu4A Cu3A Ag17 144.27(3) . . ?
S22A Cu3A Ag19 82.57(5) 2_665 2_665 ?
S25A Cu3A Ag19 39.52(5) . 2_665 ?
S12A Cu3A Ag19 53.17(4) . 2_665 ?
S8A Cu3A Ag19 105.15(3) . 2_665 ?
S11A Cu3A Ag19 144.15(3) . 2_665 ?
Cu4A Cu3A Ag19 117.21(3) . 2_665 ?
Ag17 Cu3A Ag19 98.47(2) . 2_665 ?
S7A Cu4A S23A 68.31(5) . . ?
S7A Cu4A S11A 148.18(5) . . ?
S23A Cu4A S11A 143.50(5) . . ?
S7A Cu4A Cu6A 114.72(3) . 2_665 ?
S23A Cu4A Cu6A 126.92(3) . 2_665 ?
S11A Cu4A Cu6A 52.20(3) . 2_665 ?
S7A Cu4A Ag1 52.72(3) . . ?
S23A Cu4A Ag1 91.38(3) . . ?
S11A Cu4A Ag1 112.23(3) . . ?
Cu6A Cu4A Ag1 134.69(3) 2_665 . ?
S7A Cu4A Cu3A 152.05(4) . . ?
S23A Cu4A Cu3A 85.13(3) . . ?
S11A Cu4A Cu3A 58.79(3) . . ?
Cu6A Cu4A Cu3A 73.99(3) 2_665 . ?
Ag1 Cu4A Cu3A 140.23(3) . . ?
S7A Cu4A Ag19 55.83(3) . . ?
S23A Cu4A Ag19 83.37(4) . . ?
S11A Cu4A Ag19 114.85(3) . . ?
Cu6A Cu4A Ag19 63.51(2) 2_665 . ?
Ag1 Cu4A Ag19 104.43(2) . . ?
Cu3A Cu4A Ag19 114.41(2) . . ?
S7A Cu4A Ag14 96.83(4) . . ?
S23A Cu4A Ag14 147.43(3) . . ?
S11A Cu4A Ag14 56.54(3) . . ?
Cu6A Cu4A Ag14 85.45(3) 2_665 . ?
Ag1 Cu4A Ag14 58.013(19) . . ?
Cu3A Cu4A Ag14 110.61(3) . . ?
Ag19 Cu4A Ag14 112.94(3) . . ?
S13A Cu5A S14A 172.40(4) . . ?
S22A Cu6A S11A 68.05(5) . 2_665 ?
S22A Cu6A S10A 146.25(5) . 2_665 ?
S11A Cu6A S10A 145.32(5) 2_665 2_665 ?
S22A Cu6A Cu4A 88.53(4) . 2_665 ?
S11A Cu6A Cu4A 54.69(4) 2_665 2_665 ?
S10A Cu6A Cu4A 107.82(4) 2_665 2_665 ?
S22A Cu6A Cu1A 87.89(4) . . ?
S11A Cu6A Cu1A 154.10(4) 2_665 . ?
S10A Cu6A Cu1A 58.40(3) 2_665 . ?
Cu4A Cu6A Cu1A 117.90(4) 2_665 . ?
S22A Cu6A Ag13 93.64(4) . 2_665 ?
S11A Cu6A Ag13 52.02(4) 2_665 2_665 ?
S10A Cu6A Ag13 112.08(4) 2_665 2_665 ?
Cu4A Cu6A Ag13 98.60(3) 2_665 2_665 ?
Cu1A Cu6A Ag13 143.50(4) . 2_665 ?
S22A Cu6A Ag19 121.27(5) . 2_665 ?
S11A Cu6A Ag19 115.09(4) 2_665 2_665 ?
S10A Cu6A Ag19 51.43(4) 2_665 2_665 ?
Cu4A Cu6A Ag19 61.27(2) 2_665 2_665 ?
Cu1A Cu6A Ag19 68.62(3) . 2_665 ?
Ag13 Cu6A Ag19 136.76(3) 2_665 2_665 ?
C4A C1A C2A 107.7(5) . . ?
C4A C1A C3A 105.1(5) . . ?
C2A C1A C3A 105.2(5) . . ?
C4A C1A S1A 111.3(4) . . ?
C2A C1A S1A 112.2(4) . . ?
C3A C1A S1A 114.8(4) . . ?
C1A C2A H2A1 109.5 . . ?
C1A C2A H2A2 109.5 . . ?
H2A1 C2A H2A2 109.5 . . ?
C1A C2A H2A3 109.5 . . ?
H2A1 C2A H2A3 109.5 . . ?
H2A2 C2A H2A3 109.5 . . ?
C1A C3A H3A1 109.5 . . ?
C1A C3A H3A2 109.5 . . ?
H3A1 C3A H3A2 109.5 . . ?
C1A C3A H3A3 109.5 . . ?
H3A1 C3A H3A3 109.5 . . ?
H3A2 C3A H3A3 109.5 . . ?
C1A C4A H4AA 109.5 . . ?
C1A C4A H4AB 109.5 . . ?
H4AA C4A H4AB 109.5 . . ?
C1A C4A H4AC 109.5 . . ?
H4AA C4A H4AC 109.5 . . ?
H4AB C4A H4AC 109.5 . . ?
C6A C5A C8A 112.9(5) . . ?
C6A C5A C7A 115.9(5) . . ?
C8A C5A C7A 106.7(4) . . ?
C6A C5A S2A 107.2(3) . . ?
C8A C5A S2A 106.0(4) . . ?
C7A C5A S2A 107.7(4) . . ?
C5A C6A H6A1 109.5 . . ?
C5A C6A H6A2 109.5 . . ?
H6A1 C6A H6A2 109.5 . . ?
C5A C6A H6A3 109.5 . . ?
H6A1 C6A H6A3 109.5 . . ?
H6A2 C6A H6A3 109.5 . . ?
C5A C7A H7A1 109.5 . . ?
C5A C7A H7A2 109.5 . . ?
H7A1 C7A H7A2 109.5 . . ?
C5A C7A H7A3 109.5 . . ?
H7A1 C7A H7A3 109.5 . . ?
H7A2 C7A H7A3 109.5 . . ?
C5A C8A H8A1 109.5 . . ?
C5A C8A H8A2 109.5 . . ?
H8A1 C8A H8A2 109.5 . . ?
C5A C8A H8A3 109.5 . . ?
H8A1 C8A H8A3 109.5 . . ?
H8A2 C8A H8A3 109.5 . . ?
C11A C9A C12A 106.4(5) . . ?
C11A C9A C10A 121.5(6) . . ?
C12A C9A C10A 108.6(4) . . ?
C11A C9A S3A 106.6(4) . . ?
C12A C9A S3A 108.9(4) . . ?
C10A C9A S3A 104.4(4) . . ?
C9A C10A H10A 109.5 . . ?
C9A C10A H10B 109.5 . . ?
H10A C10A H10B 109.5 . . ?
C9A C10A H10C 109.5 . . ?
H10A C10A H10C 109.5 . . ?
H10B C10A H10C 109.5 . . ?
C9A C11A H11A 109.5 . . ?
C9A C11A H11B 109.5 . . ?
H11A C11A H11B 109.5 . . ?
C9A C11A H11C 109.5 . . ?
H11A C11A H11C 109.5 . . ?
H11B C11A H11C 109.5 . . ?
C9A C12A H12A 109.5 . . ?
C9A C12A H12B 109.5 . . ?
H12A C12A H12B 109.5 . . ?
C9A C12A H12C 109.5 . . ?
H12A C12A H12C 109.5 . . ?
H12B C12A H12C 109.5 . . ?
C16A C13A C15A 97.3(4) . . ?
C16A C13A C14A 124.6(6) . . ?
C15A C13A C14A 115.8(4) . . ?
C16A C13A S4A 101.1(4) . . ?
C15A C13A S4A 111.9(5) . . ?
C14A C13A S4A 105.3(3) . . ?
C13A C14A H14A 109.5 . . ?
C13A C14A H14B 109.5 . . ?
H14A C14A H14B 109.5 . . ?
C13A C14A H14C 109.5 . . ?
H14A C14A H14C 109.5 . . ?
H14B C14A H14C 109.5 . . ?
C13A C15A H15A 109.5 . . ?
C13A C15A H15B 109.5 . . ?
H15A C15A H15B 109.5 . . ?
C13A C15A H15C 109.5 . . ?
H15A C15A H15C 109.5 . . ?
H15B C15A H15C 109.5 . . ?
C13A C16A H16A 109.5 . . ?
C13A C16A H16B 109.5 . . ?
H16A C16A H16B 109.5 . . ?
C13A C16A H16C 109.5 . . ?
H16A C16A H16C 109.5 . . ?
H16B C16A H16C 109.5 . . ?
C18A C17A C20A 107.5(5) . . ?
C18A C17A C19A 116.3(5) . . ?
C20A C17A C19A 107.4(6) . . ?
C18A C17A S5A 108.2(5) . . ?
C20A C17A S5A 106.7(4) . . ?
C19A C17A S5A 110.4(5) . . ?
C17A C18A H18A 109.5 . . ?
C17A C18A H18B 109.5 . . ?
H18A C18A H18B 109.5 . . ?
C17A C18A H18C 109.5 . . ?
H18A C18A H18C 109.5 . . ?
H18B C18A H18C 109.5 . . ?
C17A C19A H19A 109.5 . . ?
C17A C19A H19B 109.5 . . ?
H19A C19A H19B 109.5 . . ?
C17A C19A H19C 109.5 . . ?
H19A C19A H19C 109.5 . . ?
H19B C19A H19C 109.5 . . ?
C17A C20A H20A 109.5 . . ?
C17A C20A H20B 109.5 . . ?
H20A C20A H20B 109.5 . . ?
C17A C20A H20C 109.5 . . ?
H20A C20A H20C 109.5 . . ?
H20B C20A H20C 109.5 . . ?
C22A C21A C24A 111.9(5) . . ?
C22A C21A C23A 117.9(6) . . ?
C24A C21A C23A 106.7(5) . . ?
C22A C21A S6A 104.1(4) . . ?
C24A C21A S6A 108.2(4) . . ?
C23A C21A S6A 107.6(4) . . ?
C21A C22A H22A 109.5 . . ?
C21A C22A H22B 109.5 . . ?
H22A C22A H22B 109.5 . . ?
C21A C22A H22C 109.5 . . ?
H22A C22A H22C 109.5 . . ?
H22B C22A H22C 109.5 . . ?
C21A C23A H23A 109.5 . . ?
C21A C23A H23B 109.5 . . ?
H23A C23A H23B 109.5 . . ?
C21A C23A H23C 109.5 . . ?
H23A C23A H23C 109.5 . . ?
H23B C23A H23C 109.5 . . ?
C21A C24A H24A 109.5 . . ?
C21A C24A H24B 109.5 . . ?
H24A C24A H24B 109.5 . . ?
C21A C24A H24C 109.5 . . ?
H24A C24A H24C 109.5 . . ?
H24B C24A H24C 109.5 . . ?
C27A C25A C26A 116.4(4) . . ?
C27A C25A C28A 109.8(5) . . ?
C26A C25A C28A 111.2(4) . . ?
C27A C25A S13A 109.1(3) . . ?
C26A C25A S13A 105.9(3) . . ?
C28A C25A S13A 103.6(3) . . ?
C25A C26A H26A 109.5 . . ?
C25A C26A H26B 109.5 . . ?
H26A C26A H26B 109.5 . . ?
C25A C26A H26C 109.5 . . ?
H26A C26A H26C 109.5 . . ?
H26B C26A H26C 109.5 . . ?
C25A C27A H27A 109.5 . . ?
C25A C27A H27B 109.5 . . ?
H27A C27A H27B 109.5 . . ?
C25A C27A H27C 109.5 . . ?
H27A C27A H27C 109.5 . . ?
H27B C27A H27C 109.5 . . ?
C25A C28A H28A 109.5 . . ?
C25A C28A H28B 109.5 . . ?
H28A C28A H28B 109.5 . . ?
C25A C28A H28C 109.5 . . ?
H28A C28A H28C 109.5 . . ?
H28B C28A H28C 109.5 . . ?
C31A C29A C30A 121.7(5) . . ?
C31A C29A C32A 105.0(5) . . ?
C30A C29A C32A 108.6(4) . . ?
C31A C29A S14A 108.5(4) . . ?
C30A C29A S14A 107.6(4) . . ?
C32A C29A S14A 104.1(3) . . ?
C29A C30A H30A 109.5 . . ?
C29A C30A H30B 109.5 . . ?
H30A C30A H30B 109.5 . . ?
C29A C30A H30C 109.5 . . ?
H30A C30A H30C 109.5 . . ?
H30B C30A H30C 109.5 . . ?
C29A C31A H31A 109.5 . . ?
C29A C31A H31B 109.5 . . ?
H31A C31A H31B 109.5 . . ?
C29A C31A H31C 109.5 . . ?
H31A C31A H31C 109.5 . . ?
H31B C31A H31C 109.5 . . ?
C29A C32A H32A 109.5 . . ?
C29A C32A H32B 109.5 . . ?
H32A C32A H32B 109.5 . . ?
C29A C32A H32C 109.5 . . ?
H32A C32A H32C 109.5 . . ?
H32B C32A H32C 109.5 . . ?
C34A C33A C36A 96.5(4) . . ?
C34A C33A C35A 118.4(5) . . ?
C36A C33A C35A 123.6(5) . . ?
C34A C33A S19A 107.1(4) . . ?
C36A C33A S19A 105.1(3) . . ?
C35A C33A S19A 104.8(3) . . ?
C33A C34A H34A 109.5 . . ?
C33A C34A H34B 109.5 . . ?
H34A C34A H34B 109.5 . . ?
C33A C34A H34C 109.5 . . ?
H34A C34A H34C 109.5 . . ?
H34B C34A H34C 109.5 . . ?
C33A C35A H35A 109.5 . . ?
C33A C35A H35B 109.5 . . ?
H35A C35A H35B 109.5 . . ?
C33A C35A H35C 109.5 . . ?
H35A C35A H35C 109.5 . . ?
H35B C35A H35C 109.5 . . ?
C33A C36A H36A 109.5 . . ?
C33A C36A H36B 109.5 . . ?
H36A C36A H36B 109.5 . . ?
C33A C36A H36C 109.5 . . ?
H36A C36A H36C 109.5 . . ?
H36B C36A H36C 109.5 . . ?
C38A C37A C39A 108.5(4) . . ?
C38A C37A C40A 106.6(5) . . ?
C39A C37A C40A 117.3(5) . . ?
C38A C37A S15A 106.4(4) . . ?
C39A C37A S15A 110.4(4) . . ?
C40A C37A S15A 107.0(3) . . ?
C37A C38A H38A 109.5 . . ?
C37A C38A H38B 109.5 . . ?
H38A C38A H38B 109.5 . . ?
C37A C38A H38C 109.5 . . ?
H38A C38A H38C 109.5 . . ?
H38B C38A H38C 109.5 . . ?
C37A C39A H39A 109.5 . . ?
C37A C39A H39B 109.5 . . ?
H39A C39A H39B 109.5 . . ?
C37A C39A H39C 109.5 . . ?
H39A C39A H39C 109.5 . . ?
H39B C39A H39C 109.5 . . ?
C37A C40A H40A 109.5 . . ?
C37A C40A H40B 109.5 . . ?
H40A C40A H40B 109.5 . . ?
C37A C40A H40C 109.5 . . ?
H40A C40A H40C 109.5 . . ?
H40B C40A H40C 109.5 . . ?
C43A C41A C42A 109.4(6) . . ?
C43A C41A C44A 106.2(6) . . ?
C42A C41A C44A 123.0(6) . . ?
C43A C41A S16A 100.2(5) . . ?
C42A C41A S16A 109.3(5) . . ?
C44A C41A S16A 106.3(5) . . ?
C41A C42A H42A 109.5 . . ?
C41A C42A H42B 109.5 . . ?
H42A C42A H42B 109.5 . . ?
C41A C42A H42C 109.5 . . ?
H42A C42A H42C 109.5 . . ?
H42B C42A H42C 109.5 . . ?
C41A C43A H43D 109.5 . . ?
C41A C43A H43E 109.5 . . ?
H43D C43A H43E 109.5 . . ?
C41A C43A H43F 109.5 . . ?
H43D C43A H43F 109.5 . . ?
H43E C43A H43F 109.5 . . ?
C41A C44A H44A 109.5 . . ?
C41A C44A H44B 109.5 . . ?
H44A C44A H44B 109.5 . . ?
C41A C44A H44C 109.5 . . ?
H44A C44A H44C 109.5 . . ?
H44B C44A H44C 109.5 . . ?
C47A C45A C48A 111.9(5) . . ?
C47A C45A C46A 115.6(4) . . ?
C48A C45A C46A 109.2(5) . . ?
C47A C45A S17A 111.0(4) . . ?
C48A C45A S17A 105.0(3) . . ?
C46A C45A S17A 103.3(4) . . ?
C45A C46A H46A 109.5 . . ?
C45A C46A H46B 109.5 . . ?
H46A C46A H46B 109.5 . . ?
C45A C46A H46C 109.5 . . ?
H46A C46A H46C 109.5 . . ?
H46B C46A H46C 109.5 . . ?
C45A C47A H47A 109.5 . . ?
C45A C47A H47B 109.5 . . ?
H47A C47A H47B 109.5 . . ?
C45A C47A H47C 109.5 . . ?
H47A C47A H47C 109.5 . . ?
H47B C47A H47C 109.5 . . ?
C45A C48A H48A 109.5 . . ?
C45A C48A H48B 109.5 . . ?
H48A C48A H48B 109.5 . . ?
C45A C48A H48C 109.5 . . ?
H48A C48A H48C 109.5 . . ?
H48B C48A H48C 109.5 . . ?
C52A C49A C50A 109.2(5) . . ?
C52A C49A C51A 110.5(5) . . ?
C50A C49A C51A 113.4(5) . . ?
C52A C49A S18A 108.8(4) . . ?
C50A C49A S18A 107.1(4) . . ?
C51A C49A S18A 107.8(4) . . ?
C49A C50A H50A 109.5 . . ?
C49A C50A H50B 109.5 . . ?
H50A C50A H50B 109.5 . . ?
C49A C50A H50C 109.5 . . ?
H50A C50A H50C 109.5 . . ?
H50B C50A H50C 109.5 . . ?
C49A C51A H51A 109.5 . . ?
C49A C51A H51B 109.5 . . ?
H51A C51A H51B 109.5 . . ?
C49A C51A H51C 109.5 . . ?
H51A C51A H51C 109.5 . . ?
H51B C51A H51C 109.5 . . ?
C49A C52A H52A 109.5 . . ?
C49A C52A H52B 109.5 . . ?
H52A C52A H52B 109.5 . . ?
C49A C52A H52C 109.5 . . ?
H52A C52A H52C 109.5 . . ?
H52B C52A H52C 109.5 . . ?
C56A C53A C54A 108.9(4) . . ?
C56A C53A C55A 118.4(5) . . ?
C54A C53A C55A 111.1(5) . . ?
C56A C53A S20A 109.4(4) . . ?
C54A C53A S20A 103.8(4) . . ?
C55A C53A S20A 104.2(3) . . ?
C53A C54A H54A 109.5 . . ?
C53A C54A H54B 109.5 . . ?
H54A C54A H54B 109.5 . . ?
C53A C54A H54C 109.5 . . ?
H54A C54A H54C 109.5 . . ?
H54B C54A H54C 109.5 . . ?
C53A C55A H55A 109.5 . . ?
C53A C55A H55B 109.5 . . ?
H55A C55A H55B 109.5 . . ?
C53A C55A H55C 109.5 . . ?
H55A C55A H55C 109.5 . . ?
H55B C55A H55C 109.5 . . ?
C53A C56A H56A 109.5 . . ?
C53A C56A H56B 109.5 . . ?
H56A C56A H56B 109.5 . . ?
C53A C56A H56C 109.5 . . ?
H56A C56A H56C 109.5 . . ?
H56B C56A H56C 109.5 . . ?
C58A C57A C60A 122.9(5) . . ?
C58A C57A C59A 117.1(5) . . ?
C60A C57A C59A 105.5(5) . . ?
C58A C57A S21A 100.0(4) . . ?
C60A C57A S21A 104.3(4) . . ?
C59A C57A S21A 104.4(3) . . ?
C57A C58A H58A 109.5 . . ?
C57A C58A H58B 109.5 . . ?
H58A C58A H58B 109.5 . . ?
C57A C58A H58C 109.5 . . ?
H58A C58A H58C 109.5 . . ?
H58B C58A H58C 109.5 . . ?
C57A C59A H59A 109.5 . . ?
C57A C59A H59B 109.5 . . ?
H59A C59A H59B 109.5 . . ?
C57A C59A H59C 109.5 . . ?
H59A C59A H59C 109.5 . . ?
H59B C59A H59C 109.5 . . ?
C57A C60A H60A 109.5 . . ?
C57A C60A H60B 109.5 . . ?
H60A C60A H60B 109.5 . . ?
C57A C60A H60C 109.5 . . ?
H60A C60A H60C 109.5 . . ?
H60B C60A H60C 109.5 . . ?
C63A C61A C64A 117.1(5) . . ?
C63A C61A C62A 107.4(5) . . ?
C64A C61A C62A 115.1(5) . . ?
C63A C61A S24A 101.1(4) . . ?
C64A C61A S24A 108.1(4) . . ?
C62A C61A S24A 106.7(4) . . ?
C61A C62A H62A 109.5 . . ?
C61A C62A H62B 109.5 . . ?
H62A C62A H62B 109.5 . . ?
C61A C62A H62C 109.5 . . ?
H62A C62A H62C 109.5 . . ?
H62B C62A H62C 109.5 . . ?
C61A C63A H63A 109.5 . . ?
C61A C63A H63B 109.5 . . ?
H63A C63A H63B 109.5 . . ?
C61A C63A H63C 109.5 . . ?
H63A C63A H63C 109.5 . . ?
H63B C63A H63C 109.5 . . ?
C61A C64A H64A 109.5 . . ?
C61A C64A H64B 109.5 . . ?
H64A C64A H64B 109.5 . . ?
C61A C64A H64C 109.5 . . ?
H64A C64A H64C 109.5 . . ?
H64B C64A H64C 109.5 . . ?
S1A O1A Ag2 124.0(2) . . ?
S1A O2A Ag3 124.5(3) . . ?
S1A O3A Ag1 117.2(2) . . ?
S2A O4A Ag4 121.0(2) . . ?
S2A O5A Ag5 122.7(2) . . ?
S2A O6A Ag6 122.9(2) . . ?
S3A O7A Ag7 122.4(2) . . ?
S3A O8A Ag8 123.6(3) . . ?
S3A O9A Ag9 119.6(2) . . ?
S4A O10A Ag10 116.1(3) . . ?
S4A O11A Ag11 115.8(2) . . ?
S4A O12A Ag12 126.9(3) . . ?
S5A O13A Ag13 122.2(3) . . ?
S5A O14A Ag14 124.9(2) . . ?
S5A O15A Ag15 122.8(2) . . ?
S6A O16A Ag16 121.3(2) . . ?
S6A O17A Ag17 120.9(2) . . ?
S6A O18A Ag18 122.8(2) . . ?
O2A S1A O1A 121.1(3) . . ?
O2A S1A O3A 110.0(3) . . ?
O1A S1A O3A 110.7(3) . . ?
O2A S1A C1A 108.7(3) . . ?
O1A S1A C1A 103.46(19) . . ?
O3A S1A C1A 100.7(2) . . ?
O5A S2A O6A 111.6(2) . . ?
O5A S2A O4A 113.2(2) . . ?
O6A S2A O4A 115.3(2) . . ?
O5A S2A C5A 104.1(2) . . ?
O6A S2A C5A 104.44(18) . . ?
O4A S2A C5A 107.00(16) . . ?
O8A S3A O7A 115.5(3) . . ?
O8A S3A O9A 110.3(2) . . ?
O7A S3A O9A 117.2(2) . . ?
O8A S3A C9A 104.84(19) . . ?
O7A S3A C9A 104.78(18) . . ?
O9A S3A C9A 102.34(19) . . ?
O12A S4A O11A 123.5(3) . . ?
O12A S4A O10A 112.6(3) . . ?
O11A S4A O10A 110.2(3) . . ?
O12A S4A C13A 106.6(2) . . ?
O11A S4A C13A 100.13(17) . . ?
O10A S4A C13A 100.08(19) . . ?
O13A S5A O14A 110.2(2) . . ?
O13A S5A O15A 112.7(2) . . ?
O14A S5A O15A 116.9(2) . . ?
O13A S5A C17A 105.2(2) . . ?
O14A S5A C17A 104.25(18) . . ?
O15A S5A C17A 106.49(19) . . ?
O18A S6A O16A 116.3(3) . . ?
O18A S6A O17A 114.4(3) . . ?
O16A S6A O17A 112.2(2) . . ?
O18A S6A C21A 104.8(2) . . ?
O16A S6A C21A 102.38(18) . . ?
O17A S6A C21A 105.0(2) . . ?
Cu4A S7A Cu2A 88.90(5) . . ?
Cu4A S7A Ag1 78.02(5) . . ?
Cu2A S7A Ag1 133.96(6) . . ?
Cu4A S7A Ag19 77.25(4) . . ?
Cu2A S7A Ag19 71.15(4) . . ?
Ag1 S7A Ag19 143.94(7) . . ?
Cu4A S7A Ag2 107.01(6) . . ?
Cu2A S7A Ag2 145.70(6) . . ?
Ag1 S7A Ag2 79.86(4) . . ?
Ag19 S7A Ag2 82.75(4) . . ?
Cu4A S7A Ag3 128.30(5) . . ?
Cu2A S7A Ag3 75.08(5) . . ?
Ag1 S7A Ag3 79.15(4) . . ?
Ag19 S7A Ag3 136.91(7) . . ?
Ag2 S7A Ag3 113.68(5) . . ?
Ag5 S8A Cu1A 78.09(5) . . ?
Ag5 S8A Cu3A 140.89(6) . . ?
Cu1A S8A Cu3A 81.15(3) . . ?
Ag5 S8A Ag4 81.13(4) . . ?
Cu1A S8A Ag4 115.44(5) . . ?
Cu3A S8A Ag4 137.95(6) . . ?
Ag5 S8A Ag6 80.54(4) . . ?
Cu1A S8A Ag6 119.93(5) . . ?
Cu3A S8A Ag6 81.70(4) . . ?
Ag4 S8A Ag6 115.59(4) . . ?
Cu2A S9A Ag8 77.61(4) . . ?
Cu2A S9A Cu1A 76.99(5) . . ?
Ag8 S9A Cu1A 142.62(7) . . ?
Cu2A S9A Ag9 127.67(6) . . ?
Ag8 S9A Ag9 81.55(5) . . ?
Cu1A S9A Ag9 135.83(5) . . ?
Cu2A S9A Ag7 106.49(5) . . ?
Ag8 S9A Ag7 82.20(4) . . ?
Cu1A S9A Ag7 79.26(4) . . ?
Ag9 S9A Ag7 117.50(6) . . ?
Cu6A S10A Ag19 79.14(4) 2_665 . ?
Cu6A S10A S25A 96.84(7) 2_665 2_665 ?
Ag19 S10A S25A 50.18(6) . 2_665 ?
Cu6A S10A Ag10 134.32(6) 2_665 . ?
Ag19 S10A Ag10 80.58(5) . . ?
S25A S10A Ag10 100.75(8) 2_665 . ?
Cu6A S10A Cu1A 70.06(4) 2_665 2_665 ?
Ag19 S10A Cu1A 83.29(5) . 2_665 ?
S25A S10A Cu1A 47.24(5) 2_665 2_665 ?
Ag10 S10A Cu1A 146.25(7) . 2_665 ?
Cu6A S10A Ag12 77.43(4) 2_665 . ?
Ag19 S10A Ag12 116.79(5) . . ?
S25A S10A Ag12 166.90(7) 2_665 . ?
Ag10 S10A Ag12 76.04(4) . . ?
Cu1A S10A Ag12 137.64(6) 2_665 . ?
Cu6A S10A Ag11 147.44(6) 2_665 . ?
Ag19 S10A Ag11 118.08(6) . . ?
S25A S10A Ag11 78.31(6) 2_665 . ?
Ag10 S10A Ag11 77.80(4) . . ?
Cu1A S10A Ag11 84.06(4) 2_665 . ?
Ag12 S10A Ag11 112.86(5) . . ?
Cu6A S11A Ag13 76.11(4) 2_665 . ?
Cu6A S11A Cu4A 73.11(4) 2_665 . ?
Ag13 S11A Cu4A 131.29(6) . . ?
Cu6A S11A Cu3A 87.61(5) 2_665 . ?
Ag13 S11A Cu3A 144.34(6) . . ?
Cu4A S11A Cu3A 70.40(4) . . ?
Cu6A S11A Ag14 106.82(5) 2_665 . ?
Ag13 S11A Ag14 78.70(4) . . ?
Cu4A S11A Ag14 75.31(4) . . ?
Cu3A S11A Ag14 136.84(6) . . ?
Cu6A S11A Ag15 125.89(5) 2_665 . ?
Ag13 S11A Ag15 81.27(5) . . ?
Cu4A S11A Ag15 147.37(6) . . ?
Cu3A S11A Ag15 83.21(4) . . ?
Ag14 S11A Ag15 115.96(5) . . ?
Ag17 S12A Cu3A 78.05(4) . . ?
Ag17 S12A Ag19 143.16(6) . 2_665 ?
Cu3A S12A Ag19 79.21(4) . 2_665 ?
Ag17 S12A Ag16 80.90(5) . . ?
Cu3A S12A Ag16 119.62(6) . . ?
Ag19 S12A Ag16 135.83(5) 2_665 . ?
Ag17 S12A Ag18 81.36(4) . . ?
Cu3A S12A Ag18 115.96(5) . . ?
Ag19 S12A Ag18 83.05(5) 2_665 . ?
Ag16 S12A Ag18 115.70(5) . . ?
C25A S13A Ag1 114.35(14) . . ?
C25A S13A Cu5A 120.26(14) . . ?
Ag1 S13A Cu5A 125.35(5) . . ?
C25A S13A Ag14 113.46(15) . . ?
Ag1 S13A Ag14 73.76(3) . . ?
Cu5A S13A Ag14 86.44(4) . . ?
C25A S13A Ag4 113.17(16) . . ?
Ag1 S13A Ag4 71.96(4) . . ?
Cu5A S13A Ag4 84.98(4) . . ?
Ag14 S13A Ag4 130.17(5) . . ?
C29A S14A Ag17 117.49(17) . . ?
C29A S14A Cu5A 117.95(17) . . ?
Ag17 S14A Cu5A 124.54(5) . . ?
C29A S14A Ag15 114.31(18) . . ?
Ag17 S14A Ag15 73.52(3) . . ?
Cu5A S14A Ag15 85.68(4) . . ?
C29A S14A Ag6 110.78(19) . . ?
Ag17 S14A Ag6 72.28(4) . . ?
Cu5A S14A Ag6 87.08(5) . . ?
Ag15 S14A Ag6 132.17(5) . . ?
C37A S15A Ag5 119.77(18) . 2_665 ?
C37A S15A Ag20 116.16(19) . . ?
Ag5 S15A Ag20 123.98(5) 2_665 . ?
C37A S15A Ag11 115.52(14) . . ?
Ag5 S15A Ag11 72.29(4) 2_665 . ?
Ag20 S15A Ag11 87.06(4) . . ?
C37A S15A Ag7 111.57(14) . 2_665 ?
Ag5 S15A Ag7 71.24(4) 2_665 2_665 ?
Ag20 S15A Ag7 86.27(4) . 2_665 ?
Ag11 S15A Ag7 130.25(6) . 2_665 ?
C41A S16A Ag13 115.6(2) . . ?
C41A S16A Ag20 120.3(2) . . ?
Ag13 S16A Ag20 124.02(7) . . ?
C41A S16A Ag9 113.2(2) . 2_665 ?
Ag13 S16A Ag9 73.50(4) . 2_665 ?
Ag20 S16A Ag9 86.78(5) . 2_665 ?
C41A S16A Ag12 113.6(2) . . ?
Ag13 S16A Ag12 73.21(4) . . ?
Ag20 S16A Ag12 82.85(5) . . ?
Ag9 S16A Ag12 130.74(7) 2_665 . ?
C45A S17A Ag8 116.53(17) . 2_665 ?
C45A S17A Ag21 120.41(17) . . ?
Ag8 S17A Ag21 123.06(6) 2_665 . ?
C45A S17A Ag16 113.29(15) . . ?
Ag8 S17A Ag16 73.27(4) 2_665 . ?
Ag21 S17A Ag16 85.20(4) . . ?
C45A S17A Ag3 112.12(15) . 2_665 ?
Ag8 S17A Ag3 72.71(4) 2_665 2_665 ?
Ag21 S17A Ag3 85.67(5) . 2_665 ?
Ag16 S17A Ag3 131.76(5) . 2_665 ?
C49A S18A Ag10 119.92(18) . 2_665 ?
C49A S18A Ag21 114.76(18) . . ?
Ag10 S18A Ag21 125.31(5) 2_665 . ?
C49A S18A Ag18 114.31(19) . . ?
Ag10 S18A Ag18 73.39(3) 2_665 . ?
Ag21 S18A Ag18 85.80(5) . . ?
C49A S18A Ag2 114.01(19) . 2_665 ?
Ag10 S18A Ag2 74.37(4) 2_665 2_665 ?
Ag21 S18A Ag2 83.36(4) . 2_665 ?
Ag18 S18A Ag2 130.58(5) . 2_665 ?
C33A S19A Ag14 112.15(12) . . ?
C33A S19A Ag2 114.33(15) . . ?
Ag14 S19A Ag2 104.04(6) . . ?
C33A S19A Ag12 112.90(14) . . ?
Ag14 S19A Ag12 105.55(5) . . ?
Ag2 S19A Ag12 107.11(5) . . ?
C53A S20A Ag15 112.74(13) . . ?
C53A S20A Ag9 113.59(15) . 2_665 ?
Ag15 S20A Ag9 104.98(5) . 2_665 ?
C53A S20A Ag16 112.26(15) . . ?
Ag15 S20A Ag16 107.59(6) . . ?
Ag9 S20A Ag16 105.06(5) 2_665 . ?
C57A S21A Ag11 112.4(2) . 2_665 ?
C57A S21A Ag6 111.72(16) . . ?
Ag11 S21A Ag6 104.81(5) 2_665 . ?
C57A S21A Ag18 114.41(16) . . ?
Ag11 S21A Ag18 106.34(5) 2_665 . ?
Ag6 S21A Ag18 106.49(6) . . ?
Cu3A S22A Cu6A 105.59(7) 2_665 . ?
Cu3A S22A Cu2A 116.58(8) 2_665 . ?
Cu6A S22A Cu2A 107.30(6) . . ?
Cu2A S23A Cu1A 114.00(8) . . ?
Cu2A S23A Cu4A 104.72(8) . . ?
Cu1A S23A Cu4A 117.99(7) . . ?
C61A S24A Ag3 113.23(17) . . ?
C61A S24A Ag7 113.5(2) . . ?
Ag3 S24A Ag7 104.09(5) . . ?
C61A S24A Ag4 112.9(2) . . ?
Ag3 S24A Ag4 107.69(6) . . ?
Ag7 S24A Ag4 104.67(5) . . ?
Cu1A S25A Cu3A 105.69(8) . . ?
Cu1A S25A Ag19 109.65(9) . 2_665 ?
Cu3A S25A Ag19 101.45(9) . 2_665 ?
Cu1A S25A S10A 70.07(8) . 2_665 ?
Cu3A S25A S10A 161.65(9) . 2_665 ?
Ag19 S25A S10A 64.98(6) 2_665 2_665 ?
Ag19 S1C Ag19 180.0 . 2_665 ?
O1B Ag23 S21B 116.23(11) . . ?
O1B Ag23 S7B 92.04(11) . . ?
S21B Ag23 S7B 138.78(5) . . ?
O1B Ag23 S16B 95.58(9) . . ?
S21B Ag23 S16B 109.17(4) . . ?
S7B Ag23 S16B 96.25(5) . . ?
O1B Ag23 Ag39 139.06(11) . 2_756 ?
S21B Ag23 Ag39 92.52(4) . 2_756 ?
S7B Ag23 Ag39 49.74(3) . 2_756 ?
S16B Ag23 Ag39 101.91(4) . 2_756 ?
O1B Ag23 Ag25 74.32(10) . . ?
S21B Ag23 Ag25 82.42(4) . . ?
S7B Ag23 Ag25 136.42(3) . . ?
S16B Ag23 Ag25 46.26(4) . . ?
Ag39 Ag23 Ag25 141.68(2) 2_756 . ?
O2B Ag24 S13B 123.01(11) . . ?
O2B Ag24 S8B 86.98(10) . . ?
S13B Ag24 S8B 138.60(4) . . ?
O2B Ag24 S16B 91.40(9) . . ?
S13B Ag24 S16B 108.23(4) . . ?
S8B Ag24 S16B 97.70(5) . . ?
O2B Ag24 Ag26 135.39(10) . . ?
S13B Ag24 Ag26 93.35(4) . . ?
S8B Ag24 Ag26 49.26(3) . . ?
S16B Ag24 Ag26 101.41(4) . . ?
O2B Ag24 Ag25 75.45(9) . . ?
S13B Ag24 Ag25 80.79(3) . . ?
S8B Ag24 Ag25 138.44(3) . . ?
S16B Ag24 Ag25 46.70(4) . . ?
Ag26 Ag24 Ag25 141.27(2) . . ?
O3B Ag25 S12B 114.07(11) . . ?
O3B Ag25 S16B 111.46(11) . . ?
S12B Ag25 S16B 134.45(5) . . ?
O3B Ag25 Cu4B 154.31(11) . . ?
S12B Ag25 Cu4B 86.87(4) . . ?
S16B Ag25 Cu4B 49.10(4) . . ?
O3B Ag25 Ag31 118.52(11) . . ?
S12B Ag25 Ag31 57.02(3) . . ?
S16B Ag25 Ag31 101.54(4) . . ?
Cu4B Ag25 Ag31 84.89(3) . . ?
O3B Ag25 Ag32 117.50(10) . . ?
S12B Ag25 Ag32 55.69(3) . . ?
S16B Ag25 Ag32 101.24(4) . . ?
Cu4B Ag25 Ag32 61.05(2) . . ?
Ag31 Ag25 Ag32 104.109(18) . . ?
O3B Ag25 Ag24 80.03(10) . . ?
S12B Ag25 Ag24 136.02(3) . . ?
S16B Ag25 Ag24 54.42(3) . . ?
Cu4B Ag25 Ag24 95.37(3) . . ?
Ag31 Ag25 Ag24 79.374(15) . . ?
Ag32 Ag25 Ag24 155.23(2) . . ?
O3B Ag25 Ag23 80.44(11) . . ?
S12B Ag25 Ag23 132.72(3) . . ?
S16B Ag25 Ag23 54.66(4) . . ?
Cu4B Ag25 Ag23 74.22(3) . . ?
Ag31 Ag25 Ag23 155.29(2) . . ?
Ag32 Ag25 Ag23 77.410(15) . . ?
Ag24 Ag25 Ag23 89.425(17) . . ?
O4B Ag26 S18B 111.38(9) . . ?
O4B Ag26 S8B 109.68(8) . . ?
S18B Ag26 S8B 138.92(5) . . ?
O4B Ag26 Ag37 115.68(10) . . ?
S18B Ag26 Ag37 103.42(5) . . ?
S8B Ag26 Ag37 58.63(4) . . ?
O4B Ag26 Ag24 113.08(10) . . ?
S18B Ag26 Ag24 103.38(4) . . ?
S8B Ag26 Ag24 57.95(4) . . ?
Ag37 Ag26 Ag24 108.792(18) . . ?
O4B Ag26 Cu2B 164.16(8) . . ?
S18B Ag26 Cu2B 52.95(4) . . ?
S8B Ag26 Cu2B 85.97(3) . . ?
Ag37 Ag26 Cu2B 74.07(2) . . ?
Ag24 Ag26 Cu2B 72.62(2) . . ?
O4B Ag26 Ag27 80.61(10) . . ?
S18B Ag26 Ag27 55.27(4) . . ?
S8B Ag26 Ag27 135.12(5) . . ?
Ag37 Ag26 Ag27 77.290(18) . . ?
Ag24 Ag26 Ag27 158.502(18) . . ?
Cu2B Ag26 Ag27 90.03(2) . . ?
O4B Ag26 Ag28 78.55(10) . . ?
S18B Ag26 Ag28 55.66(4) . . ?
S8B Ag26 Ag28 133.88(4) . . ?
Ag37 Ag26 Ag28 158.880(19) . . ?
Ag24 Ag26 Ag28 76.786(18) . . ?
Cu2B Ag26 Ag28 88.88(2) . . ?
Ag27 Ag26 Ag28 90.611(17) . . ?
S14B Ag27 O5B 118.98(10) . . ?
S14B Ag27 S9B 135.83(5) . . ?
O5B Ag27 S9B 91.99(9) . . ?
S14B Ag27 S18B 109.61(5) . . ?
O5B Ag27 S18B 93.52(11) . . ?
S9B Ag27 S18B 98.01(4) . . ?
S14B Ag27 Ag34 89.33(4) . 2_756 ?
O5B Ag27 Ag34 139.58(9) . 2_756 ?
S9B Ag27 Ag34 50.02(3) . 2_756 ?
S18B Ag27 Ag34 103.84(3) . 2_756 ?
S14B Ag27 Ag26 84.10(4) . . ?
O5B Ag27 Ag26 75.50(10) . . ?
S9B Ag27 Ag26 136.92(4) . . ?
S18B Ag27 Ag26 43.62(3) . . ?
Ag34 Ag27 Ag26 139.944(17) 2_756 . ?
O6B Ag28 S13B 116.93(9) . . ?
O6B Ag28 S10B 91.79(8) . . ?
S13B Ag28 S10B 137.66(5) . . ?
O6B Ag28 S18B 95.85(10) . . ?
S13B Ag28 S18B 109.48(5) . . ?
S10B Ag28 S18B 96.72(5) . . ?
O6B Ag28 Ag29 138.21(8) . . ?
S13B Ag28 Ag29 91.97(3) . . ?
S10B Ag28 Ag29 49.21(3) . . ?
S18B Ag28 Ag29 102.32(3) . . ?
O6B Ag28 Ag26 76.89(9) . . ?
S13B Ag28 Ag26 83.84(4) . . ?
S10B Ag28 Ag26 135.29(4) . . ?
S18B Ag28 Ag26 43.43(3) . . ?
Ag29 Ag28 Ag26 139.318(18) . . ?
O7B Ag29 S10B 109.94(9) . . ?
O7B Ag29 S22B 111.46(9) . . ?
S10B Ag29 S22B 138.59(6) . . ?
O7B Ag29 Ag40 115.00(8) . . ?
S10B Ag29 Ag40 58.45(3) . . ?
S22B Ag29 Ag40 103.46(4) . . ?
O7B Ag29 Cu3B 163.42(9) . . ?
S10B Ag29 Cu3B 86.11(4) . . ?
S22B Ag29 Cu3B 52.70(4) . . ?
Ag40 Ag29 Cu3B 69.27(2) . . ?
O7B Ag29 Ag28 114.29(9) . . ?
S10B Ag29 Ag28 58.29(3) . . ?
S22B Ag29 Ag28 102.64(3) . . ?
Ag40 Ag29 Ag28 108.76(2) . . ?
Cu3B Ag29 Ag28 77.24(2) . . ?
O7B Ag29 Ag31 79.20(8) . . ?
S10B Ag29 Ag31 135.52(3) . . ?
S22B Ag29 Ag31 54.21(3) . . ?
Ag40 Ag29 Ag31 157.596(19) . . ?
Cu3B Ag29 Ag31 92.34(2) . . ?
Ag28 Ag29 Ag31 77.987(15) . . ?
O7B Ag29 Ag30 80.12(8) . . ?
S10B Ag29 Ag30 136.19(3) . . ?
S22B Ag29 Ag30 54.32(3) . . ?
Ag40 Ag29 Ag30 78.392(15) . . ?
Cu3B Ag29 Ag30 85.36(2) . . ?
Ag28 Ag29 Ag30 156.876(19) . . ?
Ag31 Ag29 Ag30 87.746(14) . . ?
S15B Ag30 O8B 115.05(9) . . ?
S15B Ag30 S11B 137.98(4) . . ?
O8B Ag30 S11B 93.84(9) . . ?
S15B Ag30 S22B 107.95(5) . . ?
O8B Ag30 S22B 94.77(9) . . ?
S11B Ag30 S22B 98.69(4) . . ?
S15B Ag30 Ag36 91.81(3) . 2_756 ?
O8B Ag30 Ag36 140.67(8) . 2_756 ?
S11B Ag30 Ag36 49.71(3) . 2_756 ?
S22B Ag30 Ag36 103.96(3) . 2_756 ?
S15B Ag30 Ag29 81.11(3) . . ?
O8B Ag30 Ag29 75.21(8) . . ?
S11B Ag30 Ag29 138.05(3) . . ?
S22B Ag30 Ag29 44.03(2) . . ?
Ag36 Ag30 Ag29 140.22(2) 2_756 . ?
S13B Ag31 O9B 118.24(8) . . ?
S13B Ag31 S12B 134.69(4) . . ?
O9B Ag31 S12B 93.57(9) . . ?
S13B Ag31 S22B 108.29(5) . . ?
O9B Ag31 S22B 94.99(8) . . ?
S12B Ag31 S22B 99.33(4) . . ?
S13B Ag31 Ag25 87.64(3) . . ?
O9B Ag31 Ag25 141.31(8) . . ?
S12B Ag31 Ag25 50.56(3) . . ?
S22B Ag31 Ag25 103.85(3) . . ?
S13B Ag31 Ag29 82.88(3) . . ?
O9B Ag31 Ag29 75.78(8) . . ?
S12B Ag31 Ag29 139.04(3) . . ?
S22B Ag31 Ag29 44.25(3) . . ?
Ag25 Ag31 Ag29 139.48(2) . . ?
S13B Ag31 Ag43 162.78(4) . . ?
O9B Ag31 Ag43 76.55(8) . . ?
S12B Ag31 Ag43 45.96(3) . . ?
S22B Ag31 Ag43 59.19(3) . . ?
Ag25 Ag31 Ag43 84.519(15) . . ?
Ag29 Ag31 Ag43 93.180(15) . . ?
O10B Ag32 S21B 116.82(10) . . ?
O10B Ag32 S12B 94.80(10) . . ?
S21B Ag32 S12B 136.12(4) . . ?
O10B Ag32 S23B 95.12(10) . . ?
S21B Ag32 S23B 107.44(5) . . ?
S12B Ag32 S23B 98.47(5) . . ?
O10B Ag32 Cu4B 140.76(9) . . ?
S21B Ag32 Cu4B 90.43(4) . . ?
S12B Ag32 Cu4B 81.38(4) . . ?
S23B Ag32 Cu4B 47.74(4) . . ?
O10B Ag32 Ag25 142.10(10) . . ?
S21B Ag32 Ag25 89.57(3) . . ?
S12B Ag32 Ag25 49.86(3) . . ?
S23B Ag32 Ag25 102.54(4) . . ?
Cu4B Ag32 Ag25 57.67(2) . . ?
O10B Ag32 Ag34 73.98(10) . . ?
S21B Ag32 Ag34 82.28(3) . . ?
S12B Ag32 Ag34 138.26(3) . . ?
S23B Ag32 Ag34 44.91(4) . . ?
Cu4B Ag32 Ag34 83.14(3) . . ?
Ag25 Ag32 Ag34 139.96(2) . . ?
O10B Ag32 Ag43 77.67(9) . . ?
S21B Ag32 Ag43 162.04(4) . . ?
S12B Ag32 Ag43 45.85(3) . . ?
S23B Ag32 Ag43 58.51(4) . . ?
Cu4B Ag32 Ag43 71.84(3) . . ?
Ag25 Ag32 Ag43 83.422(15) . . ?
Ag34 Ag32 Ag43 92.468(15) . . ?
S14B Ag33 O11B 119.28(9) 2_756 . ?
S14B Ag33 S11B 136.73(5) 2_756 . ?
O11B Ag33 S11B 92.65(9) . . ?
S14B Ag33 S23B 107.81(5) 2_756 . ?
O11B Ag33 S23B 95.24(9) . . ?
S11B Ag33 S23B 96.41(5) . . ?
S14B Ag33 Ag36 90.37(4) 2_756 2_756 ?
O11B Ag33 Ag36 139.82(9) . 2_756 ?
S11B Ag33 Ag36 49.33(3) . 2_756 ?
S23B Ag33 Ag36 100.87(4) . 2_756 ?
S14B Ag33 Ag34 82.55(4) 2_756 . ?
O11B Ag33 Ag34 75.94(9) . . ?
S11B Ag33 Ag34 136.59(3) . . ?
S23B Ag33 Ag34 44.91(4) . . ?
Ag36 Ag33 Ag34 138.68(2) 2_756 . ?
O12B Ag34 S23B 114.46(11) . . ?
O12B Ag34 S9B 110.46(11) . 2_756 ?
S23B Ag34 S9B 135.08(6) . 2_756 ?
O12B Ag34 Cu5B 162.57(10) . 2_756 ?
S23B Ag34 Cu5B 50.81(5) . 2_756 ?
S9B Ag34 Cu5B 84.92(4) 2_756 2_756 ?
O12B Ag34 Ag38 116.36(10) . 2_756 ?
S23B Ag34 Ag38 100.90(4) . 2_756 ?
S9B Ag34 Ag38 57.75(3) 2_756 2_756 ?
Cu5B Ag34 Ag38 64.21(2) 2_756 2_756 ?
O12B Ag34 Ag27 115.26(9) . 2_756 ?
S23B Ag34 Ag27 101.91(4) . 2_756 ?
S9B Ag34 Ag27 56.71(3) 2_756 2_756 ?
Cu5B Ag34 Ag27 79.69(3) 2_756 2_756 ?
Ag38 Ag34 Ag27 106.02(2) 2_756 2_756 ?
O12B Ag34 Ag33 80.46(10) . . ?
S23B Ag34 Ag33 56.00(4) . . ?
S9B Ag34 Ag33 134.37(3) 2_756 . ?
Cu5B Ag34 Ag33 94.76(2) 2_756 . ?
Ag38 Ag34 Ag33 156.608(18) 2_756 . ?
Ag27 Ag34 Ag33 78.272(16) 2_756 . ?
O12B Ag34 Ag32 81.45(10) . . ?
S23B Ag34 Ag32 54.92(4) . . ?
S9B Ag34 Ag32 135.36(3) 2_756 . ?
Cu5B Ag34 Ag32 81.74(2) 2_756 . ?
Ag38 Ag34 Ag32 78.162(15) 2_756 . ?
Ag27 Ag34 Ag32 156.574(18) 2_756 . ?
Ag33 Ag34 Ag32 89.219(15) . . ?
O13B Ag35 S15B 115.96(11) . 2_756 ?
O13B Ag35 S7B 91.34(10) . . ?
S15B Ag35 S7B 138.07(5) 2_756 . ?
O13B Ag35 S17B 94.27(8) . . ?
S15B Ag35 S17B 108.92(4) 2_756 . ?
S7B Ag35 S17B 99.37(4) . . ?
O13B Ag35 Ag39 138.55(9) . 2_756 ?
S15B Ag35 Ag39 92.42(4) 2_756 2_756 ?
S7B Ag35 Ag39 49.85(3) . 2_756 ?
S17B Ag35 Ag39 104.76(4) . 2_756 ?
O13B Ag35 Ag36 74.33(8) . . ?
S15B Ag35 Ag36 82.37(4) 2_756 . ?
S7B Ag35 Ag36 137.87(3) . . ?
S17B Ag35 Ag36 44.60(4) . . ?
Ag39 Ag35 Ag36 142.64(2) 2_756 . ?
O14B Ag36 S11B 111.44(13) . 2_756 ?
O14B Ag36 S17B 113.06(13) . . ?
S11B Ag36 S17B 135.48(4) 2_756 . ?
O14B Ag36 Ag30 114.11(11) . 2_756 ?
S11B Ag36 Ag30 58.02(3) 2_756 2_756 ?
S17B Ag36 Ag30 101.49(3) . 2_756 ?
O14B Ag36 Ag33 117.12(10) . 2_756 ?
S11B Ag36 Ag33 56.88(3) 2_756 2_756 ?
S17B Ag36 Ag33 102.29(3) . 2_756 ?
Ag30 Ag36 Ag33 107.024(19) 2_756 2_756 ?
O14B Ag36 Cu1B 163.70(12) . . ?
S11B Ag36 Cu1B 84.46(4) 2_756 . ?
S17B Ag36 Cu1B 51.05(3) . . ?
Ag30 Ag36 Cu1B 70.599(19) 2_756 . ?
Ag33 Ag36 Cu1B 73.986(19) 2_756 . ?
O14B Ag36 Ag37 82.01(12) . . ?
S11B Ag36 Ag37 134.53(3) 2_756 . ?
S17B Ag36 Ag37 54.96(3) . . ?
Ag30 Ag36 Ag37 156.21(2) 2_756 . ?
Ag33 Ag36 Ag37 78.079(16) 2_756 . ?
Cu1B Ag36 Ag37 89.25(2) . . ?
O14B Ag36 Ag35 80.02(11) . . ?
S11B Ag36 Ag35 134.90(3) 2_756 . ?
S17B Ag36 Ag35 54.45(3) . . ?
Ag30 Ag36 Ag35 77.259(16) 2_756 . ?
Ag33 Ag36 Ag35 156.39(2) 2_756 . ?
Cu1B Ag36 Ag35 86.16(2) . . ?
Ag37 Ag36 Ag35 89.219(18) . . ?
O15B Ag37 S14B 116.50(11) . . ?
O15B Ag37 S8B 92.82(10) . . ?
S14B Ag37 S8B 138.49(5) . . ?
O15B Ag37 S17B 95.09(9) . . ?
S14B Ag37 S17B 107.31(4) . . ?
S8B Ag37 S17B 97.90(4) . . ?
O15B Ag37 Ag26 139.98(10) . . ?
S14B Ag37 Ag26 93.06(4) . . ?
S8B Ag37 Ag26 49.13(3) . . ?
S17B Ag37 Ag26 101.35(4) . . ?
O15B Ag37 Ag36 74.66(9) . . ?
S14B Ag37 Ag36 81.67(4) . . ?
S8B Ag37 Ag36 136.94(3) . . ?
S17B Ag37 Ag36 44.55(4) . . ?
Ag26 Ag37 Ag36 139.625(19) . . ?
O16B Ag38 S21B 119.65(10) . 2_756 ?
O16B Ag38 S9B 89.73(9) . . ?
S21B Ag38 S9B 137.05(5) 2_756 . ?
O16B Ag38 S20B 93.96(10) . . ?
S21B Ag38 S20B 110.63(4) 2_756 . ?
S9B Ag38 S20B 96.43(4) . . ?
O16B Ag38 Ag34 137.66(9) . 2_756 ?
S21B Ag38 Ag34 90.37(4) 2_756 2_756 ?
S9B Ag38 Ag34 50.32(3) . 2_756 ?
S20B Ag38 Ag34 102.86(3) . 2_756 ?
O16B Ag38 Cu5B 135.84(10) . . ?
S21B Ag38 Cu5B 97.01(4) 2_756 . ?
S9B Ag38 Cu5B 77.03(3) . . ?
S20B Ag38 Cu5B 47.40(4) . . ?
Ag34 Ag38 Cu5B 57.16(2) 2_756 . ?
O16B Ag38 Ag39 75.04(9) . . ?
S21B Ag38 Ag39 84.47(4) 2_756 . ?
S9B Ag38 Ag39 136.13(4) . . ?
S20B Ag38 Ag39 45.65(3) . . ?
Ag34 Ag38 Ag39 141.731(19) 2_756 . ?
Cu5B Ag38 Ag39 85.82(2) . . ?
O17B Ag39 S7B 111.61(10) . 2_756 ?
O17B Ag39 S20B 112.48(10) . . ?
S7B Ag39 S20B 135.91(5) 2_756 . ?
O17B Ag39 Ag35 116.95(12) . 2_756 ?
S7B Ag39 Ag35 57.60(4) 2_756 2_756 ?
S20B Ag39 Ag35 101.16(4) . 2_756 ?
O17B Ag39 Ag23 114.94(12) . 2_756 ?
S7B Ag39 Ag23 57.94(4) 2_756 2_756 ?
S20B Ag39 Ag23 102.23(4) . 2_756 ?
Ag35 Ag39 Ag23 107.253(19) 2_756 2_756 ?
O17B Ag39 Ag41 164.26(10) . . ?
S7B Ag39 Ag41 84.13(3) 2_756 . ?
S20B Ag39 Ag41 51.78(3) . . ?
Ag35 Ag39 Ag41 71.128(18) 2_756 . ?
Ag23 Ag39 Ag41 72.452(18) 2_756 . ?
O17B Ag39 Ag38 79.81(11) . . ?
S7B Ag39 Ag38 134.46(4) 2_756 . ?
S20B Ag39 Ag38 55.68(4) . . ?
Ag35 Ag39 Ag38 156.46(2) 2_756 . ?
Ag23 Ag39 Ag38 77.035(18) 2_756 . ?
Ag41 Ag39 Ag38 88.882(18) . . ?
O17B Ag39 Ag40 80.73(11) . . ?
S7B Ag39 Ag40 133.58(4) 2_756 . ?
S20B Ag39 Ag40 55.64(4) . . ?
Ag35 Ag39 Ag40 76.653(18) 2_756 . ?
Ag23 Ag39 Ag40 157.54(2) 2_756 . ?
Ag41 Ag39 Ag40 88.617(19) . . ?
Ag38 Ag39 Ag40 90.957(17) . . ?
O18B Ag40 S15B 120.05(8) . . ?
O18B Ag40 S10B 89.81(8) . . ?
S15B Ag40 S10B 137.07(5) . . ?
O18B Ag40 S20B 94.20(11) . . ?
S15B Ag40 S20B 109.94(5) . . ?
S10B Ag40 S20B 96.48(4) . . ?
O18B Ag40 Ag29 137.67(8) . . ?
S15B Ag40 Ag29 90.98(4) . . ?
S10B Ag40 Ag29 49.82(3) . . ?
S20B Ag40 Ag29 101.64(3) . . ?
O18B Ag40 Ag39 75.59(9) . . ?
S15B Ag40 Ag39 84.04(4) . . ?
S10B Ag40 Ag39 136.20(4) . . ?
S20B Ag40 Ag39 45.39(3) . . ?
Ag29 Ag40 Ag39 140.442(19) . . ?
S25B Ag41 S20B 71.56(6) . . ?
S25B Ag41 S16B 160.31(6) . 2_756 ?
S20B Ag41 S16B 127.12(6) . 2_756 ?
S25B Ag41 S17B 66.09(5) . 2_756 ?
S20B Ag41 S17B 126.77(5) . 2_756 ?
S16B Ag41 S17B 100.60(5) 2_756 2_756 ?
S25B Ag41 Cu2B 101.73(5) . 2_756 ?
S20B Ag41 Cu2B 163.40(4) . 2_756 ?
S16B Ag41 Cu2B 58.59(4) 2_756 2_756 ?
S17B Ag41 Cu2B 59.52(3) 2_756 2_756 ?
S25B Ag41 S2C 71.08(5) . . ?
S20B Ag41 S2C 99.21(4) . . ?
S16B Ag41 S2C 97.30(4) 2_756 . ?
S17B Ag41 S2C 96.17(3) 2_756 . ?
Cu2B Ag41 S2C 64.199(18) 2_756 . ?
S25B Ag41 Cu4B 134.04(5) . 2_756 ?
S20B Ag41 Cu4B 95.28(5) . 2_756 ?
S16B Ag41 Cu4B 47.10(4) 2_756 2_756 ?
S17B Ag41 Cu4B 137.50(4) 2_756 2_756 ?
Cu2B Ag41 Cu4B 78.37(3) 2_756 2_756 ?
S2C Ag41 Cu4B 67.92(2) . 2_756 ?
S25B Ag41 Ag39 95.02(5) . . ?
S20B Ag41 Ag39 49.91(3) . . ?
S16B Ag41 Ag39 102.40(4) 2_756 . ?
S17B Ag41 Ag39 103.21(3) 2_756 . ?
Cu2B Ag41 Ag39 146.68(2) 2_756 . ?
S2C Ag41 Ag39 149.119(18) . . ?
Cu4B Ag41 Ag39 109.78(3) 2_756 . ?
S25B Ag41 Cu5B 92.16(5) . . ?
S20B Ag41 Cu5B 49.08(4) . . ?
S16B Ag41 Cu5B 96.95(4) 2_756 . ?
S17B Ag41 Cu5B 155.23(4) 2_756 . ?
Cu2B Ag41 Cu5B 117.79(3) 2_756 . ?
S2C Ag41 Cu5B 64.180(19) . . ?
Cu4B Ag41 Cu5B 51.51(3) 2_756 . ?
Ag39 Ag41 Cu5B 89.80(2) . . ?
S25B Ag41 Cu3B 32.78(4) . . ?
S20B Ag41 Cu3B 49.93(4) . . ?
S16B Ag41 Cu3B 152.10(4) 2_756 . ?
S17B Ag41 Cu3B 98.46(4) 2_756 . ?
Cu2B Ag41 Cu3B 116.67(3) 2_756 . ?
S2C Ag41 Cu3B 60.390(18) . . ?
Cu4B Ag41 Cu3B 105.77(3) 2_756 . ?
Ag39 Ag41 Cu3B 92.78(2) . . ?
Cu5B Ag41 Cu3B 59.42(3) . . ?
S9B Ag42 S10B 171.48(4) . . ?
S12B Ag43 S11B 171.01(6) . . ?
S12B Ag43 Ag31 49.74(3) . . ?
S11B Ag43 Ag31 134.22(3) . . ?
S12B Ag43 Ag32 49.25(3) . . ?
S11B Ag43 Ag32 133.07(3) . . ?
Ag31 Ag43 Ag32 87.795(15) . . ?
S9B Cu7B S10B 171.48(4) . . ?
S12B Cu8B S11B 171.01(6) . . ?
S25B Cu1B S19B 118.37(8) 2_756 . ?
S25B Cu1B S17B 71.42(5) 2_756 . ?
S19B Cu1B S17B 71.05(5) . . ?
S25B Cu1B S22B 70.64(6) 2_756 2_756 ?
S19B Cu1B S22B 159.53(5) . 2_756 ?
S17B Cu1B S22B 128.80(5) . 2_756 ?
S25B Cu1B S23B 162.18(6) 2_756 2_756 ?
S19B Cu1B S23B 65.32(6) . 2_756 ?
S17B Cu1B S23B 124.11(5) . 2_756 ?
S22B Cu1B S23B 100.49(5) 2_756 2_756 ?
S25B Cu1B Ag36 96.31(5) 2_756 . ?
S19B Cu1B Ag36 94.12(4) . . ?
S17B Cu1B Ag36 49.12(4) . . ?
S22B Cu1B Ag36 103.37(4) 2_756 . ?
S23B Cu1B Ag36 100.86(4) 2_756 . ?
S24B Cu2B S19B 118.12(7) . . ?
S24B Cu2B S18B 72.08(6) . . ?
S19B Cu2B S18B 69.68(6) . . ?
S24B Cu2B S16B 68.27(7) . . ?
S19B Cu2B S16B 161.71(6) . . ?
S18B Cu2B S16B 127.49(6) . . ?
S24B Cu2B S17B 161.53(6) . . ?
S19B Cu2B S17B 66.82(5) . . ?
S18B Cu2B S17B 124.43(6) . . ?
S16B Cu2B S17B 101.78(5) . . ?
S24B Cu2B Ag41 101.63(6) . 2_756 ?
S19B Cu2B Ag41 102.21(5) . 2_756 ?
S18B Cu2B Ag41 164.08(5) . 2_756 ?
S16B Cu2B Ag41 59.56(4) . 2_756 ?
S17B Cu2B Ag41 60.20(3) . 2_756 ?
S24B Cu2B Ag26 95.70(5) . . ?
S19B Cu2B Ag26 93.63(4) . . ?
S18B Cu2B Ag26 48.66(3) . . ?
S16B Cu2B Ag26 102.97(4) . . ?
S17B Cu2B Ag26 101.84(3) . . ?
Ag41 Cu2B Ag26 147.21(3) 2_756 . ?
S25B Cu3B S24B 118.90(7) . . ?
S25B Cu3B S22B 77.55(7) . . ?
S24B Cu3B S22B 70.91(6) . . ?
S25B Cu3B S20B 74.13(7) . . ?
S24B Cu3B S20B 149.33(7) . . ?
S22B Cu3B S20B 139.32(6) . . ?
S25B Cu3B Ag29 104.51(7) . . ?
S24B Cu3B Ag29 94.64(6) . . ?
S22B Cu3B Ag29 51.32(3) . . ?
S20B Cu3B Ag29 109.35(4) . . ?
S25B Cu3B Ag41 36.31(6) . . ?
S24B Cu3B Ag41 123.30(5) . . ?
S22B Cu3B Ag41 113.03(4) . . ?
S20B Cu3B Ag41 49.87(3) . . ?
Ag29 Cu3B Ag41 133.60(3) . . ?
S16B Cu4B S23B 163.81(8) . . ?
S16B Cu4B Cu5B 121.06(7) . 2_756 ?
S23B Cu4B Cu5B 54.67(5) . 2_756 ?
S16B Cu4B S24B 63.13(6) . . ?
S23B Cu4B S24B 133.02(7) . . ?
Cu5B Cu4B S24B 123.11(6) 2_756 . ?
S16B Cu4B Ag25 54.98(5) . . ?
S23B Cu4B Ag25 117.78(6) . . ?
Cu5B Cu4B Ag25 144.70(5) 2_756 . ?
S24B Cu4B Ag25 88.05(5) . . ?
S16B Cu4B Ag41 57.47(5) . 2_756 ?
S23B Cu4B Ag41 120.87(7) . 2_756 ?
Cu5B Cu4B Ag41 66.20(4) 2_756 2_756 ?
S24B Cu4B Ag41 79.55(5) . 2_756 ?
Ag25 Cu4B Ag41 109.18(3) . 2_756 ?
S16B Cu4B Ag32 106.27(6) . . ?
S23B Cu4B Ag32 60.39(5) . . ?
Cu5B Cu4B Ag32 91.92(4) 2_756 . ?
S24B Cu4B Ag32 144.42(7) . . ?
Ag25 Cu4B Ag32 61.28(3) . . ?
Ag41 Cu4B Ag32 125.40(4) 2_756 . ?
S23B Cu5B S19B 68.18(6) 2_756 . ?
S23B Cu5B S20B 150.71(7) 2_756 . ?
S19B Cu5B S20B 140.94(7) . . ?
S23B Cu5B Cu4B 56.00(5) 2_756 2_756 ?
S19B Cu5B Cu4B 95.47(5) . 2_756 ?
S20B Cu5B Cu4B 107.20(5) . 2_756 ?
S23B Cu5B Ag34 52.95(5) 2_756 2_756 ?
S19B Cu5B Ag34 91.19(5) . 2_756 ?
S20B Cu5B Ag34 115.45(4) . 2_756 ?
Cu4B Cu5B Ag34 98.69(4) 2_756 2_756 ?
S23B Cu5B Ag41 118.28(5) 2_756 . ?
S19B Cu5B Ag41 120.58(4) . . ?
S20B Cu5B Ag41 51.49(3) . . ?
Cu4B Cu5B Ag41 62.29(3) 2_756 . ?
Ag34 Cu5B Ag41 142.85(4) 2_756 . ?
S23B Cu5B Ag38 98.02(6) 2_756 . ?
S19B Cu5B Ag38 147.45(5) . . ?
S20B Cu5B Ag38 59.00(4) . . ?
Cu4B Cu5B Ag38 100.62(4) 2_756 . ?
Ag34 Cu5B Ag38 58.64(2) 2_756 . ?
Ag41 Cu5B Ag38 91.97(3) . . ?
S7B Cu6B S8B 171.60(5) . . ?
C3B C1B C2B 107.1(5) . . ?
C3B C1B C4B 119.1(5) . . ?
C2B C1B C4B 113.4(4) . . ?
C3B C1B S5B 102.9(4) . . ?
C2B C1B S5B 104.8(4) . . ?
C4B C1B S5B 108.1(4) . . ?
C1B C2B H2B1 109.5 . . ?
C1B C2B H2B2 109.5 . . ?
H2B1 C2B H2B2 109.5 . . ?
C1B C2B H2B3 109.5 . . ?
H2B1 C2B H2B3 109.5 . . ?
H2B2 C2B H2B3 109.5 . . ?
C1B C3B H3BA 109.5 . . ?
C1B C3B H3BB 109.5 . . ?
H3BA C3B H3BB 109.5 . . ?
C1B C3B H3BC 109.5 . . ?
H3BA C3B H3BC 109.5 . . ?
H3BB C3B H3BC 109.5 . . ?
C1B C4B H4B1 109.5 . . ?
C1B C4B H4B2 109.5 . . ?
H4B1 C4B H4B2 109.5 . . ?
C1B C4B H4B3 109.5 . . ?
H4B1 C4B H4B3 109.5 . . ?
H4B2 C4B H4B3 109.5 . . ?
C6B C5B C7B 107.0(5) . . ?
C6B C5B C8B 107.1(5) . . ?
C7B C5B C8B 112.1(5) . . ?
C6B C5B S2B 112.2(4) . . ?
C7B C5B S2B 109.6(4) . . ?
C8B C5B S2B 108.9(4) . . ?
C5B C6B H6BA 109.5 . . ?
C5B C6B H6BB 109.5 . . ?
H6BA C6B H6BB 109.5 . . ?
C5B C6B H6BC 109.5 . . ?
H6BA C6B H6BC 109.5 . . ?
H6BB C6B H6BC 109.5 . . ?
C5B C7B H7B1 109.5 . . ?
C5B C7B H7B2 109.5 . . ?
H7B1 C7B H7B2 109.5 . . ?
C5B C7B H7B3 109.5 . . ?
H7B1 C7B H7B3 109.5 . . ?
H7B2 C7B H7B3 109.5 . . ?
C5B C8B H8B1 109.5 . . ?
C5B C8B H8B2 109.5 . . ?
H8B1 C8B H8B2 109.5 . . ?
C5B C8B H8B3 109.5 . . ?
H8B1 C8B H8B3 109.5 . . ?
H8B2 C8B H8B3 109.5 . . ?
C10B C9B C11B 110.8(4) . . ?
C10B C9B C12B 109.0(5) . . ?
C11B C9B C12B 110.5(5) . . ?
C10B C9B S3B 111.8(4) . . ?
C11B C9B S3B 109.7(4) . . ?
C12B C9B S3B 104.9(4) . . ?
C9B C10B H10D 109.5 . . ?
C9B C10B H10E 109.5 . . ?
H10D C10B H10E 109.5 . . ?
C9B C10B H10F 109.5 . . ?
H10D C10B H10F 109.5 . . ?
H10E C10B H10F 109.5 . . ?
C9B C11B H11D 109.5 . . ?
C9B C11B H11E 109.5 . . ?
H11D C11B H11E 109.5 . . ?
C9B C11B H11F 109.5 . . ?
H11D C11B H11F 109.5 . . ?
H11E C11B H11F 109.5 . . ?
C9B C12B H12D 109.5 . . ?
C9B C12B H12E 109.5 . . ?
H12D C12B H12E 109.5 . . ?
C9B C12B H12F 109.5 . . ?
H12D C12B H12F 109.5 . . ?
H12E C12B H12F 109.5 . . ?
C14B C13B C16B 111.8(5) . . ?
C14B C13B C15B 109.1(6) . . ?
C16B C13B C15B 111.4(6) . . ?
C14B C13B S4B 103.6(5) . . ?
C16B C13B S4B 110.0(5) . . ?
C15B C13B S4B 110.8(5) . . ?
C13B C14B H14D 109.5 . . ?
C13B C14B H14E 109.5 . . ?
H14D C14B H14E 109.5 . . ?
C13B C14B H14F 109.5 . . ?
H14D C14B H14F 109.5 . . ?
H14E C14B H14F 109.5 . . ?
C13B C15B H15D 109.5 . . ?
C13B C15B H15E 109.5 . . ?
H15D C15B H15E 109.5 . . ?
C13B C15B H15F 109.5 . . ?
H15D C15B H15F 109.5 . . ?
H15E C15B H15F 109.5 . . ?
C13B C16B H16D 109.5 . . ?
C13B C16B H16E 109.5 . . ?
H16D C16B H16E 109.5 . . ?
C13B C16B H16F 109.5 . . ?
H16D C16B H16F 109.5 . . ?
H16E C16B H16F 109.5 . . ?
C18B C17B C20B 112.9(6) . . ?
C18B C17B C19B 105.9(5) . . ?
C20B C17B C19B 116.7(5) . . ?
C18B C17B S1B 109.4(4) . . ?
C20B C17B S1B 105.2(4) . . ?
C19B C17B S1B 106.5(5) . . ?
C17B C18B H18D 109.5 . . ?
C17B C18B H18E 109.5 . . ?
H18D C18B H18E 109.5 . . ?
C17B C18B H18F 109.5 . . ?
H18D C18B H18F 109.5 . . ?
H18E C18B H18F 109.5 . . ?
C17B C19B H19D 109.5 . . ?
C17B C19B H19E 109.5 . . ?
H19D C19B H19E 109.5 . . ?
C17B C19B H19F 109.5 . . ?
H19D C19B H19F 109.5 . . ?
H19E C19B H19F 109.5 . . ?
C17B C20B H20D 109.5 . . ?
C17B C20B H20E 109.5 . . ?
H20D C20B H20E 109.5 . . ?
C17B C20B H20F 109.5 . . ?
H20D C20B H20F 109.5 . . ?
H20E C20B H20F 109.5 . . ?
C23B C21B C22B 118.0(5) . . ?
C23B C21B C24B 106.7(5) . . ?
C22B C21B C24B 110.8(5) . . ?
C23B C21B S6B 106.6(4) . . ?
C22B C21B S6B 106.5(4) . . ?
C24B C21B S6B 107.8(4) . . ?
C21B C22B H22D 109.5 . . ?
C21B C22B H22E 109.5 . . ?
H22D C22B H22E 109.5 . . ?
C21B C22B H22F 109.5 . . ?
H22D C22B H22F 109.5 . . ?
H22E C22B H22F 109.5 . . ?
C21B C23B H23D 109.5 . . ?
C21B C23B H23E 109.5 . . ?
H23D C23B H23E 109.5 . . ?
C21B C23B H23F 109.5 . . ?
H23D C23B H23F 109.5 . . ?
H23E C23B H23F 109.5 . . ?
C21B C24B H24D 109.5 . . ?
C21B C24B H24E 109.5 . . ?
H24D C24B H24E 109.5 . . ?
C21B C24B H24F 109.5 . . ?
H24D C24B H24F 109.5 . . ?
H24E C24B H24F 109.5 . . ?
C28B C25B C27B 115.8(5) . . ?
C28B C25B C26B 115.4(5) . . ?
C27B C25B C26B 109.2(6) . . ?
C28B C25B S7B 107.5(4) . . ?
C27B C25B S7B 106.9(4) . . ?
C26B C25B S7B 100.5(4) . . ?
C25B C26B H26D 109.5 . . ?
C25B C26B H26E 109.5 . . ?
H26D C26B H26E 109.5 . . ?
C25B C26B H26F 109.5 . . ?
H26D C26B H26F 109.5 . . ?
H26E C26B H26F 109.5 . . ?
C25B C27B H27D 109.5 . . ?
C25B C27B H27E 109.5 . . ?
H27D C27B H27E 109.5 . . ?
C25B C27B H27F 109.5 . . ?
H27D C27B H27F 109.5 . . ?
H27E C27B H27F 109.5 . . ?
C25B C28B H28D 109.5 . . ?
C25B C28B H28E 109.5 . . ?
H28D C28B H28E 109.5 . . ?
C25B C28B H28F 109.5 . . ?
H28D C28B H28F 109.5 . . ?
H28E C28B H28F 109.5 . . ?
C32B C29B C30B 109.2(5) . . ?
C32B C29B C31B 114.7(6) . . ?
C30B C29B C31B 99.9(5) . . ?
C32B C29B S15B 111.2(4) . . ?
C30B C29B S15B 110.9(5) . . ?
C31B C29B S15B 110.4(4) . . ?
C29B C30B H30D 109.5 . . ?
C29B C30B H30E 109.5 . . ?
H30D C30B H30E 109.5 . . ?
C29B C30B H30F 109.5 . . ?
H30D C30B H30F 109.5 . . ?
H30E C30B H30F 109.5 . . ?
C29B C31B H31D 109.5 . . ?
C29B C31B H31E 109.5 . . ?
H31D C31B H31E 109.5 . . ?
C29B C31B H31F 109.5 . . ?
H31D C31B H31F 109.5 . . ?
H31E C31B H31F 109.5 . . ?
C29B C32B H32D 109.5 . . ?
C29B C32B H32E 109.5 . . ?
H32D C32B H32E 109.5 . . ?
C29B C32B H32F 109.5 . . ?
H32D C32B H32F 109.5 . . ?
H32E C32B H32F 109.5 . . ?
C36B C33B C34B 109.0(4) . . ?
C36B C33B C35B 109.5(5) . . ?
C34B C33B C35B 108.4(4) . . ?
C36B C33B S10B 108.8(3) . . ?
C34B C33B S10B 110.7(4) . . ?
C35B C33B S10B 110.4(3) . . ?
C33B C34B H34D 109.5 . . ?
C33B C34B H34E 109.5 . . ?
H34D C34B H34E 109.5 . . ?
C33B C34B H34F 109.5 . . ?
H34D C34B H34F 109.5 . . ?
H34E C34B H34F 109.5 . . ?
C33B C35B H35D 109.5 . . ?
C33B C35B H35E 109.5 . . ?
H35D C35B H35E 109.5 . . ?
C33B C35B H35F 109.5 . . ?
H35D C35B H35F 109.5 . . ?
H35E C35B H35F 109.5 . . ?
C33B C36B H36D 109.5 . . ?
C33B C36B H36E 109.5 . . ?
H36D C36B H36E 109.5 . . ?
C33B C36B H36F 109.5 . . ?
H36D C36B H36F 109.5 . . ?
H36E C36B H36F 109.5 . . ?
C40B C37B C39B 115.5(5) . . ?
C40B C37B C38B 109.5(5) . . ?
C39B C37B C38B 111.7(5) . . ?
C40B C37B S13B 108.0(4) . . ?
C39B C37B S13B 107.3(4) . . ?
C38B C37B S13B 104.1(4) . . ?
C37B C38B H38D 109.5 . . ?
C37B C38B H38E 109.5 . . ?
H38D C38B H38E 109.5 . . ?
C37B C38B H38F 109.5 . . ?
H38D C38B H38F 109.5 . . ?
H38E C38B H38F 109.5 . . ?
C37B C39B H39D 109.5 . . ?
C37B C39B H39E 109.5 . . ?
H39D C39B H39E 109.5 . . ?
C37B C39B H39F 109.5 . . ?
H39D C39B H39F 109.5 . . ?
H39E C39B H39F 109.5 . . ?
C37B C40B H40D 109.5 . . ?
C37B C40B H40E 109.5 . . ?
H40D C40B H40E 109.5 . . ?
C37B C40B H40F 109.5 . . ?
H40D C40B H40F 109.5 . . ?
H40E C40B H40F 109.5 . . ?
C44B C41B C43B 114.9(5) . . ?
C44B C41B C42B 111.5(5) . . ?
C43B C41B C42B 111.8(4) . . ?
C44B C41B S12B 105.3(4) . . ?
C43B C41B S12B 106.6(4) . . ?
C42B C41B S12B 105.9(4) . . ?
C41B C42B H42D 109.5 . . ?
C41B C42B H42E 109.5 . . ?
H42D C42B H42E 109.5 . . ?
C41B C42B H42F 109.5 . . ?
H42D C42B H42F 109.5 . . ?
H42E C42B H42F 109.5 . . ?
C41B C43B H43A 109.5 . . ?
C41B C43B H43B 109.5 . . ?
H43A C43B H43B 109.5 . . ?
C41B C43B H43C 109.5 . . ?
H43A C43B H43C 109.5 . . ?
H43B C43B H43C 109.5 . . ?
C41B C44B H44D 109.5 . . ?
C41B C44B H44E 109.5 . . ?
H44D C44B H44E 109.5 . . ?
C41B C44B H44F 109.5 . . ?
H44D C44B H44F 109.5 . . ?
H44E C44B H44F 109.5 . . ?
C46B C45B C47B 122.3(5) . . ?
C46B C45B C48B 100.1(6) . . ?
C47B C45B C48B 111.5(6) . . ?
C46B C45B S21B 104.2(4) . . ?
C47B C45B S21B 108.2(4) . . ?
C48B C45B S21B 109.8(4) . . ?
C45B C46B H46D 109.5 . . ?
C45B C46B H46E 109.5 . . ?
H46D C46B H46E 109.5 . . ?
C45B C46B H46F 109.5 . . ?
H46D C46B H46F 109.5 . . ?
H46E C46B H46F 109.5 . . ?
C45B C47B H47D 109.5 . . ?
C45B C47B H47E 109.5 . . ?
H47D C47B H47E 109.5 . . ?
C45B C47B H47F 109.5 . . ?
H47D C47B H47F 109.5 . . ?
H47E C47B H47F 109.5 . . ?
C45B C48B H48D 109.5 . . ?
C45B C48B H48E 109.5 . . ?
H48D C48B H48E 109.5 . . ?
C45B C48B H48F 109.5 . . ?
H48D C48B H48F 109.5 . . ?
H48E C48B H48F 109.5 . . ?
C59B C49B C58B 111.1(6) . . ?
C59B C49B C60B 123.6(5) . . ?
C58B C49B C60B 105.8(5) . . ?
C59B C49B S14B 106.1(4) . . ?
C58B C49B S14B 103.0(3) . . ?
C60B C49B S14B 105.3(4) . . ?
C53B C50B H50D 109.5 . . ?
C53B C50B H50E 109.5 . . ?
H50D C50B H50E 109.5 . . ?
C53B C50B H50F 109.5 . . ?
H50D C50B H50F 109.5 . . ?
H50E C50B H50F 109.5 . . ?
C53B C51B H51D 109.5 . . ?
C53B C51B H51E 109.5 . . ?
H51D C51B H51E 109.5 . . ?
C53B C51B H51F 109.5 . . ?
H51D C51B H51F 109.5 . . ?
H51E C51B H51F 109.5 . . ?
C53B C52B H52D 109.5 . . ?
C53B C52B H52E 109.5 . . ?
H52D C52B H52E 109.5 . . ?
C53B C52B H52F 109.5 . . ?
H52D C52B H52F 109.5 . . ?
H52E C52B H52F 109.5 . . ?
C50B C53B C51B 117.9(5) . . ?
C50B C53B C52B 115.1(5) . . ?
C51B C53B C52B 108.2(4) . . ?
C50B C53B S11B 106.0(4) . . ?
C51B C53B S11B 104.3(4) . . ?
C52B C53B S11B 103.7(3) . . ?
C57B C54B H54D 109.5 . . ?
C57B C54B H54E 109.5 . . ?
H54D C54B H54E 109.5 . . ?
C57B C54B H54F 109.5 . . ?
H54D C54B H54F 109.5 . . ?
H54E C54B H54F 109.5 . . ?
C57B C55B H55D 109.5 . . ?
C57B C55B H55E 109.5 . . ?
H55D C55B H55E 109.5 . . ?
C57B C55B H55F 109.5 . . ?
H55D C55B H55F 109.5 . . ?
H55E C55B H55F 109.5 . . ?
C57B C56B H56D 109.5 . . ?
C57B C56B H56E 109.5 . . ?
H56D C56B H56E 109.5 . . ?
C57B C56B H56F 109.5 . . ?
H56D C56B H56F 109.5 . . ?
H56E C56B H56F 109.5 . . ?
C56B C57B C55B 108.3(5) . . ?
C56B C57B C54B 108.6(4) . . ?
C55B C57B C54B 113.9(5) . . ?
C56B C57B S9B 110.0(3) . . ?
C55B C57B S9B 108.3(3) . . ?
C54B C57B S9B 107.7(4) . . ?
C49B C58B H58D 109.5 . . ?
C49B C58B H58E 109.5 . . ?
H58D C58B H58E 109.5 . . ?
C49B C58B H58F 109.5 . . ?
H58D C58B H58F 109.5 . . ?
H58E C58B H58F 109.5 . . ?
C49B C59B H59D 109.5 . . ?
C49B C59B H59E 109.5 . . ?
H59D C59B H59E 109.5 . . ?
C49B C59B H59F 109.5 . . ?
H59D C59B H59F 109.5 . . ?
H59E C59B H59F 109.5 . . ?
C49B C60B H60D 109.5 . . ?
C49B C60B H60E 109.5 . . ?
H60D C60B H60E 109.5 . . ?
C49B C60B H60F 109.5 . . ?
H60D C60B H60F 109.5 . . ?
H60E C60B H60F 109.5 . . ?
C62B C61B C63B 109.0(6) . . ?
C62B C61B C64B 114.4(5) . . ?
C63B C61B C64B 113.7(5) . . ?
C62B C61B S8B 107.0(4) . . ?
C63B C61B S8B 107.7(4) . . ?
C64B C61B S8B 104.6(4) . . ?
C61B C62B H62D 109.5 . . ?
C61B C62B H62E 109.5 . . ?
H62D C62B H62E 109.5 . . ?
C61B C62B H62F 109.5 . . ?
H62D C62B H62F 109.5 . . ?
H62E C62B H62F 109.5 . . ?
C61B C63B H63D 109.5 . . ?
C61B C63B H63E 109.5 . . ?
H63D C63B H63E 109.5 . . ?
C61B C63B H63F 109.5 . . ?
H63D C63B H63F 109.5 . . ?
H63E C63B H63F 109.5 . . ?
C61B C64B H64D 109.5 . . ?
C61B C64B H64E 109.5 . . ?
H64D C64B H64E 109.5 . . ?
C61B C64B H64F 109.5 . . ?
H64D C64B H64F 109.5 . . ?
H64E C64B H64F 109.5 . . ?
S1B O1B Ag23 124.5(2) . . ?
S1B O2B Ag24 124.9(2) . . ?
S1B O3B Ag25 118.2(2) . . ?
S2B O4B Ag26 124.95(18) . . ?
S2B O5B Ag27 123.6(2) . . ?
S2B O6B Ag28 122.0(2) . . ?
S3B O7B Ag29 123.4(2) . . ?
S3B O8B Ag30 123.1(2) . . ?
S3B O9B Ag31 121.7(2) . . ?
S4B O10B Ag32 126.6(3) . . ?
S4B O11B Ag33 121.9(2) . . ?
S4B O12B Ag34 118.1(2) . . ?
S5B O13B Ag35 124.28(18) . . ?
S5B O14B Ag36 120.6(3) . . ?
S5B O15B Ag37 123.41(19) . . ?
S6B O16B Ag38 124.08(19) . . ?
S6B O17B Ag39 120.3(2) . . ?
S6B O18B Ag40 120.9(2) . . ?
O1B S1B O3B 111.3(3) . . ?
O1B S1B O2B 112.6(3) . . ?
O3B S1B O2B 116.1(2) . . ?
O1B S1B C17B 105.1(3) . . ?
O3B S1B C17B 102.3(3) . . ?
O2B S1B C17B 108.1(3) . . ?
O4B S2B O5B 112.8(2) . . ?
O4B S2B O6B 109.2(2) . . ?
O5B S2B O6B 115.8(2) . . ?
O4B S2B C5B 106.2(2) . . ?
O5B S2B C5B 105.2(3) . . ?
O6B S2B C5B 107.0(3) . . ?
O8B S3B O7B 115.2(2) . . ?
O8B S3B O9B 112.8(2) . . ?
O7B S3B O9B 111.9(2) . . ?
O8B S3B C9B 106.1(2) . . ?
O7B S3B C9B 104.5(2) . . ?
O9B S3B C9B 105.2(2) . . ?
O10B S4B O11B 115.5(2) . . ?
O10B S4B O12B 112.1(3) . . ?
O11B S4B O12B 114.0(2) . . ?
O10B S4B C13B 106.3(3) . . ?
O11B S4B C13B 106.3(3) . . ?
O12B S4B C13B 101.1(3) . . ?
O13B S5B O15B 119.6(3) . . ?
O13B S5B O14B 109.0(2) . . ?
O15B S5B O14B 113.0(2) . . ?
O13B S5B C1B 102.7(2) . . ?
O15B S5B C1B 104.0(2) . . ?
O14B S5B C1B 107.3(3) . . ?
O16B S6B O18B 116.3(2) . . ?
O16B S6B O17B 112.0(2) . . ?
O18B S6B O17B 114.7(2) . . ?
O16B S6B C21B 103.8(3) . . ?
O18B S6B C21B 102.3(3) . . ?
O17B S6B C21B 105.9(2) . . ?
C25B S7B Ag39 116.45(19) . 2_756 ?
C25B S7B Cu6B 118.90(19) . . ?
Ag39 S7B Cu6B 124.63(5) 2_756 . ?
C25B S7B Ag35 111.8(2) . . ?
Ag39 S7B Ag35 72.55(4) 2_756 . ?
Cu6B S7B Ag35 85.96(5) . . ?
C25B S7B Ag23 114.8(2) . . ?
Ag39 S7B Ag23 72.32(4) 2_756 . ?
Cu6B S7B Ag23 86.12(5) . . ?
Ag35 S7B Ag23 130.31(5) . . ?
C61B S8B Ag26 119.71(18) . . ?
C61B S8B Cu6B 117.31(18) . . ?
Ag26 S8B Cu6B 122.98(5) . . ?
C61B S8B Ag24 113.8(2) . . ?
Ag26 S8B Ag24 72.78(4) . . ?
Cu6B S8B Ag24 85.22(4) . . ?
C61B S8B Ag37 112.4(2) . . ?
Ag26 S8B Ag37 72.24(4) . . ?
Cu6B S8B Ag37 86.53(5) . . ?
Ag24 S8B Ag37 131.44(5) . . ?
C57B S9B Ag34 114.60(19) . 2_756 ?
C57B S9B Cu7B 120.06(19) . . ?
Ag34 S9B Cu7B 125.34(5) 2_756 . ?
C57B S9B Ag42 120.06(19) . . ?
Ag34 S9B Ag42 125.34(5) 2_756 . ?
C57B S9B Ag27 112.85(15) . . ?
Ag34 S9B Ag27 73.27(4) 2_756 . ?
Cu7B S9B Ag27 86.26(4) . . ?
Ag42 S9B Ag27 86.26(4) . . ?
C57B S9B Ag38 113.76(15) . . ?
Ag34 S9B Ag38 71.93(3) 2_756 . ?
Cu7B S9B Ag38 85.69(4) . . ?
Ag42 S9B Ag38 85.69(4) . . ?
Ag27 S9B Ag38 130.04(4) . . ?
C33B S10B Ag29 115.8(2) . . ?
C33B S10B Cu7B 119.8(2) . . ?
Ag29 S10B Cu7B 124.37(5) . . ?
C33B S10B Ag42 119.8(2) . . ?
Ag29 S10B Ag42 124.37(5) . . ?
C33B S10B Ag40 113.73(16) . . ?
Ag29 S10B Ag40 71.73(3) . . ?
Cu7B S10B Ag40 85.81(4) . . ?
Ag42 S10B Ag40 85.81(4) . . ?
C33B S10B Ag28 112.00(16) . . ?
Ag29 S10B Ag28 72.50(4) . . ?
Cu7B S10B Ag28 87.29(5) . . ?
Ag42 S10B Ag28 87.29(5) . . ?
Ag40 S10B Ag28 130.62(5) . . ?
C53B S11B Ag36 118.56(16) . 2_756 ?
C53B S11B Cu8B 116.62(17) . . ?
Ag36 S11B Cu8B 124.78(6) 2_756 . ?
C53B S11B Ag43 116.62(17) . . ?
Ag36 S11B Ag43 124.78(6) 2_756 . ?
C53B S11B Ag33 113.38(15) . . ?
Ag36 S11B Ag33 73.79(4) 2_756 . ?
Cu8B S11B Ag33 86.87(4) . . ?
Ag43 S11B Ag33 86.87(4) . . ?
C53B S11B Ag30 112.77(15) . . ?
Ag36 S11B Ag30 72.27(4) 2_756 . ?
Cu8B S11B Ag30 85.17(4) . . ?
Ag43 S11B Ag30 85.17(4) . . ?
Ag33 S11B Ag30 131.64(6) . . ?
C41B S12B Ag25 117.87(16) . . ?
C41B S12B Cu8B 117.91(16) . . ?
Ag25 S12B Cu8B 124.15(6) . . ?
C41B S12B Ag43 117.91(16) . . ?
Ag25 S12B Ag43 124.15(6) . . ?
C41B S12B Ag32 115.32(16) . . ?
Ag25 S12B Ag32 74.44(4) . . ?
Cu8B S12B Ag32 84.91(4) . . ?
Ag43 S12B Ag32 84.91(4) . . ?
C41B S12B Ag31 112.45(16) . . ?
Ag25 S12B Ag31 72.42(4) . . ?
Cu8B S12B Ag31 84.30(4) . . ?
Ag43 S12B Ag31 84.30(4) . . ?
Ag32 S12B Ag31 130.44(6) . . ?
C37B S13B Ag24 113.05(17) . . ?
C37B S13B Ag28 113.41(17) . . ?
Ag24 S13B Ag28 103.62(6) . . ?
C37B S13B Ag31 112.98(19) . . ?
Ag24 S13B Ag31 108.16(5) . . ?
Ag28 S13B Ag31 104.87(5) . . ?
C49B S14B Ag33 113.02(19) . 2_756 ?
C49B S14B Ag37 112.44(16) . . ?
Ag33 S14B Ag37 107.19(5) 2_756 . ?
C49B S14B Ag27 113.33(17) . . ?
Ag33 S14B Ag27 106.93(5) 2_756 . ?
Ag37 S14B Ag27 103.25(6) . . ?
C29B S15B Ag30 112.1(2) . . ?
C29B S15B Ag40 114.75(18) . . ?
Ag30 S15B Ag40 106.53(5) . . ?
C29B S15B Ag35 113.9(2) . 2_756 ?
Ag30 S15B Ag35 104.98(5) . 2_756 ?
Ag40 S15B Ag35 103.70(6) . 2_756 ?
Cu4B S16B Ag25 75.92(6) . . ?
Cu4B S16B Cu2B 95.17(6) . . ?
Ag25 S16B Cu2B 143.03(7) . . ?
Cu4B S16B Ag41 75.43(6) . 2_756 ?
Ag25 S16B Ag41 143.61(6) . 2_756 ?
Cu2B S16B Ag41 61.85(5) . 2_756 ?
Cu4B S16B Ag24 133.47(8) . . ?
Ag25 S16B Ag24 78.89(5) . . ?
Cu2B S16B Ag24 82.32(4) . . ?
Ag41 S16B Ag24 137.50(7) 2_756 . ?
Cu4B S16B Ag23 96.83(6) . . ?
Ag25 S16B Ag23 79.08(5) . . ?
Cu2B S16B Ag23 137.89(7) . . ?
Ag41 S16B Ag23 82.53(5) 2_756 . ?
Ag24 S16B Ag23 115.96(5) . . ?
Ag36 S17B Cu1B 79.83(5) . . ?
Ag36 S17B Cu2B 145.38(5) . . ?
Cu1B S17B Cu2B 83.16(4) . . ?
Ag36 S17B Ag41 143.83(5) . 2_756 ?
Cu1B S17B Ag41 80.70(4) . 2_756 ?
Cu2B S17B Ag41 60.28(4) . 2_756 ?
Ag36 S17B Ag35 80.95(4) . . ?
Cu1B S17B Ag35 115.52(5) . . ?
Cu2B S17B Ag35 133.67(6) . . ?
Ag41 S17B Ag35 80.40(3) 2_756 . ?
Ag36 S17B Ag37 80.50(4) . . ?
Cu1B S17B Ag37 120.08(5) . . ?
Cu2B S17B Ag37 82.37(4) . . ?
Ag41 S17B Ag37 135.66(6) 2_756 . ?
Ag35 S17B Ag37 116.25(4) . . ?
Ag26 S18B Cu2B 78.38(5) . . ?
Ag26 S18B Ag27 81.12(5) . . ?
Cu2B S18B Ag27 118.44(7) . . ?
Ag26 S18B Ag28 80.91(5) . . ?
Cu2B S18B Ag28 116.00(6) . . ?
Ag27 S18B Ag28 116.94(5) . . ?
Cu2B S19B Cu1B 105.71(6) . . ?
Cu2B S19B Cu5B 116.93(8) . . ?
Cu1B S19B Cu5B 102.47(6) . . ?
Cu5B S20B Ag39 131.27(7) . . ?
Cu5B S20B Cu3B 79.79(5) . . ?
Ag39 S20B Cu3B 136.80(7) . . ?
Cu5B S20B Ag41 79.43(5) . . ?
Ag39 S20B Ag41 78.31(4) . . ?
Cu3B S20B Ag41 80.20(5) . . ?
Cu5B S20B Ag38 73.60(5) . . ?
Ag39 S20B Ag38 78.67(5) . . ?
Cu3B S20B Ag38 144.48(6) . . ?
Ag41 S20B Ag38 116.59(6) . . ?
Cu5B S20B Ag40 149.49(6) . . ?
Ag39 S20B Ag40 78.97(4) . . ?
Cu3B S20B Ag40 77.72(5) . . ?
Ag41 S20B Ag40 116.29(6) . . ?
Ag38 S20B Ag40 115.80(5) . . ?
C45B S21B Ag32 113.5(2) . . ?
C45B S21B Ag23 111.61(18) . . ?
Ag32 S21B Ag23 107.23(5) . . ?
C45B S21B Ag38 114.53(16) . 2_756 ?
Ag32 S21B Ag38 106.05(5) . 2_756 ?
Ag23 S21B Ag38 103.16(6) . 2_756 ?
Ag29 S22B Cu3B 75.99(4) . . ?
Ag29 S22B Cu1B 141.20(6) . 2_756 ?
Cu3B S22B Cu1B 78.38(5) . 2_756 ?
Ag29 S22B Ag31 81.54(4) . . ?
Cu3B S22B Ag31 123.53(5) . . ?
Cu1B S22B Ag31 137.22(5) 2_756 . ?
Ag29 S22B Ag30 81.66(4) . . ?
Cu3B S22B Ag30 111.72(5) . . ?
Cu1B S22B Ag30 81.36(4) 2_756 . ?
Ag31 S22B Ag30 115.27(5) . . ?
Cu5B S23B Cu4B 69.33(6) 2_756 . ?
Cu5B S23B Ag34 76.24(6) 2_756 . ?
Cu4B S23B Ag34 125.90(8) . . ?
Cu5B S23B Cu1B 89.19(7) 2_756 2_756 ?
Cu4B S23B Cu1B 76.85(6) . 2_756 ?
Ag34 S23B Cu1B 143.51(7) . 2_756 ?
Cu5B S23B Ag32 106.88(6) 2_756 . ?
Cu4B S23B Ag32 71.88(5) . . ?
Ag34 S23B Ag32 80.16(5) . . ?
Cu1B S23B Ag32 136.33(7) 2_756 . ?
Cu5B S23B Ag33 127.07(7) 2_756 . ?
Cu4B S23B Ag33 154.74(9) . . ?
Ag34 S23B Ag33 79.09(5) . . ?
Cu1B S23B Ag33 83.84(5) 2_756 . ?
Ag32 S23B Ag33 113.99(7) . . ?
Cu2B S24B Cu3B 114.04(9) . . ?
Cu2B S24B Cu4B 99.03(7) . . ?
Cu3B S24B Cu4B 115.41(7) . . ?
Cu3B S25B Cu1B 110.50(8) . 2_756 ?
Cu3B S25B Ag41 110.91(9) . . ?
Cu1B S25B Ag41 111.73(8) 2_756 . ?
Ag41 S2C Ag41 180.0 . 2_756 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag3 O2A S1A O1A 85.9(4) . . . . ?
Ag3 O2A S1A O3A -45.3(4) . . . . ?
Ag3 O2A S1A C1A -154.7(2) . . . . ?
Ag2 O1A S1A O2A -78.6(4) . . . . ?
Ag2 O1A S1A O3A 52.4(4) . . . . ?
Ag2 O1A S1A C1A 159.5(3) . . . . ?
Ag1 O3A S1A O2A 72.1(4) . . . . ?
Ag1 O3A S1A O1A -64.4(3) . . . . ?
Ag1 O3A S1A C1A -173.3(2) . . . . ?
C4A C1A S1A O2A -74.9(5) . . . . ?
C2A C1A S1A O2A 45.8(5) . . . . ?
C3A C1A S1A O2A 165.8(3) . . . . ?
C4A C1A S1A O1A 55.0(5) . . . . ?
C2A C1A S1A O1A 175.7(4) . . . . ?
C3A C1A S1A O1A -64.3(4) . . . . ?
C4A C1A S1A O3A 169.5(5) . . . . ?
C2A C1A S1A O3A -69.8(5) . . . . ?
C3A C1A S1A O3A 50.2(4) . . . . ?
Ag5 O5A S2A O6A -65.1(3) . . . . ?
Ag5 O5A S2A O4A 67.0(3) . . . . ?
Ag5 O5A S2A C5A -177.20(17) . . . . ?
Ag6 O6A S2A O5A 48.5(3) . . . . ?
Ag6 O6A S2A O4A -82.5(3) . . . . ?
Ag6 O6A S2A C5A 160.4(2) . . . . ?
Ag4 O4A S2A O5A -35.6(3) . . . . ?
Ag4 O4A S2A O6A 94.7(3) . . . . ?
Ag4 O4A S2A C5A -149.7(2) . . . . ?
C6A C5A S2A O5A 59.8(5) . . . . ?
C8A C5A S2A O5A -61.0(4) . . . . ?
C7A C5A S2A O5A -174.8(3) . . . . ?
C6A C5A S2A O6A -57.3(5) . . . . ?
C8A C5A S2A O6A -178.1(4) . . . . ?
C7A C5A S2A O6A 68.0(3) . . . . ?
C6A C5A S2A O4A 180.0(4) . . . . ?
C8A C5A S2A O4A 59.2(4) . . . . ?
C7A C5A S2A O4A -54.7(4) . . . . ?
Ag8 O8A S3A O7A 63.0(3) . . . . ?
Ag8 O8A S3A O9A -72.8(3) . . . . ?
Ag8 O8A S3A C9A 177.74(19) . . . . ?
Ag7 O7A S3A O8A -42.9(3) . . . . ?
Ag7 O7A S3A O9A 89.7(3) . . . . ?
Ag7 O7A S3A C9A -157.68(19) . . . . ?
Ag9 O9A S3A O8A 44.8(3) . . . . ?
Ag9 O9A S3A O7A -90.2(3) . . . . ?
Ag9 O9A S3A C9A 155.90(18) . . . . ?
C11A C9A S3A O8A 57.2(4) . . . . ?
C12A C9A S3A O8A -57.2(4) . . . . ?
C10A C9A S3A O8A -173.1(3) . . . . ?
C11A C9A S3A O7A 179.2(4) . . . . ?
C12A C9A S3A O7A 64.8(4) . . . . ?
C10A C9A S3A O7A -51.0(4) . . . . ?
C11A C9A S3A O9A -58.0(4) . . . . ?
C12A C9A S3A O9A -172.5(3) . . . . ?
C10A C9A S3A O9A 71.7(3) . . . . ?
Ag12 O12A S4A O11A -105.0(4) . . . . ?
Ag12 O12A S4A O10A 31.4(4) . . . . ?
Ag12 O12A S4A C13A 140.2(2) . . . . ?
Ag11 O11A S4A O12A 68.5(4) . . . . ?
Ag11 O11A S4A O10A -68.8(3) . . . . ?
Ag11 O11A S4A C13A -173.6(2) . . . . ?
Ag10 O10A S4A O12A -68.5(4) . . . . ?
Ag10 O10A S4A O11A 73.7(3) . . . . ?
Ag10 O10A S4A C13A 178.54(19) . . . . ?
C16A C13A S4A O12A 89.7(4) . . . . ?
C15A C13A S4A O12A -167.6(3) . . . . ?
C14A C13A S4A O12A -41.0(4) . . . . ?
C16A C13A S4A O11A -40.0(4) . . . . ?
C15A C13A S4A O11A 62.6(4) . . . . ?
C14A C13A S4A O11A -170.8(3) . . . . ?
C16A C13A S4A O10A -152.8(4) . . . . ?
C15A C13A S4A O10A -50.2(4) . . . . ?
C14A C13A S4A O10A 76.5(4) . . . . ?
Ag13 O13A S5A O14A -65.5(3) . . . . ?
Ag13 O13A S5A O15A 67.0(3) . . . . ?
Ag13 O13A S5A C17A -177.29(19) . . . . ?
Ag14 O14A S5A O13A 43.4(3) . . . . ?
Ag14 O14A S5A O15A -87.0(3) . . . . ?
Ag14 O14A S5A C17A 155.8(2) . . . . ?
Ag15 O15A S5A O13A -43.1(4) . . . . ?
Ag15 O15A S5A O14A 86.0(3) . . . . ?
Ag15 O15A S5A C17A -158.0(2) . . . . ?
C18A C17A S5A O13A -175.8(4) . . . . ?
C20A C17A S5A O13A -60.4(4) . . . . ?
C19A C17A S5A O13A 56.0(4) . . . . ?
C18A C17A S5A O14A 68.2(4) . . . . ?
C20A C17A S5A O14A -176.4(3) . . . . ?
C19A C17A S5A O14A -60.0(4) . . . . ?
C18A C17A S5A O15A -55.9(4) . . . . ?
C20A C17A S5A O15A 59.5(4) . . . . ?
C19A C17A S5A O15A 175.9(4) . . . . ?
Ag18 O18A S6A O16A -87.6(3) . . . . ?
Ag18 O18A S6A O17A 45.7(3) . . . . ?
Ag18 O18A S6A C21A 160.2(2) . . . . ?
Ag16 O16A S6A O18A 92.3(3) . . . . ?
Ag16 O16A S6A O17A -42.1(3) . . . . ?
Ag16 O16A S6A C21A -154.1(2) . . . . ?
Ag17 O17A S6A O18A -64.8(3) . . . . ?
Ag17 O17A S6A O16A 70.4(3) . . . . ?
Ag17 O17A S6A C21A -179.2(2) . . . . ?
C22A C21A S6A O18A -175.9(4) . . . . ?
C24A C21A S6A O18A -56.7(4) . . . . ?
C23A C21A S6A O18A 58.3(4) . . . . ?
C22A C21A S6A O16A 62.3(4) . . . . ?
C24A C21A S6A O16A -178.5(4) . . . . ?
C23A C21A S6A O16A -63.5(4) . . . . ?
C22A C21A S6A O17A -55.0(4) . . . . ?
C24A C21A S6A O17A 64.2(4) . . . . ?
C23A C21A S6A O17A 179.2(4) . . . . ?
C31A C29A S14A Ag17 170.2(3) . . . . ?
C30A C29A S14A Ag17 -56.3(4) . . . . ?
C32A C29A S14A Ag17 58.7(4) . . . . ?
C31A C29A S14A Cu5A -11.6(5) . . . . ?
C30A C29A S14A Cu5A 121.9(3) . . . . ?
C32A C29A S14A Cu5A -123.0(3) . . . . ?
C31A C29A S14A Ag15 86.8(4) . . . . ?
C30A C29A S14A Ag15 -139.7(3) . . . . ?
C32A C29A S14A Ag15 -24.6(4) . . . . ?
C31A C29A S14A Ag6 -109.6(4) . . . . ?
C30A C29A S14A Ag6 23.9(4) . . . . ?
C32A C29A S14A Ag6 139.0(3) . . . . ?
C38A C37A S15A Ag5 62.0(4) . . . 2_665 ?
C39A C37A S15A Ag5 -55.6(5) . . . 2_665 ?
C40A C37A S15A Ag5 175.7(3) . . . 2_665 ?
C38A C37A S15A Ag20 -121.2(3) . . . . ?
C39A C37A S15A Ag20 121.2(4) . . . . ?
C40A C37A S15A Ag20 -7.5(4) . . . . ?
C38A C37A S15A Ag11 -21.4(4) . . . . ?
C39A C37A S15A Ag11 -138.9(4) . . . . ?
C40A C37A S15A Ag11 92.3(4) . . . . ?
C38A C37A S15A Ag7 142.1(3) . . . 2_665 ?
C39A C37A S15A Ag7 24.5(5) . . . 2_665 ?
C40A C37A S15A Ag7 -104.2(3) . . . 2_665 ?
C43A C41A S16A Ag13 177.3(3) . . . . ?
C42A C41A S16A Ag13 62.4(5) . . . . ?
C44A C41A S16A Ag13 -72.3(5) . . . . ?
C43A C41A S16A Ag20 -5.1(5) . . . . ?
C42A C41A S16A Ag20 -120.1(5) . . . . ?
C44A C41A S16A Ag20 105.2(5) . . . . ?
C43A C41A S16A Ag9 95.2(4) . . . 2_665 ?
C42A C41A S16A Ag9 -19.7(6) . . . 2_665 ?
C44A C41A S16A Ag9 -154.4(4) . . . 2_665 ?
C43A C41A S16A Ag12 -100.7(4) . . . . ?
C42A C41A S16A Ag12 144.3(4) . . . . ?
C44A C41A S16A Ag12 9.6(6) . . . . ?
C52A C49A S18A Ag10 -173.3(3) . . . 2_665 ?
C50A C49A S18A Ag10 -55.4(5) . . . 2_665 ?
C51A C49A S18A Ag10 66.9(4) . . . 2_665 ?
C52A C49A S18A Ag21 7.7(5) . . . . ?
C50A C49A S18A Ag21 125.6(4) . . . . ?
C51A C49A S18A Ag21 -112.1(4) . . . . ?
C52A C49A S18A Ag18 -89.1(4) . . . . ?
C50A C49A S18A Ag18 28.7(4) . . . . ?
C51A C49A S18A Ag18 151.0(4) . . . . ?
C52A C49A S18A Ag2 101.5(4) . . . 2_665 ?
C50A C49A S18A Ag2 -140.6(4) . . . 2_665 ?
C51A C49A S18A Ag2 -18.3(5) . . . 2_665 ?
S9A Cu2A S23A Cu1A 39.81(8) . . . . ?
S7A Cu2A S23A Cu1A -165.42(10) . . . . ?
S22A Cu2A S23A Cu1A -22.71(12) . . . . ?
Ag8 Cu2A S23A Cu1A 83.32(8) . . . . ?
Ag19 Cu2A S23A Cu1A -112.62(8) . . . . ?
Ag3 Cu2A S23A Cu1A 136.68(8) . . . . ?
S9A Cu2A S23A Cu4A 170.21(6) . . . . ?
S7A Cu2A S23A Cu4A -35.02(5) . . . . ?
S22A Cu2A S23A Cu4A 107.70(7) . . . . ?
Ag8 Cu2A S23A Cu4A -146.28(3) . . . . ?
Ag19 Cu2A S23A Cu4A 17.79(5) . . . . ?
Cu1A Cu2A S23A Cu4A 130.40(11) . . . . ?
Ag3 Cu2A S23A Cu4A -92.92(4) . . . . ?
S25A Cu1A S23A Cu2A 126.17(9) . . . . ?
S8A Cu1A S23A Cu2A 177.67(10) . . . . ?
S9A Cu1A S23A Cu2A -35.83(8) . . . . ?
S10A Cu1A S23A Cu2A 25.3(3) 2_665 . . . ?
Cu6A Cu1A S23A Cu2A 17.34(10) . . . . ?
Ag5 Cu1A S23A Cu2A -139.21(8) . . . . ?
S25A Cu1A S23A Cu4A 2.69(10) . . . . ?
S8A Cu1A S23A Cu4A 54.19(6) . . . . ?
S9A Cu1A S23A Cu4A -159.30(8) . . . . ?
S10A Cu1A S23A Cu4A -98.2(2) 2_665 . . . ?
Cu6A Cu1A S23A Cu4A -106.14(6) . . . . ?
Cu2A Cu1A S23A Cu4A -123.48(12) . . . . ?
Ag5 Cu1A S23A Cu4A 97.31(6) . . . . ?
C63A C61A S24A Ag3 -49.0(5) . . . . ?
C64A C61A S24A Ag3 74.5(4) . . . . ?
C62A C61A S24A Ag3 -161.2(4) . . . . ?
C63A C61A S24A Ag7 -167.4(4) . . . . ?
C64A C61A S24A Ag7 -43.9(4) . . . . ?
C62A C61A S24A Ag7 80.4(5) . . . . ?
C63A C61A S24A Ag4 73.6(4) . . . . ?
C64A C61A S24A Ag4 -162.8(3) . . . . ?
C62A C61A S24A Ag4 -38.5(5) . . . . ?
Ag23 O1B S1B O3B 52.7(4) . . . . ?
Ag23 O1B S1B O2B -79.7(3) . . . . ?
Ag23 O1B S1B C17B 162.8(3) . . . . ?
Ag25 O3B S1B O1B -68.9(3) . . . . ?
Ag25 O3B S1B O2B 61.8(3) . . . . ?
Ag25 O3B S1B C17B 179.3(3) . . . . ?
Ag24 O2B S1B O1B 97.9(3) . . . . ?
Ag24 O2B S1B O3B -32.1(4) . . . . ?
Ag24 O2B S1B C17B -146.4(3) . . . . ?
C18B C17B S1B O1B 170.4(5) . . . . ?
C20B C17B S1B O1B -68.1(5) . . . . ?
C19B C17B S1B O1B 56.4(5) . . . . ?
C18B C17B S1B O3B -73.2(5) . . . . ?
C20B C17B S1B O3B 48.3(4) . . . . ?
C19B C17B S1B O3B 172.8(4) . . . . ?
C18B C17B S1B O2B 49.9(5) . . . . ?
C20B C17B S1B O2B 171.4(4) . . . . ?
C19B C17B S1B O2B -64.1(4) . . . . ?
Ag26 O4B S2B O5B -61.5(3) . . . . ?
Ag26 O4B S2B O6B 68.7(3) . . . . ?
Ag26 O4B S2B C5B -176.2(3) . . . . ?
Ag27 O5B S2B O4B 37.0(3) . . . . ?
Ag27 O5B S2B O6B -89.7(3) . . . . ?
Ag27 O5B S2B C5B 152.3(3) . . . . ?
Ag28 O6B S2B O4B -42.7(3) . . . . ?
Ag28 O6B S2B O5B 85.9(3) . . . . ?
Ag28 O6B S2B C5B -157.2(3) . . . . ?
C6B C5B S2B O4B -177.9(5) . . . . ?
C7B C5B S2B O4B 63.4(5) . . . . ?
C8B C5B S2B O4B -59.5(5) . . . . ?
C6B C5B S2B O5B 62.4(6) . . . . ?
C7B C5B S2B O5B -56.4(5) . . . . ?
C8B C5B S2B O5B -179.3(4) . . . . ?
C6B C5B S2B O6B -61.4(6) . . . . ?
C7B C5B S2B O6B 179.9(4) . . . . ?
C8B C5B S2B O6B 56.9(5) . . . . ?
Ag30 O8B S3B O7B 40.2(3) . . . . ?
Ag30 O8B S3B O9B -90.1(3) . . . . ?
Ag30 O8B S3B C9B 155.3(2) . . . . ?
Ag29 O7B S3B O8B -62.3(3) . . . . ?
Ag29 O7B S3B O9B 68.3(3) . . . . ?
Ag29 O7B S3B C9B -178.3(2) . . . . ?
Ag31 O9B S3B O8B 90.1(3) . . . . ?
Ag31 O9B S3B O7B -41.8(3) . . . . ?
Ag31 O9B S3B C9B -154.7(2) . . . . ?
C10B C9B S3B O8B 177.8(4) . . . . ?
C11B C9B S3B O8B -58.9(4) . . . . ?
C12B C9B S3B O8B 59.8(4) . . . . ?
C10B C9B S3B O7B -60.0(4) . . . . ?
C11B C9B S3B O7B 63.3(4) . . . . ?
C12B C9B S3B O7B -178.0(3) . . . . ?
C10B C9B S3B O9B 58.0(4) . . . . ?
C11B C9B S3B O9B -178.7(3) . . . . ?
C12B C9B S3B O9B -60.0(4) . . . . ?
Ag32 O10B S4B O11B -86.4(3) . . . . ?
Ag32 O10B S4B O12B 46.4(4) . . . . ?
Ag32 O10B S4B C13B 156.0(3) . . . . ?
Ag33 O11B S4B O10B 88.4(3) . . . . ?
Ag33 O11B S4B O12B -43.6(3) . . . . ?
Ag33 O11B S4B C13B -154.1(3) . . . . ?
Ag34 O12B S4B O10B -65.1(3) . . . . ?
Ag34 O12B S4B O11B 68.5(3) . . . . ?
Ag34 O12B S4B C13B -177.9(2) . . . . ?
C14B C13B S4B O10B 63.3(5) . . . . ?
C16B C13B S4B O10B -177.1(4) . . . . ?
C15B C13B S4B O10B -53.5(6) . . . . ?
C14B C13B S4B O11B -60.2(4) . . . . ?
C16B C13B S4B O11B 59.3(5) . . . . ?
C15B C13B S4B O11B -177.1(5) . . . . ?
C14B C13B S4B O12B -179.5(4) . . . . ?
C16B C13B S4B O12B -59.9(5) . . . . ?
C15B C13B S4B O12B 63.7(5) . . . . ?
Ag35 O13B S5B O15B 86.1(3) . . . . ?
Ag35 O13B S5B O14B -45.9(3) . . . . ?
Ag35 O13B S5B C1B -159.5(3) . . . . ?
Ag37 O15B S5B O13B -83.7(3) . . . . ?
Ag37 O15B S5B O14B 46.6(3) . . . . ?
Ag37 O15B S5B C1B 162.5(3) . . . . ?
Ag36 O14B S5B O13B 70.6(3) . . . . ?
Ag36 O14B S5B O15B -64.8(3) . . . . ?
Ag36 O14B S5B C1B -178.8(2) . . . . ?
C3B C1B S5B O13B 61.5(5) . . . . ?
C2B C1B S5B O13B 173.4(4) . . . . ?
C4B C1B S5B O13B -65.4(4) . . . . ?
C3B C1B S5B O15B -173.2(4) . . . . ?
C2B C1B S5B O15B -61.4(4) . . . . ?
C4B C1B S5B O15B 59.9(4) . . . . ?
C3B C1B S5B O14B -53.3(5) . . . . ?
C2B C1B S5B O14B 58.5(4) . . . . ?
C4B C1B S5B O14B 179.8(3) . . . . ?
Ag38 O16B S6B O18B 92.0(3) . . . . ?
Ag38 O16B S6B O17B -42.8(3) . . . . ?
Ag38 O16B S6B C21B -156.5(3) . . . . ?
Ag40 O18B S6B O16B -90.5(2) . . . . ?
Ag40 O18B S6B O17B 43.0(3) . . . . ?
Ag40 O18B S6B C21B 157.1(2) . . . . ?
Ag39 O17B S6B O16B 67.8(3) . . . . ?
Ag39 O17B S6B O18B -67.7(3) . . . . ?
Ag39 O17B S6B C21B -179.7(3) . . . . ?
C23B C21B S6B O16B -67.0(5) . . . . ?
C22B C21B S6B O16B 59.8(5) . . . . ?
C24B C21B S6B O16B 178.7(4) . . . . ?
C23B C21B S6B O18B 54.4(5) . . . . ?
C22B C21B S6B O18B -178.8(4) . . . . ?
C24B C21B S6B O18B -59.9(4) . . . . ?
C23B C21B S6B O17B 174.9(4) . . . . ?
C22B C21B S6B O17B -58.3(5) . . . . ?
C24B C21B S6B O17B 60.6(5) . . . . ?
C28B C25B S7B Ag39 59.4(4) . . . 2_756 ?
C27B C25B S7B Ag39 -65.6(5) . . . 2_756 ?
C26B C25B S7B Ag39 -179.6(4) . . . 2_756 ?
C28B C25B S7B Cu6B -119.1(3) . . . . ?
C27B C25B S7B Cu6B 116.0(4) . . . . ?
C26B C25B S7B Cu6B 2.0(5) . . . . ?
C28B C25B S7B Ag35 -21.3(4) . . . . ?
C27B C25B S7B Ag35 -146.3(4) . . . . ?
C26B C25B S7B Ag35 99.7(4) . . . . ?
C28B C25B S7B Ag23 141.1(3) . . . . ?
C27B C25B S7B Ag23 16.2(5) . . . . ?
C26B C25B S7B Ag23 -97.8(4) . . . . ?
C56B C57B S9B Ag34 -57.7(4) . . . 2_756 ?
C55B C57B S9B Ag34 60.5(5) . . . 2_756 ?
C54B C57B S9B Ag34 -175.9(3) . . . 2_756 ?
C56B C57B S9B Cu7B 123.0(4) . . . . ?
C55B C57B S9B Cu7B -118.8(4) . . . . ?
C54B C57B S9B Cu7B 4.8(4) . . . . ?
C56B C57B S9B Ag42 123.0(4) . . . . ?
C55B C57B S9B Ag42 -118.8(4) . . . . ?
C54B C57B S9B Ag42 4.8(4) . . . . ?
C56B C57B S9B Ag27 23.6(5) . . . . ?
C55B C57B S9B Ag27 141.8(4) . . . . ?
C54B C57B S9B Ag27 -94.5(3) . . . . ?
C56B C57B S9B Ag38 -137.9(3) . . . . ?
C55B C57B S9B Ag38 -19.6(5) . . . . ?
C54B C57B S9B Ag38 104.0(3) . . . . ?
C36B C33B S10B Ag29 57.6(4) . . . . ?
C34B C33B S10B Ag29 177.4(3) . . . . ?
C35B C33B S10B Ag29 -62.6(4) . . . . ?
C36B C33B S10B Cu7B -122.9(3) . . . . ?
C34B C33B S10B Cu7B -3.1(4) . . . . ?
C35B C33B S10B Cu7B 116.9(4) . . . . ?
C36B C33B S10B Ag42 -122.9(3) . . . . ?
C34B C33B S10B Ag42 -3.1(4) . . . . ?
C35B C33B S10B Ag42 116.9(4) . . . . ?
C36B C33B S10B Ag40 138.0(3) . . . . ?
C34B C33B S10B Ag40 -102.3(4) . . . . ?
C35B C33B S10B Ag40 17.8(5) . . . . ?
C36B C33B S10B Ag28 -22.9(4) . . . . ?
C34B C33B S10B Ag28 96.8(4) . . . . ?
C35B C33B S10B Ag28 -143.1(3) . . . . ?
C44B C41B S12B Ag25 -176.6(3) . . . . ?
C43B C41B S12B Ag25 60.8(4) . . . . ?
C42B C41B S12B Ag25 -58.4(4) . . . . ?
C44B C41B S12B Cu8B 6.5(4) . . . . ?
C43B C41B S12B Cu8B -116.0(3) . . . . ?
C42B C41B S12B Cu8B 124.7(3) . . . . ?
C44B C41B S12B Ag43 6.5(4) . . . . ?
C43B C41B S12B Ag43 -116.0(3) . . . . ?
C42B C41B S12B Ag43 124.7(3) . . . . ?
C44B C41B S12B Ag32 -91.5(4) . . . . ?
C43B C41B S12B Ag32 145.9(3) . . . . ?
C42B C41B S12B Ag32 26.7(4) . . . . ?
C44B C41B S12B Ag31 102.1(3) . . . . ?
C43B C41B S12B Ag31 -20.5(4) . . . . ?
C42B C41B S12B Ag31 -139.7(3) . . . . ?
C32B C29B S15B Ag30 51.1(5) . . . . ?
C30B C29B S15B Ag30 172.8(4) . . . . ?
C31B C29B S15B Ag30 -77.4(5) . . . . ?
C32B C29B S15B Ag40 -70.6(5) . . . . ?
C30B C29B S15B Ag40 51.1(5) . . . . ?
C31B C29B S15B Ag40 160.9(4) . . . . ?
C32B C29B S15B Ag35 170.1(4) . . . 2_756 ?
C30B C29B S15B Ag35 -68.2(5) . . . 2_756 ?
C31B C29B S15B Ag35 41.6(5) . . . 2_756 ?
C46B C45B S21B Ag32 -176.6(4) . . . . ?
C47B C45B S21B Ag32 51.8(4) . . . . ?
C48B C45B S21B Ag32 -70.1(5) . . . . ?
C46B C45B S21B Ag23 -55.3(4) . . . . ?
C47B C45B S21B Ag23 173.1(3) . . . . ?
C48B C45B S21B Ag23 51.2(5) . . . . ?
C46B C45B S21B Ag38 61.4(4) . . . 2_756 ?
C47B C45B S21B Ag38 -70.2(4) . . . 2_756 ?
C48B C45B S21B Ag38 167.9(4) . . . 2_756 ?
S24B Cu3B S25B Cu1B 16.53(14) . . . 2_756 ?
S22B Cu3B S25B Cu1B -43.18(8) . . . 2_756 ?
S20B Cu3B S25B Cu1B 166.34(10) . . . 2_756 ?
Ag29 Cu3B S25B Cu1B -87.26(9) . . . 2_756 ?
Ag41 Cu3B S25B Cu1B 124.46(13) . . . 2_756 ?
S24B Cu3B S25B Ag41 -107.93(10) . . . . ?
S22B Cu3B S25B Ag41 -167.64(8) . . . . ?
S20B Cu3B S25B Ag41 41.88(7) . . . . ?
Ag29 Cu3B S25B Ag41 148.27(6) . . . . ?

_refine_diff_density_max         3.743
_refine_diff_density_min         -1.896
_refine_diff_density_rms         0.127



