# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_xtal
_database_code_depnum_ccdc_archive 'CCDC 1854181'
_audit_update_record             
;
2018-10-12 deposited with the CCDC.
2018-10-17 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        'ytterbium magnesium antimonide'
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Mg Sb11 Yb13.82'

_chemical_formula_weight         3754.97

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      tetragonal
_space_group_IT_number           142
_space_group_name_H-M_alt        'I 41/a c d'
_space_group_name_Hall           '-I 4bd 2c'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-y+1/4, x+3/4, z+1/4'
'y+1/4, -x+1/4, z+3/4'
'-x+1/2, y, -z'
'x, -y, -z+1/2'
'y+1/4, x+3/4, -z+3/4'
'-y+1/4, -x+1/4, -z+1/4'
'x+1/2, y+1/2, z+1/2'
'-x+1, -y+1/2, z+1'
'-y+3/4, x+5/4, z+3/4'
'y+3/4, -x+3/4, z+5/4'
'-x+1, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1'
'y+3/4, x+5/4, -z+5/4'
'-y+3/4, -x+3/4, -z+3/4'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'y-1/4, -x-3/4, -z-1/4'
'-y-1/4, x-1/4, -z-3/4'
'x-1/2, -y, z'
'-x, y, z-1/2'
'-y-1/4, -x-3/4, z-3/4'
'y-1/4, x-1/4, z-1/4'
'-x+1/2, -y+1/2, -z+1/2'
'x, y+1/2, -z'
'y+1/4, -x-1/4, -z+1/4'
'-y+1/4, x+1/4, -z-1/4'
'x, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z'
'-y+1/4, -x-1/4, z-1/4'
'y+1/4, x+1/4, z+1/4'

_cell_length_a                   16.5530(7)
_cell_length_b                   16.5530(7)
_cell_length_c                   22.1368(10)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     6065.5(6)
_cell_formula_units_Z            8
_cell_measurement_temperature    90
_cell_measurement_reflns_used    9910
_cell_measurement_theta_min      2.46
_cell_measurement_theta_max      32.42

_exptl_crystal_description       block
_exptl_crystal_colour            black
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    8.224
_exptl_crystal_F_000             12323
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.09
_exptl_absorpt_coefficient_mu    51.732
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.0122
_exptl_absorpt_correction_T_max  0.0541
_exptl_absorpt_process_details   'SADABS 2014/5(Krause et al., 2015)'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      90
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'sealed tube'
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            47989
_diffrn_reflns_av_unetI/netI     0.0147
_diffrn_reflns_av_R_equivalents  0.0431
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_theta_min         2.461
_diffrn_reflns_theta_max         31.506
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_point_group_measured_fraction_full 0.999
_reflns_number_total             2534
_reflns_number_gt                2507
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'APEX2. Ver. 2014.11-0.  (Bruker-AXS, 2014)'
_computing_cell_refinement       'SAINT. Ver. 8.34A. (Bruker-AXS, 2014)'
_computing_data_reduction        'SAINT. Ver. 8.34A. (Bruker-AXS, 2014)'
_computing_structure_solution    'SHELXS-2013/1 (Sheldrick, 2013)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0123P)²+239.0132P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    undef
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_extinction_coef       0.0000378(17)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_number_reflns         2534
_refine_ls_number_parameters     62
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0228
_refine_ls_R_factor_gt           0.0225
_refine_ls_wR_factor_ref         0.0521
_refine_ls_wR_factor_gt          0.0520
_refine_ls_goodness_of_fit_ref   1.336
_refine_ls_restrained_S_all      1.336
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Yb1 Yb 0.95768(2) 0.92656(2) 0.82840(2) 0.00984(7) Uani 0.9819 1 d . . P . .
Yb2 Yb 0.97699(2) 0.12386(2) 0.00522(2) 0.01177(7) Uani 1 1 d . . . . .
Yb3 Yb 0.35411(3) 0.0000 0.2500 0.00971(8) Uani 0.9468 2 d S T P . .
Yb4 Yb 0.17909(2) 0.40755(2) 0.84276(2) 0.01166(7) Uani 1 1 d . . . . .
Mg1 Mg 0.0000 0.2500 0.8750 0.0104(8) Uani 1 4 d S T P . .
Sb1 Sb 0.13600(3) 0.38600(3) 0.1250 0.00874(11) Uani 1 2 d S T P . .
Sb2 Sb 0.00496(3) 0.10754(3) 0.80715(2) 0.01100(9) Uani 1 1 d . . . . .
Sb3 Sb 0.86957(3) 0.97330(3) 0.95214(2) 0.01169(9) Uani 1 1 d . . . . .
Sb4 Sb 0.0000 0.2500 0.1250 0.00959(15) Uani 1 4 d S T P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Yb1 Sb2 3.1319(5) 1_665 ?
Yb1 Sb2 3.1521(6) 6_666 ?
Yb1 Sb3 3.1646(6) 16_666 ?
Yb1 Sb4 3.1775(3) 17_666 ?
Yb1 Sb1 3.1981(4) 26_656 ?
Yb1 Sb3 3.1982(5) . ?
Yb1 Yb4 3.5730(4) 10_564 ?
Yb1 Yb1 3.7592(6) 16_666 ?
Yb1 Yb3 3.7678(5) 2_665 ?
Yb1 Yb2 3.9283(4) 17_766 ?
Yb1 Yb2 3.9323(4) 24_656 ?
Yb1 Yb2 4.1063(4) 31_676 ?
Yb2 Sb2 3.1367(5) 19_666 ?
Yb2 Sb3 3.1510(5) 17_766 ?
Yb2 Sb1 3.2489(4) 10_554 ?
Yb2 Sb3 3.2792(6) 1_544 ?
Yb2 Sb4 3.3965(3) 1_655 ?
Yb2 Mg1 3.5797(3) 1_654 ?
Yb2 Sb2 3.7574(6) 28_656 ?
Yb2 Yb3 3.7733(3) 20_656 ?
Yb2 Yb4 3.7954(4) 19_666 ?
Yb2 Yb1 3.9283(4) 17_766 ?
Yb2 Yb1 3.9323(4) 32_544 ?
Yb2 Yb1 4.1061(4) 23_775 ?
Yb3 Sb3 3.1190(6) 27_466 ?
Yb3 Sb3 3.1190(6) 32_444 ?
Yb3 Sb2 3.1956(5) 5_556 ?
Yb3 Sb2 3.1956(5) 2_554 ?
Yb3 Sb1 3.3533(3) 25 ?
Yb3 Sb1 3.3533(3) 20_656 ?
Yb3 Yb4 3.6785(3) 23_665 ?
Yb3 Yb4 3.6785(3) 20_657 ?
Yb3 Yb1 3.7678(5) 2_664 ?
Yb3 Yb1 3.7678(5) 5_646 ?
Yb3 Yb2 3.7733(3) 32_545 ?
Yb3 Yb2 3.7733(3) 27_565 ?
Yb4 Sb2 3.1567(5) 10_454 ?
Yb4 Sb1 3.1632(5) 11_545 ?
Yb4 Sb3 3.2253(5) 10_564 ?
Yb4 Sb3 3.2290(6) 4_464 ?
Yb4 Sb2 3.4142(6) 28_557 ?
Yb4 Yb1 3.5731(4) 10_564 ?
Yb4 Yb3 3.6786(3) 27_566 ?
Yb4 Sb3 3.7203(6) 7_446 ?
Yb4 Yb2 3.7953(4) 28_546 ?
Yb4 Yb3 3.8668(5) 26_556 ?
Yb4 Mg1 4.0123(3) . ?
Yb4 Yb4 4.0821(6) 16_556 ?
Mg1 Sb2 2.7970(4) . ?
Mg1 Sb2 2.7970(5) 28_557 ?
Mg1 Sb2 2.7970(4) 19_567 ?
Mg1 Sb2 2.7970(4) 10_454 ?
Mg1 Yb2 3.5797(3) 10 ?
Mg1 Yb2 3.5797(3) 19_576 ?
Mg1 Yb2 3.5797(3) 28_546 ?
Mg1 Yb2 3.5797(3) 1_456 ?
Mg1 Yb4 4.0122(3) 10_454 ?
Mg1 Yb4 4.0122(3) 19_567 ?
Mg1 Yb4 4.0122(3) 28_557 ?
Sb1 Yb4 3.1631(5) 5_556 ?
Sb1 Yb4 3.1631(5) 12_453 ?
Sb1 Sb4 3.1838(6) . ?
Sb1 Yb1 3.1981(4) 32_444 ?
Sb1 Yb1 3.1981(4) 26_446 ?
Sb1 Yb2 3.2490(4) 10_554 ?
Sb1 Yb2 3.2490(4) 8_565 ?
Sb1 Yb3 3.3532(3) 25 ?
Sb1 Yb3 3.3532(3) 27_565 ?
Sb2 Yb1 3.1319(5) 1_445 ?
Sb2 Yb2 3.1368(5) 28_546 ?
Sb2 Yb1 3.1520(6) 6_466 ?
Sb2 Yb4 3.1567(5) 10_454 ?
Sb2 Yb3 3.1956(5) 2 ?
Sb2 Yb4 3.4142(6) 19_567 ?
Sb2 Yb2 3.7573(6) 19_576 ?
Sb3 Yb3 3.1190(6) 20_667 ?
Sb3 Yb2 3.1510(6) 17_766 ?
Sb3 Yb1 3.1645(5) 16_666 ?
Sb3 Yb4 3.2251(5) 10_564 ?
Sb3 Yb4 3.2291(6) 3_655 ?
Sb3 Yb2 3.2793(6) 1_566 ?
Sb3 Yb4 3.7203(6) 7_556 ?
Sb4 Yb1 3.1775(3) 23_675 ?
Sb4 Yb1 3.1775(3) 26_446 ?
Sb4 Yb1 3.1775(3) 32_444 ?
Sb4 Yb1 3.1775(3) 17_666 ?
Sb4 Sb1 3.1837(6) 10_454 ?
Sb4 Yb2 3.3965(3) 1_455 ?
Sb4 Yb2 3.3965(3) 8_565 ?
Sb4 Yb2 3.3965(3) 10_554 ?
Sb4 Yb2 3.3965(3) 15_434 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Sb2 Yb1 Sb2 88.068(14) 1_665 6_666 ?
Sb2 Yb1 Sb3 115.803(15) 1_665 16_666 ?
Sb2 Yb1 Sb3 89.337(14) 6_666 16_666 ?
Sb2 Yb1 Sb4 150.867(13) 1_665 17_666 ?
Sb2 Yb1 Sb4 95.138(11) 6_666 17_666 ?
Sb3 Yb1 Sb4 93.217(11) 16_666 17_666 ?
Sb2 Yb1 Sb1 91.067(14) 1_665 26_656 ?
Sb2 Yb1 Sb1 92.309(11) 6_666 26_656 ?
Sb3 Yb1 Sb1 153.124(16) 16_666 26_656 ?
Sb4 Yb1 Sb1 59.915(11) 17_666 26_656 ?
Sb2 Yb1 Sb3 90.644(14) 1_665 . ?
Sb2 Yb1 Sb3 166.381(16) 6_666 . ?
Sb3 Yb1 Sb3 79.026(16) 16_666 . ?
Sb4 Yb1 Sb3 92.579(11) 17_666 . ?
Sb1 Yb1 Sb3 101.272(12) 26_656 . ?
Sb2 Yb1 Yb4 55.705(11) 1_665 10_564 ?
Sb2 Yb1 Yb4 112.311(12) 6_666 10_564 ?
Sb3 Yb1 Yb4 66.713(11) 16_666 10_564 ?
Sb4 Yb1 Yb4 144.856(10) 17_666 10_564 ?
Sb1 Yb1 Yb4 135.845(12) 26_656 10_564 ?
Sb3 Yb1 Yb4 56.563(10) . 10_564 ?
Sb2 Yb1 Yb1 142.710(12) 1_665 16_666 ?
Sb2 Yb1 Yb1 124.288(14) 6_666 16_666 ?
Sb3 Yb1 Yb1 54.202(11) 16_666 16_666 ?
Sb4 Yb1 Yb1 53.734(5) 17_666 16_666 ?
Sb1 Yb1 Yb1 104.150(11) 26_656 16_666 ?
Sb3 Yb1 Yb1 53.372(11) . 16_666 ?
Yb4 Yb1 Yb1 91.774(7) 10_564 16_666 ?
Sb2 Yb1 Yb3 54.237(9) 1_665 2_665 ?
Sb2 Yb1 Yb3 54.124(10) 6_666 2_665 ?
Sb3 Yb1 Yb3 139.657(13) 16_666 2_665 ?
Sb4 Yb1 Yb3 105.307(8) 17_666 2_665 ?
Sb1 Yb1 Yb3 56.847(9) 26_656 2_665 ?
Sb3 Yb1 Yb3 133.913(12) . 2_665 ?
Yb4 Yb1 Yb3 108.476(9) 10_564 2_665 ?
Yb1 Yb1 Yb3 158.793(6) 16_666 2_665 ?
Sb2 Yb1 Yb2 105.978(12) 1_665 17_766 ?
Sb2 Yb1 Yb2 141.829(13) 6_666 17_766 ?
Sb3 Yb1 Yb2 114.184(12) 16_666 17_766 ?
Sb4 Yb1 Yb2 55.911(6) 17_666 17_766 ?
Sb1 Yb1 Yb2 53.051(7) 26_656 17_766 ?
Sb3 Yb1 Yb2 51.240(10) . 17_766 ?
Yb4 Yb1 Yb2 104.733(10) 10_564 17_766 ?
Yb1 Yb1 Yb2 61.483(9) 16_666 17_766 ?
Yb3 Yb1 Yb2 105.831(9) 2_665 17_766 ?
Sb2 Yb1 Yb2 146.087(13) 1_665 24_656 ?
Sb2 Yb1 Yb2 62.931(11) 6_666 24_656 ?
Sb3 Yb1 Yb2 51.335(10) 16_666 24_656 ?
Sb4 Yb1 Yb2 55.863(6) 17_666 24_656 ?
Sb1 Yb1 Yb2 106.391(12) 26_656 24_656 ?
Sb3 Yb1 Yb2 113.275(13) . 24_656 ?
Yb4 Yb1 Yb2 117.305(10) 10_564 24_656 ?
Yb1 Yb1 Yb2 61.376(9) 16_666 24_656 ?
Yb3 Yb1 Yb2 111.903(9) 2_665 24_656 ?
Yb2 Yb1 Yb2 107.754(10) 17_766 24_656 ?
Sb2 Yb1 Yb2 111.292(12) 1_665 31_676 ?
Sb2 Yb1 Yb2 49.075(10) 6_666 31_676 ?
Sb3 Yb1 Yb2 114.156(12) 16_666 31_676 ?
Sb4 Yb1 Yb2 53.773(6) 17_666 31_676 ?
Sb1 Yb1 Yb2 50.987(7) 26_656 31_676 ?
Sb3 Yb1 Yb2 142.877(13) . 31_676 ?
Yb4 Yb1 Yb2 160.235(11) 10_564 31_676 ?
Yb1 Yb1 Yb2 104.599(7) 16_666 31_676 ?
Yb3 Yb1 Yb2 57.073(6) 2_665 31_676 ?
Yb2 Yb1 Yb2 92.949(9) 17_766 31_676 ?
Yb2 Yb1 Yb2 63.709(9) 24_656 31_676 ?
Sb2 Yb2 Sb3 165.090(16) 19_666 17_766 ?
Sb2 Yb2 Sb1 91.633(11) 19_666 10_554 ?
Sb3 Yb2 Sb1 101.181(12) 17_766 10_554 ?
Sb2 Yb2 Sb3 89.228(14) 19_666 1_544 ?
Sb3 Yb2 Sb3 99.006(14) 17_766 1_544 ?
Sb1 Yb2 Sb3 86.681(14) 10_554 1_544 ?
Sb2 Yb2 Sb4 91.213(12) 19_666 1_655 ?
Sb3 Yb2 Sb4 89.398(11) 17_766 1_655 ?
Sb1 Yb2 Sb4 57.200(11) 10_554 1_655 ?
Sb3 Yb2 Sb4 143.879(13) 1_544 1_655 ?
Sb2 Yb2 Mg1 48.671(9) 19_666 1_654 ?
Sb3 Yb2 Mg1 116.946(12) 17_766 1_654 ?
Sb1 Yb2 Mg1 138.397(10) 10_554 1_654 ?
Sb3 Yb2 Mg1 102.267(11) 1_544 1_654 ?
Sb4 Yb2 Mg1 104.959(8) 1_655 1_654 ?
Sb2 Yb2 Sb2 85.893(14) 19_666 28_656 ?
Sb3 Yb2 Sb2 79.470(13) 17_766 28_656 ?
Sb1 Yb2 Sb2 138.465(15) 10_554 28_656 ?
Sb3 Yb2 Sb2 134.632(14) 1_544 28_656 ?
Sb4 Yb2 Sb2 81.375(10) 1_655 28_656 ?
Mg1 Yb2 Sb2 44.736(8) 1_654 28_656 ?
Sb2 Yb2 Yb3 54.146(11) 19_666 20_656 ?
Sb3 Yb2 Yb3 140.142(14) 17_766 20_656 ?
Sb1 Yb2 Yb3 56.455(8) 10_554 20_656 ?
Sb3 Yb2 Yb3 51.921(11) 1_544 20_656 ?
Sb4 Yb2 Yb3 100.885(8) 1_655 20_656 ?
Mg1 Yb2 Yb3 97.576(8) 1_654 20_656 ?
Sb2 Yb2 Yb3 139.877(12) 28_656 20_656 ?
Sb2 Yb2 Yb4 113.109(13) 19_666 19_666 ?
Sb3 Yb2 Yb4 54.449(11) 17_766 19_666 ?
Sb1 Yb2 Yb4 155.246(10) 10_554 19_666 ?
Sb3 Yb2 Yb4 92.680(12) 1_544 19_666 ?
Sb4 Yb2 Yb4 119.984(9) 1_655 19_666 ?
Mg1 Yb2 Yb4 65.840(7) 1_654 19_666 ?
Sb2 Yb2 Yb4 49.407(9) 28_656 19_666 ?
Yb3 Yb2 Yb4 138.301(10) 20_656 19_666 ?
Sb2 Yb2 Yb1 136.226(13) 19_666 17_766 ?
Sb3 Yb2 Yb1 52.323(10) 17_766 17_766 ?
Sb1 Yb2 Yb1 51.874(8) 10_554 17_766 ?
Sb3 Yb2 Yb1 108.891(12) 1_544 17_766 ?
Sb4 Yb2 Yb1 50.784(6) 1_655 17_766 ?
Mg1 Yb2 Yb1 148.171(10) 1_654 17_766 ?
Sb2 Yb2 Yb1 105.458(11) 28_656 17_766 ?
Yb3 Yb2 Yb1 106.525(8) 20_656 17_766 ?
Yb4 Yb2 Yb1 105.661(10) 19_666 17_766 ?
Sb2 Yb2 Yb1 119.026(12) 19_666 32_544 ?
Sb3 Yb2 Yb1 51.646(10) 17_766 32_544 ?
Sb1 Yb2 Yb1 99.504(12) 10_554 32_544 ?
Sb3 Yb2 Yb1 150.611(13) 1_544 32_544 ?
Sb4 Yb2 Yb1 50.745(6) 1_655 32_544 ?
Mg1 Yb2 Yb1 92.093(8) 1_654 32_544 ?
Sb2 Yb2 Yb1 48.331(9) 28_656 32_544 ?
Yb3 Yb2 Yb1 151.610(10) 20_656 32_544 ?
Yb4 Yb2 Yb1 69.838(8) 19_666 32_544 ?
Yb1 Yb2 Yb1 57.140(9) 17_766 32_544 ?
Sb2 Yb2 Yb1 49.398(11) 19_666 23_775 ?
Sb3 Yb2 Yb1 136.667(13) 17_766 23_775 ?
Sb1 Yb2 Yb1 49.894(7) 10_554 23_775 ?
Sb3 Yb2 Yb1 108.776(12) 1_544 23_775 ?
Sb4 Yb2 Yb1 48.998(6) 1_655 23_775 ?
Mg1 Yb2 Yb1 89.280(8) 1_654 23_775 ?
Sb2 Yb2 Yb1 101.768(10) 28_656 23_775 ?
Yb3 Yb2 Yb1 56.944(8) 20_656 23_775 ?
Yb4 Yb2 Yb1 150.424(10) 19_666 23_775 ?
Yb1 Yb2 Yb1 86.834(9) 17_766 23_775 ?
Yb1 Yb2 Yb1 96.768(9) 32_544 23_775 ?
Sb3 Yb3 Sb3 92.07(2) 27_466 32_444 ?
Sb3 Yb3 Sb2 174.141(13) 27_466 5_556 ?
Sb3 Yb3 Sb2 91.079(12) 32_444 5_556 ?
Sb3 Yb3 Sb2 91.079(12) 27_466 2_554 ?
Sb3 Yb3 Sb2 174.141(13) 32_444 2_554 ?
Sb2 Yb3 Sb2 86.223(19) 5_556 2_554 ?
Sb3 Yb3 Sb1 96.355(13) 27_466 25 ?
Sb3 Yb3 Sb1 87.542(10) 32_444 25 ?
Sb2 Yb3 Sb1 88.715(14) 5_556 25 ?
Sb2 Yb3 Sb1 87.200(10) 2_554 25 ?
Sb3 Yb3 Sb1 87.541(10) 27_466 20_656 ?
Sb3 Yb3 Sb1 96.355(13) 32_444 20_656 ?
Sb2 Yb3 Sb1 87.200(10) 5_556 20_656 ?
Sb2 Yb3 Sb1 88.715(14) 2_554 20_656 ?
Sb1 Yb3 Sb1 174.40(2) 25 20_656 ?
Sb3 Yb3 Yb4 119.178(13) 27_466 23_665 ?
Sb3 Yb3 Yb4 55.922(10) 32_444 23_665 ?
Sb2 Yb3 Yb4 59.062(10) 5_556 23_665 ?
Sb2 Yb3 Yb4 126.205(13) 2_554 23_665 ?
Sb1 Yb3 Yb4 127.145(8) 25 23_665 ?
Sb1 Yb3 Yb4 53.222(8) 20_656 23_665 ?
Sb3 Yb3 Yb4 55.922(10) 27_466 20_657 ?
Sb3 Yb3 Yb4 119.178(13) 32_444 20_657 ?
Sb2 Yb3 Yb4 126.205(13) 5_556 20_657 ?
Sb2 Yb3 Yb4 59.062(10) 2_554 20_657 ?
Sb1 Yb3 Yb4 53.222(8) 25 20_657 ?
Sb1 Yb3 Yb4 127.145(8) 20_656 20_657 ?
Yb4 Yb3 Yb4 173.988(16) 23_665 20_657 ?
Sb3 Yb3 Yb1 128.486(10) 27_466 2_664 ?
Sb3 Yb3 Yb1 121.719(10) 32_444 2_664 ?
Sb2 Yb3 Yb1 53.057(11) 5_556 2_664 ?
Sb2 Yb3 Yb1 52.680(11) 2_554 2_664 ?
Sb1 Yb3 Yb1 52.984(9) 25 2_664 ?
Sb1 Yb3 Yb1 121.419(14) 20_656 2_664 ?
Yb4 Yb3 Yb1 112.103(10) 23_665 2_664 ?
Yb4 Yb3 Yb1 73.169(8) 20_657 2_664 ?
Sb3 Yb3 Yb1 121.719(10) 27_466 5_646 ?
Sb3 Yb3 Yb1 128.486(10) 32_444 5_646 ?
Sb2 Yb3 Yb1 52.680(11) 5_556 5_646 ?
Sb2 Yb3 Yb1 53.057(11) 2_554 5_646 ?
Sb1 Yb3 Yb1 121.419(14) 25 5_646 ?
Sb1 Yb3 Yb1 52.984(9) 20_656 5_646 ?
Yb4 Yb3 Yb1 73.169(8) 23_665 5_646 ?
Yb4 Yb3 Yb1 112.103(10) 20_657 5_646 ?
Yb1 Yb3 Yb1 68.441(12) 2_664 5_646 ?
Sb3 Yb3 Yb2 132.971(14) 27_466 32_545 ?
Sb3 Yb3 Yb2 55.852(10) 32_444 32_545 ?
Sb2 Yb3 Yb2 52.711(9) 5_556 32_545 ?
Sb2 Yb3 Yb2 118.643(13) 2_554 32_545 ?
Sb1 Yb3 Yb2 53.854(8) 25 32_545 ?
Sb1 Yb3 Yb2 125.548(7) 20_656 32_545 ?
Yb4 Yb3 Yb2 73.486(7) 23_665 32_545 ?
Yb4 Yb3 Yb2 107.058(6) 20_657 32_545 ?
Yb1 Yb3 Yb2 65.982(7) 2_664 32_545 ?
Yb1 Yb3 Yb2 105.292(10) 5_646 32_545 ?
Sb3 Yb3 Yb2 55.852(10) 27_466 27_565 ?
Sb3 Yb3 Yb2 132.971(14) 32_444 27_565 ?
Sb2 Yb3 Yb2 118.643(13) 5_556 27_565 ?
Sb2 Yb3 Yb2 52.711(9) 2_554 27_565 ?
Sb1 Yb3 Yb2 125.548(7) 25 27_565 ?
Sb1 Yb3 Yb2 53.854(8) 20_656 27_565 ?
Yb4 Yb3 Yb2 107.058(6) 23_665 27_565 ?
Yb4 Yb3 Yb2 73.486(7) 20_657 27_565 ?
Yb1 Yb3 Yb2 105.292(10) 2_664 27_565 ?
Yb1 Yb3 Yb2 65.982(7) 5_646 27_565 ?
Yb2 Yb3 Yb2 170.060(15) 32_545 27_565 ?
Sb2 Yb4 Sb1 168.902(15) 10_454 11_545 ?
Sb2 Yb4 Sb3 89.705(14) 10_454 10_564 ?
Sb1 Yb4 Sb3 98.115(13) 11_545 10_564 ?
Sb2 Yb4 Sb3 88.112(14) 10_454 4_464 ?
Sb1 Yb4 Sb3 89.000(11) 11_545 4_464 ?
Sb3 Yb4 Sb3 149.923(17) 10_564 4_464 ?
Sb2 Yb4 Sb2 86.107(17) 10_454 28_557 ?
Sb1 Yb4 Sb2 86.674(11) 11_545 28_557 ?
Sb3 Yb4 Sb2 85.459(14) 10_564 28_557 ?
Sb3 Yb4 Sb2 124.266(15) 4_464 28_557 ?
Sb2 Yb4 Yb1 55.050(10) 10_454 10_564 ?
Sb1 Yb4 Yb1 136.040(13) 11_545 10_564 ?
Sb3 Yb4 Yb1 55.845(11) 10_564 10_564 ?
Sb3 Yb4 Yb1 99.479(12) 4_464 10_564 ?
Sb2 Yb4 Yb1 120.914(12) 28_557 10_564 ?
Sb2 Yb4 Yb3 122.689(12) 10_454 27_566 ?
Sb1 Yb4 Yb3 58.114(5) 11_545 27_566 ?
Sb3 Yb4 Yb3 53.225(11) 10_564 27_566 ?
Sb3 Yb4 Yb3 146.366(13) 4_464 27_566 ?
Sb2 Yb4 Yb3 53.399(11) 28_557 27_566 ?
Yb1 Yb4 Yb3 109.066(10) 10_564 27_566 ?
Sb2 Yb4 Sb3 101.408(13) 10_454 7_446 ?
Sb1 Yb4 Sb3 88.641(11) 11_545 7_446 ?
Sb3 Yb4 Sb3 70.899(15) 10_564 7_446 ?
Sb3 Yb4 Sb3 80.155(14) 4_464 7_446 ?
Sb2 Yb4 Sb3 154.985(14) 28_557 7_446 ?
Yb1 Yb4 Sb3 51.381(9) 10_564 7_446 ?
Yb3 Yb4 Sb3 103.857(12) 27_566 7_446 ?
Sb2 Yb4 Yb2 64.670(11) 10_454 28_546 ?
Sb1 Yb4 Yb2 105.284(11) 11_545 28_546 ?
Sb3 Yb4 Yb2 148.534(13) 10_564 28_546 ?
Sb3 Yb4 Yb2 52.555(10) 4_464 28_546 ?
Sb2 Yb4 Yb2 75.361(11) 28_557 28_546 ?
Yb1 Yb4 Yb2 114.085(10) 10_564 28_546 ?
Yb3 Yb4 Yb2 124.968(11) 27_566 28_546 ?
Sb3 Yb4 Yb2 129.469(12) 7_446 28_546 ?
Sb2 Yb4 Yb3 128.450(13) 10_454 26_556 ?
Sb1 Yb4 Yb3 55.904(7) 11_545 26_556 ?
Sb3 Yb4 Yb3 110.104(12) 10_564 26_556 ?
Sb3 Yb4 Yb3 51.193(9) 4_464 26_556 ?
Sb2 Yb4 Yb3 140.396(12) 28_557 26_556 ?
Yb1 Yb4 Yb3 97.084(9) 10_564 26_556 ?
Yb3 Yb4 Yb3 106.508(8) 27_566 26_556 ?
Sb3 Yb4 Yb3 48.501(8) 7_446 26_556 ?
Yb2 Yb4 Yb3 100.441(8) 28_546 26_556 ?
Sb2 Yb4 Mg1 43.941(9) 10_454 . ?
Sb1 Yb4 Mg1 126.978(10) 11_545 . ?
Sb3 Yb4 Mg1 94.556(11) 10_564 . ?
Sb3 Yb4 Mg1 104.395(11) 4_464 . ?
Sb2 Yb4 Mg1 43.322(8) 28_557 . ?
Yb1 Yb4 Mg1 92.707(8) 10_564 . ?
Yb3 Yb4 Mg1 91.910(8) 27_566 . ?
Sb3 Yb4 Mg1 143.710(11) 7_446 . ?
Yb2 Yb4 Mg1 54.494(6) 28_546 . ?
Yb3 Yb4 Mg1 154.863(8) 26_556 . ?
Sb2 Yb4 Yb4 141.175(10) 10_454 16_556 ?
Sb1 Yb4 Yb4 49.815(9) 11_545 16_556 ?
Sb3 Yb4 Yb4 59.851(11) 10_564 16_556 ?
Sb3 Yb4 Yb4 106.204(14) 4_464 16_556 ?
Sb2 Yb4 Yb4 112.382(13) 28_557 16_556 ?
Yb1 Yb4 Yb4 86.658(7) 10_564 16_556 ?
Yb3 Yb4 Yb4 59.499(9) 27_566 16_556 ?
Sb3 Yb4 Yb4 48.560(9) 7_446 16_556 ?
Yb2 Yb4 Yb4 150.983(9) 28_546 16_556 ?
Yb3 Yb4 Yb4 55.051(8) 26_556 16_556 ?
Mg1 Yb4 Yb4 149.073(12) . 16_556 ?
Sb2 Mg1 Sb2 106.760(9) . 28_557 ?
Sb2 Mg1 Sb2 106.759(9) . 19_567 ?
Sb2 Mg1 Sb2 115.042(19) 28_557 19_567 ?
Sb2 Mg1 Sb2 115.042(19) . 10_454 ?
Sb2 Mg1 Sb2 106.760(9) 28_557 10_454 ?
Sb2 Mg1 Sb2 106.760(9) 19_567 10_454 ?
Sb2 Mg1 Yb2 157.082(11) . 10 ?
Sb2 Mg1 Yb2 57.368(11) 28_557 10 ?
Sb2 Mg1 Yb2 70.999(11) 19_567 10 ?
Sb2 Mg1 Yb2 86.777(11) 10_454 10 ?
Sb2 Mg1 Yb2 70.998(11) . 19_576 ?
Sb2 Mg1 Yb2 157.082(11) 28_557 19_576 ?
Sb2 Mg1 Yb2 86.776(11) 19_567 19_576 ?
Sb2 Mg1 Yb2 57.368(10) 10_454 19_576 ?
Yb2 Mg1 Yb2 130.424(6) 10 19_576 ?
Sb2 Mg1 Yb2 57.369(10) . 28_546 ?
Sb2 Mg1 Yb2 86.776(11) 28_557 28_546 ?
Sb2 Mg1 Yb2 157.082(11) 19_567 28_546 ?
Sb2 Mg1 Yb2 70.999(11) 10_454 28_546 ?
Yb2 Mg1 Yb2 130.424(6) 10 28_546 ?
Yb2 Mg1 Yb2 72.730(10) 19_576 28_546 ?
Sb2 Mg1 Yb2 86.776(11) . 1_456 ?
Sb2 Mg1 Yb2 70.999(11) 28_557 1_456 ?
Sb2 Mg1 Yb2 57.368(10) 19_567 1_456 ?
Sb2 Mg1 Yb2 157.082(11) 10_454 1_456 ?
Yb2 Mg1 Yb2 72.730(10) 10 1_456 ?
Yb2 Mg1 Yb2 130.424(6) 19_576 1_456 ?
Yb2 Mg1 Yb2 130.424(6) 28_546 1_456 ?
Sb2 Mg1 Yb4 51.550(10) . 10_454 ?
Sb2 Mg1 Yb4 137.519(10) 28_557 10_454 ?
Sb2 Mg1 Yb4 56.876(11) 19_567 10_454 ?
Sb2 Mg1 Yb4 115.517(10) 10_454 10_454 ?
Yb2 Mg1 Yb4 126.941(6) 10 10_454 ?
Yb2 Mg1 Yb4 59.665(6) 19_576 10_454 ?
Yb2 Mg1 Yb4 102.625(6) 28_546 10_454 ?
Yb2 Mg1 Yb4 71.669(7) 1_456 10_454 ?
Sb2 Mg1 Yb4 56.877(10) . 19_567 ?
Sb2 Mg1 Yb4 51.551(10) 28_557 19_567 ?
Sb2 Mg1 Yb4 115.517(10) 19_567 19_567 ?
Sb2 Mg1 Yb4 137.519(10) 10_454 19_567 ?
Yb2 Mg1 Yb4 102.625(7) 10 19_567 ?
Yb2 Mg1 Yb4 126.941(6) 19_576 19_567 ?
Yb2 Mg1 Yb4 71.669(7) 28_546 19_567 ?
Yb2 Mg1 Yb4 59.665(6) 1_456 19_567 ?
Yb4 Mg1 Yb4 91.813(1) 10_454 19_567 ?
Sb2 Mg1 Yb4 137.518(10) . 28_557 ?
Sb2 Mg1 Yb4 115.517(10) 28_557 28_557 ?
Sb2 Mg1 Yb4 51.551(10) 19_567 28_557 ?
Sb2 Mg1 Yb4 56.876(10) 10_454 28_557 ?
Yb2 Mg1 Yb4 59.665(6) 10 28_557 ?
Yb2 Mg1 Yb4 71.669(7) 19_576 28_557 ?
Yb2 Mg1 Yb4 126.941(6) 28_546 28_557 ?
Yb2 Mg1 Yb4 102.625(7) 1_456 28_557 ?
Yb4 Mg1 Yb4 91.813(1) 10_454 28_557 ?
Yb4 Mg1 Yb4 159.507(8) 19_567 28_557 ?
Sb2 Mg1 Yb4 115.517(10) . . ?
Sb2 Mg1 Yb4 56.877(11) 28_557 . ?
Sb2 Mg1 Yb4 137.519(10) 19_567 . ?
Sb2 Mg1 Yb4 51.550(10) 10_454 . ?
Yb2 Mg1 Yb4 71.670(6) 10 . ?
Yb2 Mg1 Yb4 102.624(6) 19_576 . ?
Yb2 Mg1 Yb4 59.664(6) 28_546 . ?
Yb2 Mg1 Yb4 126.942(6) 1_456 . ?
Yb4 Mg1 Yb4 159.505(8) 10_454 . ?
Yb4 Mg1 Yb4 91.813(1) 19_567 . ?
Yb4 Mg1 Yb4 91.814(1) 28_557 . ?
Yb4 Sb1 Yb4 80.371(17) 5_556 12_453 ?
Yb4 Sb1 Sb4 139.814(9) 5_556 . ?
Yb4 Sb1 Sb4 139.814(9) 12_453 . ?
Yb4 Sb1 Yb1 88.494(8) 5_556 32_444 ?
Yb4 Sb1 Yb1 142.815(11) 12_453 32_444 ?
Sb4 Sb1 Yb1 59.720(10) . 32_444 ?
Yb4 Sb1 Yb1 142.815(11) 5_556 26_446 ?
Yb4 Sb1 Yb1 88.494(8) 12_453 26_446 ?
Sb4 Sb1 Yb1 59.720(10) . 26_446 ?
Yb1 Sb1 Yb1 119.44(2) 32_444 26_446 ?
Yb4 Sb1 Yb2 138.321(12) 5_556 10_554 ?
Yb4 Sb1 Yb2 85.949(8) 12_453 10_554 ?
Sb4 Sb1 Yb2 63.731(11) . 10_554 ?
Yb1 Sb1 Yb2 79.119(11) 32_444 10_554 ?
Yb1 Sb1 Yb2 75.075(11) 26_446 10_554 ?
Yb4 Sb1 Yb2 85.949(8) 5_556 8_565 ?
Yb4 Sb1 Yb2 138.321(12) 12_453 8_565 ?
Sb4 Sb1 Yb2 63.731(11) . 8_565 ?
Yb1 Sb1 Yb2 75.075(11) 32_444 8_565 ?
Yb1 Sb1 Yb2 79.119(11) 26_446 8_565 ?
Yb2 Sb1 Yb2 127.46(2) 10_554 8_565 ?
Yb4 Sb1 Yb3 72.731(13) 5_556 25 ?
Yb4 Sb1 Yb3 68.664(10) 12_453 25 ?
Sb4 Sb1 Yb3 115.621(11) . 25 ?
Yb1 Sb1 Yb3 140.834(6) 32_444 25 ?
Yb1 Sb1 Yb3 70.168(9) 26_446 25 ?
Yb2 Sb1 Yb3 136.872(8) 10_554 25 ?
Yb2 Sb1 Yb3 69.692(6) 8_565 25 ?
Yb4 Sb1 Yb3 68.664(10) 5_556 27_565 ?
Yb4 Sb1 Yb3 72.731(13) 12_453 27_565 ?
Sb4 Sb1 Yb3 115.621(11) . 27_565 ?
Yb1 Sb1 Yb3 70.168(9) 32_444 27_565 ?
Yb1 Sb1 Yb3 140.834(6) 26_446 27_565 ?
Yb2 Sb1 Yb3 69.692(6) 10_554 27_565 ?
Yb2 Sb1 Yb3 136.872(8) 8_565 27_565 ?
Yb3 Sb1 Yb3 128.76(2) 25 27_565 ?
Mg1 Sb2 Yb1 135.929(17) . 1_445 ?
Mg1 Sb2 Yb2 73.961(12) . 28_546 ?
Yb1 Sb2 Yb2 145.979(17) 1_445 28_546 ?
Mg1 Sb2 Yb1 130.913(17) . 6_466 ?
Yb1 Sb2 Yb1 84.814(14) 1_445 6_466 ?
Yb2 Sb2 Yb1 81.526(13) 28_546 6_466 ?
Mg1 Sb2 Yb4 84.509(13) . 10_454 ?
Yb1 Sb2 Yb4 69.247(12) 1_445 10_454 ?
Yb2 Sb2 Yb4 140.983(17) 28_546 10_454 ?
Yb1 Sb2 Yb4 89.079(14) 6_466 10_454 ?
Mg1 Sb2 Yb3 134.722(17) . 2 ?
Yb1 Sb2 Yb3 73.082(12) 1_445 2 ?
Yb2 Sb2 Yb3 73.143(11) 28_546 2 ?
Yb1 Sb2 Yb3 72.817(12) 6_466 2 ?
Yb4 Sb2 Yb3 139.403(16) 10_454 2 ?
Mg1 Sb2 Yb4 79.802(12) . 19_567 ?
Yb1 Sb2 Yb4 85.269(13) 1_445 19_567 ?
Yb2 Sb2 Yb4 85.668(13) 28_546 19_567 ?
Yb1 Sb2 Yb4 140.325(16) 6_466 19_567 ?
Yb4 Sb2 Yb4 122.539(15) 10_454 19_567 ?
Yb3 Sb2 Yb4 67.538(11) 2 19_567 ?
Mg1 Sb2 Yb2 64.266(10) . 19_576 ?
Yb1 Sb2 Yb2 127.457(15) 1_445 19_576 ?
Yb2 Sb2 Yb2 75.413(12) 28_546 19_576 ?
Yb1 Sb2 Yb2 68.736(11) 6_466 19_576 ?
Yb4 Sb2 Yb2 65.923(11) 10_454 19_576 ?
Yb3 Sb2 Yb2 133.019(15) 2 19_576 ?
Yb4 Sb2 Yb2 142.675(15) 19_567 19_576 ?
Yb3 Sb3 Yb2 139.822(17) 20_667 17_766 ?
Yb3 Sb3 Yb1 125.217(17) 20_667 16_666 ?
Yb2 Sb3 Yb1 77.017(13) 17_766 16_666 ?
Yb3 Sb3 Yb1 138.438(16) 20_667 . ?
Yb2 Sb3 Yb1 76.439(13) 17_766 . ?
Yb1 Sb3 Yb1 72.428(13) 16_666 . ?
Yb3 Sb3 Yb4 70.853(12) 20_667 10_564 ?
Yb2 Sb3 Yb4 137.589(17) 17_766 10_564 ?
Yb1 Sb3 Yb4 110.997(16) 16_666 10_564 ?
Yb1 Sb3 Yb4 67.593(12) . 10_564 ?
Yb3 Sb3 Yb4 75.030(12) 20_667 3_655 ?
Yb2 Sb3 Yb4 72.995(12) 17_766 3_655 ?
Yb1 Sb3 Yb4 87.584(14) 16_666 3_655 ?
Yb1 Sb3 Yb4 146.531(17) . 3_655 ?
Yb4 Sb3 Yb4 145.857(17) 10_564 3_655 ?
Yb3 Sb3 Yb2 72.227(12) 20_667 1_566 ?
Yb2 Sb3 Yb2 80.992(14) 17_766 1_566 ?
Yb1 Sb3 Yb2 157.943(18) 16_666 1_566 ?
Yb1 Sb3 Yb2 104.088(15) . 1_566 ?
Yb4 Sb3 Yb2 86.539(14) 10_564 1_566 ?
Yb4 Sb3 Yb2 84.386(13) 3_655 1_566 ?
Yb3 Sb3 Yb4 68.205(11) 20_667 7_556 ?
Yb2 Sb3 Yb4 137.737(16) 17_766 7_556 ?
Yb1 Sb3 Yb4 61.907(11) 16_666 7_556 ?
Yb1 Sb3 Yb4 98.850(14) . 7_556 ?
Yb4 Sb3 Yb4 71.590(13) 10_564 7_556 ?
Yb4 Sb3 Yb4 94.694(14) 3_655 7_556 ?
Yb2 Sb3 Yb4 139.180(15) 1_566 7_556 ?
Yb1 Sb4 Yb1 72.533(10) 23_675 26_446 ?
Yb1 Sb4 Yb1 142.111(11) 23_675 32_444 ?
Yb1 Sb4 Yb1 120.728(10) 26_446 32_444 ?
Yb1 Sb4 Yb1 120.728(10) 23_675 17_666 ?
Yb1 Sb4 Yb1 142.111(11) 26_446 17_666 ?
Yb1 Sb4 Yb1 72.533(10) 32_444 17_666 ?
Yb1 Sb4 Sb1 60.364(5) 23_675 10_454 ?
Yb1 Sb4 Sb1 119.636(5) 26_446 10_454 ?
Yb1 Sb4 Sb1 119.636(5) 32_444 10_454 ?
Yb1 Sb4 Sb1 60.364(5) 17_666 10_454 ?
Yb1 Sb4 Sb1 119.636(5) 23_675 . ?
Yb1 Sb4 Sb1 60.364(5) 26_446 . ?
Yb1 Sb4 Sb1 60.364(5) 32_444 . ?
Yb1 Sb4 Sb1 119.636(5) 17_666 . ?
Sb1 Sb4 Sb1 180.000(11) 10_454 . ?
Yb1 Sb4 Yb2 77.228(7) 23_675 1_455 ?
Yb1 Sb4 Yb2 142.579(7) 26_446 1_455 ?
Yb1 Sb4 Yb2 73.391(7) 32_444 1_455 ?
Yb1 Sb4 Yb2 73.305(7) 17_666 1_455 ?
Sb1 Sb4 Yb2 59.069(5) 10_454 1_455 ?
Sb1 Sb4 Yb2 120.931(5) . 1_455 ?
Yb1 Sb4 Yb2 142.579(7) 23_675 8_565 ?
Yb1 Sb4 Yb2 77.228(7) 26_446 8_565 ?
Yb1 Sb4 Yb2 73.305(7) 32_444 8_565 ?
Yb1 Sb4 Yb2 73.391(7) 17_666 8_565 ?
Sb1 Sb4 Yb2 120.931(5) 10_454 8_565 ?
Sb1 Sb4 Yb2 59.069(5) . 8_565 ?
Yb2 Sb4 Yb2 138.362(10) 1_455 8_565 ?
Yb1 Sb4 Yb2 73.391(7) 23_675 10_554 ?
Yb1 Sb4 Yb2 73.305(7) 26_446 10_554 ?
Yb1 Sb4 Yb2 77.228(7) 32_444 10_554 ?
Yb1 Sb4 Yb2 142.579(7) 17_666 10_554 ?
Sb1 Sb4 Yb2 120.931(5) 10_454 10_554 ?
Sb1 Sb4 Yb2 59.069(5) . 10_554 ?
Yb2 Sb4 Yb2 77.353(11) 1_455 10_554 ?
Yb2 Sb4 Yb2 118.138(10) 8_565 10_554 ?
Yb1 Sb4 Yb2 73.305(7) 23_675 15_434 ?
Yb1 Sb4 Yb2 73.391(7) 26_446 15_434 ?
Yb1 Sb4 Yb2 142.579(7) 32_444 15_434 ?
Yb1 Sb4 Yb2 77.228(7) 17_666 15_434 ?
Sb1 Sb4 Yb2 59.069(5) 10_454 15_434 ?
Sb1 Sb4 Yb2 120.931(5) . 15_434 ?
Yb2 Sb4 Yb2 118.138(10) 1_455 15_434 ?
Yb2 Sb4 Yb2 77.353(11) 8_565 15_434 ?
Yb2 Sb4 Yb2 138.362(10) 10_554 15_434 ?

_refine_diff_density_max         2.102
_refine_diff_density_min         -1.446
_refine_diff_density_rms         0.348

