# Electronic Supplementary Material (ESI) for Chemical Communications.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_888
_database_code_depnum_ccdc_archive 'CCDC 1862671'
_audit_update_record             
;
2018-08-18 deposited with the CCDC.
2018-12-26 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'B7 Cs Li4 Na2 O14'
_chemical_formula_weight         506.32

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Triclinic
_symmetry_space_group_name_H-M   'P-1   '

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   6.9395(17)
_cell_length_b                   8.842(2)
_cell_length_c                   10.522(3)
_cell_angle_alpha                95.774(3)
_cell_angle_beta                 105.704(2)
_cell_angle_gamma                97.395(3)
_cell_volume                     610.1(3)
_cell_formula_units_Z            2
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    2006
_cell_measurement_theta_min      2.35
_cell_measurement_theta_max      27.53

_exptl_crystal_description       block
_exptl_crystal_colour            colourless
_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.08
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.756
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             472
_exptl_absorpt_coefficient_mu    3.187
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_correction_T_min  0.7206
_exptl_absorpt_correction_T_max  0.7846
_exptl_absorpt_process_details   face-indexed

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            3767
_diffrn_reflns_av_R_equivalents  0.0167
_diffrn_reflns_av_sigmaI/netI    0.0352
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_theta_min         2.35
_diffrn_reflns_theta_max         27.53
_reflns_number_total             2708
_reflns_number_gt                2444
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker SMART'
_computing_cell_refinement       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0355P)²+1.6760P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   none
_refine_ls_hydrogen_treatment    none
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         2708
_refine_ls_number_parameters     253
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0375
_refine_ls_R_factor_gt           0.0332
_refine_ls_wR_factor_ref         0.0795
_refine_ls_wR_factor_gt          0.0770
_refine_ls_goodness_of_fit_ref   1.026
_refine_ls_restrained_S_all      1.026
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Cs1 Cs 0.94410(4) 0.94848(3) 0.22224(3) 0.03029(10) Uani 1 1 d . . .
Na1 Na 0.8190(2) 0.41780(18) 0.18410(15) 0.0188(3) Uani 1 1 d . . .
Na2 Na 0.5674(2) 0.58718(18) 0.33475(15) 0.0203(3) Uani 1 1 d . . .
Li1 Li -0.3745(11) 0.1558(9) -0.0521(8) 0.0309(17) Uani 1 1 d . . .
Li2 Li 0.2340(12) 0.6089(10) 0.1257(7) 0.0317(18) Uani 1 1 d . . .
Li3 Li 0.4349(10) 0.1437(8) 0.5322(6) 0.0175(13) Uani 1 1 d . . .
Li4 Li 0.2567(10) 0.3245(7) 0.3142(6) 0.0166(12) Uani 1 1 d . . .
B1 B 0.4113(6) 0.4019(4) 0.0054(4) 0.0094(7) Uani 1 1 d . . .
B2 B 0.8310(6) 0.3894(5) 0.6169(4) 0.0106(7) Uani 1 1 d . . .
B3 B 1.0315(6) 0.2773(5) 0.4794(4) 0.0113(7) Uani 1 1 d . . .
B4 B 0.0835(6) 0.2849(5) 0.0383(4) 0.0119(7) Uani 1 1 d . . .
B5 B 0.4924(6) -0.0189(5) 0.2742(4) 0.0127(7) Uani 1 1 d . . .
B6 B 0.6531(6) 0.2436(5) 0.3884(4) 0.0112(7) Uani 1 1 d . . .
B7 B 0.4177(5) 0.2044(4) 0.1523(4) 0.0097(7) Uani 1 1 d . . .
O1 O 0.4580(4) 0.0458(3) 0.1566(2) 0.0129(5) Uani 1 1 d . . .
O2 O 0.4610(4) -0.1698(3) 0.2712(3) 0.0189(6) Uani 1 1 d . . .
O3 O -0.1161(4) 0.2642(3) 0.0041(3) 0.0157(5) Uani 1 1 d . . .
O4 O 1.0157(4) 0.3481(3) 0.6033(2) 0.0165(5) Uani 1 1 d . . .
O5 O 0.5672(4) 0.0809(3) 0.3948(2) 0.0133(5) Uani 1 1 d . . .
O6 O 0.4793(3) 0.2607(3) 0.0427(2) 0.0087(4) Uani 1 1 d . . .
O7 O 1.2080(4) 0.2460(3) 0.4689(2) 0.0149(5) Uani 1 1 d . . .
O8 O 0.4838(4) 0.4562(3) -0.1044(2) 0.0115(5) Uani 1 1 d . . .
O9 O 0.1957(3) 0.2038(3) 0.1313(2) 0.0126(5) Uani 1 1 d . . .
O10 O 0.8274(4) 0.4808(3) 0.7244(2) 0.0123(5) Uani 1 1 d . . .
O11 O 0.8581(3) 0.2478(3) 0.3728(2) 0.0136(5) Uani 1 1 d . . .
O12 O 0.1901(4) 0.3881(3) -0.0200(2) 0.0143(5) Uani 1 1 d . . .
O13 O 0.6577(3) 0.3358(3) 0.5136(2) 0.0135(5) Uani 1 1 d . . .
O14 O 0.5225(3) 0.3029(3) 0.2804(2) 0.0103(5) Uani 1 1 d . . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cs1 O9 3.064(2) 1_665 ?
Cs1 O11 3.154(3) 1_565 ?
Cs1 B4 3.208(4) 2_665 ?
Cs1 O12 3.345(3) 2_665 ?
Cs1 O4 3.347(3) 2_766 ?
Cs1 B5 3.367(4) 1_565 ?
Cs1 O7 3.438(3) 1_565 ?
Cs1 O3 3.442(3) 2_665 ?
Cs1 O1 3.493(3) 1_565 ?
Cs1 O2 3.569(3) 1_565 ?
Cs1 O6 3.599(2) 2_665 ?
Cs1 Li4 3.613(6) 1_665 ?
Na1 O3 2.395(3) 1_655 ?
Na1 O10 2.394(3) 2_766 ?
Na1 O8 2.489(3) 2_665 ?
Na1 O12 2.548(3) 2_665 ?
Na1 O6 2.558(3) . ?
Na1 O11 2.586(3) . ?
Na1 O14 2.663(3) . ?
Na1 O4 2.770(3) 2_766 ?
Na1 B1 2.920(4) . ?
Na1 B2 2.941(4) 2_766 ?
Na1 B1 2.940(4) 2_665 ?
Na1 B4 2.970(4) 1_655 ?
Na2 O8 2.337(3) 2_665 ?
Na2 O7 2.434(3) 2_766 ?
Na2 O2 2.458(3) 1_565 ?
Na2 O14 2.481(3) . ?
Na2 O10 2.614(3) 2_666 ?
Na2 O13 2.618(3) 2_666 ?
Na2 Li3 2.641(7) 2_666 ?
Na2 O4 2.757(3) 2_766 ?
Na2 Li2 2.770(7) . ?
Na2 Li4 2.906(7) . ?
Na2 B3 2.955(4) 2_766 ?
Na2 B2 2.972(4) 2_666 ?
Li1 O3 1.831(7) . ?
Li1 O6 1.868(7) 1_455 ?
Li1 O1 1.927(8) 2 ?
Li1 O2 2.239(9) 2 ?
Li1 B5 2.394(8) 2 ?
Li1 Li2 2.467(12) 2_565 ?
Li1 Na1 3.096(7) 1_455 ?
Li1 Li1 3.498(17) 2_455 ?
Li1 Cs1 3.818(7) 2_565 ?
Li1 Cs1 3.903(9) 1_445 ?
Li1 Cs1 4.030(7) 2_665 ?
Li2 O3 1.932(7) 2_565 ?
Li2 O10 1.957(7) 2_666 ?
Li2 O8 2.172(7) 2_665 ?
Li2 O12 2.291(9) . ?
Li2 O2 2.439(10) 1_565 ?
Li2 Li1 2.467(12) 2_565 ?
Li2 B1 2.725(8) . ?
Li2 B4 2.741(8) 2_565 ?
Li2 Na1 3.161(7) 2_665 ?
Li2 Li4 3.350(9) . ?
Li2 Na1 3.383(8) 1_455 ?
Li3 O7 1.913(7) 1_455 ?
Li3 O2 1.977(7) 2_656 ?
Li3 O5 1.982(7) . ?
Li3 O5 2.199(7) 2_656 ?
Li3 O13 2.207(7) . ?
Li3 B5 2.379(7) 2_656 ?
Li3 B6 2.555(7) . ?
Li3 Na2 2.641(7) 2_666 ?
Li3 Li3 2.882(13) 2_656 ?
Li3 Li4 3.009(9) . ?
Li3 Cs1 4.069(7) 1_445 ?
Li3 Cs1 4.220(6) 2_666 ?
Li4 O7 1.927(6) 1_455 ?
Li4 O10 1.934(7) 2_666 ?
Li4 O14 1.999(7) . ?
Li4 O9 2.012(7) . ?
Li4 B7 2.499(7) . ?
Li4 B3 2.662(7) 1_455 ?
Li4 B2 2.750(7) 2_666 ?
Li4 B4 2.791(7) . ?
Li4 Na1 3.226(6) 1_455 ?
B1 O6 1.444(4) . ?
B1 O12 1.472(4) . ?
B1 O8 1.477(4) . ?
B1 O8 1.510(4) 2_665 ?
B1 B1 2.026(7) 2_665 ?
B1 Na1 2.940(4) 2_665 ?
B1 Cs1 3.841(4) 2_665 ?
B2 O10 1.330(5) . ?
B2 O13 1.377(4) . ?
B2 O4 1.417(4) . ?
B2 Li4 2.750(7) 2_666 ?
B2 Na1 2.941(4) 2_766 ?
B2 Na2 2.972(4) 2_666 ?
B2 Cs1 3.875(4) 2_766 ?
B3 O7 1.321(4) . ?
B3 O11 1.380(4) . ?
B3 O4 1.426(5) . ?
B3 Li4 2.662(7) 1_655 ?
B3 Na2 2.955(4) 2_766 ?
B3 Cs1 3.636(4) 1_545 ?
B3 Cs1 3.864(4) 2_766 ?
B4 O3 1.316(4) . ?
B4 O12 1.393(4) . ?
B4 O9 1.397(5) . ?
B4 Li2 2.741(8) 2_565 ?
B4 Na1 2.970(4) 1_455 ?
B4 Cs1 3.208(4) 2_665 ?
B4 Cs1 3.868(4) 1_445 ?
B5 O2 1.319(5) . ?
B5 O1 1.391(4) . ?
B5 O5 1.400(5) . ?
B5 Li3 2.379(7) 2_656 ?
B5 Li1 2.394(8) 2 ?
B5 Cs1 3.367(4) 1_545 ?
B5 Cs1 3.663(4) 1_445 ?
B6 O14 1.439(4) . ?
B6 O13 1.468(5) . ?
B6 O11 1.472(4) . ?
B6 O5 1.500(5) . ?
B7 O6 1.445(4) . ?
B7 O1 1.468(4) . ?
B7 O14 1.474(4) . ?
B7 O9 1.495(4) . ?
O1 Li1 1.927(8) 2 ?
O1 Cs1 3.493(3) 1_545 ?
O2 Li3 1.977(7) 2_656 ?
O2 Li1 2.240(9) 2 ?
O2 Li2 2.439(10) 1_545 ?
O2 Na2 2.458(3) 1_545 ?
O2 Cs1 3.569(3) 1_545 ?
O2 Cs1 3.782(3) 1_445 ?
O3 Li2 1.932(7) 2_565 ?
O3 Na1 2.395(3) 1_455 ?
O3 Cs1 3.442(3) 2_665 ?
O3 Cs1 3.783(3) 1_445 ?
O4 Na2 2.757(3) 2_766 ?
O4 Na1 2.770(3) 2_766 ?
O4 Cs1 3.347(3) 2_766 ?
O5 Li3 2.199(7) 2_656 ?
O5 Cs1 3.800(3) 1_545 ?
O6 Li1 1.868(7) 1_655 ?
O6 Cs1 3.599(2) 2_665 ?
O7 Li3 1.913(7) 1_655 ?
O7 Li4 1.927(6) 1_655 ?
O7 Na2 2.434(3) 2_766 ?
O7 Cs1 3.438(3) 1_545 ?
O8 B1 1.510(4) 2_665 ?
O8 Li2 2.172(7) 2_665 ?
O8 Na2 2.337(3) 2_665 ?
O8 Na1 2.489(3) 2_665 ?
O9 Cs1 3.064(2) 1_445 ?
O9 Cs1 3.646(3) 2_665 ?
O10 Li4 1.934(7) 2_666 ?
O10 Li2 1.957(7) 2_666 ?
O10 Na1 2.394(3) 2_766 ?
O10 Na2 2.614(3) 2_666 ?
O11 Cs1 3.154(3) 1_545 ?
O12 Na1 2.548(3) 2_665 ?
O12 Cs1 3.345(3) 2_665 ?
O13 Na2 2.618(3) 2_666 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O9 Cs1 O11 78.12(7) 1_665 1_565 ?
O9 Cs1 B4 91.06(9) 1_665 2_665 ?
O11 Cs1 B4 153.93(8) 1_565 2_665 ?
O9 Cs1 O12 115.48(7) 1_665 2_665 ?
O11 Cs1 O12 154.31(6) 1_565 2_665 ?
B4 Cs1 O12 24.43(8) 2_665 2_665 ?
O9 Cs1 O4 142.60(6) 1_665 2_766 ?
O11 Cs1 O4 114.57(6) 1_565 2_766 ?
B4 Cs1 O4 88.42(9) 2_665 2_766 ?
O12 Cs1 O4 68.84(6) 2_665 2_766 ?
O9 Cs1 B5 123.32(8) 1_665 1_565 ?
O11 Cs1 B5 56.70(8) 1_565 1_565 ?
B4 Cs1 B5 114.18(10) 2_665 1_565 ?
O12 Cs1 B5 98.73(8) 2_665 1_565 ?
O4 Cs1 B5 90.45(8) 2_766 1_565 ?
O9 Cs1 O7 65.07(6) 1_665 1_565 ?
O11 Cs1 O7 41.81(6) 1_565 1_565 ?
B4 Cs1 O7 150.37(8) 2_665 1_565 ?
O12 Cs1 O7 162.83(6) 2_665 1_565 ?
O4 Cs1 O7 100.03(6) 2_766 1_565 ?
B5 Cs1 O7 94.26(8) 1_565 1_565 ?
O9 Cs1 O3 79.14(7) 1_665 2_665 ?
O11 Cs1 O3 156.78(6) 1_565 2_665 ?
B4 Cs1 O3 22.48(8) 2_665 2_665 ?
O12 Cs1 O3 40.50(6) 2_665 2_665 ?
O4 Cs1 O3 86.67(6) 2_766 2_665 ?
B5 Cs1 O3 136.54(8) 1_565 2_665 ?
O7 Cs1 O3 128.95(6) 1_565 2_665 ?
O9 Cs1 O1 105.21(6) 1_665 1_565 ?
O11 Cs1 O1 58.28(6) 1_565 1_565 ?
B4 Cs1 O1 103.18(8) 2_665 1_565 ?
O12 Cs1 O1 96.28(6) 2_665 1_565 ?
O4 Cs1 O1 111.30(6) 2_766 1_565 ?
B5 Cs1 O1 23.30(7) 1_565 1_565 ?
O7 Cs1 O1 100.06(6) 1_565 1_565 ?
O3 Cs1 O1 124.57(6) 2_665 1_565 ?
O9 Cs1 O2 143.84(6) 1_665 1_565 ?
O11 Cs1 O2 76.33(6) 1_565 1_565 ?
B4 Cs1 O2 100.93(8) 2_665 1_565 ?
O12 Cs1 O2 81.05(6) 2_665 1_565 ?
O4 Cs1 O2 72.39(6) 2_766 1_565 ?
B5 Cs1 O2 21.68(8) 1_565 1_565 ?
O7 Cs1 O2 108.70(6) 1_565 1_565 ?
O3 Cs1 O2 121.35(6) 2_665 1_565 ?
O1 Cs1 O2 38.95(6) 1_565 1_565 ?
O9 Cs1 O6 113.28(6) 1_665 2_665 ?
O11 Cs1 O6 115.31(6) 1_565 2_665 ?
B4 Cs1 O6 47.61(8) 2_665 2_665 ?
O12 Cs1 O6 40.18(5) 2_665 2_665 ?
O4 Cs1 O6 93.50(6) 2_766 2_665 ?
B5 Cs1 O6 66.82(8) 1_565 2_665 ?
O7 Cs1 O6 156.90(5) 1_565 2_665 ?
O3 Cs1 O6 70.09(6) 2_665 2_665 ?
O1 Cs1 O6 57.33(6) 1_565 2_665 ?
O2 Cs1 O6 57.84(6) 1_565 2_665 ?
O9 Cs1 Li4 33.83(11) 1_665 1_665 ?
O11 Cs1 Li4 52.15(11) 1_565 1_665 ?
B4 Cs1 Li4 124.08(12) 2_665 1_665 ?
O12 Cs1 Li4 147.98(11) 2_665 1_665 ?
O4 Cs1 Li4 126.73(11) 2_766 1_665 ?
B5 Cs1 Li4 108.03(12) 1_565 1_665 ?
O7 Cs1 Li4 31.59(11) 1_565 1_665 ?
O3 Cs1 Li4 108.21(11) 2_665 1_665 ?
O1 Cs1 Li4 101.36(11) 1_565 1_665 ?
O2 Cs1 Li4 128.46(11) 1_565 1_665 ?
O6 Cs1 Li4 139.77(11) 2_665 1_665 ?
O3 Na1 O10 91.16(10) 1_655 2_766 ?
O3 Na1 O8 111.44(10) 1_655 2_665 ?
O10 Na1 O8 132.17(11) 2_766 2_665 ?
O3 Na1 O12 79.91(10) 1_655 2_665 ?
O10 Na1 O12 86.81(9) 2_766 2_665 ?
O8 Na1 O12 58.57(8) 2_665 2_665 ?
O3 Na1 O6 72.76(9) 1_655 . ?
O10 Na1 O6 163.77(11) 2_766 . ?
O8 Na1 O6 58.95(8) 2_665 . ?
O12 Na1 O6 92.36(9) 2_665 . ?
O3 Na1 O11 104.79(10) 1_655 . ?
O10 Na1 O11 87.68(9) 2_766 . ?
O8 Na1 O11 123.08(9) 2_665 . ?
O12 Na1 O11 172.83(10) 2_665 . ?
O6 Na1 O11 94.21(9) . . ?
O3 Na1 O14 118.08(10) 1_655 . ?
O10 Na1 O14 135.59(10) 2_766 . ?
O8 Na1 O14 69.96(8) 2_665 . ?
O12 Na1 O14 128.38(9) 2_665 . ?
O6 Na1 O14 55.23(8) . . ?
O11 Na1 O14 54.43(8) . . ?
O3 Na1 O4 145.01(10) 1_655 2_766 ?
O10 Na1 O4 54.49(8) 2_766 2_766 ?
O8 Na1 O4 91.07(9) 2_665 2_766 ?
O12 Na1 O4 90.57(10) 2_665 2_766 ?
O6 Na1 O4 141.74(9) . 2_766 ?
O11 Na1 O4 82.50(9) . 2_766 ?
O14 Na1 O4 94.27(9) . 2_766 ?
O3 Na1 B1 86.00(10) 1_655 . ?
O10 Na1 B1 155.05(11) 2_766 . ?
O8 Na1 B1 31.15(9) 2_665 . ?
O12 Na1 B1 68.28(10) 2_665 . ?
O6 Na1 B1 29.64(9) . . ?
O11 Na1 B1 117.02(10) . . ?
O14 Na1 B1 65.68(9) . . ?
O4 Na1 B1 121.69(11) 2_766 . ?
O3 Na1 B2 117.56(11) 1_655 2_766 ?
O10 Na1 B2 26.40(10) 2_766 2_766 ?
O8 Na1 B2 115.89(11) 2_665 2_766 ?
O12 Na1 B2 91.99(10) 2_665 2_766 ?
O6 Na1 B2 169.40(11) . 2_766 ?
O11 Na1 B2 81.06(10) . 2_766 ?
O14 Na1 B2 114.90(10) . 2_766 ?
O4 Na1 B2 28.52(9) 2_766 2_766 ?
B1 Na1 B2 146.88(12) . 2_766 ?
O3 Na1 B1 90.21(11) 1_655 2_665 ?
O10 Na1 B1 114.91(11) 2_766 2_665 ?
O8 Na1 B1 30.13(9) 2_665 2_665 ?
O12 Na1 B1 30.04(9) 2_665 2_665 ?
O6 Na1 B1 68.46(10) . 2_665 ?
O11 Na1 B1 152.90(10) . 2_665 ?
O14 Na1 B1 98.65(10) . 2_665 ?
O4 Na1 B1 98.18(10) 2_766 2_665 ?
B1 Na1 B1 40.46(14) . 2_665 ?
B2 Na1 B1 112.17(12) 2_766 2_665 ?
O3 Na1 B4 25.66(10) 1_655 1_655 ?
O10 Na1 B4 65.71(10) 2_766 1_655 ?
O8 Na1 B4 130.92(11) 2_665 1_655 ?
O12 Na1 B4 82.46(10) 2_665 1_655 ?
O6 Na1 B4 98.10(10) . 1_655 ?
O11 Na1 B4 99.42(11) . 1_655 ?
O14 Na1 B4 135.13(11) . 1_655 ?
O4 Na1 B4 120.09(10) 2_766 1_655 ?
B1 Na1 B4 110.39(12) . 1_655 ?
B2 Na1 B4 92.05(11) 2_766 1_655 ?
B1 Na1 B4 103.45(11) 2_665 1_655 ?
O8 Na2 O7 139.43(11) 2_665 2_766 ?
O8 Na2 O2 79.26(10) 2_665 1_565 ?
O7 Na2 O2 83.33(10) 2_766 1_565 ?
O8 Na2 O14 75.66(9) 2_665 . ?
O7 Na2 O14 128.86(10) 2_766 . ?
O2 Na2 O14 147.78(10) 1_565 . ?
O8 Na2 O10 85.11(9) 2_665 2_666 ?
O7 Na2 O10 126.56(10) 2_766 2_666 ?
O2 Na2 O10 78.13(9) 1_565 2_666 ?
O14 Na2 O10 79.87(9) . 2_666 ?
O8 Na2 O13 134.20(10) 2_665 2_666 ?
O7 Na2 O13 73.15(9) 2_766 2_666 ?
O2 Na2 O13 73.91(9) 1_565 2_666 ?
O14 Na2 O13 110.55(10) . 2_666 ?
O10 Na2 O13 53.65(8) 2_666 2_666 ?
O8 Na2 Li3 123.82(15) 2_665 2_666 ?
O7 Na2 Li3 44.06(15) 2_766 2_666 ?
O2 Na2 Li3 45.45(15) 1_565 2_666 ?
O14 Na2 Li3 158.13(16) . 2_666 ?
O10 Na2 Li3 91.26(15) 2_666 2_666 ?
O13 Na2 Li3 49.62(15) 2_666 2_666 ?
O8 Na2 O4 94.74(9) 2_665 2_766 ?
O7 Na2 O4 54.16(8) 2_766 2_766 ?
O2 Na2 O4 103.10(10) 1_565 2_766 ?
O14 Na2 O4 98.86(9) . 2_766 ?
O10 Na2 O4 178.72(10) 2_666 2_766 ?
O13 Na2 O4 126.94(9) 2_666 2_766 ?
Li3 Na2 O4 89.88(16) 2_666 2_766 ?
O8 Na2 Li2 49.46(16) 2_665 . ?
O7 Na2 Li2 137.3(2) 2_766 . ?
O2 Na2 Li2 55.2(2) 1_565 . ?
O14 Na2 Li2 92.8(2) . . ?
O10 Na2 Li2 42.50(16) 2_666 . ?
O13 Na2 Li2 84.74(16) 2_666 . ?
Li3 Na2 Li2 94.0(2) 2_666 . ?
O4 Na2 Li2 137.97(17) 2_766 . ?
O8 Na2 Li4 90.35(15) 2_665 . ?
O7 Na2 Li4 130.01(15) 2_766 . ?
O2 Na2 Li4 118.64(15) 1_565 . ?
O14 Na2 Li4 42.65(14) . . ?
O10 Na2 Li4 40.60(14) 2_666 . ?
O13 Na2 Li4 71.70(14) 2_666 . ?
Li3 Na2 Li4 120.95(19) 2_666 . ?
O4 Na2 Li4 138.16(15) 2_766 . ?
Li2 Na2 Li4 72.3(2) . . ?
O8 Na2 B3 121.55(11) 2_665 2_766 ?
O7 Na2 B3 26.15(10) 2_766 2_766 ?
O2 Na2 B3 97.06(11) 1_565 2_766 ?
O14 Na2 B3 113.20(11) . 2_766 ?
O10 Na2 B3 151.90(11) 2_666 2_766 ?
O13 Na2 B3 98.30(11) 2_666 2_766 ?
Li3 Na2 B3 67.30(16) 2_666 2_766 ?
O4 Na2 B3 28.64(9) 2_766 2_766 ?
Li2 Na2 B3 150.4(2) . 2_766 ?
Li4 Na2 B3 136.75(15) . 2_766 ?
O8 Na2 B2 108.06(11) 2_665 2_666 ?
O7 Na2 B2 100.02(11) 2_766 2_666 ?
O2 Na2 B2 70.53(10) 1_565 2_666 ?
O14 Na2 B2 98.42(11) . 2_666 ?
O10 Na2 B2 26.56(9) 2_666 2_666 ?
O13 Na2 B2 27.59(9) 2_666 2_666 ?
Li3 Na2 B2 67.59(16) 2_666 2_666 ?
O4 Na2 B2 154.18(11) 2_766 2_666 ?
Li2 Na2 B2 59.69(16) . 2_666 ?
Li4 Na2 B2 55.77(15) . 2_666 ?
B3 Na2 B2 125.70(12) 2_766 2_666 ?
O3 Li1 O6 105.3(4) . 1_455 ?
O3 Li1 O1 126.0(4) . 2 ?
O6 Li1 O1 127.4(4) 1_455 2 ?
O3 Li1 O2 101.9(4) . 2 ?
O6 Li1 O2 114.8(4) 1_455 2 ?
O1 Li1 O2 68.4(3) 2 2 ?
O3 Li1 B5 118.1(4) . 2 ?
O6 Li1 B5 128.2(4) 1_455 2 ?
O1 Li1 B5 35.50(17) 2 2 ?
O2 Li1 B5 32.87(16) 2 2 ?
O3 Li1 Li2 50.8(3) . 2_565 ?
O6 Li1 Li2 93.6(4) 1_455 2_565 ?
O1 Li1 Li2 125.8(4) 2 2_565 ?
O2 Li1 Li2 62.2(3) 2 2_565 ?
B5 Li1 Li2 92.9(4) 2 2_565 ?
O3 Li1 Na1 50.58(19) . 1_455 ?
O6 Li1 Na1 55.6(2) 1_455 1_455 ?
O1 Li1 Na1 161.8(4) 2 1_455 ?
O2 Li1 Na1 128.8(3) 2 1_455 ?
B5 Li1 Na1 161.0(4) 2 1_455 ?
Li2 Li1 Na1 68.2(3) 2_565 1_455 ?
O3 Li1 Li1 134.1(5) . 2_455 ?
O6 Li1 Li1 80.3(3) 1_455 2_455 ?
O1 Li1 Li1 57.2(2) 2 2_455 ?
O2 Li1 Li1 117.1(4) 2 2_455 ?
B5 Li1 Li1 88.2(3) 2 2_455 ?
Li2 Li1 Li1 172.9(4) 2_565 2_455 ?
Na1 Li1 Li1 110.5(3) 1_455 2_455 ?
O3 Li1 Cs1 160.7(4) . 2_565 ?
O6 Li1 Cs1 69.0(2) 1_455 2_565 ?
O1 Li1 Cs1 65.6(2) 2 2_565 ?
O2 Li1 Cs1 66.37(19) 2 2_565 ?
B5 Li1 Cs1 60.60(18) 2 2_565 ?
Li2 Li1 Cs1 110.3(3) 2_565 2_565 ?
Na1 Li1 Cs1 123.9(2) 1_455 2_565 ?
Li1 Li1 Cs1 64.3(2) 2_455 2_565 ?
O3 Li1 Cs1 72.6(3) . 1_445 ?
O6 Li1 Cs1 101.5(3) 1_455 1_445 ?
O1 Li1 Cs1 85.4(3) 2 1_445 ?
O2 Li1 Cs1 143.2(3) 2 1_445 ?
B5 Li1 Cs1 116.9(3) 2 1_445 ?
Li2 Li1 Cs1 123.4(3) 2_565 1_445 ?
Na1 Li1 Cs1 76.58(17) 1_455 1_445 ?
Li1 Li1 Cs1 61.8(3) 2_455 1_445 ?
Cs1 Li1 Cs1 126.1(2) 2_565 1_445 ?
O3 Li1 Cs1 58.3(2) . 2_665 ?
O6 Li1 Cs1 162.7(3) 1_455 2_665 ?
O1 Li1 Cs1 69.8(2) 2 2_665 ?
O2 Li1 Cs1 67.33(19) 2 2_665 ?
B5 Li1 Cs1 63.68(18) 2 2_665 ?
Li2 Li1 Cs1 71.9(2) 2_565 2_665 ?
Na1 Li1 Cs1 108.78(19) 1_455 2_665 ?
Li1 Li1 Cs1 114.7(3) 2_455 2_665 ?
Cs1 Li1 Cs1 124.28(19) 2_565 2_665 ?
Cs1 Li1 Cs1 79.87(14) 1_445 2_665 ?
O3 Li2 O10 138.1(4) 2_565 2_666 ?
O3 Li2 O8 113.4(3) 2_565 2_665 ?
O10 Li2 O8 108.6(3) 2_666 2_665 ?
O3 Li2 O12 97.2(3) 2_565 . ?
O10 Li2 O12 99.5(4) 2_666 . ?
O8 Li2 O12 66.3(2) 2_665 . ?
O3 Li2 O2 92.3(3) 2_565 1_565 ?
O10 Li2 O2 92.7(3) 2_666 1_565 ?
O8 Li2 O2 82.9(3) 2_665 1_565 ?
O12 Li2 O2 149.1(3) . 1_565 ?
O3 Li2 Li1 47.3(3) 2_565 2_565 ?
O10 Li2 Li1 145.3(5) 2_666 2_565 ?
O8 Li2 Li1 80.3(3) 2_665 2_565 ?
O12 Li2 Li1 114.4(3) . 2_565 ?
O2 Li2 Li1 54.3(3) 1_565 2_565 ?
O3 Li2 B1 108.1(3) 2_565 . ?
O10 Li2 B1 106.6(3) 2_666 . ?
O8 Li2 B1 33.58(15) 2_665 . ?
O12 Li2 B1 32.69(14) . . ?
O2 Li2 B1 116.4(3) 1_565 . ?
Li1 Li2 B1 98.7(3) 2_565 . ?
O3 Li2 B4 26.07(15) 2_565 2_565 ?
O10 Li2 B4 114.7(3) 2_666 2_565 ?
O8 Li2 B4 134.4(3) 2_665 2_565 ?
O12 Li2 B4 92.6(3) . 2_565 ?
O2 Li2 B4 108.0(3) 1_565 2_565 ?
Li1 Li2 B4 72.4(3) 2_565 2_565 ?
B1 Li2 B4 116.1(3) . 2_565 ?
O3 Li2 Na2 145.3(4) 2_565 . ?
O10 Li2 Na2 64.5(2) 2_666 . ?
O8 Li2 Na2 54.85(17) 2_665 . ?
O12 Li2 Na2 104.5(3) . . ?
O2 Li2 Na2 55.87(19) 1_565 . ?
Li1 Li2 Na2 98.5(3) 2_565 . ?
B1 Li2 Na2 79.1(2) . . ?
B4 Li2 Na2 162.9(4) 2_565 . ?
O3 Li2 Na1 49.17(18) 2_565 2_665 ?
O10 Li2 Na1 148.8(4) 2_666 2_665 ?
O8 Li2 Na1 75.7(2) 2_665 2_665 ?
O12 Li2 Na1 52.86(16) . 2_665 ?
O2 Li2 Na1 118.4(3) 1_565 2_665 ?
Li1 Li2 Na1 65.4(2) 2_565 2_665 ?
B1 Li2 Na1 59.38(17) . 2_665 ?
B4 Li2 Na1 59.92(16) 2_565 2_665 ?
Na2 Li2 Na1 130.3(2) . 2_665 ?
O3 Li2 Li4 158.4(4) 2_565 . ?
O10 Li2 Li4 30.39(18) 2_666 . ?
O8 Li2 Li4 82.3(2) 2_665 . ?
O12 Li2 Li4 74.9(2) . . ?
O2 Li2 Li4 104.8(3) 1_565 . ?
Li1 Li2 Li4 154.2(4) 2_565 . ?
B1 Li2 Li4 76.3(2) . . ?
B4 Li2 Li4 132.7(3) 2_565 . ?
Na2 Li2 Li4 55.74(16) . . ?
Na1 Li2 Li4 127.8(3) 2_665 . ?
O3 Li2 Na1 102.1(3) 2_565 1_455 ?
O10 Li2 Na1 43.90(19) 2_666 1_455 ?
O8 Li2 Na1 133.9(3) 2_665 1_455 ?
O12 Li2 Na1 81.4(3) . 1_455 ?
O2 Li2 Na1 125.3(3) 1_565 1_455 ?
Li1 Li2 Na1 145.0(3) 2_565 1_455 ?
B1 Li2 Na1 108.5(3) . 1_455 ?
B4 Li2 Na1 76.0(2) 2_565 1_455 ?
Na2 Li2 Na1 107.6(2) . 1_455 ?
Na1 Li2 Na1 110.4(3) 2_665 1_455 ?
Li4 Li2 Na1 57.25(16) . 1_455 ?
O7 Li3 O2 113.4(3) 1_455 2_656 ?
O7 Li3 O5 114.3(3) 1_455 . ?
O2 Li3 O5 129.9(3) 2_656 . ?
O7 Li3 O5 127.5(3) 1_455 2_656 ?
O2 Li3 O5 69.0(2) 2_656 2_656 ?
O5 Li3 O5 93.0(3) . 2_656 ?
O7 Li3 O13 93.8(3) 1_455 . ?
O2 Li3 O13 93.6(3) 2_656 . ?
O5 Li3 O13 69.1(2) . . ?
O5 Li3 O13 138.6(3) 2_656 . ?
O7 Li3 B5 126.9(3) 1_455 2_656 ?
O2 Li3 B5 33.68(16) 2_656 2_656 ?
O5 Li3 B5 115.9(3) . 2_656 ?
O5 Li3 B5 35.34(15) 2_656 2_656 ?
O13 Li3 B5 119.4(3) . 2_656 ?
O7 Li3 B6 98.8(3) 1_455 . ?
O2 Li3 B6 121.8(3) 2_656 . ?
O5 Li3 B6 35.88(15) . . ?
O5 Li3 B6 125.2(3) 2_656 . ?
O13 Li3 B6 34.95(14) . . ?
B5 Li3 B6 132.6(3) 2_656 . ?
O7 Li3 Na2 62.2(2) 1_455 2_666 ?
O2 Li3 Na2 62.4(2) 2_656 2_666 ?
O5 Li3 Na2 133.0(3) . 2_666 ?
O5 Li3 Na2 127.6(3) 2_656 2_666 ?
O13 Li3 Na2 64.64(19) . 2_666 ?
B5 Li3 Na2 94.1(2) 2_656 2_666 ?
B6 Li3 Na2 97.2(2) . 2_666 ?
O7 Li3 Li3 138.4(4) 1_455 2_656 ?
O2 Li3 Li3 99.6(3) 2_656 2_656 ?
O5 Li3 Li3 49.6(2) . 2_656 ?
O5 Li3 Li3 43.36(18) 2_656 2_656 ?
O13 Li3 Li3 109.1(3) . 2_656 ?
B5 Li3 Li3 71.2(3) 2_656 2_656 ?
B6 Li3 Li3 83.3(3) . 2_656 ?
Na2 Li3 Li3 159.2(4) 2_666 2_656 ?
O7 Li3 Li4 38.56(18) 1_455 . ?
O2 Li3 Li4 139.4(3) 2_656 . ?
O5 Li3 Li4 78.3(2) . . ?
O5 Li3 Li4 147.2(3) 2_656 . ?
O13 Li3 Li4 67.7(2) . . ?
B5 Li3 Li4 165.3(3) 2_656 . ?
B6 Li3 Li4 61.06(19) . . ?
Na2 Li3 Li4 77.1(2) 2_666 . ?
Li3 Li3 Li4 120.2(3) 2_656 . ?
O7 Li3 Cs1 57.38(18) 1_455 1_445 ?
O2 Li3 Cs1 142.3(3) 2_656 1_445 ?
O5 Li3 Cs1 78.9(2) . 1_445 ?
O5 Li3 Cs1 88.2(2) 2_656 1_445 ?
O13 Li3 Cs1 122.0(2) . 1_445 ?
B5 Li3 Cs1 117.8(2) 2_656 1_445 ?
B6 Li3 Cs1 95.83(19) . 1_445 ?
Na2 Li3 Cs1 119.4(2) 2_666 1_445 ?
Li3 Li3 Cs1 81.1(3) 2_656 1_445 ?
Li4 Li3 Cs1 59.16(17) . 1_445 ?
O7 Li3 Cs1 74.46(19) 1_455 2_666 ?
O2 Li3 Cs1 57.45(17) 2_656 2_666 ?
O5 Li3 Cs1 152.7(3) . 2_666 ?
O5 Li3 Cs1 63.78(15) 2_656 2_666 ?
O13 Li3 Cs1 137.8(3) . 2_666 ?
B5 Li3 Cs1 52.83(15) 2_656 2_666 ?
B6 Li3 Cs1 170.8(3) . 2_666 ?
Na2 Li3 Cs1 74.24(14) 2_666 2_666 ?
Li3 Li3 Cs1 105.9(3) 2_656 2_666 ?
Li4 Li3 Cs1 112.9(2) . 2_666 ?
Cs1 Li3 Cs1 85.87(12) 1_445 2_666 ?
O7 Li4 O10 117.6(3) 1_455 2_666 ?
O7 Li4 O14 117.1(3) 1_455 . ?
O10 Li4 O14 112.6(3) 2_666 . ?
O7 Li4 O9 126.1(3) 1_455 . ?
O10 Li4 O9 102.7(3) 2_666 . ?
O14 Li4 O9 72.7(2) . . ?
O7 Li4 B7 127.8(3) 1_455 . ?
O10 Li4 B7 114.6(3) 2_666 . ?
O14 Li4 B7 36.15(15) . . ?
O9 Li4 B7 36.74(15) . . ?
O7 Li4 B3 28.02(14) 1_455 1_455 ?
O10 Li4 B3 94.6(3) 2_666 1_455 ?
O14 Li4 B3 145.0(3) . 1_455 ?
O9 Li4 B3 123.9(3) . 1_455 ?
B7 Li4 B3 146.5(3) . 1_455 ?
O7 Li4 B2 93.7(3) 1_455 2_666 ?
O10 Li4 B2 26.32(14) 2_666 2_666 ?
O14 Li4 B2 120.6(3) . 2_666 ?
O9 Li4 B2 128.5(3) . 2_666 ?
B7 Li4 B2 137.1(3) . 2_666 ?
B3 Li4 B2 75.6(2) 1_455 2_666 ?
O7 Li4 B4 139.4(3) 1_455 . ?
O10 Li4 B4 74.8(2) 2_666 . ?
O14 Li4 B4 88.0(2) . . ?
O9 Li4 B4 28.31(14) . . ?
B7 Li4 B4 56.89(17) . . ?
B3 Li4 B4 121.5(3) 1_455 . ?
B2 Li4 B4 100.3(2) 2_666 . ?
O7 Li4 Na2 122.3(3) 1_455 . ?
O10 Li4 Na2 61.55(18) 2_666 . ?
O14 Li4 Na2 57.24(17) . . ?
O9 Li4 Na2 107.6(2) . . ?
B7 Li4 Na2 83.01(19) . . ?
B3 Li4 Na2 127.4(3) 1_455 . ?
B2 Li4 Na2 63.32(16) 2_666 . ?
B4 Li4 Na2 98.0(2) . . ?
O7 Li4 Li3 38.24(18) 1_455 . ?
O10 Li4 Li3 144.9(3) 2_666 . ?
O14 Li4 Li3 79.1(2) . . ?
O9 Li4 Li3 112.4(3) . . ?
B7 Li4 Li3 94.4(2) . . ?
B3 Li4 Li3 66.22(19) 1_455 . ?
B2 Li4 Li3 118.9(3) 2_666 . ?
B4 Li4 Li3 140.1(3) . . ?
Na2 Li4 Li3 105.9(2) . . ?
O7 Li4 Na1 99.5(2) 1_455 1_455 ?
O10 Li4 Na1 47.61(16) 2_666 1_455 ?
O14 Li4 Na1 143.0(3) . 1_455 ?
O9 Li4 Na1 81.7(2) . 1_455 ?
B7 Li4 Na1 115.4(2) . 1_455 ?
B3 Li4 Na1 71.84(17) 1_455 1_455 ?
B2 Li4 Na1 58.33(14) 2_666 1_455 ?
B4 Li4 Na1 58.62(15) . 1_455 ?
Na2 Li4 Na1 108.47(19) . 1_455 ?
Li3 Li4 Na1 136.5(2) . 1_455 ?
O7 Li4 Li2 148.3(3) 1_455 . ?
O10 Li4 Li2 30.78(18) 2_666 . ?
O14 Li4 Li2 86.9(2) . . ?
O9 Li4 Li2 79.1(2) . . ?
B7 Li4 Li2 83.9(2) . . ?
B3 Li4 Li2 124.4(3) 1_455 . ?
B2 Li4 Li2 54.92(19) 2_666 . ?
B4 Li4 Li2 55.1(2) . . ?
Na2 Li4 Li2 51.97(18) . . ?
Li3 Li4 Li2 157.8(3) . . ?
Na1 Li4 Li2 61.89(17) 1_455 . ?
O6 B1 O12 110.6(3) . . ?
O6 B1 O8 113.0(3) . . ?
O12 B1 O8 113.4(3) . . ?
O6 B1 O8 114.4(3) . 2_665 ?
O12 B1 O8 109.9(3) . 2_665 ?
O8 B1 O8 94.6(2) . 2_665 ?
O6 B1 B1 126.4(3) . 2_665 ?
O12 B1 B1 122.9(3) . 2_665 ?
O8 B1 B1 47.99(18) . 2_665 ?
O8 B1 B1 46.60(18) 2_665 2_665 ?
O6 B1 Li2 131.8(3) . . ?
O12 B1 Li2 57.2(3) . . ?
O8 B1 Li2 114.2(3) . . ?
O8 B1 Li2 52.7(2) 2_665 . ?
B1 B1 Li2 81.2(3) 2_665 . ?
O6 B1 Na1 61.17(16) . . ?
O12 B1 Na1 151.5(2) . . ?
O8 B1 Na1 94.14(19) . . ?
O8 B1 Na1 58.48(15) 2_665 . ?
B1 B1 Na1 70.3(2) 2_665 . ?
Li2 B1 Na1 106.0(2) . . ?
O6 B1 Na1 152.6(2) . 2_665 ?
O12 B1 Na1 60.10(16) . 2_665 ?
O8 B1 Na1 57.80(16) . 2_665 ?
O8 B1 Na1 92.62(19) 2_665 2_665 ?
B1 B1 Na1 69.25(19) 2_665 2_665 ?
Li2 B1 Na1 67.71(16) . 2_665 ?
Na1 B1 Na1 139.54(14) . 2_665 ?
O6 B1 Cs1 69.48(17) . 2_665 ?
O12 B1 Cs1 59.54(17) . 2_665 ?
O8 B1 Cs1 93.04(19) . 2_665 ?
O8 B1 Cs1 169.0(2) 2_665 2_665 ?
B1 B1 Cs1 140.4(3) 2_665 2_665 ?
Li2 B1 Cs1 116.7(2) . 2_665 ?
Na1 B1 Cs1 128.85(12) . 2_665 ?
Na1 B1 Cs1 84.71(9) 2_665 2_665 ?
O10 B2 O13 121.5(3) . . ?
O10 B2 O4 120.8(3) . . ?
O13 B2 O4 117.7(3) . . ?
O10 B2 Li4 40.2(2) . 2_666 ?
O13 B2 Li4 98.1(3) . 2_666 ?
O4 B2 Li4 129.3(3) . 2_666 ?
O10 B2 Na1 53.19(18) . 2_766 ?
O13 B2 Na1 165.0(3) . 2_766 ?
O4 B2 Na1 69.02(18) . 2_766 ?
Li4 B2 Na1 68.96(17) 2_666 2_766 ?
O10 B2 Na2 61.53(18) . 2_666 ?
O13 B2 Na2 61.75(17) . 2_666 ?
O4 B2 Na2 168.0(2) . 2_666 ?
Li4 B2 Na2 60.91(15) 2_666 2_666 ?
Na1 B2 Na2 114.71(14) 2_766 2_666 ?
O10 B2 Cs1 100.9(2) . 2_766 ?
O13 B2 Cs1 110.9(2) . 2_766 ?
O4 B2 Cs1 57.99(17) . 2_766 ?
Li4 B2 Cs1 140.86(18) 2_666 2_766 ?
Na1 B2 Cs1 84.08(9) 2_766 2_766 ?
Na2 B2 Cs1 110.36(11) 2_666 2_766 ?
O7 B3 O11 122.5(3) . . ?
O7 B3 O4 120.1(3) . . ?
O11 B3 O4 117.4(3) . . ?
O7 B3 Li4 43.3(2) . 1_655 ?
O11 B3 Li4 90.2(2) . 1_655 ?
O4 B3 Li4 138.5(3) . 1_655 ?
O7 B3 Na2 54.33(18) . 2_766 ?
O11 B3 Na2 163.4(3) . 2_766 ?
O4 B3 Na2 67.94(18) . 2_766 ?
Li4 B3 Na2 77.73(17) 1_655 2_766 ?
O7 B3 Cs1 70.9(2) . 1_545 ?
O11 B3 Cs1 58.95(18) . 1_545 ?
O4 B3 Cs1 152.2(2) . 1_545 ?
Li4 B3 Cs1 68.00(17) 1_655 1_545 ?
Na2 B3 Cs1 124.40(12) 2_766 1_545 ?
O7 B3 Cs1 92.6(2) . 2_766 ?
O11 B3 Cs1 118.9(2) . 2_766 ?
O4 B3 Cs1 58.47(17) . 2_766 ?
Li4 B3 Cs1 135.68(18) 1_655 2_766 ?
Na2 B3 Cs1 77.52(9) 2_766 2_766 ?
Cs1 B3 Cs1 97.65(9) 1_545 2_766 ?
O3 B4 O12 120.3(3) . . ?
O3 B4 O9 122.0(3) . . ?
O12 B4 O9 117.6(3) . . ?
O3 B4 Li2 40.2(2) . 2_565 ?
O12 B4 Li2 80.2(3) . 2_565 ?
O9 B4 Li2 162.2(3) . 2_565 ?
O3 B4 Li4 112.6(3) . . ?
O12 B4 Li4 110.7(3) . . ?
O9 B4 Li4 43.1(2) . . ?
Li2 B4 Li4 133.8(2) 2_565 . ?
O3 B4 Na1 52.00(18) . 1_455 ?
O12 B4 Na1 115.9(2) . 1_455 ?
O9 B4 Na1 102.5(2) . 1_455 ?
Li2 B4 Na1 67.07(17) 2_565 1_455 ?
Li4 B4 Na1 68.02(15) . 1_455 ?
O3 B4 Cs1 88.8(2) . 2_665 ?
O12 B4 Cs1 83.3(2) . 2_665 ?
O9 B4 Cs1 96.8(2) . 2_665 ?
Li2 B4 Cs1 84.6(2) 2_565 2_665 ?
Li4 B4 Cs1 139.82(19) . 2_665 ?
Na1 B4 Cs1 140.76(13) 1_455 2_665 ?
O3 B4 Cs1 76.4(2) . 1_445 ?
O12 B4 Cs1 162.2(2) . 1_445 ?
O9 B4 Cs1 45.85(16) . 1_445 ?
Li2 B4 Cs1 116.5(2) 2_565 1_445 ?
Li4 B4 Cs1 63.31(15) . 1_445 ?
Na1 B4 Cs1 78.52(9) 1_455 1_445 ?
Cs1 B4 Cs1 91.60(10) 2_665 1_445 ?
O2 B5 O1 120.7(3) . . ?
O2 B5 O5 121.5(3) . . ?
O1 B5 O5 117.8(3) . . ?
O2 B5 Li3 56.2(2) . 2_656 ?
O1 B5 Li3 175.4(3) . 2_656 ?
O5 B5 Li3 65.3(2) . 2_656 ?
O2 B5 Li1 67.1(3) . 2 ?
O1 B5 Li1 53.6(3) . 2 ?
O5 B5 Li1 171.3(3) . 2 ?
Li3 B5 Li1 123.2(3) 2_656 2 ?
O2 B5 Cs1 87.8(2) . 1_545 ?
O1 B5 Cs1 83.47(19) . 1_545 ?
O5 B5 Cs1 97.0(2) . 1_545 ?
Li3 B5 Cs1 92.90(19) 2_656 1_545 ?
Li1 B5 Cs1 81.1(2) 2 1_545 ?
O2 B5 Cs1 84.9(2) . 1_445 ?
O1 B5 Cs1 85.75(19) . 1_445 ?
O5 B5 Cs1 101.3(2) . 1_445 ?
Li3 B5 Cs1 97.03(19) 2_656 1_445 ?
Li1 B5 Cs1 80.5(2) 2 1_445 ?
Cs1 B5 Cs1 161.57(13) 1_545 1_445 ?
O14 B6 O13 107.9(3) . . ?
O14 B6 O11 111.1(3) . . ?
O13 B6 O11 111.4(3) . . ?
O14 B6 O5 110.4(3) . . ?
O13 B6 O5 106.8(3) . . ?
O11 B6 O5 109.1(3) . . ?
O14 B6 Li3 107.2(3) . . ?
O13 B6 Li3 59.5(2) . . ?
O11 B6 Li3 141.4(3) . . ?
O5 B6 Li3 50.8(2) . . ?
O14 B6 Na1 57.56(16) . . ?
O13 B6 Na1 116.9(2) . . ?
O11 B6 Na1 54.66(16) . . ?
O5 B6 Na1 136.3(2) . . ?
Li3 B6 Na1 163.7(2) . . ?
O6 B7 O1 107.9(3) . . ?
O6 B7 O14 112.1(3) . . ?
O1 B7 O14 111.2(3) . . ?
O6 B7 O9 110.4(3) . . ?
O1 B7 O9 108.8(3) . . ?
O14 B7 O9 106.5(3) . . ?
O6 B7 Li4 131.8(3) . . ?
O1 B7 Li4 120.2(3) . . ?
O14 B7 Li4 53.1(2) . . ?
O9 B7 Li4 53.6(2) . . ?
O6 B7 Na1 55.84(15) . . ?
O1 B7 Na1 108.6(2) . . ?
O14 B7 Na1 60.04(16) . . ?
O9 B7 Na1 142.6(2) . . ?
Li4 B7 Na1 106.6(2) . . ?
B5 O1 B7 121.6(3) . . ?
B5 O1 Li1 90.9(3) . 2 ?
B7 O1 Li1 140.8(3) . 2 ?
B5 O1 Cs1 73.23(18) . 1_545 ?
B7 O1 Cs1 123.48(19) . 1_545 ?
Li1 O1 Cs1 84.3(2) 2 1_545 ?
B5 O2 Li3 90.1(3) . 2_656 ?
B5 O2 Li1 80.0(3) . 2 ?
Li3 O2 Li1 169.5(3) 2_656 2 ?
B5 O2 Li2 137.2(3) . 1_545 ?
Li3 O2 Li2 127.0(3) 2_656 1_545 ?
Li1 O2 Li2 63.5(3) 2 1_545 ?
B5 O2 Na2 152.6(2) . 1_545 ?
Li3 O2 Na2 72.2(2) 2_656 1_545 ?
Li1 O2 Na2 115.5(2) 2 1_545 ?
Li2 O2 Na2 68.89(17) 1_545 1_545 ?
B5 O2 Cs1 70.5(2) . 1_545 ?
Li3 O2 Cs1 94.7(2) 2_656 1_545 ?
Li1 O2 Cs1 78.55(19) 2 1_545 ?
Li2 O2 Cs1 119.24(19) 1_545 1_545 ?
Na2 O2 Cs1 89.84(9) 1_545 1_545 ?
B5 O2 Cs1 74.8(2) . 1_445 ?
Li3 O2 Cs1 101.6(2) 2_656 1_445 ?
Li1 O2 Cs1 79.55(19) 2 1_445 ?
Li2 O2 Cs1 77.13(17) 1_545 1_445 ?
Na2 O2 Cs1 128.30(10) 1_545 1_445 ?
Cs1 O2 Cs1 141.48(8) 1_545 1_445 ?
B4 O3 Li1 156.9(4) . . ?
B4 O3 Li2 113.8(3) . 2_565 ?
Li1 O3 Li2 81.9(4) . 2_565 ?
B4 O3 Na1 102.3(2) . 1_455 ?
Li1 O3 Na1 93.2(2) . 1_455 ?
Li2 O3 Na1 93.2(3) 2_565 1_455 ?
B4 O3 Cs1 68.7(2) . 2_665 ?
Li1 O3 Cs1 94.7(2) . 2_665 ?
Li2 O3 Cs1 92.4(2) 2_565 2_665 ?
Na1 O3 Cs1 170.82(10) 1_455 2_665 ?
B4 O3 Cs1 83.8(2) . 1_445 ?
Li1 O3 Cs1 79.9(3) . 1_445 ?
Li2 O3 Cs1 161.8(3) 2_565 1_445 ?
Na1 O3 Cs1 87.35(8) 1_455 1_445 ?
Cs1 O3 Cs1 89.54(6) 2_665 1_445 ?
B2 O4 B3 121.8(3) . . ?
B2 O4 Na2 149.5(2) . 2_766 ?
B3 O4 Na2 83.41(19) . 2_766 ?
B2 O4 Na1 82.5(2) . 2_766 ?
B3 O4 Na1 145.9(2) . 2_766 ?
Na2 O4 Na1 67.78(7) 2_766 2_766 ?
B2 O4 Cs1 100.98(19) . 2_766 ?
B3 O4 Cs1 100.2(2) . 2_766 ?
Na2 O4 Cs1 89.77(7) 2_766 2_766 ?
Na1 O4 Cs1 97.56(8) 2_766 2_766 ?
B5 O5 B6 117.1(3) . . ?
B5 O5 Li3 131.2(3) . . ?
B6 O5 Li3 93.4(3) . . ?
B5 O5 Li3 79.4(3) . 2_656 ?
B6 O5 Li3 155.8(3) . 2_656 ?
Li3 O5 Li3 87.0(3) . 2_656 ?
B5 O5 Cs1 61.56(18) . 1_545 ?
B6 O5 Cs1 88.00(18) . 1_545 ?
Li3 O5 Cs1 163.0(2) . 1_545 ?
Li3 O5 Cs1 84.94(18) 2_656 1_545 ?
B1 O6 B7 115.4(3) . . ?
B1 O6 Li1 121.2(3) . 1_655 ?
B7 O6 Li1 123.3(3) . 1_655 ?
B1 O6 Na1 89.20(18) . . ?
B7 O6 Na1 96.28(19) . . ?
Li1 O6 Na1 87.3(2) 1_655 . ?
B1 O6 Cs1 88.45(18) . 2_665 ?
B7 O6 Cs1 97.30(18) . 2_665 ?
Li1 O6 Cs1 82.0(2) 1_655 2_665 ?
Na1 O6 Cs1 165.88(9) . 2_665 ?
B3 O7 Li3 147.9(3) . 1_655 ?
B3 O7 Li4 108.7(3) . 1_655 ?
Li3 O7 Li4 103.2(3) 1_655 1_655 ?
B3 O7 Na2 99.5(2) . 2_766 ?
Li3 O7 Na2 73.7(2) 1_655 2_766 ?
Li4 O7 Na2 107.6(2) 1_655 2_766 ?
B3 O7 Cs1 87.8(2) . 1_545 ?
Li3 O7 Cs1 94.7(2) 1_655 1_545 ?
Li4 O7 Cs1 79.2(2) 1_655 1_545 ?
Na2 O7 Cs1 167.48(10) 2_766 1_545 ?
B1 O8 B1 85.4(2) . 2_665 ?
B1 O8 Li2 117.3(3) . 2_665 ?
B1 O8 Li2 93.7(3) 2_665 2_665 ?
B1 O8 Na2 143.5(2) . 2_665 ?
B1 O8 Na2 129.56(19) 2_665 2_665 ?
Li2 O8 Na2 75.7(2) 2_665 2_665 ?
B1 O8 Na1 92.07(19) . 2_665 ?
B1 O8 Na1 90.37(18) 2_665 2_665 ?
Li2 O8 Na1 150.6(2) 2_665 2_665 ?
Na2 O8 Na1 79.31(9) 2_665 2_665 ?
B4 O9 B7 122.3(3) . . ?
B4 O9 Li4 108.6(3) . . ?
B7 O9 Li4 89.6(3) . . ?
B4 O9 Cs1 115.1(2) . 1_445 ?
B7 O9 Cs1 119.94(19) . 1_445 ?
Li4 O9 Cs1 88.23(19) . 1_445 ?
B4 O9 Cs1 60.87(18) . 2_665 ?
B7 O9 Cs1 94.38(18) . 2_665 ?
Li4 O9 Cs1 169.2(2) . 2_665 ?
Cs1 O9 Cs1 98.40(7) 1_445 2_665 ?
B2 O10 Li4 113.5(3) . 2_666 ?
B2 O10 Li2 119.9(3) . 2_666 ?
Li4 O10 Li2 118.8(3) 2_666 2_666 ?
B2 O10 Na1 100.4(2) . 2_766 ?
Li4 O10 Na1 95.8(2) 2_666 2_766 ?
Li2 O10 Na1 101.6(3) 2_666 2_766 ?
B2 O10 Na2 91.9(2) . 2_666 ?
Li4 O10 Na2 77.9(2) 2_666 2_666 ?
Li2 O10 Na2 73.0(2) 2_666 2_666 ?
Na1 O10 Na2 167.60(12) 2_766 2_666 ?
B3 O11 B6 123.0(3) . . ?
B3 O11 Na1 119.8(2) . . ?
B6 O11 Na1 97.67(19) . . ?
B3 O11 Cs1 99.0(2) . 1_545 ?
B6 O11 Cs1 116.8(2) . 1_545 ?
Na1 O11 Cs1 99.07(8) . 1_545 ?
B4 O12 B1 121.6(3) . . ?
B4 O12 Li2 100.2(3) . . ?
B1 O12 Li2 90.1(3) . . ?
B4 O12 Na1 148.4(2) . 2_665 ?
B1 O12 Na1 89.86(18) . 2_665 ?
Li2 O12 Na1 81.37(19) . 2_665 ?
B4 O12 Cs1 72.24(19) . 2_665 ?
B1 O12 Cs1 98.17(19) . 2_665 ?
Li2 O12 Cs1 170.9(2) . 2_665 ?
Na1 O12 Cs1 102.29(9) 2_665 2_665 ?
B2 O13 B6 124.3(3) . . ?
B2 O13 Li3 120.2(3) . . ?
B6 O13 Li3 85.6(3) . . ?
B2 O13 Na2 90.7(2) . 2_666 ?
B6 O13 Na2 143.5(2) . 2_666 ?
Li3 O13 Na2 65.74(18) . 2_666 ?
B6 O14 B7 121.2(3) . . ?
B6 O14 Li4 111.1(3) . . ?
B7 O14 Li4 90.7(3) . . ?
B6 O14 Na2 108.8(2) . . ?
B7 O14 Na2 128.9(2) . . ?
Li4 O14 Na2 80.1(2) . . ?
B6 O14 Na1 95.29(19) . . ?
B7 O14 Na1 91.30(18) . . ?
Li4 O14 Na1 147.5(2) . . ?
Na2 O14 Na1 73.53(8) . . ?

_diffrn_measured_fraction_theta_max 0.980
_diffrn_reflns_theta_full        27.53
_diffrn_measured_fraction_theta_full 0.980
_refine_diff_density_max         1.642
_refine_diff_density_min         -1.405
_refine_diff_density_rms         0.131
