# Electronic Supplementary Material (ESI) for CrystEngComm.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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#######################################################################

data_Complex1
_database_code_depnum_ccdc_archive 'CCDC 1584341'
_audit_update_record             
;
2017-11-07 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C58 H70 Ag10 F18 O7'
_chemical_formula_weight         2299.84

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   21.2880(12)
_cell_length_b                   15.5482(9)
_cell_length_c                   22.5226(13)
_cell_angle_alpha                90
_cell_angle_beta                 90.5300(10)
_cell_angle_gamma                90
_cell_volume                     7454.4(7)
_cell_formula_units_Z            4
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9823
_cell_measurement_theta_min      2.9305
_cell_measurement_theta_max      28.3818

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.049
_exptl_crystal_F_000             4424
_exptl_transmission_factor_min   0.6402
_exptl_transmission_factor_max   0.7457
_exptl_crystal_size_max          0.326
_exptl_crystal_size_mid          0.273
_exptl_crystal_size_min          0.165
_exptl_absorpt_coefficient_mu    2.654
_shelx_estimated_absorpt_T_min   0.478
_shelx_estimated_absorpt_T_max   0.669
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            49599
_diffrn_reflns_av_unetI/netI     0.0185
_diffrn_reflns_av_R_equivalents  0.0209
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_theta_min         2.885
_diffrn_reflns_theta_max         25.026
_diffrn_reflns_theta_full        25.026
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measured_fraction_theta_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_point_group_measured_fraction_full 0.997
_reflns_number_total             13142
_reflns_number_gt                11802
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0126P)²+39.1537P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         13142
_refine_ls_number_parameters     874
_refine_ls_number_restraints     87
_refine_ls_R_factor_all          0.0413
_refine_ls_R_factor_gt           0.0353
_refine_ls_wR_factor_ref         0.0781
_refine_ls_wR_factor_gt          0.0739
_refine_ls_goodness_of_fit_ref   1.188
_refine_ls_restrained_S_all      1.203
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1A Ag 0.62529(19) 0.7817(3) 0.3929(2) 0.0342(6) Uani 0.79(4) 1 d . . P A 1
Ag1B Ag 0.6382(17) 0.7741(12) 0.3860(9) 0.049(3) Uani 0.21(4) 1 d . . P A 2
Ag2 Ag 0.76174(2) 0.77886(2) 0.36127(2) 0.03159(9) Uani 1 1 d . . . . .
Ag3 Ag 0.63298(2) 0.60096(3) 0.43535(2) 0.03442(10) Uani 1 1 d . . . . .
Ag4 Ag 0.73557(2) 0.59162(3) 0.34806(2) 0.03520(10) Uani 1 1 d . . . . .
Ag5 Ag 0.71897(2) 0.47226(3) 0.49563(2) 0.03638(10) Uani 1 1 d . . . . .
Ag6 Ag 0.88242(2) 0.70218(3) 0.40468(2) 0.03745(10) Uani 1 1 d . . . . .
Ag7 Ag 0.82976(2) 0.65846(3) 0.53596(2) 0.03830(10) Uani 1 1 d . . . . .
Ag8 Ag 0.75647(2) 0.81099(3) 0.49005(2) 0.03988(10) Uani 1 1 d . . . . .
Ag9 Ag 0.69350(8) 0.66703(4) 0.54903(8) 0.0364(3) Uani 0.945(8) 1 d . . P A 1
Ag9A Ag 0.6779(11) 0.6654(8) 0.5322(11) 0.0364(3) Uani 0.055(8) 1 d . . P A 2
Ag10 Ag 0.83476(2) 0.53304(3) 0.44038(2) 0.03183(9) Uani 1 1 d . . . . .
F1 F 1.0484(4) 0.9611(5) 0.3305(3) 0.171(4) Uani 1 1 d . U . . .
F2 F 1.0641(4) 0.8388(6) 0.3103(5) 0.205(5) Uani 1 1 d . U . . .
F3 F 0.9973(4) 0.9023(8) 0.2689(3) 0.217(6) Uani 1 1 d . U . . .
F4 F 0.8889(3) 0.5611(5) 0.6468(2) 0.151(3) Uani 1 1 d . U . . .
F5 F 0.8814(4) 0.4558(4) 0.7016(3) 0.164(4) Uani 1 1 d . U . . .
F6 F 0.8157(4) 0.5457(6) 0.7002(3) 0.161(3) Uani 1 1 d . U . . .
F7 F 0.8060(3) 0.1800(3) 0.5521(3) 0.114(2) Uani 1 1 d . . . . .
F8 F 0.7988(3) 0.1985(3) 0.6441(3) 0.113(2) Uani 1 1 d . . . . .
F9 F 0.7187(2) 0.1910(3) 0.5910(3) 0.108(2) Uani 1 1 d . . . . .
F10 F 0.9334(11) 1.0355(12) 0.4988(11) 0.150(7) Uani 0.294(14) 1 d D U P B 1
F11 F 0.8430(7) 1.0268(11) 0.4575(8) 0.111(9) Uani 0.294(14) 1 d D U P B 1
F12 F 0.8680(7) 0.9586(13) 0.5368(6) 0.150(14) Uani 0.294(14) 1 d D U P B 1
F10A F 0.8982(7) 1.0580(5) 0.4620(5) 0.150(7) Uani 0.706(14) 1 d D U P B 2
F11A F 0.8290(3) 0.9815(5) 0.5034(5) 0.091(4) Uani 0.706(14) 1 d D U P B 2
F12A F 0.9213(4) 0.9782(9) 0.5329(5) 0.146(7) Uani 0.706(14) 1 d D U P B 2
F13 F 0.4547(2) 0.8708(5) 0.2622(2) 0.111(2) Uani 1 1 d . . . . .
F14 F 0.4377(3) 0.9674(4) 0.3210(3) 0.135(3) Uani 1 1 d . . . . .
F15 F 0.3799(2) 0.8598(6) 0.3199(3) 0.151(3) Uani 1 1 d . . . . .
F16 F 0.4732(2) 0.6476(3) 0.5163(3) 0.0987(19) Uani 1 1 d . . . . .
F17 F 0.39018(18) 0.7191(3) 0.49669(19) 0.0722(12) Uani 1 1 d . . . . .
F18 F 0.4568(2) 0.7688(3) 0.55720(18) 0.0784(13) Uani 1 1 d . . . . .
O1 O 0.87221(18) 0.8396(2) 0.45377(18) 0.0408(9) Uani 1 1 d . . . . .
O2 O 0.9612(2) 0.7824(3) 0.3602(2) 0.0642(13) Uani 1 1 d . . . . .
O3 O 0.79361(18) 0.5083(2) 0.57730(16) 0.0395(9) Uani 1 1 d . . . . .
O4 O 0.74798(19) 0.3392(3) 0.53431(18) 0.0436(9) Uani 1 1 d . . . . .
O5 O 0.53909(18) 0.8532(3) 0.34918(17) 0.0441(10) Uani 1 1 d . . . . .
O6 O 0.5463(2) 0.7726(3) 0.46809(18) 0.0508(11) Uani 1 1 d . . . . .
C1 C 0.7122(2) 0.8706(3) 0.4088(2) 0.0353(12) Uani 1 1 d . . . . .
C2 C 0.6848(3) 0.9249(3) 0.4377(2) 0.0340(12) Uani 1 1 d . . . . .
C3 C 0.6548(3) 0.9973(4) 0.4702(3) 0.0439(14) Uani 1 1 d . . . . .
C4 C 0.5854(3) 0.9990(5) 0.4564(4) 0.084(3) Uani 1 1 d . . . . .
H4A H 0.5658 1.0467 0.4778 0.125 Uiso 1 1 calc R U . . .
H4B H 0.5789 1.0068 0.4136 0.125 Uiso 1 1 calc R U . . .
H4C H 0.5664 0.9446 0.4688 0.125 Uiso 1 1 calc R U . . .
C5 C 0.6848(4) 1.0818(4) 0.4495(3) 0.0609(19) Uani 1 1 d . . . . .
H5A H 0.6656 1.1302 0.4705 0.091 Uiso 1 1 calc R U . . .
H5B H 0.7300 1.0806 0.4581 0.091 Uiso 1 1 calc R U . . .
H5C H 0.6780 1.0886 0.4066 0.091 Uiso 1 1 calc R U . . .
C6 C 0.6681(4) 0.9871(5) 0.5361(3) 0.071(2) Uani 1 1 d . . . . .
H6A H 0.6485 1.0345 0.5578 0.107 Uiso 1 1 calc R U . . .
H6B H 0.6508 0.9323 0.5499 0.107 Uiso 1 1 calc R U . . .
H6C H 0.7136 0.9879 0.5432 0.107 Uiso 1 1 calc R U . . .
C7 C 0.6307(2) 0.6434(3) 0.3483(2) 0.0340(12) Uani 1 1 d . . . . .
C8 C 0.6246(2) 0.6582(4) 0.2962(2) 0.0348(12) Uani 1 1 d . . . . .
C9 C 0.6125(3) 0.6793(4) 0.2324(3) 0.0468(15) Uani 1 1 d . . . . .
C10 C 0.5430(4) 0.6650(7) 0.2189(4) 0.099(4) Uani 1 1 d . . . . .
H10A H 0.5343 0.6786 0.1772 0.149 Uiso 1 1 calc R U . . .
H10B H 0.5322 0.6047 0.2266 0.149 Uiso 1 1 calc R U . . .
H10C H 0.5178 0.7023 0.2444 0.149 Uiso 1 1 calc R U . . .
C11 C 0.6542(5) 0.6232(6) 0.1939(3) 0.090(3) Uani 1 1 d . . . . .
H11A H 0.6465 0.6367 0.1520 0.135 Uiso 1 1 calc R U . . .
H11B H 0.6983 0.6343 0.2038 0.135 Uiso 1 1 calc R U . . .
H11C H 0.6445 0.5625 0.2012 0.135 Uiso 1 1 calc R U . . .
C12 C 0.6293(4) 0.7734(5) 0.2224(3) 0.069(2) Uani 1 1 d . . . . .
H12A H 0.6216 0.7885 0.1807 0.103 Uiso 1 1 calc R U . . .
H12B H 0.6033 0.8098 0.2479 0.103 Uiso 1 1 calc R U . . .
H12C H 0.6737 0.7825 0.2322 0.103 Uiso 1 1 calc R U . . .
C13 C 0.6339(2) 0.5556(3) 0.5218(2) 0.0332(11) Uani 1 1 d . . . . .
C14 C 0.6223(2) 0.5262(4) 0.5698(3) 0.0376(13) Uani 1 1 d . . . . .
C15 C 0.6024(3) 0.4944(5) 0.6289(3) 0.0526(17) Uani 1 1 d . . . . .
C16 C 0.6311(6) 0.5513(7) 0.6777(3) 0.109(4) Uani 1 1 d . . . . .
H16A H 0.6179 0.5302 0.7166 0.163 Uiso 1 1 calc R U . . .
H16B H 0.6770 0.5493 0.6753 0.163 Uiso 1 1 calc R U . . .
H16C H 0.6167 0.6107 0.6723 0.163 Uiso 1 1 calc R U . . .
C17 C 0.5325(4) 0.4946(10) 0.6298(5) 0.148(6) Uani 1 1 d . . . . .
H17A H 0.5181 0.4738 0.6684 0.223 Uiso 1 1 calc R U . . .
H17B H 0.5171 0.5532 0.6232 0.223 Uiso 1 1 calc R U . . .
H17C H 0.5164 0.4568 0.5983 0.223 Uiso 1 1 calc R U . . .
C18 C 0.6282(4) 0.4040(5) 0.6384(3) 0.075(2) Uani 1 1 d . . . . .
H18A H 0.6152 0.3827 0.6773 0.113 Uiso 1 1 calc R U . . .
H18B H 0.6118 0.3658 0.6073 0.113 Uiso 1 1 calc R U . . .
H18C H 0.6742 0.4053 0.6366 0.113 Uiso 1 1 calc R U . . .
C19 C 0.7629(2) 0.4651(3) 0.4000(2) 0.0310(11) Uani 1 1 d . . . . .
C20 C 0.7236(2) 0.4269(3) 0.3704(2) 0.0273(10) Uani 1 1 d . . . . .
C21 C 0.6800(3) 0.3707(3) 0.3372(3) 0.0360(12) Uani 1 1 d . . . . .
C22 C 0.6123(3) 0.3942(4) 0.3531(3) 0.0514(16) Uani 1 1 d . . . . .
H22A H 0.5832 0.3569 0.3310 0.077 Uiso 1 1 calc R U . . .
H22B H 0.6061 0.3864 0.3958 0.077 Uiso 1 1 calc R U . . .
H22C H 0.6042 0.4544 0.3425 0.077 Uiso 1 1 calc R U . . .
C23 C 0.6947(4) 0.2775(4) 0.3553(4) 0.064(2) Uani 1 1 d . . . . .
H23A H 0.6664 0.2383 0.3339 0.096 Uiso 1 1 calc R U . . .
H23B H 0.7383 0.2639 0.3453 0.096 Uiso 1 1 calc R U . . .
H23C H 0.6888 0.2707 0.3981 0.096 Uiso 1 1 calc R U . . .
C24 C 0.6896(3) 0.3829(5) 0.2712(3) 0.0575(18) Uani 1 1 d . . . . .
H24A H 0.6606 0.3455 0.2492 0.086 Uiso 1 1 calc R U . . .
H24B H 0.6814 0.4430 0.2606 0.086 Uiso 1 1 calc R U . . .
H24C H 0.7329 0.3680 0.2612 0.086 Uiso 1 1 calc R U . . .
C25 C 0.8156(2) 0.6852(3) 0.3206(2) 0.0317(11) Uani 1 1 d . . . . .
C26 C 0.8508(2) 0.6349(3) 0.2962(2) 0.0309(11) Uani 1 1 d . . . . .
C27 C 0.8936(3) 0.5760(4) 0.2642(2) 0.0400(13) Uani 1 1 d . . . . .
C28 C 0.9284(4) 0.5194(5) 0.3088(3) 0.069(2) Uani 1 1 d . . . . .
H28A H 0.9567 0.4805 0.2877 0.104 Uiso 1 1 calc R U . . .
H28B H 0.9529 0.5556 0.3361 0.104 Uiso 1 1 calc R U . . .
H28C H 0.8980 0.4855 0.3314 0.104 Uiso 1 1 calc R U . . .
C29 C 0.8550(4) 0.5191(5) 0.2226(3) 0.066(2) Uani 1 1 d . . . . .
H29A H 0.8830 0.4800 0.2013 0.099 Uiso 1 1 calc R U . . .
H29B H 0.8249 0.4855 0.2458 0.099 Uiso 1 1 calc R U . . .
H29C H 0.8321 0.5552 0.1940 0.099 Uiso 1 1 calc R U . . .
C30 C 0.9399(3) 0.6289(5) 0.2285(4) 0.067(2) Uani 1 1 d . . . . .
H30A H 0.9683 0.5903 0.2073 0.101 Uiso 1 1 calc R U . . .
H30B H 0.9168 0.6647 0.1998 0.101 Uiso 1 1 calc R U . . .
H30C H 0.9643 0.6658 0.2554 0.101 Uiso 1 1 calc R U . . .
C31 C 0.9053(2) 0.6051(3) 0.4809(2) 0.0326(11) Uani 1 1 d . . . . .
C32 C 0.9534(2) 0.6391(3) 0.4984(2) 0.0286(11) Uani 1 1 d . . . . .
C33 C 1.0147(2) 0.6698(4) 0.5202(2) 0.0355(12) Uani 1 1 d . . . . .
C34 C 1.0130(4) 0.7664(4) 0.5298(4) 0.069(2) Uani 1 1 d . . . . .
H34A H 1.0541 0.7861 0.5443 0.103 Uiso 1 1 calc R U . . .
H34B H 1.0029 0.7952 0.4922 0.103 Uiso 1 1 calc R U . . .
H34C H 0.9808 0.7804 0.5592 0.103 Uiso 1 1 calc R U . . .
C35 C 1.0310(3) 0.6224(5) 0.5781(3) 0.0564(18) Uani 1 1 d . . . . .
H35A H 1.0719 0.6424 0.5931 0.085 Uiso 1 1 calc R U . . .
H35B H 0.9987 0.6342 0.6077 0.085 Uiso 1 1 calc R U . . .
H35C H 1.0330 0.5604 0.5705 0.085 Uiso 1 1 calc R U . . .
C36 C 1.0639(3) 0.6461(6) 0.4734(3) 0.071(2) Uani 1 1 d . . . . .
H36A H 1.1055 0.6658 0.4867 0.106 Uiso 1 1 calc R U . . .
H36B H 1.0647 0.5835 0.4681 0.106 Uiso 1 1 calc R U . . .
H36C H 1.0531 0.6737 0.4355 0.106 Uiso 1 1 calc R U . . .
C37 C 0.7680(3) 0.7512(3) 0.5763(2) 0.0357(12) Uani 1 1 d . . . . .
C38 C 0.7837(3) 0.7886(4) 0.6211(3) 0.0407(13) Uani 1 1 d . . . . .
C39 C 0.8027(3) 0.8330(5) 0.6763(3) 0.0582(18) Uani 1 1 d . . . . .
C40 C 0.7738(5) 0.7869(8) 0.7283(3) 0.098(3) Uani 1 1 d . . . . .
H40A H 0.7861 0.8159 0.7652 0.147 Uiso 1 1 calc R U . . .
H40B H 0.7280 0.7877 0.7242 0.147 Uiso 1 1 calc R U . . .
H40C H 0.7887 0.7272 0.7292 0.147 Uiso 1 1 calc R U . . .
C41 C 0.7784(5) 0.9250(6) 0.6739(4) 0.109(4) Uani 1 1 d . . . . .
H41A H 0.7907 0.9552 0.7104 0.164 Uiso 1 1 calc R U . . .
H41B H 0.7964 0.9546 0.6396 0.164 Uiso 1 1 calc R U . . .
H41C H 0.7325 0.9245 0.6702 0.164 Uiso 1 1 calc R U . . .
C42 C 0.8745(4) 0.8317(7) 0.6806(4) 0.093(3) Uani 1 1 d . . . . .
H42A H 0.8881 0.8610 0.7171 0.139 Uiso 1 1 calc R U . . .
H42B H 0.8893 0.7720 0.6813 0.139 Uiso 1 1 calc R U . . .
H42C H 0.8921 0.8614 0.6462 0.139 Uiso 1 1 calc R U . . .
C43 C 0.8863(3) 0.9811(4) 0.4842(3) 0.0621(19) Uani 1 1 d D . . . .
C44 C 0.9025(3) 0.9075(4) 0.4437(3) 0.0410(13) Uani 1 1 d . . . . .
C45 C 0.9492(3) 0.9215(4) 0.4021(3) 0.0502(16) Uani 1 1 d . . . . .
H45 H 0.9661 0.9779 0.3994 0.060 Uiso 1 1 calc R U . . .
C46 C 0.9729(3) 0.8598(5) 0.3643(3) 0.0489(15) Uani 1 1 d . . . . .
C47 C 1.0216(4) 0.8905(7) 0.3197(4) 0.078(3) Uani 1 1 d . . . . .
C48 C 0.8524(3) 0.5043(5) 0.6656(3) 0.0531(16) Uani 1 1 d . . . . .
C49 C 0.8146(2) 0.4592(4) 0.6166(2) 0.0355(12) Uani 1 1 d . . . . .
C50 C 0.8079(2) 0.3703(4) 0.6214(2) 0.0373(12) Uani 1 1 d . . . . .
H50 H 0.8263 0.3429 0.6550 0.045 Uiso 1 1 calc R U . . .
C51 C 0.7761(2) 0.3187(3) 0.5802(2) 0.0345(12) Uani 1 1 d . . . . .
C52 C 0.7755(3) 0.2214(4) 0.5925(3) 0.0521(16) Uani 1 1 d . . . . .
C53 C 0.4372(3) 0.8816(5) 0.3160(3) 0.0593(19) Uani 1 1 d . . . . .
C54 C 0.4829(3) 0.8440(4) 0.3617(3) 0.0410(13) Uani 1 1 d . . . . .
C55 C 0.4555(3) 0.8034(4) 0.4107(3) 0.0442(14) Uani 1 1 d . . . . .
H55 H 0.4110 0.7985 0.4112 0.053 Uiso 1 1 calc R U . . .
C56 C 0.4883(3) 0.7709(4) 0.4569(3) 0.0429(14) Uani 1 1 d . . . . .
C57 C 0.4514(3) 0.7257(5) 0.5066(3) 0.0553(17) Uani 1 1 d . . . . .
C101 C 0.5856(5) 0.8022(7) 0.6297(4) 0.098(3) Uani 1 1 d . . . . .
O101 O 0.6075(3) 0.7657(5) 0.5762(3) 0.095(2) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1A C1 2.334(6) . ?
Ag1A O5 2.354(5) . ?
Ag1A C7 2.377(7) . ?
Ag1A O6 2.402(7) . ?
Ag1A Ag3 2.973(4) . ?
Ag1A Ag2 2.997(5) . ?
Ag1B C7 2.21(2) . ?
Ag1B C1 2.23(2) . ?
Ag1B O5 2.57(3) . ?
Ag1B Ag2 2.69(4) . ?
Ag1B Ag3 2.914(16) . ?
Ag2 C25 2.072(5) . ?
Ag2 C1 2.078(5) . ?
Ag2 Ag8 2.9463(6) . ?
Ag2 Ag4 2.9785(6) . ?
Ag2 Ag6 2.9885(6) . ?
Ag3 C7 2.069(5) . ?
Ag3 C13 2.071(5) . ?
Ag3 Ag9A 2.58(3) . ?
Ag3 Ag4 2.9555(6) . ?
Ag3 Ag5 3.0252(6) . ?
Ag3 Ag9 3.035(2) . ?
Ag4 C25 2.329(5) . ?
Ag4 C19 2.358(5) . ?
Ag4 C7 2.373(5) . ?
Ag4 C20 2.623(5) . ?
Ag4 Ag10 3.0873(6) . ?
Ag5 C13 2.307(5) . ?
Ag5 O4 2.326(4) . ?
Ag5 C19 2.360(5) . ?
Ag5 O3 2.484(4) . ?
Ag5 Ag10 2.9284(6) . ?
Ag5 Ag9A 3.236(13) . ?
Ag5 Ag9 3.3050(9) . ?
Ag6 O2 2.324(4) . ?
Ag6 C31 2.333(5) . ?
Ag6 C25 2.373(5) . ?
Ag6 O1 2.417(4) . ?
Ag6 Ag10 2.9337(6) . ?
Ag6 Ag7 3.2437(6) . ?
Ag7 C37 2.157(5) . ?
Ag7 C31 2.202(5) . ?
Ag7 Ag10 2.9073(6) . ?
Ag7 Ag9 2.9213(15) . ?
Ag7 Ag8 3.0162(6) . ?
Ag7 Ag9A 3.23(2) . ?
Ag8 C37 2.166(5) . ?
Ag8 C1 2.250(5) . ?
Ag8 C2 2.612(5) . ?
Ag8 Ag9 2.9333(7) . ?
Ag8 Ag9A 2.976(13) . ?
Ag9 C37 2.141(6) . ?
Ag9 C13 2.231(6) . ?
Ag9 O101 2.470(5) . ?
Ag9 C14 2.706(6) . ?
Ag9A C13 1.961(19) . ?
Ag9A O101 2.385(14) . ?
Ag9A C37 2.53(3) . ?
Ag9A C14 2.611(14) . ?
Ag10 C19 2.063(5) . ?
Ag10 C31 2.078(5) . ?
F1 C47 1.259(11) . ?
F2 C47 1.230(11) . ?
F3 C47 1.263(11) . ?
F4 C48 1.251(8) . ?
F5 C48 1.264(8) . ?
F6 C48 1.283(9) . ?
F7 C52 1.295(8) . ?
F8 C52 1.308(8) . ?
F9 C52 1.297(8) . ?
F10 C43 1.349(16) . ?
F11 C43 1.307(14) . ?
F12 C43 1.297(14) . ?
F10A C43 1.322(10) . ?
F11A C43 1.299(9) . ?
F12A C43 1.320(10) . ?
F13 C53 1.282(8) . ?
F14 C53 1.338(10) . ?
F15 C53 1.269(8) . ?
F16 C57 1.317(8) . ?
F17 C57 1.325(8) . ?
F18 C57 1.326(8) . ?
O1 C44 1.259(7) . ?
O2 C46 1.233(8) . ?
O3 C49 1.248(6) . ?
O4 C51 1.233(7) . ?
O5 C54 1.240(7) . ?
O6 C56 1.258(7) . ?
C1 C2 1.217(7) . ?
C2 C3 1.489(7) . ?
C3 C4 1.508(9) . ?
C3 C6 1.517(9) . ?
C3 C5 1.535(9) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.202(7) . ?
C8 C9 1.494(7) . ?
C9 C11 1.522(10) . ?
C9 C10 1.523(10) . ?
C9 C12 1.523(9) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.201(7) . ?
C14 C15 1.485(8) . ?
C15 C17 1.489(10) . ?
C15 C18 1.523(10) . ?
C15 C16 1.533(12) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.219(7) . ?
C20 C21 1.473(7) . ?
C21 C24 1.514(8) . ?
C21 C22 1.533(8) . ?
C21 C23 1.537(8) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.218(7) . ?
C26 C27 1.483(7) . ?
C27 C30 1.518(9) . ?
C27 C28 1.524(8) . ?
C27 C29 1.524(9) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.216(7) . ?
C32 C33 1.469(7) . ?
C33 C34 1.518(9) . ?
C33 C35 1.537(8) . ?
C33 C36 1.539(9) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.209(8) . ?
C38 C39 1.476(8) . ?
C39 C40 1.508(11) . ?
C39 C41 1.522(12) . ?
C39 C42 1.532(10) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.506(9) . ?
C44 C45 1.389(9) . ?
C45 C46 1.380(10) . ?
C45 H45 0.9500 . ?
C46 C47 1.528(9) . ?
C48 C49 1.530(8) . ?
C49 C50 1.395(8) . ?
C50 C51 1.395(8) . ?
C50 H50 0.9500 . ?
C51 C52 1.539(8) . ?
C53 C54 1.528(9) . ?
C54 C55 1.402(8) . ?
C55 C56 1.348(8) . ?
C55 H55 0.9500 . ?
C56 C57 1.543(9) . ?
C101 O101 1.416(10) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Ag1A O5 113.5(2) . . ?
C1 Ag1A C7 124.0(3) . . ?
O5 Ag1A C7 107.0(2) . . ?
C1 Ag1A O6 119.0(3) . . ?
O5 Ag1A O6 77.0(2) . . ?
C7 Ag1A O6 106.4(2) . . ?
C1 Ag1A Ag3 117.97(19) . . ?
O5 Ag1A Ag3 128.45(17) . . ?
C7 Ag1A Ag3 43.77(14) . . ?
O6 Ag1A Ag3 75.76(15) . . ?
C1 Ag1A Ag2 43.70(15) . . ?
O5 Ag1A Ag2 131.39(19) . . ?
C7 Ag1A Ag2 80.5(2) . . ?
O6 Ag1A Ag2 148.52(17) . . ?
Ag3 Ag1A Ag2 90.68(13) . . ?
C7 Ag1B C1 139(2) . . ?
C7 Ag1B O5 105.0(8) . . ?
C1 Ag1B O5 109.1(8) . . ?
C7 Ag1B Ag2 90.8(13) . . ?
C1 Ag1B Ag2 48.8(7) . . ?
O5 Ag1B Ag2 136.0(7) . . ?
C7 Ag1B Ag3 45.1(3) . . ?
C1 Ag1B Ag3 124.3(9) . . ?
O5 Ag1B Ag3 122.0(11) . . ?
Ag2 Ag1B Ag3 98.4(10) . . ?
C25 Ag2 C1 175.0(2) . . ?
C25 Ag2 Ag1B 128.1(5) . . ?
C1 Ag2 Ag1B 53.9(5) . . ?
C25 Ag2 Ag8 125.50(14) . . ?
C1 Ag2 Ag8 49.61(15) . . ?
Ag1B Ag2 Ag8 75.8(3) . . ?
C25 Ag2 Ag4 51.15(14) . . ?
C1 Ag2 Ag4 128.83(15) . . ?
Ag1B Ag2 Ag4 79.1(4) . . ?
Ag8 Ag2 Ag4 104.791(17) . . ?
C25 Ag2 Ag6 52.18(15) . . ?
C1 Ag2 Ag6 122.99(15) . . ?
Ag1B Ag2 Ag6 139.4(3) . . ?
Ag8 Ag2 Ag6 77.640(16) . . ?
Ag4 Ag2 Ag6 78.590(15) . . ?
C25 Ag2 Ag1A 131.05(17) . . ?
C1 Ag2 Ag1A 50.90(17) . . ?
Ag8 Ag2 Ag1A 73.62(8) . . ?
Ag4 Ag2 Ag1A 81.80(9) . . ?
Ag6 Ag2 Ag1A 139.49(7) . . ?
C7 Ag3 C13 178.4(2) . . ?
C7 Ag3 Ag9A 133.2(3) . . ?
C13 Ag3 Ag9A 48.4(3) . . ?
C7 Ag3 Ag1B 49.1(4) . . ?
C13 Ag3 Ag1B 132.3(4) . . ?
Ag9A Ag3 Ag1B 87.1(4) . . ?
C7 Ag3 Ag4 52.87(15) . . ?
C13 Ag3 Ag4 127.45(14) . . ?
Ag9A Ag3 Ag4 108.2(3) . . ?
Ag1B Ag3 Ag4 76.1(8) . . ?
C7 Ag3 Ag1A 52.61(18) . . ?
C13 Ag3 Ag1A 128.68(18) . . ?
Ag4 Ag3 Ag1A 82.60(10) . . ?
C7 Ag3 Ag5 130.17(15) . . ?
C13 Ag3 Ag5 49.63(14) . . ?
Ag9A Ag3 Ag5 70.0(4) . . ?
Ag1B Ag3 Ag5 139.2(6) . . ?
Ag4 Ag3 Ag5 79.531(15) . . ?
Ag1A Ag3 Ag5 143.23(7) . . ?
C7 Ag3 Ag9 134.25(15) . . ?
C13 Ag3 Ag9 47.32(15) . . ?
Ag4 Ag3 Ag9 105.51(2) . . ?
Ag1A Ag3 Ag9 88.47(8) . . ?
Ag5 Ag3 Ag9 66.10(2) . . ?
C25 Ag4 C19 118.36(18) . . ?
C25 Ag4 C7 118.63(18) . . ?
C19 Ag4 C7 120.65(18) . . ?
C25 Ag4 C20 137.22(17) . . ?
C19 Ag4 C20 27.69(17) . . ?
C7 Ag4 C20 103.74(17) . . ?
C25 Ag4 Ag3 133.86(13) . . ?
C19 Ag4 Ag3 83.79(12) . . ?
C7 Ag4 Ag3 44.03(13) . . ?
C20 Ag4 Ag3 81.17(10) . . ?
C25 Ag4 Ag2 43.86(13) . . ?
C19 Ag4 Ag2 136.11(13) . . ?
C7 Ag4 Ag2 80.99(13) . . ?
C20 Ag4 Ag2 162.48(11) . . ?
Ag3 Ag4 Ag2 91.384(16) . . ?
C25 Ag4 Ag10 82.28(13) . . ?
C19 Ag4 Ag10 41.92(13) . . ?
C7 Ag4 Ag10 137.41(13) . . ?
C20 Ag4 Ag10 69.51(11) . . ?
Ag3 Ag4 Ag10 94.099(16) . . ?
Ag2 Ag4 Ag10 95.446(16) . . ?
C13 Ag5 O4 127.58(17) . . ?
C13 Ag5 C19 125.35(18) . . ?
O4 Ag5 C19 101.18(16) . . ?
C13 Ag5 O3 100.51(16) . . ?
O4 Ag5 O3 75.96(13) . . ?
C19 Ag5 O3 115.50(16) . . ?
C13 Ag5 Ag10 126.39(13) . . ?
O4 Ag5 Ag10 102.97(10) . . ?
C19 Ag5 Ag10 44.33(13) . . ?
O3 Ag5 Ag10 72.94(9) . . ?
C13 Ag5 Ag3 43.14(13) . . ?
O4 Ag5 Ag3 156.05(10) . . ?
C19 Ag5 Ag3 82.23(12) . . ?
O3 Ag5 Ag3 124.29(9) . . ?
Ag10 Ag5 Ag3 95.971(17) . . ?
C13 Ag5 Ag9A 36.8(4) . . ?
O4 Ag5 Ag9A 143.2(5) . . ?
C19 Ag5 Ag9A 112.8(3) . . ?
O3 Ag5 Ag9A 77.0(6) . . ?
Ag10 Ag5 Ag9A 92.2(2) . . ?
Ag3 Ag5 Ag9A 48.5(5) . . ?
C13 Ag5 Ag9 42.36(14) . . ?
O4 Ag5 Ag9 136.26(10) . . ?
C19 Ag5 Ag9 116.31(13) . . ?
O3 Ag5 Ag9 68.26(10) . . ?
Ag10 Ag5 Ag9 90.03(2) . . ?
Ag3 Ag5 Ag9 57.08(4) . . ?
O2 Ag6 C31 121.15(19) . . ?
O2 Ag6 C25 98.37(18) . . ?
C31 Ag6 C25 129.40(18) . . ?
O2 Ag6 O1 77.94(15) . . ?
C31 Ag6 O1 104.74(16) . . ?
C25 Ag6 O1 114.05(16) . . ?
O2 Ag6 Ag10 148.39(13) . . ?
C31 Ag6 Ag10 44.68(13) . . ?
C25 Ag6 Ag10 85.00(13) . . ?
O1 Ag6 Ag10 129.39(9) . . ?
O2 Ag6 Ag2 105.47(14) . . ?
C31 Ag6 Ag2 132.19(13) . . ?
C25 Ag6 Ag2 43.61(12) . . ?
O1 Ag6 Ag2 73.52(9) . . ?
Ag10 Ag6 Ag2 98.563(17) . . ?
O2 Ag6 Ag7 139.64(13) . . ?
C31 Ag6 Ag7 42.74(13) . . ?
C25 Ag6 Ag7 119.64(12) . . ?
O1 Ag6 Ag7 74.64(9) . . ?
Ag10 Ag6 Ag7 55.880(13) . . ?
Ag2 Ag6 Ag7 94.505(16) . . ?
C37 Ag7 C31 160.1(2) . . ?
C37 Ag7 Ag10 141.88(14) . . ?
C31 Ag7 Ag10 45.44(13) . . ?
C37 Ag7 Ag9 46.95(15) . . ?
C31 Ag7 Ag9 143.59(14) . . ?
Ag10 Ag7 Ag9 98.53(4) . . ?
C37 Ag7 Ag8 45.88(14) . . ?
C31 Ag7 Ag8 118.76(14) . . ?
Ag10 Ag7 Ag8 107.214(18) . . ?
Ag9 Ag7 Ag8 59.19(2) . . ?
C37 Ag7 Ag9A 51.4(4) . . ?
C31 Ag7 Ag9A 137.1(4) . . ?
Ag10 Ag7 Ag9A 92.7(4) . . ?
Ag8 Ag7 Ag9A 56.7(3) . . ?
C37 Ag7 Ag6 117.46(15) . . ?
C31 Ag7 Ag6 45.98(13) . . ?
Ag10 Ag7 Ag6 56.655(13) . . ?
Ag9 Ag7 Ag6 115.73(4) . . ?
Ag8 Ag7 Ag6 72.829(15) . . ?
Ag9A Ag7 Ag6 108.9(4) . . ?
C37 Ag8 C1 161.7(2) . . ?
C37 Ag8 C2 139.20(19) . . ?
C1 Ag8 C2 27.75(18) . . ?
C37 Ag8 Ag9 46.72(15) . . ?
C1 Ag8 Ag9 119.50(15) . . ?
C2 Ag8 Ag9 117.03(13) . . ?
C37 Ag8 Ag2 143.63(14) . . ?
C1 Ag8 Ag2 44.68(14) . . ?
C2 Ag8 Ag2 72.42(12) . . ?
Ag9 Ag8 Ag2 109.76(4) . . ?
C37 Ag8 Ag9A 56.4(6) . . ?
C1 Ag8 Ag9A 109.9(6) . . ?
C2 Ag8 Ag9A 109.4(5) . . ?
Ag2 Ag8 Ag9A 102.2(5) . . ?
C37 Ag8 Ag7 45.64(14) . . ?
C1 Ag8 Ag7 144.50(14) . . ?
C2 Ag8 Ag7 170.44(12) . . ?
Ag9 Ag8 Ag7 58.80(3) . . ?
Ag2 Ag8 Ag7 100.364(17) . . ?
Ag9A Ag8 Ag7 65.3(5) . . ?
C37 Ag9 C13 166.3(2) . . ?
C37 Ag9 O101 95.6(2) . . ?
C13 Ag9 O101 97.5(2) . . ?
C37 Ag9 C14 149.2(2) . . ?
C13 Ag9 C14 25.93(18) . . ?
O101 Ag9 C14 92.4(2) . . ?
C37 Ag9 Ag7 47.42(15) . . ?
C13 Ag9 Ag7 119.98(13) . . ?
O101 Ag9 Ag7 142.39(18) . . ?
C14 Ag9 Ag7 122.58(11) . . ?
C37 Ag9 Ag8 47.43(15) . . ?
C13 Ag9 Ag8 136.86(16) . . ?
O101 Ag9 Ag8 88.90(19) . . ?
C14 Ag9 Ag8 162.68(15) . . ?
Ag7 Ag9 Ag8 62.02(2) . . ?
C37 Ag9 Ag3 139.15(15) . . ?
C13 Ag9 Ag3 43.04(14) . . ?
O101 Ag9 Ag3 96.27(15) . . ?
C14 Ag9 Ag3 68.76(13) . . ?
Ag7 Ag9 Ag3 108.29(3) . . ?
Ag8 Ag9 Ag3 93.93(5) . . ?
C37 Ag9 Ag5 122.73(15) . . ?
C13 Ag9 Ag5 44.18(13) . . ?
O101 Ag9 Ag5 141.61(18) . . ?
C14 Ag9 Ag5 54.22(12) . . ?
Ag7 Ag9 Ag5 75.829(19) . . ?
Ag8 Ag9 Ag5 117.21(3) . . ?
Ag3 Ag9 Ag5 56.81(3) . . ?
C13 Ag9A O101 108.5(8) . . ?
C13 Ag9A C37 149.9(13) . . ?
O101 Ag9A C37 88.2(7) . . ?
C13 Ag9A Ag3 52.2(7) . . ?
O101 Ag9A Ag3 112.1(11) . . ?
C37 Ag9A Ag3 144.2(6) . . ?
C13 Ag9A C14 25.8(3) . . ?
O101 Ag9A C14 96.9(5) . . ?
C37 Ag9A C14 130.8(11) . . ?
Ag3 Ag9A C14 77.7(6) . . ?
C13 Ag9A Ag8 153.3(10) . . ?
O101 Ag9A Ag8 89.5(4) . . ?
C37 Ag9A Ag8 45.4(3) . . ?
Ag3 Ag9A Ag8 103.3(7) . . ?
C14 Ag9A Ag8 172.7(9) . . ?
C13 Ag9A Ag7 116.8(6) . . ?
O101 Ag9A Ag7 130.0(9) . . ?
C37 Ag9A Ag7 41.8(4) . . ?
Ag3 Ag9A Ag7 111.8(4) . . ?
C14 Ag9A Ag7 114.8(7) . . ?
Ag8 Ag9A Ag7 57.9(3) . . ?
C13 Ag9A Ag5 44.9(3) . . ?
O101 Ag9A Ag5 152.3(6) . . ?
C37 Ag9A Ag5 112.6(8) . . ?
Ag3 Ag9A Ag5 61.5(3) . . ?
C14 Ag9A Ag5 55.8(3) . . ?
Ag8 Ag9A Ag5 118.1(4) . . ?
Ag7 Ag9A Ag5 72.8(3) . . ?
C19 Ag10 C31 178.1(2) . . ?
C19 Ag10 Ag7 129.64(14) . . ?
C31 Ag10 Ag7 49.03(15) . . ?
C19 Ag10 Ag5 53.05(14) . . ?
C31 Ag10 Ag5 126.52(15) . . ?
Ag7 Ag10 Ag5 82.244(16) . . ?
C19 Ag10 Ag6 126.50(14) . . ?
C31 Ag10 Ag6 52.16(14) . . ?
Ag7 Ag10 Ag6 67.466(15) . . ?
Ag5 Ag10 Ag6 134.454(19) . . ?
C19 Ag10 Ag4 49.78(14) . . ?
C31 Ag10 Ag4 128.58(14) . . ?
Ag7 Ag10 Ag4 105.742(17) . . ?
Ag5 Ag10 Ag4 78.941(15) . . ?
Ag6 Ag10 Ag4 77.707(15) . . ?
C44 O1 Ag6 127.6(4) . . ?
C46 O2 Ag6 129.6(4) . . ?
C49 O3 Ag5 127.6(3) . . ?
C51 O4 Ag5 132.1(4) . . ?
C54 O5 Ag1A 126.9(4) . . ?
C54 O5 Ag1B 131.4(7) . . ?
C56 O6 Ag1A 123.5(4) . . ?
C2 C1 Ag2 177.9(5) . . ?
C2 C1 Ag1B 104.5(11) . . ?
Ag2 C1 Ag1B 77.3(10) . . ?
C2 C1 Ag8 92.9(4) . . ?
Ag2 C1 Ag8 85.71(19) . . ?
Ag1B C1 Ag8 101.5(5) . . ?
C2 C1 Ag1A 96.4(4) . . ?
Ag2 C1 Ag1A 85.4(2) . . ?
Ag8 C1 Ag1A 101.9(2) . . ?
C1 C2 C3 174.8(6) . . ?
C1 C2 Ag8 59.4(3) . . ?
C3 C2 Ag8 122.8(4) . . ?
C2 C3 C4 109.6(5) . . ?
C2 C3 C6 108.9(5) . . ?
C4 C3 C6 112.2(7) . . ?
C2 C3 C5 108.4(5) . . ?
C4 C3 C5 109.4(6) . . ?
C6 C3 C5 108.2(6) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 Ag3 171.1(5) . . ?
C8 C7 Ag1B 101.9(6) . . ?
Ag3 C7 Ag1B 85.8(5) . . ?
C8 C7 Ag4 99.0(4) . . ?
Ag3 C7 Ag4 83.10(18) . . ?
Ag1B C7 Ag4 104.3(10) . . ?
C8 C7 Ag1A 103.5(4) . . ?
Ag3 C7 Ag1A 83.6(2) . . ?
Ag4 C7 Ag1A 110.9(2) . . ?
C7 C8 C9 175.9(6) . . ?
C8 C9 C11 109.0(5) . . ?
C8 C9 C10 108.5(5) . . ?
C11 C9 C10 111.9(7) . . ?
C8 C9 C12 108.3(5) . . ?
C11 C9 C12 109.1(6) . . ?
C10 C9 C12 109.9(7) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag9A 109.0(8) . . ?
C14 C13 Ag3 167.3(5) . . ?
Ag9A C13 Ag3 79.4(8) . . ?
C14 C13 Ag9 99.7(4) . . ?
Ag3 C13 Ag9 89.6(2) . . ?
C14 C13 Ag5 100.6(4) . . ?
Ag9A C13 Ag5 98.3(5) . . ?
Ag3 C13 Ag5 87.23(18) . . ?
Ag9 C13 Ag5 93.47(19) . . ?
C13 C14 C15 174.7(6) . . ?
C13 C14 Ag9A 45.2(7) . . ?
C15 C14 Ag9A 134.4(7) . . ?
C13 C14 Ag9 54.3(4) . . ?
C15 C14 Ag9 126.1(4) . . ?
C14 C15 C17 107.8(6) . . ?
C14 C15 C18 109.1(5) . . ?
C17 C15 C18 111.0(8) . . ?
C14 C15 C16 109.6(6) . . ?
C17 C15 C16 112.4(8) . . ?
C18 C15 C16 106.9(7) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C15 C17 H17A 109.5 . . ?
C15 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C15 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 Ag10 173.1(4) . . ?
C20 C19 Ag4 88.3(3) . . ?
Ag10 C19 Ag4 88.30(19) . . ?
C20 C19 Ag5 104.2(4) . . ?
Ag10 C19 Ag5 82.62(17) . . ?
Ag4 C19 Ag5 108.4(2) . . ?
C19 C20 C21 172.8(5) . . ?
C19 C20 Ag4 64.0(3) . . ?
C21 C20 Ag4 122.9(3) . . ?
C20 C21 C24 109.5(5) . . ?
C20 C21 C22 109.3(4) . . ?
C24 C21 C22 109.5(5) . . ?
C20 C21 C23 107.4(5) . . ?
C24 C21 C23 110.4(5) . . ?
C22 C21 C23 110.7(5) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 Ag2 175.0(5) . . ?
C26 C25 Ag4 99.9(4) . . ?
Ag2 C25 Ag4 84.98(18) . . ?
C26 C25 Ag6 93.7(4) . . ?
Ag2 C25 Ag6 84.21(18) . . ?
Ag4 C25 Ag6 107.0(2) . . ?
C25 C26 C27 177.5(5) . . ?
C26 C27 C30 109.1(5) . . ?
C26 C27 C28 109.5(5) . . ?
C30 C27 C28 110.4(6) . . ?
C26 C27 C29 109.0(5) . . ?
C30 C27 C29 109.8(6) . . ?
C28 C27 C29 109.0(6) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 Ag10 168.7(5) . . ?
C32 C31 Ag7 105.7(4) . . ?
Ag10 C31 Ag7 85.53(18) . . ?
C32 C31 Ag6 97.3(4) . . ?
Ag10 C31 Ag6 83.16(17) . . ?
Ag7 C31 Ag6 91.28(19) . . ?
C31 C32 C33 173.3(5) . . ?
C32 C33 C34 110.3(5) . . ?
C32 C33 C35 108.7(5) . . ?
C34 C33 C35 111.0(5) . . ?
C32 C33 C36 107.6(5) . . ?
C34 C33 C36 110.7(6) . . ?
C35 C33 C36 108.4(5) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 Ag9 137.1(5) . . ?
C38 C37 Ag7 120.5(5) . . ?
Ag9 C37 Ag7 85.62(19) . . ?
C38 C37 Ag8 124.7(5) . . ?
Ag9 C37 Ag8 85.8(2) . . ?
Ag7 C37 Ag8 88.47(19) . . ?
C38 C37 Ag9A 141.6(6) . . ?
Ag7 C37 Ag9A 86.9(3) . . ?
Ag8 C37 Ag9A 78.2(5) . . ?
C37 C38 C39 179.0(7) . . ?
C38 C39 C40 108.8(6) . . ?
C38 C39 C41 108.7(6) . . ?
C40 C39 C41 109.5(8) . . ?
C38 C39 C42 108.2(6) . . ?
C40 C39 C42 111.0(7) . . ?
C41 C39 C42 110.6(8) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
F12 C43 F11 110.5(11) . . ?
F11A C43 F12A 104.4(8) . . ?
F11A C43 F10A 107.7(8) . . ?
F12A C43 F10A 103.7(8) . . ?
F12 C43 F10 100.1(12) . . ?
F11 C43 F10 106.9(11) . . ?
F12 C43 C44 114.9(10) . . ?
F11A C43 C44 115.3(6) . . ?
F11 C43 C44 107.4(10) . . ?
F12A C43 C44 110.3(7) . . ?
F10A C43 C44 114.3(7) . . ?
F10 C43 C44 116.8(14) . . ?
O1 C44 C45 128.6(6) . . ?
O1 C44 C43 114.0(5) . . ?
C45 C44 C43 117.3(5) . . ?
C46 C45 C44 125.1(6) . . ?
C46 C45 H45 117.5 . . ?
C44 C45 H45 117.5 . . ?
O2 C46 C45 130.6(6) . . ?
O2 C46 C47 113.1(7) . . ?
C45 C46 C47 116.3(7) . . ?
F2 C47 F1 105.7(9) . . ?
F2 C47 F3 103.6(11) . . ?
F1 C47 F3 103.3(9) . . ?
F2 C47 C46 114.4(8) . . ?
F1 C47 C46 117.0(8) . . ?
F3 C47 C46 111.5(7) . . ?
F4 C48 F5 109.7(7) . . ?
F4 C48 F6 103.6(8) . . ?
F5 C48 F6 101.9(7) . . ?
F4 C48 C49 113.8(5) . . ?
F5 C48 C49 116.1(6) . . ?
F6 C48 C49 110.3(6) . . ?
O3 C49 C50 128.6(5) . . ?
O3 C49 C48 114.4(5) . . ?
C50 C49 C48 116.9(5) . . ?
C49 C50 C51 124.7(5) . . ?
C49 C50 H50 117.7 . . ?
C51 C50 H50 117.7 . . ?
O4 C51 C50 129.6(5) . . ?
O4 C51 C52 113.6(5) . . ?
C50 C51 C52 116.8(5) . . ?
F7 C52 F9 105.8(7) . . ?
F7 C52 F8 107.5(6) . . ?
F9 C52 F8 105.7(6) . . ?
F7 C52 C51 110.9(6) . . ?
F9 C52 C51 111.2(6) . . ?
F8 C52 C51 115.1(6) . . ?
F15 C53 F13 108.5(7) . . ?
F15 C53 F14 105.5(7) . . ?
F13 C53 F14 102.0(7) . . ?
F15 C53 C54 117.3(6) . . ?
F13 C53 C54 113.5(6) . . ?
F14 C53 C54 108.7(6) . . ?
O5 C54 C55 129.9(6) . . ?
O5 C54 C53 114.3(5) . . ?
C55 C54 C53 115.8(5) . . ?
C56 C55 C54 124.0(6) . . ?
C56 C55 H55 118.0 . . ?
C54 C55 H55 118.0 . . ?
O6 C56 C55 130.4(6) . . ?
O6 C56 C57 111.7(5) . . ?
C55 C56 C57 117.9(5) . . ?
F16 C57 F17 107.6(6) . . ?
F16 C57 F18 107.3(6) . . ?
F17 C57 F18 105.1(6) . . ?
F16 C57 C56 111.0(6) . . ?
F17 C57 C56 114.8(5) . . ?
F18 C57 C56 110.6(6) . . ?
C101 O101 Ag9A 146.0(9) . . ?
C101 O101 Ag9 135.3(6) . . ?

_refine_diff_density_max         0.979
_refine_diff_density_min         -0.903
_refine_diff_density_rms         0.113

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex2
_database_code_depnum_ccdc_archive 'CCDC 1584342'
_audit_update_record             
;
2018-01-15 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C70 H84 Ag12 F24 O10'
_chemical_formula_weight         2835.81

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/n'
_space_group_name_Hall           '-P 2yn'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   15.9191(12)
_cell_length_b                   18.5105(14)
_cell_length_c                   16.4798(13)
_cell_angle_alpha                90
_cell_angle_beta                 106.631(2)
_cell_angle_gamma                90
_cell_volume                     4653.0(6)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9986
_cell_measurement_theta_min      3.0461
_cell_measurement_theta_max      28.2877

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.024
_exptl_crystal_F_000             2728
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.315
_exptl_crystal_size_mid          0.267
_exptl_crystal_size_min          0.195
_exptl_absorpt_coefficient_mu    2.559
_shelx_estimated_absorpt_T_min   0.499
_shelx_estimated_absorpt_T_max   0.635
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.5961
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            31150
_diffrn_reflns_av_unetI/netI     0.0304
_diffrn_reflns_av_R_equivalents  0.0337
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_theta_min         2.835
_diffrn_reflns_theta_max         25.026
_diffrn_reflns_theta_full        25.026
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measured_fraction_theta_full 0.991
_diffrn_reflns_Laue_measured_fraction_max 0.991
_diffrn_reflns_Laue_measured_fraction_full 0.991
_diffrn_reflns_point_group_measured_fraction_max 0.991
_diffrn_reflns_point_group_measured_fraction_full 0.991
_reflns_number_total             8131
_reflns_number_gt                7373
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0151P)²+111.7992P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         8131
_refine_ls_number_parameters     571
_refine_ls_number_restraints     339
_refine_ls_R_factor_all          0.0634
_refine_ls_R_factor_gt           0.0588
_refine_ls_wR_factor_ref         0.1584
_refine_ls_wR_factor_gt          0.1559
_refine_ls_goodness_of_fit_ref   1.156
_refine_ls_restrained_S_all      1.142
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.40686(5) 0.42303(5) -0.06690(5) 0.0366(2) Uani 1 1 d . . . . .
Ag2 Ag 0.33596(6) 0.54530(5) -0.17675(5) 0.0393(2) Uani 1 1 d . . . . .
Ag3 Ag 0.44973(6) 0.55860(5) 0.14590(6) 0.0439(2) Uani 1 1 d . . . . .
Ag4 Ag 0.32300(6) 0.44730(5) 0.06775(5) 0.0408(2) Uani 1 1 d . . . . .
Ag5 Ag 0.49377(6) 0.41424(5) 0.20841(6) 0.0424(2) Uani 1 1 d . . . . .
Ag6 Ag 0.54529(6) 0.35360(5) 0.06825(5) 0.0435(2) Uani 1 1 d . . . . .
F1 F 0.4600(7) 0.2010(5) 0.0540(9) 0.099(4) Uani 1 1 d . . . . .
F2 F 0.3613(7) 0.1342(5) 0.0765(8) 0.095(3) Uani 1 1 d . . . . .
F3 F 0.4488(8) 0.1933(7) 0.1776(9) 0.118(4) Uani 1 1 d . . . . .
F4 F 0.0444(6) 0.3016(8) 0.0064(8) 0.111(4) Uani 1 1 d . . . . .
F5 F 0.0925(7) 0.2168(6) 0.0920(12) 0.144(6) Uani 1 1 d . . . . .
F6 F 0.0751(8) 0.3218(8) 0.1325(9) 0.121(5) Uani 1 1 d . . . . .
F7 F 0.9298(6) 0.5569(7) 0.4113(8) 0.113(4) Uani 1 1 d . . . . .
F8 F 0.8778(7) 0.5180(6) 0.5070(6) 0.091(3) Uani 1 1 d . . . . .
F9 F 0.9160(7) 0.4444(6) 0.4262(7) 0.102(4) Uani 1 1 d . . . . .
F10A F 0.4981(11) 0.604(2) 0.338(2) 0.092(16) Uani 0.39(5) 1 d D . P A 1
F11A F 0.598(3) 0.610(3) 0.4583(12) 0.106(18) Uani 0.39(5) 1 d D . P A 1
F12A F 0.599(3) 0.6849(11) 0.358(4) 0.12(2) Uani 0.39(5) 1 d D . P A 1
F10B F 0.531(2) 0.5637(16) 0.399(2) 0.18(2) Uani 0.61(5) 1 d D . P A 2
F11B F 0.6245(16) 0.6518(16) 0.4397(15) 0.103(11) Uani 0.61(5) 1 d D . P A 2
F12B F 0.531(2) 0.654(2) 0.3137(12) 0.14(2) Uani 0.61(5) 1 d D . P A 2
O5 O 0.3781(5) 0.3198(4) 0.0713(6) 0.048(2) Uani 1 1 d . . . . .
O6 O 0.2011(6) 0.3721(5) 0.0644(7) 0.057(2) Uani 1 1 d . . . . .
O7 O 0.6077(5) 0.5480(5) 0.2600(5) 0.0444(19) Uani 1 1 d . . . . .
O8 O 0.7834(5) 0.4818(5) 0.2946(6) 0.057(2) Uani 1 1 d . . . . .
C1 C 0.2973(7) 0.4846(6) -0.0703(7) 0.040(3) Uani 1 1 d D U . . .
C2 C 0.2264(6) 0.5120(6) -0.0799(7) 0.040(2) Uani 1 1 d D U . . .
C3 C 0.1383(8) 0.5450(7) -0.0908(8) 0.060(3) Uani 1 1 d D U . . .
C4 C 0.1235(13) 0.5588(11) -0.0053(10) 0.110(7) Uani 1 1 d D U . . .
H4A H 0.0655 0.5805 -0.0134 0.166 Uiso 1 1 calc R U . . .
H4B H 0.1268 0.5131 0.0254 0.166 Uiso 1 1 calc R U . . .
H4C H 0.1686 0.5920 0.0275 0.166 Uiso 1 1 calc R U . . .
C5 C 0.0705(11) 0.4916(12) -0.1413(14) 0.142(9) Uani 1 1 d D U . . .
H5A H 0.0116 0.5115 -0.1498 0.213 Uiso 1 1 calc R U . . .
H5B H 0.0806 0.4830 -0.1965 0.213 Uiso 1 1 calc R U . . .
H5C H 0.0757 0.4459 -0.1102 0.213 Uiso 1 1 calc R U . . .
C6 C 0.1335(13) 0.6152(9) -0.1393(12) 0.122(8) Uani 1 1 d D U . . .
H6A H 0.0759 0.6375 -0.1470 0.184 Uiso 1 1 calc R U . . .
H6B H 0.1793 0.6482 -0.1075 0.184 Uiso 1 1 calc R U . . .
H6C H 0.1421 0.6054 -0.1949 0.184 Uiso 1 1 calc R U . . .
C7 C 0.3836(7) 0.4815(6) 0.2048(8) 0.039(2) Uani 1 1 d D U . . .
C8 C 0.3311(8) 0.4915(6) 0.2434(8) 0.045(3) Uani 1 1 d D U . . .
C9 C 0.2627(10) 0.5076(9) 0.2868(11) 0.101(4) Uani 1 1 d D U . . .
C10 C 0.2041(12) 0.4437(10) 0.2810(12) 0.101(4) Uani 1 1 d D U . . .
H10A H 0.1594 0.4545 0.3095 0.151 Uiso 1 1 calc R U . . .
H10B H 0.1756 0.4325 0.2213 0.151 Uiso 1 1 calc R U . . .
H10C H 0.2389 0.4020 0.3082 0.151 Uiso 1 1 calc R U . . .
C11 C 0.2052(14) 0.5733(11) 0.2464(14) 0.143(8) Uani 1 1 d D U . . .
H11A H 0.2425 0.6159 0.2497 0.215 Uiso 1 1 calc R U . . .
H11B H 0.1748 0.5627 0.1870 0.215 Uiso 1 1 calc R U . . .
H11C H 0.1619 0.5827 0.2771 0.215 Uiso 1 1 calc R U . . .
C12 C 0.3104(12) 0.5273(11) 0.3781(10) 0.110(6) Uani 1 1 d D U . . .
H12A H 0.3479 0.5695 0.3788 0.165 Uiso 1 1 calc R U . . .
H12B H 0.2674 0.5388 0.4084 0.165 Uiso 1 1 calc R U . . .
H12C H 0.3465 0.4865 0.4057 0.165 Uiso 1 1 calc R U . . .
C13 C 0.3961(7) 0.6501(6) -0.2029(7) 0.038(2) Uani 1 1 d . U . . .
C14 C 0.3481(7) 0.6972(6) -0.2411(6) 0.036(2) Uani 1 1 d . U . . .
C15 C 0.2903(8) 0.7531(7) -0.2892(7) 0.053(3) Uani 1 1 d D U . . .
C16A C 0.3395(13) 0.7961(11) -0.3402(15) 0.083(7) Uani 0.76(3) 1 d D U P B 1
H16A H 0.3010 0.8338 -0.3727 0.124 Uiso 0.76(3) 1 calc R U P B 1
H16B H 0.3915 0.8185 -0.3016 0.124 Uiso 0.76(3) 1 calc R U P B 1
H16C H 0.3576 0.7637 -0.3791 0.124 Uiso 0.76(3) 1 calc R U P B 1
C17A C 0.2104(12) 0.7178(12) -0.3519(13) 0.077(7) Uani 0.76(3) 1 d D U P B 1
H17A H 0.1717 0.7555 -0.3841 0.116 Uiso 0.76(3) 1 calc R U P B 1
H17B H 0.2300 0.6866 -0.3910 0.116 Uiso 0.76(3) 1 calc R U P B 1
H17C H 0.1784 0.6888 -0.3207 0.116 Uiso 0.76(3) 1 calc R U P B 1
C18A C 0.258(2) 0.8028(13) -0.2326(14) 0.119(11) Uani 0.76(3) 1 d D U P B 1
H18A H 0.2195 0.8395 -0.2670 0.178 Uiso 0.76(3) 1 calc R U P B 1
H18B H 0.2253 0.7748 -0.2011 0.178 Uiso 0.76(3) 1 calc R U P B 1
H18C H 0.3081 0.8264 -0.1926 0.178 Uiso 0.76(3) 1 calc R U P B 1
C16B C 0.289(5) 0.770(4) -0.381(2) 0.090(16) Uani 0.24(3) 1 d D U P B 2
H16D H 0.2463 0.8083 -0.4035 0.135 Uiso 0.24(3) 1 calc R U P B 2
H16E H 0.3470 0.7849 -0.3827 0.135 Uiso 0.24(3) 1 calc R U P B 2
H16F H 0.2712 0.7261 -0.4158 0.135 Uiso 0.24(3) 1 calc R U P B 2
C17B C 0.1930(19) 0.746(4) -0.292(5) 0.088(15) Uani 0.24(3) 1 d D U P B 2
H17D H 0.1596 0.7858 -0.3257 0.132 Uiso 0.24(3) 1 calc R U P B 2
H17E H 0.1700 0.6999 -0.3183 0.132 Uiso 0.24(3) 1 calc R U P B 2
H17F H 0.1875 0.7481 -0.2345 0.132 Uiso 0.24(3) 1 calc R U P B 2
C18B C 0.321(4) 0.824(2) -0.241(4) 0.075(15) Uani 0.24(3) 1 d D U P B 2
H18D H 0.2840 0.8639 -0.2707 0.113 Uiso 0.24(3) 1 calc R U P B 2
H18E H 0.3155 0.8200 -0.1836 0.113 Uiso 0.24(3) 1 calc R U P B 2
H18F H 0.3820 0.8332 -0.2388 0.113 Uiso 0.24(3) 1 calc R U P B 2
C25 C 0.5100(7) 0.3558(5) -0.0708(6) 0.032(2) Uani 1 1 d . U . . .
C26 C 0.5566(7) 0.3093(5) -0.0846(6) 0.033(2) Uani 1 1 d D U . . .
C27 C 0.6067(8) 0.2469(6) -0.1057(7) 0.048(3) Uani 1 1 d D U . . .
C28 C 0.6621(13) 0.2745(9) -0.1608(14) 0.098(6) Uani 1 1 d D U . . .
H28A H 0.6953 0.2342 -0.1751 0.146 Uiso 1 1 calc R U . . .
H28B H 0.6238 0.2954 -0.2129 0.146 Uiso 1 1 calc R U . . .
H28C H 0.7029 0.3114 -0.1299 0.146 Uiso 1 1 calc R U . . .
C29 C 0.5408(12) 0.1931(8) -0.1576(13) 0.091(5) Uani 1 1 d D U . . .
H29A H 0.5721 0.1517 -0.1722 0.136 Uiso 1 1 calc R U . . .
H29B H 0.5023 0.1764 -0.1244 0.136 Uiso 1 1 calc R U . . .
H29C H 0.5056 0.2164 -0.2096 0.136 Uiso 1 1 calc R U . . .
C30 C 0.6601(15) 0.2096(11) -0.0231(11) 0.112(7) Uani 1 1 d D U . . .
H30A H 0.6928 0.1688 -0.0371 0.168 Uiso 1 1 calc R U . . .
H30B H 0.7012 0.2443 0.0121 0.168 Uiso 1 1 calc R U . . .
H30C H 0.6201 0.1919 0.0079 0.168 Uiso 1 1 calc R U . . .
C31 C 0.4029(9) 0.1968(7) 0.0969(11) 0.060(4) Uani 1 1 d . U . . .
C32 C 0.3422(8) 0.2644(6) 0.0837(7) 0.040(2) Uani 1 1 d . U . . .
C33 C 0.2578(8) 0.2543(7) 0.0878(9) 0.050(3) Uani 1 1 d . U . . .
H33 H 0.2418 0.2067 0.0991 0.060 Uiso 1 1 calc R U . . .
C34 C 0.1946(8) 0.3069(7) 0.0768(8) 0.045(3) Uani 1 1 d . U . . .
C35 C 0.1035(9) 0.2851(8) 0.0778(10) 0.059(3) Uani 1 1 d . U . . .
C36 C 0.8794(9) 0.5056(8) 0.4282(9) 0.060(4) Uani 1 1 d . U . . .
C37 C 0.7867(7) 0.5100(7) 0.3624(7) 0.043(3) Uani 1 1 d . U . . .
C38 C 0.7239(8) 0.5479(7) 0.3884(8) 0.048(3) Uani 1 1 d . U . . .
H38 H 0.7382 0.5635 0.4457 0.058 Uiso 1 1 calc R U . . .
C39 C 0.6418(8) 0.5640(7) 0.3356(7) 0.043(3) Uani 1 1 d . U . . .
C40 C 0.5849(8) 0.6119(8) 0.3730(7) 0.066(4) Uani 1 1 d D U . . .
C101 C 0.354(7) 0.348(5) 0.352(7) 0.28(5) Uiso 0.50(2) 1 d D . P C 1
O101 O 0.400(5) 0.285(4) 0.339(4) 0.25(2) Uiso 0.50(2) 1 d D . P C 1
C102 C 0.531(4) 0.408(3) 0.401(4) 0.14(2) Uiso 0.50(2) 1 d D . P C 2
O102 O 0.486(4) 0.353(3) 0.344(4) 0.25(2) Uiso 0.50(2) 1 d D . P C 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C1 2.071(10) . ?
Ag1 C25 2.076(11) . ?
Ag1 Ag2 2.9162(12) . ?
Ag1 Ag4 2.9331(12) . ?
Ag1 Ag6 2.9426(12) . ?
Ag1 Ag3 2.9536(12) 3_665 ?
Ag2 C13 2.259(11) . ?
Ag2 C1 2.311(11) . ?
Ag2 O8 2.349(8) 3_665 ?
Ag2 O7 2.525(8) 3_665 ?
Ag2 Ag6 2.8876(13) 3_665 ?
Ag2 Ag5 2.9983(13) 3_665 ?
Ag3 C7 2.162(11) . ?
Ag3 C25 2.216(10) 3_665 ?
Ag3 C26 2.637(10) 3_665 ?
Ag3 Ag5 2.8775(13) . ?
Ag3 Ag4 2.9131(13) . ?
Ag3 Ag1 2.9535(12) 3_665 ?
Ag4 C7 2.277(12) . ?
Ag4 C1 2.299(12) . ?
Ag4 O6 2.376(9) . ?
Ag4 O5 2.513(8) . ?
Ag4 Ag5 3.0872(13) . ?
Ag5 C7 2.137(11) . ?
Ag5 C13 2.143(11) 3_665 ?
Ag5 O102 2.54(7) . ?
Ag5 Ag6 2.8900(13) . ?
Ag5 Ag2 2.9983(13) 3_665 ?
Ag6 C13 2.148(11) 3_665 ?
Ag6 C25 2.198(10) . ?
Ag6 C26 2.703(10) . ?
Ag6 Ag2 2.8876(13) 3_665 ?
F1 C31 1.303(18) . ?
F2 C31 1.329(16) . ?
F3 C31 1.323(19) . ?
F4 C35 1.315(18) . ?
F5 C35 1.306(17) . ?
F6 C35 1.310(18) . ?
F7 C36 1.324(19) . ?
F8 C36 1.325(18) . ?
F9 C36 1.279(17) . ?
F10A C40 1.344(17) . ?
F11A C40 1.360(18) . ?
F12A C40 1.401(17) . ?
F10B C40 1.385(17) . ?
F11B C40 1.324(16) . ?
F12B C40 1.356(16) . ?
O5 C32 1.219(13) . ?
O6 C34 1.233(15) . ?
O7 C39 1.244(14) . ?
O7 Ag2 2.525(8) 3_665 ?
O8 C37 1.221(15) . ?
O8 Ag2 2.349(8) 3_665 ?
C1 C2 1.205(12) . ?
C2 C3 1.492(12) . ?
C3 C4 1.516(15) . ?
C3 C6 1.517(15) . ?
C3 C5 1.524(16) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.201(13) . ?
C8 C9 1.495(14) . ?
C9 C10 1.493(16) . ?
C9 C12 1.522(16) . ?
C9 C11 1.553(17) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.209(15) . ?
C13 Ag5 2.143(11) 3_665 ?
C13 Ag6 2.148(11) 3_665 ?
C14 C15 1.459(15) . ?
C15 C18A 1.502(16) . ?
C15 C16A 1.528(16) . ?
C15 C18B 1.54(2) . ?
C15 C17A 1.537(15) . ?
C15 C16B 1.538(19) . ?
C15 C17B 1.54(2) . ?
C16A H16A 0.9800 . ?
C16A H16B 0.9800 . ?
C16A H16C 0.9800 . ?
C17A H17A 0.9800 . ?
C17A H17B 0.9800 . ?
C17A H17C 0.9800 . ?
C18A H18A 0.9800 . ?
C18A H18B 0.9800 . ?
C18A H18C 0.9800 . ?
C16B H16D 0.9800 . ?
C16B H16E 0.9800 . ?
C16B H16F 0.9800 . ?
C17B H17D 0.9800 . ?
C17B H17E 0.9800 . ?
C17B H17F 0.9800 . ?
C18B H18D 0.9800 . ?
C18B H18E 0.9800 . ?
C18B H18F 0.9800 . ?
C25 C26 1.199(14) . ?
C25 Ag3 2.216(10) 3_665 ?
C26 C27 1.500(12) . ?
C26 Ag3 2.637(10) 3_665 ?
C27 C29 1.521(15) . ?
C27 C28 1.525(14) . ?
C27 C30 1.546(14) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.557(17) . ?
C32 C33 1.378(17) . ?
C33 C34 1.375(18) . ?
C33 H33 0.9500 . ?
C34 C35 1.509(18) . ?
C36 C37 1.563(15) . ?
C37 C38 1.386(18) . ?
C38 C39 1.381(16) . ?
C38 H38 0.9500 . ?
C39 C40 1.518(18) . ?
C101 O101 1.44(2) . ?
C102 O102 1.43(2) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Ag1 C25 175.3(4) . . ?
C1 Ag1 Ag2 51.9(3) . . ?
C25 Ag1 Ag2 128.0(3) . . ?
C1 Ag1 Ag4 51.2(3) . . ?
C25 Ag1 Ag4 130.6(3) . . ?
Ag2 Ag1 Ag4 99.89(3) . . ?
C1 Ag1 Ag6 134.7(3) . . ?
C25 Ag1 Ag6 48.2(3) . . ?
Ag2 Ag1 Ag6 151.86(4) . . ?
Ag4 Ag1 Ag6 84.18(3) . . ?
C1 Ag1 Ag3 132.5(3) . 3_665 ?
C25 Ag1 Ag3 48.5(3) . 3_665 ?
Ag2 Ag1 Ag3 81.24(3) . 3_665 ?
Ag4 Ag1 Ag3 153.17(4) . 3_665 ?
Ag6 Ag1 Ag3 82.99(3) . 3_665 ?
C13 Ag2 C1 141.5(4) . . ?
C13 Ag2 O8 108.2(4) . 3_665 ?
C1 Ag2 O8 101.3(4) . 3_665 ?
C13 Ag2 O7 104.4(4) . 3_665 ?
C1 Ag2 O7 107.0(3) . 3_665 ?
O8 Ag2 O7 74.6(3) 3_665 3_665 ?
C13 Ag2 Ag6 47.4(3) . 3_665 ?
C1 Ag2 Ag6 96.6(3) . 3_665 ?
O8 Ag2 Ag6 151.8(2) 3_665 3_665 ?
O7 Ag2 Ag6 120.55(18) 3_665 3_665 ?
C13 Ag2 Ag1 132.5(3) . . ?
C1 Ag2 Ag1 44.9(3) . . ?
O8 Ag2 Ag1 115.2(3) 3_665 . ?
O7 Ag2 Ag1 70.83(19) 3_665 . ?
Ag6 Ag2 Ag1 92.87(3) 3_665 . ?
C13 Ag2 Ag5 45.5(3) . 3_665 ?
C1 Ag2 Ag5 134.8(3) . 3_665 ?
O8 Ag2 Ag5 117.8(2) 3_665 3_665 ?
O7 Ag2 Ag5 66.23(19) 3_665 3_665 ?
Ag6 Ag2 Ag5 58.78(3) 3_665 3_665 ?
Ag1 Ag2 Ag5 95.35(3) . 3_665 ?
C7 Ag3 C25 168.3(4) . 3_665 ?
C7 Ag3 C26 144.6(4) . 3_665 ?
C25 Ag3 C26 26.9(4) 3_665 3_665 ?
C7 Ag3 Ag5 47.6(3) . . ?
C25 Ag3 Ag5 141.7(3) 3_665 . ?
C26 Ag3 Ag5 167.7(2) 3_665 . ?
C7 Ag3 Ag4 50.7(3) . . ?
C25 Ag3 Ag4 122.2(3) 3_665 . ?
C26 Ag3 Ag4 122.7(2) 3_665 . ?
Ag5 Ag3 Ag4 64.43(3) . . ?
C7 Ag3 Ag1 144.2(3) . 3_665 ?
C25 Ag3 Ag1 44.6(3) 3_665 3_665 ?
C26 Ag3 Ag1 71.0(2) 3_665 3_665 ?
Ag5 Ag3 Ag1 97.17(4) . 3_665 ?
Ag4 Ag3 Ag1 114.29(4) . 3_665 ?
C7 Ag4 C1 143.4(4) . . ?
C7 Ag4 O6 107.3(4) . . ?
C1 Ag4 O6 103.9(4) . . ?
C7 Ag4 O5 101.1(3) . . ?
C1 Ag4 O5 105.5(4) . . ?
O6 Ag4 O5 74.2(3) . . ?
C7 Ag4 Ag3 47.3(3) . . ?
C1 Ag4 Ag3 97.5(3) . . ?
O6 Ag4 Ag3 151.9(2) . . ?
O5 Ag4 Ag3 117.45(19) . . ?
C7 Ag4 Ag1 129.6(3) . . ?
C1 Ag4 Ag1 44.6(3) . . ?
O6 Ag4 Ag1 116.0(2) . . ?
O5 Ag4 Ag1 69.0(2) . . ?
Ag3 Ag4 Ag1 92.02(4) . . ?
C7 Ag4 Ag5 43.8(3) . . ?
C1 Ag4 Ag5 132.2(3) . . ?
O6 Ag4 Ag5 116.0(2) . . ?
O5 Ag4 Ag5 64.5(2) . . ?
Ag3 Ag4 Ag5 57.22(3) . . ?
Ag1 Ag4 Ag5 92.53(3) . . ?
C7 Ag5 C13 175.7(4) . 3_665 ?
C7 Ag5 O102 92.3(15) . . ?
C13 Ag5 O102 91.9(15) 3_665 . ?
C7 Ag5 Ag3 48.4(3) . . ?
C13 Ag5 Ag3 128.3(3) 3_665 . ?
O102 Ag5 Ag3 131.5(14) . . ?
C7 Ag5 Ag6 128.5(3) . . ?
C13 Ag5 Ag6 47.7(3) 3_665 . ?
O102 Ag5 Ag6 128.6(14) . . ?
Ag3 Ag5 Ag6 99.81(4) . . ?
C7 Ag5 Ag2 128.7(3) . 3_665 ?
C13 Ag5 Ag2 48.7(3) 3_665 3_665 ?
O102 Ag5 Ag2 122.5(15) . 3_665 ?
Ag3 Ag5 Ag2 81.11(3) . 3_665 ?
Ag6 Ag5 Ag2 58.70(3) . 3_665 ?
C7 Ag5 Ag4 47.5(3) . . ?
C13 Ag5 Ag4 129.3(3) 3_665 . ?
O102 Ag5 Ag4 119.7(15) . . ?
Ag3 Ag5 Ag4 58.34(3) . . ?
Ag6 Ag5 Ag4 82.37(3) . . ?
Ag2 Ag5 Ag4 117.74(4) 3_665 . ?
C13 Ag6 C25 169.5(4) 3_665 . ?
C13 Ag6 C26 145.9(4) 3_665 . ?
C25 Ag6 C26 25.8(3) . . ?
C13 Ag6 Ag2 50.8(3) 3_665 3_665 ?
C25 Ag6 Ag2 124.1(3) . 3_665 ?
C26 Ag6 Ag2 124.6(2) . 3_665 ?
C13 Ag6 Ag5 47.6(3) 3_665 . ?
C25 Ag6 Ag5 141.2(3) . . ?
C26 Ag6 Ag5 166.5(2) . . ?
Ag2 Ag6 Ag5 62.52(3) 3_665 . ?
C13 Ag6 Ag1 143.7(3) 3_665 . ?
C25 Ag6 Ag1 44.8(3) . . ?
C26 Ag6 Ag1 70.3(2) . . ?
Ag2 Ag6 Ag1 113.66(4) 3_665 . ?
Ag5 Ag6 Ag1 96.49(4) . . ?
C32 O5 Ag4 128.0(8) . . ?
C34 O6 Ag4 132.6(8) . . ?
C39 O7 Ag2 125.9(8) . 3_665 ?
C37 O8 Ag2 131.4(8) . 3_665 ?
C2 C1 Ag1 170.0(11) . . ?
C2 C1 Ag4 98.7(8) . . ?
Ag1 C1 Ag4 84.1(4) . . ?
C2 C1 Ag2 98.0(8) . . ?
Ag1 C1 Ag2 83.3(4) . . ?
Ag4 C1 Ag2 152.4(6) . . ?
C1 C2 C3 179.0(13) . . ?
C2 C3 C4 110.4(11) . . ?
C2 C3 C6 108.6(11) . . ?
C4 C3 C6 110.3(11) . . ?
C2 C3 C5 107.2(12) . . ?
C4 C3 C5 110.1(11) . . ?
C6 C3 C5 110.3(11) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 Ag5 139.9(10) . . ?
C8 C7 Ag3 129.6(9) . . ?
Ag5 C7 Ag3 84.0(4) . . ?
C8 C7 Ag4 114.0(10) . . ?
Ag5 C7 Ag4 88.7(4) . . ?
Ag3 C7 Ag4 82.0(4) . . ?
C7 C8 C9 176.1(14) . . ?
C10 C9 C8 109.7(13) . . ?
C10 C9 C12 112.3(12) . . ?
C8 C9 C12 107.2(13) . . ?
C10 C9 C11 108.2(12) . . ?
C8 C9 C11 111.8(14) . . ?
C12 C9 C11 107.6(12) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag5 141.3(10) . 3_665 ?
C14 C13 Ag6 125.7(10) . 3_665 ?
Ag5 C13 Ag6 84.7(4) 3_665 3_665 ?
C14 C13 Ag2 118.6(9) . . ?
Ag5 C13 Ag2 85.8(4) 3_665 . ?
Ag6 C13 Ag2 81.8(4) 3_665 . ?
C13 C14 C15 178.6(12) . . ?
C14 C15 C18A 111.8(13) . . ?
C14 C15 C16A 109.0(11) . . ?
C18A C15 C16A 110.1(12) . . ?
C14 C15 C18B 106(3) . . ?
C14 C15 C17A 109.7(12) . . ?
C18A C15 C17A 108.2(12) . . ?
C16A C15 C17A 107.9(11) . . ?
C14 C15 C16B 120(3) . . ?
C18B C15 C16B 105(2) . . ?
C14 C15 C17B 115(3) . . ?
C18B C15 C17B 105(2) . . ?
C16B C15 C17B 104(2) . . ?
C15 C16A H16A 109.5 . . ?
C15 C16A H16B 109.5 . . ?
H16A C16A H16B 109.5 . . ?
C15 C16A H16C 109.5 . . ?
H16A C16A H16C 109.5 . . ?
H16B C16A H16C 109.5 . . ?
C15 C17A H17A 109.5 . . ?
C15 C17A H17B 109.5 . . ?
H17A C17A H17B 109.5 . . ?
C15 C17A H17C 109.5 . . ?
H17A C17A H17C 109.5 . . ?
H17B C17A H17C 109.5 . . ?
C15 C18A H18A 109.5 . . ?
C15 C18A H18B 109.5 . . ?
H18A C18A H18B 109.5 . . ?
C15 C18A H18C 109.5 . . ?
H18A C18A H18C 109.5 . . ?
H18B C18A H18C 109.5 . . ?
C15 C16B H16D 109.5 . . ?
C15 C16B H16E 109.5 . . ?
H16D C16B H16E 109.5 . . ?
C15 C16B H16F 109.5 . . ?
H16D C16B H16F 109.5 . . ?
H16E C16B H16F 109.5 . . ?
C15 C17B H17D 109.5 . . ?
C15 C17B H17E 109.5 . . ?
H17D C17B H17E 109.5 . . ?
C15 C17B H17F 109.5 . . ?
H17D C17B H17F 109.5 . . ?
H17E C17B H17F 109.5 . . ?
C15 C18B H18D 109.5 . . ?
C15 C18B H18E 109.5 . . ?
H18D C18B H18E 109.5 . . ?
C15 C18B H18F 109.5 . . ?
H18D C18B H18F 109.5 . . ?
H18E C18B H18F 109.5 . . ?
C26 C25 Ag1 166.8(9) . . ?
C26 C25 Ag6 101.3(8) . . ?
Ag1 C25 Ag6 87.0(4) . . ?
C26 C25 Ag3 96.6(8) . 3_665 ?
Ag1 C25 Ag3 86.9(4) . 3_665 ?
Ag6 C25 Ag3 124.5(5) . 3_665 ?
C25 C26 C27 174.3(12) . . ?
C25 C26 Ag3 56.6(6) . 3_665 ?
C27 C26 Ag3 126.1(7) . 3_665 ?
C25 C26 Ag6 52.9(6) . . ?
C27 C26 Ag6 129.1(7) . . ?
Ag3 C26 Ag6 94.0(3) 3_665 . ?
C26 C27 C29 108.0(10) . . ?
C26 C27 C28 108.6(10) . . ?
C29 C27 C28 107.9(14) . . ?
C26 C27 C30 109.6(11) . . ?
C29 C27 C30 108.6(14) . . ?
C28 C27 C30 114.1(15) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
F1 C31 F3 106.1(13) . . ?
F1 C31 F2 106.8(14) . . ?
F3 C31 F2 107.6(13) . . ?
F1 C31 C32 112.2(11) . . ?
F3 C31 C32 108.8(13) . . ?
F2 C31 C32 114.9(11) . . ?
O5 C32 C33 129.3(11) . . ?
O5 C32 C31 113.4(11) . . ?
C33 C32 C31 117.3(10) . . ?
C34 C33 C32 125.8(12) . . ?
C34 C33 H33 117.1 . . ?
C32 C33 H33 117.1 . . ?
O6 C34 C33 128.4(12) . . ?
O6 C34 C35 113.0(11) . . ?
C33 C34 C35 118.6(11) . . ?
F5 C35 F6 106.7(14) . . ?
F5 C35 F4 106.7(15) . . ?
F6 C35 F4 101.3(13) . . ?
F5 C35 C34 116.1(12) . . ?
F6 C35 C34 113.0(13) . . ?
F4 C35 C34 111.8(12) . . ?
F9 C36 F7 108.7(14) . . ?
F9 C36 F8 108.4(13) . . ?
F7 C36 F8 105.3(12) . . ?
F9 C36 C37 112.0(11) . . ?
F7 C36 C37 109.0(12) . . ?
F8 C36 C37 113.1(12) . . ?
O8 C37 C38 130.8(11) . . ?
O8 C37 C36 113.5(11) . . ?
C38 C37 C36 115.6(11) . . ?
C39 C38 C37 123.5(12) . . ?
C39 C38 H38 118.3 . . ?
C37 C38 H38 118.3 . . ?
O7 C39 C38 130.0(12) . . ?
O7 C39 C40 113.9(10) . . ?
C38 C39 C40 116.0(11) . . ?
F11B C40 F12B 109.1(14) . . ?
F10A C40 F11A 106.0(16) . . ?
F11B C40 F10B 107.0(13) . . ?
F12B C40 F10B 106.0(14) . . ?
F10A C40 F12A 103.0(16) . . ?
F11A C40 F12A 102.4(15) . . ?
F11B C40 C39 117.7(15) . . ?
F10A C40 C39 115.1(15) . . ?
F12B C40 C39 112.1(13) . . ?
F11A C40 C39 117.9(19) . . ?
F10B C40 C39 104.0(15) . . ?
F12A C40 C39 110.7(17) . . ?
C102 O102 Ag5 97(4) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 C25 C26 Ag3 105(4) . . . 3_665 ?
Ag6 C25 C26 Ag3 -127.2(6) . . . 3_665 ?
Ag1 C25 C26 Ag6 -128(4) . . . . ?
Ag3 C25 C26 Ag6 127.2(6) 3_665 . . . ?
Ag3 C26 C27 C29 -110.3(12) 3_665 . . . ?
Ag6 C26 C27 C29 114.8(12) . . . . ?
Ag3 C26 C27 C28 6.4(16) 3_665 . . . ?
Ag6 C26 C27 C28 -128.5(12) . . . . ?
Ag3 C26 C27 C30 131.6(13) 3_665 . . . ?
Ag6 C26 C27 C30 -3.3(17) . . . . ?
Ag4 O5 C32 C33 10(2) . . . . ?
Ag4 O5 C32 C31 -169.9(9) . . . . ?
F1 C31 C32 O5 -31.5(18) . . . . ?
F3 C31 C32 O5 85.6(15) . . . . ?
F2 C31 C32 O5 -153.8(13) . . . . ?
F1 C31 C32 C33 148.6(13) . . . . ?
F3 C31 C32 C33 -94.3(15) . . . . ?
F2 C31 C32 C33 26(2) . . . . ?
O5 C32 C33 C34 1(2) . . . . ?
C31 C32 C33 C34 -179.2(14) . . . . ?
Ag4 O6 C34 C33 -8(2) . . . . ?
Ag4 O6 C34 C35 173.0(9) . . . . ?
C32 C33 C34 O6 -3(2) . . . . ?
C32 C33 C34 C35 176.1(13) . . . . ?
O6 C34 C35 F5 -178.9(15) . . . . ?
C33 C34 C35 F5 2(2) . . . . ?
O6 C34 C35 F6 -55.1(18) . . . . ?
C33 C34 C35 F6 126.0(15) . . . . ?
O6 C34 C35 F4 58.4(18) . . . . ?
C33 C34 C35 F4 -120.5(15) . . . . ?
Ag2 O8 C37 C38 -13(2) 3_665 . . . ?
Ag2 O8 C37 C36 170.3(9) 3_665 . . . ?
F9 C36 C37 O8 -40.0(19) . . . . ?
F7 C36 C37 O8 80.3(16) . . . . ?
F8 C36 C37 O8 -162.9(13) . . . . ?
F9 C36 C37 C38 143.2(14) . . . . ?
F7 C36 C37 C38 -96.5(16) . . . . ?
F8 C36 C37 C38 20.3(18) . . . . ?
O8 C37 C38 C39 -4(2) . . . . ?
C36 C37 C38 C39 172.6(12) . . . . ?
Ag2 O7 C39 C38 14.0(19) 3_665 . . . ?
Ag2 O7 C39 C40 -169.5(8) 3_665 . . . ?
C37 C38 C39 O7 2(2) . . . . ?
C37 C38 C39 C40 -174.5(12) . . . . ?
O7 C39 C40 F11B -156.6(19) . . . . ?
C38 C39 C40 F11B 20(2) . . . . ?
O7 C39 C40 F10A 29(3) . . . . ?
C38 C39 C40 F10A -154(2) . . . . ?
O7 C39 C40 F12B -29(2) . . . . ?
C38 C39 C40 F12B 148(2) . . . . ?
O7 C39 C40 F11A 155(3) . . . . ?
C38 C39 C40 F11A -28(3) . . . . ?
O7 C39 C40 F10B 85(2) . . . . ?
C38 C39 C40 F10B -98(2) . . . . ?
O7 C39 C40 F12A -87(3) . . . . ?
C38 C39 C40 F12A 90(3) . . . . ?

_refine_diff_density_max         1.565
_refine_diff_density_min         -1.481
_refine_diff_density_rms         0.190

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex3
_database_code_depnum_ccdc_archive 'CCDC 1812183'
_audit_update_record             
;
2017-12-18 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C83 H102 Ag16 Cl F21 O8'
_chemical_formula_weight         3388.01

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   15.8413(16)
_cell_length_b                   17.2728(17)
_cell_length_c                   20.951(2)
_cell_angle_alpha                97.908(2)
_cell_angle_beta                 91.893(2)
_cell_angle_gamma                110.129(2)
_cell_volume                     5311.4(9)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9982
_cell_measurement_theta_min      2.8706
_cell_measurement_theta_max      25.3217

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.118
_exptl_crystal_F_000             3244
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.135
_exptl_crystal_size_mid          0.106
_exptl_crystal_size_min          0.083
_exptl_absorpt_coefficient_mu    2.982
_shelx_estimated_absorpt_T_min   0.689
_shelx_estimated_absorpt_T_max   0.790
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  0.6019
_exptl_absorpt_correction_T_max  0.7452
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            25121
_diffrn_reflns_av_unetI/netI     0.0374
_diffrn_reflns_av_R_equivalents  0.0233
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         2.870
_diffrn_reflns_theta_max         23.256
_diffrn_reflns_theta_full        23.256
_diffrn_measured_fraction_theta_max 0.964
_diffrn_measured_fraction_theta_full 0.964
_diffrn_reflns_Laue_measured_fraction_max 0.964
_diffrn_reflns_Laue_measured_fraction_full 0.964
_diffrn_reflns_point_group_measured_fraction_max 0.964
_diffrn_reflns_point_group_measured_fraction_full 0.964
_reflns_number_total             14714
_reflns_number_gt                11677
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+87.5652P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         14714
_refine_ls_number_parameters     1295
_refine_ls_number_restraints     853
_refine_ls_R_factor_all          0.0788
_refine_ls_R_factor_gt           0.0573
_refine_ls_wR_factor_ref         0.1302
_refine_ls_wR_factor_gt          0.1135
_refine_ls_goodness_of_fit_ref   1.167
_refine_ls_restrained_S_all      1.145
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.58356(5) 0.60234(5) 0.16797(4) 0.0404(2) Uani 1 1 d . . . . .
Ag2 Ag 0.77703(6) 0.62401(7) 0.16017(4) 0.0528(3) Uani 1 1 d . . . . .
Ag3 Ag 0.93751(7) 0.69337(6) 0.26886(5) 0.0575(3) Uani 1 1 d . . . . .
Ag4 Ag 0.83723(7) 0.91613(7) 0.12537(5) 0.0632(3) Uani 1 1 d . . . . .
Ag5 Ag 0.91475(13) 0.86405(17) 0.23697(10) 0.0523(7) Uani 0.882(10) 1 d . . P A
1
Ag5A Ag 0.9411(17) 0.8995(19) 0.2558(11) 0.099(6) Uiso 0.118(10) 1 d . . P A 2
Ag6 Ag 0.83556(7) 0.98476(6) 0.27638(5) 0.0645(3) Uani 1 1 d . . . . .
Ag7 Ag 0.63775(8) 0.92139(7) 0.15765(5) 0.0642(3) Uani 1 1 d . . . . .
Ag8 Ag 0.69205(7) 0.75911(6) 0.10152(7) 0.0741(4) Uani 1 1 d . . . . .
Ag9 Ag 0.62895(6) 0.65194(5) 0.36356(4) 0.0424(2) Uani 1 1 d . . . . .
Ag10 Ag 0.79958(6) 0.64754(6) 0.42350(4) 0.0458(2) Uani 1 1 d . . . . .
Ag11 Ag 0.55274(6) 0.49739(5) 0.27510(4) 0.0464(2) Uani 1 1 d . . . . .
Ag12 Ag 0.90330(6) 0.80681(6) 0.37665(4) 0.0492(2) Uani 1 1 d . . . . .
Ag13 Ag 0.53483(7) 0.71575(6) 0.26740(4) 0.0494(2) Uani 1 1 d . . . . .
Ag14 Ag 0.72694(7) 0.83577(6) 0.38897(5) 0.0531(2) Uani 1 1 d . . . . .
Ag15 Ag 0.64361(7) 0.89633(6) 0.29075(5) 0.0552(3) Uani 1 1 d . . . . .
Ag16 Ag 0.7613(4) 0.5546(5) 0.2801(3) 0.0439(12) Uani 0.82(5) 1 d . . P A 1
Ag6A Ag 0.763(2) 0.579(5) 0.2789(16) 0.068(7) Uani 0.18(5) 1 d . . P A 2
Cl0 Cl 0.74514(19) 0.75829(18) 0.25286(14) 0.0472(7) Uani 1 1 d . . . . .
F1 F 0.3472(10) 0.1693(8) 0.1681(6) 0.192(8) Uani 1 1 d . . . . .
F2 F 0.3410(7) 0.1974(6) 0.2665(5) 0.107(3) Uani 1 1 d . . . . .
F3 F 0.2898(8) 0.2603(9) 0.2092(8) 0.161(6) Uani 1 1 d . . . . .
F4 F 0.6283(8) 0.2606(7) 0.0926(6) 0.130(5) Uani 1 1 d . . . . .
F5 F 0.6878(7) 0.3895(7) 0.0908(5) 0.110(3) Uani 1 1 d . . . . .
F6 F 0.7377(7) 0.3382(8) 0.1634(6) 0.130(4) Uani 1 1 d . . . . .
F7 F 0.8849(7) 0.5545(9) 0.6218(5) 0.146(5) Uani 1 1 d . U . . .
F8 F 1.0206(7) 0.5916(11) 0.6156(5) 0.156(6) Uani 1 1 d . . . . .
F9 F 0.9590(13) 0.6739(9) 0.6383(5) 0.182(7) Uani 1 1 d . U . . .
F10 F 1.1566(6) 0.6377(7) 0.4291(4) 0.096(3) Uani 1 1 d . . . . .
F11 F 1.0844(7) 0.6164(8) 0.3376(4) 0.112(4) Uani 1 1 d . . . . .
F12 F 1.1286(6) 0.7363(7) 0.3936(6) 0.126(5) Uani 1 1 d . . . . .
F13 F 0.4098(9) 1.0493(11) 0.2096(9) 0.186(7) Uani 1 1 d . . . . .
F14 F 0.4509(13) 1.0150(14) 0.2952(13) 0.274(14) Uani 1 1 d . . . . .
F15 F 0.4874(9) 1.1448(10) 0.2881(8) 0.158(6) Uani 1 1 d . . . . .
C81 C 0.7992(18) 1.1833(13) 0.2868(12) 0.083(10) Uani 0.51(3) 1 d D U P B 1
F16 F 0.874(4) 1.160(4) 0.2927(19) 0.097(8) Uani 0.51(3) 1 d D U P B 1
F17 F 0.827(2) 1.2522(16) 0.2565(17) 0.122(12) Uani 0.51(3) 1 d D U P B 1
F18 F 0.7834(16) 1.2091(16) 0.3479(12) 0.116(10) Uani 0.51(3) 1 d D U P B 1
C81A C 0.8105(15) 1.1922(13) 0.2531(15) 0.079(10) Uani 0.49(3) 1 d D U P B 2
F16A F 0.877(4) 1.178(5) 0.2879(18) 0.097(8) Uani 0.49(3) 1 d D U P B 2
F17A F 0.8507(18) 1.2260(17) 0.2027(15) 0.135(11) Uani 0.49(3) 1 d D U P B 2
F18A F 0.7960(19) 1.2555(18) 0.292(2) 0.137(16) Uani 0.49(3) 1 d D U P B 2
F19 F 0.988(2) 0.7321(19) -0.0110(9) 0.182(14) Uani 0.63(2) 1 d D U P C 1
F20 F 0.9109(15) 0.6403(11) 0.0458(9) 0.132(9) Uani 0.63(2) 1 d D U P C 1
F21 F 1.0459(15) 0.7236(17) 0.0824(15) 0.195(11) Uani 0.63(2) 1 d D U P C 1
F19A F 1.0578(17) 0.782(2) 0.045(2) 0.172(17) Uani 0.37(2) 1 d D U P C 2
F20A F 0.932(2) 0.701(2) -0.0125(11) 0.129(14) Uani 0.37(2) 1 d D U P C 2
F21A F 0.982(3) 0.659(2) 0.071(2) 0.195(11) Uani 0.37(2) 1 d D U P C 2
O1 O 0.4544(6) 0.3596(6) 0.2640(5) 0.065(2) Uani 1 1 d . . . . .
O2 O 0.6280(6) 0.4256(6) 0.2074(5) 0.070(3) Uani 1 1 d . . . . .
O3 O 0.8548(5) 0.6109(5) 0.5152(4) 0.049(2) Uani 1 1 d . . . . .
O4 O 0.9398(5) 0.6381(6) 0.3918(4) 0.054(2) Uani 1 1 d . . . . .
O5 O 0.5472(8) 1.0043(7) 0.1775(7) 0.098(4) Uani 1 1 d . . . . .
O6 O 0.7449(6) 1.0596(6) 0.2087(5) 0.068(3) Uani 1 1 d . . . . .
O7 O 0.9025(7) 0.7592(6) 0.1400(4) 0.075(3) Uani 1 1 d . . . . .
O8 O 0.9212(8) 0.8379(7) 0.0618(5) 0.089(3) Uani 1 1 d . . . . .
C1 C 1.0012(7) 0.8244(7) 0.3106(5) 0.045(3) Uani 1 1 d . U . . .
C2 C 1.0715(8) 0.8561(8) 0.2867(6) 0.050(3) Uani 1 1 d . U . . .
C3 C 1.1600(8) 0.8971(9) 0.2634(6) 0.074(4) Uani 1 1 d D U . . .
C4 C 1.1464(16) 0.8812(19) 0.1877(8) 0.104(9) Uani 0.63(2) 1 d D U P D 1
H4A H 1.2041 0.9077 0.1702 0.155 Uiso 0.63(2) 1 calc R U P D 1
H4B H 1.1241 0.8210 0.1720 0.155 Uiso 0.63(2) 1 calc R U P D 1
H4C H 1.1024 0.9051 0.1736 0.155 Uiso 0.63(2) 1 calc R U P D 1
C5 C 1.1840(14) 0.9907(11) 0.2863(13) 0.094(8) Uani 0.63(2) 1 d D U P D 1
H5A H 1.2428 1.0213 0.2721 0.142 Uiso 0.63(2) 1 calc R U P D 1
H5B H 1.1379 1.0092 0.2679 0.142 Uiso 0.63(2) 1 calc R U P D 1
H5C H 1.1866 1.0015 0.3336 0.142 Uiso 0.63(2) 1 calc R U P D 1
C6 C 1.2275(15) 0.8631(17) 0.2861(13) 0.100(9) Uani 0.63(2) 1 d D U P D 1
H6A H 1.2858 0.8914 0.2700 0.150 Uiso 0.63(2) 1 calc R U P D 1
H6B H 1.2340 0.8723 0.3335 0.150 Uiso 0.63(2) 1 calc R U P D 1
H6C H 1.2076 0.8031 0.2698 0.150 Uiso 0.63(2) 1 calc R U P D 1
C4A C 1.167(3) 0.953(2) 0.2138(17) 0.114(14) Uani 0.37(2) 1 d D U P D 2
H4A1 H 1.2297 0.9757 0.2033 0.170 Uiso 0.37(2) 1 calc R U P D 2
H4A2 H 1.1284 0.9213 0.1747 0.170 Uiso 0.37(2) 1 calc R U P D 2
H4A3 H 1.1472 0.9993 0.2311 0.170 Uiso 0.37(2) 1 calc R U P D 2
C5A C 1.2265(18) 0.947(2) 0.3241(14) 0.085(12) Uani 0.37(2) 1 d D U P D 2
H5A1 H 1.2864 0.9756 0.3102 0.127 Uiso 0.37(2) 1 calc R U P D 2
H5A2 H 1.2041 0.9891 0.3466 0.127 Uiso 0.37(2) 1 calc R U P D 2
H5A3 H 1.2306 0.9090 0.3534 0.127 Uiso 0.37(2) 1 calc R U P D 2
C6A C 1.194(3) 0.826(2) 0.2378(19) 0.099(11) Uani 0.37(2) 1 d D U P D 2
H6A1 H 1.2534 0.8491 0.2215 0.148 Uiso 0.37(2) 1 calc R U P D 2
H6A2 H 1.1992 0.7950 0.2729 0.148 Uiso 0.37(2) 1 calc R U P D 2
H6A3 H 1.1514 0.7873 0.2027 0.148 Uiso 0.37(2) 1 calc R U P D 2
C7 C 0.9356(8) 0.9922(8) 0.2097(6) 0.052(3) Uani 1 1 d . U . . .
C8 C 0.9753(8) 1.0440(9) 0.1794(6) 0.057(3) Uani 1 1 d . U . . .
C9 C 1.0254(10) 1.1119(11) 0.1438(9) 0.091(5) Uani 1 1 d . U . . .
C10 C 1.0935(15) 1.0864(16) 0.1079(12) 0.157(9) Uani 1 1 d . U . . .
H10A H 1.1271 1.1308 0.0842 0.235 Uiso 1 1 calc R U . . .
H10B H 1.1354 1.0766 0.1386 0.235 Uiso 1 1 calc R U . . .
H10C H 1.0629 1.0349 0.0774 0.235 Uiso 1 1 calc R U . . .
C11 C 1.0726(16) 1.1907(13) 0.1912(14) 0.165(9) Uani 1 1 d . U . . .
H11A H 1.1057 1.2356 0.1677 0.247 Uiso 1 1 calc R U . . .
H11B H 1.0278 1.2070 0.2154 0.247 Uiso 1 1 calc R U . . .
H11C H 1.1149 1.1808 0.2214 0.247 Uiso 1 1 calc R U . . .
C12 C 0.9578(14) 1.1288(19) 0.1021(15) 0.208(13) Uani 1 1 d . U . . .
H12A H 0.9889 1.1735 0.0779 0.312 Uiso 1 1 calc R U . . .
H12B H 0.9240 1.0780 0.0718 0.312 Uiso 1 1 calc R U . . .
H12C H 0.9161 1.1459 0.1293 0.312 Uiso 1 1 calc R U . . .
C13 C 0.8183(7) 0.7896(7) 0.4507(5) 0.039(2) Uani 1 1 d . U . . .
C14 C 0.7783(8) 0.7789(7) 0.4992(5) 0.047(3) Uani 1 1 d . U . . .
C15 C 0.7304(10) 0.7691(9) 0.5607(6) 0.063(3) Uani 1 1 d . U . . .
C16 C 0.8023(13) 0.7814(15) 0.6146(7) 0.115(7) Uani 1 1 d . U . . .
H16A H 0.8464 0.8383 0.6193 0.173 Uiso 1 1 calc R U . . .
H16B H 0.7741 0.7726 0.6552 0.173 Uiso 1 1 calc R U . . .
H16C H 0.8328 0.7412 0.6040 0.173 Uiso 1 1 calc R U . . .
C17 C 0.6612(13) 0.6819(11) 0.5521(9) 0.109(6) Uani 1 1 d . U . . .
H17A H 0.6918 0.6412 0.5465 0.164 Uiso 1 1 calc R U . . .
H17B H 0.6272 0.6749 0.5905 0.164 Uiso 1 1 calc R U . . .
H17C H 0.6197 0.6731 0.5139 0.164 Uiso 1 1 calc R U . . .
C18 C 0.6829(12) 0.8318(11) 0.5694(7) 0.086(4) Uani 1 1 d . U . . .
H18A H 0.7276 0.8885 0.5750 0.128 Uiso 1 1 calc R U . . .
H18B H 0.6414 0.8229 0.5311 0.128 Uiso 1 1 calc R U . . .
H18C H 0.6488 0.8247 0.6077 0.128 Uiso 1 1 calc R U . . .
C19 C 0.4794(7) 0.5746(6) 0.2302(5) 0.035(2) Uani 1 1 d . U . . .
C20 C 0.4131(7) 0.5482(7) 0.2587(5) 0.040(2) Uani 1 1 d . U . . .
C21 C 0.3315(8) 0.5191(8) 0.2937(6) 0.050(3) Uani 1 1 d . U . . .
C22 C 0.2641(12) 0.4454(16) 0.2525(9) 0.176(11) Uani 1 1 d . U . . .
H22A H 0.2095 0.4252 0.2751 0.263 Uiso 1 1 calc R U . . .
H22B H 0.2491 0.4612 0.2117 0.263 Uiso 1 1 calc R U . . .
H22C H 0.2894 0.4010 0.2436 0.263 Uiso 1 1 calc R U . . .
C23 C 0.2956(13) 0.5893(13) 0.3074(12) 0.151(9) Uani 1 1 d . U . . .
H23A H 0.2413 0.5711 0.3307 0.227 Uiso 1 1 calc R U . . .
H23B H 0.3415 0.6376 0.3338 0.227 Uiso 1 1 calc R U . . .
H23C H 0.2805 0.6051 0.2665 0.227 Uiso 1 1 calc R U . . .
C24 C 0.3538(10) 0.4935(13) 0.3548(8) 0.104(6) Uani 1 1 d . U . . .
H24A H 0.2993 0.4743 0.3777 0.156 Uiso 1 1 calc R U . . .
H24B H 0.3774 0.4481 0.3451 0.156 Uiso 1 1 calc R U . . .
H24C H 0.3995 0.5412 0.3820 0.156 Uiso 1 1 calc R U . . .
C25 C 0.6714(7) 0.5481(7) 0.3598(5) 0.034(2) Uani 1 1 d . U . . .
C26 C 0.6860(7) 0.4899(6) 0.3770(5) 0.034(2) Uani 1 1 d . U . . .
C27 C 0.6938(9) 0.4153(7) 0.4015(6) 0.058(3) Uani 1 1 d . U . . .
C28 C 0.6251(10) 0.3347(8) 0.3626(7) 0.073(4) Uani 1 1 d . U . . .
H28A H 0.6308 0.2862 0.3791 0.109 Uiso 1 1 calc R U . . .
H28B H 0.5638 0.3351 0.3671 0.109 Uiso 1 1 calc R U . . .
H28C H 0.6368 0.3315 0.3169 0.109 Uiso 1 1 calc R U . . .
C29 C 0.6749(13) 0.4203(9) 0.4720(7) 0.090(5) Uani 1 1 d . U . . .
H29A H 0.6799 0.3716 0.4886 0.135 Uiso 1 1 calc R U . . .
H29B H 0.7188 0.4714 0.4969 0.135 Uiso 1 1 calc R U . . .
H29C H 0.6138 0.4213 0.4762 0.135 Uiso 1 1 calc R U . . .
C30 C 0.7902(10) 0.4165(9) 0.3944(9) 0.089(5) Uani 1 1 d . U . . .
H30A H 0.7969 0.3679 0.4103 0.133 Uiso 1 1 calc R U . . .
H30B H 0.8024 0.4146 0.3488 0.133 Uiso 1 1 calc R U . . .
H30C H 0.8332 0.4678 0.4197 0.133 Uiso 1 1 calc R U . . .
C31 C 0.8623(7) 0.5708(7) 0.2122(5) 0.036(2) Uani 1 1 d . U . . .
C32 C 0.9183(7) 0.5433(7) 0.1931(5) 0.042(2) Uani 1 1 d . U . . .
C33 C 0.9813(9) 0.5015(9) 0.1657(7) 0.064(3) Uani 1 1 d . U . . .
C34 C 0.9451(12) 0.4603(12) 0.0959(8) 0.102(6) Uani 1 1 d . U . . .
H34A H 0.9445 0.5033 0.0699 0.154 Uiso 1 1 calc R U . . .
H34B H 0.9840 0.4310 0.0776 0.154 Uiso 1 1 calc R U . . .
H34C H 0.8836 0.4204 0.0954 0.154 Uiso 1 1 calc R U . . .
C35 C 0.9835(11) 0.4388(10) 0.2073(10) 0.095(5) Uani 1 1 d . U . . .
H35A H 1.0241 0.4103 0.1907 0.143 Uiso 1 1 calc R U . . .
H35B H 1.0054 0.4670 0.2517 0.143 Uiso 1 1 calc R U . . .
H35C H 0.9226 0.3977 0.2069 0.143 Uiso 1 1 calc R U . . .
C36 C 1.0742(9) 0.5694(11) 0.1677(8) 0.088(5) Uani 1 1 d . U . . .
H36A H 1.0708 0.6098 0.1399 0.131 Uiso 1 1 calc R U . . .
H36B H 1.0937 0.5981 0.2122 0.131 Uiso 1 1 calc R U . . .
H36C H 1.1177 0.5439 0.1521 0.131 Uiso 1 1 calc R U . . .
C37 C 0.5700(8) 0.7440(7) 0.3824(5) 0.044(3) Uani 1 1 d . U . . .
C38 C 0.5258(9) 0.7865(7) 0.4002(6) 0.047(3) Uani 1 1 d . U . . .
C39 C 0.4744(12) 0.8394(10) 0.4263(8) 0.080(4) Uani 1 1 d . U . . .
C40 C 0.4071(19) 0.835(2) 0.3745(12) 0.188(11) Uani 1 1 d . U . . .
H40A H 0.4375 0.8514 0.3360 0.282 Uiso 1 1 calc R U . . .
H40B H 0.3639 0.7775 0.3641 0.282 Uiso 1 1 calc R U . . .
H40C H 0.3750 0.8726 0.3890 0.282 Uiso 1 1 calc R U . . .
C41 C 0.4401(17) 0.8168(15) 0.4864(11) 0.153(9) Uani 1 1 d . U . . .
H41A H 0.4903 0.8220 0.5173 0.229 Uiso 1 1 calc R U . . .
H41B H 0.4089 0.8541 0.5039 0.229 Uiso 1 1 calc R U . . .
H41C H 0.3978 0.7590 0.4790 0.229 Uiso 1 1 calc R U . . .
C42 C 0.5405(17) 0.9303(11) 0.4394(15) 0.185(11) Uani 1 1 d . U . . .
H42A H 0.5646 0.9468 0.3989 0.278 Uiso 1 1 calc R U . . .
H42B H 0.5087 0.9670 0.4571 0.278 Uiso 1 1 calc R U . . .
H42C H 0.5902 0.9350 0.4705 0.278 Uiso 1 1 calc R U . . .
C43 C 0.5399(9) 0.8302(8) 0.2200(6) 0.053(3) Uani 1 1 d . U . . .
C44 C 0.4782(8) 0.7911(8) 0.1779(6) 0.050(3) Uani 1 1 d . U . . .
C45 C 0.4054(9) 0.7530(9) 0.1256(7) 0.063(3) Uani 1 1 d . U . . .
C46 C 0.4411(10) 0.7126(11) 0.0697(7) 0.084(4) Uani 1 1 d . U . . .
H46A H 0.3932 0.6869 0.0344 0.126 Uiso 1 1 calc R U . . .
H46B H 0.4919 0.7550 0.0545 0.126 Uiso 1 1 calc R U . . .
H46C H 0.4614 0.6696 0.0838 0.126 Uiso 1 1 calc R U . . .
C47 C 0.3773(11) 0.8222(10) 0.1029(9) 0.093(5) Uani 1 1 d . U . . .
H47A H 0.3287 0.7975 0.0680 0.139 Uiso 1 1 calc R U . . .
H47B H 0.3559 0.8505 0.1392 0.139 Uiso 1 1 calc R U . . .
H47C H 0.4292 0.8626 0.0872 0.139 Uiso 1 1 calc R U . . .
C48 C 0.3271(9) 0.6879(10) 0.1497(8) 0.081(4) Uani 1 1 d . U . . .
H48A H 0.2785 0.6624 0.1149 0.122 Uiso 1 1 calc R U . . .
H48B H 0.3473 0.6447 0.1635 0.122 Uiso 1 1 calc R U . . .
H48C H 0.3048 0.7145 0.1864 0.122 Uiso 1 1 calc R U . . .
C49 C 0.7506(9) 0.9678(7) 0.3604(6) 0.053(3) Uani 1 1 d . U . . .
C50 C 0.8077(11) 1.0129(9) 0.4001(6) 0.084(5) Uani 1 1 d D U . . .
C51 C 0.8931(17) 1.0556(14) 0.4483(11) 0.101(8) Uani 0.55(2) 1 d D U P E 1
C52 C 0.977(2) 1.031(2) 0.436(2) 0.148(13) Uani 0.55(2) 1 d D U P E 1
H52A H 0.9599 0.9703 0.4340 0.222 Uiso 0.55(2) 1 calc R U P E 1
H52B H 0.9999 1.0471 0.3955 0.222 Uiso 0.55(2) 1 calc R U P E 1
H52C H 1.0236 1.0594 0.4719 0.222 Uiso 0.55(2) 1 calc R U P E 1
C53 C 0.856(3) 1.028(2) 0.5105(13) 0.150(16) Uani 0.55(2) 1 d D U P E 1
H53A H 0.8385 0.9674 0.5069 0.225 Uiso 0.55(2) 1 calc R U P E 1
H53B H 0.9015 1.0555 0.5467 0.225 Uiso 0.55(2) 1 calc R U P E 1
H53C H 0.8022 1.0436 0.5179 0.225 Uiso 0.55(2) 1 calc R U P E 1
C54 C 0.920(3) 1.1494(14) 0.452(2) 0.126(13) Uani 0.55(2) 1 d D U P E 1
H54A H 0.9443 1.1654 0.4111 0.189 Uiso 0.55(2) 1 calc R U P E 1
H54B H 0.8675 1.1657 0.4588 0.189 Uiso 0.55(2) 1 calc R U P E 1
H54C H 0.9667 1.1777 0.4876 0.189 Uiso 0.55(2) 1 calc R U P E 1
C51A C 0.846(2) 1.0869(16) 0.4538(12) 0.098(9) Uani 0.45(2) 1 d D U P E 2
C52A C 0.944(2) 1.113(3) 0.436(2) 0.116(13) Uani 0.45(2) 1 d D U P E 2
H52D H 0.9817 1.1618 0.4663 0.174 Uiso 0.45(2) 1 calc R U P E 2
H52E H 0.9661 1.0665 0.4380 0.174 Uiso 0.45(2) 1 calc R U P E 2
H52F H 0.9466 1.1261 0.3919 0.174 Uiso 0.45(2) 1 calc R U P E 2
C53A C 0.843(3) 1.069(2) 0.5227(14) 0.150(17) Uani 0.45(2) 1 d D U P E 2
H53D H 0.8701 1.1210 0.5529 0.226 Uiso 0.45(2) 1 calc R U P E 2
H53E H 0.7806 1.0410 0.5315 0.226 Uiso 0.45(2) 1 calc R U P E 2
H53F H 0.8776 1.0319 0.5282 0.226 Uiso 0.45(2) 1 calc R U P E 2
C54A C 0.815(3) 1.161(2) 0.451(2) 0.135(14) Uani 0.45(2) 1 d D U P E 2
H54D H 0.8438 1.2050 0.4877 0.203 Uiso 0.45(2) 1 calc R U P E 2
H54E H 0.8307 1.1832 0.4105 0.203 Uiso 0.45(2) 1 calc R U P E 2
H54F H 0.7490 1.1426 0.4524 0.203 Uiso 0.45(2) 1 calc R U P E 2
C55 C 0.6689(7) 0.6223(6) 0.0915(5) 0.032(2) Uani 1 1 d . U . . .
C56 C 0.6697(9) 0.6220(7) 0.0353(5) 0.048(3) Uani 1 1 d . U . . .
C57 C 0.6658(14) 0.6094(10) -0.0375(6) 0.092(5) Uani 1 1 d . U . . .
C58 C 0.5676(16) 0.5959(15) -0.0635(8) 0.153(8) Uani 1 1 d . U . . .
H58A H 0.5541 0.6466 -0.0498 0.230 Uiso 1 1 calc R U . . .
H58B H 0.5618 0.5834 -0.1108 0.230 Uiso 1 1 calc R U . . .
H58C H 0.5251 0.5491 -0.0462 0.230 Uiso 1 1 calc R U . . .
C59 C 0.7324(17) 0.6844(13) -0.0590(8) 0.151(9) Uani 1 1 d . U . . .
H59A H 0.7176 0.7339 -0.0434 0.227 Uiso 1 1 calc R U . . .
H59B H 0.7933 0.6921 -0.0412 0.227 Uiso 1 1 calc R U . . .
H59C H 0.7298 0.6761 -0.1063 0.227 Uiso 1 1 calc R U . . .
C60 C 0.683(2) 0.5323(13) -0.0590(9) 0.165(9) Uani 1 1 d . U . . .
H60A H 0.6379 0.4854 -0.0437 0.247 Uiso 1 1 calc R U . . .
H60B H 0.6801 0.5220 -0.1064 0.247 Uiso 1 1 calc R U . . .
H60C H 0.7435 0.5380 -0.0413 0.247 Uiso 1 1 calc R U . . .
C61 C 0.7046(8) 0.8751(7) 0.0732(6) 0.047(3) Uani 1 1 d . U . . .
C62 C 0.6893(8) 0.9258(7) 0.0450(5) 0.046(3) Uani 1 1 d . U . . .
C63 C 0.6704(9) 0.9833(8) 0.0035(6) 0.053(3) Uani 1 1 d . U . . .
C64 C 0.5777(10) 0.9389(11) -0.0310(7) 0.081(4) Uani 1 1 d . U . . .
H64A H 0.5635 0.9750 -0.0585 0.121 Uiso 1 1 calc R U . . .
H64B H 0.5762 0.8872 -0.0578 0.121 Uiso 1 1 calc R U . . .
H64C H 0.5330 0.9255 0.0009 0.121 Uiso 1 1 calc R U . . .
C65 C 0.6757(13) 1.0648(9) 0.0446(7) 0.083(5) Uani 1 1 d . U . . .
H65A H 0.6632 1.1015 0.0168 0.125 Uiso 1 1 calc R U . . .
H65B H 0.6311 1.0533 0.0766 0.125 Uiso 1 1 calc R U . . .
H65C H 0.7363 1.0923 0.0669 0.125 Uiso 1 1 calc R U . . .
C66 C 0.7402(11) 0.9998(11) -0.0455(7) 0.089(5) Uani 1 1 d . U . . .
H66A H 0.7295 1.0373 -0.0733 0.133 Uiso 1 1 calc R U . . .
H66B H 0.8007 1.0259 -0.0228 0.133 Uiso 1 1 calc R U . . .
H66C H 0.7357 0.9470 -0.0721 0.133 Uiso 1 1 calc R U . . .
C67 C 1.0949(10) 0.6557(11) 0.3969(7) 0.070(4) Uani 1 1 d . U . . .
C68 C 1.0034(8) 0.6371(8) 0.4282(6) 0.050(3) Uani 1 1 d . U . . .
C69 C 1.0054(8) 0.6257(7) 0.4933(5) 0.047(3) Uani 1 1 d . U . . .
H69 H 1.0604 0.6261 0.5132 0.057 Uiso 1 1 calc R U . . .
C70 C 0.9324(7) 0.6137(7) 0.5303(5) 0.041(2) Uani 1 1 d . U . . .
C71 C 0.9504(8) 0.6062(9) 0.6015(6) 0.052(3) Uani 1 1 d . U . . .
C72 C 0.3550(11) 0.2271(10) 0.2144(8) 0.074(4) Uani 1 1 d . U . . .
C73 C 0.4500(9) 0.2999(9) 0.2222(7) 0.060(3) Uani 1 1 d . U . . .
C74 C 0.5141(9) 0.2920(8) 0.1804(6) 0.055(3) Uani 1 1 d . U . . .
H74 H 0.5001 0.2405 0.1520 0.066 Uiso 1 1 calc R U . . .
C75 C 0.5975(8) 0.3542(9) 0.1771(6) 0.055(3) Uani 1 1 d . U . . .
C76 C 0.6628(11) 0.3334(11) 0.1285(8) 0.077(4) Uani 1 1 d . U . . .
C77 C 0.4764(13) 1.0663(15) 0.2578(14) 0.114(7) Uani 1 1 d . U . . .
C78 C 0.5627(11) 1.0603(11) 0.2254(9) 0.081(4) Uani 1 1 d . U . . .
C79 C 0.6432(10) 1.1185(10) 0.2543(10) 0.093(5) Uani 1 1 d . U . . .
H79 H 0.6414 1.1637 0.2850 0.111 Uiso 1 1 calc R U . . .
C80 C 0.7255(9) 1.1143(8) 0.2407(8) 0.075(4) Uani 1 1 d D U . . .
C82 C 0.9286(10) 0.7811(9) 0.0875(6) 0.068(4) Uani 1 1 d D U . . .
C83 C 0.9700(12) 0.7243(10) 0.0497(7) 0.111(7) Uani 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C19 2.102(11) . ?
Ag1 C55 2.118(10) . ?
Ag1 Ag13 2.9659(13) . ?
Ag1 Ag2 2.9698(12) . ?
Ag1 Ag11 3.0240(12) . ?
Ag1 Ag8 3.1963(14) . ?
Ag2 C55 2.190(10) . ?
Ag2 C31 2.213(10) . ?
Ag2 O7 2.591(9) . ?
Ag2 Ag6A 2.70(3) . ?
Ag2 Ag16 2.911(9) . ?
Ag2 Ag3 3.1391(14) . ?
Ag3 C1 2.175(12) . ?
Ag3 C31 2.188(11) . ?
Ag3 Ag6A 2.83(4) . ?
Ag3 Ag12 2.9710(14) . ?
Ag3 Ag16 3.030(7) . ?
Ag3 Ag5 3.244(2) . ?
Ag4 C61 2.173(13) . ?
Ag4 C7 2.247(12) . ?
Ag4 O8 2.495(10) . ?
Ag4 C8 2.601(13) . ?
Ag4 Ag8 2.8554(15) . ?
Ag4 Ag5 2.9890(17) . ?
Ag4 Ag6 3.2265(16) . ?
Ag4 Ag5A 3.24(2) . ?
Ag4 Ag7 3.2823(17) . ?
Ag5 C7 2.278(12) . ?
Ag5 C1 2.349(11) . ?
Ag5 O7 2.483(9) . ?
Ag5 Cl0 2.741(3) . ?
Ag5 Ag6 2.828(2) . ?
Ag5 Ag12 3.2066(16) . ?
Ag5A C7 2.00(2) . ?
Ag5A C1 2.26(2) . ?
Ag5A C2 2.52(2) . ?
Ag5A Ag6 2.592(18) . ?
Ag5A Ag12 3.144(17) . ?
Ag6 C7 2.129(13) . ?
Ag6 C49 2.242(12) . ?
Ag6 C50 2.651(14) . ?
Ag6 Ag15 2.9427(15) . ?
Ag7 C61 2.282(12) . ?
Ag7 O5 2.360(11) . ?
Ag7 C43 2.369(12) . ?
Ag7 O6 2.473(9) . ?
Ag7 C62 2.525(12) . ?
Ag7 Ag15 2.8836(14) . ?
Ag7 Ag8 3.2861(16) . ?
Ag8 C61 2.114(11) . ?
Ag8 C55 2.242(10) . ?
Ag8 C56 2.479(11) . ?
Ag9 C37 2.105(11) . ?
Ag9 C25 2.114(10) . ?
Ag9 Ag11 2.8795(12) . ?
Ag9 Ag10 2.9720(12) . ?
Ag9 Ag14 2.9771(13) . ?
Ag9 Ag13 3.0067(12) . ?
Ag9 Ag6A 3.27(5) . ?
Ag10 O3 2.337(7) . ?
Ag10 C13 2.354(11) . ?
Ag10 C25 2.377(11) . ?
Ag10 O4 2.391(8) . ?
Ag10 Ag12 2.9949(13) . ?
Ag10 Ag6A 3.06(4) . ?
Ag10 Ag16 3.139(6) . ?
Ag11 C19 2.313(10) . ?
Ag11 O1 2.327(9) . ?
Ag11 O2 2.370(9) . ?
Ag11 C25 2.380(10) . ?
Ag11 C20 2.674(10) . ?
Ag11 Ag16 3.100(5) . ?
Ag11 Ag6A 3.13(3) . ?
Ag12 C13 2.073(11) . ?
Ag12 C1 2.084(12) . ?
Ag12 Ag14 3.0160(14) . ?
Ag13 C19 2.299(10) . ?
Ag13 C43 2.310(11) . ?
Ag13 C37 2.398(11) . ?
Ag13 Ag15 2.9602(14) . ?
Ag14 C13 2.314(10) . ?
Ag14 C49 2.345(11) . ?
Ag14 C37 2.433(12) . ?
Ag14 Ag15 2.9043(13) . ?
Ag15 C43 2.069(13) . ?
Ag15 C49 2.104(13) . ?
Ag16 C31 2.147(12) . ?
Ag16 C25 2.220(11) . ?
Ag16 C26 2.580(13) . ?
Ag6A C31 2.17(4) . ?
Ag6A C25 2.27(3) . ?
F1 C72 1.263(17) . ?
F2 C72 1.263(18) . ?
F3 C72 1.35(2) . ?
F4 C76 1.298(17) . ?
F5 C76 1.300(19) . ?
F6 C76 1.343(18) . ?
F7 C71 1.244(15) . ?
F8 C71 1.258(14) . ?
F9 C71 1.272(17) . ?
F10 C67 1.314(15) . ?
F11 C67 1.307(17) . ?
F12 C67 1.321(18) . ?
F13 C77 1.36(3) . ?
F14 C77 1.24(2) . ?
F15 C77 1.36(2) . ?
C81 F18 1.358(18) . ?
C81 F17 1.371(19) . ?
C81 F16 1.379(19) . ?
C81 C80 1.538(18) . ?
C81A F17A 1.348(19) . ?
C81A F18A 1.361(19) . ?
C81A F16A 1.373(19) . ?
C81A C80 1.526(18) . ?
F19 C83 1.327(17) . ?
F20 C83 1.420(17) . ?
F21 C83 1.370(18) . ?
F19A C83 1.419(19) . ?
F20A C83 1.365(19) . ?
F21A C83 1.338(19) . ?
O1 C73 1.238(16) . ?
O2 C75 1.230(15) . ?
O3 C70 1.242(13) . ?
O4 C68 1.249(14) . ?
O5 C78 1.25(2) . ?
O6 C80 1.214(16) . ?
O7 C82 1.250(15) . ?
O8 C82 1.219(16) . ?
C1 C2 1.219(15) . ?
C2 C3 1.470(17) . ?
C3 C6 1.480(16) . ?
C3 C4A 1.497(19) . ?
C3 C5 1.529(17) . ?
C3 C6A 1.552(19) . ?
C3 C4 1.566(16) . ?
C3 C5A 1.568(18) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C4A H4A1 0.9800 . ?
C4A H4A2 0.9800 . ?
C4A H4A3 0.9800 . ?
C5A H5A1 0.9800 . ?
C5A H5A2 0.9800 . ?
C5A H5A3 0.9800 . ?
C6A H6A1 0.9800 . ?
C6A H6A2 0.9800 . ?
C6A H6A3 0.9800 . ?
C7 C8 1.182(16) . ?
C8 C9 1.484(18) . ?
C9 C12 1.49(2) . ?
C9 C10 1.49(3) . ?
C9 C11 1.51(3) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.217(15) . ?
C14 C15 1.518(17) . ?
C15 C17 1.51(2) . ?
C15 C18 1.512(19) . ?
C15 C16 1.52(2) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.206(14) . ?
C20 C21 1.476(15) . ?
C21 C24 1.480(17) . ?
C21 C22 1.49(2) . ?
C21 C23 1.51(2) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.202(13) . ?
C26 C27 1.493(15) . ?
C27 C29 1.515(19) . ?
C27 C30 1.53(2) . ?
C27 C28 1.541(18) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.198(14) . ?
C32 C33 1.504(16) . ?
C33 C35 1.49(2) . ?
C33 C36 1.529(19) . ?
C33 C34 1.53(2) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.210(15) . ?
C38 C39 1.483(17) . ?
C39 C41 1.44(2) . ?
C39 C40 1.47(3) . ?
C39 C42 1.54(3) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.231(17) . ?
C44 C45 1.470(18) . ?
C45 C46 1.51(2) . ?
C45 C48 1.516(18) . ?
C45 C47 1.536(18) . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.184(17) . ?
C50 C51A 1.515(18) . ?
C50 C51 1.553(18) . ?
C51 C54 1.518(19) . ?
C51 C53 1.518(19) . ?
C51 C52 1.545(19) . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 H53A 0.9800 . ?
C53 H53B 0.9800 . ?
C53 H53C 0.9800 . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C51A C53A 1.520(19) . ?
C51A C52A 1.53(2) . ?
C51A C54A 1.54(2) . ?
C52A H52D 0.9800 . ?
C52A H52E 0.9800 . ?
C52A H52F 0.9800 . ?
C53A H53D 0.9800 . ?
C53A H53E 0.9800 . ?
C53A H53F 0.9800 . ?
C54A H54D 0.9800 . ?
C54A H54E 0.9800 . ?
C54A H54F 0.9800 . ?
C55 C56 1.177(14) . ?
C56 C57 1.508(17) . ?
C57 C60 1.47(3) . ?
C57 C59 1.50(2) . ?
C57 C58 1.56(3) . ?
C58 H58A 0.9800 . ?
C58 H58B 0.9800 . ?
C58 H58C 0.9800 . ?
C59 H59A 0.9800 . ?
C59 H59B 0.9800 . ?
C59 H59C 0.9800 . ?
C60 H60A 0.9800 . ?
C60 H60B 0.9800 . ?
C60 H60C 0.9800 . ?
C61 C62 1.205(15) . ?
C62 C63 1.502(16) . ?
C63 C64 1.507(19) . ?
C63 C66 1.516(18) . ?
C63 C65 1.520(18) . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C67 C68 1.561(17) . ?
C68 C69 1.405(16) . ?
C69 C70 1.387(15) . ?
C69 H69 0.9500 . ?
C70 C71 1.540(16) . ?
C72 C73 1.581(19) . ?
C73 C74 1.393(18) . ?
C74 C75 1.398(17) . ?
C74 H74 0.9500 . ?
C75 C76 1.568(19) . ?
C77 C78 1.58(3) . ?
C78 C79 1.38(2) . ?
C79 C80 1.37(2) . ?
C79 H79 0.9500 . ?
C82 C83 1.511(15) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C19 Ag1 C55 169.4(4) . . ?
C19 Ag1 Ag13 50.5(3) . . ?
C55 Ag1 Ag13 133.5(3) . . ?
C19 Ag1 Ag2 142.4(3) . . ?
C55 Ag1 Ag2 47.4(3) . . ?
Ag13 Ag1 Ag2 118.61(4) . . ?
C19 Ag1 Ag11 49.8(3) . . ?
C55 Ag1 Ag11 136.0(3) . . ?
Ag13 Ag1 Ag11 81.32(3) . . ?
Ag2 Ag1 Ag11 96.09(3) . . ?
C19 Ag1 Ag8 136.3(3) . . ?
C55 Ag1 Ag8 44.4(3) . . ?
Ag13 Ag1 Ag8 89.49(4) . . ?
Ag2 Ag1 Ag8 66.97(3) . . ?
Ag11 Ag1 Ag8 153.88(4) . . ?
C55 Ag2 C31 156.3(4) . . ?
C55 Ag2 O7 99.5(3) . . ?
C31 Ag2 O7 98.4(4) . . ?
C55 Ag2 Ag6A 128.0(7) . . ?
C31 Ag2 Ag6A 51.3(11) . . ?
O7 Ag2 Ag6A 121.0(12) . . ?
C55 Ag2 Ag16 128.4(3) . . ?
C31 Ag2 Ag16 47.2(3) . . ?
O7 Ag2 Ag16 125.5(2) . . ?
C55 Ag2 Ag1 45.4(3) . . ?
C31 Ag2 Ag1 130.1(3) . . ?
O7 Ag2 Ag1 125.3(2) . . ?
Ag6A Ag2 Ag1 83.2(7) . . ?
Ag16 Ag2 Ag1 85.11(11) . . ?
C55 Ag2 Ag3 159.5(3) . . ?
C31 Ag2 Ag3 44.2(3) . . ?
O7 Ag2 Ag3 66.4(2) . . ?
Ag6A Ag2 Ag3 57.3(8) . . ?
Ag16 Ag2 Ag3 59.97(12) . . ?
Ag1 Ag2 Ag3 129.81(4) . . ?
C1 Ag3 C31 168.9(4) . . ?
C1 Ag3 Ag6A 130.4(15) . . ?
C31 Ag3 Ag6A 49.3(13) . . ?
C1 Ag3 Ag12 44.5(3) . . ?
C31 Ag3 Ag12 136.7(3) . . ?
Ag6A Ag3 Ag12 87.4(13) . . ?
C1 Ag3 Ag16 136.0(3) . . ?
C31 Ag3 Ag16 45.1(3) . . ?
Ag12 Ag3 Ag16 92.06(10) . . ?
C1 Ag3 Ag2 124.5(3) . . ?
C31 Ag3 Ag2 44.8(3) . . ?
Ag6A Ag3 Ag2 53.4(6) . . ?
Ag12 Ag3 Ag2 111.95(4) . . ?
Ag16 Ag3 Ag2 56.28(16) . . ?
C1 Ag3 Ag5 46.4(3) . . ?
C31 Ag3 Ag5 122.6(3) . . ?
Ag12 Ag3 Ag5 61.93(5) . . ?
Ag16 Ag3 Ag5 114.37(17) . . ?
Ag2 Ag3 Ag5 78.29(6) . . ?
C61 Ag4 C7 150.7(5) . . ?
C61 Ag4 O8 105.1(4) . . ?
C7 Ag4 O8 104.2(4) . . ?
C61 Ag4 C8 145.6(4) . . ?
C7 Ag4 C8 27.0(4) . . ?
O8 Ag4 C8 98.1(4) . . ?
C61 Ag4 Ag8 47.4(3) . . ?
C7 Ag4 Ag8 136.1(3) . . ?
O8 Ag4 Ag8 83.8(3) . . ?
C8 Ag4 Ag8 162.9(3) . . ?
C61 Ag4 Ag5 134.5(3) . . ?
C7 Ag4 Ag5 49.1(3) . . ?
O8 Ag4 Ag5 82.8(2) . . ?
C8 Ag4 Ag5 72.8(3) . . ?
Ag8 Ag4 Ag5 90.74(7) . . ?
C61 Ag4 Ag6 112.5(3) . . ?
C7 Ag4 Ag6 41.1(3) . . ?
O8 Ag4 Ag6 135.5(3) . . ?
C8 Ag4 Ag6 62.3(3) . . ?
Ag8 Ag4 Ag6 104.58(5) . . ?
Ag5 Ag4 Ag6 53.97(5) . . ?
C61 Ag4 Ag5A 142.3(5) . . ?
C7 Ag4 Ag5A 37.6(6) . . ?
O8 Ag4 Ag5A 88.3(4) . . ?
C8 Ag4 Ag5A 61.9(6) . . ?
Ag8 Ag4 Ag5A 101.4(5) . . ?
Ag6 Ag4 Ag5A 47.2(4) . . ?
C61 Ag4 Ag7 43.8(3) . . ?
C7 Ag4 Ag7 107.6(3) . . ?
O8 Ag4 Ag7 145.7(3) . . ?
C8 Ag4 Ag7 116.1(3) . . ?
Ag8 Ag4 Ag7 64.30(4) . . ?
Ag5 Ag4 Ag7 108.58(4) . . ?
Ag6 Ag4 Ag7 68.96(4) . . ?
Ag5A Ag4 Ag7 109.2(3) . . ?
C7 Ag5 C1 129.8(4) . . ?
C7 Ag5 O7 111.4(4) . . ?
C1 Ag5 O7 100.4(4) . . ?
C7 Ag5 Cl0 120.4(3) . . ?
C1 Ag5 Cl0 100.2(3) . . ?
O7 Ag5 Cl0 83.7(2) . . ?
C7 Ag5 Ag6 47.8(3) . . ?
C1 Ag5 Ag6 121.7(3) . . ?
O7 Ag5 Ag6 137.1(3) . . ?
Cl0 Ag5 Ag6 81.28(7) . . ?
C7 Ag5 Ag4 48.2(3) . . ?
C1 Ag5 Ag4 167.7(3) . . ?
O7 Ag5 Ag4 72.5(3) . . ?
Cl0 Ag5 Ag4 89.20(9) . . ?
Ag6 Ag5 Ag4 67.31(4) . . ?
C7 Ag5 Ag12 129.7(3) . . ?
C1 Ag5 Ag12 40.5(3) . . ?
O7 Ag5 Ag12 118.8(2) . . ?
Cl0 Ag5 Ag12 68.08(7) . . ?
Ag6 Ag5 Ag12 91.99(6) . . ?
Ag4 Ag5 Ag12 151.80(5) . . ?
C7 Ag5 Ag3 165.7(3) . . ?
C1 Ag5 Ag3 42.1(3) . . ?
O7 Ag5 Ag3 65.7(2) . . ?
Cl0 Ag5 Ag3 73.69(8) . . ?
Ag6 Ag5 Ag3 143.95(5) . . ?
Ag4 Ag5 Ag3 136.13(11) . . ?
Ag12 Ag5 Ag3 54.84(3) . . ?
C7 Ag5A C1 159.0(16) . . ?
C7 Ag5A C2 131.3(12) . . ?
C1 Ag5A C2 28.9(4) . . ?
C7 Ag5A Ag6 53.3(6) . . ?
C1 Ag5A Ag6 137.9(9) . . ?
C2 Ag5A Ag6 153.3(13) . . ?
C7 Ag5A Ag12 149.9(10) . . ?
C1 Ag5A Ag12 41.5(4) . . ?
C2 Ag5A Ag12 69.1(5) . . ?
Ag6 Ag5A Ag12 98.2(5) . . ?
C7 Ag5A Ag4 43.2(6) . . ?
C1 Ag5A Ag4 149.3(13) . . ?
C2 Ag5A Ag4 138.2(8) . . ?
Ag6 Ag5A Ag4 66.1(4) . . ?
Ag12 Ag5A Ag4 140.5(10) . . ?
C7 Ag6 C49 167.0(5) . . ?
C7 Ag6 Ag5A 49.1(5) . . ?
C49 Ag6 Ag5A 119.6(5) . . ?
C7 Ag6 C50 144.8(5) . . ?
C49 Ag6 C50 26.4(4) . . ?
Ag5A Ag6 C50 112.9(6) . . ?
C7 Ag6 Ag5 52.4(3) . . ?
C49 Ag6 Ag5 118.3(3) . . ?
C50 Ag6 Ag5 118.3(4) . . ?
C7 Ag6 Ag15 141.8(3) . . ?
C49 Ag6 Ag15 45.4(3) . . ?
Ag5A Ag6 Ag15 119.1(7) . . ?
C50 Ag6 Ag15 71.7(3) . . ?
Ag5 Ag6 Ag15 108.08(6) . . ?
C7 Ag6 Ag4 43.9(3) . . ?
C49 Ag6 Ag4 143.1(3) . . ?
Ag5A Ag6 Ag4 66.7(5) . . ?
C50 Ag6 Ag4 168.7(3) . . ?
Ag5 Ag6 Ag4 58.72(5) . . ?
Ag15 Ag6 Ag4 98.38(4) . . ?
C61 Ag7 O5 138.3(5) . . ?
C61 Ag7 C43 122.7(4) . . ?
O5 Ag7 C43 85.8(4) . . ?
C61 Ag7 O6 107.0(4) . . ?
O5 Ag7 O6 75.6(4) . . ?
C43 Ag7 O6 121.0(4) . . ?
C61 Ag7 C62 28.5(4) . . ?
O5 Ag7 C62 110.3(4) . . ?
C43 Ag7 C62 141.3(4) . . ?
O6 Ag7 C62 97.4(4) . . ?
C61 Ag7 Ag15 129.6(3) . . ?
O5 Ag7 Ag15 92.1(3) . . ?
C43 Ag7 Ag15 45.1(3) . . ?
O6 Ag7 Ag15 79.7(2) . . ?
C62 Ag7 Ag15 156.1(3) . . ?
C61 Ag7 Ag4 41.3(3) . . ?
O5 Ag7 Ag4 146.8(3) . . ?
C43 Ag7 Ag4 123.4(3) . . ?
O6 Ag7 Ag4 75.4(2) . . ?
C62 Ag7 Ag4 58.3(3) . . ?
Ag15 Ag7 Ag4 98.35(4) . . ?
C61 Ag7 Ag8 39.7(3) . . ?
O5 Ag7 Ag8 158.6(3) . . ?
C43 Ag7 Ag8 85.1(3) . . ?
O6 Ag7 Ag8 125.6(2) . . ?
C62 Ag7 Ag8 67.1(3) . . ?
Ag15 Ag7 Ag8 95.08(4) . . ?
Ag4 Ag7 Ag8 51.53(3) . . ?
C61 Ag8 C55 158.6(4) . . ?
C61 Ag8 C56 130.4(4) . . ?
C55 Ag8 C56 28.3(3) . . ?
C61 Ag8 Ag4 49.1(3) . . ?
C55 Ag8 Ag4 139.7(3) . . ?
C56 Ag8 Ag4 134.2(3) . . ?
C61 Ag8 Ag1 150.3(3) . . ?
C55 Ag8 Ag1 41.4(2) . . ?
C56 Ag8 Ag1 65.9(3) . . ?
Ag4 Ag8 Ag1 142.75(6) . . ?
C61 Ag8 Ag7 43.6(3) . . ?
C55 Ag8 Ag7 150.8(3) . . ?
C56 Ag8 Ag7 155.8(3) . . ?
Ag4 Ag8 Ag7 64.16(4) . . ?
Ag1 Ag8 Ag7 110.11(4) . . ?
C37 Ag9 C25 168.0(4) . . ?
C37 Ag9 Ag11 125.7(3) . . ?
C25 Ag9 Ag11 54.3(3) . . ?
C37 Ag9 Ag10 128.8(3) . . ?
C25 Ag9 Ag10 52.5(3) . . ?
Ag11 Ag9 Ag10 105.44(4) . . ?
C37 Ag9 Ag14 54.0(3) . . ?
C25 Ag9 Ag14 133.3(3) . . ?
Ag11 Ag9 Ag14 150.62(4) . . ?
Ag10 Ag9 Ag14 83.15(3) . . ?
C37 Ag9 Ag13 52.4(3) . . ?
C25 Ag9 Ag13 134.3(3) . . ?
Ag11 Ag9 Ag13 83.04(3) . . ?
Ag10 Ag9 Ag13 149.23(4) . . ?
Ag14 Ag9 Ag13 76.55(3) . . ?
C37 Ag9 Ag6A 148.5(11) . . ?
C25 Ag9 Ag6A 43.6(11) . . ?
Ag11 Ag9 Ag6A 60.8(10) . . ?
Ag10 Ag9 Ag6A 58.4(5) . . ?
Ag14 Ag9 Ag6A 104.0(12) . . ?
Ag13 Ag9 Ag6A 104.4(7) . . ?
O3 Ag10 C13 105.9(3) . . ?
O3 Ag10 C25 118.8(3) . . ?
C13 Ag10 C25 123.1(3) . . ?
O3 Ag10 O4 78.0(3) . . ?
C13 Ag10 O4 108.4(4) . . ?
C25 Ag10 O4 113.6(3) . . ?
O3 Ag10 Ag9 140.47(19) . . ?
C13 Ag10 Ag9 78.2(3) . . ?
C25 Ag10 Ag9 44.9(2) . . ?
O4 Ag10 Ag9 139.23(18) . . ?
O3 Ag10 Ag12 120.5(2) . . ?
C13 Ag10 Ag12 43.6(3) . . ?
C25 Ag10 Ag12 120.2(2) . . ?
O4 Ag10 Ag12 72.3(2) . . ?
Ag9 Ag10 Ag12 90.11(3) . . ?
O3 Ag10 Ag6A 136.6(14) . . ?
C13 Ag10 Ag6A 114.8(14) . . ?
C25 Ag10 Ag6A 47.3(7) . . ?
O4 Ag10 Ag6A 75.7(7) . . ?
Ag9 Ag10 Ag6A 65.6(9) . . ?
Ag12 Ag10 Ag6A 82.9(12) . . ?
O3 Ag10 Ag16 129.3(3) . . ?
C13 Ag10 Ag16 122.5(3) . . ?
C25 Ag10 Ag16 44.9(3) . . ?
O4 Ag10 Ag16 73.8(2) . . ?
Ag9 Ag10 Ag16 69.47(12) . . ?
Ag12 Ag10 Ag16 89.49(16) . . ?
C19 Ag11 O1 108.4(4) . . ?
C19 Ag11 O2 119.1(4) . . ?
O1 Ag11 O2 77.8(3) . . ?
C19 Ag11 C25 126.6(4) . . ?
O1 Ag11 C25 119.2(3) . . ?
O2 Ag11 C25 94.3(3) . . ?
C19 Ag11 C20 26.8(3) . . ?
O1 Ag11 C20 90.2(3) . . ?
O2 Ag11 C20 135.5(3) . . ?
C25 Ag11 C20 128.0(3) . . ?
C19 Ag11 Ag9 81.0(3) . . ?
O1 Ag11 Ag9 144.4(2) . . ?
O2 Ag11 Ag9 128.6(2) . . ?
C25 Ag11 Ag9 46.2(2) . . ?
C20 Ag11 Ag9 84.4(2) . . ?
C19 Ag11 Ag1 43.9(3) . . ?
O1 Ag11 Ag1 124.3(2) . . ?
O2 Ag11 Ag1 81.5(3) . . ?
C25 Ag11 Ag1 113.4(2) . . ?
C20 Ag11 Ag1 70.4(2) . . ?
Ag9 Ag11 Ag1 86.78(3) . . ?
C19 Ag11 Ag16 119.4(3) . . ?
O1 Ag11 Ag16 125.5(3) . . ?
O2 Ag11 Ag16 57.6(2) . . ?
C25 Ag11 Ag16 45.5(3) . . ?
C20 Ag11 Ag16 143.3(3) . . ?
Ag9 Ag11 Ag16 71.19(11) . . ?
Ag1 Ag11 Ag16 81.01(18) . . ?
C19 Ag11 Ag6A 112.2(12) . . ?
O1 Ag11 Ag6A 133.2(15) . . ?
O2 Ag11 Ag6A 62.9(13) . . ?
C25 Ag11 Ag6A 46.2(6) . . ?
C20 Ag11 Ag6A 135.5(14) . . ?
Ag9 Ag11 Ag6A 65.7(13) . . ?
Ag1 Ag11 Ag6A 75.5(8) . . ?
C13 Ag12 C1 172.9(4) . . ?
C13 Ag12 Ag3 134.4(3) . . ?
C1 Ag12 Ag3 47.0(3) . . ?
C13 Ag12 Ag10 51.5(3) . . ?
C1 Ag12 Ag10 127.4(3) . . ?
Ag3 Ag12 Ag10 83.82(4) . . ?
C13 Ag12 Ag14 50.0(3) . . ?
C1 Ag12 Ag14 136.6(3) . . ?
Ag3 Ag12 Ag14 124.24(4) . . ?
Ag10 Ag12 Ag14 82.11(3) . . ?
C13 Ag12 Ag5A 140.0(4) . . ?
C1 Ag12 Ag5A 45.8(4) . . ?
Ag3 Ag12 Ag5A 71.8(5) . . ?
Ag10 Ag12 Ag5A 145.2(6) . . ?
Ag14 Ag12 Ag5A 91.3(3) . . ?
C13 Ag12 Ag5 139.7(3) . . ?
C1 Ag12 Ag5 47.1(3) . . ?
Ag3 Ag12 Ag5 63.22(5) . . ?
Ag10 Ag12 Ag5 133.13(7) . . ?
Ag14 Ag12 Ag5 89.73(4) . . ?
C19 Ag13 C43 132.7(4) . . ?
C19 Ag13 C37 111.3(4) . . ?
C43 Ag13 C37 115.1(4) . . ?
C19 Ag13 Ag15 164.4(3) . . ?
C43 Ag13 Ag15 44.1(3) . . ?
C37 Ag13 Ag15 77.3(3) . . ?
C19 Ag13 Ag1 44.9(3) . . ?
C43 Ag13 Ag1 105.9(3) . . ?
C37 Ag13 Ag1 129.6(3) . . ?
Ag15 Ag13 Ag1 119.58(4) . . ?
C19 Ag13 Ag9 78.5(2) . . ?
C43 Ag13 Ag9 145.1(3) . . ?
C37 Ag13 Ag9 44.1(3) . . ?
Ag15 Ag13 Ag9 101.40(4) . . ?
Ag1 Ag13 Ag9 85.57(3) . . ?
C13 Ag14 C49 130.7(4) . . ?
C13 Ag14 C37 111.1(4) . . ?
C49 Ag14 C37 115.3(4) . . ?
C13 Ag14 Ag15 166.8(3) . . ?
C49 Ag14 Ag15 45.7(3) . . ?
C37 Ag14 Ag15 77.9(3) . . ?
C13 Ag14 Ag9 78.7(3) . . ?
C49 Ag14 Ag9 149.2(3) . . ?
C37 Ag14 Ag9 44.4(3) . . ?
Ag15 Ag14 Ag9 103.45(4) . . ?
C13 Ag14 Ag12 43.3(3) . . ?
C49 Ag14 Ag12 106.2(3) . . ?
C37 Ag14 Ag12 134.0(3) . . ?
Ag15 Ag14 Ag12 123.53(4) . . ?
Ag9 Ag14 Ag12 89.61(4) . . ?
C43 Ag15 C49 177.6(4) . . ?
C43 Ag15 Ag7 54.2(3) . . ?
C49 Ag15 Ag7 123.6(3) . . ?
C43 Ag15 Ag14 129.3(3) . . ?
C49 Ag15 Ag14 52.9(3) . . ?
Ag7 Ag15 Ag14 145.97(5) . . ?
C43 Ag15 Ag6 129.1(4) . . ?
C49 Ag15 Ag6 49.4(3) . . ?
Ag7 Ag15 Ag6 78.46(4) . . ?
Ag14 Ag15 Ag6 79.70(4) . . ?
C43 Ag15 Ag13 51.0(3) . . ?
C49 Ag15 Ag13 131.3(3) . . ?
Ag7 Ag15 Ag13 96.71(4) . . ?
Ag14 Ag15 Ag13 78.40(3) . . ?
Ag6 Ag15 Ag13 130.71(5) . . ?
C31 Ag16 C25 172.6(5) . . ?
C31 Ag16 C26 150.8(5) . . ?
C25 Ag16 C26 27.7(3) . . ?
C31 Ag16 Ag2 49.1(3) . . ?
C25 Ag16 Ag2 134.5(4) . . ?
C26 Ag16 Ag2 158.4(3) . . ?
C31 Ag16 Ag3 46.2(3) . . ?
C25 Ag16 Ag3 127.3(4) . . ?
C26 Ag16 Ag3 133.0(3) . . ?
Ag2 Ag16 Ag3 63.75(17) . . ?
C31 Ag16 Ag11 137.3(4) . . ?
C25 Ag16 Ag11 49.9(3) . . ?
C26 Ag16 Ag11 62.9(2) . . ?
Ag2 Ag16 Ag11 95.7(2) . . ?
Ag3 Ag16 Ag11 147.3(3) . . ?
C31 Ag16 Ag10 123.6(4) . . ?
C25 Ag16 Ag10 49.1(3) . . ?
C26 Ag16 Ag10 55.7(2) . . ?
Ag2 Ag16 Ag10 129.2(3) . . ?
Ag3 Ag16 Ag10 80.45(14) . . ?
Ag11 Ag16 Ag10 96.55(13) . . ?
C31 Ag6A C25 158(4) . . ?
C31 Ag6A Ag2 52.7(6) . . ?
C25 Ag6A Ag2 145.4(18) . . ?
C31 Ag6A Ag3 49.9(7) . . ?
C25 Ag6A Ag3 136(2) . . ?
Ag2 Ag6A Ag3 69.2(9) . . ?
C31 Ag6A Ag10 126.4(13) . . ?
C25 Ag6A Ag10 50.4(8) . . ?
Ag2 Ag6A Ag10 144(3) . . ?
Ag3 Ag6A Ag10 85.2(13) . . ?
C31 Ag6A Ag11 134(2) . . ?
C25 Ag6A Ag11 49.2(6) . . ?
Ag2 Ag6A Ag11 99.6(9) . . ?
Ag3 Ag6A Ag11 162(3) . . ?
Ag10 Ag6A Ag11 97.7(8) . . ?
C31 Ag6A Ag9 161(3) . . ?
C25 Ag6A Ag9 40.0(10) . . ?
Ag2 Ag6A Ag9 113(2) . . ?
Ag3 Ag6A Ag9 117(3) . . ?
Ag10 Ag6A Ag9 55.9(9) . . ?
Ag11 Ag6A Ag9 53.5(6) . . ?
F18 C81 F17 107.3(19) . . ?
F18 C81 F16 106(2) . . ?
F17 C81 F16 105(2) . . ?
F18 C81 C80 121(2) . . ?
F17 C81 C80 107(2) . . ?
F16 C81 C80 109(4) . . ?
F17A C81A F18A 106(2) . . ?
F17A C81A F16A 105(2) . . ?
F18A C81A F16A 104(2) . . ?
F17A C81A C80 120(2) . . ?
F18A C81A C80 111(2) . . ?
F16A C81A C80 111(4) . . ?
C73 O1 Ag11 128.4(8) . . ?
C75 O2 Ag11 128.3(8) . . ?
C70 O3 Ag10 129.1(7) . . ?
C68 O4 Ag10 126.7(7) . . ?
C78 O5 Ag7 122.8(11) . . ?
C80 O6 Ag7 126.0(9) . . ?
C82 O7 Ag5 121.2(9) . . ?
C82 O7 Ag2 128.9(9) . . ?
Ag5 O7 Ag2 105.2(3) . . ?
C82 O8 Ag4 112.7(9) . . ?
C2 C1 Ag12 159.6(10) . . ?
C2 C1 Ag3 110.8(10) . . ?
Ag12 C1 Ag3 88.4(4) . . ?
C2 C1 Ag5A 87.7(10) . . ?
Ag12 C1 Ag5A 92.7(7) . . ?
Ag3 C1 Ag5A 108.2(10) . . ?
C2 C1 Ag5 93.6(8) . . ?
Ag12 C1 Ag5 92.4(4) . . ?
Ag3 C1 Ag5 91.5(4) . . ?
C1 C2 C3 175.1(12) . . ?
C1 C2 Ag5A 63.4(9) . . ?
C3 C2 Ag5A 119.1(9) . . ?
C2 C3 C6 111.1(14) . . ?
C2 C3 C4A 119(2) . . ?
C2 C3 C5 105.9(13) . . ?
C6 C3 C5 114.1(12) . . ?
C2 C3 C6A 106(2) . . ?
C4A C3 C6A 110.1(16) . . ?
C2 C3 C4 106.8(13) . . ?
C6 C3 C4 110.6(12) . . ?
C5 C3 C4 107.9(12) . . ?
C2 C3 C5A 107.4(16) . . ?
C4A C3 C5A 108.9(16) . . ?
C6A C3 C5A 104.9(15) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C3 C4A H4A1 109.5 . . ?
C3 C4A H4A2 109.5 . . ?
H4A1 C4A H4A2 109.5 . . ?
C3 C4A H4A3 109.5 . . ?
H4A1 C4A H4A3 109.5 . . ?
H4A2 C4A H4A3 109.5 . . ?
C3 C5A H5A1 109.5 . . ?
C3 C5A H5A2 109.5 . . ?
H5A1 C5A H5A2 109.5 . . ?
C3 C5A H5A3 109.5 . . ?
H5A1 C5A H5A3 109.5 . . ?
H5A2 C5A H5A3 109.5 . . ?
C3 C6A H6A1 109.5 . . ?
C3 C6A H6A2 109.5 . . ?
H6A1 C6A H6A2 109.5 . . ?
C3 C6A H6A3 109.5 . . ?
H6A1 C6A H6A3 109.5 . . ?
H6A2 C6A H6A3 109.5 . . ?
C8 C7 Ag5A 145.4(13) . . ?
C8 C7 Ag6 133.3(12) . . ?
Ag5A C7 Ag6 77.6(7) . . ?
C8 C7 Ag4 93.5(10) . . ?
Ag5A C7 Ag4 99.2(11) . . ?
Ag6 C7 Ag4 95.0(4) . . ?
C8 C7 Ag5 146.9(12) . . ?
Ag6 C7 Ag5 79.8(4) . . ?
Ag4 C7 Ag5 82.7(4) . . ?
C7 C8 C9 177.5(17) . . ?
C7 C8 Ag4 59.6(8) . . ?
C9 C8 Ag4 122.3(11) . . ?
C8 C9 C12 107.4(13) . . ?
C8 C9 C10 108.7(15) . . ?
C12 C9 C10 114(2) . . ?
C8 C9 C11 109.5(16) . . ?
C12 C9 C11 107(2) . . ?
C10 C9 C11 109.5(17) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag12 171.0(10) . . ?
C14 C13 Ag14 102.0(9) . . ?
Ag12 C13 Ag14 86.7(4) . . ?
C14 C13 Ag10 93.3(8) . . ?
Ag12 C13 Ag10 84.9(4) . . ?
Ag14 C13 Ag10 115.5(4) . . ?
C13 C14 C15 177.8(13) . . ?
C17 C15 C18 109.3(14) . . ?
C17 C15 C16 110.8(15) . . ?
C18 C15 C16 114.3(14) . . ?
C17 C15 C14 107.9(11) . . ?
C18 C15 C14 108.0(11) . . ?
C16 C15 C14 106.3(12) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C15 C17 H17A 109.5 . . ?
C15 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C15 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 Ag1 170.0(10) . . ?
C20 C19 Ag13 104.4(8) . . ?
Ag1 C19 Ag13 84.6(4) . . ?
C20 C19 Ag11 93.6(7) . . ?
Ag1 C19 Ag11 86.3(4) . . ?
Ag13 C19 Ag11 115.6(4) . . ?
C19 C20 C21 177.8(12) . . ?
C19 C20 Ag11 59.7(6) . . ?
C21 C20 Ag11 122.1(7) . . ?
C20 C21 C24 110.1(10) . . ?
C20 C21 C22 108.4(11) . . ?
C24 C21 C22 108.5(16) . . ?
C20 C21 C23 108.4(11) . . ?
C24 C21 C23 110.5(14) . . ?
C22 C21 C23 110.9(17) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 Ag9 159.0(9) . . ?
C26 C25 Ag16 93.1(8) . . ?
Ag9 C25 Ag16 107.0(5) . . ?
C26 C25 Ag6A 103(2) . . ?
Ag9 C25 Ag6A 96(2) . . ?
C26 C25 Ag10 92.9(7) . . ?
Ag9 C25 Ag10 82.7(4) . . ?
Ag16 C25 Ag10 86.1(4) . . ?
Ag6A C25 Ag10 82.3(13) . . ?
C26 C25 Ag11 109.2(8) . . ?
Ag9 C25 Ag11 79.5(3) . . ?
Ag16 C25 Ag11 84.6(4) . . ?
Ag6A C25 Ag11 84.6(9) . . ?
Ag10 C25 Ag11 156.4(5) . . ?
C25 C26 C27 173.4(12) . . ?
C25 C26 Ag16 59.2(7) . . ?
C27 C26 Ag16 126.7(8) . . ?
C26 C27 C29 108.8(11) . . ?
C26 C27 C30 108.1(11) . . ?
C29 C27 C30 110.0(13) . . ?
C26 C27 C28 110.2(10) . . ?
C29 C27 C28 109.3(12) . . ?
C30 C27 C28 110.4(12) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 Ag16 141.7(9) . . ?
C32 C31 Ag6A 152.1(19) . . ?
C32 C31 Ag3 105.5(9) . . ?
Ag16 C31 Ag3 88.7(4) . . ?
Ag6A C31 Ag3 80.8(18) . . ?
C32 C31 Ag2 130.0(9) . . ?
Ag16 C31 Ag2 83.8(4) . . ?
Ag6A C31 Ag2 76.0(13) . . ?
Ag3 C31 Ag2 91.0(4) . . ?
C31 C32 C33 174.4(13) . . ?
C35 C33 C32 107.4(11) . . ?
C35 C33 C36 111.2(13) . . ?
C32 C33 C36 107.3(12) . . ?
C35 C33 C34 111.7(15) . . ?
C32 C33 C34 108.2(11) . . ?
C36 C33 C34 110.9(13) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 Ag9 167.6(10) . . ?
C38 C37 Ag13 102.4(8) . . ?
Ag9 C37 Ag13 83.5(4) . . ?
C38 C37 Ag14 107.7(9) . . ?
Ag9 C37 Ag14 81.6(4) . . ?
Ag13 C37 Ag14 100.2(4) . . ?
C37 C38 C39 176.3(14) . . ?
C41 C39 C40 116(2) . . ?
C41 C39 C38 110.6(13) . . ?
C40 C39 C38 107.3(14) . . ?
C41 C39 C42 108.3(19) . . ?
C40 C39 C42 106.6(19) . . ?
C38 C39 C42 107.3(13) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 Ag15 179.8(11) . . ?
C44 C43 Ag13 95.3(9) . . ?
Ag15 C43 Ag13 84.9(4) . . ?
C44 C43 Ag7 99.2(8) . . ?
Ag15 C43 Ag7 80.7(4) . . ?
Ag13 C43 Ag7 138.0(6) . . ?
C43 C44 C45 173.9(12) . . ?
C44 C45 C46 108.6(11) . . ?
C44 C45 C48 109.4(11) . . ?
C46 C45 C48 109.9(14) . . ?
C44 C45 C47 108.7(12) . . ?
C46 C45 C47 108.5(13) . . ?
C48 C45 C47 111.7(12) . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C45 C47 H47A 109.5 . . ?
C45 C47 H47B 109.5 . . ?
H47A C47 H47B 109.5 . . ?
C45 C47 H47C 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
C45 C48 H48A 109.5 . . ?
C45 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C45 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 Ag15 174.6(14) . . ?
C50 C49 Ag6 96.5(10) . . ?
Ag15 C49 Ag6 85.2(4) . . ?
C50 C49 Ag14 102.9(11) . . ?
Ag15 C49 Ag14 81.3(4) . . ?
Ag6 C49 Ag14 109.5(5) . . ?
C49 C50 C51A 153(2) . . ?
C49 C50 C51 166(2) . . ?
C49 C50 Ag6 57.2(8) . . ?
C51A C50 Ag6 134.0(13) . . ?
C51 C50 Ag6 116.4(13) . . ?
C54 C51 C53 111.2(16) . . ?
C54 C51 C52 108.8(16) . . ?
C53 C51 C52 109.6(16) . . ?
C54 C51 C50 108(2) . . ?
C53 C51 C50 100(2) . . ?
C52 C51 C50 118(2) . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C51 C53 H53A 109.5 . . ?
C51 C53 H53B 109.5 . . ?
H53A C53 H53B 109.5 . . ?
C51 C53 H53C 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C51 C54 H54A 109.5 . . ?
C51 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C51 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C50 C51A C53A 117(2) . . ?
C50 C51A C52A 97(2) . . ?
C53A C51A C52A 109.0(18) . . ?
C50 C51A C54A 117(3) . . ?
C53A C51A C54A 108.4(17) . . ?
C52A C51A C54A 107.9(17) . . ?
C51A C52A H52D 109.5 . . ?
C51A C52A H52E 109.5 . . ?
H52D C52A H52E 109.5 . . ?
C51A C52A H52F 109.5 . . ?
H52D C52A H52F 109.5 . . ?
H52E C52A H52F 109.5 . . ?
C51A C53A H53D 109.5 . . ?
C51A C53A H53E 109.5 . . ?
H53D C53A H53E 109.5 . . ?
C51A C53A H53F 109.5 . . ?
H53D C53A H53F 109.5 . . ?
H53E C53A H53F 109.5 . . ?
C51A C54A H54D 109.5 . . ?
C51A C54A H54E 109.5 . . ?
H54D C54A H54E 109.5 . . ?
C51A C54A H54F 109.5 . . ?
H54D C54A H54F 109.5 . . ?
H54E C54A H54F 109.5 . . ?
C56 C55 Ag1 143.7(10) . . ?
C56 C55 Ag2 128.3(10) . . ?
Ag1 C55 Ag2 87.2(3) . . ?
C56 C55 Ag8 87.1(8) . . ?
Ag1 C55 Ag8 94.3(4) . . ?
Ag2 C55 Ag8 100.5(4) . . ?
C55 C56 C57 172.6(12) . . ?
C55 C56 Ag8 64.6(7) . . ?
C57 C56 Ag8 122.7(9) . . ?
C60 C57 C59 112.9(19) . . ?
C60 C57 C56 107.7(14) . . ?
C59 C57 C56 109.5(13) . . ?
C60 C57 C58 107.8(17) . . ?
C59 C57 C58 111.2(18) . . ?
C56 C57 C58 107.6(15) . . ?
C57 C58 H58A 109.5 . . ?
C57 C58 H58B 109.5 . . ?
H58A C58 H58B 109.5 . . ?
C57 C58 H58C 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C57 C59 H59A 109.5 . . ?
C57 C59 H59B 109.5 . . ?
H59A C59 H59B 109.5 . . ?
C57 C59 H59C 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C57 C60 H60A 109.5 . . ?
C57 C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C57 C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C62 C61 Ag8 160.2(10) . . ?
C62 C61 Ag4 115.6(9) . . ?
Ag8 C61 Ag4 83.5(4) . . ?
C62 C61 Ag7 87.1(8) . . ?
Ag8 C61 Ag7 96.7(5) . . ?
Ag4 C61 Ag7 94.9(4) . . ?
C61 C62 C63 174.2(12) . . ?
C61 C62 Ag7 64.5(8) . . ?
C63 C62 Ag7 120.8(8) . . ?
C62 C63 C64 107.7(11) . . ?
C62 C63 C66 107.7(11) . . ?
C64 C63 C66 109.6(12) . . ?
C62 C63 C65 110.7(10) . . ?
C64 C63 C65 110.9(12) . . ?
C66 C63 C65 110.2(13) . . ?
C63 C64 H64A 109.5 . . ?
C63 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C63 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C63 C65 H65A 109.5 . . ?
C63 C65 H65B 109.5 . . ?
H65A C65 H65B 109.5 . . ?
C63 C65 H65C 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
C63 C66 H66A 109.5 . . ?
C63 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C63 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
F11 C67 F10 107.9(13) . . ?
F11 C67 F12 106.5(13) . . ?
F10 C67 F12 107.1(14) . . ?
F11 C67 C68 111.9(13) . . ?
F10 C67 C68 114.5(11) . . ?
F12 C67 C68 108.5(12) . . ?
O4 C68 C69 129.7(11) . . ?
O4 C68 C67 114.3(10) . . ?
C69 C68 C67 115.9(11) . . ?
C70 C69 C68 124.3(10) . . ?
C70 C69 H69 117.9 . . ?
C68 C69 H69 117.9 . . ?
O3 C70 C69 129.5(10) . . ?
O3 C70 C71 114.7(10) . . ?
C69 C70 C71 115.8(10) . . ?
F7 C71 F8 108.8(13) . . ?
F7 C71 F9 102.7(14) . . ?
F8 C71 F9 104.6(14) . . ?
F7 C71 C70 112.5(11) . . ?
F8 C71 C70 116.6(11) . . ?
F9 C71 C70 110.5(11) . . ?
F2 C72 F1 109.8(15) . . ?
F2 C72 F3 102.9(14) . . ?
F1 C72 F3 112.1(17) . . ?
F2 C72 C73 109.5(13) . . ?
F1 C72 C73 113.3(14) . . ?
F3 C72 C73 108.7(13) . . ?
O1 C73 C74 128.9(12) . . ?
O1 C73 C72 112.9(12) . . ?
C74 C73 C72 118.1(13) . . ?
C73 C74 C75 124.8(12) . . ?
C73 C74 H74 117.6 . . ?
C75 C74 H74 117.6 . . ?
O2 C75 C74 128.5(12) . . ?
O2 C75 C76 113.6(12) . . ?
C74 C75 C76 117.9(12) . . ?
F4 C76 F5 108.2(15) . . ?
F4 C76 F6 110.0(15) . . ?
F5 C76 F6 106.6(15) . . ?
F4 C76 C75 114.0(13) . . ?
F5 C76 C75 110.2(14) . . ?
F6 C76 C75 107.6(13) . . ?
F14 C77 F13 109(2) . . ?
F14 C77 F15 111(3) . . ?
F13 C77 F15 104.7(17) . . ?
F14 C77 C78 111.3(18) . . ?
F13 C77 C78 108(2) . . ?
F15 C77 C78 113.4(17) . . ?
O5 C78 C79 130.5(17) . . ?
O5 C78 C77 114.9(17) . . ?
C79 C78 C77 114.6(18) . . ?
C80 C79 C78 123.1(16) . . ?
C80 C79 H79 118.4 . . ?
C78 C79 H79 118.4 . . ?
O6 C80 C79 130.5(14) . . ?
O6 C80 C81A 107.3(14) . . ?
C79 C80 C81A 120.9(15) . . ?
O6 C80 C81 119.1(16) . . ?
C79 C80 C81 109.0(17) . . ?
O8 C82 O7 129.5(13) . . ?
O8 C82 C83 116.9(12) . . ?
O7 C82 C83 113.5(13) . . ?
F21A C83 F20A 110(2) . . ?
F19 C83 F21 107.8(15) . . ?
F21A C83 F19A 106.2(18) . . ?
F20A C83 F19A 104.3(17) . . ?
F19 C83 F20 104.3(16) . . ?
F21 C83 F20 102.0(13) . . ?
F19 C83 C82 120.2(18) . . ?
F21A C83 C82 123(3) . . ?
F20A C83 C82 110(2) . . ?
F21 C83 C82 112.0(17) . . ?
F19A C83 C82 101(2) . . ?
F20 C83 C82 108.9(14) . . ?

_refine_diff_density_max         1.262
_refine_diff_density_min         -1.336
_refine_diff_density_rms         0.179

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex4
_database_code_depnum_ccdc_archive 'CCDC 1584344'
_audit_update_record             
;
2017-11-07 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C88 H110 Ag17 F21 O10'
_chemical_formula_weight         3560.54

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.4518(11)
_cell_length_b                   18.0340(14)
_cell_length_c                   24.8520(19)
_cell_angle_alpha                69.198(2)
_cell_angle_beta                 73.412(2)
_cell_angle_gamma                68.675(2)
_cell_volume                     5548.6(7)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9031
_cell_measurement_theta_min      2.9262
_cell_measurement_theta_max      25.4538

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.131
_exptl_crystal_F_000             3412
_exptl_transmission_factor_min   0.5953
_exptl_transmission_factor_max   0.7452
_exptl_crystal_size_max          0.136
_exptl_crystal_size_mid          0.105
_exptl_crystal_size_min          0.085
_exptl_absorpt_coefficient_mu    3.006
_shelx_estimated_absorpt_T_min   0.685
_shelx_estimated_absorpt_T_max   0.784
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            36908
_diffrn_reflns_av_unetI/netI     0.0363
_diffrn_reflns_av_R_equivalents  0.0237
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_theta_min         2.821
_diffrn_reflns_theta_max         25.027
_diffrn_reflns_theta_full        25.027
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measured_fraction_theta_full 0.989
_diffrn_reflns_Laue_measured_fraction_max 0.989
_diffrn_reflns_Laue_measured_fraction_full 0.989
_diffrn_reflns_point_group_measured_fraction_max 0.989
_diffrn_reflns_point_group_measured_fraction_full 0.989
_reflns_number_total             19397
_reflns_number_gt                16357
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0257P)²+47.4395P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         19397
_refine_ls_number_parameters     1466
_refine_ls_number_restraints     958
_refine_ls_R_factor_all          0.0575
_refine_ls_R_factor_gt           0.0463
_refine_ls_wR_factor_ref         0.1137
_refine_ls_wR_factor_gt          0.1054
_refine_ls_goodness_of_fit_ref   1.138
_refine_ls_restrained_S_all      1.124
_refine_ls_shift/su_max          0.012
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.30358(4) 0.34009(3) 0.76164(2) 0.03050(12) Uani 1 1 d . . . . .
Ag2A Ag 0.2593(18) 0.4614(13) 0.6289(10) 0.062(6) Uani 0.0843 1 d . . P A .
Ag2B Ag 0.27765(14) 0.47848(10) 0.61477(7) 0.0357(3) Uani 0.9157 1 d . . P A .
Ag3A Ag 0.347(4) 0.537(6) 0.7692(10) 0.056(11) Uani 0.065(19) 1 d . . P A 1
Ag3B Ag 0.34292(17) 0.56513(15) 0.77606(12) 0.0382(7) Uani 0.935(19) 1 d . . P
A 2
Ag4A Ag 0.1018(3) 0.3780(2) 0.8333(2) 0.0412(8) Uani 0.7883 1 d . . P A .
Ag4B Ag 0.0966(11) 0.3772(9) 0.8262(7) 0.043(3) Uani 0.2117 1 d . . P A .
Ag5 Ag 0.38727(5) 0.07599(4) 0.84549(3) 0.04253(15) Uani 1 1 d . . . . .
Ag6A Ag 0.3571(9) 0.2900(8) 0.6268(8) 0.0412(19) Uani 0.26(2) 1 d . . P A 1
Ag6B Ag 0.3364(5) 0.2979(3) 0.6419(3) 0.0381(9) Uani 0.69(2) 1 d . . P A 2
Ag6C Ag 0.3033(13) 0.2605(14) 0.6813(12) 0.071(9) Uani 0.051(4) 1 d . . P A 3
Ag7A Ag 0.5797(4) 0.12588(18) 0.78898(17) 0.0457(7) Uani 0.71(2) 1 d . . P A 1
Ag7B Ag 0.5657(14) 0.1301(8) 0.7903(5) 0.072(4) Uani 0.25(2) 1 d . . P A 2
Ag7C Ag 0.4991(13) 0.2162(18) 0.7552(12) 0.070(10) Uani 0.033(2) 1 d . . P A 3
Ag8A Ag 0.2932(7) 0.1515(10) 0.7437(3) 0.032(2) Uani 0.28(2) 1 d . . P A 1
Ag8B Ag 0.2813(4) 0.1820(7) 0.7427(2) 0.0360(11) Uani 0.49(2) 1 d . . P A 2
Ag8C Ag 0.2922(13) 0.144(3) 0.7449(7) 0.133(9) Uani 0.23(2) 1 d . . P A 3
Ag9A Ag 0.1225(2) 0.4992(4) 0.71739(12) 0.0377(10) Uani 0.57(2) 1 d . . P A 1
Ag9B Ag 0.0975(11) 0.5353(13) 0.71725(18) 0.069(3) Uani 0.43(2) 1 d . . P A 2
Ag10 Ag 0.25325(4) 0.61526(3) 0.65898(2) 0.03268(13) Uani 1 1 d . . . . .
Ag11 Ag 0.14429(4) 0.52648(3) 0.82636(3) 0.03485(13) Uani 1 1 d . . . . .
Ag12 Ag 0.50300(4) 0.13400(3) 0.68502(3) 0.03672(13) Uani 1 1 d . . . . .
Ag13 Ag 0.19997(4) 0.19931(3) 0.86123(3) 0.03857(14) Uani 1 1 d . . . . .
Ag14 Ag 0.51086(4) 0.28385(3) 0.69439(3) 0.03791(14) Uani 1 1 d . . . . .
Ag15 Ag 0.2997(12) 0.3899(7) 0.8684(5) 0.045(3) Uani 0.2687 1 d . . P A .
A15 Ag 0.3146(4) 0.3864(3) 0.86347(16) 0.0330(7) Uani 0.7313 1 d . . P A .
Ag16 Ag 0.42259(4) 0.47134(3) 0.67058(3) 0.03952(14) Uani 1 1 d . . . . .
Ag17 Ag 0.38088(4) 0.20351(4) 0.88853(3) 0.04003(14) Uani 1 1 d . . . . .
F1 F 0.4570(9) -0.1058(4) 0.8596(4) 0.184(6) Uani 1 1 d . . . . .
F2 F 0.5248(9) -0.1993(5) 0.8186(4) 0.143(4) Uani 1 1 d . U . . .
F3 F 0.6078(10) -0.1615(8) 0.8491(5) 0.183(5) Uani 1 1 d . U . . .
F4 F 0.6866(8) -0.1567(6) 0.6178(5) 0.149(4) Uani 1 1 d . . . . .
F5 F 0.7983(8) -0.1314(9) 0.6341(6) 0.188(6) Uani 1 1 d . U . . .
F6 F 0.7306(11) -0.0523(5) 0.5689(4) 0.197(7) Uani 1 1 d . U . . .
F7 F 0.0828(17) 0.9223(8) 0.5508(9) 0.142(9) Uani 0.69(2) 1 d D U P B 1
F8 F 0.2383(13) 0.9049(8) 0.5406(7) 0.129(9) Uani 0.69(2) 1 d D U P B 1
F9 F 0.1347(9) 0.9652(5) 0.5996(5) 0.075(4) Uani 0.69(2) 1 d D U P B 1
F7A F 0.157(3) 0.8900(14) 0.5254(8) 0.076(9) Uani 0.31(2) 1 d D U P B 2
F8A F 0.082(3) 0.9643(17) 0.5840(14) 0.19(3) Uani 0.31(2) 1 d D U P B 2
F9A F 0.243(2) 0.922(2) 0.5649(16) 0.114(14) Uani 0.31(2) 1 d D U P B 2
F10 F -0.0138(12) 0.8460(7) 0.7833(6) 0.108(5) Uani 0.604(17) 1 d D U P C 1
F11 F 0.1004(9) 0.7535(8) 0.8251(5) 0.108(5) Uani 0.604(17) 1 d D U P C 1
F12 F -0.0153(11) 0.7182(10) 0.8137(6) 0.100(6) Uani 0.604(17) 1 d D U P C 1
F10A F 0.0375(18) 0.8297(12) 0.8007(9) 0.108(7) Uani 0.396(17) 1 d D U P C 2
F11A F 0.026(2) 0.7086(13) 0.8300(9) 0.108(7) Uani 0.396(17) 1 d D U P C 2
F12A F -0.0638(11) 0.8009(16) 0.7737(8) 0.120(9) Uani 0.396(17) 1 d D U P C 2
F13 F 0.1536(8) 0.4642(6) 0.4517(4) 0.152(5) Uani 1 1 d . . . . .
F14 F 0.2731(7) 0.3599(6) 0.4420(4) 0.138(4) Uani 1 1 d . . . . .
F15 F 0.3022(13) 0.4705(10) 0.4178(4) 0.223(8) Uani 1 1 d . . . . .
F16 F 0.4541(7) 0.2973(6) 1.0470(3) 0.114(3) Uani 1 1 d . . . . .
F17 F 0.5817(7) 0.2098(5) 1.0169(4) 0.134(4) Uani 1 1 d . . . . .
F18 F 0.5660(6) 0.3374(5) 0.9800(3) 0.108(3) Uani 1 1 d . . . . .
F19 F -0.2193(4) 0.3099(5) 0.9071(4) 0.111(3) Uani 1 1 d . . . . .
F20 F -0.1548(5) 0.1862(5) 0.9142(4) 0.111(3) Uani 1 1 d . . . . .
F21 F -0.1569(6) 0.2332(7) 0.9802(3) 0.133(4) Uani 1 1 d . . . . .
O1 O 0.2268(4) 0.7588(3) 0.6090(2) 0.0448(13) Uani 1 1 d . . . . .
O2 O 0.1537(4) 0.6801(3) 0.7353(2) 0.0410(13) Uani 1 1 d . . . . .
O3 O 0.5035(5) 0.0055(3) 0.7661(3) 0.0541(16) Uani 1 1 d . . . . .
O4 O 0.6115(5) 0.0271(4) 0.6418(3) 0.0601(17) Uani 1 1 d . . . . .
O5 O 0.2551(9) 0.4769(5) 0.5277(4) 0.118(4) Uani 1 1 d . . . . .
O6 O 0.2846(8) 0.3436(5) 0.5487(4) 0.112(4) Uani 1 1 d . . . . .
O7 O 0.4097(5) 0.3567(4) 0.9319(3) 0.0608(17) Uani 1 1 d . . . . .
O8 O 0.4683(6) 0.2209(4) 0.9465(4) 0.076(2) Uani 1 1 d . . . . .
O9 O -0.0427(4) 0.3363(4) 0.8718(3) 0.0580(17) Uani 1 1 d . . . . .
O10 O 0.0319(5) 0.2008(4) 0.8955(4) 0.067(2) Uani 1 1 d . . . . .
C1 C 0.1458(6) 0.5828(5) 0.6272(3) 0.0361(16) Uani 1 1 d . U . . .
C2 C 0.0840(5) 0.6278(4) 0.5982(3) 0.0318(14) Uani 1 1 d . U . . .
C3 C 0.0064(6) 0.6823(5) 0.5612(4) 0.0486(19) Uani 1 1 d . U . . .
C4 C 0.0287(9) 0.6542(8) 0.5073(5) 0.083(3) Uani 1 1 d . U . . .
H4A H -0.0221 0.6899 0.4828 0.124 Uiso 1 1 calc R U . . .
H4B H 0.0958 0.6576 0.4853 0.124 Uiso 1 1 calc R U . . .
H4C H 0.0270 0.5967 0.5189 0.124 Uiso 1 1 calc R U . . .
C5 C 0.0103(8) 0.7725(6) 0.5451(5) 0.076(3) Uani 1 1 d . U . . .
H5A H -0.0401 0.8098 0.5207 0.115 Uiso 1 1 calc R U . . .
H5B H -0.0041 0.7888 0.5810 0.115 Uiso 1 1 calc R U . . .
H5C H 0.0777 0.7758 0.5236 0.115 Uiso 1 1 calc R U . . .
C6 C -0.0977(7) 0.6772(7) 0.5965(5) 0.064(3) Uani 1 1 d . U . . .
H6A H -0.1493 0.7130 0.5725 0.096 Uiso 1 1 calc R U . . .
H6B H -0.0997 0.6198 0.6084 0.096 Uiso 1 1 calc R U . . .
H6C H -0.1109 0.6956 0.6314 0.096 Uiso 1 1 calc R U . . .
C7 C 0.1831(5) 0.3364(4) 0.7348(3) 0.0308(15) Uani 1 1 d . U . . .
C8 C 0.1181(5) 0.3342(4) 0.7135(3) 0.0321(15) Uani 1 1 d . U . . .
C9 C 0.0368(6) 0.3314(6) 0.6897(4) 0.0450(18) Uani 1 1 d . U . . .
C10 C -0.0094(10) 0.4150(8) 0.6528(6) 0.094(4) Uani 1 1 d . U . . .
H10A H -0.0631 0.4129 0.6371 0.142 Uiso 1 1 calc R U . . .
H10B H -0.0378 0.4542 0.6764 0.142 Uiso 1 1 calc R U . . .
H10C H 0.0423 0.4331 0.6204 0.142 Uiso 1 1 calc R U . . .
C11 C -0.0400(7) 0.2987(8) 0.7389(5) 0.070(3) Uani 1 1 d . U . . .
H11A H -0.0935 0.2970 0.7228 0.104 Uiso 1 1 calc R U . . .
H11B H -0.0072 0.2426 0.7613 0.104 Uiso 1 1 calc R U . . .
H11C H -0.0693 0.3350 0.7647 0.104 Uiso 1 1 calc R U . . .
C12 C 0.0813(8) 0.2706(9) 0.6524(6) 0.085(4) Uani 1 1 d . U . . .
H12A H 0.0276 0.2687 0.6367 0.128 Uiso 1 1 calc R U . . .
H12B H 0.1329 0.2890 0.6201 0.128 Uiso 1 1 calc R U . . .
H12C H 0.1119 0.2152 0.6767 0.128 Uiso 1 1 calc R U . . .
C13 C 0.4108(6) 0.5841(5) 0.6832(3) 0.0338(15) Uani 1 1 d . U . . .
C14 C 0.4342(5) 0.6416(4) 0.6847(3) 0.0311(14) Uani 1 1 d . U . . .
C15 C 0.4638(6) 0.7150(5) 0.6804(3) 0.0412(17) Uani 1 1 d . U . . .
C16 C 0.3820(9) 0.7696(6) 0.7142(5) 0.066(3) Uani 1 1 d . U . . .
H16A H 0.4027 0.8173 0.7109 0.098 Uiso 1 1 calc R U . . .
H16B H 0.3198 0.7891 0.6983 0.098 Uiso 1 1 calc R U . . .
H16C H 0.3699 0.7381 0.7554 0.098 Uiso 1 1 calc R U . . .
C17 C 0.4820(7) 0.7627(5) 0.6153(4) 0.054(2) Uani 1 1 d . U . . .
H17A H 0.5016 0.8115 0.6110 0.080 Uiso 1 1 calc R U . . .
H17B H 0.5361 0.7266 0.5938 0.080 Uiso 1 1 calc R U . . .
H17C H 0.4199 0.7806 0.5997 0.080 Uiso 1 1 calc R U . . .
C18 C 0.5620(8) 0.6833(6) 0.7041(5) 0.066(3) Uani 1 1 d . U . . .
H18A H 0.5828 0.7305 0.7018 0.099 Uiso 1 1 calc R U . . .
H18B H 0.5513 0.6501 0.7450 0.099 Uiso 1 1 calc R U . . .
H18C H 0.6148 0.6490 0.6808 0.099 Uiso 1 1 calc R U . . .
C19 C 0.2583(6) 0.5272(4) 0.8630(3) 0.0333(15) Uani 1 1 d . U . . .
C20 C 0.2986(6) 0.5548(5) 0.8845(3) 0.0348(15) Uani 1 1 d . U . . .
C21 C 0.3389(6) 0.5866(5) 0.9181(3) 0.0424(17) Uani 1 1 d . U . . .
C22 C 0.2935(9) 0.6791(6) 0.9062(5) 0.066(3) Uani 1 1 d . U . . .
H22A H 0.3205 0.6994 0.9284 0.099 Uiso 1 1 calc R U . . .
H22B H 0.3106 0.7058 0.8643 0.099 Uiso 1 1 calc R U . . .
H22C H 0.2200 0.6924 0.9180 0.099 Uiso 1 1 calc R U . . .
C23 C 0.4539(7) 0.5636(7) 0.9012(4) 0.063(3) Uani 1 1 d . U . . .
H23A H 0.4805 0.5844 0.9232 0.095 Uiso 1 1 calc R U . . .
H23B H 0.4820 0.5031 0.9104 0.095 Uiso 1 1 calc R U . . .
H23C H 0.4731 0.5884 0.8592 0.095 Uiso 1 1 calc R U . . .
C24 C 0.3098(8) 0.5437(6) 0.9831(4) 0.059(2) Uani 1 1 d . U . . .
H24A H 0.3351 0.5632 1.0066 0.088 Uiso 1 1 calc R U . . .
H24B H 0.2361 0.5569 0.9939 0.088 Uiso 1 1 calc R U . . .
H24C H 0.3395 0.4835 0.9903 0.088 Uiso 1 1 calc R U . . .
C25 C 0.4345(5) 0.3470(4) 0.7768(3) 0.0325(15) Uani 1 1 d . U . . .
C26 C 0.5162(5) 0.3512(4) 0.7762(3) 0.0311(14) Uani 1 1 d . U . . .
C27 C 0.6157(6) 0.3568(5) 0.7772(4) 0.0417(17) Uani 1 1 d . U . . .
C28 C 0.6683(7) 0.3871(7) 0.7151(5) 0.068(3) Uani 1 1 d . U . . .
H28A H 0.7340 0.3908 0.7157 0.102 Uiso 1 1 calc R U . . .
H28B H 0.6783 0.3481 0.6933 0.102 Uiso 1 1 calc R U . . .
H28C H 0.6268 0.4419 0.6961 0.102 Uiso 1 1 calc R U . . .
C29 C 0.5967(7) 0.4178(6) 0.8117(5) 0.059(2) Uani 1 1 d . U . . .
H29A H 0.6612 0.4227 0.8131 0.089 Uiso 1 1 calc R U . . .
H29B H 0.5545 0.4723 0.7926 0.089 Uiso 1 1 calc R U . . .
H29C H 0.5620 0.3976 0.8516 0.089 Uiso 1 1 calc R U . . .
C30 C 0.6789(6) 0.2709(6) 0.8078(5) 0.055(2) Uani 1 1 d . U . . .
H30A H 0.7448 0.2739 0.8087 0.082 Uiso 1 1 calc R U . . .
H30B H 0.6439 0.2523 0.8479 0.082 Uiso 1 1 calc R U . . .
H30C H 0.6885 0.2316 0.7864 0.082 Uiso 1 1 calc R U . . .
C31 C 0.3587(6) 0.1625(4) 0.6561(3) 0.0354(16) Uani 1 1 d . U . . .
C32 C 0.3525(6) 0.1314(4) 0.6221(3) 0.0388(16) Uani 1 1 d . U . . .
C33 C 0.3473(8) 0.0945(5) 0.5792(4) 0.056(2) Uani 1 1 d . U . . .
C34 C 0.4277(12) 0.1130(9) 0.5253(5) 0.105(5) Uani 1 1 d . U . . .
H34A H 0.4257 0.0891 0.4961 0.157 Uiso 1 1 calc R U . . .
H34B H 0.4146 0.1732 0.5088 0.157 Uiso 1 1 calc R U . . .
H34C H 0.4945 0.0886 0.5366 0.157 Uiso 1 1 calc R U . . .
C35 C 0.3697(11) 0.0005(6) 0.6055(6) 0.091(4) Uani 1 1 d . U . . .
H35A H 0.3663 -0.0241 0.5770 0.136 Uiso 1 1 calc R U . . .
H35B H 0.4375 -0.0229 0.6154 0.136 Uiso 1 1 calc R U . . .
H35C H 0.3198 -0.0117 0.6409 0.136 Uiso 1 1 calc R U . . .
C36 C 0.2439(10) 0.1300(8) 0.5627(6) 0.088(3) Uani 1 1 d . U . . .
H36A H 0.2420 0.1047 0.5341 0.132 Uiso 1 1 calc R U . . .
H36B H 0.1930 0.1180 0.5977 0.132 Uiso 1 1 calc R U . . .
H36C H 0.2295 0.1901 0.5454 0.132 Uiso 1 1 calc R U . . .
C37 C 0.0201(5) 0.5180(5) 0.8030(3) 0.0368(17) Uani 1 1 d . U . . .
C38 C -0.0692(6) 0.5444(5) 0.8055(3) 0.0373(16) Uani 1 1 d . U . . .
C39 C -0.1794(6) 0.5761(5) 0.8100(4) 0.0464(19) Uani 1 1 d D U . . .
C40 C -0.2133(12) 0.6684(7) 0.7868(8) 0.081(5) Uani 0.751(19) 1 d D U P D 1
H40A H -0.2869 0.6877 0.7903 0.122 Uiso 0.751(19) 1 calc R U P D 1
H40B H -0.1931 0.6932 0.8092 0.122 Uiso 0.751(19) 1 calc R U P D 1
H40C H -0.1820 0.6849 0.7455 0.122 Uiso 0.751(19) 1 calc R U P D 1
C41 C -0.2274(9) 0.5433(10) 0.8729(5) 0.073(5) Uani 0.751(19) 1 d D U P D 1
H41A H -0.3011 0.5639 0.8768 0.110 Uiso 0.751(19) 1 calc R U P D 1
H41B H -0.2061 0.4825 0.8842 0.110 Uiso 0.751(19) 1 calc R U P D 1
H41C H -0.2062 0.5623 0.8986 0.110 Uiso 0.751(19) 1 calc R U P D 1
C42 C -0.2067(10) 0.5369(9) 0.7711(7) 0.065(4) Uani 0.751(19) 1 d D U P D 1
H42A H -0.2799 0.5563 0.7726 0.098 Uiso 0.751(19) 1 calc R U P D 1
H42B H -0.1725 0.5539 0.7305 0.098 Uiso 0.751(19) 1 calc R U P D 1
H42C H -0.1847 0.4763 0.7860 0.098 Uiso 0.751(19) 1 calc R U P D 1
C40A C -0.207(4) 0.6513(19) 0.7578(14) 0.071(12) Uani 0.249(19) 1 d D U P D 2
H40D H -0.2801 0.6723 0.7610 0.107 Uiso 0.249(19) 1 calc R U P D 2
H40E H -0.1808 0.6948 0.7574 0.107 Uiso 0.249(19) 1 calc R U P D 2
H40F H -0.1763 0.6350 0.7215 0.107 Uiso 0.249(19) 1 calc R U P D 2
C41A C -0.219(3) 0.612(3) 0.8643(13) 0.064(10) Uani 0.249(19) 1 d D U P D 2
H41D H -0.2932 0.6340 0.8697 0.096 Uiso 0.249(19) 1 calc R U P D 2
H41E H -0.2002 0.5672 0.8994 0.096 Uiso 0.249(19) 1 calc R U P D 2
H41F H -0.1901 0.6559 0.8578 0.096 Uiso 0.249(19) 1 calc R U P D 2
C42A C -0.237(3) 0.518(2) 0.819(2) 0.076(11) Uani 0.249(19) 1 d D U P D 2
H42D H -0.3090 0.5475 0.8211 0.113 Uiso 0.249(19) 1 calc R U P D 2
H42E H -0.2133 0.4931 0.7863 0.113 Uiso 0.249(19) 1 calc R U P D 2
H42F H -0.2262 0.4734 0.8556 0.113 Uiso 0.249(19) 1 calc R U P D 2
C43 C 0.4360(5) 0.3928(4) 0.6167(3) 0.0303(15) Uani 1 1 d . U . . .
C44 C 0.5009(6) 0.3582(4) 0.5831(3) 0.0313(14) Uani 1 1 d . U . . .
C45 C 0.5787(6) 0.3292(5) 0.5342(3) 0.0386(17) Uani 1 1 d . U . . .
C46 C 0.6786(7) 0.3358(8) 0.5371(5) 0.077(3) Uani 1 1 d . U . . .
H46A H 0.7306 0.3172 0.5055 0.115 Uiso 1 1 calc R U . . .
H46B H 0.6719 0.3936 0.5327 0.115 Uiso 1 1 calc R U . . .
H46C H 0.6980 0.3009 0.5749 0.115 Uiso 1 1 calc R U . . .
C47 C 0.5446(9) 0.3861(6) 0.4771(4) 0.075(3) Uani 1 1 d . U . . .
H47A H 0.5939 0.3688 0.4442 0.112 Uiso 1 1 calc R U . . .
H47B H 0.4786 0.3829 0.4766 0.112 Uiso 1 1 calc R U . . .
H47C H 0.5393 0.4433 0.4737 0.112 Uiso 1 1 calc R U . . .
C48 C 0.5903(8) 0.2402(5) 0.5395(4) 0.059(2) Uani 1 1 d . U . . .
H48A H 0.6414 0.2232 0.5071 0.088 Uiso 1 1 calc R U . . .
H48B H 0.6114 0.2043 0.5767 0.088 Uiso 1 1 calc R U . . .
H48C H 0.5256 0.2355 0.5381 0.088 Uiso 1 1 calc R U . . .
C49 C 0.6315(6) 0.1666(5) 0.6973(3) 0.0370(16) Uani 1 1 d . U . . .
C50 C 0.7209(6) 0.1382(5) 0.6857(4) 0.0398(17) Uani 1 1 d . U . . .
C51 C 0.8309(7) 0.1008(7) 0.6669(5) 0.073(3) Uani 1 1 d . U . . .
C52 C 0.8850(11) 0.1565(14) 0.6647(12) 0.192(9) Uani 1 1 d . U . . .
H52A H 0.8581 0.2114 0.6387 0.288 Uiso 1 1 calc R U . . .
H52B H 0.8763 0.1611 0.7041 0.288 Uiso 1 1 calc R U . . .
H52C H 0.9570 0.1343 0.6500 0.288 Uiso 1 1 calc R U . . .
C53 C 0.8475(10) 0.0976(10) 0.6038(6) 0.120(5) Uani 1 1 d . U . . .
H53A H 0.8275 0.1542 0.5781 0.179 Uiso 1 1 calc R U . . .
H53B H 0.9190 0.0709 0.5910 0.179 Uiso 1 1 calc R U . . .
H53C H 0.8065 0.0658 0.6021 0.179 Uiso 1 1 calc R U . . .
C54 C 0.8612(12) 0.0161(10) 0.7038(8) 0.174(9) Uani 1 1 d . U . . .
H54A H 0.8198 -0.0151 0.7017 0.261 Uiso 1 1 calc R U . . .
H54B H 0.9325 -0.0102 0.6902 0.261 Uiso 1 1 calc R U . . .
H54C H 0.8517 0.0166 0.7443 0.261 Uiso 1 1 calc R U . . .
C55 C 0.5033(5) 0.0843(5) 0.8791(3) 0.0395(18) Uani 1 1 d . U . . .
C56 C 0.5828(6) 0.0491(5) 0.8963(4) 0.050(2) Uani 1 1 d . U . . .
C57 C 0.6723(7) 0.0014(6) 0.9244(5) 0.075(3) Uani 1 1 d D U . . .
C58 C 0.6607(16) -0.0840(10) 0.9603(8) 0.083(6) Uani 0.619(19) 1 d D U P E 1
H58A H 0.5944 -0.0778 0.9859 0.125 Uiso 0.619(19) 1 calc R U P E 1
H58B H 0.6667 -0.1157 0.9340 0.125 Uiso 0.619(19) 1 calc R U P E 1
H58C H 0.7137 -0.1135 0.9842 0.125 Uiso 0.619(19) 1 calc R U P E 1
C59 C 0.7694(12) -0.0016(16) 0.8847(10) 0.135(11) Uani 0.619(19) 1 d D U P E 1
H59A H 0.8243 -0.0343 0.9070 0.203 Uiso 0.619(19) 1 calc R U P E 1
H59B H 0.7744 -0.0275 0.8549 0.203 Uiso 0.619(19) 1 calc R U P E 1
H59C H 0.7747 0.0548 0.8657 0.203 Uiso 0.619(19) 1 calc R U P E 1
C60 C 0.6645(15) 0.0443(13) 0.9726(10) 0.112(8) Uani 0.619(19) 1 d D U P E 1
H60A H 0.5995 0.0465 0.9993 0.168 Uiso 0.619(19) 1 calc R U P E 1
H60B H 0.7195 0.0119 0.9948 0.168 Uiso 0.619(19) 1 calc R U P E 1
H60C H 0.6697 0.1008 0.9532 0.168 Uiso 0.619(19) 1 calc R U P E 1
C58A C 0.730(3) -0.0659(19) 0.8888(16) 0.124(12) Uani 0.381(19) 1 d D U P E 2
H58D H 0.7470 -0.0375 0.8472 0.185 Uiso 0.381(19) 1 calc R U P E 2
H58E H 0.7926 -0.1016 0.9037 0.185 Uiso 0.381(19) 1 calc R U P E 2
H58F H 0.6870 -0.0998 0.8938 0.185 Uiso 0.381(19) 1 calc R U P E 2
C59A C 0.736(2) 0.0608(18) 0.9079(16) 0.100(11) Uani 0.381(19) 1 d D U P E 2
H59D H 0.7495 0.0835 0.8652 0.151 Uiso 0.381(19) 1 calc R U P E 2
H59E H 0.6990 0.1063 0.9257 0.151 Uiso 0.381(19) 1 calc R U P E 2
H59F H 0.8000 0.0307 0.9220 0.151 Uiso 0.381(19) 1 calc R U P E 2
C60A C 0.645(3) -0.038(2) 0.9873(9) 0.127(15) Uani 0.381(19) 1 d D U P E 2
H60D H 0.7071 -0.0687 1.0039 0.191 Uiso 0.381(19) 1 calc R U P E 2
H60E H 0.6038 0.0049 1.0070 0.191 Uiso 0.381(19) 1 calc R U P E 2
H60F H 0.6074 -0.0762 0.9929 0.191 Uiso 0.381(19) 1 calc R U P E 2
C61 C 0.2416(6) 0.0886(5) 0.8287(4) 0.048(2) Uani 1 1 d . U . . .
C62 C 0.1938(8) 0.0433(5) 0.8390(6) 0.069(3) Uani 1 1 d D U . . .
C63 C 0.1259(15) -0.0127(11) 0.8686(11) 0.112(7) Uani 0.542(18) 1 d D U P F 1
C64 C 0.193(2) -0.0978(14) 0.8605(17) 0.145(11) Uani 0.542(18) 1 d D U P F 1
H64A H 0.1539 -0.1380 0.8787 0.217 Uiso 0.542(18) 1 calc R U P F 1
H64B H 0.2149 -0.0934 0.8187 0.217 Uiso 0.542(18) 1 calc R U P F 1
H64C H 0.2517 -0.1164 0.8791 0.217 Uiso 0.542(18) 1 calc R U P F 1
C65 C 0.076(2) -0.0165(17) 0.9325(11) 0.132(7) Uani 0.542(18) 1 d D U P F 1
H65A H 0.0343 -0.0543 0.9469 0.197 Uiso 0.542(18) 1 calc R U P F 1
H65B H 0.1285 -0.0366 0.9564 0.197 Uiso 0.542(18) 1 calc R U P F 1
H65C H 0.0336 0.0390 0.9351 0.197 Uiso 0.542(18) 1 calc R U P F 1
C66 C 0.049(2) 0.030(3) 0.8271(13) 0.132(7) Uani 0.542(18) 1 d D U P F 1
H66A H -0.0030 0.0010 0.8400 0.197 Uiso 0.542(18) 1 calc R U P F 1
H66B H 0.0167 0.0878 0.8277 0.197 Uiso 0.542(18) 1 calc R U P F 1
H66C H 0.0832 0.0280 0.7873 0.197 Uiso 0.542(18) 1 calc R U P F 1
C63A C 0.1449(17) -0.0139(13) 0.8335(12) 0.095(7) Uani 0.458(18) 1 d D U P F 2
C64A C 0.193(3) -0.052(2) 0.7828(16) 0.165(14) Uani 0.458(18) 1 d D U P F 2
H64D H 0.1548 -0.0879 0.7837 0.248 Uiso 0.458(18) 1 calc R U P F 2
H64E H 0.1917 -0.0079 0.7458 0.248 Uiso 0.458(18) 1 calc R U P F 2
H64F H 0.2628 -0.0851 0.7863 0.248 Uiso 0.458(18) 1 calc R U P F 2
C65A C 0.032(2) 0.028(3) 0.833(2) 0.149(12) Uani 0.458(18) 1 d D U P F 2
H65D H 0.0020 -0.0104 0.8294 0.224 Uiso 0.458(18) 1 calc R U P F 2
H65E H -0.0008 0.0431 0.8696 0.224 Uiso 0.458(18) 1 calc R U P F 2
H65F H 0.0227 0.0780 0.7998 0.224 Uiso 0.458(18) 1 calc R U P F 2
C66A C 0.156(3) -0.084(2) 0.8913(16) 0.173(16) Uani 0.458(18) 1 d D U P F 2
H66D H 0.1258 -0.1253 0.8924 0.259 Uiso 0.458(18) 1 calc R U P F 2
H66E H 0.2273 -0.1099 0.8938 0.259 Uiso 0.458(18) 1 calc R U P F 2
H66F H 0.1206 -0.0604 0.9243 0.259 Uiso 0.458(18) 1 calc R U P F 2
C67 C 0.2203(5) 0.2825(4) 0.9022(3) 0.0290(14) Uani 1 1 d . U . . .
C68 C 0.1629(5) 0.3105(4) 0.9404(3) 0.0361(16) Uani 1 1 d . U . . .
C69 C 0.0945(7) 0.3360(6) 0.9926(4) 0.056(2) Uani 1 1 d . U . . .
C70 C 0.1522(10) 0.3530(10) 1.0253(6) 0.103(4) Uani 1 1 d . U . . .
H70A H 0.1070 0.3696 1.0594 0.154 Uiso 1 1 calc R U . . .
H70B H 0.2066 0.3028 1.0381 0.154 Uiso 1 1 calc R U . . .
H70C H 0.1812 0.3978 0.9997 0.154 Uiso 1 1 calc R U . . .
C71 C 0.0042(8) 0.4126(7) 0.9725(5) 0.085(4) Uani 1 1 d . U . . .
H71A H -0.0317 0.3986 0.9512 0.127 Uiso 1 1 calc R U . . .
H71B H -0.0421 0.4281 1.0068 0.127 Uiso 1 1 calc R U . . .
H71C H 0.0297 0.4593 0.9468 0.127 Uiso 1 1 calc R U . . .
C72 C 0.0478(9) 0.2651(8) 1.0295(5) 0.084(3) Uani 1 1 d . U . . .
H72A H 0.0106 0.2564 1.0060 0.125 Uiso 1 1 calc R U . . .
H72B H 0.1015 0.2141 1.0419 0.125 Uiso 1 1 calc R U . . .
H72C H 0.0015 0.2798 1.0641 0.125 Uiso 1 1 calc R U . . .
C73 C 0.0373(8) 0.7709(5) 0.7857(4) 0.068(3) Uani 1 1 d D U . . .
C74 C 0.1055(6) 0.7530(5) 0.7289(4) 0.0447(19) Uani 1 1 d D U . . .
C75 C 0.1065(7) 0.8209(5) 0.6799(4) 0.061(3) Uani 1 1 d . U . . .
H75 H 0.0630 0.8735 0.6838 0.073 Uiso 1 1 calc R U . . .
C76 C 0.1663(6) 0.8177(4) 0.6254(4) 0.0434(18) Uani 1 1 d D U . . .
C77 C 0.1575(7) 0.9019(5) 0.5775(4) 0.066(3) Uani 1 1 d D U . . .
C78 C 0.7074(9) -0.0948(7) 0.6177(5) 0.074(3) Uani 1 1 d . U . . .
C79 C 0.6345(7) -0.0487(5) 0.6620(4) 0.052(2) Uani 1 1 d . U . . .
C80 C 0.6081(8) -0.0973(5) 0.7185(5) 0.067(3) Uani 1 1 d . U . . .
H80 H 0.6353 -0.1558 0.7257 0.080 Uiso 1 1 calc R U . . .
C81 C 0.5463(7) -0.0683(5) 0.7647(4) 0.052(2) Uani 1 1 d . U . . .
C82 C 0.5256(11) -0.1329(6) 0.8230(5) 0.088(4) Uani 1 1 d . U . . .
C83 C -0.0401(6) 0.2634(5) 0.8940(3) 0.0389(17) Uani 1 1 d . U . . .
C84 C -0.1428(6) 0.2479(6) 0.9242(4) 0.054(2) Uani 1 1 d . U . . .
C85 C 0.4588(6) 0.2863(6) 0.9546(4) 0.047(2) Uani 1 1 d . U . . .
C86 C 0.5154(8) 0.2809(7) 1.0000(5) 0.066(3) Uani 1 1 d . U . . .
C87 C 0.2633(6) 0.4140(6) 0.5181(4) 0.047(2) Uani 1 1 d . U . . .
C88 C 0.2472(9) 0.4292(8) 0.4569(5) 0.074(3) Uani 1 1 d . U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C7 2.064(7) . ?
Ag1 C25 2.086(7) . ?
Ag1 Ag6C 2.844(18) . ?
Ag1 Ag7C 2.90(2) . ?
Ag1 Ag4B 2.922(12) . ?
Ag1 Ag4A 2.931(4) . ?
Ag1 Ag14 2.9886(8) . ?
Ag1 A15 2.993(4) . ?
Ag1 Ag15 3.068(12) . ?
Ag1 Ag8B 3.188(10) . ?
Ag1 Ag6B 3.194(6) . ?
Ag1 Ag9A 3.199(4) . ?
Ag2A C1 2.20(2) . ?
Ag2A C43 2.38(3) . ?
Ag2A O5 2.44(3) . ?
Ag2A Ag9A 2.61(3) . ?
Ag2A Ag6B 2.68(2) . ?
Ag2A Ag6A 2.91(3) . ?
Ag2A Ag16 2.92(2) . ?
Ag2A Ag9B 2.99(3) . ?
Ag2A Ag10 3.09(2) . ?
Ag2A Ag6C 3.27(3) . ?
Ag2B C1 2.176(8) . ?
Ag2B C43 2.251(7) . ?
Ag2B O5 2.289(8) . ?
Ag2B Ag16 2.768(2) . ?
Ag2B Ag9A 2.911(4) . ?
Ag2B Ag10 2.9133(17) . ?
Ag2B Ag6B 2.922(5) . ?
Ag2B Ag6A 3.097(14) . ?
Ag2B Ag9B 3.231(14) . ?
Ag3A C13 2.07(2) . ?
Ag3A C19 2.29(4) . ?
Ag3A C14 2.64(5) . ?
Ag3A Ag16 2.87(7) . ?
Ag3A Ag11 2.91(3) . ?
Ag3A A15 2.98(7) . ?
Ag3A Ag15 3.05(6) . ?
Ag3A Ag10 3.05(3) . ?
Ag3B C19 2.163(7) . ?
Ag3B C13 2.190(7) . ?
Ag3B C14 2.487(7) . ?
Ag3B C20 2.541(8) . ?
Ag3B Ag11 3.013(3) . ?
Ag3B Ag10 3.224(4) . ?
Ag3B A15 3.279(5) . ?
Ag3B Ag16 3.327(4) . ?
Ag3B Ag15 3.333(12) . ?
Ag4A C37 2.307(8) . ?
Ag4A O9 2.309(7) . ?
Ag4A C67 2.503(8) . ?
Ag4A C7 2.637(9) . ?
Ag4A Ag11 2.896(5) . ?
Ag4A Ag13 2.920(3) . ?
Ag4A Ag9A 2.945(5) . ?
Ag4A Ag9B 3.245(14) . ?
Ag4A Ag15 3.315(16) . ?
Ag4B O9 2.249(16) . ?
Ag4B C37 2.298(16) . ?
Ag4B C7 2.482(18) . ?
Ag4B C67 2.664(19) . ?
Ag4B Ag9A 2.844(15) . ?
Ag4B Ag13 2.925(14) . ?
Ag4B Ag11 3.014(19) . ?
Ag4B Ag9B 3.16(2) . ?
Ag5 C55 2.146(8) . ?
Ag5 C61 2.178(9) . ?
Ag5 O3 2.583(6) . ?
Ag5 Ag17 2.8245(9) . ?
Ag5 Ag13 2.8391(8) . ?
Ag5 Ag8C 2.864(19) . ?
Ag5 Ag8A 2.877(8) . ?
Ag5 Ag7B 2.888(17) . ?
Ag5 Ag8B 3.027(7) . ?
Ag5 Ag7A 3.034(5) . ?
Ag5 Ag7C 3.30(3) . ?
Ag6A C31 2.144(15) . ?
Ag6A O6 2.213(17) . ?
Ag6A C43 2.416(15) . ?
Ag6A C44 2.575(14) . ?
Ag6A Ag12 2.999(12) . ?
Ag6A Ag14 3.096(14) . ?
Ag6A Ag8A 3.244(17) . ?
Ag6B C31 2.251(9) . ?
Ag6B O6 2.407(9) . ?
Ag6B C43 2.431(8) . ?
Ag6B Ag8B 2.763(10) . ?
Ag6B Ag14 3.050(4) . ?
Ag6B Ag12 3.119(5) . ?
Ag6C C31 1.904(17) . ?
Ag6C Ag8C 2.17(5) . ?
Ag6C C7 2.214(17) . ?
Ag6C C8 2.552(17) . ?
Ag6C Ag12 2.959(16) . ?
Ag6C Ag14 3.29(2) . ?
Ag7A C49 2.128(8) . ?
Ag7A C55 2.189(8) . ?
Ag7A C56 2.536(9) . ?
Ag7A Ag14 3.025(4) . ?
Ag7A Ag12 3.029(4) . ?
Ag7B C55 2.114(15) . ?
Ag7B C49 2.191(15) . ?
Ag7B C56 2.551(15) . ?
Ag7B Ag14 2.964(12) . ?
Ag7B Ag12 2.975(13) . ?
Ag7B Ag17 3.293(16) . ?
Ag7C Ag14 1.58(3) . ?
Ag7C C49 2.15(2) . ?
Ag7C C25 2.40(3) . ?
Ag7C Ag12 2.64(3) . ?
Ag7C Ag17 3.23(3) . ?
Ag8A C61 2.078(11) . ?
Ag8A C31 2.080(11) . ?
Ag8A Ag12 2.920(8) . ?
Ag8A Ag13 3.129(12) . ?
Ag8B C31 2.210(9) . ?
Ag8B C61 2.276(12) . ?
Ag8B C7 2.589(12) . ?
Ag8B Ag13 2.927(5) . ?
Ag8B Ag12 3.052(5) . ?
Ag8C C61 2.01(2) . ?
Ag8C C31 2.098(16) . ?
Ag8C Ag12 2.956(15) . ?
Ag8C Ag13 3.17(2) . ?
Ag9A C1 2.223(8) . ?
Ag9A C37 2.276(9) . ?
Ag9A C7 2.649(10) . ?
Ag9A Ag10 3.035(4) . ?
Ag9A Ag11 3.037(5) . ?
Ag9B C37 2.076(9) . ?
Ag9B C1 2.099(9) . ?
Ag9B Ag10 2.873(4) . ?
Ag9B Ag11 2.915(4) . ?
Ag10 C1 2.251(7) . ?
Ag10 C13 2.340(7) . ?
Ag10 O1 2.379(5) . ?
Ag10 O2 2.413(5) . ?
Ag10 Ag16 2.8391(8) . ?
Ag11 C19 2.104(7) . ?
Ag11 C37 2.108(8) . ?
Ag11 Ag15 2.773(14) . ?
Ag11 A15 2.900(5) . ?
Ag12 C31 2.223(7) . ?
Ag12 C49 2.266(8) . ?
Ag12 O4 2.375(6) . ?
Ag12 O3 2.472(5) . ?
Ag12 Ag14 2.8382(8) . ?
Ag13 C67 2.224(7) . ?
Ag13 C61 2.236(8) . ?
Ag13 O10 2.327(6) . ?
Ag13 Ag17 2.9146(9) . ?
Ag14 C49 2.190(7) . ?
Ag14 C43 2.390(7) . ?
Ag14 C25 2.482(7) . ?
Ag14 C44 2.630(7) . ?
Ag14 Ag16 3.0469(8) . ?
Ag15 C19 2.290(14) . ?
Ag15 O7 2.335(15) . ?
Ag15 C67 2.384(14) . ?
Ag15 C25 2.683(15) . ?
Ag15 Ag17 3.032(12) . ?
A15 O7 2.285(7) . ?
A15 C19 2.364(9) . ?
A15 C67 2.475(8) . ?
A15 C25 2.492(8) . ?
A15 Ag17 2.961(5) . ?
Ag16 C13 2.106(7) . ?
Ag16 C43 2.200(7) . ?
Ag17 C67 2.240(7) . ?
Ag17 C55 2.272(7) . ?
Ag17 O8 2.328(7) . ?
F1 C82 1.225(12) . ?
F2 C82 1.245(14) . ?
F3 C82 1.361(18) . ?
F4 C78 1.256(12) . ?
F5 C78 1.346(17) . ?
F6 C78 1.211(13) . ?
F7 C77 1.300(13) . ?
F8 C77 1.268(13) . ?
F9 C77 1.335(12) . ?
F7A C77 1.387(16) . ?
F8A C77 1.271(16) . ?
F9A C77 1.328(17) . ?
F10 C73 1.274(11) . ?
F11 C73 1.405(11) . ?
F12 C73 1.311(11) . ?
F10A C73 1.244(15) . ?
F11A C73 1.284(17) . ?
F12A C73 1.440(15) . ?
F13 C88 1.290(14) . ?
F14 C88 1.321(14) . ?
F15 C88 1.267(15) . ?
F16 C86 1.302(13) . ?
F17 C86 1.302(13) . ?
F18 C86 1.340(12) . ?
F19 C84 1.298(11) . ?
F20 C84 1.302(11) . ?
F21 C84 1.290(12) . ?
O1 C76 1.220(9) . ?
O2 C74 1.220(9) . ?
O3 C81 1.255(9) . ?
O4 C79 1.227(10) . ?
O5 C87 1.199(11) . ?
O6 C87 1.203(11) . ?
O7 C85 1.224(10) . ?
O8 C85 1.218(11) . ?
O9 C83 1.224(10) . ?
O10 C83 1.224(10) . ?
C1 C2 1.184(10) . ?
C2 C3 1.488(11) . ?
C3 C4 1.506(13) . ?
C3 C6 1.528(13) . ?
C3 C5 1.548(13) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.221(10) . ?
C8 C9 1.481(10) . ?
C9 C10 1.481(14) . ?
C9 C11 1.505(13) . ?
C9 C12 1.531(14) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.215(10) . ?
C14 C15 1.495(10) . ?
C15 C16 1.498(12) . ?
C15 C18 1.528(12) . ?
C15 C17 1.537(11) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.205(10) . ?
C20 C21 1.491(10) . ?
C21 C22 1.505(12) . ?
C21 C23 1.529(12) . ?
C21 C24 1.532(12) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.205(10) . ?
C26 C27 1.486(10) . ?
C27 C28 1.514(12) . ?
C27 C29 1.529(12) . ?
C27 C30 1.530(11) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.206(11) . ?
C32 C33 1.474(12) . ?
C33 C36 1.509(15) . ?
C33 C34 1.526(15) . ?
C33 C35 1.531(13) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.193(10) . ?
C38 C39 1.468(10) . ?
C39 C42A 1.491(18) . ?
C39 C40 1.493(12) . ?
C39 C41 1.517(12) . ?
C39 C40A 1.527(19) . ?
C39 C41A 1.570(18) . ?
C39 C42 1.580(12) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C40A H40D 0.9800 . ?
C40A H40E 0.9800 . ?
C40A H40F 0.9800 . ?
C41A H41D 0.9800 . ?
C41A H41E 0.9800 . ?
C41A H41F 0.9800 . ?
C42A H42D 0.9800 . ?
C42A H42E 0.9800 . ?
C42A H42F 0.9800 . ?
C43 C44 1.208(10) . ?
C44 C45 1.504(10) . ?
C45 C48 1.512(11) . ?
C45 C46 1.515(13) . ?
C45 C47 1.519(12) . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.194(10) . ?
C50 C51 1.490(11) . ?
C51 C54 1.453(18) . ?
C51 C52 1.46(2) . ?
C51 C53 1.536(18) . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 H53A 0.9800 . ?
C53 H53B 0.9800 . ?
C53 H53C 0.9800 . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C55 C56 1.209(11) . ?
C56 C57 1.476(12) . ?
C57 C59 1.463(15) . ?
C57 C60A 1.472(18) . ?
C57 C58 1.524(14) . ?
C57 C59A 1.534(18) . ?
C57 C58A 1.598(18) . ?
C57 C60 1.602(16) . ?
C58 H58A 0.9800 . ?
C58 H58B 0.9800 . ?
C58 H58C 0.9800 . ?
C59 H59A 0.9800 . ?
C59 H59B 0.9800 . ?
C59 H59C 0.9800 . ?
C60 H60A 0.9800 . ?
C60 H60B 0.9800 . ?
C60 H60C 0.9800 . ?
C58A H58D 0.9800 . ?
C58A H58E 0.9800 . ?
C58A H58F 0.9800 . ?
C59A H59D 0.9800 . ?
C59A H59E 0.9800 . ?
C59A H59F 0.9800 . ?
C60A H60D 0.9800 . ?
C60A H60E 0.9800 . ?
C60A H60F 0.9800 . ?
C61 C62 1.170(12) . ?
C62 C63A 1.507(19) . ?
C62 C63 1.519(19) . ?
C63 C65 1.532(14) . ?
C63 C64 1.536(14) . ?
C63 C66 1.540(14) . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C63A C64A 1.519(19) . ?
C63A C65A 1.529(19) . ?
C63A C66A 1.540(19) . ?
C64A H64D 0.9800 . ?
C64A H64E 0.9800 . ?
C64A H64F 0.9800 . ?
C65A H65D 0.9800 . ?
C65A H65E 0.9800 . ?
C65A H65F 0.9800 . ?
C66A H66D 0.9800 . ?
C66A H66E 0.9800 . ?
C66A H66F 0.9800 . ?
C67 C68 1.197(10) . ?
C68 C69 1.495(11) . ?
C69 C70 1.482(15) . ?
C69 C72 1.540(15) . ?
C69 C71 1.560(14) . ?
C70 H70A 0.9800 . ?
C70 H70B 0.9800 . ?
C70 H70C 0.9800 . ?
C71 H71A 0.9800 . ?
C71 H71B 0.9800 . ?
C71 H71C 0.9800 . ?
C72 H72A 0.9800 . ?
C72 H72B 0.9800 . ?
C72 H72C 0.9800 . ?
C73 C74 1.539(10) . ?
C74 C75 1.387(12) . ?
C75 C76 1.390(12) . ?
C75 H75 0.9500 . ?
C76 C77 1.549(10) . ?
C78 C79 1.538(12) . ?
C79 C80 1.395(13) . ?
C80 C81 1.375(12) . ?
C80 H80 0.9500 . ?
C81 C82 1.535(13) . ?
C83 C84 1.536(11) . ?
C85 C86 1.532(13) . ?
C87 C88 1.519(14) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C7 Ag1 C25 172.2(3) . . ?
C7 Ag1 Ag6C 50.6(4) . . ?
C25 Ag1 Ag6C 123.6(4) . . ?
C7 Ag1 Ag7C 122.8(6) . . ?
C25 Ag1 Ag7C 54.5(6) . . ?
Ag6C Ag1 Ag7C 75.3(6) . . ?
C7 Ag1 Ag4B 56.6(5) . . ?
C25 Ag1 Ag4B 130.3(5) . . ?
Ag6C Ag1 Ag4B 105.2(6) . . ?
Ag7C Ag1 Ag4B 145.3(6) . . ?
C7 Ag1 Ag4A 60.8(2) . . ?
C25 Ag1 Ag4A 126.2(2) . . ?
Ag6C Ag1 Ag4A 109.1(4) . . ?
Ag7C Ag1 Ag4A 143.8(6) . . ?
Ag4B Ag1 Ag4A 4.2(5) . . ?
C7 Ag1 Ag14 118.3(2) . . ?
C25 Ag1 Ag14 55.2(2) . . ?
Ag6C Ag1 Ag14 68.7(4) . . ?
Ag7C Ag1 Ag14 31.1(6) . . ?
Ag4B Ag1 Ag14 172.9(4) . . ?
Ag4A Ag1 Ag14 174.37(7) . . ?
C7 Ag1 A15 131.6(2) . . ?
C25 Ag1 A15 55.4(2) . . ?
Ag6C Ag1 A15 167.6(6) . . ?
Ag7C Ag1 A15 97.4(6) . . ?
Ag4B Ag1 A15 75.0(5) . . ?
Ag4A Ag1 A15 70.83(16) . . ?
Ag14 Ag1 A15 110.05(11) . . ?
C7 Ag1 Ag15 127.8(4) . . ?
C25 Ag1 Ag15 59.1(4) . . ?
Ag6C Ag1 Ag15 167.4(6) . . ?
Ag7C Ag1 Ag15 100.6(6) . . ?
Ag4B Ag1 Ag15 71.2(5) . . ?
Ag4A Ag1 Ag15 67.0(3) . . ?
Ag14 Ag1 Ag15 113.8(3) . . ?
A15 Ag1 Ag15 3.8(4) . . ?
C7 Ag1 Ag8B 54.1(2) . . ?
C25 Ag1 Ag8B 125.0(2) . . ?
Ag4B Ag1 Ag8B 91.0(4) . . ?
Ag4A Ag1 Ag8B 93.63(13) . . ?
Ag14 Ag1 Ag8B 81.92(8) . . ?
A15 Ag1 Ag8B 135.84(14) . . ?
Ag15 Ag1 Ag8B 134.9(2) . . ?
C7 Ag1 Ag6B 59.8(2) . . ?
C25 Ag1 Ag6B 113.0(2) . . ?
Ag4B Ag1 Ag6B 116.3(5) . . ?
Ag4A Ag1 Ag6B 120.58(16) . . ?
Ag14 Ag1 Ag6B 59.00(11) . . ?
A15 Ag1 Ag6B 168.04(15) . . ?
Ag15 Ag1 Ag6B 171.5(3) . . ?
Ag8B Ag1 Ag6B 51.31(13) . . ?
C7 Ag1 Ag9A 55.5(2) . . ?
C25 Ag1 Ag9A 123.6(2) . . ?
Ag4B Ag1 Ag9A 55.2(3) . . ?
Ag4A Ag1 Ag9A 57.23(8) . . ?
Ag14 Ag1 Ag9A 127.50(5) . . ?
A15 Ag1 Ag9A 96.72(14) . . ?
Ag15 Ag1 Ag9A 94.2(3) . . ?
C1 Ag2A C43 143.6(9) . . ?
C1 Ag2A O5 91.9(9) . . ?
C43 Ag2A O5 92.0(9) . . ?
C1 Ag2A Ag9A 54.2(6) . . ?
C43 Ag2A Ag9A 133.8(11) . . ?
O5 Ag2A Ag9A 134.2(11) . . ?
C1 Ag2A Ag6B 159.4(10) . . ?
C43 Ag2A Ag6B 57.0(6) . . ?
O5 Ag2A Ag6B 87.1(8) . . ?
C1 Ag2A Ag6A 162.5(11) . . ?
C43 Ag2A Ag6A 53.3(6) . . ?
O5 Ag2A Ag6A 80.9(8) . . ?
Ag9A Ag2A Ag6A 121.4(7) . . ?
C1 Ag2A Ag16 103.1(8) . . ?
C43 Ag2A Ag16 47.7(5) . . ?
O5 Ag2A Ag16 126.4(9) . . ?
Ag9A Ag2A Ag16 93.9(8) . . ?
Ag6B Ag2A Ag16 93.9(7) . . ?
Ag6A Ag2A Ag16 94.0(7) . . ?
C1 Ag2A Ag9B 44.5(6) . . ?
C43 Ag2A Ag9B 138.1(11) . . ?
O5 Ag2A Ag9B 129.1(10) . . ?
Ag6B Ag2A Ag9B 123.7(8) . . ?
Ag16 Ag2A Ag9B 93.9(7) . . ?
C1 Ag2A Ag10 46.8(5) . . ?
C43 Ag2A Ag10 100.5(8) . . ?
O5 Ag2A Ag10 117.8(7) . . ?
Ag9A Ag2A Ag10 63.7(6) . . ?
Ag6B Ag2A Ag10 148.5(10) . . ?
Ag6A Ag2A Ag10 150.1(10) . . ?
Ag16 Ag2A Ag10 56.3(4) . . ?
Ag9B Ag2A Ag10 56.4(5) . . ?
C1 Ag2A Ag6C 145.3(10) . . ?
C43 Ag2A Ag6C 69.1(7) . . ?
O5 Ag2A Ag6C 99.4(9) . . ?
Ag16 Ag2A Ag6C 96.3(7) . . ?
Ag10 Ag2A Ag6C 142.0(9) . . ?
C1 Ag2A Ag1 115.1(10) . . ?
C43 Ag2A Ag1 74.3(6) . . ?
O5 Ag2A Ag1 150.0(9) . . ?
Ag9A Ag2A Ag1 63.7(5) . . ?
Ag6B Ag2A Ag1 63.0(4) . . ?
Ag6A Ag2A Ag1 69.5(6) . . ?
Ag16 Ag2A Ag1 62.3(5) . . ?
Ag9B Ag2A Ag1 72.2(6) . . ?
Ag10 Ag2A Ag1 91.2(7) . . ?
Ag6C Ag2A Ag1 51.0(5) . . ?
C1 Ag2B C43 159.2(3) . . ?
C1 Ag2B O5 97.0(3) . . ?
C43 Ag2B O5 99.8(3) . . ?
C1 Ag2B Ag16 108.8(2) . . ?
C43 Ag2B Ag16 50.73(19) . . ?
O5 Ag2B Ag16 142.4(3) . . ?
C1 Ag2B Ag9A 49.3(2) . . ?
C43 Ag2B Ag9A 125.2(2) . . ?
O5 Ag2B Ag9A 126.7(3) . . ?
Ag16 Ag2B Ag9A 90.81(8) . . ?
C1 Ag2B Ag10 50.0(2) . . ?
C43 Ag2B Ag10 109.29(19) . . ?
O5 Ag2B Ag10 131.4(2) . . ?
Ag16 Ag2B Ag10 59.90(4) . . ?
Ag9A Ag2B Ag10 62.82(13) . . ?
C1 Ag2B Ag6B 140.4(3) . . ?
C43 Ag2B Ag6B 54.2(2) . . ?
O5 Ag2B Ag6B 84.5(2) . . ?
Ag16 Ag2B Ag6B 92.01(10) . . ?
Ag10 Ag2B Ag6B 144.10(12) . . ?
C1 Ag2B Ag6A 145.9(3) . . ?
C43 Ag2B Ag6A 50.8(3) . . ?
O5 Ag2B Ag6A 79.1(4) . . ?
Ag16 Ag2B Ag6A 92.9(3) . . ?
Ag9A Ag2B Ag6A 106.4(3) . . ?
Ag10 Ag2B Ag6A 148.9(3) . . ?
C1 Ag2B Ag9B 40.0(4) . . ?
C43 Ag2B Ag9B 131.9(3) . . ?
O5 Ag2B Ag9B 124.9(3) . . ?
Ag16 Ag2B Ag9B 91.72(13) . . ?
Ag10 Ag2B Ag9B 55.47(19) . . ?
Ag6B Ag2B Ag9B 108.6(3) . . ?
C13 Ag3A C19 163(5) . . ?
C13 Ag3A C14 26.6(8) . . ?
C19 Ag3A C14 138(4) . . ?
C13 Ag3A Ag16 47.2(14) . . ?
C19 Ag3A Ag16 149(3) . . ?
C14 Ag3A Ag16 73.0(8) . . ?
C13 Ag3A Ag11 133.5(14) . . ?
C19 Ag3A Ag11 45.9(5) . . ?
C14 Ag3A Ag11 139(3) . . ?
Ag16 Ag3A Ag11 112.7(17) . . ?
C13 Ag3A A15 146(5) . . ?
C19 Ag3A A15 51.3(10) . . ?
C14 Ag3A A15 162(3) . . ?
Ag16 Ag3A A15 100(3) . . ?
Ag11 Ag3A A15 59.1(7) . . ?
C13 Ag3A Ag15 149(5) . . ?
C19 Ag3A Ag15 48.3(10) . . ?
C14 Ag3A Ag15 166(3) . . ?
Ag16 Ag3A Ag15 102(3) . . ?
Ag11 Ag3A Ag15 55.5(7) . . ?
A15 Ag3A Ag15 3.8(4) . . ?
C13 Ag3A Ag10 50.1(6) . . ?
C19 Ag3A Ag10 125(2) . . ?
C14 Ag3A Ag10 65.3(9) . . ?
Ag16 Ag3A Ag10 57.3(5) . . ?
Ag11 Ag3A Ag10 83.4(8) . . ?
A15 Ag3A Ag10 125.3(17) . . ?
Ag15 Ag3A Ag10 124.2(15) . . ?
C19 Ag3B C13 165.3(4) . . ?
C19 Ag3B C14 164.6(3) . . ?
C13 Ag3B C14 29.2(2) . . ?
C19 Ag3B C20 28.3(3) . . ?
C13 Ag3B C20 166.1(3) . . ?
C14 Ag3B C20 138.5(3) . . ?
C19 Ag3B Ag11 44.29(19) . . ?
C13 Ag3B Ag11 122.9(3) . . ?
C14 Ag3B Ag11 141.4(2) . . ?
C20 Ag3B Ag11 70.89(17) . . ?
C19 Ag3B Ag10 122.8(2) . . ?
C13 Ag3B Ag10 46.5(2) . . ?
C14 Ag3B Ag10 63.96(18) . . ?
C20 Ag3B Ag10 145.03(19) . . ?
Ag11 Ag3B Ag10 78.84(11) . . ?
C19 Ag3B A15 46.1(2) . . ?
C13 Ag3B A15 123.2(3) . . ?
C14 Ag3B A15 148.1(2) . . ?
C20 Ag3B A15 64.75(18) . . ?
Ag11 Ag3B A15 54.69(11) . . ?
Ag10 Ag3B A15 110.82(17) . . ?
C19 Ag3B Ag16 128.5(3) . . ?
C13 Ag3B Ag16 38.3(2) . . ?
C14 Ag3B Ag16 66.84(18) . . ?
C20 Ag3B Ag16 149.11(19) . . ?
Ag11 Ag3B Ag16 98.45(15) . . ?
Ag10 Ag3B Ag16 51.34(7) . . ?
A15 Ag3B Ag16 85.25(12) . . ?
C19 Ag3B Ag15 43.0(3) . . ?
C13 Ag3B Ag15 125.8(3) . . ?
C14 Ag3B Ag15 151.4(3) . . ?
C20 Ag3B Ag15 62.8(3) . . ?
Ag11 Ag3B Ag15 51.5(3) . . ?
Ag10 Ag3B Ag15 110.5(3) . . ?
A15 Ag3B Ag15 3.6(3) . . ?
Ag16 Ag3B Ag15 87.6(2) . . ?
C37 Ag4A O9 96.0(3) . . ?
C37 Ag4A C67 138.1(4) . . ?
O9 Ag4A C67 104.0(3) . . ?
C37 Ag4A C7 103.9(3) . . ?
O9 Ag4A C7 107.2(3) . . ?
C67 Ag4A C7 104.7(3) . . ?
C37 Ag4A Ag11 46.1(2) . . ?
O9 Ag4A Ag11 131.5(2) . . ?
C67 Ag4A Ag11 94.9(2) . . ?
C7 Ag4A Ag11 110.4(2) . . ?
C37 Ag4A Ag13 174.1(3) . . ?
O9 Ag4A Ag13 82.55(19) . . ?
C67 Ag4A Ag13 47.66(17) . . ?
C7 Ag4A Ag13 71.24(18) . . ?
Ag11 Ag4A Ag13 138.22(19) . . ?
C37 Ag4A Ag1 109.9(2) . . ?
O9 Ag4A Ag1 143.7(3) . . ?
C67 Ag4A Ag1 73.37(19) . . ?
C7 Ag4A Ag1 43.11(16) . . ?
Ag11 Ag4A Ag1 84.28(12) . . ?
Ag13 Ag4A Ag1 69.06(8) . . ?
C37 Ag4A Ag9A 49.5(2) . . ?
O9 Ag4A Ag9A 120.5(3) . . ?
C67 Ag4A Ag9A 134.6(2) . . ?
C7 Ag4A Ag9A 56.3(2) . . ?
Ag11 Ag4A Ag9A 62.65(14) . . ?
Ag13 Ag4A Ag9A 126.5(2) . . ?
Ag1 Ag4A Ag9A 65.97(11) . . ?
C37 Ag4A Ag9B 39.6(4) . . ?
O9 Ag4A Ag9B 117.5(3) . . ?
C67 Ag4A Ag9B 138.4(3) . . ?
C7 Ag4A Ag9B 66.1(3) . . ?
Ag11 Ag4A Ag9B 56.33(16) . . ?
Ag13 Ag4A Ag9B 136.5(4) . . ?
Ag1 Ag4A Ag9B 74.3(3) . . ?
C37 Ag4A Ag15 98.6(3) . . ?
O9 Ag4A Ag15 143.4(3) . . ?
C67 Ag4A Ag15 45.8(3) . . ?
C7 Ag4A Ag15 101.5(3) . . ?
Ag11 Ag4A Ag15 52.5(2) . . ?
Ag13 Ag4A Ag15 85.8(2) . . ?
Ag1 Ag4A Ag15 58.5(2) . . ?
Ag9A Ag4A Ag15 94.2(2) . . ?
Ag9B Ag4A Ag15 94.5(2) . . ?
O9 Ag4B C37 98.0(5) . . ?
O9 Ag4B C7 114.7(9) . . ?
C37 Ag4B C7 109.2(7) . . ?
O9 Ag4B C67 100.8(6) . . ?
C37 Ag4B C67 129.6(10) . . ?
C7 Ag4B C67 104.5(5) . . ?
O9 Ag4B Ag9A 127.3(8) . . ?
C37 Ag4B Ag9A 51.2(4) . . ?
C7 Ag4B Ag9A 59.2(4) . . ?
C67 Ag4B Ag9A 131.9(6) . . ?
O9 Ag4B Ag1 148.7(7) . . ?
C37 Ag4B Ag1 110.4(6) . . ?
C7 Ag4B Ag1 44.0(3) . . ?
C67 Ag4B Ag1 71.3(4) . . ?
Ag9A Ag4B Ag1 67.4(3) . . ?
O9 Ag4B Ag13 83.4(5) . . ?
C37 Ag4B Ag13 176.2(10) . . ?
C7 Ag4B Ag13 73.2(4) . . ?
C67 Ag4B Ag13 46.6(3) . . ?
Ag9A Ag4B Ag13 130.4(5) . . ?
Ag1 Ag4B Ag13 69.1(3) . . ?
O9 Ag4B Ag11 128.5(6) . . ?
C37 Ag4B Ag11 44.3(4) . . ?
C7 Ag4B Ag11 111.2(5) . . ?
C67 Ag4B Ag11 89.0(6) . . ?
Ag9A Ag4B Ag11 62.4(3) . . ?
Ag1 Ag4B Ag11 82.4(4) . . ?
Ag13 Ag4B Ag11 132.4(7) . . ?
O9 Ag4B Ag9B 123.0(7) . . ?
C37 Ag4B Ag9B 41.0(4) . . ?
C7 Ag4B Ag9B 69.1(5) . . ?
C67 Ag4B Ag9B 134.8(7) . . ?
Ag1 Ag4B Ag9B 75.7(4) . . ?
Ag13 Ag4B Ag9B 140.5(6) . . ?
Ag11 Ag4B Ag9B 56.3(3) . . ?
C55 Ag5 C61 163.4(3) . . ?
C55 Ag5 O3 97.6(3) . . ?
C61 Ag5 O3 98.9(3) . . ?
C55 Ag5 Ag17 52.3(2) . . ?
C61 Ag5 Ag17 112.8(2) . . ?
O3 Ag5 Ag17 136.30(15) . . ?
C55 Ag5 Ag13 113.7(2) . . ?
C61 Ag5 Ag13 50.9(2) . . ?
O3 Ag5 Ag13 139.30(14) . . ?
Ag17 Ag5 Ag13 61.94(2) . . ?
C55 Ag5 Ag8C 141.9(7) . . ?
C61 Ag5 Ag8C 44.5(5) . . ?
O3 Ag5 Ag8C 71.8(6) . . ?
Ag17 Ag5 Ag8C 110.8(9) . . ?
Ag13 Ag5 Ag8C 67.5(6) . . ?
C55 Ag5 Ag8A 139.6(3) . . ?
C61 Ag5 Ag8A 46.0(3) . . ?
O3 Ag5 Ag8A 72.9(3) . . ?
Ag17 Ag5 Ag8A 108.1(3) . . ?
Ag13 Ag5 Ag8A 66.4(3) . . ?
C55 Ag5 Ag7B 46.9(3) . . ?
C61 Ag5 Ag7B 141.3(4) . . ?
O3 Ag5 Ag7B 66.1(3) . . ?
Ag17 Ag5 Ag7B 70.4(3) . . ?
Ag13 Ag5 Ag7B 117.8(3) . . ?
C55 Ag5 Ag8B 133.7(2) . . ?
C61 Ag5 Ag8B 48.6(3) . . ?
O3 Ag5 Ag8B 79.93(19) . . ?
Ag17 Ag5 Ag8B 98.75(18) . . ?
Ag13 Ag5 Ag8B 59.75(12) . . ?
Ag7B Ag5 Ag8B 92.8(3) . . ?
C55 Ag5 Ag7A 46.2(2) . . ?
C61 Ag5 Ag7A 142.7(2) . . ?
O3 Ag5 Ag7A 64.90(16) . . ?
Ag17 Ag5 Ag7A 71.73(7) . . ?
Ag13 Ag5 Ag7A 119.95(7) . . ?
Ag8A Ag5 Ag7A 96.72(15) . . ?
C55 Ag5 Ag7C 66.8(5) . . ?
C61 Ag5 Ag7C 115.5(5) . . ?
O3 Ag5 Ag7C 76.6(5) . . ?
Ag17 Ag5 Ag7C 63.2(5) . . ?
Ag13 Ag5 Ag7C 91.9(4) . . ?
Ag8C Ag5 Ag7C 75.1(8) . . ?
C31 Ag6A O6 104.3(7) . . ?
C31 Ag6A C43 148.8(6) . . ?
O6 Ag6A C43 102.3(6) . . ?
C31 Ag6A C44 131.6(6) . . ?
O6 Ag6A C44 96.7(6) . . ?
C43 Ag6A C44 27.8(3) . . ?
C31 Ag6A Ag2A 150.6(8) . . ?
O6 Ag6A Ag2A 77.9(7) . . ?
C43 Ag6A Ag2A 52.2(5) . . ?
C44 Ag6A Ag2A 76.0(6) . . ?
C31 Ag6A Ag12 47.7(3) . . ?
O6 Ag6A Ag12 140.1(8) . . ?
C43 Ag6A Ag12 101.1(4) . . ?
C44 Ag6A Ag12 89.3(4) . . ?
Ag2A Ag6A Ag12 141.3(8) . . ?
C31 Ag6A Ag14 100.9(5) . . ?
O6 Ag6A Ag14 150.4(6) . . ?
C43 Ag6A Ag14 49.5(3) . . ?
C44 Ag6A Ag14 54.3(3) . . ?
Ag2A Ag6A Ag14 87.8(7) . . ?
Ag12 Ag6A Ag14 55.5(2) . . ?
C31 Ag6A Ag2B 158.7(7) . . ?
O6 Ag6A Ag2B 76.1(4) . . ?
C43 Ag6A Ag2B 46.2(3) . . ?
C44 Ag6A Ag2B 68.6(3) . . ?
Ag2A Ag6A Ag2B 8.1(4) . . ?
Ag12 Ag6A Ag2B 141.3(6) . . ?
Ag14 Ag6A Ag2B 86.1(4) . . ?
C31 Ag6A Ag8A 39.1(4) . . ?
O6 Ag6A Ag8A 124.8(5) . . ?
C43 Ag6A Ag8A 129.0(7) . . ?
C44 Ag6A Ag8A 138.0(5) . . ?
Ag2A Ag6A Ag8A 115.5(8) . . ?
Ag12 Ag6A Ag8A 55.6(3) . . ?
Ag14 Ag6A Ag8A 84.8(4) . . ?
Ag2B Ag6A Ag8A 123.2(7) . . ?
C31 Ag6B O6 95.2(3) . . ?
C31 Ag6B C43 139.6(4) . . ?
O6 Ag6B C43 96.5(3) . . ?
C31 Ag6B Ag2A 165.1(6) . . ?
O6 Ag6B Ag2A 79.6(6) . . ?
C43 Ag6B Ag2A 55.3(5) . . ?
C31 Ag6B Ag8B 51.1(3) . . ?
O6 Ag6B Ag8B 128.7(3) . . ?
C43 Ag6B Ag8B 134.7(3) . . ?
Ag2A Ag6B Ag8B 122.3(6) . . ?
C31 Ag6B Ag2B 170.2(3) . . ?
O6 Ag6B Ag2B 77.1(2) . . ?
C43 Ag6B Ag2B 48.68(18) . . ?
Ag2A Ag6B Ag2B 8.2(5) . . ?
Ag8B Ag6B Ag2B 129.8(3) . . ?
C31 Ag6B Ag14 99.8(2) . . ?
O6 Ag6B Ag14 140.4(4) . . ?
C43 Ag6B Ag14 50.16(18) . . ?
Ag2A Ag6B Ag14 93.0(5) . . ?
Ag8B Ag6B Ag14 88.23(16) . . ?
Ag2B Ag6B Ag14 90.08(12) . . ?
C31 Ag6B Ag12 45.4(2) . . ?
O6 Ag6B Ag12 124.7(4) . . ?
C43 Ag6B Ag12 97.5(2) . . ?
Ag2A Ag6B Ag12 147.7(6) . . ?
Ag8B Ag6B Ag12 62.16(16) . . ?
Ag2B Ag6B Ag12 144.33(17) . . ?
Ag14 Ag6B Ag12 54.77(8) . . ?
C31 Ag6B Ag1 112.1(3) . . ?
O6 Ag6B Ag1 145.5(4) . . ?
C43 Ag6B Ag1 76.6(2) . . ?
Ag2A Ag6B Ag1 68.6(6) . . ?
Ag8B Ag6B Ag1 64.2(2) . . ?
Ag2B Ag6B Ag1 73.12(13) . . ?
Ag14 Ag6B Ag1 57.13(8) . . ?
Ag12 Ag6B Ag1 89.76(11) . . ?
C31 Ag6C Ag8C 61.6(11) . . ?
C31 Ag6C C7 150.0(15) . . ?
Ag8C Ag6C C7 93.9(12) . . ?
C31 Ag6C C8 128.4(11) . . ?
Ag8C Ag6C C8 92.4(10) . . ?
C7 Ag6C C8 28.6(3) . . ?
C31 Ag6C Ag1 145.9(11) . . ?
Ag8C Ag6C Ag1 96.9(11) . . ?
C7 Ag6C Ag1 46.1(4) . . ?
C8 Ag6C Ag1 74.6(4) . . ?
C31 Ag6C Ag12 48.7(4) . . ?
Ag8C Ag6C Ag12 68.4(8) . . ?
C7 Ag6C Ag12 141.4(10) . . ?
C8 Ag6C Ag12 159.7(13) . . ?
Ag1 Ag6C Ag12 100.3(6) . . ?
C31 Ag6C Ag2A 140.6(14) . . ?
Ag8C Ag6C Ag2A 157.3(11) . . ?
C7 Ag6C Ag2A 63.7(7) . . ?
C8 Ag6C Ag2A 69.6(6) . . ?
Ag1 Ag6C Ag2A 65.8(6) . . ?
Ag12 Ag6C Ag2A 126.9(9) . . ?
C31 Ag6C Ag14 100.2(6) . . ?
Ag8C Ag6C Ag14 105.0(9) . . ?
C7 Ag6C Ag14 103.0(6) . . ?
C8 Ag6C Ag14 130.5(6) . . ?
Ag1 Ag6C Ag14 57.7(3) . . ?
Ag12 Ag6C Ag14 53.7(3) . . ?
Ag2A Ag6C Ag14 78.8(7) . . ?
C49 Ag7A C55 170.2(4) . . ?
C49 Ag7A C56 159.9(4) . . ?
C55 Ag7A C56 28.5(3) . . ?
C49 Ag7A Ag14 46.4(2) . . ?
C55 Ag7A Ag14 129.1(3) . . ?
C56 Ag7A Ag14 150.0(3) . . ?
C49 Ag7A Ag12 48.4(2) . . ?
C55 Ag7A Ag12 122.1(3) . . ?
C56 Ag7A Ag12 142.0(3) . . ?
Ag14 Ag7A Ag12 55.92(8) . . ?
C49 Ag7A Ag5 125.3(3) . . ?
C55 Ag7A Ag5 45.0(2) . . ?
C56 Ag7A Ag5 70.2(2) . . ?
Ag14 Ag7A Ag5 102.69(17) . . ?
Ag12 Ag7A Ag5 77.17(12) . . ?
C55 Ag7B C49 174.7(7) . . ?
C55 Ag7B C56 28.1(3) . . ?
C49 Ag7B C56 151.1(9) . . ?
C55 Ag7B Ag5 47.8(4) . . ?
C49 Ag7B Ag5 129.5(6) . . ?
C56 Ag7B Ag5 72.5(4) . . ?
C55 Ag7B Ag14 136.1(8) . . ?
C49 Ag7B Ag14 47.4(3) . . ?
C56 Ag7B Ag14 153.9(6) . . ?
Ag5 Ag7B Ag14 107.9(6) . . ?
C55 Ag7B Ag12 127.6(7) . . ?
C49 Ag7B Ag12 49.2(3) . . ?
C56 Ag7B Ag12 144.4(5) . . ?
Ag5 Ag7B Ag12 80.3(4) . . ?
Ag14 Ag7B Ag12 57.1(2) . . ?
C55 Ag7B Ag17 43.2(4) . . ?
C49 Ag7B Ag17 140.7(6) . . ?
C56 Ag7B Ag17 65.3(4) . . ?
Ag5 Ag7B Ag17 53.9(3) . . ?
Ag14 Ag7B Ag17 93.3(4) . . ?
Ag12 Ag7B Ag17 115.3(6) . . ?
Ag14 Ag7C C49 70.0(9) . . ?
Ag14 Ag7C C25 74.1(11) . . ?
C49 Ag7C C25 131.6(13) . . ?
Ag14 Ag7C Ag12 80.3(11) . . ?
C49 Ag7C Ag12 55.3(6) . . ?
C25 Ag7C Ag12 145.4(12) . . ?
Ag14 Ag7C Ag1 77.6(9) . . ?
C49 Ag7C Ag1 144.9(13) . . ?
C25 Ag7C Ag1 45.2(4) . . ?
Ag12 Ag7C Ag1 107.0(8) . . ?
Ag14 Ag7C Ag17 139.6(12) . . ?
C49 Ag7C Ag17 147.3(12) . . ?
C25 Ag7C Ag17 67.0(6) . . ?
Ag12 Ag7C Ag17 128.6(9) . . ?
Ag1 Ag7C Ag17 67.7(4) . . ?
Ag14 Ag7C Ag5 149.3(12) . . ?
C49 Ag7C Ag5 113.4(11) . . ?
C25 Ag7C Ag5 114.1(8) . . ?
Ag12 Ag7C Ag5 78.2(7) . . ?
Ag1 Ag7C Ag5 88.1(5) . . ?
Ag17 Ag7C Ag5 51.2(4) . . ?
C61 Ag8A C31 154.9(10) . . ?
C61 Ag8A Ag5 49.0(3) . . ?
C31 Ag8A Ag5 129.3(5) . . ?
C61 Ag8A Ag12 127.1(5) . . ?
C31 Ag8A Ag12 49.4(3) . . ?
Ag5 Ag8A Ag12 81.4(2) . . ?
C61 Ag8A Ag13 45.5(3) . . ?
C31 Ag8A Ag13 159.5(7) . . ?
Ag5 Ag8A Ag13 56.24(17) . . ?
Ag12 Ag8A Ag13 124.6(3) . . ?
C61 Ag8A Ag6A 164.5(9) . . ?
C31 Ag8A Ag6A 40.6(4) . . ?
Ag5 Ag8A Ag6A 126.3(4) . . ?
Ag12 Ag8A Ag6A 57.9(2) . . ?
Ag13 Ag8A Ag6A 119.0(6) . . ?
C31 Ag8B C61 129.6(6) . . ?
C31 Ag8B C7 111.8(4) . . ?
C61 Ag8B C7 116.3(3) . . ?
C31 Ag8B Ag6B 52.4(3) . . ?
C61 Ag8B Ag6B 176.3(4) . . ?
C7 Ag8B Ag6B 62.9(3) . . ?
C31 Ag8B Ag13 173.8(3) . . ?
C61 Ag8B Ag13 49.0(2) . . ?
C7 Ag8B Ag13 71.8(2) . . ?
Ag6B Ag8B Ag13 128.6(4) . . ?
C31 Ag8B Ag5 117.3(3) . . ?
C61 Ag8B Ag5 45.8(3) . . ?
C7 Ag8B Ag5 120.0(3) . . ?
Ag6B Ag8B Ag5 131.0(2) . . ?
Ag13 Ag8B Ag5 56.94(9) . . ?
C31 Ag8B Ag12 46.7(2) . . ?
C61 Ag8B Ag12 114.1(4) . . ?
C7 Ag8B Ag12 119.9(3) . . ?
Ag6B Ag8B Ag12 64.65(16) . . ?
Ag13 Ag8B Ag12 127.32(17) . . ?
Ag5 Ag8B Ag12 76.94(14) . . ?
C31 Ag8B Ag1 113.6(4) . . ?
C61 Ag8B Ag1 112.5(3) . . ?
C7 Ag8B Ag1 40.2(2) . . ?
Ag6B Ag8B Ag1 64.5(2) . . ?
Ag13 Ag8B Ag1 65.53(15) . . ?
Ag5 Ag8B Ag1 88.12(14) . . ?
Ag12 Ag8B Ag1 91.10(17) . . ?
C61 Ag8C C31 162(3) . . ?
C61 Ag8C Ag6C 145(2) . . ?
C31 Ag8C Ag6C 53.0(8) . . ?
C61 Ag8C Ag5 49.3(5) . . ?
C31 Ag8C Ag5 129.1(7) . . ?
Ag6C Ag8C Ag5 121.7(14) . . ?
C61 Ag8C Ag12 128.3(10) . . ?
C31 Ag8C Ag12 48.6(4) . . ?
Ag6C Ag8C Ag12 68.6(7) . . ?
Ag5 Ag8C Ag12 81.0(4) . . ?
C61 Ag8C Ag13 44.6(6) . . ?
C31 Ag8C Ag13 153(2) . . ?
Ag6C Ag8C Ag13 100.9(15) . . ?
Ag5 Ag8C Ag13 55.9(3) . . ?
Ag12 Ag8C Ag13 122.0(8) . . ?
C1 Ag9A C37 133.8(4) . . ?
C1 Ag9A Ag2A 53.5(5) . . ?
C37 Ag9A Ag2A 171.5(6) . . ?
C1 Ag9A C7 119.8(3) . . ?
C37 Ag9A C7 104.4(3) . . ?
Ag2A Ag9A C7 70.2(5) . . ?
C1 Ag9A Ag4B 173.1(5) . . ?
C37 Ag9A Ag4B 51.9(3) . . ?
Ag2A Ag9A Ag4B 121.3(6) . . ?
C7 Ag9A Ag4B 53.6(4) . . ?
C1 Ag9A Ag2B 47.9(2) . . ?
C37 Ag9A Ag2B 171.0(3) . . ?
Ag2A Ag9A Ag2B 7.4(4) . . ?
C7 Ag9A Ag2B 77.4(2) . . ?
Ag4B Ag9A Ag2B 127.3(3) . . ?
C1 Ag9A Ag4A 175.7(4) . . ?
C37 Ag9A Ag4A 50.5(2) . . ?
Ag2A Ag9A Ag4A 122.3(5) . . ?
C7 Ag9A Ag4A 56.0(2) . . ?
Ag4B Ag9A Ag4A 3.8(6) . . ?
Ag2B Ag9A Ag4A 128.0(2) . . ?
C1 Ag9A Ag10 47.7(2) . . ?
C37 Ag9A Ag10 114.8(3) . . ?
Ag2A Ag9A Ag10 65.8(4) . . ?
C7 Ag9A Ag10 126.3(2) . . ?
Ag4B Ag9A Ag10 136.7(4) . . ?
Ag2B Ag9A Ag10 58.63(6) . . ?
Ag4A Ag9A Ag10 133.08(16) . . ?
C1 Ag9A Ag11 125.0(3) . . ?
C37 Ag9A Ag11 43.9(2) . . ?
Ag2A Ag9A Ag11 130.1(6) . . ?
C7 Ag9A Ag11 105.94(17) . . ?
Ag4B Ag9A Ag11 61.6(4) . . ?
Ag2B Ag9A Ag11 127.05(10) . . ?
Ag4A Ag9A Ag11 57.89(12) . . ?
Ag10 Ag9A Ag11 81.50(14) . . ?
C1 Ag9A Ag1 119.7(2) . . ?
C37 Ag9A Ag1 102.3(2) . . ?
Ag2A Ag9A Ag1 69.3(5) . . ?
C7 Ag9A Ag1 39.96(16) . . ?
Ag4B Ag9A Ag1 57.5(3) . . ?
Ag2B Ag9A Ag1 73.20(11) . . ?
Ag4A Ag9A Ag1 56.80(10) . . ?
Ag10 Ag9A Ag1 94.91(6) . . ?
Ag11 Ag9A Ag1 77.60(5) . . ?
C37 Ag9B C1 164.9(13) . . ?
C37 Ag9B Ag10 129.8(4) . . ?
C1 Ag9B Ag10 51.0(2) . . ?
C37 Ag9B Ag11 46.3(2) . . ?
C1 Ag9B Ag11 137.4(3) . . ?
Ag10 Ag9B Ag11 86.43(10) . . ?
C37 Ag9B Ag2A 147.6(10) . . ?
C1 Ag9B Ag2A 47.4(5) . . ?
Ag10 Ag9B Ag2A 63.5(4) . . ?
Ag11 Ag9B Ag2A 120.3(7) . . ?
C37 Ag9B Ag4B 46.6(4) . . ?
C1 Ag9B Ag4B 147.6(10) . . ?
Ag10 Ag9B Ag4B 129.8(6) . . ?
Ag11 Ag9B Ag4B 59.3(4) . . ?
Ag2A Ag9B Ag4B 101.2(8) . . ?
C37 Ag9B Ag2B 153.3(10) . . ?
C1 Ag9B Ag2B 41.8(4) . . ?
Ag10 Ag9B Ag2B 56.65(17) . . ?
Ag11 Ag9B Ag2B 120.0(5) . . ?
Ag2A Ag9B Ag2B 7.4(3) . . ?
Ag4B Ag9B Ag2B 107.6(7) . . ?
C37 Ag9B Ag4A 45.1(4) . . ?
C1 Ag9B Ag4A 149.5(10) . . ?
Ag10 Ag9B Ag4A 127.3(5) . . ?
Ag11 Ag9B Ag4A 55.8(2) . . ?
Ag2A Ag9B Ag4A 102.6(8) . . ?
Ag4B Ag9B Ag4A 3.6(5) . . ?
Ag2B Ag9B Ag4A 108.7(7) . . ?
C1 Ag10 C13 150.8(3) . . ?
C1 Ag10 O1 102.4(2) . . ?
C13 Ag10 O1 99.5(2) . . ?
C1 Ag10 O2 106.5(2) . . ?
C13 Ag10 O2 96.8(2) . . ?
O1 Ag10 O2 77.60(18) . . ?
C1 Ag10 Ag16 104.26(19) . . ?
C13 Ag10 Ag16 46.76(18) . . ?
O1 Ag10 Ag16 135.74(14) . . ?
O2 Ag10 Ag16 126.04(13) . . ?
C1 Ag10 Ag9B 46.4(2) . . ?
C13 Ag10 Ag9B 128.9(4) . . ?
O1 Ag10 Ag9B 125.6(5) . . ?
O2 Ag10 Ag9B 74.0(3) . . ?
Ag16 Ag10 Ag9B 98.2(5) . . ?
C1 Ag10 Ag2B 47.74(19) . . ?
C13 Ag10 Ag2B 103.13(18) . . ?
O1 Ag10 Ag2B 129.48(15) . . ?
O2 Ag10 Ag2B 141.58(13) . . ?
Ag16 Ag10 Ag2B 57.52(4) . . ?
Ag9B Ag10 Ag2B 67.9(3) . . ?
C1 Ag10 Ag9A 46.9(2) . . ?
C13 Ag10 Ag9A 121.57(18) . . ?
O1 Ag10 Ag9A 136.29(16) . . ?
O2 Ag10 Ag9A 83.03(17) . . ?
Ag16 Ag10 Ag9A 86.98(10) . . ?
Ag2B Ag10 Ag9A 58.55(12) . . ?
C1 Ag10 Ag3A 132.3(12) . . ?
C13 Ag10 Ag3A 42.8(5) . . ?
O1 Ag10 Ag3A 121.0(18) . . ?
O2 Ag10 Ag3A 68.4(17) . . ?
Ag16 Ag10 Ag3A 58.1(18) . . ?
Ag2B Ag10 Ag3A 106.0(19) . . ?
Ag9A Ag10 Ag3A 86.1(10) . . ?
C1 Ag10 Ag2A 45.4(5) . . ?
C13 Ag10 Ag2A 105.4(5) . . ?
O1 Ag10 Ag2A 135.4(4) . . ?
O2 Ag10 Ag2A 133.5(4) . . ?
Ag16 Ag10 Ag2A 58.8(5) . . ?
Ag9B Ag10 Ag2A 60.1(5) . . ?
Ag2B Ag10 Ag2A 8.3(4) . . ?
Ag9A Ag10 Ag2A 50.5(4) . . ?
Ag3A Ag10 Ag2A 102.1(19) . . ?
C1 Ag10 Ag3B 139.0(2) . . ?
C13 Ag10 Ag3B 42.78(17) . . ?
O1 Ag10 Ag3B 111.50(16) . . ?
O2 Ag10 Ag3B 61.40(13) . . ?
Ag16 Ag10 Ag3B 66.20(5) . . ?
Ag9B Ag10 Ag3B 93.88(16) . . ?
Ag2B Ag10 Ag3B 115.86(7) . . ?
Ag2A Ag10 Ag3B 112.0(4) . . ?
C19 Ag11 C37 171.2(3) . . ?
C19 Ag11 Ag15 53.9(3) . . ?
C37 Ag11 Ag15 123.6(3) . . ?
C19 Ag11 Ag4A 124.4(2) . . ?
C37 Ag11 Ag4A 52.1(2) . . ?
Ag15 Ag11 Ag4A 71.5(3) . . ?
C19 Ag11 A15 53.6(2) . . ?
C37 Ag11 A15 124.5(2) . . ?
Ag15 Ag11 A15 3.5(3) . . ?
Ag4A Ag11 A15 72.64(13) . . ?
C19 Ag11 Ag3A 51.5(6) . . ?
C37 Ag11 Ag3A 136.7(7) . . ?
Ag15 Ag11 Ag3A 64.9(17) . . ?
Ag4A Ag11 Ag3A 116(2) . . ?
A15 Ag11 Ag3A 61.7(17) . . ?
C19 Ag11 Ag9B 143.0(3) . . ?
C37 Ag11 Ag9B 45.4(2) . . ?
Ag15 Ag11 Ag9B 115.8(5) . . ?
Ag4A Ag11 Ag9B 67.9(3) . . ?
A15 Ag11 Ag9B 113.7(4) . . ?
C19 Ag11 Ag3B 45.9(2) . . ?
C37 Ag11 Ag3B 142.8(2) . . ?
Ag15 Ag11 Ag3B 70.2(3) . . ?
Ag4A Ag11 Ag3B 126.61(10) . . ?
A15 Ag11 Ag3B 67.33(10) . . ?
Ag9B Ag11 Ag3B 97.63(14) . . ?
C19 Ag11 Ag4B 127.3(4) . . ?
C37 Ag11 Ag4B 49.5(4) . . ?
Ag15 Ag11 Ag4B 74.1(4) . . ?
Ag4A Ag11 Ag4B 3.5(4) . . ?
A15 Ag11 Ag4B 75.0(3) . . ?
Ag3A Ag11 Ag4B 116(2) . . ?
Ag9B Ag11 Ag4B 64.4(5) . . ?
Ag3B Ag11 Ag4B 126.5(2) . . ?
C19 Ag11 Ag9A 138.9(2) . . ?
C37 Ag11 Ag9A 48.5(2) . . ?
Ag15 Ag11 Ag9A 104.3(3) . . ?
Ag4A Ag11 Ag9A 59.46(14) . . ?
A15 Ag11 Ag9A 102.45(12) . . ?
Ag3A Ag11 Ag9A 88.6(9) . . ?
Ag4B Ag11 Ag9A 56.1(3) . . ?
C31 Ag12 C49 154.5(3) . . ?
C31 Ag12 O4 102.3(3) . . ?
C49 Ag12 O4 94.1(3) . . ?
C31 Ag12 O3 101.9(2) . . ?
C49 Ag12 O3 100.9(2) . . ?
O4 Ag12 O3 76.24(19) . . ?
C31 Ag12 Ag7C 116.2(4) . . ?
C49 Ag12 Ag7C 51.4(4) . . ?
O4 Ag12 Ag7C 141.4(5) . . ?
O3 Ag12 Ag7C 92.4(7) . . ?
C31 Ag12 Ag14 107.06(19) . . ?
C49 Ag12 Ag14 49.27(18) . . ?
O4 Ag12 Ag14 137.17(17) . . ?
O3 Ag12 Ag14 125.51(15) . . ?
Ag7C Ag12 Ag14 33.3(6) . . ?
C31 Ag12 Ag8A 45.2(2) . . ?
C49 Ag12 Ag8A 133.9(3) . . ?
O4 Ag12 Ag8A 126.8(4) . . ?
O3 Ag12 Ag8A 73.7(3) . . ?
Ag14 Ag12 Ag8A 95.9(3) . . ?
C31 Ag12 Ag8C 45.1(4) . . ?
C49 Ag12 Ag8C 135.6(6) . . ?
O4 Ag12 Ag8C 124.3(9) . . ?
O3 Ag12 Ag8C 71.7(8) . . ?
Ag7C Ag12 Ag8C 84.6(8) . . ?
Ag14 Ag12 Ag8C 98.4(9) . . ?
C31 Ag12 Ag6C 40.0(4) . . ?
C49 Ag12 Ag6C 118.5(4) . . ?
O4 Ag12 Ag6C 141.0(4) . . ?
O3 Ag12 Ag6C 114.3(6) . . ?
Ag7C Ag12 Ag6C 77.3(6) . . ?
Ag14 Ag12 Ag6C 69.2(4) . . ?
Ag8C Ag12 Ag6C 43.0(11) . . ?
C31 Ag12 Ag7B 136.9(4) . . ?
C49 Ag12 Ag7B 47.1(4) . . ?
O4 Ag12 Ag7B 113.3(4) . . ?
O3 Ag12 Ag7B 65.9(3) . . ?
Ag14 Ag12 Ag7B 61.3(2) . . ?
C31 Ag12 Ag6A 45.6(3) . . ?
C49 Ag12 Ag6A 108.9(3) . . ?
O4 Ag12 Ag6A 126.0(4) . . ?
O3 Ag12 Ag6A 140.0(3) . . ?
Ag14 Ag12 Ag6A 64.0(3) . . ?
Ag8A Ag12 Ag6A 66.5(4) . . ?
C31 Ag12 Ag7A 140.3(2) . . ?
C49 Ag12 Ag7A 44.6(2) . . ?
O4 Ag12 Ag7A 110.4(2) . . ?
O3 Ag12 Ag7A 66.14(17) . . ?
Ag14 Ag12 Ag7A 61.97(5) . . ?
Ag8A Ag12 Ag7A 95.9(2) . . ?
Ag6A Ag12 Ag7A 120.4(4) . . ?
C67 Ag13 C61 156.8(3) . . ?
C67 Ag13 O10 104.6(2) . . ?
C61 Ag13 O10 93.7(3) . . ?
C67 Ag13 Ag5 108.05(17) . . ?
C61 Ag13 Ag5 49.1(2) . . ?
O10 Ag13 Ag5 135.64(15) . . ?
C67 Ag13 Ag17 49.47(17) . . ?
C61 Ag13 Ag17 107.9(2) . . ?
O10 Ag13 Ag17 145.9(2) . . ?
Ag5 Ag13 Ag17 58.78(2) . . ?
C67 Ag13 Ag4A 56.3(2) . . ?
C61 Ag13 Ag4A 143.0(3) . . ?
O10 Ag13 Ag4A 79.96(18) . . ?
Ag5 Ag13 Ag4A 143.83(8) . . ?
Ag17 Ag13 Ag4A 96.39(11) . . ?
C67 Ag13 Ag4B 60.5(5) . . ?
C61 Ag13 Ag4B 138.8(5) . . ?
O10 Ag13 Ag4B 78.7(3) . . ?
Ag5 Ag13 Ag4B 144.2(3) . . ?
Ag17 Ag13 Ag4B 99.7(4) . . ?
Ag4A Ag13 Ag4B 4.3(5) . . ?
C67 Ag13 Ag8B 129.0(2) . . ?
C61 Ag13 Ag8B 50.2(3) . . ?
O10 Ag13 Ag8B 115.0(2) . . ?
Ag5 Ag13 Ag8B 63.31(15) . . ?
Ag17 Ag13 Ag8B 99.04(10) . . ?
Ag4A Ag13 Ag8B 99.6(2) . . ?
Ag4B Ag13 Ag8B 96.4(4) . . ?
C67 Ag13 Ag8A 135.3(3) . . ?
C61 Ag13 Ag8A 41.6(3) . . ?
O10 Ag13 Ag8A 113.9(2) . . ?
Ag5 Ag13 Ag8A 57.4(2) . . ?
Ag17 Ag13 Ag8A 99.56(13) . . ?
Ag4A Ag13 Ag8A 108.2(3) . . ?
Ag4B Ag13 Ag8A 104.9(4) . . ?
C67 Ag13 Ag8C 137.5(6) . . ?
C61 Ag13 Ag8C 39.1(8) . . ?
O10 Ag13 Ag8C 112.6(4) . . ?
Ag5 Ag13 Ag8C 56.6(5) . . ?
Ag17 Ag13 Ag8C 100.6(3) . . ?
Ag4A Ag13 Ag8C 110.2(7) . . ?
Ag4B Ag13 Ag8C 106.8(8) . . ?
C67 Ag13 Ag1 68.99(18) . . ?
C61 Ag13 Ag1 109.2(2) . . ?
O10 Ag13 Ag1 131.18(17) . . ?
Ag5 Ag13 Ag1 88.87(2) . . ?
Ag17 Ag13 Ag1 66.394(19) . . ?
Ag4A Ag13 Ag1 55.62(8) . . ?
Ag4B Ag13 Ag1 55.4(3) . . ?
Ag8B Ag13 Ag1 61.03(19) . . ?
Ag8A Ag13 Ag1 68.8(2) . . ?
Ag8C Ag13 Ag1 71.2(7) . . ?
Ag7C Ag14 C49 67.4(8) . . ?
Ag7C Ag14 C43 149.5(7) . . ?
C49 Ag14 C43 133.2(3) . . ?
Ag7C Ag14 C25 68.1(9) . . ?
C49 Ag14 C25 125.1(3) . . ?
C43 Ag14 C25 101.0(2) . . ?
Ag7C Ag14 C44 156.8(10) . . ?
C49 Ag14 C44 106.1(3) . . ?
C43 Ag14 C44 27.3(2) . . ?
C25 Ag14 C44 127.0(2) . . ?
Ag7C Ag14 Ag12 66.4(10) . . ?
C49 Ag14 Ag12 51.6(2) . . ?
C43 Ag14 Ag12 106.51(17) . . ?
C25 Ag14 Ag12 129.14(17) . . ?
C44 Ag14 Ag12 91.80(15) . . ?
C49 Ag14 Ag7B 47.4(4) . . ?
C43 Ag14 Ag7B 165.6(4) . . ?
C25 Ag14 Ag7B 82.6(3) . . ?
C44 Ag14 Ag7B 150.1(3) . . ?
Ag12 Ag14 Ag7B 61.6(2) . . ?
Ag7C Ag14 Ag1 71.3(7) . . ?
C49 Ag14 Ag1 136.63(19) . . ?
C43 Ag14 Ag1 81.38(17) . . ?
C25 Ag14 Ag1 43.61(16) . . ?
C44 Ag14 Ag1 106.61(16) . . ?
Ag12 Ag14 Ag1 99.71(2) . . ?
Ag7B Ag14 Ag1 92.2(3) . . ?
C49 Ag14 Ag7A 44.7(2) . . ?
C43 Ag14 Ag7A 167.65(19) . . ?
C25 Ag14 Ag7A 84.30(18) . . ?
C44 Ag14 Ag7A 148.66(17) . . ?
Ag12 Ag14 Ag7A 62.11(7) . . ?
Ag1 Ag14 Ag7A 95.39(11) . . ?
Ag7C Ag14 Ag16 127.0(9) . . ?
C49 Ag14 Ag16 155.7(2) . . ?
C43 Ag14 Ag16 45.80(17) . . ?
C25 Ag14 Ag16 59.62(16) . . ?
C44 Ag14 Ag16 68.14(15) . . ?
Ag12 Ag14 Ag16 148.19(3) . . ?
Ag7B Ag14 Ag16 141.8(3) . . ?
Ag1 Ag14 Ag16 65.339(19) . . ?
Ag7A Ag14 Ag16 142.90(7) . . ?
C49 Ag14 Ag6B 113.3(2) . . ?
C43 Ag14 Ag6B 51.34(19) . . ?
C25 Ag14 Ag6B 106.5(2) . . ?
C44 Ag14 Ag6B 58.1(2) . . ?
Ag12 Ag14 Ag6B 63.85(9) . . ?
Ag7B Ag14 Ag6B 114.2(3) . . ?
Ag1 Ag14 Ag6B 63.86(14) . . ?
Ag16 Ag14 Ag6B 84.40(9) . . ?
C49 Ag14 Ag6A 107.8(3) . . ?
C43 Ag14 Ag6A 50.3(3) . . ?
C25 Ag14 Ag6A 114.5(4) . . ?
C44 Ag14 Ag6A 52.7(3) . . ?
Ag12 Ag14 Ag6A 60.5(2) . . ?
Ag1 Ag14 Ag6A 72.0(3) . . ?
Ag7A Ag14 Ag6A 117.4(2) . . ?
Ag16 Ag14 Ag6A 87.8(2) . . ?
C19 Ag15 O7 89.9(5) . . ?
C19 Ag15 C67 138.8(7) . . ?
O7 Ag15 C67 106.8(5) . . ?
C19 Ag15 C25 114.0(5) . . ?
O7 Ag15 C25 99.3(6) . . ?
C67 Ag15 C25 100.4(5) . . ?
C19 Ag15 Ag11 47.9(3) . . ?
O7 Ag15 Ag11 136.1(5) . . ?
C67 Ag15 Ag11 101.0(6) . . ?
C25 Ag15 Ag11 108.4(4) . . ?
C19 Ag15 Ag17 169.9(7) . . ?
O7 Ag15 Ag17 80.0(4) . . ?
C67 Ag15 Ag17 47.0(3) . . ?
C25 Ag15 Ag17 67.4(3) . . ?
Ag11 Ag15 Ag17 142.0(5) . . ?
C19 Ag15 Ag3A 48.3(17) . . ?
O7 Ag15 Ag3A 104.8(6) . . ?
C67 Ag15 Ag3A 147.4(9) . . ?
C25 Ag15 Ag3A 66.3(17) . . ?
Ag11 Ag15 Ag3A 59.7(12) . . ?
Ag17 Ag15 Ag3A 133.6(18) . . ?
C19 Ag15 Ag1 119.8(5) . . ?
O7 Ag15 Ag1 136.7(6) . . ?
C67 Ag15 Ag1 72.3(4) . . ?
C25 Ag15 Ag1 41.9(2) . . ?
Ag11 Ag15 Ag1 83.9(3) . . ?
Ag17 Ag15 Ag1 68.4(2) . . ?
Ag3A Ag15 Ag1 79.2(13) . . ?
C19 Ag15 Ag4A 103.2(5) . . ?
O7 Ag15 Ag4A 153.4(5) . . ?
C67 Ag15 Ag4A 48.8(3) . . ?
C25 Ag15 Ag4A 96.3(4) . . ?
Ag11 Ag15 Ag4A 56.0(3) . . ?
Ag17 Ag15 Ag4A 86.4(3) . . ?
Ag3A Ag15 Ag4A 101.2(5) . . ?
Ag1 Ag15 Ag4A 54.5(2) . . ?
C19 Ag15 Ag3B 40.1(3) . . ?
O7 Ag15 Ag3B 99.8(5) . . ?
C67 Ag15 Ag3B 153.3(6) . . ?
C25 Ag15 Ag3B 74.1(3) . . ?
Ag11 Ag15 Ag3B 58.3(2) . . ?
Ag17 Ag15 Ag3B 140.8(5) . . ?
Ag1 Ag15 Ag3B 87.8(3) . . ?
Ag4A Ag15 Ag3B 105.1(4) . . ?
O7 A15 C19 89.3(3) . . ?
O7 A15 C67 105.4(3) . . ?
C19 A15 C67 129.4(3) . . ?
O7 A15 C25 106.5(3) . . ?
C19 A15 C25 118.6(3) . . ?
C67 A15 C25 103.4(3) . . ?
O7 A15 Ag11 131.8(2) . . ?
C19 A15 Ag11 45.72(19) . . ?
C67 A15 Ag11 95.5(2) . . ?
C25 A15 Ag11 110.1(2) . . ?
O7 A15 Ag17 82.3(2) . . ?
C19 A15 Ag17 169.0(2) . . ?
C67 A15 Ag17 47.63(17) . . ?
C25 A15 Ag17 70.9(2) . . ?
Ag11 A15 Ag17 139.01(19) . . ?
O7 A15 Ag3A 108.4(5) . . ?
C19 A15 Ag3A 49.2(17) . . ?
C67 A15 Ag3A 146.1(5) . . ?
C25 A15 Ag3A 69.7(17) . . ?
Ag11 A15 Ag3A 59.2(11) . . ?
Ag17 A15 Ag3A 140.5(17) . . ?
O7 A15 Ag1 144.3(3) . . ?
C19 A15 Ag1 120.1(2) . . ?
C67 A15 Ag1 72.6(2) . . ?
C25 A15 Ag1 43.52(17) . . ?
Ag11 A15 Ag1 83.11(12) . . ?
Ag17 A15 Ag1 70.30(10) . . ?
Ag3A A15 Ag1 81.6(12) . . ?
O7 A15 Ag3B 102.5(2) . . ?
C19 A15 Ag3B 41.2(2) . . ?
C67 A15 Ag3B 150.4(3) . . ?
C25 A15 Ag3B 77.4(2) . . ?
Ag11 A15 Ag3B 57.97(9) . . ?
Ag17 A15 Ag3B 147.88(16) . . ?
Ag1 A15 Ag3B 90.12(13) . . ?
C13 Ag16 C43 153.5(3) . . ?
C13 Ag16 Ag2B 115.2(2) . . ?
C43 Ag16 Ag2B 52.38(18) . . ?
C13 Ag16 Ag10 54.1(2) . . ?
C43 Ag16 Ag10 113.52(18) . . ?
Ag2B Ag16 Ag10 62.59(4) . . ?
C13 Ag16 Ag3A 46.3(15) . . ?
C43 Ag16 Ag3A 156.3(10) . . ?
Ag2B Ag16 Ag3A 115.4(6) . . ?
Ag10 Ag16 Ag3A 64.6(14) . . ?
C13 Ag16 Ag2A 118.7(5) . . ?
C43 Ag16 Ag2A 53.3(5) . . ?
Ag2B Ag16 Ag2A 8.9(4) . . ?
Ag10 Ag16 Ag2A 64.8(5) . . ?
Ag3A Ag16 Ag2A 111.2(7) . . ?
C13 Ag16 Ag14 151.1(2) . . ?
C43 Ag16 Ag14 51.14(17) . . ?
Ag2B Ag16 Ag14 93.12(4) . . ?
Ag10 Ag16 Ag14 149.88(3) . . ?
Ag3A Ag16 Ag14 117.7(17) . . ?
Ag2A Ag16 Ag14 88.5(4) . . ?
C13 Ag16 Ag1 123.93(19) . . ?
C43 Ag16 Ag1 78.11(18) . . ?
Ag2B Ag16 Ag1 74.05(3) . . ?
Ag10 Ag16 Ag1 97.54(2) . . ?
Ag3A Ag16 Ag1 78.8(13) . . ?
Ag2A Ag16 Ag1 65.2(4) . . ?
Ag14 Ag16 Ag1 56.468(18) . . ?
C13 Ag16 Ag3B 40.17(19) . . ?
C43 Ag16 Ag3B 161.92(19) . . ?
Ag2B Ag16 Ag3B 116.94(7) . . ?
Ag10 Ag16 Ag3B 62.46(4) . . ?
Ag2A Ag16 Ag3B 113.7(5) . . ?
Ag14 Ag16 Ag3B 122.65(3) . . ?
Ag1 Ag16 Ag3B 84.88(5) . . ?
C67 Ag17 C55 153.8(3) . . ?
C67 Ag17 O8 108.7(3) . . ?
C55 Ag17 O8 90.5(3) . . ?
C67 Ag17 Ag5 108.08(18) . . ?
C55 Ag17 Ag5 48.3(2) . . ?
O8 Ag17 Ag5 137.33(17) . . ?
C67 Ag17 Ag13 49.00(18) . . ?
C55 Ag17 Ag13 107.2(2) . . ?
O8 Ag17 Ag13 153.5(2) . . ?
Ag5 Ag17 Ag13 59.27(2) . . ?
C67 Ag17 A15 54.7(2) . . ?
C55 Ag17 A15 149.8(2) . . ?
O8 Ag17 A15 78.86(19) . . ?
Ag5 Ag17 A15 141.71(8) . . ?
Ag13 Ag17 A15 93.73(10) . . ?
C67 Ag17 Ag15 51.1(3) . . ?
C55 Ag17 Ag15 153.7(3) . . ?
O8 Ag17 Ag15 79.7(3) . . ?
Ag5 Ag17 Ag15 141.8(2) . . ?
Ag13 Ag17 Ag15 91.3(3) . . ?
A15 Ag17 Ag15 3.9(4) . . ?
C67 Ag17 Ag7C 117.6(4) . . ?
C55 Ag17 Ag7C 67.2(5) . . ?
O8 Ag17 Ag7C 113.4(5) . . ?
Ag5 Ag17 Ag7C 65.7(5) . . ?
Ag13 Ag17 Ag7C 92.0(4) . . ?
A15 Ag17 Ag7C 91.1(5) . . ?
Ag15 Ag17 Ag7C 94.2(5) . . ?
C67 Ag17 Ag7B 143.5(3) . . ?
C55 Ag17 Ag7B 39.6(3) . . ?
O8 Ag17 Ag7B 102.0(3) . . ?
Ag5 Ag17 Ag7B 55.7(2) . . ?
Ag13 Ag17 Ag7B 104.2(3) . . ?
A15 Ag17 Ag7B 115.0(2) . . ?
Ag15 Ag17 Ag7B 118.6(3) . . ?
C76 O1 Ag10 127.7(5) . . ?
C74 O2 Ag10 126.7(5) . . ?
C81 O3 Ag12 128.3(5) . . ?
C81 O3 Ag5 134.8(5) . . ?
Ag12 O3 Ag5 96.83(18) . . ?
C79 O4 Ag12 130.8(6) . . ?
C87 O5 Ag2B 122.3(7) . . ?
C87 O5 Ag2A 114.6(9) . . ?
Ag2B O5 Ag2A 10.7(5) . . ?
C87 O6 Ag6A 129.5(8) . . ?
C87 O6 Ag6B 125.9(7) . . ?
C85 O7 A15 123.1(6) . . ?
C85 O7 Ag15 124.8(6) . . ?
A15 O7 Ag15 5.2(4) . . ?
C85 O8 Ag17 125.6(6) . . ?
C83 O9 Ag4B 122.9(6) . . ?
C83 O9 Ag4A 122.4(5) . . ?
Ag4B O9 Ag4A 5.2(7) . . ?
C83 O10 Ag13 125.0(5) . . ?
C2 C1 Ag9B 118.3(8) . . ?
C2 C1 Ag2B 132.8(6) . . ?
Ag9B C1 Ag2B 98.2(7) . . ?
C2 C1 Ag2A 135.2(9) . . ?
Ag9B C1 Ag2A 88.1(9) . . ?
Ag2B C1 Ag2A 12.2(5) . . ?
C2 C1 Ag9A 128.0(6) . . ?
Ag2B C1 Ag9A 82.8(3) . . ?
Ag2A C1 Ag9A 72.3(6) . . ?
C2 C1 Ag10 128.4(6) . . ?
Ag9B C1 Ag10 82.6(3) . . ?
Ag2B C1 Ag10 82.3(3) . . ?
Ag2A C1 Ag10 87.8(7) . . ?
Ag9A C1 Ag10 85.4(3) . . ?
C1 C2 C3 178.4(8) . . ?
C2 C3 C4 109.1(7) . . ?
C2 C3 C6 108.9(7) . . ?
C4 C3 C6 110.5(9) . . ?
C2 C3 C5 107.8(7) . . ?
C4 C3 C5 111.4(9) . . ?
C6 C3 C5 109.0(8) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 Ag1 173.5(6) . . ?
C8 C7 Ag6C 91.3(7) . . ?
Ag1 C7 Ag6C 83.3(5) . . ?
C8 C7 Ag4B 106.9(7) . . ?
Ag1 C7 Ag4B 79.4(5) . . ?
Ag6C C7 Ag4B 154.6(8) . . ?
C8 C7 Ag8B 92.6(5) . . ?
Ag1 C7 Ag8B 85.7(3) . . ?
Ag4B C7 Ag8B 118.6(4) . . ?
C8 C7 Ag4A 110.2(5) . . ?
Ag1 C7 Ag4A 76.0(2) . . ?
Ag6C C7 Ag4A 151.8(7) . . ?
Ag4B C7 Ag4A 3.4(5) . . ?
Ag8B C7 Ag4A 117.4(3) . . ?
C8 C7 Ag9A 96.3(5) . . ?
Ag1 C7 Ag9A 84.5(2) . . ?
Ag4B C7 Ag9A 67.2(4) . . ?
Ag4A C7 Ag9A 67.7(2) . . ?
C7 C8 C9 178.0(8) . . ?
C7 C8 Ag6C 60.1(6) . . ?
C9 C8 Ag6C 121.5(7) . . ?
C8 C9 C10 109.7(8) . . ?
C8 C9 C11 110.0(7) . . ?
C10 C9 C11 112.0(9) . . ?
C8 C9 C12 109.4(7) . . ?
C10 C9 C12 109.1(10) . . ?
C11 C9 C12 106.6(8) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag3A 104(2) . . ?
C14 C13 Ag16 160.8(6) . . ?
Ag3A C13 Ag16 87(3) . . ?
C14 C13 Ag3B 89.1(5) . . ?
Ag16 C13 Ag3B 101.5(3) . . ?
C14 C13 Ag10 117.0(6) . . ?
Ag3A C13 Ag10 87.1(8) . . ?
Ag16 C13 Ag10 79.2(2) . . ?
Ag3B C13 Ag10 90.7(3) . . ?
C13 C14 C15 174.7(7) . . ?
C13 C14 Ag3B 61.7(4) . . ?
C15 C14 Ag3B 123.3(5) . . ?
C13 C14 Ag3A 49.8(16) . . ?
C15 C14 Ag3A 135.3(17) . . ?
C14 C15 C16 110.7(7) . . ?
C14 C15 C18 108.1(6) . . ?
C16 C15 C18 110.9(8) . . ?
C14 C15 C17 107.4(7) . . ?
C16 C15 C17 110.2(7) . . ?
C18 C15 C17 109.5(8) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C15 C17 H17A 109.5 . . ?
C15 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C15 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 Ag11 156.3(7) . . ?
C20 C19 Ag3B 93.6(6) . . ?
Ag11 C19 Ag3B 89.8(3) . . ?
C20 C19 Ag15 124.5(7) . . ?
Ag11 C19 Ag15 78.2(4) . . ?
Ag3B C19 Ag15 96.9(4) . . ?
C20 C19 Ag3A 105.0(13) . . ?
Ag11 C19 Ag3A 82.6(5) . . ?
Ag15 C19 Ag3A 83(3) . . ?
C20 C19 A15 122.5(6) . . ?
Ag11 C19 A15 80.7(3) . . ?
Ag3B C19 A15 92.7(3) . . ?
Ag15 C19 A15 4.9(5) . . ?
Ag3A C19 A15 79(3) . . ?
C19 C20 C21 172.7(8) . . ?
C19 C20 Ag3B 58.2(5) . . ?
C21 C20 Ag3B 129.1(5) . . ?
C20 C21 C22 110.2(7) . . ?
C20 C21 C23 109.3(7) . . ?
C22 C21 C23 110.8(8) . . ?
C20 C21 C24 107.2(7) . . ?
C22 C21 C24 110.2(8) . . ?
C23 C21 C24 109.1(8) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 Ag1 169.5(6) . . ?
C26 C25 Ag7C 94.8(7) . . ?
Ag1 C25 Ag7C 80.3(5) . . ?
C26 C25 Ag14 89.2(5) . . ?
Ag1 C25 Ag14 81.2(2) . . ?
Ag7C C25 Ag14 37.8(7) . . ?
C26 C25 A15 108.9(6) . . ?
Ag1 C25 A15 81.1(3) . . ?
Ag7C C25 A15 129.8(7) . . ?
Ag14 C25 A15 160.4(3) . . ?
C26 C25 Ag15 111.0(6) . . ?
Ag1 C25 Ag15 79.0(4) . . ?
Ag7C C25 Ag15 129.4(7) . . ?
Ag14 C25 Ag15 158.6(4) . . ?
A15 C25 Ag15 2.1(4) . . ?
C25 C26 C27 178.4(8) . . ?
C26 C27 C28 109.4(7) . . ?
C26 C27 C29 107.7(7) . . ?
C28 C27 C29 110.5(8) . . ?
C26 C27 C30 108.8(6) . . ?
C28 C27 C30 110.6(7) . . ?
C29 C27 C30 109.8(7) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 Ag6C 142.5(9) . . ?
C32 C31 Ag8A 130.9(7) . . ?
C32 C31 Ag8C 127.5(12) . . ?
Ag6C C31 Ag8C 65.4(17) . . ?
C32 C31 Ag6A 119.3(8) . . ?
Ag8A C31 Ag6A 100.3(7) . . ?
C32 C31 Ag8B 139.2(7) . . ?
C32 C31 Ag12 122.1(6) . . ?
Ag6C C31 Ag12 91.3(6) . . ?
Ag8A C31 Ag12 85.4(3) . . ?
Ag8C C31 Ag12 86.3(5) . . ?
Ag6A C31 Ag12 86.7(4) . . ?
Ag8B C31 Ag12 87.0(3) . . ?
C32 C31 Ag6B 127.0(6) . . ?
Ag8B C31 Ag6B 76.5(4) . . ?
Ag12 C31 Ag6B 88.4(3) . . ?
C31 C32 C33 178.2(9) . . ?
C32 C33 C36 110.8(8) . . ?
C32 C33 C34 108.0(8) . . ?
C36 C33 C34 110.4(10) . . ?
C32 C33 C35 109.4(8) . . ?
C36 C33 C35 109.2(10) . . ?
C34 C33 C35 109.1(10) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 Ag9B 112.1(8) . . ?
C38 C37 Ag11 144.5(7) . . ?
Ag9B C37 Ag11 88.3(3) . . ?
C38 C37 Ag9A 119.8(6) . . ?
Ag11 C37 Ag9A 87.6(3) . . ?
C38 C37 Ag4B 119.9(7) . . ?
Ag9B C37 Ag4B 92.4(8) . . ?
Ag11 C37 Ag4B 86.2(6) . . ?
Ag9A C37 Ag4B 76.9(5) . . ?
C38 C37 Ag4A 122.4(6) . . ?
Ag9B C37 Ag4A 95.4(7) . . ?
Ag11 C37 Ag4A 81.8(3) . . ?
Ag9A C37 Ag4A 80.0(3) . . ?
Ag4B C37 Ag4A 5.4(7) . . ?
C37 C38 C39 178.8(9) . . ?
C38 C39 C42A 118.9(17) . . ?
C38 C39 C40 111.4(9) . . ?
C38 C39 C41 108.3(7) . . ?
C40 C39 C41 114.0(9) . . ?
C38 C39 C40A 110(2) . . ?
C42A C39 C40A 110.0(16) . . ?
C38 C39 C41A 105.5(15) . . ?
C42A C39 C41A 106.8(14) . . ?
C40A C39 C41A 104.9(14) . . ?
C38 C39 C42 106.2(7) . . ?
C40 C39 C42 108.9(9) . . ?
C41 C39 C42 107.8(8) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C39 C40A H40D 109.5 . . ?
C39 C40A H40E 109.5 . . ?
H40D C40A H40E 109.5 . . ?
C39 C40A H40F 109.5 . . ?
H40D C40A H40F 109.5 . . ?
H40E C40A H40F 109.5 . . ?
C39 C41A H41D 109.5 . . ?
C39 C41A H41E 109.5 . . ?
H41D C41A H41E 109.5 . . ?
C39 C41A H41F 109.5 . . ?
H41D C41A H41F 109.5 . . ?
H41E C41A H41F 109.5 . . ?
C39 C42A H42D 109.5 . . ?
C39 C42A H42E 109.5 . . ?
H42D C42A H42E 109.5 . . ?
C39 C42A H42F 109.5 . . ?
H42D C42A H42F 109.5 . . ?
H42E C42A H42F 109.5 . . ?
C44 C43 Ag16 137.7(6) . . ?
C44 C43 Ag2B 135.5(6) . . ?
Ag16 C43 Ag2B 76.9(2) . . ?
C44 C43 Ag2A 138.7(9) . . ?
Ag16 C43 Ag2A 79.0(6) . . ?
Ag2B C43 Ag2A 11.1(4) . . ?
C44 C43 Ag14 87.5(5) . . ?
Ag16 C43 Ag14 83.1(2) . . ?
Ag2B C43 Ag14 131.2(3) . . ?
Ag2A C43 Ag14 121.5(6) . . ?
C44 C43 Ag6A 83.4(6) . . ?
Ag16 C43 Ag6A 134.5(5) . . ?
Ag2B C43 Ag6A 83.1(4) . . ?
Ag2A C43 Ag6A 74.5(6) . . ?
Ag14 C43 Ag6A 80.2(4) . . ?
C44 C43 Ag6B 93.6(5) . . ?
Ag16 C43 Ag6B 124.3(3) . . ?
Ag2B C43 Ag6B 77.1(3) . . ?
Ag2A C43 Ag6B 67.6(5) . . ?
Ag14 C43 Ag6B 78.5(2) . . ?
C43 C44 C45 170.5(7) . . ?
C43 C44 Ag6A 68.8(6) . . ?
C45 C44 Ag6A 116.4(6) . . ?
C43 C44 Ag14 65.2(4) . . ?
C45 C44 Ag14 123.3(5) . . ?
Ag6A C44 Ag14 73.0(4) . . ?
C44 C45 C48 111.5(6) . . ?
C44 C45 C46 108.1(7) . . ?
C48 C45 C46 109.2(8) . . ?
C44 C45 C47 107.4(6) . . ?
C48 C45 C47 110.3(8) . . ?
C46 C45 C47 110.4(8) . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C45 C47 H47A 109.5 . . ?
C45 C47 H47B 109.5 . . ?
H47A C47 H47B 109.5 . . ?
C45 C47 H47C 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
C45 C48 H48A 109.5 . . ?
C45 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C45 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 Ag7A 110.6(6) . . ?
C50 C49 Ag7C 150.5(10) . . ?
C50 C49 Ag7B 115.2(8) . . ?
C50 C49 Ag14 142.8(7) . . ?
Ag7A C49 Ag14 88.9(3) . . ?
Ag7C C49 Ag14 42.7(8) . . ?
Ag7B C49 Ag14 85.1(5) . . ?
C50 C49 Ag12 131.2(7) . . ?
Ag7A C49 Ag12 87.1(3) . . ?
Ag7C C49 Ag12 73.3(7) . . ?
Ag7B C49 Ag12 83.7(5) . . ?
Ag14 C49 Ag12 79.1(2) . . ?
C49 C50 C51 175.0(10) . . ?
C54 C51 C52 116.9(16) . . ?
C54 C51 C50 108.8(10) . . ?
C52 C51 C50 108.8(10) . . ?
C54 C51 C53 108.0(13) . . ?
C52 C51 C53 106.2(14) . . ?
C50 C51 C53 107.8(9) . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C51 C53 H53A 109.5 . . ?
C51 C53 H53B 109.5 . . ?
H53A C53 H53B 109.5 . . ?
C51 C53 H53C 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C51 C54 H54A 109.5 . . ?
C51 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C51 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C56 C55 Ag7B 96.4(8) . . ?
C56 C55 Ag5 146.9(8) . . ?
Ag7B C55 Ag5 85.4(5) . . ?
C56 C55 Ag7A 91.9(6) . . ?
Ag5 C55 Ag7A 88.8(3) . . ?
C56 C55 Ag17 132.6(8) . . ?
Ag7B C55 Ag17 97.3(5) . . ?
Ag5 C55 Ag17 79.4(2) . . ?
Ag7A C55 Ag17 100.8(3) . . ?
C55 C56 C57 172.7(9) . . ?
C55 C56 Ag7A 59.6(5) . . ?
C57 C56 Ag7A 127.6(6) . . ?
C55 C56 Ag7B 55.5(6) . . ?
C57 C56 Ag7B 131.7(7) . . ?
C59 C57 C56 115.0(12) . . ?
C60A C57 C56 112.6(16) . . ?
C59 C57 C58 113.4(11) . . ?
C56 C57 C58 108.2(11) . . ?
C60A C57 C59A 116.1(14) . . ?
C56 C57 C59A 105.9(13) . . ?
C60A C57 C58A 111.8(13) . . ?
C56 C57 C58A 101.9(15) . . ?
C59A C57 C58A 107.4(13) . . ?
C59 C57 C60 109.1(11) . . ?
C56 C57 C60 106.5(9) . . ?
C58 C57 C60 103.8(10) . . ?
C57 C58 H58A 109.5 . . ?
C57 C58 H58B 109.5 . . ?
H58A C58 H58B 109.5 . . ?
C57 C58 H58C 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C57 C59 H59A 109.5 . . ?
C57 C59 H59B 109.5 . . ?
H59A C59 H59B 109.5 . . ?
C57 C59 H59C 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C57 C60 H60A 109.5 . . ?
C57 C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C57 C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C57 C58A H58D 109.5 . . ?
C57 C58A H58E 109.5 . . ?
H58D C58A H58E 109.5 . . ?
C57 C58A H58F 109.5 . . ?
H58D C58A H58F 109.5 . . ?
H58E C58A H58F 109.5 . . ?
C57 C59A H59D 109.5 . . ?
C57 C59A H59E 109.5 . . ?
H59D C59A H59E 109.5 . . ?
C57 C59A H59F 109.5 . . ?
H59D C59A H59F 109.5 . . ?
H59E C59A H59F 109.5 . . ?
C57 C60A H60D 109.5 . . ?
C57 C60A H60E 109.5 . . ?
H60D C60A H60E 109.5 . . ?
C57 C60A H60F 109.5 . . ?
H60D C60A H60F 109.5 . . ?
H60E C60A H60F 109.5 . . ?
C62 C61 Ag8C 119.5(13) . . ?
C62 C61 Ag8A 122.4(10) . . ?
C62 C61 Ag5 134.9(8) . . ?
Ag8C C61 Ag5 86.2(6) . . ?
Ag8A C61 Ag5 85.0(4) . . ?
C62 C61 Ag13 127.3(8) . . ?
Ag8C C61 Ag13 96.3(13) . . ?
Ag8A C61 Ag13 92.9(6) . . ?
Ag5 C61 Ag13 80.1(3) . . ?
C62 C61 Ag8B 129.0(9) . . ?
Ag5 C61 Ag8B 85.6(3) . . ?
Ag13 C61 Ag8B 80.9(3) . . ?
C61 C62 C63A 162.9(16) . . ?
C61 C62 C63 164.7(16) . . ?
C62 C63 C65 116.8(18) . . ?
C62 C63 C64 104.4(17) . . ?
C65 C63 C64 112.8(13) . . ?
C62 C63 C66 98(2) . . ?
C65 C63 C66 112.3(13) . . ?
C64 C63 C66 111.5(14) . . ?
C63 C64 H64A 109.5 . . ?
C63 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C63 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C63 C65 H65A 109.5 . . ?
C63 C65 H65B 109.5 . . ?
H65A C65 H65B 109.5 . . ?
C63 C65 H65C 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
C63 C66 H66A 109.5 . . ?
C63 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C63 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C62 C63A C64A 117(2) . . ?
C62 C63A C65A 111(3) . . ?
C64A C63A C65A 109.8(17) . . ?
C62 C63A C66A 102(3) . . ?
C64A C63A C66A 108.7(17) . . ?
C65A C63A C66A 107.6(17) . . ?
C63A C64A H64D 109.5 . . ?
C63A C64A H64E 109.5 . . ?
H64D C64A H64E 109.5 . . ?
C63A C64A H64F 109.5 . . ?
H64D C64A H64F 109.5 . . ?
H64E C64A H64F 109.5 . . ?
C63A C65A H65D 109.5 . . ?
C63A C65A H65E 109.5 . . ?
H65D C65A H65E 109.5 . . ?
C63A C65A H65F 109.5 . . ?
H65D C65A H65F 109.5 . . ?
H65E C65A H65F 109.5 . . ?
C63A C66A H66D 109.5 . . ?
C63A C66A H66E 109.5 . . ?
H66D C66A H66E 109.5 . . ?
C63A C66A H66F 109.5 . . ?
H66D C66A H66F 109.5 . . ?
H66E C66A H66F 109.5 . . ?
C68 C67 Ag13 127.2(6) . . ?
C68 C67 Ag17 136.5(6) . . ?
Ag13 C67 Ag17 81.5(2) . . ?
C68 C67 Ag15 92.6(6) . . ?
Ag13 C67 Ag15 134.8(4) . . ?
Ag17 C67 Ag15 81.9(4) . . ?
C68 C67 A15 96.9(5) . . ?
Ag13 C67 A15 131.7(3) . . ?
Ag17 C67 A15 77.6(2) . . ?
Ag15 C67 A15 4.6(4) . . ?
C68 C67 Ag4A 89.1(5) . . ?
Ag13 C67 Ag4A 76.0(2) . . ?
Ag17 C67 Ag4A 132.9(3) . . ?
Ag15 C67 Ag4A 85.4(4) . . ?
A15 C67 Ag4A 87.2(3) . . ?
C68 C67 Ag4B 91.6(6) . . ?
Ag13 C67 Ag4B 72.9(5) . . ?
Ag17 C67 Ag4B 130.9(4) . . ?
Ag15 C67 Ag4B 87.3(5) . . ?
A15 C67 Ag4B 88.9(4) . . ?
Ag4A C67 Ag4B 3.2(5) . . ?
C67 C68 C69 173.5(8) . . ?
C70 C69 C68 109.9(8) . . ?
C70 C69 C72 112.7(10) . . ?
C68 C69 C72 106.9(8) . . ?
C70 C69 C71 112.2(10) . . ?
C68 C69 C71 109.3(8) . . ?
C72 C69 C71 105.6(9) . . ?
C69 C70 H70A 109.5 . . ?
C69 C70 H70B 109.5 . . ?
H70A C70 H70B 109.5 . . ?
C69 C70 H70C 109.5 . . ?
H70A C70 H70C 109.5 . . ?
H70B C70 H70C 109.5 . . ?
C69 C71 H71A 109.5 . . ?
C69 C71 H71B 109.5 . . ?
H71A C71 H71B 109.5 . . ?
C69 C71 H71C 109.5 . . ?
H71A C71 H71C 109.5 . . ?
H71B C71 H71C 109.5 . . ?
C69 C72 H72A 109.5 . . ?
C69 C72 H72B 109.5 . . ?
H72A C72 H72B 109.5 . . ?
C69 C72 H72C 109.5 . . ?
H72A C72 H72C 109.5 . . ?
H72B C72 H72C 109.5 . . ?
F10A C73 F11A 111.8(13) . . ?
F10 C73 F12 113.5(11) . . ?
F10 C73 F11 101.8(9) . . ?
F12 C73 F11 101.9(9) . . ?
F10A C73 F12A 99.6(13) . . ?
F11A C73 F12A 98.0(13) . . ?
F10A C73 C74 119.9(12) . . ?
F10 C73 C74 117.3(9) . . ?
F11A C73 C74 117.8(14) . . ?
F12 C73 C74 112.7(9) . . ?
F11 C73 C74 107.4(8) . . ?
F12A C73 C74 104.7(10) . . ?
O2 C74 C75 130.3(8) . . ?
O2 C74 C73 113.1(7) . . ?
C75 C74 C73 116.5(7) . . ?
C74 C75 C76 124.9(8) . . ?
C74 C75 H75 117.5 . . ?
C76 C75 H75 117.5 . . ?
O1 C76 C75 130.4(7) . . ?
O1 C76 C77 113.6(7) . . ?
C75 C76 C77 116.0(7) . . ?
F8 C77 F7 110.2(11) . . ?
F8A C77 F9A 109.8(16) . . ?
F8 C77 F9 105.0(10) . . ?
F7 C77 F9 102.8(9) . . ?
F8A C77 F7A 106.0(14) . . ?
F9A C77 F7A 101.6(14) . . ?
F8 C77 C76 113.7(9) . . ?
F8A C77 C76 119.8(17) . . ?
F7 C77 C76 111.9(9) . . ?
F9A C77 C76 109.9(17) . . ?
F9 C77 C76 112.5(8) . . ?
F7A C77 C76 108.0(11) . . ?
F6 C78 F4 113.0(13) . . ?
F6 C78 F5 100.4(12) . . ?
F4 C78 F5 100.8(11) . . ?
F6 C78 C79 116.5(9) . . ?
F4 C78 C79 114.6(9) . . ?
F5 C78 C79 109.3(11) . . ?
O4 C79 C80 130.0(8) . . ?
O4 C79 C78 113.2(8) . . ?
C80 C79 C78 116.8(8) . . ?
C81 C80 C79 125.9(8) . . ?
C81 C80 H80 117.1 . . ?
C79 C80 H80 117.1 . . ?
O3 C81 C80 128.6(8) . . ?
O3 C81 C82 114.1(8) . . ?
C80 C81 C82 117.3(8) . . ?
F1 C82 F2 114.1(13) . . ?
F1 C82 F3 102.9(14) . . ?
F2 C82 F3 99.4(11) . . ?
F1 C82 C81 115.1(8) . . ?
F2 C82 C81 115.1(11) . . ?
F3 C82 C81 107.9(12) . . ?
O10 C83 O9 129.7(7) . . ?
O10 C83 C84 115.1(7) . . ?
O9 C83 C84 115.2(7) . . ?
F21 C84 F19 106.0(9) . . ?
F21 C84 F20 107.2(9) . . ?
F19 C84 F20 103.7(9) . . ?
F21 C84 C83 112.0(8) . . ?
F19 C84 C83 113.7(8) . . ?
F20 C84 C83 113.4(8) . . ?
O8 C85 O7 129.7(8) . . ?
O8 C85 C86 116.2(8) . . ?
O7 C85 C86 114.1(9) . . ?
F17 C86 F16 107.0(10) . . ?
F17 C86 F18 105.6(10) . . ?
F16 C86 F18 104.5(10) . . ?
F17 C86 C85 115.1(10) . . ?
F16 C86 C85 112.1(9) . . ?
F18 C86 C85 111.7(8) . . ?
O5 C87 O6 129.6(10) . . ?
O5 C87 C88 112.2(9) . . ?
O6 C87 C88 118.1(10) . . ?
F15 C88 F13 110.4(13) . . ?
F15 C88 F14 103.4(13) . . ?
F13 C88 F14 105.1(10) . . ?
F15 C88 C87 112.4(10) . . ?
F13 C88 C87 112.1(10) . . ?
F14 C88 C87 112.8(10) . . ?

_refine_diff_density_max         1.031
_refine_diff_density_min         -1.311
_refine_diff_density_rms         0.155

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex7
_database_code_depnum_ccdc_archive 'CCDC 1584347'
_audit_update_record             
;
2017-11-07 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C101 H149 Ag22 F9 N2 O14 P2'
_chemical_formula_weight         4221.29

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.1186(10)
_cell_length_b                   18.0195(12)
_cell_length_c                   26.5054(19)
_cell_angle_alpha                90.783(2)
_cell_angle_beta                 92.624(2)
_cell_angle_gamma                100.746(2)
_cell_volume                     6616.3(8)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9647
_cell_measurement_theta_min      3.0191
_cell_measurement_theta_max      30.5179

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.119
_exptl_crystal_F_000             4052
_exptl_transmission_factor_min   0.5466
_exptl_transmission_factor_max   0.7461
_exptl_crystal_size_max          0.156
_exptl_crystal_size_mid          0.124
_exptl_crystal_size_min          0.089
_exptl_absorpt_coefficient_mu    3.257
_shelx_estimated_absorpt_T_min   0.630
_shelx_estimated_absorpt_T_max   0.760
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            34259
_diffrn_reflns_av_unetI/netI     0.0422
_diffrn_reflns_av_R_equivalents  0.0257
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_theta_min         2.898
_diffrn_reflns_theta_max         23.256
_diffrn_reflns_theta_full        23.256
_diffrn_measured_fraction_theta_max 0.944
_diffrn_measured_fraction_theta_full 0.944
_diffrn_reflns_Laue_measured_fraction_max 0.944
_diffrn_reflns_Laue_measured_fraction_full 0.944
_diffrn_reflns_point_group_measured_fraction_max 0.944
_diffrn_reflns_point_group_measured_fraction_full 0.944
_reflns_number_total             17940
_reflns_number_gt                16213
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0226P)²+169.0811P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         17940
_refine_ls_number_parameters     1449
_refine_ls_number_restraints     1625
_refine_ls_R_factor_all          0.0735
_refine_ls_R_factor_gt           0.0663
_refine_ls_wR_factor_ref         0.1600
_refine_ls_wR_factor_gt          0.1546
_refine_ls_goodness_of_fit_ref   1.174
_refine_ls_restrained_S_all      1.150
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.70584(6) 0.31151(4) 0.25531(3) 0.02141(19) Uani 1 1 d . U . . .
Ag2A Ag 0.9858(17) 0.5211(11) 0.2438(11) 0.040(3) Uani 0.130(16) 1 d . U P A 1
Ag2B Ag 0.9555(5) 0.5150(4) 0.2569(2) 0.0385(10) Uani 0.76(2) 1 d . U P A 2
Ag2C Ag 0.971(3) 0.500(2) 0.2602(14) 0.037(3) Uani 0.11(2) 1 d . U P A 3
Ag3A Ag 0.8693(8) 0.3917(6) 0.3362(10) 0.034(2) Uani 0.41(5) 1 d . U P A 1
Ag3B Ag 0.8618(7) 0.3913(5) 0.3227(6) 0.0395(12) Uani 0.59(5) 1 d . U P A 2
Ag4A Ag 0.351(3) 0.1842(15) 0.2516(12) 0.038(3) Uani 0.11(2) 1 d . U P B 1
Ag4B Ag 0.3736(3) 0.1714(2) 0.24258(14) 0.0298(8) Uani 0.89(2) 1 d . U P B 2
Ag5 Ag 0.84131(7) 0.54210(5) 0.16925(4) 0.0350(2) Uani 1 1 d . U . . .
Ag6 Ag 0.41643(8) 0.05588(6) 0.17642(4) 0.0397(2) Uani 1 1 d . U . . .
Ag7 Ag 0.58392(7) 0.11540(5) 0.37437(4) 0.0391(2) Uani 1 1 d . U . . .
Ag8 Ag 0.62877(7) -0.00432(5) 0.30938(4) 0.0356(2) Uani 1 1 d . U . . .
Ag9 Ag 0.50768(7) 0.25464(6) 0.32851(4) 0.0426(3) Uani 1 1 d . U . . .
Ag10 Ag 0.79297(7) 0.06545(5) 0.25236(4) 0.0341(2) Uani 1 1 d . U . . .
Ag11 Ag 0.63615(7) 0.00129(5) 0.18037(4) 0.0377(2) Uani 1 1 d . U . . .
Ag12 Ag 0.78994(8) 0.18981(6) 0.17487(5) 0.0459(3) Uani 1 1 d . U . . .
Ag13 Ag 0.46468(7) -0.06726(6) 0.23977(4) 0.0420(3) Uani 1 1 d . U . . .
Ag14 Ag 0.86488(7) 0.38572(5) 0.19808(3) 0.0310(2) Uani 1 1 d . U . . .
Ag15 Ag 0.5150(5) 0.2556(4) 0.1627(4) 0.0416(13) Uani 0.85(4) 1 d . U P B 1
A15 Ag 0.496(3) 0.2630(12) 0.1739(11) 0.037(3) Uani 0.15(4) 1 d . U P B 2
Ag16 Ag 0.66570(7) 0.43758(5) 0.31964(4) 0.0357(2) Uani 1 1 d . U . . .
Ag17 Ag 0.72445(8) 0.56337(5) 0.25476(4) 0.0375(2) Uani 1 1 d . U . . .
Ag18 Ag 0.66359(7) 0.43121(5) 0.18982(4) 0.0340(2) Uani 1 1 d . U . . .
Ag19 Ag 0.78646(7) 0.18789(5) 0.33261(4) 0.0392(2) Uani 1 1 d . U . . .
Ag20 Ag 0.59209(8) 0.12042(6) 0.11526(4) 0.0449(3) Uani 1 1 d . U . . .
Ag21 Ag 0.41049(7) 0.04984(5) 0.30585(4) 0.0366(2) Uani 1 1 d . U . . .
Ag22 Ag 0.84513(7) 0.54816(5) 0.35075(4) 0.0360(2) Uani 1 1 d . U . . .
C1 C 0.5188(10) 0.0102(8) 0.1182(5) 0.044(2) Uani 1 1 d . U . . .
C2 C 0.4618(10) -0.0453(8) 0.1056(5) 0.045(3) Uani 1 1 d . U . . .
C3 C 0.3989(15) -0.1110(9) 0.0818(7) 0.075(5) Uani 1 1 d . U . . .
C4 C 0.4097(18) -0.1106(13) 0.0251(8) 0.102(7) Uani 1 1 d . U . . .
H4A H 0.3672 -0.1550 0.0094 0.153 Uiso 1 1 calc R U . . .
H4B H 0.3921 -0.0646 0.0113 0.153 Uiso 1 1 calc R U . . .
H4C H 0.4769 -0.1121 0.0179 0.153 Uiso 1 1 calc R U . . .
C5 C 0.2943(16) -0.1063(16) 0.0900(11) 0.128(8) Uani 1 1 d . U . . .
H5A H 0.2518 -0.1505 0.0741 0.192 Uiso 1 1 calc R U . . .
H5B H 0.2840 -0.1053 0.1263 0.192 Uiso 1 1 calc R U . . .
H5C H 0.2795 -0.0602 0.0749 0.192 Uiso 1 1 calc R U . . .
C6 C 0.420(3) -0.1807(12) 0.1077(13) 0.170(13) Uani 1 1 d . U . . .
H6A H 0.3785 -0.2257 0.0923 0.256 Uiso 1 1 calc R U . . .
H6B H 0.4879 -0.1842 0.1040 0.256 Uiso 1 1 calc R U . . .
H6C H 0.4077 -0.1775 0.1437 0.256 Uiso 1 1 calc R U . . .
C7 C 0.3733(10) 0.1754(8) 0.1638(5) 0.041(2) Uani 1 1 d . U . . .
C8 C 0.3579(11) 0.1904(9) 0.1201(6) 0.051(3) Uani 1 1 d . U . . .
C9 C 0.3204(14) 0.2089(13) 0.0714(7) 0.078(5) Uani 1 1 d . U . . .
C10 C 0.320(3) 0.2927(19) 0.0690(11) 0.183(13) Uani 1 1 d . U . . .
H10A H 0.2941 0.3043 0.0357 0.275 Uiso 1 1 calc R U . . .
H10B H 0.2792 0.3070 0.0951 0.275 Uiso 1 1 calc R U . . .
H10C H 0.3859 0.3211 0.0747 0.275 Uiso 1 1 calc R U . . .
C11 C 0.395(3) 0.198(3) 0.0339(10) 0.195(14) Uani 1 1 d . U . . .
H11A H 0.3722 0.2095 0.0000 0.293 Uiso 1 1 calc R U . . .
H11B H 0.4562 0.2310 0.0432 0.293 Uiso 1 1 calc R U . . .
H11C H 0.4034 0.1449 0.0343 0.293 Uiso 1 1 calc R U . . .
C12 C 0.227(2) 0.162(3) 0.0594(11) 0.220(17) Uani 1 1 d . U . . .
H12A H 0.2021 0.1747 0.0262 0.331 Uiso 1 1 calc R U . . .
H12B H 0.2332 0.1084 0.0589 0.331 Uiso 1 1 calc R U . . .
H12C H 0.1817 0.1698 0.0851 0.331 Uiso 1 1 calc R U . . .
C13 C 0.6906(10) 0.5563(7) 0.1751(5) 0.035(2) Uani 1 1 d . U . . .
C14 C 0.6324(11) 0.5664(8) 0.1433(5) 0.045(3) Uani 1 1 d . U . . .
C15 C 0.5629(15) 0.5813(12) 0.1022(7) 0.077(4) Uani 1 1 d . U . . .
C16 C 0.4953(16) 0.5048(14) 0.0867(9) 0.099(6) Uani 1 1 d . U . . .
H16A H 0.4599 0.4844 0.1160 0.149 Uiso 1 1 calc R U . . .
H16B H 0.4494 0.5132 0.0595 0.149 Uiso 1 1 calc R U . . .
H16C H 0.5342 0.4688 0.0750 0.149 Uiso 1 1 calc R U . . .
C17 C 0.4998(18) 0.6320(14) 0.1238(11) 0.122(8) Uani 1 1 d . U . . .
H17A H 0.4656 0.6071 0.1521 0.182 Uiso 1 1 calc R U . . .
H17B H 0.5401 0.6799 0.1356 0.182 Uiso 1 1 calc R U . . .
H17C H 0.4527 0.6419 0.0976 0.182 Uiso 1 1 calc R U . . .
C18 C 0.617(2) 0.614(2) 0.0596(10) 0.171(13) Uani 1 1 d . U . . .
H18A H 0.5720 0.6235 0.0324 0.257 Uiso 1 1 calc R U . . .
H18B H 0.6597 0.6610 0.0704 0.257 Uiso 1 1 calc R U . . .
H18C H 0.6558 0.5779 0.0473 0.257 Uiso 1 1 calc R U . . .
C19 C 0.9698(9) 0.4935(7) 0.3390(5) 0.038(2) Uani 1 1 d . U . . .
C20 C 1.0525(10) 0.5268(8) 0.3400(5) 0.040(3) Uani 1 1 d . U . . .
C21 C 1.1540(10) 0.5647(9) 0.3471(6) 0.054(3) Uani 1 1 d . U . . .
C22 C 1.2043(13) 0.5562(13) 0.2964(8) 0.082(5) Uani 1 1 d . U . . .
H22A H 1.2723 0.5811 0.3001 0.124 Uiso 1 1 calc R U . . .
H22B H 1.2002 0.5025 0.2881 0.124 Uiso 1 1 calc R U . . .
H22C H 1.1719 0.5798 0.2692 0.124 Uiso 1 1 calc R U . . .
C23 C 1.1575(14) 0.6470(11) 0.3583(10) 0.093(6) Uani 1 1 d . U . . .
H23A H 1.2249 0.6729 0.3631 0.139 Uiso 1 1 calc R U . . .
H23B H 1.1264 0.6693 0.3299 0.139 Uiso 1 1 calc R U . . .
H23C H 1.1234 0.6527 0.3891 0.139 Uiso 1 1 calc R U . . .
C24 C 1.2008(15) 0.5253(14) 0.3904(9) 0.095(6) Uani 1 1 d . U . . .
H24A H 1.2687 0.5495 0.3960 0.143 Uiso 1 1 calc R U . . .
H24B H 1.1666 0.5296 0.4214 0.143 Uiso 1 1 calc R U . . .
H24C H 1.1967 0.4718 0.3814 0.143 Uiso 1 1 calc R U . . .
C25 C 0.3674(10) 0.1702(8) 0.3201(5) 0.040(2) Uani 1 1 d . U . . .
C26 C 0.3531(11) 0.1747(8) 0.3649(6) 0.047(3) Uani 1 1 d . U . . .
C27 C 0.3177(14) 0.1851(12) 0.4156(6) 0.072(4) Uani 1 1 d . U . . .
C28 C 0.3913(17) 0.1545(16) 0.4536(8) 0.103(7) Uani 1 1 d . U . . .
H28A H 0.4560 0.1852 0.4512 0.154 Uiso 1 1 calc R U . . .
H28B H 0.3705 0.1577 0.4882 0.154 Uiso 1 1 calc R U . . .
H28C H 0.3929 0.1018 0.4448 0.154 Uiso 1 1 calc R U . . .
C29 C 0.326(2) 0.2657(16) 0.4288(9) 0.133(9) Uani 1 1 d . U . . .
H29A H 0.3926 0.2917 0.4263 0.200 Uiso 1 1 calc R U . . .
H29B H 0.2836 0.2882 0.4054 0.200 Uiso 1 1 calc R U . . .
H29C H 0.3056 0.2709 0.4634 0.200 Uiso 1 1 calc R U . . .
C30 C 0.2200(17) 0.141(2) 0.4181(8) 0.145(11) Uani 1 1 d . U . . .
H30A H 0.2204 0.0878 0.4089 0.217 Uiso 1 1 calc R U . . .
H30B H 0.1981 0.1435 0.4525 0.217 Uiso 1 1 calc R U . . .
H30C H 0.1761 0.1607 0.3945 0.217 Uiso 1 1 calc R U . . .
C31 C 0.5809(9) 0.3593(7) 0.2516(5) 0.0344(19) Uani 1 1 d . U . . .
C32 C 0.5004(10) 0.3812(7) 0.2549(4) 0.033(2) Uani 1 1 d . U . . .
C33 C 0.4171(10) 0.4133(10) 0.2586(6) 0.054(3) Uani 1 1 d . U . . .
C34 C 0.4418(12) 0.5014(9) 0.2493(7) 0.062(4) Uani 1 1 d . U . . .
H34A H 0.3834 0.5229 0.2520 0.093 Uiso 1 1 calc R U . . .
H34B H 0.4910 0.5255 0.2747 0.093 Uiso 1 1 calc R U . . .
H34C H 0.4665 0.5102 0.2155 0.093 Uiso 1 1 calc R U . . .
C35 C 0.3828(16) 0.4039(13) 0.3126(8) 0.087(6) Uani 1 1 d . U . . .
H35A H 0.3249 0.4260 0.3156 0.131 Uiso 1 1 calc R U . . .
H35B H 0.3677 0.3501 0.3203 0.131 Uiso 1 1 calc R U . . .
H35C H 0.4339 0.4297 0.3364 0.131 Uiso 1 1 calc R U . . .
C36 C 0.3425(15) 0.3784(13) 0.2177(9) 0.096(7) Uani 1 1 d . U . . .
H36A H 0.2844 0.4005 0.2200 0.144 Uiso 1 1 calc R U . . .
H36B H 0.3691 0.3885 0.1844 0.144 Uiso 1 1 calc R U . . .
H36C H 0.3259 0.3237 0.2222 0.144 Uiso 1 1 calc R U . . .
C37 C 0.9676(9) 0.4872(7) 0.1755(5) 0.036(2) Uani 1 1 d . U . . .
C38 C 1.0278(11) 0.4850(11) 0.1481(6) 0.058(4) Uani 1 1 d . U . . .
C39 C 1.1016(14) 0.4852(15) 0.1113(8) 0.111(8) Uani 1 1 d D U . . .
C40 C 1.060(2) 0.499(2) 0.0590(8) 0.199(17) Uani 1 1 d D U . . .
H40A H 1.1100 0.4988 0.0343 0.298 Uiso 1 1 calc R U . . .
H40B H 1.0050 0.4584 0.0500 0.298 Uiso 1 1 calc R U . . .
H40C H 1.0393 0.5476 0.0589 0.298 Uiso 1 1 calc R U . . .
C41 C 1.135(3) 0.4098(18) 0.1112(18) 0.26(2) Uiso 1 1 d D U . . .
H41A H 1.1842 0.4102 0.0865 0.388 Uiso 1 1 calc R U . . .
H41B H 1.1616 0.4011 0.1449 0.388 Uiso 1 1 calc R U . . .
H41C H 1.0795 0.3693 0.1023 0.388 Uiso 1 1 calc R U . . .
C42 C 1.185(3) 0.5488(19) 0.1265(18) 0.25(2) Uiso 1 1 d D U . . .
H42A H 1.2360 0.5504 0.1024 0.382 Uiso 1 1 calc R U . . .
H42B H 1.1624 0.5970 0.1264 0.382 Uiso 1 1 calc R U . . .
H42C H 1.2107 0.5400 0.1604 0.382 Uiso 1 1 calc R U . . .
C43 C 0.5089(10) 0.0034(8) 0.3659(5) 0.043(2) Uani 1 1 d . U . . .
C44 C 0.4586(9) -0.0552(8) 0.3757(6) 0.046(3) Uani 1 1 d . U . . .
C45 C 0.3976(17) -0.1190(13) 0.3951(12) 0.118(7) Uani 1 1 d . U . . .
C46 C 0.401(3) -0.1847(16) 0.3528(19) 0.231(16) Uani 1 1 d . U . . .
H46A H 0.4681 -0.1893 0.3483 0.346 Uiso 1 1 calc R U . . .
H46B H 0.3646 -0.2329 0.3639 0.346 Uiso 1 1 calc R U . . .
H46C H 0.3721 -0.1714 0.3206 0.346 Uiso 1 1 calc R U . . .
C47 C 0.300(2) -0.113(2) 0.4014(19) 0.230(17) Uani 1 1 d . U . . .
H47A H 0.2653 -0.1596 0.4150 0.346 Uiso 1 1 calc R U . . .
H47B H 0.2982 -0.0706 0.4250 0.346 Uiso 1 1 calc R U . . .
H47C H 0.2701 -0.1031 0.3687 0.346 Uiso 1 1 calc R U . . .
C48 C 0.441(2) -0.150(2) 0.4378(16) 0.239(18) Uani 1 1 d . U . . .
H48A H 0.5080 -0.1531 0.4310 0.359 Uiso 1 1 calc R U . . .
H48B H 0.4401 -0.1180 0.4677 0.359 Uiso 1 1 calc R U . . .
H48C H 0.4048 -0.2010 0.4437 0.359 Uiso 1 1 calc R U . . .
C49 C 0.8495(9) 0.2919(7) 0.2593(5) 0.0354(19) Uani 1 1 d . U . . .
C50 C 0.9311(8) 0.2674(8) 0.2625(5) 0.038(2) Uani 1 1 d . U . . .
C51 C 1.0312(11) 0.2604(10) 0.2698(7) 0.062(4) Uani 1 1 d . U . . .
C52 C 1.0940(14) 0.3277(15) 0.2896(15) 0.160(12) Uani 1 1 d . U . . .
H52A H 1.1601 0.3186 0.2935 0.240 Uiso 1 1 calc R U . . .
H52B H 1.0920 0.3691 0.2662 0.240 Uiso 1 1 calc R U . . .
H52C H 1.0725 0.3414 0.3225 0.240 Uiso 1 1 calc R U . . .
C53 C 1.0588(18) 0.2490(19) 0.2179(10) 0.131(9) Uani 1 1 d . U . . .
H53A H 1.0177 0.2035 0.2029 0.197 Uiso 1 1 calc R U . . .
H53B H 1.0508 0.2928 0.1979 0.197 Uiso 1 1 calc R U . . .
H53C H 1.1265 0.2431 0.2184 0.197 Uiso 1 1 calc R U . . .
C59 C 1.0332(16) 0.1888(16) 0.2971(13) 0.138(11) Uani 1 1 d . U . . .
H59A H 0.9876 0.1474 0.2801 0.207 Uiso 1 1 calc R U . . .
H59B H 1.0984 0.1775 0.2972 0.207 Uiso 1 1 calc R U . . .
H59C H 1.0149 0.1946 0.3320 0.207 Uiso 1 1 calc R U . . .
C61 C 0.3326(10) -0.0312(8) 0.2356(5) 0.043(2) Uani 1 1 d . U . . .
C62 C 0.2498(10) -0.0204(9) 0.2344(6) 0.051(3) Uani 1 1 d . U . . .
C63 C 0.1495(11) -0.0162(9) 0.2316(8) 0.065(4) Uani 1 1 d . U . . .
C64 C 0.0878(17) -0.0864(16) 0.2055(13) 0.136(10) Uani 1 1 d . U . . .
H64A H 0.0198 -0.0814 0.2043 0.204 Uiso 1 1 calc R U . . .
H64B H 0.1085 -0.0912 0.1710 0.204 Uiso 1 1 calc R U . . .
H64C H 0.0956 -0.1314 0.2244 0.204 Uiso 1 1 calc R U . . .
C65 C 0.1364(17) 0.0492(16) 0.1976(12) 0.126(9) Uani 1 1 d . U . . .
H65A H 0.0681 0.0532 0.1952 0.189 Uiso 1 1 calc R U . . .
H65B H 0.1746 0.0964 0.2120 0.189 Uiso 1 1 calc R U . . .
H65C H 0.1580 0.0400 0.1639 0.189 Uiso 1 1 calc R U . . .
C66 C 0.1150(19) -0.0053(18) 0.2848(10) 0.126(9) Uani 1 1 d . U . . .
H66A H 0.0463 -0.0025 0.2826 0.189 Uiso 1 1 calc R U . . .
H66B H 0.1246 -0.0481 0.3056 0.189 Uiso 1 1 calc R U . . .
H66C H 0.1521 0.0416 0.3001 0.189 Uiso 1 1 calc R U . . .
C67 C 0.6026(11) -0.0956(7) 0.2421(6) 0.047(2) Uani 1 1 d . U . . .
C68 C 0.6701(11) -0.1267(8) 0.2373(6) 0.048(3) Uani 1 1 d . U . . .
C69 C 0.7366(14) -0.1748(10) 0.2317(9) 0.107(6) Uani 1 1 d D U . . .
C70 C 0.8365(14) -0.1329(13) 0.2481(14) 0.195(15) Uani 1 1 d D U . . .
H70A H 0.8832 -0.1664 0.2442 0.292 Uiso 1 1 calc R U . . .
H70B H 0.8538 -0.0886 0.2271 0.292 Uiso 1 1 calc R U . . .
H70C H 0.8373 -0.1167 0.2836 0.292 Uiso 1 1 calc R U . . .
C71 C 0.738(3) -0.199(2) 0.1763(11) 0.240(16) Uani 1 1 d D U . . .
H71A H 0.7846 -0.2324 0.1727 0.360 Uiso 1 1 calc R U . . .
H71B H 0.6736 -0.2255 0.1646 0.360 Uiso 1 1 calc R U . . .
H71C H 0.7567 -0.1539 0.1559 0.360 Uiso 1 1 calc R U . . .
C72 C 0.712(2) -0.2446(13) 0.2623(14) 0.209(15) Uani 1 1 d D U . . .
H72A H 0.7601 -0.2767 0.2574 0.314 Uiso 1 1 calc R U . . .
H72B H 0.7127 -0.2303 0.2981 0.314 Uiso 1 1 calc R U . . .
H72C H 0.6480 -0.2724 0.2513 0.314 Uiso 1 1 calc R U . . .
C73 C 0.7908(10) 0.0637(7) 0.3314(5) 0.040(2) Uani 1 1 d . U . . .
C74 C 0.8093(10) 0.0622(8) 0.3753(5) 0.043(3) Uani 1 1 d . U . . .
C75 C 0.8456(13) 0.0513(10) 0.4266(6) 0.072(4) Uani 1 1 d D U . . .
C76 C 0.833(3) 0.1193(19) 0.4595(12) 0.101(11) Uani 0.55(3) 1 d D U P C 1
H76A H 0.8569 0.1131 0.4942 0.151 Uiso 0.55(3) 1 calc R U P C 1
H76B H 0.8694 0.1658 0.4459 0.151 Uiso 0.55(3) 1 calc R U P C 1
H76C H 0.7643 0.1224 0.4594 0.151 Uiso 0.55(3) 1 calc R U P C 1
C77 C 0.783(3) -0.0223(18) 0.4436(18) 0.131(15) Uani 0.55(3) 1 d D U P C 1
H77A H 0.8034 -0.0332 0.4781 0.197 Uiso 0.55(3) 1 calc R U P C 1
H77B H 0.7150 -0.0166 0.4428 0.197 Uiso 0.55(3) 1 calc R U P C 1
H77C H 0.7899 -0.0639 0.4208 0.197 Uiso 0.55(3) 1 calc R U P C 1
C78 C 0.9530(19) 0.044(3) 0.4271(15) 0.110(12) Uani 0.55(3) 1 d D U P C 1
H78A H 0.9760 0.0365 0.4618 0.165 Uiso 0.55(3) 1 calc R U P C 1
H78B H 0.9597 0.0002 0.4060 0.165 Uiso 0.55(3) 1 calc R U P C 1
H78C H 0.9913 0.0897 0.4140 0.165 Uiso 0.55(3) 1 calc R U P C 1
C76A C 0.926(4) 0.118(3) 0.4427(19) 0.110(14) Uani 0.45(3) 1 d . U P C 2
H76D H 0.9506 0.1103 0.4772 0.164 Uiso 0.45(3) 1 calc R U P C 2
H76E H 0.9792 0.1208 0.4196 0.164 Uiso 0.45(3) 1 calc R U P C 2
H76F H 0.9011 0.1649 0.4417 0.164 Uiso 0.45(3) 1 calc R U P C 2
C77A C 0.860(5) -0.029(3) 0.437(2) 0.111(13) Uani 0.45(3) 1 d . U P C 2
H77D H 0.8847 -0.0316 0.4716 0.167 Uiso 0.45(3) 1 calc R U P C 2
H77E H 0.7987 -0.0637 0.4311 0.167 Uiso 0.45(3) 1 calc R U P C 2
H77F H 0.9072 -0.0419 0.4135 0.167 Uiso 0.45(3) 1 calc R U P C 2
C78A C 0.756(5) 0.054(3) 0.4647(19) 0.108(13) Uani 0.45(3) 1 d . U P C 2
H78D H 0.7780 0.0464 0.4996 0.163 Uiso 0.45(3) 1 calc R U P C 2
H78E H 0.7355 0.1025 0.4622 0.163 Uiso 0.45(3) 1 calc R U P C 2
H78F H 0.7014 0.0131 0.4547 0.163 Uiso 0.45(3) 1 calc R U P C 2
C79 C 0.6936(10) 0.5619(7) 0.3327(5) 0.035(2) Uani 1 1 d . U . . .
C80 C 0.6505(11) 0.5878(8) 0.3633(6) 0.047(3) Uani 1 1 d . U . . .
C81 C 0.5966(14) 0.6244(12) 0.4002(7) 0.073(4) Uani 1 1 d . U . . .
C82 C 0.592(2) 0.5748(19) 0.4485(9) 0.140(10) Uani 1 1 d . U . . .
H82A H 0.5564 0.5239 0.4401 0.210 Uiso 1 1 calc R U . . .
H82B H 0.5597 0.5977 0.4749 0.210 Uiso 1 1 calc R U . . .
H82C H 0.6580 0.5719 0.4608 0.210 Uiso 1 1 calc R U . . .
C83 C 0.6558(19) 0.7041(14) 0.4147(10) 0.121(8) Uani 1 1 d . U . . .
H83A H 0.6666 0.7340 0.3842 0.181 Uiso 1 1 calc R U . . .
H83B H 0.7182 0.6991 0.4308 0.181 Uiso 1 1 calc R U . . .
H83C H 0.6201 0.7294 0.4383 0.181 Uiso 1 1 calc R U . . .
C84 C 0.4987(15) 0.6292(14) 0.3781(8) 0.095(7) Uani 1 1 d . U . . .
H84A H 0.5045 0.6484 0.3437 0.142 Uiso 1 1 calc R U . . .
H84B H 0.4697 0.6634 0.3990 0.142 Uiso 1 1 calc R U . . .
H84C H 0.4578 0.5788 0.3770 0.142 Uiso 1 1 calc R U . . .
C85 C 0.8027(10) 0.0667(8) 0.1748(5) 0.043(2) Uani 1 1 d . U . . .
C86 C 0.8301(13) 0.0676(9) 0.1317(6) 0.060(3) Uani 1 1 d . U . . .
C87 C 0.8708(14) 0.0622(12) 0.0833(7) 0.091(6) Uani 1 1 d D U . . .
C88 C 0.927(3) 0.1402(15) 0.0706(14) 0.250(18) Uani 1 1 d D U . . .
H88A H 0.9552 0.1376 0.0377 0.376 Uiso 1 1 calc R U . . .
H88B H 0.8832 0.1765 0.0694 0.376 Uiso 1 1 calc R U . . .
H88C H 0.9786 0.1566 0.0966 0.376 Uiso 1 1 calc R U . . .
C89 C 0.937(2) 0.0065(17) 0.0819(11) 0.177(13) Uani 1 1 d D U . . .
H89A H 0.9626 0.0054 0.0481 0.265 Uiso 1 1 calc R U . . .
H89B H 0.9909 0.0216 0.1069 0.265 Uiso 1 1 calc R U . . .
H89C H 0.9018 -0.0438 0.0896 0.265 Uiso 1 1 calc R U . . .
C90 C 0.787(2) 0.041(2) 0.0459(10) 0.254(18) Uani 1 1 d D U . . .
H90A H 0.8114 0.0368 0.0121 0.381 Uiso 1 1 calc R U . . .
H90B H 0.7485 -0.0073 0.0549 0.381 Uiso 1 1 calc R U . . .
H90C H 0.7475 0.0802 0.0462 0.381 Uiso 1 1 calc R U . . .
C91 C 0.7206(10) 0.3465(8) 0.4611(5) 0.043(3) Uani 1 1 d . U . . .
C92 C 0.7860(15) 0.3053(10) 0.4940(6) 0.070(5) Uani 1 1 d . U . . .
H92A H 0.7530 0.2532 0.4989 0.105 Uiso 1 1 calc R U . . .
H92B H 0.8463 0.3048 0.4772 0.105 Uiso 1 1 calc R U . . .
H92C H 0.8005 0.3315 0.5269 0.105 Uiso 1 1 calc R U . . .
C93 C 0.6278(13) 0.3494(10) 0.4883(6) 0.065(4) Uani 1 1 d . U . . .
H93A H 0.5931 0.2978 0.4934 0.097 Uiso 1 1 calc R U . . .
H93B H 0.6442 0.3753 0.5212 0.097 Uiso 1 1 calc R U . . .
H93C H 0.5868 0.3769 0.4679 0.097 Uiso 1 1 calc R U . . .
C94 C 0.7726(13) 0.4268(8) 0.4539(5) 0.055(4) Uani 1 1 d . U . . .
H94A H 0.8322 0.4260 0.4365 0.082 Uiso 1 1 calc R U . . .
H94B H 0.7310 0.4539 0.4336 0.082 Uiso 1 1 calc R U . . .
H94C H 0.7884 0.4523 0.4869 0.082 Uiso 1 1 calc R U . . .
C95 C 0.7392(11) 0.3547(8) 0.0462(5) 0.046(3) Uani 1 1 d . U . . .
C96 C 0.7804(13) 0.4357(8) 0.0605(5) 0.057(4) Uani 1 1 d . U . . .
H96A H 0.8383 0.4380 0.0827 0.086 Uiso 1 1 calc R U . . .
H96B H 0.7973 0.4642 0.0300 0.086 Uiso 1 1 calc R U . . .
H96C H 0.7323 0.4576 0.0782 0.086 Uiso 1 1 calc R U . . .
C97 C 0.8149(14) 0.3175(10) 0.0191(7) 0.066(4) Uani 1 1 d . U . . .
H97A H 0.7867 0.2648 0.0101 0.099 Uiso 1 1 calc R U . . .
H97B H 0.8335 0.3451 -0.0116 0.099 Uiso 1 1 calc R U . . .
H97C H 0.8721 0.3191 0.0418 0.099 Uiso 1 1 calc R U . . .
C98 C 0.6486(14) 0.3537(10) 0.0113(6) 0.064(4) Uani 1 1 d . U . . .
H98A H 0.6202 0.3015 0.0014 0.095 Uiso 1 1 calc R U . . .
H98B H 0.6014 0.3763 0.0294 0.095 Uiso 1 1 calc R U . . .
H98C H 0.6664 0.3829 -0.0189 0.095 Uiso 1 1 calc R U . . .
C99 C 0.9504(14) 0.7273(9) 0.3872(7) 0.067(4) Uani 1 1 d . U . . .
C100 C 0.9096(13) 0.6500(10) 0.4589(6) 0.063(4) Uani 1 1 d . U . . .
C101 C 0.9539(13) 0.7173(11) 0.4397(7) 0.071(4) Uani 1 1 d . U . . .
H101 H 0.9867 0.7567 0.4618 0.085 Uiso 1 1 calc R U . . .
C102 C 0.9139(11) 0.6433(9) 0.5179(6) 0.081(4) Uani 1 1 d D U . . .
C103 C 0.9992(15) 0.8052(11) 0.3743(7) 0.110(6) Uani 1 1 d D U . . .
C104 C 0.9455(19) 0.6945(12) 0.1243(9) 0.096(6) Uani 1 1 d D U . . .
C105 C 0.9639(14) 0.7457(10) 0.0808(8) 0.109(6) Uani 1 1 d D U . . .
O1 O 0.6291(7) 0.3384(5) 0.1275(3) 0.0420(17) Uani 1 1 d . U . . .
O2 O 0.7924(7) 0.3007(5) 0.1355(3) 0.0407(17) Uani 1 1 d . U . . .
O3 O 0.6584(8) 0.2222(5) 0.0829(4) 0.049(2) Uani 1 1 d . U . . .
O4 O 0.7823(7) 0.2972(5) 0.3747(3) 0.0403(17) Uani 1 1 d . U . . .
O5 O 0.6198(6) 0.3387(5) 0.3715(3) 0.0403(17) Uani 1 1 d . U . . .
O6 O 0.6406(7) 0.2182(5) 0.4141(3) 0.047(2) Uani 1 1 d . U . . .
O7 O 0.5586(6) 0.0872(5) 0.2449(3) 0.0335(19) Uani 1 1 d . U . . .
O8 O 0.6260(6) 0.1907(5) 0.2899(3) 0.0337(15) Uani 1 1 d . U . . .
O9 O 0.6298(6) 0.1911(5) 0.2068(3) 0.0334(15) Uani 1 1 d . U . . .
O10 O 0.8696(10) 0.5920(7) 0.4387(4) 0.081(4) Uani 1 1 d . U . . .
O11 O 0.9213(9) 0.6883(6) 0.3523(4) 0.067(3) Uani 1 1 d . U . . .
O12 O 0.960(2) 0.7127(13) 0.1664(8) 0.160(8) Uani 1 1 d D U . . .
O13 O 0.8905(11) 0.6351(10) 0.1126(6) 0.111(5) Uani 1 1 d . U . . .
N1 N 0.6056(8) 0.1551(6) 0.2473(4) 0.038(2) Uani 1 1 d . U . . .
F1 F 0.8229(9) 0.6227(8) 0.5337(5) 0.111(4) Uani 1 1 d D U . . .
F2 F 0.9627(9) 0.5900(8) 0.5340(5) 0.116(4) Uani 1 1 d D U . . .
F3 F 0.9520(12) 0.7078(8) 0.5433(5) 0.153(6) Uani 1 1 d D U . . .
F4 F 1.0534(14) 0.8500(9) 0.4071(6) 0.182(8) Uani 1 1 d D U . . .
F5 F 0.9362(14) 0.8482(9) 0.3580(8) 0.194(8) Uani 1 1 d D U . . .
F6 F 1.0529(15) 0.8064(9) 0.3338(7) 0.179(8) Uani 1 1 d D U . . .
F7 F 0.934(3) 0.8113(15) 0.0883(17) 0.160(14) Uani 0.48(3) 1 d D U P D 1
F8 F 1.0638(17) 0.763(2) 0.0791(17) 0.160(13) Uani 0.48(3) 1 d D U P D 1
F9 F 0.929(4) 0.715(3) 0.0358(10) 0.166(14) Uani 0.48(3) 1 d D U P D 1
F7B F 1.020(3) 0.8113(18) 0.0936(16) 0.180(16) Uani 0.52(3) 1 d D U P D 2
F8B F 0.998(3) 0.721(2) 0.0386(12) 0.144(12) Uani 0.52(3) 1 d D U P D 2
F9B F 0.879(2) 0.765(2) 0.0639(13) 0.141(12) Uani 0.52(3) 1 d D U P D 2
P1 P 0.7025(3) 0.30006(19) 0.10143(12) 0.0359(7) Uani 1 1 d . U . . .
P2 P 0.6895(3) 0.29675(18) 0.40180(12) 0.0357(7) Uani 1 1 d . U . . .
O1W O 0.9076(17) 0.6483(10) 0.2546(6) 0.060(7) Uiso 0.66(4) 1 d . U P E 1
O1WA O 0.971(3) 0.6533(19) 0.2541(12) 0.061(13) Uiso 0.34(4) 1 d D U P A 2
N2 N 1.216(3) 0.753(2) 0.2174(16) 0.174(16) Uiso 0.78(2) 1 d D U P F 1
C107 C 1.280(3) 0.720(2) 0.2195(16) 0.134(14) Uiso 0.78(2) 1 d D U P F 1
C106 C 1.369(3) 0.694(2) 0.2289(16) 0.131(13) Uiso 0.78(2) 1 d D U P F 1
N3 N 1.105(7) 0.681(9) 0.121(2) 0.20(5) Uiso 0.22(2) 1 d D U P F 2
C108 C 1.102(5) 0.673(4) 0.1652(17) 0.048(17) Uiso 0.22(2) 1 d D U P F 2
C109 C 1.087(3) 0.658(3) 0.2173(16) 0.030(13) Uiso 0.22(2) 1 d D U P F 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C31 2.101(13) . ?
Ag1 C49 2.122(13) . ?
Ag1 O8 2.466(8) . ?
Ag1 O9 2.538(8) . ?
Ag1 Ag14 2.8946(12) . ?
Ag1 Ag3B 2.915(13) . ?
Ag1 Ag18 2.9169(12) . ?
Ag1 Ag16 2.9753(12) . ?
Ag1 Ag3A 3.20(2) . ?
Ag1 Ag19 3.3634(13) . ?
Ag2A C37 1.89(3) . ?
Ag2A C19 2.59(3) . ?
Ag2A C20 2.67(3) . ?
Ag2A Ag5 2.855(16) . ?
Ag2A Ag14 2.918(16) . ?
Ag2B C19 2.221(15) . ?
Ag2B C37 2.231(14) . ?
Ag2B O1WA 2.46(3) . ?
Ag2B C20 2.523(14) . ?
Ag2B Ag14 2.847(5) . ?
Ag2B Ag5 2.867(6) . ?
Ag2B Ag3B 2.995(14) . ?
Ag2B Ag22 3.103(7) . ?
Ag2C C19 2.09(4) . ?
Ag2C C37 2.25(4) . ?
Ag2C C20 2.36(4) . ?
Ag2C Ag14 2.78(3) . ?
Ag2C Ag5 3.15(4) . ?
Ag2C Ag22 3.26(4) . ?
Ag3A C19 2.098(17) . ?
Ag3A O4 2.199(17) . ?
Ag3A C49 2.67(3) . ?
Ag3A Ag22 2.924(12) . ?
Ag3A Ag16 3.149(13) . ?
Ag3B C19 2.185(15) . ?
Ag3B O4 2.352(14) . ?
Ag3B C49 2.416(17) . ?
Ag3B Ag22 2.967(9) . ?
Ag3B Ag16 3.035(11) . ?
Ag3B Ag14 3.305(15) . ?
Ag4A C25 1.85(3) . ?
Ag4A C7 2.37(4) . ?
Ag4A Ag9 3.02(2) . ?
Ag4A Ag21 3.06(3) . ?
Ag4A Ag6 3.32(5) . ?
Ag4B C25 2.060(14) . ?
Ag4B C7 2.091(14) . ?
Ag4B Ag6 2.871(7) . ?
Ag4B Ag21 2.886(3) . ?
Ag4B A15 2.89(4) . ?
Ag4B Ag9 3.078(3) . ?
Ag5 C37 2.196(13) . ?
Ag5 C13 2.202(14) . ?
Ag5 O13 2.297(12) . ?
Ag5 Ag17 2.9258(14) . ?
Ag5 Ag18 2.9784(13) . ?
Ag5 Ag14 3.0034(13) . ?
Ag6 C7 2.370(14) . ?
Ag6 C1 2.399(14) . ?
Ag6 C61 2.422(14) . ?
Ag6 Ag13 2.9609(15) . ?
Ag6 Ag20 3.0781(16) . ?
Ag7 C43 2.100(14) . ?
Ag7 O6 2.120(9) . ?
Ag7 Ag8 2.9208(14) . ?
Ag7 Ag21 3.0241(14) . ?
Ag7 Ag9 3.1468(15) . ?
Ag7 Ag19 3.1695(15) . ?
Ag8 C43 2.332(14) . ?
Ag8 C67 2.378(14) . ?
Ag8 C73 2.426(13) . ?
Ag8 Ag10 2.9198(14) . ?
Ag8 Ag13 2.9377(14) . ?
Ag9 O5 2.233(9) . ?
Ag9 C25 2.261(14) . ?
Ag9 O8 2.450(9) . ?
Ag9 C26 2.612(14) . ?
Ag10 C85 2.068(14) . ?
Ag10 C73 2.097(14) . ?
Ag10 Ag11 2.9118(13) . ?
Ag10 Ag19 3.0602(13) . ?
Ag10 Ag12 3.0650(14) . ?
Ag11 C1 2.311(15) . ?
Ag11 C67 2.405(15) . ?
Ag11 C85 2.437(14) . ?
Ag11 Ag20 2.9108(14) . ?
Ag11 Ag13 3.0253(15) . ?
Ag12 C85 2.259(13) . ?
Ag12 O2 2.262(9) . ?
Ag12 O9 2.454(8) . ?
Ag12 C86 2.634(15) . ?
Ag12 Ag20 3.1784(16) . ?
Ag13 C61 2.085(15) . ?
Ag13 C67 2.102(15) . ?
Ag13 Ag21 2.9546(14) . ?
Ag14 C37 2.220(12) . ?
Ag14 O2 2.311(9) . ?
Ag14 C49 2.346(13) . ?
Ag14 Ag18 3.1004(14) . ?
Ag15 O1 2.230(11) . ?
Ag15 C7 2.241(14) . ?
Ag15 O9 2.431(10) . ?
Ag15 C8 2.517(15) . ?
Ag15 Ag20 3.119(13) . ?
A15 C7 2.12(4) . ?
A15 O1 2.49(4) . ?
A15 C8 2.51(3) . ?
Ag16 C79 2.220(12) . ?
Ag16 O5 2.281(9) . ?
Ag16 C31 2.404(13) . ?
Ag16 Ag17 2.8843(14) . ?
Ag16 Ag22 2.9915(13) . ?
Ag17 C79 2.130(13) . ?
Ag17 C13 2.141(13) . ?
Ag17 Ag18 2.8919(13) . ?
Ag17 Ag22 3.0410(14) . ?
Ag18 C13 2.258(12) . ?
Ag18 O1 2.304(9) . ?
Ag18 C31 2.322(12) . ?
Ag19 C73 2.250(13) . ?
Ag19 O4 2.262(9) . ?
Ag19 O8 2.495(8) . ?
Ag19 C74 2.612(13) . ?
Ag20 C1 2.066(14) . ?
Ag20 O3 2.109(9) . ?
Ag21 C43 2.330(14) . ?
Ag21 C25 2.390(14) . ?
Ag21 C61 2.438(14) . ?
Ag22 C19 2.203(14) . ?
Ag22 C79 2.231(13) . ?
Ag22 O10 2.438(11) . ?
Ag22 O11 2.553(11) . ?
C1 C2 1.194(19) . ?
C2 C3 1.46(2) . ?
C3 C6 1.51(3) . ?
C3 C4 1.52(3) . ?
C3 C5 1.52(3) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.211(19) . ?
C8 C9 1.44(2) . ?
C9 C12 1.45(3) . ?
C9 C10 1.51(4) . ?
C9 C11 1.52(3) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.189(18) . ?
C14 C15 1.49(2) . ?
C15 C18 1.46(3) . ?
C15 C17 1.52(3) . ?
C15 C16 1.56(3) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.208(18) . ?
C20 C21 1.470(19) . ?
C21 C23 1.50(2) . ?
C21 C24 1.54(3) . ?
C21 C22 1.57(2) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.217(19) . ?
C26 C27 1.48(2) . ?
C27 C30 1.47(3) . ?
C27 C29 1.47(3) . ?
C27 C28 1.59(3) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.277(18) . ?
C32 C33 1.41(2) . ?
C33 C36 1.52(2) . ?
C33 C35 1.53(2) . ?
C33 C34 1.59(2) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.148(19) . ?
C38 C39 1.46(2) . ?
C39 C42 1.517(19) . ?
C39 C41 1.517(19) . ?
C39 C40 1.521(18) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.197(19) . ?
C44 C45 1.42(2) . ?
C45 C47 1.42(4) . ?
C45 C48 1.43(4) . ?
C45 C46 1.63(5) . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.308(18) . ?
C50 C51 1.446(19) . ?
C51 C52 1.44(3) . ?
C51 C53 1.47(3) . ?
C51 C59 1.49(3) . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 H53A 0.9800 . ?
C53 H53B 0.9800 . ?
C53 H53C 0.9800 . ?
C59 H59A 0.9800 . ?
C59 H59B 0.9800 . ?
C59 H59C 0.9800 . ?
C61 C62 1.22(2) . ?
C62 C63 1.43(2) . ?
C63 C65 1.53(3) . ?
C63 C64 1.53(3) . ?
C63 C66 1.53(3) . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C67 C68 1.20(2) . ?
C68 C69 1.40(2) . ?
C69 C72 1.499(18) . ?
C69 C70 1.512(18) . ?
C69 C71 1.528(18) . ?
C70 H70A 0.9800 . ?
C70 H70B 0.9800 . ?
C70 H70C 0.9800 . ?
C71 H71A 0.9800 . ?
C71 H71B 0.9800 . ?
C71 H71C 0.9800 . ?
C72 H72A 0.9800 . ?
C72 H72B 0.9800 . ?
C72 H72C 0.9800 . ?
C73 C74 1.183(19) . ?
C74 C75 1.46(2) . ?
C75 C77A 1.52(5) . ?
C75 C76A 1.53(5) . ?
C75 C76 1.536(19) . ?
C75 C77 1.537(19) . ?
C75 C78 1.547(19) . ?
C75 C78A 1.66(5) . ?
C76 H76A 0.9800 . ?
C76 H76B 0.9800 . ?
C76 H76C 0.9800 . ?
C77 H77A 0.9800 . ?
C77 H77B 0.9800 . ?
C77 H77C 0.9800 . ?
C78 H78A 0.9800 . ?
C78 H78B 0.9800 . ?
C78 H78C 0.9800 . ?
C76A H76D 0.9800 . ?
C76A H76E 0.9800 . ?
C76A H76F 0.9800 . ?
C77A H77D 0.9800 . ?
C77A H77E 0.9800 . ?
C77A H77F 0.9800 . ?
C78A H78D 0.9800 . ?
C78A H78E 0.9800 . ?
C78A H78F 0.9800 . ?
C79 C80 1.178(18) . ?
C80 C81 1.49(2) . ?
C81 C84 1.49(3) . ?
C81 C83 1.55(3) . ?
C81 C82 1.57(3) . ?
C82 H82A 0.9800 . ?
C82 H82B 0.9800 . ?
C82 H82C 0.9800 . ?
C83 H83A 0.9800 . ?
C83 H83B 0.9800 . ?
C83 H83C 0.9800 . ?
C84 H84A 0.9800 . ?
C84 H84B 0.9800 . ?
C84 H84C 0.9800 . ?
C85 C86 1.22(2) . ?
C86 C87 1.44(2) . ?
C87 C90 1.494(18) . ?
C87 C89 1.497(17) . ?
C87 C88 1.530(18) . ?
C88 H88A 0.9800 . ?
C88 H88B 0.9800 . ?
C88 H88C 0.9800 . ?
C89 H89A 0.9800 . ?
C89 H89B 0.9800 . ?
C89 H89C 0.9800 . ?
C90 H90A 0.9800 . ?
C90 H90B 0.9800 . ?
C90 H90C 0.9800 . ?
C91 C94 1.514(19) . ?
C91 C93 1.53(2) . ?
C91 C92 1.54(2) . ?
C91 P2 1.794(14) . ?
C92 H92A 0.9800 . ?
C92 H92B 0.9800 . ?
C92 H92C 0.9800 . ?
C93 H93A 0.9800 . ?
C93 H93B 0.9800 . ?
C93 H93C 0.9800 . ?
C94 H94A 0.9800 . ?
C94 H94B 0.9800 . ?
C94 H94C 0.9800 . ?
C95 C96 1.503(19) . ?
C95 C98 1.54(2) . ?
C95 C97 1.56(2) . ?
C95 P1 1.817(14) . ?
C96 H96A 0.9800 . ?
C96 H96B 0.9800 . ?
C96 H96C 0.9800 . ?
C97 H97A 0.9800 . ?
C97 H97B 0.9800 . ?
C97 H97C 0.9800 . ?
C98 H98A 0.9800 . ?
C98 H98B 0.9800 . ?
C98 H98C 0.9800 . ?
C99 O11 1.165(19) . ?
C99 C101 1.41(3) . ?
C99 C103 1.50(3) . ?
C100 O10 1.198(19) . ?
C100 C101 1.37(3) . ?
C100 C102 1.57(2) . ?
C101 H101 0.9500 . ?
C102 F3 1.345(15) . ?
C102 F2 1.346(16) . ?
C102 F1 1.356(15) . ?
C103 F4 1.298(16) . ?
C103 F6 1.341(17) . ?
C103 F5 1.343(17) . ?
C104 O12 1.16(3) . ?
C104 O13 1.23(3) . ?
C104 C105 1.49(3) . ?
C105 F7B 1.327(18) . ?
C105 F8B 1.340(19) . ?
C105 F9 1.341(19) . ?
C105 F7 1.343(18) . ?
C105 F9B 1.368(18) . ?
C105 F8 1.390(18) . ?
O1 P1 1.533(10) . ?
O2 P1 1.521(10) . ?
O3 P1 1.492(10) . ?
O4 P2 1.521(10) . ?
O5 P2 1.552(10) . ?
O6 P2 1.502(9) . ?
O7 N1 1.278(14) . ?
O8 N1 1.285(13) . ?
O9 N1 1.289(13) . ?
N2 C107 1.177(19) . ?
C107 C106 1.42(3) . ?
N3 C108 1.171(19) . ?
C108 C109 1.43(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C31 Ag1 C49 165.7(5) . . ?
C31 Ag1 O8 95.0(4) . . ?
C49 Ag1 O8 98.2(4) . . ?
C31 Ag1 O9 95.2(4) . . ?
C49 Ag1 O9 97.2(4) . . ?
O8 Ag1 O9 52.3(3) . . ?
C31 Ag1 Ag14 116.1(3) . . ?
C49 Ag1 Ag14 53.1(3) . . ?
O8 Ag1 Ag14 145.4(2) . . ?
O9 Ag1 Ag14 107.01(19) . . ?
C31 Ag1 Ag3B 114.8(4) . . ?
C49 Ag1 Ag3B 54.6(4) . . ?
O8 Ag1 Ag3B 112.4(3) . . ?
O9 Ag1 Ag3B 148.5(3) . . ?
Ag14 Ag1 Ag3B 69.4(2) . . ?
C31 Ag1 Ag18 52.1(3) . . ?
C49 Ag1 Ag18 117.5(3) . . ?
O8 Ag1 Ag18 140.4(2) . . ?
O9 Ag1 Ag18 103.68(19) . . ?
Ag14 Ag1 Ag18 64.48(3) . . ?
Ag3B Ag1 Ag18 102.4(2) . . ?
C31 Ag1 Ag16 53.2(3) . . ?
C49 Ag1 Ag16 116.5(3) . . ?
O8 Ag1 Ag16 108.8(2) . . ?
O9 Ag1 Ag16 144.48(19) . . ?
Ag14 Ag1 Ag16 102.27(3) . . ?
Ag3B Ag1 Ag16 62.02(19) . . ?
Ag18 Ag1 Ag16 71.43(3) . . ?
C31 Ag1 Ag3A 114.4(4) . . ?
C49 Ag1 Ag3A 56.0(4) . . ?
O8 Ag1 Ag3A 108.3(4) . . ?
O9 Ag1 Ag3A 147.1(3) . . ?
Ag14 Ag1 Ag3A 73.6(3) . . ?
Ag18 Ag1 Ag3A 105.8(3) . . ?
Ag16 Ag1 Ag3A 61.2(2) . . ?
C31 Ag1 Ag19 133.9(3) . . ?
C49 Ag1 Ag19 55.5(3) . . ?
O8 Ag1 Ag19 47.69(19) . . ?
O9 Ag1 Ag19 82.05(19) . . ?
Ag14 Ag1 Ag19 108.55(4) . . ?
Ag3B Ag1 Ag19 70.4(2) . . ?
Ag18 Ag1 Ag19 171.88(4) . . ?
Ag16 Ag1 Ag19 107.31(3) . . ?
Ag3A Ag1 Ag19 67.3(3) . . ?
C37 Ag2A C19 149.7(11) . . ?
C37 Ag2A C20 157.6(12) . . ?
C19 Ag2A C20 26.5(5) . . ?
C37 Ag2A Ag5 50.3(6) . . ?
C19 Ag2A Ag5 129.5(12) . . ?
C20 Ag2A Ag5 150.5(13) . . ?
C37 Ag2A Ag14 49.5(5) . . ?
C19 Ag2A Ag14 101.1(9) . . ?
C20 Ag2A Ag14 122.2(10) . . ?
Ag5 Ag2A Ag14 62.7(3) . . ?
C19 Ag2B C37 153.4(6) . . ?
C19 Ag2B O1WA 103.3(9) . . ?
C37 Ag2B O1WA 100.6(9) . . ?
C19 Ag2B C20 28.6(4) . . ?
C37 Ag2B C20 140.8(6) . . ?
O1WA Ag2B C20 90.7(9) . . ?
C19 Ag2B Ag14 113.8(5) . . ?
C37 Ag2B Ag14 50.1(3) . . ?
O1WA Ag2B Ag14 138.1(9) . . ?
C20 Ag2B Ag14 131.2(4) . . ?
C19 Ag2B Ag5 150.6(5) . . ?
C37 Ag2B Ag5 49.1(4) . . ?
O1WA Ag2B Ag5 74.7(9) . . ?
C20 Ag2B Ag5 164.7(4) . . ?
Ag14 Ag2B Ag5 63.42(9) . . ?
C19 Ag2B Ag3B 46.7(4) . . ?
C37 Ag2B Ag3B 117.9(5) . . ?
O1WA Ag2B Ag3B 136.5(8) . . ?
C20 Ag2B Ag3B 72.6(4) . . ?
Ag14 Ag2B Ag3B 68.9(3) . . ?
Ag5 Ag2B Ag3B 115.2(3) . . ?
C19 Ag2B Ag22 45.2(4) . . ?
C37 Ag2B Ag22 154.3(4) . . ?
O1WA Ag2B Ag22 78.3(8) . . ?
C20 Ag2B Ag22 64.7(3) . . ?
Ag14 Ag2B Ag22 114.7(2) . . ?
Ag5 Ag2B Ag22 107.2(2) . . ?
Ag3B Ag2B Ag22 58.2(2) . . ?
C19 Ag2C C37 171(2) . . ?
C19 Ag2C C20 30.7(7) . . ?
C37 Ag2C C20 152.7(19) . . ?
C19 Ag2C Ag14 121.4(16) . . ?
C37 Ag2C Ag14 51.1(7) . . ?
C20 Ag2C Ag14 144.5(18) . . ?
C19 Ag2C Ag5 138.9(17) . . ?
C37 Ag2C Ag5 44.2(8) . . ?
C20 Ag2C Ag5 151.3(16) . . ?
Ag14 Ag2C Ag5 60.5(7) . . ?
C19 Ag2C Ag22 42.0(8) . . ?
C37 Ag2C Ag22 141.1(16) . . ?
C20 Ag2C Ag22 63.4(9) . . ?
Ag14 Ag2C Ag22 112.0(12) . . ?
Ag5 Ag2C Ag22 97.2(11) . . ?
C19 Ag3A O4 150.3(14) . . ?
C19 Ag3A C49 123.4(10) . . ?
O4 Ag3A C49 83.1(6) . . ?
C19 Ag3A Ag22 48.7(4) . . ?
O4 Ag3A Ag22 122.4(7) . . ?
C49 Ag3A Ag22 136.5(9) . . ?
C19 Ag3A Ag16 105.7(6) . . ?
O4 Ag3A Ag16 81.4(4) . . ?
C49 Ag3A Ag16 96.6(7) . . ?
Ag22 Ag3A Ag16 58.9(2) . . ?
C19 Ag3A Ag1 134.6(10) . . ?
O4 Ag3A Ag1 73.5(5) . . ?
C49 Ag3A Ag1 41.2(4) . . ?
Ag22 Ag3A Ag1 108.0(5) . . ?
Ag16 Ag3A Ag1 55.9(3) . . ?
C19 Ag3B O4 132.5(8) . . ?
C19 Ag3B C49 132.2(7) . . ?
O4 Ag3B C49 85.9(5) . . ?
C19 Ag3B Ag1 147.8(7) . . ?
O4 Ag3B Ag1 77.5(3) . . ?
C49 Ag3B Ag1 45.7(4) . . ?
C19 Ag3B Ag22 47.7(4) . . ?
O4 Ag3B Ag22 115.2(5) . . ?
C49 Ag3B Ag22 149.7(7) . . ?
Ag1 Ag3B Ag22 114.9(4) . . ?
C19 Ag3B Ag2B 47.7(4) . . ?
O4 Ag3B Ag2B 177.3(5) . . ?
C49 Ag3B Ag2B 95.4(5) . . ?
Ag1 Ag3B Ag2B 101.8(5) . . ?
Ag22 Ag3B Ag2B 62.7(2) . . ?
C19 Ag3B Ag16 107.1(5) . . ?
O4 Ag3B Ag16 81.7(3) . . ?
C49 Ag3B Ag16 105.6(5) . . ?
Ag1 Ag3B Ag16 60.0(2) . . ?
Ag22 Ag3B Ag16 59.78(19) . . ?
Ag2B Ag3B Ag16 95.8(4) . . ?
C19 Ag3B Ag14 99.7(5) . . ?
O4 Ag3B Ag14 127.1(5) . . ?
C49 Ag3B Ag14 45.2(4) . . ?
Ag1 Ag3B Ag14 55.0(3) . . ?
Ag22 Ag3B Ag14 105.9(4) . . ?
Ag2B Ag3B Ag14 53.4(2) . . ?
Ag16 Ag3B Ag14 92.2(4) . . ?
C25 Ag4A C7 160(3) . . ?
C25 Ag4A Ag9 48.3(6) . . ?
C7 Ag4A Ag9 124.1(16) . . ?
C25 Ag4A Ag21 51.3(8) . . ?
C7 Ag4A Ag21 110.5(18) . . ?
Ag9 Ag4A Ag21 75.4(5) . . ?
C25 Ag4A Ag6 116.1(16) . . ?
C7 Ag4A Ag6 45.6(9) . . ?
Ag9 Ag4A Ag6 113.6(14) . . ?
Ag21 Ag4A Ag6 65.1(9) . . ?
C25 Ag4B C7 176.9(7) . . ?
C25 Ag4B Ag6 128.1(4) . . ?
C7 Ag4B Ag6 54.3(4) . . ?
C25 Ag4B Ag21 54.7(4) . . ?
C7 Ag4B Ag21 127.6(5) . . ?
Ag6 Ag4B Ag21 73.33(14) . . ?
C25 Ag4B A15 133.7(6) . . ?
C7 Ag4B A15 47.2(6) . . ?
Ag6 Ag4B A15 79.8(6) . . ?
Ag21 Ag4B A15 130.4(8) . . ?
C25 Ag4B Ag9 47.3(4) . . ?
C7 Ag4B Ag9 133.9(4) . . ?
Ag6 Ag4B Ag9 126.15(19) . . ?
Ag21 Ag4B Ag9 77.10(6) . . ?
A15 Ag4B Ag9 86.7(5) . . ?
C37 Ag5 C13 158.4(5) . . ?
C37 Ag5 O13 101.5(5) . . ?
C13 Ag5 O13 99.1(5) . . ?
C37 Ag5 Ag2A 41.6(7) . . ?
C13 Ag5 Ag2A 132.0(8) . . ?
O13 Ag5 Ag2A 114.8(7) . . ?
C37 Ag5 Ag2B 50.2(4) . . ?
C13 Ag5 Ag2B 121.1(4) . . ?
O13 Ag5 Ag2B 123.7(4) . . ?
C37 Ag5 Ag17 123.2(3) . . ?
C13 Ag5 Ag17 46.8(3) . . ?
O13 Ag5 Ag17 123.1(5) . . ?
Ag2A Ag5 Ag17 85.6(7) . . ?
Ag2B Ag5 Ag17 75.04(15) . . ?
C37 Ag5 Ag18 109.8(3) . . ?
C13 Ag5 Ag18 48.9(3) . . ?
O13 Ag5 Ag18 138.3(4) . . ?
Ag2A Ag5 Ag18 106.9(6) . . ?
Ag2B Ag5 Ag18 97.65(16) . . ?
Ag17 Ag5 Ag18 58.65(3) . . ?
C37 Ag5 Ag14 47.5(3) . . ?
C13 Ag5 Ag14 111.0(3) . . ?
O13 Ag5 Ag14 142.3(5) . . ?
Ag2A Ag5 Ag14 59.7(4) . . ?
Ag2B Ag5 Ag14 57.96(14) . . ?
Ag17 Ag5 Ag14 94.45(4) . . ?
Ag18 Ag5 Ag14 62.44(3) . . ?
C37 Ag5 Ag2C 45.6(8) . . ?
C13 Ag5 Ag2C 124.2(8) . . ?
O13 Ag5 Ag2C 124.7(8) . . ?
Ag17 Ag5 Ag2C 78.9(7) . . ?
Ag18 Ag5 Ag2C 96.9(7) . . ?
Ag14 Ag5 Ag2C 53.6(6) . . ?
C7 Ag6 C1 119.4(5) . . ?
C7 Ag6 C61 120.5(5) . . ?
C1 Ag6 C61 118.8(5) . . ?
C7 Ag6 Ag4B 45.8(3) . . ?
C1 Ag6 Ag4B 151.3(3) . . ?
C61 Ag6 Ag4B 84.9(3) . . ?
C7 Ag6 Ag13 153.6(3) . . ?
C1 Ag6 Ag13 83.3(4) . . ?
C61 Ag6 Ag13 44.2(4) . . ?
Ag4B Ag6 Ag13 107.85(5) . . ?
C7 Ag6 Ag20 84.3(3) . . ?
C1 Ag6 Ag20 42.1(3) . . ?
C61 Ag6 Ag20 153.0(4) . . ?
Ag4B Ag6 Ag20 109.70(7) . . ?
Ag13 Ag6 Ag20 108.89(4) . . ?
C7 Ag6 Ag4A 45.6(5) . . ?
C1 Ag6 Ag4A 154.7(6) . . ?
C61 Ag6 Ag4A 82.9(5) . . ?
Ag13 Ag6 Ag4A 108.2(3) . . ?
Ag20 Ag6 Ag4A 112.9(5) . . ?
C43 Ag7 O6 155.8(5) . . ?
C43 Ag7 Ag8 52.3(4) . . ?
O6 Ag7 Ag8 145.3(3) . . ?
C43 Ag7 Ag21 50.2(4) . . ?
O6 Ag7 Ag21 138.3(3) . . ?
Ag8 Ag7 Ag21 69.73(3) . . ?
C43 Ag7 Ag9 123.6(4) . . ?
O6 Ag7 Ag9 67.1(3) . . ?
Ag8 Ag7 Ag9 121.16(4) . . ?
Ag21 Ag7 Ag9 74.11(3) . . ?
C43 Ag7 Ag19 128.4(4) . . ?
O6 Ag7 Ag19 70.2(3) . . ?
Ag8 Ag7 Ag19 76.56(4) . . ?
Ag21 Ag7 Ag19 122.71(4) . . ?
Ag9 Ag7 Ag19 86.36(4) . . ?
C43 Ag8 C67 121.1(5) . . ?
C43 Ag8 C73 117.8(5) . . ?
C67 Ag8 C73 119.9(5) . . ?
C43 Ag8 Ag10 151.3(3) . . ?
C67 Ag8 Ag10 84.0(4) . . ?
C73 Ag8 Ag10 45.0(3) . . ?
C43 Ag8 Ag7 45.4(3) . . ?
C67 Ag8 Ag7 156.4(4) . . ?
C73 Ag8 Ag7 80.1(3) . . ?
Ag10 Ag8 Ag7 106.03(4) . . ?
C43 Ag8 Ag13 83.8(4) . . ?
C67 Ag8 Ag13 45.1(4) . . ?
C73 Ag8 Ag13 155.0(3) . . ?
Ag10 Ag8 Ag13 109.98(4) . . ?
Ag7 Ag8 Ag13 111.54(4) . . ?
O5 Ag9 C25 153.9(4) . . ?
O5 Ag9 O8 93.9(3) . . ?
C25 Ag9 O8 104.4(4) . . ?
O5 Ag9 C26 126.2(4) . . ?
C25 Ag9 C26 27.7(5) . . ?
O8 Ag9 C26 119.7(4) . . ?
O5 Ag9 Ag4A 162.1(5) . . ?
C25 Ag9 Ag4A 37.6(7) . . ?
O8 Ag9 Ag4A 91.7(11) . . ?
C26 Ag9 Ag4A 64.1(8) . . ?
O5 Ag9 Ag4B 162.3(2) . . ?
C25 Ag9 Ag4B 42.0(4) . . ?
O8 Ag9 Ag4B 82.5(2) . . ?
C26 Ag9 Ag4B 69.5(3) . . ?
O5 Ag9 Ag7 93.3(2) . . ?
C25 Ag9 Ag7 82.5(4) . . ?
O8 Ag9 Ag7 55.23(19) . . ?
C26 Ag9 Ag7 77.1(3) . . ?
Ag4A Ag9 Ag7 103.9(6) . . ?
Ag4B Ag9 Ag7 98.71(9) . . ?
C85 Ag10 C73 177.0(5) . . ?
C85 Ag10 Ag11 55.5(4) . . ?
C73 Ag10 Ag11 126.9(4) . . ?
C85 Ag10 Ag8 127.5(4) . . ?
C73 Ag10 Ag8 54.9(4) . . ?
Ag11 Ag10 Ag8 72.01(4) . . ?
C85 Ag10 Ag19 133.5(4) . . ?
C73 Ag10 Ag19 47.3(4) . . ?
Ag11 Ag10 Ag19 125.83(4) . . ?
Ag8 Ag10 Ag19 78.32(4) . . ?
C85 Ag10 Ag12 47.5(4) . . ?
C73 Ag10 Ag12 133.5(4) . . ?
Ag11 Ag10 Ag12 76.04(4) . . ?
Ag8 Ag10 Ag12 125.21(4) . . ?
Ag19 Ag10 Ag12 86.16(4) . . ?
C1 Ag11 C67 118.7(5) . . ?
C1 Ag11 C85 121.9(5) . . ?
C67 Ag11 C85 118.0(5) . . ?
C1 Ag11 Ag20 44.8(3) . . ?
C67 Ag11 Ag20 155.4(4) . . ?
C85 Ag11 Ag20 84.1(3) . . ?
C1 Ag11 Ag10 153.1(3) . . ?
C67 Ag11 Ag10 83.7(4) . . ?
C85 Ag11 Ag10 44.4(3) . . ?
Ag20 Ag11 Ag10 108.86(4) . . ?
C1 Ag11 Ag13 83.3(4) . . ?
C67 Ag11 Ag13 43.7(4) . . ?
C85 Ag11 Ag13 152.2(3) . . ?
Ag20 Ag11 Ag13 111.72(4) . . ?
Ag10 Ag11 Ag13 107.80(4) . . ?
C85 Ag12 O2 151.7(4) . . ?
C85 Ag12 O9 104.4(4) . . ?
O2 Ag12 O9 92.1(3) . . ?
C85 Ag12 C86 27.6(5) . . ?
O2 Ag12 C86 124.2(4) . . ?
O9 Ag12 C86 121.2(4) . . ?
C85 Ag12 Ag10 42.4(4) . . ?
O2 Ag12 Ag10 165.4(2) . . ?
O9 Ag12 Ag10 83.3(2) . . ?
C86 Ag12 Ag10 69.4(4) . . ?
C85 Ag12 Ag20 81.0(4) . . ?
O2 Ag12 Ag20 90.0(2) . . ?
O9 Ag12 Ag20 55.71(19) . . ?
C86 Ag12 Ag20 77.6(4) . . ?
Ag10 Ag12 Ag20 98.66(4) . . ?
C61 Ag13 C67 175.7(5) . . ?
C61 Ag13 Ag8 125.0(4) . . ?
C67 Ag13 Ag8 53.2(4) . . ?
C61 Ag13 Ag21 54.6(4) . . ?
C67 Ag13 Ag21 123.7(4) . . ?
Ag8 Ag13 Ag21 70.47(4) . . ?
C61 Ag13 Ag6 54.1(4) . . ?
C67 Ag13 Ag6 122.0(4) . . ?
Ag8 Ag13 Ag6 108.56(4) . . ?
Ag21 Ag13 Ag6 71.07(3) . . ?
C61 Ag13 Ag11 123.8(4) . . ?
C67 Ag13 Ag11 52.3(4) . . ?
Ag8 Ag13 Ag11 70.17(3) . . ?
Ag21 Ag13 Ag11 109.70(4) . . ?
Ag6 Ag13 Ag11 69.73(4) . . ?
C37 Ag14 O2 118.1(4) . . ?
C37 Ag14 C49 140.4(5) . . ?
O2 Ag14 C49 92.2(4) . . ?
C37 Ag14 Ag2C 52.1(9) . . ?
O2 Ag14 Ag2C 170.1(8) . . ?
C49 Ag14 Ag2C 95.9(9) . . ?
C37 Ag14 Ag2B 50.4(4) . . ?
O2 Ag14 Ag2B 166.7(3) . . ?
C49 Ag14 Ag2B 101.1(3) . . ?
C37 Ag14 Ag1 152.4(3) . . ?
O2 Ag14 Ag1 82.8(2) . . ?
C49 Ag14 Ag1 46.3(3) . . ?
Ag2C Ag14 Ag1 106.9(8) . . ?
Ag2B Ag14 Ag1 106.03(16) . . ?
C37 Ag14 Ag2A 40.5(7) . . ?
O2 Ag14 Ag2A 158.6(7) . . ?
C49 Ag14 Ag2A 107.3(6) . . ?
Ag1 Ag14 Ag2A 117.0(7) . . ?
C37 Ag14 Ag5 46.8(3) . . ?
O2 Ag14 Ag5 109.2(2) . . ?
C49 Ag14 Ag5 148.1(3) . . ?
Ag2C Ag14 Ag5 65.9(8) . . ?
Ag2B Ag14 Ag5 58.62(16) . . ?
Ag1 Ag14 Ag5 111.67(4) . . ?
Ag2A Ag14 Ag5 57.6(4) . . ?
C37 Ag14 Ag18 105.1(4) . . ?
O2 Ag14 Ag18 80.8(2) . . ?
C49 Ag14 Ag18 104.3(3) . . ?
Ag2C Ag14 Ag18 102.5(8) . . ?
Ag2B Ag14 Ag18 95.36(16) . . ?
Ag1 Ag14 Ag18 58.11(3) . . ?
Ag2A Ag14 Ag18 102.2(5) . . ?
Ag5 Ag14 Ag18 58.39(3) . . ?
C37 Ag14 Ag3B 107.2(4) . . ?
O2 Ag14 Ag3B 134.6(3) . . ?
C49 Ag14 Ag3B 46.9(4) . . ?
Ag2B Ag14 Ag3B 57.7(2) . . ?
Ag1 Ag14 Ag3B 55.61(17) . . ?
Ag5 Ag14 Ag3B 103.24(17) . . ?
Ag18 Ag14 Ag3B 90.36(19) . . ?
O1 Ag15 C7 154.8(6) . . ?
O1 Ag15 O9 93.9(4) . . ?
C7 Ag15 O9 104.9(4) . . ?
O1 Ag15 C8 126.1(5) . . ?
C7 Ag15 C8 28.7(5) . . ?
O9 Ag15 C8 124.6(5) . . ?
O1 Ag15 Ag20 91.2(5) . . ?
C7 Ag15 Ag20 85.5(5) . . ?
O9 Ag15 Ag20 56.8(3) . . ?
C8 Ag15 Ag20 82.9(5) . . ?
C7 A15 O1 142.3(15) . . ?
C7 A15 C8 28.8(6) . . ?
O1 A15 C8 115.8(12) . . ?
C7 A15 Ag4B 46.3(9) . . ?
O1 A15 Ag4B 168.1(14) . . ?
C8 A15 Ag4B 74.3(11) . . ?
C79 Ag16 O5 132.5(4) . . ?
C79 Ag16 C31 131.5(5) . . ?
O5 Ag16 C31 87.4(4) . . ?
C79 Ag16 Ag17 47.1(3) . . ?
O5 Ag16 Ag17 179.6(2) . . ?
C31 Ag16 Ag17 93.0(3) . . ?
C79 Ag16 Ag1 145.5(3) . . ?
O5 Ag16 Ag1 80.1(2) . . ?
C31 Ag16 Ag1 44.4(3) . . ?
Ag17 Ag16 Ag1 100.25(4) . . ?
C79 Ag16 Ag22 47.9(3) . . ?
O5 Ag16 Ag22 117.3(2) . . ?
C31 Ag16 Ag22 145.1(3) . . ?
Ag17 Ag16 Ag22 62.30(3) . . ?
Ag1 Ag16 Ag22 112.36(4) . . ?
C79 Ag16 Ag3B 106.3(4) . . ?
O5 Ag16 Ag3B 86.1(3) . . ?
C31 Ag16 Ag3B 102.1(4) . . ?
Ag17 Ag16 Ag3B 93.8(2) . . ?
Ag1 Ag16 Ag3B 58.0(2) . . ?
Ag22 Ag16 Ag3B 58.99(18) . . ?
C79 Ag16 Ag3A 104.7(4) . . ?
O5 Ag16 Ag3A 82.6(4) . . ?
C31 Ag16 Ag3A 107.2(5) . . ?
Ag17 Ag16 Ag3A 97.3(3) . . ?
Ag1 Ag16 Ag3A 62.9(4) . . ?
Ag22 Ag16 Ag3A 56.8(2) . . ?
C79 Ag17 C13 155.8(5) . . ?
C79 Ag17 Ag16 49.8(3) . . ?
C13 Ag17 Ag16 122.0(3) . . ?
C79 Ag17 Ag18 121.3(3) . . ?
C13 Ag17 Ag18 50.7(3) . . ?
Ag16 Ag17 Ag18 73.10(4) . . ?
C79 Ag17 Ag5 154.1(4) . . ?
C13 Ag17 Ag5 48.5(4) . . ?
Ag16 Ag17 Ag5 118.57(4) . . ?
Ag18 Ag17 Ag5 61.58(3) . . ?
C79 Ag17 Ag22 47.2(4) . . ?
C13 Ag17 Ag22 155.4(4) . . ?
Ag16 Ag17 Ag22 60.58(3) . . ?
Ag18 Ag17 Ag22 118.28(4) . . ?
Ag5 Ag17 Ag22 107.36(4) . . ?
C13 Ag18 O1 124.2(4) . . ?
C13 Ag18 C31 132.3(5) . . ?
O1 Ag18 C31 95.3(4) . . ?
C13 Ag18 Ag17 47.2(3) . . ?
O1 Ag18 Ag17 170.1(2) . . ?
C31 Ag18 Ag17 94.6(3) . . ?
C13 Ag18 Ag1 146.6(3) . . ?
O1 Ag18 Ag1 85.6(2) . . ?
C31 Ag18 Ag1 45.5(3) . . ?
Ag17 Ag18 Ag1 101.46(4) . . ?
C13 Ag18 Ag5 47.3(3) . . ?
O1 Ag18 Ag5 111.3(2) . . ?
C31 Ag18 Ag5 144.7(3) . . ?
Ag17 Ag18 Ag5 59.77(3) . . ?
Ag1 Ag18 Ag5 111.76(4) . . ?
C13 Ag18 Ag14 106.2(3) . . ?
O1 Ag18 Ag14 84.8(2) . . ?
C31 Ag18 Ag14 102.6(3) . . ?
Ag17 Ag18 Ag14 93.10(4) . . ?
Ag1 Ag18 Ag14 57.41(3) . . ?
Ag5 Ag18 Ag14 59.18(3) . . ?
C73 Ag19 O4 151.2(4) . . ?
C73 Ag19 O8 102.3(4) . . ?
O4 Ag19 O8 90.6(3) . . ?
C73 Ag19 C74 26.9(4) . . ?
O4 Ag19 C74 124.8(4) . . ?
O8 Ag19 C74 117.3(4) . . ?
C73 Ag19 Ag10 43.3(4) . . ?
O4 Ag19 Ag10 165.5(2) . . ?
O8 Ag19 Ag10 83.2(2) . . ?
C74 Ag19 Ag10 69.6(3) . . ?
C73 Ag19 Ag7 77.4(4) . . ?
O4 Ag19 Ag7 90.0(2) . . ?
O8 Ag19 Ag7 54.61(19) . . ?
C74 Ag19 Ag7 73.5(3) . . ?
Ag10 Ag19 Ag7 96.97(4) . . ?
C73 Ag19 Ag1 137.1(3) . . ?
O4 Ag19 Ag1 69.3(2) . . ?
O8 Ag19 Ag1 46.96(18) . . ?
C74 Ag19 Ag1 162.0(3) . . ?
Ag10 Ag19 Ag1 97.07(4) . . ?
Ag7 Ag19 Ag1 96.97(4) . . ?
C1 Ag20 O3 158.2(5) . . ?
C1 Ag20 Ag11 52.0(4) . . ?
O3 Ag20 Ag11 141.3(3) . . ?
C1 Ag20 Ag6 51.1(4) . . ?
O3 Ag20 Ag6 140.6(3) . . ?
Ag11 Ag20 Ag6 69.64(4) . . ?
C1 Ag20 Ag15 122.4(4) . . ?
O3 Ag20 Ag15 70.3(3) . . ?
Ag11 Ag20 Ag15 119.17(14) . . ?
Ag6 Ag20 Ag15 71.90(11) . . ?
C1 Ag20 Ag12 126.1(4) . . ?
O3 Ag20 Ag12 69.1(3) . . ?
Ag11 Ag20 Ag12 74.30(4) . . ?
Ag6 Ag20 Ag12 118.50(4) . . ?
Ag15 Ag20 Ag12 85.25(8) . . ?
C43 Ag21 C25 119.5(5) . . ?
C43 Ag21 C61 120.2(5) . . ?
C25 Ag21 C61 119.8(5) . . ?
C43 Ag21 Ag4B 149.5(3) . . ?
C25 Ag21 Ag4B 44.8(4) . . ?
C61 Ag21 Ag4B 84.3(4) . . ?
C43 Ag21 Ag13 83.4(4) . . ?
C25 Ag21 Ag13 152.3(3) . . ?
C61 Ag21 Ag13 44.2(3) . . ?
Ag4B Ag21 Ag13 107.62(13) . . ?
C43 Ag21 Ag7 43.8(3) . . ?
C25 Ag21 Ag7 83.2(3) . . ?
C61 Ag21 Ag7 152.2(3) . . ?
Ag4B Ag21 Ag7 106.07(6) . . ?
Ag13 Ag21 Ag7 108.21(4) . . ?
C43 Ag21 Ag4A 149.6(5) . . ?
C25 Ag21 Ag4A 37.1(9) . . ?
C61 Ag21 Ag4A 88.3(6) . . ?
Ag13 Ag21 Ag4A 115.6(9) . . ?
Ag7 Ag21 Ag4A 105.8(4) . . ?
C19 Ag22 C79 151.8(5) . . ?
C19 Ag22 O10 103.3(5) . . ?
C79 Ag22 O10 102.0(5) . . ?
C19 Ag22 O11 102.5(4) . . ?
C79 Ag22 O11 97.0(4) . . ?
O10 Ag22 O11 71.8(4) . . ?
C19 Ag22 Ag3A 45.7(4) . . ?
C79 Ag22 Ag3A 111.9(4) . . ?
O10 Ag22 Ag3A 113.2(6) . . ?
O11 Ag22 Ag3A 148.0(4) . . ?
C19 Ag22 Ag3B 47.2(4) . . ?
C79 Ag22 Ag3B 108.2(4) . . ?
O10 Ag22 Ag3B 120.3(5) . . ?
O11 Ag22 Ag3B 147.6(3) . . ?
C19 Ag22 Ag16 108.0(3) . . ?
C79 Ag22 Ag16 47.6(3) . . ?
O10 Ag22 Ag16 118.8(3) . . ?
O11 Ag22 Ag16 143.3(3) . . ?
Ag3A Ag22 Ag16 64.3(3) . . ?
Ag3B Ag22 Ag16 61.2(2) . . ?
C19 Ag22 Ag17 114.1(3) . . ?
C79 Ag22 Ag17 44.4(3) . . ?
O10 Ag22 Ag17 141.8(4) . . ?
O11 Ag22 Ag17 92.1(3) . . ?
Ag3A Ag22 Ag17 98.9(5) . . ?
Ag3B Ag22 Ag17 92.0(3) . . ?
Ag16 Ag22 Ag17 57.12(3) . . ?
C19 Ag22 Ag2B 45.7(4) . . ?
C79 Ag22 Ag2B 113.9(3) . . ?
O10 Ag22 Ag2B 142.4(4) . . ?
O11 Ag22 Ag2B 92.5(3) . . ?
Ag3B Ag22 Ag2B 59.1(3) . . ?
Ag16 Ag22 Ag2B 94.41(11) . . ?
Ag17 Ag22 Ag2B 70.08(12) . . ?
C19 Ag22 Ag2C 39.5(8) . . ?
C79 Ag22 Ag2C 118.8(7) . . ?
O10 Ag22 Ag2C 138.8(7) . . ?
O11 Ag22 Ag2C 95.9(7) . . ?
Ag16 Ag22 Ag2C 94.8(6) . . ?
Ag17 Ag22 Ag2C 75.6(7) . . ?
C2 C1 Ag20 157.5(13) . . ?
C2 C1 Ag11 118.9(12) . . ?
Ag20 C1 Ag11 83.2(5) . . ?
C2 C1 Ag6 95.3(11) . . ?
Ag20 C1 Ag6 86.8(5) . . ?
Ag11 C1 Ag6 93.2(5) . . ?
C1 C2 C3 170.4(17) . . ?
C2 C3 C6 108.1(17) . . ?
C2 C3 C4 110.0(16) . . ?
C6 C3 C4 115(2) . . ?
C2 C3 C5 109.3(17) . . ?
C6 C3 C5 108(2) . . ?
C4 C3 C5 106.5(19) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 Ag4B 163.5(14) . . ?
C8 C7 A15 93.7(12) . . ?
Ag4B C7 A15 86.5(10) . . ?
C8 C7 Ag15 88.4(10) . . ?
C8 C7 Ag6 115.2(12) . . ?
Ag4B C7 Ag6 79.9(5) . . ?
A15 C7 Ag6 110.6(11) . . ?
Ag15 C7 Ag6 104.2(6) . . ?
C8 C7 Ag4A 153.2(17) . . ?
Ag15 C7 Ag4A 97.5(9) . . ?
Ag6 C7 Ag4A 88.8(10) . . ?
C7 C8 C9 168.4(17) . . ?
C7 C8 A15 57.5(11) . . ?
C9 C8 A15 128.9(13) . . ?
C7 C8 Ag15 62.9(9) . . ?
C9 C8 Ag15 125.2(12) . . ?
C8 C9 C12 110.3(19) . . ?
C8 C9 C10 110.5(19) . . ?
C12 C9 C10 114(3) . . ?
C8 C9 C11 106.4(18) . . ?
C12 C9 C11 112(3) . . ?
C10 C9 C11 103(3) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag17 143.7(12) . . ?
C14 C13 Ag5 130.5(12) . . ?
Ag17 C13 Ag5 84.7(5) . . ?
C14 C13 Ag18 107.0(10) . . ?
Ag17 C13 Ag18 82.2(4) . . ?
Ag5 C13 Ag18 83.8(4) . . ?
C13 C14 C15 177.4(17) . . ?
C18 C15 C14 108.9(18) . . ?
C18 C15 C17 114(2) . . ?
C14 C15 C17 108.0(16) . . ?
C18 C15 C16 111(2) . . ?
C14 C15 C16 108.1(15) . . ?
C17 C15 C16 106.8(19) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C15 C17 H17A 109.5 . . ?
C15 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C15 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 Ag2C 86.9(14) . . ?
C20 C19 Ag3A 150.0(12) . . ?
C20 C19 Ag3B 150.4(12) . . ?
C20 C19 Ag22 124.1(11) . . ?
Ag2C C19 Ag22 98.6(12) . . ?
Ag3A C19 Ag22 85.6(5) . . ?
Ag3B C19 Ag22 85.1(5) . . ?
C20 C19 Ag2B 89.7(10) . . ?
Ag3B C19 Ag2B 85.6(6) . . ?
Ag22 C19 Ag2B 89.1(5) . . ?
C20 C19 Ag2A 80.5(10) . . ?
Ag3A C19 Ag2A 101.3(10) . . ?
Ag22 C19 Ag2A 97.5(7) . . ?
C19 C20 C21 173.5(15) . . ?
C19 C20 Ag2C 62.4(12) . . ?
C21 C20 Ag2C 123.8(14) . . ?
C19 C20 Ag2B 61.7(9) . . ?
C21 C20 Ag2B 124.8(10) . . ?
C19 C20 Ag2A 73.0(11) . . ?
C21 C20 Ag2A 113.3(11) . . ?
C20 C21 C23 108.8(14) . . ?
C20 C21 C24 107.8(14) . . ?
C23 C21 C24 112.5(16) . . ?
C20 C21 C22 107.8(13) . . ?
C23 C21 C22 108.9(16) . . ?
C24 C21 C22 110.9(16) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 Ag4A 158(2) . . ?
C26 C25 Ag4B 170.9(13) . . ?
C26 C25 Ag9 92.4(10) . . ?
Ag4A C25 Ag9 94.1(10) . . ?
Ag4B C25 Ag9 90.7(5) . . ?
C26 C25 Ag21 106.8(11) . . ?
Ag4A C25 Ag21 91.6(14) . . ?
Ag4B C25 Ag21 80.5(5) . . ?
Ag9 C25 Ag21 106.2(5) . . ?
C25 C26 C27 168.5(17) . . ?
C25 C26 Ag9 59.8(9) . . ?
C27 C26 Ag9 125.5(12) . . ?
C30 C27 C29 114(2) . . ?
C30 C27 C26 108.9(16) . . ?
C29 C27 C26 111.3(18) . . ?
C30 C27 C28 111(2) . . ?
C29 C27 C28 106.0(19) . . ?
C26 C27 C28 105.0(15) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 Ag1 170.9(10) . . ?
C32 C31 Ag18 106.7(9) . . ?
Ag1 C31 Ag18 82.4(4) . . ?
C32 C31 Ag16 96.7(9) . . ?
Ag1 C31 Ag16 82.4(4) . . ?
Ag18 C31 Ag16 93.4(4) . . ?
C31 C32 C33 173.9(14) . . ?
C32 C33 C36 109.0(14) . . ?
C32 C33 C35 108.7(14) . . ?
C36 C33 C35 114.7(17) . . ?
C32 C33 C34 110.4(12) . . ?
C36 C33 C34 107.4(15) . . ?
C35 C33 C34 106.6(15) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 Ag2A 125.7(15) . . ?
C38 C37 Ag5 130.8(12) . . ?
Ag2A C37 Ag5 88.2(8) . . ?
C38 C37 Ag14 123.5(13) . . ?
Ag2A C37 Ag14 90.0(9) . . ?
Ag5 C37 Ag14 85.7(4) . . ?
C38 C37 Ag2B 137.7(13) . . ?
Ag5 C37 Ag2B 80.7(5) . . ?
Ag14 C37 Ag2B 79.5(5) . . ?
C38 C37 Ag2C 131.5(15) . . ?
Ag5 C37 Ag2C 90.2(11) . . ?
Ag14 C37 Ag2C 76.8(10) . . ?
C37 C38 C39 176.5(18) . . ?
C38 C39 C42 107(3) . . ?
C38 C39 C41 110(3) . . ?
C42 C39 C41 110.6(17) . . ?
C38 C39 C40 109.6(17) . . ?
C42 C39 C40 110.0(17) . . ?
C41 C39 C40 109.4(17) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 Ag7 159.7(13) . . ?
C44 C43 Ag21 101.1(11) . . ?
Ag7 C43 Ag21 85.9(5) . . ?
C44 C43 Ag8 115.9(12) . . ?
Ag7 C43 Ag8 82.3(5) . . ?
Ag21 C43 Ag8 93.6(5) . . ?
C43 C44 C45 171(2) . . ?
C47 C45 C44 117(2) . . ?
C47 C45 C48 114(3) . . ?
C44 C45 C48 113(2) . . ?
C47 C45 C46 109(3) . . ?
C44 C45 C46 103(2) . . ?
C48 C45 C46 100(3) . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C45 C47 H47A 109.5 . . ?
C45 C47 H47B 109.5 . . ?
H47A C47 H47B 109.5 . . ?
C45 C47 H47C 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
C45 C48 H48A 109.5 . . ?
C45 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C45 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 Ag1 170.0(10) . . ?
C50 C49 Ag14 107.2(9) . . ?
Ag1 C49 Ag14 80.6(4) . . ?
C50 C49 Ag3B 106.5(10) . . ?
Ag1 C49 Ag3B 79.6(5) . . ?
Ag14 C49 Ag3B 87.9(5) . . ?
C50 C49 Ag3A 102.6(9) . . ?
Ag1 C49 Ag3A 82.9(5) . . ?
Ag14 C49 Ag3A 93.4(6) . . ?
C49 C50 C51 165.2(15) . . ?
C52 C51 C50 114.3(15) . . ?
C52 C51 C53 107(2) . . ?
C50 C51 C53 102.4(15) . . ?
C52 C51 C59 117(2) . . ?
C50 C51 C59 107.4(15) . . ?
C53 C51 C59 107(2) . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C51 C53 H53A 109.5 . . ?
C51 C53 H53B 109.5 . . ?
H53A C53 H53B 109.5 . . ?
C51 C53 H53C 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C51 C59 H59A 109.5 . . ?
C51 C59 H59B 109.5 . . ?
H59A C59 H59B 109.5 . . ?
C51 C59 H59C 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C62 C61 Ag13 171.0(13) . . ?
C62 C61 Ag6 105.9(12) . . ?
Ag13 C61 Ag6 81.8(5) . . ?
C62 C61 Ag21 103.4(11) . . ?
Ag13 C61 Ag21 81.2(5) . . ?
Ag6 C61 Ag21 90.0(4) . . ?
C61 C62 C63 173.9(16) . . ?
C62 C63 C65 108.0(15) . . ?
C62 C63 C64 111.9(16) . . ?
C65 C63 C64 105(2) . . ?
C62 C63 C66 109.9(18) . . ?
C65 C63 C66 112(2) . . ?
C64 C63 C66 110(2) . . ?
C63 C64 H64A 109.5 . . ?
C63 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C63 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C63 C65 H65A 109.5 . . ?
C63 C65 H65B 109.5 . . ?
H65A C65 H65B 109.5 . . ?
C63 C65 H65C 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
C63 C66 H66A 109.5 . . ?
C63 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C63 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C68 C67 Ag13 164.6(13) . . ?
C68 C67 Ag8 112.8(12) . . ?
Ag13 C67 Ag8 81.7(5) . . ?
C68 C67 Ag11 100.3(11) . . ?
Ag13 C67 Ag11 84.0(5) . . ?
Ag8 C67 Ag11 91.6(4) . . ?
C67 C68 C69 169.8(16) . . ?
C68 C69 C72 111.8(19) . . ?
C68 C69 C70 109.2(16) . . ?
C72 C69 C70 109.3(14) . . ?
C68 C69 C71 110.1(18) . . ?
C72 C69 C71 108.4(14) . . ?
C70 C69 C71 108.0(15) . . ?
C69 C70 H70A 109.5 . . ?
C69 C70 H70B 109.5 . . ?
H70A C70 H70B 109.5 . . ?
C69 C70 H70C 109.5 . . ?
H70A C70 H70C 109.5 . . ?
H70B C70 H70C 109.5 . . ?
C69 C71 H71A 109.5 . . ?
C69 C71 H71B 109.5 . . ?
H71A C71 H71B 109.5 . . ?
C69 C71 H71C 109.5 . . ?
H71A C71 H71C 109.5 . . ?
H71B C71 H71C 109.5 . . ?
C69 C72 H72A 109.5 . . ?
C69 C72 H72B 109.5 . . ?
H72A C72 H72B 109.5 . . ?
C69 C72 H72C 109.5 . . ?
H72A C72 H72C 109.5 . . ?
H72B C72 H72C 109.5 . . ?
C74 C73 Ag10 166.3(13) . . ?
C74 C73 Ag19 93.9(10) . . ?
Ag10 C73 Ag19 89.4(5) . . ?
C74 C73 Ag8 111.4(11) . . ?
Ag10 C73 Ag8 80.0(4) . . ?
Ag19 C73 Ag8 107.7(5) . . ?
C73 C74 C75 168.8(16) . . ?
C73 C74 Ag19 59.3(8) . . ?
C75 C74 Ag19 128.6(10) . . ?
C74 C75 C77A 114(2) . . ?
C74 C75 C76A 110(2) . . ?
C77A C75 C76A 119(4) . . ?
C74 C75 C76 108.2(18) . . ?
C74 C75 C77 105(2) . . ?
C76 C75 C77 111.5(15) . . ?
C74 C75 C78 110.8(19) . . ?
C76 C75 C78 110.6(15) . . ?
C77 C75 C78 110.6(15) . . ?
C74 C75 C78A 107(2) . . ?
C77A C75 C78A 98(3) . . ?
C76A C75 C78A 107(3) . . ?
C75 C76 H76A 109.5 . . ?
C75 C76 H76B 109.5 . . ?
H76A C76 H76B 109.5 . . ?
C75 C76 H76C 109.5 . . ?
H76A C76 H76C 109.5 . . ?
H76B C76 H76C 109.5 . . ?
C75 C77 H77A 109.5 . . ?
C75 C77 H77B 109.5 . . ?
H77A C77 H77B 109.5 . . ?
C75 C77 H77C 109.5 . . ?
H77A C77 H77C 109.5 . . ?
H77B C77 H77C 109.5 . . ?
C75 C78 H78A 109.5 . . ?
C75 C78 H78B 109.5 . . ?
H78A C78 H78B 109.5 . . ?
C75 C78 H78C 109.5 . . ?
H78A C78 H78C 109.5 . . ?
H78B C78 H78C 109.5 . . ?
C75 C76A H76D 109.5 . . ?
C75 C76A H76E 109.5 . . ?
H76D C76A H76E 109.5 . . ?
C75 C76A H76F 109.5 . . ?
H76D C76A H76F 109.5 . . ?
H76E C76A H76F 109.5 . . ?
C75 C77A H77D 109.5 . . ?
C75 C77A H77E 109.5 . . ?
H77D C77A H77E 109.5 . . ?
C75 C77A H77F 109.5 . . ?
H77D C77A H77F 109.5 . . ?
H77E C77A H77F 109.5 . . ?
C75 C78A H78D 109.5 . . ?
C75 C78A H78E 109.5 . . ?
H78D C78A H78E 109.5 . . ?
C75 C78A H78F 109.5 . . ?
H78D C78A H78F 109.5 . . ?
H78E C78A H78F 109.5 . . ?
C80 C79 Ag17 143.8(12) . . ?
C80 C79 Ag16 119.2(11) . . ?
Ag17 C79 Ag16 83.0(4) . . ?
C80 C79 Ag22 119.9(11) . . ?
Ag17 C79 Ag22 88.4(5) . . ?
Ag16 C79 Ag22 84.5(4) . . ?
C79 C80 C81 176.7(17) . . ?
C80 C81 C84 110.0(15) . . ?
C80 C81 C83 108.7(16) . . ?
C84 C81 C83 111.2(18) . . ?
C80 C81 C82 105.9(16) . . ?
C84 C81 C82 113(2) . . ?
C83 C81 C82 108(2) . . ?
C81 C82 H82A 109.5 . . ?
C81 C82 H82B 109.5 . . ?
H82A C82 H82B 109.5 . . ?
C81 C82 H82C 109.5 . . ?
H82A C82 H82C 109.5 . . ?
H82B C82 H82C 109.5 . . ?
C81 C83 H83A 109.5 . . ?
C81 C83 H83B 109.5 . . ?
H83A C83 H83B 109.5 . . ?
C81 C83 H83C 109.5 . . ?
H83A C83 H83C 109.5 . . ?
H83B C83 H83C 109.5 . . ?
C81 C84 H84A 109.5 . . ?
C81 C84 H84B 109.5 . . ?
H84A C84 H84B 109.5 . . ?
C81 C84 H84C 109.5 . . ?
H84A C84 H84C 109.5 . . ?
H84B C84 H84C 109.5 . . ?
C86 C85 Ag10 165.3(14) . . ?
C86 C85 Ag12 93.6(11) . . ?
Ag10 C85 Ag12 90.1(5) . . ?
C86 C85 Ag11 112.7(13) . . ?
Ag10 C85 Ag11 80.1(5) . . ?
Ag12 C85 Ag11 103.2(5) . . ?
C85 C86 C87 172.5(18) . . ?
C85 C86 Ag12 58.9(9) . . ?
C87 C86 Ag12 126.9(12) . . ?
C86 C87 C90 106.2(18) . . ?
C86 C87 C89 113.2(18) . . ?
C90 C87 C89 111.3(15) . . ?
C86 C87 C88 108.4(19) . . ?
C90 C87 C88 108.7(15) . . ?
C89 C87 C88 108.8(14) . . ?
C87 C88 H88A 109.5 . . ?
C87 C88 H88B 109.5 . . ?
H88A C88 H88B 109.5 . . ?
C87 C88 H88C 109.5 . . ?
H88A C88 H88C 109.5 . . ?
H88B C88 H88C 109.5 . . ?
C87 C89 H89A 109.5 . . ?
C87 C89 H89B 109.5 . . ?
H89A C89 H89B 109.5 . . ?
C87 C89 H89C 109.5 . . ?
H89A C89 H89C 109.5 . . ?
H89B C89 H89C 109.5 . . ?
C87 C90 H90A 109.5 . . ?
C87 C90 H90B 109.5 . . ?
H90A C90 H90B 109.5 . . ?
C87 C90 H90C 109.5 . . ?
H90A C90 H90C 109.5 . . ?
H90B C90 H90C 109.5 . . ?
C94 C91 C93 108.3(13) . . ?
C94 C91 C92 108.8(13) . . ?
C93 C91 C92 109.4(14) . . ?
C94 C91 P2 111.6(10) . . ?
C93 C91 P2 108.9(10) . . ?
C92 C91 P2 109.8(10) . . ?
C91 C92 H92A 109.5 . . ?
C91 C92 H92B 109.5 . . ?
H92A C92 H92B 109.5 . . ?
C91 C92 H92C 109.5 . . ?
H92A C92 H92C 109.5 . . ?
H92B C92 H92C 109.5 . . ?
C91 C93 H93A 109.5 . . ?
C91 C93 H93B 109.5 . . ?
H93A C93 H93B 109.5 . . ?
C91 C93 H93C 109.5 . . ?
H93A C93 H93C 109.5 . . ?
H93B C93 H93C 109.5 . . ?
C91 C94 H94A 109.5 . . ?
C91 C94 H94B 109.5 . . ?
H94A C94 H94B 109.5 . . ?
C91 C94 H94C 109.5 . . ?
H94A C94 H94C 109.5 . . ?
H94B C94 H94C 109.5 . . ?
C96 C95 C98 107.7(13) . . ?
C96 C95 C97 110.8(13) . . ?
C98 C95 C97 110.9(13) . . ?
C96 C95 P1 111.2(10) . . ?
C98 C95 P1 107.8(11) . . ?
C97 C95 P1 108.5(10) . . ?
C95 C96 H96A 109.5 . . ?
C95 C96 H96B 109.5 . . ?
H96A C96 H96B 109.5 . . ?
C95 C96 H96C 109.5 . . ?
H96A C96 H96C 109.5 . . ?
H96B C96 H96C 109.5 . . ?
C95 C97 H97A 109.5 . . ?
C95 C97 H97B 109.5 . . ?
H97A C97 H97B 109.5 . . ?
C95 C97 H97C 109.5 . . ?
H97A C97 H97C 109.5 . . ?
H97B C97 H97C 109.5 . . ?
C95 C98 H98A 109.5 . . ?
C95 C98 H98B 109.5 . . ?
H98A C98 H98B 109.5 . . ?
C95 C98 H98C 109.5 . . ?
H98A C98 H98C 109.5 . . ?
H98B C98 H98C 109.5 . . ?
O11 C99 C101 134.5(18) . . ?
O11 C99 C103 114.3(17) . . ?
C101 C99 C103 111.2(15) . . ?
O10 C100 C101 131.8(17) . . ?
O10 C100 C102 111.3(16) . . ?
C101 C100 C102 116.8(14) . . ?
C100 C101 C99 119.4(16) . . ?
C100 C101 H101 120.3 . . ?
C99 C101 H101 120.3 . . ?
F3 C102 F2 107.3(14) . . ?
F3 C102 F1 105.9(13) . . ?
F2 C102 F1 106.3(14) . . ?
F3 C102 C100 114.7(15) . . ?
F2 C102 C100 113.0(14) . . ?
F1 C102 C100 109.1(14) . . ?
F4 C103 F6 104.4(16) . . ?
F4 C103 F5 102.0(15) . . ?
F6 C103 F5 100.2(16) . . ?
F4 C103 C99 122.0(18) . . ?
F6 C103 C99 113.1(16) . . ?
F5 C103 C99 112.5(18) . . ?
O12 C104 O13 120(2) . . ?
O12 C104 C105 125(2) . . ?
O13 C104 C105 112(2) . . ?
F7B C105 F8B 106.4(19) . . ?
F9 C105 F7 110.3(19) . . ?
F7B C105 F9B 104.4(19) . . ?
F8B C105 F9B 102.7(19) . . ?
F9 C105 F8 107.0(18) . . ?
F7 C105 F8 106.9(17) . . ?
F7B C105 C104 113(3) . . ?
F8B C105 C104 120(2) . . ?
F9 C105 C104 115(2) . . ?
F7 C105 C104 112(2) . . ?
F9B C105 C104 109(2) . . ?
F8 C105 C104 105(2) . . ?
P1 O1 Ag15 112.4(6) . . ?
P1 O1 Ag18 126.2(5) . . ?
Ag15 O1 Ag18 101.1(5) . . ?
P1 O1 A15 120.8(9) . . ?
Ag18 O1 A15 93.3(7) . . ?
P1 O2 Ag12 112.5(5) . . ?
P1 O2 Ag14 130.7(5) . . ?
Ag12 O2 Ag14 101.0(4) . . ?
P1 O3 Ag20 136.6(6) . . ?
P2 O4 Ag3A 127.9(6) . . ?
P2 O4 Ag19 113.9(5) . . ?
Ag3A O4 Ag19 109.4(6) . . ?
P2 O4 Ag3B 127.8(6) . . ?
Ag19 O4 Ag3B 104.1(4) . . ?
P2 O5 Ag9 109.6(5) . . ?
P2 O5 Ag16 125.3(5) . . ?
Ag9 O5 Ag16 107.3(4) . . ?
P2 O6 Ag7 137.6(6) . . ?
N1 O8 Ag9 120.5(7) . . ?
N1 O8 Ag1 96.6(6) . . ?
Ag9 O8 Ag1 90.2(3) . . ?
N1 O8 Ag19 117.6(7) . . ?
Ag9 O8 Ag19 121.8(3) . . ?
Ag1 O8 Ag19 85.4(3) . . ?
N1 O9 Ag15 119.5(8) . . ?
N1 O9 Ag12 118.8(7) . . ?
Ag15 O9 Ag12 121.6(4) . . ?
N1 O9 Ag1 93.1(6) . . ?
Ag15 O9 Ag1 91.2(3) . . ?
Ag12 O9 Ag1 87.1(3) . . ?
C100 O10 Ag22 133.5(12) . . ?
C99 O11 Ag22 128.3(13) . . ?
C104 O13 Ag5 123.2(15) . . ?
O7 N1 O8 121.2(10) . . ?
O7 N1 O9 120.7(9) . . ?
O8 N1 O9 118.0(10) . . ?
O3 P1 O2 111.8(6) . . ?
O3 P1 O1 111.6(6) . . ?
O2 P1 O1 111.4(5) . . ?
O3 P1 C95 106.9(6) . . ?
O2 P1 C95 107.6(6) . . ?
O1 P1 C95 107.3(6) . . ?
O6 P2 O4 112.1(5) . . ?
O6 P2 O5 111.1(6) . . ?
O4 P2 O5 111.5(5) . . ?
O6 P2 C91 106.4(6) . . ?
O4 P2 C91 107.9(6) . . ?
O5 P2 C91 107.4(6) . . ?
N2 C107 C106 167(5) . . ?
N3 C108 C109 173(9) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag4B C7 C8 C9 -36(12) . . . . ?
A15 C7 C8 C9 -127(9) . . . . ?
Ag15 C7 C8 C9 -137(9) . . . . ?
Ag6 C7 C8 C9 119(9) . . . . ?
Ag4A C7 C8 C9 -33(11) . . . . ?
Ag4B C7 C8 A15 90(4) . . . . ?
Ag6 C7 C8 A15 -114.8(15) . . . . ?
Ag6 C7 C8 Ag15 -104.9(9) . . . . ?
Ag4A C7 C8 Ag15 104(3) . . . . ?
C7 C8 C9 C12 -47(10) . . . . ?
A15 C8 C9 C12 -166(3) . . . . ?
Ag15 C8 C9 C12 -178(2) . . . . ?
C7 C8 C9 C10 80(9) . . . . ?
A15 C8 C9 C10 -40(3) . . . . ?
Ag15 C8 C9 C10 -52(3) . . . . ?
C7 C8 C9 C11 -169(9) . . . . ?
A15 C8 C9 C11 72(3) . . . . ?
Ag15 C8 C9 C11 60(3) . . . . ?
Ag22 C19 C20 Ag2C -98.2(15) . . . . ?
Ag3B C19 C20 Ag2B 81(2) . . . . ?
Ag22 C19 C20 Ag2B -88.7(10) . . . . ?
Ag3A C19 C20 Ag2A 96(3) . . . . ?
Ag22 C19 C20 Ag2A -92.7(11) . . . . ?
Ag2C C20 C21 C23 98(2) . . . . ?
Ag2B C20 C21 C23 87.8(17) . . . . ?
Ag2A C20 C21 C23 91.8(16) . . . . ?
Ag2C C20 C21 C24 -139.7(18) . . . . ?
Ag2B C20 C21 C24 -149.9(13) . . . . ?
Ag2A C20 C21 C24 -145.9(14) . . . . ?
Ag2C C20 C21 C22 -20(2) . . . . ?
Ag2B C20 C21 C22 -30.1(18) . . . . ?
Ag2A C20 C21 C22 -26.2(17) . . . . ?
C7 Ag4A C25 C26 -177(3) . . . . ?
Ag9 Ag4A C25 C26 107(4) . . . . ?
Ag21 Ag4A C25 C26 -147(4) . . . . ?
Ag6 Ag4A C25 C26 -154(3) . . . . ?
C7 Ag4A C25 Ag9 76(4) . . . . ?
Ag21 Ag4A C25 Ag9 106.4(6) . . . . ?
Ag6 Ag4A C25 Ag9 99.3(11) . . . . ?
C7 Ag4A C25 Ag21 -30(4) . . . . ?
Ag9 Ag4A C25 Ag21 -106.4(6) . . . . ?
Ag6 Ag4A C25 Ag21 -7.1(13) . . . . ?
Ag4A C25 C26 C27 13(11) . . . . ?
Ag9 C25 C26 C27 121(8) . . . . ?
Ag21 C25 C26 C27 -132(8) . . . . ?
Ag4A C25 C26 Ag9 -107(4) . . . . ?
Ag21 C25 C26 Ag9 107.7(8) . . . . ?
C25 C26 C27 C30 55(9) . . . . ?
Ag9 C26 C27 C30 168.6(18) . . . . ?
C25 C26 C27 C29 -72(9) . . . . ?
Ag9 C26 C27 C29 42(2) . . . . ?
C25 C26 C27 C28 174(8) . . . . ?
Ag9 C26 C27 C28 -72(2) . . . . ?
C19 Ag2A C37 C38 -116(3) . . . . ?
C20 Ag2A C37 C38 -56(4) . . . . ?
Ag5 Ag2A C37 C38 141.5(18) . . . . ?
Ag14 Ag2A C37 C38 -132.8(18) . . . . ?
C19 Ag2A C37 Ag5 102(2) . . . . ?
C20 Ag2A C37 Ag5 162(4) . . . . ?
Ag14 Ag2A C37 Ag5 85.7(4) . . . . ?
C19 Ag2A C37 Ag14 17(3) . . . . ?
C20 Ag2A C37 Ag14 77(4) . . . . ?
Ag5 Ag2A C37 Ag14 -85.7(4) . . . . ?
Ag1 C49 C50 C51 -159(5) . . . . ?
Ag14 C49 C50 C51 61(6) . . . . ?
Ag3B C49 C50 C51 -32(6) . . . . ?
Ag3A C49 C50 C51 -37(6) . . . . ?
C49 C50 C51 C52 5(7) . . . . ?
C49 C50 C51 C53 -110(5) . . . . ?
C49 C50 C51 C59 137(5) . . . . ?
Ag13 C67 C68 C69 -28(15) . . . . ?
Ag8 C67 C68 C69 130(10) . . . . ?
Ag11 C67 C68 C69 -134(10) . . . . ?
C67 C68 C69 C72 -39(11) . . . . ?
C67 C68 C69 C70 -160(10) . . . . ?
C67 C68 C69 C71 82(11) . . . . ?
Ag10 C73 C74 C75 -33(12) . . . . ?
Ag19 C73 C74 C75 -137(8) . . . . ?
Ag8 C73 C74 C75 113(8) . . . . ?
Ag10 C73 C74 Ag19 104(5) . . . . ?
Ag8 C73 C74 Ag19 -110.7(9) . . . . ?
C73 C74 C75 C77A -42(9) . . . . ?
Ag19 C74 C75 C77A -173(3) . . . . ?
C73 C74 C75 C76A 94(9) . . . . ?
Ag19 C74 C75 C76A -37(3) . . . . ?
C73 C74 C75 C76 153(8) . . . . ?
Ag19 C74 C75 C76 22(2) . . . . ?
C73 C74 C75 C77 -88(8) . . . . ?
Ag19 C74 C75 C77 141(2) . . . . ?
C73 C74 C75 C78 31(9) . . . . ?
Ag19 C74 C75 C78 -100(2) . . . . ?
C73 C74 C75 C78A -150(8) . . . . ?
Ag19 C74 C75 C78A 79(3) . . . . ?
Ag10 C85 C86 Ag12 -104(5) . . . . ?
Ag11 C85 C86 Ag12 106.0(9) . . . . ?
Ag12 C86 C87 C90 -92(2) . . . . ?
Ag12 C86 C87 C89 145.1(17) . . . . ?
Ag12 C86 C87 C88 24(2) . . . . ?
O10 C100 C101 C99 5(3) . . . . ?
C102 C100 C101 C99 -178.4(16) . . . . ?
O11 C99 C101 C100 -5(4) . . . . ?
C103 C99 C101 C100 177.6(18) . . . . ?
O10 C100 C102 F3 -175.8(16) . . . . ?
C101 C100 C102 F3 7(2) . . . . ?
O10 C100 C102 F2 61(2) . . . . ?
C101 C100 C102 F2 -116.6(18) . . . . ?
O10 C100 C102 F1 -57(2) . . . . ?
C101 C100 C102 F1 125.4(17) . . . . ?
O11 C99 C103 F4 -164.7(19) . . . . ?
C101 C99 C103 F4 13(3) . . . . ?
O11 C99 C103 F6 -39(3) . . . . ?
C101 C99 C103 F6 138.8(18) . . . . ?
O11 C99 C103 F5 74(2) . . . . ?
C101 C99 C103 F5 -109(2) . . . . ?
O12 C104 C105 F7B 16(4) . . . . ?
O13 C104 C105 F7B 178(3) . . . . ?
O12 C104 C105 F8B 142(3) . . . . ?
O13 C104 C105 F8B -56(3) . . . . ?
O12 C104 C105 F9 -171(4) . . . . ?
O13 C104 C105 F9 -9(3) . . . . ?
O12 C104 C105 F7 -43(4) . . . . ?
O13 C104 C105 F7 118(3) . . . . ?
O12 C104 C105 F9B -100(4) . . . . ?
O13 C104 C105 F9B 62(3) . . . . ?
O12 C104 C105 F8 72(4) . . . . ?
O13 C104 C105 F8 -126(3) . . . . ?
C101 C100 O10 Ag22 4(3) . . . . ?
C102 C100 O10 Ag22 -172.9(11) . . . . ?
C101 C99 O11 Ag22 -2(3) . . . . ?
C103 C99 O11 Ag22 174.5(12) . . . . ?
O12 C104 O13 Ag5 -16(4) . . . . ?
C105 C104 O13 Ag5 -178.7(13) . . . . ?
Ag9 O8 N1 O7 -83.5(12) . . . . ?
Ag1 O8 N1 O7 -177.6(10) . . . . ?
Ag19 O8 N1 O7 94.2(11) . . . . ?
Ag9 O8 N1 O9 93.1(11) . . . . ?
Ag1 O8 N1 O9 -1.0(11) . . . . ?
Ag19 O8 N1 O9 -89.1(11) . . . . ?
Ag15 O9 N1 O7 84.4(12) . . . . ?
Ag12 O9 N1 O7 -94.0(11) . . . . ?
Ag1 O9 N1 O7 177.6(10) . . . . ?
Ag15 O9 N1 O8 -92.3(11) . . . . ?
Ag12 O9 N1 O8 89.4(11) . . . . ?
Ag1 O9 N1 O8 0.9(11) . . . . ?
Ag20 O3 P1 O2 64.6(11) . . . . ?
Ag20 O3 P1 O1 -60.9(11) . . . . ?
Ag20 O3 P1 C95 -177.9(9) . . . . ?
Ag12 O2 P1 O3 -26.7(7) . . . . ?
Ag14 O2 P1 O3 -155.5(6) . . . . ?
Ag12 O2 P1 O1 98.9(6) . . . . ?
Ag14 O2 P1 O1 -29.9(9) . . . . ?
Ag12 O2 P1 C95 -143.8(6) . . . . ?
Ag14 O2 P1 C95 87.4(8) . . . . ?
Ag15 O1 P1 O3 28.6(7) . . . . ?
Ag18 O1 P1 O3 152.7(6) . . . . ?
A15 O1 P1 O3 31.4(10) . . . . ?
Ag15 O1 P1 O2 -97.1(6) . . . . ?
Ag18 O1 P1 O2 26.9(8) . . . . ?
A15 O1 P1 O2 -94.4(9) . . . . ?
Ag15 O1 P1 C95 145.4(6) . . . . ?
Ag18 O1 P1 C95 -90.6(7) . . . . ?
A15 O1 P1 C95 148.1(9) . . . . ?
C96 C95 P1 O3 177.1(11) . . . . ?
C98 C95 P1 O3 59.3(11) . . . . ?
C97 C95 P1 O3 -60.8(12) . . . . ?
C96 C95 P1 O2 -62.6(13) . . . . ?
C98 C95 P1 O2 179.6(10) . . . . ?
C97 C95 P1 O2 59.4(11) . . . . ?
C96 C95 P1 O1 57.4(13) . . . . ?
C98 C95 P1 O1 -60.5(11) . . . . ?
C97 C95 P1 O1 179.4(10) . . . . ?
Ag7 O6 P2 O4 -58.2(11) . . . . ?
Ag7 O6 P2 O5 67.4(11) . . . . ?
Ag7 O6 P2 C91 -176.0(9) . . . . ?
Ag3A O4 P2 O6 168.2(10) . . . . ?
Ag19 O4 P2 O6 24.7(7) . . . . ?
Ag3B O4 P2 O6 157.5(7) . . . . ?
Ag3A O4 P2 O5 42.9(11) . . . . ?
Ag19 O4 P2 O5 -100.7(6) . . . . ?
Ag3B O4 P2 O5 32.2(9) . . . . ?
Ag3A O4 P2 C91 -74.9(11) . . . . ?
Ag19 O4 P2 C91 141.5(6) . . . . ?
Ag3B O4 P2 C91 -85.6(9) . . . . ?
Ag9 O5 P2 O6 -26.7(7) . . . . ?
Ag16 O5 P2 O6 -156.4(6) . . . . ?
Ag9 O5 P2 O4 99.2(5) . . . . ?
Ag16 O5 P2 O4 -30.5(7) . . . . ?
Ag9 O5 P2 C91 -142.8(6) . . . . ?
Ag16 O5 P2 C91 87.5(7) . . . . ?
C94 C91 P2 O6 178.9(11) . . . . ?
C93 C91 P2 O6 -61.5(12) . . . . ?
C92 C91 P2 O6 58.2(12) . . . . ?
C94 C91 P2 O4 58.4(12) . . . . ?
C93 C91 P2 O4 177.9(10) . . . . ?
C92 C91 P2 O4 -62.3(12) . . . . ?
C94 C91 P2 O5 -62.0(12) . . . . ?
C93 C91 P2 O5 57.6(12) . . . . ?
C92 C91 P2 O5 177.3(11) . . . . ?

_refine_diff_density_max         2.142
_refine_diff_density_min         -1.778
_refine_diff_density_rms         0.217

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex8
_database_code_depnum_ccdc_archive 'CCDC 1584348'
_audit_update_record             
;
2017-11-07 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C172 H242 Ag40 F30 O33 P4 V2'
_chemical_formula_weight         7948.20

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
V V 0.3005 0.5294 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 21/c'
_space_group_name_Hall           '-P 2ybc'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   22.419(4)
_cell_length_b                   19.817(3)
_cell_length_c                   27.289(4)
_cell_angle_alpha                90
_cell_angle_beta                 106.543(4)
_cell_angle_gamma                90
_cell_volume                     11622(3)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9170
_cell_measurement_theta_min      3.0077
_cell_measurement_theta_max      26.3635

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.271
_exptl_crystal_F_000             7588
_exptl_transmission_factor_min   0.3978
_exptl_transmission_factor_max   0.7454
_exptl_crystal_size_max          0.084
_exptl_crystal_size_mid          0.063
_exptl_crystal_size_min          0.045
_exptl_absorpt_coefficient_mu    3.462
_shelx_estimated_absorpt_T_min   0.760
_shelx_estimated_absorpt_T_max   0.860
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            56142
_diffrn_reflns_av_unetI/netI     0.0591
_diffrn_reflns_av_R_equivalents  0.0590
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_theta_min         2.897
_diffrn_reflns_theta_max         23.256
_diffrn_reflns_theta_full        23.256
_diffrn_measured_fraction_theta_max 0.973
_diffrn_measured_fraction_theta_full 0.973
_diffrn_reflns_Laue_measured_fraction_max 0.973
_diffrn_reflns_Laue_measured_fraction_full 0.973
_diffrn_reflns_point_group_measured_fraction_max 0.973
_diffrn_reflns_point_group_measured_fraction_full 0.973
_reflns_number_total             16257
_reflns_number_gt                12247
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+1217.8906P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         16257
_refine_ls_number_parameters     1257
_refine_ls_number_restraints     644
_refine_ls_R_factor_all          0.1321
_refine_ls_R_factor_gt           0.1009
_refine_ls_wR_factor_ref         0.2440
_refine_ls_wR_factor_gt          0.2223
_refine_ls_goodness_of_fit_ref   1.090
_refine_ls_restrained_S_all      1.071
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.59553(9) -0.20260(11) 0.58924(10) 0.0558(6) Uani 1 1 d . . . . .
Ag2 Ag 0.47265(10) -0.15597(11) 0.59822(10) 0.0571(6) Uani 1 1 d . . . . .
Ag3 Ag 0.42606(8) -0.00896(9) 0.59005(7) 0.0355(4) Uani 1 1 d . . . . .
Ag4 Ag 0.16188(11) 0.24546(11) 0.35020(9) 0.0593(6) Uani 1 1 d . . . . .
Ag5 Ag 0.17213(8) 0.08147(10) 0.34851(8) 0.0443(5) Uani 1 1 d . . . . .
Ag6 Ag 0.67856(8) -0.04412(9) 0.64622(7) 0.0364(4) Uani 1 1 d . . . . .
Ag7 Ag 0.16910(11) 0.35899(15) 0.43488(10) 0.0700(7) Uani 1 1 d . . . . .
Ag8 Ag 0.14803(9) 0.04735(11) 0.45229(8) 0.0490(5) Uani 1 1 d . . . . .
Ag9 Ag 0.48541(9) -0.14450(11) 0.40927(8) 0.0504(5) Uani 1 1 d . . . . .
Ag10 Ag 0.37938(8) 0.12153(9) 0.55786(7) 0.0376(4) Uani 1 1 d . . . . .
Ag11 Ag 0.28882(8) 0.12574(9) 0.44342(6) 0.0325(4) Uani 1 1 d . . . . .
Ag12 Ag 0.31089(8) -0.01031(9) 0.50683(7) 0.0368(4) Uani 1 1 d . . . . .
Ag13 Ag 0.05653(8) 0.11690(10) 0.36887(7) 0.0437(5) Uani 1 1 d . . . . .
Ag14 Ag 0.39136(10) -0.12446(10) 0.48630(8) 0.0497(5) Uani 1 1 d . . . . .
Ag15 Ag 0.55842(8) 0.01732(10) 0.66023(7) 0.0421(5) Uani 1 1 d . . . . .
Ag16 Ag 0.48764(10) -0.22698(11) 0.49841(8) 0.0503(5) Uani 1 1 d . . . . .
Ag17 Ag 0.35431(8) -0.09852(9) 0.37566(7) 0.0392(4) Uani 1 1 d . . . . .
Ag18 Ag 0.11471(9) 0.20555(11) 0.46024(9) 0.0526(5) Uani 1 1 d . . . . .
Ag19 Ag 0.24394(9) 0.22293(11) 0.50858(8) 0.0489(5) Uani 1 1 d . . . . .
Ag20 Ag 0.28843(12) 0.28661(16) 0.42255(10) 0.0788(8) Uani 1 1 d . . . . .
V1 V 0.44158(17) 0.04886(19) 0.46197(15) 0.0320(9) Uani 1 1 d . . . . .
C1 C 0.5097(12) -0.2507(13) 0.5823(11) 0.047(6) Uani 1 1 d . U . . .
C2 C 0.4882(12) -0.3087(13) 0.5771(10) 0.045(5) Uani 1 1 d . U . . .
C3 C 0.4683(14) -0.3831(13) 0.5739(10) 0.054(5) Uani 1 1 d . U . . .
C4 C 0.4246(17) -0.3928(15) 0.6077(13) 0.074(8) Uani 1 1 d . U . . .
H4A H 0.3871 -0.3653 0.5944 0.111 Uiso 1 1 calc R U . . .
H4B H 0.4128 -0.4405 0.6075 0.111 Uiso 1 1 calc R U . . .
H4C H 0.4459 -0.3789 0.6428 0.111 Uiso 1 1 calc R U . . .
C5 C 0.4334(19) -0.3992(18) 0.5180(12) 0.090(11) Uani 1 1 d . U . . .
H5A H 0.3956 -0.3717 0.5073 0.135 Uiso 1 1 calc R U . . .
H5B H 0.4602 -0.3890 0.4962 0.135 Uiso 1 1 calc R U . . .
H5C H 0.4221 -0.4471 0.5149 0.135 Uiso 1 1 calc R U . . .
C6 C 0.5268(16) -0.4241(16) 0.5922(16) 0.085(10) Uani 1 1 d . U . . .
H6A H 0.5532 -0.4164 0.5696 0.127 Uiso 1 1 calc R U . . .
H6B H 0.5492 -0.4106 0.6271 0.127 Uiso 1 1 calc R U . . .
H6C H 0.5161 -0.4721 0.5918 0.127 Uiso 1 1 calc R U . . .
C7 C 0.0784(13) 0.1909(14) 0.2811(10) 0.054(6) Uani 1 1 d . U . . .
C8 C 0.1103(11) 0.1533(13) 0.3152(10) 0.047(6) Uani 1 1 d . U . . .
C9 C 0.0369(15) 0.2270(17) 0.2388(11) 0.068(7) Uani 1 1 d . U . . .
C10 C -0.0143(16) 0.176(2) 0.2096(14) 0.099(11) Uani 1 1 d . U . . .
H10A H -0.0432 0.1992 0.1806 0.149 Uiso 1 1 calc R U . . .
H10B H 0.0054 0.1384 0.1970 0.149 Uiso 1 1 calc R U . . .
H10C H -0.0371 0.1592 0.2327 0.149 Uiso 1 1 calc R U . . .
C11 C 0.0045(19) 0.2882(18) 0.2593(13) 0.088(10) Uani 1 1 d . U . . .
H11A H -0.0233 0.3121 0.2303 0.132 Uiso 1 1 calc R U . . .
H11B H -0.0195 0.2708 0.2815 0.132 Uiso 1 1 calc R U . . .
H11C H 0.0365 0.3194 0.2788 0.132 Uiso 1 1 calc R U . . .
C12 C 0.0758(18) 0.2539(18) 0.2050(12) 0.085(9) Uani 1 1 d . U . . .
H12A H 0.0487 0.2786 0.1760 0.127 Uiso 1 1 calc R U . . .
H12B H 0.1081 0.2842 0.2250 0.127 Uiso 1 1 calc R U . . .
H12C H 0.0952 0.2160 0.1923 0.127 Uiso 1 1 calc R U . . .
C13 C 0.1689(12) 0.2890(13) 0.5004(11) 0.051(6) Uani 1 1 d . U . . .
C14 C 0.1448(11) 0.3314(13) 0.5221(10) 0.046(5) Uani 1 1 d . U . . .
C15 C 0.1150(15) 0.3782(16) 0.5521(13) 0.065(6) Uani 1 1 d . U . . .
C16 C 0.1026(18) 0.337(2) 0.5931(14) 0.092(10) Uani 1 1 d . U . . .
H16A H 0.0831 0.3645 0.6138 0.137 Uiso 1 1 calc R U . . .
H16B H 0.0746 0.2994 0.5778 0.137 Uiso 1 1 calc R U . . .
H16C H 0.1418 0.3182 0.6147 0.137 Uiso 1 1 calc R U . . .
C17 C 0.0532(13) 0.4067(17) 0.5134(13) 0.071(8) Uani 1 1 d . U . . .
H17A H 0.0638 0.4338 0.4871 0.106 Uiso 1 1 calc R U . . .
H17B H 0.0265 0.3690 0.4973 0.106 Uiso 1 1 calc R U . . .
H17C H 0.0310 0.4349 0.5321 0.106 Uiso 1 1 calc R U . . .
C18 C 0.1597(17) 0.4370(19) 0.5714(15) 0.089(10) Uani 1 1 d . U . . .
H18A H 0.1656 0.4621 0.5422 0.134 Uiso 1 1 calc R U . . .
H18B H 0.1423 0.4671 0.5923 0.134 Uiso 1 1 calc R U . . .
H18C H 0.1999 0.4195 0.5921 0.134 Uiso 1 1 calc R U . . .
C19 C 0.2692(11) 0.1004(12) 0.5107(9) 0.036(5) Uani 1 1 d . U . . .
C20 C 0.2607(11) 0.0896(13) 0.5532(8) 0.043(5) Uani 1 1 d D U . . .
C21 C 0.2413(9) 0.0776(10) 0.6013(7) 0.038(5) Uani 1 1 d D U . . .
C22A C 0.2922(15) 0.0408(18) 0.6413(14) 0.062(12) Uiso 0.68(3) 1 d D U P A 1
H22A H 0.2788 0.0336 0.6720 0.093 Uiso 0.68(3) 1 calc R U P A 1
H22B H 0.3004 -0.0028 0.6276 0.093 Uiso 0.68(3) 1 calc R U P A 1
H22C H 0.3303 0.0680 0.6499 0.093 Uiso 0.68(3) 1 calc R U P A 1
C23A C 0.1807(12) 0.0370(17) 0.5873(15) 0.053(11) Uiso 0.68(3) 1 d D U P A 1
H23A H 0.1676 0.0289 0.6181 0.079 Uiso 0.68(3) 1 calc R U P A 1
H23B H 0.1483 0.0623 0.5624 0.079 Uiso 0.68(3) 1 calc R U P A 1
H23C H 0.1875 -0.0063 0.5723 0.079 Uiso 0.68(3) 1 calc R U P A 1
C24A C 0.230(2) 0.1478(17) 0.621(2) 0.111(19) Uiso 0.68(3) 1 d D U P A 1
H24A H 0.2172 0.1429 0.6524 0.166 Uiso 0.68(3) 1 calc R U P A 1
H24B H 0.2683 0.1744 0.6284 0.166 Uiso 0.68(3) 1 calc R U P A 1
H24C H 0.1970 0.1710 0.5950 0.166 Uiso 0.68(3) 1 calc R U P A 1
C22B C 0.237(3) 0.0021(17) 0.611(3) 0.07(2) Uiso 0.32(3) 1 d D U P A 2
H22D H 0.2239 -0.0049 0.6417 0.101 Uiso 0.32(3) 1 calc R U P A 2
H22E H 0.2055 -0.0181 0.5814 0.101 Uiso 0.32(3) 1 calc R U P A 2
H22F H 0.2771 -0.0192 0.6144 0.101 Uiso 0.32(3) 1 calc R U P A 2
C23B C 0.178(2) 0.111(4) 0.598(4) 0.08(2) Uiso 0.32(3) 1 d D U P A 2
H23D H 0.1669 0.1027 0.6293 0.120 Uiso 0.32(3) 1 calc R U P A 2
H23E H 0.1815 0.1600 0.5930 0.120 Uiso 0.32(3) 1 calc R U P A 2
H23F H 0.1463 0.0924 0.5686 0.120 Uiso 0.32(3) 1 calc R U P A 2
C24B C 0.291(3) 0.109(4) 0.647(3) 0.07(2) Uiso 0.32(3) 1 d D U P A 2
H24D H 0.2785 0.1013 0.6784 0.112 Uiso 0.32(3) 1 calc R U P A 2
H24E H 0.3310 0.0874 0.6503 0.112 Uiso 0.32(3) 1 calc R U P A 2
H24F H 0.2938 0.1573 0.6414 0.112 Uiso 0.32(3) 1 calc R U P A 2
C25 C 0.3712(10) -0.0957(12) 0.5587(9) 0.035(5) Uani 1 1 d . U . . .
C26 C 0.3392(11) -0.1440(13) 0.5615(9) 0.041(5) Uani 1 1 d . U . . .
C27 C 0.2994(12) -0.1986(16) 0.5669(12) 0.060(6) Uani 1 1 d . U . . .
C28 C 0.2988(13) -0.2510(15) 0.5262(15) 0.074(8) Uani 1 1 d . U . . .
H28A H 0.2718 -0.2887 0.5294 0.112 Uiso 1 1 calc R U . . .
H28B H 0.2830 -0.2305 0.4923 0.112 Uiso 1 1 calc R U . . .
H28C H 0.3412 -0.2677 0.5307 0.112 Uiso 1 1 calc R U . . .
C29 C 0.3269(16) -0.228(2) 0.6219(15) 0.096(11) Uani 1 1 d . U . . .
H29A H 0.3010 -0.2652 0.6272 0.144 Uiso 1 1 calc R U . . .
H29B H 0.3694 -0.2438 0.6259 0.144 Uiso 1 1 calc R U . . .
H29C H 0.3276 -0.1922 0.6471 0.144 Uiso 1 1 calc R U . . .
C30 C 0.2323(13) -0.1713(19) 0.5565(15) 0.083(10) Uani 1 1 d . U . . .
H30A H 0.2046 -0.2080 0.5601 0.124 Uiso 1 1 calc R U . . .
H30B H 0.2316 -0.1355 0.5811 0.124 Uiso 1 1 calc R U . . .
H30C H 0.2184 -0.1530 0.5217 0.124 Uiso 1 1 calc R U . . .
C31 C 0.0721(11) 0.1033(11) 0.4528(10) 0.041(5) Uani 1 1 d . U . . .
C32 C 0.0317(10) 0.1196(13) 0.4717(9) 0.040(5) Uani 1 1 d . U . . .
C33 C -0.0204(12) 0.1364(14) 0.4977(12) 0.054(5) Uani 1 1 d . U . . .
C34 C -0.0453(15) 0.2048(16) 0.4849(17) 0.092(11) Uani 1 1 d . U . . .
H34A H -0.0640 0.2085 0.4479 0.138 Uiso 1 1 calc R U . . .
H34B H -0.0770 0.2139 0.5024 0.138 Uiso 1 1 calc R U . . .
H34C H -0.0115 0.2378 0.4959 0.138 Uiso 1 1 calc R U . . .
C35 C -0.0700(13) 0.0837(16) 0.4784(13) 0.068(8) Uani 1 1 d . U . . .
H35A H -0.0520 0.0387 0.4874 0.101 Uiso 1 1 calc R U . . .
H35B H -0.1038 0.0907 0.4940 0.101 Uiso 1 1 calc R U . . .
H35C H -0.0864 0.0873 0.4411 0.101 Uiso 1 1 calc R U . . .
C36 C 0.0077(15) 0.133(3) 0.5546(13) 0.105(12) Uani 1 1 d . U . . .
H36A H 0.0247 0.0877 0.5642 0.158 Uiso 1 1 calc R U . . .
H36B H 0.0412 0.1664 0.5651 0.158 Uiso 1 1 calc R U . . .
H36C H -0.0243 0.1426 0.5716 0.158 Uiso 1 1 calc R U . . .
C37 C 0.4569(10) 0.0823(13) 0.6300(8) 0.035(5) Uani 1 1 d . U . . .
C38 C 0.4709(9) 0.1151(10) 0.6663(7) 0.034(5) Uani 1 1 d D U . . .
C39 C 0.4825(9) 0.1547(11) 0.7161(8) 0.058(6) Uani 1 1 d D U . . .
C40 C 0.5528(10) 0.1529(17) 0.7451(12) 0.100(12) Uani 1 1 d D U . . .
H40A H 0.5765 0.1736 0.7240 0.150 Uiso 1 1 calc R U . . .
H40B H 0.5601 0.1779 0.7773 0.150 Uiso 1 1 calc R U . . .
H40C H 0.5661 0.1059 0.7525 0.150 Uiso 1 1 calc R U . . .
C41 C 0.4446(14) 0.1227(15) 0.7483(11) 0.084(9) Uani 1 1 d D U . . .
H41A H 0.4516 0.1476 0.7805 0.126 Uiso 1 1 calc R U . . .
H41B H 0.4003 0.1242 0.7295 0.126 Uiso 1 1 calc R U . . .
H41C H 0.4575 0.0756 0.7556 0.126 Uiso 1 1 calc R U . . .
C42 C 0.4624(15) 0.2278(11) 0.7020(13) 0.099(11) Uani 1 1 d D U . . .
H42A H 0.4875 0.2469 0.6814 0.149 Uiso 1 1 calc R U . . .
H42B H 0.4184 0.2287 0.6824 0.149 Uiso 1 1 calc R U . . .
H42C H 0.4684 0.2545 0.7333 0.149 Uiso 1 1 calc R U . . .
C43 C 0.6960(10) -0.1559(11) 0.6255(8) 0.032(5) Uani 1 1 d D U . . .
C44 C 0.6866(11) -0.1691(11) 0.6650(8) 0.040(5) Uani 1 1 d D U . . .
C45 C 0.6883(9) -0.1922(11) 0.7189(8) 0.058(6) Uani 1 1 d D U . . .
C46 C 0.6837(13) -0.2687(11) 0.7178(12) 0.078(8) Uani 1 1 d D U . . .
H46A H 0.6441 -0.2824 0.6939 0.117 Uiso 1 1 calc R U . . .
H46B H 0.7181 -0.2876 0.7068 0.117 Uiso 1 1 calc R U . . .
H46C H 0.6860 -0.2854 0.7521 0.117 Uiso 1 1 calc R U . . .
C47 C 0.7491(10) -0.1668(15) 0.7554(11) 0.079(9) Uani 1 1 d D U . . .
H47A H 0.7498 -0.1174 0.7548 0.118 Uiso 1 1 calc R U . . .
H47B H 0.7521 -0.1823 0.7902 0.118 Uiso 1 1 calc R U . . .
H47C H 0.7843 -0.1846 0.7448 0.118 Uiso 1 1 calc R U . . .
C48 C 0.6314(11) -0.1592(14) 0.7300(12) 0.077(9) Uani 1 1 d D U . . .
H48A H 0.6361 -0.1100 0.7304 0.115 Uiso 1 1 calc R U . . .
H48B H 0.5936 -0.1720 0.7034 0.115 Uiso 1 1 calc R U . . .
H48C H 0.6283 -0.1745 0.7634 0.115 Uiso 1 1 calc R U . . .
C49 C 0.4032(10) -0.1896(11) 0.4270(10) 0.036(5) Uani 1 1 d . U . . .
C50 C 0.3800(11) -0.2359(11) 0.3980(10) 0.042(5) Uani 1 1 d . U . . .
C51 C 0.3470(12) -0.2908(13) 0.3669(11) 0.050(5) Uani 1 1 d . U . . .
C52 C 0.3931(15) -0.3507(14) 0.3705(11) 0.063(7) Uani 1 1 d . U . . .
H52A H 0.3714 -0.3883 0.3496 0.094 Uiso 1 1 calc R U . . .
H52B H 0.4279 -0.3361 0.3580 0.094 Uiso 1 1 calc R U . . .
H52C H 0.4089 -0.3653 0.4062 0.094 Uiso 1 1 calc R U . . .
C53 C 0.2897(14) -0.3113(16) 0.3823(14) 0.072(8) Uani 1 1 d . U . . .
H53A H 0.2686 -0.3485 0.3605 0.109 Uiso 1 1 calc R U . . .
H53B H 0.3021 -0.3260 0.4181 0.109 Uiso 1 1 calc R U . . .
H53C H 0.2614 -0.2727 0.3783 0.109 Uiso 1 1 calc R U . . .
C54 C 0.3234(17) -0.2640(18) 0.3113(11) 0.078(9) Uani 1 1 d . U . . .
H54A H 0.3007 -0.2999 0.2889 0.117 Uiso 1 1 calc R U . . .
H54B H 0.2956 -0.2255 0.3102 0.117 Uiso 1 1 calc R U . . .
H54C H 0.3589 -0.2497 0.2997 0.117 Uiso 1 1 calc R U . . .
C55 C 0.2100(12) 0.3381(12) 0.3681(10) 0.047(6) Uani 1 1 d . U . . .
C56 C 0.2366(14) 0.3892(14) 0.3654(12) 0.057(6) Uani 1 1 d . U . . .
C57 C 0.2616(17) 0.4567(17) 0.3561(14) 0.078(7) Uani 1 1 d . U . . .
C58 C 0.213(2) 0.5042(15) 0.3327(14) 0.093(10) Uani 1 1 d . U . . .
H58A H 0.2318 0.5473 0.3275 0.139 Uiso 1 1 calc R U . . .
H58B H 0.1882 0.4865 0.2997 0.139 Uiso 1 1 calc R U . . .
H58C H 0.1862 0.5111 0.3550 0.139 Uiso 1 1 calc R U . . .
C59 C 0.3017(19) 0.4446(18) 0.3176(15) 0.092(10) Uani 1 1 d . U . . .
H59A H 0.3352 0.4125 0.3326 0.139 Uiso 1 1 calc R U . . .
H59B H 0.2751 0.4264 0.2854 0.139 Uiso 1 1 calc R U . . .
H59C H 0.3198 0.4875 0.3110 0.139 Uiso 1 1 calc R U . . .
C60 C 0.3050(18) 0.480(2) 0.4084(15) 0.098(11) Uani 1 1 d . U . . .
H60A H 0.3366 0.4458 0.4220 0.148 Uiso 1 1 calc R U . . .
H60B H 0.3254 0.5227 0.4037 0.148 Uiso 1 1 calc R U . . .
H60C H 0.2804 0.4875 0.4324 0.148 Uiso 1 1 calc R U . . .
C61 C 0.1565(11) -0.1149(15) 0.3690(10) 0.048(5) Uani 1 1 d . U . . .
C62 C 0.1723(12) -0.1409(16) 0.3202(11) 0.061(7) Uani 1 1 d . U . . .
H62A H 0.2106 -0.1679 0.3303 0.092 Uiso 1 1 calc R U . . .
H62B H 0.1380 -0.1689 0.3000 0.092 Uiso 1 1 calc R U . . .
H62C H 0.1784 -0.1024 0.2996 0.092 Uiso 1 1 calc R U . . .
C63 C 0.1490(13) -0.1748(13) 0.4025(13) 0.060(7) Uani 1 1 d . U . . .
H63A H 0.1877 -0.2008 0.4125 0.090 Uiso 1 1 calc R U . . .
H63B H 0.1394 -0.1580 0.4331 0.090 Uiso 1 1 calc R U . . .
H63C H 0.1150 -0.2038 0.3831 0.090 Uiso 1 1 calc R U . . .
C64 C 0.0969(10) -0.0732(15) 0.3526(10) 0.053(6) Uani 1 1 d . U . . .
H64A H 0.1029 -0.0353 0.3314 0.079 Uiso 1 1 calc R U . . .
H64B H 0.0626 -0.1016 0.3330 0.079 Uiso 1 1 calc R U . . .
H64C H 0.0870 -0.0557 0.3830 0.079 Uiso 1 1 calc R U . . .
C65 C 0.3823(11) 0.3628(14) 0.5630(11) 0.052(6) Uani 1 1 d . U . . .
C66 C 0.3178(13) 0.3918(16) 0.5376(13) 0.068(8) Uani 1 1 d . U . . .
H66A H 0.3098 0.3908 0.5004 0.101 Uiso 1 1 calc R U . . .
H66B H 0.2863 0.3647 0.5472 0.101 Uiso 1 1 calc R U . . .
H66C H 0.3159 0.4385 0.5489 0.101 Uiso 1 1 calc R U . . .
C67 C 0.4301(14) 0.4074(17) 0.5490(17) 0.088(10) Uani 1 1 d . U . . .
H67A H 0.4204 0.4103 0.5117 0.132 Uiso 1 1 calc R U . . .
H67B H 0.4290 0.4526 0.5632 0.132 Uiso 1 1 calc R U . . .
H67C H 0.4716 0.3879 0.5630 0.132 Uiso 1 1 calc R U . . .
C68 C 0.401(2) 0.361(2) 0.6205(14) 0.106(12) Uani 1 1 d . U . . .
H68A H 0.3714 0.3331 0.6319 0.158 Uiso 1 1 calc R U . . .
H68B H 0.4428 0.3425 0.6333 0.158 Uiso 1 1 calc R U . . .
H68C H 0.4002 0.4073 0.6336 0.158 Uiso 1 1 calc R U . . .
C69 C -0.0947(13) 0.1514(17) 0.3233(11) 0.058(6) Uani 1 1 d . U . . .
C70 C -0.1149(12) 0.0797(16) 0.3105(10) 0.054(6) Uani 1 1 d . U . . .
H70 H -0.1580 0.0691 0.2995 0.065 Uiso 1 1 calc R U . . .
C71 C -0.0710(11) 0.0285(15) 0.3148(10) 0.051(6) Uani 1 1 d . U . . .
C72 C -0.1515(16) 0.199(2) 0.3101(14) 0.073(8) Uani 1 1 d . U . . .
C73 C -0.0962(12) -0.0421(17) 0.2999(11) 0.058(7) Uani 1 1 d . U . . .
C74 C 0.0447(14) 0.4567(17) 0.3779(13) 0.065(7) Uani 1 1 d . U . . .
C75 C 0.0681(18) 0.519(2) 0.3991(16) 0.089(9) Uani 1 1 d . U . . .
H75 H 0.0437 0.5589 0.3901 0.107 Uiso 1 1 calc R U . . .
C76 C 0.129(2) 0.523(2) 0.434(2) 0.107(11) Uani 1 1 d . U . . .
C78 C 0.1470(15) 0.5942(19) 0.4562(14) 0.117(14) Uani 1 1 d D U . . .
C77 C -0.0158(13) 0.4613(13) 0.3454(12) 0.090(10) Uani 1 1 d D U . . .
C79 C 0.6604(11) 0.0422(13) 0.6950(8) 0.038(5) Uani 1 1 d . U . . .
C80 C 0.6904(11) 0.0479(14) 0.7355(9) 0.043(5) Uani 1 1 d . U . . .
C81 C 0.7279(13) 0.0588(15) 0.7898(10) 0.053(5) Uani 1 1 d . U . . .
C82 C 0.730(2) 0.1332(18) 0.8030(13) 0.099(12) Uani 1 1 d . U . . .
H82A H 0.7545 0.1397 0.8386 0.149 Uiso 1 1 calc R U . . .
H82B H 0.7489 0.1584 0.7805 0.149 Uiso 1 1 calc R U . . .
H82C H 0.6874 0.1497 0.7986 0.149 Uiso 1 1 calc R U . . .
C83 C 0.7947(14) 0.034(2) 0.7992(13) 0.082(9) Uani 1 1 d . U . . .
H83A H 0.8179 0.0421 0.8350 0.123 Uiso 1 1 calc R U . . .
H83B H 0.7945 -0.0142 0.7917 0.123 Uiso 1 1 calc R U . . .
H83C H 0.8145 0.0588 0.7769 0.123 Uiso 1 1 calc R U . . .
C84 C 0.6968(15) 0.019(2) 0.8252(11) 0.081(9) Uani 1 1 d . U . . .
H84A H 0.7209 0.0260 0.8610 0.121 Uiso 1 1 calc R U . . .
H84B H 0.6543 0.0359 0.8201 0.121 Uiso 1 1 calc R U . . .
H84C H 0.6957 -0.0289 0.8169 0.121 Uiso 1 1 calc R U . . .
C85 C 0.4764(17) -0.085(3) 0.7080(15) 0.090(11) Uani 1 1 d D U . . .
C86 C 0.4404(12) -0.0905(13) 0.7474(10) 0.103(12) Uani 1 1 d D U . . .
O1 O 0.2275(7) -0.0036(9) 0.3693(7) 0.044(4) Uani 1 1 d . . . . .
O2 O 0.2075(8) -0.0373(8) 0.4537(6) 0.043(4) Uani 1 1 d . . . . .
O3 O 0.2792(7) -0.1078(8) 0.4176(7) 0.042(4) Uani 1 1 d . . . . .
O4 O 0.3456(8) 0.2315(8) 0.5545(8) 0.056(5) Uani 1 1 d . . . . .
O5 O 0.4587(7) 0.2541(9) 0.5596(7) 0.049(5) Uani 1 1 d . . . . .
O6 O 0.3733(8) 0.2819(11) 0.4792(8) 0.068(6) Uani 1 1 d . . . . .
O7 O 0.0687(9) 0.4009(10) 0.3841(8) 0.061(5) Uani 1 1 d . . . . .
O8 O 0.1703(12) 0.4808(13) 0.4519(9) 0.085(8) Uani 1 1 d . . . . .
O9 O -0.0453(9) 0.1745(10) 0.3407(9) 0.073(5) Uani 1 1 d . . . . .
O10 O -0.0165(9) 0.0318(10) 0.3297(9) 0.073(5) Uani 1 1 d . . . . .
O11 O 0.5103(17) -0.0370(17) 0.7155(15) 0.133(14) Uani 1 1 d . . . . .
O12 O 0.4644(15) -0.131(3) 0.6786(11) 0.18(2) Uani 1 1 d . . . . .
O13 O 0.4584(9) 0.0657(9) 0.4076(8) 0.061(5) Uani 1 1 d . . . . .
O14 O 0.4345(11) 0.1223(11) 0.4903(9) 0.083(8) Uani 1 1 d . . . . .
O15 O 0.3747(8) 0.0090(11) 0.4483(7) 0.066(6) Uani 1 1 d . . . . .
O16 O 0.486(2) -0.0225(18) 0.4979(18) 0.075(14) Uani 0.5 1 d . . P B -1
P1 P 0.2212(2) -0.0623(3) 0.4047(2) 0.0310(13) Uani 1 1 d . . . . .
P2 P 0.3905(3) 0.2779(3) 0.5374(3) 0.0400(15) Uani 1 1 d . . . . .
F1 F 0.1568(17) 0.5968(19) 0.5070(13) 0.177(13) Uiso 1 1 d D . . . .
F2 F 0.1069(19) 0.6433(15) 0.4373(16) 0.33(4) Uani 1 1 d D . . . .
F3 F 0.2004(18) 0.6114(16) 0.4485(17) 0.25(3) Uani 1 1 d D . . . .
F4 F -0.0231(16) 0.453(2) 0.2953(12) 0.28(3) Uani 1 1 d D . . . .
F5 F -0.0518(12) 0.5148(10) 0.3420(11) 0.151(12) Uani 1 1 d D . . . .
F6 F -0.0556(12) 0.4141(13) 0.3503(18) 0.26(3) Uani 1 1 d D . . . .
F7 F -0.1562(15) 0.2331(18) 0.2742(14) 0.20(2) Uani 1 1 d . . . . .
F8 F -0.2056(11) 0.1734(15) 0.3107(13) 0.146(12) Uani 1 1 d . . . . .
F9 F -0.1441(16) 0.2420(18) 0.3498(13) 0.184(17) Uani 1 1 d . . . . .
F10 F -0.1560(8) -0.0499(10) 0.2900(7) 0.076(5) Uani 1 1 d . . . . .
F11 F -0.0801(9) -0.0633(10) 0.2593(8) 0.086(6) Uani 1 1 d . . . . .
F12 F -0.0686(12) -0.0848(11) 0.3379(8) 0.108(8) Uani 1 1 d . . . . .
F13 F 0.3875(10) -0.0571(15) 0.7337(9) 0.148(13) Uani 1 1 d D . . . .
F14 F 0.4231(15) -0.1522(11) 0.7566(10) 0.169(15) Uani 1 1 d D . . . .
F15 F 0.4677(13) -0.0672(14) 0.7939(9) 0.152(12) Uani 1 1 d D . . . .
O1W O 0.0352(10) 0.2714(10) 0.3969(9) 0.084(8) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C1 2.11(3) . ?
Ag1 C43 2.38(2) . ?
Ag1 C44 2.55(2) . ?
Ag1 Ag16 2.969(3) . ?
Ag1 Ag2 2.981(3) . ?
Ag1 Ag20 3.181(3) 3_656 ?
Ag1 Ag11 3.340(3) 3_656 ?
Ag2 C1 2.15(2) . ?
Ag2 O12 2.31(3) . ?
Ag2 O13 2.399(17) 3_656 ?
Ag2 C25 2.52(2) . ?
Ag2 Ag3 3.081(3) . ?
Ag2 Ag14 3.142(3) . ?
Ag2 Ag16 3.167(3) . ?
Ag3 C37 2.12(2) . ?
Ag3 C25 2.15(2) . ?
Ag3 Ag10 2.834(3) . ?
Ag3 Ag12 2.913(2) . ?
Ag3 Ag15 3.084(2) . ?
Ag4 C55 2.11(3) . ?
Ag4 C8 2.23(2) . ?
Ag4 C7 2.49(3) . ?
Ag4 Ag20 3.070(4) . ?
Ag4 Ag7 3.196(4) . ?
Ag4 Ag5 3.259(3) . ?
Ag5 C8 2.01(2) . ?
Ag5 O1 2.076(16) . ?
Ag5 Ag13 2.888(3) . ?
Ag5 Ag8 3.105(3) . ?
Ag5 Ag11 3.235(3) . ?
Ag6 C79 2.27(2) . ?
Ag6 C43 2.35(2) . ?
Ag6 O1 2.452(15) 3_656 ?
Ag6 C44 2.52(2) . ?
Ag6 Ag17 2.939(3) 3_656 ?
Ag6 Ag15 3.077(2) . ?
Ag6 Ag11 3.186(2) 3_656 ?
Ag7 C13 2.26(3) . ?
Ag7 C55 2.30(3) . ?
Ag7 O7 2.428(19) . ?
Ag7 O8 2.46(3) . ?
Ag7 C14 2.64(3) . ?
Ag7 Ag20 3.137(4) . ?
Ag8 C31 2.03(2) . ?
Ag8 O2 2.136(15) . ?
Ag8 Ag13 2.938(3) . ?
Ag8 Ag18 3.244(3) . ?
Ag9 C49 2.22(2) . ?
Ag9 C37 2.26(2) 3_656 ?
Ag9 O5 2.530(18) 3_656 ?
Ag9 C38 2.589(18) 3_656 ?
Ag9 Ag16 2.919(3) . ?
Ag9 Ag10 2.941(3) 3_656 ?
Ag9 Ag17 2.962(3) . ?
Ag9 Ag15 3.139(3) 3_656 ?
Ag10 O4 2.299(17) . ?
Ag10 C37 2.36(2) . ?
Ag10 C19 2.47(2) . ?
Ag10 O14 2.493(18) . ?
Ag10 C20 2.70(2) . ?
Ag10 Ag9 2.941(3) 3_656 ?
Ag10 Ag12 3.147(3) . ?
Ag10 Ag11 3.205(3) . ?
Ag11 C19 2.07(2) . ?
Ag11 C43 2.092(19) 3_656 ?
Ag11 Ag19 2.984(3) . ?
Ag11 Ag12 3.165(3) . ?
Ag11 Ag6 3.186(2) 3_656 ?
Ag11 Ag20 3.238(4) . ?
Ag11 Ag1 3.340(3) 3_656 ?
Ag12 C25 2.37(2) . ?
Ag12 C19 2.40(2) . ?
Ag12 O2 2.418(16) . ?
Ag12 O15 2.458(16) . ?
Ag12 Ag14 3.043(3) . ?
Ag13 C31 2.23(3) . ?
Ag13 C8 2.26(3) . ?
Ag13 O10 2.381(19) . ?
Ag13 O9 2.47(2) . ?
Ag13 Ag18 3.025(3) . ?
Ag14 C49 2.14(2) . ?
Ag14 C25 2.22(2) . ?
Ag14 C26 2.66(2) . ?
Ag14 Ag16 2.914(3) . ?
Ag14 Ag17 2.940(3) . ?
Ag15 C79 2.27(2) . ?
Ag15 O11 2.35(3) . ?
Ag15 O13 2.42(2) 3_656 ?
Ag15 C37 2.54(2) . ?
Ag15 Ag17 2.910(3) 3_656 ?
Ag15 Ag9 3.139(3) 3_656 ?
Ag16 C1 2.25(3) . ?
Ag16 O5 2.307(17) 3_656 ?
Ag16 C49 2.41(2) . ?
Ag16 C2 2.69(3) . ?
Ag17 C79 2.17(2) 3_656 ?
Ag17 O3 2.298(15) . ?
Ag17 C49 2.36(2) . ?
Ag17 Ag15 2.910(3) 3_656 ?
Ag17 Ag6 2.939(3) 3_656 ?
Ag18 C13 2.16(3) . ?
Ag18 C31 2.22(2) . ?
Ag18 O1W 2.473(18) . ?
Ag18 C32 2.61(2) . ?
Ag18 Ag19 2.842(3) . ?
Ag19 C13 2.09(3) . ?
Ag19 O4 2.273(18) . ?
Ag19 C19 2.49(2) . ?
Ag19 Ag20 3.071(4) . ?
Ag20 O6 2.084(17) . ?
Ag20 C55 2.20(2) . ?
Ag20 C56 2.62(3) . ?
Ag20 Ag1 3.181(3) 3_656 ?
V1 O15 1.642(16) . ?
V1 O13 1.67(2) . ?
V1 O14 1.68(2) . ?
V1 O16 1.84(4) . ?
C1 C2 1.24(4) . ?
C2 C3 1.54(4) . ?
C3 C6 1.50(4) . ?
C3 C4 1.54(4) . ?
C3 C5 1.54(4) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.25(3) . ?
C7 C9 1.45(3) . ?
C9 C12 1.54(5) . ?
C9 C10 1.56(5) . ?
C9 C11 1.59(4) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.24(3) . ?
C14 C15 1.51(4) . ?
C15 C16 1.48(5) . ?
C15 C18 1.53(5) . ?
C15 C17 1.59(4) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.24(3) . ?
C20 C21 1.515(17) . ?
C21 C22A 1.522(19) . ?
C21 C22B 1.53(2) . ?
C21 C23A 1.531(19) . ?
C21 C24A 1.540(19) . ?
C21 C23B 1.54(2) . ?
C21 C24B 1.54(2) . ?
C22A H22A 0.9800 . ?
C22A H22B 0.9800 . ?
C22A H22C 0.9800 . ?
C23A H23A 0.9800 . ?
C23A H23B 0.9800 . ?
C23A H23C 0.9800 . ?
C24A H24A 0.9800 . ?
C24A H24B 0.9800 . ?
C24A H24C 0.9800 . ?
C22B H22D 0.9800 . ?
C22B H22E 0.9800 . ?
C22B H22F 0.9800 . ?
C23B H23D 0.9800 . ?
C23B H23E 0.9800 . ?
C23B H23F 0.9800 . ?
C24B H24D 0.9800 . ?
C24B H24E 0.9800 . ?
C24B H24F 0.9800 . ?
C25 C26 1.21(3) . ?
C26 C27 1.44(4) . ?
C27 C28 1.52(4) . ?
C27 C30 1.55(4) . ?
C27 C29 1.56(4) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.21(3) . ?
C32 C33 1.57(4) . ?
C33 C34 1.47(4) . ?
C33 C36 1.50(4) . ?
C33 C35 1.51(4) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.15(3) . ?
C37 Ag9 2.26(2) 3_656 ?
C38 C39 1.526(17) . ?
C38 Ag9 2.589(18) 3_656 ?
C39 C41 1.522(18) . ?
C39 C42 1.534(18) . ?
C39 C40 1.549(18) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.184(17) . ?
C43 Ag11 2.092(19) 3_656 ?
C44 C45 1.530(17) . ?
C45 C46 1.519(18) . ?
C45 C47 1.527(18) . ?
C45 C48 1.538(18) . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.23(3) . ?
C50 C51 1.45(3) . ?
C51 C53 1.52(4) . ?
C51 C54 1.55(4) . ?
C51 C52 1.56(4) . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 H53A 0.9800 . ?
C53 H53B 0.9800 . ?
C53 H53C 0.9800 . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C55 C56 1.19(4) . ?
C56 C57 1.50(4) . ?
C57 C58 1.44(5) . ?
C57 C60 1.55(5) . ?
C57 C59 1.59(5) . ?
C58 H58A 0.9800 . ?
C58 H58B 0.9800 . ?
C58 H58C 0.9800 . ?
C59 H59A 0.9800 . ?
C59 H59B 0.9800 . ?
C59 H59C 0.9800 . ?
C60 H60A 0.9800 . ?
C60 H60B 0.9800 . ?
C60 H60C 0.9800 . ?
C61 C64 1.53(4) . ?
C61 C63 1.54(4) . ?
C61 C62 1.56(4) . ?
C61 P1 1.83(2) . ?
C62 H62A 0.9800 . ?
C62 H62B 0.9800 . ?
C62 H62C 0.9800 . ?
C63 H63A 0.9800 . ?
C63 H63B 0.9800 . ?
C63 H63C 0.9800 . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C65 C68 1.50(4) . ?
C65 C67 1.52(4) . ?
C65 C66 1.53(4) . ?
C65 P2 1.85(3) . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C67 H67A 0.9800 . ?
C67 H67B 0.9800 . ?
C67 H67C 0.9800 . ?
C68 H68A 0.9800 . ?
C68 H68B 0.9800 . ?
C68 H68C 0.9800 . ?
C69 O9 1.17(3) . ?
C69 C70 1.50(4) . ?
C69 C72 1.55(4) . ?
C70 C71 1.40(4) . ?
C70 H70 0.9500 . ?
C71 O10 1.17(3) . ?
C71 C73 1.52(4) . ?
C72 F7 1.17(4) . ?
C72 F8 1.32(4) . ?
C72 F9 1.35(4) . ?
C73 F10 1.30(3) . ?
C73 F11 1.33(3) . ?
C73 F12 1.34(3) . ?
C74 O7 1.22(4) . ?
C74 C77 1.40(4) . ?
C74 C75 1.40(5) . ?
C75 C76 1.42(6) . ?
C75 H75 0.9500 . ?
C76 O8 1.24(5) . ?
C76 C78 1.55(6) . ?
C78 F3 1.319(19) . ?
C78 F2 1.33(2) . ?
C78 F1 1.342(19) . ?
C77 F5 1.319(19) . ?
C77 F6 1.327(19) . ?
C77 F4 1.339(19) . ?
C79 C80 1.12(3) . ?
C79 Ag17 2.17(2) 3_656 ?
C80 C81 1.50(3) . ?
C81 C82 1.51(4) . ?
C81 C83 1.53(4) . ?
C81 C84 1.55(4) . ?
C82 H82A 0.9800 . ?
C82 H82B 0.9800 . ?
C82 H82C 0.9800 . ?
C83 H83A 0.9800 . ?
C83 H83B 0.9800 . ?
C83 H83C 0.9800 . ?
C84 H84A 0.9800 . ?
C84 H84B 0.9800 . ?
C84 H84C 0.9800 . ?
C85 O11 1.19(5) . ?
C85 O12 1.20(6) . ?
C85 C86 1.523(19) . ?
C86 F13 1.317(19) . ?
C86 F15 1.325(19) . ?
C86 F14 1.328(19) . ?
O1 P1 1.545(17) . ?
O1 Ag6 2.452(15) 3_656 ?
O2 P1 1.537(17) . ?
O3 P1 1.539(16) . ?
O4 P2 1.532(19) . ?
O5 P2 1.548(17) . ?
O5 Ag16 2.307(17) 3_656 ?
O5 Ag9 2.530(18) 3_656 ?
O6 P2 1.53(2) . ?
O13 Ag2 2.399(17) 3_656 ?
O13 Ag15 2.42(2) 3_656 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Ag1 C43 161.3(9) . . ?
C1 Ag1 C44 133.8(9) . . ?
C43 Ag1 C44 27.6(4) . . ?
C1 Ag1 Ag16 49.1(8) . . ?
C43 Ag1 Ag16 149.6(5) . . ?
C44 Ag1 Ag16 174.2(5) . . ?
C1 Ag1 Ag2 46.1(7) . . ?
C43 Ag1 Ag2 129.3(5) . . ?
C44 Ag1 Ag2 113.5(5) . . ?
Ag16 Ag1 Ag2 64.33(8) . . ?
C1 Ag1 Ag20 120.4(7) . 3_656 ?
C43 Ag1 Ag20 62.6(5) . 3_656 ?
C44 Ag1 Ag20 74.3(5) . 3_656 ?
Ag16 Ag1 Ag20 109.01(10) . 3_656 ?
Ag2 Ag1 Ag20 166.41(11) . 3_656 ?
C1 Ag1 Ag11 160.2(8) . 3_656 ?
C43 Ag1 Ag11 38.5(5) . 3_656 ?
C44 Ag1 Ag11 66.0(4) . 3_656 ?
Ag16 Ag1 Ag11 111.18(9) . 3_656 ?
Ag2 Ag1 Ag11 133.34(9) . 3_656 ?
Ag20 Ag1 Ag11 59.49(7) 3_656 3_656 ?
C1 Ag2 O12 121.4(16) . . ?
C1 Ag2 O13 110.2(8) . 3_656 ?
O12 Ag2 O13 97.4(13) . 3_656 ?
C1 Ag2 C25 132.9(9) . . ?
O12 Ag2 C25 89.9(12) . . ?
O13 Ag2 C25 98.0(7) 3_656 . ?
C1 Ag2 Ag1 45.0(7) . . ?
O12 Ag2 Ag1 118.1(9) . . ?
O13 Ag2 Ag1 66.3(5) 3_656 . ?
C25 Ag2 Ag1 148.6(5) . . ?
C1 Ag2 Ag3 162.7(7) . . ?
O12 Ag2 Ag3 75.4(14) . . ?
O13 Ag2 Ag3 60.1(5) 3_656 . ?
C25 Ag2 Ag3 43.6(5) . . ?
Ag1 Ag2 Ag3 126.10(9) . . ?
C1 Ag2 Ag14 97.4(8) . . ?
O12 Ag2 Ag14 134.4(11) . . ?
O13 Ag2 Ag14 89.7(5) 3_656 . ?
C25 Ag2 Ag14 44.6(5) . . ?
Ag1 Ag2 Ag14 106.00(9) . . ?
Ag3 Ag2 Ag14 69.57(7) . . ?
C1 Ag2 Ag16 45.2(7) . . ?
O12 Ag2 Ag16 166.0(15) . . ?
O13 Ag2 Ag16 92.7(5) 3_656 . ?
C25 Ag2 Ag16 98.4(5) . . ?
Ag1 Ag2 Ag16 57.65(7) . . ?
Ag3 Ag2 Ag16 118.34(9) . . ?
Ag14 Ag2 Ag16 55.01(7) . . ?
C37 Ag3 C25 162.5(8) . . ?
C37 Ag3 Ag10 54.5(6) . . ?
C25 Ag3 Ag10 119.3(6) . . ?
C37 Ag3 Ag12 119.7(6) . . ?
C25 Ag3 Ag12 53.2(6) . . ?
Ag10 Ag3 Ag12 66.39(6) . . ?
C37 Ag3 Ag2 135.6(6) . . ?
C25 Ag3 Ag2 54.2(6) . . ?
Ag10 Ag3 Ag2 166.61(9) . . ?
Ag12 Ag3 Ag2 104.75(8) . . ?
C37 Ag3 Ag15 54.7(6) . . ?
C25 Ag3 Ag15 136.4(6) . . ?
Ag10 Ag3 Ag15 104.10(7) . . ?
Ag12 Ag3 Ag15 165.55(9) . . ?
Ag2 Ag3 Ag15 82.43(7) . . ?
C55 Ag4 C8 168.5(10) . . ?
C55 Ag4 C7 140.8(9) . . ?
C8 Ag4 C7 29.9(9) . . ?
C55 Ag4 Ag20 45.9(6) . . ?
C8 Ag4 Ag20 140.0(6) . . ?
C7 Ag4 Ag20 163.5(7) . . ?
C55 Ag4 Ag7 45.9(8) . . ?
C8 Ag4 Ag7 143.2(8) . . ?
C7 Ag4 Ag7 136.4(7) . . ?
Ag20 Ag4 Ag7 60.04(8) . . ?
C55 Ag4 Ag5 146.7(7) . . ?
C8 Ag4 Ag5 37.4(6) . . ?
C7 Ag4 Ag5 66.3(6) . . ?
Ag20 Ag4 Ag5 102.59(10) . . ?
Ag7 Ag4 Ag5 136.29(10) . . ?
C8 Ag5 O1 168.3(9) . . ?
C8 Ag5 Ag13 51.3(8) . . ?
O1 Ag5 Ag13 130.2(4) . . ?
C8 Ag5 Ag8 106.8(8) . . ?
O1 Ag5 Ag8 79.6(5) . . ?
Ag13 Ag5 Ag8 58.58(6) . . ?
C8 Ag5 Ag11 117.7(7) . . ?
O1 Ag5 Ag11 73.6(5) . . ?
Ag13 Ag5 Ag11 110.22(8) . . ?
Ag8 Ag5 Ag11 68.89(7) . . ?
C8 Ag5 Ag4 42.2(7) . . ?
O1 Ag5 Ag4 147.7(5) . . ?
Ag13 Ag5 Ag4 71.58(7) . . ?
Ag8 Ag5 Ag4 99.96(8) . . ?
Ag11 Ag5 Ag4 76.26(7) . . ?
C79 Ag6 C43 157.0(7) . . ?
C79 Ag6 O1 96.7(8) . 3_656 ?
C43 Ag6 O1 96.5(6) . 3_656 ?
C79 Ag6 C44 129.3(7) . . ?
C43 Ag6 C44 27.8(4) . . ?
O1 Ag6 C44 113.5(6) 3_656 . ?
C79 Ag6 Ag17 47.1(6) . 3_656 ?
C43 Ag6 Ag17 155.3(5) . 3_656 ?
O1 Ag6 Ag17 76.8(4) 3_656 3_656 ?
C44 Ag6 Ag17 169.7(5) . 3_656 ?
C79 Ag6 Ag15 47.2(6) . . ?
C43 Ag6 Ag15 128.0(5) . . ?
O1 Ag6 Ag15 133.9(4) 3_656 . ?
C44 Ag6 Ag15 112.2(5) . . ?
Ag17 Ag6 Ag15 57.80(6) 3_656 . ?
C79 Ag6 Ag11 161.7(6) . 3_656 ?
C43 Ag6 Ag11 41.0(5) . 3_656 ?
O1 Ag6 Ag11 70.6(4) 3_656 3_656 ?
C44 Ag6 Ag11 68.8(4) . 3_656 ?
Ag17 Ag6 Ag11 115.55(8) 3_656 3_656 ?
Ag15 Ag6 Ag11 134.15(8) . 3_656 ?
C13 Ag7 C55 127.3(9) . . ?
C13 Ag7 O7 116.8(8) . . ?
C55 Ag7 O7 97.1(8) . . ?
C13 Ag7 O8 117.0(9) . . ?
C55 Ag7 O8 110.0(9) . . ?
O7 Ag7 O8 74.4(7) . . ?
C13 Ag7 C14 27.8(8) . . ?
C55 Ag7 C14 155.0(8) . . ?
O7 Ag7 C14 100.9(7) . . ?
O8 Ag7 C14 91.5(8) . . ?
C13 Ag7 Ag20 89.9(6) . . ?
C55 Ag7 Ag20 44.6(6) . . ?
O7 Ag7 Ag20 140.8(5) . . ?
O8 Ag7 Ag20 120.4(6) . . ?
C14 Ag7 Ag20 113.7(5) . . ?
C13 Ag7 Ag4 97.4(7) . . ?
C55 Ag7 Ag4 41.4(7) . . ?
O7 Ag7 Ag4 88.8(5) . . ?
O8 Ag7 Ag4 145.5(6) . . ?
C14 Ag7 Ag4 121.6(6) . . ?
Ag20 Ag7 Ag4 57.98(9) . . ?
C31 Ag8 O2 161.2(8) . . ?
C31 Ag8 Ag13 49.4(7) . . ?
O2 Ag8 Ag13 132.6(4) . . ?
C31 Ag8 Ag5 104.5(8) . . ?
O2 Ag8 Ag5 85.3(5) . . ?
Ag13 Ag8 Ag5 57.01(6) . . ?
C31 Ag8 Ag18 42.6(7) . . ?
O2 Ag8 Ag18 155.8(5) . . ?
Ag13 Ag8 Ag18 58.34(7) . . ?
Ag5 Ag8 Ag18 87.35(8) . . ?
C49 Ag9 C37 160.5(8) . 3_656 ?
C49 Ag9 O5 86.8(7) . 3_656 ?
C37 Ag9 O5 109.4(7) 3_656 3_656 ?
C49 Ag9 C38 142.2(8) . 3_656 ?
C37 Ag9 C38 26.4(7) 3_656 3_656 ?
O5 Ag9 C38 101.4(6) 3_656 3_656 ?
C49 Ag9 Ag16 54.0(6) . . ?
C37 Ag9 Ag16 145.3(6) 3_656 . ?
O5 Ag9 Ag16 49.5(4) 3_656 . ?
C38 Ag9 Ag16 150.4(5) 3_656 . ?
C49 Ag9 Ag10 147.4(6) . 3_656 ?
C37 Ag9 Ag10 51.9(6) 3_656 3_656 ?
O5 Ag9 Ag10 70.2(4) 3_656 3_656 ?
C38 Ag9 Ag10 67.5(4) 3_656 3_656 ?
Ag16 Ag9 Ag10 93.49(8) . 3_656 ?
C49 Ag9 Ag17 51.7(6) . . ?
C37 Ag9 Ag17 109.6(6) 3_656 . ?
O5 Ag9 Ag17 136.1(4) 3_656 . ?
C38 Ag9 Ag17 104.6(5) 3_656 . ?
Ag16 Ag9 Ag17 102.14(8) . . ?
Ag10 Ag9 Ag17 153.16(10) 3_656 . ?
C49 Ag9 Ag15 108.6(6) . 3_656 ?
C37 Ag9 Ag15 53.1(6) 3_656 3_656 ?
O5 Ag9 Ag15 158.8(4) 3_656 3_656 ?
C38 Ag9 Ag15 57.5(5) 3_656 3_656 ?
Ag16 Ag9 Ag15 151.78(10) . 3_656 ?
Ag10 Ag9 Ag15 100.26(7) 3_656 3_656 ?
Ag17 Ag9 Ag15 56.88(6) . 3_656 ?
O4 Ag10 C37 120.1(8) . . ?
O4 Ag10 C19 82.6(7) . . ?
C37 Ag10 C19 140.2(8) . . ?
O4 Ag10 O14 101.0(8) . . ?
C37 Ag10 O14 102.5(8) . . ?
C19 Ag10 O14 104.4(8) . . ?
O4 Ag10 C20 84.9(7) . . ?
C37 Ag10 C20 116.4(7) . . ?
C19 Ag10 C20 27.4(7) . . ?
O14 Ag10 C20 130.9(7) . . ?
O4 Ag10 Ag3 164.9(5) . . ?
C37 Ag10 Ag3 47.2(6) . . ?
C19 Ag10 Ag3 103.4(6) . . ?
O14 Ag10 Ag3 91.0(6) . . ?
C20 Ag10 Ag3 94.2(5) . . ?
O4 Ag10 Ag9 99.5(4) . 3_656 ?
C37 Ag10 Ag9 49.1(5) . 3_656 ?
C19 Ag10 Ag9 167.0(5) . 3_656 ?
O14 Ag10 Ag9 62.6(6) . 3_656 ?
C20 Ag10 Ag9 165.0(4) . 3_656 ?
Ag3 Ag10 Ag9 77.83(7) . 3_656 ?
O4 Ag10 Ag12 130.9(5) . . ?
C37 Ag10 Ag12 104.3(6) . . ?
C19 Ag10 Ag12 48.7(6) . . ?
O14 Ag10 Ag12 87.7(5) . . ?
C20 Ag10 Ag12 55.6(5) . . ?
Ag3 Ag10 Ag12 58.01(6) . . ?
Ag9 Ag10 Ag12 126.44(8) 3_656 . ?
O4 Ag10 Ag11 80.0(5) . . ?
C37 Ag10 Ag11 159.2(6) . . ?
C19 Ag10 Ag11 40.2(5) . . ?
O14 Ag10 Ag11 65.8(6) . . ?
C20 Ag10 Ag11 67.5(4) . . ?
Ag3 Ag10 Ag11 113.67(7) . . ?
Ag9 Ag10 Ag11 127.23(8) 3_656 . ?
Ag12 Ag10 Ag11 59.77(6) . . ?
C19 Ag11 C43 176.3(9) . 3_656 ?
C19 Ag11 Ag19 55.6(7) . . ?
C43 Ag11 Ag19 121.3(6) 3_656 . ?
C19 Ag11 Ag12 49.3(7) . . ?
C43 Ag11 Ag12 134.0(6) 3_656 . ?
Ag19 Ag11 Ag12 104.52(7) . . ?
C19 Ag11 Ag6 135.4(7) . 3_656 ?
C43 Ag11 Ag6 47.4(6) 3_656 3_656 ?
Ag19 Ag11 Ag6 167.22(8) . 3_656 ?
Ag12 Ag11 Ag6 87.31(6) . 3_656 ?
C19 Ag11 Ag10 50.5(6) . . ?
C43 Ag11 Ag10 131.6(6) 3_656 . ?
Ag19 Ag11 Ag10 70.34(6) . . ?
Ag12 Ag11 Ag10 59.21(6) . . ?
Ag6 Ag11 Ag10 120.98(7) 3_656 . ?
C19 Ag11 Ag5 108.5(6) . . ?
C43 Ag11 Ag5 70.0(6) 3_656 . ?
Ag19 Ag11 Ag5 108.61(7) . . ?
Ag12 Ag11 Ag5 99.88(7) . . ?
Ag6 Ag11 Ag5 63.75(6) 3_656 . ?
Ag10 Ag11 Ag5 156.45(8) . . ?
C19 Ag11 Ag20 113.9(7) . . ?
C43 Ag11 Ag20 63.5(6) 3_656 . ?
Ag19 Ag11 Ag20 58.99(7) . . ?
Ag12 Ag11 Ag20 157.95(8) . . ?
Ag6 Ag11 Ag20 110.76(8) 3_656 . ?
Ag10 Ag11 Ag20 99.57(7) . . ?
Ag5 Ag11 Ag20 99.50(7) . . ?
C19 Ag11 Ag1 136.5(6) . 3_656 ?
C43 Ag11 Ag1 45.0(6) 3_656 3_656 ?
Ag19 Ag11 Ag1 106.49(8) . 3_656 ?
Ag12 Ag11 Ag1 121.47(7) . 3_656 ?
Ag6 Ag11 Ag1 70.21(6) 3_656 3_656 ?
Ag10 Ag11 Ag1 86.98(7) . 3_656 ?
Ag5 Ag11 Ag1 114.99(7) . 3_656 ?
Ag20 Ag11 Ag1 57.82(7) . 3_656 ?
C25 Ag12 C19 142.2(8) . . ?
C25 Ag12 O2 119.2(7) . . ?
C19 Ag12 O2 84.8(6) . . ?
C25 Ag12 O15 99.2(8) . . ?
C19 Ag12 O15 101.1(8) . . ?
O2 Ag12 O15 106.3(6) . . ?
C25 Ag12 Ag3 46.5(6) . . ?
C19 Ag12 Ag3 103.1(5) . . ?
O2 Ag12 Ag3 162.8(4) . . ?
O15 Ag12 Ag3 87.4(5) . . ?
C25 Ag12 Ag14 46.5(5) . . ?
C19 Ag12 Ag14 161.2(5) . . ?
O2 Ag12 Ag14 104.0(4) . . ?
O15 Ag12 Ag14 60.7(6) . . ?
Ag3 Ag12 Ag14 73.14(7) . . ?
C25 Ag12 Ag10 101.8(6) . . ?
C19 Ag12 Ag10 50.8(5) . . ?
O2 Ag12 Ag10 135.4(4) . . ?
O15 Ag12 Ag10 81.8(4) . . ?
Ag3 Ag12 Ag10 55.59(6) . . ?
Ag14 Ag12 Ag10 117.28(7) . . ?
C25 Ag12 Ag11 155.4(6) . . ?
C19 Ag12 Ag11 40.8(5) . . ?
O2 Ag12 Ag11 83.5(4) . . ?
O15 Ag12 Ag11 62.7(6) . . ?
Ag3 Ag12 Ag11 112.60(7) . . ?
Ag14 Ag12 Ag11 122.75(8) . . ?
Ag10 Ag12 Ag11 61.02(6) . . ?
C31 Ag13 C8 138.2(9) . . ?
C31 Ag13 O10 105.2(8) . . ?
C8 Ag13 O10 111.1(9) . . ?
C31 Ag13 O9 103.6(8) . . ?
C8 Ag13 O9 105.5(8) . . ?
O10 Ag13 O9 74.4(7) . . ?
C31 Ag13 Ag5 106.3(6) . . ?
C8 Ag13 Ag5 44.0(6) . . ?
O10 Ag13 Ag5 106.4(6) . . ?
O9 Ag13 Ag5 148.5(6) . . ?
C31 Ag13 Ag8 43.7(6) . . ?
C8 Ag13 Ag8 105.5(6) . . ?
O10 Ag13 Ag8 104.8(5) . . ?
O9 Ag13 Ag8 146.8(6) . . ?
Ag5 Ag13 Ag8 64.41(7) . . ?
C31 Ag13 Ag18 47.1(6) . . ?
C8 Ag13 Ag18 99.4(6) . . ?
O10 Ag13 Ag18 149.4(6) . . ?
O9 Ag13 Ag18 97.6(5) . . ?
Ag5 Ag13 Ag18 95.73(8) . . ?
Ag8 Ag13 Ag18 65.90(7) . . ?
C49 Ag14 C25 157.7(8) . . ?
C49 Ag14 C26 132.0(8) . . ?
C25 Ag14 C26 26.8(8) . . ?
C49 Ag14 Ag16 54.5(6) . . ?
C25 Ag14 Ag16 114.2(6) . . ?
C26 Ag14 Ag16 106.6(5) . . ?
C49 Ag14 Ag17 52.4(6) . . ?
C25 Ag14 Ag17 143.0(6) . . ?
C26 Ag14 Ag17 139.4(5) . . ?
Ag16 Ag14 Ag17 102.83(8) . . ?
C49 Ag14 Ag12 142.5(6) . . ?
C25 Ag14 Ag12 50.6(6) . . ?
C26 Ag14 Ag12 63.4(6) . . ?
Ag16 Ag14 Ag12 162.99(10) . . ?
Ag17 Ag14 Ag12 92.88(8) . . ?
C49 Ag14 Ag2 116.8(6) . . ?
C25 Ag14 Ag2 52.8(6) . . ?
C26 Ag14 Ag2 58.8(5) . . ?
Ag16 Ag14 Ag2 62.95(7) . . ?
Ag17 Ag14 Ag2 161.68(9) . . ?
Ag12 Ag14 Ag2 100.31(8) . . ?
C79 Ag15 O11 115.1(12) . . ?
C79 Ag15 O13 112.7(7) . 3_656 ?
O11 Ag15 O13 100.3(11) . 3_656 ?
C79 Ag15 C37 136.8(8) . . ?
O11 Ag15 C37 84.7(9) . . ?
O13 Ag15 C37 99.5(7) 3_656 . ?
C79 Ag15 Ag17 47.6(6) . 3_656 ?
O11 Ag15 Ag17 160.9(11) . 3_656 ?
O13 Ag15 Ag17 95.3(4) 3_656 3_656 ?
C37 Ag15 Ag17 103.6(5) . 3_656 ?
C79 Ag15 Ag6 47.4(6) . . ?
O11 Ag15 Ag6 118.5(7) . . ?
O13 Ag15 Ag6 65.7(5) 3_656 . ?
C37 Ag15 Ag6 153.5(5) . . ?
Ag17 Ag15 Ag6 58.72(6) 3_656 . ?
C79 Ag15 Ag3 167.0(5) . . ?
O11 Ag15 Ag3 77.5(11) . . ?
O13 Ag15 Ag3 59.9(5) 3_656 . ?
C37 Ag15 Ag3 43.0(6) . . ?
Ag17 Ag15 Ag3 120.31(8) 3_656 . ?
Ag6 Ag15 Ag3 125.28(8) . . ?
C79 Ag15 Ag9 100.6(6) . 3_656 ?
O11 Ag15 Ag9 129.3(7) . 3_656 ?
O13 Ag15 Ag9 97.4(5) 3_656 3_656 ?
C37 Ag15 Ag9 45.5(5) . 3_656 ?
Ag17 Ag15 Ag9 58.50(6) 3_656 3_656 ?
Ag6 Ag15 Ag9 112.15(7) . 3_656 ?
Ag3 Ag15 Ag9 71.34(6) . 3_656 ?
C1 Ag16 O5 130.0(8) . 3_656 ?
C1 Ag16 C49 141.3(9) . . ?
O5 Ag16 C49 87.7(7) 3_656 . ?
C1 Ag16 C2 27.2(8) . . ?
O5 Ag16 C2 121.6(7) 3_656 . ?
C49 Ag16 C2 130.8(7) . . ?
C1 Ag16 Ag14 101.7(6) . . ?
O5 Ag16 Ag14 126.8(5) 3_656 . ?
C49 Ag16 Ag14 46.3(6) . . ?
C2 Ag16 Ag14 110.2(6) . . ?
C1 Ag16 Ag9 155.7(7) . . ?
O5 Ag16 Ag9 56.5(5) 3_656 . ?
C49 Ag16 Ag9 48.1(5) . . ?
C2 Ag16 Ag9 176.9(5) . . ?
Ag14 Ag16 Ag9 71.26(8) . . ?
C1 Ag16 Ag1 45.1(7) . . ?
O5 Ag16 Ag1 98.6(4) 3_656 . ?
C49 Ag16 Ag1 152.7(5) . . ?
C2 Ag16 Ag1 67.3(5) . . ?
Ag14 Ag16 Ag1 112.48(9) . . ?
Ag9 Ag16 Ag1 114.90(9) . . ?
C1 Ag16 Ag2 42.7(6) . . ?
O5 Ag16 Ag2 153.7(4) 3_656 . ?
C49 Ag16 Ag2 107.8(6) . . ?
C2 Ag16 Ag2 63.7(5) . . ?
Ag14 Ag16 Ag2 62.04(7) . . ?
Ag9 Ag16 Ag2 119.14(9) . . ?
Ag1 Ag16 Ag2 58.03(7) . . ?
C79 Ag17 O3 122.5(7) 3_656 . ?
C79 Ag17 C49 148.2(8) 3_656 . ?
O3 Ag17 C49 85.7(7) . . ?
C79 Ag17 Ag15 50.4(7) 3_656 3_656 ?
O3 Ag17 Ag15 150.5(4) . 3_656 ?
C49 Ag17 Ag15 112.3(5) . 3_656 ?
C79 Ag17 Ag6 50.1(6) 3_656 3_656 ?
O3 Ag17 Ag6 90.1(4) . 3_656 ?
C49 Ag17 Ag6 154.8(6) . 3_656 ?
Ag15 Ag17 Ag6 63.49(6) 3_656 3_656 ?
C79 Ag17 Ag14 158.3(7) 3_656 . ?
O3 Ag17 Ag14 60.4(4) . . ?
C49 Ag17 Ag14 46.1(6) . . ?
Ag15 Ag17 Ag14 114.96(8) 3_656 . ?
Ag6 Ag17 Ag14 110.98(8) 3_656 . ?
C79 Ag17 Ag9 108.6(6) 3_656 . ?
O3 Ag17 Ag9 128.6(4) . . ?
C49 Ag17 Ag9 47.7(5) . . ?
Ag15 Ag17 Ag9 64.62(7) 3_656 . ?
Ag6 Ag17 Ag9 121.87(8) 3_656 . ?
Ag14 Ag17 Ag9 70.30(7) . . ?
C13 Ag18 C31 155.4(10) . . ?
C13 Ag18 O1W 98.1(9) . . ?
C31 Ag18 O1W 102.2(8) . . ?
C13 Ag18 C32 139.3(10) . . ?
C31 Ag18 C32 27.5(8) . . ?
O1W Ag18 C32 91.8(8) . . ?
C13 Ag18 Ag19 47.1(7) . . ?
C31 Ag18 Ag19 120.5(6) . . ?
O1W Ag18 Ag19 134.2(6) . . ?
C32 Ag18 Ag19 133.8(5) . . ?
C13 Ag18 Ag13 155.8(8) . . ?
C31 Ag18 Ag13 47.4(7) . . ?
O1W Ag18 Ag13 71.0(5) . . ?
C32 Ag18 Ag13 64.1(6) . . ?
Ag19 Ag18 Ag13 126.60(9) . . ?
C13 Ag18 Ag8 131.9(7) . . ?
C31 Ag18 Ag8 38.2(6) . . ?
O1W Ag18 Ag8 126.7(5) . . ?
C32 Ag18 Ag8 64.0(6) . . ?
Ag19 Ag18 Ag8 85.67(8) . . ?
Ag13 Ag18 Ag8 55.75(6) . . ?
C13 Ag19 O4 131.4(9) . . ?
C13 Ag19 C19 141.6(9) . . ?
O4 Ag19 C19 82.7(7) . . ?
C13 Ag19 Ag18 49.0(7) . . ?
O4 Ag19 Ag18 174.0(5) . . ?
C19 Ag19 Ag18 95.1(5) . . ?
C13 Ag19 Ag11 137.5(8) . . ?
O4 Ag19 Ag11 85.5(5) . . ?
C19 Ag19 Ag11 43.2(5) . . ?
Ag18 Ag19 Ag11 96.74(8) . . ?
C13 Ag19 Ag20 95.0(8) . . ?
O4 Ag19 Ag20 84.1(5) . . ?
C19 Ag19 Ag20 107.3(5) . . ?
Ag18 Ag19 Ag20 101.83(9) . . ?
Ag11 Ag19 Ag20 64.64(8) . . ?
O6 Ag20 C55 154.9(9) . . ?
O6 Ag20 C56 129.2(9) . . ?
C55 Ag20 C56 26.8(9) . . ?
O6 Ag20 Ag4 161.2(7) . . ?
C55 Ag20 Ag4 43.5(7) . . ?
C56 Ag20 Ag4 69.6(6) . . ?
O6 Ag20 Ag19 80.8(6) . . ?
C55 Ag20 Ag19 109.6(7) . . ?
C56 Ag20 Ag19 126.0(7) . . ?
Ag4 Ag20 Ag19 86.60(10) . . ?
O6 Ag20 Ag7 124.5(6) . . ?
C55 Ag20 Ag7 47.1(8) . . ?
C56 Ag20 Ag7 57.5(7) . . ?
Ag4 Ag20 Ag7 61.98(8) . . ?
Ag19 Ag20 Ag7 68.50(8) . . ?
O6 Ag20 Ag1 56.8(6) . 3_656 ?
C55 Ag20 Ag1 133.9(8) . 3_656 ?
C56 Ag20 Ag1 125.6(7) . 3_656 ?
Ag4 Ag20 Ag1 115.38(11) . 3_656 ?
Ag19 Ag20 Ag1 108.37(10) . 3_656 ?
Ag7 Ag20 Ag1 175.66(13) . 3_656 ?
O6 Ag20 Ag11 82.5(6) . . ?
C55 Ag20 Ag11 122.4(7) . . ?
C56 Ag20 Ag11 147.8(6) . . ?
Ag4 Ag20 Ag11 78.89(9) . . ?
Ag19 Ag20 Ag11 56.37(7) . . ?
Ag7 Ag20 Ag11 113.02(11) . . ?
Ag1 Ag20 Ag11 62.69(7) 3_656 . ?
O15 V1 O13 108.6(9) . . ?
O15 V1 O14 108.7(10) . . ?
O13 V1 O14 108.3(10) . . ?
O15 V1 O16 94.2(17) . . ?
O13 V1 O16 113.6(18) . . ?
O14 V1 O16 121.9(18) . . ?
C2 C1 Ag1 138(2) . . ?
C2 C1 Ag2 132(2) . . ?
Ag1 C1 Ag2 89.0(10) . . ?
C2 C1 Ag16 96(2) . . ?
Ag1 C1 Ag16 85.8(9) . . ?
Ag2 C1 Ag16 92.1(10) . . ?
C1 C2 C3 174(3) . . ?
C1 C2 Ag16 56.3(17) . . ?
C3 C2 Ag16 126.7(17) . . ?
C6 C3 C4 112(3) . . ?
C6 C3 C5 112(3) . . ?
C4 C3 C5 110(3) . . ?
C6 C3 C2 107(2) . . ?
C4 C3 C2 108(2) . . ?
C5 C3 C2 108(2) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 C9 173(3) . . ?
C8 C7 Ag4 63.1(16) . . ?
C9 C7 Ag4 124(2) . . ?
C7 C8 Ag5 159(3) . . ?
C7 C8 Ag4 87.0(19) . . ?
Ag5 C8 Ag4 100.3(10) . . ?
C7 C8 Ag13 112(2) . . ?
Ag5 C8 Ag13 84.8(9) . . ?
Ag4 C8 Ag13 107.0(12) . . ?
C7 C9 C12 108(3) . . ?
C7 C9 C10 107(3) . . ?
C12 C9 C10 112(3) . . ?
C7 C9 C11 110(3) . . ?
C12 C9 C11 110(3) . . ?
C10 C9 C11 109(3) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag19 145(2) . . ?
C14 C13 Ag18 120(2) . . ?
Ag19 C13 Ag18 83.9(9) . . ?
C14 C13 Ag7 93(2) . . ?
Ag19 C13 Ag7 106.6(12) . . ?
Ag18 C13 Ag7 101.3(12) . . ?
C13 C14 C15 175(3) . . ?
C13 C14 Ag7 58.7(18) . . ?
C15 C14 Ag7 126.6(19) . . ?
C16 C15 C14 106(3) . . ?
C16 C15 C18 114(3) . . ?
C14 C15 C18 108(2) . . ?
C16 C15 C17 113(3) . . ?
C14 C15 C17 107(2) . . ?
C18 C15 C17 109(3) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C15 C17 H17A 109.5 . . ?
C15 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C15 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 Ag11 175(2) . . ?
C20 C19 Ag12 92.8(18) . . ?
Ag11 C19 Ag12 89.9(8) . . ?
C20 C19 Ag10 86.6(17) . . ?
Ag11 C19 Ag10 89.3(8) . . ?
Ag12 C19 Ag10 80.5(7) . . ?
C20 C19 Ag19 95.5(17) . . ?
Ag11 C19 Ag19 81.2(8) . . ?
Ag12 C19 Ag19 168.4(10) . . ?
Ag10 C19 Ag19 92.0(7) . . ?
C19 C20 C21 172(2) . . ?
C19 C20 Ag10 66.0(15) . . ?
C21 C20 Ag10 121.2(15) . . ?
C20 C21 C22A 111(2) . . ?
C20 C21 C22B 110(4) . . ?
C20 C21 C23A 109(2) . . ?
C22A C21 C23A 111.0(17) . . ?
C20 C21 C24A 106(3) . . ?
C22A C21 C24A 110.3(17) . . ?
C23A C21 C24A 109.9(17) . . ?
C20 C21 C23B 111(4) . . ?
C22B C21 C23B 109(3) . . ?
C20 C21 C24B 109(4) . . ?
C22B C21 C24B 109(3) . . ?
C23B C21 C24B 108(3) . . ?
C21 C22A H22A 109.5 . . ?
C21 C22A H22B 109.5 . . ?
H22A C22A H22B 109.5 . . ?
C21 C22A H22C 109.5 . . ?
H22A C22A H22C 109.5 . . ?
H22B C22A H22C 109.5 . . ?
C21 C23A H23A 109.5 . . ?
C21 C23A H23B 109.5 . . ?
H23A C23A H23B 109.5 . . ?
C21 C23A H23C 109.5 . . ?
H23A C23A H23C 109.5 . . ?
H23B C23A H23C 109.5 . . ?
C21 C24A H24A 109.5 . . ?
C21 C24A H24B 109.5 . . ?
H24A C24A H24B 109.5 . . ?
C21 C24A H24C 109.5 . . ?
H24A C24A H24C 109.5 . . ?
H24B C24A H24C 109.5 . . ?
C21 C22B H22D 109.5 . . ?
C21 C22B H22E 109.5 . . ?
H22D C22B H22E 109.5 . . ?
C21 C22B H22F 109.5 . . ?
H22D C22B H22F 109.5 . . ?
H22E C22B H22F 109.5 . . ?
C21 C23B H23D 109.5 . . ?
C21 C23B H23E 109.5 . . ?
H23D C23B H23E 109.5 . . ?
C21 C23B H23F 109.5 . . ?
H23D C23B H23F 109.5 . . ?
H23E C23B H23F 109.5 . . ?
C21 C24B H24D 109.5 . . ?
C21 C24B H24E 109.5 . . ?
H24D C24B H24E 109.5 . . ?
C21 C24B H24F 109.5 . . ?
H24D C24B H24F 109.5 . . ?
H24E C24B H24F 109.5 . . ?
C26 C25 Ag3 153(2) . . ?
C26 C25 Ag14 97.3(18) . . ?
Ag3 C25 Ag14 108.7(10) . . ?
C26 C25 Ag12 110.7(18) . . ?
Ag3 C25 Ag12 80.2(8) . . ?
Ag14 C25 Ag12 83.0(8) . . ?
C26 C25 Ag2 94.5(17) . . ?
Ag3 C25 Ag2 82.2(8) . . ?
Ag14 C25 Ag2 82.6(7) . . ?
Ag12 C25 Ag2 152.3(10) . . ?
C25 C26 C27 176(3) . . ?
C25 C26 Ag14 55.9(14) . . ?
C27 C26 Ag14 128(2) . . ?
C26 C27 C28 108(3) . . ?
C26 C27 C30 108(3) . . ?
C28 C27 C30 107(3) . . ?
C26 C27 C29 107(2) . . ?
C28 C27 C29 112(3) . . ?
C30 C27 C29 114(3) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 Ag8 152(2) . . ?
C32 C31 Ag18 94.2(17) . . ?
Ag8 C31 Ag18 99.2(10) . . ?
C32 C31 Ag13 119(2) . . ?
Ag8 C31 Ag13 86.9(9) . . ?
Ag18 C31 Ag13 85.5(9) . . ?
C31 C32 C33 176(3) . . ?
C31 C32 Ag18 58.3(15) . . ?
C33 C32 Ag18 124.5(17) . . ?
C34 C33 C36 108(3) . . ?
C34 C33 C35 111(3) . . ?
C36 C33 C35 112(3) . . ?
C34 C33 C32 112(2) . . ?
C36 C33 C32 108(2) . . ?
C35 C33 C32 105(2) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 Ag3 153(2) . . ?
C38 C37 Ag9 92.8(16) . 3_656 ?
Ag3 C37 Ag9 111.6(10) . 3_656 ?
C38 C37 Ag10 119(2) . . ?
Ag3 C37 Ag10 78.3(8) . . ?
Ag9 C37 Ag10 79.1(7) 3_656 . ?
C38 C37 Ag15 90.5(17) . . ?
Ag3 C37 Ag15 82.3(8) . . ?
Ag9 C37 Ag15 81.4(7) 3_656 . ?
Ag10 C37 Ag15 144.9(10) . . ?
C37 C38 C39 173(2) . . ?
C37 C38 Ag9 60.8(13) . 3_656 ?
C39 C38 Ag9 126.0(12) . 3_656 ?
C41 C39 C38 108.6(17) . . ?
C41 C39 C42 111.5(14) . . ?
C38 C39 C42 107.3(18) . . ?
C41 C39 C40 110.4(15) . . ?
C38 C39 C40 109.5(17) . . ?
C42 C39 C40 109.5(14) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 Ag11 176(2) . 3_656 ?
C44 C43 Ag6 84.5(15) . . ?
Ag11 C43 Ag6 91.6(8) 3_656 . ?
C44 C43 Ag1 84.3(16) . . ?
Ag11 C43 Ag1 96.5(8) 3_656 . ?
Ag6 C43 Ag1 105.3(8) . . ?
C43 C44 C45 168(2) . . ?
C43 C44 Ag6 67.7(14) . . ?
C45 C44 Ag6 118.0(14) . . ?
C43 C44 Ag1 68.2(15) . . ?
C45 C44 Ag1 119.8(14) . . ?
Ag6 C44 Ag1 95.5(7) . . ?
C46 C45 C47 112.5(14) . . ?
C46 C45 C44 107(2) . . ?
C47 C45 C44 108(2) . . ?
C46 C45 C48 111.9(14) . . ?
C47 C45 C48 111.5(15) . . ?
C44 C45 C48 105.5(18) . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C45 C47 H47A 109.5 . . ?
C45 C47 H47B 109.5 . . ?
H47A C47 H47B 109.5 . . ?
C45 C47 H47C 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
C45 C48 H48A 109.5 . . ?
C45 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C45 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 Ag14 145(2) . . ?
C50 C49 Ag9 113(2) . . ?
Ag14 C49 Ag9 102.2(9) . . ?
C50 C49 Ag17 98.6(17) . . ?
Ag14 C49 Ag17 81.4(7) . . ?
Ag9 C49 Ag17 80.6(7) . . ?
C50 C49 Ag16 112.5(17) . . ?
Ag14 C49 Ag16 79.3(8) . . ?
Ag9 C49 Ag16 77.9(7) . . ?
Ag17 C49 Ag16 147.2(10) . . ?
C49 C50 C51 173(3) . . ?
C50 C51 C53 112(2) . . ?
C50 C51 C54 107(2) . . ?
C53 C51 C54 106(3) . . ?
C50 C51 C52 108(2) . . ?
C53 C51 C52 112(2) . . ?
C54 C51 C52 111(2) . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C51 C53 H53A 109.5 . . ?
C51 C53 H53B 109.5 . . ?
H53A C53 H53B 109.5 . . ?
C51 C53 H53C 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C51 C54 H54A 109.5 . . ?
C51 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C51 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C56 C55 Ag4 163(3) . . ?
C56 C55 Ag20 97(2) . . ?
Ag4 C55 Ag20 90.6(9) . . ?
C56 C55 Ag7 102(2) . . ?
Ag4 C55 Ag7 92.7(10) . . ?
Ag20 C55 Ag7 88.3(9) . . ?
C55 C56 C57 172(3) . . ?
C55 C56 Ag20 56.5(17) . . ?
C57 C56 Ag20 132(2) . . ?
C58 C57 C56 113(3) . . ?
C58 C57 C60 114(3) . . ?
C56 C57 C60 106(3) . . ?
C58 C57 C59 108(3) . . ?
C56 C57 C59 107(3) . . ?
C60 C57 C59 109(3) . . ?
C57 C58 H58A 109.5 . . ?
C57 C58 H58B 109.5 . . ?
H58A C58 H58B 109.5 . . ?
C57 C58 H58C 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C57 C59 H59A 109.5 . . ?
C57 C59 H59B 109.5 . . ?
H59A C59 H59B 109.5 . . ?
C57 C59 H59C 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C57 C60 H60A 109.5 . . ?
C57 C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C57 C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C64 C61 C63 111(2) . . ?
C64 C61 C62 109(2) . . ?
C63 C61 C62 110(2) . . ?
C64 C61 P1 110.0(19) . . ?
C63 C61 P1 109.2(18) . . ?
C62 C61 P1 107.7(17) . . ?
C61 C62 H62A 109.5 . . ?
C61 C62 H62B 109.5 . . ?
H62A C62 H62B 109.5 . . ?
C61 C62 H62C 109.5 . . ?
H62A C62 H62C 109.5 . . ?
H62B C62 H62C 109.5 . . ?
C61 C63 H63A 109.5 . . ?
C61 C63 H63B 109.5 . . ?
H63A C63 H63B 109.5 . . ?
C61 C63 H63C 109.5 . . ?
H63A C63 H63C 109.5 . . ?
H63B C63 H63C 109.5 . . ?
C61 C64 H64A 109.5 . . ?
C61 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C61 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C68 C65 C67 106(3) . . ?
C68 C65 C66 115(3) . . ?
C67 C65 C66 108(3) . . ?
C68 C65 P2 110(2) . . ?
C67 C65 P2 106(2) . . ?
C66 C65 P2 110.7(18) . . ?
C65 C66 H66A 109.5 . . ?
C65 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C65 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C65 C67 H67A 109.5 . . ?
C65 C67 H67B 109.5 . . ?
H67A C67 H67B 109.5 . . ?
C65 C67 H67C 109.5 . . ?
H67A C67 H67C 109.5 . . ?
H67B C67 H67C 109.5 . . ?
C65 C68 H68A 109.5 . . ?
C65 C68 H68B 109.5 . . ?
H68A C68 H68B 109.5 . . ?
C65 C68 H68C 109.5 . . ?
H68A C68 H68C 109.5 . . ?
H68B C68 H68C 109.5 . . ?
O9 C69 C70 131(3) . . ?
O9 C69 C72 119(3) . . ?
C70 C69 C72 111(3) . . ?
C71 C70 C69 121(2) . . ?
C71 C70 H70 119.7 . . ?
C69 C70 H70 119.7 . . ?
O10 C71 C70 129(3) . . ?
O10 C71 C73 114(3) . . ?
C70 C71 C73 117(2) . . ?
F7 C72 F8 112(4) . . ?
F7 C72 F9 106(4) . . ?
F8 C72 F9 98(3) . . ?
F7 C72 C69 115(3) . . ?
F8 C72 C69 117(3) . . ?
F9 C72 C69 107(3) . . ?
F10 C73 F11 107(2) . . ?
F10 C73 F12 108(3) . . ?
F11 C73 F12 106(3) . . ?
F10 C73 C71 117(3) . . ?
F11 C73 C71 110(2) . . ?
F12 C73 C71 109(2) . . ?
O7 C74 C77 117(3) . . ?
O7 C74 C75 130(3) . . ?
C77 C74 C75 113(3) . . ?
C74 C75 C76 120(4) . . ?
C74 C75 H75 120.2 . . ?
C76 C75 H75 120.2 . . ?
O8 C76 C75 134(4) . . ?
O8 C76 C78 112(4) . . ?
C75 C76 C78 114(4) . . ?
F3 C78 F2 107(2) . . ?
F3 C78 F1 105(2) . . ?
F2 C78 F1 106(2) . . ?
F3 C78 C76 109(3) . . ?
F2 C78 C76 116(3) . . ?
F1 C78 C76 113(4) . . ?
F5 C77 F6 99(2) . . ?
F5 C77 F4 97(2) . . ?
F6 C77 F4 97(2) . . ?
F5 C77 C74 124(3) . . ?
F6 C77 C74 117(3) . . ?
F4 C77 C74 117(3) . . ?
C80 C79 Ag17 136(2) . 3_656 ?
C80 C79 Ag15 133(2) . . ?
Ag17 C79 Ag15 82.0(8) 3_656 . ?
C80 C79 Ag6 120(2) . . ?
Ag17 C79 Ag6 82.8(7) 3_656 . ?
Ag15 C79 Ag6 85.4(9) . . ?
C79 C80 C81 177(3) . . ?
C80 C81 C82 110(2) . . ?
C80 C81 C83 112(2) . . ?
C82 C81 C83 108(3) . . ?
C80 C81 C84 109(2) . . ?
C82 C81 C84 109(3) . . ?
C83 C81 C84 109(3) . . ?
C81 C82 H82A 109.5 . . ?
C81 C82 H82B 109.5 . . ?
H82A C82 H82B 109.5 . . ?
C81 C82 H82C 109.5 . . ?
H82A C82 H82C 109.5 . . ?
H82B C82 H82C 109.5 . . ?
C81 C83 H83A 109.5 . . ?
C81 C83 H83B 109.5 . . ?
H83A C83 H83B 109.5 . . ?
C81 C83 H83C 109.5 . . ?
H83A C83 H83C 109.5 . . ?
H83B C83 H83C 109.5 . . ?
C81 C84 H84A 109.5 . . ?
C81 C84 H84B 109.5 . . ?
H84A C84 H84B 109.5 . . ?
C81 C84 H84C 109.5 . . ?
H84A C84 H84C 109.5 . . ?
H84B C84 H84C 109.5 . . ?
O11 C85 O12 137(4) . . ?
O11 C85 C86 112(4) . . ?
O12 C85 C86 111(4) . . ?
F13 C86 F15 103(2) . . ?
F13 C86 F14 103.2(19) . . ?
F15 C86 F14 102.7(19) . . ?
F13 C86 C85 112(2) . . ?
F15 C86 C85 117(3) . . ?
F14 C86 C85 116(3) . . ?
P1 O1 Ag5 128.9(9) . . ?
P1 O1 Ag6 129.4(8) . 3_656 ?
Ag5 O1 Ag6 96.7(6) . 3_656 ?
P1 O2 Ag8 121.1(9) . . ?
P1 O2 Ag12 101.4(8) . . ?
Ag8 O2 Ag12 108.9(6) . . ?
P1 O3 Ag17 122.0(9) . . ?
P2 O4 Ag19 121.4(11) . . ?
P2 O4 Ag10 110.1(9) . . ?
Ag19 O4 Ag10 102.6(7) . . ?
P2 O5 Ag16 116.9(10) . 3_656 ?
P2 O5 Ag9 137.1(10) . 3_656 ?
Ag16 O5 Ag9 74.1(5) 3_656 3_656 ?
P2 O6 Ag20 133.0(12) . . ?
C74 O7 Ag7 134(2) . . ?
C76 O8 Ag7 128(2) . . ?
C69 O9 Ag13 129(2) . . ?
C71 O10 Ag13 135(2) . . ?
C85 O11 Ag15 130(3) . . ?
C85 O12 Ag2 138(4) . . ?
V1 O13 Ag2 121.4(10) . 3_656 ?
V1 O13 Ag15 121.3(9) . 3_656 ?
Ag2 O13 Ag15 114.8(8) 3_656 3_656 ?
V1 O14 Ag10 117.9(10) . . ?
V1 O15 Ag12 126.2(9) . . ?
O2 P1 O3 110.8(10) . . ?
O2 P1 O1 112.3(10) . . ?
O3 P1 O1 111.2(9) . . ?
O2 P1 C61 108.9(11) . . ?
O3 P1 C61 106.2(11) . . ?
O1 P1 C61 107.3(11) . . ?
O6 P2 O4 110.7(12) . . ?
O6 P2 O5 110.7(10) . . ?
O4 P2 O5 111.1(10) . . ?
O6 P2 C65 108.8(13) . . ?
O4 P2 C65 106.6(12) . . ?
O5 P2 C65 108.9(11) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 C1 C2 Ag16 -91(3) . . . . ?
Ag2 C1 C2 Ag16 99(3) . . . . ?
Ag16 C2 C3 C6 107(3) . . . . ?
Ag16 C2 C3 C4 -132(2) . . . . ?
Ag16 C2 C3 C5 -13(4) . . . . ?
Ag4 C7 C8 Ag5 -111(6) . . . . ?
Ag4 C7 C8 Ag13 107.1(17) . . . . ?
Ag4 C7 C9 C12 68(3) . . . . ?
Ag4 C7 C9 C10 -171(2) . . . . ?
Ag4 C7 C9 C11 -52(4) . . . . ?
Ag19 C13 C14 Ag7 126(4) . . . . ?
Ag18 C13 C14 Ag7 -105(2) . . . . ?
Ag7 C14 C15 C16 171(2) . . . . ?
Ag7 C14 C15 C18 -66(3) . . . . ?
Ag7 C14 C15 C17 51(3) . . . . ?
Ag12 C19 C20 Ag10 80.3(7) . . . . ?
Ag19 C19 C20 Ag10 -91.6(8) . . . . ?
Ag10 C20 C21 C22A -38(2) . . . . ?
Ag10 C20 C21 C22B -101(3) . . . . ?
Ag10 C20 C21 C23A -159.8(17) . . . . ?
Ag10 C20 C21 C24A 82(2) . . . . ?
Ag10 C20 C21 C23B 137(3) . . . . ?
Ag10 C20 C21 C24B 18(3) . . . . ?
Ag3 C25 C26 Ag14 -165(5) . . . . ?
Ag12 C25 C26 Ag14 85.2(13) . . . . ?
Ag2 C25 C26 Ag14 -83.1(9) . . . . ?
Ag14 C26 C27 C28 8(3) . . . . ?
Ag14 C26 C27 C30 -108(3) . . . . ?
Ag14 C26 C27 C29 129(3) . . . . ?
Ag8 C31 C32 Ag18 118(4) . . . . ?
Ag13 C31 C32 Ag18 -87.1(16) . . . . ?
Ag18 C32 C33 C34 38(3) . . . . ?
Ag18 C32 C33 C36 -81(3) . . . . ?
Ag18 C32 C33 C35 158.9(18) . . . . ?
Ag3 C37 C38 Ag9 155(5) . . . 3_656 ?
Ag10 C37 C38 Ag9 -79.0(14) . . . 3_656 ?
Ag15 C37 C38 Ag9 81.4(7) . . . 3_656 ?
Ag9 C38 C39 C41 176.2(16) 3_656 . . . ?
Ag9 C38 C39 C42 56(2) 3_656 . . . ?
Ag9 C38 C39 C40 -63(2) 3_656 . . . ?
Ag6 C43 C44 C45 -121(12) . . . . ?
Ag1 C43 C44 C45 133(12) . . . . ?
Ag1 C43 C44 Ag6 -106.1(7) . . . . ?
Ag6 C43 C44 Ag1 106.1(7) . . . . ?
C43 C44 C45 C46 -72(12) . . . . ?
Ag6 C44 C45 C46 172.0(14) . . . . ?
Ag1 C44 C45 C46 56.5(19) . . . . ?
C43 C44 C45 C47 49(12) . . . . ?
Ag6 C44 C45 C47 -66.7(19) . . . . ?
Ag1 C44 C45 C47 177.8(14) . . . . ?
C43 C44 C45 C48 168(11) . . . . ?
Ag6 C44 C45 C48 52.5(19) . . . . ?
Ag1 C44 C45 C48 -63.0(19) . . . . ?
Ag4 C55 C56 Ag20 -116(8) . . . . ?
Ag7 C55 C56 Ag20 89.8(13) . . . . ?
Ag20 C56 C57 C58 -165(2) . . . . ?
Ag20 C56 C57 C60 -39(4) . . . . ?
Ag20 C56 C57 C59 77(4) . . . . ?
O9 C69 C70 C71 -6(5) . . . . ?
C72 C69 C70 C71 174(3) . . . . ?
C69 C70 C71 O10 4(5) . . . . ?
C69 C70 C71 C73 -179(2) . . . . ?
O9 C69 C72 F7 73(5) . . . . ?
C70 C69 C72 F7 -107(4) . . . . ?
O9 C69 C72 F8 -153(3) . . . . ?
C70 C69 C72 F8 27(4) . . . . ?
O9 C69 C72 F9 -44(5) . . . . ?
C70 C69 C72 F9 135(3) . . . . ?
O10 C71 C73 F10 171(3) . . . . ?
C70 C71 C73 F10 -7(4) . . . . ?
O10 C71 C73 F11 -67(3) . . . . ?
C70 C71 C73 F11 115(3) . . . . ?
O10 C71 C73 F12 49(4) . . . . ?
C70 C71 C73 F12 -129(3) . . . . ?
O7 C74 C75 C76 -1(6) . . . . ?
C77 C74 C75 C76 178(3) . . . . ?
C74 C75 C76 O8 1(8) . . . . ?
C74 C75 C76 C78 -177(3) . . . . ?
O8 C76 C78 F3 55(5) . . . . ?
C75 C76 C78 F3 -126(4) . . . . ?
O8 C76 C78 F2 176(4) . . . . ?
C75 C76 C78 F2 -5(5) . . . . ?
O8 C76 C78 F1 -62(5) . . . . ?
C75 C76 C78 F1 117(4) . . . . ?
O7 C74 C77 F5 167(3) . . . . ?
C75 C74 C77 F5 -12(5) . . . . ?
O7 C74 C77 F6 43(4) . . . . ?
C75 C74 C77 F6 -136(3) . . . . ?
O7 C74 C77 F4 -71(4) . . . . ?
C75 C74 C77 F4 109(4) . . . . ?
O11 C85 C86 F13 89(4) . . . . ?
O12 C85 C86 F13 -93(4) . . . . ?
O11 C85 C86 F15 -30(5) . . . . ?
O12 C85 C86 F15 147(4) . . . . ?
O11 C85 C86 F14 -152(3) . . . . ?
O12 C85 C86 F14 25(5) . . . . ?
C77 C74 O7 Ag7 -179(2) . . . . ?
C75 C74 O7 Ag7 0(5) . . . . ?
C75 C76 O8 Ag7 -1(8) . . . . ?
C78 C76 O8 Ag7 178(2) . . . . ?
C70 C69 O9 Ag13 -1(5) . . . . ?
C72 C69 O9 Ag13 178(2) . . . . ?
C70 C71 O10 Ag13 7(5) . . . . ?
C73 C71 O10 Ag13 -171(2) . . . . ?
O12 C85 O11 Ag15 21(9) . . . . ?
C86 C85 O11 Ag15 -163(2) . . . . ?
O11 C85 O12 Ag2 -22(10) . . . . ?
C86 C85 O12 Ag2 161(3) . . . . ?
O15 V1 O13 Ag2 156.6(12) . . . 3_656 ?
O14 V1 O13 Ag2 38.7(16) . . . 3_656 ?
O16 V1 O13 Ag2 -100.0(18) . . . 3_656 ?
O15 V1 O13 Ag15 -42.4(15) . . . 3_656 ?
O14 V1 O13 Ag15 -160.3(12) . . . 3_656 ?
O16 V1 O13 Ag15 61(2) . . . 3_656 ?
O15 V1 O14 Ag10 44.3(17) . . . . ?
O13 V1 O14 Ag10 162.1(12) . . . . ?
O16 V1 O14 Ag10 -63(2) . . . . ?
O13 V1 O15 Ag12 -166.3(13) . . . . ?
O14 V1 O15 Ag12 -48.7(19) . . . . ?
O16 V1 O15 Ag12 77(2) . . . . ?
Ag8 O2 P1 O3 162.5(9) . . . . ?
Ag12 O2 P1 O3 42.0(10) . . . . ?
Ag8 O2 P1 O1 37.4(14) . . . . ?
Ag12 O2 P1 O1 -83.1(9) . . . . ?
Ag8 O2 P1 C61 -81.1(14) . . . . ?
Ag12 O2 P1 C61 158.3(10) . . . . ?
Ag17 O3 P1 O2 -136.6(11) . . . . ?
Ag17 O3 P1 O1 -11.0(15) . . . . ?
Ag17 O3 P1 C61 105.4(13) . . . . ?
Ag5 O1 P1 O2 -44.4(15) . . . . ?
Ag6 O1 P1 O2 104.5(13) 3_656 . . . ?
Ag5 O1 P1 O3 -169.2(12) . . . . ?
Ag6 O1 P1 O3 -20.3(16) 3_656 . . . ?
Ag5 O1 P1 C61 75.2(16) . . . . ?
Ag6 O1 P1 C61 -136.0(13) 3_656 . . . ?
C64 C61 P1 O2 63(2) . . . . ?
C63 C61 P1 O2 -59(2) . . . . ?
C62 C61 P1 O2 -178.7(18) . . . . ?
C64 C61 P1 O3 -177.9(18) . . . . ?
C63 C61 P1 O3 60(2) . . . . ?
C62 C61 P1 O3 -59(2) . . . . ?
C64 C61 P1 O1 -59(2) . . . . ?
C63 C61 P1 O1 179.1(17) . . . . ?
C62 C61 P1 O1 60(2) . . . . ?
Ag20 O6 P2 O4 39(2) . . . . ?
Ag20 O6 P2 O5 162.8(15) . . . . ?
Ag20 O6 P2 C65 -78(2) . . . . ?
Ag19 O4 P2 O6 -32.8(15) . . . . ?
Ag10 O4 P2 O6 86.9(12) . . . . ?
Ag19 O4 P2 O5 -156.2(10) . . . . ?
Ag10 O4 P2 O5 -36.4(14) . . . . ?
Ag19 O4 P2 C65 85.4(14) . . . . ?
Ag10 O4 P2 C65 -154.9(11) . . . . ?
Ag16 O5 P2 O6 -2.9(15) 3_656 . . . ?
Ag9 O5 P2 O6 -98.3(17) 3_656 . . . ?
Ag16 O5 P2 O4 120.5(12) 3_656 . . . ?
Ag9 O5 P2 O4 25.2(19) 3_656 . . . ?
Ag16 O5 P2 C65 -122.4(13) 3_656 . . . ?
Ag9 O5 P2 C65 142.2(16) 3_656 . . . ?
C68 C65 P2 O6 -178(2) . . . . ?
C67 C65 P2 O6 -64(2) . . . . ?
C66 C65 P2 O6 53(2) . . . . ?
C68 C65 P2 O4 62(3) . . . . ?
C67 C65 P2 O4 176(2) . . . . ?
C66 C65 P2 O4 -67(2) . . . . ?
C68 C65 P2 O5 -58(3) . . . . ?
C67 C65 P2 O5 56(2) . . . . ?
C66 C65 P2 O5 174(2) . . . . ?

_refine_diff_density_max         2.062
_refine_diff_density_min         -2.057
_refine_diff_density_rms         0.330

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex6
_database_code_depnum_ccdc_archive 'CCDC 1584346'
_audit_update_record             
;
2018-01-15 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C228 H264 Ag48 F72 O38 V4'
_chemical_formula_weight         10361.90

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
V V 0.3005 0.5294 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   19.6076(11)
_cell_length_b                   27.3026(17)
_cell_length_c                   28.8060(16)
_cell_angle_alpha                88.022(2)
_cell_angle_beta                 85.9040(10)
_cell_angle_gamma                88.203(2)
_cell_volume                     15365.9(15)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9848
_cell_measurement_theta_min      2.9998
_cell_measurement_theta_max      27.9752

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.240
_exptl_crystal_F_000             9864
_exptl_transmission_factor_min   0.5945
_exptl_transmission_factor_max   0.7456
_exptl_crystal_size_max          0.156
_exptl_crystal_size_mid          0.121
_exptl_crystal_size_min          0.083
_exptl_absorpt_coefficient_mu    3.189
_shelx_estimated_absorpt_T_min   0.636
_shelx_estimated_absorpt_T_max   0.778
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            86717
_diffrn_reflns_av_unetI/netI     0.0349
_diffrn_reflns_av_R_equivalents  0.0223
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_theta_min         2.802
_diffrn_reflns_theta_max         23.257
_diffrn_reflns_theta_full        23.257
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measured_fraction_theta_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_point_group_measured_fraction_full 0.996
_reflns_number_total             43946
_reflns_number_gt                34950
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0159P)²+119.1925P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         43946
_refine_ls_number_parameters     3773
_refine_ls_number_restraints     1845
_refine_ls_R_factor_all          0.0557
_refine_ls_R_factor_gt           0.0389
_refine_ls_wR_factor_ref         0.0909
_refine_ls_wR_factor_gt          0.0807
_refine_ls_goodness_of_fit_ref   1.058
_refine_ls_restrained_S_all      1.046
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.48808(4) 1.16005(2) 0.00201(2) 0.05312(17) Uani 1 1 d . . . . .
Ag2 Ag 0.38691(4) 1.08853(3) 0.01248(3) 0.0650(2) Uani 1 1 d . . . . .
Ag3A Ag 0.3801(2) 0.9071(4) 0.1012(4) 0.0636(17) Uani 0.326(19) 1 d . . P A 1
Ag3B Ag 0.3684(3) 0.8872(3) 0.0869(2) 0.085(2) Uani 0.674(19) 1 d . . P A 2
Ag4A Ag 0.3041(5) 0.9921(2) 0.0728(8) 0.0668(15) Uani 0.56(6) 1 d . . P A 1
Ag4B Ag 0.3005(4) 0.9931(3) 0.0651(3) 0.0525(15) Uani 0.44(6) 1 d . . P A 2
Ag5 Ag 0.27864(5) 0.90318(3) 0.01115(3) 0.0793(3) Uani 1 1 d . . . . .
Ag6 Ag 0.57278(3) 0.98798(3) -0.10645(3) 0.05689(18) Uani 1 1 d . . . . .
Ag7 Ag 0.41198(3) 1.01166(3) -0.13522(2) 0.05437(17) Uani 1 1 d . . . . .
Ag8 Ag 0.28352(3) 1.02046(3) -0.06732(2) 0.05136(17) Uani 1 1 d . . . . .
Ag9 Ag 0.32669(3) 0.92773(2) -0.10506(2) 0.04529(15) Uani 1 1 d . . . . .
Ag10 Ag 0.51448(4) 0.87908(2) -0.09994(2) 0.05526(17) Uani 1 1 d . . . . .
Ag11 Ag 0.38255(3) 0.83882(2) -0.05308(3) 0.05413(17) Uani 1 1 d . . . . .
Ag12 Ag 0.47959(4) 1.08539(3) -0.08382(3) 0.06078(19) Uani 1 1 d . . . . .
Ag13 Ag -0.07576(3) 0.60485(2) -0.14067(2) 0.05031(16) Uani 1 1 d . . . . .
Ag14 Ag 0.06986(3) 0.55835(3) -0.17216(2) 0.05547(18) Uani 1 1 d . . . . .
Ag15 Ag -0.07367(4) 0.50290(3) -0.17407(2) 0.05500(18) Uani 1 1 d . . . . .
Ag16 Ag 0.127(3) 0.4465(17) -0.123(4) 0.076(14) Uani 0.07(2) 1 d . . P B 1
A16 Ag 0.11949(9) 0.45491(10) -0.1439(2) 0.0537(8) Uani 0.93(2) 1 d . . P B 2
Ag17 Ag 0.16130(3) 0.55230(2) -0.09249(2) 0.04617(15) Uani 1 1 d . . . . .
Ag18 Ag 0.10793(3) 0.59076(2) 0.00961(2) 0.04475(15) Uani 1 1 d . . . . .
Ag19 Ag 0.16437(3) 0.48277(2) -0.01006(2) 0.05156(16) Uani 1 1 d . . . . .
Ag20 Ag 0.07075(3) 0.40535(3) -0.04108(2) 0.05038(16) Uani 1 1 d . . . . .
Ag21 Ag 0.12986(3) 0.37350(2) 0.04587(2) 0.04787(16) Uani 1 1 d . . . . .
Ag22 Ag -0.02933(3) 0.34519(2) 0.08068(3) 0.05796(19) Uani 1 1 d . . . . .
Ag23 Ag 0.18485(3) 0.50207(3) 0.09732(3) 0.0690(2) Uani 1 1 d . . . . .
Ag24 Ag 0.06027(3) 0.58762(2) 0.10609(2) 0.04614(15) Uani 1 1 d . . . . .
Ag25 Ag 0.48342(3) 0.60245(2) 0.35964(2) 0.04494(15) Uani 1 1 d . . . . .
Ag26 Ag 0.31411(3) 0.56012(2) 0.39329(2) 0.04490(15) Uani 1 1 d . . . . .
Ag27 Ag 0.58247(3) 0.50303(2) 0.35296(2) 0.03648(13) Uani 1 1 d . . . . .
Ag28 Ag 0.43266(3) 0.50507(2) 0.33074(2) 0.04122(14) Uani 1 1 d . . . . .
Ag29 Ag 0.32372(3) 0.44563(2) 0.39153(2) 0.04924(16) Uani 1 1 d . . . . .
Ag30 Ag 0.26740(3) 0.52275(2) 0.49403(3) 0.05375(17) Uani 1 1 d . . . . .
Ag31 Ag 0.45821(3) 0.38378(2) 0.38740(2) 0.04574(15) Uani 1 1 d . . . . .
Ag32 Ag 0.35331(3) 0.38840(2) 0.48060(2) 0.03907(14) Uani 1 1 d . . . . .
Ag33 Ag 0.64535(3) 0.38483(2) 0.52418(2) 0.03746(13) Uani 1 1 d . . . . .
Ag34 Ag 0.47076(3) 0.38679(2) 0.53176(2) 0.04568(15) Uani 1 1 d . . . . .
Ag35 Ag 0.34979(3) 0.46567(2) 0.57147(2) 0.04318(14) Uani 1 1 d . . . . .
Ag36 Ag 0.58622(3) 0.41886(2) 0.44180(2) 0.04178(14) Uani 1 1 d . . . . .
Ag37 Ag 0.03928(5) -0.03119(3) 0.65489(3) 0.0814(3) Uani 1 1 d . . . . .
Ag38 Ag 0.17652(4) 0.01083(3) 0.63362(2) 0.06102(19) Uani 1 1 d . . . . .
Ag39 Ag 0.14889(3) -0.08134(2) 0.58055(2) 0.04043(14) Uani 1 1 d . . . . .
Ag40 Ag 0.12040(3) -0.07710(3) 0.46883(2) 0.05328(17) Uani 1 1 d . . . . .
Ag41 Ag 0.2208(2) -0.00898(13) 0.4641(2) 0.0486(16) Uani 0.274(7) 1 d . . P C 1
A41A Ag 0.24487(11) 0.00162(6) 0.48816(10) 0.0546(8) Uani 0.726(7) 1 d . . P C
2
Ag42 Ag 0.08813(4) 0.01771(3) 0.40429(2) 0.05964(19) Uani 1 1 d . . . . .
Ag43 Ag 0.15625(3) 0.09505(2) 0.44904(2) 0.04519(15) Uani 1 1 d . . . . .
Ag44 Ag -0.01318(3) 0.10830(2) 0.43619(2) 0.04145(14) Uani 1 1 d . . . . .
Ag45 Ag 0.024(2) 0.1543(8) 0.5324(10) 0.082(6) Uani 0.30(4) 1 d . . P C 1
A45A Ag 0.0421(2) 0.16147(17) 0.5449(3) 0.0580(10) Uani 0.70(4) 1 d . . P C 2
Ag46 Ag 0.2189(6) 0.0759(15) 0.5401(2) 0.083(5) Uani 0.41(4) 1 d . . P C 1
A46A Ag 0.2101(3) 0.0960(2) 0.54044(15) 0.0455(13) Uani 0.59(4) 1 d . . P C 2
Ag47 Ag -0.04699(3) 0.09612(2) 0.61505(2) 0.04572(15) Uani 1 1 d . . . . .
Ag48 Ag 0.1040(8) 0.1146(14) 0.6151(16) 0.078(5) Uani 0.24(4) 1 d . . P C 1
A48 Ag 0.1013(3) 0.1033(3) 0.62592(19) 0.0560(11) Uani 0.76(4) 1 d . . P C 2
V1 V 0.43537(6) 0.96482(4) -0.01763(4) 0.0312(3) Uani 1 1 d . . . . .
V2 V 0.00714(6) 0.47987(4) 0.05882(4) 0.0269(3) Uani 1 1 d . . . . .
V3 V 0.45071(6) 0.50224(4) 0.45241(4) 0.0272(3) Uani 1 1 d . . . . .
V4 V 0.06099(6) 0.02446(4) 0.53397(4) 0.0280(3) Uani 1 1 d . . . . .
F1 F 0.4976(4) 0.7302(3) 0.0369(2) 0.102(2) Uani 1 1 d . . . . .
F2 F 0.3932(5) 0.7307(4) 0.0222(3) 0.151(4) Uani 1 1 d . . . . .
F3 F 0.4275(6) 0.6876(3) 0.0798(3) 0.163(4) Uani 1 1 d . . . . .
F4 F 0.3559(5) 0.8166(3) 0.2447(3) 0.135(3) Uani 1 1 d . . . . .
F5 F 0.4319(6) 0.7647(4) 0.2324(3) 0.182(5) Uani 1 1 d . . . . .
F6 F 0.3341(8) 0.7495(4) 0.2206(3) 0.214(7) Uani 1 1 d . . . . .
F7 F 0.6415(8) 0.8842(5) -0.2577(5) 0.243(8) Uani 1 1 d . . . . .
F8 F 0.5848(6) 0.8381(6) -0.2863(4) 0.224(7) Uani 1 1 d . . . . .
F9 F 0.6414(6) 0.8147(5) -0.2336(3) 0.215(7) Uani 1 1 d . . . . .
F10 F 0.3035(4) 0.8839(3) -0.1992(3) 0.119(3) Uani 1 1 d . . . . .
F11 F 0.3313(5) 0.8129(4) -0.1869(5) 0.186(5) Uani 1 1 d . . . . .
F12 F 0.3517(4) 0.8445(4) -0.2532(3) 0.169(5) Uani 1 1 d . . . . .
F13 F 0.0537(5) 1.0352(6) 0.0601(3) 0.258(9) Uani 1 1 d . . . . .
F14 F 0.1483(5) 1.0181(5) 0.0899(3) 0.198(6) Uani 1 1 d . . . . .
F15 F 0.1044(6) 0.9681(7) 0.0473(4) 0.207(7) Uani 1 1 d . . . . .
F16 F 0.0385(5) 1.1292(4) -0.0724(4) 0.160(4) Uani 1 1 d . . . . .
F17 F 0.1194(5) 1.1437(4) -0.1225(4) 0.187(5) Uani 1 1 d . . . . .
F18 F 0.0697(6) 1.0761(4) -0.1219(4) 0.181(5) Uani 1 1 d . . . . .
F19 F -0.2638(4) 0.3145(3) 0.0159(3) 0.131(3) Uani 1 1 d . . . . .
F20 F -0.1930(4) 0.2568(4) 0.0050(3) 0.147(4) Uani 1 1 d . . . . .
F21 F -0.2705(4) 0.2523(3) 0.0566(3) 0.123(3) Uani 1 1 d . . . . .
F22 F -0.1965(5) 0.3654(3) 0.2237(2) 0.128(3) Uani 1 1 d . . . . .
F23 F -0.1896(5) 0.2900(3) 0.2227(3) 0.145(4) Uani 1 1 d . . . . .
F24 F -0.2754(4) 0.3286(4) 0.1992(3) 0.158(4) Uani 1 1 d . . . . .
F25 F 0.3116(3) 0.3397(3) 0.1844(2) 0.095(2) Uani 1 1 d . . . . .
F26 F 0.2043(3) 0.3515(3) 0.1927(2) 0.102(2) Uani 1 1 d . . . . .
F27 F 0.2486(4) 0.3150(2) 0.1339(2) 0.097(2) Uani 1 1 d . . . . .
F28 F 0.4221(3) 0.5224(3) 0.0960(3) 0.130(3) Uani 1 1 d . . . . .
F29 F 0.4384(3) 0.4703(3) 0.0477(3) 0.121(3) Uani 1 1 d . . . . .
F30 F 0.4570(3) 0.4523(3) 0.1163(3) 0.128(3) Uani 1 1 d . . . . .
F31 F 0.2043(5) 0.2936(4) -0.2380(3) 0.156(4) Uani 1 1 d . . . . .
F32 F 0.1830(7) 0.2722(4) -0.1704(5) 0.267(9) Uani 1 1 d . . . . .
F33 F 0.2572(6) 0.3185(4) -0.1889(5) 0.184(5) Uani 1 1 d . . . . .
F34 F 0.0313(4) 0.3829(3) -0.3002(2) 0.109(2) Uani 1 1 d . . . . .
F35 F -0.0553(4) 0.3797(4) -0.2517(3) 0.154(4) Uani 1 1 d . . . . .
F36 F -0.0122(6) 0.4477(3) -0.2715(3) 0.162(4) Uani 1 1 d . . . . .
F37 F 0.0587(3) 0.5013(3) 0.5902(2) 0.101(2) Uani 1 1 d . . . . .
F38 F 0.1332(3) 0.4752(3) 0.63605(19) 0.091(2) Uani 1 1 d . . . . .
F39 F 0.0684(3) 0.4251(3) 0.6068(2) 0.102(2) Uani 1 1 d . . . . .
F40A F 0.0732(6) 0.3973(18) 0.4447(9) 0.137(15) Uani 0.55(4) 1 d D . P D 1
F41A F 0.1682(15) 0.3586(6) 0.4395(12) 0.119(11) Uani 0.55(4) 1 d D . P D 1
F42A F 0.1586(15) 0.4184(10) 0.3962(4) 0.106(11) Uani 0.55(4) 1 d D . P D 1
F40B F 0.095(3) 0.4284(11) 0.4172(19) 0.19(3) Uani 0.45(4) 1 d D . P D 2
F41B F 0.0948(19) 0.3689(12) 0.4612(12) 0.158(15) Uani 0.45(4) 1 d D . P D 2
F42B F 0.1735(12) 0.3677(12) 0.4176(13) 0.127(17) Uani 0.45(4) 1 d D . P D 2
F43 F 0.2665(4) 0.7328(3) 0.3240(4) 0.172(5) Uani 1 1 d . . . . .
F44 F 0.2451(4) 0.6965(3) 0.3854(3) 0.147(3) Uani 1 1 d . . . . .
F45 F 0.2562(4) 0.6574(4) 0.3267(4) 0.169(5) Uani 1 1 d . . . . .
F46 F 0.5506(4) 0.7593(2) 0.2997(3) 0.108(2) Uani 1 1 d . . . . .
F47 F 0.4707(4) 0.8063(2) 0.3255(3) 0.112(2) Uani 1 1 d . . . . .
F48 F 0.5450(5) 0.7803(3) 0.3695(3) 0.138(3) Uani 1 1 d . . . . .
F49 F 0.6269(6) 0.2703(3) 0.2680(3) 0.196(6) Uani 1 1 d . . . . .
F50 F 0.5554(5) 0.2427(3) 0.3144(4) 0.165(4) Uani 1 1 d . . . . .
F51 F 0.6416(5) 0.2643(3) 0.3364(4) 0.171(5) Uani 1 1 d . . . . .
F52 F 0.4364(9) 0.4068(11) 0.2187(8) 0.117(14) Uani 0.54(3) 1 d D . P E 1
F53 F 0.5384(11) 0.4036(8) 0.1944(4) 0.082(7) Uani 0.54(3) 1 d D . P E 1
F54 F 0.5001(17) 0.4663(4) 0.2259(4) 0.102(12) Uani 0.54(3) 1 d D . P E 1
F52A F 0.4377(11) 0.4507(11) 0.2347(5) 0.087(8) Uani 0.46(3) 1 d D . P E 2
F53A F 0.475(2) 0.3886(6) 0.2018(9) 0.121(17) Uani 0.46(3) 1 d D . P E 2
F54A F 0.5383(9) 0.4476(12) 0.2077(10) 0.120(15) Uani 0.46(3) 1 d D . P E 2
F55 F 0.3212(6) -0.0688(5) 0.6273(4) 0.183(5) Uani 1 1 d . . . . .
F56 F 0.3157(7) -0.1368(5) 0.6071(4) 0.211(6) Uani 1 1 d . . . . .
F57 F 0.4090(4) -0.1024(6) 0.5985(4) 0.221(7) Uani 1 1 d . . . . .
F58 F 0.3940(4) -0.1446(3) 0.4120(3) 0.143(3) Uani 1 1 d . . . . .
F59 F 0.4732(4) -0.1148(3) 0.4447(3) 0.138(3) Uani 1 1 d . . . . .
F60 F 0.4249(4) -0.0730(3) 0.3915(3) 0.139(3) Uani 1 1 d . . . . .
F61 F 0.0797(4) 0.1242(3) 0.7292(3) 0.111(2) Uani 1 1 d . . . . .
F62 F -0.0271(4) 0.1383(3) 0.7344(2) 0.107(2) Uani 1 1 d . . . . .
F63 F 0.0237(5) 0.1129(3) 0.7936(2) 0.132(3) Uani 1 1 d . . . . .
F64 F -0.0242(7) -0.0447(4) 0.8421(3) 0.189(5) Uani 1 1 d . . . . .
F65 F -0.0202(10) -0.1037(5) 0.7999(4) 0.252(9) Uani 1 1 d . . . . .
F66 F -0.1069(7) -0.0617(7) 0.8105(4) 0.243(8) Uani 1 1 d . . . . .
F67 F -0.0186(8) 0.2946(5) 0.4397(6) 0.212(7) Uani 1 1 d . . . . .
F68 F -0.0182(7) 0.2395(4) 0.3947(4) 0.208(6) Uani 1 1 d . . . . .
F69 F 0.0571(6) 0.2931(4) 0.3927(4) 0.198(6) Uani 1 1 d . . . . .
F70 F 0.2541(8) 0.2768(6) 0.4695(12) 0.115(11) Uani 0.61(4) 1 d D . P F 1
F71 F 0.2526(14) 0.2371(14) 0.5332(6) 0.165(14) Uani 0.61(4) 1 d D . P F 1
F72 F 0.2869(6) 0.2017(6) 0.4733(10) 0.104(10) Uani 0.61(4) 1 d D . P F 1
F70A F 0.2375(16) 0.2789(9) 0.5066(16) 0.124(14) Uani 0.39(4) 1 d D . P F 2
F71A F 0.2836(14) 0.2130(13) 0.5186(14) 0.118(16) Uani 0.39(4) 1 d D . P F 2
F72A F 0.2760(15) 0.239(3) 0.4482(6) 0.18(3) Uani 0.39(4) 1 d D . P F 2
O1 O 0.4544(3) 0.94941(18) -0.07302(17) 0.0431(13) Uani 1 1 d . . . . .
O2 O 0.4287(4) 0.9159(2) 0.0177(2) 0.087(2) Uani 1 1 d . . . . .
O3 O 0.3635(4) 0.9979(3) -0.0139(2) 0.105(3) Uani 1 1 d . . . . .
O4 O 0.5150(6) 0.9841(4) 0.0016(5) 0.054(3) Uani 0.5 1 d . . P . .
O5 O 0.4257(4) 0.8150(3) 0.0650(2) 0.083(2) Uani 1 1 d . . . . .
O6 O 0.3919(4) 0.8478(3) 0.1598(2) 0.079(2) Uani 1 1 d . . . . .
O7 O 0.5662(3) 0.8820(3) -0.1756(2) 0.0733(19) Uani 1 1 d . . . . .
O8 O 0.4191(3) 0.8899(2) -0.15605(19) 0.0570(15) Uani 1 1 d . . . . .
O9 O 0.2047(4) 1.0851(3) -0.0782(3) 0.096(3) Uani 1 1 d . . . . .
O10 O 0.2161(4) 1.0248(3) 0.0050(2) 0.095(3) Uani 1 1 d . . . . .
O11 O -0.0221(2) 0.52541(19) 0.09357(17) 0.0421(13) Uani 1 1 d . . . . .
O12 O 0.0895(2) 0.46545(19) 0.06674(17) 0.0403(12) Uani 1 1 d . . . . .
O13 O 0.0000 0.5000 0.0000 0.062(2) Uani 1 2 d S . P . .
O14 O -0.0404(2) 0.43046(18) 0.07065(18) 0.0400(12) Uani 1 1 d . . . . .
O15 O 0.0308(3) 0.4238(3) -0.1877(2) 0.075(2) Uani 1 1 d . . . . .
O16 O 0.1479(4) 0.3714(2) -0.1501(2) 0.0697(18) Uani 1 1 d . . . . .
O17 O -0.1272(3) 0.3215(2) 0.05001(19) 0.0569(16) Uani 1 1 d . . . . .
O18 O -0.1200(3) 0.3534(2) 0.1463(2) 0.0596(16) Uani 1 1 d . . . . .
O19 O 0.3002(3) 0.4885(2) 0.0761(2) 0.0611(16) Uani 1 1 d . . . . .
O20 O 0.2064(3) 0.4158(2) 0.1198(2) 0.0547(15) Uani 1 1 d . . . . .
O21 O 0.4507(3) 0.55981(18) 0.42915(17) 0.0418(13) Uani 1 1 d . . . . .
O22 O 0.4837(3) 0.46181(18) 0.41368(17) 0.0423(13) Uani 1 1 d . . . . .
O23 O 0.4791(6) 0.4929(5) 0.5091(4) 0.057(4) Uani 0.5 1 d . . P . .
O24 O 0.3725(3) 0.4871(2) 0.4709(3) 0.100(3) Uani 1 1 d . . . . .
O25 O 0.2075(3) 0.4849(2) 0.55688(19) 0.0537(15) Uani 1 1 d . . . . .
O26 O 0.2260(3) 0.4479(2) 0.4633(2) 0.0547(15) Uani 1 1 d . . . . .
O27 O 0.4919(3) 0.42231(18) 0.31103(18) 0.0443(13) Uani 1 1 d . . . . .
O28 O 0.5506(3) 0.3362(2) 0.3576(2) 0.0531(15) Uani 1 1 d . . . . .
O29 O 0.3716(3) 0.6419(2) 0.3690(2) 0.0579(16) Uani 1 1 d . . . . .
O30 O 0.5049(3) 0.6861(2) 0.3641(2) 0.0635(17) Uani 1 1 d . . . . .
O31 O 0.0749(3) 0.0822(2) 0.5163(2) 0.0685(19) Uani 1 1 d . . . . .
O32 O 0.1346(3) -0.00797(19) 0.52751(19) 0.0461(13) Uani 1 1 d . . . . .
O33 O 0.0301(3) 0.02269(18) 0.58996(16) 0.0388(12) Uani 1 1 d . . . . .
O34 O 0.0000 0.0000 0.5000 0.108(5) Uani 1 2 d S . P . .
O35 O 0.2686(3) -0.0584(3) 0.5452(3) 0.087(2) Uani 1 1 d . . . . .
O36 O 0.3105(4) -0.0613(3) 0.4463(3) 0.087(2) Uani 1 1 d . . . . .
O37 O -0.0264(4) -0.0482(3) 0.7229(2) 0.093(3) Uani 1 1 d D . . . .
O38 O 0.0168(4) 0.0504(3) 0.6913(2) 0.084(2) Uani 1 1 d D . . . .
O39 O 0.1564(4) 0.1813(3) 0.5129(3) 0.096(3) Uani 1 1 d . . . . .
O40 O 0.0245(4) 0.1996(2) 0.4723(2) 0.076(2) Uani 1 1 d . . . . .
C1 C 0.3510(5) 1.0617(4) 0.0843(3) 0.059(2) Uani 1 1 d . U . . .
C2 C 0.3198(5) 1.0994(4) 0.0859(4) 0.067(3) Uani 1 1 d . U . . .
C3 C 0.2754(6) 1.1460(5) 0.0939(5) 0.093(3) Uani 1 1 d . U . . .
C4 C 0.2334(7) 1.1563(6) 0.0506(6) 0.149(6) Uani 1 1 d . U . . .
H4A H 0.2040 1.1286 0.0467 0.224 Uiso 1 1 calc R U . . .
H4B H 0.2051 1.1862 0.0551 0.224 Uiso 1 1 calc R U . . .
H4C H 0.2648 1.1606 0.0228 0.224 Uiso 1 1 calc R U . . .
C5 C 0.3205(7) 1.1886(5) 0.0998(5) 0.118(5) Uani 1 1 d . U . . .
H5A H 0.3478 1.1954 0.0706 0.177 Uiso 1 1 calc R U . . .
H5B H 0.2920 1.2176 0.1080 0.177 Uiso 1 1 calc R U . . .
H5C H 0.3511 1.1806 0.1246 0.177 Uiso 1 1 calc R U . . .
C6 C 0.2326(9) 1.1352(6) 0.1395(6) 0.178(8) Uani 1 1 d . U . . .
H6A H 0.2033 1.1074 0.1356 0.267 Uiso 1 1 calc R U . . .
H6B H 0.2631 1.1271 0.1644 0.267 Uiso 1 1 calc R U . . .
H6C H 0.2040 1.1641 0.1478 0.267 Uiso 1 1 calc R U . . .
C7 C 0.4106(5) 1.1381(4) -0.0452(3) 0.064(3) Uani 1 1 d . U . . .
C8 C 0.3913(5) 1.1549(3) -0.0807(4) 0.060(2) Uani 1 1 d . U . . .
C9 C 0.3628(6) 1.1797(4) -0.1226(4) 0.087(3) Uani 1 1 d . U . . .
C10 C 0.2875(8) 1.1940(7) -0.1074(8) 0.194(8) Uani 1 1 d . U . . .
H10A H 0.2865 1.2172 -0.0822 0.291 Uiso 1 1 calc R U . . .
H10B H 0.2653 1.2092 -0.1340 0.291 Uiso 1 1 calc R U . . .
H10C H 0.2630 1.1645 -0.0965 0.291 Uiso 1 1 calc R U . . .
C11 C 0.3958(8) 1.2264(5) -0.1339(5) 0.133(5) Uani 1 1 d . U . . .
H11A H 0.3953 1.2456 -0.1057 0.199 Uiso 1 1 calc R U . . .
H11B H 0.4431 1.2202 -0.1459 0.199 Uiso 1 1 calc R U . . .
H11C H 0.3709 1.2448 -0.1575 0.199 Uiso 1 1 calc R U . . .
C12 C 0.3580(13) 1.1455(5) -0.1599(6) 0.225(10) Uani 1 1 d . U . . .
H12A H 0.3349 1.1160 -0.1474 0.338 Uiso 1 1 calc R U . . .
H12B H 0.3318 1.1610 -0.1844 0.338 Uiso 1 1 calc R U . . .
H12C H 0.4041 1.1364 -0.1728 0.338 Uiso 1 1 calc R U . . .
C13 C 0.5156(4) 1.0446(3) -0.1426(3) 0.055(2) Uani 1 1 d . U . . .
C14 C 0.5233(4) 1.0377(3) -0.1834(3) 0.055(2) Uani 1 1 d . U . . .
C15 C 0.5386(7) 1.0329(5) -0.2337(4) 0.099(4) Uani 1 1 d . U . . .
C16 C 0.5230(13) 1.0798(7) -0.2571(5) 0.208(8) Uani 1 1 d . U . . .
H16A H 0.5330 1.0771 -0.2907 0.312 Uiso 1 1 calc R U . . .
H16B H 0.4744 1.0886 -0.2506 0.312 Uiso 1 1 calc R U . . .
H16C H 0.5510 1.1053 -0.2455 0.312 Uiso 1 1 calc R U . . .
C17 C 0.6162(9) 1.0148(11) -0.2407(6) 0.221(9) Uani 1 1 d . U . . .
C18 C 0.4982(8) 0.9922(6) -0.2512(4) 0.129(5) Uani 1 1 d . U . . .
H18A H 0.5099 0.9613 -0.2348 0.194 Uiso 1 1 calc R U . . .
H18B H 0.4492 0.9998 -0.2454 0.194 Uiso 1 1 calc R U . . .
H18C H 0.5092 0.9890 -0.2847 0.194 Uiso 1 1 calc R U . . .
C19 C 0.2646(5) 0.9210(4) 0.0851(3) 0.062(2) Uani 1 1 d . U . . .
C20 C 0.2287(4) 0.8902(3) 0.1020(3) 0.053(2) Uani 1 1 d . U . . .
C21 C 0.1820(6) 0.8547(5) 0.1259(4) 0.087(3) Uani 1 1 d . U . . .
C22 C 0.1104(6) 0.8662(7) 0.1142(7) 0.167(7) Uani 1 1 d . U . . .
H22A H 0.1081 0.8671 0.0803 0.251 Uiso 1 1 calc R U . . .
H22B H 0.0803 0.8409 0.1281 0.251 Uiso 1 1 calc R U . . .
H22C H 0.0955 0.8982 0.1264 0.251 Uiso 1 1 calc R U . . .
C23 C 0.1921(10) 0.8523(9) 0.1742(5) 0.231(11) Uani 1 1 d . U . . .
H23A H 0.1609 0.8287 0.1899 0.346 Uiso 1 1 calc R U . . .
H23B H 0.2395 0.8419 0.1788 0.346 Uiso 1 1 calc R U . . .
H23C H 0.1829 0.8847 0.1872 0.346 Uiso 1 1 calc R U . . .
C24 C 0.2013(10) 0.8041(6) 0.1048(8) 0.194(8) Uani 1 1 d . U . . .
H24A H 0.1945 0.8056 0.0715 0.291 Uiso 1 1 calc R U . . .
H24B H 0.2494 0.7958 0.1094 0.291 Uiso 1 1 calc R U . . .
H24C H 0.1723 0.7790 0.1204 0.291 Uiso 1 1 calc R U . . .
C25 C 0.4837(4) 0.8062(3) -0.0640(3) 0.047(2) Uani 1 1 d . U . . .
C26 C 0.4860(4) 0.7708(3) -0.0872(3) 0.0446(19) Uani 1 1 d . U . . .
C27 C 0.4906(5) 0.7256(3) -0.1138(4) 0.064(2) Uani 1 1 d . U . . .
C28 C 0.5396(9) 0.7324(5) -0.1566(6) 0.180(8) Uani 1 1 d . U . . .
H28A H 0.5242 0.7606 -0.1755 0.270 Uiso 1 1 calc R U . . .
H28B H 0.5855 0.7381 -0.1469 0.270 Uiso 1 1 calc R U . . .
H28C H 0.5409 0.7028 -0.1750 0.270 Uiso 1 1 calc R U . . .
C29 C 0.4228(7) 0.7159(5) -0.1311(5) 0.126(5) Uani 1 1 d . U . . .
H29A H 0.4086 0.7436 -0.1511 0.188 Uiso 1 1 calc R U . . .
H29B H 0.4261 0.6859 -0.1489 0.188 Uiso 1 1 calc R U . . .
H29C H 0.3891 0.7119 -0.1046 0.188 Uiso 1 1 calc R U . . .
C30 C 0.5106(12) 0.6844(5) -0.0843(6) 0.206(9) Uani 1 1 d . U . . .
H30A H 0.5136 0.6545 -0.1024 0.309 Uiso 1 1 calc R U . . .
H30B H 0.5553 0.6903 -0.0727 0.309 Uiso 1 1 calc R U . . .
H30C H 0.4766 0.6805 -0.0580 0.309 Uiso 1 1 calc R U . . .
C31 C 0.3056(4) 0.9991(3) -0.1406(3) 0.0445(19) Uani 1 1 d . U . . .
C32 C 0.2775(4) 1.0080(3) -0.1759(3) 0.0439(18) Uani 1 1 d . U . . .
C33 C 0.2418(5) 1.0189(4) -0.2182(3) 0.064(2) Uani 1 1 d . U . . .
C34 C 0.2850(6) 0.9984(5) -0.2601(3) 0.097(4) Uani 1 1 d . U . . .
H34A H 0.2616 1.0055 -0.2886 0.145 Uiso 1 1 calc R U . . .
H34B H 0.3297 1.0137 -0.2628 0.145 Uiso 1 1 calc R U . . .
H34C H 0.2914 0.9628 -0.2557 0.145 Uiso 1 1 calc R U . . .
C35 C 0.2306(7) 1.0738(5) -0.2238(4) 0.108(4) Uani 1 1 d . U . . .
H35A H 0.2068 1.0814 -0.2521 0.162 Uiso 1 1 calc R U . . .
H35B H 0.2029 1.0859 -0.1967 0.162 Uiso 1 1 calc R U . . .
H35C H 0.2749 1.0897 -0.2263 0.162 Uiso 1 1 calc R U . . .
C36 C 0.1738(5) 0.9941(5) -0.2145(4) 0.096(4) Uani 1 1 d . U . . .
H36A H 0.1500 1.0014 -0.2428 0.144 Uiso 1 1 calc R U . . .
H36B H 0.1813 0.9585 -0.2107 0.144 Uiso 1 1 calc R U . . .
H36C H 0.1458 1.0062 -0.1875 0.144 Uiso 1 1 calc R U . . .
C37 C 0.2826(4) 0.8673(3) -0.0554(3) 0.049(2) Uani 1 1 d . U . . .
C38 C 0.2238(4) 0.8786(3) -0.0636(3) 0.0474(19) Uani 1 1 d . U . . .
C39 C 0.1520(5) 0.8854(4) -0.0763(3) 0.062(2) Uani 1 1 d . U . . .
C40 C 0.1054(5) 0.8594(5) -0.0386(4) 0.103(4) Uani 1 1 d . U . . .
H40A H 0.0577 0.8635 -0.0464 0.154 Uiso 1 1 calc R U . . .
H40B H 0.1181 0.8244 -0.0370 0.154 Uiso 1 1 calc R U . . .
H40C H 0.1108 0.8738 -0.0084 0.154 Uiso 1 1 calc R U . . .
C41 C 0.1457(6) 0.8613(5) -0.1231(4) 0.098(4) Uani 1 1 d . U . . .
H41A H 0.0986 0.8654 -0.1321 0.148 Uiso 1 1 calc R U . . .
H41B H 0.1768 0.8769 -0.1469 0.148 Uiso 1 1 calc R U . . .
H41C H 0.1578 0.8263 -0.1201 0.148 Uiso 1 1 calc R U . . .
C42 C 0.1327(5) 0.9392(4) -0.0803(4) 0.087(3) Uani 1 1 d . U . . .
H42A H 0.0852 0.9431 -0.0886 0.131 Uiso 1 1 calc R U . . .
H42B H 0.1373 0.9544 -0.0504 0.131 Uiso 1 1 calc R U . . .
H42C H 0.1629 0.9552 -0.1044 0.131 Uiso 1 1 calc R U . . .
C43 C 0.0928(8) 1.1104(6) -0.0946(5) 0.109(4) Uani 1 1 d . U . . .
C44 C 0.1444(6) 1.0861(4) -0.0623(4) 0.076(3) Uani 1 1 d . U . . .
C45 C 0.1169(5) 1.0666(5) -0.0213(4) 0.083(3) Uani 1 1 d . U . . .
H45 H 0.0700 1.0736 -0.0129 0.100 Uiso 1 1 calc R U . . .
C46 C 0.1533(5) 1.0372(5) 0.0089(3) 0.093(4) Uani 1 1 d . U . . .
C47 C 0.1135(9) 1.0164(9) 0.0523(6) 0.141(7) Uani 1 1 d . U . . .
C48 C 0.3769(8) 0.7841(5) 0.2159(4) 0.093(4) Uani 1 1 d . U . . .
C49 C 0.3905(5) 0.8029(4) 0.1662(4) 0.071(3) Uani 1 1 d . U . . .
C50 C 0.4026(5) 0.7664(4) 0.1337(4) 0.072(3) Uani 1 1 d . U . . .
H50 H 0.3991 0.7333 0.1447 0.086 Uiso 1 1 calc R U . . .
C51 C 0.4194(5) 0.7749(4) 0.0865(4) 0.068(2) Uani 1 1 d . U . . .
C52 C 0.4336(7) 0.7299(5) 0.0572(5) 0.094(4) Uani 1 1 d . U . . .
C53 C 0.6018(9) 0.8476(8) -0.2455(6) 0.122(5) Uani 1 1 d . U . . .
C54 C 0.5451(6) 0.8637(4) -0.2104(4) 0.076(3) Uani 1 1 d . U . . .
C55 C 0.4791(6) 0.8548(4) -0.2212(3) 0.075(3) Uani 1 1 d . U . . .
H55 H 0.4731 0.8391 -0.2495 0.090 Uiso 1 1 calc R U . . .
C56 C 0.4211(5) 0.8675(3) -0.1932(3) 0.058(2) Uani 1 1 d . U . . .
C57 C 0.3527(6) 0.8531(5) -0.2093(5) 0.084(3) Uani 1 1 d . U . . .
C58 C 0.1377(4) 0.5545(3) 0.1509(3) 0.0451(19) Uani 1 1 d . U . . .
C59 C 0.1746(5) 0.5892(3) 0.1421(3) 0.058(2) Uani 1 1 d . U . . .
C60 C 0.2231(6) 0.6312(4) 0.1363(4) 0.081(3) Uani 1 1 d . U . . .
C61 C 0.2070(10) 0.6642(6) 0.1748(7) 0.188(8) Uani 1 1 d . U . . .
H61A H 0.2112 0.6461 0.2045 0.281 Uiso 1 1 calc R U . . .
H61B H 0.2390 0.6913 0.1724 0.281 Uiso 1 1 calc R U . . .
H61C H 0.1602 0.6775 0.1733 0.281 Uiso 1 1 calc R U . . .
C62 C 0.2177(9) 0.6565(6) 0.0899(5) 0.167(8) Uani 1 1 d . U . . .
H62A H 0.2289 0.6330 0.0653 0.251 Uiso 1 1 calc R U . . .
H62B H 0.1710 0.6696 0.0874 0.251 Uiso 1 1 calc R U . . .
H62C H 0.2498 0.6834 0.0865 0.251 Uiso 1 1 calc R U . . .
C63 C 0.2944(7) 0.6114(6) 0.1407(6) 0.147(6) Uani 1 1 d . U . . .
H63A H 0.3068 0.5891 0.1153 0.220 Uiso 1 1 calc R U . . .
H63B H 0.3261 0.6386 0.1389 0.220 Uiso 1 1 calc R U . . .
H63C H 0.2970 0.5936 0.1707 0.220 Uiso 1 1 calc R U . . .
C64 C -0.0291(4) 0.5682(3) -0.2022(3) 0.047(2) Uani 1 1 d . U . . .
C65 C -0.0173(4) 0.5913(3) -0.2378(3) 0.0450(19) Uani 1 1 d . U . . .
C66 C -0.0062(6) 0.6184(4) -0.2828(3) 0.079(3) Uani 1 1 d . U . . .
C67 C 0.0470(7) 0.6563(6) -0.2808(5) 0.130(5) Uani 1 1 d . U . . .
H67A H 0.0342 0.6780 -0.2550 0.195 Uiso 1 1 calc R U . . .
H67B H 0.0913 0.6401 -0.2759 0.195 Uiso 1 1 calc R U . . .
H67C H 0.0502 0.6756 -0.3101 0.195 Uiso 1 1 calc R U . . .
C68 C 0.0074(10) 0.5836(6) -0.3203(4) 0.166(7) Uani 1 1 d . U . . .
H68A H 0.0147 0.6016 -0.3501 0.249 Uiso 1 1 calc R U . . .
H68B H 0.0483 0.5635 -0.3143 0.249 Uiso 1 1 calc R U . . .
H68C H -0.0319 0.5624 -0.3213 0.249 Uiso 1 1 calc R U . . .
C69 C -0.0753(7) 0.6456(7) -0.2904(5) 0.157(6) Uani 1 1 d . U . . .
H69A H -0.0854 0.6691 -0.2657 0.235 Uiso 1 1 calc R U . . .
H69B H -0.0724 0.6630 -0.3207 0.235 Uiso 1 1 calc R U . . .
H69C H -0.1118 0.6217 -0.2895 0.235 Uiso 1 1 calc R U . . .
C70 C 0.1988(4) 0.5581(3) -0.0200(3) 0.0422(19) Uani 1 1 d . U . . .
C71 C 0.2566(4) 0.5573(3) -0.0378(3) 0.0427(18) Uani 1 1 d . U . . .
C72 C 0.3299(4) 0.5568(3) -0.0543(3) 0.057(2) Uani 1 1 d . U . . .
C73 C 0.3395(5) 0.5869(4) -0.0998(3) 0.072(3) Uani 1 1 d . U . . .
H73A H 0.3880 0.5864 -0.1106 0.107 Uiso 1 1 calc R U . . .
H73B H 0.3130 0.5728 -0.1233 0.107 Uiso 1 1 calc R U . . .
H73C H 0.3235 0.6208 -0.0946 0.107 Uiso 1 1 calc R U . . .
C74 C 0.3692(5) 0.5790(5) -0.0170(4) 0.086(3) Uani 1 1 d . U . . .
H74A H 0.4180 0.5791 -0.0271 0.129 Uiso 1 1 calc R U . . .
H74B H 0.3524 0.6127 -0.0119 0.129 Uiso 1 1 calc R U . . .
H74C H 0.3626 0.5595 0.0121 0.129 Uiso 1 1 calc R U . . .
C75 C 0.3534(6) 0.5033(4) -0.0624(5) 0.107(4) Uani 1 1 d . U . . .
H75A H 0.4019 0.5022 -0.0734 0.161 Uiso 1 1 calc R U . . .
H75B H 0.3470 0.4841 -0.0332 0.161 Uiso 1 1 calc R U . . .
H75C H 0.3262 0.4896 -0.0859 0.161 Uiso 1 1 calc R U . . .
C76 C 0.1708(4) 0.5255(3) -0.1612(3) 0.049(2) Uani 1 1 d . U . . .
C77 C 0.2111(4) 0.5069(3) -0.1902(3) 0.0465(19) Uani 1 1 d . U . . .
C78 C 0.2623(5) 0.4896(4) -0.2259(3) 0.061(2) Uani 1 1 d . U . . .
C79 C 0.3145(5) 0.5305(5) -0.2357(4) 0.089(3) Uani 1 1 d . U . . .
H79A H 0.3496 0.5200 -0.2596 0.134 Uiso 1 1 calc R U . . .
H79B H 0.2909 0.5604 -0.2469 0.134 Uiso 1 1 calc R U . . .
H79C H 0.3362 0.5372 -0.2071 0.134 Uiso 1 1 calc R U . . .
C80 C 0.2265(6) 0.4809(5) -0.2699(4) 0.099(4) Uani 1 1 d . U . . .
H80A H 0.2601 0.4692 -0.2942 0.148 Uiso 1 1 calc R U . . .
H80B H 0.1916 0.4562 -0.2632 0.148 Uiso 1 1 calc R U . . .
H80C H 0.2047 0.5116 -0.2806 0.148 Uiso 1 1 calc R U . . .
C81 C 0.2982(7) 0.4436(5) -0.2089(5) 0.127(5) Uani 1 1 d . U . . .
H81A H 0.3323 0.4325 -0.2331 0.190 Uiso 1 1 calc R U . . .
H81B H 0.3210 0.4504 -0.1807 0.190 Uiso 1 1 calc R U . . .
H81C H 0.2647 0.4180 -0.2018 0.190 Uiso 1 1 calc R U . . .
C82 C -0.0295(4) 0.3680(3) -0.0447(3) 0.0439(19) Uani 1 1 d . U . . .
C83 C -0.0007(4) 0.3285(3) -0.0521(3) 0.0473(19) Uani 1 1 d . U . . .
C84 C 0.0243(5) 0.2782(3) -0.0599(3) 0.061(2) Uani 1 1 d . U . . .
C85 C 0.0143(7) 0.2661(4) -0.1107(4) 0.097(4) Uani 1 1 d . U . . .
H85A H 0.0308 0.2324 -0.1165 0.146 Uiso 1 1 calc R U . . .
H85B H -0.0344 0.2692 -0.1162 0.146 Uiso 1 1 calc R U . . .
H85C H 0.0400 0.2889 -0.1317 0.146 Uiso 1 1 calc R U . . .
C86 C 0.1007(6) 0.2735(4) -0.0524(5) 0.101(4) Uani 1 1 d . U . . .
H86A H 0.1170 0.2397 -0.0577 0.152 Uiso 1 1 calc R U . . .
H86B H 0.1259 0.2959 -0.0743 0.152 Uiso 1 1 calc R U . . .
H86C H 0.1083 0.2820 -0.0205 0.152 Uiso 1 1 calc R U . . .
C87 C -0.0169(8) 0.2439(4) -0.0276(5) 0.124(5) Uani 1 1 d . U . . .
H87A H -0.0006 0.2101 -0.0326 0.186 Uiso 1 1 calc R U . . .
H87B H -0.0117 0.2522 0.0047 0.186 Uiso 1 1 calc R U . . .
H87C H -0.0653 0.2472 -0.0341 0.186 Uiso 1 1 calc R U . . .
C88 C 0.0796(4) 0.3284(3) 0.0972(3) 0.0414(18) Uani 1 1 d . U . . .
C89 C 0.0573(4) 0.2917(3) 0.1176(3) 0.0413(17) Uani 1 1 d . U . . .
C90 C 0.0420(5) 0.2445(3) 0.1424(3) 0.056(2) Uani 1 1 d . U . . .
C91 C 0.0939(6) 0.2360(4) 0.1785(4) 0.092(3) Uani 1 1 d . U . . .
H91A H 0.0851 0.2049 0.1955 0.138 Uiso 1 1 calc R U . . .
H91B H 0.1401 0.2347 0.1629 0.138 Uiso 1 1 calc R U . . .
H91C H 0.0903 0.2629 0.2003 0.138 Uiso 1 1 calc R U . . .
C92 C -0.0309(6) 0.2461(4) 0.1649(5) 0.107(4) Uani 1 1 d . U . . .
H92A H -0.0405 0.2148 0.1812 0.161 Uiso 1 1 calc R U . . .
H92B H -0.0358 0.2726 0.1871 0.161 Uiso 1 1 calc R U . . .
H92C H -0.0632 0.2521 0.1407 0.161 Uiso 1 1 calc R U . . .
C93 C 0.0481(6) 0.2040(4) 0.1069(4) 0.080(3) Uani 1 1 d . U . . .
H93A H 0.0382 0.1724 0.1226 0.120 Uiso 1 1 calc R U . . .
H93B H 0.0155 0.2109 0.0831 0.120 Uiso 1 1 calc R U . . .
H93C H 0.0947 0.2028 0.0921 0.120 Uiso 1 1 calc R U . . .
C94 C 0.1751(4) 0.4051(3) -0.0212(3) 0.048(2) Uani 1 1 d . U . . .
C95 C 0.2267(4) 0.3798(3) -0.0211(3) 0.0471(19) Uani 1 1 d . U . . .
C96 C 0.2913(4) 0.3501(3) -0.0254(3) 0.057(2) Uani 1 1 d . U . . .
C97 C 0.3424(5) 0.3710(5) 0.0056(4) 0.093(4) Uani 1 1 d . U . . .
H97A H 0.3853 0.3515 0.0029 0.139 Uiso 1 1 calc R U . . .
H97B H 0.3512 0.4051 -0.0042 0.139 Uiso 1 1 calc R U . . .
H97C H 0.3235 0.3697 0.0380 0.139 Uiso 1 1 calc R U . . .
C98 C 0.2779(6) 0.2974(4) -0.0096(6) 0.117(5) Uani 1 1 d . U . . .
H98A H 0.3208 0.2779 -0.0125 0.175 Uiso 1 1 calc R U . . .
H98B H 0.2597 0.2965 0.0230 0.175 Uiso 1 1 calc R U . . .
H98C H 0.2447 0.2837 -0.0290 0.175 Uiso 1 1 calc R U . . .
C99 C 0.3199(6) 0.3542(5) -0.0752(4) 0.094(4) Uani 1 1 d . U . . .
H99A H 0.3627 0.3348 -0.0789 0.141 Uiso 1 1 calc R U . . .
H99B H 0.2869 0.3418 -0.0956 0.141 Uiso 1 1 calc R U . . .
H99C H 0.3287 0.3886 -0.0836 0.141 Uiso 1 1 calc R U . . .
C100 C 0.4146(5) 0.4753(4) 0.0907(3) 0.062(2) Uani 1 1 d . U . . .
C101 C 0.3396(4) 0.4609(3) 0.0973(3) 0.050(2) Uani 1 1 d . U . . .
C102 C 0.3264(4) 0.4198(3) 0.1256(3) 0.0470(19) Uani 1 1 d . U . . .
H102 H 0.3636 0.4042 0.1403 0.056 Uiso 1 1 calc R U . . .
C103 C 0.2621(4) 0.3997(3) 0.1340(3) 0.0430(18) Uani 1 1 d . U . . .
C104 C 0.2576(4) 0.3518(4) 0.1618(3) 0.057(2) Uani 1 1 d . U . . .
C105 C 0.0036(7) 0.4019(5) -0.2614(4) 0.089(3) Uani 1 1 d . U . . .
C106 C 0.0473(5) 0.3956(4) -0.2200(3) 0.062(2) Uani 1 1 d . U . . .
C107 C 0.0996(5) 0.3603(3) -0.2224(3) 0.065(2) Uani 1 1 d . U . . .
H107 H 0.1056 0.3415 -0.2496 0.078 Uiso 1 1 calc R U . . .
C108 C 0.1435(5) 0.3506(3) -0.1873(3) 0.061(2) Uani 1 1 d . U . . .
C109 C 0.1944(8) 0.3080(5) -0.1956(5) 0.088(3) Uani 1 1 d . U . . .
C110 C -0.2249(5) 0.2814(4) 0.0362(4) 0.063(2) Uani 1 1 d . U . . .
C111 C -0.1806(4) 0.3049(3) 0.0699(3) 0.0461(19) Uani 1 1 d . U . . .
C112 C -0.2049(4) 0.3064(3) 0.1155(3) 0.0470(19) Uani 1 1 d . U . . .
H112 H -0.2457 0.2897 0.1245 0.056 Uiso 1 1 calc R U . . .
C113 C -0.1739(4) 0.3307(3) 0.1494(3) 0.050(2) Uani 1 1 d . U . . .
C114 C -0.2091(5) 0.3273(5) 0.1985(4) 0.073(3) Uani 1 1 d . U . . .
C115 C 0.3427(4) 0.5352(3) 0.6067(3) 0.0369(17) Uani 1 1 d . U . . .
C116 C 0.3067(4) 0.5716(3) 0.6087(2) 0.0380(16) Uani 1 1 d . U . . .
C117 C 0.2572(4) 0.6137(3) 0.6164(3) 0.0492(19) Uani 1 1 d . U . . .
C118 C 0.2505(6) 0.6226(4) 0.6674(3) 0.074(3) Uani 1 1 d . U . . .
H11F H 0.2181 0.6502 0.6735 0.111 Uiso 1 1 calc R U . . .
H11G H 0.2336 0.5932 0.6843 0.111 Uiso 1 1 calc R U . . .
H11H H 0.2952 0.6304 0.6779 0.111 Uiso 1 1 calc R U . . .
C119 C 0.2834(6) 0.6607(4) 0.5915(3) 0.077(3) Uani 1 1 d . U . . .
H11I H 0.2498 0.6876 0.5971 0.115 Uiso 1 1 calc R U . . .
H11J H 0.3270 0.6690 0.6034 0.115 Uiso 1 1 calc R U . . .
H11K H 0.2900 0.6555 0.5579 0.115 Uiso 1 1 calc R U . . .
C120 C 0.1908(5) 0.6017(5) 0.5976(5) 0.105(4) Uani 1 1 d . U . . .
H12D H 0.1579 0.6292 0.6025 0.158 Uiso 1 1 calc R U . . .
H12E H 0.1981 0.5959 0.5642 0.158 Uiso 1 1 calc R U . . .
H12F H 0.1728 0.5722 0.6137 0.158 Uiso 1 1 calc R U . . .
C121 C 0.3616(4) 0.3873(3) 0.5546(3) 0.0387(17) Uani 1 1 d . U . . .
C122 C 0.3325(4) 0.3721(3) 0.5897(3) 0.0410(18) Uani 1 1 d . U . . .
C123 C 0.2969(4) 0.3492(3) 0.6317(3) 0.052(2) Uani 1 1 d . U . . .
C124 C 0.3353(5) 0.3604(4) 0.6748(3) 0.068(3) Uani 1 1 d . U . . .
H12G H 0.3119 0.3454 0.7026 0.102 Uiso 1 1 calc R U . . .
H12H H 0.3823 0.3471 0.6709 0.102 Uiso 1 1 calc R U . . .
H12I H 0.3362 0.3960 0.6782 0.102 Uiso 1 1 calc R U . . .
C125 C 0.2237(5) 0.3709(5) 0.6370(4) 0.090(3) Uani 1 1 d . U . . .
H12J H 0.1994 0.3561 0.6646 0.135 Uiso 1 1 calc R U . . .
H12K H 0.2252 0.4064 0.6404 0.135 Uiso 1 1 calc R U . . .
H12L H 0.1997 0.3640 0.6093 0.135 Uiso 1 1 calc R U . . .
C126 C 0.2971(7) 0.2945(4) 0.6252(4) 0.098(4) Uani 1 1 d . U . . .
H12M H 0.2738 0.2785 0.6526 0.147 Uiso 1 1 calc R U . . .
H12N H 0.2733 0.2877 0.5975 0.147 Uiso 1 1 calc R U . . .
H12O H 0.3444 0.2818 0.6214 0.147 Uiso 1 1 calc R U . . .
C127 C 0.2593(4) 0.5963(3) 0.4547(3) 0.0388(17) Uani 1 1 d . U . . .
C128 C 0.1986(4) 0.5917(3) 0.4506(3) 0.0433(18) Uani 1 1 d . U . . .
C129 C 0.1250(4) 0.5916(3) 0.4432(3) 0.064(2) Uani 1 1 d D U . . .
C130 C 0.0936(13) 0.6414(7) 0.4392(13) 0.142(11) Uani 0.508(19) 1 d D U P G 1
H13A H 0.0449 0.6390 0.4344 0.212 Uiso 0.508(19) 1 calc R U P G 1
H13B H 0.0987 0.6587 0.4680 0.212 Uiso 0.508(19) 1 calc R U P G 1
H13C H 0.1163 0.6594 0.4128 0.212 Uiso 0.508(19) 1 calc R U P G 1
C131 C 0.0875(10) 0.5617(9) 0.4835(7) 0.079(7) Uani 0.508(19) 1 d D U P G 1
H13D H 0.0385 0.5615 0.4786 0.118 Uiso 0.508(19) 1 calc R U P G 1
H13E H 0.1060 0.5280 0.4840 0.118 Uiso 0.508(19) 1 calc R U P G 1
H13F H 0.0941 0.5767 0.5131 0.118 Uiso 0.508(19) 1 calc R U P G 1
C132 C 0.1172(11) 0.5629(12) 0.3988(7) 0.113(9) Uani 0.508(19) 1 d D U P G 1
H13G H 0.0687 0.5620 0.3928 0.170 Uiso 0.508(19) 1 calc R U P G 1
H13H H 0.1426 0.5790 0.3723 0.170 Uiso 0.508(19) 1 calc R U P G 1
H13I H 0.1354 0.5293 0.4031 0.170 Uiso 0.508(19) 1 calc R U P G 1
C30A C 0.1104(11) 0.6147(12) 0.3950(7) 0.102(9) Uani 0.492(19) 1 d D U P G 2
H30D H 0.0612 0.6142 0.3909 0.154 Uiso 0.492(19) 1 calc R U P G 2
H30E H 0.1253 0.6487 0.3930 0.154 Uiso 0.492(19) 1 calc R U P G 2
H30F H 0.1354 0.5960 0.3705 0.154 Uiso 0.492(19) 1 calc R U P G 2
C31A C 0.0971(14) 0.5414(7) 0.4484(13) 0.144(12) Uani 0.492(19) 1 d D U P G 2
H31A H 0.0482 0.5431 0.4431 0.215 Uiso 0.492(19) 1 calc R U P G 2
H31B H 0.1212 0.5202 0.4255 0.215 Uiso 0.492(19) 1 calc R U P G 2
H31C H 0.1034 0.5281 0.4798 0.215 Uiso 0.492(19) 1 calc R U P G 2
C32A C 0.0892(12) 0.6254(11) 0.4795(9) 0.112(9) Uani 0.492(19) 1 d D U P G 2
H32A H 0.0399 0.6266 0.4760 0.168 Uiso 0.492(19) 1 calc R U P G 2
H32B H 0.0980 0.6128 0.5109 0.168 Uiso 0.492(19) 1 calc R U P G 2
H32C H 0.1070 0.6585 0.4749 0.168 Uiso 0.492(19) 1 calc R U P G 2
C133 C 0.5271(4) 0.5470(3) 0.3067(2) 0.0344(16) Uani 1 1 d . U . . .
C134 C 0.5086(4) 0.5747(3) 0.2756(3) 0.0367(16) Uani 1 1 d . U . . .
C135 C 0.4894(4) 0.6061(3) 0.2351(3) 0.0443(18) Uani 1 1 d . U . . .
C136 C 0.5369(6) 0.6497(3) 0.2292(3) 0.070(3) Uani 1 1 d . U . . .
H13J H 0.5244 0.6704 0.2025 0.104 Uiso 1 1 calc R U . . .
H13K H 0.5324 0.6688 0.2574 0.104 Uiso 1 1 calc R U . . .
H13L H 0.5843 0.6376 0.2238 0.104 Uiso 1 1 calc R U . . .
C137 C 0.4966(6) 0.5757(3) 0.1913(3) 0.076(3) Uani 1 1 d . U . . .
H13M H 0.4840 0.5961 0.1644 0.114 Uiso 1 1 calc R U . . .
H13N H 0.5441 0.5637 0.1861 0.114 Uiso 1 1 calc R U . . .
H13O H 0.4664 0.5477 0.1953 0.114 Uiso 1 1 calc R U . . .
C138 C 0.4162(5) 0.6260(4) 0.2437(4) 0.075(3) Uani 1 1 d . U . . .
H13P H 0.4038 0.6466 0.2170 0.112 Uiso 1 1 calc R U . . .
H13Q H 0.3850 0.5986 0.2481 0.112 Uiso 1 1 calc R U . . .
H13R H 0.4128 0.6455 0.2718 0.112 Uiso 1 1 calc R U . . .
C139 C 0.3214(4) 0.5057(3) 0.3397(3) 0.0363(17) Uani 1 1 d . U . . .
C140 C 0.2841(4) 0.5033(3) 0.3096(3) 0.0447(19) Uani 1 1 d . U . . .
C141 C 0.2375(6) 0.5026(5) 0.2713(4) 0.085(3) Uani 1 1 d . U . . .
C142 C 0.2780(7) 0.4950(6) 0.2266(4) 0.133(6) Uani 1 1 d . U . . .
H14A H 0.3123 0.5204 0.2218 0.200 Uiso 1 1 calc R U . . .
H14B H 0.3010 0.4626 0.2275 0.200 Uiso 1 1 calc R U . . .
H14C H 0.2475 0.4970 0.2011 0.200 Uiso 1 1 calc R U . . .
C143 C 0.1869(12) 0.4686(10) 0.2820(7) 0.295(13) Uani 1 1 d . U . . .
H14D H 0.1626 0.4762 0.3120 0.442 Uiso 1 1 calc R U . . .
H14E H 0.1544 0.4700 0.2576 0.442 Uiso 1 1 calc R U . . .
H14F H 0.2079 0.4356 0.2841 0.442 Uiso 1 1 calc R U . . .
C144 C 0.2027(8) 0.5531(7) 0.2681(5) 0.168(7) Uani 1 1 d . U . . .
H14G H 0.2372 0.5779 0.2606 0.252 Uiso 1 1 calc R U . . .
H14H H 0.1703 0.5537 0.2437 0.252 Uiso 1 1 calc R U . . .
H14I H 0.1780 0.5603 0.2980 0.252 Uiso 1 1 calc R U . . .
C145 C 0.3477(4) 0.3678(3) 0.4117(3) 0.0354(17) Uani 1 1 d . U . . .
C146 C 0.3413(4) 0.3439(3) 0.3778(3) 0.0421(18) Uani 1 1 d . U . . .
C147 C 0.3271(5) 0.3112(4) 0.3398(3) 0.067(2) Uani 1 1 d . U . . .
C148 C 0.3608(8) 0.3292(6) 0.2946(4) 0.134(6) Uani 1 1 d . U . . .
H14J H 0.3509 0.3073 0.2699 0.201 Uiso 1 1 calc R U . . .
H14K H 0.3432 0.3624 0.2872 0.201 Uiso 1 1 calc R U . . .
H14L H 0.4103 0.3299 0.2971 0.201 Uiso 1 1 calc R U . . .
C149 C 0.2506(5) 0.3059(5) 0.3383(4) 0.090(4) Uani 1 1 d . U . . .
H14M H 0.2415 0.2843 0.3131 0.136 Uiso 1 1 calc R U . . .
H14N H 0.2319 0.2918 0.3681 0.136 Uiso 1 1 calc R U . . .
H14O H 0.2290 0.3383 0.3327 0.136 Uiso 1 1 calc R U . . .
C150 C 0.3594(7) 0.2597(4) 0.3519(5) 0.107(4) Uani 1 1 d . U . . .
H15A H 0.3511 0.2369 0.3275 0.161 Uiso 1 1 calc R U . . .
H15B H 0.4088 0.2625 0.3540 0.161 Uiso 1 1 calc R U . . .
H15C H 0.3386 0.2474 0.3818 0.161 Uiso 1 1 calc R U . . .
C151 C 0.5625(4) 0.3572(3) 0.4894(3) 0.0392(18) Uani 1 1 d . U . . .
C152 C 0.5382(4) 0.3173(3) 0.4889(3) 0.0368(16) Uani 1 1 d . U . . .
C153 C 0.5157(4) 0.2665(3) 0.4865(3) 0.052(2) Uani 1 1 d D U . . .
C154 C 0.5231(13) 0.2493(8) 0.4381(6) 0.080(4) Uani 0.433(12) 1 d D U P H 1
H15D H 0.5077 0.2155 0.4376 0.119 Uiso 0.433(12) 1 calc R U P H 1
H15E H 0.4952 0.2705 0.4183 0.119 Uiso 0.433(12) 1 calc R U P H 1
H15F H 0.5712 0.2505 0.4264 0.119 Uiso 0.433(12) 1 calc R U P H 1
C155 C 0.4404(9) 0.2630(8) 0.5074(9) 0.088(7) Uani 0.433(12) 1 d D U P H 1
H15G H 0.4255 0.2292 0.5058 0.132 Uiso 0.433(12) 1 calc R U P H 1
H15H H 0.4377 0.2726 0.5400 0.132 Uiso 0.433(12) 1 calc R U P H 1
H15I H 0.4108 0.2850 0.4897 0.132 Uiso 0.433(12) 1 calc R U P H 1
C156 C 0.5616(12) 0.2362(9) 0.5192(8) 0.086(7) Uani 0.433(12) 1 d D U P H 1
H15J H 0.5496 0.2016 0.5194 0.129 Uiso 0.433(12) 1 calc R U P H 1
H15K H 0.6097 0.2394 0.5081 0.129 Uiso 0.433(12) 1 calc R U P H 1
H15L H 0.5546 0.2484 0.5509 0.129 Uiso 0.433(12) 1 calc R U P H 1
C54A C 0.4631(9) 0.2651(6) 0.4489(6) 0.080(4) Uani 0.567(12) 1 d D U P H 2
H54A H 0.4475 0.2316 0.4467 0.119 Uiso 0.567(12) 1 calc R U P H 2
H54B H 0.4238 0.2869 0.4574 0.119 Uiso 0.567(12) 1 calc R U P H 2
H54C H 0.4846 0.2761 0.4187 0.119 Uiso 0.567(12) 1 calc R U P H 2
C55A C 0.4872(12) 0.2458(8) 0.5319(5) 0.109(8) Uani 0.567(12) 1 d D U P H 2
H55C H 0.4732 0.2121 0.5280 0.163 Uiso 0.567(12) 1 calc R U P H 2
H55D H 0.5221 0.2458 0.5546 0.163 Uiso 0.567(12) 1 calc R U P H 2
H55E H 0.4474 0.2658 0.5431 0.163 Uiso 0.567(12) 1 calc R U P H 2
C56A C 0.5783(10) 0.2344(6) 0.4675(8) 0.097(6) Uani 0.567(12) 1 d D U P H 2
H56A H 0.5646 0.2004 0.4655 0.145 Uiso 0.567(12) 1 calc R U P H 2
H56B H 0.5944 0.2470 0.4364 0.145 Uiso 0.567(12) 1 calc R U P H 2
H56C H 0.6153 0.2358 0.4885 0.145 Uiso 0.567(12) 1 calc R U P H 2
C157 C 0.4945(4) 0.4202(3) 0.2296(3) 0.052(2) Uani 1 1 d D U . . .
C158 C 0.5137(4) 0.3986(3) 0.2766(3) 0.0396(17) Uani 1 1 d . U . . .
C159 C 0.5500(4) 0.3545(3) 0.2763(3) 0.050(2) Uani 1 1 d . U . . .
H159 H 0.5667 0.3424 0.2470 0.059 Uiso 1 1 calc R U . . .
C160 C 0.5637(4) 0.3268(3) 0.3159(3) 0.050(2) Uani 1 1 d . U . . .
C161 C 0.5972(6) 0.2765(4) 0.3080(4) 0.069(3) Uani 1 1 d . U . . .
C162 C 0.5086(7) 0.7672(4) 0.3356(4) 0.074(3) Uani 1 1 d . U . . .
C163 C 0.4680(5) 0.7214(3) 0.3506(3) 0.056(2) Uani 1 1 d . U . . .
C164 C 0.3985(5) 0.7234(3) 0.3458(3) 0.057(2) Uani 1 1 d . U . . .
H164 H 0.3788 0.7538 0.3354 0.068 Uiso 1 1 calc R U . . .
C165 C 0.3552(5) 0.6846(3) 0.3548(3) 0.052(2) Uani 1 1 d . U . . .
C166 C 0.2814(6) 0.6924(4) 0.3455(4) 0.075(3) Uani 1 1 d . U . . .
C167 C 0.1042(5) 0.4647(4) 0.5980(3) 0.066(3) Uani 1 1 d . U . . .
C168 C 0.1550(4) 0.4603(3) 0.5554(3) 0.052(2) Uani 1 1 d . U . . .
C169 C 0.1357(4) 0.4312(3) 0.5201(3) 0.050(2) Uani 1 1 d . U . . .
H169 H 0.0964 0.4119 0.5261 0.060 Uiso 1 1 calc R U . . .
C170 C 0.1709(4) 0.4290(3) 0.4768(3) 0.049(2) Uani 1 1 d . U . . .
C171 C 0.1386(5) 0.4018(4) 0.4393(4) 0.076(3) Uani 1 1 d D U . . .
C172 C 0.0151(5) 0.1578(3) 0.6183(3) 0.054(2) Uani 1 1 d . U . . .
C173 C 0.0280(4) 0.1987(3) 0.6247(3) 0.058(2) Uani 1 1 d . U . . .
C174 C 0.0394(6) 0.2497(4) 0.6384(5) 0.089(3) Uani 1 1 d . U . . .
C175 C -0.0302(8) 0.2695(5) 0.6598(6) 0.145(6) Uani 1 1 d . U . . .
H17D H -0.0643 0.2690 0.6366 0.218 Uiso 1 1 calc R U . . .
H17E H -0.0450 0.2488 0.6869 0.218 Uiso 1 1 calc R U . . .
H17F H -0.0254 0.3032 0.6695 0.218 Uiso 1 1 calc R U . . .
C176 C 0.0931(9) 0.2493(5) 0.6713(6) 0.164(7) Uani 1 1 d . U . . .
H17G H 0.1005 0.2829 0.6803 0.246 Uiso 1 1 calc R U . . .
H17H H 0.0790 0.2293 0.6991 0.246 Uiso 1 1 calc R U . . .
H17I H 0.1356 0.2354 0.6566 0.246 Uiso 1 1 calc R U . . .
C177 C 0.0586(8) 0.2817(4) 0.5943(5) 0.118(4) Uani 1 1 d . U . . .
H17J H 0.0218 0.2812 0.5731 0.177 Uiso 1 1 calc R U . . .
H17K H 0.0651 0.3154 0.6032 0.177 Uiso 1 1 calc R U . . .
H17L H 0.1011 0.2686 0.5787 0.177 Uiso 1 1 calc R U . . .
C178 C -0.1077(4) 0.1301(3) 0.4701(3) 0.0458(19) Uani 1 1 d . U . . .
C179 C -0.1420(4) 0.1602(3) 0.4925(3) 0.0422(17) Uani 1 1 d . U . . .
C180 C -0.1805(4) 0.2018(3) 0.5150(3) 0.055(2) Uani 1 1 d . U . . .
C181 C -0.2454(5) 0.1824(4) 0.5405(4) 0.087(3) Uani 1 1 d . U . . .
H18D H -0.2713 0.2095 0.5555 0.130 Uiso 1 1 calc R U . . .
H18E H -0.2735 0.1676 0.5182 0.130 Uiso 1 1 calc R U . . .
H18F H -0.2332 0.1577 0.5642 0.130 Uiso 1 1 calc R U . . .
C182 C -0.1358(5) 0.2224(4) 0.5498(4) 0.084(3) Uani 1 1 d . U . . .
H18G H -0.1601 0.2500 0.5652 0.126 Uiso 1 1 calc R U . . .
H18H H -0.1251 0.1969 0.5731 0.126 Uiso 1 1 calc R U . . .
H18I H -0.0932 0.2338 0.5336 0.126 Uiso 1 1 calc R U . . .
C183 C -0.1970(7) 0.2397(5) 0.4787(5) 0.109(4) Uani 1 1 d . U . . .
H18J H -0.2225 0.2672 0.4934 0.164 Uiso 1 1 calc R U . . .
H18K H -0.1545 0.2515 0.4628 0.164 Uiso 1 1 calc R U . . .
H18L H -0.2250 0.2254 0.4560 0.164 Uiso 1 1 calc R U . . .
C184 C 0.0776(4) 0.0975(3) 0.3941(3) 0.047(2) Uani 1 1 d . U . . .
C185 C 0.1204(4) 0.1125(4) 0.3662(3) 0.063(3) Uani 1 1 d . U . . .
C186 C 0.1700(6) 0.1303(6) 0.3288(4) 0.098(3) Uani 1 1 d . U . . .
C187 C 0.2270(5) 0.1568(4) 0.3471(4) 0.073(3) Uani 1 1 d . U . . .
H18M H 0.2466 0.1369 0.3721 0.110 Uiso 1 1 calc R U . . .
H18N H 0.2624 0.1627 0.3220 0.110 Uiso 1 1 calc R U . . .
H18O H 0.2096 0.1882 0.3593 0.110 Uiso 1 1 calc R U . . .
C188 C 0.2088(8) 0.0775(7) 0.3067(6) 0.158(6) Uani 1 1 d . U . . .
C189 C 0.1372(7) 0.1535(8) 0.2935(5) 0.190(8) Uani 1 1 d . U . . .
H18S H 0.1711 0.1650 0.2692 0.285 Uiso 1 1 calc R U . . .
H18T H 0.1069 0.1306 0.2803 0.285 Uiso 1 1 calc R U . . .
H18U H 0.1101 0.1816 0.3057 0.285 Uiso 1 1 calc R U . . .
C190 C 0.2581(4) 0.0785(3) 0.4696(3) 0.053(2) Uani 1 1 d . U . . .
C191 C 0.3168(4) 0.0750(3) 0.4538(3) 0.0441(18) Uani 1 1 d . U . . .
C192 C 0.3884(4) 0.0747(3) 0.4333(3) 0.057(2) Uani 1 1 d . U . . .
C193 C 0.4109(5) 0.1282(4) 0.4281(5) 0.094(4) Uani 1 1 d . U . . .
H19A H 0.4582 0.1290 0.4147 0.141 Uiso 1 1 calc R U . . .
H19B H 0.3809 0.1466 0.4076 0.141 Uiso 1 1 calc R U . . .
H19C H 0.4079 0.1429 0.4588 0.141 Uiso 1 1 calc R U . . .
C194 C 0.3917(5) 0.0518(4) 0.3859(4) 0.078(3) Uani 1 1 d . U . . .
H19D H 0.4390 0.0516 0.3723 0.117 Uiso 1 1 calc R U . . .
H19E H 0.3758 0.0181 0.3893 0.117 Uiso 1 1 calc R U . . .
H19F H 0.3624 0.0710 0.3654 0.117 Uiso 1 1 calc R U . . .
C195 C 0.4341(4) 0.0453(4) 0.4647(4) 0.072(3) Uani 1 1 d . U . . .
H19G H 0.4813 0.0453 0.4509 0.108 Uiso 1 1 calc R U . . .
H19H H 0.4321 0.0600 0.4953 0.108 Uiso 1 1 calc R U . . .
H19I H 0.4186 0.0115 0.4681 0.108 Uiso 1 1 calc R U . . .
C196 C 0.1506(4) -0.0600(4) 0.6548(3) 0.052(2) Uani 1 1 d . U . . .
C197 C 0.1432(4) -0.1018(4) 0.6698(3) 0.053(2) Uani 1 1 d . U . . .
C198 C 0.1373(5) -0.1518(4) 0.6924(3) 0.065(2) Uani 1 1 d . U . . .
C199 C 0.0631(6) -0.1670(5) 0.6925(5) 0.107(4) Uani 1 1 d . U . . .
H19J H 0.0335 -0.1432 0.7096 0.160 Uiso 1 1 calc R U . . .
H19K H 0.0499 -0.1680 0.6604 0.160 Uiso 1 1 calc R U . . .
H19L H 0.0582 -0.1995 0.7077 0.160 Uiso 1 1 calc R U . . .
C200 C 0.1551(8) -0.1489(5) 0.7428(4) 0.133(6) Uani 1 1 d . U . . .
H20A H 0.1244 -0.1248 0.7587 0.200 Uiso 1 1 calc R U . . .
H20B H 0.1498 -0.1811 0.7585 0.200 Uiso 1 1 calc R U . . .
H20C H 0.2025 -0.1389 0.7436 0.200 Uiso 1 1 calc R U . . .
C201 C 0.1825(9) -0.1881(5) 0.6664(6) 0.153(7) Uani 1 1 d . U . . .
H20D H 0.1780 -0.2205 0.6816 0.230 Uiso 1 1 calc R U . . .
H20E H 0.1691 -0.1893 0.6343 0.230 Uiso 1 1 calc R U . . .
H20F H 0.2301 -0.1781 0.6661 0.230 Uiso 1 1 calc R U . . .
C202 C 0.1390(4) -0.0541(3) 0.3987(3) 0.053(2) Uani 1 1 d D U . . .
C203 C 0.1690(6) -0.0735(5) 0.3631(4) 0.047(3) Uani 0.723(10) 1 d D U P C 1
C204 C 0.2110(7) -0.0959(5) 0.3220(5) 0.065(4) Uani 0.723(10) 1 d D U P C 1
C205 C 0.2004(8) -0.0654(5) 0.2780(4) 0.084(4) Uani 0.723(10) 1 d D U P C 1
H20G H 0.2275 -0.0799 0.2517 0.126 Uiso 0.723(10) 1 calc R U P C 1
H20H H 0.1519 -0.0647 0.2718 0.126 Uiso 0.723(10) 1 calc R U P C 1
H20I H 0.2151 -0.0319 0.2819 0.126 Uiso 0.723(10) 1 calc R U P C 1
C206 C 0.1906(8) -0.1486(5) 0.3147(5) 0.094(5) Uani 0.723(10) 1 d D U P C 1
H20J H 0.1973 -0.1686 0.3430 0.141 Uiso 0.723(10) 1 calc R U P C 1
H20K H 0.1424 -0.1488 0.3078 0.141 Uiso 0.723(10) 1 calc R U P C 1
H20L H 0.2191 -0.1622 0.2886 0.141 Uiso 0.723(10) 1 calc R U P C 1
C207 C 0.2867(6) -0.0965(7) 0.3322(5) 0.106(6) Uani 0.723(10) 1 d D U P C 1
H20M H 0.2933 -0.1162 0.3607 0.159 Uiso 0.723(10) 1 calc R U P C 1
H20N H 0.3144 -0.1108 0.3061 0.159 Uiso 0.723(10) 1 calc R U P C 1
H20O H 0.3009 -0.0629 0.3363 0.159 Uiso 0.723(10) 1 calc R U P C 1
C23A C 0.1614(13) -0.0416(11) 0.3649(7) 0.037(6) Uani 0.277(10) 1 d D U P C 2
C24A C 0.2064(11) -0.0413(8) 0.3209(7) 0.053(6) Uani 0.277(10) 1 d D U P C 2
C25A C 0.2584(13) -0.0025(10) 0.3305(11) 0.064(9) Uani 0.277(10) 1 d D U P C 2
H25A H 0.2914 0.0010 0.3035 0.096 Uiso 0.277(10) 1 calc R U P C 2
H25B H 0.2344 0.0289 0.3361 0.096 Uiso 0.277(10) 1 calc R U P C 2
H25C H 0.2826 -0.0129 0.3579 0.096 Uiso 0.277(10) 1 calc R U P C 2
C26A C 0.1591(17) -0.0253(13) 0.2826(11) 0.079(10) Uani 0.277(10) 1 d D U P C 2
H26A H 0.1854 -0.0243 0.2524 0.119 Uiso 0.277(10) 1 calc R U P C 2
H26B H 0.1224 -0.0488 0.2819 0.119 Uiso 0.277(10) 1 calc R U P C 2
H26C H 0.1391 0.0073 0.2891 0.119 Uiso 0.277(10) 1 calc R U P C 2
C27A C 0.2362(18) -0.0932(10) 0.3171(13) 0.057(9) Uani 0.277(10) 1 d D U P C 2
H27A H 0.2665 -0.0954 0.2887 0.085 Uiso 0.277(10) 1 calc R U P C 2
H27B H 0.2622 -0.1014 0.3443 0.085 Uiso 0.277(10) 1 calc R U P C 2
H27C H 0.1990 -0.1161 0.3160 0.085 Uiso 0.277(10) 1 calc R U P C 2
C208 C 0.2075(4) 0.0841(3) 0.6185(3) 0.055(2) Uani 1 1 d . U . . .
C209 C 0.2654(4) 0.0942(3) 0.6167(3) 0.051(2) Uani 1 1 d . U . . .
C210 C 0.3383(6) 0.1060(5) 0.6194(4) 0.103(4) Uani 1 1 d . U . . .
C211 C 0.3601(6) 0.1421(5) 0.5801(4) 0.097(4) Uani 1 1 d . U . . .
H21A H 0.3530 0.1278 0.5501 0.146 Uiso 1 1 calc R U . . .
H21B H 0.3326 0.1726 0.5833 0.146 Uiso 1 1 calc R U . . .
H21C H 0.4086 0.1491 0.5816 0.146 Uiso 1 1 calc R U . . .
C212 C 0.3480(9) 0.1259(8) 0.6655(5) 0.199(8) Uani 1 1 d . U . . .
H21D H 0.3962 0.1338 0.6673 0.299 Uiso 1 1 calc R U . . .
H21E H 0.3194 0.1558 0.6697 0.299 Uiso 1 1 calc R U . . .
H21F H 0.3349 0.1015 0.6899 0.299 Uiso 1 1 calc R U . . .
C213 C 0.3805(7) 0.0569(7) 0.6123(7) 0.193(7) Uani 1 1 d . U . . .
H21G H 0.3732 0.0445 0.5816 0.289 Uiso 1 1 calc R U . . .
H21H H 0.4292 0.0628 0.6144 0.289 Uiso 1 1 calc R U . . .
H21I H 0.3654 0.0327 0.6365 0.289 Uiso 1 1 calc R U . . .
C214 C 0.0229(7) 0.1084(4) 0.7481(4) 0.082(3) Uani 1 1 d D U . . .
C215 C 0.0089(5) 0.0569(4) 0.7337(3) 0.068(2) Uani 1 1 d D U . . .
C216 C -0.0101(5) 0.0218(4) 0.7691(3) 0.073(3) Uani 1 1 d D U . . .
H216 H -0.0129 0.0315 0.8005 0.087 Uiso 1 1 calc R U . . .
C217 C -0.0255(6) -0.0279(4) 0.7598(3) 0.086(3) Uani 1 1 d D U . . .
C218 C -0.0441(11) -0.0600(7) 0.8034(4) 0.123(5) Uani 1 1 d D U . . .
C219 C 0.4131(6) -0.1032(5) 0.4266(6) 0.098(4) Uani 1 1 d . U . . .
C220 C 0.3595(5) -0.0836(4) 0.4642(5) 0.076(3) Uani 1 1 d . U . . .
C221 C 0.3716(5) -0.0919(3) 0.5101(5) 0.076(3) Uani 1 1 d . U . . .
H221 H 0.4142 -0.1068 0.5173 0.091 Uiso 1 1 calc R U . . .
C222 C 0.3258(5) -0.0800(4) 0.5458(5) 0.077(3) Uani 1 1 d . U . . .
C223 C 0.3477(7) -0.0944(6) 0.5943(6) 0.113(4) Uani 1 1 d . U . . .
C224 C 0.0226(9) 0.2616(6) 0.4170(6) 0.111(5) Uani 1 1 d . U . . .
C225 C 0.0617(5) 0.2310(3) 0.4519(3) 0.061(2) Uani 1 1 d . U . . .
C226 C 0.1284(5) 0.2410(3) 0.4569(3) 0.056(2) Uani 1 1 d . U . . .
H226 H 0.1477 0.2669 0.4379 0.067 Uiso 1 1 calc R U . . .
C227 C 0.1699(5) 0.2169(3) 0.4871(3) 0.059(2) Uani 1 1 d . U . . .
C228 C 0.2419(5) 0.2342(4) 0.4895(4) 0.076(3) Uani 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 C25 2.152(8) 2_675 ?
Ag1 C7 2.220(10) . ?
Ag1 O5 2.562(7) 2_675 ?
Ag1 Ag2 2.8205(10) . ?
Ag1 Ag10 2.9795(10) 2_675 ?
Ag1 Ag11 3.0235(10) 2_675 ?
Ag1 Ag12 3.2748(9) . ?
Ag2 C7 2.141(11) . ?
Ag2 C1 2.243(9) . ?
Ag2 C2 2.431(10) . ?
Ag2 Ag12 3.2081(11) . ?
Ag3A O6 2.317(8) . ?
Ag3A C19 2.360(10) . ?
Ag3A O2 2.529(11) . ?
Ag3A Ag12 2.774(4) 2_675 ?
Ag3A Ag4A 2.846(16) . ?
Ag3A Ag6 3.050(11) 2_675 ?
Ag3B C19 2.212(10) . ?
Ag3B O5 2.321(11) . ?
Ag3B O2 2.368(6) . ?
Ag3B O6 2.393(8) . ?
Ag3B Ag5 2.913(8) . ?
Ag3B Ag12 3.091(9) 2_675 ?
Ag3B Ag4B 3.208(10) . ?
Ag4A C19 2.122(12) . ?
Ag4A C1 2.183(12) . ?
Ag4A Ag6 2.741(16) 2_675 ?
Ag4A Ag5 3.130(13) . ?
Ag4B C19 2.158(13) . ?
Ag4B C1 2.250(13) . ?
Ag4B O3 2.511(11) . ?
Ag4B O10 2.587(11) . ?
Ag4B Ag6 2.900(9) 2_675 ?
Ag4B Ag5 3.008(9) . ?
Ag5 C37 2.178(8) . ?
Ag5 C19 2.199(9) . ?
Ag5 C38 2.593(8) . ?
Ag5 Ag11 3.1816(12) . ?
Ag6 C1 2.104(10) 2_675 ?
Ag6 C13 2.162(9) . ?
Ag6 Ag4A 2.741(16) 2_675 ?
Ag6 Ag4B 2.900(9) 2_675 ?
Ag6 Ag3A 3.051(11) 2_675 ?
Ag6 Ag10 3.2134(10) . ?
Ag6 Ag12 3.2373(10) . ?
Ag6 Ag7 3.3545(10) . ?
Ag7 C31 2.141(8) . ?
Ag7 C13 2.241(8) . ?
Ag7 O1 2.589(5) . ?
Ag7 C14 2.607(8) . ?
Ag7 Ag12 2.9419(10) . ?
Ag7 Ag9 2.9491(9) . ?
Ag7 Ag8 3.0851(9) . ?
Ag8 C31 2.220(8) . ?
Ag8 O3 2.329(6) . ?
Ag8 O9 2.337(7) . ?
Ag8 O10 2.392(6) . ?
Ag8 Ag9 2.8693(9) . ?
Ag9 C31 2.211(8) . ?
Ag9 C37 2.294(8) . ?
Ag9 O8 2.473(5) . ?
Ag9 C38 2.647(8) . ?
Ag9 Ag11 3.0252(9) . ?
Ag10 C25 2.289(8) . ?
Ag10 O7 2.337(6) . ?
Ag10 O1 2.347(5) . ?
Ag10 O8 2.561(6) . ?
Ag10 Ag1 2.9794(10) 2_675 ?
Ag10 Ag11 3.0496(10) . ?
Ag11 C37 2.091(9) . ?
Ag11 C25 2.155(8) . ?
Ag11 Ag1 3.0234(10) 2_675 ?
Ag12 C13 2.126(9) . ?
Ag12 C7 2.215(9) . ?
Ag12 C8 2.528(9) . ?
Ag12 Ag3A 2.774(5) 2_675 ?
Ag12 Ag3B 3.091(9) 2_675 ?
Ag13 C64 2.193(9) . ?
Ag13 C88 2.243(8) 2_565 ?
Ag13 Ag21 2.9308(9) 2_565 ?
Ag13 Ag15 2.9744(10) . ?
Ag13 Ag22 3.1532(10) 2_565 ?
Ag13 Ag14 3.1732(9) . ?
Ag14 C64 2.186(8) . ?
Ag14 C76 2.186(8) . ?
Ag14 Ag17 3.0087(9) . ?
Ag14 A16 3.061(4) . ?
Ag14 Ag15 3.2420(10) . ?
Ag15 C58 2.100(8) 2_565 ?
Ag15 C64 2.121(8) . ?
Ag15 Ag23 2.9946(11) 2_565 ?
Ag15 Ag24 3.1163(9) 2_565 ?
Ag16 O16 2.23(3) . ?
Ag16 O11 2.29(4) 2_565 ?
Ag16 C76 2.53(6) . ?
Ag16 Ag20 2.75(8) . ?
Ag16 Ag17 3.15(3) . ?
A16 C76 2.227(9) . ?
A16 O16 2.339(7) . ?
A16 O11 2.372(6) 2_565 ?
A16 O15 2.412(7) . ?
A16 C77 2.589(9) . ?
A16 Ag17 3.243(2) . ?
A16 Ag20 3.303(6) . ?
Ag17 C76 2.128(8) . ?
Ag17 C70 2.276(7) . ?
Ag17 O14 2.444(5) 2_565 ?
Ag17 C71 2.539(8) . ?
Ag17 Ag19 2.9913(9) . ?
Ag17 Ag18 3.2483(9) . ?
Ag18 C82 2.098(8) 2_565 ?
Ag18 C70 2.105(8) . ?
Ag18 Ag24 2.8674(9) . ?
Ag18 Ag19 3.1719(10) . ?
Ag19 C94 2.157(9) . ?
Ag19 C70 2.188(8) . ?
Ag19 Ag20 3.0403(9) . ?
Ag19 Ag23 3.2110(11) . ?
Ag20 C94 2.163(8) . ?
Ag20 C82 2.253(8) . ?
Ag20 O11 2.581(5) 2_565 ?
Ag20 C83 2.601(8) . ?
Ag20 Ag21 2.9282(9) . ?
Ag20 Ag24 3.2824(9) 2_565 ?
Ag21 C88 2.100(8) . ?
Ag21 C94 2.225(8) . ?
Ag21 C95 2.614(8) . ?
Ag21 Ag13 2.9309(9) 2_565 ?
Ag21 Ag22 3.3161(9) . ?
Ag22 C88 2.252(7) . ?
Ag22 O17 2.288(6) . ?
Ag22 O14 2.341(5) . ?
Ag22 C89 2.479(8) . ?
Ag22 O18 2.511(6) . ?
Ag22 Ag13 3.1530(10) 2_565 ?
Ag23 C58 2.269(8) . ?
Ag23 O19 2.321(6) . ?
Ag23 O12 2.384(5) . ?
Ag23 O20 2.453(6) . ?
Ag23 Ag15 2.9946(11) 2_565 ?
Ag23 Ag24 3.3290(10) . ?
Ag24 C58 2.214(7) . ?
Ag24 C82 2.219(8) 2_565 ?
Ag24 O11 2.434(5) . ?
Ag24 C59 2.539(9) . ?
Ag24 Ag15 3.1163(9) 2_565 ?
Ag24 Ag20 3.2826(9) 2_565 ?
Ag25 C133 2.289(7) . ?
Ag25 O21 2.340(5) . ?
Ag25 O30 2.344(6) . ?
Ag25 O29 2.415(6) . ?
Ag25 C134 2.571(7) . ?
Ag25 Ag28 3.0313(8) . ?
Ag25 Ag27 3.2905(9) . ?
Ag25 Ag34 3.3409(9) 2_666 ?
Ag26 C139 2.172(7) . ?
Ag26 C127 2.244(8) . ?
Ag26 O29 2.586(6) . ?
Ag26 Ag33 3.0221(8) 2_666 ?
Ag26 Ag30 3.1264(9) . ?
Ag26 Ag29 3.1276(9) . ?
Ag26 Ag28 3.2061(9) . ?
Ag27 C133 2.100(7) . ?
Ag27 C115 2.159(7) 2_666 ?
Ag27 Ag35 2.8010(8) 2_666 ?
Ag27 Ag28 3.0490(8) . ?
Ag28 C139 2.178(7) . ?
Ag28 C133 2.262(7) . ?
Ag28 O27 2.570(5) . ?
Ag28 Ag29 3.1227(9) . ?
Ag29 C139 2.181(7) . ?
Ag29 C145 2.228(7) . ?
Ag29 Ag32 3.0398(9) . ?
Ag29 Ag31 3.0838(9) . ?
Ag30 C127 2.278(7) . ?
Ag30 O24 2.315(6) . ?
Ag30 O25 2.317(5) . ?
Ag30 O26 2.438(6) . ?
Ag30 C128 2.617(8) . ?
Ag30 Ag33 3.1016(8) 2_666 ?
Ag30 Ag35 3.1830(9) . ?
Ag31 C145 2.279(7) . ?
Ag31 O28 2.327(5) . ?
Ag31 O22 2.365(5) . ?
Ag31 O27 2.461(5) . ?
Ag31 C146 2.604(7) . ?
Ag31 Ag36 3.2386(9) . ?
Ag31 Ag32 3.2669(8) . ?
Ag32 C145 2.092(7) . ?
Ag32 C121 2.147(7) . ?
Ag32 Ag34 2.8196(8) . ?
Ag33 C127 2.092(7) 2_666 ?
Ag33 C151 2.138(7) . ?
Ag33 Ag36 2.8307(8) . ?
Ag33 Ag26 3.0221(8) 2_666 ?
Ag33 Ag30 3.1016(8) 2_666 ?
Ag34 C121 2.194(8) . ?
Ag34 C151 2.244(8) . ?
Ag34 O21 2.503(5) 2_666 ?
Ag34 C152 2.577(7) . ?
Ag34 Ag35 3.3218(9) . ?
Ag34 Ag25 3.3409(9) 2_666 ?
Ag35 C115 2.179(8) . ?
Ag35 C121 2.212(7) . ?
Ag35 C122 2.618(8) . ?
Ag35 Ag27 2.8010(8) 2_666 ?
Ag36 C151 2.175(8) . ?
Ag36 C115 2.274(7) 2_666 ?
Ag36 O22 2.468(5) . ?
Ag36 C116 2.482(7) 2_666 ?
Ag37 C196 2.297(9) . ?
Ag37 O37 2.309(7) . ?
Ag37 O33 2.353(5) . ?
Ag37 O38 2.509(7) . ?
Ag37 Ag38 2.9737(12) . ?
Ag37 Ag42 3.1291(12) 2_556 ?
Ag37 Ag39 3.2311(10) . ?
Ag38 C196 2.075(10) . ?
Ag38 C208 2.131(9) . ?
Ag38 A48 2.892(7) . ?
Ag38 Ag39 3.0712(9) . ?
Ag38 Ag48 3.18(4) . ?
Ag38 Ag46 3.25(2) . ?
Ag39 C178 2.219(8) 2_556 ?
Ag39 C196 2.240(8) . ?
Ag39 O32 2.498(5) . ?
Ag39 O35 2.578(6) . ?
Ag39 C197 2.606(8) . ?
Ag39 Ag44 2.8611(8) 2_556 ?
Ag39 Ag40 3.3030(9) . ?
Ag40 C202 2.106(9) . ?
Ag40 C178 2.245(8) 2_556 ?
Ag40 C179 2.531(8) 2_556 ?
Ag40 Ag41 2.743(6) . ?
Ag40 Ag47 2.9678(9) 2_556 ?
Ag40 Ag42 3.2078(10) . ?
Ag41 O36 2.271(7) . ?
Ag41 O32 2.399(6) . ?
Ag41 C190 2.533(10) . ?
Ag41 Ag43 3.102(3) . ?
Ag41 Ag46 3.24(3) . ?
Ag41 Ag42 3.270(7) . ?
A41A C190 2.166(9) . ?
A41A O35 2.340(7) . ?
A41A O32 2.385(5) . ?
A41A O36 2.417(7) . ?
A41A C191 2.614(8) . ?
A41A A46A 3.063(8) . ?
A41A Ag43 3.2558(16) . ?
Ag42 C202 2.177(9) . ?
Ag42 C184 2.192(8) . ?
Ag42 C23A 2.39(3) . ?
Ag42 O33 2.591(5) 2_556 ?
Ag42 Ag43 2.9179(9) . ?
Ag42 Ag37 3.1290(12) 2_556 ?
Ag42 Ag44 3.2397(10) . ?
Ag42 Ag47 3.3106(9) 2_556 ?
Ag43 C190 2.154(8) . ?
Ag43 C184 2.285(8) . ?
Ag43 O31 2.443(5) . ?
Ag43 C185 2.560(9) . ?
Ag43 A46A 2.907(4) . ?
Ag43 Ag46 2.998(14) . ?
Ag43 Ag44 3.3757(8) . ?
Ag44 C184 2.099(8) . ?
Ag44 C178 2.110(8) . ?
Ag44 Ag39 2.8610(8) 2_556 ?
Ag44 Ag45 3.22(4) . ?
Ag45 O40 2.092(17) . ?
Ag45 O31 2.226(12) . ?
Ag45 C172 2.47(3) . ?
Ag45 Ag47 3.086(11) . ?
Ag45 Ag48 3.09(6) . ?
A45A C172 2.143(12) . ?
A45A O40 2.345(10) . ?
A45A O31 2.394(8) . ?
A45A O39 2.431(8) . ?
A45A C173 2.539(13) . ?
A45A A48 3.056(10) . ?
A45A Ag47 3.125(4) . ?
Ag46 C190 2.119(10) . ?
Ag46 C208 2.272(11) . ?
Ag46 C209 2.518(11) . ?
Ag46 Ag48 3.19(3) . ?
A46A C190 2.246(11) . ?
A46A C208 2.259(10) . ?
A46A C209 2.517(9) . ?
A46A A48 3.148(8) . ?
Ag47 C172 2.117(8) . ?
Ag47 C202 2.235(8) 2_556 ?
Ag47 C203 2.519(10) 2_556 ?
Ag47 O33 2.565(5) . ?
Ag47 A48 2.960(5) . ?
Ag47 Ag40 2.9680(9) 2_556 ?
Ag47 Ag48 3.020(17) . ?
Ag47 Ag42 3.3108(9) 2_556 ?
Ag48 C172 2.07(2) . ?
Ag48 C208 2.18(2) . ?
Ag48 C173 2.71(3) . ?
A48 C208 2.128(10) . ?
A48 C172 2.235(11) . ?
V1 O3 1.649(6) . ?
V1 O2 1.653(6) . ?
V1 O1 1.677(5) . ?
V1 O4 1.794(11) . ?
V1 O4 1.816(12) 2_675 ?
V2 O14 1.676(5) . ?
V2 O12 1.681(5) . ?
V2 O11 1.684(5) . ?
V2 O13 1.7768(11) . ?
V3 O24 1.648(6) . ?
V3 O22 1.679(5) . ?
V3 O21 1.687(5) . ?
V3 O23 1.770(11) . ?
V3 O23 1.839(11) 2_666 ?
V4 O31 1.666(6) . ?
V4 O32 1.672(5) . ?
V4 O33 1.681(5) . ?
V4 O34 1.7596(11) . ?
F1 C52 1.345(14) . ?
F2 C52 1.324(15) . ?
F3 C52 1.311(14) . ?
F4 C48 1.274(15) . ?
F5 C48 1.301(16) . ?
F6 C48 1.282(14) . ?
F7 C53 1.309(19) . ?
F8 C53 1.281(18) . ?
F9 C53 1.23(2) . ?
F10 C57 1.285(12) . ?
F11 C57 1.317(15) . ?
F12 C57 1.296(13) . ?
F13 C47 1.272(17) . ?
F14 C47 1.325(19) . ?
F15 C47 1.35(2) . ?
F16 C43 1.301(15) . ?
F17 C43 1.291(17) . ?
F18 C43 1.352(17) . ?
F19 C110 1.314(12) . ?
F20 C110 1.258(11) . ?
F21 C110 1.309(11) . ?
F22 C114 1.329(13) . ?
F23 C114 1.278(13) . ?
F24 C114 1.297(12) . ?
F25 C104 1.311(10) . ?
F26 C104 1.324(10) . ?
F27 C104 1.330(11) . ?
F28 C100 1.313(12) . ?
F29 C100 1.302(11) . ?
F30 C100 1.285(11) . ?
F31 C109 1.296(13) . ?
F32 C109 1.213(15) . ?
F33 C109 1.302(15) . ?
F34 C105 1.324(12) . ?
F35 C105 1.328(15) . ?
F36 C105 1.306(14) . ?
F37 C167 1.343(12) . ?
F38 C167 1.314(10) . ?
F39 C167 1.315(11) . ?
F40A C171 1.290(15) . ?
F41A C171 1.299(16) . ?
F42A C171 1.344(14) . ?
F40B C171 1.293(17) . ?
F41B C171 1.369(18) . ?
F42B C171 1.291(17) . ?
F43 C166 1.283(12) . ?
F44 C166 1.315(13) . ?
F45 C166 1.247(13) . ?
F46 C162 1.297(13) . ?
F47 C162 1.320(13) . ?
F48 C162 1.314(11) . ?
F49 C161 1.267(12) . ?
F50 C161 1.253(12) . ?
F51 C161 1.266(13) . ?
F52 C157 1.273(13) . ?
F53 C157 1.363(11) . ?
F54 C157 1.266(12) . ?
F52A C157 1.371(13) . ?
F53A C157 1.283(13) . ?
F54A C157 1.275(13) . ?
F55 C223 1.271(18) . ?
F56 C223 1.363(17) . ?
F57 C223 1.228(15) . ?
F58 C219 1.294(14) . ?
F59 C219 1.348(15) . ?
F60 C219 1.295(14) . ?
F61 C214 1.285(13) . ?
F62 C214 1.329(12) . ?
F63 C214 1.320(12) . ?
F64 C218 1.293(17) . ?
F65 C218 1.271(19) . ?
F66 C218 1.24(2) . ?
F67 C224 1.35(2) . ?
F68 C224 1.244(14) . ?
F69 C224 1.270(15) . ?
F70 C228 1.302(14) . ?
F71 C228 1.298(15) . ?
F72 C228 1.303(13) . ?
F70A C228 1.332(18) . ?
F71A C228 1.318(17) . ?
F72A C228 1.328(16) . ?
O4 O4 1.04(2) 2_675 ?
O4 V1 1.816(12) 2_675 ?
O5 C51 1.245(11) . ?
O5 Ag1 2.562(7) 2_675 ?
O6 C49 1.234(12) . ?
O7 C54 1.239(12) . ?
O8 C56 1.249(10) . ?
O9 C44 1.238(12) . ?
O10 C46 1.266(11) . ?
O11 Ag16 2.29(4) 2_565 ?
O11 A16 2.372(6) 2_565 ?
O11 Ag20 2.582(5) 2_565 ?
O13 V2 1.7769(11) 2_565 ?
O14 Ag17 2.444(5) 2_565 ?
O15 C106 1.247(10) . ?
O16 C108 1.241(10) . ?
O17 C111 1.248(9) . ?
O18 C113 1.238(10) . ?
O19 C101 1.241(10) . ?
O20 C103 1.253(9) . ?
O21 Ag34 2.503(5) 2_666 ?
O23 O23 1.02(2) 2_666 ?
O23 V3 1.839(11) 2_666 ?
O25 C168 1.251(9) . ?
O26 C170 1.243(9) . ?
O27 C158 1.246(8) . ?
O28 C160 1.243(9) . ?
O29 C165 1.260(10) . ?
O30 C163 1.255(11) . ?
O33 Ag42 2.591(5) 2_556 ?
O34 V4 1.7596(11) 2_556 ?
O35 C222 1.252(11) . ?
O36 C220 1.254(13) . ?
O37 C217 1.216(11) . ?
O38 C215 1.239(9) . ?
O39 C227 1.227(10) . ?
O40 C225 1.248(10) . ?
C1 C2 1.181(13) . ?
C1 Ag6 2.104(10) 2_675 ?
C2 C3 1.533(14) . ?
C3 C5 1.504(17) . ?
C3 C6 1.533(18) . ?
C3 C4 1.556(19) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.188(13) . ?
C8 C9 1.499(14) . ?
C9 C12 1.456(17) . ?
C9 C11 1.464(16) . ?
C9 C10 1.55(2) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.195(12) . ?
C14 C15 1.468(13) . ?
C15 C16 1.46(2) . ?
C15 C18 1.505(16) . ?
C15 C17 1.58(2) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.183(12) . ?
C20 C21 1.472(13) . ?
C21 C23 1.418(17) . ?
C21 C22 1.490(17) . ?
C21 C24 1.55(2) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 C26 1.190(10) . ?
C25 Ag1 2.152(8) 2_675 ?
C26 C27 1.474(11) . ?
C27 C30 1.447(16) . ?
C27 C29 1.486(15) . ?
C27 C28 1.517(16) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 H29C 0.9800 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 C32 1.203(10) . ?
C32 C33 1.468(12) . ?
C33 C36 1.511(13) . ?
C33 C35 1.514(15) . ?
C33 C34 1.535(14) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.220(11) . ?
C38 C39 1.484(12) . ?
C39 C42 1.510(14) . ?
C39 C41 1.532(14) . ?
C39 C40 1.536(13) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.541(16) . ?
C44 C45 1.361(15) . ?
C45 C46 1.383(15) . ?
C45 H45 0.9500 . ?
C46 C47 1.53(2) . ?
C48 C49 1.514(15) . ?
C49 C50 1.392(15) . ?
C50 C51 1.390(14) . ?
C50 H50 0.9500 . ?
C51 C52 1.523(16) . ?
C53 C54 1.513(15) . ?
C54 C55 1.383(15) . ?
C55 C56 1.388(13) . ?
C55 H55 0.9500 . ?
C56 C57 1.517(14) . ?
C58 C59 1.219(11) . ?
C58 Ag15 2.100(8) 2_565 ?
C59 C60 1.511(13) . ?
C60 C61 1.463(18) . ?
C60 C62 1.492(16) . ?
C60 C63 1.496(18) . ?
C61 H61A 0.9800 . ?
C61 H61B 0.9800 . ?
C61 H61C 0.9800 . ?
C62 H62A 0.9800 . ?
C62 H62B 0.9800 . ?
C62 H62C 0.9800 . ?
C63 H63A 0.9800 . ?
C63 H63B 0.9800 . ?
C63 H63C 0.9800 . ?
C64 C65 1.198(11) . ?
C65 C66 1.475(12) . ?
C66 C68 1.468(17) . ?
C66 C67 1.498(15) . ?
C66 C69 1.549(18) . ?
C67 H67A 0.9800 . ?
C67 H67B 0.9800 . ?
C67 H67C 0.9800 . ?
C68 H68A 0.9800 . ?
C68 H68B 0.9800 . ?
C68 H68C 0.9800 . ?
C69 H69A 0.9800 . ?
C69 H69B 0.9800 . ?
C69 H69C 0.9800 . ?
C70 C71 1.210(10) . ?
C71 C72 1.482(11) . ?
C72 C74 1.519(13) . ?
C72 C73 1.525(12) . ?
C72 C75 1.538(14) . ?
C73 H73A 0.9800 . ?
C73 H73B 0.9800 . ?
C73 H73C 0.9800 . ?
C74 H74A 0.9800 . ?
C74 H74B 0.9800 . ?
C74 H74C 0.9800 . ?
C75 H75A 0.9800 . ?
C75 H75B 0.9800 . ?
C75 H75C 0.9800 . ?
C76 C77 1.219(11) . ?
C77 C78 1.465(11) . ?
C78 C81 1.503(15) . ?
C78 C80 1.521(14) . ?
C78 C79 1.546(14) . ?
C79 H79A 0.9800 . ?
C79 H79B 0.9800 . ?
C79 H79C 0.9800 . ?
C80 H80A 0.9800 . ?
C80 H80B 0.9800 . ?
C80 H80C 0.9800 . ?
C81 H81A 0.9800 . ?
C81 H81B 0.9800 . ?
C81 H81C 0.9800 . ?
C82 C83 1.220(11) . ?
C82 Ag18 2.098(8) 2_565 ?
C82 Ag24 2.219(8) 2_565 ?
C83 C84 1.462(12) . ?
C84 C87 1.508(14) . ?
C84 C86 1.530(14) . ?
C84 C85 1.539(14) . ?
C85 H85A 0.9800 . ?
C85 H85B 0.9800 . ?
C85 H85C 0.9800 . ?
C86 H86A 0.9800 . ?
C86 H86B 0.9800 . ?
C86 H86C 0.9800 . ?
C87 H87A 0.9800 . ?
C87 H87B 0.9800 . ?
C87 H87C 0.9800 . ?
C88 C89 1.223(10) . ?
C88 Ag13 2.243(8) 2_565 ?
C89 C90 1.479(11) . ?
C90 C91 1.514(13) . ?
C90 C92 1.526(13) . ?
C90 C93 1.528(13) . ?
C91 H91A 0.9800 . ?
C91 H91B 0.9800 . ?
C91 H91C 0.9800 . ?
C92 H92A 0.9800 . ?
C92 H92B 0.9800 . ?
C92 H92C 0.9800 . ?
C93 H93A 0.9800 . ?
C93 H93B 0.9800 . ?
C93 H93C 0.9800 . ?
C94 C95 1.208(11) . ?
C95 C96 1.483(12) . ?
C96 C99 1.503(13) . ?
C96 C98 1.520(14) . ?
C96 C97 1.524(13) . ?
C97 H97A 0.9800 . ?
C97 H97B 0.9800 . ?
C97 H97C 0.9800 . ?
C98 H98A 0.9800 . ?
C98 H98B 0.9800 . ?
C98 H98C 0.9800 . ?
C99 H99A 0.9800 . ?
C99 H99B 0.9800 . ?
C99 H99C 0.9800 . ?
C100 C101 1.531(12) . ?
C101 C102 1.385(12) . ?
C102 C103 1.394(11) . ?
C102 H102 0.9500 . ?
C103 C104 1.511(12) . ?
C105 C106 1.519(15) . ?
C106 C107 1.384(13) . ?
C107 C108 1.387(13) . ?
C107 H107 0.9500 . ?
C108 C109 1.523(14) . ?
C110 C111 1.518(12) . ?
C111 C112 1.366(11) . ?
C112 C113 1.387(12) . ?
C112 H112 0.9500 . ?
C113 C114 1.529(13) . ?
C115 C116 1.201(10) . ?
C115 Ag27 2.159(7) 2_666 ?
C115 Ag36 2.274(7) 2_666 ?
C116 C117 1.492(11) . ?
C116 Ag36 2.482(7) 2_666 ?
C117 C118 1.494(12) . ?
C117 C120 1.496(13) . ?
C117 C119 1.532(13) . ?
C118 H11F 0.9800 . ?
C118 H11G 0.9800 . ?
C118 H11H 0.9800 . ?
C119 H11I 0.9800 . ?
C119 H11J 0.9800 . ?
C119 H11K 0.9800 . ?
C120 H12D 0.9800 . ?
C120 H12E 0.9800 . ?
C120 H12F 0.9800 . ?
C121 C122 1.195(10) . ?
C122 C123 1.481(11) . ?
C123 C126 1.512(13) . ?
C123 C125 1.535(14) . ?
C123 C124 1.542(11) . ?
C124 H12G 0.9800 . ?
C124 H12H 0.9800 . ?
C124 H12I 0.9800 . ?
C125 H12J 0.9800 . ?
C125 H12K 0.9800 . ?
C125 H12L 0.9800 . ?
C126 H12M 0.9800 . ?
C126 H12N 0.9800 . ?
C126 H12O 0.9800 . ?
C127 C128 1.216(10) . ?
C127 Ag33 2.091(7) 2_666 ?
C128 C129 1.473(11) . ?
C129 C130 1.480(16) . ?
C129 C31A 1.488(16) . ?
C129 C32A 1.538(16) . ?
C129 C132 1.542(16) . ?
C129 C30A 1.548(16) . ?
C129 C131 1.550(15) . ?
C130 H13A 0.9800 . ?
C130 H13B 0.9800 . ?
C130 H13C 0.9800 . ?
C131 H13D 0.9800 . ?
C131 H13E 0.9800 . ?
C131 H13F 0.9800 . ?
C132 H13G 0.9800 . ?
C132 H13H 0.9800 . ?
C132 H13I 0.9800 . ?
C30A H30D 0.9800 . ?
C30A H30E 0.9800 . ?
C30A H30F 0.9800 . ?
C31A H31A 0.9800 . ?
C31A H31B 0.9800 . ?
C31A H31C 0.9800 . ?
C32A H32A 0.9800 . ?
C32A H32B 0.9800 . ?
C32A H32C 0.9800 . ?
C133 C134 1.220(10) . ?
C134 C135 1.488(10) . ?
C135 C138 1.524(12) . ?
C135 C137 1.529(11) . ?
C135 C136 1.531(12) . ?
C136 H13J 0.9800 . ?
C136 H13K 0.9800 . ?
C136 H13L 0.9800 . ?
C137 H13M 0.9800 . ?
C137 H13N 0.9800 . ?
C137 H13O 0.9800 . ?
C138 H13P 0.9800 . ?
C138 H13Q 0.9800 . ?
C138 H13R 0.9800 . ?
C139 C140 1.178(10) . ?
C140 C141 1.483(11) . ?
C141 C143 1.393(18) . ?
C141 C142 1.481(16) . ?
C141 C144 1.522(18) . ?
C142 H14A 0.9800 . ?
C142 H14B 0.9800 . ?
C142 H14C 0.9800 . ?
C143 H14D 0.9800 . ?
C143 H14E 0.9800 . ?
C143 H14F 0.9800 . ?
C144 H14G 0.9800 . ?
C144 H14H 0.9800 . ?
C144 H14I 0.9800 . ?
C145 C146 1.208(10) . ?
C146 C147 1.485(11) . ?
C147 C148 1.490(14) . ?
C147 C149 1.514(13) . ?
C147 C150 1.564(16) . ?
C148 H14J 0.9800 . ?
C148 H14K 0.9800 . ?
C148 H14L 0.9800 . ?
C149 H14M 0.9800 . ?
C149 H14N 0.9800 . ?
C149 H14O 0.9800 . ?
C150 H15A 0.9800 . ?
C150 H15B 0.9800 . ?
C150 H15C 0.9800 . ?
C151 C152 1.204(10) . ?
C152 C153 1.474(11) . ?
C153 C154 1.482(15) . ?
C153 C55A 1.486(12) . ?
C153 C54A 1.550(14) . ?
C153 C156 1.551(15) . ?
C153 C155 1.559(15) . ?
C153 C56A 1.564(19) . ?
C154 H15D 0.9800 . ?
C154 H15E 0.9800 . ?
C154 H15F 0.9800 . ?
C155 H15G 0.9800 . ?
C155 H15H 0.9800 . ?
C155 H15I 0.9800 . ?
C156 H15J 0.9800 . ?
C156 H15K 0.9800 . ?
C156 H15L 0.9800 . ?
C54A H54A 0.9800 . ?
C54A H54B 0.9800 . ?
C54A H54C 0.9800 . ?
C55A H55C 0.9800 . ?
C55A H55D 0.9800 . ?
C55A H55E 0.9800 . ?
C56A H56A 0.9800 . ?
C56A H56B 0.9800 . ?
C56A H56C 0.9800 . ?
C157 C158 1.525(11) . ?
C158 C159 1.378(11) . ?
C159 C160 1.385(12) . ?
C159 H159 0.9500 . ?
C160 C161 1.521(13) . ?
C162 C163 1.535(13) . ?
C163 C164 1.380(13) . ?
C164 C165 1.386(12) . ?
C164 H164 0.9500 . ?
C165 C166 1.498(14) . ?
C167 C168 1.531(12) . ?
C168 C169 1.390(12) . ?
C169 C170 1.384(12) . ?
C169 H169 0.9500 . ?
C170 C171 1.516(12) . ?
C172 C173 1.177(11) . ?
C173 C174 1.487(13) . ?
C174 C176 1.466(17) . ?
C174 C175 1.547(18) . ?
C174 C177 1.547(17) . ?
C175 H17D 0.9800 . ?
C175 H17E 0.9800 . ?
C175 H17F 0.9800 . ?
C176 H17G 0.9800 . ?
C176 H17H 0.9800 . ?
C176 H17I 0.9800 . ?
C177 H17J 0.9800 . ?
C177 H17K 0.9800 . ?
C177 H17L 0.9800 . ?
C178 C179 1.219(11) . ?
C178 Ag39 2.219(8) 2_556 ?
C178 Ag40 2.245(8) 2_556 ?
C179 C180 1.484(12) . ?
C179 Ag40 2.531(8) 2_556 ?
C180 C183 1.491(14) . ?
C180 C182 1.513(13) . ?
C180 C181 1.523(13) . ?
C181 H18D 0.9800 . ?
C181 H18E 0.9800 . ?
C181 H18F 0.9800 . ?
C182 H18G 0.9800 . ?
C182 H18H 0.9800 . ?
C182 H18I 0.9800 . ?
C183 H18J 0.9800 . ?
C183 H18K 0.9800 . ?
C183 H18L 0.9800 . ?
C184 C185 1.192(11) . ?
C185 C186 1.480(13) . ?
C186 C189 1.369(17) . ?
C186 C187 1.487(13) . ?
C186 C188 1.73(2) . ?
C187 H18M 0.9800 . ?
C187 H18N 0.9800 . ?
C187 H18O 0.9800 . ?
C189 H18S 0.9800 . ?
C189 H18T 0.9800 . ?
C189 H18U 0.9800 . ?
C190 C191 1.210(11) . ?
C191 C192 1.483(11) . ?
C192 C195 1.511(13) . ?
C192 C194 1.520(13) . ?
C192 C193 1.536(12) . ?
C193 H19A 0.9800 . ?
C193 H19B 0.9800 . ?
C193 H19C 0.9800 . ?
C194 H19D 0.9800 . ?
C194 H19E 0.9800 . ?
C194 H19F 0.9800 . ?
C195 H19G 0.9800 . ?
C195 H19H 0.9800 . ?
C195 H19I 0.9800 . ?
C196 C197 1.217(12) . ?
C197 C198 1.496(13) . ?
C198 C201 1.492(16) . ?
C198 C200 1.523(14) . ?
C198 C199 1.524(14) . ?
C199 H19J 0.9800 . ?
C199 H19K 0.9800 . ?
C199 H19L 0.9800 . ?
C200 H20A 0.9800 . ?
C200 H20B 0.9800 . ?
C200 H20C 0.9800 . ?
C201 H20D 0.9800 . ?
C201 H20E 0.9800 . ?
C201 H20F 0.9800 . ?
C202 C23A 1.086(16) . ?
C202 C203 1.267(14) . ?
C202 Ag47 2.234(8) 2_556 ?
C203 C204 1.527(15) . ?
C203 Ag47 2.519(10) 2_556 ?
C204 C205 1.517(16) . ?
C204 C206 1.531(15) . ?
C204 C207 1.534(14) . ?
C205 H20G 0.9800 . ?
C205 H20H 0.9800 . ?
C205 H20I 0.9800 . ?
C206 H20J 0.9800 . ?
C206 H20K 0.9800 . ?
C206 H20L 0.9800 . ?
C207 H20M 0.9800 . ?
C207 H20N 0.9800 . ?
C207 H20O 0.9800 . ?
C23A C24A 1.492(18) . ?
C24A C27A 1.519(19) . ?
C24A C26A 1.535(19) . ?
C24A C25A 1.537(18) . ?
C25A H25A 0.9800 . ?
C25A H25B 0.9800 . ?
C25A H25C 0.9800 . ?
C26A H26A 0.9800 . ?
C26A H26B 0.9800 . ?
C26A H26C 0.9800 . ?
C27A H27A 0.9800 . ?
C27A H27B 0.9800 . ?
C27A H27C 0.9800 . ?
C208 C209 1.174(11) . ?
C209 C210 1.483(13) . ?
C210 C212 1.477(19) . ?
C210 C211 1.522(14) . ?
C210 C213 1.56(2) . ?
C211 H21A 0.9800 . ?
C211 H21B 0.9800 . ?
C211 H21C 0.9800 . ?
C212 H21D 0.9800 . ?
C212 H21E 0.9800 . ?
C212 H21F 0.9800 . ?
C213 H21G 0.9800 . ?
C213 H21H 0.9800 . ?
C213 H21I 0.9800 . ?
C214 C215 1.518(12) . ?
C215 C216 1.413(11) . ?
C216 C217 1.437(12) . ?
C216 H216 0.9500 . ?
C217 C218 1.536(13) . ?
C219 C220 1.551(16) . ?
C220 C221 1.372(16) . ?
C221 C222 1.356(15) . ?
C221 H221 0.9500 . ?
C222 C223 1.525(19) . ?
C224 C225 1.519(16) . ?
C225 C226 1.363(13) . ?
C226 C227 1.371(13) . ?
C226 H226 0.9500 . ?
C227 C228 1.510(13) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C25 Ag1 C7 151.7(3) 2_675 . ?
C25 Ag1 O5 108.0(3) 2_675 2_675 ?
C7 Ag1 O5 93.6(3) . 2_675 ?
C25 Ag1 Ag2 117.5(2) 2_675 . ?
C7 Ag1 Ag2 48.5(3) . . ?
O5 Ag1 Ag2 133.38(19) 2_675 . ?
C25 Ag1 Ag10 49.8(2) 2_675 2_675 ?
C7 Ag1 Ag10 120.7(3) . 2_675 ?
O5 Ag1 Ag10 139.79(16) 2_675 2_675 ?
Ag2 Ag1 Ag10 72.67(3) . 2_675 ?
C25 Ag1 Ag11 45.5(2) 2_675 2_675 ?
C7 Ag1 Ag11 161.4(2) . 2_675 ?
O5 Ag1 Ag11 79.68(17) 2_675 2_675 ?
Ag2 Ag1 Ag11 126.38(3) . 2_675 ?
Ag10 Ag1 Ag11 61.06(2) 2_675 2_675 ?
C25 Ag1 Ag12 163.3(2) 2_675 . ?
C7 Ag1 Ag12 42.3(2) . . ?
O5 Ag1 Ag12 70.54(19) 2_675 . ?
Ag2 Ag1 Ag12 63.00(2) . . ?
Ag10 Ag1 Ag12 120.23(3) 2_675 . ?
Ag11 Ag1 Ag12 119.37(3) 2_675 . ?
C7 Ag2 C1 159.8(3) . . ?
C7 Ag2 C2 131.8(4) . . ?
C1 Ag2 C2 28.9(3) . . ?
C7 Ag2 Ag1 50.9(3) . . ?
C1 Ag2 Ag1 119.2(2) . . ?
C2 Ag2 Ag1 109.3(2) . . ?
C7 Ag2 Ag12 43.5(2) . . ?
C1 Ag2 Ag12 155.0(2) . . ?
C2 Ag2 Ag12 174.3(3) . . ?
Ag1 Ag2 Ag12 65.44(2) . . ?
O6 Ag3A C19 111.9(4) . . ?
O6 Ag3A O2 133.8(6) . . ?
C19 Ag3A O2 96.1(4) . . ?
O6 Ag3A Ag12 92.8(2) . 2_675 ?
C19 Ag3A Ag12 154.8(3) . 2_675 ?
O2 Ag3A Ag12 61.3(2) . 2_675 ?
O6 Ag3A Ag4A 145.0(6) . . ?
C19 Ag3A Ag4A 47.0(3) . . ?
O2 Ag3A Ag4A 80.6(4) . . ?
Ag12 Ag3A Ag4A 113.7(2) 2_675 . ?
O6 Ag3A Ag6 123.7(5) . 2_675 ?
C19 Ag3A Ag6 100.9(4) . 2_675 ?
O2 Ag3A Ag6 83.2(2) . 2_675 ?
Ag12 Ag3A Ag6 67.34(15) 2_675 2_675 ?
Ag4A Ag3A Ag6 55.3(3) . 2_675 ?
C19 Ag3B O5 138.5(7) . . ?
C19 Ag3B O2 105.2(3) . . ?
O5 Ag3B O2 80.6(3) . . ?
C19 Ag3B O6 114.5(3) . . ?
O5 Ag3B O6 76.8(3) . . ?
O2 Ag3B O6 139.0(4) . . ?
C19 Ag3B Ag5 48.5(3) . . ?
O5 Ag3B Ag5 101.0(4) . . ?
O2 Ag3B Ag5 68.1(3) . . ?
O6 Ag3B Ag5 149.7(4) . . ?
C19 Ag3B Ag12 141.3(5) . 2_675 ?
O5 Ag3B Ag12 76.9(2) . 2_675 ?
O2 Ag3B Ag12 57.7(3) . 2_675 ?
O6 Ag3B Ag12 83.9(3) . 2_675 ?
Ag5 Ag3B Ag12 125.53(8) . 2_675 ?
C19 Ag3B Ag4B 42.1(3) . . ?
O5 Ag3B Ag4B 152.8(3) . . ?
O2 Ag3B Ag4B 75.1(2) . . ?
O6 Ag3B Ag4B 130.1(4) . . ?
Ag5 Ag3B Ag4B 58.63(18) . . ?
Ag12 Ag3B Ag4B 99.6(3) 2_675 . ?
C19 Ag4A C1 161.0(13) . . ?
C19 Ag4A Ag6 118.7(8) . 2_675 ?
C1 Ag4A Ag6 49.0(4) . 2_675 ?
C19 Ag4A Ag3A 54.4(4) . . ?
C1 Ag4A Ag3A 115.1(8) . . ?
Ag6 Ag4A Ag3A 66.1(4) 2_675 . ?
C19 Ag4A Ag5 44.6(4) . . ?
C1 Ag4A Ag5 152.1(7) . . ?
Ag6 Ag4A Ag5 124.8(3) 2_675 . ?
Ag3A Ag4A Ag5 68.8(3) . . ?
C19 Ag4B C1 148.8(6) . . ?
C19 Ag4B O3 113.9(5) . . ?
C1 Ag4B O3 89.7(4) . . ?
C19 Ag4B O10 103.5(5) . . ?
C1 Ag4B O10 103.2(5) . . ?
O3 Ag4B O10 71.4(3) . . ?
C19 Ag4B Ag6 111.3(4) . 2_675 ?
C1 Ag4B Ag6 46.1(3) . 2_675 ?
O3 Ag4B Ag6 89.0(3) . 2_675 ?
O10 Ag4B Ag6 144.8(4) . 2_675 ?
C19 Ag4B Ag5 46.9(3) . . ?
C1 Ag4B Ag5 157.6(4) . . ?
O3 Ag4B Ag5 69.0(3) . . ?
O10 Ag4B Ag5 77.2(3) . . ?
Ag6 Ag4B Ag5 123.5(3) 2_675 . ?
C19 Ag4B Ag3B 43.4(3) . . ?
C1 Ag4B Ag3B 120.6(5) . . ?
O3 Ag4B Ag3B 91.4(3) . . ?
O10 Ag4B Ag3B 133.0(5) . . ?
Ag6 Ag4B Ag3B 74.5(3) 2_675 . ?
Ag5 Ag4B Ag3B 55.8(3) . . ?
C37 Ag5 C19 165.1(3) . . ?
C37 Ag5 C38 27.9(3) . . ?
C19 Ag5 C38 148.1(3) . . ?
C37 Ag5 Ag3B 128.5(3) . . ?
C19 Ag5 Ag3B 48.9(3) . . ?
C38 Ag5 Ag3B 153.8(3) . . ?
C37 Ag5 Ag4B 149.1(3) . . ?
C19 Ag5 Ag4B 45.8(3) . . ?
C38 Ag5 Ag4B 139.7(3) . . ?
Ag3B Ag5 Ag4B 65.6(3) . . ?
C37 Ag5 Ag4A 152.2(4) . . ?
C19 Ag5 Ag4A 42.6(4) . . ?
C38 Ag5 Ag4A 143.4(4) . . ?
C37 Ag5 Ag11 40.8(2) . . ?
C19 Ag5 Ag11 137.1(3) . . ?
C38 Ag5 Ag11 68.7(2) . . ?
Ag3B Ag5 Ag11 88.95(11) . . ?
Ag4B Ag5 Ag11 130.89(17) . . ?
Ag4A Ag5 Ag11 130.56(14) . . ?
C1 Ag6 C13 164.9(3) 2_675 . ?
C1 Ag6 Ag4A 51.5(3) 2_675 2_675 ?
C13 Ag6 Ag4A 120.4(3) . 2_675 ?
C1 Ag6 Ag4B 50.4(3) 2_675 2_675 ?
C13 Ag6 Ag4B 122.4(3) . 2_675 ?
C1 Ag6 Ag3A 110.0(3) 2_675 2_675 ?
C13 Ag6 Ag3A 62.9(3) . 2_675 ?
Ag4A Ag6 Ag3A 58.6(2) 2_675 2_675 ?
C1 Ag6 Ag10 70.6(3) 2_675 . ?
C13 Ag6 Ag10 118.1(2) . . ?
Ag4A Ag6 Ag10 121.3(2) 2_675 . ?
Ag4B Ag6 Ag10 119.47(17) 2_675 . ?
Ag3A Ag6 Ag10 173.2(2) 2_675 . ?
C1 Ag6 Ag12 146.9(2) 2_675 . ?
C13 Ag6 Ag12 40.5(2) . . ?
Ag4A Ag6 Ag12 103.51(13) 2_675 . ?
Ag4B Ag6 Ag12 103.13(17) 2_675 . ?
Ag3A Ag6 Ag12 52.26(14) 2_675 . ?
Ag10 Ag6 Ag12 123.54(3) . . ?
C1 Ag6 Ag7 150.3(3) 2_675 . ?
C13 Ag6 Ag7 41.3(2) . . ?
Ag4A Ag6 Ag7 156.32(13) 2_675 . ?
Ag4B Ag6 Ag7 156.10(17) 2_675 . ?
Ag3A Ag6 Ag7 99.11(9) 2_675 . ?
Ag10 Ag6 Ag7 79.78(2) . . ?
Ag12 Ag6 Ag7 52.98(2) . . ?
C31 Ag7 C13 162.9(3) . . ?
C31 Ag7 O1 107.0(2) . . ?
C13 Ag7 O1 89.9(3) . . ?
C31 Ag7 C14 142.9(3) . . ?
C13 Ag7 C14 27.2(3) . . ?
O1 Ag7 C14 104.2(2) . . ?
C31 Ag7 Ag12 130.5(2) . . ?
C13 Ag7 Ag12 46.0(2) . . ?
O1 Ag7 Ag12 85.40(11) . . ?
C14 Ag7 Ag12 71.1(2) . . ?
C31 Ag7 Ag9 48.4(2) . . ?
C13 Ag7 Ag9 148.6(2) . . ?
O1 Ag7 Ag9 60.72(12) . . ?
C14 Ag7 Ag9 144.4(2) . . ?
Ag12 Ag7 Ag9 132.81(3) . . ?
C31 Ag7 Ag8 46.0(2) . . ?
C13 Ag7 Ag8 136.2(2) . . ?
O1 Ag7 Ag8 83.99(11) . . ?
C14 Ag7 Ag8 158.7(2) . . ?
Ag12 Ag7 Ag8 90.26(3) . . ?
Ag9 Ag7 Ag8 56.73(2) . . ?
C31 Ag7 Ag6 157.5(2) . . ?
C13 Ag7 Ag6 39.5(2) . . ?
O1 Ag7 Ag6 51.69(12) . . ?
C14 Ag7 Ag6 53.8(2) . . ?
Ag12 Ag7 Ag6 61.47(2) . . ?
Ag9 Ag7 Ag6 109.19(3) . . ?
Ag8 Ag7 Ag6 126.44(3) . . ?
C31 Ag8 O3 117.9(3) . . ?
C31 Ag8 O9 99.8(3) . . ?
O3 Ag8 O9 137.0(3) . . ?
C31 Ag8 O10 154.8(3) . . ?
O3 Ag8 O10 78.2(2) . . ?
O9 Ag8 O10 75.0(3) . . ?
C31 Ag8 Ag9 49.5(2) . . ?
O3 Ag8 Ag9 81.96(19) . . ?
O9 Ag8 Ag9 140.9(2) . . ?
O10 Ag8 Ag9 121.0(2) . . ?
C31 Ag8 Ag7 44.0(2) . . ?
O3 Ag8 Ag7 81.09(17) . . ?
O9 Ag8 Ag7 119.1(2) . . ?
O10 Ag8 Ag7 158.85(17) . . ?
Ag9 Ag8 Ag7 59.24(2) . . ?
C31 Ag9 C37 145.4(3) . . ?
C31 Ag9 O8 103.6(3) . . ?
C37 Ag9 O8 107.6(3) . . ?
C31 Ag9 C38 119.4(3) . . ?
C37 Ag9 C38 27.4(3) . . ?
O8 Ag9 C38 123.8(2) . . ?
C31 Ag9 Ag8 49.8(2) . . ?
C37 Ag9 Ag8 107.7(2) . . ?
O8 Ag9 Ag8 141.00(15) . . ?
C38 Ag9 Ag8 95.23(19) . . ?
C31 Ag9 Ag7 46.4(2) . . ?
C37 Ag9 Ag7 157.0(2) . . ?
O8 Ag9 Ag7 77.01(15) . . ?
C38 Ag9 Ag7 159.18(19) . . ?
Ag8 Ag9 Ag7 64.03(2) . . ?
C31 Ag9 Ag11 168.6(2) . . ?
C37 Ag9 Ag11 43.7(2) . . ?
O8 Ag9 Ag11 72.33(14) . . ?
C38 Ag9 Ag11 70.67(19) . . ?
Ag8 Ag9 Ag11 127.29(3) . . ?
Ag7 Ag9 Ag11 122.38(3) . . ?
C25 Ag10 O7 121.2(3) . . ?
C25 Ag10 O1 116.2(2) . . ?
O7 Ag10 O1 118.0(2) . . ?
C25 Ag10 O8 99.5(2) . . ?
O7 Ag10 O8 72.5(2) . . ?
O1 Ag10 O8 77.27(18) . . ?
C25 Ag10 Ag1 45.9(2) . 2_675 ?
O7 Ag10 Ag1 149.82(18) . 2_675 ?
O1 Ag10 Ag1 88.77(12) . 2_675 ?
O8 Ag10 Ag1 130.94(14) . 2_675 ?
C25 Ag10 Ag11 44.9(2) . . ?
O7 Ag10 Ag11 135.79(18) . . ?
O1 Ag10 Ag11 76.49(13) . . ?
O8 Ag10 Ag11 70.82(13) . . ?
Ag1 Ag10 Ag11 60.18(2) 2_675 . ?
C25 Ag10 Ag6 155.9(2) . . ?
O7 Ag10 Ag6 78.57(18) . . ?
O1 Ag10 Ag6 55.03(13) . . ?
O8 Ag10 Ag6 99.79(14) . . ?
Ag1 Ag10 Ag6 110.02(3) 2_675 . ?
Ag11 Ag10 Ag6 131.31(3) . . ?
C37 Ag11 C25 169.3(3) . . ?
C37 Ag11 Ag1 144.8(2) . 2_675 ?
C25 Ag11 Ag1 45.4(2) . 2_675 ?
C37 Ag11 Ag9 49.2(2) . . ?
C25 Ag11 Ag9 126.2(2) . . ?
Ag1 Ag11 Ag9 122.98(3) 2_675 . ?
C37 Ag11 Ag10 128.7(2) . . ?
C25 Ag11 Ag10 48.5(2) . . ?
Ag1 Ag11 Ag10 58.76(2) 2_675 . ?
Ag9 Ag11 Ag10 79.54(2) . . ?
C37 Ag11 Ag5 42.9(2) . . ?
C25 Ag11 Ag5 147.6(2) . . ?
Ag1 Ag11 Ag5 102.26(3) 2_675 . ?
Ag9 Ag11 Ag5 67.72(3) . . ?
Ag10 Ag11 Ag5 122.67(3) . . ?
C13 Ag12 C7 155.0(4) . . ?
C13 Ag12 C8 127.7(3) . . ?
C7 Ag12 C8 28.0(3) . . ?
C13 Ag12 Ag3A 68.9(4) . 2_675 ?
C7 Ag12 Ag3A 126.0(4) . 2_675 ?
C8 Ag12 Ag3A 127.0(3) . 2_675 ?
C13 Ag12 Ag7 49.3(2) . . ?
C7 Ag12 Ag7 115.8(3) . . ?
C8 Ag12 Ag7 102.1(2) . . ?
Ag3A Ag12 Ag7 117.1(3) 2_675 . ?
C13 Ag12 Ag3B 81.9(3) . 2_675 ?
C7 Ag12 Ag3B 113.0(3) . 2_675 ?
C8 Ag12 Ag3B 117.3(2) . 2_675 ?
Ag7 Ag12 Ag3B 130.34(19) . 2_675 ?
C13 Ag12 Ag2 147.7(2) . . ?
C7 Ag12 Ag2 41.7(3) . . ?
C8 Ag12 Ag2 66.2(2) . . ?
Ag3A Ag12 Ag2 130.2(2) 2_675 . ?
Ag7 Ag12 Ag2 102.40(3) . . ?
Ag3B Ag12 Ag2 120.03(16) 2_675 . ?
C13 Ag12 Ag6 41.4(3) . . ?
C7 Ag12 Ag6 160.3(3) . . ?
C8 Ag12 Ag6 167.0(2) . . ?
Ag3A Ag12 Ag6 60.4(2) 2_675 . ?
Ag7 Ag12 Ag6 65.56(2) . . ?
Ag3B Ag12 Ag6 71.67(16) 2_675 . ?
Ag2 Ag12 Ag6 118.84(3) . . ?
C13 Ag12 Ag1 157.1(2) . . ?
C7 Ag12 Ag1 42.5(3) . . ?
C8 Ag12 Ag1 64.5(2) . . ?
Ag3A Ag12 Ag1 88.2(3) 2_675 . ?
Ag7 Ag12 Ag1 153.31(3) . . ?
Ag3B Ag12 Ag1 75.23(19) 2_675 . ?
Ag2 Ag12 Ag1 51.57(2) . . ?
Ag6 Ag12 Ag1 128.39(3) . . ?
C64 Ag13 C88 146.9(3) . 2_565 ?
C64 Ag13 Ag21 163.7(2) . 2_565 ?
C88 Ag13 Ag21 45.5(2) 2_565 2_565 ?
C64 Ag13 Ag15 45.4(2) . . ?
C88 Ag13 Ag15 165.0(2) 2_565 . ?
Ag21 Ag13 Ag15 120.50(3) 2_565 . ?
C64 Ag13 Ag22 114.4(2) . 2_565 ?
C88 Ag13 Ag22 45.56(19) 2_565 2_565 ?
Ag21 Ag13 Ag22 65.94(2) 2_565 2_565 ?
Ag15 Ag13 Ag22 129.00(3) . 2_565 ?
C64 Ag13 Ag14 43.5(2) . . ?
C88 Ag13 Ag14 118.10(19) 2_565 . ?
Ag21 Ag13 Ag14 127.59(3) 2_565 . ?
Ag15 Ag13 Ag14 63.56(2) . . ?
Ag22 Ag13 Ag14 74.20(2) 2_565 . ?
C64 Ag14 C76 157.7(3) . . ?
C64 Ag14 Ag17 153.5(2) . . ?
C76 Ag14 Ag17 45.0(2) . . ?
C64 Ag14 A16 119.1(2) . . ?
C76 Ag14 A16 46.6(2) . . ?
Ag17 Ag14 A16 64.58(7) . . ?
C64 Ag14 Ag13 43.6(2) . . ?
C76 Ag14 Ag13 155.2(2) . . ?
Ag17 Ag14 Ag13 110.98(3) . . ?
A16 Ag14 Ag13 124.41(8) . . ?
C64 Ag14 Ag15 40.4(2) . . ?
C76 Ag14 Ag15 127.7(2) . . ?
Ag17 Ag14 Ag15 124.90(3) . . ?
A16 Ag14 Ag15 81.37(4) . . ?
Ag13 Ag14 Ag15 55.23(2) . . ?
C58 Ag15 C64 167.4(3) 2_565 . ?
C58 Ag15 Ag13 128.1(2) 2_565 . ?
C64 Ag15 Ag13 47.4(2) . . ?
C58 Ag15 Ag23 49.1(2) 2_565 2_565 ?
C64 Ag15 Ag23 125.2(2) . 2_565 ?
Ag13 Ag15 Ag23 78.99(3) . 2_565 ?
C58 Ag15 Ag24 45.2(2) 2_565 2_565 ?
C64 Ag15 Ag24 146.7(2) . 2_565 ?
Ag13 Ag15 Ag24 121.63(3) . 2_565 ?
Ag23 Ag15 Ag24 65.98(2) 2_565 2_565 ?
C58 Ag15 Ag14 150.2(2) 2_565 . ?
C64 Ag15 Ag14 41.9(2) . . ?
Ag13 Ag15 Ag14 61.21(2) . . ?
Ag23 Ag15 Ag14 126.56(3) 2_565 . ?
Ag24 Ag15 Ag14 104.95(3) 2_565 . ?
O16 Ag16 O11 124.0(16) . 2_565 ?
O16 Ag16 C76 126(2) . . ?
O11 Ag16 C76 99(3) 2_565 . ?
O16 Ag16 Ag20 89(2) . . ?
O11 Ag16 Ag20 60.8(11) 2_565 . ?
C76 Ag16 Ag20 143.9(18) . . ?
O16 Ag16 Ag17 157(2) . . ?
O11 Ag16 Ag17 78.6(7) 2_565 . ?
C76 Ag16 Ag17 42.3(4) . . ?
Ag20 Ag16 Ag17 102(2) . . ?
C76 A16 O16 136.6(3) . . ?
C76 A16 O11 105.9(3) . 2_565 ?
O16 A16 O11 116.0(3) . 2_565 ?
C76 A16 O15 123.7(4) . . ?
O16 A16 O15 75.8(2) . . ?
O11 A16 O15 80.1(2) 2_565 . ?
C76 A16 C77 28.1(3) . . ?
O16 A16 C77 110.1(3) . . ?
O11 A16 C77 133.6(2) 2_565 . ?
O15 A16 C77 116.5(3) . . ?
C76 A16 Ag14 45.5(2) . . ?
O16 A16 Ag14 159.1(3) . . ?
O11 A16 Ag14 72.81(14) 2_565 . ?
O15 A16 Ag14 87.8(2) . . ?
C77 A16 Ag14 65.5(2) . . ?
C76 A16 Ag17 40.7(2) . . ?
O16 A16 Ag17 141.9(2) . . ?
O11 A16 Ag17 75.66(14) 2_565 . ?
O15 A16 Ag17 141.69(19) . . ?
C77 A16 Ag17 65.22(19) . . ?
Ag14 A16 Ag17 56.93(4) . . ?
C76 A16 Ag20 129.5(3) . . ?
O16 A16 Ag20 75.2(2) . . ?
O11 A16 Ag20 50.95(17) 2_565 . ?
O15 A16 Ag20 98.2(2) . . ?
C77 A16 Ag20 145.2(2) . . ?
Ag14 A16 Ag20 120.76(11) . . ?
Ag17 A16 Ag20 89.14(13) . . ?
C76 Ag17 C70 151.9(3) . . ?
C76 Ag17 O14 108.8(2) . 2_565 ?
C70 Ag17 O14 96.6(2) . 2_565 ?
C76 Ag17 C71 126.4(3) . . ?
C70 Ag17 C71 28.5(2) . . ?
O14 Ag17 C71 124.5(2) 2_565 . ?
C76 Ag17 Ag19 120.4(2) . . ?
C70 Ag17 Ag19 46.7(2) . . ?
O14 Ag17 Ag19 88.45(12) 2_565 . ?
C71 Ag17 Ag19 60.70(18) . . ?
C76 Ag17 Ag14 46.6(2) . . ?
C70 Ag17 Ag14 161.1(2) . . ?
O14 Ag17 Ag14 64.90(12) 2_565 . ?
C71 Ag17 Ag14 167.34(18) . . ?
Ag19 Ag17 Ag14 131.08(3) . . ?
C76 Ag17 Ag16 53.1(17) . . ?
C70 Ag17 Ag16 117(2) . . ?
O14 Ag17 Ag16 90.6(9) 2_565 . ?
C71 Ag17 Ag16 116(2) . . ?
Ag19 Ag17 Ag16 71(2) . . ?
Ag14 Ag17 Ag16 69(2) . . ?
C76 Ag17 A16 43.1(3) . . ?
C70 Ag17 A16 128.4(2) . . ?
O14 Ag17 A16 89.43(12) 2_565 . ?
C71 Ag17 A16 125.90(19) . . ?
Ag19 Ag17 A16 82.52(11) . . ?
Ag14 Ag17 A16 58.49(9) . . ?
C76 Ag17 Ag18 166.2(2) . . ?
C70 Ag17 Ag18 40.2(2) . . ?
O14 Ag17 Ag18 57.57(12) 2_565 . ?
C71 Ag17 Ag18 66.98(18) . . ?
Ag19 Ag17 Ag18 60.94(2) . . ?
Ag14 Ag17 Ag18 121.02(3) . . ?
Ag16 Ag17 Ag18 120.8(12) . . ?
A16 Ag17 Ag18 128.88(10) . . ?
C82 Ag18 C70 169.4(3) 2_565 . ?
C82 Ag18 Ag24 50.2(2) 2_565 . ?
C70 Ag18 Ag24 126.7(2) . . ?
C82 Ag18 Ag19 144.2(2) 2_565 . ?
C70 Ag18 Ag19 43.4(2) . . ?
Ag24 Ag18 Ag19 104.63(3) . . ?
C82 Ag18 Ag17 142.8(2) 2_565 . ?
C70 Ag18 Ag17 44.2(2) . . ?
Ag24 Ag18 Ag17 159.45(3) . . ?
Ag19 Ag18 Ag17 55.52(2) . . ?
C94 Ag19 C70 152.4(3) . . ?
C94 Ag19 Ag17 119.1(2) . . ?
C70 Ag19 Ag17 49.2(2) . . ?
C94 Ag19 Ag20 45.3(2) . . ?
C70 Ag19 Ag20 146.4(2) . . ?
Ag17 Ag19 Ag20 99.22(3) . . ?
C94 Ag19 Ag18 165.2(2) . . ?
C70 Ag19 Ag18 41.4(2) . . ?
Ag17 Ag19 Ag18 63.53(2) . . ?
Ag20 Ag19 Ag18 120.81(3) . . ?
C94 Ag19 Ag23 108.9(2) . . ?
C70 Ag19 Ag23 82.9(2) . . ?
Ag17 Ag19 Ag23 130.73(3) . . ?
Ag20 Ag19 Ag23 123.19(3) . . ?
Ag18 Ag19 Ag23 73.00(2) . . ?
C94 Ag20 C82 150.8(3) . . ?
C94 Ag20 O11 121.7(2) . 2_565 ?
C82 Ag20 O11 87.2(2) . 2_565 ?
C94 Ag20 C83 126.1(3) . . ?
C82 Ag20 C83 28.0(3) . . ?
O11 Ag20 C83 106.5(2) 2_565 . ?
C94 Ag20 Ag16 83(2) . . ?
C82 Ag20 Ag16 116.7(19) . . ?
O11 Ag20 Ag16 50.8(17) 2_565 . ?
C83 Ag20 Ag16 114.1(13) . . ?
C94 Ag20 Ag21 49.1(2) . . ?
C82 Ag20 Ag21 108.3(2) . . ?
O11 Ag20 Ag21 149.73(11) 2_565 . ?
C83 Ag20 Ag21 98.15(18) . . ?
Ag16 Ag20 Ag21 132(2) . . ?
C94 Ag20 Ag19 45.2(2) . . ?
C82 Ag20 Ag19 155.3(2) . . ?
O11 Ag20 Ag19 85.41(11) 2_565 . ?
C83 Ag20 Ag19 167.67(18) . . ?
Ag16 Ag20 Ag19 75.7(15) . . ?
Ag21 Ag20 Ag19 69.54(2) . . ?
C94 Ag20 Ag24 160.4(2) . 2_565 ?
C82 Ag20 Ag24 42.4(2) . 2_565 ?
O11 Ag20 Ag24 47.19(11) 2_565 2_565 ?
C83 Ag20 Ag24 59.52(19) . 2_565 ?
Ag16 Ag20 Ag24 78(2) . 2_565 ?
Ag21 Ag20 Ag24 149.71(3) . 2_565 ?
Ag19 Ag20 Ag24 132.04(3) . 2_565 ?
C94 Ag20 A16 90.2(2) . . ?
C82 Ag20 A16 110.1(2) . . ?
O11 Ag20 A16 45.52(11) 2_565 . ?
C83 Ag20 A16 109.64(17) . . ?
Ag21 Ag20 A16 139.28(4) . . ?
Ag19 Ag20 A16 80.78(4) . . ?
Ag24 Ag20 A16 70.86(4) 2_565 . ?
C88 Ag21 C94 164.1(3) . . ?
C88 Ag21 C95 146.6(3) . . ?
C94 Ag21 C95 27.4(3) . . ?
C88 Ag21 Ag20 123.6(2) . . ?
C94 Ag21 Ag20 47.2(2) . . ?
C95 Ag21 Ag20 70.34(18) . . ?
C88 Ag21 Ag13 49.7(2) . 2_565 ?
C94 Ag21 Ag13 145.2(2) . 2_565 ?
C95 Ag21 Ag13 150.39(18) . 2_565 ?
Ag20 Ag21 Ag13 126.89(3) . 2_565 ?
C88 Ag21 Ag22 42.1(2) . . ?
C94 Ag21 Ag22 131.6(2) . . ?
C95 Ag21 Ag22 149.03(18) . . ?
Ag20 Ag21 Ag22 84.39(2) . . ?
Ag13 Ag21 Ag22 60.25(2) 2_565 . ?
C88 Ag22 O17 149.4(3) . . ?
C88 Ag22 O14 106.7(2) . . ?
O17 Ag22 O14 100.5(2) . . ?
C88 Ag22 C89 29.5(3) . . ?
O17 Ag22 C89 127.2(2) . . ?
O14 Ag22 C89 132.2(2) . . ?
C88 Ag22 O18 119.2(2) . . ?
O17 Ag22 O18 75.7(2) . . ?
O14 Ag22 O18 86.19(19) . . ?
C89 Ag22 O18 101.5(2) . . ?
C88 Ag22 Ag13 45.4(2) . 2_565 ?
O17 Ag22 Ag13 163.87(16) . 2_565 ?
O14 Ag22 Ag13 70.81(12) . 2_565 ?
C89 Ag22 Ag13 62.15(18) . 2_565 ?
O18 Ag22 Ag13 89.92(13) . 2_565 ?
C88 Ag22 Ag21 38.7(2) . . ?
O17 Ag22 Ag21 139.52(14) . . ?
O14 Ag22 Ag21 78.89(11) . . ?
C89 Ag22 Ag21 67.12(18) . . ?
O18 Ag22 Ag21 143.55(13) . . ?
Ag13 Ag22 Ag21 53.808(19) 2_565 . ?
C58 Ag23 O19 127.6(3) . . ?
C58 Ag23 O12 104.6(2) . . ?
O19 Ag23 O12 127.8(2) . . ?
C58 Ag23 O20 119.8(2) . . ?
O19 Ag23 O20 75.9(2) . . ?
O12 Ag23 O20 79.59(18) . . ?
C58 Ag23 Ag15 44.4(2) . 2_565 ?
O19 Ag23 Ag15 146.36(16) . 2_565 ?
O12 Ag23 Ag15 72.83(12) . 2_565 ?
O20 Ag23 Ag15 83.99(14) . 2_565 ?
C58 Ag23 Ag19 135.30(19) . . ?
O19 Ag23 Ag19 84.51(15) . . ?
O12 Ag23 Ag19 52.99(12) . . ?
O20 Ag23 Ag19 95.66(14) . . ?
Ag15 Ag23 Ag19 124.61(3) 2_565 . ?
C58 Ag23 Ag24 41.42(19) . . ?
O19 Ag23 Ag24 144.02(16) . . ?
O12 Ag23 Ag24 75.50(12) . . ?
O20 Ag23 Ag24 139.77(13) . . ?
Ag15 Ag23 Ag24 58.77(2) 2_565 . ?
Ag19 Ag23 Ag24 93.98(3) . . ?
C58 Ag24 C82 152.5(3) . 2_565 ?
C58 Ag24 O11 108.0(2) . . ?
C82 Ag24 O11 91.8(2) 2_565 . ?
C58 Ag24 C59 28.7(3) . . ?
C82 Ag24 C59 126.4(3) 2_565 . ?
O11 Ag24 C59 135.8(2) . . ?
C58 Ag24 Ag18 112.1(2) . . ?
C82 Ag24 Ag18 46.6(2) 2_565 . ?
O11 Ag24 Ag18 92.04(11) . . ?
C59 Ag24 Ag18 99.1(2) . . ?
C58 Ag24 Ag15 42.3(2) . 2_565 ?
C82 Ag24 Ag15 158.8(2) 2_565 2_565 ?
O11 Ag24 Ag15 67.83(13) . 2_565 ?
C59 Ag24 Ag15 70.9(2) . 2_565 ?
Ag18 Ag24 Ag15 125.26(3) . 2_565 ?
C58 Ag24 Ag20 158.9(2) . 2_565 ?
C82 Ag24 Ag20 43.2(2) 2_565 2_565 ?
O11 Ag24 Ag20 51.10(13) . 2_565 ?
C59 Ag24 Ag20 168.6(2) . 2_565 ?
Ag18 Ag24 Ag20 70.26(2) . 2_565 ?
Ag15 Ag24 Ag20 118.23(3) 2_565 2_565 ?
C58 Ag24 Ag23 42.7(2) . . ?
C82 Ag24 Ag23 121.8(2) 2_565 . ?
O11 Ag24 Ag23 89.22(12) . . ?
C59 Ag24 Ag23 53.6(2) . . ?
Ag18 Ag24 Ag23 75.16(3) . . ?
Ag15 Ag24 Ag23 55.25(2) 2_565 . ?
Ag20 Ag24 Ag23 124.44(3) 2_565 . ?
C133 Ag25 O21 108.4(2) . . ?
C133 Ag25 O30 129.5(2) . . ?
O21 Ag25 O30 117.39(19) . . ?
C133 Ag25 O29 130.7(2) . . ?
O21 Ag25 O29 85.07(19) . . ?
O30 Ag25 O29 75.2(2) . . ?
C133 Ag25 C134 28.3(2) . . ?
O21 Ag25 C134 132.4(2) . . ?
O30 Ag25 C134 110.1(2) . . ?
O29 Ag25 C134 110.7(2) . . ?
C133 Ag25 Ag28 47.87(17) . . ?
O21 Ag25 Ag28 74.46(12) . . ?
O30 Ag25 Ag28 163.51(16) . . ?
O29 Ag25 Ag28 95.51(15) . . ?
C134 Ag25 Ag28 59.92(16) . . ?
C133 Ag25 Ag27 39.30(19) . . ?
O21 Ag25 Ag27 77.86(13) . . ?
O30 Ag25 Ag27 133.58(17) . . ?
O29 Ag25 Ag27 150.99(14) . . ?
C134 Ag25 Ag27 67.17(17) . . ?
Ag28 Ag25 Ag27 57.497(19) . . ?
C133 Ag25 Ag34 126.65(19) . 2_666 ?
O21 Ag25 Ag34 48.44(12) . 2_666 ?
O30 Ag25 Ag34 76.19(16) . 2_666 ?
O29 Ag25 Ag34 98.23(15) . 2_666 ?
C134 Ag25 Ag34 151.10(17) . 2_666 ?
Ag28 Ag25 Ag34 119.17(2) . 2_666 ?
Ag27 Ag25 Ag34 87.85(2) . 2_666 ?
C139 Ag26 C127 151.9(3) . . ?
C139 Ag26 O29 114.5(2) . . ?
C127 Ag26 O29 89.8(2) . . ?
C139 Ag26 Ag33 157.87(19) . 2_666 ?
C127 Ag26 Ag33 43.77(19) . 2_666 ?
O29 Ag26 Ag33 67.46(14) . 2_666 ?
C139 Ag26 Ag30 116.4(2) . . ?
C127 Ag26 Ag30 46.70(19) . . ?
O29 Ag26 Ag30 127.45(14) . . ?
Ag33 Ag26 Ag30 60.56(2) 2_666 . ?
C139 Ag26 Ag29 44.2(2) . . ?
C127 Ag26 Ag29 119.26(19) . . ?
O29 Ag26 Ag29 146.88(13) . . ?
Ag33 Ag26 Ag29 121.71(3) 2_666 . ?
Ag30 Ag26 Ag29 74.07(2) . . ?
C139 Ag26 Ag28 42.61(19) . . ?
C127 Ag26 Ag28 160.08(19) . . ?
O29 Ag26 Ag28 88.13(13) . . ?
Ag33 Ag26 Ag28 117.99(2) 2_666 . ?
Ag30 Ag26 Ag28 122.21(3) . . ?
Ag29 Ag26 Ag28 59.06(2) . . ?
C133 Ag27 C115 168.3(3) . 2_666 ?
C133 Ag27 Ag35 126.98(19) . 2_666 ?
C115 Ag27 Ag35 50.1(2) 2_666 2_666 ?
C133 Ag27 Ag28 47.88(19) . . ?
C115 Ag27 Ag28 143.61(19) 2_666 . ?
Ag35 Ag27 Ag28 133.29(3) 2_666 . ?
C133 Ag27 Ag25 43.67(19) . . ?
C115 Ag27 Ag25 138.4(2) 2_666 . ?
Ag35 Ag27 Ag25 89.09(2) 2_666 . ?
Ag28 Ag27 Ag25 56.978(19) . . ?
C139 Ag28 C133 146.8(3) . . ?
C139 Ag28 O27 116.3(2) . . ?
C133 Ag28 O27 92.3(2) . . ?
C139 Ag28 Ag25 109.23(19) . . ?
C133 Ag28 Ag25 48.62(18) . . ?
O27 Ag28 Ag25 133.74(12) . . ?
C139 Ag28 Ag27 161.09(19) . . ?
C133 Ag28 Ag27 43.51(19) . . ?
O27 Ag28 Ag27 68.69(12) . . ?
Ag25 Ag28 Ag27 65.53(2) . . ?
C139 Ag28 Ag29 44.3(2) . . ?
C133 Ag28 Ag29 162.96(18) . . ?
O27 Ag28 Ag29 87.05(12) . . ?
Ag25 Ag28 Ag29 122.60(3) . . ?
Ag27 Ag28 Ag29 121.53(3) . . ?
C139 Ag28 Ag26 42.44(18) . . ?
C133 Ag28 Ag26 118.31(18) . . ?
O27 Ag28 Ag26 145.91(12) . . ?
Ag25 Ag28 Ag26 70.57(2) . . ?
Ag27 Ag28 Ag26 122.93(2) . . ?
Ag29 Ag28 Ag26 59.22(2) . . ?
C139 Ag29 C145 151.2(3) . . ?
C139 Ag29 Ag32 160.01(18) . . ?
C145 Ag29 Ag32 43.48(19) . . ?
C139 Ag29 Ag31 114.4(2) . . ?
C145 Ag29 Ag31 47.52(18) . . ?
Ag32 Ag29 Ag31 64.48(2) . . ?
C139 Ag29 Ag28 44.22(19) . . ?
C145 Ag29 Ag28 119.14(19) . . ?
Ag32 Ag29 Ag28 124.00(3) . . ?
Ag31 Ag29 Ag28 72.67(2) . . ?
C139 Ag29 Ag26 43.95(19) . . ?
C145 Ag29 Ag26 160.98(18) . . ?
Ag32 Ag29 Ag26 118.62(3) . . ?
Ag31 Ag29 Ag26 124.90(3) . . ?
Ag28 Ag29 Ag26 61.72(2) . . ?
C127 Ag30 O24 107.2(3) . . ?
C127 Ag30 O25 135.6(2) . . ?
O24 Ag30 O25 116.2(2) . . ?
C127 Ag30 O26 121.7(2) . . ?
O24 Ag30 O26 82.0(2) . . ?
O25 Ag30 O26 75.3(2) . . ?
C127 Ag30 C128 27.7(2) . . ?
O24 Ag30 C128 128.1(3) . . ?
O25 Ag30 C128 114.9(2) . . ?
O26 Ag30 C128 102.8(2) . . ?
C127 Ag30 Ag33 42.40(19) . 2_666 ?
O24 Ag30 Ag33 79.35(15) . 2_666 ?
O25 Ag30 Ag33 137.20(14) . 2_666 ?
O26 Ag30 Ag33 147.40(14) . 2_666 ?
C128 Ag30 Ag33 69.47(17) . 2_666 ?
C127 Ag30 Ag26 45.82(19) . . ?
O24 Ag30 Ag26 70.0(2) . . ?
O25 Ag30 Ag26 162.85(13) . . ?
O26 Ag30 Ag26 90.47(14) . . ?
C128 Ag30 Ag26 58.39(18) . . ?
Ag33 Ag30 Ag26 58.056(19) 2_666 . ?
C127 Ag30 Ag35 142.39(19) . . ?
O24 Ag30 Ag35 62.4(2) . . ?
O25 Ag30 Ag35 60.78(14) . . ?
O26 Ag30 Ag35 93.75(15) . . ?
C128 Ag30 Ag35 161.27(17) . . ?
Ag33 Ag30 Ag35 100.86(2) 2_666 . ?
Ag26 Ag30 Ag35 131.02(3) . . ?
C145 Ag31 O28 134.1(2) . . ?
C145 Ag31 O22 108.2(2) . . ?
O28 Ag31 O22 116.3(2) . . ?
C145 Ag31 O27 123.3(2) . . ?
O28 Ag31 O27 74.87(19) . . ?
O22 Ag31 O27 82.20(17) . . ?
C145 Ag31 C146 27.6(2) . . ?
O28 Ag31 C146 112.5(2) . . ?
O22 Ag31 C146 130.8(2) . . ?
O27 Ag31 C146 105.7(2) . . ?
C145 Ag31 Ag29 46.14(18) . . ?
O28 Ag31 Ag29 160.10(14) . . ?
O22 Ag31 Ag29 72.98(13) . . ?
O27 Ag31 Ag29 89.86(13) . . ?
C146 Ag31 Ag29 58.82(18) . . ?
C145 Ag31 Ag36 132.36(18) . . ?
O28 Ag31 Ag36 75.72(15) . . ?
O22 Ag31 Ag36 49.30(13) . . ?
O27 Ag31 Ag36 97.32(12) . . ?
C146 Ag31 Ag36 156.86(17) . . ?
Ag29 Ag31 Ag36 119.65(2) . . ?
C145 Ag31 Ag32 39.50(18) . . ?
O28 Ag31 Ag32 139.24(14) . . ?
O22 Ag31 Ag32 80.14(12) . . ?
O27 Ag31 Ag32 145.90(13) . . ?
C146 Ag31 Ag32 66.45(17) . . ?
Ag29 Ag31 Ag32 57.109(19) . . ?
Ag36 Ag31 Ag32 92.93(2) . . ?
C145 Ag32 C121 163.6(3) . . ?
C145 Ag32 Ag34 127.1(2) . . ?
C121 Ag32 Ag34 50.2(2) . . ?
C145 Ag32 Ag29 47.1(2) . . ?
C121 Ag32 Ag29 149.1(2) . . ?
Ag34 Ag32 Ag29 129.67(3) . . ?
C145 Ag32 Ag31 43.86(19) . . ?
C121 Ag32 Ag31 136.8(2) . . ?
Ag34 Ag32 Ag31 86.60(2) . . ?
Ag29 Ag32 Ag31 58.41(2) . . ?
C127 Ag33 C151 166.2(3) 2_666 . ?
C127 Ag33 Ag36 126.1(2) 2_666 . ?
C151 Ag33 Ag36 49.5(2) . . ?
C127 Ag33 Ag26 47.9(2) 2_666 2_666 ?
C151 Ag33 Ag26 145.8(2) . 2_666 ?
Ag36 Ag33 Ag26 130.69(3) . 2_666 ?
C127 Ag33 Ag30 47.2(2) 2_666 2_666 ?
C151 Ag33 Ag30 132.3(2) . 2_666 ?
Ag36 Ag33 Ag30 82.84(2) . 2_666 ?
Ag26 Ag33 Ag30 61.38(2) 2_666 2_666 ?
C121 Ag34 C151 152.2(3) . . ?
C121 Ag34 O21 119.4(2) . 2_666 ?
C151 Ag34 O21 88.2(2) . 2_666 ?
C121 Ag34 C152 126.1(3) . . ?
C151 Ag34 C152 27.8(2) . . ?
O21 Ag34 C152 111.0(2) 2_666 . ?
C121 Ag34 Ag32 48.77(19) . . ?
C151 Ag34 Ag32 111.01(19) . . ?
O21 Ag34 Ag32 143.36(12) 2_666 . ?
C152 Ag34 Ag32 98.02(16) . . ?
C121 Ag34 Ag35 41.28(19) . . ?
C151 Ag34 Ag35 159.6(2) . . ?
O21 Ag34 Ag35 84.14(12) 2_666 . ?
C152 Ag34 Ag35 164.59(16) . . ?
Ag32 Ag34 Ag35 66.96(2) . . ?
C121 Ag34 Ag25 92.44(19) . 2_666 ?
C151 Ag34 Ag25 107.21(19) . 2_666 ?
O21 Ag34 Ag25 44.40(11) 2_666 2_666 ?
C152 Ag34 Ag25 112.33(17) . 2_666 ?
Ag32 Ag34 Ag25 140.85(3) . 2_666 ?
Ag35 Ag34 Ag25 80.10(2) . 2_666 ?
C115 Ag35 C121 164.8(3) . . ?
C115 Ag35 C122 139.9(3) . . ?
C121 Ag35 C122 27.0(2) . . ?
C115 Ag35 Ag27 49.46(19) . 2_666 ?
C121 Ag35 Ag27 117.38(19) . 2_666 ?
C122 Ag35 Ag27 104.07(16) . 2_666 ?
C115 Ag35 Ag30 84.8(2) . . ?
C121 Ag35 Ag30 109.44(19) . . ?
C122 Ag35 Ag30 120.87(16) . . ?
Ag27 Ag35 Ag30 132.82(3) 2_666 . ?
C115 Ag35 Ag34 138.18(19) . . ?
C121 Ag35 Ag34 40.9(2) . . ?
C122 Ag35 Ag34 61.81(17) . . ?
Ag27 Ag35 Ag34 97.05(2) 2_666 . ?
Ag30 Ag35 Ag34 115.50(2) . . ?
C151 Ag36 C115 153.9(3) . 2_666 ?
C151 Ag36 O22 113.3(2) . . ?
C115 Ag36 O22 92.0(2) 2_666 . ?
C151 Ag36 C116 126.0(3) . 2_666 ?
C115 Ag36 C116 28.8(2) 2_666 2_666 ?
O22 Ag36 C116 115.7(2) . 2_666 ?
C151 Ag36 Ag33 48.43(19) . . ?
C115 Ag36 Ag33 113.71(18) 2_666 . ?
O22 Ag36 Ag33 142.29(12) . . ?
C116 Ag36 Ag33 98.26(17) 2_666 . ?
C151 Ag36 Ag31 84.9(2) . . ?
C115 Ag36 Ag31 110.49(18) 2_666 . ?
O22 Ag36 Ag31 46.59(11) . . ?
C116 Ag36 Ag31 113.93(16) 2_666 . ?
Ag33 Ag36 Ag31 133.27(3) . . ?
C196 Ag37 O37 114.5(3) . . ?
C196 Ag37 O33 108.1(3) . . ?
O37 Ag37 O33 135.8(3) . . ?
C196 Ag37 O38 114.8(3) . . ?
O37 Ag37 O38 75.2(3) . . ?
O33 Ag37 O38 77.10(19) . . ?
C196 Ag37 Ag38 44.1(2) . . ?
O37 Ag37 Ag38 133.9(2) . . ?
O33 Ag37 Ag38 73.30(12) . . ?
O38 Ag37 Ag38 81.38(19) . . ?
C196 Ag37 Ag42 144.8(2) . 2_556 ?
O37 Ag37 Ag42 93.3(2) . 2_556 ?
O33 Ag37 Ag42 54.19(12) . 2_556 ?
O38 Ag37 Ag42 92.19(18) . 2_556 ?
Ag38 Ag37 Ag42 127.06(3) . 2_556 ?
C196 Ag37 Ag39 43.9(2) . . ?
O37 Ag37 Ag39 141.9(2) . . ?
O33 Ag37 Ag39 79.15(12) . . ?
O38 Ag37 Ag39 138.38(18) . . ?
Ag38 Ag37 Ag39 59.16(2) . . ?
Ag42 Ag37 Ag39 100.92(3) 2_556 . ?
C196 Ag38 C208 174.1(3) . . ?
C196 Ag38 A48 134.5(3) . . ?
C208 Ag38 A48 47.2(3) . . ?
C196 Ag38 Ag37 50.4(2) . . ?
C208 Ag38 Ag37 131.7(2) . . ?
A48 Ag38 Ag37 84.55(15) . . ?
C196 Ag38 Ag39 46.8(2) . . ?
C208 Ag38 Ag39 138.5(2) . . ?
A48 Ag38 Ag39 124.91(9) . . ?
Ag37 Ag38 Ag39 64.60(2) . . ?
C196 Ag38 Ag48 139.2(6) . . ?
C208 Ag38 Ag48 43.0(5) . . ?
Ag37 Ag38 Ag48 88.9(5) . . ?
Ag39 Ag38 Ag48 123.7(4) . . ?
C196 Ag38 Ag46 140.9(6) . . ?
C208 Ag38 Ag46 44.2(6) . . ?
Ag37 Ag38 Ag46 124.05(14) . . ?
Ag39 Ag38 Ag46 94.3(5) . . ?
Ag48 Ag38 Ag46 59.5(10) . . ?
C178 Ag39 C196 147.6(3) 2_556 . ?
C178 Ag39 O32 91.7(2) 2_556 . ?
C196 Ag39 O32 111.4(3) . . ?
C178 Ag39 O35 105.5(3) 2_556 . ?
C196 Ag39 O35 103.1(3) . . ?
O32 Ag39 O35 72.31(18) . . ?
C178 Ag39 C197 122.6(3) 2_556 . ?
C196 Ag39 C197 27.8(3) . . ?
O32 Ag39 C197 138.2(3) . . ?
O35 Ag39 C197 114.3(3) . . ?
C178 Ag39 Ag44 47.0(2) 2_556 2_556 ?
C196 Ag39 Ag44 108.9(2) . 2_556 ?
O32 Ag39 Ag44 88.79(12) . 2_556 ?
O35 Ag39 Ag44 147.09(19) . 2_556 ?
C197 Ag39 Ag44 97.87(19) . 2_556 ?
C178 Ag39 Ag38 161.1(2) 2_556 . ?
C196 Ag39 Ag38 42.5(2) . . ?
O32 Ag39 Ag38 71.38(13) . . ?
O35 Ag39 Ag38 78.02(19) . . ?
C197 Ag39 Ag38 70.1(2) . . ?
Ag44 Ag39 Ag38 121.90(3) 2_556 . ?
C178 Ag39 Ag37 116.7(2) 2_556 . ?
C196 Ag39 Ag37 45.3(2) . . ?
O32 Ag39 Ag37 88.64(12) . . ?
O35 Ag39 Ag37 134.13(19) . . ?
C197 Ag39 Ag37 56.3(2) . . ?
Ag44 Ag39 Ag37 69.72(3) 2_556 . ?
Ag38 Ag39 Ag37 56.24(3) . . ?
C178 Ag39 Ag40 42.6(2) 2_556 . ?
C196 Ag39 Ag40 161.0(2) . . ?
O32 Ag39 Ag40 51.24(13) . . ?
O35 Ag39 Ag40 80.08(19) . . ?
C197 Ag39 Ag40 163.81(19) . . ?
Ag44 Ag39 Ag40 67.16(2) 2_556 . ?
Ag38 Ag39 Ag40 122.38(3) . . ?
Ag37 Ag39 Ag40 119.77(3) . . ?
C202 Ag40 C178 157.2(3) . 2_556 ?
C202 Ag40 C179 129.5(3) . 2_556 ?
C178 Ag40 C179 28.8(3) 2_556 2_556 ?
C202 Ag40 Ag41 71.8(3) . . ?
C178 Ag40 Ag41 120.9(2) 2_556 . ?
C179 Ag40 Ag41 119.52(19) 2_556 . ?
C202 Ag40 Ag47 48.7(2) . 2_556 ?
C178 Ag40 Ag47 117.9(2) 2_556 2_556 ?
C179 Ag40 Ag47 105.82(17) 2_556 2_556 ?
Ag41 Ag40 Ag47 119.92(15) . 2_556 ?
C202 Ag40 Ag42 42.4(3) . . ?
C178 Ag40 Ag42 157.4(2) 2_556 . ?
C179 Ag40 Ag42 170.08(18) 2_556 . ?
Ag41 Ag40 Ag42 66.13(12) . . ?
Ag47 Ag40 Ag42 64.70(2) 2_556 . ?
C202 Ag40 Ag39 154.6(2) . . ?
C178 Ag40 Ag39 42.0(2) 2_556 . ?
C179 Ag40 Ag39 61.94(18) 2_556 . ?
Ag41 Ag40 Ag39 82.89(15) . . ?
Ag47 Ag40 Ag39 156.62(3) 2_556 . ?
Ag42 Ag40 Ag39 127.93(3) . . ?
O36 Ag41 O32 132.3(3) . . ?
O36 Ag41 C190 112.1(3) . . ?
O32 Ag41 C190 97.4(3) . . ?
O36 Ag41 Ag40 97.1(2) . . ?
O32 Ag41 Ag40 60.60(15) . . ?
C190 Ag41 Ag40 150.8(2) . . ?
O36 Ag41 Ag43 146.6(2) . . ?
O32 Ag41 Ag43 79.64(14) . . ?
C190 Ag41 Ag43 43.49(19) . . ?
Ag40 Ag41 Ag43 109.66(17) . . ?
O36 Ag41 Ag46 125.2(5) . . ?
O32 Ag41 Ag46 60.0(3) . . ?
C190 Ag41 Ag46 40.8(5) . . ?
Ag40 Ag41 Ag46 120.5(2) . . ?
Ag43 Ag41 Ag46 56.4(6) . . ?
O36 Ag41 Ag42 128.5(4) . . ?
O32 Ag41 Ag42 81.66(19) . . ?
C190 Ag41 Ag42 96.1(2) . . ?
Ag40 Ag41 Ag42 63.77(15) . . ?
Ag43 Ag41 Ag42 54.43(8) . . ?
Ag46 Ag41 Ag42 104.5(5) . . ?
C190 A41A O35 142.4(4) . . ?
C190 A41A O32 108.9(3) . . ?
O35 A41A O32 78.7(2) . . ?
C190 A41A O36 120.8(3) . . ?
O35 A41A O36 75.4(3) . . ?
O32 A41A O36 125.6(2) . . ?
C190 A41A C191 27.3(3) . . ?
O35 A41A C191 130.8(3) . . ?
O32 A41A C191 136.1(2) . . ?
O36 A41A C191 96.0(3) . . ?
C190 A41A A46A 47.1(3) . . ?
O35 A41A A46A 105.9(2) . . ?
O32 A41A A46A 72.99(15) . . ?
O36 A41A A46A 160.5(2) . . ?
C191 A41A A46A 68.0(2) . . ?
C190 A41A Ag43 40.9(2) . . ?
O35 A41A Ag43 152.33(18) . . ?
O32 A41A Ag43 76.64(13) . . ?
O36 A41A Ag43 129.9(2) . . ?
C191 A41A Ag43 64.78(18) . . ?
A46A A41A Ag43 54.68(8) . . ?
C202 Ag42 C184 155.9(3) . . ?
C202 Ag42 C23A 27.0(5) . . ?
C184 Ag42 C23A 131.3(6) . . ?
C202 Ag42 O33 90.4(2) . 2_556 ?
C184 Ag42 O33 111.2(2) . 2_556 ?
C23A Ag42 O33 103.3(6) . 2_556 ?
C202 Ag42 Ag43 118.7(2) . . ?
C184 Ag42 Ag43 50.7(2) . . ?
C23A Ag42 Ag43 116.1(6) . . ?
O33 Ag42 Ag43 138.33(11) 2_556 . ?
C202 Ag42 Ag37 113.8(2) . 2_556 ?
C184 Ag42 Ag37 76.6(2) . 2_556 ?
C23A Ag42 Ag37 105.5(7) . 2_556 ?
O33 Ag42 Ag37 47.44(11) 2_556 2_556 ?
Ag43 Ag42 Ag37 126.32(3) . 2_556 ?
C202 Ag42 Ag40 40.7(3) . . ?
C184 Ag42 Ag40 150.6(2) . . ?
C23A Ag42 Ag40 67.2(5) . . ?
O33 Ag42 Ag40 79.76(11) 2_556 . ?
Ag43 Ag42 Ag40 102.56(3) . . ?
Ag37 Ag42 Ag40 124.78(3) 2_556 . ?
C202 Ag42 Ag44 163.6(2) . . ?
C184 Ag42 Ag44 39.9(2) . . ?
C23A Ag42 Ag44 168.1(6) . . ?
O33 Ag42 Ag44 78.17(11) 2_556 . ?
Ag43 Ag42 Ag44 66.25(2) . . ?
Ag37 Ag42 Ag44 66.55(3) 2_556 . ?
Ag40 Ag42 Ag44 124.50(3) . . ?
C202 Ag42 Ag41 60.2(2) . . ?
C184 Ag42 Ag41 109.5(2) . . ?
O33 Ag42 Ag41 128.74(12) 2_556 . ?
Ag43 Ag42 Ag41 59.85(9) . . ?
Ag37 Ag42 Ag41 173.83(9) 2_556 . ?
Ag40 Ag42 Ag41 50.10(6) . . ?
Ag44 Ag42 Ag41 118.71(10) . . ?
C202 Ag42 Ag47 42.0(2) . 2_556 ?
C184 Ag42 Ag47 152.8(2) . 2_556 ?
C23A Ag42 Ag47 54.8(6) . 2_556 ?
O33 Ag42 Ag47 49.71(11) 2_556 2_556 ?
Ag43 Ag42 Ag47 156.33(3) . 2_556 ?
Ag37 Ag42 Ag47 76.44(3) 2_556 2_556 ?
Ag40 Ag42 Ag47 54.14(2) . 2_556 ?
Ag44 Ag42 Ag47 127.88(3) . 2_556 ?
Ag41 Ag42 Ag47 97.43(9) . 2_556 ?
C190 Ag43 C184 150.6(3) . . ?
C190 Ag43 O31 108.9(3) . . ?
C184 Ag43 O31 96.4(3) . . ?
C190 Ag43 C185 127.0(3) . . ?
C184 Ag43 C185 27.8(3) . . ?
O31 Ag43 C185 123.5(3) . . ?
C190 Ag43 A46A 50.0(3) . . ?
C184 Ag43 A46A 158.8(2) . . ?
O31 Ag43 A46A 63.1(2) . . ?
C185 Ag43 A46A 167.6(2) . . ?
C190 Ag43 Ag42 117.0(3) . . ?
C184 Ag43 Ag42 48.0(2) . . ?
O31 Ag43 Ag42 87.38(17) . . ?
C185 Ag43 Ag42 62.2(2) . . ?
A46A Ag43 Ag42 130.15(11) . . ?
C190 Ag43 Ag46 45.0(3) . . ?
C184 Ag43 Ag46 160.2(3) . . ?
O31 Ag43 Ag46 64.7(2) . . ?
C185 Ag43 Ag46 171.8(2) . . ?
Ag42 Ag43 Ag46 121.0(7) . . ?
C190 Ag43 Ag41 54.0(3) . . ?
C184 Ag43 Ag41 112.5(3) . . ?
O31 Ag43 Ag41 90.96(14) . . ?
C185 Ag43 Ag41 113.7(3) . . ?
Ag42 Ag43 Ag41 65.72(15) . . ?
Ag46 Ag43 Ag41 64.2(8) . . ?
C190 Ag43 A41A 41.2(2) . . ?
C184 Ag43 A41A 129.0(2) . . ?
O31 Ag43 A41A 87.53(14) . . ?
C185 Ag43 A41A 128.3(2) . . ?
A46A Ag43 A41A 59.28(16) . . ?
Ag42 Ag43 A41A 81.72(7) . . ?
C190 Ag43 Ag44 168.7(2) . . ?
C184 Ag43 Ag44 37.7(2) . . ?
O31 Ag43 Ag44 60.33(17) . . ?
C185 Ag43 Ag44 63.3(2) . . ?
A46A Ag43 Ag44 121.19(11) . . ?
Ag42 Ag43 Ag44 61.45(2) . . ?
Ag46 Ag43 Ag44 124.87(19) . . ?
Ag41 Ag43 Ag44 119.62(12) . . ?
A41A Ag43 Ag44 130.20(4) . . ?
C184 Ag44 C178 169.6(3) . . ?
C184 Ag44 Ag39 128.6(2) . 2_556 ?
C178 Ag44 Ag39 50.3(2) . 2_556 ?
C184 Ag44 Ag45 108.7(6) . . ?
C178 Ag44 Ag45 74.4(6) . . ?
Ag39 Ag44 Ag45 122.6(6) 2_556 . ?
C184 Ag44 Ag42 42.1(2) . . ?
C178 Ag44 Ag42 146.7(2) . . ?
Ag39 Ag44 Ag42 106.87(3) 2_556 . ?
Ag45 Ag44 Ag42 113.2(4) . . ?
C184 Ag44 Ag43 41.7(2) . . ?
C178 Ag44 Ag43 143.8(2) . . ?
Ag39 Ag44 Ag43 158.51(3) 2_556 . ?
Ag45 Ag44 Ag43 69.7(5) . . ?
Ag42 Ag44 Ag43 52.297(19) . . ?
O40 Ag45 O31 110.2(8) . . ?
O40 Ag45 C172 141.5(13) . . ?
O31 Ag45 C172 105.6(9) . . ?
O40 Ag45 Ag47 153.6(18) . . ?
O31 Ag45 Ag47 83.8(4) . . ?
C172 Ag45 Ag47 43.0(2) . . ?
O40 Ag45 Ag48 147(2) . . ?
O31 Ag45 Ag48 69.3(8) . . ?
C172 Ag45 Ag48 41.9(7) . . ?
Ag47 Ag45 Ag48 58.5(7) . . ?
O40 Ag45 Ag44 61.1(10) . . ?
O31 Ag45 Ag44 64.7(10) . . ?
C172 Ag45 Ag44 152.4(14) . . ?
Ag47 Ag45 Ag44 109.4(13) . . ?
Ag48 Ag45 Ag44 133.6(5) . . ?
C172 A45A O40 147.7(4) . . ?
C172 A45A O31 111.2(3) . . ?
O40 A45A O31 96.7(4) . . ?
C172 A45A O39 122.4(5) . . ?
O40 A45A O39 75.8(3) . . ?
O31 A45A O39 82.4(3) . . ?
C172 A45A C173 27.5(3) . . ?
O40 A45A C173 128.1(3) . . ?
O31 A45A C173 135.1(4) . . ?
O39 A45A C173 106.2(4) . . ?
C172 A45A A48 47.0(3) . . ?
O40 A45A A48 164.6(3) . . ?
O31 A45A A48 73.6(2) . . ?
O39 A45A A48 90.9(3) . . ?
C173 A45A A48 62.5(3) . . ?
C172 A45A Ag47 42.5(2) . . ?
O40 A45A Ag47 134.1(3) . . ?
O31 A45A Ag47 80.38(17) . . ?
O39 A45A Ag47 146.9(3) . . ?
C173 A45A Ag47 68.7(2) . . ?
A48 A45A Ag47 57.22(17) . . ?
C190 Ag46 C208 162.5(6) . . ?
C190 Ag46 C209 135.0(4) . . ?
C208 Ag46 C209 27.8(3) . . ?
C190 Ag46 Ag43 45.9(3) . . ?
C208 Ag46 Ag43 146.5(12) . . ?
C209 Ag46 Ag43 158.5(17) . . ?
C190 Ag46 Ag48 146.7(17) . . ?
C208 Ag46 Ag48 43.0(8) . . ?
C209 Ag46 Ag48 67.0(7) . . ?
Ag43 Ag46 Ag48 103.6(11) . . ?
C190 Ag46 Ag41 51.3(6) . . ?
C208 Ag46 Ag41 139.7(15) . . ?
C209 Ag46 Ag41 141.3(15) . . ?
Ag43 Ag46 Ag41 59.5(3) . . ?
Ag48 Ag46 Ag41 132.6(5) . . ?
C190 Ag46 Ag38 148.6(18) . . ?
C208 Ag46 Ag38 40.8(5) . . ?
C209 Ag46 Ag38 59.2(4) . . ?
Ag43 Ag46 Ag38 134.2(4) . . ?
Ag48 Ag46 Ag38 59.1(10) . . ?
Ag41 Ag46 Ag38 99.3(10) . . ?
C190 A46A C208 149.0(5) . . ?
C190 A46A C209 128.2(4) . . ?
C208 A46A C209 27.8(3) . . ?
C190 A46A Ag43 47.3(2) . . ?
C208 A46A Ag43 155.7(3) . . ?
C209 A46A Ag43 175.5(4) . . ?
C190 A46A A41A 45.0(3) . . ?
C208 A46A A41A 112.6(3) . . ?
C209 A46A A41A 110.8(3) . . ?
Ag43 A46A A41A 66.04(13) . . ?
C190 A46A A48 160.6(3) . . ?
C208 A46A A48 42.5(3) . . ?
C209 A46A A48 68.0(2) . . ?
Ag43 A46A A48 116.25(18) . . ?
A41A A46A A48 123.9(2) . . ?
C172 Ag47 C202 157.8(3) . 2_556 ?
C172 Ag47 C203 138.1(4) . 2_556 ?
C202 Ag47 C203 30.2(4) 2_556 2_556 ?
C172 Ag47 O33 108.2(3) . . ?
C202 Ag47 O33 89.8(3) 2_556 . ?
C203 Ag47 O33 113.2(3) 2_556 . ?
C172 Ag47 A48 48.8(3) . . ?
C202 Ag47 A48 152.2(3) 2_556 . ?
O33 Ag47 A48 62.88(16) . . ?
C172 Ag47 Ag40 121.8(3) . 2_556 ?
C202 Ag47 Ag40 45.1(2) 2_556 2_556 ?
C203 Ag47 Ag40 68.8(3) 2_556 2_556 ?
O33 Ag47 Ag40 84.95(11) . 2_556 ?
A48 Ag47 Ag40 130.07(10) . 2_556 ?
C172 Ag47 Ag48 43.3(7) . . ?
C202 Ag47 Ag48 155.7(4) 2_556 . ?
C203 Ag47 Ag48 164.9(10) 2_556 . ?
O33 Ag47 Ag48 66.2(5) . . ?
Ag40 Ag47 Ag48 125.1(8) 2_556 . ?
C172 Ag47 Ag45 52.8(9) . . ?
C202 Ag47 Ag45 117.6(10) 2_556 . ?
C203 Ag47 Ag45 133.9(9) 2_556 . ?
O33 Ag47 Ag45 86.9(2) . . ?
Ag40 Ag47 Ag45 72.6(10) 2_556 . ?
Ag48 Ag47 Ag45 60.8(14) . . ?
C172 Ag47 A45A 43.1(3) . . ?
C202 Ag47 A45A 128.0(3) 2_556 . ?
O33 Ag47 A45A 87.96(14) . . ?
A48 Ag47 A45A 60.2(2) . . ?
Ag40 Ag47 A45A 83.02(16) 2_556 . ?
C172 Ag47 Ag42 158.6(2) . 2_556 ?
C202 Ag47 Ag42 40.7(2) 2_556 2_556 ?
C203 Ag47 Ag42 63.3(3) 2_556 2_556 ?
O33 Ag47 Ag42 50.39(11) . 2_556 ?
A48 Ag47 Ag42 111.46(14) . 2_556 ?
Ag40 Ag47 Ag42 61.16(2) 2_556 2_556 ?
Ag48 Ag47 Ag42 116.1(5) . 2_556 ?
Ag45 Ag47 Ag42 116.8(7) . 2_556 ?
A45A Ag47 Ag42 124.20(14) . 2_556 ?
C172 Ag48 C208 166.7(11) . . ?
C172 Ag48 C173 24.1(5) . . ?
C208 Ag48 C173 142.8(10) . . ?
C172 Ag48 Ag47 44.5(4) . . ?
C208 Ag48 Ag47 147.8(17) . . ?
C173 Ag48 Ag47 68.5(4) . . ?
C172 Ag48 Ag45 52.8(10) . . ?
C208 Ag48 Ag45 131.9(17) . . ?
C173 Ag48 Ag45 61.1(10) . . ?
Ag47 Ag48 Ag45 60.6(8) . . ?
C172 Ag48 Ag38 148.4(18) . . ?
C208 Ag48 Ag38 41.9(8) . . ?
C173 Ag48 Ag38 163.7(19) . . ?
Ag47 Ag48 Ag38 106.1(12) . . ?
Ag45 Ag48 Ag38 130.9(8) . . ?
C172 Ag48 Ag46 140(2) . . ?
C208 Ag48 Ag46 45.4(6) . . ?
C173 Ag48 Ag46 135(2) . . ?
Ag47 Ag48 Ag46 125.3(7) . . ?
Ag45 Ag48 Ag46 87.3(12) . . ?
Ag38 Ag48 Ag46 61.3(7) . . ?
C208 A48 C172 150.5(6) . . ?
C208 A48 Ag38 47.3(3) . . ?
C172 A48 Ag38 161.1(4) . . ?
C208 A48 Ag47 158.1(3) . . ?
C172 A48 Ag47 45.5(2) . . ?
Ag38 A48 Ag47 115.6(3) . . ?
C208 A48 A45A 116.7(4) . . ?
C172 A48 A45A 44.5(3) . . ?
Ag38 A48 A45A 133.85(19) . . ?
Ag47 A48 A45A 62.56(13) . . ?
C208 A48 A46A 45.8(3) . . ?
C172 A48 A46A 116.2(4) . . ?
Ag38 A48 A46A 71.37(15) . . ?
Ag47 A48 A46A 121.76(16) . . ?
A45A A48 A46A 73.1(2) . . ?
O3 V1 O2 110.0(4) . . ?
O3 V1 O1 109.8(3) . . ?
O2 V1 O1 111.7(3) . . ?
O3 V1 O4 124.4(5) . . ?
O2 V1 O4 96.1(5) . . ?
O1 V1 O4 104.2(5) . . ?
O3 V1 O4 92.3(5) . 2_675 ?
O2 V1 O4 119.3(5) . 2_675 ?
O1 V1 O4 112.0(5) . 2_675 ?
O4 V1 O4 33.4(6) . 2_675 ?
O14 V2 O12 109.6(2) . . ?
O14 V2 O11 109.2(2) . . ?
O12 V2 O11 111.0(2) . . ?
O14 V2 O13 109.70(18) . . ?
O12 V2 O13 108.96(18) . . ?
O11 V2 O13 108.35(19) . . ?
O24 V3 O22 109.9(3) . . ?
O24 V3 O21 110.5(3) . . ?
O22 V3 O21 111.1(2) . . ?
O24 V3 O23 91.2(5) . . ?
O22 V3 O23 114.4(5) . . ?
O21 V3 O23 117.9(5) . . ?
O24 V3 O23 123.8(5) . 2_666 ?
O22 V3 O23 102.0(5) . 2_666 ?
O21 V3 O23 98.8(4) . 2_666 ?
O23 V3 O23 32.8(6) . 2_666 ?
O31 V4 O32 108.7(3) . . ?
O31 V4 O33 109.8(3) . . ?
O32 V4 O33 110.7(3) . . ?
O31 V4 O34 109.2(3) . . ?
O32 V4 O34 109.9(2) . . ?
O33 V4 O34 108.49(18) . . ?
V1 O1 Ag10 127.7(3) . . ?
V1 O1 Ag7 115.1(2) . . ?
Ag10 O1 Ag7 117.1(2) . . ?
V1 O2 Ag3B 141.5(4) . . ?
V1 O2 Ag3A 130.7(4) . . ?
V1 O3 Ag8 133.2(3) . . ?
V1 O3 Ag4B 113.8(4) . . ?
Ag8 O3 Ag4B 107.2(3) . . ?
O4 O4 V1 74.5(12) 2_675 . ?
O4 O4 V1 72.2(12) 2_675 2_675 ?
V1 O4 V1 146.6(6) . 2_675 ?
C51 O5 Ag3B 124.4(7) . . ?
C51 O5 Ag1 129.5(7) . 2_675 ?
Ag3B O5 Ag1 105.5(3) . 2_675 ?
C49 O6 Ag3A 140.2(8) . . ?
C49 O6 Ag3B 122.3(7) . . ?
C54 O7 Ag10 126.9(7) . . ?
C56 O8 Ag9 134.5(6) . . ?
C56 O8 Ag10 121.6(6) . . ?
Ag9 O8 Ag10 101.03(19) . . ?
C44 O9 Ag8 125.3(7) . . ?
C46 O10 Ag8 124.5(6) . . ?
C46 O10 Ag4B 132.4(7) . . ?
Ag8 O10 Ag4B 102.9(3) . . ?
V2 O11 Ag16 135.8(15) . 2_565 ?
V2 O11 A16 139.0(3) . 2_565 ?
V2 O11 Ag24 115.3(2) . . ?
Ag16 O11 Ag24 107.7(9) 2_565 . ?
A16 O11 Ag24 105.21(18) 2_565 . ?
V2 O11 Ag20 107.5(2) . 2_565 ?
Ag16 O11 Ag20 68(3) 2_565 2_565 ?
A16 O11 Ag20 83.5(2) 2_565 2_565 ?
Ag24 O11 Ag20 81.71(16) . 2_565 ?
V2 O12 Ag23 138.1(3) . . ?
V2 O13 V2 180.0 . 2_565 ?
V2 O14 Ag22 140.8(3) . . ?
V2 O14 Ag17 115.3(2) . 2_565 ?
Ag22 O14 Ag17 103.52(18) . 2_565 ?
C106 O15 A16 118.8(6) . . ?
C108 O16 Ag16 137(3) . . ?
C108 O16 A16 120.7(6) . . ?
C111 O17 Ag22 130.0(5) . . ?
C113 O18 Ag22 124.1(6) . . ?
C101 O19 Ag23 125.3(6) . . ?
C103 O20 Ag23 123.4(5) . . ?
V3 O21 Ag25 140.3(3) . . ?
V3 O21 Ag34 111.8(2) . 2_666 ?
Ag25 O21 Ag34 87.16(16) . 2_666 ?
V3 O22 Ag31 138.3(3) . . ?
V3 O22 Ag36 111.1(2) . . ?
Ag31 O22 Ag36 84.12(16) . . ?
O23 O23 V3 77.3(12) 2_666 . ?
O23 O23 V3 69.9(12) 2_666 2_666 ?
V3 O23 V3 147.2(6) . 2_666 ?
V3 O24 Ag30 140.6(4) . . ?
C168 O25 Ag30 126.2(5) . . ?
C170 O26 Ag30 124.3(5) . . ?
C158 O27 Ag31 123.3(5) . . ?
C158 O27 Ag28 140.2(5) . . ?
Ag31 O27 Ag28 93.89(17) . . ?
C160 O28 Ag31 125.9(5) . . ?
C165 O29 Ag25 126.6(5) . . ?
C165 O29 Ag26 139.2(6) . . ?
Ag25 O29 Ag26 92.21(19) . . ?
C163 O30 Ag25 126.9(6) . . ?
V4 O31 Ag45 134.5(6) . . ?
V4 O31 A45A 135.7(3) . . ?
V4 O31 Ag43 117.0(3) . . ?
Ag45 O31 Ag43 107.7(4) . . ?
A45A O31 Ag43 107.1(2) . . ?
V4 O32 A41A 137.5(3) . . ?
V4 O32 Ag41 130.4(3) . . ?
V4 O32 Ag39 117.3(2) . . ?
A41A O32 Ag39 104.38(19) . . ?
Ag41 O32 Ag39 110.5(2) . . ?
V4 O33 Ag37 136.3(3) . . ?
V4 O33 Ag47 115.4(2) . . ?
Ag37 O33 Ag47 108.24(18) . . ?
V4 O33 Ag42 108.9(2) . 2_556 ?
Ag37 O33 Ag42 78.37(14) . 2_556 ?
Ag47 O33 Ag42 79.90(14) . 2_556 ?
V4 O34 V4 180.00(7) . 2_556 ?
C222 O35 A41A 121.9(6) . . ?
C222 O35 Ag39 132.2(6) . . ?
A41A O35 Ag39 103.3(2) . . ?
C220 O36 Ag41 141.7(8) . . ?
C220 O36 A41A 120.6(8) . . ?
C217 O37 Ag37 127.4(7) . . ?
C215 O38 Ag37 125.0(6) . . ?
C227 O39 A45A 124.7(7) . . ?
C225 O40 Ag45 138.3(15) . . ?
C225 O40 A45A 125.7(6) . . ?
C2 C1 Ag6 152.8(9) . 2_675 ?
C2 C1 Ag4A 123.0(9) . . ?
Ag6 C1 Ag4A 79.5(5) 2_675 . ?
C2 C1 Ag2 84.4(8) . . ?
Ag6 C1 Ag2 106.4(4) 2_675 . ?
Ag4A C1 Ag2 103.8(7) . . ?
C2 C1 Ag4B 120.3(8) . . ?
Ag6 C1 Ag4B 83.4(4) 2_675 . ?
Ag2 C1 Ag4B 98.5(4) . . ?
C1 C2 C3 172.7(12) . . ?
C1 C2 Ag2 66.7(7) . . ?
C3 C2 Ag2 120.6(8) . . ?
C5 C3 C6 109.8(13) . . ?
C5 C3 C2 109.6(9) . . ?
C6 C3 C2 104.7(11) . . ?
C5 C3 C4 109.2(13) . . ?
C6 C3 C4 115.0(12) . . ?
C2 C3 C4 108.4(11) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 Ag2 144.6(9) . . ?
C8 C7 Ag12 90.8(7) . . ?
Ag2 C7 Ag12 94.8(4) . . ?
C8 C7 Ag1 133.7(9) . . ?
Ag2 C7 Ag1 80.6(3) . . ?
Ag12 C7 Ag1 95.2(4) . . ?
C7 C8 C9 174.3(11) . . ?
C7 C8 Ag12 61.2(6) . . ?
C9 C8 Ag12 124.5(7) . . ?
C12 C9 C11 118.4(15) . . ?
C12 C9 C8 111.3(9) . . ?
C11 C9 C8 110.8(9) . . ?
C12 C9 C10 104.6(14) . . ?
C11 C9 C10 104.8(12) . . ?
C8 C9 C10 105.6(12) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag12 153.6(8) . . ?
C14 C13 Ag6 108.2(7) . . ?
Ag12 C13 Ag6 98.0(4) . . ?
C14 C13 Ag7 93.7(7) . . ?
Ag12 C13 Ag7 84.7(3) . . ?
Ag6 C13 Ag7 99.2(3) . . ?
C13 C14 C15 174.0(10) . . ?
C13 C14 Ag7 59.1(5) . . ?
C15 C14 Ag7 126.7(7) . . ?
C16 C15 C14 108.6(13) . . ?
C16 C15 C18 111.6(13) . . ?
C14 C15 C18 110.1(9) . . ?
C16 C15 C17 114.6(15) . . ?
C14 C15 C17 106.7(11) . . ?
C18 C15 C17 105.2(14) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 Ag4A 158.0(9) . . ?
C20 C19 Ag4B 159.5(9) . . ?
C20 C19 Ag5 104.4(7) . . ?
Ag4A C19 Ag5 92.8(7) . . ?
Ag4B C19 Ag5 87.3(4) . . ?
C20 C19 Ag3B 103.5(8) . . ?
Ag4B C19 Ag3B 94.5(5) . . ?
Ag5 C19 Ag3B 82.7(4) . . ?
C20 C19 Ag3A 112.4(8) . . ?
Ag4A C19 Ag3A 78.6(6) . . ?
Ag5 C19 Ag3A 95.8(5) . . ?
C19 C20 C21 175.3(11) . . ?
C23 C21 C20 109.8(11) . . ?
C23 C21 C22 115.0(14) . . ?
C20 C21 C22 110.2(10) . . ?
C23 C21 C24 109.1(16) . . ?
C20 C21 C24 106.4(10) . . ?
C22 C21 C24 105.9(13) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C26 C25 Ag1 148.0(7) . 2_675 ?
C26 C25 Ag11 113.8(6) . . ?
Ag1 C25 Ag11 89.2(3) 2_675 . ?
C26 C25 Ag10 117.6(7) . . ?
Ag1 C25 Ag10 84.2(3) 2_675 . ?
Ag11 C25 Ag10 86.6(3) . . ?
C25 C26 C27 176.9(10) . . ?
C30 C27 C26 110.1(9) . . ?
C30 C27 C29 108.6(13) . . ?
C26 C27 C29 109.6(8) . . ?
C30 C27 C28 112.2(13) . . ?
C26 C27 C28 109.7(8) . . ?
C29 C27 C28 106.5(12) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
C27 C29 H29A 109.5 . . ?
C27 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C27 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C27 C30 H30A 109.5 . . ?
C27 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
C27 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C32 C31 Ag7 122.5(7) . . ?
C32 C31 Ag9 129.6(7) . . ?
Ag7 C31 Ag9 85.3(3) . . ?
C32 C31 Ag8 133.3(7) . . ?
Ag7 C31 Ag8 90.0(3) . . ?
Ag9 C31 Ag8 80.7(3) . . ?
C31 C32 C33 178.8(9) . . ?
C32 C33 C36 109.6(8) . . ?
C32 C33 C35 109.1(8) . . ?
C36 C33 C35 109.8(10) . . ?
C32 C33 C34 108.9(8) . . ?
C36 C33 C34 108.3(9) . . ?
C35 C33 C34 111.1(10) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 Ag11 168.2(8) . . ?
C38 C37 Ag5 95.3(6) . . ?
Ag11 C37 Ag5 96.3(3) . . ?
C38 C37 Ag9 92.6(6) . . ?
Ag11 C37 Ag9 87.1(3) . . ?
Ag5 C37 Ag9 101.4(3) . . ?
C37 C38 C39 172.0(10) . . ?
C37 C38 Ag5 56.8(5) . . ?
C39 C38 Ag5 129.3(6) . . ?
C37 C38 Ag9 60.0(5) . . ?
C39 C38 Ag9 123.4(6) . . ?
Ag5 C38 Ag9 82.7(2) . . ?
C38 C39 C42 110.4(8) . . ?
C38 C39 C41 108.2(8) . . ?
C42 C39 C41 110.0(9) . . ?
C38 C39 C40 108.3(8) . . ?
C42 C39 C40 110.6(9) . . ?
C41 C39 C40 109.3(9) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
F17 C43 F16 108.5(13) . . ?
F17 C43 F18 106.2(14) . . ?
F16 C43 F18 105.5(15) . . ?
F17 C43 C44 113.1(14) . . ?
F16 C43 C44 113.7(12) . . ?
F18 C43 C44 109.3(11) . . ?
O9 C44 C45 128.9(10) . . ?
O9 C44 C43 115.4(12) . . ?
C45 C44 C43 115.6(11) . . ?
C44 C45 C46 124.0(10) . . ?
C44 C45 H45 118.0 . . ?
C46 C45 H45 118.0 . . ?
O10 C46 C45 128.0(11) . . ?
O10 C46 C47 115.0(11) . . ?
C45 C46 C47 117.0(10) . . ?
F13 C47 F14 110.2(14) . . ?
F13 C47 F15 105(2) . . ?
F14 C47 F15 104.1(17) . . ?
F13 C47 C46 114.8(15) . . ?
F14 C47 C46 112.1(16) . . ?
F15 C47 C46 109.4(14) . . ?
F4 C48 F6 106.7(13) . . ?
F4 C48 F5 105.2(11) . . ?
F6 C48 F5 103.7(13) . . ?
F4 C48 C49 115.0(12) . . ?
F6 C48 C49 113.9(11) . . ?
F5 C48 C49 111.3(12) . . ?
O6 C49 C50 128.7(10) . . ?
O6 C49 C48 116.7(11) . . ?
C50 C49 C48 114.6(10) . . ?
C51 C50 C49 124.8(10) . . ?
C51 C50 H50 117.6 . . ?
C49 C50 H50 117.6 . . ?
O5 C51 C50 128.0(11) . . ?
O5 C51 C52 115.3(10) . . ?
C50 C51 C52 116.7(10) . . ?
F3 C52 F2 108.3(12) . . ?
F3 C52 F1 106.5(12) . . ?
F2 C52 F1 105.2(10) . . ?
F3 C52 C51 115.4(10) . . ?
F2 C52 C51 110.4(12) . . ?
F1 C52 C51 110.6(10) . . ?
F9 C53 F8 107.3(14) . . ?
F9 C53 F7 104.0(17) . . ?
F8 C53 F7 97.4(16) . . ?
F9 C53 C54 117.8(16) . . ?
F8 C53 C54 117.1(15) . . ?
F7 C53 C54 110.4(14) . . ?
O7 C54 C55 130.3(9) . . ?
O7 C54 C53 113.4(12) . . ?
C55 C54 C53 116.3(11) . . ?
C54 C55 C56 123.9(9) . . ?
C54 C55 H55 118.0 . . ?
C56 C55 H55 118.0 . . ?
O8 C56 C55 126.8(9) . . ?
O8 C56 C57 116.2(9) . . ?
C55 C56 C57 117.1(9) . . ?
F10 C57 F12 107.2(10) . . ?
F10 C57 F11 102.1(12) . . ?
F12 C57 F11 105.9(11) . . ?
F10 C57 C56 113.9(9) . . ?
F12 C57 C56 115.9(11) . . ?
F11 C57 C56 110.8(10) . . ?
C59 C58 Ag15 173.3(7) . 2_565 ?
C59 C58 Ag24 90.6(6) . . ?
Ag15 C58 Ag24 92.5(3) 2_565 . ?
C59 C58 Ag23 99.1(7) . . ?
Ag15 C58 Ag23 86.5(3) 2_565 . ?
Ag24 C58 Ag23 95.9(3) . . ?
C58 C59 C60 174.0(9) . . ?
C58 C59 Ag24 60.7(5) . . ?
C60 C59 Ag24 124.5(6) . . ?
C61 C60 C62 112.4(14) . . ?
C61 C60 C63 107.3(13) . . ?
C62 C60 C63 110.0(13) . . ?
C61 C60 C59 108.0(11) . . ?
C62 C60 C59 110.4(8) . . ?
C63 C60 C59 108.6(10) . . ?
C60 C61 H61A 109.5 . . ?
C60 C61 H61B 109.5 . . ?
H61A C61 H61B 109.5 . . ?
C60 C61 H61C 109.5 . . ?
H61A C61 H61C 109.5 . . ?
H61B C61 H61C 109.5 . . ?
C60 C62 H62A 109.5 . . ?
C60 C62 H62B 109.5 . . ?
H62A C62 H62B 109.5 . . ?
C60 C62 H62C 109.5 . . ?
H62A C62 H62C 109.5 . . ?
H62B C62 H62C 109.5 . . ?
C60 C63 H63A 109.5 . . ?
C60 C63 H63B 109.5 . . ?
H63A C63 H63B 109.5 . . ?
C60 C63 H63C 109.5 . . ?
H63A C63 H63C 109.5 . . ?
H63B C63 H63C 109.5 . . ?
C65 C64 Ag15 143.1(7) . . ?
C65 C64 Ag14 104.8(6) . . ?
Ag15 C64 Ag14 97.7(3) . . ?
C65 C64 Ag13 119.9(7) . . ?
Ag15 C64 Ag13 87.2(3) . . ?
Ag14 C64 Ag13 92.9(3) . . ?
C64 C65 C66 176.6(9) . . ?
C68 C66 C65 109.6(10) . . ?
C68 C66 C67 114.6(11) . . ?
C65 C66 C67 111.4(9) . . ?
C68 C66 C69 108.0(13) . . ?
C65 C66 C69 105.1(9) . . ?
C67 C66 C69 107.7(12) . . ?
C66 C67 H67A 109.5 . . ?
C66 C67 H67B 109.5 . . ?
H67A C67 H67B 109.5 . . ?
C66 C67 H67C 109.5 . . ?
H67A C67 H67C 109.5 . . ?
H67B C67 H67C 109.5 . . ?
C66 C68 H68A 109.5 . . ?
C66 C68 H68B 109.5 . . ?
H68A C68 H68B 109.5 . . ?
C66 C68 H68C 109.5 . . ?
H68A C68 H68C 109.5 . . ?
H68B C68 H68C 109.5 . . ?
C66 C69 H69A 109.5 . . ?
C66 C69 H69B 109.5 . . ?
H69A C69 H69B 109.5 . . ?
C66 C69 H69C 109.5 . . ?
H69A C69 H69C 109.5 . . ?
H69B C69 H69C 109.5 . . ?
C71 C70 Ag18 155.9(7) . . ?
C71 C70 Ag19 108.8(6) . . ?
Ag18 C70 Ag19 95.3(3) . . ?
C71 C70 Ag17 88.0(5) . . ?
Ag18 C70 Ag17 95.6(3) . . ?
Ag19 C70 Ag17 84.1(2) . . ?
C70 C71 C72 173.7(9) . . ?
C70 C71 Ag17 63.6(5) . . ?
C72 C71 Ag17 122.7(6) . . ?
C71 C72 C74 107.8(8) . . ?
C71 C72 C73 109.8(7) . . ?
C74 C72 C73 110.1(8) . . ?
C71 C72 C75 108.2(8) . . ?
C74 C72 C75 111.2(9) . . ?
C73 C72 C75 109.7(9) . . ?
C72 C73 H73A 109.5 . . ?
C72 C73 H73B 109.5 . . ?
H73A C73 H73B 109.5 . . ?
C72 C73 H73C 109.5 . . ?
H73A C73 H73C 109.5 . . ?
H73B C73 H73C 109.5 . . ?
C72 C74 H74A 109.5 . . ?
C72 C74 H74B 109.5 . . ?
H74A C74 H74B 109.5 . . ?
C72 C74 H74C 109.5 . . ?
H74A C74 H74C 109.5 . . ?
H74B C74 H74C 109.5 . . ?
C72 C75 H75A 109.5 . . ?
C72 C75 H75B 109.5 . . ?
H75A C75 H75B 109.5 . . ?
C72 C75 H75C 109.5 . . ?
H75A C75 H75C 109.5 . . ?
H75B C75 H75C 109.5 . . ?
C77 C76 Ag17 143.3(7) . . ?
C77 C76 Ag14 127.5(7) . . ?
Ag17 C76 Ag14 88.4(3) . . ?
C77 C76 A16 92.7(7) . . ?
Ag17 C76 A16 96.2(3) . . ?
Ag14 C76 A16 87.8(3) . . ?
C77 C76 Ag16 97.1(8) . . ?
Ag17 C76 Ag16 84.6(17) . . ?
Ag14 C76 Ag16 96(2) . . ?
C76 C77 C78 174.1(10) . . ?
C76 C77 A16 59.2(5) . . ?
C78 C77 A16 126.7(6) . . ?
C77 C78 C81 110.4(8) . . ?
C77 C78 C80 108.3(8) . . ?
C81 C78 C80 111.3(11) . . ?
C77 C78 C79 107.5(8) . . ?
C81 C78 C79 109.8(10) . . ?
C80 C78 C79 109.4(9) . . ?
C78 C79 H79A 109.5 . . ?
C78 C79 H79B 109.5 . . ?
H79A C79 H79B 109.5 . . ?
C78 C79 H79C 109.5 . . ?
H79A C79 H79C 109.5 . . ?
H79B C79 H79C 109.5 . . ?
C78 C80 H80A 109.5 . . ?
C78 C80 H80B 109.5 . . ?
H80A C80 H80B 109.5 . . ?
C78 C80 H80C 109.5 . . ?
H80A C80 H80C 109.5 . . ?
H80B C80 H80C 109.5 . . ?
C78 C81 H81A 109.5 . . ?
C78 C81 H81B 109.5 . . ?
H81A C81 H81B 109.5 . . ?
C78 C81 H81C 109.5 . . ?
H81A C81 H81C 109.5 . . ?
H81B C81 H81C 109.5 . . ?
C83 C82 Ag18 149.7(7) . 2_565 ?
C83 C82 Ag24 117.1(6) . 2_565 ?
Ag18 C82 Ag24 83.2(3) 2_565 2_565 ?
C83 C82 Ag20 92.1(6) . . ?
Ag18 C82 Ag20 109.5(4) 2_565 . ?
Ag24 C82 Ag20 94.4(3) 2_565 . ?
C82 C83 C84 171.9(9) . . ?
C82 C83 Ag20 60.0(5) . . ?
C84 C83 Ag20 127.9(6) . . ?
C83 C84 C87 108.8(8) . . ?
C83 C84 C86 110.1(8) . . ?
C87 C84 C86 111.8(10) . . ?
C83 C84 C85 108.5(8) . . ?
C87 C84 C85 109.4(10) . . ?
C86 C84 C85 108.3(9) . . ?
C84 C85 H85A 109.5 . . ?
C84 C85 H85B 109.5 . . ?
H85A C85 H85B 109.5 . . ?
C84 C85 H85C 109.5 . . ?
H85A C85 H85C 109.5 . . ?
H85B C85 H85C 109.5 . . ?
C84 C86 H86A 109.5 . . ?
C84 C86 H86B 109.5 . . ?
H86A C86 H86B 109.5 . . ?
C84 C86 H86C 109.5 . . ?
H86A C86 H86C 109.5 . . ?
H86B C86 H86C 109.5 . . ?
C84 C87 H87A 109.5 . . ?
C84 C87 H87B 109.5 . . ?
H87A C87 H87B 109.5 . . ?
C84 C87 H87C 109.5 . . ?
H87A C87 H87C 109.5 . . ?
H87B C87 H87C 109.5 . . ?
C89 C88 Ag21 160.5(7) . . ?
C89 C88 Ag13 114.3(6) . 2_565 ?
Ag21 C88 Ag13 84.8(3) . 2_565 ?
C89 C88 Ag22 85.6(5) . . ?
Ag21 C88 Ag22 99.2(3) . . ?
Ag13 C88 Ag22 89.1(3) 2_565 . ?
C88 C89 C90 170.7(8) . . ?
C88 C89 Ag22 64.9(5) . . ?
C90 C89 Ag22 124.1(5) . . ?
C89 C90 C91 107.5(8) . . ?
C89 C90 C92 110.1(7) . . ?
C91 C90 C92 111.4(9) . . ?
C89 C90 C93 108.3(8) . . ?
C91 C90 C93 110.7(8) . . ?
C92 C90 C93 108.8(9) . . ?
C90 C91 H91A 109.5 . . ?
C90 C91 H91B 109.5 . . ?
H91A C91 H91B 109.5 . . ?
C90 C91 H91C 109.5 . . ?
H91A C91 H91C 109.5 . . ?
H91B C91 H91C 109.5 . . ?
C90 C92 H92A 109.5 . . ?
C90 C92 H92B 109.5 . . ?
H92A C92 H92B 109.5 . . ?
C90 C92 H92C 109.5 . . ?
H92A C92 H92C 109.5 . . ?
H92B C92 H92C 109.5 . . ?
C90 C93 H93A 109.5 . . ?
C90 C93 H93B 109.5 . . ?
H93A C93 H93B 109.5 . . ?
C90 C93 H93C 109.5 . . ?
H93A C93 H93C 109.5 . . ?
H93B C93 H93C 109.5 . . ?
C95 C94 Ag19 127.6(7) . . ?
C95 C94 Ag20 142.1(7) . . ?
Ag19 C94 Ag20 89.5(3) . . ?
C95 C94 Ag21 94.5(6) . . ?
Ag19 C94 Ag21 101.9(3) . . ?
Ag20 C94 Ag21 83.7(3) . . ?
C94 C95 C96 174.8(9) . . ?
C94 C95 Ag21 58.1(5) . . ?
C96 C95 Ag21 127.0(6) . . ?
C95 C96 C99 108.1(8) . . ?
C95 C96 C98 109.7(8) . . ?
C99 C96 C98 112.4(10) . . ?
C95 C96 C97 109.0(8) . . ?
C99 C96 C97 108.7(9) . . ?
C98 C96 C97 108.7(10) . . ?
C96 C97 H97A 109.5 . . ?
C96 C97 H97B 109.5 . . ?
H97A C97 H97B 109.5 . . ?
C96 C97 H97C 109.5 . . ?
H97A C97 H97C 109.5 . . ?
H97B C97 H97C 109.5 . . ?
C96 C98 H98A 109.5 . . ?
C96 C98 H98B 109.5 . . ?
H98A C98 H98B 109.5 . . ?
C96 C98 H98C 109.5 . . ?
H98A C98 H98C 109.5 . . ?
H98B C98 H98C 109.5 . . ?
C96 C99 H99A 109.5 . . ?
C96 C99 H99B 109.5 . . ?
H99A C99 H99B 109.5 . . ?
C96 C99 H99C 109.5 . . ?
H99A C99 H99C 109.5 . . ?
H99B C99 H99C 109.5 . . ?
F30 C100 F29 106.5(9) . . ?
F30 C100 F28 107.1(9) . . ?
F29 C100 F28 101.6(9) . . ?
F30 C100 C101 117.0(9) . . ?
F29 C100 C101 111.0(8) . . ?
F28 C100 C101 112.3(8) . . ?
O19 C101 C102 130.3(8) . . ?
O19 C101 C100 113.7(8) . . ?
C102 C101 C100 115.9(8) . . ?
C101 C102 C103 124.2(8) . . ?
C101 C102 H102 117.9 . . ?
C103 C102 H102 117.9 . . ?
O20 C103 C102 127.7(8) . . ?
O20 C103 C104 114.7(7) . . ?
C102 C103 C104 117.5(7) . . ?
F25 C104 F26 106.9(8) . . ?
F25 C104 F27 106.3(8) . . ?
F26 C104 F27 105.5(8) . . ?
F25 C104 C103 115.0(7) . . ?
F26 C104 C103 112.1(8) . . ?
F27 C104 C103 110.4(8) . . ?
F36 C105 F34 106.6(11) . . ?
F36 C105 F35 106.2(12) . . ?
F34 C105 F35 106.4(10) . . ?
F36 C105 C106 113.2(10) . . ?
F34 C105 C106 114.5(10) . . ?
F35 C105 C106 109.4(11) . . ?
O15 C106 C107 128.1(10) . . ?
O15 C106 C105 114.2(9) . . ?
C107 C106 C105 117.6(8) . . ?
C106 C107 C108 123.9(9) . . ?
C106 C107 H107 118.1 . . ?
C108 C107 H107 118.1 . . ?
O16 C108 C107 129.9(9) . . ?
O16 C108 C109 114.7(10) . . ?
C107 C108 C109 115.4(9) . . ?
F32 C109 F31 108.1(13) . . ?
F32 C109 F33 104.6(14) . . ?
F31 C109 F33 98.2(12) . . ?
F32 C109 C108 114.0(12) . . ?
F31 C109 C108 116.5(11) . . ?
F33 C109 C108 113.7(11) . . ?
F20 C110 F21 106.1(10) . . ?
F20 C110 F19 108.2(10) . . ?
F21 C110 F19 101.6(9) . . ?
F20 C110 C111 115.5(8) . . ?
F21 C110 C111 113.7(8) . . ?
F19 C110 C111 110.8(8) . . ?
O17 C111 C112 130.1(8) . . ?
O17 C111 C110 112.3(8) . . ?
C112 C111 C110 117.5(7) . . ?
C111 C112 C113 124.4(7) . . ?
C111 C112 H112 117.8 . . ?
C113 C112 H112 117.8 . . ?
O18 C113 C112 129.3(8) . . ?
O18 C113 C114 114.8(8) . . ?
C112 C113 C114 115.9(8) . . ?
F23 C114 F24 109.0(10) . . ?
F23 C114 F22 104.5(10) . . ?
F24 C114 F22 102.6(10) . . ?
F23 C114 C113 113.8(9) . . ?
F24 C114 C113 113.7(9) . . ?
F22 C114 C113 112.3(9) . . ?
C116 C115 Ag27 138.8(6) . 2_666 ?
C116 C115 Ag35 139.3(6) . . ?
Ag27 C115 Ag35 80.4(3) 2_666 . ?
C116 C115 Ag36 85.2(5) . 2_666 ?
Ag27 C115 Ag36 99.5(3) 2_666 2_666 ?
Ag35 C115 Ag36 100.7(3) . 2_666 ?
C115 C116 C117 172.7(8) . . ?
C115 C116 Ag36 65.9(5) . 2_666 ?
C117 C116 Ag36 121.1(5) . 2_666 ?
C116 C117 C118 107.7(7) . . ?
C116 C117 C120 108.9(7) . . ?
C118 C117 C120 112.8(9) . . ?
C116 C117 C119 111.4(7) . . ?
C118 C117 C119 107.6(8) . . ?
C120 C117 C119 108.4(9) . . ?
C117 C118 H11F 109.5 . . ?
C117 C118 H11G 109.5 . . ?
H11F C118 H11G 109.5 . . ?
C117 C118 H11H 109.5 . . ?
H11F C118 H11H 109.5 . . ?
H11G C118 H11H 109.5 . . ?
C117 C119 H11I 109.5 . . ?
C117 C119 H11J 109.5 . . ?
H11I C119 H11J 109.5 . . ?
C117 C119 H11K 109.5 . . ?
H11I C119 H11K 109.5 . . ?
H11J C119 H11K 109.5 . . ?
C117 C120 H12D 109.5 . . ?
C117 C120 H12E 109.5 . . ?
H12D C120 H12E 109.5 . . ?
C117 C120 H12F 109.5 . . ?
H12D C120 H12F 109.5 . . ?
H12E C120 H12F 109.5 . . ?
C122 C121 Ag32 140.2(6) . . ?
C122 C121 Ag34 130.9(6) . . ?
Ag32 C121 Ag34 81.0(3) . . ?
C122 C121 Ag35 95.8(6) . . ?
Ag32 C121 Ag35 103.1(3) . . ?
Ag34 C121 Ag35 97.9(3) . . ?
C121 C122 C123 175.3(8) . . ?
C121 C122 Ag35 57.2(5) . . ?
C123 C122 Ag35 127.5(6) . . ?
C122 C123 C126 108.0(7) . . ?
C122 C123 C125 108.5(8) . . ?
C126 C123 C125 111.3(9) . . ?
C122 C123 C124 109.2(7) . . ?
C126 C123 C124 109.9(8) . . ?
C125 C123 C124 109.8(8) . . ?
C123 C124 H12G 109.5 . . ?
C123 C124 H12H 109.5 . . ?
H12G C124 H12H 109.5 . . ?
C123 C124 H12I 109.5 . . ?
H12G C124 H12I 109.5 . . ?
H12H C124 H12I 109.5 . . ?
C123 C125 H12J 109.5 . . ?
C123 C125 H12K 109.5 . . ?
H12J C125 H12K 109.5 . . ?
C123 C125 H12L 109.5 . . ?
H12J C125 H12L 109.5 . . ?
H12K C125 H12L 109.5 . . ?
C123 C126 H12M 109.5 . . ?
C123 C126 H12N 109.5 . . ?
H12M C126 H12N 109.5 . . ?
C123 C126 H12O 109.5 . . ?
H12M C126 H12O 109.5 . . ?
H12N C126 H12O 109.5 . . ?
C128 C127 Ag33 165.3(7) . 2_666 ?
C128 C127 Ag26 106.3(6) . . ?
Ag33 C127 Ag26 88.3(3) 2_666 . ?
C128 C127 Ag30 91.9(6) . . ?
Ag33 C127 Ag30 90.4(3) 2_666 . ?
Ag26 C127 Ag30 87.5(3) . . ?
C127 C128 C129 173.7(9) . . ?
C127 C128 Ag30 60.4(5) . . ?
C129 C128 Ag30 125.8(5) . . ?
C128 C129 C130 113.2(12) . . ?
C128 C129 C31A 112.2(12) . . ?
C128 C129 C32A 106.4(11) . . ?
C31A C129 C32A 110.6(12) . . ?
C128 C129 C132 107.3(11) . . ?
C130 C129 C132 111.0(11) . . ?
C128 C129 C30A 111.1(11) . . ?
C31A C129 C30A 110.2(11) . . ?
C32A C129 C30A 106.1(10) . . ?
C128 C129 C131 109.2(10) . . ?
C130 C129 C131 110.1(11) . . ?
C132 C129 C131 105.8(10) . . ?
C129 C130 H13A 109.5 . . ?
C129 C130 H13B 109.5 . . ?
H13A C130 H13B 109.5 . . ?
C129 C130 H13C 109.5 . . ?
H13A C130 H13C 109.5 . . ?
H13B C130 H13C 109.5 . . ?
C129 C131 H13D 109.5 . . ?
C129 C131 H13E 109.5 . . ?
H13D C131 H13E 109.5 . . ?
C129 C131 H13F 109.5 . . ?
H13D C131 H13F 109.5 . . ?
H13E C131 H13F 109.5 . . ?
C129 C132 H13G 109.5 . . ?
C129 C132 H13H 109.5 . . ?
H13G C132 H13H 109.5 . . ?
C129 C132 H13I 109.5 . . ?
H13G C132 H13I 109.5 . . ?
H13H C132 H13I 109.5 . . ?
C129 C30A H30D 109.5 . . ?
C129 C30A H30E 109.5 . . ?
H30D C30A H30E 109.5 . . ?
C129 C30A H30F 109.5 . . ?
H30D C30A H30F 109.5 . . ?
H30E C30A H30F 109.5 . . ?
C129 C31A H31A 109.5 . . ?
C129 C31A H31B 109.5 . . ?
H31A C31A H31B 109.5 . . ?
C129 C31A H31C 109.5 . . ?
H31A C31A H31C 109.5 . . ?
H31B C31A H31C 109.5 . . ?
C129 C32A H32A 109.5 . . ?
C129 C32A H32B 109.5 . . ?
H32A C32A H32B 109.5 . . ?
C129 C32A H32C 109.5 . . ?
H32A C32A H32C 109.5 . . ?
H32B C32A H32C 109.5 . . ?
C134 C133 Ag27 166.2(6) . . ?
C134 C133 Ag28 104.5(5) . . ?
Ag27 C133 Ag28 88.6(3) . . ?
C134 C133 Ag25 88.8(5) . . ?
Ag27 C133 Ag25 97.0(3) . . ?
Ag28 C133 Ag25 83.5(2) . . ?
C133 C134 C135 175.5(8) . . ?
C133 C134 Ag25 62.9(5) . . ?
C135 C134 Ag25 121.5(5) . . ?
C134 C135 C138 109.8(7) . . ?
C134 C135 C137 109.0(7) . . ?
C138 C135 C137 110.8(8) . . ?
C134 C135 C136 109.3(7) . . ?
C138 C135 C136 108.2(8) . . ?
C137 C135 C136 109.8(8) . . ?
C135 C136 H13J 109.5 . . ?
C135 C136 H13K 109.5 . . ?
H13J C136 H13K 109.5 . . ?
C135 C136 H13L 109.5 . . ?
H13J C136 H13L 109.5 . . ?
H13K C136 H13L 109.5 . . ?
C135 C137 H13M 109.5 . . ?
C135 C137 H13N 109.5 . . ?
H13M C137 H13N 109.5 . . ?
C135 C137 H13O 109.5 . . ?
H13M C137 H13O 109.5 . . ?
H13N C137 H13O 109.5 . . ?
C135 C138 H13P 109.5 . . ?
C135 C138 H13Q 109.5 . . ?
H13P C138 H13Q 109.5 . . ?
C135 C138 H13R 109.5 . . ?
H13P C138 H13R 109.5 . . ?
H13Q C138 H13R 109.5 . . ?
C140 C139 Ag26 125.5(7) . . ?
C140 C139 Ag28 125.5(6) . . ?
Ag26 C139 Ag28 95.0(3) . . ?
C140 C139 Ag29 118.2(6) . . ?
Ag26 C139 Ag29 91.9(3) . . ?
Ag28 C139 Ag29 91.5(3) . . ?
C139 C140 C141 177.4(10) . . ?
C143 C141 C142 114.7(15) . . ?
C143 C141 C140 110.0(10) . . ?
C142 C141 C140 109.5(9) . . ?
C143 C141 C144 107.7(17) . . ?
C142 C141 C144 107.4(11) . . ?
C140 C141 C144 107.2(10) . . ?
C141 C142 H14A 109.5 . . ?
C141 C142 H14B 109.5 . . ?
H14A C142 H14B 109.5 . . ?
C141 C142 H14C 109.5 . . ?
H14A C142 H14C 109.5 . . ?
H14B C142 H14C 109.5 . . ?
C141 C143 H14D 109.5 . . ?
C141 C143 H14E 109.5 . . ?
H14D C143 H14E 109.5 . . ?
C141 C143 H14F 109.5 . . ?
H14D C143 H14F 109.5 . . ?
H14E C143 H14F 109.5 . . ?
C141 C144 H14G 109.5 . . ?
C141 C144 H14H 109.5 . . ?
H14G C144 H14H 109.5 . . ?
C141 C144 H14I 109.5 . . ?
H14G C144 H14I 109.5 . . ?
H14H C144 H14I 109.5 . . ?
C146 C145 Ag32 162.4(6) . . ?
C146 C145 Ag29 106.8(6) . . ?
Ag32 C145 Ag29 89.4(3) . . ?
C146 C145 Ag31 91.3(5) . . ?
Ag32 C145 Ag31 96.6(3) . . ?
Ag29 C145 Ag31 86.3(2) . . ?
C145 C146 C147 173.1(8) . . ?
C145 C146 Ag31 61.0(5) . . ?
C147 C146 Ag31 125.0(6) . . ?
C146 C147 C148 110.5(8) . . ?
C146 C147 C149 109.8(8) . . ?
C148 C147 C149 113.2(10) . . ?
C146 C147 C150 106.9(8) . . ?
C148 C147 C150 108.0(11) . . ?
C149 C147 C150 108.2(9) . . ?
C147 C148 H14J 109.5 . . ?
C147 C148 H14K 109.5 . . ?
H14J C148 H14K 109.5 . . ?
C147 C148 H14L 109.5 . . ?
H14J C148 H14L 109.5 . . ?
H14K C148 H14L 109.5 . . ?
C147 C149 H14M 109.5 . . ?
C147 C149 H14N 109.5 . . ?
H14M C149 H14N 109.5 . . ?
C147 C149 H14O 109.5 . . ?
H14M C149 H14O 109.5 . . ?
H14N C149 H14O 109.5 . . ?
C147 C150 H15A 109.5 . . ?
C147 C150 H15B 109.5 . . ?
H15A C150 H15B 109.5 . . ?
C147 C150 H15C 109.5 . . ?
H15A C150 H15C 109.5 . . ?
H15B C150 H15C 109.5 . . ?
C152 C151 Ag33 132.8(7) . . ?
C152 C151 Ag36 139.1(6) . . ?
Ag33 C151 Ag36 82.0(3) . . ?
C152 C151 Ag34 91.7(5) . . ?
Ag33 C151 Ag34 102.3(3) . . ?
Ag36 C151 Ag34 101.7(3) . . ?
C151 C152 C153 174.0(8) . . ?
C151 C152 Ag34 60.5(5) . . ?
C153 C152 Ag34 125.4(5) . . ?
C152 C153 C154 111.4(10) . . ?
C152 C153 C55A 113.4(10) . . ?
C152 C153 C54A 108.4(8) . . ?
C55A C153 C54A 111.3(10) . . ?
C152 C153 C156 104.6(12) . . ?
C154 C153 C156 112.2(11) . . ?
C152 C153 C155 109.5(10) . . ?
C154 C153 C155 111.4(11) . . ?
C156 C153 C155 107.5(10) . . ?
C152 C153 C56A 107.9(9) . . ?
C55A C153 C56A 110.3(10) . . ?
C54A C153 C56A 105.2(9) . . ?
C153 C154 H15D 109.5 . . ?
C153 C154 H15E 109.5 . . ?
H15D C154 H15E 109.5 . . ?
C153 C154 H15F 109.5 . . ?
H15D C154 H15F 109.5 . . ?
H15E C154 H15F 109.5 . . ?
C153 C155 H15G 109.5 . . ?
C153 C155 H15H 109.5 . . ?
H15G C155 H15H 109.5 . . ?
C153 C155 H15I 109.5 . . ?
H15G C155 H15I 109.5 . . ?
H15H C155 H15I 109.5 . . ?
C153 C156 H15J 109.5 . . ?
C153 C156 H15K 109.5 . . ?
H15J C156 H15K 109.5 . . ?
C153 C156 H15L 109.5 . . ?
H15J C156 H15L 109.5 . . ?
H15K C156 H15L 109.5 . . ?
C153 C54A H54A 109.5 . . ?
C153 C54A H54B 109.5 . . ?
H54A C54A H54B 109.5 . . ?
C153 C54A H54C 109.5 . . ?
H54A C54A H54C 109.5 . . ?
H54B C54A H54C 109.5 . . ?
C153 C55A H55C 109.5 . . ?
C153 C55A H55D 109.5 . . ?
H55C C55A H55D 109.5 . . ?
C153 C55A H55E 109.5 . . ?
H55C C55A H55E 109.5 . . ?
H55D C55A H55E 109.5 . . ?
C153 C56A H56A 109.5 . . ?
C153 C56A H56B 109.5 . . ?
H56A C56A H56B 109.5 . . ?
C153 C56A H56C 109.5 . . ?
H56A C56A H56C 109.5 . . ?
H56B C56A H56C 109.5 . . ?
F54 C157 F52 112.1(11) . . ?
F54A C157 F53A 109.0(12) . . ?
F54 C157 F53 103.1(9) . . ?
F52 C157 F53 103.5(10) . . ?
F54A C157 F52A 102.7(11) . . ?
F53A C157 F52A 101.9(11) . . ?
F54 C157 C158 113.4(8) . . ?
F52 C157 C158 112.8(10) . . ?
F54A C157 C158 116.5(11) . . ?
F53A C157 C158 114.1(11) . . ?
F53 C157 C158 111.1(9) . . ?
F52A C157 C158 111.0(9) . . ?
O27 C158 C159 127.8(8) . . ?
O27 C158 C157 115.2(7) . . ?
C159 C158 C157 116.9(7) . . ?
C158 C159 C160 124.3(7) . . ?
C158 C159 H159 117.9 . . ?
C160 C159 H159 117.9 . . ?
O28 C160 C159 129.5(8) . . ?
O28 C160 C161 114.2(8) . . ?
C159 C160 C161 116.2(8) . . ?
F50 C161 F51 102.3(11) . . ?
F50 C161 F49 106.0(11) . . ?
F51 C161 F49 105.0(11) . . ?
F50 C161 C160 112.3(9) . . ?
F51 C161 C160 114.1(9) . . ?
F49 C161 C160 115.9(10) . . ?
F46 C162 F48 107.5(11) . . ?
F46 C162 F47 107.2(9) . . ?
F48 C162 F47 105.1(9) . . ?
F46 C162 C163 111.6(8) . . ?
F48 C162 C163 110.4(9) . . ?
F47 C162 C163 114.7(10) . . ?
O30 C163 C164 128.9(8) . . ?
O30 C163 C162 113.4(9) . . ?
C164 C163 C162 117.6(9) . . ?
C163 C164 C165 125.0(8) . . ?
C163 C164 H164 117.5 . . ?
C165 C164 H164 117.5 . . ?
O29 C165 C164 126.8(9) . . ?
O29 C165 C166 115.2(8) . . ?
C164 C165 C166 118.0(8) . . ?
F45 C166 F43 110.2(12) . . ?
F45 C166 F44 104.4(11) . . ?
F43 C166 F44 102.2(10) . . ?
F45 C166 C165 114.3(9) . . ?
F43 C166 C165 115.5(10) . . ?
F44 C166 C165 108.9(10) . . ?
F38 C167 F39 108.2(9) . . ?
F38 C167 F37 106.5(9) . . ?
F39 C167 F37 106.1(8) . . ?
F38 C167 C168 113.3(7) . . ?
F39 C167 C168 113.0(9) . . ?
F37 C167 C168 109.2(8) . . ?
O25 C168 C169 129.3(8) . . ?
O25 C168 C167 114.4(8) . . ?
C169 C168 C167 116.3(7) . . ?
C170 C169 C168 123.4(7) . . ?
C170 C169 H169 118.3 . . ?
C168 C169 H169 118.3 . . ?
O26 C170 C169 128.4(8) . . ?
O26 C170 C171 113.7(8) . . ?
C169 C170 C171 117.8(8) . . ?
F42B C171 F40B 119(2) . . ?
F40A C171 F41A 109(2) . . ?
F40A C171 F42A 111.8(17) . . ?
F41A C171 F42A 100.6(16) . . ?
F42B C171 F41B 92(2) . . ?
F40B C171 F41B 99(2) . . ?
F40A C171 C170 116.1(13) . . ?
F42B C171 C170 119.4(16) . . ?
F40B C171 C170 113.5(13) . . ?
F41A C171 C170 105.0(14) . . ?
F42A C171 C170 112.5(10) . . ?
F41B C171 C170 107.5(16) . . ?
C173 C172 Ag48 109.9(10) . . ?
C173 C172 Ag47 157.0(8) . . ?
Ag48 C172 Ag47 92.3(9) . . ?
C173 C172 A45A 95.3(7) . . ?
Ag47 C172 A45A 94.4(4) . . ?
C173 C172 A48 115.3(7) . . ?
Ag47 C172 A48 85.7(4) . . ?
A45A C172 A48 88.5(4) . . ?
C173 C172 Ag45 102.9(10) . . ?
Ag48 C172 Ag45 85.3(14) . . ?
Ag47 C172 Ag45 84.1(10) . . ?
C172 C173 C174 172.9(11) . . ?
C172 C173 A45A 57.2(6) . . ?
C174 C173 A45A 129.7(8) . . ?
C172 C173 Ag48 45.9(7) . . ?
C174 C173 Ag48 136.6(8) . . ?
C176 C174 C173 109.6(10) . . ?
C176 C174 C175 112.5(13) . . ?
C173 C174 C175 106.3(9) . . ?
C176 C174 C177 111.5(12) . . ?
C173 C174 C177 109.3(10) . . ?
C175 C174 C177 107.5(11) . . ?
C174 C175 H17D 109.5 . . ?
C174 C175 H17E 109.5 . . ?
H17D C175 H17E 109.5 . . ?
C174 C175 H17F 109.5 . . ?
H17D C175 H17F 109.5 . . ?
H17E C175 H17F 109.5 . . ?
C174 C176 H17G 109.5 . . ?
C174 C176 H17H 109.5 . . ?
H17G C176 H17H 109.5 . . ?
C174 C176 H17I 109.5 . . ?
H17G C176 H17I 109.5 . . ?
H17H C176 H17I 109.5 . . ?
C174 C177 H17J 109.5 . . ?
C174 C177 H17K 109.5 . . ?
H17J C177 H17K 109.5 . . ?
C174 C177 H17L 109.5 . . ?
H17J C177 H17L 109.5 . . ?
H17K C177 H17L 109.5 . . ?
C179 C178 Ag44 149.4(7) . . ?
C179 C178 Ag39 124.3(6) . 2_556 ?
Ag44 C178 Ag39 82.7(3) . 2_556 ?
C179 C178 Ag40 88.8(6) . 2_556 ?
Ag44 C178 Ag40 103.9(4) . 2_556 ?
Ag39 C178 Ag40 95.5(3) 2_556 2_556 ?
C178 C179 C180 172.4(9) . . ?
C178 C179 Ag40 62.4(5) . 2_556 ?
C180 C179 Ag40 124.9(6) . 2_556 ?
C179 C180 C183 109.2(9) . . ?
C179 C180 C182 107.8(7) . . ?
C183 C180 C182 110.7(9) . . ?
C179 C180 C181 108.7(8) . . ?
C183 C180 C181 111.0(9) . . ?
C182 C180 C181 109.3(9) . . ?
C180 C181 H18D 109.5 . . ?
C180 C181 H18E 109.5 . . ?
H18D C181 H18E 109.5 . . ?
C180 C181 H18F 109.5 . . ?
H18D C181 H18F 109.5 . . ?
H18E C181 H18F 109.5 . . ?
C180 C182 H18G 109.5 . . ?
C180 C182 H18H 109.5 . . ?
H18G C182 H18H 109.5 . . ?
C180 C182 H18I 109.5 . . ?
H18G C182 H18I 109.5 . . ?
H18H C182 H18I 109.5 . . ?
C180 C183 H18J 109.5 . . ?
C180 C183 H18K 109.5 . . ?
H18J C183 H18K 109.5 . . ?
C180 C183 H18L 109.5 . . ?
H18J C183 H18L 109.5 . . ?
H18K C183 H18L 109.5 . . ?
C185 C184 Ag44 150.5(8) . . ?
C185 C184 Ag42 111.0(8) . . ?
Ag44 C184 Ag42 98.0(3) . . ?
C185 C184 Ag43 89.0(6) . . ?
Ag44 C184 Ag43 100.6(3) . . ?
Ag42 C184 Ag43 81.3(3) . . ?
C184 C185 C186 175.6(10) . . ?
C184 C185 Ag43 63.2(6) . . ?
C186 C185 Ag43 121.1(6) . . ?
C189 C186 C185 111.1(10) . . ?
C189 C186 C187 116.6(12) . . ?
C185 C186 C187 112.5(9) . . ?
C189 C186 C188 107.2(14) . . ?
C185 C186 C188 104.3(11) . . ?
C187 C186 C188 104.0(10) . . ?
C186 C187 H18M 109.5 . . ?
C186 C187 H18N 109.5 . . ?
H18M C187 H18N 109.5 . . ?
C186 C187 H18O 109.5 . . ?
H18M C187 H18O 109.5 . . ?
H18N C187 H18O 109.5 . . ?
C186 C189 H18S 109.5 . . ?
C186 C189 H18T 109.5 . . ?
H18S C189 H18T 109.5 . . ?
C186 C189 H18U 109.5 . . ?
H18S C189 H18U 109.5 . . ?
H18T C189 H18U 109.5 . . ?
C191 C190 Ag46 129.2(8) . . ?
C191 C190 Ag43 141.5(7) . . ?
Ag46 C190 Ag43 89.1(6) . . ?
C191 C190 A41A 97.4(7) . . ?
Ag43 C190 A41A 97.8(3) . . ?
C191 C190 A46A 133.1(7) . . ?
Ag43 C190 A46A 82.7(3) . . ?
A41A C190 A46A 87.9(3) . . ?
C191 C190 Ag41 100.9(7) . . ?
Ag46 C190 Ag41 87.9(10) . . ?
Ag43 C190 Ag41 82.5(3) . . ?
C190 C191 C192 175.7(9) . . ?
C190 C191 A41A 55.3(5) . . ?
C192 C191 A41A 129.0(6) . . ?
C191 C192 C195 110.0(8) . . ?
C191 C192 C194 109.3(8) . . ?
C195 C192 C194 109.3(8) . . ?
C191 C192 C193 107.8(7) . . ?
C195 C192 C193 110.6(8) . . ?
C194 C192 C193 109.9(9) . . ?
C192 C193 H19A 109.5 . . ?
C192 C193 H19B 109.5 . . ?
H19A C193 H19B 109.5 . . ?
C192 C193 H19C 109.5 . . ?
H19A C193 H19C 109.5 . . ?
H19B C193 H19C 109.5 . . ?
C192 C194 H19D 109.5 . . ?
C192 C194 H19E 109.5 . . ?
H19D C194 H19E 109.5 . . ?
C192 C194 H19F 109.5 . . ?
H19D C194 H19F 109.5 . . ?
H19E C194 H19F 109.5 . . ?
C192 C195 H19G 109.5 . . ?
C192 C195 H19H 109.5 . . ?
H19G C195 H19H 109.5 . . ?
C192 C195 H19I 109.5 . . ?
H19G C195 H19I 109.5 . . ?
H19H C195 H19I 109.5 . . ?
C197 C196 Ag38 171.9(7) . . ?
C197 C196 Ag39 93.1(6) . . ?
Ag38 C196 Ag39 90.7(3) . . ?
C197 C196 Ag37 101.6(7) . . ?
Ag38 C196 Ag37 85.6(3) . . ?
Ag39 C196 Ag37 90.8(3) . . ?
C196 C197 C198 174.3(9) . . ?
C196 C197 Ag39 59.1(5) . . ?
C198 C197 Ag39 126.1(6) . . ?
C201 C198 C197 110.6(9) . . ?
C201 C198 C200 111.8(12) . . ?
C197 C198 C200 108.4(9) . . ?
C201 C198 C199 109.6(11) . . ?
C197 C198 C199 108.5(8) . . ?
C200 C198 C199 107.9(10) . . ?
C198 C199 H19J 109.5 . . ?
C198 C199 H19K 109.5 . . ?
H19J C199 H19K 109.5 . . ?
C198 C199 H19L 109.5 . . ?
H19J C199 H19L 109.5 . . ?
H19K C199 H19L 109.5 . . ?
C198 C200 H20A 109.5 . . ?
C198 C200 H20B 109.5 . . ?
H20A C200 H20B 109.5 . . ?
C198 C200 H20C 109.5 . . ?
H20A C200 H20C 109.5 . . ?
H20B C200 H20C 109.5 . . ?
C198 C201 H20D 109.5 . . ?
C198 C201 H20E 109.5 . . ?
H20D C201 H20E 109.5 . . ?
C198 C201 H20F 109.5 . . ?
H20D C201 H20F 109.5 . . ?
H20E C201 H20F 109.5 . . ?
C23A C202 Ag40 165.9(17) . . ?
C203 C202 Ag40 134.1(9) . . ?
C23A C202 Ag42 87.6(17) . . ?
C203 C202 Ag42 128.9(9) . . ?
Ag40 C202 Ag42 97.0(4) . . ?
C23A C202 Ag47 106.5(16) . 2_556 ?
C203 C202 Ag47 87.4(7) . 2_556 ?
Ag40 C202 Ag47 86.2(3) . 2_556 ?
Ag42 C202 Ag47 97.2(3) . 2_556 ?
C202 C203 C204 175.0(12) . . ?
C202 C203 Ag47 62.4(6) . 2_556 ?
C204 C203 Ag47 122.3(8) . 2_556 ?
C205 C204 C203 109.9(12) . . ?
C205 C204 C206 108.9(11) . . ?
C203 C204 C206 111.4(12) . . ?
C205 C204 C207 109.7(11) . . ?
C203 C204 C207 108.5(12) . . ?
C206 C204 C207 108.4(11) . . ?
C204 C205 H20G 109.5 . . ?
C204 C205 H20H 109.5 . . ?
H20G C205 H20H 109.5 . . ?
C204 C205 H20I 109.5 . . ?
H20G C205 H20I 109.5 . . ?
H20H C205 H20I 109.5 . . ?
C204 C206 H20J 109.5 . . ?
C204 C206 H20K 109.5 . . ?
H20J C206 H20K 109.5 . . ?
C204 C206 H20L 109.5 . . ?
H20J C206 H20L 109.5 . . ?
H20K C206 H20L 109.5 . . ?
C204 C207 H20M 109.5 . . ?
C204 C207 H20N 109.5 . . ?
H20M C207 H20N 109.5 . . ?
C204 C207 H20O 109.5 . . ?
H20M C207 H20O 109.5 . . ?
H20N C207 H20O 109.5 . . ?
C202 C23A C24A 159(3) . . ?
C202 C23A Ag42 65.4(14) . . ?
C24A C23A Ag42 134.9(18) . . ?
C23A C24A C27A 105(2) . . ?
C23A C24A C26A 105(2) . . ?
C27A C24A C26A 114.7(15) . . ?
C23A C24A C25A 102(2) . . ?
C27A C24A C25A 114.6(15) . . ?
C26A C24A C25A 113.6(14) . . ?
C24A C25A H25A 109.5 . . ?
C24A C25A H25B 109.5 . . ?
H25A C25A H25B 109.5 . . ?
C24A C25A H25C 109.5 . . ?
H25A C25A H25C 109.5 . . ?
H25B C25A H25C 109.5 . . ?
C24A C26A H26A 109.5 . . ?
C24A C26A H26B 109.5 . . ?
H26A C26A H26B 109.5 . . ?
C24A C26A H26C 109.5 . . ?
H26A C26A H26C 109.5 . . ?
H26B C26A H26C 109.5 . . ?
C24A C27A H27A 109.5 . . ?
C24A C27A H27B 109.5 . . ?
H27A C27A H27B 109.5 . . ?
C24A C27A H27C 109.5 . . ?
H27A C27A H27C 109.5 . . ?
H27B C27A H27C 109.5 . . ?
C209 C208 A48 152.0(9) . . ?
C209 C208 Ag38 121.1(8) . . ?
A48 C208 Ag38 85.6(4) . . ?
C209 C208 Ag48 143.8(13) . . ?
Ag38 C208 Ag48 95.0(12) . . ?
C209 C208 A46A 88.4(6) . . ?
A48 C208 A46A 91.7(4) . . ?
Ag38 C208 A46A 107.0(4) . . ?
C209 C208 Ag46 87.8(6) . . ?
Ag38 C208 Ag46 95.0(10) . . ?
Ag48 C208 Ag46 91.6(13) . . ?
C208 C209 C210 174.3(10) . . ?
C208 C209 A46A 63.8(6) . . ?
C210 C209 A46A 121.9(7) . . ?
C208 C209 Ag46 64.4(6) . . ?
C210 C209 Ag46 121.1(7) . . ?
C212 C210 C209 109.5(12) . . ?
C212 C210 C211 111.5(11) . . ?
C209 C210 C211 109.8(9) . . ?
C212 C210 C213 111.0(14) . . ?
C209 C210 C213 106.5(10) . . ?
C211 C210 C213 108.5(12) . . ?
C210 C211 H21A 109.5 . . ?
C210 C211 H21B 109.5 . . ?
H21A C211 H21B 109.5 . . ?
C210 C211 H21C 109.5 . . ?
H21A C211 H21C 109.5 . . ?
H21B C211 H21C 109.5 . . ?
C210 C212 H21D 109.5 . . ?
C210 C212 H21E 109.5 . . ?
H21D C212 H21E 109.5 . . ?
C210 C212 H21F 109.5 . . ?
H21D C212 H21F 109.5 . . ?
H21E C212 H21F 109.5 . . ?
C210 C213 H21G 109.5 . . ?
C210 C213 H21H 109.5 . . ?
H21G C213 H21H 109.5 . . ?
C210 C213 H21I 109.5 . . ?
H21G C213 H21I 109.5 . . ?
H21H C213 H21I 109.5 . . ?
F61 C214 F63 107.8(10) . . ?
F61 C214 F62 107.9(10) . . ?
F63 C214 F62 106.3(10) . . ?
F61 C214 C215 112.3(10) . . ?
F63 C214 C215 113.8(10) . . ?
F62 C214 C215 108.4(9) . . ?
O38 C215 C216 127.1(10) . . ?
O38 C215 C214 114.8(9) . . ?
C216 C215 C214 118.1(9) . . ?
C215 C216 C217 123.3(9) . . ?
C215 C216 H216 118.3 . . ?
C217 C216 H216 118.3 . . ?
O37 C217 C216 130.0(10) . . ?
O37 C217 C218 115.4(11) . . ?
C216 C217 C218 114.6(11) . . ?
F66 C218 F65 108.3(18) . . ?
F66 C218 F64 103.7(14) . . ?
F65 C218 F64 105.8(18) . . ?
F66 C218 C217 110.2(17) . . ?
F65 C218 C217 112.5(13) . . ?
F64 C218 C217 115.8(14) . . ?
F58 C219 F60 109.8(14) . . ?
F58 C219 F59 103.5(10) . . ?
F60 C219 F59 107.9(10) . . ?
F58 C219 C220 109.9(9) . . ?
F60 C219 C220 113.8(10) . . ?
F59 C219 C220 111.4(13) . . ?
O36 C220 C221 130.0(10) . . ?
O36 C220 C219 111.7(12) . . ?
C221 C220 C219 118.3(11) . . ?
C222 C221 C220 123.3(10) . . ?
C222 C221 H221 118.3 . . ?
C220 C221 H221 118.3 . . ?
O35 C222 C221 129.9(12) . . ?
O35 C222 C223 114.8(11) . . ?
C221 C222 C223 115.3(11) . . ?
F57 C223 F55 111.0(18) . . ?
F57 C223 F56 106.5(14) . . ?
F55 C223 F56 97.1(13) . . ?
F57 C223 C222 117.4(13) . . ?
F55 C223 C222 115.9(13) . . ?
F56 C223 C222 106.2(14) . . ?
F68 C224 F69 113.9(13) . . ?
F68 C224 F67 102.3(16) . . ?
F69 C224 F67 95.4(15) . . ?
F68 C224 C225 116.6(13) . . ?
F69 C224 C225 115.8(12) . . ?
F67 C224 C225 109.5(13) . . ?
O40 C225 C226 130.1(9) . . ?
O40 C225 C224 111.0(9) . . ?
C226 C225 C224 118.8(9) . . ?
C225 C226 C227 125.5(8) . . ?
C225 C226 H226 117.2 . . ?
C227 C226 H226 117.2 . . ?
O39 C227 C226 127.8(9) . . ?
O39 C227 C228 113.7(9) . . ?
C226 C227 C228 118.5(8) . . ?
F71 C228 F70 108(2) . . ?
F71 C228 F72 105.2(16) . . ?
F70 C228 F72 109.7(13) . . ?
F71A C228 F72A 108(2) . . ?
F71A C228 F70A 99(2) . . ?
F72A C228 F70A 105(3) . . ?
F71 C228 C227 107.1(13) . . ?
F70 C228 C227 115.2(11) . . ?
F72 C228 C227 111.3(10) . . ?
F71A C228 C227 121.0(14) . . ?
F72A C228 C227 113.8(13) . . ?
F70A C228 C227 107.4(16) . . ?

_refine_diff_density_max         1.537
_refine_diff_density_min         -1.543
_refine_diff_density_rms         0.120

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Complex5
_database_code_depnum_ccdc_archive 'CCDC 1584345'
_audit_update_record             
;
2017-11-07 deposited with the CCDC.
2018-03-05 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2014/7
_shelx_SHELXL_version_number     2014/7
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C88 H110 Ag19 F21 Mo O14'
_chemical_formula_weight         3936.22

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      orthorhombic
_space_group_IT_number           19
_space_group_name_H-M_alt        'P 21 21 21'
_space_group_name_Hall           'P 2ac 2ab'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'

_cell_length_a                   14.7978(17)
_cell_length_b                   25.140(3)
_cell_length_c                   32.296(4)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     12015(2)
_cell_formula_units_Z            4
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    9769
_cell_measurement_theta_min      2.8740
_cell_measurement_theta_max      26.8701

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    2.176
_exptl_crystal_F_000             7496
_exptl_transmission_factor_min   0.5868
_exptl_transmission_factor_max   0.7455
_exptl_crystal_size_max          0.278
_exptl_crystal_size_mid          0.206
_exptl_crystal_size_min          0.137
_exptl_absorpt_coefficient_mu    3.198
_shelx_estimated_absorpt_T_min   0.470
_shelx_estimated_absorpt_T_max   0.668
_exptl_absorpt_correction_type   Multi-scan
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   SADABS
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            65305
_diffrn_reflns_av_unetI/netI     0.0384
_diffrn_reflns_av_R_equivalents  0.0408
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_limit_l_max       35
_diffrn_reflns_theta_min         2.864
_diffrn_reflns_theta_max         23.255
_diffrn_reflns_theta_full        23.255
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measured_fraction_theta_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_point_group_measured_fraction_full 0.994
_reflns_number_total             17133
_reflns_number_gt                16432
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.838
_reflns_Friedel_fraction_max     0.997
_reflns_Friedel_fraction_full    0.997

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Apex2 (Bruker, 2014)'
_computing_cell_refinement       'SAINT (Bruker, 2014)'
_computing_data_reduction        'SAINT (Bruker, 2014)'
_computing_structure_solution    'SHELXTL XT-2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics    ?
_computing_publication_material  ?
_refine_special_details          
;
 Refined as a 2-component inversion twin.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0325P)²+819.4069P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.53(15)
_chemical_absolute_configuration ?
_refine_ls_number_reflns         17133
_refine_ls_number_parameters     1348
_refine_ls_number_restraints     1613
_refine_ls_R_factor_all          0.0964
_refine_ls_R_factor_gt           0.0927
_refine_ls_wR_factor_ref         0.2198
_refine_ls_wR_factor_gt          0.2172
_refine_ls_goodness_of_fit_ref   1.114
_refine_ls_restrained_S_all      1.089
_refine_ls_shift/su_max          0.012
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1A Ag 0.4728(2) 0.44354(17) 0.38377(11) 0.0329(10) Uani 0.881(11) 1 d . U P A
1
Ag1B Ag 0.491(2) 0.4130(19) 0.3819(9) 0.046(3) Uani 0.119(11) 1 d . U P A 2
Ag2A Ag 0.4813(2) 0.5707(2) 0.38359(11) 0.0352(11) Uani 0.880(13) 1 d . U P A 1
Ag2B Ag 0.4765(17) 0.540(2) 0.3826(9) 0.040(4) Uani 0.120(13) 1 d . U P A 2
Ag3A Ag 0.4664(2) 0.51411(14) 0.46207(9) 0.0367(9) Uani 0.902(8) 1 d . U P A 1
Ag3B Ag 0.475(2) 0.4679(15) 0.4600(9) 0.044(4) Uani 0.098(8) 1 d . U P A 2
Ag4A Ag 0.6121(3) 0.43723(15) 0.50862(12) 0.0495(12) Uani 0.877(8) 1 d . U P A
1
Ag4B Ag 0.6657(19) 0.4632(12) 0.5142(7) 0.043(4) Uani 0.123(8) 1 d . U P A 2
Ag5A Ag 0.623(2) 0.579(2) 0.5131(10) 0.045(5) Uani 0.112(15) 1 d . U P A 1
Ag5B Ag 0.6510(3) 0.5503(2) 0.51376(12) 0.0449(15) Uani 0.888(15) 1 d . U P A 2
Ag6A Ag 0.848(3) 0.606(3) 0.4873(13) 0.045(8) Uani 0.081(15) 1 d . U P A 1
Ag6B Ag 0.8600(2) 0.5773(2) 0.48045(12) 0.0391(11) Uani 0.919(15) 1 d . U P A 2
Ag7A Ag 0.8330(2) 0.40637(14) 0.48421(11) 0.0448(10) Uani 0.922(7) 1 d . U P A
1
Ag7B Ag 0.883(3) 0.4379(17) 0.4809(11) 0.040(4) Uani 0.078(7) 1 d . U P A 2
Ag8 Ag 0.9355(2) 0.43179(12) 0.36495(9) 0.0430(7) Uani 1 1 d . U . . .
Ag9 Ag 0.7000(2) 0.32851(12) 0.46147(11) 0.0505(8) Uani 1 1 d . U . . .
Ag10 Ag 0.8268(2) 0.34757(14) 0.39658(11) 0.0546(9) Uani 1 1 d . U . . .
Ag11 Ag 0.6281(2) 0.42781(14) 0.32545(10) 0.0540(9) Uani 1 1 d . U . . .
Ag12 Ag 0.95150(19) 0.48726(11) 0.44070(8) 0.0344(6) Uani 1 1 d . U . . .
Ag13 Ag 0.81074(17) 0.48870(13) 0.30037(8) 0.0398(7) Uani 1 1 d . U . . .
Ag14 Ag 0.9439(2) 0.54146(11) 0.36301(9) 0.0375(6) Uani 1 1 d . U . . .
Ag15 Ag 0.64540(19) 0.56416(13) 0.32307(9) 0.0403(7) Uani 1 1 d . U . . .
Ag16 Ag 0.6199(3) 0.33175(18) 0.37962(15) 0.0829(13) Uani 1 1 d . U . . .
Ag17 Ag 0.8524(2) 0.63222(13) 0.39556(11) 0.0513(8) Uani 1 1 d . U . . .
Ag18 Ag 0.7349(2) 0.65923(12) 0.46396(10) 0.0460(7) Uani 1 1 d . U . . .
Ag19 Ag 0.6556(2) 0.65447(15) 0.37911(11) 0.0589(9) Uani 1 1 d . U . . .
Mo Mo 0.71719(18) 0.49366(12) 0.41089(8) 0.0243(6) Uani 1 1 d . U . . .
F1 F 1.093(3) 0.7208(15) 0.3193(13) 0.149(15) Uani 1 1 d D U . . .
F2 F 1.1485(19) 0.6464(15) 0.3031(12) 0.130(14) Uani 1 1 d D U . . .
F3 F 1.0871(19) 0.6941(14) 0.2574(10) 0.110(12) Uani 1 1 d D U . . .
F4 F 0.787(2) 0.6830(12) 0.2221(9) 0.077(8) Uani 1 1 d . U . . .
F5 F 0.755(2) 0.6033(12) 0.2264(10) 0.088(9) Uani 1 1 d . U . . .
F6 F 0.6830(19) 0.6605(18) 0.2605(9) 0.107(12) Uani 1 1 d . U . . .
F7 F 1.122(3) 0.334(2) 0.3052(18) 0.156(16) Uani 1 1 d . U . . .
F8 F 1.077(4) 0.2560(18) 0.3192(16) 0.170(19) Uani 1 1 d . U . . .
F9 F 1.075(3) 0.285(2) 0.2616(13) 0.142(14) Uani 1 1 d . U . . .
F10 F 0.738(3) 0.3793(14) 0.2313(12) 0.097(10) Uani 1 1 d . U . . .
F11 F 0.772(3) 0.3017(15) 0.2227(11) 0.118(14) Uani 1 1 d . U . . .
F12 F 0.672(3) 0.328(2) 0.2640(14) 0.133(13) Uani 1 1 d . U . . .
F13 F 0.358(3) 0.2850(14) 0.4522(17) 0.19(2) Uani 1 1 d D U . . .
F14 F 0.367(4) 0.3427(19) 0.5101(12) 0.186(19) Uani 1 1 d D U . . .
F15 F 0.326(3) 0.3764(16) 0.4445(14) 0.166(19) Uani 1 1 d D U . . .
F16A F 1.082(3) 0.531(3) 0.579(2) 0.12(2) Uani 0.54(5) 1 d D U P B 1
F17A F 0.947(4) 0.522(3) 0.6048(19) 0.12(2) Uani 0.54(5) 1 d D U P B 1
F18A F 1.036(5) 0.453(2) 0.5993(19) 0.12(2) Uani 0.54(5) 1 d D U P B 1
F16B F 1.093(3) 0.478(3) 0.583(2) 0.100(19) Uani 0.46(5) 1 d D U P B 2
F17B F 1.016(6) 0.552(2) 0.585(2) 0.12(2) Uani 0.46(5) 1 d D U P B 2
F18B F 0.964(5) 0.481(4) 0.6148(16) 0.11(2) Uani 0.46(5) 1 d D U P B 2
F19 F 0.427(3) 0.674(2) 0.5175(14) 0.155(15) Uani 1 1 d . U . . .
F20 F 0.416(2) 0.7209(12) 0.4600(15) 0.119(12) Uani 1 1 d . U . . .
F21 F 0.379(2) 0.6414(13) 0.4623(12) 0.098(11) Uani 1 1 d . U . . .
O1 O 0.7639(15) 0.4969(10) 0.4618(6) 0.035(3) Uani 1 1 d . U . . .
O2 O 0.7604(17) 0.5519(10) 0.3835(8) 0.041(4) Uani 1 1 d . U . . .
O3 O 0.6003(14) 0.4990(10) 0.4129(7) 0.035(3) Uani 1 1 d . U . . .
O4 O 0.7418(16) 0.4371(10) 0.3851(8) 0.040(4) Uani 1 1 d . U . . .
O5 O 0.984(2) 0.6309(12) 0.3412(8) 0.057(6) Uani 1 1 d . U . . .
O6 O 0.8010(17) 0.6128(12) 0.3147(9) 0.049(7) Uani 1 1 d . U . . .
O7 O 0.5319(19) 0.3090(13) 0.4543(14) 0.087(7) Uani 1 1 d D U . . .
O8 O 0.512(2) 0.3943(12) 0.4557(9) 0.062(5) Uani 1 1 d D U . . .
O9 O 0.597(2) 0.6948(11) 0.4829(11) 0.065(6) Uani 1 1 d . U . . .
O10 O 0.5533(19) 0.6201(10) 0.4491(9) 0.049(5) Uani 1 1 d . U . . .
O11 O 0.791(3) 0.3662(14) 0.3168(9) 0.086(12) Uani 1 1 d . U . . .
O12 O 0.969(2) 0.3387(12) 0.3451(10) 0.062(6) Uani 1 1 d . U . . .
O13 O 0.913(3) 0.4402(17) 0.5414(9) 0.083(8) Uani 1 1 d . U . . .
O14 O 0.977(2) 0.5082(13) 0.5102(8) 0.065(6) Uani 1 1 d . U . . .
C1 C 0.724(3) 0.2836(18) 0.4072(15) 0.060(5) Uani 1 1 d . U . . .
C2 C 0.740(4) 0.2413(17) 0.3890(13) 0.064(9) Uani 1 1 d . U . . .
C3 C 0.757(4) 0.1912(18) 0.3696(14) 0.067(10) Uani 1 1 d . U . . .
C4 C 0.697(5) 0.1464(19) 0.388(2) 0.12(2) Uani 1 1 d . U . . .
H4A H 0.7098 0.1126 0.3745 0.180 Uiso 1 1 calc R U . . .
H4B H 0.7096 0.1430 0.4180 0.180 Uiso 1 1 calc R U . . .
H4C H 0.6328 0.1554 0.3845 0.180 Uiso 1 1 calc R U . . .
C5 C 0.853(5) 0.177(2) 0.376(2) 0.101(16) Uani 1 1 d . U . . .
H5A H 0.8651 0.1422 0.3631 0.151 Uiso 1 1 calc R U . . .
H5B H 0.8918 0.2039 0.3641 0.151 Uiso 1 1 calc R U . . .
H5C H 0.8648 0.1740 0.4060 0.151 Uiso 1 1 calc R U . . .
C6 C 0.746(6) 0.197(3) 0.3217(16) 0.12(2) Uani 1 1 d . U . . .
H6A H 0.7578 0.1630 0.3083 0.185 Uiso 1 1 calc R U . . .
H6B H 0.6848 0.2091 0.3152 0.185 Uiso 1 1 calc R U . . .
H6C H 0.7898 0.2237 0.3116 0.185 Uiso 1 1 calc R U . . .
C7 C 0.673(2) 0.4909(17) 0.2827(12) 0.044(4) Uani 1 1 d D U . . .
C8 C 0.602(2) 0.5003(17) 0.2664(11) 0.043(4) Uani 1 1 d D U . . .
C9 C 0.518(2) 0.4972(16) 0.2393(10) 0.072(8) Uani 1 1 d D U . . .
C10 C 0.433(2) 0.497(2) 0.2663(12) 0.089(15) Uani 1 1 d D U . . .
H10A H 0.3794 0.4953 0.2485 0.133 Uiso 1 1 calc R U . . .
H10B H 0.4342 0.4665 0.2849 0.133 Uiso 1 1 calc R U . . .
H10C H 0.4310 0.5301 0.2827 0.133 Uiso 1 1 calc R U . . .
C11 C 0.527(3) 0.5490(17) 0.2145(15) 0.087(14) Uani 1 1 d D U . . .
H11A H 0.4764 0.5523 0.1953 0.131 Uiso 1 1 calc R U . . .
H11B H 0.5277 0.5794 0.2335 0.131 Uiso 1 1 calc R U . . .
H11C H 0.5840 0.5483 0.1987 0.131 Uiso 1 1 calc R U . . .
C12 C 0.522(3) 0.4485(17) 0.2110(13) 0.072(8) Uani 1 1 d D U . . .
H12A H 0.4675 0.4472 0.1938 0.108 Uiso 1 1 calc R U . . .
H12B H 0.5754 0.4510 0.1931 0.108 Uiso 1 1 calc R U . . .
H12C H 0.5259 0.4162 0.2278 0.108 Uiso 1 1 calc R U . . .
C13 C 0.767(3) 0.7008(17) 0.4043(15) 0.052(5) Uani 1 1 d . U . . .
C14 C 0.770(3) 0.7393(18) 0.3869(15) 0.059(9) Uani 1 1 d . U . . .
C15 C 0.783(4) 0.7930(19) 0.3648(17) 0.073(10) Uani 1 1 d . U . . .
C16 C 0.876(5) 0.812(3) 0.370(2) 0.109(19) Uani 1 1 d . U . . .
H16A H 0.9179 0.7865 0.3578 0.163 Uiso 1 1 calc R U . . .
H16B H 0.8826 0.8467 0.3565 0.163 Uiso 1 1 calc R U . . .
H16C H 0.8889 0.8158 0.3998 0.163 Uiso 1 1 calc R U . . .
C17 C 0.716(5) 0.830(2) 0.3830(19) 0.094(16) Uani 1 1 d . U . . .
H17A H 0.6548 0.8164 0.3788 0.141 Uiso 1 1 calc R U . . .
H17B H 0.7276 0.8343 0.4127 0.141 Uiso 1 1 calc R U . . .
H17C H 0.7213 0.8652 0.3695 0.141 Uiso 1 1 calc R U . . .
C18 C 0.751(4) 0.785(2) 0.3211(16) 0.082(15) Uani 1 1 d . U . . .
H18A H 0.6886 0.7726 0.3213 0.122 Uiso 1 1 calc R U . . .
H18B H 0.7545 0.8193 0.3063 0.122 Uiso 1 1 calc R U . . .
H18C H 0.7898 0.7592 0.3073 0.122 Uiso 1 1 calc R U . . .
C19 C 0.517(3) 0.3761(17) 0.3439(14) 0.049(4) Uani 1 1 d . U . . .
C20 C 0.476(3) 0.3373(16) 0.3345(12) 0.054(7) Uani 1 1 d D U . . .
C21 C 0.423(2) 0.2945(14) 0.3185(12) 0.061(9) Uani 1 1 d D U . . .
C22 C 0.393(4) 0.308(2) 0.2739(13) 0.14(2) Uani 1 1 d D U . . .
H22A H 0.3564 0.2789 0.2628 0.207 Uiso 1 1 calc R U . . .
H22B H 0.3576 0.3409 0.2740 0.207 Uiso 1 1 calc R U . . .
H22C H 0.4469 0.3128 0.2565 0.207 Uiso 1 1 calc R U . . .
C23 C 0.338(3) 0.2868(16) 0.3447(18) 0.096(19) Uani 1 1 d D U . . .
H23A H 0.3017 0.2575 0.3333 0.144 Uiso 1 1 calc R U . . .
H23B H 0.3548 0.2785 0.3733 0.144 Uiso 1 1 calc R U . . .
H23C H 0.3017 0.3196 0.3443 0.144 Uiso 1 1 calc R U . . .
C24 C 0.475(4) 0.2424(14) 0.318(2) 0.14(2) Uani 1 1 d D U . . .
H24A H 0.4362 0.2141 0.3065 0.209 Uiso 1 1 calc R U . . .
H24B H 0.5283 0.2464 0.2999 0.209 Uiso 1 1 calc R U . . .
H24C H 0.4940 0.2331 0.3457 0.209 Uiso 1 1 calc R U . . .
C26 C 0.479(4) 0.351(2) 0.462(2) 0.077(7) Uani 1 1 d . U . . .
C27 C 0.3838(19) 0.3392(13) 0.4651(12) 0.092(10) Uani 1 1 d D U . . .
C31 C 0.547(3) 0.6241(15) 0.3409(12) 0.040(4) Uani 1 1 d . U . . .
C32 C 0.485(3) 0.6503(16) 0.3355(12) 0.041(7) Uani 1 1 d . U . . .
C33 C 0.412(3) 0.689(2) 0.3215(16) 0.064(10) Uani 1 1 d . U . . .
C34 C 0.335(3) 0.678(3) 0.3538(18) 0.085(15) Uani 1 1 d . U . . .
H34A H 0.3584 0.6850 0.3818 0.127 Uiso 1 1 calc R U . . .
H34B H 0.2843 0.7021 0.3482 0.127 Uiso 1 1 calc R U . . .
H34C H 0.3154 0.6413 0.3516 0.127 Uiso 1 1 calc R U . . .
C35 C 0.447(5) 0.745(2) 0.325(2) 0.104(19) Uani 1 1 d . U . . .
H35A H 0.4757 0.7497 0.3516 0.157 Uiso 1 1 calc R U . . .
H35B H 0.4909 0.7510 0.3026 0.157 Uiso 1 1 calc R U . . .
H35C H 0.3963 0.7696 0.3218 0.157 Uiso 1 1 calc R U . . .
C36 C 0.368(3) 0.678(3) 0.2822(18) 0.091(16) Uani 1 1 d . U . . .
H36A H 0.3467 0.6406 0.2821 0.137 Uiso 1 1 calc R U . . .
H36B H 0.3160 0.7014 0.2786 0.137 Uiso 1 1 calc R U . . .
H36C H 0.4106 0.6829 0.2594 0.137 Uiso 1 1 calc R U . . .
C37 C 0.966(3) 0.5723(15) 0.4255(11) 0.038(3) Uani 1 1 d . U . . .
C38 C 1.003(3) 0.6117(15) 0.4436(12) 0.041(5) Uani 1 1 d . U . . .
C39 C 1.058(3) 0.6514(19) 0.4585(14) 0.078(13) Uani 1 1 d D U . . .
C40 C 1.080(6) 0.644(4) 0.5046(17) 0.21(4) Uiso 1 1 d D U . . .
H40A H 1.1186 0.6725 0.5141 0.316 Uiso 1 1 calc R U . . .
H40B H 1.0232 0.6437 0.5205 0.316 Uiso 1 1 calc R U . . .
H40C H 1.1105 0.6095 0.5085 0.316 Uiso 1 1 calc R U . . .
C41 C 1.003(4) 0.704(2) 0.456(2) 0.12(2) Uiso 1 1 d D U . . .
H41A H 1.0404 0.7330 0.4664 0.174 Uiso 1 1 calc R U . . .
H41B H 0.9867 0.7105 0.4272 0.174 Uiso 1 1 calc R U . . .
H41C H 0.9487 0.7003 0.4729 0.174 Uiso 1 1 calc R U . . .
C42 C 1.147(4) 0.662(3) 0.436(2) 0.13(3) Uiso 1 1 d D U . . .
H42A H 1.1791 0.6908 0.4502 0.198 Uiso 1 1 calc R U . . .
H42B H 1.1843 0.6294 0.4373 0.198 Uiso 1 1 calc R U . . .
H42C H 1.1353 0.6713 0.4075 0.198 Uiso 1 1 calc R U . . .
C43 C 0.713(3) 0.3707(17) 0.5157(14) 0.052(4) Uani 1 1 d . U . . .
C44 C 0.707(3) 0.3817(17) 0.5542(13) 0.047(6) Uani 1 1 d . U . . .
C45 C 0.715(3) 0.3827(16) 0.5970(13) 0.074(10) Uani 1 1 d D U . . .
C46 C 0.722(4) 0.4395(18) 0.6137(16) 0.096(16) Uani 1 1 d D U . . .
H46A H 0.7271 0.4385 0.6440 0.144 Uiso 1 1 calc R U . . .
H46B H 0.7746 0.4571 0.6019 0.144 Uiso 1 1 calc R U . . .
H46C H 0.6669 0.4592 0.6061 0.144 Uiso 1 1 calc R U . . .
C47 C 0.798(4) 0.354(2) 0.6146(15) 0.12(2) Uani 1 1 d D U . . .
H47A H 0.7978 0.3571 0.6449 0.178 Uiso 1 1 calc R U . . .
H47B H 0.7965 0.3166 0.6066 0.178 Uiso 1 1 calc R U . . .
H47C H 0.8531 0.3707 0.6037 0.178 Uiso 1 1 calc R U . . .
C48 C 0.636(4) 0.358(2) 0.620(2) 0.15(3) Uani 1 1 d D U . . .
H48A H 0.6467 0.3604 0.6503 0.225 Uiso 1 1 calc R U . . .
H48B H 0.5801 0.3775 0.6136 0.225 Uiso 1 1 calc R U . . .
H48C H 0.6289 0.3207 0.6125 0.225 Uiso 1 1 calc R U . . .
C49 C 0.386(2) 0.5139(16) 0.4065(11) 0.041(4) Uani 1 1 d . U . . .
C50 C 0.319(2) 0.4940(18) 0.3886(12) 0.049(6) Uani 1 1 d . U . . .
C51 C 0.231(3) 0.486(3) 0.371(2) 0.092(8) Uani 1 1 d . U . . .
C52 C 0.191(3) 0.534(2) 0.351(2) 0.092(8) Uani 1 1 d . U . . .
H52A H 0.2361 0.5508 0.3327 0.138 Uiso 1 1 calc R U . . .
H52B H 0.1380 0.5241 0.3347 0.138 Uiso 1 1 calc R U . . .
H52C H 0.1732 0.5600 0.3724 0.138 Uiso 1 1 calc R U . . .
C53 C 0.242(3) 0.439(2) 0.338(2) 0.092(8) Uani 1 1 d . U . . .
H53A H 0.2797 0.4512 0.3147 0.138 Uiso 1 1 calc R U . . .
H53B H 0.2695 0.4082 0.3510 0.138 Uiso 1 1 calc R U . . .
H53C H 0.1818 0.4292 0.3270 0.138 Uiso 1 1 calc R U . . .
C54 C 0.174(3) 0.457(2) 0.399(2) 0.092(8) Uani 1 1 d . U . . .
H54A H 0.1145 0.4524 0.3864 0.138 Uiso 1 1 calc R U . . .
H54B H 0.2014 0.4224 0.4044 0.138 Uiso 1 1 calc R U . . .
H54C H 0.1683 0.4770 0.4249 0.138 Uiso 1 1 calc R U . . .
C55 C 0.534(2) 0.5073(16) 0.5236(11) 0.040(3) Uani 1 1 d . U . . .
C56 C 0.456(2) 0.5057(17) 0.5361(11) 0.043(6) Uani 1 1 d . U . . .
C57 C 0.363(3) 0.509(2) 0.5578(13) 0.062(9) Uani 1 1 d . U . . .
C58 C 0.302(4) 0.466(3) 0.535(2) 0.12(2) Uani 1 1 d . U . . .
H58A H 0.2980 0.4741 0.5056 0.184 Uiso 1 1 calc R U . . .
H58B H 0.3288 0.4302 0.5385 0.184 Uiso 1 1 calc R U . . .
H58C H 0.2413 0.4659 0.5473 0.184 Uiso 1 1 calc R U . . .
C59 C 0.375(4) 0.501(4) 0.6006(15) 0.12(2) Uani 1 1 d . U . . .
H59A H 0.4141 0.4703 0.6055 0.186 Uiso 1 1 calc R U . . .
H59B H 0.4034 0.5330 0.6125 0.186 Uiso 1 1 calc R U . . .
H59C H 0.3163 0.4954 0.6137 0.186 Uiso 1 1 calc R U . . .
C60 C 0.304(4) 0.556(3) 0.546(2) 0.13(2) Uani 1 1 d . U . . .
H60A H 0.2995 0.5576 0.5156 0.189 Uiso 1 1 calc R U . . .
H60B H 0.2436 0.5508 0.5576 0.189 Uiso 1 1 calc R U . . .
H60C H 0.3307 0.5885 0.5565 0.189 Uiso 1 1 calc R U . . .
C61 C 0.765(3) 0.6110(16) 0.5212(13) 0.044(4) Uani 1 1 d . U . . .
C62 C 0.736(2) 0.6177(15) 0.5553(12) 0.037(5) Uani 1 1 d . U . . .
C63 C 0.713(3) 0.6325(14) 0.6001(14) 0.065(10) Uani 1 1 d D U . . .
C64 C 0.609(3) 0.635(3) 0.603(2) 0.13(2) Uani 1 1 d D U . . .
H64A H 0.5845 0.5989 0.6001 0.194 Uiso 1 1 calc R U . . .
H64B H 0.5920 0.6491 0.6303 0.194 Uiso 1 1 calc R U . . .
H64C H 0.5856 0.6578 0.5813 0.194 Uiso 1 1 calc R U . . .
C65 C 0.753(5) 0.589(3) 0.6275(19) 0.16(3) Uani 1 1 d D U . . .
H65A H 0.7200 0.5554 0.6229 0.236 Uiso 1 1 calc R U . . .
H65B H 0.8167 0.5837 0.6203 0.236 Uiso 1 1 calc R U . . .
H65C H 0.7479 0.5991 0.6566 0.236 Uiso 1 1 calc R U . . .
C66 C 0.758(5) 0.686(2) 0.605(2) 0.16(3) Uani 1 1 d D U . . .
H66A H 0.8238 0.6812 0.6023 0.240 Uiso 1 1 calc R U . . .
H66B H 0.7370 0.7097 0.5828 0.240 Uiso 1 1 calc R U . . .
H66C H 0.7435 0.7009 0.6318 0.240 Uiso 1 1 calc R U . . .
C67 C 0.946(3) 0.3997(15) 0.4265(13) 0.045(4) Uani 1 1 d . U . . .
C68 C 0.979(3) 0.3632(15) 0.4469(15) 0.054(5) Uani 1 1 d . U . . .
C69 C 1.033(4) 0.3143(18) 0.4694(15) 0.095(14) Uani 1 1 d D U . . .
C70 C 1.133(4) 0.331(3) 0.469(3) 0.21(3) Uani 1 1 d D U . . .
H70A H 1.1412 0.3626 0.4859 0.315 Uiso 1 1 calc R U . . .
H70B H 1.1700 0.3017 0.4803 0.315 Uiso 1 1 calc R U . . .
H70C H 1.1520 0.3381 0.4405 0.315 Uiso 1 1 calc R U . . .
C71 C 1.014(6) 0.265(2) 0.444(2) 0.20(3) Uani 1 1 d D U . . .
H71A H 0.9497 0.2560 0.4451 0.294 Uiso 1 1 calc R U . . .
H71B H 1.0314 0.2710 0.4148 0.294 Uiso 1 1 calc R U . . .
H71C H 1.0494 0.2346 0.4546 0.294 Uiso 1 1 calc R U . . .
C72 C 0.995(5) 0.311(3) 0.5135(16) 0.16(3) Uani 1 1 d D U . . .
H72A H 1.0091 0.3435 0.5286 0.240 Uiso 1 1 calc R U . . .
H72B H 0.9293 0.3061 0.5122 0.240 Uiso 1 1 calc R U . . .
H72C H 1.0221 0.2803 0.5279 0.240 Uiso 1 1 calc R U . . .
C73 C 0.956(2) 0.4851(17) 0.3130(10) 0.041(4) Uani 1 1 d . U . . .
C74 C 0.975(2) 0.4830(16) 0.2744(11) 0.040(7) Uani 1 1 d . U . . .
C75 C 1.007(3) 0.484(2) 0.2318(14) 0.069(11) Uani 1 1 d . U . . .
C76 C 1.090(5) 0.527(3) 0.2307(17) 0.13(2) Uani 1 1 d . U . . .
H76A H 1.1142 0.5293 0.2025 0.192 Uiso 1 1 calc R U . . .
H76B H 1.0680 0.5621 0.2393 0.192 Uiso 1 1 calc R U . . .
H76C H 1.1380 0.5154 0.2496 0.192 Uiso 1 1 calc R U . . .
C77 C 0.953(6) 0.522(4) 0.2056(17) 0.15(3) Uani 1 1 d . U . . .
H77A H 0.9768 0.5221 0.1773 0.227 Uiso 1 1 calc R U . . .
H77B H 0.8897 0.5107 0.2053 0.227 Uiso 1 1 calc R U . . .
H77C H 0.9570 0.5581 0.2171 0.227 Uiso 1 1 calc R U . . .
C78 C 1.038(7) 0.431(3) 0.216(3) 0.17(3) Uani 1 1 d . U . . .
H78A H 1.0592 0.4343 0.1878 0.262 Uiso 1 1 calc R U . . .
H78B H 1.0874 0.4180 0.2340 0.262 Uiso 1 1 calc R U . . .
H78C H 0.9874 0.4059 0.2176 0.262 Uiso 1 1 calc R U . . .
C79 C 0.428(4) 0.6749(19) 0.4761(19) 0.075(9) Uani 1 1 d . U . . .
C80 C 0.536(3) 0.6628(14) 0.4668(17) 0.059(7) Uani 1 1 d . U . . .
C81 C 0.768(3) 0.648(2) 0.2478(14) 0.054(7) Uani 1 1 d . U . . .
C82 C 0.836(2) 0.6380(15) 0.2825(11) 0.037(6) Uani 1 1 d . U . . .
C83 C 0.920(3) 0.6598(15) 0.2772(11) 0.038(7) Uani 1 1 d . U . . .
H83 H 0.9318 0.6793 0.2526 0.046 Uiso 1 1 calc R U . . .
C84 C 0.991(3) 0.6544(16) 0.3078(14) 0.049(8) Uani 1 1 d . U . . .
C85 C 1.072(2) 0.6764(13) 0.2969(9) 0.084(10) Uani 1 1 d D U . . .
C86 C 0.750(4) 0.336(2) 0.2515(16) 0.066(8) Uani 1 1 d . U . . .
C87 C 0.810(3) 0.3419(19) 0.2852(12) 0.057(9) Uani 1 1 d . U . . .
C88 C 0.901(3) 0.3229(18) 0.2788(15) 0.056(8) Uani 1 1 d . U . . .
H88 H 0.9184 0.3112 0.2520 0.067 Uiso 1 1 calc R U . . .
C89 C 0.961(3) 0.3213(18) 0.3094(15) 0.058(8) Uani 1 1 d D U . . .
C90 C 1.059(3) 0.301(2) 0.300(2) 0.083(10) Uani 1 1 d D U . . .
C91 C 0.965(3) 0.483(2) 0.5390(14) 0.070(8) Uani 1 1 d . U . . .
C92 C 1.007(2) 0.4977(18) 0.5792(11) 0.082(10) Uani 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1A C19 2.23(4) . ?
Ag1A C49 2.30(4) . ?
Ag1A O3 2.53(2) . ?
Ag1A C50 2.61(4) . ?
Ag1A Ag11 2.998(5) . ?
Ag1A Ag3A 3.091(5) . ?
Ag1A Ag2A 3.199(7) . ?
Ag1B C19 1.59(6) . ?
Ag1B O8 2.45(4) . ?
Ag1B C20 2.45(6) . ?
Ag1B Ag11 2.75(3) . ?
Ag1B Ag16 2.79(5) . ?
Ag1B Ag3B 2.89(5) . ?
Ag1B Ag2B 3.19(7) . ?
Ag2A C49 2.14(4) . ?
Ag2A C31 2.16(4) . ?
Ag2A C32 2.53(4) . ?
Ag2A Ag3A 2.915(5) . ?
Ag2A Ag15 3.121(4) . ?
Ag2A Ag19 3.332(6) . ?
Ag2B C49 1.67(5) . ?
Ag2B O3 2.31(4) . ?
Ag2B C50 2.60(5) . ?
Ag2B Ag3B 3.08(5) . ?
Ag2B Ag15 3.21(3) . ?
Ag3A C49 2.15(4) . ?
Ag3A C55 2.23(3) . ?
Ag3A C56 2.40(3) . ?
Ag3A O3 2.57(2) . ?
Ag3A Ag4A 3.263(5) . ?
Ag3A Ag5A 3.28(3) . ?
Ag3B O8 1.94(5) . ?
Ag3B C55 2.44(5) . ?
Ag3B C49 2.46(5) . ?
Ag3B O3 2.53(4) . ?
Ag3B C56 2.65(5) . ?
Ag3B Ag4B 3.33(4) . ?
Ag4A C55 2.17(4) . ?
Ag4A C43 2.25(4) . ?
Ag4A C44 2.47(4) . ?
Ag4A O8 2.50(3) . ?
Ag4B Ag5B 2.20(3) . ?
Ag4B C55 2.27(4) . ?
Ag4B O1 2.39(3) . ?
Ag4B C43 2.43(5) . ?
Ag4B C44 2.50(5) . ?
Ag5A C61 2.26(5) . ?
Ag5A C55 2.27(5) . ?
Ag5A C62 2.36(5) . ?
Ag5A O10 2.53(5) . ?
Ag5A Ag18 3.05(3) . ?
Ag5B C55 2.07(4) . ?
Ag5B C61 2.29(4) . ?
Ag5B C62 2.50(4) . ?
Ag5B Ag6B 3.343(5) . ?
Ag6A C61 1.65(6) . ?
Ag6A Ag18 2.27(6) . ?
Ag6A C38 2.70(6) . ?
Ag6A Ag17 3.03(4) . ?
Ag6B C61 2.10(4) . ?
Ag6B C37 2.37(4) . ?
Ag6B O1 2.54(2) . ?
Ag6B C38 2.58(4) . ?
Ag6B Ag18 2.821(6) . ?
Ag6B Ag12 2.933(6) . ?
Ag6B Ag17 3.072(5) . ?
Ag7A C43 2.23(4) . ?
Ag7A O13 2.35(3) . ?
Ag7A C67 2.51(4) . ?
Ag7A O1 2.60(3) . ?
Ag7A C68 2.71(5) . ?
Ag7A Ag9 2.871(5) . ?
Ag7A Ag12 3.031(4) . ?
Ag7A Ag10 3.194(5) . ?
Ag7B O13 2.01(5) . ?
Ag7B Ag12 2.06(4) . ?
Ag7B C67 2.21(6) . ?
Ag7B O1 2.38(4) . ?
Ag7B O14 2.44(5) . ?
Ag7B C91 2.51(6) . ?
Ag7B C68 2.60(6) . ?
Ag8 C67 2.15(4) . ?
Ag8 C73 2.17(4) . ?
Ag8 O12 2.48(3) . ?
Ag8 Ag14 2.761(4) . ?
Ag8 Ag12 2.826(4) . ?
Ag8 Ag10 2.849(5) . ?
Ag8 Ag13 3.132(4) . ?
Ag9 C43 2.06(5) . ?
Ag9 C1 2.11(5) . ?
Ag9 O7 2.55(3) . ?
Ag9 Ag10 2.853(5) . ?
Ag9 Ag16 2.898(6) . ?
Ag10 C1 2.24(5) . ?
Ag10 C67 2.40(4) . ?
Ag10 Ag16 3.136(6) . ?
Ag11 C19 2.17(4) . ?
Ag11 C7 2.20(4) . ?
Ag11 O4 2.57(3) . ?
Ag11 C8 2.66(4) . ?
Ag11 Ag16 2.985(6) . ?
Ag11 Ag13 3.210(4) . ?
Ag12 C37 2.20(4) . ?
Ag12 C67 2.25(4) . ?
Ag12 O14 2.34(3) . ?
Ag12 Ag14 2.857(4) . ?
Ag13 C7 2.12(3) . ?
Ag13 C73 2.19(4) . ?
Ag13 C74 2.57(4) . ?
Ag13 Ag14 3.121(4) . ?
Ag13 Ag15 3.182(4) . ?
Ag14 C73 2.16(4) . ?
Ag14 C37 2.19(4) . ?
Ag14 O5 2.43(3) . ?
Ag14 Ag17 2.854(4) . ?
Ag15 C31 2.17(4) . ?
Ag15 C7 2.29(4) . ?
Ag15 C8 2.52(4) . ?
Ag15 Ag19 2.907(5) . ?
Ag16 C1 2.15(5) . ?
Ag16 C19 2.21(5) . ?
Ag16 C20 2.58(4) . ?
Ag17 C13 2.16(4) . ?
Ag17 C37 2.45(4) . ?
Ag17 O2 2.47(2) . ?
Ag17 Ag18 2.892(5) . ?
Ag17 Ag19 3.013(5) . ?
Ag18 C13 2.24(5) . ?
Ag18 C61 2.25(4) . ?
Ag18 O9 2.31(3) . ?
Ag18 Ag19 2.983(5) . ?
Ag19 C31 2.16(4) . ?
Ag19 C13 2.17(4) . ?
Mo O4 1.69(2) . ?
Mo O3 1.74(2) . ?
Mo O1 1.79(2) . ?
Mo O2 1.83(2) . ?
F1 C85 1.37(2) . ?
F2 C85 1.37(2) . ?
F3 C85 1.37(2) . ?
F4 C81 1.24(5) . ?
F5 C81 1.33(6) . ?
F6 C81 1.36(5) . ?
F7 C90 1.25(7) . ?
F8 C90 1.32(7) . ?
F9 C90 1.33(7) . ?
F10 C86 1.28(6) . ?
F11 C86 1.31(6) . ?
F12 C86 1.24(6) . ?
F13 C27 1.47(3) . ?
F14 C27 1.48(3) . ?
F15 C27 1.44(3) . ?
F16A C92 1.40(3) . ?
F17A C92 1.36(3) . ?
F18A C92 1.37(3) . ?
F16B C92 1.38(3) . ?
F17B C92 1.38(3) . ?
F18B C92 1.37(3) . ?
F19 C79 1.34(7) . ?
F20 C79 1.28(7) . ?
F21 C79 1.20(5) . ?
O5 C84 1.24(5) . ?
O6 C82 1.32(4) . ?
O7 C26 1.34(6) . ?
O8 C26 1.21(5) . ?
O9 C80 1.32(5) . ?
O10 C80 1.25(5) . ?
O11 C87 1.22(5) . ?
O12 C89 1.24(5) . ?
O13 C91 1.32(6) . ?
O14 C91 1.14(5) . ?
C1 C2 1.24(6) . ?
C2 C3 1.43(6) . ?
C3 C5 1.48(8) . ?
C3 C4 1.56(7) . ?
C3 C6 1.56(7) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.19(3) . ?
C8 C9 1.52(5) . ?
C9 C10 1.53(3) . ?
C9 C12 1.53(3) . ?
C9 C11 1.54(3) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C14 1.12(6) . ?
C14 C15 1.54(6) . ?
C15 C16 1.46(8) . ?
C15 C17 1.49(8) . ?
C15 C18 1.50(7) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C20 1.19(6) . ?
C20 C21 1.43(6) . ?
C21 C24 1.52(3) . ?
C21 C23 1.53(3) . ?
C21 C22 1.54(3) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 H23C 0.9800 . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C26 C27 1.45(6) . ?
C31 C32 1.14(5) . ?
C32 C33 1.52(5) . ?
C33 C36 1.46(7) . ?
C33 C35 1.49(8) . ?
C33 C34 1.57(7) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 H35C 0.9800 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 H36C 0.9800 . ?
C37 C38 1.28(5) . ?
C38 C39 1.37(6) . ?
C39 C42 1.52(3) . ?
C39 C40 1.54(3) . ?
C39 C41 1.54(3) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 H40C 0.9800 . ?
C41 H41A 0.9800 . ?
C41 H41B 0.9800 . ?
C41 H41C 0.9800 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 H42C 0.9800 . ?
C43 C44 1.28(6) . ?
C44 C45 1.39(6) . ?
C45 C47 1.53(3) . ?
C45 C46 1.53(3) . ?
C45 C48 1.53(3) . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 H46C 0.9800 . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C49 C50 1.25(5) . ?
C50 C51 1.44(5) . ?
C51 C54 1.43(8) . ?
C51 C52 1.49(8) . ?
C51 C53 1.61(9) . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 H53A 0.9800 . ?
C53 H53B 0.9800 . ?
C53 H53C 0.9800 . ?
C54 H54A 0.9800 . ?
C54 H54B 0.9800 . ?
C54 H54C 0.9800 . ?
C55 C56 1.21(5) . ?
C56 C57 1.55(5) . ?
C57 C59 1.41(6) . ?
C57 C60 1.52(8) . ?
C57 C58 1.59(7) . ?
C58 H58A 0.9800 . ?
C58 H58B 0.9800 . ?
C58 H58C 0.9800 . ?
C59 H59A 0.9800 . ?
C59 H59B 0.9800 . ?
C59 H59C 0.9800 . ?
C60 H60A 0.9800 . ?
C60 H60B 0.9800 . ?
C60 H60C 0.9800 . ?
C61 C62 1.19(5) . ?
C62 C63 1.54(6) . ?
C63 C66 1.51(3) . ?
C63 C64 1.53(3) . ?
C63 C65 1.53(3) . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C65 H65A 0.9800 . ?
C65 H65B 0.9800 . ?
C65 H65C 0.9800 . ?
C66 H66A 0.9800 . ?
C66 H66B 0.9800 . ?
C66 H66C 0.9800 . ?
C67 C68 1.23(6) . ?
C68 C69 1.64(6) . ?
C69 C71 1.53(3) . ?
C69 C70 1.53(3) . ?
C69 C72 1.54(3) . ?
C70 H70A 0.9800 . ?
C70 H70B 0.9800 . ?
C70 H70C 0.9800 . ?
C71 H71A 0.9800 . ?
C71 H71B 0.9800 . ?
C71 H71C 0.9800 . ?
C72 H72A 0.9800 . ?
C72 H72B 0.9800 . ?
C72 H72C 0.9800 . ?
C73 C74 1.28(5) . ?
C74 C75 1.46(5) . ?
C75 C78 1.50(8) . ?
C75 C77 1.50(7) . ?
C75 C76 1.63(8) . ?
C76 H76A 0.9800 . ?
C76 H76B 0.9800 . ?
C76 H76C 0.9800 . ?
C77 H77A 0.9800 . ?
C77 H77B 0.9800 . ?
C77 H77C 0.9800 . ?
C78 H78A 0.9800 . ?
C78 H78B 0.9800 . ?
C78 H78C 0.9800 . ?
C79 C80 1.64(7) . ?
C81 C82 1.53(6) . ?
C82 C83 1.36(5) . ?
C83 C84 1.45(5) . ?
C83 H83 0.9500 . ?
C84 C85 1.36(6) . ?
C86 C87 1.41(7) . ?
C87 C88 1.45(6) . ?
C88 C89 1.33(7) . ?
C88 H88 0.9500 . ?
C89 C90 1.57(3) . ?
C91 C92 1.49(6) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C19 Ag1A C49 158.8(15) . . ?
C19 Ag1A O3 114.4(12) . . ?
C49 Ag1A O3 82.7(11) . . ?
C19 Ag1A C50 131.5(15) . . ?
C49 Ag1A C50 28.7(13) . . ?
O3 Ag1A C50 111.1(11) . . ?
C19 Ag1A Ag11 46.3(11) . . ?
C49 Ag1A Ag11 136.7(10) . . ?
O3 Ag1A Ag11 74.6(5) . . ?
C50 Ag1A Ag11 140.3(8) . . ?
C19 Ag1A Ag3A 156.7(12) . . ?
C49 Ag1A Ag3A 44.1(9) . . ?
O3 Ag1A Ag3A 53.2(5) . . ?
C50 Ag1A Ag3A 69.2(10) . . ?
Ag11 Ag1A Ag3A 127.83(13) . . ?
C19 Ag1A Ag2A 138.3(11) . . ?
C49 Ag1A Ag2A 41.9(9) . . ?
O3 Ag1A Ag2A 54.6(6) . . ?
C50 Ag1A Ag2A 63.1(9) . . ?
Ag11 Ag1A Ag2A 95.76(13) . . ?
Ag3A Ag1A Ag2A 55.18(12) . . ?
C19 Ag1B O8 128(3) . . ?
C19 Ag1B C20 23.8(19) . . ?
O8 Ag1B C20 118(2) . . ?
C19 Ag1B Ag11 52.1(17) . . ?
O8 Ag1B Ag11 125.2(15) . . ?
C20 Ag1B Ag11 75.9(13) . . ?
C19 Ag1B Ag16 52(2) . . ?
O8 Ag1B Ag16 78.4(15) . . ?
C20 Ag1B Ag16 58.4(14) . . ?
Ag11 Ag1B Ag16 65.1(8) . . ?
C19 Ag1B Ag3B 168(3) . . ?
O8 Ag1B Ag3B 41.6(11) . . ?
C20 Ag1B Ag3B 155.5(19) . . ?
Ag11 Ag1B Ag3B 125.2(12) . . ?
Ag16 Ag1B Ag3B 115.6(14) . . ?
C19 Ag1B Ag2B 127(2) . . ?
O8 Ag1B Ag2B 101.1(14) . . ?
C20 Ag1B Ag2B 140.6(18) . . ?
Ag11 Ag1B Ag2B 85.4(11) . . ?
Ag16 Ag1B Ag2B 140.9(10) . . ?
Ag3B Ag1B Ag2B 60.7(12) . . ?
C49 Ag2A C31 159.1(15) . . ?
C49 Ag2A C32 138.9(13) . . ?
C31 Ag2A C32 26.7(13) . . ?
C49 Ag2A Ag3A 47.4(10) . . ?
C31 Ag2A Ag3A 153.3(11) . . ?
C32 Ag2A Ag3A 157.0(9) . . ?
C49 Ag2A Ag15 133.9(11) . . ?
C31 Ag2A Ag15 44.0(10) . . ?
C32 Ag2A Ag15 68.9(9) . . ?
Ag3A Ag2A Ag15 125.30(15) . . ?
C49 Ag2A Ag1A 46.0(11) . . ?
C31 Ag2A Ag1A 129.8(10) . . ?
C32 Ag2A Ag1A 142.3(9) . . ?
Ag3A Ag2A Ag1A 60.52(13) . . ?
Ag15 Ag2A Ag1A 88.81(14) . . ?
C49 Ag2A Ag19 161.3(10) . . ?
C31 Ag2A Ag19 39.6(11) . . ?
C32 Ag2A Ag19 57.1(9) . . ?
Ag3A Ag2A Ag19 113.89(14) . . ?
Ag15 Ag2A Ag19 53.43(10) . . ?
Ag1A Ag2A Ag19 131.47(14) . . ?
C49 Ag2B O3 106(2) . . ?
C49 Ag2B C50 23.1(16) . . ?
O3 Ag2B C50 119(2) . . ?
C49 Ag2B Ag3B 52.6(17) . . ?
O3 Ag2B Ag3B 53.6(11) . . ?
C50 Ag2B Ag3B 70.9(13) . . ?
C49 Ag2B Ag1B 71(2) . . ?
O3 Ag2B Ag1B 60.6(13) . . ?
C50 Ag2B Ag1B 67.7(16) . . ?
Ag3B Ag2B Ag1B 54.7(11) . . ?
C49 Ag2B Ag15 166(3) . . ?
O3 Ag2B Ag15 73.9(9) . . ?
C50 Ag2B Ag15 145.5(16) . . ?
Ag3B Ag2B Ag15 127.2(11) . . ?
Ag1B Ag2B Ag15 97.7(11) . . ?
C49 Ag3A C55 171.8(14) . . ?
C49 Ag3A C56 142.7(13) . . ?
C55 Ag3A C56 30.0(12) . . ?
C49 Ag3A O3 84.8(11) . . ?
C55 Ag3A O3 101.3(10) . . ?
C56 Ag3A O3 130.5(11) . . ?
C49 Ag3A Ag2A 47.0(10) . . ?
C55 Ag3A Ag2A 141.2(10) . . ?
C56 Ag3A Ag2A 155.8(10) . . ?
O3 Ag3A Ag2A 58.4(5) . . ?
C49 Ag3A Ag1A 48.1(11) . . ?
C55 Ag3A Ag1A 132.2(10) . . ?
C56 Ag3A Ag1A 139.9(10) . . ?
O3 Ag3A Ag1A 52.1(5) . . ?
Ag2A Ag3A Ag1A 64.30(13) . . ?
C49 Ag3A Ag4A 138.3(11) . . ?
C55 Ag3A Ag4A 41.3(10) . . ?
C56 Ag3A Ag4A 62.0(10) . . ?
O3 Ag3A Ag4A 71.7(5) . . ?
Ag2A Ag3A Ag4A 129.75(14) . . ?
Ag1A Ag3A Ag4A 90.95(13) . . ?
C49 Ag3A Ag5A 144.0(13) . . ?
C55 Ag3A Ag5A 43.6(12) . . ?
C56 Ag3A Ag5A 65.7(11) . . ?
O3 Ag3A Ag5A 80.7(9) . . ?
Ag2A Ag3A Ag5A 98.0(7) . . ?
Ag1A Ag3A Ag5A 132.5(8) . . ?
Ag4A Ag3A Ag5A 66.3(9) . . ?
O8 Ag3B C55 110.0(19) . . ?
O8 Ag3B C49 123.6(19) . . ?
C55 Ag3B C49 126(2) . . ?
O8 Ag3B O3 92.3(16) . . ?
C55 Ag3B O3 96.7(14) . . ?
C49 Ag3B O3 79.8(14) . . ?
O8 Ag3B C56 115.9(19) . . ?
C55 Ag3B C56 27.2(12) . . ?
C49 Ag3B C56 115.5(19) . . ?
O3 Ag3B C56 121.5(15) . . ?
O8 Ag3B Ag1B 57.1(16) . . ?
C55 Ag3B Ag1B 154.0(17) . . ?
C49 Ag3B Ag1B 69.9(15) . . ?
O3 Ag3B Ag1B 63.9(10) . . ?
C56 Ag3B Ag1B 172.3(19) . . ?
O8 Ag3B Ag2B 119.9(18) . . ?
C55 Ag3B Ag2B 116.2(18) . . ?
C49 Ag3B Ag2B 32.8(11) . . ?
O3 Ag3B Ag2B 47.5(9) . . ?
C56 Ag3B Ag2B 122.9(18) . . ?
Ag1B Ag3B Ag2B 64.6(14) . . ?
O8 Ag3B Ag4B 76.0(14) . . ?
C55 Ag3B Ag4B 42.9(11) . . ?
C49 Ag3B Ag4B 147.1(16) . . ?
O3 Ag3B Ag4B 72.6(10) . . ?
C56 Ag3B Ag4B 67.1(11) . . ?
Ag1B Ag3B Ag4B 111.7(14) . . ?
Ag2B Ag3B Ag4B 116.1(12) . . ?
C55 Ag4A C43 159.5(15) . . ?
C55 Ag4A C44 129.2(13) . . ?
C43 Ag4A C44 30.9(14) . . ?
C55 Ag4A O8 100.8(12) . . ?
C43 Ag4A O8 98.0(15) . . ?
C44 Ag4A O8 120.0(13) . . ?
C55 Ag4A Ag3A 42.8(9) . . ?
C43 Ag4A Ag3A 157.5(12) . . ?
C44 Ag4A Ag3A 170.5(9) . . ?
O8 Ag4A Ag3A 63.3(7) . . ?
Ag5B Ag4B C55 55.2(12) . . ?
Ag5B Ag4B O1 72.6(10) . . ?
C55 Ag4B O1 116.5(16) . . ?
Ag5B Ag4B C43 168.9(18) . . ?
C55 Ag4B C43 136(2) . . ?
O1 Ag4B C43 100.3(15) . . ?
Ag5B Ag4B C44 147.6(16) . . ?
C55 Ag4B C44 123.0(18) . . ?
O1 Ag4B C44 120.5(15) . . ?
C43 Ag4B C44 30.0(14) . . ?
Ag5B Ag4B Ag3B 82.9(10) . . ?
C55 Ag4B Ag3B 47.2(12) . . ?
O1 Ag4B Ag3B 97.5(11) . . ?
C43 Ag4B Ag3B 106.8(16) . . ?
C44 Ag4B Ag3B 120.7(16) . . ?
C61 Ag5A C55 144(3) . . ?
C61 Ag5A C62 29.8(13) . . ?
C55 Ag5A C62 131(2) . . ?
C61 Ag5A O10 109.3(19) . . ?
C55 Ag5A O10 102.0(15) . . ?
C62 Ag5A O10 127(2) . . ?
C61 Ag5A Ag18 47.5(13) . . ?
C55 Ag5A Ag18 157.1(18) . . ?
C62 Ag5A Ag18 69.3(12) . . ?
O10 Ag5A Ag18 61.9(11) . . ?
C61 Ag5A Ag3A 153(2) . . ?
C55 Ag5A Ag3A 42.7(10) . . ?
C62 Ag5A Ag3A 173(2) . . ?
O10 Ag5A Ag3A 60.2(9) . . ?
Ag18 Ag5A Ag3A 116.8(10) . . ?
C55 Ag5B Ag4B 64.0(13) . . ?
C55 Ag5B C61 161.9(14) . . ?
Ag4B Ag5B C61 126.2(13) . . ?
C55 Ag5B C62 133.9(13) . . ?
Ag4B Ag5B C62 128.4(11) . . ?
C61 Ag5B C62 28.5(13) . . ?
C55 Ag5B Ag6B 158.7(11) . . ?
Ag4B Ag5B Ag6B 96.5(8) . . ?
C61 Ag5B Ag6B 38.4(10) . . ?
C62 Ag5B Ag6B 64.5(8) . . ?
C61 Ag6A Ag18 68(3) . . ?
C61 Ag6A C38 168(3) . . ?
Ag18 Ag6A C38 115(2) . . ?
C61 Ag6A Ag17 130(3) . . ?
Ag18 Ag6A Ag17 64.2(11) . . ?
C38 Ag6A Ag17 57.3(12) . . ?
C61 Ag6B C37 158.6(15) . . ?
C61 Ag6B O1 95.4(12) . . ?
C37 Ag6B O1 98.6(10) . . ?
C61 Ag6B C38 134.6(14) . . ?
C37 Ag6B C38 29.5(12) . . ?
O1 Ag6B C38 128.1(10) . . ?
C61 Ag6B Ag18 52.0(12) . . ?
C37 Ag6B Ag18 109.3(10) . . ?
O1 Ag6B Ag18 99.7(6) . . ?
C38 Ag6B Ag18 102.0(9) . . ?
C61 Ag6B Ag12 153.3(12) . . ?
C37 Ag6B Ag12 47.7(9) . . ?
O1 Ag6B Ag12 62.7(5) . . ?
C38 Ag6B Ag12 71.2(9) . . ?
Ag18 Ag6B Ag12 141.62(16) . . ?
C61 Ag6B Ag17 110.6(12) . . ?
C37 Ag6B Ag17 51.6(9) . . ?
O1 Ag6B Ag17 97.2(5) . . ?
C38 Ag6B Ag17 57.8(9) . . ?
Ag18 Ag6B Ag17 58.60(12) . . ?
Ag12 Ag6B Ag17 88.46(14) . . ?
C61 Ag6B Ag5B 42.5(11) . . ?
C37 Ag6B Ag5B 147.2(9) . . ?
O1 Ag6B Ag5B 53.0(5) . . ?
C38 Ag6B Ag5B 167.5(10) . . ?
Ag18 Ag6B Ag5B 66.55(16) . . ?
Ag12 Ag6B Ag5B 114.28(19) . . ?
Ag17 Ag6B Ag5B 110.16(15) . . ?
C43 Ag7A O13 100.7(15) . . ?
C43 Ag7A C67 147.2(16) . . ?
O13 Ag7A C67 106.0(14) . . ?
C43 Ag7A O1 99.5(12) . . ?
O13 Ag7A O1 95.7(11) . . ?
C67 Ag7A O1 96.5(10) . . ?
C43 Ag7A C68 132.7(14) . . ?
O13 Ag7A C68 95.4(15) . . ?
C67 Ag7A C68 27.0(12) . . ?
O1 Ag7A C68 122.9(9) . . ?
C43 Ag7A Ag9 45.4(12) . . ?
O13 Ag7A Ag9 142.3(9) . . ?
C67 Ag7A Ag9 102.7(10) . . ?
O1 Ag7A Ag9 104.9(5) . . ?
C68 Ag7A Ag9 99.3(9) . . ?
C43 Ag7A Ag12 160.1(11) . . ?
O13 Ag7A Ag12 80.3(9) . . ?
C67 Ag7A Ag12 46.8(9) . . ?
O1 Ag7A Ag12 60.7(5) . . ?
C68 Ag7A Ag12 66.4(8) . . ?
Ag9 Ag7A Ag12 137.35(15) . . ?
C43 Ag7A Ag10 101.2(12) . . ?
O13 Ag7A Ag10 151.5(10) . . ?
C67 Ag7A Ag10 47.9(10) . . ?
O1 Ag7A Ag10 98.5(5) . . ?
C68 Ag7A Ag10 56.1(11) . . ?
Ag9 Ag7A Ag10 55.82(11) . . ?
Ag12 Ag7A Ag10 85.20(12) . . ?
O13 Ag7B Ag12 119(2) . . ?
O13 Ag7B C67 134(3) . . ?
Ag12 Ag7B C67 63.5(15) . . ?
O13 Ag7B O1 113(2) . . ?
Ag12 Ag7B O1 80.0(14) . . ?
C67 Ag7B O1 112.1(19) . . ?
O13 Ag7B O14 58.4(16) . . ?
Ag12 Ag7B O14 61.8(13) . . ?
C67 Ag7B O14 113(2) . . ?
O1 Ag7B O14 94.1(17) . . ?
O13 Ag7B C91 31.7(16) . . ?
Ag12 Ag7B C91 87.8(19) . . ?
C67 Ag7B C91 126(2) . . ?
O1 Ag7B C91 106(2) . . ?
O14 Ag7B C91 26.7(14) . . ?
O13 Ag7B C68 108(2) . . ?
Ag12 Ag7B C68 84.2(16) . . ?
C67 Ag7B C68 28.2(15) . . ?
O1 Ag7B C68 138(2) . . ?
O14 Ag7B C68 112(2) . . ?
C91 Ag7B C68 112(2) . . ?
C67 Ag8 C73 159.7(16) . . ?
C67 Ag8 O12 82.6(13) . . ?
C73 Ag8 O12 110.8(12) . . ?
C67 Ag8 Ag14 113.1(11) . . ?
C73 Ag8 Ag14 50.1(10) . . ?
O12 Ag8 Ag14 158.2(8) . . ?
C67 Ag8 Ag12 51.6(11) . . ?
C73 Ag8 Ag12 110.7(10) . . ?
O12 Ag8 Ag12 132.4(8) . . ?
Ag14 Ag8 Ag12 61.51(10) . . ?
C67 Ag8 Ag10 55.2(12) . . ?
C73 Ag8 Ag10 144.6(11) . . ?
O12 Ag8 Ag10 60.3(8) . . ?
Ag14 Ag8 Ag10 140.88(15) . . ?
Ag12 Ag8 Ag10 95.94(13) . . ?
C67 Ag8 Ag13 145.9(12) . . ?
C73 Ag8 Ag13 44.3(10) . . ?
O12 Ag8 Ag13 112.2(8) . . ?
Ag14 Ag8 Ag13 63.59(11) . . ?
Ag12 Ag8 Ag13 113.60(12) . . ?
Ag10 Ag8 Ag13 104.20(14) . . ?
C43 Ag9 C1 165.0(19) . . ?
C43 Ag9 O7 105.5(16) . . ?
C1 Ag9 O7 89.1(17) . . ?
C43 Ag9 Ag10 118.5(12) . . ?
C1 Ag9 Ag10 51.1(13) . . ?
O7 Ag9 Ag10 127.4(10) . . ?
C43 Ag9 Ag7A 50.7(12) . . ?
C1 Ag9 Ag7A 117.5(13) . . ?
O7 Ag9 Ag7A 145.5(8) . . ?
Ag10 Ag9 Ag7A 67.84(12) . . ?
C43 Ag9 Ag16 143.1(12) . . ?
C1 Ag9 Ag16 47.7(13) . . ?
O7 Ag9 Ag16 61.5(10) . . ?
Ag10 Ag9 Ag16 66.09(15) . . ?
Ag7A Ag9 Ag16 119.65(16) . . ?
C1 Ag10 C67 146.0(15) . . ?
C1 Ag10 Ag8 166.4(12) . . ?
C67 Ag10 Ag8 47.5(9) . . ?
C1 Ag10 Ag9 47.2(13) . . ?
C67 Ag10 Ag9 106.1(10) . . ?
Ag8 Ag10 Ag9 139.43(15) . . ?
C1 Ag10 Ag16 43.3(13) . . ?
C67 Ag10 Ag16 148.9(10) . . ?
Ag8 Ag10 Ag16 125.67(17) . . ?
Ag9 Ag10 Ag16 57.65(13) . . ?
C1 Ag10 Ag7A 102.5(13) . . ?
C67 Ag10 Ag7A 50.8(10) . . ?
Ag8 Ag10 Ag7A 87.57(12) . . ?
Ag9 Ag10 Ag7A 56.34(11) . . ?
Ag16 Ag10 Ag7A 103.96(15) . . ?
C19 Ag11 C7 145.8(15) . . ?
C19 Ag11 O4 110.1(13) . . ?
C7 Ag11 O4 102.1(11) . . ?
C19 Ag11 C8 119.8(14) . . ?
C7 Ag11 C8 26.1(8) . . ?
O4 Ag11 C8 124.6(10) . . ?
C19 Ag11 Ag1B 35.2(14) . . ?
C7 Ag11 Ag1B 137.1(14) . . ?
O4 Ag11 Ag1B 89.9(8) . . ?
C8 Ag11 Ag1B 117.5(12) . . ?
C19 Ag11 Ag16 47.5(12) . . ?
C7 Ag11 Ag16 164.2(8) . . ?
O4 Ag11 Ag16 70.2(6) . . ?
C8 Ag11 Ag16 165.2(8) . . ?
Ag1B Ag11 Ag16 58.1(10) . . ?
C19 Ag11 Ag1A 47.9(11) . . ?
C7 Ag11 Ag1A 121.8(9) . . ?
O4 Ag11 Ag1A 91.1(5) . . ?
C8 Ag11 Ag1A 104.4(8) . . ?
Ag16 Ag11 Ag1A 72.96(15) . . ?
C19 Ag11 Ag13 171.3(12) . . ?
C7 Ag11 Ag13 41.2(8) . . ?
O4 Ag11 Ag13 66.1(6) . . ?
C8 Ag11 Ag13 67.3(7) . . ?
Ag1B Ag11 Ag13 148.4(7) . . ?
Ag16 Ag11 Ag13 124.64(17) . . ?
Ag1A Ag11 Ag13 137.83(15) . . ?
Ag7B Ag12 C37 140.4(15) . . ?
Ag7B Ag12 C67 61.3(16) . . ?
C37 Ag12 C67 155.2(13) . . ?
Ag7B Ag12 O14 67.1(14) . . ?
C37 Ag12 O14 88.8(12) . . ?
C67 Ag12 O14 115.0(13) . . ?
Ag7B Ag12 Ag8 101.9(11) . . ?
C37 Ag12 Ag8 107.1(9) . . ?
C67 Ag12 Ag8 48.5(10) . . ?
O14 Ag12 Ag8 163.0(8) . . ?
Ag7B Ag12 Ag14 145.1(10) . . ?
C37 Ag12 Ag14 49.1(9) . . ?
C67 Ag12 Ag14 106.6(10) . . ?
O14 Ag12 Ag14 137.9(8) . . ?
Ag8 Ag12 Ag14 58.12(9) . . ?
Ag7B Ag12 Ag6B 87.8(12) . . ?
C37 Ag12 Ag6B 52.6(10) . . ?
C67 Ag12 Ag6B 145.7(11) . . ?
O14 Ag12 Ag6B 58.7(8) . . ?
Ag8 Ag12 Ag6B 136.14(13) . . ?
Ag14 Ag12 Ag6B 89.91(12) . . ?
C37 Ag12 Ag7A 144.0(10) . . ?
C67 Ag12 Ag7A 54.2(11) . . ?
O14 Ag12 Ag7A 78.5(8) . . ?
Ag8 Ag12 Ag7A 91.26(12) . . ?
Ag14 Ag12 Ag7A 134.78(13) . . ?
C7 Ag13 C73 175.1(14) . . ?
C7 Ag13 C74 145.4(13) . . ?
C73 Ag13 C74 29.8(12) . . ?
C7 Ag13 Ag14 140.5(11) . . ?
C73 Ag13 Ag14 43.7(10) . . ?
C74 Ag13 Ag14 68.8(8) . . ?
C7 Ag13 Ag8 139.3(11) . . ?
C73 Ag13 Ag8 43.8(10) . . ?
C74 Ag13 Ag8 68.6(8) . . ?
Ag14 Ag13 Ag8 52.40(9) . . ?
C7 Ag13 Ag15 46.0(11) . . ?
C73 Ag13 Ag15 137.4(10) . . ?
C74 Ag13 Ag15 146.5(9) . . ?
Ag14 Ag13 Ag15 94.75(11) . . ?
Ag8 Ag13 Ag15 124.92(11) . . ?
C7 Ag13 Ag11 43.1(11) . . ?
C73 Ag13 Ag11 139.4(11) . . ?
C74 Ag13 Ag11 148.2(9) . . ?
Ag14 Ag13 Ag11 124.81(12) . . ?
Ag8 Ag13 Ag11 96.34(12) . . ?
Ag15 Ag13 Ag11 65.09(10) . . ?
C73 Ag14 C37 155.9(14) . . ?
C73 Ag14 O5 111.8(13) . . ?
C37 Ag14 O5 84.5(12) . . ?
C73 Ag14 Ag8 50.5(11) . . ?
C37 Ag14 Ag8 109.9(10) . . ?
O5 Ag14 Ag8 160.4(8) . . ?
C73 Ag14 Ag17 147.1(9) . . ?
C37 Ag14 Ag17 56.4(10) . . ?
O5 Ag14 Ag17 58.8(8) . . ?
Ag8 Ag14 Ag17 140.23(15) . . ?
C73 Ag14 Ag12 110.0(10) . . ?
C37 Ag14 Ag12 49.7(10) . . ?
O5 Ag14 Ag12 133.3(7) . . ?
Ag8 Ag14 Ag12 60.37(10) . . ?
Ag17 Ag14 Ag12 94.38(12) . . ?
C73 Ag14 Ag13 44.5(10) . . ?
C37 Ag14 Ag13 147.4(10) . . ?
O5 Ag14 Ag13 111.0(7) . . ?
Ag8 Ag14 Ag13 64.01(11) . . ?
Ag17 Ag14 Ag13 106.19(13) . . ?
Ag12 Ag14 Ag13 113.03(12) . . ?
C31 Ag15 C7 145.7(13) . . ?
C31 Ag15 C8 117.8(13) . . ?
C7 Ag15 C8 28.1(7) . . ?
C31 Ag15 Ag19 47.7(11) . . ?
C7 Ag15 Ag19 166.5(7) . . ?
C8 Ag15 Ag19 164.6(8) . . ?
C31 Ag15 Ag2A 43.7(10) . . ?
C7 Ag15 Ag2A 122.3(9) . . ?
C8 Ag15 Ag2A 107.0(8) . . ?
Ag19 Ag15 Ag2A 67.00(13) . . ?
C31 Ag15 Ag13 171.7(11) . . ?
C7 Ag15 Ag13 41.8(7) . . ?
C8 Ag15 Ag13 69.3(7) . . ?
Ag19 Ag15 Ag13 124.71(13) . . ?
Ag2A Ag15 Ag13 140.71(15) . . ?
C31 Ag15 Ag2B 56.9(13) . . ?
C7 Ag15 Ag2B 108.8(13) . . ?
C8 Ag15 Ag2B 96.6(11) . . ?
Ag19 Ag15 Ag2B 79.5(8) . . ?
Ag13 Ag15 Ag2B 128.4(8) . . ?
C1 Ag16 C19 172.7(17) . . ?
C1 Ag16 C20 148.6(15) . . ?
C19 Ag16 C20 27.4(14) . . ?
C1 Ag16 Ag1B 152.6(14) . . ?
C19 Ag16 Ag1B 34.6(12) . . ?
C20 Ag16 Ag1B 54.1(11) . . ?
C1 Ag16 Ag9 46.7(13) . . ?
C19 Ag16 Ag9 140.6(11) . . ?
C20 Ag16 Ag9 148.6(8) . . ?
Ag1B Ag16 Ag9 106.0(6) . . ?
C1 Ag16 Ag11 132.0(13) . . ?
C19 Ag16 Ag11 46.6(11) . . ?
C20 Ag16 Ag11 70.1(9) . . ?
Ag1B Ag16 Ag11 56.8(7) . . ?
Ag9 Ag16 Ag11 122.72(18) . . ?
C1 Ag16 Ag10 45.6(13) . . ?
C19 Ag16 Ag10 134.3(11) . . ?
C20 Ag16 Ag10 153.6(9) . . ?
Ag1B Ag16 Ag10 124.7(6) . . ?
Ag9 Ag16 Ag10 56.27(12) . . ?
Ag11 Ag16 Ag10 87.69(16) . . ?
C13 Ag17 C37 147.2(15) . . ?
C13 Ag17 O2 110.5(13) . . ?
C37 Ag17 O2 86.4(11) . . ?
C13 Ag17 Ag14 164.9(13) . . ?
C37 Ag17 Ag14 47.9(9) . . ?
O2 Ag17 Ag14 63.2(6) . . ?
C13 Ag17 Ag18 50.2(12) . . ?
C37 Ag17 Ag18 104.7(9) . . ?
O2 Ag17 Ag18 88.9(6) . . ?
Ag14 Ag17 Ag18 138.97(15) . . ?
C13 Ag17 Ag19 46.1(11) . . ?
C37 Ag17 Ag19 147.6(9) . . ?
O2 Ag17 Ag19 65.8(6) . . ?
Ag14 Ag17 Ag19 122.84(15) . . ?
Ag18 Ag17 Ag19 60.65(12) . . ?
C13 Ag17 Ag6A 91.8(19) . . ?
C37 Ag17 Ag6A 59.9(16) . . ?
O2 Ag17 Ag6A 88.0(14) . . ?
Ag14 Ag17 Ag6A 101.5(15) . . ?
Ag18 Ag17 Ag6A 44.9(13) . . ?
Ag19 Ag17 Ag6A 101.0(9) . . ?
C13 Ag17 Ag6B 105.3(13) . . ?
C37 Ag17 Ag6B 49.2(9) . . ?
O2 Ag17 Ag6B 78.0(6) . . ?
Ag14 Ag17 Ag6B 87.24(15) . . ?
Ag18 Ag17 Ag6B 56.36(13) . . ?
Ag19 Ag17 Ag6B 106.03(14) . . ?
C13 Ag18 C61 156.0(15) . . ?
C13 Ag18 Ag6A 113.9(16) . . ?
C61 Ag18 Ag6A 42.7(15) . . ?
C13 Ag18 O9 103.4(14) . . ?
C61 Ag18 O9 99.6(14) . . ?
Ag6A Ag18 O9 142.3(15) . . ?
C13 Ag18 Ag6B 111.4(11) . . ?
C61 Ag18 Ag6B 47.4(10) . . ?
O9 Ag18 Ag6B 144.4(9) . . ?
C13 Ag18 Ag17 47.7(11) . . ?
C61 Ag18 Ag17 112.4(10) . . ?
Ag6A Ag18 Ag17 70.9(12) . . ?
O9 Ag18 Ag17 145.5(9) . . ?
Ag6B Ag18 Ag17 65.04(12) . . ?
C13 Ag18 Ag19 46.5(11) . . ?
C61 Ag18 Ag19 144.0(10) . . ?
Ag6A Ag18 Ag19 124.9(15) . . ?
O9 Ag18 Ag19 84.9(9) . . ?
Ag6B Ag18 Ag19 113.73(15) . . ?
Ag17 Ag18 Ag19 61.68(12) . . ?
C13 Ag18 Ag5A 150.3(13) . . ?
C61 Ag18 Ag5A 47.6(12) . . ?
Ag6A Ag18 Ag5A 80.8(15) . . ?
O9 Ag18 Ag5A 68.8(13) . . ?
Ag17 Ag18 Ag5A 124.7(10) . . ?
Ag19 Ag18 Ag5A 103.8(6) . . ?
C31 Ag19 C13 164.5(16) . . ?
C31 Ag19 Ag15 48.0(10) . . ?
C13 Ag19 Ag15 133.6(12) . . ?
C31 Ag19 Ag18 146.1(10) . . ?
C13 Ag19 Ag18 48.5(12) . . ?
Ag15 Ag19 Ag18 128.56(16) . . ?
C31 Ag19 Ag17 138.7(10) . . ?
C13 Ag19 Ag17 45.7(11) . . ?
Ag15 Ag19 Ag17 90.84(14) . . ?
Ag18 Ag19 Ag17 57.67(11) . . ?
C31 Ag19 Ag2A 39.5(10) . . ?
C13 Ag19 Ag2A 155.2(13) . . ?
Ag15 Ag19 Ag2A 59.57(11) . . ?
Ag18 Ag19 Ag2A 106.85(15) . . ?
Ag17 Ag19 Ag2A 128.53(16) . . ?
O4 Mo O3 107.4(12) . . ?
O4 Mo O1 114.2(12) . . ?
O3 Mo O1 110.3(10) . . ?
O4 Mo O2 111.1(12) . . ?
O3 Mo O2 107.8(12) . . ?
O1 Mo O2 105.9(11) . . ?
Mo O1 Ag4B 113.7(12) . . ?
Mo O1 Ag7B 119.7(15) . . ?
Ag4B O1 Ag7B 92.6(14) . . ?
Mo O1 Ag6B 118.1(11) . . ?
Ag4B O1 Ag6B 117.0(11) . . ?
Ag7B O1 Ag6B 91.2(12) . . ?
Mo O1 Ag7A 111.6(11) . . ?
Mo O2 Ag17 140.7(13) . . ?
Mo O3 Ag2B 143.7(16) . . ?
Mo O3 Ag3B 137.2(14) . . ?
Ag2B O3 Ag3B 78.9(13) . . ?
Mo O3 Ag1A 133.4(12) . . ?
Mo O3 Ag3A 143.5(12) . . ?
Ag1A O3 Ag3A 74.7(6) . . ?
Mo O4 Ag11 107.8(11) . . ?
C84 O5 Ag14 136(3) . . ?
C26 O7 Ag9 113(3) . . ?
C26 O8 Ag3B 137(4) . . ?
C26 O8 Ag1B 107(4) . . ?
Ag3B O8 Ag1B 81.3(18) . . ?
C26 O8 Ag4A 121(3) . . ?
C80 O9 Ag18 105(2) . . ?
C80 O10 Ag5A 93(3) . . ?
C89 O12 Ag8 124(3) . . ?
C91 O13 Ag7B 95(3) . . ?
C91 O13 Ag7A 123(3) . . ?
C91 O14 Ag12 129(3) . . ?
C91 O14 Ag7B 80(3) . . ?
Ag12 O14 Ag7B 51.1(10) . . ?
C2 C1 Ag9 152(4) . . ?
C2 C1 Ag16 115(4) . . ?
Ag9 C1 Ag16 85.6(18) . . ?
C2 C1 Ag10 114(4) . . ?
Ag9 C1 Ag10 81.8(15) . . ?
Ag16 C1 Ag10 91.1(18) . . ?
C1 C2 C3 177(5) . . ?
C2 C3 C5 109(5) . . ?
C2 C3 C4 112(5) . . ?
C5 C3 C4 108(5) . . ?
C2 C3 C6 109(4) . . ?
C5 C3 C6 105(6) . . ?
C4 C3 C6 114(6) . . ?
C3 C4 H4A 109.5 . . ?
C3 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C3 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C3 C5 H5A 109.5 . . ?
C3 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C3 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C3 C6 H6A 109.5 . . ?
C3 C6 H6B 109.5 . . ?
H6A C6 H6B 109.5 . . ?
C3 C6 H6C 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C8 C7 Ag13 165(4) . . ?
C8 C7 Ag11 99(3) . . ?
Ag13 C7 Ag11 95.8(14) . . ?
C8 C7 Ag15 87(3) . . ?
Ag13 C7 Ag15 92.1(14) . . ?
Ag11 C7 Ag15 99.8(15) . . ?
C7 C8 C9 164(4) . . ?
C7 C8 Ag15 65(3) . . ?
C9 C8 Ag15 131(3) . . ?
C7 C8 Ag11 55(2) . . ?
C9 C8 Ag11 120(3) . . ?
Ag15 C8 Ag11 83.1(10) . . ?
C8 C9 C10 110(3) . . ?
C8 C9 C12 111(3) . . ?
C10 C9 C12 112(2) . . ?
C8 C9 C11 101(3) . . ?
C10 C9 C11 112(2) . . ?
C12 C9 C11 111(2) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 Ag17 127(4) . . ?
C14 C13 Ag19 108(4) . . ?
Ag17 C13 Ag19 88.2(16) . . ?
C14 C13 Ag18 147(4) . . ?
Ag17 C13 Ag18 82.2(15) . . ?
Ag19 C13 Ag18 85.0(15) . . ?
C13 C14 C15 174(5) . . ?
C16 C15 C17 112(5) . . ?
C16 C15 C18 117(5) . . ?
C17 C15 C18 104(5) . . ?
C16 C15 C14 111(5) . . ?
C17 C15 C14 107(5) . . ?
C18 C15 C14 106(4) . . ?
C15 C16 H16A 109.5 . . ?
C15 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C15 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C15 C17 H17A 109.5 . . ?
C15 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C15 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C15 C18 H18A 109.5 . . ?
C15 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C15 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C20 C19 Ag1B 123(4) . . ?
C20 C19 Ag11 144(4) . . ?
Ag1B C19 Ag11 93(2) . . ?
C20 C19 Ag16 94(3) . . ?
Ag1B C19 Ag16 93(3) . . ?
Ag11 C19 Ag16 85.8(16) . . ?
C20 C19 Ag1A 128(4) . . ?
Ag11 C19 Ag1A 85.8(14) . . ?
Ag16 C19 Ag1A 106.6(18) . . ?
C19 C20 C21 172(4) . . ?
C19 C20 Ag1B 33(3) . . ?
C21 C20 Ag1B 149(2) . . ?
C19 C20 Ag16 59(3) . . ?
C21 C20 Ag16 128(2) . . ?
Ag1B C20 Ag16 67.4(14) . . ?
C20 C21 C24 112(3) . . ?
C20 C21 C23 111(3) . . ?
C24 C21 C23 109(2) . . ?
C20 C21 C22 109(2) . . ?
C24 C21 C22 108(3) . . ?
C23 C21 C22 108(3) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
C21 C23 H23A 109.5 . . ?
C21 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C21 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C21 C24 H24A 109.5 . . ?
C21 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C21 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
O8 C26 O7 116(5) . . ?
O8 C26 C27 127(5) . . ?
O7 C26 C27 114(4) . . ?
F15 C27 C26 115(4) . . ?
F15 C27 F13 109(2) . . ?
C26 C27 F13 115(3) . . ?
F15 C27 F14 109(2) . . ?
C26 C27 F14 102(4) . . ?
F13 C27 F14 107(2) . . ?
C32 C31 Ag2A 95(3) . . ?
C32 C31 Ag19 119(3) . . ?
Ag2A C31 Ag19 100.9(16) . . ?
C32 C31 Ag15 154(4) . . ?
Ag2A C31 Ag15 92.3(14) . . ?
Ag19 C31 Ag15 84.3(14) . . ?
C31 C32 C33 169(4) . . ?
C31 C32 Ag2A 58(3) . . ?
C33 C32 Ag2A 132(3) . . ?
C36 C33 C35 114(5) . . ?
C36 C33 C32 117(4) . . ?
C35 C33 C32 110(4) . . ?
C36 C33 C34 103(4) . . ?
C35 C33 C34 111(5) . . ?
C32 C33 C34 102(4) . . ?
C33 C34 H34A 109.5 . . ?
C33 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
C33 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
C33 C35 H35A 109.5 . . ?
C33 C35 H35B 109.5 . . ?
H35A C35 H35B 109.5 . . ?
C33 C35 H35C 109.5 . . ?
H35A C35 H35C 109.5 . . ?
H35B C35 H35C 109.5 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
C38 C37 Ag14 140(3) . . ?
C38 C37 Ag12 134(3) . . ?
Ag14 C37 Ag12 81.2(13) . . ?
C38 C37 Ag6B 85(3) . . ?
Ag14 C37 Ag6B 127.8(17) . . ?
Ag12 C37 Ag6B 79.7(12) . . ?
C38 C37 Ag17 90(3) . . ?
Ag14 C37 Ag17 75.7(12) . . ?
Ag12 C37 Ag17 128.2(16) . . ?
Ag6B C37 Ag17 79.1(12) . . ?
C37 C38 C39 169(4) . . ?
C37 C38 Ag6B 66(2) . . ?
C39 C38 Ag6B 124(3) . . ?
C37 C38 Ag6A 80(3) . . ?
C39 C38 Ag6A 111(3) . . ?
C38 C39 C42 118(5) . . ?
C38 C39 C40 112(6) . . ?
C42 C39 C40 107(3) . . ?
C38 C39 C41 107(5) . . ?
C42 C39 C41 107(3) . . ?
C40 C39 C41 105(3) . . ?
C39 C40 H40A 109.5 . . ?
C39 C40 H40B 109.5 . . ?
H40A C40 H40B 109.5 . . ?
C39 C40 H40C 109.5 . . ?
H40A C40 H40C 109.5 . . ?
H40B C40 H40C 109.5 . . ?
C39 C41 H41A 109.5 . . ?
C39 C41 H41B 109.5 . . ?
H41A C41 H41B 109.5 . . ?
C39 C41 H41C 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
C39 C42 H42A 109.5 . . ?
C39 C42 H42B 109.5 . . ?
H42A C42 H42B 109.5 . . ?
C39 C42 H42C 109.5 . . ?
H42A C42 H42C 109.5 . . ?
H42B C42 H42C 109.5 . . ?
C44 C43 Ag9 159(4) . . ?
C44 C43 Ag7A 114(4) . . ?
Ag9 C43 Ag7A 83.9(15) . . ?
C44 C43 Ag4A 84(3) . . ?
Ag9 C43 Ag4A 103.6(19) . . ?
Ag7A C43 Ag4A 100.5(16) . . ?
C44 C43 Ag4B 78(3) . . ?
Ag9 C43 Ag4B 117(2) . . ?
C43 C44 C45 166(4) . . ?
C43 C44 Ag4A 65(3) . . ?
C45 C44 Ag4A 129(3) . . ?
C43 C44 Ag4B 72(3) . . ?
C45 C44 Ag4B 121(3) . . ?
C44 C45 C47 116(4) . . ?
C44 C45 C46 112(4) . . ?
C47 C45 C46 105(3) . . ?
C44 C45 C48 115(5) . . ?
C47 C45 C48 104(3) . . ?
C46 C45 C48 104(3) . . ?
C45 C46 H46A 109.5 . . ?
C45 C46 H46B 109.5 . . ?
H46A C46 H46B 109.5 . . ?
C45 C46 H46C 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C45 C47 H47A 109.5 . . ?
C45 C47 H47B 109.5 . . ?
H47A C47 H47B 109.5 . . ?
C45 C47 H47C 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
C45 C48 H48A 109.5 . . ?
C45 C48 H48B 109.5 . . ?
H48A C48 H48B 109.5 . . ?
C45 C48 H48C 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C50 C49 Ag2B 125(3) . . ?
C50 C49 Ag2A 129(3) . . ?
C50 C49 Ag3A 145(3) . . ?
Ag2A C49 Ag3A 85.6(13) . . ?
C50 C49 Ag1A 89(3) . . ?
Ag2A C49 Ag1A 92.1(14) . . ?
Ag3A C49 Ag1A 87.7(13) . . ?
C50 C49 Ag3B 124(3) . . ?
Ag2B C49 Ag3B 95(2) . . ?
C49 C50 C51 163(5) . . ?
C49 C50 Ag2B 32(2) . . ?
C51 C50 Ag2B 147(3) . . ?
C49 C50 Ag1A 62(2) . . ?
C51 C50 Ag1A 135(4) . . ?
C54 C51 C50 110(5) . . ?
C54 C51 C52 117(5) . . ?
C50 C51 C52 115(5) . . ?
C54 C51 C53 96(5) . . ?
C50 C51 C53 106(4) . . ?
C52 C51 C53 110(5) . . ?
C51 C52 H52A 109.5 . . ?
C51 C52 H52B 109.5 . . ?
H52A C52 H52B 109.5 . . ?
C51 C52 H52C 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C51 C53 H53A 109.5 . . ?
C51 C53 H53B 109.5 . . ?
H53A C53 H53B 109.5 . . ?
C51 C53 H53C 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C51 C54 H54A 109.5 . . ?
C51 C54 H54B 109.5 . . ?
H54A C54 H54B 109.5 . . ?
C51 C54 H54C 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C56 C55 Ag5B 149(4) . . ?
C56 C55 Ag4A 124(3) . . ?
C56 C55 Ag3A 83(2) . . ?
Ag4A C55 Ag3A 95.9(14) . . ?
C56 C55 Ag4B 147(4) . . ?
Ag5B C55 Ag4B 60.8(12) . . ?
C56 C55 Ag5A 129(4) . . ?
Ag4A C55 Ag5A 107.6(19) . . ?
Ag3A C55 Ag5A 93.7(17) . . ?
C56 C55 Ag3B 86(3) . . ?
Ag5B C55 Ag3B 112.4(16) . . ?
Ag4B C55 Ag3B 89.9(16) . . ?
C55 C56 C57 171(4) . . ?
C55 C56 Ag3A 67(2) . . ?
C57 C56 Ag3A 120(3) . . ?
C55 C56 Ag3B 67(2) . . ?
C57 C56 Ag3B 122(3) . . ?
C59 C57 C60 115(6) . . ?
C59 C57 C56 109(4) . . ?
C60 C57 C56 116(4) . . ?
C59 C57 C58 116(6) . . ?
C60 C57 C58 95(5) . . ?
C56 C57 C58 106(4) . . ?
C57 C58 H58A 109.5 . . ?
C57 C58 H58B 109.5 . . ?
H58A C58 H58B 109.5 . . ?
C57 C58 H58C 109.5 . . ?
H58A C58 H58C 109.5 . . ?
H58B C58 H58C 109.5 . . ?
C57 C59 H59A 109.5 . . ?
C57 C59 H59B 109.5 . . ?
H59A C59 H59B 109.5 . . ?
C57 C59 H59C 109.5 . . ?
H59A C59 H59C 109.5 . . ?
H59B C59 H59C 109.5 . . ?
C57 C60 H60A 109.5 . . ?
C57 C60 H60B 109.5 . . ?
H60A C60 H60B 109.5 . . ?
C57 C60 H60C 109.5 . . ?
H60A C60 H60C 109.5 . . ?
H60B C60 H60C 109.5 . . ?
C62 C61 Ag6A 153(4) . . ?
C62 C61 Ag6B 151(4) . . ?
C62 C61 Ag18 128(3) . . ?
Ag6A C61 Ag18 69(3) . . ?
Ag6B C61 Ag18 80.6(14) . . ?
C62 C61 Ag5A 80(3) . . ?
Ag6A C61 Ag5A 126(3) . . ?
Ag18 C61 Ag5A 84.9(17) . . ?
C62 C61 Ag5B 86(3) . . ?
Ag6B C61 Ag5B 99.1(15) . . ?
Ag18 C61 Ag5B 97.4(15) . . ?
C61 C62 C63 170(4) . . ?
C61 C62 Ag5A 70(3) . . ?
C63 C62 Ag5A 119(3) . . ?
C61 C62 Ag5B 66(3) . . ?
C63 C62 Ag5B 124(2) . . ?
C66 C63 C64 114(3) . . ?
C66 C63 C65 114(3) . . ?
C64 C63 C65 112(3) . . ?
C66 C63 C62 102(4) . . ?
C64 C63 C62 107(4) . . ?
C65 C63 C62 106(4) . . ?
C63 C64 H64A 109.5 . . ?
C63 C64 H64B 109.5 . . ?
H64A C64 H64B 109.5 . . ?
C63 C64 H64C 109.5 . . ?
H64A C64 H64C 109.5 . . ?
H64B C64 H64C 109.5 . . ?
C63 C65 H65A 109.5 . . ?
C63 C65 H65B 109.5 . . ?
H65A C65 H65B 109.5 . . ?
C63 C65 H65C 109.5 . . ?
H65A C65 H65C 109.5 . . ?
H65B C65 H65C 109.5 . . ?
C63 C66 H66A 109.5 . . ?
C63 C66 H66B 109.5 . . ?
H66A C66 H66B 109.5 . . ?
C63 C66 H66C 109.5 . . ?
H66A C66 H66C 109.5 . . ?
H66B C66 H66C 109.5 . . ?
C68 C67 Ag8 143(4) . . ?
C68 C67 Ag7B 94(3) . . ?
Ag8 C67 Ag7B 123(2) . . ?
C68 C67 Ag12 127(4) . . ?
Ag8 C67 Ag12 79.8(13) . . ?
Ag7B C67 Ag12 55.1(14) . . ?
C68 C67 Ag10 96(3) . . ?
Ag8 C67 Ag10 77.4(14) . . ?
Ag7B C67 Ag10 105(2) . . ?
Ag12 C67 Ag10 130.2(19) . . ?
C68 C67 Ag7A 86(3) . . ?
Ag8 C67 Ag7A 128.0(18) . . ?
Ag12 C67 Ag7A 79.0(12) . . ?
Ag10 C67 Ag7A 81.3(13) . . ?
C67 C68 C69 173(5) . . ?
C67 C68 Ag7B 58(3) . . ?
C69 C68 Ag7B 129(3) . . ?
C67 C68 Ag7A 67(3) . . ?
C69 C68 Ag7A 120(3) . . ?
C71 C69 C70 113(3) . . ?
C71 C69 C72 113(3) . . ?
C70 C69 C72 112(3) . . ?
C71 C69 C68 106(4) . . ?
C70 C69 C68 105(4) . . ?
C72 C69 C68 106(4) . . ?
C69 C70 H70A 109.4 . . ?
C69 C70 H70B 109.5 . . ?
H70A C70 H70B 109.5 . . ?
C69 C70 H70C 109.5 . . ?
H70A C70 H70C 109.5 . . ?
H70B C70 H70C 109.5 . . ?
C69 C71 H71A 109.5 . . ?
C69 C71 H71B 109.4 . . ?
H71A C71 H71B 109.5 . . ?
C69 C71 H71C 109.5 . . ?
H71A C71 H71C 109.5 . . ?
H71B C71 H71C 109.5 . . ?
C69 C72 H72A 109.5 . . ?
C69 C72 H72B 109.4 . . ?
H72A C72 H72B 109.5 . . ?
C69 C72 H72C 109.5 . . ?
H72A C72 H72C 109.5 . . ?
H72B C72 H72C 109.5 . . ?
C74 C73 Ag14 141(3) . . ?
C74 C73 Ag8 139(3) . . ?
Ag14 C73 Ag8 79.3(11) . . ?
C74 C73 Ag13 92(2) . . ?
Ag14 C73 Ag13 91.9(13) . . ?
Ag8 C73 Ag13 92.0(15) . . ?
C73 C74 C75 172(5) . . ?
C73 C74 Ag13 58(2) . . ?
C75 C74 Ag13 128(3) . . ?
C74 C75 C78 113(5) . . ?
C74 C75 C77 112(4) . . ?
C78 C75 C77 123(6) . . ?
C74 C75 C76 107(4) . . ?
C78 C75 C76 111(6) . . ?
C77 C75 C76 89(5) . . ?
C75 C76 H76A 109.5 . . ?
C75 C76 H76B 109.5 . . ?
H76A C76 H76B 109.5 . . ?
C75 C76 H76C 109.5 . . ?
H76A C76 H76C 109.5 . . ?
H76B C76 H76C 109.5 . . ?
C75 C77 H77A 109.5 . . ?
C75 C77 H77B 109.5 . . ?
H77A C77 H77B 109.5 . . ?
C75 C77 H77C 109.5 . . ?
H77A C77 H77C 109.5 . . ?
H77B C77 H77C 109.5 . . ?
C75 C78 H78A 109.5 . . ?
C75 C78 H78B 109.5 . . ?
H78A C78 H78B 109.5 . . ?
C75 C78 H78C 109.5 . . ?
H78A C78 H78C 109.5 . . ?
H78B C78 H78C 109.5 . . ?
F21 C79 F20 113(6) . . ?
F21 C79 F19 110(5) . . ?
F20 C79 F19 115(5) . . ?
F21 C79 C80 113(4) . . ?
F20 C79 C80 103(4) . . ?
F19 C79 C80 101(5) . . ?
O10 C80 O9 124(4) . . ?
O10 C80 C79 116(4) . . ?
O9 C80 C79 119(4) . . ?
F4 C81 F5 106(4) . . ?
F4 C81 F6 104(4) . . ?
F5 C81 F6 103(4) . . ?
F4 C81 C82 117(4) . . ?
F5 C81 C82 110(4) . . ?
F6 C81 C82 115(4) . . ?
O6 C82 C83 130(4) . . ?
O6 C82 C81 113(3) . . ?
C83 C82 C81 116(3) . . ?
C82 C83 C84 123(3) . . ?
C82 C83 H83 118.7 . . ?
C84 C83 H83 118.7 . . ?
O5 C84 C85 120(4) . . ?
O5 C84 C83 125(4) . . ?
C85 C84 C83 115(3) . . ?
C84 C85 F1 113(4) . . ?
C84 C85 F3 121(3) . . ?
F1 C85 F3 101(3) . . ?
C84 C85 F2 118(3) . . ?
F1 C85 F2 100(3) . . ?
F3 C85 F2 100(2) . . ?
F12 C86 F10 100(5) . . ?
F12 C86 F11 112(5) . . ?
F10 C86 F11 104(5) . . ?
F12 C86 C87 111(5) . . ?
F10 C86 C87 113(4) . . ?
F11 C86 C87 117(5) . . ?
O11 C87 C86 123(5) . . ?
O11 C87 C88 120(5) . . ?
C86 C87 C88 116(4) . . ?
C89 C88 C87 122(4) . . ?
C89 C88 H88 119.1 . . ?
C87 C88 H88 119.1 . . ?
O12 C89 C88 139(4) . . ?
O12 C89 C90 101(4) . . ?
C88 C89 C90 119(4) . . ?
F7 C90 F8 112(6) . . ?
F7 C90 F9 101(5) . . ?
F8 C90 F9 98(5) . . ?
F7 C90 C89 117(5) . . ?
F8 C90 C89 112(5) . . ?
F9 C90 C89 116(5) . . ?
O14 C91 O13 126(4) . . ?
O14 C91 C92 120(5) . . ?
O13 C91 C92 113(4) . . ?
O14 C91 Ag7B 74(3) . . ?
O13 C91 Ag7B 53(2) . . ?
C92 C91 Ag7B 166(4) . . ?
F17A C92 F18A 107(3) . . ?
F18B C92 F16B 104(3) . . ?
F18B C92 F17B 103(3) . . ?
F16B C92 F17B 104(3) . . ?
F17A C92 F16A 105(3) . . ?
F18A C92 F16A 104(3) . . ?
F17A C92 C91 112(4) . . ?
F18A C92 C91 109(4) . . ?
F18B C92 C91 118(5) . . ?
F16B C92 C91 112(5) . . ?
F17B C92 C91 115(5) . . ?
F16A C92 C91 118(5) . . ?

_refine_diff_density_max         2.920
_refine_diff_density_min         -1.686
_refine_diff_density_rms         0.310

