# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_11
_database_code_depnum_ccdc_archive 'CCDC 1842463'
_audit_update_record             
;
2018-05-10 deposited with the CCDC.
2018-06-29 downloaded from the CCDC.
;
_audit_creation_date             2017-12-19
_audit_creation_method           
;
Olex2 1.2
(compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381)
;
_shelx_SHELXL_version_number     2016/6
_chemical_name_common            ?
_chemical_name_systematic        
;
 ? 
;
_chemical_formula_moiety         'B28 K11 O48 Rb'
_chemical_formula_sum            'B28 K11 O48 Rb'
_chemical_formula_weight         1586.25
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   6.6231(2)
_cell_length_b                   11.3213(3)
_cell_length_c                   28.7010(9)
_cell_angle_alpha                92.208(2)
_cell_angle_beta                 91.584(2)
_cell_angle_gamma                90.200(2)
_cell_volume                     2149.62(11)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    1777
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      21.084
_cell_measurement_theta_min      3.177
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    2.363
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.6276
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.0717 before and 0.0608 after correction. The Ratio of minimum to maximum transmission is 0.8417. The λ/2 correction factor is 0.0015.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    2.451
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1540
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_special_details           
;
 ? 
;
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0869
_diffrn_reflns_av_unetI/netI     0.1145
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.979
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            26849
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.979
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.556
_diffrn_reflns_theta_min         1.421
_diffrn_ambient_temperature      296.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                5476
_reflns_number_total             9738
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v7.68A (Bruker, 2009)'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'SAINT v7.68A (Bruker, 2009)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_refine_diff_density_max         1.851
_refine_diff_density_min         -2.685
_refine_diff_density_rms         0.176
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     793
_refine_ls_number_reflns         9738
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1361
_refine_ls_R_factor_gt           0.0719
_refine_ls_restrained_S_all      1.049
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0960P)²+6.0956P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1805
_refine_ls_wR_factor_ref         0.2200
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rb1 Rb -0.55521(19) -0.15323(11) 0.13790(4) 0.0570(3) Uani 1 1 d . . . . .
K1 K 0.4538(2) 0.14552(14) 0.47972(6) 0.0220(4) Uani 1 1 d . . . . .
K2 K 0.1130(2) 0.29728(15) 0.16022(6) 0.0221(4) Uani 1 1 d . . . . .
K3 K 0.4001(3) 0.43274(15) 0.29987(6) 0.0230(4) Uani 1 1 d . . . . .
K4 K -0.0289(3) 0.35203(14) 0.02627(6) 0.0225(4) Uani 1 1 d . . . . .
K5 K 0.6233(3) 0.15763(15) 0.34196(7) 0.0264(4) Uani 1 1 d . . . . .
K6 K -0.0687(3) -0.02331(17) 0.18919(7) 0.0322(5) Uani 1 1 d . . . . .
K7 K 1.0661(3) -0.07151(15) 0.30746(6) 0.0248(4) Uani 1 1 d . . . . .
K8 K -1.4235(3) -0.50773(15) 0.18009(7) 0.0265(4) Uani 1 1 d . . . . .
K9 K 0.0478(3) 0.34855(16) 0.53110(6) 0.0278(4) Uani 1 1 d . . . . .
K10 K 0.0187(4) 0.36077(17) 0.64034(6) 0.0403(6) Uani 1 1 d . . . . .
K11 K -0.5681(3) -0.15025(15) 0.02524(6) 0.0259(4) Uani 1 1 d . . . . .
B1 B 0.0968(13) 0.2364(7) 0.3546(3) 0.0180(18) Uani 1 1 d . . . . .
B2 B 0.5602(12) 0.2057(7) 0.5902(3) 0.0171(17) Uani 1 1 d . . . . .
B3 B -1.0620(12) -0.3294(7) 0.0814(3) 0.0164(17) Uani 1 1 d . . . . .
B4 B -0.2499(12) 0.4443(7) -0.0906(3) 0.0180(18) Uani 1 1 d . . . . .
B5 B -0.2607(12) 0.0594(7) 0.0795(3) 0.0144(16) Uani 1 1 d . . . . .
B6 B 0.6948(12) 0.2411(7) 0.2347(3) 0.0157(17) Uani 1 1 d . . . . .
B7 B -0.0713(12) 0.3952(7) 0.2649(3) 0.0148(17) Uani 1 1 d . . . . .
B8 B 0.3861(12) 0.7021(7) 0.2474(3) 0.0171(18) Uani 1 1 d . . . . .
B9 B 0.0317(11) 0.5999(7) 0.2466(3) 0.0152(17) Uani 1 1 d . . . . .
B10 B 0.3375(12) 0.5798(7) 0.5686(3) 0.0157(17) Uani 1 1 d . . . . .
B11 B 0.5896(13) 0.4315(8) 0.5846(3) 0.0213(19) Uani 1 1 d . . . . .
B12 B 0.8605(13) 0.0781(7) 0.5690(3) 0.0164(17) Uani 1 1 d . . . . .
B13 B 0.3101(12) 0.3530(7) 0.4096(3) 0.0182(18) Uani 1 1 d . . . . .
B14 B 0.9076(12) 0.0801(7) 0.4472(3) 0.0170(18) Uani 1 1 d . . . . .
B15 B 1.0413(12) 0.1892(7) 0.2657(3) 0.0163(17) Uani 1 1 d . . . . .
B16 B -0.9751(12) -0.4030(7) 0.1574(3) 0.0176(18) Uani 1 1 d . . . . .
B17 B 0.4998(12) -0.0909(7) 0.2500(3) 0.0144(17) Uani 1 1 d . . . . .
B18 B 0.3825(11) 0.1125(7) 0.2363(3) 0.0125(16) Uani 1 1 d . . . . .
B19 B -0.5213(12) 0.3950(7) 0.0637(3) 0.0164(17) Uani 1 1 d . . . . .
B20 B -0.5680(12) 0.1773(7) 0.0758(3) 0.0177(18) Uani 1 1 d . . . . .
B21 B -1.0228(12) -0.1065(8) 0.0795(3) 0.0178(18) Uani 1 1 d . . . . .
B22 B -0.4013(13) 0.5963(7) 0.0620(3) 0.0181(18) Uani 1 1 d . . . . .
B23 B 0.6381(14) 0.1912(8) 0.1463(3) 0.025(2) Uani 1 1 d . . . . .
B24 B 0.0824(13) 0.0919(7) 0.0620(3) 0.0193(18) Uani 1 1 d . . . . .
B25 B -0.2541(13) -0.2542(8) 0.2517(3) 0.0212(19) Uani 1 1 d . . . . .
B26 B 0.4589(13) 0.1071(7) 0.6610(3) 0.0201(18) Uani 1 1 d . . . . .
B27 B 0.2267(12) 0.1053(7) 0.5920(3) 0.0177(18) Uani 1 1 d . . . . .
B28 B -0.0275(12) 0.2905(7) 0.4322(3) 0.0188(18) Uani 1 1 d . . . . .
O1 O -0.0279(7) 0.5107(4) 0.27972(17) 0.0136(10) Uani 1 1 d . . . . .
O2 O 0.4878(7) 0.2119(4) 0.24621(19) 0.0209(12) Uani 1 1 d . . . . .
O3 O -0.1185(7) 0.1967(4) 0.46070(18) 0.0180(11) Uani 1 1 d . . . . .
O4 O 0.0818(7) 0.3170(4) 0.25998(19) 0.0191(11) Uani 1 1 d . . . . .
O5 O 0.3909(8) 0.4616(4) 0.5720(2) 0.0294(14) Uani 1 1 d . . . . .
O6 O -0.5276(7) 0.0081(4) 0.21960(17) 0.0158(11) Uani 1 1 d . . . . .
O7 O -0.0696(7) 0.4226(4) -0.06393(18) 0.0162(11) Uani 1 1 d . . . . .
O8 O -1.1182(8) -0.3529(5) 0.12997(19) 0.0237(12) Uani 1 1 d . . . . .
O9 O -0.4713(7) 0.2809(4) 0.05387(18) 0.0171(11) Uani 1 1 d . . . . .
O10 O 0.3087(8) 0.4313(4) 0.0834(2) 0.0221(12) Uani 1 1 d . . . . .
O11 O -0.8704(7) -0.0202(4) 0.07913(19) 0.0207(12) Uani 1 1 d . . . . .
O12 O 0.3474(7) 0.1993(4) 0.57613(17) 0.0146(10) Uani 1 1 d . . . . .
O13 O 0.2185(7) 0.1762(4) 0.0613(2) 0.0214(12) Uani 1 1 d . . . . .
O14 O 0.1805(7) 0.3103(4) 0.44444(17) 0.0151(10) Uani 1 1 d . . . . .
O15 O -0.2189(7) -0.0694(4) 0.0837(2) 0.0206(12) Uani 1 1 d . . . . .
O16 O 0.2527(7) 0.6127(4) 0.25091(19) 0.0186(11) Uani 1 1 d . . . . .
O17 O 0.7336(7) 0.3615(4) 0.25738(18) 0.0164(11) Uani 1 1 d . . . . .
O18 O 0.0119(7) 0.1438(4) 0.59014(18) 0.0168(11) Uani 1 1 d . . . . .
O19 O 0.1405(7) 0.5982(4) 0.55681(19) 0.0212(12) Uani 1 1 d . . . . .
O20 O -0.9561(8) -0.2164(4) 0.0792(2) 0.0239(13) Uani 1 1 d . . . . .
O21 O -0.2953(7) -0.1404(4) 0.2435(2) 0.0205(12) Uani 1 1 d . . . . .
O22 O -1.0323(8) -0.4399(5) 0.20025(18) 0.0231(12) Uani 1 1 d . . . . .
O23 O 0.1764(7) 0.1118(4) 0.23897(19) 0.0189(11) Uani 1 1 d . . . . .
O24 O -0.6534(7) -0.1849(4) 0.23730(19) 0.0197(12) Uani 1 1 d . . . . .
O25 O -0.2233(8) 0.1185(5) 0.12551(19) 0.0247(12) Uani 1 1 d . . . . .
O26 O 0.7500(7) 0.0091(4) 0.4343(2) 0.0231(12) Uani 1 1 d . . . . .
O27 O 0.8375(7) 0.1574(4) 0.2499(2) 0.0267(13) Uani 1 1 d . . . . .
O28 O 0.6675(7) 0.1144(4) 0.56276(19) 0.0205(12) Uani 1 1 d . . . . .
O29 O -0.4642(7) 0.0722(4) 0.06251(18) 0.0162(11) Uani 1 1 d . . . . .
O30 O 0.5958(8) 0.1787(5) 0.64032(19) 0.0229(12) Uani 1 1 d . . . . .
O31 O -0.5796(7) -0.3653(4) 0.07919(19) 0.0207(12) Uani 1 1 d . . . . .
O32 O 0.4783(8) -0.0522(4) 0.29865(18) 0.0201(11) Uani 1 1 d . . . . .
O33 O 0.5881(7) 0.6657(4) 0.2549(2) 0.0243(13) Uani 1 1 d . . . . .
O34 O -0.0585(8) 0.2534(5) 0.38313(18) 0.0236(12) Uani 1 1 d . . . . .
O35 O 0.2805(8) 0.2866(5) 0.36456(19) 0.0239(12) Uani 1 1 d . . . . .
O36 O 0.6558(7) 0.3212(4) 0.5833(2) 0.0216(12) Uani 1 1 d . . . . .
O37 O 0.4493(8) 0.2021(5) 0.12750(19) 0.0251(13) Uani 1 1 d . . . . .
O38 O 0.2785(8) 0.4814(4) 0.4011(2) 0.0248(13) Uani 1 1 d . . . . .
O39 O -0.3727(8) 0.4766(4) 0.0528(2) 0.0281(14) Uani 1 1 d . . . . .
O40 O 0.2143(8) 0.5732(5) 0.14223(18) 0.0245(12) Uani 1 1 d . . . . .
O41 O -0.1122(7) 0.1094(4) 0.04753(19) 0.0201(12) Uani 1 1 d . . . . .
O42 O 0.7036(9) 0.2611(5) 0.1839(2) 0.0318(14) Uani 1 1 d . . . . .
O43 O 0.4748(7) 0.6662(4) 0.5763(2) 0.0239(13) Uani 1 1 d . . . . .
O44 O 0.8982(8) -0.0354(4) 0.5521(2) 0.0297(14) Uani 1 1 d . . . . .
O45 O -1.2521(7) -0.3263(4) 0.05324(18) 0.0192(11) Uani 1 1 d . . . . .
O46 O 0.0685(10) 0.1639(5) 0.31543(19) 0.0312(14) Uani 1 1 d . . . . .
O47 O -0.0592(7) 0.7153(4) 0.2601(2) 0.0224(12) Uani 1 1 d . . . . .
O48 O 0.7227(7) -0.0815(5) 0.35777(18) 0.0226(12) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rb1 K11 3.234(2) . ?
Rb1 B17 3.276(9) 1_455 ?
Rb1 B21 3.532(8) . ?
Rb1 O6 2.917(5) . ?
Rb1 O11 3.081(5) . ?
Rb1 O15 2.928(5) . ?
Rb1 O20 3.170(5) . ?
Rb1 O21 3.441(6) . ?
Rb1 O24 2.978(5) . ?
Rb1 O29 3.471(5) . ?
Rb1 O31 2.881(5) . ?
Rb1 O40 3.456(6) 1_445 ?
K1 B2 3.274(9) . ?
K1 B13 3.278(8) . ?
K1 B14 3.251(8) . ?
K1 O3 2.959(5) 1_655 ?
K1 O12 2.916(5) . ?
K1 O14 2.802(5) . ?
K1 O26 3.387(6) 2_656 ?
K1 O26 2.818(5) . ?
K1 O28 3.231(5) 2_656 ?
K1 O28 2.773(5) . ?
K1 O43 2.767(5) 2_666 ?
K1 O44 2.756(6) 2_656 ?
K2 B7 3.422(9) . ?
K2 B15 3.355(9) 1_455 ?
K2 B23 3.371(10) 1_455 ?
K2 O4 2.876(6) . ?
K2 O10 3.041(5) . ?
K2 O13 3.199(6) . ?
K2 O22 3.304(6) 1_665 ?
K2 O23 3.164(5) . ?
K2 O25 3.121(6) . ?
K2 O37 2.657(5) . ?
K2 O40 3.256(6) . ?
K2 O42 2.846(6) 1_455 ?
K3 B1 3.444(8) . ?
K3 B6 3.454(8) . ?
K3 B7 3.274(8) . ?
K3 B13 3.378(9) . ?
K3 O1 3.019(5) . ?
K3 O2 2.953(5) . ?
K3 O4 2.684(5) . ?
K3 O16 2.690(5) . ?
K3 O17 2.665(5) . ?
K3 O33 3.240(5) . ?
K3 O35 2.668(5) . ?
K3 O38 3.066(6) . ?
K4 B3 3.164(9) 2_455 ?
K4 B4 3.404(9) 2_565 ?
K4 B24 3.237(8) . ?
K4 O7 2.801(5) 2_565 ?
K4 O7 2.745(5) . ?
K4 O9 3.166(5) . ?
K4 O10 2.857(6) . ?
K4 O13 2.783(5) . ?
K4 O20 3.339(6) 2_455 ?
K4 O39 2.791(5) . ?
K4 O41 2.891(5) . ?
K4 O45 2.990(5) 2_455 ?
K5 B1 3.264(9) 1_655 ?
K5 B6 3.300(9) . ?
K5 B26 3.042(9) 2_656 ?
K5 O2 2.955(6) . ?
K5 O26 3.284(6) . ?
K5 O27 3.032(6) . ?
K5 O32 2.793(6) . ?
K5 O34 2.601(6) 1_655 ?
K5 O35 2.782(5) . ?
K5 O43 3.104(6) 2_666 ?
K5 O46 3.067(7) 1_655 ?
K5 O48 2.839(5) . ?
K6 B5 3.524(8) . ?
K6 B15 3.262(9) 1_455 ?
K6 B17 3.487(8) 1_455 ?
K6 B21 3.275(9) 1_655 ?
K6 B23 3.364(9) 1_455 ?
K6 B25 3.468(9) . ?
K6 O6 3.203(5) . ?
K6 O15 3.184(6) . ?
K6 O21 2.591(5) . ?
K6 O23 2.589(5) . ?
K6 O25 2.664(6) . ?
K6 O27 2.722(6) 1_455 ?
K7 B15 3.231(8) . ?
K7 B25 3.296(10) 1_655 ?
K7 B26 3.280(9) 2_756 ?
K7 O18 3.137(5) 2_656 ?
K7 O21 3.057(6) 1_655 ?
K7 O23 3.014(5) 1_655 ?
K7 O24 3.029(5) 1_755 ?
K7 O30 2.950(5) 2_756 ?
K7 O32 2.757(5) 1_655 ?
K7 O46 2.666(6) 1_655 ?
K7 O47 2.834(6) 1_645 ?
K7 O48 2.732(5) . ?
K8 B4 3.411(9) 2_355 ?
K8 B6 3.384(8) 1_345 ?
K8 B8 3.282(8) 1_345 ?
K8 B16 3.285(8) . ?
K8 O8 3.092(6) . ?
K8 O10 3.301(6) 1_345 ?
K8 O16 3.261(5) 1_345 ?
K8 O17 2.886(5) 1_345 ?
K8 O22 2.740(5) . ?
K8 O33 2.852(6) 1_345 ?
K8 O40 2.779(5) 1_345 ?
K8 O42 2.757(6) 1_345 ?
K9 K10 3.144(3) . ?
K9 B10 3.366(9) . ?
K9 B27 3.511(8) . ?
K9 B28 2.917(9) . ?
K9 O3 2.802(6) . ?
K9 O5 2.810(6) . ?
K9 O12 2.917(5) . ?
K9 O14 2.681(5) . ?
K9 O18 2.936(5) . ?
K9 O19 2.870(6) 2_566 ?
K9 O19 2.951(5) . ?
K9 O36 3.055(5) 1_455 ?
K10 B9 3.283(9) 2_566 ?
K10 B11 3.338(9) 1_455 ?
K10 B27 3.466(9) . ?
K10 O1 2.668(5) 2_566 ?
K10 O5 3.412(6) . ?
K10 O12 3.387(5) . ?
K10 O18 2.799(5) . ?
K10 O36 2.894(6) 1_455 ?
K10 O38 2.922(5) 2_566 ?
K10 O47 3.020(6) 2_566 ?
K11 B20 3.064(9) 2_455 ?
K11 B22 3.280(8) 1_545 ?
K11 O9 2.681(5) 2_455 ?
K11 O11 2.930(5) . ?
K11 O15 2.942(6) . ?
K11 O20 3.139(6) . ?
K11 O29 2.715(5) 2_455 ?
K11 O29 2.775(5) . ?
K11 O31 2.937(5) . ?
K11 O41 2.982(5) 2_455 ?
K11 O45 3.010(5) 1_655 ?
B1 O34 1.342(10) . ?
B1 O35 1.359(10) . ?
B1 O46 1.375(11) . ?
B2 O12 1.456(9) . ?
B2 O28 1.472(10) . ?
B2 O30 1.495(10) . ?
B2 O36 1.473(9) . ?
B3 O7 1.453(9) 2_455 ?
B3 O8 1.488(10) . ?
B3 O20 1.460(9) . ?
B3 O45 1.478(10) . ?
B4 O7 1.428(9) . ?
B4 O10 1.470(9) 2_565 ?
B4 O31 1.490(10) 2_455 ?
B4 O40 1.512(10) 2_565 ?
B5 O15 1.493(9) . ?
B5 O25 1.472(10) . ?
B5 O29 1.431(9) . ?
B5 O41 1.489(9) . ?
B6 O2 1.459(9) . ?
B6 O17 1.505(9) . ?
B6 O27 1.413(9) . ?
B6 O42 1.487(10) . ?
B7 O1 1.386(9) . ?
B7 O4 1.356(9) . ?
B7 O17 1.355(9) 1_455 ?
B8 O16 1.350(9) . ?
B8 O24 1.347(9) 1_665 ?
B8 O33 1.414(9) . ?
B9 O1 1.473(9) . ?
B9 O16 1.472(9) . ?
B9 O22 1.441(10) 1_665 ?
B9 O47 1.482(9) . ?
B10 O5 1.392(9) . ?
B10 O19 1.358(9) . ?
B10 O43 1.340(10) . ?
B11 O5 1.402(10) . ?
B11 O36 1.325(10) . ?
B11 O38 1.359(10) 2_666 ?
B12 O18 1.362(9) 1_655 ?
B12 O28 1.353(9) . ?
B12 O44 1.383(10) . ?
B13 O14 1.432(10) . ?
B13 O35 1.479(10) . ?
B13 O38 1.498(9) . ?
B13 O43 1.489(9) 2_666 ?
B14 O3 1.374(9) 1_655 ?
B14 O26 1.351(10) . ?
B14 O44 1.384(9) 2_756 ?
B15 O4 1.487(9) 1_655 ?
B15 O23 1.466(9) 1_655 ?
B15 O27 1.452(9) . ?
B15 O46 1.472(10) 1_655 ?
B16 O8 1.355(9) . ?
B16 O22 1.377(10) . ?
B16 O40 1.364(9) 1_445 ?
B17 O6 1.454(9) 1_655 ?
B17 O21 1.484(9) 1_655 ?
B17 O24 1.496(9) 1_655 ?
B17 O32 1.459(10) . ?
B18 O2 1.339(9) . ?
B18 O6 1.400(9) 1_655 ?
B18 O23 1.369(9) . ?
B19 O9 1.357(9) . ?
B19 O10 1.332(9) 1_455 ?
B19 O39 1.398(10) . ?
B20 O9 1.501(9) . ?
B20 O13 1.462(9) 1_455 ?
B20 O29 1.420(9) . ?
B20 O37 1.501(11) 1_455 ?
B21 O11 1.403(10) . ?
B21 O15 1.374(9) 1_455 ?
B21 O20 1.322(10) . ?
B22 O31 1.358(10) 1_565 ?
B22 O39 1.386(10) . ?
B22 O45 1.354(10) 1_665 ?
B23 O25 1.369(11) 1_655 ?
B23 O37 1.356(11) . ?
B23 O42 1.375(11) . ?
B24 O11 1.411(9) 1_655 ?
B24 O13 1.311(10) . ?
B24 O41 1.361(10) . ?
B25 O21 1.346(9) . ?
B25 O33 1.389(10) 1_445 ?
B25 O47 1.356(10) 1_545 ?
B26 O30 1.376(10) . ?
B26 O32 1.390(10) 2_656 ?
B26 O48 1.331(10) 2_656 ?
B27 O12 1.426(9) . ?
B27 O18 1.490(9) . ?
B27 O26 1.484(10) 2_656 ?
B27 O48 1.505(10) 2_656 ?
B28 O3 1.500(10) . ?
B28 O14 1.427(9) . ?
B28 O19 1.495(9) 2_566 ?
B28 O34 1.464(11) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
K11 Rb1 B17 166.07(15) . 1_455 ?
K11 Rb1 B21 61.25(14) . . ?
K11 Rb1 O21 151.34(10) . . ?
K11 Rb1 O29 48.75(9) . . ?
K11 Rb1 O40 94.61(10) . 1_445 ?
B17 Rb1 B21 120.5(2) 1_455 . ?
B17 Rb1 O21 25.38(15) 1_455 . ?
B17 Rb1 O29 117.39(16) 1_455 . ?
B17 Rb1 O40 99.25(16) 1_455 1_445 ?
O6 Rb1 K11 140.59(10) . . ?
O6 Rb1 B17 26.35(16) . 1_455 ?
O6 Rb1 B21 108.29(18) . . ?
O6 Rb1 O11 99.27(14) . . ?
O6 Rb1 O15 101.03(15) . . ?
O6 Rb1 O20 125.45(14) . . ?
O6 Rb1 O21 43.19(12) . . ?
O6 Rb1 O24 48.31(13) . . ?
O6 Rb1 O29 92.34(13) . . ?
O6 Rb1 O40 121.46(13) . 1_445 ?
O11 Rb1 K11 55.23(11) . . ?
O11 Rb1 B17 120.06(17) . 1_455 ?
O11 Rb1 B21 23.23(16) . . ?
O11 Rb1 O20 42.97(13) . . ?
O11 Rb1 O21 142.44(13) . . ?
O11 Rb1 O29 52.94(12) . . ?
O11 Rb1 O40 100.69(13) . 1_445 ?
O15 Rb1 K11 56.78(11) . . ?
O15 Rb1 B17 113.24(18) . 1_455 ?
O15 Rb1 B21 111.06(17) . . ?
O15 Rb1 O11 92.76(14) . . ?
O15 Rb1 O20 115.18(15) . . ?
O15 Rb1 O21 95.48(14) . . ?
O15 Rb1 O24 138.71(15) . . ?
O15 Rb1 O29 42.43(12) . . ?
O15 Rb1 O40 131.98(14) . 1_445 ?
O20 Rb1 K11 58.71(11) . . ?
O20 Rb1 B17 128.74(18) . 1_455 ?
O20 Rb1 B21 21.90(17) . . ?
O20 Rb1 O21 149.31(14) . . ?
O20 Rb1 O29 88.85(13) . . ?
O20 Rb1 O40 58.23(12) . 1_445 ?
O21 Rb1 B21 145.79(17) . . ?
O21 Rb1 O29 116.86(12) . . ?
O21 Rb1 O40 100.65(12) . 1_445 ?
O24 Rb1 K11 164.50(11) . . ?
O24 Rb1 B17 27.14(17) . 1_455 ?
O24 Rb1 B21 105.61(17) . . ?
O24 Rb1 O11 116.18(14) . . ?
O24 Rb1 O20 105.95(15) . . ?
O24 Rb1 O21 43.62(13) . . ?
O24 Rb1 O29 139.59(13) . . ?
O24 Rb1 O40 73.55(13) . 1_445 ?
O29 Rb1 B21 74.91(16) . . ?
O31 Rb1 K11 57.06(11) . . ?
O31 Rb1 B17 136.05(17) . 1_455 ?
O31 Rb1 B21 80.05(18) . . ?
O31 Rb1 O6 162.33(15) . . ?
O31 Rb1 O11 93.98(15) . . ?
O31 Rb1 O15 89.89(15) . . ?
O31 Rb1 O20 59.53(14) . . ?
O31 Rb1 O21 122.55(14) . . ?
O31 Rb1 O24 114.97(14) . . ?
O31 Rb1 O29 105.01(14) . . ?
O31 Rb1 O40 43.70(13) . 1_445 ?
O40 Rb1 B21 77.77(16) 1_445 . ?
O40 Rb1 O29 141.89(12) 1_445 . ?
B2 K1 B13 121.2(2) . . ?
B2 K1 O26 57.81(17) . 2_656 ?
B13 K1 O26 137.28(18) . 2_656 ?
B14 K1 B2 98.0(2) . . ?
B14 K1 B13 104.0(2) . . ?
B14 K1 O26 118.63(17) . 2_656 ?
O3 K1 B2 87.88(18) 1_655 . ?
O3 K1 B13 90.11(18) 1_655 . ?
O3 K1 B14 25.00(17) 1_655 . ?
O3 K1 O26 130.19(14) 1_655 2_656 ?
O3 K1 O28 109.77(14) 1_655 2_656 ?
O12 K1 B2 26.40(17) . . ?
O12 K1 B13 112.31(18) . . ?
O12 K1 B14 124.01(19) . . ?
O12 K1 O3 113.45(15) . 1_655 ?
O12 K1 O26 44.95(13) . 2_656 ?
O12 K1 O28 116.64(14) . 2_656 ?
O14 K1 B2 110.67(18) . . ?
O14 K1 B13 25.75(18) . . ?
O14 K1 B14 129.77(18) . . ?
O14 K1 O3 114.16(14) . 1_655 ?
O14 K1 O12 93.08(14) . . ?
O14 K1 O26 111.55(14) . 2_656 ?
O14 K1 O26 130.34(16) . . ?
O14 K1 O28 108.86(14) . 2_656 ?
O26 K1 B2 113.84(19) . . ?
O26 K1 B13 107.8(2) . . ?
O26 K1 B14 24.40(19) . . ?
O26 K1 O3 48.61(14) . 1_655 ?
O26 K1 O12 136.07(15) . . ?
O26 K1 O26 110.10(12) . 2_656 ?
O26 K1 O28 61.16(14) . 2_656 ?
O28 K1 B2 26.56(17) . . ?
O28 K1 B2 124.17(18) 2_656 . ?
O28 K1 B13 141.20(19) . . ?
O28 K1 B13 111.56(18) 2_656 . ?
O28 K1 B14 75.9(2) . . ?
O28 K1 B14 85.24(18) 2_656 . ?
O28 K1 O3 73.88(15) . 1_655 ?
O28 K1 O12 49.06(14) . . ?
O28 K1 O14 136.87(16) . . ?
O28 K1 O26 88.02(16) . . ?
O28 K1 O26 59.39(14) . 2_656 ?
O28 K1 O26 71.84(14) 2_656 2_656 ?
O28 K1 O28 107.11(13) . 2_656 ?
O43 K1 B2 113.06(19) 2_666 . ?
O43 K1 B13 26.85(17) 2_666 . ?
O43 K1 B14 80.41(18) 2_666 . ?
O43 K1 O3 63.56(14) 2_666 1_655 ?
O43 K1 O12 117.60(16) 2_666 . ?
O43 K1 O14 50.87(14) 2_666 . ?
O43 K1 O26 91.20(16) 2_666 . ?
O43 K1 O26 158.66(15) 2_666 2_656 ?
O43 K1 O28 122.40(17) 2_666 . ?
O43 K1 O28 122.34(16) 2_666 2_656 ?
O44 K1 B2 123.5(2) 2_656 . ?
O44 K1 B13 83.81(19) 2_656 . ?
O44 K1 B14 126.1(2) 2_656 . ?
O44 K1 O3 146.24(17) 2_656 1_655 ?
O44 K1 O12 99.50(17) 2_656 . ?
O44 K1 O14 69.28(15) 2_656 . ?
O44 K1 O26 101.99(16) 2_656 . ?
O44 K1 O26 69.72(16) 2_656 2_656 ?
O44 K1 O28 44.40(13) 2_656 2_656 ?
O44 K1 O28 128.34(18) 2_656 . ?
O44 K1 O43 108.08(17) 2_656 2_666 ?
B15 K2 B7 42.40(19) 1_455 . ?
B15 K2 B23 79.2(2) 1_455 1_455 ?
B23 K2 B7 81.4(2) 1_455 . ?
O4 K2 B7 22.81(16) . . ?
O4 K2 B15 26.19(17) . 1_455 ?
O4 K2 B23 92.2(2) . 1_455 ?
O4 K2 O10 138.06(16) . . ?
O4 K2 O13 157.02(14) . . ?
O4 K2 O22 65.77(13) . 1_665 ?
O4 K2 O23 47.87(13) . . ?
O4 K2 O25 105.78(15) . . ?
O4 K2 O40 98.07(14) . . ?
O10 K2 B7 130.73(17) . . ?
O10 K2 B15 159.59(19) . 1_455 ?
O10 K2 B23 120.8(2) . 1_455 ?
O10 K2 O13 57.14(13) . . ?
O10 K2 O22 85.36(14) . 1_665 ?
O10 K2 O23 146.10(14) . . ?
O10 K2 O25 114.62(16) . . ?
O10 K2 O40 44.31(14) . . ?
O13 K2 B7 170.07(17) . . ?
O13 K2 B15 132.98(17) . 1_455 ?
O13 K2 B23 89.03(19) . 1_455 ?
O13 K2 O22 137.03(13) . 1_665 ?
O13 K2 O40 100.93(14) . . ?
O22 K2 B7 47.29(16) 1_665 . ?
O22 K2 B15 89.48(17) 1_665 1_455 ?
O22 K2 B23 94.07(19) 1_665 1_455 ?
O23 K2 B7 67.58(16) . . ?
O23 K2 B15 25.78(16) . 1_455 ?
O23 K2 B23 87.04(18) . 1_455 ?
O23 K2 O13 109.36(13) . . ?
O23 K2 O22 113.60(14) . 1_665 ?
O23 K2 O40 139.16(15) . . ?
O25 K2 B7 101.28(17) . . ?
O25 K2 B15 85.25(18) . 1_455 ?
O25 K2 B23 23.94(19) . 1_455 ?
O25 K2 O13 68.80(14) . . ?
O25 K2 O22 117.48(14) . 1_665 ?
O25 K2 O23 82.45(14) . . ?
O25 K2 O40 135.17(14) . . ?
O37 K2 B7 138.44(19) . . ?
O37 K2 B15 107.58(18) . 1_455 ?
O37 K2 B23 127.5(2) . 1_455 ?
O37 K2 O4 116.81(16) . . ?
O37 K2 O10 64.75(15) . . ?
O37 K2 O13 47.55(15) . . ?
O37 K2 O22 136.78(16) . 1_665 ?
O37 K2 O23 83.29(15) . . ?
O37 K2 O25 103.58(17) . . ?
O37 K2 O40 98.44(15) . . ?
O37 K2 O42 147.02(18) . 1_455 ?
O40 K2 B7 86.45(16) . . ?
O40 K2 B15 124.25(18) . 1_455 ?
O40 K2 B23 120.87(18) . 1_455 ?
O40 K2 O22 42.40(13) . 1_665 ?
O42 K2 B7 57.87(18) 1_455 . ?
O42 K2 B15 64.21(18) 1_455 1_455 ?
O42 K2 B23 23.7(2) 1_455 1_455 ?
O42 K2 O4 70.91(15) 1_455 . ?
O42 K2 O10 132.83(17) 1_455 . ?
O42 K2 O13 112.68(16) 1_455 . ?
O42 K2 O22 76.19(15) 1_455 1_665 ?
O42 K2 O23 80.45(15) 1_455 . ?
O42 K2 O25 45.98(15) 1_455 . ?
O42 K2 O40 112.59(15) 1_455 . ?
B1 K3 B6 100.9(2) . . ?
B7 K3 B1 60.0(2) . . ?
B7 K3 B6 108.2(2) . . ?
B7 K3 B13 93.4(2) . . ?
B13 K3 B1 41.8(2) . . ?
B13 K3 B6 115.89(19) . . ?
O1 K3 B1 74.41(16) . . ?
O1 K3 B6 128.52(18) . . ?
O1 K3 B7 25.02(16) . . ?
O1 K3 B13 94.65(17) . . ?
O1 K3 O33 92.40(12) . . ?
O1 K3 O38 82.39(14) . . ?
O2 K3 B1 79.43(18) . . ?
O2 K3 B6 24.77(16) . . ?
O2 K3 B7 86.86(18) . . ?
O2 K3 B13 106.12(18) . . ?
O2 K3 O1 110.36(14) . . ?
O2 K3 O33 113.20(15) . . ?
O2 K3 O38 132.32(15) . . ?
O4 K3 B1 54.77(19) . . ?
O4 K3 B6 86.14(18) . . ?
O4 K3 B7 23.76(18) . . ?
O4 K3 B13 95.65(19) . . ?
O4 K3 O1 48.58(14) . . ?
O4 K3 O2 63.47(14) . . ?
O4 K3 O16 82.73(15) . . ?
O4 K3 O33 121.63(16) . . ?
O4 K3 O38 104.31(16) . . ?
O16 K3 B1 123.03(18) . . ?
O16 K3 B6 113.23(18) . . ?
O16 K3 B7 66.45(17) . . ?
O16 K3 B13 130.62(18) . . ?
O16 K3 O1 48.62(13) . . ?
O16 K3 O2 116.48(17) . . ?
O16 K3 O33 44.38(13) . . ?
O16 K3 O38 106.31(15) . . ?
O17 K3 B1 121.31(18) . . ?
O17 K3 B6 24.40(17) . . ?
O17 K3 B7 128.51(19) . . ?
O17 K3 B13 120.59(18) . . ?
O17 K3 O1 141.76(16) . . ?
O17 K3 O2 49.17(14) . . ?
O17 K3 O4 108.74(16) . . ?
O17 K3 O16 106.19(16) . . ?
O17 K3 O33 73.96(14) . . ?
O17 K3 O35 113.46(16) . . ?
O17 K3 O38 135.84(16) . . ?
O33 K3 B1 164.64(17) . . ?
O33 K3 B6 93.43(17) . . ?
O33 K3 B7 110.29(17) . . ?
O33 K3 B13 134.53(19) . . ?
O35 K3 B1 21.22(19) . . ?
O35 K3 B6 99.55(18) . . ?
O35 K3 B7 80.76(19) . . ?
O35 K3 B13 24.95(18) . . ?
O35 K3 O1 91.91(15) . . ?
O35 K3 O2 83.96(16) . . ?
O35 K3 O4 75.44(17) . . ?
O35 K3 O16 139.04(17) . . ?
O35 K3 O33 159.43(18) . . ?
O35 K3 O38 49.00(15) . . ?
O38 K3 B1 59.44(18) . . ?
O38 K3 B6 140.10(17) . . ?
O38 K3 B7 91.87(18) . . ?
O38 K3 B13 26.32(16) . . ?
O38 K3 O33 111.82(15) . . ?
B3 K4 B4 116.3(2) 2_455 2_565 ?
B3 K4 B24 102.8(2) 2_455 . ?
B3 K4 O9 115.78(18) 2_455 . ?
B3 K4 O20 25.77(17) 2_455 2_455 ?
B24 K4 B4 108.5(2) . 2_565 ?
B24 K4 O20 84.03(19) . 2_455 ?
O7 K4 B3 27.31(17) . 2_455 ?
O7 K4 B3 111.55(19) 2_565 2_455 ?
O7 K4 B4 24.19(16) 2_565 2_565 ?
O7 K4 B4 109.52(19) . 2_565 ?
O7 K4 B24 128.1(2) . . ?
O7 K4 B24 131.0(2) 2_565 . ?
O7 K4 O7 94.93(15) . 2_565 ?
O7 K4 O9 110.14(14) 2_565 . ?
O7 K4 O9 104.71(14) . . ?
O7 K4 O10 120.02(16) . . ?
O7 K4 O10 49.42(14) 2_565 . ?
O7 K4 O13 128.43(16) . . ?
O7 K4 O20 44.43(13) . 2_455 ?
O7 K4 O20 136.93(15) 2_565 2_455 ?
O7 K4 O39 91.97(16) . . ?
O7 K4 O41 119.88(16) . . ?
O7 K4 O41 145.08(16) 2_565 . ?
O7 K4 O45 102.35(15) 2_565 2_455 ?
O7 K4 O45 49.55(13) . 2_455 ?
O9 K4 B4 121.80(18) . 2_565 ?
O9 K4 B24 83.35(18) . . ?
O9 K4 O20 96.38(14) . 2_455 ?
O10 K4 B3 113.90(19) . 2_455 ?
O10 K4 B4 25.28(16) . 2_565 ?
O10 K4 B24 85.27(19) . . ?
O10 K4 O9 130.32(15) . . ?
O10 K4 O20 130.20(15) . 2_455 ?
O10 K4 O41 107.89(15) . . ?
O10 K4 O45 87.93(15) . 2_455 ?
O13 K4 B3 101.21(19) . 2_455 ?
O13 K4 B4 88.72(18) . 2_565 ?
O13 K4 B24 23.66(18) . . ?
O13 K4 O7 112.76(16) . 2_565 ?
O13 K4 O9 104.98(14) . . ?
O13 K4 O10 63.96(15) . . ?
O13 K4 O20 91.11(15) . 2_455 ?
O13 K4 O39 137.90(18) . . ?
O13 K4 O41 48.51(14) . . ?
O13 K4 O45 81.47(15) . 2_455 ?
O20 K4 B4 140.45(18) 2_455 2_565 ?
O39 K4 B3 117.8(2) . 2_455 ?
O39 K4 B4 87.76(18) . 2_565 ?
O39 K4 B24 123.59(19) . . ?
O39 K4 O7 68.42(15) . 2_565 ?
O39 K4 O9 45.09(13) . . ?
O39 K4 O10 109.33(17) . . ?
O39 K4 O20 117.01(17) . 2_455 ?
O39 K4 O41 104.90(15) . . ?
O39 K4 O45 140.58(16) . 2_455 ?
O41 K4 B3 101.89(19) . 2_455 ?
O41 K4 B4 128.04(18) . 2_565 ?
O41 K4 B24 24.86(18) . . ?
O41 K4 O9 60.92(13) . . ?
O41 K4 O20 77.48(14) . 2_455 ?
O41 K4 O45 102.71(15) . 2_455 ?
O45 K4 B3 27.60(17) 2_455 2_455 ?
O45 K4 B4 96.88(18) 2_455 2_565 ?
O45 K4 B24 92.05(18) 2_455 . ?
O45 K4 O9 140.55(15) 2_455 . ?
O45 K4 O20 44.20(13) 2_455 2_455 ?
B1 K5 B6 81.7(2) 1_655 . ?
B1 K5 O26 80.31(17) 1_655 . ?
B26 K5 B1 115.8(2) 2_656 1_655 ?
B26 K5 B6 108.7(2) 2_656 . ?
B26 K5 O26 61.9(2) 2_656 . ?
B26 K5 O43 125.8(2) 2_656 2_666 ?
B26 K5 O46 101.2(2) 2_656 1_655 ?
O2 K5 B1 107.72(18) . 1_655 ?
O2 K5 B6 26.24(17) . . ?
O2 K5 B26 99.5(2) . 2_656 ?
O2 K5 O26 161.21(15) . . ?
O2 K5 O27 47.23(13) . . ?
O2 K5 O43 119.11(14) . 2_666 ?
O2 K5 O46 91.81(15) . 1_655 ?
O26 K5 B6 152.43(17) . . ?
O27 K5 B1 67.51(19) . 1_655 ?
O27 K5 B6 25.33(16) . . ?
O27 K5 B26 95.4(2) . 2_656 ?
O27 K5 O26 127.13(14) . . ?
O27 K5 O43 138.66(15) . 2_666 ?
O27 K5 O46 46.13(15) . 1_655 ?
O32 K5 B1 126.01(19) . 1_655 ?
O32 K5 B6 84.83(18) . . ?
O32 K5 B26 27.1(2) . 2_656 ?
O32 K5 O2 72.46(14) . . ?
O32 K5 O26 89.02(14) . . ?
O32 K5 O27 78.59(15) . . ?
O32 K5 O43 140.39(16) . 2_666 ?
O32 K5 O46 103.60(16) . 1_655 ?
O32 K5 O48 49.24(14) . . ?
O34 K5 B1 23.09(19) 1_655 1_655 ?
O34 K5 B6 99.20(19) 1_655 . ?
O34 K5 B26 123.0(2) 1_655 2_656 ?
O34 K5 O2 123.10(16) 1_655 . ?
O34 K5 O26 70.38(15) 1_655 . ?
O34 K5 O27 89.43(16) 1_655 . ?
O34 K5 O32 142.80(17) 1_655 . ?
O34 K5 O35 110.17(17) 1_655 . ?
O34 K5 O43 66.26(15) 1_655 2_666 ?
O34 K5 O46 47.81(16) 1_655 1_655 ?
O34 K5 O48 97.31(16) 1_655 . ?
O35 K5 B1 128.62(19) . 1_655 ?
O35 K5 B6 100.91(18) . . ?
O35 K5 B26 111.7(2) . 2_656 ?
O35 K5 O2 81.98(15) . . ?
O35 K5 O26 106.64(15) . . ?
O35 K5 O27 126.23(16) . . ?
O35 K5 O32 105.22(16) . . ?
O35 K5 O43 46.86(15) . 2_666 ?
O35 K5 O46 147.04(16) . 1_655 ?
O35 K5 O48 130.42(16) . . ?
O43 K5 B1 88.48(18) 2_666 1_655 ?
O43 K5 B6 122.97(18) 2_666 . ?
O43 K5 O26 77.27(14) 2_666 . ?
O46 K5 B1 24.83(19) 1_655 1_655 ?
O46 K5 B6 66.14(18) 1_655 . ?
O46 K5 O26 89.44(14) 1_655 . ?
O46 K5 O43 113.09(15) 1_655 2_666 ?
O48 K5 B1 91.11(17) . 1_655 ?
O48 K5 B6 114.79(19) . . ?
O48 K5 B26 25.86(19) . 2_656 ?
O48 K5 O2 116.54(16) . . ?
O48 K5 O26 45.23(14) . . ?
O48 K5 O27 93.26(15) . . ?
O48 K5 O43 121.47(16) . 2_666 ?
O48 K5 O46 81.23(15) . 1_655 ?
B15 K6 B5 117.1(2) 1_455 . ?
B15 K6 B17 90.1(2) 1_455 1_455 ?
B15 K6 B21 143.1(2) 1_455 1_655 ?
B15 K6 B23 80.6(2) 1_455 1_455 ?
B15 K6 B25 106.1(2) 1_455 . ?
B17 K6 B5 103.70(19) 1_455 . ?
B21 K6 B5 42.14(19) 1_655 . ?
B21 K6 B17 121.4(2) 1_655 1_455 ?
B21 K6 B23 84.4(2) 1_655 1_455 ?
B21 K6 B25 110.3(2) 1_655 . ?
B23 K6 B5 42.3(2) 1_455 . ?
B23 K6 B17 83.3(2) 1_455 1_455 ?
B23 K6 B25 123.4(2) 1_455 . ?
B25 K6 B5 124.8(2) . . ?
B25 K6 B17 41.61(18) . 1_455 ?
O6 K6 B5 83.70(16) . . ?
O6 K6 B15 86.50(17) . 1_455 ?
O6 K6 B17 24.65(14) . 1_455 ?
O6 K6 B21 113.70(17) . 1_655 ?
O6 K6 B23 58.70(18) . 1_455 ?
O6 K6 B25 65.59(16) . . ?
O15 K6 B5 25.07(15) . . ?
O15 K6 B15 141.93(18) . 1_455 ?
O15 K6 B17 101.92(17) . 1_455 ?
O15 K6 B21 24.51(16) . 1_655 ?
O15 K6 B23 65.38(19) . 1_455 ?
O15 K6 B25 106.76(19) . . ?
O15 K6 O6 89.89(14) . . ?
O21 K6 B5 119.75(19) . . ?
O21 K6 B15 95.6(2) . 1_455 ?
O21 K6 B17 22.70(16) . 1_455 ?
O21 K6 B21 121.0(2) . 1_655 ?
O21 K6 B23 106.0(2) . 1_455 ?
O21 K6 B25 19.61(17) . . ?
O21 K6 O6 47.29(13) . . ?
O21 K6 O15 109.44(16) . . ?
O21 K6 O25 121.99(17) . . ?
O21 K6 O27 81.77(17) . 1_455 ?
O23 K6 B5 121.78(18) . . ?
O23 K6 B15 25.91(17) . 1_455 ?
O23 K6 B17 111.60(19) . 1_455 ?
O23 K6 B21 126.8(2) . 1_655 ?
O23 K6 B23 97.5(2) . 1_455 ?
O23 K6 B25 112.3(2) . . ?
O23 K6 O6 112.10(16) . . ?
O23 K6 O15 140.37(16) . . ?
O23 K6 O21 109.62(18) . . ?
O23 K6 O25 104.09(17) . . ?
O23 K6 O27 52.03(15) . 1_455 ?
O25 K6 B5 22.49(17) . . ?
O25 K6 B15 95.03(19) . 1_455 ?
O25 K6 B17 100.75(18) . 1_455 ?
O25 K6 B21 62.85(18) . 1_655 ?
O25 K6 B23 22.7(2) . 1_455 ?
O25 K6 B25 135.0(2) . . ?
O25 K6 O6 76.81(15) . . ?
O25 K6 O15 47.48(15) . . ?
O25 K6 O27 83.67(17) . 1_455 ?
O27 K6 B5 105.61(18) 1_455 . ?
O27 K6 B15 26.15(17) 1_455 1_455 ?
O27 K6 B17 69.31(18) 1_455 1_455 ?
O27 K6 B21 145.8(2) 1_455 1_655 ?
O27 K6 B23 63.7(2) 1_455 1_455 ?
O27 K6 B25 98.09(19) 1_455 . ?
O27 K6 O6 60.97(14) 1_455 . ?
O27 K6 O15 128.99(16) 1_455 . ?
B15 K7 B25 111.0(2) . 1_655 ?
B15 K7 B26 105.5(2) . 2_756 ?
B26 K7 B25 130.6(2) 2_756 1_655 ?
O18 K7 B15 127.87(18) 2_656 . ?
O18 K7 B25 98.84(19) 2_656 1_655 ?
O18 K7 B26 83.28(18) 2_656 2_756 ?
O21 K7 B15 87.68(18) 1_655 . ?
O21 K7 B25 24.09(17) 1_655 1_655 ?
O21 K7 B26 149.67(19) 1_655 2_756 ?
O21 K7 O18 110.34(14) 1_655 2_656 ?
O23 K7 B15 26.87(17) 1_655 . ?
O23 K7 B25 106.29(19) 1_655 1_655 ?
O23 K7 B26 91.68(18) 1_655 2_756 ?
O23 K7 O18 150.52(14) 1_655 2_656 ?
O23 K7 O21 88.40(14) 1_655 1_655 ?
O23 K7 O24 71.85(13) 1_655 1_755 ?
O24 K7 B15 98.71(18) 1_755 . ?
O24 K7 B25 80.40(18) 1_755 1_655 ?
O24 K7 B26 61.79(19) 1_755 2_756 ?
O24 K7 O18 128.54(14) 1_755 2_656 ?
O24 K7 O21 89.64(15) 1_755 1_655 ?
O30 K7 B15 128.34(18) 2_756 . ?
O30 K7 B25 116.90(18) 2_756 1_655 ?
O30 K7 B26 24.80(18) 2_756 2_756 ?
O30 K7 O18 62.52(14) 2_756 2_656 ?
O30 K7 O21 140.89(15) 2_756 1_655 ?
O30 K7 O23 116.46(14) 2_756 1_655 ?
O30 K7 O24 72.12(15) 2_756 1_755 ?
O32 K7 B15 86.13(18) 1_655 . ?
O32 K7 B25 129.00(19) 1_655 1_655 ?
O32 K7 B26 24.73(18) 1_655 2_756 ?
O32 K7 O18 107.37(15) 1_655 2_656 ?
O32 K7 O21 136.38(16) 1_655 1_655 ?
O32 K7 O23 67.99(14) 1_655 1_655 ?
O32 K7 O24 49.02(15) 1_655 1_755 ?
O32 K7 O30 48.83(14) 1_655 2_756 ?
O32 K7 O47 107.44(16) 1_655 1_645 ?
O46 K7 B15 26.78(19) 1_655 . ?
O46 K7 B25 130.4(2) 1_655 1_655 ?
O46 K7 B26 96.3(2) 1_655 2_756 ?
O46 K7 O18 102.46(16) 1_655 2_656 ?
O46 K7 O21 106.42(17) 1_655 1_655 ?
O46 K7 O23 49.07(15) 1_655 1_655 ?
O46 K7 O24 116.97(16) 1_655 1_755 ?
O46 K7 O30 112.68(18) 1_655 2_756 ?
O46 K7 O32 85.70(18) 1_655 1_655 ?
O46 K7 O47 150.60(18) 1_655 1_645 ?
O46 K7 O48 90.95(18) 1_655 . ?
O47 K7 B15 125.7(2) 1_645 . ?
O47 K7 B25 24.07(17) 1_645 1_655 ?
O47 K7 B26 106.50(19) 1_645 2_756 ?
O47 K7 O18 98.51(15) 1_645 2_656 ?
O47 K7 O21 46.18(13) 1_645 1_655 ?
O47 K7 O23 110.73(16) 1_645 1_655 ?
O47 K7 O24 61.66(14) 1_645 1_755 ?
O47 K7 O30 95.19(15) 1_645 2_756 ?
O48 K7 B15 102.47(19) . . ?
O48 K7 B25 71.72(19) . 1_655 ?
O48 K7 B26 130.7(2) . 2_756 ?
O48 K7 O18 47.69(14) . 2_656 ?
O48 K7 O21 69.77(15) . 1_655 ?
O48 K7 O23 127.34(15) . 1_655 ?
O48 K7 O24 149.54(16) . 1_755 ?
O48 K7 O30 109.72(16) . 2_756 ?
O48 K7 O32 153.38(17) . 1_655 ?
O48 K7 O47 88.10(16) . 1_645 ?
B6 K8 B4 133.6(2) 1_345 2_355 ?
B8 K8 B4 91.5(2) 1_345 2_355 ?
B8 K8 B6 114.8(2) 1_345 1_345 ?
B8 K8 B16 102.9(2) 1_345 . ?
B8 K8 O10 114.27(17) 1_345 1_345 ?
B16 K8 B4 108.7(2) . 2_355 ?
B16 K8 B6 101.9(2) . 1_345 ?
B16 K8 O10 111.39(19) . 1_345 ?
O8 K8 B4 85.33(18) . 2_355 ?
O8 K8 B6 124.73(17) . 1_345 ?
O8 K8 B8 97.53(18) . 1_345 ?
O8 K8 B16 24.28(17) . . ?
O8 K8 O10 93.11(14) . 1_345 ?
O8 K8 O16 120.55(14) . 1_345 ?
O10 K8 B4 25.24(16) 1_345 2_355 ?
O10 K8 B6 110.56(18) 1_345 1_345 ?
O16 K8 B4 87.63(17) 1_345 2_355 ?
O16 K8 B6 101.52(17) 1_345 1_345 ?
O16 K8 B8 23.81(17) 1_345 1_345 ?
O16 K8 B16 126.32(19) 1_345 . ?
O16 K8 O10 104.20(13) 1_345 1_345 ?
O17 K8 B4 156.46(18) 1_345 2_355 ?
O17 K8 B6 26.28(17) 1_345 1_345 ?
O17 K8 B8 93.80(18) 1_345 1_345 ?
O17 K8 B16 92.43(18) 1_345 . ?
O17 K8 O8 116.56(14) 1_345 . ?
O17 K8 O10 136.40(14) 1_345 1_345 ?
O17 K8 O16 88.08(14) 1_345 1_345 ?
O22 K8 B4 132.06(19) . 2_355 ?
O22 K8 B6 85.84(18) . 1_345 ?
O22 K8 B8 93.64(19) . 1_345 ?
O22 K8 B16 24.34(19) . . ?
O22 K8 O8 46.74(15) . . ?
O22 K8 O10 135.00(15) . 1_345 ?
O22 K8 O16 113.35(16) . 1_345 ?
O22 K8 O17 70.45(15) . 1_345 ?
O22 K8 O33 70.03(15) . 1_345 ?
O22 K8 O40 142.18(17) . 1_345 ?
O22 K8 O42 87.78(17) . 1_345 ?
O33 K8 B4 114.19(18) 1_345 2_355 ?
O33 K8 B6 102.53(19) 1_345 1_345 ?
O33 K8 B8 25.44(17) 1_345 1_345 ?
O33 K8 B16 84.41(19) 1_345 . ?
O33 K8 O8 87.77(15) 1_345 . ?
O33 K8 O10 138.57(14) 1_345 1_345 ?
O33 K8 O16 43.51(13) 1_345 1_345 ?
O33 K8 O17 77.25(14) 1_345 1_345 ?
O40 K8 B4 25.78(18) 1_345 2_355 ?
O40 K8 B6 131.77(19) 1_345 1_345 ?
O40 K8 B8 69.16(19) 1_345 1_345 ?
O40 K8 B16 124.79(19) 1_345 . ?
O40 K8 O8 100.61(15) 1_345 . ?
O40 K8 O10 45.14(14) 1_345 1_345 ?
O40 K8 O16 61.98(15) 1_345 1_345 ?
O40 K8 O17 141.09(16) 1_345 1_345 ?
O40 K8 O33 93.99(16) 1_345 1_345 ?
O42 K8 B4 116.5(2) 1_345 2_355 ?
O42 K8 B6 25.50(18) 1_345 1_345 ?
O42 K8 B8 140.1(2) 1_345 1_345 ?
O42 K8 B16 94.53(19) 1_345 . ?
O42 K8 O8 111.73(16) 1_345 . ?
O42 K8 O10 91.36(15) 1_345 1_345 ?
O42 K8 O16 123.89(16) 1_345 1_345 ?
O42 K8 O17 49.35(15) 1_345 1_345 ?
O42 K8 O33 126.55(17) 1_345 1_345 ?
O42 K8 O40 127.31(18) 1_345 1_345 ?
K10 K9 B10 74.17(16) . . ?
K10 K9 B27 62.50(16) . . ?
B10 K9 B27 105.9(2) . . ?
B28 K9 K10 162.96(19) . . ?
B28 K9 B10 122.3(2) . . ?
B28 K9 B27 112.3(2) . . ?
B28 K9 O12 114.47(19) . . ?
B28 K9 O18 113.2(2) . . ?
B28 K9 O19 116.7(2) . . ?
B28 K9 O36 109.3(2) . 1_455 ?
O3 K9 K10 133.45(13) . . ?
O3 K9 B10 152.37(19) . . ?
O3 K9 B27 90.50(18) . . ?
O3 K9 B28 30.32(19) . . ?
O3 K9 O5 148.58(18) . . ?
O3 K9 O12 102.60(15) . . ?
O3 K9 O18 84.54(15) . . ?
O3 K9 O19 143.95(16) . . ?
O3 K9 O19 50.03(14) . 2_566 ?
O3 K9 O36 87.83(15) . 1_455 ?
O5 K9 K10 69.68(15) . . ?
O5 K9 B10 23.95(16) . . ?
O5 K9 B27 83.45(18) . . ?
O5 K9 B28 127.0(2) . . ?
O5 K9 O12 62.90(14) . . ?
O5 K9 O18 101.01(16) . . ?
O5 K9 O19 47.31(14) . . ?
O5 K9 O19 125.91(17) . 2_566 ?
O5 K9 O36 122.35(18) . 1_455 ?
O12 K9 K10 67.81(11) . . ?
O12 K9 B10 86.62(17) . . ?
O12 K9 B27 23.37(16) . . ?
O12 K9 O18 47.48(13) . . ?
O12 K9 O19 108.80(15) . . ?
O12 K9 O36 106.84(14) . 1_455 ?
O14 K9 K10 162.81(13) . . ?
O14 K9 B10 101.22(18) . . ?
O14 K9 B27 104.15(19) . . ?
O14 K9 B28 29.15(19) . . ?
O14 K9 O3 52.42(14) . . ?
O14 K9 O5 99.24(17) . . ?
O14 K9 O12 95.63(15) . . ?
O14 K9 O18 117.76(15) . . ?
O14 K9 O19 50.37(14) . 2_566 ?
O14 K9 O19 106.28(16) . . ?
O14 K9 O36 138.13(16) . 1_455 ?
O18 K9 K10 54.69(11) . . ?
O18 K9 B10 119.33(18) . . ?
O18 K9 B27 24.72(16) . . ?
O18 K9 O19 130.10(16) . . ?
O18 K9 O36 62.50(13) . 1_455 ?
O19 K9 K10 146.80(13) 2_566 . ?
O19 K9 K10 76.33(12) . . ?
O19 K9 B10 108.87(18) 2_566 . ?
O19 K9 B10 23.67(16) . . ?
O19 K9 B27 124.98(19) . . ?
O19 K9 B27 140.11(19) 2_566 . ?
O19 K9 B28 29.94(18) 2_566 . ?
O19 K9 O12 144.05(16) 2_566 . ?
O19 K9 O18 131.73(15) 2_566 . ?
O19 K9 O19 93.97(16) 2_566 . ?
O19 K9 O36 99.36(15) . 1_455 ?
O19 K9 O36 96.02(15) 2_566 1_455 ?
O36 K9 K10 55.64(12) 1_455 . ?
O36 K9 B10 114.69(18) 1_455 . ?
O36 K9 B27 86.63(17) 1_455 . ?
K9 K10 K7 114.34(7) . 2_656 ?
K9 K10 B9 174.23(15) . 2_566 ?
K9 K10 B11 66.36(17) . 1_455 ?
K9 K10 B27 63.94(15) . . ?
K9 K10 O5 50.55(11) . . ?
K9 K10 O12 52.91(9) . . ?
B9 K10 K7 70.60(15) 2_566 2_656 ?
B9 K10 B11 109.8(2) 2_566 1_455 ?
B9 K10 B27 121.8(2) 2_566 . ?
B9 K10 O5 128.84(18) 2_566 . ?
B9 K10 O12 132.24(16) 2_566 . ?
B11 K10 K7 107.00(16) 1_455 2_656 ?
B11 K10 B27 111.4(2) 1_455 . ?
B11 K10 O5 104.55(18) 1_455 . ?
B11 K10 O12 115.29(19) 1_455 . ?
B27 K10 K7 59.33(14) . 2_656 ?
O1 K10 K7 96.51(11) 2_566 2_656 ?
O1 K10 K9 149.15(13) 2_566 . ?
O1 K10 B9 26.13(17) 2_566 2_566 ?
O1 K10 B11 106.1(2) 2_566 1_455 ?
O1 K10 B27 139.82(18) 2_566 . ?
O1 K10 O5 108.21(16) 2_566 . ?
O1 K10 O12 137.26(15) 2_566 . ?
O1 K10 O18 151.75(16) 2_566 . ?
O1 K10 O36 123.44(17) 2_566 1_455 ?
O1 K10 O38 91.48(16) 2_566 2_566 ?
O1 K10 O47 49.71(14) 2_566 2_566 ?
O5 K10 K7 132.16(10) . 2_656 ?
O5 K10 B27 76.08(17) . . ?
O12 K10 K7 81.85(9) . 2_656 ?
O12 K10 B27 23.98(16) . . ?
O12 K10 O5 52.17(12) . . ?
O18 K10 K7 55.65(11) . 2_656 ?
O18 K10 K9 58.87(11) . . ?
O18 K10 B9 126.23(19) . 2_566 ?
O18 K10 B11 88.6(2) . 1_455 ?
O18 K10 B27 24.69(17) . . ?
O18 K10 O5 90.57(15) . . ?
O18 K10 O12 43.51(13) . . ?
O18 K10 O36 66.19(15) . 1_455 ?
O18 K10 O38 109.26(16) . 2_566 ?
O18 K10 O47 102.12(15) . 2_566 ?
O36 K10 K7 88.76(11) 1_455 2_656 ?
O36 K10 K9 60.61(12) 1_455 . ?
O36 K10 B9 117.71(19) 1_455 2_566 ?
O36 K10 B11 23.17(18) 1_455 1_455 ?
O36 K10 B27 90.01(18) 1_455 . ?
O36 K10 O5 108.88(15) 1_455 . ?
O36 K10 O12 99.28(14) 1_455 . ?
O36 K10 O38 46.60(14) 1_455 2_566 ?
O36 K10 O47 122.87(16) 1_455 2_566 ?
O38 K10 K7 128.53(14) 2_566 2_656 ?
O38 K10 K9 70.00(13) 2_566 . ?
O38 K10 B9 104.71(18) 2_566 2_566 ?
O38 K10 B11 23.91(18) 2_566 1_455 ?
O38 K10 B27 128.66(19) 2_566 . ?
O38 K10 O5 91.88(15) 2_566 . ?
O38 K10 O12 122.89(15) 2_566 . ?
O38 K10 O47 128.89(17) 2_566 2_566 ?
O47 K10 K7 48.59(10) 2_566 2_656 ?
O47 K10 K9 158.99(12) 2_566 . ?
O47 K10 B9 26.78(16) 2_566 2_566 ?
O47 K10 B11 126.1(2) 2_566 1_455 ?
O47 K10 B27 95.06(17) 2_566 . ?
O47 K10 O5 127.59(15) 2_566 . ?
O47 K10 O12 107.74(13) 2_566 . ?
Rb1 K11 B22 68.62(16) . 1_545 ?
B20 K11 Rb1 160.25(16) 2_455 . ?
B20 K11 B22 98.2(2) 2_455 1_545 ?
B20 K11 O20 135.70(19) 2_455 . ?
O9 K11 Rb1 145.05(12) 2_455 . ?
O9 K11 B20 29.34(18) 2_455 2_455 ?
O9 K11 B22 76.78(19) 2_455 1_545 ?
O9 K11 O11 141.46(16) 2_455 . ?
O9 K11 O15 122.52(16) 2_455 . ?
O9 K11 O20 112.64(15) 2_455 . ?
O9 K11 O29 52.46(14) 2_455 2_455 ?
O9 K11 O29 139.49(16) 2_455 . ?
O9 K11 O31 90.55(15) 2_455 . ?
O9 K11 O41 65.64(15) 2_455 2_455 ?
O9 K11 O45 77.99(15) 2_455 1_655 ?
O11 K11 Rb1 59.75(11) . . ?
O11 K11 B20 138.87(19) . 2_455 ?
O11 K11 B22 119.31(19) . 1_545 ?
O11 K11 O15 95.65(15) . . ?
O11 K11 O20 44.19(13) . . ?
O11 K11 O31 96.05(14) . . ?
O11 K11 O41 78.31(15) . 2_455 ?
O11 K11 O45 131.81(16) . 1_655 ?
O15 K11 Rb1 56.37(11) . . ?
O15 K11 B20 108.06(19) . 2_455 ?
O15 K11 B22 79.56(18) . 1_545 ?
O15 K11 O20 115.69(15) . . ?
O15 K11 O41 151.34(14) . 2_455 ?
O15 K11 O45 60.75(14) . 1_655 ?
O20 K11 Rb1 59.63(11) . . ?
O20 K11 B22 83.56(18) . 1_545 ?
O29 K11 Rb1 160.64(12) 2_455 . ?
O29 K11 Rb1 70.09(11) . . ?
O29 K11 B20 27.61(18) 2_455 2_455 ?
O29 K11 B20 110.21(19) . 2_455 ?
O29 K11 B22 125.76(19) 2_455 1_545 ?
O29 K11 B22 126.20(19) . 1_545 ?
O29 K11 O11 112.75(15) 2_455 . ?
O29 K11 O11 61.99(14) . . ?
O29 K11 O15 48.88(13) . . ?
O29 K11 O15 110.12(15) 2_455 . ?
O29 K11 O20 129.45(15) 2_455 . ?
O29 K11 O20 103.59(15) . . ?
O29 K11 O29 90.59(16) 2_455 . ?
O29 K11 O31 124.34(16) . . ?
O29 K11 O31 143.01(16) 2_455 . ?
O29 K11 O41 50.02(14) 2_455 2_455 ?
O29 K11 O41 105.58(15) . 2_455 ?
O29 K11 O45 109.63(15) . 1_655 ?
O29 K11 O45 114.76(15) 2_455 1_655 ?
O31 K11 Rb1 55.41(11) . . ?
O31 K11 B20 117.13(19) . 2_455 ?
O31 K11 B22 24.44(17) . 1_545 ?
O31 K11 O15 88.54(15) . . ?
O31 K11 O20 59.37(13) . . ?
O31 K11 O41 119.80(15) . 2_455 ?
O31 K11 O45 46.72(13) . 1_655 ?
O41 K11 Rb1 134.97(12) 2_455 . ?
O41 K11 B20 64.67(18) 2_455 2_455 ?
O41 K11 B22 127.97(19) 2_455 1_545 ?
O41 K11 O20 79.45(15) 2_455 . ?
O41 K11 O45 141.82(16) 2_455 1_655 ?
O45 K11 Rb1 72.63(11) 1_655 . ?
O45 K11 B20 89.32(18) 1_655 2_455 ?
O45 K11 B22 24.38(18) 1_655 1_545 ?
O45 K11 O20 105.62(14) 1_655 . ?
K5 B1 K3 134.1(3) 1_455 . ?
O34 B1 K3 131.5(5) . . ?
O34 B1 K5 49.5(4) . 1_455 ?
O34 B1 O35 121.3(7) . . ?
O34 B1 O46 118.6(7) . . ?
O35 B1 K3 45.3(3) . . ?
O35 B1 K5 169.3(6) . 1_455 ?
O35 B1 O46 120.1(7) . . ?
O46 B1 K3 93.9(5) . . ?
O46 B1 K5 69.5(4) . 1_455 ?
O12 B2 K1 62.9(4) . . ?
O12 B2 O28 107.8(6) . . ?
O12 B2 O30 112.6(6) . . ?
O12 B2 O36 114.3(6) . . ?
O28 B2 K1 57.4(4) . . ?
O28 B2 O30 106.4(6) . . ?
O28 B2 O36 108.8(6) . . ?
O30 B2 K1 156.0(5) . . ?
O36 B2 K1 96.0(4) . . ?
O36 B2 O30 106.7(6) . . ?
O7 B3 K4 60.1(4) 2_455 2_455 ?
O7 B3 O8 109.7(6) 2_455 . ?
O7 B3 O20 108.5(6) 2_455 . ?
O7 B3 O45 110.9(7) 2_455 . ?
O8 B3 K4 164.6(5) . 2_455 ?
O20 B3 K4 83.8(4) . 2_455 ?
O20 B3 O8 111.2(7) . . ?
O20 B3 O45 109.7(6) . . ?
O45 B3 K4 69.6(4) . 2_455 ?
O45 B3 O8 106.9(6) . . ?
K4 B4 Rb1 160.5(3) 2_565 2_455 ?
K4 B4 K8 124.9(2) 2_565 2_355 ?
K8 B4 Rb1 74.36(17) 2_355 2_455 ?
O7 B4 Rb1 107.5(4) . 2_455 ?
O7 B4 K4 53.5(3) . 2_565 ?
O7 B4 K8 162.5(5) . 2_355 ?
O7 B4 O10 109.4(6) . 2_565 ?
O7 B4 O31 113.0(6) . 2_455 ?
O7 B4 O40 110.8(6) . 2_565 ?
O10 B4 Rb1 142.1(5) 2_565 2_455 ?
O10 B4 K4 56.1(4) 2_565 2_565 ?
O10 B4 K8 73.2(4) 2_565 2_355 ?
O10 B4 O31 110.0(6) 2_565 2_455 ?
O10 B4 O40 106.1(6) 2_565 2_565 ?
O31 B4 Rb1 45.3(3) 2_455 2_455 ?
O31 B4 K4 132.9(5) 2_455 2_565 ?
O31 B4 K8 81.0(4) 2_455 2_355 ?
O31 B4 O40 107.3(6) 2_455 2_565 ?
O40 B4 Rb1 67.9(4) 2_565 2_455 ?
O40 B4 K4 119.7(5) 2_565 2_565 ?
O40 B4 K8 53.1(3) 2_565 2_355 ?
K6 B5 Rb1 64.13(14) . . ?
K11 B5 Rb1 54.89(12) . . ?
K11 B5 Rb1 118.3(2) 2_455 . ?
K11 B5 K6 113.5(2) . . ?
K11 B5 K6 177.3(3) 2_455 . ?
K11 B5 K11 69.17(17) 2_455 . ?
O15 B5 Rb1 52.5(3) . . ?
O15 B5 K6 64.6(4) . . ?
O15 B5 K11 58.9(3) . . ?
O15 B5 K11 117.5(5) . 2_455 ?
O15 B5 O41 108.6(6) . . ?
O25 B5 Rb1 87.1(4) . . ?
O25 B5 K6 43.8(3) . . ?
O25 B5 K11 134.2(5) . 2_455 ?
O25 B5 K11 140.7(5) . . ?
O25 B5 O15 108.2(6) . . ?
O25 B5 O41 106.6(6) . . ?
O29 B5 Rb1 73.8(4) . . ?
O29 B5 K6 130.8(5) . . ?
O29 B5 K11 50.8(3) . 2_455 ?
O29 B5 K11 51.8(3) . . ?
O29 B5 O15 108.3(6) . . ?
O29 B5 O25 112.9(6) . . ?
O29 B5 O41 112.0(6) . . ?
O41 B5 Rb1 160.2(5) . . ?
O41 B5 K6 116.3(4) . . ?
O41 B5 K11 112.7(5) . . ?
O41 B5 K11 61.8(3) . 2_455 ?
K5 B6 K3 66.06(16) . . ?
K5 B6 K8 132.1(3) . 1_765 ?
K8 B6 K3 66.43(15) 1_765 . ?
O2 B6 K3 58.0(3) . . ?
O2 B6 K5 63.6(4) . . ?
O2 B6 K8 95.5(4) . 1_765 ?
O2 B6 O17 105.0(6) . . ?
O2 B6 O42 109.1(6) . . ?
O17 B6 K3 47.0(3) . . ?
O17 B6 K5 84.9(4) . . ?
O17 B6 K8 58.1(3) . 1_765 ?
O27 B6 K3 129.3(5) . . ?
O27 B6 K5 66.7(4) . . ?
O27 B6 K8 151.1(5) . 1_765 ?
O27 B6 O2 113.3(6) . . ?
O27 B6 O17 111.8(6) . . ?
O27 B6 O42 112.8(6) . . ?
O42 B6 K3 116.9(4) . . ?
O42 B6 K5 170.0(5) . . ?
O42 B6 K8 53.0(3) . 1_765 ?
O42 B6 O17 104.1(6) . . ?
K2 B7 K8 74.90(17) . 1_665 ?
K3 B7 K2 86.64(19) . . ?
K3 B7 K8 141.0(3) . 1_665 ?
O1 B7 K2 117.6(5) . . ?
O1 B7 K3 67.1(4) . . ?
O1 B7 K8 91.2(4) . 1_665 ?
O4 B7 K2 55.4(4) . . ?
O4 B7 K3 52.9(4) . . ?
O4 B7 K8 129.1(5) . 1_665 ?
O4 B7 O1 119.3(6) . . ?
O17 B7 K2 98.2(5) 1_455 . ?
O17 B7 K3 167.7(5) 1_455 . ?
O17 B7 K8 51.2(3) 1_455 1_665 ?
O17 B7 O1 119.4(6) 1_455 . ?
O17 B7 O4 121.3(7) 1_455 . ?
K3 B8 Rb1 144.1(3) . 1_665 ?
K8 B8 Rb1 77.21(19) 1_765 1_665 ?
K8 B8 K3 67.52(16) 1_765 . ?
O16 B8 Rb1 120.9(5) . 1_665 ?
O16 B8 K3 45.7(3) . . ?
O16 B8 K8 77.2(4) . 1_765 ?
O16 B8 O24 127.7(7) . 1_665 ?
O16 B8 O33 112.4(6) . . ?
O24 B8 Rb1 51.3(4) 1_665 1_665 ?
O24 B8 K3 163.6(6) 1_665 . ?
O24 B8 K8 128.4(5) 1_665 1_765 ?
O24 B8 O33 119.9(7) 1_665 . ?
O33 B8 Rb1 98.8(5) . 1_665 ?
O33 B8 K3 69.5(4) . . ?
O33 B8 K8 60.0(4) . 1_765 ?
K10 B9 K3 73.08(17) 2_566 . ?
O1 B9 K3 60.7(3) . . ?
O1 B9 K10 52.9(3) . 2_566 ?
O1 B9 O16 107.2(5) . . ?
O1 B9 O47 109.5(6) . . ?
O16 B9 K3 47.6(3) . . ?
O16 B9 K10 92.1(4) . 2_566 ?
O16 B9 O47 108.0(6) . . ?
O22 B9 K3 115.9(4) 1_665 . ?
O22 B9 K10 154.5(5) 1_665 2_566 ?
O22 B9 O1 108.7(6) 1_665 . ?
O22 B9 O16 111.6(6) 1_665 . ?
O22 B9 O47 111.8(6) 1_665 . ?
O47 B9 K3 131.8(5) . . ?
O47 B9 K10 66.7(4) . 2_566 ?
O5 B10 K9 55.0(4) . . ?
O19 B10 K9 60.8(4) . . ?
O19 B10 O5 114.7(7) . . ?
O43 B10 K9 168.7(6) . . ?
O43 B10 O5 120.9(6) . . ?
O43 B10 O19 124.4(6) . . ?
K10 B11 K9 54.20(14) 1_655 1_655 ?
O5 B11 K9 139.6(6) . 1_655 ?
O5 B11 K10 166.1(6) . 1_655 ?
O36 B11 K9 57.6(4) . 1_655 ?
O36 B11 K10 59.2(4) . 1_655 ?
O36 B11 O5 122.9(8) . . ?
O36 B11 O38 118.0(7) . 2_666 ?
O38 B11 K9 76.1(4) 2_666 1_655 ?
O38 B11 K10 60.6(4) 2_666 1_655 ?
O38 B11 O5 119.1(7) 2_666 . ?
K1 B12 K7 114.7(2) 2_656 2_756 ?
K1 B12 K9 135.2(3) 2_656 1_655 ?
K9 B12 K7 108.6(2) 1_655 2_756 ?
O18 B12 K1 166.6(5) 1_655 2_656 ?
O18 B12 K7 60.7(4) 1_655 2_756 ?
O18 B12 K9 54.0(4) 1_655 1_655 ?
O18 B12 O44 120.1(7) 1_655 . ?
O28 B12 K1 67.5(4) . 2_656 ?
O28 B12 K7 104.6(5) . 2_756 ?
O28 B12 K9 91.4(4) . 1_655 ?
O28 B12 O18 125.2(7) . 1_655 ?
O28 B12 O44 114.8(7) . . ?
O44 B12 K1 47.4(3) . 2_656 ?
O44 B12 K7 105.8(5) . 2_756 ?
O44 B12 K9 129.1(5) . 1_655 ?
K1 B13 K3 137.7(3) . . ?
K1 B13 K5 74.13(16) . . ?
K3 B13 K5 63.74(16) . . ?
O14 B13 K1 58.2(3) . . ?
O14 B13 K3 152.1(5) . . ?
O14 B13 K5 121.8(4) . . ?
O14 B13 O35 111.7(6) . . ?
O14 B13 O38 112.6(6) . . ?
O14 B13 O43 110.0(6) . 2_666 ?
O35 B13 K1 102.4(4) . . ?
O35 B13 K3 49.6(3) . . ?
O35 B13 K5 46.3(3) . . ?
O35 B13 O38 107.8(6) . . ?
O35 B13 O43 105.3(6) . 2_666 ?
O38 B13 K1 149.5(5) . . ?
O38 B13 K3 65.1(4) . . ?
O38 B13 K5 125.1(5) . . ?
O43 B13 K1 57.1(3) 2_666 . ?
O43 B13 K3 96.2(5) 2_666 . ?
O43 B13 K5 59.2(4) 2_666 . ?
O43 B13 O38 109.2(6) 2_666 . ?
O3 B14 K1 65.5(4) 1_655 . ?
O3 B14 O44 118.1(7) 1_655 2_756 ?
O26 B14 K1 59.5(4) . . ?
O26 B14 O3 121.9(6) . 1_655 ?
O26 B14 O44 120.0(7) . 2_756 ?
O44 B14 K1 160.7(6) 2_756 . ?
K6 B15 K2 73.21(19) 1_655 1_655 ?
K7 B15 K2 134.2(3) . 1_655 ?
K7 B15 K6 66.27(17) . 1_655 ?
O4 B15 K2 58.6(4) 1_655 1_655 ?
O4 B15 K6 131.1(5) 1_655 1_655 ?
O4 B15 K7 160.1(5) 1_655 . ?
O23 B15 K2 69.8(4) 1_655 1_655 ?
O23 B15 K6 50.5(3) 1_655 1_655 ?
O23 B15 K7 68.3(4) 1_655 . ?
O23 B15 O4 113.2(6) 1_655 1_655 ?
O27 B15 K2 88.0(4) . 1_655 ?
O27 B15 K6 55.7(4) . 1_655 ?
O27 B15 K7 86.4(4) . . ?
O27 B15 O4 111.2(6) . 1_655 ?
O27 B15 O23 106.1(6) . 1_655 ?
O27 B15 O46 109.6(6) . 1_655 ?
O46 B15 K2 161.7(5) 1_655 1_655 ?
O46 B15 K6 120.4(5) 1_655 1_655 ?
O46 B15 K7 54.7(3) 1_655 . ?
O46 B15 O4 108.5(6) 1_655 1_655 ?
O46 B15 O23 108.2(6) 1_655 1_655 ?
K8 B16 K2 77.79(18) . 1_445 ?
O8 B16 K2 124.5(5) . 1_445 ?
O8 B16 K8 69.8(4) . . ?
O8 B16 O22 117.5(7) . . ?
O8 B16 O40 122.3(7) . 1_445 ?
O22 B16 K2 72.4(4) . 1_445 ?
O22 B16 K8 55.1(4) . . ?
O40 B16 K2 70.4(4) 1_445 1_445 ?
O40 B16 K8 147.0(5) 1_445 . ?
O40 B16 O22 119.9(7) 1_445 . ?
Rb1 B17 K6 67.77(16) 1_655 1_655 ?
Rb1 B17 K7 114.7(2) 1_655 1_455 ?
K7 B17 K6 163.5(3) 1_455 1_655 ?
O6 B17 Rb1 62.9(4) 1_655 1_655 ?
O6 B17 K6 66.7(3) 1_655 1_655 ?
O6 B17 K7 99.3(4) 1_655 1_455 ?
O6 B17 O21 108.8(6) 1_655 1_655 ?
O6 B17 O24 109.8(6) 1_655 1_655 ?
O6 B17 O32 110.5(6) 1_655 . ?
O21 B17 Rb1 83.5(4) 1_655 1_655 ?
O21 B17 K6 42.3(3) 1_655 1_655 ?
O21 B17 K7 151.5(5) 1_655 1_455 ?
O21 B17 O24 108.8(6) 1_655 1_655 ?
O24 B17 Rb1 65.3(4) 1_655 1_655 ?
O24 B17 K6 127.1(5) 1_655 1_655 ?
O24 B17 K7 64.5(3) 1_655 1_455 ?
O32 B17 Rb1 167.0(5) . 1_655 ?
O32 B17 K6 121.3(5) . 1_655 ?
O32 B17 K7 53.8(3) . 1_455 ?
O32 B17 O21 109.5(6) . 1_655 ?
O32 B17 O24 109.5(6) . 1_655 ?
K2 B18 K6 67.53(15) . . ?
K5 B18 K2 134.0(2) . . ?
K5 B18 K6 138.7(2) . . ?
O2 B18 K2 82.5(4) . . ?
O2 B18 K5 59.3(4) . . ?
O2 B18 K6 148.2(5) . . ?
O2 B18 O6 122.7(6) . 1_655 ?
O2 B18 O23 120.4(7) . . ?
O6 B18 K2 121.0(5) 1_655 . ?
O6 B18 K5 101.9(4) 1_655 . ?
O6 B18 K6 83.4(4) 1_655 . ?
O23 B18 K2 63.3(4) . . ?
O23 B18 K5 113.2(5) . . ?
O23 B18 K6 36.2(3) . . ?
O23 B18 O6 116.7(6) . 1_655 ?
K4 B19 K4 141.3(3) . 1_455 ?
K4 B19 K8 100.3(2) . 1_665 ?
K8 B19 K4 118.1(2) 1_665 1_455 ?
O9 B19 K4 93.2(4) . 1_455 ?
O9 B19 K4 65.0(4) . . ?
O9 B19 K8 114.8(5) . 1_665 ?
O9 B19 O39 114.0(6) . . ?
O10 B19 K4 167.5(6) 1_455 . ?
O10 B19 K4 49.9(4) 1_455 1_455 ?
O10 B19 K8 69.7(4) 1_455 1_665 ?
O10 B19 O9 125.6(7) 1_455 . ?
O10 B19 O39 120.5(6) 1_455 . ?
O39 B19 K4 49.3(3) . . ?
O39 B19 K4 133.2(5) . 1_455 ?
O39 B19 K8 85.3(5) . 1_665 ?
K11 B20 K2 151.3(3) 2_455 1_455 ?
O9 B20 K2 105.8(4) . 1_455 ?
O9 B20 K11 61.0(4) . 2_455 ?
O13 B20 K2 66.2(4) 1_455 1_455 ?
O13 B20 K11 92.3(5) 1_455 2_455 ?
O13 B20 O9 107.3(6) 1_455 . ?
O13 B20 O37 109.0(6) 1_455 1_455 ?
O29 B20 K2 142.5(5) . 1_455 ?
O29 B20 K11 62.4(4) . 2_455 ?
O29 B20 O9 109.4(6) . . ?
O29 B20 O13 113.6(6) . 1_455 ?
O29 B20 O37 111.3(6) . 1_455 ?
O37 B20 K2 45.0(3) 1_455 1_455 ?
O37 B20 K11 158.0(5) 1_455 2_455 ?
O37 B20 O9 105.9(6) 1_455 . ?
K6 B21 Rb1 71.97(17) 1_455 . ?
K6 B21 K11 124.8(3) 1_455 . ?
K11 B21 Rb1 55.11(12) . . ?
O11 B21 Rb1 60.0(3) . . ?
O11 B21 K6 85.3(5) . 1_455 ?
O11 B21 K11 56.7(4) . . ?
O15 B21 Rb1 146.0(6) 1_455 . ?
O15 B21 K6 74.0(4) 1_455 1_455 ?
O15 B21 K11 156.5(5) 1_455 . ?
O15 B21 O11 118.0(7) 1_455 . ?
O20 B21 Rb1 63.4(4) . . ?
O20 B21 K6 106.4(5) . 1_455 ?
O20 B21 K11 65.2(4) . . ?
O20 B21 O11 114.4(6) . . ?
O20 B21 O15 127.3(7) . 1_455 ?
K11 B22 Rb1 55.09(13) 1_565 1_565 ?
O31 B22 Rb1 45.2(4) 1_565 1_565 ?
O31 B22 K11 63.5(4) 1_565 1_565 ?
O31 B22 O39 119.7(7) 1_565 . ?
O39 B22 Rb1 152.1(5) . 1_565 ?
O39 B22 K11 147.9(6) . 1_565 ?
O45 B22 Rb1 80.7(4) 1_665 1_565 ?
O45 B22 K11 66.6(4) 1_665 1_565 ?
O45 B22 O31 120.8(7) 1_665 1_565 ?
O45 B22 O39 119.5(7) 1_665 . ?
K2 B23 K8 75.5(2) 1_655 1_765 ?
K6 B23 K2 71.7(2) 1_655 1_655 ?
K6 B23 K8 132.3(3) 1_655 1_765 ?
O25 B23 K2 67.7(4) 1_655 1_655 ?
O25 B23 K6 48.6(4) 1_655 1_655 ?
O25 B23 K8 139.7(6) 1_655 1_765 ?
O25 B23 O42 117.4(8) 1_655 . ?
O37 B23 K2 148.9(6) . 1_655 ?
O37 B23 K6 138.0(6) . 1_655 ?
O37 B23 K8 83.8(5) . 1_765 ?
O37 B23 O25 120.9(8) . 1_655 ?
O37 B23 O42 121.3(8) . . ?
O42 B23 K2 56.2(4) . 1_655 ?
O42 B23 K6 87.0(5) . 1_655 ?
O42 B23 K8 45.7(4) . 1_765 ?
K4 B24 K2 71.70(17) . . ?
O11 B24 K2 106.6(5) 1_655 . ?
O11 B24 K4 178.2(6) 1_655 . ?
O13 B24 K2 62.6(4) . . ?
O13 B24 K4 58.4(4) . . ?
O13 B24 O11 121.5(7) . 1_655 ?
O13 B24 O41 121.6(7) . . ?
O41 B24 K2 100.0(5) . . ?
O41 B24 K4 63.2(4) . . ?
O41 B24 O11 116.8(7) . 1_655 ?
K7 B25 K6 63.24(17) 1_455 . ?
O21 B25 K6 40.2(4) . . ?
O21 B25 K7 68.0(4) . 1_455 ?
O21 B25 O33 119.5(7) . 1_445 ?
O21 B25 O47 118.3(7) . 1_545 ?
O33 B25 K6 144.7(6) 1_445 . ?
O33 B25 K7 147.2(6) 1_445 1_455 ?
O47 B25 K6 87.0(5) 1_545 . ?
O47 B25 K7 58.5(4) 1_545 1_455 ?
O47 B25 O33 122.0(7) 1_545 1_445 ?
K5 B26 K7 92.4(2) 2_656 2_756 ?
O30 B26 K5 134.5(5) . 2_656 ?
O30 B26 K7 64.1(4) . 2_756 ?
O30 B26 O32 117.6(7) . 2_656 ?
O32 B26 K5 66.4(4) 2_656 2_656 ?
O32 B26 K7 56.1(4) 2_656 2_756 ?
O48 B26 K5 68.5(4) 2_656 2_656 ?
O48 B26 K7 159.0(6) 2_656 2_756 ?
O48 B26 O30 123.0(7) 2_656 . ?
O48 B26 O32 119.2(7) 2_656 2_656 ?
K9 B27 K7 109.2(2) . 2_656 ?
K10 B27 K7 63.62(16) . 2_656 ?
K10 B27 K9 53.57(12) . . ?
O12 B27 K7 133.4(5) . 2_656 ?
O12 B27 K9 54.3(3) . . ?
O12 B27 K10 74.9(4) . . ?
O12 B27 O18 107.8(6) . . ?
O12 B27 O26 114.6(7) . 2_656 ?
O12 B27 O48 110.9(6) . 2_656 ?
O18 B27 K7 61.8(4) . 2_656 ?
O18 B27 K9 55.5(3) . . ?
O18 B27 K10 51.7(3) . . ?
O18 B27 O48 106.6(6) . 2_656 ?
O26 B27 K7 111.3(4) 2_656 2_656 ?
O26 B27 K9 118.2(5) 2_656 . ?
O26 B27 K10 162.1(5) 2_656 . ?
O26 B27 O18 110.4(6) 2_656 . ?
O26 B27 O48 106.2(6) 2_656 2_656 ?
O48 B27 K7 46.0(3) 2_656 2_656 ?
O48 B27 K9 135.5(5) 2_656 . ?
O48 B27 K10 82.8(4) 2_656 . ?
O3 B28 K9 70.6(4) . . ?
O14 B28 K9 66.2(4) . . ?
O14 B28 O3 111.8(6) . . ?
O14 B28 O19 108.3(6) . 2_566 ?
O14 B28 O34 112.4(7) . . ?
O19 B28 K9 73.3(4) 2_566 . ?
O19 B28 O3 106.5(6) 2_566 . ?
O34 B28 K9 176.0(5) . . ?
O34 B28 O3 107.1(6) . . ?
O34 B28 O19 110.7(6) . 2_566 ?
K10 O1 K3 89.53(15) 2_566 . ?
B7 O1 K3 87.8(4) . . ?
B7 O1 K10 137.7(4) . 2_566 ?
B7 O1 B9 121.4(6) . . ?
B9 O1 K3 94.1(3) . . ?
B9 O1 K10 100.9(4) . 2_566 ?
K3 O2 K5 77.14(14) . . ?
B6 O2 K3 97.2(4) . . ?
B6 O2 K5 90.2(4) . . ?
B18 O2 K3 133.5(4) . . ?
B18 O2 K5 97.8(4) . . ?
B18 O2 B6 129.2(6) . . ?
K9 O3 K1 110.07(17) . 1_455 ?
B14 O3 K1 89.5(4) 1_455 1_455 ?
B14 O3 K9 135.1(5) 1_455 . ?
B14 O3 B28 118.9(6) 1_455 . ?
B28 O3 K1 130.3(4) . 1_455 ?
B28 O3 K9 79.1(4) . . ?
K3 O4 K2 111.42(17) . . ?
B7 O4 K2 101.8(4) . . ?
B7 O4 K3 103.3(4) . . ?
B7 O4 B15 119.1(6) . 1_455 ?
B15 O4 K2 95.2(4) 1_455 . ?
B15 O4 K3 123.6(4) 1_455 . ?
K9 O5 K10 59.77(11) . . ?
B10 O5 K9 101.0(4) . . ?
B10 O5 K10 101.3(4) . . ?
B10 O5 B11 120.0(6) . . ?
B11 O5 K9 137.6(5) . . ?
B11 O5 K10 116.8(5) . . ?
Rb1 O6 K6 76.01(12) . . ?
B17 O6 Rb1 90.7(4) 1_455 . ?
B17 O6 K6 88.7(4) 1_455 . ?
B18 O6 Rb1 138.8(4) 1_455 . ?
B18 O6 K6 126.6(4) 1_455 . ?
B18 O6 B17 120.2(6) 1_455 1_455 ?
K4 O7 K4 85.07(15) . 2_565 ?
B3 O7 K4 129.6(4) 2_455 2_565 ?
B3 O7 K4 92.6(4) 2_455 . ?
B4 O7 K4 102.3(4) . 2_565 ?
B4 O7 K4 128.9(4) . . ?
B4 O7 B3 117.1(6) . 2_455 ?
B3 O8 K8 138.1(4) . . ?
B16 O8 K8 85.9(4) . . ?
B16 O8 B3 116.7(6) . . ?
K11 O9 K4 79.12(13) 2_455 . ?
B19 O9 K4 92.2(4) . . ?
B19 O9 K11 134.2(5) . 2_455 ?
B19 O9 B20 123.8(6) . . ?
B20 O9 K4 136.1(4) . . ?
B20 O9 K11 89.6(4) . 2_455 ?
K2 O10 K8 73.30(13) . 1_765 ?
K4 O10 K2 85.47(14) . . ?
K4 O10 K8 157.81(19) . 1_765 ?
B4 O10 K2 106.2(4) 2_565 . ?
B4 O10 K4 98.7(4) 2_565 . ?
B4 O10 K8 81.6(4) 2_565 1_765 ?
B19 O10 K2 122.2(4) 1_655 . ?
B19 O10 K4 109.2(5) 1_655 . ?
B19 O10 K8 88.1(5) 1_655 1_765 ?
B19 O10 B4 124.8(6) 1_655 2_565 ?
K11 O11 Rb1 65.03(11) . . ?
B21 O11 Rb1 96.7(4) . . ?
B21 O11 K11 99.7(4) . . ?
B21 O11 B24 119.0(6) . 1_455 ?
B24 O11 Rb1 142.9(5) 1_455 . ?
B24 O11 K11 114.1(4) 1_455 . ?
K1 O12 K9 82.14(13) . . ?
K1 O12 K10 141.42(16) . . ?
K9 O12 K10 59.28(9) . . ?
B2 O12 K1 90.7(4) . . ?
B2 O12 K9 137.9(4) . . ?
B2 O12 K10 117.6(4) . . ?
B27 O12 K1 108.9(4) . . ?
B27 O12 K9 102.4(4) . . ?
B27 O12 K10 81.2(4) . . ?
B27 O12 B2 119.0(5) . . ?
K4 O13 K2 83.73(14) . . ?
B20 O13 K2 89.1(4) 1_655 . ?
B20 O13 K4 131.4(4) 1_655 . ?
B24 O13 K2 96.1(5) . . ?
B24 O13 K4 98.0(4) . . ?
B24 O13 B20 130.6(6) . 1_655 ?
K9 O14 K1 88.66(15) . . ?
B13 O14 K1 96.0(4) . . ?
B13 O14 K9 145.0(5) . . ?
B28 O14 K1 126.8(4) . . ?
B28 O14 K9 84.6(4) . . ?
B28 O14 B13 118.3(6) . . ?
Rb1 O15 K6 76.16(13) . . ?
Rb1 O15 K11 66.86(11) . . ?
K11 O15 K6 142.90(18) . . ?
B5 O15 Rb1 103.6(4) . . ?
B5 O15 K6 90.3(4) . . ?
B5 O15 K11 95.4(4) . . ?
B21 O15 Rb1 132.6(4) 1_655 . ?
B21 O15 K6 81.5(4) 1_655 . ?
B21 O15 K11 126.3(5) 1_655 . ?
B21 O15 B5 117.8(6) 1_655 . ?
K3 O16 K8 77.36(12) . 1_765 ?
B8 O16 K3 113.2(4) . . ?
B8 O16 K8 79.0(4) . 1_765 ?
B8 O16 B9 135.5(6) . . ?
B9 O16 K3 108.5(4) . . ?
B9 O16 K8 125.6(5) . 1_765 ?
K3 O17 K8 84.77(14) . 1_765 ?
B6 O17 K3 108.6(4) . . ?
B6 O17 K8 95.6(4) . 1_765 ?
B7 O17 K3 130.3(5) 1_655 . ?
B7 O17 K8 107.3(4) 1_655 1_765 ?
B7 O17 B6 117.4(6) 1_655 . ?
K9 O18 K7 142.99(18) . 2_656 ?
K10 O18 K7 76.90(13) . 2_656 ?
K10 O18 K9 66.44(12) . . ?
B12 O18 K7 97.1(4) 1_455 2_656 ?
B12 O18 K9 103.9(4) 1_455 . ?
B12 O18 K10 133.0(4) 1_455 . ?
B12 O18 B27 123.4(6) 1_455 . ?
B27 O18 K7 93.4(4) . 2_656 ?
B27 O18 K9 99.8(4) . . ?
B27 O18 K10 103.6(4) . . ?
K9 O19 K9 86.03(15) 2_566 . ?
B10 O19 K9 130.6(5) . 2_566 ?
B10 O19 K9 95.6(4) . . ?
B10 O19 B28 124.7(6) . 2_566 ?
B28 O19 K9 76.8(4) 2_566 2_566 ?
B28 O19 K9 138.0(4) 2_566 . ?
Rb1 O20 K4 124.79(17) . 2_455 ?
K11 O20 Rb1 61.66(10) . . ?
K11 O20 K4 70.50(13) . 2_455 ?
B3 O20 Rb1 123.4(4) . . ?
B3 O20 K4 70.4(4) . 2_455 ?
B3 O20 K11 130.2(4) . . ?
B21 O20 Rb1 94.7(4) . . ?
B21 O20 K4 113.9(5) . 2_455 ?
B21 O20 K11 92.4(4) . . ?
B21 O20 B3 131.6(6) . . ?
K6 O21 Rb1 76.04(14) . . ?
K6 O21 K7 77.38(14) . 1_455 ?
K7 O21 Rb1 153.38(17) 1_455 . ?
B17 O21 Rb1 71.1(4) 1_455 . ?
B17 O21 K6 115.0(4) 1_455 . ?
B17 O21 K7 122.8(4) 1_455 1_455 ?
B25 O21 Rb1 104.0(5) . . ?
B25 O21 K6 120.1(5) . . ?
B25 O21 K7 87.9(5) . 1_455 ?
B25 O21 B17 121.5(6) . 1_455 ?
K8 O22 K2 88.33(15) . 1_445 ?
B9 O22 K2 119.0(4) 1_445 1_445 ?
B9 O22 K8 121.4(4) 1_445 . ?
B16 O22 K2 84.2(4) . 1_445 ?
B16 O22 K8 100.6(4) . . ?
B16 O22 B9 130.5(6) . 1_445 ?
K6 O23 K2 85.99(15) . . ?
K6 O23 K7 78.20(14) . 1_455 ?
K7 O23 K2 158.17(18) 1_455 . ?
B15 O23 K2 84.4(4) 1_455 . ?
B15 O23 K6 103.6(4) 1_455 . ?
B15 O23 K7 84.8(4) 1_455 1_455 ?
B18 O23 K2 94.0(4) . . ?
B18 O23 K6 125.7(5) . . ?
B18 O23 K7 107.4(4) . 1_455 ?
B18 O23 B15 130.5(6) . 1_455 ?
Rb1 O24 K7 136.65(17) . 1_355 ?
B8 O24 Rb1 108.1(5) 1_445 . ?
B8 O24 K7 111.1(5) 1_445 1_355 ?
B8 O24 B17 119.5(6) 1_445 1_455 ?
B17 O24 Rb1 87.6(4) 1_455 . ?
B17 O24 K7 89.0(4) 1_455 1_355 ?
K6 O25 K2 85.62(15) . . ?
B5 O25 K2 130.8(4) . . ?
B5 O25 K6 113.7(4) . . ?
B23 O25 K2 88.3(5) 1_455 . ?
B23 O25 K6 108.7(5) 1_455 . ?
B23 O25 B5 122.6(6) 1_455 . ?
K1 O26 K1 69.90(12) . 2_656 ?
K1 O26 K5 85.27(13) . . ?
K5 O26 K1 141.69(16) . 2_656 ?
B14 O26 K1 96.1(4) . . ?
B14 O26 K1 115.9(5) . 2_656 ?
B14 O26 K5 94.8(4) . . ?
B14 O26 B27 123.1(6) . 2_656 ?
B27 O26 K1 87.5(4) 2_656 2_656 ?
B27 O26 K1 140.6(4) 2_656 . ?
B27 O26 K5 94.7(4) 2_656 . ?
K6 O27 K5 130.94(19) 1_655 . ?
B6 O27 K5 88.0(4) . . ?
B6 O27 K6 117.6(5) . 1_655 ?
B6 O27 B15 123.0(6) . . ?
B15 O27 K5 100.9(5) . . ?
B15 O27 K6 98.2(4) . 1_655 ?
K1 O28 K1 72.89(13) . 2_656 ?
B2 O28 K1 96.1(4) . . ?
B2 O28 K1 134.0(4) . 2_656 ?
B12 O28 K1 128.4(5) . . ?
B12 O28 K1 89.7(4) . 2_656 ?
B12 O28 B2 127.6(6) . . ?
K11 O29 Rb1 150.56(18) 2_455 . ?
K11 O29 Rb1 61.17(10) . . ?
K11 O29 K11 89.41(16) 2_455 . ?
B5 O29 Rb1 82.9(4) . . ?
B5 O29 K11 104.3(4) . . ?
B5 O29 K11 105.1(4) . 2_455 ?
B20 O29 Rb1 111.6(4) . . ?
B20 O29 K11 136.5(4) . . ?
B20 O29 K11 90.0(4) . 2_455 ?
B20 O29 B5 117.7(6) . . ?
B2 O30 K7 133.7(4) . 2_756 ?
B26 O30 K7 91.1(4) . 2_756 ?
B26 O30 B2 118.2(6) . . ?
Rb1 O31 K11 67.53(11) . . ?
B4 O31 Rb1 113.2(4) 2_455 . ?
B4 O31 K11 131.4(4) 2_455 . ?
B22 O31 Rb1 115.3(5) 1_545 . ?
B22 O31 K11 92.1(4) 1_545 . ?
B22 O31 B4 124.3(6) 1_545 2_455 ?
K7 O32 K5 110.77(18) 1_455 . ?
B17 O32 K5 127.1(4) . . ?
B17 O32 K7 100.9(4) . 1_455 ?
B26 O32 K5 86.5(4) 2_656 . ?
B26 O32 K7 99.2(4) 2_656 1_455 ?
B26 O32 B17 129.4(6) 2_656 . ?
K8 O33 K3 75.59(13) 1_765 . ?
B8 O33 K3 86.4(4) . . ?
B8 O33 K8 94.6(5) . 1_765 ?
B25 O33 K3 149.9(5) 1_665 . ?
B25 O33 K8 112.7(5) 1_665 1_765 ?
B25 O33 B8 120.3(6) 1_665 . ?
B1 O34 K5 107.5(5) . 1_455 ?
B1 O34 B28 121.8(6) . . ?
B28 O34 K5 128.7(4) . 1_455 ?
K3 O35 K5 85.01(16) . . ?
B1 O35 K3 113.5(4) . . ?
B1 O35 K5 118.1(5) . . ?
B1 O35 B13 118.2(6) . . ?
B13 O35 K3 105.5(4) . . ?
B13 O35 K5 111.1(4) . . ?
K10 O36 K9 63.75(11) 1_655 1_655 ?
B2 O36 K9 123.0(4) . 1_655 ?
B2 O36 K10 113.2(4) . 1_655 ?
B11 O36 K9 100.9(4) . 1_655 ?
B11 O36 K10 97.6(5) . 1_655 ?
B11 O36 B2 133.9(6) . . ?
B20 O37 K2 111.5(4) 1_655 . ?
B23 O37 K2 132.5(5) . . ?
B23 O37 B20 114.9(6) . 1_655 ?
K10 O38 K3 84.13(15) 2_566 . ?
B11 O38 K3 101.9(5) 2_666 . ?
B11 O38 K10 95.5(4) 2_666 2_566 ?
B11 O38 B13 124.0(6) 2_666 . ?
B13 O38 K3 88.6(4) . . ?
B13 O38 K10 140.5(4) . 2_566 ?
B19 O39 K4 108.3(4) . . ?
B22 O39 K4 130.8(5) . . ?
B22 O39 B19 120.2(6) . . ?
K2 O40 Rb1 164.40(17) . 1_665 ?
K8 O40 Rb1 87.04(15) 1_765 1_665 ?
K8 O40 K2 77.40(13) 1_765 . ?
B4 O40 Rb1 88.2(4) 2_565 1_665 ?
B4 O40 K2 95.9(4) 2_565 . ?
B4 O40 K8 101.2(4) 2_565 1_765 ?
B16 O40 Rb1 104.7(4) 1_665 1_665 ?
B16 O40 K2 86.3(4) 1_665 . ?
B16 O40 K8 137.1(5) 1_665 1_765 ?
B16 O40 B4 120.0(6) 1_665 2_565 ?
K4 O41 K11 79.15(13) . 2_455 ?
B5 O41 K4 130.4(4) . . ?
B5 O41 K11 92.1(4) . 2_455 ?
B24 O41 K4 91.9(4) . . ?
B24 O41 K11 153.1(5) . 2_455 ?
B24 O41 B5 112.5(6) . . ?
K8 O42 K2 98.04(18) 1_765 1_655 ?
B6 O42 K2 109.0(4) . 1_655 ?
B6 O42 K8 101.5(4) . 1_765 ?
B23 O42 K2 100.1(5) . 1_655 ?
B23 O42 K8 113.4(5) . 1_765 ?
B23 O42 B6 130.3(6) . . ?
K1 O43 K5 89.69(15) 2_666 2_666 ?
B10 O43 K1 127.0(5) . 2_666 ?
B10 O43 K5 114.3(5) . 2_666 ?
B10 O43 B13 124.7(6) . 2_666 ?
B13 O43 K1 96.1(4) 2_666 2_666 ?
B13 O43 K5 96.5(4) 2_666 2_666 ?
B12 O44 K1 110.9(4) . 2_656 ?
B12 O44 B14 120.7(6) . 2_756 ?
B14 O44 K1 128.4(5) 2_756 2_656 ?
K4 O45 K11 106.67(16) 2_455 1_455 ?
B3 O45 K4 82.8(4) . 2_455 ?
B3 O45 K11 138.9(4) . 1_455 ?
B22 O45 K4 124.7(5) 1_445 2_455 ?
B22 O45 K11 89.1(4) 1_445 1_455 ?
B22 O45 B3 118.8(6) 1_445 . ?
K7 O46 K5 89.34(17) 1_455 1_455 ?
B1 O46 K5 85.6(5) . 1_455 ?
B1 O46 K7 129.3(4) . 1_455 ?
B1 O46 B15 132.1(6) . 1_455 ?
B15 O46 K5 98.9(4) 1_455 1_455 ?
B15 O46 K7 98.5(4) 1_455 1_455 ?
K7 O47 K10 78.34(15) 1_465 2_566 ?
B9 O47 K7 137.3(4) . 1_465 ?
B9 O47 K10 86.6(4) . 2_566 ?
B25 O47 K7 97.4(5) 1_565 1_465 ?
B25 O47 K10 108.2(5) 1_565 2_566 ?
B25 O47 B9 125.2(6) 1_565 . ?
K7 O48 K5 92.97(16) . . ?
B26 O48 K5 85.6(4) 2_656 . ?
B26 O48 K7 123.7(5) 2_656 . ?
B26 O48 B27 121.2(6) 2_656 2_656 ?
B27 O48 K5 113.9(4) 2_656 . ?
B27 O48 K7 110.6(4) 2_656 . ?

_olex2_submission_special_instructions 'No special instructions were received'
