# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_2
_database_code_depnum_ccdc_archive 'CCDC 1855794'
_audit_update_record             
;
2018-07-13 deposited with the CCDC.
2018-08-02 downloaded from the CCDC.
;
_audit_creation_date             2018-03-28
_audit_creation_method           
;
Olex2 1.2
(compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5335)
;
_shelx_SHELXL_version_number     2014/7
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C36 H26 Sb2'
_chemical_formula_sum            'C36 H26 Sb2'
_chemical_formula_weight         702.07
_chemical_absolute_configuration ?
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_H-M_alt        'P 1 21 1'
_space_group_name_Hall           'P 2yb'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   6.205(3)
_cell_length_b                   17.811(9)
_cell_length_c                   12.643(6)
_cell_angle_alpha                90
_cell_angle_beta                 96.512(6)
_cell_angle_gamma                90
_cell_volume                     1388.2(12)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    4404
_cell_measurement_temperature    110
_cell_measurement_theta_max      25.857
_cell_measurement_theta_min      2.287
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    1.969
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_correction_T_min  0.5998
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
'SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.1077 before and 0.0813 after correction. The Ratio of minimum to maximum transmission is 0.8047. The λ/2 correction factor is 0.00150.'
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.680
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             688
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0630
_diffrn_reflns_av_unetI/netI     0.0921
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            13087
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.782
_diffrn_reflns_theta_min         1.621
_diffrn_ambient_temperature      110
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.930
_reflns_Friedel_fraction_full    0.996
_reflns_Friedel_fraction_max     0.991
_reflns_number_gt                5239
_reflns_number_total             5877
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.34A (Bruker, 2013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    ?
_refine_diff_density_max         0.705
_refine_diff_density_min         -1.619
_refine_diff_density_rms         0.154
_refine_ls_abs_structure_details 
;
 Flack x determined using 2192 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   0.05(3)
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.997
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     343
_refine_ls_number_reflns         5877
_refine_ls_number_restraints     1
_refine_ls_R_factor_all          0.0511
_refine_ls_R_factor_gt           0.0433
_refine_ls_restrained_S_all      0.997
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0321P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0946
_refine_ls_wR_factor_ref         0.0986
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C10(H10), C9(H9), C16(H16), C22(H22), C4(H4), C23(H23), C3(H3), C24(H24),
 C14(H14), C21(H21), C18(H18), C2(H2), C15(H15), C11(H11), C20(H20), C17(H17),
 C26(H26), C32(H32), C27(H27), C30(H30), C28(H28), C29(H29), C34(H34), C33(H33),
  C36(H36), C35(H35)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb1 Sb -0.72429(10) -0.42136(3) -0.61609(5) 0.01439(16) Uani 1 1 d . . . . .
Sb2 Sb -1.09531(9) -0.53482(3) -0.85319(5) 0.01351(16) Uani 1 1 d . . . . .
C13 C -0.4826(16) -0.3327(5) -0.6085(9) 0.014(2) Uani 1 1 d . . . . .
C1 C -0.4938(17) -0.5118(5) -0.6077(9) 0.017(2) Uani 1 1 d . . . . .
C8 C -0.8552(16) -0.6215(6) -0.8243(8) 0.014(2) Uani 1 1 d . . . . .
C10 C -0.7443(18) -0.7521(6) -0.8631(9) 0.020(2) Uani 1 1 d . . . . .
H10 H -0.7767 -0.7965 -0.9002 0.024 Uiso 1 1 calc R . . . .
C6 C -0.5239(16) -0.5762(5) -0.6675(8) 0.014(2) Uani 1 1 d . . . . .
C9 C -0.8877(17) -0.6922(6) -0.8788(9) 0.017(2) Uani 1 1 d . . . . .
H9 H -1.0113 -0.6981 -0.9270 0.020 Uiso 1 1 calc R . . . .
C16 C -0.185(2) -0.2150(6) -0.6135(10) 0.020(2) Uani 1 1 d . . . . .
H16 H -0.0853 -0.1762 -0.6141 0.024 Uiso 1 1 calc R . . . .
C22 C -0.8696(18) -0.4011(6) -0.2398(9) 0.025(2) Uani 1 1 d . . . . .
H22 H -0.9032 -0.3965 -0.1703 0.030 Uiso 1 1 calc R . . . .
C7 C -0.6698(15) -0.6210(5) -0.7516(8) 0.012(2) Uani 1 1 d . . . . .
C4 C -0.1828(17) -0.6350(6) -0.5973(9) 0.020(2) Uani 1 1 d . . . . .
H4 H -0.0844 -0.6745 -0.5935 0.024 Uiso 1 1 calc R . . . .
C19 C -0.7691(14) -0.4163(6) -0.4497(7) 0.0155(19) Uani 1 1 d . . . . .
C23 C -0.9746(19) -0.3571(6) -0.3198(10) 0.029(3) Uani 1 1 d . . . . .
H23 H -1.0756 -0.3215 -0.3038 0.034 Uiso 1 1 calc R . . . .
C5 C -0.3731(16) -0.6371(6) -0.6603(8) 0.017(2) Uani 1 1 d . . . . .
C3 C -0.1434(16) -0.5678(5) -0.5372(8) 0.018(2) Uani 1 1 d . . . . .
H3 H -0.0145 -0.5634 -0.4923 0.021 Uiso 1 1 calc R . . . .
C24 C -0.9294(18) -0.3661(6) -0.4237(8) 0.020(2) Uani 1 1 d . . . . .
H24 H -1.0070 -0.3383 -0.4775 0.024 Uiso 1 1 calc R . . . .
C14 C -0.3337(18) -0.3315(6) -0.6838(9) 0.021(2) Uani 1 1 d . . . . .
H14 H -0.3352 -0.3700 -0.7336 0.025 Uiso 1 1 calc R . . . .
C21 C -0.7146(19) -0.4516(6) -0.2642(9) 0.026(2) Uani 1 1 d . . . . .
H21 H -0.6432 -0.4812 -0.2106 0.031 Uiso 1 1 calc R . . . .
C18 C -0.4824(16) -0.2729(5) -0.5390(8) 0.018(2) Uani 1 1 d . . . . .
H18 H -0.5830 -0.2719 -0.4898 0.022 Uiso 1 1 calc R . . . .
C2 C -0.2886(16) -0.5093(5) -0.5428(9) 0.020(2) Uani 1 1 d . . . . .
H2 H -0.2524 -0.4663 -0.5030 0.024 Uiso 1 1 calc R . . . .
C15 C -0.1844(17) -0.2740(6) -0.6854(9) 0.021(2) Uani 1 1 d . . . . .
H15 H -0.0836 -0.2748 -0.7345 0.026 Uiso 1 1 calc R . . . .
C12 C -0.5208(15) -0.6816(5) -0.7389(8) 0.015(2) Uani 1 1 d . . . . .
C11 C -0.5531(17) -0.7478(6) -0.7936(9) 0.021(2) Uani 1 1 d . . . . .
H11 H -0.4544 -0.7873 -0.7850 0.025 Uiso 1 1 calc R . . . .
C20 C -0.6628(18) -0.4592(6) -0.3694(8) 0.021(2) Uani 1 1 d . . . . .
H20 H -0.5567 -0.4931 -0.3846 0.025 Uiso 1 1 calc R . . . .
C17 C -0.3371(17) -0.2148(6) -0.5408(9) 0.023(2) Uani 1 1 d . . . . .
H17 H -0.3404 -0.1752 -0.4932 0.028 Uiso 1 1 calc R . . . .
C25 C -1.2081(16) -0.5750(5) -1.0113(8) 0.017(2) Uani 1 1 d . . . . .
C26 C -1.3964(16) -0.6186(5) -1.0281(9) 0.019(2) Uani 1 1 d . . . . .
H26 H -1.4704 -0.6305 -0.9704 0.023 Uiso 1 1 calc R . . . .
C31 C -0.8845(15) -0.4489(5) -0.9041(8) 0.014(2) Uani 1 1 d . . . . .
C32 C -0.6868(16) -0.4643(5) -0.9415(8) 0.016(2) Uani 1 1 d . . . . .
H32 H -0.6406 -0.5138 -0.9460 0.019 Uiso 1 1 calc R . . . .
C27 C -1.4751(18) -0.6443(6) -1.1276(8) 0.023(2) Uani 1 1 d . . . . .
H27 H -1.6007 -0.6732 -1.1361 0.028 Uiso 1 1 calc R . . . .
C30 C -1.1025(17) -0.5584(6) -1.1001(8) 0.021(2) Uani 1 1 d . . . . .
H30 H -0.9776 -0.5291 -1.0921 0.026 Uiso 1 1 calc R . . . .
C28 C -1.3680(19) -0.6273(6) -1.2156(9) 0.028(3) Uani 1 1 d . . . . .
H28 H -1.4212 -0.6442 -1.2832 0.034 Uiso 1 1 calc R . . . .
C29 C -1.1811(19) -0.5849(7) -1.2001(10) 0.029(3) Uani 1 1 d . . . . .
H29 H -1.1064 -0.5738 -1.2579 0.035 Uiso 1 1 calc R . . . .
C34 C -0.6246(16) -0.3322(6) -0.9617(8) 0.020(2) Uani 1 1 d . . . . .
H34 H -0.5366 -0.2931 -0.9800 0.025 Uiso 1 1 calc R . . . .
C33 C -0.5573(16) -0.4057(5) -0.9723(8) 0.018(2) Uani 1 1 d . . . . .
H33 H -0.4274 -0.4160 -0.9996 0.022 Uiso 1 1 calc R . . . .
C36 C -0.9506(17) -0.3744(5) -0.8972(8) 0.014(2) Uani 1 1 d . . . . .
H36 H -1.0843 -0.3638 -0.8740 0.017 Uiso 1 1 calc R . . . .
C35 C -0.8202(17) -0.3161(6) -0.9245(9) 0.021(2) Uani 1 1 d . . . . .
H35 H -0.8639 -0.2665 -0.9178 0.025 Uiso 1 1 calc R . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb1 C13 2.172(10) . ?
Sb1 C1 2.149(10) . ?
Sb1 C19 2.154(9) . ?
Sb2 C8 2.148(10) . ?
Sb2 C25 2.164(10) . ?
Sb2 C31 2.159(9) . ?
C13 C14 1.401(15) . ?
C13 C18 1.380(14) . ?
C1 C6 1.375(14) . ?
C1 C2 1.434(14) . ?
C8 C9 1.439(14) . ?
C8 C7 1.388(14) . ?
C10 C9 1.389(14) . ?
C10 C11 1.396(15) . ?
C6 C7 1.538(13) . ?
C6 C5 1.428(14) . ?
C16 C15 1.389(16) . ?
C16 C17 1.389(16) . ?
C22 C23 1.382(15) . ?
C22 C21 1.377(15) . ?
C7 C12 1.419(13) . ?
C4 C5 1.348(14) . ?
C4 C3 1.424(14) . ?
C19 C24 1.404(14) . ?
C19 C20 1.378(14) . ?
C23 C24 1.383(16) . ?
C5 C12 1.499(14) . ?
C3 C2 1.374(14) . ?
C14 C15 1.383(14) . ?
C21 C20 1.410(15) . ?
C18 C17 1.375(14) . ?
C12 C11 1.371(14) . ?
C25 C26 1.399(14) . ?
C25 C30 1.394(14) . ?
C26 C27 1.375(14) . ?
C31 C32 1.391(14) . ?
C31 C36 1.394(13) . ?
C32 C33 1.400(14) . ?
C27 C28 1.392(17) . ?
C30 C29 1.385(15) . ?
C28 C29 1.380(17) . ?
C34 C33 1.385(14) . ?
C34 C35 1.381(15) . ?
C36 C35 1.384(14) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Sb1 C13 95.2(3) . . ?
C1 Sb1 C19 98.2(4) . . ?
C19 Sb1 C13 95.2(4) . . ?
C8 Sb2 C25 93.7(4) . . ?
C8 Sb2 C31 97.4(4) . . ?
C31 Sb2 C25 95.9(4) . . ?
C14 C13 Sb1 119.1(7) . . ?
C18 C13 Sb1 122.7(8) . . ?
C18 C13 C14 117.9(9) . . ?
C6 C1 Sb1 123.4(7) . . ?
C6 C1 C2 113.4(9) . . ?
C2 C1 Sb1 123.2(7) . . ?
C9 C8 Sb2 119.4(7) . . ?
C7 C8 Sb2 128.0(7) . . ?
C7 C8 C9 112.5(9) . . ?
C9 C10 C11 122.2(10) . . ?
C1 C6 C7 147.6(9) . . ?
C1 C6 C5 123.4(9) . . ?
C5 C6 C7 88.9(8) . . ?
C10 C9 C8 123.4(9) . . ?
C17 C16 C15 119.2(10) . . ?
C21 C22 C23 119.3(11) . . ?
C8 C7 C6 147.0(9) . . ?
C8 C7 C12 123.4(9) . . ?
C12 C7 C6 89.5(7) . . ?
C5 C4 C3 115.2(10) . . ?
C24 C19 Sb1 115.4(7) . . ?
C20 C19 Sb1 126.3(7) . . ?
C20 C19 C24 118.2(9) . . ?
C22 C23 C24 120.0(10) . . ?
C6 C5 C12 90.7(8) . . ?
C4 C5 C6 122.7(10) . . ?
C4 C5 C12 146.6(10) . . ?
C2 C3 C4 122.5(9) . . ?
C23 C24 C19 121.5(10) . . ?
C15 C14 C13 121.1(10) . . ?
C22 C21 C20 120.9(10) . . ?
C17 C18 C13 121.5(10) . . ?
C3 C2 C1 122.7(9) . . ?
C14 C15 C16 119.9(11) . . ?
C7 C12 C5 90.8(7) . . ?
C11 C12 C7 122.8(9) . . ?
C11 C12 C5 146.4(10) . . ?
C12 C11 C10 115.5(10) . . ?
C19 C20 C21 120.1(10) . . ?
C18 C17 C16 120.3(10) . . ?
C26 C25 Sb2 120.1(8) . . ?
C30 C25 Sb2 122.8(7) . . ?
C30 C25 C26 117.1(10) . . ?
C27 C26 C25 121.9(11) . . ?
C32 C31 Sb2 123.3(7) . . ?
C32 C31 C36 119.1(8) . . ?
C36 C31 Sb2 117.6(7) . . ?
C31 C32 C33 120.2(9) . . ?
C26 C27 C28 120.4(10) . . ?
C29 C30 C25 120.9(10) . . ?
C29 C28 C27 118.3(10) . . ?
C28 C29 C30 121.3(11) . . ?
C35 C34 C33 121.0(10) . . ?
C34 C33 C32 119.3(10) . . ?
C35 C36 C31 120.9(9) . . ?
C34 C35 C36 119.3(10) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_3
_database_code_depnum_ccdc_archive 'CCDC 1855795'
_audit_update_record             
;
2018-07-13 deposited with the CCDC.
2018-08-02 downloaded from the CCDC.
;
_audit_creation_date             2018-03-28
_audit_creation_method           
;
Olex2 1.2
(compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5335)
;
_shelx_SHELXL_version_number     2014/7
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C42 H26 Cl4 O3 Sb2, 1.43(C H Cl3)'
_chemical_formula_sum            'C43.43 H27.43 Cl8.30 O3 Sb2'
_chemical_formula_weight         1134.83
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   16.192(2)
_cell_length_b                   17.205(3)
_cell_length_c                   16.316(2)
_cell_angle_alpha                90
_cell_angle_beta                 90.4177(19)
_cell_angle_gamma                90
_cell_volume                     4545.0(12)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9888
_cell_measurement_temperature    110
_cell_measurement_theta_max      26.28
_cell_measurement_theta_min      2.37
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    1.714
_exptl_absorpt_correction_T_max  0.7454
_exptl_absorpt_correction_T_min  0.6494
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2014/5 (Bruker,2014/5) was used for absorption correction.
wR2(int) was 0.0830 before and 0.0601 after correction.
The Ratio of minimum to maximum transmission is 0.8712.
The λ/2 correction factor is 0.00150.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.658
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             2220
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0878
_diffrn_reflns_av_unetI/netI     0.0503
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            49072
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.449
_diffrn_reflns_theta_min         1.720
_diffrn_ambient_temperature      110
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                7767
_reflns_number_total             9353
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.34A (Bruker, 2013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'XL (Sheldrick, 2008)'
_computing_structure_solution    ?
_refine_diff_density_max         2.211
_refine_diff_density_min         -2.214
_refine_diff_density_rms         0.185
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.064
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     527
_refine_ls_number_reflns         9353
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0670
_refine_ls_R_factor_gt           0.0543
_refine_ls_restrained_S_all      1.064
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0778P)²+33.3940P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1514
_refine_ls_wR_factor_ref         0.1637
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
2. Uiso/Uaniso restraints and constraints
Uanis(C43) = Uanis(C44)
3. Others
 Sof(Cl8)=Sof(Cl9)=Sof(Cl10)=Sof(C44)=Sof(H44)=FVAR(1)
4.a Ternary CH refined with riding coordinates:
 C43(H43), C44(H44)
4.b Aromatic/amide H refined with riding coordinates:
 C2(H2), C3(H3), C4(H4), C9(H9), C10(H10), C11(H11), C14(H14), C15(H15),
 C16(H16), C17(H17), C18(H18), C20(H20), C21(H21), C22(H22), C23(H23), C24(H24),
  C26(H26), C27(H27), C28(H28), C29(H29), C30(H30), C32(H32), C33(H33),
 C34(H34), C35(H35), C36(H36)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb1 Sb 0.21621(2) 0.05176(2) 0.00560(2) 0.02038(12) Uani 1 1 d . . . . .
Sb2 Sb 0.27908(2) 0.01246(2) 0.21542(2) 0.01956(12) Uani 1 1 d . . . . .
Cl1 Cl 0.42463(9) 0.25003(9) 0.10659(9) 0.0261(3) Uani 1 1 d . . . . .
Cl2 Cl 0.33777(11) 0.40406(10) 0.16245(11) 0.0361(4) Uani 1 1 d . . . . .
Cl3 Cl 0.16869(11) 0.39522(11) 0.25570(12) 0.0415(4) Uani 1 1 d . . . . .
Cl4 Cl 0.09391(9) 0.23226(11) 0.29975(10) 0.0338(4) Uani 1 1 d . . . . .
O1 O 0.2106(2) 0.0010(3) 0.1074(2) 0.0237(9) Uani 1 1 d . . . . .
O2 O 0.3312(2) 0.1073(2) 0.1527(2) 0.0213(8) Uani 1 1 d . . . . .
O3 O 0.1952(2) 0.1010(3) 0.2414(3) 0.0250(9) Uani 1 1 d . . . . .
C1 C 0.3246(3) 0.0101(4) -0.0471(4) 0.0219(12) Uani 1 1 d . . . . .
C2 C 0.3465(4) 0.0153(4) -0.1311(4) 0.0262(13) Uani 1 1 d . . . . .
H2 H 0.3137 0.0441 -0.1669 0.031 Uiso 1 1 calc R . . . .
C3 C 0.4159(4) -0.0219(4) -0.1603(4) 0.0255(13) Uani 1 1 d . . . . .
H3 H 0.4303 -0.0148 -0.2148 0.031 Uiso 1 1 calc R . . . .
C4 C 0.4660(4) -0.0704(4) -0.1104(4) 0.0243(12) Uani 1 1 d . . . . .
H4 H 0.5121 -0.0959 -0.1309 0.029 Uiso 1 1 calc R . . . .
C5 C 0.4428(3) -0.0774(4) -0.0306(4) 0.0213(12) Uani 1 1 d . . . . .
C6 C 0.3744(3) -0.0355(4) 0.0010(4) 0.0214(12) Uani 1 1 d . . . . .
C7 C 0.3909(3) -0.0676(4) 0.0854(4) 0.0225(12) Uani 1 1 d . . . . .
C8 C 0.3696(3) -0.0647(3) 0.1663(4) 0.0204(12) Uani 1 1 d . . . . .
C9 C 0.4175(4) -0.1151(4) 0.2168(4) 0.0259(13) Uani 1 1 d . . . . .
H9 H 0.4065 -0.1170 0.2727 0.031 Uiso 1 1 calc R . . . .
C10 C 0.4802(4) -0.1617(4) 0.1858(4) 0.0272(13) Uani 1 1 d . . . . .
H10 H 0.5088 -0.1942 0.2216 0.033 Uiso 1 1 calc R . . . .
C11 C 0.5021(4) -0.1617(4) 0.1026(4) 0.0251(13) Uani 1 1 d . . . . .
H11 H 0.5438 -0.1932 0.0822 0.030 Uiso 1 1 calc R . . . .
C12 C 0.4576(3) -0.1122(4) 0.0536(4) 0.0216(12) Uani 1 1 d . . . . .
C13 C 0.1163(4) 0.0074(4) -0.0625(4) 0.0238(13) Uani 1 1 d . . . . .
C14 C 0.0495(4) 0.0555(4) -0.0817(4) 0.0265(13) Uani 1 1 d . . . . .
H14 H 0.0477 0.1063 -0.0624 0.032 Uiso 1 1 calc R . . . .
C15 C -0.0141(4) 0.0263(4) -0.1301(4) 0.0323(15) Uani 1 1 d . . . . .
H15 H -0.0587 0.0578 -0.1439 0.039 Uiso 1 1 calc R . . . .
C16 C -0.0113(4) -0.0493(5) -0.1575(4) 0.0381(17) Uani 1 1 d . . . . .
H16 H -0.0547 -0.0689 -0.1890 0.046 Uiso 1 1 calc R . . . .
C17 C 0.0551(5) -0.0961(5) -0.1387(6) 0.049(2) Uani 1 1 d . . . . .
H17 H 0.0571 -0.1469 -0.1583 0.059 Uiso 1 1 calc R . . . .
C18 C 0.1189(4) -0.0676(5) -0.0909(5) 0.0406(18) Uani 1 1 d . . . . .
H18 H 0.1637 -0.0992 -0.0779 0.049 Uiso 1 1 calc R . . . .
C19 C 0.2065(3) 0.1726(4) 0.0033(4) 0.0237(13) Uani 1 1 d . . . . .
C20 C 0.2618(4) 0.2144(4) -0.0446(4) 0.0289(14) Uani 1 1 d . . . . .
H20 H 0.3031 0.1880 -0.0724 0.035 Uiso 1 1 calc R . . . .
C21 C 0.2565(4) 0.2937(4) -0.0516(4) 0.0334(15) Uani 1 1 d . . . . .
H21 H 0.2940 0.3206 -0.0841 0.040 Uiso 1 1 calc R . . . .
C22 C 0.1956(5) 0.3334(4) -0.0105(4) 0.0353(15) Uani 1 1 d . . . . .
H22 H 0.1922 0.3872 -0.0146 0.042 Uiso 1 1 calc R . . . .
C23 C 0.1393(4) 0.2927(4) 0.0371(4) 0.0345(15) Uani 1 1 d . . . . .
H23 H 0.0979 0.3197 0.0642 0.041 Uiso 1 1 calc R . . . .
C24 C 0.1440(4) 0.2122(4) 0.0447(4) 0.0269(13) Uani 1 1 d . . . . .
H24 H 0.1063 0.1853 0.0767 0.032 Uiso 1 1 calc R . . . .
C25 C 0.1915(4) -0.0665(4) 0.2666(4) 0.0265(13) Uani 1 1 d . . . . .
C26 C 0.1333(4) -0.0425(5) 0.3240(4) 0.0330(15) Uani 1 1 d . . . . .
H26 H 0.1348 0.0081 0.3439 0.040 Uiso 1 1 calc R . . . .
C27 C 0.0736(4) -0.0930(5) 0.3513(5) 0.0420(19) Uani 1 1 d . . . . .
H27 H 0.0350 -0.0764 0.3894 0.050 Uiso 1 1 calc R . . . .
C28 C 0.0710(5) -0.1686(6) 0.3221(5) 0.051(2) Uani 1 1 d . . . . .
H28 H 0.0305 -0.2026 0.3403 0.062 Uiso 1 1 calc R . . . .
C29 C 0.1286(5) -0.1935(5) 0.2658(5) 0.0444(19) Uani 1 1 d . . . . .
H29 H 0.1273 -0.2444 0.2467 0.053 Uiso 1 1 calc R . . . .
C30 C 0.1880(4) -0.1426(4) 0.2380(4) 0.0326(15) Uani 1 1 d . . . . .
H30 H 0.2262 -0.1595 0.1996 0.039 Uiso 1 1 calc R . . . .
C31 C 0.3506(3) 0.0427(4) 0.3223(4) 0.0211(12) Uani 1 1 d . . . . .
C32 C 0.3332(4) 0.0076(4) 0.3974(4) 0.0270(13) Uani 1 1 d . . . . .
H32 H 0.2900 -0.0277 0.4009 0.032 Uiso 1 1 calc R . . . .
C33 C 0.3800(4) 0.0250(4) 0.4670(4) 0.0309(14) Uani 1 1 d . . . . .
H33 H 0.3680 0.0014 0.5167 0.037 Uiso 1 1 calc R . . . .
C34 C 0.4448(4) 0.0779(4) 0.4618(4) 0.0311(15) Uani 1 1 d . . . . .
H34 H 0.4753 0.0904 0.5085 0.037 Uiso 1 1 calc R . . . .
C35 C 0.4640(4) 0.1117(4) 0.3880(4) 0.0295(14) Uani 1 1 d . . . . .
H35 H 0.5081 0.1461 0.3845 0.035 Uiso 1 1 calc R . . . .
C36 C 0.4172(4) 0.0943(4) 0.3183(4) 0.0250(13) Uani 1 1 d . . . . .
H36 H 0.4305 0.1172 0.2685 0.030 Uiso 1 1 calc R . . . .
C37 C 0.2257(3) 0.1711(4) 0.2251(3) 0.0230(12) Uani 1 1 d . . . . .
C38 C 0.2994(4) 0.1748(4) 0.1788(3) 0.0215(12) Uani 1 1 d . . . . .
C39 C 0.3334(4) 0.2464(4) 0.1615(4) 0.0228(12) Uani 1 1 d . . . . .
C40 C 0.2947(4) 0.3151(4) 0.1869(4) 0.0252(13) Uani 1 1 d . . . . .
C41 C 0.2211(4) 0.3113(4) 0.2289(4) 0.0286(14) Uani 1 1 d . . . . .
C42 C 0.1865(4) 0.2392(4) 0.2485(4) 0.0244(13) Uani 1 1 d . . . . .
Cl5 Cl 0.3003(3) -0.1987(3) -0.1456(4) 0.1485(19) Uani 1 1 d . . . . .
Cl6 Cl 0.2301(5) -0.2263(4) 0.0114(4) 0.193(3) Uani 1 1 d . . . . .
Cl7 Cl 0.3727(3) -0.3083(3) -0.0393(5) 0.171(3) Uani 1 1 d . . . . .
C43 C 0.2876(13) -0.2655(9) -0.0607(14) 0.153(8) Uani 1 1 d . . . . .
H43 H 0.2527 -0.3069 -0.0835 0.183 Uiso 1 1 calc R . . . .
Cl8 Cl 0.0473(7) -0.3789(7) 0.1256(9) 0.142(5) Uani 0.431(8) 1 d . . P A 2
Cl9 Cl 0.2117(6) -0.3961(5) 0.1845(7) 0.112(3) Uani 0.431(8) 1 d . . P A 2
Cl10 Cl 0.1559(10) -0.4752(11) 0.0503(8) 0.203(9) Uani 0.431(8) 1 d . . P A 2
C44 C 0.115(3) -0.440(2) 0.113(3) 0.153(8) Uani 0.431(8) 1 d . . P A 2
H44 H 0.0953 -0.4836 0.1455 0.183 Uiso 0.431(8) 1 calc R . P A 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb1 O1 1.880(4) . ?
Sb1 C1 2.087(6) . ?
Sb1 C13 2.100(6) . ?
Sb1 C19 2.086(7) . ?
Sb2 O1 2.084(4) . ?
Sb2 O2 2.107(4) . ?
Sb2 O3 2.088(4) . ?
Sb2 C8 2.139(6) . ?
Sb2 C25 2.137(6) . ?
Sb2 C31 2.150(6) . ?
Cl1 C39 1.735(6) . ?
Cl2 C40 1.729(7) . ?
Cl3 C41 1.732(6) . ?
Cl4 C42 1.727(6) . ?
O2 C38 1.341(7) . ?
O3 C37 1.330(8) . ?
C1 C2 1.422(8) . ?
C1 C6 1.367(9) . ?
C2 C3 1.380(9) . ?
C3 C4 1.417(9) . ?
C4 C5 1.364(8) . ?
C5 C6 1.420(8) . ?
C5 C12 1.515(8) . ?
C6 C7 1.506(8) . ?
C7 C8 1.368(8) . ?
C7 C12 1.425(8) . ?
C8 C9 1.422(8) . ?
C9 C10 1.392(9) . ?
C10 C11 1.406(9) . ?
C11 C12 1.370(9) . ?
C13 C14 1.394(9) . ?
C13 C18 1.371(10) . ?
C14 C15 1.388(9) . ?
C15 C16 1.375(11) . ?
C16 C17 1.377(11) . ?
C17 C18 1.380(10) . ?
C19 C20 1.392(9) . ?
C19 C24 1.397(9) . ?
C20 C21 1.373(10) . ?
C21 C22 1.378(10) . ?
C22 C23 1.391(10) . ?
C23 C24 1.393(10) . ?
C25 C26 1.396(9) . ?
C25 C30 1.392(10) . ?
C26 C27 1.375(10) . ?
C27 C28 1.386(12) . ?
C28 C29 1.381(11) . ?
C29 C30 1.379(10) . ?
C31 C32 1.396(9) . ?
C31 C36 1.398(9) . ?
C32 C33 1.393(9) . ?
C33 C34 1.391(10) . ?
C34 C35 1.376(10) . ?
C35 C36 1.393(9) . ?
C37 C38 1.419(8) . ?
C37 C42 1.387(9) . ?
C38 C39 1.379(9) . ?
C39 C40 1.402(9) . ?
C40 C41 1.380(9) . ?
C41 C42 1.399(10) . ?
Cl5 C43 1.812(19) . ?
Cl6 C43 1.651(19) . ?
Cl7 C43 1.60(2) . ?
Cl8 C44 1.53(4) . ?
Cl9 C44 2.08(6) . ?
Cl10 C44 1.37(5) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Sb1 C1 104.5(2) . . ?
O1 Sb1 C13 104.9(2) . . ?
O1 Sb1 C19 118.4(2) . . ?
C1 Sb1 C13 107.7(2) . . ?
C19 Sb1 C1 113.5(2) . . ?
C19 Sb1 C13 107.2(2) . . ?
O1 Sb2 O2 82.82(16) . . ?
O1 Sb2 O3 84.15(17) . . ?
O1 Sb2 C8 89.21(19) . . ?
O1 Sb2 C25 85.4(2) . . ?
O1 Sb2 C31 171.3(2) . . ?
O2 Sb2 C8 91.19(19) . . ?
O2 Sb2 C25 162.1(2) . . ?
O2 Sb2 C31 89.48(19) . . ?
O3 Sb2 O2 78.28(16) . . ?
O3 Sb2 C8 168.2(2) . . ?
O3 Sb2 C25 87.1(2) . . ?
O3 Sb2 C31 90.3(2) . . ?
C8 Sb2 C31 95.0(2) . . ?
C25 Sb2 C8 102.2(2) . . ?
C25 Sb2 C31 101.1(2) . . ?
Sb1 O1 Sb2 132.4(2) . . ?
C38 O2 Sb2 111.1(3) . . ?
C37 O3 Sb2 112.2(3) . . ?
C2 C1 Sb1 126.2(4) . . ?
C6 C1 Sb1 117.1(4) . . ?
C6 C1 C2 116.1(5) . . ?
C3 C2 C1 120.8(6) . . ?
C2 C3 C4 122.7(6) . . ?
C5 C4 C3 116.1(5) . . ?
C4 C5 C6 121.5(6) . . ?
C4 C5 C12 149.0(6) . . ?
C6 C5 C12 89.5(5) . . ?
C1 C6 C5 122.8(5) . . ?
C1 C6 C7 146.5(6) . . ?
C5 C6 C7 90.7(5) . . ?
C8 C7 C6 145.6(6) . . ?
C8 C7 C12 124.6(6) . . ?
C12 C7 C6 89.7(5) . . ?
C7 C8 Sb2 124.2(4) . . ?
C7 C8 C9 113.4(5) . . ?
C9 C8 Sb2 122.3(4) . . ?
C10 C9 C8 122.4(6) . . ?
C9 C10 C11 122.7(6) . . ?
C12 C11 C10 115.4(5) . . ?
C7 C12 C5 90.1(5) . . ?
C11 C12 C5 148.6(6) . . ?
C11 C12 C7 121.2(5) . . ?
C14 C13 Sb1 119.7(5) . . ?
C18 C13 Sb1 119.7(5) . . ?
C18 C13 C14 120.5(6) . . ?
C15 C14 C13 119.0(6) . . ?
C16 C15 C14 120.0(6) . . ?
C15 C16 C17 120.6(7) . . ?
C16 C17 C18 119.8(7) . . ?
C13 C18 C17 120.0(7) . . ?
C20 C19 Sb1 118.4(5) . . ?
C20 C19 C24 119.4(6) . . ?
C24 C19 Sb1 122.1(5) . . ?
C21 C20 C19 121.4(6) . . ?
C20 C21 C22 119.7(7) . . ?
C21 C22 C23 119.8(7) . . ?
C22 C23 C24 120.9(7) . . ?
C23 C24 C19 118.8(6) . . ?
C26 C25 Sb2 121.9(5) . . ?
C30 C25 Sb2 119.6(5) . . ?
C30 C25 C26 118.4(6) . . ?
C27 C26 C25 120.7(7) . . ?
C26 C27 C28 120.1(7) . . ?
C29 C28 C27 120.0(7) . . ?
C30 C29 C28 119.8(8) . . ?
C29 C30 C25 121.0(7) . . ?
C32 C31 Sb2 119.7(4) . . ?
C32 C31 C36 118.4(6) . . ?
C36 C31 Sb2 121.8(4) . . ?
C33 C32 C31 120.6(6) . . ?
C34 C33 C32 119.9(6) . . ?
C35 C34 C33 120.2(6) . . ?
C34 C35 C36 119.9(6) . . ?
C35 C36 C31 120.9(6) . . ?
O3 C37 C38 117.6(5) . . ?
O3 C37 C42 122.7(5) . . ?
C42 C37 C38 119.7(6) . . ?
O2 C38 C37 117.2(6) . . ?
O2 C38 C39 123.6(5) . . ?
C39 C38 C37 119.2(6) . . ?
C38 C39 Cl1 118.7(5) . . ?
C38 C39 C40 120.9(5) . . ?
C40 C39 Cl1 120.4(5) . . ?
C39 C40 Cl2 119.8(5) . . ?
C41 C40 Cl2 120.5(5) . . ?
C41 C40 C39 119.7(6) . . ?
C40 C41 Cl3 120.8(5) . . ?
C40 C41 C42 120.3(6) . . ?
C42 C41 Cl3 118.9(5) . . ?
C37 C42 Cl4 118.3(5) . . ?
C37 C42 C41 120.1(6) . . ?
C41 C42 Cl4 121.5(5) . . ?
Cl6 C43 Cl5 110.7(9) . . ?
Cl7 C43 Cl5 110.9(11) . . ?
Cl7 C43 Cl6 121.5(16) . . ?
Cl8 C44 Cl9 102(2) . . ?
Cl10 C44 Cl8 139(4) . . ?
Cl10 C44 Cl9 102(3) . . ?

_olex2_submission_special_instructions 'No special instructions were received'
