# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2019

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Dy_24DNB
_database_code_depnum_ccdc_archive 'CCDC 1584540'
loop_
_audit_author_name
_audit_author_address
'Geeta Hundal'
;Guru Nanak Dev University, Amritsar, Punjab
India
;
_audit_update_record             
;
2018-03-14 deposited with the CCDC.	2019-02-15 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2017/1
_shelx_SHELXL_version_number     2017/1
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C22 H26 Dy2 N4 O24'
_chemical_formula_sum            'C22 H26 Dy2 N4 O24'
_chemical_formula_weight         1055.47

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      orthorhombic
_space_group_IT_number           61
_space_group_name_H-M_alt        'P b c a'
_space_group_name_Hall           '-P 2ac 2ab'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x-1/2, y, -z-1/2'
'x, -y-1/2, z-1/2'
'-x-1/2, y-1/2, z'

_cell_length_a                   13.8285(4)
_cell_length_b                   8.9016(3)
_cell_length_c                   27.5841(9)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     3395.49(19)
_cell_formula_units_Z            4
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    5607
_cell_measurement_theta_min      2.82
_cell_measurement_theta_max      31.494

_exptl_crystal_description       rectangular
_exptl_crystal_colour            colourless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_density_diffrn    2.065
_exptl_crystal_F_000             2040
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.100
_exptl_absorpt_coefficient_mu    4.468
_shelx_estimated_absorpt_T_min   0.469
_shelx_estimated_absorpt_T_max   0.664
_exptl_absorpt_correction_type   'multi scan'
_exptl_absorpt_correction_T_min  0.462
_exptl_absorpt_correction_T_max  0.669
_exptl_absorpt_process_details   
'SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction '
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            60008
_diffrn_reflns_av_unetI/netI     0.0250
_diffrn_reflns_av_R_equivalents  0.0448
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_l_min       -39
_diffrn_reflns_limit_l_max       40
_diffrn_reflns_theta_min         2.820
_diffrn_reflns_theta_max         31.494
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measured_fraction_theta_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_point_group_measured_fraction_full 0.999
_reflns_number_total             5607
_reflns_number_gt                4218
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXT 2014/4 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.All non-hydrogen atoms were
 refined anisotropically. All hydrogen atoms were fixed geometrically with
 their Uiso values 1.2 times that of the phenylene carbons. The hydrogen
 atoms of the water molecules were located from the difference Fourier 
synthesis and were refined isotropically with a distance of 0.82 Å with
 Uiso values 1.2 times that of their carrier oxygen atoms. The hydrogen
 atoms of the methyl groups of the coordinated acetate group were fixed 
geometrically with their Uiso values 1.5 times that of their carrier 
carbons. 
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0399P)²+1.1425P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         5607
_refine_ls_number_parameters     247
_refine_ls_number_restraints     4
_refine_ls_R_factor_all          0.0472
_refine_ls_R_factor_gt           0.0286
_refine_ls_wR_factor_ref         0.0791
_refine_ls_wR_factor_gt          0.0708
_refine_ls_goodness_of_fit_ref   1.064
_refine_ls_restrained_S_all      1.064
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.61003(19) 0.6643(3) 0.35841(11) 0.0308(6) Uani 1 1 d . . . . .
C2 C 0.6367(2) 0.7448(3) 0.31221(11) 0.0320(6) Uani 1 1 d . . . . .
C3 C 0.5791(2) 0.7493(3) 0.27077(11) 0.0343(6) Uani 1 1 d . . . . .
C4 C 0.6091(2) 0.8117(4) 0.22818(12) 0.0390(7) Uani 1 1 d . . . . .
H4 H 0.569609 0.811678 0.200889 0.047 Uiso 1 1 calc R U . . .
C5 C 0.6997(2) 0.8747(3) 0.22706(12) 0.0391(7) Uani 1 1 d . . . . .
C6 C 0.7588(2) 0.8755(4) 0.26632(12) 0.0423(8) Uani 1 1 d . . . . .
H6 H 0.819616 0.919884 0.264545 0.051 Uiso 1 1 calc R U . . .
C7 C 0.7279(2) 0.8098(4) 0.30898(12) 0.0422(7) Uani 1 1 d . . . . .
H7 H 0.768521 0.809020 0.335843 0.051 Uiso 1 1 calc R U . . .
C8 C 0.5340(2) 0.2149(3) 0.40905(11) 0.0316(6) Uani 1 1 d . . . . .
C9 C 0.4928(3) 0.0711(4) 0.39148(19) 0.0723(13) Uani 1 1 d . . . . .
H9A H 0.543295 0.010523 0.377798 0.108 Uiso 1 1 calc R U . . .
H9B H 0.463513 0.018471 0.418093 0.108 Uiso 1 1 calc R U . . .
H9C H 0.444755 0.091148 0.367186 0.108 Uiso 1 1 calc R U . . .
C10 C 0.3783(2) 0.6692(3) 0.46386(11) 0.0287(6) Uani 1 1 d . . . . .
C11 C 0.3513(3) 0.7370(4) 0.41672(13) 0.0521(9) Uani 1 1 d . . . . .
H11A H 0.403389 0.724424 0.394100 0.078 Uiso 1 1 calc R U . . .
H11B H 0.294348 0.688406 0.404426 0.078 Uiso 1 1 calc R U . . .
H11C H 0.338512 0.842166 0.421089 0.078 Uiso 1 1 calc R U . . .
N1 N 0.4792(2) 0.6920(3) 0.27181(12) 0.0498(7) Uani 1 1 d . . . . .
N2 N 0.7319(3) 0.9449(4) 0.18131(12) 0.0507(7) Uani 1 1 d . . . . .
O1 O 0.62901(16) 0.7268(2) 0.39819(8) 0.0361(5) Uani 1 1 d . . . . .
O2 O 0.57607(18) 0.5344(3) 0.35631(9) 0.0420(5) Uani 1 1 d . . . . .
O3 O 0.4313(2) 0.7134(4) 0.30755(11) 0.0723(9) Uani 1 1 d . . . . .
O4 O 0.4493(2) 0.6291(4) 0.23561(12) 0.0857(11) Uani 1 1 d . . . . .
O5 O 0.6851(2) 0.9190(4) 0.14473(10) 0.0714(8) Uani 1 1 d . . . . .
O6 O 0.8033(3) 1.0233(4) 0.18247(13) 0.0827(11) Uani 1 1 d . . . . .
O7 O 0.62334(14) 0.2405(2) 0.40502(9) 0.0362(5) Uani 1 1 d . . . . .
O8 O 0.48005(14) 0.3110(2) 0.42834(8) 0.0377(5) Uani 1 1 d . . . . .
O9 O 0.45852(13) 0.6032(2) 0.46943(8) 0.0350(5) Uani 1 1 d . . . . .
O10 O 0.32011(15) 0.6733(3) 0.49870(8) 0.0414(5) Uani 1 1 d . . . . .
Dy1 Dy 0.60198(2) 0.49119(2) 0.44389(2) 0.02372(5) Uani 1 1 d . . . . .
O1W O 0.76440(16) 0.4909(2) 0.41926(10) 0.0366(5) Uani 1 1 d D . . . .
H11W H 0.796(2) 0.417(3) 0.4137(12) 0.044 Uiso 1 1 d D U . . .
H12W H 0.796(2) 0.568(3) 0.4160(13) 0.044 Uiso 1 1 d D U . . .
O2W O 0.65708(16) 0.6628(3) 0.50184(9) 0.0431(6) Uani 1 1 d D . . . .
H21W H 0.7082(18) 0.714(3) 0.5016(14) 0.052 Uiso 1 1 d D U . . .
H22W H 0.624(2) 0.686(4) 0.5242(10) 0.052 Uiso 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 O2 1.249(4) . ?
C1 O1 1.258(4) . ?
C1 C2 1.508(4) . ?
C2 C7 1.391(4) . ?
C2 C3 1.394(4) . ?
C3 C4 1.364(4) . ?
C3 N1 1.473(4) . ?
C4 C5 1.373(4) . ?
C4 H4 0.9300 . ?
C5 C6 1.357(5) . ?
C5 N2 1.477(4) . ?
C6 C7 1.382(4) . ?
C6 H6 0.9300 . ?
C7 H7 0.9300 . ?
C8 O8 1.254(3) . ?
C8 O7 1.261(3) . ?
C8 C9 1.483(4) . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
C10 O10 1.254(3) . ?
C10 O9 1.265(3) . ?
C10 C11 1.482(5) . ?
C10 Dy1 2.930(3) 5_666 ?
C11 H11A 0.9600 . ?
C11 H11B 0.9600 . ?
C11 H11C 0.9600 . ?
N1 O3 1.203(4) . ?
N1 O4 1.217(4) . ?
N2 O6 1.209(4) . ?
N2 O5 1.221(4) . ?
O1 Dy1 2.475(2) . ?
O2 Dy1 2.472(2) . ?
O7 Dy1 2.493(2) . ?
O8 Dy1 2.3661(19) . ?
O9 Dy1 2.3293(18) . ?
O9 Dy1 2.669(2) 5_666 ?
O10 Dy1 2.411(2) 5_666 ?
Dy1 O2W 2.339(2) . ?
Dy1 O1W 2.347(2) . ?
O1W H11W 0.805(18) . ?
O1W H12W 0.823(18) . ?
O2W H21W 0.843(18) . ?
O2W H22W 0.797(18) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 C1 O1 121.9(3) . . ?
O2 C1 C2 119.5(3) . . ?
O1 C1 C2 118.4(3) . . ?
C7 C2 C3 117.0(3) . . ?
C7 C2 C1 118.3(3) . . ?
C3 C2 C1 124.6(3) . . ?
C4 C3 C2 123.0(3) . . ?
C4 C3 N1 116.3(3) . . ?
C2 C3 N1 120.7(3) . . ?
C3 C4 C5 117.6(3) . . ?
C3 C4 H4 121.2 . . ?
C5 C4 H4 121.2 . . ?
C6 C5 C4 122.3(3) . . ?
C6 C5 N2 119.8(3) . . ?
C4 C5 N2 117.9(3) . . ?
C5 C6 C7 119.4(3) . . ?
C5 C6 H6 120.3 . . ?
C7 C6 H6 120.3 . . ?
C6 C7 C2 120.8(3) . . ?
C6 C7 H7 119.6 . . ?
C2 C7 H7 119.6 . . ?
O8 C8 O7 119.8(3) . . ?
O8 C8 C9 120.0(3) . . ?
O7 C8 C9 120.3(3) . . ?
C8 C9 H9A 109.5 . . ?
C8 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C8 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
O10 C10 O9 118.9(3) . . ?
O10 C10 C11 119.9(3) . . ?
O9 C10 C11 121.1(3) . . ?
O10 C10 Dy1 53.74(15) . 5_666 ?
O9 C10 Dy1 65.58(16) . 5_666 ?
C11 C10 Dy1 169.8(2) . 5_666 ?
C10 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C10 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
O3 N1 O4 124.0(3) . . ?
O3 N1 C3 118.5(3) . . ?
O4 N1 C3 117.5(3) . . ?
O6 N2 O5 124.3(3) . . ?
O6 N2 C5 117.9(4) . . ?
O5 N2 C5 117.8(3) . . ?
C1 O1 Dy1 92.16(17) . . ?
C1 O2 Dy1 92.53(19) . . ?
C8 O7 Dy1 90.46(17) . . ?
C8 O8 Dy1 96.65(17) . . ?
C10 O9 Dy1 155.4(2) . . ?
C10 O9 Dy1 88.86(17) . 5_666 ?
Dy1 O9 Dy1 113.78(8) . 5_666 ?
C10 O10 Dy1 101.47(17) . 5_666 ?
O9 Dy1 O2W 77.95(8) . . ?
O9 Dy1 O1W 154.58(7) . . ?
O2W Dy1 O1W 83.49(8) . . ?
O9 Dy1 O8 74.81(7) . . ?
O2W Dy1 O8 143.02(8) . . ?
O1W Dy1 O8 128.97(7) . . ?
O9 Dy1 O10 116.23(7) . 5_666 ?
O2W Dy1 O10 78.60(10) . 5_666 ?
O1W Dy1 O10 76.22(8) . 5_666 ?
O8 Dy1 O10 91.49(8) . 5_666 ?
O9 Dy1 O2 96.05(8) . . ?
O2W Dy1 O2 127.83(8) . . ?
O1W Dy1 O2 81.71(9) . . ?
O8 Dy1 O2 79.92(7) . . ?
O10 Dy1 O2 143.23(8) 5_666 . ?
O9 Dy1 O1 85.41(7) . . ?
O2W Dy1 O1 75.25(8) . . ?
O1W Dy1 O1 73.07(7) . . ?
O8 Dy1 O1 126.12(8) . . ?
O10 Dy1 O1 141.41(8) 5_666 . ?
O2 Dy1 O1 52.58(7) . . ?
O9 Dy1 O7 127.88(7) . . ?
O2W Dy1 O7 147.15(8) . . ?
O1W Dy1 O7 76.19(7) . . ?
O8 Dy1 O7 53.12(7) . . ?
O10 Dy1 O7 71.70(8) 5_666 . ?
O2 Dy1 O7 74.70(8) . . ?
O1 Dy1 O7 121.42(8) . . ?
O9 Dy1 O9 66.22(8) . 5_666 ?
O2W Dy1 O9 72.27(7) . 5_666 ?
O1W Dy1 O9 124.00(8) . 5_666 ?
O8 Dy1 O9 74.08(7) . 5_666 ?
O10 Dy1 O9 50.24(6) 5_666 5_666 ?
O2 Dy1 O9 151.52(7) . 5_666 ?
O1 Dy1 O9 140.38(7) . 5_666 ?
O7 Dy1 O9 98.09(7) . 5_666 ?
O9 Dy1 C10 91.45(8) . 5_666 ?
O2W Dy1 C10 72.22(8) . 5_666 ?
O1W Dy1 C10 99.32(9) . 5_666 ?
O8 Dy1 C10 83.89(8) . 5_666 ?
O10 Dy1 C10 24.79(7) 5_666 5_666 ?
O2 Dy1 C10 159.68(8) . 5_666 ?
O1 Dy1 C10 147.24(8) . 5_666 ?
O7 Dy1 C10 85.78(8) . 5_666 ?
O9 Dy1 C10 25.56(6) 5_666 5_666 ?
Dy1 O1W H11W 126(3) . . ?
Dy1 O1W H12W 123(2) . . ?
H11W O1W H12W 111(4) . . ?
Dy1 O2W H21W 129(3) . . ?
Dy1 O2W H22W 120(3) . . ?
H21W O2W H22W 111(4) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O2 C1 C2 C7 -129.7(3) . . . . ?
O1 C1 C2 C7 45.5(4) . . . . ?
O2 C1 C2 C3 45.1(4) . . . . ?
O1 C1 C2 C3 -139.6(3) . . . . ?
C7 C2 C3 C4 1.0(5) . . . . ?
C1 C2 C3 C4 -174.0(3) . . . . ?
C7 C2 C3 N1 -176.0(3) . . . . ?
C1 C2 C3 N1 9.1(5) . . . . ?
C2 C3 C4 C5 -1.2(5) . . . . ?
N1 C3 C4 C5 176.0(3) . . . . ?
C3 C4 C5 C6 0.3(5) . . . . ?
C3 C4 C5 N2 -178.9(3) . . . . ?
C4 C5 C6 C7 0.6(5) . . . . ?
N2 C5 C6 C7 179.9(3) . . . . ?
C5 C6 C7 C2 -0.8(5) . . . . ?
C3 C2 C7 C6 0.0(5) . . . . ?
C1 C2 C7 C6 175.3(3) . . . . ?
C4 C3 N1 O3 -139.3(3) . . . . ?
C2 C3 N1 O3 37.9(5) . . . . ?
C4 C3 N1 O4 38.7(5) . . . . ?
C2 C3 N1 O4 -144.1(3) . . . . ?
C6 C5 N2 O6 -12.3(5) . . . . ?
C4 C5 N2 O6 167.0(4) . . . . ?
C6 C5 N2 O5 167.1(3) . . . . ?
C4 C5 N2 O5 -13.6(5) . . . . ?
O2 C1 O1 Dy1 9.3(3) . . . . ?
C2 C1 O1 Dy1 -165.8(2) . . . . ?
O1 C1 O2 Dy1 -9.3(3) . . . . ?
C2 C1 O2 Dy1 165.8(2) . . . . ?
O8 C8 O7 Dy1 -0.5(3) . . . . ?
C9 C8 O7 Dy1 -179.9(3) . . . . ?
O7 C8 O8 Dy1 0.5(3) . . . . ?
C9 C8 O8 Dy1 180.0(3) . . . . ?
O10 C10 O9 Dy1 164.5(3) . . . . ?
C11 C10 O9 Dy1 -13.6(6) . . . . ?
Dy1 C10 O9 Dy1 157.7(5) 5_666 . . . ?
O10 C10 O9 Dy1 6.9(3) . . . 5_666 ?
C11 C10 O9 Dy1 -171.3(3) . . . 5_666 ?
O9 C10 O10 Dy1 -7.7(3) . . . 5_666 ?
C11 C10 O10 Dy1 170.4(3) . . . 5_666 ?

_refine_diff_density_max         0.649
_refine_diff_density_min         -0.879
_refine_diff_density_rms         0.103

