# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_leung1092m
_database_code_depnum_ccdc_archive 'CCDC 1874977'
_audit_update_record             
;
2018-10-24 deposited with the CCDC.
2018-12-17 downloaded from the CCDC.
;
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C29 H25 Au Cl Fe O2 P'
_chemical_formula_iupac          ?
_chemical_formula_weight         724.72

_chemical_melting_point          ?

_space_group_crystal_system      monoclinic
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   9.0226(2)
_cell_length_b                   11.2002(2)
_cell_length_c                   25.5416(6)
_cell_angle_alpha                90
_cell_angle_beta                 96.9250(10)
_cell_angle_gamma                90
_cell_volume                     2562.27(9)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9985
_cell_measurement_theta_min      2.4265
_cell_measurement_theta_max      31.4798
_cell_measurement_temperature    100.(2)

_exptl_crystal_description       block
_exptl_crystal_colour            orange
_exptl_crystal_size_max          0.100
_exptl_crystal_size_mid          0.040
_exptl_crystal_size_min          0.020
_exptl_crystal_density_diffrn    1.879
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1408

_exptl_absorpt_coefficient_mu    6.477
_exptl_absorpt_correction_type   Multi-Scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction
;
_exptl_absorpt_correction_T_min  0.58
_exptl_absorpt_correction_T_max  0.88

_exptl_special_details           
;
;

_diffrn_ambient_temperature      100.(2)

_diffrn_source                   'Incoatec microfocus source'
_diffrn_source_type              'Bruker D8 Quest'

_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_monochromator  'Multilayer Mirror'

_diffrn_measurement_device_type  'Photon II CPADs detector'
_diffrn_measurement_method       'phi and omega scans'

_diffrn_detector_area_resol_mean 7.4074

_diffrn_reflns_number            34522
_diffrn_reflns_av_R_equivalents  0.0622
_diffrn_reflns_av_unetI/netI     0.0624
_diffrn_reflns_theta_min         2.27
_diffrn_reflns_theta_max         31.53
_diffrn_reflns_theta_full        31.53
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measured_fraction_theta_full 0.997
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_limit_l_max       37

_refine_special_details          
;
;

_reflns_number_total             8538
_reflns_number_gt                6521
_reflns_threshold_expression     'I > 2σ(I)'

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_R_factor_all          0.0617
_refine_ls_R_factor_gt           0.0386
_refine_ls_wR_factor_gt          0.0621
_refine_ls_wR_factor_ref         0.0708
_refine_ls_goodness_of_fit_ref   1.030
_refine_ls_restrained_S_all      1.030
_refine_ls_number_reflns         8538
_refine_ls_number_parameters     316
_refine_ls_number_restraints     0
_refine_ls_number_constraints    ?
_refine_ls_hydrogen_treatment    constr
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0169P)²+3.8876P] where P=(Fo²+2Fc²)/3'

_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?

_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_diff_density_max         1.396
_refine_diff_density_min         -1.609
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_computing_data_collection       'APEX3 (Bruker AXS Inc., 2018)'
_computing_cell_refinement       'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_data_reduction        'SAINT V8.38A (Bruker AXS Inc., 2017)'
_computing_structure_solution    'XT, VERSION 2014/5'
_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_computing_molecular_graphics    'XP (Bruker AXS Inc., 2018)'
_computing_publication_material  'APEX3 (Bruker AXS Inc., 2018)'

loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_refinement_flags_posn
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au Au1 0.83846(2) 0.84284(2) 0.47177(2) 0.01478(4) Uani d . . . 1 . .
C C1 0.1629(6) 0.4717(5) 0.4439(2) 0.0406(13) Uani d . . . 1 . .
H H1 0.161451 0.432824 0.479135 0.049 Uiso calc U . R 1 . .
C C2 0.0660(5) 0.5618(5) 0.4226(2) 0.0304(11) Uani d . . . 1 . .
H H2 -0.016082 0.598924 0.440063 0.037 Uiso calc U . R 1 . .
C C3 0.1051(5) 0.5918(4) 0.37261(19) 0.0248(10) Uani d . . . 1 . .
H H3 0.055618 0.654133 0.34848 0.03 Uiso calc U . R 1 . .
C C4 0.2265(5) 0.5202(4) 0.3625(2) 0.0300(11) Uani d . . . 1 . .
H H4 0.277867 0.521523 0.329926 0.036 Uiso calc U . R 1 . .
C C5 0.2616(5) 0.4450(4) 0.4070(2) 0.0389(14) Uani d . . . 1 . .
H H5 0.343047 0.383882 0.411449 0.047 Uiso calc U . R 1 . .
C C6 0.4876(4) 0.6504(4) 0.46978(16) 0.0188(8) Uani d . . . 1 . .
H H6 0.565875 0.588942 0.480406 0.023 Uiso calc U . R 1 . .
C C7 0.3720(5) 0.6869(4) 0.50000(18) 0.0249(10) Uani d . . . 1 . .
H H7 0.355469 0.655553 0.535503 0.03 Uiso calc U . R 1 . .
C C8 0.2844(5) 0.7744(4) 0.47080(19) 0.0254(10) Uani d . . . 1 . .
H H8 0.195275 0.815676 0.482123 0.03 Uiso calc U . R 1 . .
C C9 0.3436(4) 0.7927(3) 0.42250(18) 0.0189(9) Uani d . . . 1 . .
H H9 0.303282 0.849251 0.393967 0.023 Uiso calc U . R 1 . .
C C10 0.4701(4) 0.7157(3) 0.42122(16) 0.0138(7) Uani d . . . 1 . .
C C11 0.5747(4) 0.7170(3) 0.37960(16) 0.0139(8) Uani d . . . 1 . .
H H11 0.51376 0.731093 0.344777 0.017 Uiso calc U . R 1 . .
C C12 0.6632(4) 0.6001(3) 0.37542(16) 0.0154(8) Uani d . . . 1 . .
H H12A 0.769159 0.620059 0.373145 0.018 Uiso calc U . R 1 . .
H H12B 0.659138 0.552796 0.407963 0.018 Uiso calc U . R 1 . .
C C13 0.6053(4) 0.5244(3) 0.32832(16) 0.0147(8) Uani d . . . 1 . .
C C14 0.6693(4) 0.4052(3) 0.32628(15) 0.0145(8) Uani d . . . 1 . .
C C15 0.7727(4) 0.3434(4) 0.35862(16) 0.0181(8) Uani d . . . 1 . .
H H15 0.823714 0.370306 0.391203 0.022 Uiso calc U . R 1 . .
C C16 0.7899(5) 0.2315(3) 0.33451(18) 0.0211(9) Uani d . . . 1 . .
H H16 0.855249 0.168931 0.347525 0.025 Uiso calc U . R 1 . .
C C17 0.6961(5) 0.2310(3) 0.28980(18) 0.0227(9) Uani d . . . 1 . .
H H17 0.683763 0.165686 0.265918 0.027 Uiso calc U . R 1 . .
C C18 0.5764(4) 0.9716(3) 0.38421(15) 0.0126(7) Uani d . . . 1 . .
C C19 0.5408(4) 1.0332(3) 0.42876(16) 0.0178(8) Uani d . . . 1 . .
H H19 0.593602 1.017587 0.462527 0.021 Uiso calc U . R 1 . .
C C20 0.4267(5) 1.1178(4) 0.42278(18) 0.0209(9) Uani d . . . 1 . .
H H20 0.400035 1.158762 0.45284 0.025 Uiso calc U . R 1 . .
C C21 0.3518(5) 1.1428(4) 0.37336(17) 0.0203(9) Uani d . . . 1 . .
H H21 0.272977 1.199495 0.369779 0.024 Uiso calc U . R 1 . .
C C22 0.3919(5) 1.0849(4) 0.32914(17) 0.0194(8) Uani d . . . 1 . .
H H22 0.343513 1.104312 0.295094 0.023 Uiso calc U . R 1 . .
C C23 0.5030(4) 0.9986(3) 0.33483(16) 0.0159(8) Uani d . . . 1 . .
H H23 0.52896 0.957747 0.304647 0.019 Uiso calc U . R 1 . .
C C24 0.8145(4) 0.8527(3) 0.33870(15) 0.0144(7) Uani d . . . 1 . .
C C25 0.7650(5) 0.8105(4) 0.28828(17) 0.0201(9) Uani d . . . 1 . .
H H25 0.671506 0.770949 0.281839 0.024 Uiso calc U . R 1 . .
C C26 0.8516(5) 0.8261(4) 0.24750(18) 0.0250(10) Uani d . . . 1 . .
H H26 0.81763 0.796694 0.213256 0.03 Uiso calc U . R 1 . .
C C27 0.9870(5) 0.8841(4) 0.25668(19) 0.0259(10) Uani d . . . 1 . .
H H27 1.045667 0.895782 0.228604 0.031 Uiso calc U . R 1 . .
C C28 1.0375(5) 0.9254(4) 0.30656(19) 0.0254(10) Uani d . . . 1 . .
H H28 1.131275 0.964708 0.312746 0.031 Uiso calc U . R 1 . .
C C29 0.9524(4) 0.9098(4) 0.34764(17) 0.0186(8) Uani d . . . 1 . .
H H29 0.987948 0.938068 0.381933 0.022 Uiso calc U . R 1 . .
Cl Cl1 0.97890(11) 0.84359(10) 0.55232(4) 0.0250(2) Uani d . . . 1 . .
Fe Fe1 0.28153(6) 0.61895(5) 0.42895(2) 0.01630(12) Uani d . . . 1 . .
O O1 0.5147(3) 0.5612(2) 0.29272(11) 0.0199(6) Uani d . . . 1 . .
O O2 0.6202(3) 0.3364(2) 0.28290(12) 0.0211(6) Uani d . . . 1 . .
P P1 0.70238(10) 0.84546(9) 0.39305(4) 0.01203(18) Uani d . . . 1 . .


_geom_special_details            
;

All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix.  The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry.  An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Au1 P1 . 2.2260(10) ?
Au1 Cl1 . 2.2825(11) ?
C1 C2 . 1.402(7) ?
C1 C5 . 1.406(8) ?
C1 Fe1 . 2.028(5) ?
C1 H1 . 1.0 ?
C2 C3 . 1.406(6) ?
C2 Fe1 . 2.035(4) ?
C2 H2 . 1.0 ?
C3 C4 . 1.406(6) ?
C3 Fe1 . 2.036(4) ?
C3 H3 . 1.0 ?
C4 C5 . 1.420(7) ?
C4 Fe1 . 2.037(4) ?
C4 H4 . 1.0 ?
C5 Fe1 . 2.030(4) ?
C5 H5 . 1.0 ?
C6 C7 . 1.431(5) ?
C6 C10 . 1.432(5) ?
C6 Fe1 . 2.050(4) ?
C6 H6 . 1.0 ?
C7 C8 . 1.414(7) ?
C7 Fe1 . 2.045(5) ?
C7 H7 . 1.0 ?
C8 C9 . 1.417(6) ?
C8 Fe1 . 2.042(4) ?
C8 H8 . 1.0 ?
C9 C10 . 1.435(5) ?
C9 Fe1 . 2.038(4) ?
C9 H9 . 1.0 ?
C10 C11 . 1.504(5) ?
C10 Fe1 . 2.047(4) ?
C11 C12 . 1.545(5) ?
C11 P1 . 1.849(4) ?
C11 H11 . 1.0 ?
C12 C13 . 1.513(5) ?
C12 H12A . 0.99 ?
C12 H12B . 0.99 ?
C13 O1 . 1.219(5) ?
C13 C14 . 1.458(5) ?
C14 C15 . 1.358(5) ?
C14 O2 . 1.378(5) ?
C15 C16 . 1.413(6) ?
C15 H15 . 0.95 ?
C16 C17 . 1.337(6) ?
C16 H16 . 0.95 ?
C17 O2 . 1.366(5) ?
C17 H17 . 0.95 ?
C18 C23 . 1.385(5) ?
C18 C19 . 1.401(5) ?
C18 P1 . 1.811(4) ?
C19 C20 . 1.394(6) ?
C19 H19 . 0.95 ?
C20 C21 . 1.386(6) ?
C20 H20 . 0.95 ?
C21 C22 . 1.388(6) ?
C21 H21 . 0.95 ?
C22 C23 . 1.387(5) ?
C22 H22 . 0.95 ?
C23 H23 . 0.95 ?
C24 C29 . 1.392(5) ?
C24 C25 . 1.394(6) ?
C24 P1 . 1.816(4) ?
C25 C26 . 1.386(5) ?
C25 H25 . 0.95 ?
C26 C27 . 1.379(6) ?
C26 H26 . 0.95 ?
C27 C28 . 1.380(6) ?
C27 H27 . 0.95 ?
C28 C29 . 1.384(5) ?
C28 H28 . 0.95 ?
C29 H29 . 0.95 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
P1 Au1 Cl1 . . 179.00(4) ?
C2 C1 C5 . . 108.0(5) ?
C2 C1 Fe1 . . 70.1(3) ?
C5 C1 Fe1 . . 69.8(3) ?
C2 C1 H1 . . 126.0 ?
C5 C1 H1 . . 126.0 ?
Fe1 C1 H1 . . 126.0 ?
C1 C2 C3 . . 108.2(4) ?
C1 C2 Fe1 . . 69.6(3) ?
C3 C2 Fe1 . . 69.8(2) ?
C1 C2 H2 . . 125.9 ?
C3 C2 H2 . . 125.9 ?
Fe1 C2 H2 . . 125.9 ?
C4 C3 C2 . . 108.5(4) ?
C4 C3 Fe1 . . 69.8(3) ?
C2 C3 Fe1 . . 69.8(3) ?
C4 C3 H3 . . 125.8 ?
C2 C3 H3 . . 125.8 ?
Fe1 C3 H3 . . 125.8 ?
C3 C4 C5 . . 107.2(4) ?
C3 C4 Fe1 . . 69.8(3) ?
C5 C4 Fe1 . . 69.3(3) ?
C3 C4 H4 . . 126.4 ?
C5 C4 H4 . . 126.4 ?
Fe1 C4 H4 . . 126.4 ?
C1 C5 C4 . . 108.2(4) ?
C1 C5 Fe1 . . 69.7(3) ?
C4 C5 Fe1 . . 69.8(3) ?
C1 C5 H5 . . 125.9 ?
C4 C5 H5 . . 125.9 ?
Fe1 C5 H5 . . 125.9 ?
C7 C6 C10 . . 108.1(4) ?
C7 C6 Fe1 . . 69.4(2) ?
C10 C6 Fe1 . . 69.4(2) ?
C7 C6 H6 . . 126.0 ?
C10 C6 H6 . . 126.0 ?
Fe1 C6 H6 . . 126.0 ?
C8 C7 C6 . . 108.1(4) ?
C8 C7 Fe1 . . 69.6(3) ?
C6 C7 Fe1 . . 69.7(2) ?
C8 C7 H7 . . 125.9 ?
C6 C7 H7 . . 125.9 ?
Fe1 C7 H7 . . 125.9 ?
C7 C8 C9 . . 108.3(4) ?
C7 C8 Fe1 . . 69.9(3) ?
C9 C8 Fe1 . . 69.5(2) ?
C7 C8 H8 . . 125.8 ?
C9 C8 H8 . . 125.8 ?
Fe1 C8 H8 . . 125.8 ?
C8 C9 C10 . . 108.5(4) ?
C8 C9 Fe1 . . 69.8(2) ?
C10 C9 Fe1 . . 69.8(2) ?
C8 C9 H9 . . 125.8 ?
C10 C9 H9 . . 125.8 ?
Fe1 C9 H9 . . 125.8 ?
C6 C10 C9 . . 107.0(3) ?
C6 C10 C11 . . 127.2(3) ?
C9 C10 C11 . . 125.4(4) ?
C6 C10 Fe1 . . 69.7(2) ?
C9 C10 Fe1 . . 69.1(2) ?
C11 C10 Fe1 . . 132.3(3) ?
C10 C11 C12 . . 114.5(3) ?
C10 C11 P1 . . 107.8(3) ?
C12 C11 P1 . . 110.9(2) ?
C10 C11 H11 . . 107.8 ?
C12 C11 H11 . . 107.8 ?
P1 C11 H11 . . 107.8 ?
C13 C12 C11 . . 113.5(3) ?
C13 C12 H12A . . 108.9 ?
C11 C12 H12A . . 108.9 ?
C13 C12 H12B . . 108.9 ?
C11 C12 H12B . . 108.9 ?
H12A C12 H12B . . 107.7 ?
O1 C13 C14 . . 121.1(4) ?
O1 C13 C12 . . 122.7(3) ?
C14 C13 C12 . . 116.2(3) ?
C15 C14 O2 . . 109.6(3) ?
C15 C14 C13 . . 133.7(4) ?
O2 C14 C13 . . 116.7(3) ?
C14 C15 C16 . . 106.8(4) ?
C14 C15 H15 . . 126.6 ?
C16 C15 H15 . . 126.6 ?
C17 C16 C15 . . 106.6(4) ?
C17 C16 H16 . . 126.7 ?
C15 C16 H16 . . 126.7 ?
C16 C17 O2 . . 111.2(4) ?
C16 C17 H17 . . 124.4 ?
O2 C17 H17 . . 124.4 ?
C23 C18 C19 . . 120.1(4) ?
C23 C18 P1 . . 120.5(3) ?
C19 C18 P1 . . 119.0(3) ?
C20 C19 C18 . . 119.0(4) ?
C20 C19 H19 . . 120.5 ?
C18 C19 H19 . . 120.5 ?
C21 C20 C19 . . 120.6(4) ?
C21 C20 H20 . . 119.7 ?
C19 C20 H20 . . 119.7 ?
C22 C21 C20 . . 120.0(4) ?
C22 C21 H21 . . 120.0 ?
C20 C21 H21 . . 120.0 ?
C21 C22 C23 . . 119.7(4) ?
C21 C22 H22 . . 120.1 ?
C23 C22 H22 . . 120.1 ?
C18 C23 C22 . . 120.5(4) ?
C18 C23 H23 . . 119.8 ?
C22 C23 H23 . . 119.8 ?
C29 C24 C25 . . 119.2(3) ?
C29 C24 P1 . . 117.7(3) ?
C25 C24 P1 . . 123.0(3) ?
C26 C25 C24 . . 120.3(4) ?
C26 C25 H25 . . 119.8 ?
C24 C25 H25 . . 119.8 ?
C27 C26 C25 . . 120.0(4) ?
C27 C26 H26 . . 120.0 ?
C25 C26 H26 . . 120.0 ?
C26 C27 C28 . . 120.1(4) ?
C26 C27 H27 . . 119.9 ?
C28 C27 H27 . . 119.9 ?
C29 C28 C27 . . 120.4(4) ?
C29 C28 H28 . . 119.8 ?
C27 C28 H28 . . 119.8 ?
C28 C29 C24 . . 120.0(4) ?
C28 C29 H29 . . 120.0 ?
C24 C29 H29 . . 120.0 ?
C1 Fe1 C5 . . 40.5(2) ?
C1 Fe1 C2 . . 40.4(2) ?
C5 Fe1 C2 . . 67.9(2) ?
C1 Fe1 C3 . . 68.1(2) ?
C5 Fe1 C3 . . 68.0(2) ?
C2 Fe1 C3 . . 40.40(18) ?
C1 Fe1 C4 . . 68.6(2) ?
C5 Fe1 C4 . . 40.9(2) ?
C2 Fe1 C4 . . 68.17(18) ?
C3 Fe1 C4 . . 40.41(17) ?
C1 Fe1 C9 . . 161.6(2) ?
C5 Fe1 C9 . . 155.7(2) ?
C2 Fe1 C9 . . 124.26(19) ?
C3 Fe1 C9 . . 106.53(18) ?
C4 Fe1 C9 . . 119.6(2) ?
C1 Fe1 C8 . . 124.6(2) ?
C5 Fe1 C8 . . 163.4(2) ?
C2 Fe1 C8 . . 105.16(18) ?
C3 Fe1 C8 . . 117.18(19) ?
C4 Fe1 C8 . . 152.4(2) ?
C9 Fe1 C8 . . 40.64(16) ?
C1 Fe1 C7 . . 107.4(2) ?
C5 Fe1 C7 . . 127.9(2) ?
C2 Fe1 C7 . . 117.57(18) ?
C3 Fe1 C7 . . 151.30(17) ?
C4 Fe1 C7 . . 166.6(2) ?
C9 Fe1 C7 . . 68.41(18) ?
C8 Fe1 C7 . . 40.48(19) ?
C1 Fe1 C10 . . 155.89(19) ?
C5 Fe1 C10 . . 121.91(18) ?
C2 Fe1 C10 . . 163.00(19) ?
C3 Fe1 C10 . . 126.81(17) ?
C4 Fe1 C10 . . 109.23(17) ?
C9 Fe1 C10 . . 41.13(15) ?
C8 Fe1 C10 . . 68.94(15) ?
C7 Fe1 C10 . . 68.97(16) ?
C1 Fe1 C6 . . 120.7(2) ?
C5 Fe1 C6 . . 110.49(19) ?
C2 Fe1 C6 . . 153.39(18) ?
C3 Fe1 C6 . . 165.77(17) ?
C4 Fe1 C6 . . 129.24(17) ?
C9 Fe1 C6 . . 68.64(17) ?
C8 Fe1 C6 . . 68.50(18) ?
C7 Fe1 C6 . . 40.90(15) ?
C10 Fe1 C6 . . 40.92(15) ?
C17 O2 C14 . . 105.8(3) ?
C18 P1 C24 . . 105.60(17) ?
C18 P1 C11 . . 102.48(16) ?
C24 P1 C11 . . 106.56(18) ?
C18 P1 Au1 . . 113.12(13) ?
C24 P1 Au1 . . 113.18(13) ?
C11 P1 Au1 . . 114.90(13) ?

