# Electronic Supplementary Material (ESI) for RSC Advances.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
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data_eo18a
_database_code_depnum_ccdc_archive 'CCDC 1555880'
_audit_update_record             
;
2017-06-13 deposited with the CCDC.
2018-03-27 downloaded from the CCDC.
;
_audit_creation_date             2016-08-31
_audit_creation_method           
;
Olex2 1.2
(compiled 2016.08.25 svn.r3337 for OlexSys, GUI svn.r5221)
;
_chemical_name_common            ?
_chemical_name_systematic        
'bis(2-benzyl-3,5-diphenyl-2,3-dihydro-1H-pyrazol-1-yl)palladium(IV) chloride'
_chemical_formula_moiety         'C22 H18 Cl N2 Pd0.5'
_chemical_formula_sum            'C22 H18 Cl N2 Pd0.50'
_chemical_formula_weight         399.03
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   6.7767(6)
_cell_length_b                   10.2586(9)
_cell_length_c                   13.5319(13)
_cell_angle_alpha                102.123(2)
_cell_angle_beta                 98.442(2)
_cell_angle_gamma                94.970(2)
_cell_volume                     903.05(14)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    6135
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.33
_cell_measurement_theta_min      2.28
_shelx_estimated_absorpt_T_max   0.921
_shelx_estimated_absorpt_T_min   0.785
_exptl_absorpt_coefficient_mu    0.700
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.6894
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2014/5 (Bruker,2014/5) was used for absorption correction.
wR2(int) was 0.0500 before and 0.0442 after correction.
The Ratio of minimum to maximum transmission is 0.9245.
The λ/2 correction factor is 0.00150.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.467
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             408
_exptl_crystal_size_max          0.364
_exptl_crystal_size_mid          0.125
_exptl_crystal_size_min          0.12
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0346
_diffrn_reflns_av_unetI/netI     0.0391
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            12765
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         28.357
_diffrn_reflns_theta_min         2.046
_diffrn_ambient_temperature      100(2)
_diffrn_detector                 'Bruker APEX2 area detector'
_diffrn_detector_area_resol_mean 7.9
_diffrn_detector_type            'CCD area detector'
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker SMART APEX2 area detector'
_diffrn_measurement_method       'ω and φ scans'
_diffrn_radiation_monochromator  'mirror optics'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'microfocus sealed X-ray tube'
_diffrn_source_type              'Incoatec I\ms'
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                4175
_reflns_number_total             4497
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.34A (Bruker, 2013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_refine_diff_density_max         0.457
_refine_diff_density_min         -0.311
_refine_diff_density_rms         0.079
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.082
_refine_ls_hydrogen_treatment    refall
_refine_ls_matrix_type           full
_refine_ls_number_parameters     304
_refine_ls_number_reflns         4497
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0316
_refine_ls_R_factor_gt           0.0287
_refine_ls_restrained_S_all      1.082
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0280P)²+0.4300P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0674
_refine_ls_wR_factor_ref         0.0687
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
_atom_sites_special_details      
;
The structure was solved using Patterson Methods, followed by a Tangent Expansion (ShelXS). RE = 0.2, Nqual =   0, Ralpha = 0.032
;
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd1 Pd 0.5000 0.5000 0.0000 0.01115(6) Uani 1 2 d S T P . .
Cl1 Cl 0.73553(6) 0.68220(4) 0.07234(3) 0.01664(10) Uani 1 1 d . . . . .
N2 N 0.3330(2) 0.56765(15) 0.19516(12) 0.0131(3) Uani 1 1 d . . . . .
N1 N 0.4455(2) 0.48586(15) 0.13993(12) 0.0127(3) Uani 1 1 d . . . . .
C22 C 0.2749(3) 0.61495(19) 0.46003(15) 0.0171(4) Uani 1 1 d . . . . .
H22 H 0.402(4) 0.600(2) 0.4759(18) 0.020(6) Uiso 1 1 d . . . . .
C6 C 0.3043(3) 0.81257(18) 0.23966(14) 0.0150(4) Uani 1 1 d . . . . .
C5 C 0.4987(3) 0.8591(2) 0.29212(16) 0.0192(4) Uani 1 1 d . . . . .
H5 H 0.595(4) 0.807(3) 0.2804(19) 0.028(6) Uiso 1 1 d . . . . .
C18 C -0.0138(3) 0.6094(2) 0.33138(16) 0.0184(4) Uani 1 1 d . . . . .
H18 H -0.078(3) 0.587(2) 0.2614(19) 0.021(6) Uiso 1 1 d . . . . .
C21 C 0.1668(3) 0.6650(2) 0.53660(16) 0.0205(4) Uani 1 1 d . . . . .
H21 H 0.224(4) 0.682(3) 0.603(2) 0.033(7) Uiso 1 1 d . . . . .
C12 C 0.7861(3) 0.3086(2) 0.11812(15) 0.0191(4) Uani 1 1 d . . . . .
H12 H 0.829(3) 0.392(2) 0.1175(16) 0.013(5) Uiso 1 1 d . . . . .
C7 C 0.2602(3) 0.68345(18) 0.15880(14) 0.0147(3) Uani 1 1 d . . . . .
H7A H 0.124(3) 0.663(2) 0.1328(17) 0.015(5) Uiso 1 1 d . . . . .
H7B H 0.323(3) 0.689(2) 0.1012(18) 0.018(6) Uiso 1 1 d . . . . .
C19 C -0.1213(3) 0.6583(2) 0.40821(17) 0.0217(4) Uani 1 1 d . . . . .
H19 H -0.248(4) 0.675(3) 0.390(2) 0.030(7) Uiso 1 1 d . . . . .
C1 C 0.1504(3) 0.8899(2) 0.26067(17) 0.0217(4) Uani 1 1 d . . . . .
H1 H 0.029(4) 0.863(2) 0.2270(18) 0.019(6) Uiso 1 1 d . . . . .
C16 C 0.5415(4) 0.1498(2) 0.15566(18) 0.0287(5) Uani 1 1 d . . . . .
H16 H 0.419(4) 0.129(3) 0.175(2) 0.034(7) Uiso 1 1 d . . . . .
C20 C -0.0319(3) 0.68541(19) 0.51009(16) 0.0211(4) Uani 1 1 d . . . . .
H20 H -0.105(4) 0.710(2) 0.5567(19) 0.028(6) Uiso 1 1 d . . . . .
C13 C 0.8999(4) 0.2053(2) 0.08767(18) 0.0279(5) Uani 1 1 d . . . . .
H13 H 1.021(4) 0.226(3) 0.067(2) 0.035(7) Uiso 1 1 d . . . . .
C4 C 0.5374(3) 0.9793(2) 0.36510(17) 0.0251(4) Uani 1 1 d . . . . .
H4 H 0.663(4) 1.009(3) 0.400(2) 0.036(7) Uiso 1 1 d . . . . .
C14 C 0.8340(4) 0.0756(2) 0.0906(2) 0.0378(6) Uani 1 1 d . . . . .
H14 H 0.909(4) 0.006(3) 0.072(2) 0.044(8) Uiso 1 1 d . . . . .
C3 C 0.3821(4) 1.0549(2) 0.38611(17) 0.0268(5) Uani 1 1 d . . . . .
H3 H 0.403(4) 1.136(3) 0.437(2) 0.036(7) Uiso 1 1 d . . . . .
C2 C 0.1891(4) 1.0105(2) 0.33322(19) 0.0281(5) Uani 1 1 d . . . . .
H2 H 0.083(4) 1.063(3) 0.348(2) 0.036(7) Uiso 1 1 d . . . . .
C15 C 0.6553(5) 0.0471(2) 0.1238(2) 0.0413(7) Uani 1 1 d . . . . .
H15 H 0.617(4) -0.034(3) 0.123(2) 0.032(7) Uiso 1 1 d . . . . .
C10 C 0.4853(3) 0.38862(18) 0.18966(14) 0.0143(3) Uani 1 1 d . . . . .
C8 C 0.3007(3) 0.52245(18) 0.27964(14) 0.0137(3) Uani 1 1 d . . . . .
C17 C 0.1858(3) 0.58587(17) 0.35731(14) 0.0142(3) Uani 1 1 d . . . . .
C11 C 0.6058(3) 0.28117(19) 0.15298(14) 0.0171(4) Uani 1 1 d . . . . .
C9 C 0.3969(3) 0.40849(18) 0.27776(14) 0.0154(4) Uani 1 1 d . . . . .
H9 H 0.399(3) 0.355(2) 0.3262(17) 0.018(6) Uiso 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pd1 Cl1 2.2924(4) . ?
Pd1 Cl1 2.2924(4) 2_665 ?
Pd1 N1 2.0135(15) 2_665 ?
Pd1 N1 2.0135(15) . ?
N2 N1 1.363(2) . ?
N2 C7 1.474(2) . ?
N2 C8 1.359(2) . ?
N1 C10 1.340(2) . ?
C22 H22 0.89(2) . ?
C22 C21 1.392(3) . ?
C22 C17 1.391(3) . ?
C6 C5 1.393(3) . ?
C6 C7 1.506(3) . ?
C6 C1 1.391(3) . ?
C5 H5 0.89(3) . ?
C5 C4 1.386(3) . ?
C18 H18 0.95(2) . ?
C18 C19 1.389(3) . ?
C18 C17 1.402(3) . ?
C21 H21 0.90(3) . ?
C21 C20 1.387(3) . ?
C12 H12 0.88(2) . ?
C12 C13 1.393(3) . ?
C12 C11 1.400(3) . ?
C7 H7A 0.93(2) . ?
C7 H7B 0.95(2) . ?
C19 H19 0.89(3) . ?
C19 C20 1.382(3) . ?
C1 H1 0.87(2) . ?
C1 C2 1.386(3) . ?
C16 H16 0.93(3) . ?
C16 C15 1.392(3) . ?
C16 C11 1.390(3) . ?
C20 H20 0.87(3) . ?
C13 H13 0.93(3) . ?
C13 C14 1.377(3) . ?
C4 H4 0.90(3) . ?
C4 C3 1.388(3) . ?
C14 H14 0.93(3) . ?
C14 C15 1.381(4) . ?
C3 H3 0.95(3) . ?
C3 C2 1.383(3) . ?
C2 H2 0.95(3) . ?
C15 H15 0.85(3) . ?
C10 C11 1.474(2) . ?
C10 C9 1.397(2) . ?
C8 C17 1.475(2) . ?
C8 C9 1.384(2) . ?
C9 H9 0.94(2) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Pd1 Cl1 180.0 2_665 . ?
N1 Pd1 Cl1 90.39(4) 2_665 2_665 ?
N1 Pd1 Cl1 89.61(4) 2_665 . ?
N1 Pd1 Cl1 90.39(4) . . ?
N1 Pd1 Cl1 89.61(4) . 2_665 ?
N1 Pd1 N1 180.0 2_665 . ?
N1 N2 C7 120.47(14) . . ?
C8 N2 N1 110.22(14) . . ?
C8 N2 C7 129.29(15) . . ?
N2 N1 Pd1 123.97(11) . . ?
C10 N1 Pd1 128.22(13) . . ?
C10 N1 N2 107.24(14) . . ?
C21 C22 H22 120.7(16) . . ?
C17 C22 H22 118.7(16) . . ?
C17 C22 C21 120.59(19) . . ?
C5 C6 C7 121.28(17) . . ?
C1 C6 C5 118.82(18) . . ?
C1 C6 C7 119.86(17) . . ?
C6 C5 H5 118.3(17) . . ?
C4 C5 C6 120.58(19) . . ?
C4 C5 H5 121.0(17) . . ?
C19 C18 H18 120.3(14) . . ?
C19 C18 C17 119.84(19) . . ?
C17 C18 H18 119.8(14) . . ?
C22 C21 H21 120.4(17) . . ?
C20 C21 C22 119.64(19) . . ?
C20 C21 H21 119.9(17) . . ?
C13 C12 H12 120.1(14) . . ?
C13 C12 C11 120.13(19) . . ?
C11 C12 H12 119.8(14) . . ?
N2 C7 C6 113.30(15) . . ?
N2 C7 H7A 108.5(13) . . ?
N2 C7 H7B 105.5(13) . . ?
C6 C7 H7A 112.0(14) . . ?
C6 C7 H7B 111.6(14) . . ?
H7A C7 H7B 105.4(18) . . ?
C18 C19 H19 118.9(17) . . ?
C20 C19 C18 120.43(19) . . ?
C20 C19 H19 120.7(17) . . ?
C6 C1 H1 119.5(16) . . ?
C2 C1 C6 120.7(2) . . ?
C2 C1 H1 119.9(16) . . ?
C15 C16 H16 119.2(16) . . ?
C11 C16 H16 120.6(16) . . ?
C11 C16 C15 120.2(2) . . ?
C21 C20 H20 121.0(17) . . ?
C19 C20 C21 120.25(19) . . ?
C19 C20 H20 118.6(17) . . ?
C12 C13 H13 118.6(17) . . ?
C14 C13 C12 120.0(2) . . ?
C14 C13 H13 121.4(17) . . ?
C5 C4 H4 120.5(18) . . ?
C5 C4 C3 120.0(2) . . ?
C3 C4 H4 119.5(18) . . ?
C13 C14 H14 120.9(17) . . ?
C13 C14 C15 120.3(2) . . ?
C15 C14 H14 118.8(17) . . ?
C4 C3 H3 122.0(17) . . ?
C2 C3 C4 119.8(2) . . ?
C2 C3 H3 118.2(17) . . ?
C1 C2 H2 120.7(17) . . ?
C3 C2 C1 120.1(2) . . ?
C3 C2 H2 119.2(16) . . ?
C16 C15 H15 121.6(18) . . ?
C14 C15 C16 120.2(2) . . ?
C14 C15 H15 118.2(18) . . ?
N1 C10 C11 122.90(16) . . ?
N1 C10 C9 109.13(16) . . ?
C9 C10 C11 127.97(16) . . ?
N2 C8 C17 125.41(16) . . ?
N2 C8 C9 106.75(16) . . ?
C9 C8 C17 127.84(16) . . ?
C22 C17 C18 119.23(17) . . ?
C22 C17 C8 118.56(17) . . ?
C18 C17 C8 122.08(17) . . ?
C12 C11 C10 121.68(17) . . ?
C16 C11 C12 119.16(18) . . ?
C16 C11 C10 119.14(17) . . ?
C10 C9 H9 127.2(14) . . ?
C8 C9 C10 106.65(15) . . ?
C8 C9 H9 126.2(14) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Pd1 N1 C10 C11 8.9(3) . . . . ?
Pd1 N1 C10 C9 -171.46(13) . . . . ?
N2 N1 C10 C11 -179.58(17) . . . . ?
N2 N1 C10 C9 0.1(2) . . . . ?
N2 C8 C17 C22 -127.92(19) . . . . ?
N2 C8 C17 C18 56.3(3) . . . . ?
N2 C8 C9 C10 -0.2(2) . . . . ?
N1 N2 C7 C6 -129.97(17) . . . . ?
N1 N2 C8 C17 179.78(16) . . . . ?
N1 N2 C8 C9 0.2(2) . . . . ?
N1 C10 C11 C12 45.2(3) . . . . ?
N1 C10 C11 C16 -136.6(2) . . . . ?
N1 C10 C9 C8 0.1(2) . . . . ?
C22 C21 C20 C19 -1.0(3) . . . . ?
C6 C5 C4 C3 -0.4(3) . . . . ?
C6 C1 C2 C3 -0.4(3) . . . . ?
C5 C6 C7 N2 53.8(2) . . . . ?
C5 C6 C1 C2 -0.6(3) . . . . ?
C5 C4 C3 C2 -0.7(3) . . . . ?
C18 C19 C20 C21 0.5(3) . . . . ?
C21 C22 C17 C18 1.0(3) . . . . ?
C21 C22 C17 C8 -174.90(17) . . . . ?
C12 C13 C14 C15 -0.1(4) . . . . ?
C7 N2 N1 Pd1 -6.5(2) . . . . ?
C7 N2 N1 C10 -178.50(16) . . . . ?
C7 N2 C8 C17 -2.1(3) . . . . ?
C7 N2 C8 C9 178.35(18) . . . . ?
C7 C6 C5 C4 178.89(17) . . . . ?
C7 C6 C1 C2 -178.55(18) . . . . ?
C19 C18 C17 C22 -1.5(3) . . . . ?
C19 C18 C17 C8 174.26(17) . . . . ?
C1 C6 C5 C4 1.0(3) . . . . ?
C1 C6 C7 N2 -128.27(18) . . . . ?
C13 C12 C11 C16 -0.7(3) . . . . ?
C13 C12 C11 C10 177.56(19) . . . . ?
C13 C14 C15 C16 -0.7(4) . . . . ?
C4 C3 C2 C1 1.0(3) . . . . ?
C15 C16 C11 C12 -0.1(4) . . . . ?
C15 C16 C11 C10 -178.4(2) . . . . ?
C8 N2 N1 Pd1 171.79(12) . . . . ?
C8 N2 N1 C10 -0.2(2) . . . . ?
C8 N2 C7 C6 52.1(2) . . . . ?
C17 C22 C21 C20 0.3(3) . . . . ?
C17 C18 C19 C20 0.7(3) . . . . ?
C17 C8 C9 C10 -179.72(18) . . . . ?
C11 C12 C13 C14 0.8(3) . . . . ?
C11 C16 C15 C14 0.8(4) . . . . ?
C11 C10 C9 C8 179.69(19) . . . . ?
C9 C10 C11 C12 -134.4(2) . . . . ?
C9 C10 C11 C16 43.8(3) . . . . ?
C9 C8 C17 C22 51.5(3) . . . . ?
C9 C8 C17 C18 -124.2(2) . . . . ?

_shelx_SHELXL_version_number     2014/7
_olex2_exptl_crystal_mounting_method 
'mounted on a MiTeGen DualThickness Micro-Mount, coated in a layer of Paratone oil'
_olex2_submission_original_sample_id EOI8A
_olex2_submission_special_instructions 'No special instructions were received'
