# Electronic Supplementary Material (ESI) for Chemical Science.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_BARE_OXO_publ
_database_code_depnum_ccdc_archive 'CCDC 1582001'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-02-13T17:24|BARE_OXO||bt1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-02-13T17:24

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     36
_refine_ls_goodness_of_fit_all   1.03
_refine_ls_number_restraints     7
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?


_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from F:/Gas Storage Research/Jeff Long/Fe-BTT with Kenji/0p5 wt %/'
_cell_length_a                   18.6689(4)
_cell_length_b                   18.6689
_cell_length_c                   18.6689
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6506.6(4)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cr Cr1 0.1357(11) 0.5 0.0 1.0 Uiso 0.00605 12
C C1 0.14944(28) 0.3365(4) -0.14944(28) 1.0 Uiso 0.0094(10) 24
C C2 0.18167(26) 0.2737(4) -0.18167(26) 1.0 Uiso 0.0094(10) 24
C C3 0.24345(29) 0.24345(29) -0.1507(4) 1.0 Uiso 0.0094(10) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.032(5) 3
N N1 0.13112(19) 0.42339(20) -0.08009(19) 1.0 Uiso 0.0119(6) 48
N N2 0.17499(22) 0.36941(20) -0.09090(19) 1.0 Uiso 0.0119(6) 48
H H1 0.2675(5) 0.2675(5) -0.1062(7) 1.0 Uiso 0.016(4) 24
O Os 0.2330(23) 0.5 0.0 0.235(17) Uiso 0.00351 12

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C24 H8 Cl Cr4 N32 O0.94'
_chemical_formula_weight         1003.05
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cr1 Cl1 2.533(20) . 1_555 N
Cr1 N1 2.0708(33) . 1_555 N
Cr1 N1 2.0708(33) . 4_555 N
Cr1 N1 2.0708(33) . 12_565 N
Cr1 N1 2.0708(33) . -10_565 N
Cr1 Os 1.82(5) . 1_555 N
C1 C2 1.448(10) . 1_555 N
C1 N1 2.103(7) . 1_555 N
C1 N1 2.103(7) . 19_555 N
C1 N2 1.341(5) . 1_555 N
C1 N2 1.341(5) . 19_555 N
C2 C1 1.448(10) . 1_555 N
C2 C3 1.408(5) . 1_555 N
C2 C3 1.408(5) . 7_555 N
C3 C2 1.408(5) . 1_555 N
C3 C2 1.408(5) . 9_555 N
C3 H1 1.046(17) . 1_555 N
Cl1 Cr1 2.533(20) . 1_555 N
Cl1 Cr1 2.533(20) . 10_555 N
Cl1 Cr1 2.533(20) . 14_555 N
Cl1 Cr1 2.533(20) . 19_555 N
N1 Cr1 2.0708(33) . 1_555 N
N1 C1 2.103(7) . 1_555 N
N1 N1 1.347(8) . 19_555 N
N1 N2 1.314(5) . 1_555 N
N2 C1 1.341(5) . 1_555 N
N2 N1 1.314(5) . 1_555 N
H1 C3 1.046(17) . 1_555 N
Os Cr1 1.82(5) . 1_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Cr1 N1 87.7(6) 1_555 . 1_555 N
Cl1 Cr1 N1 87.7(6) 1_555 . 4_555 N
Cl1 Cr1 N1 87.7(6) 1_555 . 12_565 N
Cl1 Cr1 N1 87.7(6) 1_555 . -10_565 N
Cl1 Cr1 Os 180.0 1_555 . 1_555 N
N1 Cr1 N1 92.45(22) 1_555 . 4_555 N
N1 Cr1 N1 175.3(11) 1_555 . 12_565 N
N1 Cr1 N1 87.36(23) 1_555 . -10_565 N
N1 Cr1 Os 92.3(6) 1_555 . 1_555 N
N1 Cr1 N1 87.36(23) 4_555 . 12_565 N
N1 Cr1 N1 175.3(11) 4_555 . -10_565 N
N1 Cr1 Os 92.3(6) 4_555 . 1_555 N
N1 Cr1 N1 92.45(22) 12_565 . -10_565 N
N1 Cr1 Os 92.3(6) 12_565 . 1_555 N
N1 Cr1 Os 92.3(6) -10_565 . 1_555 N
C2 C1 N2 124.15(34) 1_555 . 1_555 N
C2 C1 N2 124.15(34) 1_555 . 19_555 N
N2 C1 N2 111.7(7) 1_555 . 19_555 N
C1 C2 C3 119.7(4) 1_555 . 1_555 N
C1 C2 C3 119.7(4) 1_555 . 7_555 N
C3 C2 C3 120.7(7) 1_555 . 7_555 N
C2 C3 C2 119.3(7) 1_555 . 9_555 N
C2 C3 H1 120.3(4) 1_555 . 1_555 N
C2 C3 H1 120.3(4) 9_555 . 1_555 N
Cr1 Cl1 Cr1 180.0 1_555 . 10_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 19_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 19_555 N
Cr1 Cl1 Cr1 180.0 14_555 . 19_555 N
Cr1 N1 N1 122.7(5) 1_555 . 19_555 N
Cr1 N1 N2 127.9(5) 1_555 . 1_555 N
N1 N1 N2 109.40(24) 19_555 . 1_555 N
C1 N2 N1 104.8(4) 1_555 . 1_555 N

# Powder diffraction data for histogram  4
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT602_BARE_OXO_publ       
;
PROBLEM: Test for (Unreported) solvent accessible voids        ! Info 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT049_BARE_OXO_publ       
;
PROBLEM: Calculated Density less than 1.0 gcm-3 .........     0.7680 Check 
RESPONSE: This is expected as the material is porous.
;




_cell_measurement_theta_min      3.5
_cell_measurement_theta_max      155

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Cr 12.0 0.3635 International_Tables_Vol_C
C 72.0 0.6646 International_Tables_Vol_C
Cl 3.0 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 24.0 -0.3739 International_Tables_Vol_C
O 2.824 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.078
_pd_proc_ls_prof_R_factor        0.0255
_pd_proc_ls_prof_wR_factor       0.0296
_pd_proc_ls_prof_wR_expected     0.0290
_refine_ls_R_Fsqd_factor         0.03682

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    1093.52     2:   -403.647     3:    269.341     4:   -109.609    
      5:    124.893     6:   -62.4409     7:    65.0456     8:   -33.7647    
      9:    36.8115    10:   -12.4660    11:    12.0154    12:   -2.86529    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  337.218 #2(GV)   = -174.464 #3(GW)   =   89.748
 #4(GP)   =   12.844 #5(LX)   =    1.214 #6(LY)   =   24.953
 #7(S/L)  =   0.0443 #8(H/L)  =   0.0341
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0005 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00050
_pd_proc_info_datetime           2016-02-13T17:24:48
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.5478
_pd_proc_2theta_range_max        166.2978
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
7730(190) 0.0 2717. .
7030(180) 0.0 2703. .
5810(160) 0.0 2689. .
5330(150) 0.0 2675. .
4720(150) 0.0 2661. .
4260(140) 0.0 2647. .
3810(130) 0.0 2633. .
3370(120) 0.0 2620. .
3030(120) 0.0 2607. .
2890(110) 0.0 2593. .
3030(120) 0.0 2580. .
2550(110) 0.0 2567. .
2560(110) 0.0 2554. .
2430(100) 0.0 2541. .
2380(100) 0.0 2529. .
2450(100) 0.0 2516. .
2280(100) 0.0 2504. .
2247(99) 0.0 2491. .
2280(100) 0.0 2479. .
2310(100) 0.0 2467. .
2280(100) 0.0 2455. .
2229(99) 0.0 2443. .
2175(98) 0.0 2431. .
2161(97) 0.0 2420. .
2490(110) 0.0 2408. .
2480(100) 0.0 2397. .
2500(110) 0.0 2385. .
2430(100) 0.0 2374. .
2610(110) 0.0 2363. .
2320(100) 0.0 2352. .
2570(110) 0.0 2341. .
2310(100) 0.0 2330. .
2570(110) 0.0 2319. .
2620(110) 0.0 2308. .
2215(98) 0.0 2298. .
2450(100) 0.0 2287. .
2134(97) 0.0 2277. .
2330(100) 0.0 2267. .
2152(97) 0.0 2256. .
2188(98) 0.0 2246. .
2380(100) 0.0 2236. .
2175(98) 0.0001041 2226. 2232.
2252(99) 0.0001020 2217. 2222.
2188(98) 0.0001041 2207. 2213.
2166(97) 0.0001063 2197. 2204.
2129(96) 0.0001085 2188. 2194.
2166(97) 0.0001063 2178. 2185.
2066(95) 0.0001108 2169. 2176.
2184(98) 0.0001041 2160. 2168.
2030(94) 0.0001132 2150. 2159.
2229(99) 0.0001020 2141. 2150.
2350(100) 0.0000961 2132. 2142.
2070(95) 0.0001108 2123. 2134.
2129(96) 0.0001085 2114. 2125.
2243(99) 0.0001020 2106. 2118.
2107(96) 0.0001085 2097. 2110.
2116(96) 0.0001085 2088. 2104.
2310(100) 0.0000980 2080. 2099.
2129(96) 0.0001085 2071. 2099.
2360(100) 0.0000961 2063. 2104.
2152(97) 0.0001063 2055. 2117.
2129(96) 0.0001085 2046. 2137.
2270(100) 0.0001000 2038. 2166.
2270(100) 0.0001000 2030. 2199.
2420(100) 0.0000943 2022. 2237.
2360(100) 0.0000961 2014. 2278.
2270(100) 0.0001000 2007. 2322.
2400(100) 0.0000943 1999. 2369.
2570(110) 0.0000890 1991. 2420.
2570(110) 0.0000890 1983. 2474.
2720(110) 0.0000842 1976. 2531.
2610(110) 0.0000873 1968. 2593.
2600(110) 0.0000873 1961. 2660.
2640(110) 0.0000857 1954. 2732.
2590(110) 0.0000873 1946. 2809.
2830(110) 0.0000797 1939. 2892.
2900(110) 0.0000783 1932. 2983.
3000(120) 0.0000756 1925. 3082.
3030(120) 0.0000743 1918. 3189.
3370(120) 0.0000672 1911. 3307.
3290(120) 0.0000683 1904. 3436.
3470(120) 0.0000650 1898. 3580.
3790(130) 0.0000592 1891. 3740.
3910(130) 0.0000574 1884. 3919.
3990(130) 0.0000565 1878. 4121.
4410(140) 0.0000510 1871. 4352.
4610(140) 0.0000489 1865. 4620.
4720(150) 0.0000476 1858. 4934.
5150(150) 0.0000433 1852. 5314.
5720(160) 0.0000391 1846. 5782.
6630(170) 0.0000338 1839. 6388.
7840(190) 0.0000283 1833. 7209.
9220(200) 0.0000240 1827. 8333.
10310(220) 0.0000216 1821. 9769.
12740(240) 0.0000174 1815. 11274.
13220(240) 0.0000168 1809. 12259.
12540(240) 0.0000177 1803. 12014.
11380(230) 0.0000196 1798. 10278.
8630(200) 0.0000258 1792. 7660.
5900(160) 0.0000381 1786. 5171.
3672(88) 0.0001291 1781. 3434.
2649(74) 0.0001826 1775. 2496.
2053(65) 0.0002367 1769. 2090.
1791(60) 0.0002778 1764. 1937.
1729(59) 0.0002873 1759. 1879.
1834(61) 0.0002687 1753. 1849.
1795(60) 0.0002778 1748. 1828.
1852(61) 0.0002687 1743. 1812.
1791(60) 0.0002778 1737. 1798.
1813(61) 0.0002687 1732. 1787.
1692(59) 0.0002873 1727. 1776.
1693(59) 0.0002873 1722. 1767.
1624(57) 0.0003078 1717. 1758.
1666(58) 0.0002973 1712. 1751.
1644(58) 0.0002973 1707. 1743.
1669(58) 0.0002973 1702. 1737.
1654(58) 0.0002973 1698. 1731.
1742(59) 0.0002873 1693. 1725.
1679(58) 0.0002973 1688. 1720.
1687(58) 0.0002973 1684. 1715.
1614(57) 0.0003078 1679. 1710.
1694(59) 0.0002873 1674. 1707.
1745(60) 0.0002778 1670. 1704.
1758(60) 0.0002778 1665. 1704.
1713(59) 0.0002873 1661. 1709.
1748(60) 0.0002778 1657. 1722.
1773(60) 0.0002778 1652. 1745.
1795(60) 0.0002778 1648. 1781.
1898(62) 0.0002601 1644. 1830.
1862(62) 0.0002601 1639. 1893.
1893(62) 0.0002601 1635. 1960.
1990(64) 0.0002441 1631. 2035.
2083(65) 0.0002367 1627. 2117.
2202(67) 0.0002228 1623. 2208.
2220(68) 0.0002163 1619. 2309.
2384(70) 0.0002041 1615. 2421.
2434(71) 0.0001984 1611. 2547.
2552(73) 0.0001877 1607. 2688.
2712(75) 0.0001778 1603. 2850.
3003(79) 0.0001602 1600. 3038.
3196(82) 0.0001487 1596. 3257.
3425(85) 0.0001384 1592. 3516.
3704(88) 0.0001291 1588. 3842.
4027(92) 0.0001181 1585. 4265.
4760(100) 0.0001000 1581. 4836.
5510(110) 0.0000857 1578. 5617.
6610(120) 0.0000706 1574. 6615.
7750(130) 0.0000601 1571. 7665.
8260(130) 0.0000565 1567. 8366.
8120(130) 0.0000574 1564. 8233.
7030(120) 0.0000672 1560. 7091.
5680(110) 0.0000826 1557. 5371.
3668(88) 0.0001291 1554. 3752.
2592(73) 0.0001877 1550. 2636.
2011(64) 0.0002441 1547. 2039.
1678(58) 0.0002973 1544. 1781.
1568(56) 0.0003189 1541. 1683.
1480(55) 0.0003306 1537. 1644.
1542(56) 0.0003189 1534. 1624.
1530(55) 0.0003306 1531. 1611.
1511(55) 0.0003306 1528. 1601.
1620(57) 0.0003078 1525. 1593.
1646(58) 0.0002973 1522. 1587.
1694(59) 0.0002873 1519. 1582.
1596(57) 0.0003078 1516. 1579.
1625(57) 0.0003078 1513. 1577.
1649(58) 0.0002973 1510. 1576.
1740(59) 0.0002873 1508. 1578.
1795(60) 0.0002778 1505. 1584.
1873(62) 0.0002601 1502. 1599.
1901(62) 0.0002601 1499. 1631.
1947(63) 0.0002520 1496. 1689.
1897(62) 0.0002601 1494. 1782.
2018(64) 0.0002441 1491. 1912.
2266(68) 0.0002163 1488. 2077.
2450(71) 0.0001984 1486. 2275.
2502(72) 0.0001929 1483. 2502.
2684(75) 0.0001778 1481. 2759.
2984(79) 0.0001602 1478. 3052.
3347(84) 0.0001417 1476. 3386.
3658(88) 0.0001291 1473. 3774.
3970(91) 0.0001208 1471. 4231.
4359(96) 0.0001085 1468. 4782.
5170(110) 0.0000907 1466. 5471.
6110(110) 0.0000769 1463. 6371.
7560(130) 0.0000620 1461. 7596.
9430(140) 0.0000496 1459. 9252.
11240(160) 0.0000416 1456. 11286.
13300(170) 0.0000350 1454. 13253.
14070(170) 0.0000330 1452. 14285.
13410(170) 0.0000346 1450. 13525.
10880(150) 0.0000427 1447. 10949.
7640(130) 0.0000610 1445. 7654.
4990(100) 0.0000961 1443. 4853.
3002(79) 0.0001602 1441. 3069.
2101(66) 0.0002296 1439. 2176.
1644(79) 0.0001602 1437. 1806.
1449(74) 0.0001826 1434. 1665.
1389(72) 0.0001929 1432. 1604.
1486(75) 0.0001778 1430. 1569.
1512(55) 0.0003306 1428. 1545.
1515(55) 0.0003306 1426. 1526.
1530(55) 0.0003306 1424. 1510.
1506(55) 0.0003306 1422. 1497.
1470(54) 0.0003429 1420. 1487.
1555(56) 0.0003189 1418. 1478.
1455(54) 0.0003429 1417. 1470.
1479(54) 0.0003429 1415. 1464.
1514(55) 0.0003306 1413. 1458.
1404(53) 0.000356 1411. 1454.
1406(53) 0.000356 1409. 1452.
1483(54) 0.0003429 1407. 1450.
1355(52) 0.000370 1406. 1450.
1469(54) 0.0003429 1404. 1451.
1490(55) 0.0003306 1402. 1452.
1423(53) 0.000356 1400. 1455.
1464(54) 0.0003429 1399. 1460.
1427(53) 0.000356 1397. 1466.
1526(55) 0.0003306 1395. 1475.
1466(54) 0.0003429 1394. 1488.
1553(56) 0.0003189 1392. 1508.
1592(57) 0.0003078 1390. 1534.
1630(57) 0.0003078 1389. 1562.
1641(57) 0.0003078 1387. 1582.
1611(57) 0.0003078 1385. 1580.
1564(56) 0.0003189 1384. 1550.
1521(55) 0.0003306 1382. 1502.
1508(55) 0.0003306 1381. 1455.
1459(54) 0.0003429 1379. 1422.
1394(53) 0.000356 1378. 1403.
1370(52) 0.000370 1376. 1394.
1366(52) 0.000370 1375. 1389.
1432(53) 0.000356 1373. 1386.
1466(54) 0.0003429 1372. 1383.
1456(54) 0.0003429 1370. 1381.
1438(53) 0.000356 1369. 1379.
1408(53) 0.000356 1368. 1377.
1425(53) 0.000356 1366. 1375.
1416(53) 0.000356 1365. 1373.
1473(54) 0.0003429 1363. 1372.
1467(54) 0.0003429 1362. 1370.
1310(51) 0.000384 1361. 1368.
1459(54) 0.0003429 1359. 1367.
1278(50) 0.000400 1358. 1365.
1285(50) 0.000400 1357. 1364.
1390(52) 0.000370 1356. 1362.
1387(52) 0.000370 1354. 1361.
1432(53) 0.000356 1353. 1359.
1398(53) 0.000356 1352. 1358.
1321(51) 0.000384 1351. 1356.
1316(51) 0.000384 1349. 1355.
1346(52) 0.000370 1348. 1354.
1437(53) 0.000356 1347. 1353.
1360(52) 0.000370 1346. 1351.
1375(52) 0.000370 1344. 1350.
1386(52) 0.000370 1343. 1349.
1376(52) 0.000370 1342. 1347.
1333(51) 0.000384 1341. 1346.
1363(52) 0.000370 1340. 1344.
1293(50) 0.000400 1339. 1343.
1391(53) 0.000356 1338. 1342.
1435(53) 0.000356 1337. 1341.
1315(51) 0.000384 1335. 1340.
1301(51) 0.000384 1334. 1338.
1285(50) 0.000400 1333. 1337.
1299(51) 0.000384 1332. 1336.
1334(51) 0.000384 1331. 1335.
1328(51) 0.000384 1330. 1334.
1292(50) 0.000400 1329. 1334.
1277(50) 0.000400 1328. 1333.
1272(50) 0.000400 1327. 1334.
1283(50) 0.000400 1326. 1334.
1258(50) 0.000400 1325. 1335.
1386(52) 0.000370 1324. 1337.
1402(53) 0.000356 1323. 1339.
1295(50) 0.000400 1322. 1342.
1381(52) 0.000370 1321. 1346.
1399(53) 0.000356 1320. 1352.
1386(52) 0.000370 1319. 1361.
1390(52) 0.000370 1318. 1371.
1440(54) 0.0003429 1317. 1383.
1451(54) 0.0003429 1316. 1390.
1439(54) 0.0003429 1315. 1387.
1410(53) 0.000356 1315. 1374.
1371(52) 0.000370 1314. 1355.
1352(52) 0.000370 1313. 1338.
1359(52) 0.000370 1312. 1326.
1379(52) 0.000370 1311. 1320.
1389(52) 0.000370 1310. 1317.
1386(52) 0.000370 1309. 1315.
1358(52) 0.000370 1308. 1314.
1424(53) 0.000356 1308. 1313.
1278(50) 0.000400 1307. 1313.
1303(51) 0.000384 1306. 1312.
1386(52) 0.000370 1305. 1312.
1393(53) 0.000356 1304. 1311.
1432(78) 0.0001644 1303. 1310.
1341(51) 0.000384 1303. 1310.
1283(50) 0.000400 1302. 1309.
1359(51) 0.000384 1301. 1308.
1367(51) 0.000384 1300. 1308.
1276(49) 0.000416 1299. 1307.
1329(51) 0.000384 1299. 1307.
1332(51) 0.000384 1298. 1307.
1347(51) 0.000384 1297. 1306.
1345(51) 0.000384 1296. 1306.
1272(49) 0.000416 1296. 1306.
1265(49) 0.000416 1295. 1306.
1314(50) 0.000400 1294. 1306.
1380(52) 0.000370 1293. 1306.
1363(51) 0.000384 1293. 1306.
1339(51) 0.000384 1292. 1306.
1356(51) 0.000384 1291. 1307.
1357(51) 0.000384 1290. 1308.
1378(52) 0.000370 1290. 1309.
1264(49) 0.000416 1289. 1310.
1332(51) 0.000384 1288. 1313.
1376(52) 0.000370 1288. 1318.
1326(51) 0.000384 1287. 1326.
1340(51) 0.000384 1286. 1342.
1394(52) 0.000370 1285. 1370.
1445(53) 0.000356 1285. 1414.
1542(55) 0.0003306 1284. 1477.
1599(56) 0.0003189 1283. 1562.
1689(57) 0.0003078 1283. 1674.
1839(60) 0.0002778 1282. 1823.
2043(64) 0.0002441 1281. 2026.
2260(67) 0.0002228 1281. 2299.
2711(74) 0.0001826 1280. 2636.
3066(79) 0.0001602 1279. 2972.
3148(80) 0.0001562 1279. 3175.
3175(80) 0.0001562 1278. 3103.
2687(73) 0.0001877 1278. 2741.
2163(65) 0.0002367 1277. 2259.
1678(57) 0.0003078 1276. 1842.
1588(56) 0.0003189 1276. 1572.
1352(51) 0.000384 1275. 1435.
1297(50) 0.000400 1274. 1378.
1343(51) 0.000384 1274. 1358.
1317(50) 0.000400 1273. 1353.
1376(52) 0.000370 1273. 1359.
1406(52) 0.000370 1272. 1376.
1389(52) 0.000370 1271. 1413.
1445(53) 0.000356 1271. 1478.
1519(54) 0.0003429 1270. 1584.
1782(59) 0.0002873 1269. 1736.
1950(62) 0.0002601 1269. 1946.
2127(65) 0.0002367 1268. 2231.
2469(70) 0.0002041 1268. 2621.
3095(79) 0.0001602 1267. 3149.
3795(88) 0.0001291 1267. 3815.
4463(95) 0.0001108 1266. 4510.
4857(99) 0.0001020 1265. 4989.
4764(98) 0.0001041 1265. 4958.
4010(90) 0.0001235 1264. 4321.
3074(79) 0.0001602 1264. 3365.
2344(68) 0.0002163 1263. 2490.
1700(58) 0.0002973 1263. 1895.
1563(55) 0.0003306 1262. 1575.
1233(49) 0.000416 1261. 1432.
1236(49) 0.000416 1261. 1372.
1176(47) 0.000453 1260. 1346.
1225(48) 0.000434 1260. 1331.
1202(48) 0.000434 1259. 1321.
1316(50) 0.000400 1259. 1314.
1191(48) 0.000434 1258. 1309.
1253(49) 0.000416 1258. 1307.
1320(50) 0.000400 1257. 1306.
1296(50) 0.000400 1256. 1308.
1276(49) 0.000416 1256. 1313.
1297(50) 0.000400 1255. 1320.
1342(51) 0.000384 1255. 1330.
1310(50) 0.000400 1254. 1342.
1282(50) 0.000400 1254. 1350.
1341(51) 0.000384 1253. 1349.
1263(49) 0.000416 1253. 1339.
1251(49) 0.000416 1252. 1323.
1283(50) 0.000400 1252. 1310.
1274(49) 0.000416 1251. 1302.
1251(49) 0.000416 1251. 1299.
1274(49) 0.000416 1250. 1301.
1274(49) 0.000416 1250. 1308.
1300(50) 0.000400 1249. 1320.
1432(53) 0.000356 1249. 1344.
1401(52) 0.000370 1248. 1388.
1529(55) 0.0003306 1248. 1464.
1744(58) 0.0002973 1247. 1587.
1862(61) 0.0002687 1247. 1770.
2076(64) 0.0002441 1246. 2031.
2486(70) 0.0002041 1245. 2397.
3098(79) 0.0001602 1245. 2899.
3755(87) 0.0001321 1244. 3532.
4215(92) 0.0001181 1244. 4199.
4718(98) 0.0001041 1243. 4674.
4498(96) 0.0001085 1243. 4678.
3972(90) 0.0001235 1242. 4112.
3225(76) 0.0001731 1242. 3234.
2352(65) 0.0002367 1241. 2418.
1765(56) 0.0003189 1241. 1856.
1564(52) 0.000370 1240. 1550.
1342(48) 0.000434 1240. 1410.
1316(48) 0.000434 1239. 1351.
1284(47) 0.000453 1239. 1326.
1291(47) 0.000453 1239. 1314.
1334(48) 0.000434 1238. 1309.
1335(48) 0.000434 1238. 1312.
1360(49) 0.000416 1237. 1323.
1374(49) 0.000416 1237. 1344.
1398(49) 0.000416 1236. 1376.
1460(50) 0.000400 1236. 1424.
1471(51) 0.000384 1235. 1487.
1617(53) 0.000356 1235. 1557.
1677(54) 0.0003429 1234. 1611.
1701(55) 0.0003306 1234. 1620.
1632(54) 0.0003429 1233. 1568.
1516(51) 0.000384 1233. 1476.
1358(49) 0.000416 1232. 1385.
1304(47) 0.000453 1232. 1320.
1343(48) 0.000434 1231. 1282.
1221(46) 0.000473 1231. 1264.
1324(48) 0.000434 1230. 1256.
1324(48) 0.000434 1230. 1253.
1299(47) 0.000453 1229. 1251.
1272(47) 0.000453 1229. 1251.
1223(46) 0.000473 1228. 1253.
1246(46) 0.000473 1228. 1258.
1215(46) 0.000473 1227. 1266.
1235(46) 0.000473 1227. 1278.
1326(48) 0.000434 1226. 1294.
1338(48) 0.000434 1226. 1313.
1344(48) 0.000434 1225. 1332.
1386(49) 0.000416 1225. 1341.
1424(50) 0.000400 1224. 1333.
1334(48) 0.000434 1224. 1310.
1282(47) 0.000453 1224. 1283.
1240(46) 0.000473 1223. 1261.
1251(46) 0.000473 1223. 1247.
1262(47) 0.000453 1222. 1239.
1254(46) 0.000473 1222. 1236.
1248(46) 0.000473 1221. 1235.
1290(47) 0.000453 1221. 1234.
1237(46) 0.000473 1220. 1234.
1239(46) 0.000473 1220. 1235.
1272(47) 0.000453 1219. 1237.
1252(46) 0.000473 1219. 1240.
1196(45) 0.000494 1218. 1245.
1230(46) 0.000473 1218. 1252.
1246(46) 0.000473 1217. 1259.
1250(46) 0.000473 1217. 1266.
1271(47) 0.000453 1216. 1268.
1250(46) 0.000473 1216. 1263.
1267(47) 0.000453 1216. 1254.
1198(45) 0.000494 1215. 1244.
1278(47) 0.000453 1215. 1237.
1241(46) 0.000473 1214. 1233.
1260(47) 0.000453 1214. 1231.
1237(46) 0.000473 1213. 1230.
1351(48) 0.000434 1213. 1230.
1231(46) 0.000473 1212. 1230.
1255(46) 0.000473 1212. 1230.
1267(47) 0.000453 1211. 1231.
1289(47) 0.000453 1211. 1233.
1263(47) 0.000453 1210. 1234.
1257(47) 0.000453 1210. 1235.
1236(46) 0.000473 1209. 1237.
1180(45) 0.000494 1209. 1239.
1209(46) 0.000473 1208. 1241.
1231(46) 0.000473 1208. 1244.
1277(47) 0.000453 1208. 1248.
1280(47) 0.000453 1207. 1253.
1305(47) 0.000453 1207. 1260.
1340(48) 0.000434 1206. 1269.
1326(48) 0.000434 1206. 1283.
1349(48) 0.000434 1205. 1306.
1359(49) 0.000416 1205. 1350.
1412(50) 0.000400 1204. 1428.
1594(53) 0.000356 1204. 1566.
1719(55) 0.0003306 1203. 1791.
2069(61) 0.0002687 1203. 2136.
2604(68) 0.0002163 1202. 2632.
3258(77) 0.0001687 1202. 3269.
4029(86) 0.0001352 1201. 3949.
4597(92) 0.0001181 1201. 4456.
4581(91) 0.0001208 1201. 4518.
4022(86) 0.0001352 1200. 4021.
3361(78) 0.0001644 1200. 3204.
2428(66) 0.0002296 1199. 2424.
1806(56) 0.0003189 1199. 1875.
1502(51) 0.000384 1198. 1567.
1381(49) 0.000416 1198. 1428.
1314(48) 0.000434 1197. 1379.
1379(49) 0.000416 1197. 1381.
1346(48) 0.000434 1196. 1420.
1525(52) 0.000370 1196. 1504.
1616(53) 0.000356 1195. 1647.
1833(57) 0.0003078 1195. 1862.
2176(62) 0.0002601 1194. 2147.
2471(66) 0.0002296 1194. 2463.
2711(70) 0.0002041 1194. 2713.
2803(71) 0.0001984 1193. 2772.
2577(68) 0.0002163 1193. 2570.
2177(62) 0.0002601 1192. 2200.
1834(57) 0.0003078 1192. 1832.
1514(51) 0.000384 1191. 1564.
1437(50) 0.000400 1191. 1411.
1318(48) 0.000434 1190. 1343.
1304(48) 0.000434 1190. 1327.
1249(46) 0.000473 1189. 1345.
1407(49) 0.000416 1189. 1397.
1454(50) 0.000400 1188. 1494.
1597(53) 0.000356 1188. 1652.
1821(57) 0.0003078 1187. 1881.
2116(61) 0.0002687 1187. 2170.
2448(66) 0.0002296 1187. 2466.
2754(70) 0.0002041 1186. 2663.
2750(70) 0.0002041 1186. 2645.
2505(67) 0.0002228 1185. 2390.
2109(61) 0.0002687 1185. 2028.
1734(55) 0.0003306 1184. 1705.
1513(51) 0.000384 1184. 1489.
1388(49) 0.000416 1183. 1376.
1320(48) 0.000434 1183. 1336.
1296(47) 0.000453 1182. 1344.
1410(50) 0.000400 1182. 1394.
1506(51) 0.000384 1181. 1497.
1714(55) 0.0003306 1181. 1671.
1957(59) 0.0002873 1180. 1935.
2255(63) 0.0002520 1180. 2286.
2741(70) 0.0002041 1180. 2671.
3064(74) 0.0001826 1179. 2973.
3169(76) 0.0001731 1179. 3038.
2903(72) 0.0001929 1178. 2790.
2415(66) 0.0002296 1178. 2345.
1970(59) 0.0002873 1177. 1905.
1606(53) 0.000356 1177. 1584.
1371(49) 0.000416 1176. 1396.
1226(46) 0.000473 1176. 1303.
1227(46) 0.000473 1175. 1262.
1257(47) 0.000453 1175. 1244.
1200(45) 0.000494 1174. 1237.
1175(45) 0.000494 1174. 1237.
1190(45) 0.000494 1173. 1242.
1190(45) 0.000494 1173. 1253.
1317(48) 0.000434 1173. 1265.
1310(48) 0.000434 1172. 1274.
1303(48) 0.000434 1172. 1272.
1280(47) 0.000453 1171. 1258.
1235(46) 0.000473 1171. 1237.
1251(46) 0.000473 1170. 1217.
1160(45) 0.000494 1170. 1202.
1189(45) 0.000494 1169. 1193.
1180(45) 0.000494 1169. 1188.
1199(45) 0.000494 1168. 1185.
1203(46) 0.000473 1168. 1183.
1223(46) 0.000473 1167. 1182.
1143(44) 0.000517 1167. 1181.
1205(46) 0.000473 1166. 1180.
1154(45) 0.000494 1166. 1179.
1137(44) 0.000517 1166. 1178.
1181(45) 0.000494 1165. 1177.
1123(44) 0.000517 1165. 1177.
1125(44) 0.000517 1164. 1176.
1147(44) 0.000517 1164. 1175.
1155(45) 0.000494 1163. 1175.
1209(46) 0.000473 1163. 1175.
1131(44) 0.000517 1162. 1176.
1195(45) 0.000494 1162. 1179.
1202(45) 0.000494 1161. 1184.
1220(46) 0.000473 1161. 1193.
1260(47) 0.000453 1160. 1209.
1245(46) 0.000473 1160. 1233.
1238(46) 0.000473 1160. 1263.
1283(47) 0.000453 1159. 1294.
1375(49) 0.000416 1159. 1315.
1310(48) 0.000434 1158. 1313.
1242(46) 0.000473 1158. 1286.
1245(46) 0.000473 1157. 1248.
1212(46) 0.000473 1157. 1214.
1177(45) 0.000494 1156. 1190.
1162(45) 0.000494 1156. 1177.
1150(44) 0.000517 1155. 1170.
1160(45) 0.000494 1155. 1167.
1181(45) 0.000494 1154. 1165.
1186(45) 0.000494 1154. 1163.
1164(45) 0.000494 1154. 1162.
1191(45) 0.000494 1153. 1162.
1130(44) 0.000517 1153. 1161.
1122(44) 0.000517 1152. 1160.
1203(46) 0.000473 1152. 1160.
1219(46) 0.000473 1151. 1159.
1211(46) 0.000473 1151. 1159.
1172(45) 0.000494 1150. 1158.
1210(46) 0.000473 1150. 1158.
1141(44) 0.000517 1149. 1158.
1094(43) 0.000541 1149. 1158.
1127(44) 0.000517 1148. 1158.
1229(44) 0.000517 1148. 1159.
1187(44) 0.000517 1148. 1160.
1183(44) 0.000517 1147. 1162.
1142(43) 0.000541 1147. 1165.
1165(43) 0.000541 1146. 1167.
1156(43) 0.000541 1146. 1168.
1179(44) 0.000517 1145. 1167.
1193(44) 0.000517 1145. 1165.
1167(43) 0.000541 1144. 1163.
1177(43) 0.000541 1144. 1162.
1179(44) 0.000517 1143. 1162.
1178(44) 0.000517 1143. 1165.
1246(45) 0.000494 1143. 1172.
1280(46) 0.000473 1142. 1184.
1285(46) 0.000473 1142. 1206.
1280(45) 0.000494 1141. 1238.
1277(45) 0.000494 1141. 1279.
1334(47) 0.000453 1140. 1322.
1347(47) 0.000453 1140. 1351.
1406(48) 0.000434 1139. 1351.
1364(47) 0.000453 1139. 1320.
1262(45) 0.000494 1138. 1275.
1203(44) 0.000517 1138. 1236.
1207(44) 0.000517 1138. 1213.
1188(44) 0.000517 1137. 1208.
1197(44) 0.000517 1137. 1223.
1295(46) 0.000473 1136. 1263.
1358(47) 0.000453 1136. 1337.
1405(48) 0.000434 1135. 1454.
1585(51) 0.000384 1135. 1610.
1727(53) 0.000356 1134. 1778.
1762(54) 0.0003429 1134. 1904.
1849(55) 0.0003306 1134. 1925.
1777(54) 0.0003429 1133. 1817.
1566(51) 0.000384 1133. 1638.
1474(49) 0.000416 1132. 1468.
1318(46) 0.000473 1132. 1351.
1224(44) 0.000517 1131. 1296.
1211(44) 0.000517 1131. 1296.
1328(46) 0.000473 1130. 1352.
1428(48) 0.000434 1130. 1471.
1701(53) 0.000356 1130. 1663.
1994(58) 0.0002973 1129. 1921.
2245(61) 0.0002687 1129. 2196.
2441(64) 0.0002441 1128. 2394.
2430(64) 0.0002441 1128. 2412.
2244(61) 0.0002687 1127. 2216.
1935(57) 0.0003078 1127. 1909.
1551(50) 0.000400 1126. 1618.
1390(48) 0.000434 1126. 1410.
1268(45) 0.000494 1126. 1286.
1193(44) 0.000517 1125. 1224.
1168(43) 0.000541 1125. 1194.
1147(43) 0.000541 1124. 1179.
1149(43) 0.000541 1124. 1171.
1155(43) 0.000541 1123. 1165.
1155(43) 0.000541 1123. 1161.
1113(42) 0.000567 1123. 1159.
1127(42) 0.000567 1122. 1157.
1096(42) 0.000567 1122. 1157.
1131(43) 0.000541 1121. 1158.
1125(42) 0.000567 1121. 1161.
1180(44) 0.000517 1120. 1167.
1185(44) 0.000517 1120. 1181.
1182(44) 0.000517 1120. 1209.
1193(44) 0.000517 1119. 1260.
1320(46) 0.000473 1119. 1341.
1490(49) 0.000416 1118. 1453.
1619(52) 0.000370 1118. 1579.
1725(53) 0.000356 1117. 1681.
1733(53) 0.000356 1117. 1711.
1694(53) 0.000356 1117. 1644.
1581(51) 0.000384 1116. 1514.
1411(48) 0.000434 1116. 1381.
1321(46) 0.000473 1115. 1283.
1215(44) 0.000517 1115. 1227.
1154(43) 0.000541 1114. 1208.
1206(44) 0.000517 1114. 1218.
1237(45) 0.000494 1114. 1253.
1307(46) 0.000473 1113. 1312.
1379(47) 0.000453 1113. 1386.
1432(48) 0.000434 1112. 1455.
1439(48) 0.000434 1112. 1489.
1381(47) 0.000453 1111. 1466.
1336(47) 0.000453 1111. 1394.
1262(45) 0.000494 1111. 1308.
1202(44) 0.000517 1110. 1238.
1145(43) 0.000541 1110. 1192.
1157(43) 0.000541 1109. 1166.
1158(43) 0.000541 1109. 1154.
1155(43) 0.000541 1109. 1149.
1139(43) 0.000541 1108. 1148.
1141(43) 0.000541 1108. 1148.
1122(42) 0.000567 1107. 1150.
1132(43) 0.000541 1107. 1153.
1124(42) 0.000567 1106. 1157.
1102(42) 0.000567 1106. 1164.
1161(43) 0.000541 1106. 1174.
1250(45) 0.000494 1105. 1192.
1193(44) 0.000517 1105. 1226.
1271(36) 0.000772 1104. 1292.
1486(45) 0.000494 1104. 1413.
1679(48) 0.000434 1104. 1620.
2044(54) 0.0003429 1103. 1927.
2456(59) 0.0002873 1103. 2309.
2885(64) 0.0002441 1102. 2677.
2981(65) 0.0002367 1102. 2888.
2829(64) 0.0002441 1102. 2815.
2432(59) 0.0002873 1101. 2480.
2052(54) 0.0003429 1101. 2057.
1696(49) 0.000416 1100. 1694.
1463(45) 0.000494 1100. 1449.
1291(42) 0.000567 1100. 1315.
1274(42) 0.000567 1099. 1258.
1273(42) 0.000567 1099. 1247.
1224(41) 0.000595 1098. 1264.
1260(42) 0.000567 1098. 1295.
1354(43) 0.000541 1098. 1326.
1330(43) 0.000541 1097. 1339.
1360(43) 0.000541 1097. 1323.
1283(42) 0.000567 1096. 1284.
1190(40) 0.000625 1096. 1242.
1164(40) 0.000625 1096. 1213.
1215(41) 0.000595 1095. 1206.
1211(41) 0.000595 1095. 1227.
1276(42) 0.000567 1094. 1283.
1425(44) 0.000517 1094. 1380.
1552(47) 0.000453 1094. 1513.
1635(48) 0.000434 1093. 1657.
1798(50) 0.000400 1093. 1767.
1805(50) 0.000400 1092. 1786.
1689(49) 0.000416 1092. 1695.
1501(46) 0.000473 1092. 1543.
1332(43) 0.000541 1091. 1398.
1289(42) 0.000567 1091. 1295.
1215(41) 0.000595 1091. 1246.
1204(41) 0.000595 1090. 1247.
1304(42) 0.000567 1090. 1292.
1293(42) 0.000567 1089. 1376.
1522(46) 0.000473 1089. 1484.
1617(48) 0.000434 1089. 1586.
1631(48) 0.000434 1088. 1639.
1621(48) 0.000434 1088. 1606.
1475(45) 0.000494 1087. 1501.
1405(44) 0.000517 1087. 1374.
1306(42) 0.000567 1087. 1268.
1209(41) 0.000595 1086. 1196.
1202(41) 0.000595 1086. 1154.
1142(40) 0.000625 1086. 1134.
1129(39) 0.000657 1085. 1124.
1146(40) 0.000625 1085. 1121.
1117(39) 0.000657 1084. 1119.
1152(40) 0.000625 1084. 1118.
1123(39) 0.000657 1084. 1115.
1099(39) 0.000657 1083. 1111.
1120(39) 0.000657 1083. 1107.
1144(40) 0.000625 1083. 1103.
1116(39) 0.000657 1082. 1100.
1123(39) 0.000657 1082. 1098.
1111(39) 0.000657 1081. 1097.
1049(38) 0.000693 1081. 1096.
1071(38) 0.000693 1081. 1096.
1096(39) 0.000657 1080. 1097.
1127(39) 0.000657 1080. 1097.
1098(39) 0.000657 1080. 1097.
1085(38) 0.000693 1079. 1097.
1137(39) 0.000657 1079. 1097.
1149(40) 0.000625 1079. 1098.
1152(40) 0.000625 1078. 1102.
1135(39) 0.000657 1078. 1111.
1099(39) 0.000657 1077. 1127.
1175(40) 0.000625 1077. 1153.
1263(42) 0.000567 1077. 1190.
1319(43) 0.000541 1076. 1232.
1290(42) 0.000567 1076. 1266.
1310(43) 0.000541 1076. 1276.
1299(42) 0.000567 1075. 1254.
1168(40) 0.000625 1075. 1212.
1135(39) 0.000657 1075. 1169.
1169(40) 0.000625 1074. 1134.
1192(40) 0.000625 1074. 1112.
1153(40) 0.000625 1074. 1099.
1138(39) 0.000657 1073. 1093.
1127(39) 0.000657 1073. 1090.
1124(39) 0.000657 1072. 1088.
1151(40) 0.000625 1072. 1087.
1113(39) 0.000657 1072. 1086.
1156(40) 0.000625 1071. 1086.
1095(39) 0.000657 1071. 1086.
1083(38) 0.000693 1071. 1087.
1121(39) 0.000657 1070. 1088.
1095(39) 0.000657 1070. 1091.
1121(39) 0.000657 1070. 1096.
1121(39) 0.000657 1069. 1103.
1143(40) 0.000625 1069. 1114.
1164(40) 0.000625 1069. 1125.
1114(39) 0.000657 1068. 1134.
1152(40) 0.000625 1068. 1138.
1122(39) 0.000657 1068. 1136.
1141(39) 0.000657 1067. 1133.
1170(38) 0.000693 1067. 1136.
1188(38) 0.000693 1067. 1152.
1249(39) 0.000657 1066. 1191.
1267(40) 0.000625 1066. 1264.
1424(42) 0.000567 1066. 1376.
1537(44) 0.000517 1065. 1518.
1653(46) 0.000473 1065. 1660.
1717(47) 0.000453 1065. 1748.
1760(47) 0.000453 1064. 1734.
1581(45) 0.000494 1064. 1621.
1435(42) 0.000567 1064. 1469.
1322(41) 0.000595 1063. 1335.
1219(39) 0.000657 1063. 1245.
1176(38) 0.000693 1063. 1204.
1145(38) 0.000693 1062. 1204.
1249(39) 0.000657 1062. 1234.
1298(40) 0.000625 1062. 1279.
1350(41) 0.000595 1061. 1321.
1352(41) 0.000595 1061. 1337.
1377(41) 0.000595 1061. 1313.
1262(40) 0.000625 1060. 1259.
1213(39) 0.000657 1060. 1201.
1128(37) 0.000730 1060. 1153.
1100(37) 0.000730 1059. 1120.
1066(36) 0.000772 1059. 1101.
1080(36) 0.000772 1059. 1091.
1065(36) 0.000772 1058. 1086.
1078(36) 0.000772 1058. 1084.
1066(36) 0.000772 1058. 1083.
1060(36) 0.000772 1057. 1082.
1101(37) 0.000730 1057. 1082.
1092(37) 0.000730 1057. 1082.
1112(37) 0.000730 1057. 1085.
1154(38) 0.000693 1056. 1091.
1138(37) 0.000730 1056. 1103.
1109(37) 0.000730 1056. 1123.
1152(38) 0.000693 1055. 1150.
1224(39) 0.000657 1055. 1182.
1218(39) 0.000657 1055. 1209.
1220(39) 0.000657 1054. 1220.
1197(39) 0.000657 1054. 1210.
1191(38) 0.000693 1054. 1187.
1157(38) 0.000693 1053. 1167.
1195(38) 0.000693 1053. 1164.
1260(40) 0.000625 1053. 1187.
1229(39) 0.000657 1052. 1244.
1328(41) 0.000595 1052. 1333.
1480(43) 0.000541 1052. 1442.
1619(45) 0.000494 1052. 1540.
1669(46) 0.000473 1051. 1586.
1536(44) 0.000517 1051. 1552.
1517(44) 0.000517 1051. 1451.
1327(41) 0.000595 1050. 1332.
1219(39) 0.000657 1050. 1232.
1156(38) 0.000693 1050. 1162.
1076(36) 0.000772 1049. 1120.
1083(37) 0.000730 1049. 1098.
1077(36) 0.000772 1049. 1087.
1059(36) 0.000772 1049. 1081.
1123(37) 0.000730 1048. 1078.
1062(36) 0.000772 1048. 1075.
1062(36) 0.000772 1048. 1072.
1084(37) 0.000730 1047. 1070.
1078(36) 0.000772 1047. 1069.
1106(37) 0.000730 1047. 1068.
1109(37) 0.000730 1047. 1067.
1079(36) 0.000772 1046. 1067.
1068(36) 0.000772 1046. 1067.
1065(36) 0.000772 1046. 1068.
1123(37) 0.000730 1045. 1069.
1131(37) 0.000730 1045. 1072.
1110(37) 0.000730 1045. 1075.
1047(36) 0.000772 1044. 1082.
1041(36) 0.000772 1044. 1094.
1096(37) 0.000730 1044. 1117.
1125(37) 0.000730 1044. 1154.
1192(38) 0.000693 1043. 1211.
1285(40) 0.000625 1043. 1282.
1326(41) 0.000595 1043. 1354.
1363(41) 0.000595 1042. 1402.
1332(41) 0.000595 1042. 1402.
1342(41) 0.000595 1042. 1353.
1285(40) 0.000625 1042. 1283.
1209(39) 0.000657 1041. 1222.
1145(38) 0.000693 1041. 1186.
1160(38) 0.000693 1041. 1180.
1179(38) 0.000693 1040. 1201.
1246(39) 0.000657 1040. 1242.
1290(40) 0.000625 1040. 1287.
1313(40) 0.000625 1040. 1319.
1317(41) 0.000595 1039. 1321.
1308(40) 0.000625 1039. 1295.
1253(39) 0.000657 1039. 1265.
1244(39) 0.000657 1039. 1257.
1276(40) 0.000625 1038. 1292.
1272(40) 0.000625 1038. 1385.
1483(43) 0.000541 1038. 1540.
1742(47) 0.000453 1037. 1737.
1969(50) 0.000400 1037. 1925.
2009(51) 0.000384 1037. 2033.
1921(46) 0.000473 1037. 1999.
1717(44) 0.000517 1036. 1837.
1552(42) 0.000567 1036. 1631.
1453(40) 0.000625 1036. 1455.
1330(38) 0.000693 1036. 1343.
1280(38) 0.000693 1035. 1299.
1194(36) 0.000772 1035. 1312.
1252(37) 0.000730 1035. 1359.
1353(39) 0.000657 1034. 1409.
1372(39) 0.000657 1034. 1430.
1333(38) 0.000693 1034. 1404.
1294(38) 0.000693 1034. 1342.
1259(37) 0.000730 1033. 1275.
1204(36) 0.000772 1033. 1229.
1257(37) 0.000730 1033. 1218.
1314(38) 0.000693 1033. 1243.
1304(38) 0.000693 1032. 1300.
1428(40) 0.000625 1032. 1369.
1530(41) 0.000595 1032. 1424.
1522(41) 0.000595 1032. 1436.
1425(40) 0.000625 1031. 1392.
1366(39) 0.000657 1031. 1314.
1297(38) 0.000693 1031. 1236.
1241(37) 0.000730 1031. 1175.
1181(36) 0.000772 1030. 1140.
1096(35) 0.000816 1030.0 1126.2
1104(35) 0.000816 1029.7 1128.0
1135(35) 0.000816 1029.5 1136.4
1121(35) 0.000816 1029.2 1142.2
1112(35) 0.000816 1029.0 1139.0
1091(35) 0.000816 1028.7 1126.6
1125(35) 0.000816 1028.5 1112.4
1127(35) 0.000816 1028.2 1104.1
1061(34) 0.000865 1027.9 1107.1
1105(35) 0.000816 1027.7 1124.0
1181(36) 0.000772 1027. 1154.
1206(36) 0.000772 1027. 1191.
1234(37) 0.000730 1027. 1222.
1281(38) 0.000693 1027. 1233.
1272(37) 0.000730 1026. 1215.
1200(36) 0.000772 1026. 1178.
1107(35) 0.000816 1025.9 1135.8
1075(34) 0.000865 1025.7 1100.6
1075(34) 0.000865 1025.4 1075.9
1064(34) 0.000865 1025.2 1060.4
1049(34) 0.000865 1024.9 1051.7
1004(33) 0.000918 1024.7 1046.9
1023(33) 0.000918 1024.4 1044.3
1051(34) 0.000865 1024.2 1042.7
1008(33) 0.000918 1023.9 1041.9
1023(33) 0.000918 1023.7 1041.8
1018(33) 0.000918 1023.4 1042.4
1057(34) 0.000865 1023.2 1044.3
1056(34) 0.000865 1023.0 1047.3
1070(34) 0.000865 1022.7 1051.5
1085(34) 0.000865 1022.5 1056.5
1018(33) 0.000918 1022.2 1061.1
1017(33) 0.000918 1022.0 1064.2
1112(35) 0.000816 1021.7 1065.8
1077(34) 0.000865 1021.5 1068.5
1081(34) 0.000865 1021.3 1076.6
1147(35) 0.000816 1021.0 1094.8
1116(35) 0.000816 1020.8 1127.2
1194(36) 0.000772 1021. 1174.
1256(37) 0.000730 1020. 1231.
1257(37) 0.000730 1020. 1284.
1262(37) 0.000730 1020. 1311.
1291(38) 0.000693 1020. 1299.
1211(36) 0.000772 1019. 1253.
1183(36) 0.000772 1019. 1196.
1194(36) 0.000772 1019. 1146.
1157(36) 0.000772 1019. 1113.
1073(34) 0.000865 1018.4 1097.4
1085(34) 0.000865 1018.1 1094.8
1088(35) 0.000816 1017.9 1099.2
1094(35) 0.000816 1017.7 1103.8
1095(35) 0.000816 1017.4 1103.5
1027(33) 0.000918 1017.2 1097.9
1069(34) 0.000865 1017.0 1092.6
1085(34) 0.000865 1016.7 1094.2
1073(34) 0.000865 1016.5 1107.9
1118(35) 0.000816 1016.3 1136.3
1158(36) 0.000772 1016. 1177.
1189(36) 0.000772 1016. 1223.
1254(37) 0.000730 1016. 1257.
1228(37) 0.000730 1015. 1264.
1265(37) 0.000730 1015. 1237.
1179(36) 0.000772 1015. 1190.
1131(35) 0.000816 1014.6 1142.0
1103(35) 0.000816 1014.4 1102.9
1059(34) 0.000865 1014.2 1076.1
1046(34) 0.000865 1014.0 1060.2
1036(34) 0.000865 1013.7 1052.2
991(33) 0.000918 1013.5 1049.4
978(33) 0.000918 1013.3 1050.1
1042(34) 0.000865 1013.0 1054.6
1095(35) 0.000816 1012.8 1064.8
1139(35) 0.000816 1012.6 1084.3
1128(35) 0.000816 1012.4 1118.3
1172(36) 0.000772 1012. 1171.
1254(35) 0.000816 1011.9 1241.4
1337(37) 0.000730 1012. 1321.
1417(38) 0.000693 1011. 1388.
1477(39) 0.000657 1011. 1414.
1437(38) 0.000693 1011. 1386.
1375(37) 0.000730 1011. 1319.
1281(36) 0.000772 1011. 1244.
1123(33) 0.000918 1010.3 1183.1
1148(34) 0.000865 1010.1 1146.6
1107(33) 0.000918 1009.9 1133.7
1153(34) 0.000865 1009.7 1137.0
1172(34) 0.000865 1009.4 1145.9
1175(34) 0.000865 1009.2 1148.0
1145(34) 0.000865 1009.0 1136.6
1127(34) 0.000865 1008.8 1114.5
1118(33) 0.000918 1008.6 1089.8
1088(33) 0.000918 1008.3 1068.2
1043(32) 0.000977 1008.1 1052.3
996(31) 0.001041 1007.9 1042.0
1025(32) 0.000977 1007.7 1035.9
1017(32) 0.000977 1007.5 1032.5
1018(32) 0.000977 1007.2 1030.8
1004(32) 0.000977 1007.0 1030.0
987(31) 0.001041 1006.8 1029.8
1009(32) 0.000977 1006.6 1030.1
1054(32) 0.000977 1006.4 1030.9
1047(32) 0.000977 1006.1 1032.2
985(31) 0.001041 1005.9 1034.1
997(32) 0.000977 1005.7 1036.8
1051(32) 0.000977 1005.5 1040.8
1080(33) 0.000918 1005.3 1047.0
1096(33) 0.000918 1005.1 1057.7
1081(33) 0.000918 1004.8 1076.7
1064(33) 0.000918 1004.6 1109.6
1175(34) 0.000865 1004.4 1162.1
1211(35) 0.000816 1004.2 1236.7
1311(36) 0.000772 1004. 1328.
1396(37) 0.000730 1004. 1419.
1440(38) 0.000693 1004. 1477.
1410(38) 0.000693 1003. 1473.
1419(38) 0.000693 1003. 1418.
1335(37) 0.000730 1003. 1351.
1304(36) 0.000772 1003. 1306.
1265(36) 0.000772 1002. 1303.
1233(35) 0.000816 1002.3 1347.0
1380(37) 0.000730 1002. 1424.
1432(38) 0.000693 1002. 1507.
1440(38) 0.000693 1002. 1549.
1487(39) 0.000657 1001. 1520.
1424(38) 0.000693 1001. 1433.
1347(37) 0.000730 1001. 1326.
1279(36) 0.000772 1001. 1231.
1196(35) 0.000816 1000.6 1160.8
1094(33) 0.000918 1000.4 1116.2
1042(32) 0.000977 1000.1 1092.0
1093(33) 0.000918 999.9 1080.4
1052(32) 0.000977 999.7 1074.4
1054(32) 0.000977 999.5 1070.2
1087(33) 0.000918 999.3 1068.4
1061(33) 0.000918 999.1 1072.0
1067(33) 0.000918 998.9 1084.0
1049(32) 0.000977 998.7 1106.5
1101(33) 0.000918 998.5 1138.2
1168(34) 0.000865 998.3 1173.8
1210(35) 0.000816 998.0 1202.3
1177(34) 0.000865 997.8 1210.2
1240(35) 0.000816 997.6 1194.7
1180(34) 0.000865 997.4 1168.6
1126(34) 0.000865 997.2 1148.0
1179(34) 0.000865 997.0 1143.3
1163(34) 0.000865 996.8 1157.9
1206(35) 0.000816 996.6 1188.7
1209(35) 0.000816 996.4 1224.9
1243(35) 0.000816 996.2 1248.8
1221(35) 0.000816 996.0 1243.5
1234(35) 0.000816 995.8 1209.7
1206(35) 0.000816 995.6 1163.7
1182(34) 0.000865 995.4 1120.1
1080(33) 0.000918 995.2 1086.7
1070(33) 0.000918 994.9 1065.2
1047(32) 0.000977 994.7 1053.7
1048(32) 0.000977 994.5 1048.4
1081(33) 0.000918 994.3 1044.9
1076(33) 0.000918 994.1 1040.5
1032(32) 0.000977 993.9 1034.8
1049(32) 0.000977 993.7 1029.1
1021(32) 0.000977 993.5 1024.3
1043(32) 0.000977 993.3 1020.7
1018(32) 0.000977 993.1 1018.5
1040(32) 0.000977 992.9 1017.4
1029(32) 0.000977 992.7 1017.0
1040(32) 0.000977 992.5 1017.4
1076(33) 0.000918 992.3 1018.3
1037(32) 0.000977 992.1 1019.8
1038(32) 0.000977 991.9 1022.1
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1034(32) 0.000977 991.3 1035.2
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1176(33) 0.000918 989.9 1244.9
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1438(37) 0.000730 989. 1537.
1549(38) 0.000693 989. 1569.
1520(38) 0.000693 989. 1538.
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1401(36) 0.000772 988. 1434.
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1677(40) 0.000625 987. 1740.
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1558(38) 0.000693 987. 1603.
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1340(36) 0.000772 986. 1259.
1178(33) 0.000918 986.3 1205.8
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1191(33) 0.000918 985.7 1155.4
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1142(33) 0.000918 983.5 1080.1
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1162(33) 0.000918 981.8 1135.7
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1074(32) 0.000977 975.0 1126.3
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1016(31) 0.001041 972.7 1024.7
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1191(32) 0.000977 970.0 1198.3
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1430(35) 0.000816 968.5 1404.3
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999(28) 0.001276 913.5 950.0
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1127(30) 0.001111 816.6 1154.8
1155(31) 0.001041 816.6 1154.4
1165(31) 0.001041 816.7 1153.5
1147(31) 0.001041 816.8 1152.0
1148(31) 0.001041 816.9 1149.9
1209(32) 0.000977 817.0 1147.3
1168(31) 0.001041 817.0 1144.3
1146(31) 0.001041 817.1 1140.8
1184(31) 0.001041 817.2 1137.0
1163(31) 0.001041 817.3 1132.7
1188(31) 0.001041 817.4 1128.2
1144(31) 0.001041 817.5 1123.3
1184(31) 0.001041 817.6 1118.2
1108(30) 0.001111 817.6 1112.9
1055(30) 0.001111 817.7 1107.4
1070(30) 0.001111 817.8 1101.7
1094(30) 0.001111 817.9 1095.8
1104(30) 0.001111 818.0 1089.9
1031(29) 0.001189 818.1 1083.9
1060(30) 0.001111 818.2 1077.9
1071(30) 0.001111 818.4 1072.0
1081(30) 0.001111 818.5 1066.1
1029(29) 0.001189 818.6 1060.4
1044(29) 0.001189 818.7 1054.9
1054(30) 0.001111 818.8 1049.5
1014(29) 0.001189 818.9 1044.4
1016(29) 0.001189 819.0 1039.5
993(29) 0.001189 819.2 1034.9
1040(29) 0.001189 819.3 1030.6
1031(29) 0.001189 819.4 1026.5
995(29) 0.001189 819.5 1022.7
1027(29) 0.001189 819.7 1019.1
1028(29) 0.001189 819.8 1015.8
995(29) 0.001189 819.9 1012.8
1008(29) 0.001189 820.1 1009.9
1023(29) 0.001189 820.2 1007.3
992(29) 0.001189 820.4 1004.8
959(28) 0.001276 820.5 1002.5
951(28) 0.001276 820.7 1000.3
986(29) 0.001189 820.8 998.3
993(29) 0.001189 821.0 996.4
962(28) 0.001276 821.1 994.6
992(29) 0.001189 821.3 993.0
962(28) 0.001276 821.5 991.6
999(29) 0.001189 821.6 990.4
1006(29) 0.001189 821.8 989.4
968(28) 0.001276 822.0 988.7
978(29) 0.001189 822.2 988.3
1001(29) 0.001189 822.3 988.2
1003(29) 0.001189 822.5 988.4
1049(29) 0.001189 822.7 989.0
1008(29) 0.001189 822.9 990.1
1009(29) 0.001189 823.1 991.5
1009(29) 0.001189 823.3 993.4
1011(29) 0.001189 823.5 995.7
990(29) 0.001189 823.7 998.5
1005(29) 0.001189 823.9 1001.7
1029(29) 0.001189 824.1 1005.3
1057(30) 0.001111 824.3 1009.4
1019(29) 0.001189 824.5 1013.9
1000(29) 0.001189 824.8 1018.7
1035(30) 0.001111 825.0 1023.9
1049(30) 0.001111 825.2 1029.4
1079(30) 0.001111 825.4 1035.2
1032(30) 0.001111 825.7 1041.3
1019(29) 0.001189 825.9 1047.5
1038(30) 0.001111 826.2 1053.9
1053(30) 0.001111 826.4 1060.4
1050(30) 0.001111 826.7 1066.8
1054(30) 0.001111 826.9 1073.3
1085(30) 0.001111 827.2 1079.6
1071(30) 0.001111 827.4 1085.7
1085(30) 0.001111 827.7 1091.6
1097(30) 0.001111 828.0 1097.1
1084(30) 0.001111 828.3 1102.2
1138(31) 0.001041 828.5 1106.8
1130(31) 0.001041 828.8 1110.9
1131(31) 0.001041 829.1 1114.4
1098(30) 0.001111 829.4 1117.4
1089(30) 0.001111 829.7 1119.7
1102(30) 0.001111 830.0 1121.4
1110(31) 0.001041 830.3 1122.5
1086(30) 0.001111 830.6 1123.1
1105(30) 0.001111 831.0 1123.2
1118(31) 0.001041 831.3 1122.8
1130(31) 0.001041 831.6 1122.1
1171(31) 0.001041 831.9 1121.0
1150(31) 0.001041 832.3 1119.7
1113(31) 0.001041 832.6 1118.2
1111(31) 0.001041 833.0 1116.6
1117(31) 0.001041 833.3 1114.8
1089(30) 0.001111 833.7 1113.0
1131(31) 0.001041 834.1 1111.1
1075(30) 0.001111 834.4 1109.2
1107(30) 0.001111 834.8 1107.3
1149(31) 0.001041 835.2 1105.4
1157(31) 0.001041 835.6 1103.5
1140(31) 0.001041 836.0 1101.6
1116(31) 0.001041 836.4 1099.7
1093(30) 0.001111 836.8 1097.8
1112(31) 0.001041 837.2 1095.9
1083(30) 0.001111 837.6 1093.8
1081(30) 0.001111 838.0 1091.7
1080(30) 0.001111 838.4 1089.5
1093(30) 0.001111 838.9 1087.2
1105(30) 0.001111 839.3 1084.8
1106(30) 0.001111 839.8 1082.3
1075(30) 0.001111 840.2 1079.6
1090(30) 0.001111 840.7 1076.8
1054(30) 0.001111 841.1 1074.0
1071(30) 0.001111 841.6 1071.0
1100(30) 0.001111 842.1 1068.0
1092(30) 0.001111 842.6 1065.0
1059(30) 0.001111 843.1 1062.0
1048(30) 0.001111 843.6 1058.9
1065(30) 0.001111 844.1 1055.9
1039(30) 0.001111 844.6 1052.9
1046(30) 0.001111 845.1 1050.0
1053(30) 0.001111 845.6 1047.2
1070(30) 0.001111 846.2 1044.4
1029(29) 0.001189 846.7 1041.7
1021(29) 0.001189 847.3 1039.2
1066(30) 0.001111 847.8 1036.6
1043(30) 0.001111 848.4 1034.2
1017(29) 0.001189 849.0 1031.9
1003(29) 0.001189 849.5 1029.7
998(29) 0.001189 850.1 1027.5
1006(29) 0.001189 850.7 1025.4
983(29) 0.001189 851.3 1023.4
988(29) 0.001189 851.9 1021.4
1021(29) 0.001189 852.5 1019.5
986(29) 0.001189 853.2 1017.6
972(29) 0.001189 853.8 1015.8
999(29) 0.001189 854.4 1014.0
1032(30) 0.001111 855.1 1012.2
1039(30) 0.001111 855.8 1010.4
1007(29) 0.001189 856.4 1008.7
1011(29) 0.001189 857.1 1006.9
998(29) 0.001189 857.8 1005.3
1043(30) 0.001111 858.5 1003.6
1034(30) 0.001111 859.2 1002.0
1038(30) 0.001111 859.9 1000.4
992(29) 0.001189 860.6 998.9
943(28) 0.001276 861.3 997.5
979(29) 0.001189 862.1 996.1
1007(29) 0.001189 862.8 994.7
1005(29) 0.001189 863.6 993.5
960(29) 0.001189 864.4 992.3
924(28) 0.001276 865.1 991.3
954(28) 0.001276 865.9 990.3
991(29) 0.001189 866.7 989.5
1039(30) 0.001111 867.5 988.8
1003(29) 0.001189 868.3 988.2
972(29) 0.001189 869.2 987.8
1002(29) 0.001189 870.0 987.6
983(29) 0.001189 870.8 987.5
939(28) 0.001276 871.7 987.6
936(28) 0.001276 872.6 988.0
974(29) 0.001189 873.4 988.5
969(29) 0.001189 874.3 989.3
1014(24) 0.001736 875.2 990.3
1002(29) 0.001189 876.1 991.6
989(29) 0.001189 877.0 993.1
996(29) 0.001189 878.0 994.8
988(29) 0.001189 878.9 996.9
1014(30) 0.001111 879.9 999.2
1036(30) 0.001111 880.8 1001.8
1054(30) 0.001111 881.8 1004.7
1053(30) 0.001111 882.8 1007.8
1027(30) 0.001111 883.8 1011.2
1039(30) 0.001111 884.8 1014.9
1042(30) 0.001111 885.8 1018.9
1015(30) 0.001111 886.9 1023.1
1009(30) 0.001111 887.9 1027.6
1026(30) 0.001111 889.0 1032.3
1054(30) 0.001111 890.0 1037.3
1075(30) 0.001111 891.1 1042.5
1072(30) 0.001111 892.2 1048.0
1044(30) 0.001111 893.3 1053.6
1040(30) 0.001111 894.4 1059.5
1055(30) 0.001111 895.6 1065.5
1091(31) 0.001041 896.7 1071.7
1092(31) 0.001041 897.9 1078.0
1079(30) 0.001111 899.0 1084.5
1101(31) 0.001041 900.2 1091.0
1119(31) 0.001041 901.4 1097.6
1098(31) 0.001041 902.6 1104.3
1109(31) 0.001041 903.8 1111.0
1118(31) 0.001041 905.1 1117.7
1135(31) 0.001041 906.3 1124.4
1174(32) 0.000977 907.6 1131.0
1190(32) 0.000977 908.9 1137.6
1160(31) 0.001041 910.2 1144.1
1123(31) 0.001041 911.5 1150.5
1129(31) 0.001041 912.8 1156.8
1192(32) 0.000977 914.1 1163.0
1185(32) 0.000977 915.5 1169.0
1179(32) 0.000977 916.8 1174.9
1203(32) 0.000977 918.2 1180.6
1169(32) 0.000977 919.6 1186.2
1191(32) 0.000977 921.0 1191.6
1202(32) 0.000977 922.5 1196.8
1200(32) 0.000977 923.9 1201.9
1218(32) 0.000977 925.3 1206.7
1215(32) 0.000977 926.8 1211.4
1238(32) 0.000977 928.3 1215.8
1229(32) 0.000977 929.8 1220.1
1193(32) 0.000977 931.3 1224.2
1227(32) 0.000977 932.9 1228.1
1242(32) 0.000977 934.4 1231.8
1239(32) 0.000977 936.0 1235.3
1241(32) 0.000977 937.6 1238.7
1252(33) 0.000918 939.2 1241.9
1269(33) 0.000918 940.8 1245.1
1289(33) 0.000918 942.4 1248.1
1266(33) 0.000918 944.1 1251.1
1238(32) 0.000977 945.7 1253.9
1239(32) 0.000977 947.4 1256.8
1232(32) 0.000977 949.1 1259.6
1273(33) 0.000918 950.8 1262.4
1260(33) 0.000918 952.6 1265.2
1273(33) 0.000918 954.3 1268.1
1271(33) 0.000918 956.1 1270.9
1259(33) 0.000918 957.9 1273.8
1279(33) 0.000918 959.7 1276.6
1300(33) 0.000918 961.5 1279.5
1329(34) 0.000865 963.4 1282.4
1308(33) 0.000918 965.2 1285.3
1248(33) 0.000918 967.1 1288.1
1219(32) 0.000977 969.0 1290.9
1245(33) 0.000918 971.0 1293.6
1277(33) 0.000918 972.9 1296.2
1284(33) 0.000918 974.9 1298.7
1276(33) 0.000918 976.8 1301.0
1301(33) . . .
1311(33) . . .
1297(33) . . .
1306(33) . . .
1262(33) . . .
1264(33) . . .
1306(33) . . .
1315(33) . . .
1285(33) . . .
1269(33) . . .
1266(33) . . .
1282(33) . . .
1274(33) . . .
1275(33) . . .
1326(33) . . .
1310(33) . . .
1286(33) . . .
1281(33) . . .
1249(33) . . .
1260(33) . . .
1308(33) . . .
1306(33) . . .
1279(33) . . .
1298(33) . . .
1275(33) . . .
1274(33) . . .
1273(34) . . .
1275(34) . . .
1231(33) . . .
1236(33) . . .
1275(34) . . .
1302(34) . . .
1279(34) . . .
1270(34) . . .
1286(34) . . .
1311(34) . . .
1303(34) . . .
1305(34) . . .
1281(34) . . .
1258(33) . . .
1263(33) . . .
1302(34) . . .
1264(33) . . .
1280(34) . . .
1290(34) . . .
1287(34) . . .
1263(33) . . .
1300(34) . . .
1277(34) . . .
1248(33) . . .
1252(33) . . .
1243(33) . . .
1262(33) . . .
1309(34) . . .
1312(34) . . .
1286(34) . . .
1237(33) . . .
1261(33) . . .
1286(34) . . .
1278(34) . . .
1328(34) . . .
1274(34) . . .
1330(34) . . .
1376(35) . . .
1302(34) . . .
1303(34) . . .
1349(34) . . .
1313(34) . . .
1335(34) . . .
1358(35) . . .
1351(35) . . .
1357(35) . . .
1368(35) . . .
1366(35) . . .
1376(35) . . .
1359(35) . . .
1368(35) . . .
1430(35) . . .
1413(35) . . .
1412(35) . . .
1424(35) . . .
1401(35) . . .
1411(35) . . .
1426(35) . . .
1437(35) . . .
1469(36) . . .
1488(36) . . .
1475(36) . . .
1454(36) . . .
1463(36) . . .
1560(37) . . .
1546(37) . . .
1467(36) . . .
1481(36) . . .
1504(36) . . .
1501(36) . . .
1533(37) . . .
1567(37) . . .
1520(36) . . .
1550(37) . . .
1545(37) . . .
1536(37) . . .
1556(37) . . .
1589(37) . . .
1591(37) . . .
1574(37) . . .
1588(37) . . .
1624(37) . . .
1604(37) . . .
1643(38) . . .
1675(38) . . .
1705(38) . . .
1681(38) . . .
1665(38) . . .
1698(38) . . .
1704(38) . . .
1722(39) . . .
1729(39) . . .
1689(38) . . .
1679(38) . . .
1745(39) . . .
1731(39) . . .
1688(38) . . .
1817(39) . . .
1774(39) . . .
1774(39) . . .
1817(57) . . .
1786(56) . . .
1805(56) . . .
1831(57) . . .
1850(57) . . .
1714(55) . . .
1740(56) . . .
1777(56) . . .
1875(57) . . .
1934(58) . . .
1844(57) . . .
1935(58) . . .
1786(56) . . .
1910(58) . . .
1888(58) . . .
1847(57) . . .
1892(58) . . .
1975(59) . . .
1904(58) . . .
2026(59) . . .
1986(59) . . .
1900(58) . . .
1931(58) . . .
1940(58) . . .
1898(58) . . .
1903(58) . . .
1865(57) . . .
1965(59) . . .
1965(59) . . .
1907(58) . . .
1974(59) . . .
2016(59) . . .
1927(58) . . .
1997(59) . . .
1977(59) . . .
1937(58) . . .
2002(59) . . .
1984(59) . . .
2012(59) . . .
2047(60) . . .
2013(59) . . .
2018(59) . . .
1941(58) . . .
2048(60) . . .
2080(60) . . .
2068(60) . . .
2079(60) . . .
2015(59) . . .
2091(60) . . .
2045(60) . . .
2048(60) . . .
2064(60) . . .
2111(61) . . .
2053(60) . . .
2031(59) . . .
2058(60) . . .
2100(60) . . .
2135(61) . . .
2098(60) . . .
2115(61) . . .
2128(61) . . .
2118(61) . . .
2124(61) . . .
2196(62) . . .
2113(61) . . .
2158(61) . . .
2096(60) . . .
2081(60) . . .
2133(61) . . .
2100(60) . . .
2205(62) . . .
2132(61) . . .
2155(61) . . .
2159(61) . . .
2197(62) . . .
2247(62) . . .
2229(62) . . .
2274(63) . . .
2244(62) . . .
2191(62) . . .
2123(61) . . .
2112(61) . . .
2298(63) . . .
2287(63) . . .
2333(63) . . .
2309(63) . . .
2200(62) . . .
2299(63) . . .
2298(63) . . .
2324(63) . . .
2224(62) . . .
2329(63) . . .
2264(62) . . .
2140(61) . . .
2243(62) . . .
2232(62) . . .
2231(62) . . .
2244(62) . . .
2342(63) . . .
2419(64) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_cell_measurement_reflns_used    632
_reflns_number_total             632
_reflns_limit_h_min              1
_reflns_limit_h_max              17
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.065
_reflns_d_resolution_low         18.669
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_FREECL_publ
_database_code_depnum_ccdc_archive 'CCDC 1582009'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-02-13T16:11|FREECL||c2

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-02-13T16:11

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.07
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     39
_refine_ls_goodness_of_fit_all   0.99
_refine_ls_number_restraints     11
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
"from Z:/queen/Dropbox (EPFL Valais Wallis)/Mehrdad's Work/CO2 in M"
_cell_length_a                   18.51977(35)
_cell_length_b                   18.51977
_cell_length_c                   18.51977
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6351.9(4)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cu Cu1 0.1322(5) 0.5 0.0 1.0 Uiso 0.0095(27) 12
C C1 0.14834(26) 0.33711(31) -0.14834(26) 1.0 Uiso 0.0063(8) 24
C C2 0.18083(23) 0.27352(32) -0.18083(23) 1.0 Uiso 0.0063(8) 24
C C3 0.24163(25) 0.24163(25) -0.1492(4) 1.0 Uiso 0.0063(8) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.045(5) 3
N N1 0.12964(18) 0.42512(18) -0.07873(18) 1.0 Uiso 0.0102(5) 48
N N2 0.17467(19) 0.37041(18) -0.08916(17) 1.0 Uiso 0.0102(5) 48
H H1 0.2664(5) 0.2664(5) -0.1027(7) 1.0 Uiso 0.021(4) 24
Cu Cu2 0.2309(24) 0.3557(26) 0.0 0.192(8) Uiso 0.06409 24
O Os 0.2496(32) 0.5 0.0 0.174(17) Uiso 0.01168 12
Cl Cl2 0.3662(20) 0.3662(20) 0.0 0.192(8) Uiso 0.06535 12

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C24 H8 Cl1.77 Cu5.54 N32 O0.70'
_chemical_formula_weight         1170.15
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 Cl1 2.449(9) . 1_555 N
Cu1 N1 2.0127(30) . 1_555 N
Cu1 N1 2.0127(30) . 4_555 N
Cu1 N1 2.0127(30) . 12_565 N
Cu1 N1 2.944(4) . 17_555 N
Cu1 N1 2.944(4) . 19_555 N
Cu1 N1 2.944(4) . 23_565 N
Cu1 N1 2.0127(30) . -10_565 N
Cu1 N1 2.944(4) . -14_565 N
Cu1 Cu2 3.24(5) . 1_555 N
Cu1 Cu2 3.24(5) . 12_565 N
Cu1 Os 2.17(6) . 1_555 N
C1 C2 1.453(9) . 1_555 N
C1 C3 2.472(5) . 1_555 N
C1 C3 2.472(5) . 7_555 N
C1 N1 2.107(6) . 1_555 N
C1 N1 2.107(6) . 19_555 N
C1 N2 1.349(4) . 1_555 N
C1 N2 1.349(4) . 19_555 N
C2 C1 1.453(9) . 1_555 N
C2 C2 2.428(11) . 7_555 N
C2 C2 2.428(11) . 9_555 N
C2 C3 1.400(5) . 1_555 N
C2 C3 1.400(5) . 7_555 N
C2 N2 2.473(6) . 1_555 N
C2 N2 2.473(6) . 19_555 N
C3 C1 2.472(5) . 1_555 N
C3 C1 2.472(5) . 9_555 N
C3 C2 1.400(5) . 1_555 N
C3 C2 1.400(5) . 9_555 N
C3 C3 2.422(12) . 7_555 N
C3 C3 2.422(12) . 9_555 N
C3 H1 1.077(17) . 1_555 N
Cl1 Cu1 2.449(9) . 1_555 N
Cl1 Cu1 2.449(9) . 10_555 N
Cl1 Cu1 2.449(9) . 14_555 N
Cl1 Cu1 2.449(9) . 19_555 N
Cl1 N1 3.1325(31) . 1_555 N
Cl1 N1 3.1325(31) . 4_555 N
Cl1 N1 3.1325(31) . 10_555 N
Cl1 N1 3.1325(31) . 12_565 N
Cl1 N1 3.1325(31) . 14_555 N
Cl1 N1 3.1325(31) . 17_555 N
Cl1 N1 3.1325(31) . 19_555 N
Cl1 N1 3.1325(31) . 23_565 N
Cl1 N1 3.1325(31) . -1_565 N
Cl1 N1 3.1325(31) . -4_565 N
Cl1 N1 3.1325(31) . -10_565 N
Cl1 N1 3.1325(31) . -12_555 N
Cl1 N1 3.1325(31) . -14_565 N
Cl1 N1 3.1325(31) . -17_565 N
Cl1 N1 3.1325(31) . -19_565 N
Cl1 N1 3.1325(31) . -23_555 N
N1 Cu1 2.0127(30) . 1_555 N
N1 Cu1 2.944(4) . 19_555 N
N1 C1 2.107(6) . 1_555 N
N1 Cl1 3.1325(31) . 1_555 N
N1 N1 1.333(7) . 19_555 N
N1 N2 1.327(5) . 1_555 N
N1 N2 2.178(4) . 19_555 N
N1 Cu2 2.70(4) . 1_555 N
N2 C1 1.349(4) . 1_555 N
N2 C2 2.473(6) . 1_555 N
N2 N1 1.327(5) . 1_555 N
N2 N1 2.178(4) . 19_555 N
N2 N2 2.240(6) . 19_555 N
N2 Cu2 1.971(26) . 1_555 N
H1 C3 1.077(17) . 1_555 N
H1 Cu2 2.61(4) . 1_555 N
H1 Cu2 2.61(4) . 13_555 N
Cu2 Cu1 3.24(5) . 1_555 N
Cu2 N1 2.70(4) . 1_555 N
Cu2 N1 2.70(4) . 4_555 N
Cu2 N2 1.971(26) . 1_555 N
Cu2 N2 1.971(26) . 4_555 N
Cu2 H1 2.61(4) . 1_555 N
Cu2 H1 2.61(4) . 4_555 N
Cu2 Cu2 3.27(10) . 13_555 N
Cu2 Os 2.69(5) . 1_555 N
Cu2 Cl2 2.51(6) . 1_555 N
Os Cu1 2.17(6) . 1_555 N
Os Cu2 2.69(5) . 1_555 N
Os Cu2 2.69(5) . 12_565 N
Cl2 Cu2 2.51(6) . 1_555 N
Cl2 Cu2 2.51(6) . 13_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Cu1 N1 88.63(28) 1_555 . 1_555 N
Cl1 Cu1 N1 88.63(28) 1_555 . 4_555 N
Cl1 Cu1 N1 88.63(28) 1_555 . 12_565 N
Cl1 Cu1 N1 88.63(28) 1_555 . -10_565 N
N1 Cu1 N1 92.83(21) 1_555 . 4_555 N
N1 Cu1 N1 177.3(6) 1_555 . 12_565 N
N1 Cu1 N1 87.10(21) 1_555 . -10_565 N
N1 Cu1 N1 87.10(21) 4_555 . 12_565 N
N1 Cu1 N1 177.3(6) 4_555 . -10_565 N
N1 Cu1 N1 92.83(21) 12_565 . -10_565 N
C2 C1 N2 123.88(29) 1_555 . 1_555 N
C2 C1 N2 123.88(29) 1_555 . 19_555 N
N2 C1 N2 112.2(6) 1_555 . 19_555 N
C1 C2 C3 120.10(32) 1_555 . 1_555 N
C1 C2 C3 120.10(32) 1_555 . 7_555 N
C3 C2 C3 119.7(6) 1_555 . 7_555 N
C2 C3 C2 120.2(6) 1_555 . 9_555 N
C2 C3 H1 119.81(32) 1_555 . 1_555 N
C2 C3 H1 119.81(32) 9_555 . 1_555 N
Cu1 Cl1 Cu1 180.0 1_555 . 10_555 N
Cu1 Cl1 Cu1 90.0 1_555 . 14_555 N
Cu1 Cl1 Cu1 90.0 1_555 . 19_555 N
Cu1 Cl1 Cu1 90.0 10_555 . 14_555 N
Cu1 Cl1 Cu1 90.0 10_555 . 19_555 N
Cu1 Cl1 Cu1 180.0 14_555 . 19_555 N
Cu1 N1 N1 121.94(24) 1_555 . 19_555 N
Cu1 N1 N2 128.08(35) 1_555 . 1_555 N
N1 N1 N2 109.97(21) 19_555 . 1_555 N
C1 N2 N1 103.9(4) 1_555 . 1_555 N
C1 N2 Cu2 143.9(14) 1_555 . 1_555 N
N1 N2 Cu2 108.4(14) 1_555 . 1_555 N
N2 Cu2 N2 113.8(23) 1_555 . 4_555 N
N2 Cu2 Cl2 121.1(11) 1_555 . 1_555 N
N2 Cu2 Cl2 121.1(11) 4_555 . 1_555 N
Cu2 Cl2 Cu2 81.1(28) 1_555 . 13_555 N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT602_FREECL_publ         
;
PROBLEM: VERY LARGE Solvent Accessible VOID(S) in Structure        ! Info 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT049_FREECL_publ         
;
PROBLEM: Calculated Density less than 1.0 gcm-3 .........     0.9178 Check 
RESPONSE: This is expected as the material is porous.
;


# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;


_cell_measurement_theta_min      4.5
_cell_measurement_theta_max      160

_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Cu 16.608 0.7718 International_Tables_Vol_C
C 72.0 0.6646 International_Tables_Vol_C
Cl 5.304 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 24.0 -0.3739 International_Tables_Vol_C
O 2.085 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.0782
_pd_proc_ls_prof_R_factor        0.0308
_pd_proc_ls_prof_wR_factor       0.0354
_pd_proc_ls_prof_wR_expected     0.0361
_refine_ls_R_Fsqd_factor         0.03802

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 10 terms.
 Shifted Chebyshev function of 1st kind
      1:    633.269     2:   -154.264     3:    105.010     4:   -5.24822    
      5:    51.1678     6:   -13.0859     7:    25.3142     8:   -1.13472    
      9:    10.1443    10:   -4.25140    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  473.335 #2(GV)   = -194.093 #3(GW)   =  105.811
 #4(GP)   =    3.221 #5(LX)   =    1.028 #6(LY)   =   10.160
 #7(S/L)  =   0.0326 #8(H/L)  =   0.0287
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2016-02-13T16:11:39
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.5019
_pd_proc_2theta_range_max        166.2519
_pd_proc_2theta_range_inc        0.05


loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
5700(160) 0.0 1186. .
5170(160) 0.0 1182. .
4420(140) 0.0 1178. .
4140(140) 0.0 1175. .
3830(130) 0.0 1171. .
3250(120) 0.0 1168. .
3150(120) 0.0 1164. .
2760(110) 0.0 1161. .
2320(110) 0.0 1157. .
2140(100) 0.0 1154. .
2260(100) 0.0 1150. .
2032(98) 0.0 1147. .
1767(92) 0.0 1143. .
1897(95) 0.0 1140. .
1734(91) 0.0 1137. .
1762(91) 0.0 1133. .
1655(89) 0.0 1130. .
1701(90) 0.0 1127. .
1534(85) 0.0 1123. .
1571(86) 0.0 1120. .
1501(85) 0.0 1117. .
1394(82) 0.0 1114. .
1594(87) 0.0 1111. .
1422(82) 0.0 1108. .
1580(87) 0.0 1104. .
1459(83) 0.0 1101. .
1436(83) 0.0 1098. .
1375(81) 0.0 1095. .
1338(80) 0.0 1092. .
1450(83) 0.0 1089. .
1268(78) 0.0 1086. .
1254(77) 0.0 1083. .
1422(82) 0.0 1080. .
1235(77) 0.0 1077. .
1212(76) 0.0 1074. .
1333(80) 0.0 1071. .
1198(76) 0.0 1069. .
1114(73) 0.0 1066. .
998(69) 0.0 1063. .
1235(77) 0.0 1060. .
1110(73) 0.0 1057. .
1072(72) 0.0 1054. .
1133(74) 0.0 1052. .
1133(74) 0.0 1049. .
1077(72) 0.0 1046. .
1091(72) 0.0 1044. .
1054(71) 0.0 1041. .
1021(70) 0.0 1038. .
1119(73) 0.0 1036. .
1133(74) 0.0 1033. .
1082(72) 0.0 1030. .
975(68) 0.0 1028. .
1007(70) 0.0 1025. .
881(65) 0.0 1023. .
1114(73) 0.0 1020. .
961(68) 0.0 1018. .
1003(69) 0.0 1015. .
1105(73) 0.0 1013. .
1138(74) 0.0 1010. .
1040(71) 0.0 1008. .
956(68) 0.0 1005. .
1119(73) 0.0001877 1003. 1003.
867(65) 0.0002367 1000. 1000.
923(67) 0.0002228 998. 998.
942(67) 0.0002228 996. 1003.
1054(71) 0.0001984 993. 1001.
891(66) 0.0002296 991. 999.
867(65) 0.0002367 989. 997.
989(69) 0.0002100 987. 996.
909(66) 0.0002296 984. 994.
914(66) 0.0002296 982. 993.
1091(72) 0.0001929 980. 992.
933(67) 0.0002228 978. 991.
961(68) 0.0002163 975. 991.
1161(75) 0.0001778 973. 992.
1170(75) 0.0001778 971. 998.
1357(80) 0.0001562 969. 1012.
1240(77) 0.0001687 967. 1040.
1161(75) 0.0001778 965. 1089.
1235(77) 0.0001687 962. 1162.
1566(86) 0.0001352 960. 1259.
1576(87) 0.0001321 958. 1378.
1604(87) 0.0001321 956. 1515.
1762(91) 0.0001208 954. 1670.
1795(92) 0.0001181 952. 1843.
1967(97) 0.0001063 950. 2037.
2160(100) 0.0000980 948. 2256.
2390(110) 0.0000890 946. 2506.
2680(110) 0.0000797 944. 2795.
3160(120) 0.0000672 942. 3135.
3470(130) 0.0000610 940. 3545.
4280(140) 0.0000496 938. 4054.
4680(150) 0.0000457 936. 4720.
6170(170) 0.0000346 934. 5631.
7170(180) 0.0000299 932. 6894.
9290(210) 0.0000231 931. 8530.
11190(230) 0.0000191 929. 10274.
12360(240) 0.0000174 927. 11477.
12520(240) 0.0000171 925. 11369.
10630(220) 0.0000201 923. 9671.
7170(130) 0.0000630 921. 7002.
4790(100) 0.0000943 920. 4411.
2877(80) 0.0001562 918. 2584.
1991(66) 0.0002296 916. 1599.
1319(54) 0.0003429 914. 1180.
979(47) 0.000453 913. 1032.
995(47) 0.000453 911. 983.
1041(48) 0.000434 909. 963.
974(47) 0.000453 907. 952.
986(47) 0.000453 906. 943.
933(45) 0.000494 904. 936.
916(45) 0.000494 902. 930.
934(45) 0.000494 901. 925.
940(46) 0.000473 899. 921.
851(43) 0.000541 897. 917.
917(45) 0.000494 896. 913.
912(45) 0.000494 894. 910.
866(44) 0.000517 893. 907.
845(43) 0.000541 891. 904.
839(43) 0.000541 889. 901.
806(42) 0.000567 888. 888.
855(43) 0.000541 886. 886.
851(43) 0.000541 885. 885.
845(43) 0.000541 883. 890.
848(43) 0.000541 882. 889.
801(42) 0.000567 880. 888.
805(42) 0.000567 879. 887.
817(43) 0.000541 877. 887.
891(44) 0.000517 876. 886.
835(43) 0.000541 874. 886.
896(44) 0.000517 873. 886.
809(42) 0.000567 872. 886.
792(42) 0.000567 870. 886.
871(44) 0.000517 869. 888.
876(44) 0.000517 867. 891.
1044(48) 0.000434 866. 900.
1039(48) 0.000434 865. 920.
1001(47) 0.000453 863. 960.
1128(50) 0.000400 862. 1031.
1156(51) 0.000384 860. 1142.
1327(54) 0.0003429 859. 1296.
1497(58) 0.0002973 858. 1493.
1617(60) 0.0002778 856. 1735.
2002(67) 0.0002228 855. 2029.
2236(70) 0.0002041 854. 2390.
2738(78) 0.0001644 853. 2853.
3314(86) 0.0001352 851. 3474.
4393(99) 0.0001020 850. 4341.
5560(110) 0.0000812 849. 5520.
7030(130) 0.0000640 848. 6926.
8020(130) 0.0000557 846. 8180.
8390(140) 0.0000533 845. 8666.
7870(130) 0.0000574 844. 7930.
6050(120) 0.0000743 843. 6160.
4208(97) 0.0001063 841. 4122.
2642(76) 0.0001731 840. 2511.
1640(60) 0.0002778 839. 1558.
1210(52) 0.000370 838. 1120.
878(44) 0.000517 837. 957.
799(42) 0.000567 836. 903.
811(42) 0.000567 834. 882.
838(43) 0.000541 833. 872.
830(43) 0.000541 832. 864.
840(43) 0.000541 831. 858.
834(43) 0.000541 830. 864.
828(43) 0.000541 829. 861.
796(42) 0.000567 828. 858.
855(43) 0.000541 827. 856.
840(43) 0.000541 826. 855.
815(42) 0.000567 825. 854.
792(42) 0.000567 823. 853.
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732(39) 0.000657 752. 752.
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665(36) 0.000772 713. 730.
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744(37) 0.000730 709. 728.
745(37) 0.000730 709. 728.
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877(40) 0.000625 708. 805.
911(41) 0.000595 708. 864.
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818(39) 0.000657 707. 745.
725(36) 0.000772 707. 724.
674(35) 0.000816 706.3 716.0
703(36) 0.000772 706. 713.
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728(37) 0.000730 706. 708.
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707(36) 0.000772 705. 708.
671(35) 0.000816 705.3 708.7
711(36) 0.000772 705. 711.
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713(36) 0.000772 705. 730.
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758(37) 0.000730 704. 720.
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687(35) 0.000816 703.4 707.4
731(37) 0.000730 703. 705.
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701(36) 0.000772 703. 704.
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703(36) 0.000772 702. 704.
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700(36) 0.000772 702. 706.
692(36) 0.000772 702. 710.
675(35) 0.000816 701.8 716.8
679(35) 0.000816 701.7 725.0
773(38) 0.000693 701. 733.
761(37) 0.000730 701. 736.
730(37) 0.000730 701. 734.
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698(36) 0.000772 701. 717.
710(36) 0.000772 701. 710.
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653(34) 0.000865 700.4 704.5
720(36) 0.000772 700. 704.
675(35) 0.000816 700.1 703.8
695(36) 0.000772 700. 704.
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654(35) 0.000816 699.5 704.3
697(36) 0.000772 699. 705.
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683(35) 0.000816 698.9 705.8
699(36) 0.000772 699. 708.
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725(36) 0.000772 698. 715.
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672(35) 0.000816 697.7 721.7
683(35) 0.000816 697.5 727.9
699(36) 0.000772 697. 740.
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790(38) 0.000693 697. 835.
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781(38) 0.000693 695. 766.
735(37) 0.000730 695. 754.
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783(37) 0.000730 695. 785.
877(40) 0.000625 695. 855.
1054(44) 0.000517 694. 1007.
1319(49) 0.000416 694. 1277.
1621(55) 0.0003306 694. 1661.
1968(60) 0.0002778 694. 2063.
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1853(58) 0.0002973 694. 1914.
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821(38) 0.000693 693. 791.
757(37) 0.000730 693. 753.
715(35) 0.000816 692.8 743.9
691(35) 0.000816 692.6 750.9
799(38) 0.000693 692. 780.
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1037(43) 0.000541 692. 1011.
1327(49) 0.000416 692. 1281.
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2194(64) 0.0002441 692. 2011.
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672(34) 0.000865 690.5 738.9
716(36) 0.000772 690. 753.
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906(40) 0.000625 690. 901.
1070(44) 0.000517 690. 1095.
1378(50) 0.000400 690. 1390.
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1989(61) 0.0002687 689. 1999.
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704(35) 0.000816 688.6 730.7
701(35) 0.000816 688.5 715.2
652(34) 0.000865 688.3 710.2
700(35) 0.000816 688.2 710.6
734(36) 0.000772 688. 717.
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790(37) 0.000730 688. 756.
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833(38) 0.000693 687. 789.
807(38) 0.000693 687. 757.
726(36) 0.000772 687. 727.
697(35) 0.000816 686.8 707.6
711(35) 0.000816 686.7 697.7
725(36) 0.000772 687. 693.
695(35) 0.000816 686.4 691.9
716(35) 0.000816 686.3 691.8
749(36) 0.000772 686. 693.
717(35) 0.000816 686.0 695.9
690(35) 0.000816 685.9 701.8
702(35) 0.000816 685.8 710.5
732(36) 0.000772 686. 720.
729(36) 0.000772 685. 725.
722(36) 0.000772 685. 723.
709(35) 0.000816 685.2 715.3
689(35) 0.000816 685.1 705.3
666(34) 0.000865 684.9 696.1
673(34) 0.000865 684.8 691.3
677(34) 0.000865 684.7 689.3
726(36) 0.000772 685. 689.
698(35) 0.000816 684.4 691.4
692(35) 0.000816 684.3 697.5
681(35) 0.000816 684.1 711.8
724(36) 0.000772 684. 739.
738(36) 0.000772 684. 783.
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814(38) 0.000693 684. 875.
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792(37) 0.000730 683. 851.
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760(37) 0.000730 683. 748.
714(35) 0.000816 682.9 714.4
702(35) 0.000816 682.8 696.8
685(35) 0.000816 682.7 689.2
679(34) 0.000865 682.5 686.3
683(35) 0.000816 682.4 685.2
660(34) 0.000865 682.3 684.5
704(35) 0.000816 682.1 684.0
739(36) 0.000772 682. 684.
765(37) 0.000730 682. 683.
650(33) 0.000918 681.7 683.0
642(33) 0.000918 681.6 682.7
682(35) 0.000816 681.5 682.5
690(33) 0.000918 681.3 682.3
681(33) 0.000918 681.2 682.1
694(34) 0.000865 681.1 681.9
648(32) 0.000977 680.9 681.7
683(33) 0.000918 680.8 681.6
695(34) 0.000865 680.7 681.9
699(34) 0.000865 680.5 681.8
668(33) 0.000918 680.4 681.9
672(33) 0.000918 680.3 682.1
688(33) 0.000918 680.1 682.6
684(33) 0.000918 680.0 683.1
698(34) 0.000865 679.9 683.4
706(34) 0.000865 679.7 683.5
680(33) 0.000918 679.6 683.1
690(33) 0.000918 679.5 682.6
682(33) 0.000918 679.3 682.2
673(33) 0.000918 679.2 682.1
670(33) 0.000918 679.1 682.3
688(33) 0.000918 678.9 684.4
702(34) 0.000865 678.8 687.3
721(34) 0.000865 678.7 694.3
707(34) 0.000865 678.5 708.8
706(34) 0.000865 678.4 733.4
778(36) 0.000772 678. 766.
828(37) 0.000730 678. 798.
795(36) 0.000772 678. 813.
820(37) 0.000730 678. 802.
731(34) 0.000865 677.7 772.1
688(33) 0.000918 677.6 738.5
674(33) 0.000918 677.4 713.2
685(33) 0.000918 677.3 699.6
688(33) 0.000918 677.2 695.8
681(33) 0.000918 677.0 701.0
705(34) 0.000865 676.9 719.3
762(35) 0.000816 676.8 760.5
812(37) 0.000730 677. 836.
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992(41) 0.000595 676. 1032.
873(38) 0.000693 676. 911.
802(36) 0.000772 676. 811.
749(35) 0.000816 675.6 751.2
720(34) 0.000865 675.5 726.9
766(35) 0.000816 675.3 732.2
772(36) 0.000772 675. 772.
888(38) 0.000693 675. 869.
1106(43) 0.000541 675. 1050.
1373(48) 0.000434 675. 1315.
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1883(57) 0.0003078 675. 1795.
1888(57) 0.0003078 674. 1778.
1593(52) 0.000370 674. 1556.
1281(47) 0.000453 674. 1255.
976(40) 0.000625 674. 996.
802(36) 0.000772 674. 830.
733(35) 0.000816 673.7 746.3
715(34) 0.000865 673.6 711.0
677(33) 0.000918 673.5 697.3
642(32) 0.000977 673.3 691.6
664(33) 0.000918 673.2 688.5
690(33) 0.000918 673.1 686.5
669(33) 0.000918 672.9 685.1
693(34) 0.000865 672.8 684.2
679(33) 0.000918 672.7 683.6
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659(23) 0.001890 542.9 655.6
636(23) 0.001890 543.4 653.7
626(23) 0.001890 544.0 651.8
654(23) 0.001890 544.5 650.1
654(23) 0.001890 545.1 648.4
639(23) 0.001890 545.7 646.8
626(23) 0.001890 546.2 645.3
643(23) 0.001890 546.8 643.8
653(23) 0.001890 547.4 642.5
681(24) 0.001736 548.0 641.2
684(24) 0.001736 548.6 640.0
647(23) 0.001890 549.2 638.9
625(23) 0.001890 549.8 637.9
626(23) 0.001890 550.4 637.0
652(23) 0.001890 551.0 636.1
679(24) 0.001736 551.6 635.4
672(23) 0.001890 552.2 634.8
638(23) 0.001890 552.9 634.3
621(23) 0.001890 553.5 633.9
618(23) 0.001890 554.1 633.6
606(22) 0.002066 554.8 633.4
598(22) 0.002066 555.4 633.4
618(23) 0.001890 556.1 633.5
632(23) 0.001890 556.7 633.7
625(23) 0.001890 557.4 634.1
618(23) 0.001890 558.0 634.6
627(23) 0.001890 558.7 635.3
622(23) 0.001890 559.4 636.2
612(22) 0.002066 560.0 637.2
614(22) 0.002066 560.7 638.4
648(23) 0.001890 561.4 639.8
635(23) 0.001890 562.1 641.3
630(23) 0.001890 562.8 643.0
662(23) 0.001890 563.5 644.9
681(24) 0.001736 564.2 647.0
681(24) 0.001736 564.9 649.3
665(23) 0.001890 565.6 651.7
645(23) 0.001890 566.3 654.3
647(23) 0.001890 567.0 657.1
645(23) 0.001890 567.7 660.0
644(23) 0.001890 568.5 663.2
670(23) 0.001890 569.2 666.5
681(24) 0.001736 570.0 669.9
671(23) 0.001890 570.7 673.6
678(24) 0.001736 571.4 677.3
673(23) 0.001890 572.2 681.3
667(23) 0.001890 573.0 685.3
691(24) 0.001736 573.7 689.5
719(24) 0.001736 574.5 693.8
739(25) 0.001600 575.3 698.3
743(25) 0.001600 576.1 702.8
707(25) 0.001600 576.8 707.4
695(24) 0.001736 577.6 712.1
733(25) 0.001600 578.4 716.9
744(25) 0.001600 579.2 721.8
753(25) 0.001600 580.0 726.7
729(25) 0.001600 580.8 731.7
701(25) 0.001600 581.7 736.7
747(25) 0.001600 582.5 741.7
744(25) 0.001600 583.3 746.7
767(26) 0.001479 584.1 751.7
769(26) 0.001479 585.0 756.7
744(25) 0.001600 585.8 761.7
747(25) 0.001600 586.7 766.6
761(26) 0.001479 587.5 771.5
748(25) 0.001600 588.4 776.4
770(26) 0.001479 589.2 781.1
761(26) 0.001479 590.1 785.8
745(25) 0.001600 591.0 790.4
744(25) 0.001600 591.9 795.0
774(26) 0.001479 592.8 799.4
807(26) 0.001479 593.7 803.7
814(26) 0.001479 594.5 807.9
818(26) 0.001479 595.5 812.0
822(26) 0.001479 596.4 816.0
812(26) 0.001479 597.3 819.9
821(26) 0.001479 598.2 823.7
833(27) 0.001372 599.1 827.3
823(27) 0.001372 600.0 830.8
819(26) 0.001479 601.0 834.1
827(27) 0.001372 601.9 837.4
810(26) 0.001479 602.9 840.4
834(27) 0.001372 603.8 843.4
852(27) 0.001372 604.8 846.2
838(27) 0.001372 605.8 848.9
839(27) 0.001372 606.7 851.5
850(27) 0.001372 607.7 854.0
840(27) 0.001372 608.7 856.3
843(27) 0.001372 609.7 858.5
901(28) 0.001276 610.7 860.6
861(27) 0.001372 611.7 862.7
867(27) 0.001372 612.7 864.6
835(27) 0.001372 613.7 866.4
858(27) 0.001372 614.7 868.2
873(27) 0.001372 615.7 869.9
910(28) 0.001276 616.8 871.5
901(28) 0.001276 617.8 873.1
863(27) 0.001372 618.8 874.6
936(28) 0.001276 619.9 876.0
893(28) 0.001276 620.9 877.5
905(28) 0.001276 622.0 878.8
856(27) 0.001372 623.1 880.2
912(28) 0.001276 624.1 881.5
918(28) 0.001276 625.2 882.7
881(27) 0.001372 626.3 883.9
882(27) 0.001372 627.4 885.1
932(28) 0.001276 628.5 886.2
896(28) 0.001276 629.6 887.3
891(27) 0.001372 630.7 888.3
899(28) 0.001276 631.8 889.3
910(28) 0.001276 632.9 890.2
904(28) 0.001276 634.1 891.0
905(28) 0.001276 635.2 891.8
913(28) 0.001276 636.4 892.5
923(28) 0.001276 637.5 893.1
894(28) 0.001276 638.7 893.6
891(28) 0.001276 639.8 894.0
901(28) 0.001276 641.0 894.4
880(27) 0.001372 642.2 894.6
886(27) 0.001372 643.3 894.6
902(28) 0.001276 644.5 894.6
888(27) 0.001372 645.7 894.4
912(28) 0.001276 646.9 894.1
929(28) . . .
879(27) . . .
870(27) . . .
937(28) . . .
926(28) . . .
930(28) . . .
927(28) . . .
937(28) . . .
924(28) . . .
908(28) . . .
928(28) . . .
929(28) . . .
929(28) . . .
941(28) . . .
924(28) . . .
912(28) . . .
886(27) . . .
910(28) . . .
966(29) . . .
957(28) . . .
965(29) . . .
966(29) . . .
934(28) . . .
933(28) . . .
943(28) . . .
920(28) . . .
985(42) . . .
961(41) . . .
886(40) . . .
892(40) . . .
931(41) . . .
941(41) . . .
872(39) . . .
917(40) . . .
856(39) . . .
885(40) . . .
865(39) . . .
905(40) . . .
902(40) . . .
921(40) . . .
916(40) . . .
835(39) . . .
912(40) . . .
928(41) . . .
949(41) . . .
947(41) . . .
909(40) . . .
899(40) . . .
891(40) . . .
909(40) . . .
926(41) . . .
883(40) . . .
947(41) . . .
896(40) . . .
891(40) . . .
888(40) . . .
924(41) . . .
953(41) . . .
902(40) . . .
901(40) . . .
879(40) . . .
860(39) . . .
958(41) . . .
947(41) . . .
882(40) . . .
890(40) . . .
948(41) . . .
899(40) . . .
888(40) . . .
896(40) . . .
948(41) . . .
980(42) . . .
921(40) . . .
921(40) . . .
928(41) . . .
897(40) . . .
955(41) . . .
927(41) . . .
951(41) . . .
964(41) . . .
946(41) . . .
915(40) . . .
959(41) . . .
966(41) . . .
973(41) . . .
960(41) . . .
932(41) . . .
974(42) . . .
1011(42) . . .
1022(42) . . .
972(41) . . .
984(42) . . .
1055(43) . . .
969(41) . . .
1032(43) . . .
1032(43) . . .
1037(43) . . .
1057(43) . . .
1032(43) . . .
995(42) . . .
993(42) . . .
1003(42) . . .
1057(43) . . .
1024(42) . . .
1033(43) . . .
1004(42) . . .
1072(43) . . .
1057(43) . . .
1000(42) . . .
1091(44) . . .
1125(44) . . .
1059(43) . . .
1039(43) . . .
1109(44) . . .
1063(43) . . .
1050(43) . . .
1062(43) . . .
1005(42) . . .
1119(44) . . .
1131(44) . . .
1021(42) . . .
988(42) . . .
1015(42) . . .
1074(43) . . .
1089(44) . . .
1135(45) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_cell_measurement_reflns_used    632
_reflns_number_total             632
_reflns_limit_h_min              1
_reflns_limit_h_max              17
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.057
_reflns_d_resolution_low         18.520
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_0P5CO2_publ
_database_code_depnum_ccdc_archive 'CCDC 1582003'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-03-03T19:10|0P5CO2|wendy|bt1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-03-03T19:10

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     39
_refine_ls_goodness_of_fit_all   1.16
_refine_ls_number_restraints     4
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10

_cell_special_details            
; ?
;

_geom_special_details            ?



# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from Z:/queen/Desktop/MBTT series_CO2/CrBTT/BARE_final_NIST/BARE.E'
_cell_length_a                   18.6867(5)
_cell_length_b                   18.6867
_cell_length_c                   18.6867
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6525.2(5)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cr Cr1 0.1322(13) 0.5 0.0 1.0 Uiso 0.00991 12
C C1 0.14846(34) 0.3366(4) -0.14846(34) 1.0 Uiso 0.0132(12) 24
C C2 0.18059(31) 0.2713(4) -0.18059(31) 1.0 Uiso 0.0132(12) 24
C C3 0.24254(31) 0.24254(31) -0.1486(5) 1.0 Uiso 0.0132(12) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.057(7) 3
N N1 0.13009(22) 0.42305(23) -0.07918(22) 1.0 Uiso 0.0139(7) 48
N N2 0.17526(25) 0.36979(23) -0.09004(22) 1.0 Uiso 0.0139(7) 48
H H1 0.2662(6) 0.2662(6) -0.1068(8) 1.0 Uiso 0.016(5) 24
O Os 0.2296(13) 0.5 0.0 0.2353 Uiso 0.00351 12
C Ca 0.2913(13) 0.4399(7) 0.0 0.277(5) Uiso 0.07288 24
O Oa 0.2746(18) 0.5 0.0 0.555(10) Uiso 0.08225 12
O Ob 0.3121(19) 0.3817(11) 0.0 0.277(5) Uiso 0.07411 24

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C26.22 H8 Cl Cr4 N32 O5.38'
_chemical_formula_weight         1100.68
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cr1 Cr1 4.94(5) . 10_555 N
Cr1 Cr1 3.493(33) . 14_555 N
Cr1 Cr1 3.493(33) . 19_555 N
Cr1 Cl1 2.470(24) . 1_555 N
Cr1 N1 2.064(4) . 1_555 N
Cr1 N1 2.064(4) . 4_555 N
Cr1 N1 2.064(4) . 12_565 N
Cr1 N1 2.993(8) . 17_555 N
Cr1 N1 2.993(8) . 19_555 N
Cr1 N1 2.993(8) . 23_565 N
Cr1 N1 2.064(4) . -10_565 N
Cr1 N1 2.993(8) . -14_565 N
Cr1 N2 3.066(7) . 1_555 N
Cr1 N2 3.066(7) . 4_555 N
Cr1 N2 3.066(7) . 12_565 N
Cr1 N2 3.066(7) . -10_565 N
Cr1 Os 1.819(8) . 1_555 N
Cr1 Ca 3.178(29) . 1_555 N
Cr1 Ca 3.178(29) . 12_565 N
Cr1 Oa 2.66(4) . 1_555 N
C1 C2 1.486(11) . 1_555 N
C1 N1 2.098(8) . 1_555 N
C1 N1 2.098(8) . 19_555 N
C1 N2 1.352(6) . 1_555 N
C1 N2 1.352(6) . 19_555 N
C2 C1 1.486(11) . 1_555 N
C2 C3 1.410(6) . 1_555 N
C2 C3 1.410(6) . 7_555 N
C3 C2 1.410(6) . 1_555 N
C3 C2 1.410(6) . 9_555 N
C3 H1 1.001(20) . 1_555 N
Cl1 Cr1 2.470(24) . 1_555 N
Cl1 Cr1 2.470(24) . 10_555 N
Cl1 Cr1 2.470(24) . 14_555 N
Cl1 Cr1 2.470(24) . 19_555 N
N1 Cr1 2.064(4) . 1_555 N
N1 Cr1 2.993(8) . 19_555 N
N1 C1 2.098(8) . 1_555 N
N1 N1 1.345(9) . 19_555 N
N1 N2 1.321(6) . 1_555 N
N2 Cr1 3.066(7) . 1_555 N
N2 C1 1.352(6) . 1_555 N
N2 N1 1.321(6) . 1_555 N
H1 C3 1.001(20) . 1_555 N
Os Cr1 1.819(8) . 1_555 N
Os Ca 1.610(23) . 1_555 N
Os Ca 1.610(23) . 12_565 N
Os Oa 0.84(4) . 1_555 N
Ca Cr1 3.178(29) . 1_555 N
Ca Os 1.610(23) . 1_555 N
Ca Oa 1.166(8) . 1_555 N
Ca Ob 1.156(8) . 1_555 N
Oa Cr1 2.66(4) . 1_555 N
Oa Os 0.84(4) . 1_555 N
Oa Ca 1.166(8) . 1_555 N
Oa Ca 1.166(8) . 12_565 N
Ob Ca 1.156(8) . 1_555 N


loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Cr1 N1 88.9(7) 1_555 . 1_555 N
Cl1 Cr1 N1 88.9(7) 1_555 . 4_555 N
Cl1 Cr1 N1 88.9(7) 1_555 . 12_565 N
Cl1 Cr1 N1 88.9(7) 1_555 . -10_565 N
Cl1 Cr1 Os 180.0 1_555 . 1_555 N
N1 Cr1 N1 91.61(25) 1_555 . 4_555 N
N1 Cr1 N1 177.8(14) 1_555 . 12_565 N
N1 Cr1 N1 88.35(26) 1_555 . -10_565 N
N1 Cr1 Os 91.1(7) 1_555 . 1_555 N
N1 Cr1 N1 88.35(26) 4_555 . 12_565 N
N1 Cr1 N1 177.8(14) 4_555 . -10_565 N
N1 Cr1 Os 91.1(7) 4_555 . 1_555 N
N1 Cr1 N1 91.61(25) 12_565 . -10_565 N
N1 Cr1 Os 91.1(7) 12_565 . 1_555 N
N1 Cr1 Os 91.1(7) -10_565 . 1_555 N
C2 C1 N2 123.6(4) 1_555 . 1_555 N
C2 C1 N2 123.6(4) 1_555 . 19_555 N
N2 C1 N2 112.8(8) 1_555 . 19_555 N
C1 C2 C3 118.3(4) 1_555 . 1_555 N
C1 C2 C3 118.3(4) 1_555 . 7_555 N
C3 C2 C3 123.5(9) 1_555 . 7_555 N
C2 C3 C2 116.5(9) 1_555 . 9_555 N
C2 C3 H1 121.7(4) 1_555 . 1_555 N
C2 C3 H1 121.7(4) 9_555 . 1_555 N
Cr1 Cl1 Cr1 180.0 1_555 . 10_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 19_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 19_555 N
Cr1 Cl1 Cr1 180.0 14_555 . 19_555 N
Cr1 N1 N1 121.4(6) 1_555 . 19_555 N
Cr1 N1 N2 128.5(6) 1_555 . 1_555 N
N1 N1 N2 110.08(27) 19_555 . 1_555 N
C1 N2 N1 103.5(5) 1_555 . 1_555 N
Cr1 Os Ca 135.8(10) 1_555 . 1_555 N
Cr1 Os Ca 135.8(10) 1_555 . 12_565 N
Cr1 Os Oa 180.0 1_555 . 1_555 N
Ca Os Ca 88.5(19) 1_555 . 12_565 N
Ca Os Oa 44.2(10) 1_555 . 1_555 N
Ca Os Oa 44.2(10) 12_565 . 1_555 N
Os Ca Oa 30.2(14) 1_555 . 1_555 N
Os Ca Ob 153.9(22) 1_555 . 1_555 N
Oa Ca Ob 175.8(24) 1_555 . 1_555 N
Os Oa Ca 105.5(18) 1_555 . 1_555 N
Os Oa Ca 105.5(18) 1_555 . 12_565 N
Ca Oa Ca 149(4) 1_555 . 12_565 N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;


# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT602_0P5CO2_publ         
;
PROBLEM: Test for (Unreported) solvent accessible voids        ! Info 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT049_0P5CO2_publ         
;
PROBLEM: Calculated Density less than 1.0 gcm-3 .........     0.8403 Check 
RESPONSE: This is expected as the material is porous.
;

_vrf_PLAT430_0P5CO2_publ         
;
PROBLEM:  Short Inter D...A Contact  Ob     ..  Ob      ..       1.84 Ang. 
RESPONSE: The problem happens because the adsorbed carbon dioxide on the open metal sites are disordered and thus some atoms ostensibly are seemed to be close to each other.
;


# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_cell_measurement_theta_min      4
_cell_measurement_theta_max      160

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Cr 12.0 0.3635 International_Tables_Vol_C
C 78.656 0.6646 International_Tables_Vol_C
Cl 3.0 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 24.0 -0.3739 International_Tables_Vol_C
O 16.135 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.078
_pd_proc_ls_prof_R_factor        0.0288
_pd_proc_ls_prof_wR_factor       0.0333
_pd_proc_ls_prof_wR_expected     0.0289
_refine_ls_R_Fsqd_factor         0.06629

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 10 terms.
 Shifted Chebyshev function of 1st kind
      1:    1119.85     2:   -251.388     3:    313.676     4:   -43.4275    
      5:    156.400     6:   -11.6657     7:    80.6467     8:   -2.92753    
      9:    43.7712    10:  -0.506341    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  593.475 #2(GV)   = -251.867 #3(GW)   =  114.090
 #4(GP)   =    4.877 #5(LX)   =    0.000 #6(LY)   =   17.308
 #7(S/L)  =   0.0449 #8(H/L)  =   0.0356
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2016-03-03T19:10:53
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.5452
_pd_proc_2theta_range_max        166.2952
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
7490(180) 0.0 2437. .
6460(170) 0.0 2428. .
5620(160) 0.0 2418. .
4780(150) 0.0 2409. .
4410(140) 0.0 2399. .
4020(140) 0.0 2390. .
3750(130) 0.0 2381. .
3290(120) 0.0 2372. .
2950(120) 0.0 2363. .
2850(110) 0.0 2354. .
2660(110) 0.0 2345. .
2600(110) 0.0 2336. .
2520(110) 0.0 2327. .
2440(110) 0.0 2318. .
2210(100) 0.0 2310. .
2220(100) 0.0 2301. .
2085(97) 0.0 2292. .
2260(100) 0.0 2284. .
2320(100) 0.0 2275. .
2130(98) 0.0 2267. .
2510(110) 0.0 2258. .
2470(110) 0.0 2250. .
2300(100) 0.0 2242. .
2330(100) 0.0 2234. .
2220(100) 0.0 2225. .
2200(100) 0.0 2217. .
2230(100) 0.0 2209. .
2350(100) 0.0 2201. .
2350(100) 0.0 2193. .
2350(100) 0.0 2185. .
2230(100) 0.0 2177. .
2310(100) 0.0 2170. .
2190(100) 0.0 2162. .
2290(100) 0.0 2154. .
2076(97) 0.0 2147. .
2166(99) 0.0 2139. .
2157(99) 0.0 2131. .
2180(100) 0.0 2124. .
2270(100) 0.0 2117. .
2094(97) 0.0 2109. .
2058(97) 0.0 2102. .
2094(97) 0.0 2094. .
1977(95) 0.0 2087. .
1955(94) 0.0 2080. .
2062(97) 0.0 2073. .
2053(97) 0.0 2066. .
2220(100) 0.0 2059. .
1941(94) 0.0 2052. .
2080(97) 0.0 2045. .
2220(100) 0.0 2038. .
1982(95) 0.0 2031. .
1991(95) 0.0001108 2024. 2028.
2049(96) 0.0001085 2017. 2022.
2134(98) 0.0001041 2011. 2016.
1937(94) 0.0001132 2004. 2011.
2220(100) 0.0001000 1997. 2009.
1977(95) 0.0001108 1991. 2011.
2200(100) 0.0001000 1984. 2019.
2152(99) 0.0001020 1978. 2033.
2270(100) 0.0000980 1971. 2054.
2340(100) 0.0000943 1965. 2080.
2049(96) 0.0001085 1959. 2110.
2350(100) 0.0000943 1952. 2142.
2080(97) 0.0001063 1946. 2178.
2240(100) 0.0000980 1940. 2215.
2220(100) 0.0001000 1934. 2255.
2190(100) 0.0001000 1928. 2297.
2116(98) 0.0001041 1921. 2342.
2460(110) 0.0000890 1915. 2390.
2280(100) 0.0000961 1909. 2441.
2690(110) 0.0000826 1903. 2496.
2630(110) 0.0000842 1898. 2554.
2570(110) 0.0000857 1892. 2617.
2520(110) 0.0000873 1886. 2684.
2700(110) 0.0000812 1880. 2757.
2980(120) 0.0000743 1874. 2835.
2750(110) 0.0000797 1868. 2920.
3050(120) 0.0000731 1863. 3013.
3180(120) 0.0000694 1857. 3114.
3060(120) 0.0000718 1852. 3224.
3270(120) 0.0000672 1846. 3346.
3450(130) 0.0000640 1840. 3480.
3450(130) 0.0000640 1835. 3630.
3830(130) 0.0000574 1830. 3798.
4150(140) 0.0000533 1824. 3989.
4250(140) 0.0000518 1819. 4207.
4420(140) 0.0000503 1813. 4460.
4800(150) 0.0000463 1808. 4759.
5490(160) 0.0000406 1803. 5121.
5980(160) 0.0000372 1798. 5576.
6950(180) 0.0000319 1793. 6172.
7660(190) 0.0000289 1787. 6989.
9230(200) 0.0000240 1782. 8104.
10770(220) 0.0000207 1777. 9497.
12140(230) 0.0000183 1772. 10892.
13060(240) 0.0000171 1767. 11714.
13200(240) 0.0000168 1762. 11353.
11190(220) 0.0000199 1757. 9666.
8550(200) 0.0000260 1752. 7219.
5760(160) 0.0000386 1748. 4887.
3821(90) 0.0001235 1743. 3241.
2514(73) 0.0001877 1738. 2343.
2021(65) 0.0002367 1733. 1954.
1817(62) 0.0002601 1728. 1815.
1732(61) 0.0002687 1724. 1770.
1669(59) 0.0002873 1719. 1752.
1722(60) 0.0002778 1715. 1741.
1743(61) 0.0002687 1710. 1732.
1760(61) 0.0002687 1705. 1725.
1634(59) 0.0002873 1701. 1718.
1690(60) 0.0002778 1696. 1711.
1668(59) 0.0002873 1692. 1705.
1614(58) 0.0002973 1688. 1699.
1601(58) 0.0002973 1683. 1694.
1570(58) 0.0002973 1679. 1688.
1680(60) 0.0002778 1675. 1689.
1647(59) 0.0002873 1670. 1685.
1528(57) 0.0003078 1666. 1680.
1698(60) 0.0002778 1662. 1670.
1712(60) 0.0002778 1658. 1666.
1716(60) 0.0002778 1653. 1664.
1589(58) 0.0002973 1649. 1663.
1693(60) 0.0002778 1645. 1667.
1698(60) 0.0002778 1641. 1678.
1697(60) 0.0002778 1637. 1700.
1780(61) 0.0002687 1633. 1736.
1824(62) 0.0002601 1629. 1786.
1901(63) 0.0002520 1625. 1849.
1965(64) 0.0002441 1621. 1922.
2054(66) 0.0002296 1617. 2004.
2083(66) 0.0002296 1614. 2094.
2214(68) 0.0002163 1610. 2192.
2181(68) 0.0002163 1606. 2299.
2315(70) 0.0002041 1602. 2418.
2338(70) 0.0002041 1598. 2548.
2631(75) 0.0001778 1595. 2694.
2614(75) 0.0001778 1591. 2857.
2748(76) 0.0001731 1587. 3041.
3034(80) 0.0001562 1584. 3252.
3278(84) 0.0001417 1580. 3496.
3518(87) 0.0001321 1577. 3785.
3993(92) 0.0001181 1573. 4134.
4374(97) 0.0001063 1569. 4571.
4800(100) 0.0000980 1566. 5147.
5900(110) 0.0000797 1563. 5937.
7160(120) 0.0000650 1559. 7017.
8410(130) 0.0000557 1556. 8369.
9710(140) 0.0000482 1552. 9719.
10210(150) 0.0000457 1549. 10508.
9990(150) 0.0000469 1546. 10157.
8510(140) 0.0000549 1542. 8560.
6300(120) 0.0000743 1539. 6304.
4077(93) 0.0001156 1536. 4217.
2637(75) 0.0001778 1532. 2790.
1989(65) 0.0002367 1529. 2036.
1608(58) 0.0002973 1526. 1727.
1507(56) 0.0003189 1523. 1616.
1556(57) 0.0003078 1520. 1579.
1465(56) 0.0003189 1517. 1564.
1501(56) 0.0003189 1514. 1555.
1551(57) 0.0003078 1511. 1548.
1525(57) 0.0003078 1507. 1542.
1479(56) 0.0003189 1504. 1537.
1599(58) 0.0002973 1501. 1533.
1618(58) 0.0002973 1499. 1529.
1576(58) 0.0002973 1496. 1527.
1592(58) 0.0002973 1493. 1526.
1614(58) 0.0002973 1490. 1529.
1573(58) 0.0002973 1487. 1540.
1791(61) 0.0002687 1484. 1567.
1774(61) 0.0002687 1481. 1615.
1848(62) 0.0002601 1478. 1690.
1986(65) 0.0002367 1476. 1795.
2018(65) 0.0002367 1473. 1926.
2122(67) 0.0002228 1470. 2079.
2309(70) 0.0002041 1467. 2254.
2478(73) 0.0001877 1465. 2446.
2517(73) 0.0001877 1462. 2668.
2745(76) 0.0001731 1459. 2920.
3041(80) 0.0001562 1457. 3209.
3430(85) 0.0001384 1454. 3545.
3722(89) 0.0001262 1451. 3944.
4142(94) 0.0001132 1449. 4431.
4750(100) 0.0000980 1446. 5049.
5680(110) 0.0000826 1444. 5873.
7090(120) 0.0000661 1441. 7012.
8430(130) 0.0000557 1439. 8547.
10480(150) 0.0000444 1436. 10377.
11770(160) 0.0000396 1434. 12025.
12410(160) 0.0000376 1431. 12693.
11460(160) 0.0000406 1429. 11749.
8940(140) 0.0000525 1427. 9352.
6160(120) 0.0000756 1424. 6468.
4060(93) 0.0001156 1422. 4083.
2656(75) 0.0001778 1420. 2603.
1761(61) 0.0002687 1417. 1886.
1460(75) 0.0001778 1415. 1607.
1419(74) 0.0001826 1413. 1512.
1368(73) 0.0001877 1410. 1478.
1465(76) 0.0001731 1408. 1462.
1501(56) 0.0003189 1406. 1451.
1396(54) 0.0003429 1404. 1442.
1355(53) 0.000356 1401. 1434.
1389(54) 0.0003429 1399. 1428.
1343(53) 0.000356 1397. 1422.
1362(53) 0.000356 1395. 1417.
1358(53) 0.000356 1393. 1413.
1430(54) 0.0003429 1391. 1409.
1435(54) 0.0003429 1389. 1405.
1376(53) 0.000356 1387. 1402.
1377(53) 0.000356 1385. 1400.
1396(54) 0.0003429 1383. 1397.
1437(55) 0.0003306 1380. 1395.
1382(53) 0.000356 1378. 1393.
1382(53) 0.000356 1377. 1391.
1397(54) 0.0003429 1375. 1389.
1398(54) 0.0003429 1373. 1388.
1388(54) 0.0003429 1371. 1380.
1477(55) 0.0003306 1369. 1380.
1488(56) 0.0003189 1367. 1381.
1449(55) 0.0003306 1365. 1384.
1446(55) 0.0003306 1363. 1387.
1433(54) 0.0003429 1361. 1391.
1493(56) 0.0003189 1359. 1393.
1451(55) 0.0003306 1358. 1390.
1479(55) 0.0003306 1356. 1382.
1356(53) 0.000356 1354. 1372.
1349(53) 0.000356 1352. 1362.
1390(54) 0.0003429 1350. 1355.
1359(53) 0.000356 1349. 1351.
1305(52) 0.000370 1347. 1348.
1280(51) 0.000384 1345. 1346.
1330(52) 0.000370 1343. 1344.
1317(52) 0.000370 1342. 1342.
1354(53) 0.000356 1340. 1340.
1330(52) 0.000370 1338. 1339.
1352(53) 0.000356 1337. 1337.
1333(52) 0.000370 1335. 1335.
1323(52) 0.000370 1333. 1334.
1357(53) 0.000356 1332. 1333.
1324(52) 0.000370 1330. 1331.
1310(52) 0.000370 1329. 1330.
1282(51) 0.000384 1327. 1330.
1358(53) 0.000356 1325. 1329.
1409(54) 0.0003429 1324. 1329.
1317(52) 0.000370 1322. 1329.
1347(53) 0.000356 1321. 1329.
1364(53) 0.000356 1319. 1330.
1359(53) 0.000356 1318. 1331.
1273(51) 0.000384 1316. 1334.
1303(52) 0.000370 1315. 1338.
1325(52) 0.000370 1313. 1343.
1349(53) 0.000356 1312. 1350.
1357(53) 0.000356 1311. 1355.
1404(54) 0.0003429 1309. 1354.
1374(53) 0.000356 1308. 1347.
1301(52) 0.000370 1306. 1334.
1316(52) 0.000370 1305. 1322.
1330(52) 0.000370 1304. 1312.
1335(53) 0.000356 1302. 1306.
1306(52) 0.000370 1301. 1303.
1345(53) 0.000356 1300. 1301.
1327(52) 0.000370 1298. 1299.
1300(52) 0.000370 1297. 1298.
1287(51) 0.000384 1296. 1297.
1273(51) 0.000384 1294. 1296.
1278(51) 0.000384 1293. 1295.
1276(51) 0.000384 1292. 1295.
1261(51) 0.000384 1290. 1297.
1328(52) 0.000370 1289. 1299.
1297(52) 0.000370 1288. 1304.
1354(53) 0.000356 1287. 1311.
1311(52) 0.000370 1285. 1320.
1328(52) 0.000370 1284. 1331.
1368(53) 0.000356 1283. 1345.
1326(52) 0.000370 1282. 1363.
1500(56) 0.0003189 1281. 1387.
1366(53) 0.000356 1279. 1421.
1507(56) 0.0003189 1278. 1468.
1533(56) 0.0003189 1277. 1525.
1622(58) 0.0002973 1276. 1579.
1589(57) 0.0003078 1275. 1606.
1612(58) 0.0002973 1274. 1584.
1558(57) 0.0003078 1273. 1514.
1411(54) 0.0003429 1272. 1427.
1297(52) 0.000370 1270. 1354.
1213(50) 0.000400 1269. 1307.
1242(51) 0.000384 1268. 1284.
1293(52) 0.000370 1267. 1274.
1275(51) 0.000384 1266. 1270.
1260(51) 0.000384 1265. 1269.
1196(50) 0.000400 1264. 1267.
1224(50) 0.000400 1263. 1266.
1257(51) 0.000384 1262. 1264.
1313(52) 0.000370 1261. 1263.
1287(52) 0.000370 1260. 1262.
1253(74) 0.0001826 1259. 1261.
1357(52) 0.000370 1258. 1260.
1260(50) 0.000400 1257. 1259.
1250(50) 0.000400 1256. 1258.
1346(52) 0.000370 1255. 1257.
1251(50) 0.000400 1254. 1256.
1261(50) 0.000400 1253. 1255.
1243(50) 0.000400 1252. 1254.
1243(50) 0.000400 1251. 1254.
1258(50) 0.000400 1250. 1253.
1233(50) 0.000400 1249. 1252.
1251(50) 0.000400 1249. 1251.
1318(51) 0.000384 1248. 1251.
1326(52) 0.000370 1247. 1250.
1339(52) 0.000370 1246. 1249.
1272(51) 0.000384 1245. 1249.
1254(50) 0.000400 1244. 1248.
1277(51) 0.000384 1243. 1250.
1324(52) 0.000370 1242. 1250.
1348(52) 0.000370 1241. 1250.
1296(51) 0.000384 1241. 1251.
1210(49) 0.000416 1240. 1255.
1288(51) 0.000384 1239. 1263.
1322(52) 0.000370 1238. 1277.
1297(51) 0.000384 1237. 1302.
1426(54) 0.0003429 1236. 1337.
1420(53) 0.000356 1236. 1386.
1401(53) 0.000356 1235. 1449.
1535(56) 0.0003189 1234. 1531.
1644(58) 0.0002973 1233. 1642.
1862(61) 0.0002687 1233. 1796.
2060(65) 0.0002367 1232. 2004.
2260(68) 0.0002163 1231. 2250.
2644(73) 0.0001877 1230. 2471.
2564(72) 0.0001929 1229. 2563.
2442(70) 0.0002041 1229. 2446.
2091(65) 0.0002367 1228. 2150.
1775(60) 0.0002778 1227. 1807.
1562(56) 0.0003189 1226. 1534.
1346(52) 0.000370 1226. 1370.
1218(49) 0.000416 1225. 1294.
1248(50) 0.000400 1224. 1265.
1257(50) 0.000400 1224. 1257.
1301(51) 0.000384 1223. 1259.
1307(51) 0.000384 1222. 1268.
1329(52) 0.000370 1222. 1290.
1426(54) 0.0003429 1221. 1331.
1448(54) 0.0003429 1220. 1399.
1447(54) 0.0003429 1219. 1499.
1585(57) 0.0003078 1219. 1636.
1772(60) 0.0002778 1218. 1819.
1918(62) 0.0002601 1217. 2068.
2376(69) 0.0002100 1217. 2412.
2698(74) 0.0001826 1216. 2881.
3332(82) 0.0001487 1216. 3454.
3818(88) 0.0001291 1215. 4001.
3990(90) 0.0001235 1214. 4288.
3682(87) 0.0001321 1214. 4103.
2997(78) 0.0001644 1213. 3469.
2353(69) 0.0002100 1212. 2668.
1884(62) 0.0002601 1212. 1996.
1484(55) 0.0003306 1211. 1575.
1265(50) 0.000400 1211. 1369.
1237(50) 0.000400 1210. 1286.
1249(50) 0.000400 1209. 1255.
1284(51) 0.000384 1209. 1243.
1256(50) 0.000400 1208. 1237.
1293(51) 0.000384 1208. 1232.
1227(50) 0.000400 1207. 1228.
1200(49) 0.000416 1206. 1225.
1215(49) 0.000416 1206. 1223.
1212(49) 0.000416 1205. 1221.
1207(49) 0.000416 1205. 1219.
1154(48) 0.000434 1204. 1218.
1231(50) 0.000400 1204. 1217.
1204(49) 0.000416 1203. 1216.
1218(49) 0.000416 1202. 1216.
1165(48) 0.000434 1202. 1216.
1157(48) 0.000434 1201. 1216.
1264(50) 0.000400 1201. 1216.
1161(48) 0.000434 1200. 1216.
1264(50) 0.000400 1200. 1217.
1126(47) 0.000453 1199. 1218.
1157(48) 0.000434 1199. 1219.
1224(50) 0.000400 1198. 1222.
1256(50) 0.000400 1198. 1229.
1320(52) 0.000370 1197. 1242.
1314(51) 0.000384 1197. 1268.
1369(52) 0.000370 1196. 1318.
1440(54) 0.0003429 1196. 1399.
1533(56) 0.0003189 1195. 1520.
1817(61) 0.0002687 1195. 1696.
2044(64) 0.0002441 1194. 1943.
2406(70) 0.0002041 1194. 2290.
2893(77) 0.0001687 1193. 2762.
3504(85) 0.0001384 1193. 3339.
4014(91) 0.0001208 1192. 3890.
4137(92) 0.0001181 1192. 4184.
3998(90) 0.0001235 1191. 4012.
3373(83) 0.0001452 1191. 3395.
2528(68) 0.0002163 1190. 2616.
1916(59) 0.0002873 1190. 1963.
1497(52) 0.000370 1189. 1552.
1301(48) 0.000434 1189. 1350.
1249(47) 0.000453 1188. 1269.
1240(47) 0.000453 1188. 1241.
1249(47) 0.000453 1187. 1234.
1242(47) 0.000453 1187. 1236.
1204(47) 0.000453 1187. 1248.
1299(48) 0.000434 1186. 1271.
1273(48) 0.000434 1186. 1308.
1326(49) 0.000416 1185. 1362.
1391(50) 0.000400 1185. 1441.
1526(53) 0.000356 1184. 1551.
1734(56) 0.0003189 1184. 1688.
1838(58) 0.0002973 1183. 1825.
1982(60) 0.0002778 1183. 1909.
1989(60) 0.0002778 1183. 1884.
1822(58) 0.0002973 1182. 1746.
1555(53) 0.000356 1182. 1558.
1459(51) 0.000384 1181. 1393.
1330(49) 0.000416 1181. 1285.
1263(48) 0.000434 1181. 1230.
1221(47) 0.000453 1180. 1207.
1211(47) 0.000453 1180. 1198.
1206(47) 0.000453 1179. 1196.
1199(46) 0.000473 1179. 1197.
1223(47) 0.000453 1178. 1201.
1193(46) 0.000473 1178. 1209.
1193(46) 0.000473 1178. 1221.
1243(47) 0.000453 1177. 1240.
1270(48) 0.000434 1177. 1267.
1343(49) 0.000416 1176. 1303.
1417(51) 0.000384 1176. 1344.
1394(50) 0.000400 1176. 1375.
1429(51) 0.000384 1175. 1381.
1384(50) 0.000400 1175. 1354.
1356(50) 0.000400 1174. 1302.
1284(48) 0.000434 1174. 1251.
1229(47) 0.000453 1174. 1214.
1213(47) 0.000453 1173. 1193.
1240(47) 0.000453 1173. 1183.
1191(46) 0.000473 1173. 1180.
1134(45) 0.000494 1172. 1179.
1208(47) 0.000453 1172. 1181.
1158(46) 0.000473 1171. 1184.
1189(46) 0.000473 1171. 1190.
1173(46) 0.000473 1171. 1202.
1219(47) 0.000453 1170. 1217.
1197(46) 0.000473 1170. 1238.
1193(46) 0.000473 1170. 1264.
1199(46) 0.000473 1169. 1292.
1220(47) 0.000453 1169. 1311.
1202(47) 0.000453 1168. 1309.
1211(47) 0.000453 1168. 1285.
1272(48) 0.000434 1168. 1248.
1191(46) 0.000473 1167. 1215.
1237(47) 0.000453 1167. 1192.
1129(45) 0.000494 1167. 1181.
1174(46) 0.000473 1166. 1175.
1205(47) 0.000453 1166. 1173.
1259(48) 0.000434 1166. 1173.
1178(46) 0.000473 1165. 1172.
1157(46) 0.000473 1165. 1173.
1186(46) 0.000473 1165. 1174.
1200(47) 0.000453 1164. 1174.
1172(46) 0.000473 1164. 1174.
1152(46) 0.000473 1163. 1175.
1180(46) 0.000473 1163. 1175.
1160(46) 0.000473 1163. 1176.
1154(46) 0.000473 1162. 1177.
1191(46) 0.000473 1162. 1179.
1266(48) 0.000434 1162. 1181.
1272(48) 0.000434 1161. 1184.
1258(48) 0.000434 1161. 1188.
1251(48) 0.000434 1161. 1194.
1228(47) 0.000453 1160. 1205.
1309(49) 0.000416 1160. 1229.
1366(50) 0.000400 1160. 1274.
1462(51) 0.000384 1159. 1358.
1495(52) 0.000370 1159. 1500.
1818(57) 0.0003078 1159. 1724.
2082(62) 0.0002601 1158. 2059.
2517(68) 0.0002163 1158. 2524.
2987(74) 0.0001826 1158. 3089.
3576(81) 0.0001524 1157. 3622.
4009(86) 0.0001352 1157. 3907.
3804(84) 0.0001417 1157. 3754.
3275(77) 0.0001687 1156. 3190.
2565(68) 0.0002163 1156. 2484.
1860(58) 0.0002973 1156. 1893.
1597(54) 0.0003429 1155. 1522.
1505(52) 0.000370 1155. 1340.
1272(48) 0.000434 1155. 1274.
1214(47) 0.000453 1154. 1268.
1288(48) 0.000434 1154. 1302.
1427(51) 0.000384 1154. 1376.
1621(54) 0.0003429 1153. 1504.
1840(58) 0.0002973 1153. 1702.
1999(60) 0.0002778 1153. 1985.
2410(66) 0.0002296 1152. 2337.
2958(73) 0.0001877 1152. 2682.
3117(75) 0.0001778 1152. 2886.
3077(75) 0.0001778 1151. 2821.
2704(70) 0.0002041 1151. 2489.
2169(63) 0.0002520 1151. 2047.
1767(57) 0.0003078 1150. 1663.
1434(51) 0.000384 1150. 1414.
1302(48) 0.000434 1150. 1290.
1228(47) 0.000453 1149. 1244.
1312(49) 0.000416 1149. 1244.
1300(48) 0.000434 1149. 1275.
1361(50) 0.000400 1148. 1340.
1374(50) 0.000400 1148. 1451.
1598(54) 0.0003429 1148. 1622.
1800(57) 0.0003078 1147. 1857.
2159(63) 0.0002520 1147. 2130.
2350(65) 0.0002367 1147. 2369.
2411(66) 0.0002296 1146. 2465.
2330(65) 0.0002367 1146. 2344.
2042(61) 0.0002687 1146. 2053.
1768(57) 0.0003078 1145. 1727.
1498(52) 0.000370 1145. 1472.
1304(49) 0.000416 1145. 1323.
1266(48) 0.000434 1144. 1261.
1311(49) 0.000416 1144. 1257.
1310(49) 0.000416 1144. 1297.
1407(50) 0.000400 1143. 1392.
1623(54) 0.0003429 1143. 1557.
1746(56) 0.0003189 1143. 1820.
2145(62) 0.0002601 1142. 2195.
2620(69) 0.0002100 1142. 2655.
3139(76) 0.0001731 1142. 3095.
3416(79) 0.0001602 1141. 3339.
3296(78) 0.0001644 1141. 3233.
2862(72) 0.0001929 1141. 2795.
2386(66) 0.0002296 1141. 2233.
1878(58) 0.0002973 1140. 1753.
1468(52) 0.000370 1140. 1443.
1297(48) 0.000434 1140. 1284.
1132(45) 0.000494 1139. 1215.
1146(45) 0.000494 1139. 1189.
1179(46) 0.000473 1139. 1178.
1206(47) 0.000453 1138. 1174.
1227(47) 0.000453 1138. 1175.
1144(45) 0.000494 1138. 1180.
1159(46) 0.000473 1137. 1186.
1203(47) 0.000453 1137. 1193.
1232(47) 0.000453 1137. 1195.
1199(47) 0.000453 1136. 1190.
1162(46) 0.000473 1136. 1179.
1142(45) 0.000494 1136. 1166.
1197(46) 0.000473 1135. 1156.
1170(46) 0.000473 1135. 1149.
1118(45) 0.000494 1135. 1145.
1122(45) 0.000494 1134. 1143.
1162(46) 0.000473 1134. 1142.
1133(45) 0.000494 1134. 1141.
1081(44) 0.000517 1133. 1142.
1157(46) 0.000473 1133. 1144.
1125(45) 0.000494 1133. 1147.
1139(45) 0.000494 1132. 1150.
1145(45) 0.000494 1132. 1152.
1168(46) 0.000473 1132. 1152.
1186(46) 0.000473 1131. 1150.
1154(46) 0.000473 1131. 1145.
1143(45) 0.000494 1131. 1141.
1105(45) 0.000494 1130. 1138.
1165(46) 0.000473 1130. 1136.
1097(44) 0.000517 1130. 1136.
1066(44) 0.000517 1129. 1138.
1104(45) 0.000494 1129. 1143.
1161(46) 0.000473 1129. 1152.
1168(46) 0.000473 1128. 1166.
1145(45) 0.000494 1128. 1186.
1187(46) 0.000473 1128. 1208.
1202(47) 0.000453 1127. 1227.
1175(46) 0.000473 1127. 1234.
1170(46) 0.000473 1127. 1223.
1164(46) 0.000473 1126. 1197.
1152(46) 0.000473 1126. 1171.
1101(45) 0.000494 1126. 1150.
1103(45) 0.000494 1125. 1137.
1171(46) 0.000473 1125. 1131.
1072(44) 0.000517 1125. 1128.
1117(45) 0.000494 1124. 1127.
1142(45) 0.000494 1124. 1126.
1144(45) 0.000494 1124. 1126.
1136(45) 0.000494 1123. 1125.
1188(46) 0.000473 1123. 1125.
1160(46) 0.000473 1123. 1125.
1117(45) 0.000494 1122. 1124.
1135(45) 0.000494 1122. 1124.
1138(45) 0.000494 1122. 1123.
1223(47) 0.000453 1121. 1123.
1127(45) 0.000494 1121. 1123.
1106(45) 0.000494 1121. 1123.
1035(43) 0.000541 1120. 1122.
1112(45) 0.000494 1120. 1123.
1183(46) 0.000473 1120. 1123.
1154(44) 0.000517 1119. 1123.
1169(44) 0.000517 1119. 1123.
1180(44) 0.000517 1119. 1123.
1211(45) 0.000494 1118. 1123.
1128(43) 0.000541 1118. 1123.
1112(43) 0.000541 1118. 1124.
1111(43) 0.000541 1117. 1124.
1143(44) 0.000517 1117. 1124.
1145(44) 0.000517 1116. 1124.
1130(44) 0.000517 1116. 1125.
1130(43) 0.000541 1116. 1128.
1109(43) 0.000541 1115. 1133.
1112(43) 0.000541 1115. 1144.
1150(44) 0.000517 1115. 1163.
1170(44) 0.000517 1114. 1194.
1229(45) 0.000494 1114. 1237.
1304(47) 0.000453 1114. 1286.
1362(48) 0.000434 1113. 1327.
1337(47) 0.000453 1113. 1342.
1330(47) 0.000453 1113. 1321.
1250(46) 0.000473 1112. 1273.
1214(45) 0.000494 1112. 1222.
1191(45) 0.000494 1112. 1184.
1160(44) 0.000517 1111. 1168.
1113(43) 0.000541 1111. 1173.
1178(44) 0.000517 1111. 1204.
1244(46) 0.000473 1110. 1267.
1299(47) 0.000453 1110. 1374.
1491(50) 0.000400 1110. 1528.
1694(54) 0.0003429 1109. 1711.
1820(56) 0.0003189 1109. 1874.
1970(58) 0.0002973 1108. 1948.
1912(57) 0.0003078 1108. 1887.
1723(54) 0.0003429 1108. 1716.
1427(49) 0.000416 1107. 1516.
1300(47) 0.000453 1107. 1357.
1272(46) 0.000473 1107. 1267.
1281(46) 0.000473 1106. 1247.
1349(48) 0.000434 1106. 1293.
1494(50) 0.000400 1106. 1412.
1707(54) 0.0003429 1105. 1620.
2016(58) 0.0002973 1105. 1918.
2477(65) 0.0002367 1105. 2268.
2796(69) 0.0002100 1104. 2569.
2988(71) 0.0001984 1104. 2692.
2818(69) 0.0002100 1103. 2553.
2407(64) 0.0002441 1103. 2210.
1959(57) 0.0003078 1103. 1820.
1521(51) 0.000384 1102. 1506.
1335(47) 0.000453 1102. 1309.
1195(45) 0.000494 1102. 1207.
1199(45) 0.000494 1101. 1162.
1185(45) 0.000494 1101. 1143.
1134(44) 0.000517 1101. 1135.
1096(43) 0.000541 1100. 1130.
1124(43) 0.000541 1100. 1127.
1110(43) 0.000541 1099. 1125.
1088(43) 0.000541 1099. 1123.
1122(43) 0.000541 1099. 1123.
1163(44) 0.000517 1098. 1123.
1093(43) 0.000541 1098. 1125.
1090(43) 0.000541 1098. 1131.
1169(44) 0.000517 1097. 1145.
1133(44) 0.000517 1097. 1173.
1172(44) 0.000517 1097. 1228.
1326(47) 0.000453 1096. 1321.
1482(50) 0.000400 1096. 1460.
1662(53) 0.000356 1095. 1630.
1750(54) 0.0003429 1095. 1788.
1777(55) 0.0003306 1095. 1872.
1761(55) 0.0003306 1094. 1833.
1646(53) 0.000356 1094. 1683.
1478(50) 0.000400 1094. 1494.
1321(47) 0.000453 1093. 1332.
1232(45) 0.000494 1093. 1226.
1219(45) 0.000494 1093. 1174.
1224(45) 0.000494 1092. 1162.
1178(44) 0.000517 1092. 1175.
1147(44) 0.000517 1091. 1210.
1144(44) 0.000517 1091. 1259.
1236(46) 0.000473 1091. 1311.
1301(47) 0.000453 1090. 1346.
1357(48) 0.000434 1090. 1346.
1276(46) 0.000473 1090. 1307.
1203(45) 0.000494 1089. 1247.
1101(43) 0.000541 1089. 1190.
1088(43) 0.000541 1088. 1150.
1149(44) 0.000517 1088. 1126.
1080(43) 0.000541 1088. 1115.
1064(42) 0.000567 1087. 1111.
1094(43) 0.000541 1087. 1109.
1071(42) 0.000567 1087. 1109.
1029(41) 0.000595 1086. 1110.
1056(42) 0.000567 1086. 1111.
1060(42) 0.000567 1085. 1114.
1073(42) 0.000567 1085. 1118.
1138(44) 0.000517 1085. 1125.
1133(44) 0.000517 1084. 1137.
1133(44) 0.000517 1084. 1163.
1211(45) 0.000494 1084. 1217.
1342(37) 0.000730 1083. 1324.
1581(48) 0.000434 1083. 1519.
1898(52) 0.000370 1082. 1826.
2258(57) 0.0003078 1082. 2234.
2663(62) 0.0002601 1082. 2666.
2876(65) 0.0002367 1081. 2975.
2851(64) 0.0002441 1081. 3012.
2572(61) 0.0002687 1081. 2736.
2199(56) 0.0003189 1080. 2281.
1778(51) 0.000384 1080. 1831.
1465(46) 0.000473 1079. 1500.
1287(43) 0.000541 1079. 1305.
1163(41) 0.000595 1079. 1217.
1113(40) 0.000625 1078. 1194.
1195(41) 0.000595 1078. 1207.
1220(42) 0.000567 1078. 1238.
1218(42) 0.000567 1077. 1273.
1275(43) 0.000541 1077. 1295.
1328(44) 0.000517 1076. 1289.
1290(43) 0.000541 1076. 1256.
1226(42) 0.000567 1076. 1211.
1192(41) 0.000595 1075. 1173.
1135(40) 0.000625 1075. 1154.
1138(40) 0.000625 1075. 1160.
1216(42) 0.000567 1074. 1197.
1269(43) 0.000541 1074. 1270.
1340(44) 0.000517 1073. 1380.
1442(46) 0.000473 1073. 1509.
1600(48) 0.000434 1073. 1622.
1709(50) 0.000400 1072. 1671.
1642(49) 0.000416 1072. 1626.
1451(46) 0.000473 1072. 1507.
1354(44) 0.000517 1071. 1369.
1245(42) 0.000567 1071. 1258.
1164(41) 0.000595 1070. 1194.
1191(41) 0.000595 1070. 1180.
1219(42) 0.000567 1070. 1209.
1265(43) 0.000541 1069. 1277.
1419(45) 0.000494 1069. 1373.
1504(47) 0.000453 1068. 1473.
1606(48) 0.000434 1068. 1541.
1599(48) 0.000434 1068. 1541.
1508(47) 0.000453 1067. 1468.
1407(45) 0.000494 1067. 1357.
1273(43) 0.000541 1067. 1250.
1192(41) 0.000595 1066. 1172.
1147(41) 0.000595 1066. 1127.
1098(40) 0.000625 1065. 1106.
1118(40) 0.000625 1065. 1102.
1155(41) 0.000595 1065. 1105.
1140(40) 0.000625 1064. 1113.
1184(41) 0.000595 1064. 1119.
1160(41) 0.000595 1064. 1119.
1169(41) 0.000595 1063. 1113.
1141(40) 0.000625 1063. 1102.
1058(39) 0.000657 1062. 1091.
1098(40) 0.000625 1062. 1081.
1071(39) 0.000657 1062. 1076.
1044(39) 0.000657 1061. 1074.
1079(39) 0.000657 1061. 1075.
1099(40) 0.000625 1060. 1079.
1052(39) 0.000657 1060. 1083.
1069(39) 0.000657 1060. 1087.
1113(40) 0.000625 1059. 1089.
1085(39) 0.000657 1059. 1087.
1034(38) 0.000693 1059. 1083.
1050(39) 0.000657 1058. 1079.
1083(39) 0.000657 1058. 1078.
1083(39) 0.000657 1057. 1082.
1100(40) 0.000625 1057. 1094.
1132(40) 0.000625 1057. 1118.
1119(40) 0.000625 1056. 1153.
1206(42) 0.000567 1056. 1195.
1229(42) 0.000567 1056. 1233.
1274(43) 0.000541 1055. 1252.
1227(42) 0.000567 1055. 1240.
1187(41) 0.000595 1054. 1202.
1120(40) 0.000625 1054. 1156.
1087(39) 0.000657 1054. 1116.
1036(39) 0.000657 1053. 1089.
1084(39) 0.000657 1053. 1073.
1118(40) 0.000625 1053. 1065.
1072(39) 0.000657 1052. 1061.
1031(38) 0.000693 1052. 1060.
1045(39) 0.000657 1051. 1059.
1030(38) 0.000693 1051. 1058.
1059(39) 0.000657 1051. 1058.
1014(38) 0.000693 1050. 1058.
1022(38) 0.000693 1050. 1058.
1062(39) 0.000657 1049. 1060.
1065(39) 0.000657 1049. 1063.
1163(41) 0.000595 1049. 1068.
1093(40) 0.000625 1048. 1078.
1102(40) 0.000625 1048. 1092.
1122(40) 0.000625 1048. 1107.
1167(41) 0.000595 1047. 1120.
1143(40) 0.000625 1047. 1126.
1120(40) 0.000625 1046. 1122.
1094(40) 0.000625 1046. 1112.
1098(40) 0.000625 1046. 1104.
1147(38) 0.000693 1045. 1109.
1163(39) 0.000657 1045. 1134.
1210(40) 0.000625 1045. 1190.
1340(42) 0.000567 1044. 1284.
1459(43) 0.000541 1044. 1409.
1542(45) 0.000494 1043. 1540.
1719(47) 0.000453 1043. 1633.
1759(48) 0.000434 1043. 1645.
1511(44) 0.000517 1042. 1566.
1449(43) 0.000541 1042. 1434.
1336(42) 0.000567 1042. 1303.
1187(39) 0.000657 1041. 1206.
1127(38) 0.000693 1041. 1155.
1135(38) 0.000693 1041. 1147.
1182(39) 0.000657 1040. 1170.
1220(40) 0.000625 1040. 1211.
1161(39) 0.000657 1039. 1252.
1231(40) 0.000625 1039. 1273.
1224(40) 0.000625 1039. 1262.
1230(40) 0.000625 1038. 1221.
1123(38) 0.000693 1038. 1169.
1127(38) 0.000693 1038. 1122.
1111(38) 0.000693 1037. 1089.
1096(38) 0.000693 1037. 1070.
1073(37) 0.000730 1036. 1062.
1076(37) 0.000730 1036. 1060.
1058(37) 0.000730 1036. 1061.
1048(37) 0.000730 1035. 1062.
1020(36) 0.000772 1035. 1062.
1051(37) 0.000730 1035. 1060.
1066(37) 0.000730 1034. 1056.
1043(37) 0.000730 1034. 1053.
1032(36) 0.000772 1034. 1053.
1059(37) 0.000730 1033. 1056.
1084(37) 0.000730 1033. 1063.
1068(37) 0.000730 1032. 1075.
1086(37) 0.000730 1032. 1089.
1070(37) 0.000730 1032. 1102.
1104(38) 0.000693 1031. 1109.
1122(38) 0.000693 1031. 1108.
1102(38) 0.000693 1031. 1101.
1120(38) 0.000693 1030. 1096.
1084(37) 0.000730 1030. 1104.
1122(38) 0.000693 1030. 1136.
1204(39) 0.000657 1029. 1201.
1321(41) 0.000595 1029. 1302.
1545(45) 0.000494 1028. 1430.
1704(47) 0.000453 1028. 1554.
1733(47) 0.000453 1028. 1629.
1642(46) 0.000473 1027. 1618.
1549(45) 0.000494 1027. 1523.
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1713(47) 0.000453 1011. 1750.
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1160(32) 0.000977 942.5 1216.7
1207(33) 0.000918 942.5 1279.8
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1236(46) 0.000473 942. 1372.
1262(32) 0.000977 942.4 1373.8
1274(32) 0.000977 942.3 1342.0
1294(32) 0.000977 942.3 1288.2
1216(31) 0.001041 942.3 1227.6
1148(30) 0.001111 942.2 1171.9
1109(30) 0.001111 942.2 1127.1
1074(29) 0.001189 942.1 1094.4
1046(29) 0.001189 942.1 1071.1
1022(29) 0.001189 942.1 1053.4
1057(29) 0.001189 942.0 1038.9
1047(29) 0.001189 942.0 1027.2
1046(29) 0.001189 941.9 1018.6
1054(29) 0.001189 941.9 1013.0
1056(29) 0.001189 941.9 1010.2
1047(29) 0.001189 941.8 1008.7
1061(29) 0.001189 941.8 1007.6
1055(29) 0.001189 941.7 1005.8
1038(29) 0.001189 941.7 1004.0
1031(29) 0.001189 941.7 1003.1
1013(29) 0.001189 941.6 1004.1
1028(29) 0.001189 941.6 1007.6
1055(29) 0.001189 941.6 1013.7
1043(29) 0.001189 941.5 1021.8
1022(29) 0.001189 941.5 1032.9
1013(29) 0.001189 941.4 1047.9
1035(29) 0.001189 941.4 1068.6
1071(29) 0.001189 941.4 1096.3
1101(30) 0.001111 941.3 1129.7
1134(30) 0.001111 941.3 1164.6
1186(31) 0.001041 941.3 1193.8
1139(30) 0.001111 941.2 1208.5
1158(31) 0.001041 941.2 1202.7
1190(31) 0.001041 941.2 1177.3
1161(31) 0.001041 941.1 1139.6
1084(30) 0.001111 941.1 1098.1
1061(29) 0.001189 941.1 1059.4
1057(29) 0.001189 941.0 1027.1
1004(29) 0.001189 941.0 1002.8
1004(28) 0.001276 941.0 985.9
1014(29) 0.001189 940.9 974.8
963(28) 0.001276 940.9 967.9
967(28) 0.001276 940.9 963.8
976(28) 0.001276 940.8 961.8
986(28) 0.001276 940.8 961.3
974(28) 0.001276 940.8 962.4
969(28) 0.001276 940.7 965.5
1008(29) 0.001189 940.7 971.3
973(28) 0.001276 940.7 980.5
928(27) 0.001372 940.6 993.3
943(28) 0.001276 940.6 1009.7
990(28) 0.001276 940.6 1028.8
1038(29) 0.001189 940.5 1048.6
1059(29) 0.001189 940.5 1066.7
1081(30) 0.001111 940.5 1080.1
1077(30) 0.001111 940.4 1088.0
1085(30) 0.001111 940.4 1092.1
1085(30) 0.001111 940.4 1095.8
1144(30) 0.001111 940.3 1102.0
1131(30) 0.001111 940.3 1111.1
1147(30) 0.001111 940.3 1121.2
1172(31) 0.001041 940.2 1128.3
1187(31) 0.001041 940.2 1127.9
1135(30) 0.001111 940.2 1118.5
1134(30) 0.001111 940.1 1102.6
1113(30) 0.001111 940.1 1084.6
1083(30) 0.001111 940.1 1068.3
1109(30) 0.001111 940.0 1056.1
1106(30) 0.001111 940.0 1049.0
1087(30) 0.001111 940.0 1046.3
1032(29) 0.001189 939.9 1047.7
1082(30) 0.001111 939.9 1053.1
1117(30) 0.001111 939.9 1063.2
1153(31) 0.001041 939.8 1078.2
1159(31) 0.001041 939.8 1096.6
1164(31) 0.001041 939.8 1115.6
1205(31) 0.001041 939.7 1130.9
1220(31) 0.001041 939.7 1138.3
1177(31) 0.001041 939.7 1136.1
1152(31) 0.001041 939.6 1127.4
1143(30) 0.001111 939.6 1116.3
1166(31) 0.001041 939.6 1106.7
1144(30) 0.001111 939.5 1099.9
1125(30) 0.001111 939.5 1095.0
1105(30) 0.001111 939.5 1089.5
1109(30) 0.001111 939.5 1080.9
1111(30) 0.001111 939.4 1068.1
1105(30) 0.001111 939.4 1052.9
1050(29) 0.001189 939.4 1037.8
1012(29) 0.001189 939.3 1024.6
998(28) 0.001276 939.3 1014.3
1028(29) 0.001189 939.3 1006.7
1004(28) 0.001276 939.2 1001.3
988(28) 0.001276 939.2 997.6
1001(28) 0.001276 939.2 995.3
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1032(29) 0.001189 939.1 996.7
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1030(29) 0.001189 938.9 984.3
1026(29) 0.001189 938.9 976.9
987(28) 0.001276 938.8 969.9
943(28) 0.001276 938.8 963.8
981(28) 0.001276 938.8 959.2
975(28) 0.001276 938.7 956.0
948(28) 0.001276 938.7 954.0
963(28) 0.001276 938.7 953.2
994(28) 0.001276 938.6 953.5
981(28) 0.001276 938.6 954.8
971(28) 0.001276 938.6 957.6
953(28) 0.001276 938.5 962.4
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969(28) 0.001276 938.5 981.4
978(28) 0.001276 938.4 996.9
1000(29) 0.001189 938.4 1016.9
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1097(30) 0.001111 938.3 1066.2
1092(30) 0.001111 938.3 1091.2
1073(30) 0.001111 938.2 1112.0
1130(30) 0.001111 938.2 1125.8
1133(30) 0.001111 938.2 1132.0
1142(31) 0.001041 938.1 1133.0
1125(30) 0.001111 938.1 1132.4
1112(30) 0.001111 938.1 1132.9
1163(31) 0.001041 938.0 1134.4
1114(30) 0.001111 938.0 1135.1
1140(30) 0.001111 938.0 1131.4
1098(30) 0.001111 937.9 1120.8
1137(30) 0.001111 937.9 1103.2
1099(30) 0.001111 937.8 1081.4
1046(29) 0.001189 937.8 1058.8
1016(29) 0.001189 937.8 1038.1
1026(29) 0.001189 937.7 1020.6
1018(29) 0.001189 937.7 1007.0
986(28) 0.001276 937.7 996.9
977(28) 0.001276 937.6 989.7
982(28) 0.001276 937.6 985.0
996(28) 0.001276 937.5 982.3
1012(29) 0.001189 937.5 981.1
967(28) 0.001276 937.5 980.9
942(28) 0.001276 937.4 980.8
906(27) 0.001372 937.4 980.2
973(28) 0.001276 937.3 978.6
967(28) 0.001276 937.3 976.2
936(28) 0.001276 937.3 973.5
947(28) 0.001276 937.2 971.1
979(28) 0.001276 937.2 969.8
1006(29) 0.001189 937.1 970.2
979(28) 0.001276 937.1 972.5
970(28) 0.001276 937.1 977.1
988(28) 0.001276 937.0 984.0
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1001(29) 0.001189 936.9 1004.4
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1044(29) 0.001189 936.8 1034.4
1032(29) 0.001189 936.8 1036.8
1042(29) 0.001189 936.7 1033.3
1013(29) 0.001189 936.7 1025.0
1022(29) 0.001189 936.6 1014.1
985(28) 0.001276 936.6 1002.5
1001(29) 0.001189 936.5 992.2
988(28) 0.001276 936.5 984.2
950(28) 0.001276 936.4 979.1
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1014(29) 0.001189 936.4 978.9
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1235(32) 0.000977 936.0 1253.6
1332(33) 0.000918 935.9 1340.7
1431(34) 0.000865 935.9 1431.8
1558(36) 0.000772 936. 1516.
1611(36) 0.000772 936. 1579.
1565(36) 0.000772 936. 1609.
1558(36) 0.000772 936. 1602.
1564(36) 0.000772 936. 1563.
1541(35) 0.000816 935.6 1505.5
1508(35) 0.000816 935.5 1443.0
1335(33) 0.000918 935.5 1383.6
1267(32) 0.000977 935.4 1330.6
1192(31) 0.001041 935.4 1283.4
1224(32) 0.000977 935.3 1239.9
1137(30) 0.001111 935.3 1199.3
1124(30) 0.001111 935.2 1162.4
1104(30) 0.001111 935.2 1129.9
1069(30) 0.001111 935.1 1102.4
1088(30) 0.001111 935.1 1079.6
1029(29) 0.001189 935.0 1060.3
1018(29) 0.001189 935.0 1043.5
1052(29) 0.001189 934.9 1028.2
1010(29) 0.001189 934.8 1014.6
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1017(23) 0.001890 934.7 994.0
964(28) 0.001276 934.7 988.0
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940(27) 0.001372 934.5 993.2
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1062(29) 0.001189 934.3 1029.3
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1059(29) 0.001189 934.1 1058.2
1025(29) 0.001189 934.0 1051.6
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996(28) 0.001276 933.7 996.0
980(28) 0.001276 933.7 987.3
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972(28) 0.001276 933.5 967.4
945(28) 0.001276 933.4 963.1
961(28) 0.001276 933.3 960.3
979(28) 0.001276 933.3 959.1
991(28) 0.001276 933.2 959.6
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970(28) 0.001276 933.1 965.4
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962(28) 0.001276 932.9 983.2
1020(29) 0.001189 932.8 990.1
1017(29) 0.001189 932.8 996.8
984(28) 0.001276 932.7 1003.2
1051(29) 0.001189 932.6 1009.6
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1027(29) 0.001189 932.1 1049.3
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1054(29) 0.001189 931.9 1053.9
1051(29) 0.001189 931.8 1058.3
1017(29) 0.001189 931.8 1063.9
1028(29) 0.001189 931.7 1070.4
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1040(29) 0.001189 931.5 1096.4
1104(30) 0.001111 931.4 1107.4
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1084(30) 0.001111 931.1 1124.9
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1102(30) 0.001111 930.9 1109.8
1122(30) 0.001111 930.8 1100.6
1061(29) 0.001189 930.8 1091.3
1052(29) 0.001189 930.7 1081.4
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1014(29) 0.001189 930.4 1041.8
997(28) 0.001276 930.4 1026.5
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1022(29) 0.001189 930.2 999.5
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1010(28) 0.001276 930.0 982.1
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962(28) 0.001276 929.9 975.4
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944(28) 0.001276 929.6 978.4
978(28) 0.001276 929.5 980.1
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979(28) 0.001276 928.5 980.1
965(28) 0.001276 928.5 989.2
995(28) 0.001276 928.4 1000.1
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1079(29) 0.001189 927.7 1111.2
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1217(31) 0.001041 927.2 1211.2
1257(44) 0.000517 927. 1228.
1267(31) 0.001041 927.0 1242.4
1290(31) 0.001041 926.9 1254.0
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1278(31) 0.001041 926.7 1253.0
1266(31) 0.001041 926.6 1235.1
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1127(29) 0.001189 926.3 1132.3
1089(29) 0.001189 926.2 1094.7
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1000(28) 0.001276 925.4 957.4
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981(27) 0.001372 924.6 984.2
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1004(28) 0.001276 924.4 1010.0
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1065(29) 0.001189 923.6 1106.2
1113(29) 0.001189 923.5 1101.4
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1044(28) 0.001276 923.2 1068.1
1049(28) 0.001276 923.0 1061.2
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1087(29) 0.001189 922.8 1067.5
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1116(29) 0.001189 922.5 1131.3
1163(30) 0.001111 922.3 1160.0
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1208(30) 0.001111 922.1 1206.7
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1223(31) 0.001041 921.7 1200.5
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1155(30) 0.001111 920.8 1125.5
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1125(29) 0.001189 920.4 1181.5
1194(30) 0.001111 920.3 1198.8
1196(30) 0.001111 920.1 1211.8
1185(30) 0.001111 920.0 1220.3
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1171(30) 0.001111 919.6 1227.6
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1136(29) 0.001189 918.7 1124.1
1083(29) 0.001189 918.6 1105.6
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1052(28) 0.001276 918.3 1077.1
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1059(28) 0.001276 917.5 1046.3
1012(28) 0.001276 917.4 1042.0
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965(27) 0.001372 914.7 988.2
972(28) 0.001276 914.5 1002.4
1021(28) 0.001276 914.4 1019.7
1044(29) 0.001189 914.2 1040.1
1029(28) 0.001276 914.1 1063.2
1098(29) 0.001189 914.0 1088.7
1150(30) 0.001111 913.8 1115.8
1148(30) 0.001111 913.7 1143.1
1195(30) 0.001111 913.5 1168.7
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1268(31) 0.001041 912.6 1247.5
1330(32) 0.000977 912.5 1248.1
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1251(31) 0.001041 912.2 1231.7
1208(31) 0.001041 912.0 1214.5
1226(31) 0.001041 911.9 1193.4
1181(30) 0.001111 911.7 1170.3
1167(30) 0.001111 911.6 1146.6
1065(29) 0.001189 911.4 1123.3
1136(30) 0.001111 911.2 1100.8
1064(29) 0.001189 911.1 1079.3
1093(29) 0.001189 910.9 1059.3
1032(28) 0.001276 910.8 1041.5
985(28) 0.001276 910.6 1026.7
981(28) 0.001276 910.5 1015.7
1008(28) 0.001276 910.3 1008.9
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1265(32) 0.000977 974.3 1231.8
1238(32) 0.000977 975.9 1235.2
1260(32) 0.000977 977.6 1238.5
1253(32) 0.000977 979.3 1241.6
1232(32) 0.000977 981.0 1244.6
1192(32) 0.000977 982.7 1247.5
1267(32) 0.000977 984.4 1250.3
1297(33) 0.000918 986.2 1252.9
1263(32) 0.000977 988.0 1255.4
1270(32) 0.000977 989.8 1257.8
1290(33) 0.000918 991.6 1260.1
1292(33) 0.000918 993.4 1262.4
1279(33) 0.000918 995.2 1264.5
1291(33) 0.000918 997.1 1266.6
1264(32) 0.000977 999.0 1268.5
1233(32) 0.000977 1000.9 1270.4
1251(32) 0.000977 1002.8 1272.2
1271(33) 0.000918 1004.8 1274.0
1303(33) 0.000918 1006.7 1275.6
1296(33) 0.000918 1008.7 1277.2
1260(32) 0.000977 1010.7 1278.6
1241(32) 0.000977 1012.7 1280.0
1203(32) 0.000977 1014.8 1281.3
1221(32) 0.000977 1016.8 1282.4
1226(32) 0.000977 1018.9 1283.5
1204(32) 0.000977 1021.0 1284.4
1221(32) 0.000977 1023.2 1285.2
1249(32) 0.000977 1025.3 1285.8
1235(32) 0.000977 1027.5 1286.3
1220(32) 0.000977 1029.7 1286.7
1241(32) 0.000977 1031.9 1286.9
1253(32) 0.000977 1034.1 1286.9
1266(32) 0.000977 1036.3 1286.9
1236(32) 0.000977 1038.6 1286.6
1243(32) 0.000977 1040.9 1286.3
1285(33) 0.000918 1043.2 1285.7
1270(32) 0.000977 1045.6 1285.1
1228(32) 0.000977 1047.9 1284.3
1247(32) 0.000977 1050.3 1283.5
1238(32) 0.000977 1052.7 1282.5
1228(32) 0.000977 1055.2 1281.4
1236(32) 0.000977 1057.6 1280.3
1242(32) 0.000977 1060.1 1279.1
1262(32) 0.000977 1062.6 1277.8
1258(32) 0.000977 1065.1 1276.5
1249(32) 0.000977 1067.6 1275.2
1222(32) 0.000977 1070.2 1273.8
1220(32) 0.000977 1072.8 1272.4
1202(32) 0.000977 1075.4 1271.1
1230(32) 0.000977 1078.1 1269.8
1267(32) 0.000977 1080.7 1268.5
1237(32) 0.000977 1083.4 1267.2
1252(32) 0.000977 1086.1 1266.0
1244(32) 0.000977 1088.9 1264.9
1232(32) 0.000977 1091.6 1263.8
1256(32) 0.000977 1094.4 1262.8
1292(33) 0.000918 1097.2 1261.8
1278(33) 0.000918 1100.1 1261.0
1258(32) 0.000977 1102.9 1260.2
1266(32) 0.000977 1105.8 1259.6
1252(33) 0.000918 1108.7 1259.1
1248(33) 0.000918 1111.7 1258.6
1238(33) 0.000918 1114.7 1258.3
1258(33) 0.000918 1117.7 1258.1
1253(33) 0.000918 1120.7 1258.1
1248(33) 0.000918 1123.7 1258.1
1274(33) 0.000918 1126.8 1258.3
1264(33) 0.000918 1129.9 1258.7
1229(33) 0.000918 1133.0 1259.1
1269(33) 0.000918 1136.2 1259.8
1278(33) 0.000918 1139.4 1260.5
1277(33) 0.000918 1142.6 1261.5
1285(33) 0.000918 1145.8 1262.5
1282(33) 0.000918 1149.1 1263.8
1313(34) 0.000865 1152.4 1265.2
1264(33) 0.000918 1155.7 1266.7
1302(34) 0.000865 1159.1 1268.5
1310(34) 0.000865 1162.5 1270.4
1253(33) 0.000918 1165.9 1272.5
1318(34) 0.000865 1169.3 1274.7
1298(34) 0.000865 1172.8 1277.1
1323(34) 0.000865 1176.3 1279.7
1303(34) 0.000865 1179.8 1282.5
1271(33) 0.000918 1183.4 1285.5
1269(33) 0.000918 1187.0 1288.6
1260(33) 0.000918 1190.6 1291.9
1298(34) 0.000865 1194.3 1295.4
1312(34) 0.000865 1198.0 1299.1
1343(34) 0.000865 1201.7 1302.9
1351(34) 0.000865 1205.4 1307.0
1329(34) 0.000865 1209.2 1311.2
1371(34) 0.000865 1213.0 1315.6
1321(34) 0.000865 1216.9 1320.2
1308(34) 0.000865 1220.7 1324.9
1332(34) 0.000865 1224.6 1329.8
1314(34) 0.000865 1228.6 1334.9
1317(34) 0.000865 1232.6 1340.1
1341(34) 0.000865 1236.6 1345.6
1356(34) 0.000865 1240.6 1351.1
1334(34) 0.000865 1244.7 1356.9
1344(34) 0.000865 1248.8 1362.8
1364(34) 0.000865 1252.9 1368.8
1353(34) 0.000865 1257.1 1375.0
1380(34) 0.000865 1261.3 1381.4
1381(34) 0.000865 1265.5 1387.9
1427(35) 0.000816 1269.8 1394.5
1413(35) 0.000816 1274.1 1401.2
1420(35) 0.000816 1278.5 1408.1
1455(35) 0.000816 1282.8 1415.1
1421(35) 0.000816 1287.3 1422.2
1394(35) 0.000816 1291.7 1429.5
1421(35) 0.000816 1296.2 1436.8
1405(35) 0.000816 1300.7 1444.2
1452(35) 0.000816 1305.3 1451.7
1475(36) 0.000772 1310. 1459.
1491(36) 0.000772 1315. 1467.
1515(36) 0.000772 1319. 1475.
1489(36) 0.000772 1324. 1483.
1478(36) 0.000772 1329. 1490.
1512(36) 0.000772 1333. 1498.
1534(36) 0.000772 1338. 1506.
1542(36) 0.000772 1343. 1514.
1529(36) 0.000772 1348. 1522.
1509(36) 0.000772 1353. 1530.
1516(36) 0.000772 1358. 1538.
1566(37) 0.000730 1363. 1547.
1565(36) 0.000772 1368. 1555.
1586(37) 0.000730 1373. 1563.
1659(37) 0.000730 1378. 1571.
1609(37) 0.000730 1383. 1578.
1570(37) 0.000730 1389. 1586.
1678(38) 0.000693 1394. 1594.
1677(38) 0.000693 1399. 1602.
1668(38) 0.000693 1404. 1610.
1706(38) . . .
1672(38) . . .
1642(37) . . .
1663(38) . . .
1677(38) . . .
1626(37) . . .
1672(38) . . .
1691(38) . . .
1696(38) . . .
1695(38) . . .
1726(38) . . .
1741(38) . . .
1723(38) . . .
1758(38) . . .
1752(38) . . .
1694(38) . . .
1716(38) . . .
1735(38) . . .
1749(38) . . .
1702(38) . . .
1732(38) . . .
1767(39) . . .
1768(39) . . .
1715(38) . . .
1736(38) . . .
1769(39) . . .
1742(55) . . .
1861(57) . . .
1792(56) . . .
1804(56) . . .
1950(58) . . .
1853(57) . . .
1850(57) . . .
1812(56) . . .
1840(56) . . .
1825(56) . . .
1939(58) . . .
1920(58) . . .
1869(57) . . .
1876(57) . . .
1960(58) . . .
1873(57) . . .
1865(57) . . .
1915(58) . . .
1926(58) . . .
1986(58) . . .
1879(57) . . .
1936(58) . . .
1872(57) . . .
1849(57) . . .
1902(57) . . .
1937(58) . . .
1874(57) . . .
1998(59) . . .
1915(58) . . .
1967(58) . . .
1960(58) . . .
1907(57) . . .
2074(60) . . .
1998(59) . . .
1894(57) . . .
2003(59) . . .
2040(59) . . .
2023(59) . . .
1938(58) . . .
1983(58) . . .
2044(59) . . .
2036(59) . . .
2028(59) . . .
1918(58) . . .
2012(59) . . .
1972(58) . . .
1966(58) . . .
1924(58) . . .
2060(59) . . .
2055(59) . . .
2059(59) . . .
2005(59) . . .
2026(59) . . .
2018(59) . . .
1990(59) . . .
1988(58) . . .
2044(59) . . .
2088(60) . . .
2178(61) . . .
2112(60) . . .
2168(61) . . .
2054(59) . . .
2103(60) . . .
2087(60) . . .
2147(61) . . .
2099(60) . . .
2111(60) . . .
2162(61) . . .
2092(60) . . .
2133(60) . . .
2129(60) . . .
2142(60) . . .
2223(62) . . .
2207(61) . . .
2213(61) . . .
2236(62) . . .
2202(61) . . .
2231(62) . . .
2263(62) . . .
2174(61) . . .
2257(62) . . .
2233(62) . . .
2215(61) . . .
2208(61) . . .
2239(62) . . .
2191(61) . . .
2259(62) . . .
2185(61) . . .
2199(61) . . .
2234(62) . . .
2240(62) . . .
2266(62) . . .
2286(62) . . .
2170(61) . . .
2133(60) . . .
2207(61) . . .
2293(62) . . .
2251(62) . . .
2186(61) . . .
2321(63) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_cell_measurement_reflns_used    643
_reflns_number_total             643
_reflns_limit_h_min              1
_reflns_limit_h_max              17
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.056
_reflns_d_resolution_low         18.687
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_0P5_CH3O_FINAL_publ
_database_code_depnum_ccdc_archive 'CCDC 1582011'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-06-08T15:27|0P5_CH3O_FINAL|WENDY|BT1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-06-08T15:27

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.07
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     47
_refine_ls_goodness_of_fit_all   1.12
_refine_ls_number_restraints     21
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10

_cell_measurement_theta_min      4
_cell_measurement_theta_max      160

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from Z:/queen/Desktop/FeBTT/FeBTT_CO2 _September2013_new/bare/BARE'
_cell_length_a                   18.90048(32)
_cell_length_b                   18.90048
_cell_length_c                   18.90048
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6751.78(34)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Fe Fe1 0.1331(4) 0.5 0.0 1.0 Uiso 0.002(1) 12
C C1 0.15171(32) 0.3369(4) -0.15171(32) 1.0 Uiso 0.0169(10) 24
C C2 0.18118(30) 0.2724(4) -0.18118(30) 1.0 Uiso 0.0169(10) 24
C C3 0.24214(27) 0.24214(27) -0.1470(4) 1.0 Uiso 0.0169(10) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.006(4) 3
N N1 0.13058(21) 0.42070(19) -0.08111(22) 1.0 Uiso 0.0148(5) 48
N N2 0.17655(22) 0.36792(21) -0.09175(21) 1.0 Uiso 0.0148(5) 48
H H1 0.2633(5) 0.2633(5) -0.1073(6) 1.0 Uiso 0.025(4) 24
Fe Fe2 0.2678(27) 0.0 0.0 0.1793 Uiso 0.10322 6
O Os 0.2482(6) 0.5 0.0 0.6471 Uiso 0.03508 12
C Cs 0.3013(10) 0.5 0.0538(10) 0.3236 Uiso 0.03508 24
O O1a 0.2582(15) 0.5 0.0 0.358(11) Uiso 0.09(1) 12
O O1b 0.3078(32) 0.3881(17) 0.0 0.179(5) Uiso 0.10(2) 24
C C1a 0.2849(20) 0.4448(12) 0.0 0.179(5) Uiso 0.10(2) 24
H Hsa 0.2772(19) 0.5 0.1009(9) 0.3236 Uiso 0.10908 24
H Hsb 0.3296(14) 0.4532(8) 0.0489(17) 0.3236 Uiso 0.10908 48
C C2a 0.0 0.2854(17) 0.0404(19) 0.074(4) Uiso 0.09(3) 24
O O2b 0.0 0.240(5) 0.081(6) 0.074(4) Uiso 0.09(3) 24
O O2a 0.0 0.3308(4) 0.0 0.295(15) Uiso 0.07(4) 6
C C3a 0.135(4) 0.135(4) 0.0 0.156(7) Uiso 0.07(2) 12
O O3a 0.076(5) 0.118(5) 0.0 0.078(4) Uiso 0.07(2) 24
O O3b 0.194(5) 0.153(5) 0.0 0.078(4) Uiso 0.07(2) 24

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C29.23 H15.77 Cl Fe4.36 N32 O7.88'
_chemical_formula_weight         1220.15
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Fe1 Fe1 3.559(10) . 14_555 N
Fe1 Fe1 3.559(10) . 19_555 N
Fe1 Cl1 2.516(7) . 1_555 N
Fe1 N1 2.1445(34) . 1_555 N
Fe1 N1 2.1445(34) . 4_555 N
Fe1 N1 2.1445(34) . 12_565 N
Fe1 N1 3.050(5) . 17_555 N
Fe1 N1 3.050(5) . 19_555 N
Fe1 N1 3.050(5) . 23_565 N
Fe1 N1 2.1445(34) . -10_565 N
Fe1 N1 3.050(5) . -14_565 N
Fe1 N2 3.148(4) . 1_555 N
Fe1 N2 3.148(4) . 4_555 N
Fe1 N2 3.148(4) . 12_565 N
Fe1 N2 3.148(4) . -10_565 N
Fe1 Os 2.175(10) . 1_555 N
Fe1 Cs 3.338(16) . 1_555 N
Fe1 Cs 3.338(16) . 4_555 N
Fe1 O1a 2.364(29) . 1_555 N
Fe1 O1b 3.92(4) . 1_555 N
Fe1 O1b 3.92(4) . 12_565 N
Fe1 C1a 3.053(32) . 1_555 N
Fe1 C1a 3.053(32) . 12_565 N
Fe1 Hsa 3.324(29) . 1_555 N
Fe1 Hsa 3.324(29) . 4_555 N
C1 C2 1.451(11) . 1_555 N
C1 N1 2.109(8) . 1_555 N
C1 N1 2.109(8) . 19_555 N
C1 N2 1.360(6) . 1_555 N
C1 N2 1.360(6) . 19_555 N
C2 C1 1.451(11) . 1_555 N
C2 C3 1.439(5) . 1_555 N
C2 C3 1.439(5) . 7_555 N
C3 C2 1.439(5) . 1_555 N
C3 C2 1.439(5) . 9_555 N
C3 H1 0.940(10) . 1_555 N
Cl1 Fe1 2.516(7) . 1_555 N
Cl1 Fe1 2.516(7) . 10_555 N
Cl1 Fe1 2.516(7) . 14_555 N
Cl1 Fe1 2.516(7) . 19_555 N
Cl1 N1 3.269(4) . 1_555 N
Cl1 N1 3.269(4) . 4_555 N
Cl1 N1 3.269(4) . 10_555 N
Cl1 N1 3.269(4) . 12_565 N
Cl1 N1 3.269(4) . 14_555 N
Cl1 N1 3.269(4) . 17_555 N
Cl1 N1 3.269(4) . 19_555 N
Cl1 N1 3.269(4) . 23_565 N
Cl1 N1 3.269(4) . -1_565 N
Cl1 N1 3.269(4) . -4_565 N
Cl1 N1 3.269(4) . -10_565 N
Cl1 N1 3.269(4) . -12_555 N
Cl1 N1 3.269(4) . -14_565 N
Cl1 N1 3.269(4) . -17_565 N
Cl1 N1 3.269(4) . -19_565 N
Cl1 N1 3.269(4) . -23_555 N
Cl1 Fe2 4.39(5) . 2_555 N
Cl1 Fe2 4.39(5) . 11_565 N
Cl1 O2a 3.198(8) . 1_555 N
Cl1 O2a 3.198(8) . 12_565 N
N1 Fe1 2.1445(34) . 1_555 N
N1 Fe1 3.050(5) . 19_555 N
N1 C1 2.109(8) . 1_555 N
N1 Cl1 3.269(4) . 1_555 N
N1 N1 1.322(9) . 19_555 N
N1 N2 1.338(5) . 1_555 N
N2 Fe1 3.148(4) . 1_555 N
N2 C1 1.360(6) . 1_555 N
N2 N1 1.338(5) . 1_555 N
H1 C3 0.940(10) . 1_555 N
Fe2 Cl1 4.39(5) . 3_555 N
Fe2 C2a 0.83(5) . 3_555 N
Fe2 C2a 0.83(5) . 6_555 N
Fe2 C2a 0.83(5) . 13_555 N
Fe2 C2a 0.83(5) . 16_555 N
Fe2 O2b 1.61(7) . 3_555 N
Fe2 O2b 1.61(7) . 6_555 N
Fe2 O2b 1.61(7) . 13_555 N
Fe2 O2b 1.61(7) . 16_555 N
Fe2 O2a 1.19(5) . 3_555 N
Fe2 C3a 3.58(4) . 1_555 N
Fe2 C3a 3.58(4) . 3_555 N
Fe2 C3a 3.58(4) . 9_555 N
Fe2 C3a 3.58(4) . 12_555 N
Fe2 O3a 3.17(9) . 3_555 N
Fe2 O3a 3.17(9) . 9_555 N
Fe2 O3a 3.17(9) . 13_555 N
Fe2 O3a 3.17(9) . 24_555 N
Fe2 O3b 3.21(9) . 1_555 N
Fe2 O3b 3.21(9) . 12_555 N
Fe2 O3b 3.21(9) . 15_555 N
Fe2 O3b 3.21(9) . 21_555 N
Os Fe1 2.175(10) . 1_555 N
Os Cs 1.429(11) . 1_555 N
Os Cs 1.429(11) . 4_555 N
Os O1a 0.189(32) . 1_555 N
Os O1b 2.396(21) . 1_555 N
Os O1b 2.396(21) . 12_565 N
Os C1a 1.253(19) . 1_555 N
Os C1a 1.253(19) . 12_565 N
Cs Fe1 3.338(16) . 1_555 N
Cs Os 1.429(11) . 1_555 N
Cs Cs 2.03(4) . 4_555 N
Cs O1a 1.303(23) . 1_555 N
Cs O1b 2.350(29) . 1_555 N
Cs O1b 2.350(29) . 12_565 N
Cs C1a 1.490(25) . 1_555 N
Cs C1a 1.490(25) . 12_565 N
Cs Hsa 1.000(11) . 1_555 N
Cs Hsb 1.037(11) . 1_555 N
Cs Hsb 1.037(11) . -10_565 N
O1a Fe1 2.364(29) . 1_555 N
O1a Os 0.189(32) . 1_555 N
O1a Cs 1.303(23) . 1_555 N
O1a Cs 1.303(23) . 4_555 N
O1a O1b 2.313(16) . 1_555 N
O1a O1b 2.313(16) . 12_565 N
O1a C1a 1.160(11) . 1_555 N
O1a C1a 1.160(11) . 12_565 N
O1b Fe1 3.92(4) . 1_555 N
O1b Os 2.396(21) . 1_555 N
O1b Cs 2.350(29) . 1_555 N
O1b Cs 2.350(29) . 4_555 N
O1b O1a 2.313(16) . 1_555 N
O1b O1b 2.15(6) . 13_555 N
O1b C1a 1.155(11) . 1_555 N
C1a Fe1 3.053(32) . 1_555 N
C1a Os 1.253(19) . 1_555 N
C1a Cs 1.490(25) . 1_555 N
C1a Cs 1.490(25) . 4_555 N
C1a O1a 1.160(11) . 1_555 N
C1a O1b 1.155(11) . 1_555 N
C1a C1a 2.09(5) . 12_565 N
C1a Hsb 1.26(4) . 1_555 N
C1a Hsb 1.26(4) . 4_555 N
Hsa Fe1 3.324(29) . 1_555 N
Hsa Cs 1.000(11) . 1_555 N
Hsa Hsb 1.652(16) . 1_555 N
Hsa Hsb 1.652(16) . -10_565 N
Hsb Cs 1.037(11) . 1_555 N
Hsb C1a 1.26(4) . 1_555 N
Hsb Hsa 1.652(16) . 1_555 N
Hsb Hsb 1.85(6) . 4_555 N
Hsb Hsb 1.768(32) . -10_565 N
C2a Fe2 0.83(5) . 2_555 N
C2a C2a 1.53(7) . 4_555 N
C2a C2a 1.08(5) . 14_555 N
C2a C2a 1.08(5) . 17_555 N
C2a O2b 1.149(11) . 1_555 N
C2a O2b 2.45(11) . 4_555 N
C2a O2b 1.91(7) . 14_555 N
C2a O2b 1.91(7) . 17_555 N
C2a O2a 1.148(11) . 1_555 N
O2b Fe2 1.61(7) . 2_555 N
O2b C2a 1.149(11) . 1_555 N
O2b C2a 2.45(11) . 4_555 N
O2b C2a 1.91(7) . 14_555 N
O2b C2a 1.91(7) . 17_555 N
O2b O2b 2.16(15) . 14_555 N
O2b O2b 2.16(15) . 17_555 N
O2b O2a 2.298(16) . 1_555 N
O2b C3a 2.23(5) . 2_555 N
O2b O3a 2.30(13) . 14_555 N
O2b O3b 1.62(10) . 2_555 N
O2b O3b 2.70(8) . 14_555 N
O2a Cl1 3.198(8) . 1_555 N
O2a Fe2 1.19(5) . 2_555 N
O2a C2a 1.148(11) . 1_555 N
O2a C2a 1.148(11) . 4_555 N
O2a C2a 1.148(11) . 14_555 N
O2a C2a 1.148(11) . 17_555 N
O2a O2b 2.298(16) . 1_555 N
O2a O2b 2.298(16) . 4_555 N
O2a O2b 2.298(16) . 14_555 N
O2a O2b 2.298(16) . 17_555 N
C3a Fe2 3.58(4) . 1_555 N
C3a Fe2 3.58(4) . 2_555 N
C3a O2b 2.23(5) . 3_555 N
C3a O2b 2.23(5) . 14_555 N
C3a O3a 1.154(11) . 1_555 N
C3a O3a 1.154(11) . 13_555 N
C3a O3b 1.154(11) . 1_555 N
C3a O3b 1.154(11) . 13_555 N
O3a Fe2 3.17(9) . 2_555 N
O3a O2b 2.30(13) . 14_555 N
O3a C3a 1.154(11) . 1_555 N
O3a O3a 2.78(11) . 2_555 N
O3a O3a 2.78(11) . 3_555 N
O3a O3a 2.78(11) . 7_555 N
O3a O3a 2.78(11) . 9_555 N
O3a O3a 2.89(18) . 10_555 N
O3a O3a 1.12(16) . 13_555 N
O3a O3a 2.04(13) . 14_555 N
O3a O3a 2.04(13) . 19_555 N
O3a O3b 2.308(16) . 1_555 N
O3a O3b 2.03(8) . 13_555 N
O3b Fe2 3.21(9) . 1_555 N
O3b O2b 1.62(10) . 3_555 N
O3b O2b 2.70(8) . 14_555 N
O3b C3a 1.154(11) . 1_555 N
O3b O3a 2.308(16) . 1_555 N
O3b O3a 2.03(8) . 13_555 N
O3b O3b 1.09(16) . 13_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Fe1 N1 88.71(24) 1_555 . 1_555 N
Cl1 Fe1 N1 88.71(24) 1_555 . 4_555 N
Cl1 Fe1 N1 88.71(24) 1_555 . 12_565 N
Cl1 Fe1 N1 88.71(24) 1_555 . -10_565 N
N1 Fe1 N1 91.26(24) 1_555 . 4_555 N
N1 Fe1 N1 177.4(5) 1_555 . 12_565 N
N1 Fe1 N1 88.68(24) 1_555 . -10_565 N
N1 Fe1 N1 88.68(24) 4_555 . 12_565 N
N1 Fe1 N1 177.4(5) 4_555 . -10_565 N
N1 Fe1 N1 91.26(24) 12_565 . -10_565 N
C2 C1 N2 123.3(4) 1_555 . 1_555 N
C2 C1 N2 123.3(4) 1_555 . 19_555 N
N2 C1 N2 112.9(7) 1_555 . 19_555 N
C1 C2 C3 118.0(4) 1_555 . 1_555 N
C1 C2 C3 118.0(4) 1_555 . 7_555 N
C3 C2 C3 124.1(7) 1_555 . 7_555 N
C2 C3 C2 115.8(7) 1_555 . 9_555 N
C2 C3 H1 122.0(4) 1_555 . 1_555 N
C2 C3 H1 122.0(4) 9_555 . 1_555 N
Fe1 Cl1 Fe1 180.0 1_555 . 10_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 19_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 19_555 N
Fe1 Cl1 Fe1 180.0 14_555 . 19_555 N
Fe1 N1 N1 121.43(21) 1_555 . 19_555 N
Fe1 N1 N2 127.9(4) 1_555 . 1_555 N
N1 N1 N2 110.66(26) 19_555 . 1_555 N
C1 N2 N1 102.9(4) 1_555 . 1_555 N
C2a Fe2 C2a 133(7) 3_555 . 6_555 N
C2a Fe2 C2a 80.8(26) 3_555 . 13_555 N
C2a Fe2 C2a 80.8(26) 3_555 . 16_555 N
C2a Fe2 O2b 43(4) 3_555 . 3_555 N
C2a Fe2 O2b 175(8) 3_555 . 6_555 N
C2a Fe2 O2b 97.5(14) 3_555 . 13_555 N
C2a Fe2 O2b 97.5(14) 3_555 . 16_555 N
C2a Fe2 O2a 66(4) 3_555 . 3_555 N
C2a Fe2 C2a 80.8(26) 6_555 . 13_555 N
C2a Fe2 C2a 80.8(26) 6_555 . 16_555 N
C2a Fe2 O2b 175(8) 6_555 . 3_555 N
C2a Fe2 O2b 43(4) 6_555 . 6_555 N
C2a Fe2 O2b 97.5(14) 6_555 . 13_555 N
C2a Fe2 O2b 97.5(14) 6_555 . 16_555 N
C2a Fe2 O2a 66(4) 6_555 . 3_555 N
C2a Fe2 C2a 133(7) 13_555 . 16_555 N
C2a Fe2 O2b 97.5(14) 13_555 . 3_555 N
C2a Fe2 O2b 97.5(14) 13_555 . 6_555 N
C2a Fe2 O2b 43(4) 13_555 . 13_555 N
C2a Fe2 O2b 175(8) 13_555 . 16_555 N
C2a Fe2 O2a 66(4) 13_555 . 3_555 N
C2a Fe2 O2b 97.5(14) 16_555 . 3_555 N
C2a Fe2 O2b 97.5(14) 16_555 . 6_555 N
C2a Fe2 O2b 175(8) 16_555 . 13_555 N
C2a Fe2 O2b 43(4) 16_555 . 16_555 N
C2a Fe2 O2a 66(4) 16_555 . 3_555 N
O2b Fe2 O2b 142(10) 3_555 . 6_555 N
O2b Fe2 O2b 83.9(31) 3_555 . 13_555 N
O2b Fe2 O2b 83.9(31) 3_555 . 16_555 N
O2b Fe2 O2a 109(5) 3_555 . 3_555 N
O2b Fe2 O2b 83.9(31) 6_555 . 13_555 N
O2b Fe2 O2b 83.9(31) 6_555 . 16_555 N
O2b Fe2 O2a 109(5) 6_555 . 3_555 N
O2b Fe2 O2b 142(10) 13_555 . 16_555 N
O2b Fe2 O2a 109(5) 13_555 . 3_555 N
O2b Fe2 O2a 109(5) 16_555 . 3_555 N
Cs Os Cs 90.8(20) 1_555 . 4_555 N
Cs Os O1a 45.4(10) 1_555 . 1_555 N
Cs Os C1a 67.1(14) 1_555 . 1_555 N
Cs Os C1a 67.1(14) 1_555 . 12_565 N
Cs Os O1a 45.4(10) 4_555 . 1_555 N
Cs Os C1a 67.1(14) 4_555 . 1_555 N
Cs Os C1a 67.1(14) 4_555 . 12_565 N
O1a Os C1a 56.4(20) 1_555 . 1_555 N
O1a Os C1a 56.4(20) 1_555 . 12_565 N
C1a Os C1a 113(4) 1_555 . 12_565 N
Os Cs O1a 5.9(11) 1_555 . 1_555 N
Os Cs C1a 50.8(10) 1_555 . 1_555 N
Os Cs C1a 50.8(10) 1_555 . 12_565 N
Os Cs Hsa 108.2(11) 1_555 . 1_555 N
Os Cs Hsb 107.4(10) 1_555 . 1_555 N
Os Cs Hsb 107.4(10) 1_555 . -10_565 N
O1a Cs C1a 48.5(8) 1_555 . 1_555 N
O1a Cs C1a 48.5(8) 1_555 . 12_565 N
O1a Cs Hsa 114.2(15) 1_555 . 1_555 N
O1a Cs Hsb 104.7(11) 1_555 . 1_555 N
O1a Cs Hsb 104.7(11) 1_555 . -10_565 N
C1a Cs C1a 89.0(13) 1_555 . 12_565 N
C1a Cs Hsa 120.8(15) 1_555 . 1_555 N
C1a Cs Hsb 56.6(15) 1_555 . 1_555 N
C1a Cs Hsb 130.1(16) 1_555 . -10_565 N
C1a Cs Hsa 120.8(15) 12_565 . 1_555 N
C1a Cs Hsb 130.1(16) 12_565 . 1_555 N
C1a Cs Hsb 56.6(15) 12_565 . -10_565 N
Hsa Cs Hsb 108.3(10) 1_555 . 1_555 N
Hsa Cs Hsb 108.3(10) 1_555 . -10_565 N
Hsb Cs Hsb 116.9(27) 1_555 . -10_565 N
Os O1a Cs 128.7(14) 1_555 . 1_555 N
Os O1a Cs 128.7(14) 1_555 . 4_555 N
Os O1a C1a 115.8(24) 1_555 . 1_555 N
Os O1a C1a 115.8(24) 1_555 . 12_565 N
Cs O1a Cs 102.6(28) 1_555 . 4_555 N
Cs O1a C1a 74.2(16) 1_555 . 1_555 N
Cs O1a C1a 74.2(16) 1_555 . 12_565 N
Cs O1a C1a 74.2(16) 4_555 . 1_555 N
Cs O1a C1a 74.2(16) 4_555 . 12_565 N
C1a O1a C1a 128(5) 1_555 . 12_565 N
C1a O1b Hsb 51.8(17) 1_555 . 1_555 N
C1a O1b Hsb 51.8(17) 1_555 . 4_555 N
Hsb O1b Hsb 70.9(27) 1_555 . 4_555 N
Os C1a Cs 62.1(9) 1_555 . 1_555 N
Os C1a Cs 62.1(9) 1_555 . 4_555 N
Os C1a O1a 7.8(13) 1_555 . 1_555 N
Os C1a O1b 168(4) 1_555 . 1_555 N
Os C1a Hsb 105.3(17) 1_555 . 1_555 N
Os C1a Hsb 105.3(17) 1_555 . 4_555 N
Cs C1a Cs 86.1(20) 1_555 . 4_555 N
Cs C1a O1a 57.3(14) 1_555 . 1_555 N
Cs C1a O1b 124.8(21) 1_555 . 1_555 N
Cs C1a Hsb 43.3(10) 1_555 . 1_555 N
Cs C1a Hsb 105.7(31) 1_555 . 4_555 N
Cs C1a O1a 57.3(14) 4_555 . 1_555 N
Cs C1a O1b 124.8(21) 4_555 . 1_555 N
Cs C1a Hsb 105.7(31) 4_555 . 1_555 N
Cs C1a Hsb 43.3(10) 4_555 . 4_555 N
O1a C1a O1b 176(4) 1_555 . 1_555 N
O1a C1a Hsb 100.2(22) 1_555 . 1_555 N
O1a C1a Hsb 100.2(22) 1_555 . 4_555 N
O1b C1a Hsb 82.3(24) 1_555 . 1_555 N
O1b C1a Hsb 82.3(24) 1_555 . 4_555 N
Hsb C1a Hsb 94(4) 1_555 . 4_555 N
Cs Hsb O1b 125.2(21) 1_555 . 1_555 N
Cs Hsb C1a 80.1(13) 1_555 . 1_555 N
O1b Hsb C1a 45.9(14) 1_555 . 1_555 N
Fe2 C2a C2a 24(4) 2_555 . 4_555 N
Fe2 C2a C2a 49.6(13) 2_555 . 14_555 N
Fe2 C2a C2a 49.6(13) 2_555 . 17_555 N
Fe2 C2a O2b 108(5) 2_555 . 1_555 N
Fe2 C2a O2a 71.9(34) 2_555 . 1_555 N
C2a C2a C2a 45.0000(7) 4_555 . 14_555 N
C2a C2a C2a 45.0000(7) 4_555 . 17_555 N
C2a C2a O2b 132(5) 4_555 . 1_555 N
C2a C2a O2a 48.3(23) 4_555 . 1_555 N
C2a C2a C2a 90.0000(14) 14_555 . 17_555 N
C2a C2a O2b 117.9(30) 14_555 . 1_555 N
C2a C2a O2a 61.9(14) 14_555 . 1_555 N
C2a C2a O2b 117.9(30) 17_555 . 1_555 N
C2a C2a O2a 61.9(14) 17_555 . 1_555 N
O2b C2a O2a 180.000(10) 1_555 . 1_555 N
Fe2 O2b C2a 29.4(19) 2_555 . 1_555 N
Fe2 O2b O3b 166(11) 2_555 . 2_555 N
C2a O2b O3b 164(11) 1_555 . 2_555 N
Fe2 O2a C2a 41.7(23) 2_555 . 1_555 N
Fe2 O2a C2a 41.7(23) 2_555 . 4_555 N
Fe2 O2a C2a 41.7(23) 2_555 . 14_555 N
Fe2 O2a C2a 41.7(23) 2_555 . 17_555 N
C2a O2a C2a 83(5) 1_555 . 4_555 N
C2a O2a C2a 56.1(27) 1_555 . 14_555 N
C2a O2a C2a 56.1(27) 1_555 . 17_555 N
C2a O2a C2a 56.1(27) 4_555 . 14_555 N
C2a O2a C2a 56.1(27) 4_555 . 17_555 N
C2a O2a C2a 83(5) 14_555 . 17_555 N
O3a C3a O3a 58(9) 1_555 . 13_555 N
O3a C3a O3b 180.00(4) 1_555 . 1_555 N
O3a C3a O3b 123(9) 1_555 . 13_555 N
O3a C3a O3b 123(9) 13_555 . 1_555 N
O3a C3a O3b 180.00(4) 13_555 . 13_555 N
O3b C3a O3b 57(9) 1_555 . 13_555 N
C3a O3a O3a 61(5) 1_555 . 13_555 N
O2b O3b C3a 106(8) 3_555 . 1_555 N
O2b O3b O3b 168(7) 3_555 . 13_555 N
C3a O3b O3b 62(5) 1_555 . 13_555 N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT601_0P5_CH3O_FINAL_publ 
;
PROBLEM: Structure Contains Solvent Accessible VOIDS of .       2571 Ang3 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT430_0P5_CH3O_FINAL_publ 
;
PROBLEM:Short Inter D...A Contact  O1A    ..  O1B     ..       2.33 Ang.   
RESPONSE: The problem happens because the adsorbed carbon dioxide on the open metal sites are disordered and thus some atoms ostensibly are seemed to be close to each other.
;
_vrf_PLAT307_0P5_CH3O_FINAL_publ 
;
PROBLEM: Isolated Metal Atom found in Structure (Unusual)        Fe2 Check  
RESPONSE: It is charge balancing extra framework cation and it is supposed to be sorrounded by solvent molecules which couldn't be modeled because lack of their highly ordered pattern.
;

_vrf_PLAT049_0P5_CH3O_FINAL_publ 
;
PROBLEM: Calculated Density less than 1.0 gcm-3 .........     0.9004 Check 
RESPONSE: This is expected as the material is porous.
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_cell_measurement_reflns_used    666
_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Fe 13.076 0.9450 International_Tables_Vol_C
C 87.698 0.6646 International_Tables_Vol_C
Cl 3.0 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 47.299 -0.3739 International_Tables_Vol_C
O 23.635 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.0775
_pd_proc_ls_prof_R_factor        0.0235
_pd_proc_ls_prof_wR_factor       0.0272
_pd_proc_ls_prof_wR_expected     0.0245
_refine_ls_R_Fsqd_factor         0.05084

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 10 terms.
 Shifted Chebyshev function of 1st kind
      1:    1557.91     2:   -414.969     3:    325.380     4:   -22.4670    
      5:    176.528     6:   -46.2753     7:    104.427     8:   -21.3932    
      9:    54.3467    10:   -3.99837    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  532.082 #2(GV)   = -269.462 #3(GW)   =  125.486
 #4(GP)   =    0.636 #5(LX)   =    0.000 #6(LY)   =   20.328
 #7(S/L)  =   0.0433 #8(H/L)  =   0.0360
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0005 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00050
_pd_proc_info_datetime           2016-06-08T15:27:16
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.6717
_pd_proc_2theta_range_max        166.4217
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
5900(170) 0.0 3248. .
5340(160) 0.0 3235. .
4890(150) 0.0 3222. .
4680(150) 0.0 3209. .
4390(140) 0.0 3196. .
4350(140) 0.0 3184. .
3860(140) 0.0 3171. .
3980(140) 0.0 3159. .
3620(130) 0.0 3147. .
3770(130) 0.0 3134. .
3570(130) 0.0 3122. .
3660(130) 0.0 3110. .
3680(130) 0.0 3098. .
3580(130) 0.0 3086. .
3680(130) 0.0 3074. .
3780(130) 0.0 3063. .
3520(130) 0.0 3051. .
3770(130) 0.0 3039. .
3820(130) 0.0 3028. .
3620(130) 0.0 3016. .
3420(130) 0.0 3005. .
3650(130) 0.0 2994. .
3720(130) 0.0 2983. .
3550(130) 0.0 2972. .
3660(130) 0.0 2960. .
3770(130) 0.0 2950. .
3580(130) 0.0 2939. .
3620(130) 0.0 2928. .
3490(130) 0.0 2917. .
3720(130) 0.0 2907. .
3670(130) 0.0 2896. .
3430(130) 0.0 2885. .
3110(120) 0.0 2875. .
3250(120) 0.0 2865. .
3260(120) 0.0 2854. .
3140(120) 0.0 2844. .
3340(130) 0.0 2834. .
3160(120) 0.0 2824. .
3380(130) 0.0 2814. .
3100(120) 0.0 2804. .
3200(120) 0.0 2794. .
3270(130) 0.0 2785. .
2880(120) 0.0 2775. .
3020(120) 0.0 2765. .
3130(120) 0.0 2756. .
2910(120) 0.0 2746. .
2980(120) 0.0 2737. .
2900(120) 0.0000718 2728. 2736.
3060(120) 0.0000683 2718. 2728.
3020(120) 0.0000694 2709. 2721.
3160(120) 0.0000661 2700. 2717.
2970(120) 0.0000706 2691. 2719.
3320(130) 0.0000640 2682. 2729.
3190(120) 0.0000661 2673. 2749.
3030(120) 0.0000694 2664. 2781.
3260(120) 0.0000650 2655. 2823.
3180(120) 0.0000661 2647. 2873.
3430(130) 0.0000610 2638. 2929.
3290(130) 0.0000640 2630. 2990.
3230(120) 0.0000650 2621. 3054.
3380(130) 0.0000620 2613. 3123.
3400(130) 0.0000620 2604. 3196.
3590(130) 0.0000592 2596. 3273.
3510(130) 0.0000601 2588. 3355.
3470(130) 0.0000610 2579. 3442.
3660(130) 0.0000574 2571. 3535.
3660(130) 0.0000574 2563. 3634.
3840(140) 0.0000549 2555. 3739.
3930(140) 0.0000541 2547. 3853.
3820(130) 0.0000557 2539. 3975.
4200(140) 0.0000503 2531. 4105.
4230(140) 0.0000503 2524. 4247.
4110(140) 0.0000518 2516. 4400.
4620(150) 0.0000463 2508. 4566.
4770(150) 0.0000444 2501. 4746.
4890(150) 0.0000433 2493. 4944.
4900(150) 0.0000433 2485. 5162.
5070(150) 0.0000422 2478. 5403.
5400(160) 0.0000396 2471. 5671.
5740(160) 0.0000372 2463. 5972.
6430(170) 0.0000334 2456. 6313.
6590(180) 0.0000327 2449. 6703.
7140(180) 0.0000302 2442. 7156.
7590(190) 0.0000283 2435. 7692.
8340(200) 0.0000258 2428. 8342.
9580(210) 0.0000225 2421. 9160.
10810(220) 0.0000199 2414. 10239.
12150(240) 0.0000178 2407. 11709.
13750(250) 0.0000157 2400. 13689.
16460(280) 0.0000131 2393. 16105.
18700(290) 0.0000116 2387. 18461.
20140(310) 0.0000107 2380. 19799.
20190(310) 0.0000107 2373. 19150.
17100(280) 0.0000127 2367. 16302.
12860(240) 0.0000168 2360. 12165.
8860(200) 0.0000243 2354. 8152.
6000(170) 0.0000354 2347. 5231.
3610(130) 0.0000583 2341. 3566.
2810(120) 0.0000743 2335. 2808.
2520(110) 0.0000826 2328. 2520.
2346(72) 0.0001929 2322. 2423.
2238(70) 0.0002041 2316. 2387.
2234(70) 0.0002041 2310. 2367.
2143(69) 0.0002100 2304. 2353.
2300(71) 0.0001984 2298. 2341.
2147(69) 0.0002100 2292. 2331.
2114(68) 0.0002163 2286. 2321.
2106(68) 0.0002163 2280. 2312.
2182(69) 0.0002100 2275. 2304.
2042(67) 0.0002228 2269. 2296.
2226(70) 0.0002041 2263. 2289.
2205(70) 0.0002041 2257. 2282.
2144(69) 0.0002100 2252. 2275.
2108(68) 0.0002163 2246. 2269.
2187(69) 0.0002100 2241. 2264.
2241(70) 0.0002041 2235. 2259.
2271(71) 0.0001984 2230. 2255.
2281(71) 0.0001984 2224. 2255.
2283(71) 0.0001984 2219. 2261.
2238(70) 0.0002041 2214. 2276.
2244(70) 0.0002041 2208. 2305.
2487(74) 0.0001826 2203. 2347.
2341(72) 0.0001929 2198. 2402.
2397(73) 0.0001877 2193. 2469.
2329(72) 0.0001929 2188. 2546.
2509(74) 0.0001826 2183. 2624.
2600(76) 0.0001731 2178. 2717.
2644(76) 0.0001731 2173. 2819.
2707(77) 0.0001687 2168. 2932.
2854(79) 0.0001602 2163. 3056.
3161(83) 0.0001452 2158. 3194.
3249(85) 0.0001384 2154. 3348.
3200(84) 0.0001417 2149. 3522.
3503(88) 0.0001291 2144. 3721.
3756(91) 0.0001208 2139. 3950.
4051(94) 0.0001132 2135. 4219.
4382(98) 0.0001041 2130. 4542.
4890(100) 0.0000925 2126. 4943.
5720(110) 0.0000797 2121. 5468.
6220(120) 0.0000731 2117. 6171.
7600(130) 0.0000601 2112. 7134.
8910(140) 0.0000510 2108. 8371.
10150(150) 0.0000450 2104. 9711.
11180(160) 0.0000406 2099. 10717.
11310(160) 0.0000401 2095. 10822.
10300(150) 0.0000444 2091. 9727.
7810(130) 0.0000583 2087. 7740.
5800(110) 0.0000783 2082. 5597.
3877(92) 0.0001181 2078. 3917.
2982(81) 0.0001524 2074. 2900.
2519(74) 0.0001826 2070. 2410.
2227(70) 0.0002041 2066. 2216.
2141(69) 0.0002100 2062. 2148.
1975(66) 0.0002296 2058. 2122.
2068(67) 0.0002228 2054. 2109.
2065(67) 0.0002228 2050. 2101.
2123(68) 0.0002163 2047. 2094.
2015(67) 0.0002228 2043. 2088.
2042(67) 0.0002228 2039. 2083.
2134(69) 0.0002100 2035. 2080.
2111(68) 0.0002163 2032. 2078.
2308(71) 0.0001984 2028. 2078.
2236(70) 0.0002041 2024. 2085.
2466(74) 0.0001826 2021. 2105.
2393(73) 0.0001877 2017. 2146.
2464(74) 0.0001826 2014. 2220.
2623(76) 0.0001731 2010. 2335.
2832(79) 0.0001602 2007. 2491.
2810(79) 0.0001602 2003. 2687.
2887(80) 0.0001562 2000. 2917.
3075(82) 0.0001487 1996. 3180.
3385(86) 0.0001352 1993. 3476.
3715(90) 0.0001235 1990. 3811.
3900(93) 0.0001156 1986. 4191.
4363(98) 0.0001041 1983. 4627.
4790(100) 0.0000943 1980. 5136.
5540(110) 0.0000826 1977. 5743.
6290(120) 0.0000718 1974. 6488.
7030(120) 0.0000650 1970. 7441.
8410(140) 0.0000541 1967. 8718.
10530(150) 0.0000433 1964. 10470.
12980(170) 0.0000350 1961. 12776.
15420(180) 0.0000295 1958. 15412.
17650(200) 0.0000258 1955. 17636.
18130(200) 0.0000250 1952. 18357.
16380(190) 0.0000277 1949. 16799.
12810(170) 0.0000354 1946. 13301.
8940(140) 0.0000510 1943. 9218.
5680(110) 0.0000797 1941. 5853.
3890(92) 0.0001181 1938. 3734.
2596(76) 0.0001731 1935. 2679.
2172(69) 0.0002100 1932. 2250.
2081(68) 0.0002163 1930. 2097.
1926(65) 0.0002367 1927. 2041.
1951(66) 0.0002296 1924. 2014.
2037(67) 0.0002228 1921. 1997.
1918(88) 0.0001291 1919. 1983.
1911(88) 0.0001291 1916. 1971.
1844(86) 0.0001352 1914. 1962.
1846(86) 0.0001352 1911. 1953.
1870(63) 0.0002520 1909. 1946.
1910(64) 0.0002441 1906. 1940.
1916(64) 0.0002441 1904. 1934.
1867(63) 0.0002520 1901. 1928.
1922(64) 0.0002441 1899. 1924.
1858(63) 0.0002520 1896. 1919.
1839(63) 0.0002520 1894. 1915.
1890(64) 0.0002441 1892. 1911.
1912(64) 0.0002441 1889. 1907.
1919(64) 0.0002441 1887. 1904.
1873(63) 0.0002520 1885. 1900.
1917(64) 0.0002441 1882. 1897.
1895(64) 0.0002441 1880. 1894.
1929(64) 0.0002441 1878. 1891.
1938(64) 0.0002441 1876. 1889.
2002(65) 0.0002367 1873. 1887.
1847(63) 0.0002520 1871. 1884.
1864(63) 0.0002520 1869. 1882.
1934(64) 0.0002441 1867. 1880.
1922(64) 0.0002441 1865. 1877.
1881(63) 0.0002520 1863. 1873.
1889(63) 0.0002520 1861. 1870.
1827(62) 0.0002601 1859. 1867.
1797(62) 0.0002601 1857. 1857.
1942(64) 0.0002441 1855. 1855.
1890(64) 0.0002441 1853. 1853.
1841(63) 0.0002520 1851. 1851.
1934(64) 0.0002441 1849. 1849.
1828(62) 0.0002601 1847. 1847.
1801(62) 0.0002601 1845. 1845.
1894(64) 0.0002441 1843. 1844.
1834(62) 0.0002601 1842. 1842.
1761(61) 0.0002687 1840. 1840.
1908(64) 0.0002441 1838. 1838.
1932(64) 0.0002441 1836. 1836.
1831(62) 0.0002601 1834. 1835.
1892(64) 0.0002441 1833. 1833.
1771(61) 0.0002687 1831. 1831.
1829(62) 0.0002601 1829. 1830.
1822(62) 0.0002601 1828. 1828.
1785(62) 0.0002601 1826. 1827.
1797(62) 0.0002601 1824. 1825.
1837(63) 0.0002520 1823. 1824.
1824(62) 0.0002601 1821. 1823.
1852(63) 0.0002520 1819. 1822.
1797(62) 0.0002601 1818. 1821.
1865(63) 0.0002520 1816. 1820.
1769(61) 0.0002687 1815. 1819.
1834(62) 0.0002601 1813. 1818.
1765(61) 0.0002687 1812. 1816.
1811(62) 0.0002601 1810. 1813.
1827(62) 0.0002601 1809. 1811.
1774(61) 0.0002687 1807. 1809.
1801(62) 0.0002601 1806. 1807.
1722(61) 0.0002687 1804. 1805.
1762(61) 0.0002687 1803. 1804.
1782(62) 0.0002601 1802. 1802.
1812(62) 0.0002601 1800. 1801.
1762(61) 0.0002687 1799. 1800.
1792(62) 0.0002601 1798. 1799.
1886(63) 0.0002520 1796. 1798.
1788(62) 0.0002601 1795. 1798.
1710(60) 0.0002778 1794. 1798.
1751(61) 0.0002687 1792. 1800.
1859(63) 0.0002520 1791. 1803.
1840(63) 0.0002520 1790. 1808.
1820(62) 0.0002601 1789. 1814.
1836(63) 0.0002520 1787. 1822.
1848(63) 0.0002520 1786. 1832.
1881(63) 0.0002520 1785. 1845.
1827(62) 0.0002601 1784. 1863.
1800(62) 0.0002601 1783. 1888.
1959(65) 0.0002367 1781. 1922.
1975(65) 0.0002367 1780. 1961.
1811(62) 0.0002601 1779. 1995.
1774(61) 0.0002687 1778. 2008.
1891(64) 0.0002441 1777. 1986.
1892(64) 0.0002441 1776. 1936.
1868(63) 0.0002520 1775. 1877.
1866(63) 0.0002520 1774. 1829.
1860(63) 0.0002520 1773. 1799.
1761(61) 0.0002687 1772. 1784.
1729(61) 0.0002687 1771. 1777.
1750(61) 0.0002687 1770. 1774.
1903(64) 0.0002441 1769. 1772.
1746(61) 0.0002687 1768. 1771.
1849(63) 0.0002520 1767. 1769.
1771(61) 0.0002687 1766. 1768.
1747(61) 0.0002687 1765. 1767.
1812(62) 0.0002601 1764. 1766.
1755(61) 0.0002687 1763. 1765.
1780(62) 0.0002601 1762. 1764.
1854(63) 0.0002520 1761. 1765.
1866(63) 0.0002520 1760. 1764.
1776(61) 0.0002687 1759. 1763.
1738(61) 0.0002687 1759. 1763.
1638(86) 0.0001352 1758. 1762.
1661(59) 0.0002873 1757. 1761.
1647(58) 0.0002973 1756. 1761.
1719(60) 0.0002778 1755. 1760.
1712(60) 0.0002778 1754. 1760.
1733(60) 0.0002778 1754. 1759.
1745(60) 0.0002778 1753. 1759.
1814(61) 0.0002687 1752. 1759.
1767(60) 0.0002778 1751. 1759.
1810(61) 0.0002687 1750. 1759.
1894(63) 0.0002520 1750. 1759.
1896(63) 0.0002520 1749. 1759.
1804(61) 0.0002687 1748. 1760.
1767(60) 0.0002778 1747. 1762.
1840(62) 0.0002601 1747. 1766.
1913(63) 0.0002520 1746. 1775.
1834(62) 0.0002601 1745. 1791.
1896(63) 0.0002520 1745. 1818.
1947(64) 0.0002441 1744. 1859.
1961(64) 0.0002441 1743. 1916.
2054(65) 0.0002367 1743. 1991.
2120(66) 0.0002296 1742. 2090.
2213(68) 0.0002163 1741. 2221.
2426(71) 0.0001984 1741. 2402.
2657(74) 0.0001826 1740. 2646.
3171(81) 0.0001524 1740. 2943.
3503(86) 0.0001352 1739. 3230.
3550(86) 0.0001352 1738. 3391.
3423(85) 0.0001384 1738. 3317.
2944(78) 0.0001644 1737. 3004.
2486(72) 0.0001929 1737. 2586.
2282(69) 0.0002100 1736. 2219.
1999(64) 0.0002441 1735. 1977.
1880(62) 0.0002601 1735. 1852.
1836(62) 0.0002601 1734. 1801.
1834(62) 0.0002601 1734. 1784.
1797(61) 0.0002687 1733. 1784.
1929(63) 0.0002520 1733. 1796.
1966(64) 0.0002441 1732. 1822.
1919(63) 0.0002520 1732. 1872.
1934(63) 0.0002520 1731. 1953.
2185(67) 0.0002228 1731. 2073.
2286(69) 0.0002100 1730. 2239.
2504(72) 0.0001929 1730. 2463.
2716(75) 0.0001778 1729. 2767.
3216(82) 0.0001487 1729. 3186.
3594(87) 0.0001321 1728. 3750.
4264(94) 0.0001132 1728. 4424.
4980(100) 0.0000961 1728. 5056.
5230(110) 0.0000907 1727. 5379.
4890(100) 0.0000980 1727. 5159.
4168(93) 0.0001156 1726. 4424.
3461(85) 0.0001384 1726. 3495.
2620(74) 0.0001826 1725. 2704.
2143(67) 0.0002228 1725. 2196.
1906(63) 0.0002520 1725. 1938.
1878(62) 0.0002601 1724. 1830.
1797(61) 0.0002687 1724. 1789.
1749(60) 0.0002778 1723. 1772.
1727(60) 0.0002778 1723. 1763.
1678(59) 0.0002873 1723. 1757.
1699(59) 0.0002873 1722. 1753.
1726(60) 0.0002778 1722. 1749.
1778(61) 0.0002687 1722. 1747.
1862(62) 0.0002601 1721. 1745.
1835(62) 0.0002601 1721. 1743.
1780(61) 0.0002687 1721. 1742.
1822(61) 0.0002687 1720. 1741.
1721(60) 0.0002778 1720. 1740.
1782(61) 0.0002687 1720. 1740.
1781(61) 0.0002687 1719. 1740.
1644(58) 0.0002973 1719. 1740.
1714(60) 0.0002778 1719. 1741.
1703(59) 0.0002873 1718. 1741.
1721(60) 0.0002778 1718. 1742.
1743(60) 0.0002778 1718. 1744.
1798(61) 0.0002687 1718. 1747.
1886(63) 0.0002520 1717. 1753.
1965(64) 0.0002441 1717. 1764.
1825(61) 0.0002687 1717. 1786.
1967(64) 0.0002441 1716. 1828.
1978(64) 0.0002441 1716. 1901.
2093(66) 0.0002296 1716. 2015.
2244(68) 0.0002163 1716. 2184.
2489(72) 0.0001929 1715. 2422.
2718(75) 0.0001778 1715. 2757.
3176(81) 0.0001524 1715. 3220.
3970(91) 0.0001208 1715. 3816.
4580(98) 0.0001041 1714. 4464.
5130(100) 0.0000925 1714. 4959.
5200(100) 0.0000925 1714. 5043.
4575(98) 0.0001041 1714. 4589.
3602(87) 0.0001321 1713. 3781.
2885(77) 0.0001687 1713. 2962.
2328(70) 0.0002041 1713. 2361.
2065(65) 0.0002367 1713. 2018.
1935(63) 0.0002520 1713. 1862.
1828(62) 0.0002601 1712. 1802.
1908(63) 0.0002520 1712. 1785.
1744(60) 0.0002778 1712. 1787.
1729(57) 0.0003078 1712. 1804.
1913(60) 0.0002778 1712. 1839.
1955(60) 0.0002778 1711. 1894.
1868(59) 0.0002873 1711. 1980.
1966(60) 0.0002778 1711. 2103.
2260(65) 0.0002367 1711. 2276.
2433(67) 0.0002228 1711. 2498.
2626(70) 0.0002041 1710. 2735.
2757(72) 0.0001929 1710. 2908.
2784(72) 0.0001929 1710. 2924.
2497(68) 0.0002163 1710. 2743.
2419(67) 0.0002228 1710. 2443.
2117(63) 0.0002520 1710. 2148.
1856(59) 0.0002873 1709. 1936.
1820(58) 0.0002973 1709. 1818.
1815(58) 0.0002973 1709. 1763.
1786(58) 0.0002973 1709. 1742.
1744(57) 0.0003078 1709. 1734.
1805(58) 0.0002973 1709. 1731.
1745(57) 0.0003078 1708. 1729.
1709(56) 0.0003189 1708. 1730.
1766(57) 0.0003078 1708. 1732.
1754(57) 0.0003078 1708. 1737.
1809(58) 0.0002973 1708. 1744.
1826(58) 0.0002973 1708. 1754.
1879(59) 0.0002873 1708. 1765.
1881(59) 0.0002873 1707. 1775.
1786(58) 0.0002973 1707. 1777.
1707(56) 0.0003189 1707. 1769.
1714(56) 0.0003189 1707. 1754.
1746(57) 0.0003078 1707. 1738.
1731(57) 0.0003078 1707. 1726.
1710(56) 0.0003189 1707. 1720.
1684(56) 0.0003189 1706. 1717.
1689(56) 0.0003189 1706. 1716.
1632(55) 0.0003306 1706. 1717.
1652(55) 0.0003306 1706. 1719.
1841(59) 0.0002873 1706. 1722.
1832(58) 0.0002973 1706. 1729.
1834(58) 0.0002973 1706. 1738.
1708(56) 0.0003189 1706. 1753.
1782(58) 0.0002973 1705. 1772.
1785(58) 0.0002973 1705. 1796.
1778(58) 0.0002973 1705. 1818.
1812(58) 0.0002973 1705. 1832.
1801(58) 0.0002973 1705. 1828.
1772(57) 0.0003078 1705. 1805.
1789(58) 0.0002973 1705. 1773.
1803(58) 0.0002973 1705. 1747.
1680(56) 0.0003189 1705. 1729.
1728(57) 0.0003078 1704. 1720.
1725(57) 0.0003078 1704. 1716.
1739(57) 0.0003078 1704. 1715.
1773(57) 0.0003078 1704. 1714.
1691(56) 0.0003189 1704. 1715.
1714(56) 0.0003189 1704. 1715.
1796(58) 0.0002973 1704. 1715.
1728(57) 0.0003078 1704. 1716.
1695(56) 0.0003189 1704. 1716.
1665(56) 0.0003189 1703. 1717.
1748(57) 0.0003078 1703. 1719.
1673(56) 0.0003189 1703. 1720.
1696(56) 0.0003189 1703. 1721.
1681(56) 0.0003189 1703. 1723.
1755(57) 0.0003078 1703. 1727.
1753(57) 0.0003078 1703. 1730.
1741(57) 0.0003078 1703. 1735.
1756(57) 0.0003078 1703. 1744.
1754(57) 0.0003078 1703. 1760.
1798(58) 0.0002973 1702. 1791.
1886(59) 0.0002873 1702. 1849.
2070(62) 0.0002601 1702. 1950.
2242(65) 0.0002367 1702. 2114.
2392(67) 0.0002228 1702. 2364.
2747(72) 0.0001929 1702. 2723.
3233(78) 0.0001644 1702. 3185.
3798(84) 0.0001417 1702. 3677.
4137(88) 0.0001291 1702. 4039.
4142(88) 0.0001291 1702. 4082.
3900(86) 0.0001352 1701. 3732.
3319(79) 0.0001602 1701. 3148.
2639(70) 0.0002041 1701. 2577.
2204(64) 0.0002441 1701. 2171.
2005(61) 0.0002687 1701. 1947.
1817(58) 0.0002973 1701. 1854.
1776(57) 0.0003078 1701. 1837.
1877(59) 0.0002873 1701. 1870.
1923(60) 0.0002778 1701. 1952.
2107(63) 0.0002520 1701. 2096.
2318(66) 0.0002296 1701. 2323.
2483(68) 0.0002163 1700. 2652.
3111(76) 0.0001731 1700. 3073.
3641(83) 0.0001452 1700. 3513.
3902(86) 0.0001352 1700. 3821.
3765(84) 0.0001417 1700. 3829.
3439(80) 0.0001562 1700. 3489.
3062(76) 0.0001731 1700. 2958.
2489(68) 0.0002163 1700. 2456.
2116(63) 0.0002520 1700. 2106.
1927(60) 0.0002778 1699. 1917.
1849(59) 0.0002873 1699. 1842.
1850(58) 0.0002973 1699. 1833.
1913(59) 0.0002873 1699. 1869.
2024(60) 0.0002778 1699. 1953.
2150(62) 0.0002601 1699. 2096.
2290(64) 0.0002441 1699. 2316.
2563(68) 0.0002163 1699. 2621.
2884(72) 0.0001929 1699. 2976.
3210(77) 0.0001687 1699. 3291.
3390(79) 0.0001602 1698. 3426.
3273(77) 0.0001687 1698. 3283.
2980(74) 0.0001826 1698. 2912.
2556(68) 0.0002163 1698. 2487.
2246(64) 0.0002441 1698. 2148.
2046(61) 0.0002687 1698. 1943.
1878(58) 0.0002973 1698. 1852.
1874(58) 0.0002973 1698. 1835.
1961(59) 0.0002873 1698. 1871.
1975(60) 0.0002778 1697. 1962.
2159(62) 0.0002601 1697. 2122.
2337(65) 0.0002367 1697. 2375.
2546(68) 0.0002163 1697. 2728.
2921(73) 0.0001877 1697. 3148.
3381(79) 0.0001602 1697. 3529.
3601(81) 0.0001524 1697. 3711.
3316(78) 0.0001644 1697. 3567.
3061(75) 0.0001778 1696. 3143.
2523(68) 0.0002163 1696. 2637.
2136(62) 0.0002601 1696. 2223.
1924(59) 0.0002873 1696. 1962.
1808(57) 0.0003078 1696. 1828.
1764(56) 0.0003189 1696. 1769.
1735(56) 0.0003189 1696. 1745.
1767(56) 0.0003189 1696. 1734.
1794(57) 0.0003078 1695. 1727.
1739(56) 0.0003189 1695. 1723.
1779(56) 0.0003189 1695. 1720.
1862(58) 0.0002973 1695. 1718.
1770(56) 0.0003189 1695. 1716.
1768(56) 0.0003189 1695. 1714.
1756(56) 0.0003189 1695. 1712.
1683(55) 0.0003306 1694. 1710.
1776(56) 0.0003189 1694. 1707.
1747(56) 0.0003189 1694. 1706.
1705(55) 0.0003306 1694. 1705.
1712(55) 0.0003306 1694. 1704.
1766(56) 0.0003189 1694. 1703.
1685(55) 0.0003306 1694. 1703.
1834(57) 0.0003078 1693. 1703.
1797(57) 0.0003078 1693. 1705.
1728(56) 0.0003189 1693. 1708.
1857(58) 0.0002973 1693. 1712.
1805(57) 0.0003078 1693. 1715.
1689(55) 0.0003306 1693. 1717.
1744(56) 0.0003189 1693. 1715.
1780(56) 0.0003189 1692. 1711.
1787(57) 0.0003078 1692. 1706.
1713(55) 0.0003306 1692. 1701.
1760(56) 0.0003189 1692. 1699.
1683(55) 0.0003306 1692. 1697.
1717(55) 0.0003306 1692. 1697.
1720(55) 0.0003306 1691. 1698.
1798(57) 0.0003078 1691. 1699.
1635(54) 0.0003429 1691. 1701.
1695(55) 0.0003306 1691. 1705.
1752(56) 0.0003189 1691. 1710.
1773(56) 0.0003189 1691. 1715.
1767(56) 0.0003189 1690. 1717.
1707(55) 0.0003306 1690. 1716.
1722(55) 0.0003306 1690. 1711.
1740(56) 0.0003189 1690. 1704.
1731(56) 0.0003189 1690. 1699.
1732(56) 0.0003189 1689. 1695.
1641(54) 0.0003429 1689. 1694.
1637(54) 0.0003429 1689. 1693.
1725(55) 0.0003306 1689. 1693.
1744(56) 0.0003189 1689. 1692.
1733(56) 0.0003189 1689. 1692.
1664(54) 0.0003429 1688. 1692.
1707(55) 0.0003306 1688. 1692.
1704(55) 0.0003306 1688. 1692.
1665(54) 0.0003429 1688. 1692.
1648(54) 0.0003429 1688. 1692.
1621(54) 0.0003429 1687. 1692.
1713(55) 0.0003306 1687. 1692.
1703(55) 0.0003306 1687. 1691.
1696(55) 0.0003306 1687. 1692.
1762(56) 0.0003189 1687. 1693.
1691(55) 0.0003306 1686. 1695.
1677(55) 0.0003306 1686. 1698.
1678(55) 0.0003306 1686. 1705.
1735(56) 0.0003189 1686. 1715.
1780(56) 0.0003189 1686. 1727.
1721(55) 0.0003306 1685. 1740.
1658(54) 0.0003429 1685. 1749.
1717(55) 0.0003306 1685. 1749.
1649(54) 0.0003429 1685. 1740.
1777(56) 0.0003189 1685. 1726.
1638(54) 0.0003429 1684. 1714.
1664(54) 0.0003429 1684. 1707.
1738(54) 0.0003429 1684. 1705.
1798(55) 0.0003306 1684. 1711.
1792(55) 0.0003306 1683. 1725.
1805(55) 0.0003306 1683. 1751.
1758(54) 0.0003429 1683. 1792.
1856(56) 0.0003189 1683. 1847.
1931(57) 0.0003078 1682. 1907.
1959(57) 0.0003078 1682. 1954.
1970(57) 0.0003078 1682. 1966.
1951(57) 0.0003078 1682. 1931.
1845(55) 0.0003306 1682. 1868.
1788(55) 0.0003306 1681. 1805.
1718(53) 0.000356 1681. 1761.
1700(53) 0.000356 1681. 1742.
1785(55) 0.0003306 1681. 1744.
1750(54) 0.0003429 1680. 1770.
1825(55) 0.0003306 1680. 1824.
1850(56) 0.0003189 1680. 1910.
2017(58) 0.0002973 1680. 2028.
2071(59) 0.0002873 1679. 2157.
2169(60) 0.0002778 1679. 2256.
2208(61) 0.0002687 1679. 2279.
2138(60) 0.0002778 1679. 2205.
2013(58) 0.0002973 1678. 2073.
1882(56) 0.0003189 1678. 1943.
1873(56) 0.0003189 1678. 1857.
1917(57) 0.0003078 1678. 1829.
1874(56) 0.0003189 1677. 1862.
2026(58) 0.0002973 1677. 1968.
2193(61) 0.0002687 1677. 2170.
2426(64) 0.0002441 1677. 2485.
2850(70) 0.0002041 1676. 2895.
3443(77) 0.0001687 1676. 3315.
3675(79) 0.0001602 1676. 3595.
3597(78) 0.0001644 1675. 3585.
3340(76) 0.0001731 1675. 3262.
2854(70) 0.0002041 1675. 2785.
2373(63) 0.0002520 1675. 2344.
2078(59) 0.0002873 1674. 2035.
1869(56) 0.0003189 1674. 1860.
1787(55) 0.0003306 1674. 1777.
1725(54) 0.0003429 1674. 1741.
1696(53) 0.000356 1673. 1725.
1663(53) 0.000356 1673. 1717.
1605(52) 0.000370 1673. 1712.
1634(52) 0.000370 1672. 1708.
1703(53) 0.000356 1672. 1706.
1695(53) 0.000356 1672. 1705.
1634(52) 0.000370 1671. 1705.
1696(53) 0.000356 1671. 1708.
1712(53) 0.000356 1671. 1714.
1741(54) 0.0003429 1671. 1727.
1761(54) 0.0003429 1670. 1755.
1792(55) 0.0003306 1670. 1811.
1888(56) 0.0003189 1670. 1908.
2029(58) 0.0002973 1669. 2055.
2189(61) 0.0002687 1669. 2243.
2357(63) 0.0002520 1669. 2429.
2507(65) 0.0002367 1668. 2543.
2386(63) 0.0002520 1668. 2523.
2235(61) 0.0002687 1668. 2368.
2061(59) 0.0002873 1668. 2156.
1926(57) 0.0003078 1667. 1967.
1759(54) 0.0003429 1667. 1840.
1706(53) 0.000356 1667. 1776.
1723(53) 0.000356 1666. 1760.
1717(53) 0.000356 1666. 1777.
1790(55) 0.0003306 1666. 1822.
1833(55) 0.0003306 1665. 1885.
1809(55) 0.0003306 1665. 1952.
1804(55) 0.0003306 1665. 1999.
1906(56) 0.0003189 1664. 1999.
1792(55) 0.0003306 1664. 1948.
1744(54) 0.0003429 1664. 1871.
1755(54) 0.0003429 1663. 1798.
1720(53) 0.000356 1663. 1747.
1645(52) 0.000370 1663. 1717.
1665(53) 0.000356 1662. 1704.
1761(54) 0.0003429 1662. 1698.
1748(54) 0.0003429 1662. 1697.
1665(53) 0.000356 1661. 1698.
1631(52) 0.000370 1661. 1700.
1637(52) 0.000370 1661. 1703.
1717(53) 0.000356 1660. 1708.
1677(53) 0.000356 1660. 1715.
1703(53) 0.000356 1660. 1727.
1726(54) 0.0003429 1659. 1749.
1754(54) 0.0003429 1659. 1793.
1888(56) 0.0003189 1659. 1882.
2103(59) 0.0002873 1658. 2055.
2389(63) 0.0002520 1658. 2357.
2837(69) 0.0002100 1658. 2816.
3447(77) 0.0001687 1657. 3393.
4032(83) 0.0001452 1657. 3956.
4302(86) 0.0001352 1657. 4288.
4261(86) 0.0001352 1656. 4204.
3791(81) 0.0001524 1656. 3722.
3019(72) 0.0001929 1655. 3081.
2427(64) 0.0002441 1655. 2516.
2084(59) 0.0002873 1655. 2133.
1872(44) 0.000517 1654. 1928.
1850(52) 0.000370 1654. 1849.
1772(51) 0.000384 1654. 1845.
1848(52) 0.000370 1653. 1884.
1958(53) 0.000356 1653. 1942.
1925(53) 0.000356 1653. 1993.
1936(53) 0.000356 1652. 2011.
1988(54) 0.0003429 1652. 1980.
1893(52) 0.000370 1651. 1914.
1793(51) 0.000384 1651. 1845.
1854(52) 0.000370 1651. 1799.
1797(51) 0.000384 1650. 1791.
1803(51) 0.000384 1650. 1831.
1908(53) 0.000356 1650. 1931.
2134(56) 0.0003189 1649. 2095.
2304(58) 0.0002973 1649. 2312.
2418(59) 0.0002873 1648. 2531.
2497(60) 0.0002778 1648. 2672.
2565(61) 0.0002687 1648. 2659.
2394(59) 0.0002873 1647. 2488.
2168(56) 0.0003189 1647. 2246.
1976(54) 0.0003429 1647. 2027.
1824(52) 0.000370 1646. 1880.
1796(51) 0.000384 1646. 1812.
1807(51) 0.000384 1645. 1811.
1910(53) 0.000356 1645. 1865.
1972(54) 0.0003429 1645. 1958.
2102(55) 0.0003306 1644. 2066.
2169(56) 0.0003189 1644. 2151.
2187(57) 0.0003078 1643. 2171.
2150(56) 0.0003189 1643. 2107.
2070(55) 0.0003306 1643. 1991.
1905(53) 0.000356 1642. 1872.
1771(51) 0.000384 1642. 1782.
1660(49) 0.000416 1641. 1731.
1666(49) 0.000416 1641. 1712.
1736(50) 0.000400 1641. 1717.
1719(50) 0.000400 1640. 1738.
1767(51) 0.000384 1640. 1766.
1840(52) 0.000370 1639. 1791.
1843(52) 0.000370 1639. 1800.
1821(51) 0.000384 1639. 1785.
1734(50) 0.000400 1638. 1753.
1768(51) 0.000384 1638. 1717.
1703(50) 0.000400 1637. 1688.
1667(49) 0.000416 1637. 1669.
1644(49) 0.000416 1637. 1658.
1661(49) 0.000416 1636. 1653.
1632(49) 0.000416 1636. 1651.
1592(48) 0.000434 1635. 1650.
1637(49) 0.000416 1635. 1649.
1602(48) 0.000434 1634. 1648.
1653(49) 0.000416 1634. 1648.
1628(49) 0.000416 1634. 1649.
1617(48) 0.000434 1633. 1651.
1711(50) 0.000400 1633. 1656.
1707(50) 0.000400 1632. 1666.
1710(50) 0.000400 1632. 1688.
1676(49) 0.000416 1632. 1724.
1832(52) 0.000370 1631. 1776.
1869(52) 0.000370 1631. 1836.
1846(52) 0.000370 1630. 1888.
2003(54) 0.0003429 1630. 1907.
1915(53) 0.000356 1629. 1881.
1751(50) 0.000400 1629. 1824.
1706(50) 0.000400 1629. 1759.
1697(50) 0.000400 1628. 1707.
1716(50) 0.000400 1628. 1673.
1681(49) 0.000416 1627. 1654.
1721(50) 0.000400 1627. 1645.
1672(49) 0.000416 1626. 1641.
1625(49) 0.000416 1626. 1638.
1616(48) 0.000434 1626. 1637.
1634(49) 0.000416 1625. 1636.
1631(49) 0.000416 1625. 1636.
1640(49) 0.000416 1624. 1635.
1613(48) 0.000434 1624. 1636.
1565(48) 0.000434 1623. 1637.
1556(47) 0.000453 1623. 1641.
1608(48) 0.000434 1623. 1646.
1689(50) 0.000400 1622. 1656.
1587(48) 0.000434 1622. 1668.
1558(48) 0.000434 1621. 1680.
1645(49) 0.000416 1621. 1689.
1675(49) 0.000416 1620. 1690.
1688(49) 0.000416 1620. 1685.
1620(48) 0.000434 1620. 1679.
1623(48) 0.000434 1619. 1681.
1712(50) 0.000400 1619. 1700.
1735(50) 0.000400 1618. 1748.
1862(52) 0.000370 1618. 1833.
1975(54) 0.0003429 1617. 1958.
2143(56) 0.0003189 1617. 2104.
2266(58) 0.0002973 1616. 2231.
2342(59) 0.0002873 1616. 2284.
2273(58) 0.0002973 1616. 2231.
2063(55) 0.0003306 1615. 2098.
1987(54) 0.0003429 1615. 1947.
1811(51) 0.000384 1614. 1828.
1745(50) 0.000400 1614. 1761.
1716(47) 0.000453 1613. 1744.
1797(48) 0.000434 1613. 1768.
1823(48) 0.000434 1612. 1819.
1835(49) 0.000416 1612. 1876.
1842(49) 0.000416 1612. 1913.
1880(49) 0.000416 1611. 1909.
1863(49) 0.000416 1611. 1863.
1777(48) 0.000434 1610. 1796.
1707(47) 0.000453 1610. 1735.
1700(47) 0.000453 1609. 1693.
1663(46) 0.000473 1609. 1675.
1661(46) 0.000473 1608. 1676.
1672(46) 0.000473 1608. 1693.
1733(47) 0.000453 1607. 1715.
1778(48) 0.000434 1607. 1734.
1729(47) 0.000453 1607. 1738.
1688(47) 0.000453 1606. 1724.
1641(46) 0.000473 1606. 1698.
1651(46) 0.000473 1605. 1670.
1611(45) 0.000494 1605. 1649.
1650(46) 0.000473 1604. 1635.
1639(46) 0.000473 1604. 1627.
1651(46) 0.000473 1603. 1625.
1643(46) 0.000473 1603. 1624.
1608(45) 0.000494 1602. 1625.
1661(46) 0.000473 1602. 1626.
1634(46) 0.000473 1602. 1629.
1655(46) 0.000473 1601. 1633.
1661(46) 0.000473 1601. 1642.
1766(48) 0.000434 1600. 1663.
1696(47) 0.000453 1600. 1704.
1807(48) 0.000434 1599. 1775.
1940(50) 0.000400 1599. 1882.
2023(51) 0.000384 1598. 2013.
2243(54) 0.0003429 1598. 2135.
2236(54) 0.0003429 1597. 2201.
2178(53) 0.000356 1597. 2175.
2057(52) 0.000370 1597. 2067.
1874(49) 0.000416 1596. 1928.
1799(48) 0.000434 1596. 1805.
1771(48) 0.000434 1595. 1718.
1681(46) 0.000473 1595. 1668.
1715(47) 0.000453 1594. 1643.
1682(46) 0.000473 1594. 1633.
1582(45) 0.000494 1593. 1629.
1583(45) 0.000494 1593. 1626.
1540(44) 0.000517 1592. 1624.
1578(45) 0.000494 1592. 1620.
1591(45) 0.000494 1592. 1615.
1597(45) 0.000494 1591. 1612.
1605(45) 0.000494 1591. 1609.
1631(46) 0.000473 1590. 1608.
1612(45) 0.000494 1590. 1607.
1561(45) 0.000494 1589. 1607.
1581(45) 0.000494 1589. 1607.
1650(46) 0.000473 1588. 1608.
1644(46) 0.000473 1588. 1610.
1628(46) 0.000473 1587. 1614.
1628(46) 0.000473 1587. 1622.
1590(45) 0.000494 1586. 1637.
1659(46) 0.000473 1586. 1666.
1720(47) 0.000453 1586. 1714.
1784(48) 0.000434 1585. 1783.
1836(49) 0.000416 1585. 1865.
1937(50) 0.000400 1584. 1938.
1938(50) 0.000400 1584. 1973.
1944(50) 0.000400 1583. 1952.
1861(49) 0.000416 1583. 1887.
1833(49) 0.000416 1582. 1809.
1745(47) 0.000453 1582. 1749.
1752(47) 0.000453 1581. 1721.
1735(47) 0.000453 1581. 1728.
1751(47) 0.000453 1580. 1763.
1763(48) 0.000434 1580. 1813.
1779(48) 0.000434 1580. 1858.
1899(50) 0.000400 1579. 1879.
1814(48) 0.000434 1579. 1866.
1777(48) 0.000434 1578. 1836.
1784(48) 0.000434 1578. 1822.
1827(49) 0.000416 1577. 1857.
1872(49) 0.000416 1577. 1969.
2172(53) 0.000356 1576. 2173.
2442(56) 0.0003189 1576. 2454.
2725(60) 0.0002778 1575. 2753.
2914(62) 0.0002601 1575. 2968.
2986(62) 0.0002601 1575. 2996.
2876(61) 0.0002687 1574. 2816.
2406(56) 0.0003189 1574. 2521.
2155(53) 0.000356 1573. 2234.
2001(51) 0.000384 1573. 2031.
1861(49) 0.000416 1572. 1937.
1851(49) 0.000416 1572. 1941.
1967(50) 0.000400 1571. 2007.
2041(51) 0.000384 1571. 2090.
2108(52) 0.000370 1570. 2137.
2087(52) 0.000370 1570. 2114.
1988(51) 0.000384 1569. 2030.
1881(49) 0.000416 1569. 1927.
1846(49) 0.000416 1569. 1850.
1829(49) 0.000416 1568. 1826.
1914(47) 0.000453 1568. 1863.
2080(49) 0.000416 1567. 1951.
2185(50) 0.000400 1567. 2064.
2272(51) 0.000384 1566. 2156.
2251(51) 0.000384 1566. 2181.
2221(50) 0.000400 1565. 2120.
2138(50) 0.000400 1565. 2004.
1955(47) 0.000453 1564. 1883.
1834(46) 0.000473 1564. 1795.
1752(45) 0.000494 1564. 1753.
1768(45) 0.000494 1563. 1757.
1782(45) 0.000494 1563. 1790.
1783(45) 0.000494 1562. 1832.
1849(46) 0.000473 1562. 1857.
1832(46) 0.000473 1561. 1846.
1780(45) 0.000494 1561. 1802.
1653(43) 0.000541 1560. 1747.
1692(44) 0.000517 1560. 1702.
1668(44) 0.000517 1560. 1679.
1613(43) 0.000541 1559. 1682.
1631(43) 0.000541 1559. 1706.
1713(44) 0.000517 1558. 1739.
1786(45) 0.000494 1558. 1765.
1823(46) 0.000473 1557. 1768.
1773(45) 0.000494 1557. 1744.
1732(44) 0.000517 1556. 1703.
1677(44) 0.000517 1556. 1660.
1634(43) 0.000541 1556. 1625.
1595(43) 0.000541 1555. 1601.
1562(42) 0.000567 1555. 1587.
1536(42) 0.000567 1554. 1580.
1536(42) 0.000567 1554. 1577.
1519(42) 0.000567 1553. 1575.
1576(42) 0.000567 1553. 1575.
1553(42) 0.000567 1552. 1576.
1562(42) 0.000567 1552. 1579.
1625(43) 0.000541 1552. 1587.
1620(43) 0.000541 1551. 1599.
1712(44) 0.000517 1551. 1617.
1632(43) 0.000541 1550. 1640.
1674(44) 0.000517 1550. 1662.
1633(43) 0.000541 1549. 1676.
1628(43) 0.000541 1549. 1678.
1616(43) 0.000541 1548. 1670.
1646(43) 0.000541 1548. 1665.
1685(44) 0.000517 1548. 1676.
1723(44) 0.000517 1547. 1716.
1811(45) 0.000494 1547. 1788.
1929(47) 0.000453 1546. 1887.
2065(49) 0.000416 1546. 1989.
2102(49) 0.000416 1545. 2058.
1986(48) 0.000434 1545. 2060.
1875(46) 0.000473 1544. 1992.
1848(46) 0.000473 1544. 1887.
1768(45) 0.000494 1544. 1781.
1689(44) 0.000517 1543. 1699.
1690(44) 0.000517 1543. 1647.
1662(44) 0.000517 1542. 1620.
1624(43) 0.000541 1542. 1609.
1578(42) 0.000567 1541. 1606.
1614(43) 0.000541 1541. 1608.
1580(42) 0.000567 1541. 1614.
1641(43) 0.000541 1540. 1630.
1666(44) 0.000517 1540. 1665.
1741(45) 0.000494 1539. 1731.
1814(46) 0.000473 1539. 1834.
1968(47) 0.000453 1538. 1967.
2097(49) 0.000416 1538. 2106.
2124(49) 0.000416 1538. 2206.
2125(49) 0.000416 1537. 2223.
2147(50) 0.000400 1537. 2144.
1957(47) 0.000453 1536. 2007.
1896(47) 0.000453 1536. 1864.
1784(45) 0.000494 1535. 1747.
1671(44) 0.000517 1535. 1667.
1578(42) 0.000567 1535. 1621.
1577(42) 0.000567 1534. 1597.
1582(42) 0.000567 1534. 1587.
1561(42) 0.000567 1533. 1585.
1564(42) 0.000567 1533. 1591.
1657(43) 0.000541 1533. 1608.
1659(43) 0.000541 1532. 1643.
1746(45) 0.000494 1532. 1705.
1817(46) 0.000473 1531. 1797.
1942(47) 0.000453 1531. 1916.
2035(48) 0.000434 1530. 2037.
2188(50) 0.000400 1530. 2124.
2212(50) 0.000400 1530. 2139.
2067(49) 0.000416 1529. 2073.
1963(47) 0.000453 1529. 1959.
1830(46) 0.000473 1528. 1844.
1790(45) 0.000494 1528. 1759.
1783(45) 0.000494 1528. 1714.
1751(45) 0.000494 1527. 1704.
1712(44) 0.000517 1527. 1714.
1767(45) 0.000494 1526. 1724.
1802(45) 0.000494 1526. 1719.
1740(45) 0.000494 1525. 1694.
1740(45) 0.000494 1525. 1658.
1664(44) 0.000517 1525. 1621.
1572(40) 0.000625 1524. 1591.
1640(41) 0.000595 1524. 1571.
1622(41) 0.000595 1523. 1559.
1585(40) 0.000625 1523. 1552.
1549(40) 0.000625 1523. 1550.
1588(40) 0.000625 1522. 1549.
1561(40) 0.000625 1522. 1550.
1625(41) 0.000595 1521. 1554.
1624(41) 0.000595 1521. 1561.
1604(40) 0.000625 1521. 1573.
1701(42) 0.000567 1520. 1591.
1617(41) 0.000595 1520. 1612.
1603(40) 0.000625 1519. 1631.
1648(41) 0.000595 1519. 1644.
1606(41) 0.000595 1519. 1647.
1641(41) 0.000595 1518. 1644.
1690(42) 0.000567 1518. 1648.
1682(41) 0.000595 1517. 1669.
1652(41) 0.000595 1517. 1715.
1777(43) 0.000541 1517. 1785.
1860(44) 0.000517 1516. 1868.
1997(45) 0.000494 1516. 1938.
2008(45) 0.000494 1516. 1970.
1930(44) 0.000517 1515. 1950.
1971(45) 0.000494 1515. 1898.
1879(44) 0.000517 1514. 1850.
1864(44) 0.000517 1514. 1838.
1864(44) 0.000517 1514. 1876.
1995(45) 0.000494 1513. 1959.
2049(46) 0.000473 1513. 2059.
2053(46) 0.000473 1512. 2135.
2103(46) 0.000473 1512. 2144.
2040(46) 0.000473 1512. 2074.
1980(45) 0.000494 1511. 1956.
1753(42) 0.000567 1511. 1831.
1668(41) 0.000595 1510. 1728.
1654(41) 0.000595 1510. 1656.
1569(40) 0.000625 1510. 1615.
1573(40) 0.000625 1509. 1594.
1503(39) 0.000657 1509. 1585.
1555(40) 0.000625 1509. 1580.
1608(41) 0.000595 1508. 1579.
1556(40) 0.000625 1508. 1585.
1521(39) 0.000657 1507. 1601.
1546(40) 0.000625 1507. 1631.
1632(41) 0.000595 1507. 1674.
1667(41) 0.000595 1506. 1721.
1688(42) 0.000567 1506. 1759.
1726(42) 0.000567 1506. 1772.
1701(42) 0.000567 1505. 1754.
1641(41) 0.000595 1505. 1714.
1646(41) 0.000595 1504. 1669.
1609(41) 0.000595 1504. 1634.
1552(40) 0.000625 1504. 1615.
1542(40) 0.000625 1503. 1612.
1611(41) 0.000595 1503. 1616.
1618(41) 0.000595 1503. 1621.
1580(40) 0.000625 1502. 1617.
1588(40) 0.000625 1502. 1604.
1566(40) 0.000625 1502. 1587.
1573(40) 0.000625 1501. 1572.
1542(40) 0.000625 1501. 1562.
1576(40) 0.000625 1500. 1559.
1534(40) 0.000625 1500. 1561.
1586(40) 0.000625 1500. 1565.
1581(40) 0.000625 1499. 1565.
1537(40) 0.000625 1499. 1561.
1599(40) 0.000625 1499. 1552.
1588(40) 0.000625 1498. 1543.
1538(40) 0.000625 1498. 1534.
1568(40) 0.000625 1498. 1528.
1498(39) 0.000657 1497. 1524.
1525(39) 0.000657 1497. 1522.
1531(40) 0.000625 1497. 1521.
1571(40) 0.000625 1496. 1522.
1507(39) 0.000657 1496. 1523.
1511(39) 0.000657 1495. 1526.
1534(40) 0.000625 1495. 1531.
1563(40) 0.000625 1495. 1537.
1614(41) 0.000595 1494. 1546.
1615(41) 0.000595 1494. 1555.
1574(40) 0.000625 1494. 1567.
1573(40) 0.000625 1493. 1580.
1586(40) 0.000625 1493. 1601.
1611(41) 0.000595 1493. 1636.
1697(42) 0.000567 1492. 1696.
1816(43) 0.000541 1492. 1791.
1962(45) 0.000494 1492. 1919.
2174(47) 0.000453 1491. 2066.
2256(48) 0.000434 1491. 2201.
2327(49) 0.000416 1491. 2281.
2326(49) 0.000416 1490. 2282.
2249(48) 0.000434 1490. 2222.
2209(48) 0.000434 1490. 2159.
2141(47) 0.000453 1489. 2145.
2188(47) 0.000453 1489. 2207.
2310(49) 0.000416 1489. 2337.
2507(51) 0.000384 1488. 2492.
2545(51) 0.000384 1488. 2602.
2505(51) 0.000384 1488. 2603.
2354(48) 0.000434 1487. 2485.
2256(47) 0.000453 1487. 2300.
2112(45) 0.000494 1487. 2114.
1985(44) 0.000517 1486. 1972.
1959(43) 0.000541 1486. 1888.
1909(43) 0.000541 1486. 1854.
1913(43) 0.000541 1485. 1844.
1877(42) 0.000567 1485. 1829.
1809(42) 0.000567 1485. 1793.
1746(41) 0.000595 1484. 1739.
1679(40) 0.000625 1484. 1681.
1663(40) 0.000625 1484. 1632.
1596(39) 0.000657 1483. 1595.
1592(39) 0.000657 1483. 1572.
1640(40) 0.000625 1483. 1560.
1551(38) 0.000693 1482. 1554.
1587(39) 0.000657 1482. 1553.
1580(39) 0.000657 1482. 1555.
1577(39) 0.000657 1481. 1565.
1574(39) 0.000657 1481. 1584.
1636(39) 0.000657 1481. 1613.
1618(39) 0.000657 1480. 1647.
1664(40) 0.000625 1480. 1679.
1655(40) 0.000625 1480. 1698.
1636(39) 0.000657 1480. 1695.
1658(40) 0.000625 1479. 1672.
1576(39) 0.000657 1479. 1639.
1691(40) 0.000625 1479. 1609.
1639(40) 0.000625 1478. 1589.
1592(39) 0.000657 1478. 1579.
1694(40) 0.000625 1478. 1576.
1725(41) 0.000595 1477. 1576.
1637(40) 0.000625 1477. 1572.
1707(40) 0.000625 1477. 1563.
1716(40) 0.000625 1476. 1550.
1646(40) 0.000625 1476. 1537.
1570(39) 0.000657 1476. 1527.
1565(39) 0.000657 1476. 1520.
1606(39) 0.000657 1475. 1518.
1575(39) 0.000657 1475. 1520.
1542(38) 0.000693 1475. 1528.
1561(39) 0.000657 1474. 1545.
1585(39) 0.000657 1474. 1575.
1612(39) 0.000657 1474. 1619.
1684(40) 0.000625 1473. 1679.
1737(41) 0.000595 1473. 1748.
1833(42) 0.000567 1473. 1815.
1761(41) 0.000595 1473. 1861.
1840(42) 0.000567 1472. 1875.
1808(42) 0.000567 1472. 1866.
1863(42) 0.000567 1472. 1859.
1873(42) 0.000567 1471. 1880.
1985(44) 0.000517 1471. 1941.
2028(44) 0.000517 1471. 2035.
2173(46) 0.000473 1470. 2135.
2244(46) 0.000473 1470. 2200.
2222(46) 0.000473 1470. 2190.
2187(46) 0.000473 1470. 2105.
2038(44) 0.000517 1469. 1979.
1865(42) 0.000567 1469. 1851.
1858(42) 0.000567 1469. 1745.
1690(40) 0.000625 1468. 1670.
1639(40) 0.000625 1468. 1624.
1584(39) 0.000657 1468. 1597.
1587(39) 0.000657 1468. 1578.
1600(39) 0.000657 1467. 1562.
1605(39) 0.000657 1467. 1546.
1594(39) 0.000657 1467. 1532.
1555(38) 0.000693 1466. 1521.
1478(37) 0.000730 1466. 1514.
1485(38) 0.000693 1466. 1510.
1511(38) 0.000693 1466. 1509.
1518(38) 0.000693 1465. 1512.
1470(37) 0.000730 1465. 1519.
1641(40) 0.000625 1465. 1532.
1584(39) 0.000657 1464. 1553.
1594(39) 0.000657 1464. 1582.
1635(39) 0.000657 1464. 1617.
1710(40) 0.000625 1464. 1650.
1759(41) 0.000595 1463. 1673.
1732(41) 0.000595 1463. 1677.
1667(40) 0.000625 1463. 1664.
1741(41) 0.000595 1463. 1642.
1660(40) 0.000625 1462. 1624.
1622(39) 0.000657 1462. 1616.
1561(39) 0.000657 1462. 1619.
1606(39) 0.000657 1461. 1629.
1671(40) 0.000625 1461. 1642.
1636(40) 0.000625 1461. 1650.
1646(40) 0.000625 1461. 1658.
1646(40) 0.000625 1460. 1675.
1716(40) 0.000625 1460. 1709.
1803(42) 0.000567 1460. 1765.
1886(43) 0.000541 1460. 1834.
1913(43) 0.000541 1459. 1902.
1946(43) 0.000541 1459. 1941.
1924(43) 0.000541 1459. 1932.
1883(42) 0.000567 1458. 1876.
1844(42) 0.000567 1458. 1794.
1751(41) 0.000595 1458. 1709.
1668(39) 0.000657 1458. 1637.
1630(38) 0.000693 1457. 1583.
1556(37) 0.000730 1457. 1549.
1493(36) 0.000772 1457. 1532.
1478(36) 0.000772 1457. 1528.
1518(37) 0.000730 1456. 1536.
1504(37) 0.000730 1456. 1557.
1617(38) 0.000693 1456. 1588.
1582(37) 0.000730 1456. 1629.
1650(38) 0.000693 1455. 1674.
1722(39) 0.000657 1455. 1713.
1692(39) 0.000657 1455. 1735.
1772(40) 0.000625 1455. 1734.
1736(39) 0.000657 1454. 1714.
1657(38) 0.000693 1454. 1691.
1674(39) 0.000657 1454. 1676.
1686(39) 0.000657 1454. 1674.
1696(39) 0.000657 1453. 1686.
1706(39) 0.000657 1453. 1705.
1705(39) 0.000657 1453. 1726.
1741(39) 0.000657 1453. 1747.
1773(40) 0.000625 1452. 1779.
1810(40) 0.000625 1452. 1836.
1945(42) 0.000567 1452. 1925.
2149(44) 0.000517 1452. 2040.
2122(44) 0.000517 1451. 2162.
2282(45) 0.000494 1451. 2253.
2302(45) 0.000494 1451. 2276.
2225(45) 0.000494 1451. 2217.
2118(44) 0.000517 1450. 2103.
2074(43) 0.000541 1450. 1974.
1892(41) 0.000595 1450. 1860.
1778(40) 0.000625 1450. 1775.
1698(39) 0.000657 1449. 1719.
1601(38) 0.000693 1449. 1683.
1684(39) 0.000657 1449. 1653.
1672(39) 0.000657 1449. 1622.
1582(37) 0.000730 1448. 1589.
1567(37) 0.000730 1448. 1558.
1529(37) 0.000730 1448. 1532.
1548(37) 0.000730 1448. 1511.
1463(36) 0.000772 1447. 1496.
1431(36) 0.000772 1447. 1487.
1516(37) 0.000730 1447. 1481.
1486(36) 0.000772 1447. 1477.
1493(36) 0.000772 1446. 1475.
1506(37) 0.000730 1446. 1475.
1500(36) 0.000772 1446. 1475.
1458(36) 0.000772 1446. 1476.
1490(36) 0.000772 1445. 1479.
1476(36) 0.000772 1445. 1484.
1493(36) 0.000772 1445. 1491.
1511(37) 0.000730 1445. 1504.
1514(37) 0.000730 1444. 1522.
1572(37) 0.000730 1444. 1547.
1582(37) 0.000730 1444. 1575.
1647(38) 0.000693 1444. 1603.
1705(39) 0.000657 1444. 1623.
1685(39) 0.000657 1443. 1628.
1629(38) 0.000693 1443. 1614.
1645(38) 0.000693 1443. 1589.
1575(37) 0.000730 1443. 1559.
1557(37) 0.000730 1442. 1531.
1544(37) 0.000730 1442. 1509.
1495(36) 0.000772 1442. 1494.
1449(36) 0.000772 1442. 1485.
1464(36) 0.000772 1441. 1482.
1453(36) 0.000772 1441. 1484.
1488(36) 0.000772 1441. 1489.
1532(37) 0.000730 1441. 1499.
1567(37) 0.000730 1440. 1512.
1637(38) 0.000693 1440. 1528.
1599(38) 0.000693 1440. 1546.
1537(37) 0.000730 1440. 1566.
1643(38) 0.000693 1440. 1591.
1599(38) 0.000693 1439. 1625.
1669(39) 0.000657 1439. 1675.
1732(39) 0.000657 1439. 1742.
1810(40) 0.000625 1439. 1820.
1814(40) 0.000625 1438. 1897.
1920(41) 0.000595 1438. 1952.
1942(42) 0.000567 1438. 1964.
1870(41) 0.000595 1438. 1930.
1841(41) 0.000595 1438. 1864.
1805(40) 0.000625 1437. 1791.
1772(40) 0.000625 1437. 1726.
1762(40) 0.000625 1437. 1677.
1696(39) 0.000657 1437. 1644.
1633(38) 0.000693 1436. 1622.
1683(39) 0.000657 1436. 1604.
1618(38) 0.000693 1436. 1589.
1597(38) 0.000693 1436. 1576.
1569(37) 0.000730 1435. 1569.
1622(38) 0.000693 1435. 1568.
1626(38) 0.000693 1435. 1571.
1655(38) 0.000693 1435. 1576.
1563(37) 0.000730 1435. 1577.
1594(38) 0.000693 1434. 1575.
1596(38) 0.000693 1434. 1569.
1643(38) 0.000693 1434. 1566.
1575(52) 0.000370 1434. 1568.
1568(36) 0.000772 1433. 1575.
1601(36) 0.000772 1433. 1585.
1648(37) 0.000730 1433. 1596.
1573(36) 0.000772 1433. 1606.
1597(36) 0.000772 1433. 1615.
1626(37) 0.000730 1432. 1628.
1674(37) 0.000730 1432. 1651.
1729(38) 0.000693 1432. 1682.
1744(38) 0.000693 1432. 1716.
1766(38) 0.000693 1431. 1743.
1786(39) 0.000657 1431. 1751.
1731(38) 0.000693 1431. 1732.
1751(38) 0.000693 1431. 1692.
1708(38) 0.000693 1431. 1643.
1622(37) 0.000730 1430. 1594.
1579(36) 0.000772 1430. 1552.
1558(36) 0.000772 1430. 1520.
1514(35) 0.000816 1429.7 1497.4
1467(35) 0.000816 1429.5 1482.4
1486(35) 0.000816 1429.3 1472.6
1420(34) 0.000865 1429.1 1466.2
1412(34) 0.000865 1428.9 1462.2
1440(35) 0.000816 1428.7 1460.1
1439(35) 0.000816 1428.4 1459.7
1422(34) 0.000865 1428.2 1461.6
1422(34) 0.000865 1428.0 1466.3
1488(35) 0.000816 1427.8 1474.9
1450(35) 0.000816 1427.6 1488.1
1482(35) 0.000816 1427.4 1506.3
1488(35) 0.000816 1427.1 1529.1
1473(35) 0.000816 1426.9 1554.8
1522(36) 0.000772 1427. 1580.
1591(36) 0.000772 1426. 1600.
1593(36) 0.000772 1426. 1612.
1638(37) 0.000730 1426. 1619.
1619(37) 0.000730 1426. 1626.
1584(36) 0.000772 1426. 1637.
1650(37) 0.000730 1425. 1655.
1702(38) 0.000693 1425. 1676.
1678(37) 0.000730 1425. 1693.
1747(38) 0.000693 1425. 1699.
1763(38) 0.000693 1425. 1688.
1659(37) 0.000730 1424. 1665.
1634(37) 0.000730 1424. 1639.
1608(37) 0.000730 1424. 1616.
1611(37) 0.000730 1424. 1600.
1571(36) 0.000772 1423. 1590.
1590(36) 0.000772 1423. 1586.
1561(36) 0.000772 1423. 1582.
1550(36) 0.000772 1423. 1581.
1572(36) 0.000772 1423. 1583.
1606(37) 0.000730 1422. 1590.
1613(37) 0.000730 1422. 1603.
1596(36) 0.000772 1422. 1619.
1578(36) 0.000772 1422. 1633.
1595(36) 0.000772 1422. 1640.
1637(37) 0.000730 1421. 1638.
1688(37) 0.000730 1421. 1632.
1653(37) 0.000730 1421. 1628.
1610(37) 0.000730 1421. 1628.
1614(37) 0.000730 1420. 1633.
1654(37) 0.000730 1420. 1638.
1648(37) 0.000730 1420. 1637.
1634(37) 0.000730 1420. 1626.
1635(37) 0.000730 1420. 1605.
1552(36) 0.000772 1419. 1580.
1526(36) 0.000772 1419. 1555.
1474(35) 0.000816 1419.0 1534.6
1463(35) 0.000816 1418.8 1520.2
1499(35) 0.000816 1418.5 1511.8
1482(35) 0.000816 1418.3 1508.9
1513(35) 0.000816 1418.1 1511.0
1498(35) 0.000816 1417.9 1518.4
1535(36) 0.000772 1418. 1531.
1554(36) 0.000772 1417. 1547.
1578(36) 0.000772 1417. 1563.
1607(37) 0.000730 1417. 1575.
1572(36) 0.000772 1417. 1578.
1577(36) 0.000772 1417. 1569.
1572(36) 0.000772 1416. 1551.
1487(35) 0.000816 1416.2 1528.2
1531(36) 0.000772 1416. 1505.
1487(35) 0.000816 1415.7 1484.7
1473(35) 0.000816 1415.5 1468.6
1446(35) 0.000816 1415.3 1457.0
1460(35) 0.000816 1415.1 1449.5
1401(34) 0.000865 1414.9 1445.2
1378(34) 0.000865 1414.7 1443.4
1383(34) 0.000865 1414.5 1443.6
1422(34) 0.000865 1414.2 1445.9
1476(35) 0.000816 1414.0 1450.9
1432(35) 0.000816 1413.8 1459.7
1434(35) 0.000816 1413.6 1473.5
1518(36) 0.000772 1413. 1494.
1574(36) 0.000772 1413. 1521.
1618(37) 0.000730 1413. 1556.
1606(37) 0.000730 1413. 1594.
1660(37) 0.000730 1413. 1634.
1674(37) 0.000730 1412. 1668.
1706(38) 0.000693 1412. 1690.
1730(38) 0.000693 1412. 1699.
1673(37) 0.000730 1412. 1700.
1689(38) 0.000693 1411. 1698.
1669(37) 0.000730 1411. 1701.
1644(37) 0.000730 1411. 1707.
1660(37) 0.000730 1411. 1713.
1710(38) 0.000693 1411. 1711.
1632(37) 0.000730 1410. 1695.
1589(36) 0.000772 1410. 1666.
1611(37) 0.000730 1410. 1630.
1591(37) 0.000730 1410. 1593.
1559(36) 0.000772 1409. 1560.
1507(36) 0.000772 1409. 1533.
1518(36) 0.000772 1409. 1513.
1517(36) 0.000772 1409. 1496.
1523(36) 0.000772 1409. 1483.
1448(35) 0.000816 1408.4 1473.2
1448(35) 0.000816 1408.2 1465.4
1442(35) 0.000816 1407.9 1459.8
1437(35) 0.000816 1407.7 1456.2
1420(34) 0.000865 1407.5 1454.2
1412(34) 0.000865 1407.3 1453.5
1460(35) 0.000816 1407.1 1454.0
1447(35) 0.000816 1406.8 1455.8
1494(35) 0.000816 1406.6 1459.1
1474(35) 0.000816 1406.4 1463.9
1449(35) 0.000816 1406.2 1469.8
1490(35) 0.000816 1405.9 1476.2
1456(35) 0.000816 1405.7 1482.6
1471(35) 0.000816 1405.5 1488.7
1488(35) 0.000816 1405.3 1495.1
1523(36) 0.000772 1405. 1503.
1486(35) 0.000816 1404.8 1512.6
1526(36) 0.000772 1405. 1523.
1534(36) 0.000772 1404. 1531.
1547(36) 0.000772 1404. 1535.
1518(36) 0.000772 1404. 1532.
1491(35) 0.000816 1403.7 1521.7
1508(36) 0.000772 1403. 1507.
1492(35) 0.000816 1403.3 1492.3
1464(35) 0.000816 1403.0 1478.3
1435(35) 0.000816 1402.8 1467.0
1438(35) 0.000816 1402.6 1459.1
1448(35) 0.000816 1402.4 1454.9
1400(34) 0.000865 1402.1 1454.3
1394(34) 0.000865 1401.9 1457.6
1413(34) 0.000865 1401.7 1465.7
1473(35) 0.000816 1401.5 1480.3
1440(35) 0.000816 1401.2 1504.5
1479(35) 0.000816 1401.0 1542.5
1555(36) 0.000772 1401. 1599.
1614(37) 0.000730 1401. 1678.
1752(38) 0.000693 1400. 1779.
1854(39) 0.000657 1400. 1901.
2001(41) 0.000595 1400. 2033.
2164(43) 0.000541 1400. 2159.
2154(42) 0.000567 1399. 2255.
2225(43) 0.000541 1399. 2298.
2200(43) 0.000541 1399. 2276.
2151(42) 0.000567 1399. 2203.
2093(42) 0.000567 1398. 2103.
1974(41) 0.000595 1398. 1998.
1885(40) 0.000625 1398. 1903.
1757(38) 0.000693 1398. 1826.
1722(38) 0.000693 1398. 1766.
1688(38) 0.000693 1397. 1722.
1615(37) 0.000730 1397. 1690.
1637(37) 0.000730 1397. 1670.
1633(37) 0.000730 1397. 1659.
1652(37) 0.000730 1396. 1655.
1656(37) 0.000730 1396. 1653.
1658(37) 0.000730 1396. 1646.
1589(36) 0.000772 1396. 1631.
1622(37) 0.000730 1395. 1607.
1555(36) 0.000772 1395. 1577.
1537(36) 0.000772 1395. 1547.
1504(35) 0.000816 1394.8 1520.6
1497(35) 0.000816 1394.5 1499.8
1461(35) 0.000816 1394.3 1486.6
1441(35) 0.000816 1394.1 1481.7
1502(35) 0.000816 1393.8 1484.9
1478(35) 0.000816 1393.6 1495.2
1557(36) 0.000772 1393. 1510.
1555(36) 0.000772 1393. 1528.
1557(36) 0.000772 1393. 1545.
1635(37) 0.000730 1393. 1556.
1576(36) 0.000772 1392. 1559.
1587(36) 0.000772 1392. 1552.
1565(36) 0.000772 1392. 1539.
1532(36) 0.000772 1392. 1523.
1532(36) 0.000772 1391. 1506.
1531(36) 0.000772 1391. 1491.
1479(35) 0.000816 1390.9 1477.9
1471(35) 0.000816 1390.7 1466.4
1470(35) 0.000816 1390.5 1456.0
1396(34) 0.000865 1390.2 1446.5
1450(35) 0.000816 1390.0 1438.1
1415(34) 0.000865 1389.7 1430.9
1388(34) 0.000865 1389.5 1425.1
1408(28) 0.001276 1389.2 1420.8
1378(34) 0.000865 1389.0 1417.7
1384(34) 0.000865 1388.8 1416.1
1366(34) 0.000865 1388.5 1415.8
1355(34) 0.000865 1388.3 1416.8
1427(35) 0.000816 1388.0 1419.4
1405(34) 0.000865 1387.8 1423.9
1473(35) 0.000816 1387.5 1431.1
1416(34) 0.000865 1387.3 1441.4
1362(34) 0.000865 1387.0 1455.6
1466(35) 0.000816 1386.8 1473.7
1490(35) 0.000816 1386.5 1495.4
1499(35) 0.000816 1386.3 1519.5
1598(37) 0.000730 1386. 1544.
1556(36) 0.000772 1386. 1565.
1562(36) 0.000772 1386. 1580.
1507(36) 0.000772 1385. 1587.
1561(36) 0.000772 1385. 1587.
1563(36) 0.000772 1385. 1584.
1582(36) 0.000772 1385. 1581.
1538(36) 0.000772 1384. 1579.
1599(37) 0.000730 1384. 1579.
1541(36) 0.000772 1384. 1580.
1532(36) 0.000772 1384. 1580.
1539(36) 0.000772 1383. 1580.
1571(36) 0.000772 1383. 1582.
1663(37) 0.000730 1383. 1586.
1651(37) 0.000730 1382. 1591.
1586(36) 0.000772 1382. 1595.
1595(37) 0.000730 1382. 1595.
1565(36) 0.000772 1382. 1588.
1534(36) 0.000772 1381. 1575.
1620(37) 0.000730 1381. 1558.
1564(36) 0.000772 1381. 1539.
1553(36) 0.000772 1381. 1522.
1554(36) 0.000772 1380. 1507.
1524(36) 0.000772 1380. 1493.
1492(35) 0.000816 1379.9 1480.8
1512(36) 0.000772 1380. 1469.
1453(35) 0.000816 1379.4 1458.8
1461(35) 0.000816 1379.1 1449.9
1450(35) 0.000816 1378.9 1442.7
1383(34) 0.000865 1378.6 1437.1
1417(34) 0.000865 1378.3 1433.1
1436(35) 0.000816 1378.1 1430.3
1420(35) 0.000816 1377.8 1428.5
1405(34) 0.000865 1377.5 1427.7
1438(35) 0.000816 1377.3 1427.8
1447(35) 0.000816 1377.0 1428.5
1451(35) 0.000816 1376.7 1429.3
1408(34) 0.000865 1376.5 1429.6
1463(35) 0.000816 1376.2 1429.0
1412(34) 0.000865 1375.9 1427.5
1410(34) 0.000865 1375.7 1425.5
1415(34) 0.000865 1375.4 1424.0
1438(35) 0.000816 1375.1 1423.7
1426(35) 0.000816 1374.9 1425.5
1436(35) 0.000816 1374.6 1430.2
1437(35) 0.000816 1374.3 1438.2
1467(35) 0.000816 1374.1 1450.0
1465(35) 0.000816 1373.8 1465.6
1429(35) 0.000816 1373.5 1484.7
1484(35) 0.000816 1373.2 1506.6
1516(36) 0.000772 1373. 1530.
1503(35) 0.000816 1372.7 1553.5
1533(36) 0.000772 1372. 1576.
1520(36) 0.000772 1372. 1598.
1566(36) 0.000772 1372. 1621.
1596(37) 0.000730 1372. 1647.
1639(37) 0.000730 1371. 1677.
1625(37) 0.000730 1371. 1711.
1629(37) 0.000730 1371. 1746.
1651(37) 0.000730 1370. 1779.
1714(38) 0.000693 1370. 1811.
1797(39) 0.000657 1370. 1843.
1852(39) 0.000657 1370. 1876.
1850(39) 0.000657 1369. 1909.
1872(40) 0.000625 1369. 1936.
1907(40) 0.000625 1369. 1949.
1925(40) 0.000625 1369. 1937.
1908(40) 0.000625 1368. 1900.
1852(39) 0.000657 1368. 1842.
1767(38) 0.000693 1368. 1773.
1687(38) 0.000693 1367. 1701.
1615(37) 0.000730 1367. 1635.
1546(36) 0.000772 1367. 1578.
1508(36) 0.000772 1367. 1531.
1469(35) 0.000816 1366.3 1494.2
1448(35) 0.000816 1366.0 1466.9
1450(35) 0.000816 1365.7 1447.5
1440(35) 0.000816 1365.4 1434.1
1445(35) 0.000816 1365.1 1425.2
1450(35) 0.000816 1364.8 1419.7
1419(35) 0.000816 1364.5 1416.8
1439(35) 0.000816 1364.3 1416.0
1385(34) 0.000865 1364.0 1417.3
1380(34) 0.000865 1363.7 1420.4
1415(34) 0.000865 1363.4 1425.8
1429(35) 0.000816 1363.1 1433.6
1376(34) 0.000865 1362.8 1444.2
1467(49) 0.000416 1363. 1458.
1486(34) 0.000865 1362.2 1473.9
1478(34) 0.000865 1361.9 1493.0
1522(34) 0.000865 1361.6 1513.9
1551(35) 0.000816 1361.3 1535.1
1532(35) 0.000816 1361.1 1554.0
1517(34) 0.000865 1360.8 1567.5
1556(35) 0.000816 1360.5 1572.8
1561(35) 0.000816 1360.2 1569.5
1516(34) 0.000865 1359.9 1560.4
1546(35) 0.000816 1359.6 1549.6
1516(34) 0.000865 1359.3 1542.2
1466(34) 0.000865 1359.0 1542.6
1514(34) 0.000865 1358.7 1554.4
1517(34) 0.000865 1358.4 1579.7
1568(35) 0.000816 1358.1 1619.3
1640(36) 0.000772 1358. 1672.
1753(37) 0.000730 1357. 1733.
1889(38) 0.000693 1357. 1797.
1812(38) 0.000693 1357. 1855.
1917(39) 0.000657 1357. 1897.
1960(39) 0.000657 1356. 1913.
1959(39) 0.000657 1356. 1902.
1877(38) 0.000693 1356. 1867.
1911(39) 0.000657 1355. 1819.
1839(38) 0.000693 1355. 1768.
1796(37) 0.000730 1355. 1719.
1604(35) 0.000816 1354.5 1679.2
1638(36) 0.000772 1354. 1649.
1568(35) 0.000816 1353.8 1630.3
1634(36) 0.000772 1354. 1623.
1666(36) 0.000772 1353. 1625.
1689(36) 0.000772 1353. 1636.
1638(36) 0.000772 1353. 1653.
1684(36) 0.000772 1352. 1673.
1656(36) 0.000772 1352. 1691.
1738(37) 0.000730 1352. 1708.
1804(38) 0.000693 1351. 1723.
1745(37) 0.000730 1351. 1738.
1776(37) 0.000730 1351. 1751.
1735(37) 0.000730 1350. 1760.
1693(36) 0.000772 1350. 1762.
1695(36) 0.000772 1350. 1751.
1667(36) 0.000772 1349. 1728.
1680(36) 0.000772 1349. 1694.
1694(36) 0.000772 1349. 1655.
1631(36) 0.000772 1349. 1615.
1526(35) 0.000816 1348.2 1578.5
1518(34) 0.000865 1347.9 1546.5
1524(35) 0.000816 1347.6 1520.2
1512(34) 0.000865 1347.3 1499.7
1464(34) 0.000865 1347.0 1484.7
1507(34) 0.000865 1346.7 1474.6
1413(33) 0.000918 1346.3 1468.4
1432(33) 0.000918 1346.0 1464.7
1407(33) 0.000918 1345.7 1462.0
1488(34) 0.000865 1345.4 1459.1
1476(34) 0.000865 1345.1 1455.2
1441(34) 0.000865 1344.7 1450.6
1447(34) 0.000865 1344.4 1445.8
1434(33) 0.000918 1344.1 1440.9
1430(33) 0.000918 1343.8 1436.0
1457(34) 0.000865 1343.4 1430.9
1401(33) 0.000918 1343.1 1425.2
1441(34) 0.000865 1342.8 1419.0
1410(33) 0.000918 1342.5 1412.4
1415(33) 0.000918 1342.2 1406.1
1447(34) 0.000865 1341.8 1400.5
1421(33) 0.000918 1341.5 1396.0
1417(33) 0.000918 1341.2 1393.1
1409(33) 0.000918 1340.9 1391.9
1384(33) 0.000918 1340.5 1392.7
1430(33) 0.000918 1340.2 1395.9
1391(33) 0.000918 1339.9 1401.7
1438(34) 0.000865 1339.5 1410.8
1433(33) 0.000918 1339.2 1423.5
1458(34) 0.000865 1338.9 1440.3
1447(34) 0.000865 1338.6 1461.6
1492(34) 0.000865 1338.2 1487.9
1572(35) 0.000816 1337.9 1519.0
1580(35) 0.000816 1337.6 1554.6
1663(36) 0.000772 1337. 1594.
1659(36) 0.000772 1337. 1635.
1734(37) 0.000730 1337. 1675.
1720(37) 0.000730 1336. 1712.
1773(37) 0.000730 1336. 1747.
1867(38) 0.000693 1336. 1779.
1894(38) 0.000693 1335. 1810.
1842(38) 0.000693 1335. 1838.
1850(38) 0.000693 1335. 1859.
1810(38) 0.000693 1334. 1871.
1818(38) 0.000693 1334. 1868.
1785(37) 0.000730 1334. 1850.
1816(38) 0.000693 1333. 1822.
1769(37) 0.000730 1333. 1788.
1727(37) 0.000730 1333. 1752.
1704(36) 0.000772 1332. 1715.
1717(37) 0.000730 1332. 1678.
1657(36) 0.000772 1332. 1640.
1593(35) 0.000816 1331.2 1602.4
1565(35) 0.000816 1330.9 1566.1
1527(34) 0.000865 1330.5 1533.3
1505(34) 0.000865 1330.2 1505.8
1530(34) 0.000865 1329.8 1484.5
1446(33) 0.000918 1329.5 1469.9
1450(34) 0.000865 1329.1 1462.2
1505(34) 0.000865 1328.8 1460.5
1465(34) 0.000865 1328.5 1463.8
1496(34) 0.000865 1328.1 1470.3
1488(34) 0.000865 1327.8 1478.0
1511(34) 0.000865 1327.4 1484.3
1491(34) 0.000865 1327.1 1486.7
1459(34) 0.000865 1326.7 1483.8
1514(34) 0.000865 1326.4 1475.6
1497(34) 0.000865 1326.1 1463.2
1442(33) 0.000918 1325.7 1448.6
1485(34) 0.000865 1325.4 1433.6
1445(33) 0.000918 1325.0 1419.5
1394(33) 0.000918 1324.7 1407.5
1432(33) 0.000918 1324.3 1398.3
1432(33) 0.000918 1324.0 1392.3
1385(33) 0.000918 1323.6 1389.9
1391(33) 0.000918 1323.3 1391.3
1396(33) 0.000918 1322.9 1396.7
1415(33) 0.000918 1322.6 1406.4
1408(33) 0.000918 1322.2 1420.3
1374(33) 0.000918 1321.9 1438.4
1417(33) 0.000918 1321.5 1460.1
1510(34) 0.000865 1321.2 1484.6
1538(35) 0.000816 1320.8 1510.4
1575(35) 0.000816 1320.5 1535.7
1546(35) 0.000816 1320.1 1557.9
1652(36) 0.000772 1320. 1575.
1641(36) 0.000772 1319. 1586.
1604(35) 0.000816 1319.1 1591.6
1671(36) 0.000772 1319. 1594.
1600(35) 0.000816 1318.4 1597.2
1650(36) 0.000772 1318. 1602.
1583(35) 0.000816 1317.7 1609.3
1645(36) 0.000772 1317. 1620.
1677(36) 0.000772 1317. 1634.
1681(36) 0.000772 1317. 1650.
1702(36) 0.000772 1316. 1669.
1715(37) 0.000730 1316. 1688.
1661(36) 0.000772 1316. 1704.
1595(35) 0.000816 1315.2 1714.5
1677(36) 0.000772 1315. 1715.
1627(36) 0.000772 1314. 1706.
1667(36) 0.000772 1314. 1688.
1617(35) 0.000816 1313.7 1665.8
1564(35) 0.000816 1313.4 1645.3
1570(35) 0.000816 1313.0 1631.0
1640(36) 0.000772 1313. 1626.
1667(36) 0.000772 1312. 1633.
1612(35) 0.000816 1312.0 1651.4
1655(36) 0.000772 1312. 1680.
1766(37) 0.000730 1311. 1717.
1790(37) 0.000730 1311. 1757.
1755(37) 0.000730 1311. 1793.
1858(38) 0.000693 1310. 1819.
1826(38) 0.000693 1310. 1829.
1826(38) 0.000693 1309. 1821.
1904(39) 0.000657 1309. 1795.
1766(37) 0.000730 1309. 1759.
1716(37) 0.000730 1308. 1716.
1742(37) 0.000730 1308. 1672.
1637(36) 0.000772 1308. 1629.
1574(35) 0.000816 1307.3 1589.4
1532(34) 0.000865 1306.9 1554.2
1506(34) 0.000865 1306.5 1524.0
1515(34) 0.000865 1306.2 1498.9
1461(34) 0.000865 1305.8 1478.6
1443(33) 0.000918 1305.5 1462.4
1445(33) 0.000918 1305.1 1449.0
1453(34) 0.000865 1304.7 1437.5
1407(33) 0.000918 1304.4 1427.5
1444(33) 0.000918 1304.0 1418.9
1445(33) 0.000918 1303.6 1412.2
1378(33) 0.000918 1303.3 1408.1
1407(33) 0.000918 1302.9 1407.1
1416(33) 0.000918 1302.5 1409.4
1387(33) 0.000918 1302.2 1415.1
1421(33) 0.000918 1301.8 1424.1
1460(34) 0.000865 1301.4 1435.5
1436(33) 0.000918 1301.1 1448.6
1466(34) 0.000865 1300.7 1461.8
1491(34) 0.000865 1300.3 1473.5
1464(34) 0.000865 1300.0 1482.1
1484(34) 0.000865 1299.6 1486.4
1516(34) 0.000865 1299.2 1486.5
1509(34) 0.000865 1298.9 1483.8
1535(35) 0.000816 1298.5 1480.2
1507(34) 0.000865 1298.1 1477.9
1436(33) 0.000918 1297.8 1479.0
1470(34) 0.000865 1297.4 1484.7
1526(34) 0.000865 1297.0 1496.1
1510(34) 0.000865 1296.7 1514.0
1493(34) 0.000865 1296.3 1538.5
1561(35) 0.000816 1295.9 1569.2
1562(35) 0.000816 1295.6 1605.1
1683(36) 0.000772 1295. 1645.
1775(39) 0.000657 1295. 1685.
1732(38) 0.000693 1294. 1725.
1729(38) 0.000693 1294. 1764.
1803(39) 0.000657 1294. 1799.
1851(39) 0.000657 1293. 1830.
1910(40) 0.000625 1293. 1856.
1881(40) 0.000625 1293. 1872.
1950(40) 0.000625 1292. 1875.
1886(40) 0.000625 1292. 1863.
1886(40) 0.000625 1291. 1836.
1760(38) 0.000693 1291. 1798.
1813(39) 0.000657 1291. 1756.
1723(38) 0.000693 1290. 1713.
1664(37) 0.000730 1290. 1675.
1624(37) 0.000730 1290. 1644.
1580(36) 0.000772 1289. 1620.
1587(36) 0.000772 1289. 1604.
1603(37) 0.000730 1289. 1596.
1572(36) 0.000772 1288. 1593.
1530(36) 0.000772 1288. 1594.
1582(36) 0.000772 1287. 1594.
1544(36) 0.000772 1287. 1591.
1612(37) 0.000730 1287. 1583.
1542(36) 0.000772 1286. 1568.
1584(36) 0.000772 1286. 1549.
1542(36) 0.000772 1286. 1526.
1555(36) 0.000772 1285. 1503.
1491(35) 0.000816 1284.8 1478.9
1493(35) 0.000816 1284.5 1456.2
1498(35) 0.000816 1284.1 1435.1
1443(35) 0.000816 1283.7 1416.1
1437(35) 0.000816 1283.3 1399.8
1412(34) 0.000865 1283.0 1386.4
1376(34) 0.000865 1282.6 1376.3
1407(34) 0.000865 1282.2 1369.4
1426(35) 0.000816 1281.9 1365.8
1339(33) 0.000918 1281.5 1364.9
1380(34) 0.000865 1281.1 1366.7
1330(33) 0.000918 1280.7 1370.9
1310(33) 0.000918 1280.4 1376.9
1412(34) 0.000865 1280.0 1384.4
1386(34) 0.000865 1279.6 1392.6
1382(34) 0.000865 1279.3 1401.2
1418(34) 0.000865 1278.9 1409.5
1409(34) 0.000865 1278.5 1417.6
1382(34) 0.000865 1278.1 1425.4
1450(35) 0.000816 1277.8 1432.9
1411(34) 0.000865 1277.4 1439.9
1419(34) 0.000865 1277.0 1446.1
1415(34) 0.000865 1276.7 1451.0
1456(35) 0.000816 1276.3 1454.6
1447(35) 0.000816 1275.9 1457.5
1476(35) 0.000816 1275.5 1460.5
1489(35) 0.000816 1275.2 1464.5
1502(35) 0.000816 1274.8 1470.2
1455(35) 0.000816 1274.4 1477.8
1462(35) 0.000816 1274.1 1487.2
1522(36) 0.000772 1274. 1498.
1546(36) 0.000772 1273. 1511.
1513(36) 0.000772 1273. 1525.
1613(37) 0.000730 1273. 1539.
1476(35) 0.000816 1272.2 1552.4
1514(36) 0.000772 1272. 1563.
1576(36) 0.000772 1271. 1570.
1567(36) 0.000772 1271. 1573.
1612(37) 0.000730 1271. 1571.
1525(36) 0.000772 1270. 1567.
1500(35) 0.000816 1270.0 1561.7
1543(36) 0.000772 1270. 1556.
1610(37) 0.000730 1269. 1551.
1541(36) 0.000772 1269. 1545.
1531(36) 0.000772 1269. 1541.
1528(36) 0.000772 1268. 1537.
1495(35) 0.000816 1267.8 1533.5
1586(36) 0.000772 1267. 1531.
1563(36) 0.000772 1267. 1529.
1562(36) 0.000772 1267. 1526.
1515(36) 0.000772 1266. 1521.
1552(36) 0.000772 1266. 1514.
1527(36) 0.000772 1266. 1504.
1496(35) 0.000816 1265.2 1492.9
1434(35) 0.000816 1264.8 1480.5
1483(35) 0.000816 1264.5 1467.3
1536(36) 0.000772 1264. 1453.
1448(35) 0.000816 1263.7 1438.0
1469(35) 0.000816 1263.4 1422.0
1478(35) 0.000816 1263.0 1405.6
1454(35) 0.000816 1262.6 1389.3
1427(35) 0.000816 1262.3 1374.0
1388(34) 0.000865 1261.9 1360.2
1390(34) 0.000865 1261.5 1348.2
1398(34) 0.000865 1261.2 1338.4
1386(34) 0.000865 1260.8 1331.0
1378(34) 0.000865 1260.4 1325.9
1329(33) 0.000918 1260.1 1323.2
1281(33) 0.000918 1259.7 1322.9
1335(33) 0.000918 1259.3 1325.1
1322(33) 0.000918 1259.0 1329.7
1359(34) 0.000865 1258.6 1336.7
1327(34) 0.000865 1258.2 1346.1
1338(34) 0.000865 1257.9 1357.9
1325(34) 0.000865 1257.5 1371.8
1332(34) 0.000865 1257.2 1387.7
1430(35) 0.000816 1256.8 1405.2
1366(34) 0.000865 1256.4 1423.7
1408(35) 0.000816 1256.1 1442.6
1429(35) 0.000816 1255.7 1461.5
1544(36) 0.000772 1255. 1480.
1506(36) 0.000772 1255. 1498.
1549(36) 0.000772 1255. 1513.
1547(36) 0.000772 1254. 1526.
1546(36) 0.000772 1254. 1535.
1518(36) 0.000772 1254. 1539.
1554(36) 0.000772 1253. 1536.
1577(37) 0.000730 1253. 1529.
1584(37) 0.000730 1252. 1518.
1563(37) 0.000730 1252. 1505.
1523(36) 0.000772 1252. 1489.
1474(36) 0.000772 1251. 1473.
1490(36) 0.000772 1251. 1456.
1461(35) 0.000816 1250.7 1438.0
1447(35) 0.000816 1250.3 1421.1
1419(35) 0.000816 1250.0 1405.7
1403(35) 0.000816 1249.6 1392.6
1426(35) 0.000816 1249.2 1382.3
1377(34) 0.000865 1248.9 1375.2
1332(34) 0.000865 1248.5 1371.4
1393(35) 0.000816 1248.2 1370.7
1452(35) 0.000816 1247.8 1372.6
1386(34) 0.000865 1247.5 1376.8
1416(35) 0.000816 1247.1 1382.2
1384(34) 0.000865 1246.8 1388.0
1441(35) 0.000816 1246.4 1393.3
1429(35) 0.000816 1246.1 1397.2
1447(35) 0.000816 1245.7 1399.4
1460(35) 0.000816 1245.4 1399.9
1424(35) 0.000816 1245.0 1399.0
1328(34) 0.000865 1244.6 1397.0
1387(34) 0.000865 1244.3 1394.3
1385(34) 0.000865 1243.9 1391.2
1376(34) 0.000865 1243.6 1388.0
1419(35) 0.000816 1243.2 1385.2
1415(35) 0.000816 1242.9 1383.5
1355(34) 0.000865 1242.5 1383.9
1388(34) 0.000865 1242.2 1387.4
1377(34) 0.000865 1241.9 1394.4
1389(34) 0.000865 1241.5 1405.8
1358(34) 0.000865 1241.2 1421.9
1373(34) 0.000865 1240.8 1442.8
1387(34) 0.000865 1240.5 1468.4
1417(35) 0.000816 1240.1 1498.2
1477(36) 0.000772 1240. 1531.
1445(35) 0.000816 1239.4 1566.6
1549(36) 0.000772 1239. 1603.
1549(36) 0.000772 1239. 1638.
1644(38) 0.000693 1238. 1671.
1656(38) 0.000693 1238. 1703.
1683(38) 0.000693 1238. 1731.
1686(38) 0.000693 1237. 1756.
1773(39) 0.000657 1237. 1776.
1788(39) 0.000657 1237. 1789.
1742(39) 0.000657 1236. 1795.
1761(39) 0.000657 1236. 1792.
1861(40) 0.000625 1236. 1781.
1793(39) 0.000657 1235. 1765.
1801(39) 0.000657 1235. 1744.
1807(39) 0.000657 1235. 1720.
1762(39) 0.000657 1234. 1693.
1717(38) 0.000693 1234. 1665.
1681(38) 0.000693 1234. 1635.
1643(38) 0.000693 1233. 1605.
1580(37) 0.000730 1233. 1576.
1561(37) 0.000730 1233. 1549.
1633(37) 0.000730 1232. 1525.
1588(37) 0.000730 1232. 1505.
1491(36) 0.000772 1232. 1488.
1475(36) 0.000772 1231. 1475.
1441(35) 0.000816 1231.0 1464.9
1493(36) 0.000772 1231. 1458.
1505(36) 0.000772 1230. 1453.
1455(35) 0.000816 1230.0 1450.9
1446(35) 0.000816 1229.7 1449.2
1421(35) 0.000816 1229.3 1447.8
1466(35) 0.000816 1229.0 1446.1
1423(35) 0.000816 1228.7 1443.9
1436(35) 0.000816 1228.3 1441.2
1418(35) 0.000816 1228.0 1438.2
1430(35) 0.000816 1227.7 1434.7
1394(35) 0.000816 1227.4 1430.7
1404(35) 0.000816 1227.0 1425.8
1417(35) 0.000816 1226.7 1420.0
1419(35) 0.000816 1226.4 1413.4
1433(35) 0.000816 1226.1 1406.3
1402(35) 0.000816 1225.8 1398.9
1416(35) 0.000816 1225.4 1391.4
1419(35) 0.000816 1225.1 1383.7
1354(34) 0.000865 1224.8 1375.9
1342(34) 0.000865 1224.5 1368.1
1408(35) 0.000816 1224.2 1360.6
1350(34) 0.000865 1223.8 1354.0
1413(33) 0.000918 1223.5 1348.6
1366(33) 0.000918 1223.2 1345.0
1398(33) 0.000918 1222.9 1343.4
1416(33) 0.000918 1222.6 1344.0
1372(33) 0.000918 1222.3 1346.8
1329(32) 0.000977 1221.9 1351.6
1358(33) 0.000918 1221.6 1358.2
1382(33) 0.000918 1221.3 1366.1
1393(33) 0.000918 1221.0 1374.7
1410(33) 0.000918 1220.7 1383.4
1496(34) 0.000865 1220.4 1391.6
1455(34) 0.000865 1220.1 1399.0
1460(34) 0.000865 1219.8 1405.6
1448(34) 0.000865 1219.5 1411.7
1528(35) 0.000816 1219.1 1417.5
1575(35) 0.000816 1218.8 1423.3
1469(34) 0.000865 1218.5 1429.4
1488(34) 0.000865 1218.2 1435.8
1521(35) 0.000816 1217.9 1442.4
1507(34) 0.000865 1217.6 1449.4
1509(34) 0.000865 1217.3 1456.7
1540(35) 0.000816 1217.0 1464.3
1510(34) 0.000865 1216.7 1471.9
1505(34) 0.000865 1216.4 1479.0
1511(34) 0.000865 1216.1 1485.1
1551(35) 0.000816 1215.8 1489.8
1506(34) 0.000865 1215.5 1493.1
1504(34) 0.000865 1215.2 1495.0
1538(35) 0.000816 1214.9 1495.9
1561(35) 0.000816 1214.6 1495.9
1505(34) 0.000865 1214.3 1495.1
1511(34) 0.000865 1214.0 1493.4
1508(34) 0.000865 1213.7 1490.7
1522(35) 0.000816 1213.4 1487.2
1518(35) 0.000816 1213.1 1483.4
1492(34) 0.000865 1212.9 1479.6
1461(34) 0.000865 1212.6 1476.3
1536(35) 0.000816 1212.3 1473.6
1483(34) 0.000865 1212.0 1471.4
1426(33) 0.000918 1211.7 1469.9
1464(34) 0.000865 1211.4 1468.8
1454(34) 0.000865 1211.1 1468.5
1536(35) 0.000816 1210.8 1468.8
1509(34) 0.000865 1210.5 1469.8
1462(34) 0.000865 1210.3 1471.2
1514(34) 0.000865 1210.0 1472.7
1507(34) 0.000865 1209.7 1473.8
1514(34) 0.000865 1209.4 1474.3
1482(34) 0.000865 1209.1 1474.1
1492(34) 0.000865 1208.8 1473.2
1446(34) 0.000865 1208.6 1471.8
1471(34) 0.000865 1208.3 1469.8
1489(34) 0.000865 1208.0 1467.1
1432(34) 0.000865 1207.7 1463.9
1434(34) 0.000865 1207.5 1460.4
1446(34) 0.000865 1207.2 1457.5
1433(34) 0.000865 1206.9 1456.1
1476(34) 0.000865 1206.6 1457.3
1497(34) 0.000865 1206.4 1461.8
1474(34) 0.000865 1206.1 1470.5
1460(34) 0.000865 1205.8 1483.5
1461(34) 0.000865 1205.5 1500.8
1476(34) 0.000865 1205.3 1521.9
1540(35) 0.000816 1205.0 1546.0
1556(35) 0.000816 1204.7 1571.7
1616(36) 0.000772 1204. 1597.
1565(35) 0.000816 1204.2 1621.0
1647(36) 0.000772 1204. 1641.
1609(36) 0.000772 1204. 1657.
1617(36) 0.000772 1203. 1667.
1592(35) 0.000816 1203.1 1672.2
1636(36) 0.000772 1203. 1673.
1652(36) 0.000772 1203. 1670.
1660(36) 0.000772 1202. 1662.
1607(36) 0.000772 1202. 1651.
1543(35) 0.000816 1201.8 1636.8
1560(35) 0.000816 1201.6 1619.6
1487(34) 0.000865 1201.3 1600.4
1516(35) 0.000816 1201.1 1580.4
1512(34) 0.000865 1200.8 1560.3
1514(34) 0.000865 1200.6 1541.0
1527(35) 0.000816 1200.3 1522.6
1514(34) 0.000865 1200.1 1505.4
1456(34) 0.000865 1199.8 1489.6
1408(33) 0.000918 1199.6 1475.4
1398(33) 0.000918 1199.3 1462.9
1455(34) 0.000865 1199.1 1452.1
1390(33) 0.000918 1198.8 1443.0
1420(33) 0.000918 1198.6 1435.1
1414(33) 0.000918 1198.3 1428.2
1484(34) 0.000865 1198.1 1421.8
1487(34) 0.000865 1197.8 1415.8
1388(33) 0.000918 1197.6 1409.9
1380(33) 0.000918 1197.4 1403.8
1373(33) 0.000918 1197.1 1397.4
1373(33) 0.000918 1196.9 1390.3
1392(33) 0.000918 1196.6 1382.0
1401(33) 0.000918 1196.4 1372.7
1367(33) 0.000918 1196.2 1362.5
1333(44) 0.000517 1196. 1352.
1307(32) 0.000977 1195.7 1340.7
1285(31) 0.001041 1195.5 1330.0
1334(32) 0.000977 1195.2 1320.1
1342(32) 0.000977 1195.0 1311.1
1303(32) 0.000977 1194.8 1303.2
1321(32) 0.000977 1194.5 1296.4
1297(32) 0.000977 1194.3 1290.9
1326(32) 0.000977 1194.1 1286.4
1307(32) 0.000977 1193.8 1282.8
1292(32) 0.000977 1193.6 1280.1
1301(32) 0.000977 1193.4 1277.9
1202(30) 0.001111 1193.2 1276.3
1233(31) 0.001041 1192.9 1275.1
1282(31) 0.001041 1192.7 1274.5
1239(31) 0.001041 1192.5 1274.5
1249(31) 0.001041 1192.3 1275.3
1273(31) 0.001041 1192.1 1277.2
1270(31) 0.001041 1191.8 1280.2
1252(31) 0.001041 1191.6 1284.5
1270(31) 0.001041 1191.4 1290.2
1293(32) 0.000977 1191.2 1297.4
1297(32) 0.000977 1191.0 1305.8
1304(32) 0.000977 1190.8 1315.6
1322(32) 0.000977 1190.6 1326.6
1308(32) 0.000977 1190.3 1338.5
1379(33) 0.000918 1190.1 1351.2
1375(33) 0.000918 1189.9 1364.5
1347(32) 0.000977 1189.7 1378.3
1343(32) 0.000977 1189.5 1392.6
1409(33) 0.000918 1189.3 1407.3
1411(33) 0.000918 1189.1 1422.2
1420(33) 0.000918 1188.9 1437.3
1389(33) 0.000918 1188.7 1452.2
1455(34) 0.000865 1188.5 1467.1
1510(34) 0.000865 1188.3 1482.0
1466(34) 0.000865 1188.1 1497.3
1484(34) 0.000865 1187.9 1513.0
1540(35) 0.000816 1187.7 1529.4
1544(35) 0.000816 1187.5 1546.2
1545(35) 0.000816 1187.3 1563.2
1637(36) 0.000772 1187. 1580.
1608(35) 0.000816 1186.9 1595.8
1617(35) 0.000816 1186.7 1610.3
1648(36) 0.000772 1187. 1623.
1583(35) 0.000816 1186.3 1632.0
1591(35) 0.000816 1186.1 1637.4
1616(35) 0.000816 1186.0 1637.8
1621(35) 0.000816 1185.8 1632.6
1620(35) 0.000816 1185.6 1621.8
1591(35) 0.000816 1185.4 1606.1
1649(36) 0.000772 1185. 1587.
1635(36) 0.000772 1185. 1565.
1605(35) 0.000816 1184.8 1543.0
1551(35) 0.000816 1184.7 1521.5
1518(34) 0.000865 1184.5 1501.6
1449(33) 0.000918 1184.3 1484.1
1443(33) 0.000918 1184.1 1469.0
1438(33) 0.000918 1183.9 1456.5
1444(33) 0.000918 1183.8 1446.0
1407(33) 0.000918 1183.6 1436.9
1402(33) 0.000918 1183.4 1428.5
1381(33) 0.000918 1183.2 1419.8
1364(32) 0.000977 1183.1 1410.3
1374(33) 0.000918 1182.9 1399.6
1385(33) 0.000918 1182.7 1387.7
1409(33) 0.000918 1182.6 1374.7
1383(33) 0.000918 1182.4 1361.0
1368(32) 0.000977 1182.2 1347.1
1342(32) 0.000977 1182.1 1333.3
1338(32) 0.000977 1181.9 1320.1
1273(31) 0.001041 1181.7 1307.7
1270(31) 0.001041 1181.6 1296.4
1280(31) 0.001041 1181.4 1286.6
1277(31) 0.001041 1181.2 1278.3
1241(31) 0.001041 1181.1 1271.9
1235(31) 0.001041 1180.9 1267.4
1275(31) 0.001041 1180.8 1265.0
1286(31) 0.001041 1180.6 1264.7
1266(31) 0.001041 1180.5 1266.5
1295(32) 0.000977 1180.3 1270.5
1282(31) 0.001041 1180.2 1276.6
1305(32) 0.000977 1180.0 1284.7
1293(32) 0.000977 1179.8 1294.8
1289(31) 0.001041 1179.7 1306.8
1321(32) 0.000977 1179.5 1320.3
1294(32) 0.000977 1179.4 1335.3
1359(32) 0.000977 1179.3 1351.1
1429(33) 0.000918 1179.1 1367.5
1442(33) 0.000918 1179.0 1383.8
1419(33) 0.000918 1178.8 1399.6
1389(33) 0.000918 1178.7 1414.0
1404(33) 0.000918 1178.5 1426.7
1422(33) 0.000918 1178.4 1437.2
1470(34) 0.000865 1178.3 1445.4
1495(34) 0.000865 1178.1 1451.5
1467(34) 0.000865 1178.0 1455.6
1412(33) 0.000918 1177.8 1457.9
1434(33) 0.000918 1177.7 1458.5
1441(33) 0.000918 1177.6 1457.6
1444(33) 0.000918 1177.4 1455.4
1435(33) 0.000918 1177.3 1452.0
1410(33) 0.000918 1177.2 1448.0
1435(33) 0.000918 1177.0 1443.6
1441(33) 0.000918 1176.9 1439.2
1436(33) 0.000918 1176.8 1435.1
1429(33) 0.000918 1176.7 1431.4
1394(33) 0.000918 1176.5 1428.3
1390(33) 0.000918 1176.4 1425.8
1441(33) 0.000918 1176.3 1424.1
1414(33) 0.000918 1176.2 1423.1
1373(32) 0.000977 1176.0 1422.8
1387(33) 0.000918 1175.9 1423.3
1430(33) 0.000918 1175.8 1424.1
1386(33) 0.000918 1175.7 1425.2
1343(32) 0.000977 1175.6 1426.2
1398(33) 0.000918 1175.5 1426.9
1458(33) 0.000918 1175.3 1427.0
1395(33) 0.000918 1175.2 1426.3
1355(32) 0.000977 1175.1 1424.5
1351(32) 0.000977 1175.0 1421.4
1395(33) 0.000918 1174.9 1416.6
1369(32) 0.000977 1174.8 1409.9
1375(32) 0.000977 1174.7 1401.2
1363(32) 0.000977 1174.6 1390.7
1347(32) 0.000977 1174.5 1378.7
1361(32) 0.000977 1174.3 1365.6
1347(32) 0.000977 1174.2 1351.9
1347(32) 0.000977 1174.1 1338.0
1292(31) 0.001041 1174.0 1324.3
1291(31) 0.001041 1173.9 1311.2
1289(31) 0.001041 1173.8 1298.7
1273(31) 0.001041 1173.7 1287.3
1242(31) 0.001041 1173.6 1277.1
1217(30) 0.001111 1173.5 1268.2
1259(31) 0.001041 1173.4 1260.9
1226(31) 0.001041 1173.3 1255.1
1205(30) 0.001111 1173.3 1250.9
1222(31) 0.001041 1173.2 1248.4
1274(31) 0.001041 1173.1 1247.6
1206(30) 0.001111 1173.0 1248.3
1195(30) 0.001111 1172.9 1250.6
1224(31) 0.001041 1172.8 1254.4
1282(31) 0.001041 1172.7 1259.6
1260(31) 0.001041 1172.6 1266.0
1269(31) 0.001041 1172.5 1273.7
1276(31) 0.001041 1172.4 1282.3
1266(31) 0.001041 1172.4 1291.6
1320(32) 0.000977 1172.3 1301.5
1344(32) 0.000977 1172.2 1311.5
1340(32) 0.000977 1172.1 1321.3
1316(32) 0.000977 1172.0 1330.6
1362(32) 0.000977 1172.0 1339.1
1392(33) 0.000918 1171.9 1346.6
1377(32) 0.000977 1171.8 1352.8
1388(33) 0.000918 1171.7 1357.9
1386(33) 0.000918 1171.6 1361.7
1401(33) 0.000918 1171.6 1364.3
1385(33) 0.000918 1171.5 1365.7
1347(32) 0.000977 1171.4 1365.9
1358(32) 0.000977 1171.4 1364.9
1369(32) 0.000977 1171.3 1362.9
1383(33) 0.000918 1171.2 1360.1
1391(33) 0.000918 1171.1 1356.6
1349(32) 0.000977 1171.1 1352.7
1327(32) 0.000977 1171.0 1348.8
1358(32) 0.000977 1170.9 1344.9
1356(32) 0.000977 1170.9 1341.2
1381(33) 0.000918 1170.8 1337.7
1382(33) 0.000918 1170.8 1334.7
1364(32) 0.000977 1170.7 1332.1
1339(32) 0.000977 1170.6 1330.0
1337(32) 0.000977 1170.6 1328.4
1335(32) 0.000977 1170.5 1327.3
1329(32) 0.000977 1170.5 1326.4
1294(31) 0.001041 1170.4 1325.8
1284(31) 0.001041 1170.3 1325.2
1292(31) 0.001041 1170.3 1324.5
1316(32) 0.000977 1170.2 1323.6
1290(31) 0.001041 1170.2 1322.4
1274(31) 0.001041 1170.1 1320.6
1248(31) 0.001041 1170.1 1318.2
1290(31) 0.001041 1170.0 1315.1
1290(31) 0.001041 1170.0 1311.0
1282(31) 0.001041 1169.9 1306.1
1240(31) 0.001041 1169.9 1300.5
1237(31) 0.001041 1169.8 1294.1
1261(31) 0.001041 1169.8 1287.4
1264(31) 0.001041 1169.7 1280.5
1227(31) 0.001041 1169.7 1273.6
1214(30) 0.001111 1169.7 1266.9
1197(30) 0.001111 1169.6 1260.5
1226(31) 0.001041 1169.6 1254.8
1254(31) 0.001041 1169.5 1249.7
1227(31) 0.001041 1169.5 1245.4
1257(31) 0.001041 1169.4 1242.0
1256(31) 0.001041 1169.4 1239.6
1227(31) 0.001041 1169.4 1238.4
1212(30) 0.001111 1169.3 1238.3
1211(30) 0.001111 1169.3 1239.5
1220(31) 0.001041 1169.3 1242.0
1258(32) 0.000977 1169.2 1246.0
1236(32) 0.000977 1169.2 1251.4
1201(31) 0.001041 1169.2 1258.4
1212(31) 0.001041 1169.1 1266.9
1270(32) 0.000977 1169.1 1277.2
1301(32) 0.000977 1169.1 1289.2
1282(32) 0.000977 1169.1 1302.8
1328(33) 0.000918 1169.0 1318.1
1376(33) 0.000918 1169.0 1334.9
1372(33) 0.000918 1169.0 1353.2
1383(33) 0.000918 1168.9 1372.7
1355(33) 0.000918 1168.9 1393.2
1434(34) 0.000865 1168.9 1414.4
1473(35) 0.000816 1168.9 1435.9
1495(35) 0.000816 1168.9 1457.7
1475(35) 0.000816 1168.8 1479.1
1494(35) 0.000816 1168.8 1500.0
1526(35) 0.000816 1168.8 1519.9
1534(35) 0.000816 1168.8 1538.3
1582(36) 0.000772 1169. 1555.
1550(35) 0.000816 1168.7 1569.3
1597(36) 0.000772 1169. 1581.
1600(36) 0.000772 1169. 1590.
1633(36) 0.000772 1169. 1597.
1640(37) 0.000730 1169. 1601.
1627(36) 0.000772 1169. 1604.
1671(37) 0.000730 1169. 1604.
1609(36) 0.000772 1169. 1603.
1645(37) 0.000730 1169. 1600.
1646(37) 0.000730 1169. 1596.
1619(36) 0.000772 1169. 1591.
1605(36) 0.000772 1169. 1584.
1613(36) 0.000772 1169. 1577.
1649(37) 0.000730 1169. 1569.
1564(36) 0.000772 1169. 1560.
1590(36) 0.000772 1169. 1550.
1629(36) 0.000772 1169. 1540.
1610(36) 0.000772 1169. 1528.
1558(36) 0.000772 1169. 1516.
1514(35) 0.000816 1168.6 1504.0
1505(35) 0.000816 1168.6 1491.2
1480(35) 0.000816 1168.6 1478.2
1480(35) 0.000816 1168.6 1465.4
1458(34) 0.000865 1168.6 1452.6
1454(34) 0.000865 1168.6 1440.1
1429(34) 0.000865 1168.6 1427.9
1424(34) 0.000865 1168.6 1416.1
1456(34) 0.000865 1168.6 1404.8
1421(34) 0.000865 1168.6 1394.0
1392(34) 0.000865 1168.6 1383.9
1389(34) 0.000865 1168.6 1374.3
1349(33) 0.000918 1168.6 1365.4
1323(33) 0.000918 1168.6 1357.2
1347(33) 0.000918 1168.6 1349.8
1321(33) 0.000918 1168.6 1343.4
1332(33) 0.000918 1168.6 1338.0
1319(33) 0.000918 1168.6 1333.9
1357(33) 0.000918 1168.7 1331.2
1352(33) 0.000918 1168.7 1330.1
1312(33) 0.000918 1168.7 1330.7
1307(33) 0.000918 1168.7 1333.1
1311(33) 0.000918 1168.7 1337.4
1307(33) 0.000918 1168.7 1343.6
1329(33) 0.000918 1168.7 1351.6
1353(33) 0.000918 1168.7 1361.1
1361(33) 0.000918 1168.8 1372.1
1387(34) 0.000865 1168.8 1384.2
1382(33) 0.000918 1168.8 1397.0
1394(34) 0.000865 1168.8 1410.3
1368(33) 0.000918 1168.8 1423.6
1426(34) 0.000865 1168.8 1436.5
1494(35) 0.000816 1168.9 1448.5
1495(35) 0.000816 1168.9 1459.0
1506(35) 0.000816 1168.9 1467.7
1478(35) 0.000816 1168.9 1473.9
1486(35) 0.000816 1168.9 1477.2
1464(34) 0.000865 1169.0 1477.4
1487(35) 0.000816 1169.0 1474.3
1465(34) 0.000865 1169.0 1468.2
1464(34) 0.000865 1169.0 1459.3
1465(34) 0.000865 1169.0 1448.0
1438(34) 0.000865 1169.1 1435.0
1431(34) 0.000865 1169.1 1420.8
1471(35) 0.000816 1169.1 1405.8
1408(34) 0.000865 1169.1 1390.7
1348(33) 0.000918 1169.2 1375.6
1408(34) 0.000865 1169.2 1360.9
1320(33) 0.000918 1169.2 1347.0
1347(33) 0.000918 1169.3 1334.0
1339(33) 0.000918 1169.3 1322.2
1337(33) 0.000918 1169.3 1311.5
1343(33) 0.000918 1169.3 1302.1
1307(33) 0.000918 1169.4 1294.0
1278(32) 0.000977 1169.4 1287.2
1278(32) 0.000977 1169.4 1281.6
1316(33) 0.000918 1169.5 1277.4
1254(32) 0.000977 1169.5 1274.4
1342(33) 0.000918 1169.5 1272.5
1248(32) 0.000977 1169.6 1271.9
1305(27) 0.001372 1169.6 1272.3
1367(34) 0.000865 1169.6 1273.8
1296(33) 0.000918 1169.7 1276.3
1370(34) 0.000865 1169.7 1279.6
1318(34) 0.000865 1169.7 1283.6
1292(33) 0.000918 1169.8 1288.2
1275(33) 0.000918 1169.8 1293.3
1319(34) 0.000865 1169.8 1298.6
1387(34) 0.000865 1169.9 1304.0
1443(35) 0.000816 1169.9 1309.2
1393(34) 0.000865 1169.9 1314.1
1362(34) 0.000865 1170.0 1318.7
1344(34) 0.000865 1170.0 1322.6
1361(34) 0.000865 1170.1 1325.9
1346(34) 0.000865 1170.1 1328.3
1383(34) 0.000865 1170.1 1329.9
1428(35) 0.000816 1170.2 1330.5
1351(34) 0.000865 1170.2 1330.1
1420(35) 0.000816 1170.2 1328.6
1393(34) 0.000865 1170.3 1326.3
1404(35) 0.000816 1170.3 1323.2
1380(34) 0.000865 1170.4 1319.4
1386(34) 0.000865 1170.4 1315.4
1346(34) 0.000865 1170.4 1311.2
1403(35) 0.000816 1170.5 1307.1
1325(34) 0.000865 1170.5 1303.3
1339(34) 0.000865 1170.6 1300.1
1330(34) 0.000865 1170.6 1297.4
1293(33) 0.000918 1170.7 1295.4
1281(33) 0.000918 1170.7 1294.2
1258(33) 0.000918 1170.7 1293.8
1278(33) 0.000918 1170.8 1294.2
1311(33) 0.000918 1170.8 1295.3
1288(33) 0.000918 1170.9 1297.0
1296(33) 0.000918 1170.9 1299.4
1279(33) 0.000918 1171.0 1302.3
1240(33) 0.000918 1171.0 1305.7
1259(33) 0.000918 1171.0 1309.4
1300(33) 0.000918 1171.1 1313.4
1313(33) 0.000918 1171.1 1317.6
1289(33) 0.000918 1171.2 1321.9
1283(33) 0.000918 1171.2 1326.2
1282(33) 0.000918 1171.3 1330.5
1334(34) 0.000865 1171.3 1334.7
1348(34) 0.000865 1171.4 1338.8
1374(34) 0.000865 1171.4 1342.9
1363(34) 0.000865 1171.5 1347.0
1384(34) 0.000865 1171.5 1351.2
1377(34) 0.000865 1171.6 1355.4
1363(34) 0.000865 1171.6 1359.8
1360(34) 0.000865 1171.6 1364.4
1350(34) 0.000865 1171.7 1369.1
1367(34) 0.000865 1171.7 1373.9
1329(34) 0.000865 1171.8 1378.9
1447(35) 0.000816 1171.8 1383.8
1451(35) 0.000816 1171.9 1388.7
1432(35) 0.000816 1171.9 1393.5
1377(34) 0.000865 1172.0 1397.9
1377(34) 0.000865 1172.0 1402.0
1455(35) 0.000816 1172.1 1405.5
1447(35) 0.000816 1172.1 1408.6
1453(35) 0.000816 1172.2 1411.0
1436(35) 0.000816 1172.2 1413.0
1426(35) 0.000816 1172.3 1414.4
1488(36) 0.000772 1172. 1415.
1428(35) 0.000816 1172.4 1415.8
1452(35) 0.000816 1172.4 1416.0
1421(35) 0.000816 1172.5 1415.7
1406(35) 0.000816 1172.5 1415.0
1450(35) 0.000816 1172.6 1413.9
1421(35) 0.000816 1172.6 1412.4
1378(34) 0.000865 1172.6 1410.4
1381(34) 0.000865 1172.7 1407.9
1436(35) 0.000816 1172.7 1404.8
1420(35) 0.000816 1172.8 1401.2
1384(34) 0.000865 1172.8 1396.8
1395(35) 0.000816 1172.9 1391.8
1386(34) 0.000865 1172.9 1386.1
1383(34) 0.000865 1173.0 1379.8
1326(34) 0.000865 1173.0 1372.9
1331(34) 0.000865 1173.1 1365.7
1325(34) 0.000865 1173.1 1358.3
1330(34) 0.000865 1173.2 1350.8
1372(34) 0.000865 1173.2 1343.4
1318(34) 0.000865 1173.3 1336.2
1379(34) 0.000865 1173.3 1329.3
1305(33) 0.000918 1173.4 1322.9
1261(33) 0.000918 1173.4 1317.1
1296(33) 0.000918 1173.5 1311.9
1257(33) 0.000918 1173.5 1307.5
1345(34) 0.000865 1173.6 1303.9
1297(33) 0.000918 1173.6 1301.1
1295(33) 0.000918 1173.7 1299.1
1273(33) 0.000918 1173.7 1298.0
1278(33) 0.000918 1173.7 1297.8
1296(33) 0.000918 1173.8 1298.2
1293(33) 0.000918 1173.8 1299.3
1289(33) 0.000918 1173.9 1301.1
1292(33) 0.000918 1173.9 1303.3
1328(34) 0.000865 1174.0 1305.8
1306(33) 0.000918 1174.0 1308.6
1363(33) 0.000918 1174.1 1311.5
1309(33) 0.000918 1174.1 1314.5
1293(32) 0.000977 1174.2 1317.5
1297(32) 0.000977 1174.2 1320.4
1318(33) 0.000918 1174.3 1323.2
1353(33) 0.000918 1174.3 1325.9
1360(33) 0.000918 1174.3 1328.4
1359(33) 0.000918 1174.4 1330.9
1367(33) 0.000918 1174.4 1333.2
1358(33) 0.000918 1174.5 1335.4
1384(33) 0.000918 1174.5 1337.5
1404(34) 0.000865 1174.6 1339.5
1384(33) 0.000918 1174.6 1341.3
1322(33) 0.000918 1174.7 1343.0
1381(33) 0.000918 1174.7 1344.6
1420(34) 0.000865 1174.7 1346.0
1296(32) 0.000977 1174.8 1347.4
1309(33) 0.000918 1174.8 1348.7
1333(33) 0.000918 1174.9 1349.9
1361(33) 0.000918 1174.9 1351.2
1380(33) 0.000918 1174.9 1352.5
1372(33) 0.000918 1175.0 1354.1
1326(33) 0.000918 1175.0 1356.0
1326(33) 0.000918 1175.1 1358.3
1394(34) 0.000865 1175.1 1361.2
1404(34) 0.000865 1175.1 1364.7
1302(32) 0.000977 1175.2 1369.0
1368(33) 0.000918 1175.2 1374.0
1396(34) 0.000865 1175.3 1380.0
1375(33) 0.000918 1175.3 1386.7
1381(33) 0.000918 1175.3 1394.2
1407(34) 0.000865 1175.4 1402.5
1475(35) 0.000816 1175.4 1411.5
1416(34) 0.000865 1175.5 1421.0
1447(34) 0.000865 1175.5 1430.9
1439(34) 0.000865 1175.5 1441.0
1507(35) 0.000816 1175.6 1451.3
1486(35) 0.000816 1175.6 1461.6
1534(35) 0.000816 1175.6 1471.7
1515(35) 0.000816 1175.7 1481.6
1549(35) 0.000816 1175.7 1491.0
1532(35) 0.000816 1175.7 1499.8
1498(35) 0.000816 1175.8 1507.8
1505(35) 0.000816 1175.8 1515.0
1582(36) 0.000772 1176. 1521.
1528(35) 0.000816 1175.9 1526.0
1560(36) 0.000772 1176. 1530.
1524(35) 0.000816 1175.9 1532.0
1509(35) 0.000816 1176.0 1533.0
1605(36) 0.000772 1176. 1533.
1594(36) 0.000772 1176. 1531.
1514(35) 0.000816 1176.1 1527.4
1521(35) 0.000816 1176.1 1522.7
1541(35) 0.000816 1176.1 1516.7
1562(36) 0.000772 1176. 1509.
1518(35) 0.000816 1176.2 1501.2
1507(35) 0.000816 1176.2 1491.9
1450(34) 0.000865 1176.2 1482.0
1468(34) 0.000865 1176.2 1471.7
1552(35) 0.000816 1176.3 1461.3
1442(34) 0.000865 1176.3 1450.9
1455(34) 0.000865 1176.3 1440.8
1466(34) 0.000865 1176.3 1431.2
1465(34) 0.000865 1176.4 1422.2
1400(34) 0.000865 1176.4 1413.9
1450(34) 0.000865 1176.4 1406.3
1352(33) 0.000918 1176.4 1399.5
1402(34) 0.000865 1176.5 1393.5
1390(34) 0.000865 1176.5 1388.1
1378(33) 0.000918 1176.5 1383.4
1334(33) 0.000918 1176.5 1379.3
1361(33) 0.000918 1176.5 1375.7
1352(33) 0.000918 1176.6 1372.5
1395(34) 0.000865 1176.6 1369.7
1373(33) 0.000918 1176.6 1367.3
1316(33) 0.000918 1176.6 1365.3
1336(33) 0.000918 1176.6 1363.6
1325(33) 0.000918 1176.7 1362.2
1329(33) 0.000918 1176.7 1361.1
1292(32) 0.000977 1176.7 1360.4
1340(33) 0.000918 1176.7 1360.1
1289(32) 0.000977 1176.7 1360.0
1341(33) 0.000918 1176.7 1360.3
1329(33) 0.000918 1176.7 1361.0
1332(33) 0.000918 1176.8 1361.9
1296(32) 0.000977 1176.8 1363.1
1314(33) 0.000918 1176.8 1364.7
1329(33) 0.000918 1176.8 1366.4
1327(33) 0.000918 1176.8 1368.5
1359(33) 0.000918 1176.8 1370.7
1346(33) 0.000918 1176.8 1373.2
1321(33) 0.000918 1176.8 1375.9
1364(33) 0.000918 1176.8 1378.8
1381(33) 0.000918 1176.8 1382.0
1297(32) 0.000977 1176.9 1385.4
1336(33) 0.000918 1176.9 1389.1
1370(33) 0.000918 1176.9 1393.0
1403(34) 0.000865 1176.9 1397.1
1372(33) 0.000918 1176.9 1401.4
1390(47) 0.000453 1177. 1406.
1393(33) 0.000918 1176.9 1410.1
1365(33) 0.000918 1176.9 1414.3
1371(33) 0.000918 1176.9 1418.3
1441(33) 0.000918 1176.9 1421.9
1434(33) 0.000918 1176.9 1424.9
1408(33) 0.000918 1176.9 1427.2
1353(32) 0.000977 1176.9 1428.6
1408(33) 0.000918 1176.9 1429.0
1389(33) 0.000918 1176.9 1428.3
1373(33) 0.000918 1176.9 1426.4
1422(33) 0.000918 1176.9 1423.3
1356(32) 0.000977 1176.9 1419.2
1364(33) 0.000918 1176.9 1414.0
1383(33) 0.000918 1176.9 1407.9
1323(32) 0.000977 1176.9 1401.0
1386(33) 0.000918 1176.8 1393.4
1364(32) 0.000977 1176.8 1385.4
1344(32) 0.000977 1176.8 1377.0
1400(33) 0.000918 1176.8 1368.4
1360(32) 0.000977 1176.8 1359.6
1318(32) 0.000977 1176.8 1350.8
1294(32) 0.000977 1176.8 1342.1
1368(33) 0.000918 1176.8 1333.6
1356(32) 0.000977 1176.8 1325.4
1257(31) 0.001041 1176.8 1317.6
1254(31) 0.001041 1176.7 1310.1
1292(32) 0.000977 1176.7 1303.1
1286(32) 0.000977 1176.7 1296.6
1293(32) 0.000977 1176.7 1290.7
1267(31) 0.001041 1176.7 1285.3
1275(31) 0.001041 1176.7 1280.6
1278(31) 0.001041 1176.6 1276.4
1263(31) 0.001041 1176.6 1272.9
1256(31) 0.001041 1176.6 1270.1
1259(31) 0.001041 1176.6 1267.9
1237(31) 0.001041 1176.6 1266.4
1273(31) 0.001041 1176.6 1265.6
1228(31) 0.001041 1176.5 1265.4
1257(31) 0.001041 1176.5 1265.9
1272(31) 0.001041 1176.5 1267.0
1285(32) 0.000977 1176.5 1268.7
1262(31) 0.001041 1176.4 1271.0
1277(31) 0.001041 1176.4 1273.9
1303(32) 0.000977 1176.4 1277.2
1297(32) 0.000977 1176.4 1281.1
1313(32) 0.000977 1176.3 1285.4
1282(31) 0.001041 1176.3 1290.0
1315(32) 0.000977 1176.3 1295.0
1351(32) 0.000977 1176.3 1300.3
1258(31) 0.001041 1176.2 1305.7
1309(32) 0.000977 1176.2 1311.3
1336(32) 0.000977 1176.2 1316.9
1318(32) 0.000977 1176.1 1322.4
1330(32) 0.000977 1176.1 1327.8
1334(32) 0.000977 1176.1 1333.1
1372(33) 0.000918 1176.0 1338.1
1326(32) 0.000977 1176.0 1342.7
1358(32) 0.000977 1176.0 1347.1
1393(33) 0.000918 1175.9 1351.1
1384(33) 0.000918 1175.9 1354.8
1395(33) 0.000918 1175.9 1358.1
1418(33) 0.000918 1175.8 1361.1
1363(32) 0.000977 1175.8 1363.7
1396(33) 0.000918 1175.7 1366.1
1352(32) 0.000977 1175.7 1368.1
1356(32) 0.000977 1175.7 1369.9
1395(33) 0.000918 1175.6 1371.3
1404(33) 0.000918 1175.6 1372.5
1401(33) 0.000918 1175.5 1373.3
1421(33) 0.000918 1175.5 1373.7
1367(33) 0.000918 1175.4 1373.8
1315(32) 0.000977 1175.4 1373.5
1396(33) 0.000918 1175.4 1372.8
1381(33) 0.000918 1175.3 1371.7
1351(32) 0.000977 1175.3 1370.2
1382(33) 0.000918 1175.2 1368.2
1353(32) 0.000977 1175.2 1365.8
1367(33) 0.000918 1175.1 1363.0
1354(32) 0.000977 1175.1 1359.9
1369(33) 0.000918 1175.0 1356.6
1376(33) 0.000918 1175.0 1353.1
1349(32) 0.000977 1174.9 1349.5
1351(32) 0.000977 1174.9 1345.9
1315(32) 0.000977 1174.8 1342.4
1380(33) 0.000918 1174.8 1339.1
1329(32) 0.000977 1174.7 1336.0
1329(32) 0.000977 1174.7 1333.2
1308(32) 0.000977 1174.6 1330.6
1269(31) 0.001041 1174.6 1328.4
1324(32) 0.000977 1174.5 1326.5
1301(32) 0.000977 1174.5 1324.9
1297(32) 0.000977 1174.4 1323.6
1341(32) 0.000977 1174.4 1322.6
1301(32) 0.000977 1174.3 1321.8
1347(32) 0.000977 1174.2 1321.2
1308(32) 0.000977 1174.2 1320.8
1337(32) 0.000977 1174.1 1320.5
1359(32) 0.000977 1174.1 1320.3
1348(32) 0.000977 1174.0 1320.1
1324(26) 0.001479 1173.9 1319.9
1358(32) 0.000977 1173.9 1319.6
1297(32) 0.000977 1173.8 1319.2
1300(32) 0.000977 1173.8 1318.6
1341(32) 0.000977 1173.7 1317.8
1334(32) 0.000977 1173.6 1316.9
1295(32) 0.000977 1173.6 1315.7
1305(32) 0.000977 1173.5 1314.3
1289(32) 0.000977 1173.5 1312.7
1308(32) 0.000977 1173.4 1310.9
1297(32) 0.000977 1173.3 1309.1
1297(32) 0.000977 1173.3 1307.1
1315(32) 0.000977 1173.2 1305.2
1314(32) 0.000977 1173.1 1303.3
1338(32) 0.000977 1173.1 1301.5
1355(32) 0.000977 1173.0 1300.0
1322(32) 0.000977 1172.9 1298.7
1310(32) 0.000977 1172.9 1297.7
1329(32) 0.000977 1172.8 1297.1
1284(31) 0.001041 1172.7 1297.0
1267(31) 0.001041 1172.7 1297.4
1265(31) 0.001041 1172.6 1298.2
1303(32) 0.000977 1172.5 1299.7
1254(31) 0.001041 1172.5 1301.7
1279(31) 0.001041 1172.4 1304.4
1290(32) 0.000977 1172.3 1307.7
1267(31) 0.001041 1172.3 1311.7
1339(32) 0.000977 1172.2 1316.3
1377(33) 0.000918 1172.1 1321.6
1363(32) 0.000977 1172.1 1327.6
1398(33) 0.000918 1172.0 1334.2
1359(32) 0.000977 1171.9 1341.5
1377(33) 0.000918 1171.8 1349.5
1393(33) 0.000918 1171.8 1358.0
1445(33) 0.000918 1171.7 1367.1
1422(33) 0.000918 1171.6 1376.8
1372(33) 0.000918 1171.6 1386.9
1414(33) 0.000918 1171.5 1397.3
1356(32) 0.000977 1171.4 1408.1
1419(33) 0.000918 1171.4 1419.1
1402(33) 0.000918 1171.3 1430.1
1463(34) 0.000865 1171.2 1441.2
1481(34) 0.000865 1171.1 1452.1
1448(33) 0.000918 1171.1 1462.8
1470(34) 0.000865 1171.0 1473.0
1475(34) 0.000865 1170.9 1482.7
1456(34) 0.000865 1170.8 1491.8
1481(34) 0.000865 1170.8 1500.2
1484(34) 0.000865 1170.7 1507.7
1444(33) 0.000918 1170.6 1514.3
1478(34) 0.000865 1170.6 1519.9
1566(35) 0.000816 1170.5 1524.5
1532(34) 0.000865 1170.4 1528.2
1517(34) 0.000865 1170.3 1530.8
1505(34) 0.000865 1170.3 1532.4
1558(35) 0.000816 1170.2 1533.0
1564(35) 0.000816 1170.1 1532.5
1560(35) 0.000816 1170.1 1531.1
1509(34) 0.000865 1170.0 1528.8
1495(34) 0.000865 1169.9 1525.6
1506(34) 0.000865 1169.9 1521.6
1483(34) 0.000865 1169.8 1516.8
1494(34) 0.000865 1169.7 1511.4
1512(34) 0.000865 1169.6 1505.4
1521(34) 0.000865 1169.6 1498.9
1486(34) 0.000865 1169.5 1492.0
1537(34) 0.000865 1169.4 1484.8
1525(34) 0.000865 1169.4 1477.4
1497(34) 0.000865 1169.3 1469.8
1461(34) 0.000865 1169.2 1462.2
1491(34) 0.000865 1169.2 1454.5
1477(34) 0.000865 1169.1 1446.9
1445(33) 0.000918 1169.0 1439.4
1437(33) 0.000918 1169.0 1432.0
1417(33) 0.000918 1168.9 1424.8
1410(33) 0.000918 1168.8 1417.9
1458(34) 0.000865 1168.8 1411.2
1412(33) 0.000918 1168.7 1404.8
1412(33) 0.000918 1168.6 1398.7
1399(33) 0.000918 1168.6 1392.9
1421(33) 0.000918 1168.5 1387.5
1413(33) 0.000918 1168.4 1382.3
1378(33) 0.000918 1168.4 1377.6
1371(33) 0.000918 1168.3 1373.1
1425(33) 0.000918 1168.3 1369.1
1370(32) 0.000977 1168.2 1365.3
1348(32) 0.000977 1168.1 1361.9
1340(32) 0.000977 1168.1 1358.9
1405(33) 0.000918 1168.0 1356.1
1396(33) 0.000918 1168.0 1353.8
1370(32) 0.000977 1167.9 1351.8
1352(32) 0.000977 1167.9 1350.1
1381(33) 0.000918 1167.8 1348.9
1372(33) 0.000918 1167.8 1348.0
1303(32) 0.000977 1167.7 1347.6
1326(32) 0.000977 1167.6 1347.7
1337(32) 0.000977 1167.6 1348.2
1371(33) 0.000918 1167.5 1349.3
1338(32) 0.000977 1167.5 1350.9
1352(32) 0.000977 1167.4 1353.1
1409(33) 0.000918 1167.4 1355.9
1412(33) 0.000918 1167.4 1359.3
1393(33) 0.000918 1167.3 1363.3
1381(33) 0.000918 1167.3 1367.9
1397(33) 0.000918 1167.2 1373.1
1407(33) 0.000918 1167.2 1379.0
1394(33) 0.000918 1167.1 1385.4
1403(33) 0.000918 1167.1 1392.3
1395(33) 0.000918 1167.1 1399.8
1413(33) 0.000918 1167.0 1407.7
1432(34) 0.000865 1167.0 1416.1
1440(34) 0.000865 1167.0 1424.8
1465(34) 0.000865 1166.9 1433.7
1453(34) 0.000865 1166.9 1442.9
1476(34) 0.000865 1166.9 1452.1
1485(34) 0.000865 1166.8 1461.4
1493(34) 0.000865 1166.8 1470.6
1433(34) 0.000865 1166.8 1479.6
1456(34) 0.000865 1166.7 1488.4
1507(35) 0.000816 1166.7 1496.7
1501(34) 0.000865 1166.7 1504.6
1579(35) 0.000816 1166.7 1511.8
1531(35) 0.000816 1166.7 1518.5
1515(35) 0.000816 1166.6 1524.3
1546(35) 0.000816 1166.6 1529.4
1543(35) 0.000816 1166.6 1533.7
1588(35) 0.000816 1166.6 1537.2
1602(36) 0.000772 1167. 1540.
1572(35) 0.000816 1166.6 1541.8
1605(36) 0.000772 1167. 1543.
1545(35) 0.000816 1166.6 1543.6
1526(35) 0.000816 1166.6 1543.6
1524(35) 0.000816 1166.6 1543.1
1565(35) 0.000816 1166.6 1542.2
1541(35) 0.000816 1166.6 1541.0
1509(35) 0.000816 1166.6 1539.4
1521(35) 0.000816 1166.6 1537.5
1524(35) 0.000816 1166.6 1535.4
1538(35) 0.000816 1166.6 1533.1
1522(35) 0.000816 1166.6 1530.6
1525(35) 0.000816 1166.6 1527.8
1499(34) 0.000865 1166.7 1524.9
1484(34) 0.000865 1166.7 1521.8
1504(34) 0.000865 1166.7 1518.5
1489(34) 0.000865 1166.7 1514.9
1447(34) 0.000865 1166.7 1511.0
1494(34) 0.000865 1166.8 1506.8
1475(34) 0.000865 1166.8 1502.3
1488(34) 0.000865 1166.8 1497.5
1494(34) 0.000865 1166.9 1492.5
1460(34) 0.000865 1166.9 1487.1
1404(33) 0.000918 1167.0 1481.4
1436(34) 0.000865 1167.0 1475.5
1424(34) 0.000865 1167.1 1469.3
1449(34) 0.000865 1167.1 1463.0
1455(34) 0.000865 1167.2 1456.5
1442(34) 0.000865 1167.2 1449.8
1411(33) 0.000918 1167.3 1443.1
1446(34) 0.000865 1167.3 1436.3
1386(33) 0.000918 1167.4 1429.5
1398(33) 0.000918 1167.5 1422.7
1403(33) 0.000918 1167.5 1415.9
1404(33) 0.000918 1167.6 1409.2
1372(33) 0.000918 1167.7 1402.5
1342(33) 0.000918 1167.8 1396.0
1374(33) 0.000918 1167.8 1389.5
1362(33) 0.000918 1167.9 1383.2
1379(33) 0.000918 1168.0 1377.1
1339(33) 0.000918 1168.1 1371.1
1368(33) 0.000918 1168.2 1365.4
1311(32) 0.000977 1168.3 1359.8
1380(33) 0.000918 1168.4 1354.4
1354(33) 0.000918 1168.5 1349.3
1285(32) 0.000977 1168.6 1344.4
1336(32) 0.000977 1168.7 1339.7
1294(32) 0.000977 1168.8 1335.3
1289(32) 0.000977 1169.0 1331.1
1328(32) 0.000977 1169.1 1327.2
1301(32) 0.000977 1169.2 1323.6
1288(32) 0.000977 1169.3 1320.3
1327(32) 0.000977 1169.5 1317.3
1337(33) 0.000918 1169.6 1314.5
1301(32) 0.000977 1169.8 1312.1
1323(32) 0.000977 1169.9 1310.0
1355(33) 0.000918 1170.1 1308.2
1351(33) 0.000918 1170.2 1306.7
1308(32) 0.000977 1170.4 1305.6
1301(32) 0.000977 1170.5 1304.9
1327(32) 0.000977 1170.7 1304.5
1274(32) 0.000977 1170.9 1304.4
1286(32) 0.000977 1171.0 1304.8
1309(32) 0.000977 1171.2 1305.6
1298(32) 0.000977 1171.4 1306.7
1309(32) 0.000977 1171.6 1308.3
1346(33) 0.000918 1171.8 1310.3
1367(33) 0.000918 1172.0 1312.8
1358(33) 0.000918 1172.2 1315.6
1360(33) 0.000918 1172.4 1318.9
1309(32) 0.000977 1172.6 1322.7
1311(32) 0.000977 1172.8 1326.9
1321(32) 0.000977 1173.1 1331.5
1330(33) 0.000918 1173.3 1336.5
1363(33) 0.000918 1173.5 1342.0
1374(33) 0.000918 1173.7 1347.9
1365(33) 0.000918 1174.0 1354.2
1367(33) 0.000918 1174.2 1360.8
1369(33) 0.000918 1174.5 1367.8
1362(33) 0.000918 1174.7 1375.2
1390(33) 0.000918 1175.0 1382.9
1409(33) 0.000918 1175.3 1390.8
1432(34) 0.000865 1175.5 1399.0
1487(34) 0.000865 1175.8 1407.5
1469(34) 0.000865 1176.1 1416.1
1444(34) 0.000865 1176.4 1424.9
1427(34) 0.000865 1176.7 1433.7
1476(34) 0.000865 1177.0 1442.7
1479(34) 0.000865 1177.3 1451.7
1461(34) 0.000865 1177.6 1460.6
1448(34) 0.000865 1177.9 1469.5
1474(34) 0.000865 1178.3 1478.3
1470(34) 0.000865 1178.6 1486.9
1515(35) 0.000816 1178.9 1495.4
1506(35) 0.000816 1179.3 1503.7
1553(35) 0.000816 1179.6 1511.7
1555(35) 0.000816 1180.0 1519.4
1529(35) 0.000816 1180.3 1526.9
1522(35) 0.000816 1180.7 1534.0
1550(35) 0.000816 1181.1 1540.8
1569(35) 0.000816 1181.4 1547.3
1520(35) 0.000816 1181.8 1553.3
1558(35) 0.000816 1182.2 1559.0
1543(35) 0.000816 1182.6 1564.3
1580(35) 0.000816 1183.0 1569.1
1578(35) 0.000816 1183.4 1573.6
1589(36) 0.000772 1184. 1578.
1589(36) 0.000772 1184. 1581.
1583(35) 0.000816 1184.7 1584.6
1556(35) 0.000816 1185.2 1587.5
1593(36) 0.000772 1186. 1590.
1662(36) 0.000772 1186. 1592.
1621(36) 0.000772 1187. 1594.
1621(36) 0.000772 1187. 1596.
1620(36) 0.000772 1187. 1597.
1606(36) 0.000772 1188. 1598.
1597(36) 0.000772 1188. 1599.
1593(36) 0.000772 1189. 1600.
1614(36) 0.000772 1189. 1601.
1610(36) 0.000772 1190. 1601.
1594(36) 0.000772 1191. 1601.
1638(36) 0.000772 1191. 1601.
1650(36) 0.000772 1192. 1601.
1649(36) 0.000772 1192. 1600.
1649(36) 0.000772 1193. 1600.
1627(36) 0.000772 1193. 1599.
1580(35) 0.000816 1193.8 1597.4
1578(35) 0.000816 1194.4 1595.7
1583(35) 0.000816 1195.0 1593.8
1601(36) 0.000772 1196. 1591.
1605(36) 0.000772 1196. 1589.
1562(35) 0.000816 1196.8 1585.5
1529(35) 0.000816 1197.5 1581.9
1572(35) 0.000816 1198.1 1577.9
1607(36) 0.000772 1199. 1574.
1564(35) 0.000816 1199.4 1568.7
1523(35) 0.000816 1200.1 1563.4
1536(35) 0.000816 1200.7 1557.8
1584(35) 0.000816 1201.4 1551.8
1588(36) 0.000772 1202. 1546.
1593(36) 0.000772 1203. 1539.
1551(35) 0.000816 1203.5 1532.2
1540(35) 0.000816 1204.2 1525.3
1487(34) 0.000865 1204.9 1518.2
1513(35) 0.000816 1205.7 1511.0
1498(35) 0.000816 1206.4 1503.8
1509(35) 0.000816 1207.2 1496.5
1502(35) 0.000816 1208.0 1489.3
1472(34) 0.000865 1208.7 1482.1
1481(34) 0.000865 1209.5 1475.0
1463(34) 0.000865 1210.3 1468.1
1444(34) 0.000865 1211.1 1461.2
1442(34) 0.000865 1211.9 1454.6
1415(34) 0.000865 1212.8 1448.1
1423(34) 0.000865 1213.6 1441.8
1426(34) 0.000865 1214.5 1435.8
1402(33) 0.000918 1215.3 1430.0
1412(34) 0.000865 1216.2 1424.4
1385(33) 0.000918 1217.1 1419.0
1361(33) 0.000918 1218.0 1414.0
1372(33) 0.000918 1218.9 1409.2
1374(33) 0.000918 1219.8 1404.7
1370(33) 0.000918 1220.7 1400.5
1391(33) 0.000918 1221.7 1396.6
1381(33) 0.000918 1222.6 1393.0
1380(33) 0.000918 1223.6 1389.7
1360(33) 0.000918 1224.6 1386.7
1387(33) 0.000918 1225.6 1384.1
1382(33) 0.000918 1226.6 1381.8
1363(33) 0.000918 1227.6 1379.8
1367(33) 0.000918 1228.6 1378.2
1402(33) 0.000918 1229.6 1377.0
1378(27) 0.001372 1230.7 1376.1
1406(34) 0.000865 1231.7 1375.6
1401(34) 0.000865 1232.8 1375.5
1382(33) 0.000918 1233.9 1375.7
1411(34) 0.000865 1235.0 1376.3
1399(34) 0.000865 1236.1 1377.3
1384(33) 0.000918 1237.2 1378.7
1388(34) 0.000865 1238.4 1380.5
1366(33) 0.000918 1239.5 1382.6
1338(33) 0.000918 1240.7 1385.1
1358(33) 0.000918 1241.9 1388.0
1406(34) 0.000865 1243.1 1391.3
1410(34) 0.000865 1244.3 1394.9
1412(34) 0.000865 1245.5 1398.8
1404(34) 0.000865 1246.7 1403.2
1403(34) 0.000865 1248.0 1407.8
1440(34) 0.000865 1249.2 1412.8
1409(34) 0.000865 1250.5 1418.1
1396(34) 0.000865 1251.8 1423.8
1424(34) 0.000865 1253.1 1429.7
1437(34) 0.000865 1254.4 1435.9
1427(34) 0.000865 1255.7 1442.4
1460(34) 0.000865 1257.1 1449.2
1482(35) 0.000816 1258.4 1456.1
1484(35) 0.000816 1259.8 1463.3
1467(34) 0.000865 1261.2 1470.7
1428(34) 0.000865 1262.6 1478.3
1465(34) 0.000865 1264.0 1486.0
1530(35) 0.000816 1265.5 1493.8
1528(35) 0.000816 1266.9 1501.8
1500(35) 0.000816 1268.4 1509.8
1495(35) 0.000816 1269.9 1517.8
1505(35) 0.000816 1271.4 1525.8
1518(35) 0.000816 1272.9 1533.9
1524(35) 0.000816 1274.4 1541.8
1548(35) 0.000816 1276.0 1549.7
1519(35) 0.000816 1277.5 1557.5
1504(35) 0.000816 1279.1 1565.1
1541(35) 0.000816 1280.7 1572.5
1513(35) 0.000816 1282.3 1579.6
1546(35) 0.000816 1284.0 1586.5
1567(36) 0.000772 1286. 1593.
1496(35) 0.000816 1287.3 1599.3
1535(35) 0.000816 1289.0 1605.2
1581(36) 0.000772 1291. 1611.
1580(36) 0.000772 1292. 1616.
1563(36) 0.000772 1294. 1620.
1544(35) 0.000816 1295.9 1624.3
1570(36) 0.000772 1298. 1628.
1580(36) 0.000772 1299. 1631.
1567(36) 0.000772 1301. 1634.
1572(36) 0.000772 1303. 1636.
1605(36) 0.000772 1305. 1638.
1623(36) 0.000772 1307. 1639.
1622(36) 0.000772 1309. 1640.
1616(36) 0.000772 1311. 1640.
1614(36) 0.000772 1312. 1641.
1605(36) 0.000772 1314. 1640.
1614(36) 0.000772 1316. 1640.
1628(36) 0.000772 1318. 1639.
1653(37) 0.000730 1320. 1638.
1646(36) 0.000772 1322. 1637.
1635(36) 0.000772 1324. 1635.
1659(37) 0.000730 1326. 1634.
1673(37) 0.000730 1329. 1632.
1642(36) 0.000772 1331. 1631.
1659(37) 0.000730 1333. 1629.
1661(37) 0.000730 1335. 1627.
1626(36) 0.000772 1337. 1625.
1609(36) 0.000772 1339. 1624.
1599(36) 0.000772 1341. 1622.
1612(36) 0.000772 1344. 1621.
1565(36) 0.000772 1346. 1619.
1580(36) 0.000772 1348. 1618.
1603(36) 0.000772 1350. 1617.
1610(36) 0.000772 1353. 1616.
1628(36) 0.000772 1355. 1615.
1635(36) 0.000772 1357. 1614.
1615(36) 0.000772 1360. 1614.
1618(36) 0.000772 1362. 1614.
1617(36) 0.000772 1365. 1613.
1620(36) 0.000772 1367. 1613.
1634(36) 0.000772 1369. 1614.
1598(36) 0.000772 1372. 1614.
1581(36) 0.000772 1374. 1614.
1645(36) 0.000772 1377. 1615.
1634(36) 0.000772 1379. 1616.
1617(36) 0.000772 1382. 1616.
1622(36) 0.000772 1385. 1617.
1616(36) 0.000772 1387. 1618.
1631(36) 0.000772 1390. 1619.
1646(36) 0.000772 1393. 1621.
1649(36) 0.000772 1395. 1622.
1604(36) 0.000772 1398. 1623.
1610(36) 0.000772 1401. 1624.
1648(36) 0.000772 1404. 1625.
1617(36) 0.000772 1406. 1627.
1611(36) 0.000772 1409. 1628.
1614(36) 0.000772 1412. 1629.
1627(36) 0.000772 1415. 1630.
1586(36) 0.000772 1418. 1631.
1617(37) 0.000730 1421. 1632.
1656(37) 0.000730 1424. 1633.
1704(38) 0.000693 1427. 1634.
1673(37) 0.000730 1430. 1635.
1682(37) 0.000730 1433. 1636.
1647(37) 0.000730 1436. 1637.
1652(37) 0.000730 1439. 1637.
1694(38) 0.000693 1442. 1638.
1660(37) 0.000730 1445. 1639.
1666(37) 0.000730 1448. 1639.
1667(37) 0.000730 1451. 1640.
1643(37) 0.000730 1454. 1641.
1629(37) 0.000730 1458. 1642.
1646(37) 0.000730 1461. 1642.
1721(38) 0.000693 1464. 1643.
1734(38) 0.000693 1468. 1644.
1701(38) 0.000693 1471. 1645.
1650(37) 0.000730 1474. 1646.
1692(38) 0.000693 1478. 1647.
1690(38) 0.000693 1481. 1648.
1632(37) 0.000730 1485. 1649.
1711(38) 0.000693 1488. 1651.
1637(37) 0.000730 1492. 1652.
1653(37) 0.000730 1495. 1654.
1701(38) 0.000693 1499. 1655.
1656(37) 0.000730 1502. 1657.
1666(37) 0.000730 1506. 1659.
1684(37) 0.000730 1510. 1661.
1672(37) 0.000730 1513. 1664.
1685(38) 0.000693 1517. 1666.
1685(38) 0.000693 1521. 1669.
1711(38) 0.000693 1525. 1672.
1700(38) 0.000693 1528. 1674.
1700(38) 0.000693 1532. 1678.
1642(37) 0.000730 1536. 1681.
1674(37) 0.000730 1540. 1684.
1743(38) 0.000693 1544. 1688.
1738(38) 0.000693 1548. 1692.
1717(38) 0.000693 1552. 1696.
1722(38) 0.000693 1556. 1700.
1722(38) 0.000693 1560. 1705.
1708(38) 0.000693 1564. 1709.
1762(38) 0.000693 1569. 1714.
1775(38) 0.000693 1573. 1719.
1706(38) 0.000693 1577. 1724.
1733(38) 0.000693 1581. 1729.
1682(37) 0.000730 1585. 1734.
1667(37) 0.000730 1590. 1740.
1724(38) 0.000693 1594. 1746.
1706(38) 0.000693 1599. 1752.
1761(38) 0.000693 1603. 1758.
1779(38) 0.000693 1607. 1764.
1792(39) 0.000657 1612. 1770.
1757(38) 0.000693 1616. 1776.
1798(39) 0.000657 1621. 1783.
1793(39) 0.000657 1626. 1789.
1780(38) 0.000693 1630. 1796.
1754(38) 0.000693 1635. 1803.
1762(38) 0.000693 1640. 1810.
1816(39) 0.000657 1644. 1817.
1813(39) 0.000657 1649. 1824.
1818(39) 0.000657 1654. 1831.
1824(39) 0.000657 1659. 1838.
1812(39) 0.000657 1664. 1845.
1828(39) 0.000657 1669. 1852.
1850(39) 0.000657 1674. 1860.
1870(39) 0.000657 1679. 1867.
1861(39) 0.000657 1684. 1875.
1825(39) 0.000657 1689. 1882.
1894(40) 0.000625 1694. 1889.
1933(40) 0.000625 1699. 1897.
1950(40) 0.000625 1704. 1904.
1921(40) 0.000625 1709. 1912.
1880(40) . . .
1927(40) . . .
1916(40) . . .
1915(40) . . .
1940(40) . . .
1963(40) . . .
1976(40) . . .
1978(40) . . .
1957(40) . . .
1992(41) . . .
2024(41) . . .
2005(41) . . .
2017(41) . . .
2055(41) . . .
2049(41) . . .
2073(41) . . .
2067(41) . . .
2061(41) . . .
2093(42) . . .
2049(41) . . .
2087(42) . . .
2100(42) . . .
2102(42) . . .
2086(42) . . .
2130(42) . . .
2145(42) . . .
2180(61) . . .
2211(61) . . .
2259(62) . . .
2127(60) . . .
2243(62) . . .
2281(62) . . .
2222(61) . . .
2288(62) . . .
2256(62) . . .
2237(62) . . .
2211(61) . . .
2241(62) . . .
2202(61) . . .
2224(61) . . .
2269(62) . . .
2348(63) . . .
2312(63) . . .
2287(62) . . .
2264(62) . . .
2249(62) . . .
2262(62) . . .
2364(63) . . .
2362(63) . . .
2580(66) . . .
2461(64) . . .
2364(63) . . .
2442(64) . . .
2433(64) . . .
2453(64) . . .
2398(64) . . .
2382(63) . . .
2418(64) . . .
2572(66) . . .
2514(65) . . .
2540(65) . . .
2459(64) . . .
2552(66) . . .
2609(66) . . .
2453(64) . . .
2488(65) . . .
2553(66) . . .
2588(66) . . .
2564(66) . . .
2501(65) . . .
2518(65) . . .
2512(65) . . .
2592(66) . . .
2527(65) . . .
2590(66) . . .
2581(66) . . .
2639(67) . . .
2605(66) . . .
2572(66) . . .
2675(67) . . .
2718(67) . . .
2610(66) . . .
2648(67) . . .
2679(67) . . .
2689(67) . . .
2579(66) . . .
2612(66) . . .
2663(67) . . .
2666(67) . . .
2553(66) . . .
2617(66) . . .
2646(67) . . .
2602(66) . . .
2677(67) . . .
2543(65) . . .
2566(66) . . .
2799(68) . . .
2695(67) . . .
2705(67) . . .
2629(66) . . .
2621(66) . . .
2733(68) . . .
2716(67) . . .
2746(68) . . .
2743(68) . . .
2701(67) . . .
2677(67) . . .
2657(67) . . .
2659(67) . . .
2735(68) . . .
2755(68) . . .
2687(67) . . .
2738(68) . . .
2665(67) . . .
2783(68) . . .
2710(67) . . .
2746(68) . . .
2696(67) . . .
2739(68) . . .
2762(68) . . .
2732(68) . . .
2737(68) . . .
2853(69) . . .
2708(67) . . .
2702(67) . . .
2745(68) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_reflns_number_total             666
_reflns_limit_h_min              1
_reflns_limit_h_max              18
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.055
_reflns_d_resolution_low         18.900
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_FINAL_publ
_database_code_depnum_ccdc_archive 'CCDC 1582010'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-05-24T18:46|FINAL|wendy|bt1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-05-24T18:46

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.06
_refine_ls_shift/su_mean         0.02
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     46
_refine_ls_goodness_of_fit_all   1.08
_refine_ls_number_restraints     7
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?


_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from Z:/queen/Desktop/FeBTT/Bare_final/BARE.EXP'
_cell_length_a                   18.8957(4)
_cell_length_b                   18.8957
_cell_length_c                   18.8957
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6746.6(5)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Fe Fe1 0.1343(4) 0.5 0.0 1.0 Uiso 0.006(2) 12
C C1 0.15118(34) 0.3361(5) -0.15118(34) 1.0 Uiso 0.0186(12) 24
C C2 0.18069(31) 0.2710(4) -0.18069(31) 1.0 Uiso 0.0186(12) 24
C C3 0.24190(27) 0.24190(27) -0.1466(4) 1.0 Uiso 0.0186(12) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.007(3) 3
N N1 0.13030(22) 0.42082(22) -0.08157(22) 1.0 Uiso 0.0161(7) 48
N N2 0.17575(24) 0.36819(23) -0.09153(22) 1.0 Uiso 0.0161(7) 48
H H1 0.2629(5) 0.2629(5) -0.1069(6) 1.0 Uiso 0.028(5) 24
Fe Fe2 0.264(5) 0.0 0.0 0.179(20) Uiso 0.10(5) 6
O Os 0.2512(12) 0.5 0.0 0.647(19) Uiso 0.035(6) 12
C Cs 0.3034(12) 0.5 0.0550(10) 0.324(9) Uiso 0.035(6) 24
H Hsa 0.2797(19) 0.5 0.0995(9) 0.324(9) Uiso 0.11(2) 24
H Hsb 0.3301(15) 0.4578(8) 0.0530(16) 0.324(9) Uiso 0.11(2) 48

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C26.59 H15.77 Cl Fe4.36 N32 O2.59'
_chemical_formula_weight         1103.75
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Fe1 Fe1 3.590(12) . 14_555 N
Fe1 Fe1 3.590(12) . 19_555 N
Fe1 Cl1 2.539(8) . 1_555 N
Fe1 N1 2.149(4) . 1_555 N
Fe1 N1 2.149(4) . 4_555 N
Fe1 N1 2.149(4) . 12_565 N
Fe1 N1 3.049(5) . 17_555 N
Fe1 N1 3.049(5) . 19_555 N
Fe1 N1 3.049(5) . 23_565 N
Fe1 N1 2.149(4) . -10_565 N
Fe1 N1 3.049(5) . -14_565 N
Fe1 N2 3.132(4) . 1_555 N
Fe1 N2 3.132(4) . 4_555 N
Fe1 N2 3.132(4) . 12_565 N
Fe1 N2 3.132(4) . -10_565 N
Fe1 Os 2.208(22) . 1_555 N
Fe1 Cs 3.358(21) . 1_555 N
Fe1 Cs 3.358(21) . 4_555 N
Fe1 Hsa 3.329(29) . 1_555 N
Fe1 Hsa 3.329(29) . 4_555 N
C1 C2 1.461(12) . 1_555 N
C1 N1 2.109(8) . 1_555 N
C1 N1 2.109(8) . 19_555 N
C1 N2 1.362(6) . 1_555 N
C1 N2 1.362(6) . 19_555 N
C2 C1 1.461(12) . 1_555 N
C2 C3 1.433(5) . 1_555 N
C2 C3 1.433(5) . 7_555 N
C3 C2 1.433(5) . 1_555 N
C3 C2 1.433(5) . 9_555 N
C3 H1 0.937(10) . 1_555 N
Cl1 Fe1 2.539(8) . 1_555 N
Cl1 Fe1 2.539(8) . 10_555 N
Cl1 Fe1 2.539(8) . 14_555 N
Cl1 Fe1 2.539(8) . 19_555 N
Cl1 N1 3.267(4) . 1_555 N
Cl1 N1 3.267(4) . 4_555 N
Cl1 N1 3.267(4) . 10_555 N
Cl1 N1 3.267(4) . 12_565 N
Cl1 N1 3.267(4) . 14_555 N
Cl1 N1 3.267(4) . 17_555 N
Cl1 N1 3.267(4) . 19_555 N
Cl1 N1 3.267(4) . 23_565 N
Cl1 N1 3.267(4) . -1_565 N
Cl1 N1 3.267(4) . -4_565 N
Cl1 N1 3.267(4) . -10_565 N
Cl1 N1 3.267(4) . -12_555 N
Cl1 N1 3.267(4) . -14_565 N
Cl1 N1 3.267(4) . -17_565 N
Cl1 N1 3.267(4) . -19_565 N
Cl1 N1 3.267(4) . -23_555 N
Cl1 Fe2 4.45(10) . 2_555 N
Cl1 Fe2 4.45(10) . 11_565 N
N1 Fe1 2.149(4) . 1_555 N
N1 Fe1 3.049(5) . 19_555 N
N1 C1 2.109(8) . 1_555 N
N1 Cl1 3.267(4) . 1_555 N
N1 N1 1.302(9) . 19_555 N
N1 N2 1.327(6) . 1_555 N
N2 Fe1 3.132(4) . 1_555 N
N2 C1 1.362(6) . 1_555 N
N2 N1 1.327(6) . 1_555 N
H1 C3 0.937(10) . 1_555 N
Fe2 Cl1 4.45(10) . 3_555 N
Os Fe1 2.208(22) . 1_555 N
Os Cs 1.431(10) . 1_555 N
Os Cs 1.431(10) . 4_555 N
Cs Fe1 3.358(21) . 1_555 N
Cs Os 1.431(10) . 1_555 N
Cs Cs 2.08(4) . 4_555 N
Cs Hsa 0.952(11) . 1_555 N
Cs Hsb 0.945(11) . 1_555 N
Cs Hsb 0.945(11) . -10_565 N
Hsa Fe1 3.329(29) . 1_555 N
Hsa Cs 0.952(11) . 1_555 N
Hsa Hsb 1.521(16) . 1_555 N
Hsa Hsb 1.521(16) . -10_565 N
Hsb Cs 0.945(11) . 1_555 N
Hsb Hsa 1.521(16) . 1_555 N
Hsb Hsb 1.594(30) . -10_565 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Fe1 N1 87.97(26) 1_555 . 1_555 N
Cl1 Fe1 N1 87.97(26) 1_555 . 4_555 N
Cl1 Fe1 N1 87.97(26) 1_555 . 12_565 N
Cl1 Fe1 N1 87.97(26) 1_555 . -10_565 N
N1 Fe1 N1 91.63(23) 1_555 . 4_555 N
N1 Fe1 N1 175.9(5) 1_555 . 12_565 N
N1 Fe1 N1 88.22(23) 1_555 . -10_565 N
N1 Fe1 N1 88.22(23) 4_555 . 12_565 N
N1 Fe1 N1 175.9(5) 4_555 . -10_565 N
N1 Fe1 N1 91.63(23) 12_565 . -10_565 N
C2 C1 N2 124.1(4) 1_555 . 1_555 N
C2 C1 N2 124.1(4) 1_555 . 19_555 N
N2 C1 N2 111.5(8) 1_555 . 19_555 N
C1 C2 C3 117.4(4) 1_555 . 1_555 N
C1 C2 C3 117.4(4) 1_555 . 7_555 N
C3 C2 C3 125.3(7) 1_555 . 7_555 N
C2 C3 C2 114.7(7) 1_555 . 9_555 N
C2 C3 H1 122.6(4) 1_555 . 1_555 N
C2 C3 H1 122.6(4) 9_555 . 1_555 N
Fe1 Cl1 Fe1 180.0 1_555 . 10_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 19_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 19_555 N
Fe1 Cl1 Fe1 180.0 14_555 . 19_555 N
Fe1 N1 N1 122.15(23) 1_555 . 19_555 N
Fe1 N1 N2 126.9(4) 1_555 . 1_555 N
N1 N1 N2 110.93(28) 19_555 . 1_555 N
C1 N2 N1 103.3(5) 1_555 . 1_555 N
Cs Os Cs 93.0(22) 1_555 . 4_555 N
Os Cs Hsa 108.6(10) 1_555 . 1_555 N
Os Cs Hsb 109.9(10) 1_555 . 1_555 N
Os Cs Hsb 109.9(10) 1_555 . -10_565 N
Hsa Cs Hsb 106.6(10) 1_555 . 1_555 N
Hsa Cs Hsb 106.6(10) 1_555 . -10_565 N
Hsb Cs Hsb 115.1(27) 1_555 . -10_565 N
Cs Hsa Hsb 36.5(6) 1_555 . 1_555 N
Cs Hsa Hsb 36.5(6) 1_555 . -10_565 N
Hsb Hsa Hsb 63.2(15) 1_555 . -10_565 N
Cs Hsb Hsa 36.9(6) 1_555 . 1_555 N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT601_FINAL_publ          
;
PROBLEM: Structure Contains Solvent Accessible VOIDS of .       2558 Ang3   
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT049_FINAL_publ          
;
PROBLEM: Calculated Density less than 1.0 gcm-3 .........     0.8151 Check 
RESPONSE: This is expected as the material is porous.
;

_vrf_PLAT307_FINAL_publ          
;
PROBLEM:  Isolated Metal Atom found in Structure (Unusual)        Fe2 Check  
RESPONSE: It is charge balancing extra framework cation and it is supposed to be sorrounded by solvent molecules which couldn't be modeled because lack of their highly ordered pattern.
;





# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_cell_measurement_theta_min      10
_cell_measurement_theta_max      160
_cell_measurement_temperature    10
_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Fe 13.076 0.9450 International_Tables_Vol_C
C 79.766 0.6646 International_Tables_Vol_C
Cl 3.0 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 47.297 -0.3739 International_Tables_Vol_C
O 7.766 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.0775
_pd_proc_ls_prof_R_factor        0.0236
_pd_proc_ls_prof_wR_factor       0.0272
_pd_proc_ls_prof_wR_expected     0.0253
_refine_ls_R_Fsqd_factor         0.05216

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 14 terms.
 Shifted Chebyshev function of 1st kind
      1:    1458.99     2:   -340.297     3:    313.063     4:   -13.2036    
      5:    154.310     6:   -20.5586     7:    84.6450     8:   -7.41900    
      9:    55.1880    10:   -7.60255    11:    16.3253    12:   -13.3603    
     13:    6.92335    14:   -1.86831    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  532.564 #2(GV)   = -249.786 #3(GW)   =  126.763
 #4(GP)   =    0.000 #5(LX)   =    0.000 #6(LY)   =   17.120
 #7(S/L)  =   0.0427 #8(H/L)  =   0.0352
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2016-05-24T18:46:58
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.6719
_pd_proc_2theta_range_max        166.4219
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
5640(160) 0.0 3262. .
4980(150) 0.0 3241. .
4610(150) 0.0 3222. .
4100(140) 0.0 3202. .
4000(140) 0.0 3183. .
3890(140) 0.0 3164. .
3630(130) 0.0 3145. .
3280(120) 0.0 3126. .
3470(130) 0.0 3107. .
3750(130) 0.0 3089. .
3180(120) 0.0 3071. .
3270(120) 0.0 3053. .
3380(130) 0.0 3036. .
3240(120) 0.0 3018. .
3370(130) 0.0 3001. .
3500(130) 0.0 2984. .
3170(120) 0.0 2968. .
3210(120) 0.0 2951. .
3250(120) 0.0 2935. .
3210(120) 0.0 2918. .
3210(120) 0.0 2902. .
3150(120) 0.0 2887. .
3000(120) 0.0 2871. .
3090(120) 0.0 2856. .
3270(120) 0.0 2840. .
3040(120) 0.0 2825. .
3160(120) 0.0 2811. .
3370(130) 0.0 2796. .
3270(120) 0.0 2781. .
3140(120) 0.0 2767. .
3020(120) 0.0 2753. .
2960(120) 0.0 2739. .
2640(110) 0.0 2725. .
2880(120) 0.0 2712. .
2740(110) 0.0 2698. .
3150(120) 0.0 2685. .
2770(110) 0.0 2672. .
2930(120) 0.0 2659. .
2760(110) 0.0 2646. .
2590(110) 0.0 2634. .
2780(110) 0.0 2621. .
2560(110) 0.0 2609. .
2670(110) 0.0 2597. .
2810(120) 0.0 2585. .
2620(110) 0.0 2573. .
2730(110) 0.0 2561. .
2490(110) 0.0 2549. .
2590(110) 0.0 2538. .
2560(110) 0.0 2527. .
2920(120) 0.0 2516. .
2670(110) 0.0 2505. .
2590(110) 0.0000826 2494. 2494.
2790(120) 0.0000756 2483. 2497.
2820(120) 0.0000756 2472. 2497.
2610(110) 0.0000812 2462. 2504.
2690(110) 0.0000797 2452. 2521.
2720(110) 0.0000783 2442. 2546.
2810(120) 0.0000756 2431. 2580.
2530(110) 0.0000842 2422. 2620.
2720(110) 0.0000783 2412. 2664.
2820(120) 0.0000756 2402. 2712.
2820(120) 0.0000756 2393. 2764.
2970(120) 0.0000718 2383. 2820.
2990(120) 0.0000706 2374. 2879.
2800(120) 0.0000756 2365. 2942.
2690(110) 0.0000797 2356. 3009.
2900(120) 0.0000731 2347. 3082.
2840(120) 0.0000756 2338. 3159.
3180(120) 0.0000672 2329. 3242.
3090(120) 0.0000694 2320. 3332.
3360(130) 0.0000640 2312. 3429.
3460(130) 0.0000620 2304. 3533.
3460(130) 0.0000620 2295. 3647.
3690(130) 0.0000583 2287. 3770.
3660(130) 0.0000583 2279. 3905.
3930(140) 0.0000549 2271. 4053.
3980(140) 0.0000541 2263. 4216.
4370(140) 0.0000489 2255. 4396.
4670(150) 0.0000457 2248. 4598.
4730(150) 0.0000457 2240. 4824.
4740(150) 0.0000450 2233. 5080.
5130(150) 0.0000422 2225. 5374.
5640(160) 0.0000381 2218. 5715.
5900(170) 0.0000367 2211. 6119.
6440(170) 0.0000334 2204. 6610.
7650(190) 0.0000283 2197. 7228.
8310(200) 0.0000260 2190. 8044.
9450(210) 0.0000229 2183. 9156.
11090(230) 0.0000196 2177. 10653.
13410(250) 0.0000161 2170. 12485.
14910(260) 0.0000146 2163. 14279.
16170(270) 0.0000134 2157. 15320.
15940(270) 0.0000136 2151. 14875.
13660(250) 0.0000159 2144. 12769.
10860(220) 0.0000199 2138. 9661.
7740(190) 0.0000280 2132. 6611.
4820(150) 0.0000444 2126. 4365.
3320(130) 0.0000640 2120. 3071.
2490(110) 0.0000857 2114. 2474.
2160(100) 0.0000980 2108. 2246.
2134(68) 0.0002163 2103. 2169.
2058(67) 0.0002228 2097. 2140.
2075(67) 0.0002228 2092. 2126.
2010(66) 0.0002296 2086. 2115.
1997(66) 0.0002296 2081. 2105.
1918(65) 0.0002367 2075. 2097.
1938(65) 0.0002367 2070. 2089.
1931(65) 0.0002367 2065. 2082.
2009(66) 0.0002296 2060. 2075.
1972(66) 0.0002296 2055. 2068.
1904(64) 0.0002441 2050. 2055.
1981(66) 0.0002296 2045. 2050.
2061(67) 0.0002228 2040. 2046.
1948(65) 0.0002367 2035. 2042.
1998(66) 0.0002296 2030. 2037.
1955(65) 0.0002367 2026. 2034.
2049(67) 0.0002228 2021. 2030.
2132(68) 0.0002163 2017. 2029.
2056(67) 0.0002228 2012. 2030.
2033(67) 0.0002228 2008. 2038.
2086(67) 0.0002228 2003. 2055.
2178(69) 0.0002100 1999. 2086.
2181(69) 0.0002100 1995. 2131.
2236(70) 0.0002041 1991. 2189.
2221(70) 0.0002041 1986. 2259.
2220(70) 0.0002041 1982. 2339.
2456(73) 0.0001877 1978. 2428.
2576(75) 0.0001778 1974. 2525.
2585(75) 0.0001778 1971. 2633.
2639(76) 0.0001731 1967. 2751.
2808(78) 0.0001644 1963. 2883.
2878(79) 0.0001602 1959. 3030.
3148(83) 0.0001452 1955. 3196.
3279(85) 0.0001384 1952. 3385.
3618(89) 0.0001262 1948. 3604.
3672(90) 0.0001235 1945. 3860.
4250(96) 0.0001085 1941. 4167.
4501(99) 0.0001020 1938. 4548.
5000(110) 0.0000907 1934. 5042.
6160(120) 0.0000743 1931. 5709.
6950(120) 0.0000661 1928. 6622.
8380(140) 0.0000541 1924. 7798.
9620(150) 0.0000476 1921. 9081.
10670(150) 0.0000427 1918. 10062.
10580(150) 0.0000433 1915. 10206.
9620(150) 0.0000476 1912. 9219.
7470(130) 0.0000610 1909. 7364.
5610(110) 0.0000812 1906. 5325.
3849(92) 0.0001181 1903. 3700.
2735(77) 0.0001687 1900. 2702.
2231(70) 0.0002041 1897. 2214.
2005(66) 0.0002296 1894. 2020.
1898(64) 0.0002441 1891. 1953.
1846(63) 0.0002520 1888. 1929.
1961(65) 0.0002367 1886. 1917.
1858(64) 0.0002441 1883. 1909.
1941(65) 0.0002367 1880. 1919.
1868(64) 0.0002441 1878. 1915.
1832(63) 0.0002520 1875. 1911.
1905(64) 0.0002441 1872. 1909.
1980(66) 0.0002296 1870. 1907.
2052(67) 0.0002228 1867. 1907.
1997(66) 0.0002296 1865. 1911.
2067(67) 0.0002228 1862. 1923.
2172(69) 0.0002100 1860. 1950.
2373(72) 0.0001929 1858. 2005.
2383(72) 0.0001929 1855. 2097.
2450(73) 0.0001877 1853. 2229.
2730(77) 0.0001687 1851. 2415.
2877(79) 0.0001602 1849. 2643.
3025(81) 0.0001524 1846. 2911.
3344(86) 0.0001352 1844. 3216.
3609(89) 0.0001262 1842. 3562.
3829(92) 0.0001181 1840. 3955.
4053(94) 0.0001132 1838. 4406.
4730(100) 0.0000961 1836. 4933.
5150(110) 0.0000890 1834. 5559.
5750(110) 0.0000797 1832. 6328.
6970(120) 0.0000650 1830. 7310.
8360(140) 0.0000549 1828. 8627.
10090(150) 0.0000450 1826. 10432.
12800(170) 0.0000354 1824. 12815.
15480(180) 0.0000295 1822. 15559.
17860(200) 0.0000255 1820. 17921.
18460(200) 0.0000248 1818. 18777.
16750(190) 0.0000271 1816. 17307.
13240(170) 0.0000346 1815. 13793.
9200(140) 0.0000496 1813. 9577.
5950(110) 0.0000769 1811. 6029.
3723(90) 0.0001235 1809. 3752.
2667(76) 0.0001731 1808. 2601.
2107(68) 0.0002163 1806. 2128.
1910(64) 0.0002441 1804. 1962.
1883(64) 0.0002441 1803. 1905.
1775(62) 0.0002601 1801. 1880.
1808(63) 0.0002520 1799. 1865.
1797(85) 0.0001384 1798. 1854.
1936(88) 0.0001291 1796. 1844.
1852(86) 0.0001352 1795. 1837.
1750(84) 0.0001417 1793. 1830.
1893(63) 0.0002520 1792. 1824.
1857(63) 0.0002520 1790. 1820.
1877(63) 0.0002520 1789. 1815.
1859(63) 0.0002520 1787. 1811.
1704(60) 0.0002778 1786. 1808.
1774(61) 0.0002687 1784. 1805.
1828(62) 0.0002601 1783. 1803.
1817(62) 0.0002601 1782. 1784.
1679(59) 0.0002873 1780. 1784.
1736(60) 0.0002778 1779. 1783.
1834(62) 0.0002601 1777. 1783.
1779(61) 0.0002687 1776. 1783.
1922(64) 0.0002441 1775. 1784.
1916(64) 0.0002441 1773. 1785.
1838(62) 0.0002601 1772. 1787.
1762(61) 0.0002687 1771. 1791.
1731(60) 0.0002778 1770. 1795.
1898(63) 0.0002520 1768. 1798.
1821(62) 0.0002601 1767. 1798.
1786(61) 0.0002687 1766. 1794.
1831(62) 0.0002601 1765. 1786.
1868(63) 0.0002520 1764. 1777.
1803(62) 0.0002601 1762. 1770.
1815(62) 0.0002601 1761. 1765.
1779(61) 0.0002687 1760. 1761.
1731(60) 0.0002778 1759. 1759.
1669(59) 0.0002873 1758. 1758.
1754(61) 0.0002687 1757. 1757.
1874(63) 0.0002520 1756. 1756.
1812(62) 0.0002601 1754. 1755.
1775(61) 0.0002687 1753. 1753.
1711(60) 0.0002778 1752. 1752.
1680(59) 0.0002873 1751. 1751.
1817(62) 0.0002601 1750. 1750.
1713(60) 0.0002778 1749. 1749.
1688(60) 0.0002778 1748. 1748.
1700(60) 0.0002778 1747. 1747.
1765(61) 0.0002687 1746. 1747.
1792(61) 0.0002687 1745. 1746.
1793(61) 0.0002687 1744. 1745.
1701(60) 0.0002778 1743. 1744.
1725(60) 0.0002778 1742. 1744.
1734(60) 0.0002778 1741. 1744.
1713(60) 0.0002778 1740. 1743.
1798(62) 0.0002601 1739. 1743.
1697(60) 0.0002778 1738. 1744.
1676(59) 0.0002873 1737. 1744.
1708(60) 0.0002778 1736. 1745.
1730(60) 0.0002778 1735. 1744.
1755(61) 0.0002687 1734. 1742.
1628(58) 0.0002973 1734. 1740.
1696(60) 0.0002778 1733. 1737.
1745(61) 0.0002687 1732. 1734.
1706(60) 0.0002778 1731. 1732.
1798(62) 0.0002601 1730. 1731.
1802(62) 0.0002601 1729. 1729.
1781(61) 0.0002687 1728. 1729.
1730(60) 0.0002778 1727. 1728.
1678(59) 0.0002873 1726. 1727.
1667(59) 0.0002873 1726. 1726.
1604(58) 0.0002973 1725. 1725.
1609(58) 0.0002973 1724. 1725.
1714(60) 0.0002778 1723. 1725.
1715(60) 0.0002778 1722. 1725.
1737(60) 0.0002778 1721. 1726.
1692(60) 0.0002778 1721. 1727.
1711(60) 0.0002778 1720. 1729.
1784(61) 0.0002687 1719. 1732.
1715(60) 0.0002778 1718. 1736.
1767(61) 0.0002687 1717. 1741.
1720(60) 0.0002778 1717. 1748.
1709(60) 0.0002778 1716. 1758.
1744(61) 0.0002687 1715. 1772.
1727(60) 0.0002778 1714. 1788.
1863(63) 0.0002520 1713. 1802.
1789(61) 0.0002687 1713. 1808.
1830(62) 0.0002601 1712. 1800.
1766(61) 0.0002687 1711. 1780.
1728(60) 0.0002778 1710. 1755.
1702(60) 0.0002778 1710. 1734.
1658(59) 0.0002873 1709. 1720.
1681(59) 0.0002873 1708. 1713.
1717(60) 0.0002778 1707. 1709.
1706(60) 0.0002778 1707. 1708.
1754(61) 0.0002687 1706. 1707.
1710(60) 0.0002778 1705. 1706.
1683(59) 0.0002873 1704. 1705.
1682(59) 0.0002873 1704. 1704.
1724(60) 0.0002778 1703. 1703.
1794(61) 0.0002687 1702. 1703.
1662(59) 0.0002873 1702. 1703.
1728(60) 0.0002778 1701. 1703.
1658(59) 0.0002873 1700. 1702.
1642(59) 0.0002873 1699. 1702.
1629(58) 0.0002973 1699. 1701.
1715(60) 0.0002778 1698. 1700.
1617(85) 0.0001384 1697. 1700.
1706(59) 0.0002873 1697. 1699.
1722(59) 0.0002873 1696. 1699.
1697(59) 0.0002873 1695. 1698.
1666(58) 0.0002973 1695. 1698.
1599(57) 0.0003078 1694. 1698.
1718(59) 0.0002873 1693. 1697.
1720(59) 0.0002873 1692. 1697.
1784(61) 0.0002687 1692. 1697.
1705(59) 0.0002873 1691. 1697.
1737(60) 0.0002778 1690. 1697.
1688(59) 0.0002873 1690. 1697.
1767(60) 0.0002778 1689. 1698.
1759(60) 0.0002778 1688. 1699.
1667(58) 0.0002973 1688. 1703.
1813(61) 0.0002687 1687. 1711.
1725(60) 0.0002778 1686. 1730.
1825(61) 0.0002687 1686. 1759.
1858(62) 0.0002601 1685. 1804.
1924(63) 0.0002520 1684. 1870.
1941(63) 0.0002520 1684. 1960.
2079(65) 0.0002367 1683. 2080.
2286(69) 0.0002100 1682. 2241.
2454(71) 0.0001984 1682. 2464.
2715(75) 0.0001778 1681. 2765.
3241(82) 0.0001487 1680. 3137.
3737(88) 0.0001291 1680. 3505.
3688(88) 0.0001291 1679. 3728.
3816(89) 0.0001262 1678. 3667.
3277(82) 0.0001487 1678. 3302.
2753(76) 0.0001731 1677. 2787.
2303(69) 0.0002100 1677. 2316.
1995(64) 0.0002441 1676. 1995.
1744(60) 0.0002778 1675. 1824.
1743(60) 0.0002778 1675. 1752.
1786(61) 0.0002687 1674. 1728.
1748(60) 0.0002778 1673. 1724.
1838(62) 0.0002601 1673. 1733.
1941(63) 0.0002520 1672. 1757.
1901(63) 0.0002520 1671. 1806.
1965(64) 0.0002441 1671. 1891.
2082(66) 0.0002296 1670. 2024.
2330(69) 0.0002100 1669. 2216.
2518(72) 0.0001929 1669. 2479.
2875(77) 0.0001687 1668. 2842.
3384(84) 0.0001417 1668. 3345.
4001(91) 0.0001208 1667. 4026.
4830(100) 0.0001000 1666. 4853.
5680(110) 0.0000842 1666. 5649.
6060(110) 0.0000783 1665. 6098.
5800(110) 0.0000826 1664. 5905.
4860(100) 0.0000980 1664. 5066.
3906(90) 0.0001235 1663. 3940.
2804(76) 0.0001731 1663. 2942.
2166(67) 0.0002228 1662. 2278.
1841(62) 0.0002601 1661. 1929.
1709(59) 0.0002873 1661. 1784.
1631(58) 0.0002973 1660. 1729.
1690(59) 0.0002873 1659. 1708.
1576(57) 0.0003078 1659. 1698.
1658(58) 0.0002973 1658. 1691.
1659(58) 0.0002973 1658. 1686.
1669(59) 0.0002873 1657. 1683.
1634(58) 0.0002973 1656. 1680.
1599(57) 0.0003078 1656. 1677.
1661(58) 0.0002973 1655. 1676.
1643(58) 0.0002973 1654. 1675.
1719(59) 0.0002873 1654. 1674.
1606(57) 0.0003078 1653. 1673.
1591(57) 0.0003078 1653. 1673.
1623(58) 0.0002973 1652. 1673.
1722(59) 0.0002873 1651. 1672.
1685(59) 0.0002873 1651. 1671.
1628(58) 0.0002973 1650. 1671.
1698(59) 0.0002873 1649. 1671.
1671(59) 0.0002873 1649. 1672.
1627(58) 0.0002973 1648. 1674.
1685(59) 0.0002873 1648. 1678.
1742(60) 0.0002778 1647. 1686.
1783(61) 0.0002687 1646. 1703.
1825(61) 0.0002687 1646. 1738.
1968(64) 0.0002441 1645. 1802.
1988(64) 0.0002441 1645. 1910.
2206(67) 0.0002228 1644. 2071.
2337(70) 0.0002041 1643. 2310.
2655(74) 0.0001826 1643. 2653.
3198(82) 0.0001487 1642. 3132.
3781(89) 0.0001262 1641. 3757.
4458(96) 0.0001085 1641. 4451.
5100(100) 0.0000943 1640. 5008.
5060(100) 0.0000943 1640. 5157.
4584(98) 0.0001041 1639. 4745.
3806(89) 0.0001262 1638. 3924.
2902(77) 0.0001687 1638. 3046.
2343(70) 0.0002041 1637. 2373.
1921(63) 0.0002520 1637. 1976.
1779(60) 0.0002778 1636. 1789.
1711(59) 0.0002873 1635. 1715.
1690(59) 0.0002873 1635. 1690.
1681(59) 0.0002873 1634. 1683.
1697(56) 0.0003189 1633. 1687.
1677(56) 0.0003189 1633. 1700.
1773(58) 0.0002973 1632. 1725.
1682(56) 0.0003189 1632. 1765.
1794(58) 0.0002973 1631. 1826.
1879(59) 0.0002873 1630. 1912.
2036(62) 0.0002601 1630. 2026.
2160(64) 0.0002441 1629. 2149.
2222(64) 0.0002441 1629. 2245.
2324(66) 0.0002296 1628. 2263.
2289(65) 0.0002367 1627. 2181.
2072(62) 0.0002601 1627. 2029.
1871(59) 0.0002873 1626. 1873.
1761(57) 0.0003078 1626. 1756.
1709(56) 0.0003189 1625. 1687.
1665(56) 0.0003189 1624. 1655.
1542(54) 0.0003429 1624. 1642.
1564(54) 0.0003429 1623. 1637.
1606(55) 0.0003306 1623. 1634.
1729(57) 0.0003078 1622. 1633.
1626(55) 0.0003306 1621. 1633.
1607(55) 0.0003306 1621. 1635.
1598(55) 0.0003306 1620. 1637.
1634(55) 0.0003306 1620. 1639.
1679(56) 0.0003189 1619. 1646.
1736(57) 0.0003078 1618. 1653.
1744(57) 0.0003078 1618. 1660.
1681(56) 0.0003189 1617. 1662.
1654(56) 0.0003189 1617. 1657.
1690(56) 0.0003189 1616. 1646.
1689(56) 0.0003189 1615. 1635.
1659(56) 0.0003189 1615. 1626.
1638(55) 0.0003306 1614. 1620.
1633(55) 0.0003306 1614. 1618.
1610(55) 0.0003306 1613. 1616.
1607(55) 0.0003306 1612. 1616.
1608(55) 0.0003306 1612. 1617.
1588(54) 0.0003429 1611. 1619.
1653(55) 0.0003306 1611. 1623.
1637(55) 0.0003306 1610. 1629.
1571(54) 0.0003429 1610. 1640.
1681(56) 0.0003189 1609. 1654.
1679(56) 0.0003189 1608. 1672.
1697(56) 0.0003189 1608. 1691.
1682(56) 0.0003189 1607. 1705.
1741(57) 0.0003078 1607. 1704.
1674(56) 0.0003189 1606. 1687.
1710(56) 0.0003189 1605. 1662.
1646(55) 0.0003306 1605. 1639.
1633(55) 0.0003306 1604. 1624.
1560(54) 0.0003429 1604. 1615.
1592(54) 0.0003429 1603. 1611.
1565(54) 0.0003429 1603. 1609.
1619(55) 0.0003306 1602. 1609.
1587(54) 0.0003429 1601. 1608.
1607(55) 0.0003306 1601. 1608.
1640(55) 0.0003306 1600. 1608.
1566(54) 0.0003429 1600. 1608.
1583(54) 0.0003429 1599. 1608.
1601(55) 0.0003306 1598. 1608.
1572(54) 0.0003429 1598. 1611.
1593(54) 0.0003429 1597. 1612.
1495(53) 0.000356 1597. 1613.
1486(53) 0.000356 1596. 1614.
1676(56) 0.0003189 1596. 1616.
1669(56) 0.0003189 1595. 1619.
1720(57) 0.0003078 1594. 1623.
1669(56) 0.0003189 1594. 1631.
1708(56) 0.0003189 1593. 1645.
1655(56) 0.0003189 1593. 1675.
1699(56) 0.0003189 1592. 1736.
1857(59) 0.0002873 1592. 1845.
2082(62) 0.0002601 1591. 2028.
2276(65) 0.0002367 1591. 2318.
2665(71) 0.0001984 1590. 2744.
3198(77) 0.0001687 1589. 3305.
3917(86) 0.0001352 1589. 3921.
4345(90) 0.0001235 1588. 4405.
4264(90) 0.0001235 1588. 4522.
3876(85) 0.0001384 1587. 4158.
3415(80) 0.0001562 1587. 3466.
2816(73) 0.0001877 1586. 2745.
2272(65) 0.0002367 1586. 2204.
1991(61) 0.0002687 1585. 1891.
1783(58) 0.0002973 1584. 1750.
1707(56) 0.0003189 1584. 1710.
1741(57) 0.0003078 1583. 1725.
1840(59) 0.0002873 1583. 1787.
1870(59) 0.0002873 1582. 1906.
1956(60) 0.0002778 1582. 2102.
2307(66) 0.0002296 1581. 2394.
2845(73) 0.0001877 1581. 2779.
3198(77) 0.0001687 1580. 3194.
3553(82) 0.0001487 1579. 3507.
3563(82) 0.0001487 1579. 3562.
3221(78) 0.0001644 1578. 3292.
2806(73) 0.0001877 1578. 2818.
2242(65) 0.0002367 1577. 2339.
1926(60) 0.0002778 1577. 1989.
1805(58) 0.0002973 1576. 1791.
1763(57) 0.0003078 1576. 1707.
1716(56) 0.0003189 1575. 1692.
1691(55) 0.0003306 1575. 1725.
1806(57) 0.0003078 1574. 1807.
1904(59) 0.0002873 1574. 1953.
2058(61) 0.0002687 1573. 2185.
2466(67) 0.0002228 1573. 2513.
2888(73) 0.0001877 1572. 2908.
3230(77) 0.0001687 1571. 3275.
3372(79) 0.0001602 1571. 3463.
3266(78) 0.0001644 1570. 3354.
3040(75) 0.0001778 1570. 2972.
2552(68) 0.0002163 1569. 2499.
2115(62) 0.0002601 1569. 2100.
1889(59) 0.0002873 1568. 1846.
1717(56) 0.0003189 1568. 1721.
1696(55) 0.0003306 1567. 1682.
1712(56) 0.0003189 1567. 1699.
1794(57) 0.0003078 1566. 1765.
1923(59) 0.0002873 1566. 1892.
2098(62) 0.0002601 1565. 2099.
2368(66) 0.0002296 1565. 2398.
2699(70) 0.0002041 1564. 2764.
3164(76) 0.0001731 1564. 3114.
3322(78) 0.0001644 1563. 3309.
3220(77) 0.0001687 1563. 3231.
2942(73) 0.0001877 1562. 2893.
2405(66) 0.0002296 1562. 2451.
2080(62) 0.0002601 1561. 2068.
1773(57) 0.0003078 1561. 1815.
1638(54) 0.0003429 1560. 1681.
1634(54) 0.0003429 1560. 1622.
1604(54) 0.0003429 1559. 1598.
1565(53) 0.000356 1559. 1588.
1564(53) 0.000356 1558. 1583.
1617(54) 0.0003429 1558. 1581.
1678(55) 0.0003306 1557. 1579.
1632(54) 0.0003429 1557. 1579.
1634(54) 0.0003429 1556. 1578.
1603(54) 0.0003429 1556. 1577.
1605(54) 0.0003429 1555. 1574.
1569(53) 0.000356 1555. 1571.
1602(54) 0.0003429 1554. 1567.
1616(54) 0.0003429 1554. 1562.
1563(53) 0.000356 1553. 1560.
1553(53) 0.000356 1553. 1559.
1598(54) 0.0003429 1552. 1558.
1590(54) 0.0003429 1552. 1558.
1516(52) 0.000370 1551. 1559.
1580(53) 0.000356 1551. 1561.
1629(54) 0.0003429 1550. 1565.
1666(55) 0.0003306 1550. 1569.
1572(53) 0.000356 1549. 1574.
1585(53) 0.000356 1549. 1576.
1589(54) 0.0003429 1548. 1575.
1587(53) 0.000356 1548. 1570.
1563(53) 0.000356 1548. 1564.
1530(52) 0.000370 1547. 1558.
1553(53) 0.000356 1547. 1552.
1644(54) 0.0003429 1546. 1551.
1598(54) 0.0003429 1546. 1552.
1550(53) 0.000356 1545. 1555.
1610(54) 0.0003429 1545. 1561.
1627(54) 0.0003429 1544. 1573.
1569(53) 0.000356 1544. 1591.
1593(54) 0.0003429 1543. 1614.
1715(56) 0.0003189 1543. 1637.
1726(56) 0.0003189 1542. 1652.
1706(56) 0.0003189 1542. 1650.
1730(56) 0.0003189 1542. 1630.
1728(56) 0.0003189 1541. 1602.
1572(53) 0.000356 1541. 1576.
1627(54) 0.0003429 1540. 1559.
1603(54) 0.0003429 1540. 1549.
1576(53) 0.000356 1539. 1544.
1509(52) 0.000370 1539. 1542.
1521(52) 0.000370 1538. 1541.
1575(53) 0.000356 1538. 1540.
1581(53) 0.000356 1538. 1539.
1521(52) 0.000370 1537. 1539.
1513(52) 0.000370 1537. 1538.
1526(52) 0.000370 1536. 1538.
1529(52) 0.000370 1536. 1538.
1579(53) 0.000356 1535. 1537.
1549(53) 0.000356 1535. 1537.
1567(53) 0.000356 1534. 1537.
1608(54) 0.0003429 1534. 1536.
1526(52) 0.000370 1534. 1536.
1535(53) 0.000356 1533. 1537.
1638(54) 0.0003429 1533. 1539.
1555(53) 0.000356 1532. 1542.
1503(52) 0.000370 1532. 1546.
1517(52) 0.000370 1532. 1553.
1485(52) 0.000370 1531. 1560.
1516(52) 0.000370 1531. 1567.
1620(54) 0.0003429 1530. 1568.
1609(54) 0.0003429 1530. 1563.
1544(53) 0.000356 1529. 1555.
1596(54) 0.0003429 1529. 1548.
1569(53) 0.000356 1529. 1543.
1538(51) 0.000384 1528. 1542.
1548(51) 0.000384 1528. 1545.
1583(52) 0.000370 1527. 1553.
1540(51) 0.000384 1527. 1570.
1596(52) 0.000370 1527. 1598.
1632(52) 0.000370 1526. 1638.
1613(52) 0.000370 1526. 1683.
1713(54) 0.0003429 1525. 1720.
1706(54) 0.0003429 1525. 1734.
1655(53) 0.000356 1524. 1715.
1652(53) 0.000356 1524. 1671.
1683(53) 0.000356 1524. 1623.
1603(52) 0.000370 1523. 1587.
1606(52) 0.000370 1523. 1569.
1565(51) 0.000384 1522. 1570.
1608(52) 0.000370 1522. 1590.
1613(52) 0.000370 1522. 1635.
1752(54) 0.0003429 1521. 1710.
1781(55) 0.0003306 1521. 1817.
1874(56) 0.0003189 1521. 1939.
2058(59) 0.0002873 1520. 2041.
2103(60) 0.0002778 1520. 2077.
1983(58) 0.0002973 1519. 2024.
1875(56) 0.0003189 1519. 1906.
1761(55) 0.0003306 1519. 1778.
1674(53) 0.000356 1518. 1683.
1590(52) 0.000370 1518. 1639.
1676(53) 0.000356 1517. 1649.
1692(53) 0.000356 1517. 1719.
1851(56) 0.0003189 1517. 1867.
2130(60) 0.0002778 1516. 2108.
2383(64) 0.0002441 1516. 2435.
2702(68) 0.0002163 1516. 2788.
3004(72) 0.0001929 1515. 3050.
3142(74) 0.0001826 1515. 3093.
2935(71) 0.0001984 1514. 2874.
2491(65) 0.0002367 1514. 2498.
2112(60) 0.0002778 1514. 2122.
1776(55) 0.0003306 1513. 1843.
1553(51) 0.000384 1513. 1678.
1557(51) 0.000384 1513. 1597.
1545(51) 0.000384 1512. 1563.
1555(51) 0.000384 1512. 1548.
1559(51) 0.000384 1511. 1541.
1501(50) 0.000400 1511. 1536.
1539(51) 0.000384 1511. 1533.
1576(52) 0.000370 1510. 1531.
1590(52) 0.000370 1510. 1530.
1488(50) 0.000400 1510. 1529.
1508(50) 0.000400 1509. 1530.
1525(51) 0.000384 1509. 1532.
1539(51) 0.000384 1509. 1539.
1538(51) 0.000384 1508. 1554.
1527(51) 0.000384 1508. 1585.
1638(53) 0.000356 1507. 1642.
1781(55) 0.0003306 1507. 1736.
1902(57) 0.0003078 1507. 1857.
1932(57) 0.0003078 1506. 1984.
2064(59) 0.0002873 1506. 2074.
2050(59) 0.0002873 1506. 2080.
1941(57) 0.0003078 1505. 1994.
1894(57) 0.0003078 1505. 1857.
1772(55) 0.0003306 1505. 1725.
1676(53) 0.000356 1504. 1632.
1550(51) 0.000384 1504. 1582.
1583(52) 0.000370 1504. 1568.
1475(50) 0.000400 1503. 1581.
1525(51) 0.000384 1503. 1618.
1603(52) 0.000370 1503. 1672.
1675(53) 0.000356 1502. 1732.
1701(54) 0.0003429 1502. 1778.
1706(54) 0.0003429 1502. 1788.
1612(52) 0.000370 1501. 1753.
1619(52) 0.000370 1501. 1688.
1605(52) 0.000370 1501. 1623.
1543(51) 0.000384 1500. 1573.
1546(51) 0.000384 1500. 1544.
1536(51) 0.000384 1500. 1529.
1554(51) 0.000384 1499. 1524.
1612(52) 0.000370 1499. 1523.
1567(51) 0.000384 1499. 1523.
1529(51) 0.000384 1498. 1524.
1507(50) 0.000400 1498. 1527.
1485(50) 0.000400 1498. 1530.
1512(50) 0.000400 1497. 1535.
1546(51) 0.000384 1497. 1544.
1600(52) 0.000370 1497. 1559.
1625(52) 0.000370 1496. 1590.
1691(53) 0.000356 1496. 1656.
1847(56) 0.0003189 1496. 1790.
2084(60) 0.0002778 1495. 2032.
2409(64) 0.0002441 1495. 2413.
2993(72) 0.0001929 1495. 2914.
3477(77) 0.0001687 1494. 3430.
3845(81) 0.0001524 1494. 3779.
3883(82) 0.0001487 1494. 3785.
3473(77) 0.0001687 1493. 3422.
2909(71) 0.0001984 1493. 2868.
2285(62) 0.0002601 1493. 2341.
2001(58) 0.0002973 1492. 1963.
1779(43) 0.000541 1492. 1749.
1647(49) 0.000416 1492. 1660.
1645(49) 0.000416 1491. 1648.
1703(50) 0.000400 1491. 1682.
1777(51) 0.000384 1491. 1737.
1746(51) 0.000384 1490. 1791.
1794(51) 0.000384 1490. 1818.
1763(51) 0.000384 1490. 1800.
1677(50) 0.000400 1489. 1742.
1663(49) 0.000416 1489. 1675.
1598(48) 0.000434 1489. 1622.
1589(48) 0.000434 1488. 1602.
1636(49) 0.000416 1488. 1624.
1635(49) 0.000416 1488. 1697.
1794(51) 0.000384 1488. 1828.
1988(54) 0.0003429 1487. 2009.
2194(57) 0.0003078 1487. 2205.
2290(58) 0.0002973 1487. 2348.
2231(57) 0.0003078 1486. 2371.
2122(56) 0.0003189 1486. 2252.
1957(54) 0.0003429 1486. 2050.
1788(51) 0.000384 1485. 1851.
1696(50) 0.000400 1485. 1706.
1722(50) 0.000400 1485. 1633.
1671(50) 0.000400 1484. 1624.
1771(51) 0.000384 1484. 1667.
1796(51) 0.000384 1484. 1752.
1914(53) 0.000356 1484. 1857.
1983(54) 0.0003429 1483. 1949.
2047(55) 0.0003306 1483. 1986.
1948(54) 0.0003429 1483. 1943.
1786(51) 0.000384 1482. 1840.
1716(50) 0.000400 1482. 1722.
1596(48) 0.000434 1482. 1626.
1587(48) 0.000434 1481. 1563.
1603(48) 0.000434 1481. 1533.
1560(48) 0.000434 1481. 1526.
1554(48) 0.000434 1481. 1532.
1556(48) 0.000434 1480. 1545.
1630(49) 0.000416 1480. 1558.
1631(49) 0.000416 1480. 1565.
1635(49) 0.000416 1479. 1560.
1579(48) 0.000434 1479. 1544.
1645(49) 0.000416 1479. 1525.
1539(48) 0.000434 1478. 1509.
1496(47) 0.000453 1478. 1497.
1475(47) 0.000453 1478. 1490.
1458(46) 0.000473 1478. 1487.
1581(48) 0.000434 1477. 1486.
1513(47) 0.000453 1477. 1485.
1514(47) 0.000453 1477. 1485.
1535(47) 0.000453 1476. 1485.
1540(48) 0.000434 1476. 1485.
1486(47) 0.000453 1476. 1485.
1476(47) 0.000453 1475. 1487.
1470(46) 0.000473 1475. 1491.
1488(47) 0.000453 1475. 1501.
1518(47) 0.000453 1475. 1519.
1594(48) 0.000434 1474. 1553.
1618(49) 0.000416 1474. 1603.
1629(49) 0.000416 1474. 1664.
1706(50) 0.000400 1473. 1720.
1726(50) 0.000400 1473. 1749.
1685(50) 0.000400 1473. 1734.
1651(49) 0.000416 1473. 1682.
1609(49) 0.000416 1472. 1616.
1640(49) 0.000416 1472. 1559.
1587(48) 0.000434 1472. 1520.
1514(47) 0.000453 1471. 1498.
1484(47) 0.000453 1471. 1486.
1498(47) 0.000453 1471. 1482.
1399(45) 0.000494 1470. 1479.
1411(45) 0.000494 1470. 1478.
1409(45) 0.000494 1470. 1477.
1459(46) 0.000473 1470. 1477.
1494(47) 0.000453 1469. 1477.
1504(47) 0.000453 1469. 1477.
1529(47) 0.000453 1469. 1477.
1466(46) 0.000473 1468. 1479.
1440(46) 0.000473 1468. 1482.
1493(47) 0.000453 1468. 1488.
1492(47) 0.000453 1468. 1495.
1499(47) 0.000453 1467. 1502.
1551(48) 0.000434 1467. 1509.
1545(48) 0.000434 1467. 1511.
1465(46) 0.000473 1466. 1510.
1511(47) 0.000453 1466. 1508.
1502(47) 0.000453 1466. 1512.
1460(46) 0.000473 1466. 1530.
1543(48) 0.000434 1465. 1574.
1625(49) 0.000416 1465. 1653.
1754(51) 0.000384 1465. 1775.
1964(54) 0.0003429 1464. 1926.
2110(56) 0.0003189 1464. 2068.
2095(56) 0.0003189 1464. 2147.
2057(55) 0.0003306 1464. 2121.
1924(53) 0.000356 1463. 2000.
1797(51) 0.000384 1463. 1842.
1672(50) 0.000400 1463. 1703.
1668(49) 0.000416 1462. 1613.
1624(46) 0.000473 1462. 1573.
1598(46) 0.000473 1462. 1576.
1689(47) 0.000453 1461. 1607.
1704(47) 0.000453 1461. 1649.
1768(48) 0.000434 1461. 1682.
1708(47) 0.000453 1461. 1687.
1727(47) 0.000453 1460. 1660.
1726(47) 0.000453 1460. 1612.
1551(45) 0.000494 1460. 1563.
1541(45) 0.000494 1459. 1527.
1564(45) 0.000494 1459. 1507.
1517(44) 0.000517 1459. 1504.
1542(45) 0.000494 1459. 1512.
1571(45) 0.000494 1458. 1526.
1583(45) 0.000494 1458. 1540.
1518(44) 0.000517 1458. 1546.
1564(45) 0.000494 1457. 1539.
1611(46) 0.000473 1457. 1524.
1505(44) 0.000517 1457. 1505.
1517(44) 0.000517 1457. 1491.
1454(43) 0.000541 1456. 1482.
1525(45) 0.000494 1456. 1480.
1442(43) 0.000541 1456. 1483.
1423(43) 0.000541 1455. 1489.
1458(44) 0.000517 1455. 1495.
1490(44) 0.000517 1455. 1500.
1531(45) 0.000494 1455. 1501.
1448(43) 0.000541 1454. 1499.
1431(43) 0.000541 1454. 1498.
1528(45) 0.000494 1454. 1508.
1534(45) 0.000494 1453. 1534.
1555(45) 0.000494 1453. 1589.
1671(47) 0.000453 1453. 1676.
1764(48) 0.000434 1452. 1789.
1865(49) 0.000416 1452. 1903.
2000(51) 0.000384 1452. 1977.
1885(50) 0.000400 1452. 1975.
1796(48) 0.000434 1451. 1894.
1741(48) 0.000434 1451. 1774.
1562(45) 0.000494 1451. 1659.
1547(45) 0.000494 1450. 1572.
1540(45) 0.000494 1450. 1519.
1469(44) 0.000517 1450. 1491.
1530(45) 0.000494 1450. 1480.
1503(44) 0.000517 1449. 1475.
1471(44) 0.000517 1449. 1474.
1447(43) 0.000541 1449. 1472.
1432(43) 0.000541 1448. 1469.
1422(43) 0.000541 1448. 1466.
1484(44) 0.000517 1448. 1464.
1433(43) 0.000541 1448. 1462.
1486(44) 0.000517 1447. 1460.
1506(44) 0.000517 1447. 1460.
1443(43) 0.000541 1447. 1460.
1464(44) 0.000517 1446. 1460.
1454(43) 0.000541 1446. 1461.
1441(43) 0.000541 1446. 1463.
1461(44) 0.000517 1445. 1466.
1455(43) 0.000541 1445. 1474.
1452(43) 0.000541 1445. 1489.
1529(45) 0.000494 1445. 1518.
1568(45) 0.000494 1444. 1569.
1664(47) 0.000453 1444. 1646.
1726(47) 0.000453 1444. 1742.
1816(49) 0.000416 1443. 1836.
1878(50) 0.000400 1443. 1895.
1833(49) 0.000416 1443. 1889.
1808(49) 0.000416 1443. 1822.
1676(47) 0.000453 1442. 1727.
1630(46) 0.000473 1442. 1640.
1564(45) 0.000494 1442. 1584.
1538(45) 0.000494 1441. 1564.
1515(44) 0.000517 1441. 1576.
1597(46) 0.000473 1441. 1608.
1645(46) 0.000473 1440. 1643.
1658(46) 0.000473 1440. 1664.
1640(46) 0.000473 1440. 1661.
1564(45) 0.000494 1440. 1641.
1575(45) 0.000494 1439. 1626.
1576(45) 0.000494 1439. 1643.
1765(48) 0.000434 1439. 1718.
1879(50) 0.000400 1438. 1869.
2105(52) 0.000370 1438. 2092.
2341(55) 0.0003306 1438. 2347.
2566(58) 0.0002973 1437. 2558.
2641(59) 0.0002873 1437. 2635.
2465(57) 0.0003078 1437. 2534.
2309(55) 0.0003306 1437. 2308.
2036(52) 0.000370 1436. 2058.
1844(49) 0.000416 1436. 1863.
1714(47) 0.000453 1436. 1761.
1666(47) 0.000453 1435. 1749.
1800(48) 0.000434 1435. 1804.
1872(49) 0.000416 1435. 1882.
1972(51) 0.000384 1434. 1940.
1996(51) 0.000384 1434. 1938.
1871(49) 0.000416 1434. 1874.
1742(48) 0.000434 1434. 1782.
1655(46) 0.000473 1433. 1704.
1693(47) 0.000453 1433. 1671.
1728(45) 0.000494 1433. 1698.
1765(45) 0.000494 1432. 1779.
1972(48) 0.000434 1432. 1893.
2133(50) 0.000400 1432. 1997.
2182(50) 0.000400 1431. 2044.
2071(49) 0.000416 1431. 2005.
1981(48) 0.000434 1431. 1899.
1899(47) 0.000453 1430. 1774.
1726(45) 0.000494 1430. 1671.
1614(43) 0.000541 1430. 1612.
1639(44) 0.000517 1430. 1599.
1587(43) 0.000541 1429. 1620.
1597(43) 0.000541 1429. 1657.
1612(43) 0.000541 1429. 1684.
1601(43) 0.000541 1428. 1684.
1612(43) 0.000541 1428. 1653.
1577(43) 0.000541 1428. 1607.
1588(43) 0.000541 1427. 1566.
1524(42) 0.000567 1427. 1544.
1488(42) 0.000567 1427. 1549.
1546(42) 0.000567 1427. 1578.
1610(43) 0.000541 1426. 1619.
1679(44) 0.000517 1426. 1656.
1713(45) 0.000494 1426. 1670.
1653(44) 0.000517 1425. 1650.
1628(44) 0.000517 1425. 1606.
1580(43) 0.000541 1425. 1554.
1550(42) 0.000567 1424. 1509.
1524(42) 0.000567 1424. 1477.
1502(42) 0.000567 1424. 1457.
1549(42) 0.000567 1423. 1447.
1503(42) 0.000567 1423. 1441.
1429(41) 0.000595 1423. 1439.
1436(41) 0.000595 1422. 1438.
1407(40) 0.000625 1422. 1439.
1404(40) 0.000625 1422. 1441.
1453(41) 0.000595 1422. 1446.
1464(41) 0.000595 1421. 1454.
1411(40) 0.000625 1421. 1468.
1445(41) 0.000595 1421. 1485.
1497(42) 0.000567 1420. 1503.
1517(42) 0.000567 1420. 1516.
1457(41) 0.000595 1420. 1521.
1492(42) 0.000567 1419. 1518.
1435(41) 0.000595 1419. 1514.
1494(42) 0.000567 1419. 1524.
1536(42) 0.000567 1418. 1559.
1651(44) 0.000517 1418. 1624.
1725(45) 0.000494 1418. 1719.
1757(45) 0.000494 1417. 1823.
1886(47) 0.000453 1417. 1903.
1996(48) 0.000434 1417. 1926.
1904(47) 0.000453 1417. 1877.
1756(45) 0.000494 1416. 1779.
1610(43) 0.000541 1416. 1671.
1473(41) 0.000595 1416. 1580.
1458(41) 0.000595 1415. 1518.
1456(41) 0.000595 1415. 1483.
1466(41) 0.000595 1415. 1467.
1430(41) 0.000595 1414. 1461.
1439(41) 0.000595 1414. 1460.
1460(41) 0.000595 1414. 1463.
1457(41) 0.000595 1413. 1472.
1492(42) 0.000567 1413. 1494.
1543(42) 0.000567 1413. 1538.
1624(43) 0.000541 1412. 1611.
1782(46) 0.000473 1412. 1713.
1885(47) 0.000453 1412. 1828.
1989(48) 0.000434 1412. 1926.
1993(48) 0.000434 1411. 1969.
1957(48) 0.000434 1411. 1933.
1847(46) 0.000473 1411. 1836.
1792(46) 0.000473 1410. 1718.
1626(44) 0.000517 1410. 1612.
1538(42) 0.000567 1410. 1534.
1511(42) 0.000567 1409. 1486.
1495(42) 0.000567 1409. 1460.
1473(41) 0.000595 1409. 1448.
1454(41) 0.000595 1408. 1446.
1437(41) 0.000595 1408. 1449.
1487(42) 0.000567 1408. 1462.
1486(42) 0.000567 1407. 1489.
1524(42) 0.000567 1407. 1538.
1576(43) 0.000541 1407. 1618.
1693(44) 0.000517 1406. 1726.
1827(46) 0.000473 1406. 1847.
1992(48) 0.000434 1406. 1950.
2032(49) 0.000416 1405. 1993.
1953(48) 0.000434 1405. 1957.
1893(47) 0.000453 1405. 1858.
1785(46) 0.000473 1405. 1739.
1657(44) 0.000517 1404. 1637.
1574(43) 0.000541 1404. 1568.
1566(43) 0.000541 1404. 1535.
1578(43) 0.000541 1403. 1527.
1597(43) 0.000541 1403. 1529.
1565(43) 0.000541 1403. 1528.
1594(43) 0.000541 1402. 1516.
1593(43) 0.000541 1402. 1495.
1536(42) 0.000567 1402. 1471.
1502(40) 0.000625 1401. 1451.
1487(40) 0.000625 1401. 1435.
1426(39) 0.000657 1401. 1426.
1419(39) 0.000657 1400. 1420.
1418(39) 0.000657 1400. 1417.
1389(38) 0.000693 1400. 1416.
1407(38) 0.000693 1399. 1416.
1451(39) 0.000657 1399. 1418.
1401(38) 0.000693 1399. 1422.
1411(39) 0.000657 1398. 1429.
1424(39) 0.000657 1398. 1439.
1485(39) 0.000657 1398. 1451.
1481(39) 0.000657 1397. 1464.
1499(40) 0.000625 1397. 1473.
1477(39) 0.000657 1397. 1478.
1550(40) 0.000625 1396. 1480.
1506(40) 0.000625 1396. 1486.
1561(40) 0.000625 1396. 1506.
1541(40) 0.000625 1396. 1546.
1616(41) 0.000595 1395. 1608.
1666(42) 0.000567 1395. 1683.
1802(43) 0.000541 1395. 1754.
1830(44) 0.000517 1394. 1795.
1769(43) 0.000541 1394. 1791.
1776(43) 0.000541 1394. 1751.
1636(41) 0.000595 1393. 1705.
1685(42) 0.000567 1393. 1685.
1717(42) 0.000567 1393. 1709.
1815(44) 0.000517 1392. 1780.
1838(44) 0.000517 1392. 1876.
1906(45) 0.000494 1392. 1960.
1953(45) 0.000494 1391. 1991.
1960(45) 0.000494 1391. 1947.
1919(45) 0.000494 1391. 1846.
1664(42) 0.000567 1390. 1726.
1589(41) 0.000595 1390. 1619.
1518(40) 0.000625 1390. 1542.
1503(40) 0.000625 1389. 1495.
1486(39) 0.000657 1389. 1474.
1489(40) 0.000625 1389. 1463.
1438(39) 0.000657 1388. 1458.
1453(39) 0.000657 1388. 1454.
1437(39) 0.000657 1388. 1455.
1375(38) 0.000693 1388. 1464.
1494(40) 0.000625 1387. 1484.
1505(40) 0.000625 1387. 1516.
1547(40) 0.000625 1387. 1555.
1584(41) 0.000595 1386. 1591.
1539(40) 0.000625 1386. 1610.
1582(41) 0.000595 1386. 1603.
1580(41) 0.000595 1385. 1574.
1553(40) 0.000625 1385. 1537.
1495(40) 0.000625 1385. 1506.
1424(39) 0.000657 1384. 1489.
1464(39) 0.000657 1384. 1486.
1493(40) 0.000625 1384. 1493.
1464(39) 0.000657 1383. 1501.
1449(39) 0.000657 1383. 1501.
1410(38) 0.000693 1383. 1489.
1430(39) 0.000657 1382. 1470.
1414(39) 0.000657 1382. 1450.
1397(38) 0.000693 1382. 1433.
1416(39) 0.000657 1381. 1422.
1364(38) 0.000693 1381. 1416.
1427(39) 0.000657 1381. 1414.
1328(37) 0.000730 1380. 1413.
1422(39) 0.000657 1380. 1411.
1363(38) 0.000693 1380. 1407.
1441(39) 0.000657 1380. 1403.
1428(39) 0.000657 1379. 1400.
1392(38) 0.000693 1379. 1397.
1403(38) 0.000693 1379. 1395.
1379(38) 0.000693 1378. 1394.
1401(38) 0.000693 1378. 1394.
1385(38) 0.000693 1378. 1395.
1431(39) 0.000657 1377. 1396.
1358(38) 0.000693 1377. 1399.
1372(38) 0.000693 1377. 1403.
1466(39) 0.000657 1376. 1409.
1404(38) 0.000693 1376. 1417.
1397(38) 0.000693 1376. 1427.
1395(38) 0.000693 1375. 1437.
1417(39) 0.000657 1375. 1448.
1427(39) 0.000657 1375. 1463.
1485(39) 0.000657 1374. 1486.
1466(39) 0.000657 1374. 1529.
1591(41) 0.000595 1374. 1601.
1779(43) 0.000541 1374. 1705.
1782(43) 0.000541 1373. 1831.
1923(45) 0.000494 1373. 1955.
2044(46) 0.000473 1373. 2043.
2053(46) 0.000473 1372. 2065.
2058(46) 0.000473 1372. 2025.
1918(45) 0.000494 1372. 1963.
1916(45) 0.000494 1371. 1931.
1913(45) 0.000494 1371. 1959.
2040(46) 0.000473 1371. 2053.
2248(48) 0.000434 1370. 2182.
2351(50) 0.000400 1370. 2294.
2342(49) 0.000416 1370. 2328.
2231(47) 0.000453 1369. 2259.
2109(46) 0.000473 1369. 2114.
1935(44) 0.000517 1369. 1950.
1867(43) 0.000541 1369. 1813.
1742(41) 0.000595 1368. 1726.
1743(41) 0.000595 1368. 1685.
1755(41) 0.000595 1368. 1673.
1705(41) 0.000595 1367. 1665.
1731(41) 0.000595 1367. 1642.
1668(40) 0.000625 1367. 1600.
1566(39) 0.000657 1366. 1551.
1541(39) 0.000657 1366. 1506.
1456(38) 0.000693 1366. 1472.
1494(38) 0.000693 1365. 1451.
1455(38) 0.000693 1365. 1440.
1434(37) 0.000730 1365. 1435.
1434(37) 0.000730 1365. 1433.
1375(37) 0.000730 1364. 1433.
1419(37) 0.000730 1364. 1438.
1461(38) 0.000693 1364. 1452.
1435(37) 0.000730 1363. 1475.
1497(38) 0.000693 1363. 1505.
1508(38) 0.000693 1363. 1537.
1531(39) 0.000657 1362. 1559.
1525(39) 0.000657 1362. 1563.
1593(40) 0.000625 1362. 1547.
1545(39) 0.000657 1362. 1517.
1528(39) 0.000657 1361. 1487.
1478(38) 0.000693 1361. 1463.
1545(39) 0.000657 1361. 1449.
1476(38) 0.000693 1360. 1444.
1528(39) 0.000657 1360. 1443.
1524(39) 0.000657 1360. 1440.
1575(39) 0.000657 1359. 1433.
1502(38) 0.000693 1359. 1422.
1511(38) 0.000693 1359. 1411.
1534(39) 0.000657 1359. 1400.
1457(38) 0.000693 1358. 1393.
1444(38) 0.000693 1358. 1389.
1396(37) 0.000730 1358. 1388.
1389(37) 0.000730 1357. 1392.
1352(36) 0.000772 1357. 1401.
1402(37) 0.000730 1357. 1418.
1465(38) 0.000693 1356. 1445.
1502(38) 0.000693 1356. 1485.
1559(39) 0.000657 1356. 1536.
1633(40) 0.000625 1356. 1593.
1602(40) 0.000625 1355. 1643.
1649(40) 0.000625 1355. 1676.
1618(40) 0.000625 1355. 1687.
1680(41) 0.000595 1354. 1688.
1694(41) 0.000595 1354. 1703.
1748(41) 0.000595 1354. 1749.
1818(42) 0.000567 1353. 1831.
1944(44) 0.000517 1353. 1935.
2052(45) 0.000494 1353. 2031.
2097(45) 0.000494 1353. 2078.
2021(45) 0.000494 1352. 2049.
1961(44) 0.000517 1352. 1953.
1879(43) 0.000541 1352. 1823.
1695(41) 0.000595 1351. 1697.
1567(39) 0.000657 1351. 1596.
1544(39) 0.000657 1351. 1525.
1503(38) 0.000693 1351. 1482.
1449(38) 0.000693 1350. 1456.
1428(37) 0.000730 1350. 1439.
1390(37) 0.000730 1350. 1424.
1438(38) 0.000693 1349. 1412.
1415(37) 0.000730 1349. 1401.
1411(37) 0.000730 1349. 1394.
1399(37) 0.000730 1349. 1389.
1367(37) 0.000730 1348. 1388.
1286(35) 0.000816 1348.0 1388.9
1404(37) 0.000730 1348. 1392.
1428(37) 0.000730 1347. 1400.
1376(37) 0.000730 1347. 1413.
1522(39) 0.000657 1347. 1432.
1527(39) 0.000657 1347. 1457.
1529(39) 0.000657 1346. 1483.
1492(38) 0.000693 1346. 1504.
1504(38) 0.000693 1346. 1514.
1456(38) 0.000693 1346. 1509.
1532(39) 0.000657 1345. 1497.
1500(38) 0.000693 1345. 1485.
1455(38) 0.000693 1345. 1482.
1562(39) 0.000657 1344. 1488.
1534(39) 0.000657 1344. 1502.
1545(39) 0.000657 1344. 1518.
1562(39) 0.000657 1344. 1530.
1569(39) 0.000657 1343. 1538.
1496(38) 0.000693 1343. 1550.
1508(38) 0.000693 1343. 1576.
1513(38) 0.000693 1342. 1623.
1636(40) 0.000625 1342. 1689.
1745(41) 0.000595 1342. 1759.
1755(41) 0.000595 1342. 1811.
1825(42) 0.000567 1341. 1820.
1775(42) 0.000567 1341. 1779.
1649(40) 0.000625 1341. 1704.
1611(40) 0.000625 1341. 1617.
1572(38) 0.000693 1340. 1537.
1414(36) 0.000772 1340. 1474.
1389(36) 0.000772 1340. 1431.
1367(35) 0.000816 1339.5 1406.7
1403(36) 0.000772 1339. 1397.
1419(36) 0.000772 1339. 1398.
1391(36) 0.000772 1339. 1410.
1427(36) 0.000772 1338. 1432.
1472(37) 0.000730 1338. 1462.
1461(36) 0.000772 1338. 1498.
1514(37) 0.000730 1338. 1532.
1549(38) 0.000693 1337. 1555.
1518(37) 0.000730 1337. 1562.
1604(38) 0.000693 1337. 1554.
1562(38) 0.000693 1337. 1540.
1454(36) 0.000772 1336. 1530.
1475(37) 0.000730 1336. 1532.
1480(37) 0.000730 1336. 1545.
1490(37) 0.000730 1336. 1566.
1552(38) 0.000693 1335. 1589.
1538(37) 0.000730 1335. 1611.
1624(38) 0.000693 1335. 1638.
1648(39) 0.000657 1335. 1685.
1705(39) 0.000657 1334. 1763.
1832(41) 0.000595 1334. 1870.
2008(43) 0.000541 1334. 1993.
2038(43) 0.000541 1333. 2099.
2150(44) 0.000517 1333. 2150.
2143(44) 0.000517 1333. 2120.
2056(43) 0.000541 1333. 2023.
1903(42) 0.000567 1332. 1894.
1807(41) 0.000595 1332. 1769.
1688(39) 0.000657 1332. 1668.
1636(39) 0.000657 1332. 1598.
1512(37) 0.000730 1331. 1554.
1529(37) 0.000730 1331. 1522.
1458(36) 0.000772 1331. 1494.
1486(37) 0.000730 1331. 1464.
1414(36) 0.000772 1330. 1435.
1386(35) 0.000816 1330.2 1409.9
1351(35) 0.000816 1330.0 1389.4
1395(36) 0.000772 1330. 1374.
1371(35) 0.000816 1329.5 1364.3
1354(35) 0.000816 1329.2 1358.5
1340(35) 0.000816 1329.0 1355.5
1340(35) 0.000816 1328.8 1354.5
1321(35) 0.000816 1328.5 1355.0
1391(36) 0.000772 1328. 1357.
1374(35) 0.000816 1328.0 1359.8
1347(35) 0.000816 1327.8 1363.7
1342(35) 0.000816 1327.5 1369.0
1359(35) 0.000816 1327.3 1376.5
1350(35) 0.000816 1327.1 1388.0
1383(35) 0.000816 1326.8 1405.6
1421(36) 0.000772 1327. 1430.
1432(36) 0.000772 1326. 1461.
1482(37) 0.000730 1326. 1494.
1484(37) 0.000730 1326. 1521.
1503(37) 0.000730 1326. 1533.
1499(37) 0.000730 1325. 1525.
1453(36) 0.000772 1325. 1500.
1483(37) 0.000730 1325. 1466.
1439(36) 0.000772 1325. 1432.
1451(36) 0.000772 1324. 1403.
1377(35) 0.000816 1324.2 1381.3
1377(35) 0.000816 1324.0 1367.8
1349(35) 0.000816 1323.7 1361.3
1345(35) 0.000816 1323.5 1360.6
1352(35) 0.000816 1323.3 1364.7
1328(35) 0.000816 1323.1 1373.1
1398(36) 0.000772 1323. 1385.
1462(36) 0.000772 1323. 1400.
1410(36) 0.000772 1322. 1418.
1447(36) 0.000772 1322. 1438.
1498(37) 0.000730 1322. 1463.
1502(37) 0.000730 1322. 1497.
1534(37) 0.000730 1321. 1546.
1648(39) 0.000657 1321. 1615.
1652(39) 0.000657 1321. 1699.
1769(40) 0.000625 1321. 1788.
1810(41) 0.000595 1321. 1861.
1872(41) 0.000595 1320. 1895.
1819(41) 0.000595 1320. 1876.
1791(40) 0.000625 1320. 1815.
1721(40) 0.000625 1320. 1735.
1709(39) 0.000657 1319. 1656.
1645(39) 0.000657 1319. 1593.
1523(37) 0.000730 1319. 1548.
1501(37) 0.000730 1319. 1518.
1524(37) 0.000730 1319. 1496.
1512(37) 0.000730 1318. 1476.
1482(37) 0.000730 1318. 1458.
1508(37) 0.000730 1318. 1443.
1551(38) 0.000693 1318. 1434.
1515(37) 0.000730 1317. 1431.
1489(37) 0.000730 1317. 1431.
1412(36) 0.000772 1317. 1431.
1524(37) 0.000730 1317. 1429.
1485(37) 0.000730 1317. 1425.
1472(37) 0.000730 1316. 1422.
1491(51) 0.000384 1316. 1423.
1450(35) 0.000816 1316.0 1428.4
1463(35) 0.000816 1315.7 1437.3
1420(35) 0.000816 1315.5 1447.7
1423(35) 0.000816 1315.3 1457.1
1425(35) 0.000816 1315.1 1465.7
1487(35) 0.000816 1314.9 1477.1
1555(36) 0.000772 1315. 1495.
1581(37) 0.000730 1314. 1522.
1659(37) 0.000730 1314. 1553.
1638(37) 0.000730 1314. 1582.
1679(38) 0.000693 1314. 1597.
1653(37) 0.000730 1314. 1590.
1597(37) 0.000730 1313. 1562.
1548(36) 0.000772 1313. 1520.
1515(36) 0.000772 1313. 1475.
1514(36) 0.000772 1313. 1434.
1448(35) 0.000816 1312.6 1401.4
1381(34) 0.000865 1312.4 1377.8
1386(34) 0.000865 1312.2 1361.9
1328(34) 0.000865 1312.0 1351.3
1281(33) 0.000918 1311.8 1344.2
1326(33) 0.000918 1311.6 1339.6
1368(34) 0.000865 1311.4 1336.6
1329(34) 0.000865 1311.2 1335.3
1307(33) 0.000918 1311.0 1336.0
1372(34) 0.000865 1310.8 1339.2
1352(34) 0.000865 1310.6 1345.6
1410(35) 0.000816 1310.4 1356.5
1419(35) 0.000816 1310.2 1372.3
1374(34) 0.000865 1310.0 1392.8
1408(34) 0.000865 1309.8 1416.8
1445(35) 0.000816 1309.6 1441.4
1463(35) 0.000816 1309.4 1462.4
1488(35) 0.000816 1309.2 1476.6
1472(35) 0.000816 1309.0 1483.5
1460(35) 0.000816 1308.8 1487.1
1526(36) 0.000772 1309. 1493.
1531(36) 0.000772 1308. 1504.
1534(36) 0.000772 1308. 1520.
1577(36) 0.000772 1308. 1535.
1570(36) 0.000772 1308. 1544.
1622(37) 0.000730 1308. 1540.
1596(37) 0.000730 1307. 1524.
1528(36) 0.000772 1307. 1502.
1538(36) 0.000772 1307. 1480.
1505(36) 0.000772 1307. 1464.
1516(36) 0.000772 1307. 1454.
1467(35) 0.000816 1306.5 1448.3
1456(35) 0.000816 1306.3 1445.0
1446(35) 0.000816 1306.1 1442.0
1488(35) 0.000816 1305.9 1441.6
1505(36) 0.000772 1306. 1445.
1485(35) 0.000816 1305.5 1453.7
1451(35) 0.000816 1305.4 1465.8
1442(35) 0.000816 1305.2 1478.1
1432(35) 0.000816 1305.0 1486.1
1461(35) 0.000816 1304.8 1487.1
1456(35) 0.000816 1304.6 1482.6
1448(35) 0.000816 1304.4 1477.2
1505(36) 0.000772 1304. 1475.
1500(36) 0.000772 1304. 1476.
1456(35) 0.000816 1303.9 1479.8
1495(36) 0.000772 1304. 1481.
1510(36) 0.000772 1304. 1475.
1485(35) 0.000816 1303.3 1460.6
1465(35) 0.000816 1303.1 1440.3
1364(34) 0.000865 1303.0 1418.7
1347(34) 0.000865 1302.8 1399.4
1354(34) 0.000865 1302.6 1384.7
1384(34) 0.000865 1302.4 1375.4
1334(34) 0.000865 1302.2 1371.4
1299(33) 0.000918 1302.1 1372.2
1330(34) 0.000865 1301.9 1378.0
1341(34) 0.000865 1301.7 1388.4
1373(34) 0.000865 1301.5 1402.6
1415(35) 0.000816 1301.3 1418.4
1425(35) 0.000816 1301.2 1432.0
1452(35) 0.000816 1301.0 1438.9
1430(35) 0.000816 1300.8 1435.9
1472(35) 0.000816 1300.6 1423.0
1454(35) 0.000816 1300.4 1404.8
1337(34) 0.000865 1300.3 1383.9
1331(34) 0.000865 1300.1 1364.4
1305(33) 0.000918 1299.9 1348.2
1292(33) 0.000918 1299.7 1336.1
1302(33) 0.000918 1299.6 1328.0
1312(33) 0.000918 1299.4 1323.1
1305(33) 0.000918 1299.2 1320.7
1291(33) 0.000918 1299.0 1320.5
1272(33) 0.000918 1298.9 1322.0
1288(33) 0.000918 1298.7 1325.9
1319(33) 0.000918 1298.5 1333.0
1359(34) 0.000865 1298.4 1344.9
1420(35) 0.000816 1298.2 1362.9
1399(34) 0.000865 1298.0 1388.4
1410(35) 0.000816 1297.8 1421.4
1402(34) 0.000865 1297.7 1460.0
1464(35) 0.000816 1297.5 1500.7
1535(36) 0.000772 1297. 1538.
1557(36) 0.000772 1297. 1564.
1559(36) 0.000772 1297. 1576.
1568(36) 0.000772 1297. 1575.
1552(36) 0.000772 1297. 1568.
1571(36) 0.000772 1296. 1561.
1571(36) 0.000772 1296. 1558.
1535(36) 0.000772 1296. 1558.
1503(36) 0.000772 1296. 1555.
1480(35) 0.000816 1295.8 1543.5
1491(36) 0.000772 1296. 1522.
1488(35) 0.000816 1295.5 1491.9
1425(35) 0.000816 1295.3 1459.7
1426(35) 0.000816 1295.1 1429.6
1450(35) 0.000816 1295.0 1404.3
1357(34) 0.000865 1294.8 1384.4
1479(35) 0.000816 1294.6 1369.3
1394(34) 0.000865 1294.5 1357.8
1372(34) 0.000865 1294.3 1349.0
1350(34) 0.000865 1294.1 1342.4
1338(34) 0.000865 1294.0 1338.0
1372(34) 0.000865 1293.8 1335.3
1351(34) 0.000865 1293.6 1334.3
1313(33) 0.000918 1293.5 1334.5
1342(34) 0.000865 1293.3 1335.9
1333(34) 0.000865 1293.1 1338.6
1330(34) 0.000865 1293.0 1342.7
1369(34) 0.000865 1292.8 1348.6
1307(33) 0.000918 1292.6 1355.9
1328(34) 0.000865 1292.5 1364.1
1343(34) 0.000865 1292.3 1372.3
1322(33) 0.000918 1292.1 1380.0
1334(34) 0.000865 1292.0 1387.7
1351(34) 0.000865 1291.8 1396.5
1411(35) 0.000816 1291.7 1407.2
1375(34) 0.000865 1291.5 1419.4
1405(34) 0.000865 1291.3 1430.7
1408(35) 0.000816 1291.2 1437.8
1376(34) 0.000865 1291.0 1437.4
1395(34) 0.000865 1290.8 1428.3
1391(34) 0.000865 1290.7 1412.6
1388(34) 0.000865 1290.5 1393.6
1368(34) 0.000865 1290.4 1374.7
1345(34) 0.000865 1290.2 1358.3
1344(34) 0.000865 1290.0 1345.6
1326(34) 0.000865 1289.9 1337.2
1351(34) 0.000865 1289.7 1332.9
1297(33) 0.000918 1289.6 1332.6
1304(33) 0.000918 1289.4 1336.3
1298(33) 0.000918 1289.2 1345.5
1345(34) 0.000865 1289.1 1362.1
1364(34) 0.000865 1288.9 1389.8
1420(35) 0.000816 1288.7 1432.7
1499(36) 0.000772 1289. 1495.
1644(37) 0.000730 1288. 1579.
1730(38) 0.000693 1288. 1684.
1797(39) 0.000657 1288. 1803.
1862(40) 0.000625 1288. 1923.
2002(41) 0.000595 1288. 2026.
2005(41) 0.000595 1288. 2089.
1996(41) 0.000595 1287. 2098.
1919(40) 0.000625 1287. 2052.
1887(40) 0.000625 1287. 1972.
1885(40) 0.000625 1287. 1878.
1784(39) 0.000657 1287. 1788.
1683(38) 0.000693 1287. 1711.
1564(36) 0.000772 1287. 1651.
1517(36) 0.000772 1286. 1605.
1549(36) 0.000772 1286. 1571.
1556(36) 0.000772 1286. 1547.
1479(35) 0.000816 1285.9 1533.1
1586(37) 0.000730 1286. 1526.
1566(36) 0.000772 1286. 1523.
1549(36) 0.000772 1285. 1518.
1538(36) 0.000772 1285. 1507.
1491(36) 0.000772 1285. 1488.
1478(35) 0.000816 1284.9 1462.0
1410(35) 0.000816 1284.8 1433.3
1423(35) 0.000816 1284.6 1405.9
1406(34) 0.000865 1284.4 1383.1
1358(34) 0.000865 1284.3 1366.9
1365(34) 0.000865 1284.1 1358.3
1341(34) 0.000865 1284.0 1357.4
1383(34) 0.000865 1283.8 1363.7
1410(35) 0.000816 1283.7 1375.5
1378(34) 0.000865 1283.5 1390.7
1501(36) 0.000772 1283. 1406.
1518(36) 0.000772 1283. 1419.
1483(35) 0.000816 1283.0 1425.0
1428(35) 0.000816 1282.9 1422.9
1495(36) 0.000772 1283. 1413.
1470(35) 0.000816 1282.5 1399.5
1399(34) 0.000865 1282.4 1384.3
1359(34) 0.000865 1282.2 1369.7
1364(34) 0.000865 1282.1 1357.3
1348(34) 0.000865 1281.9 1346.4
1351(34) 0.000865 1281.7 1336.9
1338(34) 0.000865 1281.6 1328.5
1311(33) 0.000918 1281.4 1321.1
1285(33) 0.000918 1281.3 1314.9
1328(34) 0.000865 1281.1 1309.7
1320(27) 0.001372 1280.9 1305.8
1275(33) 0.000918 1280.8 1303.1
1314(33) 0.000918 1280.6 1301.6
1283(33) 0.000918 1280.5 1301.2
1339(34) 0.000865 1280.3 1302.0
1317(33) 0.000918 1280.1 1304.2
1354(34) 0.000865 1280.0 1308.0
1321(33) 0.000918 1279.8 1313.9
1310(33) 0.000918 1279.7 1322.7
1351(34) 0.000865 1279.5 1334.8
1364(34) 0.000865 1279.3 1350.8
1362(34) 0.000865 1279.2 1370.4
1353(34) 0.000865 1279.0 1393.1
1365(34) 0.000865 1278.9 1416.8
1376(34) 0.000865 1278.7 1439.0
1466(35) 0.000816 1278.5 1456.4
1472(35) 0.000816 1278.4 1466.4
1413(34) 0.000865 1278.2 1468.8
1468(35) 0.000816 1278.1 1466.2
1448(35) 0.000816 1277.9 1461.9
1426(35) 0.000816 1277.7 1458.6
1463(35) 0.000816 1277.6 1457.5
1436(35) 0.000816 1277.4 1458.1
1454(35) 0.000816 1277.2 1459.6
1488(35) 0.000816 1277.1 1461.6
1460(35) 0.000816 1276.9 1465.0
1493(35) 0.000816 1276.8 1470.5
1523(36) 0.000772 1277. 1478.
1503(35) 0.000816 1276.4 1485.1
1506(36) 0.000772 1276. 1489.
1530(36) 0.000772 1276. 1487.
1509(36) 0.000772 1276. 1476.
1560(36) 0.000772 1276. 1460.
1445(35) 0.000816 1275.6 1440.4
1435(35) 0.000816 1275.5 1420.6
1393(34) 0.000865 1275.3 1403.0
1413(34) 0.000865 1275.1 1386.4
1388(34) 0.000865 1275.0 1372.5
1419(34) 0.000865 1274.8 1359.9
1387(34) 0.000865 1274.6 1348.7
1371(34) 0.000865 1274.5 1339.0
1293(33) 0.000918 1274.3 1331.0
1328(33) 0.000918 1274.1 1324.8
1304(33) 0.000918 1274.0 1320.2
1308(33) 0.000918 1273.8 1317.1
1312(33) 0.000918 1273.6 1315.3
1358(34) 0.000865 1273.5 1314.5
1345(34) 0.000865 1273.3 1314.7
1314(33) 0.000918 1273.1 1315.6
1347(34) 0.000865 1273.0 1316.9
1349(34) 0.000865 1272.8 1317.7
1293(33) 0.000918 1272.6 1317.7
1288(33) 0.000918 1272.5 1316.6
1313(33) 0.000918 1272.3 1314.6
1349(34) 0.000865 1272.1 1312.5
1351(34) 0.000865 1272.0 1311.0
1268(33) 0.000918 1271.8 1311.2
1287(33) 0.000918 1271.6 1313.5
1331(33) 0.000918 1271.4 1318.6
1352(34) 0.000865 1271.3 1327.2
1359(34) 0.000865 1271.1 1339.2
1347(34) 0.000865 1270.9 1354.6
1367(34) 0.000865 1270.8 1372.9
1387(34) 0.000865 1270.6 1393.3
1406(34) 0.000865 1270.4 1414.3
1406(34) 0.000865 1270.2 1435.2
1422(35) 0.000816 1270.1 1455.5
1437(35) 0.000816 1269.9 1476.2
1493(35) 0.000816 1269.7 1498.7
1473(35) 0.000816 1269.6 1524.3
1498(35) 0.000816 1269.4 1552.8
1512(36) 0.000772 1269. 1583.
1553(36) 0.000772 1269. 1612.
1623(37) 0.000730 1269. 1638.
1613(37) 0.000730 1269. 1663.
1659(37) 0.000730 1269. 1689.
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1754(38) 0.000693 1268. 1751.
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1756(38) 0.000693 1268. 1727.
1710(38) 0.000693 1267. 1685.
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1589(36) 0.000772 1267. 1569.
1558(36) 0.000772 1267. 1510.
1475(35) 0.000816 1266.7 1457.3
1470(35) 0.000816 1266.6 1413.0
1396(34) 0.000865 1266.4 1378.1
1357(34) 0.000865 1266.2 1351.7
1316(33) 0.000918 1266.0 1333.0
1338(33) 0.000918 1265.8 1319.9
1304(33) 0.000918 1265.7 1311.3
1331(33) 0.000918 1265.5 1306.0
1318(33) 0.000918 1265.3 1302.9
1296(33) 0.000918 1265.1 1302.0
1290(33) 0.000918 1264.9 1302.8
1298(33) 0.000918 1264.7 1305.7
1312(33) 0.000918 1264.6 1310.1
1303(33) 0.000918 1264.4 1316.5
1355(34) 0.000865 1264.2 1325.2
1279(45) 0.000494 1264. 1336.
1342(32) 0.000977 1263.8 1350.5
1370(33) 0.000918 1263.6 1367.1
1365(33) 0.000918 1263.4 1386.0
1420(33) 0.000918 1263.3 1405.7
1408(33) 0.000918 1263.1 1424.4
1374(33) 0.000918 1262.9 1439.5
1442(34) 0.000865 1262.7 1447.9
1469(34) 0.000865 1262.5 1448.4
1400(33) 0.000918 1262.3 1441.9
1447(34) 0.000865 1262.1 1431.7
1394(33) 0.000918 1261.9 1422.2
1406(33) 0.000918 1261.8 1417.9
1431(33) 0.000918 1261.6 1422.8
1435(34) 0.000865 1261.4 1439.7
1488(34) 0.000865 1261.2 1470.1
1497(34) 0.000865 1261.0 1513.7
1538(35) 0.000816 1260.8 1567.9
1606(35) 0.000816 1260.6 1627.8
1669(36) 0.000772 1260. 1686.
1757(37) 0.000730 1260. 1734.
1774(37) 0.000730 1260. 1763.
1766(37) 0.000730 1260. 1766.
1747(37) 0.000730 1260. 1744.
1717(37) 0.000730 1259. 1706.
1677(36) 0.000772 1259. 1659.
1554(35) 0.000816 1259.1 1611.6
1541(35) 0.000816 1258.9 1570.1
1575(35) 0.000816 1258.7 1537.6
1508(34) 0.000865 1258.5 1515.6
1523(35) 0.000816 1258.3 1504.2
1523(35) 0.000816 1258.1 1503.3
1506(34) 0.000865 1257.9 1511.2
1536(35) 0.000816 1257.7 1525.9
1558(35) 0.000816 1257.5 1544.4
1631(36) 0.000772 1257. 1563.
1593(35) 0.000816 1257.1 1580.6
1625(36) 0.000772 1257. 1596.
1599(35) 0.000816 1256.7 1609.5
1633(36) 0.000772 1256. 1622.
1624(36) 0.000772 1256. 1632.
1596(35) 0.000816 1256.1 1636.8
1594(35) 0.000816 1255.9 1632.1
1569(35) 0.000816 1255.7 1615.3
1539(35) 0.000816 1255.5 1587.3
1514(34) 0.000865 1255.2 1551.7
1467(34) 0.000865 1255.0 1513.2
1456(34) 0.000865 1254.8 1475.8
1390(33) 0.000918 1254.6 1442.5
1390(33) 0.000918 1254.4 1414.6
1417(33) 0.000918 1254.2 1392.6
1386(33) 0.000918 1254.0 1376.7
1348(32) 0.000977 1253.8 1365.8
1386(33) 0.000918 1253.6 1359.3
1435(34) 0.000865 1253.4 1355.9
1388(33) 0.000918 1253.2 1354.0
1346(32) 0.000977 1253.0 1352.3
1340(32) 0.000977 1252.7 1349.8
1353(33) 0.000918 1252.5 1346.1
1365(33) 0.000918 1252.3 1341.9
1312(32) 0.000977 1252.1 1337.4
1320(32) 0.000977 1251.9 1332.8
1307(32) 0.000977 1251.7 1328.0
1356(33) 0.000918 1251.5 1323.0
1284(32) 0.000977 1251.3 1317.5
1270(32) 0.000977 1251.0 1311.5
1323(32) 0.000977 1250.8 1305.6
1258(31) 0.001041 1250.6 1300.2
1315(32) 0.000977 1250.4 1295.7
1321(32) 0.000977 1250.2 1292.4
1305(32) 0.000977 1250.0 1290.7
1310(32) 0.000977 1249.7 1290.7
1333(32) 0.000977 1249.5 1292.9
1291(32) 0.000977 1249.3 1297.4
1306(32) 0.000977 1249.1 1304.5
1367(33) 0.000918 1248.9 1314.8
1329(32) 0.000977 1248.6 1328.5
1347(32) 0.000977 1248.4 1346.2
1401(33) 0.000918 1248.2 1368.1
1459(34) 0.000865 1248.0 1394.5
1495(34) 0.000865 1247.7 1425.2
1467(34) 0.000865 1247.5 1459.5
1531(35) 0.000816 1247.3 1496.3
1629(36) 0.000772 1247. 1534.
1693(36) 0.000772 1247. 1570.
1720(37) 0.000730 1247. 1603.
1626(36) 0.000772 1246. 1634.
1729(37) 0.000730 1246. 1664.
1729(37) 0.000730 1246. 1691.
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1650(36) 0.000772 1245. 1730.
1687(36) 0.000772 1245. 1733.
1665(36) 0.000772 1245. 1723.
1726(37) 0.000730 1245. 1701.
1708(37) 0.000730 1245. 1671.
1624(36) 0.000772 1244. 1636.
1603(35) 0.000816 1244.1 1600.7
1573(35) 0.000816 1243.9 1565.2
1569(35) 0.000816 1243.6 1529.7
1515(34) 0.000865 1243.4 1494.3
1502(34) 0.000865 1243.2 1460.2
1463(34) 0.000865 1242.9 1428.7
1401(33) 0.000918 1242.7 1401.4
1440(34) 0.000865 1242.5 1379.4
1384(33) 0.000918 1242.2 1363.9
1441(34) 0.000865 1242.0 1354.3
1380(33) 0.000918 1241.8 1350.7
1392(33) 0.000918 1241.5 1351.7
1338(32) 0.000977 1241.3 1357.1
1348(32) 0.000977 1241.0 1364.4
1345(32) 0.000977 1240.8 1371.6
1396(33) 0.000918 1240.6 1376.3
1384(33) 0.000918 1240.3 1376.8
1361(33) 0.000918 1240.1 1372.1
1326(32) 0.000977 1239.8 1362.8
1332(32) 0.000977 1239.6 1350.5
1334(32) 0.000977 1239.4 1336.8
1336(32) 0.000977 1239.1 1323.5
1289(32) 0.000977 1238.9 1311.4
1326(32) 0.000977 1238.6 1301.5
1253(31) 0.001041 1238.4 1294.4
1287(32) 0.000977 1238.1 1290.4
1268(31) 0.001041 1237.9 1290.1
1253(31) 0.001041 1237.6 1293.6
1317(32) 0.000977 1237.4 1301.2
1300(32) 0.000977 1237.2 1312.9
1279(32) 0.000977 1236.9 1328.7
1333(32) 0.000977 1236.7 1348.4
1384(33) 0.000918 1236.4 1371.3
1428(33) 0.000918 1236.2 1396.1
1445(34) 0.000865 1235.9 1421.2
1472(34) 0.000865 1235.7 1444.4
1492(34) 0.000865 1235.4 1463.2
1496(34) 0.000865 1235.2 1476.1
1511(34) 0.000865 1234.9 1482.8
1534(35) 0.000816 1234.6 1485.0
1505(34) 0.000865 1234.4 1485.2
1528(35) 0.000816 1234.1 1485.9
1523(35) 0.000816 1233.9 1489.0
1471(34) 0.000865 1233.6 1495.3
1450(34) 0.000865 1233.4 1505.0
1519(34) 0.000865 1233.1 1518.1
1582(35) 0.000816 1232.9 1533.9
1549(35) 0.000816 1232.6 1551.2
1545(35) 0.000816 1232.4 1567.9
1431(33) 0.000918 1232.1 1580.8
1534(35) 0.000816 1231.8 1586.3
1544(35) 0.000816 1231.6 1582.1
1565(35) 0.000816 1231.3 1568.5
1460(34) 0.000865 1231.1 1548.5
1466(34) 0.000865 1230.8 1526.7
1462(34) 0.000865 1230.5 1507.7
1500(34) 0.000865 1230.3 1495.7
1499(34) 0.000865 1230.0 1493.3
1461(34) 0.000865 1229.7 1501.9
1558(35) 0.000816 1229.5 1521.1
1553(35) 0.000816 1229.2 1549.2
1576(35) 0.000816 1229.0 1582.7
1579(35) 0.000816 1228.7 1616.7
1717(37) 0.000730 1228. 1646.
1692(36) 0.000772 1228. 1663.
1691(36) 0.000772 1228. 1666.
1671(36) 0.000772 1228. 1653.
1702(36) 0.000772 1227. 1627.
1639(36) 0.000772 1227. 1594.
1594(35) 0.000816 1226.8 1556.6
1618(36) 0.000772 1227. 1519.
1437(34) 0.000865 1226.3 1484.2
1471(34) 0.000865 1226.0 1452.5
1395(33) 0.000918 1225.8 1425.0
1371(33) 0.000918 1225.5 1402.0
1359(33) 0.000918 1225.2 1383.4
1401(33) 0.000918 1224.9 1368.6
1333(32) 0.000977 1224.7 1356.6
1292(32) 0.000977 1224.4 1346.2
1321(32) 0.000977 1224.1 1336.7
1350(32) 0.000977 1223.8 1327.9
1393(33) 0.000918 1223.6 1320.2
1313(32) 0.000977 1223.3 1314.1
1357(33) 0.000918 1223.0 1310.2
1330(32) 0.000977 1222.7 1309.3
1224(31) 0.001041 1222.5 1311.3
1355(33) 0.000918 1222.2 1316.3
1262(31) 0.001041 1221.9 1324.1
1313(32) 0.000977 1221.6 1334.0
1349(32) 0.000977 1221.4 1344.8
1311(32) 0.000977 1221.1 1355.2
1348(32) 0.000977 1220.8 1363.8
1376(33) 0.000918 1220.5 1369.3
1414(33) 0.000918 1220.3 1371.1
1379(33) 0.000918 1220.0 1369.7
1436(33) 0.000918 1219.7 1366.6
1370(33) 0.000918 1219.4 1363.6
1360(33) 0.000918 1219.1 1362.6
1405(33) 0.000918 1218.8 1365.0
1427(33) 0.000918 1218.6 1372.1
1336(32) 0.000977 1218.3 1384.7
1443(34) 0.000865 1218.0 1403.4
1422(33) 0.000918 1217.7 1427.9
1420(33) 0.000918 1217.4 1457.9
1419(33) 0.000918 1217.2 1492.2
1507(36) 0.000772 1217. 1529.
1524(36) 0.000772 1217. 1567.
1588(37) 0.000730 1216. 1604.
1683(38) 0.000693 1216. 1640.
1716(38) 0.000693 1216. 1673.
1744(38) 0.000693 1215. 1701.
1775(39) 0.000657 1215. 1723.
1784(39) 0.000657 1215. 1734.
1760(38) 0.000693 1215. 1731.
1768(39) 0.000657 1214. 1715.
1766(39) 0.000657 1214. 1686.
1712(38) 0.000693 1214. 1649.
1637(37) 0.000730 1213. 1609.
1530(36) 0.000772 1213. 1571.
1539(36) 0.000772 1213. 1538.
1500(35) 0.000816 1212.6 1512.3
1485(35) 0.000816 1212.3 1494.0
1469(35) 0.000816 1212.0 1483.3
1423(35) 0.000816 1211.7 1479.0
1470(35) 0.000816 1211.4 1479.2
1462(35) 0.000816 1211.1 1480.9
1383(34) 0.000865 1210.8 1481.2
1436(35) 0.000816 1210.5 1477.3
1419(35) 0.000816 1210.2 1467.9
1436(35) 0.000816 1209.9 1453.2
1485(35) 0.000816 1209.6 1434.4
1453(35) 0.000816 1209.3 1413.2
1410(34) 0.000865 1209.0 1391.2
1384(34) 0.000865 1208.7 1369.5
1357(34) 0.000865 1208.5 1349.0
1347(34) 0.000865 1208.2 1330.3
1325(33) 0.000918 1207.9 1313.8
1278(33) 0.000918 1207.6 1300.0
1308(33) 0.000918 1207.3 1289.1
1318(33) 0.000918 1207.0 1281.3
1283(33) 0.000918 1206.7 1276.4
1272(33) 0.000918 1206.4 1274.3
1234(32) 0.000977 1206.1 1274.9
1334(33) 0.000918 1205.8 1278.0
1240(32) 0.000977 1205.5 1283.1
1252(32) 0.000977 1205.2 1289.7
1228(32) 0.000977 1204.9 1297.6
1284(33) 0.000918 1204.6 1306.2
1293(33) 0.000918 1204.3 1315.0
1321(33) 0.000918 1204.0 1323.8
1266(33) 0.000918 1203.7 1332.5
1301(33) 0.000918 1203.4 1341.3
1280(33) 0.000918 1203.1 1349.5
1275(33) 0.000918 1202.8 1357.0
1301(33) 0.000918 1202.5 1363.5
1313(33) 0.000918 1202.2 1368.7
1320(33) 0.000918 1201.9 1372.6
1357(34) 0.000865 1201.6 1376.1
1379(34) 0.000865 1201.3 1380.1
1364(34) 0.000865 1201.0 1385.0
1392(34) 0.000865 1200.7 1391.4
1432(35) 0.000816 1200.4 1399.5
1408(34) 0.000865 1200.1 1409.2
1448(35) 0.000816 1199.8 1420.2
1396(34) 0.000865 1199.5 1432.3
1477(35) 0.000816 1199.2 1445.2
1485(35) 0.000816 1198.9 1457.8
1534(36) 0.000772 1199. 1469.
1482(35) 0.000816 1198.2 1477.1
1522(36) 0.000772 1198. 1481.
1514(36) 0.000772 1198. 1481.
1530(36) 0.000772 1197. 1478.
1526(36) 0.000772 1197. 1472.
1460(35) 0.000816 1196.7 1465.5
1431(35) 0.000816 1196.4 1458.5
1458(35) 0.000816 1196.1 1451.6
1439(35) 0.000816 1195.8 1445.0
1423(35) 0.000816 1195.5 1438.7
1444(35) 0.000816 1195.2 1433.1
1350(34) 0.000865 1194.9 1428.6
1419(35) 0.000816 1194.6 1424.9
1402(34) 0.000865 1194.3 1421.4
1456(35) 0.000816 1194.0 1417.5
1420(35) 0.000816 1193.7 1412.4
1416(34) 0.000865 1193.4 1405.7
1405(34) 0.000865 1193.0 1397.7
1377(34) 0.000865 1192.7 1388.7
1351(34) 0.000865 1192.4 1378.8
1329(33) 0.000918 1192.1 1368.0
1359(34) 0.000865 1191.8 1356.0
1283(33) 0.000918 1191.5 1342.8
1379(34) 0.000865 1191.2 1328.4
1338(34) 0.000865 1190.9 1313.5
1292(33) 0.000918 1190.6 1298.7
1283(33) 0.000918 1190.3 1284.6
1296(33) 0.000918 1190.0 1271.9
1235(32) 0.000977 1189.7 1261.0
1230(32) 0.000977 1189.3 1252.0
1219(32) 0.000977 1189.0 1245.1
1248(32) 0.000977 1188.7 1240.5
1247(32) 0.000977 1188.4 1238.3
1212(32) 0.000977 1188.1 1238.2
1258(32) 0.000977 1187.8 1240.3
1249(32) 0.000977 1187.5 1244.9
1234(32) 0.000977 1187.2 1251.5
1246(33) 0.000918 1186.9 1260.4
1287(33) 0.000918 1186.6 1271.4
1274(33) 0.000918 1186.3 1284.6
1244(33) 0.000918 1186.0 1299.8
1271(33) 0.000918 1185.6 1316.6
1347(34) 0.000865 1185.3 1334.7
1338(34) 0.000865 1185.0 1353.3
1349(34) 0.000865 1184.7 1372.3
1372(34) 0.000865 1184.4 1390.9
1366(34) 0.000865 1184.1 1408.6
1403(35) 0.000816 1183.8 1424.4
1410(35) 0.000816 1183.5 1437.0
1397(35) 0.000816 1183.2 1445.2
1512(36) 0.000772 1183. 1448.
1496(36) 0.000772 1183. 1445.
1455(35) 0.000816 1182.2 1438.1
1379(34) 0.000865 1181.9 1427.4
1431(35) 0.000816 1181.6 1414.1
1401(35) 0.000816 1181.3 1399.2
1343(34) 0.000865 1181.0 1383.0
1351(34) 0.000865 1180.7 1366.3
1370(34) 0.000865 1180.4 1349.5
1319(34) 0.000865 1180.1 1333.5
1348(34) 0.000865 1179.8 1319.4
1346(34) 0.000865 1179.5 1307.7
1340(34) 0.000865 1179.1 1299.1
1296(33) 0.000918 1178.8 1293.6
1284(33) 0.000918 1178.5 1291.6
1281(33) 0.000918 1178.2 1292.3
1337(34) 0.000865 1177.9 1295.4
1280(33) 0.000918 1177.6 1300.2
1310(33) 0.000918 1177.3 1305.8
1348(34) 0.000865 1177.0 1311.1
1375(34) 0.000865 1176.7 1315.1
1329(34) 0.000865 1176.4 1317.3
1316(34) 0.000865 1176.1 1317.3
1388(34) 0.000865 1175.8 1315.4
1342(34) 0.000865 1175.4 1312.0
1352(34) 0.000865 1175.1 1307.7
1337(34) 0.000865 1174.8 1302.9
1344(34) 0.000865 1174.5 1298.0
1324(34) 0.000865 1174.2 1293.9
1264(33) 0.000918 1173.9 1290.7
1313(34) 0.000865 1173.6 1289.3
1264(33) 0.000918 1173.3 1290.5
1233(32) 0.000977 1173.0 1295.2
1250(33) 0.000918 1172.7 1303.8
1277(33) 0.000918 1172.4 1316.8
1287(33) 0.000918 1172.1 1334.7
1286(33) 0.000918 1171.8 1357.0
1301(33) 0.000918 1171.5 1383.6
1316(34) 0.000865 1171.2 1414.1
1390(34) 0.000865 1170.8 1447.3
1429(35) 0.000816 1170.5 1482.1
1515(36) 0.000772 1170. 1517.
1543(36) 0.000772 1170. 1551.
1529(36) 0.000772 1170. 1583.
1626(37) 0.000730 1169. 1612.
1630(37) 0.000730 1169. 1639.
1613(37) 0.000730 1169. 1661.
1634(37) 0.000730 1168. 1677.
1702(38) 0.000693 1168. 1686.
1707(38) 0.000693 1168. 1687.
1710(38) 0.000693 1167. 1680.
1660(38) 0.000693 1167. 1666.
1685(38) 0.000693 1167. 1646.
1613(37) 0.000730 1167. 1623.
1588(37) 0.000730 1166. 1597.
1640(37) 0.000730 1166. 1569.
1621(37) 0.000730 1166. 1540.
1530(36) 0.000772 1165. 1510.
1466(35) 0.000816 1165.1 1480.6
1452(35) 0.000816 1164.8 1452.9
1467(35) 0.000816 1164.5 1427.9
1378(34) 0.000865 1164.2 1406.2
1402(35) 0.000816 1163.9 1388.0
1391(34) 0.000865 1163.6 1373.3
1319(34) 0.000865 1163.3 1362.0
1387(34) 0.000865 1163.0 1353.9
1374(34) 0.000865 1162.7 1348.5
1317(34) 0.000865 1162.4 1345.3
1406(35) 0.000816 1162.1 1343.7
1328(34) 0.000865 1161.8 1342.8
1347(34) 0.000865 1161.5 1342.2
1306(33) 0.000918 1161.2 1341.3
1320(34) 0.000865 1160.9 1340.1
1355(34) 0.000865 1160.6 1338.5
1395(35) 0.000816 1160.3 1336.7
1361(34) 0.000865 1160.0 1334.4
1274(33) 0.000918 1159.7 1331.6
1332(34) 0.000865 1159.4 1328.0
1329(34) 0.000865 1159.1 1323.6
1334(34) 0.000865 1158.8 1318.5
1323(34) 0.000865 1158.5 1312.9
1360(34) 0.000865 1158.3 1307.0
1329(34) 0.000865 1158.0 1300.8
1351(34) 0.000865 1157.7 1294.3
1264(33) 0.000918 1157.4 1287.4
1263(33) 0.000918 1157.1 1280.4
1296(33) 0.000918 1156.8 1273.7
1276(32) 0.000977 1156.5 1267.7
1268(32) 0.000977 1156.2 1263.0
1256(31) 0.001041 1155.9 1259.9
1284(32) 0.000977 1155.6 1258.7
1271(32) 0.000977 1155.3 1259.5
1265(31) 0.001041 1155.1 1262.4
1276(32) 0.000977 1154.8 1267.1
1308(32) 0.000977 1154.5 1273.4
1297(32) 0.000977 1154.2 1280.8
1293(32) 0.000977 1153.9 1289.1
1307(32) 0.000977 1153.6 1297.1
1317(32) 0.000977 1153.3 1304.7
1334(32) 0.000977 1153.1 1311.6
1374(33) 0.000918 1152.8 1318.0
1383(33) 0.000918 1152.5 1324.1
1382(33) 0.000918 1152.2 1330.1
1410(33) 0.000918 1151.9 1336.4
1402(33) 0.000918 1151.6 1343.0
1369(33) 0.000918 1151.4 1349.9
1443(34) 0.000865 1151.1 1357.2
1408(33) 0.000918 1150.8 1364.8
1488(34) 0.000865 1150.5 1372.7
1448(34) 0.000865 1150.2 1380.8
1404(33) 0.000918 1150.0 1388.6
1412(33) 0.000918 1149.7 1395.8
1486(34) 0.000865 1149.4 1401.5
1483(34) 0.000865 1149.1 1405.5
1476(34) 0.000865 1148.8 1407.9
1404(33) 0.000918 1148.6 1408.8
1409(33) 0.000918 1148.3 1408.6
1389(33) 0.000918 1148.0 1407.3
1453(34) 0.000865 1147.7 1405.0
1426(33) 0.000918 1147.5 1401.6
1485(34) 0.000865 1147.2 1397.3
1400(33) 0.000918 1146.9 1392.2
1402(33) 0.000918 1146.6 1386.8
1408(33) 0.000918 1146.4 1381.5
1387(33) 0.000918 1146.1 1376.7
1397(33) 0.000918 1145.8 1372.4
1427(33) 0.000918 1145.6 1368.8
1321(32) 0.000977 1145.3 1365.7
1374(33) 0.000918 1145.0 1363.3
1463(34) 0.000865 1144.8 1361.5
1382(33) 0.000918 1144.5 1360.6
1388(33) 0.000918 1144.2 1360.3
1399(33) 0.000918 1144.0 1360.4
1397(33) 0.000918 1143.7 1360.6
1387(33) 0.000918 1143.4 1360.6
1443(34) 0.000865 1143.2 1360.2
1410(33) 0.000918 1142.9 1359.3
1354(33) 0.000918 1142.6 1358.0
1342(32) 0.000977 1142.4 1356.3
1316(32) 0.000977 1142.1 1354.1
1306(32) 0.000977 1141.9 1351.6
1266(31) 0.001041 1141.6 1349.0
1307(32) 0.000977 1141.3 1346.4
1342(32) 0.000977 1141.1 1344.9
1369(33) 0.000918 1140.8 1345.1
1317(32) 0.000977 1140.6 1348.1
1341(32) 0.000977 1140.3 1354.6
1370(33) 0.000918 1140.1 1365.0
1375(33) 0.000918 1139.8 1379.6
1400(33) 0.000918 1139.5 1398.0
1452(34) 0.000865 1139.3 1419.8
1468(34) 0.000865 1139.0 1444.0
1453(34) 0.000865 1138.8 1469.3
1458(34) 0.000865 1138.5 1494.0
1506(34) 0.000865 1138.3 1516.6
1521(35) 0.000816 1138.0 1535.6
1527(35) 0.000816 1137.8 1550.1
1556(35) 0.000816 1137.5 1559.6
1548(35) 0.000816 1137.3 1564.6
1619(36) 0.000772 1137. 1565.
1531(35) 0.000816 1136.8 1561.6
1513(34) 0.000865 1136.5 1554.3
1474(34) 0.000865 1136.3 1543.3
1511(34) 0.000865 1136.1 1529.0
1466(34) 0.000865 1135.8 1512.0
1421(33) 0.000918 1135.6 1493.3
1429(33) 0.000918 1135.3 1473.9
1447(34) 0.000865 1135.1 1454.5
1415(33) 0.000918 1134.9 1435.7
1391(33) 0.000918 1134.6 1417.9
1371(33) 0.000918 1134.4 1401.3
1348(33) 0.000918 1134.1 1386.2
1332(32) 0.000977 1133.9 1372.7
1378(33) 0.000918 1133.7 1361.0
1364(33) 0.000918 1133.4 1351.1
1348(33) 0.000918 1133.2 1342.8
1342(32) 0.000977 1133.0 1335.9
1306(32) 0.000977 1132.7 1330.1
1299(32) 0.000977 1132.5 1325.0
1324(32) 0.000977 1132.3 1320.3
1310(32) 0.000977 1132.0 1315.8
1287(32) 0.000977 1131.8 1311.1
1333(32) 0.000977 1131.6 1306.0
1224(31) 0.001041 1131.4 1300.0
1304(32) 0.000977 1131.1 1293.0
1233(31) 0.001041 1130.9 1284.9
1257(43) 0.000541 1131. 1276.
1269(31) 0.001041 1130.5 1266.1
1277(31) 0.001041 1130.2 1256.3
1228(31) 0.001041 1130.0 1246.8
1214(31) 0.001041 1129.8 1237.7
1187(30) 0.001111 1129.6 1229.4
1222(31) 0.001041 1129.3 1222.0
1191(30) 0.001111 1129.1 1215.7
1200(30) 0.001111 1128.9 1210.3
1172(30) 0.001111 1128.7 1205.9
1217(31) 0.001041 1128.5 1202.4
1223(31) 0.001041 1128.3 1199.5
1203(30) 0.001111 1128.0 1197.2
1179(30) 0.001111 1127.8 1195.3
1158(30) 0.001111 1127.6 1194.0
1115(29) 0.001189 1127.4 1193.2
1167(30) 0.001111 1127.2 1193.1
1180(30) 0.001111 1127.0 1193.8
1216(31) 0.001041 1126.8 1195.6
1212(31) 0.001041 1126.6 1198.5
1211(31) 0.001041 1126.4 1202.6
1207(31) 0.001041 1126.2 1208.1
1204(30) 0.001111 1126.0 1215.0
1201(30) 0.001111 1125.8 1223.3
1247(31) 0.001041 1125.6 1232.8
1254(31) 0.001041 1125.4 1243.6
1250(31) 0.001041 1125.2 1255.4
1235(31) 0.001041 1125.0 1268.1
1205(30) 0.001111 1124.8 1281.4
1241(31) 0.001041 1124.6 1295.4
1284(31) 0.001041 1124.4 1309.8
1309(32) 0.000977 1124.2 1324.6
1308(32) 0.000977 1124.0 1339.4
1313(32) 0.000977 1123.8 1354.3
1369(33) 0.000918 1123.6 1368.9
1379(33) 0.000918 1123.4 1383.2
1385(33) 0.000918 1123.2 1397.3
1396(33) 0.000918 1123.0 1411.6
1411(33) 0.000918 1122.8 1426.2
1416(33) 0.000918 1122.6 1441.2
1460(34) 0.000865 1122.4 1456.3
1452(34) 0.000865 1122.3 1471.3
1469(34) 0.000865 1122.1 1485.8
1524(34) 0.000865 1121.9 1499.2
1543(35) 0.000816 1121.7 1511.0
1567(35) 0.000816 1121.5 1520.5
1567(35) 0.000816 1121.3 1527.1
1503(34) 0.000865 1121.2 1529.7
1523(34) 0.000865 1121.0 1527.7
1531(34) 0.000865 1120.8 1520.6
1530(34) 0.000865 1120.6 1508.6
1506(34) 0.000865 1120.5 1492.4
1513(34) 0.000865 1120.3 1473.3
1482(34) 0.000865 1120.1 1452.6
1485(34) 0.000865 1119.9 1431.8
1433(33) 0.000918 1119.8 1412.0
1371(33) 0.000918 1119.6 1394.0
1349(32) 0.000977 1119.4 1378.3
1349(32) 0.000977 1119.3 1365.2
1356(32) 0.000977 1119.1 1354.4
1339(32) 0.000977 1118.9 1345.8
1356(32) 0.000977 1118.8 1338.4
1311(32) 0.000977 1118.6 1331.4
1288(32) 0.000977 1118.4 1324.3
1266(31) 0.001041 1118.3 1316.4
1308(32) 0.000977 1118.1 1307.3
1279(31) 0.001041 1117.9 1297.0
1262(31) 0.001041 1117.8 1285.9
1207(31) 0.001041 1117.6 1274.1
1221(31) 0.001041 1117.5 1261.9
1200(30) 0.001111 1117.3 1249.7
1189(30) 0.001111 1117.2 1237.9
1218(31) 0.001041 1117.0 1226.7
1263(31) 0.001041 1116.9 1216.6
1208(31) 0.001041 1116.7 1207.7
1191(30) 0.001111 1116.6 1200.4
1195(30) 0.001111 1116.4 1194.6
1216(31) 0.001041 1116.3 1190.6
1169(30) 0.001111 1116.1 1188.6
1178(30) 0.001111 1116.0 1188.5
1217(31) 0.001041 1115.8 1190.5
1248(31) 0.001041 1115.7 1194.6
1199(30) 0.001111 1115.5 1200.6
1197(30) 0.001111 1115.4 1208.7
1219(31) 0.001041 1115.3 1218.6
1233(31) 0.001041 1115.1 1230.1
1266(31) 0.001041 1115.0 1243.2
1292(32) 0.000977 1114.8 1257.4
1270(31) 0.001041 1114.7 1272.5
1293(32) 0.000977 1114.6 1287.9
1331(32) 0.000977 1114.4 1303.1
1308(32) 0.000977 1114.3 1317.7
1321(32) 0.000977 1114.2 1330.9
1357(32) 0.000977 1114.0 1342.3
1332(32) 0.000977 1113.9 1351.7
1361(32) 0.000977 1113.8 1358.8
1339(32) 0.000977 1113.7 1363.9
1329(32) 0.000977 1113.5 1367.0
1418(33) 0.000918 1113.4 1368.5
1363(32) 0.000977 1113.3 1368.3
1384(33) 0.000918 1113.2 1366.8
1367(32) 0.000977 1113.0 1364.0
1330(32) 0.000977 1112.9 1360.4
1381(33) 0.000918 1112.8 1356.0
1345(32) 0.000977 1112.7 1351.5
1304(32) 0.000977 1112.6 1347.0
1318(32) 0.000977 1112.5 1342.9
1301(32) 0.000977 1112.3 1339.3
1299(32) 0.000977 1112.2 1336.4
1326(32) 0.000977 1112.1 1334.1
1319(32) 0.000977 1112.0 1332.6
1313(32) 0.000977 1111.9 1331.8
1316(32) 0.000977 1111.8 1331.7
1336(32) 0.000977 1111.7 1332.1
1344(32) 0.000977 1111.6 1332.9
1346(32) 0.000977 1111.5 1333.8
1335(32) 0.000977 1111.4 1334.5
1351(32) 0.000977 1111.3 1334.7
1343(32) 0.000977 1111.2 1334.2
1330(32) 0.000977 1111.1 1332.9
1308(32) 0.000977 1111.0 1330.5
1325(32) 0.000977 1110.9 1326.7
1294(31) 0.001041 1110.8 1321.4
1289(31) 0.001041 1110.7 1314.3
1284(31) 0.001041 1110.6 1305.6
1273(31) 0.001041 1110.5 1295.2
1316(32) 0.000977 1110.4 1283.7
1320(32) 0.000977 1110.3 1271.3
1284(31) 0.001041 1110.2 1258.5
1262(31) 0.001041 1110.1 1245.7
1235(31) 0.001041 1110.0 1233.2
1219(31) 0.001041 1109.9 1221.3
1205(30) 0.001111 1109.9 1210.2
1243(31) 0.001041 1109.8 1200.2
1221(31) 0.001041 1109.7 1191.4
1207(30) 0.001111 1109.6 1183.9
1166(30) 0.001111 1109.5 1177.8
1150(30) 0.001111 1109.4 1173.2
1169(30) 0.001111 1109.4 1170.1
1189(30) 0.001111 1109.3 1168.5
1201(30) 0.001111 1109.2 1168.4
1219(31) 0.001041 1109.1 1169.8
1212(30) 0.001111 1109.1 1172.7
1206(30) 0.001111 1109.0 1176.9
1169(30) 0.001111 1108.9 1182.4
1181(30) 0.001111 1108.8 1189.0
1197(30) 0.001111 1108.8 1196.6
1226(31) 0.001041 1108.7 1205.0
1250(31) 0.001041 1108.6 1213.9
1266(31) 0.001041 1108.6 1223.2
1264(31) 0.001041 1108.5 1232.6
1265(31) 0.001041 1108.4 1241.5
1290(31) 0.001041 1108.4 1249.9
1282(31) 0.001041 1108.3 1257.3
1255(31) 0.001041 1108.3 1263.7
1259(31) 0.001041 1108.2 1268.8
1366(32) 0.000977 1108.1 1272.7
1368(32) 0.000977 1108.1 1275.4
1321(32) 0.000977 1108.0 1277.1
1322(32) 0.000977 1108.0 1277.7
1320(32) 0.000977 1107.9 1277.3
1292(31) 0.001041 1107.9 1276.0
1290(31) 0.001041 1107.8 1274.0
1306(32) 0.000977 1107.8 1271.3
1315(32) 0.000977 1107.7 1268.3
1290(31) 0.001041 1107.7 1265.1
1283(31) 0.001041 1107.6 1261.9
1304(32) 0.000977 1107.6 1258.9
1260(31) 0.001041 1107.5 1256.1
1230(31) 0.001041 1107.5 1253.5
1227(31) 0.001041 1107.4 1251.3
1240(31) 0.001041 1107.4 1249.6
1251(31) 0.001041 1107.4 1248.0
1259(31) 0.001041 1107.3 1246.8
1248(31) 0.001041 1107.3 1245.8
1266(31) 0.001041 1107.3 1244.9
1216(30) 0.001111 1107.2 1243.9
1187(30) 0.001111 1107.2 1242.8
1208(30) 0.001111 1107.2 1241.5
1228(31) 0.001041 1107.1 1239.8
1223(31) 0.001041 1107.1 1237.7
1203(30) 0.001111 1107.1 1235.1
1165(30) 0.001111 1107.0 1232.0
1176(30) 0.001111 1107.0 1228.2
1148(30) 0.001111 1107.0 1223.7
1180(30) 0.001111 1106.9 1218.7
1213(30) 0.001111 1106.9 1213.1
1220(31) 0.001041 1106.9 1207.1
1167(30) 0.001111 1106.9 1201.0
1131(29) 0.001189 1106.9 1194.8
1155(30) 0.001111 1106.8 1188.7
1149(30) 0.001111 1106.8 1183.0
1152(30) 0.001111 1106.8 1177.6
1169(30) 0.001111 1106.8 1172.8
1170(30) 0.001111 1106.8 1168.7
1202(30) 0.001111 1106.8 1165.3
1117(29) 0.001189 1106.7 1162.8
1128(29) 0.001189 1106.7 1161.3
1116(29) 0.001189 1106.7 1160.7
1109(29) 0.001189 1106.7 1161.3
1161(30) 0.001111 1106.7 1163.0
1178(31) 0.001041 1106.7 1166.0
1138(30) 0.001111 1106.7 1170.3
1134(30) 0.001111 1106.7 1176.1
1185(31) 0.001041 1106.7 1183.3
1165(31) 0.001041 1106.7 1192.0
1201(31) 0.001041 1106.7 1202.4
1234(32) 0.000977 1106.7 1214.4
1216(31) 0.001041 1106.7 1228.0
1197(31) 0.001041 1106.7 1243.2
1250(32) 0.000977 1106.7 1259.8
1289(32) 0.000977 1106.7 1277.8
1328(33) 0.000918 1106.7 1296.8
1370(33) 0.000918 1106.7 1316.7
1330(33) 0.000918 1106.7 1337.1
1385(33) 0.000918 1106.7 1357.8
1441(34) 0.000865 1106.7 1378.3
1431(34) 0.000865 1106.7 1398.5
1423(34) 0.000865 1106.7 1417.8
1497(35) 0.000816 1106.7 1436.0
1442(34) 0.000865 1106.7 1452.7
1499(35) 0.000816 1106.8 1467.4
1463(34) 0.000865 1106.8 1479.8
1476(35) 0.000816 1106.8 1489.6
1487(35) 0.000816 1106.8 1497.0
1523(35) 0.000816 1106.8 1501.8
1566(36) 0.000772 1107. 1504.
1556(35) 0.000816 1106.8 1505.1
1568(36) 0.000772 1107. 1504.
1516(35) 0.000816 1106.9 1501.3
1510(35) 0.000816 1106.9 1497.3
1479(35) 0.000816 1106.9 1492.0
1483(35) 0.000816 1107.0 1485.6
1522(35) 0.000816 1107.0 1478.3
1526(35) 0.000816 1107.0 1470.3
1439(34) 0.000865 1107.0 1461.6
1449(34) 0.000865 1107.1 1452.3
1460(34) 0.000865 1107.1 1442.4
1447(34) 0.000865 1107.1 1431.9
1388(33) 0.000918 1107.2 1420.7
1442(34) 0.000865 1107.2 1409.0
1492(35) 0.000816 1107.2 1397.0
1398(34) 0.000865 1107.3 1384.7
1360(33) 0.000918 1107.3 1372.6
1351(33) 0.000918 1107.3 1360.6
1356(33) 0.000918 1107.4 1348.7
1376(33) 0.000918 1107.4 1337.3
1333(33) 0.000918 1107.4 1326.2
1312(33) 0.000918 1107.5 1315.6
1303(32) 0.000977 1107.5 1305.5
1264(32) 0.000977 1107.6 1296.0
1231(31) 0.001041 1107.6 1287.1
1270(32) 0.000977 1107.6 1279.0
1303(32) 0.000977 1107.7 1271.3
1262(32) 0.000977 1107.7 1264.2
1235(32) 0.000977 1107.8 1257.8
1228(31) 0.001041 1107.8 1252.3
1252(32) 0.000977 1107.9 1247.7
1267(32) 0.000977 1107.9 1244.2
1248(32) 0.000977 1108.0 1242.0
1211(31) 0.001041 1108.0 1241.2
1270(32) 0.000977 1108.1 1242.0
1212(31) 0.001041 1108.1 1244.5
1226(31) 0.001041 1108.2 1248.7
1208(31) 0.001041 1108.2 1254.8
1273(32) 0.000977 1108.3 1262.5
1329(33) 0.000918 1108.3 1271.8
1332(33) 0.000918 1108.4 1282.5
1318(33) 0.000918 1108.4 1294.3
1259(32) 0.000977 1108.5 1307.0
1302(32) 0.000977 1108.6 1320.1
1293(32) 0.000977 1108.6 1333.4
1318(33) 0.000918 1108.7 1346.2
1324(33) 0.000918 1108.7 1358.3
1307(32) 0.000977 1108.8 1369.1
1341(33) 0.000918 1108.9 1377.9
1344(33) 0.000918 1108.9 1384.5
1390(33) 0.000918 1109.0 1388.4
1343(33) 0.000918 1109.1 1389.2
1314(33) 0.000918 1109.1 1386.9
1360(33) 0.000918 1109.2 1381.7
1386(33) 0.000918 1109.3 1373.7
1292(32) 0.000977 1109.3 1363.5
1330(33) 0.000918 1109.4 1351.5
1297(32) 0.000977 1109.5 1338.3
1332(33) 0.000918 1109.5 1324.2
1296(32) 0.000977 1109.6 1309.9
1278(32) 0.000977 1109.7 1295.5
1296(32) 0.000977 1109.8 1281.5
1254(32) 0.000977 1109.8 1268.2
1235(32) 0.000977 1109.9 1255.7
1232(31) 0.001041 1110.0 1244.3
1208(31) 0.001041 1110.1 1234.1
1248(32) 0.000977 1110.1 1225.0
1220(31) 0.001041 1110.2 1217.1
1253(32) 0.000977 1110.3 1210.5
1196(31) 0.001041 1110.4 1205.1
1203(31) 0.001041 1110.4 1200.9
1160(31) 0.001041 1110.5 1197.8
1216(31) 0.001041 1110.6 1196.0
1204(25) 0.001600 1110.7 1195.3
1225(32) 0.000977 1110.8 1195.6
1220(32) 0.000977 1110.9 1196.9
1185(32) 0.000977 1110.9 1199.2
1227(32) 0.000977 1111.0 1202.3
1240(32) 0.000977 1111.1 1206.0
1253(33) 0.000918 1111.2 1210.4
1274(33) 0.000918 1111.3 1215.1
1241(32) 0.000977 1111.4 1220.1
1265(33) 0.000918 1111.4 1225.2
1240(32) 0.000977 1111.5 1230.2
1271(33) 0.000918 1111.6 1235.0
1282(33) 0.000918 1111.7 1239.3
1319(33) 0.000918 1111.8 1243.1
1310(33) 0.000918 1111.9 1246.2
1311(33) 0.000918 1112.0 1248.6
1334(34) 0.000865 1112.1 1250.1
1274(33) 0.000918 1112.2 1250.6
1274(33) 0.000918 1112.3 1250.2
1228(32) 0.000977 1112.4 1248.8
1282(33) 0.000918 1112.4 1246.5
1285(33) 0.000918 1112.5 1243.4
1323(33) 0.000918 1112.6 1239.7
1306(33) 0.000918 1112.7 1235.7
1300(33) 0.000918 1112.8 1231.5
1272(33) 0.000918 1112.9 1227.5
1260(33) 0.000918 1113.0 1223.6
1239(32) 0.000977 1113.1 1220.2
1222(32) 0.000977 1113.2 1217.4
1249(32) 0.000977 1113.3 1215.2
1257(33) 0.000918 1113.4 1213.8
1181(32) 0.000977 1113.5 1213.2
1176(31) 0.001041 1113.6 1213.3
1250(32) 0.000977 1113.7 1214.2
1222(32) 0.000977 1113.8 1215.8
1208(32) 0.000977 1113.9 1218.0
1182(32) 0.000977 1114.0 1220.8
1198(32) 0.000977 1114.1 1224.0
1253(33) 0.000918 1114.2 1227.7
1217(32) 0.000977 1114.3 1231.6
1219(32) 0.000977 1114.4 1235.8
1211(32) 0.000977 1114.5 1240.1
1202(32) 0.000977 1114.6 1244.4
1230(32) 0.000977 1114.8 1248.7
1200(32) 0.000977 1114.9 1252.9
1233(32) 0.000977 1115.0 1257.2
1260(33) 0.000918 1115.1 1261.3
1278(33) 0.000918 1115.2 1265.4
1225(32) 0.000977 1115.3 1269.5
1339(34) 0.000865 1115.4 1273.7
1278(33) 0.000918 1115.5 1278.0
1321(33) 0.000918 1115.6 1282.3
1304(33) 0.000918 1115.7 1286.8
1301(33) 0.000918 1115.8 1291.3
1352(34) 0.000865 1115.9 1295.9
1337(34) 0.000865 1116.0 1300.5
1295(33) 0.000918 1116.2 1305.0
1266(33) 0.000918 1116.3 1309.3
1304(33) 0.000918 1116.4 1313.4
1366(34) 0.000865 1116.5 1317.2
1311(33) 0.000918 1116.6 1320.5
1355(34) 0.000865 1116.7 1323.3
1379(34) 0.000865 1116.8 1325.6
1331(34) 0.000865 1116.9 1327.4
1325(33) 0.000918 1117.0 1328.9
1325(33) 0.000918 1117.2 1329.9
1345(34) 0.000865 1117.3 1330.6
1357(34) 0.000865 1117.4 1331.0
1318(33) 0.000918 1117.5 1331.1
1329(34) 0.000865 1117.6 1330.8
1344(34) 0.000865 1117.7 1330.3
1354(34) 0.000865 1117.8 1329.3
1279(33) 0.000918 1118.0 1328.0
1295(33) 0.000918 1118.1 1326.2
1338(34) 0.000865 1118.2 1323.9
1325(33) 0.000918 1118.3 1320.9
1363(34) 0.000865 1118.4 1317.3
1307(33) 0.000918 1118.5 1313.1
1293(33) 0.000918 1118.6 1308.1
1225(32) 0.000977 1118.8 1302.4
1261(33) 0.000918 1118.9 1296.2
1345(34) 0.000865 1119.0 1289.6
1256(33) 0.000918 1119.1 1282.6
1274(33) 0.000918 1119.2 1275.5
1281(33) 0.000918 1119.3 1268.6
1271(33) 0.000918 1119.5 1261.7
1241(32) 0.000977 1119.6 1255.1
1221(32) 0.000977 1119.7 1248.9
1271(33) 0.000918 1119.8 1243.2
1179(32) 0.000977 1119.9 1238.1
1236(32) 0.000977 1120.0 1233.7
1207(32) 0.000977 1120.2 1230.1
1218(32) 0.000977 1120.3 1227.3
1184(32) 0.000977 1120.4 1225.3
1242(32) 0.000977 1120.5 1224.1
1177(32) 0.000977 1120.6 1223.8
1158(31) 0.001041 1120.8 1224.2
1151(31) 0.001041 1120.9 1225.2
1216(32) 0.000977 1121.0 1226.8
1165(31) 0.001041 1121.1 1229.0
1204(32) 0.000977 1121.2 1231.5
1235(31) 0.001041 1121.3 1234.3
1224(31) 0.001041 1121.5 1237.2
1201(31) 0.001041 1121.6 1240.3
1224(31) 0.001041 1121.7 1243.4
1200(31) 0.001041 1121.8 1246.4
1226(31) 0.001041 1121.9 1249.5
1219(31) 0.001041 1122.1 1252.4
1282(32) 0.000977 1122.2 1255.3
1245(32) 0.000977 1122.3 1258.0
1226(31) 0.001041 1122.4 1260.7
1338(33) 0.000918 1122.5 1263.2
1226(31) 0.001041 1122.6 1265.6
1263(32) 0.000977 1122.8 1267.8
1242(31) 0.001041 1122.9 1269.8
1289(32) 0.000977 1123.0 1271.8
1261(32) 0.000977 1123.1 1273.5
1296(32) 0.000977 1123.2 1275.2
1259(32) 0.000977 1123.3 1276.6
1275(32) 0.000977 1123.5 1278.0
1269(32) 0.000977 1123.6 1279.3
1276(32) 0.000977 1123.7 1280.5
1283(32) 0.000977 1123.8 1281.8
1300(32) 0.000977 1123.9 1283.2
1273(32) 0.000977 1124.0 1284.9
1310(32) 0.000977 1124.2 1287.0
1313(32) 0.000977 1124.3 1289.7
1311(32) 0.000977 1124.4 1292.9
1331(33) 0.000918 1124.5 1297.0
1350(33) 0.000918 1124.6 1301.7
1266(32) 0.000977 1124.7 1307.3
1320(32) 0.000977 1124.9 1313.6
1341(33) 0.000918 1125.0 1320.7
1342(33) 0.000918 1125.1 1328.6
1363(33) 0.000918 1125.2 1337.2
1327(33) 0.000918 1125.3 1346.3
1336(33) 0.000918 1125.4 1355.9
1394(33) 0.000918 1125.5 1365.8
1394(33) 0.000918 1125.7 1375.9
1480(34) 0.000865 1125.8 1386.0
1420(34) 0.000865 1125.9 1395.9
1444(34) 0.000865 1126.0 1405.7
1473(34) 0.000865 1126.1 1415.1
1518(35) 0.000816 1126.2 1423.9
1523(35) 0.000816 1126.3 1432.0
1498(35) 0.000816 1126.4 1439.3
1512(35) 0.000816 1126.6 1445.6
1473(34) 0.000865 1126.7 1450.8
1514(35) 0.000816 1126.8 1454.8
1505(35) 0.000816 1126.9 1457.5
1462(34) 0.000865 1127.0 1458.9
1492(35) 0.000816 1127.1 1459.0
1479(34) 0.000865 1127.2 1457.6
1467(34) 0.000865 1127.3 1454.8
1479(34) 0.000865 1127.4 1450.8
1465(34) 0.000865 1127.5 1445.3
1467(34) 0.000865 1127.6 1438.6
1432(34) 0.000865 1127.8 1430.8
1411(34) 0.000865 1127.9 1422.0
1427(34) 0.000865 1128.0 1412.6
1402(33) 0.000918 1128.1 1402.6
1418(34) 0.000865 1128.2 1392.5
1366(33) 0.000918 1128.3 1382.4
1403(33) 0.000918 1128.4 1372.5
1451(34) 0.000865 1128.5 1363.1
1404(33) 0.000918 1128.6 1354.1
1330(33) 0.000918 1128.7 1345.9
1343(33) 0.000918 1128.8 1338.3
1343(33) 0.000918 1128.9 1331.5
1371(33) 0.000918 1129.0 1325.4
1348(33) 0.000918 1129.1 1320.0
1307(32) 0.000977 1129.2 1315.2
1280(32) 0.000977 1129.3 1310.9
1295(32) 0.000977 1129.4 1307.2
1278(32) 0.000977 1129.5 1303.8
1242(31) 0.001041 1129.6 1300.8
1281(32) 0.000977 1129.7 1298.2
1346(33) 0.000918 1129.8 1295.8
1282(32) 0.000977 1129.9 1293.8
1303(32) 0.000977 1130.0 1292.0
1333(33) 0.000918 1130.1 1290.6
1265(32) 0.000977 1130.2 1289.4
1284(32) 0.000977 1130.3 1288.7
1301(32) 0.000977 1130.4 1288.2
1253(32) 0.000977 1130.5 1288.2
1211(31) 0.001041 1130.6 1288.3
1269(32) 0.000977 1130.7 1288.8
1284(32) 0.000977 1130.8 1289.6
1238(31) 0.001041 1130.9 1290.8
1223(31) 0.001041 1131.0 1292.2
1278(32) 0.000977 1131.0 1294.1
1252(32) 0.000977 1131.1 1296.1
1293(32) 0.000977 1131.2 1298.4
1341(33) 0.000918 1131.3 1301.0
1290(32) 0.000977 1131.4 1303.9
1357(33) 0.000918 1131.5 1307.0
1331(33) 0.000918 1131.6 1310.5
1349(33) 0.000918 1131.7 1314.2
1292(32) 0.000977 1131.8 1318.2
1303(32) 0.000977 1131.8 1322.5
1205(44) 0.000517 1132. 1327.
1301(31) 0.001041 1132.0 1331.4
1343(32) 0.000977 1132.1 1336.0
1339(32) 0.000977 1132.2 1340.4
1301(31) 0.001041 1132.3 1344.7
1300(31) 0.001041 1132.3 1348.5
1313(32) 0.000977 1132.4 1351.9
1321(32) 0.000977 1132.5 1354.6
1321(32) 0.000977 1132.6 1356.5
1343(32) 0.000977 1132.7 1357.4
1349(32) 0.000977 1132.7 1357.3
1334(32) 0.000977 1132.8 1356.3
1356(32) 0.000977 1132.9 1354.0
1351(32) 0.000977 1133.0 1350.6
1336(32) 0.000977 1133.0 1346.1
1296(31) 0.001041 1133.1 1340.7
1282(31) 0.001041 1133.2 1334.5
1323(32) 0.000977 1133.3 1327.7
1295(31) 0.001041 1133.3 1320.3
1298(31) 0.001041 1133.4 1312.6
1298(31) 0.001041 1133.5 1304.8
1268(31) 0.001041 1133.5 1296.7
1284(31) 0.001041 1133.6 1288.5
1283(31) 0.001041 1133.7 1280.4
1263(31) 0.001041 1133.7 1272.4
1250(31) 0.001041 1133.8 1264.7
1249(31) 0.001041 1133.9 1257.3
1285(31) 0.001041 1133.9 1250.4
1210(30) 0.001111 1134.0 1243.8
1196(30) 0.001111 1134.1 1237.7
1234(31) 0.001041 1134.1 1232.0
1229(31) 0.001041 1134.2 1226.9
1204(30) 0.001111 1134.3 1222.4
1208(30) 0.001111 1134.3 1218.4
1200(30) 0.001111 1134.4 1215.1
1181(30) 0.001111 1134.4 1212.3
1236(31) 0.001041 1134.5 1210.2
1210(30) 0.001111 1134.6 1208.7
1242(31) 0.001041 1134.6 1207.7
1245(31) 0.001041 1134.7 1207.4
1219(30) 0.001111 1134.7 1207.7
1253(31) 0.001041 1134.8 1208.6
1194(30) 0.001111 1134.8 1210.0
1195(30) 0.001111 1134.9 1212.0
1233(31) 0.001041 1134.9 1214.5
1240(31) 0.001041 1135.0 1217.4
1194(30) 0.001111 1135.0 1220.9
1222(30) 0.001111 1135.1 1224.7
1193(30) 0.001111 1135.1 1228.9
1214(30) 0.001111 1135.2 1233.4
1236(31) 0.001041 1135.2 1238.2
1242(31) 0.001041 1135.3 1243.2
1234(31) 0.001041 1135.3 1248.4
1235(31) 0.001041 1135.4 1253.6
1232(31) 0.001041 1135.4 1258.8
1239(31) 0.001041 1135.4 1263.9
1225(30) 0.001111 1135.5 1268.9
1276(31) 0.001041 1135.5 1273.7
1302(31) 0.001041 1135.6 1278.3
1319(32) 0.000977 1135.6 1282.6
1350(32) 0.000977 1135.6 1286.6
1303(31) 0.001041 1135.7 1290.3
1319(32) 0.000977 1135.7 1293.7
1311(32) 0.000977 1135.7 1296.8
1296(31) 0.001041 1135.8 1299.6
1310(32) 0.000977 1135.8 1302.1
1316(32) 0.000977 1135.8 1304.4
1288(31) 0.001041 1135.9 1306.3
1281(31) 0.001041 1135.9 1308.0
1296(31) 0.001041 1135.9 1309.4
1305(32) 0.000977 1136.0 1310.5
1285(31) 0.001041 1136.0 1311.3
1287(31) 0.001041 1136.0 1311.7
1346(32) 0.000977 1136.1 1311.8
1325(32) 0.000977 1136.1 1311.5
1313(32) 0.000977 1136.1 1310.9
1310(32) 0.000977 1136.1 1309.8
1300(31) 0.001041 1136.1 1308.4
1311(32) 0.000977 1136.2 1306.6
1327(32) 0.000977 1136.2 1304.4
1274(31) 0.001041 1136.2 1302.0
1251(31) 0.001041 1136.2 1299.3
1248(31) 0.001041 1136.2 1296.5
1282(31) 0.001041 1136.3 1293.6
1302(31) 0.001041 1136.3 1290.7
1244(31) 0.001041 1136.3 1287.9
1246(31) 0.001041 1136.3 1285.2
1245(31) 0.001041 1136.3 1282.8
1245(31) 0.001041 1136.3 1280.6
1310(32) 0.000977 1136.3 1278.6
1285(31) 0.001041 1136.4 1277.0
1285(31) 0.001041 1136.4 1275.6
1277(31) 0.001041 1136.4 1274.6
1262(31) 0.001041 1136.4 1273.8
1271(31) 0.001041 1136.4 1273.3
1286(31) 0.001041 1136.4 1272.9
1279(31) 0.001041 1136.4 1272.8
1286(31) 0.001041 1136.4 1272.8
1251(31) 0.001041 1136.4 1272.8
1313(32) 0.000977 1136.4 1272.9
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1258(31) 0.001041 1136.4 1272.9
1310(31) 0.001041 1136.4 1272.7
1302(31) 0.001041 1136.4 1272.3
1274(31) 0.001041 1136.4 1271.6
1312(31) 0.001041 1136.4 1270.7
1320(32) 0.000977 1136.4 1269.5
1262(31) 0.001041 1136.4 1268.0
1294(31) 0.001041 1136.4 1266.4
1276(31) 0.001041 1136.4 1264.4
1233(30) 0.001111 1136.4 1262.4
1264(31) 0.001041 1136.4 1260.2
1261(31) 0.001041 1136.4 1257.9
1269(31) 0.001041 1136.4 1255.6
1266(31) 0.001041 1136.4 1253.5
1282(31) 0.001041 1136.3 1251.4
1249(31) 0.001041 1136.3 1249.6
1203(30) 0.001111 1136.3 1248.1
1219(30) 0.001111 1136.3 1246.9
1218(30) 0.001111 1136.3 1246.1
1232(30) 0.001111 1136.3 1245.8
1281(31) 0.001041 1136.3 1245.9
1233(30) 0.001111 1136.2 1246.6
1238(31) 0.001041 1136.2 1247.8
1256(31) 0.001041 1136.2 1249.7
1274(31) 0.001041 1136.2 1252.2
1267(31) 0.001041 1136.2 1255.3
1262(31) 0.001041 1136.2 1259.0
1296(31) 0.001041 1136.1 1263.5
1261(31) 0.001041 1136.1 1268.6
1251(31) 0.001041 1136.1 1274.3
1266(31) 0.001041 1136.1 1280.7
1294(31) 0.001041 1136.0 1287.7
1295(31) 0.001041 1136.0 1295.3
1292(31) 0.001041 1136.0 1303.6
1323(32) 0.000977 1136.0 1312.3
1311(31) 0.001041 1135.9 1321.5
1379(32) 0.000977 1135.9 1331.1
1353(32) 0.000977 1135.9 1341.0
1340(32) 0.000977 1135.9 1351.2
1351(32) 0.000977 1135.8 1361.5
1334(32) 0.000977 1135.8 1371.9
1387(32) 0.000977 1135.8 1382.2
1384(32) 0.000977 1135.7 1392.3
1389(32) 0.000977 1135.7 1402.0
1427(33) 0.000918 1135.7 1411.4
1365(32) 0.000977 1135.6 1420.2
1374(32) 0.000977 1135.6 1428.3
1386(32) 0.000977 1135.6 1435.7
1436(33) 0.000918 1135.5 1442.2
1489(34) 0.000865 1135.5 1447.9
1504(34) 0.000865 1135.5 1452.6
1486(34) 0.000865 1135.4 1456.3
1466(33) 0.000918 1135.4 1459.2
1493(34) 0.000865 1135.4 1461.0
1433(33) 0.000918 1135.3 1461.9
1463(33) 0.000918 1135.3 1461.8
1452(33) 0.000918 1135.3 1460.8
1456(33) 0.000918 1135.2 1458.9
1464(33) 0.000918 1135.2 1456.1
1454(33) 0.000918 1135.1 1452.6
1446(33) 0.000918 1135.1 1448.3
1455(33) 0.000918 1135.1 1443.4
1469(33) 0.000918 1135.0 1438.0
1403(33) 0.000918 1135.0 1432.0
1429(33) 0.000918 1134.9 1425.7
1489(34) 0.000865 1134.9 1419.0
1382(32) 0.000977 1134.9 1412.2
1407(33) 0.000918 1134.8 1405.2
1418(33) 0.000918 1134.8 1398.1
1389(32) 0.000977 1134.7 1391.0
1408(33) 0.000918 1134.7 1383.9
1403(33) 0.000918 1134.6 1377.0
1397(32) 0.000977 1134.6 1370.2
1377(32) 0.000977 1134.6 1363.6
1368(32) 0.000977 1134.5 1357.2
1354(32) 0.000977 1134.5 1351.1
1344(32) 0.000977 1134.4 1345.2
1322(32) 0.000977 1134.4 1339.7
1314(31) 0.001041 1134.3 1334.5
1338(32) 0.000977 1134.3 1329.6
1376(32) 0.000977 1134.2 1325.0
1324(32) 0.000977 1134.2 1320.7
1319(32) 0.000977 1134.2 1316.7
1283(31) 0.001041 1134.1 1313.1
1336(32) 0.000977 1134.1 1309.8
1299(31) 0.001041 1134.0 1306.7
1260(31) 0.001041 1134.0 1304.0
1282(31) 0.001041 1133.9 1301.5
1299(31) 0.001041 1133.9 1299.4
1295(31) 0.001041 1133.9 1297.5
1270(31) 0.001041 1133.8 1295.9
1324(32) 0.000977 1133.8 1294.7
1315(32) 0.000977 1133.7 1293.7
1300(31) 0.001041 1133.7 1293.2
1280(31) 0.001041 1133.6 1293.0
1308(31) 0.001041 1133.6 1293.2
1240(31) 0.001041 1133.5 1293.9
1312(31) 0.001041 1133.5 1295.1
1324(32) 0.000977 1133.5 1296.8
1303(32) 0.000977 1133.4 1299.0
1291(32) 0.000977 1133.4 1301.8
1312(32) 0.000977 1133.3 1305.2
1288(32) 0.000977 1133.3 1309.2
1329(32) 0.000977 1133.3 1313.8
1371(33) 0.000918 1133.2 1318.9
1362(32) 0.000977 1133.2 1324.7
1329(32) 0.000977 1133.1 1331.0
1399(33) 0.000918 1133.1 1337.8
1403(33) 0.000918 1133.1 1345.1
1401(33) 0.000918 1133.0 1352.8
1459(34) 0.000865 1133.0 1360.9
1354(32) 0.000977 1133.0 1369.3
1407(33) 0.000918 1132.9 1377.9
1372(33) 0.000918 1132.9 1386.7
1419(33) 0.000918 1132.8 1395.6
1444(33) 0.000918 1132.8 1404.5
1440(33) 0.000918 1132.8 1413.2
1466(34) 0.000865 1132.7 1421.7
1467(34) 0.000865 1132.7 1429.9
1429(33) 0.000918 1132.7 1437.7
1418(33) 0.000918 1132.7 1445.0
1462(34) 0.000865 1132.6 1451.6
1497(34) 0.000865 1132.6 1457.6
1492(34) 0.000865 1132.6 1462.8
1489(34) 0.000865 1132.5 1467.3
1514(34) 0.000865 1132.5 1470.9
1526(34) 0.000865 1132.5 1473.8
1530(34) 0.000865 1132.5 1475.8
1480(34) 0.000865 1132.5 1477.2
1499(34) 0.000865 1132.4 1477.8
1485(34) 0.000865 1132.4 1477.9
1457(34) 0.000865 1132.4 1477.4
1502(34) 0.000865 1132.4 1476.4
1449(34) 0.000865 1132.4 1475.0
1489(34) 0.000865 1132.3 1473.3
1434(33) 0.000918 1132.3 1471.2
1481(34) 0.000865 1132.3 1468.9
1484(34) 0.000865 1132.3 1466.4
1440(33) 0.000918 1132.3 1463.6
1454(34) 0.000865 1132.3 1460.7
1430(33) 0.000918 1132.3 1457.6
1437(33) 0.000918 1132.3 1454.3
1454(34) 0.000865 1132.3 1450.8
1440(33) 0.000918 1132.3 1447.1
1400(33) 0.000918 1132.3 1443.2
1416(33) 0.000918 1132.3 1439.1
1419(33) 0.000918 1132.3 1434.7
1417(33) 0.000918 1132.3 1430.0
1426(33) 0.000918 1132.3 1425.1
1372(33) 0.000918 1132.3 1419.9
1361(32) 0.000977 1132.3 1414.5
1354(32) 0.000977 1132.3 1408.8
1409(33) 0.000918 1132.3 1403.0
1397(33) 0.000918 1132.4 1396.9
1369(33) 0.000918 1132.4 1390.7
1338(32) 0.000977 1132.4 1384.4
1394(33) 0.000918 1132.4 1378.0
1339(32) 0.000977 1132.4 1371.6
1372(33) 0.000918 1132.5 1365.1
1340(32) 0.000977 1132.5 1358.6
1377(33) 0.000918 1132.5 1352.1
1342(32) 0.000977 1132.6 1345.7
1349(32) 0.000977 1132.6 1339.3
1357(32) 0.000977 1132.6 1333.1
1301(32) 0.000977 1132.7 1326.9
1320(32) 0.000977 1132.7 1320.9
1313(32) 0.000977 1132.8 1315.0
1270(31) 0.001041 1132.8 1309.2
1288(32) 0.000977 1132.9 1303.6
1312(32) 0.000977 1132.9 1298.2
1317(32) 0.000977 1133.0 1293.0
1310(32) 0.000977 1133.0 1288.0
1265(31) 0.001041 1133.1 1283.2
1265(31) 0.001041 1133.2 1278.6
1232(31) 0.001041 1133.2 1274.3
1241(31) 0.001041 1133.3 1270.1
1269(31) 0.001041 1133.4 1266.2
1238(31) 0.001041 1133.4 1262.6
1208(31) 0.001041 1133.5 1259.2
1214(31) 0.001041 1133.6 1256.1
1221(31) 0.001041 1133.7 1253.2
1235(31) 0.001041 1133.8 1250.6
1242(31) 0.001041 1133.9 1248.3
1263(31) 0.001041 1134.0 1246.3
1232(31) 0.001041 1134.1 1244.6
1215(31) 0.001041 1134.2 1243.1
1220(31) 0.001041 1134.3 1242.0
1285(32) 0.000977 1134.4 1241.3
1257(31) 0.001041 1134.5 1240.8
1258(31) 0.001041 1134.6 1240.7
1260(31) 0.001041 1134.7 1240.9
1252(31) 0.001041 1134.9 1241.5
1235(31) 0.001041 1135.0 1242.5
1257(31) 0.001041 1135.1 1243.8
1230(31) 0.001041 1135.3 1245.5
1196(30) 0.001111 1135.4 1247.6
1224(31) 0.001041 1135.6 1250.1
1280(31) 0.001041 1135.7 1253.0
1299(32) 0.000977 1135.9 1256.3
1286(32) 0.000977 1136.0 1260.0
1254(31) 0.001041 1136.2 1264.0
1263(31) 0.001041 1136.3 1268.4
1295(32) 0.000977 1136.5 1273.2
1261(31) 0.001041 1136.7 1278.4
1284(32) 0.000977 1136.9 1283.9
1300(32) 0.000977 1137.0 1289.7
1317(32) 0.000977 1137.2 1295.9
1318(32) 0.000977 1137.4 1302.3
1328(32) 0.000977 1137.6 1309.0
1295(32) 0.000977 1137.8 1315.9
1309(32) 0.000977 1138.0 1323.0
1302(32) 0.000977 1138.3 1330.4
1288(32) 0.000977 1138.5 1337.8
1344(32) 0.000977 1138.7 1345.4
1320(32) 0.000977 1138.9 1353.0
1381(33) 0.000918 1139.2 1360.7
1419(33) 0.000918 1139.4 1368.4
1397(33) 0.000918 1139.6 1376.0
1366(33) 0.000918 1139.9 1383.6
1389(33) 0.000918 1140.1 1391.0
1414(33) 0.000918 1140.4 1398.3
1406(33) 0.000918 1140.7 1405.4
1400(33) 0.000918 1140.9 1412.3
1399(33) 0.000918 1141.2 1419.0
1419(33) 0.000918 1141.5 1425.4
1421(33) 0.000918 1141.8 1431.5
1448(34) 0.000865 1142.1 1437.4
1490(34) 0.000865 1142.4 1443.0
1493(34) 0.000865 1142.7 1448.2
1495(34) 0.000865 1143.0 1453.1
1458(34) 0.000865 1143.3 1457.7
1484(34) 0.000865 1143.7 1462.0
1489(34) 0.000865 1144.0 1466.0
1479(34) 0.000865 1144.3 1469.6
1471(34) 0.000865 1144.7 1472.9
1496(34) 0.000865 1145.0 1475.9
1493(34) 0.000865 1145.4 1478.6
1501(34) 0.000865 1145.8 1481.0
1515(34) 0.000865 1146.2 1483.2
1543(35) 0.000816 1146.5 1485.1
1522(35) 0.000816 1146.9 1486.7
1518(34) 0.000865 1147.3 1488.2
1524(35) 0.000816 1147.7 1489.5
1508(34) 0.000865 1148.1 1490.6
1445(34) 0.000865 1148.6 1491.5
1447(34) 0.000865 1149.0 1492.3
1566(35) 0.000816 1149.4 1492.9
1563(35) 0.000816 1149.9 1493.4
1487(34) 0.000865 1150.3 1493.8
1479(34) 0.000865 1150.8 1494.0
1484(34) 0.000865 1151.2 1494.0
1458(34) 0.000865 1151.7 1493.8
1490(34) 0.000865 1152.2 1493.4
1485(34) 0.000865 1152.7 1492.8
1464(34) 0.000865 1153.2 1491.9
1456(34) 0.000865 1153.7 1490.8
1462(34) 0.000865 1154.2 1489.3
1447(34) 0.000865 1154.7 1487.5
1445(34) 0.000865 1155.3 1485.4
1415(33) 0.000918 1155.8 1482.9
1449(34) 0.000865 1156.3 1480.0
1480(34) 0.000865 1156.9 1476.7
1459(34) 0.000865 1157.5 1473.0
1446(34) 0.000865 1158.0 1469.0
1488(34) 0.000865 1158.6 1464.6
1447(34) 0.000865 1159.2 1459.8
1437(34) 0.000865 1159.8 1454.7
1478(34) 0.000865 1160.5 1449.3
1465(34) 0.000865 1161.1 1443.7
1444(34) 0.000865 1161.7 1437.9
1453(34) 0.000865 1162.4 1431.9
1458(34) 0.000865 1163.0 1425.7
1459(34) 0.000865 1163.7 1419.4
1440(34) 0.000865 1164.4 1413.1
1401(33) 0.000918 1165.0 1406.8
1444(34) 0.000865 1165.7 1400.4
1410(33) 0.000918 1166.4 1394.1
1362(33) 0.000918 1167.2 1387.9
1385(33) 0.000918 1167.9 1381.7
1375(33) 0.000918 1168.6 1375.7
1393(33) 0.000918 1169.4 1369.8
1396(33) 0.000918 1170.1 1364.1
1332(32) 0.000977 1170.9 1358.6
1338(32) 0.000977 1171.7 1353.2
1374(33) 0.000918 1172.5 1348.1
1364(33) 0.000918 1173.3 1343.1
1353(33) 0.000918 1174.1 1338.4
1336(32) 0.000977 1174.9 1334.0
1358(33) 0.000918 1175.8 1329.8
1310(32) 0.000977 1176.6 1325.8
1333(32) 0.000977 1177.5 1322.1
1358(33) 0.000918 1178.4 1318.7
1301(32) 0.000977 1179.3 1315.6
1310(32) 0.000977 1180.2 1312.7
1299(32) 0.000977 1181.1 1310.2
1306(32) 0.000977 1182.0 1307.9
1345(32) 0.000977 1182.9 1305.9
1354(33) 0.000918 1183.9 1304.3
1296(26) 0.001479 1184.8 1303.0
1278(32) 0.000977 1185.8 1302.0
1314(32) 0.000977 1186.8 1301.3
1351(33) 0.000918 1187.8 1301.0
1317(32) 0.000977 1188.8 1301.0
1303(32) 0.000977 1189.9 1301.3
1319(33) 0.000918 1190.9 1302.0
1307(32) 0.000977 1192.0 1303.0
1330(33) 0.000918 1193.1 1304.4
1357(33) 0.000918 1194.1 1306.1
1312(32) 0.000977 1195.2 1308.1
1292(32) 0.000977 1196.4 1310.5
1320(33) 0.000918 1197.5 1313.2
1346(33) 0.000918 1198.6 1316.3
1345(33) 0.000918 1199.8 1319.7
1299(32) 0.000977 1201.0 1323.4
1320(33) 0.000918 1202.2 1327.4
1364(33) 0.000918 1203.4 1331.8
1346(33) 0.000918 1204.6 1336.5
1353(33) 0.000918 1205.8 1341.4
1377(33) 0.000918 1207.1 1346.7
1323(33) 0.000918 1208.3 1352.2
1336(33) 0.000918 1209.6 1358.1
1354(33) 0.000918 1210.9 1364.1
1381(33) 0.000918 1212.2 1370.4
1389(33) 0.000918 1213.6 1377.0
1398(33) 0.000918 1214.9 1383.7
1334(33) 0.000918 1216.3 1390.6
1362(33) 0.000918 1217.6 1397.7
1408(34) 0.000865 1219.0 1404.9
1408(34) 0.000865 1220.5 1412.3
1414(34) 0.000865 1221.9 1419.8
1462(34) 0.000865 1223.3 1427.3
1435(34) 0.000865 1224.8 1434.9
1417(34) 0.000865 1226.3 1442.5
1413(34) 0.000865 1227.8 1450.0
1439(34) 0.000865 1229.3 1457.6
1444(34) 0.000865 1230.8 1465.0
1428(34) 0.000865 1232.4 1472.4
1443(34) 0.000865 1234.0 1479.6
1425(34) 0.000865 1235.6 1486.6
1429(34) 0.000865 1237.2 1493.4
1460(34) 0.000865 1238.8 1500.0
1490(35) 0.000816 1240.4 1506.3
1488(34) 0.000865 1242.1 1512.3
1458(34) 0.000865 1243.8 1518.0
1462(34) 0.000865 1245.5 1523.3
1470(34) 0.000865 1247.2 1528.2
1490(35) 0.000816 1249.0 1532.7
1496(35) 0.000816 1250.7 1536.8
1511(35) 0.000816 1252.5 1540.4
1532(35) 0.000816 1254.3 1543.7
1507(35) 0.000816 1256.1 1546.4
1490(35) 0.000816 1258.0 1548.8
1527(35) 0.000816 1259.9 1550.7
1554(35) 0.000816 1261.7 1552.2
1550(35) 0.000816 1263.6 1553.2
1535(35) 0.000816 1265.6 1554.0
1509(35) 0.000816 1267.5 1554.3
1547(35) 0.000816 1269.5 1554.4
1562(35) 0.000816 1271.5 1554.1
1520(35) 0.000816 1273.5 1553.6
1494(35) 0.000816 1275.5 1552.9
1555(35) 0.000816 1277.6 1552.0
1594(36) 0.000772 1280. 1551.
1572(35) 0.000816 1281.8 1549.7
1529(35) 0.000816 1283.9 1548.4
1518(35) 0.000816 1286.1 1547.0
1567(35) 0.000816 1288.2 1545.6
1582(36) 0.000772 1290. 1544.
1546(35) 0.000816 1292.7 1542.7
1554(35) 0.000816 1294.9 1541.4
1536(35) 0.000816 1297.2 1540.1
1565(35) 0.000816 1299.5 1538.8
1557(35) 0.000816 1301.8 1537.7
1542(35) 0.000816 1304.1 1536.7
1550(35) 0.000816 1306.5 1535.8
1540(35) 0.000816 1308.9 1535.1
1551(35) 0.000816 1311.3 1534.5
1521(35) 0.000816 1313.7 1534.1
1521(35) 0.000816 1316.2 1533.8
1512(35) 0.000816 1318.7 1533.7
1510(35) 0.000816 1321.2 1533.8
1482(34) 0.000865 1323.7 1534.0
1510(35) 0.000816 1326.3 1534.4
1542(35) 0.000816 1328.9 1534.9
1553(35) 0.000816 1331.5 1535.7
1533(35) 0.000816 1334.1 1536.5
1540(35) 0.000816 1336.8 1537.5
1548(35) 0.000816 1339.5 1538.6
1519(35) 0.000816 1342.2 1539.8
1525(35) 0.000816 1345.0 1541.2
1544(35) 0.000816 1347.8 1542.6
1541(35) 0.000816 1350.6 1544.1
1531(35) 0.000816 1353.4 1545.6
1517(35) 0.000816 1356.3 1547.2
1515(35) 0.000816 1359.2 1548.8
1558(35) 0.000816 1362.1 1550.4
1587(36) 0.000772 1365. 1552.
1572(35) 0.000816 1368.0 1553.7
1572(36) 0.000772 1371. 1555.
1591(36) 0.000772 1374. 1557.
1599(36) 0.000772 1377. 1558.
1541(36) 0.000772 1380. 1560.
1535(36) 0.000772 1383. 1561.
1630(37) 0.000730 1387. 1563.
1616(37) 0.000730 1390. 1564.
1621(37) 0.000730 1393. 1566.
1585(36) 0.000772 1396. 1567.
1594(36) 0.000772 1399. 1568.
1603(36) 0.000772 1403. 1569.
1570(36) 0.000772 1406. 1571.
1605(36) 0.000772 1410. 1572.
1662(37) 0.000730 1413. 1573.
1622(37) 0.000730 1416. 1574.
1617(37) 0.000730 1420. 1576.
1621(37) 0.000730 1423. 1577.
1589(36) 0.000772 1427. 1578.
1594(36) 0.000772 1430. 1580.
1596(36) 0.000772 1434. 1581.
1616(37) 0.000730 1438. 1582.
1651(37) 0.000730 1441. 1584.
1618(37) 0.000730 1445. 1585.
1564(36) 0.000772 1449. 1587.
1544(36) 0.000772 1453. 1589.
1565(36) 0.000772 1456. 1591.
1615(37) 0.000730 1460. 1593.
1608(37) 0.000730 1464. 1595.
1570(36) 0.000772 1468. 1597.
1633(37) 0.000730 1472. 1600.
1654(37) 0.000730 1476. 1602.
1617(37) 0.000730 1480. 1605.
1644(37) 0.000730 1484. 1608.
1614(37) 0.000730 1488. 1611.
1634(37) 0.000730 1492. 1614.
1632(37) 0.000730 1496. 1617.
1665(37) 0.000730 1501. 1621.
1647(37) 0.000730 1505. 1624.
1613(37) 0.000730 1509. 1628.
1631(37) 0.000730 1514. 1632.
1617(37) 0.000730 1518. 1636.
1641(37) 0.000730 1522. 1641.
1664(37) 0.000730 1527. 1645.
1658(37) 0.000730 1531. 1650.
1635(37) 0.000730 1536. 1655.
1661(37) 0.000730 1540. 1660.
1691(37) 0.000730 1545. 1665.
1656(37) 0.000730 1550. 1671.
1697(37) 0.000730 1554. 1676.
1664(37) 0.000730 1559. 1682.
1649(37) 0.000730 1564. 1688.
1643(37) 0.000730 1569. 1694.
1659(37) 0.000730 1573. 1700.
1721(38) 0.000693 1578. 1707.
1665(37) 0.000730 1583. 1713.
1672(37) 0.000730 1588. 1720.
1705(38) 0.000693 1593. 1727.
1769(38) 0.000693 1598. 1733.
1783(38) 0.000693 1603. 1740.
1745(38) 0.000693 1608. 1748.
1750(38) 0.000693 1614. 1755.
1736(38) 0.000693 1619. 1762.
1724(38) 0.000693 1624. 1770.
1797(39) 0.000657 1629. 1777.
1759(38) 0.000693 1635. 1785.
1810(39) 0.000657 1640. 1792.
1735(38) 0.000693 1646. 1800.
1771(38) 0.000693 1651. 1808.
1807(39) 0.000657 1657. 1816.
1861(39) 0.000657 1662. 1824.
1852(39) 0.000657 1668. 1832.
1824(39) 0.000657 1674. 1840.
1849(39) 0.000657 1679. 1848.
1840(39) 0.000657 1685. 1856.
1848(39) . . .
1789(38) . . .
1804(39) . . .
1824(39) . . .
1904(40) . . .
1912(40) . . .
1901(40) . . .
1899(40) . . .
1935(40) . . .
1947(40) . . .
1919(40) . . .
1952(40) . . .
1973(40) . . .
1903(40) . . .
1900(40) . . .
1925(40) . . .
1996(41) . . .
1984(40) . . .
1987(40) . . .
2037(41) . . .
2032(41) . . .
2063(41) . . .
2029(41) . . .
2012(41) . . .
2049(41) . . .
2081(41) . . .
2105(60) . . .
1999(58) . . .
2090(60) . . .
2219(61) . . .
2076(59) . . .
2109(60) . . .
2107(60) . . .
2115(60) . . .
2074(59) . . .
2140(60) . . .
2116(60) . . .
2137(60) . . .
2176(61) . . .
2136(60) . . .
2178(61) . . .
2177(61) . . .
2163(60) . . .
2198(61) . . .
2195(61) . . .
2229(61) . . .
2310(62) . . .
2302(62) . . .
2323(63) . . .
2285(62) . . .
2275(62) . . .
2313(62) . . .
2289(62) . . .
2335(63) . . .
2288(62) . . .
2310(62) . . .
2282(62) . . .
2363(63) . . .
2366(63) . . .
2454(64) . . .
2365(63) . . .
2441(64) . . .
2355(63) . . .
2419(64) . . .
2436(64) . . .
2349(63) . . .
2390(63) . . .
2459(64) . . .
2451(64) . . .
2425(64) . . .
2491(65) . . .
2488(65) . . .
2476(64) . . .
2521(65) . . .
2550(65) . . .
2588(66) . . .
2543(65) . . .
2479(64) . . .
2406(64) . . .
2523(65) . . .
2502(65) . . .
2615(66) . . .
2576(66) . . .
2501(65) . . .
2486(65) . . .
2525(65) . . .
2570(66) . . .
2575(66) . . .
2474(64) . . .
2570(66) . . .
2491(65) . . .
2649(67) . . .
2630(66) . . .
2598(66) . . .
2587(66) . . .
2625(66) . . .
2592(66) . . .
2608(66) . . .
2636(66) . . .
2743(68) . . .
2669(67) . . .
2676(67) . . .
2665(67) . . .
2565(66) . . .
2498(65) . . .
2539(65) . . .
2601(66) . . .
2716(67) . . .
2667(67) . . .
2619(66) . . .
2627(66) . . .
2570(66) . . .
2595(66) . . .
2657(67) . . .
2654(67) . . .
2680(67) . . .
2700(67) . . .
2640(66) . . .
2666(67) . . .
2575(66) . . .
2655(67) . . .
2666(67) . . .
2737(68) . . .
2748(68) . . .
2765(68) . . .
2690(67) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_cell_measurement_reflns_used    660
_reflns_number_total             660
_reflns_limit_h_min              1
_reflns_limit_h_max              18
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.056
_reflns_d_resolution_low         18.896
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_FINAL_publ_CCDC1
_database_code_depnum_ccdc_archive 'CCDC 1582005'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-03-08T12:39|FINAL|blah|17BM

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-03-08T12:39

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.04
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     30
_refine_ls_goodness_of_fit_all   3.20
_refine_ls_number_restraints     6
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    100

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from Z:/Users/wendyqueen/Desktop/research/Gas Storage Research/Jef'
_cell_length_a                   18.80041(11)
_cell_length_b                   18.80041
_cell_length_c                   18.80041
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6645.10(11)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Fe Fe1 0.13601(10) 0.5 0.0 1.0 Uiso 0.0183(4) 12
C C1 0.1498(4) 0.3341(5) -0.1498(4) 1.0 Uiso 0.0477(23) 24
C C2 0.1810(4) 0.2701(4) -0.1810(4) 1.0 Uiso 0.0477(23) 24
C C3 0.23970(34) 0.23970(34) -0.1468(4) 1.0 Uiso 0.0477(23) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.0153(23) 3
N N1 0.12935(14) 0.42012(20) -0.07952(16) 1.0 Uiso 0.0191(11) 48
N N2 0.17459(24) 0.36607(23) -0.09201(23) 1.0 Uiso 0.0191(11) 48
Fe Fe3 0.2447(24) 0.0 0.0 0.1137(23) Uiso 0.28059 6
O Os 0.2578(5) 0.5 0.0 1.0 Uiso 0.09725 12
C Cs 0.3180(6) 0.5 0.0491(7) 0.5 Uiso 0.09725 24
O Os2 0.3698(30) 0.3698(30) 0.0 0.1272(13) Uiso 0.12388 12
C Cs2 0.4194(22) 0.4194(22) -0.031(8) 0.0636(7) Uiso 0.12388 24
O Os3 -0.086(5) 0.0 0.0 0.1137(23) Uiso 0.28059 6
Fe Fe2 0.2523(8) 0.3619(7) 0.0 0.1272(13) Uiso 0.12388 24

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C28.51 Cl Fe5.24 N32 O4.74'
_chemical_formula_weight         1194.78
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Fe1 Cl1 2.5570(18) . 1_555 N
Fe1 N1 2.1228(29) . 1_555 N
Fe1 N1 2.1228(29) . 4_555 N
Fe1 N1 2.1228(29) . 12_565 N
Fe1 N1 2.1228(29) . -10_565 N
Fe1 Os 2.290(9) . 1_555 N
C1 C2 1.461(7) . 1_555 N
C1 N1 2.124(7) . 1_555 N
C1 N1 2.124(7) . 19_555 N
C1 N2 1.326(4) . 1_555 N
C1 N2 1.326(4) . 19_555 N
C2 C1 1.461(7) . 1_555 N
C2 C3 1.4000(30) . 1_555 N
C2 C3 1.4000(30) . 7_555 N
C3 C2 1.4000(30) . 1_555 N
C3 C2 1.4000(30) . 9_555 N
Cl1 Fe1 2.5570(18) . 1_555 N
Cl1 Fe1 2.5570(18) . 10_555 N
Cl1 Fe1 2.5570(18) . 14_555 N
Cl1 Fe1 2.5570(18) . 19_555 N
N1 Fe1 2.1228(29) . 1_555 N
N1 C1 2.124(7) . 1_555 N
N1 N1 1.325(4) . 19_555 N
N1 N2 1.346(5) . 1_555 N
N2 C1 1.326(4) . 1_555 N
N2 N1 1.346(5) . 1_555 N
N2 Fe2 2.266(10) . 1_555 N
Os Fe1 2.290(9) . 1_555 N
Os Cs 1.461(9) . 1_555 N
Os Cs 1.461(9) . 4_555 N
Cs Os 1.461(9) . 1_555 N
Cs Cs 1.846(28) . 4_555 N
Os2 Cs2 1.439(10) . 1_555 N
Os2 Cs2 1.439(10) . 4_555 N
Os2 Fe2 2.21(6) . 1_555 N
Os2 Fe2 2.21(6) . 13_555 N
Cs2 Os2 1.439(10) . 1_555 N
Cs2 Cs2 1.15(32) . 4_555 N
Fe2 N2 2.266(10) . 1_555 N
Fe2 N2 2.266(10) . 4_555 N
Fe2 Os2 2.21(6) . 1_555 N
Fe2 Fe2 2.915(33) . 13_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Fe1 N1 86.62(10) 1_555 . 1_555 N
Cl1 Fe1 N1 86.62(10) 1_555 . 4_555 N
Cl1 Fe1 N1 86.62(10) 1_555 . 12_565 N
Cl1 Fe1 N1 86.62(10) 1_555 . -10_565 N
N1 Fe1 N1 89.54(22) 1_555 . 4_555 N
N1 Fe1 N1 173.24(21) 1_555 . 12_565 N
N1 Fe1 N1 90.06(21) 1_555 . -10_565 N
N1 Fe1 N1 90.06(21) 4_555 . 12_565 N
N1 Fe1 N1 173.24(21) 4_555 . -10_565 N
N1 Fe1 N1 89.54(22) 12_565 . -10_565 N
C2 C1 N2 124.1(4) 1_555 . 1_555 N
C2 C1 N2 124.1(4) 1_555 . 19_555 N
N2 C1 N2 111.7(8) 1_555 . 19_555 N
C1 C2 C3 117.93(26) 1_555 . 1_555 N
C1 C2 C3 117.93(26) 1_555 . 7_555 N
C3 C2 C3 123.9(5) 1_555 . 7_555 N
C2 C3 C2 115.7(5) 1_555 . 9_555 N
Fe1 Cl1 Fe1 180.0 1_555 . 10_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 19_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 19_555 N
Fe1 Cl1 Fe1 180.0 14_555 . 19_555 N
Fe1 N1 N1 122.66(8) 1_555 . 19_555 N
Fe1 N1 N2 128.30(23) 1_555 . 1_555 N
N1 N1 N2 108.88(21) 19_555 . 1_555 N
C1 N2 N1 105.3(5) 1_555 . 1_555 N
Cs Os Cs 78.4(13) 1_555 . 4_555 N
Cs2 Os2 Cs2 47(14) 1_555 . 4_555 N
Os2 Cs2 Cs2 66(7) 1_555 . 4_555 N

# Powder diffraction data for histogram  5
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT601_FINAL_publ          
;
PROBLEM: Structure Contains Solvent Accessible VOIDS of .       2348 Ang3    ! Info 
RESPONSE: This is expected as the material is porous and it is evacuated.
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_diffrn_ambient_temperature      100
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  17-BM
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Fe 15.735 0.000 0.000 11.7695 4.76110 7.35730 0.30720 3.52220 15.3535 2.30450
76.8805 1.03690 International_Tables_Vol_C
C 85.526 0.000 0.000 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500
51.6512 0.21560 International_Tables_Vol_C
Cl 3.0 0.000 0.000 11.4604 0.01040 7.19640 1.16620 6.25560 18.5194 1.64550
47.7784 -9.5574 International_Tables_Vol_C
N 96.0 0.000 0.000 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630
0.58260 -11.529 International_Tables_Vol_C
H 0.0 0.000 0.000 0.49300 10.5109 0.32291 26.1257 0.14019 3.14236 0.04081
57.7997 0.00304 International_Tables_Vol_C
O 14.208 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
_diffrn_radiation_probe          x-ray
_diffrn_radiation_polarisn_ratio 0.95
_diffrn_radiation_wavelength     0.61072
_diffrn_radiation_type           ?
_pd_proc_ls_prof_R_factor        0.0213
_pd_proc_ls_prof_wR_factor       0.0289
_pd_proc_ls_prof_wR_expected     0.0091
_refine_ls_R_Fsqd_factor         0.05319

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 32 terms.
 Shifted Chebyshev function of 1st kind
      1:    7968.44     2:   -6915.90     3:    2832.16     4:   -787.614    
      5:   -192.508     6:   -155.474     7:    660.745     8:   -540.162    
      9:    127.716    10:    214.669    11:   -460.023    12:    208.526    
     13:   -16.7118    14:   -108.416    15:    80.7819    16:   -47.9302    
     17:   -9.22506    18:   -37.5550    19:    76.0069    20:   -132.787    
     21:    124.008    22:   -91.7071    23:    31.9891    24:    20.5344    
     25:   -28.0893    26:    42.7098    27:   -16.2578    28:    33.1962    
     29:   -75.9283    30:    78.3085    31:   -43.1458    32:    19.0254    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  207.010 #2(GV)   =  -17.288 #3(GW)   =    3.999
 #4(GP)   =    0.897 #5(LX)   =    0.161 #6(LY)   =   22.980
 #7(S/L)  =   0.0005 #8(H/L)  =   0.0005
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2016-03-08T12:39:00
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        0.0108
_pd_meas_2theta_range_max        35.9964
_pd_meas_2theta_range_inc        0.0072
_pd_proc_2theta_range_min        0.00853
_pd_proc_2theta_range_max        35.99413
_pd_proc_2theta_range_inc        0.0072

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3733.0 0.0002679 3261.02759 3720.11377
3751.0 0.0002666 3262.00293 3746.35400
3795.0 0.0002635 3262.96997 3772.25537
3819.0 0.0002618 3263.92627 3797.42139
3862.0 0.0002589 3264.87134 3821.57593
3876.0 0.0002580 3265.80225 3844.46582
3919.0 0.0002552 3266.71802 3866.08203
3952.0 0.0002530 3267.61548 3886.20581
4005.0 0.0002497 3268.49512 3904.76636
4040.0 0.0002475 3269.35352 3922.02710
4083.0 0.0002449 3270.18823 3937.78784
4090.0 0.0002445 3270.99829 3952.03711
4121.0 0.0002427 3271.78027 3964.82983
4120.0 0.0002427 3272.53345 3976.40430
4122.0 0.0002426 3273.25415 3986.97559
4099.0 0.0002440 3273.94116 3996.90405
4112.0 0.0002432 3274.59082 4006.34180
4129.0 0.0002422 3275.20190 4015.65210
4131.0 0.0002421 3275.77173 4024.72119
4115.0 0.0002430 3276.29688 4033.40332
4103.0 0.0002437 3276.77515 4041.50122
4114.0 0.0002431 3277.20410 4048.46875
4106.0 0.0002435 3277.58057 4053.84937
4108.0 0.0002434 3277.90137 4056.97119
4088.0 0.0002446 3278.16431 4057.10938
4097.0 0.0002441 3278.36621 4053.55688
4079.0 0.0002452 3278.50391 4045.78687
4077.0 0.0002453 3278.57422 4033.57788
4042.0 0.0002474 3278.57397 4017.08154
4038.0 0.0002476 3278.50000 3996.74365
3991.0 0.0002506 3278.34912 3973.27148
3986.0 0.0002509 3278.11792 3947.39209
3948.0 0.0002533 3277.80347 3919.89526
3942.0 0.0002537 3277.40137 3891.46094
3862.0 0.0002589 3276.90894 3862.79517
3835.0 0.0002608 3276.32275 3834.55786
3796.0 0.0002634 3275.63843 3807.39160
3786.0 0.0002641 3274.85327 3781.95825
3739.0 0.0002675 3273.96289 3758.77856
3698.0 0.0002704 3272.96533 3738.33252
3682.0 0.0002716 3271.85449 3720.91187
3655.0 0.0002736 3270.62817 3706.69702
3650.0 0.0002740 3269.28174 3695.67139
3635.0 0.0002751 3267.81226 3687.69922
3639.0 0.0002748 3266.21631 3682.50635
3634.0 0.0002752 3264.48926 3679.70752
3649.0 0.0002740 3262.62817 3678.84399
3657.0 0.0002734 3260.62842 3679.46851
3656.0 0.0002735 3258.48926 3681.14941
3656.0 0.0002735 3256.20239 3683.54248
3654.0 0.0002737 3253.76636 3686.40576
3691.0 0.0002709 3251.17920 3689.56787
3695.0 0.0002706 3248.43457 3692.90161
3717.0 0.0002690 3245.53223 3696.29370
3694.0 0.0002707 3242.46558 3699.23267
3728.0 0.0002682 3239.23633 3702.32935
3736.0 0.0002677 3235.83447 3705.06274
3759.0 0.0002660 3232.26270 3707.30200
3748.0 0.0002668 3228.51367 3708.90674
3756.0 0.0002662 3224.58643 3709.72607
3737.0 0.0002676 3220.48145 3709.58057
3705.0 0.0002699 3216.19116 3708.24316
3680.0 0.0002717 3211.71802 3705.49048
3663.0 0.0002730 3207.05566 3701.20410
3663.0 0.0002730 3202.20923 3695.29419
3640.0 0.0002747 3197.16699 3687.75220
3650.0 0.0002740 3191.93604 3678.65601
3614.0 0.0002767 3186.50879 3668.08398
3617.0 0.0002765 3180.88818 3656.14111
3595.0 0.0002782 3175.07666 3642.94360
3603.0 0.0002775 3169.06763 3628.64355
3578.0 0.0002795 3162.86816 3613.50977
3559.0 0.0002810 3156.47217 3597.88086
3564.0 0.0002806 3149.89087 3582.21289
3557.0 0.0002811 3143.11255 3566.93408
3571.0 0.0002800 3136.14551 3552.49048
3522.0 0.0002839 3128.99634 3539.20972
3529.0 0.0002834 3121.66064 3527.14307
3476.0 0.0002877 3114.15015 3516.65186
3505.0 0.0002853 3106.46069 3507.48438
3468.0 0.0002884 3098.60962 3499.40991
3500.0 0.0002857 3090.58618 3492.04761
3471.0 0.0002881 3082.40942 3484.96704
3471.0 0.0002881 3074.07764 3477.68335
3460.0 0.0002890 3065.60718 3469.71997
3463.0 0.0002888 3056.99829 3460.84668
3479.0 0.0002874 3048.26538 3450.83179
3440.0 0.0002907 3039.42334 3439.63867
3453.0 0.0002896 3030.47461 3427.32056
3408.0 0.0002934 3021.44580 3414.03735
3445.0 0.0002903 3012.33203 3399.93896
3409.0 0.0002933 3003.16260 3385.25293
3438.0 0.0002909 2993.94385 3370.21313
3361.0 0.0002975 2984.69800 3355.13525
3354.0 0.0002982 2975.44849 3340.39697
3320.0 0.0003012 2966.20630 3326.39551
3350.0 0.0002985 2957.00757 3313.58374
3311.0 0.0003020 2947.85571 3302.33838
3272.0 0.0003056 2938.79004 3293.03345
3236.0 0.0003090 2929.82813 3285.93677
3256.0 0.0003071 2921.00269 3281.10327
3285.0 0.0003044 2912.34839 3278.94385
3254.0 0.0003073 2903.88818 3279.33838
3258.0 0.0003069 2895.66528 3282.25464
3280.0 0.0003049 2887.70703 3287.62500
3365.0 0.0002972 2880.06494 3295.36304
3341.0 0.0002993 2872.76221 3305.44165
3334.0 0.0002999 2865.85522 3317.63159
3275.0 0.0003053 2859.38184 3332.50903
3370.0 . . .
3402.0 . . .
3494.0 . . .
3537.0 . . .
3574.0 . . .
3647.0 . . .
3584.0 . . .
3629.0 . . .
3551.0 . . .
3624.0 . . .
3618.0 . . .
3792.0 . . .
3784.0 . . .
3836.0 . . .
3808.0 . . .
3888.0 . . .
3915.0 . . .
3894.0 . . .
3866.0 . . .
3806.0 . . .
3734.0 . . .
3733.0 . . .
3778.0 . . .
3811.0 . . .
3809.0 . . .
3731.0 . . .
3541.0 . . .
3542.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
-331.0 . . .
-331.0 . . .
-128.0 . . .
11.0 . . .
-71.0 . . .
-117.0 . . .
-26.0 . . .
208.0 . . .
208.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
0.0 . . .
_pd_meas_number_of_points        4999
_pd_proc_number_of_points        4999

_reflns_number_total             755
_reflns_limit_h_min              1
_reflns_limit_h_max              19
_reflns_limit_k_min              0
_reflns_limit_k_max              13
_reflns_limit_l_min              0
_reflns_limit_l_max              11
_reflns_d_resolution_high        1.002
_reflns_d_resolution_low         18.800
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_0P5CO2_FREECL_publ
_database_code_depnum_ccdc_archive 'CCDC 1582006'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-02-13T16:21|0P5CO2_FREECL|bt1|bt1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-02-13T16:21

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.07
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     45
_refine_ls_goodness_of_fit_all   1.01
_refine_ls_number_restraints     6
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   'Cu MOF'
_cell_length_a                   18.52951(33)
_cell_length_b                   18.52951
_cell_length_c                   18.52951
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6361.97(34)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cu Cu1 0.1330(5) 0.5 0.0 1.0 Uiso 0.0084(27) 12
C C1 0.14765(26) 0.33736(33) -0.14765(26) 1.0 Uiso 0.0065(9) 24
C C2 0.18009(24) 0.27141(33) -0.18009(24) 1.0 Uiso 0.0065(9) 24
C C3 0.24201(25) 0.24201(25) -0.1484(4) 1.0 Uiso 0.0065(9) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.041(5) 3
N N1 0.12938(18) 0.42535(18) -0.07844(18) 1.0 Uiso 0.0081(5) 48
N N2 0.17411(20) 0.37008(18) -0.08936(17) 1.0 Uiso 0.0081(5) 48
H H1 0.2657(5) 0.2657(5) -0.1013(7) 1.0 Uiso 0.020(4) 24
Cu Cu2 0.2270(14) 0.3842(22) 0.0 0.19199 Uiso 0.06409 24
C C1a 0.2913(10) 0.4388(6) 0.0 0.266(5) Uiso 0.011(6) 24
O O1a 0.2735(15) 0.5 0.0 0.533(9) Uiso 0.08(1) 12
O O1b 0.3118(15) 0.3796(10) 0.0 0.266(5) Uiso 0.05(1) 24
Cl Cl2 0.3576(18) 0.3576(18) 0.0 0.19199 Uiso 0.06535 12
O Os 0.2505(7) 0.5 0.0 0.17378 Uiso 0.01168 12

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C26.13 H8 Cl1.77 Cu5.54 N32 O4.96'
_chemical_formula_weight         1263.93
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 Cu1 3.485(13) . 14_555 N
Cu1 Cu1 3.485(13) . 19_555 N
Cu1 Cl1 2.465(9) . 1_555 N
Cu1 N1 2.0076(31) . 1_555 N
Cu1 N1 2.0076(31) . 4_555 N
Cu1 N1 2.0076(31) . 12_565 N
Cu1 N1 2.947(4) . 17_555 N
Cu1 N1 2.947(4) . 19_555 N
Cu1 N1 2.947(4) . 23_565 N
Cu1 N1 2.0076(31) . -10_565 N
Cu1 N1 2.947(4) . -14_565 N
Cu1 N2 3.019(4) . 1_555 N
Cu1 N2 3.019(4) . 4_555 N
Cu1 N2 3.019(4) . 12_565 N
Cu1 N2 3.019(4) . -10_565 N
Cu1 Cu2 2.76(4) . 1_555 N
Cu1 Cu2 2.76(4) . 12_565 N
Cu1 C1a 3.145(18) . 1_555 N
Cu1 C1a 3.145(18) . 12_565 N
Cu1 O1a 2.603(29) . 1_555 N
Cu1 Os 2.178(10) . 1_555 N
C1 C2 1.489(9) . 1_555 N
C1 C3 2.486(6) . 1_555 N
C1 C3 2.486(6) . 7_555 N
C1 N1 2.102(7) . 1_555 N
C1 N1 2.102(7) . 19_555 N
C1 N2 1.332(5) . 1_555 N
C1 N2 1.332(5) . 19_555 N
C1 Cu2 3.225(16) . 1_555 N
C1 Cu2 3.225(16) . 19_555 N
C2 C1 1.489(9) . 1_555 N
C2 C2 2.393(11) . 7_555 N
C2 C2 2.393(11) . 9_555 N
C2 C3 1.399(5) . 1_555 N
C2 C3 1.399(5) . 7_555 N
C2 C3 2.798(9) . 9_555 N
C2 N2 2.486(6) . 1_555 N
C2 N2 2.486(6) . 19_555 N
C3 C1 2.486(6) . 1_555 N
C3 C1 2.486(6) . 9_555 N
C3 C2 1.399(5) . 1_555 N
C3 C2 2.798(9) . 7_555 N
C3 C2 1.399(5) . 9_555 N
C3 C3 2.453(12) . 7_555 N
C3 C3 2.453(12) . 9_555 N
C3 N2 2.900(5) . 1_555 N
C3 N2 2.900(5) . 13_555 N
C3 H1 1.071(17) . 1_555 N
Cl1 Cu1 2.465(9) . 1_555 N
Cl1 Cu1 2.465(9) . 10_555 N
Cl1 Cu1 2.465(9) . 14_555 N
Cl1 Cu1 2.465(9) . 19_555 N
Cl1 N1 3.1263(32) . 1_555 N
Cl1 N1 3.1263(32) . 4_555 N
Cl1 N1 3.1263(32) . 10_555 N
Cl1 N1 3.1263(32) . 12_565 N
Cl1 N1 3.1263(32) . 14_555 N
Cl1 N1 3.1263(32) . 17_555 N
Cl1 N1 3.1263(32) . 19_555 N
Cl1 N1 3.1263(32) . 23_565 N
Cl1 N1 3.1263(32) . -1_565 N
Cl1 N1 3.1263(32) . -4_565 N
Cl1 N1 3.1263(32) . -10_565 N
Cl1 N1 3.1263(32) . -12_555 N
Cl1 N1 3.1263(32) . -14_565 N
Cl1 N1 3.1263(32) . -17_565 N
Cl1 N1 3.1263(32) . -19_565 N
Cl1 N1 3.1263(32) . -23_555 N
N1 Cu1 2.0076(31) . 1_555 N
N1 Cu1 2.947(4) . 19_555 N
N1 C1 2.102(7) . 1_555 N
N1 Cl1 3.1263(32) . 1_555 N
N1 N1 2.907(7) . 4_555 N
N1 N1 1.335(7) . 19_555 N
N1 N1 2.767(7) . -10_565 N
N1 N1 3.072(7) . -14_565 N
N1 N2 1.333(5) . 1_555 N
N1 N2 3.377(5) . 4_555 N
N1 N2 2.177(4) . 19_555 N
N1 Cu2 2.442(24) . 1_555 N
N1 O1a 3.340(23) . 1_555 N
N1 Os 3.011(11) . 1_555 N
N2 Cu1 3.019(4) . 1_555 N
N2 C1 1.332(5) . 1_555 N
N2 C2 2.486(6) . 1_555 N
N2 C3 2.900(5) . 1_555 N
N2 N1 1.333(5) . 1_555 N
N2 N1 3.377(5) . 4_555 N
N2 N1 2.177(4) . 19_555 N
N2 N2 3.312(6) . 4_555 N
N2 N2 2.221(6) . 19_555 N
N2 Cu2 1.942(14) . 1_555 N
N2 C1a 3.014(14) . 1_555 N
N2 O1a 3.453(15) . 1_555 N
N2 O1b 3.047(24) . 1_555 N
N2 Cl2 3.789(29) . 1_555 N
N2 Os 3.247(7) . 1_555 N
H1 C3 1.071(17) . 1_555 N
H1 Cu2 2.977(31) . 1_555 N
H1 Cu2 2.977(31) . 13_555 N
H1 Cl2 3.05(4) . 1_555 N
Cu2 Cu1 2.76(4) . 1_555 N
Cu2 C1 3.225(16) . 1_555 N
Cu2 C1 3.225(16) . 4_555 N
Cu2 N1 2.442(24) . 1_555 N
Cu2 N1 2.442(24) . 4_555 N
Cu2 N2 1.942(14) . 1_555 N
Cu2 N2 1.942(14) . 4_555 N
Cu2 H1 2.977(31) . 1_555 N
Cu2 H1 2.977(31) . 4_555 N
Cu2 C1a 1.56(4) . 1_555 N
Cu2 O1a 2.31(4) . 1_555 N
Cu2 O1b 1.57(4) . 1_555 N
Cu2 O1b 3.129(33) . 13_555 N
Cu2 Cl2 2.469(19) . 1_555 N
Cu2 Os 2.19(4) . 1_555 N
C1a Cu1 3.145(18) . 1_555 N
C1a N2 3.014(14) . 1_555 N
C1a N2 3.014(14) . 4_555 N
C1a Cu2 1.56(4) . 1_555 N
C1a C1a 2.268(23) . 12_565 N
C1a O1a 1.181(9) . 1_555 N
C1a O1b 1.162(10) . 1_555 N
C1a O1b 3.387(26) . 12_565 N
C1a O1b 2.865(29) . 13_555 N
C1a Cl2 1.942(14) . 1_555 N
C1a Os 1.363(15) . 1_555 N
O1a Cu1 2.603(29) . 1_555 N
O1a N1 3.340(23) . 1_555 N
O1a N1 3.340(23) . 4_555 N
O1a N1 3.340(23) . 12_565 N
O1a N1 3.340(23) . -10_565 N
O1a N2 3.453(15) . 1_555 N
O1a N2 3.453(15) . 4_555 N
O1a N2 3.453(15) . 12_565 N
O1a N2 3.453(15) . -10_565 N
O1a Cu2 2.31(4) . 1_555 N
O1a Cu2 2.31(4) . 12_565 N
O1a C1a 1.181(9) . 1_555 N
O1a C1a 1.181(9) . 12_565 N
O1a O1b 2.342(14) . 1_555 N
O1a O1b 2.342(14) . 12_565 N
O1a Cl2 3.065(18) . 1_555 N
O1a Cl2 3.065(18) . 12_565 N
O1a Os 0.425(31) . 1_555 N
O1b N2 3.047(24) . 1_555 N
O1b N2 3.047(24) . 4_555 N
O1b Cu2 1.57(4) . 1_555 N
O1b Cu2 3.129(33) . 13_555 N
O1b C1a 1.162(10) . 1_555 N
O1b C1a 3.387(26) . 12_565 N
O1b C1a 2.865(29) . 13_555 N
O1b O1a 2.342(14) . 1_555 N
O1b Cl2 0.941(30) . 1_555 N
O1b Os 2.504(16) . 1_555 N
Cl2 N2 3.789(29) . 1_555 N
Cl2 N2 3.789(29) . 4_555 N
Cl2 N2 3.789(29) . 13_555 N
Cl2 N2 3.789(29) . 16_555 N
Cl2 H1 3.05(4) . 1_555 N
Cl2 H1 3.05(4) . 4_555 N
Cl2 Cu2 2.469(19) . 1_555 N
Cl2 Cu2 2.469(19) . 13_555 N
Cl2 C1a 1.942(14) . 1_555 N
Cl2 C1a 1.942(14) . 13_555 N
Cl2 O1a 3.065(18) . 1_555 N
Cl2 O1a 3.065(18) . 13_555 N
Cl2 O1b 0.941(30) . 1_555 N
Cl2 O1b 0.941(30) . 13_555 N
Cl2 Os 3.301(10) . 1_555 N
Cl2 Os 3.301(10) . 13_555 N
Os Cu1 2.178(10) . 1_555 N
Os N1 3.011(11) . 1_555 N
Os N1 3.011(11) . 4_555 N
Os N1 3.011(11) . 12_565 N
Os N1 3.011(11) . -10_565 N
Os N2 3.247(7) . 1_555 N
Os N2 3.247(7) . 4_555 N
Os N2 3.247(7) . 12_565 N
Os N2 3.247(7) . -10_565 N
Os Cu2 2.19(4) . 1_555 N
Os Cu2 2.19(4) . 12_565 N
Os C1a 1.363(15) . 1_555 N
Os C1a 1.363(15) . 12_565 N
Os O1a 0.425(31) . 1_555 N
Os O1b 2.504(16) . 1_555 N
Os O1b 2.504(16) . 12_565 N
Os Cl2 3.301(10) . 1_555 N
Os Cl2 3.301(10) . 12_565 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Cu1 N1 88.08(29) 1_555 . 1_555 N
Cl1 Cu1 N1 88.08(29) 1_555 . 4_555 N
Cl1 Cu1 N1 88.08(29) 1_555 . 12_565 N
Cl1 Cu1 N1 88.08(29) 1_555 . -10_565 N
N1 Cu1 N1 92.77(21) 1_555 . 4_555 N
N1 Cu1 N1 176.2(6) 1_555 . 12_565 N
N1 Cu1 N1 87.11(21) 1_555 . -10_565 N
N1 Cu1 N1 87.11(21) 4_555 . 12_565 N
N1 Cu1 N1 176.2(6) 4_555 . -10_565 N
N1 Cu1 N1 92.77(21) 12_565 . -10_565 N
C2 C1 N2 123.53(30) 1_555 . 1_555 N
C2 C1 N2 123.53(30) 1_555 . 19_555 N
N2 C1 N2 112.9(6) 1_555 . 19_555 N
C1 C2 C3 118.77(33) 1_555 . 1_555 N
C1 C2 C3 118.77(33) 1_555 . 7_555 N
C3 C2 C3 122.4(7) 1_555 . 7_555 N
C2 C3 C2 117.6(7) 1_555 . 9_555 N
C2 C3 H1 121.22(33) 1_555 . 1_555 N
C2 C3 H1 121.22(33) 9_555 . 1_555 N
Cu1 Cl1 Cu1 180.0 1_555 . 10_555 N
Cu1 Cl1 Cu1 90.0 1_555 . 14_555 N
Cu1 Cl1 Cu1 90.0 1_555 . 19_555 N
Cu1 Cl1 Cu1 90.0 10_555 . 14_555 N
Cu1 Cl1 Cu1 90.0 10_555 . 19_555 N
Cu1 Cl1 Cu1 180.0 14_555 . 19_555 N
Cu1 N1 N1 122.38(25) 1_555 . 19_555 N
Cu1 N1 N2 128.2(4) 1_555 . 1_555 N
N1 N1 N2 109.41(21) 19_555 . 1_555 N
C1 N2 N1 104.1(4) 1_555 . 1_555 N
C1 N2 Cu2 159.8(13) 1_555 . 1_555 N
N1 N2 Cu2 94.6(11) 1_555 . 1_555 N
N2 Cu2 N2 117.0(14) 1_555 . 4_555 N
N2 Cu2 C1a 118.2(11) 1_555 . 1_555 N
N2 Cu2 O1b 119.8(8) 1_555 . 1_555 N
N2 Cu2 Cl2 117.9(11) 1_555 . 1_555 N
N2 Cu2 C1a 118.2(11) 4_555 . 1_555 N
N2 Cu2 O1b 119.8(8) 4_555 . 1_555 N
N2 Cu2 Cl2 117.9(11) 4_555 . 1_555 N
C1a Cu2 O1b 43.5(10) 1_555 . 1_555 N
C1a Cu2 Cl2 51.8(8) 1_555 . 1_555 N
O1b Cu2 Cl2 8.4(12) 1_555 . 1_555 N
Cu2 C1a O1a 114.0(19) 1_555 . 1_555 N
Cu2 C1a O1b 68.7(18) 1_555 . 1_555 N
Cu2 C1a Cl2 88.9(14) 1_555 . 1_555 N
Cu2 C1a Os 96.6(19) 1_555 . 1_555 N
O1a C1a O1b 177.2(13) 1_555 . 1_555 N
O1a C1a Cl2 157.1(22) 1_555 . 1_555 N
O1a C1a Os 17.4(13) 1_555 . 1_555 N
O1b C1a Cl2 20.1(21) 1_555 . 1_555 N
O1b C1a Os 165.4(16) 1_555 . 1_555 N
Cl2 C1a Os 174.5(21) 1_555 . 1_555 N
C1a O1a C1a 147.4(25) 1_555 . 12_565 N
C1a O1a Os 106.3(13) 1_555 . 1_555 N
C1a O1a Os 106.3(13) 12_565 . 1_555 N
Cu2 O1b C1a 67.8(18) 1_555 . 1_555 N
Cu2 O1b O1b 138.2(17) 1_555 . 13_555 N
Cu2 O1b Cl2 158(4) 1_555 . 1_555 N
C1a O1b O1b 154.1(13) 1_555 . 13_555 N
C1a O1b Cl2 135(4) 1_555 . 1_555 N
O1b O1b Cl2 19.4(34) 13_555 . 1_555 N
Cu2 Cl2 Cu2 113.1(29) 1_555 . 13_555 N
Cu2 Cl2 C1a 39.3(11) 1_555 . 1_555 N
Cu2 Cl2 C1a 152.3(28) 1_555 . 13_555 N
Cu2 Cl2 O1b 14.1(26) 1_555 . 1_555 N
Cu2 Cl2 O1b 127(4) 1_555 . 13_555 N
Cu2 Cl2 C1a 152.3(28) 13_555 . 1_555 N
Cu2 Cl2 C1a 39.3(11) 13_555 . 13_555 N
Cu2 Cl2 O1b 127(4) 13_555 . 1_555 N
Cu2 Cl2 O1b 14.1(26) 13_555 . 13_555 N
C1a Cl2 C1a 168.4(32) 1_555 . 13_555 N
C1a Cl2 O1b 25.2(20) 1_555 . 1_555 N
C1a Cl2 O1b 166(5) 1_555 . 13_555 N
C1a Cl2 O1b 166(5) 13_555 . 1_555 N
C1a Cl2 O1b 25.2(20) 13_555 . 13_555 N
O1b Cl2 O1b 141(7) 1_555 . 13_555 N
C1a Os C1a 112.6(16) 1_555 . 12_565 N
C1a Os O1a 56.3(8) 1_555 . 1_555 N
C1a Os O1a 56.3(8) 12_565 . 1_555 N

# Powder diffraction data for histogram  2
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT602_0P5CO2_FREECL_publ  
;
PROBLEM: Test for (Unreported) solvent accessible voids        ! Info 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT049_0P5CO2_FREECL_publ  
;
PROBLEM: Calculated Density less than 1.0 gcm-3 .........     0.9897 Check 
RESPONSE: This is expected as the material is porous.
;

_vrf_PLAT430_0P5CO2_FREECL_publ  
;
PROBLEM:  Short Inter D...A Contact  O1B    ..  O1B     ..       1.78 Ang. 
RESPONSE: The problem happens because the adsorbed carbon dioxide on the open metal sites are disordered and thus some atoms ostensibly are seemed to be close to each other.

;


# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;


_cell_measurement_theta_min      4.5
_cell_measurement_theta_max      160
_cell_measurement_reflns_used    639
_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Cu 16.608 0.7718 International_Tables_Vol_C
C 78.393 0.6648 International_Tables_Vol_C
Cl 5.304 0.9579 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 24.0 -0.3741 International_Tables_Vol_C
O 14.871 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.0782
_pd_proc_ls_prof_R_factor        0.0305
_pd_proc_ls_prof_wR_factor       0.0354
_pd_proc_ls_prof_wR_expected     0.0355
_refine_ls_R_Fsqd_factor         0.03713

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    685.137     2:   -127.077     3:    172.110     4:    25.0628    
      5:    80.6130     6:    7.25467     7:    51.4706     8:    5.18258    
      9:    26.0298    10:   -3.28640    11:    5.08910    12:   -3.54885    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  427.388 #2(GV)   = -290.569 #3(GW)   =   67.938
 #4(GP)   =   60.535 #5(LX)   =    0.000 #6(LY)   =   15.132
 #7(S/L)  =   0.0349 #8(H/L)  =   0.0256
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0005 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00050
_pd_proc_info_datetime           2016-02-13T16:21:16
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.503
_pd_proc_2theta_range_max        166.253
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
5650(160) 0.0 1439. .
5370(160) 0.0 1432. .
4500(150) 0.0 1426. .
4110(140) 0.0 1419. .
3570(130) 0.0 1412. .
3420(130) 0.0 1405. .
2950(120) 0.0 1399. .
2990(120) 0.0 1392. .
2400(110) 0.0 1386. .
2420(110) 0.0 1379. .
2240(100) 0.0 1373. .
2074(98) 0.0 1367. .
2051(98) 0.0 1360. .
1901(94) 0.0 1354. .
1667(88) 0.0 1348. .
1700(89) 0.0 1342. .
1733(90) 0.0 1336. .
1546(85) 0.0 1330. .
1648(88) 0.0 1324. .
1770(91) 0.0 1318. .
1634(87) 0.0 1312. .
1546(85) 0.0 1307. .
1574(86) 0.0 1301. .
1588(86) 0.0 1295. .
1564(86) 0.0 1290. .
1541(85) 0.0 1284. .
1705(89) 0.0 1279. .
1611(87) 0.0 1273. .
1620(87) 0.0 1268. .
1372(80) 0.0 1263. .
1475(83) 0.0 1257. .
1354(80) 0.0 1252. .
1330(79) 0.0 1247. .
1396(81) 0.0 1242. .
1307(78) 0.0 1237. .
1419(81) 0.0 1232. .
1349(79) 0.0 1227. .
1246(76) 0.0 1222. .
1120(72) 0.0 1217. .
1260(77) 0.0 1212. .
1157(74) 0.0 1207. .
1209(75) 0.0 1202. .
1246(76) 0.0 1198. .
1246(76) 0.0 1193. .
1190(75) 0.0 1189. .
1110(72) 0.0 1184. .
1096(72) 0.0 1179. .
1162(74) 0.0 1175. .
1092(71) 0.0 1171. .
1087(71) 0.0 1166. .
1110(72) 0.0 1162. .
1162(74) 0.0 1158. .
1036(70) 0.0 1153. .
1157(74) 0.0 1149. .
1124(72) 0.0 1145. .
1059(70) 0.0 1141. .
1050(70) 0.0 1137. .
1050(70) 0.0 1133. .
1050(70) 0.0 1129. .
1106(72) 0.0 1125. .
970(67) 0.0 1121. .
1040(70) 0.0002041 1117. 1117.
1003(68) 0.0002163 1113. 1113.
1129(73) 0.0001877 1109. 1109.
1087(71) 0.0001984 1105. 1109.
1054(70) 0.0002041 1102. 1105.
1092(71) 0.0001984 1098. 1102.
1017(69) 0.0002100 1094. 1099.
1092(71) 0.0001984 1091. 1095.
1115(72) 0.0001929 1087. 1092.
1120(72) 0.0001929 1084. 1089.
1012(69) 0.0002100 1080. 1086.
1073(71) 0.0001984 1077. 1084.
1078(71) 0.0001984 1073. 1081.
993(68) 0.0002163 1070. 1080.
984(68) 0.0002163 1066. 1083.
1148(73) 0.0001877 1063. 1092.
1302(78) 0.0001644 1060. 1113.
1284(77) 0.0001687 1056. 1153.
1415(81) 0.0001524 1053. 1217.
1597(86) 0.0001352 1050. 1306.
1578(86) 0.0001352 1047. 1419.
1527(84) 0.0001417 1044. 1553.
1723(90) 0.0001235 1041. 1706.
1901(94) 0.0001132 1037. 1879.
1770(91) 0.0001208 1034. 2074.
2310(100) 0.0000925 1031. 2295.
2290(100) 0.0000943 1028. 2548.
2730(110) 0.0000783 1025. 2841.
3210(120) 0.0000672 1023. 3189.
3630(130) 0.0000592 1020. 3611.
4190(140) 0.0000510 1017. 4144.
5220(160) 0.0000411 1014. 4847.
5980(170) 0.0000359 1011. 5808.
7850(190) 0.0000271 1008. 7103.
9130(210) 0.0000233 1006. 8684.
11290(230) 0.0000189 1003. 10228.
12090(240) 0.0000177 1000. 11131.
12520(240) 0.0000171 998. 10796.
10480(220) 0.0000205 995. 9116.
6960(120) 0.0000650 992. 6665.
4630(100) 0.0000980 990. 4305.
2887(80) 0.0001562 987. 2607.
1743(62) 0.0002601 985. 1654.
1237(52) 0.000370 982. 1228.
1080(48) 0.000434 980. 1072.
1062(48) 0.000434 977. 1021.
1128(49) 0.000416 975. 1004.
950(45) 0.000494 973. 995.
1025(47) 0.000453 970. 989.
976(46) 0.000473 968. 984.
970(46) 0.000473 966. 980.
966(46) 0.000473 963. 976.
993(46) 0.000473 961. 972.
962(45) 0.000494 959. 968.
991(46) 0.000473 957. 965.
975(46) 0.000473 954. 962.
921(44) 0.000517 952. 963.
932(45) 0.000494 950. 961.
794(41) 0.000595 948. 958.
857(43) 0.000541 946. 956.
825(42) 0.000567 944. 954.
877(43) 0.000541 942. 952.
884(43) 0.000541 940. 950.
905(44) 0.000517 938. 948.
904(44) 0.000517 936. 942.
935(45) 0.000494 934. 941.
837(42) 0.000567 932. 940.
939(45) 0.000494 930. 939.
921(44) 0.000517 928. 938.
868(43) 0.000541 926. 937.
997(46) 0.000473 924. 936.
948(45) 0.000494 922. 936.
919(44) 0.000517 920. 937.
954(45) 0.000494 919. 941.
1006(46) 0.000473 917. 951.
1086(48) 0.000434 915. 975.
1158(50) 0.000400 913. 1025.
1194(51) 0.000384 912. 1116.
1377(55) 0.0003306 910. 1259.
1564(58) 0.0002973 908. 1462.
1788(63) 0.0002520 907. 1727.
1933(65) 0.0002367 905. 2057.
2339(72) 0.0001929 903. 2464.
2801(79) 0.0001602 902. 2971.
3431(87) 0.0001321 900. 3629.
4295(97) 0.0001063 899. 4522.
5740(110) 0.0000783 897. 5749.
7320(130) 0.0000610 895. 7349.
9150(140) 0.0000489 894. 9128.
10370(150) 0.0000433 892. 10548.
10580(150) 0.0000422 891. 10894.
9620(150) 0.0000469 889. 9761.
7290(130) 0.0000620 888. 7494.
5010(110) 0.0000907 887. 4982.
3250(84) 0.0001417 885. 2999.
1827(63) 0.0002520 884. 1803.
1315(53) 0.000356 882. 1234.
971(46) 0.000473 881. 1021.
859(43) 0.000541 880. 949.
893(44) 0.000517 878. 925.
852(43) 0.000541 877. 915.
902(44) 0.000517 876. 909.
899(44) 0.000517 874. 904.
812(41) 0.000595 873. 900.
795(41) 0.000595 872. 897.
868(43) 0.000541 870. 894.
808(41) 0.000595 869. 892.
838(42) 0.000567 868. 890.
910(44) 0.000517 867. 888.
869(43) 0.000541 866. 887.
915(44) 0.000517 864. 886.
804(41) 0.000595 863. 886.
922(44) 0.000517 862. 886.
897(44) 0.000517 861. 886.
874(43) 0.000541 860. 887.
921(44) 0.000517 859. 889.
938(45) 0.000494 858. 894.
913(44) 0.000517 856. 904.
1031(47) 0.000453 855. 924.
1120(49) 0.000416 854. 979.
1293(53) 0.000356 853. 1089.
1472(57) 0.0003078 852. 1280.
1662(60) 0.0002778 851. 1580.
2069(67) 0.0002228 850. 2006.
2381(72) 0.0001929 849. 2583.
3080(82) 0.0001487 848. 3359.
4194(96) 0.0001085 847. 4426.
5700(110) 0.0000783 846. 5905.
7570(130) 0.0000592 845. 7859.
9910(150) 0.0000450 844. 10078.
11890(160) 0.0000376 843. 11922.
12300(170) 0.0000363 842. 12500.
11000(160) 0.0000406 841. 11270.
8230(140) 0.0000549 840. 8622.
5420(110) 0.0000842 840. 5653.
2930(110) 0.0000826 839. 3312.
1758(85) 0.0001384 838. 1910.
1154(68) 0.0002163 837. 1252.
962(62) 0.0002601 836. 1002.
897(43) 0.000541 835. 920.
884(43) 0.000541 834. 891.
820(41) 0.000595 834. 879.
829(41) 0.000595 833. 870.
855(42) 0.000567 832. 864.
960(44) 0.000517 831. 858.
924(44) 0.000517 830. 854.
855(42) 0.000567 830. 850.
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728(35) 0.000816 725.8 727.6
732(34) 0.000865 725.6 727.3
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720(34) 0.000865 724.8 726.7
761(35) 0.000816 724.6 726.5
767(35) 0.000816 724.4 726.4
717(34) 0.000865 724.2 726.3
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781(35) 0.000816 723.8 726.1
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716(34) 0.000865 722.1 727.5
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751(35) 0.000816 719.7 751.5
776(35) 0.000816 719.5 741.6
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782(35) 0.000816 719.0 750.0
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771(35) 0.000816 713.1 733.3
725(34) 0.000865 712.9 731.0
696(33) 0.000918 712.7 729.4
701(33) 0.000918 712.5 728.3
710(34) 0.000865 712.3 727.8
682(33) 0.000918 712.1 727.7
722(34) 0.000865 711.9 728.2
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714(34) 0.000865 711.5 732.9
745(34) 0.000865 711.3 741.4
755(35) 0.000816 711.1 763.2
768(35) 0.000816 710.9 814.3
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737(34) 0.000865 706.5 733.9
751(35) 0.000816 706.3 724.3
697(33) 0.000918 706.1 720.6
745(34) 0.000865 705.9 719.3
740(34) 0.000865 705.7 718.9
694(33) 0.000918 705.5 719.0
741(27) 0.001372 705.3 719.5
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643(23) 0.001890 569.0 662.5
639(23) 0.001890 569.8 664.2
649(23) 0.001890 570.7 666.0
687(24) 0.001736 571.5 668.0
665(23) 0.001890 572.3 670.2
666(23) 0.001890 573.2 672.6
682(24) 0.001736 574.0 675.2
673(23) 0.001890 574.9 678.0
678(24) 0.001736 575.8 680.9
681(24) 0.001736 576.7 684.1
700(24) 0.001736 577.5 687.4
729(24) 0.001736 578.5 690.9
687(24) 0.001736 579.4 694.5
693(24) 0.001736 580.3 698.3
717(24) 0.001736 581.2 702.3
696(24) 0.001736 582.2 706.4
708(24) 0.001736 583.1 710.6
720(24) 0.001736 584.1 714.9
737(24) 0.001736 585.1 719.4
756(25) 0.001600 586.0 724.0
742(25) 0.001600 587.0 728.7
729(24) 0.001736 588.0 733.5
745(25) 0.001600 589.1 738.3
752(25) 0.001600 590.1 743.2
761(25) 0.001600 591.1 748.2
772(26) 0.001479 592.2 753.2
754(25) 0.001600 593.2 758.2
773(26) 0.001479 594.3 763.2
742(25) 0.001600 595.4 768.3
773(26) 0.001479 596.5 773.3
790(26) 0.001479 597.6 778.3
770(26) 0.001479 598.7 783.3
790(26) 0.001479 599.8 788.3
781(26) 0.001479 600.9 793.2
826(26) 0.001479 602.1 798.0
799(26) 0.001479 603.2 802.8
810(26) 0.001479 604.4 807.4
814(26) 0.001479 605.6 812.0
809(26) 0.001479 606.8 816.6
835(27) 0.001372 608.0 821.0
831(27) 0.001372 609.2 825.3
825(26) 0.001479 610.4 829.5
815(26) 0.001479 611.7 833.6
797(26) 0.001479 612.9 837.5
833(27) 0.001372 614.2 841.4
837(27) 0.001372 615.5 845.1
838(27) 0.001372 616.7 848.7
817(26) 0.001479 618.0 852.2
834(27) 0.001372 619.4 855.6
855(27) 0.001372 620.7 858.8
872(27) 0.001372 622.0 861.9
863(27) 0.001372 623.4 864.9
838(27) 0.001372 624.7 867.7
890(27) 0.001372 626.1 870.5
852(27) 0.001372 627.5 873.1
871(27) 0.001372 628.9 875.6
864(27) 0.001372 630.3 878.0
860(27) 0.001372 631.7 880.3
897(28) 0.001276 633.2 882.5
865(27) 0.001372 634.6 884.6
862(27) 0.001372 636.1 886.7
877(27) 0.001372 637.6 888.6
895(28) 0.001276 639.1 890.5
930(28) 0.001276 640.6 892.4
908(28) 0.001276 642.1 894.2
906(28) 0.001276 643.6 895.9
934(28) 0.001276 645.2 897.7
891(27) 0.001372 646.7 899.3
871(27) 0.001372 648.3 901.0
902(28) 0.001276 649.9 902.6
911(28) 0.001276 651.5 904.2
858(27) 0.001372 653.1 905.8
947(28) 0.001276 654.8 907.3
919(28) 0.001276 656.4 908.9
945(28) 0.001276 658.1 910.4
932(28) 0.001276 659.8 911.8
936(28) 0.001276 661.4 913.3
930(28) 0.001276 663.2 914.7
919(28) 0.001276 664.9 916.0
895(27) 0.001372 666.6 917.3
875(27) 0.001372 668.4 918.6
931(28) 0.001276 670.1 919.8
940(28) 0.001276 671.9 920.9
922(28) 0.001276 673.7 922.0
938(28) 0.001276 675.5 923.0
945(28) 0.001276 677.3 923.9
929(28) 0.001276 679.2 924.7
923(28) 0.001276 681.0 925.4
920(28) 0.001276 682.9 926.0
911(28) 0.001276 684.8 926.5
902(28) 0.001276 686.7 926.9
934(28) 0.001276 688.6 927.1
909(28) 0.001276 690.6 927.3
894(27) 0.001372 692.5 927.3
883(27) 0.001372 694.5 927.2
935(28) 0.001276 696.5 927.0
954(28) 0.001276 698.5 926.6
905(28) 0.001276 700.5 926.2
913(28) 0.001276 702.5 925.6
935(28) 0.001276 704.6 924.9
928(28) 0.001276 706.7 924.2
929(28) 0.001276 708.8 923.3
952(28) 0.001276 710.9 922.4
950(28) 0.001276 713.0 921.4
968(29) 0.001189 715.1 920.4
915(28) 0.001276 717.3 919.2
879(27) 0.001372 719.4 918.1
937(28) 0.001276 721.6 916.9
920(28) 0.001276 723.8 915.7
945(28) 0.001276 726.1 914.5
923(28) 0.001276 728.3 913.2
896(28) 0.001276 730.6 912.0
905(28) 0.001276 732.8 910.8
916(28) 0.001276 735.1 909.6
945(28) 0.001276 737.5 908.4
935(28) 0.001276 739.8 907.3
902(28) 0.001276 742.1 906.1
949(28) 0.001276 744.5 905.1
945(28) 0.001276 746.9 904.1
920(28) 0.001276 749.3 903.1
894(27) 0.001372 751.7 902.3
952(28) 0.001276 754.2 901.4
956(28) 0.001276 756.6 900.7
904(28) 0.001276 759.1 900.0
862(39) 0.000657 762. 899.
880(40) 0.000625 764. 899.
878(40) 0.000625 767. 899.
890(40) 0.000625 769. 898.
951(41) 0.000595 772. 898.
940(41) 0.000595 774. 898.
888(40) 0.000625 777. 898.
829(39) 0.000657 780. 898.
864(39) 0.000657 782. 898.
920(40) 0.000625 785. 898.
878(40) 0.000625 788. 899.
907(40) 0.000625 790. 899.
916(40) 0.000625 793. 900.
934(41) 0.000595 796. 901.
941(41) 0.000595 799. 901.
930(41) 0.000595 801. 902.
935(41) 0.000595 804. 903.
911(40) 0.000625 807. 905.
911(40) 0.000625 810. 906.
910(40) 0.000625 813. 907.
867(39) 0.000657 816. 909.
924(40) 0.000625 819. 910.
903(40) 0.000625 822. 912.
932(41) 0.000595 825. 914.
936(41) 0.000595 828. 916.
903(40) 0.000625 831. 918.
922(40) 0.000625 834. 920.
882(40) 0.000625 837. 922.
923(40) 0.000625 840. 924.
921(40) 0.000625 843. 927.
902(40) 0.000625 846. 929.
894(40) 0.000625 849. 932.
920(40) 0.000625 852. 935.
929(41) 0.000595 855. 937.
965(41) 0.000595 859. 940.
922(40) 0.000625 862. 943.
935(41) 0.000595 865. 947.
943(41) 0.000595 868. 950.
960(41) 0.000595 872. 953.
945(41) 0.000595 875. 957.
942(41) 0.000595 878. 960.
920(40) 0.000625 882. 964.
944(41) 0.000595 885. 968.
968(41) 0.000595 889. 971.
986(42) 0.000567 892. 975.
995(42) 0.000567 895. 979.
977(41) 0.000595 899. 983.
1001(42) 0.000567 902. 988.
928(41) 0.000595 906. 992.
982(42) 0.000567 910. 996.
966(41) 0.000595 913. 1001.
1044(43) 0.000541 917. 1005.
965(41) 0.000595 920. 1010.
978(42) 0.000567 924. 1015.
949(41) . . .
1027(42) . . .
1074(43) . . .
1027(42) . . .
992(42) . . .
1025(42) . . .
1001(42) . . .
1048(43) . . .
1032(43) . . .
1011(42) . . .
1011(42) . . .
1017(42) . . .
1104(44) . . .
1047(43) . . .
1037(43) . . .
1025(42) . . .
1084(44) . . .
1066(43) . . .
1091(44) . . .
1102(44) . . .
1084(44) . . .
1102(44) . . .
1097(44) . . .
1104(44) . . .
1039(43) . . .
1104(44) . . .
1096(44) . . .
1047(43) . . .
1170(45) . . .
1104(44) . . .
1190(45) . . .
1123(44) . . .
1096(44) . . .
1098(44) . . .
1183(45) . . .
1143(45) . . .
1190(45) . . .
1134(44) . . .
1139(45) . . .
1076(43) . . .
1146(45) . . .
1103(44) . . .
1118(44) . . .
1233(46) . . .
1197(46) . . .
1159(45) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296


_reflns_number_total             639
_reflns_limit_h_min              1
_reflns_limit_h_max              17
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.052
_reflns_d_resolution_low         18.530
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1P5_FINAL_publ
_database_code_depnum_ccdc_archive 'CCDC 1582008'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-05-25T14:04|1P5_FINAL|wendy|bt1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-05-25T14:04

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.07
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     54
_refine_ls_goodness_of_fit_all   1.26
_refine_ls_number_restraints     21
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10


_cell_measurement_theta_min      4
_cell_measurement_theta_max      160

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from Z:/queen/Desktop/1P5CO2_NIST_final/0P5CO2.EXP'
_cell_length_a                   18.8952(4)
_cell_length_b                   18.8952
_cell_length_c                   18.8952
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6746.1(4)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Fe Fe1 0.1351(5) 0.5 0.0 1.0 Uiso 0.002(2) 12
C C1 0.1508(4) 0.3368(5) -0.1508(4) 1.0 Uiso 0.0190(12) 24
C C2 0.1795(4) 0.2707(5) -0.1795(4) 1.0 Uiso 0.0190(12) 24
C C3 0.24188(34) 0.24188(34) -0.1473(5) 1.0 Uiso 0.0190(12) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.027(5) 3
N N1 0.13076(26) 0.42088(25) -0.08032(27) 1.0 Uiso 0.0211(7) 48
N N2 0.17522(26) 0.36653(27) -0.09042(24) 1.0 Uiso 0.0211(7) 48
H H1 0.2616(6) 0.2616(6) -0.1100(8) 1.0 Uiso 0.026(5) 24
Fe Fe2 0.2679(7) 0.0 0.0 0.1793 Uiso 0.10322 6
O Os 0.2508(7) 0.5 0.0 0.6471 Uiso 0.03508 12
C Cs 0.3090(11) 0.5 0.0465(12) 0.3236 Uiso 0.03508 24
O O1a 0.2607(8) 0.5 0.0 0.35765 Uiso 0.09372 12
O O1b 0.3048(35) 0.3852(16) 0.0 0.17882 Uiso 0.10422 24
C C1a 0.2856(20) 0.4437(11) 0.0 0.17882 Uiso 0.10422 24
H Hsa 0.2909(22) 0.5 0.0951(19) 0.3236 Uiso 0.10908 24
H Hsb 0.3433(16) 0.4598(17) 0.0317(25) 0.3236 Uiso 0.10908 48
C C2a 0.0 0.2766(12) 0.0398(10) 0.205 Uiso 0.015(6) 24
O O2b 0.0 0.2309(15) 0.0796(19) 0.205 Uiso 0.021(6) 24
O O2a 0.0 0.3206(14) 0.0 0.82 Uiso 0.013(6) 6
C C3a 0.1590(8) 0.1590(8) 0.0 0.67(1) Uiso 0.06(1) 12
O O3a 0.0989(10) 0.1590(18) 0.0 0.33(1) Uiso 0.06(1) 24
O O3b 0.2179(10) 0.1580(16) 0.0 0.33(1) Uiso 0.06(1) 24
C C4a 0.1007(23) 0.0483(26) 0.0483(26) 0.14(1) Uiso 0.06(2) 24
O O4a 0.144(4) 0.0787(15) 0.0787(15) 0.14(1) Uiso 0.06(2) 24
O O4b 0.0552(24) 0.0187(20) 0.0187(20) 0.14(1) Uiso 0.06(2) 24

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C33.47 H15.77 Cl Fe4.36 N32 O16.34'
_chemical_formula_weight         1406.39
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Fe1 Fe1 5.107(17) . 10_555 N
Fe1 Fe1 3.611(12) . 14_555 N
Fe1 Fe1 3.611(12) . 19_555 N
Fe1 Cl1 2.554(9) . 1_555 N
Fe1 N1 2.132(4) . 1_555 N
Fe1 N1 2.132(4) . 4_555 N
Fe1 N1 2.132(4) . 12_565 N
Fe1 N1 3.068(6) . 17_555 N
Fe1 N1 3.068(6) . 19_555 N
Fe1 N1 3.068(6) . 23_565 N
Fe1 N1 2.132(4) . -10_565 N
Fe1 N1 3.068(6) . -14_565 N
Fe1 N2 3.139(5) . 1_555 N
Fe1 N2 3.139(5) . 4_555 N
Fe1 N2 3.139(5) . 12_565 N
Fe1 N2 3.139(5) . -10_565 N
Fe1 Fe2 5.075(12) . 2_555 N
Fe1 Fe2 5.075(12) . 11_565 N
Fe1 Os 2.186(11) . 1_555 N
Fe1 Cs 3.401(17) . 1_555 N
Fe1 Cs 3.401(17) . 4_555 N
Fe1 O1a 2.373(12) . 1_555 N
Fe1 O1b 3.87(4) . 1_555 N
Fe1 O1b 3.87(4) . 12_565 N
Fe1 C1a 3.035(32) . 1_555 N
Fe1 C1a 3.035(32) . 12_565 N
Fe1 Hsa 3.449(33) . 1_555 N
Fe1 Hsa 3.449(33) . 4_555 N
C1 C2 1.465(13) . 1_555 N
C1 N1 2.108(9) . 1_555 N
C1 N1 2.108(9) . 19_555 N
C1 N2 1.353(7) . 1_555 N
C1 N2 1.353(7) . 19_555 N
C2 C1 1.465(13) . 1_555 N
C2 C3 1.434(6) . 1_555 N
C2 C3 1.434(6) . 7_555 N
C3 C2 1.434(6) . 1_555 N
C3 C2 1.434(6) . 9_555 N
C3 H1 0.880(17) . 1_555 N
Cl1 Fe1 2.554(9) . 1_555 N
Cl1 Fe1 2.554(9) . 10_555 N
Cl1 Fe1 2.554(9) . 14_555 N
Cl1 Fe1 2.554(9) . 19_555 N
Cl1 N1 3.262(5) . 1_555 N
Cl1 N1 3.262(5) . 4_555 N
Cl1 N1 3.262(5) . 10_555 N
Cl1 N1 3.262(5) . 12_565 N
Cl1 N1 3.262(5) . 14_555 N
Cl1 N1 3.262(5) . 17_555 N
Cl1 N1 3.262(5) . 19_555 N
Cl1 N1 3.262(5) . 23_565 N
Cl1 N1 3.262(5) . -1_565 N
Cl1 N1 3.262(5) . -4_565 N
Cl1 N1 3.262(5) . -10_565 N
Cl1 N1 3.262(5) . -12_555 N
Cl1 N1 3.262(5) . -14_565 N
Cl1 N1 3.262(5) . -17_565 N
Cl1 N1 3.262(5) . -19_565 N
Cl1 N1 3.262(5) . -23_555 N
Cl1 Fe2 4.386(13) . 2_555 N
Cl1 Fe2 4.386(13) . 11_565 N
Cl1 O2a 3.390(27) . 1_555 N
Cl1 O2a 3.390(27) . 12_565 N
N1 Fe1 2.132(4) . 1_555 N
N1 Fe1 3.068(6) . 19_555 N
N1 C1 2.108(9) . 1_555 N
N1 Cl1 3.262(5) . 1_555 N
N1 N1 1.348(11) . 19_555 N
N1 N2 1.340(6) . 1_555 N
N2 Fe1 3.139(5) . 1_555 N
N2 C1 1.353(7) . 1_555 N
N2 N1 1.340(6) . 1_555 N
H1 C3 0.880(17) . 1_555 N
Fe2 Fe1 5.075(12) . 3_555 N
Fe2 Fe1 5.075(12) . 9_555 N
Fe2 Fe1 5.075(12) . 13_555 N
Fe2 Fe1 5.075(12) . 24_555 N
Fe2 Cl1 4.386(13) . 3_555 N
Fe2 C2a 0.769(19) . 3_555 N
Fe2 C2a 0.769(19) . 6_555 N
Fe2 C2a 0.769(19) . 13_555 N
Fe2 C2a 0.769(19) . 16_555 N
Fe2 O2b 1.658(30) . 3_555 N
Fe2 O2b 1.658(30) . 6_555 N
Fe2 O2b 1.658(30) . 13_555 N
Fe2 O2b 1.658(30) . 16_555 N
Fe2 O2a 0.996(30) . 3_555 N
Fe2 C3a 3.641(8) . 1_555 N
Fe2 C3a 3.641(8) . 3_555 N
Fe2 C3a 3.641(8) . 9_555 N
Fe2 C3a 3.641(8) . 12_555 N
Fe2 O3a 2.780(25) . 3_555 N
Fe2 O3a 2.780(25) . 9_555 N
Fe2 O3a 2.780(25) . 13_555 N
Fe2 O3a 2.780(25) . 24_555 N
Fe2 O3b 3.131(28) . 1_555 N
Fe2 O3b 3.131(28) . 12_555 N
Fe2 O3b 3.131(28) . 15_555 N
Fe2 O3b 3.131(28) . 21_555 N
Fe2 C4a 3.41(6) . 1_555 N
Fe2 C4a 3.41(6) . 4_555 N
Fe2 C4a 3.41(6) . 12_555 N
Fe2 C4a 3.41(6) . 18_555 N
Fe2 O4a 3.14(7) . 1_555 N
Fe2 O4a 3.14(7) . 4_555 N
Fe2 O4a 3.14(7) . 12_555 N
Fe2 O4a 3.14(7) . 18_555 N
Fe2 O4b 4.05(5) . 1_555 N
Fe2 O4b 4.05(5) . 4_555 N
Fe2 O4b 4.05(5) . 12_555 N
Fe2 O4b 4.05(5) . 18_555 N
Os Fe1 2.186(11) . 1_555 N
Os Cs 1.407(12) . 1_555 N
Os Cs 1.407(12) . 4_555 N
Os O1a 0.187(17) . 1_555 N
Os C1a 1.250(16) . 1_555 N
Os C1a 1.250(16) . 12_565 N
Cs Fe1 3.401(17) . 1_555 N
Cs Os 1.407(12) . 1_555 N
Cs Cs 1.76(5) . 4_555 N
Cs O1a 1.266(17) . 1_555 N
Cs C1a 1.449(29) . 1_555 N
Cs C1a 1.449(29) . 12_565 N
Cs Hsa 0.98(4) . 1_555 N
Cs Hsb 1.036(6) . 1_555 N
Cs Hsb 1.036(6) . -10_565 N
O1a Fe1 2.373(12) . 1_555 N
O1a Os 0.187(17) . 1_555 N
O1a Cs 1.266(17) . 1_555 N
O1a Cs 1.266(17) . 4_555 N
O1a C1a 1.163(12) . 1_555 N
O1a C1a 1.163(12) . 12_565 N
O1b Fe1 3.87(4) . 1_555 N
O1b O1b 2.15(7) . 13_555 N
O1b C1a 1.163(13) . 1_555 N
C1a Fe1 3.035(32) . 1_555 N
C1a Os 1.250(16) . 1_555 N
C1a Cs 1.449(29) . 1_555 N
C1a Cs 1.449(29) . 4_555 N
C1a O1a 1.163(12) . 1_555 N
C1a O1b 1.163(13) . 1_555 N
C1a C1a 2.13(4) . 12_565 N
C1a Hsb 1.28(5) . 1_555 N
C1a Hsb 1.28(5) . 4_555 N
Hsa Fe1 3.449(33) . 1_555 N
Hsa Cs 0.98(4) . 1_555 N
Hsa Hsb 1.73(4) . 1_555 N
Hsa Hsb 1.73(4) . -10_565 N
Hsb Cs 1.036(6) . 1_555 N
Hsb C1a 1.28(5) . 1_555 N
Hsb Hsa 1.73(4) . 1_555 N
Hsb Hsb 1.20(10) . 4_555 N
Hsb Hsb 1.93(9) . 12_565 N
Hsb Hsb 1.52(6) . -10_565 N
C2a Fe2 0.769(19) . 2_555 N
C2a C2a 1.50(4) . 4_555 N
C2a C2a 1.063(27) . 14_555 N
C2a C2a 1.063(27) . 17_555 N
C2a O2b 1.146(12) . 1_555 N
C2a O2b 1.890(29) . 14_555 N
C2a O2b 1.890(29) . 17_555 N
C2a O2a 1.120(12) . 1_555 N
O2b Fe2 1.658(30) . 2_555 N
O2b C2a 1.146(12) . 1_555 N
O2b C2a 1.890(29) . 14_555 N
O2b C2a 1.890(29) . 17_555 N
O2b O2b 2.13(5) . 14_555 N
O2b O2b 2.13(5) . 17_555 N
O2b C3a 2.024(26) . 2_555 N
O2b O3a 1.41(4) . 14_555 N
O2b O3b 1.50(4) . 2_555 N
O2a Cl1 3.390(27) . 1_555 N
O2a Fe2 0.996(30) . 2_555 N
O2a C2a 1.120(12) . 1_555 N
O2a C2a 1.120(12) . 4_555 N
O2a C2a 1.120(12) . 14_555 N
O2a C2a 1.120(12) . 17_555 N
C3a Fe2 3.641(8) . 1_555 N
C3a Fe2 3.641(8) . 2_555 N
C3a O2b 2.024(26) . 3_555 N
C3a O2b 2.024(26) . 14_555 N
C3a O3a 1.136(12) . 1_555 N
C3a O3a 1.136(12) . 13_555 N
C3a O3b 1.112(12) . 1_555 N
C3a O3b 1.112(12) . 13_555 N
C3a O4a 2.143(14) . 1_555 N
C3a O4a 2.143(14) . 2_555 N
C3a O4a 2.143(14) . 4_555 N
C3a O4a 2.143(14) . 16_555 N
O3a Fe2 2.780(25) . 2_555 N
O3a O2b 1.41(4) . 14_555 N
O3a C3a 1.136(12) . 1_555 N
O3a O3a 1.61(5) . 13_555 N
O3a O3b 1.58(4) . 13_555 N
O3a C4a 1.72(4) . 2_555 N
O3a C4a 1.72(4) . 16_555 N
O3a O4a 1.560(30) . 2_555 N
O3a O4a 1.560(30) . 16_555 N
O3b Fe2 3.131(28) . 1_555 N
O3b O2b 1.50(4) . 3_555 N
O3b C3a 1.112(12) . 1_555 N
O3b O3a 1.58(4) . 13_555 N
O3b O3b 1.60(4) . 13_555 N
C4a Fe2 3.41(6) . 1_555 N
C4a O3a 1.72(4) . 3_555 N
C4a O3a 1.72(4) . 13_555 N
C4a C4a 1.40(11) . 2_555 N
C4a C4a 1.40(11) . 3_555 N
C4a C4a 1.82(10) . 4_555 N
C4a C4a 1.82(10) . 18_555 N
C4a O4a 1.158(13) . 1_555 N
C4a O4a 1.95(7) . 2_555 N
C4a O4a 1.95(7) . 3_555 N
C4a O4b 1.168(12) . 1_555 N
C4a O4b 1.65(6) . 2_555 N
C4a O4b 1.65(6) . 3_555 N
C4a O4b 1.63(6) . 4_555 N
C4a O4b 2.004(32) . 6_555 N
C4a O4b 1.98(10) . 12_555 N
C4a O4b 2.004(32) . 16_555 N
C4a O4b 1.63(6) . 18_555 N
O4a Fe2 3.14(7) . 1_555 N
O4a C3a 2.143(14) . 1_555 N
O4a C3a 2.143(14) . 3_555 N
O4a O3a 1.560(30) . 3_555 N
O4a O3a 1.560(30) . 13_555 N
O4a C4a 1.158(13) . 1_555 N
O4a C4a 1.95(7) . 2_555 N
O4a C4a 1.95(7) . 3_555 N
O4a O4a 1.75(12) . 2_555 N
O4a O4a 1.75(12) . 3_555 N
O4b Fe2 4.05(5) . 1_555 N
O4b C4a 1.168(12) . 1_555 N
O4b C4a 1.65(6) . 2_555 N
O4b C4a 1.65(6) . 3_555 N
O4b C4a 1.63(6) . 4_555 N
O4b C4a 2.004(32) . 6_555 N
O4b C4a 1.98(10) . 12_555 N
O4b C4a 2.004(32) . 16_555 N
O4b C4a 1.63(6) . 18_555 N
O4b O4b 0.98(9) . 2_555 N
O4b O4b 0.98(9) . 3_555 N
O4b O4b 0.71(7) . 4_555 N
O4b O4b 1.56(6) . 5_555 N
O4b O4b 1.20(5) . 6_555 N
O4b O4b 1.71(6) . 7_555 N
O4b O4b 1.71(6) . 8_555 N
O4b O4b 1.71(6) . 9_555 N
O4b O4b 1.97(7) . 11_555 N
O4b O4b 1.00(11) . 12_555 N
O4b O4b 1.20(5) . 16_555 N
O4b O4b 1.56(6) . 17_555 N
O4b O4b 0.71(7) . 18_555 N
O4b O4b 1.97(7) . 19_555 N
O4b O4b 1.71(6) . 24_555 N
O4b O4b 2.10(8) . -2_555 N
O4b O4b 2.10(8) . -3_555 N
O4b O4b 1.56(6) . -7_555 N
O4b O4b 1.56(6) . -8_555 N
O4b O4b 2.09(9) . -12_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Fe1 N1 87.77(29) 1_555 . 1_555 N
Cl1 Fe1 N1 87.77(29) 1_555 . 4_555 N
Cl1 Fe1 N1 87.77(29) 1_555 . 12_565 N
Cl1 Fe1 N1 87.77(29) 1_555 . -10_565 N
N1 Fe1 N1 90.78(28) 1_555 . 4_555 N
N1 Fe1 N1 175.5(6) 1_555 . 12_565 N
N1 Fe1 N1 89.05(28) 1_555 . -10_565 N
N1 Fe1 N1 89.05(28) 4_555 . 12_565 N
N1 Fe1 N1 175.5(6) 4_555 . -10_565 N
N1 Fe1 N1 90.78(28) 12_565 . -10_565 N
C2 C1 N2 122.7(4) 1_555 . 1_555 N
C2 C1 N2 122.7(4) 1_555 . 19_555 N
N2 C1 N2 113.7(9) 1_555 . 19_555 N
C1 C2 C3 118.1(5) 1_555 . 1_555 N
C1 C2 C3 118.1(5) 1_555 . 7_555 N
C3 C2 C3 123.6(10) 1_555 . 7_555 N
C2 C3 C2 116.4(9) 1_555 . 9_555 N
C2 C3 H1 121.8(5) 1_555 . 1_555 N
C2 C3 H1 121.8(5) 9_555 . 1_555 N
Fe1 Cl1 Fe1 180.0 1_555 . 10_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 1_555 . 19_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 14_555 N
Fe1 Cl1 Fe1 90.0 10_555 . 19_555 N
Fe1 Cl1 Fe1 180.0 14_555 . 19_555 N
Fe1 N1 N1 122.06(26) 1_555 . 19_555 N
Fe1 N1 N2 127.9(4) 1_555 . 1_555 N
N1 N1 N2 110.03(31) 19_555 . 1_555 N
C1 N2 N1 103.0(5) 1_555 . 1_555 N
C2a Fe2 C2a 155(4) 3_555 . 6_555 N
C2a Fe2 C2a 87.3(8) 3_555 . 13_555 N
C2a Fe2 C2a 87.3(8) 3_555 . 16_555 N
C2a Fe2 O2b 37.4(18) 3_555 . 3_555 N
C2a Fe2 O2b 167.5(27) 3_555 . 6_555 N
C2a Fe2 O2b 95.2(7) 3_555 . 13_555 N
C2a Fe2 O2b 95.2(7) 3_555 . 16_555 N
C2a Fe2 O2a 77.6(20) 3_555 . 3_555 N
C2a Fe2 C2a 87.3(8) 6_555 . 13_555 N
C2a Fe2 C2a 87.3(8) 6_555 . 16_555 N
C2a Fe2 O2b 167.5(27) 6_555 . 3_555 N
C2a Fe2 O2b 37.4(18) 6_555 . 6_555 N
C2a Fe2 O2b 95.2(7) 6_555 . 13_555 N
C2a Fe2 O2b 95.2(7) 6_555 . 16_555 N
C2a Fe2 O2a 77.6(20) 6_555 . 3_555 N
C2a Fe2 C2a 155(4) 13_555 . 16_555 N
C2a Fe2 O2b 95.2(7) 13_555 . 3_555 N
C2a Fe2 O2b 95.2(7) 13_555 . 6_555 N
C2a Fe2 O2b 37.4(18) 13_555 . 13_555 N
C2a Fe2 O2b 167.5(27) 13_555 . 16_555 N
C2a Fe2 O2a 77.6(20) 13_555 . 3_555 N
C2a Fe2 O2b 95.2(7) 16_555 . 3_555 N
C2a Fe2 O2b 95.2(7) 16_555 . 6_555 N
C2a Fe2 O2b 167.5(27) 16_555 . 13_555 N
C2a Fe2 O2b 37.4(18) 16_555 . 16_555 N
C2a Fe2 O2a 77.6(20) 16_555 . 3_555 N
O2b Fe2 O2b 130.1(25) 3_555 . 6_555 N
O2b Fe2 O2b 79.7(10) 3_555 . 13_555 N
O2b Fe2 O2b 79.7(10) 3_555 . 16_555 N
O2b Fe2 O2a 115.0(13) 3_555 . 3_555 N
O2b Fe2 O2b 79.7(10) 6_555 . 13_555 N
O2b Fe2 O2b 79.7(10) 6_555 . 16_555 N
O2b Fe2 O2a 115.0(13) 6_555 . 3_555 N
O2b Fe2 O2b 130.1(25) 13_555 . 16_555 N
O2b Fe2 O2a 115.0(13) 13_555 . 3_555 N
O2b Fe2 O2a 115.0(13) 16_555 . 3_555 N
Cs Os Cs 77.2(23) 1_555 . 4_555 N
Cs Os O1a 38.6(11) 1_555 . 1_555 N
Cs Os C1a 65.8(16) 1_555 . 1_555 N
Cs Os C1a 65.8(16) 1_555 . 12_565 N
Cs Os O1a 38.6(11) 4_555 . 1_555 N
Cs Os C1a 65.8(16) 4_555 . 1_555 N
Cs Os C1a 65.8(16) 4_555 . 12_565 N
O1a Os C1a 58.3(20) 1_555 . 1_555 N
O1a Os C1a 58.3(20) 1_555 . 12_565 N
C1a Os C1a 117(4) 1_555 . 12_565 N
Os Cs Cs 51.4(11) 1_555 . 4_555 N
Os Cs O1a 5.3(5) 1_555 . 1_555 N
Os Cs C1a 51.9(11) 1_555 . 1_555 N
Os Cs C1a 51.9(11) 1_555 . 12_565 N
Os Cs Hsa 108.2(12) 1_555 . 1_555 N
Os Cs Hsb 108.6(12) 1_555 . 1_555 N
Os Cs Hsb 108.6(12) 1_555 . -10_565 N
Cs Cs O1a 46.1(13) 4_555 . 1_555 N
Cs Cs C1a 52.7(11) 4_555 . 1_555 N
Cs Cs C1a 52.7(11) 4_555 . 12_565 N
Cs Cs Hsa 159.6(16) 4_555 . 1_555 N
Cs Cs Hsb 74.4(21) 4_555 . 1_555 N
Cs Cs Hsb 74.4(21) 4_555 . -10_565 N
O1a Cs C1a 50.2(9) 1_555 . 1_555 N
O1a Cs C1a 50.2(9) 1_555 . 12_565 N
O1a Cs Hsa 113.5(13) 1_555 . 1_555 N
O1a Cs Hsb 105.2(12) 1_555 . 1_555 N
O1a Cs Hsb 105.2(12) 1_555 . -10_565 N
C1a Cs C1a 94.5(13) 1_555 . 12_565 N
C1a Cs Hsa 117.5(14) 1_555 . 1_555 N
C1a Cs Hsb 59.3(18) 1_555 . 1_555 N
C1a Cs Hsb 124.5(28) 1_555 . -10_565 N
C1a Cs Hsa 117.5(14) 12_565 . 1_555 N
C1a Cs Hsb 124.5(28) 12_565 . 1_555 N
C1a Cs Hsb 59.3(18) 12_565 . -10_565 N
Hsa Cs Hsb 118.0(25) 1_555 . 1_555 N
Hsa Cs Hsb 118.0(25) 1_555 . -10_565 N
Hsb Cs Hsb 94(5) 1_555 . -10_565 N
Os O1a Cs 136.1(13) 1_555 . 1_555 N
Os O1a Cs 136.1(13) 1_555 . 4_555 N
Os O1a C1a 113.8(22) 1_555 . 1_555 N
Os O1a C1a 113.8(22) 1_555 . 12_565 N
Cs O1a Cs 87.8(26) 1_555 . 4_555 N
Cs O1a C1a 73.1(16) 1_555 . 1_555 N
Cs O1a C1a 73.1(16) 1_555 . 12_565 N
Cs O1a C1a 73.1(16) 4_555 . 1_555 N
Cs O1a C1a 73.1(16) 4_555 . 12_565 N
C1a O1a C1a 132(4) 1_555 . 12_565 N
Os C1a Cs 62.3(9) 1_555 . 1_555 N
Os C1a Cs 62.3(9) 1_555 . 4_555 N
Os C1a O1a 7.9(7) 1_555 . 1_555 N
Os C1a O1b 167(4) 1_555 . 1_555 N
Os C1a Hsb 104.2(22) 1_555 . 1_555 N
Os C1a Hsb 104.2(22) 1_555 . 4_555 N
Cs C1a Cs 74.6(22) 1_555 . 4_555 N
Cs C1a O1a 56.7(11) 1_555 . 1_555 N
Cs C1a O1b 127.0(21) 1_555 . 1_555 N
Cs C1a Hsb 44.1(12) 1_555 . 1_555 N
Cs C1a Hsb 81.3(34) 1_555 . 4_555 N
Cs C1a O1a 56.7(11) 4_555 . 1_555 N
Cs C1a O1b 127.0(21) 4_555 . 1_555 N
Cs C1a Hsb 81.3(34) 4_555 . 1_555 N
Cs C1a Hsb 44.1(12) 4_555 . 4_555 N
O1a C1a O1b 174(4) 1_555 . 1_555 N
O1a C1a Hsb 97.3(24) 1_555 . 1_555 N
O1a C1a Hsb 97.3(24) 1_555 . 4_555 N
O1b C1a Hsb 87.7(29) 1_555 . 1_555 N
O1b C1a Hsb 87.7(29) 1_555 . 4_555 N
Hsb C1a Hsb 56(5) 1_555 . 4_555 N
Cs Hsb C1a 76.6(12) 1_555 . 1_555 N
Cs Hsb Hsb 105.6(21) 1_555 . 4_555 N
Cs Hsb Hsb 42.9(25) 1_555 . -10_565 N
C1a Hsb Hsb 62.1(24) 1_555 . 4_555 N
C1a Hsb Hsb 103.7(15) 1_555 . -10_565 N
Hsb Hsb Hsb 90.0 4_555 . -10_565 N
Fe2 C2a C2a 12.4(20) 2_555 . 4_555 N
Fe2 C2a C2a 46.3(4) 2_555 . 14_555 N
Fe2 C2a C2a 46.3(4) 2_555 . 17_555 N
Fe2 C2a O2b 118.6(27) 2_555 . 1_555 N
Fe2 C2a O2a 60.3(25) 2_555 . 1_555 N
C2a C2a C2a 45.0000(8) 4_555 . 14_555 N
C2a C2a C2a 45.0000(8) 4_555 . 17_555 N
C2a C2a O2b 131.0(14) 4_555 . 1_555 N
C2a C2a O2a 47.9(12) 4_555 . 1_555 N
C2a C2a C2a 90.0000(16) 14_555 . 17_555 N
C2a C2a O2b 117.6(9) 14_555 . 1_555 N
C2a C2a O2a 61.7(7) 14_555 . 1_555 N
C2a C2a O2b 117.6(9) 17_555 . 1_555 N
C2a C2a O2a 61.7(7) 17_555 . 1_555 N
O2b C2a O2a 178.9(12) 1_555 . 1_555 N
Fe2 O2b C2a 24.0(10) 2_555 . 1_555 N
Fe2 O2b O3a 130.0(29) 2_555 . 14_555 N
Fe2 O2b O3b 164.5(25) 2_555 . 2_555 N
C2a O2b O3a 154.1(31) 1_555 . 14_555 N
C2a O2b O3b 140.4(25) 1_555 . 2_555 N
O3a O2b O3b 65.5(14) 14_555 . 2_555 N
Fe2 O2a C2a 42.1(12) 2_555 . 1_555 N
Fe2 O2a C2a 42.1(12) 2_555 . 4_555 N
Fe2 O2a C2a 42.1(12) 2_555 . 14_555 N
Fe2 O2a C2a 42.1(12) 2_555 . 17_555 N
C2a O2a C2a 84.3(24) 1_555 . 4_555 N
C2a O2a C2a 56.6(15) 1_555 . 14_555 N
C2a O2a C2a 56.6(15) 1_555 . 17_555 N
C2a O2a C2a 56.6(15) 4_555 . 14_555 N
C2a O2a C2a 56.6(15) 4_555 . 17_555 N
C2a O2a C2a 84.3(24) 14_555 . 17_555 N
O3a C3a O3a 89.9(30) 1_555 . 13_555 N
O3a C3a O3b 179.0(12) 1_555 . 1_555 N
O3a C3a O3b 89.1(28) 1_555 . 13_555 N
O3a C3a O3b 89.1(28) 13_555 . 1_555 N
O3a C3a O3b 179.0(12) 13_555 . 13_555 N
O3b C3a O3b 92.0(31) 1_555 . 13_555 N
O2b O3a C3a 105.0(26) 14_555 . 1_555 N
O2b O3a O3a 150.1(18) 14_555 . 13_555 N
O2b O3a O3b 60.2(19) 14_555 . 13_555 N
O2b O3a C4a 118.3(22) 14_555 . 2_555 N
O2b O3a C4a 118.3(22) 14_555 . 16_555 N
O2b O3a O4a 96.2(27) 14_555 . 2_555 N
O2b O3a O4a 96.2(27) 14_555 . 16_555 N
C3a O3a O3a 45.0(15) 1_555 . 13_555 N
C3a O3a O3b 44.9(14) 1_555 . 13_555 N
C3a O3a C4a 123.8(30) 1_555 . 2_555 N
C3a O3a C4a 123.8(30) 1_555 . 16_555 N
C3a O3a O4a 104.2(15) 1_555 . 2_555 N
C3a O3a O4a 104.2(15) 1_555 . 16_555 N
O3a O3a O3b 89.9(8) 13_555 . 13_555 N
O3a O3a C4a 86.6(21) 13_555 . 2_555 N
O3a O3a C4a 86.6(21) 13_555 . 16_555 N
O3a O3a O4a 92.7(25) 13_555 . 2_555 N
O3a O3a O4a 92.7(25) 13_555 . 16_555 N
O3b O3a C4a 147.7(19) 13_555 . 2_555 N
O3b O3a C4a 147.7(19) 13_555 . 16_555 N
O3b O3a O4a 107.4(17) 13_555 . 2_555 N
O3b O3a O4a 107.4(17) 13_555 . 16_555 N
C4a O3a C4a 64.0(35) 2_555 . 16_555 N
C4a O3a O4a 41.0(10) 2_555 . 2_555 N
C4a O3a O4a 104.8(34) 2_555 . 16_555 N
C4a O3a O4a 104.8(34) 16_555 . 2_555 N
C4a O3a O4a 41.0(10) 16_555 . 16_555 N
O4a O3a O4a 144.8(30) 2_555 . 16_555 N
O2b O3b C3a 100.4(21) 3_555 . 1_555 N
O2b O3b O3a 54.3(15) 3_555 . 13_555 N
O2b O3b O3b 144.4(14) 3_555 . 13_555 N
C3a O3b O3a 46.1(15) 1_555 . 13_555 N
C3a O3b O3b 44.0(15) 1_555 . 13_555 N
O3a O3b O3b 90.1(8) 13_555 . 13_555 N
O3a C4a O3a 100.3(30) 3_555 . 13_555 N
O3a C4a C4a 145.9(24) 3_555 . 2_555 N
O3a C4a C4a 93.4(21) 3_555 . 3_555 N
O3a C4a C4a 123.8(24) 3_555 . 4_555 N
O3a C4a C4a 58.0(17) 3_555 . 18_555 N
O3a C4a O4a 62.0(15) 3_555 . 1_555 N
O3a C4a O4b 118.9(27) 3_555 . 1_555 N
O3a C4a O4b 146.1(16) 3_555 . 2_555 N
O3a C4a O4b 112.1(18) 3_555 . 3_555 N
O3a C4a O4b 126.0(33) 3_555 . 4_555 N
O3a C4a O4b 96.7(34) 3_555 . 18_555 N
O3a C4a C4a 93.4(21) 13_555 . 2_555 N
O3a C4a C4a 145.9(24) 13_555 . 3_555 N
O3a C4a C4a 58.0(17) 13_555 . 4_555 N
O3a C4a C4a 123.8(24) 13_555 . 18_555 N
O3a C4a O4a 62.0(15) 13_555 . 1_555 N
O3a C4a O4b 118.9(27) 13_555 . 1_555 N
O3a C4a O4b 112.1(18) 13_555 . 2_555 N
O3a C4a O4b 146.1(16) 13_555 . 3_555 N
O3a C4a O4b 96.7(34) 13_555 . 4_555 N
O3a C4a O4b 126.0(33) 13_555 . 18_555 N
C4a C4a C4a 60.0000(5) 2_555 . 3_555 N
C4a C4a C4a 90.0 2_555 . 4_555 N
C4a C4a C4a 135.0 2_555 . 18_555 N
C4a C4a O4a 99(4) 2_555 . 1_555 N
C4a C4a O4b 79.6(30) 2_555 . 1_555 N
C4a C4a O4b 44.1(21) 2_555 . 2_555 N
C4a C4a O4b 64.9(15) 2_555 . 3_555 N
C4a C4a O4b 82.5(22) 2_555 . 4_555 N
C4a C4a O4b 100.2(24) 2_555 . 18_555 N
C4a C4a C4a 135.0000(8) 3_555 . 4_555 N
C4a C4a C4a 90.0 3_555 . 18_555 N
C4a C4a O4a 99(4) 3_555 . 1_555 N
C4a C4a O4b 79.6(30) 3_555 . 1_555 N
C4a C4a O4b 64.9(15) 3_555 . 2_555 N
C4a C4a O4b 44.1(21) 3_555 . 3_555 N
C4a C4a O4b 100.2(24) 3_555 . 4_555 N
C4a C4a O4b 82.5(22) 3_555 . 18_555 N
C4a C4a C4a 90.0 4_555 . 18_555 N
C4a C4a O4a 119.7(28) 4_555 . 1_555 N
C4a C4a O4b 61.4(20) 4_555 . 1_555 N
C4a C4a O4b 70.2(16) 4_555 . 2_555 N
C4a C4a O4b 94.5(19) 4_555 . 3_555 N
C4a C4a O4b 39.0(20) 4_555 . 4_555 N
C4a C4a O4b 69.9(15) 4_555 . 18_555 N
C4a C4a O4a 119.7(28) 18_555 . 1_555 N
C4a C4a O4b 61.4(20) 18_555 . 1_555 N
C4a C4a O4b 94.5(19) 18_555 . 2_555 N
C4a C4a O4b 70.2(16) 18_555 . 3_555 N
C4a C4a O4b 69.9(15) 18_555 . 4_555 N
C4a C4a O4b 39.0(20) 18_555 . 18_555 N
O4a C4a O4b 178(6) 1_555 . 1_555 N
O4a C4a O4b 143(6) 1_555 . 2_555 N
O4a C4a O4b 143(6) 1_555 . 3_555 N
O4a C4a O4b 159(4) 1_555 . 4_555 N
O4a C4a O4b 159(4) 1_555 . 18_555 N
O4b C4a O4b 35.5(30) 1_555 . 2_555 N
O4b C4a O4b 35.5(30) 1_555 . 3_555 N
O4b C4a O4b 22.3(19) 1_555 . 4_555 N
O4b C4a O4b 22.3(19) 1_555 . 18_555 N
O4b C4a O4b 34.3(24) 2_555 . 3_555 N
O4b C4a O4b 43.1(16) 2_555 . 4_555 N
O4b C4a O4b 56.6(18) 2_555 . 18_555 N
O4b C4a O4b 56.6(18) 3_555 . 4_555 N
O4b C4a O4b 43.1(16) 3_555 . 18_555 N
O4b C4a O4b 35.7(27) 4_555 . 18_555 N
O3a O4a O3a 116(4) 3_555 . 13_555 N
O3a O4a C4a 77.0(21) 3_555 . 1_555 N
O3a O4a O4a 143.1(28) 3_555 . 2_555 N
O3a O4a O4a 87.3(25) 3_555 . 3_555 N
O3a O4a C4a 77.0(21) 13_555 . 1_555 N
O3a O4a O4a 87.3(25) 13_555 . 2_555 N
O3a O4a O4a 143.1(28) 13_555 . 3_555 N
C4a O4a O4a 81(4) 1_555 . 2_555 N
C4a O4a O4a 81(4) 1_555 . 3_555 N
O4a O4a O4a 60.0000(5) 2_555 . 3_555 N
C4a O4b C4a 56(4) 1_555 . 2_555 N
C4a O4b C4a 56(4) 1_555 . 3_555 N
C4a O4b C4a 80(4) 1_555 . 4_555 N
C4a O4b C4a 80(4) 1_555 . 18_555 N
C4a O4b O4b 100.4(30) 1_555 . 2_555 N
C4a O4b O4b 100.4(30) 1_555 . 3_555 N
C4a O4b O4b 118.6(20) 1_555 . 4_555 N
C4a O4b O4b 117(4) 1_555 . 5_555 N
C4a O4b O4b 115.3(24) 1_555 . 6_555 N
C4a O4b O4b 127(4) 1_555 . 7_555 N
C4a O4b O4b 127(4) 1_555 . 8_555 N
C4a O4b O4b 152.4(33) 1_555 . 9_555 N
C4a O4b O4b 132.6(34) 1_555 . 12_555 N
C4a O4b O4b 115.3(24) 1_555 . 16_555 N
C4a O4b O4b 117(4) 1_555 . 17_555 N
C4a O4b O4b 118.6(20) 1_555 . 18_555 N
C4a O4b O4b 152.4(33) 1_555 . 24_555 N
C4a O4b O4b 139.1(19) 1_555 . -7_555 N
C4a O4b O4b 139.1(19) 1_555 . -8_555 N
C4a O4b C4a 50.1(30) 2_555 . 3_555 N
C4a O4b C4a 89.0(7) 2_555 . 4_555 N
C4a O4b C4a 130.8(16) 2_555 . 18_555 N
C4a O4b O4b 44.1(21) 2_555 . 2_555 N
C4a O4b O4b 72.8(12) 2_555 . 3_555 N
C4a O4b O4b 109.8(16) 2_555 . 4_555 N
C4a O4b O4b 61(4) 2_555 . 5_555 N
C4a O4b O4b 108(6) 2_555 . 6_555 N
C4a O4b O4b 72(5) 2_555 . 7_555 N
C4a O4b O4b 101(4) 2_555 . 8_555 N
C4a O4b O4b 129(4) 2_555 . 9_555 N
C4a O4b O4b 154.5(17) 2_555 . 12_555 N
C4a O4b O4b 67(5) 2_555 . 16_555 N
C4a O4b O4b 77.2(20) 2_555 . 17_555 N
C4a O4b O4b 159.6(13) 2_555 . 18_555 N
C4a O4b O4b 151(4) 2_555 . 24_555 N
C4a O4b O4b 143.7(31) 2_555 . -7_555 N
C4a O4b O4b 105.6(23) 2_555 . -8_555 N
C4a O4b C4a 130.8(16) 3_555 . 4_555 N
C4a O4b C4a 89.0(7) 3_555 . 18_555 N
C4a O4b O4b 72.8(12) 3_555 . 2_555 N
C4a O4b O4b 44.1(21) 3_555 . 3_555 N
C4a O4b O4b 159.6(13) 3_555 . 4_555 N
C4a O4b O4b 77.2(20) 3_555 . 5_555 N
C4a O4b O4b 67(5) 3_555 . 6_555 N
C4a O4b O4b 101(4) 3_555 . 7_555 N
C4a O4b O4b 72(5) 3_555 . 8_555 N
C4a O4b O4b 151(4) 3_555 . 9_555 N
C4a O4b O4b 154.5(17) 3_555 . 12_555 N
C4a O4b O4b 108(6) 3_555 . 16_555 N
C4a O4b O4b 61(4) 3_555 . 17_555 N
C4a O4b O4b 109.8(16) 3_555 . 18_555 N
C4a O4b O4b 129(4) 3_555 . 24_555 N
C4a O4b O4b 105.6(23) 3_555 . -7_555 N
C4a O4b O4b 143.7(31) 3_555 . -8_555 N
C4a O4b C4a 105(4) 4_555 . 18_555 N
C4a O4b O4b 97.5(22) 4_555 . 2_555 N
C4a O4b O4b 157.3(20) 4_555 . 3_555 N
C4a O4b O4b 39.0(20) 4_555 . 4_555 N
C4a O4b O4b 108.7(27) 4_555 . 5_555 N
C4a O4b O4b 162(6) 4_555 . 6_555 N
C4a O4b O4b 88.4(28) 4_555 . 7_555 N
C4a O4b O4b 152(4) 4_555 . 8_555 N
C4a O4b O4b 73.8(22) 4_555 . 9_555 N
C4a O4b O4b 72.2(13) 4_555 . 12_555 N
C4a O4b O4b 70(5) 4_555 . 16_555 N
C4a O4b O4b 144.8(31) 4_555 . 17_555 N
C4a O4b O4b 110.1(15) 4_555 . 18_555 N
C4a O4b O4b 100(4) 4_555 . 24_555 N
C4a O4b O4b 122.8(21) 4_555 . -7_555 N
C4a O4b O4b 62(4) 4_555 . -8_555 N
C4a O4b O4b 157.3(20) 18_555 . 2_555 N
C4a O4b O4b 97.5(22) 18_555 . 3_555 N
C4a O4b O4b 110.1(15) 18_555 . 4_555 N
C4a O4b O4b 144.8(31) 18_555 . 5_555 N
C4a O4b O4b 70(5) 18_555 . 6_555 N
C4a O4b O4b 152(4) 18_555 . 7_555 N
C4a O4b O4b 88.4(28) 18_555 . 8_555 N
C4a O4b O4b 100(4) 18_555 . 9_555 N
C4a O4b O4b 72.2(13) 18_555 . 12_555 N
C4a O4b O4b 162(6) 18_555 . 16_555 N
C4a O4b O4b 108.7(27) 18_555 . 17_555 N
C4a O4b O4b 39.0(20) 18_555 . 18_555 N
C4a O4b O4b 73.8(22) 18_555 . 24_555 N
C4a O4b O4b 62(4) 18_555 . -7_555 N
C4a O4b O4b 122.8(21) 18_555 . -8_555 N
O4b O4b O4b 60.0000(5) 2_555 . 3_555 N
O4b O4b O4b 90.0 2_555 . 4_555 N
O4b O4b O4b 18.7(22) 2_555 . 5_555 N
O4b O4b O4b 91(4) 2_555 . 6_555 N
O4b O4b O4b 30.4(31) 2_555 . 7_555 N
O4b O4b O4b 73.4(16) 2_555 . 8_555 N
O4b O4b O4b 90.4(31) 2_555 . 9_555 N
O4b O4b O4b 120.0000(5) 2_555 . 12_555 N
O4b O4b O4b 36(5) 2_555 . 16_555 N
O4b O4b O4b 50.7(9) 2_555 . 17_555 N
O4b O4b O4b 135.0 2_555 . 18_555 N
O4b O4b O4b 107.0(16) 2_555 . 24_555 N
O4b O4b O4b 108.7(22) 2_555 . -7_555 N
O4b O4b O4b 71.7(14) 2_555 . -8_555 N
O4b O4b O4b 135.0000(8) 3_555 . 4_555 N
O4b O4b O4b 50.7(9) 3_555 . 5_555 N
O4b O4b O4b 36(5) 3_555 . 6_555 N
O4b O4b O4b 73.4(16) 3_555 . 7_555 N
O4b O4b O4b 30.4(31) 3_555 . 8_555 N
O4b O4b O4b 107.0(16) 3_555 . 9_555 N
O4b O4b O4b 120.0000(9) 3_555 . 12_555 N
O4b O4b O4b 91(4) 3_555 . 16_555 N
O4b O4b O4b 18.7(22) 3_555 . 17_555 N
O4b O4b O4b 90.0 3_555 . 18_555 N
O4b O4b O4b 90.4(31) 3_555 . 24_555 N
O4b O4b O4b 71.7(14) 3_555 . -7_555 N
O4b O4b O4b 108.7(22) 3_555 . -8_555 N
O4b O4b O4b 90.0 4_555 . 5_555 N
O4b O4b O4b 125.0(26) 4_555 . 6_555 N
O4b O4b O4b 65.6(24) 4_555 . 7_555 N
O4b O4b O4b 113.8(24) 4_555 . 8_555 N
O4b O4b O4b 35.266(28) 4_555 . 9_555 N
O4b O4b O4b 45.0000(8) 4_555 . 12_555 N
O4b O4b O4b 54(5) 4_555 . 16_555 N
O4b O4b O4b 116.3(22) 4_555 . 17_555 N
O4b O4b O4b 90.0 4_555 . 18_555 N
O4b O4b O4b 65.6(24) 4_555 . 24_555 N
O4b O4b O4b 90.0 4_555 . -7_555 N
O4b O4b O4b 26.3(22) 4_555 . -8_555 N
O4b O4b O4b 75.3(21) 5_555 . 6_555 N
O4b O4b O4b 24.4(24) 5_555 . 7_555 N
O4b O4b O4b 56.7(7) 5_555 . 8_555 N
O4b O4b O4b 79.7(18) 5_555 . 9_555 N
O4b O4b O4b 108.3(14) 5_555 . 12_555 N
O4b O4b O4b 40(5) 5_555 . 16_555 N
O4b O4b O4b 36.5(29) 5_555 . 17_555 N
O4b O4b O4b 116.3(22) 5_555 . 18_555 N
O4b O4b O4b 90.0 5_555 . 24_555 N
O4b O4b O4b 90.0 5_555 . -7_555 N
O4b O4b O4b 66.6(14) 5_555 . -8_555 N
O4b O4b O4b 90.3(25) 6_555 . 7_555 N
O4b O4b O4b 19.8(26) 6_555 . 8_555 N
O4b O4b O4b 89.7(26) 6_555 . 9_555 N
O4b O4b O4b 89(4) 6_555 . 12_555 N
O4b O4b O4b 110(5) 6_555 . 16_555 N
O4b O4b O4b 40(5) 6_555 . 17_555 N
O4b O4b O4b 54(5) 6_555 . 18_555 N
O4b O4b O4b 61.8(10) 6_555 . 24_555 N
O4b O4b O4b 39(4) 6_555 . -7_555 N
O4b O4b O4b 105.1(7) 6_555 . -8_555 N
O4b O4b O4b 70.527(28) 7_555 . 8_555 N
O4b O4b O4b 60.0000(5) 7_555 . 9_555 N
O4b O4b O4b 89.6(31) 7_555 . 12_555 N
O4b O4b O4b 19.8(26) 7_555 . 16_555 N
O4b O4b O4b 56.7(7) 7_555 . 17_555 N
O4b O4b O4b 113.8(24) 7_555 . 18_555 N
O4b O4b O4b 80.2(18) 7_555 . 24_555 N
O4b O4b O4b 90.0 7_555 . -7_555 N
O4b O4b O4b 43.0(11) 7_555 . -8_555 N
O4b O4b O4b 80.2(18) 8_555 . 9_555 N
O4b O4b O4b 89.6(31) 8_555 . 12_555 N
O4b O4b O4b 90.3(25) 8_555 . 16_555 N
O4b O4b O4b 24.4(24) 8_555 . 17_555 N
O4b O4b O4b 65.6(24) 8_555 . 18_555 N
O4b O4b O4b 60.0000(9) 8_555 . 24_555 N
O4b O4b O4b 43.0(11) 8_555 . -7_555 N
O4b O4b O4b 90.0000(11) 8_555 . -8_555 N
O4b O4b O4b 29.6(31) 9_555 . 12_555 N
O4b O4b O4b 61.8(10) 9_555 . 16_555 N
O4b O4b O4b 90.0000(11) 9_555 . 17_555 N
O4b O4b O4b 65.6(24) 9_555 . 18_555 N
O4b O4b O4b 33.2(32) 9_555 . 24_555 N
O4b O4b O4b 56.7(7) 9_555 . -7_555 N
O4b O4b O4b 24.4(24) 9_555 . -8_555 N
O4b O4b O4b 89(4) 12_555 . 16_555 N
O4b O4b O4b 108.3(14) 12_555 . 17_555 N
O4b O4b O4b 45.0000(8) 12_555 . 18_555 N
O4b O4b O4b 29.6(31) 12_555 . 24_555 N
O4b O4b O4b 50.7(9) 12_555 . -7_555 N
O4b O4b O4b 50.7(9) 12_555 . -8_555 N
O4b O4b O4b 75.3(21) 16_555 . 17_555 N
O4b O4b O4b 125.0(26) 16_555 . 18_555 N
O4b O4b O4b 89.7(26) 16_555 . 24_555 N
O4b O4b O4b 105.1(7) 16_555 . -7_555 N
O4b O4b O4b 39(4) 16_555 . -8_555 N
O4b O4b O4b 90.0 17_555 . 18_555 N
O4b O4b O4b 79.7(18) 17_555 . 24_555 N
O4b O4b O4b 66.6(14) 17_555 . -7_555 N
O4b O4b O4b 90.0000(13) 17_555 . -8_555 N
O4b O4b O4b 35.266(28) 18_555 . 24_555 N
O4b O4b O4b 26.3(22) 18_555 . -7_555 N
O4b O4b O4b 90.0 18_555 . -8_555 N
O4b O4b O4b 24.4(24) 24_555 . -7_555 N
O4b O4b O4b 56.7(7) 24_555 . -8_555 N
O4b O4b O4b 78.7(17) -7_555 . -8_555 N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?

;
_vrf_PLAT601_1P5_FINAL_publ      
;
PROBLEM: Structure Contains Solvent Accessible VOIDS of .       2571 Ang3 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT430_1P5_FINAL_publ      
;
PROBLEM:Short Inter D...A Contact  O1A    ..  O1B     ..       2.33 Ang.   
RESPONSE: The problem happens because the adsorbed carbon dioxide on the open metal sites are disordered and thus some atoms ostensibly are seemed to be close to each other.
;
_vrf_PLAT307_1P5_FINAL_publ      
;
PROBLEM: Isolated Metal Atom found in Structure (Unusual)        Fe2 Check  
RESPONSE: It is charge balancing extra framework cation and it is supposed to be sorrounded by solvent molecules which couldn't be modeled because lack of their highly ordered pattern.
;



# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;
_vrf_PLAT602_FREECL_publ         
;
PROBLEM: Structure Contains Solvent Accessible VOIDS of .       2571 Ang3     
RESPONSE: This is expected as the material is porous and it is evacuated.
;

_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Fe 13.076 0.9450 International_Tables_Vol_C
C 100.396 0.6646 International_Tables_Vol_C
Cl 3.0 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 47.299 -0.3739 International_Tables_Vol_C
O 49.026 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.0775
_pd_proc_ls_prof_R_factor        0.0271
_pd_proc_ls_prof_wR_factor       0.0306
_pd_proc_ls_prof_wR_expected     0.0245
_refine_ls_R_Fsqd_factor         0.06561

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    1557.02     2:   -350.606     3:    330.706     4:   -47.1962    
      5:    193.284     6:   -72.2921     7:    129.383     8:   -50.4273    
      9:    65.6738    10:   -19.3719    11:    7.45674    12:   -16.1080    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  535.109 #2(GV)   = -250.839 #3(GW)   =  123.954
 #4(GP)   =    9.454 #5(LX)   =    0.000 #6(LY)   =   16.442
 #7(S/L)  =   0.0408 #8(H/L)  =   0.0382
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2016-05-25T14:04:12
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.6692
_pd_proc_2theta_range_max        166.4192
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
5710(160) 0.0 3660. .
5100(160) 0.0 3638. .
5040(150) 0.0 3616. .
4850(150) 0.0 3594. .
4600(150) 0.0 3572. .
4330(140) 0.0 3550. .
4290(140) 0.0 3529. .
4070(140) 0.0 3508. .
4020(140) 0.0 3487. .
4120(140) 0.0 3466. .
3760(130) 0.0 3445. .
3780(130) 0.0 3425. .
3750(130) 0.0 3405. .
3770(130) 0.0 3385. .
3810(140) 0.0 3365. .
3730(130) 0.0 3346. .
3940(140) 0.0 3326. .
3750(130) 0.0 3307. .
3690(130) 0.0 3288. .
3710(130) 0.0 3269. .
3720(130) 0.0 3251. .
3630(130) 0.0 3232. .
3710(130) 0.0 3214. .
3660(130) 0.0 3196. .
3860(140) 0.0 3178. .
3650(130) 0.0 3160. .
3840(140) 0.0 3142. .
3540(130) 0.0 3125. .
3750(130) 0.0 3108. .
3530(130) 0.0 3091. .
3580(130) 0.0 3074. .
3440(130) 0.0 3057. .
3470(130) 0.0 3040. .
3310(130) 0.0 3024. .
3270(130) 0.0 3008. .
3360(130) 0.0 2992. .
3300(130) 0.0 2976. .
3140(120) 0.0 2960. .
3080(120) 0.0 2944. .
3370(130) 0.0 2929. .
3260(130) 0.0 2914. .
3260(130) 0.0 2899. .
3240(130) 0.0 2884. .
3220(120) 0.0 2869. .
2970(120) 0.0 2854. .
3200(120) 0.0000650 2840. 2851.
3030(120) 0.0000683 2825. 2837.
3200(120) 0.0000650 2811. 2824.
3110(120) 0.0000672 2797. 2812.
3120(120) 0.0000661 2783. 2801.
3290(130) 0.0000630 2769. 2796.
3280(130) 0.0000640 2755. 2799.
3520(130) 0.0000592 2742. 2817.
3250(130) 0.0000640 2728. 2854.
3520(130) 0.0000592 2715. 2916.
3680(130) 0.0000565 2702. 3001.
3720(130) 0.0000565 2689. 3105.
3480(130) 0.0000601 2676. 3224.
3660(130) 0.0000574 2663. 3356.
4170(140) 0.0000503 2651. 3496.
3970(140) 0.0000533 2638. 3645.
4080(140) 0.0000518 2626. 3803.
4120(140) 0.0000510 2614. 3971.
4170(140) 0.0000503 2602. 4149.
4410(140) 0.0000482 2590. 4337.
4550(150) 0.0000463 2578. 4537.
4800(150) 0.0000444 2566. 4751.
4840(150) 0.0000439 2555. 4979.
5090(160) 0.0000416 2543. 5222.
5160(160) 0.0000411 2532. 5483.
5200(160) 0.0000411 2521. 5763.
5680(160) 0.0000376 2510. 6065.
5820(170) 0.0000367 2499. 6391.
6310(170) 0.0000338 2488. 6745.
6600(180) 0.0000323 2477. 7130.
7150(180) 0.0000299 2466. 7551.
7370(190) 0.0000292 2456. 8013.
7930(190) 0.0000271 2445. 8524.
8450(200) 0.0000255 2435. 9092.
9470(210) 0.0000227 2425. 9729.
9960(220) 0.0000216 2415. 10449.
11040(230) 0.0000196 2405. 11272.
11980(240) 0.0000181 2395. 12228.
13310(250) 0.0000163 2385. 13358.
14480(260) 0.0000150 2376. 14730.
16580(280) 0.0000131 2366. 16461.
19080(300) 0.0000114 2357. 18740.
23040(330) 9.47e-6 2347. 21837.
27520(360) 7.93e-6 2338. 25974.
32400(390) 6.75e-6 2329. 30991.
37350(410) 5.86e-6 2320. 35900.
40060(430) 5.46e-6 2311. 38835.
39540(430) 5.54e-6 2302. 37878.
33900(390) 6.44e-6 2293. 32475.
25690(340) 8.50e-6 2285. 24196.
16760(280) 0.0000129 2276. 15770.
9810(210) 0.0000220 2268. 9300.
6020(170) 0.0000354 2259. 5383.
3810(140) 0.0000549 2251. 3473.
2490(110) 0.0000826 2243. 2706.
2259(72) 0.0001929 2235. 2441.
2193(70) 0.0002041 2227. 2352.
2134(70) 0.0002041 2219. 2314.
2207(71) 0.0001984 2211. 2290.
2179(70) 0.0002041 2203. 2272.
2022(68) 0.0002163 2196. 2256.
1983(67) 0.0002228 2188. 2241.
1981(67) 0.0002228 2181. 2228.
1894(66) 0.0002296 2173. 2216.
1952(67) 0.0002228 2166. 2204.
2005(67) 0.0002228 2159. 2194.
2026(68) 0.0002163 2151. 2184.
1933(66) 0.0002296 2144. 2174.
1970(67) 0.0002228 2137. 2165.
1930(66) 0.0002296 2131. 2156.
2084(69) 0.0002100 2124. 2148.
2006(67) 0.0002228 2117. 2140.
1910(66) 0.0002296 2110. 2134.
1986(67) 0.0002228 2104. 2129.
2000(67) 0.0002228 2097. 2110.
2008(67) 0.0002228 2091. 2113.
1960(67) 0.0002228 2084. 2119.
2037(68) 0.0002163 2078. 2130.
2071(69) 0.0002100 2072. 2144.
2200(70) 0.0002041 2066. 2161.
2081(69) 0.0002100 2060. 2182.
1974(67) 0.0002228 2054. 2204.
2090(69) 0.0002100 2048. 2230.
2258(71) 0.0001984 2042. 2258.
2221(71) 0.0001984 2036. 2290.
2330(73) 0.0001877 2030. 2326.
2289(72) 0.0001929 2025. 2366.
2248(71) 0.0001984 2019. 2413.
2351(73) 0.0001877 2014. 2467.
2528(75) 0.0001778 2008. 2529.
2499(75) 0.0001778 2003. 2604.
2711(78) 0.0001644 1997. 2694.
2891(81) 0.0001524 1992. 2808.
3177(84) 0.0001417 1987. 2956.
3453(88) 0.0001291 1982. 3158.
3651(90) 0.0001235 1977. 3434.
4213(97) 0.0001063 1972. 3787.
4720(100) 0.0000961 1967. 4170.
4970(110) 0.0000907 1962. 4465.
5030(110) 0.0000907 1957. 4523.
4500(100) 0.0001000 1952. 4245.
4051(95) 0.0001108 1947. 3700.
3323(86) 0.0001352 1943. 3079.
2693(78) 0.0001644 1938. 2563.
2198(70) 0.0002041 1934. 2228.
2048(68) 0.0002163 1929. 2055.
1874(65) 0.0002367 1925. 1979.
1961(67) 0.0002228 1920. 1950.
1830(65) 0.0002367 1916. 1938.
1923(66) 0.0002296 1912. 1931.
1971(67) 0.0002228 1907. 1926.
1913(66) 0.0002296 1903. 1922.
1864(65) 0.0002367 1899. 1918.
1909(66) 0.0002296 1895. 1914.
1827(65) 0.0002367 1891. 1911.
1954(67) 0.0002228 1887. 1909.
2025(68) 0.0002163 1883. 1909.
2034(68) 0.0002163 1879. 1912.
2012(68) 0.0002163 1875. 1924.
2041(68) 0.0002163 1872. 1951.
2170(70) 0.0002041 1868. 2000.
2369(73) 0.0001877 1864. 2079.
2442(74) 0.0001826 1861. 2190.
2501(75) 0.0001778 1857. 2332.
2639(77) 0.0001687 1854. 2503.
2742(79) 0.0001602 1850. 2700.
2951(81) 0.0001524 1847. 2923.
3166(84) 0.0001417 1843. 3175.
3336(86) 0.0001352 1840. 3462.
3615(90) 0.0001235 1837. 3792.
3912(93) 0.0001156 1833. 4177.
4269(97) 0.0001063 1830. 4636.
4930(110) 0.0000907 1827. 5199.
5630(110) 0.0000797 1824. 5923.
6830(120) 0.0000661 1821. 6892.
8110(130) 0.0000557 1818. 8215.
9820(150) 0.0000463 1815. 9946.
12040(160) 0.0000376 1812. 11925.
13850(170) 0.0000330 1809. 13634.
14240(180) 0.0000319 1806. 14302.
12880(170) 0.0000354 1803. 13350.
10370(150) 0.0000439 1800. 10919.
7370(130) 0.0000620 1797. 7891.
5020(110) 0.0000907 1795. 5234.
3423(87) 0.0001321 1792. 3445.
2390(73) 0.0001877 1789. 2487.
2025(68) 0.0002163 1787. 2069.
1828(65) 0.0002367 1784. 1915.
1861(65) 0.0002367 1781. 1860.
1739(63) 0.0002520 1779. 1838.
1779(64) 0.0002441 1776. 1825.
1778(86) 0.0001352 1774. 1815.
1721(85) 0.0001384 1772. 1807.
1842(88) 0.0001291 1769. 1800.
1707(85) 0.0001384 1767. 1794.
1845(64) 0.0002441 1764. 1789.
1823(63) 0.0002520 1762. 1785.
1891(64) 0.0002441 1760. 1782.
1902(65) 0.0002367 1758. 1780.
1875(64) 0.0002441 1755. 1778.
1793(63) 0.0002520 1753. 1778.
1875(64) 0.0002441 1751. 1779.
1772(62) 0.0002601 1749. 1780.
1842(64) 0.0002441 1747. 1783.
1819(63) 0.0002520 1745. 1786.
1816(63) 0.0002520 1743. 1791.
1852(64) 0.0002441 1741. 1798.
1859(64) 0.0002441 1739. 1807.
1853(64) 0.0002441 1737. 1821.
1939(65) 0.0002367 1735. 1840.
1937(65) 0.0002367 1733. 1866.
1872(64) 0.0002441 1731. 1896.
1861(64) 0.0002441 1730. 1916.
1928(65) 0.0002367 1728. 1924.
1957(65) 0.0002367 1726. 1907.
1926(65) 0.0002367 1724. 1866.
1830(63) 0.0002520 1723. 1816.
1788(63) 0.0002520 1721. 1773.
1855(64) 0.0002441 1719. 1744.
1697(61) 0.0002687 1718. 1728.
1732(62) 0.0002601 1716. 1721.
1713(61) 0.0002687 1714. 1717.
1700(61) 0.0002687 1713. 1714.
1636(60) 0.0002778 1711. 1713.
1767(62) 0.0002601 1710. 1711.
1807(63) 0.0002520 1708. 1709.
1759(62) 0.0002601 1707. 1708.
1754(62) 0.0002601 1705. 1707.
1742(62) 0.0002601 1704. 1706.
1794(63) 0.0002520 1703. 1705.
1743(62) 0.0002601 1701. 1705.
1813(63) 0.0002520 1700. 1706.
1739(62) 0.0002601 1699. 1707.
1702(61) 0.0002687 1697. 1708.
1773(62) 0.0002601 1696. 1711.
1854(64) 0.0002441 1695. 1714.
1735(62) 0.0002601 1693. 1718.
1693(61) 0.0002687 1692. 1724.
1752(62) 0.0002601 1691. 1732.
1773(62) 0.0002601 1690. 1743.
1741(62) 0.0002601 1689. 1758.
1765(62) 0.0002601 1687. 1776.
1748(62) 0.0002601 1686. 1790.
1660(60) 0.0002778 1685. 1795.
1677(61) 0.0002687 1684. 1785.
1693(61) 0.0002687 1683. 1761.
1648(60) 0.0002778 1682. 1733.
1758(62) 0.0002601 1681. 1709.
1717(61) 0.0002687 1680. 1694.
1729(62) 0.0002601 1679. 1685.
1659(60) 0.0002778 1678. 1681.
1688(61) 0.0002687 1677. 1679.
1749(62) 0.0002601 1676. 1677.
1740(62) 0.0002601 1675. 1676.
1718(61) 0.0002687 1674. 1675.
1731(62) 0.0002601 1673. 1675.
1796(63) 0.0002520 1672. 1675.
1721(61) 0.0002687 1671. 1675.
1733(62) 0.0002601 1670. 1677.
1738(62) 0.0002601 1670. 1680.
1724(61) 0.0002687 1669. 1684.
1766(62) 0.0002601 1668. 1690.
1756(62) 0.0002601 1667. 1697.
1677(61) 0.0002687 1666. 1707.
1646(60) 0.0002778 1666. 1719.
1738(62) 0.0002601 1665. 1736.
1759(62) 0.0002601 1664. 1759.
1777(62) 0.0002601 1663. 1790.
1723(61) 0.0002687 1663. 1826.
1761(62) 0.0002601 1662. 1858.
1667(60) 0.0002778 1661. 1872.
1824(63) 0.0002520 1660. 1858.
1814(63) 0.0002520 1660. 1816.
1776(62) 0.0002601 1659. 1764.
1720(61) 0.0002687 1658. 1718.
1697(61) 0.0002687 1658. 1686.
1692(61) 0.0002687 1657. 1670.
1685(61) 0.0002687 1657. 1662.
1610(59) 0.0002873 1656. 1659.
1764(62) 0.0002601 1655. 1658.
1777(62) 0.0002601 1655. 1657.
1689(61) 0.0002687 1654. 1656.
1642(60) 0.0002778 1654. 1655.
1752(62) 0.0002601 1653. 1655.
1761(62) 0.0002601 1653. 1654.
1647(60) 0.0002778 1652. 1654.
1677(61) 0.0002687 1652. 1653.
1666(60) 0.0002778 1651. 1653.
1672(61) 0.0002687 1651. 1652.
1725(61) 0.0002687 1650. 1652.
1686(61) 0.0002687 1650. 1651.
1734(89) 0.0001262 1649. 1651.
1704(60) 0.0002778 1649. 1650.
1718(60) 0.0002778 1648. 1650.
1652(59) 0.0002873 1648. 1650.
1753(61) 0.0002687 1647. 1650.
1797(62) 0.0002601 1647. 1649.
1748(61) 0.0002687 1647. 1649.
1777(61) 0.0002687 1646. 1649.
1779(61) 0.0002687 1646. 1649.
1784(61) 0.0002687 1645. 1649.
1795(62) 0.0002601 1645. 1650.
1728(60) 0.0002778 1645. 1651.
1771(61) 0.0002687 1644. 1651.
1732(61) 0.0002687 1644. 1652.
1729(60) 0.0002778 1644. 1655.
1788(61) 0.0002687 1643. 1660.
1676(60) 0.0002778 1643. 1670.
1680(60) 0.0002778 1643. 1688.
1769(61) 0.0002687 1642. 1715.
1749(61) 0.0002687 1642. 1753.
1827(62) 0.0002601 1642. 1804.
1869(63) 0.0002520 1641. 1871.
2117(67) 0.0002228 1641. 1962.
2193(68) 0.0002163 1641. 2086.
2277(69) 0.0002100 1641. 2253.
2519(73) 0.0001877 1640. 2457.
2777(76) 0.0001731 1640. 2657.
2907(78) 0.0001644 1640. 2782.
2813(77) 0.0001687 1640. 2757.
2621(74) 0.0001826 1639. 2570.
2282(69) 0.0002100 1639. 2293.
2083(66) 0.0002296 1639. 2029.
1885(63) 0.0002520 1639. 1841.
1741(61) 0.0002687 1638. 1735.
1706(60) 0.0002778 1638. 1688.
1731(61) 0.0002687 1638. 1671.
1838(62) 0.0002601 1638. 1669.
1827(62) 0.0002601 1638. 1676.
1794(62) 0.0002601 1637. 1694.
1849(63) 0.0002520 1637. 1728.
1861(63) 0.0002520 1637. 1785.
1891(63) 0.0002520 1637. 1871.
1933(64) 0.0002441 1637. 1992.
2211(68) 0.0002163 1636. 2157.
2287(69) 0.0002100 1636. 2384.
2658(75) 0.0001778 1636. 2696.
2987(79) 0.0001602 1636. 3113.
3604(87) 0.0001321 1636. 3614.
3938(91) 0.0001208 1636. 4095.
4223(94) 0.0001132 1636. 4374.
4086(93) 0.0001156 1635. 4281.
3599(87) 0.0001321 1635. 3802.
2816(77) 0.0001687 1635. 3129.
2316(70) 0.0002041 1635. 2507.
2011(65) 0.0002367 1635. 2072.
1778(61) 0.0002687 1635. 1832.
1670(59) 0.0002873 1635. 1724.
1616(58) 0.0002973 1635. 1683.
1606(58) 0.0002973 1634. 1667.
1655(59) 0.0002873 1634. 1660.
1707(60) 0.0002778 1634. 1656.
1618(59) 0.0002873 1634. 1654.
1540(57) 0.0003078 1634. 1652.
1600(58) 0.0002973 1634. 1651.
1689(60) 0.0002778 1634. 1650.
1674(60) 0.0002778 1634. 1649.
1659(59) 0.0002873 1634. 1649.
1650(59) 0.0002873 1634. 1648.
1692(60) 0.0002778 1634. 1649.
1712(60) 0.0002778 1634. 1649.
1672(59) 0.0002873 1633. 1649.
1646(59) 0.0002873 1633. 1650.
1602(58) 0.0002973 1633. 1650.
1654(59) 0.0002873 1633. 1650.
1702(60) 0.0002778 1633. 1651.
1664(59) 0.0002873 1633. 1652.
1655(59) 0.0002873 1633. 1654.
1646(59) 0.0002873 1633. 1659.
1753(61) 0.0002687 1633. 1667.
1784(61) 0.0002687 1633. 1685.
1810(62) 0.0002601 1633. 1719.
1882(63) 0.0002520 1633. 1779.
1925(64) 0.0002441 1633. 1875.
2039(66) 0.0002296 1633. 2020.
2173(68) 0.0002163 1633. 2228.
2510(73) 0.0001877 1633. 2522.
2733(76) 0.0001731 1633. 2930.
3217(82) 0.0001487 1633. 3455.
3736(89) 0.0001262 1633. 4034.
4271(95) 0.0001108 1633. 4500.
4196(94) 0.0001132 1632. 4642.
3873(90) 0.0001235 1632. 4330.
3430(85) 0.0001384 1632. 3669.
2670(75) 0.0001778 1632. 2930.
2229(69) 0.0002100 1632. 2339.
1907(63) 0.0002520 1632. 1971.
1797(62) 0.0002601 1632. 1789.
1809(62) 0.0002601 1632. 1715.
1735(61) 0.0002687 1632. 1692.
1812(62) 0.0002601 1632. 1693.
1692(57) 0.0003078 1632. 1710.
1705(57) 0.0003078 1632. 1744.
1732(58) 0.0002973 1632. 1800.
1880(60) 0.0002778 1632. 1885.
2035(62) 0.0002601 1632. 2009.
2083(63) 0.0002520 1632. 2182.
2249(65) 0.0002367 1632. 2405.
2584(70) 0.0002041 1632. 2647.
2741(72) 0.0001929 1632. 2836.
2723(72) 0.0001929 1632. 2883.
2589(70) 0.0002041 1632. 2739.
2397(68) 0.0002163 1632. 2458.
2176(64) 0.0002441 1632. 2153.
1940(61) 0.0002687 1632. 1914.
1833(59) 0.0002873 1632. 1767.
1704(57) 0.0003078 1632. 1695.
1730(58) 0.0002973 1632. 1665.
1767(58) 0.0002973 1632. 1653.
1704(57) 0.0003078 1632. 1649.
1671(57) 0.0003078 1632. 1646.
1673(57) 0.0003078 1632. 1645.
1596(55) 0.0003306 1632. 1645.
1644(56) 0.0003189 1632. 1645.
1630(56) 0.0003189 1632. 1647.
1637(56) 0.0003189 1632. 1649.
1723(57) 0.0003078 1632. 1651.
1652(56) 0.0003189 1632. 1653.
1692(57) 0.0003078 1632. 1654.
1698(57) 0.0003078 1632. 1652.
1616(56) 0.0003189 1632. 1648.
1691(57) 0.0003078 1632. 1644.
1615(56) 0.0003189 1632. 1641.
1645(56) 0.0003189 1632. 1639.
1582(55) 0.0003306 1632. 1638.
1669(57) 0.0003078 1632. 1638.
1692(57) 0.0003078 1632. 1639.
1656(56) 0.0003189 1632. 1639.
1638(56) 0.0003189 1632. 1642.
1619(56) 0.0003189 1632. 1648.
1658(56) 0.0003189 1632. 1656.
1650(56) 0.0003189 1632. 1668.
1682(57) 0.0003078 1632. 1684.
1690(57) 0.0003078 1632. 1705.
1651(56) 0.0003189 1632. 1725.
1748(58) 0.0002973 1632. 1739.
1625(56) 0.0003189 1632. 1738.
1631(56) 0.0003189 1632. 1722.
1556(55) 0.0003306 1632. 1696.
1556(55) 0.0003306 1632. 1673.
1662(56) 0.0003189 1632. 1655.
1651(56) 0.0003189 1632. 1645.
1682(57) 0.0003078 1632. 1641.
1642(56) 0.0003189 1632. 1639.
1601(55) 0.0003306 1632. 1638.
1605(55) 0.0003306 1632. 1638.
1530(54) 0.0003429 1632. 1638.
1627(56) 0.0003189 1632. 1638.
1590(55) 0.0003306 1632. 1639.
1609(56) 0.0003189 1632. 1639.
1613(56) 0.0003189 1632. 1640.
1573(55) 0.0003306 1632. 1641.
1567(55) 0.0003306 1632. 1641.
1631(56) 0.0003189 1632. 1643.
1656(56) 0.0003189 1632. 1645.
1617(56) 0.0003189 1632. 1646.
1622(56) 0.0003189 1632. 1649.
1739(58) 0.0002973 1632. 1652.
1718(57) 0.0003078 1632. 1658.
1718(57) 0.0003078 1632. 1669.
1654(56) 0.0003189 1632. 1690.
1641(56) 0.0003189 1632. 1732.
1763(58) 0.0002973 1632. 1805.
1958(61) 0.0002687 1632. 1927.
2086(63) 0.0002520 1632. 2115.
2341(67) 0.0002228 1632. 2389.
2788(73) 0.0001877 1632. 2745.
3240(78) 0.0001644 1632. 3135.
3599(83) 0.0001452 1632. 3446.
3713(84) 0.0001417 1632. 3537.
3392(80) 0.0001562 1632. 3332.
2963(75) 0.0001778 1632. 2910.
2503(69) 0.0002100 1632. 2449.
2133(64) 0.0002441 1632. 2086.
1908(60) 0.0002778 1632. 1864.
1845(59) 0.0002873 1632. 1760.
1782(58) 0.0002973 1632. 1729.
1691(57) 0.0003078 1632. 1745.
1761(58) 0.0002973 1632. 1798.
1816(59) 0.0002873 1631. 1897.
1984(62) 0.0002601 1631. 2056.
2243(65) 0.0002367 1631. 2289.
2561(70) 0.0002041 1631. 2592.
2989(75) 0.0001778 1631. 2916.
3316(79) 0.0001602 1631. 3163.
3295(79) 0.0001602 1631. 3218.
3173(78) 0.0001644 1631. 3027.
2690(71) 0.0001984 1631. 2668.
2369(67) 0.0002228 1631. 2289.
2122(64) 0.0002441 1631. 1998.
1876(60) 0.0002778 1631. 1826.
1776(58) 0.0002973 1631. 1749.
1652(55) 0.0003306 1631. 1735.
1787(57) 0.0003078 1631. 1765.
1830(58) 0.0002973 1631. 1839.
1896(59) 0.0002873 1631. 1968.
2128(63) 0.0002520 1631. 2169.
2339(66) 0.0002296 1631. 2449.
2759(72) 0.0001929 1631. 2783.
2942(74) 0.0001826 1631. 3093.
3154(77) 0.0001687 1631. 3259.
3083(76) 0.0001731 1631. 3184.
2859(73) 0.0001877 1631. 2882.
2395(67) 0.0002228 1631. 2486.
2129(63) 0.0002520 1630. 2137.
1909(59) 0.0002873 1630. 1902.
1824(58) 0.0002973 1630. 1782.
1736(57) 0.0003078 1630. 1742.
1751(57) 0.0003078 1630. 1758.
1837(58) 0.0002973 1630. 1820.
1907(59) 0.0002873 1630. 1939.
2004(61) 0.0002687 1630. 2129.
2281(65) 0.0002367 1630. 2399.
2471(68) 0.0002163 1630. 2727.
2746(71) 0.0001984 1630. 3039.
3045(75) 0.0001778 1630. 3218.
3063(75) 0.0001778 1630. 3166.
2723(71) 0.0001984 1630. 2882.
2382(66) 0.0002296 1630. 2493.
2082(62) 0.0002601 1630. 2139.
1913(59) 0.0002873 1630. 1894.
1751(57) 0.0003078 1629. 1757.
1675(56) 0.0003189 1629. 1694.
1659(55) 0.0003306 1629. 1668.
1650(55) 0.0003306 1629. 1658.
1736(57) 0.0003078 1629. 1654.
1675(56) 0.0003189 1629. 1652.
1679(56) 0.0003189 1629. 1652.
1748(57) 0.0003078 1629. 1652.
1712(56) 0.0003189 1629. 1653.
1631(55) 0.0003306 1629. 1653.
1686(56) 0.0003189 1629. 1650.
1642(55) 0.0003306 1629. 1646.
1694(56) 0.0003189 1629. 1642.
1643(55) 0.0003306 1628. 1639.
1633(55) 0.0003306 1628. 1636.
1666(56) 0.0003189 1628. 1635.
1712(56) 0.0003189 1628. 1634.
1612(55) 0.0003306 1628. 1634.
1601(54) 0.0003429 1628. 1634.
1636(55) 0.0003306 1628. 1635.
1620(55) 0.0003306 1628. 1637.
1637(55) 0.0003306 1628. 1639.
1727(57) 0.0003078 1628. 1641.
1607(54) 0.0003429 1628. 1642.
1670(56) 0.0003189 1627. 1642.
1689(56) 0.0003189 1627. 1639.
1689(56) 0.0003189 1627. 1636.
1653(55) 0.0003306 1627. 1633.
1633(55) 0.0003306 1627. 1631.
1628(55) 0.0003306 1627. 1630.
1730(57) 0.0003078 1627. 1630.
1634(55) 0.0003306 1627. 1631.
1634(55) 0.0003306 1627. 1632.
1696(56) 0.0003189 1627. 1635.
1606(54) 0.0003429 1626. 1639.
1620(55) 0.0003306 1626. 1645.
1664(55) 0.0003306 1626. 1650.
1566(54) 0.0003429 1626. 1654.
1646(55) 0.0003306 1626. 1654.
1633(55) 0.0003306 1626. 1649.
1689(56) 0.0003189 1626. 1642.
1629(55) 0.0003306 1626. 1636.
1625(55) 0.0003306 1626. 1631.
1611(55) 0.0003306 1625. 1629.
1574(54) 0.0003429 1625. 1627.
1704(56) 0.0003189 1625. 1627.
1714(56) 0.0003189 1625. 1626.
1691(56) 0.0003189 1625. 1626.
1606(54) 0.0003429 1625. 1626.
1682(56) 0.0003189 1625. 1626.
1679(56) 0.0003189 1625. 1626.
1603(54) 0.0003429 1624. 1627.
1576(54) 0.0003429 1624. 1627.
1682(56) 0.0003189 1624. 1627.
1662(55) 0.0003306 1624. 1627.
1630(55) 0.0003306 1624. 1628.
1599(54) 0.0003429 1624. 1628.
1618(55) 0.0003306 1624. 1628.
1551(54) 0.0003429 1624. 1629.
1628(55) 0.0003306 1623. 1631.
1609(55) 0.0003306 1623. 1633.
1611(55) 0.0003306 1623. 1638.
1589(54) 0.0003429 1623. 1643.
1596(54) 0.0003429 1623. 1649.
1694(56) 0.0003189 1623. 1654.
1642(55) 0.0003306 1623. 1655.
1657(55) 0.0003306 1622. 1652.
1688(56) 0.0003189 1622. 1647.
1725(56) 0.0003189 1622. 1642.
1667(56) 0.0003189 1622. 1639.
1637(53) 0.000356 1622. 1640.
1668(54) 0.0003429 1622. 1647.
1714(54) 0.0003429 1622. 1662.
1672(54) 0.0003429 1621. 1689.
1783(55) 0.0003306 1621. 1732.
1774(55) 0.0003306 1621. 1791.
1890(57) 0.0003078 1621. 1859.
1915(58) 0.0002973 1621. 1915.
1958(58) 0.0002973 1621. 1938.
1922(58) 0.0002973 1621. 1912.
1911(57) 0.0003078 1620. 1850.
1749(55) 0.0003306 1620. 1779.
1645(53) 0.000356 1620. 1724.
1659(53) 0.000356 1620. 1694.
1686(54) 0.0003429 1620. 1693.
1699(54) 0.0003429 1620. 1720.
1748(55) 0.0003306 1619. 1782.
1789(56) 0.0003189 1619. 1886.
1904(57) 0.0003078 1619. 2029.
2101(60) 0.0002778 1619. 2193.
2128(61) 0.0002687 1619. 2330.
2080(60) 0.0002778 1619. 2384.
2020(59) 0.0002873 1618. 2323.
1976(58) 0.0002973 1618. 2174.
1871(57) 0.0003078 1618. 2005.
1849(57) 0.0003078 1618. 1877.
1903(57) 0.0003078 1618. 1820.
1926(58) 0.0002973 1618. 1847.
2003(59) 0.0002873 1617. 1975.
2345(64) 0.0002441 1617. 2231.
2744(69) 0.0002100 1617. 2641.
3270(75) 0.0001778 1617. 3188.
3864(82) 0.0001487 1617. 3773.
4398(87) 0.0001321 1617. 4211.
4603(89) 0.0001262 1616. 4303.
4181(85) 0.0001384 1616. 3971.
3335(76) 0.0001731 1616. 3364.
2753(69) 0.0002100 1616. 2730.
2330(63) 0.0002520 1616. 2238.
2050(60) 0.0002778 1615. 1934.
1807(56) 0.0003189 1615. 1777.
1697(54) 0.0003429 1615. 1708.
1670(54) 0.0003429 1615. 1681.
1699(54) 0.0003429 1615. 1668.
1716(54) 0.0003429 1615. 1661.
1634(53) 0.000356 1614. 1657.
1547(52) 0.000370 1614. 1654.
1643(53) 0.000356 1614. 1653.
1632(53) 0.000356 1614. 1654.
1648(53) 0.000356 1614. 1657.
1633(53) 0.000356 1613. 1665.
1572(52) 0.000370 1613. 1684.
1723(55) 0.0003306 1613. 1725.
1882(57) 0.0003078 1613. 1807.
1972(58) 0.0002973 1613. 1951.
2198(62) 0.0002601 1612. 2176.
2479(65) 0.0002367 1612. 2470.
2829(70) 0.0002041 1612. 2777.
3013(72) 0.0001929 1612. 2997.
3000(72) 0.0001929 1612. 3027.
2680(68) 0.0002163 1611. 2837.
2448(65) 0.0002367 1611. 2515.
2133(61) 0.0002687 1611. 2190.
1920(58) 0.0002973 1611. 1946.
1801(56) 0.0003189 1611. 1805.
1672(54) 0.0003429 1610. 1753.
1712(54) 0.0003429 1610. 1762.
1736(55) 0.0003306 1610. 1818.
1771(55) 0.0003306 1610. 1906.
1825(56) 0.0003189 1610. 2006.
1914(58) 0.0002973 1609. 2083.
1920(58) 0.0002973 1609. 2102.
1894(57) 0.0003078 1609. 2048.
1758(55) 0.0003306 1609. 1944.
1757(55) 0.0003306 1608. 1833.
1749(55) 0.0003306 1608. 1745.
1695(54) 0.0003429 1608. 1689.
1669(54) 0.0003429 1608. 1661.
1660(54) 0.0003429 1608. 1648.
1714(54) 0.0003429 1607. 1643.
1667(54) 0.0003429 1607. 1643.
1674(54) 0.0003429 1607. 1644.
1655(53) 0.000356 1607. 1646.
1683(54) 0.0003429 1606. 1649.
1682(54) 0.0003429 1606. 1655.
1647(53) 0.000356 1606. 1664.
1712(54) 0.0003429 1606. 1682.
1802(56) 0.0003189 1606. 1718.
1815(56) 0.0003189 1605. 1797.
1892(57) 0.0003078 1605. 1952.
2197(62) 0.0002601 1605. 2228.
2742(69) 0.0002100 1605. 2655.
3292(76) 0.0001731 1604. 3209.
4015(83) 0.0001452 1604. 3779.
4404(87) 0.0001321 1604. 4175.
4471(88) 0.0001291 1604. 4211.
3995(83) 0.0001452 1604. 3844.
3144(74) 0.0001826 1603. 3247.
2600(67) 0.0002228 1603. 2651.
2312(63) 0.0002520 1603. 2204.
2014(46) 0.000473 1603. 1941.
1709(50) 0.000400 1602. 1826.
1750(51) 0.000384 1602. 1810.
1898(53) 0.000356 1602. 1853.
1969(54) 0.0003429 1602. 1925.
1982(54) 0.0003429 1601. 1997.
2043(55) 0.0003306 1601. 2036.
2035(55) 0.0003306 1601. 2019.
1958(54) 0.0003429 1601. 1954.
1855(53) 0.000356 1600. 1873.
1855(53) 0.000356 1600. 1814.
1859(53) 0.000356 1600. 1807.
1843(52) 0.000370 1600. 1875.
2036(55) 0.0003306 1599. 2044.
2330(59) 0.0002873 1599. 2330.
2706(63) 0.0002520 1599. 2718.
3165(69) 0.0002100 1599. 3132.
3515(72) 0.0001929 1598. 3440.
3546(73) 0.0001877 1598. 3502.
3214(69) 0.0002100 1598. 3272.
2832(65) 0.0002367 1598. 2856.
2496(61) 0.0002687 1597. 2423.
2173(57) 0.0003078 1597. 2091.
1915(53) 0.000356 1597. 1896.
1860(53) 0.000356 1597. 1825.
1826(52) 0.000370 1596. 1845.
1976(54) 0.0003429 1596. 1927.
2176(57) 0.0003078 1596. 2039.
2242(58) 0.0002973 1596. 2138.
2308(59) 0.0002873 1595. 2181.
2166(57) 0.0003078 1595. 2139.
2094(56) 0.0003189 1595. 2029.
1936(54) 0.0003429 1595. 1899.
1842(52) 0.000370 1594. 1792.
1755(51) 0.000384 1594. 1728.
1717(51) 0.000384 1594. 1709.
1786(52) 0.000370 1594. 1731.
1883(53) 0.000356 1593. 1785.
1899(53) 0.000356 1593. 1859.
2007(55) 0.0003306 1593. 1928.
2024(55) 0.0003306 1593. 1966.
1991(54) 0.0003429 1592. 1950.
1866(53) 0.000356 1592. 1886.
1828(52) 0.000370 1592. 1802.
1762(51) 0.000384 1592. 1726.
1690(50) 0.000400 1591. 1674.
1682(50) 0.000400 1591. 1646.
1597(49) 0.000416 1591. 1638.
1587(49) 0.000416 1590. 1641.
1530(48) 0.000434 1590. 1653.
1621(49) 0.000416 1590. 1665.
1688(50) 0.000400 1590. 1673.
1724(51) 0.000384 1589. 1670.
1640(49) 0.000416 1589. 1658.
1588(49) 0.000416 1589. 1644.
1551(48) 0.000434 1589. 1633.
1604(49) 0.000416 1588. 1631.
1662(50) 0.000400 1588. 1642.
1663(50) 0.000400 1588. 1670.
1695(50) 0.000400 1587. 1714.
1782(52) 0.000370 1587. 1770.
1771(51) 0.000384 1587. 1821.
1904(53) 0.000356 1587. 1849.
1794(52) 0.000370 1586. 1839.
1772(51) 0.000384 1586. 1793.
1708(50) 0.000400 1586. 1733.
1701(50) 0.000400 1585. 1678.
1604(49) 0.000416 1585. 1639.
1599(49) 0.000416 1585. 1615.
1604(49) 0.000416 1585. 1603.
1595(49) 0.000416 1584. 1598.
1708(50) 0.000400 1584. 1594.
1545(48) 0.000434 1584. 1593.
1552(48) 0.000434 1583. 1592.
1632(49) 0.000416 1583. 1592.
1620(49) 0.000416 1583. 1592.
1568(48) 0.000434 1583. 1592.
1563(48) 0.000434 1582. 1594.
1613(49) 0.000416 1582. 1597.
1592(49) 0.000416 1582. 1603.
1611(49) 0.000416 1581. 1612.
1628(49) 0.000416 1581. 1624.
1616(49) 0.000416 1581. 1637.
1614(49) 0.000416 1581. 1648.
1704(50) 0.000400 1580. 1651.
1624(49) 0.000416 1580. 1647.
1588(49) 0.000416 1580. 1640.
1651(50) 0.000400 1579. 1638.
1621(49) 0.000416 1579. 1650.
1651(50) 0.000400 1579. 1686.
1619(49) 0.000416 1578. 1757.
1745(51) 0.000384 1578. 1865.
1970(54) 0.0003429 1578. 1999.
2069(56) 0.0003189 1578. 2125.
2039(55) 0.0003306 1577. 2198.
2058(55) 0.0003306 1577. 2181.
2012(55) 0.0003306 1577. 2081.
1958(54) 0.0003429 1576. 1944.
1804(52) 0.000370 1576. 1821.
1742(51) 0.000384 1576. 1740.
1674(47) 0.000453 1575. 1711.
1719(47) 0.000453 1575. 1727.
1809(49) 0.000416 1575. 1775.
1850(49) 0.000416 1574. 1836.
1895(50) 0.000400 1574. 1885.
1878(50) 0.000400 1574. 1897.
1901(50) 0.000400 1574. 1864.
1830(49) 0.000416 1573. 1800.
1732(48) 0.000434 1573. 1734.
1692(47) 0.000453 1573. 1685.
1694(47) 0.000453 1572. 1665.
1731(48) 0.000434 1572. 1674.
1680(47) 0.000453 1572. 1707.
1739(48) 0.000434 1571. 1754.
1779(48) 0.000434 1571. 1797.
1829(49) 0.000416 1571. 1818.
1816(49) 0.000416 1570. 1804.
1722(47) 0.000453 1570. 1761.
1680(47) 0.000453 1570. 1706.
1649(46) 0.000473 1570. 1657.
1630(46) 0.000473 1569. 1623.
1645(46) 0.000473 1569. 1602.
1609(46) 0.000473 1569. 1591.
1576(45) 0.000494 1568. 1587.
1580(45) 0.000494 1568. 1586.
1610(46) 0.000473 1568. 1586.
1657(47) 0.000453 1567. 1587.
1633(46) 0.000473 1567. 1591.
1554(45) 0.000494 1567. 1599.
1647(46) 0.000473 1566. 1617.
1732(48) 0.000434 1566. 1653.
1774(48) 0.000434 1566. 1716.
1906(50) 0.000400 1565. 1813.
1981(51) 0.000384 1565. 1936.
2195(54) 0.0003429 1565. 2059.
2329(55) 0.0003306 1564. 2141.
2337(55) 0.0003306 1564. 2144.
2142(53) 0.000356 1564. 2064.
2003(51) 0.000384 1563. 1937.
1852(49) 0.000416 1563. 1809.
1738(48) 0.000434 1563. 1709.
1657(47) 0.000453 1562. 1644.
1667(47) 0.000453 1562. 1609.
1657(47) 0.000453 1562. 1592.
1605(46) 0.000473 1561. 1583.
1646(46) 0.000473 1561. 1580.
1610(46) 0.000473 1561. 1577.
1597(46) 0.000473 1560. 1576.
1607(46) 0.000473 1560. 1574.
1691(47) 0.000453 1560. 1573.
1664(47) 0.000453 1559. 1573.
1626(46) 0.000473 1559. 1572.
1584(45) 0.000494 1559. 1572.
1620(46) 0.000473 1558. 1572.
1557(45) 0.000494 1558. 1572.
1536(45) 0.000494 1558. 1573.
1591(46) 0.000473 1557. 1574.
1647(46) 0.000473 1557. 1577.
1641(46) 0.000473 1557. 1582.
1628(46) 0.000473 1556. 1594.
1640(46) 0.000473 1556. 1615.
1637(46) 0.000473 1556. 1653.
1669(47) 0.000453 1555. 1708.
1792(48) 0.000434 1555. 1777.
1836(49) 0.000416 1555. 1844.
1926(50) 0.000400 1554. 1888.
1953(51) 0.000384 1554. 1888.
1805(49) 0.000416 1554. 1846.
1823(49) 0.000416 1553. 1784.
1763(48) 0.000434 1553. 1730.
1710(47) 0.000453 1553. 1704.
1753(48) 0.000434 1552. 1714.
1749(48) 0.000434 1552. 1760.
1843(49) 0.000416 1552. 1827.
1929(50) 0.000400 1551. 1893.
1925(50) 0.000400 1551. 1933.
1942(50) 0.000400 1551. 1928.
1841(49) 0.000416 1550. 1886.
1873(50) 0.000400 1550. 1841.
1865(49) 0.000416 1550. 1832.
1910(50) 0.000400 1549. 1893.
2035(52) 0.000370 1549. 2041.
2215(54) 0.0003429 1549. 2271.
2538(58) 0.0002973 1548. 2538.
2810(61) 0.0002687 1548. 2762.
2823(61) 0.0002687 1547. 2851.
2730(60) 0.0002778 1547. 2758.
2434(57) 0.0003078 1547. 2529.
2274(55) 0.0003306 1546. 2263.
2086(52) 0.000370 1546. 2048.
1939(50) 0.000400 1546. 1929.
1901(50) 0.000400 1545. 1909.
1961(51) 0.000384 1545. 1964.
2092(52) 0.000370 1545. 2050.
2064(52) 0.000370 1544. 2117.
2011(51) 0.000384 1544. 2124.
1948(50) 0.000400 1544. 2061.
1884(50) 0.000400 1543. 1961.
1822(49) 0.000416 1543. 1871.
1804(49) 0.000416 1543. 1828.
1887(47) 0.000453 1542. 1851.
2051(49) 0.000416 1542. 1937.
2178(50) 0.000400 1541. 2061.
2285(52) 0.000370 1541. 2178.
2422(53) 0.000356 1541. 2238.
2430(53) 0.000356 1540. 2205.
2264(51) 0.000384 1540. 2095.
2030(49) 0.000416 1540. 1955.
1945(48) 0.000434 1539. 1833.
1771(45) 0.000494 1539. 1757.
1706(45) 0.000494 1539. 1731.
1796(46) 0.000473 1538. 1745.
1800(46) 0.000473 1538. 1777.
1825(46) 0.000473 1537. 1804.
1833(46) 0.000473 1537. 1804.
1839(46) 0.000473 1537. 1772.
1746(45) 0.000494 1536. 1722.
1669(44) 0.000517 1536. 1671.
1584(43) 0.000541 1536. 1634.
1612(43) 0.000541 1535. 1614.
1642(44) 0.000517 1535. 1611.
1668(44) 0.000517 1535. 1618.
1647(44) 0.000517 1534. 1627.
1719(45) 0.000494 1534. 1630.
1637(44) 0.000517 1533. 1623.
1651(44) 0.000517 1533. 1607.
1597(43) 0.000541 1533. 1589.
1583(43) 0.000541 1532. 1572.
1595(43) 0.000541 1532. 1560.
1570(43) 0.000541 1532. 1552.
1537(42) 0.000567 1531. 1548.
1540(42) 0.000567 1531. 1546.
1555(42) 0.000567 1531. 1545.
1511(42) 0.000567 1530. 1545.
1550(42) 0.000567 1530. 1546.
1504(42) 0.000567 1529. 1548.
1547(42) 0.000567 1529. 1553.
1612(43) 0.000541 1529. 1563.
1598(43) 0.000541 1528. 1577.
1565(43) 0.000541 1528. 1595.
1600(43) 0.000541 1528. 1614.
1640(44) 0.000517 1527. 1628.
1567(43) 0.000541 1527. 1634.
1549(42) 0.000567 1526. 1631.
1622(43) 0.000541 1526. 1628.
1585(43) 0.000541 1526. 1637.
1637(44) 0.000517 1525. 1670.
1770(45) 0.000494 1525. 1734.
1796(46) 0.000473 1525. 1825.
1854(46) 0.000473 1524. 1926.
2008(48) 0.000434 1524. 2006.
2029(49) 0.000416 1523. 2031.
1961(48) 0.000434 1523. 1989.
1889(47) 0.000453 1523. 1898.
1764(45) 0.000494 1522. 1793.
1710(45) 0.000494 1522. 1702.
1697(44) 0.000517 1522. 1638.
1662(44) 0.000517 1521. 1602.
1658(44) 0.000517 1521. 1586.
1671(44) 0.000517 1520. 1581.
1614(43) 0.000541 1520. 1581.
1589(43) 0.000541 1520. 1582.
1581(43) 0.000541 1519. 1589.
1639(44) 0.000517 1519. 1608.
1660(44) 0.000517 1519. 1647.
1731(45) 0.000494 1518. 1714.
1791(46) 0.000473 1518. 1809.
1854(46) 0.000473 1517. 1916.
1942(48) 0.000434 1517. 2008.
1942(48) 0.000434 1517. 2051.
1926(47) 0.000453 1516. 2023.
1793(46) 0.000473 1516. 1936.
1749(45) 0.000494 1516. 1826.
1663(44) 0.000517 1515. 1723.
1679(44) 0.000517 1515. 1645.
1629(43) 0.000541 1514. 1594.
1567(43) 0.000541 1514. 1566.
1573(43) 0.000541 1514. 1553.
1524(42) 0.000567 1513. 1549.
1520(42) 0.000567 1513. 1552.
1549(42) 0.000567 1513. 1563.
1692(44) 0.000517 1512. 1587.
1670(44) 0.000517 1512. 1631.
1683(44) 0.000517 1511. 1701.
1801(46) 0.000473 1511. 1794.
1945(48) 0.000434 1511. 1898.
2020(48) 0.000434 1510. 1987.
2168(50) 0.000400 1510. 2029.
2101(49) 0.000416 1509. 2006.
1991(48) 0.000434 1509. 1930.
1860(46) 0.000473 1509. 1838.
1741(45) 0.000494 1508. 1763.
1828(46) 0.000473 1508. 1723.
1747(45) 0.000494 1508. 1720.
1769(45) 0.000494 1507. 1743.
1823(46) 0.000473 1507. 1771.
1801(46) 0.000473 1506. 1781.
1816(46) 0.000473 1506. 1760.
1726(45) 0.000494 1506. 1715.
1654(44) 0.000517 1505. 1661.
1649(42) 0.000567 1505. 1611.
1659(42) 0.000567 1504. 1574.
1549(40) 0.000625 1504. 1549.
1496(40) 0.000625 1504. 1535.
1500(40) 0.000625 1503. 1528.
1544(40) 0.000625 1503. 1525.
1510(40) 0.000625 1503. 1524.
1586(41) 0.000595 1502. 1527.
1547(40) 0.000625 1502. 1533.
1567(41) 0.000595 1501. 1544.
1494(40) 0.000625 1501. 1559.
1587(41) 0.000595 1501. 1579.
1603(41) 0.000595 1500. 1600.
1623(41) 0.000595 1500. 1616.
1721(42) 0.000567 1500. 1623.
1678(42) 0.000567 1499. 1622.
1650(42) 0.000567 1499. 1622.
1627(41) 0.000595 1498. 1634.
1667(42) 0.000567 1498. 1667.
1689(42) 0.000567 1498. 1725.
1841(44) 0.000517 1497. 1801.
1894(44) 0.000517 1497. 1875.
1933(45) 0.000494 1496. 1923.
1895(45) 0.000494 1496. 1924.
1856(44) 0.000517 1496. 1883.
1785(43) 0.000541 1495. 1825.
1785(43) 0.000541 1495. 1781.
1746(43) 0.000541 1494. 1771.
1761(43) 0.000541 1494. 1800.
1810(44) 0.000517 1494. 1852.
1897(45) 0.000494 1493. 1904.
1954(45) 0.000494 1493. 1923.
1901(45) 0.000494 1493. 1895.
1795(43) 0.000541 1492. 1826.
1640(41) 0.000595 1492. 1741.
1591(41) 0.000595 1491. 1662.
1565(41) 0.000595 1491. 1601.
1552(40) 0.000625 1491. 1561.
1558(40) 0.000625 1490. 1537.
1496(40) 0.000625 1490. 1525.
1439(39) 0.000657 1489. 1520.
1551(40) 0.000625 1489. 1520.
1510(40) 0.000625 1489. 1524.
1506(40) 0.000625 1488. 1534.
1512(40) 0.000625 1488. 1552.
1553(40) 0.000625 1488. 1577.
1574(41) 0.000595 1487. 1606.
1579(41) 0.000595 1487. 1631.
1620(41) 0.000595 1486. 1646.
1605(41) 0.000595 1486. 1642.
1590(41) 0.000595 1486. 1623.
1567(41) 0.000595 1485. 1597.
1536(40) 0.000625 1485. 1574.
1552(40) 0.000625 1484. 1560.
1538(40) 0.000625 1484. 1555.
1586(41) 0.000595 1484. 1556.
1493(40) 0.000625 1483. 1560.
1536(40) 0.000625 1483. 1560.
1548(40) 0.000625 1483. 1553.
1489(40) 0.000625 1482. 1543.
1512(40) 0.000625 1482. 1531.
1473(39) 0.000657 1481. 1522.
1473(39) 0.000657 1481. 1517.
1494(40) 0.000625 1481. 1516.
1464(39) 0.000657 1480. 1517.
1441(39) 0.000657 1480. 1517.
1493(40) 0.000625 1480. 1516.
1532(40) 0.000625 1479. 1512.
1547(40) 0.000625 1479. 1507.
1554(40) 0.000625 1478. 1502.
1528(40) 0.000625 1478. 1499.
1458(39) 0.000657 1478. 1496.
1498(40) 0.000625 1477. 1495.
1470(39) 0.000657 1477. 1495.
1503(40) 0.000625 1476. 1496.
1502(40) 0.000625 1476. 1498.
1501(40) 0.000625 1476. 1501.
1480(39) 0.000657 1475. 1506.
1547(40) 0.000625 1475. 1513.
1512(40) 0.000625 1475. 1524.
1534(40) 0.000625 1474. 1535.
1521(40) 0.000625 1474. 1548.
1490(40) 0.000625 1473. 1563.
1545(40) 0.000625 1473. 1582.
1609(41) 0.000595 1473. 1613.
1568(41) 0.000595 1472. 1668.
1715(42) 0.000567 1472. 1758.
1887(44) 0.000517 1472. 1887.
2090(47) 0.000453 1471. 2042.
2282(49) 0.000416 1471. 2195.
2380(50) 0.000400 1470. 2306.
2355(50) 0.000400 1470. 2338.
2319(49) 0.000416 1470. 2293.
2323(49) 0.000416 1469. 2213.
2135(47) 0.000453 1469. 2158.
2170(48) 0.000434 1469. 2167.
2262(49) 0.000416 1468. 2247.
2353(50) 0.000400 1468. 2372.
2467(51) 0.000384 1467. 2484.
2433(50) 0.000400 1467. 2523.
2360(48) 0.000434 1467. 2456.
2166(46) 0.000473 1466. 2306.
2118(46) 0.000473 1466. 2130.
1940(44) 0.000517 1466. 1977.
1866(43) 0.000541 1465. 1873.
1736(41) 0.000595 1465. 1819.
1752(41) 0.000595 1464. 1798.
1741(41) 0.000595 1464. 1785.
1727(41) 0.000595 1464. 1760.
1656(40) 0.000625 1463. 1716.
1617(40) 0.000625 1463. 1664.
1610(40) 0.000625 1463. 1613.
1585(39) 0.000657 1462. 1573.
1497(38) 0.000693 1462. 1545.
1534(39) 0.000657 1461. 1528.
1535(39) 0.000657 1461. 1519.
1546(39) 0.000657 1461. 1515.
1479(38) 0.000693 1460. 1514.
1524(39) 0.000657 1460. 1517.
1489(38) 0.000693 1460. 1526.
1494(38) 0.000693 1459. 1541.
1533(39) 0.000657 1459. 1560.
1589(39) 0.000657 1458. 1581.
1612(40) 0.000625 1458. 1596.
1550(39) 0.000657 1458. 1599.
1569(39) 0.000657 1457. 1590.
1556(39) 0.000657 1457. 1573.
1582(39) 0.000657 1457. 1554.
1514(38) 0.000693 1456. 1541.
1604(40) 0.000625 1456. 1534.
1496(38) 0.000693 1456. 1533.
1559(39) 0.000657 1455. 1534.
1588(39) 0.000657 1455. 1533.
1672(40) 0.000625 1454. 1527.
1644(40) 0.000625 1454. 1518.
1676(40) 0.000625 1454. 1506.
1563(39) 0.000657 1453. 1496.
1577(39) 0.000657 1453. 1488.
1508(38) 0.000693 1453. 1484.
1469(38) 0.000693 1452. 1483.
1537(39) 0.000657 1452. 1487.
1519(39) 0.000657 1452. 1497.
1534(39) 0.000657 1451. 1515.
1535(39) 0.000657 1451. 1544.
1579(39) 0.000657 1450. 1587.
1679(41) 0.000595 1450. 1641.
1742(41) 0.000595 1450. 1700.
1693(41) 0.000595 1449. 1753.
1769(42) 0.000567 1449. 1787.
1817(42) 0.000567 1449. 1797.
1773(42) 0.000567 1448. 1794.
1850(43) 0.000541 1448. 1797.
1841(42) 0.000567 1448. 1826.
1985(44) 0.000517 1447. 1885.
2076(45) 0.000494 1447. 1965.
2140(46) 0.000473 1447. 2042.
2156(46) 0.000473 1446. 2083.
2063(45) 0.000494 1446. 2064.
1989(44) 0.000517 1445. 1990.
1836(42) 0.000567 1445. 1889.
1805(42) 0.000567 1445. 1789.
1656(40) 0.000625 1444. 1709.
1627(40) 0.000625 1444. 1656.
1574(39) 0.000657 1444. 1626.
1511(38) 0.000693 1443. 1607.
1523(39) 0.000657 1443. 1589.
1604(40) 0.000625 1443. 1568.
1522(39) 0.000657 1442. 1545.
1505(38) 0.000693 1442. 1523.
1479(38) 0.000693 1442. 1506.
1485(38) 0.000693 1441. 1495.
1489(38) 0.000693 1441. 1488.
1461(38) 0.000693 1441. 1486.
1508(38) 0.000693 1440. 1487.
1479(38) 0.000693 1440. 1492.
1504(38) 0.000693 1440. 1503.
1528(39) 0.000657 1439. 1520.
1602(40) 0.000625 1439. 1543.
1636(40) 0.000625 1439. 1569.
1700(41) 0.000595 1438. 1592.
1629(40) 0.000625 1438. 1605.
1749(41) 0.000595 1437. 1605.
1581(39) 0.000657 1437. 1591.
1631(40) 0.000625 1437. 1571.
1640(40) 0.000625 1436. 1553.
1586(39) 0.000657 1436. 1541.
1519(39) 0.000657 1436. 1537.
1549(39) 0.000657 1435. 1540.
1589(39) 0.000657 1435. 1548.
1576(39) 0.000657 1435. 1561.
1580(39) 0.000657 1434. 1584.
1590(39) 0.000657 1434. 1623.
1603(40) 0.000625 1434. 1682.
1697(41) 0.000595 1433. 1758.
1843(42) 0.000567 1433. 1840.
1889(43) 0.000541 1433. 1911.
1959(44) 0.000517 1432. 1944.
1875(43) 0.000541 1432. 1925.
1815(42) 0.000567 1432. 1862.
1764(42) 0.000567 1431. 1774.
1677(39) 0.000657 1431. 1684.
1618(38) 0.000693 1431. 1608.
1516(37) 0.000730 1430. 1551.
1475(37) 0.000730 1430. 1516.
1436(36) 0.000772 1430. 1498.
1450(36) 0.000772 1429. 1496.
1508(37) 0.000730 1429. 1505.
1534(37) 0.000730 1429. 1526.
1533(37) 0.000730 1428. 1556.
1598(38) 0.000693 1428. 1592.
1646(39) 0.000657 1428. 1626.
1659(39) 0.000657 1428. 1650.
1659(39) 0.000657 1427. 1659.
1675(39) 0.000657 1427. 1651.
1652(39) 0.000657 1427. 1637.
1609(38) 0.000693 1426. 1627.
1612(38) 0.000693 1426. 1627.
1587(38) 0.000693 1426. 1638.
1608(38) 0.000693 1425. 1657.
1593(38) 0.000693 1425. 1678.
1635(38) 0.000693 1425. 1699.
1665(39) 0.000657 1424. 1724.
1737(40) 0.000625 1424. 1766.
1860(41) 0.000595 1424. 1835.
2030(43) 0.000541 1423. 1931.
2058(43) 0.000541 1423. 2040.
2188(45) 0.000494 1423. 2137.
2262(45) 0.000494 1422. 2187.
2233(45) 0.000494 1422. 2168.
2139(44) 0.000517 1422. 2089.
2035(43) 0.000541 1422. 1979.
1949(42) 0.000567 1421. 1872.
1824(41) 0.000595 1421. 1786.
1759(40) 0.000625 1421. 1727.
1643(39) 0.000657 1420. 1689.
1621(38) 0.000693 1420. 1660.
1564(38) 0.000693 1420. 1629.
1580(38) 0.000693 1419. 1594.
1507(37) 0.000730 1419. 1557.
1449(36) 0.000772 1419. 1523.
1454(36) 0.000772 1418. 1495.
1453(36) 0.000772 1418. 1474.
1425(36) 0.000772 1418. 1459.
1426(36) 0.000772 1418. 1450.
1452(36) 0.000772 1417. 1444.
1428(36) 0.000772 1417. 1441.
1420(36) 0.000772 1417. 1439.
1456(36) 0.000772 1416. 1438.
1488(37) 0.000730 1416. 1438.
1471(36) 0.000772 1416. 1440.
1460(36) 0.000772 1415. 1444.
1502(37) 0.000730 1415. 1451.
1436(36) 0.000772 1415. 1464.
1487(37) 0.000730 1415. 1484.
1500(37) 0.000730 1414. 1511.
1507(37) 0.000730 1414. 1543.
1515(37) 0.000730 1414. 1577.
1571(38) 0.000693 1413. 1605.
1566(38) 0.000693 1413. 1619.
1576(38) 0.000693 1413. 1613.
1521(37) 0.000730 1413. 1590.
1529(37) 0.000730 1412. 1558.
1508(37) 0.000730 1412. 1524.
1511(37) 0.000730 1412. 1495.
1493(37) 0.000730 1411. 1473.
1475(37) 0.000730 1411. 1458.
1406(36) 0.000772 1411. 1451.
1452(36) 0.000772 1411. 1450.
1431(36) 0.000772 1410. 1454.
1475(37) 0.000730 1410. 1463.
1491(37) 0.000730 1410. 1476.
1486(37) 0.000730 1409. 1492.
1518(37) 0.000730 1409. 1510.
1553(37) 0.000730 1409. 1531.
1599(38) 0.000693 1409. 1556.
1600(38) 0.000693 1408. 1589.
1610(38) 0.000693 1408. 1637.
1682(39) 0.000657 1408. 1702.
1722(39) 0.000657 1407. 1782.
1744(40) 0.000625 1407. 1866.
1799(40) 0.000625 1407. 1936.
1849(41) 0.000595 1407. 1970.
1804(40) 0.000625 1406. 1955.
1811(40) 0.000625 1406. 1898.
1726(40) 0.000625 1406. 1818.
1655(39) 0.000657 1406. 1738.
1632(38) 0.000693 1405. 1670.
1624(38) 0.000693 1405. 1620.
1572(38) 0.000693 1405. 1588.
1565(38) 0.000693 1404. 1568.
1588(38) 0.000693 1404. 1556.
1595(38) 0.000693 1404. 1552.
1599(38) 0.000693 1404. 1556.
1542(37) 0.000730 1403. 1567.
1598(38) 0.000693 1403. 1584.
1623(38) 0.000693 1403. 1601.
1610(38) 0.000693 1403. 1612.
1634(38) 0.000693 1402. 1613.
1585(38) 0.000693 1402. 1604.
1580(38) 0.000693 1402. 1593.
1618(53) 0.000356 1402. 1584.
1562(36) 0.000772 1401. 1582.
1529(36) 0.000772 1401. 1586.
1551(36) 0.000772 1401. 1595.
1554(36) 0.000772 1401. 1605.
1538(36) 0.000772 1400. 1615.
1576(36) 0.000772 1400. 1629.
1638(37) 0.000730 1400. 1651.
1625(37) 0.000730 1399. 1684.
1709(38) 0.000693 1399. 1724.
1720(38) 0.000693 1399. 1761.
1737(38) 0.000693 1399. 1782.
1708(38) 0.000693 1398. 1774.
1713(38) 0.000693 1398. 1738.
1698(38) 0.000693 1398. 1683.
1637(37) 0.000730 1398. 1622.
1603(37) 0.000730 1397. 1566.
1557(36) 0.000772 1397. 1520.
1488(35) 0.000816 1397.0 1485.9
1441(35) 0.000816 1396.8 1462.3
1420(35) 0.000816 1396.5 1446.8
1384(34) 0.000865 1396.3 1436.6
1416(34) 0.000865 1396.0 1430.0
1452(35) 0.000816 1395.8 1425.7
1442(35) 0.000816 1395.5 1423.2
1440(35) 0.000816 1395.3 1422.6
1431(35) 0.000816 1395.1 1424.2
1453(35) 0.000816 1394.8 1428.5
1428(35) 0.000816 1394.6 1436.0
1452(35) 0.000816 1394.4 1447.2
1438(35) 0.000816 1394.1 1461.9
1465(35) 0.000816 1393.9 1479.4
1540(36) 0.000772 1394. 1498.
1505(36) 0.000772 1393. 1516.
1509(36) 0.000772 1393. 1531.
1554(36) 0.000772 1393. 1543.
1544(36) 0.000772 1393. 1555.
1563(36) 0.000772 1392. 1572.
1614(37) 0.000730 1392. 1595.
1673(37) 0.000730 1392. 1621.
1745(38) 0.000693 1392. 1647.
1748(38) 0.000693 1392. 1664.
1728(38) 0.000693 1391. 1667.
1737(38) 0.000693 1391. 1656.
1683(38) 0.000693 1391. 1639.
1665(37) 0.000730 1391. 1623.
1687(38) 0.000693 1390. 1613.
1638(37) 0.000730 1390. 1608.
1582(36) 0.000772 1390. 1606.
1583(36) 0.000772 1390. 1602.
1576(36) 0.000772 1390. 1594.
1587(36) 0.000772 1389. 1583.
1573(36) 0.000772 1389. 1574.
1586(36) 0.000772 1389. 1569.
1564(36) 0.000772 1389. 1570.
1574(36) 0.000772 1388. 1574.
1565(36) 0.000772 1388. 1577.
1638(37) 0.000730 1388. 1579.
1569(36) 0.000772 1388. 1578.
1594(37) 0.000730 1388. 1580.
1611(37) 0.000730 1387. 1585.
1626(37) 0.000730 1387. 1595.
1613(37) 0.000730 1387. 1606.
1594(37) 0.000730 1387. 1614.
1610(37) 0.000730 1387. 1610.
1581(36) 0.000772 1386. 1594.
1541(36) 0.000772 1386. 1569.
1493(35) 0.000816 1385.9 1540.8
1479(35) 0.000816 1385.7 1514.8
1501(35) 0.000816 1385.5 1493.7
1462(35) 0.000816 1385.2 1478.9
1466(35) 0.000816 1385.0 1469.9
1460(35) 0.000816 1384.8 1465.9
1478(35) 0.000816 1384.6 1466.6
1537(36) 0.000772 1384. 1472.
1548(36) 0.000772 1384. 1480.
1564(36) 0.000772 1384. 1490.
1550(36) 0.000772 1384. 1500.
1498(35) 0.000816 1383.6 1504.2
1528(36) 0.000772 1383. 1501.
1553(36) 0.000772 1383. 1491.
1546(36) 0.000772 1383. 1476.
1471(35) 0.000816 1382.8 1458.5
1493(35) 0.000816 1382.6 1442.0
1450(35) 0.000816 1382.4 1428.1
1423(35) 0.000816 1382.2 1417.5
1401(34) 0.000865 1382.0 1410.2
1425(35) 0.000816 1381.8 1405.7
1389(34) 0.000865 1381.6 1403.4
1383(34) 0.000865 1381.4 1402.9
1397(34) 0.000865 1381.2 1404.0
1390(34) 0.000865 1381.0 1407.1
1403(34) 0.000865 1380.9 1412.8
1399(34) 0.000865 1380.7 1422.3
1459(35) 0.000816 1380.5 1436.8
1499(35) 0.000816 1380.3 1457.1
1480(35) 0.000816 1380.1 1483.3
1548(36) 0.000772 1380. 1515.
1598(37) 0.000730 1380. 1548.
1619(37) 0.000730 1380. 1581.
1628(37) 0.000730 1379. 1608.
1630(37) 0.000730 1379. 1627.
1652(37) 0.000730 1379. 1639.
1664(37) 0.000730 1379. 1650.
1621(37) 0.000730 1379. 1663.
1645(37) 0.000730 1378. 1680.
1702(38) 0.000693 1378. 1697.
1706(38) 0.000693 1378. 1707.
1670(38) 0.000693 1378. 1703.
1581(37) 0.000730 1378. 1682.
1606(37) 0.000730 1377. 1648.
1644(37) 0.000730 1377. 1609.
1573(36) 0.000772 1377. 1570.
1498(36) 0.000772 1377. 1537.
1555(36) 0.000772 1377. 1510.
1511(36) 0.000772 1377. 1489.
1477(35) 0.000816 1376.4 1471.3
1485(35) 0.000816 1376.2 1456.8
1439(35) 0.000816 1376.1 1444.7
1449(35) 0.000816 1375.9 1435.0
1434(35) 0.000816 1375.7 1427.6
1390(34) 0.000865 1375.5 1422.4
1430(35) 0.000816 1375.4 1418.9
1411(35) 0.000816 1375.2 1416.8
1396(34) 0.000865 1375.0 1415.9
1403(34) 0.000865 1374.9 1416.3
1408(35) 0.000816 1374.7 1417.9
1400(34) 0.000865 1374.5 1420.4
1473(35) 0.000816 1374.3 1423.5
1474(35) 0.000816 1374.2 1426.7
1443(35) 0.000816 1374.0 1429.6
1508(36) 0.000772 1374. 1432.
1475(35) 0.000816 1373.7 1435.0
1478(35) 0.000816 1373.5 1438.4
1504(36) 0.000772 1373. 1443.
1521(36) 0.000772 1373. 1447.
1512(36) 0.000772 1373. 1449.
1472(35) 0.000816 1372.8 1449.0
1503(36) 0.000772 1373. 1445.
1461(35) 0.000816 1372.5 1439.1
1441(35) 0.000816 1372.3 1431.5
1388(34) 0.000865 1372.2 1424.1
1388(34) 0.000865 1372.0 1417.7
1400(34) 0.000865 1371.8 1413.2
1372(34) 0.000865 1371.7 1410.9
1415(35) 0.000816 1371.5 1411.0
1384(34) 0.000865 1371.4 1414.0
1406(34) 0.000865 1371.2 1420.7
1420(35) 0.000816 1371.0 1433.0
1427(35) 0.000816 1370.9 1453.9
1471(35) 0.000816 1370.7 1487.5
1499(36) 0.000772 1371. 1539.
1549(36) 0.000772 1370. 1614.
1705(38) 0.000693 1370. 1714.
1828(39) 0.000657 1370. 1838.
1989(41) 0.000595 1370. 1978.
2088(42) 0.000567 1370. 2120.
2254(44) 0.000517 1370. 2242.
2354(44) 0.000517 1369. 2319.
2292(44) 0.000517 1369. 2332.
2244(43) 0.000541 1369. 2281.
2209(43) 0.000541 1369. 2184.
2069(42) 0.000567 1369. 2067.
2012(41) 0.000595 1369. 1951.
1898(40) 0.000625 1369. 1849.
1770(39) 0.000657 1368. 1766.
1730(38) 0.000693 1368. 1704.
1688(38) 0.000693 1368. 1658.
1670(38) 0.000693 1368. 1626.
1628(37) 0.000730 1368. 1606.
1677(38) 0.000693 1368. 1595.
1611(37) 0.000730 1367. 1589.
1600(37) 0.000730 1367. 1583.
1598(37) 0.000730 1367. 1573.
1561(36) 0.000772 1367. 1557.
1588(37) 0.000730 1367. 1535.
1536(36) 0.000772 1367. 1511.
1536(36) 0.000772 1367. 1488.
1507(36) 0.000772 1366. 1470.
1481(35) 0.000816 1366.3 1459.9
1485(35) 0.000816 1366.1 1458.2
1450(35) 0.000816 1366.0 1465.9
1498(36) 0.000772 1366. 1482.
1513(36) 0.000772 1366. 1506.
1528(36) 0.000772 1366. 1535.
1573(36) 0.000772 1365. 1563.
1581(37) 0.000730 1365. 1587.
1591(37) 0.000730 1365. 1599.
1606(37) 0.000730 1365. 1599.
1580(37) 0.000730 1365. 1585.
1537(36) 0.000772 1365. 1564.
1536(36) 0.000772 1365. 1539.
1519(36) 0.000772 1364. 1515.
1510(36) 0.000772 1364. 1494.
1499(36) 0.000772 1364. 1475.
1462(35) 0.000816 1364.0 1458.4
1433(35) 0.000816 1363.9 1443.4
1486(35) 0.000816 1363.7 1430.0
1437(35) 0.000816 1363.6 1418.4
1342(34) 0.000865 1363.4 1408.7
1418(28) 0.001276 1363.3 1401.0
1354(34) 0.000865 1363.2 1395.4
1353(34) 0.000865 1363.0 1391.7
1327(34) 0.000865 1362.9 1389.9
1365(34) 0.000865 1362.7 1389.7
1394(34) 0.000865 1362.6 1391.4
1410(35) 0.000816 1362.5 1395.3
1438(35) 0.000816 1362.3 1401.3
1414(35) 0.000816 1362.2 1410.2
1448(35) 0.000816 1362.0 1422.6
1427(35) 0.000816 1361.9 1438.9
1480(35) 0.000816 1361.8 1458.9
1452(35) 0.000816 1361.6 1482.1
1509(36) 0.000772 1361. 1507.
1528(36) 0.000772 1361. 1530.
1574(36) 0.000772 1361. 1550.
1553(36) 0.000772 1361. 1562.
1544(36) 0.000772 1361. 1567.
1515(36) 0.000772 1361. 1567.
1511(36) 0.000772 1361. 1565.
1537(36) 0.000772 1361. 1564.
1596(37) 0.000730 1360. 1563.
1542(36) 0.000772 1360. 1562.
1531(36) 0.000772 1360. 1561.
1582(36) 0.000772 1360. 1557.
1532(36) 0.000772 1360. 1552.
1501(36) 0.000772 1360. 1549.
1529(36) 0.000772 1360. 1546.
1553(36) 0.000772 1359. 1545.
1576(36) 0.000772 1359. 1543.
1653(37) 0.000730 1359. 1539.
1585(37) 0.000730 1359. 1532.
1580(36) 0.000772 1359. 1522.
1585(37) 0.000730 1359. 1511.
1542(36) 0.000772 1359. 1501.
1526(36) 0.000772 1359. 1491.
1542(36) 0.000772 1358. 1482.
1520(36) 0.000772 1358. 1472.
1489(35) 0.000816 1358.1 1461.5
1460(35) 0.000816 1358.0 1449.7
1454(35) 0.000816 1357.9 1438.0
1447(35) 0.000816 1357.7 1427.3
1439(35) 0.000816 1357.6 1418.5
1410(35) 0.000816 1357.5 1412.5
1417(35) 0.000816 1357.3 1409.4
1469(35) 0.000816 1357.2 1409.4
1436(35) 0.000816 1357.1 1412.1
1424(35) 0.000816 1356.9 1417.1
1432(35) 0.000816 1356.8 1423.4
1417(35) 0.000816 1356.7 1429.9
1416(35) 0.000816 1356.6 1435.0
1419(35) 0.000816 1356.4 1437.6
1456(35) 0.000816 1356.3 1436.7
1378(34) 0.000865 1356.2 1433.0
1389(34) 0.000865 1356.0 1427.7
1393(34) 0.000865 1355.9 1422.7
1417(35) 0.000816 1355.8 1419.6
1393(34) 0.000865 1355.6 1419.8
1404(34) 0.000865 1355.5 1424.4
1388(34) 0.000865 1355.4 1434.2
1409(34) 0.000865 1355.2 1449.2
1423(35) 0.000816 1355.1 1469.1
1478(35) 0.000816 1355.0 1492.6
1507(36) 0.000772 1355. 1518.
1534(36) 0.000772 1355. 1544.
1495(36) 0.000772 1355. 1568.
1532(36) 0.000772 1354. 1589.
1537(36) 0.000772 1354. 1607.
1587(37) 0.000730 1354. 1626.
1581(36) 0.000772 1354. 1648.
1565(36) 0.000772 1354. 1673.
1598(37) 0.000730 1354. 1701.
1644(37) 0.000730 1354. 1731.
1701(38) 0.000693 1354. 1762.
1702(38) 0.000693 1353. 1793.
1759(38) 0.000693 1353. 1826.
1840(39) 0.000657 1353. 1859.
1863(40) 0.000625 1353. 1890.
1906(40) 0.000625 1353. 1912.
1848(39) 0.000657 1353. 1915.
1846(39) 0.000657 1353. 1895.
1871(40) 0.000625 1352. 1850.
1760(38) 0.000693 1352. 1790.
1748(38) 0.000693 1352. 1721.
1691(38) 0.000693 1352. 1653.
1647(37) 0.000730 1352. 1591.
1550(36) 0.000772 1352. 1538.
1522(36) 0.000772 1352. 1495.
1497(36) 0.000772 1352. 1463.
1445(35) 0.000816 1351.4 1438.6
1437(35) 0.000816 1351.3 1421.8
1384(34) 0.000865 1351.1 1410.5
1398(34) 0.000865 1351.0 1403.5
1425(35) 0.000816 1350.9 1399.6
1392(34) 0.000865 1350.7 1398.4
1434(35) 0.000816 1350.6 1399.3
1410(35) 0.000816 1350.5 1402.3
1401(34) 0.000865 1350.3 1407.2
1445(35) 0.000816 1350.2 1414.1
1425(35) 0.000816 1350.1 1422.9
1434(48) 0.000434 1350. 1434.
1474(34) 0.000865 1349.8 1446.2
1468(34) 0.000865 1349.7 1460.5
1535(35) 0.000816 1349.5 1476.3
1495(34) 0.000865 1349.4 1492.8
1486(34) 0.000865 1349.3 1508.4
1539(35) 0.000816 1349.1 1521.3
1565(35) 0.000816 1349.0 1528.9
1491(34) 0.000865 1348.8 1530.0
1534(35) 0.000816 1348.7 1525.5
1503(34) 0.000865 1348.6 1518.4
1452(34) 0.000865 1348.4 1512.9
1483(34) 0.000865 1348.3 1513.4
1473(34) 0.000865 1348.2 1523.9
1544(35) 0.000816 1348.0 1547.6
1559(35) 0.000816 1347.9 1586.1
1640(36) 0.000772 1348. 1639.
1716(37) 0.000730 1348. 1704.
1805(38) 0.000693 1347. 1776.
1795(38) 0.000693 1347. 1846.
1890(39) 0.000657 1347. 1906.
1942(39) 0.000657 1347. 1945.
1943(39) 0.000657 1347. 1956.
1934(39) 0.000657 1347. 1939.
1897(39) 0.000657 1347. 1901.
1826(38) 0.000693 1346. 1852.
1797(38) 0.000693 1346. 1801.
1740(37) 0.000730 1346. 1753.
1642(36) 0.000772 1346. 1714.
1591(35) 0.000816 1345.9 1682.9
1602(35) 0.000816 1345.8 1661.6
1639(36) 0.000772 1346. 1650.
1606(36) 0.000772 1345. 1648.
1649(36) 0.000772 1345. 1653.
1648(36) 0.000772 1345. 1664.
1708(37) 0.000730 1345. 1677.
1675(36) 0.000772 1345. 1690.
1754(37) 0.000730 1345. 1702.
1752(37) 0.000730 1345. 1713.
1744(37) 0.000730 1344. 1724.
1638(36) 0.000772 1344. 1733.
1656(36) 0.000772 1344. 1738.
1645(36) 0.000772 1344. 1734.
1714(37) 0.000730 1344. 1719.
1704(37) 0.000730 1344. 1693.
1669(36) 0.000772 1344. 1659.
1623(36) 0.000772 1343. 1621.
1564(35) 0.000816 1343.3 1584.3
1550(35) 0.000816 1343.2 1550.2
1514(35) 0.000816 1343.0 1520.3
1505(34) 0.000865 1342.9 1495.3
1496(34) 0.000865 1342.7 1475.2
1527(35) 0.000816 1342.6 1459.7
1493(34) 0.000865 1342.4 1448.3
1433(34) 0.000865 1342.3 1440.1
1434(34) 0.000865 1342.1 1434.3
1397(33) 0.000918 1341.9 1429.7
1447(34) 0.000865 1341.8 1425.5
1494(34) 0.000865 1341.6 1421.5
1468(34) 0.000865 1341.5 1417.6
1450(34) 0.000865 1341.3 1414.0
1399(33) 0.000918 1341.2 1410.5
1439(34) 0.000865 1341.0 1407.1
1439(34) 0.000865 1340.9 1403.4
1430(34) 0.000865 1340.7 1399.3
1433(34) 0.000865 1340.6 1394.8
1439(34) 0.000865 1340.4 1390.2
1465(34) 0.000865 1340.2 1385.9
1357(33) 0.000918 1340.1 1382.3
1417(33) 0.000918 1339.9 1379.6
1381(33) 0.000918 1339.8 1378.2
1430(34) 0.000865 1339.6 1378.5
1456(34) 0.000865 1339.5 1380.6
1359(33) 0.000918 1339.3 1385.0
1391(33) 0.000918 1339.1 1392.1
1422(33) 0.000918 1339.0 1402.6
1425(33) 0.000918 1338.8 1416.8
1454(34) 0.000865 1338.7 1435.4
1478(34) 0.000865 1338.5 1458.6
1610(36) 0.000772 1338. 1486.
1576(35) 0.000816 1338.2 1518.4
1617(36) 0.000772 1338. 1554.
1664(36) 0.000772 1338. 1590.
1650(36) 0.000772 1338. 1626.
1718(37) 0.000730 1338. 1659.
1822(38) 0.000693 1337. 1687.
1793(38) 0.000693 1337. 1711.
1800(38) 0.000693 1337. 1731.
1784(37) 0.000730 1337. 1748.
1839(38) 0.000693 1337. 1763.
1784(37) 0.000730 1337. 1772.
1780(37) 0.000730 1336. 1773.
1701(37) 0.000730 1336. 1764.
1732(37) 0.000730 1336. 1748.
1775(37) 0.000730 1336. 1725.
1748(37) 0.000730 1336. 1699.
1732(37) 0.000730 1335. 1672.
1658(36) 0.000772 1335. 1644.
1656(36) 0.000772 1335. 1616.
1620(36) 0.000772 1335. 1586.
1546(35) 0.000816 1334.8 1555.2
1536(35) 0.000816 1334.6 1526.2
1459(34) 0.000865 1334.5 1500.4
1457(34) 0.000865 1334.3 1479.2
1461(34) 0.000865 1334.1 1463.9
1503(34) 0.000865 1333.9 1454.7
1465(34) 0.000865 1333.7 1451.8
1475(34) 0.000865 1333.6 1454.2
1494(34) 0.000865 1333.4 1460.7
1510(34) 0.000865 1333.2 1469.5
1441(34) 0.000865 1333.0 1478.3
1456(34) 0.000865 1332.9 1484.6
1460(34) 0.000865 1332.7 1486.3
1465(34) 0.000865 1332.5 1482.5
1412(33) 0.000918 1332.3 1473.6
1410(33) 0.000918 1332.1 1460.9
1440(34) 0.000865 1332.0 1446.4
1464(34) 0.000865 1331.8 1431.7
1407(33) 0.000918 1331.6 1418.0
1419(33) 0.000918 1331.4 1406.3
1360(33) 0.000918 1331.2 1397.3
1399(33) 0.000918 1331.0 1391.4
1381(33) 0.000918 1330.8 1388.9
1411(33) 0.000918 1330.7 1390.2
1365(33) 0.000918 1330.5 1395.3
1381(33) 0.000918 1330.3 1404.4
1374(33) 0.000918 1330.1 1417.7
1414(33) 0.000918 1329.9 1434.6
1443(34) 0.000865 1329.7 1454.6
1460(34) 0.000865 1329.5 1476.9
1514(34) 0.000865 1329.3 1500.1
1580(35) 0.000816 1329.1 1522.4
1606(35) 0.000816 1328.9 1542.0
1591(35) 0.000816 1328.8 1557.6
1664(36) 0.000772 1329. 1569.
1586(35) 0.000816 1328.4 1576.5
1632(36) 0.000772 1328. 1583.
1714(37) 0.000730 1328. 1591.
1673(36) 0.000772 1328. 1601.
1674(36) 0.000772 1328. 1614.
1635(36) 0.000772 1327. 1629.
1639(36) 0.000772 1327. 1648.
1716(37) 0.000730 1327. 1668.
1737(37) 0.000730 1327. 1689.
1636(36) 0.000772 1327. 1708.
1658(36) 0.000772 1326. 1723.
1663(36) 0.000772 1326. 1729.
1752(37) 0.000730 1326. 1725.
1614(36) 0.000772 1326. 1710.
1662(36) 0.000772 1326. 1687.
1631(36) 0.000772 1325. 1661.
1590(35) 0.000816 1325.2 1636.7
1618(36) 0.000772 1325. 1619.
1578(35) 0.000816 1324.8 1611.5
1583(35) 0.000816 1324.6 1615.1
1633(36) 0.000772 1324. 1630.
1600(35) 0.000816 1324.1 1654.4
1682(36) 0.000772 1324. 1685.
1693(36) 0.000772 1324. 1717.
1752(37) 0.000730 1324. 1743.
1659(36) 0.000772 1323. 1760.
1736(37) 0.000730 1323. 1761.
1777(37) 0.000730 1323. 1747.
1752(37) 0.000730 1323. 1719.
1730(37) 0.000730 1322. 1683.
1695(36) 0.000772 1322. 1642.
1597(35) 0.000816 1322.0 1601.3
1602(35) 0.000816 1321.8 1562.8
1565(35) 0.000816 1321.6 1528.6
1465(34) 0.000865 1321.4 1499.6
1472(34) 0.000865 1321.2 1476.0
1476(34) 0.000865 1320.9 1457.6
1412(33) 0.000918 1320.7 1443.5
1446(34) 0.000865 1320.5 1432.6
1467(34) 0.000865 1320.3 1423.9
1437(34) 0.000865 1320.1 1416.3
1436(34) 0.000865 1319.9 1409.6
1424(33) 0.000918 1319.6 1403.8
1384(33) 0.000918 1319.4 1399.3
1403(33) 0.000918 1319.2 1396.7
1421(33) 0.000918 1319.0 1396.4
1468(34) 0.000865 1318.7 1398.6
1405(33) 0.000918 1318.5 1403.6
1402(33) 0.000918 1318.3 1411.0
1452(34) 0.000865 1318.1 1420.5
1525(35) 0.000816 1317.8 1431.3
1512(34) 0.000865 1317.6 1442.5
1509(34) 0.000865 1317.4 1452.9
1444(34) 0.000865 1317.2 1461.4
1524(35) 0.000816 1316.9 1467.6
1489(34) 0.000865 1316.7 1471.5
1472(34) 0.000865 1316.5 1474.0
1544(35) 0.000816 1316.2 1476.2
1443(34) 0.000865 1316.0 1479.1
1501(34) 0.000865 1315.8 1483.6
1513(34) 0.000865 1315.5 1490.3
1547(35) 0.000816 1315.3 1499.7
1500(34) 0.000865 1315.1 1512.6
1535(35) 0.000816 1314.8 1529.5
1496(34) 0.000865 1314.6 1550.9
1541(35) 0.000816 1314.4 1576.6
1558(36) 0.000772 1314. 1606.
1690(38) 0.000693 1314. 1638.
1795(39) 0.000657 1314. 1672.
1739(38) 0.000693 1313. 1706.
1853(39) 0.000657 1313. 1739.
1884(40) 0.000625 1313. 1768.
1930(40) 0.000625 1313. 1792.
1890(40) 0.000625 1312. 1806.
1923(40) 0.000625 1312. 1807.
1886(40) 0.000625 1312. 1794.
1853(39) 0.000657 1312. 1769.
1827(39) 0.000657 1311. 1735.
1753(38) 0.000693 1311. 1698.
1706(38) 0.000693 1311. 1663.
1612(37) 0.000730 1311. 1632.
1551(36) 0.000772 1310. 1609.
1570(36) 0.000772 1310. 1595.
1595(37) 0.000730 1310. 1588.
1502(35) 0.000816 1309.7 1589.4
1518(36) 0.000772 1309. 1595.
1563(36) 0.000772 1309. 1602.
1606(37) 0.000730 1309. 1606.
1566(36) 0.000772 1309. 1605.
1583(36) 0.000772 1308. 1598.
1595(37) 0.000730 1308. 1583.
1491(35) 0.000816 1308.0 1562.3
1556(36) 0.000772 1308. 1538.
1556(36) 0.000772 1307. 1513.
1486(35) 0.000816 1307.2 1487.3
1471(35) 0.000816 1307.0 1463.1
1521(36) 0.000772 1307. 1441.
1458(35) 0.000816 1306.4 1421.4
1416(34) 0.000865 1306.2 1405.1
1406(34) 0.000865 1305.9 1392.1
1380(34) 0.000865 1305.7 1382.4
1295(33) 0.000918 1305.4 1376.0
1327(33) 0.000918 1305.2 1372.5
1365(34) 0.000865 1304.9 1371.6
1371(34) 0.000865 1304.6 1373.0
1319(33) 0.000918 1304.4 1376.2
1354(34) 0.000865 1304.1 1380.8
1357(34) 0.000865 1303.8 1386.2
1373(34) 0.000865 1303.6 1391.9
1415(34) 0.000865 1303.3 1397.4
1379(34) 0.000865 1303.1 1402.6
1346(34) 0.000865 1302.8 1407.3
1399(34) 0.000865 1302.5 1411.6
1392(34) 0.000865 1302.3 1415.8
1391(34) 0.000865 1302.0 1419.8
1365(34) 0.000865 1301.7 1423.6
1421(35) 0.000816 1301.5 1427.1
1383(34) 0.000865 1301.2 1430.7
1414(34) 0.000865 1300.9 1435.0
1459(35) 0.000816 1300.6 1440.6
1502(35) 0.000816 1300.4 1448.1
1480(35) 0.000816 1300.1 1458.1
1499(35) 0.000816 1299.8 1470.6
1514(36) 0.000772 1300. 1486.
1514(36) 0.000772 1299. 1503.
1556(36) 0.000772 1299. 1522.
1569(36) 0.000772 1299. 1543.
1583(36) 0.000772 1298. 1564.
1546(36) 0.000772 1298. 1584.
1608(37) 0.000730 1298. 1601.
1594(37) 0.000730 1298. 1614.
1641(37) 0.000730 1297. 1622.
1577(36) 0.000772 1297. 1626.
1626(37) 0.000730 1297. 1627.
1578(36) 0.000772 1297. 1626.
1521(36) 0.000772 1296. 1622.
1627(37) 0.000730 1296. 1617.
1531(36) 0.000772 1296. 1610.
1514(36) 0.000772 1295. 1600.
1527(36) 0.000772 1295. 1590.
1581(36) 0.000772 1295. 1579.
1528(36) 0.000772 1295. 1568.
1505(36) 0.000772 1294. 1557.
1500(35) 0.000816 1294.0 1546.7
1456(35) 0.000816 1293.7 1535.4
1568(36) 0.000772 1293. 1523.
1519(36) 0.000772 1293. 1511.
1519(36) 0.000772 1293. 1498.
1538(36) 0.000772 1293. 1485.
1510(36) 0.000772 1292. 1472.
1445(35) 0.000816 1292.0 1459.0
1425(35) 0.000816 1291.7 1444.9
1444(35) 0.000816 1291.5 1430.2
1425(35) 0.000816 1291.2 1415.2
1351(34) 0.000865 1290.9 1400.5
1344(34) 0.000865 1290.6 1386.6
1370(34) 0.000865 1290.3 1374.1
1334(33) 0.000918 1290.0 1363.4
1332(33) 0.000918 1289.7 1354.7
1371(34) 0.000865 1289.4 1348.1
1324(33) 0.000918 1289.2 1343.8
1342(34) 0.000865 1288.9 1341.8
1348(34) 0.000865 1288.6 1342.2
1267(33) 0.000918 1288.3 1345.0
1264(33) 0.000918 1288.0 1350.3
1257(33) 0.000918 1287.7 1358.0
1296(33) 0.000918 1287.4 1368.2
1378(34) 0.000865 1287.1 1380.8
1359(34) 0.000865 1286.8 1395.7
1409(35) 0.000816 1286.5 1412.9
1425(35) 0.000816 1286.2 1431.8
1469(35) 0.000816 1285.9 1452.1
1451(35) 0.000816 1285.6 1472.9
1470(35) 0.000816 1285.4 1493.8
1518(36) 0.000772 1285. 1514.
1534(36) 0.000772 1285. 1533.
1589(37) 0.000730 1284. 1550.
1535(36) 0.000772 1284. 1563.
1626(37) 0.000730 1284. 1570.
1559(36) 0.000772 1284. 1572.
1574(37) 0.000730 1283. 1567.
1558(36) 0.000772 1283. 1557.
1576(37) 0.000730 1283. 1543.
1505(36) 0.000772 1282. 1526.
1517(36) 0.000772 1282. 1507.
1452(35) 0.000816 1281.8 1487.4
1435(35) 0.000816 1281.5 1467.8
1382(34) 0.000865 1281.2 1448.7
1456(35) 0.000816 1280.9 1430.9
1405(35) 0.000816 1280.6 1415.3
1358(34) 0.000865 1280.3 1402.4
1386(34) 0.000865 1280.0 1392.6
1413(35) 0.000816 1279.7 1386.0
1337(34) 0.000865 1279.4 1382.7
1401(34) 0.000865 1279.1 1382.4
1442(35) 0.000816 1278.8 1384.6
1377(34) 0.000865 1278.5 1388.8
1387(34) 0.000865 1278.2 1394.3
1471(35) 0.000816 1277.9 1400.2
1448(35) 0.000816 1277.6 1405.8
1462(35) 0.000816 1277.3 1410.5
1429(35) 0.000816 1277.0 1413.8
1497(36) 0.000772 1277. 1416.
1493(36) 0.000772 1276. 1416.
1415(35) 0.000816 1276.1 1416.1
1424(35) 0.000816 1275.8 1414.7
1469(35) 0.000816 1275.5 1412.4
1375(34) 0.000865 1275.2 1409.5
1423(35) 0.000816 1274.9 1406.6
1414(35) 0.000816 1274.6 1404.4
1346(34) 0.000865 1274.3 1403.8
1369(34) 0.000865 1273.9 1405.7
1345(34) 0.000865 1273.6 1411.1
1352(34) 0.000865 1273.3 1420.4
1390(34) 0.000865 1273.0 1434.3
1429(35) 0.000816 1272.7 1452.8
1344(34) 0.000865 1272.4 1476.0
1360(34) 0.000865 1272.1 1503.4
1469(35) 0.000816 1271.8 1534.4
1474(35) 0.000816 1271.5 1567.9
1476(35) 0.000816 1271.2 1602.7
1550(36) 0.000772 1271. 1638.
1594(37) 0.000730 1271. 1672.
1615(37) 0.000730 1270. 1704.
1685(38) 0.000693 1270. 1734.
1745(38) 0.000693 1270. 1760.
1696(38) 0.000693 1269. 1781.
1747(39) 0.000657 1269. 1795.
1825(39) 0.000657 1269. 1800.
1844(40) 0.000625 1268. 1798.
1792(39) 0.000657 1268. 1787.
1764(39) 0.000657 1268. 1771.
1768(39) 0.000657 1268. 1750.
1758(39) 0.000657 1267. 1725.
1704(38) 0.000693 1267. 1698.
1660(38) 0.000693 1267. 1668.
1641(37) 0.000730 1266. 1638.
1664(38) 0.000693 1266. 1608.
1626(37) 0.000730 1266. 1579.
1600(37) 0.000730 1265. 1554.
1529(36) 0.000772 1265. 1532.
1559(36) 0.000772 1265. 1514.
1525(36) 0.000772 1264. 1501.
1524(36) 0.000772 1264. 1492.
1489(36) 0.000772 1264. 1486.
1425(35) 0.000816 1263.6 1483.8
1526(36) 0.000772 1263. 1484.
1456(35) 0.000816 1262.9 1485.0
1471(35) 0.000816 1262.6 1486.3
1501(36) 0.000772 1262. 1487.
1491(36) 0.000772 1262. 1486.
1435(35) 0.000816 1261.7 1483.4
1461(35) 0.000816 1261.4 1479.5
1482(35) 0.000816 1261.1 1474.3
1459(35) 0.000816 1260.8 1468.1
1471(35) 0.000816 1260.5 1460.7
1451(35) 0.000816 1260.2 1452.2
1378(34) 0.000865 1259.9 1442.8
1381(34) 0.000865 1259.6 1432.6
1432(35) 0.000816 1259.3 1422.2
1452(35) 0.000816 1259.0 1411.7
1419(35) 0.000816 1258.7 1401.4
1366(34) 0.000865 1258.4 1391.4
1389(34) 0.000865 1258.1 1381.7
1395(34) 0.000865 1257.8 1372.6
1397(34) 0.000865 1257.5 1364.1
1359(32) 0.000977 1257.2 1356.6
1329(32) 0.000977 1256.9 1350.5
1378(33) 0.000918 1256.6 1345.9
1355(32) 0.000977 1256.3 1343.1
1338(32) 0.000977 1256.0 1342.1
1325(32) 0.000977 1255.7 1342.9
1353(32) 0.000977 1255.4 1345.4
1376(33) 0.000918 1255.0 1349.4
1342(32) 0.000977 1254.7 1354.6
1419(33) 0.000918 1254.4 1360.7
1485(34) 0.000865 1254.1 1367.5
1473(34) 0.000865 1253.8 1374.5
1396(33) 0.000918 1253.5 1381.8
1464(34) 0.000865 1253.2 1389.3
1396(33) 0.000918 1252.9 1397.4
1539(35) 0.000816 1252.6 1406.1
1518(34) 0.000865 1252.3 1415.6
1518(34) 0.000865 1252.0 1426.0
1496(34) 0.000865 1251.8 1437.3
1528(34) 0.000865 1251.5 1449.1
1473(34) 0.000865 1251.2 1461.5
1534(35) 0.000816 1250.9 1474.1
1538(35) 0.000816 1250.6 1486.7
1563(35) 0.000816 1250.3 1498.7
1496(34) 0.000865 1250.0 1509.5
1521(34) 0.000865 1249.7 1518.5
1524(34) 0.000865 1249.4 1525.1
1531(34) 0.000865 1249.1 1529.5
1564(35) 0.000816 1248.8 1531.9
1489(34) 0.000865 1248.5 1532.8
1552(35) 0.000816 1248.2 1532.5
1502(34) 0.000865 1247.9 1531.3
1481(34) 0.000865 1247.6 1529.3
1499(34) 0.000865 1247.3 1526.5
1506(34) 0.000865 1247.0 1523.2
1486(34) 0.000865 1246.7 1519.6
1484(34) 0.000865 1246.4 1516.2
1491(34) 0.000865 1246.2 1513.0
1478(34) 0.000865 1245.9 1510.0
1471(34) 0.000865 1245.6 1507.1
1478(34) 0.000865 1245.3 1504.1
1483(34) 0.000865 1245.0 1501.0
1500(34) 0.000865 1244.7 1497.9
1481(34) 0.000865 1244.4 1494.9
1466(34) 0.000865 1244.1 1492.1
1489(34) 0.000865 1243.8 1489.5
1447(33) 0.000918 1243.6 1486.8
1513(34) 0.000865 1243.3 1483.8
1535(35) 0.000816 1243.0 1480.4
1522(34) 0.000865 1242.7 1476.7
1486(34) 0.000865 1242.4 1472.8
1462(34) 0.000865 1242.1 1468.7
1444(33) 0.000918 1241.9 1464.6
1437(33) 0.000918 1241.6 1460.6
1439(33) 0.000918 1241.3 1456.7
1388(33) 0.000918 1241.0 1453.6
1451(34) 0.000865 1240.7 1451.7
1457(34) 0.000865 1240.4 1452.2
1502(34) 0.000865 1240.2 1455.6
1413(33) 0.000918 1239.9 1462.7
1486(34) 0.000865 1239.6 1474.0
1478(34) 0.000865 1239.3 1489.7
1491(34) 0.000865 1239.1 1509.5
1524(34) 0.000865 1238.8 1532.8
1567(35) 0.000816 1238.5 1558.8
1525(34) 0.000865 1238.2 1586.0
1571(35) 0.000816 1237.9 1612.9
1567(35) 0.000816 1237.7 1637.6
1602(35) 0.000816 1237.4 1658.7
1603(35) 0.000816 1237.1 1675.0
1625(36) 0.000772 1237. 1686.
1608(35) 0.000816 1236.6 1691.9
1634(36) 0.000772 1236. 1693.
1683(36) 0.000772 1236. 1689.
1633(36) 0.000772 1236. 1681.
1586(35) 0.000816 1235.5 1668.6
1587(35) 0.000816 1235.2 1652.2
1599(35) 0.000816 1235.0 1632.7
1592(35) 0.000816 1234.7 1611.1
1535(35) 0.000816 1234.4 1588.4
1564(35) 0.000816 1234.2 1565.9
1560(35) 0.000816 1233.9 1544.0
1432(33) 0.000918 1233.6 1523.5
1476(34) 0.000865 1233.4 1504.6
1490(34) 0.000865 1233.1 1487.6
1442(33) 0.000918 1232.9 1472.6
1467(34) 0.000865 1232.6 1459.9
1483(34) 0.000865 1232.3 1449.1
1416(33) 0.000918 1232.1 1440.2
1417(33) 0.000918 1231.8 1432.8
1490(34) 0.000865 1231.6 1426.5
1448(34) 0.000865 1231.3 1420.9
1447(33) 0.000918 1231.1 1415.7
1401(33) 0.000918 1230.8 1410.6
1451(34) 0.000865 1230.6 1405.5
1452(34) 0.000865 1230.3 1399.9
1421(33) 0.000918 1230.1 1393.7
1447(34) 0.000865 1229.8 1386.6
1424(33) 0.000918 1229.5 1378.5
1397(45) 0.000494 1229. 1370.
1371(32) 0.000977 1229.1 1360.3
1381(32) 0.000977 1228.8 1350.8
1359(32) 0.000977 1228.6 1341.6
1342(32) 0.000977 1228.3 1332.8
1346(32) 0.000977 1228.1 1324.8
1324(32) 0.000977 1227.8 1317.6
1319(32) 0.000977 1227.6 1311.4
1303(31) 0.001041 1227.3 1306.0
1320(32) 0.000977 1227.1 1301.7
1304(31) 0.001041 1226.9 1298.1
1331(32) 0.000977 1226.6 1295.4
1314(32) 0.000977 1226.4 1293.4
1288(31) 0.001041 1226.1 1292.0
1273(31) 0.001041 1225.9 1291.3
1298(31) 0.001041 1225.7 1291.2
1270(31) 0.001041 1225.4 1292.0
1289(31) 0.001041 1225.2 1293.8
1308(32) 0.000977 1225.0 1296.7
1274(31) 0.001041 1224.7 1300.8
1266(31) 0.001041 1224.5 1306.2
1310(32) 0.000977 1224.3 1313.1
1349(32) 0.000977 1224.1 1321.3
1320(32) 0.000977 1223.8 1330.8
1308(32) 0.000977 1223.6 1341.5
1396(33) 0.000918 1223.4 1353.2
1386(33) 0.000918 1223.2 1365.6
1385(32) 0.000977 1222.9 1378.5
1358(32) 0.000977 1222.7 1391.8
1390(33) 0.000918 1222.5 1405.3
1415(33) 0.000918 1222.3 1418.8
1394(33) 0.000918 1222.1 1432.3
1455(33) 0.000918 1221.8 1445.5
1458(33) 0.000918 1221.6 1458.3
1425(33) 0.000918 1221.4 1470.6
1470(33) 0.000918 1221.2 1482.3
1460(33) 0.000918 1221.0 1493.7
1481(34) 0.000865 1220.8 1504.9
1510(34) 0.000865 1220.6 1516.2
1573(35) 0.000816 1220.3 1527.7
1548(34) 0.000865 1220.1 1539.5
1569(35) 0.000816 1219.9 1551.3
1601(35) 0.000816 1219.7 1562.7
1596(35) 0.000816 1219.5 1573.4
1630(35) 0.000816 1219.3 1582.8
1678(36) 0.000772 1219. 1591.
1637(35) 0.000816 1218.9 1595.7
1659(36) 0.000772 1219. 1598.
1664(36) 0.000772 1219. 1596.
1650(36) 0.000772 1218. 1589.
1644(35) 0.000816 1218.1 1578.6
1615(35) 0.000816 1217.9 1564.1
1616(35) 0.000816 1217.7 1546.9
1576(35) 0.000816 1217.5 1528.0
1622(35) 0.000816 1217.3 1508.8
1612(35) 0.000816 1217.1 1490.4
1561(35) 0.000816 1216.9 1473.3
1508(34) 0.000865 1216.8 1458.3
1503(34) 0.000865 1216.6 1445.5
1516(34) 0.000865 1216.4 1434.8
1466(33) 0.000918 1216.2 1426.0
1441(33) 0.000918 1216.0 1418.4
1375(32) 0.000977 1215.8 1411.4
1371(32) 0.000977 1215.7 1404.4
1381(32) 0.000977 1215.5 1396.9
1373(32) 0.000977 1215.3 1388.4
1392(33) 0.000918 1215.1 1379.0
1422(33) 0.000918 1214.9 1368.7
1359(32) 0.000977 1214.8 1357.8
1376(32) 0.000977 1214.6 1346.7
1319(32) 0.000977 1214.4 1335.7
1248(31) 0.001041 1214.2 1325.1
1286(31) 0.001041 1214.1 1315.1
1322(32) 0.000977 1213.9 1306.1
1292(31) 0.001041 1213.7 1298.2
1275(31) 0.001041 1213.6 1291.8
1272(31) 0.001041 1213.4 1287.0
1307(32) 0.000977 1213.2 1284.0
1271(31) 0.001041 1213.1 1282.8
1275(31) 0.001041 1212.9 1283.5
1280(31) 0.001041 1212.8 1286.2
1326(32) 0.000977 1212.6 1290.9
1265(31) 0.001041 1212.4 1297.7
1296(31) 0.001041 1212.3 1306.4
1332(32) 0.000977 1212.1 1317.0
1309(32) 0.000977 1212.0 1329.4
1304(31) 0.001041 1211.8 1343.4
1352(32) 0.000977 1211.7 1358.6
1373(32) 0.000977 1211.5 1374.8
1372(32) 0.000977 1211.4 1391.5
1391(33) 0.000918 1211.2 1408.2
1382(32) 0.000977 1211.1 1424.4
1383(32) 0.000977 1210.9 1439.5
1427(33) 0.000918 1210.8 1453.0
1453(33) 0.000918 1210.7 1464.6
1468(33) 0.000918 1210.5 1474.1
1478(34) 0.000865 1210.4 1481.6
1506(34) 0.000865 1210.2 1487.1
1478(34) 0.000865 1210.1 1490.9
1446(33) 0.000918 1210.0 1493.0
1439(33) 0.000918 1209.8 1493.5
1441(33) 0.000918 1209.7 1492.6
1443(33) 0.000918 1209.6 1490.3
1397(32) 0.000977 1209.4 1487.2
1393(32) 0.000977 1209.3 1483.4
1411(33) 0.000918 1209.2 1479.3
1451(33) 0.000918 1209.1 1475.1
1445(33) 0.000918 1208.9 1471.0
1398(32) 0.000977 1208.8 1467.0
1419(33) 0.000918 1208.7 1463.3
1468(33) 0.000918 1208.6 1460.0
1404(33) 0.000918 1208.5 1457.1
1415(33) 0.000918 1208.4 1454.8
1447(33) 0.000918 1208.2 1453.0
1453(33) 0.000918 1208.1 1451.5
1384(32) 0.000977 1208.0 1450.3
1378(32) 0.000977 1207.9 1449.1
1410(33) 0.000918 1207.8 1447.7
1399(32) 0.000977 1207.7 1445.9
1389(32) 0.000977 1207.6 1443.5
1428(33) 0.000918 1207.5 1440.3
1404(33) 0.000918 1207.4 1436.0
1410(33) 0.000918 1207.3 1430.4
1377(32) 0.000977 1207.2 1423.2
1363(32) 0.000977 1207.1 1414.4
1412(33) 0.000918 1207.0 1404.1
1430(33) 0.000918 1206.9 1392.7
1361(32) 0.000977 1206.8 1380.3
1336(32) 0.000977 1206.7 1367.4
1365(32) 0.000977 1206.6 1354.4
1374(32) 0.000977 1206.5 1341.6
1403(32) 0.000977 1206.4 1329.3
1318(31) 0.001041 1206.3 1317.7
1312(31) 0.001041 1206.2 1307.1
1294(31) 0.001041 1206.1 1297.7
1282(31) 0.001041 1206.1 1289.6
1279(31) 0.001041 1206.0 1283.0
1305(31) 0.001041 1205.9 1278.0
1294(31) 0.001041 1205.8 1274.6
1252(31) 0.001041 1205.7 1272.9
1279(31) 0.001041 1205.7 1272.9
1294(31) 0.001041 1205.6 1274.5
1278(31) 0.001041 1205.5 1277.7
1270(31) 0.001041 1205.4 1282.5
1287(31) 0.001041 1205.4 1288.7
1308(31) 0.001041 1205.3 1296.2
1351(32) 0.000977 1205.2 1304.7
1358(32) 0.000977 1205.2 1314.2
1324(32) 0.000977 1205.1 1324.2
1318(31) 0.001041 1205.0 1334.5
1347(32) 0.000977 1205.0 1344.7
1372(32) 0.000977 1204.9 1354.4
1352(32) 0.000977 1204.9 1363.1
1379(32) 0.000977 1204.8 1370.7
1393(32) 0.000977 1204.8 1376.8
1406(33) 0.000918 1204.7 1381.4
1389(32) 0.000977 1204.6 1384.5
1407(33) 0.000918 1204.6 1386.1
1411(33) 0.000918 1204.5 1386.4
1409(33) 0.000918 1204.5 1385.6
1406(33) 0.000918 1204.4 1383.8
1408(33) 0.000918 1204.4 1381.2
1430(33) 0.000918 1204.4 1377.9
1367(32) 0.000977 1204.3 1374.2
1442(33) 0.000918 1204.3 1370.3
1424(33) 0.000918 1204.2 1366.4
1384(32) 0.000977 1204.2 1362.8
1361(32) 0.000977 1204.2 1359.6
1347(32) 0.000977 1204.1 1356.8
1340(32) 0.000977 1204.1 1354.6
1350(32) 0.000977 1204.0 1353.0
1356(32) 0.000977 1204.0 1352.1
1339(32) 0.000977 1204.0 1351.7
1370(32) 0.000977 1204.0 1351.8
1334(32) 0.000977 1203.9 1352.4
1351(32) 0.000977 1203.9 1353.3
1354(32) 0.000977 1203.9 1354.2
1364(32) 0.000977 1203.9 1355.1
1336(32) 0.000977 1203.8 1355.9
1330(32) 0.000977 1203.8 1356.2
1363(32) 0.000977 1203.8 1356.1
1366(32) 0.000977 1203.8 1355.3
1368(32) 0.000977 1203.8 1353.7
1351(32) 0.000977 1203.7 1351.3
1258(31) 0.001041 1203.7 1347.8
1295(31) 0.001041 1203.7 1343.3
1302(31) 0.001041 1203.7 1337.8
1256(31) 0.001041 1203.7 1331.5
1269(31) 0.001041 1203.7 1324.7
1283(31) 0.001041 1203.7 1317.5
1285(31) 0.001041 1203.7 1310.2
1278(31) 0.001041 1203.7 1302.9
1280(31) 0.001041 1203.7 1296.0
1263(31) 0.001041 1203.7 1289.4
1266(31) 0.001041 1203.7 1283.4
1288(31) 0.001041 1203.7 1278.0
1291(31) 0.001041 1203.7 1273.5
1283(31) 0.001041 1203.7 1270.0
1287(31) 0.001041 1203.7 1267.5
1253(31) 0.001041 1203.7 1266.2
1235(30) 0.001111 1203.7 1266.1
1256(32) 0.000977 1203.7 1267.4
1216(31) 0.001041 1203.7 1270.2
1265(32) 0.000977 1203.7 1274.4
1291(32) 0.000977 1203.8 1280.2
1284(32) 0.000977 1203.8 1287.7
1295(32) 0.000977 1203.8 1296.9
1305(32) 0.000977 1203.8 1307.8
1351(33) 0.000918 1203.8 1320.6
1364(33) 0.000918 1203.9 1335.2
1346(33) 0.000918 1203.9 1351.4
1389(33) 0.000918 1203.9 1369.3
1485(34) 0.000865 1203.9 1388.7
1463(34) 0.000865 1203.9 1409.3
1458(34) 0.000865 1204.0 1430.8
1471(34) 0.000865 1204.0 1452.9
1460(34) 0.000865 1204.0 1475.3
1497(35) 0.000816 1204.1 1497.6
1507(35) 0.000816 1204.1 1519.4
1552(35) 0.000816 1204.1 1540.3
1557(35) 0.000816 1204.2 1559.8
1669(37) 0.000730 1204. 1577.
1585(36) 0.000772 1204. 1593.
1622(36) 0.000772 1204. 1605.
1599(36) 0.000772 1204. 1615.
1678(37) 0.000730 1204. 1622.
1658(36) 0.000772 1204. 1626.
1653(36) 0.000772 1204. 1628.
1660(36) 0.000772 1204. 1627.
1649(36) 0.000772 1205. 1625.
1619(36) 0.000772 1205. 1621.
1626(36) 0.000772 1205. 1615.
1662(36) 0.000772 1205. 1608.
1632(36) 0.000772 1205. 1600.
1607(36) 0.000772 1205. 1591.
1561(35) 0.000816 1204.8 1581.0
1612(36) 0.000772 1205. 1570.
1616(36) 0.000772 1205. 1559.
1637(36) 0.000772 1205. 1547.
1599(36) 0.000772 1205. 1535.
1570(35) 0.000816 1205.1 1522.4
1584(36) 0.000772 1205. 1510.
1572(35) 0.000816 1205.3 1496.8
1550(35) 0.000816 1205.3 1484.1
1510(35) 0.000816 1205.4 1471.8
1487(34) 0.000865 1205.5 1459.9
1433(34) 0.000865 1205.5 1448.5
1443(34) 0.000865 1205.6 1437.7
1470(34) 0.000865 1205.7 1427.5
1423(34) 0.000865 1205.7 1417.9
1412(34) 0.000865 1205.8 1408.9
1380(33) 0.000918 1205.9 1400.5
1332(33) 0.000918 1205.9 1392.7
1342(33) 0.000918 1206.0 1385.5
1355(33) 0.000918 1206.1 1378.8
1337(33) 0.000918 1206.2 1372.7
1333(33) 0.000918 1206.2 1367.4
1342(33) 0.000918 1206.3 1362.9
1381(33) 0.000918 1206.4 1359.4
1382(33) 0.000918 1206.5 1357.1
1404(33) 0.000918 1206.6 1356.3
1379(33) 0.000918 1206.7 1357.0
1393(33) 0.000918 1206.7 1359.4
1363(33) 0.000918 1206.8 1363.7
1322(32) 0.000977 1206.9 1369.7
1373(33) 0.000918 1207.0 1377.5
1382(33) 0.000918 1207.1 1387.0
1381(33) 0.000918 1207.2 1398.0
1386(33) 0.000918 1207.3 1410.2
1430(34) 0.000865 1207.4 1423.3
1421(34) 0.000865 1207.4 1437.0
1487(34) 0.000865 1207.5 1450.8
1433(34) 0.000865 1207.6 1464.4
1463(34) 0.000865 1207.7 1477.3
1450(34) 0.000865 1207.8 1488.9
1503(35) 0.000816 1207.9 1498.9
1515(35) 0.000816 1208.0 1506.6
1504(35) 0.000816 1208.1 1511.7
1509(35) 0.000816 1208.2 1513.9
1504(35) 0.000816 1208.3 1512.9
1525(35) 0.000816 1208.4 1508.9
1529(35) 0.000816 1208.5 1502.0
1493(35) 0.000816 1208.6 1492.6
1535(35) 0.000816 1208.7 1481.2
1477(34) 0.000865 1208.8 1468.1
1438(34) 0.000865 1208.9 1453.9
1457(34) 0.000865 1209.0 1438.9
1461(34) 0.000865 1209.1 1423.5
1441(34) 0.000865 1209.3 1408.1
1433(34) 0.000865 1209.4 1393.1
1369(33) 0.000918 1209.5 1378.6
1332(33) 0.000918 1209.6 1364.9
1372(33) 0.000918 1209.7 1352.3
1392(33) 0.000918 1209.8 1340.9
1375(33) 0.000918 1209.9 1330.7
1331(33) 0.000918 1210.0 1321.9
1292(32) 0.000977 1210.1 1314.4
1379(33) 0.000918 1210.3 1308.4
1350(33) 0.000918 1210.4 1303.6
1314(32) 0.000977 1210.5 1300.2
1316(26) 0.001479 1210.6 1298.1
1299(33) 0.000918 1210.7 1297.2
1275(33) 0.000918 1210.8 1297.4
1339(34) 0.000865 1211.0 1298.8
1358(34) 0.000865 1211.1 1301.0
1330(33) 0.000918 1211.2 1304.1
1324(33) 0.000918 1211.3 1307.9
1346(34) 0.000865 1211.4 1312.2
1420(35) 0.000816 1211.6 1316.9
1384(34) 0.000865 1211.7 1321.7
1380(34) 0.000865 1211.8 1326.6
1316(33) 0.000918 1211.9 1331.2
1387(34) 0.000865 1212.1 1335.5
1403(34) 0.000865 1212.2 1339.3
1373(34) 0.000865 1212.3 1342.6
1420(35) 0.000816 1212.4 1345.1
1427(35) 0.000816 1212.6 1346.9
1420(35) 0.000816 1212.7 1347.7
1390(34) 0.000865 1212.8 1347.6
1418(35) 0.000816 1213.0 1346.6
1453(35) 0.000816 1213.1 1344.7
1400(34) 0.000865 1213.2 1342.0
1367(34) 0.000865 1213.3 1338.7
1393(34) 0.000865 1213.5 1335.1
1416(35) 0.000816 1213.6 1331.2
1405(34) 0.000865 1213.7 1327.3
1354(34) 0.000865 1213.9 1323.7
1375(34) 0.000865 1214.0 1320.5
1342(34) 0.000865 1214.1 1317.9
1338(34) 0.000865 1214.3 1315.8
1358(34) 0.000865 1214.4 1314.5
1380(34) 0.000865 1214.5 1314.0
1283(33) 0.000918 1214.7 1314.2
1318(33) 0.000918 1214.8 1315.3
1248(32) 0.000977 1214.9 1317.0
1325(33) 0.000918 1215.1 1319.4
1286(33) 0.000918 1215.2 1322.5
1323(33) 0.000918 1215.3 1326.0
1301(33) 0.000918 1215.5 1329.9
1351(34) 0.000865 1215.6 1334.1
1344(34) 0.000865 1215.8 1338.5
1311(33) 0.000918 1215.9 1343.0
1279(33) 0.000918 1216.0 1347.5
1366(34) 0.000865 1216.2 1352.0
1352(34) 0.000865 1216.3 1356.3
1363(34) 0.000865 1216.4 1360.4
1325(33) 0.000918 1216.6 1364.3
1315(33) 0.000918 1216.7 1368.1
1380(34) 0.000865 1216.9 1371.8
1354(34) 0.000865 1217.0 1375.4
1422(35) 0.000816 1217.1 1378.9
1377(34) 0.000865 1217.3 1382.4
1380(34) 0.000865 1217.4 1385.9
1429(35) 0.000816 1217.5 1389.3
1342(34) 0.000865 1217.7 1392.8
1377(34) 0.000865 1217.8 1396.3
1413(35) 0.000816 1218.0 1399.7
1418(35) 0.000816 1218.1 1403.2
1432(35) 0.000816 1218.2 1406.6
1381(34) 0.000865 1218.4 1410.1
1498(36) 0.000772 1219. 1413.
1439(35) 0.000816 1218.7 1416.4
1431(35) 0.000816 1218.8 1419.3
1433(35) 0.000816 1218.9 1422.1
1458(35) 0.000816 1219.1 1424.7
1444(35) 0.000816 1219.2 1427.1
1480(35) 0.000816 1219.4 1429.4
1487(35) 0.000816 1219.5 1431.5
1454(35) 0.000816 1219.6 1433.4
1448(35) 0.000816 1219.8 1435.0
1472(35) 0.000816 1219.9 1436.3
1432(35) 0.000816 1220.1 1437.1
1456(35) 0.000816 1220.2 1437.6
1388(34) 0.000865 1220.3 1437.3
1391(34) 0.000865 1220.5 1436.5
1391(34) 0.000865 1220.6 1434.9
1384(34) 0.000865 1220.8 1432.4
1385(34) 0.000865 1220.9 1429.1
1393(34) 0.000865 1221.0 1424.8
1398(34) 0.000865 1221.2 1419.7
1373(34) 0.000865 1221.3 1413.7
1292(33) 0.000918 1221.5 1407.2
1359(34) 0.000865 1221.6 1400.1
1383(34) 0.000865 1221.7 1392.6
1384(34) 0.000865 1221.9 1384.9
1341(34) 0.000865 1222.0 1377.3
1306(33) 0.000918 1222.2 1369.6
1357(34) 0.000865 1222.3 1362.2
1286(33) 0.000918 1222.4 1355.2
1321(33) 0.000918 1222.6 1348.7
1288(33) 0.000918 1222.7 1342.7
1309(33) 0.000918 1222.8 1337.3
1276(33) 0.000918 1223.0 1332.6
1271(33) 0.000918 1223.1 1328.7
1290(33) 0.000918 1223.2 1325.5
1299(33) 0.000918 1223.4 1323.1
1255(33) 0.000918 1223.5 1321.5
1340(34) 0.000865 1223.6 1320.5
1305(33) 0.000918 1223.8 1320.2
1299(33) 0.000918 1223.9 1320.5
1318(33) 0.000918 1224.0 1321.2
1241(31) 0.001041 1224.2 1322.4
1312(32) 0.000977 1224.3 1323.9
1305(32) 0.000977 1224.4 1325.6
1306(32) 0.000977 1224.6 1327.5
1283(32) 0.000977 1224.7 1329.6
1379(33) 0.000918 1224.8 1331.9
1306(32) 0.000977 1225.0 1334.2
1367(33) 0.000918 1225.1 1336.6
1286(32) 0.000977 1225.2 1339.2
1336(33) 0.000918 1225.3 1341.8
1349(33) 0.000918 1225.5 1344.4
1357(33) 0.000918 1225.6 1347.1
1363(33) 0.000918 1225.7 1349.8
1398(33) 0.000918 1225.8 1352.6
1342(33) 0.000918 1226.0 1355.3
1394(33) 0.000918 1226.1 1358.1
1360(33) 0.000918 1226.2 1360.8
1431(34) 0.000865 1226.3 1363.4
1350(33) 0.000918 1226.5 1366.1
1413(34) 0.000865 1226.6 1368.7
1410(34) 0.000865 1226.7 1371.3
1398(33) 0.000918 1226.8 1374.0
1382(33) 0.000918 1226.9 1376.8
1438(34) 0.000865 1227.1 1380.0
1403(33) 0.000918 1227.2 1383.5
1376(33) 0.000918 1227.3 1387.5
1402(33) 0.000918 1227.4 1392.2
1395(33) 0.000918 1227.5 1397.5
1399(33) 0.000918 1227.7 1403.6
1443(34) 0.000865 1227.8 1410.4
1405(33) 0.000918 1227.9 1418.1
1386(33) 0.000918 1228.0 1426.4
1424(34) 0.000865 1228.1 1435.5
1463(34) 0.000865 1228.2 1445.2
1421(34) 0.000865 1228.3 1455.4
1464(34) 0.000865 1228.4 1466.0
1494(35) 0.000816 1228.5 1476.8
1472(34) 0.000865 1228.7 1487.7
1518(35) 0.000816 1228.8 1498.5
1528(35) 0.000816 1228.9 1509.2
1562(35) 0.000816 1229.0 1519.5
1566(35) 0.000816 1229.1 1529.4
1536(35) 0.000816 1229.2 1538.7
1538(35) 0.000816 1229.3 1547.3
1550(35) 0.000816 1229.4 1555.1
1572(35) 0.000816 1229.5 1561.8
1596(36) 0.000772 1230. 1567.
1594(36) 0.000772 1230. 1572.
1621(36) 0.000772 1230. 1575.
1593(36) 0.000772 1230. 1577.
1655(36) 0.000772 1230. 1577.
1576(35) 0.000816 1230.1 1576.2
1587(36) 0.000772 1230. 1574.
1600(36) 0.000772 1230. 1570.
1584(36) 0.000772 1230. 1565.
1597(36) 0.000772 1230. 1558.
1581(36) 0.000772 1231. 1550.
1540(35) 0.000816 1230.6 1541.2
1509(35) 0.000816 1230.7 1531.6
1460(34) 0.000865 1230.8 1521.3
1516(35) 0.000816 1230.9 1510.7
1551(35) 0.000816 1231.0 1500.0
1511(35) 0.000816 1231.1 1489.5
1489(34) 0.000865 1231.1 1479.4
1477(34) 0.000865 1231.2 1469.7
1420(34) 0.000865 1231.3 1460.7
1490(34) 0.000865 1231.4 1452.4
1425(34) 0.000865 1231.5 1444.9
1451(34) 0.000865 1231.5 1438.0
1441(34) 0.000865 1231.6 1431.9
1444(34) 0.000865 1231.7 1426.5
1384(33) 0.000918 1231.8 1421.7
1391(33) 0.000918 1231.8 1417.4
1381(33) 0.000918 1231.9 1413.6
1455(34) 0.000865 1232.0 1410.2
1407(34) 0.000865 1232.0 1407.2
1424(34) 0.000865 1232.1 1404.5
1396(33) 0.000918 1232.2 1402.1
1388(33) 0.000918 1232.2 1400.1
1396(33) 0.000918 1232.3 1398.3
1385(33) 0.000918 1232.4 1396.8
1364(33) 0.000918 1232.4 1395.6
1410(34) 0.000865 1232.5 1394.7
1380(33) 0.000918 1232.5 1394.1
1359(33) 0.000918 1232.6 1393.7
1366(33) 0.000918 1232.7 1393.6
1333(33) 0.000918 1232.7 1393.8
1381(33) 0.000918 1232.8 1394.3
1380(33) 0.000918 1232.8 1395.0
1382(33) 0.000918 1232.9 1396.0
1389(33) 0.000918 1232.9 1397.2
1374(33) 0.000918 1233.0 1398.7
1400(33) 0.000918 1233.0 1400.4
1361(33) 0.000918 1233.1 1402.4
1362(33) 0.000918 1233.1 1404.7
1432(34) 0.000865 1233.1 1407.2
1418(34) 0.000865 1233.2 1410.0
1444(34) 0.000865 1233.2 1413.0
1423(34) 0.000865 1233.3 1416.3
1481(49) 0.000416 1233. 1420.
1428(33) 0.000918 1233.3 1423.5
1396(33) 0.000918 1233.4 1427.2
1473(34) 0.000865 1233.4 1430.9
1396(33) 0.000918 1233.4 1434.4
1402(33) 0.000918 1233.5 1437.7
1416(33) 0.000918 1233.5 1440.6
1389(33) 0.000918 1233.5 1442.9
1349(32) 0.000977 1233.5 1444.6
1356(32) 0.000977 1233.6 1445.5
1445(33) 0.000918 1233.6 1445.5
1453(33) 0.000918 1233.6 1444.5
1387(33) 0.000918 1233.6 1442.5
1385(33) 0.000918 1233.7 1439.5
1396(33) 0.000918 1233.7 1435.7
1415(33) 0.000918 1233.7 1430.9
1390(33) 0.000918 1233.7 1425.5
1360(32) 0.000977 1233.7 1419.4
1337(32) 0.000977 1233.7 1412.7
1331(32) 0.000977 1233.7 1405.7
1378(32) 0.000977 1233.7 1398.4
1373(32) 0.000977 1233.8 1390.8
1378(32) 0.000977 1233.8 1383.2
1386(33) 0.000918 1233.8 1375.6
1337(32) 0.000977 1233.8 1368.1
1342(32) 0.000977 1233.8 1360.7
1363(32) 0.000977 1233.8 1353.6
1341(32) 0.000977 1233.8 1346.8
1298(31) 0.001041 1233.8 1340.3
1291(31) 0.001041 1233.8 1334.3
1316(32) 0.000977 1233.8 1328.7
1323(32) 0.000977 1233.7 1323.5
1313(32) 0.000977 1233.7 1318.8
1312(32) 0.000977 1233.7 1314.7
1305(32) 0.000977 1233.7 1311.1
1318(32) 0.000977 1233.7 1308.0
1265(31) 0.001041 1233.7 1305.5
1304(32) 0.000977 1233.7 1303.5
1295(31) 0.001041 1233.7 1302.0
1290(31) 0.001041 1233.6 1301.2
1314(32) 0.000977 1233.6 1300.8
1333(32) 0.000977 1233.6 1301.0
1317(32) 0.000977 1233.6 1301.7
1305(32) 0.000977 1233.5 1302.9
1315(32) 0.000977 1233.5 1304.5
1340(32) 0.000977 1233.5 1306.5
1303(32) 0.000977 1233.5 1309.0
1318(32) 0.000977 1233.4 1311.8
1307(32) 0.000977 1233.4 1314.9
1330(32) 0.000977 1233.4 1318.3
1334(32) 0.000977 1233.3 1321.9
1341(32) 0.000977 1233.3 1325.7
1334(32) 0.000977 1233.2 1329.6
1322(32) 0.000977 1233.2 1333.5
1343(32) 0.000977 1233.2 1337.4
1335(32) 0.000977 1233.1 1341.2
1377(32) 0.000977 1233.1 1344.9
1373(32) 0.000977 1233.0 1348.4
1360(32) 0.000977 1233.0 1351.7
1348(32) 0.000977 1232.9 1354.8
1353(32) 0.000977 1232.9 1357.6
1376(32) 0.000977 1232.8 1360.1
1405(33) 0.000918 1232.8 1362.4
1411(33) 0.000918 1232.7 1364.5
1384(33) 0.000918 1232.7 1366.3
1397(33) 0.000918 1232.6 1368.0
1432(33) 0.000918 1232.6 1369.4
1423(33) 0.000918 1232.5 1370.7
1375(32) 0.000977 1232.4 1371.8
1393(33) 0.000918 1232.4 1372.8
1399(33) 0.000918 1232.3 1373.5
1400(33) 0.000918 1232.2 1374.1
1397(33) 0.000918 1232.2 1374.4
1389(33) 0.000918 1232.1 1374.6
1370(32) 0.000977 1232.0 1374.4
1371(32) 0.000977 1232.0 1374.0
1374(32) 0.000977 1231.9 1373.3
1380(32) 0.000977 1231.8 1372.3
1331(32) 0.000977 1231.7 1371.0
1298(31) 0.001041 1231.7 1369.4
1343(32) 0.000977 1231.6 1367.6
1384(32) 0.000977 1231.5 1365.5
1442(33) 0.000918 1231.4 1363.4
1377(32) 0.000977 1231.3 1361.1
1402(33) 0.000918 1231.3 1358.9
1383(32) 0.000977 1231.2 1356.7
1345(32) 0.000977 1231.1 1354.6
1377(32) 0.000977 1231.0 1352.8
1364(32) 0.000977 1230.9 1351.1
1367(32) 0.000977 1230.8 1349.7
1371(32) 0.000977 1230.7 1348.6
1409(33) 0.000918 1230.6 1347.8
1349(32) 0.000977 1230.5 1347.4
1343(32) 0.000977 1230.4 1347.2
1333(32) 0.000977 1230.4 1347.3
1342(32) 0.000977 1230.3 1347.7
1360(32) 0.000977 1230.2 1348.3
1404(33) 0.000918 1230.1 1349.1
1345(32) 0.000977 1230.0 1350.0
1319(32) 0.000977 1229.9 1351.1
1343(26) 0.001479 1229.8 1352.2
1303(31) 0.001041 1229.6 1353.2
1361(32) 0.000977 1229.5 1354.2
1305(32) 0.000977 1229.4 1355.1
1375(32) 0.000977 1229.3 1355.8
1318(32) 0.000977 1229.2 1356.2
1350(32) 0.000977 1229.1 1356.3
1351(32) 0.000977 1229.0 1356.1
1352(32) 0.000977 1228.9 1355.6
1392(33) 0.000918 1228.8 1354.8
1370(32) 0.000977 1228.7 1353.6
1317(32) 0.000977 1228.5 1352.2
1324(32) 0.000977 1228.4 1350.5
1336(32) 0.000977 1228.3 1348.7
1336(32) 0.000977 1228.2 1346.7
1310(32) 0.000977 1228.1 1344.8
1295(31) 0.001041 1228.0 1342.9
1376(32) 0.000977 1227.8 1341.1
1337(32) 0.000977 1227.7 1339.5
1347(32) 0.000977 1227.6 1338.2
1358(32) 0.000977 1227.5 1337.2
1361(32) 0.000977 1227.4 1336.6
1312(32) 0.000977 1227.2 1336.5
1346(32) 0.000977 1227.1 1336.8
1346(32) 0.000977 1227.0 1337.7
1315(32) 0.000977 1226.8 1339.2
1306(32) 0.000977 1226.7 1341.3
1325(32) 0.000977 1226.6 1344.0
1308(32) 0.000977 1226.5 1347.3
1299(31) 0.001041 1226.3 1351.3
1327(32) 0.000977 1226.2 1356.0
1304(32) 0.000977 1226.1 1361.4
1354(32) 0.000977 1225.9 1367.4
1378(32) 0.000977 1225.8 1374.0
1356(32) 0.000977 1225.7 1381.3
1391(33) 0.000918 1225.5 1389.1
1369(32) 0.000977 1225.4 1397.5
1365(32) 0.000977 1225.3 1406.3
1432(33) 0.000918 1225.1 1415.5
1436(33) 0.000918 1225.0 1425.1
1426(33) 0.000918 1224.9 1434.9
1473(34) 0.000865 1224.7 1444.9
1470(33) 0.000918 1224.6 1455.0
1453(33) 0.000918 1224.5 1464.9
1459(33) 0.000918 1224.3 1474.8
1518(34) 0.000865 1224.2 1484.3
1497(34) 0.000865 1224.1 1493.4
1483(34) 0.000865 1223.9 1502.0
1456(33) 0.000918 1223.8 1510.0
1469(33) 0.000918 1223.6 1517.3
1491(34) 0.000865 1223.5 1523.7
1503(34) 0.000865 1223.4 1529.4
1533(34) 0.000865 1223.2 1534.1
1574(35) 0.000816 1223.1 1537.9
1548(34) 0.000865 1222.9 1540.8
1517(34) 0.000865 1222.8 1542.8
1513(34) 0.000865 1222.7 1543.8
1531(34) 0.000865 1222.5 1543.9
1579(35) 0.000816 1222.4 1543.1
1607(35) 0.000816 1222.2 1541.5
1513(34) 0.000865 1222.1 1539.1
1493(34) 0.000865 1222.0 1535.8
1527(34) 0.000865 1221.8 1531.9
1494(34) 0.000865 1221.7 1527.4
1505(34) 0.000865 1221.6 1522.3
1482(34) 0.000865 1221.4 1516.8
1536(34) 0.000865 1221.3 1510.8
1514(34) 0.000865 1221.1 1504.6
1501(34) 0.000865 1221.0 1498.2
1502(34) 0.000865 1220.9 1491.6
1495(34) 0.000865 1220.7 1484.9
1475(34) 0.000865 1220.6 1478.2
1486(34) 0.000865 1220.5 1471.6
1449(33) 0.000918 1220.3 1465.1
1475(34) 0.000865 1220.2 1458.7
1450(33) 0.000918 1220.0 1452.5
1423(33) 0.000918 1219.9 1446.6
1369(32) 0.000977 1219.8 1440.9
1394(33) 0.000918 1219.6 1435.5
1461(33) 0.000918 1219.5 1430.4
1439(33) 0.000918 1219.4 1425.6
1428(33) 0.000918 1219.3 1421.1
1429(33) 0.000918 1219.1 1417.0
1392(33) 0.000918 1219.0 1413.1
1422(33) 0.000918 1218.9 1409.6
1384(32) 0.000977 1218.7 1406.3
1374(32) 0.000977 1218.6 1403.3
1370(32) 0.000977 1218.5 1400.6
1375(32) 0.000977 1218.4 1398.2
1414(33) 0.000918 1218.2 1396.0
1383(32) 0.000977 1218.1 1394.0
1402(33) 0.000918 1218.0 1392.3
1442(33) 0.000918 1217.9 1390.8
1433(33) 0.000918 1217.8 1389.6
1433(33) 0.000918 1217.6 1388.7
1450(33) 0.000918 1217.5 1388.1
1380(32) 0.000977 1217.4 1387.7
1347(32) 0.000977 1217.3 1387.8
1339(32) 0.000977 1217.2 1388.3
1371(32) 0.000977 1217.1 1389.2
1371(32) 0.000977 1217.0 1390.5
1429(33) 0.000918 1216.8 1392.4
1380(33) 0.000918 1216.7 1394.9
1407(33) 0.000918 1216.6 1397.9
1404(33) 0.000918 1216.5 1401.5
1423(33) 0.000918 1216.4 1405.7
1448(34) 0.000865 1216.3 1410.5
1431(33) 0.000918 1216.2 1415.9
1440(34) 0.000865 1216.1 1421.9
1448(34) 0.000865 1216.0 1428.5
1447(34) 0.000865 1215.9 1435.5
1475(34) 0.000865 1215.9 1443.1
1462(34) 0.000865 1215.8 1451.0
1469(34) 0.000865 1215.7 1459.4
1498(34) 0.000865 1215.6 1468.0
1466(34) 0.000865 1215.5 1476.9
1484(34) 0.000865 1215.4 1485.9
1518(34) 0.000865 1215.3 1494.9
1482(34) 0.000865 1215.3 1503.9
1510(34) 0.000865 1215.2 1512.8
1532(35) 0.000816 1215.1 1521.3
1528(35) 0.000816 1215.0 1529.5
1522(34) 0.000865 1215.0 1537.3
1533(35) 0.000816 1214.9 1544.5
1565(35) 0.000816 1214.8 1551.0
1590(35) 0.000816 1214.8 1556.9
1610(35) 0.000816 1214.7 1561.9
1597(35) 0.000816 1214.7 1566.2
1584(35) 0.000816 1214.6 1569.7
1600(35) 0.000816 1214.6 1572.5
1585(35) 0.000816 1214.5 1574.4
1584(35) 0.000816 1214.5 1575.7
1586(35) 0.000816 1214.4 1576.4
1587(35) 0.000816 1214.4 1576.4
1599(35) 0.000816 1214.4 1575.9
1607(35) 0.000816 1214.3 1575.0
1552(35) 0.000816 1214.3 1573.7
1567(35) 0.000816 1214.3 1572.1
1609(35) 0.000816 1214.3 1570.1
1602(35) 0.000816 1214.2 1567.9
1549(35) 0.000816 1214.2 1565.4
1550(35) 0.000816 1214.2 1562.8
1563(35) 0.000816 1214.2 1559.9
1534(35) 0.000816 1214.2 1556.8
1526(35) 0.000816 1214.2 1553.5
1527(35) 0.000816 1214.2 1550.0
1564(35) 0.000816 1214.2 1546.3
1524(34) 0.000865 1214.2 1542.3
1555(35) 0.000816 1214.2 1538.1
1540(35) 0.000816 1214.2 1533.6
1494(34) 0.000865 1214.2 1528.8
1488(34) 0.000865 1214.3 1523.8
1504(34) 0.000865 1214.3 1518.5
1462(34) 0.000865 1214.3 1513.0
1508(34) 0.000865 1214.3 1507.2
1517(34) 0.000865 1214.4 1501.2
1488(34) 0.000865 1214.4 1495.1
1482(34) 0.000865 1214.5 1488.9
1461(34) 0.000865 1214.5 1482.5
1459(34) 0.000865 1214.6 1476.1
1414(33) 0.000918 1214.6 1469.6
1508(34) 0.000865 1214.7 1463.1
1450(34) 0.000865 1214.8 1456.5
1415(33) 0.000918 1214.8 1450.0
1440(34) 0.000865 1214.9 1443.6
1378(33) 0.000918 1215.0 1437.2
1422(33) 0.000918 1215.1 1430.9
1395(33) 0.000918 1215.2 1424.8
1444(34) 0.000865 1215.3 1418.7
1386(33) 0.000918 1215.4 1412.8
1384(33) 0.000918 1215.5 1407.1
1418(33) 0.000918 1215.6 1401.5
1437(33) 0.000918 1215.7 1396.1
1415(33) 0.000918 1215.8 1390.9
1394(33) 0.000918 1215.9 1385.9
1394(33) 0.000918 1216.1 1381.1
1376(33) 0.000918 1216.2 1376.5
1384(33) 0.000918 1216.3 1372.1
1362(33) 0.000918 1216.5 1368.0
1367(33) 0.000918 1216.6 1364.1
1343(32) 0.000977 1216.8 1360.5
1301(32) 0.000977 1217.0 1357.1
1293(32) 0.000977 1217.1 1354.0
1328(32) 0.000977 1217.3 1351.2
1320(32) 0.000977 1217.5 1348.7
1318(32) 0.000977 1217.7 1346.4
1347(32) 0.000977 1217.9 1344.5
1341(32) 0.000977 1218.1 1342.8
1355(32) 0.000977 1218.3 1341.5
1315(32) 0.000977 1218.5 1340.5
1320(32) 0.000977 1218.7 1339.9
1316(32) 0.000977 1218.9 1339.6
1383(33) 0.000918 1219.1 1339.7
1346(32) 0.000977 1219.4 1340.2
1379(33) 0.000918 1219.6 1341.1
1367(33) 0.000918 1219.9 1342.3
1379(33) 0.000918 1220.1 1344.0
1329(32) 0.000977 1220.4 1346.2
1361(33) 0.000918 1220.7 1348.7
1355(33) 0.000918 1220.9 1351.7
1384(33) 0.000918 1221.2 1355.1
1378(33) 0.000918 1221.5 1359.0
1351(33) 0.000918 1221.8 1363.3
1354(33) 0.000918 1222.1 1368.0
1358(33) 0.000918 1222.4 1373.1
1400(33) 0.000918 1222.7 1378.7
1425(33) 0.000918 1223.0 1384.6
1425(33) 0.000918 1223.4 1391.0
1404(33) 0.000918 1223.7 1397.7
1432(33) 0.000918 1224.0 1404.7
1428(33) 0.000918 1224.4 1412.0
1438(34) 0.000865 1224.8 1419.7
1405(33) 0.000918 1225.1 1427.6
1437(34) 0.000865 1225.5 1435.7
1467(34) 0.000865 1225.9 1444.0
1433(33) 0.000918 1226.3 1452.5
1422(33) 0.000918 1226.7 1461.1
1485(34) 0.000865 1227.1 1469.7
1524(35) 0.000816 1227.5 1478.4
1529(35) 0.000816 1227.9 1487.0
1503(34) 0.000865 1228.3 1495.6
1474(34) 0.000865 1228.8 1504.1
1517(34) 0.000865 1229.2 1512.4
1544(35) 0.000816 1229.7 1520.6
1565(35) 0.000816 1230.1 1528.5
1556(35) 0.000816 1230.6 1536.3
1572(35) 0.000816 1231.1 1543.7
1562(35) 0.000816 1231.6 1550.8
1567(35) 0.000816 1232.1 1557.7
1547(35) 0.000816 1232.6 1564.2
1579(35) 0.000816 1233.1 1570.3
1589(35) 0.000816 1233.6 1576.1
1606(35) 0.000816 1234.1 1581.5
1622(36) 0.000772 1235. 1587.
1635(36) 0.000772 1235. 1591.
1613(36) 0.000772 1236. 1595.
1571(35) 0.000816 1236.3 1599.2
1606(35) 0.000816 1236.9 1602.7
1622(36) 0.000772 1237. 1606.
1652(36) 0.000772 1238. 1609.
1640(36) 0.000772 1239. 1611.
1635(36) 0.000772 1239. 1613.
1646(36) 0.000772 1240. 1615.
1668(36) 0.000772 1241. 1616.
1678(36) 0.000772 1241. 1617.
1723(37) 0.000730 1242. 1618.
1635(36) 0.000772 1243. 1619.
1666(36) 0.000772 1243. 1620.
1642(36) 0.000772 1244. 1620.
1623(36) 0.000772 1245. 1620.
1595(35) 0.000816 1245.3 1619.9
1621(36) 0.000772 1246. 1620.
1669(36) 0.000772 1247. 1619.
1654(36) 0.000772 1247. 1618.
1675(36) 0.000772 1248. 1617.
1651(36) 0.000772 1249. 1616.
1608(35) 0.000816 1249.7 1614.6
1584(35) 0.000816 1250.5 1612.8
1639(36) 0.000772 1251. 1611.
1598(35) 0.000816 1252.0 1608.3
1607(35) 0.000816 1252.8 1605.6
1616(36) 0.000772 1254. 1603.
1590(35) 0.000816 1254.5 1599.2
1613(36) 0.000772 1255. 1595.
1635(36) 0.000772 1256. 1591.
1667(36) 0.000772 1257. 1587.
1639(36) 0.000772 1258. 1582.
1569(35) 0.000816 1258.8 1577.1
1568(35) 0.000816 1259.7 1571.7
1557(35) 0.000816 1260.6 1566.1
1544(35) 0.000816 1261.5 1560.3
1536(35) 0.000816 1262.4 1554.3
1544(35) 0.000816 1263.4 1548.2
1570(35) 0.000816 1264.3 1542.0
1577(35) 0.000816 1265.3 1535.7
1565(35) 0.000816 1266.2 1529.3
1526(35) 0.000816 1267.2 1523.0
1531(35) 0.000816 1268.2 1516.7
1575(35) 0.000816 1269.2 1510.4
1504(34) 0.000865 1270.2 1504.3
1531(35) 0.000816 1271.3 1498.2
1586(35) 0.000816 1272.3 1492.4
1547(35) 0.000816 1273.4 1486.6
1486(34) 0.000865 1274.4 1481.1
1491(34) 0.000865 1275.5 1475.7
1492(34) 0.000865 1276.6 1470.5
1455(34) 0.000865 1277.7 1465.6
1464(34) 0.000865 1278.8 1460.9
1460(34) 0.000865 1280.0 1456.4
1489(34) 0.000865 1281.1 1452.2
1433(33) 0.000918 1282.3 1448.2
1433(33) 0.000918 1283.4 1444.5
1429(33) 0.000918 1284.6 1441.0
1442(34) 0.000865 1285.8 1437.8
1464(34) 0.000865 1287.0 1434.9
1448(34) 0.000865 1288.2 1432.3
1449(34) 0.000865 1289.5 1430.0
1422(33) 0.000918 1290.7 1427.9
1447(34) 0.000865 1292.0 1426.2
1423(33) 0.000918 1293.2 1424.7
1416(27) 0.001372 1294.5 1423.6
1425(34) 0.000865 1295.8 1422.8
1421(34) 0.000865 1297.1 1422.4
1422(34) 0.000865 1298.5 1422.2
1416(34) 0.000865 1299.8 1422.4
1407(33) 0.000918 1301.1 1422.9
1424(34) 0.000865 1302.5 1423.8
1407(33) 0.000918 1303.9 1425.0
1392(33) 0.000918 1305.3 1426.5
1390(33) 0.000918 1306.7 1428.4
1402(33) 0.000918 1308.1 1430.6
1433(34) 0.000865 1309.5 1433.2
1423(34) 0.000865 1311.0 1436.1
1440(34) 0.000865 1312.4 1439.3
1475(34) 0.000865 1313.9 1442.9
1435(34) 0.000865 1315.4 1446.8
1447(34) 0.000865 1316.9 1451.0
1428(34) 0.000865 1318.4 1455.5
1453(34) 0.000865 1319.9 1460.3
1477(34) 0.000865 1321.5 1465.4
1487(34) 0.000865 1323.0 1470.8
1460(34) 0.000865 1324.6 1476.5
1459(34) 0.000865 1326.2 1482.4
1487(34) 0.000865 1327.8 1488.6
1503(35) 0.000816 1329.4 1495.0
1535(35) 0.000816 1331.0 1501.6
1528(35) 0.000816 1332.7 1508.4
1518(35) 0.000816 1334.3 1515.4
1519(35) 0.000816 1336.0 1522.6
1532(35) 0.000816 1337.7 1529.9
1502(35) 0.000816 1339.4 1537.3
1465(34) 0.000865 1341.1 1544.8
1513(35) 0.000816 1342.8 1552.4
1542(35) 0.000816 1344.6 1560.0
1528(35) 0.000816 1346.3 1567.6
1571(35) 0.000816 1348.1 1575.2
1578(35) 0.000816 1349.9 1582.7
1554(35) 0.000816 1351.7 1590.2
1538(35) 0.000816 1353.5 1597.5
1574(35) 0.000816 1355.3 1604.7
1566(35) 0.000816 1357.2 1611.7
1554(35) 0.000816 1359.0 1618.6
1527(35) 0.000816 1360.9 1625.1
1557(35) 0.000816 1362.8 1631.4
1520(35) 0.000816 1364.7 1637.4
1568(35) 0.000816 1366.6 1643.1
1635(36) 0.000772 1369. 1648.
1646(36) 0.000772 1370. 1653.
1619(36) 0.000772 1372. 1658.
1607(36) 0.000772 1374. 1662.
1643(36) 0.000772 1376. 1666.
1629(36) 0.000772 1378. 1669.
1646(36) 0.000772 1380. 1672.
1650(36) 0.000772 1383. 1674.
1643(36) 0.000772 1385. 1676.
1640(36) 0.000772 1387. 1677.
1637(36) 0.000772 1389. 1679.
1674(36) 0.000772 1391. 1679.
1667(36) 0.000772 1393. 1680.
1667(36) 0.000772 1395. 1680.
1674(36) 0.000772 1397. 1679.
1668(36) 0.000772 1399. 1679.
1669(36) 0.000772 1402. 1678.
1669(36) 0.000772 1404. 1677.
1692(37) 0.000730 1406. 1675.
1690(37) 0.000730 1408. 1674.
1646(36) 0.000772 1410. 1672.
1618(36) 0.000772 1413. 1671.
1616(36) 0.000772 1415. 1669.
1653(36) 0.000772 1417. 1667.
1692(37) 0.000730 1419. 1665.
1646(36) 0.000772 1422. 1664.
1659(36) 0.000772 1424. 1662.
1643(36) 0.000772 1426. 1660.
1634(36) 0.000772 1429. 1659.
1657(36) 0.000772 1431. 1657.
1666(36) 0.000772 1434. 1656.
1643(36) 0.000772 1436. 1654.
1630(36) 0.000772 1438. 1653.
1660(36) 0.000772 1441. 1652.
1681(36) 0.000772 1443. 1651.
1636(36) 0.000772 1446. 1650.
1615(36) 0.000772 1448. 1650.
1603(36) 0.000772 1451. 1649.
1651(36) 0.000772 1453. 1649.
1694(37) 0.000730 1456. 1649.
1638(36) 0.000772 1458. 1649.
1656(36) 0.000772 1461. 1649.
1683(37) 0.000730 1463. 1650.
1662(36) 0.000772 1466. 1650.
1648(36) 0.000772 1469. 1651.
1644(36) 0.000772 1471. 1652.
1676(36) 0.000772 1474. 1652.
1640(36) 0.000772 1476. 1653.
1614(36) 0.000772 1479. 1654.
1637(36) 0.000772 1482. 1655.
1619(36) 0.000772 1484. 1657.
1637(36) 0.000772 1487. 1658.
1676(36) 0.000772 1490. 1659.
1660(36) 0.000772 1493. 1660.
1652(37) 0.000730 1495. 1662.
1693(37) 0.000730 1498. 1663.
1677(37) 0.000730 1501. 1664.
1678(37) 0.000730 1504. 1666.
1645(37) 0.000730 1506. 1667.
1670(37) 0.000730 1509. 1668.
1693(37) 0.000730 1512. 1670.
1682(37) 0.000730 1515. 1671.
1669(37) 0.000730 1518. 1672.
1664(37) 0.000730 1521. 1674.
1693(37) 0.000730 1523. 1675.
1688(37) 0.000730 1526. 1676.
1675(37) 0.000730 1529. 1677.
1709(37) 0.000730 1532. 1679.
1686(37) 0.000730 1535. 1680.
1700(37) 0.000730 1538. 1681.
1681(37) 0.000730 1541. 1683.
1705(37) 0.000730 1544. 1684.
1677(37) 0.000730 1547. 1685.
1737(38) 0.000693 1550. 1687.
1782(38) 0.000693 1553. 1688.
1728(38) 0.000693 1556. 1690.
1698(37) 0.000730 1559. 1692.
1692(37) 0.000730 1562. 1693.
1703(37) 0.000730 1565. 1695.
1713(37) 0.000730 1568. 1697.
1729(38) 0.000693 1571. 1699.
1713(37) 0.000730 1574. 1701.
1684(37) 0.000730 1578. 1703.
1699(37) 0.000730 1581. 1706.
1721(38) 0.000693 1584. 1708.
1693(37) 0.000730 1587. 1710.
1709(37) 0.000730 1590. 1713.
1746(38) 0.000693 1593. 1716.
1720(38) 0.000693 1596. 1719.
1728(38) 0.000693 1600. 1722.
1750(38) 0.000693 1603. 1725.
1750(38) 0.000693 1606. 1728.
1709(37) 0.000730 1609. 1732.
1787(38) 0.000693 1613. 1735.
1788(38) 0.000693 1616. 1739.
1737(38) 0.000693 1619. 1743.
1738(38) 0.000693 1622. 1747.
1752(38) 0.000693 1626. 1751.
1763(38) 0.000693 1629. 1756.
1738(38) 0.000693 1632. 1760.
1801(38) 0.000693 1635. 1765.
1794(38) 0.000693 1639. 1769.
1748(38) 0.000693 1642. 1774.
1723(38) 0.000693 1645. 1779.
1729(38) 0.000693 1649. 1784.
1812(38) 0.000693 1652. 1789.
1775(38) 0.000693 1655. 1795.
1789(38) 0.000693 1659. 1800.
1816(39) 0.000657 1662. 1806.
1828(39) 0.000657 1666. 1811.
1824(39) 0.000657 1669. 1817.
1892(39) 0.000657 1672. 1823.
1836(39) 0.000657 1676. 1829.
1862(39) 0.000657 1679. 1834.
1833(39) 0.000657 1683. 1840.
1809(38) 0.000693 1686. 1846.
1824(39) 0.000657 1689. 1852.
1847(39) 0.000657 1693. 1858.
1848(39) 0.000657 1696. 1865.
1910(39) 0.000657 1700. 1871.
1871(39) 0.000657 1703. 1877.
1888(39) 0.000657 1707. 1883.
1847(39) 0.000657 1710. 1889.
1917(40) 0.000625 1714. 1895.
1929(40) 0.000625 1717. 1901.
1876(39) 0.000657 1721. 1907.
1939(40) 0.000625 1724. 1913.
1883(39) 0.000657 1728. 1919.
1880(39) . . .
1968(40) . . .
1947(40) . . .
1903(39) . . .
1934(40) . . .
1935(40) . . .
2038(41) . . .
2029(41) . . .
2037(41) . . .
2043(41) . . .
2042(41) . . .
2014(40) . . .
2048(41) . . .
2058(41) . . .
2040(41) . . .
2067(41) . . .
2083(41) . . .
2164(42) . . .
2148(42) . . .
2109(41) . . .
2088(41) . . .
2126(42) . . .
2181(42) . . .
2174(42) . . .
2168(42) . . .
2156(42) . . .
2138(60) . . .
2115(60) . . .
2164(60) . . .
2214(61) . . .
2130(60) . . .
2128(60) . . .
2193(61) . . .
2223(61) . . .
2223(61) . . .
2180(60) . . .
2204(61) . . .
2235(61) . . .
2274(62) . . .
2332(62) . . .
2385(63) . . .
2292(62) . . .
2419(63) . . .
2400(63) . . .
2300(62) . . .
2383(63) . . .
2444(64) . . .
2389(63) . . .
2432(64) . . .
2379(63) . . .
2449(64) . . .
2440(64) . . .
2413(63) . . .
2460(64) . . .
2409(63) . . .
2401(63) . . .
2479(64) . . .
2449(64) . . .
2476(64) . . .
2487(64) . . .
2449(64) . . .
2580(65) . . .
2454(64) . . .
2476(64) . . .
2507(64) . . .
2499(64) . . .
2572(65) . . .
2559(65) . . .
2556(65) . . .
2471(64) . . .
2528(65) . . .
2699(67) . . .
2636(66) . . .
2652(66) . . .
2610(66) . . .
2644(66) . . .
2569(65) . . .
2568(65) . . .
2637(66) . . .
2624(66) . . .
2676(66) . . .
2707(67) . . .
2696(67) . . .
2757(67) . . .
2652(66) . . .
2654(66) . . .
2639(66) . . .
2747(67) . . .
2739(67) . . .
2823(68) . . .
2697(67) . . .
2766(68) . . .
2771(68) . . .
2730(67) . . .
2669(66) . . .
2703(67) . . .
2774(68) . . .
2667(66) . . .
2667(66) . . .
2734(67) . . .
2844(68) . . .
2779(68) . . .
2700(67) . . .
2767(68) . . .
2709(67) . . .
2717(67) . . .
2731(67) . . .
2757(67) . . .
2749(67) . . .
2757(67) . . .
2760(67) . . .
2791(68) . . .
2808(68) . . .
2810(68) . . .
2839(68) . . .
2736(67) . . .
2764(68) . . .
2755(67) . . .
2798(68) . . .
2800(68) . . .
2829(68) . . .
2848(68) . . .
2751(67) . . .
2901(69) . . .
2827(68) . . .
2801(68) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_cell_measurement_reflns_used    660
_reflns_number_total             660
_reflns_limit_h_min              1
_reflns_limit_h_max              18
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.056
_reflns_d_resolution_low         18.895
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1P5CO2_FINAL_publ
_database_code_depnum_ccdc_archive 'CCDC 1582007'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-02-24T11:36|1P5CO2_FINAL|bt1|blah

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-02-24T11:36

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.05
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     51
_refine_ls_goodness_of_fit_all   1.05
_refine_ls_number_restraints     20
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10


_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   'Cu MOF'
_cell_length_a                   18.5323(4)
_cell_length_b                   18.5323
_cell_length_c                   18.5323
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6364.8(4)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cu Cu1 0.1330(5) 0.5 0.0 1.0 Uiso 0.0162(27) 12
C C1 0.14780(26) 0.33629(34) -0.14780(26) 1.0 Uiso 0.0085(8) 24
C C2 0.17930(26) 0.27168(35) -0.17930(26) 1.0 Uiso 0.0085(8) 24
C C3 0.24046(26) 0.24046(26) -0.1474(4) 1.0 Uiso 0.0085(8) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.061(6) 3
N N1 0.12987(19) 0.42584(20) -0.07784(20) 1.0 Uiso 0.0103(5) 48
N N2 0.17437(20) 0.36991(19) -0.08899(18) 1.0 Uiso 0.0103(5) 48
H H1 0.2636(5) 0.2636(5) -0.1014(7) 1.0 Uiso 0.0155(34) 24
Cu Cu2 0.2160(14) 0.3282(16) 0.0 0.19199 Uiso 0.06409 24
C C1a 0.2915(7) 0.43892(35) 0.0 0.434(5) Uiso 0.03625 24
O O1a 0.2753(8) 0.5 0.0 0.868(10) Uiso 0.10109 12
O O1b 0.3091(11) 0.3787(7) 0.0 0.434(5) Uiso 0.07825 24
C C4a 0.095(4) 0.0664(34) 0.0664(34) 0.0581(34) Uiso 0.04533 24
O O4a 0.080(5) 0.0234(29) 0.0234(29) 0.0581(34) Uiso 0.04533 24
O O4b 0.1096(26) 0.1096(26) 0.1096(26) 0.174(10) Uiso 0.04533 8
C C2a 0.0 0.2722(11) 0.0358(12) 0.180(4) Uiso 0.03761 24
O O2b 0.0 0.2212(12) 0.0721(16) 0.180(4) Uiso 0.06551 24
O O2a 0.0 0.3235(12) 0.0 0.721(15) Uiso 0.05482 6
C C3a 0.1597(8) 0.1597(8) 0.0 0.330(10) Uiso 0.06602 12
O O3a 0.0990(8) 0.173(4) 0.0 0.165(5) Uiso 0.04786 24
O O3b 0.2199(8) 0.146(4) 0.0 0.165(5) Uiso 0.04786 24
O Os 0.2505(8) 0.5 0.0 0.17378 Uiso 0.01168 12
Cl Cl2 0.3491(15) 0.3491(15) 0.0 0.19199 Uiso 0.06535 12

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C30.70 H8 Cl1.77 Cu5.54 N32 O14.09'
_chemical_formula_weight         1464.80
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cu1 Cu1 4.930(19) . 10_555 N
Cu1 Cu1 3.486(14) . 14_555 N
Cu1 Cu1 3.486(14) . 19_555 N
Cu1 C1 4.097(6) . 1_555 N
Cu1 C1 4.097(6) . 4_555 N
Cu1 C1 4.097(6) . 12_565 N
Cu1 C1 4.097(6) . -10_565 N
Cu1 Cl1 2.465(10) . 1_555 N
Cu1 N1 1.9933(32) . 1_555 N
Cu1 N1 1.9933(32) . 4_555 N
Cu1 N1 1.9933(32) . 12_565 N
Cu1 N1 2.954(5) . 17_555 N
Cu1 N1 2.954(5) . 19_555 N
Cu1 N1 2.954(5) . 23_565 N
Cu1 N1 1.9933(32) . -10_565 N
Cu1 N1 2.954(5) . -14_565 N
Cu1 N2 3.020(4) . 1_555 N
Cu1 N2 3.020(4) . 4_555 N
Cu1 N2 3.020(4) . 12_565 N
Cu1 N2 3.020(4) . -10_565 N
Cu1 Cu2 3.536(22) . 1_555 N
Cu1 Cu2 3.536(22) . 12_565 N
Cu1 C1a 3.148(13) . 1_555 N
Cu1 C1a 3.148(13) . 12_565 N
Cu1 O1a 2.638(16) . 1_555 N
Cu1 O1b 3.963(18) . 1_555 N
Cu1 O1b 3.963(18) . 12_565 N
Cu1 O2a 4.096(19) . 1_555 N
Cu1 O2a 4.096(19) . 12_565 N
Cu1 Os 2.177(10) . 1_555 N
Cu1 Cl2 4.884(11) . 1_555 N
Cu1 Cl2 4.884(11) . 12_565 N
C1 Cu1 4.097(6) . 1_555 N
C1 Cu1 4.097(6) . 19_555 N
C1 C2 1.454(9) . 1_555 N
C1 C3 2.470(5) . 1_555 N
C1 C3 2.470(5) . 7_555 N
C1 N1 2.132(7) . 1_555 N
C1 N1 2.132(7) . 19_555 N
C1 N2 1.349(5) . 1_555 N
C1 N2 1.349(5) . 19_555 N
C1 Cu2 3.020(11) . 1_555 N
C1 Cu2 3.020(11) . 19_555 N
C2 C1 1.454(9) . 1_555 N
C2 C2 2.421(12) . 7_555 N
C2 C2 2.421(12) . 9_555 N
C2 C3 1.403(5) . 1_555 N
C2 C3 1.403(5) . 7_555 N
C2 C3 2.806(9) . 9_555 N
C2 N2 2.475(7) . 1_555 N
C2 N2 2.475(7) . 19_555 N
C2 Cu2 3.550(13) . 1_555 N
C2 Cu2 3.550(13) . 19_555 N
C3 C1 2.470(5) . 1_555 N
C3 C1 2.470(5) . 9_555 N
C3 C2 1.403(5) . 1_555 N
C3 C2 2.806(9) . 7_555 N
C3 C2 1.403(5) . 9_555 N
C3 C3 2.440(12) . 7_555 N
C3 C3 2.440(12) . 9_555 N
C3 N2 2.903(5) . 1_555 N
C3 N2 2.903(5) . 13_555 N
C3 H1 1.047(17) . 1_555 N
C3 Cu2 3.211(14) . 1_555 N
C3 Cu2 3.211(14) . 13_555 N
C3 Cl2 3.946(28) . 1_555 N
Cl1 Cu1 2.465(10) . 1_555 N
Cl1 Cu1 2.465(10) . 10_555 N
Cl1 Cu1 2.465(10) . 14_555 N
Cl1 Cu1 2.465(10) . 19_555 N
Cl1 N1 3.1245(34) . 1_555 N
Cl1 N1 3.1245(34) . 4_555 N
Cl1 N1 3.1245(34) . 10_555 N
Cl1 N1 3.1245(34) . 12_565 N
Cl1 N1 3.1245(34) . 14_555 N
Cl1 N1 3.1245(34) . 17_555 N
Cl1 N1 3.1245(34) . 19_555 N
Cl1 N1 3.1245(34) . 23_565 N
Cl1 N1 3.1245(34) . -1_565 N
Cl1 N1 3.1245(34) . -4_565 N
Cl1 N1 3.1245(34) . -10_565 N
Cl1 N1 3.1245(34) . -12_555 N
Cl1 N1 3.1245(34) . -14_565 N
Cl1 N1 3.1245(34) . -17_565 N
Cl1 N1 3.1245(34) . -19_565 N
Cl1 N1 3.1245(34) . -23_555 N
Cl1 N2 4.356(4) . 1_555 N
Cl1 N2 4.356(4) . 4_555 N
Cl1 N2 4.356(4) . 10_555 N
Cl1 N2 4.356(4) . 12_565 N
Cl1 N2 4.356(4) . 14_555 N
Cl1 N2 4.356(4) . 17_555 N
Cl1 N2 4.356(4) . 19_555 N
Cl1 N2 4.356(4) . 23_565 N
Cl1 N2 4.356(4) . -1_565 N
Cl1 N2 4.356(4) . -4_565 N
Cl1 N2 4.356(4) . -10_565 N
Cl1 N2 4.356(4) . -12_555 N
Cl1 N2 4.356(4) . -14_565 N
Cl1 N2 4.356(4) . -17_565 N
Cl1 N2 4.356(4) . -19_565 N
Cl1 N2 4.356(4) . -23_555 N
Cl1 Cu2 5.115(18) . 1_555 N
Cl1 Cu2 5.115(18) . 10_555 N
Cl1 Cu2 5.115(18) . 12_565 N
Cl1 Cu2 5.115(18) . 14_555 N
Cl1 Cu2 5.115(18) . 19_555 N
Cl1 Cu2 5.115(18) . 23_565 N
Cl1 Cu2 5.115(18) . -1_565 N
Cl1 Cu2 5.115(18) . -14_565 N
Cl1 C2a 4.274(20) . 1_555 N
Cl1 C2a 4.274(20) . 4_555 N
Cl1 C2a 4.274(20) . 12_565 N
Cl1 C2a 4.274(20) . 14_555 N
Cl1 C2a 4.274(20) . 17_555 N
Cl1 C2a 4.274(20) . 23_565 N
Cl1 C2a 4.274(20) . -4_565 N
Cl1 C2a 4.274(20) . -17_565 N
Cl1 O2a 3.271(23) . 1_555 N
Cl1 O2a 3.271(23) . 12_565 N
N1 Cu1 1.9933(32) . 1_555 N
N1 Cu1 2.954(5) . 19_555 N
N1 C1 2.132(7) . 1_555 N
N1 Cl1 3.1245(34) . 1_555 N
N1 N1 2.885(7) . 4_555 N
N1 N1 1.364(8) . 19_555 N
N1 N1 2.749(7) . -10_565 N
N1 N1 3.068(8) . -14_565 N
N1 N2 1.341(5) . 1_555 N
N1 N2 2.202(4) . 19_555 N
N1 Cu2 2.811(16) . 1_555 N
N1 Cu2 3.953(15) . 19_555 N
N1 Os 2.994(11) . 1_555 N
N1 Cl2 4.540(16) . 1_555 N
N2 Cu1 3.020(4) . 1_555 N
N2 C1 1.349(5) . 1_555 N
N2 C2 2.475(7) . 1_555 N
N2 C3 2.903(5) . 1_555 N
N2 Cl1 4.356(4) . 1_555 N
N2 N1 1.341(5) . 1_555 N
N2 N1 2.202(4) . 19_555 N
N2 N2 2.238(6) . 19_555 N
N2 Cu2 1.978(10) . 1_555 N
N2 Cu2 4.072(14) . 19_555 N
N2 C1a 3.011(10) . 1_555 N
N2 O1b 2.997(18) . 1_555 N
N2 Cl2 3.654(21) . 1_555 N
H1 C3 1.047(17) . 1_555 N
H1 Cu2 2.396(16) . 1_555 N
H1 Cu2 2.396(16) . 13_555 N
H1 Cl2 2.924(32) . 1_555 N
Cu2 Cu1 3.536(22) . 1_555 N
Cu2 C1 3.020(11) . 1_555 N
Cu2 C1 3.020(11) . 4_555 N
Cu2 C2 3.550(13) . 1_555 N
Cu2 C2 3.550(13) . 4_555 N
Cu2 C3 3.211(14) . 1_555 N
Cu2 C3 3.211(14) . 4_555 N
Cu2 Cl1 5.115(18) . 1_555 N
Cu2 N1 2.811(16) . 1_555 N
Cu2 N1 2.811(16) . 4_555 N
Cu2 N1 3.953(15) . 17_555 N
Cu2 N1 3.953(15) . 19_555 N
Cu2 N2 1.978(10) . 1_555 N
Cu2 N2 1.978(10) . 4_555 N
Cu2 N2 4.072(14) . 17_555 N
Cu2 N2 4.072(14) . 19_555 N
Cu2 H1 2.396(16) . 1_555 N
Cu2 H1 2.396(16) . 4_555 N
Cu2 Cu2 2.94(4) . 13_555 N
Cu2 C1a 2.48(4) . 1_555 N
Cu2 O1a 3.369(34) . 1_555 N
Cu2 O1b 1.96(4) . 1_555 N
Cu2 O1b 3.036(28) . 13_555 N
Cu2 C2a 3.50(4) . 14_555 N
Cu2 O2b 3.32(5) . 14_555 N
Cu2 O2a 4.004(27) . 1_555 N
Cu2 C3a 3.29(4) . 1_555 N
Cu2 O3a 3.60(7) . 1_555 N
Cu2 O3b 3.37(7) . 1_555 N
Cu2 O3b 2.39(5) . 13_555 N
Cu2 Os 3.247(32) . 1_555 N
Cu2 Cl2 2.497(20) . 1_555 N
C1a Cu1 3.148(13) . 1_555 N
C1a N2 3.011(10) . 1_555 N
C1a N2 3.011(10) . 4_555 N
C1a Cu2 2.48(4) . 1_555 N
C1a C1a 2.264(13) . 12_565 N
C1a O1a 1.171(5) . 1_555 N
C1a O1b 1.162(10) . 1_555 N
C1a O1b 2.898(20) . 13_555 N
C1a Os 1.364(10) . 1_555 N
C1a Cl2 1.977(11) . 1_555 N
C1a Cl2 4.071(19) . 12_565 N
O1a Cu1 2.638(16) . 1_555 N
O1a Cu2 3.369(34) . 1_555 N
O1a Cu2 3.369(34) . 12_565 N
O1a C1a 1.171(5) . 1_555 N
O1a C1a 1.171(5) . 12_565 N
O1a O1b 2.333(11) . 1_555 N
O1a O1b 2.333(11) . 12_565 N
O1a Os 0.461(19) . 1_555 N
O1a Cl2 3.113(14) . 1_555 N
O1a Cl2 3.113(14) . 12_565 N
O1b Cu1 3.963(18) . 1_555 N
O1b N2 2.997(18) . 1_555 N
O1b N2 2.997(18) . 4_555 N
O1b Cu2 1.96(4) . 1_555 N
O1b Cu2 3.036(28) . 13_555 N
O1b C1a 1.162(10) . 1_555 N
O1b C1a 2.898(20) . 13_555 N
O1b O1a 2.333(11) . 1_555 N
O1b O1b 1.824(28) . 13_555 N
O1b Os 2.497(13) . 1_555 N
O1b Cl2 0.922(17) . 1_555 N
C4a C4a 0.75(16) . 2_555 N
C4a C4a 0.75(16) . 3_555 N
C4a C4a 2.46(12) . 4_555 N
C4a C4a 3.04(6) . 5_555 N
C4a C4a 2.57(8) . 6_555 N
C4a C4a 2.57(8) . 16_555 N
C4a C4a 3.04(6) . 17_555 N
C4a C4a 2.46(12) . 18_555 N
C4a C4a 3.04(6) . -7_555 N
C4a C4a 3.04(6) . -8_555 N
C4a O4a 1.161(9) . 1_555 N
C4a O4a 1.57(11) . 2_555 N
C4a O4a 1.57(11) . 3_555 N
C4a O4a 1.87(10) . 4_555 N
C4a O4a 2.35(6) . 5_555 N
C4a O4a 2.14(5) . 6_555 N
C4a O4a 2.76(8) . 7_555 N
C4a O4a 2.76(8) . 8_555 N
C4a O4a 2.37(16) . 12_555 N
C4a O4a 2.14(5) . 16_555 N
C4a O4a 2.35(6) . 17_555 N
C4a O4a 1.87(10) . 18_555 N
C4a O4a 3.12(11) . -7_555 N
C4a O4a 3.12(11) . -8_555 N
C4a O4b 1.165(10) . 1_555 N
C4a O2b 3.15(4) . 2_555 N
C4a O2b 2.65(8) . 3_555 N
C4a O2b 2.65(8) . 13_555 N
C4a O2b 3.15(4) . 14_555 N
C4a C3a 2.438(32) . 1_555 N
C4a C3a 3.01(10) . 2_555 N
C4a C3a 2.438(32) . 3_555 N
C4a O3a 2.33(6) . 1_555 N
C4a O3a 2.71(11) . 2_555 N
C4a O3a 1.99(8) . 3_555 N
C4a O3a 1.99(8) . 13_555 N
C4a O3a 2.71(11) . 14_555 N
C4a O3a 2.33(6) . 15_555 N
C4a O3b 3.01(6) . 1_555 N
C4a O3b 3.01(6) . 15_555 N
O4a C4a 1.161(9) . 1_555 N
O4a C4a 1.57(11) . 2_555 N
O4a C4a 1.57(11) . 3_555 N
O4a C4a 1.87(10) . 4_555 N
O4a C4a 3.12(11) . 5_555 N
O4a C4a 2.14(5) . 6_555 N
O4a C4a 2.76(8) . 9_555 N
O4a C4a 2.37(16) . 12_555 N
O4a C4a 2.14(5) . 16_555 N
O4a C4a 3.12(11) . 17_555 N
O4a C4a 1.87(10) . 18_555 N
O4a C4a 2.76(8) . 24_555 N
O4a C4a 2.35(6) . -7_555 N
O4a C4a 2.35(6) . -8_555 N
O4a O4a 1.48(16) . 2_555 N
O4a O4a 1.48(16) . 3_555 N
O4a O4a 0.87(11) . 4_555 N
O4a O4a 2.18(13) . 5_555 N
O4a O4a 1.72(12) . 6_555 N
O4a O4a 2.35(13) . 7_555 N
O4a O4a 2.35(13) . 8_555 N
O4a O4a 2.35(13) . 9_555 N
O4a O4a 3.09(19) . 10_555 N
O4a O4a 2.71(15) . 11_555 N
O4a O4a 1.23(15) . 12_555 N
O4a O4a 1.72(12) . 16_555 N
O4a O4a 2.18(13) . 17_555 N
O4a O4a 0.87(11) . 18_555 N
O4a O4a 2.71(15) . 19_555 N
O4a O4a 3.09(19) . 20_555 N
O4a O4a 2.35(13) . 24_555 N
O4a O4a 2.84(17) . -2_555 N
O4a O4a 2.84(17) . -3_555 N
O4a O4a 2.18(13) . -7_555 N
O4a O4a 2.18(13) . -8_555 N
O4a O4a 2.96(19) . -12_555 N
O4a O4b 2.326(14) . 1_555 N
O4a O4b 2.99(9) . 4_555 N
O4a O4b 2.99(9) . 6_555 N
O4a O2b 2.80(9) . 3_555 N
O4a O2b 3.19(9) . 6_555 N
O4a O2b 2.80(9) . 13_555 N
O4a O2b 3.19(9) . 16_555 N
O4a C3a 2.96(6) . 1_555 N
O4a C3a 2.96(6) . 3_555 N
O4a O3a 2.82(8) . 1_555 N
O4a O3a 2.26(10) . 3_555 N
O4a O3a 2.88(9) . 9_555 N
O4a O3a 2.26(10) . 13_555 N
O4a O3a 2.82(8) . 15_555 N
O4a O3a 2.88(9) . 24_555 N
O4b C4a 1.165(10) . 1_555 N
O4b C4a 1.165(10) . 2_555 N
O4b C4a 1.165(10) . 3_555 N
O4b O4a 2.326(14) . 1_555 N
O4b O4a 2.326(14) . 2_555 N
O4b O4a 2.326(14) . 3_555 N
O4b O4a 2.99(9) . 4_555 N
O4b O4a 2.99(9) . 5_555 N
O4b O4a 2.99(9) . 6_555 N
O4b O4a 2.99(9) . 16_555 N
O4b O4a 2.99(9) . 17_555 N
O4b O4a 2.99(9) . 18_555 N
O4b O2b 2.981(18) . 1_555 N
O4b O2b 2.981(18) . 2_555 N
O4b O2b 2.981(18) . 3_555 N
O4b O2b 2.981(18) . 13_555 N
O4b O2b 2.981(18) . 14_555 N
O4b O2b 2.981(18) . 15_555 N
O4b C3a 2.418(12) . 1_555 N
O4b C3a 2.418(12) . 2_555 N
O4b C3a 2.418(12) . 3_555 N
O4b O3a 2.35(4) . 1_555 N
O4b O3a 2.35(4) . 2_555 N
O4b O3a 2.35(4) . 3_555 N
O4b O3a 2.35(4) . 13_555 N
O4b O3a 2.35(4) . 14_555 N
O4b O3a 2.35(4) . 15_555 N
O4b O3b 2.961(24) . 1_555 N
O4b O3b 2.961(24) . 2_555 N
O4b O3b 2.961(24) . 3_555 N
O4b O3b 2.961(24) . 13_555 N
O4b O3b 2.961(24) . 14_555 N
O4b O3b 2.961(24) . 15_555 N
C2a Cl1 4.274(20) . 1_555 N
C2a Cu2 3.50(4) . 14_555 N
C2a C2a 1.33(5) . 4_555 N
C2a C2a 0.938(32) . 14_555 N
C2a C2a 0.938(32) . 17_555 N
C2a O2b 1.159(5) . 1_555 N
C2a O2b 2.21(4) . 4_555 N
C2a O2b 1.766(27) . 14_555 N
C2a O2b 1.766(27) . 17_555 N
C2a O2a 1.1599(10) . 1_555 N
C2a C3a 3.101(19) . 2_555 N
C2a O3a 2.68(4) . 1_555 N
C2a O3a 2.68(4) . 10_555 N
C2a O3a 2.18(6) . 14_555 N
C2a O3a 3.10(4) . 19_555 N
C2a O3b 2.27(6) . 2_555 N
C2a O3b 2.96(6) . 13_555 N
C2a O3b 2.96(6) . 22_555 N
O2b Cu2 3.32(5) . 14_555 N
O2b C4a 2.65(8) . 2_555 N
O2b C4a 3.15(4) . 3_555 N
O2b C4a 2.65(8) . 5_555 N
O2b C4a 3.15(4) . 17_555 N
O2b O4a 2.80(9) . 2_555 N
O2b O4a 2.80(9) . 5_555 N
O2b O4a 3.19(9) . 7_555 N
O2b O4a 3.19(9) . 16_555 N
O2b O4b 2.981(18) . 1_555 N
O2b O4b 2.981(18) . 5_555 N
O2b C2a 1.159(5) . 1_555 N
O2b C2a 2.21(4) . 4_555 N
O2b C2a 1.766(27) . 14_555 N
O2b C2a 1.766(27) . 17_555 N
O2b O2b 2.67(6) . 4_555 N
O2b O2b 1.89(4) . 14_555 N
O2b O2b 1.89(4) . 17_555 N
O2b O2a 2.319(5) . 1_555 N
O2b C3a 1.983(22) . 2_555 N
O2b O3a 2.440(30) . 1_555 N
O2b O3a 2.93(5) . 2_555 N
O2b O3a 2.440(30) . 10_555 N
O2b O3a 1.03(6) . 14_555 N
O2b O3b 1.38(7) . 2_555 N
O2b O3b 3.03(6) . 13_555 N
O2b O3b 3.07(4) . 14_555 N
O2b O3b 3.03(6) . 22_555 N
O2a Cu1 4.096(19) . 1_555 N
O2a Cu1 4.096(19) . 10_555 N
O2a Cu1 4.096(19) . 14_555 N
O2a Cu1 4.096(19) . 19_555 N
O2a Cl1 3.271(23) . 1_555 N
O2a Cu2 4.004(27) . 1_555 N
O2a Cu2 4.004(27) . 10_555 N
O2a Cu2 4.004(27) . 14_555 N
O2a Cu2 4.004(27) . 19_555 N
O2a C2a 1.1599(10) . 1_555 N
O2a C2a 1.1599(10) . 4_555 N
O2a C2a 1.1599(10) . 14_555 N
O2a C2a 1.1599(10) . 17_555 N
O2a O2b 2.319(5) . 1_555 N
O2a O2b 2.319(5) . 4_555 N
O2a O2b 2.319(5) . 14_555 N
O2a O2b 2.319(5) . 17_555 N
C3a Cu2 3.29(4) . 1_555 N
C3a Cu2 3.29(4) . 13_555 N
C3a C4a 2.438(32) . 1_555 N
C3a C4a 2.438(32) . 2_555 N
C3a C4a 3.01(10) . 3_555 N
C3a C4a 2.438(32) . 4_555 N
C3a C4a 2.438(32) . 16_555 N
C3a C4a 3.01(10) . -8_555 N
C3a O4a 2.96(6) . 1_555 N
C3a O4a 2.96(6) . 2_555 N
C3a O4a 2.96(6) . 4_555 N
C3a O4a 2.96(6) . 16_555 N
C3a O4b 2.418(12) . 1_555 N
C3a O4b 2.418(12) . 4_555 N
C3a C2a 3.101(19) . 3_555 N
C3a C2a 3.101(19) . 14_555 N
C3a O2b 1.983(22) . 3_555 N
C3a O2b 1.983(22) . 14_555 N
C3a O3a 1.151(10) . 1_555 N
C3a O3a 1.151(10) . 13_555 N
C3a O3b 1.142(10) . 1_555 N
C3a O3b 1.142(10) . 13_555 N
O3a Cu2 3.60(7) . 1_555 N
O3a C4a 2.33(6) . 1_555 N
O3a C4a 1.99(8) . 2_555 N
O3a C4a 2.71(11) . 3_555 N
O3a C4a 2.33(6) . 4_555 N
O3a C4a 1.99(8) . 16_555 N
O3a C4a 2.71(11) . -8_555 N
O3a O4a 2.82(8) . 1_555 N
O3a O4a 2.26(10) . 2_555 N
O3a O4a 2.82(8) . 4_555 N
O3a O4a 2.88(9) . 5_555 N
O3a O4a 2.88(9) . 7_555 N
O3a O4a 2.26(10) . 16_555 N
O3a O4b 2.35(4) . 1_555 N
O3a O4b 2.35(4) . 4_555 N
O3a C2a 2.68(4) . 1_555 N
O3a C2a 2.68(4) . 4_555 N
O3a C2a 2.18(6) . 14_555 N
O3a C2a 3.10(4) . 17_555 N
O3a O2b 2.440(30) . 1_555 N
O3a O2b 2.93(5) . 3_555 N
O3a O2b 2.440(30) . 4_555 N
O3a O2b 1.03(6) . 14_555 N
O3a C3a 1.151(10) . 1_555 N
O3a O3a 1.93(9) . 13_555 N
O3a O3a 2.594(22) . 14_555 N
O3a O3a 2.594(22) . 19_555 N
O3a O3b 2.293(15) . 1_555 N
O3a O3b 1.24(7) . 13_555 N
O3b Cu2 3.37(7) . 1_555 N
O3b Cu2 2.39(5) . 13_555 N
O3b C4a 3.01(6) . 1_555 N
O3b C4a 3.01(6) . 4_555 N
O3b O4b 2.961(24) . 1_555 N
O3b O4b 2.961(24) . 4_555 N
O3b C2a 2.27(6) . 3_555 N
O3b C2a 2.96(6) . 13_555 N
O3b C2a 2.96(6) . 16_555 N
O3b O2b 1.38(7) . 3_555 N
O3b O2b 3.03(6) . 13_555 N
O3b O2b 3.07(4) . 14_555 N
O3b O2b 3.03(6) . 16_555 N
O3b C3a 1.142(10) . 1_555 N
O3b O3a 2.293(15) . 1_555 N
O3b O3a 1.24(7) . 13_555 N
O3b O3b 1.92(9) . 13_555 N
O3b Cl2 4.45(7) . 1_555 N
Os Cu1 2.177(10) . 1_555 N
Os N1 2.994(11) . 1_555 N
Os N1 2.994(11) . 4_555 N
Os N1 2.994(11) . 12_565 N
Os N1 2.994(11) . -10_565 N
Os Cu2 3.247(32) . 1_555 N
Os Cu2 3.247(32) . 12_565 N
Os C1a 1.364(10) . 1_555 N
Os C1a 1.364(10) . 12_565 N
Os O1a 0.461(19) . 1_555 N
Os O1b 2.497(13) . 1_555 N
Os O1b 2.497(13) . 12_565 N
Os Cl2 3.341(11) . 1_555 N
Os Cl2 3.341(11) . 12_565 N
Cl2 Cu1 4.884(11) . 1_555 N
Cl2 Cu1 4.884(11) . 13_555 N
Cl2 C3 3.946(28) . 1_555 N
Cl2 C3 3.946(28) . 4_555 N
Cl2 N1 4.540(16) . 1_555 N
Cl2 N1 4.540(16) . 4_555 N
Cl2 N1 4.540(16) . 13_555 N
Cl2 N1 4.540(16) . 16_555 N
Cl2 N2 3.654(21) . 1_555 N
Cl2 N2 3.654(21) . 4_555 N
Cl2 N2 3.654(21) . 13_555 N
Cl2 N2 3.654(21) . 16_555 N
Cl2 H1 2.924(32) . 1_555 N
Cl2 H1 2.924(32) . 4_555 N
Cl2 Cu2 2.497(20) . 1_555 N
Cl2 Cu2 2.497(20) . 13_555 N
Cl2 C1a 1.977(11) . 1_555 N
Cl2 C1a 4.071(19) . 12_565 N
Cl2 C1a 1.977(11) . 13_555 N
Cl2 C1a 4.071(19) . 22_655 N
Cl2 O1a 3.113(14) . 1_555 N
Cl2 O1a 3.113(14) . 13_555 N
Cl2 O1b 0.922(17) . 1_555 N
Cl2 O1b 0.922(17) . 13_555 N
Cl2 O3b 4.45(7) . 1_555 N
Cl2 O3b 4.45(7) . 13_555 N
Cl2 Os 3.341(11) . 1_555 N
Cl2 Os 3.341(11) . 13_555 N
Cl2 Cl2 5.59(5) . 10_655 N
Cl2 Cl2 5.59(5) . 12_565 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Cu1 N1 88.32(31) 1_555 . 1_555 N
Cl1 Cu1 N1 88.32(31) 1_555 . 4_555 N
Cl1 Cu1 N1 88.32(31) 1_555 . 12_565 N
Cl1 Cu1 N1 88.32(31) 1_555 . -10_565 N
N1 Cu1 N1 92.73(23) 1_555 . 4_555 N
N1 Cu1 N1 176.6(6) 1_555 . 12_565 N
N1 Cu1 N1 87.18(23) 1_555 . -10_565 N
N1 Cu1 N1 87.18(23) 4_555 . 12_565 N
N1 Cu1 N1 176.6(6) 4_555 . -10_565 N
N1 Cu1 N1 92.73(23) 12_565 . -10_565 N
C2 C1 N2 123.93(29) 1_555 . 1_555 N
C2 C1 N2 123.93(29) 1_555 . 19_555 N
N2 C1 N2 112.1(6) 1_555 . 19_555 N
C1 C2 C3 119.6(4) 1_555 . 1_555 N
C1 C2 C3 119.6(4) 1_555 . 7_555 N
C3 C2 C3 120.7(7) 1_555 . 7_555 N
C2 C3 C2 119.2(7) 1_555 . 9_555 N
C2 C3 H1 120.4(4) 1_555 . 1_555 N
C2 C3 H1 120.4(4) 9_555 . 1_555 N
Cu1 Cl1 Cu1 180.0 1_555 . 10_555 N
Cu1 Cl1 Cu1 90.0 1_555 . 14_555 N
Cu1 Cl1 Cu1 90.0 1_555 . 19_555 N
Cu1 Cl1 Cu1 90.0 10_555 . 14_555 N
Cu1 Cl1 Cu1 90.0 10_555 . 19_555 N
Cu1 Cl1 Cu1 180.0 14_555 . 19_555 N
Cu1 N1 N1 122.17(28) 1_555 . 19_555 N
Cu1 N1 N2 128.8(4) 1_555 . 1_555 N
N1 N1 N2 109.03(22) 19_555 . 1_555 N
C1 N2 N1 104.9(4) 1_555 . 1_555 N
C1 N2 Cu2 129.5(9) 1_555 . 1_555 N
N1 N2 Cu2 114.4(6) 1_555 . 1_555 N
N2 Cu2 N2 113.0(9) 1_555 . 4_555 N
N2 Cu2 O1b 99.0(12) 1_555 . 1_555 N
N2 Cu2 Cl2 108.9(9) 1_555 . 1_555 N
N2 Cu2 O1b 99.0(12) 4_555 . 1_555 N
N2 Cu2 Cl2 108.9(9) 4_555 . 1_555 N
O1b Cu2 Cl2 19.6(5) 1_555 . 1_555 N
O1a C1a O1b 178.5(10) 1_555 . 1_555 N
O1a C1a Os 19.1(8) 1_555 . 1_555 N
O1a C1a Cl2 162.2(16) 1_555 . 1_555 N
O1b C1a Os 162.4(11) 1_555 . 1_555 N
O1b C1a Cl2 16.3(16) 1_555 . 1_555 N
Os C1a Cl2 178.8(15) 1_555 . 1_555 N
C1a O1a C1a 150.3(16) 1_555 . 12_565 N
C1a O1a Os 104.8(8) 1_555 . 1_555 N
C1a O1a Os 104.8(8) 12_565 . 1_555 N
Cu2 O1b C1a 102.2(12) 1_555 . 1_555 N
Cu2 O1b Cl2 115.0(30) 1_555 . 1_555 N
C1a O1b Cl2 142.9(33) 1_555 . 1_555 N
C4a C4a C4a 60.0000(4) 2_555 . 3_555 N
C4a C4a O4a 108.4(30) 2_555 . 1_555 N
C4a C4a O4a 45(4) 2_555 . 2_555 N
C4a C4a O4a 76.2(21) 2_555 . 3_555 N
C4a C4a O4b 71(4) 2_555 . 1_555 N
C4a C4a O4a 108.4(30) 3_555 . 1_555 N
C4a C4a O4a 76.2(21) 3_555 . 2_555 N
C4a C4a O4a 45(4) 3_555 . 3_555 N
C4a C4a O4b 71(4) 3_555 . 1_555 N
O4a C4a O4a 64(5) 1_555 . 2_555 N
O4a C4a O4a 64(5) 1_555 . 3_555 N
O4a C4a O4b 180.00(5) 1_555 . 1_555 N
O4a C4a O4a 56.5(35) 2_555 . 3_555 N
O4a C4a O4b 116(8) 2_555 . 1_555 N
O4a C4a O4b 116(8) 3_555 . 1_555 N
C4a O4a C4a 27(5) 1_555 . 2_555 N
C4a O4a C4a 27(5) 1_555 . 3_555 N
C4a O4a O4a 71.6(30) 1_555 . 2_555 N
C4a O4a O4a 71.6(30) 1_555 . 3_555 N
C4a O4a O4a 133.4(8) 1_555 . 4_555 N
C4a O4a O4a 94(4) 1_555 . 6_555 N
C4a O4a O4a 166(4) 1_555 . 12_555 N
C4a O4a O4a 94(4) 1_555 . 16_555 N
C4a O4a O4a 133.4(8) 1_555 . 18_555 N
C4a O4a C4a 28(4) 2_555 . 3_555 N
C4a O4a O4a 45(4) 2_555 . 2_555 N
C4a O4a O4a 61.8(17) 2_555 . 3_555 N
C4a O4a O4a 120.5(25) 2_555 . 4_555 N
C4a O4a O4a 91(5) 2_555 . 6_555 N
C4a O4a O4a 163.3(35) 2_555 . 12_555 N
C4a O4a O4a 69(8) 2_555 . 16_555 N
C4a O4a O4a 147.8(16) 2_555 . 18_555 N
C4a O4a O4a 61.8(17) 3_555 . 2_555 N
C4a O4a O4a 45(4) 3_555 . 3_555 N
C4a O4a O4a 147.8(16) 3_555 . 4_555 N
C4a O4a O4a 69(8) 3_555 . 6_555 N
C4a O4a O4a 163.3(35) 3_555 . 12_555 N
C4a O4a O4a 91(5) 3_555 . 16_555 N
C4a O4a O4a 120.5(25) 3_555 . 18_555 N
O4a O4a O4a 60.0000(4) 2_555 . 3_555 N
O4a O4a O4a 90.0 2_555 . 4_555 N
O4a O4a O4a 86(4) 2_555 . 6_555 N
O4a O4a O4a 120.0000(4) 2_555 . 12_555 N
O4a O4a O4a 30(5) 2_555 . 16_555 N
O4a O4a O4a 135.0 2_555 . 18_555 N
O4a O4a O4a 135.0000(8) 3_555 . 4_555 N
O4a O4a O4a 30(5) 3_555 . 6_555 N
O4a O4a O4a 120.0000(9) 3_555 . 12_555 N
O4a O4a O4a 86(4) 3_555 . 16_555 N
O4a O4a O4a 90.0 3_555 . 18_555 N
O4a O4a O4a 127.6(23) 4_555 . 6_555 N
O4a O4a O4a 45.0000(8) 4_555 . 12_555 N
O4a O4a O4a 60(5) 4_555 . 16_555 N
O4a O4a O4a 90.0 4_555 . 18_555 N
O4a O4a O4a 94(4) 6_555 . 12_555 N
O4a O4a O4a 104(6) 6_555 . 16_555 N
O4a O4a O4a 60(5) 6_555 . 18_555 N
O4a O4a O4a 94(4) 12_555 . 16_555 N
O4a O4a O4a 45.0000(8) 12_555 . 18_555 N
O4a O4a O4a 127.6(23) 16_555 . 18_555 N
C4a O4b C4a 38(8) 1_555 . 2_555 N
C4a O4b C4a 38(8) 1_555 . 3_555 N
C4a O4b C4a 38(8) 2_555 . 3_555 N
C2a C2a C2a 45.0000(8) 4_555 . 14_555 N
C2a C2a C2a 45.0000(8) 4_555 . 17_555 N
C2a C2a O2b 125.5(10) 4_555 . 1_555 N
C2a C2a O2b 67.9(5) 4_555 . 14_555 N
C2a C2a O2b 67.9(5) 4_555 . 17_555 N
C2a C2a O2a 55.1(14) 4_555 . 1_555 N
C2a C2a C2a 90.0000(15) 14_555 . 17_555 N
C2a C2a O2b 114.2(6) 14_555 . 1_555 N
C2a C2a O2b 36.8(8) 14_555 . 14_555 N
C2a C2a O2b 105.6(4) 14_555 . 17_555 N
C2a C2a O2a 66.1(9) 14_555 . 1_555 N
C2a C2a O2b 114.2(6) 17_555 . 1_555 N
C2a C2a O2b 105.6(4) 17_555 . 14_555 N
C2a C2a O2b 36.8(8) 17_555 . 17_555 N
C2a C2a O2a 66.1(9) 17_555 . 1_555 N
O2b C2a O2b 77.4(12) 1_555 . 14_555 N
O2b C2a O2b 77.4(12) 1_555 . 17_555 N
O2b C2a O2a 180.000(16) 1_555 . 1_555 N
O2b C2a O2b 98.4(12) 14_555 . 17_555 N
O2b C2a O2a 102.9(16) 14_555 . 1_555 N
O2b C2a O2a 102.9(16) 17_555 . 1_555 N
C2a O2b C2a 29.0(7) 1_555 . 14_555 N
C2a O2b C2a 29.0(7) 1_555 . 17_555 N
C2a O2b O3a 174(4) 1_555 . 14_555 N
C2a O2b O3b 126.5(18) 1_555 . 2_555 N
C2a O2b C2a 44.1(9) 14_555 . 17_555 N
C2a O2b O3a 146.6(28) 14_555 . 14_555 N
C2a O2b O3b 140.0(13) 14_555 . 2_555 N
C2a O2b O3a 146.6(28) 17_555 . 14_555 N
C2a O2b O3b 140.0(13) 17_555 . 2_555 N
O3a O2b O3b 59.9(30) 14_555 . 2_555 N
C2a O2a C2a 69.8(27) 1_555 . 4_555 N
C2a O2a C2a 47.7(17) 1_555 . 14_555 N
C2a O2a C2a 47.7(17) 1_555 . 17_555 N
C2a O2a C2a 47.7(17) 4_555 . 14_555 N
C2a O2a C2a 47.7(17) 4_555 . 17_555 N
C2a O2a C2a 69.8(27) 14_555 . 17_555 N
O3a C3a O3a 114(8) 1_555 . 13_555 N
O3a C3a O3b 180.000(19) 1_555 . 1_555 N
O3a C3a O3b 65(4) 1_555 . 13_555 N
O3a C3a O3b 65(4) 13_555 . 1_555 N
O3a C3a O3b 180.000(19) 13_555 . 13_555 N
O3b C3a O3b 115(8) 1_555 . 13_555 N
O2b O3a C3a 131(6) 14_555 . 1_555 N
O2b O3a O3b 74(5) 14_555 . 13_555 N
C3a O3a O3b 56.9(22) 1_555 . 13_555 N
O2b O3b C3a 103(4) 3_555 . 1_555 N
O2b O3b O3a 46(4) 3_555 . 13_555 N
C3a O3b O3a 57.6(22) 1_555 . 13_555 N
C1a Os C1a 112.2(13) 1_555 . 12_565 N
C1a Os O1a 56.1(7) 1_555 . 1_555 N
C1a Os O1a 56.1(7) 12_565 . 1_555 N
Cu2 Cl2 Cu2 72.1(12) 1_555 . 13_555 N
Cu2 Cl2 C1a 66.3(11) 1_555 . 1_555 N
Cu2 Cl2 C1a 138.4(15) 1_555 . 13_555 N
Cu2 Cl2 O1b 45.5(27) 1_555 . 1_555 N
Cu2 Cl2 O1b 117.6(31) 1_555 . 13_555 N
Cu2 Cl2 C1a 138.4(15) 13_555 . 1_555 N
Cu2 Cl2 C1a 66.3(11) 13_555 . 13_555 N
Cu2 Cl2 O1b 117.6(31) 13_555 . 1_555 N
Cu2 Cl2 O1b 45.5(27) 13_555 . 13_555 N
C1a Cl2 C1a 155.3(24) 1_555 . 13_555 N
C1a Cl2 O1b 20.8(18) 1_555 . 1_555 N
C1a Cl2 O1b 176(4) 1_555 . 13_555 N
C1a Cl2 O1b 176(4) 13_555 . 1_555 N
C1a Cl2 O1b 20.8(18) 13_555 . 13_555 N
O1b Cl2 O1b 163(6) 1_555 . 13_555 N

# Powder diffraction data for histogram  6
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT601_1P5CO2_FINAL_publ   
;
PROBLEM: Structure Contains Solvent Accessible VOIDS of .   2673 Ang3     ! Info 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT430_1P5CO2_FINAL_publ   
;
PROBLEM:  Short Inter D...A Contact  O3A    ..  O3A     ..       2.60 Ang. 
RESPONSE:The problem happens because the adsorbed carbon dioxide on the open metal sites are disordered and thus some atoms ostensibly are seemed to be close to each other.
;



# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_cell_measurement_theta_min      4.5
_cell_measurement_theta_max      160

_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Cu 16.608 0.7718 International_Tables_Vol_C
C 92.086 0.6648 International_Tables_Vol_C
Cl 5.304 0.9579 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 24.0 -0.3741 International_Tables_Vol_C
O 42.258 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.0782
_pd_proc_ls_prof_R_factor        0.0319
_pd_proc_ls_prof_wR_factor       0.0369
_pd_proc_ls_prof_wR_expected     0.0355
_refine_ls_R_Fsqd_factor         0.05263

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    698.466     2:   -121.677     3:    185.559     4:    1.99339    
      5:    96.4740     6:   -9.51754     7:    57.9160     8:   -9.09569    
      9:    30.1520    10:   -9.64698    11:    5.82812    12:   -6.89541    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  537.085 #2(GV)   = -265.342 #3(GW)   =   81.753
 #4(GP)   =   37.085 #5(LX)   =    1.057 #6(LY)   =    7.902
 #7(S/L)  =   0.0326 #8(H/L)  =   0.0280
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0005 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00050
_pd_proc_info_datetime           2016-02-24T11:36:21
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.5014
_pd_proc_2theta_range_max        166.2514
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
6050(170) 0.0 1618. .
5230(160) 0.0 1608. .
5020(150) 0.0 1598. .
4400(140) 0.0 1589. .
3960(140) 0.0 1580. .
3670(130) 0.0 1570. .
3450(130) 0.0 1561. .
3130(120) 0.0 1552. .
2830(110) 0.0 1543. .
2430(110) 0.0 1534. .
2520(110) 0.0 1525. .
2220(100) 0.0 1516. .
2330(100) 0.0 1508. .
1836(92) 0.0 1499. .
2026(97) 0.0 1491. .
2100(99) 0.0 1482. .
1638(87) 0.0 1474. .
1841(92) 0.0 1466. .
1809(92) 0.0 1457. .
1887(94) 0.0 1449. .
1859(93) 0.0 1441. .
1841(92) 0.0 1433. .
1698(89) 0.0 1426. .
1813(92) 0.0 1418. .
1850(93) 0.0 1410. .
1712(89) 0.0 1402. .
1813(92) 0.0 1395. .
1679(88) 0.0 1387. .
1693(89) 0.0 1380. .
1850(93) 0.0 1373. .
1573(85) 0.0 1365. .
1568(85) 0.0 1358. .
1439(82) 0.0 1351. .
1513(84) 0.0 1344. .
1397(80) 0.0 1337. .
1328(78) 0.0 1330. .
1420(81) 0.0 1324. .
1351(79) 0.0 1317. .
1503(83) 0.0 1310. .
1332(79) 0.0 1303. .
1226(75) 0.0 1297. .
1268(77) 0.0 1290. .
1411(81) 0.0 1284. .
1355(79) 0.0 1278. .
1397(80) 0.0 1271. .
1240(76) 0.0 1265. .
1346(79) 0.0 1259. .
1166(74) 0.0 1253. .
1166(74) 0.0 1247. .
1124(72) 0.0 1241. .
1018(69) 0.0 1235. .
1101(71) 0.0001984 1229. 1229.
1254(76) 0.0001731 1223. 1223.
1203(75) 0.0001778 1218. 1218.
1249(76) 0.0001731 1212. 1212.
1244(76) 0.0001731 1206. 1206.
1189(74) 0.0001826 1201. 1201.
1110(72) 0.0001929 1195. 1195.
1194(74) 0.0001826 1190. 1198.
1124(72) 0.0001929 1185. 1193.
981(67) 0.0002228 1179. 1188.
1240(76) 0.0001731 1174. 1184.
1110(72) 0.0001929 1169. 1179.
1194(74) 0.0001826 1164. 1175.
1120(72) 0.0001929 1159. 1170.
1046(70) 0.0002041 1154. 1166.
1027(69) 0.0002100 1149. 1162.
1207(75) 0.0001778 1144. 1158.
1129(72) 0.0001929 1139. 1155.
1069(70) 0.0002041 1134. 1151.
1180(74) 0.0001826 1129. 1148.
1157(73) 0.0001877 1125. 1145.
1217(75) 0.0001778 1120. 1143.
1221(75) 0.0001778 1115. 1142.
1351(79) 0.0001602 1111. 1143.
1513(84) 0.0001417 1106. 1150.
1471(83) 0.0001452 1102. 1169.
1443(82) 0.0001487 1097. 1211.
1633(87) 0.0001321 1093. 1289.
1785(91) 0.0001208 1089. 1411.
1735(90) 0.0001235 1084. 1580.
1994(96) 0.0001085 1080. 1794.
2150(100) 0.0001000 1076. 2047.
2360(110) 0.0000907 1072. 2335.
2660(110) 0.0000812 1068. 2660.
2860(120) 0.0000756 1064. 3025.
3380(130) 0.0000640 1060. 3439.
3700(130) 0.0000583 1056. 3912.
4300(140) 0.0000503 1052. 4459.
4710(150) 0.0000457 1048. 5105.
5610(160) 0.0000386 1044. 5887.
6650(180) 0.0000327 1040. 6868.
7770(190) 0.0000277 1037. 8158.
9560(210) 0.0000227 1033. 9926.
12440(240) 0.0000174 1029. 12345.
15890(270) 0.0000136 1026. 15380.
18900(300) 0.0000114 1022. 18466.
20920(310) 0.0000103 1018. 20414.
21060(310) 0.0000103 1015. 19950.
17820(290) 0.0000121 1012. 16744.
11310(160) 0.0000401 1008. 11949.
7440(130) 0.0000610 1005. 7345.
4431(98) 0.0001041 1001. 4078.
2451(73) 0.0001877 998. 2283.
1622(59) 0.0002873 995. 1497.
1213(51) 0.000384 992. 1211.
1139(49) 0.000416 988. 1116.
1023(47) 0.000453 985. 1079.
1065(48) 0.000434 982. 1058.
1009(47) 0.000453 979. 1043.
1065(48) 0.000434 976. 1031.
1067(48) 0.000434 973. 1023.
972(46) 0.000473 970. 1014.
951(45) 0.000494 967. 1007.
1010(47) 0.000453 964. 1000.
966(46) 0.000473 961. 994.
873(43) 0.000541 958. 988.
917(44) 0.000517 956. 983.
937(45) 0.000494 953. 979.
989(46) 0.000473 950. 974.
881(43) 0.000541 947. 970.
982(46) 0.000473 945. 966.
803(41) 0.000595 942. 963.
928(45) 0.000494 939. 959.
866(43) 0.000541 937. 956.
885(43) 0.000541 934. 953.
848(43) 0.000541 932. 950.
813(42) 0.000567 929. 948.
927(45) 0.000494 927. 945.
946(45) 0.000494 924. 943.
892(44) 0.000517 922. 941.
900(44) 0.000517 920. 931.
869(43) 0.000541 917. 930.
929(45) 0.000494 915. 930.
969(46) 0.000473 913. 932.
1083(48) 0.000434 910. 938.
1087(48) 0.000434 908. 953.
1083(48) 0.000434 906. 985.
1239(52) 0.000370 904. 1044.
1252(52) 0.000370 902. 1139.
1318(53) 0.000356 899. 1273.
1421(55) 0.0003306 897. 1448.
1620(59) 0.0002873 895. 1666.
1892(64) 0.0002441 893. 1932.
2182(69) 0.0002100 891. 2265.
2657(76) 0.0001731 889. 2694.
3186(84) 0.0001417 887. 3275.
4075(95) 0.0001108 885. 4084.
5310(110) 0.0000857 883. 5159.
6690(120) 0.0000683 881. 6392.
7860(130) 0.0000574 880. 7417.
7810(130) 0.0000583 878. 7714.
7110(130) 0.0000640 876. 6961.
5500(110) 0.0000826 874. 5383.
3750(91) 0.0001208 872. 3637.
2458(73) 0.0001877 870. 2280.
1531(58) 0.0002973 869. 1479.
1197(51) 0.000384 867. 1109.
953(45) 0.000494 865. 970.
906(44) 0.000517 864. 923.
873(43) 0.000541 862. 906.
917(44) 0.000517 860. 897.
873(43) 0.000541 859. 891.
810(42) 0.000567 857. 886.
856(43) 0.000541 855. 881.
824(42) 0.000567 854. 878.
846(42) 0.000567 852. 875.
856(43) 0.000541 851. 873.
821(42) 0.000567 849. 871.
832(42) 0.000567 848. 869.
820(42) 0.000567 846. 868.
755(40) 0.000625 845. 867.
879(43) 0.000541 844. 866.
858(43) 0.000541 842. 866.
890(44) 0.000517 841. 866.
809(41) 0.000595 839. 867.
899(44) 0.000517 838. 869.
961(45) 0.000494 837. 872.
906(44) 0.000517 835. 880.
1020(47) 0.000453 834. 900.
980(46) 0.000473 833. 943.
1185(51) 0.000384 831. 1030.
1297(53) 0.000356 830. 1185.
1525(58) 0.0002973 829. 1425.
1800(63) 0.0002520 828. 1765.
2208(69) 0.0002100 827. 2228.
2693(77) 0.0001687 825. 2847.
3432(87) 0.0001321 824. 3697.
4680(100) 0.0000980 823. 4887.
6570(120) 0.0000694 822. 6487.
8220(140) 0.0000549 821. 8356.
9920(150) 0.0000457 820. 9964.
10190(150) 0.0000444 819. 10523.
9080(140) 0.0000503 817. 9515.
6990(120) 0.0000650 816. 7263.
4650(100) 0.0000980 815. 4749.
2460(100) 0.0001000 814. 2800.
1450(77) 0.0001687 813. 1663.
1060(65) 0.0002367 812. 1146.
969(62) 0.0002601 811. 954.
903(43) 0.000541 810. 890.
826(41) 0.000595 809. 867.
820(41) 0.000595 808. 854.
826(41) 0.000595 807. 846.
896(43) 0.000541 807. 839.
909(44) 0.000517 806. 834.
845(42) 0.000567 805. 829.
863(42) 0.000567 804. 825.
899(43) 0.000541 803. 822.
858(42) 0.000567 802. 819.
866(42) 0.000567 801. 816.
852(42) 0.000567 800. 814.
817(41) 0.000595 799. 812.
874(43) 0.000541 799. 810.
857(42) 0.000567 798. 809.
789(40) 0.000625 797. 807.
832(42) 0.000567 796. 807.
880(43) 0.000541 795. 807.
829(41) 0.000595 795. 809.
795(41) 0.000595 794. 813.
833(42) 0.000567 793. 819.
821(41) 0.000595 792. 829.
873(43) 0.000541 792. 844.
962(45) 0.000494 791. 865.
967(45) 0.000494 790. 893.
969(45) 0.000494 790. 919.
1018(46) 0.000473 789. 941.
966(45) 0.000494 788. 942.
931(44) 0.000517 788. 917.
899(43) 0.000541 787. 876.
864(42) 0.000567 786. 836.
859(42) 0.000567 786. 809.
817(41) 0.000595 785. 795.
822(41) 0.000595 784. 788.
785(40) 0.000625 784. 786.
818(41) 0.000595 783. 784.
756(39) 0.000657 782. 783.
800(41) 0.000595 782. 783.
765(40) 0.000625 781. 782.
778(40) 0.000625 781. 781.
836(42) 0.000567 780. 781.
725(39) 0.000657 780. 780.
776(40) 0.000625 779. 780.
793(41) 0.000595 779. 779.
766(40) 0.000625 778. 778.
750(39) 0.000657 777. 778.
790(40) 0.000625 777. 778.
740(39) 0.000657 776. 777.
742(39) 0.000657 776. 777.
772(40) 0.000625 775. 777.
803(41) 0.000595 775. 778.
790(40) 0.000625 774. 780.
747(39) 0.000657 774. 783.
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819(26) 0.001479 644.0 846.3
826(26) 0.001479 645.2 850.4
836(26) 0.001479 646.4 854.5
842(26) 0.001479 647.7 858.4
856(27) 0.001372 648.9 862.2
865(27) 0.001372 650.2 865.8
857(27) 0.001372 651.4 869.3
834(26) 0.001479 652.7 872.7
895(27) 0.001372 654.0 876.0
845(26) 0.001479 655.3 879.1
868(27) 0.001372 656.6 882.1
870(27) 0.001372 657.9 885.0
869(27) 0.001372 659.2 887.7
882(27) 0.001372 660.6 890.3
877(27) 0.001372 661.9 892.8
937(28) 0.001276 663.3 895.1
908(27) 0.001372 664.6 897.3
883(27) 0.001372 666.0 899.4
865(27) 0.001372 667.4 901.3
878(27) 0.001372 668.8 903.2
914(27) 0.001372 670.2 904.9
919(28) 0.001276 671.6 906.6
913(27) 0.001372 673.0 908.2
872(27) 0.001372 674.5 909.6
906(27) 0.001372 675.9 911.0
922(28) 0.001276 677.4 912.4
898(27) 0.001372 678.9 913.6
913(28) 0.001276 680.3 914.8
960(28) 0.001276 681.8 915.9
902(27) 0.001372 683.3 917.0
930(28) 0.001276 684.8 918.0
912(27) 0.001372 686.4 919.0
940(28) 0.001276 687.9 919.9
915(27) 0.001372 689.5 920.7
881(27) 0.001372 691.0 921.6
924(28) 0.001276 692.6 922.3
925(28) 0.001276 694.2 923.1
914(27) 0.001372 695.7 923.8
893(27) 0.001372 697.3 924.4
922(28) 0.001276 699.0 925.0
932(28) 0.001276 700.6 925.6
934(28) 0.001276 702.2 926.1
930(28) 0.001276 703.9 926.5
912(27) 0.001372 705.5 927.0
903(27) 0.001372 707.2 927.3
968(28) 0.001276 708.9 927.6
912(27) 0.001372 710.6 927.8
929(28) 0.001276 712.3 928.0
935(28) 0.001276 714.0 928.1
925(28) 0.001276 715.7 928.2
935(28) 0.001276 717.4 928.1
900(27) 0.001372 719.2 928.0
950(28) 0.001276 720.9 927.9
961(28) 0.001276 722.7 927.7
896(27) 0.001372 724.5 927.4
926(28) 0.001276 726.3 927.0
904(27) 0.001372 728.1 926.6
921(28) 0.001276 729.9 926.1
930(28) 0.001276 731.7 925.5
931(28) 0.001276 733.6 924.9
941(28) 0.001276 735.4 924.3
909(27) 0.001372 737.3 923.6
939(28) 0.001276 739.2 922.8
957(28) 0.001276 741.1 922.0
943(28) 0.001276 743.0 921.2
922(28) 0.001276 744.9 920.3
913(27) 0.001372 746.8 919.4
938(28) 0.001276 748.7 918.5
932(28) 0.001276 750.7 917.6
885(27) 0.001372 752.6 916.7
907(27) 0.001372 754.6 915.8
927(28) 0.001276 756.6 914.8
933(28) 0.001276 758.6 913.9
947(28) 0.001276 760.6 913.0
940(28) 0.001276 762.6 912.2
913(28) 0.001276 764.6 911.3
936(28) 0.001276 766.7 910.5
904(27) 0.001372 768.7 909.7
929(28) 0.001276 770.8 908.9
938(28) 0.001276 772.9 908.2
908(27) 0.001372 774.9 907.6
928(28) 0.001276 777.0 906.9
944(28) 0.001276 779.2 906.4
945(28) 0.001276 781.3 905.9
897(27) 0.001372 783.4 905.5
905(27) 0.001372 785.6 905.1
960(41) 0.000595 788. 905.
873(39) 0.000657 790. 905.
923(40) 0.000625 792. 904.
917(40) 0.000625 794. 904.
877(39) 0.000657 797. 904.
833(38) 0.000693 799. 904.
899(40) 0.000625 801. 905.
966(41) 0.000595 803. 905.
900(40) 0.000625 805. 905.
912(40) 0.000625 808. 905.
868(39) 0.000657 810. 906.
881(39) 0.000657 812. 907.
952(41) 0.000595 815. 907.
881(39) 0.000657 817. 908.
920(40) 0.000625 819. 909.
939(40) 0.000625 822. 910.
936(40) 0.000625 824. 911.
912(40) 0.000625 826. 912.
981(41) 0.000595 829. 913.
932(40) 0.000625 831. 914.
949(41) 0.000595 834. 916.
918(40) 0.000625 836. 917.
925(40) 0.000625 838. 919.
880(39) 0.000657 841. 920.
910(40) 0.000625 843. 922.
904(40) 0.000625 846. 924.
909(40) 0.000625 848. 926.
925(40) 0.000625 851. 928.
920(40) 0.000625 853. 930.
901(40) 0.000625 856. 932.
1014(42) 0.000567 858. 934.
1004(42) 0.000567 861. 937.
907(40) 0.000625 863. 939.
859(39) 0.000657 866. 942.
952(41) 0.000595 868. 944.
1041(42) 0.000567 871. 947.
979(41) 0.000595 874. 950.
946(40) 0.000625 876. 953.
901(40) 0.000625 879. 956.
948(41) 0.000595 881. 959.
971(41) 0.000595 884. 962.
963(41) 0.000595 887. 965.
929(40) 0.000625 889. 969.
927(40) 0.000625 892. 972.
933(40) 0.000625 895. 975.
1012(42) 0.000567 898. 979.
933(40) 0.000625 900. 983.
919(40) 0.000625 903. 986.
968(41) 0.000595 906. 990.
985(41) 0.000595 908. 994.
987(41) 0.000595 911. 998.
1055(43) 0.000541 914. 1002.
1027(42) 0.000567 917. 1006.
1031(42) 0.000567 920. 1010.
1030(42) . . .
1077(43) . . .
1075(43) . . .
1065(43) . . .
1087(43) . . .
1073(43) . . .
1076(43) . . .
1025(42) . . .
1029(42) . . .
1072(43) . . .
1062(43) . . .
1111(44) . . .
1075(43) . . .
1074(43) . . .
1022(42) . . .
1048(42) . . .
1064(43) . . .
1051(42) . . .
1052(42) . . .
1081(43) . . .
1032(42) . . .
1086(43) . . .
1165(45) . . .
1171(45) . . .
1096(43) . . .
1090(43) . . .
1134(44) . . .
1121(44) . . .
1168(45) . . .
1082(43) . . .
1103(43) . . .
1129(44) . . .
1085(43) . . .
1109(44) . . .
1174(45) . . .
1117(44) . . .
1136(44) . . .
1139(44) . . .
1244(46) . . .
1215(45) . . .
1148(44) . . .
1148(44) . . .
1177(45) . . .
1132(44) . . .
1097(43) . . .
1146(44) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_cell_measurement_reflns_used    639
_reflns_number_total             639
_reflns_limit_h_min              1
_reflns_limit_h_max              17
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.053
_reflns_d_resolution_low         18.532
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1CO2_publ
_database_code_depnum_ccdc_archive 'CCDC 1582004'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-03-08T11:11|1CO2||c2

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-03-08T11:11

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.04
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     45
_refine_ls_goodness_of_fit_all   2.13
_refine_ls_number_restraints     7
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    30

_cell_measurement_theta_min      5
_cell_measurement_theta_max      117

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from F:/Gas Storage Research/Jeff Long/Fe-BTT with Kenji/0p5 wt %/'
_cell_length_a                   18.7761(6)
_cell_length_b                   18.7761
_cell_length_c                   18.7761
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6619.4(6)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cr Cr1 0.1340(16) 0.5 0.0 1.0 Uiso 0.010(3) 12
C C1 0.1476(5) 0.3328(8) -0.1476(5) 1.0 Uiso 0.0115(29) 24
C C2 0.1811(5) 0.2703(6) -0.1811(5) 1.0 Uiso 0.0115(29) 24
C C3 0.2440(5) 0.2440(5) -0.1484(6) 1.0 Uiso 0.0115(29) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.124(15) 3
N N1 0.13139(30) 0.42209(34) -0.07877(30) 1.0 Uiso 0.0103(14) 48
N N2 0.1748(4) 0.36949(32) -0.0924(4) 1.0 Uiso 0.0103(14) 48
H H1 0.2635(7) 0.2635(7) -0.1027(9) 1.0 Uiso 0.02(1) 24
O Os 0.2334(19) 0.5 0.0 0.22 Uiso 0.004 12
C Ca 0.2892(21) 0.4385(8) 0.0 0.218(5) Uiso 0.012(3) 24
O Oa 0.2767(18) 0.5 0.0 0.436(10) Uiso 0.018(2) 12
O Ob 0.3057(27) 0.3784(11) 0.0 0.218(5) Uiso 0.012(2) 24

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C25.75 H8 Cl Cr4 N32 O4.45'
_chemical_formula_weight         1080.17
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cr1 Cl1 2.517(30) . 1_555 N
Cr1 N1 2.081(5) . 1_555 N
Cr1 N1 2.081(5) . 4_555 N
Cr1 N1 2.081(5) . 12_565 N
Cr1 N1 2.081(5) . -10_565 N
Cr1 Os 1.865(21) . 1_555 N
Cr1 Oa 2.678(20) . 1_555 N
C1 C2 1.471(16) . 1_555 N
C1 N1 2.139(14) . 1_555 N
C1 N1 2.139(14) . 19_555 N
C1 N2 1.345(8) . 1_555 N
C1 N2 1.345(8) . 19_555 N
C2 C1 1.471(16) . 1_555 N
C2 C2 2.369(20) . 7_555 N
C2 C2 2.369(20) . 9_555 N
C2 C3 1.420(7) . 1_555 N
C2 C3 1.420(7) . 7_555 N
C3 C2 1.420(7) . 1_555 N
C3 C2 1.420(7) . 9_555 N
C3 H1 1.001(18) . 1_555 N
Cl1 Cr1 2.517(30) . 1_555 N
Cl1 Cr1 2.517(30) . 10_555 N
Cl1 Cr1 2.517(30) . 14_555 N
Cl1 Cr1 2.517(30) . 19_555 N
N1 Cr1 2.081(5) . 1_555 N
N1 C1 2.139(14) . 1_555 N
N1 N1 1.397(12) . 19_555 N
N1 N2 1.306(7) . 1_555 N
N1 N2 2.182(7) . 19_555 N
N2 C1 1.345(8) . 1_555 N
N2 N1 1.306(7) . 1_555 N
N2 N1 2.182(7) . 19_555 N
N2 N2 2.188(14) . 19_555 N
H1 C3 1.001(18) . 1_555 N
Os Cr1 1.865(21) . 1_555 N
Os Ca 1.560(30) . 1_555 N
Os Ca 1.560(30) . 12_565 N
Os Oa 0.813(29) . 1_555 N
Ca Os 1.560(30) . 1_555 N
Ca Ca 2.311(29) . 12_565 N
Ca Oa 1.179(10) . 1_555 N
Ca Ob 1.169(11) . 1_555 N
Oa Cr1 2.678(20) . 1_555 N
Oa Os 0.813(29) . 1_555 N
Oa Ca 1.179(10) . 1_555 N
Oa Ca 1.179(10) . 12_565 N
Oa Ob 2.347(15) . 1_555 N
Oa Ob 2.347(15) . 12_565 N
Ob Ca 1.169(11) . 1_555 N
Ob Oa 2.347(15) . 1_555 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Cr1 N1 88.6(9) 1_555 . 1_555 N
Cl1 Cr1 N1 88.6(9) 1_555 . 4_555 N
Cl1 Cr1 N1 88.6(9) 1_555 . 12_565 N
Cl1 Cr1 N1 88.6(9) 1_555 . -10_565 N
Cl1 Cr1 Os 180.0 1_555 . 1_555 N
N1 Cr1 N1 90.6(4) 1_555 . 4_555 N
N1 Cr1 N1 177.3(17) 1_555 . 12_565 N
N1 Cr1 N1 89.3(4) 1_555 . -10_565 N
N1 Cr1 Os 91.4(9) 1_555 . 1_555 N
N1 Cr1 N1 89.3(4) 4_555 . 12_565 N
N1 Cr1 N1 177.3(17) 4_555 . -10_565 N
N1 Cr1 Os 91.4(9) 4_555 . 1_555 N
N1 Cr1 N1 90.6(4) 12_565 . -10_565 N
N1 Cr1 Os 91.4(9) 12_565 . 1_555 N
N1 Cr1 Os 91.4(9) -10_565 . 1_555 N
C2 C1 N2 125.1(6) 1_555 . 1_555 N
C2 C1 N2 125.1(6) 1_555 . 19_555 N
N2 C1 N2 108.8(13) 1_555 . 19_555 N
C1 C2 C3 116.6(6) 1_555 . 1_555 N
C1 C2 C3 116.6(6) 1_555 . 7_555 N
C3 C2 C3 126.8(12) 1_555 . 7_555 N
C2 C3 C2 113.0(12) 1_555 . 9_555 N
C2 C3 H1 123.2(6) 1_555 . 1_555 N
C2 C3 H1 123.2(6) 9_555 . 1_555 N
Cr1 Cl1 Cr1 180.0 1_555 . 10_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 19_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 19_555 N
Cr1 Cl1 Cr1 180.0 14_555 . 19_555 N
Cr1 N1 N1 121.3(7) 1_555 . 19_555 N
Cr1 N1 N2 131.0(9) 1_555 . 1_555 N
N1 N1 N2 107.6(5) 19_555 . 1_555 N
C1 N2 N1 107.6(9) 1_555 . 1_555 N
Cr1 Os Ca 132.2(16) 1_555 . 1_555 N
Cr1 Os Ca 132.2(16) 1_555 . 12_565 N
Cr1 Os Oa 180.0 1_555 . 1_555 N
Ca Os Ca 95.6(33) 1_555 . 12_565 N
Ca Os Oa 47.8(16) 1_555 . 1_555 N
Ca Os Oa 47.8(16) 12_565 . 1_555 N
Os Ca Oa 30.7(13) 1_555 . 1_555 N
Os Ca Ob 153(4) 1_555 . 1_555 N
Oa Ca Ob 176(5) 1_555 . 1_555 N
Os Oa Ca 101.5(25) 1_555 . 1_555 N
Os Oa Ca 101.5(25) 1_555 . 12_565 N
Ca Oa Ca 157(5) 1_555 . 12_565 N

# Powder diffraction data for histogram  4
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT602_1CO2_publ           
;
PROBLEM: Test for (Unreported) solvent accessible voids        ! Info 
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT049_1CO2_publ           
;
PROBLEM: Calculated Density less than 1.0 gcm-3 .........     0.9020 Check 
RESPONSE: This is expected as the material is porous.
;

_vrf_PLAT183_1CO2_publ           
;
PROBLEM:  Missing _cell_measurement_reflns_used value ....     Please Do ! 
RESPONSE: This is the CIF file based on rietvald refinement of powder diffraction pattern and therefore the number of reflections is not provided.
;

_vrf_PLAT430_1CO2_publ           
;
PROBLEM: Short Inter D...A Contact  Ob     ..  Ob      ..       1.92 Ang.  
RESPONSE:  The problem happens because the adsorbed carbon dioxide on the open metal sites are disordered and thus some atoms ostensibly are seemed to be close to each other.
;


# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_diffrn_ambient_temperature      30
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  C2
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Cr 12.0 0.3635 International_Tables_Vol_C
C 77.237 0.6646 International_Tables_Vol_C
Cl 3.0 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 24.0 -0.3739 International_Tables_Vol_C
O 13.353 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.37039
_pd_proc_ls_prof_R_factor        0.0284
_pd_proc_ls_prof_wR_factor       0.0360
_pd_proc_ls_prof_wR_expected     0.0173
_refine_ls_R_Fsqd_factor         0.05807

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 16 terms.
 Shifted Chebyshev function of 1st kind
      1:    2374.65     2:   -509.536     3:    174.214     4:   -8.44540    
      5:    77.9087     6:    26.6667     7:   -13.0880     8:   -20.3936    
      9:   -16.7192    10:    34.8309    11:    14.8467    12:   -14.3354    
     13:   -5.46108    14:    1.58679    15:    13.0466    16:    26.5208    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  972.824 #2(GV)   = ******** #3(GW)   =  326.988
 #4(GP)   =  317.388 #5(LX)   =    0.000 #6(LY)   =   13.069
 #7(S/L)  =   0.0402 #8(H/L)  =   0.0058
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2016-03-08T11:11:49
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        2.9001
_pd_meas_2theta_range_max        117.0758
_pd_meas_2theta_range_inc        0.1002
_pd_proc_2theta_range_min        2.5385
_pd_proc_2theta_range_max        116.7141
_pd_proc_2theta_range_inc        0.1002

loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
3628.0 0.0 2602.65112 .
3731.0 0.0 2651.89355 .
3766.0 0.0 2697.38379 .
3501.0 0.0 2739.33691 .
3429.0 0.0 2777.95752 .
3592.0 0.0 2813.44141 .
3278.0 0.0 2845.97485 .
3434.0 0.0 2875.73584 .
3457.0 0.0 2902.89307 .
3293.0 0.0 2927.60791 .
3437.0 0.0 2950.03345 .
3413.0 0.0 2970.31567 .
3317.0 0.0 2988.59277 .
3332.0 0.0 3004.99707 .
3218.0 0.0 3019.65259 .
3190.0 0.0 3032.67847 .
3227.0 0.0 3044.18677 .
3275.0 0.0 3054.28442 .
3141.0 0.0 3063.07178 .
3229.0 0.0 3070.64478 .
3114.0 0.0 3077.09326 .
3160.0 0.0003165 3082.50293 3082.50610
3001.0 0.0003332 3086.95386 3086.95703
3135.0 0.0003190 3090.52246 3090.52515
3167.0 0.0003158 3093.27979 3093.28223
3089.0 0.0003237 3095.29346 3095.29590
3047.0 0.0003282 3096.62695 3096.62915
3100.0 0.0003226 3097.33984 3097.34180
3025.0 0.0003306 3097.48779 3097.48950
3049.0 0.0003280 3097.12378 3097.12524
3146.0 0.0003179 3096.29639 3096.29761
3102.0 0.0003224 3095.05200 3111.07520
3173.0 0.0003152 3093.43359 3111.86865
3031.0 0.0003299 3091.48071 3113.08398
3128.0 0.0003197 3089.23120 3115.82983
3119.0 0.0003206 3086.71973 3124.42456
3100.0 0.0003226 3083.97852 3154.45801
3298.0 0.0003032 3081.03735 3253.94165
3424.0 0.0002921 3077.92383 3545.49048
4173.0 0.0002396 3074.66382 4283.90430
5744.0 0.0001741 3071.28076 5887.06787
8368.0 0.0001195 3067.79590 8856.06152
13636.0 0.0000733 3064.22949 13507.39551
20150.0 0.0000496 3060.59961 19559.40039
26867.0 0.0000372 3056.92261 25825.29102
31525.0 0.0000317 3053.21362 30399.80078
32564.0 0.0000307 3049.48608 31498.13867
28638.0 0.0000349 3045.75244 28535.38086
23117.0 0.0000433 3042.02319 22611.87305
16308.0 0.0000613 3038.30835 15865.37891
10686.0 0.0000936 3034.61670 10194.82324
6602.0 0.0001515 3030.95532 6434.66992
4366.0 0.0002290 3027.33130 4414.29004
3352.0 0.0002983 3023.74976 3520.87891
3218.0 0.0003108 3020.21606 3190.24976
3171.0 0.0003154 3016.73364 3083.87866
3037.0 0.0003293 3013.30615 3050.52271
3035.0 0.0003295 3009.93604 3009.93164
3021.0 0.0003310 3006.62524 3006.62085
3110.0 0.0003215 3003.37500 3003.37036
2989.0 0.0003346 3000.18604 3000.18140
3082.0 0.0003245 2997.05859 2997.05396
2998.0 0.0003336 2993.99268 3011.26953
3189.0 0.0003136 2990.98779 3010.95068
2871.0 0.0003483 2988.04248 3011.43408
2911.0 0.0003435 2985.15576 3013.40601
2970.0 0.0003367 2982.32593 3019.65283
3021.0 0.0003310 2979.55127 3041.47412
3135.0 0.0003190 2976.82910 3118.37109
3192.0 0.0003133 2974.15747 3363.41235
3914.0 0.0002555 2971.53369 4033.22876
5591.0 0.0001789 2968.95508 5568.39746
8475.0 0.0001180 2966.41870 8474.63965
13455.0 0.0000743 2963.92139 12935.57813
18369.0 0.0000544 2961.46021 18296.99609
23398.0 0.0000427 2959.03198 22920.17578
24438.0 0.0000409 2956.63354 24872.34570
22225.0 0.0000450 2954.26147 23183.52734
18045.0 0.0000554 2951.91284 18616.96875
13047.0 0.0000766 2949.58398 13121.37109
8582.0 0.0001165 2947.27148 8488.11035
5515.0 0.0001813 2944.97241 5485.75781
3747.0 0.0002669 2942.68359 3937.02393
3249.0 0.0003078 2940.40161 3287.93872
2963.0 0.0003375 2938.12329 3061.49341
3085.0 0.0003241 2935.84570 3017.30957
2962.0 0.0003376 2933.56592 2998.76855
3130.0 0.0003195 2931.28076 2993.50000
2935.0 0.0003407 2928.98755 2992.94043
3221.0 0.0003105 2926.68384 2996.61206
3127.0 0.0003198 2924.36646 2993.37817
3018.0 0.0003313 2922.03345 3046.86792
3131.0 0.0003194 2919.68213 3229.68188
3642.0 0.0002746 2917.31006 3793.46167
5107.0 0.0001958 2914.91528 5259.23828
8360.0 0.0001196 2912.49585 8382.11523
13740.0 0.0000728 2910.04956 13719.87402
21097.0 0.0000474 2907.57471 20813.83008
28120.0 0.0000356 2905.06958 27640.02344
31177.0 0.0000321 2902.53296 31287.86328
28766.0 0.0000348 2899.96313 29875.31445
22879.0 0.0000437 2897.35864 24099.57813
15758.0 0.0000635 2894.71875 16692.23828
10207.0 0.0000980 2892.04224 10341.19727
6322.0 0.0001582 2889.32837 6245.01514
4091.0 0.0002444 2886.57617 4172.40088
3237.0 0.0003089 2883.78491 3329.26440
3099.0 0.0003227 2880.95435 3044.95654
3027.0 0.0003304 2878.08398 2959.13721
3048.0 0.0003281 2875.17334 2930.57910
2946.0 0.0003394 2872.22266 2916.63452
2896.0 0.0003453 2869.23169 2907.09961
2935.0 0.0003407 2866.20044 2900.57397
2882.0 0.0003470 2863.12915 2871.84009
2916.0 0.0003429 2860.01831 2883.09033
2888.0 0.0003463 2856.86792 2909.32764
2957.0 0.0003382 2853.67871 2953.32813
3125.0 0.0003200 2850.45117 3007.02124
3232.0 0.0003094 2847.18628 3049.62305
3283.0 0.0003046 2843.88452 3058.45557
3255.0 0.0003072 2840.54688 3026.42773
2966.0 0.0003372 2837.17432 2968.97656
2961.0 0.0003377 2833.76758 2910.49805
2871.0 0.0003483 2830.32837 2867.21436
2698.0 0.000371 2826.85718 2841.76392
2819.0 0.000355 2823.35571 2828.72754
2702.0 0.000370 2819.82520 2821.87036
2816.0 0.000355 2816.26709 2817.36230
2870.0 0.0003484 2812.68262 2813.62744
2711.0 0.000369 2809.07324 2810.39624
2823.0 0.000354 2805.44067 2808.32715
2766.0 0.000362 2801.78662 2809.21216
2779.0 0.000360 2798.11230 2815.92603
2877.0 0.0003476 2794.41968 2830.55957
2881.0 0.0003471 2790.71021 2851.82593
2923.0 0.0003421 2786.98608 2871.89282
2961.0 0.0003377 2783.24854 2878.41455
2957.0 0.0003382 2779.49976 2865.95581
2941.0 0.0003400 2775.74121 2839.55127
2770.0 0.000361 2771.97485 2810.55078
2876.0 0.0003477 2768.20264 2787.68994
2705.0 0.000370 2764.42627 2773.19824
2737.0 0.000365 2760.64771 2764.89502
2712.0 0.000369 2756.86890 2759.93237
2670.0 0.000375 2753.09131 2757.01880
2655.0 0.000377 2749.31714 2757.73730
2820.0 0.000355 2745.54810 2768.97925
2713.0 0.000369 2741.78613 2806.13232
2955.0 0.0003384 2738.03296 2890.76880
3031.0 0.0003299 2734.29077 3033.74097
3285.0 0.0003044 2730.56079 3208.12354
3586.0 0.0002789 2726.84521 3341.97192
3480.0 0.0002874 2723.14551 3359.51099
3153.0 0.0003172 2719.46387 3247.08081
3058.0 0.0003270 2715.80176 3067.71533
2930.0 0.0003413 2712.16064 2901.94922
2773.0 0.000361 2708.54272 2792.13501
2800.0 0.000357 2704.94922 2735.96021
2777.0 0.000360 2701.38184 2712.03369
2746.0 0.000364 2697.84204 2702.05713
2717.0 0.000368 2694.33179 2696.69165
2705.0 0.000370 2690.85205 2692.57764
2675.0 0.000374 2687.40479 2691.81885
2706.0 0.000370 2683.99097 2688.54761
2693.0 0.000371 2680.61230 2685.43677
2688.0 0.000372 2677.26978 2682.49121
2709.0 0.000369 2673.96484 2679.72925
2742.0 0.000365 2670.69897 2677.18408
2710.0 0.000369 2667.47314 2674.90649
2608.0 0.000383 2664.28857 2672.46753
2711.0 0.000369 2661.14624 2671.12891
2661.0 0.000376 2658.04736 2671.00342
2744.0 0.000364 2654.99268 2675.25586
2585.0 0.000387 2651.98340 2696.76489
2792.0 0.000358 2649.02051 2775.92822
2988.0 0.0003347 2646.10449 3010.57861
3463.0 0.0002888 2643.23633 3514.53564
4365.0 0.0002291 2640.41699 4349.39697
5222.0 0.0001915 2637.64673 5329.28711
5894.0 0.0001697 2634.92651 6005.68750
5815.0 0.0001720 2632.25684 5965.16699
4932.0 0.0002028 2629.63818 5231.93994
4153.0 0.0002408 2627.07129 4245.37842
3373.0 0.0002965 2624.55615 3439.50952
2969.0 0.0003368 2622.09375 2973.74170
2764.0 0.000362 2619.68359 2786.51904
2798.0 0.000357 2617.32690 2790.60376
2975.0 0.0003361 2615.02295 3021.51099
3530.0 0.0002833 2612.77271 3687.37866
4808.0 0.0002080 2610.57593 5057.75000
7246.0 0.0001380 2608.43262 7115.37695
9163.0 0.0001091 2606.34302 9197.45703
9785.0 0.0001022 2604.30688 10184.38965
8614.0 0.0001161 2602.32446 9415.76758
7032.0 0.0001422 2600.39526 7403.62158
5180.0 0.0001931 2598.51929 5281.64795
3915.0 0.0002554 2596.69653 3794.75439
2997.0 0.0003337 2594.92627 3042.12646
2696.0 0.000371 2593.20850 2751.43945
2794.0 0.000358 2591.54297 2661.69434
2804.0 0.000357 2589.92920 2637.90308
2704.0 0.000370 2588.36670 2633.37256
2652.0 0.000377 2586.85498 2635.74023
2651.0 0.000377 2585.39355 2640.06372
2745.0 0.000364 2583.98193 2641.82202
2719.0 0.000368 2582.61963 2638.71704
2698.0 0.000371 2581.30566 2634.26392
2748.0 0.000364 2580.03979 2631.03467
2705.0 0.000370 2578.82104 2637.23706
2808.0 0.000356 2577.64893 2666.57373
2786.0 0.000359 2576.52222 2809.17212
3206.0 0.0003119 2575.44092 3250.00903
4136.0 0.0002418 2574.40332 4303.14990
6072.0 0.0001647 2573.40918 6162.21582
8299.0 0.0001205 2572.45752 8439.88379
9817.0 0.0001019 2571.54736 10034.18066
9673.0 0.0001034 2570.67773 9883.80469
8168.0 0.0001224 2569.84790 8094.47607
6157.0 0.0001624 2569.05664 5818.77588
4339.0 0.0002305 2568.30298 4079.46460
3256.0 0.0003071 2567.58618 3152.66162
2771.0 0.000361 2566.90479 2811.51050
2699.0 0.000371 2566.25806 2795.06543
3025.0 0.0003306 2565.64502 3003.27612
3264.0 0.0003064 2565.06421 3414.46045
3923.0 0.0002549 2564.51489 3914.40063
4074.0 0.0002455 2563.99561 4240.59180
4116.0 0.0002430 2563.50562 4162.87842
3739.0 0.0002675 2563.04370 3735.31763
3315.0 0.0003017 2562.60840 3231.83374
2970.0 0.0003367 2562.19897 2868.01611
2702.0 0.000370 2561.81421 2686.15039
2625.0 0.000381 2561.45264 2631.01514
2651.0 0.000377 2561.11328 2654.36206
2661.0 0.000376 2560.79517 2743.10449
2892.0 0.0003458 2560.49683 2876.28052
2959.0 0.0003380 2560.21704 3008.33276
3028.0 0.0003303 2559.95508 3047.90723
2860.0 0.0003497 2559.70923 2963.83057
2849.0 0.000351 2559.47876 2816.71802
2618.0 0.000382 2559.26245 2687.99414
2714.0 0.000368 2559.05884 2614.14502
2468.0 0.000405 2558.86694 2589.48779
2555.0 0.000391 2558.68579 2601.73047
2639.0 0.000379 2558.51392 2649.58374
2618.0 0.000382 2558.35034 2728.80664
2660.0 0.000376 2558.19385 2813.94702
2725.0 0.000367 2558.04346 2845.45239
2713.0 0.000369 2557.89795 2803.13452
2653.0 0.000377 2557.75635 2719.24658
2642.0 0.000379 2557.61768 2643.26343
2790.0 0.000358 2557.48047 2598.54028
2550.0 0.000392 2557.34375 2580.37524
2558.0 0.000391 2557.20679 2575.76489
2719.0 0.000368 2557.06836 2576.18701
2604.0 0.000384 2556.92749 2582.16235
2562.0 0.000390 2556.78296 2585.97412
2579.0 0.000388 2556.63428 2590.84619
2716.0 0.000368 2556.47998 2598.43408
2736.0 0.000365 2556.31934 2611.82617
2724.0 0.000367 2556.15137 2648.41309
2789.0 0.000359 2555.97534 2779.28320
3057.0 0.0003271 2555.79028 3207.68701
4062.0 0.0002462 2555.59521 4286.20410
6026.0 0.0001659 2555.38940 6227.74561
8728.0 0.0001146 2555.17188 8517.54297
10038.0 0.0000996 2554.94214 9831.27051
9392.0 0.0001065 2554.69897 9143.83203
7625.0 0.0001311 2554.44214 7018.25000
5277.0 0.0001895 2554.17041 4873.04395
3853.0 0.0002595 2553.88330 3566.30176
3278.0 0.0003051 2553.58032 3163.65796
3442.0 0.0002905 2553.26050 3506.22168
4682.0 0.0002136 2552.92334 4520.10498
6033.0 0.0001658 2552.56836 5905.87207
7202.0 0.0001389 2552.19458 6896.23682
7144.0 0.0001400 2551.80176 6720.78516
6007.0 0.0001665 2551.38916 5523.66016
4705.0 0.0002125 2550.95654 4169.01416
3400.0 0.0002941 2550.50317 3291.82959
3142.0 0.0003183 2550.02856 3017.12085
3190.0 0.0003135 2549.53247 3284.73755
3932.0 0.0002543 2549.01440 4058.05371
5219.0 0.0001916 2548.47388 5111.71533
5703.0 0.0001753 2547.91089 5840.27539
5757.0 0.0001737 2547.32446 5661.41162
4803.0 0.0002082 2546.71484 4723.39063
3986.0 0.0002509 2546.08154 3725.63477
3129.0 0.0003196 2545.42407 3155.08765
3052.0 0.0003277 2544.74268 3178.64771
3501.0 0.0002856 2544.03687 3910.03638
5171.0 0.0001934 2543.30640 5390.07666
6590.0 0.0001517 2542.55127 7125.25781
7500.0 0.0001333 2541.77124 7992.34668
6858.0 0.0001458 2540.96606 7247.98633
5545.0 0.0001803 2540.13599 5521.58350
4082.0 0.0002450 2539.28076 3959.53491
3213.0 0.0003112 2538.40015 3073.66650
2799.0 0.000357 2537.49438 2732.20410
2673.0 0.000374 2536.56348 2648.88501
2741.0 0.000365 2535.60742 2652.84351
2870.0 0.0003484 2534.62622 2670.11548
2792.0 0.000358 2533.61987 2664.65112
2644.0 0.000378 2532.58838 2631.89844
2620.0 0.000382 2531.53223 2589.77002
2671.0 0.000374 2530.45142 2562.67603
2420.0 0.000413 2529.34570 2550.65771
2475.0 0.000404 2528.21582 2549.91650
2480.0 0.000403 2527.06152 2556.43457
2588.0 0.000386 2525.88354 2564.68408
2553.0 0.000392 2524.68140 2566.70142
2525.0 0.000396 2523.45605 2558.87256
2553.0 0.000392 2522.20728 2547.02148
2572.0 0.000389 2520.93555 2535.19385
2413.0 0.000414 2519.64111 2543.22754
2536.0 0.000394 2518.32422 2578.60962
2537.0 0.000394 2516.98535 2649.92920
2645.0 0.000378 2515.62500 2735.48633
2669.0 0.000375 2514.24316 2777.12109
2708.0 0.000369 2512.84033 2735.95752
2541.0 0.000394 2511.41699 2647.89136
2492.0 0.000401 2509.97363 2571.82275
2457.0 0.000407 2508.51050 2530.97314
2482.0 0.000403 2507.02808 2514.94312
2366.0 0.000423 2505.52686 2509.40283
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3149.0 0.0003176 2263.10840 3056.09204
2906.0 0.0003441 2261.71973 3042.10400
2713.0 0.000369 2260.28516 2767.50537
2455.0 0.000407 2258.80518 2506.65503
2351.0 0.000425 2257.27930 2371.36230
2264.0 0.000442 2255.70801 2327.27344
2245.0 0.000445 2254.09106 2325.43286
2336.0 0.000428 2252.42822 2355.64111
2490.0 0.000402 2250.71997 2430.19580
2654.0 0.000377 2248.96631 2533.30176
2665.0 0.000375 2247.16699 2603.56616
2560.0 0.000391 2245.32275 2646.54004
2825.0 0.000354 2243.43335 2842.19678
3457.0 0.0002893 2241.49878 3317.79126
3828.0 0.0002612 2239.51978 3844.85718
3602.0 0.0002776 2237.49634 3874.81909
3210.0 0.0003115 2235.42871 3364.82739
2762.0 0.000362 2233.31738 2859.56812
2768.0 0.000361 2231.16211 2623.00586
2617.0 0.000382 2228.96362 2562.88745
2498.0 0.000400 2226.72266 2506.20654
2502.0 0.000400 2224.43872 2436.66919
2407.0 0.000415 2222.11279 2415.77124
2457.0 0.000407 2219.74512 2446.42603
2526.0 0.000396 2217.33618 2463.85181
2417.0 0.000414 2214.88672 2424.80151
2419.0 0.000413 2212.39673 2383.72119
2405.0 0.000416 2209.86719 2391.00244
2538.0 0.000394 2207.29834 2430.96753
2444.0 0.000409 2204.69092 2458.07056
2500.0 0.000400 2202.04565 2503.98730
2801.0 0.000357 2199.36304 2674.93579
3145.0 0.0003180 2196.64355 2977.92139
3194.0 0.0003131 2193.88770 3200.94238
2944.0 0.0003397 2191.09717 3077.66748
2812.0 0.000356 2188.27148 2737.74414
2459.0 0.000407 2185.41211 2451.69922
2368.0 0.000422 2182.51953 2303.75854
2328.0 0.000430 2179.59448 2247.76611
2336.0 0.000428 2176.63794 2226.79272
2277.0 0.000439 2173.65063 2216.38477
2307.0 0.000433 2170.63354 2211.16382
2250.0 0.000444 2167.58740 2211.81128
2340.0 0.000427 2164.51318 2225.80835
2328.0 0.000430 2161.41162 2272.17090
2398.0 0.000417 2158.28394 2370.18628
2535.0 0.000394 2155.13062 2508.17017
2728.0 0.000367 2151.95288 2602.77539
2600.0 0.000385 2148.75195 2585.88013
2625.0 0.000381 2145.52856 2556.18750
2866.0 0.0003489 2142.28369 2630.96851
3011.0 0.0003321 2139.01855 2774.95947
3109.0 0.0003216 2135.73413 2811.36450
2630.0 0.000380 2132.43164 2671.62378
2712.0 0.000369 2129.11182 2513.24146
2382.0 0.000420 2125.77563 2448.09668
2576.0 0.000388 2122.42480 2452.78467
2590.0 0.000386 2119.06030 2453.16138
2639.0 0.000379 2115.68311 2472.45679
2817.0 0.000355 2112.29419 2587.35107
3015.0 0.0003317 2108.89478 2774.26978
2952.0 0.0003388 2105.48657 2876.63867
2885.0 0.0003466 2102.06982 2790.33936
2852.0 0.0003506 2098.64697 2669.22729
2858.0 0.0003499 2095.21753 2664.13354
3056.0 0.0003272 2091.78467 2734.53271
2834.0 0.000353 2088.34766 2709.46338
2318.0 0.000431 2084.90942 2547.04907
2439.0 0.000410 2081.47046 2374.99634
2120.0 0.000472 2078.03125 2275.73169
2082.0 0.000480 2074.59424 2236.47461
2125.0 0.000471 2071.16113 2215.67578
2037.0 0.000491 2067.73096 2210.75122
2173.0 0.000460 2064.30713 2235.91724
2229.0 0.000449 2060.88940 2275.16260
2254.0 0.000444 2057.47974 2280.22119
2137.0 0.000468 2054.08032 2229.44580
2128.0 0.000470 2050.69019 2161.45190
2070.0 0.000483 2047.31262 2110.68359
1980.0 0.000505 2043.94763 2083.81494
2015.0 0.000496 2040.59717 2072.47900
1948.0 0.000513 2037.26282 2068.32007
1998.0 0.000501 2033.94446 2067.87476
1890.0 0.000529 2030.64478 2073.85791
2024.0 0.000494 2027.36340 2096.42285
1988.0 0.000503 2024.10352 2158.58691
2135.0 0.000468 2020.86511 2288.14551
2348.0 0.000426 2017.64929 2474.79346
2467.0 0.000405 2014.45813 2642.95825
2588.0 0.000386 2011.29150 2680.69873
2554.0 0.000392 2008.15247 2613.83350
2523.0 0.000396 2005.04077 2586.44800
2651.0 0.000377 2001.95728 2643.61230
2655.0 0.000377 1998.90417 2684.14087
2481.0 0.000403 1995.88281 2591.54956
2277.0 0.000439 1992.89282 2420.32544
2203.0 0.000454 1989.93677 2281.57471
2169.0 0.000461 1987.01440 2209.77124
2062.0 0.000485 1984.12805 2174.40796
2075.0 0.000482 1981.27881 2149.11768
2081.0 0.000481 1978.46619 2141.28955
2098.0 0.000477 1975.69275 2155.09229
1996.0 0.000501 1972.95850 2166.56592
2037.0 0.000491 1970.26526 2145.14624
2130.0 0.0 1967.61340 .
14.0 0.0 1965.00354 .
2123.0 0.0 1962.43750 .
2068.0 0.000484 1959.91528 2030.60974
2068.0 0.000484 1957.43860 2062.65894
2187.0 0.000457 1955.00781 2129.08179
2240.0 0.000446 1952.62329 2216.47070
2314.0 0.000432 1950.28674 2280.39966
2301.0 0.000435 1947.99780 2268.57520
2244.0 0.000446 1945.75842 2192.05908
2101.0 0.000476 1943.56860 2107.53809
2045.0 0.000489 1941.42883 2050.54956
2048.0 0.000488 1939.34009 2027.72058
2020.0 0.000495 1937.30322 2032.11084
2024.0 0.000494 1935.31812 2059.02319
1995.0 0.000501 1933.38586 2111.84204
2151.0 0.000465 1931.50635 2213.19019
2181.0 0.000459 1929.68079 2419.95532
2709.0 0.000369 1927.90967 2819.80127
3533.0 0.0002830 1926.19250 3442.76245
4017.0 0.0002489 1924.53052 4129.56104
4322.0 0.0002314 1922.92358 4508.00146
4380.0 0.0002283 1921.37231 4319.22461
3795.0 0.0002635 1919.87671 3827.36304
3452.0 0.0002897 1918.43689 3412.25635
3095.0 0.0003231 1917.05359 3181.57178
2948.0 0.0003392 1915.72656 3000.27734
2755.0 0.000363 1914.45605 2770.29932
2509.0 0.000399 1913.24219 2550.30322
2509.0 0.000399 1912.08472 2400.29077
2422.0 0.000413 1910.98413 2309.33521
2303.0 0.000434 1909.94031 2227.73950
2191.0 0.000456 1908.95264 2141.81079
2100.0 0.000476 1908.02161 2070.83838
2131.0 0.000469 1907.14685 2033.07520
2177.0 0.000459 1906.32825 2039.89636
2146.0 0.000466 1905.56567 2098.23950
2257.0 0.000443 1904.85864 2205.04736
2389.0 0.000419 1904.20703 2331.56421
2554.0 0.000392 1903.61035 2416.09375
2469.0 0.000405 1903.06848 2400.97485
2516.0 0.000397 1902.58093 2309.46021
2305.0 0.000434 1902.14722 2210.31201
2310.0 0.000433 1901.76672 2140.21094
2263.0 0.000442 1901.43909 2092.88452
2246.0 0.000445 1901.16382 2050.00977
2170.0 0.000461 1900.94019 2010.08887
2010.0 0.000498 1900.76770 1980.75293
1998.0 0.000501 1900.64551 1968.09814
1975.0 0.000506 1900.57300 1975.23669
2018.0 0.000496 1900.54956 2002.71863
2112.0 0.000473 1900.57422 2048.55664
2101.0 0.000476 1900.64624 2099.79321
2200.0 0.000455 1900.76477 2143.98486
2242.0 0.000446 1900.92896 2179.18726
2227.0 0.000449 1901.13806 2223.77808
2280.0 0.000439 1901.39087 2285.83350
2295.0 0.000436 1901.68652 2341.31860
2379.0 0.000420 1902.02405 2351.47583
2216.0 0.000451 1902.40234 2317.45093
2258.0 0.000443 1902.82043 2278.93823
2349.0 0.000426 1903.27722 2270.00806
2230.0 0.000448 1903.77148 2289.50659
2381.0 0.000420 1904.30212 2332.43750
2399.0 0.000417 1904.86804 2409.72070
2534.0 0.000395 1905.46802 2522.76685
2525.0 0.000396 1906.10071 2629.46167
2635.0 0.000380 1906.76514 2666.01660
2520.0 0.000397 1907.45972 2623.92334
2516.0 0.000397 1908.18323 2562.80811
2485.0 0.000402 1908.93457 2520.64038
2454.0 0.000407 1909.71216 2478.40283
2337.0 0.000428 1910.51465 2395.49512
2342.0 0.000427 1911.34119 2276.11475
2212.0 0.000452 1912.18958 2158.09839
2093.0 0.000478 1913.05908 2070.91309
2008.0 0.000498 1913.94800 2024.86145
2105.0 0.000475 1914.85486 2015.08362
2145.0 0.000466 1915.77844 2029.89355
2015.0 0.000496 1916.71704 2053.64233
2089.0 0.000479 1917.66956 2070.20679
2038.0 0.000491 1918.63428 2067.05688
2038.0 0.000491 1919.60950 2047.08240
2001.0 0.000500 1920.59436 2024.45483
2097.0 0.000477 1921.58691 2012.70215
2028.0 0.000493 1922.58606 2020.85510
2010.0 0.000498 1923.58984 2053.29004
2077.0 0.000481 1924.59717 2109.83911
2192.0 0.000456 1925.60669 2182.17285
2198.0 0.000455 1926.61646 2259.32739
2248.0 0.000445 1927.62549 2332.97388
2351.0 0.000425 1928.63196 2412.98193
2546.0 0.000393 1929.63452 2517.23657
2564.0 0.000390 1930.63220 2641.73608
2775.0 0.000360 1931.62305 2762.40625
2863.0 0.0003493 1932.60559 2865.82593
2983.0 0.0003352 1933.57898 2975.91846
3058.0 0.0003270 1934.54138 3100.55762
3183.0 0.0003142 1935.49182 3184.10034
2998.0 0.0003336 1936.42871 3136.09570
2976.0 0.0003360 1937.35059 2936.23975
2873.0 0.0003481 1938.25671 2664.04199
2463.0 0.000406 1939.14526 2409.50757
2391.0 0.000418 1940.01550 2221.43604
2276.0 0.000439 1940.86584 2106.97510
2124.0 0.000471 1941.69507 2048.30713
2164.0 0.000462 1942.50256 2023.89551
2027.0 0.000493 1943.28662 2018.59546
2059.0 0.000486 1944.04675 2025.88928
1982.0 0.000505 1944.78125 2044.52502
1982.0 0.000505 1945.48962 2074.73169
2102.0 0.000476 1946.17090 2118.98267
2085.0 0.000480 1946.82385 2178.18628
2179.0 0.000459 1947.44800 2254.68530
2267.0 0.000441 1948.04211 2350.64917
2381.0 0.000420 1948.60571 2460.21533
2527.0 0.000396 1949.13794 2553.04883
2627.0 0.000381 1949.63818 2586.23022
2543.0 0.000393 1950.10547 2538.13770
2332.0 0.000429 1950.53979 2439.99268
2337.0 0.000428 1950.94019 2348.98413
2336.0 0.000428 1951.30640 2312.00098
2290.0 0.000437 1951.63782 2358.21899
2539.0 0.000394 1951.93408 2489.22803
2744.0 0.000364 1952.19507 2676.50928
2796.0 0.000358 1952.42029 2859.91333
2870.0 0.0003484 1952.60974 2962.23560
2954.0 0.0003385 1952.76318 2933.23389
2895.0 0.0003454 1952.88049 2801.75513
2695.0 0.000371 1952.96179 2644.40186
2667.0 0.000375 1953.00696 2527.64038
2439.0 0.000410 1953.01624 2487.59302
2566.0 0.000390 1952.98962 2531.75244
2641.0 0.000379 1952.92761 2644.56226
2724.0 0.000367 1952.83032 2791.24219
2880.0 0.0003472 1952.69812 2920.34717
2829.0 0.000353 1952.53149 2990.69653
2891.0 0.0003459 1952.33093 3004.58447
2958.0 0.0003381 1952.09705 2993.19604
2869.0 0.0003486 1951.83032 2969.45923
2750.0 0.000364 1951.53149 2916.33569
2824.0 0.000354 1951.20154 2817.56128
2561.0 0.000390 1950.84094 2690.47754
2674.0 0.000374 1950.45081 2569.08838
2521.0 0.000397 1950.03198 2474.43628
2414.0 0.000414 1949.58557 2412.85889
2349.0 0.000426 1949.11279 2382.08203
2378.0 0.000421 1948.61438 2376.08008
2381.0 0.000420 1948.09192 2385.89233
2307.0 0.000433 1947.54651 2392.84937
2336.0 0.000428 1946.97961 2382.26294
2279.0 0.000439 1946.39270 2354.55420
2351.0 0.000425 1945.78687 2320.45996
2271.0 0.000440 1945.16394 2284.03882
2227.0 0.000449 1944.52539 2243.65918
2098.0 0.000477 1943.87292 2196.63208
2091.0 0.000478 1943.20813 2146.97607
2184.0 0.000458 1942.53271 2102.12427
1956.0 0.000511 1941.84851 2068.14478
1928.0 0.000519 1941.15759 2048.98120
1977.0 0.000506 1940.46130 2047.23364
1997.0 0.000501 1939.76208 2066.35107
2174.0 0.000460 1939.06165 2112.20117
2193.0 0.000456 1938.36206 2189.66504
2265.0 0.000442 1937.66553 2303.75171
2443.0 0.000409 1936.97375 2451.62085
2723.0 0.000367 1936.28918 2621.19751
2746.0 0.000364 1935.61365 2787.25830
2935.0 0.0003407 1934.94971 2919.49585
3020.0 0.0003311 1934.29944 3004.01074
3219.0 0.0003107 1933.66492 3052.22095
3107.0 0.0003219 1933.04846 3077.12549
3069.0 0.0003258 1932.45227 3071.61768
3089.0 0.0003237 1931.87866 3017.84912
3108.0 0.0003218 1931.32996 2914.41870
2952.0 0.0003388 1930.80823 2786.47949
2809.0 0.000356 1930.31592 2656.87476
2639.0 0.000379 1929.85535 2535.22314
2552.0 0.000392 1929.42859 2423.40210
2430.0 0.000412 1929.03796 2326.03687
2372.0 0.000422 1928.68579 2252.57983
2359.0 0.000424 1928.37402 2211.41528
2164.0 0.000462 1928.10522 2207.23071
2230.0 0.000448 1927.88110 2237.52710
2327.0 0.000430 1927.70410 2293.83643
2410.0 0.000415 1927.57617 2357.28833
2440.0 0.000410 1927.49939 2403.38647
2447.0 0.000409 1927.47571 2411.15894
2365.0 0.000423 1927.50708 2374.95728
2256.0 0.000443 1927.59534 2310.23779
2251.0 0.000444 1927.74231 2237.34766
2207.0 0.000453 1927.94971 2170.64844
2154.0 0.000464 1928.21924 2121.26733
2136.0 0.000468 1928.55249 2095.05371
2060.0 0.000485 1928.95093 2095.69116
2185.0 0.000458 1929.41614 2125.95874
2170.0 0.000461 1929.94910 2187.04956
2172.0 0.000460 1930.55115 2277.09204
2386.0 0.000419 1931.22363 2388.27393
2452.0 0.000408 1931.96729 2505.46289
2606.0 0.000384 1932.78296 2607.96045
2472.0 0.000405 1933.67175 2674.29346
2759.0 0.000362 1934.63391 2699.18311
2644.0 0.000378 1935.67041 2698.80786
2741.0 0.000365 1936.78125 2695.67676
2769.0 0.000361 1937.96655 2706.30713
2711.0 0.000369 1939.22681 2736.43018
2630.0 0.000380 1940.56165 2784.54175
2791.0 0.000358 1941.97107 2842.37158
2736.0 0.000365 1943.45447 2891.12769
2676.0 0.000374 1945.01135 2904.91577
2586.0 0.000387 1946.64148 2866.59302
2770.0 0.000361 1948.34326 2784.45166
2618.0 0.000382 1950.11621 2688.56689
2552.0 0.000392 1951.95862 2612.49951
2646.0 0.000378 1953.86938 2579.61450
2599.0 0.000385 1955.84705 2598.96851
2618.0 0.000382 1957.88940 2663.06958
2786.0 0.000359 1959.99512 2749.64307
2862.0 0.0003494 1962.16125 2826.65698
2832.0 0.000353 1964.38574 2862.20068
2901.0 0.0003447 1966.66650 2841.29858
2930.0 0.0003413 1969.00037 2775.41040
2843.0 0.000352 1971.38403 2686.33472
2740.0 0.000365 1973.81531 2594.49487
2670.0 0.000375 1976.29004 2510.39233
2378.0 0.000421 1978.80566 2442.09619
2511.0 0.000398 1981.35742 2390.28198
2285.0 0.000438 1983.94153 2351.91382
2431.0 0.000411 1986.55481 2320.84985
2223.0 0.000450 1989.19202 2290.91040
2301.0 0.000435 1991.84973 2261.79004
2313.0 0.000432 1994.52209 2237.15210
2299.0 0.000435 1997.20483 2222.56104
2267.0 0.000441 1999.89380 2222.72900
2286.0 0.000437 2002.58276 2238.09692
2314.0 0.000432 2005.26733 2266.82397
2348.0 0.000426 2007.94141 2303.03687
2377.0 0.000421 2010.59973 2338.32324
2346.0 0.000426 2013.23743 2364.32202
2328.0 0.000430 2015.84778 2375.79468
2310.0 0.000433 2018.42468 2376.83765
2422.0 0.000413 2020.96387 2375.39868
2454.0 0.000407 2023.45776 2380.85449
2333.0 0.000429 2025.90161 2401.03979
2434.0 0.000411 2028.28857 2441.93408
2413.0 0.000414 2030.61230 2507.40259
2556.0 0.000391 2032.86829 2598.28955
2716.0 0.000368 2035.04907 2710.97192
2905.0 0.0003442 2037.14954 2837.83032
2953.0 0.0003386 2039.16357 2968.66626
3086.0 0.0003240 2041.08521 3092.21631
3279.0 0.0003050 2042.90967 3193.24390
3229.0 0.0003097 2044.63086 3252.05737
3207.0 0.0003118 2046.24414 3252.41602
3208.0 0.0003117 2047.74390 3193.29688
3184.0 0.0003141 2049.12598 3094.39282
3021.0 0.0003310 2050.38599 2983.97852
2970.0 0.0003367 2051.51953 2886.83618
2917.0 0.0003428 2052.52368 2818.03247
2729.0 0.000366 2053.39453 2783.33472
2682.0 0.000373 2054.12988 2777.31128
2807.0 0.000356 2054.72778 2786.45435
2817.0 0.000355 2055.18628 2792.46655
2763.0 0.000362 2055.50464 2778.96265
2621.0 0.000382 2055.68286 2739.93237
2628.0 0.000381 2055.72119 2679.18677
2534.0 0.000395 2055.62134 2605.57739
2433.0 0.000411 2055.38574 2526.88477
2382.0 0.000420 2055.01733 2451.50098
2405.0 0.000416 2054.52051 2384.40088
2335.0 0.000428 2053.90112 2329.83594
2234.0 0.000448 2053.16528 2291.07593
2244.0 0.000446 2052.32129 2269.16211
2290.0 0.000437 2051.37817 2263.49268
2214.0 0.000452 2050.34692 2272.08423
2293.0 0.000436 2049.23975 2291.86597
2237.0 0.000447 2048.07056 2318.87524
2285.0 0.000438 2046.85535 2347.99097
2294.0 0.000436 2045.61145 2377.38892
2320.0 0.000431 2044.35828 2404.13159
2450.0 0.000408 2043.11768 2428.39990
2518.0 0.000397 2041.91394 2450.45239
2409.0 0.000415 2040.77234 2470.08472
2458.0 0.000407 2039.72229 2488.22314
2458.0 0.000407 2038.79456 2508.03784
2604.0 0.000384 2038.02356 2531.10083
2548.0 0.000392 2037.44617 2560.98901
2506.0 0.000399 2037.10205 2597.84229
2771.0 0.000361 2037.03467 2640.23730
2622.0 0.000381 2037.29028 2685.54175
2805.0 0.000357 2037.91919 2728.48291
2958.0 0.0003381 2038.97498 2763.59912
2810.0 0.000356 2040.51550 2784.13135
2875.0 0.0003478 2042.60217 2785.94678
2886.0 0.0003465 2045.30176 2771.34326
2760.0 0.000362 2048.68384 2747.88110
2861.0 0.0003495 2052.82373 2724.48462
2879.0 0.0003473 2057.80347 2708.67993
2892.0 0.0003458 2063.70532 2704.41675
2735.0 0.000366 2070.62231 2712.35962
2629.0 0.000380 2078.64893 2729.90039
2774.0 0.000360 2087.88794 2751.14331
2784.0 0.000359 2098.44995 2767.80859
2787.0 0.000359 2110.44604 2773.11914
2673.0 0.000374 2123.99561 2763.66528
2657.0 0.000376 2139.23560 2740.85938
2522.0 0.000397 2156.29248 2708.37622
0.0 . . .
_pd_meas_number_of_points        1140
_pd_proc_number_of_points        1140

_reflns_number_total             310
_reflns_limit_h_min              1
_reflns_limit_h_max              14
_reflns_limit_k_min              0
_reflns_limit_k_max              9
_reflns_limit_l_min              0
_reflns_limit_l_max              8
_reflns_d_resolution_high        1.396
_reflns_d_resolution_low         18.776
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1P5CO2_1_publ
_database_code_depnum_ccdc_archive 'CCDC 1582002'
_audit_update_record             
;
2017-10-25 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;

_pd_block_id                     2016-03-03T18:49|1P5CO2_1|wendy|bt1

_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_creation_date             2016-03-03T18:49

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details          
; ?
;
_pd_proc_ls_special_details      
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_ls_weighting_scheme      ?
_refine_ls_weighting_details     ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     ?
_refine_ls_extinction_coef       ?
_refine_ls_number_constraints    ?

_refine_ls_restrained_S_all      ?
_refine_ls_restrained_S_obs      ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate               ?
_pd_prep_pressure                ?
_pd_prep_temperature             ?

_pd_char_colour                  ? # use ICDD colour descriptions
_refine_ls_shift/su_max          0.06
_refine_ls_shift/su_mean         0.01
_computing_structure_refinement  GSAS
_refine_ls_number_parameters     47
_refine_ls_goodness_of_fit_all   1.18
_refine_ls_number_restraints     17
_refine_ls_matrix_type           full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology     ?

_chemical_name_systematic        
; ?
;
_chemical_name_common            ?
_chemical_formula_moiety         ?
_chemical_formula_structural     ?
_chemical_formula_analytical     ?
_chemical_melting_point          ?
_chemical_compound_source        ? # for minerals and
# natural products
_symmetry_space_group_name_Hall  ?

_exptl_crystal_F_000             ?
_exptl_crystal_density_diffrn    ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?

_cell_measurement_temperature    10

_cell_special_details            
; ?
;

_geom_special_details            ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution    ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                   
'from Z:/queen/Desktop/MBTT series_CO2/CuBTT/Copy of 1.5 CO2_finali'
_cell_length_a                   18.68163(34)
_cell_length_b                   18.68163
_cell_length_c                   18.68163
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_volume                     6520.0(4)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_H-M   'P m -3 m'
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 +z,+x,+y
3 +y,+z,+x
4 +x,+y,-z
5 -z,+x,+y
6 +y,-z,+x
7 -z,+x,-y
8 -y,-z,+x
9 +y,-z,-x
10 -x,+y,-z
11 -z,-x,+y
12 +x,-y,-z
13 +y,+x,+z
14 +z,+y,+x
15 +x,+z,+y
16 +y,+x,-z
17 -z,+y,+x
18 +x,-z,+y
19 -z,+y,-x
20 -x,-z,+y
21 +x,-z,-y
22 -y,+x,-z
23 -z,-y,+x
24 +y,-x,-z
-1 -x,-y,-z
-2 -z,-x,-y
-3 -y,-z,-x
-4 -x,-y,+z
-5 +z,-x,-y
-6 -y,+z,-x
-7 +z,-x,+y
-8 +y,+z,-x
-9 -y,+z,+x
-10 +x,-y,+z
-11 +z,+x,-y
-12 -x,+y,+z
-13 -y,-x,-z
-14 -z,-y,-x
-15 -x,-z,-y
-16 -y,-x,+z
-17 +z,-y,-x
-18 -x,+z,-y
-19 +z,-y,+x
-20 +x,+z,-y
-21 -x,+z,+y
-22 +y,-x,+z
-23 +z,+y,-x
-24 -y,+x,+z

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Cr Cr1 0.1311(10) 0.5 0.0 1.0 Uiso 0.00372 12
C C1 0.14880(33) 0.3368(4) -0.14880(33) 1.0 Uiso 0.0111(9) 24
C C2 0.17778(32) 0.2690(4) -0.17778(32) 1.0 Uiso 0.0111(9) 24
C C3 0.24100(30) 0.24100(30) -0.1460(5) 1.0 Uiso 0.0111(9) 24
Cl Cl1 0.0 0.5 0.0 1.0 Uiso 0.112(10) 3
N N1 0.13061(23) 0.42228(23) -0.07883(23) 1.0 Uiso 0.0122(5) 48
N N2 0.17480(24) 0.36944(23) -0.09048(22) 1.0 Uiso 0.0122(5) 48
H H1 0.2610(6) 0.2610(6) -0.1040(7) 1.0 Uiso 0.010(4) 24
C C1a 0.2907(9) 0.4397(5) 0.0 0.386(6) Uiso 0.10145 24
O O1a 0.2724(10) 0.5 0.0 0.773(11) Uiso 0.065 12
O O1b 0.3097(16) 0.3808(9) 0.0 0.386(6) Uiso 0.10486 24
C C4a 0.1143(35) 0.0641(9) 0.0641(9) 0.133(5) Uiso 0.10621 24
O O4a 0.071(4) 0.0336(34) 0.0336(34) 0.133(5) Uiso 0.10621 24
O O4b 0.158(4) 0.0945(29) 0.0945(29) 0.133(5) Uiso 0.10621 24
C C2a 0.0 0.2772(16) 0.0310(10) 0.187(4) Uiso 0.03831 24
O O2b 0.0 0.2239(16) 0.0617(24) 0.187(4) Uiso 0.05208 24
O O2a 0.0 0.3301(18) 0.0 0.749(16) Uiso 0.06768 6
C C3a 0.1656(7) 0.1656(7) 0.0 0.501(12) Uiso 0.0634 12
O O3a 0.1107(12) 0.1934(20) 0.0 0.250(6) Uiso 0.0634 24
O O3b 0.2199(13) 0.1372(20) 0.0 0.250(6) Uiso 0.0634 24
O Os 0.2289(13) 0.5 0.0 0.2353 Uiso 0.00351 12

# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum            'C31.66 H8 Cl Cr4 N32 O16.26'
_chemical_formula_weight         1340.08
_cell_formula_units_Z            3

# MOLECULAR GEOMETRY

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cr1 Cr1 4.90(4) . 10_555 N
Cr1 Cr1 3.465(27) . 14_555 N
Cr1 Cr1 3.465(27) . 19_555 N
Cr1 Cl1 2.450(19) . 1_555 N
Cr1 N1 2.068(4) . 1_555 N
Cr1 N1 2.068(4) . 4_555 N
Cr1 N1 2.068(4) . 12_565 N
Cr1 N1 3.003(7) . 17_555 N
Cr1 N1 3.003(7) . 19_555 N
Cr1 N1 3.003(7) . 23_565 N
Cr1 N1 2.068(4) . -10_565 N
Cr1 N1 3.003(7) . -14_565 N
Cr1 N2 3.078(6) . 1_555 N
Cr1 N2 3.078(6) . 4_555 N
Cr1 N2 3.078(6) . 12_565 N
Cr1 N2 3.078(6) . -10_565 N
Cr1 C1a 3.187(20) . 1_555 N
Cr1 C1a 3.187(20) . 12_565 N
Cr1 O1a 2.639(14) . 1_555 N
Cr1 O1b 4.011(27) . 1_555 N
Cr1 O1b 4.011(27) . 12_565 N
Cr1 O2a 4.010(30) . 1_555 N
Cr1 O2a 4.010(30) . 12_565 N
Cr1 Os 1.826(16) . 1_555 N
C1 C2 1.480(11) . 1_555 N
C1 C3 2.484(6) . 1_555 N
C1 C3 2.484(6) . 7_555 N
C1 N1 2.092(7) . 1_555 N
C1 N1 2.092(7) . 19_555 N
C1 N2 1.340(6) . 1_555 N
C1 N2 1.340(6) . 19_555 N
C2 C1 1.480(11) . 1_555 N
C2 C2 2.409(14) . 7_555 N
C2 C2 2.409(14) . 9_555 N
C2 C3 1.421(6) . 1_555 N
C2 C3 1.421(6) . 7_555 N
C2 C3 2.840(11) . 9_555 N
C2 N2 2.487(8) . 1_555 N
C2 N2 2.487(8) . 19_555 N
C3 C1 2.484(6) . 1_555 N
C3 C1 2.484(6) . 9_555 N
C3 C2 1.421(6) . 1_555 N
C3 C2 2.840(11) . 7_555 N
C3 C2 1.421(6) . 9_555 N
C3 C3 2.510(15) . 7_555 N
C3 C3 2.510(15) . 9_555 N
C3 N2 2.892(6) . 1_555 N
C3 N2 2.892(6) . 13_555 N
C3 H1 0.946(19) . 1_555 N
Cl1 Cr1 2.450(19) . 1_555 N
Cl1 Cr1 2.450(19) . 10_555 N
Cl1 Cr1 2.450(19) . 14_555 N
Cl1 Cr1 2.450(19) . 19_555 N
Cl1 N1 3.199(4) . 1_555 N
Cl1 N1 3.199(4) . 4_555 N
Cl1 N1 3.199(4) . 10_555 N
Cl1 N1 3.199(4) . 12_565 N
Cl1 N1 3.199(4) . 14_555 N
Cl1 N1 3.199(4) . 17_555 N
Cl1 N1 3.199(4) . 19_555 N
Cl1 N1 3.199(4) . 23_565 N
Cl1 N1 3.199(4) . -1_565 N
Cl1 N1 3.199(4) . -4_565 N
Cl1 N1 3.199(4) . -10_565 N
Cl1 N1 3.199(4) . -12_555 N
Cl1 N1 3.199(4) . -14_565 N
Cl1 N1 3.199(4) . -17_565 N
Cl1 N1 3.199(4) . -19_565 N
Cl1 N1 3.199(4) . -23_555 N
Cl1 O2a 3.174(34) . 1_555 N
Cl1 O2a 3.174(34) . 12_565 N
N1 Cr1 2.068(4) . 1_555 N
N1 Cr1 3.003(7) . 19_555 N
N1 C1 2.092(7) . 1_555 N
N1 Cl1 3.199(4) . 1_555 N
N1 N1 2.945(9) . 4_555 N
N1 N1 1.368(9) . 19_555 N
N1 N1 2.904(9) . -10_565 N
N1 N2 1.305(6) . 1_555 N
N1 N2 2.180(5) . 19_555 N
N1 Os 2.765(17) . 1_555 N
N2 Cr1 3.078(6) . 1_555 N
N2 C1 1.340(6) . 1_555 N
N2 C2 2.487(8) . 1_555 N
N2 C3 2.892(6) . 1_555 N
N2 N1 1.305(6) . 1_555 N
N2 N1 2.180(5) . 19_555 N
N2 N2 2.228(8) . 19_555 N
H1 C3 0.946(19) . 1_555 N
C1a Cr1 3.187(20) . 1_555 N
C1a C1a 2.254(20) . 12_565 N
C1a O1a 1.178(8) . 1_555 N
C1a O1b 1.156(8) . 1_555 N
C1a O1b 2.953(27) . 13_555 N
C1a Os 1.614(19) . 1_555 N
O1a Cr1 2.639(14) . 1_555 N
O1a C1a 1.178(8) . 1_555 N
O1a C1a 1.178(8) . 12_565 N
O1a O1b 2.334(11) . 1_555 N
O1a O1b 2.334(11) . 12_565 N
O1a Os 0.814(21) . 1_555 N
O1b Cr1 4.011(27) . 1_555 N
O1b C1a 1.156(8) . 1_555 N
O1b C1a 2.953(27) . 13_555 N
O1b O1a 2.334(11) . 1_555 N
O1b Os 2.691(19) . 1_555 N
C4a C4a 1.33(10) . 2_555 N
C4a C4a 1.33(10) . 3_555 N
C4a C4a 2.394(34) . 4_555 N
C4a C4a 2.74(4) . 6_555 N
C4a C4a 2.74(4) . 16_555 N
C4a C4a 2.394(34) . 18_555 N
C4a O4a 1.149(8) . 1_555 N
C4a O4a 1.62(8) . 2_555 N
C4a O4a 1.62(8) . 3_555 N
C4a O4a 2.08(8) . 4_555 N
C4a O4a 2.82(10) . 5_555 N
C4a O4a 2.37(5) . 6_555 N
C4a O4a 2.71(12) . 12_555 N
C4a O4a 2.37(5) . 16_555 N
C4a O4a 2.82(10) . 17_555 N
C4a O4a 2.08(8) . 18_555 N
C4a O4a 2.99(9) . -7_555 N
C4a O4a 2.99(9) . -8_555 N
C4a O4b 1.151(8) . 1_555 N
C4a O4b 1.89(8) . 2_555 N
C4a O4b 1.89(8) . 3_555 N
C4a O2b 2.37(6) . 3_555 N
C4a O2b 2.37(6) . 13_555 N
C4a C3a 2.438(27) . 1_555 N
C4a C3a 2.438(27) . 3_555 N
C4a O3a 2.696(34) . 1_555 N
C4a O3a 2.09(6) . 3_555 N
C4a O3a 2.09(6) . 13_555 N
C4a O3a 2.696(34) . 15_555 N
C4a O3b 2.68(6) . 1_555 N
C4a O3b 2.68(6) . 15_555 N
O4a C4a 1.149(8) . 1_555 N
O4a C4a 1.62(8) . 2_555 N
O4a C4a 1.62(8) . 3_555 N
O4a C4a 2.08(8) . 4_555 N
O4a C4a 2.99(9) . 5_555 N
O4a C4a 2.37(5) . 6_555 N
O4a C4a 2.71(12) . 12_555 N
O4a C4a 2.37(5) . 16_555 N
O4a C4a 2.99(9) . 17_555 N
O4a C4a 2.08(8) . 18_555 N
O4a C4a 2.82(10) . -7_555 N
O4a C4a 2.82(10) . -8_555 N
O4a O4a 0.98(17) . 2_555 N
O4a O4a 0.98(17) . 3_555 N
O4a O4a 1.25(13) . 4_555 N
O4a O4a 2.06(7) . 5_555 N
O4a O4a 1.59(4) . 6_555 N
O4a O4a 2.41(7) . 7_555 N
O4a O4a 2.41(7) . 8_555 N
O4a O4a 2.41(7) . 9_555 N
O4a O4a 2.92(9) . 10_555 N
O4a O4a 2.75(7) . 11_555 N
O4a O4a 1.77(18) . 12_555 N
O4a O4a 1.59(4) . 16_555 N
O4a O4a 2.06(7) . 17_555 N
O4a O4a 1.25(13) . 18_555 N
O4a O4a 2.75(7) . 19_555 N
O4a O4a 2.92(9) . 20_555 N
O4a O4a 2.41(7) . 24_555 N
O4a O4a 2.06(7) . -7_555 N
O4a O4a 2.06(7) . -8_555 N
O4a O4a 2.64(14) . -12_555 N
O4a O4b 2.299(12) . 1_555 N
O4a O4b 2.63(5) . 2_555 N
O4a O4b 2.63(5) . 3_555 N
O4a O2b 2.98(7) . 3_555 N
O4a O2b 2.98(7) . 13_555 N
O4a O3a 2.78(6) . 3_555 N
O4a O3a 2.78(6) . 13_555 N
O4b C4a 1.151(8) . 1_555 N
O4b C4a 1.89(8) . 2_555 N
O4b C4a 1.89(8) . 3_555 N
O4b O4a 2.299(12) . 1_555 N
O4b O4a 2.63(5) . 2_555 N
O4b O4a 2.63(5) . 3_555 N
O4b O4b 1.69(16) . 2_555 N
O4b O4b 1.69(16) . 3_555 N
O4b O2b 2.23(9) . 3_555 N
O4b O2b 2.23(9) . 13_555 N
O4b C3a 2.213(17) . 1_555 N
O4b C3a 2.213(17) . 3_555 N
O4b O3a 2.706(30) . 1_555 N
O4b O3a 1.91(6) . 3_555 N
O4b O3a 1.91(6) . 13_555 N
O4b O3a 2.706(30) . 15_555 N
O4b O3b 2.25(6) . 1_555 N
O4b O3b 2.959(24) . 3_555 N
O4b O3b 2.959(24) . 13_555 N
O4b O3b 2.25(6) . 15_555 N
C2a C2a 1.16(4) . 4_555 N
C2a C2a 0.818(28) . 14_555 N
C2a C2a 0.818(28) . 17_555 N
C2a O2b 1.149(8) . 1_555 N
C2a O2b 2.00(5) . 4_555 N
C2a O2b 1.629(29) . 14_555 N
C2a O2b 1.629(29) . 17_555 N
C2a O2a 1.145(8) . 1_555 N
C2a O3a 2.658(20) . 1_555 N
C2a O3a 2.658(20) . 10_555 N
C2a O3a 2.162(31) . 14_555 N
C2a O3b 2.256(31) . 2_555 N
C2a O3b 2.838(29) . 13_555 N
C2a O3b 2.838(29) . 22_555 N
O2b C4a 2.37(6) . 2_555 N
O2b C4a 2.37(6) . 5_555 N
O2b O4a 2.98(7) . 2_555 N
O2b O4a 2.98(7) . 5_555 N
O2b O4b 2.23(9) . 2_555 N
O2b O4b 2.23(9) . 5_555 N
O2b C2a 1.149(8) . 1_555 N
O2b C2a 2.00(5) . 4_555 N
O2b C2a 1.629(29) . 14_555 N
O2b C2a 1.629(29) . 17_555 N
O2b O2b 2.30(9) . 4_555 N
O2b O2b 1.63(6) . 14_555 N
O2b O2b 1.63(6) . 17_555 N
O2b O2a 2.294(12) . 1_555 N
O2b C3a 2.23(4) . 2_555 N
O2b O3a 2.435(25) . 1_555 N
O2b O3a 2.435(25) . 10_555 N
O2b O3a 1.08(4) . 14_555 N
O2b O3b 1.41(5) . 2_555 N
O2b O3b 2.81(4) . 13_555 N
O2b O3b 2.81(4) . 22_555 N
O2a Cr1 4.010(30) . 1_555 N
O2a Cr1 4.010(30) . 10_555 N
O2a Cr1 4.010(30) . 14_555 N
O2a Cr1 4.010(30) . 19_555 N
O2a Cl1 3.174(34) . 1_555 N
O2a C2a 1.145(8) . 1_555 N
O2a C2a 1.145(8) . 4_555 N
O2a C2a 1.145(8) . 14_555 N
O2a C2a 1.145(8) . 17_555 N
O2a O2b 2.294(12) . 1_555 N
O2a O2b 2.294(12) . 4_555 N
O2a O2b 2.294(12) . 14_555 N
O2a O2b 2.294(12) . 17_555 N
C3a C4a 2.438(27) . 1_555 N
C3a C4a 2.438(27) . 2_555 N
C3a C4a 2.438(27) . 4_555 N
C3a C4a 2.438(27) . 16_555 N
C3a O4b 2.213(17) . 1_555 N
C3a O4b 2.213(17) . 2_555 N
C3a O4b 2.213(17) . 4_555 N
C3a O4b 2.213(17) . 16_555 N
C3a O2b 2.23(4) . 3_555 N
C3a O2b 2.23(4) . 14_555 N
C3a O3a 1.149(8) . 1_555 N
C3a O3a 1.149(8) . 13_555 N
C3a O3b 1.144(8) . 1_555 N
C3a O3b 1.144(8) . 13_555 N
O3a C4a 2.696(34) . 1_555 N
O3a C4a 2.09(6) . 2_555 N
O3a C4a 2.696(34) . 4_555 N
O3a C4a 2.09(6) . 16_555 N
O3a O4a 2.78(6) . 2_555 N
O3a O4a 2.78(6) . 16_555 N
O3a O4b 2.706(30) . 1_555 N
O3a O4b 1.91(6) . 2_555 N
O3a O4b 2.706(30) . 4_555 N
O3a O4b 1.91(6) . 16_555 N
O3a C2a 2.658(20) . 1_555 N
O3a C2a 2.658(20) . 4_555 N
O3a C2a 2.162(31) . 14_555 N
O3a O2b 2.435(25) . 1_555 N
O3a O2b 2.435(25) . 4_555 N
O3a O2b 1.08(4) . 14_555 N
O3a C3a 1.149(8) . 1_555 N
O3a O3a 2.184(30) . 13_555 N
O3a O3a 2.925(33) . 14_555 N
O3a O3a 2.925(33) . 19_555 N
O3a O3b 2.293(12) . 1_555 N
O3a O3b 0.70(7) . 13_555 N
O3b C4a 2.68(6) . 1_555 N
O3b C4a 2.68(6) . 4_555 N
O3b O4b 2.25(6) . 1_555 N
O3b O4b 2.959(24) . 2_555 N
O3b O4b 2.25(6) . 4_555 N
O3b O4b 2.959(24) . 16_555 N
O3b C2a 2.256(31) . 3_555 N
O3b C2a 2.838(29) . 13_555 N
O3b C2a 2.838(29) . 16_555 N
O3b O2b 1.41(5) . 3_555 N
O3b O2b 2.81(4) . 13_555 N
O3b O2b 2.81(4) . 16_555 N
O3b C3a 1.144(8) . 1_555 N
O3b O3a 2.293(12) . 1_555 N
O3b O3a 0.70(7) . 13_555 N
O3b O3b 2.183(29) . 13_555 N
Os Cr1 1.826(16) . 1_555 N
Os N1 2.765(17) . 1_555 N
Os N1 2.765(17) . 4_555 N
Os N1 2.765(17) . 12_565 N
Os N1 2.765(17) . -10_565 N
Os C1a 1.614(19) . 1_555 N
Os C1a 1.614(19) . 12_565 N
Os O1a 0.814(21) . 1_555 N
Os O1b 2.691(19) . 1_555 N
Os O1b 2.691(19) . 12_565 N

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Cr1 N1 89.7(6) 1_555 . 1_555 N
Cl1 Cr1 N1 89.7(6) 1_555 . 4_555 N
Cl1 Cr1 N1 89.7(6) 1_555 . 12_565 N
Cl1 Cr1 N1 89.7(6) 1_555 . -10_565 N
Cl1 Cr1 Os 180.0 1_555 . 1_555 N
N1 Cr1 N1 90.81(26) 1_555 . 4_555 N
N1 Cr1 N1 180.000(11) 1_555 . 12_565 N
N1 Cr1 N1 89.19(26) 1_555 . -10_565 N
N1 Cr1 Os 90.3(6) 1_555 . 1_555 N
N1 Cr1 N1 89.19(26) 4_555 . 12_565 N
N1 Cr1 N1 180.000(11) 4_555 . -10_565 N
N1 Cr1 Os 90.3(6) 4_555 . 1_555 N
N1 Cr1 N1 90.81(26) 12_565 . -10_565 N
N1 Cr1 Os 90.3(6) 12_565 . 1_555 N
N1 Cr1 Os 90.3(6) -10_565 . 1_555 N
C2 C1 N2 123.7(4) 1_555 . 1_555 N
C2 C1 N2 123.7(4) 1_555 . 19_555 N
N2 C1 N2 112.5(7) 1_555 . 19_555 N
C1 C2 C3 117.8(4) 1_555 . 1_555 N
C1 C2 C3 117.8(4) 1_555 . 7_555 N
C3 C2 C3 124.0(9) 1_555 . 7_555 N
C2 C3 C2 115.9(9) 1_555 . 9_555 N
C2 C3 H1 122.0(4) 1_555 . 1_555 N
C2 C3 H1 122.0(4) 9_555 . 1_555 N
Cr1 Cl1 Cr1 180.0 1_555 . 10_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 1_555 . 19_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 14_555 N
Cr1 Cl1 Cr1 90.0 10_555 . 19_555 N
Cr1 Cl1 Cr1 180.0 14_555 . 19_555 N
Cr1 N1 N1 120.5(5) 1_555 . 19_555 N
Cr1 N1 N2 130.3(6) 1_555 . 1_555 N
N1 N1 N2 109.23(27) 19_555 . 1_555 N
C1 N2 N1 104.5(5) 1_555 . 1_555 N
O1a C1a O1b 179.0(11) 1_555 . 1_555 N
O1a C1a Os 28.8(7) 1_555 . 1_555 N
O1b C1a Os 152.2(12) 1_555 . 1_555 N
C1a O1a C1a 146.2(22) 1_555 . 12_565 N
C1a O1a Os 106.9(11) 1_555 . 1_555 N
C1a O1a Os 106.9(11) 12_565 . 1_555 N
C4a C4a C4a 60.0000(4) 2_555 . 3_555 N
C4a C4a O4a 81(5) 2_555 . 1_555 N
C4a C4a O4a 44.6(24) 2_555 . 2_555 N
C4a C4a O4a 65.8(18) 2_555 . 3_555 N
C4a C4a O4b 99(4) 2_555 . 1_555 N
C4a C4a O4a 81(5) 3_555 . 1_555 N
C4a C4a O4a 65.8(18) 3_555 . 2_555 N
C4a C4a O4a 44.6(24) 3_555 . 3_555 N
C4a C4a O4b 99(4) 3_555 . 1_555 N
O4a C4a O4a 37(6) 1_555 . 2_555 N
O4a C4a O4a 37(6) 1_555 . 3_555 N
O4a C4a O4b 180.000(34) 1_555 . 1_555 N
O4a C4a O4a 35(5) 2_555 . 3_555 N
O4a C4a O4b 144(6) 2_555 . 1_555 N
O4a C4a O4b 144(6) 3_555 . 1_555 N
C4a O4a C4a 54(5) 1_555 . 2_555 N
C4a O4a C4a 54(5) 1_555 . 3_555 N
C4a O4a O4a 99(5) 1_555 . 2_555 N
C4a O4a O4a 99(5) 1_555 . 3_555 N
C4a O4a O4a 119.8(33) 1_555 . 4_555 N
C4a O4a O4a 119.0(24) 1_555 . 6_555 N
C4a O4a O4a 135(6) 1_555 . 12_555 N
C4a O4a O4a 119.0(24) 1_555 . 16_555 N
C4a O4a O4a 119.8(33) 1_555 . 18_555 N
C4a O4a C4a 48(4) 2_555 . 3_555 N
C4a O4a O4a 44.6(24) 2_555 . 2_555 N
C4a O4a O4a 72.4(25) 2_555 . 3_555 N
C4a O4a O4a 110.6(18) 2_555 . 4_555 N
C4a O4a O4a 123(10) 2_555 . 6_555 N
C4a O4a O4a 155.4(18) 2_555 . 12_555 N
C4a O4a O4a 81(6) 2_555 . 16_555 N
C4a O4a O4a 158.9(19) 2_555 . 18_555 N
C4a O4a O4a 72.4(25) 3_555 . 2_555 N
C4a O4a O4a 44.6(24) 3_555 . 3_555 N
C4a O4a O4a 158.9(19) 3_555 . 4_555 N
C4a O4a O4a 81(6) 3_555 . 6_555 N
C4a O4a O4a 155.4(18) 3_555 . 12_555 N
C4a O4a O4a 123(10) 3_555 . 16_555 N
C4a O4a O4a 110.6(18) 3_555 . 18_555 N
O4a O4a O4a 60.0000(4) 2_555 . 3_555 N
O4a O4a O4a 90.0 2_555 . 4_555 N
O4a O4a O4a 105(7) 2_555 . 6_555 N
O4a O4a O4a 120.0000(4) 2_555 . 12_555 N
O4a O4a O4a 52(8) 2_555 . 16_555 N
O4a O4a O4a 135.0 2_555 . 18_555 N
O4a O4a O4a 135.0000(7) 3_555 . 4_555 N
O4a O4a O4a 52(8) 3_555 . 6_555 N
O4a O4a O4a 120.0000(9) 3_555 . 12_555 N
O4a O4a O4a 105(7) 3_555 . 16_555 N
O4a O4a O4a 90.0 3_555 . 18_555 N
O4a O4a O4a 116(5) 4_555 . 6_555 N
O4a O4a O4a 45.0000(7) 4_555 . 12_555 N
O4a O4a O4a 38(8) 4_555 . 16_555 N
O4a O4a O4a 90.0 4_555 . 18_555 N
O4a O4a O4a 75(7) 6_555 . 12_555 N
O4a O4a O4a 119.8(12) 6_555 . 16_555 N
O4a O4a O4a 38(8) 6_555 . 18_555 N
O4a O4a O4a 75(7) 12_555 . 16_555 N
O4a O4a O4a 45.0000(7) 12_555 . 18_555 N
O4a O4a O4a 116(5) 16_555 . 18_555 N
C4a O4b O4b 81(4) 1_555 . 2_555 N
C4a O4b O4b 81(4) 1_555 . 3_555 N
O4b O4b O4b 60.0000(4) 2_555 . 3_555 N
C2a C2a C2a 45.0000(7) 4_555 . 14_555 N
C2a C2a C2a 45.0000(7) 4_555 . 17_555 N
C2a C2a O2b 120.0(17) 4_555 . 1_555 N
C2a C2a O2b 69.2(4) 4_555 . 14_555 N
C2a C2a O2b 69.2(4) 4_555 . 17_555 N
C2a C2a O2a 59.7(11) 4_555 . 1_555 N
C2a C2a C2a 90.0000(15) 14_555 . 17_555 N
C2a C2a O2b 110.7(11) 14_555 . 1_555 N
C2a C2a O2b 41.3(12) 14_555 . 14_555 N
C2a C2a O2b 104.4(6) 14_555 . 17_555 N
C2a C2a O2a 69.1(7) 14_555 . 1_555 N
C2a C2a O2b 110.7(11) 17_555 . 1_555 N
C2a C2a O2b 104.4(6) 17_555 . 14_555 N
C2a C2a O2b 41.3(12) 17_555 . 17_555 N
C2a C2a O2a 69.1(7) 17_555 . 1_555 N
O2b C2a O2b 69.4(23) 1_555 . 14_555 N
O2b C2a O2b 69.4(23) 1_555 . 17_555 N
O2b C2a O2a 180.000(9) 1_555 . 1_555 N
O2b C2a O2b 90.1(25) 14_555 . 17_555 N
O2b C2a O2a 110.4(19) 14_555 . 1_555 N
O2b C2a O2a 110.4(19) 17_555 . 1_555 N
C2a O2b C2a 28.0(5) 1_555 . 14_555 N
C2a O2b C2a 28.0(5) 1_555 . 17_555 N
C2a O2b O2b 69.3(11) 1_555 . 14_555 N
C2a O2b O2b 69.3(11) 1_555 . 17_555 N
C2a O2b O3a 152(5) 1_555 . 14_555 N
C2a O2b O3b 123.0(24) 1_555 . 2_555 N
C2a O2b C2a 41.6(8) 14_555 . 17_555 N
C2a O2b O2b 41.3(12) 14_555 . 14_555 N
C2a O2b O2b 75.6(6) 14_555 . 17_555 N
C2a O2b O3a 157.5(16) 14_555 . 14_555 N
C2a O2b O3b 137.7(19) 14_555 . 2_555 N
C2a O2b O2b 75.6(6) 17_555 . 14_555 N
C2a O2b O2b 41.3(12) 17_555 . 17_555 N
C2a O2b O3a 157.5(16) 17_555 . 14_555 N
C2a O2b O3b 137.7(19) 17_555 . 2_555 N
O2b O2b O2b 90.0000(15) 14_555 . 17_555 N
O2b O2b O3a 126.9(16) 14_555 . 14_555 N
O2b O2b O3b 134.92(8) 14_555 . 2_555 N
O2b O2b O3a 126.9(16) 17_555 . 14_555 N
O2b O2b O3b 134.92(8) 17_555 . 2_555 N
O3a O2b O3b 28.9(35) 14_555 . 2_555 N
C2a O2a C2a 60.7(22) 1_555 . 4_555 N
C2a O2a C2a 41.9(15) 1_555 . 14_555 N
C2a O2a C2a 41.9(15) 1_555 . 17_555 N
C2a O2a C2a 41.9(15) 4_555 . 14_555 N
C2a O2a C2a 41.9(15) 4_555 . 17_555 N
C2a O2a C2a 60.7(22) 14_555 . 17_555 N
O3a C3a O3a 144(4) 1_555 . 13_555 N
O3a C3a O3b 180.000(13) 1_555 . 1_555 N
O3a C3a O3b 36(4) 1_555 . 13_555 N
O3a C3a O3b 36(4) 13_555 . 1_555 N
O3a C3a O3b 180.000(13) 13_555 . 13_555 N
O3b C3a O3b 145(4) 1_555 . 13_555 N
O2b O3a C3a 175(5) 14_555 . 1_555 N
O2b O3a O3b 103(4) 14_555 . 13_555 N
C3a O3a O3b 71.9(21) 1_555 . 13_555 N
O2b O3b C3a 120.6(30) 3_555 . 1_555 N
O2b O3b O3a 48.1(18) 3_555 . 13_555 N
C3a O3b O3a 72.6(22) 1_555 . 13_555 N
Cr1 Os C1a 135.7(8) 1_555 . 1_555 N
Cr1 Os C1a 135.7(8) 1_555 . 12_565 N
Cr1 Os O1a 180.0 1_555 . 1_555 N
C1a Os C1a 88.6(17) 1_555 . 12_565 N
C1a Os O1a 44.3(8) 1_555 . 1_555 N
C1a Os O1a 44.3(8) 12_565 . 1_555 N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_cell_measurement_theta_min      4
_cell_measurement_theta_max      160


_exptl_special_details           
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions   
; ?
;
_vrf_PLAT601_1P5CO2_1_publ       
;
PROBLEM: Structure Contains Solvent Accessible VOIDS of .       2815 Ang3   
RESPONSE: This is expected as the material is porous and it is evacuated.
;
_vrf_PLAT430_1P5CO2_1_publ       
;
PROBLEM: Short Inter D...A Contact  O1B    ..  O1B     ..       1.88 Ang.  
RESPONSE:  The problem happens because the adsorbed carbon dioxide on the open metal sites are disordered and thus some atoms ostensibly are seemed to be close to each other.
;


# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location               
; ?
;
_pd_calibration_special_details  
# description of the method used
# to calibrate the instrument
; ?
;

_diffrn_ambient_temperature      10
_diffrn_source                   ?
_diffrn_source_target            ?
_diffrn_source_type              ?
_diffrn_measurement_device_type  BT1
_diffrn_detector                 ?
_diffrn_detector_type            ? # make or model of detector

_pd_meas_scan_method             ? # options are 'step', 'cont',
# 'tof', 'fixed' or
# 'disp' (= dispersive)
_pd_meas_special_details         
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection       ?
_computing_data_reduction        ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction     ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator  ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono          ?
_pd_instr_dist_mono/spec         ?
_pd_instr_dist_src/spec          ?
_pd_instr_dist_spec/anal         ?
_pd_instr_dist_anal/detc         ?
_pd_instr_dist_spec/detc         ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial              ? # perpendicular to
# equatorial plane

_pd_spec_size_equat              ? # parallel to
# scattering vector
# in transmission

_pd_spec_size_thick              ? # parallel to
# scattering vector
# in reflection

_pd_spec_mounting                
# This field should be
# used to give details of the
# container.
; ?
;

_pd_spec_mount_mode              ? # options are 'reflection'
# or 'transmission'

_pd_spec_shape                   ? # options are 'cylinder'
# 'flat_sheet' or 'irregular'


loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_length_neutron
_atom_type_scat_source
Cr 12.0 0.3635 International_Tables_Vol_C
C 94.974 0.6646 International_Tables_Vol_C
Cl 3.0 0.9577 International_Tables_Vol_C
N 96.0 0.9360 International_Tables_Vol_C
H 24.0 -0.3739 International_Tables_Vol_C
O 48.773 0.5803 International_Tables_Vol_C
_diffrn_radiation_probe          neutron
_diffrn_radiation_wavelength     2.078
_pd_proc_ls_prof_R_factor        0.0271
_pd_proc_ls_prof_wR_factor       0.0317
_pd_proc_ls_prof_wR_expected     0.0272
_refine_ls_R_Fsqd_factor         0.05488

_pd_proc_ls_background_function  
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    1275.77     2:   -299.604     3:    396.780     4:   -83.1875    
      5:    235.412     6:   -61.9798     7:    148.343     8:   -46.3653    
      9:    74.4780    10:   -19.7223    11:    18.3584    12:   -13.5676    
;

_exptl_absorpt_process_details   
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_correction_T_max  1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min   1.00000
_gsas_exptl_extinct_corr_T_max   1.00000

_pd_proc_ls_profile_function     
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =  507.887 #2(GV)   = -279.924 #3(GW)   =  120.258
 #4(GP)   =    0.000 #5(LX)   =    0.000 #6(LY)   =   26.221
 #7(S/L)  =   0.0431 #8(H/L)  =   0.0353
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_info_datetime           2016-03-03T18:49:17
_pd_calc_method                  'Rietveld Refinement'

#---- raw/calc data loop -----
_pd_meas_2theta_range_min        1.5
_pd_meas_2theta_range_max        166.25
_pd_meas_2theta_range_inc        0.05
_pd_proc_2theta_range_min        1.552
_pd_proc_2theta_range_max        166.302
_pd_proc_2theta_range_inc        0.05

loop_
_pd_meas_intensity_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
7910(190) 0.0 3754. .
7000(180) 0.0 3728. .
6080(170) 0.0 3701. .
5680(160) 0.0 3675. .
5000(150) 0.0 3649. .
4370(140) 0.0 3623. .
3990(130) 0.0 3598. .
3950(130) 0.0 3573. .
3310(120) 0.0 3548. .
3310(120) 0.0 3523. .
3120(120) 0.0 3498. .
2850(110) 0.0 3474. .
3090(120) 0.0 3450. .
2790(110) 0.0 3426. .
2590(110) 0.0 3403. .
2760(110) 0.0 3379. .
2810(110) 0.0 3356. .
2600(110) 0.0 3333. .
2730(110) 0.0 3311. .
2710(110) 0.0 3288. .
2780(110) 0.0 3266. .
2950(120) 0.0 3244. .
2920(120) 0.0 3222. .
2930(120) 0.0 3200. .
2960(120) 0.0 3179. .
2780(110) 0.0 3158. .
2700(110) 0.0 3137. .
3110(120) 0.0 3116. .
2890(110) 0.0 3095. .
2970(120) 0.0 3075. .
3070(120) 0.0 3055. .
2910(120) 0.0 3035. .
2960(120) 0.0 3015. .
2710(110) 0.0 2995. .
3170(120) 0.0 2976. .
2800(110) 0.0 2956. .
2850(110) 0.0 2937. .
2760(110) 0.0 2919. .
2790(110) 0.0 2900. .
2720(110) 0.0 2881. .
2810(110) 0.0 2863. .
2570(110) 0.0 2845. .
2830(110) 0.0 2827. .
2710(110) 0.0 2809. .
2750(110) 0.0 2792. .
2810(110) 0.0 2774. .
2720(110) 0.0 2757. .
2810(110) 0.0 2740. .
2660(110) 0.0 2723. .
3020(120) 0.0 2706. .
2720(110) 0.0 2690. .
2750(110) 0.0000797 2674. 2674.
2670(110) 0.0000826 2657. 2657.
3100(120) 0.0000706 2641. 2641.
3070(120) 0.0000718 2625. 2625.
2960(120) 0.0000743 2610. 2610.
3140(120) 0.0000706 2594. 2621.
3080(120) 0.0000718 2579. 2618.
2770(110) 0.0000797 2563. 2627.
3090(120) 0.0000718 2548. 2652.
3070(120) 0.0000718 2533. 2698.
3070(120) 0.0000718 2519. 2763.
3140(120) 0.0000706 2504. 2847.
3250(120) 0.0000683 2490. 2943.
3150(120) 0.0000706 2475. 3050.
3430(130) 0.0000640 2461. 3164.
3460(130) 0.0000640 2447. 3287.
3530(130) 0.0000630 2433. 3417.
3370(120) 0.0000661 2419. 3556.
3930(130) 0.0000565 2406. 3704.
3990(130) 0.0000557 2392. 3862.
3860(130) 0.0000574 2379. 4031.
4160(140) 0.0000533 2366. 4212.
4500(140) 0.0000489 2353. 4407.
4510(140) 0.0000489 2340. 4616.
4760(150) 0.0000463 2327. 4842.
4870(150) 0.0000457 2314. 5087.
5030(150) 0.0000439 2302. 5352.
5290(150) 0.0000422 2289. 5642.
5830(160) 0.0000381 2277. 5959.
5950(160) 0.0000372 2265. 6308.
6620(170) 0.0000334 2253. 6694.
6890(180) 0.0000323 2241. 7125.
7440(180) 0.0000299 2230. 7607.
8130(190) 0.0000274 2218. 8154.
8540(200) 0.0000260 2206. 8780.
9070(200) 0.0000245 2195. 9506.
10130(210) 0.0000220 2184. 10366.
11370(230) 0.0000196 2173. 11408.
12590(240) 0.0000177 2162. 12720.
14200(250) 0.0000157 2151. 14449.
16700(270) 0.0000134 2140. 16815.
21490(310) 0.0000104 2129. 20018.
24900(330) 8.96e-6 2119. 23943.
27880(350) 8.03e-6 2108. 27745.
29030(360) 7.72e-6 2098. 29793.
27600(350) 8.12e-6 2088. 28475.
24050(330) 9.30e-6 2078. 23559.
17570(280) 0.0000128 2068. 16755.
11760(230) 0.0000189 2058. 10450.
6050(110) 0.0000783 2048. 6077.
3767(90) 0.0001235 2039. 3713.
2695(76) 0.0001731 2029. 2688.
2216(69) 0.0002100 2020. 2315.
2106(67) 0.0002228 2010. 2187.
2122(67) 0.0002228 2001. 2133.
2025(66) 0.0002296 1992. 2101.
1970(65) 0.0002367 1983. 2075.
2076(67) 0.0002228 1974. 2054.
2010(65) 0.0002367 1965. 2035.
2048(66) 0.0002296 1956. 2018.
1866(63) 0.0002520 1948. 2002.
1877(63) 0.0002520 1939. 1988.
1778(62) 0.0002601 1931. 1974.
1872(63) 0.0002520 1922. 1962.
1781(62) 0.0002601 1914. 1954.
1759(61) 0.0002687 1906. 1943.
1711(60) 0.0002778 1898. 1933.
1762(61) 0.0002687 1890. 1923.
1722(61) 0.0002687 1882. 1913.
1795(62) 0.0002601 1874. 1904.
1818(62) 0.0002601 1867. 1896.
1749(61) 0.0002687 1859. 1889.
1760(61) 0.0002687 1851. 1864.
1875(63) 0.0002520 1844. 1864.
1859(63) 0.0002520 1837. 1869.
1893(64) 0.0002441 1829. 1882.
1899(64) 0.0002441 1822. 1902.
1854(63) 0.0002520 1815. 1929.
1900(64) 0.0002441 1808. 1962.
1906(64) 0.0002441 1801. 2000.
2037(66) 0.0002296 1794. 2044.
2095(67) 0.0002228 1787. 2092.
2139(68) 0.0002163 1781. 2145.
2087(67) 0.0002228 1774. 2205.
2205(69) 0.0002100 1768. 2272.
2341(71) 0.0001984 1761. 2347.
2315(70) 0.0002041 1755. 2434.
2314(70) 0.0002041 1748. 2534.
2557(74) 0.0001826 1742. 2650.
2778(77) 0.0001687 1736. 2789.
2945(79) 0.0001602 1730. 2957.
3052(81) 0.0001524 1724. 3171.
3395(85) 0.0001384 1718. 3454.
3955(92) 0.0001181 1712. 3843.
4480(98) 0.0001041 1706. 4372.
5300(110) 0.0000890 1700. 5021.
5810(110) 0.0000812 1695. 5650.
6050(110) 0.0000769 1689. 5988.
5950(110) 0.0000783 1683. 5770.
5190(110) 0.0000907 1678. 4970.
3944(92) 0.0001181 1673. 3889.
2897(79) 0.0001602 1667. 2914.
2224(69) 0.0002100 1662. 2255.
1798(62) 0.0002601 1657. 1907.
1639(59) 0.0002873 1652. 1766.
1681(60) 0.0002778 1646. 1709.
1636(59) 0.0002873 1641. 1687.
1607(59) 0.0002873 1636. 1675.
1593(58) 0.0002973 1631. 1666.
1633(59) 0.0002873 1627. 1658.
1579(58) 0.0002973 1622. 1652.
1640(59) 0.0002873 1617. 1646.
1587(58) 0.0002973 1612. 1642.
1663(60) 0.0002778 1608. 1637.
1693(60) 0.0002778 1603. 1634.
1858(63) 0.0002520 1599. 1631.
1653(59) 0.0002873 1594. 1630.
1760(61) 0.0002687 1590. 1633.
1731(61) 0.0002687 1586. 1644.
1782(62) 0.0002601 1581. 1669.
1913(64) 0.0002441 1577. 1714.
1916(64) 0.0002441 1573. 1785.
1985(65) 0.0002367 1569. 1883.
2091(67) 0.0002228 1565. 2006.
2219(69) 0.0002100 1561. 2150.
2327(71) 0.0001984 1557. 2312.
2592(74) 0.0001826 1553. 2501.
2728(76) 0.0001731 1549. 2716.
2850(78) 0.0001644 1545. 2964.
3137(82) 0.0001487 1541. 3252.
3442(86) 0.0001352 1537. 3595.
3683(89) 0.0001262 1534. 4014.
4299(96) 0.0001085 1530. 4548.
5210(110) 0.0000907 1527. 5260.
6070(110) 0.0000769 1523. 6238.
7370(130) 0.0000640 1520. 7543.
9310(140) 0.0000503 1516. 9066.
10410(150) 0.0000450 1513. 10394.
10740(150) 0.0000439 1509. 10871.
9830(150) 0.0000476 1506. 9998.
7950(130) 0.0000592 1503. 7962.
5540(110) 0.0000842 1500. 5594.
3623(88) 0.0001291 1496. 3673.
2428(72) 0.0001929 1493. 2490.
1859(63) 0.0002520 1490. 1914.
1566(79) 0.0001602 1487. 1683.
1542(78) 0.0001644 1484. 1599.
1472(76) 0.0001731 1481. 1564.
1361(73) 0.0001877 1478. 1545.
1492(56) 0.0003189 1475. 1531.
1541(57) 0.0003078 1472. 1520.
1566(58) 0.0002973 1469. 1511.
1566(58) 0.0002973 1467. 1503.
1467(56) 0.0003189 1464. 1496.
1510(57) 0.0003078 1461. 1489.
1522(57) 0.0003078 1458. 1484.
1525(57) 0.0003078 1456. 1479.
1472(56) 0.0003189 1453. 1475.
1533(57) 0.0003078 1451. 1471.
1552(57) 0.0003078 1448. 1468.
1602(58) 0.0002973 1446. 1465.
1516(57) 0.0003078 1443. 1463.
1471(56) 0.0003189 1441. 1462.
1445(55) 0.0003306 1438. 1461.
1486(56) 0.0003189 1436. 1460.
1477(56) 0.0003189 1434. 1461.
1488(56) 0.0003189 1431. 1462.
1458(56) 0.0003189 1429. 1464.
1473(56) 0.0003189 1427. 1469.
1497(56) 0.0003189 1424. 1476.
1494(56) 0.0003189 1422. 1486.
1542(57) 0.0003078 1420. 1489.
1470(56) 0.0003189 1418. 1494.
1488(56) 0.0003189 1416. 1489.
1459(56) 0.0003189 1414. 1473.
1370(54) 0.0003429 1412. 1452.
1396(54) 0.0003429 1410. 1432.
1474(56) 0.0003189 1408. 1419.
1445(55) 0.0003306 1406. 1411.
1424(55) 0.0003306 1404. 1406.
1449(55) 0.0003306 1402. 1403.
1489(56) 0.0003189 1400. 1401.
1445(55) 0.0003306 1398. 1399.
1417(55) 0.0003306 1396. 1397.
1459(56) 0.0003189 1395. 1395.
1467(56) 0.0003189 1393. 1393.
1348(53) 0.000356 1391. 1392.
1462(56) 0.0003189 1389. 1390.
1486(56) 0.0003189 1388. 1388.
1459(56) 0.0003189 1386. 1387.
1357(54) 0.0003429 1384. 1385.
1479(56) 0.0003189 1383. 1384.
1507(56) 0.0003189 1381. 1383.
1502(56) 0.0003189 1380. 1382.
1470(56) 0.0003189 1378. 1381.
1383(54) 0.0003429 1377. 1380.
1443(55) 0.0003306 1375. 1380.
1438(55) 0.0003306 1374. 1380.
1426(55) 0.0003306 1372. 1380.
1433(55) 0.0003306 1371. 1381.
1341(53) 0.000356 1369. 1383.
1416(55) 0.0003306 1368. 1385.
1412(55) 0.0003306 1366. 1386.
1397(54) 0.0003429 1365. 1385.
1470(56) 0.0003189 1364. 1381.
1448(55) 0.0003306 1362. 1375.
1377(54) 0.0003429 1361. 1369.
1381(54) 0.0003429 1360. 1364.
1400(54) 0.0003429 1359. 1361.
1421(55) 0.0003306 1357. 1359.
1424(55) 0.0003306 1356. 1357.
1355(54) 0.0003429 1355. 1356.
1413(55) 0.0003306 1354. 1355.
1412(55) 0.0003306 1352. 1354.
1412(55) 0.0003306 1351. 1353.
1385(54) 0.0003429 1350. 1352.
1469(56) 0.0003189 1349. 1352.
1429(55) 0.0003306 1348. 1352.
1451(55) 0.0003306 1347. 1354.
1347(53) 0.000356 1346. 1357.
1291(52) 0.000370 1345. 1362.
1373(54) 0.0003429 1344. 1369.
1378(54) 0.0003429 1343. 1378.
1471(56) 0.0003189 1342. 1389.
1496(56) 0.0003189 1341. 1404.
1481(56) 0.0003189 1340. 1423.
1507(57) 0.0003078 1339. 1451.
1527(57) 0.0003078 1338. 1488.
1569(58) 0.0002973 1337. 1532.
1543(57) 0.0003078 1336. 1574.
1566(58) 0.0002973 1335. 1594.
1550(57) 0.0003078 1334. 1575.
1565(58) 0.0002973 1333. 1520.
1460(56) 0.0003189 1332. 1452.
1467(56) 0.0003189 1331. 1397.
1490(56) 0.0003189 1331. 1361.
1358(54) 0.0003429 1330. 1344.
1376(54) 0.0003429 1329. 1336.
1385(54) 0.0003429 1328. 1332.
1348(53) 0.000356 1327. 1331.
1307(53) 0.000356 1327. 1330.
1347(53) 0.000356 1326. 1329.
1306(53) 0.000356 1325. 1328.
1277(52) 0.000370 1324. 1327.
1269(52) 0.000370 1324. 1326.
1286(76) 0.0001731 1323. 1325.
1375(53) 0.000356 1322. 1324.
1392(54) 0.0003429 1321. 1323.
1363(53) 0.000356 1321. 1323.
1381(54) 0.0003429 1320. 1322.
1410(54) 0.0003429 1319. 1321.
1355(53) 0.000356 1319. 1321.
1396(54) 0.0003429 1318. 1320.
1351(53) 0.000356 1317. 1319.
1333(53) 0.000356 1317. 1319.
1330(53) 0.000356 1316. 1318.
1392(54) 0.0003429 1316. 1318.
1371(53) 0.000356 1315. 1318.
1246(51) 0.000384 1314. 1317.
1328(52) 0.000370 1314. 1317.
1386(54) 0.0003429 1313. 1317.
1331(53) 0.000356 1313. 1316.
1403(54) 0.0003429 1312. 1318.
1380(53) 0.000356 1312. 1318.
1390(54) 0.0003429 1311. 1318.
1321(52) 0.000370 1310. 1319.
1356(53) 0.000356 1310. 1321.
1372(53) 0.000356 1309. 1325.
1383(54) 0.0003429 1309. 1332.
1422(54) 0.0003429 1308. 1344.
1396(54) 0.0003429 1308. 1364.
1423(54) 0.0003429 1307. 1391.
1471(55) 0.0003306 1307. 1428.
1494(56) 0.0003189 1306. 1477.
1571(57) 0.0003078 1306. 1542.
1714(60) 0.0002778 1306. 1633.
1805(61) 0.0002687 1305. 1753.
1967(64) 0.0002441 1305. 1894.
2238(68) 0.0002163 1304. 2018.
2145(67) 0.0002228 1304. 2068.
1996(64) 0.0002441 1303. 1998.
1868(62) 0.0002601 1303. 1827.
1619(58) 0.0002973 1302. 1634.
1440(55) 0.0003306 1302. 1483.
1337(53) 0.000356 1302. 1393.
1351(53) 0.000356 1301. 1350.
1350(53) 0.000356 1301. 1334.
1322(52) 0.000370 1300. 1329.
1348(53) 0.000356 1300. 1330.
1301(52) 0.000370 1300. 1334.
1438(55) 0.0003306 1299. 1346.
1371(53) 0.000356 1299. 1368.
1400(54) 0.0003429 1299. 1407.
1534(56) 0.0003189 1298. 1467.
1657(59) 0.0002873 1298. 1553.
1618(58) 0.0002973 1298. 1669.
1809(61) 0.0002687 1297. 1828.
1954(64) 0.0002441 1297. 2048.
2300(69) 0.0002100 1297. 2344.
2672(74) 0.0001826 1296. 2703.
2906(77) 0.0001687 1296. 3043.
3027(79) 0.0001602 1296. 3219.
2860(77) 0.0001687 1295. 3097.
2424(71) 0.0001984 1295. 2698.
2053(65) 0.0002367 1295. 2202.
1731(60) 0.0002778 1294. 1792.
1426(54) 0.0003429 1294. 1537.
1248(51) 0.000384 1294. 1410.
1267(51) 0.000384 1293. 1357.
1279(52) 0.000370 1293. 1336.
1281(52) 0.000370 1293. 1326.
1261(51) 0.000384 1293. 1320.
1253(51) 0.000384 1292. 1317.
1234(51) 0.000384 1292. 1314.
1277(51) 0.000384 1292. 1311.
1301(52) 0.000370 1291. 1310.
1379(53) 0.000356 1291. 1308.
1274(51) 0.000384 1291. 1307.
1323(52) 0.000370 1291. 1306.
1180(49) 0.000416 1290. 1305.
1263(51) 0.000384 1290. 1305.
1261(51) 0.000384 1290. 1305.
1219(50) 0.000400 1290. 1307.
1231(51) 0.000384 1289. 1307.
1228(50) 0.000400 1289. 1308.
1350(53) 0.000356 1289. 1309.
1288(52) 0.000370 1289. 1310.
1293(52) 0.000370 1288. 1312.
1356(53) 0.000356 1288. 1315.
1302(52) 0.000370 1288. 1319.
1297(52) 0.000370 1288. 1326.
1315(52) 0.000370 1287. 1337.
1361(53) 0.000356 1287. 1360.
1501(56) 0.0003189 1287. 1400.
1541(56) 0.0003189 1287. 1470.
1644(58) 0.0002973 1286. 1580.
1805(61) 0.0002687 1286. 1740.
1979(64) 0.0002441 1286. 1967.
2190(67) 0.0002228 1286. 2286.
2774(76) 0.0001731 1286. 2718.
3368(83) 0.0001452 1285. 3240.
3928(90) 0.0001235 1285. 3735.
3985(91) 0.0001208 1285. 3997.
3676(87) 0.0001321 1285. 3834.
3127(80) 0.0001562 1284. 3269.
2396(67) 0.0002228 1284. 2572.
1950(60) 0.0002778 1284. 1997.
1600(55) 0.0003306 1284. 1639.
1406(51) 0.000384 1284. 1461.
1317(50) 0.000400 1283. 1388.
1350(50) 0.000400 1283. 1362.
1353(50) 0.000400 1283. 1356.
1320(50) 0.000400 1283. 1363.
1375(51) 0.000384 1283. 1385.
1342(50) 0.000400 1282. 1427.
1401(51) 0.000384 1282. 1495.
1499(53) 0.000356 1282. 1597.
1622(55) 0.0003306 1282. 1744.
1805(58) 0.0002973 1282. 1947.
2125(63) 0.0002520 1281. 2199.
2297(65) 0.0002367 1281. 2451.
2527(68) 0.0002163 1281. 2605.
2422(67) 0.0002228 1281. 2560.
2278(65) 0.0002367 1281. 2305.
1907(59) 0.0002873 1280. 1964.
1656(55) 0.0003306 1280. 1669.
1382(51) 0.000384 1280. 1478.
1373(51) 0.000384 1280. 1379.
1336(50) 0.000400 1280. 1336.
1294(49) 0.000416 1279. 1319.
1254(48) 0.000434 1279. 1312.
1248(48) 0.000434 1279. 1310.
1300(49) 0.000416 1279. 1311.
1272(49) 0.000416 1279. 1316.
1277(49) 0.000416 1278. 1326.
1365(50) 0.000400 1278. 1342.
1347(50) 0.000400 1278. 1366.
1382(51) 0.000384 1278. 1398.
1470(52) 0.000370 1278. 1434.
1528(53) 0.000356 1277. 1462.
1563(54) 0.0003429 1277. 1467.
1538(53) 0.000356 1277. 1442.
1432(52) 0.000370 1277. 1394.
1301(49) 0.000416 1277. 1349.
1269(49) 0.000416 1276. 1316.
1259(48) 0.000434 1276. 1299.
1297(49) 0.000416 1276. 1291.
1352(50) 0.000400 1276. 1287.
1264(49) 0.000416 1276. 1286.
1271(49) 0.000416 1275. 1286.
1299(49) 0.000416 1275. 1288.
1260(48) 0.000434 1275. 1291.
1277(49) 0.000416 1275. 1296.
1278(49) 0.000416 1275. 1303.
1245(48) 0.000434 1274. 1315.
1324(50) 0.000400 1274. 1329.
1297(49) 0.000416 1274. 1344.
1283(49) 0.000416 1274. 1354.
1270(49) 0.000416 1274. 1353.
1228(48) 0.000434 1274. 1340.
1251(48) 0.000434 1273. 1320.
1356(50) 0.000400 1273. 1303.
1244(48) 0.000434 1273. 1292.
1281(49) 0.000416 1273. 1286.
1194(47) 0.000453 1273. 1283.
1208(47) 0.000453 1272. 1282.
1256(48) 0.000434 1272. 1282.
1264(49) 0.000416 1272. 1282.
1247(48) 0.000434 1272. 1282.
1239(48) 0.000434 1272. 1283.
1267(49) 0.000416 1271. 1283.
1247(48) 0.000434 1271. 1284.
1296(49) 0.000416 1271. 1285.
1303(49) 0.000416 1271. 1286.
1155(46) 0.000473 1270. 1288.
1252(48) 0.000434 1270. 1289.
1256(48) 0.000434 1270. 1291.
1214(48) 0.000434 1270. 1295.
1239(48) 0.000434 1270. 1299.
1219(48) 0.000434 1269. 1303.
1366(50) 0.000400 1269. 1310.
1343(50) 0.000400 1269. 1321.
1372(51) 0.000384 1269. 1340.
1340(50) 0.000400 1269. 1378.
1416(51) 0.000384 1268. 1446.
1557(54) 0.0003429 1268. 1563.
1665(56) 0.0003189 1268. 1751.
1920(60) 0.0002778 1268. 2034.
2426(67) 0.0002228 1268. 2429.
3052(75) 0.0001778 1267. 2910.
3524(81) 0.0001524 1267. 3369.
3746(83) 0.0001452 1267. 3621.
3632(82) 0.0001487 1267. 3494.
3159(76) 0.0001731 1266. 3009.
2516(68) 0.0002163 1266. 2411.
1921(60) 0.0002778 1266. 1919.
1644(55) 0.0003306 1266. 1612.
1424(51) 0.000384 1266. 1461.
1362(50) 0.000400 1265. 1404.
1328(50) 0.000400 1265. 1398.
1334(50) 0.000400 1265. 1426.
1470(52) 0.000370 1265. 1493.
1633(55) 0.0003306 1265. 1612.
1835(58) 0.0002973 1264. 1800.
2109(62) 0.0002601 1264. 2071.
2650(70) 0.0002041 1264. 2410.
3044(75) 0.0001778 1264. 2748.
3278(78) 0.0001644 1263. 2954.
3214(77) 0.0001687 1263. 2897.
2856(72) 0.0001929 1263. 2573.
2343(66) 0.0002296 1263. 2145.
1891(59) 0.0002873 1262. 1780.
1588(54) 0.0003429 1262. 1545.
1371(50) 0.000400 1262. 1425.
1303(49) 0.000416 1262. 1379.
1321(49) 0.000416 1262. 1374.
1367(50) 0.000400 1261. 1397.
1473(52) 0.000370 1261. 1451.
1489(52) 0.000370 1261. 1547.
1641(55) 0.0003306 1261. 1697.
1948(60) 0.0002778 1260. 1907.
2190(63) 0.0002520 1260. 2154.
2451(67) 0.0002228 1260. 2374.
2503(68) 0.0002163 1260. 2467.
2230(64) 0.0002441 1259. 2361.
2138(63) 0.0002520 1259. 2096.
1853(58) 0.0002973 1259. 1804.
1598(54) 0.0003429 1259. 1580.
1410(51) 0.000384 1258. 1450.
1427(51) 0.000384 1258. 1395.
1427(51) 0.000384 1258. 1392.
1431(51) 0.000384 1258. 1430.
1491(52) 0.000370 1257. 1516.
1665(55) 0.0003306 1257. 1673.
1847(58) 0.0002973 1257. 1925.
2258(64) 0.0002441 1257. 2290.
2559(69) 0.0002100 1257. 2744.
3084(75) 0.0001778 1256. 3185.
3426(79) 0.0001602 1256. 3443.
3318(78) 0.0001644 1256. 3349.
2941(73) 0.0001877 1256. 2911.
2350(66) 0.0002296 1255. 2353.
1834(58) 0.0002973 1255. 1884.
1507(53) 0.000356 1255. 1582.
1399(51) 0.000384 1254. 1425.
1375(50) 0.000400 1254. 1354.
1268(48) 0.000434 1254. 1323.
1214(47) 0.000453 1254. 1309.
1320(49) 0.000416 1253. 1301.
1351(50) 0.000400 1253. 1297.
1348(50) 0.000400 1253. 1295.
1308(49) 0.000416 1253. 1296.
1329(50) 0.000400 1252. 1297.
1329(50) 0.000400 1252. 1295.
1320(49) 0.000416 1252. 1291.
1374(50) 0.000400 1252. 1284.
1340(50) 0.000400 1251. 1276.
1256(48) 0.000434 1251. 1270.
1268(48) 0.000434 1251. 1266.
1320(49) 0.000416 1251. 1263.
1234(48) 0.000434 1250. 1261.
1295(49) 0.000416 1250. 1260.
1247(48) 0.000434 1250. 1259.
1260(48) 0.000434 1250. 1259.
1289(49) 0.000416 1249. 1259.
1228(48) 0.000434 1249. 1259.
1276(49) 0.000416 1249. 1260.
1256(48) 0.000434 1248. 1260.
1242(48) 0.000434 1248. 1260.
1247(48) 0.000434 1248. 1257.
1294(49) 0.000416 1248. 1256.
1240(48) 0.000434 1247. 1254.
1268(48) 0.000434 1247. 1252.
1309(49) 0.000416 1247. 1251.
1260(48) 0.000434 1247. 1250.
1305(49) 0.000416 1246. 1250.
1231(48) 0.000434 1246. 1249.
1208(47) 0.000453 1246. 1249.
1275(49) 0.000416 1245. 1249.
1260(48) 0.000434 1245. 1248.
1285(49) 0.000416 1245. 1248.
1262(48) 0.000434 1245. 1247.
1286(49) 0.000416 1244. 1247.
1177(47) 0.000453 1244. 1248.
1282(49) 0.000416 1244. 1245.
1241(48) 0.000434 1244. 1245.
1221(48) 0.000434 1243. 1245.
1291(49) 0.000416 1243. 1245.
1254(48) 0.000434 1243. 1244.
1268(48) 0.000434 1242. 1244.
1209(47) 0.000453 1242. 1244.
1281(49) 0.000416 1242. 1244.
1284(49) 0.000416 1242. 1244.
1211(47) 0.000453 1241. 1244.
1252(48) 0.000434 1241. 1243.
1265(48) 0.000434 1241. 1243.
1271(48) 0.000434 1240. 1245.
1238(48) 0.000434 1240. 1245.
1201(47) 0.000453 1240. 1245.
1237(48) 0.000434 1240. 1245.
1292(49) 0.000416 1239. 1245.
1215(47) 0.000453 1239. 1245.
1173(47) 0.000453 1239. 1245.
1201(47) 0.000453 1238. 1245.
1187(47) 0.000453 1238. 1245.
1285(47) 0.000453 1238. 1246.
1269(46) 0.000473 1238. 1246.
1274(46) 0.000473 1237. 1246.
1282(47) 0.000453 1237. 1247.
1301(47) 0.000453 1237. 1248.
1271(46) 0.000473 1236. 1248.
1393(49) 0.000416 1236. 1249.
1297(47) 0.000453 1236. 1251.
1322(47) 0.000453 1236. 1253.
1322(47) 0.000453 1235. 1256.
1300(47) 0.000453 1235. 1261.
1303(47) 0.000453 1235. 1271.
1380(48) 0.000434 1234. 1291.
1367(48) 0.000434 1234. 1325.
1393(49) 0.000416 1234. 1380.
1471(50) 0.000400 1234. 1458.
1451(50) 0.000400 1233. 1551.
1596(52) 0.000370 1233. 1632.
1609(52) 0.000370 1233. 1666.
1568(52) 0.000370 1232. 1628.
1462(50) 0.000400 1232. 1539.
1416(49) 0.000416 1232. 1443.
1379(48) 0.000434 1231. 1373.
1425(49) 0.000416 1231. 1338.
1363(48) 0.000434 1231. 1337.
1293(47) 0.000453 1231. 1370.
1416(49) 0.000416 1230. 1444.
1640(53) 0.000356 1230. 1574.
1741(54) 0.0003429 1230. 1764.
1972(58) 0.0002973 1229. 1996.
2201(61) 0.0002687 1229. 2210.
2285(62) 0.0002601 1229. 2317.
2144(60) 0.0002778 1229. 2245.
1915(57) 0.0003078 1228. 2027.
1739(54) 0.0003429 1228. 1776.
1554(51) 0.000384 1228. 1582.
1539(51) 0.000384 1227. 1477.
1556(51) 0.000384 1227. 1459.
1551(51) 0.000384 1227. 1527.
1708(54) 0.0003429 1226. 1694.
2139(60) 0.0002778 1226. 1990.
2543(66) 0.0002296 1226. 2424.
3120(73) 0.0001877 1226. 2945.
3663(79) 0.0001602 1225. 3414.
3866(81) 0.0001524 1225. 3623.
3639(79) 0.0001602 1225. 3422.
3114(73) 0.0001877 1224. 2901.
2427(64) 0.0002441 1224. 2317.
1852(56) 0.0003189 1224. 1856.
1561(51) 0.000384 1223. 1568.
1343(48) 0.000434 1223. 1417.
1375(48) 0.000434 1223. 1348.
1304(47) 0.000453 1223. 1316.
1270(46) 0.000473 1222. 1301.
1230(46) 0.000473 1222. 1291.
1267(46) 0.000473 1222. 1285.
1299(47) 0.000453 1221. 1280.
1237(46) 0.000473 1221. 1278.
1236(46) 0.000473 1221. 1278.
1215(45) 0.000494 1220. 1280.
1210(45) 0.000494 1220. 1285.
1275(46) 0.000473 1220. 1296.
1334(48) 0.000434 1220. 1319.
1384(48) 0.000434 1219. 1366.
1530(51) 0.000384 1219. 1457.
1653(53) 0.000356 1219. 1614.
1842(56) 0.0003189 1218. 1853.
2113(60) 0.0002778 1218. 2154.
2386(64) 0.0002441 1218. 2447.
2605(67) 0.0002228 1217. 2617.
2582(66) 0.0002296 1217. 2559.
2292(62) 0.0002601 1217. 2289.
1890(57) 0.0003078 1217. 1949.
1608(52) 0.000370 1216. 1662.
1470(50) 0.000400 1216. 1477.
1378(48) 0.000434 1216. 1384.
1355(48) 0.000434 1215. 1357.
1336(48) 0.000434 1215. 1375.
1417(49) 0.000416 1215. 1427.
1529(51) 0.000384 1214. 1505.
1572(52) 0.000370 1214. 1591.
1594(52) 0.000370 1214. 1653.
1576(52) 0.000370 1214. 1654.
1574(52) 0.000370 1213. 1586.
1486(50) 0.000400 1213. 1484.
1370(48) 0.000434 1213. 1390.
1335(48) 0.000434 1212. 1324.
1283(47) 0.000453 1212. 1286.
1196(45) 0.000494 1212. 1269.
1273(46) 0.000473 1211. 1261.
1271(46) 0.000473 1211. 1258.
1344(48) 0.000434 1211. 1258.
1319(47) 0.000453 1211. 1259.
1262(46) 0.000473 1210. 1262.
1327(47) 0.000453 1210. 1266.
1293(47) 0.000453 1210. 1272.
1332(48) 0.000434 1209. 1282.
1345(48) 0.000434 1209. 1297.
1283(47) 0.000453 1209. 1327.
1416(49) 0.000416 1208. 1387.
1587(41) 0.000595 1208. 1502.
1739(50) 0.000400 1208. 1709.
2143(56) 0.0003189 1208. 2043.
2554(61) 0.0002687 1207. 2498.
2996(66) 0.0002296 1207. 2995.
3317(69) 0.0002100 1207. 3371.
3360(70) 0.0002041 1206. 3434.
2926(65) 0.0002367 1206. 3116.
2412(59) 0.0002873 1206. 2590.
1904(52) 0.000370 1205. 2084.
1682(49) 0.000416 1205. 1717.
1488(46) 0.000473 1205. 1506.
1382(45) 0.000494 1205. 1410.
1392(45) 0.000494 1204. 1387.
1452(46) 0.000473 1204. 1408.
1499(47) 0.000453 1204. 1455.
1498(46) 0.000473 1203. 1509.
1508(47) 0.000453 1203. 1546.
1495(46) 0.000473 1203. 1542.
1452(46) 0.000473 1203. 1494.
1445(46) 0.000473 1202. 1430.
1398(45) 0.000494 1202. 1378.
1361(44) 0.000517 1202. 1355.
1403(45) 0.000494 1201. 1375.
1507(47) 0.000453 1201. 1448.
1663(49) 0.000416 1201. 1590.
1834(51) 0.000384 1200. 1805.
2161(56) 0.0003189 1200. 2070.
2418(59) 0.0002873 1200. 2314.
2472(60) 0.0002778 1200. 2433.
2314(58) 0.0002973 1199. 2348.
2106(55) 0.0003306 1199. 2101.
1836(51) 0.000384 1199. 1815.
1581(48) 0.000434 1198. 1587.
1434(45) 0.000494 1198. 1449.
1435(46) 0.000473 1198. 1397.
1486(46) 0.000473 1197. 1415.
1549(47) 0.000453 1197. 1490.
1688(49) 0.000416 1197. 1607.
1819(51) 0.000384 1197. 1739.
1948(53) 0.000356 1196. 1834.
1944(53) 0.000356 1196. 1840.
1776(51) 0.000384 1196. 1744.
1679(49) 0.000416 1195. 1597.
1550(47) 0.000453 1195. 1458.
1384(45) 0.000494 1195. 1360.
1368(44) 0.000517 1195. 1308.
1331(44) 0.000517 1194. 1292.
1270(43) 0.000541 1194. 1304.
1383(45) 0.000494 1194. 1336.
1372(44) 0.000517 1193. 1379.
1401(45) 0.000494 1193. 1416.
1477(46) 0.000473 1193. 1429.
1437(46) 0.000473 1193. 1406.
1379(45) 0.000494 1192. 1357.
1335(44) 0.000517 1192. 1306.
1321(44) 0.000517 1192. 1265.
1284(43) 0.000541 1191. 1239.
1205(42) 0.000567 1191. 1224.
1195(42) 0.000567 1191. 1215.
1195(42) 0.000567 1190. 1211.
1169(41) 0.000595 1190. 1209.
1230(42) 0.000567 1190. 1208.
1204(42) 0.000567 1190. 1208.
1218(42) 0.000567 1189. 1207.
1252(42) 0.000567 1189. 1208.
1222(42) 0.000567 1189. 1209.
1269(43) 0.000541 1188. 1213.
1214(42) 0.000567 1188. 1221.
1248(42) 0.000567 1188. 1237.
1271(43) 0.000541 1188. 1265.
1279(43) 0.000541 1187. 1307.
1269(43) 0.000541 1187. 1360.
1358(44) 0.000517 1187. 1409.
1343(44) 0.000517 1186. 1435.
1392(45) 0.000494 1186. 1421.
1318(44) 0.000517 1186. 1374.
1329(44) 0.000517 1186. 1316.
1332(44) 0.000517 1185. 1268.
1257(43) 0.000541 1185. 1235.
1175(41) 0.000595 1185. 1217.
1175(41) 0.000595 1184. 1207.
1180(41) 0.000595 1184. 1202.
1263(43) 0.000541 1184. 1200.
1263(43) 0.000541 1184. 1199.
1211(42) 0.000567 1183. 1198.
1128(40) 0.000625 1183. 1198.
1144(41) 0.000595 1183. 1199.
1265(43) 0.000541 1182. 1201.
1217(42) 0.000567 1182. 1204.
1234(42) 0.000567 1182. 1210.
1255(43) 0.000541 1182. 1222.
1202(42) 0.000567 1181. 1241.
1291(43) 0.000541 1181. 1268.
1320(44) 0.000517 1181. 1300.
1381(45) 0.000494 1180. 1328.
1391(45) 0.000494 1180. 1342.
1337(44) 0.000517 1180. 1333.
1323(44) 0.000517 1180. 1310.
1301(43) 0.000541 1179. 1288.
1317(41) 0.000595 1179. 1283.
1348(42) 0.000567 1179. 1305.
1387(42) 0.000567 1178. 1365.
1495(44) 0.000517 1178. 1472.
1702(47) 0.000453 1178. 1622.
1773(48) 0.000434 1178. 1786.
1948(50) 0.000400 1177. 1913.
1932(50) 0.000400 1177. 1937.
1833(49) 0.000416 1177. 1839.
1674(47) 0.000453 1177. 1672.
1524(44) 0.000517 1176. 1510.
1381(42) 0.000567 1176. 1394.
1281(41) 0.000595 1176. 1335.
1269(41) 0.000595 1175. 1326.
1352(42) 0.000567 1175. 1357.
1367(42) 0.000567 1175. 1413.
1448(43) 0.000541 1175. 1471.
1464(44) 0.000517 1174. 1505.
1420(43) 0.000541 1174. 1492.
1374(42) 0.000567 1174. 1434.
1328(42) 0.000567 1173. 1362.
1265(41) 0.000595 1173. 1299.
1227(40) 0.000625 1173. 1257.
1231(40) 0.000625 1173. 1237.
1232(40) 0.000625 1172. 1233.
1229(40) 0.000625 1172. 1241.
1284(41) 0.000595 1172. 1255.
1308(41) 0.000595 1172. 1266.
1257(40) 0.000625 1171. 1268.
1289(41) 0.000595 1171. 1258.
1270(41) 0.000595 1171. 1240.
1248(40) 0.000625 1170. 1222.
1188(39) 0.000657 1170. 1208.
1234(40) 0.000625 1170. 1199.
1176(39) 0.000657 1170. 1196.
1202(40) 0.000625 1169. 1195.
1224(40) 0.000625 1169. 1196.
1213(40) 0.000625 1169. 1199.
1212(40) 0.000625 1168. 1202.
1198(39) 0.000657 1168. 1205.
1190(39) 0.000657 1168. 1210.
1280(41) 0.000595 1168. 1219.
1240(40) 0.000625 1167. 1239.
1281(41) 0.000595 1167. 1279.
1412(43) 0.000541 1167. 1350.
1502(44) 0.000517 1167. 1461.
1715(47) 0.000453 1166. 1605.
1873(49) 0.000416 1166. 1753.
1983(51) 0.000384 1166. 1854.
2041(51) 0.000384 1165. 1852.
1861(49) 0.000416 1165. 1745.
1643(46) 0.000473 1165. 1588.
1463(44) 0.000517 1165. 1441.
1336(42) 0.000567 1164. 1332.
1275(41) 0.000595 1164. 1264.
1227(40) 0.000625 1164. 1227.
1178(39) 0.000657 1164. 1208.
1188(39) 0.000657 1163. 1199.
1238(40) 0.000625 1163. 1194.
1208(40) 0.000625 1163. 1190.
1152(39) 0.000657 1162. 1187.
1161(39) 0.000657 1162. 1185.
1148(39) 0.000657 1162. 1184.
1170(39) 0.000657 1162. 1183.
1204(40) 0.000625 1161. 1183.
1171(39) 0.000657 1161. 1183.
1269(41) 0.000595 1161. 1183.
1221(40) 0.000625 1161. 1183.
1171(39) 0.000657 1160. 1184.
1210(40) 0.000625 1160. 1186.
1235(40) 0.000625 1160. 1189.
1222(40) 0.000625 1160. 1194.
1197(39) 0.000657 1159. 1204.
1222(40) 0.000625 1159. 1222.
1243(40) 0.000625 1159. 1254.
1265(41) 0.000595 1158. 1304.
1327(42) 0.000567 1158. 1370.
1448(43) 0.000541 1158. 1442.
1496(44) 0.000517 1158. 1498.
1477(44) 0.000517 1157. 1513.
1485(44) 0.000517 1157. 1479.
1455(43) 0.000541 1157. 1418.
1389(42) 0.000567 1157. 1363.
1394(43) 0.000541 1156. 1336.
1382(42) 0.000567 1156. 1348.
1352(42) 0.000567 1156. 1403.
1408(43) 0.000541 1155. 1492.
1516(44) 0.000517 1155. 1593.
1573(45) 0.000494 1155. 1671.
1570(45) 0.000494 1155. 1689.
1578(45) 0.000494 1154. 1639.
1498(44) 0.000517 1154. 1557.
1443(43) 0.000541 1154. 1495.
1465(44) 0.000517 1154. 1492.
1521(44) 0.000517 1153. 1573.
1702(47) 0.000453 1153. 1744.
1966(50) 0.000400 1153. 1987.
2192(53) 0.000356 1153. 2242.
2404(56) 0.0003189 1152. 2416.
2423(56) 0.0003189 1152. 2418.
2134(49) 0.000416 1152. 2236.
1885(46) 0.000473 1151. 1967.
1680(44) 0.000517 1151. 1716.
1539(42) 0.000567 1151. 1540.
1473(41) 0.000595 1151. 1451.
1456(41) 0.000595 1150. 1437.
1493(41) 0.000595 1150. 1470.
1550(42) 0.000567 1150. 1517.
1534(42) 0.000567 1150. 1546.
1511(42) 0.000567 1149. 1531.
1487(41) 0.000595 1149. 1476.
1449(41) 0.000595 1149. 1411.
1381(40) 0.000625 1149. 1366.
1346(39) 0.000657 1148. 1360.
1317(39) 0.000657 1148. 1399.
1408(40) 0.000625 1148. 1480.
1552(42) 0.000567 1147. 1584.
1580(42) 0.000567 1147. 1674.
1599(43) 0.000541 1147. 1710.
1641(43) 0.000541 1147. 1664.
1599(43) 0.000541 1146. 1559.
1462(41) 0.000595 1146. 1442.
1300(39) 0.000657 1146. 1345.
1239(38) 0.000693 1146. 1281.
1227(37) 0.000730 1145. 1247.
1198(37) 0.000730 1145. 1236.
1209(37) 0.000730 1145. 1236.
1252(38) 0.000693 1145. 1238.
1178(37) 0.000730 1144. 1235.
1197(37) 0.000730 1144. 1223.
1206(37) 0.000730 1144. 1209.
1145(36) 0.000772 1144. 1196.
1144(36) 0.000772 1143. 1188.
1147(36) 0.000772 1143. 1186.
1176(37) 0.000730 1143. 1190.
1176(37) 0.000730 1142. 1197.
1233(38) 0.000693 1142. 1205.
1185(37) 0.000730 1142. 1208.
1180(37) 0.000730 1142. 1204.
1223(37) 0.000730 1141. 1194.
1180(37) 0.000730 1141. 1182.
1197(37) 0.000730 1141. 1171.
1139(36) 0.000772 1141. 1164.
1131(36) 0.000772 1140. 1159.
1141(36) 0.000772 1140. 1156.
1106(36) 0.000772 1140. 1155.
1128(36) 0.000772 1140. 1154.
1157(36) 0.000772 1139. 1154.
1156(36) 0.000772 1139. 1154.
1171(37) 0.000730 1139. 1155.
1201(37) 0.000730 1139. 1157.
1171(37) 0.000730 1138. 1161.
1193(37) 0.000730 1138. 1168.
1179(37) 0.000730 1138. 1177.
1127(36) 0.000772 1137. 1188.
1155(36) 0.000772 1137. 1197.
1177(37) 0.000730 1137. 1203.
1144(36) 0.000772 1137. 1203.
1152(36) 0.000772 1136. 1200.
1173(37) 0.000730 1136. 1200.
1206(37) 0.000730 1136. 1212.
1223(37) 0.000730 1136. 1238.
1311(39) 0.000657 1135. 1282.
1363(39) 0.000657 1135. 1338.
1365(39) 0.000657 1135. 1394.
1416(40) 0.000625 1135. 1428.
1399(40) 0.000625 1134. 1424.
1404(40) 0.000625 1134. 1383.
1301(39) 0.000657 1134. 1326.
1305(39) 0.000657 1134. 1276.
1254(38) 0.000693 1133. 1243.
1199(37) 0.000730 1133. 1231.
1299(39) 0.000657 1133. 1236.
1267(38) 0.000693 1132. 1249.
1286(38) 0.000693 1132. 1262.
1330(39) 0.000657 1132. 1264.
1285(38) 0.000693 1132. 1255.
1260(38) 0.000693 1131. 1242.
1212(37) 0.000730 1131. 1236.
1235(38) 0.000693 1131. 1246.
1309(39) 0.000657 1131. 1277.
1386(40) 0.000625 1130. 1326.
1477(41) 0.000595 1130. 1385.
1421(40) 0.000625 1130. 1434.
1395(40) 0.000625 1130. 1449.
1396(40) 0.000625 1129. 1421.
1418(40) 0.000625 1129. 1363.
1304(39) 0.000657 1129. 1300.
1233(38) 0.000693 1129. 1246.
1265(38) 0.000693 1128. 1209.
1200(37) 0.000730 1128. 1186.
1149(36) 0.000772 1128. 1174.
1141(36) 0.000772 1128. 1170.
1133(36) 0.000772 1127. 1170.
1170(37) 0.000730 1127. 1175.
1188(37) 0.000730 1127. 1187.
1205(37) 0.000730 1126. 1210.
1223(37) 0.000730 1126. 1251.
1313(39) 0.000657 1126. 1316.
1410(40) 0.000625 1126. 1405.
1611(41) 0.000595 1125. 1508.
1657(41) 0.000595 1125. 1600.
1762(43) 0.000541 1125. 1646.
1714(42) 0.000567 1125. 1623.
1557(40) 0.000625 1124. 1546.
1495(39) 0.000657 1124. 1456.
1424(38) 0.000693 1124. 1386.
1302(37) 0.000730 1124. 1355.
1320(37) 0.000730 1123. 1363.
1373(38) 0.000693 1123. 1399.
1398(38) 0.000693 1123. 1441.
1433(38) 0.000693 1123. 1461.
1390(38) 0.000693 1122. 1441.
1366(38) 0.000693 1122. 1387.
1345(37) 0.000730 1122. 1320.
1210(35) 0.000816 1121.5 1260.1
1189(35) 0.000816 1121.3 1214.6
1161(35) 0.000816 1121.0 1184.4
1198(35) 0.000816 1120.7 1166.6
1110(34) 0.000865 1120.5 1156.7
1180(35) 0.000816 1120.2 1151.4
1176(35) 0.000816 1120.0 1148.6
1142(34) 0.000865 1119.7 1147.4
1163(35) 0.000816 1119.4 1147.7
1101(34) 0.000865 1119.2 1149.6
1185(35) 0.000816 1118.9 1153.4
1168(35) 0.000816 1118.7 1159.0
1161(35) 0.000816 1118.4 1166.0
1145(34) 0.000865 1118.1 1173.3
1152(35) 0.000816 1117.9 1179.4
1219(36) 0.000772 1118. 1185.
1229(36) 0.000772 1117. 1192.
1238(36) 0.000772 1117. 1209.
1315(37) 0.000730 1117. 1241.
1310(37) 0.000730 1117. 1293.
1317(37) 0.000730 1116. 1365.
1472(39) 0.000657 1116. 1445.
1556(40) 0.000625 1116. 1514.
1584(40) 0.000625 1116. 1545.
1537(40) 0.000625 1115. 1523.
1491(39) 0.000657 1115. 1467.
1421(38) 0.000693 1115. 1412.
1413(38) 0.000693 1115. 1382.
1305(37) 0.000730 1114. 1389.
1382(38) 0.000693 1114. 1426.
1417(38) 0.000693 1114. 1474.
1422(38) 0.000693 1113. 1503.
1469(39) 0.000657 1113. 1487.
1433(38) 0.000693 1113. 1428.
1370(38) 0.000693 1113. 1353.
1314(37) 0.000730 1112. 1284.
1271(36) 0.000772 1112. 1232.
1227(36) 0.000772 1112. 1198.
1117(34) 0.000865 1111.7 1179.9
1123(34) 0.000865 1111.4 1171.0
1109(34) 0.000865 1111.2 1166.0
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1155(35) 0.000816 1109.6 1167.1
1263(36) 0.000772 1109. 1178.
1251(36) 0.000772 1109. 1187.
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1206(35) 0.000816 1107.3 1264.9
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1190(35) 0.000816 1106.8 1330.0
1301(37) 0.000730 1107. 1330.
1247(36) 0.000772 1106. 1304.
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1250(36) 0.000772 1106. 1228.
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1175(35) 0.000816 1104.5 1183.8
1221(36) 0.000772 1104. 1178.
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1232(34) 0.000865 1099.4 1223.3
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1390(37) 0.000730 1099. 1365.
1550(39) 0.000657 1099. 1471.
1588(39) 0.000657 1098. 1585.
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1829(42) 0.000567 1096. 1853.
1920(43) 0.000541 1096. 1994.
1972(44) 0.000517 1096. 2075.
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1918(43) 0.000541 1095. 1911.
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1641(40) 0.000625 1095. 1574.
1495(38) 0.000693 1095. 1451.
1409(37) 0.000730 1094. 1375.
1369(36) 0.000772 1094. 1336.
1310(36) 0.000772 1094. 1316.
1263(35) 0.000816 1093.6 1298.7
1237(35) 0.000816 1093.3 1272.8
1255(35) 0.000816 1093.1 1241.3
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1314(36) 0.000772 1090. 1267.
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1325(36) 0.000772 1089. 1334.
1307(36) 0.000772 1089. 1308.
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1120(33) 0.000918 1086.1 1128.1
1140(33) 0.000918 1085.9 1124.1
1132(33) 0.000918 1085.6 1123.2
1109(33) 0.000918 1085.4 1125.6
1082(32) 0.000977 1085.2 1132.1
1139(33) 0.000918 1084.9 1144.3
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1147(33) 0.000918 1084.4 1194.9
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1202(34) 0.000865 1083.9 1279.7
1259(35) 0.000816 1083.7 1323.7
1309(36) 0.000772 1083. 1354.
1234(35) 0.000816 1083.2 1362.8
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1251(35) 0.000816 1082.7 1351.5
1299(35) 0.000816 1082.5 1365.3
1389(37) 0.000730 1082. 1405.
1446(37) 0.000730 1082. 1466.
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1426(37) 0.000730 1081. 1445.
1401(37) 0.000730 1081. 1363.
1294(35) 0.000816 1080.3 1295.2
1233(35) 0.000816 1080.1 1248.2
1198(34) 0.000865 1079.9 1219.9
1178(34) 0.000865 1079.6 1203.4
1194(34) 0.000865 1079.4 1190.7
1116(33) 0.000918 1079.1 1177.1
1123(33) 0.000918 1078.9 1162.6
1130(33) 0.000918 1078.7 1149.4
1084(32) 0.000977 1078.4 1139.1
1068(32) 0.000977 1078.2 1132.4
1081(32) 0.000977 1078.0 1129.1
1144(33) 0.000918 1077.7 1128.6
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1097(33) 0.000918 1077.3 1135.3
1190(34) 0.000865 1077.0 1143.2
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1232(35) 0.000816 1076.6 1181.7
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1247(35) 0.000816 1076.1 1243.2
1295(35) 0.000816 1075.9 1270.2
1357(36) 0.000772 1076. 1282.
1310(36) 0.000772 1075. 1275.
1275(34) 0.000865 1075.2 1253.8
1253(33) 0.000918 1074.9 1230.2
1244(33) 0.000918 1074.7 1212.3
1253(33) 0.000918 1074.5 1203.6
1224(33) 0.000918 1074.2 1204.1
1232(33) 0.000918 1074.0 1210.4
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1225(33) 0.000918 1073.6 1226.6
1242(33) 0.000918 1073.3 1239.5
1282(34) 0.000865 1073.1 1264.4
1328(34) 0.000865 1072.9 1306.2
1394(35) 0.000816 1072.6 1364.5
1477(36) 0.000772 1072. 1431.
1449(36) 0.000772 1072. 1489.
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1462(36) 0.000772 1072. 1494.
1439(36) 0.000772 1072. 1435.
1408(35) 0.000816 1071.3 1360.2
1330(34) 0.000865 1071.1 1287.9
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1190(32) 0.000977 1069.3 1183.2
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1319(34) 0.000865 1068.4 1292.6
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1348(35) 0.000816 1067.9 1292.9
1302(34) 0.000865 1067.7 1291.2
1326(34) 0.000865 1067.5 1300.6
1356(35) 0.000816 1067.3 1323.9
1302(34) 0.000865 1067.1 1358.1
1381(35) 0.000816 1066.9 1394.3
1389(35) 0.000816 1066.6 1420.5
1361(35) 0.000816 1066.4 1431.6
1436(36) 0.000772 1066. 1438.
1479(36) 0.000772 1066. 1456.
1561(37) 0.000730 1066. 1498.
1615(38) 0.000693 1066. 1566.
1698(39) 0.000657 1065. 1649.
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1770(40) 0.000625 1065. 1747.
1846(40) 0.000625 1065. 1711.
1760(39) 0.000657 1064. 1626.
1641(38) 0.000693 1064. 1525.
1471(36) 0.000772 1064. 1433.
1477(36) 0.000772 1064. 1361.
1350(35) 0.000816 1063.6 1313.4
1252(33) 0.000918 1063.4 1282.4
1194(32) 0.000977 1063.2 1257.8
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1121(31) 0.001041 1062.0 1116.4
1086(31) 0.001041 1061.8 1106.0
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1105(31) 0.001041 1060.1 1098.1
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1131(32) 0.000977 1059.5 1120.8
1152(32) 0.000977 1059.3 1136.6
1159(32) 0.000977 1059.1 1157.0
1193(32) 0.000977 1058.9 1179.8
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1194(32) 0.000977 1058.3 1214.3
1242(33) 0.000918 1058.1 1199.9
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1154(32) 0.000977 1057.7 1153.3
1171(32) 0.000977 1057.5 1131.8
1171(32) 0.000977 1057.3 1114.9
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1115(31) 0.001041 1056.9 1096.2
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1087(31) 0.001041 1056.6 1092.9
1118(31) 0.001041 1056.4 1095.2
1084(31) 0.001041 1056.2 1099.8
1108(31) 0.001041 1056.0 1106.5
1115(31) 0.001041 1055.8 1115.1
1135(32) 0.000977 1055.6 1127.0
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1128(32) 0.000977 1055.2 1164.9
1203(33) 0.000918 1055.0 1196.8
1195(32) 0.000977 1054.8 1241.6
1277(34) 0.000865 1054.6 1300.1
1324(34) 0.000865 1054.5 1368.4
1362(35) 0.000816 1054.3 1436.6
1330(47) 0.000453 1054. 1488.
1420(34) 0.000865 1053.9 1504.1
1407(34) 0.000865 1053.7 1478.8
1361(33) 0.000918 1053.5 1424.4
1315(33) 0.000918 1053.3 1360.4
1233(32) 0.000977 1053.2 1301.4
1197(31) 0.001041 1053.0 1254.8
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1136(31) 0.001041 1052.6 1199.8
1158(31) 0.001041 1052.4 1184.1
1167(31) 0.001041 1052.2 1172.1
1147(31) 0.001041 1052.1 1163.8
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1182(31) 0.001041 1051.5 1166.1
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1205(31) 0.001041 1051.2 1175.6
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1149(31) 0.001041 1050.8 1167.3
1158(31) 0.001041 1050.6 1159.8
1140(31) 0.001041 1050.5 1154.4
1147(31) 0.001041 1050.3 1153.1
1106(30) 0.001111 1050.1 1156.1
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1108(30) 0.001111 1049.6 1181.3
1159(31) 0.001041 1049.4 1196.4
1175(31) 0.001041 1049.2 1219.2
1224(32) 0.000977 1049.1 1250.3
1270(32) 0.000977 1048.9 1287.2
1286(32) 0.000977 1048.7 1323.1
1320(33) 0.000918 1048.6 1346.7
1338(33) 0.000918 1048.4 1346.7
1303(33) 0.000918 1048.2 1322.1
1332(33) 0.000918 1048.1 1281.0
1201(31) 0.001041 1047.9 1234.4
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1054(29) 0.001189 1046.4 1077.5
1069(30) 0.001111 1046.2 1077.9
1055(29) 0.001189 1046.1 1080.2
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1156(31) 0.001041 1045.0 1184.3
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1193(31) 0.001041 1044.7 1210.7
1228(32) 0.000977 1044.5 1213.2
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1223(32) 0.000977 1044.2 1216.9
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1265(32) 0.000977 1043.9 1237.1
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1151(31) 0.001041 1042.5 1187.6
1151(31) 0.001041 1042.4 1186.2
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1252(32) 0.000977 1042.0 1185.5
1223(32) 0.000977 1041.8 1192.7
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1315(33) 0.000918 1041.0 1229.4
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1265(32) 0.000977 1040.1 1245.5
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1094(30) 0.001111 1036.5 1075.7
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1235(32) 0.000977 1035.5 1255.8
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1314(33) 0.000918 1035.3 1256.4
1305(33) 0.000918 1035.1 1257.9
1278(32) 0.000977 1035.0 1262.9
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1123(30) 0.001111 1034.0 1129.3
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1102(30) 0.001111 1033.7 1106.0
1088(30) 0.001111 1033.6 1104.6
1116(30) 0.001111 1033.5 1105.6
1077(30) 0.001111 1033.4 1108.3
1109(30) 0.001111 1033.3 1111.1
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1084(30) 0.001111 1033.1 1110.1
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1105(30) 0.001111 1032.8 1089.6
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1354(33) 0.000918 1030.2 1404.3
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1684(37) 0.000730 1030. 1740.
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1889(39) 0.000657 1030. 1899.
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1517(35) 0.000816 1029.3 1541.9
1370(34) 0.000865 1029.2 1483.4
1403(34) 0.000865 1029.1 1429.3
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1326(33) 0.000918 1029.0 1326.9
1302(33) 0.000918 1028.9 1282.4
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1154(31) 0.001041 1027.7 1150.2
1213(31) 0.001041 1027.7 1164.1
1184(31) 0.001041 1027.6 1173.3
1211(31) 0.001041 1027.5 1175.1
1179(31) 0.001041 1027.5 1169.4
1188(31) 0.001041 1027.4 1158.6
1183(31) 0.001041 1027.3 1145.8
1207(31) 0.001041 1027.3 1133.3
1142(31) 0.001041 1027.2 1122.1
1126(30) 0.001111 1027.1 1112.4
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1125(30) 0.001111 1026.9 1079.7
1075(30) 0.001111 1026.8 1074.0
1071(30) 0.001111 1026.7 1070.1
1071(30) 0.001111 1026.7 1068.0
1094(30) 0.001111 1026.6 1067.9
1105(30) 0.001111 1026.5 1070.2
1028(29) 0.001189 1026.5 1074.6
1029(29) 0.001189 1026.4 1081.1
1091(30) 0.001111 1026.4 1089.4
1124(30) 0.001111 1026.3 1098.9
1134(30) 0.001111 1026.2 1109.2
1160(31) 0.001041 1026.2 1118.9
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1192(31) 0.001041 1026.1 1136.2
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1194(31) 0.001041 1025.9 1166.0
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1197(31) 0.001041 1025.5 1177.9
1166(31) 0.001041 1025.5 1174.9
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1187(31) 0.001041 1025.4 1174.5
1159(31) 0.001041 1025.3 1175.5
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1194(31) 0.001041 1025.2 1178.7
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1148(31) 0.001041 1025.1 1189.4
1141(31) 0.001041 1025.0 1198.0
1184(31) 0.001041 1025.0 1207.1
1182(31) 0.001041 1024.9 1214.1
1152(31) 0.001041 1024.9 1218.2
1188(31) 0.001041 1024.8 1220.2
1226(32) 0.000977 1024.8 1221.7
1221(32) 0.000977 1024.7 1224.1
1222(32) 0.000977 1024.7 1227.0
1253(32) 0.000977 1024.6 1228.2
1182(31) 0.001041 1024.6 1224.6
1192(31) 0.001041 1024.5 1214.0
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1157(31) 0.001041 1024.4 1175.7
1166(31) 0.001041 1024.4 1153.9
1112(30) 0.001111 1024.3 1133.9
1096(30) 0.001111 1024.3 1117.6
1073(30) 0.001111 1024.2 1105.7
1059(29) 0.001189 1024.2 1098.7
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1126(30) 0.001111 1023.9 1115.3
1101(30) 0.001111 1023.9 1119.6
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977(28) 0.001276 1023.6 1087.5
1044(29) 0.001189 1023.5 1087.7
1091(30) 0.001111 1023.5 1091.4
1101(30) 0.001111 1023.4 1098.3
1092(30) 0.001111 1023.4 1108.6
1129(30) 0.001111 1023.3 1121.7
1134(30) 0.001111 1023.3 1137.3
1140(31) 0.001041 1023.2 1154.4
1154(31) 0.001041 1023.2 1172.1
1195(31) 0.001041 1023.1 1190.3
1222(32) 0.000977 1023.1 1209.8
1239(32) 0.000977 1023.1 1231.4
1228(32) 0.000977 1023.0 1255.6
1290(32) 0.000977 1023.0 1281.7
1280(32) 0.000977 1022.9 1307.5
1275(32) 0.000977 1022.9 1329.8
1308(33) 0.000918 1022.8 1346.8
1354(33) 0.000918 1022.8 1358.9
1390(47) 0.000453 1023. 1369.
1433(33) 0.000918 1022.7 1378.0
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1364(32) 0.000977 1022.6 1391.6
1466(34) 0.000865 1022.6 1387.8
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1259(31) 0.001041 1022.4 1260.8
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1163(30) 0.001111 1022.3 1150.9
1094(29) 0.001189 1022.3 1125.7
1127(29) 0.001189 1022.2 1106.9
1097(29) 0.001189 1022.2 1093.5
1047(28) 0.001276 1022.1 1084.9
1111(29) 0.001189 1022.1 1080.3
1077(29) 0.001189 1022.1 1079.0
1085(29) 0.001189 1022.0 1080.8
1055(29) 0.001189 1022.0 1085.2
1061(29) 0.001189 1021.9 1092.3
1091(29) 0.001189 1021.9 1101.9
1088(29) 0.001189 1021.9 1113.8
1079(29) 0.001189 1021.8 1127.6
1130(30) 0.001111 1021.8 1142.8
1124(29) 0.001189 1021.7 1158.4
1143(30) 0.001111 1021.7 1173.3
1185(30) 0.001111 1021.7 1187.1
1199(30) 0.001111 1021.6 1200.3
1190(30) 0.001111 1021.6 1213.3
1226(31) 0.001041 1021.5 1226.3
1224(31) 0.001041 1021.5 1238.0
1232(31) 0.001041 1021.5 1246.1
1255(31) 0.001041 1021.4 1247.8
1296(32) 0.000977 1021.4 1242.1
1233(31) 0.001041 1021.3 1230.0
1214(31) 0.001041 1021.3 1215.1
1247(31) 0.001041 1021.3 1201.3
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1178(30) 0.001111 1021.2 1189.8
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1232(31) 0.001041 1021.1 1238.5
1262(31) 0.001041 1021.0 1271.8
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1445(33) 0.000918 1020.9 1348.0
1405(33) 0.000918 1020.9 1380.4
1417(33) 0.000918 1020.9 1400.3
1422(33) 0.000918 1020.8 1403.7
1387(33) 0.000918 1020.8 1390.2
1413(33) 0.000918 1020.7 1365.0
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1309(32) 0.000977 1020.7 1304.7
1281(31) 0.001041 1020.6 1279.1
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1238(31) 0.001041 1020.5 1248.2
1228(31) 0.001041 1020.5 1244.3
1226(31) 0.001041 1020.5 1247.9
1266(31) 0.001041 1020.4 1258.4
1242(31) 0.001041 1020.4 1273.9
1292(32) 0.000977 1020.3 1291.7
1315(32) 0.000977 1020.3 1308.6
1332(32) 0.000977 1020.3 1321.8
1358(32) 0.000977 1020.2 1330.6
1316(32) 0.000977 1020.2 1335.7
1337(32) 0.000977 1020.1 1339.2
1363(32) 0.000977 1020.1 1342.1
1346(32) 0.000977 1020.1 1343.8
1302(32) 0.000977 1020.0 1342.0
1286(31) 0.001041 1020.0 1334.3
1269(31) 0.001041 1019.9 1320.0
1268(31) 0.001041 1019.9 1300.6
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1231(31) 0.001041 1019.8 1239.0
1182(30) 0.001111 1019.7 1222.4
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1195(30) 0.001111 1019.6 1195.0
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1191(30) 0.001111 1019.6 1175.1
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1119(29) 0.001189 1019.4 1158.3
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1162(30) 0.001111 1019.3 1138.0
1134(30) 0.001111 1019.3 1129.2
1141(30) 0.001111 1019.2 1120.7
1149(30) 0.001111 1019.2 1112.7
1165(30) 0.001111 1019.1 1105.3
1148(30) 0.001111 1019.1 1098.4
1127(29) 0.001189 1019.0 1091.8
1158(30) 0.001111 1019.0 1085.6
1095(29) 0.001189 1018.9 1080.0
1107(29) 0.001189 1018.9 1075.3
1070(29) 0.001189 1018.9 1071.7
1089(29) 0.001189 1018.8 1069.3
1101(29) 0.001189 1018.8 1068.2
1087(29) 0.001189 1018.7 1068.8
1106(29) 0.001189 1018.7 1071.1
1054(29) 0.001189 1018.6 1075.6
1097(29) 0.001189 1018.6 1082.8
1065(29) 0.001189 1018.5 1092.6
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1111(29) 0.001189 1018.4 1143.6
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1288(32) 0.000977 1018.2 1259.5
1339(32) 0.000977 1018.2 1289.8
1382(33) 0.000918 1018.1 1315.5
1368(33) 0.000918 1018.1 1334.6
1391(33) 0.000918 1018.0 1346.6
1410(33) 0.000918 1018.0 1353.4
1454(34) 0.000865 1017.9 1357.1
1435(33) 0.000918 1017.9 1358.6
1378(33) 0.000918 1017.8 1357.6
1358(32) 0.000977 1017.8 1352.7
1371(33) 0.000918 1017.7 1342.0
1358(32) 0.000977 1017.7 1325.5
1314(32) 0.000977 1017.6 1304.8
1317(32) 0.000977 1017.6 1282.5
1334(32) 0.000977 1017.5 1260.3
1250(31) 0.001041 1017.5 1239.3
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1133(30) 0.001111 1017.1 1141.7
1155(30) 0.001111 1017.0 1142.3
1134(30) 0.001111 1017.0 1148.1
1183(30) 0.001111 1016.9 1158.7
1160(30) 0.001111 1016.9 1173.4
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1166(30) 0.001111 1016.8 1209.3
1145(30) 0.001111 1016.7 1226.0
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1221(31) 0.001041 1016.6 1242.7
1195(30) 0.001111 1016.5 1239.1
1180(30) 0.001111 1016.5 1228.0
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1222(31) 0.001041 1016.4 1193.4
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1077(29) 0.001189 1015.8 1137.3
1162(30) 0.001111 1015.7 1154.2
1124(29) 0.001189 1015.6 1175.0
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1199(30) 0.001111 1015.5 1224.3
1179(30) 0.001111 1015.4 1249.0
1275(31) 0.001041 1015.4 1270.6
1256(31) 0.001041 1015.3 1286.8
1338(32) 0.000977 1015.2 1296.2
1299(32) 0.000977 1015.2 1299.7
1313(32) 0.000977 1015.1 1299.6
1312(32) 0.000977 1015.0 1298.9
1300(32) 0.000977 1015.0 1299.7
1324(32) 0.000977 1014.9 1303.5
1334(32) 0.000977 1014.8 1310.7
1350(32) 0.000977 1014.8 1321.4
1305(32) 0.000977 1014.7 1335.2
1376(33) 0.000918 1014.6 1351.8
1380(33) 0.000918 1014.6 1370.0
1357(32) 0.000977 1014.5 1387.2
1333(32) 0.000977 1014.4 1399.8
1327(32) 0.000977 1014.4 1404.3
1321(32) 0.000977 1014.3 1398.0
1343(32) 0.000977 1014.2 1381.3
1332(32) 0.000977 1014.2 1357.1
1320(32) 0.000977 1014.1 1329.8
1261(31) 0.001041 1014.0 1303.6
1252(31) 0.001041 1013.9 1281.4
1268(31) 0.001041 1013.9 1265.5
1204(31) 0.001041 1013.8 1256.7
1254(31) 0.001041 1013.7 1255.3
1260(31) 0.001041 1013.6 1260.3
1250(31) 0.001041 1013.6 1270.3
1287(32) 0.000977 1013.5 1282.5
1258(31) 0.001041 1013.4 1293.9
1278(31) 0.001041 1013.3 1300.8
1296(32) 0.000977 1013.3 1300.7
1270(31) 0.001041 1013.2 1292.7
1226(31) 0.001041 1013.1 1278.1
1257(31) 0.001041 1013.0 1259.3
1274(31) 0.001041 1013.0 1238.9
1247(31) 0.001041 1012.9 1218.7
1204(31) 0.001041 1012.8 1200.0
1160(30) 0.001111 1012.7 1183.1
1160(30) 0.001111 1012.6 1168.5
1174(30) 0.001111 1012.6 1156.5
1176(30) 0.001111 1012.5 1146.8
1095(30) 0.001111 1012.4 1139.3
1145(31) 0.001041 1012.3 1133.2
1178(31) 0.001041 1012.2 1127.9
1131(30) 0.001111 1012.1 1122.5
1088(30) 0.001111 1012.1 1116.7
1117(30) 0.001111 1012.0 1110.7
1144(31) 0.001041 1011.9 1105.0
1158(31) 0.001041 1011.8 1100.2
1148(31) 0.001041 1011.7 1096.8
1076(30) 0.001111 1011.6 1095.3
1103(30) 0.001111 1011.6 1095.7
1095(30) 0.001111 1011.5 1098.3
1092(30) 0.001111 1011.4 1102.7
1091(30) 0.001111 1011.3 1108.8
1133(30) 0.001111 1011.2 1115.8
1109(30) 0.001111 1011.1 1123.2
1166(31) 0.001041 1011.0 1130.1
1093(30) 0.001111 1010.9 1135.6
1210(32) 0.000977 1010.9 1139.4
1193(31) 0.001041 1010.8 1141.8
1141(31) 0.001041 1010.7 1143.4
1164(31) 0.001041 1010.6 1145.0
1158(31) 0.001041 1010.5 1147.3
1164(31) 0.001041 1010.4 1150.5
1176(31) 0.001041 1010.3 1155.1
1123(30) 0.001111 1010.2 1161.2
1154(31) 0.001041 1010.1 1169.4
1097(30) 0.001111 1010.0 1180.2
1194(31) 0.001041 1009.9 1193.9
1206(31) 0.001041 1009.8 1210.8
1171(31) 0.001041 1009.7 1230.4
1252(32) 0.000977 1009.6 1252.2
1324(33) 0.000918 1009.5 1275.4
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1384(34) 0.000865 1009.3 1347.3
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1416(34) 0.000865 1008.9 1387.2
1429(34) 0.000865 1008.8 1375.3
1406(34) 0.000865 1008.7 1356.7
1291(33) 0.000918 1008.6 1334.9
1379(34) 0.000865 1008.5 1313.3
1362(33) 0.000918 1008.4 1294.1
1299(33) 0.000918 1008.2 1279.3
1265(32) 0.000977 1008.1 1269.0
1255(32) 0.000977 1008.0 1263.5
1220(32) 0.000977 1007.9 1262.5
1228(32) 0.000977 1007.8 1264.9
1260(32) 0.000977 1007.7 1269.0
1239(32) 0.000977 1007.6 1272.3
1281(32) 0.000977 1007.5 1272.6
1265(32) 0.000977 1007.4 1267.9
1260(32) 0.000977 1007.3 1257.5
1288(33) 0.000918 1007.2 1242.5
1271(32) 0.000977 1007.1 1224.2
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1177(31) 0.001041 1006.8 1165.0
1158(31) 0.001041 1006.6 1147.1
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1155(31) 0.001041 1006.4 1117.1
1136(31) 0.001041 1006.3 1105.6
1110(30) 0.001111 1006.2 1096.8
1129(30) 0.001111 1006.1 1090.7
1109(30) 0.001111 1006.0 1087.2
1083(30) 0.001111 1005.9 1086.0
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1069(30) 0.001111 1005.6 1089.9
1069(30) 0.001111 1005.5 1094.2
1112(30) 0.001111 1005.4 1099.6
1097(30) 0.001111 1005.3 1105.3
1105(30) 0.001111 1005.2 1110.9
1107(30) 0.001111 1005.1 1115.8
1087(30) 0.001111 1004.9 1119.9
1123(30) 0.001111 1004.8 1123.2
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1089(30) 0.001111 1004.6 1128.7
1106(30) 0.001111 1004.5 1131.5
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1123(30) 0.001111 1004.2 1137.9
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1179(31) 0.001041 1004.0 1146.6
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1155(31) 0.001041 1003.6 1172.4
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1214(32) 0.000977 1003.4 1201.4
1236(32) 0.000977 1003.2 1219.1
1251(32) 0.000977 1003.1 1238.3
1231(32) 0.000977 1003.0 1258.5
1322(33) 0.000918 1002.9 1278.6
1306(33) 0.000918 1002.7 1297.2
1283(32) 0.000977 1002.6 1312.4
1321(33) 0.000918 1002.5 1322.2
1339(33) 0.000918 1002.4 1325.6
1279(32) 0.000977 1002.2 1322.7
1309(33) 0.000918 1002.1 1315.0
1226(32) 0.000977 1002.0 1304.2
1346(33) 0.000918 1001.8 1292.1
1325(33) 0.000918 1001.7 1279.9
1255(32) 0.000977 1001.6 1268.1
1272(33) 0.000918 1001.5 1257.1
1188(31) 0.001041 1001.3 1247.2
1226(32) 0.000977 1001.2 1238.7
1287(33) 0.000918 1001.1 1231.9
1173(31) 0.001041 1000.9 1226.2
1229(32) 0.000977 1000.8 1221.1
1207(32) 0.000977 1000.7 1215.8
1223(32) 0.000977 1000.5 1209.4
1228(32) 0.000977 1000.4 1201.5
1198(32) 0.000977 1000.3 1192.4
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1271(33) 0.000918 1000.0 1171.9
1193(32) 0.000977 999.8 1161.2
1153(31) 0.001041 999.7 1150.1
1160(31) 0.001041 999.6 1138.6
1123(31) 0.001041 999.4 1126.8
1128(31) 0.001041 999.3 1115.0
1055(30) 0.001111 999.2 1103.7
1069(30) 0.001111 999.0 1093.1
1031(29) 0.001189 998.9 1083.8
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1112(30) 0.001111 962.5 1126.6
1142(30) 0.001111 962.4 1125.2
1105(29) 0.001189 962.3 1123.7
1062(29) 0.001189 962.2 1122.2
1101(29) 0.001189 962.1 1120.8
1134(30) 0.001111 962.0 1119.4
1104(29) 0.001189 961.9 1118.3
1065(29) 0.001189 961.9 1117.3
1114(30) 0.001111 961.8 1116.6
1136(30) 0.001111 961.7 1116.1
1107(29) 0.001189 961.6 1116.0
1099(29) 0.001189 961.5 1116.3
1096(29) 0.001189 961.5 1116.9
1084(29) 0.001189 961.4 1118.0
1109(29) 0.001189 961.3 1119.5
1117(30) 0.001111 961.2 1121.5
1103(29) 0.001189 961.2 1123.9
1087(30) 0.001111 961.1 1126.8
1099(30) 0.001111 961.0 1130.1
1186(31) 0.001041 960.9 1134.0
1126(30) 0.001111 960.9 1138.3
1091(30) 0.001111 960.8 1143.0
1136(30) 0.001111 960.7 1148.2
1153(31) 0.001041 960.7 1153.8
1178(31) 0.001041 960.6 1159.9
1161(31) 0.001041 960.6 1166.4
1160(31) 0.001041 960.5 1173.2
1123(30) 0.001111 960.4 1180.4
1161(31) 0.001041 960.4 1187.8
1161(31) 0.001041 960.3 1195.6
1165(31) 0.001041 960.3 1203.5
1207(31) 0.001041 960.2 1211.7
1188(31) 0.001041 960.2 1219.9
1202(31) 0.001041 960.1 1228.2
1227(31) 0.001041 960.1 1236.5
1210(31) 0.001041 960.0 1244.7
1208(31) 0.001041 960.0 1252.7
1236(32) 0.000977 959.9 1260.5
1199(31) 0.001041 959.9 1268.0
1267(32) 0.000977 959.9 1275.1
1304(32) 0.000977 959.8 1281.8
1296(32) 0.000977 959.8 1288.0
1302(32) 0.000977 959.8 1293.7
1302(32) 0.000977 959.7 1298.7
1247(32) 0.000977 959.7 1303.1
1209(31) 0.001041 959.7 1306.9
1249(32) 0.000977 959.7 1310.1
1310(32) 0.000977 959.6 1312.6
1322(33) 0.000918 959.6 1314.5
1307(32) 0.000977 959.6 1315.7
1303(32) 0.000977 959.6 1316.4
1335(33) 0.000918 959.6 1316.5
1319(33) 0.000918 959.6 1316.0
1294(32) 0.000977 959.6 1315.0
1299(32) 0.000977 959.6 1313.5
1310(32) 0.000977 959.6 1311.5
1262(32) 0.000977 959.6 1309.1
1283(32) 0.000977 959.6 1306.2
1320(33) 0.000918 959.6 1303.0
1348(33) 0.000918 959.6 1299.4
1341(33) 0.000918 959.6 1295.4
1286(32) 0.000977 959.7 1291.2
1292(32) 0.000977 959.7 1286.7
1307(32) 0.000977 959.7 1282.0
1260(32) 0.000977 959.7 1277.0
1267(32) 0.000977 959.8 1271.9
1232(32) 0.000977 959.8 1266.6
1276(32) 0.000977 959.8 1261.3
1229(31) 0.001041 959.9 1255.8
1222(31) 0.001041 959.9 1250.3
1238(32) 0.000977 960.0 1244.8
1262(32) 0.000977 960.0 1239.3
1242(32) 0.000977 960.1 1233.9
1236(32) 0.000977 960.1 1228.6
1223(31) 0.001041 960.2 1223.4
1213(31) 0.001041 960.3 1218.3
1249(32) 0.000977 960.4 1213.4
1195(31) 0.001041 960.4 1208.8
1242(32) 0.000977 960.5 1204.3
1192(31) 0.001041 960.6 1200.0
1196(31) 0.001041 960.7 1196.0
1204(31) 0.001041 960.8 1192.3
1183(31) 0.001041 960.9 1188.8
1143(30) 0.001111 961.0 1185.6
1160(31) 0.001041 961.1 1182.6
1202(31) 0.001041 961.2 1179.9
1178(31) 0.001041 961.3 1177.4
1197(31) 0.001041 961.4 1175.2
1163(31) 0.001041 961.6 1173.3
1154(31) 0.001041 961.7 1171.6
1124(30) 0.001111 961.8 1170.2
1169(31) 0.001041 962.0 1169.1
1164(31) 0.001041 962.1 1168.3
1104(30) 0.001111 962.2 1167.7
1167(31) 0.001041 962.4 1167.5
1111(30) 0.001111 962.6 1167.6
1165(31) 0.001041 962.7 1168.0
1189(31) 0.001041 962.9 1168.8
1182(31) 0.001041 963.1 1170.0
1157(31) 0.001041 963.2 1171.5
1158(31) 0.001041 963.4 1173.5
1181(31) 0.001041 963.6 1175.8
1219(31) 0.001041 963.8 1178.6
1231(32) 0.000977 964.0 1181.8
1214(31) 0.001041 964.2 1185.4
1181(31) 0.001041 964.4 1189.4
1220(31) 0.001041 964.7 1193.9
1218(31) 0.001041 964.9 1198.7
1211(31) 0.001041 965.1 1203.9
1234(32) 0.000977 965.3 1209.5
1237(32) 0.000977 965.6 1215.4
1218(31) 0.001041 965.8 1221.6
1238(32) 0.000977 966.1 1228.0
1240(32) 0.000977 966.4 1234.7
1277(32) 0.000977 966.6 1241.6
1254(32) 0.000977 966.9 1248.6
1248(32) 0.000977 967.2 1255.7
1256(32) 0.000977 967.5 1262.9
1254(32) 0.000977 967.8 1270.1
1306(33) 0.000918 968.1 1277.2
1294(32) 0.000977 968.4 1284.2
1280(32) 0.000977 968.7 1291.0
1320(33) 0.000918 969.0 1297.6
1341(33) 0.000918 969.3 1303.9
1350(33) 0.000918 969.7 1309.8
1324(33) 0.000918 970.0 1315.4
1342(33) 0.000918 970.4 1320.5
1316(33) 0.000918 970.7 1325.1
1308(33) 0.000918 971.1 1329.3
1334(33) 0.000918 971.5 1332.9
1354(33) 0.000918 971.8 1335.9
1296(32) 0.000977 972.2 1338.5
1336(33) 0.000918 972.6 1340.5
1358(33) 0.000918 973.0 1342.0
1334(33) 0.000918 973.5 1343.0
1348(33) 0.000918 973.9 1343.5
1385(34) 0.000865 974.3 1343.7
1373(33) 0.000918 974.7 1343.5
1381(33) 0.000918 975.2 1342.9
1339(33) 0.000918 975.6 1342.0
1356(33) 0.000918 976.1 1340.9
1365(33) 0.000918 976.6 1339.5
1336(33) 0.000918 977.0 1337.9
1351(33) 0.000918 977.5 1336.0
1334(33) 0.000918 978.0 1334.0
1343(33) 0.000918 978.5 1331.9
1328(33) 0.000918 979.1 1329.5
1318(33) 0.000918 979.6 1327.0
1300(33) 0.000918 980.1 1324.4
1299(33) 0.000918 980.7 1321.6
1304(33) 0.000918 981.2 1318.7
1301(33) 0.000918 981.8 1315.6
1319(33) 0.000918 982.3 1312.3
1328(33) 0.000918 982.9 1308.9
1307(33) 0.000918 983.5 1305.4
1286(32) 0.000977 984.1 1301.6
1279(32) 0.000977 984.7 1297.8
1297(33) 0.000918 985.3 1293.8
1253(32) 0.000977 986.0 1289.6
1253(32) 0.000977 986.6 1285.4
1265(32) 0.000977 987.3 1281.1
1263(32) 0.000977 987.9 1276.7
1275(32) 0.000977 988.6 1272.2
1262(32) 0.000977 989.3 1267.7
1256(32) 0.000977 990.0 1263.2
1233(32) 0.000977 990.7 1258.7
1217(32) 0.000977 991.4 1254.3
1298(32) 0.000977 992.1 1249.9
1274(32) 0.000977 992.8 1245.5
1260(32) 0.000977 993.6 1241.2
1287(32) 0.000977 994.3 1237.0
1308(33) 0.000918 995.1 1232.9
1230(32) 0.000977 995.9 1228.9
1216(32) 0.000977 996.7 1225.0
1201(31) 0.001041 997.5 1221.2
1240(32) 0.000977 998.3 1217.5
1216(32) 0.000977 999.1 1213.9
1262(32) 0.000977 1000.0 1210.4
1216(32) 0.000977 1000.8 1207.0
1215(32) 0.000977 1001.7 1203.8
1235(32) 0.000977 1002.5 1200.6
1218(32) 0.000977 1003.4 1197.5
1232(32) 0.000977 1004.3 1194.5
1185(31) 0.001041 1005.2 1191.6
1168(31) 0.001041 1006.2 1188.8
1191(31) 0.001041 1007.1 1186.2
1184(31) 0.001041 1008.1 1183.6
1204(31) 0.001041 1009.0 1181.1
1169(31) 0.001041 1010.0 1178.7
1167(31) 0.001041 1011.0 1176.5
1171(31) 0.001041 1012.0 1174.3
1195(31) 0.001041 1013.0 1172.3
1165(31) 0.001041 1014.0 1170.4
1139(31) 0.001041 1015.1 1168.7
1143(31) 0.001041 1016.1 1167.1
1149(31) 0.001041 1017.2 1165.7
1171(31) 0.001041 1018.3 1164.4
1172(31) 0.001041 1019.4 1163.3
1125(30) 0.001111 1020.5 1162.3
1166(31) 0.001041 1021.6 1161.6
1174(31) 0.001041 1022.8 1161.0
1156(31) 0.001041 1023.9 1160.6
1159(31) 0.001041 1025.1 1160.4
1158(31) 0.001041 1026.3 1160.4
1153(31) 0.001041 1027.5 1160.7
1176(31) 0.001041 1028.7 1161.1
1167(31) 0.001041 1029.9 1161.8
1231(32) 0.000977 1031.1 1162.7
1225(32) 0.000977 1032.4 1163.9
1184(31) 0.001041 1033.7 1165.2
1196(31) 0.001041 1035.0 1166.9
1197(31) 0.001041 1036.3 1168.7
1183(31) 0.001041 1037.6 1170.9
1217(32) 0.000977 1038.9 1173.2
1225(32) 0.000977 1040.3 1175.9
1178(31) 0.001041 1041.6 1178.7
1199(26) 0.001479 1043.0 1181.9
1241(32) 0.000977 1044.4 1185.2
1253(32) 0.000977 1045.8 1188.8
1234(32) 0.000977 1047.2 1192.7
1205(32) 0.000977 1048.7 1196.8
1209(32) 0.000977 1050.2 1201.0
1223(32) 0.000977 1051.6 1205.6
1228(32) 0.000977 1053.1 1210.3
1246(32) 0.000977 1054.6 1215.2
1234(32) 0.000977 1056.2 1220.3
1244(32) 0.000977 1057.7 1225.6
1242(32) 0.000977 1059.3 1231.0
1247(32) 0.000977 1060.9 1236.6
1259(32) 0.000977 1062.5 1242.3
1264(32) 0.000977 1064.1 1248.2
1243(32) 0.000977 1065.7 1254.1
1212(32) 0.000977 1067.4 1260.1
1228(32) 0.000977 1069.0 1266.2
1255(32) 0.000977 1070.7 1272.3
1271(33) 0.000918 1072.4 1278.5
1290(33) 0.000918 1074.2 1284.7
1331(33) 0.000918 1075.9 1290.8
1308(33) 0.000918 1077.7 1297.0
1307(33) 0.000918 1079.5 1303.1
1322(33) 0.000918 1081.3 1309.1
1319(33) 0.000918 1083.1 1315.0
1306(33) 0.000918 1084.9 1320.9
1310(33) 0.000918 1086.8 1326.6
1284(33) 0.000918 1088.6 1332.2
1274(33) 0.000918 1090.5 1337.7
1307(33) 0.000918 1092.4 1343.1
1318(33) 0.000918 1094.4 1348.2
1330(33) 0.000918 1096.3 1353.3
1325(33) 0.000918 1098.3 1358.1
1347(33) 0.000918 1100.3 1362.8
1398(34) 0.000865 1102.3 1367.3
1364(34) 0.000865 1104.3 1371.6
1351(33) 0.000918 1106.4 1375.7
1396(34) 0.000865 1108.5 1379.6
1416(34) 0.000865 1110.6 1383.4
1398(34) 0.000865 1112.7 1386.9
1366(34) 0.000865 1114.8 1390.2
1425(34) 0.000865 1117.0 1393.4
1492(35) 0.000816 1119.2 1396.4
1432(34) 0.000865 1121.3 1399.2
1433(34) 0.000865 1123.6 1401.9
1436(34) 0.000865 1125.8 1404.4
1381(34) 0.000865 1128.1 1406.8
1376(34) 0.000865 1130.4 1409.0
1424(34) 0.000865 1132.7 1411.2
1449(35) 0.000816 1135.0 1413.2
1436(34) 0.000865 1137.3 1415.2
1439(34) 0.000865 1139.7 1417.1
1416(34) 0.000865 1142.1 1418.9
1408(34) 0.000865 1144.5 1420.6
1424(34) 0.000865 1147.0 1422.4
1436(34) 0.000865 1149.4 1424.0
1462(35) 0.000816 1151.9 1425.7
1460(35) 0.000816 1154.4 1427.3
1431(34) 0.000865 1156.9 1428.8
1434(34) 0.000865 1159.5 1430.4
1415(34) 0.000865 1162.1 1431.9
1414(34) 0.000865 1164.7 1433.4
1453(35) 0.000816 1167.3 1434.9
1416(34) 0.000865 1169.9 1436.3
1400(34) 0.000865 1172.6 1437.6
1386(34) 0.000865 1175.3 1438.9
1402(34) 0.000865 1178.0 1440.2
1421(34) 0.000865 1180.8 1441.4
1439(34) 0.000865 1183.5 1442.5
1426(34) 0.000865 1186.3 1443.6
1374(34) 0.000865 1189.1 1444.5
1383(34) 0.000865 1192.0 1445.4
1399(34) 0.000865 1194.8 1446.2
1400(34) 0.000865 1197.7 1446.9
1404(34) 0.000865 1200.6 1447.6
1434(34) 0.000865 1203.6 1448.1
1432(34) 0.000865 1206.5 1448.6
1438(34) 0.000865 1209.5 1448.9
1440(34) 0.000865 1212.5 1449.2
1429(34) 0.000865 1215.6 1449.5
1458(35) 0.000816 1218.6 1449.7
1467(35) 0.000816 1221.7 1449.8
1429(34) 0.000865 1224.8 1449.9
1468(35) 0.000816 1228.0 1450.0
1538(36) 0.000772 1231. 1450.
1490(35) 0.000816 1234.3 1450.1
1465(35) 0.000816 1237.5 1450.1
1497(35) 0.000816 1240.8 1450.2
1456(35) 0.000816 1244.1 1450.3
1416(34) 0.000865 1247.4 1450.4
1444(35) 0.000816 1250.7 1450.6
1431(34) 0.000865 1254.0 1450.8
1436(34) 0.000865 1257.4 1451.0
1456(35) 0.000816 1260.8 1451.4
1428(34) 0.000865 1264.3 1451.7
1439(34) 0.000865 1267.7 1452.2
1451(35) 0.000816 1271.2 1452.7
1465(35) 0.000816 1274.7 1453.3
1439(34) 0.000865 1278.3 1454.0
1433(35) 0.000816 1281.8 1454.7
1461(36) 0.000772 1285. 1456.
1463(36) 0.000772 1289. 1457.
1417(35) 0.000816 1292.7 1457.5
1472(36) 0.000772 1296. 1459.
1416(35) 0.000816 1300.1 1459.8
1392(35) 0.000816 1303.8 1461.1
1431(35) 0.000816 1307.6 1462.5
1466(36) 0.000772 1311. 1464.
1515(36) 0.000772 1315. 1466.
1461(36) 0.000772 1319. 1467.
1404(35) 0.000816 1323.0 1469.1
1399(35) 0.000816 1326.9 1471.0
1443(35) 0.000816 1330.8 1473.0
1458(36) 0.000772 1335. 1475.
1475(36) 0.000772 1339. 1477.
1447(35) 0.000816 1342.8 1479.8
1482(36) 0.000772 1347. 1482.
1502(36) 0.000772 1351. 1485.
1491(36) 0.000772 1355. 1488.
1459(36) 0.000772 1359. 1491.
1506(36) 0.000772 1363. 1494.
1508(36) 0.000772 1368. 1497.
1432(35) 0.000816 1371.9 1500.3
1443(35) 0.000816 1376.2 1503.8
1459(36) 0.000772 1380. 1507.
1491(36) 0.000772 1385. 1511.
1452(35) 0.000816 1389.2 1515.3
1502(36) 0.000772 1394. 1519.
1520(36) 0.000772 1398. 1524.
1556(37) 0.000730 1402. 1528.
1566(37) 0.000730 1407. 1533.
1540(36) 0.000772 1411. 1538.
1503(36) 0.000772 1416. 1543.
1585(37) 0.000730 1421. 1548.
1591(37) 0.000730 1425. 1553.
1567(37) 0.000730 1430. 1559.
1542(36) 0.000772 1434. 1564.
1536(36) 0.000772 1439. 1570.
1616(37) 0.000730 1444. 1576.
1624(37) 0.000730 1449. 1582.
1634(37) 0.000730 1454. 1589.
1652(38) 0.000693 1458. 1595.
1619(37) 0.000730 1463. 1602.
1628(37) 0.000730 1468. 1608.
1643(37) 0.000730 1473. 1615.
1576(37) 0.000730 1478. 1622.
1629(37) 0.000730 1483. 1630.
1660(38) 0.000693 1488. 1637.
1658(38) 0.000693 1493. 1645.
1680(38) 0.000693 1498. 1652.
1629(37) 0.000730 1503. 1660.
1633(37) 0.000730 1509. 1668.
1649(38) 0.000693 1514. 1676.
1713(38) 0.000693 1519. 1684.
1756(39) 0.000657 1524. 1692.
1700(38) 0.000693 1529. 1701.
1715(38) 0.000693 1535. 1709.
1726(38) 0.000693 1540. 1717.
1733(38) 0.000693 1546. 1726.
1706(38) 0.000693 1551. 1735.
1763(39) 0.000657 1556. 1743.
1732(38) 0.000693 1562. 1752.
1765(39) 0.000657 1568. 1761.
1750(39) 0.000657 1573. 1770.
1783(39) 0.000657 1579. 1779.
1736(38) 0.000693 1584. 1788.
1826(39) 0.000657 1590. 1797.
1827(39) 0.000657 1596. 1805.
1881(40) 0.000625 1601. 1814.
1874(40) 0.000625 1607. 1823.
1842(40) 0.000625 1613. 1832.
1859(40) 0.000625 1619. 1841.
1891(40) 0.000625 1625. 1850.
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2602(66) . . .
2587(66) . . .
2518(65) . . .
2615(66) . . .
2538(66) . . .
2457(65) . . .
2501(65) . . .
2546(66) . . .
2516(65) . . .
2493(65) . . .
2584(66) . . .
2469(65) . . .
2515(65) . . .
2539(66) . . .
2628(67) . . .
2557(66) . . .
2621(67) . . .
2612(66) . . .
2572(66) . . .
2578(66) . . .
2603(66) . . .
2573(66) . . .
2654(67) . . .
2696(67) . . .
2610(66) . . .
2585(66) . . .
2681(67) . . .
2627(67) . . .
2715(68) . . .
2643(67) . . .
2757(68) . . .
2789(68) . . .
2707(68) . . .
2691(67) . . .
2637(67) . . .
_pd_meas_number_of_points        3296
_pd_proc_number_of_points        3296

_cell_measurement_reflns_used    643
_reflns_number_total             643
_reflns_limit_h_min              1
_reflns_limit_h_max              17
_reflns_limit_k_min              0
_reflns_limit_k_max              12
_reflns_limit_l_min              0
_reflns_limit_l_max              10
_reflns_d_resolution_high        1.056
_reflns_d_resolution_low         18.682
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
