# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_e:LiNaRbSO_CIF_LYQ
_database_code_depnum_ccdc_archive 'CCDC 1832967'
_audit_update_record             
;
2018-03-27 deposited with the CCDC.
2018-10-03 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'H4 Li8 Na O26 Rb3 S6'
_chemical_formula_weight         947.31

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   C2

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'

_cell_length_a                   29.838(6)
_cell_length_b                   4.9519(10)
_cell_length_c                   8.1859(16)
_cell_angle_alpha                90.00
_cell_angle_beta                 100.81(3)
_cell_angle_gamma                90.00
_cell_volume                     1188.1(4)
_cell_formula_units_Z            2
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    3209
_cell_measurement_theta_min      2.65
_cell_measurement_theta_max      25.24

_exptl_crystal_description       strip
_exptl_crystal_colour            colourless
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.648
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             908
_exptl_absorpt_coefficient_mu    6.813
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'ω scans'
_diffrn_measurement_method       'Bruker APEX-II CCD'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            7924
_diffrn_reflns_av_R_equivalents  0.0464
_diffrn_reflns_av_sigmaI/netI    0.0444
_diffrn_reflns_limit_h_min       -35
_diffrn_reflns_limit_h_max       35
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_theta_min         2.53
_diffrn_reflns_theta_max         25.07
_reflns_number_total             2104
_reflns_number_gt                1956
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.1015P)²+13.1174P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.25(2)
_refine_ls_number_reflns         2104
_refine_ls_number_parameters     182
_refine_ls_number_restraints     1
_refine_ls_R_factor_all          0.0611
_refine_ls_R_factor_gt           0.0570
_refine_ls_wR_factor_ref         0.1708
_refine_ls_wR_factor_gt          0.1668
_refine_ls_goodness_of_fit_ref   1.090
_refine_ls_restrained_S_all      1.090
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Rb1 Rb 0.5000 0.8832(3) 1.0000 0.0251(4) Uani 1 2 d S . .
Rb2 Rb 0.63192(4) 0.9100(3) 1.39260(16) 0.0487(4) Uani 1 1 d . . .
S1 S 0.46018(7) 0.3887(6) 0.6888(3) 0.0185(5) Uani 1 1 d . . .
S2 S 0.61505(7) 0.8839(6) 0.8531(3) 0.0183(5) Uani 1 1 d . . .
S3 S 0.78589(7) 0.8964(6) 1.7733(2) 0.0170(5) Uani 1 1 d . . .
Na1 Na 0.5000 -0.1569(15) 0.5000 0.074(3) Uani 1 2 d S . .
O1 O 0.4635(3) 0.0935(15) 0.6663(10) 0.0269(17) Uani 1 1 d . . .
O2 O 0.4317(2) 0.5047(14) 0.5378(9) 0.0224(16) Uani 1 1 d . . .
O3 O 0.5067(2) 0.5073(16) 0.7140(9) 0.0252(17) Uani 1 1 d . . .
O4 O 0.4400(2) 0.4539(15) 0.8289(9) 0.0275(18) Uani 1 1 d . . .
O5 O 0.5849(3) 1.0032(15) 0.7095(9) 0.0271(17) Uani 1 1 d . . .
O6 O 0.6056(2) 0.5901(14) 0.8561(9) 0.0213(15) Uani 1 1 d . . .
O7 O 0.6626(2) 0.9229(18) 0.8357(9) 0.0289(17) Uani 1 1 d . . .
O8 O 0.6079(3) 1.0039(15) 1.0087(10) 0.0285(18) Uani 1 1 d . . .
O9 O 0.8343(2) 0.9548(15) 1.7794(9) 0.0247(17) Uani 1 1 d . . .
O10 O 0.7784(2) 0.6005(15) 1.7780(9) 0.0224(16) Uani 1 1 d . . .
O11 O 0.7590(2) 1.0036(15) 1.6171(9) 0.0244(16) Uani 1 1 d . . .
O12 O 0.7697(2) 1.0149(14) 1.9163(9) 0.0226(16) Uani 1 1 d . . .
O13 O 0.68307(17) 0.3893(16) 1.6535(7) 0.0127(11) Uani 1 1 d . . .
Li1 Li 0.7833(5) 0.398(5) 1.9879(19) 0.025(3) Uiso 1 1 d . . .
H13A H 0.7115 0.3871 1.7126 0.030 Uiso 1 1 d R . .
H13B H 0.6647 0.3564 1.7242 0.030 Uiso 1 1 d R . .
Li2 Li 0.7391(5) 0.391(5) 1.611(2) 0.028(3) Uiso 1 1 d . . .
Li3 Li 0.6088(5) 1.385(5) 1.060(2) 0.028(3) Uiso 1 1 d . . .
Li4 Li 0.4334(5) 0.394(6) 0.3126(19) 0.025(3) Uiso 1 1 d . . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rb1 O1 2.936(8) 2_667 ?
Rb1 O1 2.936(8) 1_565 ?
Rb1 O4 2.957(7) . ?
Rb1 O4 2.957(7) 2_657 ?
Rb1 O3 3.027(8) . ?
Rb1 O3 3.027(8) 2_657 ?
Rb1 O8 3.261(8) . ?
Rb1 O8 3.261(8) 2_657 ?
Rb1 O4 3.494(8) 2_667 ?
Rb1 O4 3.494(8) 1_565 ?
Rb1 S1 3.572(3) . ?
Rb1 S1 3.572(3) 2_657 ?
Rb2 O2 2.893(7) 2_657 ?
Rb2 O9 2.935(8) 4_648 ?
Rb2 O1 2.940(8) 2_667 ?
Rb2 O8 3.125(8) . ?
Rb2 O5 3.206(8) 1_556 ?
Rb2 O9 3.288(8) 4_658 ?
Rb2 O13 3.362(7) 1_565 ?
Rb2 O10 3.377(8) 4_658 ?
Rb2 O4 3.397(8) 2_657 ?
Rb2 O13 3.510(7) . ?
Rb2 Li3 3.56(2) . ?
Rb2 O7 3.571(8) 1_556 ?
S1 O4 1.428(7) . ?
S1 O2 1.478(7) . ?
S1 O1 1.479(8) . ?
S1 O3 1.487(7) . ?
S1 Li4 3.033(15) . ?
S1 Na1 3.090(6) 1_565 ?
S1 Rb2 3.596(3) 2_647 ?
S1 Rb1 3.610(3) 1_545 ?
S1 Rb2 3.738(3) 2_657 ?
S2 O8 1.457(8) . ?
S2 O5 1.465(8) . ?
S2 O7 1.466(7) . ?
S2 O6 1.483(8) . ?
S2 Li4 3.01(3) 2_656 ?
S2 Li3 3.02(2) 1_545 ?
S2 Li3 3.03(2) . ?
S2 Rb2 3.898(3) 1_554 ?
S3 O9 1.465(7) . ?
S3 O12 1.469(7) . ?
S3 O11 1.476(7) . ?
S3 O10 1.483(8) . ?
S3 Li2 3.01(2) 1_565 ?
S3 Li1 3.04(2) . ?
S3 Li2 3.05(2) . ?
S3 Rb2 3.861(3) 4_648 ?
S3 Rb2 3.947(3) 4_658 ?
Na1 O1 2.266(9) 2_656 ?
Na1 O1 2.266(9) . ?
Na1 O3 2.396(9) 2_646 ?
Na1 O3 2.396(9) 1_545 ?
Na1 O2 2.700(9) 2_646 ?
Na1 O2 2.700(9) 1_545 ?
Na1 O5 2.891(8) 1_545 ?
Na1 O5 2.891(8) 2_646 ?
Na1 S1 3.090(6) 2_646 ?
Na1 S1 3.090(6) 1_545 ?
Na1 Li4 3.18(2) 2_646 ?
Na1 Li4 3.18(2) 1_545 ?
O1 Rb1 2.936(8) 1_545 ?
O1 Rb2 2.940(8) 2_647 ?
O2 Li4 1.932(18) . ?
O2 Na1 2.700(9) 1_565 ?
O2 Rb2 2.893(7) 2_657 ?
O2 Rb2 3.607(8) 2_647 ?
O3 Li4 1.925(18) 2_656 ?
O3 Na1 2.396(9) 1_565 ?
O4 Li3 1.887(18) 2_647 ?
O4 Rb2 3.397(8) 2_657 ?
O4 Rb1 3.494(8) 1_545 ?
O5 Li4 2.01(3) 2_666 ?
O5 Na1 2.891(8) 1_565 ?
O5 Rb2 3.206(8) 1_554 ?
O6 Li4 1.90(2) 2_656 ?
O6 Li3 1.94(2) 1_545 ?
O7 Li1 1.958(17) 4_658 ?
O7 Rb2 3.571(8) 1_554 ?
O8 Li3 1.93(3) . ?
O9 Li3 1.971(18) 4_648 ?
O9 Rb2 2.935(8) 4_658 ?
O9 Rb2 3.288(8) 4_648 ?
O10 Li2 1.93(2) . ?
O10 Li1 1.971(19) . ?
O10 Rb2 3.377(8) 4_648 ?
O11 Li2 1.957(19) 4_658 ?
O11 Li2 2.01(2) 1_565 ?
O12 Li1 1.978(18) 4_659 ?
O12 Li1 2.00(2) 1_565 ?
O13 Li2 1.771(17) . ?
O13 Rb2 3.362(7) 1_545 ?
Li1 O7 1.958(17) 4_648 ?
Li1 O12 1.978(17) 4_649 ?
Li1 O12 2.00(2) 1_545 ?
Li1 Li2 3.12(2) . ?
Li1 Li1 3.203(19) 4_649 ?
Li1 Li1 3.203(19) 4_659 ?
Li1 Rb2 4.366(15) 4_648 ?
Li2 O11 1.957(19) 4_648 ?
Li2 O11 2.01(2) 1_545 ?
Li2 S3 3.01(2) 1_545 ?
Li2 Li2 3.21(2) 4_648 ?
Li2 Li2 3.21(2) 4_658 ?
Li2 Rb2 3.855(16) 4_648 ?
Li2 Rb2 4.117(18) 1_545 ?
Li3 O4 1.887(18) 2_667 ?
Li3 O6 1.94(2) 1_565 ?
Li3 O9 1.971(18) 4_658 ?
Li3 S2 3.02(2) 1_565 ?
Li3 Li4 3.08(2) 2_666 ?
Li3 Rb2 3.73(2) 1_565 ?
Li3 Rb1 4.04(2) 1_565 ?
Li4 O6 1.90(2) 2_656 ?
Li4 O3 1.925(18) 2_656 ?
Li4 O5 2.01(3) 2_646 ?
Li4 S2 3.01(3) 2_656 ?
Li4 Li3 3.08(2) 2_646 ?
Li4 Na1 3.18(2) 1_565 ?
Li4 Rb2 4.14(2) 2_647 ?
Li4 Rb2 4.23(2) 2_657 ?
Li4 Rb1 4.28(2) 1_554 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Rb1 O1 138.4(3) 2_667 1_565 ?
O1 Rb1 O4 141.4(2) 2_667 . ?
O1 Rb1 O4 74.2(2) 1_565 . ?
O1 Rb1 O4 74.2(2) 2_667 2_657 ?
O1 Rb1 O4 141.4(2) 1_565 2_657 ?
O4 Rb1 O4 88.0(3) . 2_657 ?
O1 Rb1 O3 150.6(2) 2_667 . ?
O1 Rb1 O3 64.2(2) 1_565 . ?
O4 Rb1 O3 46.7(2) . . ?
O4 Rb1 O3 78.6(2) 2_657 . ?
O1 Rb1 O3 64.2(2) 2_667 2_657 ?
O1 Rb1 O3 150.6(2) 1_565 2_657 ?
O4 Rb1 O3 78.6(2) . 2_657 ?
O4 Rb1 O3 46.7(2) 2_657 2_657 ?
O3 Rb1 O3 104.1(3) . 2_657 ?
O1 Rb1 O8 73.9(2) 2_667 . ?
O1 Rb1 O8 98.5(2) 1_565 . ?
O4 Rb1 O8 130.5(2) . . ?
O4 Rb1 O8 67.3(2) 2_657 . ?
O3 Rb1 O8 85.47(19) . . ?
O3 Rb1 O8 107.7(2) 2_657 . ?
O1 Rb1 O8 98.5(2) 2_667 2_657 ?
O1 Rb1 O8 73.9(2) 1_565 2_657 ?
O4 Rb1 O8 67.3(2) . 2_657 ?
O4 Rb1 O8 130.5(2) 2_657 2_657 ?
O3 Rb1 O8 107.7(2) . 2_657 ?
O3 Rb1 O8 85.47(19) 2_657 2_657 ?
O8 Rb1 O8 158.9(3) . 2_657 ?
O1 Rb1 O4 42.88(19) 2_667 2_667 ?
O1 Rb1 O4 99.1(2) 1_565 2_667 ?
O4 Rb1 O4 172.00(17) . 2_667 ?
O4 Rb1 O4 100.0(2) 2_657 2_667 ?
O3 Rb1 O4 134.75(19) . 2_667 ?
O3 Rb1 O4 106.90(19) 2_657 2_667 ?
O8 Rb1 O4 54.13(18) . 2_667 ?
O8 Rb1 O4 106.83(18) 2_657 2_667 ?
O1 Rb1 O4 99.1(2) 2_667 1_565 ?
O1 Rb1 O4 42.88(19) 1_565 1_565 ?
O4 Rb1 O4 100.0(2) . 1_565 ?
O4 Rb1 O4 172.00(18) 2_657 1_565 ?
O3 Rb1 O4 106.90(18) . 1_565 ?
O3 Rb1 O4 134.75(19) 2_657 1_565 ?
O8 Rb1 O4 106.83(18) . 1_565 ?
O8 Rb1 O4 54.13(18) 2_657 1_565 ?
O4 Rb1 O4 72.0(2) 2_667 1_565 ?
O1 Rb1 S1 157.30(17) 2_667 . ?
O1 Rb1 S1 64.14(15) 1_565 . ?
O4 Rb1 S1 22.87(14) . . ?
O4 Rb1 S1 86.31(17) 2_657 . ?
O3 Rb1 S1 24.28(14) . . ?
O3 Rb1 S1 93.93(16) 2_657 . ?
O8 Rb1 S1 109.64(14) . . ?
O8 Rb1 S1 85.14(15) 2_657 . ?
O4 Rb1 S1 156.50(13) 2_667 . ?
O4 Rb1 S1 101.05(13) 1_565 . ?
O1 Rb1 S1 64.14(15) 2_667 2_657 ?
O1 Rb1 S1 157.30(17) 1_565 2_657 ?
O4 Rb1 S1 86.31(17) . 2_657 ?
O4 Rb1 S1 22.87(14) 2_657 2_657 ?
O3 Rb1 S1 93.93(16) . 2_657 ?
O3 Rb1 S1 24.28(14) 2_657 2_657 ?
O8 Rb1 S1 85.14(15) . 2_657 ?
O8 Rb1 S1 109.64(14) 2_657 2_657 ?
O4 Rb1 S1 101.05(13) 2_667 2_657 ?
O4 Rb1 S1 156.50(12) 1_565 2_657 ?
S1 Rb1 S1 93.46(10) . 2_657 ?
O2 Rb2 O9 81.9(2) 2_657 4_648 ?
O2 Rb2 O1 66.1(2) 2_657 2_667 ?
O9 Rb2 O1 124.6(2) 4_648 2_667 ?
O2 Rb2 O8 105.4(2) 2_657 . ?
O9 Rb2 O8 70.5(2) 4_648 . ?
O1 Rb2 O8 75.9(2) 2_667 . ?
O2 Rb2 O5 62.4(2) 2_657 1_556 ?
O9 Rb2 O5 137.8(2) 4_648 1_556 ?
O1 Rb2 O5 62.0(2) 2_667 1_556 ?
O8 Rb2 O5 137.7(2) . 1_556 ?
O2 Rb2 O9 156.80(18) 2_657 4_658 ?
O9 Rb2 O9 105.3(2) 4_648 4_658 ?
O1 Rb2 O9 92.4(2) 2_667 4_658 ?
O8 Rb2 O9 58.54(19) . 4_658 ?
O5 Rb2 O9 116.38(19) 1_556 4_658 ?
O2 Rb2 O13 126.96(18) 2_657 1_565 ?
O9 Rb2 O13 133.74(17) 4_648 1_565 ?
O1 Rb2 O13 101.31(18) 2_667 1_565 ?
O8 Rb2 O13 121.69(19) . 1_565 ?
O5 Rb2 O13 66.40(18) 1_556 1_565 ?
O9 Rb2 O13 63.50(18) 4_658 1_565 ?
O2 Rb2 O10 151.2(2) 2_657 4_658 ?
O9 Rb2 O10 69.28(18) 4_648 4_658 ?
O1 Rb2 O10 131.6(2) 2_667 4_658 ?
O8 Rb2 O10 65.98(19) . 4_658 ?
O5 Rb2 O10 142.7(2) 1_556 4_658 ?
O9 Rb2 O10 42.54(17) 4_658 4_658 ?
O13 Rb2 O10 76.41(16) 1_565 4_658 ?
O2 Rb2 O4 43.21(19) 2_657 2_657 ?
O9 Rb2 O4 58.18(18) 4_648 2_657 ?
O1 Rb2 O4 67.82(19) 2_667 2_657 ?
O8 Rb2 O4 63.83(19) . 2_657 ?
O5 Rb2 O4 101.47(19) 1_556 2_657 ?
O9 Rb2 O4 122.06(18) 4_658 2_657 ?
O13 Rb2 O4 167.09(16) 1_565 2_657 ?
O10 Rb2 O4 115.83(17) 4_658 2_657 ?
O2 Rb2 O13 66.23(17) 2_657 . ?
O9 Rb2 O13 65.07(18) 4_648 . ?
O1 Rb2 O13 128.61(19) 2_667 . ?
O8 Rb2 O13 135.50(18) . . ?
O5 Rb2 O13 79.62(17) 1_556 . ?
O9 Rb2 O13 136.91(16) 4_658 . ?
O13 Rb2 O13 92.19(13) 1_565 . ?
O10 Rb2 O13 99.74(16) 4_658 . ?
O4 Rb2 O13 89.75(16) 2_657 . ?
O2 Rb2 Li3 124.6(3) 2_657 . ?
O9 Rb2 Li3 100.1(4) 4_648 . ?
O1 Rb2 Li3 68.2(3) 2_667 . ?
O8 Rb2 Li3 32.7(4) . . ?
O5 Rb2 Li3 118.1(3) 1_556 . ?
O9 Rb2 Li3 33.1(3) 4_658 . ?
O13 Rb2 Li3 91.1(4) 1_565 . ?
O10 Rb2 Li3 63.6(3) 4_658 . ?
O4 Rb2 Li3 91.1(4) 2_657 . ?
O13 Rb2 Li3 161.6(3) . . ?
O2 Rb2 O7 82.26(19) 2_657 1_556 ?
O9 Rb2 O7 117.1(2) 4_648 1_556 ?
O1 Rb2 O7 102.5(2) 2_667 1_556 ?
O8 Rb2 O7 170.3(2) . 1_556 ?
O5 Rb2 O7 40.85(17) 1_556 1_556 ?
O9 Rb2 O7 112.30(19) 4_658 1_556 ?
O13 Rb2 O7 48.89(18) 1_565 1_556 ?
O10 Rb2 O7 110.04(17) 4_658 1_556 ?
O4 Rb2 O7 124.77(19) 2_657 1_556 ?
O13 Rb2 O7 52.81(18) . 1_556 ?
Li3 Rb2 O7 137.7(4) . 1_556 ?
O4 S1 O2 108.8(5) . . ?
O4 S1 O1 111.8(5) . . ?
O2 S1 O1 108.7(4) . . ?
O4 S1 O3 108.8(4) . . ?
O2 S1 O3 109.7(5) . . ?
O1 S1 O3 109.0(5) . . ?
O4 S1 Li4 138.0(5) . . ?
O2 S1 Li4 31.4(5) . . ?
O1 S1 Li4 83.8(6) . . ?
O3 S1 Li4 101.5(5) . . ?
O4 S1 Na1 119.8(4) . 1_565 ?
O2 S1 Na1 60.9(3) . 1_565 ?
O1 S1 Na1 128.1(4) . 1_565 ?
O3 S1 Na1 49.1(3) . 1_565 ?
Li4 S1 Na1 62.6(5) . 1_565 ?
O4 S1 Rb1 53.6(3) . . ?
O2 S1 Rb1 113.1(3) . . ?
O1 S1 Rb1 138.2(3) . . ?
O3 S1 Rb1 56.9(3) . . ?
Li4 S1 Rb1 135.0(6) . . ?
Na1 S1 Rb1 75.52(11) 1_565 . ?
O4 S1 Rb2 82.9(3) . 2_647 ?
O2 S1 Rb2 78.6(3) . 2_647 ?
O1 S1 Rb2 52.5(3) . 2_647 ?
O3 S1 Rb2 161.4(3) . 2_647 ?
Li4 S1 Rb2 76.7(4) . 2_647 ?
Na1 S1 Rb2 137.68(8) 1_565 2_647 ?
Rb1 S1 Rb2 136.43(7) . 2_647 ?
O4 S1 Rb1 73.9(3) . 1_545 ?
O2 S1 Rb1 157.1(3) . 1_545 ?
O1 S1 Rb1 51.8(3) . 1_545 ?
O3 S1 Rb1 90.0(3) . 1_545 ?
Li4 S1 Rb1 135.3(6) . 1_545 ?
Na1 S1 Rb1 138.70(7) 1_565 1_545 ?
Rb1 S1 Rb1 87.17(5) . 1_545 ?
Rb2 S1 Rb1 79.20(7) 2_647 1_545 ?
O4 S1 Rb2 65.2(3) . 2_657 ?
O2 S1 Rb2 45.2(3) . 2_657 ?
O1 S1 Rb2 136.4(3) . 2_657 ?
O3 S1 Rb2 112.9(3) . 2_657 ?
Li4 S1 Rb2 76.6(4) . 2_657 ?
Na1 S1 Rb2 75.34(11) 1_565 2_657 ?
Rb1 S1 Rb2 77.81(7) . 2_657 ?
Rb2 S1 Rb2 84.92(5) 2_647 2_657 ?
Rb1 S1 Rb2 137.59(7) 1_545 2_657 ?
O8 S2 O5 111.6(5) . . ?
O8 S2 O7 109.6(5) . . ?
O5 S2 O7 109.2(5) . . ?
O8 S2 O6 109.0(5) . . ?
O5 S2 O6 108.6(4) . . ?
O7 S2 O6 108.8(5) . . ?
O8 S2 Li4 125.8(4) . 2_656 ?
O5 S2 Li4 78.1(5) . 2_656 ?
O7 S2 Li4 117.0(5) . 2_656 ?
O6 S2 Li4 30.8(5) . 2_656 ?
O8 S2 Li3 79.0(5) . 1_545 ?
O5 S2 Li3 133.4(5) . 1_545 ?
O7 S2 Li3 108.9(5) . 1_545 ?
O6 S2 Li3 32.5(5) . 1_545 ?
Li4 S2 Li3 61.3(5) 2_656 1_545 ?
O8 S2 Li3 30.9(5) . . ?
O5 S2 Li3 91.5(5) . . ?
O7 S2 Li3 96.2(5) . . ?
O6 S2 Li3 139.6(5) . . ?
Li4 S2 Li3 146.8(4) 2_656 . ?
Li3 S2 Li3 109.8(5) 1_545 . ?
O8 S2 Rb1 56.0(3) . . ?
O5 S2 Rb1 78.5(3) . . ?
O7 S2 Rb1 165.6(4) . . ?
O6 S2 Rb1 79.0(3) . . ?
Li4 S2 Rb1 76.1(3) 2_656 . ?
Li3 S2 Rb1 70.8(3) 1_545 . ?
Li3 S2 Rb1 70.9(3) . . ?
O8 S2 Rb2 154.0(4) . 1_554 ?
O5 S2 Rb2 51.8(3) . 1_554 ?
O7 S2 Rb2 66.3(3) . 1_554 ?
O6 S2 Rb2 96.2(3) . 1_554 ?
Li4 S2 Rb2 74.3(3) 2_656 1_554 ?
Li3 S2 Rb2 127.0(4) 1_545 1_554 ?
Li3 S2 Rb2 123.2(4) . 1_554 ?
Rb1 S2 Rb2 125.98(6) . 1_554 ?
O9 S3 O12 111.3(4) . . ?
O9 S3 O11 109.3(4) . . ?
O12 S3 O11 109.9(4) . . ?
O9 S3 O10 110.3(4) . . ?
O12 S3 O10 107.5(4) . . ?
O11 S3 O10 108.5(4) . . ?
O9 S3 Li2 103.2(5) . 1_565 ?
O12 S3 Li2 80.3(4) . 1_565 ?
O11 S3 Li2 36.0(5) . 1_565 ?
O10 S3 Li2 139.2(5) . 1_565 ?
O9 S3 Li1 105.8(4) . . ?
O12 S3 Li1 79.4(4) . . ?
O11 S3 Li1 136.4(5) . . ?
O10 S3 Li1 33.1(4) . . ?
Li2 S3 Li1 149.1(4) 1_565 . ?
O9 S3 Li2 123.0(4) . . ?
O12 S3 Li2 118.9(4) . . ?
O11 S3 Li2 77.7(5) . . ?
O10 S3 Li2 30.9(5) . . ?
Li2 S3 Li2 109.8(5) 1_565 . ?
Li1 S3 Li2 61.7(5) . . ?
O9 S3 Rb2 56.5(3) . 4_648 ?
O12 S3 Rb2 148.7(3) . 4_648 ?
O11 S3 Rb2 101.4(3) . 4_648 ?
O10 S3 Rb2 60.1(3) . 4_648 ?
Li2 S3 Rb2 128.8(3) 1_565 4_648 ?
Li1 S3 Rb2 77.5(3) . 4_648 ?
Li2 S3 Rb2 66.6(3) . 4_648 ?
O9 S3 Rb2 38.0(3) . 4_658 ?
O12 S3 Rb2 109.6(3) . 4_658 ?
O11 S3 Rb2 75.0(3) . 4_658 ?
O10 S3 Rb2 138.7(3) . 4_658 ?
Li2 S3 Rb2 65.7(3) 1_565 4_658 ?
Li1 S3 Rb2 143.8(3) . 4_658 ?
Li2 S3 Rb2 130.0(3) . 4_658 ?
Rb2 S3 Rb2 78.71(5) 4_648 4_658 ?
O1 Na1 O1 113.6(5) 2_656 . ?
O1 Na1 O3 85.7(3) 2_656 2_646 ?
O1 Na1 O3 146.6(3) . 2_646 ?
O1 Na1 O3 146.6(3) 2_656 1_545 ?
O1 Na1 O3 85.7(3) . 1_545 ?
O3 Na1 O3 92.1(4) 2_646 1_545 ?
O1 Na1 O2 79.2(3) 2_656 2_646 ?
O1 Na1 O2 150.1(2) . 2_646 ?
O3 Na1 O2 56.5(2) 2_646 2_646 ?
O3 Na1 O2 72.0(3) 1_545 2_646 ?
O1 Na1 O2 150.1(2) 2_656 1_545 ?
O1 Na1 O2 79.2(3) . 1_545 ?
O3 Na1 O2 72.0(3) 2_646 1_545 ?
O3 Na1 O2 56.5(2) 1_545 1_545 ?
O2 Na1 O2 103.3(4) 2_646 1_545 ?
O1 Na1 O5 74.9(3) 2_656 1_545 ?
O1 Na1 O5 87.7(3) . 1_545 ?
O3 Na1 O5 124.6(3) 2_646 1_545 ?
O3 Na1 O5 79.2(2) 1_545 1_545 ?
O2 Na1 O5 69.0(2) 2_646 1_545 ?
O2 Na1 O5 134.3(3) 1_545 1_545 ?
O1 Na1 O5 87.7(3) 2_656 2_646 ?
O1 Na1 O5 74.9(3) . 2_646 ?
O3 Na1 O5 79.2(2) 2_646 2_646 ?
O3 Na1 O5 124.6(3) 1_545 2_646 ?
O2 Na1 O5 134.3(3) 2_646 2_646 ?
O2 Na1 O5 69.0(2) 1_545 2_646 ?
O5 Na1 O5 148.1(4) 1_545 2_646 ?
O1 Na1 S1 79.9(2) 2_656 2_646 ?
O1 Na1 S1 166.4(3) . 2_646 ?
O3 Na1 S1 27.96(18) 2_646 2_646 ?
O3 Na1 S1 82.7(3) 1_545 2_646 ?
O2 Na1 S1 28.58(16) 2_646 2_646 ?
O2 Na1 S1 88.5(3) 1_545 2_646 ?
O5 Na1 S1 96.90(18) 1_545 2_646 ?
O5 Na1 S1 106.22(19) 2_646 2_646 ?
O1 Na1 S1 166.4(3) 2_656 1_545 ?
O1 Na1 S1 79.9(2) . 1_545 ?
O3 Na1 S1 82.7(3) 2_646 1_545 ?
O3 Na1 S1 27.96(18) 1_545 1_545 ?
O2 Na1 S1 88.5(3) 2_646 1_545 ?
O2 Na1 S1 28.58(16) 1_545 1_545 ?
O5 Na1 S1 106.22(19) 1_545 1_545 ?
O5 Na1 S1 96.90(18) 2_646 1_545 ?
S1 Na1 S1 86.6(2) 2_646 1_545 ?
O1 Na1 Li4 110.2(4) 2_656 2_646 ?
O1 Na1 Li4 114.9(4) . 2_646 ?
O3 Na1 Li4 80.0(5) 2_646 2_646 ?
O3 Na1 Li4 37.1(3) 1_545 2_646 ?
O2 Na1 Li4 37.2(3) 2_646 2_646 ?
O2 Na1 Li4 85.8(4) 1_545 2_646 ?
O5 Na1 Li4 60.5(4) 1_545 2_646 ?
O5 Na1 Li4 151.3(5) 2_646 2_646 ?
S1 Na1 Li4 57.8(4) 2_646 2_646 ?
S1 Na1 Li4 60.9(4) 1_545 2_646 ?
O1 Na1 Li4 114.9(4) 2_656 1_545 ?
O1 Na1 Li4 110.2(4) . 1_545 ?
O3 Na1 Li4 37.1(3) 2_646 1_545 ?
O3 Na1 Li4 80.0(5) 1_545 1_545 ?
O2 Na1 Li4 85.8(4) 2_646 1_545 ?
O2 Na1 Li4 37.2(3) 1_545 1_545 ?
O5 Na1 Li4 151.3(5) 1_545 1_545 ?
O5 Na1 Li4 60.5(5) 2_646 1_545 ?
S1 Na1 Li4 60.9(4) 2_646 1_545 ?
S1 Na1 Li4 57.8(4) 1_545 1_545 ?
Li4 Na1 Li4 91.2(9) 2_646 1_545 ?
S1 O1 Na1 131.8(5) . . ?
S1 O1 Rb1 104.9(4) . 1_545 ?
Na1 O1 Rb1 103.2(3) . 1_545 ?
S1 O1 Rb2 104.0(4) . 2_647 ?
Na1 O1 Rb2 107.0(3) . 2_647 ?
Rb1 O1 Rb2 102.8(2) 1_545 2_647 ?
S1 O2 Li4 125.0(8) . . ?
S1 O2 Na1 90.6(3) . 1_565 ?
Li4 O2 Na1 85.0(7) . 1_565 ?
S1 O2 Rb2 113.6(4) . 2_657 ?
Li4 O2 Rb2 121.3(7) . 2_657 ?
Na1 O2 Rb2 97.4(3) 1_565 2_657 ?
S1 O2 Rb2 77.7(3) . 2_647 ?
Li4 O2 Rb2 91.5(8) . 2_647 ?
Na1 O2 Rb2 162.9(3) 1_565 2_647 ?
Rb2 O2 Rb2 98.7(2) 2_657 2_647 ?
S1 O3 Li4 137.1(10) . 2_656 ?
S1 O3 Na1 103.0(4) . 1_565 ?
Li4 O3 Na1 94.2(8) 2_656 1_565 ?
S1 O3 Rb1 98.9(4) . . ?
Li4 O3 Rb1 117.7(7) 2_656 . ?
Na1 O3 Rb1 97.5(3) 1_565 . ?
S1 O4 Li3 145.5(8) . 2_647 ?
S1 O4 Rb1 103.6(4) . . ?
Li3 O4 Rb1 110.9(7) 2_647 . ?
S1 O4 Rb2 92.3(4) . 2_657 ?
Li3 O4 Rb2 84.8(7) 2_647 2_657 ?
Rb1 O4 Rb2 92.3(2) . 2_657 ?
S1 O4 Rb1 83.0(3) . 1_545 ?
Li3 O4 Rb1 92.5(8) 2_647 1_545 ?
Rb1 O4 Rb1 100.0(2) . 1_545 ?
Rb2 O4 Rb1 167.6(2) 2_657 1_545 ?
S2 O5 Li4 125.2(7) . 2_666 ?
S2 O5 Na1 134.7(5) . 1_565 ?
Li4 O5 Na1 91.0(5) 2_666 1_565 ?
S2 O5 Rb2 107.2(4) . 1_554 ?
Li4 O5 Rb2 102.6(5) 2_666 1_554 ?
Na1 O5 Rb2 87.0(2) 1_565 1_554 ?
S2 O6 Li4 125.7(9) . 2_656 ?
S2 O6 Li3 123.3(8) . 1_545 ?
Li4 O6 Li3 106.4(10) 2_656 1_545 ?
S2 O7 Li1 126.8(7) . 4_658 ?
S2 O7 Rb2 91.6(3) . 1_554 ?
Li1 O7 Rb2 140.1(5) 4_658 1_554 ?
S2 O8 Li3 126.2(7) . . ?
S2 O8 Rb2 140.8(5) . . ?
Li3 O8 Rb2 86.2(6) . . ?
S2 O8 Rb1 102.3(4) . . ?
Li3 O8 Rb1 99.1(6) . . ?
Rb2 O8 Rb1 92.0(2) . . ?
S3 O9 Li3 135.1(8) . 4_648 ?
S3 O9 Rb2 124.1(4) . 4_658 ?
Li3 O9 Rb2 97.2(7) 4_648 4_658 ?
S3 O9 Rb2 101.7(4) . 4_648 ?
Li3 O9 Rb2 81.1(7) 4_648 4_648 ?
Rb2 O9 Rb2 105.3(2) 4_658 4_648 ?
S3 O10 Li2 125.9(8) . . ?
S3 O10 Li1 122.6(8) . . ?
Li2 O10 Li1 106.3(9) . . ?
S3 O10 Rb2 97.5(3) . 4_648 ?
Li2 O10 Rb2 88.9(6) . 4_648 ?
Li1 O10 Rb2 106.5(6) . 4_648 ?
S3 O11 Li2 128.0(7) . 4_658 ?
S3 O11 Li2 118.5(7) . 1_565 ?
Li2 O11 Li2 108.0(8) 4_658 1_565 ?
S3 O12 Li1 127.2(7) . 4_659 ?
S3 O12 Li1 122.2(6) . 1_565 ?
Li1 O12 Li1 107.1(7) 4_659 1_565 ?
Li2 O13 Rb2 102.2(7) . 1_545 ?
Li2 O13 Rb2 101.2(7) . . ?
Rb2 O13 Rb2 92.19(12) 1_545 . ?
O7 Li1 O10 121.8(10) 4_648 . ?
O7 Li1 O12 107.3(8) 4_648 4_649 ?
O10 Li1 O12 105.2(9) . 4_649 ?
O7 Li1 O12 111.7(10) 4_648 1_545 ?
O10 Li1 O12 104.4(8) . 1_545 ?
O12 Li1 O12 105.1(8) 4_649 1_545 ?
O7 Li1 S3 105.5(8) 4_648 . ?
O10 Li1 S3 24.3(4) . . ?
O12 Li1 S3 95.7(8) 4_649 . ?
O12 Li1 S3 128.7(7) 1_545 . ?
O7 Li1 Li2 150.1(8) 4_648 . ?
O10 Li1 Li2 36.4(5) . . ?
O12 Li1 Li2 100.1(7) 4_649 . ?
O12 Li1 Li2 71.1(7) 1_545 . ?
S3 Li1 Li2 59.3(5) . . ?
O7 Li1 Li1 116.0(9) 4_648 4_649 ?
O10 Li1 Li1 120.2(10) . 4_649 ?
O12 Li1 Li1 69.6(9) 4_649 4_649 ?
O12 Li1 Li1 36.2(2) 1_545 4_649 ?
S3 Li1 Li1 138.4(8) . 4_649 ?
Li2 Li1 Li1 84.4(7) . 4_649 ?
O7 Li1 Li1 109.9(8) 4_648 4_659 ?
O10 Li1 Li1 73.5(6) . 4_659 ?
O12 Li1 Li1 36.7(7) 4_649 4_659 ?
O12 Li1 Li1 131.0(9) 1_545 4_659 ?
S3 Li1 Li1 59.4(3) . 4_659 ?
Li2 Li1 Li1 85.3(7) . 4_659 ?
Li1 Li1 Li1 101.3(8) 4_649 4_659 ?
O7 Li1 Rb2 91.0(5) 4_648 4_648 ?
O10 Li1 Rb2 47.9(4) . 4_648 ?
O12 Li1 Rb2 153.1(8) 4_649 4_648 ?
O12 Li1 Rb2 85.2(5) 1_545 4_648 ?
S3 Li1 Rb2 59.7(3) . 4_648 ?
Li2 Li1 Rb2 59.2(4) . 4_648 ?
Li1 Li1 Rb2 120.2(6) 4_649 4_648 ?
Li1 Li1 Rb2 118.8(6) 4_659 4_648 ?
O13 Li2 O10 109.5(10) . . ?
O13 Li2 O11 112.8(9) . 4_648 ?
O10 Li2 O11 113.6(11) . 4_648 ?
O13 Li2 O11 106.0(11) . 1_545 ?
O10 Li2 O11 111.0(9) . 1_545 ?
O11 Li2 O11 103.6(9) 4_648 1_545 ?
O13 Li2 S3 106.6(9) . 1_545 ?
O10 Li2 S3 87.3(6) . 1_545 ?
O11 Li2 S3 124.0(9) 4_648 1_545 ?
O11 Li2 S3 25.6(3) 1_545 1_545 ?
O13 Li2 S3 106.9(9) . . ?
O10 Li2 S3 23.2(4) . . ?
O11 Li2 S3 95.2(8) 4_648 . ?
O11 Li2 S3 131.7(7) 1_545 . ?
S3 Li2 S3 109.8(5) 1_545 . ?
O13 Li2 Li1 92.5(7) . . ?
O10 Li2 Li1 37.3(6) . . ?
O11 Li2 Li1 149.0(9) 4_648 . ?
O11 Li2 Li1 85.2(7) 1_545 . ?
S3 Li2 Li1 59.7(5) 1_545 . ?
S3 Li2 Li1 59.0(5) . . ?
O13 Li2 Li2 114.0(9) . 4_648 ?
O10 Li2 Li2 130.9(10) . 4_648 ?
O11 Li2 Li2 68.6(9) 4_648 4_648 ?
O11 Li2 Li2 35.5(2) 1_545 4_648 ?
S3 Li2 Li2 59.6(3) 1_545 4_648 ?
S3 Li2 Li2 139.1(8) . 4_648 ?
Li1 Li2 Li2 118.3(8) . 4_648 ?
O13 Li2 Li2 114.6(9) . 4_658 ?
O10 Li2 Li2 80.0(6) . 4_658 ?
O11 Li2 Li2 36.5(7) 4_648 4_658 ?
O11 Li2 Li2 131.5(10) 1_545 4_658 ?
S3 Li2 Li2 138.9(8) 1_545 4_658 ?
S3 Li2 Li2 59.2(3) . 4_658 ?
Li1 Li2 Li2 117.3(8) . 4_658 ?
Li2 Li2 Li2 101.1(9) 4_648 4_658 ?
O13 Li2 Rb2 169.1(8) . 4_648 ?
O10 Li2 Rb2 61.1(5) . 4_648 ?
O11 Li2 Rb2 77.2(5) 4_648 4_648 ?
O11 Li2 Rb2 74.5(5) 1_545 4_648 ?
S3 Li2 Rb2 69.0(3) 1_545 4_648 ?
S3 Li2 Rb2 66.9(3) . 4_648 ?
Li1 Li2 Rb2 76.7(4) . 4_648 ?
Li2 Li2 Rb2 72.9(6) 4_648 4_648 ?
Li2 Li2 Rb2 70.6(6) 4_658 4_648 ?
O13 Li2 Rb2 53.0(5) . 1_545 ?
O10 Li2 Rb2 159.7(8) . 1_545 ?
O11 Li2 Rb2 84.9(6) 4_648 1_545 ?
O11 Li2 Rb2 70.1(6) 1_545 1_545 ?
S3 Li2 Rb2 88.8(5) 1_545 1_545 ?
S3 Li2 Rb2 156.9(6) . 1_545 ?
Li1 Li2 Rb2 125.8(6) . 1_545 ?
Li2 Li2 Rb2 62.1(5) 4_648 1_545 ?
Li2 Li2 Rb2 115.2(7) 4_658 1_545 ?
Rb2 Li2 Rb2 134.9(5) 4_648 1_545 ?
O13 Li2 Rb2 54.5(6) . . ?
O10 Li2 Rb2 106.5(8) . . ?
O11 Li2 Rb2 65.2(6) 4_648 . ?
O11 Li2 Rb2 142.1(7) 1_545 . ?
S3 Li2 Rb2 159.2(6) 1_545 . ?
S3 Li2 Rb2 86.2(5) . . ?
Li1 Li2 Rb2 123.9(6) . . ?
Li2 Li2 Rb2 116.6(7) 4_648 . ?
Li2 Li2 Rb2 60.7(4) 4_658 . ?
Rb2 Li2 Rb2 131.3(5) 4_648 . ?
Rb2 Li2 Rb2 72.8(3) 1_545 . ?
O4 Li3 O8 107.6(11) 2_667 . ?
O4 Li3 O6 113.5(11) 2_667 1_565 ?
O8 Li3 O6 109.1(9) . 1_565 ?
O4 Li3 O9 107.1(9) 2_667 4_658 ?
O8 Li3 O9 107.1(10) . 4_658 ?
O6 Li3 O9 112.2(10) 1_565 4_658 ?
O4 Li3 S2 104.8(10) 2_667 1_565 ?
O8 Li3 S2 132.5(8) . 1_565 ?
O6 Li3 S2 24.2(4) 1_565 1_565 ?
O9 Li3 S2 95.3(9) 4_658 1_565 ?
O4 Li3 S2 123.5(10) 2_667 . ?
O8 Li3 S2 22.8(4) . . ?
O6 Li3 S2 86.9(7) 1_565 . ?
O9 Li3 S2 112.4(9) 4_658 . ?
S2 Li3 S2 109.8(5) 1_565 . ?
O4 Li3 Li4 105.4(7) 2_667 2_666 ?
O8 Li3 Li4 79.1(8) . 2_666 ?
O6 Li3 Li4 36.3(6) 1_565 2_666 ?
O9 Li3 Li4 143.0(9) 4_658 2_666 ?
S2 Li3 Li4 59.2(6) 1_565 2_666 ?
S2 Li3 Li4 60.9(6) . 2_666 ?
O4 Li3 Rb2 79.0(7) 2_667 . ?
O8 Li3 Rb2 61.1(6) . . ?
O6 Li3 Rb2 166.7(10) 1_565 . ?
O9 Li3 Rb2 65.7(6) 4_658 . ?
S2 Li3 Rb2 160.8(6) 1_565 . ?
S2 Li3 Rb2 82.2(6) . . ?
Li4 Li3 Rb2 138.8(9) 2_666 . ?
O4 Li3 Rb2 65.0(6) 2_667 1_565 ?
O8 Li3 Rb2 146.4(8) . 1_565 ?
O6 Li3 Rb2 103.5(10) 1_565 1_565 ?
O9 Li3 Rb2 51.3(6) 4_658 1_565 ?
S2 Li3 Rb2 79.4(6) 1_565 1_565 ?
S2 Li3 Rb2 162.9(6) . 1_565 ?
Li4 Li3 Rb2 134.3(9) 2_666 1_565 ?
Rb2 Li3 Rb2 85.4(4) . 1_565 ?
O4 Li3 Rb1 43.2(5) 2_667 1_565 ?
O8 Li3 Rb1 126.3(7) . 1_565 ?
O6 Li3 Rb1 70.4(6) 1_565 1_565 ?
O9 Li3 Rb1 123.1(10) 4_658 1_565 ?
S2 Li3 Rb1 64.1(4) 1_565 1_565 ?
S2 Li3 Rb1 124.4(5) . 1_565 ?
Li4 Li3 Rb1 72.5(5) 2_666 1_565 ?
Rb2 Li3 Rb1 122.2(4) . 1_565 ?
Rb2 Li3 Rb1 72.4(4) 1_565 1_565 ?
O4 Li3 Rb1 59.7(6) 2_667 . ?
O8 Li3 Rb1 52.8(5) . . ?
O6 Li3 Rb1 107.9(6) 1_565 . ?
O9 Li3 Rb1 139.6(9) 4_658 . ?
S2 Li3 Rb1 124.5(5) 1_565 . ?
S2 Li3 Rb1 64.0(4) . . ?
Li4 Li3 Rb1 73.6(5) 2_666 . ?
Rb2 Li3 Rb1 74.0(4) . . ?
Rb2 Li3 Rb1 123.4(4) 1_565 . ?
Rb1 Li3 Rb1 75.6(3) 1_565 . ?
O6 Li4 O3 102.8(11) 2_656 2_656 ?
O6 Li4 O2 115.3(12) 2_656 . ?
O3 Li4 O2 102.4(9) 2_656 . ?
O6 Li4 O5 108.0(9) 2_656 2_646 ?
O3 Li4 O5 120.9(12) 2_656 2_646 ?
O2 Li4 O5 107.8(11) . 2_646 ?
O6 Li4 S2 23.6(5) 2_656 2_656 ?
O3 Li4 S2 95.2(10) 2_656 2_656 ?
O2 Li4 S2 96.0(10) . 2_656 ?
O5 Li4 S2 129.5(7) 2_646 2_656 ?
O6 Li4 S1 138.8(11) 2_656 . ?
O3 Li4 S1 92.5(6) 2_656 . ?
O2 Li4 S1 23.5(3) . . ?
O5 Li4 S1 95.7(8) 2_646 . ?
S2 Li4 S1 118.5(8) 2_656 . ?
O6 Li4 Li3 37.3(6) 2_656 2_646 ?
O3 Li4 Li3 96.2(7) 2_656 2_646 ?
O2 Li4 Li3 150.7(10) . 2_646 ?
O5 Li4 Li3 81.0(8) 2_646 2_646 ?
S2 Li4 Li3 59.5(6) 2_656 2_646 ?
S1 Li4 Li3 171.2(7) . 2_646 ?
O6 Li4 Na1 103.6(12) 2_656 1_565 ?
O3 Li4 Na1 48.7(6) 2_656 1_565 ?
O2 Li4 Na1 57.7(6) . 1_565 ?
O5 Li4 Na1 148.4(9) 2_646 1_565 ?
S2 Li4 Na1 81.8(7) 2_656 1_565 ?
S1 Li4 Na1 59.6(4) . 1_565 ?
Li3 Li4 Na1 126.3(9) 2_646 1_565 ?
O6 Li4 Na1 157.7(11) 2_656 . ?
O3 Li4 Na1 79.4(7) 2_656 . ?
O2 Li4 Na1 85.3(7) . . ?
O5 Li4 Na1 54.5(6) 2_646 . ?
S2 Li4 Na1 174.6(6) 2_656 . ?
S1 Li4 Na1 62.3(4) . . ?
Li3 Li4 Na1 120.6(9) 2_646 . ?
Na1 Li4 Na1 94.6(4) 1_565 . ?
O6 Li4 Rb2 115.5(7) 2_656 2_647 ?
O3 Li4 Rb2 141.6(8) 2_656 2_647 ?
O2 Li4 Rb2 60.6(6) . 2_647 ?
O5 Li4 Rb2 49.1(5) 2_646 2_647 ?
S2 Li4 Rb2 119.4(4) 2_656 2_647 ?
S1 Li4 Rb2 57.8(3) . 2_647 ?
Li3 Li4 Rb2 114.9(7) 2_646 2_647 ?
Na1 Li4 Rb2 116.4(4) 1_565 2_647 ?
Na1 Li4 Rb2 65.8(4) . 2_647 ?
O6 Li4 Rb2 79.7(7) 2_656 2_657 ?
O3 Li4 Rb2 115.1(10) 2_656 2_657 ?
O2 Li4 Rb2 35.7(5) . 2_657 ?
O5 Li4 Rb2 119.2(6) 2_646 2_657 ?
S2 Li4 Rb2 62.4(4) 2_656 2_657 ?
S1 Li4 Rb2 59.2(3) . 2_657 ?
Li3 Li4 Rb2 115.4(7) 2_646 2_657 ?
Na1 Li4 Rb2 67.4(4) 1_565 2_657 ?
Na1 Li4 Rb2 119.9(4) . 2_657 ?
Rb2 Li4 Rb2 72.5(3) 2_647 2_657 ?
O6 Li4 Rb1 64.1(6) 2_656 1_554 ?
O3 Li4 Rb1 38.8(5) 2_656 1_554 ?
O2 Li4 Rb1 120.5(11) . 1_554 ?
O5 Li4 Rb1 129.8(7) 2_646 1_554 ?
S2 Li4 Rb1 60.8(4) 2_656 1_554 ?
S1 Li4 Rb1 123.3(6) . 1_554 ?
Li3 Li4 Rb1 64.2(5) 2_646 1_554 ?
Na1 Li4 Rb1 64.7(4) 1_565 1_554 ?
Na1 Li4 Rb1 114.1(4) . 1_554 ?
Rb2 Li4 Rb1 178.9(6) 2_647 1_554 ?
Rb2 Li4 Rb1 108.3(6) 2_657 1_554 ?

_diffrn_measured_fraction_theta_max 0.995
_diffrn_reflns_theta_full        25.07
_diffrn_measured_fraction_theta_full 0.995
_refine_diff_density_max         1.079
_refine_diff_density_min         -1.342
_refine_diff_density_rms         0.213
