# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Fddd_a
_database_code_depnum_ccdc_archive 'CCDC 1965026'
loop_
_audit_author_name
_audit_author_address
'Wei Zhang'
;KTH Royal Institute of Technology
Sweden
;
_audit_update_record             
;
2019-11-11 deposited with the CCDC.	2020-01-03 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2016/6
_shelx_SHELXL_version_number     2016/6
_chemical_name_systematic        
"2,2',7,7'-Tetrakis[N,N-di(4-methoxyphenyl)amino]-9,9'-spirobifluorene bis(trifluoromethanesulfonyl)imide"
_chemical_name_common            Spiro(TFSI)2
_chemical_melting_point          ?
_chemical_formula_moiety         'C81 H68 N4 O8, 2(C F2 N O4 S2), 2(C F3), 2(F)'
_chemical_formula_sum            'C85 H68 F12 N6 O16 S4'
_chemical_formula_weight         1785.69

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      orthorhombic
_space_group_IT_number           70
_space_group_name_H-M_alt        'F d d d'
_space_group_name_Hall           '-F 2uv 2vw'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+3/4, -y+3/4, z'
'-x+3/4, y, -z+3/4'
'x, -y+3/4, -z+3/4'
'x, y+1/2, z+1/2'
'-x+3/4, -y+5/4, z+1/2'
'-x+3/4, y+1/2, -z+5/4'
'x, -y+5/4, -z+5/4'
'x+1/2, y, z+1/2'
'-x+5/4, -y+3/4, z+1/2'
'-x+5/4, y, -z+5/4'
'x+1/2, -y+3/4, -z+5/4'
'x+1/2, y+1/2, z'
'-x+5/4, -y+5/4, z'
'-x+5/4, y+1/2, -z+3/4'
'x+1/2, -y+5/4, -z+3/4'
'-x, -y, -z'
'x-3/4, y-3/4, -z'
'x-3/4, -y, z-3/4'
'-x, y-3/4, z-3/4'
'-x, -y+1/2, -z+1/2'
'x-3/4, y-1/4, -z+1/2'
'x-3/4, -y+1/2, z-1/4'
'-x, y-1/4, z-1/4'
'-x+1/2, -y, -z+1/2'
'x-1/4, y-3/4, -z+1/2'
'x-1/4, -y, z-1/4'
'-x+1/2, y-3/4, z-1/4'
'-x+1/2, -y+1/2, -z'
'x-1/4, y-1/4, -z'
'x-1/4, -y+1/2, z-3/4'
'-x+1/2, y-1/4, z-3/4'

_cell_length_a                   20.677(4)
_cell_length_b                   21.726(4)
_cell_length_c                   36.877(7)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     16566(6)
_cell_formula_units_Z            8
_cell_measurement_temperature    293(2)
_cell_measurement_reflns_used    9226
_cell_measurement_theta_min      2.40
_cell_measurement_theta_max      74.61

_exptl_crystal_description       block
_exptl_crystal_colour            greenish
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.432
_exptl_crystal_F_000             7360
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_absorpt_coefficient_mu    0.213
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   none
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      293(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            34241
_diffrn_reflns_av_unetI/netI     0.0414
_diffrn_reflns_av_R_equivalents  0.1080
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_limit_l_max       45
_diffrn_reflns_theta_min         1.467
_diffrn_reflns_theta_max         26.387
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measured_fraction_theta_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_point_group_measured_fraction_full 0.996
_reflns_number_total             4235
_reflns_number_gt                3867
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1000P)²] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_extinction_coef       0.00044(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_number_reflns         4235
_refine_ls_number_parameters     319
_refine_ls_number_restraints     3
_refine_ls_R_factor_all          0.0736
_refine_ls_R_factor_gt           0.0697
_refine_ls_wR_factor_ref         0.2323
_refine_ls_wR_factor_gt          0.2277
_refine_ls_goodness_of_fit_ref   1.915
_refine_ls_restrained_S_all      1.915
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O003 O 1.00324(7) 0.74569(7) 0.68148(4) 0.0376(4) Uani 1 1 d . . . . .
O004 O 0.64788(8) 0.51409(7) 0.76782(5) 0.0470(5) Uani 1 1 d . . . . .
N005 N 0.80437(8) 0.72054(8) 0.78168(5) 0.0335(4) Uani 1 1 d . . . . .
C1 C 0.875000 0.875000 0.875000 0.0215(6) Uani 1 4 d S T P . .
C007 C 0.82827(8) 0.83740(7) 0.85200(4) 0.0227(4) Uani 1 1 d . . . . .
C008 C 0.76339(8) 0.85150(8) 0.86134(5) 0.0237(4) Uani 1 1 d . . . . .
C009 C 0.71241(9) 0.82060(9) 0.84412(5) 0.0270(4) Uani 1 1 d . . . . .
H009 H 0.669701 0.829543 0.850009 0.032 Uiso 1 1 calc R U . . .
C00A C 0.84292(9) 0.79542(8) 0.82546(5) 0.0264(4) Uani 1 1 d . . . . .
H00A H 0.885573 0.787745 0.818864 0.032 Uiso 1 1 calc R U . . .
C00B C 0.79109(9) 0.76409(8) 0.80839(5) 0.0284(4) Uani 1 1 d . . . . .
C00C C 0.85731(10) 0.72949(9) 0.75741(5) 0.0315(5) Uani 1 1 d . . . . .
C00D C 0.72661(9) 0.77679(9) 0.81832(5) 0.0299(4) Uani 1 1 d . . . . .
H00D H 0.693116 0.755233 0.807279 0.036 Uiso 1 1 calc R U . . .
C00E C 0.95497(10) 0.74397(10) 0.70656(5) 0.0316(4) Uani 1 1 d . . . . .
C00G C 0.76462(9) 0.66790(9) 0.77717(6) 0.0334(5) Uani 1 1 d . . . . .
C00H C 0.90100(11) 0.68171(9) 0.75120(6) 0.0359(5) Uani 1 1 d . . . . .
H00H H 0.897554 0.645111 0.764142 0.043 Uiso 1 1 calc R U . . .
C00I C 0.75146(11) 0.64520(10) 0.74267(6) 0.0386(5) Uani 1 1 d . . . . .
H00I H 0.768589 0.664782 0.722410 0.046 Uiso 1 1 calc R U . . .
C00J C 0.86353(10) 0.78466(10) 0.73887(6) 0.0346(5) Uani 1 1 d . . . . .
H00J H 0.834850 0.816701 0.743456 0.041 Uiso 1 1 calc R U . . .
C00K C 0.73945(10) 0.63762(10) 0.80738(6) 0.0369(5) Uani 1 1 d . . . . .
H00K H 0.748876 0.652035 0.830526 0.044 Uiso 1 1 calc R U . . .
C00L C 0.94944(10) 0.68901(10) 0.72574(6) 0.0360(5) Uani 1 1 d . . . . .
H00L H 0.978433 0.657124 0.721392 0.043 Uiso 1 1 calc R U . . .
C00M C 0.68697(10) 0.56472(9) 0.76861(7) 0.0384(5) Uani 1 1 d . . . . .
C00N C 0.91253(10) 0.79225(10) 0.71342(5) 0.0354(5) Uani 1 1 d . . . . .
H00N H 0.916877 0.829348 0.701071 0.042 Uiso 1 1 calc R U . . .
C00O C 0.70085(10) 0.58665(10) 0.80320(7) 0.0399(5) Uani 1 1 d . . . . .
H00O H 0.684014 0.566821 0.823458 0.048 Uiso 1 1 calc R U . . .
C00P C 0.71278(10) 0.59333(11) 0.73838(7) 0.0400(5) Uani 1 1 d . . . . .
H00P H 0.704314 0.577977 0.715318 0.048 Uiso 1 1 calc R U . . .
C00Q C 1.00882(14) 0.80014(13) 0.65998(7) 0.0503(6) Uani 1 1 d . . . . .
H00B H 1.044365 0.795802 0.643435 0.075 Uiso 1 1 calc R U . . .
H00C H 0.969563 0.806302 0.646567 0.075 Uiso 1 1 calc R U . . .
H00E H 1.016271 0.834892 0.675508 0.075 Uiso 1 1 calc R U . . .
C00R C 0.62980(13) 0.49120(12) 0.73303(9) 0.0549(7) Uani 1 1 d . . . . .
H00F H 0.602507 0.455796 0.735925 0.082 Uiso 1 1 calc R U . . .
H00G H 0.606818 0.522555 0.719975 0.082 Uiso 1 1 calc R U . . .
H00M H 0.667917 0.479835 0.719754 0.082 Uiso 1 1 calc R U . . .
S001 S 0.625000 0.44337(5) 0.625000 0.0677(4) Uani 1 2 d S T P . .
S002 S 0.75948(6) 0.47706(6) 0.60228(3) 0.0409(3) Uani 0.5 1 d . . P . .
F00S F 0.42114(17) 0.57480(18) 0.65760(9) 0.0635(9) Uani 0.5 1 d . . P . .
F00T F 0.45498(17) 0.5632(2) 0.60256(9) 0.0674(10) Uani 0.5 1 d . . P . .
F00U F 0.6451(2) 0.5467(2) 0.65902(10) 0.0688(10) Uani 0.5 1 d . . P . .
F00V F 0.52059(19) 0.59441(17) 0.64411(13) 0.0740(11) Uani 0.5 1 d . . P . .
F00W F 0.5975(2) 0.55179(17) 0.64901(10) 0.0668(9) Uani 0.5 1 d D . P . .
F2 F 0.7232(2) 0.5037(3) 0.63172(14) 0.0888(13) Uiso 0.5 1 d . . P . .
O00X O 0.81725(18) 0.44481(19) 0.61112(11) 0.0543(9) Uani 0.5 1 d . . P . .
N00Y N 0.7065(2) 0.4639(2) 0.63133(12) 0.0474(10) Uani 0.5 1 d . . P . .
O00Z O 0.73973(19) 0.4780(2) 0.56503(10) 0.0557(10) Uani 0.5 1 d . . P . .
O00F O 0.63169(12) 0.41452(12) 0.59144(7) 0.0772(7) Uani 1 1 d . . . . .
C2 C 0.5881(3) 0.5155(3) 0.62050(16) 0.0553(13) Uiso 0.5 1 d D . P . .
C3 C 0.4707(2) 0.5576(2) 0.63738(14) 0.0429(10) Uiso 0.5 1 d . . P . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O003 C00E 1.361(2) . ?
O003 C00Q 1.429(3) . ?
O004 C00M 1.365(2) . ?
O004 C00R 1.426(3) . ?
N005 C00B 1.393(2) . ?
N005 C00G 1.418(2) . ?
N005 C00C 1.427(2) . ?
C1 C007 1.5233(16) . ?
C1 C007 1.5233(16) 3_656 ?
C1 C007 1.5233(17) 2_665 ?
C1 C007 1.5233(16) 4_566 ?
C007 C00A 1.372(2) . ?
C007 C008 1.419(2) . ?
C008 C009 1.402(2) . ?
C008 C008 1.434(3) 4_566 ?
C009 C00D 1.377(3) . ?
C009 H009 0.9300 . ?
C00A C00B 1.417(2) . ?
C00A H00A 0.9300 . ?
C00B C00D 1.410(3) . ?
C00C C00J 1.386(3) . ?
C00C C00H 1.395(3) . ?
C00D H00D 0.9300 . ?
C00E C00L 1.392(3) . ?
C00E C00N 1.391(3) . ?
C00G C00I 1.391(3) . ?
C00G C00K 1.395(3) . ?
C00H C00L 1.382(3) . ?
C00H H00H 0.9300 . ?
C00I C00P 1.391(3) . ?
C00I H00I 0.9300 . ?
C00J C00N 1.391(3) . ?
C00J H00J 0.9300 . ?
C00K C00O 1.374(3) . ?
C00K H00K 0.9300 . ?
C00L H00L 0.9300 . ?
C00M C00P 1.384(3) . ?
C00M C00O 1.391(3) . ?
C00N H00N 0.9300 . ?
C00O H00O 0.9300 . ?
C00P H00P 0.9300 . ?
C00Q H00B 0.9600 . ?
C00Q H00C 0.9600 . ?
C00Q H00E 0.9600 . ?
C00R H00F 0.9600 . ?
C00R H00G 0.9600 . ?
C00R H00M 0.9600 . ?
S001 O00F 1.394(3) . ?
S001 O00F 1.394(3) 11 ?
S001 C2 1.751(6) 11 ?
S001 C2 1.751(6) . ?
S001 N00Y 1.759(5) . ?
S001 N00Y 1.759(5) 11 ?
S002 O00X 1.423(4) . ?
S002 O00Z 1.433(4) . ?
S002 N00Y 1.559(5) . ?
S002 C3 1.836(5) 11 ?
F00S C3 1.322(6) . ?
F00T C3 1.330(6) . ?
F00U C2 1.328(7) 11 ?
F00V C3 1.329(6) . ?
F00W C2 1.328(6) . ?
F00W C2 1.707(7) 11 ?
F2 C2 1.297(7) 11 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C00E O003 C00Q 117.31(17) . . ?
C00M O004 C00R 117.1(2) . . ?
C00B N005 C00G 121.10(16) . . ?
C00B N005 C00C 120.14(15) . . ?
C00G N005 C00C 118.73(15) . . ?
C007 C1 C007 115.13(13) . 3_656 ?
C007 C1 C007 112.32(12) . 2_665 ?
C007 C1 C007 101.28(13) 3_656 2_665 ?
C007 C1 C007 101.27(13) . 4_566 ?
C007 C1 C007 112.31(12) 3_656 4_566 ?
C007 C1 C007 115.14(13) 2_665 4_566 ?
C00A C007 C008 121.71(16) . . ?
C00A C007 C1 127.88(14) . . ?
C008 C007 C1 110.41(13) . . ?
C009 C008 C007 119.84(15) . . ?
C009 C008 C008 131.24(10) . 4_566 ?
C007 C008 C008 108.93(10) . 4_566 ?
C00D C009 C008 118.93(17) . . ?
C00D C009 H009 120.5 . . ?
C008 C009 H009 120.5 . . ?
C007 C00A C00B 118.00(16) . . ?
C007 C00A H00A 121.0 . . ?
C00B C00A H00A 121.0 . . ?
N005 C00B C00D 120.20(17) . . ?
N005 C00B C00A 119.42(17) . . ?
C00D C00B C00A 120.38(17) . . ?
C00J C00C C00H 120.17(18) . . ?
C00J C00C N005 119.89(18) . . ?
C00H C00C N005 119.88(18) . . ?
C009 C00D C00B 121.08(17) . . ?
C009 C00D H00D 119.5 . . ?
C00B C00D H00D 119.5 . . ?
O003 C00E C00L 115.38(18) . . ?
O003 C00E C00N 124.43(19) . . ?
C00L C00E C00N 120.19(18) . . ?
C00I C00G C00K 119.35(19) . . ?
C00I C00G N005 120.44(19) . . ?
C00K C00G N005 120.19(18) . . ?
C00L C00H C00C 119.7(2) . . ?
C00L C00H H00H 120.2 . . ?
C00C C00H H00H 120.2 . . ?
C00P C00I C00G 120.3(2) . . ?
C00P C00I H00I 119.9 . . ?
C00G C00I H00I 119.9 . . ?
C00C C00J C00N 120.21(19) . . ?
C00C C00J H00J 119.9 . . ?
C00N C00J H00J 119.9 . . ?
C00O C00K C00G 120.5(2) . . ?
C00O C00K H00K 119.8 . . ?
C00G C00K H00K 119.8 . . ?
C00H C00L C00E 120.19(19) . . ?
C00H C00L H00L 119.9 . . ?
C00E C00L H00L 119.9 . . ?
O004 C00M C00P 125.0(2) . . ?
O004 C00M C00O 114.7(2) . . ?
C00P C00M C00O 120.35(18) . . ?
C00J C00N C00E 119.5(2) . . ?
C00J C00N H00N 120.2 . . ?
C00E C00N H00N 120.2 . . ?
C00K C00O C00M 119.9(2) . . ?
C00K C00O H00O 120.0 . . ?
C00M C00O H00O 120.0 . . ?
C00M C00P C00I 119.6(2) . . ?
C00M C00P H00P 120.2 . . ?
C00I C00P H00P 120.2 . . ?
O003 C00Q H00B 109.5 . . ?
O003 C00Q H00C 109.5 . . ?
H00B C00Q H00C 109.5 . . ?
O003 C00Q H00E 109.5 . . ?
H00B C00Q H00E 109.5 . . ?
H00C C00Q H00E 109.5 . . ?
O004 C00R H00F 109.5 . . ?
O004 C00R H00G 109.5 . . ?
H00F C00R H00G 109.5 . . ?
O004 C00R H00M 109.5 . . ?
H00F C00R H00M 109.5 . . ?
H00G C00R H00M 109.5 . . ?
O00F S001 O00F 126.6(2) . 11 ?
O00F S001 C2 116.3(2) . 11 ?
O00F S001 C2 111.2(2) 11 11 ?
O00F S001 C2 111.2(2) . . ?
O00F S001 C2 116.3(2) 11 . ?
C2 S001 C2 52.9(4) 11 . ?
O00F S001 N00Y 97.86(19) . . ?
O00F S001 N00Y 95.23(18) 11 . ?
C2 S001 N00Y 49.0(2) 11 . ?
C2 S001 N00Y 101.7(2) . . ?
O00F S001 N00Y 95.23(18) . 11 ?
O00F S001 N00Y 97.86(19) 11 11 ?
C2 S001 N00Y 101.7(2) 11 11 ?
C2 S001 N00Y 49.0(2) . 11 ?
N00Y S001 N00Y 150.6(3) . 11 ?
O00X S002 O00Z 117.8(3) . . ?
O00X S002 N00Y 110.0(2) . . ?
O00Z S002 N00Y 117.4(2) . . ?
O00X S002 C3 103.5(2) . 11 ?
O00Z S002 C3 104.4(2) . 11 ?
N00Y S002 C3 100.9(2) . 11 ?
C2 F00W C2 60.4(4) . 11 ?
S002 N00Y S001 129.0(3) . . ?
F2 C2 F00U 107.7(5) 11 11 ?
F2 C2 F00W 108.0(5) 11 . ?
F00U C2 F00W 108.0(5) 11 . ?
F2 C2 S001 104.7(5) 11 . ?
F00U C2 S001 114.9(4) 11 . ?
F00W C2 S001 113.1(4) . . ?
F00S C3 F00T 109.2(4) . . ?
F00S C3 F00V 109.0(4) . . ?
F00T C3 F00V 108.3(5) . . ?
F00S C3 S002 109.0(3) . 11 ?
F00T C3 S002 110.0(4) . 11 ?
F00V C3 S002 111.2(4) . 11 ?

_refine_diff_density_max         0.579
_refine_diff_density_min         -0.660
_refine_diff_density_rms         0.080


_chemical_properties_physical    Air-sensitive,Light-sensitive
