# Electronic Supplementary Material (ESI) for ChemComm.
# This journal is © The Royal Society of Chemistry 2020

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_jwu59
_database_code_depnum_ccdc_archive 'CCDC 1972215'
loop_
_audit_author_name
_audit_author_address
'Sebastian Dechert'
;University of Goettingen
Germany
;
_audit_update_record             
;
2019-12-16 deposited with the CCDC.	2020-02-27 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2018/3
_shelx_SHELXL_version_number     2018/3
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C84 H138 Cl16 Dy6 K4 O6'
_chemical_formula_sum            'C84 H138 Cl16 Dy6 K4 O6'
_chemical_formula_weight         2942.54

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   13.9788(2)
_cell_length_b                   16.4794(2)
_cell_length_c                   37.2813(6)
_cell_angle_alpha                85.9330(10)
_cell_angle_beta                 84.3340(10)
_cell_angle_gamma                70.8680(10)
_cell_volume                     8067.4(2)
_cell_formula_units_Z            3
_cell_measurement_temperature    133(2)
_cell_measurement_reflns_used    94553
_cell_measurement_theta_min      1.099
_cell_measurement_theta_max      25.693

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.817
_exptl_crystal_F_000             4302
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.500
_exptl_crystal_size_mid          0.410
_exptl_crystal_size_min          0.360
_exptl_absorpt_coefficient_mu    4.711
_shelx_estimated_absorpt_T_min   0.202
_shelx_estimated_absorpt_T_max   0.282
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_correction_T_min  0.1681
_exptl_absorpt_correction_T_max  0.3283
_exptl_absorpt_process_details   'X-RED (Stoe & Cie, 2015)'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      133(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Stoe IPDS II'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            94553
_diffrn_reflns_av_unetI/netI     0.0225
_diffrn_reflns_av_R_equivalents  0.0314
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_l_min       -45
_diffrn_reflns_limit_l_max       45
_diffrn_reflns_theta_min         1.099
_diffrn_reflns_theta_max         25.693
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.987
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.987
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             30247
_reflns_number_gt                26742
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'X-AREA (Stoe & Cie, 2015)'
_computing_cell_refinement       'X-AREA (Stoe & Cie, 2015)'
_computing_data_reduction        'X-AREA (Stoe & Cie, 2015)'
_computing_structure_solution    'SHELXT-2018/2 (Sheldrick, 2018)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_molecular_graphics    'DIAMOND (Brandenburg, 2012)'
_computing_publication_material  'SHELXL-2018/3 (Sheldrick, 2018)'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0530P)²+32.7065P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         30247
_refine_ls_number_parameters     1704
_refine_ls_number_restraints     260
_refine_ls_R_factor_all          0.0439
_refine_ls_R_factor_gt           0.0372
_refine_ls_wR_factor_ref         0.1059
_refine_ls_wR_factor_gt          0.0982
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_restrained_S_all      1.046
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.12621(2) 0.76801(2) 0.91982(2) 0.03003(6) Uani 1 1 d . . . . .
Dy2 Dy 0.15022(2) 0.96926(2) 0.85647(2) 0.03051(6) Uani 1 1 d . . . . .
Dy3 Dy 0.37449(2) 0.83924(2) 0.92303(2) 0.03253(6) Uani 1 1 d . . . . .
Dy4 Dy 0.49691(2) 0.56785(2) 0.74889(2) 0.03004(6) Uani 1 1 d . . . . .
Dy5 Dy 0.50250(2) 0.35925(2) 0.81358(2) 0.03095(6) Uani 1 1 d . . . . .
Dy6 Dy 0.28197(2) 0.45953(2) 0.74305(2) 0.03082(6) Uani 1 1 d . . . . .
K1 K 0.46624(10) 0.86099(8) 0.81177(3) 0.0403(3) Uani 1 1 d . . . . .
K2 K 0.19174(9) 0.45367(8) 0.85671(3) 0.0372(3) Uani 1 1 d . . . . .
K3 K 0.42393(10) 0.60069(8) 0.86836(3) 0.0390(3) Uani 1 1 d . . . . .
K4 K 0.18682(10) 0.72501(9) 0.80007(3) 0.0433(3) Uani 1 1 d . . . . .
Cl1 Cl 0.15844(10) 0.92273(8) 0.93273(3) 0.0339(3) Uani 1 1 d . . . . .
Cl2 Cl 0.02619(10) 0.86942(8) 0.86533(3) 0.0360(3) Uani 1 1 d . . . . .
Cl3 Cl 0.33427(10) 0.97831(9) 0.87428(3) 0.0366(3) Uani 1 1 d . . . . .
Cl4 Cl 0.30894(10) 0.70524(9) 0.94861(3) 0.0370(3) Uani 1 1 d . . . . .
Cl5 Cl 0.17520(11) 0.63360(9) 0.87890(3) 0.0393(3) Uani 1 1 d . . . . .
Cl6 Cl 0.22616(11) 0.92287(9) 0.79153(3) 0.0392(3) Uani 1 1 d . . . . .
Cl7 Cl 0.42271(11) 0.70153(9) 0.78875(4) 0.0387(3) Uani 1 1 d . . . . .
Cl8 Cl 0.52126(10) 0.74536(9) 0.88023(4) 0.0393(3) Uani 1 1 d . . . . .
Cl9 Cl 0.27404(10) 0.79801(8) 0.86751(3) 0.0324(3) Uani 1 1 d . . . . .
Cl10 Cl 0.49945(10) 0.40084(8) 0.73707(3) 0.0334(3) Uani 1 1 d . . . . .
Cl11 Cl 0.33298(10) 0.32729(8) 0.79442(3) 0.0360(3) Uani 1 1 d . . . . .
Cl12 Cl 0.32119(10) 0.60544(9) 0.71677(3) 0.0375(3) Uani 1 1 d . . . . .
Cl14 Cl 0.35535(10) 0.52191(8) 0.80011(3) 0.0319(3) Uani 1 1 d . . . . .
Cl15 Cl 0.42084(11) 0.40673(9) 0.87783(3) 0.0371(3) Uani 1 1 d . . . . .
Cl16 Cl 0.11746(10) 0.54733(9) 0.78096(3) 0.0385(3) Uani 1 1 d . . . . .
Cl17 Cl 0.60224(10) 0.47799(9) 0.80490(3) 0.0356(3) Uani 1 1 d . . . . .
O11 O 0.6617(4) 0.8490(4) 0.82139(14) 0.0646(13) Uani 1 1 d . . . . .
O12 O 0.5067(4) 0.9617(3) 0.75529(13) 0.0630(13) Uani 1 1 d . . . . .
O22 O -0.0088(3) 0.4627(3) 0.87000(12) 0.0523(11) Uani 1 1 d . . . . .
O31 O 0.5685(4) 0.5275(4) 0.91216(14) 0.0701(15) Uani 1 1 d . . . . .
O41 O 0.0463(4) 0.8039(3) 0.75320(12) 0.0529(11) Uani 1 1 d D . . . .
C11 C -0.0622(4) 0.7985(4) 0.94838(15) 0.0384(12) Uani 1 1 d . . . . .
C12 C -0.0221(4) 0.7087(4) 0.94454(15) 0.0391(12) Uani 1 1 d . . . . .
C13 C 0.0551(4) 0.6754(3) 0.96851(13) 0.0356(12) Uani 1 1 d . . . . .
C14 C 0.0623(4) 0.7451(4) 0.98748(14) 0.0354(11) Uani 1 1 d . . . . .
C15 C -0.0107(4) 0.8212(4) 0.97467(14) 0.0347(11) Uani 1 1 d . . . . .
C16 C -0.1548(5) 0.8588(4) 0.93153(16) 0.0456(14) Uani 1 1 d . . . . .
H16A H -0.215099 0.864898 0.948268 0.068 Uiso 1 1 calc R U . . .
H16B H -0.163197 0.835490 0.909036 0.068 Uiso 1 1 calc R U . . .
H16C H -0.145995 0.915237 0.926374 0.068 Uiso 1 1 calc R U . . .
C17 C -0.0619(5) 0.6574(5) 0.92148(17) 0.0499(15) Uani 1 1 d . . . . .
H17A H -0.120212 0.645138 0.934595 0.075 Uiso 1 1 calc R U . . .
H17B H -0.008304 0.603258 0.915751 0.075 Uiso 1 1 calc R U . . .
H17C H -0.083001 0.690503 0.899080 0.075 Uiso 1 1 calc R U . . .
C18 C 0.1148(5) 0.5824(4) 0.97474(17) 0.0500(15) Uani 1 1 d . . . . .
H18A H 0.075973 0.555595 0.992176 0.075 Uiso 1 1 calc R U . . .
H18B H 0.179459 0.577788 0.984227 0.075 Uiso 1 1 calc R U . . .
H18C H 0.128179 0.553159 0.951907 0.075 Uiso 1 1 calc R U . . .
C19 C 0.1263(5) 0.7372(4) 1.01825(14) 0.0413(13) Uani 1 1 d . . . . .
H19A H 0.090935 0.723019 1.040607 0.062 Uiso 1 1 calc R U . . .
H19B H 0.138501 0.791777 1.020540 0.062 Uiso 1 1 calc R U . . .
H19C H 0.191361 0.691537 1.013752 0.062 Uiso 1 1 calc R U . . .
C20 C -0.0362(5) 0.9076(4) 0.99011(15) 0.0415(13) Uani 1 1 d . . . . .
H20A H -0.092818 0.915552 1.008683 0.062 Uiso 1 1 calc R U . . .
H20B H -0.055609 0.952263 0.970904 0.062 Uiso 1 1 calc R U . . .
H20C H 0.023188 0.911734 1.000856 0.062 Uiso 1 1 calc R U . . .
C21 C 0.1117(4) 1.1340(4) 0.84191(14) 0.0368(12) Uani 1 1 d . . . . .
C22 C 0.0685(4) 1.1263(3) 0.87763(14) 0.0362(12) Uani 1 1 d . . . . .
C23 C -0.0138(4) 1.0953(3) 0.87566(14) 0.0364(12) Uani 1 1 d . . . . .
C24 C -0.0223(4) 1.0849(3) 0.83893(15) 0.0361(12) Uani 1 1 d . . . . .
C25 C 0.0543(5) 1.1096(4) 0.81809(15) 0.0384(12) Uani 1 1 d . . . . .
C26 C 0.1963(5) 1.1707(4) 0.83107(17) 0.0466(14) Uani 1 1 d . . . . .
H26A H 0.167468 1.231657 0.823897 0.070 Uiso 1 1 calc R U . . .
H26B H 0.239090 1.139505 0.810745 0.070 Uiso 1 1 calc R U . . .
H26C H 0.237462 1.164840 0.851506 0.070 Uiso 1 1 calc R U . . .
C27 C 0.1023(5) 1.1511(4) 0.91098(15) 0.0430(13) Uani 1 1 d . . . . .
H27A H 0.087727 1.213506 0.910335 0.065 Uiso 1 1 calc R U . . .
H27B H 0.175490 1.122312 0.912064 0.065 Uiso 1 1 calc R U . . .
H27C H 0.065782 1.133627 0.932326 0.065 Uiso 1 1 calc R U . . .
C28 C -0.0868(5) 1.0835(4) 0.90669(16) 0.0469(14) Uani 1 1 d . . . . .
H28A H -0.145187 1.136190 0.908992 0.070 Uiso 1 1 calc R U . . .
H28B H -0.052286 1.071131 0.929059 0.070 Uiso 1 1 calc R U . . .
H28C H -0.110146 1.035500 0.902142 0.070 Uiso 1 1 calc R U . . .
C29 C -0.1058(5) 1.0600(4) 0.82426(17) 0.0450(14) Uani 1 1 d . . . . .
H29A H -0.163845 1.111712 0.820198 0.068 Uiso 1 1 calc R U . . .
H29B H -0.127210 1.020700 0.841695 0.068 Uiso 1 1 calc R U . . .
H29C H -0.080241 1.031477 0.801420 0.068 Uiso 1 1 calc R U . . .
C30 C 0.0654(5) 1.1188(4) 0.77762(15) 0.0445(14) Uani 1 1 d . . . . .
H30A H 0.023835 1.176557 0.769790 0.067 Uiso 1 1 calc R U . . .
H30B H 0.042716 1.075901 0.767207 0.067 Uiso 1 1 calc R U . . .
H30C H 0.136779 1.109886 0.769473 0.067 Uiso 1 1 calc R U . . .
C31 C 0.4998(5) 0.9058(4) 0.94779(16) 0.0433(14) Uani 1 1 d . . . . .
C32 C 0.4042(5) 0.9453(4) 0.96632(15) 0.0412(13) Uani 1 1 d . . . . .
C33 C 0.3784(4) 0.8826(4) 0.98945(15) 0.0401(13) Uani 1 1 d . . . . .
C34 C 0.4586(5) 0.8042(4) 0.98521(14) 0.0406(13) Uani 1 1 d . . . . .
C35 C 0.5345(5) 0.8183(4) 0.95971(15) 0.0417(13) Uani 1 1 d . . . . .
C36 C 0.5581(6) 0.9506(5) 0.92226(19) 0.0610(19) Uani 1 1 d . . . . .
H36A H 0.601539 0.971271 0.935801 0.091 Uiso 1 1 calc R U . . .
H36B H 0.510451 0.999427 0.909899 0.091 Uiso 1 1 calc R U . . .
H36C H 0.600353 0.910278 0.904418 0.091 Uiso 1 1 calc R U . . .
C37 C 0.3451(6) 1.0399(4) 0.96539(19) 0.0586(18) Uani 1 1 d . . . . .
H37A H 0.362575 1.066991 0.985247 0.088 Uiso 1 1 calc R U . . .
H37B H 0.272208 1.047835 0.967971 0.088 Uiso 1 1 calc R U . . .
H37C H 0.362139 1.066469 0.942355 0.088 Uiso 1 1 calc R U . . .
C38 C 0.2870(5) 0.8980(4) 1.01610(16) 0.0494(15) Uani 1 1 d . . . . .
H38A H 0.293158 0.932798 1.035449 0.074 Uiso 1 1 calc R U . . .
H38B H 0.282707 0.842749 1.026372 0.074 Uiso 1 1 calc R U . . .
H38C H 0.225538 0.928435 1.003869 0.074 Uiso 1 1 calc R U . . .
C39 C 0.4689(5) 0.7218(4) 1.00662(15) 0.0445(14) Uani 1 1 d . . . . .
H39A H 0.505525 0.720169 1.027911 0.067 Uiso 1 1 calc R U . . .
H39B H 0.506700 0.673162 0.991675 0.067 Uiso 1 1 calc R U . . .
H39C H 0.401272 0.718231 1.014302 0.067 Uiso 1 1 calc R U . . .
C40 C 0.6367(5) 0.7549(4) 0.95011(16) 0.0498(15) Uani 1 1 d . . . . .
H40A H 0.686413 0.762971 0.965071 0.075 Uiso 1 1 calc R U . . .
H40B H 0.657032 0.763723 0.924606 0.075 Uiso 1 1 calc R U . . .
H40C H 0.633503 0.696428 0.954360 0.075 Uiso 1 1 calc R U . . .
C41 C 0.6336(5) 0.6410(4) 0.72874(14) 0.0421(14) Uani 1 1 d . . . . .
C42 C 0.5559(5) 0.6775(4) 0.70556(15) 0.0400(13) Uani 1 1 d . . . . .
C43 C 0.5554(5) 0.6122(4) 0.68265(15) 0.0403(13) Uani 1 1 d . . . . .
C44 C 0.6320(4) 0.5355(4) 0.69251(14) 0.0385(12) Uani 1 1 d . . . . .
C45 C 0.6804(4) 0.5545(4) 0.72093(15) 0.0399(13) Uani 1 1 d . . . . .
C46 C 0.6703(6) 0.6864(5) 0.75573(18) 0.0609(19) Uani 1 1 d . . . . .
H46A H 0.739996 0.684951 0.748092 0.091 Uiso 1 1 calc R U . . .
H46B H 0.668843 0.657424 0.779557 0.091 Uiso 1 1 calc R U . . .
H46C H 0.625935 0.746298 0.757001 0.091 Uiso 1 1 calc R U . . .
C47 C 0.4896(6) 0.7696(4) 0.7027(2) 0.0597(18) Uani 1 1 d . . . . .
H47A H 0.512668 0.797751 0.681121 0.090 Uiso 1 1 calc R U . . .
H47B H 0.493532 0.799122 0.724143 0.090 Uiso 1 1 calc R U . . .
H47C H 0.419129 0.772155 0.700962 0.090 Uiso 1 1 calc R U . . .
C48 C 0.4956(6) 0.6252(5) 0.65020(16) 0.0553(17) Uani 1 1 d . . . . .
H48A H 0.527786 0.651317 0.630190 0.083 Uiso 1 1 calc R U . . .
H48B H 0.426122 0.663128 0.656038 0.083 Uiso 1 1 calc R U . . .
H48C H 0.493703 0.569533 0.643193 0.083 Uiso 1 1 calc R U . . .
C49 C 0.6658(5) 0.4526(4) 0.67297(17) 0.0533(16) Uani 1 1 d . . . . .
H49A H 0.717502 0.454430 0.653457 0.080 Uiso 1 1 calc R U . . .
H49B H 0.607374 0.444915 0.662845 0.080 Uiso 1 1 calc R U . . .
H49C H 0.694453 0.404381 0.689924 0.080 Uiso 1 1 calc R U . . .
C50 C 0.7758(5) 0.4931(5) 0.73541(19) 0.0617(19) Uani 1 1 d . . . . .
H50A H 0.827353 0.472712 0.715377 0.092 Uiso 1 1 calc R U . . .
H50B H 0.760698 0.444078 0.748098 0.092 Uiso 1 1 calc R U . . .
H50C H 0.801514 0.522782 0.752178 0.092 Uiso 1 1 calc R U . . .
C51 C 0.6792(5) 0.2620(4) 0.83427(16) 0.0413(13) Uani 1 1 d . . . . .
C52 C 0.6094(5) 0.2265(4) 0.85380(15) 0.0408(13) Uani 1 1 d . . . . .
C53 C 0.5647(5) 0.1921(4) 0.82862(15) 0.0395(12) Uani 1 1 d . . . . .
C54 C 0.6101(4) 0.2042(3) 0.79380(14) 0.0375(12) Uani 1 1 d . . . . .
C55 C 0.6810(4) 0.2479(4) 0.79733(15) 0.0379(12) Uani 1 1 d . . . . .
C56 C 0.7502(5) 0.2979(4) 0.8508(2) 0.0571(17) Uani 1 1 d . . . . .
H56A H 0.815140 0.252354 0.853698 0.086 Uiso 1 1 calc R U . . .
H56B H 0.720015 0.320238 0.874419 0.086 Uiso 1 1 calc R U . . .
H56C H 0.761696 0.344537 0.834989 0.086 Uiso 1 1 calc R U . . .
C57 C 0.5928(6) 0.2168(5) 0.89377(17) 0.0567(17) Uani 1 1 d . . . . .
H57A H 0.638072 0.161043 0.902141 0.085 Uiso 1 1 calc R U . . .
H57B H 0.522019 0.220128 0.900353 0.085 Uiso 1 1 calc R U . . .
H57C H 0.607300 0.262960 0.905077 0.085 Uiso 1 1 calc R U . . .
C58 C 0.4921(5) 0.1421(4) 0.83786(19) 0.0521(16) Uani 1 1 d . . . . .
H58A H 0.529209 0.084374 0.847207 0.078 Uiso 1 1 calc R U . . .
H58B H 0.460182 0.137541 0.816159 0.078 Uiso 1 1 calc R U . . .
H58C H 0.439534 0.171776 0.856231 0.078 Uiso 1 1 calc R U . . .
C59 C 0.5935(5) 0.1692(4) 0.75984(16) 0.0504(15) Uani 1 1 d . . . . .
H59A H 0.638568 0.109714 0.757737 0.076 Uiso 1 1 calc R U . . .
H59B H 0.608493 0.204183 0.739042 0.076 Uiso 1 1 calc R U . . .
H59C H 0.522686 0.170812 0.760488 0.076 Uiso 1 1 calc R U . . .
C60 C 0.7512(5) 0.2673(4) 0.76750(18) 0.0507(15) Uani 1 1 d . . . . .
H60A H 0.813950 0.218317 0.765140 0.076 Uiso 1 1 calc R U . . .
H60B H 0.767247 0.318466 0.773024 0.076 Uiso 1 1 calc R U . . .
H60C H 0.718311 0.277959 0.744809 0.076 Uiso 1 1 calc R U . . .
C61 C 0.2072(4) 0.3547(4) 0.71385(14) 0.0379(12) Uani 1 1 d . . . . .
C62 C 0.1450(4) 0.4386(4) 0.70418(14) 0.0386(12) Uani 1 1 d . . . . .
C63 C 0.2031(4) 0.4783(4) 0.68038(13) 0.0357(12) Uani 1 1 d . . . . .
C64 C 0.3029(4) 0.4181(4) 0.67523(14) 0.0365(12) Uani 1 1 d . . . . .
C65 C 0.3043(4) 0.3424(4) 0.69589(14) 0.0377(12) Uani 1 1 d . . . . .
C66 C 0.1729(5) 0.2868(4) 0.73528(16) 0.0509(16) Uani 1 1 d . . . . .
H66A H 0.152911 0.252485 0.718842 0.076 Uiso 1 1 calc R U . . .
H66B H 0.114811 0.314402 0.752165 0.076 Uiso 1 1 calc R U . . .
H66C H 0.228730 0.249377 0.748774 0.076 Uiso 1 1 calc R U . . .
C67 C 0.0328(5) 0.4737(5) 0.71437(16) 0.0503(15) Uani 1 1 d . . . . .
H67A H -0.004261 0.460530 0.695791 0.075 Uiso 1 1 calc R U . . .
H67B H 0.012609 0.536138 0.716378 0.075 Uiso 1 1 calc R U . . .
H67C H 0.016763 0.447289 0.737578 0.075 Uiso 1 1 calc R U . . .
C68 C 0.1640(5) 0.5638(4) 0.66072(15) 0.0464(14) Uani 1 1 d . . . . .
H68A H 0.141134 0.555973 0.637580 0.070 Uiso 1 1 calc R U . . .
H68B H 0.218350 0.589553 0.656421 0.070 Uiso 1 1 calc R U . . .
H68C H 0.106893 0.601878 0.675315 0.070 Uiso 1 1 calc R U . . .
C69 C 0.3868(5) 0.4306(4) 0.64977(15) 0.0423(13) Uani 1 1 d . . . . .
H69A H 0.386524 0.405887 0.626655 0.063 Uiso 1 1 calc R U . . .
H69B H 0.452032 0.402074 0.659971 0.063 Uiso 1 1 calc R U . . .
H69C H 0.376759 0.492242 0.645972 0.063 Uiso 1 1 calc R U . . .
C70 C 0.3907(5) 0.2594(4) 0.69581(17) 0.0501(15) Uani 1 1 d . . . . .
H70A H 0.380485 0.221239 0.678629 0.075 Uiso 1 1 calc R U . . .
H70B H 0.393622 0.231806 0.720027 0.075 Uiso 1 1 calc R U . . .
H70C H 0.454629 0.270875 0.688717 0.075 Uiso 1 1 calc R U . . .
C111 C 0.7412(5) 0.7758(5) 0.8344(2) 0.0635(19) Uani 1 1 d . . . . .
H11A H 0.728399 0.721850 0.829979 0.076 Uiso 1 1 calc R U . . .
H11B H 0.745200 0.778818 0.860577 0.076 Uiso 1 1 calc R U . . .
C112 C 0.8395(6) 0.7788(6) 0.8136(2) 0.074(2) Uani 1 1 d . . . . .
H11C H 0.863768 0.733587 0.795583 0.089 Uiso 1 1 calc R U . . .
H11D H 0.893260 0.771400 0.830084 0.089 Uiso 1 1 calc R U . . .
C113 C 0.8096(7) 0.8682(6) 0.7952(2) 0.080(2) Uani 1 1 d . . . . .
H11E H 0.859658 0.897188 0.798551 0.096 Uiso 1 1 calc R U . . .
H11F H 0.805209 0.864757 0.769009 0.096 Uiso 1 1 calc R U . . .
C114 C 0.7083(6) 0.9150(6) 0.8131(2) 0.073(2) Uani 1 1 d . . . . .
H11G H 0.715468 0.941242 0.835390 0.088 Uiso 1 1 calc R U . . .
H11H H 0.667987 0.960679 0.796781 0.088 Uiso 1 1 calc R U . . .
C115 C 0.5753(6) 0.9578(5) 0.7241(2) 0.0598(18) Uani 1 1 d . . . . .
H11I H 0.611322 0.897231 0.718077 0.072 Uiso 1 1 calc R U . . .
H11J H 0.626383 0.985030 0.728454 0.072 Uiso 1 1 calc R U . . .
C116 C 0.5135(8) 1.0052(6) 0.6935(2) 0.089(3) Uani 1 1 d . . . . .
H11K H 0.528164 0.969455 0.672133 0.107 Uiso 1 1 calc R U . . .
H11L H 0.527371 1.059667 0.686553 0.107 Uiso 1 1 calc R U . . .
C117 C 0.4050(7) 1.0223(6) 0.7092(2) 0.078(2) Uani 1 1 d . . . . .
H11M H 0.359600 1.077111 0.699300 0.093 Uiso 1 1 calc R U . . .
H11N H 0.379532 0.975023 0.704376 0.093 Uiso 1 1 calc R U . . .
C118 C 0.4127(6) 1.0266(5) 0.74815(19) 0.0612(19) Uani 1 1 d . . . . .
H11O H 0.413679 1.084062 0.753948 0.073 Uiso 1 1 calc R U . . .
H11P H 0.355009 1.014619 0.762471 0.073 Uiso 1 1 calc R U . . .
O21A O 0.1799(18) 0.3458(17) 0.9096(5) 0.056(6) Uani 0.62(3) 1 d D U P A 1
C21A C 0.2713(18) 0.2790(19) 0.9181(4) 0.062(6) Uani 0.62(3) 1 d D U P A 1
H21A H 0.330044 0.283629 0.901923 0.075 Uiso 0.62(3) 1 calc R U P A 1
H21B H 0.264700 0.221563 0.916043 0.075 Uiso 0.62(3) 1 calc R U P A 1
C22A C 0.2830(11) 0.2942(15) 0.9562(4) 0.080(5) Uani 0.62(3) 1 d D U P A 1
H22A H 0.311095 0.341713 0.957510 0.097 Uiso 0.62(3) 1 calc R U P A 1
H22B H 0.327329 0.241714 0.968190 0.097 Uiso 0.62(3) 1 calc R U P A 1
C23A C 0.1739(13) 0.3181(18) 0.9730(5) 0.093(8) Uani 0.62(3) 1 d D U P A 1
H23A H 0.157288 0.266295 0.982571 0.111 Uiso 0.62(3) 1 calc R U P A 1
H23B H 0.162358 0.358260 0.992678 0.111 Uiso 0.62(3) 1 calc R U P A 1
C24A C 0.1127(16) 0.360(3) 0.9422(6) 0.057(6) Uani 0.62(3) 1 d D U P A 1
H24A H 0.058018 0.334935 0.940450 0.069 Uiso 0.62(3) 1 calc R U P A 1
H24B H 0.081228 0.422380 0.945738 0.069 Uiso 0.62(3) 1 calc R U P A 1
O21B O 0.179(2) 0.329(2) 0.9122(6) 0.032(4) Uani 0.38(3) 1 d D U P A 2
C21B C 0.2726(17) 0.273(2) 0.9244(5) 0.033(5) Uani 0.38(3) 1 d D U P A 2
H21C H 0.326325 0.300587 0.919823 0.039 Uiso 0.38(3) 1 calc R U P A 2
H21D H 0.294665 0.218534 0.911770 0.039 Uiso 0.38(3) 1 calc R U P A 2
C22B C 0.2519(18) 0.2581(10) 0.9638(4) 0.045(6) Uani 0.38(3) 1 d D U P A 2
H22C H 0.314575 0.243762 0.976554 0.054 Uiso 0.38(3) 1 calc R U P A 2
H22D H 0.222001 0.211204 0.968590 0.054 Uiso 0.38(3) 1 calc R U P A 2
C23B C 0.176(2) 0.3447(14) 0.9750(7) 0.050(6) Uani 0.38(3) 1 d D U P A 2
H23C H 0.134291 0.338840 0.997552 0.060 Uiso 0.38(3) 1 calc R U P A 2
H23D H 0.209941 0.387515 0.977967 0.060 Uiso 0.38(3) 1 calc R U P A 2
C24B C 0.114(2) 0.367(4) 0.9431(9) 0.046(8) Uani 0.38(3) 1 d D U P A 2
H24C H 0.056147 0.344281 0.947101 0.056 Uiso 0.38(3) 1 calc R U P A 2
H24D H 0.086539 0.430176 0.939218 0.056 Uiso 0.38(3) 1 calc R U P A 2
C125 C -0.0240(6) 0.3857(5) 0.85977(19) 0.0573(17) Uani 1 1 d . . . . .
H12I H -0.082845 0.375663 0.874129 0.069 Uiso 1 1 calc R U . . .
H12J H 0.037146 0.335102 0.862991 0.069 Uiso 1 1 calc R U . . .
C126 C -0.0437(6) 0.4035(6) 0.8206(2) 0.068(2) Uani 1 1 d . . . . .
H12K H -0.079888 0.366223 0.812607 0.082 Uiso 1 1 calc R U . . .
H12L H 0.020315 0.395016 0.805164 0.082 Uiso 1 1 calc R U . . .
C127 C -0.1101(6) 0.4975(6) 0.81991(18) 0.065(2) Uani 1 1 d . . . . .
H12M H -0.183120 0.502959 0.822685 0.078 Uiso 1 1 calc R U . . .
H12N H -0.095999 0.527733 0.797121 0.078 Uiso 1 1 calc R U . . .
C128 C -0.0797(5) 0.5333(5) 0.85228(17) 0.0521(16) Uani 1 1 d . . . . .
H12O H -0.048310 0.577854 0.844070 0.062 Uiso 1 1 calc R U . . .
H12P H -0.140205 0.559298 0.868922 0.062 Uiso 1 1 calc R U . . .
C131 C 0.5539(6) 0.4862(6) 0.9462(2) 0.067(2) Uani 1 1 d . . . . .
H13A H 0.547921 0.429026 0.942851 0.080 Uiso 1 1 calc R U . . .
H13B H 0.491526 0.521314 0.959895 0.080 Uiso 1 1 calc R U . . .
C132 C 0.6456(6) 0.4775(6) 0.9655(2) 0.072(2) Uani 1 1 d . . . . .
H13C H 0.634599 0.528009 0.980144 0.086 Uiso 1 1 calc R U . . .
H13D H 0.663009 0.424889 0.981373 0.086 Uiso 1 1 calc R U . . .
C133 C 0.7265(7) 0.4722(7) 0.9360(2) 0.084(3) Uani 1 1 d . . . . .
H13E H 0.762824 0.411686 0.929993 0.101 Uiso 1 1 calc R U . . .
H13F H 0.776184 0.498292 0.942940 0.101 Uiso 1 1 calc R U . . .
C134 C 0.6712(5) 0.5218(5) 0.90474(19) 0.0561(17) Uani 1 1 d . . . . .
H13G H 0.677974 0.579956 0.902142 0.067 Uiso 1 1 calc R U . . .
H13H H 0.699453 0.491772 0.882074 0.067 Uiso 1 1 calc R U . . .
C141 C 0.0322(6) 0.7595(5) 0.72381(18) 0.0611(18) Uani 1 1 d D . . . .
H14A H -0.041025 0.772219 0.721057 0.073 Uiso 1 1 calc R U . . .
H14B H 0.063715 0.696662 0.727732 0.073 Uiso 1 1 calc R U . . .
C142 C 0.0831(7) 0.7914(5) 0.69084(19) 0.068(2) Uani 1 1 d D . . . .
H14C H 0.040541 0.802436 0.670166 0.081 Uiso 1 1 calc R U . . .
H14D H 0.150235 0.749190 0.684003 0.081 Uiso 1 1 calc R U . . .
C143 C 0.0942(6) 0.8745(5) 0.7024(2) 0.070(2) Uani 1 1 d D . . . .
H14E H 0.166521 0.868157 0.704215 0.083 Uiso 1 1 calc R U . . .
H14F H 0.065116 0.922725 0.685110 0.083 Uiso 1 1 calc R U . . .
C144 C 0.0360(6) 0.8886(4) 0.7385(2) 0.0634(19) Uani 1 1 d D . . . .
H14G H 0.064916 0.919554 0.753978 0.076 Uiso 1 1 calc R U . . .
H14H H -0.036300 0.922136 0.736015 0.076 Uiso 1 1 calc R U . . .
Dy7 Dy 0.83285(2) 0.30625(2) 0.51963(2) 0.03595(7) Uani 1 1 d . . . . .
Dy8 Dy 0.82036(2) 0.10684(2) 0.58687(2) 0.03271(6) Uani 1 1 d . . . . .
Dy9 Dy 1.05745(2) 0.19130(2) 0.58769(2) 0.03488(7) Uani 1 1 d . . . . .
K5 K 0.86262(11) -0.19990(9) 0.52749(3) 0.0429(3) Uani 1 1 d . . . . .
K6 K 0.88093(12) 0.06138(9) 0.46745(4) 0.0511(3) Uani 1 1 d . . . . .
Cl21 Cl 0.84270(11) 0.26686(8) 0.59593(3) 0.0370(3) Uani 1 1 d . . . . .
Cl22 Cl 0.71676(11) 0.20059(10) 0.53144(4) 0.0415(3) Uani 1 1 d . . . . .
Cl23 Cl 1.00409(11) 0.05252(9) 0.61492(4) 0.0395(3) Uani 1 1 d . . . . .
Cl24 Cl 1.01469(11) 0.32264(9) 0.53572(3) 0.0405(3) Uani 1 1 d . . . . .
Cl25 Cl 1.21162(12) 0.09758(10) 0.54699(4) 0.0466(3) Uani 1 1 d . . . . .
Cl26 Cl 0.90696(12) 0.25605(10) 0.45507(4) 0.0448(3) Uani 1 1 d . . . . .
Cl27 Cl 0.87405(13) -0.02920(10) 0.54789(4) 0.0474(3) Uani 1 1 d . . . . .
Cl28 Cl 0.96595(10) 0.13762(8) 0.53264(3) 0.0353(3) Uani 1 1 d . . . . .
O51 O 0.6633(4) -0.1874(4) 0.53186(15) 0.0764(16) Uani 1 1 d . . . . .
O52 O 0.8311(4) -0.2838(4) 0.58984(13) 0.0697(15) Uani 1 1 d . . . . .
C71 C 0.7866(5) 0.4705(4) 0.5032(2) 0.0554(17) Uani 1 1 d . . . . .
C72 C 0.7306(6) 0.4418(4) 0.48051(17) 0.0543(17) Uani 1 1 d . . . . .
C73 C 0.6571(6) 0.4162(4) 0.5029(2) 0.0562(17) Uani 1 1 d . . . . .
C74 C 0.6671(5) 0.4307(4) 0.53822(18) 0.0525(16) Uani 1 1 d . . . . .
C75 C 0.7456(6) 0.4649(4) 0.53907(18) 0.0527(16) Uani 1 1 d . . . . .
C76 C 0.8673(7) 0.5105(6) 0.4909(3) 0.091(3) Uani 1 1 d . . . . .
H76A H 0.835258 0.571630 0.484732 0.137 Uiso 1 1 calc R U . . .
H76B H 0.907338 0.481547 0.469654 0.137 Uiso 1 1 calc R U . . .
H76C H 0.911905 0.504363 0.510332 0.137 Uiso 1 1 calc R U . . .
C77 C 0.7396(8) 0.4484(6) 0.44015(19) 0.090(3) Uani 1 1 d . . . . .
H77A H 0.696929 0.505453 0.431918 0.135 Uiso 1 1 calc R U . . .
H77B H 0.717106 0.404290 0.430675 0.135 Uiso 1 1 calc R U . . .
H77C H 0.810504 0.439886 0.431429 0.135 Uiso 1 1 calc R U . . .
C78 C 0.5749(8) 0.3873(6) 0.4901(3) 0.099(3) Uani 1 1 d . . . . .
H78A H 0.514717 0.437411 0.486277 0.148 Uiso 1 1 calc R U . . .
H78B H 0.557037 0.347593 0.508241 0.148 Uiso 1 1 calc R U . . .
H78C H 0.599382 0.358105 0.467303 0.148 Uiso 1 1 calc R U . . .
C79 C 0.5973(7) 0.4203(6) 0.5708(2) 0.086(3) Uani 1 1 d . . . . .
H79A H 0.542148 0.474659 0.574508 0.129 Uiso 1 1 calc R U . . .
H79B H 0.635956 0.404389 0.592170 0.129 Uiso 1 1 calc R U . . .
H79C H 0.568732 0.375149 0.566622 0.129 Uiso 1 1 calc R U . . .
C80 C 0.7761(8) 0.4965(5) 0.5718(2) 0.089(3) Uani 1 1 d . . . . .
H80A H 0.737382 0.557532 0.574502 0.134 Uiso 1 1 calc R U . . .
H80B H 0.848857 0.489126 0.568828 0.134 Uiso 1 1 calc R U . . .
H80C H 0.761758 0.463440 0.593360 0.134 Uiso 1 1 calc R U . . .
C81 C 0.7630(4) 0.0802(4) 0.65523(14) 0.0386(12) Uani 1 1 d . . . . .
C82 C 0.6909(4) 0.1569(4) 0.64368(14) 0.0382(12) Uani 1 1 d . . . . .
C83 C 0.6344(4) 0.1379(4) 0.61750(15) 0.0389(12) Uani 1 1 d . . . . .
C84 C 0.6732(5) 0.0487(4) 0.61281(16) 0.0434(13) Uani 1 1 d . . . . .
C85 C 0.7519(5) 0.0130(4) 0.63607(15) 0.0452(14) Uani 1 1 d . . . . .
C86 C 0.8280(5) 0.0690(5) 0.68619(16) 0.0526(16) Uani 1 1 d . . . . .
H86A H 0.791970 0.055063 0.708435 0.079 Uiso 1 1 calc R U . . .
H86B H 0.842652 0.122355 0.688890 0.079 Uiso 1 1 calc R U . . .
H86C H 0.891887 0.022126 0.681443 0.079 Uiso 1 1 calc R U . . .
C87 C 0.6686(5) 0.2438(4) 0.65952(15) 0.0429(13) Uani 1 1 d . . . . .
H87A H 0.623476 0.247580 0.681639 0.064 Uiso 1 1 calc R U . . .
H87B H 0.635599 0.289163 0.642039 0.064 Uiso 1 1 calc R U . . .
H87C H 0.732287 0.251002 0.665157 0.064 Uiso 1 1 calc R U . . .
C88 C 0.5424(5) 0.2001(5) 0.60150(16) 0.0505(15) Uani 1 1 d . . . . .
H88A H 0.481422 0.201549 0.617232 0.076 Uiso 1 1 calc R U . . .
H88B H 0.536537 0.181677 0.577612 0.076 Uiso 1 1 calc R U . . .
H88C H 0.549176 0.257597 0.599216 0.076 Uiso 1 1 calc R U . . .
C89 C 0.6304(6) 0.0003(5) 0.58943(18) 0.0578(18) Uani 1 1 d . . . . .
H89A H 0.567581 -0.005894 0.601562 0.087 Uiso 1 1 calc R U . . .
H89B H 0.679970 -0.056756 0.585249 0.087 Uiso 1 1 calc R U . . .
H89C H 0.615912 0.031999 0.566280 0.087 Uiso 1 1 calc R U . . .
C90 C 0.8118(7) -0.0805(5) 0.6411(2) 0.066(2) Uani 1 1 d . . . . .
H90A H 0.789106 -0.102905 0.664275 0.098 Uiso 1 1 calc R U . . .
H90B H 0.884164 -0.087179 0.640830 0.098 Uiso 1 1 calc R U . . .
H90C H 0.801234 -0.112471 0.621503 0.098 Uiso 1 1 calc R U . . .
C91 C 1.2042(5) 0.1821(4) 0.62845(15) 0.0463(14) Uani 1 1 d . . . . .
C92 C 1.1743(5) 0.2661(5) 0.61312(17) 0.0524(17) Uani 1 1 d . . . . .
C93 C 1.0744(6) 0.3093(4) 0.62764(17) 0.0495(16) Uani 1 1 d . . . . .
C94 C 1.0432(5) 0.2522(4) 0.65254(15) 0.0448(14) Uani 1 1 d . . . . .
C95 C 1.1238(5) 0.1730(4) 0.65302(15) 0.0405(13) Uani 1 1 d . . . . .
C96 C 1.2417(7) 0.3042(6) 0.5883(2) 0.071(2) Uani 1 1 d . . . . .
H96A H 1.281220 0.327219 0.602738 0.106 Uiso 1 1 calc R U . . .
H96B H 1.199777 0.350686 0.573153 0.106 Uiso 1 1 calc R U . . .
H96C H 1.288043 0.259610 0.573037 0.106 Uiso 1 1 calc R U . . .
C97 C 1.0189(7) 0.4035(5) 0.6210(2) 0.074(2) Uani 1 1 d . . . . .
H97A H 0.946205 0.415284 0.627581 0.110 Uiso 1 1 calc R U . . .
H97B H 1.029431 0.419073 0.595364 0.110 Uiso 1 1 calc R U . . .
H97C H 1.045101 0.437427 0.635589 0.110 Uiso 1 1 calc R U . . .
C98 C 0.9471(6) 0.2730(5) 0.67683(17) 0.0616(19) Uani 1 1 d . . . . .
H98A H 0.958252 0.293282 0.699650 0.092 Uiso 1 1 calc R U . . .
H98B H 0.927160 0.221255 0.681580 0.092 Uiso 1 1 calc R U . . .
H98C H 0.893147 0.317922 0.665163 0.092 Uiso 1 1 calc R U . . .
C99 C 1.1278(5) 0.0978(4) 0.67830(15) 0.0485(15) Uani 1 1 d . . . . .
H99A H 1.159555 0.102645 0.699980 0.073 Uiso 1 1 calc R U . . .
H99B H 1.167786 0.044598 0.666438 0.073 Uiso 1 1 calc R U . . .
H99C H 1.058698 0.096617 0.685067 0.073 Uiso 1 1 calc R U . . .
C100 C 1.3088(5) 0.1155(5) 0.62330(17) 0.0555(17) Uani 1 1 d . . . . .
H10A H 1.355707 0.129725 0.637654 0.083 Uiso 1 1 calc R U . . .
H10B H 1.333328 0.115151 0.597745 0.083 Uiso 1 1 calc R U . . .
H10C H 1.304789 0.058581 0.631160 0.083 Uiso 1 1 calc R U . . .
C151 C 0.6507(13) -0.2606(8) 0.5199(4) 0.146(6) Uani 1 1 d . . . . .
H15A H 0.634348 -0.295451 0.540884 0.175 Uiso 1 1 calc R U . . .
H15B H 0.714807 -0.295601 0.507120 0.175 Uiso 1 1 calc R U . . .
C152 C 0.5704(12) -0.2383(9) 0.4961(3) 0.137(5) Uani 1 1 d . . . . .
H15C H 0.510587 -0.252173 0.507725 0.164 Uiso 1 1 calc R U . . .
H15D H 0.593357 -0.269607 0.473487 0.164 Uiso 1 1 calc R U . . .
C153 C 0.5450(7) -0.1429(7) 0.4886(2) 0.086(3) Uani 1 1 d . . . . .
H15E H 0.577191 -0.130216 0.464956 0.103 Uiso 1 1 calc R U . . .
H15F H 0.470685 -0.114179 0.488987 0.103 Uiso 1 1 calc R U . . .
C154 C 0.5878(6) -0.1154(6) 0.5186(2) 0.072(2) Uani 1 1 d . . . . .
H15G H 0.617237 -0.069860 0.509805 0.087 Uiso 1 1 calc R U . . .
H15H H 0.533741 -0.092118 0.537923 0.087 Uiso 1 1 calc R U . . .
C155 C 0.9146(7) -0.3374(7) 0.6091(3) 0.102(4) Uani 1 1 d . . . . .
H15I H 0.970723 -0.312711 0.606723 0.123 Uiso 1 1 calc R U . . .
H15J H 0.940267 -0.395700 0.599351 0.123 Uiso 1 1 calc R U . . .
C156 C 0.8763(8) -0.3414(9) 0.6468(3) 0.124(5) Uani 1 1 d . . . . .
H15K H 0.902946 -0.400714 0.657188 0.149 Uiso 1 1 calc R U . . .
H15L H 0.897433 -0.302683 0.661080 0.149 Uiso 1 1 calc R U . . .
C157 C 0.7713(7) -0.3156(9) 0.6473(3) 0.119(5) Uani 1 1 d . . . . .
H15M H 0.740456 -0.273293 0.666164 0.143 Uiso 1 1 calc R U . . .
H15N H 0.747531 -0.365774 0.652942 0.143 Uiso 1 1 calc R U . . .
C158 C 0.7400(5) -0.2770(5) 0.61213(19) 0.0551(16) Uani 1 1 d . . . . .
H15O H 0.699977 -0.307885 0.601721 0.066 Uiso 1 1 calc R U . . .
H15P H 0.697749 -0.215938 0.614374 0.066 Uiso 1 1 calc R U . . .
O61A O 0.7410(8) 0.1499(10) 0.4288(3) 0.092(5) Uani 0.646(16) 1 d D U P B 3
C61A C 0.7596(13) 0.1765(12) 0.3932(3) 0.077(5) Uani 0.646(16) 1 d D U P B 3
H61A H 0.833281 0.156604 0.385769 0.092 Uiso 0.646(16) 1 calc R U P B 3
H61B H 0.733112 0.239883 0.390124 0.092 Uiso 0.646(16) 1 calc R U P B 3
C62A C 0.7041(19) 0.1352(19) 0.3720(5) 0.091(6) Uani 0.646(16) 1 d D U P B 3
H62A H 0.746132 0.075619 0.366392 0.109 Uiso 0.646(16) 1 calc R U P B 3
H62B H 0.684584 0.168446 0.349172 0.109 Uiso 0.646(16) 1 calc R U P B 3
C63A C 0.6105(12) 0.1365(13) 0.3970(4) 0.095(5) Uani 0.646(16) 1 d D U P B 3
H63A H 0.550232 0.184648 0.390245 0.114 Uiso 0.646(16) 1 calc R U P B 3
H63B H 0.595802 0.081782 0.396600 0.114 Uiso 0.646(16) 1 calc R U P B 3
C64A C 0.6395(11) 0.1481(16) 0.4326(4) 0.096(6) Uani 0.646(16) 1 d D U P B 3
H64A H 0.593188 0.202543 0.442488 0.115 Uiso 0.646(16) 1 calc R U P B 3
H64B H 0.634602 0.100150 0.449455 0.115 Uiso 0.646(16) 1 calc R U P B 3
O61B O 0.6864(18) 0.1499(11) 0.4351(4) 0.076(7) Uani 0.354(16) 1 d D U P B 4
C61B C 0.6870(16) 0.2309(11) 0.4194(5) 0.073(6) Uani 0.354(16) 1 d D U P B 4
H61C H 0.720941 0.258828 0.434336 0.087 Uiso 0.354(16) 1 calc R U P B 4
H61D H 0.617039 0.269750 0.416276 0.087 Uiso 0.354(16) 1 calc R U P B 4
C62B C 0.745(2) 0.2087(19) 0.3839(7) 0.096(8) Uani 0.354(16) 1 d D U P B 4
H62C H 0.818510 0.198552 0.385639 0.116 Uiso 0.354(16) 1 calc R U P B 4
H62D H 0.720023 0.255171 0.365413 0.116 Uiso 0.354(16) 1 calc R U P B 4
C63B C 0.727(4) 0.127(3) 0.3748(8) 0.104(12) Uani 0.354(16) 1 d D U P B 4
H63C H 0.691791 0.135296 0.352251 0.125 Uiso 0.354(16) 1 calc R U P B 4
H63D H 0.791246 0.078633 0.371959 0.125 Uiso 0.354(16) 1 calc R U P B 4
C64B C 0.661(3) 0.1099(16) 0.4064(7) 0.090(8) Uani 0.354(16) 1 d D U P B 4
H64C H 0.587735 0.135988 0.402165 0.107 Uiso 0.354(16) 1 calc R U P B 4
H64D H 0.675555 0.047404 0.411632 0.107 Uiso 0.354(16) 1 calc R U P B 4


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 C13 2.618(5) . ?
Dy1 C12 2.632(6) . ?
Dy1 C14 2.635(5) . ?
Dy1 C11 2.641(6) . ?
Dy1 Cl5 2.6421(13) . ?
Dy1 C15 2.645(5) . ?
Dy1 Cl4 2.7200(13) . ?
Dy1 Cl2 2.7241(13) . ?
Dy1 Cl1 2.8118(13) . ?
Dy1 Cl9 2.8382(12) . ?
Dy1 K3 4.5006(13) . ?
Dy2 Cl6 2.6068(13) . ?
Dy2 C22 2.607(5) . ?
Dy2 C23 2.617(5) . ?
Dy2 C21 2.617(6) . ?
Dy2 C24 2.646(5) . ?
Dy2 C25 2.659(6) . ?
Dy2 Cl2 2.7388(13) . ?
Dy2 Cl3 2.7724(14) . ?
Dy2 Cl9 2.8113(13) . ?
Dy2 Cl1 2.8953(12) . ?
Dy2 K1 4.3906(13) . ?
Dy3 Cl8 2.6024(14) . ?
Dy3 C32 2.616(5) . ?
Dy3 C31 2.617(5) . ?
Dy3 C33 2.636(5) . ?
Dy3 C34 2.644(5) . ?
Dy3 C35 2.650(6) . ?
Dy3 Cl4 2.7349(13) . ?
Dy3 Cl3 2.7637(13) . ?
Dy3 Cl9 2.8489(12) . ?
Dy3 Cl1 2.8768(14) . ?
Dy3 K1 4.2449(12) . ?
Dy3 K3 4.3776(12) . ?
Dy4 C41 2.601(6) . ?
Dy4 Cl7 2.6077(13) . ?
Dy4 C45 2.617(5) . ?
Dy4 C42 2.618(5) . ?
Dy4 C44 2.643(5) . ?
Dy4 C43 2.653(5) . ?
Dy4 Cl12 2.7072(13) . ?
Dy4 Cl17 2.7314(13) . ?
Dy4 Cl10 2.8063(13) . ?
Dy4 Cl14 2.8575(12) . ?
Dy4 Dy6 3.9951(3) . ?
Dy4 K3 4.5006(12) . ?
Dy5 Cl15 2.6061(13) . ?
Dy5 C55 2.611(6) . ?
Dy5 C54 2.620(5) . ?
Dy5 C51 2.621(6) . ?
Dy5 C53 2.639(6) . ?
Dy5 C52 2.665(6) . ?
Dy5 Cl17 2.7363(13) . ?
Dy5 Cl11 2.7584(13) . ?
Dy5 Cl14 2.8403(13) . ?
Dy5 Cl10 2.8873(12) . ?
Dy5 K2 4.2920(13) . ?
Dy5 K3 4.3649(12) . ?
Dy6 Cl16 2.6168(13) . ?
Dy6 C65 2.626(5) . ?
Dy6 C64 2.629(5) . ?
Dy6 C62 2.633(5) . ?
Dy6 C61 2.634(5) . ?
Dy6 C63 2.637(5) . ?
Dy6 Cl12 2.7323(13) . ?
Dy6 Cl11 2.7539(13) . ?
Dy6 Cl14 2.8401(12) . ?
Dy6 Cl10 2.8630(13) . ?
Dy6 K2 4.3036(12) . ?
K1 O12 2.719(5) . ?
K1 O11 2.732(5) . ?
K1 Cl8 3.0780(18) . ?
K1 Cl7 3.0794(18) . ?
K1 Cl3 3.1662(18) . ?
K1 Cl6 3.3197(19) . ?
K1 C118 3.425(7) . ?
K1 Cl9 3.6102(17) . ?
K1 K3 4.8307(17) . ?
K2 O21A 2.59(2) . ?
K2 O22 2.755(5) . ?
K2 O21B 2.84(3) . ?
K2 Cl5 3.0644(18) . ?
K2 Cl15 3.2035(18) . ?
K2 Cl16 3.2162(18) . ?
K2 Cl11 3.2732(18) . ?
K2 Cl14 3.3682(17) . ?
K2 C21A 3.50(3) . ?
K2 C125 3.534(7) . ?
K3 O31 2.641(5) . ?
K3 Cl8 3.1821(19) . ?
K3 Cl15 3.2047(18) . ?
K3 Cl9 3.2400(18) . ?
K3 Cl14 3.2933(17) . ?
K3 Cl7 3.2960(18) . ?
K3 Cl5 3.3260(19) . ?
K3 Cl17 3.4798(18) . ?
K3 Cl4 3.5310(18) . ?
K3 K4 4.2593(17) . ?
K4 O41 2.699(4) . ?
K4 Cl7 3.1802(19) . ?
K4 Cl5 3.2204(18) . ?
K4 Cl9 3.3542(17) . ?
K4 Cl14 3.4035(19) . ?
K4 Cl6 3.4683(19) . ?
K4 Cl16 3.5093(19) . ?
K4 Cl2 3.5867(19) . ?
O11 C111 1.439(9) . ?
O11 C114 1.442(9) . ?
O12 C115 1.424(8) . ?
O12 C118 1.431(9) . ?
O22 C128 1.427(8) . ?
O22 C125 1.436(8) . ?
O31 C134 1.410(9) . ?
O31 C131 1.424(8) . ?
O41 C141 1.423(7) . ?
O41 C144 1.430(7) . ?
C11 C15 1.409(8) . ?
C11 C12 1.413(8) . ?
C11 C16 1.512(8) . ?
C12 C13 1.413(8) . ?
C12 C17 1.505(8) . ?
C13 C14 1.427(7) . ?
C13 C18 1.500(8) . ?
C14 C15 1.419(8) . ?
C14 C19 1.496(8) . ?
C15 C20 1.493(8) . ?
C21 C25 1.413(8) . ?
C21 C22 1.422(7) . ?
C21 C26 1.506(8) . ?
C22 C23 1.414(8) . ?
C22 C27 1.500(8) . ?
C23 C24 1.413(8) . ?
C23 C28 1.510(8) . ?
C24 C25 1.412(8) . ?
C24 C29 1.517(8) . ?
C25 C30 1.504(7) . ?
C31 C32 1.414(9) . ?
C31 C35 1.416(9) . ?
C31 C36 1.502(9) . ?
C32 C33 1.414(8) . ?
C32 C37 1.506(9) . ?
C33 C34 1.412(8) . ?
C33 C38 1.502(8) . ?
C34 C35 1.419(8) . ?
C34 C39 1.498(8) . ?
C35 C40 1.495(9) . ?
C41 C45 1.397(9) . ?
C41 C42 1.404(8) . ?
C41 C46 1.516(8) . ?
C42 C43 1.422(8) . ?
C42 C47 1.500(9) . ?
C43 C44 1.415(8) . ?
C43 C48 1.502(8) . ?
C44 C45 1.415(8) . ?
C44 C49 1.508(8) . ?
C45 C50 1.509(9) . ?
C51 C55 1.409(8) . ?
C51 C52 1.414(8) . ?
C51 C56 1.507(9) . ?
C52 C53 1.421(8) . ?
C52 C57 1.491(8) . ?
C53 C54 1.419(8) . ?
C53 C58 1.506(8) . ?
C54 C55 1.422(8) . ?
C54 C59 1.496(8) . ?
C55 C60 1.498(8) . ?
C61 C65 1.411(8) . ?
C61 C62 1.415(8) . ?
C61 C66 1.506(8) . ?
C62 C63 1.413(8) . ?
C62 C67 1.504(8) . ?
C63 C64 1.427(8) . ?
C63 C68 1.500(8) . ?
C64 C65 1.414(8) . ?
C64 C69 1.493(7) . ?
C65 C70 1.499(8) . ?
C111 C112 1.522(10) . ?
C112 C113 1.524(12) . ?
C113 C114 1.490(11) . ?
C115 C116 1.511(11) . ?
C116 C117 1.514(13) . ?
C117 C118 1.474(11) . ?
O21A C21A 1.433(12) . ?
O21A C24A 1.441(13) . ?
C21A C22A 1.494(15) . ?
C22A C23A 1.524(15) . ?
C23A C24A 1.491(13) . ?
O21B C21B 1.426(13) . ?
O21B C24B 1.436(14) . ?
C21B C22B 1.490(16) . ?
C22B C23B 1.532(15) . ?
C23B C24B 1.494(16) . ?
C125 C126 1.503(10) . ?
C126 C127 1.523(12) . ?
C127 C128 1.533(9) . ?
C131 C132 1.493(10) . ?
C132 C133 1.482(11) . ?
C133 C134 1.501(9) . ?
C141 C142 1.508(9) . ?
C142 C143 1.523(9) . ?
C143 C144 1.494(9) . ?
Dy7 Cl26 2.6037(14) . ?
Dy7 C71 2.611(6) . ?
Dy7 C74 2.612(7) . ?
Dy7 C75 2.618(6) . ?
Dy7 C73 2.633(7) . ?
Dy7 C72 2.649(6) . ?
Dy7 Cl22 2.7316(14) . ?
Dy7 Cl24 2.7692(14) . ?
Dy7 Cl28 2.8314(14) . ?
Dy7 Cl21 2.8792(13) . ?
Dy7 K5 4.2837(14) 2_756 ?
Dy7 K6 4.4269(14) . ?
Dy8 Cl27 2.6162(14) . ?
Dy8 C84 2.617(6) . ?
Dy8 C85 2.625(6) . ?
Dy8 C83 2.636(6) . ?
Dy8 C82 2.637(5) . ?
Dy8 C81 2.646(5) . ?
Dy8 Cl23 2.7170(14) . ?
Dy8 Cl22 2.7249(14) . ?
Dy8 Cl21 2.8023(13) . ?
Dy8 Cl28 2.8645(13) . ?
Dy8 Dy9 3.9966(4) . ?
Dy8 K6 4.5178(13) . ?
Dy9 Cl25 2.6147(15) . ?
Dy9 C93 2.616(6) . ?
Dy9 C92 2.623(6) . ?
Dy9 C91 2.630(6) . ?
Dy9 C94 2.648(5) . ?
Dy9 C95 2.654(5) . ?
Dy9 Cl23 2.7308(14) . ?
Dy9 Cl24 2.7533(14) . ?
Dy9 Cl21 2.8424(15) . ?
Dy9 Cl28 2.8545(13) . ?
Dy9 K5 4.3335(12) 2_756 ?
K5 O52 2.693(5) . ?
K5 O51 2.714(6) . ?
K5 Cl27 3.0231(19) . ?
K5 Cl26 3.167(2) 2_756 ?
K5 Cl24 3.1924(19) 2_756 ?
K5 Cl25 3.223(2) 2_756 ?
K5 C151 3.464(15) . ?
K5 Cl28 3.4708(18) 2_756 ?
K5 K6 4.7809(19) . ?
K5 K6 4.864(2) 2_756 ?
K6 O61A 2.533(11) . ?
K6 O61B 2.96(2) . ?
K6 Cl27 3.261(2) . ?
K6 Cl28 3.276(2) 2_756 ?
K6 Cl27 3.287(2) 2_756 ?
K6 Cl28 3.2984(18) . ?
K6 Cl26 3.341(2) . ?
K6 Cl25 3.374(2) 2_756 ?
K6 C61A 3.493(15) . ?
K6 Cl22 3.531(2) . ?
K6 Cl23 3.6610(19) 2_756 ?
K6 K6 4.189(3) 2_756 ?
O51 C151 1.384(12) . ?
O51 C154 1.402(10) . ?
O52 C158 1.427(8) . ?
O52 C155 1.434(10) . ?
C71 C75 1.409(10) . ?
C71 C72 1.409(10) . ?
C71 C76 1.503(10) . ?
C72 C73 1.412(10) . ?
C72 C77 1.497(9) . ?
C73 C74 1.384(10) . ?
C73 C78 1.510(11) . ?
C74 C75 1.393(10) . ?
C74 C79 1.516(10) . ?
C75 C80 1.510(10) . ?
C81 C82 1.404(8) . ?
C81 C85 1.417(8) . ?
C81 C86 1.503(8) . ?
C82 C83 1.425(8) . ?
C82 C87 1.513(8) . ?
C83 C84 1.406(8) . ?
C83 C88 1.504(8) . ?
C84 C85 1.415(9) . ?
C84 C89 1.506(8) . ?
C85 C90 1.502(9) . ?
C91 C92 1.406(9) . ?
C91 C95 1.418(8) . ?
C91 C100 1.516(9) . ?
C92 C93 1.415(10) . ?
C92 C96 1.507(9) . ?
C93 C94 1.415(9) . ?
C93 C97 1.505(10) . ?
C94 C95 1.418(9) . ?
C94 C98 1.498(9) . ?
C95 C99 1.493(8) . ?
C151 C152 1.436(16) . ?
C152 C153 1.506(16) . ?
C153 C154 1.480(11) . ?
C155 C156 1.460(13) . ?
C156 C157 1.387(13) . ?
C157 C158 1.458(10) . ?
O61A C61A 1.394(12) . ?
O61A C64A 1.421(13) . ?
C61A C62A 1.495(15) . ?
C62A C63A 1.526(15) . ?
C63A C64A 1.466(14) . ?
O61B C61B 1.423(15) . ?
O61B C64B 1.429(15) . ?
C61B C62B 1.486(17) . ?
C62B C63B 1.524(17) . ?
C63B C64B 1.492(17) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C13 Dy1 C12 31.22(18) . . ?
C13 Dy1 C14 31.51(16) . . ?
C12 Dy1 C14 51.79(17) . . ?
C13 Dy1 C11 51.44(18) . . ?
C12 Dy1 C11 31.08(17) . . ?
C14 Dy1 C11 51.44(17) . . ?
C13 Dy1 Cl5 86.18(12) . . ?
C12 Dy1 Cl5 82.05(12) . . ?
C14 Dy1 Cl5 116.54(12) . . ?
C11 Dy1 Cl5 108.98(13) . . ?
C13 Dy1 C15 51.64(17) . . ?
C12 Dy1 C15 51.47(16) . . ?
C14 Dy1 C15 31.18(17) . . ?
C11 Dy1 C15 30.92(16) . . ?
Cl5 Dy1 C15 133.10(12) . . ?
C13 Dy1 Cl4 88.80(13) . . ?
C12 Dy1 Cl4 119.64(13) . . ?
C14 Dy1 Cl4 80.92(13) . . ?
C11 Dy1 Cl4 132.36(13) . . ?
Cl5 Dy1 Cl4 90.42(4) . . ?
C15 Dy1 Cl4 106.04(12) . . ?
C13 Dy1 Cl2 127.16(13) . . ?
C12 Dy1 Cl2 96.06(13) . . ?
C14 Dy1 Cl2 130.25(13) . . ?
C11 Dy1 Cl2 81.04(13) . . ?
Cl5 Dy1 Cl2 89.68(4) . . ?
C15 Dy1 Cl2 99.96(12) . . ?
Cl4 Dy1 Cl2 143.95(4) . . ?
C13 Dy1 Cl1 124.88(12) . . ?
C12 Dy1 Cl1 130.28(12) . . ?
C14 Dy1 Cl1 93.39(12) . . ?
C11 Dy1 Cl1 100.76(13) . . ?
Cl5 Dy1 Cl1 146.78(4) . . ?
C15 Dy1 Cl1 80.04(12) . . ?
Cl4 Dy1 Cl1 79.91(4) . . ?
Cl2 Dy1 Cl1 80.50(4) . . ?
C13 Dy1 Cl9 154.49(13) . . ?
C12 Dy1 Cl9 155.71(12) . . ?
C14 Dy1 Cl9 150.73(12) . . ?
C11 Dy1 Cl9 152.75(13) . . ?
Cl5 Dy1 Cl9 76.78(4) . . ?
C15 Dy1 Cl9 149.84(12) . . ?
Cl4 Dy1 Cl9 72.70(4) . . ?
Cl2 Dy1 Cl9 72.26(4) . . ?
Cl1 Dy1 Cl9 70.01(4) . . ?
C13 Dy1 K3 108.86(13) . . ?
C12 Dy1 K3 122.91(13) . . ?
C14 Dy1 K3 123.00(12) . . ?
C11 Dy1 K3 153.77(12) . . ?
Cl5 Dy1 K3 47.15(4) . . ?
C15 Dy1 K3 153.97(12) . . ?
Cl4 Dy1 K3 51.67(3) . . ?
Cl2 Dy1 K3 106.04(3) . . ?
Cl1 Dy1 K3 105.29(3) . . ?
Cl9 Dy1 K3 45.79(3) . . ?
Cl6 Dy2 C22 126.53(12) . . ?
Cl6 Dy2 C23 128.31(12) . . ?
C22 Dy2 C23 31.41(18) . . ?
Cl6 Dy2 C21 95.21(12) . . ?
C22 Dy2 C21 31.58(16) . . ?
C23 Dy2 C21 51.94(17) . . ?
Cl6 Dy2 C24 97.92(12) . . ?
C22 Dy2 C24 51.60(17) . . ?
C23 Dy2 C24 31.15(17) . . ?
C21 Dy2 C24 51.47(17) . . ?
Cl6 Dy2 C25 79.49(13) . . ?
C22 Dy2 C25 51.58(17) . . ?
C23 Dy2 C25 51.43(17) . . ?
C21 Dy2 C25 31.05(17) . . ?
C24 Dy2 C25 30.87(17) . . ?
Cl6 Dy2 Cl2 96.50(4) . . ?
C22 Dy2 Cl2 115.51(13) . . ?
C23 Dy2 Cl2 85.04(13) . . ?
C21 Dy2 Cl2 131.65(13) . . ?
C24 Dy2 Cl2 80.46(12) . . ?
C25 Dy2 Cl2 106.96(13) . . ?
Cl6 Dy2 Cl3 91.51(4) . . ?
C22 Dy2 Cl3 87.19(13) . . ?
C23 Dy2 Cl3 117.40(13) . . ?
C21 Dy2 Cl3 83.11(13) . . ?
C24 Dy2 Cl3 134.13(12) . . ?
C25 Dy2 Cl3 110.04(13) . . ?
Cl2 Dy2 Cl3 142.98(4) . . ?
Cl6 Dy2 Cl9 76.80(4) . . ?
C22 Dy2 Cl9 151.21(12) . . ?
C23 Dy2 Cl9 148.75(12) . . ?
C21 Dy2 Cl9 155.74(13) . . ?
C24 Dy2 Cl9 151.47(12) . . ?
C25 Dy2 Cl9 156.01(12) . . ?
Cl2 Dy2 Cl9 72.46(4) . . ?
Cl3 Dy2 Cl9 74.37(4) . . ?
Cl6 Dy2 Cl1 145.54(4) . . ?
C22 Dy2 Cl1 84.83(12) . . ?
C23 Dy2 Cl1 85.63(12) . . ?
C21 Dy2 Cl1 113.57(12) . . ?
C24 Dy2 Cl1 114.57(12) . . ?
C25 Dy2 Cl1 134.75(12) . . ?
Cl2 Dy2 Cl1 78.78(4) . . ?
Cl3 Dy2 Cl1 74.45(4) . . ?
Cl9 Dy2 Cl1 69.20(4) . . ?
Cl6 Dy2 K1 48.88(4) . . ?
C22 Dy2 K1 124.21(13) . . ?
C23 Dy2 K1 153.99(12) . . ?
C21 Dy2 K1 102.44(13) . . ?
C24 Dy2 K1 139.46(12) . . ?
C25 Dy2 K1 110.18(13) . . ?
Cl2 Dy2 K1 120.26(3) . . ?
Cl3 Dy2 K1 45.91(3) . . ?
Cl9 Dy2 K1 55.03(3) . . ?
Cl1 Dy2 K1 104.06(3) . . ?
Cl8 Dy3 C32 121.69(14) . . ?
Cl8 Dy3 C31 90.34(15) . . ?
C32 Dy3 C31 31.35(19) . . ?
Cl8 Dy3 C33 129.37(13) . . ?
C32 Dy3 C33 31.24(18) . . ?
C31 Dy3 C33 51.79(19) . . ?
Cl8 Dy3 C34 100.74(14) . . ?
C32 Dy3 C34 51.35(18) . . ?
C31 Dy3 C34 51.49(18) . . ?
C33 Dy3 C34 31.02(18) . . ?
Cl8 Dy3 C35 78.39(13) . . ?
C32 Dy3 C35 51.55(19) . . ?
C31 Dy3 C35 31.18(19) . . ?
C33 Dy3 C35 51.57(18) . . ?
C34 Dy3 C35 31.10(18) . . ?
Cl8 Dy3 Cl4 94.21(4) . . ?
C32 Dy3 Cl4 121.79(13) . . ?
C31 Dy3 Cl4 131.42(14) . . ?
C33 Dy3 Cl4 90.62(13) . . ?
C34 Dy3 Cl4 80.22(13) . . ?
C35 Dy3 Cl4 103.17(13) . . ?
Cl8 Dy3 Cl3 92.49(4) . . ?
C32 Dy3 Cl3 84.43(13) . . ?
C31 Dy3 Cl3 85.17(14) . . ?
C33 Dy3 Cl3 112.80(13) . . ?
C34 Dy3 Cl3 134.20(13) . . ?
C35 Dy3 Cl3 114.17(13) . . ?
Cl4 Dy3 Cl3 142.65(4) . . ?
Cl8 Dy3 Cl9 75.68(4) . . ?
C32 Dy3 Cl9 153.20(13) . . ?
C31 Dy3 Cl9 154.03(13) . . ?
C33 Dy3 Cl9 151.61(13) . . ?
C34 Dy3 Cl9 151.84(13) . . ?
C35 Dy3 Cl9 153.19(13) . . ?
Cl4 Dy3 Cl9 72.32(4) . . ?
Cl3 Dy3 Cl9 73.90(4) . . ?
Cl8 Dy3 Cl1 144.46(4) . . ?
C32 Dy3 Cl1 90.55(14) . . ?
C31 Dy3 Cl1 120.65(15) . . ?
C33 Dy3 Cl1 85.80(13) . . ?
C34 Dy3 Cl1 111.94(14) . . ?
C35 Dy3 Cl1 137.14(13) . . ?
Cl4 Dy3 Cl1 78.52(4) . . ?
Cl3 Dy3 Cl1 74.87(4) . . ?
Cl9 Dy3 Cl1 68.95(4) . . ?
Cl8 Dy3 K1 46.11(4) . . ?
C32 Dy3 K1 117.87(13) . . ?
C31 Dy3 K1 97.35(13) . . ?
C33 Dy3 K1 148.06(13) . . ?
C34 Dy3 K1 138.28(13) . . ?
C35 Dy3 K1 107.67(13) . . ?
Cl4 Dy3 K1 119.90(3) . . ?
Cl3 Dy3 K1 48.22(3) . . ?
Cl9 Dy3 K1 57.20(3) . . ?
Cl1 Dy3 K1 107.98(3) . . ?
Cl8 Dy3 K3 46.06(4) . . ?
C32 Dy3 K3 159.00(13) . . ?
C31 Dy3 K3 132.22(15) . . ?
C33 Dy3 K3 136.43(13) . . ?
C34 Dy3 K3 109.85(13) . . ?
C35 Dy3 K3 107.74(13) . . ?
Cl4 Dy3 K3 53.70(3) . . ?
Cl3 Dy3 K3 110.75(3) . . ?
Cl9 Dy3 K3 47.72(3) . . ?
Cl1 Dy3 K3 107.08(3) . . ?
K1 Dy3 K3 68.12(2) . . ?
C41 Dy4 Cl7 82.44(13) . . ?
C41 Dy4 C45 31.07(19) . . ?
Cl7 Dy4 C45 111.23(14) . . ?
C41 Dy4 C42 31.21(19) . . ?
Cl7 Dy4 C42 82.18(13) . . ?
C45 Dy4 C42 51.56(18) . . ?
C41 Dy4 C44 51.58(17) . . ?
Cl7 Dy4 C44 131.90(13) . . ?
C45 Dy4 C44 31.22(17) . . ?
C42 Dy4 C44 51.72(18) . . ?
C41 Dy4 C43 51.43(17) . . ?
Cl7 Dy4 C43 111.20(13) . . ?
C45 Dy4 C43 51.29(18) . . ?
C42 Dy4 C43 31.30(17) . . ?
C44 Dy4 C43 31.00(18) . . ?
C41 Dy4 Cl12 122.75(14) . . ?
Cl7 Dy4 Cl12 91.71(4) . . ?
C45 Dy4 Cl12 130.14(13) . . ?
C42 Dy4 Cl12 91.54(14) . . ?
C44 Dy4 Cl12 101.29(13) . . ?
C43 Dy4 Cl12 79.49(13) . . ?
C41 Dy4 Cl17 92.77(14) . . ?
Cl7 Dy4 Cl17 89.58(4) . . ?
C45 Dy4 Cl17 81.73(13) . . ?
C42 Dy4 Cl17 123.92(14) . . ?
C44 Dy4 Cl17 104.17(13) . . ?
C43 Dy4 Cl17 132.57(13) . . ?
Cl12 Dy4 Cl17 144.32(4) . . ?
C41 Dy4 Cl10 129.10(14) . . ?
Cl7 Dy4 Cl10 146.51(4) . . ?
C45 Dy4 Cl10 98.33(14) . . ?
C42 Dy4 Cl10 130.14(13) . . ?
C44 Dy4 Cl10 81.58(13) . . ?
C43 Dy4 Cl10 99.34(13) . . ?
Cl12 Dy4 Cl10 80.33(4) . . ?
Cl17 Dy4 Cl10 79.14(4) . . ?
C41 Dy4 Cl14 153.88(12) . . ?
Cl7 Dy4 Cl14 76.15(4) . . ?
C45 Dy4 Cl14 153.28(13) . . ?
C42 Dy4 Cl14 152.88(13) . . ?
C44 Dy4 Cl14 151.93(13) . . ?
C43 Dy4 Cl14 152.03(13) . . ?
Cl12 Dy4 Cl14 73.23(4) . . ?
Cl17 Dy4 Cl14 72.50(4) . . ?
Cl10 Dy4 Cl14 70.39(4) . . ?
C41 Dy4 Dy6 160.16(12) . . ?
Cl7 Dy4 Dy6 108.72(3) . . ?
C45 Dy4 Dy6 139.76(13) . . ?
C42 Dy4 Dy6 131.83(13) . . ?
C44 Dy4 Dy6 112.21(12) . . ?
C43 Dy4 Dy6 108.74(12) . . ?
Cl12 Dy4 Dy6 42.98(3) . . ?
Cl17 Dy4 Dy6 103.41(3) . . ?
Cl10 Dy4 Dy6 45.77(3) . . ?
Cl14 Dy4 Dy6 45.30(2) . . ?
C41 Dy4 K3 107.09(12) . . ?
Cl7 Dy4 K3 46.38(3) . . ?
C45 Dy4 K3 119.10(13) . . ?
C42 Dy4 K3 123.39(13) . . ?
C44 Dy4 K3 149.71(13) . . ?
C43 Dy4 K3 154.68(13) . . ?
Cl12 Dy4 K3 108.89(3) . . ?
Cl17 Dy4 K3 50.59(3) . . ?
Cl10 Dy4 K3 105.56(3) . . ?
Cl14 Dy4 K3 46.90(3) . . ?
Dy6 Dy4 K3 92.164(17) . . ?
Cl15 Dy5 C55 127.01(13) . . ?
Cl15 Dy5 C54 127.72(12) . . ?
C55 Dy5 C54 31.56(18) . . ?
Cl15 Dy5 C51 96.10(13) . . ?
C55 Dy5 C51 31.25(18) . . ?
C54 Dy5 C51 51.65(18) . . ?
Cl15 Dy5 C53 97.06(13) . . ?
C55 Dy5 C53 52.03(18) . . ?
C54 Dy5 C53 31.30(17) . . ?
C51 Dy5 C53 51.64(19) . . ?
Cl15 Dy5 C52 79.46(13) . . ?
C55 Dy5 C52 51.56(18) . . ?
C54 Dy5 C52 51.38(17) . . ?
C51 Dy5 C52 31.01(18) . . ?
C53 Dy5 C52 31.07(18) . . ?
Cl15 Dy5 Cl17 94.26(4) . . ?
C55 Dy5 Cl17 84.86(13) . . ?
C54 Dy5 Cl17 115.26(13) . . ?
C51 Dy5 Cl17 81.31(14) . . ?
C53 Dy5 Cl17 132.42(14) . . ?
C52 Dy5 Cl17 108.43(14) . . ?
Cl15 Dy5 Cl11 93.49(4) . . ?
C55 Dy5 Cl11 118.50(13) . . ?
C54 Dy5 Cl11 87.97(13) . . ?
C51 Dy5 Cl11 134.26(14) . . ?
C53 Dy5 Cl11 82.85(14) . . ?
C52 Dy5 Cl11 109.24(14) . . ?
Cl17 Dy5 Cl11 142.32(4) . . ?
Cl15 Dy5 Cl14 76.65(4) . . ?
C55 Dy5 Cl14 149.16(13) . . ?
C54 Dy5 Cl14 150.90(12) . . ?
C51 Dy5 Cl14 152.23(13) . . ?
C53 Dy5 Cl14 154.84(14) . . ?
C52 Dy5 Cl14 156.09(13) . . ?
Cl17 Dy5 Cl14 72.70(4) . . ?
Cl11 Dy5 Cl14 73.39(4) . . ?
Cl15 Dy5 Cl10 146.10(4) . . ?
C55 Dy5 Cl10 85.49(13) . . ?
C54 Dy5 Cl10 84.51(12) . . ?
C51 Dy5 Cl10 114.70(13) . . ?
C53 Dy5 Cl10 112.80(12) . . ?
C52 Dy5 Cl10 134.42(13) . . ?
Cl17 Dy5 Cl10 77.66(4) . . ?
Cl11 Dy5 Cl10 75.49(4) . . ?
Cl14 Dy5 Cl10 69.49(4) . . ?
Cl15 Dy5 K2 48.06(3) . . ?
C55 Dy5 K2 158.17(12) . . ?
C54 Dy5 K2 129.22(13) . . ?
C51 Dy5 K2 138.92(13) . . ?
C53 Dy5 K2 106.15(13) . . ?
C52 Dy5 K2 111.01(13) . . ?
Cl17 Dy5 K2 115.52(3) . . ?
Cl11 Dy5 K2 49.69(3) . . ?
Cl14 Dy5 K2 51.60(3) . . ?
Cl10 Dy5 K2 105.69(3) . . ?
Cl15 Dy5 K3 46.80(3) . . ?
C55 Dy5 K3 129.39(13) . . ?
C54 Dy5 K3 158.47(13) . . ?
C51 Dy5 K3 106.83(13) . . ?
C53 Dy5 K3 139.59(12) . . ?
C52 Dy5 K3 111.70(13) . . ?
Cl17 Dy5 K3 52.83(3) . . ?
Cl11 Dy5 K3 112.11(3) . . ?
Cl14 Dy5 K3 48.98(3) . . ?
Cl10 Dy5 K3 107.36(3) . . ?
K2 Dy5 K3 65.90(2) . . ?
Cl16 Dy6 C65 129.00(13) . . ?
Cl16 Dy6 C64 128.62(13) . . ?
C65 Dy6 C64 31.22(17) . . ?
Cl16 Dy6 C62 80.93(13) . . ?
C65 Dy6 C62 51.32(18) . . ?
C64 Dy6 C62 51.57(17) . . ?
Cl16 Dy6 C61 98.44(13) . . ?
C65 Dy6 C61 31.12(17) . . ?
C64 Dy6 C61 51.75(16) . . ?
C62 Dy6 C61 31.17(18) . . ?
Cl16 Dy6 C63 97.55(12) . . ?
C65 Dy6 C63 51.65(17) . . ?
C64 Dy6 C63 31.44(17) . . ?
C62 Dy6 C63 31.10(17) . . ?
C61 Dy6 C63 51.73(17) . . ?
Cl16 Dy6 Cl12 92.24(4) . . ?
C65 Dy6 Cl12 115.97(13) . . ?
C64 Dy6 Cl12 85.59(12) . . ?
C62 Dy6 Cl12 107.34(13) . . ?
C61 Dy6 Cl12 132.04(12) . . ?
C63 Dy6 Cl12 80.61(13) . . ?
Cl16 Dy6 Cl11 93.68(4) . . ?
C65 Dy6 Cl11 87.36(12) . . ?
C64 Dy6 Cl11 117.45(13) . . ?
C62 Dy6 Cl11 109.24(13) . . ?
C61 Dy6 Cl11 82.57(12) . . ?
C63 Dy6 Cl11 134.01(13) . . ?
Cl12 Dy6 Cl11 143.41(4) . . ?
Cl16 Dy6 Cl14 75.76(4) . . ?
C65 Dy6 Cl14 150.35(13) . . ?
C64 Dy6 Cl14 148.90(12) . . ?
C62 Dy6 Cl14 156.68(12) . . ?
C61 Dy6 Cl14 154.76(12) . . ?
C63 Dy6 Cl14 152.49(13) . . ?
Cl12 Dy6 Cl14 73.14(4) . . ?
Cl11 Dy6 Cl14 73.46(4) . . ?
Cl16 Dy6 Cl10 145.59(4) . . ?
C65 Dy6 Cl10 83.88(13) . . ?
C64 Dy6 Cl10 84.21(13) . . ?
C62 Dy6 Cl10 133.48(12) . . ?
C61 Dy6 Cl10 112.25(14) . . ?
C63 Dy6 Cl10 113.37(12) . . ?
Cl12 Dy6 Cl10 78.91(4) . . ?
Cl11 Dy6 Cl10 75.96(4) . . ?
Cl14 Dy6 Cl10 69.84(4) . . ?
Cl16 Dy6 Dy4 108.80(3) . . ?
C65 Dy6 Dy4 120.84(13) . . ?
C64 Dy6 Dy4 103.59(12) . . ?
C62 Dy6 Dy4 146.78(12) . . ?
C61 Dy6 Dy4 151.92(13) . . ?
C63 Dy6 Dy4 116.00(12) . . ?
Cl12 Dy6 Dy4 42.49(3) . . ?
Cl11 Dy6 Dy4 101.89(3) . . ?
Cl14 Dy6 Dy4 45.65(2) . . ?
Cl10 Dy6 Dy4 44.62(3) . . ?
Cl16 Dy6 K2 48.16(3) . . ?
C65 Dy6 K2 128.84(12) . . ?
C64 Dy6 K2 158.03(12) . . ?
C62 Dy6 K2 111.78(12) . . ?
C61 Dy6 K2 106.36(12) . . ?
C63 Dy6 K2 140.00(12) . . ?
Cl12 Dy6 K2 115.19(3) . . ?
Cl11 Dy6 K2 49.51(3) . . ?
Cl14 Dy6 K2 51.42(3) . . ?
Cl10 Dy6 K2 105.88(3) . . ?
Dy4 Dy6 K2 97.040(17) . . ?
O12 K1 O11 78.85(15) . . ?
O12 K1 Cl8 153.19(12) . . ?
O11 K1 Cl8 74.35(11) . . ?
O12 K1 Cl7 113.57(12) . . ?
O11 K1 Cl7 118.97(13) . . ?
Cl8 K1 Cl7 80.97(5) . . ?
O12 K1 Cl3 109.59(13) . . ?
O11 K1 Cl3 104.43(13) . . ?
Cl8 K1 Cl3 76.76(4) . . ?
Cl7 K1 Cl3 122.86(5) . . ?
O12 K1 Cl6 88.97(11) . . ?
O11 K1 Cl6 165.94(12) . . ?
Cl8 K1 Cl6 117.47(5) . . ?
Cl7 K1 Cl6 72.32(4) . . ?
Cl3 K1 Cl6 72.89(4) . . ?
O12 K1 C118 23.53(16) . . ?
O11 K1 C118 99.24(16) . . ?
Cl8 K1 C118 166.01(14) . . ?
Cl7 K1 C118 112.88(14) . . ?
Cl3 K1 C118 93.22(14) . . ?
Cl6 K1 C118 67.48(12) . . ?
O12 K1 Cl9 146.62(12) . . ?
O11 K1 Cl9 133.08(11) . . ?
Cl8 K1 Cl9 59.48(4) . . ?
Cl7 K1 Cl9 63.97(4) . . ?
Cl3 K1 Cl9 59.31(4) . . ?
Cl6 K1 Cl9 58.00(4) . . ?
C118 K1 Cl9 123.64(13) . . ?
O12 K1 Dy3 147.90(13) . . ?
O11 K1 Dy3 95.83(11) . . ?
Cl8 K1 Dy3 37.54(3) . . ?
Cl7 K1 Dy3 96.82(4) . . ?
Cl3 K1 Dy3 40.61(3) . . ?
Cl6 K1 Dy3 90.75(4) . . ?
C118 K1 Dy3 133.78(14) . . ?
Cl9 K1 Dy3 41.55(2) . . ?
O12 K1 Dy2 110.47(12) . . ?
O11 K1 Dy2 143.37(12) . . ?
Cl8 K1 Dy2 90.95(4) . . ?
Cl7 K1 Dy2 90.54(4) . . ?
Cl3 K1 Dy2 38.97(3) . . ?
Cl6 K1 Dy2 36.27(3) . . ?
C118 K1 Dy2 87.08(13) . . ?
Cl9 K1 Dy2 39.65(2) . . ?
Dy3 K1 Dy2 56.930(16) . . ?
O12 K1 K3 154.81(12) . . ?
O11 K1 K3 104.96(11) . . ?
Cl8 K1 K3 40.29(3) . . ?
Cl7 K1 K3 42.44(3) . . ?
Cl3 K1 K3 93.77(4) . . ?
Cl6 K1 K3 89.05(4) . . ?
C118 K1 K3 152.21(13) . . ?
Cl9 K1 K3 42.12(3) . . ?
Dy3 K1 K3 57.24(2) . . ?
Dy2 K1 K3 81.64(3) . . ?
O21A K2 O22 72.0(5) . . ?
O22 K2 O21B 71.7(6) . . ?
O21A K2 Cl5 115.1(6) . . ?
O22 K2 Cl5 99.28(11) . . ?
O21B K2 Cl5 118.0(7) . . ?
O21A K2 Cl15 83.2(5) . . ?
O22 K2 Cl15 153.77(10) . . ?
O21B K2 Cl15 84.0(6) . . ?
Cl5 K2 Cl15 83.26(5) . . ?
O21A K2 Cl16 149.9(6) . . ?
O22 K2 Cl16 83.34(10) . . ?
O21B K2 Cl16 147.8(6) . . ?
Cl5 K2 Cl16 85.17(5) . . ?
Cl15 K2 Cl16 122.87(5) . . ?
O21A K2 Cl11 102.4(6) . . ?
O22 K2 Cl11 118.81(10) . . ?
O21B K2 Cl11 100.0(7) . . ?
Cl5 K2 Cl11 133.25(5) . . ?
Cl15 K2 Cl11 74.23(4) . . ?
Cl16 K2 Cl11 74.29(4) . . ?
O21A K2 Cl14 143.7(5) . . ?
O22 K2 Cl14 143.91(11) . . ?
O21B K2 Cl14 143.6(6) . . ?
Cl5 K2 Cl14 72.79(4) . . ?
Cl15 K2 Cl14 61.90(4) . . ?
Cl16 K2 Cl14 61.22(4) . . ?
Cl11 K2 Cl14 60.49(4) . . ?
O21A K2 C21A 21.2(5) . . ?
O22 K2 C21A 92.2(4) . . ?
Cl5 K2 C21A 119.3(4) . . ?
Cl15 K2 C21A 64.6(5) . . ?
Cl16 K2 C21A 155.5(4) . . ?
Cl11 K2 C21A 87.1(3) . . ?
Cl14 K2 C21A 122.7(4) . . ?
O21A K2 C125 65.7(6) . . ?
O22 K2 C125 22.29(15) . . ?
O21B K2 C125 64.2(6) . . ?
Cl5 K2 C125 121.53(13) . . ?
Cl15 K2 C125 145.95(14) . . ?
Cl16 K2 C125 84.94(13) . . ?
Cl11 K2 C125 98.32(12) . . ?
Cl14 K2 C125 143.10(12) . . ?
C21A K2 C125 82.1(5) . . ?
O21A K2 Dy5 104.1(5) . . ?
O22 K2 Dy5 158.22(10) . . ?
O21B K2 Dy5 103.4(6) . . ?
Cl5 K2 Dy5 101.61(4) . . ?
Cl15 K2 Dy5 37.24(3) . . ?
Cl16 K2 Dy5 92.31(4) . . ?
Cl11 K2 Dy5 39.99(3) . . ?
Cl14 K2 Dy5 41.37(3) . . ?
C21A K2 Dy5 82.9(4) . . ?
C125 K2 Dy5 136.25(12) . . ?
O21A K2 Dy6 140.6(6) . . ?
O22 K2 Dy6 112.08(9) . . ?
O21B K2 Dy6 137.9(7) . . ?
Cl5 K2 Dy6 103.06(4) . . ?
Cl15 K2 Dy6 92.47(4) . . ?
Cl16 K2 Dy6 37.31(3) . . ?
Cl11 K2 Dy6 39.78(3) . . ?
Cl14 K2 Dy6 41.24(2) . . ?
C21A K2 Dy6 126.9(3) . . ?
C125 K2 Dy6 102.69(11) . . ?
Dy5 K2 Dy6 56.947(16) . . ?
O31 K3 Cl8 74.95(12) . . ?
O31 K3 Cl15 76.98(13) . . ?
Cl8 K3 Cl15 151.68(6) . . ?
O31 K3 Cl9 127.34(14) . . ?
Cl8 K3 Cl9 62.87(4) . . ?
Cl15 K3 Cl9 141.71(5) . . ?
O31 K3 Cl14 130.09(15) . . ?
Cl8 K3 Cl14 137.35(5) . . ?
Cl15 K3 Cl14 62.72(4) . . ?
Cl9 K3 Cl14 102.54(5) . . ?
O31 K3 Cl7 132.90(12) . . ?
Cl8 K3 Cl7 76.19(4) . . ?
Cl15 K3 Cl7 122.26(5) . . ?
Cl9 K3 Cl7 66.25(4) . . ?
Cl14 K3 Cl7 61.64(4) . . ?
O31 K3 Cl5 130.94(12) . . ?
Cl8 K3 Cl5 122.94(5) . . ?
Cl15 K3 Cl5 79.23(4) . . ?
Cl9 K3 Cl5 62.49(4) . . ?
Cl14 K3 Cl5 70.59(4) . . ?
Cl7 K3 Cl5 96.03(5) . . ?
O31 K3 Cl17 82.59(14) . . ?
Cl8 K3 Cl17 100.95(5) . . ?
Cl15 K3 Cl17 71.60(4) . . ?
Cl9 K3 Cl17 133.33(5) . . ?
Cl14 K3 Cl17 58.36(4) . . ?
Cl7 K3 Cl17 67.39(4) . . ?
Cl5 K3 Cl17 128.37(5) . . ?
O31 K3 Cl4 80.02(14) . . ?
Cl8 K3 Cl4 71.05(4) . . ?
Cl15 K3 Cl4 107.63(5) . . ?
Cl9 K3 Cl4 58.07(4) . . ?
Cl14 K3 Cl4 137.92(5) . . ?
Cl7 K3 Cl4 123.46(5) . . ?
Cl5 K3 Cl4 67.35(4) . . ?
Cl17 K3 Cl4 162.24(5) . . ?
O31 K3 K4 178.19(15) . . ?
Cl8 K3 K4 104.01(4) . . ?
Cl15 K3 K4 104.15(4) . . ?
Cl9 K3 K4 50.95(3) . . ?
Cl14 K3 K4 51.66(3) . . ?
Cl7 K3 K4 47.71(3) . . ?
Cl5 K3 K4 48.34(3) . . ?
Cl17 K3 K4 99.09(4) . . ?
Cl4 K3 K4 98.26(4) . . ?
O31 K3 Dy5 89.51(14) . . ?
Cl8 K3 Dy5 139.16(4) . . ?
Cl15 K3 Dy5 36.36(3) . . ?
Cl9 K3 Dy5 143.13(4) . . ?
Cl14 K3 Dy5 40.59(3) . . ?
Cl7 K3 Dy5 88.69(3) . . ?
Cl5 K3 Dy5 95.91(4) . . ?
Cl17 K3 Dy5 38.80(2) . . ?
Cl4 K3 Dy5 143.94(4) . . ?
K4 K3 Dy5 92.21(3) . . ?
O31 K3 Dy3 86.82(14) . . ?
Cl8 K3 Dy3 36.08(3) . . ?
Cl15 K3 Dy3 145.38(4) . . ?
Cl9 K3 Dy3 40.58(3) . . ?
Cl14 K3 Dy3 142.81(4) . . ?
Cl7 K3 Dy3 91.15(4) . . ?
Cl5 K3 Dy3 89.23(3) . . ?
Cl17 K3 Dy3 136.85(4) . . ?
Cl4 K3 Dy3 38.63(2) . . ?
K4 K3 Dy3 91.49(3) . . ?
Dy5 K3 Dy3 174.84(3) . . ?
O41 K4 Cl7 126.17(11) . . ?
O41 K4 Cl5 133.29(12) . . ?
Cl7 K4 Cl5 100.54(5) . . ?
O41 K4 Cl9 132.32(11) . . ?
Cl7 K4 Cl9 66.21(4) . . ?
Cl5 K4 Cl9 62.38(4) . . ?
O41 K4 Cl14 129.27(11) . . ?
Cl7 K4 Cl14 61.59(4) . . ?
Cl5 K4 Cl14 70.47(4) . . ?
Cl9 K4 Cl14 97.91(4) . . ?
O41 K4 Cl6 81.49(10) . . ?
Cl7 K4 Cl6 69.15(4) . . ?
Cl5 K4 Cl6 119.53(5) . . ?
Cl9 K4 Cl6 59.16(4) . . ?
Cl14 K4 Cl6 130.73(5) . . ?
O41 K4 Cl16 81.40(10) . . ?
Cl7 K4 Cl16 115.98(5) . . ?
Cl5 K4 Cl16 78.23(4) . . ?
Cl9 K4 Cl16 139.55(5) . . ?
Cl14 K4 Cl16 58.05(4) . . ?
Cl6 K4 Cl16 161.24(5) . . ?
O41 K4 Cl2 86.40(11) . . ?
Cl7 K4 Cl2 120.26(5) . . ?
Cl5 K4 Cl2 67.30(4) . . ?
Cl9 K4 Cl2 56.30(4) . . ?
Cl14 K4 Cl2 137.24(5) . . ?
Cl6 K4 Cl2 68.84(4) . . ?
Cl16 K4 Cl2 117.57(5) . . ?
O41 K4 K3 176.13(11) . . ?
Cl7 K4 K3 50.06(3) . . ?
Cl5 K4 K3 50.50(4) . . ?
Cl9 K4 K3 48.60(3) . . ?
Cl14 K4 K3 49.37(3) . . ?
Cl6 K4 K3 97.10(4) . . ?
Cl16 K4 K3 99.47(4) . . ?
Cl2 K4 K3 96.47(4) . . ?
O41 K4 K2 119.69(10) . . ?
Cl7 K4 K2 101.42(4) . . ?
Cl5 K4 K2 39.15(3) . . ?
Cl9 K4 K2 97.48(4) . . ?
Cl14 K4 K2 44.68(3) . . ?
Cl6 K4 K2 156.59(4) . . ?
Cl16 K4 K2 42.17(3) . . ?
Cl2 K4 K2 100.67(4) . . ?
K3 K4 K2 62.39(3) . . ?
Dy1 Cl1 Dy3 90.10(4) . . ?
Dy1 Cl1 Dy2 89.52(3) . . ?
Dy3 Cl1 Dy2 91.02(4) . . ?
Dy1 Cl2 Dy2 94.73(4) . . ?
Dy1 Cl2 K4 90.51(4) . . ?
Dy2 Cl2 K4 90.45(4) . . ?
Dy3 Cl3 Dy2 96.11(4) . . ?
Dy3 Cl3 K1 91.17(4) . . ?
Dy2 Cl3 K1 95.12(4) . . ?
Dy1 Cl4 Dy3 95.14(4) . . ?
Dy1 Cl4 K3 91.16(4) . . ?
Dy3 Cl4 K3 87.67(4) . . ?
Dy1 Cl5 K2 158.15(6) . . ?
Dy1 Cl5 K4 100.52(5) . . ?
K2 Cl5 K4 99.28(5) . . ?
Dy1 Cl5 K3 97.23(5) . . ?
K2 Cl5 K3 94.85(5) . . ?
K4 Cl5 K3 81.16(4) . . ?
Dy2 Cl6 K1 94.84(4) . . ?
Dy2 Cl6 K4 95.38(4) . . ?
K1 Cl6 K4 99.07(5) . . ?
Dy4 Cl7 K1 142.75(6) . . ?
Dy4 Cl7 K4 103.72(5) . . ?
K1 Cl7 K4 111.21(5) . . ?
Dy4 Cl7 K3 98.67(5) . . ?
K1 Cl7 K3 98.47(5) . . ?
K4 Cl7 K3 82.23(4) . . ?
Dy3 Cl8 K1 96.35(5) . . ?
Dy3 Cl8 K3 97.86(5) . . ?
K1 Cl8 K3 100.99(5) . . ?
Dy2 Cl9 Dy1 90.69(4) . . ?
Dy2 Cl9 Dy3 93.35(4) . . ?
Dy1 Cl9 Dy3 90.14(3) . . ?
Dy2 Cl9 K3 172.14(5) . . ?
Dy1 Cl9 K3 95.31(4) . . ?
Dy3 Cl9 K3 91.70(4) . . ?
Dy2 Cl9 K4 94.16(4) . . ?
Dy1 Cl9 K4 93.47(4) . . ?
Dy3 Cl9 K4 171.63(5) . . ?
K3 Cl9 K4 80.45(4) . . ?
Dy2 Cl9 K1 85.31(4) . . ?
Dy1 Cl9 K1 170.26(5) . . ?
Dy3 Cl9 K1 81.25(4) . . ?
K3 Cl9 K1 89.52(4) . . ?
K4 Cl9 K1 95.68(4) . . ?
Dy4 Cl10 Dy6 89.60(4) . . ?
Dy4 Cl10 Dy5 90.40(3) . . ?
Dy6 Cl10 Dy5 90.90(4) . . ?
Dy6 Cl11 Dy5 96.05(4) . . ?
Dy6 Cl11 K2 90.71(4) . . ?
Dy5 Cl11 K2 90.31(4) . . ?
Dy4 Cl12 Dy6 94.52(4) . . ?
Dy6 Cl14 Dy5 92.34(4) . . ?
Dy6 Cl14 Dy4 89.05(3) . . ?
Dy5 Cl14 Dy4 90.33(4) . . ?
Dy6 Cl14 K3 176.03(5) . . ?
Dy5 Cl14 K3 90.43(4) . . ?
Dy4 Cl14 K3 93.79(4) . . ?
Dy6 Cl14 K2 87.34(4) . . ?
Dy5 Cl14 K2 87.03(4) . . ?
Dy4 Cl14 K2 175.43(5) . . ?
K3 Cl14 K2 89.96(4) . . ?
Dy6 Cl14 K4 98.11(4) . . ?
Dy5 Cl14 K4 169.01(5) . . ?
Dy4 Cl14 K4 93.24(4) . . ?
K3 Cl14 K4 78.97(4) . . ?
K2 Cl14 K4 90.04(4) . . ?
Dy5 Cl15 K2 94.70(4) . . ?
Dy5 Cl15 K3 96.84(4) . . ?
K2 Cl15 K3 94.59(5) . . ?
Dy6 Cl16 K2 94.53(5) . . ?
Dy6 Cl16 K4 100.08(5) . . ?
K2 Cl16 K4 90.72(4) . . ?
Dy4 Cl17 Dy5 95.29(4) . . ?
Dy4 Cl17 K3 92.07(4) . . ?
Dy5 Cl17 K3 88.36(4) . . ?
C111 O11 C114 105.0(6) . . ?
C111 O11 K1 128.2(4) . . ?
C114 O11 K1 126.8(5) . . ?
C115 O12 C118 107.6(5) . . ?
C115 O12 K1 140.8(4) . . ?
C118 O12 K1 107.1(4) . . ?
C128 O22 C125 107.1(5) . . ?
C128 O22 K2 115.3(4) . . ?
C125 O22 K2 111.0(4) . . ?
C134 O31 C131 110.5(5) . . ?
C134 O31 K3 124.8(4) . . ?
C131 O31 K3 124.7(4) . . ?
C141 O41 C144 104.3(5) . . ?
C141 O41 K4 120.9(4) . . ?
C144 O41 K4 121.3(4) . . ?
C15 C11 C12 108.6(5) . . ?
C15 C11 C16 124.8(5) . . ?
C12 C11 C16 126.0(5) . . ?
C15 C11 Dy1 74.7(3) . . ?
C12 C11 Dy1 74.1(3) . . ?
C16 C11 Dy1 124.2(4) . . ?
C13 C12 C11 107.8(5) . . ?
C13 C12 C17 126.5(5) . . ?
C11 C12 C17 125.5(6) . . ?
C13 C12 Dy1 73.9(3) . . ?
C11 C12 Dy1 74.8(3) . . ?
C17 C12 Dy1 121.5(4) . . ?
C12 C13 C14 108.2(5) . . ?
C12 C13 C18 126.1(5) . . ?
C14 C13 C18 125.6(5) . . ?
C12 C13 Dy1 74.9(3) . . ?
C14 C13 Dy1 74.9(3) . . ?
C18 C13 Dy1 119.2(4) . . ?
C15 C14 C13 107.3(5) . . ?
C15 C14 C19 126.6(5) . . ?
C13 C14 C19 125.7(5) . . ?
C15 C14 Dy1 74.8(3) . . ?
C13 C14 Dy1 73.6(3) . . ?
C19 C14 Dy1 122.9(4) . . ?
C11 C15 C14 108.1(5) . . ?
C11 C15 C20 126.6(5) . . ?
C14 C15 C20 124.9(5) . . ?
C11 C15 Dy1 74.4(3) . . ?
C14 C15 Dy1 74.0(3) . . ?
C20 C15 Dy1 123.4(3) . . ?
C25 C21 C22 107.9(5) . . ?
C25 C21 C26 125.8(5) . . ?
C22 C21 C26 126.0(5) . . ?
C25 C21 Dy2 76.1(3) . . ?
C22 C21 Dy2 73.8(3) . . ?
C26 C21 Dy2 120.9(4) . . ?
C23 C22 C21 107.8(5) . . ?
C23 C22 C27 126.7(5) . . ?
C21 C22 C27 125.3(5) . . ?
C23 C22 Dy2 74.7(3) . . ?
C21 C22 Dy2 74.6(3) . . ?
C27 C22 Dy2 119.0(4) . . ?
C24 C23 C22 108.0(5) . . ?
C24 C23 C28 125.4(5) . . ?
C22 C23 C28 126.4(5) . . ?
C24 C23 Dy2 75.5(3) . . ?
C22 C23 Dy2 73.9(3) . . ?
C28 C23 Dy2 121.1(4) . . ?
C25 C24 C23 108.3(5) . . ?
C25 C24 C29 125.8(5) . . ?
C23 C24 C29 125.6(5) . . ?
C25 C24 Dy2 75.1(3) . . ?
C23 C24 Dy2 73.3(3) . . ?
C29 C24 Dy2 122.1(4) . . ?
C24 C25 C21 108.0(5) . . ?
C24 C25 C30 126.0(5) . . ?
C21 C25 C30 125.5(5) . . ?
C24 C25 Dy2 74.0(3) . . ?
C21 C25 Dy2 72.8(3) . . ?
C30 C25 Dy2 124.6(4) . . ?
C32 C31 C35 108.0(5) . . ?
C32 C31 C36 125.8(6) . . ?
C35 C31 C36 126.0(6) . . ?
C32 C31 Dy3 74.3(3) . . ?
C35 C31 Dy3 75.7(3) . . ?
C36 C31 Dy3 119.9(4) . . ?
C31 C32 C33 108.4(5) . . ?
C31 C32 C37 126.2(6) . . ?
C33 C32 C37 124.9(6) . . ?
C31 C32 Dy3 74.4(3) . . ?
C33 C32 Dy3 75.2(3) . . ?
C37 C32 Dy3 122.3(4) . . ?
C34 C33 C32 107.5(5) . . ?
C34 C33 C38 126.0(6) . . ?
C32 C33 C38 126.3(6) . . ?
C34 C33 Dy3 74.8(3) . . ?
C32 C33 Dy3 73.6(3) . . ?
C38 C33 Dy3 121.5(4) . . ?
C33 C34 C35 108.6(5) . . ?
C33 C34 C39 126.5(5) . . ?
C35 C34 C39 124.6(6) . . ?
C33 C34 Dy3 74.1(3) . . ?
C35 C34 Dy3 74.7(3) . . ?
C39 C34 Dy3 122.4(4) . . ?
C31 C35 C34 107.4(5) . . ?
C31 C35 C40 126.2(6) . . ?
C34 C35 C40 126.1(6) . . ?
C31 C35 Dy3 73.1(3) . . ?
C34 C35 Dy3 74.2(3) . . ?
C40 C35 Dy3 123.0(4) . . ?
C45 C41 C42 108.7(5) . . ?
C45 C41 C46 123.6(6) . . ?
C42 C41 C46 127.5(6) . . ?
C45 C41 Dy4 75.1(3) . . ?
C42 C41 Dy4 75.1(3) . . ?
C46 C41 Dy4 120.4(4) . . ?
C41 C42 C43 107.5(5) . . ?
C41 C42 C47 127.5(6) . . ?
C43 C42 C47 124.8(6) . . ?
C41 C42 Dy4 73.7(3) . . ?
C43 C42 Dy4 75.7(3) . . ?
C47 C42 Dy4 120.0(4) . . ?
C44 C43 C42 107.9(5) . . ?
C44 C43 C48 125.5(6) . . ?
C42 C43 C48 126.0(6) . . ?
C44 C43 Dy4 74.1(3) . . ?
C42 C43 Dy4 73.0(3) . . ?
C48 C43 Dy4 125.7(4) . . ?
C43 C44 C45 107.4(5) . . ?
C43 C44 C49 126.2(5) . . ?
C45 C44 C49 125.9(6) . . ?
C43 C44 Dy4 74.9(3) . . ?
C45 C44 Dy4 73.4(3) . . ?
C49 C44 Dy4 123.8(4) . . ?
C41 C45 C44 108.4(5) . . ?
C41 C45 C50 127.3(6) . . ?
C44 C45 C50 123.6(6) . . ?
C41 C45 Dy4 73.9(3) . . ?
C44 C45 Dy4 75.4(3) . . ?
C50 C45 Dy4 123.9(4) . . ?
C55 C51 C52 108.7(5) . . ?
C55 C51 C56 125.5(6) . . ?
C52 C51 C56 125.2(6) . . ?
C55 C51 Dy5 74.0(3) . . ?
C52 C51 Dy5 76.2(3) . . ?
C56 C51 Dy5 122.6(4) . . ?
C51 C52 C53 107.9(5) . . ?
C51 C52 C57 127.1(6) . . ?
C53 C52 C57 124.7(6) . . ?
C51 C52 Dy5 72.8(3) . . ?
C53 C52 Dy5 73.5(3) . . ?
C57 C52 Dy5 124.7(4) . . ?
C54 C53 C52 107.6(5) . . ?
C54 C53 C58 126.2(5) . . ?
C52 C53 C58 125.8(5) . . ?
C54 C53 Dy5 73.6(3) . . ?
C52 C53 Dy5 75.4(3) . . ?
C58 C53 Dy5 122.5(4) . . ?
C53 C54 C55 108.3(5) . . ?
C53 C54 C59 125.4(6) . . ?
C55 C54 C59 126.0(5) . . ?
C53 C54 Dy5 75.1(3) . . ?
C55 C54 Dy5 73.9(3) . . ?
C59 C54 Dy5 121.7(4) . . ?
C51 C55 C54 107.5(5) . . ?
C51 C55 C60 126.6(6) . . ?
C54 C55 C60 125.7(5) . . ?
C51 C55 Dy5 74.8(3) . . ?
C54 C55 Dy5 74.6(3) . . ?
C60 C55 Dy5 120.8(4) . . ?
C65 C61 C62 107.4(5) . . ?
C65 C61 C66 125.8(6) . . ?
C62 C61 C66 126.3(6) . . ?
C65 C61 Dy6 74.1(3) . . ?
C62 C61 Dy6 74.4(3) . . ?
C66 C61 Dy6 123.3(4) . . ?
C63 C62 C61 108.8(5) . . ?
C63 C62 C67 126.6(6) . . ?
C61 C62 C67 124.2(5) . . ?
C63 C62 Dy6 74.6(3) . . ?
C61 C62 Dy6 74.5(3) . . ?
C67 C62 Dy6 123.0(4) . . ?
C62 C63 C64 107.4(5) . . ?
C62 C63 C68 126.2(5) . . ?
C64 C63 C68 126.0(5) . . ?
C62 C63 Dy6 74.3(3) . . ?
C64 C63 Dy6 74.0(3) . . ?
C68 C63 Dy6 122.8(4) . . ?
C65 C64 C63 107.6(5) . . ?
C65 C64 C69 126.7(5) . . ?
C63 C64 C69 125.5(5) . . ?
C65 C64 Dy6 74.2(3) . . ?
C63 C64 Dy6 74.6(3) . . ?
C69 C64 Dy6 121.4(4) . . ?
C61 C65 C64 108.8(5) . . ?
C61 C65 C70 125.1(5) . . ?
C64 C65 C70 125.8(5) . . ?
C61 C65 Dy6 74.8(3) . . ?
C64 C65 Dy6 74.5(3) . . ?
C70 C65 Dy6 121.9(4) . . ?
O11 C111 C112 106.3(6) . . ?
C111 C112 C113 103.5(7) . . ?
C114 C113 C112 104.8(7) . . ?
O11 C114 C113 103.6(7) . . ?
O12 C115 C116 107.4(6) . . ?
C115 C116 C117 103.3(6) . . ?
C118 C117 C116 103.0(7) . . ?
O12 C118 C117 104.4(7) . . ?
O12 C118 K1 49.4(3) . . ?
C117 C118 K1 128.0(5) . . ?
C21A O21A C24A 107.0(11) . . ?
C21A O21A K2 117.8(16) . . ?
C24A O21A K2 128.9(19) . . ?
O21A C21A C22A 103.7(13) . . ?
O21A C21A K2 40.9(12) . . ?
C22A C21A K2 119.8(16) . . ?
C21A C22A C23A 102.2(13) . . ?
C24A C23A C22A 103.3(12) . . ?
O21A C24A C23A 107.9(10) . . ?
C21B O21B C24B 108.5(12) . . ?
C21B O21B K2 117(2) . . ?
C24B O21B K2 112(3) . . ?
O21B C21B C22B 105.6(12) . . ?
C21B C22B C23B 102.4(13) . . ?
C24B C23B C22B 99.9(15) . . ?
O21B C24B C23B 107.7(13) . . ?
O22 C125 C126 103.5(6) . . ?
O22 C125 K2 46.7(3) . . ?
C126 C125 K2 97.6(4) . . ?
C125 C126 C127 102.4(6) . . ?
C126 C127 C128 103.5(6) . . ?
O22 C128 C127 107.0(6) . . ?
O31 C131 C132 105.6(6) . . ?
C133 C132 C131 103.9(7) . . ?
C132 C133 C134 104.5(7) . . ?
O31 C134 C133 106.7(6) . . ?
O41 C141 C142 105.9(5) . . ?
C141 C142 C143 104.0(6) . . ?
C144 C143 C142 103.8(6) . . ?
O41 C144 C143 104.3(6) . . ?
Cl26 Dy7 C71 95.74(17) . . ?
Cl26 Dy7 C74 128.24(15) . . ?
C71 Dy7 C74 51.2(2) . . ?
Cl26 Dy7 C75 126.74(15) . . ?
C71 Dy7 C75 31.3(2) . . ?
C74 Dy7 C75 30.9(2) . . ?
Cl26 Dy7 C73 98.49(17) . . ?
C71 Dy7 C73 51.3(2) . . ?
C74 Dy7 C73 30.6(2) . . ?
C75 Dy7 C73 51.1(2) . . ?
Cl26 Dy7 C72 79.79(15) . . ?
C71 Dy7 C72 31.1(2) . . ?
C74 Dy7 C72 51.0(2) . . ?
C75 Dy7 C72 51.4(2) . . ?
C73 Dy7 C72 31.0(2) . . ?
Cl26 Dy7 Cl22 96.05(5) . . ?
C71 Dy7 Cl22 132.02(16) . . ?
C74 Dy7 Cl22 86.04(16) . . ?
C75 Dy7 Cl22 115.94(17) . . ?
C73 Dy7 Cl22 81.03(16) . . ?
C72 Dy7 Cl22 107.40(17) . . ?
Cl26 Dy7 Cl24 92.04(4) . . ?
C71 Dy7 Cl24 83.40(16) . . ?
C74 Dy7 Cl24 116.95(17) . . ?
C75 Dy7 Cl24 87.25(17) . . ?
C73 Dy7 Cl24 134.11(16) . . ?
C72 Dy7 Cl24 110.37(17) . . ?
Cl22 Dy7 Cl24 142.19(4) . . ?
Cl26 Dy7 Cl28 76.95(4) . . ?
C71 Dy7 Cl28 155.24(16) . . ?
C74 Dy7 Cl28 149.34(14) . . ?
C75 Dy7 Cl28 150.57(15) . . ?
C73 Dy7 Cl28 152.51(16) . . ?
C72 Dy7 Cl28 156.58(15) . . ?
Cl22 Dy7 Cl28 72.66(4) . . ?
Cl24 Dy7 Cl28 73.38(4) . . ?
Cl26 Dy7 Cl21 146.11(5) . . ?
C71 Dy7 Cl21 113.02(17) . . ?
C74 Dy7 Cl21 85.06(14) . . ?
C75 Dy7 Cl21 84.40(14) . . ?
C73 Dy7 Cl21 113.23(17) . . ?
C72 Dy7 Cl21 133.96(15) . . ?
Cl22 Dy7 Cl21 78.22(4) . . ?
Cl24 Dy7 Cl21 74.71(4) . . ?
Cl28 Dy7 Cl21 69.43(4) . . ?
Cl26 Dy7 K5 47.39(4) . 2_756 ?
C71 Dy7 K5 103.88(16) . 2_756 ?
C74 Dy7 K5 154.88(15) . 2_756 ?
C75 Dy7 K5 126.03(17) . 2_756 ?
C73 Dy7 K5 139.54(16) . 2_756 ?
C72 Dy7 K5 110.43(16) . 2_756 ?
Cl22 Dy7 K5 118.03(4) . 2_756 ?
Cl24 Dy7 K5 48.16(3) . 2_756 ?
Cl28 Dy7 K5 53.82(3) . 2_756 ?
Cl21 Dy7 K5 105.81(3) . 2_756 ?
Cl26 Dy7 K6 48.69(4) . . ?
C71 Dy7 K6 139.85(17) . . ?
C74 Dy7 K6 131.45(17) . . ?
C75 Dy7 K6 159.83(16) . . ?
C73 Dy7 K6 108.72(16) . . ?
C72 Dy7 K6 112.40(15) . . ?
Cl22 Dy7 K6 52.88(4) . . ?
Cl24 Dy7 K6 111.58(4) . . ?
Cl28 Dy7 K6 48.12(3) . . ?
Cl21 Dy7 K6 106.92(3) . . ?
K5 Dy7 K6 67.87(3) 2_756 . ?
Cl27 Dy8 C84 83.41(14) . . ?
Cl27 Dy8 C85 85.43(14) . . ?
C84 Dy8 C85 31.3(2) . . ?
Cl27 Dy8 C83 111.23(13) . . ?
C84 Dy8 C83 31.05(18) . . ?
C85 Dy8 C83 51.5(2) . . ?
Cl27 Dy8 C82 133.60(13) . . ?
C84 Dy8 C82 51.43(17) . . ?
C85 Dy8 C82 51.11(19) . . ?
C83 Dy8 C82 31.37(17) . . ?
Cl27 Dy8 C81 114.74(13) . . ?
C84 Dy8 C81 51.78(18) . . ?
C85 Dy8 C81 31.19(18) . . ?
C83 Dy8 C81 51.70(17) . . ?
C82 Dy8 C81 30.83(18) . . ?
Cl27 Dy8 Cl23 90.46(5) . . ?
C84 Dy8 Cl23 121.51(14) . . ?
C85 Dy8 Cl23 90.32(15) . . ?
C83 Dy8 Cl23 131.65(12) . . ?
C82 Dy8 Cl23 103.48(13) . . ?
C81 Dy8 Cl23 80.11(13) . . ?
Cl27 Dy8 Cl22 89.04(5) . . ?
C84 Dy8 Cl22 94.49(14) . . ?
C85 Dy8 Cl22 125.79(15) . . ?
C83 Dy8 Cl22 81.57(13) . . ?
C82 Dy8 Cl22 102.95(13) . . ?
C81 Dy8 Cl22 132.15(13) . . ?
Cl23 Dy8 Cl22 143.69(4) . . ?
Cl27 Dy8 Cl21 146.24(4) . . ?
C84 Dy8 Cl21 128.81(14) . . ?
C85 Dy8 Cl21 126.84(13) . . ?
C83 Dy8 Cl21 98.55(13) . . ?
C82 Dy8 Cl21 80.13(13) . . ?
C81 Dy8 Cl21 95.92(13) . . ?
Cl23 Dy8 Cl21 80.82(4) . . ?
Cl22 Dy8 Cl21 79.68(4) . . ?
Cl27 Dy8 Cl28 76.22(4) . . ?
C84 Dy8 Cl28 155.66(13) . . ?
C85 Dy8 Cl28 154.42(15) . . ?
C83 Dy8 Cl28 152.79(13) . . ?
C82 Dy8 Cl28 150.16(13) . . ?
C81 Dy8 Cl28 150.65(13) . . ?
Cl23 Dy8 Cl28 72.41(4) . . ?
Cl22 Dy8 Cl28 72.24(4) . . ?
Cl21 Dy8 Cl28 70.04(4) . . ?
Cl27 Dy8 Dy9 108.93(4) . . ?
C84 Dy8 Dy9 157.95(13) . . ?
C85 Dy8 Dy9 129.03(14) . . ?
C83 Dy8 Dy9 139.58(12) . . ?
C82 Dy8 Dy9 111.23(12) . . ?
C81 Dy8 Dy9 106.20(13) . . ?
Cl23 Dy8 Dy9 42.94(3) . . ?
Cl22 Dy8 Dy9 103.69(3) . . ?
Cl21 Dy8 Dy9 45.33(3) . . ?
Cl28 Dy8 Dy9 45.56(3) . . ?
Cl27 Dy8 K6 45.32(4) . . ?
C84 Dy8 K6 109.02(13) . . ?
C85 Dy8 K6 126.46(13) . . ?
C83 Dy8 K6 119.54(12) . . ?
C82 Dy8 K6 149.89(13) . . ?
C81 Dy8 K6 157.63(13) . . ?
Cl23 Dy8 K6 106.59(4) . . ?
Cl22 Dy8 K6 51.37(4) . . ?
Cl21 Dy8 K6 106.15(3) . . ?
Cl28 Dy8 K6 46.74(3) . . ?
Dy9 Dy8 K6 92.21(2) . . ?
Cl25 Dy9 C93 121.67(17) . . ?
Cl25 Dy9 C92 90.49(17) . . ?
C93 Dy9 C92 31.4(2) . . ?
Cl25 Dy9 C91 81.04(14) . . ?
C93 Dy9 C91 51.5(2) . . ?
C92 Dy9 C91 31.0(2) . . ?
Cl25 Dy9 C94 132.37(15) . . ?
C93 Dy9 C94 31.18(19) . . ?
C92 Dy9 C94 51.6(2) . . ?
C91 Dy9 C94 51.5(2) . . ?
Cl25 Dy9 C95 104.76(14) . . ?
C93 Dy9 C95 51.44(19) . . ?
C92 Dy9 C95 51.44(18) . . ?
C91 Dy9 C95 31.13(18) . . ?
C94 Dy9 C95 31.02(19) . . ?
Cl25 Dy9 Cl23 93.14(5) . . ?
C93 Dy9 Cl23 123.61(15) . . ?
C92 Dy9 Cl23 129.68(14) . . ?
C91 Dy9 Cl23 100.45(14) . . ?
C94 Dy9 Cl23 92.44(14) . . ?
C95 Dy9 Cl23 79.30(13) . . ?
Cl25 Dy9 Cl24 91.62(5) . . ?
C93 Dy9 Cl24 83.64(14) . . ?
C92 Dy9 Cl24 86.98(15) . . ?
C91 Dy9 Cl24 116.61(14) . . ?
C94 Dy9 Cl24 110.90(14) . . ?
C95 Dy9 Cl24 134.42(13) . . ?
Cl23 Dy9 Cl24 142.93(4) . . ?
Cl25 Dy9 Cl21 145.34(4) . . ?
C93 Dy9 Cl21 89.30(16) . . ?
C92 Dy9 Cl21 120.15(18) . . ?
C91 Dy9 Cl21 133.55(14) . . ?
C94 Dy9 Cl21 82.11(14) . . ?
C95 Dy9 Cl21 107.13(14) . . ?
Cl23 Dy9 Cl21 79.86(4) . . ?
Cl24 Dy9 Cl21 75.55(4) . . ?
Cl25 Dy9 Cl28 75.88(4) . . ?
C93 Dy9 Cl28 151.76(15) . . ?
C92 Dy9 Cl28 155.38(14) . . ?
C91 Dy9 Cl28 155.27(15) . . ?
C94 Dy9 Cl28 149.64(14) . . ?
C95 Dy9 Cl28 151.64(13) . . ?
Cl23 Dy9 Cl28 72.37(4) . . ?
Cl24 Dy9 Cl28 73.26(4) . . ?
Cl21 Dy9 Cl28 69.62(4) . . ?
Cl25 Dy9 Dy8 110.20(3) . . ?
C93 Dy9 Dy8 127.74(16) . . ?
C92 Dy9 Dy8 157.08(16) . . ?
C91 Dy9 Dy8 140.03(13) . . ?
C94 Dy9 Dy8 105.59(14) . . ?
C95 Dy9 Dy8 111.37(12) . . ?
Cl23 Dy9 Dy8 42.68(3) . . ?
Cl24 Dy9 Dy8 101.68(3) . . ?
Cl21 Dy9 Dy8 44.52(3) . . ?
Cl28 Dy9 Dy8 45.77(3) . . ?
Cl25 Dy9 K5 47.79(4) . 2_756 ?
C93 Dy9 K5 119.88(15) . 2_756 ?
C92 Dy9 K5 102.70(14) . 2_756 ?
C91 Dy9 K5 115.22(13) . 2_756 ?
C94 Dy9 K5 150.98(14) . 2_756 ?
C95 Dy9 K5 146.06(13) . 2_756 ?
Cl23 Dy9 K5 116.36(3) . 2_756 ?
Cl24 Dy9 K5 47.35(3) . 2_756 ?
Cl21 Dy9 K5 105.30(3) . 2_756 ?
Cl28 Dy9 K5 53.02(3) . 2_756 ?
Dy8 Dy9 K5 98.656(18) . 2_756 ?
O52 K5 O51 74.72(17) . . ?
O52 K5 Cl27 106.26(14) . . ?
O51 K5 Cl27 107.45(15) . . ?
O52 K5 Cl26 86.38(12) . 2_756 ?
O51 K5 Cl26 160.92(13) . 2_756 ?
Cl27 K5 Cl26 80.02(5) . 2_756 ?
O52 K5 Cl24 114.23(13) . 2_756 ?
O51 K5 Cl24 110.25(14) . 2_756 ?
Cl27 K5 Cl24 130.13(6) . 2_756 ?
Cl26 K5 Cl24 74.92(5) 2_756 2_756 ?
O52 K5 Cl25 152.07(13) . 2_756 ?
O51 K5 Cl25 77.43(12) . 2_756 ?
Cl27 K5 Cl25 84.04(5) . 2_756 ?
Cl26 K5 Cl25 121.30(5) 2_756 2_756 ?
Cl24 K5 Cl25 73.76(5) 2_756 2_756 ?
O52 K5 C151 73.1(2) . . ?
O51 K5 C151 21.9(3) . . ?
Cl27 K5 C151 129.2(2) . . ?
Cl26 K5 C151 147.6(2) 2_756 . ?
Cl24 K5 C151 90.7(2) 2_756 . ?
Cl25 K5 C151 80.3(2) 2_756 . ?
O52 K5 Cl28 147.53(13) . 2_756 ?
O51 K5 Cl28 137.71(13) . 2_756 ?
Cl27 K5 Cl28 70.05(4) . 2_756 ?
Cl26 K5 Cl28 61.15(4) 2_756 2_756 ?
Cl24 K5 Cl28 60.13(4) 2_756 2_756 ?
Cl25 K5 Cl28 60.28(4) 2_756 2_756 ?
C151 K5 Cl28 135.3(2) . 2_756 ?
O52 K5 Dy7 111.77(12) . 2_756 ?
O51 K5 Dy7 150.43(14) . 2_756 ?
Cl27 K5 Dy7 98.46(4) . 2_756 ?
Cl26 K5 Dy7 37.24(3) 2_756 2_756 ?
Cl24 K5 Dy7 40.25(3) 2_756 2_756 ?
Cl25 K5 Dy7 91.65(4) 2_756 2_756 ?
C151 K5 Dy7 129.8(2) . 2_756 ?
Cl28 K5 Dy7 41.18(3) 2_756 2_756 ?
O52 K5 Dy9 152.06(14) . 2_756 ?
O51 K5 Dy9 103.26(12) . 2_756 ?
Cl27 K5 Dy9 100.93(4) . 2_756 ?
Cl26 K5 Dy9 92.17(4) 2_756 2_756 ?
Cl24 K5 Dy9 39.37(3) 2_756 2_756 ?
Cl25 K5 Dy9 36.93(3) 2_756 2_756 ?
C151 K5 Dy9 94.7(2) . 2_756 ?
Cl28 K5 Dy9 41.08(2) 2_756 2_756 ?
Dy7 K5 Dy9 56.943(17) 2_756 2_756 ?
O52 K5 K6 148.04(14) . . ?
O51 K5 K6 105.48(13) . . ?
Cl27 K5 K6 42.35(4) . . ?
Cl26 K5 K6 91.88(4) 2_756 . ?
Cl24 K5 K6 95.95(4) 2_756 . ?
Cl25 K5 K6 44.82(4) 2_756 . ?
C151 K5 K6 118.8(2) . . ?
Cl28 K5 K6 43.26(3) 2_756 . ?
Dy7 K5 K6 84.13(3) 2_756 . ?
Dy9 K5 K6 59.85(2) 2_756 . ?
O52 K5 K6 112.84(13) . 2_756 ?
O51 K5 K6 148.79(15) . 2_756 ?
Cl27 K5 K6 41.60(4) . 2_756 ?
Cl26 K5 K6 43.01(4) 2_756 2_756 ?
Cl24 K5 K6 94.49(4) 2_756 2_756 ?
Cl25 K5 K6 92.26(4) 2_756 2_756 ?
C151 K5 K6 169.4(2) . 2_756 ?
Cl28 K5 K6 42.67(3) 2_756 2_756 ?
Dy7 K5 K6 57.47(2) 2_756 2_756 ?
Dy9 K5 K6 83.65(3) 2_756 2_756 ?
K6 K5 K6 51.48(3) . 2_756 ?
O61A K6 Cl27 131.8(2) . . ?
O61B K6 Cl27 118.5(4) . . ?
O61A K6 Cl28 134.4(3) . 2_756 ?
O61B K6 Cl28 133.1(3) . 2_756 ?
Cl27 K6 Cl28 69.90(4) . 2_756 ?
Cl27 K6 Cl27 100.45(5) . 2_756 ?
Cl28 K6 Cl27 62.16(4) 2_756 2_756 ?
O61A K6 Cl28 124.6(3) . . ?
O61B K6 Cl28 124.5(3) . . ?
Cl27 K6 Cl28 62.20(4) . . ?
Cl28 K6 Cl28 100.84(5) 2_756 . ?
Cl27 K6 Cl28 69.31(4) 2_756 . ?
O61A K6 Cl26 73.4(3) . . ?
O61B K6 Cl26 82.3(4) . . ?
Cl27 K6 Cl26 121.21(5) . . ?
Cl28 K6 Cl26 135.99(6) 2_756 . ?
Cl27 K6 Cl26 73.83(5) 2_756 . ?
Cl28 K6 Cl26 61.33(4) . . ?
Cl27 K6 Cl25 78.17(5) . 2_756 ?
Cl28 K6 Cl25 60.83(4) 2_756 2_756 ?
Cl27 K6 Cl25 119.33(6) 2_756 2_756 ?
Cl28 K6 Cl25 140.31(6) . 2_756 ?
Cl26 K6 Cl25 155.98(6) . 2_756 ?
O61A K6 C61A 19.6(3) . . ?
Cl27 K6 C61A 151.1(2) . . ?
Cl28 K6 C61A 125.4(3) 2_756 . ?
Cl27 K6 C61A 108.4(2) 2_756 . ?
Cl28 K6 C61A 127.2(3) . . ?
Cl26 K6 C61A 67.4(3) . . ?
Cl25 K6 C61A 88.8(3) 2_756 . ?
O61A K6 Cl22 79.0(3) . . ?
O61B K6 Cl22 71.9(3) . . ?
Cl27 K6 Cl22 66.81(4) . . ?
Cl28 K6 Cl22 136.70(5) 2_756 . ?
Cl27 K6 Cl22 125.34(5) 2_756 . ?
Cl28 K6 Cl22 57.61(4) . . ?
Cl26 K6 Cl22 70.48(4) . . ?
Cl25 K6 Cl22 109.83(5) 2_756 . ?
C61A K6 Cl22 94.5(3) . . ?
Cl27 K6 Cl23 125.07(5) . 2_756 ?
Cl28 K6 Cl23 56.46(4) 2_756 2_756 ?
Cl27 K6 Cl23 65.80(4) 2_756 2_756 ?
Cl28 K6 Cl23 135.09(6) . 2_756 ?
Cl26 K6 Cl23 106.01(5) . 2_756 ?
Cl25 K6 Cl23 66.85(4) 2_756 2_756 ?
Cl22 K6 Cl23 164.30(6) . 2_756 ?
Cl27 K6 K6 50.51(4) . 2_756 ?
Cl28 K6 K6 50.65(4) 2_756 2_756 ?
Cl27 K6 K6 49.95(4) 2_756 2_756 ?
Cl28 K6 K6 50.19(4) . 2_756 ?
Cl26 K6 K6 100.65(6) . 2_756 ?
Cl25 K6 K6 102.99(6) 2_756 2_756 ?
Cl22 K6 K6 98.48(5) . 2_756 ?
Cl23 K6 K6 97.21(5) 2_756 2_756 ?
Dy8 Cl21 Dy9 90.15(4) . . ?
Dy8 Cl21 Dy7 90.32(4) . . ?
Dy9 Cl21 Dy7 91.78(4) . . ?
Dy8 Cl22 Dy7 95.19(4) . . ?
Dy8 Cl22 K6 91.55(5) . . ?
Dy7 Cl22 K6 89.02(4) . . ?
Dy8 Cl23 Dy9 94.38(4) . . ?
Dy8 Cl23 K6 89.93(4) . 2_756 ?
Dy9 Cl23 K6 89.89(4) . 2_756 ?
Dy9 Cl24 Dy7 96.13(4) . . ?
Dy9 Cl24 K5 93.28(5) . 2_756 ?
Dy7 Cl24 K5 91.59(4) . 2_756 ?
Dy9 Cl25 K5 95.28(5) . 2_756 ?
Dy9 Cl25 K6 98.47(5) . 2_756 ?
K5 Cl25 K6 92.85(5) 2_756 2_756 ?
Dy7 Cl26 K5 95.36(5) . 2_756 ?
Dy7 Cl26 K6 95.47(5) . . ?
K5 Cl26 K6 96.70(5) 2_756 . ?
Dy8 Cl27 K5 153.77(6) . . ?
Dy8 Cl27 K6 99.90(5) . . ?
K5 Cl27 K6 99.00(5) . . ?
Dy8 Cl27 K6 100.42(5) . 2_756 ?
K5 Cl27 K6 100.76(6) . 2_756 ?
K6 Cl27 K6 79.55(5) . 2_756 ?
Dy7 Cl28 Dy9 92.52(4) . . ?
Dy7 Cl28 Dy8 90.04(4) . . ?
Dy9 Cl28 Dy8 88.67(3) . . ?
Dy7 Cl28 K6 169.94(5) . 2_756 ?
Dy9 Cl28 K6 95.95(4) . 2_756 ?
Dy8 Cl28 K6 95.57(4) . 2_756 ?
Dy7 Cl28 K6 92.15(4) . . ?
Dy9 Cl28 K6 174.61(6) . . ?
Dy8 Cl28 K6 94.02(4) . . ?
K6 Cl28 K6 79.16(5) 2_756 . ?
Dy7 Cl28 K5 85.00(4) . 2_756 ?
Dy9 Cl28 K5 85.90(4) . 2_756 ?
Dy8 Cl28 K5 172.47(5) . 2_756 ?
K6 Cl28 K5 90.19(5) 2_756 2_756 ?
K6 Cl28 K5 91.83(4) . 2_756 ?
C151 O51 C154 108.5(7) . . ?
C151 O51 K5 111.2(8) . . ?
C154 O51 K5 123.1(5) . . ?
C158 O52 C155 107.6(5) . . ?
C158 O52 K5 130.7(4) . . ?
C155 O52 K5 121.1(4) . . ?
C75 C71 C72 108.3(6) . . ?
C75 C71 C76 125.8(8) . . ?
C72 C71 C76 125.6(7) . . ?
C75 C71 Dy7 74.6(4) . . ?
C72 C71 Dy7 76.0(4) . . ?
C76 C71 Dy7 121.3(5) . . ?
C71 C72 C73 107.0(6) . . ?
C71 C72 C77 125.6(7) . . ?
C73 C72 C77 126.9(8) . . ?
C71 C72 Dy7 73.0(4) . . ?
C73 C72 Dy7 73.9(4) . . ?
C77 C72 Dy7 124.5(5) . . ?
C74 C73 C72 108.1(6) . . ?
C74 C73 C78 125.9(8) . . ?
C72 C73 C78 125.7(8) . . ?
C74 C73 Dy7 73.9(4) . . ?
C72 C73 Dy7 75.1(4) . . ?
C78 C73 Dy7 122.0(5) . . ?
C73 C74 C75 109.3(6) . . ?
C73 C74 C79 125.9(8) . . ?
C75 C74 C79 124.4(7) . . ?
C73 C74 Dy7 75.5(4) . . ?
C75 C74 Dy7 74.8(4) . . ?
C79 C74 Dy7 121.1(5) . . ?
C74 C75 C71 107.2(6) . . ?
C74 C75 C80 126.4(7) . . ?
C71 C75 C80 126.2(7) . . ?
C74 C75 Dy7 74.3(4) . . ?
C71 C75 Dy7 74.1(4) . . ?
C80 C75 Dy7 120.7(5) . . ?
C82 C81 C85 107.1(5) . . ?
C82 C81 C86 126.5(5) . . ?
C85 C81 C86 125.7(6) . . ?
C82 C81 Dy8 74.3(3) . . ?
C85 C81 Dy8 73.6(3) . . ?
C86 C81 Dy8 125.0(4) . . ?
C81 C82 C83 108.9(5) . . ?
C81 C82 C87 125.4(5) . . ?
C83 C82 C87 125.3(5) . . ?
C81 C82 Dy8 74.9(3) . . ?
C83 C82 Dy8 74.3(3) . . ?
C87 C82 Dy8 122.5(4) . . ?
C84 C83 C82 107.3(5) . . ?
C84 C83 C88 126.5(5) . . ?
C82 C83 C88 125.8(6) . . ?
C84 C83 Dy8 73.7(3) . . ?
C82 C83 Dy8 74.4(3) . . ?
C88 C83 Dy8 123.1(4) . . ?
C83 C84 C85 108.2(5) . . ?
C83 C84 C89 124.9(6) . . ?
C85 C84 C89 126.8(6) . . ?
C83 C84 Dy8 75.2(3) . . ?
C85 C84 Dy8 74.6(3) . . ?
C89 C84 Dy8 120.5(4) . . ?
C84 C85 C81 108.5(5) . . ?
C84 C85 C90 126.5(6) . . ?
C81 C85 C90 125.0(6) . . ?
C84 C85 Dy8 74.0(3) . . ?
C81 C85 Dy8 75.2(3) . . ?
C90 C85 Dy8 118.8(4) . . ?
C92 C91 C95 108.4(6) . . ?
C92 C91 C100 126.1(6) . . ?
C95 C91 C100 125.2(6) . . ?
C92 C91 Dy9 74.2(3) . . ?
C95 C91 Dy9 75.3(3) . . ?
C100 C91 Dy9 122.2(4) . . ?
C91 C92 C93 107.9(6) . . ?
C91 C92 C96 125.0(7) . . ?
C93 C92 C96 126.9(7) . . ?
C91 C92 Dy9 74.8(3) . . ?
C93 C92 Dy9 74.1(3) . . ?
C96 C92 Dy9 121.4(4) . . ?
C94 C93 C92 108.3(6) . . ?
C94 C93 C97 126.9(7) . . ?
C92 C93 C97 124.3(7) . . ?
C94 C93 Dy9 75.7(3) . . ?
C92 C93 Dy9 74.6(3) . . ?
C97 C93 Dy9 122.2(4) . . ?
C93 C94 C95 107.7(6) . . ?
C93 C94 C98 126.8(6) . . ?
C95 C94 C98 125.3(6) . . ?
C93 C94 Dy9 73.2(3) . . ?
C95 C94 Dy9 74.7(3) . . ?
C98 C94 Dy9 122.3(4) . . ?
C94 C95 C91 107.8(5) . . ?
C94 C95 C99 125.6(6) . . ?
C91 C95 C99 126.2(6) . . ?
C94 C95 Dy9 74.3(3) . . ?
C91 C95 Dy9 73.5(3) . . ?
C99 C95 Dy9 123.8(4) . . ?
O51 C151 C152 110.7(10) . . ?
O51 C151 K5 46.9(6) . . ?
C152 C151 K5 135.7(10) . . ?
C151 C152 C153 105.0(9) . . ?
C154 C153 C152 103.1(8) . . ?
O51 C154 C153 107.9(8) . . ?
O52 C155 C156 106.8(7) . . ?
C157 C156 C155 106.5(8) . . ?
C156 C157 C158 109.5(7) . . ?
O52 C158 C157 106.4(6) . . ?
C61A O61A C64A 107.0(10) . . ?
C61A O61A K6 122.9(9) . . ?
C64A O61A K6 124.9(11) . . ?
O61A C61A C62A 103.9(11) . . ?
O61A C61A K6 37.5(7) . . ?
C62A C61A K6 118.4(14) . . ?
C61A C62A C63A 103.5(11) . . ?
C64A C63A C62A 103.3(11) . . ?
O61A C64A C63A 108.7(11) . . ?
C61B O61B C64B 103.4(13) . . ?
C61B O61B K6 109.8(14) . . ?
C64B O61B K6 118.3(15) . . ?
O61B C61B C62B 103.4(14) . . ?
C61B C62B C63B 103.9(14) . . ?
C64B C63B C62B 103.8(15) . . ?
O61B C64B C63B 103.3(15) . . ?

_refine_diff_density_max         1.028
_refine_diff_density_min         -2.283
_refine_diff_density_rms         0.141

