# Electronic Supplementary Material (ESI) for Nanoscale Advances.
# This journal is © The Royal Society of Chemistry 2019

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_Ag3Au8
_database_code_depnum_ccdc_archive 'CCDC 1873307'
loop_
_audit_author_name
_audit_author_address
'Jiangwei Zhang'
;Dalian Institute of Chemical Physics, Chinese Academy of Sciences
China
;
_audit_update_record             
;
2018-10-14 deposited with the CCDC.	2019-05-08 downloaded from the CCDC.
;
_audit_creation_date             2018-07-15
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C126 H105 Ag3 Au8 Cl3 P7, C4 H10 O, 2(C H4 O)'
_chemical_formula_sum            'C132 H123 Ag3 Au8 Cl3 O3 P7'
_chemical_formula_weight         3979.78
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/n 1'
_space_group_name_Hall           '-P 2yn'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   17.93474(11)
_cell_length_b                   26.24001(17)
_cell_length_c                   27.00016(18)
_cell_angle_alpha                90
_cell_angle_beta                 91.6646(6)
_cell_angle_gamma                90
_cell_volume                     12701.12(14)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    18415
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      66.601
_cell_measurement_theta_min      3.369
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    22.314
_exptl_absorpt_correction_T_max  0.107
_exptl_absorpt_correction_T_min  0.012
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.081
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             7472
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0554
_diffrn_reflns_av_unetI/netI     0.0596
_diffrn_reflns_Laue_measured_fraction_full 0.963
_diffrn_reflns_Laue_measured_fraction_max 0.963
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       31
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            53435
_diffrn_reflns_point_group_measured_fraction_full 0.963
_diffrn_reflns_point_group_measured_fraction_max 0.963
_diffrn_reflns_theta_full        66.601
_diffrn_reflns_theta_max         66.601
_diffrn_reflns_theta_min         3.369
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 16.0971
_diffrn_measured_fraction_theta_full 0.963
_diffrn_measured_fraction_theta_max 0.963
_diffrn_measurement_device_type  'Xcalibur, Eos, Gemini'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                18415
_reflns_number_total             21589
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         1.102
_refine_diff_density_min         -2.328
_refine_diff_density_rms         0.238
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.010
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1411
_refine_ls_number_reflns         21589
_refine_ls_number_restraints     8
_refine_ls_R_factor_all          0.0526
_refine_ls_R_factor_gt           0.0454
_refine_ls_restrained_S_all      1.011
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0843P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1175
_refine_ls_wR_factor_ref         0.1232
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups, All O(H) groups
2. Restrained distances
 C132-C131 = C130-C129
 1.53 with sigma of 0.02
 O3-C127
 1.45 with sigma of 0.02
 C129-C130 = C130-C129
 1.35 with sigma of 0.04
 O1-C131 = O1-C130
 1.3 with sigma of 0.04
 O3-C127 = O2-C128
 1.4 with sigma of 0.04
 O1-C130 = O1-C131
 1.4 with sigma of 0.04
3. Uiso/Uaniso restraints and constraints
Uanis(O2) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C130) \\sim Ueq: with sigma of 0.1 and sigma for terminal atoms of 0.2
4.a Secondary CH2 refined with riding coordinates:
 C130(H13A,H13B), C131(H13C,H13D)
4.b Aromatic/amide H refined with riding coordinates:
 C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C8(H8), C9(H9), C10(H10), C11(H11),
 C12(H12), C14(H14), C15(H15), C16(H16), C17(H17), C18(H18), C20(H20), C21(H21),
  C22(H22), C23(H23), C24(H24), C26(H26), C27(H27), C28(H28), C29(H29),
 C30(H30), C32(H32), C33(H33), C34(H34), C35(H35), C36(H36), C38(H38), C39(H39),
  C40(H40), C41(H41), C42(H42), C44(H44), C45(H45), C46(H46), C47(H47),
 C48(H48), C50(H50), C51(H51), C52(H52), C53(H53), C54(H54), C56(H56), C57(H57),
  C58(H58), C59(H59), C60(H60), C62(H62), C63(H63), C64(H64), C65(H65),
 C66(H66), C68(H68), C69(H69), C70(H70), C71(H71), C72(H72), C74(H74), C75(H75),
  C76(H76), C77(H77), C78(H78), C80(H80), C81(H81), C82(H82), C83(H83),
 C84(H84), C86(H86), C87(H87), C88(H88), C89(H89), C90(H90), C92(H92), C93(H93),
  C94(H94), C95(H95), C96(H96), C98(H98), C99(H99), C100(H100), C101(H101),
 C102(H102), C104(H104), C105(H105), C106(H106), C107(H107), C108(H108),
 C110(H110), C111(H111), C112(H112), C113(H113), C114(H114), C116(H116),
 C117(H117), C118(H118), C119(H119), C120(H120), C122(H122), C123(H123),
 C124(H124), C125(H125), C126(H126)
4.c Idealised Me refined as rotating group:
 C129(H12A,H12B,H12C), C132(H13E,H13F,H13G), C128(H12D,H12E,H12F), C127(H12G,
 H12H,H12I)
4.d Idealised tetrahedral OH refined as rotating group:
 O2(H2A), O3(H3A)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.55346(2) 0.24821(2) 0.55274(2) 0.02949(8) Uani 1 1 d . . . . .
Au2 Au 0.54486(2) 0.33115(2) 0.62452(2) 0.02929(8) Uani 1 1 d . . . . .
Au3 Au 0.56780(2) 0.16851(2) 0.62966(2) 0.02904(8) Uani 1 1 d . . . . .
Au4 Au 0.39214(2) 0.23718(2) 0.54324(2) 0.03126(9) Uani 1 1 d . . . . .
Au5 Au 0.46855(2) 0.24413(2) 0.62929(2) 0.02261(8) Uani 1 1 d . . . . .
Au6 Au 0.43995(2) 0.18701(2) 0.70739(2) 0.02637(8) Uani 1 1 d . . . . .
Au7 Au 0.44131(2) 0.30049(2) 0.70841(2) 0.02787(8) Uani 1 1 d . . . . .
Au8 Au 0.32320(2) 0.24203(2) 0.64706(2) 0.02760(8) Uani 1 1 d . . . . .
Ag1 Ag 0.58553(3) 0.25198(2) 0.69695(2) 0.03154(12) Uani 1 1 d . . . . .
Ag2 Ag 0.38856(3) 0.33020(2) 0.60303(2) 0.03273(12) Uani 1 1 d . . . . .
Ag3 Ag 0.40828(3) 0.15013(2) 0.60653(2) 0.03156(12) Uani 1 1 d . . . . .
Cl1 Cl 0.68738(12) 0.25215(8) 0.75784(9) 0.0491(5) Uani 1 1 d . . . . .
Cl2 Cl 0.31768(11) 0.40674(7) 0.58643(7) 0.0443(4) Uani 1 1 d . . . . .
Cl3 Cl 0.34118(12) 0.07383(8) 0.58169(8) 0.0480(5) Uani 1 1 d . . . . .
P1 P 0.62304(11) 0.24825(7) 0.48369(7) 0.0294(4) Uani 1 1 d . . . . .
P2 P 0.65348(10) 0.10363(7) 0.63527(7) 0.0307(4) Uani 1 1 d . . . . .
P3 P 0.31996(11) 0.22908(9) 0.47238(7) 0.0374(4) Uani 1 1 d . . . . .
P4 P 0.60544(11) 0.40797(7) 0.62089(7) 0.0330(4) Uani 1 1 d . . . . .
P5 P 0.43049(10) 0.35431(7) 0.77459(6) 0.0308(4) Uani 1 1 d . . . . .
P6 P 0.19686(10) 0.24403(7) 0.65810(7) 0.0289(4) Uani 1 1 d . . . . .
P7 P 0.42605(10) 0.12857(7) 0.76959(6) 0.0276(4) Uani 1 1 d . . . . .
C1 C 0.7096(4) 0.2834(3) 0.4910(3) 0.0339(16) Uani 1 1 d . . . . .
C2 C 0.7460(5) 0.2841(3) 0.5378(3) 0.046(2) Uani 1 1 d . . . . .
H2 H 0.726796 0.265178 0.563637 0.055 Uiso 1 1 calc R . . . .
C3 C 0.8094(5) 0.3125(4) 0.5458(4) 0.056(2) Uani 1 1 d . . . . .
H3 H 0.833678 0.311807 0.576694 0.067 Uiso 1 1 calc R . . . .
C4 C 0.8376(5) 0.3419(3) 0.5085(4) 0.058(2) Uani 1 1 d . . . . .
H4 H 0.879971 0.361646 0.514477 0.069 Uiso 1 1 calc R . . . .
C5 C 0.8033(5) 0.3422(3) 0.4627(4) 0.051(2) Uani 1 1 d . . . . .
H5 H 0.822441 0.362312 0.437727 0.061 Uiso 1 1 calc R . . . .
C6 C 0.7397(4) 0.3127(3) 0.4530(3) 0.0408(18) Uani 1 1 d . . . . .
H6 H 0.717479 0.312502 0.421482 0.049 Uiso 1 1 calc R . . . .
C7 C 0.6473(4) 0.1843(3) 0.4653(3) 0.0319(15) Uani 1 1 d . . . . .
C8 C 0.7079(4) 0.1729(3) 0.4358(3) 0.0389(18) Uani 1 1 d . . . . .
H8 H 0.737792 0.199223 0.424643 0.047 Uiso 1 1 calc R . . . .
C9 C 0.7239(5) 0.1234(3) 0.4231(3) 0.052(2) Uani 1 1 d . . . . .
H9 H 0.764184 0.116484 0.403155 0.062 Uiso 1 1 calc R . . . .
C10 C 0.6809(6) 0.0844(4) 0.4396(3) 0.056(2) Uani 1 1 d . . . . .
H10 H 0.691535 0.051077 0.430368 0.067 Uiso 1 1 calc R . . . .
C11 C 0.6221(5) 0.0939(3) 0.4697(3) 0.051(2) Uani 1 1 d . . . . .
H11 H 0.593684 0.067184 0.481740 0.062 Uiso 1 1 calc R . . . .
C12 C 0.6058(5) 0.1435(3) 0.4817(3) 0.0425(19) Uani 1 1 d . . . . .
H12 H 0.565369 0.149950 0.501577 0.051 Uiso 1 1 calc R . . . .
C13 C 0.5745(4) 0.2762(3) 0.4296(3) 0.0336(16) Uani 1 1 d . . . . .
C14 C 0.5254(5) 0.3163(4) 0.4378(3) 0.047(2) Uani 1 1 d . . . . .
H14 H 0.519775 0.328979 0.469676 0.056 Uiso 1 1 calc R . . . .
C15 C 0.4855(5) 0.3371(4) 0.3986(4) 0.057(2) Uani 1 1 d . . . . .
H15 H 0.452801 0.363903 0.404067 0.068 Uiso 1 1 calc R . . . .
C16 C 0.4933(5) 0.3188(4) 0.3517(3) 0.051(2) Uani 1 1 d . . . . .
H16 H 0.465205 0.332647 0.325479 0.062 Uiso 1 1 calc R . . . .
C17 C 0.5417(5) 0.2808(4) 0.3433(3) 0.054(2) Uani 1 1 d . . . . .
H17 H 0.547897 0.269454 0.311052 0.065 Uiso 1 1 calc R . . . .
C18 C 0.5826(5) 0.2582(4) 0.3821(3) 0.046(2) Uani 1 1 d . . . . .
H18 H 0.614947 0.231359 0.375948 0.055 Uiso 1 1 calc R . . . .
C19 C 0.7482(4) 0.1188(3) 0.6176(3) 0.0374(17) Uani 1 1 d . . . . .
C20 C 0.7580(5) 0.1484(4) 0.5754(3) 0.049(2) Uani 1 1 d . . . . .
H20 H 0.716347 0.161868 0.558818 0.059 Uiso 1 1 calc R . . . .
C21 C 0.8285(5) 0.1583(4) 0.5576(3) 0.057(2) Uani 1 1 d . . . . .
H21 H 0.834088 0.178320 0.529527 0.068 Uiso 1 1 calc R . . . .
C22 C 0.8888(5) 0.1383(4) 0.5818(4) 0.064(3) Uani 1 1 d . . . . .
H22 H 0.935996 0.144275 0.569685 0.077 Uiso 1 1 calc R . . . .
C23 C 0.8819(5) 0.1091(4) 0.6242(4) 0.069(3) Uani 1 1 d . . . . .
H23 H 0.924326 0.095825 0.640147 0.083 Uiso 1 1 calc R . . . .
C24 C 0.8126(5) 0.0996(4) 0.6428(4) 0.056(2) Uani 1 1 d . . . . .
H24 H 0.808047 0.080799 0.671788 0.067 Uiso 1 1 calc R . . . .
C25 C 0.6285(4) 0.0492(3) 0.5966(3) 0.0359(16) Uani 1 1 d . . . . .
C26 C 0.6802(5) 0.0191(3) 0.5715(3) 0.050(2) Uani 1 1 d . . . . .
H26 H 0.730744 0.027097 0.573719 0.060 Uiso 1 1 calc R . . . .
C27 C 0.6568(6) -0.0218(4) 0.5439(3) 0.058(2) Uani 1 1 d . . . . .
H27 H 0.691419 -0.041594 0.527607 0.070 Uiso 1 1 calc R . . . .
C28 C 0.5822(6) -0.0338(4) 0.5402(4) 0.066(3) Uani 1 1 d . . . . .
H28 H 0.566557 -0.061920 0.521771 0.080 Uiso 1 1 calc R . . . .
C29 C 0.5300(6) -0.0038(4) 0.5641(4) 0.066(3) Uani 1 1 d . . . . .
H29 H 0.479501 -0.011723 0.561277 0.079 Uiso 1 1 calc R . . . .
C30 C 0.5534(5) 0.0374(3) 0.5919(3) 0.0417(18) Uani 1 1 d . . . . .
H30 H 0.518546 0.057443 0.607716 0.050 Uiso 1 1 calc R . . . .
C31 C 0.6653(4) 0.0769(3) 0.6969(3) 0.0374(17) Uani 1 1 d . . . . .
C32 C 0.6610(4) 0.1082(3) 0.7378(3) 0.0397(17) Uani 1 1 d . . . . .
H32 H 0.650371 0.142682 0.733592 0.048 Uiso 1 1 calc R . . . .
C33 C 0.6722(5) 0.0889(4) 0.7849(3) 0.049(2) Uani 1 1 d . . . . .
H33 H 0.668665 0.110222 0.812263 0.058 Uiso 1 1 calc R . . . .
C34 C 0.6890(5) 0.0375(4) 0.7916(3) 0.052(2) Uani 1 1 d . . . . .
H34 H 0.697394 0.024591 0.823379 0.062 Uiso 1 1 calc R . . . .
C35 C 0.6930(5) 0.0061(4) 0.7515(3) 0.055(2) Uani 1 1 d . . . . .
H35 H 0.704032 -0.028238 0.755874 0.066 Uiso 1 1 calc R . . . .
C36 C 0.6806(5) 0.0254(3) 0.7047(3) 0.0457(19) Uani 1 1 d . . . . .
H36 H 0.682473 0.003610 0.677650 0.055 Uiso 1 1 calc R . . . .
C37 C 0.3053(4) 0.2893(4) 0.4406(3) 0.0425(19) Uani 1 1 d . . . . .
C38 C 0.3004(5) 0.3324(3) 0.4699(3) 0.0443(19) Uani 1 1 d . . . . .
H38 H 0.303692 0.329403 0.504179 0.053 Uiso 1 1 calc R . . . .
C39 C 0.2908(6) 0.3797(4) 0.4485(4) 0.060(2) Uani 1 1 d . . . . .
H39 H 0.286781 0.408467 0.468400 0.072 Uiso 1 1 calc R . . . .
C40 C 0.2870(5) 0.3844(4) 0.3976(4) 0.065(3) Uani 1 1 d . . . . .
H40 H 0.281358 0.416390 0.383222 0.077 Uiso 1 1 calc R . . . .
C41 C 0.2917(6) 0.3419(4) 0.3680(4) 0.062(3) Uani 1 1 d . . . . .
H41 H 0.288743 0.345059 0.333659 0.074 Uiso 1 1 calc R . . . .
C42 C 0.3008(5) 0.2944(4) 0.3896(3) 0.058(3) Uani 1 1 d . . . . .
H42 H 0.303974 0.265665 0.369684 0.070 Uiso 1 1 calc R . . . .
C43 C 0.2280(4) 0.2042(3) 0.4827(3) 0.0385(17) Uani 1 1 d . . . . .
C44 C 0.1664(5) 0.2185(4) 0.4546(4) 0.064(3) Uani 1 1 d . . . . .
H44 H 0.170671 0.244477 0.431414 0.077 Uiso 1 1 calc R . . . .
C45 C 0.0986(6) 0.1952(6) 0.4599(5) 0.087(4) Uani 1 1 d . . . . .
H45 H 0.057115 0.206321 0.441442 0.105 Uiso 1 1 calc R . . . .
C46 C 0.0920(7) 0.1559(5) 0.4922(5) 0.084(4) Uani 1 1 d . . . . .
H46 H 0.046623 0.138898 0.493874 0.100 Uiso 1 1 calc R . . . .
C47 C 0.1510(7) 0.1404(5) 0.5224(5) 0.083(4) Uani 1 1 d . . . . .
H47 H 0.145284 0.114883 0.545866 0.100 Uiso 1 1 calc R . . . .
C48 C 0.2202(5) 0.1647(4) 0.5167(4) 0.059(2) Uani 1 1 d . . . . .
H48 H 0.261322 0.154188 0.535844 0.071 Uiso 1 1 calc R . . . .
C49 C 0.3544(5) 0.1861(4) 0.4256(3) 0.049(2) Uani 1 1 d . . . . .
C50 C 0.4290(6) 0.1822(5) 0.4193(5) 0.087(4) Uani 1 1 d . . . . .
H50 H 0.462280 0.199591 0.440306 0.104 Uiso 1 1 calc R . . . .
C51 C 0.4555(8) 0.1519(6) 0.3810(6) 0.114(6) Uani 1 1 d . . . . .
H51 H 0.506670 0.149520 0.376716 0.137 Uiso 1 1 calc R . . . .
C52 C 0.4095(7) 0.1264(6) 0.3504(5) 0.093(4) Uani 1 1 d . . . . .
H52 H 0.427881 0.109328 0.323184 0.112 Uiso 1 1 calc R . . . .
C53 C 0.3371(8) 0.1256(7) 0.3592(6) 0.137(8) Uani 1 1 d . . . . .
H53 H 0.305597 0.104458 0.340478 0.164 Uiso 1 1 calc R . . . .
C54 C 0.3077(7) 0.1563(7) 0.3964(6) 0.128(7) Uani 1 1 d . . . . .
H54 H 0.256649 0.156479 0.401426 0.153 Uiso 1 1 calc R . . . .
C55 C 0.7017(4) 0.4029(3) 0.6428(3) 0.0394(18) Uani 1 1 d . . . . .
C56 C 0.7603(5) 0.4260(4) 0.6190(4) 0.056(2) Uani 1 1 d . . . . .
H56 H 0.750862 0.446404 0.591361 0.067 Uiso 1 1 calc R . . . .
C57 C 0.8338(6) 0.4186(5) 0.6365(4) 0.070(3) Uani 1 1 d . . . . .
H57 H 0.873151 0.434206 0.620767 0.084 Uiso 1 1 calc R . . . .
C58 C 0.8470(6) 0.3885(4) 0.6765(5) 0.068(3) Uani 1 1 d . . . . .
H58 H 0.895831 0.383854 0.688133 0.082 Uiso 1 1 calc R . . . .
C59 C 0.7907(6) 0.3650(4) 0.6999(4) 0.068(3) Uani 1 1 d . . . . .
H59 H 0.801325 0.344233 0.727169 0.081 Uiso 1 1 calc R . . . .
C60 C 0.7174(5) 0.3718(3) 0.6835(3) 0.051(2) Uani 1 1 d . . . . .
H60 H 0.678833 0.355551 0.699581 0.062 Uiso 1 1 calc R . . . .
C61 C 0.6098(4) 0.4363(3) 0.5594(3) 0.0365(17) Uani 1 1 d . . . . .
C62 C 0.5955(6) 0.4874(3) 0.5497(3) 0.054(2) Uani 1 1 d . . . . .
H62 H 0.582772 0.509252 0.575214 0.064 Uiso 1 1 calc R . . . .
C63 C 0.6002(6) 0.5056(4) 0.5018(3) 0.061(3) Uani 1 1 d . . . . .
H63 H 0.590906 0.539889 0.495525 0.073 Uiso 1 1 calc R . . . .
C64 C 0.6182(5) 0.4747(3) 0.4638(3) 0.050(2) Uani 1 1 d . . . . .
H64 H 0.621166 0.487555 0.431804 0.060 Uiso 1 1 calc R . . . .
C65 C 0.6317(6) 0.4245(4) 0.4730(3) 0.059(3) Uani 1 1 d . . . . .
H65 H 0.644399 0.403215 0.447031 0.070 Uiso 1 1 calc R . . . .
C66 C 0.6271(5) 0.4044(3) 0.5201(3) 0.052(2) Uani 1 1 d . . . . .
H66 H 0.635423 0.369861 0.525496 0.062 Uiso 1 1 calc R . . . .
C67 C 0.5652(4) 0.4595(3) 0.6562(3) 0.0385(17) Uani 1 1 d . . . . .
C68 C 0.6071(5) 0.4986(3) 0.6765(3) 0.050(2) Uani 1 1 d . . . . .
H68 H 0.658892 0.496507 0.677224 0.060 Uiso 1 1 calc R . . . .
C69 C 0.5729(6) 0.5408(3) 0.6956(3) 0.060(3) Uani 1 1 d . . . . .
H69 H 0.601606 0.566902 0.709595 0.072 Uiso 1 1 calc R . . . .
C70 C 0.4957(7) 0.5446(4) 0.6941(4) 0.065(3) Uani 1 1 d . . . . .
H70 H 0.472684 0.574069 0.705254 0.078 Uiso 1 1 calc R . . . .
C71 C 0.4535(6) 0.5050(4) 0.6761(3) 0.054(2) Uani 1 1 d . . . . .
H71 H 0.401765 0.506700 0.676899 0.064 Uiso 1 1 calc R . . . .
C72 C 0.4871(5) 0.4628(3) 0.6568(3) 0.0427(19) Uani 1 1 d . . . . .
H72 H 0.458060 0.436217 0.644062 0.051 Uiso 1 1 calc R . . . .
C73 C 0.5152(5) 0.3903(3) 0.7885(3) 0.0421(19) Uani 1 1 d . . . . .
C74 C 0.5796(5) 0.3619(4) 0.7980(4) 0.061(3) Uani 1 1 d . . . . .
H74 H 0.578090 0.326553 0.796555 0.074 Uiso 1 1 calc R . . . .
C75 C 0.6447(6) 0.3862(6) 0.8093(6) 0.099(5) Uani 1 1 d . . . . .
H75 H 0.688132 0.367499 0.814967 0.118 Uiso 1 1 calc R . . . .
C76 C 0.6462(7) 0.4404(6) 0.8126(5) 0.092(4) Uani 1 1 d . . . . .
H76 H 0.689829 0.457197 0.822580 0.111 Uiso 1 1 calc R . . . .
C77 C 0.5835(6) 0.4673(5) 0.8011(4) 0.071(3) Uani 1 1 d . . . . .
H77 H 0.585472 0.502700 0.800403 0.086 Uiso 1 1 calc R . . . .
C78 C 0.5174(6) 0.4431(3) 0.7905(3) 0.053(2) Uani 1 1 d . . . . .
H78 H 0.474160 0.461973 0.784595 0.064 Uiso 1 1 calc R . . . .
C79 C 0.4161(4) 0.3221(3) 0.8338(3) 0.0323(16) Uani 1 1 d . . . . .
C80 C 0.4280(4) 0.3460(3) 0.8788(3) 0.0394(17) Uani 1 1 d . . . . .
H80 H 0.445294 0.379433 0.879713 0.047 Uiso 1 1 calc R . . . .
C81 C 0.4144(4) 0.3205(4) 0.9228(3) 0.0426(19) Uani 1 1 d . . . . .
H81 H 0.421710 0.337264 0.952961 0.051 Uiso 1 1 calc R . . . .
C82 C 0.3904(5) 0.2710(4) 0.9222(3) 0.045(2) Uani 1 1 d . . . . .
H82 H 0.380848 0.254240 0.951652 0.054 Uiso 1 1 calc R . . . .
C83 C 0.3803(5) 0.2462(3) 0.8774(3) 0.045(2) Uani 1 1 d . . . . .
H83 H 0.365223 0.212338 0.876801 0.054 Uiso 1 1 calc R . . . .
C84 C 0.3927(4) 0.2716(3) 0.8328(3) 0.0389(17) Uani 1 1 d . . . . .
H84 H 0.385287 0.254838 0.802738 0.047 Uiso 1 1 calc R . . . .
C85 C 0.3558(4) 0.4004(3) 0.7680(3) 0.0386(18) Uani 1 1 d . . . . .
C86 C 0.3273(5) 0.4288(3) 0.8078(3) 0.049(2) Uani 1 1 d . . . . .
H86 H 0.348426 0.425372 0.839456 0.059 Uiso 1 1 calc R . . . .
C87 C 0.2688(6) 0.4612(3) 0.7995(4) 0.058(3) Uani 1 1 d . . . . .
H87 H 0.250344 0.479523 0.825990 0.070 Uiso 1 1 calc R . . . .
C88 C 0.2365(6) 0.4676(5) 0.7532(4) 0.079(4) Uani 1 1 d . . . . .
H88 H 0.196520 0.489850 0.748486 0.095 Uiso 1 1 calc R . . . .
C89 C 0.2639(6) 0.4405(5) 0.7134(4) 0.078(4) Uani 1 1 d . . . . .
H89 H 0.243135 0.444817 0.681731 0.094 Uiso 1 1 calc R . . . .
C90 C 0.3226(5) 0.4069(4) 0.7216(3) 0.052(2) Uani 1 1 d . . . . .
H90 H 0.340092 0.388220 0.695050 0.063 Uiso 1 1 calc R . . . .
C91 C 0.1708(4) 0.2845(3) 0.7098(3) 0.0342(16) Uani 1 1 d . . . . .
C92 C 0.2202(4) 0.2914(3) 0.7486(3) 0.0361(16) Uani 1 1 d . . . . .
H92 H 0.267077 0.276439 0.747243 0.043 Uiso 1 1 calc R . . . .
C93 C 0.2034(5) 0.3195(3) 0.7892(3) 0.0416(18) Uani 1 1 d . . . . .
H93 H 0.237619 0.322534 0.815536 0.050 Uiso 1 1 calc R . . . .
C94 C 0.1345(6) 0.3435(4) 0.7908(3) 0.053(2) Uani 1 1 d . . . . .
H94 H 0.122714 0.363633 0.817784 0.063 Uiso 1 1 calc R . . . .
C95 C 0.0840(5) 0.3371(4) 0.7521(4) 0.061(3) Uani 1 1 d . . . . .
H95 H 0.037467 0.352690 0.753457 0.074 Uiso 1 1 calc R . . . .
C96 C 0.1007(5) 0.3082(4) 0.7115(3) 0.053(2) Uani 1 1 d . . . . .
H96 H 0.066091 0.304436 0.685391 0.064 Uiso 1 1 calc R . . . .
C97 C 0.1400(4) 0.2689(3) 0.6070(3) 0.0359(16) Uani 1 1 d . . . . .
C98 C 0.1661(5) 0.3104(3) 0.5809(3) 0.0452(19) Uani 1 1 d . . . . .
H98 H 0.213598 0.323253 0.587512 0.054 Uiso 1 1 calc R . . . .
C99 C 0.1200(6) 0.3323(4) 0.5445(3) 0.062(3) Uani 1 1 d . . . . .
H99 H 0.136824 0.361098 0.528137 0.074 Uiso 1 1 calc R . . . .
C100 C 0.0525(6) 0.3138(5) 0.5321(4) 0.071(3) Uani 1 1 d . . . . .
H100 H 0.023810 0.329432 0.507245 0.085 Uiso 1 1 calc R . . . .
C101 C 0.0256(6) 0.2718(5) 0.5559(4) 0.065(3) Uani 1 1 d . . . . .
H101 H -0.021103 0.258711 0.547132 0.078 Uiso 1 1 calc R . . . .
C102 C 0.0694(5) 0.2489(4) 0.5936(4) 0.054(2) Uani 1 1 d . . . . .
H102 H 0.051674 0.220308 0.609771 0.065 Uiso 1 1 calc R . . . .
C103 C 0.1577(4) 0.1823(3) 0.6726(3) 0.0344(16) Uani 1 1 d . . . . .
C104 C 0.0892(5) 0.1768(3) 0.6963(3) 0.046(2) Uani 1 1 d . . . . .
H104 H 0.062535 0.205364 0.705766 0.055 Uiso 1 1 calc R . . . .
C105 C 0.0620(6) 0.1284(5) 0.7054(4) 0.067(3) Uani 1 1 d . . . . .
H105 H 0.018012 0.124634 0.722397 0.081 Uiso 1 1 calc R . . . .
C106 C 0.0987(7) 0.0867(4) 0.6898(5) 0.081(4) Uani 1 1 d . . . . .
H106 H 0.078885 0.054363 0.694629 0.098 Uiso 1 1 calc R . . . .
C107 C 0.1655(7) 0.0922(4) 0.6667(4) 0.071(3) Uani 1 1 d . . . . .
H107 H 0.191157 0.063276 0.656906 0.085 Uiso 1 1 calc R . . . .
C108 C 0.1948(5) 0.1389(3) 0.6579(4) 0.053(2) Uani 1 1 d . . . . .
H108 H 0.239827 0.141685 0.641899 0.063 Uiso 1 1 calc R . . . .
C109 C 0.3323(4) 0.1225(3) 0.7940(2) 0.0320(15) Uani 1 1 d . . . . .
C110 C 0.2813(4) 0.1615(3) 0.7851(3) 0.0370(17) Uani 1 1 d . . . . .
H110 H 0.294790 0.189168 0.765737 0.044 Uiso 1 1 calc R . . . .
C111 C 0.2112(5) 0.1599(4) 0.8045(3) 0.047(2) Uani 1 1 d . . . . .
H111 H 0.177979 0.186552 0.798531 0.057 Uiso 1 1 calc R . . . .
C112 C 0.1902(4) 0.1187(4) 0.8328(3) 0.048(2) Uani 1 1 d . . . . .
H112 H 0.143041 0.117475 0.846222 0.057 Uiso 1 1 calc R . . . .
C113 C 0.2395(5) 0.0799(4) 0.8407(3) 0.051(2) Uani 1 1 d . . . . .
H113 H 0.225258 0.051950 0.859371 0.061 Uiso 1 1 calc R . . . .
C114 C 0.3103(5) 0.0809(3) 0.8215(3) 0.045(2) Uani 1 1 d . . . . .
H114 H 0.342850 0.053792 0.827183 0.054 Uiso 1 1 calc R . . . .
C115 C 0.4447(4) 0.0653(3) 0.7468(3) 0.0359(17) Uani 1 1 d . . . . .
C116 C 0.4095(5) 0.0513(3) 0.7029(3) 0.046(2) Uani 1 1 d . . . . .
H116 H 0.377883 0.074556 0.686910 0.055 Uiso 1 1 calc R . . . .
C117 C 0.4196(6) 0.0043(3) 0.6818(4) 0.057(2) Uani 1 1 d . . . . .
H117 H 0.395140 -0.004141 0.652035 0.068 Uiso 1 1 calc R . . . .
C118 C 0.4655(6) -0.0296(4) 0.7049(5) 0.069(3) Uani 1 1 d . . . . .
H118 H 0.471961 -0.061747 0.691177 0.083 Uiso 1 1 calc R . . . .
C119 C 0.5021(6) -0.0173(4) 0.7479(5) 0.072(3) Uani 1 1 d . . . . .
H119 H 0.534289 -0.040856 0.762850 0.086 Uiso 1 1 calc R . . . .
C120 C 0.4923(5) 0.0299(3) 0.7697(4) 0.052(2) Uani 1 1 d . . . . .
H120 H 0.517259 0.037908 0.799354 0.063 Uiso 1 1 calc R . . . .
C121 C 0.4865(4) 0.1402(3) 0.8240(2) 0.0321(15) Uani 1 1 d . . . . .
C122 C 0.5389(4) 0.1780(3) 0.8213(3) 0.0364(17) Uani 1 1 d . . . . .
H122 H 0.541425 0.197229 0.792461 0.044 Uiso 1 1 calc R . . . .
C123 C 0.5882(5) 0.1882(3) 0.8604(3) 0.046(2) Uani 1 1 d . . . . .
H123 H 0.623224 0.214083 0.857968 0.055 Uiso 1 1 calc R . . . .
C124 C 0.5847(6) 0.1598(4) 0.9025(3) 0.063(3) Uani 1 1 d . . . . .
H124 H 0.617960 0.166113 0.928858 0.075 Uiso 1 1 calc R . . . .
C125 C 0.5326(6) 0.1222(5) 0.9061(3) 0.070(3) Uani 1 1 d . . . . .
H125 H 0.530556 0.103312 0.935177 0.083 Uiso 1 1 calc R . . . .
C126 C 0.4823(5) 0.1115(4) 0.8672(3) 0.056(2) Uani 1 1 d . . . . .
H126 H 0.446913 0.085874 0.869955 0.067 Uiso 1 1 calc R . . . .
O1 O 0.125(2) 0.4736(13) 0.5838(16) 0.56(4) Uani 1 1 d D . . . .
C129 C 0.0404(9) 0.4315(9) 0.6248(7) 0.154(8) Uani 1 1 d D . . . .
H12A H 0.032705 0.408717 0.597254 0.231 Uiso 1 1 calc GR . . . .
H12B H 0.007907 0.460359 0.620882 0.231 Uiso 1 1 calc GR . . . .
H12C H 0.029729 0.414042 0.654993 0.231 Uiso 1 1 calc GR . . . .
C130 C 0.1160(12) 0.4483(18) 0.6265(14) 0.39(3) Uani 1 1 d D U . . .
H13A H 0.125288 0.470555 0.654652 0.467 Uiso 1 1 calc R . . . .
H13B H 0.149817 0.419510 0.628894 0.467 Uiso 1 1 calc R . . . .
C131 C 0.140(5) 0.505(2) 0.5453(11) 0.58(7) Uani 1 1 d D . . . .
H13C H 0.182927 0.523790 0.558038 0.702 Uiso 1 1 calc R . . . .
H13D H 0.099038 0.528801 0.545500 0.702 Uiso 1 1 calc R . . . .
C132 C 0.155(2) 0.5007(12) 0.4920(11) 0.273(19) Uani 1 1 d D . . . .
H13E H 0.110016 0.505742 0.472937 0.410 Uiso 1 1 calc GR . . . .
H13F H 0.175096 0.467464 0.485151 0.410 Uiso 1 1 calc GR . . . .
H13G H 0.191144 0.526148 0.483237 0.410 Uiso 1 1 calc GR . . . .
O2 O 0.047(3) -0.0216(15) 0.5621(14) 0.413(18) Uani 1 1 d D U . . .
H2A H 0.044857 -0.052201 0.556151 0.619 Uiso 1 1 calc GR . . . .
C128 C 0.101(2) 0.0003(8) 0.534(2) 0.44(4) Uani 1 1 d D . . . .
H12D H 0.133576 0.020438 0.554510 0.654 Uiso 1 1 calc GR . . . .
H12E H 0.077215 0.021719 0.509047 0.654 Uiso 1 1 calc GR . . . .
H12F H 0.128716 -0.025883 0.517889 0.654 Uiso 1 1 calc GR . . . .
O3 O 0.8486(8) 0.1917(6) 0.7481(5) 0.153(5) Uani 1 1 d D . . . .
H3A H 0.804003 0.189861 0.740871 0.230 Uiso 1 1 calc GR . . . .
C127 C 0.8826(10) 0.2333(7) 0.7196(14) 0.30(3) Uani 1 1 d D . . . .
H12G H 0.845151 0.258029 0.710724 0.445 Uiso 1 1 calc GR . . . .
H12H H 0.903563 0.219598 0.690125 0.445 Uiso 1 1 calc GR . . . .
H12I H 0.921265 0.249256 0.739479 0.445 Uiso 1 1 calc GR . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 Au2 2.9214(4) . ?
Au1 Au3 2.9532(4) . ?
Au1 Au4 2.9115(4) . ?
Au1 Au5 2.6048(4) . ?
Au1 P1 2.2735(18) . ?
Au2 Au5 2.6672(4) . ?
Au2 Au7 3.0774(4) . ?
Au2 Ag1 2.9306(6) . ?
Au2 Ag2 2.8463(6) . ?
Au2 P4 2.2933(18) . ?
Au3 Au5 2.6655(4) . ?
Au3 Au6 3.1903(4) . ?
Au3 Ag1 2.8576(6) . ?
Au3 Ag3 2.9503(6) . ?
Au3 P2 2.2954(18) . ?
Au4 Au5 2.6692(4) . ?
Au4 Au8 3.0991(4) . ?
Au4 Ag2 2.9282(6) . ?
Au4 Ag3 2.8625(6) . ?
Au4 P3 2.289(2) . ?
Au5 Au6 2.6494(4) . ?
Au5 Au7 2.6550(4) . ?
Au5 Au8 2.6650(4) . ?
Au5 Ag1 2.7492(6) . ?
Au5 Ag2 2.7573(6) . ?
Au5 Ag3 2.7554(6) . ?
Au6 Au7 2.9779(4) . ?
Au6 Au8 2.9873(4) . ?
Au6 Ag1 3.1379(6) . ?
Au6 Ag3 2.9301(6) . ?
Au6 P7 2.2931(17) . ?
Au7 Au8 3.0628(4) . ?
Au7 Ag1 2.9073(6) . ?
Au7 Ag2 3.0727(6) . ?
Au7 P5 2.2903(17) . ?
Au8 Ag2 2.8674(6) . ?
Au8 Ag3 3.0722(6) . ?
Au8 P6 2.2944(18) . ?
Ag1 Cl1 2.422(2) . ?
Ag2 Cl2 2.4119(18) . ?
Ag3 Cl3 2.420(2) . ?
P1 C1 1.811(8) . ?
P1 C7 1.808(7) . ?
P1 C13 1.831(8) . ?
P2 C19 1.821(8) . ?
P2 C25 1.818(8) . ?
P2 C31 1.813(8) . ?
P3 C37 1.815(9) . ?
P3 C43 1.802(8) . ?
P3 C49 1.816(9) . ?
P4 C55 1.813(8) . ?
P4 C61 1.822(8) . ?
P4 C67 1.816(8) . ?
P5 C73 1.819(8) . ?
P5 C79 1.833(7) . ?
P5 C85 1.810(8) . ?
P6 C91 1.826(8) . ?
P6 C97 1.813(8) . ?
P6 C103 1.812(8) . ?
P7 C109 1.830(7) . ?
P7 C115 1.806(8) . ?
P7 C121 1.827(7) . ?
C1 C2 1.406(11) . ?
C1 C6 1.402(10) . ?
C2 H2 0.9300 . ?
C2 C3 1.372(12) . ?
C3 H3 0.9300 . ?
C3 C4 1.377(14) . ?
C4 H4 0.9300 . ?
C4 C5 1.363(14) . ?
C5 H5 0.9300 . ?
C5 C6 1.397(11) . ?
C6 H6 0.9300 . ?
C7 C8 1.396(10) . ?
C7 C12 1.383(10) . ?
C8 H8 0.9300 . ?
C8 C9 1.378(12) . ?
C9 H9 0.9300 . ?
C9 C10 1.364(13) . ?
C10 H10 0.9300 . ?
C10 C11 1.374(13) . ?
C11 H11 0.9300 . ?
C11 C12 1.376(12) . ?
C12 H12 0.9300 . ?
C13 C14 1.395(11) . ?
C13 C18 1.380(11) . ?
C14 H14 0.9300 . ?
C14 C15 1.374(13) . ?
C15 H15 0.9300 . ?
C15 C16 1.367(13) . ?
C16 H16 0.9300 . ?
C16 C17 1.344(13) . ?
C17 H17 0.9300 . ?
C17 C18 1.394(12) . ?
C18 H18 0.9300 . ?
C19 C20 1.393(11) . ?
C19 C24 1.417(11) . ?
C20 H20 0.9300 . ?
C20 C21 1.390(11) . ?
C21 H21 0.9300 . ?
C21 C22 1.353(14) . ?
C22 H22 0.9300 . ?
C22 C23 1.386(15) . ?
C23 H23 0.9300 . ?
C23 C24 1.378(13) . ?
C24 H24 0.9300 . ?
C25 C26 1.407(10) . ?
C25 C30 1.385(11) . ?
C26 H26 0.9300 . ?
C26 C27 1.365(13) . ?
C27 H27 0.9300 . ?
C27 C28 1.375(14) . ?
C28 H28 0.9300 . ?
C28 C29 1.395(15) . ?
C29 H29 0.9300 . ?
C29 C30 1.375(12) . ?
C30 H30 0.9300 . ?
C31 C32 1.381(10) . ?
C31 C36 1.394(11) . ?
C32 H32 0.9300 . ?
C32 C33 1.378(11) . ?
C33 H33 0.9300 . ?
C33 C34 1.393(13) . ?
C34 H34 0.9300 . ?
C34 C35 1.363(13) . ?
C35 H35 0.9300 . ?
C35 C36 1.373(12) . ?
C36 H36 0.9300 . ?
C37 C38 1.384(12) . ?
C37 C42 1.382(11) . ?
C38 H38 0.9300 . ?
C38 C39 1.377(13) . ?
C39 H39 0.9300 . ?
C39 C40 1.380(14) . ?
C40 H40 0.9300 . ?
C40 C41 1.376(15) . ?
C41 H41 0.9300 . ?
C41 C42 1.383(15) . ?
C42 H42 0.9300 . ?
C43 C44 1.375(12) . ?
C43 C48 1.396(12) . ?
C44 H44 0.9300 . ?
C44 C45 1.372(14) . ?
C45 H45 0.9300 . ?
C45 C46 1.357(17) . ?
C46 H46 0.9300 . ?
C46 C47 1.379(17) . ?
C47 H47 0.9300 . ?
C47 C48 1.407(13) . ?
C48 H48 0.9300 . ?
C49 C50 1.357(13) . ?
C49 C54 1.376(16) . ?
C50 H50 0.9300 . ?
C50 C51 1.400(16) . ?
C51 H51 0.9300 . ?
C51 C52 1.330(18) . ?
C52 H52 0.9300 . ?
C52 C53 1.326(18) . ?
C53 H53 0.9300 . ?
C53 C54 1.403(16) . ?
C54 H54 0.9300 . ?
C55 C56 1.388(11) . ?
C55 C60 1.391(12) . ?
C56 H56 0.9300 . ?
C56 C57 1.400(14) . ?
C57 H57 0.9300 . ?
C57 C58 1.352(16) . ?
C58 H58 0.9300 . ?
C58 C59 1.356(15) . ?
C59 H59 0.9300 . ?
C59 C60 1.388(13) . ?
C60 H60 0.9300 . ?
C61 C62 1.388(11) . ?
C61 C66 1.395(11) . ?
C62 H62 0.9300 . ?
C62 C63 1.384(12) . ?
C63 H63 0.9300 . ?
C63 C64 1.354(12) . ?
C64 H64 0.9300 . ?
C64 C65 1.361(12) . ?
C65 H65 0.9300 . ?
C65 C66 1.380(11) . ?
C66 H66 0.9300 . ?
C67 C68 1.377(11) . ?
C67 C72 1.404(11) . ?
C68 H68 0.9300 . ?
C68 C69 1.373(12) . ?
C69 H69 0.9300 . ?
C69 C70 1.389(15) . ?
C70 H70 0.9300 . ?
C70 C71 1.366(15) . ?
C71 H71 0.9300 . ?
C71 C72 1.371(12) . ?
C72 H72 0.9300 . ?
C73 C74 1.392(13) . ?
C73 C78 1.387(12) . ?
C74 H74 0.9300 . ?
C74 C75 1.356(15) . ?
C75 H75 0.9300 . ?
C75 C76 1.43(2) . ?
C76 H76 0.9300 . ?
C76 C77 1.356(18) . ?
C77 H77 0.9300 . ?
C77 C78 1.368(13) . ?
C78 H78 0.9300 . ?
C79 C80 1.378(10) . ?
C79 C84 1.390(11) . ?
C80 H80 0.9300 . ?
C80 C81 1.393(11) . ?
C81 H81 0.9300 . ?
C81 C82 1.368(13) . ?
C82 H82 0.9300 . ?
C82 C83 1.381(12) . ?
C83 H83 0.9300 . ?
C83 C84 1.398(11) . ?
C84 H84 0.9300 . ?
C85 C86 1.414(11) . ?
C85 C90 1.383(12) . ?
C86 H86 0.9300 . ?
C86 C87 1.364(13) . ?
C87 H87 0.9300 . ?
C87 C88 1.374(15) . ?
C88 H88 0.9300 . ?
C88 C89 1.391(14) . ?
C89 H89 0.9300 . ?
C89 C90 1.384(12) . ?
C90 H90 0.9300 . ?
C91 C92 1.363(11) . ?
C91 C96 1.406(10) . ?
C92 H92 0.9300 . ?
C92 C93 1.362(11) . ?
C93 H93 0.9300 . ?
C93 C94 1.388(12) . ?
C94 H94 0.9300 . ?
C94 C95 1.373(14) . ?
C95 H95 0.9300 . ?
C95 C96 1.375(12) . ?
C96 H96 0.9300 . ?
C97 C98 1.385(11) . ?
C97 C102 1.408(12) . ?
C98 H98 0.9300 . ?
C98 C99 1.389(12) . ?
C99 H99 0.9300 . ?
C99 C100 1.338(15) . ?
C100 H100 0.9300 . ?
C100 C101 1.368(15) . ?
C101 H101 0.9300 . ?
C101 C102 1.402(13) . ?
C102 H102 0.9300 . ?
C103 C104 1.408(10) . ?
C103 C108 1.384(11) . ?
C104 H104 0.9300 . ?
C104 C105 1.383(13) . ?
C105 H105 0.9300 . ?
C105 C106 1.353(16) . ?
C106 H106 0.9300 . ?
C106 C107 1.373(16) . ?
C107 H107 0.9300 . ?
C107 C108 1.357(13) . ?
C108 H108 0.9300 . ?
C109 C110 1.389(11) . ?
C109 C114 1.385(11) . ?
C110 H110 0.9300 . ?
C110 C111 1.377(10) . ?
C111 H111 0.9300 . ?
C111 C112 1.384(12) . ?
C112 H112 0.9300 . ?
C112 C113 1.361(13) . ?
C113 H113 0.9300 . ?
C113 C114 1.385(11) . ?
C114 H114 0.9300 . ?
C115 C116 1.377(11) . ?
C115 C120 1.394(11) . ?
C116 H116 0.9300 . ?
C116 C117 1.373(12) . ?
C117 H117 0.9300 . ?
C117 C118 1.352(15) . ?
C118 H118 0.9300 . ?
C118 C119 1.355(16) . ?
C119 H119 0.9300 . ?
C119 C120 1.385(13) . ?
C120 H120 0.9300 . ?
C121 C122 1.370(10) . ?
C121 C126 1.390(10) . ?
C122 H122 0.9300 . ?
C122 C123 1.383(11) . ?
C123 H123 0.9300 . ?
C123 C124 1.361(13) . ?
C124 H124 0.9300 . ?
C124 C125 1.365(14) . ?
C125 H125 0.9300 . ?
C125 C126 1.393(13) . ?
C126 H126 0.9300 . ?
O1 C130 1.34(3) . ?
O1 C131 1.36(3) . ?
C129 H12A 0.9600 . ?
C129 H12B 0.9600 . ?
C129 H12C 0.9600 . ?
C129 C130 1.424(15) . ?
C130 H13A 0.9700 . ?
C130 H13B 0.9700 . ?
C131 H13C 0.9700 . ?
C131 H13D 0.9700 . ?
C131 C132 1.48(2) . ?
C132 H13E 0.9672 . ?
C132 H13F 0.9741 . ?
C132 H13G 0.9758 . ?
O2 H2A 0.8742 . ?
O2 C128 1.37(3) . ?
C128 H12D 0.9851 . ?
C128 H12E 0.9804 . ?
C128 H12F 0.9899 . ?
O3 H3A 0.8204 . ?
O3 C127 1.478(16) . ?
C127 H12G 1.0401 . ?
C127 H12H 1.0619 . ?
C127 H12I 1.0543 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au2 Au1 Au3 93.800(12) . . ?
Au4 Au1 Au2 93.500(11) . . ?
Au4 Au1 Au3 93.305(11) . . ?
Au5 Au1 Au2 57.375(10) . . ?
Au5 Au1 Au3 56.903(9) . . ?
Au5 Au1 Au4 57.556(10) . . ?
P1 Au1 Au2 125.77(5) . . ?
P1 Au1 Au3 122.57(5) . . ?
P1 Au1 Au4 119.70(5) . . ?
P1 Au1 Au5 176.57(5) . . ?
Au1 Au2 Au7 109.757(12) . . ?
Au1 Au2 Ag1 84.123(14) . . ?
Au5 Au2 Au1 55.335(10) . . ?
Au5 Au2 Au7 54.489(9) . . ?
Au5 Au2 Ag1 58.603(13) . . ?
Au5 Au2 Ag2 59.908(13) . . ?
Ag1 Au2 Au7 57.819(13) . . ?
Ag2 Au2 Au1 85.922(15) . . ?
Ag2 Au2 Au7 62.346(13) . . ?
Ag2 Au2 Ag1 110.754(17) . . ?
P4 Au2 Au1 126.32(5) . . ?
P4 Au2 Au5 177.36(5) . . ?
P4 Au2 Au7 123.92(5) . . ?
P4 Au2 Ag1 122.86(5) . . ?
P4 Au2 Ag2 117.64(5) . . ?
Au1 Au3 Au6 107.776(11) . . ?
Au5 Au3 Au1 54.950(9) . . ?
Au5 Au3 Au6 52.881(9) . . ?
Au5 Au3 Ag1 59.583(13) . . ?
Au5 Au3 Ag3 58.505(13) . . ?
Ag1 Au3 Au1 84.842(14) . . ?
Ag1 Au3 Au6 62.222(13) . . ?
Ag1 Au3 Ag3 110.440(16) . . ?
Ag3 Au3 Au1 84.424(14) . . ?
Ag3 Au3 Au6 56.840(12) . . ?
P2 Au3 Au1 128.03(4) . . ?
P2 Au3 Au5 176.43(5) . . ?
P2 Au3 Au6 124.19(4) . . ?
P2 Au3 Ag1 117.68(5) . . ?
P2 Au3 Ag3 122.41(5) . . ?
Au1 Au4 Au8 109.741(12) . . ?
Au1 Au4 Ag2 84.622(14) . . ?
Au5 Au4 Au1 55.440(10) . . ?
Au5 Au4 Au8 54.416(9) . . ?
Au5 Au4 Ag2 58.806(13) . . ?
Au5 Au4 Ag3 59.629(13) . . ?
Ag2 Au4 Au8 56.728(12) . . ?
Ag3 Au4 Au1 86.771(14) . . ?
Ag3 Au4 Au8 61.888(12) . . ?
Ag3 Au4 Ag2 109.848(17) . . ?
P3 Au4 Au1 128.28(5) . . ?
P3 Au4 Au5 176.10(5) . . ?
P3 Au4 Au8 121.94(5) . . ?
P3 Au4 Ag2 121.16(6) . . ?
P3 Au4 Ag3 118.03(6) . . ?
Au1 Au5 Au2 67.290(10) . . ?
Au1 Au5 Au3 68.147(11) . . ?
Au1 Au5 Au4 67.004(11) . . ?
Au1 Au5 Au6 141.807(14) . . ?
Au1 Au5 Au7 137.819(14) . . ?
Au1 Au5 Au8 137.833(15) . . ?
Au1 Au5 Ag1 94.111(16) . . ?
Au1 Au5 Ag2 94.255(15) . . ?
Au1 Au5 Ag3 95.416(14) . . ?
Au2 Au5 Au4 105.526(13) . . ?
Au2 Au5 Ag1 65.491(14) . . ?
Au2 Au5 Ag2 63.273(14) . . ?
Au2 Au5 Ag3 162.589(16) . . ?
Au3 Au5 Au2 107.096(13) . . ?
Au3 Au5 Au4 106.157(13) . . ?
Au3 Au5 Ag1 63.685(14) . . ?
Au3 Au5 Ag2 162.393(16) . . ?
Au3 Au5 Ag3 65.920(14) . . ?
Au4 Au5 Ag1 161.100(17) . . ?
Au4 Au5 Ag2 65.291(14) . . ?
Au4 Au5 Ag3 63.674(14) . . ?
Au6 Au5 Au2 129.365(14) . . ?
Au6 Au5 Au3 73.776(11) . . ?
Au6 Au5 Au4 123.214(13) . . ?
Au6 Au5 Au7 68.304(11) . . ?
Au6 Au5 Au8 68.402(11) . . ?
Au6 Au5 Ag1 71.049(14) . . ?
Au6 Au5 Ag2 123.828(15) . . ?
Au6 Au5 Ag3 65.622(13) . . ?
Au7 Au5 Au2 70.652(11) . . ?
Au7 Au5 Au3 123.375(14) . . ?
Au7 Au5 Au4 129.537(14) . . ?
Au7 Au5 Au8 70.298(11) . . ?
Au7 Au5 Ag1 65.064(14) . . ?
Au7 Au5 Ag2 69.153(14) . . ?
Au7 Au5 Ag3 126.718(15) . . ?
Au8 Au5 Au2 122.172(13) . . ?
Au8 Au5 Au3 129.829(13) . . ?
Au8 Au5 Au4 71.041(11) . . ?
Au8 Au5 Ag1 127.847(16) . . ?
Au8 Au5 Ag2 63.824(13) . . ?
Au8 Au5 Ag3 69.028(14) . . ?
Ag1 Au5 Ag2 119.394(18) . . ?
Ag1 Au5 Ag3 120.141(18) . . ?
Ag3 Au5 Ag2 118.561(19) . . ?
Au5 Au6 Au3 53.343(9) . . ?
Au5 Au6 Au7 55.936(9) . . ?
Au5 Au6 Au8 56.045(9) . . ?
Au5 Au6 Ag1 55.958(13) . . ?
Au5 Au6 Ag3 58.931(13) . . ?
Au7 Au6 Au3 98.762(10) . . ?
Au7 Au6 Au8 61.787(9) . . ?
Au7 Au6 Ag1 56.695(12) . . ?
Au8 Au6 Au3 102.745(10) . . ?
Au8 Au6 Ag1 105.089(14) . . ?
Ag1 Au6 Au3 53.680(12) . . ?
Ag3 Au6 Au3 57.448(12) . . ?
Ag3 Au6 Au7 109.886(14) . . ?
Ag3 Au6 Au8 62.545(13) . . ?
Ag3 Au6 Ag1 103.607(16) . . ?
P7 Au6 Au3 118.39(4) . . ?
P7 Au6 Au5 171.46(4) . . ?
P7 Au6 Au7 131.53(4) . . ?
P7 Au6 Au8 129.28(5) . . ?
P7 Au6 Ag1 122.52(5) . . ?
P7 Au6 Ag3 115.95(5) . . ?
Au5 Au7 Au2 54.860(9) . . ?
Au5 Au7 Au6 55.759(9) . . ?
Au5 Au7 Au8 55.004(9) . . ?
Au5 Au7 Ag1 59.034(13) . . ?
Au5 Au7 Ag2 56.995(12) . . ?
Au6 Au7 Au2 105.050(10) . . ?
Au6 Au7 Au8 59.257(9) . . ?
Au6 Au7 Ag2 104.064(13) . . ?
Au8 Au7 Au2 98.956(11) . . ?
Au8 Au7 Ag2 55.724(12) . . ?
Ag1 Au7 Au2 58.557(13) . . ?
Ag1 Au7 Au6 64.430(13) . . ?
Ag1 Au7 Au8 109.068(14) . . ?
Ag1 Au7 Ag2 105.279(16) . . ?
Ag2 Au7 Au2 55.137(12) . . ?
P5 Au7 Au2 118.66(5) . . ?
P5 Au7 Au5 173.18(5) . . ?
P5 Au7 Au6 128.53(5) . . ?
P5 Au7 Au8 131.13(5) . . ?
P5 Au7 Ag1 116.67(5) . . ?
P5 Au7 Ag2 122.36(5) . . ?
Au5 Au8 Au4 54.543(9) . . ?
Au5 Au8 Au6 55.552(9) . . ?
Au5 Au8 Au7 54.698(9) . . ?
Au5 Au8 Ag2 59.655(13) . . ?
Au5 Au8 Ag3 56.876(12) . . ?
Au6 Au8 Au4 100.466(11) . . ?
Au6 Au8 Au7 58.956(10) . . ?
Au6 Au8 Ag3 57.816(12) . . ?
Au7 Au8 Au4 102.816(11) . . ?
Au7 Au8 Ag3 104.057(14) . . ?
Ag2 Au8 Au4 58.630(13) . . ?
Ag2 Au8 Au6 109.117(15) . . ?
Ag2 Au8 Au7 62.313(13) . . ?
Ag2 Au8 Ag3 105.810(17) . . ?
Ag3 Au8 Au4 55.268(12) . . ?
P6 Au8 Au4 122.68(5) . . ?
P6 Au8 Au5 176.16(5) . . ?
P6 Au8 Au6 128.28(5) . . ?
P6 Au8 Au7 126.04(5) . . ?
P6 Au8 Ag2 116.90(5) . . ?
P6 Au8 Ag3 124.53(5) . . ?
Au2 Ag1 Au6 104.685(18) . . ?
Au3 Ag1 Au2 95.635(18) . . ?
Au3 Ag1 Au6 64.097(13) . . ?
Au3 Ag1 Au7 108.681(19) . . ?
Au5 Ag1 Au2 55.906(13) . . ?
Au5 Ag1 Au3 56.732(13) . . ?
Au5 Ag1 Au6 52.993(12) . . ?
Au5 Ag1 Au7 55.903(13) . . ?
Au7 Ag1 Au2 63.624(13) . . ?
Au7 Ag1 Au6 58.875(13) . . ?
Cl1 Ag1 Au2 128.31(5) . . ?
Cl1 Ag1 Au3 120.05(6) . . ?
Cl1 Ag1 Au5 175.69(5) . . ?
Cl1 Ag1 Au6 123.58(6) . . ?
Cl1 Ag1 Au7 125.64(6) . . ?
Au2 Ag2 Au4 94.727(17) . . ?
Au2 Ag2 Au7 62.516(13) . . ?
Au2 Ag2 Au8 109.550(18) . . ?
Au4 Ag2 Au7 106.731(17) . . ?
Au5 Ag2 Au2 56.819(13) . . ?
Au5 Ag2 Au4 55.903(13) . . ?
Au5 Ag2 Au7 53.852(12) . . ?
Au5 Ag2 Au8 56.522(12) . . ?
Au8 Ag2 Au4 64.642(13) . . ?
Au8 Ag2 Au7 61.963(13) . . ?
Cl2 Ag2 Au2 122.77(5) . . ?
Cl2 Ag2 Au4 127.70(5) . . ?
Cl2 Ag2 Au5 175.82(5) . . ?
Cl2 Ag2 Au7 122.00(5) . . ?
Cl2 Ag2 Au8 121.97(5) . . ?
Au3 Ag3 Au8 106.554(17) . . ?
Au4 Ag3 Au3 94.386(16) . . ?
Au4 Ag3 Au6 107.744(18) . . ?
Au4 Ag3 Au8 62.844(13) . . ?
Au5 Ag3 Au3 55.575(12) . . ?
Au5 Ag3 Au4 56.696(13) . . ?
Au5 Ag3 Au6 55.446(12) . . ?
Au5 Ag3 Au8 54.096(12) . . ?
Au6 Ag3 Au3 65.713(13) . . ?
Au6 Ag3 Au8 59.638(12) . . ?
Cl3 Ag3 Au3 131.69(5) . . ?
Cl3 Ag3 Au4 116.99(6) . . ?
Cl3 Ag3 Au5 172.26(6) . . ?
Cl3 Ag3 Au6 127.74(5) . . ?
Cl3 Ag3 Au8 119.99(5) . . ?
C1 P1 Au1 113.6(2) . . ?
C1 P1 C13 105.6(3) . . ?
C7 P1 Au1 111.6(2) . . ?
C7 P1 C1 106.9(3) . . ?
C7 P1 C13 105.4(3) . . ?
C13 P1 Au1 113.2(2) . . ?
C19 P2 Au3 116.6(3) . . ?
C25 P2 Au3 113.1(3) . . ?
C25 P2 C19 103.7(3) . . ?
C31 P2 Au3 114.1(2) . . ?
C31 P2 C19 103.9(4) . . ?
C31 P2 C25 104.1(4) . . ?
C37 P3 Au4 112.7(3) . . ?
C37 P3 C49 105.0(4) . . ?
C43 P3 Au4 113.8(3) . . ?
C43 P3 C37 105.5(4) . . ?
C43 P3 C49 102.3(4) . . ?
C49 P3 Au4 116.3(3) . . ?
C55 P4 Au2 111.7(3) . . ?
C55 P4 C61 105.2(4) . . ?
C55 P4 C67 105.8(4) . . ?
C61 P4 Au2 115.5(3) . . ?
C67 P4 Au2 115.8(3) . . ?
C67 P4 C61 101.7(3) . . ?
C73 P5 Au7 113.1(2) . . ?
C73 P5 C79 101.4(3) . . ?
C79 P5 Au7 114.4(2) . . ?
C85 P5 Au7 114.5(3) . . ?
C85 P5 C73 106.5(4) . . ?
C85 P5 C79 105.7(3) . . ?
C91 P6 Au8 112.8(2) . . ?
C97 P6 Au8 116.5(2) . . ?
C97 P6 C91 102.8(3) . . ?
C103 P6 Au8 113.4(2) . . ?
C103 P6 C91 104.2(3) . . ?
C103 P6 C97 105.9(4) . . ?
C109 P7 Au6 116.3(2) . . ?
C115 P7 Au6 109.9(2) . . ?
C115 P7 C109 102.9(3) . . ?
C115 P7 C121 108.4(3) . . ?
C121 P7 Au6 113.8(2) . . ?
C121 P7 C109 104.8(3) . . ?
C2 C1 P1 118.6(6) . . ?
C6 C1 P1 123.2(6) . . ?
C6 C1 C2 118.1(7) . . ?
C1 C2 H2 119.7 . . ?
C3 C2 C1 120.6(8) . . ?
C3 C2 H2 119.7 . . ?
C2 C3 H3 119.7 . . ?
C2 C3 C4 120.7(9) . . ?
C4 C3 H3 119.7 . . ?
C3 C4 H4 120.0 . . ?
C5 C4 C3 120.0(8) . . ?
C5 C4 H4 120.0 . . ?
C4 C5 H5 119.7 . . ?
C4 C5 C6 120.7(8) . . ?
C6 C5 H5 119.6 . . ?
C1 C6 H6 120.1 . . ?
C5 C6 C1 119.8(8) . . ?
C5 C6 H6 120.1 . . ?
C8 C7 P1 123.5(6) . . ?
C12 C7 P1 119.5(5) . . ?
C12 C7 C8 116.9(7) . . ?
C7 C8 H8 119.5 . . ?
C9 C8 C7 121.0(7) . . ?
C9 C8 H8 119.5 . . ?
C8 C9 H9 119.9 . . ?
C10 C9 C8 120.1(8) . . ?
C10 C9 H9 120.0 . . ?
C9 C10 H10 119.7 . . ?
C9 C10 C11 120.6(8) . . ?
C11 C10 H10 119.7 . . ?
C10 C11 H11 120.6 . . ?
C10 C11 C12 118.9(8) . . ?
C12 C11 H11 120.6 . . ?
C7 C12 H12 118.8 . . ?
C11 C12 C7 122.4(7) . . ?
C11 C12 H12 118.8 . . ?
C14 C13 P1 117.6(6) . . ?
C18 C13 P1 123.0(6) . . ?
C18 C13 C14 119.4(8) . . ?
C13 C14 H14 120.2 . . ?
C15 C14 C13 119.6(8) . . ?
C15 C14 H14 120.2 . . ?
C14 C15 H15 119.7 . . ?
C16 C15 C14 120.7(9) . . ?
C16 C15 H15 119.6 . . ?
C15 C16 H16 120.0 . . ?
C17 C16 C15 120.0(9) . . ?
C17 C16 H16 119.9 . . ?
C16 C17 H17 119.4 . . ?
C16 C17 C18 121.2(9) . . ?
C18 C17 H17 119.4 . . ?
C13 C18 C17 119.1(8) . . ?
C13 C18 H18 120.5 . . ?
C17 C18 H18 120.4 . . ?
C20 C19 P2 118.5(6) . . ?
C20 C19 C24 118.1(7) . . ?
C24 C19 P2 123.3(6) . . ?
C19 C20 H20 119.1 . . ?
C21 C20 C19 121.7(8) . . ?
C21 C20 H20 119.2 . . ?
C20 C21 H21 120.6 . . ?
C22 C21 C20 118.8(9) . . ?
C22 C21 H21 120.6 . . ?
C21 C22 H22 119.2 . . ?
C21 C22 C23 121.7(8) . . ?
C23 C22 H22 119.2 . . ?
C22 C23 H23 119.9 . . ?
C24 C23 C22 120.2(9) . . ?
C24 C23 H23 119.9 . . ?
C19 C24 H24 120.2 . . ?
C23 C24 C19 119.5(9) . . ?
C23 C24 H24 120.3 . . ?
C26 C25 P2 124.3(6) . . ?
C30 C25 P2 116.8(6) . . ?
C30 C25 C26 118.9(7) . . ?
C25 C26 H26 119.7 . . ?
C27 C26 C25 120.5(9) . . ?
C27 C26 H26 119.8 . . ?
C26 C27 H27 119.9 . . ?
C26 C27 C28 120.2(9) . . ?
C28 C27 H27 119.9 . . ?
C27 C28 H28 120.0 . . ?
C27 C28 C29 120.2(9) . . ?
C29 C28 H28 119.9 . . ?
C28 C29 H29 120.1 . . ?
C30 C29 C28 119.8(9) . . ?
C30 C29 H29 120.1 . . ?
C25 C30 H30 119.8 . . ?
C29 C30 C25 120.4(8) . . ?
C29 C30 H30 119.8 . . ?
C32 C31 P2 119.8(6) . . ?
C32 C31 C36 118.1(7) . . ?
C36 C31 P2 122.1(6) . . ?
C31 C32 H32 119.7 . . ?
C33 C32 C31 120.6(8) . . ?
C33 C32 H32 119.7 . . ?
C32 C33 H33 119.9 . . ?
C32 C33 C34 120.1(8) . . ?
C34 C33 H33 119.9 . . ?
C33 C34 H34 120.1 . . ?
C35 C34 C33 119.8(8) . . ?
C35 C34 H34 120.1 . . ?
C34 C35 H35 120.1 . . ?
C34 C35 C36 119.8(9) . . ?
C36 C35 H35 120.1 . . ?
C31 C36 H36 119.3 . . ?
C35 C36 C31 121.5(8) . . ?
C35 C36 H36 119.2 . . ?
C38 C37 P3 116.9(6) . . ?
C42 C37 P3 124.0(8) . . ?
C42 C37 C38 119.1(9) . . ?
C37 C38 H38 119.8 . . ?
C39 C38 C37 120.4(8) . . ?
C39 C38 H38 119.8 . . ?
C38 C39 H39 120.0 . . ?
C38 C39 C40 119.9(10) . . ?
C40 C39 H39 120.1 . . ?
C39 C40 H40 119.8 . . ?
C41 C40 C39 120.4(10) . . ?
C41 C40 H40 119.8 . . ?
C40 C41 H41 120.3 . . ?
C40 C41 C42 119.5(9) . . ?
C42 C41 H41 120.2 . . ?
C37 C42 C41 120.7(10) . . ?
C37 C42 H42 119.6 . . ?
C41 C42 H42 119.7 . . ?
C44 C43 P3 122.8(7) . . ?
C44 C43 C48 118.1(8) . . ?
C48 C43 P3 118.7(6) . . ?
C43 C44 H44 119.3 . . ?
C45 C44 C43 121.5(10) . . ?
C45 C44 H44 119.2 . . ?
C44 C45 H45 120.1 . . ?
C46 C45 C44 120.0(11) . . ?
C46 C45 H45 120.0 . . ?
C45 C46 H46 119.2 . . ?
C45 C46 C47 121.6(11) . . ?
C47 C46 H46 119.2 . . ?
C46 C47 H47 121.0 . . ?
C46 C47 C48 117.8(11) . . ?
C48 C47 H47 121.2 . . ?
C43 C48 C47 121.0(9) . . ?
C43 C48 H48 119.5 . . ?
C47 C48 H48 119.5 . . ?
C50 C49 P3 119.3(8) . . ?
C50 C49 C54 118.2(9) . . ?
C54 C49 P3 122.5(7) . . ?
C49 C50 H50 120.3 . . ?
C49 C50 C51 119.4(11) . . ?
C51 C50 H50 120.3 . . ?
C50 C51 H51 119.1 . . ?
C52 C51 C50 121.8(12) . . ?
C52 C51 H51 119.1 . . ?
C51 C52 H52 120.3 . . ?
C53 C52 C51 119.4(11) . . ?
C53 C52 H52 120.3 . . ?
C52 C53 H53 119.7 . . ?
C52 C53 C54 120.5(13) . . ?
C54 C53 H53 119.7 . . ?
C49 C54 C53 120.1(12) . . ?
C49 C54 H54 120.0 . . ?
C53 C54 H54 119.9 . . ?
C56 C55 P4 123.0(7) . . ?
C56 C55 C60 118.9(8) . . ?
C60 C55 P4 118.0(6) . . ?
C55 C56 H56 119.9 . . ?
C55 C56 C57 120.1(10) . . ?
C57 C56 H56 120.0 . . ?
C56 C57 H57 120.3 . . ?
C58 C57 C56 119.5(10) . . ?
C58 C57 H57 120.2 . . ?
C57 C58 H58 119.3 . . ?
C57 C58 C59 121.5(10) . . ?
C59 C58 H58 119.2 . . ?
C58 C59 H59 119.9 . . ?
C58 C59 C60 120.2(10) . . ?
C60 C59 H59 119.9 . . ?
C55 C60 H60 120.1 . . ?
C59 C60 C55 119.7(9) . . ?
C59 C60 H60 120.1 . . ?
C62 C61 P4 123.6(6) . . ?
C62 C61 C66 118.6(7) . . ?
C66 C61 P4 117.7(6) . . ?
C61 C62 H62 120.2 . . ?
C63 C62 C61 119.6(8) . . ?
C63 C62 H62 120.2 . . ?
C62 C63 H63 119.2 . . ?
C64 C63 C62 121.6(9) . . ?
C64 C63 H63 119.2 . . ?
C63 C64 H64 120.5 . . ?
C63 C64 C65 119.1(8) . . ?
C65 C64 H64 120.5 . . ?
C64 C65 H65 119.2 . . ?
C64 C65 C66 121.5(8) . . ?
C66 C65 H65 119.2 . . ?
C61 C66 H66 120.2 . . ?
C65 C66 C61 119.5(8) . . ?
C65 C66 H66 120.2 . . ?
C68 C67 P4 122.9(6) . . ?
C68 C67 C72 118.9(7) . . ?
C72 C67 P4 117.6(6) . . ?
C67 C68 H68 119.8 . . ?
C67 C68 C69 120.4(9) . . ?
C69 C68 H68 119.8 . . ?
C68 C69 H69 119.9 . . ?
C68 C69 C70 120.2(9) . . ?
C70 C69 H69 119.9 . . ?
C69 C70 H70 120.1 . . ?
C71 C70 C69 119.8(8) . . ?
C71 C70 H70 120.1 . . ?
C70 C71 H71 119.8 . . ?
C70 C71 C72 120.3(9) . . ?
C72 C71 H71 119.8 . . ?
C67 C72 H72 119.9 . . ?
C71 C72 C67 120.2(8) . . ?
C71 C72 H72 119.9 . . ?
C74 C73 P5 116.4(7) . . ?
C78 C73 P5 123.3(7) . . ?
C78 C73 C74 120.3(9) . . ?
C73 C74 H74 120.2 . . ?
C75 C74 C73 119.7(11) . . ?
C75 C74 H74 120.2 . . ?
C74 C75 H75 120.0 . . ?
C74 C75 C76 119.9(12) . . ?
C76 C75 H75 120.1 . . ?
C75 C76 H76 120.3 . . ?
C77 C76 C75 119.3(11) . . ?
C77 C76 H76 120.3 . . ?
C76 C77 H77 119.5 . . ?
C76 C77 C78 121.0(12) . . ?
C78 C77 H77 119.5 . . ?
C73 C78 H78 120.2 . . ?
C77 C78 C73 119.7(10) . . ?
C77 C78 H78 120.1 . . ?
C80 C79 P5 122.5(6) . . ?
C80 C79 C84 119.3(7) . . ?
C84 C79 P5 118.2(5) . . ?
C79 C80 H80 119.7 . . ?
C79 C80 C81 120.5(8) . . ?
C81 C80 H80 119.8 . . ?
C80 C81 H81 119.7 . . ?
C82 C81 C80 120.5(7) . . ?
C82 C81 H81 119.8 . . ?
C81 C82 H82 120.3 . . ?
C81 C82 C83 119.5(7) . . ?
C83 C82 H82 120.3 . . ?
C82 C83 H83 119.7 . . ?
C82 C83 C84 120.6(8) . . ?
C84 C83 H83 119.7 . . ?
C79 C84 C83 119.5(7) . . ?
C79 C84 H84 120.2 . . ?
C83 C84 H84 120.2 . . ?
C86 C85 P5 124.0(7) . . ?
C90 C85 P5 118.0(6) . . ?
C90 C85 C86 117.9(8) . . ?
C85 C86 H86 120.1 . . ?
C87 C86 C85 119.8(9) . . ?
C87 C86 H86 120.1 . . ?
C86 C87 H87 119.1 . . ?
C86 C87 C88 121.8(8) . . ?
C88 C87 H87 119.1 . . ?
C87 C88 H88 120.3 . . ?
C87 C88 C89 119.4(9) . . ?
C89 C88 H88 120.3 . . ?
C88 C89 H89 120.4 . . ?
C90 C89 C88 119.2(10) . . ?
C90 C89 H89 120.4 . . ?
C85 C90 C89 121.9(8) . . ?
C85 C90 H90 119.1 . . ?
C89 C90 H90 119.0 . . ?
C92 C91 P6 119.3(5) . . ?
C92 C91 C96 118.6(7) . . ?
C96 C91 P6 122.0(6) . . ?
C91 C92 H92 118.8 . . ?
C93 C92 C91 122.4(7) . . ?
C93 C92 H92 118.8 . . ?
C92 C93 H93 120.4 . . ?
C92 C93 C94 119.2(8) . . ?
C94 C93 H93 120.3 . . ?
C93 C94 H94 120.4 . . ?
C95 C94 C93 119.3(8) . . ?
C95 C94 H94 120.3 . . ?
C94 C95 H95 119.3 . . ?
C94 C95 C96 121.3(8) . . ?
C96 C95 H95 119.4 . . ?
C91 C96 H96 120.5 . . ?
C95 C96 C91 119.1(9) . . ?
C95 C96 H96 120.4 . . ?
C98 C97 P6 118.7(6) . . ?
C98 C97 C102 118.4(8) . . ?
C102 C97 P6 123.0(6) . . ?
C97 C98 H98 120.6 . . ?
C97 C98 C99 118.9(8) . . ?
C99 C98 H98 120.5 . . ?
C98 C99 H99 118.6 . . ?
C100 C99 C98 122.7(9) . . ?
C100 C99 H99 118.6 . . ?
C99 C100 H100 119.9 . . ?
C99 C100 C101 120.2(9) . . ?
C101 C100 H100 119.8 . . ?
C100 C101 H101 120.4 . . ?
C100 C101 C102 119.1(10) . . ?
C102 C101 H101 120.4 . . ?
C97 C102 H102 119.8 . . ?
C101 C102 C97 120.5(9) . . ?
C101 C102 H102 119.7 . . ?
C104 C103 P6 122.6(6) . . ?
C108 C103 P6 118.8(6) . . ?
C108 C103 C104 118.5(7) . . ?
C103 C104 H104 120.3 . . ?
C105 C104 C103 119.5(9) . . ?
C105 C104 H104 120.2 . . ?
C104 C105 H105 119.7 . . ?
C106 C105 C104 120.7(9) . . ?
C106 C105 H105 119.6 . . ?
C105 C106 H106 120.2 . . ?
C105 C106 C107 119.6(10) . . ?
C107 C106 H106 120.2 . . ?
C106 C107 H107 119.2 . . ?
C108 C107 C106 121.5(10) . . ?
C108 C107 H107 119.3 . . ?
C103 C108 H108 120.0 . . ?
C107 C108 C103 120.1(8) . . ?
C107 C108 H108 119.9 . . ?
C110 C109 P7 118.7(5) . . ?
C114 C109 P7 122.8(6) . . ?
C114 C109 C110 118.5(7) . . ?
C109 C110 H110 119.5 . . ?
C111 C110 C109 121.0(7) . . ?
C111 C110 H110 119.5 . . ?
C110 C111 H111 120.0 . . ?
C110 C111 C112 120.1(8) . . ?
C112 C111 H111 119.9 . . ?
C111 C112 H112 120.5 . . ?
C113 C112 C111 119.0(7) . . ?
C113 C112 H112 120.5 . . ?
C112 C113 H113 119.1 . . ?
C112 C113 C114 121.7(8) . . ?
C114 C113 H113 119.2 . . ?
C109 C114 H114 120.2 . . ?
C113 C114 C109 119.6(8) . . ?
C113 C114 H114 120.2 . . ?
C116 C115 P7 117.0(6) . . ?
C116 C115 C120 117.7(8) . . ?
C120 C115 P7 125.3(6) . . ?
C115 C116 H116 118.9 . . ?
C117 C116 C115 122.3(9) . . ?
C117 C116 H116 118.9 . . ?
C116 C117 H117 120.5 . . ?
C118 C117 C116 119.0(10) . . ?
C118 C117 H117 120.5 . . ?
C117 C118 H118 119.6 . . ?
C117 C118 C119 120.8(9) . . ?
C119 C118 H118 119.6 . . ?
C118 C119 H119 119.6 . . ?
C118 C119 C120 120.8(10) . . ?
C120 C119 H119 119.6 . . ?
C115 C120 H120 120.3 . . ?
C119 C120 C115 119.4(9) . . ?
C119 C120 H120 120.3 . . ?
C122 C121 P7 118.0(5) . . ?
C122 C121 C126 119.4(7) . . ?
C126 C121 P7 122.6(6) . . ?
C121 C122 H122 119.3 . . ?
C121 C122 C123 121.5(7) . . ?
C123 C122 H122 119.2 . . ?
C122 C123 H123 120.4 . . ?
C124 C123 C122 119.3(8) . . ?
C124 C123 H123 120.4 . . ?
C123 C124 H124 119.9 . . ?
C123 C124 C125 120.2(9) . . ?
C125 C124 H124 119.9 . . ?
C124 C125 H125 119.3 . . ?
C124 C125 C126 121.4(9) . . ?
C126 C125 H125 119.3 . . ?
C121 C126 C125 118.3(8) . . ?
C121 C126 H126 120.8 . . ?
C125 C126 H126 120.9 . . ?
C130 O1 C131 170(5) . . ?
H12A C129 H12B 109.5 . . ?
H12A C129 H12C 109.5 . . ?
H12B C129 H12C 109.5 . . ?
C130 C129 H12A 108.1 . . ?
C130 C129 H12B 110.1 . . ?
C130 C129 H12C 110.2 . . ?
O1 C130 C129 105(2) . . ?
O1 C130 H13A 108.7 . . ?
O1 C130 H13B 112.6 . . ?
C129 C130 H13A 109.7 . . ?
C129 C130 H13B 111.7 . . ?
H13A C130 H13B 109.0 . . ?
O1 C131 H13C 99.1 . . ?
O1 C131 H13D 104.9 . . ?
O1 C131 C132 139(5) . . ?
H13C C131 H13D 104.7 . . ?
C132 C131 H13C 99.2 . . ?
C132 C131 H13D 106.0 . . ?
C131 C132 H13E 106.1 . . ?
C131 C132 H13F 112.3 . . ?
C131 C132 H13G 113.5 . . ?
H13E C132 H13F 109.2 . . ?
H13E C132 H13G 107.4 . . ?
H13F C132 H13G 108.1 . . ?
C128 O2 H2A 115.4 . . ?
O2 C128 H12D 112.3 . . ?
O2 C128 H12E 110.2 . . ?
O2 C128 H12F 114.2 . . ?
H12D C128 H12E 106.4 . . ?
H12D C128 H12F 105.9 . . ?
H12E C128 H12F 107.4 . . ?
C127 O3 H3A 110.4 . . ?
O3 C127 H12G 117.1 . . ?
O3 C127 H12H 120.3 . . ?
O3 C127 H12I 119.2 . . ?
H12G C127 H12H 98.2 . . ?
H12G C127 H12I 99.6 . . ?
H12H C127 H12I 98.3 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au1 P1 C1 C2 32.7(7) . . . . ?
Au1 P1 C1 C6 -143.1(6) . . . . ?
Au1 P1 C7 C8 -157.9(6) . . . . ?
Au1 P1 C7 C12 20.4(7) . . . . ?
Au1 P1 C13 C14 33.8(7) . . . . ?
Au1 P1 C13 C18 -144.0(6) . . . . ?
Au2 P4 C55 C56 136.9(7) . . . . ?
Au2 P4 C55 C60 -39.0(7) . . . . ?
Au2 P4 C61 C62 135.2(7) . . . . ?
Au2 P4 C61 C66 -43.6(7) . . . . ?
Au2 P4 C67 C68 150.2(6) . . . . ?
Au2 P4 C67 C72 -38.7(7) . . . . ?
Au3 P2 C19 C20 -42.3(7) . . . . ?
Au3 P2 C19 C24 141.4(7) . . . . ?
Au3 P2 C25 C26 143.8(6) . . . . ?
Au3 P2 C25 C30 -36.0(7) . . . . ?
Au3 P2 C31 C32 -35.6(7) . . . . ?
Au3 P2 C31 C36 145.9(6) . . . . ?
Au4 P3 C37 C38 -33.8(7) . . . . ?
Au4 P3 C37 C42 144.5(7) . . . . ?
Au4 P3 C43 C44 146.9(7) . . . . ?
Au4 P3 C43 C48 -40.6(8) . . . . ?
Au4 P3 C49 C50 -34.8(10) . . . . ?
Au4 P3 C49 C54 144.1(12) . . . . ?
Au6 P7 C109 C110 -18.3(7) . . . . ?
Au6 P7 C109 C114 162.7(6) . . . . ?
Au6 P7 C115 C116 -48.9(6) . . . . ?
Au6 P7 C115 C120 130.2(6) . . . . ?
Au6 P7 C121 C122 -6.8(7) . . . . ?
Au6 P7 C121 C126 174.8(7) . . . . ?
Au7 P5 C73 C74 -57.0(7) . . . . ?
Au7 P5 C73 C78 123.8(6) . . . . ?
Au7 P5 C79 C80 162.3(6) . . . . ?
Au7 P5 C79 C84 -17.3(7) . . . . ?
Au7 P5 C85 C86 164.2(6) . . . . ?
Au7 P5 C85 C90 -13.2(7) . . . . ?
Au8 P6 C91 C92 -28.0(7) . . . . ?
Au8 P6 C91 C96 153.0(6) . . . . ?
Au8 P6 C97 C98 -38.9(7) . . . . ?
Au8 P6 C97 C102 142.9(7) . . . . ?
Au8 P6 C103 C104 158.6(6) . . . . ?
Au8 P6 C103 C108 -24.4(8) . . . . ?
P1 C1 C2 C3 -176.4(7) . . . . ?
P1 C1 C6 C5 174.5(6) . . . . ?
P1 C7 C8 C9 179.7(7) . . . . ?
P1 C7 C12 C11 -178.9(7) . . . . ?
P1 C13 C14 C15 -177.4(7) . . . . ?
P1 C13 C18 C17 178.0(7) . . . . ?
P2 C19 C20 C21 -175.1(7) . . . . ?
P2 C19 C24 C23 173.9(8) . . . . ?
P2 C25 C26 C27 178.8(7) . . . . ?
P2 C25 C30 C29 -178.7(7) . . . . ?
P2 C31 C32 C33 -177.9(7) . . . . ?
P2 C31 C36 C35 176.8(7) . . . . ?
P3 C37 C38 C39 178.7(7) . . . . ?
P3 C37 C42 C41 -178.1(7) . . . . ?
P3 C43 C44 C45 173.3(10) . . . . ?
P3 C43 C48 C47 -173.5(9) . . . . ?
P3 C49 C50 C51 -175.5(12) . . . . ?
P3 C49 C54 C53 176.9(15) . . . . ?
P4 C55 C56 C57 -177.0(7) . . . . ?
P4 C55 C60 C59 177.0(7) . . . . ?
P4 C61 C62 C63 179.9(8) . . . . ?
P4 C61 C66 C65 -179.3(8) . . . . ?
P4 C67 C68 C69 169.1(7) . . . . ?
P4 C67 C72 C71 -169.7(6) . . . . ?
P5 C73 C74 C75 -179.0(9) . . . . ?
P5 C73 C78 C77 -179.9(7) . . . . ?
P5 C79 C80 C81 178.2(6) . . . . ?
P5 C79 C84 C83 -179.2(6) . . . . ?
P5 C85 C86 C87 -177.3(7) . . . . ?
P5 C85 C90 C89 178.4(8) . . . . ?
P6 C91 C92 C93 -177.4(6) . . . . ?
P6 C91 C96 C95 178.3(7) . . . . ?
P6 C97 C98 C99 -174.5(7) . . . . ?
P6 C97 C102 C101 175.7(8) . . . . ?
P6 C103 C104 C105 178.8(7) . . . . ?
P6 C103 C108 C107 -177.7(8) . . . . ?
P7 C109 C110 C111 -177.1(6) . . . . ?
P7 C109 C114 C113 177.2(7) . . . . ?
P7 C115 C116 C117 179.8(6) . . . . ?
P7 C115 C120 C119 -179.4(7) . . . . ?
P7 C121 C122 C123 -178.2(6) . . . . ?
P7 C121 C126 C125 177.9(8) . . . . ?
C1 P1 C7 C8 -33.2(7) . . . . ?
C1 P1 C7 C12 145.2(6) . . . . ?
C1 P1 C13 C14 -91.1(7) . . . . ?
C1 P1 C13 C18 91.1(7) . . . . ?
C1 C2 C3 C4 1.9(14) . . . . ?
C2 C1 C6 C5 -1.2(11) . . . . ?
C2 C3 C4 C5 -1.5(14) . . . . ?
C3 C4 C5 C6 -0.3(14) . . . . ?
C4 C5 C6 C1 1.6(13) . . . . ?
C6 C1 C2 C3 -0.5(12) . . . . ?
C7 P1 C1 C2 -90.8(7) . . . . ?
C7 P1 C1 C6 93.5(7) . . . . ?
C7 P1 C13 C14 156.0(6) . . . . ?
C7 P1 C13 C18 -21.8(8) . . . . ?
C7 C8 C9 C10 -0.6(14) . . . . ?
C8 C7 C12 C11 -0.5(12) . . . . ?
C8 C9 C10 C11 -1.1(15) . . . . ?
C9 C10 C11 C12 2.0(15) . . . . ?
C10 C11 C12 C7 -1.2(14) . . . . ?
C12 C7 C8 C9 1.4(12) . . . . ?
C13 P1 C1 C2 157.3(6) . . . . ?
C13 P1 C1 C6 -18.4(7) . . . . ?
C13 P1 C7 C8 78.8(7) . . . . ?
C13 P1 C7 C12 -102.8(7) . . . . ?
C13 C14 C15 C16 0.0(14) . . . . ?
C14 C13 C18 C17 0.3(13) . . . . ?
C14 C15 C16 C17 -1.4(15) . . . . ?
C15 C16 C17 C18 2.3(15) . . . . ?
C16 C17 C18 C13 -1.7(14) . . . . ?
C18 C13 C14 C15 0.5(13) . . . . ?
C19 P2 C25 C26 16.5(8) . . . . ?
C19 P2 C25 C30 -163.2(6) . . . . ?
C19 P2 C31 C32 92.4(7) . . . . ?
C19 P2 C31 C36 -86.0(7) . . . . ?
C19 C20 C21 C22 0.4(15) . . . . ?
C20 C19 C24 C23 -2.4(14) . . . . ?
C20 C21 C22 C23 -1.2(16) . . . . ?
C21 C22 C23 C24 0.1(17) . . . . ?
C22 C23 C24 C19 1.7(16) . . . . ?
C24 C19 C20 C21 1.4(13) . . . . ?
C25 P2 C19 C20 82.7(7) . . . . ?
C25 P2 C19 C24 -93.6(8) . . . . ?
C25 P2 C31 C32 -159.3(6) . . . . ?
C25 P2 C31 C36 22.3(8) . . . . ?
C25 C26 C27 C28 0.3(15) . . . . ?
C26 C25 C30 C29 1.5(12) . . . . ?
C26 C27 C28 C29 0.8(16) . . . . ?
C27 C28 C29 C30 -0.8(16) . . . . ?
C28 C29 C30 C25 -0.4(15) . . . . ?
C30 C25 C26 C27 -1.5(13) . . . . ?
C31 P2 C19 C20 -168.7(7) . . . . ?
C31 P2 C19 C24 14.9(8) . . . . ?
C31 P2 C25 C26 -91.9(7) . . . . ?
C31 P2 C25 C30 88.3(7) . . . . ?
C31 C32 C33 C34 0.7(13) . . . . ?
C32 C31 C36 C35 -1.6(13) . . . . ?
C32 C33 C34 C35 -1.1(14) . . . . ?
C33 C34 C35 C36 0.1(15) . . . . ?
C34 C35 C36 C31 1.3(14) . . . . ?
C36 C31 C32 C33 0.6(12) . . . . ?
C37 P3 C43 C44 22.8(9) . . . . ?
C37 P3 C43 C48 -164.6(7) . . . . ?
C37 P3 C49 C50 90.6(10) . . . . ?
C37 P3 C49 C54 -90.5(13) . . . . ?
C37 C38 C39 C40 -1.0(14) . . . . ?
C38 C37 C42 C41 0.1(13) . . . . ?
C38 C39 C40 C41 1.1(15) . . . . ?
C39 C40 C41 C42 -0.6(15) . . . . ?
C40 C41 C42 C37 0.0(15) . . . . ?
C42 C37 C38 C39 0.4(13) . . . . ?
C43 P3 C37 C38 90.9(7) . . . . ?
C43 P3 C37 C42 -90.8(8) . . . . ?
C43 P3 C49 C50 -159.4(10) . . . . ?
C43 P3 C49 C54 19.5(13) . . . . ?
C43 C44 C45 C46 -3(2) . . . . ?
C44 C43 C48 C47 -0.6(15) . . . . ?
C44 C45 C46 C47 4(2) . . . . ?
C45 C46 C47 C48 -4(2) . . . . ?
C46 C47 C48 C43 2.2(18) . . . . ?
C48 C43 C44 C45 0.7(16) . . . . ?
C49 P3 C37 C38 -161.4(6) . . . . ?
C49 P3 C37 C42 16.9(8) . . . . ?
C49 P3 C43 C44 -86.8(9) . . . . ?
C49 P3 C43 C48 85.8(8) . . . . ?
C49 C50 C51 C52 0(3) . . . . ?
C50 C49 C54 C53 -4(3) . . . . ?
C50 C51 C52 C53 -7(3) . . . . ?
C51 C52 C53 C54 8(3) . . . . ?
C52 C53 C54 C49 -3(3) . . . . ?
C54 C49 C50 C51 6(2) . . . . ?
C55 P4 C61 C62 -101.3(8) . . . . ?
C55 P4 C61 C66 80.0(7) . . . . ?
C55 P4 C67 C68 25.9(8) . . . . ?
C55 P4 C67 C72 -163.0(6) . . . . ?
C55 C56 C57 C58 0.5(15) . . . . ?
C56 C55 C60 C59 1.0(13) . . . . ?
C56 C57 C58 C59 0.4(17) . . . . ?
C57 C58 C59 C60 -0.6(17) . . . . ?
C58 C59 C60 C55 -0.1(15) . . . . ?
C60 C55 C56 C57 -1.1(13) . . . . ?
C61 P4 C55 C56 10.9(8) . . . . ?
C61 P4 C55 C60 -165.0(6) . . . . ?
C61 P4 C67 C68 -83.7(7) . . . . ?
C61 P4 C67 C72 87.4(6) . . . . ?
C61 C62 C63 C64 0.4(16) . . . . ?
C62 C61 C66 C65 1.9(14) . . . . ?
C62 C63 C64 C65 0.1(16) . . . . ?
C63 C64 C65 C66 0.5(17) . . . . ?
C64 C65 C66 C61 -1.5(16) . . . . ?
C66 C61 C62 C63 -1.4(14) . . . . ?
C67 P4 C55 C56 -96.2(8) . . . . ?
C67 P4 C55 C60 87.9(7) . . . . ?
C67 P4 C61 C62 8.9(8) . . . . ?
C67 P4 C61 C66 -169.9(7) . . . . ?
C67 C68 C69 C70 -0.8(14) . . . . ?
C68 C67 C72 C71 1.7(12) . . . . ?
C68 C69 C70 C71 3.8(15) . . . . ?
C69 C70 C71 C72 -3.9(14) . . . . ?
C70 C71 C72 C67 1.2(13) . . . . ?
C72 C67 C68 C69 -1.9(12) . . . . ?
C73 P5 C79 C80 40.2(7) . . . . ?
C73 P5 C79 C84 -139.4(6) . . . . ?
C73 P5 C85 C86 -70.1(7) . . . . ?
C73 P5 C85 C90 112.6(7) . . . . ?
C73 C74 C75 C76 1.5(19) . . . . ?
C74 C73 C78 C77 1.0(13) . . . . ?
C74 C75 C76 C77 -4(2) . . . . ?
C75 C76 C77 C78 5.6(19) . . . . ?
C76 C77 C78 C73 -3.9(16) . . . . ?
C78 C73 C74 C75 0.2(15) . . . . ?
C79 P5 C73 C74 66.0(7) . . . . ?
C79 P5 C73 C78 -113.2(7) . . . . ?
C79 P5 C85 C86 37.3(8) . . . . ?
C79 P5 C85 C90 -140.1(7) . . . . ?
C79 C80 C81 C82 1.3(12) . . . . ?
C80 C79 C84 C83 1.2(11) . . . . ?
C80 C81 C82 C83 0.6(13) . . . . ?
C81 C82 C83 C84 -1.6(13) . . . . ?
C82 C83 C84 C79 0.7(13) . . . . ?
C84 C79 C80 C81 -2.2(11) . . . . ?
C85 P5 C73 C74 176.4(7) . . . . ?
C85 P5 C73 C78 -2.8(8) . . . . ?
C85 P5 C79 C80 -70.8(7) . . . . ?
C85 P5 C79 C84 109.7(6) . . . . ?
C85 C86 C87 C88 -0.4(15) . . . . ?
C86 C85 C90 C89 0.9(14) . . . . ?
C86 C87 C88 C89 -0.2(18) . . . . ?
C87 C88 C89 C90 1.1(19) . . . . ?
C88 C89 C90 C85 -1.5(17) . . . . ?
C90 C85 C86 C87 0.1(12) . . . . ?
C91 P6 C97 C98 85.0(7) . . . . ?
C91 P6 C97 C102 -93.2(8) . . . . ?
C91 P6 C103 C104 35.5(7) . . . . ?
C91 P6 C103 C108 -147.5(7) . . . . ?
C91 C92 C93 C94 -2.2(12) . . . . ?
C92 C91 C96 C95 -0.6(13) . . . . ?
C92 C93 C94 C95 2.0(13) . . . . ?
C93 C94 C95 C96 -1.2(15) . . . . ?
C94 C95 C96 C91 0.5(15) . . . . ?
C96 C91 C92 C93 1.6(12) . . . . ?
C97 P6 C91 C92 -154.3(6) . . . . ?
C97 P6 C91 C96 26.8(8) . . . . ?
C97 P6 C103 C104 -72.5(7) . . . . ?
C97 P6 C103 C108 104.5(7) . . . . ?
C97 C98 C99 C100 -3.0(15) . . . . ?
C98 C97 C102 C101 -2.5(14) . . . . ?
C98 C99 C100 C101 0.8(17) . . . . ?
C99 C100 C101 C102 0.5(17) . . . . ?
C100 C101 C102 C97 0.4(16) . . . . ?
C102 C97 C98 C99 3.8(12) . . . . ?
C103 P6 C91 C92 95.5(6) . . . . ?
C103 P6 C91 C96 -83.5(7) . . . . ?
C103 P6 C97 C98 -166.0(6) . . . . ?
C103 P6 C97 C102 15.8(8) . . . . ?
C103 C104 C105 C106 -3.0(15) . . . . ?
C104 C103 C108 C107 -0.6(14) . . . . ?
C104 C105 C106 C107 3.0(18) . . . . ?
C105 C106 C107 C108 -1.8(19) . . . . ?
C106 C107 C108 C103 0.6(18) . . . . ?
C108 C103 C104 C105 1.8(13) . . . . ?
C109 P7 C115 C116 75.5(6) . . . . ?
C109 P7 C115 C120 -105.3(7) . . . . ?
C109 P7 C121 C122 -134.8(6) . . . . ?
C109 P7 C121 C126 46.7(8) . . . . ?
C109 C110 C111 C112 -0.8(12) . . . . ?
C110 C109 C114 C113 -1.9(12) . . . . ?
C110 C111 C112 C113 -0.6(13) . . . . ?
C111 C112 C113 C114 0.7(14) . . . . ?
C112 C113 C114 C109 0.6(14) . . . . ?
C114 C109 C110 C111 2.1(11) . . . . ?
C115 P7 C109 C110 -138.4(6) . . . . ?
C115 P7 C109 C114 42.5(7) . . . . ?
C115 P7 C121 C122 115.8(6) . . . . ?
C115 P7 C121 C126 -62.6(8) . . . . ?
C115 C116 C117 C118 0.1(13) . . . . ?
C116 C115 C120 C119 -0.2(12) . . . . ?
C116 C117 C118 C119 -1.0(15) . . . . ?
C117 C118 C119 C120 1.4(16) . . . . ?
C118 C119 C120 C115 -0.7(15) . . . . ?
C120 C115 C116 C117 0.5(12) . . . . ?
C121 P7 C109 C110 108.3(6) . . . . ?
C121 P7 C109 C114 -70.8(7) . . . . ?
C121 P7 C115 C116 -173.9(6) . . . . ?
C121 P7 C115 C120 5.3(8) . . . . ?
C121 C122 C123 C124 0.3(13) . . . . ?
C122 C121 C126 C125 -0.6(14) . . . . ?
C122 C123 C124 C125 -0.8(15) . . . . ?
C123 C124 C125 C126 0.5(18) . . . . ?
C124 C125 C126 C121 0.1(17) . . . . ?
C126 C121 C122 C123 0.3(12) . . . . ?
