# Electronic Supplementary Material (ESI) for Nanoscale.
# This journal is © The Royal Society of Chemistry 2019

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_1_a
_database_code_depnum_ccdc_archive 'CCDC 1892178'
_audit_update_record             
;
2019-01-21 deposited with the CCDC.	2019-03-11 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2016/6
_shelx_SHELXL_version_number     2016/6
_chemical_name_systematic        ?
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Bi3 Cl16 Rb7'
_chemical_formula_weight         1792.43

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      trigonal
_space_group_IT_number           163
_space_group_name_H-M_alt        'P -3 1 c'
_space_group_name_Hall           '-P 3 2c'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-y, -x, -z+1/2'
'x, x-y, -z+1/2'
'-x+y, y, -z+1/2'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'y, x, z-1/2'
'-x, -x+y, z-1/2'
'x-y, -y, z-1/2'

_cell_length_a                   7.5561(3)
_cell_length_b                   7.5561(3)
_cell_length_c                   34.3002(16)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_volume                     1695.99(16)
_cell_formula_units_Z            2
_cell_measurement_temperature    273(2)
_cell_measurement_reflns_used    1172
_cell_measurement_theta_min      3.11
_cell_measurement_theta_max      26.32

_exptl_crystal_description       bulk
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_density_diffrn    3.510
_exptl_crystal_F_000             1560
_exptl_transmission_factor_min   0.0027
_exptl_transmission_factor_max   0.0195
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.1
_exptl_absorpt_coefficient_mu    26.763
_shelx_estimated_absorpt_T_min   0.0027
_shelx_estimated_absorpt_T_max   0.0195
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.0027
_exptl_absorpt_correction_T_max  0.0195
_exptl_absorpt_process_details   'SADABS 2014/5'
_exptl_absorpt_special_details   ?
_diffrn_ambient_temperature      273(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   'fine-focus sealed tube'
_diffrn_measurement_device_type  'Bruker D8 VENTURE'
_diffrn_measurement_method       dtprofit.ref
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            16424
_diffrn_reflns_av_unetI/netI     0.0247
_diffrn_reflns_av_R_equivalents  0.0604
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_l_min       -42
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_theta_min         3.113
_diffrn_reflns_theta_max         26.316
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total             1172
_reflns_number_gt                1079
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       'Bruker APEX2(Bruker AXS Inc., 2015)'
_computing_cell_refinement       'Bruker APEX2(Bruker AXS Inc., 2015)'
_computing_data_reduction        'Bruker APEX2(Bruker AXS Inc., 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_molecular_graphics    'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_publication_material  'SHELXL-2016/6 (Sheldrick, 2016)'
_refine_special_details          ?
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0476P)²+27.0489P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    undef
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_extinction_coef       0.0042(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_number_reflns         1172
_refine_ls_number_parameters     84
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0469
_refine_ls_R_factor_gt           0.0432
_refine_ls_wR_factor_ref         0.1081
_refine_ls_wR_factor_gt          0.1053
_refine_ls_goodness_of_fit_ref   1.065
_refine_ls_restrained_S_all      1.065
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Bi1 Bi 0.000000 0.000000 0.500000 0.0415(3) Uani 1 6 d S T P . .
Cl1 Cl 0.3330(6) 0.2030(9) 0.45506(15) 0.1093(17) Uani 1 1 d . . . . .
Bi2 Bi 0.333333 0.666667 0.18448(2) 0.0351(3) Uani 1 3 d S T P . .
Cl2 Cl 0.6155(16) 0.8077(8) 0.250000 0.047(3) Uani 0.3333 2 d S T P A .
Cl3 Cl 0.0525(17) 0.5263(8) 0.250000 0.057(3) Uani 0.3333 2 d S T P A .
Cl4 Cl 0.3493(12) 1.0321(11) 0.1851(2) 0.0420(15) Uani 0.3333 1 d . . P A -1
Cl5 Cl 0.3491(12) 0.3152(11) 0.1844(2) 0.0440(16) Uani 0.3333 1 d . . P A -1
Cl6 Cl 0.0834(15) 0.5392(16) 0.1271(3) 0.063(2) Uani 0.3333 1 d . . P A -1
Cl7 Cl 0.6307(15) 0.8152(15) 0.1359(4) 0.071(3) Uani 0.3333 1 d . . P A -1
Rb1 Rb 0.000000 0.000000 0.250000 0.0460(8) Uani 0.6667 6 d S T P . .
Rb2 Rb 0.333333 0.666667 0.46475(7) 0.0701(6) Uani 1 3 d S T P . .
Rb3 Rb 0.000000 0.000000 0.37815(7) 0.0493(6) Uani 0.6667 3 d S T P . .
Rb4 Rb 0.5755(5) 0.2871(5) 0.38461(9) 0.0433(7) Uani 0.3333 1 d . . P . .
Rb5 Rb -0.2804(3) 0.2804(3) 0.250000 0.0427(9) Uani 0.3333 2 d S T P A .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Bi1 Cl1 2.684(4) 9_556 ?
Bi1 Cl1 2.684(4) 3 ?
Bi1 Cl1 2.684(4) 8_556 ?
Bi1 Cl1 2.684(4) 2 ?
Bi1 Cl1 2.684(4) 7_556 ?
Bi1 Cl1 2.684(4) . ?
Bi1 Rb3 4.180(3) . ?
Bi1 Rb3 4.180(3) 7_556 ?
Bi1 Rb2 4.5269(7) 7_666 ?
Bi1 Rb2 4.5269(7) 1_445 ?
Bi1 Rb2 4.5269(7) 7_556 ?
Bi1 Rb2 4.5270(7) . ?
Cl1 Rb4 2.904(6) . ?
Cl1 Rb3 3.433(5) . ?
Cl1 Rb4 3.469(5) 3_665 ?
Cl1 Rb2 3.518(6) . ?
Cl1 Rb2 3.523(5) 7_666 ?
Cl1 Rb4 3.555(6) 2_655 ?
Bi2 Cl6 2.560(8) . ?
Bi2 Cl7 2.561(9) . ?
Bi2 Cl4 2.703(7) . ?
Bi2 Cl5 2.717(7) . ?
Bi2 Cl3 2.903(7) 2_665 ?
Bi2 Cl3 2.903(7) . ?
Bi2 Cl3 2.903(7) 3_565 ?
Bi2 Cl2 2.908(7) . ?
Bi2 Cl2 2.908(7) 2_665 ?
Bi2 Cl2 2.908(7) 3_565 ?
Cl2 Cl3 1.842(8) 2_665 ?
Cl2 Cl3 1.842(8) 3_565 ?
Cl2 Rb1 2.516(11) 1_665 ?
Cl2 Rb5 3.250(4) 2_665 ?
Cl2 Rb5 3.250(4) 1_665 ?
Cl2 Rb5 3.7950(11) 3 ?
Cl2 Rb5 3.7949(11) 3_565 ?
Cl3 Rb5 2.260(11) 2_565 ?
Cl3 Rb5 2.260(11) . ?
Cl3 Rb5 3.218(12) 3_455 ?
Cl3 Rb1 3.7937(10) 1_565 ?
Cl3 Rb1 3.7937(10) . ?
Cl5 Rb1 3.377(7) . ?
Rb1 Rb5 3.670(4) 3 ?
Rb1 Rb5 3.670(4) 2 ?
Rb1 Rb5 3.670(4) . ?
Rb2 Rb4 4.930(4) 2 ?
Rb2 Rb4 4.930(4) 1_565 ?
Rb2 Rb4 4.930(4) 3_665 ?
Rb3 Rb4 3.773(3) 3 ?
Rb3 Rb4 3.773(3) 2 ?
Rb3 Rb4 3.773(3) . ?
Rb3 Rb4 4.691(3) 3_665 ?
Rb3 Rb4 4.691(3) 2_545 ?
Rb3 Rb4 4.691(3) 1_455 ?
Rb3 Rb4 4.698(3) 2_655 ?
Rb4 Rb4 1.033(5) 3_665 ?
Rb4 Rb4 1.033(5) 2_655 ?
Rb4 Rb5 4.618(3) 3 ?
Rb4 Rb5 4.750(3) 1_655 ?
Rb4 Rb5 4.751(3) 2_665 ?
Rb5 Rb5 1.200(7) 3_455 ?
Rb5 Rb5 1.200(7) 2_565 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Bi1 Cl1 180.00(12) 9_556 3 ?
Cl1 Bi1 Cl1 90.29(14) 9_556 8_556 ?
Cl1 Bi1 Cl1 89.71(14) 3 8_556 ?
Cl1 Bi1 Cl1 89.71(14) 9_556 2 ?
Cl1 Bi1 Cl1 90.29(14) 3 2 ?
Cl1 Bi1 Cl1 180.00(18) 8_556 2 ?
Cl1 Bi1 Cl1 90.29(14) 9_556 7_556 ?
Cl1 Bi1 Cl1 89.71(14) 3 7_556 ?
Cl1 Bi1 Cl1 90.29(14) 8_556 7_556 ?
Cl1 Bi1 Cl1 89.71(14) 2 7_556 ?
Cl1 Bi1 Cl1 89.71(14) 9_556 . ?
Cl1 Bi1 Cl1 90.29(14) 3 . ?
Cl1 Bi1 Cl1 89.71(14) 8_556 . ?
Cl1 Bi1 Cl1 90.29(14) 2 . ?
Cl1 Bi1 Cl1 180.0 7_556 . ?
Cl1 Bi1 Rb3 125.06(10) 9_556 . ?
Cl1 Bi1 Rb3 54.94(10) 3 . ?
Cl1 Bi1 Rb3 125.06(10) 8_556 . ?
Cl1 Bi1 Rb3 54.94(10) 2 . ?
Cl1 Bi1 Rb3 125.06(10) 7_556 . ?
Cl1 Bi1 Rb3 54.94(10) . . ?
Cl1 Bi1 Rb3 54.94(10) 9_556 7_556 ?
Cl1 Bi1 Rb3 125.06(10) 3 7_556 ?
Cl1 Bi1 Rb3 54.94(10) 8_556 7_556 ?
Cl1 Bi1 Rb3 125.06(10) 2 7_556 ?
Cl1 Bi1 Rb3 54.94(10) 7_556 7_556 ?
Cl1 Bi1 Rb3 125.06(10) . 7_556 ?
Rb3 Bi1 Rb3 180.0 . 7_556 ?
Cl1 Bi1 Rb2 62.68(14) 9_556 7_666 ?
Cl1 Bi1 Rb2 117.32(14) 3 7_666 ?
Cl1 Bi1 Rb2 50.91(14) 8_556 7_666 ?
Cl1 Bi1 Rb2 129.09(14) 2 7_666 ?
Cl1 Bi1 Rb2 128.99(11) 7_556 7_666 ?
Cl1 Bi1 Rb2 51.01(11) . 7_666 ?
Rb3 Bi1 Rb2 105.49(3) . 7_666 ?
Rb3 Bi1 Rb2 74.51(3) 7_556 7_666 ?
Cl1 Bi1 Rb2 117.32(14) 9_556 1_445 ?
Cl1 Bi1 Rb2 62.68(14) 3 1_445 ?
Cl1 Bi1 Rb2 129.09(14) 8_556 1_445 ?
Cl1 Bi1 Rb2 50.91(14) 2 1_445 ?
Cl1 Bi1 Rb2 51.01(11) 7_556 1_445 ?
Cl1 Bi1 Rb2 128.99(11) . 1_445 ?
Rb3 Bi1 Rb2 74.51(3) . 1_445 ?
Rb3 Bi1 Rb2 105.49(3) 7_556 1_445 ?
Rb2 Bi1 Rb2 180.0 7_666 1_445 ?
Cl1 Bi1 Rb2 128.99(11) 9_556 7_556 ?
Cl1 Bi1 Rb2 51.01(11) 3 7_556 ?
Cl1 Bi1 Rb2 62.68(14) 8_556 7_556 ?
Cl1 Bi1 Rb2 117.32(14) 2 7_556 ?
Cl1 Bi1 Rb2 50.91(14) 7_556 7_556 ?
Cl1 Bi1 Rb2 129.09(14) . 7_556 ?
Rb3 Bi1 Rb2 105.49(3) . 7_556 ?
Rb3 Bi1 Rb2 74.51(3) 7_556 7_556 ?
Rb2 Bi1 Rb2 113.14(2) 7_666 7_556 ?
Rb2 Bi1 Rb2 66.86(2) 1_445 7_556 ?
Cl1 Bi1 Rb2 51.01(11) 9_556 . ?
Cl1 Bi1 Rb2 128.99(11) 3 . ?
Cl1 Bi1 Rb2 117.32(14) 8_556 . ?
Cl1 Bi1 Rb2 62.68(14) 2 . ?
Cl1 Bi1 Rb2 129.09(14) 7_556 . ?
Cl1 Bi1 Rb2 50.91(14) . . ?
Rb3 Bi1 Rb2 74.51(3) . . ?
Rb3 Bi1 Rb2 105.49(3) 7_556 . ?
Rb2 Bi1 Rb2 66.86(2) 7_666 . ?
Rb2 Bi1 Rb2 113.14(2) 1_445 . ?
Rb2 Bi1 Rb2 180.0 7_556 . ?
Bi1 Cl1 Rb4 155.7(2) . . ?
Bi1 Cl1 Rb3 85.28(10) . . ?
Rb4 Cl1 Rb3 72.53(13) . . ?
Bi1 Cl1 Rb4 170.83(18) . 3_665 ?
Rb4 Cl1 Rb4 15.66(9) . 3_665 ?
Rb3 Cl1 Rb4 85.63(13) . 3_665 ?
Bi1 Cl1 Rb2 92.78(15) . . ?
Rb4 Cl1 Rb2 100.05(17) . . ?
Rb3 Cl1 Rb2 98.80(14) . . ?
Rb4 Cl1 Rb2 89.75(14) 3_665 . ?
Bi1 Cl1 Rb2 92.68(14) . 7_666 ?
Rb4 Cl1 Rb2 107.67(13) . 7_666 ?
Rb3 Cl1 Rb2 170.8(2) . 7_666 ?
Rb4 Cl1 Rb2 96.13(11) 3_665 7_666 ?
Rb2 Cl1 Rb2 90.22(13) . 7_666 ?
Bi1 Cl1 Rb4 159.3(2) . 2_655 ?
Rb4 Cl1 Rb4 14.34(8) . 2_655 ?
Rb3 Cl1 Rb4 84.48(13) . 2_655 ?
Rb4 Cl1 Rb4 16.86(8) 3_665 2_655 ?
Rb2 Cl1 Rb4 106.56(15) . 2_655 ?
Rb2 Cl1 Rb4 94.59(11) 7_666 2_655 ?
Cl6 Bi2 Cl7 89.2(4) . . ?
Cl6 Bi2 Cl4 92.2(3) . . ?
Cl7 Bi2 Cl4 88.7(3) . . ?
Cl6 Bi2 Cl5 91.0(3) . . ?
Cl7 Bi2 Cl5 88.3(3) . . ?
Cl4 Bi2 Cl5 175.6(2) . . ?
Cl6 Bi2 Cl3 142.5(3) . 2_665 ?
Cl7 Bi2 Cl3 105.2(3) . 2_665 ?
Cl4 Bi2 Cl3 121.9(2) . 2_665 ?
Cl5 Bi2 Cl3 56.0(2) . 2_665 ?
Cl6 Bi2 Cl3 101.0(3) . . ?
Cl7 Bi2 Cl3 169.8(3) . . ?
Cl4 Bi2 Cl3 91.04(15) . . ?
Cl5 Bi2 Cl3 91.40(16) . . ?
Cl3 Bi2 Cl3 66.5(3) 2_665 . ?
Cl6 Bi2 Cl3 143.3(3) . 3_565 ?
Cl7 Bi2 Cl3 105.3(3) . 3_565 ?
Cl4 Bi2 Cl3 55.5(2) . 3_565 ?
Cl5 Bi2 Cl3 122.4(2) . 3_565 ?
Cl3 Bi2 Cl3 66.5(3) 2_665 3_565 ?
Cl3 Bi2 Cl3 66.5(3) . 3_565 ?
Cl6 Bi2 Cl2 179.5(3) . . ?
Cl7 Bi2 Cl2 91.1(3) . . ?
Cl4 Bi2 Cl2 88.22(15) . . ?
Cl5 Bi2 Cl2 88.64(16) . . ?
Cl3 Bi2 Cl2 36.96(9) 2_665 . ?
Cl3 Bi2 Cl2 78.7(2) . . ?
Cl3 Bi2 Cl2 36.96(9) 3_565 . ?
Cl6 Bi2 Cl2 113.3(3) . 2_665 ?
Cl7 Bi2 Cl2 138.1(2) . 2_665 ?
Cl4 Bi2 Cl2 57.1(2) . 2_665 ?
Cl5 Bi2 Cl2 124.2(2) . 2_665 ?
Cl3 Bi2 Cl2 78.7(2) 2_665 2_665 ?
Cl3 Bi2 Cl2 36.96(9) . 2_665 ?
Cl3 Bi2 Cl2 36.96(9) 3_565 2_665 ?
Cl2 Bi2 Cl2 66.7(3) . 2_665 ?
Cl6 Bi2 Cl2 112.8(3) . 3_565 ?
Cl7 Bi2 Cl2 138.0(2) . 3_565 ?
Cl4 Bi2 Cl2 123.7(2) . 3_565 ?
Cl5 Bi2 Cl2 57.5(2) . 3_565 ?
Cl3 Bi2 Cl2 36.96(9) 2_665 3_565 ?
Cl3 Bi2 Cl2 36.96(9) . 3_565 ?
Cl3 Bi2 Cl2 78.7(2) 3_565 3_565 ?
Cl2 Bi2 Cl2 66.7(3) . 3_565 ?
Cl2 Bi2 Cl2 66.7(3) 2_665 3_565 ?
Cl3 Cl2 Cl3 119.5(9) 2_665 3_565 ?
Cl3 Cl2 Rb1 120.2(4) 2_665 1_665 ?
Cl3 Cl2 Rb1 120.2(4) 3_565 1_665 ?
Cl3 Cl2 Bi2 71.4(3) 2_665 4_665 ?
Cl3 Cl2 Bi2 71.4(3) 3_565 4_665 ?
Rb1 Cl2 Bi2 129.41(16) 1_665 4_665 ?
Cl3 Cl2 Bi2 71.4(3) 2_665 . ?
Cl3 Cl2 Bi2 71.4(3) 3_565 . ?
Rb1 Cl2 Bi2 129.41(16) 1_665 . ?
Bi2 Cl2 Bi2 101.2(3) 4_665 . ?
Cl3 Cl2 Rb5 42.3(3) 2_665 2_665 ?
Cl3 Cl2 Rb5 161.9(6) 3_565 2_665 ?
Rb1 Cl2 Rb5 77.90(19) 1_665 2_665 ?
Bi2 Cl2 Rb5 97.65(10) 4_665 2_665 ?
Bi2 Cl2 Rb5 97.65(10) . 2_665 ?
Cl3 Cl2 Rb5 161.9(6) 2_665 1_665 ?
Cl3 Cl2 Rb5 42.3(3) 3_565 1_665 ?
Rb1 Cl2 Rb5 77.90(19) 1_665 1_665 ?
Bi2 Cl2 Rb5 97.65(10) 4_665 1_665 ?
Bi2 Cl2 Rb5 97.65(10) . 1_665 ?
Rb5 Cl2 Rb5 155.8(4) 2_665 1_665 ?
Cl3 Cl2 Rb5 24.8(3) 2_665 3 ?
Cl3 Cl2 Rb5 144.4(6) 3_565 3 ?
Rb1 Cl2 Rb5 95.41(17) 1_665 3 ?
Bi2 Cl2 Rb5 86.57(12) 4_665 3 ?
Bi2 Cl2 Rb5 86.57(12) . 3 ?
Rb5 Cl2 Rb5 17.51(12) 2_665 3 ?
Rb5 Cl2 Rb5 173.3(3) 1_665 3 ?
Cl3 Cl2 Rb5 144.4(6) 2_665 3_565 ?
Cl3 Cl2 Rb5 24.8(3) 3_565 3_565 ?
Rb1 Cl2 Rb5 95.41(17) 1_665 3_565 ?
Bi2 Cl2 Rb5 86.57(12) 4_665 3_565 ?
Bi2 Cl2 Rb5 86.57(12) . 3_565 ?
Rb5 Cl2 Rb5 173.3(3) 2_665 3_565 ?
Rb5 Cl2 Rb5 17.51(12) 1_665 3_565 ?
Rb5 Cl2 Rb5 169.2(3) 3 3_565 ?
Cl2 Cl3 Cl2 120.5(9) 2_665 3_565 ?
Cl2 Cl3 Rb5 104.4(4) 2_665 2_565 ?
Cl2 Cl3 Rb5 135.2(5) 3_565 2_565 ?
Cl2 Cl3 Rb5 135.2(5) 2_665 . ?
Cl2 Cl3 Rb5 104.4(4) 3_565 . ?
Rb5 Cl3 Rb5 30.8(3) 2_565 . ?
Cl2 Cl3 Bi2 71.7(3) 2_665 4_665 ?
Cl2 Cl3 Bi2 71.7(3) 3_565 4_665 ?
Rb5 Cl3 Bi2 127.61(14) 2_565 4_665 ?
Rb5 Cl3 Bi2 127.61(14) . 4_665 ?
Cl2 Cl3 Bi2 71.7(3) 2_665 . ?
Cl2 Cl3 Bi2 71.7(3) 3_565 . ?
Rb5 Cl3 Bi2 127.61(14) 2_565 . ?
Rb5 Cl3 Bi2 127.61(14) . . ?
Bi2 Cl3 Bi2 101.5(3) 4_665 . ?
Cl2 Cl3 Rb5 119.8(4) 2_665 3_455 ?
Cl2 Cl3 Rb5 119.8(4) 3_565 3_455 ?
Rb5 Cl3 Rb5 15.40(13) 2_565 3_455 ?
Rb5 Cl3 Rb5 15.40(13) . 3_455 ?
Bi2 Cl3 Rb5 129.27(17) 4_665 3_455 ?
Bi2 Cl3 Rb5 129.27(17) . 3_455 ?
Cl2 Cl3 Rb1 35.0(3) 2_665 1_565 ?
Cl2 Cl3 Rb1 155.4(6) 3_565 1_565 ?
Rb5 Cl3 Rb1 69.41(14) 2_565 1_565 ?
Rb5 Cl3 Rb1 100.2(3) . 1_565 ?
Bi2 Cl3 Rb1 93.29(9) 4_665 1_565 ?
Bi2 Cl3 Rb1 93.29(9) . 1_565 ?
Rb5 Cl3 Rb1 84.80(16) 3_455 1_565 ?
Cl2 Cl3 Rb1 155.4(6) 2_665 . ?
Cl2 Cl3 Rb1 35.0(3) 3_565 . ?
Rb5 Cl3 Rb1 100.2(3) 2_565 . ?
Rb5 Cl3 Rb1 69.41(14) . . ?
Bi2 Cl3 Rb1 93.29(9) 4_665 . ?
Bi2 Cl3 Rb1 93.29(9) . . ?
Rb5 Cl3 Rb1 84.80(16) 3_455 . ?
Rb1 Cl3 Rb1 169.6(3) 1_565 . ?
Bi2 Cl5 Rb1 106.8(2) . . ?
Cl2 Rb1 Cl2 120.000(1) 3_565 1_445 ?
Cl2 Rb1 Cl2 120.000(1) 3_565 2_655 ?
Cl2 Rb1 Cl2 120.000(1) 1_445 2_655 ?
Cl2 Rb1 Cl5 52.35(13) 3_565 . ?
Cl2 Rb1 Cl5 132.56(13) 1_445 . ?
Cl2 Rb1 Cl5 86.24(13) 2_655 . ?
Cl2 Rb1 Rb5 60.000(1) 3_565 3 ?
Cl2 Rb1 Rb5 180.0 1_445 3 ?
Cl2 Rb1 Rb5 60.0 2_655 3 ?
Cl5 Rb1 Rb5 47.44(13) . 3 ?
Cl2 Rb1 Rb5 180.0 3_565 2 ?
Cl2 Rb1 Rb5 60.000(1) 1_445 2 ?
Cl2 Rb1 Rb5 60.0 2_655 2 ?
Cl5 Rb1 Rb5 127.65(12) . 2 ?
Rb5 Rb1 Rb5 120.0 3 2 ?
Cl2 Rb1 Rb5 60.000(1) 3_565 . ?
Cl2 Rb1 Rb5 60.0 1_445 . ?
Cl2 Rb1 Rb5 180.0 2_655 . ?
Cl5 Rb1 Rb5 93.76(13) . . ?
Rb5 Rb1 Rb5 120.0 3 . ?
Rb5 Rb1 Rb5 120.0 2 . ?
Cl2 Rb1 Cl3 95.20(17) 3_565 3 ?
Cl2 Rb1 Cl3 144.80(17) 1_445 3 ?
Cl2 Rb1 Cl3 24.80(17) 2_655 3 ?
Cl5 Rb1 Cl3 68.21(17) . 3 ?
Rb5 Rb1 Cl3 35.20(17) 3 3 ?
Rb5 Rb1 Cl3 84.80(17) 2 3 ?
Rb5 Rb1 Cl3 155.20(17) . 3 ?
Cl2 Rb1 Cl3 144.80(17) 3_565 1_545 ?
Cl2 Rb1 Cl3 95.20(17) 1_445 1_545 ?
Cl2 Rb1 Cl3 24.80(17) 2_655 1_545 ?
Cl5 Rb1 Cl3 104.61(17) . 1_545 ?
Rb5 Rb1 Cl3 84.80(17) 3 1_545 ?
Rb5 Rb1 Cl3 35.20(17) 2 1_545 ?
Rb5 Rb1 Cl3 155.20(17) . 1_545 ?
Cl3 Rb1 Cl3 49.6(3) 3 1_545 ?
Cl2 Rb1 Cl3 24.80(17) 3_565 2_665 ?
Cl2 Rb1 Cl3 144.80(17) 1_445 2_665 ?
Cl2 Rb1 Cl3 95.20(17) 2_655 2_665 ?
Cl5 Rb1 Cl3 42.76(13) . 2_665 ?
Rb5 Rb1 Cl3 35.20(17) 3 2_665 ?
Rb5 Rb1 Cl3 155.20(17) 2 2_665 ?
Rb5 Rb1 Cl3 84.80(17) . 2_665 ?
Cl3 Rb1 Cl3 70.4(3) 3 2_665 ?
Cl3 Rb1 Cl3 120.0 1_545 2_665 ?
Cl2 Rb1 Cl3 144.80(17) 3_565 2 ?
Cl2 Rb1 Cl3 24.80(17) 1_445 2 ?
Cl2 Rb1 Cl3 95.20(17) 2_655 2 ?
Cl5 Rb1 Cl3 138.25(13) . 2 ?
Rb5 Rb1 Cl3 155.20(17) 3 2 ?
Rb5 Rb1 Cl3 35.20(17) 2 2 ?
Rb5 Rb1 Cl3 84.80(17) . 2 ?
Cl3 Rb1 Cl3 120.0 3 2 ?
Cl3 Rb1 Cl3 70.4(3) 1_545 2 ?
Cl3 Rb1 Cl3 169.6(3) 2_665 2 ?
Cl2 Rb1 Cl3 24.80(16) 3_565 . ?
Cl2 Rb1 Cl3 95.20(16) 1_445 . ?
Cl2 Rb1 Cl3 144.80(17) 2_655 . ?
Cl5 Rb1 Cl3 67.99(17) . . ?
Rb5 Rb1 Cl3 84.80(17) 3 . ?
Rb5 Rb1 Cl3 155.20(17) 2 . ?
Rb5 Rb1 Cl3 35.20(17) . . ?
Cl3 Rb1 Cl3 120.0 3 . ?
Cl3 Rb1 Cl3 169.6(3) 1_545 . ?
Cl3 Rb1 Cl3 49.6(3) 2_665 . ?
Cl3 Rb1 Cl3 120.0 2 . ?
Cl1 Rb2 Cl1 119.12(3) 3_565 2_665 ?
Cl1 Rb2 Cl1 119.12(3) 3_565 . ?
Cl1 Rb2 Cl1 119.12(3) 2_665 . ?
Cl1 Rb2 Cl1 65.06(15) 3_565 8_566 ?
Cl1 Rb2 Cl1 89.78(13) 2_665 8_566 ?
Cl1 Rb2 Cl1 130.32(10) . 8_566 ?
Cl1 Rb2 Cl1 130.32(10) 3_565 7_666 ?
Cl1 Rb2 Cl1 65.06(15) 2_665 7_666 ?
Cl1 Rb2 Cl1 89.78(13) . 7_666 ?
Cl1 Rb2 Cl1 65.51(12) 8_566 7_666 ?
Cl1 Rb2 Cl1 89.78(13) 3_565 9_556 ?
Cl1 Rb2 Cl1 130.32(10) 2_665 9_556 ?
Cl1 Rb2 Cl1 65.06(15) . 9_556 ?
Cl1 Rb2 Cl1 65.51(12) 8_566 9_556 ?
Cl1 Rb2 Cl1 65.51(12) 7_666 9_556 ?
Cl1 Rb2 Bi1 36.31(7) 3_565 1_565 ?
Cl1 Rb2 Bi1 91.48(6) 2_665 1_565 ?
Cl1 Rb2 Bi1 148.85(7) . 1_565 ?
Cl1 Rb2 Bi1 36.31(7) 8_566 1_565 ?
Cl1 Rb2 Bi1 98.94(10) 7_666 1_565 ?
Cl1 Rb2 Bi1 91.42(10) 9_556 1_565 ?
Cl1 Rb2 Bi1 148.85(7) 3_565 1_665 ?
Cl1 Rb2 Bi1 36.31(7) 2_665 1_665 ?
Cl1 Rb2 Bi1 91.48(6) . 1_665 ?
Cl1 Rb2 Bi1 91.42(10) 8_566 1_665 ?
Cl1 Rb2 Bi1 36.31(7) 7_666 1_665 ?
Cl1 Rb2 Bi1 98.94(10) 9_556 1_665 ?
Bi1 Rb2 Bi1 113.14(2) 1_565 1_665 ?
Cl1 Rb2 Bi1 91.48(6) 3_565 . ?
Cl1 Rb2 Bi1 148.85(7) 2_665 . ?
Cl1 Rb2 Bi1 36.31(7) . . ?
Cl1 Rb2 Bi1 98.94(10) 8_566 . ?
Cl1 Rb2 Bi1 91.42(10) 7_666 . ?
Cl1 Rb2 Bi1 36.31(7) 9_556 . ?
Bi1 Rb2 Bi1 113.14(2) 1_565 . ?
Bi1 Rb2 Bi1 113.14(2) 1_665 . ?
Cl1 Rb2 Rb4 44.72(8) 3_565 2 ?
Cl1 Rb2 Rb4 135.19(10) 2_665 2 ?
Cl1 Rb2 Rb4 80.97(8) . 2 ?
Cl1 Rb2 Rb4 107.22(10) 8_566 2 ?
Cl1 Rb2 Rb4 159.66(10) 7_666 2 ?
Cl1 Rb2 Rb4 94.15(10) 9_556 2 ?
Bi1 Rb2 Rb4 80.74(4) 1_565 2 ?
Bi1 Rb2 Rb4 160.49(6) 1_665 2 ?
Bi1 Rb2 Rb4 70.43(4) . 2 ?
Cl1 Rb2 Rb4 80.97(8) 3_565 1_565 ?
Cl1 Rb2 Rb4 44.72(8) 2_665 1_565 ?
Cl1 Rb2 Rb4 135.19(10) . 1_565 ?
Cl1 Rb2 Rb4 94.15(9) 8_566 1_565 ?
Cl1 Rb2 Rb4 107.22(10) 7_666 1_565 ?
Cl1 Rb2 Rb4 159.66(10) 9_556 1_565 ?
Bi1 Rb2 Rb4 70.43(4) 1_565 1_565 ?
Bi1 Rb2 Rb4 80.74(4) 1_665 1_565 ?
Bi1 Rb2 Rb4 160.49(6) . 1_565 ?
Rb4 Rb2 Rb4 91.93(6) 2 1_565 ?
Cl1 Rb2 Rb4 135.19(10) 3_565 3_665 ?
Cl1 Rb2 Rb4 80.97(8) 2_665 3_665 ?
Cl1 Rb2 Rb4 44.72(8) . 3_665 ?
Cl1 Rb2 Rb4 159.66(10) 8_566 3_665 ?
Cl1 Rb2 Rb4 94.15(9) 7_666 3_665 ?
Cl1 Rb2 Rb4 107.22(10) 9_556 3_665 ?
Bi1 Rb2 Rb4 160.49(6) 1_565 3_665 ?
Bi1 Rb2 Rb4 70.43(4) 1_665 3_665 ?
Bi1 Rb2 Rb4 80.74(4) . 3_665 ?
Rb4 Rb2 Rb4 91.93(6) 2 3_665 ?
Rb4 Rb2 Rb4 91.93(6) 1_565 3_665 ?
Cl1 Rb3 Cl1 67.31(12) 2 3 ?
Cl1 Rb3 Cl1 67.31(12) 2 . ?
Cl1 Rb3 Cl1 67.31(12) 3 . ?
Cl1 Rb3 Rb4 101.62(12) 2 3 ?
Cl1 Rb3 Rb4 47.25(9) 3 3 ?
Cl1 Rb3 Rb4 109.99(12) . 3 ?
Cl1 Rb3 Rb4 47.25(9) 2 2 ?
Cl1 Rb3 Rb4 109.99(12) 3 2 ?
Cl1 Rb3 Rb4 101.62(12) . 2 ?
Rb4 Rb3 Rb4 119.658(13) 3 2 ?
Cl1 Rb3 Rb4 109.99(12) 2 . ?
Cl1 Rb3 Rb4 101.62(12) 3 . ?
Cl1 Rb3 Rb4 47.25(9) . . ?
Rb4 Rb3 Rb4 119.658(12) 3 . ?
Rb4 Rb3 Rb4 119.657(13) 2 . ?
Cl1 Rb3 Bi1 39.78(8) 2 . ?
Cl1 Rb3 Bi1 39.78(8) 3 . ?
Cl1 Rb3 Bi1 39.78(8) . . ?
Rb4 Rb3 Bi1 86.63(6) 3 . ?
Rb4 Rb3 Bi1 86.63(6) 2 . ?
Rb4 Rb3 Bi1 86.63(6) . . ?
Cl1 Rb3 Rb1 140.22(8) 2 . ?
Cl1 Rb3 Rb1 140.22(8) 3 . ?
Cl1 Rb3 Rb1 140.22(8) . . ?
Rb4 Rb3 Rb1 93.37(6) 3 . ?
Rb4 Rb3 Rb1 93.37(6) 2 . ?
Rb4 Rb3 Rb1 93.37(6) . . ?
Bi1 Rb3 Rb1 180.0 . . ?
Cl1 Rb3 Rb4 106.95(12) 2 3_665 ?
Cl1 Rb3 Rb4 105.96(11) 3 3_665 ?
Cl1 Rb3 Rb4 47.51(8) . 3_665 ?
Rb4 Rb3 Rb4 126.11(8) 3 3_665 ?
Rb4 Rb3 Rb4 113.32(8) 2 3_665 ?
Rb4 Rb3 Rb4 6.46(8) . 3_665 ?
Bi1 Rb3 Rb4 87.29(5) . 3_665 ?
Rb1 Rb3 Rb4 92.71(5) . 3_665 ?
Cl1 Rb3 Rb4 105.96(11) 2 2_545 ?
Cl1 Rb3 Rb4 47.51(8) 3 2_545 ?
Cl1 Rb3 Rb4 106.95(11) . 2_545 ?
Rb4 Rb3 Rb4 6.46(8) 3 2_545 ?
Rb4 Rb3 Rb4 126.11(8) 2 2_545 ?
Rb4 Rb3 Rb4 113.32(8) . 2_545 ?
Bi1 Rb3 Rb4 87.29(5) . 2_545 ?
Rb1 Rb3 Rb4 92.71(5) . 2_545 ?
Rb4 Rb3 Rb4 119.778(8) 3_665 2_545 ?
Cl1 Rb3 Rb4 47.51(8) 2 1_455 ?
Cl1 Rb3 Rb4 106.95(11) 3 1_455 ?
Cl1 Rb3 Rb4 105.96(11) . 1_455 ?
Rb4 Rb3 Rb4 113.32(8) 3 1_455 ?
Rb4 Rb3 Rb4 6.46(8) 2 1_455 ?
Rb4 Rb3 Rb4 126.11(8) . 1_455 ?
Bi1 Rb3 Rb4 87.29(5) . 1_455 ?
Rb1 Rb3 Rb4 92.71(5) . 1_455 ?
Rb4 Rb3 Rb4 119.778(8) 3_665 1_455 ?
Rb4 Rb3 Rb4 119.778(8) 2_545 1_455 ?
Cl1 Rb3 Rb4 113.81(11) 2 2_655 ?
Cl1 Rb3 Rb4 98.35(11) 3 2_655 ?
Cl1 Rb3 Rb4 48.87(8) . 2_655 ?
Rb4 Rb3 Rb4 113.54(8) 3 2_655 ?
Rb4 Rb3 Rb4 125.90(8) 2 2_655 ?
Rb4 Rb3 Rb4 6.24(8) . 2_655 ?
Bi1 Rb3 Rb4 87.29(5) . 2_655 ?
Rb1 Rb3 Rb4 92.71(5) . 2_655 ?
Rb4 Rb3 Rb4 12.63(6) 3_665 2_655 ?
Rb4 Rb3 Rb4 107.18(6) 2_545 2_655 ?
Rb4 Rb3 Rb4 132.36(6) 1_455 2_655 ?
Rb4 Rb4 Rb4 60.001(2) 3_665 2_655 ?
Rb4 Rb4 Cl1 115.0(2) 3_665 . ?
Rb4 Rb4 Cl1 121.53(15) 2_655 . ?
Rb4 Rb4 Cl1 86.3(2) 3_665 2_655 ?
Rb4 Rb4 Cl1 49.37(17) 2_655 2_655 ?
Cl1 Rb4 Cl1 72.85(15) . 2_655 ?
Rb4 Rb4 Cl1 44.12(13) 3_665 3_665 ?
Rb4 Rb4 Cl1 76.8(2) 2_655 3_665 ?
Cl1 Rb4 Cl1 71.51(15) . 3_665 ?
Cl1 Rb4 Cl1 65.71(12) 2_655 3_665 ?
Rb4 Rb4 Rb3 149.3(4) 3_665 . ?
Rb4 Rb4 Rb3 150.4(4) 2_655 . ?
Cl1 Rb4 Rb3 60.22(11) . . ?
Cl1 Rb4 Rb3 117.30(13) 2_655 . ?
Cl1 Rb4 Rb3 125.48(14) 3_665 . ?
Rb4 Rb4 Rb5 91.01(6) 3_665 3 ?
Rb4 Rb4 Rb5 91.08(6) 2_655 3 ?
Cl1 Rb4 Rb5 145.11(13) . 3 ?
Cl1 Rb4 Rb5 134.89(11) 2_655 3 ?
Cl1 Rb4 Rb5 133.65(12) 3_665 3 ?
Rb3 Rb4 Rb5 85.44(9) . 3 ?
Rb4 Rb4 Rb3 84.1(3) 3_665 1_655 ?
Rb4 Rb4 Rb3 24.2(3) 2_655 1_655 ?
Cl1 Rb4 Rb3 116.14(15) . 1_655 ?
Cl1 Rb4 Rb3 46.86(9) 2_655 1_655 ?
Cl1 Rb4 Rb3 96.25(12) 3_665 1_655 ?
Rb3 Rb4 Rb3 126.11(8) . 1_655 ?
Rb5 Rb4 Rb3 88.05(7) 3 1_655 ?
Rb4 Rb4 Rb3 23.4(3) 3_665 1_665 ?
Rb4 Rb4 Rb3 83.3(3) 2_655 1_665 ?
Cl1 Rb4 Rb3 106.53(15) . 1_665 ?
Cl1 Rb4 Rb3 104.81(13) 2_655 1_665 ?
Cl1 Rb4 Rb3 46.66(9) 3_665 1_665 ?
Rb3 Rb4 Rb3 125.90(8) . 1_665 ?
Rb5 Rb4 Rb3 87.95(7) 3 1_665 ?
Rb3 Rb4 Rb3 107.18(6) 1_655 1_665 ?
Rb4 Rb4 Rb5 83.83(5) 3_665 1_655 ?
Rb4 Rb4 Rb5 76.45(6) 2_655 1_655 ?
Cl1 Rb4 Rb5 158.32(13) . 1_655 ?
Cl1 Rb4 Rb5 121.40(12) 2_655 1_655 ?
Cl1 Rb4 Rb5 127.95(12) 3_665 1_655 ?
Rb3 Rb4 Rb5 98.12(8) . 1_655 ?
Rb5 Rb4 Rb5 14.63(9) 3 1_655 ?
Rb3 Rb4 Rb5 74.68(8) 1_655 1_655 ?
Rb3 Rb4 Rb5 86.43(6) 1_665 1_655 ?
Rb4 Rb4 Rb5 76.38(6) 3_665 2_665 ?
Rb4 Rb4 Rb5 83.70(6) 2_655 2_665 ?
Cl1 Rb4 Rb5 154.77(14) . 2_665 ?
Cl1 Rb4 Rb5 131.93(11) 2_655 2_665 ?
Cl1 Rb4 Rb5 119.34(12) 3_665 2_665 ?
Rb3 Rb4 Rb5 98.10(8) . 2_665 ?
Rb5 Rb4 Rb5 14.63(9) 3 2_665 ?
Rb3 Rb4 Rb5 86.50(6) 1_655 2_665 ?
Rb3 Rb4 Rb5 74.59(8) 1_665 2_665 ?
Rb5 Rb4 Rb5 14.51(9) 1_655 2_665 ?
Rb4 Rb4 Rb2 131.7(2) 3_665 1_545 ?
Rb4 Rb4 Rb2 84.4(3) 2_655 1_545 ?
Cl1 Rb4 Rb2 55.56(14) . 1_545 ?
Cl1 Rb4 Rb2 45.52(11) 2_655 1_545 ?
Cl1 Rb4 Rb2 100.00(10) 3_665 1_545 ?
Rb3 Rb4 Rb2 73.31(6) . 1_545 ?
Rb5 Rb4 Rb2 123.47(8) 3 1_545 ?
Rb3 Rb4 Rb2 66.49(5) 1_655 1_545 ?
Rb3 Rb4 Rb2 146.37(8) 1_665 1_545 ?
Rb5 Rb4 Rb2 120.66(8) 1_655 1_545 ?
Rb5 Rb4 Rb2 134.67(9) 2_665 1_545 ?
Rb5 Rb5 Rb5 60.001(3) 3_455 2_565 ?
Rb5 Rb5 Cl3 74.60(13) 3_455 3_455 ?
Rb5 Rb5 Cl3 134.60(13) 2_565 3_455 ?
Rb5 Rb5 Cl3 134.61(13) 3_455 . ?
Rb5 Rb5 Cl3 74.60(13) 2_565 . ?
Cl3 Rb5 Cl3 150.8(3) 3_455 . ?
Rb5 Rb5 Cl3 30.001(3) 3_455 2_565 ?
Rb5 Rb5 Cl3 30.001(1) 2_565 2_565 ?
Cl3 Rb5 Cl3 104.60(13) 3_455 2_565 ?
Cl3 Rb5 Cl3 104.60(13) . 2_565 ?
Rb5 Rb5 Cl2 107.9(2) 3_455 1_445 ?
Rb5 Rb5 Cl2 167.9(2) 2_565 1_445 ?
Cl3 Rb5 Cl2 33.3(2) 3_455 1_445 ?
Cl3 Rb5 Cl2 117.5(3) . 1_445 ?
Cl3 Rb5 Cl2 137.9(2) 2_565 1_445 ?
Rb5 Rb5 Cl2 167.9(2) 3_455 3_565 ?
Rb5 Rb5 Cl2 107.9(2) 2_565 3_565 ?
Cl3 Rb5 Cl2 117.5(3) 3_455 3_565 ?
Cl3 Rb5 Cl2 33.3(2) . 3_565 ?
Cl3 Rb5 Cl2 137.9(2) 2_565 3_565 ?
Cl2 Rb5 Cl2 84.2(4) 1_445 3_565 ?
Rb5 Rb5 Rb1 149.999(3) 3_455 . ?
Rb5 Rb5 Rb1 149.999(3) 2_565 . ?
Cl3 Rb5 Rb1 75.40(13) 3_455 . ?
Cl3 Rb5 Rb1 75.40(13) . . ?
Cl3 Rb5 Rb1 180.0 2_565 . ?
Cl2 Rb5 Rb1 42.10(19) 1_445 . ?
Cl2 Rb5 Rb1 42.10(19) 3_565 . ?
Rb5 Rb5 Cl2 114.59(18) 3_455 2_665 ?
Rb5 Rb5 Cl2 54.59(18) 2_565 2_665 ?
Cl3 Rb5 Cl2 170.8(2) 3_455 2_665 ?
Cl3 Rb5 Cl2 20.01(19) . 2_665 ?
Cl3 Rb5 Cl2 84.59(17) 2_565 2_665 ?
Cl2 Rb5 Cl2 137.51(12) 1_445 2_665 ?
Cl2 Rb5 Cl2 53.3(4) 3_565 2_665 ?
Rb1 Rb5 Cl2 95.41(17) . 2_665 ?
Rb5 Rb5 Cl2 54.59(18) 3_455 2 ?
Rb5 Rb5 Cl2 114.59(18) 2_565 2 ?
Cl3 Rb5 Cl2 20.01(19) 3_455 2 ?
Cl3 Rb5 Cl2 170.8(2) . 2 ?
Cl3 Rb5 Cl2 84.59(18) 2_565 2 ?
Cl2 Rb5 Cl2 53.3(4) 1_445 2 ?
Cl2 Rb5 Cl2 137.51(12) 3_565 2 ?
Rb1 Rb5 Cl2 95.41(17) . 2 ?
Cl2 Rb5 Cl2 169.2(3) 2_665 2 ?
Rb5 Rb5 Rb4 88.94(6) 3_455 6 ?
Rb5 Rb5 Rb4 89.00(6) 2_565 6 ?
Cl3 Rb5 Rb4 90.24(4) 3_455 6 ?
Cl3 Rb5 Rb4 90.36(4) . 6 ?
Cl3 Rb5 Rb4 88.81(6) 2_565 6 ?
Cl2 Rb5 Rb4 90.85(5) 1_445 6 ?
Cl2 Rb5 Rb4 90.93(5) 3_565 6 ?
Rb1 Rb5 Rb4 91.19(6) . 6 ?
Cl2 Rb5 Rb4 89.95(4) 2_665 6 ?
Cl2 Rb5 Rb4 89.83(4) 2 6 ?
Rb5 Rb5 Rb4 89.00(6) 3_455 2 ?
Rb5 Rb5 Rb4 88.94(6) 2_565 2 ?
Cl3 Rb5 Rb4 90.36(4) 3_455 2 ?
Cl3 Rb5 Rb4 90.24(4) . 2 ?
Cl3 Rb5 Rb4 88.81(6) 2_565 2 ?
Cl2 Rb5 Rb4 90.93(5) 1_445 2 ?
Cl2 Rb5 Rb4 90.85(5) 3_565 2 ?
Rb1 Rb5 Rb4 91.19(6) . 2 ?
Cl2 Rb5 Rb4 89.83(4) 2_665 2 ?
Cl2 Rb5 Rb4 89.95(4) 2 2 ?
Rb4 Rb5 Rb4 177.61(12) 6 2 ?


_refine_diff_density_max         1.847
_refine_diff_density_min         -1.824
_refine_diff_density_rms         0.206

