Supplementary Material (ESI) for Chemical Communications This journal is © The Royal Society of Chemistry 2002 data_fare _database_code_CSD 180632 #---Eu3(C63H65N13O2)3 (CF3SO3)9 (C2H3N)9 (H2O)2 ---------- --- _audit_creation_date '2001-07-03' _audit_creation_method from_xtal_archive_file_using_CIFIO _audit_update_record '2001-07-03' _audit_conform_dict_name 'cif_core.dic' _audit_conform_dict_version '2.0.1' #--------------------------------------------------------------------------- _journal_coden_Cambridge 182 loop_ _publ_author_name 'Piguet, Claude' 'Bernardinelli, Gerald' 'Bocquet, Bernard' 'Floquet, Sebastien' 'Hopfgartner, Gerard' 'Quali, Nadjet' 'Renaud, Fabien' _publ_requested_journal 'Chem. Commun.' _publ_contact_author_name 'Prof Claude Piguet' _publ_contact_author_address ; Department of Inorganic Chemistry University of Geneva 30 quai E. Ansermet 1211 Geneva 4 1211 Geneva 4 SWITZERLAND ; _publ_contact_author_email 'CLAUDE.PIGUET@CHIAM.UNIGE.CH' _publ_contact_author_phone '41 (22) 702 62 02' _publ_contact_author_fax '41 (22) 702 61 08' _publ_section_title ; The First Self-Assembled Trimetallic Lanthanide Helicate: Different Coordination Sites in Symmetrical Molecular Architectures. ; _chemical_formula_moiety ; Eu3 (C63 H65 N13 O2)3 (C F3 S O3)9 (C2 H3 N)9 (H2 O)2 ; _chemical_formula_sum 'C216 H226 N48 O35 F27 S9 Eu3' _chemical_formula_weight 5312.3 _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1' loop_ _symmetry_equiv_pos_as_xyz +x,+y,+z -x,-y,-z _cell_length_a 14.9286(7) _cell_length_b 21.7201(11) _cell_length_c 39.2254(17) _cell_angle_alpha 96.885(5) _cell_angle_beta 99.428(5) _cell_angle_gamma 104.033(6) _cell_volume 12002.2(11) _cell_formula_units_Z 2 _exptl_crystal_density_diffrn 1.47 _exptl_crystal_density_meas not_measured _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength .71073 _cell_measurement_reflns_used 8004 _cell_measurement_theta_min 3.3 _cell_measurement_theta_max 26 _cell_measurement_temperature 200 _exptl_absorpt_coefficient_mu .95 _exptl_crystal_description plate _exptl_crystal_size_max .35 _exptl_crystal_size_mid .32 _exptl_crystal_size_min .12 _exptl_crystal_colour colorless _diffrn_measurement_device_type 'Stoe Ipds' _diffrn_measurement_method \f _diffrn_detector_area_resol_mean 6 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'XRED; Stoe & Cie, 1999' _exptl_absorpt_correction_T_min .7552 _exptl_absorpt_correction_T_max .8963 _diffrn_reflns_number .131723+06 _reflns_number_total .426770+05 _reflns_number_gt .226160+05 _reflns_threshold_expression 'refl observed if Fo > 4.0 \s(Fo)' _diffrn_reflns_theta_max 25.99 _diffrn_reflns_av_R_equivalents .071 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_l_min -48 _diffrn_reflns_limit_l_max 48 _diffrn_standards_decay_% 0 _refine_ls_structure_factor_coef F _refine_ls_R_factor_gt .055 _refine_ls_wR_factor_ref .055 _refine_ls_goodness_of_fit_ref 1.854 _refine_ls_number_reflns .240810+05 _refine_ls_number_parameters 3024 _refine_ls_weighting_scheme calc _refine_ls_weighting_details '\w=1/[\s^2^(Fo)+0.0001(Fo^2^)]' _refine_ls_hydrogen_treatment calculated _refine_ls_shift/su_max .203 _refine_diff_density_max 1.294 _refine_diff_density_min -1.624 _refine_ls_extinction_method none _refine_ls_abs_structure_details none _publ_section_exptl_refinement ; The methyl group C53a shows two disordered positions refined with isotropic displacement paremeters and population parameters of 0.70 and 0.30. All triflate anions have been refined with restraints on bond lenghts and bond angles. Three of them (j,k,l) show large disorders. ; _computing_data_collection 'EXPOSE (Stoe & Cie, 1999)' _computing_cell_refinement 'CELL (Stoe & Cie, 1999)' _computing_data_reduction 'XRED (Stoe & Cie, 1999)' _computing_structure_solution 'Multan_87' _computing_structure_refinement xtal_CRYLSQ _computing_molecular_graphics xtal_gx3 _computing_publication_material xtal_CIFIO loop_ _atom_type_symbol _atom_type_scat_source _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag C Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 .002 .002 H Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 0 0 N Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 .004 .003 O Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 .008 .006 F Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 .014 .01 S Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 .11 .124 Eu Int._Tables_Vol_IV_Tables_2.2B_and_2.3.1 -.542 3.669 loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_occupancy _atom_site_adp_type 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-.3995(3) .053(5) 1.00000 Uani C20a .2982(7) .1705(4) -.4422(3) .041(4) 1.00000 Uani C21a .3726(7) .2016(4) -.4594(3) .046(4) 1.00000 Uani C22a .3860(8) .1790(5) -.4926(3) .063(5) 1.00000 Uani C23a .4528(8) .2179(5) -.5071(3) .067(6) 1.00000 Uani C24a .5087(7) .2758(5) -.4879(3) .057(5) 1.00000 Uani C25a .4947(6) .2945(4) -.4544(3) .044(4) 1.00000 Uani C26a .5412(6) .3575(4) -.4319(3) .043(4) 1.00000 Uani C27a .7033(7) .3546(5) -.4395(3) .064(5) 1.00000 Uani C28a .7465(10) .3238(6) -.4111(4) .089(7) 1.00000 Uani C29a .6720(7) .4527(5) -.4091(3) .063(5) 1.00000 Uani C30a .6773(9) .5025(5) -.4326(4) .083(7) 1.00000 Uani C31a .5130(6) .0146(4) -.1912(3) .042(4) 1.00000 Uani C32a .4816(6) -.0864(4) -.2121(3) .043(4) 1.00000 Uani C33a .4424(7) -.1502(5) -.2291(3) .049(5) 1.00000 Uani C34a .4908(6) -.1952(4) -.2215(3) .044(4) 1.00000 Uani C35a .5778(7) -.1769(5) -.1972(3) .054(5) 1.00000 Uani C36a .6173(7) -.1142(5) -.1798(3) .058(5) 1.00000 Uani C37a .5669(7) -.0704(5) -.1880(3) .050(5) 1.00000 Uani C38a .4507(7) -.2655(5) -.2395(3) .055(5) 1.00000 Uani C39a .3509(7) -.2958(4) -.2356(3) .047(4) 1.00000 Uani C40a .3283(7) -.2898(4) -.2020(3) .049(4) 1.00000 Uani C41a .2360(7) -.3163(4) -.1993(3) .048(4) 1.00000 Uani C42a .1684(7) -.3466(4) -.2283(3) .048(5) 1.00000 Uani C43a .1890(8) -.3542(5) -.2619(3) .062(5) 1.00000 Uani C44a .2820(8) -.3283(5) -.2643(3) .055(5) 1.00000 Uani C45a .1044(7) -.3439(4) -.1811(3) .047(5) 1.00000 Uani C46a .0396(8) -.3458(4) -.1564(3) .056(5) 1.00000 Uani C47a -.0573(8) -.3492(5) -.1662(4) .074(6) 1.00000 Uani C48a -.1061(9) -.3440(6) -.1391(4) .086(7) 1.00000 Uani C49a -.0639(9) -.3412(6) -.1054(4) .084(7) 1.00000 Uani C50a .0311(8) -.3405(5) -.0980(3) .063(5) 1.00000 Uani C51a .0916(8) -.3356(5) -.0633(3) .061(5) 1.00000 Uani C52a -.0296(14) -.4126(9) -.0415(6) .158(13) 1.00000 Uani C53a -.090(3) -.3941(18) -.0187(12) .211(16) .70000 Uiso C53a' -.050(6) -.476(4) -.032(2) .16(3) .30000 Uiso C54a .1331(14) -.3589(7) -.0044(4) .113(10) 1.00000 Uani C55a .1942(15) -.4012(10) -.0069(5) .138(12) 1.00000 Uani C56a .2308(8) .2120(5) -.1767(3) .062(5) 1.00000 Uani C57a .2304(9) .1784(5) -.1445(3) .071(6) 1.00000 Uani C58a .2363(8) .0573(5) -.4806(3) .069(6) 1.00000 Uani C59a .1678(10) .0602(7) -.5128(3) .102(7) 1.00000 Uani C60a .6681(7) .0278(5) -.1463(3) .056(5) 1.00000 Uani C61a .7506(8) .0650(6) -.1603(3) .073(6) 1.00000 Uani C62a -.0047(8) -.4052(5) -.2396(3) .062(5) 1.00000 Uani C63a -.0193(11) -.4734(6) -.2380(5) .125(9) 1.00000 Uani O1b .2938(5) .3291(3) -.44958(16) .050(3) 1.00000 Uani O2b .3906(6) -.2834(3) -.05635(17) .063(4) 1.00000 Uani N1b .4082(5) -.0607(3) -.29239(17) .040(3) 1.00000 Uani N2b .4619(5) .0684(3) -.27379(17) .039(3) 1.00000 Uani N3b .6168(5) .0745(4) -.26454(19) .045(4) 1.00000 Uani N4b .2908(5) .3152(3) -.33920(18) .040(4) 1.00000 Uani N5b .1763(5) .3241(4) -.30907(19) .045(4) 1.00000 Uani N6b .1872(5) .3185(3) -.40198(18) .040(3) 1.00000 Uani N7b .1690(7) .2941(4) -.4949(3) .064(5) 1.00000 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1.00000 Uani C45c .4853(7) -.2459(5) -.1145(3) .050(5) 1.00000 Uani C46c .4666(7) -.3164(5) -.1239(3) .059(5) 1.00000 Uani C47c .5330(8) -.3489(5) -.1313(4) .079(6) 1.00000 Uani C48c .5069(10) -.4155(6) -.1358(5) .102(8) 1.00000 Uani C49c .4162(8) -.4477(5) -.1347(4) .084(7) 1.00000 Uani C50c .3521(7) -.4122(5) -.1302(3) .063(5) 1.00000 Uani C51c .2533(7) -.4386(4) -.1255(3) .055(5) 1.00000 Uani C52c .2196(16) -.5325(9) -.1758(10) .25(3) 1.00000 Uani C53c .235(2) -.579(3) -.1611(7) .39(3) 1.00000 Uani C54c .0993(15) -.5145(6) -.1361(6) .128(12) 1.00000 Uani C55c .1053(13) -.5363(9) -.1042(8) .167(15) 1.00000 Uani C56c .0577(7) -.1358(4) -.3837(3) .050(4) 1.00000 Uani C57c -.0121(7) -.1184(5) -.4112(3) .057(5) 1.00000 Uani C58c .7336(7) .3241(5) -.2971(3) .053(5) 1.00000 Uani C59c .8231(7) .3410(5) -.3110(4) .068(6) 1.00000 Uani C60c .0029(7) .0051(5) -.1793(3) .058(5) 1.00000 Uani C61c -.0162(8) .0650(6) -.1914(4) .083(7) 1.00000 Uani C62c .6630(7) -.2153(5) -.0874(3) .058(5) 1.00000 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H2c -.03566 -.07945 -.34434 .05000 1.00000 Uiso H3c -.12999 -.06895 -.30186 .05000 1.00000 Uiso H4c -.05794 -.03993 -.24174 .05000 1.00000 Uiso H8c .41402 .05305 -.33901 .05000 1.00000 Uiso H10c .34266 -.04741 -.43973 .05000 1.00000 Uiso H11c .19284 -.10458 -.43058 .05000 1.00000 Uiso H131c .52591 .01785 -.39528 .05000 1.00000 Uiso H132c .47092 .04994 -.42363 .05000 1.00000 Uiso H15c .42427 .15300 -.39706 .05000 1.00000 Uiso H18c .71859 .18779 -.31642 .05000 1.00000 Uiso H19c .64046 .08542 -.35020 .05000 1.00000 Uiso H22c .72675 .43303 -.31415 .05000 1.00000 Uiso H23c .71386 .54038 -.30965 .05000 1.00000 Uiso H24c .56373 .55946 -.32351 .05000 1.00000 Uiso H271c .46399 .54456 -.29153 .05000 1.00000 Uiso H272c .39214 .58817 -.29706 .05000 1.00000 Uiso H281c .28467 .51722 -.27536 .05000 1.00000 Uiso H282c .35653 .47361 -.26983 .05000 1.00000 Uiso H283c .37961 .54299 -.24654 .05000 1.00000 Uiso H291c .21884 .46264 -.35494 .05000 1.00000 Uiso H292c .23317 .52875 -.32918 .05000 1.00000 Uiso H301c .29359 .58525 -.36977 .05000 1.00000 Uiso H302c .27925 .51915 -.39553 .05000 1.00000 Uiso H303c .19012 .54179 -.38726 .05000 1.00000 Uiso H33c .38431 -.01141 -.15889 .05000 1.00000 Uiso H35c .26987 .03012 -.07299 .05000 1.00000 Uiso H36c .12294 .02245 -.10897 .05000 1.00000 Uiso H381c .48018 .05545 -.09292 .05000 1.00000 Uiso H382c .42603 .02645 -.06401 .05000 1.00000 Uiso H40c .34948 -.10741 -.11509 .05000 1.00000 Uiso H43c .68117 -.07412 -.07294 .05000 1.00000 Uiso H44c .61322 .01275 -.07068 .05000 1.00000 Uiso H47c .59625 -.32529 -.13304 .05000 1.00000 Uiso H48c .55295 -.43953 -.13985 .05000 1.00000 Uiso H49c .39751 -.49463 -.13711 .05000 1.00000 Uiso H521c .16476 -.54588 -.19395 .05000 1.00000 Uiso H522c .27435 -.50868 -.18269 .05000 1.00000 Uiso H531c .29107 -.56860 -.14140 .05000 1.00000 Uiso H532c .18148 -.60580 -.15266 .05000 1.00000 Uiso H533c .24821 -.60506 -.18166 .05000 1.00000 Uiso H541c .07175 -.47750 -.13591 .05000 1.00000 Uiso H542c .06059 -.54875 -.15550 .05000 1.00000 Uiso H551c .13172 -.57273 -.10536 .05000 1.00000 Uiso H552c .14288 -.50147 -.08577 .05000 1.00000 Uiso H553c .03900 -.54850 -.10202 .05000 1.00000 Uiso H561c .08311 -.16846 -.39526 .05000 1.00000 Uiso H562c .02399 -.15372 -.36619 .05000 1.00000 Uiso H571c -.03712 -.08580 -.39958 .05000 1.00000 Uiso H572c .02200 -.10054 -.42865 .05000 1.00000 Uiso H573c -.06502 -.15472 -.42337 .05000 1.00000 Uiso H581c .72634 .36344 -.28404 .05000 1.00000 Uiso H582c .73872 .29295 -.28126 .05000 1.00000 Uiso H591c .83022 .30151 -.32398 .05000 1.00000 Uiso H592c .81784 .37199 -.32677 .05000 1.00000 Uiso H593c .87952 .35947 -.29254 .05000 1.00000 Uiso H601c -.04564 -.03249 -.19334 .05000 1.00000 Uiso H602c -.00158 .00683 -.15459 .05000 1.00000 Uiso H611c .03245 .10239 -.17728 .05000 1.00000 Uiso H612c -.01162 .06307 -.21603 .05000 1.00000 Uiso H613c -.07798 .07005 -.18873 .05000 1.00000 Uiso H621c .69190 -.18636 -.06517 .05000 1.00000 Uiso H622c .65108 -.26012 -.08347 .05000 1.00000 Uiso H631c .70151 -.23387 -.13482 .05000 1.00000 Uiso H632c .74233 -.16011 -.11652 .05000 1.00000 Uiso H633c .79105 -.21304 -.10349 .05000 1.00000 Uiso H21m .22045 -.12214 .43874 .08000 1.00000 Uiso H22m .25607 -.08841 .40231 .08000 1.00000 Uiso H23m .30864 -.14679 .41929 .08000 1.00000 Uiso H21n .38575 .19487 .27358 .08000 1.00000 Uiso H22n .28917 .22628 .26032 .08000 1.00000 Uiso H23n .29587 .18953 .29850 .08000 1.00000 Uiso H21o .78371 .39765 .47540 .08000 1.00000 Uiso H22o .88228 .41077 .45455 .08000 1.00000 Uiso H23o .89879 .41494 .50090 .08000 1.00000 Uiso H21p .29395 .36155 .37068 .08000 1.00000 Uiso H22p .23944 .31109 .32981 .08000 1.00000 Uiso H23p .19173 .37420 .34492 .08000 1.00000 Uiso H21q .56679 .46721 .41875 .08000 1.00000 Uiso H22q .54244 .52902 .44667 .08000 1.00000 Uiso H23q .66025 .52169 .45070 .08000 1.00000 Uiso H21r .39256 .48537 .06968 .08000 1.00000 Uiso H22r .32966 .44664 .02707 .08000 1.00000 Uiso H23r .27260 .48515 .05588 .08000 1.00000 Uiso H21s .05041 -.08084 .04309 .08000 1.00000 Uiso H22s .02790 -.00934 .03162 .08000 1.00000 Uiso H23s .14138 -.02159 .03292 .08000 1.00000 Uiso H21t .04336 .17968 .56183 .08000 1.00000 Uiso H22t -.05966 .20253 .54299 .08000 1.00000 Uiso H23t -.07061 .13834 .56824 .08000 1.00000 Uiso H21u .19950 .56979 .21676 .08000 1.00000 Uiso H22u .25390 .50624 .21012 .08000 1.00000 Uiso H23u .29288 .57959 .19404 .08000 1.00000 Uiso loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Eu1 .0283(3) .0368(3) .0320(3) .00594(17) .0078(2) .00094(17) Eu2 .0305(3) .0392(3) .0406(3) .00770(18) .0083(3) .00905(19) Eu3 .0432(3) .0376(3) .0417(3) .00849(19) .0061(3) -.00276(19) O1a .034(4) .047(4) .055(4) .006(3) .017(3) .019(3) O2a .072(5) .052(4) .056(5) -.000(4) .025(4) -.006(4) N1a .038(4) .040(4) .043(5) .013(3) .017(4) .007(3) N2a .034(4) .039(4) .044(5) .006(3) .012(4) -.002(3) N3a .062(6) .042(4) .042(5) .018(4) .021(5) .001(4) N4a .034(4) .045(4) .043(5) .005(3) .012(4) .007(3) N5a .053(5) .040(4) .044(5) -.001(4) .016(4) .001(4) N6a .038(4) .039(4) .039(4) .005(3) .005(4) .009(3) N7a .038(5) .050(5) .061(6) .004(4) .010(4) .011(4) N8a .033(4) .046(4) .038(4) .014(3) .008(4) .000(3) N9a .036(4) .057(5) .048(5) .018(4) .004(4) .005(4) N10a .036(4) .055(5) .044(5) .012(4) .004(4) -.008(4) N11a .054(5) .047(5) .047(5) .011(4) -.003(5) -.006(4) N12a .048(5) .038(4) .062(6) .003(4) .014(5) -.004(4) N13a .114(10) .084(7) .067(7) -.018(7) .033(7) .007(6) C1a .044(6) .050(5) .033(5) .005(4) .011(5) .007(4) C2a .071(7) .041(5) .046(6) .012(5) .011(6) -.003(4) C3a .068(8) .055(6) .052(7) .000(5) .002(6) -.010(5) C4a .052(6) .057(6) .054(6) .004(5) -.014(6) .006(5) C5a .040(5) .050(5) .040(5) .006(4) .006(5) .006(4) C6a .051(6) .027(4) .038(5) .009(4) .013(5) -.000(4) C7a .038(5) .038(5) .052(6) .010(4) .018(5) .008(4) C8a .041(5) .035(5) .045(6) .015(4) .010(5) .011(4) C9a .035(5) .042(5) .049(6) .005(4) .014(5) .014(4) C10a .036(5) .058(6) .061(7) .024(4) .019(5) .022(5) C11a .061(7) .065(6) .052(6) .038(5) .019(6) .010(5) C12a .049(6) .046(5) .047(6) .018(4) .021(5) .012(4) C13a .038(5) .047(5) .051(6) .004(4) .006(5) .014(4) C14a .037(5) .050(5) .037(5) .005(4) .007(5) .016(4) C15a .034(5) .043(5) .044(5) .003(4) .004(5) .013(4) C16a .036(5) .046(5) .036(5) .001(4) .004(5) .011(4) C17a .041(5) .044(5) .042(5) -.007(4) .009(5) .001(4) C18a .068(7) .045(5) .060(7) -.001(5) .020(6) -.001(5) C19a .047(6) .058(6) .044(6) -.005(5) .012(5) .008(5) C20a .040(5) .044(5) .038(5) .007(4) .005(5) .014(4) C21a .040(5) .052(5) .046(6) .007(4) .012(5) .010(4) C22a .073(7) .055(6) .054(6) .000(5) .025(6) -.005(5) C23a .079(8) .060(6) .058(7) .002(6) .036(6) -.003(5) C24a .053(6) .056(6) .059(6) -.001(5) .027(6) .009(5) C25a .040(5) .052(5) .042(5) .007(4) .017(5) .012(4) C26a .036(5) .047(5) .056(6) .008(4) .027(5) .027(4) C27a .038(6) .084(7) .068(7) .012(5) .016(6) .011(6) C28a .079(9) .103(9) .095(10) .035(7) .030(8) .014(8) C29a .045(6) .072(7) .057(7) -.009(5) .004(6) .010(5) C30a .075(8) .060(7) .091(9) -.003(6) -.011(8) .007(6) C31a .030(5) .056(6) .040(5) .010(4) .006(5) .008(4) C32a .043(5) .055(6) .037(5) .021(4) .017(5) .007(4) C33a .047(6) .058(6) .045(6) .020(5) .006(5) .005(5) C34a .041(5) .053(5) .046(6) .022(4) .014(5) .009(4) C35a .045(6) .073(7) .050(6) .026(5) .007(5) .012(5) C36a .043(6) .077(7) .058(7) .025(5) .006(6) .013(6) C37a .032(5) .076(7) .043(6) .018(5) .005(5) .008(5) C38a .060(7) .063(6) .047(6) .023(5) .015(6) .008(5) C39a .056(6) .045(5) .044(6) .028(5) .007(5) .000(4) C40a .045(6) .053(5) .041(6) .017(4) -.001(5) -.009(4) C41a .048(6) .048(5) .048(6) .016(4) .008(5) -.001(4) C42a .039(5) .051(6) .048(6) .010(4) .001(5) -.007(5) C43a .070(7) .067(7) .045(6) .027(6) -.003(6) -.008(5) C44a .066(7) .058(6) .048(6) .029(5) .015(6) .001(5) C45a .043(6) .043(5) .053(6) .011(4) .008(5) .003(4) C46a .058(7) .041(5) .067(7) .007(5) .020(6) -.001(5) C47a .039(6) .075(7) .099(9) .009(5) .014(7) -.005(6) C48a .048(7) .095(9) .106(11) .005(6) .022(8) .003(8) C49a .055(8) .106(10) .081(10) .003(7) .022(8) -.004(7) C50a .060(7) .053(6) .065(7) -.009(5) .027(6) -.003(5) C51a .063(7) .053(6) .059(7) -.002(5) .023(6) -.003(5) C52a .138(17) .136(14) .20(2) -.015(12) .102(16) .029(13) C54a .156(17) .091(10) .057(9) -.036(10) .034(10) .002(7) C55a .153(19) .155(17) .079(11) -.003(13) -.001(12) .044(11) C56a .077(8) .066(6) .043(6) .024(6) .020(6) -.004(5) C57a .089(9) .069(7) .055(7) .019(6) .030(7) -.001(5) C58a .079(8) .052(6) .061(7) -.009(5) .033(7) -.015(5) C59a .101(11) .113(10) .053(7) -.035(8) .022(8) -.019(7) C60a .029(5) .074(7) .052(6) .005(5) -.003(5) -.000(5) C61a .042(6) .104(8) .062(7) -.001(6) .013(6) .009(6) C62a .052(6) .061(6) .062(7) .016(5) -.008(6) -.010(5) C63a .115(13) .065(8) .139(14) -.016(8) -.043(11) -.020(9) O1b .046(4) .061(4) .046(4) .016(3) .013(4) .015(3) O2b .076(5) .053(4) .053(5) .024(4) -.001(4) -.009(4) N1b .032(4) .043(4) .040(4) .003(3) .010(4) .003(3) N2b .032(4) .045(4) .039(4) .006(3) .009(4) .006(3) N3b .032(4) .050(5) .051(5) .012(3) .008(4) .005(4) N4b .038(4) .040(4) .042(5) .008(3) .012(4) .007(3) N5b .037(4) .056(5) .045(5) .014(4) .013(4) .008(4) N6b .033(4) .039(4) .045(5) .005(3) .006(4) .006(3) N7b .057(6) .084(6) .048(6) .019(5) .005(5) .007(5) N8b .034(4) .031(4) .040(4) .002(3) .009(4) .000(3) N9b .053(5) .047(5) .050(5) -.000(4) .014(5) -.016(4) N10b .034(4) .041(4) .040(4) .005(3) .008(4) -.002(3) N11b .051(5) .054(5) .049(5) .022(4) .015(5) -.001(4) N12b .053(5) .037(4) .048(5) .016(4) .017(5) .003(4) N13b .079(7) .061(5) .061(6) .032(5) .004(6) .008(5) C1b .043(5) .047(5) .042(5) .013(4) .019(5) .002(4) C2b .040(5) .066(6) .076(7) .007(5) .036(6) .000(5) C3b .063(7) .061(6) .095(9) .011(5) .049(7) -.007(6) C4b .060(7) .054(6) .065(7) .011(5) .027(6) -.016(5) C5b .043(5) .048(5) .042(5) .008(4) .010(5) -.005(4) C6b .032(5) .046(5) .047(6) .001(4) .014(5) .001(4) C7b .035(5) .041(5) .036(5) .004(4) .004(4) .004(4) C8b .034(5) .040(5) .048(6) .002(4) .009(5) .007(4) C9b .045(5) .036(5) .041(5) .001(4) .008(5) .010(4) C10b .044(6) .044(5) .054(6) .004(4) .010(5) .007(4) C11b .031(5) .055(6) .057(6) .001(4) .000(5) .006(5) C12b .032(5) .049(5) .037(5) .005(4) .002(4) .003(4) C13b .054(6) .048(5) .045(6) -.000(5) .006(5) .006(4) C14b .045(5) .035(5) .040(5) .006(4) .004(5) .000(4) C15b .032(5) .043(5) .038(5) .005(4) .005(4) .004(4) C16b .040(5) .035(5) .044(6) .008(4) .011(5) .007(4) C17b .036(5) .049(5) .049(6) .010(4) .014(5) .011(4) C18b .044(6) .069(6) .050(6) .014(5) .020(5) .012(5) C19b .058(6) .064(6) .043(6) .011(5) .014(5) .018(5) C20b .028(4) .039(5) .045(5) .008(4) .010(4) .006(4) C21b .037(5) .041(5) .051(6) .004(4) .010(5) .013(4) C22b .034(5) .068(6) .050(6) .020(5) -.000(5) .004(5) C23b .044(6) .075(7) .066(7) .029(5) .012(6) .005(5) C24b .041(6) .084(7) .053(6) .023(5) -.007(5) .014(5) C25b .038(5) .042(5) .053(6) .007(4) .004(5) .009(4) C26b .049(6) .055(6) .046(6) .011(5) .007(6) .009(5) C27b .050(7) .157(12) .051(8) .016(8) -.012(7) -.022(8) C28b .072(10) .31(3) .051(9) .066(13) -.026(9) .008(12) C29b .072(8) .090(8) .061(7) .021(6) .032(7) .004(6) C30b .120(13) .118(12) .114(12) .032(10) .042(11) .028(9) C31b .045(6) .036(5) .045(6) .008(4) .011(5) -.007(4) C32b .024(4) .043(5) .044(5) .006(4) .002(4) .005(4) C33b .045(5) .037(5) .039(5) .012(4) .004(5) .009(4) C34b .038(5) .045(5) .052(6) .010(4) .007(5) .017(4) C35b .045(6) .050(6) .062(7) -.004(5) -.000(6) .007(5) C36b .052(6) .051(6) .060(7) .003(5) .006(6) -.009(5) C37b .039(5) .049(5) .044(6) .006(4) .002(5) -.000(4) C38b .036(5) .063(6) .061(7) .007(5) .006(5) .023(5) C39b .037(5) .048(5) .050(6) .001(4) .009(5) .017(4) C40b .041(5) .036(5) .041(5) .007(4) .010(5) .006(4) C41b .039(5) .034(5) .048(6) .008(4) .016(5) .006(4) C42b .047(6) .049(5) .051(6) .017(4) .016(5) .006(4) C43b .042(6) .063(6) .067(7) .024(5) .020(6) .001(5) C44b .037(5) .059(6) .079(8) .022(5) .015(6) .018(5) C45b .041(5) .037(5) .046(6) .012(4) .010(5) .006(4) C46b .057(6) .050(5) .036(5) .014(5) .013(5) .001(4) C47b .070(7) .046(5) .039(6) .015(5) .015(6) -.001(4) C48b .086(8) .041(5) .039(6) .001(5) .004(6) -.005(4) C49b .066(7) .061(6) .032(5) .007(5) -.004(5) .000(5) C50b .060(6) .051(6) .040(6) .017(5) .014(6) .003(4) C51b .051(6) .048(6) .051(6) .013(5) -.003(6) .005(5) C52b .057(7) .072(7) .057(7) .014(5) .008(6) .015(5) C53b .083(9) .088(8) .051(7) .020(7) -.002(7) .006(6) C54b .167(19) .24(3) .080(11) .152(19) .011(13) .037(12) C55b .19(3) .111(14) .21(3) .044(15) -.07(3) .042(15) C56b .037(5) .051(5) .066(7) .011(4) .005(5) .009(5) C57b .042(6) .069(6) .078(8) .012(5) .021(6) .006(6) C58b .039(5) .073(6) .058(6) .020(5) .019(5) .017(5) C59b .042(6) .077(7) .071(7) .018(5) .018(6) -.003(6) C60b .067(7) .058(6) .067(7) .012(5) .010(6) -.001(5) C61b .072(8) .075(7) .075(8) .015(6) .020(7) .000(6) C62b .067(7) .070(7) .063(7) .020(6) .026(6) -.008(5) C63b .100(11) .128(11) .095(10) .024(9) .064(9) -.011(8) O1c .041(4) .044(4) .064(5) .013(3) .010(4) .009(3) O2c .062(5) .031(3) .081(5) .006(3) .012(4) -.004(3) N1c .041(4) .034(4) .041(5) .009(3) .008(4) .006(3) N2c .033(4) .039(4) .027(4) .007(3) .005(3) -.006(3) N3c .037(4) .056(5) .040(5) .003(4) .011(4) -.004(4) N4c .035(4) .040(4) .046(5) .009(3) .010(4) .010(3) N5c .029(4) .047(4) .052(5) .006(3) .006(4) .012(4) N6c .038(4) .041(4) .047(5) .009(3) .011(4) .008(3) N7c .043(5) .049(5) .094(7) .007(4) .016(5) .002(5) N8c .032(4) .043(4) .035(4) .006(3) .010(4) .011(3) N9c .038(4) .056(5) .038(5) .021(4) .014(4) .011(4) N10c .041(5) .048(5) .051(5) .008(4) .004(4) -.009(4) N11c .042(5) .053(5) .046(5) .016(4) -.000(4) -.001(4) N12c .050(5) .046(5) .059(5) .012(4) .007(4) -.010(4) N13c .059(6) .054(6) .116(9) .012(5) .015(6) -.026(5) C1c .031(5) .046(5) .044(6) .009(4) .011(5) .004(4) C2c .034(5) .091(7) .043(6) .014(5) .002(5) .008(5) C3c .038(6) .124(10) .064(8) .021(6) .009(6) .000(7) C4c .038(6) .104(8) .052(7) .030(5) .016(5) .007(6) C5c .036(5) .052(5) .035(5) .011(4) .016(5) .015(4) C6c .035(5) .042(5) .035(5) .001(4) .006(4) -.000(4) C7c .039(5) .038(5) .045(5) .007(4) .011(5) .004(4) C8c .040(5) .047(5) .042(5) .011(4) .013(5) .002(4) C9c .047(5) .041(5) .046(6) .014(4) .021(5) .005(4) C10c .061(6) .053(6) .047(6) .016(5) .028(5) .008(5) C11c .063(7) .051(6) .039(6) .006(5) .009(5) -.007(4) C12c .044(5) .045(5) .041(5) .007(4) .012(5) .001(4) C13c .049(6) .050(5) .045(5) .009(4) .022(5) .006(4) C14c .035(5) .052(5) .055(6) .013(4) .021(5) .019(4) C15c .032(5) .050(5) .042(5) .008(4) .009(4) .011(4) C16c .034(5) .041(5) .037(5) .011(4) .006(4) .015(4) C17c .032(5) .047(5) .046(6) .008(4) .003(5) .015(4) C18c .037(5) .057(6) .069(7) .015(5) .002(6) .022(5) C19c .041(6) .051(6) .087(8) .018(5) .011(6) .021(5) C20c .035(5) .041(5) .046(5) .010(4) .009(5) .008(4) C21c .040(5) .049(5) .039(5) .011(4) .008(5) .009(4) C22c .034(5) .055(6) .058(6) .001(4) .002(5) .014(5) C23c .045(6) .049(6) .075(7) .002(5) .005(6) .002(5) C24c .054(6) .043(5) .068(7) .004(5) .014(6) .004(5) C25c .047(6) .035(5) .063(6) .008(4) .017(5) .009(4) C26c .047(6) .044(5) .074(8) .014(5) .022(6) .014(5) C27c .060(7) .050(6) .093(9) .008(5) .019(7) -.013(6) C28c .110(12) .089(9) .085(10) -.005(8) .010(9) -.005(7) C29c .052(7) .045(6) .120(11) .017(5) .018(7) -.004(6) C30c .059(8) .103(10) .175(17) .037(7) .007(10) .051(10) C31c .032(5) .046(5) .033(5) .009(4) .012(4) .008(4) C32c .047(6) .036(5) .029(5) .011(4) .012(5) .008(4) C33c .041(5) .041(5) .041(5) .008(4) .011(5) .005(4) C34c .059(6) .034(5) .042(5) .010(4) .010(5) .005(4) C35c .065(7) .056(6) .036(5) .018(5) .018(5) .008(4) C36c .050(6) .055(6) .039(6) .011(5) .016(5) .004(4) C37c .048(6) .052(5) .040(6) .016(4) .015(5) .003(4) C38c .056(6) .037(5) .040(5) .003(4) .010(5) -.003(4) C39c .050(6) .056(6) .027(5) .009(5) .005(5) .006(4) C40c .040(5) .043(5) .037(5) .005(4) .004(5) .003(4) C41c .042(5) .043(5) .040(5) .005(4) .005(5) -.001(4) C42c .045(6) .055(6) .043(6) .013(5) -.002(5) .004(4) C43c .037(5) .058(6) .043(6) .001(4) .000(5) .001(5) C44c .050(6) .053(6) .042(6) .001(5) .001(5) .001(5) C45c .036(5) .052(6) .054(6) .008(4) .004(5) -.005(5) C46c .048(6) .058(6) .061(7) .009(5) .007(6) -.008(5) C47c .048(6) .066(7) .113(10) .013(5) .014(7) -.019(7) C48c .078(9) .063(8) .153(14) .028(7) .007(10) -.030(8) C49c .058(7) .055(6) .130(11) .021(6) .018(8) -.026(7) C50c .049(6) .043(6) .083(8) .012(5) -.001(6) -.016(5) C51c .051(6) .036(5) .072(7) .010(4) .009(6) -.010(5) C52c .090(13) .082(11) .49(6) .026(10) -.01(3) -.16(2) C53c .13(3) .71(8) .115(18) -.17(4) .059(17) -.20(4) C54c .167(19) .032(7) .172(18) .011(8) .048(16) -.017(9) C55c .077(11) .106(14) .28(4) .004(10) -.010(17) -.005(16) C56c .040(5) .049(5) .049(6) .002(4) -.003(5) -.001(4) C57c .049(6) .061(6) .047(6) -.001(5) .004(5) -.002(5) C58c .040(5) .058(6) .048(6) -.002(4) -.010(5) .016(5) C59c .039(6) .082(7) .079(8) .006(5) .004(6) .023(6) C60c .041(6) .085(7) .053(6) .023(5) .018(5) .007(5) C61c .046(6) .082(8) .120(11) .028(6) .011(7) -.003(7) C62c .044(6) .066(6) .062(7) .024(5) -.003(6) .005(5) C63c .036(6) .087(8) .105(10) .021(5) .018(7) .026(7) S1d .137(5) .145(5) .121(4) .054(4) -.012(4) -.035(4) O1d .29(3) .116(9) .171(13) .001(11) .096(15) .013(9) O2d .42(4) .39(3) .184(16) .32(3) -.152(19) -.192(18) O3d .085(8) .168(10) .098(8) .008(7) .003(7) -.034(7) C1d .107(14) .194(18) .087(12) .056(13) .019(11) -.031(12) F1d .160(11) .165(10) .201(13) .072(8) -.078(10) -.068(9) F2d .180(13) .41(3) .112(9) .045(14) .084(10) -.006(11) F3d .145(9) .149(8) .131(8) .069(7) .042(7) -.000(6) S1e .0649(18) .0573(16) .103(3) .0190(13) .0245(18) .0122(15) O1e .097(7) .166(9) .095(7) .067(7) .042(6) .021(6) O2e .093(7) .101(7) .115(8) -.007(6) -.005(7) -.009(6) O3e .133(9) .075(6) .145(10) .036(6) .006(8) .030(6) C1e .089(9) .061(7) .102(10) .028(7) .043(8) .004(7) F1e .118(7) .081(5) .119(7) .003(5) .013(6) .009(5) F2e .169(9) .074(5) .108(6) .043(5) .006(7) .012(4) F3e .174(10) .116(7) .111(7) .008(6) .067(7) -.002(5) S1f .097(4) .123(4) .126(4) .028(3) -.016(4) -.013(3) O1f .179(15) .215(14) .148(12) .045(11) -.019(11) -.075(11) O2f .187(13) .166(11) .107(9) .081(9) -.101(10) -.018(8) O3f .061(7) .266(15) .225(16) .068(9) .029(9) -.007(12) C1f .16(3) .159(18) .105(15) -.005(15) .009(16) .002(13) F1f .135(10) .38(2) .106(9) .004(11) -.024(9) .090(11) F2f .160(13) .46(3) .195(15) .121(16) .068(12) .002(15) F3f .230(15) .147(9) .147(10) -.013(9) .018(10) .006(8) S1g .0633(17) .0794(17) .0549(16) .0134(14) .0168(15) .0091(13) O1g .064(6) .174(9) .084(7) .035(6) .021(6) .051(6) O2g .113(7) .072(5) .064(5) .010(5) .026(5) -.015(4) O3g .092(7) .090(5) .054(5) .008(5) .024(5) -.002(4) C1g .083(10) .088(9) .084(9) .007(8) .018(8) .020(7) F1g .254(14) .061(5) .162(10) -.006(7) .041(10) .008(6) F2g .103(6) .142(7) .098(6) .051(5) .043(6) .061(5) F3g .101(7) .163(8) .208(11) .070(6) .076(8) .103(8) S1h .0638(17) .0591(15) .0679(18) .0151(13) .0169(15) -.0040(13) O1h .076(6) .124(7) .097(7) -.030(6) .028(6) -.016(6) O2h .302(18) .161(10) .111(9) .179(12) .061(11) .025(8) O3h .067(6) .099(6) .076(6) -.004(5) .022(5) -.009(5) C1h .062(8) .077(8) .072(8) -.002(6) .010(7) -.020(7) F1h .312(17) .128(8) .129(8) .114(9) .090(10) .058(7) F2h .104(6) .115(6) .073(5) -.001(5) .013(5) -.015(4) F3h .094(7) .255(12) .096(7) -.064(8) .037(6) -.015(7) S1i .0505(15) .0571(15) .0679(18) .0100(12) .0023(14) .0054(12) O1i .45(7) .21(4) .14(3) .25(5) .15(4) .11(3) O2i .061(15) .32(5) .13(3) .02(3) .048(16) .08(3) O3i .32(6) .15(3) .060(13) -.14(3) -.01(3) -.027(17) C1i .077(10) .069(8) .103(11) .014(7) .023(9) .008(8) F1i .23(4) .17(3) .085(13) .08(3) .064(18) .036(14) F2i .20(4) .22(4) .12(3) .13(3) .03(3) .10(3) F3i .036(10) .39(6) .18(4) -.04(3) .018(16) .15(4) O1i' .095(15) .047(10) .114(16) -.034(11) -.018(15) .021(10) O2i' .091(15) .101(14) .109(16) .036(11) .055(14) .033(12) O3i' .045(9) .071(12) .088(13) .018(9) -.030(9) -.012(10) F1i' .104(18) .134(16) .091(12) .029(13) .052(14) -.011(12) F2i' .028(8) .17(3) .119(19) -.012(13) -.015(10) .073(18) F3i' .11(2) .063(9) .111(14) -.008(9) .019(13) .014(8) S1j .0657(19) .084(3) .086(3) .0128(16) .0122(19) -.0149(17) O1j .064(14) .088(14) .052(14) .018(11) -.001(12) -.020(10) O2j .112(17) .041(9) .21(3) .016(9) .082(17) -.002(11) O3j .097(16) .15(2) .095(16) .049(14) -.048(15) .018(14) F1j .063(10) .174(18) .20(3) .016(11) .018(14) .028(16) F2j .15(3) .176(18) .157(19) -.035(15) .089(17) -.081(15) F3j .17(5) .50(8) .21(6) -.13(5) -.02(4) .11(5) O1j' .09(3) .15(3) .061(15) -.045(17) -.028(15) .019(14) O2j' .27(5) .38(6) .14(3) .25(5) .02(4) -.04(4) O3j' .077(12) .075(11) .072(11) -.021(9) -.004(10) -.012(9) F1j' .11(3) .073(11) .106(19) -.025(11) .044(17) -.009(11) F2j' .21(3) .25(3) .074(12) -.06(3) .041(15) -.014(14) F3j' .19(3) .141(16) .120(16) .008(15) .011(17) .032(12) S1k .0413(16) .084(3) .180(5) .0163(15) .017(3) -.030(3) S1l .241(7) .075(3) .125(4) .053(4) -.022(5) -.016(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance Eu1 Eu2 . . 9.3165(8) Eu1 Eu3 . . 9.0762(7) Eu2 Eu3 . . 18.3650(9) Eu1 N1a . . 2.607(6) Eu1 N2a . . 2.534(7) Eu1 N8a . . 2.599(7) Eu1 N1b . . 2.555(8) Eu1 N2b . . 2.593(7) Eu1 N8b . . 2.583(6) Eu1 N1c . . 2.608(7) Eu1 N2c . . 2.599(7) Eu1 N8c . . 2.585(8) Eu2 O1a . . 2.381(6) Eu2 N4a . . 2.597(6) Eu2 N6a . . 2.594(8) Eu2 O1b . . 2.376(7) Eu2 N4b . . 2.549(8) Eu2 O1c . . 2.408(7) Eu3 O2a . . 2.375(8) Eu3 N10a . . 2.565(7) Eu3 N12a . . 2.597(7) Eu3 O2b . . 2.400(7) Eu3 N12b . . 2.571(7) Eu3 O2c . . 2.405(6) Eu3 N10c . . 2.594(8) Eu3 N12c . . 2.565(9) O1a C26a . . 1.251(12) O2a C51a . . 1.252(13) N1a C1a . . 1.337(12) N1a C5a . . 1.374(12) N2a C6a . . 1.362(10) N2a C7a . . 1.406(12) N3a C6a . . 1.362(13) N3a C12a . . 1.391(11) N3a C56a . . 1.481(13) N4a C16a . . 1.397(11) N4a C20a . . 1.349(12) N5a C17a . . 1.384(13) N5a C20a . . 1.381(10) N5a C58a . . 1.485(12) N6a C21a . . 1.353(9) N6a C25a . . 1.344(11) N7a C26a . . 1.347(11) N7a C27a . . 1.459(15) N7a C29a . . 1.493(12) N8a C31a . . 1.339(9) N8a C32a . . 1.388(12) N9a C31a . . 1.358(12) N9a C37a . . 1.385(12) N9a C60a . . 1.488(10) N10a C41a . . 1.391(13) N10a C45a . . 1.338(11) N11a C42a . . 1.386(13) N11a C45a . . 1.383(12) N11a C62a . . 1.479(11) N12a C46a . . 1.329(13) N12a C50a . . 1.355(15) N13a C51a . . 1.325(16) N13a C52a . . 1.49(3) N13a C54a . . 1.503(19) C1a C2a . . 1.385(11) C1a C6a . . 1.460(13) C2a C3a . . 1.363(16) C3a C4a . . 1.374(16) C4a C5a . . 1.384(11) C5a C31a . . 1.488(13) C7a C8a . . 1.367(12) C7a C12a . . 1.416(13) C8a C9a . . 1.365(13) C9a C10a . . 1.410(14) C9a C13a . . 1.500(12) C10a C11a . . 1.369(13) C11a C12a . . 1.408(15) C13a C14a . . 1.517(14) C14a C15a . . 1.393(11) C14a C19a . . 1.402(12) C15a C16a . . 1.401(14) C16a C17a . . 1.392(11) C17a C18a . . 1.383(13) C18a C19a . . 1.396(16) C20a C21a . . 1.462(13) C21a C22a . . 1.398(14) C22a C23a . . 1.386(15) C23a C24a . . 1.379(12) C24a C25a . . 1.392(14) C25a C26a . . 1.477(11) C27a C28a . . 1.500(19) C29a C30a . . 1.501(17) C32a C33a . . 1.402(11) C32a C37a . . 1.397(12) C33a C34a . . 1.382(14) C34a C35a . . 1.418(12) C34a C38a . . 1.531(12) C35a C36a . . 1.388(13) C36a C37a . . 1.383(16) C38a C39a . . 1.515(14) C39a C40a . . 1.411(14) C39a C44a . . 1.380(12) C40a C41a . . 1.384(13) C41a C42a . . 1.368(11) C42a C43a . . 1.398(15) C43a C44a . . 1.390(16) C45a C46a . . 1.474(16) C46a C47a . . 1.416(15) C47a C48a . . 1.39(3) C48a C49a . . 1.35(2) C49a C50a . . 1.396(18) C50a C51a . . 1.483(15) C52a C53a . . 1.46(6) C52a C53a' . . 1.45(8) C54a C55a . . 1.45(4) C56a C57a . . 1.533(15) C58a C59a . . 1.508(17) C60a C61a . . 1.524(15) C62a C63a . . 1.454(17) O1b C26b . . 1.272(12) O2b C51b . . 1.272(11) N1b C1b . . 1.343(11) N1b C5b . . 1.356(10) N2b C6b . . 1.345(12) N2b C7b . . 1.413(9) N3b C6b . . 1.364(10) N3b C12b . . 1.384(12) N3b C56b . . 1.458(13) N4b C16b . . 1.383(11) N4b C20b . . 1.333(12) N5b C17b . . 1.390(12) N5b C20b . . 1.400(12) N5b C58b . . 1.480(13) N6b C21b . . 1.327(13) N6b C25b . . 1.356(12) N7b C26b . . 1.325(12) N7b C27b . . 1.492(14) N7b C29b . . 1.480(16) N8b C31b . . 1.328(12) N8b C32b . . 1.423(10) N9b C31b . . 1.359(10) N9b C37b . . 1.372(13) N9b C60b . . 1.504(13) N10b C41b . . 1.409(11) N10b C45b . . 1.341(11) N11b C42b . . 1.382(11) N11b C45b . . 1.378(13) N11b C62b . . 1.496(15) N12b C46b . . 1.345(13) N12b C50b . . 1.345(12) N13b C51b . . 1.310(14) N13b C52b . . 1.466(14) N13b C54b . . 1.49(3) C1b C2b . . 1.399(15) C1b C6b . . 1.445(11) C2b C3b . . 1.384(13) C3b C4b . . 1.367(15) C4b C5b . . 1.395(15) C5b C31b . . 1.471(13) C7b C8b . . 1.402(13) C7b C12b . . 1.398(12) C8b C9b . . 1.380(10) C9b C10b . . 1.396(14) C9b C13b . . 1.526(13) C10b C11b . . 1.408(14) C11b C12b . . 1.391(11) C13b C14b . . 1.518(13) C14b C15b . . 1.393(12) C14b C19b . . 1.401(15) C15b C16b . . 1.389(12) C16b C17b . . 1.403(14) C17b C18b . . 1.376(14) C18b C19b . . 1.403(14) C20b C21b . . 1.473(12) C21b C22b . . 1.392(14) C22b C23b . . 1.352(15) C23b C24b . . 1.404(16) C24b C25b . . 1.370(15) C25b C26b . . 1.517(15) C27b C28b . . 1.48(3) C29b C30b . . 1.48(2) C32b C33b . . 1.369(13) C32b C37b . . 1.420(12) C33b C34b . . 1.397(11) C34b C35b . . 1.411(12) C34b C38b . . 1.504(15) C35b C36b . . 1.369(16) C36b C37b . . 1.389(12) C38b C39b . . 1.513(13) C39b C40b . . 1.380(13) C39b C44b . . 1.435(15) C40b C41b . . 1.394(12) C41b C42b . . 1.400(14) C42b C43b . . 1.404(14) C43b C44b . . 1.375(14) C45b C46b . . 1.454(12) C46b C47b . . 1.415(11) C47b C48b . . 1.401(15) C48b C49b . . 1.368(16) C49b C50b . . 1.368(12) C50b C51b . . 1.514(14) C52b C53b . . 1.519(15) C54b C55b . . 1.34(4) C56b C57b . . 1.491(15) C58b C59b . . 1.527(14) C60b C61b . . 1.433(17) C62b C63b . . 1.466(18) O1c C26c . . 1.256(11) O2c C51c . . 1.268(13) N1c C1c . . 1.374(10) N1c C5c . . 1.327(12) N2c C6c . . 1.346(10) N2c C7c . . 1.394(12) N3c C6c . . 1.354(11) N3c C12c . . 1.406(12) N3c C56c . . 1.482(10) N4c C16c . . 1.400(11) N4c C20c . . 1.346(9) N5c C17c . . 1.398(10) N5c C20c . . 1.370(12) N5c C58c . . 1.476(11) N6c C21c . . 1.356(12) N6c C25c . . 1.340(11) N7c C26c . . 1.331(14) N7c C27c . . 1.491(14) N7c C29c . . 1.470(14) N8c C31c . . 1.337(11) N8c C32c . . 1.403(10) N9c C31c . . 1.399(12) N9c C37c . . 1.373(11) N9c C60c . . 1.481(13) N10c C41c . . 1.379(10) N10c C45c . . 1.333(13) N11c C42c . . 1.396(13) N11c C45c . . 1.379(10) N11c C62c . . 1.469(13) N12c C46c . . 1.321(13) N12c C50c . . 1.361(11) N13c C51c . . 1.292(11) N13c C52c . . 1.62(4) N13c C54c . . 1.51(3) C1c C2c . . 1.405(12) C1c C6c . . 1.466(13) C2c C3c . . 1.377(16) C3c C4c . . 1.382(15) C4c C5c . . 1.405(13) C5c C31c . . 1.460(11) C7c C8c . . 1.407(12) C7c C12c . . 1.395(10) C8c C9c . . 1.398(13) C9c C10c . . 1.391(11) C9c C13c . . 1.525(13) C10c C11c . . 1.394(14) C11c C12c . . 1.372(14) C13c C14c . . 1.511(11) C14c C15c . . 1.404(13) C14c C19c . . 1.402(13) C15c C16c . . 1.409(10) C16c C17c . . 1.384(11) C17c C18c . . 1.403(14) C18c C19c . . 1.371(12) C20c C21c . . 1.468(12) C21c C22c . . 1.380(11) C22c C23c . . 1.379(14) C23c C24c . . 1.364(15) C24c C25c . . 1.365(11) C25c C26c . . 1.532(14) C27c C28c . . 1.45(2) C29c C30c . . 1.46(3) C32c C33c . . 1.390(12) C32c C37c . . 1.389(14) C33c C34c . . 1.408(12) C34c C35c . . 1.405(16) C34c C38c . . 1.502(13) C35c C36c . . 1.388(14) C36c C37c . . 1.414(13) C38c C39c . . 1.539(14) C39c C40c . . 1.388(11) C39c C44c . . 1.413(14) C40c C41c . . 1.393(14) C41c C42c . . 1.395(13) C42c C43c . . 1.422(11) C43c C44c . . 1.365(15) C45c C46c . . 1.478(13) C46c C47c . . 1.396(17) C47c C48c . . 1.386(16) C48c C49c . . 1.376(18) C49c C50c . . 1.385(17) C50c C51c . . 1.497(14) C52c C53c . . 1.27(6) C54c C55c . . 1.39(4) C56c C57c . . 1.521(14) C58c C59c . . 1.506(15) C60c C61c . . 1.510(17) C62c C63c . . 1.516(17) S1d O1d . . 1.589(19) S1d O2d . . 1.35(3) S1d O3d . . 1.377(11) S1d C1d . . 1.712(15) C1d F1d . . 1.396(16) C1d F2d . . 1.27(2) C1d F3d . . 1.29(2) S1e O1e . . 1.413(12) S1e O2e . . 1.395(9) S1e O3e . . 1.432(10) S1e C1e . . 1.830(12) C1e F1e . . 1.345(12) C1e F2e . . 1.342(14) C1e F3e . . 1.315(17) S1f O1f . . 1.437(15) S1f O2f . . 1.451(13) S1f O3f . . 1.443(15) S1f C1f . . 1.704(17) C1f F1f . . 1.36(2) C1f F2f . . 1.43(3) C1f F3f . . 1.317(18) S1g O1g . . 1.424(10) S1g O2g . . 1.439(7) S1g O3g . . 1.429(9) S1g C1g . . 1.798(13) C1g F1g . . 1.310(12) C1g F2g . . 1.326(15) C1g F3g . . 1.318(16) S1h O1h . . 1.414(10) S1h O2h . . 1.367(15) S1h O3h . . 1.431(8) S1h C1h . . 1.806(11) C1h F1h . . 1.294(18) C1h F2h . . 1.318(11) C1h F3h . . 1.294(14) S1i O1i . . 1.38(4) S1i O2i . . 1.39(3) S1i O3i . . 1.36(3) S1i C1i . . 1.827(12) C1i F1i . . 1.36(3) C1i F2i . . 1.28(5) C1i F3i . . 1.23(3) S1i O1i' . . 1.374(16) S1i O2i' . . 1.40(3) S1i O3i' . . 1.409(15) S1i C1i . . 1.827(12) C1i F1i' . . 1.28(3) C1i F2i' . . 1.23(3) C1i F3i' . . 1.403(18) S1j O1j . . 1.39(3) S1j O2j . . 1.402(18) S1j O3j . . 1.39(3) S1j C1j . . 1.870(19) C1j F1j . . 1.35(3) C1j F2j . . 1.30(3) C1j F3j . . 1.29(5) S1j O1j' . . 1.51(4) S1j O2j' . . 1.45(4) S1j O3j' . . 1.479(16) S1j C1j' . . 1.78(3) C1j' F1j' . . 1.42(3) C1j' F2j' . . 1.36(3) C1j' F3j' . . 1.32(4) S1k O1k . . 1.32(2) S1k O2k . . 1.428(18) S1k O3k . . 1.68(2) S1k C1k . . 1.623(19) C1k F1k . . 1.44(4) C1k F2k . . 1.33(3) C1k F3k . . 1.43(4) S1k O1k' . . 1.41(3) S1k O2k' . . 1.37(3) S1k O3k' . . 1.425(19) S1k C1k' . . 1.815(14) C1k' F1k' . . 1.40(3) C1k' F2k' . . 1.26(3) C1k' F3k' . . 1.225(18) S1l O1l . . 1.34(3) S1l O2l . . 1.46(3) S1l O3l . . 1.49(3) S1l C1l . . 1.91(3) C1l F1l . . 1.36(3) C1l F2l . . 1.32(4) C1l F3l . . 1.36(4) S1l O1l' . . 1.28(4) S1l O2l' . . 1.72(5) S1l O3l' . . 1.34(4) S1l C1l' . . 2.02(3) C1l' F1l' . . 1.30(6) C1l' F2l' . . 1.34(5) C1l' F3l' . . 1.43(5) S1l O1l'' . . 1.31(3) S1l O2l'' . . 1.44(3) S1l O3l'' . . 1.53(5) C1l' F1l'' . . 1.37(5) C1l' F2l'' . . 1.39(5) C1l' F3l'' . . 1.48(5) N1m C1m . . 1.058(18) C1m C2m . . 1.52(3) N1n C1n . . 1.099(15) C1n C2n . . 1.413(19) N1o C1o . . 1.15(4) C1o C2o . . 1.31(4) N1p C1p . . 1.16(3) C1p C2p . . 1.40(3) N1q C1q . . 1.17(3) C1q C2q . . 1.38(3) N1r C1r . . .97(4) C1r C2r . . 1.42(5) N1s C1s . . 1.118(18) C1s C2s . . 1.431(19) N1t C1t . . 1.11(3) C1t C2t . . 1.41(3) N1u C1u . . 1.23(5) C1u C2u . . 1.45(5) N1v C1v . . 1.03(7) C1v C2v . . 1.52(7) loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle Eu2 Eu1 Eu3 . . . 173.708(13) N1a Eu1 N2a . . . 63.7(3) N1a Eu1 N8a . . . 62.2(3) N1a Eu1 N1b . . . 118.3(3) N1a Eu1 N2b . . . 72.1(3) N1a Eu1 N8b . . . 140.2(3) N1a Eu1 N1c . . . 122.3(3) N1a Eu1 N2c . . . 140.5(2) N1a Eu1 N8c . . . 72.1(2) N2a Eu1 N8a . . . 125.87(19) N2a Eu1 N1b . . . 139.4(3) N2a Eu1 N2b . . . 81.7(3) N2a Eu1 N8b . . . 144.8(3) N2a Eu1 N1c . . . 74.18(19) N2a Eu1 N2c . . . 84.1(3) N2a Eu1 N8c . . . 78.2(3) N8a Eu1 N1b . . . 70.4(3) N8a Eu1 N2b . . . 81.0(3) N8a Eu1 N8b . . . 84.1(2) N8a Eu1 N1c . . . 140.0(3) N8a Eu1 N2c . . . 142.2(3) N8a Eu1 N8c . . . 86.9(3) N1b Eu1 N2b . . . 63.2(2) N1b Eu1 N8b . . . 62.4(3) N1b Eu1 N1c . . . 119.39(19) N1b Eu1 N2c . . . 71.7(3) N1b Eu1 N8c . . . 142.4(3) N2b Eu1 N8b . . . 125.5(3) N2b Eu1 N1c . . . 139.0(3) N2b Eu1 N2c . . . 81.6(2) N2b Eu1 N8c . . . 143.85(18) N8b Eu1 N1c . . . 70.6(3) N8b Eu1 N2c . . . 79.2(2) N8b Eu1 N8c . . . 86.4(3) N1c Eu1 N2c . . . 63.5(3) N1c Eu1 N8c . . . 61.8(3) N2c Eu1 N8c . . . 125.2(3) O1a Eu2 N4a . . . 127.1(3) O1a Eu2 N6a . . . 64.45(19) O1a Eu2 O1b . . . 76.1(2) O1a Eu2 N4b . . . 144.19(18) O1a Eu2 O1c . . . 79.7(3) N4a Eu2 N6a . . . 62.8(3) N4a Eu2 O1b . . . 81.8(2) N4a Eu2 N4b . . . 86.8(2) N4a Eu2 O1c . . . 144.6(3) N6a Eu2 O1b . . . 67.7(3) N6a Eu2 N4b . . . 146.0(2) N6a Eu2 O1c . . . 138.1(3) O1b Eu2 N4b . . . 125.7(3) O1b Eu2 O1c . . . 83.8(3) N4b Eu2 O1c . . . 75.7(3) O2a Eu3 N10a . . . 125.7(3) O2a Eu3 N12a . . . 63.1(3) O2a Eu3 O2b . . . 81.6(3) O2a Eu3 N12b . . . 66.0(3) O2a Eu3 O2c . . . 76.3(3) O2a Eu3 N10c . . . 144.3(2) O2a Eu3 N12c . . . 130.1(3) N10a Eu3 N12a . . . 62.6(3) N10a Eu3 O2b . . . 146.6(3) N10a Eu3 N12b . . . 141.5(3) N10a Eu3 O2c . . . 83.9(3) N10a Eu3 N10c . . . 87.4(3) N10a Eu3 N12c . . . 78.4(3) N12a Eu3 O2b . . . 139.5(3) N12a Eu3 N12b . . . 114.2(3) N12a Eu3 O2c . . . 68.3(3) N12a Eu3 N10c . . . 146.8(3) N12a Eu3 N12c . . . 119.2(3) O2b Eu3 N12b . . . 62.7(3) O2b Eu3 O2c . . . 85.2(3) O2b Eu3 N10c . . . 73.7(3) O2b Eu3 N12c . . . 68.5(3) N12b Eu3 O2c . . . 132.7(3) N12b Eu3 N10c . . . 79.7(3) N12b Eu3 N12c . . . 124.9(3) O2c Eu3 N10c . . . 125.6(3) O2c Eu3 N12c . . . 62.6(3) N10c Eu3 N12c . . . 63.1(3) Eu2 O1a C26a . . . 120.9(5) Eu3 O2a C51a . . . 124.8(7) Eu1 N1a C1a . . . 119.8(5) Eu1 N1a C5a . . . 121.4(6) C1a N1a C5a . . . 117.9(7) Eu1 N2a C6a . . . 114.5(6) Eu1 N2a C7a . . . 130.9(5) C6a N2a C7a . . . 105.7(8) C6a N3a C12a . . . 106.9(8) C6a N3a C56a . . . 130.4(8) C12a N3a C56a . . . 122.7(9) Eu2 N4a C16a . . . 135.0(6) Eu2 N4a C20a . . . 117.9(5) C16a N4a C20a . . . 106.5(6) C17a N5a C20a . . . 107.1(7) C17a N5a C58a . . . 123.3(7) C20a N5a C58a . . . 129.6(8) Eu2 N6a C21a . . . 121.5(6) Eu2 N6a C25a . . . 115.5(5) C21a N6a C25a . . . 119.7(8) C26a N7a C27a . . . 125.9(7) C26a N7a C29a . . . 117.8(8) C27a N7a C29a . . . 115.6(7) Eu1 N8a C31a . . . 119.5(6) Eu1 N8a C32a . . . 135.6(5) C31a N8a C32a . . . 104.5(7) C31a N9a C37a . . . 106.2(7) C31a N9a C60a . . . 132.1(8) C37a N9a C60a . . . 121.6(8) Eu3 N10a C41a . . . 134.5(6) Eu3 N10a C45a . . . 119.6(7) C41a N10a C45a . . . 105.6(7) C42a N11a C45a . . . 106.7(7) C42a N11a C62a . . . 123.8(8) C45a N11a C62a . . . 129.2(9) Eu3 N12a C46a . . . 121.9(7) Eu3 N12a C50a . . . 117.2(6) C46a N12a C50a . . . 118.2(9) C51a N13a C52a . . . 124.3(12) C51a N13a C54a . . . 119.0(12) C52a N13a C54a . . . 116.2(13) N1a C1a C2a . . . 124.0(9) N1a C1a C6a . . . 113.0(7) C2a C1a C6a . . . 122.7(9) C1a C2a C3a . . . 116.6(10) C2a C3a C4a . . . 122.1(8) C3a C4a C5a . . . 118.3(10) N1a C5a C4a . . . 121.0(9) N1a C5a C31a . . . 112.4(6) C4a C5a C31a . . . 126.3(9) N2a C6a N3a . . . 112.2(8) N2a C6a C1a . . . 119.0(9) N3a C6a C1a . . . 128.4(7) N2a C7a C8a . . . 130.9(9) N2a C7a C12a . . . 107.9(7) C8a C7a C12a . . . 121.0(9) C7a C8a C9a . . . 120.1(9) C8a C9a C10a . . . 119.0(8) C8a C9a C13a . . . 121.5(9) C10a C9a C13a . . . 119.5(9) C9a C10a C11a . . . 122.7(9) C10a C11a C12a . . . 117.5(10) N3a C12a C7a . . . 107.2(9) N3a C12a C11a . . . 133.4(9) C7a C12a C11a . . . 119.3(8) C9a C13a C14a . . . 116.6(8) C13a C14a C15a . . . 120.5(7) C13a C14a C19a . . . 119.5(8) C15a C14a C19a . . . 120.0(9) C14a C15a C16a . . . 118.1(7) N4a C16a C15a . . . 131.1(7) N4a C16a C17a . . . 108.6(8) C15a C16a C17a . . . 120.4(8) N5a C17a C16a . . . 107.1(7) N5a C17a C18a . . . 130.2(8) C16a C17a C18a . . . 122.6(9) C17a C18a C19a . . . 116.4(8) C14a C19a C18a . . . 122.4(8) N4a C20a N5a . . . 110.7(8) N4a C20a C21a . . . 121.6(7) N5a C20a C21a . . . 127.7(8) N6a C21a C20a . . . 113.1(8) N6a C21a C22a . . . 121.0(9) C20a C21a C22a . . . 125.8(7) C21a C22a C23a . . . 118.7(8) C22a C23a C24a . . . 120.1(10) C23a C24a C25a . . . 118.5(9) N6a C25a C24a . . . 121.9(7) N6a C25a C26a . . . 112.1(8) C24a C25a C26a . . . 125.4(8) O1a C26a N7a . . . 120.5(7) O1a C26a C25a . . . 117.9(8) N7a C26a C25a . . . 121.6(9) N7a C27a C28a . . . 113.5(10) N7a C29a C30a . . . 112.0(8) N8a C31a N9a . . . 113.3(8) N8a C31a C5a . . . 120.2(8) N9a C31a C5a . . . 126.4(7) N8a C32a C33a . . . 130.7(8) N8a C32a C37a . . . 109.7(7) C33a C32a C37a . . . 119.6(9) C32a C33a C34a . . . 118.2(8) C33a C34a C35a . . . 120.5(8) C33a C34a C38a . . . 120.1(8) C35a C34a C38a . . . 119.4(9) C34a C35a C36a . . . 122.2(10) C35a C36a C37a . . . 115.9(9) N9a C37a C32a . . . 106.2(9) N9a C37a C36a . . . 130.1(8) C32a C37a C36a . . . 123.7(9) C34a C38a C39a . . . 114.4(9) C38a C39a C40a . . . 119.2(7) C38a C39a C44a . . . 121.1(9) C40a C39a C44a . . . 119.7(9) C39a C40a C41a . . . 118.0(8) N10a C41a C40a . . . 128.8(8) N10a C41a C42a . . . 110.1(8) C40a C41a C42a . . . 121.1(9) N11a C42a C41a . . . 106.6(8) N11a C42a C43a . . . 131.3(8) C41a C42a C43a . . . 122.1(9) C42a C43a C44a . . . 116.4(8) C39a C44a C43a . . . 122.5(10) N10a C45a N11a . . . 111.0(9) N10a C45a C46a . . . 119.7(8) N11a C45a C46a . . . 129.2(8) N12a C46a C45a . . . 112.6(9) N12a C46a C47a . . . 123.0(11) C45a C46a C47a . . . 124.2(10) C46a C47a C48a . . . 116.7(11) C47a C48a C49a . . . 120.8(12) C48a C49a C50a . . . 118.9(13) N12a C50a C49a . . . 121.8(11) N12a C50a C51a . . . 110.0(10) C49a C50a C51a . . . 127.9(12) O2a C51a N13a . . . 118.6(10) O2a C51a C50a . . . 117.1(10) N13a C51a C50a . . . 124.2(10) N13a C52a C53a . . . 115.2(19) N13a C52a C53a' . . . 129(4) C53a C52a C53a' . . . 90(4) N13a C54a C55a . . . 112.9(13) N3a C56a C57a . . . 113.7(9) N5a C58a C59a . . . 110.7(10) N9a C60a C61a . . . 112.4(8) N11a C62a C63a . . . 113.1(10) Eu2 O1b C26b . . . 126.4(7) Eu3 O2b C51b . . . 125.3(7) Eu1 N1b C1b . . . 119.2(5) Eu1 N1b C5b . . . 122.1(6) C1b N1b C5b . . . 118.7(8) Eu1 N2b C6b . . . 110.4(5) Eu1 N2b C7b . . . 130.5(6) C6b N2b C7b . . . 104.7(7) C6b N3b C12b . . . 107.5(8) C6b N3b C56b . . . 128.3(8) C12b N3b C56b . . . 123.2(6) Eu2 N4b C16b . . . 133.8(6) Eu2 N4b C20b . . . 119.4(6) C16b N4b C20b . . . 106.2(8) C17b N5b C20b . . . 105.8(8) C17b N5b C58b . . . 123.0(8) C20b N5b C58b . . . 131.2(8) C21b N6b C25b . . . 119.8(8) C26b N7b C27b . . . 126.5(10) C26b N7b C29b . . . 118.8(9) C27b N7b C29b . . . 114.5(9) Eu1 N8b C31b . . . 115.2(5) Eu1 N8b C32b . . . 131.4(6) C31b N8b C32b . . . 105.0(6) C31b N9b C37b . . . 107.7(8) C31b N9b C60b . . . 128.2(9) C37b N9b C60b . . . 123.5(7) C41b N10b C45b . . . 105.4(8) C42b N11b C45b . . . 107.7(8) C42b N11b C62b . . . 123.5(9) C45b N11b C62b . . . 126.9(8) Eu3 N12b C46b . . . 120.9(6) Eu3 N12b C50b . . . 120.5(6) C46b N12b C50b . . . 118.1(7) C51b N13b C52b . . . 127.1(10) C51b N13b C54b . . . 117.4(10) C52b N13b C54b . . . 112.7(10) N1b C1b C2b . . . 121.9(7) N1b C1b C6b . . . 114.2(8) C2b C1b C6b . . . 123.9(8) C1b C2b C3b . . . 118.7(9) C2b C3b C4b . . . 119.7(11) C3b C4b C5b . . . 119.2(8) N1b C5b C4b . . . 121.6(8) N1b C5b C31b . . . 112.2(8) C4b C5b C31b . . . 125.8(7) N2b C6b N3b . . . 112.3(7) N2b C6b C1b . . . 118.1(7) N3b C6b C1b . . . 129.2(9) N2b C7b C8b . . . 129.3(8) N2b C7b C12b . . . 109.2(8) C8b C7b C12b . . . 121.5(7) C7b C8b C9b . . . 117.6(8) C8b C9b C10b . . . 120.2(9) C8b C9b C13b . . . 121.4(9) C10b C9b C13b . . . 118.3(7) C9b C10b C11b . . . 123.3(7) C10b C11b C12b . . . 115.4(8) N3b C12b C7b . . . 106.2(7) N3b C12b C11b . . . 132.1(9) C7b C12b C11b . . . 121.8(9) C9b C13b C14b . . . 116.8(7) C13b C14b C15b . . . 120.1(9) C13b C14b C19b . . . 119.9(8) C15b C14b C19b . . . 119.9(9) C14b C15b C16b . . . 118.7(9) N4b C16b C15b . . . 130.6(9) N4b C16b C17b . . . 109.6(8) C15b C16b C17b . . . 119.8(8) N5b C17b C16b . . . 106.6(8) N5b C17b C18b . . . 130.3(10) C16b C17b C18b . . . 123.1(9) C17b C18b C19b . . . 116.0(10) C14b C19b C18b . . . 122.3(9) N4b C20b N5b . . . 111.8(7) N4b C20b C21b . . . 122.1(8) N5b C20b C21b . . . 126.1(8) N6b C21b C20b . . . 112.8(8) N6b C21b C22b . . . 119.9(9) C20b C21b C22b . . . 127.1(9) C21b C22b C23b . . . 120.7(10) C22b C23b C24b . . . 119.8(10) C23b C24b C25b . . . 116.8(10) N6b C25b C24b . . . 123.0(10) N6b C25b C26b . . . 112.0(8) C24b C25b C26b . . . 124.6(9) O1b C26b N7b . . . 121.0(10) O1b C26b C25b . . . 115.5(8) N7b C26b C25b . . . 123.4(9) N7b C27b C28b . . . 112.7(12) N7b C29b C30b . . . 111.6(12) N8b C31b N9b . . . 113.1(8) N8b C31b C5b . . . 118.7(7) N9b C31b C5b . . . 127.8(9) N8b C32b C33b . . . 130.3(7) N8b C32b C37b . . . 108.0(8) C33b C32b C37b . . . 121.6(7) C32b C33b C34b . . . 118.6(7) C33b C34b C35b . . . 118.6(9) C33b C34b C38b . . . 121.5(8) C35b C34b C38b . . . 119.9(8) C34b C35b C36b . . . 123.5(8) C35b C36b C37b . . . 117.2(8) N9b C37b C32b . . . 106.2(7) N9b C37b C36b . . . 133.6(9) C32b C37b C36b . . . 120.1(9) C34b C38b C39b . . . 118.6(8) C38b C39b C40b . . . 123.1(9) C38b C39b C44b . . . 117.4(9) C40b C39b C44b . . . 119.5(8) C39b C40b C41b . . . 119.0(9) N10b C41b C40b . . . 130.4(9) N10b C41b C42b . . . 109.2(8) C40b C41b C42b . . . 120.4(8) N11b C42b C41b . . . 106.0(8) N11b C42b C43b . . . 131.7(10) C41b C42b C43b . . . 122.2(8) C42b C43b C44b . . . 116.4(10) C39b C44b C43b . . . 122.5(9) N10b C45b N11b . . . 111.4(7) N10b C45b C46b . . . 121.3(9) N11b C45b C46b . . . 127.1(8) N12b C46b C45b . . . 112.6(7) N12b C46b C47b . . . 123.2(9) C45b C46b C47b . . . 124.0(9) C46b C47b C48b . . . 115.5(10) C47b C48b C49b . . . 120.8(8) C48b C49b C50b . . . 119.2(9) N12b C50b C49b . . . 122.3(10) N12b C50b C51b . . . 110.0(7) C49b C50b C51b . . . 127.7(9) O2b C51b N13b . . . 121.6(10) O2b C51b C50b . . . 115.7(9) N13b C51b C50b . . . 122.7(9) N13b C52b C53b . . . 113.6(10) N13b C54b C55b . . . 106.9(18) N3b C56b C57b . . . 115.9(9) N5b C58b C59b . . . 110.9(7) N9b C60b C61b . . . 112.4(10) N11b C62b C63b . . . 111.1(10) Eu2 O1c C26c . . . 123.3(7) Eu3 O2c C51c . . . 122.9(6) Eu1 N1c C1c . . . 119.0(6) Eu1 N1c C5c . . . 122.7(5) C1c N1c C5c . . . 118.3(7) Eu1 N2c C6c . . . 113.3(6) Eu1 N2c C7c . . . 133.2(6) C6c N2c C7c . . . 103.9(6) C6c N3c C12c . . . 106.9(6) C6c N3c C56c . . . 129.4(8) C12c N3c C56c . . . 123.2(7) C16c N4c C20c . . . 104.3(7) C17c N5c C20c . . . 105.9(6) C17c N5c C58c . . . 123.5(8) C20c N5c C58c . . . 130.4(7) C21c N6c C25c . . . 116.6(7) C26c N7c C27c . . . 124.6(9) C26c N7c C29c . . . 118.3(9) C27c N7c C29c . . . 116.8(9) Eu1 N8c C31c . . . 118.0(6) Eu1 N8c C32c . . . 133.9(6) C31c N8c C32c . . . 105.3(8) C31c N9c C37c . . . 106.1(8) C31c N9c C60c . . . 129.4(7) C37c N9c C60c . . . 124.4(8) Eu3 N10c C41c . . . 127.3(7) Eu3 N10c C45c . . . 111.7(6) C41c N10c C45c . . . 105.8(7) C42c N11c C45c . . . 104.4(8) C42c N11c C62c . . . 124.4(7) C45c N11c C62c . . . 129.8(8) Eu3 N12c C46c . . . 121.5(6) Eu3 N12c C50c . . . 119.0(7) C46c N12c C50c . . . 118.7(9) C51c N13c C52c . . . 121.9(12) C51c N13c C54c . . . 119.2(11) C52c N13c C54c . . . 114.2(11) N1c C1c C2c . . . 122.3(9) N1c C1c C6c . . . 113.8(7) C2c C1c C6c . . . 123.3(8) C1c C2c C3c . . . 117.8(9) C2c C3c C4c . . . 120.3(10) C3c C4c C5c . . . 118.8(10) N1c C5c C4c . . . 122.3(8) N1c C5c C31c . . . 113.1(8) C4c C5c C31c . . . 124.4(9) N2c C6c N3c . . . 113.3(8) N2c C6c C1c . . . 120.2(7) N3c C6c C1c . . . 126.4(7) N2c C7c C8c . . . 128.5(7) N2c C7c C12c . . . 111.0(8) C8c C7c C12c . . . 120.6(9) C7c C8c C9c . . . 116.6(7) C8c C9c C10c . . . 120.8(9) C8c C9c C13c . . . 119.7(7) C10c C9c C13c . . . 119.5(9) C9c C10c C11c . . . 122.9(9) C10c C11c C12c . . . 115.6(8) N3c C12c C7c . . . 104.9(8) N3c C12c C11c . . . 131.8(7) C7c C12c C11c . . . 123.3(9) C9c C13c C14c . . . 115.9(8) C13c C14c C15c . . . 119.3(8) C13c C14c C19c . . . 120.7(9) C15c C14c C19c . . . 120.0(7) C14c C15c C16c . . . 117.8(7) N4c C16c C15c . . . 130.3(8) N4c C16c C17c . . . 110.2(6) C15c C16c C17c . . . 119.5(8) N5c C17c C16c . . . 106.5(8) N5c C17c C18c . . . 129.7(8) C16c C17c C18c . . . 123.7(7) C17c C18c C19c . . . 115.4(9) C14c C19c C18c . . . 123.3(10) N4c C20c N5c . . . 113.1(7) N4c C20c C21c . . . 121.1(8) N5c C20c C21c . . . 125.7(7) N6c C21c C20c . . . 112.1(7) N6c C21c C22c . . . 122.2(8) C20c C21c C22c . . . 125.7(9) C21c C22c C23c . . . 118.5(9) C22c C23c C24c . . . 120.4(8) C23c C24c C25c . . . 117.4(9) N6c C25c C24c . . . 124.8(9) N6c C25c C26c . . . 109.4(7) C24c C25c C26c . . . 125.5(9) O1c C26c N7c . . . 122.2(9) O1c C26c C25c . . . 116.2(9) N7c C26c C25c . . . 121.6(8) N7c C27c C28c . . . 112.3(9) N7c C29c C30c . . . 112.6(10) N8c C31c N9c . . . 111.8(7) N8c C31c C5c . . . 120.4(8) N9c C31c C5c . . . 127.5(8) N8c C32c C33c . . . 129.0(9) N8c C32c C37c . . . 109.4(8) C33c C32c C37c . . . 121.6(8) C32c C33c C34c . . . 118.4(9) C33c C34c C35c . . . 118.8(9) C33c C34c C38c . . . 120.2(9) C35c C34c C38c . . . 121.0(8) C34c C35c C36c . . . 123.8(9) C35c C36c C37c . . . 115.9(10) N9c C37c C32c . . . 107.4(8) N9c C37c C36c . . . 131.1(10) C32c C37c C36c . . . 121.4(9) C34c C38c C39c . . . 115.8(7) C38c C39c C40c . . . 120.6(8) C38c C39c C44c . . . 119.1(7) C40c C39c C44c . . . 120.3(9) C39c C40c C41c . . . 118.5(8) N10c C41c C40c . . . 130.4(8) N10c C41c C42c . . . 108.9(9) C40c C41c C42c . . . 120.8(7) N11c C42c C41c . . . 107.6(7) N11c C42c C43c . . . 131.4(9) C41c C42c C43c . . . 120.9(9) C42c C43c C44c . . . 117.4(9) C39c C44c C43c . . . 122.1(8) N10c C45c N11c . . . 113.2(8) N10c C45c C46c . . . 120.9(8) N11c C45c C46c . . . 125.9(9) N12c C46c C45c . . . 112.1(10) N12c C46c C47c . . . 122.6(9) C45c C46c C47c . . . 125.3(9) C46c C47c C48c . . . 118.1(11) C47c C48c C49c . . . 119.7(13) C48c C49c C50c . . . 118.6(10) N12c C50c C49c . . . 121.9(9) N12c C50c C51c . . . 111.7(9) C49c C50c C51c . . . 125.7(9) O2c C51c N13c . . . 121.5(10) O2c C51c C50c . . . 114.7(7) N13c C51c C50c . . . 123.8(10) N13c C52c C53c . . . 94(3) N13c C54c C55c . . . 104.1(16) N3c C56c C57c . . . 114.6(8) N5c C58c C59c . . . 113.4(8) N9c C60c C61c . . . 113.3(9) N11c C62c C63c . . . 112.5(9) O1d S1d O2d . . . 111.0(10) O1d S1d O3d . . . 112.7(8) O1d S1d C1d . . . 101.6(9) O2d S1d O3d . . . 115.4(10) O2d S1d C1d . . . 104.6(9) O3d S1d C1d . . . 110.3(8) S1d C1d F1d . . . 111.2(11) S1d C1d F2d . . . 109.9(12) S1d C1d F3d . . . 108.3(10) F1d C1d F2d . . . 108.2(12) F1d C1d F3d . . . 106.0(12) F2d C1d F3d . . . 113.1(15) O1e S1e O2e . . . 115.2(6) O1e S1e O3e . . . 115.1(7) O1e S1e C1e . . . 103.2(6) O2e S1e O3e . . . 116.9(7) O2e S1e C1e . . . 102.6(6) O3e S1e C1e . . . 100.5(6) S1e C1e F1e . . . 110.8(8) S1e C1e F2e . . . 111.3(8) S1e C1e F3e . . . 110.5(9) F1e C1e F2e . . . 106.8(10) F1e C1e F3e . . . 108.9(9) F2e C1e F3e . . . 108.4(10) O1f S1f O2f . . . 114.9(9) O1f S1f O3f . . . 115.1(9) O1f S1f C1f . . . 103.8(9) O2f S1f O3f . . . 113.9(9) O2f S1f C1f . . . 103.2(8) O3f S1f C1f . . . 104.0(9) S1f C1f F1f . . . 112.9(11) S1f C1f F2f . . . 106.1(13) S1f C1f F3f . . . 114.8(12) F1f C1f F2f . . . 107.0(14) F1f C1f F3f . . . 108.4(15) F2f C1f F3f . . . 107.2(13) O1g S1g O2g . . . 112.7(6) O1g S1g O3g . . . 115.4(5) O1g S1g C1g . . . 104.5(6) O2g S1g O3g . . . 114.4(5) O2g S1g C1g . . . 103.9(5) O3g S1g C1g . . . 104.2(6) S1g C1g F1g . . . 111.5(9) S1g C1g F2g . . . 112.7(9) S1g C1g F3g . . . 110.4(9) F1g C1g F2g . . . 107.4(10) F1g C1g F3g . . . 107.0(12) F2g C1g F3g . . . 107.5(10) O1h S1h O2h . . . 115.9(7) O1h S1h O3h . . . 113.3(6) O1h S1h C1h . . . 102.5(6) O2h S1h O3h . . . 114.1(6) O2h S1h C1h . . . 104.8(7) O3h S1h C1h . . . 104.4(5) S1h C1h F1h . . . 111.4(9) S1h C1h F2h . . . 112.1(8) S1h C1h F3h . . . 112.2(8) F1h C1h F2h . . . 107.9(9) F1h C1h F3h . . . 106.7(11) F2h C1h F3h . . . 106.1(10) O1i S1i O2i . . . 114(3) O1i S1i O3i . . . 113(3) O1i S1i C1i . . . 103.6(14) O2i S1i O3i . . . 116(3) O2i S1i C1i . . . 107.0(14) O3i S1i C1i . . . 101.6(11) S1i C1i F1i . . . 105.3(12) S1i C1i F2i . . . 113.1(16) S1i C1i F3i . . . 117.7(16) F1i C1i F2i . . . 102(3) F1i C1i F3i . . . 106(3) F2i C1i F3i . . . 110(3) O1i' S1i O2i' . . . 114.6(14) O1i' S1i O3i' . . . 114.5(12) O1i' S1i C1i . . . 103.2(10) O2i' S1i O3i' . . . 110.3(11) O2i' S1i C1i . . . 105.0(10) O3i' S1i C1i . . . 108.3(9) S1i C1i F1i' . . . 111.5(12) S1i C1i F2i' . . . 115.7(14) S1i C1i F3i' . . . 104.9(10) F1i' C1i F2i' . . . 112.5(17) F1i' C1i F3i' . . . 102.9(16) F2i' C1i F3i' . . . 108.0(18) O1j S1j O2j . . . 114.1(16) O1j S1j O3j . . . 113.9(16) O1j S1j C1j . . . 104.5(12) O2j S1j O3j . . . 115.1(13) O2j S1j C1j . . . 103.2(12) O3j S1j C1j . . . 104.2(11) S1j C1j F1j . . . 109.5(15) S1j C1j F2j . . . 112.2(13) S1j C1j F3j . . . 108(3) F1j C1j F2j . . . 110(2) F1j C1j F3j . . . 109(2) F2j C1j F3j . . . 108(3) O1j' S1j O2j' . . . 113.1(18) O1j' S1j O3j' . . . 114.1(14) O1j' S1j C1j' . . . 107.2(14) O2j' S1j O3j' . . . 108.6(13) O2j' S1j C1j' . . . 109.5(15) O3j' S1j C1j' . . . 103.9(10) S1j C1j' F1j' . . . 110.3(15) S1j C1j' F2j' . . . 108.0(15) S1j C1j' F3j' . . . 110.2(16) F1j' C1j' F2j' . . . 109(2) F1j' C1j' F3j' . . . 110.1(17) F2j' C1j' F3j' . . . 109(2) O1k S1k O2k . . . 120.5(11) O1k S1k O3k . . . 97.0(12) O1k S1k C1k . . . 105.7(11) O2k S1k O3k . . . 119.6(10) O2k S1k C1k . . . 104.8(11) O3k S1k C1k . . . 108.1(10) S1k C1k F1k . . . 112.8(15) S1k C1k F2k . . . 114.6(17) S1k C1k F3k . . . 97.1(15) F1k C1k F2k . . . 106.0(18) F1k C1k F3k . . . 116(3) F2k C1k F3k . . . 110(2) O1k' S1k O2k' . . . 111.7(17) O1k' S1k O3k' . . . 108.9(13) O1k' S1k C1k' . . . 113.0(12) O2k' S1k O3k' . . . 117.5(14) O2k' S1k C1k' . . . 103.8(11) O3k' S1k C1k' . . . 101.6(9) S1k C1k' F1k' . . . 107.4(11) S1k C1k' F2k' . . . 109.0(11) S1k C1k' F3k' . . . 117.2(13) F1k' C1k' F2k' . . . 111.7(17) F1k' C1k' F3k' . . . 104.3(12) F2k' C1k' F3k' . . . 107.2(15) O1l S1l O2l . . . 113.3(15) O1l S1l O3l . . . 112.2(16) O1l S1l C1l . . . 99.6(12) O2l S1l O3l . . . 109.2(16) O2l S1l C1l . . . 105.1(15) O3l S1l C1l . . . 117.2(15) S1l C1l F1l . . . 109.6(19) S1l C1l F2l . . . 113.0(16) S1l C1l F3l . . . 108.4(18) F1l C1l F2l . . . 106(3) F1l C1l F3l . . . 106(2) F2l C1l F3l . . . 113(3) O1l' S1l O2l' . . . 118(3) O1l' S1l O3l' . . . 111(3) O1l' S1l C1l' . . . 112(2) O2l' S1l O3l' . . . 109(3) O2l' S1l C1l' . . . 102.0(18) O3l' S1l C1l' . . . 104(3) S1l C1l' F1l' . . . 115(3) S1l C1l' F2l' . . . 107(3) S1l C1l' F3l' . . . 110(3) F1l' C1l' F2l' . . . 109(4) F1l' C1l' F3l' . . . 107(4) F2l' C1l' F3l' . . . 108(4) O1l'' S1l O2l'' . . . 107.9(16) O1l'' S1l O3l'' . . . 113(2) O1l'' S1l C1l' . . . 114.4(14) O2l'' S1l O3l'' . . . 116(2) O2l'' S1l C1l' . . . 99.2(15) O3l'' S1l C1l' . . . 105.8(19) S1l C1l' F1l'' . . . 103(3) S1l C1l' F2l'' . . . 117(3) S1l C1l' F3l'' . . . 112(3) F1l'' C1l' F2l'' . . . 107(3) F1l'' C1l' F3l'' . . . 108(3) F2l'' C1l' F3l'' . . . 109(3) N1m C1m C2m . . . 174(3) N1n C1n C2n . . . 176.9(17) N1o C1o C2o . . . 167(3) N1p C1p C2p . . . 173(2) N1q C1q C2q . . . 170(3) N1r C1r C2r . . . 178(3) N1s C1s C2s . . . 175.0(16) N1t C1t C2t . . . 176(3) N1u C1u C2u . . . 177(5) N1v C1v C2v . . . 161(7) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion O1a Eu2 Eu3 O2a . . . . 140.5(3) O1b Eu2 Eu3 O2b . . . . 158.4(4) O1c Eu2 Eu3 O2c . . . . 152.8(4) N2a Eu1 N1a C1a . . . . 9.3(6) N2a Eu1 N1a C5a . . . . -160.1(7) N8a Eu1 N1a C1a . . . . -172.1(7) N8a Eu1 N1a C5a . . . . 18.5(6) N1b Eu1 N1a C1a . . . . 143.4(6) N1b Eu1 N1a C5a . . . . -26.0(7) N2b Eu1 N1a C1a . . . . 98.8(7) N2b Eu1 N1a C5a . . . . -70.6(7) N8b Eu1 N1a C1a . . . . -136.8(6) N8b Eu1 N1a C5a . . . . 53.8(8) N1c Eu1 N1a C1a . . . . -38.4(7) N1c Eu1 N1a C5a . . . . 152.2(6) N2c Eu1 N1a C1a . . . . 48.1(8) N2c Eu1 N1a C5a . . . . -121.3(7) N8c Eu1 N1a C1a . . . . -76.1(7) N8c Eu1 N1a C5a . . . . 114.5(7) N1a Eu1 N2a C6a . . . . -23.3(6) N1a Eu1 N2a C7a . . . . -165.3(8) N8a Eu1 N2a C6a . . . . -24.9(7) N8a Eu1 N2a C7a . . . . -166.8(7) N1b Eu1 N2a C6a . . . . -126.9(6) N1b Eu1 N2a C7a . . . . 91.2(8) N2b Eu1 N2a C6a . . . . -97.3(6) N2b Eu1 N2a C7a . . . . 120.7(8) N8b Eu1 N2a C6a . . . . 118.4(6) N8b Eu1 N2a C7a . . . . -23.5(10) N1c Eu1 N2a C6a . . . . 116.2(6) N1c Eu1 N2a C7a . . . . -25.8(8) N2c Eu1 N2a C6a . . . . -179.7(6) N2c Eu1 N2a C7a . . . . 38.4(8) N8c Eu1 N2a C6a . . . . 52.4(6) N8c Eu1 N2a C7a . . . . -89.5(8) N1a Eu1 N8a C31a . . . . -15.3(7) N1a Eu1 N8a C32a . . . . 174.1(9) N2a Eu1 N8a C31a . . . . -13.7(8) N2a Eu1 N8a C32a . . . . 175.6(8) N1b Eu1 N8a C31a . . . . 123.8(7) N1b Eu1 N8a C32a . . . . -46.9(8) N2b Eu1 N8a C31a . . . . 59.1(7) N2b Eu1 N8a C32a . . . . -111.5(8) N8b Eu1 N8a C31a . . . . -173.4(7) N8b Eu1 N8a C32a . . . . 15.9(8) N1c Eu1 N8a C31a . . . . -123.5(7) N1c Eu1 N8a C32a . . . . 65.9(9) N2c Eu1 N8a C31a . . . . 122.7(7) N2c Eu1 N8a C32a . . . . -48.0(9) N8c Eu1 N8a C31a . . . . -86.7(7) N8c Eu1 N8a C32a . . . . 102.6(8) N1a Eu1 N1b C1b . . . . -30.5(7) N1a Eu1 N1b C5b . . . . 149.8(6) N2a Eu1 N1b C1b . . . . 51.1(7) N2a Eu1 N1b C5b . . . . -128.6(7) N8a Eu1 N1b C1b . . . . -71.7(6) N8a Eu1 N1b C5b . . . . 108.7(7) N2b Eu1 N1b C1b . . . . 17.9(6) N2b Eu1 N1b C5b . . . . -161.7(7) N8b Eu1 N1b C1b . . . . -165.2(7) N8b Eu1 N1b C5b . . . . 15.1(6) N1c Eu1 N1b C1b . . . . 151.2(6) N1c Eu1 N1b C5b . . . . -28.5(8) N2c Eu1 N1b C1b . . . . 107.6(7) N2c Eu1 N1b C5b . . . . -72.0(7) N8c Eu1 N1b C1b . . . . -127.8(6) N8c Eu1 N1b C5b . . . . 52.5(8) N1a Eu1 N2b C6b . . . . 105.6(6) N1a Eu1 N2b C7b . . . . -26.8(7) N2a Eu1 N2b C6b . . . . 170.6(6) N2a Eu1 N2b C7b . . . . 38.1(7) N8a Eu1 N2b C6b . . . . 42.0(5) N8a Eu1 N2b C7b . . . . -90.4(7) N1b Eu1 N2b C6b . . . . -30.5(5) N1b Eu1 N2b C7b . . . . -163.0(8) N8b Eu1 N2b C6b . . . . -33.9(6) N8b Eu1 N2b C7b . . . . -166.4(7) N1c Eu1 N2b C6b . . . . -135.4(5) N1c Eu1 N2b C7b . . . . 92.2(7) N2c Eu1 N2b C6b . . . . -104.2(6) N2c Eu1 N2b C7b . . . . 123.3(7) N8c Eu1 N2b C6b . . . . 113.9(6) N8c Eu1 N2b C7b . . . . -18.5(9) N1a Eu1 N8b C31b . . . . -127.3(6) N1a Eu1 N8b C32b . . . . 90.1(8) N2a Eu1 N8b C31b . . . . 112.8(7) N2a Eu1 N8b C32b . . . . -29.8(9) N8a Eu1 N8b C31b . . . . -96.3(6) N8a Eu1 N8b C32b . . . . 121.1(7) N1b Eu1 N8b C31b . . . . -25.3(6) N1b Eu1 N8b C32b . . . . -167.9(8) N2b Eu1 N8b C31b . . . . -21.9(7) N2b Eu1 N8b C32b . . . . -164.5(7) N1c Eu1 N8b C31b . . . . 115.1(7) N1c Eu1 N8b C32b . . . . -27.5(7) N2c Eu1 N8b C31b . . . . 49.6(6) N2c Eu1 N8b C32b . . . . -93.0(7) N8c Eu1 N8b C31b . . . . 176.5(6) N8c Eu1 N8b C32b . . . . 33.9(7) N1a Eu1 N1c C1c . . . . 150.2(6) N1a Eu1 N1c C5c . . . . -28.7(7) N2a Eu1 N1c C1c . . . . 106.7(6) N2a Eu1 N1c C5c . . . . -72.2(7) N8a Eu1 N1c C1c . . . . -125.8(6) N8a Eu1 N1c C5c . . . . 55.3(8) N1b Eu1 N1c C1c . . . . -31.5(7) N1b Eu1 N1c C5c . . . . 149.6(6) N2b Eu1 N1c C1c . . . . 50.3(7) N2b Eu1 N1c C5c . . . . -128.6(6) N8b Eu1 N1c C1c . . . . -71.9(6) N8b Eu1 N1c C5c . . . . 109.2(7) N2c Eu1 N1c C1c . . . . 15.4(6) N2c Eu1 N1c C5c . . . . -163.5(7) N8c Eu1 N1c C1c . . . . -168.4(7) N8c Eu1 N1c C5c . . . . 12.7(6) N1a Eu1 N2c C6c . . . . -135.5(6) N1a Eu1 N2c C7c . . . . 85.0(8) N2a Eu1 N2c C6c . . . . -101.2(6) N2a Eu1 N2c C7c . . . . 119.3(7) N8a Eu1 N2c C6c . . . . 113.0(6) N8a Eu1 N2c C7c . . . . -26.5(8) N1b Eu1 N2c C6c . . . . 111.9(6) N1b Eu1 N2c C7c . . . . -27.6(7) N2b Eu1 N2c C6c . . . . 176.4(6) N2b Eu1 N2c C7c . . . . 36.9(7) N8b Eu1 N2c C6c . . . . 47.6(6) N8b Eu1 N2c C7c . . . . -91.9(7) N1c Eu1 N2c C6c . . . . -25.9(6) N1c Eu1 N2c C7c . . . . -165.4(7) N8c Eu1 N2c C6c . . . . -30.1(7) N8c Eu1 N2c C7c . . . . -169.6(6) N1a Eu1 N8c C31c . . . . 127.1(6) N1a Eu1 N8c C32c . . . . -30.9(7) N2a Eu1 N8c C31c . . . . 61.2(6) N2a Eu1 N8c C32c . . . . -96.8(7) N8a Eu1 N8c C31c . . . . -171.1(6) N8a Eu1 N8c C32c . . . . 30.9(7) N1b Eu1 N8c C31c . . . . -119.5(6) N1b Eu1 N8c C32c . . . . 82.5(8) N2b Eu1 N8c C31c . . . . 118.8(6) N2b Eu1 N8c C32c . . . . -39.1(9) N8b Eu1 N8c C31c . . . . -86.9(6) N8b Eu1 N8c C32c . . . . 115.1(8) N1c Eu1 N8c C31c . . . . -17.0(5) N1c Eu1 N8c C32c . . . . -175.0(8) N2c Eu1 N8c C31c . . . . -12.8(6) N2c Eu1 N8c C32c . . . . -170.7(7) N4a Eu2 O1a C26a . . . . -21.4(7) N6a Eu2 O1a C26a . . . . -18.0(6) O1b Eu2 O1a C26a . . . . -89.6(6) N4b Eu2 O1a C26a . . . . 137.2(6) O1c Eu2 O1a C26a . . . . -175.7(7) O1a Eu2 N4a C16a . . . . -177.6(7) O1a Eu2 N4a C20a . . . . -8.0(7) N6a Eu2 N4a C16a . . . . 178.9(9) N6a Eu2 N4a C20a . . . . -11.4(6) O1b Eu2 N4a C16a . . . . -112.1(8) O1b Eu2 N4a C20a . . . . 57.6(7) N4b Eu2 N4a C16a . . . . 14.7(8) N4b Eu2 N4a C20a . . . . -175.6(7) O1c Eu2 N4a C16a . . . . -45.1(10) O1c Eu2 N4a C20a . . . . 124.6(7) O1a Eu2 N6a C21a . . . . -160.6(8) O1a Eu2 N6a C25a . . . . -1.3(6) N4a Eu2 N6a C21a . . . . 16.4(7) N4a Eu2 N6a C25a . . . . 175.6(7) O1b Eu2 N6a C21a . . . . -75.8(7) O1b Eu2 N6a C25a . . . . 83.4(6) N4b Eu2 N6a C21a . . . . 45.4(9) N4b Eu2 N6a C25a . . . . -155.3(6) O1c Eu2 N6a C21a . . . . -126.6(7) O1c Eu2 N6a C25a . . . . 32.6(7) O1a Eu2 O1b C26b . . . . -164.6(8) N4a Eu2 O1b C26b . . . . 63.7(7) N6a Eu2 O1b C26b . . . . 127.6(8) N4b Eu2 O1b C26b . . . . -16.4(8) O1c Eu2 O1b C26b . . . . -83.8(7) O1a Eu2 N4b C16b . . . . -58.1(8) O1a Eu2 N4b C20b . . . . 111.4(6) N4a Eu2 N4b C16b . . . . 105.1(7) N4a Eu2 N4b C20b . . . . -85.5(6) N6a Eu2 N4b C16b . . . . 79.4(7) N6a Eu2 N4b C20b . . . . -111.1(6) O1b Eu2 N4b C16b . . . . -177.4(6) O1b Eu2 N4b C20b . . . . -7.9(6) O1c Eu2 N4b C16b . . . . -106.1(7) O1c Eu2 N4b C20b . . . . 63.4(5) O1a Eu2 O1c C26c . . . . -85.8(8) N4a Eu2 O1c C26c . . . . 130.8(8) N6a Eu2 O1c C26c . . . . -116.6(8) O1b Eu2 O1c C26c . . . . -162.7(8) N4b Eu2 O1c C26c . . . . 68.0(8) N10a Eu3 O2a C51a . . . . 11.0(10) N12a Eu3 O2a C51a . . . . 11.5(8) O2b Eu3 O2a C51a . . . . -148.0(9) N12b Eu3 O2a C51a . . . . 148.3(9) O2c Eu3 O2a C51a . . . . -60.9(9) N10c Eu3 O2a C51a . . . . 165.6(8) N12c Eu3 O2a C51a . . . . -95.3(9) O2a Eu3 N10a C41a . . . . -173.3(8) O2a Eu3 N10a C45a . . . . -.4(8) N12a Eu3 N10a C41a . . . . -173.7(9) N12a Eu3 N10a C45a . . . . -.8(7) O2b Eu3 N10a C41a . . . . -33.4(10) O2b Eu3 N10a C45a . . . . 139.5(7) N12b Eu3 N10a C41a . . . . 91.1(9) N12b Eu3 N10a C45a . . . . -96.1(7) O2c Eu3 N10a C41a . . . . -105.0(9) O2c Eu3 N10a C45a . . . . 67.9(7) N10c Eu3 N10a C41a . . . . 21.2(8) N10c Eu3 N10a C45a . . . . -165.9(7) N12c Eu3 N10a C41a . . . . -41.8(8) N12c Eu3 N10a C45a . . . . 131.0(7) O2a Eu3 N12a C46a . . . . 169.1(8) O2a Eu3 N12a C50a . . . . 7.9(7) N10a Eu3 N12a C46a . . . . -11.3(7) N10a Eu3 N12a C50a . . . . -172.4(8) O2b Eu3 N12a C46a . . . . -158.6(7) O2b Eu3 N12a C50a . . . . 40.3(8) N12b Eu3 N12a C46a . . . . 125.9(7) N12b Eu3 N12a C50a . . . . -35.3(8) O2c Eu3 N12a C46a . . . . -105.7(8) O2c Eu3 N12a C50a . . . . 93.1(7) N10c Eu3 N12a C46a . . . . 16.7(10) N10c Eu3 N12a C50a . . . . -144.4(7) N12c Eu3 N12a C46a . . . . -68.0(8) N12c Eu3 N12a C50a . . . . 130.8(7) O2a Eu3 O2b C51b . . . . -54.0(8) N10a Eu3 O2b C51b . . . . 157.9(7) N12a Eu3 O2b C51b . . . . -82.9(8) N12b Eu3 O2b C51b . . . . 13.2(7) O2c Eu3 O2b C51b . . . . -130.8(8) N10c Eu3 O2b C51b . . . . 99.8(8) N12c Eu3 O2b C51b . . . . 166.8(8) O2a Eu3 N12b C46b . . . . -92.0(8) O2a Eu3 N12b C50b . . . . 97.0(8) N10a Eu3 N12b C46b . . . . 25.8(9) N10a Eu3 N12b C50b . . . . -145.2(7) N12a Eu3 N12b C46b . . . . -50.0(8) N12a Eu3 N12b C50b . . . . 138.9(7) O2b Eu3 N12b C46b . . . . 175.1(8) O2b Eu3 N12b C50b . . . . 4.1(7) O2c Eu3 N12b C46b . . . . -132.2(7) O2c Eu3 N12b C50b . . . . 56.8(8) N10c Eu3 N12b C46b . . . . 98.2(7) N10c Eu3 N12b C50b . . . . -72.8(7) N12c Eu3 N12b C46b . . . . 144.8(7) N12c Eu3 N12b C50b . . . . -26.3(8) O2a Eu3 O2c C51c . . . . -176.4(8) N10a Eu3 O2c C51c . . . . 54.5(7) N12a Eu3 O2c C51c . . . . 117.5(8) O2b Eu3 O2c C51c . . . . -93.9(7) N12b Eu3 O2c C51c . . . . -139.0(7) N10c Eu3 O2c C51c . . . . -27.8(8) N12c Eu3 O2c C51c . . . . -25.6(7) O2a Eu3 N10c C41c . . . . -36.6(10) O2a Eu3 N10c C45c . . . . 95.7(7) N10a Eu3 N10c C41c . . . . 123.0(8) N10a Eu3 N10c C45c . . . . -104.7(6) N12a Eu3 N10c C41c . . . . 98.3(8) N12a Eu3 N10c C45c . . . . -129.4(6) O2b Eu3 N10c C41c . . . . -84.9(7) O2b Eu3 N10c C45c . . . . 47.4(6) N12b Eu3 N10c C41c . . . . -20.6(7) N12b Eu3 N10c C45c . . . . 111.8(6) O2c Eu3 N10c C41c . . . . -156.4(7) O2c Eu3 N10c C45c . . . . -24.1(7) N12c Eu3 N10c C41c . . . . -158.7(8) N12c Eu3 N10c C45c . . . . -26.4(6) O2a Eu3 N12c C46c . . . . -122.2(8) O2a Eu3 N12c C50c . . . . 47.3(8) N10a Eu3 N12c C46c . . . . 110.5(8) N10a Eu3 N12c C50c . . . . -80.0(8) N12a Eu3 N12c C46c . . . . 159.8(7) N12a Eu3 N12c C50c . . . . -30.7(8) O2b Eu3 N12c C46c . . . . -64.5(8) O2b Eu3 N12c C50c . . . . 105.0(8) N12b Eu3 N12c C46c . . . . -35.7(9) N12b Eu3 N12c C50c . . . . 133.8(7) O2c Eu3 N12c C46c . . . . -160.4(9) O2c Eu3 N12c C50c . . . . 9.1(7) N10c Eu3 N12c C46c . . . . 17.5(7) N10c Eu3 N12c C50c . . . . -173.0(8) Eu2 O1a C26a N7a . . . . -145.0(7) Eu2 O1a C26a C25a . . . . 35.1(11) Eu3 O2a C51a N13a . . . . 149.3(9) Eu3 O2a C51a C50a . . . . -28.3(14) Eu1 N1a C1a C2a . . . . -169.1(8) Eu1 N1a C1a C6a . . . . 5.0(10) C5a N1a C1a C2a . . . . .7(14) C5a N1a C1a C6a . . . . 174.7(8) Eu1 N1a C5a C4a . . . . 166.4(8) Eu1 N1a C5a C31a . . . . -19.4(10) C1a N1a C5a C4a . . . . -3.2(13) C1a N1a C5a C31a . . . . 171.0(8) Eu1 N2a C6a N3a . . . . -148.4(6) Eu1 N2a C6a C1a . . . . 38.1(9) C7a N2a C6a N3a . . . . 2.6(9) C7a N2a C6a C1a . . . . -170.9(7) Eu1 N2a C7a C8a . . . . -44.5(13) Eu1 N2a C7a C12a . . . . 141.1(6) C6a N2a C7a C8a . . . . 171.2(9) C6a N2a C7a C12a . . . . -3.3(9) C12a N3a C6a N2a . . . . -.9(10) C12a N3a C6a C1a . . . . 171.9(9) C56a N3a C6a N2a . . . . 180.0(8) C56a N3a C6a C1a . . . . -7.3(15) C6a N3a C12a C7a . . . . -1.3(9) C6a N3a C12a C11a . . . . -179.2(10) C56a N3a C12a C7a . . . . 178.0(8) C56a N3a C12a C11a . . . . .0(15) C6a N3a C56a C57a . . . . -55.4(13) C12a N3a C56a C57a . . . . 125.6(10) Eu2 N4a C16a C15a . . . . -7.6(15) Eu2 N4a C16a C17a . . . . 171.3(6) C20a N4a C16a C15a . . . . -178.1(10) C20a N4a C16a C17a . . . . .8(10) Eu2 N4a C20a N5a . . . . -174.3(6) Eu2 N4a C20a C21a . . . . 7.5(11) C16a N4a C20a N5a . . . . -1.9(10) C16a N4a C20a C21a . . . . 179.9(9) C20a N5a C17a C16a . . . . -1.7(10) C20a N5a C17a C18a . . . . 176.3(10) C58a N5a C17a C16a . . . . 178.1(9) C58a N5a C17a C18a . . . . -3.9(16) C17a N5a C20a N4a . . . . 2.2(10) C17a N5a C20a C21a . . . . -179.7(9) C58a N5a C20a N4a . . . . -177.6(9) C58a N5a C20a C21a . . . . .5(16) C17a N5a C58a C59a . . . . 88.8(12) C20a N5a C58a C59a . . . . -91.4(12) Eu2 N6a C21a C20a . . . . -18.7(11) Eu2 N6a C21a C22a . . . . 157.0(8) C25a N6a C21a C20a . . . . -177.1(8) C25a N6a C21a C22a . . . . -1.4(14) Eu2 N6a C25a C24a . . . . -155.3(8) Eu2 N6a C25a C26a . . . . 16.3(10) C21a N6a C25a C24a . . . . 4.3(14) C21a N6a C25a C26a . . . . 176.0(8) C27a N7a C26a O1a . . . . 163.2(9) C27a N7a C26a C25a . . . . -16.9(15) C29a N7a C26a O1a . . . . -6.5(13) C29a N7a C26a C25a . . . . 173.4(9) C26a N7a C27a C28a . . . . -86.5(11) C29a N7a C27a C28a . . . . 83.4(11) C26a N7a C29a C30a . . . . -97.6(11) C27a N7a C29a C30a . . . . 91.6(11) Eu1 N8a C31a N9a . . . . -171.5(6) Eu1 N8a C31a C5a . . . . 12.6(11) C32a N8a C31a N9a . . . . 1.8(11) C32a N8a C31a C5a . . . . -174.2(9) Eu1 N8a C32a C33a . . . . -11.1(15) Eu1 N8a C32a C37a . . . . 169.4(7) C31a N8a C32a C33a . . . . 177.3(10) C31a N8a C32a C37a . . . . -2.3(10) C37a N9a C31a N8a . . . . -.6(11) C37a N9a C31a C5a . . . . 175.0(9) C60a N9a C31a N8a . . . . -176.9(9) C60a N9a C31a C5a . . . . -1.3(16) C31a N9a C37a C32a . . . . -.8(11) C31a N9a C37a C36a . . . . -179.1(11) C60a N9a C37a C32a . . . . 176.0(9) C60a N9a C37a C36a . . . . -2.3(16) C31a N9a C60a C61a . . . . -85.4(13) C37a N9a C60a C61a . . . . 98.8(11) Eu3 N10a C41a C40a . . . . -10.6(15) Eu3 N10a C41a C42a . . . . 170.5(7) C45a N10a C41a C40a . . . . 175.8(10) C45a N10a C41a C42a . . . . -3.0(11) Eu3 N10a C45a N11a . . . . -171.4(6) Eu3 N10a C45a C46a . . . . 11.5(12) C41a N10a C45a N11a . . . . 3.3(10) C41a N10a C45a C46a . . . . -173.8(9) C45a N11a C42a C41a . . . . .5(11) C45a N11a C42a C43a . . . . -178.9(11) C62a N11a C42a C41a . . . . -173.0(9) C62a N11a C42a C43a . . . . 7.6(17) C42a N11a C45a N10a . . . . -2.4(11) C42a N11a C45a C46a . . . . 174.3(10) C62a N11a C45a N10a . . . . 170.5(9) C62a N11a C45a C46a . . . . -12.7(16) C42a N11a C62a C63a . . . . 93.2(13) C45a N11a C62a C63a . . . . -78.7(15) Eu3 N12a C46a C45a . . . . 20.3(10) Eu3 N12a C46a C47a . . . . -154.3(8) C50a N12a C46a C45a . . . . -178.7(8) C50a N12a C46a C47a . . . . 6.7(13) Eu3 N12a C50a C49a . . . . 152.8(8) Eu3 N12a C50a C51a . . . . -21.9(10) C46a N12a C50a C49a . . . . -9.0(14) C46a N12a C50a C51a . . . . 176.2(8) C52a N13a C51a O2a . . . . -171.8(14) C52a N13a C51a C50a . . . . 6(3) C54a N13a C51a O2a . . . . .0(18) C54a N13a C51a C50a . . . . 177.4(12) C51a N13a C52a C53a . . . . -118(3) C51a N13a C52a C53a' . . . . 131(5) C54a N13a C52a C53a . . . . 70(3) C54a N13a C52a C53a' . . . . -41(5) C51a N13a C54a C55a . . . . -80.6(17) C52a N13a C54a C55a . . . . 91.9(19) N1a C1a C2a C3a . . . . 2.1(15) C6a C1a C2a C3a . . . . -171.4(10) N1a C1a C6a N2a . . . . -28.8(11) N1a C1a C6a N3a . . . . 158.9(9) C2a C1a C6a N2a . . . . 145.3(9) C2a C1a C6a N3a . . . . -27.0(15) C1a C2a C3a C4a . . . . -2.6(16) C2a C3a C4a C5a . . . . .2(17) C3a C4a C5a N1a . . . . 2.7(15) C3a C4a C5a C31a . . . . -170.6(10) N1a C5a C31a N8a . . . . 4.2(13) N1a C5a C31a N9a . . . . -171.1(9) C4a C5a C31a N8a . . . . 178.0(10) C4a C5a C31a N9a . . . . 2.7(16) N2a C7a C8a C9a . . . . -177.2(8) C12a C7a C8a C9a . . . . -3.3(12) N2a C7a C12a N3a . . . . 2.8(9) N2a C7a C12a C11a . . . . -178.9(8) C8a C7a C12a N3a . . . . -172.3(8) C8a C7a C12a C11a . . . . 6.0(13) C7a C8a C9a C10a . . . . -.8(12) C7a C8a C9a C13a . . . . 179.1(8) C8a C9a C10a C11a . . . . 2.3(13) C13a C9a C10a C11a . . . . -177.6(8) C8a C9a C13a C14a . . . . -32.0(11) C10a C9a C13a C14a . . . . 148.0(8) C9a C10a C11a C12a . . . . .4(14) C10a C11a C12a N3a . . . . 173.4(9) C10a C11a C12a C7a . . . . -4.4(13) C9a C13a C14a C15a . . . . -60.5(12) C9a C13a C14a C19a . . . . 121.2(9) C13a C14a C15a C16a . . . . -176.1(9) C19a C14a C15a C16a . . . . 2.2(14) C13a C14a C19a C18a . . . . 177.7(10) C15a C14a C19a C18a . . . . -.6(15) C14a C15a C16a N4a . . . . 176.1(9) C14a C15a C16a C17a . . . . -2.6(14) N4a C16a C17a N5a . . . . .6(10) N4a C16a C17a C18a . . . . -177.5(9) C15a C16a C17a N5a . . . . 179.6(8) C15a C16a C17a C18a . . . . 1.5(15) N5a C17a C18a C19a . . . . -177.5(10) C16a C17a C18a C19a . . . . .2(15) C17a C18a C19a C14a . . . . -.6(15) N4a C20a C21a N6a . . . . 7.0(13) N4a C20a C21a C22a . . . . -168.5(10) N5a C20a C21a N6a . . . . -170.9(9) N5a C20a C21a C22a . . . . 13.6(16) N6a C21a C22a C23a . . . . -2.9(16) C20a C21a C22a C23a . . . . 172.3(10) C21a C22a C23a C24a . . . . 4.2(17) C22a C23a C24a C25a . . . . -1.4(17) C23a C24a C25a N6a . . . . -2.9(15) C23a C24a C25a C26a . . . . -173.4(10) N6a C25a C26a O1a . . . . -33.4(12) N6a C25a C26a N7a . . . . 146.6(9) C24a C25a C26a O1a . . . . 137.9(10) C24a C25a C26a N7a . . . . -42.1(15) N8a C32a C33a C34a . . . . 179.9(10) C37a C32a C33a C34a . . . . -.5(14) N8a C32a C37a N9a . . . . 2.0(11) N8a C32a C37a C36a . . . . -179.7(10) C33a C32a C37a N9a . . . . -177.7(9) C33a C32a C37a C36a . . . . .7(16) C32a C33a C34a C35a . . . . -.2(15) C32a C33a C34a C38a . . . . 179.9(9) C33a C34a C35a C36a . . . . .8(16) C38a C34a C35a C36a . . . . -179.3(10) C33a C34a C38a C39a . . . . -54.3(12) C35a C34a C38a C39a . . . . 125.8(10) C34a C35a C36a C37a . . . . -.6(16) C35a C36a C37a N9a . . . . 177.8(10) C35a C36a C37a C32a . . . . -.1(16) C34a C38a C39a C40a . . . . -49.3(13) C34a C38a C39a C44a . . . . 130.0(10) C38a C39a C40a C41a . . . . 178.2(9) C44a C39a C40a C41a . . . . -1.1(14) C38a C39a C44a C43a . . . . -177.2(10) C40a C39a C44a C43a . . . . 2.1(16) C39a C40a C41a N10a . . . . -179.7(9) C39a C40a C41a C42a . . . . -1.0(15) N10a C41a C42a N11a . . . . 1.6(11) N10a C41a C42a C43a . . . . -179.0(9) C40a C41a C42a N11a . . . . -177.3(9) C40a C41a C42a C43a . . . . 2.1(15) N11a C42a C43a C44a . . . . 178.2(10) C41a C42a C43a C44a . . . . -1.2(16) C42a C43a C44a C39a . . . . -.9(16) N10a C45a C46a N12a . . . . -20.7(12) N10a C45a C46a C47a . . . . 153.9(10) N11a C45a C46a N12a . . . . 162.8(9) N11a C45a C46a C47a . . . . -22.6(15) N12a C46a C47a C48a . . . . .3(15) C45a C46a C47a C48a . . . . -173.7(10) C46a C47a C48a C49a . . . . -5.3(17) C47a C48a C49a C50a . . . . 3.1(18) C48a C49a C50a N12a . . . . 4.2(17) C48a C49a C50a C51a . . . . 178.0(11) N12a C50a C51a O2a . . . . 32.0(13) N12a C50a C51a N13a . . . . -145.5(11) C49a C50a C51a O2a . . . . -142.3(12) C49a C50a C51a N13a . . . . 40.2(18) Eu2 O1b C26b N7b . . . . -149.3(8) Eu2 O1b C26b C25b . . . . 28.5(11) Eu3 O2b C51b N13b . . . . 151.6(8) Eu3 O2b C51b C50b . . . . -27.0(12) Eu1 N1b C1b C2b . . . . 179.2(7) Eu1 N1b C1b C6b . . . . -3.5(10) C5b N1b C1b C2b . . . . -1.1(13) C5b N1b C1b C6b . . . . 176.2(8) Eu1 N1b C5b C4b . . . . -178.2(7) Eu1 N1b C5b C31b . . . . -4.3(10) C1b N1b C5b C4b . . . . 2.1(13) C1b N1b C5b C31b . . . . 176.1(8) Eu1 N2b C6b N3b . . . . -142.1(6) Eu1 N2b C6b C1b . . . . 44.2(9) C7b N2b C6b N3b . . . . 2.5(10) C7b N2b C6b C1b . . . . -171.2(8) Eu1 N2b C7b C8b . . . . -50.2(13) Eu1 N2b C7b C12b . . . . 130.4(7) C6b N2b C7b C8b . . . . 175.4(9) C6b N2b C7b C12b . . . . -3.9(10) C12b N3b C6b N2b . . . . -.1(11) C12b N3b C6b C1b . . . . 172.7(9) C56b N3b C6b N2b . . . . 168.9(9) C56b N3b C6b C1b . . . . -18.3(16) C6b N3b C12b C7b . . . . -2.4(10) C6b N3b C12b C11b . . . . 178.3(10) C56b N3b C12b C7b . . . . -172.1(9) C56b N3b C12b C11b . . . . 8.6(16) C6b N3b C56b C57b . . . . 116.1(10) C12b N3b C56b C57b . . . . -76.5(11) Eu2 N4b C16b C15b . . . . -7.5(12) Eu2 N4b C16b C17b . . . . 171.7(5) C20b N4b C16b C15b . . . . -177.9(8) C20b N4b C16b C17b . . . . 1.3(8) Eu2 N4b C20b N5b . . . . -174.5(5) Eu2 N4b C20b C21b . . . . 5.9(9) C16b N4b C20b N5b . . . . -2.4(8) C16b N4b C20b C21b . . . . 178.0(7) C20b N5b C17b C16b . . . . -1.6(8) C20b N5b C17b C18b . . . . 175.9(9) C58b N5b C17b C16b . . . . 179.4(7) C58b N5b C17b C18b . . . . -3.1(13) C17b N5b C20b N4b . . . . 2.6(9) C17b N5b C20b C21b . . . . -177.9(7) C58b N5b C20b N4b . . . . -178.5(8) C58b N5b C20b C21b . . . . 1.0(13) C17b N5b C58b C59b . . . . 88.0(10) C20b N5b C58b C59b . . . . -90.7(10) C25b N6b C21b C20b . . . . -175.9(7) C25b N6b C21b C22b . . . . -.6(11) C21b N6b C25b C24b . . . . 2.3(11) C21b N6b C25b C26b . . . . 175.4(7) C27b N7b C26b O1b . . . . 170.0(11) C27b N7b C26b C25b . . . . -7.7(17) C29b N7b C26b O1b . . . . -5.5(15) C29b N7b C26b C25b . . . . 176.9(9) C26b N7b C27b C28b . . . . 115.7(14) C29b N7b C27b C28b . . . . -68.6(15) C26b N7b C29b C30b . . . . -76.3(14) C27b N7b C29b C30b . . . . 107.7(12) Eu1 N8b C31b N9b . . . . -150.4(6) Eu1 N8b C31b C5b . . . . 35.5(10) C32b N8b C31b N9b . . . . 1.5(10) C32b N8b C31b C5b . . . . -172.6(8) Eu1 N8b C32b C33b . . . . -38.8(13) Eu1 N8b C32b C37b . . . . 145.0(7) C31b N8b C32b C33b . . . . 175.8(10) C31b N8b C32b C37b . . . . -.3(10) C37b N9b C31b N8b . . . . -2.1(11) C37b N9b C31b C5b . . . . 171.3(9) C60b N9b C31b N8b . . . . 169.0(9) C60b N9b C31b C5b . . . . -17.5(16) C31b N9b C37b C32b . . . . 1.8(11) C31b N9b C37b C36b . . . . 177.6(11) C60b N9b C37b C32b . . . . -169.9(9) C60b N9b C37b C36b . . . . 5.9(17) C31b N9b C60b C61b . . . . 110.6(11) C37b N9b C60b C61b . . . . -79.5(13) C45b N10b C41b C40b . . . . 173.8(8) C45b N10b C41b C42b . . . . -5.1(9) C41b N10b C45b N11b . . . . 4.4(9) C41b N10b C45b C46b . . . . -171.7(8) C45b N11b C42b C41b . . . . -1.2(9) C45b N11b C42b C43b . . . . -179.0(10) C62b N11b C42b C41b . . . . -166.3(8) C62b N11b C42b C43b . . . . 16.0(15) C42b N11b C45b N10b . . . . -2.1(10) C42b N11b C45b C46b . . . . 173.8(9) C62b N11b C45b N10b . . . . 162.4(8) C62b N11b C45b C46b . . . . -21.8(13) C42b N11b C62b C63b . . . . 82.6(12) C45b N11b C62b C63b . . . . -79.6(12) Eu3 N12b C46b C45b . . . . 8.4(11) Eu3 N12b C46b C47b . . . . -167.3(8) C50b N12b C46b C45b . . . . 179.6(9) C50b N12b C46b C47b . . . . 3.9(15) Eu3 N12b C50b C49b . . . . 161.8(8) Eu3 N12b C50b C51b . . . . -16.4(11) C46b N12b C50b C49b . . . . -9.5(15) C46b N12b C50b C51b . . . . 172.4(9) C52b N13b C51b O2b . . . . -162.5(10) C52b N13b C51b C50b . . . . 16.0(16) C54b N13b C51b O2b . . . . -3.0(18) C54b N13b C51b C50b . . . . 175.4(13) C51b N13b C52b C53b . . . . -115.5(12) C54b N13b C52b C53b . . . . 84.2(14) C51b N13b C54b C55b . . . . 80.3(18) C52b N13b C54b C55b . . . . -117.3(16) N1b C1b C2b C3b . . . . .9(15) C6b C1b C2b C3b . . . . -176.1(10) N1b C1b C6b N2b . . . . -28.8(12) N1b C1b C6b N3b . . . . 158.8(9) C2b C1b C6b N2b . . . . 148.5(9) C2b C1b C6b N3b . . . . -24.0(15) C1b C2b C3b C4b . . . . -1.6(16) C2b C3b C4b C5b . . . . 2.6(16) C3b C4b C5b N1b . . . . -2.9(15) C3b C4b C5b C31b . . . . -176.0(10) N1b C5b C31b N8b . . . . -21.3(12) N1b C5b C31b N9b . . . . 165.6(9) C4b C5b C31b N8b . . . . 152.4(10) C4b C5b C31b N9b . . . . -20.8(16) N2b C7b C8b C9b . . . . 178.3(9) C12b C7b C8b C9b . . . . -2.4(13) N2b C7b C12b N3b . . . . 3.9(10) N2b C7b C12b C11b . . . . -176.7(9) C8b C7b C12b N3b . . . . -175.5(8) C8b C7b C12b C11b . . . . 3.9(14) C7b C8b C9b C10b . . . . -.9(13) C7b C8b C9b C13b . . . . -177.5(8) C8b C9b C10b C11b . . . . 3.1(15) C13b C9b C10b C11b . . . . 179.8(9) C8b C9b C13b C14b . . . . -23.0(13) C10b C9b C13b C14b . . . . 160.4(9) C9b C10b C11b C12b . . . . -1.7(15) C10b C11b C12b N3b . . . . 177.4(10) C10b C11b C12b C7b . . . . -1.8(14) C9b C13b C14b C15b . . . . -63.3(11) C9b C13b C14b C19b . . . . 117.2(9) C13b C14b C15b C16b . . . . -177.1(7) C19b C14b C15b C16b . . . . 2.5(11) C13b C14b C19b C18b . . . . 179.3(8) C15b C14b C19b C18b . . . . -.3(13) C14b C15b C16b N4b . . . . 176.0(7) C14b C15b C16b C17b . . . . -3.2(11) N4b C16b C17b N5b . . . . .2(9) N4b C16b C17b C18b . . . . -177.5(8) C15b C16b C17b N5b . . . . 179.6(7) C15b C16b C17b C18b . . . . 1.9(12) N5b C17b C18b C19b . . . . -176.8(8) C16b C17b C18b C19b . . . . .3(13) C17b C18b C19b C14b . . . . -1.1(13) N4b C20b C21b N6b . . . . 8.4(10) N4b C20b C21b C22b . . . . -166.6(8) N5b C20b C21b N6b . . . . -171.1(7) N5b C20b C21b C22b . . . . 13.9(13) N6b C21b C22b C23b . . . . -.8(12) C20b C21b C22b C23b . . . . 173.8(8) C21b C22b C23b C24b . . . . .6(13) C22b C23b C24b C25b . . . . 1.0(13) C23b C24b C25b N6b . . . . -2.4(13) C23b C24b C25b C26b . . . . -174.6(8) N6b C25b C26b O1b . . . . -28.3(11) N6b C25b C26b N7b . . . . 149.4(9) C24b C25b C26b O1b . . . . 144.6(9) C24b C25b C26b N7b . . . . -37.6(14) N8b C32b C33b C34b . . . . 179.9(9) C37b C32b C33b C34b . . . . -4.5(14) N8b C32b C37b N9b . . . . -.9(10) N8b C32b C37b C36b . . . . -177.4(9) C33b C32b C37b N9b . . . . -177.5(9) C33b C32b C37b C36b . . . . 6.1(15) C32b C33b C34b C35b . . . . 2.9(14) C32b C33b C34b C38b . . . . -175.0(9) C33b C34b C35b C36b . . . . -3.1(16) C38b C34b C35b C36b . . . . 174.8(10) C33b C34b C38b C39b . . . . -35.2(13) C35b C34b C38b C39b . . . . 146.9(9) C34b C35b C36b C37b . . . . 4.6(16) C35b C36b C37b N9b . . . . 178.8(11) C35b C36b C37b C32b . . . . -5.9(15) C34b C38b C39b C40b . . . . -34.0(13) C34b C38b C39b C44b . . . . 149.2(9) C38b C39b C40b C41b . . . . -176.6(8) C44b C39b C40b C41b . . . . .0(12) C38b C39b C44b C43b . . . . 179.1(9) C40b C39b C44b C43b . . . . 2.2(14) C39b C40b C41b N10b . . . . 178.7(8) C39b C40b C41b C42b . . . . -2.5(12) N10b C41b C42b N11b . . . . 3.9(9) N10b C41b C42b C43b . . . . -178.1(8) C40b C41b C42b N11b . . . . -175.2(7) C40b C41b C42b C43b . . . . 2.8(13) N11b C42b C43b C44b . . . . 176.8(9) C41b C42b C43b C44b . . . . -.6(13) C42b C43b C44b C39b . . . . -1.9(14) N10b C45b C46b N12b . . . . -36.0(12) N10b C45b C46b C47b . . . . 139.6(10) N11b C45b C46b N12b . . . . 148.5(9) N11b C45b C46b C47b . . . . -35.8(15) N12b C46b C47b C48b . . . . 3.5(15) C45b C46b C47b C48b . . . . -171.7(10) C46b C47b C48b C49b . . . . -5.8(15) C47b C48b C49b C50b . . . . .8(16) C48b C49b C50b N12b . . . . 7.2(16) C48b C49b C50b C51b . . . . -175.0(11) N12b C50b C51b O2b . . . . 26.7(13) N12b C50b C51b N13b . . . . -151.8(10) C49b C50b C51b O2b . . . . -151.3(11) C49b C50b C51b N13b . . . . 30.1(17) Eu2 O1c C26c N7c . . . . -144.2(8) Eu2 O1c C26c C25c . . . . 34.6(12) Eu3 O2c C51c N13c . . . . -142.1(9) Eu3 O2c C51c C50c . . . . 37.7(11) Eu1 N1c C1c C2c . . . . -176.2(7) Eu1 N1c C1c C6c . . . . -4.0(9) C5c N1c C1c C2c . . . . 2.8(13) C5c N1c C1c C6c . . . . 175.0(8) Eu1 N1c C5c C4c . . . . 177.5(7) Eu1 N1c C5c C31c . . . . -7.2(10) C1c N1c C5c C4c . . . . -1.4(13) C1c N1c C5c C31c . . . . 173.9(7) Eu1 N2c C6c N3c . . . . -146.9(6) Eu1 N2c C6c C1c . . . . 37.3(10) C7c N2c C6c N3c . . . . 3.9(10) C7c N2c C6c C1c . . . . -171.9(8) Eu1 N2c C7c C8c . . . . -43.3(13) Eu1 N2c C7c C12c . . . . 138.9(7) C6c N2c C7c C8c . . . . 174.6(10) C6c N2c C7c C12c . . . . -3.2(10) C12c N3c C6c N2c . . . . -3.2(11) C12c N3c C6c C1c . . . . 172.4(9) C56c N3c C6c N2c . . . . 168.4(9) C56c N3c C6c C1c . . . . -16.1(15) C6c N3c C12c C7c . . . . .9(10) C6c N3c C12c C11c . . . . -179.3(11) C56c N3c C12c C7c . . . . -171.3(8) C56c N3c C12c C11c . . . . 8.5(16) C6c N3c C56c C57c . . . . 108.8(11) C12c N3c C56c C57c . . . . -80.8(12) C20c N4c C16c C15c . . . . -177.8(10) C20c N4c C16c C17c . . . . .1(10) C16c N4c C20c N5c . . . . -1.0(11) C16c N4c C20c C21c . . . . 177.3(9) C20c N5c C17c C16c . . . . -1.4(10) C20c N5c C17c C18c . . . . -179.0(10) C58c N5c C17c C16c . . . . 174.6(9) C58c N5c C17c C18c . . . . -3.0(16) C17c N5c C20c N4c . . . . 1.5(11) C17c N5c C20c C21c . . . . -176.7(9) C58c N5c C20c N4c . . . . -174.0(9) C58c N5c C20c C21c . . . . 7.7(16) C17c N5c C58c C59c . . . . 83.8(11) C20c N5c C58c C59c . . . . -101.3(12) C25c N6c C21c C20c . . . . -179.5(8) C25c N6c C21c C22c . . . . -.2(14) C21c N6c C25c C24c . . . . 2.1(15) C21c N6c C25c C26c . . . . 176.4(9) C27c N7c C26c O1c . . . . 169.4(10) C27c N7c C26c C25c . . . . -9.3(15) C29c N7c C26c O1c . . . . -4.0(15) C29c N7c C26c C25c . . . . 177.3(9) C26c N7c C27c C28c . . . . -105.2(13) C29c N7c C27c C28c . . . . 68.4(13) C26c N7c C29c C30c . . . . -74.5(12) C27c N7c C29c C30c . . . . 111.6(12) Eu1 N8c C31c N9c . . . . -162.7(5) Eu1 N8c C31c C5c . . . . 22.0(10) C32c N8c C31c N9c . . . . 1.0(9) C32c N8c C31c C5c . . . . -174.2(7) Eu1 N8c C32c C33c . . . . -20.9(12) Eu1 N8c C32c C37c . . . . 158.9(6) C31c N8c C32c C33c . . . . 179.2(8) C31c N8c C32c C37c . . . . -1.0(9) C37c N9c C31c N8c . . . . -.7(9) C37c N9c C31c C5c . . . . 174.1(8) C60c N9c C31c N8c . . . . 177.2(8) C60c N9c C31c C5c . . . . -8.0(14) C31c N9c C37c C32c . . . . .1(9) C31c N9c C37c C36c . . . . 177.7(9) C60c N9c C37c C32c . . . . -178.0(8) C60c N9c C37c C36c . . . . -.3(14) C31c N9c C60c C61c . . . . -66.4(11) C37c N9c C60c C61c . . . . 111.2(10) Eu3 N10c C41c C40c . . . . -46.7(13) Eu3 N10c C41c C42c . . . . 133.3(7) C45c N10c C41c C40c . . . . 178.8(10) C45c N10c C41c C42c . . . . -1.2(11) Eu3 N10c C45c N11c . . . . -142.5(7) Eu3 N10c C45c C46c . . . . 37.3(11) C41c N10c C45c N11c . . . . -.1(11) C41c N10c C45c C46c . . . . 179.6(9) C45c N11c C42c C41c . . . . -2.0(10) C45c N11c C42c C43c . . . . 177.7(11) C62c N11c C42c C41c . . . . -169.9(9) C62c N11c C42c C43c . . . . 9.8(16) C42c N11c C45c N10c . . . . 1.4(11) C42c N11c C45c C46c . . . . -178.4(10) C62c N11c C45c N10c . . . . 168.4(10) C62c N11c C45c C46c . . . . -11.4(17) C42c N11c C62c C63c . . . . -89.2(11) C45c N11c C62c C63c . . . . 106.1(11) Eu3 N12c C46c C45c . . . . -6.4(12) Eu3 N12c C46c C47c . . . . 172.7(9) C50c N12c C46c C45c . . . . -176.0(9) C50c N12c C46c C47c . . . . 3.1(16) Eu3 N12c C50c C49c . . . . -167.2(10) Eu3 N12c C50c C51c . . . . 3.7(11) C46c N12c C50c C49c . . . . 2.7(16) C46c N12c C50c C51c . . . . 173.5(9) C52c N13c C51c O2c . . . . 158.5(14) C52c N13c C51c C50c . . . . -21.3(19) C54c N13c C51c O2c . . . . 4.1(18) C54c N13c C51c C50c . . . . -175.6(13) C51c N13c C52c C53c . . . . 117.2(18) C54c N13c C52c C53c . . . . -87(2) C51c N13c C54c C55c . . . . -82.6(16) C52c N13c C54c C55c . . . . 121.1(17) N1c C1c C2c C3c . . . . -1.6(15) C6c C1c C2c C3c . . . . -173.1(10) N1c C1c C6c N2c . . . . -23.0(12) N1c C1c C6c N3c . . . . 161.8(9) C2c C1c C6c N2c . . . . 149.1(9) C2c C1c C6c N3c . . . . -26.1(14) C1c C2c C3c C4c . . . . -.9(18) C2c C3c C4c C5c . . . . 2.2(18) C3c C4c C5c N1c . . . . -1.0(16) C3c C4c C5c C31c . . . . -175.8(10) N1c C5c C31c N8c . . . . -10.0(11) N1c C5c C31c N9c . . . . 175.5(8) C4c C5c C31c N8c . . . . 165.2(9) C4c C5c C31c N9c . . . . -9.3(14) N2c C7c C8c C9c . . . . -179.3(9) C12c C7c C8c C9c . . . . -1.7(14) N2c C7c C12c N3c . . . . 1.4(10) N2c C7c C12c C11c . . . . -178.3(9) C8c C7c C12c N3c . . . . -176.6(9) C8c C7c C12c C11c . . . . 3.7(15) C7c C8c C9c C10c . . . . -1.8(14) C7c C8c C9c C13c . . . . -179.2(9) C8c C9c C10c C11c . . . . 3.7(16) C13c C9c C10c C11c . . . . -178.9(10) C8c C9c C13c C14c . . . . -26.9(13) C10c C9c C13c C14c . . . . 155.6(9) C9c C10c C11c C12c . . . . -1.7(15) C10c C11c C12c N3c . . . . 178.4(10) C10c C11c C12c C7c . . . . -1.9(15) C9c C13c C14c C15c . . . . -67.6(12) C9c C13c C14c C19c . . . . 113.0(11) C13c C14c C15c C16c . . . . -176.5(9) C19c C14c C15c C16c . . . . 2.9(14) C13c C14c C19c C18c . . . . 177.4(10) C15c C14c C19c C18c . . . . -1.9(17) C14c C15c C16c N4c . . . . 177.3(9) C14c C15c C16c C17c . . . . -.4(13) N4c C16c C17c N5c . . . . .8(11) N4c C16c C17c C18c . . . . 178.6(9) C15c C16c C17c N5c . . . . 178.9(8) C15c C16c C17c C18c . . . . -3.3(15) N5c C17c C18c C19c . . . . -178.6(10) C16c C17c C18c C19c . . . . 4.2(16) C17c C18c C19c C14c . . . . -1.5(17) N4c C20c C21c N6c . . . . 21.9(13) N4c C20c C21c C22c . . . . -157.4(10) N5c C20c C21c N6c . . . . -160.0(9) N5c C20c C21c C22c . . . . 20.8(16) N6c C21c C22c C23c . . . . -2.0(15) C20c C21c C22c C23c . . . . 177.2(10) C21c C22c C23c C24c . . . . 2.5(16) C22c C23c C24c C25c . . . . -.7(17) C23c C24c C25c N6c . . . . -1.7(17) C23c C24c C25c C26c . . . . -175.1(11) N6c C25c C26c O1c . . . . -39.5(13) N6c C25c C26c N7c . . . . 139.3(10) C24c C25c C26c O1c . . . . 134.8(11) C24c C25c C26c N7c . . . . -46.4(16) N8c C32c C33c C34c . . . . 176.3(8) C37c C32c C33c C34c . . . . -3.6(12) N8c C32c C37c N9c . . . . .6(9) N8c C32c C37c C36c . . . . -177.4(8) C33c C32c C37c N9c . . . . -179.6(7) C33c C32c C37c C36c . . . . 2.5(13) C32c C33c C34c C35c . . . . 2.4(11) C32c C33c C34c C38c . . . . -176.2(7) C33c C34c C35c C36c . . . . -.2(13) C38c C34c C35c C36c . . . . 178.4(8) C33c C34c C38c C39c . . . . -56.7(11) C35c C34c C38c C39c . . . . 124.7(9) C34c C35c C36c C37c . . . . -.9(13) C35c C36c C37c N9c . . . . -177.6(9) C35c C36c C37c C32c . . . . -.3(13) C34c C38c C39c C40c . . . . -22.8(13) C34c C38c C39c C44c . . . . 158.8(9) C38c C39c C40c C41c . . . . -176.4(9) C44c C39c C40c C41c . . . . 2.0(14) C38c C39c C44c C43c . . . . 177.2(9) C40c C39c C44c C43c . . . . -1.2(15) C39c C40c C41c N10c . . . . 177.4(9) C39c C40c C41c C42c . . . . -2.6(14) N10c C41c C42c N11c . . . . 2.0(11) N10c C41c C42c C43c . . . . -177.7(9) C40c C41c C42c N11c . . . . -178.0(9) C40c C41c C42c C43c . . . . 2.3(14) N11c C42c C43c C44c . . . . 178.9(10) C41c C42c C43c C44c . . . . -1.4(14) C42c C43c C44c C39c . . . . .8(15) N10c C45c C46c N12c . . . . -22.0(14) N10c C45c C46c C47c . . . . 158.9(11) N11c C45c C46c N12c . . . . 157.7(10) N11c C45c C46c C47c . . . . -21.4(17) N12c C46c C47c C48c . . . . -6.1(18) C45c C46c C47c C48c . . . . 172.9(12) C46c C47c C48c C49c . . . . 3(3) C47c C48c C49c C50c . . . . 2(3) C48c C49c C50c N12c . . . . -5(2) C48c C49c C50c C51c . . . . -174.7(13) N12c C50c C51c O2c . . . . -24.8(13) N12c C50c C51c N13c . . . . 154.9(11) C49c C50c C51c O2c . . . . 145.6(12) C49c C50c C51c N13c . . . . -34.7(18) O1d S1d C1d F1d . . . . -56.9(13) O1d S1d C1d F2d . . . . -176.8(12) O1d S1d C1d F3d . . . . 59.2(11) O2d S1d C1d F1d . . . . 58.7(15) O2d S1d C1d F2d . . . . -61.2(15) O2d S1d C1d F3d . . . . 174.8(12) O3d S1d C1d F1d . . . . -176.7(11) O3d S1d C1d F2d . . . . 63.5(14) O3d S1d C1d F3d . . . . -60.5(12) O1e S1e C1e F1e . . . . 62.5(10) O1e S1e C1e F2e . . . . -56.2(9) O1e S1e C1e F3e . . . . -176.7(7) O2e S1e C1e F1e . . . . -177.4(9) O2e S1e C1e F2e . . . . 63.9(10) O2e S1e C1e F3e . . . . -56.7(9) O3e S1e C1e F1e . . . . -56.6(10) O3e S1e C1e F2e . . . . -175.3(9) O3e S1e C1e F3e . . . . 64.2(8) O1f S1f C1f F1f . . . . 55.6(16) O1f S1f C1f F2f . . . . -61.2(12) O1f S1f C1f F3f . . . . -179.4(14) O2f S1f C1f F1f . . . . 175.8(13) O2f S1f C1f F2f . . . . 58.9(12) O2f S1f C1f F3f . . . . -59.3(15) O3f S1f C1f F1f . . . . -65.1(15) O3f S1f C1f F2f . . . . 178.1(10) O3f S1f C1f F3f . . . . 59.8(15) O1g S1g C1g F1g . . . . -61.0(11) O1g S1g C1g F2g . . . . 59.9(9) O1g S1g C1g F3g . . . . -179.8(8) O2g S1g C1g F1g . . . . -179.3(10) O2g S1g C1g F2g . . . . -58.4(9) O2g S1g C1g F3g . . . . 61.8(10) O3g S1g C1g F1g . . . . 60.6(11) O3g S1g C1g F2g . . . . -178.5(7) O3g S1g C1g F3g . . . . -58.2(9) O1h S1h C1h F1h . . . . 57.7(9) O1h S1h C1h F2h . . . . -63.3(10) O1h S1h C1h F3h . . . . 177.4(9) O2h S1h C1h F1h . . . . 179.1(9) O2h S1h C1h F2h . . . . 58.1(10) O2h S1h C1h F3h . . . . -61.3(10) O3h S1h C1h F1h . . . . -60.6(9) O3h S1h C1h F2h . . . . 178.3(9) O3h S1h C1h F3h . . . . 59.0(10) O1i S1i C1i F1i . . . . -47(3) O1i S1i C1i F2i . . . . -158(3) O1i S1i C1i F3i . . . . 72(3) O2i S1i C1i F1i . . . . 74(3) O2i S1i C1i F2i . . . . -37(3) O2i S1i C1i F3i . . . . -168(3) O3i S1i C1i F1i . . . . -165(3) O3i S1i C1i F2i . . . . 84(3) O3i S1i C1i F3i . . . . -46(3) O1i' S1i C1i F1i' . . . . 66.9(15) O1i' S1i C1i F2i' . . . . -63.4(19) O1i' S1i C1i F3i' . . . . 177.7(16) O2i' S1i C1i F1i' . . . . -172.7(14) O2i' S1i C1i F2i' . . . . 57.0(18) O2i' S1i C1i F3i' . . . . -61.9(15) O3i' S1i C1i F1i' . . . . -54.8(14) O3i' S1i C1i F2i' . . . . 174.9(17) O3i' S1i C1i F3i' . . . . 55.9(15) O1j S1j C1j F1j . . . . -52(2) O1j S1j C1j F2j . . . . -174(2) O1j S1j C1j F3j . . . . 67(3) O2j S1j C1j F1j . . . . 68.0(18) O2j S1j C1j F2j . . . . -55(2) O2j S1j C1j F3j . . . . -174(3) O3j S1j C1j F1j . . . . -171.4(17) O3j S1j C1j F2j . . . . 66(2) O3j S1j C1j F3j . . . . -53(3) O1j' S1j C1j' F1j' . . . . -58(3) O1j' S1j C1j' F2j' . . . . -178(2) O1j' S1j C1j' F3j' . . . . 63.3(19) O2j' S1j C1j' F1j' . . . . 64.6(19) O2j' S1j C1j' F2j' . . . . -55(3) O2j' S1j C1j' F3j' . . . . -173.6(16) O3j' S1j C1j' F1j' . . . . -179.6(15) O3j' S1j C1j' F2j' . . . . 60.8(19) O3j' S1j C1j' F3j' . . . . -57.8(15) O1k S1k C1k F1k . . . . 175.1(17) O1k S1k C1k F2k . . . . 54(3) O1k S1k C1k F3k . . . . -62.4(19) O2k S1k C1k F1k . . . . -56.5(19) O2k S1k C1k F2k . . . . -178.0(18) O2k S1k C1k F3k . . . . 66.0(18) O3k S1k C1k F1k . . . . 72.1(19) O3k S1k C1k F2k . . . . -49(3) O3k S1k C1k F3k . . . . -165.4(16) O1k' S1k C1k' F1k' . . . . -173.2(15) O1k' S1k C1k' F2k' . . . . 65.6(19) O1k' S1k C1k' F3k' . . . . -56.3(18) O2k' S1k C1k' F1k' . . . . -52.0(17) O2k' S1k C1k' F2k' . . . . -173.2(18) O2k' S1k C1k' F3k' . . . . 64.8(18) O3k' S1k C1k' F1k' . . . . 70.4(14) O3k' S1k C1k' F2k' . . . . -50.8(17) O3k' S1k C1k' F3k' . . . . -172.8(14) O1l S1l C1l F1l . . . . -44(3) O1l S1l C1l F2l . . . . -162.2(18) O1l S1l C1l F3l . . . . 71.5(18) O2l S1l C1l F1l . . . . 73(3) O2l S1l C1l F2l . . . . -45(2) O2l S1l C1l F3l . . . . -171.1(17) O3l S1l C1l F1l . . . . -165(3) O3l S1l C1l F2l . . . . 77(3) O3l S1l C1l F3l . . . . -50(3) O1l' S1l C1l' F1l' . . . . -172(3) O1l' S1l C1l' F2l' . . . . 67(3) O1l' S1l C1l' F3l' . . . . -50(3) O2l' S1l C1l' F1l' . . . . 61(3) O2l' S1l C1l' F2l' . . . . -60(4) O2l' S1l C1l' F3l' . . . . -177(4) O3l' S1l C1l' F1l' . . . . -52(3) O3l' S1l C1l' F2l' . . . . -173(4) O3l' S1l C1l' F3l' . . . . 70(4) O1l'' S1l C1l' F1l'' . . . . -161(3) O1l'' S1l C1l' F2l'' . . . . 81(3) O1l'' S1l C1l' F3l'' . . . . -46(3) O2l'' S1l C1l' F1l'' . . . . 84(3) O2l'' S1l C1l' F2l'' . . . . -33(3) O2l'' S1l C1l' F3l'' . . . . -160(3) O3l'' S1l C1l' F1l'' . . . . -36(3) O3l'' S1l C1l' F2l'' . . . . -153(3) O3l'' S1l C1l' F3l'' . . . . 80(3)