# Supplementary Material (ESI) for Chemical Communications # This journal is (c) The Royal Society of Chemistry 2007 data_global _journal_name_full Chem.Commun. _journal_coden_Cambridge 0182 _publ_contact_author_name 'Takeshi Akasaka' _publ_contact_author_address ; Centre for Tsukuba Advanced Research Alliance University of Tsukuba Tsukuba Ibaraki 305 8577 JAPAN ; _publ_contact_author_email AKASAKA@TARA.TSUKUBA.AC.JP _publ_section_title ; Location of the Metal Atoms in Ce2@C78 and Its Bis-silylated Derivative ; loop_ _publ_author_name 'Takeshi Akasaka' 'Ernst Horn' 'Yutaka Maeda' 'Naomi Mizorogi' 'Shigeru Nagase' 'Takahiro Tsuchiya' ; T.Wakahara ; 'Michio Yamada' 'Kenji Yoza' data_Ce2@C78Si130krev2 _database_code_depnum_ccdc_archive 'CCDC 656005' _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C117.50 H46 Ce2 S5 Si2' _chemical_formula_weight 1954.26 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M P212121 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' _cell_length_a 11.300(2) _cell_length_b 23.437(4) _cell_length_c 27.993(6) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 7414(2) _cell_formula_units_Z 4 _cell_measurement_temperature 130(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description platelet _exptl_crystal_colour black _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.01 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.751 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3900 _exptl_absorpt_coefficient_mu 1.449 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.8119 _exptl_absorpt_correction_T_max 0.9857 _exptl_absorpt_process_details 'SADABS Sheldrick 1996' _exptl_special_details ; ? ; _diffrn_ambient_temperature 130(2) _diffrn_radiation_wavelength 0.68880 _diffrn_radiation_type synchrotron _diffrn_radiation_source synchrotron _diffrn_radiation_source_type 'KEK BL1B' _diffrn_radiation_monochromator Si(111) _diffrn_measurement_device_type IPDSC _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 34138 _diffrn_reflns_av_R_equivalents 0.0387 _diffrn_reflns_av_sigmaI/netI 0.0346 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_theta_min 1.41 _diffrn_reflns_theta_max 24.51 _reflns_number_total 10295 _reflns_number_gt 8808 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'Bruker SMART' _computing_cell_refinement 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The 977 restraints were used in the refinements. All atoms were refined with SIMU to generate similar Uij restraints automatically using connectivity. S5, C118, and S6 were refined with ISOR so that their Uij components approximate to isotropic behavior. S5, C118, and S6 were also refined with DELU to generate rigid bond Uij restraints automatically using connectivity. S5, C118, and S6 were also refined with DANG to restrain the 1,3-distance S5...S6. ; _chemical_absolute_configuration unk _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.1131P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.349(15) _refine_ls_number_reflns 10295 _refine_ls_number_parameters 1186 _refine_ls_number_restraints 977 _refine_ls_R_factor_all 0.0582 _refine_ls_R_factor_gt 0.0491 _refine_ls_wR_factor_ref 0.1445 _refine_ls_wR_factor_gt 0.1365 _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_restrained_S_all 1.027 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ce1 Ce 0.51548(4) 0.59511(2) 0.102516(15) 0.05016(17) Uani 0.9578(14) 1 d P A 2 Ce2 Ce 0.87060(5) 0.60788(2) 0.114013(14) 0.05056(17) Uani 0.9578(14) 1 d P A 2 Si1 Si 0.5698(2) 0.74718(11) 0.28555(7) 0.0496(6) Uani 1 1 d . . . Si2 Si 0.7107(3) 0.62315(12) 0.32820(7) 0.0562(7) Uani 1 1 d . . . C79 C 0.8072(13) 0.4997(5) 0.3517(3) 0.086(3) Uani 1 1 d U . . H1 H 0.8447 0.5165 0.3790 0.128 Uiso 1 1 calc R . . H2 H 0.8351 0.5181 0.3232 0.128 Uiso 1 1 calc R . . H3 H 0.8261 0.4598 0.3503 0.128 Uiso 1 1 calc R . . C1 C 0.3874(9) 0.6653(4) 0.1618(3) 0.0555(15) Uani 1 1 d U . . C2 C 0.9632(8) 0.5997(4) 0.2050(3) 0.0555(14) Uani 1 1 d U . . C3 C 0.9782(9) 0.6400(4) 0.0245(3) 0.0599(15) Uani 1 1 d U . . C4 C 0.6075(8) 0.6003(4) 0.2433(2) 0.0527(14) Uani 1 1 d U A . C5 C 0.9399(8) 0.6942(4) 0.1750(3) 0.0552(15) Uani 1 1 d U . . C6 C 0.9580(9) 0.4889(4) 0.0942(3) 0.0611(16) Uani 1 1 d U . . C7 C 0.7923(9) 0.5528(4) 0.2397(3) 0.0535(15) Uani 1 1 d U . . C8 C 0.4857(9) 0.5277(4) 0.2022(3) 0.0539(14) Uani 1 1 d U . . C9 C 0.8954(9) 0.5482(4) 0.2144(3) 0.0553(15) Uani 1 1 d U A . C80 C 0.4203(11) 0.6142(5) 0.3446(3) 0.075(3) Uani 1 1 d U . . H4 H 0.3387 0.6043 0.3399 0.112 Uiso 1 1 calc R . . H5 H 0.4493 0.6338 0.3169 0.112 Uiso 1 1 calc R . . H6 H 0.4272 0.6387 0.3720 0.112 Uiso 1 1 calc R . . C10 C 0.6966(9) 0.5143(4) 0.2313(3) 0.0555(15) Uani 1 1 d U A . C81 C 0.5833(8) 0.8616(4) 0.2497(3) 0.0487(15) Uani 1 1 d U . . C11 C 0.9995(10) 0.5290(4) 0.0590(3) 0.0626(15) Uani 1 1 d U A . C12 C 1.0357(9) 0.6655(4) 0.1482(3) 0.0593(16) Uani 1 1 d U A . C13 C 0.4259(9) 0.6119(4) 0.0100(3) 0.0580(15) Uani 1 1 d U . . C82 C 0.6755(12) 0.5070(5) 0.3555(3) 0.078(2) Uani 1 1 d U . . C14 C 1.0453(8) 0.6079(4) 0.1676(3) 0.0579(15) Uani 1 1 d U A . C15 C 0.5031(10) 0.4800(4) 0.1691(3) 0.0576(15) Uani 1 1 d U A . C16 C 0.3540(9) 0.5349(4) 0.0634(3) 0.0606(16) Uani 1 1 d U . . C17 C 0.7383(8) 0.6093(4) 0.2594(2) 0.0517(14) Uani 1 1 d U A . C18 C 0.8693(9) 0.7471(4) 0.1059(3) 0.0570(15) Uani 1 1 d U . . C83 C 1.0013(12) 0.6520(5) 0.4471(3) 0.079(2) Uani 1 1 d U . . C19 C 0.7865(8) 0.6590(4) 0.2329(3) 0.0496(14) Uani 1 1 d U . . C20 C 0.9235(9) 0.6929(5) 0.0321(3) 0.0606(15) Uani 1 1 d U A . C84 C 0.3083(9) 0.7478(4) 0.3041(3) 0.0562(16) Uani 1 1 d U . . C21 C 0.7990(9) 0.4580(4) 0.0417(3) 0.0591(15) Uani 1 1 d U . . C22 C 0.3477(9) 0.5233(4) 0.1151(3) 0.0607(15) Uani 1 1 d U A . C23 C 0.3987(8) 0.6869(4) 0.0634(3) 0.0567(15) Uani 1 1 d U . . C24 C 0.5469(8) 0.7353(4) 0.1770(3) 0.0494(14) Uani 1 1 d U . . C25 C 0.8169(9) 0.6116(4) -0.0269(3) 0.0599(15) Uani 1 1 d U . . C26 C 0.7551(8) 0.7419(4) 0.1806(3) 0.0494(14) Uani 1 1 d U . . C27 C 0.6125(9) 0.7396(4) 0.0311(3) 0.0573(15) Uani 1 1 d U . . C28 C 0.5804(8) 0.7053(4) 0.2244(2) 0.0474(14) Uani 1 1 d U A . C29 C 0.7169(8) 0.7044(4) 0.2184(2) 0.0471(14) Uani 1 1 d U A . C85 C 0.7692(8) 0.8312(4) 0.2842(3) 0.0532(16) Uani 1 1 d U . . C86 C 0.4561(8) 0.8536(4) 0.2360(3) 0.055(2) Uani 1 1 d U . . H7 H 0.4078 0.8542 0.2642 0.083 Uiso 1 1 calc R . . H8 H 0.4469 0.8177 0.2199 0.083 Uiso 1 1 calc R . . H9 H 0.4323 0.8840 0.2150 0.083 Uiso 1 1 calc R . . C30 C 0.4539(8) 0.7153(4) 0.1469(3) 0.0531(15) Uani 1 1 d U A . C31 C 0.9002(8) 0.6521(4) 0.2114(3) 0.0536(15) Uani 1 1 d U A . C32 C 0.9519(9) 0.7157(4) 0.0784(3) 0.0595(16) Uani 1 1 d U A . C33 C 0.4063(8) 0.5721(4) 0.1893(3) 0.0533(15) Uani 1 1 d U A . C34 C 0.3245(9) 0.6422(5) 0.0794(3) 0.0606(16) Uani 1 1 d U A . C35 C 0.4934(10) 0.4632(4) 0.0815(3) 0.0608(15) Uani 1 1 d U . . C87 C 0.4214(9) 0.7624(4) 0.3176(3) 0.0550(17) Uani 1 1 d U . . C88 C 0.6497(8) 0.8183(4) 0.2730(3) 0.0497(16) Uani 1 1 d U . . C36 C 0.3436(8) 0.5926(5) 0.0463(3) 0.0603(15) Uani 1 1 d U A . C37 C 0.6363(9) 0.6603(4) -0.0248(2) 0.0566(15) Uani 1 1 d U . . C38 C 0.6760(9) 0.4502(4) 0.0390(3) 0.0590(15) Uani 1 1 d U A . C89 C 0.8850(12) 0.6518(5) 0.4564(3) 0.076(2) Uani 1 1 d U . . H10 H 0.8606 0.6592 0.4875 0.091 Uiso 1 1 calc R . . C39 C 0.7579(9) 0.6675(4) -0.0222(3) 0.0575(15) Uani 1 1 d U A . C40 C 0.6055(9) 0.4402(4) 0.0802(3) 0.0592(15) Uani 1 1 d U A . C41 C 0.4453(9) 0.4994(4) 0.0446(3) 0.0623(16) Uani 1 1 d U A . C90 C 0.3361(9) 0.7971(4) 0.3925(3) 0.0621(18) Uani 1 1 d U . . H11 H 0.3466 0.8122 0.4229 0.075 Uiso 1 1 calc R . . C91 C 0.5513(9) 0.8121(4) 0.3827(3) 0.067(2) Uani 1 1 d U . . H47 H 0.6041 0.7808 0.3885 0.100 Uiso 1 1 calc R . . H48 H 0.5371 0.8322 0.4121 0.100 Uiso 1 1 calc R . . H49 H 0.5863 0.8377 0.3599 0.100 Uiso 1 1 calc R . . C42 C 0.9934(9) 0.5098(4) 0.1408(3) 0.0595(15) Uani 1 1 d U A . C43 C 0.3335(8) 0.5697(4) 0.1473(3) 0.0565(15) Uani 1 1 d U . . C44 C 0.9119(9) 0.5017(4) 0.1812(3) 0.0565(15) Uani 1 1 d U . . C45 C 0.6098(8) 0.6019(4) -0.0324(2) 0.0570(14) Uani 1 1 d U A . C46 C 0.4594(8) 0.7261(4) 0.0960(3) 0.0555(15) Uani 1 1 d U A . C47 C 0.9294(9) 0.5370(4) 0.0163(3) 0.0592(15) Uani 1 1 d U . . C48 C 0.9175(9) 0.5971(5) -0.0014(3) 0.0597(15) Uani 1 1 d U A . C49 C 0.8200(9) 0.4631(4) 0.1743(3) 0.0572(15) Uani 1 1 d U A . C50 C 0.6544(9) 0.7723(4) 0.1069(3) 0.0568(15) Uani 1 1 d U . . C51 C 0.8365(9) 0.4985(4) 0.0078(3) 0.0579(15) Uani 1 1 d U A . C52 C 0.5098(9) 0.5746(4) -0.0123(3) 0.0570(15) Uani 1 1 d U A . C53 C 0.5192(9) 0.5157(4) 0.0051(3) 0.0585(15) Uani 1 1 d U . . C92 C 0.6353(8) 0.9136(4) 0.2405(2) 0.0481(15) Uani 1 1 d U . . H15 H 0.5906 0.9413 0.2251 0.058 Uiso 1 1 calc R . . C54 C 0.5844(9) 0.5426(4) 0.2319(3) 0.0523(15) Uani 1 1 d U A . C55 C 1.0567(9) 0.6300(5) 0.0661(3) 0.0632(16) Uani 1 1 d U A . C56 C 0.8109(9) 0.7094(4) 0.0102(3) 0.0608(15) Uani 1 1 d U . . C93 C 0.8555(9) 0.7874(4) 0.3077(3) 0.061(2) Uani 1 1 d U . . H16 H 0.9355 0.8006 0.3042 0.092 Uiso 1 1 calc R . . H17 H 0.8470 0.7510 0.2924 0.092 Uiso 1 1 calc R . . H18 H 0.8370 0.7838 0.3411 0.092 Uiso 1 1 calc R . . C57 C 1.0388(9) 0.6774(4) 0.0982(3) 0.0634(16) Uani 1 1 d U . . C94 C 0.7497(8) 0.9267(4) 0.2530(3) 0.0528(16) Uani 1 1 d U . . C58 C 0.5365(8) 0.6461(4) 0.2261(2) 0.0509(14) Uani 1 1 d U . . C59 C 0.6300(10) 0.4886(4) 0.0019(3) 0.0584(15) Uani 1 1 d U A . C95 C 0.6463(9) 0.6973(4) 0.3293(2) 0.058(2) Uani 1 1 d . . . H19 H 0.7116 0.7202 0.3410 0.070 Uiso 1 1 calc R . . H20 H 0.5908 0.6955 0.3557 0.070 Uiso 1 1 calc R . . C60 C 0.8550(10) 0.4534(4) 0.0868(3) 0.0600(15) Uani 1 1 d U A . C61 C 0.4544(8) 0.6716(4) 0.0202(3) 0.0574(15) Uani 1 1 d U A . C62 C 0.4363(8) 0.6288(4) 0.1986(3) 0.0517(15) Uani 1 1 d U A . C63 C 0.4348(9) 0.4817(4) 0.1260(3) 0.0590(15) Uani 1 1 d U A . C64 C 1.0618(9) 0.5608(5) 0.1336(3) 0.0596(15) Uani 1 1 d U . . C96 C 0.6149(12) 0.5618(4) 0.3467(3) 0.072(2) Uani 1 1 d U . . C65 C 0.5613(9) 0.6955(4) 0.0033(3) 0.0568(15) Uani 1 1 d U A . C97 C 0.4359(9) 0.7899(4) 0.3633(3) 0.0588(17) Uani 1 1 d U . . C98 C 0.2840(9) 0.7198(4) 0.2553(3) 0.063(2) Uani 1 1 d U . . H21 H 0.3308 0.7383 0.2312 0.095 Uiso 1 1 calc R . . H22 H 0.2016 0.7236 0.2476 0.095 Uiso 1 1 calc R . . H23 H 0.3046 0.6801 0.2568 0.095 Uiso 1 1 calc R . . C99 C 0.4884(12) 0.5633(5) 0.3523(3) 0.075(2) Uani 1 1 d U . . C66 C 0.7322(9) 0.5177(4) -0.0175(3) 0.0603(15) Uani 1 1 d U . . C67 C 0.7216(9) 0.5721(4) -0.0353(3) 0.0587(15) Uani 1 1 d U A . C68 C 0.6140(10) 0.4514(4) 0.1680(3) 0.0593(15) Uani 1 1 d U . . C100 C 0.7979(11) 0.6412(5) 0.4217(3) 0.0718(19) Uani 1 1 d U . . C69 C 0.7100(9) 0.4683(4) 0.1987(3) 0.0591(15) Uani 1 1 d U A . C70 C 0.6491(9) 0.7604(4) 0.1563(3) 0.0520(15) Uani 1 1 d U A . C101 C 0.1203(11) 0.7960(5) 0.4096(3) 0.078(3) Uani 1 1 d U . . H24 H 0.1485 0.8083 0.4403 0.116 Uiso 1 1 calc R . . H25 H 0.0725 0.7624 0.4135 0.116 Uiso 1 1 calc R . . H26 H 0.0738 0.8257 0.3954 0.116 Uiso 1 1 calc R . . C102 C 1.0408(11) 0.6416(5) 0.3994(3) 0.080(2) Uani 1 1 d U . . H27 H 1.1213 0.6422 0.3924 0.096 Uiso 1 1 calc R . . C103 C 0.9598(11) 0.6307(5) 0.3636(3) 0.0738(19) Uani 1 1 d U . . C104 C 0.4932(14) 0.4645(5) 0.3758(3) 0.090(2) Uani 1 1 d U . . C105 C 0.2134(10) 0.7578(4) 0.3343(3) 0.0605(17) Uani 1 1 d U . . H28 H 0.1385 0.7470 0.3239 0.073 Uiso 1 1 calc R . . C71 C 0.8626(9) 0.7355(4) 0.1563(3) 0.0536(15) Uani 1 1 d U A . C72 C 0.7349(9) 0.7468(4) 0.0338(3) 0.0575(15) Uani 1 1 d U A . C106 C 0.8117(8) 0.8853(4) 0.2748(3) 0.0551(17) Uani 1 1 d U . . H29 H 0.8887 0.8937 0.2843 0.066 Uiso 1 1 calc R . . C107 C 1.0127(11) 0.6197(5) 0.3143(3) 0.077(3) Uani 1 1 d U . . H30 H 0.9597 0.5963 0.2961 0.115 Uiso 1 1 calc R . . H31 H 1.0873 0.6005 0.3177 0.115 Uiso 1 1 calc R . . H32 H 1.0245 0.6554 0.2982 0.115 Uiso 1 1 calc R . . C73 C 0.7668(9) 0.7650(4) 0.0824(3) 0.0590(15) Uani 1 1 d U A . C74 C 0.3206(9) 0.6277(4) 0.1309(3) 0.0591(16) Uani 1 1 d U A . C108 C 0.2230(10) 0.7827(4) 0.3782(3) 0.0634(17) Uani 1 1 d U . . C109 C 0.6152(14) 0.4604(5) 0.3682(3) 0.086(2) Uani 1 1 d U . . H33 H 0.6538 0.4256 0.3719 0.103 Uiso 1 1 calc R . . C110 C 0.4313(13) 0.5169(5) 0.3674(3) 0.083(2) Uani 1 1 d U . . H34 H 0.3501 0.5186 0.3727 0.100 Uiso 1 1 calc R . . C111 C 0.8340(10) 0.6305(5) 0.3739(3) 0.0708(19) Uani 1 1 d U . . C75 C 1.0658(9) 0.5733(5) 0.0838(3) 0.0631(16) Uani 1 1 d U A . C76 C 0.6654(9) 0.4324(4) 0.1244(3) 0.0582(15) Uani 1 1 d U A . C112 C 0.8012(10) 0.9836(5) 0.2427(4) 0.070(3) Uani 1 1 d U . . H35 H 0.8835 0.9794 0.2348 0.105 Uiso 1 1 calc R . . H36 H 0.7934 1.0076 0.2703 0.105 Uiso 1 1 calc R . . H37 H 0.7602 1.0006 0.2163 0.105 Uiso 1 1 calc R . . C77 C 0.5582(9) 0.7553(4) 0.0770(3) 0.0559(15) Uani 1 1 d U A . C78 C 0.7921(9) 0.4370(4) 0.1277(3) 0.0588(15) Uani 1 1 d U . . C113 C 0.6769(11) 0.6419(5) 0.4389(3) 0.077(3) Uani 1 1 d U . . H38 H 0.6760 0.6338 0.4726 0.116 Uiso 1 1 calc R . . H39 H 0.6316 0.6135 0.4223 0.116 Uiso 1 1 calc R . . H40 H 0.6429 0.6789 0.4334 0.116 Uiso 1 1 calc R . . C114 C 1.1008(13) 0.6618(6) 0.4844(4) 0.101(3) Uani 1 1 d U . . H41 H 1.0948 0.6337 0.5092 0.151 Uiso 1 1 calc R . . H42 H 1.0926 0.6992 0.4980 0.151 Uiso 1 1 calc R . . H43 H 1.1765 0.6587 0.4691 0.151 Uiso 1 1 calc R . . C115 C 0.4120(15) 0.4115(6) 0.3902(4) 0.120(4) Uani 1 1 d U . . H44 H 0.3997 0.3877 0.3628 0.179 Uiso 1 1 calc R . . H45 H 0.3371 0.4251 0.4017 0.179 Uiso 1 1 calc R . . H46 H 0.4505 0.3899 0.4149 0.179 Uiso 1 1 calc R . . S1 S 0.6958(4) 0.69485(17) -0.13975(10) 0.0973(10) Uani 1 1 d U B 1 S3 S 0.3120(4) 0.6084(2) 0.58627(16) 0.1255(14) Uani 1 1 d U C 1 S2 S 0.6276(4) 0.6377(2) -0.23367(14) 0.1203(13) Uani 1 1 d U B 1 S4 S 0.3804(6) 0.5770(3) 0.48360(19) 0.191(3) Uani 1 1 d U C 1 C116 C 0.6550(13) 0.6666(6) -0.1856(4) 0.103(3) Uani 1 1 d U B 1 C117 C 0.3510(15) 0.5967(9) 0.5350(6) 0.145(4) Uani 1 1 d U C 1 S6 S 0.1003(9) 0.3880(4) 0.3580(3) 0.133(2) Uani 0.50 1 d PDU D 1 S5 S 0.1239(10) 0.5071(4) 0.4001(4) 0.139(2) Uani 0.50 1 d PDU D 1 Ce3 Ce 0.6290(18) 0.5245(8) 0.1290(5) 0.079(5) Uani 0.0422(14) 1 d P A 3 Ce4 Ce 0.7543(13) 0.6815(8) 0.0906(5) 0.073(5) Uani 0.0422(14) 1 d P A 3 C118 C 0.122(3) 0.4467(7) 0.3792(11) 0.136(2) Uani 0.50 1 d PDU . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ce1 0.0628(3) 0.0435(4) 0.0441(2) -0.00068(19) 0.00224(18) -0.0039(2) Ce2 0.0604(3) 0.0452(4) 0.0461(2) -0.0009(2) 0.00411(18) 0.0014(2) Si1 0.0741(16) 0.0352(19) 0.0396(10) -0.0012(9) 0.0010(9) 0.0075(12) Si2 0.0926(19) 0.0413(19) 0.0346(10) 0.0006(9) 0.0016(10) 0.0115(13) C79 0.159(8) 0.048(7) 0.050(4) 0.007(4) -0.010(5) 0.022(6) C1 0.073(3) 0.045(3) 0.048(3) -0.002(2) 0.005(2) 0.004(3) C2 0.077(3) 0.043(3) 0.046(2) -0.002(3) -0.006(2) 0.008(3) C3 0.076(3) 0.053(4) 0.051(3) 0.005(3) 0.012(3) -0.002(3) C4 0.081(3) 0.039(3) 0.038(2) 0.001(2) 0.011(2) 0.002(3) C5 0.073(3) 0.044(3) 0.049(3) -0.003(3) 0.000(3) -0.008(3) C6 0.081(3) 0.045(3) 0.057(3) -0.005(3) 0.007(3) 0.015(3) C7 0.086(3) 0.037(3) 0.037(2) 0.002(2) 0.000(2) 0.008(3) C8 0.079(3) 0.038(3) 0.045(2) 0.001(2) 0.013(3) -0.008(3) C9 0.082(3) 0.040(3) 0.044(3) 0.000(2) -0.006(2) 0.012(3) C80 0.123(7) 0.046(7) 0.055(4) 0.008(4) 0.016(4) 0.004(5) C10 0.089(3) 0.037(3) 0.041(2) 0.007(2) 0.008(3) 0.005(3) C81 0.064(3) 0.037(4) 0.045(3) -0.004(3) 0.000(3) 0.002(3) C11 0.082(3) 0.049(3) 0.058(3) -0.003(3) 0.012(3) 0.010(3) C12 0.074(3) 0.049(3) 0.055(3) -0.006(3) 0.003(3) -0.003(3) C13 0.074(3) 0.051(3) 0.049(3) -0.002(3) -0.010(2) 0.001(3) C82 0.149(5) 0.046(5) 0.037(3) 0.002(3) -0.018(3) -0.005(4) C14 0.072(3) 0.048(3) 0.054(3) -0.009(3) 0.000(2) 0.006(3) C15 0.086(3) 0.035(3) 0.052(3) 0.004(2) 0.009(3) -0.011(3) C16 0.079(3) 0.045(3) 0.058(3) -0.007(3) -0.001(3) -0.014(3) C17 0.079(3) 0.038(3) 0.038(2) -0.001(2) 0.000(2) 0.007(3) C18 0.075(3) 0.041(3) 0.054(3) 0.004(3) 0.006(3) -0.019(3) C83 0.122(5) 0.066(4) 0.051(3) -0.003(3) -0.018(3) 0.008(4) C19 0.075(3) 0.036(3) 0.039(2) -0.005(2) -0.002(2) 0.002(3) C20 0.078(3) 0.052(3) 0.052(3) 0.010(3) 0.011(3) -0.013(3) C84 0.085(4) 0.037(4) 0.047(3) 0.001(3) 0.009(3) -0.002(3) C21 0.088(3) 0.042(3) 0.048(3) -0.010(2) 0.006(3) 0.006(3) C22 0.076(3) 0.045(3) 0.061(3) -0.005(3) 0.006(3) -0.015(3) C23 0.071(3) 0.045(3) 0.054(3) 0.005(3) -0.007(3) 0.008(3) C24 0.072(3) 0.033(3) 0.044(2) -0.002(2) 0.001(2) 0.009(3) C25 0.084(3) 0.053(4) 0.042(2) 0.003(3) 0.010(2) -0.005(3) C26 0.071(3) 0.032(3) 0.045(2) -0.001(2) -0.002(2) -0.003(3) C27 0.084(3) 0.043(3) 0.045(3) 0.012(2) 0.000(3) 0.001(3) C28 0.072(3) 0.033(3) 0.037(2) -0.001(2) 0.002(2) 0.007(3) C29 0.074(3) 0.030(3) 0.037(2) -0.002(2) 0.001(2) 0.002(3) C85 0.068(3) 0.043(4) 0.049(3) -0.010(3) -0.001(3) 0.007(3) C86 0.076(6) 0.032(6) 0.057(4) 0.000(4) 0.000(4) 0.001(4) C30 0.072(3) 0.040(3) 0.047(3) 0.001(2) 0.001(2) 0.008(3) C31 0.076(3) 0.042(3) 0.043(3) -0.004(2) -0.003(2) 0.000(3) C32 0.076(3) 0.046(3) 0.056(3) 0.007(3) 0.010(3) -0.018(3) C33 0.073(3) 0.039(3) 0.048(3) -0.003(2) 0.014(2) -0.006(3) C34 0.072(3) 0.050(4) 0.060(3) -0.004(3) -0.004(3) 0.002(3) C35 0.086(3) 0.042(3) 0.055(3) -0.008(3) 0.002(3) -0.012(3) C87 0.086(4) 0.035(4) 0.044(3) 0.002(3) 0.008(3) 0.002(3) C88 0.064(3) 0.040(4) 0.046(3) -0.008(3) 0.001(3) 0.004(3) C36 0.074(3) 0.050(3) 0.056(3) -0.007(3) -0.006(2) -0.005(3) C37 0.085(3) 0.049(3) 0.036(2) 0.008(2) 0.000(3) -0.006(3) C38 0.087(3) 0.040(3) 0.049(3) -0.009(3) 0.003(3) 0.000(3) C89 0.125(5) 0.056(4) 0.047(3) -0.002(3) -0.011(3) 0.002(4) C39 0.085(3) 0.051(3) 0.036(2) 0.008(2) 0.007(3) -0.006(3) C40 0.086(3) 0.038(3) 0.053(3) -0.006(3) 0.002(3) -0.004(3) C41 0.084(3) 0.045(3) 0.057(3) -0.009(3) -0.001(3) -0.013(3) C90 0.099(4) 0.041(4) 0.047(3) -0.001(3) 0.011(3) 0.003(3) C91 0.101(7) 0.048(6) 0.052(4) -0.012(4) 0.006(4) 0.007(5) C42 0.082(3) 0.043(3) 0.053(3) -0.003(3) 0.002(3) 0.014(3) C43 0.072(3) 0.043(3) 0.054(3) -0.005(3) 0.010(3) -0.012(3) C44 0.081(3) 0.039(3) 0.049(3) 0.000(3) -0.002(3) 0.014(3) C45 0.082(3) 0.050(3) 0.038(2) 0.001(3) -0.003(2) -0.007(3) C46 0.075(3) 0.040(3) 0.051(3) 0.004(2) -0.003(2) 0.010(3) C47 0.082(3) 0.050(3) 0.046(3) -0.004(3) 0.011(3) 0.007(3) C48 0.079(3) 0.055(3) 0.045(2) 0.001(3) 0.012(2) 0.000(3) C49 0.085(3) 0.035(3) 0.051(3) 0.004(3) 0.006(3) 0.012(3) C50 0.083(3) 0.037(3) 0.050(3) 0.006(2) 0.001(3) -0.003(3) C51 0.085(3) 0.044(3) 0.045(3) -0.007(2) 0.009(2) 0.007(3) C52 0.077(3) 0.049(3) 0.045(2) -0.006(2) -0.007(2) -0.006(3) C53 0.083(3) 0.044(3) 0.048(3) -0.009(2) -0.003(3) -0.011(3) C92 0.064(3) 0.033(4) 0.047(3) -0.002(3) 0.003(3) 0.002(3) C54 0.083(3) 0.035(3) 0.038(2) 0.002(2) 0.014(2) -0.003(3) C55 0.075(3) 0.054(4) 0.060(3) 0.001(3) 0.014(3) -0.006(3) C56 0.084(3) 0.052(3) 0.046(3) 0.011(3) 0.010(3) -0.008(3) C93 0.076(5) 0.042(6) 0.066(5) -0.001(4) -0.009(4) 0.014(4) C57 0.076(3) 0.053(4) 0.061(3) -0.001(3) 0.010(3) -0.010(3) C94 0.068(3) 0.037(4) 0.054(3) -0.003(3) 0.001(3) 0.001(3) C58 0.074(3) 0.040(3) 0.038(2) -0.002(2) 0.006(2) 0.005(3) C59 0.087(3) 0.041(3) 0.047(3) -0.012(2) 0.000(3) -0.001(3) C95 0.105(7) 0.034(7) 0.036(4) -0.001(3) 0.003(4) 0.019(5) C60 0.086(3) 0.040(3) 0.054(3) -0.004(3) 0.006(3) 0.011(3) C61 0.076(3) 0.047(3) 0.048(3) 0.002(3) -0.011(2) 0.002(3) C62 0.072(3) 0.041(3) 0.042(2) -0.003(2) 0.009(2) 0.001(3) C63 0.082(3) 0.039(3) 0.057(3) -0.003(3) 0.007(3) -0.018(3) C64 0.076(3) 0.048(4) 0.054(3) -0.005(3) 0.004(3) 0.009(3) C96 0.142(5) 0.041(5) 0.033(3) 0.006(3) -0.009(3) -0.009(4) C65 0.083(3) 0.046(3) 0.042(3) 0.009(2) -0.004(2) -0.001(3) C97 0.091(4) 0.037(4) 0.048(3) 0.002(3) 0.009(3) 0.007(3) C98 0.084(6) 0.051(6) 0.055(4) -0.009(4) 0.004(4) 0.004(5) C99 0.140(5) 0.043(5) 0.040(3) 0.007(3) -0.010(3) -0.017(4) C66 0.090(3) 0.045(3) 0.046(3) -0.009(3) 0.006(3) 0.003(3) C67 0.086(3) 0.050(3) 0.041(2) -0.002(2) 0.004(3) -0.006(3) C68 0.090(3) 0.034(3) 0.053(3) 0.004(2) 0.008(3) -0.006(3) C100 0.120(5) 0.053(4) 0.043(3) 0.000(3) -0.009(3) 0.007(4) C69 0.091(3) 0.036(3) 0.050(3) 0.003(3) 0.009(3) 0.006(3) C70 0.079(3) 0.032(3) 0.045(2) -0.001(2) 0.000(2) 0.001(3) C101 0.103(7) 0.061(7) 0.068(5) -0.017(4) 0.025(5) -0.004(5) C102 0.117(5) 0.069(4) 0.054(3) -0.002(3) -0.019(3) 0.015(4) C103 0.109(4) 0.064(4) 0.048(3) -0.004(3) -0.016(3) 0.018(4) C104 0.160(5) 0.054(5) 0.055(3) 0.010(3) -0.031(4) -0.028(4) C105 0.092(4) 0.040(4) 0.050(3) -0.002(3) 0.009(3) 0.001(3) C71 0.073(3) 0.039(3) 0.049(3) 0.001(2) -0.001(3) -0.010(3) C72 0.084(3) 0.043(3) 0.046(3) 0.010(2) 0.005(3) -0.004(3) C106 0.067(3) 0.042(4) 0.057(3) -0.006(3) -0.001(3) 0.000(3) C107 0.097(6) 0.078(7) 0.056(4) 0.001(4) -0.014(4) 0.020(5) C73 0.083(3) 0.041(3) 0.054(3) 0.008(3) 0.007(3) -0.008(3) C74 0.074(3) 0.047(3) 0.056(3) -0.004(3) 0.004(3) -0.003(3) C108 0.094(4) 0.041(4) 0.054(3) -0.001(3) 0.018(3) 0.001(3) C109 0.156(5) 0.051(5) 0.051(3) 0.005(3) -0.031(4) -0.017(4) C110 0.150(5) 0.051(5) 0.049(3) 0.011(3) -0.020(4) -0.025(4) C111 0.113(5) 0.057(4) 0.042(3) 0.001(3) -0.010(3) 0.016(4) C75 0.079(3) 0.051(4) 0.060(3) -0.006(3) 0.011(3) 0.009(3) C76 0.088(3) 0.034(3) 0.052(3) -0.002(3) 0.007(3) -0.001(3) C112 0.077(6) 0.058(7) 0.076(5) 0.000(5) 0.009(4) -0.010(5) C77 0.080(3) 0.040(3) 0.048(3) 0.007(2) -0.004(2) 0.003(3) C78 0.088(3) 0.036(3) 0.052(3) -0.001(3) 0.005(3) 0.008(3) C113 0.125(7) 0.062(7) 0.045(4) 0.003(4) 0.003(4) -0.001(6) C114 0.146(8) 0.097(8) 0.059(5) -0.003(5) -0.023(5) -0.007(7) C115 0.183(9) 0.084(8) 0.092(6) 0.021(6) -0.044(7) -0.050(7) S1 0.131(3) 0.089(3) 0.0713(17) 0.0036(15) 0.0066(16) 0.003(2) S3 0.103(3) 0.143(4) 0.131(3) -0.017(3) -0.001(2) 0.021(3) S2 0.130(3) 0.135(4) 0.096(2) -0.011(2) -0.017(2) -0.009(3) S4 0.179(5) 0.263(7) 0.131(3) 0.042(4) 0.035(3) 0.101(5) C116 0.127(6) 0.102(6) 0.080(5) -0.004(5) -0.002(5) 0.010(6) C117 0.116(6) 0.203(8) 0.117(6) 0.009(7) 0.015(6) 0.068(6) S6 0.133(2) 0.134(2) 0.132(2) 0.0025(10) 0.0012(10) 0.0004(10) S5 0.140(2) 0.138(2) 0.140(2) -0.0017(10) 0.0014(10) -0.0003(10) Ce3 0.111(13) 0.067(13) 0.060(7) -0.007(6) 0.011(7) 0.017(10) Ce4 0.067(9) 0.091(14) 0.062(7) 0.006(7) 0.004(6) -0.008(8) C118 0.136(3) 0.136(2) 0.136(3) 0.0002(10) 0.0000(10) -0.0001(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ce1 C74 2.462(10) . ? Ce1 C43 2.481(9) . ? Ce1 C36 2.500(9) . ? Ce1 C34 2.508(10) . ? Ce1 C16 2.554(9) . ? Ce1 C22 2.558(9) . ? Ce1 C1 2.749(9) . ? Ce1 C23 2.750(9) . ? Ce1 C33 2.778(8) . ? Ce1 C13 2.809(8) . ? Ce1 C41 2.880(9) . ? Ce1 C63 2.885(9) . ? Ce2 C14 2.479(9) . ? Ce2 C64 2.486(10) . ? Ce2 C12 2.494(10) . ? Ce2 C75 2.497(10) . ? Ce2 C57 2.542(10) . ? Ce2 C55 2.546(9) . ? Ce2 C5 2.760(9) . ? Ce2 C2 2.761(7) . ? Ce2 C42 2.788(9) . ? Ce2 C11 2.812(9) . ? Ce2 C32 2.868(9) . ? Ce2 C3 2.886(8) . ? Si1 C95 1.901(8) . ? Si1 C88 1.928(10) . ? Si1 C87 1.935(10) . ? Si1 C28 1.976(8) . ? Si2 C96 1.874(11) . ? Si2 C95 1.884(9) . ? Si2 C111 1.900(10) . ? Si2 C17 1.979(7) . ? C79 C82 1.502(17) . ? C79 H1 0.9600 . ? C79 H2 0.9600 . ? C79 H3 0.9600 . ? C1 C74 1.448(13) . ? C1 C62 1.449(12) . ? C1 C30 1.453(13) . ? C2 C14 1.413(12) . ? C2 C31 1.430(13) . ? C2 C9 1.455(14) . ? C3 C20 1.401(14) . ? C3 C48 1.415(13) . ? C3 C55 1.485(13) . ? C4 C54 1.414(13) . ? C4 C58 1.426(12) . ? C4 C17 1.559(13) . ? C5 C71 1.405(13) . ? C5 C12 1.479(13) . ? C5 C31 1.486(13) . ? C6 C11 1.441(13) . ? C6 C60 1.445(15) . ? C6 C42 1.449(12) . ? C7 C9 1.368(13) . ? C7 C10 1.427(14) . ? C7 C17 1.559(12) . ? C8 C33 1.419(13) . ? C8 C54 1.433(13) . ? C8 C15 1.467(12) . ? C8 Ce3 2.614(17) . ? C9 C44 1.445(12) . ? C80 C99 1.436(15) . ? C80 H4 0.9600 . ? C80 H5 0.9600 . ? C80 H6 0.9600 . ? C10 C69 1.420(13) . ? C10 C54 1.431(14) . ? C10 Ce3 2.973(17) . ? C81 C92 1.376(12) . ? C81 C88 1.421(12) . ? C81 C86 1.500(12) . ? C11 C47 1.446(13) . ? C11 C75 1.456(14) . ? C12 C57 1.429(12) . ? C12 C14 1.458(14) . ? C13 C52 1.431(14) . ? C13 C36 1.451(13) . ? C13 C61 1.465(14) . ? C82 C109 1.336(15) . ? C82 C96 1.475(16) . ? C14 C64 1.469(13) . ? C15 C68 1.422(15) . ? C15 C63 1.432(13) . ? C15 Ce3 2.09(2) . ? C16 C41 1.426(14) . ? C16 C36 1.439(14) . ? C16 C22 1.474(12) . ? C17 C19 1.483(12) . ? C18 C73 1.396(14) . ? C18 C32 1.416(13) . ? C18 C71 1.439(11) . ? C18 Ce4 2.060(18) . ? C83 C89 1.340(17) . ? C83 C102 1.429(14) . ? C83 C114 1.552(15) . ? C19 C29 1.384(12) . ? C19 C31 1.428(12) . ? C20 C32 1.438(13) . ? C20 C56 1.465(14) . ? C20 Ce4 2.532(16) . ? C84 C87 1.377(13) . ? C84 C105 1.386(13) . ? C84 C98 1.538(11) . ? C21 C38 1.405(14) . ? C21 C51 1.408(13) . ? C21 C60 1.416(13) . ? C22 C63 1.419(15) . ? C22 C43 1.420(13) . ? C23 C61 1.410(12) . ? C23 C34 1.414(14) . ? C23 C46 1.465(13) . ? C24 C70 1.420(13) . ? C24 C30 1.425(12) . ? C24 C28 1.548(10) . ? C25 C48 1.385(13) . ? C25 C67 1.439(13) . ? C25 C39 1.475(14) . ? C26 C71 1.400(13) . ? C26 C70 1.444(12) . ? C26 C29 1.444(11) . ? C26 Ce4 2.891(17) . ? C27 C72 1.395(14) . ? C27 C65 1.417(13) . ? C27 C77 1.469(12) . ? C27 Ce4 2.681(17) . ? C28 C58 1.474(13) . ? C28 C29 1.552(12) . ? C85 C106 1.380(13) . ? C85 C88 1.419(12) . ? C85 C93 1.561(12) . ? C86 H7 0.9600 . ? C86 H8 0.9600 . ? C86 H9 0.9600 . ? C30 C46 1.450(11) . ? C32 C57 1.442(14) . ? C32 Ce4 2.397(17) . ? C33 C62 1.395(13) . ? C33 C43 1.438(13) . ? C34 C74 1.482(13) . ? C34 C36 1.501(13) . ? C35 C40 1.377(15) . ? C35 C41 1.442(14) . ? C35 C63 1.477(12) . ? C35 Ce3 2.49(2) . ? C87 C97 1.441(12) . ? C37 C39 1.386(13) . ? C37 C45 1.417(13) . ? C37 C65 1.421(13) . ? C38 C40 1.421(13) . ? C38 C59 1.470(13) . ? C89 C100 1.405(14) . ? C89 H10 0.9300 . ? C39 C56 1.465(13) . ? C40 C76 1.422(13) . ? C40 Ce3 2.416(19) . ? C41 C53 1.437(13) . ? C90 C108 1.381(14) . ? C90 C97 1.403(13) . ? C90 H11 0.9300 . ? C91 C97 1.506(14) . ? C91 H47 0.9600 . ? C91 H48 0.9600 . ? C91 H49 0.9600 . ? C42 C64 1.438(14) . ? C42 C44 1.470(13) . ? C43 C74 1.441(14) . ? C44 C49 1.392(14) . ? C45 C52 1.416(13) . ? C45 C67 1.446(14) . ? C46 C77 1.413(13) . ? C47 C51 1.405(14) . ? C47 C48 1.499(14) . ? C49 C69 1.424(13) . ? C49 C78 1.474(12) . ? C49 Ce3 2.89(2) . ? C50 C70 1.413(11) . ? C50 C77 1.430(12) . ? C50 C73 1.454(13) . ? C50 Ce4 2.45(2) . ? C51 C66 1.446(13) . ? C52 C53 1.466(13) . ? C53 C59 1.408(14) . ? C92 C94 1.373(12) . ? C92 H15 0.9300 . ? C54 Ce3 2.954(15) . ? C55 C75 1.422(14) . ? C55 C57 1.443(14) . ? C56 C72 1.394(13) . ? C56 Ce4 2.429(15) . ? C93 H16 0.9600 . ? C93 H17 0.9600 . ? C93 H18 0.9600 . ? C94 C106 1.344(13) . ? C94 C112 1.483(14) . ? C58 C62 1.428(12) . ? C59 C66 1.446(14) . ? C95 H19 0.9700 . ? C95 H20 0.9700 . ? C60 C78 1.401(13) . ? C61 C65 1.414(13) . ? C63 Ce3 2.41(2) . ? C64 C75 1.423(12) . ? C96 C99 1.438(18) . ? C98 H21 0.9600 . ? C98 H22 0.9600 . ? C98 H23 0.9600 . ? C99 C110 1.334(15) . ? C66 C67 1.374(13) . ? C68 C76 1.422(12) . ? C68 C69 1.439(14) . ? C68 Ce3 2.039(19) . ? C100 C111 1.420(13) . ? C100 C113 1.450(16) . ? C69 Ce3 2.527(18) . ? C70 Ce4 2.868(18) . ? C101 C108 1.489(14) . ? C101 H24 0.9600 . ? C101 H25 0.9600 . ? C101 H26 0.9600 . ? C102 C103 1.381(14) . ? C102 H27 0.9300 . ? C103 C111 1.451(16) . ? C103 C107 1.525(13) . ? C104 C109 1.398(19) . ? C104 C110 1.431(18) . ? C104 C115 1.596(17) . ? C105 C108 1.365(12) . ? C105 H28 0.9300 . ? C71 Ce4 2.546(17) . ? C72 C73 1.472(12) . ? C72 Ce4 2.218(17) . ? C106 H29 0.9300 . ? C107 H30 0.9600 . ? C107 H31 0.9600 . ? C107 H32 0.9600 . ? C73 Ce4 1.98(2) . ? C109 H33 0.9300 . ? C110 H34 0.9300 . ? C76 C78 1.439(14) . ? C76 Ce3 2.200(19) . ? C112 H35 0.9600 . ? C112 H36 0.9600 . ? C112 H37 0.9600 . ? C77 Ce4 2.837(19) . ? C78 Ce3 2.76(2) . ? C113 H38 0.9600 . ? C113 H39 0.9600 . ? C113 H40 0.9600 . ? C114 H41 0.9600 . ? C114 H42 0.9600 . ? C114 H43 0.9600 . ? C115 H44 0.9600 . ? C115 H45 0.9600 . ? C115 H46 0.9600 . ? S1 C116 1.516(13) . ? S3 C117 1.526(16) . ? S2 C116 1.538(13) . ? S4 C117 1.547(17) . ? S6 C118 1.518(9) . ? S5 C118 1.532(9) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C74 Ce1 C43 33.9(3) . . ? C74 Ce1 C36 61.0(3) . . ? C43 Ce1 C36 70.6(3) . . ? C74 Ce1 C34 34.7(3) . . ? C43 Ce1 C34 61.5(3) . . ? C36 Ce1 C34 34.9(3) . . ? C74 Ce1 C16 70.8(3) . . ? C43 Ce1 C16 59.4(3) . . ? C36 Ce1 C16 33.1(3) . . ? C34 Ce1 C16 61.2(3) . . ? C74 Ce1 C22 59.8(3) . . ? C43 Ce1 C22 32.7(3) . . ? C36 Ce1 C22 59.7(3) . . ? C34 Ce1 C22 71.8(3) . . ? C16 Ce1 C22 33.5(3) . . ? C74 Ce1 C1 31.7(3) . . ? C43 Ce1 C1 53.3(3) . . ? C36 Ce1 C1 89.1(3) . . ? C34 Ce1 C1 55.9(3) . . ? C16 Ce1 C1 102.3(3) . . ? C22 Ce1 C1 85.4(3) . . ? C74 Ce1 C23 57.1(3) . . ? C43 Ce1 C23 89.5(3) . . ? C36 Ce1 C23 52.8(3) . . ? C34 Ce1 C23 30.8(3) . . ? C16 Ce1 C23 85.3(3) . . ? C22 Ce1 C23 102.3(3) . . ? C1 Ce1 C23 61.3(3) . . ? C74 Ce1 C33 51.7(3) . . ? C43 Ce1 C33 31.1(3) . . ? C36 Ce1 C33 101.6(3) . . ? C34 Ce1 C33 85.9(3) . . ? C16 Ce1 C33 87.2(3) . . ? C22 Ce1 C33 54.8(3) . . ? C1 Ce1 C33 49.8(3) . . ? C23 Ce1 C33 106.7(3) . . ? C74 Ce1 C13 86.1(3) . . ? C43 Ce1 C13 101.6(3) . . ? C36 Ce1 C13 31.0(3) . . ? C34 Ce1 C13 52.5(3) . . ? C16 Ce1 C13 54.8(3) . . ? C22 Ce1 C13 87.2(3) . . ? C1 Ce1 C13 106.5(3) . . ? C23 Ce1 C13 49.5(3) . . ? C33 Ce1 C13 132.4(3) . . ? C74 Ce1 C41 100.2(3) . . ? C43 Ce1 C41 82.5(3) . . ? C36 Ce1 C41 54.1(3) . . ? C34 Ce1 C41 87.7(3) . . ? C16 Ce1 C41 29.7(3) . . ? C22 Ce1 C41 50.3(3) . . ? C1 Ce1 C41 131.4(3) . . ? C23 Ce1 C41 104.6(3) . . ? C33 Ce1 C41 102.7(3) . . ? C13 Ce1 C41 59.3(3) . . ? C74 Ce1 C63 85.9(3) . . ? C43 Ce1 C63 53.2(3) . . ? C36 Ce1 C63 82.9(3) . . ? C34 Ce1 C63 101.1(3) . . ? C16 Ce1 C63 50.4(3) . . ? C22 Ce1 C63 29.4(3) . . ? C1 Ce1 C63 104.3(3) . . ? C23 Ce1 C63 131.2(3) . . ? C33 Ce1 C63 58.8(3) . . ? C13 Ce1 C63 103.0(3) . . ? C41 Ce1 C63 47.5(3) . . ? C14 Ce2 C64 34.4(3) . . ? C14 Ce2 C12 34.1(3) . . ? C64 Ce2 C12 60.4(3) . . ? C14 Ce2 C75 60.1(3) . . ? C64 Ce2 C75 33.2(3) . . ? C12 Ce2 C75 69.2(3) . . ? C14 Ce2 C57 60.7(3) . . ? C64 Ce2 C57 70.9(3) . . ? C12 Ce2 C57 32.9(3) . . ? C75 Ce2 C57 59.3(3) . . ? C14 Ce2 C55 70.2(3) . . ? C64 Ce2 C55 59.2(3) . . ? C12 Ce2 C55 58.3(3) . . ? C75 Ce2 C55 32.7(3) . . ? C57 Ce2 C55 32.9(3) . . ? C14 Ce2 C5 53.1(3) . . ? C64 Ce2 C5 86.7(3) . . ? C12 Ce2 C5 32.2(3) . . ? C75 Ce2 C5 101.3(3) . . ? C57 Ce2 C5 55.0(3) . . ? C55 Ce2 C5 86.7(3) . . ? C14 Ce2 C2 30.7(3) . . ? C64 Ce2 C2 55.7(3) . . ? C12 Ce2 C2 53.1(3) . . ? C75 Ce2 C2 87.4(3) . . ? C57 Ce2 C2 85.5(3) . . ? C55 Ce2 C2 100.8(3) . . ? C5 Ce2 C2 51.1(3) . . ? C14 Ce2 C42 56.0(3) . . ? C64 Ce2 C42 31.0(3) . . ? C12 Ce2 C42 88.3(3) . . ? C75 Ce2 C42 51.9(3) . . ? C57 Ce2 C42 101.7(3) . . ? C55 Ce2 C42 84.1(3) . . ? C5 Ce2 C42 107.3(3) . . ? C2 Ce2 C42 60.4(3) . . ? C14 Ce2 C11 85.4(3) . . ? C64 Ce2 C11 51.6(3) . . ? C12 Ce2 C11 100.3(3) . . ? C75 Ce2 C11 31.1(3) . . ? C57 Ce2 C11 86.5(3) . . ? C55 Ce2 C11 54.4(3) . . ? C5 Ce2 C11 132.3(3) . . ? C2 Ce2 C11 105.3(3) . . ? C42 Ce2 C11 49.3(3) . . ? C14 Ce2 C32 87.4(3) . . ? C64 Ce2 C32 100.9(3) . . ? C12 Ce2 C32 54.3(3) . . ? C75 Ce2 C32 83.4(3) . . ? C57 Ce2 C32 30.1(3) . . ? C55 Ce2 C32 51.2(3) . . ? C5 Ce2 C32 58.6(3) . . ? C2 Ce2 C32 105.1(3) . . ? C42 Ce2 C32 131.4(3) . . ? C11 Ce2 C32 102.9(3) . . ? C14 Ce2 C3 100.9(3) . . ? C64 Ce2 C3 86.6(3) . . ? C12 Ce2 C3 83.0(3) . . ? C75 Ce2 C3 54.5(3) . . ? C57 Ce2 C3 50.7(3) . . ? C55 Ce2 C3 30.9(3) . . ? C5 Ce2 C3 103.1(3) . . ? C2 Ce2 C3 131.3(3) . . ? C42 Ce2 C3 103.8(3) . . ? C11 Ce2 C3 58.5(3) . . ? C32 Ce2 C3 48.2(3) . . ? C95 Si1 C88 115.8(4) . . ? C95 Si1 C87 102.1(4) . . ? C88 Si1 C87 109.3(4) . . ? C95 Si1 C28 103.0(4) . . ? C88 Si1 C28 104.1(3) . . ? C87 Si1 C28 123.0(4) . . ? C96 Si2 C95 118.7(5) . . ? C96 Si2 C111 107.9(5) . . ? C95 Si2 C111 100.8(4) . . ? C96 Si2 C17 103.6(4) . . ? C95 Si2 C17 103.2(3) . . ? C111 Si2 C17 123.8(4) . . ? C82 C79 H1 109.5 . . ? C82 C79 H2 109.5 . . ? H1 C79 H2 109.5 . . ? C82 C79 H3 109.5 . . ? H1 C79 H3 109.5 . . ? H2 C79 H3 109.5 . . ? C74 C1 C62 105.3(8) . . ? C74 C1 C30 126.1(8) . . ? C62 C1 C30 118.9(8) . . ? C74 C1 Ce1 63.2(5) . . ? C62 C1 Ce1 82.8(5) . . ? C30 C1 Ce1 92.1(5) . . ? C14 C2 C31 107.6(8) . . ? C14 C2 C9 126.3(8) . . ? C31 C2 C9 115.4(8) . . ? C14 C2 Ce2 63.6(4) . . ? C31 C2 Ce2 82.4(5) . . ? C9 C2 Ce2 91.4(5) . . ? C20 C3 C48 119.5(9) . . ? C20 C3 C55 106.5(8) . . ? C48 C3 C55 125.3(9) . . ? C20 C3 Ce2 85.0(5) . . ? C48 C3 Ce2 93.1(5) . . ? C55 C3 Ce2 61.8(4) . . ? C54 C4 C58 122.6(8) . . ? C54 C4 C17 111.8(8) . . ? C58 C4 C17 121.9(8) . . ? C71 C5 C12 125.4(8) . . ? C71 C5 C31 121.7(8) . . ? C12 C5 C31 105.5(8) . . ? C71 C5 Ce2 95.6(5) . . ? C12 C5 Ce2 63.9(5) . . ? C31 C5 Ce2 81.5(5) . . ? C11 C6 C60 122.6(9) . . ? C11 C6 C42 107.8(9) . . ? C60 C6 C42 123.1(8) . . ? C11 C6 Ce2 68.2(5) . . ? C60 C6 Ce2 107.1(6) . . ? C42 C6 Ce2 67.2(5) . . ? C9 C7 C10 120.7(8) . . ? C9 C7 C17 125.6(9) . . ? C10 C7 C17 107.4(8) . . ? C33 C8 C54 117.5(8) . . ? C33 C8 C15 118.9(8) . . ? C54 C8 C15 116.5(9) . . ? C33 C8 Ce3 102.3(6) . . ? C54 C8 Ce3 88.8(6) . . ? C15 C8 Ce3 53.1(6) . . ? C7 C9 C44 120.2(9) . . ? C7 C9 C2 118.5(8) . . ? C44 C9 C2 116.2(8) . . ? C99 C80 H4 109.5 . . ? C99 C80 H5 109.5 . . ? H4 C80 H5 109.5 . . ? C99 C80 H6 109.5 . . ? H4 C80 H6 109.5 . . ? H5 C80 H6 109.5 . . ? C69 C10 C7 120.4(9) . . ? C69 C10 C54 117.0(9) . . ? C7 C10 C54 112.2(8) . . ? C69 C10 Ce3 58.0(6) . . ? C7 C10 Ce3 107.7(6) . . ? C54 C10 Ce3 75.3(6) . . ? C92 C81 C88 119.5(8) . . ? C92 C81 C86 118.1(8) . . ? C88 C81 C86 122.3(9) . . ? C6 C11 C47 118.2(10) . . ? C6 C11 C75 107.8(8) . . ? C47 C11 C75 125.8(9) . . ? C6 C11 Ce2 83.4(5) . . ? C47 C11 Ce2 94.8(6) . . ? C75 C11 Ce2 62.4(5) . . ? C57 C12 C14 122.9(8) . . ? C57 C12 C5 115.2(9) . . ? C14 C12 C5 106.7(8) . . ? C57 C12 Ce2 75.4(5) . . ? C14 C12 Ce2 72.4(5) . . ? C5 C12 Ce2 83.9(6) . . ? C52 C13 C36 122.7(9) . . ? C52 C13 C61 121.6(9) . . ? C36 C13 C61 107.5(8) . . ? C52 C13 Ce1 94.4(5) . . ? C36 C13 Ce1 62.6(4) . . ? C61 C13 Ce1 82.8(5) . . ? C109 C82 C96 121.3(13) . . ? C109 C82 C79 115.5(11) . . ? C96 C82 C79 123.2(10) . . ? C2 C14 C12 110.6(8) . . ? C2 C14 C64 117.6(9) . . ? C12 C14 C64 117.6(7) . . ? C2 C14 Ce2 85.8(5) . . ? C12 C14 Ce2 73.5(5) . . ? C64 C14 Ce2 73.1(5) . . ? C68 C15 C63 118.1(8) . . ? C68 C15 C8 119.4(9) . . ? C63 C15 C8 115.9(9) . . ? C68 C15 Ce3 67.9(7) . . ? C63 C15 Ce3 84.3(7) . . ? C8 C15 Ce3 92.8(7) . . ? C41 C16 C36 119.1(9) . . ? C41 C16 C22 106.9(9) . . ? C36 C16 C22 119.6(8) . . ? C41 C16 Ce1 88.0(6) . . ? C36 C16 Ce1 71.4(5) . . ? C22 C16 Ce1 73.4(5) . . ? C19 C17 C7 110.4(7) . . ? C19 C17 C4 108.1(7) . . ? C7 C17 C4 98.9(7) . . ? C19 C17 Si2 114.5(6) . . ? C7 C17 Si2 123.0(5) . . ? C4 C17 Si2 98.8(5) . . ? C73 C18 C32 116.6(8) . . ? C73 C18 C71 118.3(8) . . ? C32 C18 C71 117.9(9) . . ? C73 C18 Ce4 66.6(7) . . ? C32 C18 Ce4 85.1(7) . . ? C71 C18 Ce4 91.6(6) . . ? C89 C83 C102 119.2(10) . . ? C89 C83 C114 125.5(10) . . ? C102 C83 C114 115.3(12) . . ? C29 C19 C31 118.3(8) . . ? C29 C19 C17 122.7(8) . . ? C31 C19 C17 116.9(8) . . ? C3 C20 C32 111.6(9) . . ? C3 C20 C56 123.5(9) . . ? C32 C20 C56 118.3(9) . . ? C3 C20 Ce4 109.7(7) . . ? C32 C20 Ce4 68.0(6) . . ? C56 C20 Ce4 69.0(6) . . ? C3 C20 Ce2 68.2(5) . . ? C32 C20 Ce2 67.3(5) . . ? C56 C20 Ce2 108.1(5) . . ? Ce4 C20 Ce2 46.1(4) . . ? C87 C84 C105 120.6(8) . . ? C87 C84 C98 121.1(8) . . ? C105 C84 C98 118.4(9) . . ? C38 C21 C51 110.4(9) . . ? C38 C21 C60 118.7(9) . . ? C51 C21 C60 121.3(10) . . ? C63 C22 C43 117.8(8) . . ? C63 C22 C16 107.7(8) . . ? C43 C22 C16 119.2(9) . . ? C63 C22 Ce1 88.1(6) . . ? C43 C22 Ce1 70.7(5) . . ? C16 C22 Ce1 73.1(5) . . ? C61 C23 C34 110.4(9) . . ? C61 C23 C46 119.0(9) . . ? C34 C23 C46 123.0(8) . . ? C61 C23 Ce1 85.9(6) . . ? C34 C23 Ce1 65.1(5) . . ? C46 C23 Ce1 91.1(5) . . ? C70 C24 C30 119.7(7) . . ? C70 C24 C28 109.8(7) . . ? C30 C24 C28 122.5(8) . . ? C48 C25 C67 122.7(9) . . ? C48 C25 C39 122.9(9) . . ? C67 C25 C39 104.3(8) . . ? C71 C26 C70 121.6(7) . . ? C71 C26 C29 123.4(8) . . ? C70 C26 C29 106.2(8) . . ? C71 C26 Ce4 61.7(5) . . ? C70 C26 Ce4 74.6(5) . . ? C29 C26 Ce4 109.9(6) . . ? C72 C27 C65 121.4(9) . . ? C72 C27 C77 109.7(8) . . ? C65 C27 C77 119.5(9) . . ? C72 C27 Ce4 55.7(6) . . ? C65 C27 Ce4 102.4(7) . . ? C77 C27 Ce4 80.5(6) . . ? C58 C28 C24 111.8(7) . . ? C58 C28 C29 108.9(7) . . ? C24 C28 C29 99.0(6) . . ? C58 C28 Si1 114.8(5) . . ? C24 C28 Si1 120.2(6) . . ? C29 C28 Si1 99.2(5) . . ? C19 C29 C26 120.9(8) . . ? C19 C29 C28 123.0(8) . . ? C26 C29 C28 111.6(7) . . ? C106 C85 C88 119.0(8) . . ? C106 C85 C93 117.8(8) . . ? C88 C85 C93 123.2(9) . . ? C81 C86 H7 109.5 . . ? C81 C86 H8 109.5 . . ? H7 C86 H8 109.5 . . ? C81 C86 H9 109.5 . . ? H7 C86 H9 109.5 . . ? H8 C86 H9 109.5 . . ? C24 C30 C46 119.5(8) . . ? C24 C30 C1 118.5(8) . . ? C46 C30 C1 116.4(8) . . ? C19 C31 C2 126.6(8) . . ? C19 C31 C5 119.1(8) . . ? C2 C31 C5 109.5(8) . . ? C19 C31 Ce2 109.2(5) . . ? C2 C31 Ce2 68.8(4) . . ? C5 C31 Ce2 68.4(4) . . ? C18 C32 C20 122.4(9) . . ? C18 C32 C57 124.4(8) . . ? C20 C32 C57 105.5(9) . . ? C18 C32 Ce4 58.9(6) . . ? C20 C32 Ce4 78.3(6) . . ? C57 C32 Ce4 111.8(7) . . ? C18 C32 Ce2 93.4(5) . . ? C20 C32 Ce2 85.1(6) . . ? C57 C32 Ce2 62.3(5) . . ? Ce4 C32 Ce2 50.0(4) . . ? C62 C33 C8 119.8(9) . . ? C62 C33 C43 109.2(8) . . ? C8 C33 C43 122.8(8) . . ? C62 C33 Ce1 82.6(5) . . ? C8 C33 Ce1 94.8(5) . . ? C43 C33 Ce1 63.0(4) . . ? C23 C34 C74 119.7(8) . . ? C23 C34 C36 107.0(8) . . ? C74 C34 C36 115.2(9) . . ? C23 C34 Ce1 84.1(6) . . ? C74 C34 Ce1 70.9(5) . . ? C36 C34 Ce1 72.3(5) . . ? C40 C35 C41 123.9(9) . . ? C40 C35 C63 123.3(9) . . ? C41 C35 C63 105.2(9) . . ? C40 C35 Ce3 70.9(7) . . ? C41 C35 Ce3 106.1(7) . . ? C63 C35 Ce3 69.8(6) . . ? C84 C87 C97 117.4(8) . . ? C84 C87 Si1 129.1(6) . . ? C97 C87 Si1 113.3(7) . . ? C85 C88 C81 116.8(8) . . ? C85 C88 Si1 126.1(7) . . ? C81 C88 Si1 117.0(7) . . ? C16 C36 C13 118.2(9) . . ? C16 C36 C34 122.3(8) . . ? C13 C36 C34 106.5(9) . . ? C16 C36 Ce1 75.5(5) . . ? C13 C36 Ce1 86.3(5) . . ? C34 C36 Ce1 72.9(5) . . ? C39 C37 C45 109.6(9) . . ? C39 C37 C65 119.5(8) . . ? C45 C37 C65 121.2(9) . . ? C21 C38 C40 122.2(8) . . ? C21 C38 C59 107.9(9) . . ? C40 C38 C59 118.5(9) . . ? C83 C89 C100 123.6(9) . . ? C83 C89 H10 118.2 . . ? C100 C89 H10 118.2 . . ? C37 C39 C56 121.3(8) . . ? C37 C39 C25 109.6(8) . . ? C56 C39 C25 117.7(9) . . ? C35 C40 C38 118.2(9) . . ? C35 C40 C76 117.7(8) . . ? C38 C40 C76 117.4(9) . . ? C35 C40 Ce3 76.5(7) . . ? C38 C40 Ce3 105.2(7) . . ? C76 C40 Ce3 63.9(6) . . ? C16 C41 C53 123.3(9) . . ? C16 C41 C35 110.6(8) . . ? C53 C41 C35 119.2(10) . . ? C16 C41 Ce1 62.4(5) . . ? C53 C41 Ce1 93.7(6) . . ? C35 C41 Ce1 87.1(5) . . ? C108 C90 C97 123.0(8) . . ? C108 C90 H11 118.5 . . ? C97 C90 H11 118.5 . . ? C97 C91 H47 109.5 . . ? C97 C91 H48 109.5 . . ? H47 C91 H48 109.5 . . ? C97 C91 H49 109.5 . . ? H47 C91 H49 109.5 . . ? H48 C91 H49 109.5 . . ? C64 C42 C6 107.6(8) . . ? C64 C42 C44 123.5(8) . . ? C6 C42 C44 118.4(9) . . ? C64 C42 Ce2 62.8(5) . . ? C6 C42 Ce2 84.2(5) . . ? C44 C42 Ce2 90.0(6) . . ? C22 C43 C33 119.0(9) . . ? C22 C43 C74 122.0(8) . . ? C33 C43 C74 106.3(8) . . ? C22 C43 Ce1 76.7(5) . . ? C33 C43 Ce1 86.0(5) . . ? C74 C43 Ce1 72.3(5) . . ? C49 C44 C9 118.9(9) . . ? C49 C44 C42 116.4(8) . . ? C9 C44 C42 118.7(9) . . ? C52 C45 C37 123.1(8) . . ? C52 C45 C67 120.1(9) . . ? C37 C45 C67 106.8(8) . . ? C77 C46 C30 119.3(8) . . ? C77 C46 C23 116.0(8) . . ? C30 C46 C23 118.8(9) . . ? C51 C47 C11 117.8(9) . . ? C51 C47 C48 118.8(9) . . ? C11 C47 C48 116.3(9) . . ? C25 C48 C3 119.2(10) . . ? C25 C48 C47 118.3(9) . . ? C3 C48 C47 117.1(8) . . ? C44 C49 C69 122.0(8) . . ? C44 C49 C78 123.4(8) . . ? C69 C49 C78 105.9(9) . . ? C44 C49 Ce3 107.1(7) . . ? C69 C49 Ce3 61.0(6) . . ? C78 C49 Ce3 70.0(6) . . ? C70 C50 C77 119.1(8) . . ? C70 C50 C73 118.4(8) . . ? C77 C50 C73 110.8(7) . . ? C70 C50 Ce4 91.7(6) . . ? C77 C50 Ce4 89.9(7) . . ? C73 C50 Ce4 53.6(6) . . ? C47 C51 C21 122.9(8) . . ? C47 C51 C66 119.5(9) . . ? C21 C51 C66 107.2(9) . . ? C45 C52 C13 115.2(9) . . ? C45 C52 C53 120.0(9) . . ? C13 C52 C53 118.6(8) . . ? C59 C53 C41 116.5(9) . . ? C59 C53 C52 117.9(9) . . ? C41 C53 C52 117.6(9) . . ? C94 C92 C81 123.5(8) . . ? C94 C92 H15 118.2 . . ? C81 C92 H15 118.2 . . ? C4 C54 C10 106.3(8) . . ? C4 C54 C8 120.5(8) . . ? C10 C54 C8 124.8(8) . . ? C4 C54 Ce3 109.1(6) . . ? C10 C54 Ce3 76.8(6) . . ? C8 C54 Ce3 62.2(6) . . ? C75 C55 C57 120.9(8) . . ? C75 C55 C3 117.8(9) . . ? C57 C55 C3 106.4(9) . . ? C75 C55 Ce2 71.7(5) . . ? C57 C55 Ce2 73.4(5) . . ? C3 C55 Ce2 87.3(6) . . ? C72 C56 C39 117.6(9) . . ? C72 C56 C20 120.2(8) . . ? C39 C56 C20 116.0(9) . . ? C72 C56 Ce4 64.4(6) . . ? C39 C56 Ce4 106.6(7) . . ? C20 C56 Ce4 76.7(6) . . ? C85 C93 H16 109.5 . . ? C85 C93 H17 109.5 . . ? H16 C93 H17 109.5 . . ? C85 C93 H18 109.5 . . ? H16 C93 H18 109.5 . . ? H17 C93 H18 109.5 . . ? C12 C57 C32 118.8(8) . . ? C12 C57 C55 117.5(9) . . ? C32 C57 C55 109.6(8) . . ? C12 C57 Ce2 71.7(5) . . ? C32 C57 Ce2 87.5(6) . . ? C55 C57 Ce2 73.7(5) . . ? C106 C94 C92 116.4(9) . . ? C106 C94 C112 122.2(9) . . ? C92 C94 C112 121.4(9) . . ? C4 C58 C62 114.5(9) . . ? C4 C58 C28 122.1(8) . . ? C62 C58 C28 121.2(8) . . ? C53 C59 C66 121.5(9) . . ? C53 C59 C38 123.0(8) . . ? C66 C59 C38 105.8(9) . . ? Si2 C95 Si1 137.0(4) . . ? Si2 C95 H19 102.9 . . ? Si1 C95 H19 102.9 . . ? Si2 C95 H20 102.9 . . ? Si1 C95 H20 102.9 . . ? H19 C95 H20 105.1 . . ? C78 C60 C21 121.5(10) . . ? C78 C60 C6 116.7(8) . . ? C21 C60 C6 116.3(9) . . ? C23 C61 C65 124.6(9) . . ? C23 C61 C13 108.2(8) . . ? C65 C61 C13 120.1(9) . . ? C23 C61 Ce1 66.1(5) . . ? C65 C61 Ce1 107.3(5) . . ? C13 C61 Ce1 68.3(4) . . ? C33 C62 C58 124.3(9) . . ? C33 C62 C1 109.7(8) . . ? C58 C62 C1 121.1(8) . . ? C33 C62 Ce1 69.4(4) . . ? C58 C62 Ce1 109.1(5) . . ? C1 C62 Ce1 67.9(4) . . ? C22 C63 C15 125.1(9) . . ? C22 C63 C35 109.3(8) . . ? C15 C63 C35 117.4(10) . . ? C22 C63 Ce3 110.7(7) . . ? C15 C63 Ce3 59.6(6) . . ? C35 C63 Ce3 75.1(6) . . ? C22 C63 Ce1 62.4(5) . . ? C15 C63 Ce1 92.8(6) . . ? C35 C63 Ce1 86.4(5) . . ? Ce3 C63 Ce1 48.6(4) . . ? C75 C64 C42 109.0(8) . . ? C75 C64 C14 119.0(9) . . ? C42 C64 C14 117.7(8) . . ? C75 C64 Ce2 73.8(6) . . ? C42 C64 Ce2 86.2(6) . . ? C14 C64 Ce2 72.5(5) . . ? C99 C96 C82 117.7(10) . . ? C99 C96 Si2 125.8(8) . . ? C82 C96 Si2 116.5(10) . . ? C61 C65 C27 117.0(8) . . ? C61 C65 C37 117.7(9) . . ? C27 C65 C37 119.0(9) . . ? C90 C97 C87 118.7(9) . . ? C90 C97 C91 116.4(8) . . ? C87 C97 C91 125.0(8) . . ? C84 C98 H21 109.5 . . ? C84 C98 H22 109.5 . . ? H21 C98 H22 109.5 . . ? C84 C98 H23 109.5 . . ? H21 C98 H23 109.5 . . ? H22 C98 H23 109.5 . . ? C110 C99 C80 117.7(13) . . ? C110 C99 C96 119.6(11) . . ? C80 C99 C96 122.5(9) . . ? C67 C66 C51 122.5(9) . . ? C67 C66 C59 120.3(9) . . ? C51 C66 C59 108.7(8) . . ? C66 C67 C25 118.3(9) . . ? C66 C67 C45 120.3(9) . . ? C25 C67 C45 109.5(8) . . ? C15 C68 C76 121.7(8) . . ? C15 C68 C69 121.4(8) . . ? C76 C68 C69 106.9(9) . . ? C15 C68 Ce3 71.9(7) . . ? C76 C68 Ce3 76.6(6) . . ? C69 C68 Ce3 91.5(8) . . ? C89 C100 C111 118.7(11) . . ? C89 C100 C113 115.4(9) . . ? C111 C100 C113 125.8(10) . . ? C10 C69 C49 117.8(9) . . ? C10 C69 C68 120.8(9) . . ? C49 C69 C68 110.3(8) . . ? C10 C69 Ce3 93.5(7) . . ? C49 C69 Ce3 89.4(7) . . ? C68 C69 Ce3 53.8(6) . . ? C50 C70 C24 121.1(8) . . ? C50 C70 C26 118.9(8) . . ? C24 C70 C26 111.1(7) . . ? C50 C70 Ce4 58.8(6) . . ? C24 C70 Ce4 109.4(7) . . ? C26 C70 Ce4 76.4(6) . . ? C108 C101 H24 109.5 . . ? C108 C101 H25 109.5 . . ? H24 C101 H25 109.5 . . ? C108 C101 H26 109.5 . . ? H24 C101 H26 109.5 . . ? H25 C101 H26 109.5 . . ? C103 C102 C83 120.2(12) . . ? C103 C102 H27 119.9 . . ? C83 C102 H27 119.9 . . ? C102 C103 C111 120.3(9) . . ? C102 C103 C107 115.3(11) . . ? C111 C103 C107 124.4(9) . . ? C109 C104 C110 121.1(11) . . ? C109 C104 C115 123.4(12) . . ? C110 C104 C115 115.3(14) . . ? C108 C105 C84 124.1(10) . . ? C108 C105 H28 117.9 . . ? C84 C105 H28 117.9 . . ? C26 C71 C5 115.6(7) . . ? C26 C71 C18 120.1(8) . . ? C5 C71 C18 117.7(8) . . ? C26 C71 Ce4 89.3(6) . . ? C5 C71 Ce4 103.1(7) . . ? C18 C71 Ce4 54.0(5) . . ? C56 C72 C27 120.7(9) . . ? C56 C72 C73 118.0(9) . . ? C27 C72 C73 109.1(8) . . ? C56 C72 Ce4 81.1(7) . . ? C27 C72 Ce4 93.0(7) . . ? C73 C72 Ce4 60.8(6) . . ? C94 C106 C85 124.6(9) . . ? C94 C106 H29 117.7 . . ? C85 C106 H29 117.7 . . ? C103 C107 H30 109.5 . . ? C103 C107 H31 109.5 . . ? H30 C107 H31 109.5 . . ? C103 C107 H32 109.5 . . ? H30 C107 H32 109.5 . . ? H31 C107 H32 109.5 . . ? C18 C73 C50 122.6(7) . . ? C18 C73 C72 123.5(9) . . ? C50 C73 C72 104.9(8) . . ? C18 C73 Ce4 73.0(7) . . ? C50 C73 Ce4 90.0(7) . . ? C72 C73 Ce4 78.6(7) . . ? C43 C74 C1 109.4(8) . . ? C43 C74 C34 121.5(8) . . ? C1 C74 C34 115.2(9) . . ? C43 C74 Ce1 73.8(5) . . ? C1 C74 Ce1 85.2(6) . . ? C34 C74 Ce1 74.4(5) . . ? C105 C108 C90 116.1(9) . . ? C105 C108 C101 124.0(10) . . ? C90 C108 C101 119.9(9) . . ? C82 C109 C104 119.1(12) . . ? C82 C109 H33 120.4 . . ? C104 C109 H33 120.4 . . ? C99 C110 C104 121.0(14) . . ? C99 C110 H34 119.5 . . ? C104 C110 H34 119.5 . . ? C100 C111 C103 118.0(9) . . ? C100 C111 Si2 116.1(9) . . ? C103 C111 Si2 125.7(7) . . ? C55 C75 C64 122.0(9) . . ? C55 C75 C11 117.5(9) . . ? C64 C75 C11 107.8(9) . . ? C55 C75 Ce2 75.5(6) . . ? C64 C75 Ce2 73.0(5) . . ? C11 C75 Ce2 86.5(6) . . ? C40 C76 C68 120.8(10) . . ? C40 C76 C78 121.3(8) . . ? C68 C76 C78 109.1(8) . . ? C40 C76 Ce3 80.6(7) . . ? C68 C76 Ce3 64.4(6) . . ? C78 C76 Ce3 96.2(8) . . ? C94 C112 H35 109.5 . . ? C94 C112 H36 109.5 . . ? H35 C112 H36 109.5 . . ? C94 C112 H37 109.5 . . ? H35 C112 H37 109.5 . . ? H36 C112 H37 109.5 . . ? C46 C77 C50 121.0(7) . . ? C46 C77 C27 122.5(9) . . ? C50 C77 C27 105.3(8) . . ? C46 C77 Ce4 105.8(7) . . ? C50 C77 Ce4 59.8(6) . . ? C27 C77 Ce4 68.8(6) . . ? C60 C78 C76 118.2(9) . . ? C60 C78 C49 120.1(9) . . ? C76 C78 C49 107.5(8) . . ? C60 C78 Ce3 98.4(7) . . ? C76 C78 Ce3 52.5(7) . . ? C49 C78 Ce3 79.9(6) . . ? C100 C113 H38 109.5 . . ? C100 C113 H39 109.5 . . ? H38 C113 H39 109.5 . . ? C100 C113 H40 109.5 . . ? H38 C113 H40 109.5 . . ? H39 C113 H40 109.5 . . ? C83 C114 H41 109.5 . . ? C83 C114 H42 109.5 . . ? H41 C114 H42 109.5 . . ? C83 C114 H43 109.5 . . ? H41 C114 H43 109.5 . . ? H42 C114 H43 109.5 . . ? C104 C115 H44 109.5 . . ? C104 C115 H45 109.5 . . ? H44 C115 H45 109.5 . . ? C104 C115 H46 109.5 . . ? H44 C115 H46 109.5 . . ? H45 C115 H46 109.5 . . ? S1 C116 S2 173.9(12) . . ? S3 C117 S4 172.0(18) . . ? C68 Ce3 C15 40.2(5) . . ? C68 Ce3 C76 39.0(5) . . ? C15 Ce3 C76 70.7(7) . . ? C68 Ce3 C63 66.1(7) . . ? C15 Ce3 C63 36.2(5) . . ? C76 Ce3 C63 76.2(7) . . ? C68 Ce3 C40 66.8(6) . . ? C15 Ce3 C40 79.7(7) . . ? C76 Ce3 C40 35.5(4) . . ? C63 Ce3 C40 62.7(6) . . ? C68 Ce3 C35 75.5(7) . . ? C15 Ce3 C35 65.1(6) . . ? C76 Ce3 C35 61.1(6) . . ? C63 Ce3 C35 35.0(4) . . ? C40 Ce3 C35 32.6(4) . . ? C68 Ce3 C69 34.7(4) . . ? C15 Ce3 C69 64.6(6) . . ? C76 Ce3 C69 57.7(5) . . ? C63 Ce3 C69 98.0(7) . . ? C40 Ce3 C69 92.9(7) . . ? C35 Ce3 C69 109.6(8) . . ? C68 Ce3 C8 63.4(5) . . ? C15 Ce3 C8 34.1(4) . . ? C76 Ce3 C8 101.0(7) . . ? C63 Ce3 C8 58.4(5) . . ? C40 Ce3 C8 113.5(8) . . ? C35 Ce3 C8 93.1(7) . . ? C69 Ce3 C8 68.5(5) . . ? C68 Ce3 C78 55.8(5) . . ? C15 Ce3 C78 95.2(7) . . ? C76 Ce3 C78 31.3(4) . . ? C63 Ce3 C78 107.4(7) . . ? C40 Ce3 C78 57.2(5) . . ? C35 Ce3 C78 88.6(6) . . ? C69 Ce3 C78 51.7(4) . . ? C8 Ce3 C78 116.5(6) . . ? C68 Ce3 C49 53.7(5) . . ? C15 Ce3 C49 91.4(7) . . ? C76 Ce3 C49 52.9(5) . . ? C63 Ce3 C49 119.2(7) . . ? C40 Ce3 C49 85.6(6) . . ? C35 Ce3 C49 114.1(7) . . ? C69 Ce3 C49 29.5(3) . . ? C8 Ce3 C49 97.7(5) . . ? C78 Ce3 C49 30.2(3) . . ? C68 Ce3 C54 65.4(5) . . ? C15 Ce3 C54 55.4(4) . . ? C76 Ce3 C54 103.3(6) . . ? C63 Ce3 C54 86.4(6) . . ? C40 Ce3 C54 130.5(7) . . ? C35 Ce3 C54 119.9(7) . . ? C69 Ce3 C54 51.9(4) . . ? C8 Ce3 C54 29.0(3) . . ? C78 Ce3 C54 103.5(6) . . ? C49 Ce3 C54 76.8(4) . . ? C68 Ce3 C10 55.8(5) . . ? C15 Ce3 C10 67.5(5) . . ? C76 Ce3 C10 86.0(6) . . ? C63 Ce3 C10 103.5(6) . . ? C40 Ce3 C10 120.5(7) . . ? C35 Ce3 C10 128.8(7) . . ? C69 Ce3 C10 28.5(3) . . ? C8 Ce3 C10 53.6(4) . . ? C78 Ce3 C10 77.3(5) . . ? C49 Ce3 C10 49.1(4) . . ? C54 Ce3 C10 27.9(3) . . ? C73 Ce4 C18 40.4(5) . . ? C73 Ce4 C72 40.6(5) . . ? C18 Ce4 C72 72.3(6) . . ? C73 Ce4 C32 65.5(6) . . ? C18 Ce4 C32 36.0(4) . . ? C72 Ce4 C32 76.1(6) . . ? C73 Ce4 C56 66.9(5) . . ? C18 Ce4 C56 79.9(6) . . ? C72 Ce4 C56 34.5(4) . . ? C32 Ce4 C56 62.2(5) . . ? C73 Ce4 C50 36.3(5) . . ? C18 Ce4 C50 66.6(6) . . ? C72 Ce4 C50 59.3(5) . . ? C32 Ce4 C50 99.5(7) . . ? C56 Ce4 C50 93.4(6) . . ? C73 Ce4 C20 76.5(6) . . ? C18 Ce4 C20 65.1(5) . . ? C72 Ce4 C20 62.5(5) . . ? C32 Ce4 C20 33.8(4) . . ? C56 Ce4 C20 34.3(4) . . ? C50 Ce4 C20 112.1(7) . . ? C73 Ce4 C71 63.7(6) . . ? C18 Ce4 C71 34.4(4) . . ? C72 Ce4 C71 102.9(7) . . ? C32 Ce4 C71 59.2(5) . . ? C56 Ce4 C71 114.1(7) . . ? C50 Ce4 C71 69.8(5) . . ? C20 Ce4 C71 92.9(6) . . ? C73 Ce4 C27 57.8(5) . . ? C18 Ce4 C27 97.3(7) . . ? C72 Ce4 C27 31.3(4) . . ? C32 Ce4 C27 107.4(6) . . ? C56 Ce4 C27 56.3(4) . . ? C50 Ce4 C27 53.1(4) . . ? C20 Ce4 C27 89.8(5) . . ? C71 Ce4 C27 118.9(8) . . ? C73 Ce4 C77 55.7(6) . . ? C18 Ce4 C77 93.7(7) . . ? C72 Ce4 C77 53.5(5) . . ? C32 Ce4 C77 120.3(7) . . ? C56 Ce4 C77 85.2(6) . . ? C50 Ce4 C77 30.3(3) . . ? C20 Ce4 C77 116.0(6) . . ? C71 Ce4 C77 99.7(6) . . ? C27 Ce4 C77 30.7(3) . . ? C73 Ce4 C70 57.7(5) . . ? C18 Ce4 C70 69.3(6) . . ? C72 Ce4 C70 88.5(6) . . ? C32 Ce4 C70 105.1(7) . . ? C56 Ce4 C70 122.0(7) . . ? C50 Ce4 C70 29.5(3) . . ? C20 Ce4 C70 131.3(7) . . ? C71 Ce4 C70 54.2(4) . . ? C27 Ce4 C70 79.8(5) . . ? C77 Ce4 C70 50.9(4) . . ? C73 Ce4 C26 67.4(6) . . ? C18 Ce4 C26 56.6(5) . . ? C72 Ce4 C26 106.7(7) . . ? C32 Ce4 C26 87.5(6) . . ? C56 Ce4 C26 132.4(8) . . ? C50 Ce4 C26 54.1(4) . . ? C20 Ce4 C26 120.6(6) . . ? C71 Ce4 C26 29.0(3) . . ? C27 Ce4 C26 107.1(6) . . ? C77 Ce4 C26 79.7(5) . . ? C70 Ce4 C26 29.0(3) . . ? S6 C118 S5 171(3) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C43 Ce1 C1 C74 -40.2(6) . . . . ? C36 Ce1 C1 C74 26.0(6) . . . . ? C34 Ce1 C1 C74 37.4(6) . . . . ? C16 Ce1 C1 C74 -4.5(6) . . . . ? C22 Ce1 C1 C74 -33.7(6) . . . . ? C23 Ce1 C1 C74 73.0(6) . . . . ? C33 Ce1 C1 C74 -80.0(6) . . . . ? C13 Ce1 C1 C74 52.1(6) . . . . ? C41 Ce1 C1 C74 -11.3(7) . . . . ? C63 Ce1 C1 C74 -56.4(6) . . . . ? C74 Ce1 C1 C62 111.2(8) . . . . ? C43 Ce1 C1 C62 70.9(6) . . . . ? C36 Ce1 C1 C62 137.2(6) . . . . ? C34 Ce1 C1 C62 148.6(7) . . . . ? C16 Ce1 C1 C62 106.6(6) . . . . ? C22 Ce1 C1 C62 77.5(6) . . . . ? C23 Ce1 C1 C62 -175.8(6) . . . . ? C33 Ce1 C1 C62 31.2(5) . . . . ? C13 Ce1 C1 C62 163.3(5) . . . . ? C41 Ce1 C1 C62 99.9(6) . . . . ? C63 Ce1 C1 C62 54.7(6) . . . . ? C74 Ce1 C1 C30 -130.0(8) . . . . ? C43 Ce1 C1 C30 -170.2(7) . . . . ? C36 Ce1 C1 C30 -104.0(6) . . . . ? C34 Ce1 C1 C30 -92.6(6) . . . . ? C16 Ce1 C1 C30 -134.5(5) . . . . ? C22 Ce1 C1 C30 -163.6(6) . . . . ? C23 Ce1 C1 C30 -56.9(5) . . . . ? C33 Ce1 C1 C30 150.0(7) . . . . ? C13 Ce1 C1 C30 -77.9(6) . . . . ? C41 Ce1 C1 C30 -141.3(5) . . . . ? C63 Ce1 C1 C30 173.6(5) . . . . ? C64 Ce2 C2 C14 36.1(6) . . . . ? C12 Ce2 C2 C14 -40.2(6) . . . . ? C75 Ce2 C2 C14 25.6(6) . . . . ? C57 Ce2 C2 C14 -33.8(6) . . . . ? C55 Ce2 C2 C14 -4.5(7) . . . . ? C5 Ce2 C2 C14 -81.3(6) . . . . ? C42 Ce2 C2 C14 72.4(6) . . . . ? C11 Ce2 C2 C14 51.3(7) . . . . ? C32 Ce2 C2 C14 -56.9(6) . . . . ? C3 Ce2 C2 C14 -10.0(8) . . . . ? C14 Ce2 C2 C31 114.1(8) . . . . ? C64 Ce2 C2 C31 150.2(7) . . . . ? C12 Ce2 C2 C31 73.9(6) . . . . ? C75 Ce2 C2 C31 139.6(6) . . . . ? C57 Ce2 C2 C31 80.3(6) . . . . ? C55 Ce2 C2 C31 109.6(6) . . . . ? C5 Ce2 C2 C31 32.8(5) . . . . ? C42 Ce2 C2 C31 -173.5(6) . . . . ? C11 Ce2 C2 C31 165.4(5) . . . . ? C32 Ce2 C2 C31 57.1(6) . . . . ? C3 Ce2 C2 C31 104.1(6) . . . . ? C14 Ce2 C2 C9 -130.5(9) . . . . ? C64 Ce2 C2 C9 -94.4(6) . . . . ? C12 Ce2 C2 C9 -170.7(7) . . . . ? C75 Ce2 C2 C9 -104.9(6) . . . . ? C57 Ce2 C2 C9 -164.3(6) . . . . ? C55 Ce2 C2 C9 -135.0(5) . . . . ? C5 Ce2 C2 C9 148.2(7) . . . . ? C42 Ce2 C2 C9 -58.1(5) . . . . ? C11 Ce2 C2 C9 -79.2(6) . . . . ? C32 Ce2 C2 C9 172.6(5) . . . . ? C3 Ce2 C2 C9 -140.5(5) . . . . ? C14 Ce2 C3 C20 -106.3(6) . . . . ? C64 Ce2 C3 C20 -137.8(6) . . . . ? C12 Ce2 C3 C20 -77.2(6) . . . . ? C75 Ce2 C3 C20 -146.7(7) . . . . ? C57 Ce2 C3 C20 -69.8(6) . . . . ? C55 Ce2 C3 C20 -111.7(9) . . . . ? C5 Ce2 C3 C20 -52.0(6) . . . . ? C2 Ce2 C3 C20 -101.2(6) . . . . ? C42 Ce2 C3 C20 -163.7(6) . . . . ? C11 Ce2 C3 C20 176.1(7) . . . . ? C32 Ce2 C3 C20 -29.9(6) . . . . ? C14 Ce2 C3 C48 134.3(6) . . . . ? C64 Ce2 C3 C48 102.8(7) . . . . ? C12 Ce2 C3 C48 163.4(7) . . . . ? C75 Ce2 C3 C48 93.9(7) . . . . ? C57 Ce2 C3 C48 170.8(8) . . . . ? C55 Ce2 C3 C48 128.9(9) . . . . ? C5 Ce2 C3 C48 -171.4(6) . . . . ? C2 Ce2 C3 C48 139.5(6) . . . . ? C42 Ce2 C3 C48 76.9(7) . . . . ? C11 Ce2 C3 C48 56.7(6) . . . . ? C32 Ce2 C3 C48 -149.3(8) . . . . ? C14 Ce2 C3 C55 5.4(7) . . . . ? C64 Ce2 C3 C55 -26.0(6) . . . . ? C12 Ce2 C3 C55 34.5(6) . . . . ? C75 Ce2 C3 C55 -34.9(6) . . . . ? C57 Ce2 C3 C55 41.9(6) . . . . ? C5 Ce2 C3 C55 59.8(6) . . . . ? C2 Ce2 C3 C55 10.6(8) . . . . ? C42 Ce2 C3 C55 -52.0(7) . . . . ? C11 Ce2 C3 C55 -72.2(6) . . . . ? C32 Ce2 C3 C55 81.8(7) . . . . ? C14 Ce2 C5 C71 168.1(7) . . . . ? C64 Ce2 C5 C71 159.9(6) . . . . ? C12 Ce2 C5 C71 126.8(8) . . . . ? C75 Ce2 C5 C71 130.0(6) . . . . ? C57 Ce2 C5 C71 91.0(6) . . . . ? C55 Ce2 C5 C71 100.6(6) . . . . ? C2 Ce2 C5 C71 -152.8(7) . . . . ? C42 Ce2 C5 C71 -176.6(5) . . . . ? C11 Ce2 C5 C71 133.3(5) . . . . ? C32 Ce2 C5 C71 55.0(5) . . . . ? C3 Ce2 C5 C71 74.2(6) . . . . ? C14 Ce2 C5 C12 41.3(5) . . . . ? C64 Ce2 C5 C12 33.1(6) . . . . ? C75 Ce2 C5 C12 3.2(6) . . . . ? C57 Ce2 C5 C12 -35.9(6) . . . . ? C55 Ce2 C5 C12 -26.3(6) . . . . ? C2 Ce2 C5 C12 80.4(6) . . . . ? C42 Ce2 C5 C12 56.5(6) . . . . ? C11 Ce2 C5 C12 6.4(7) . . . . ? C32 Ce2 C5 C12 -71.8(6) . . . . ? C3 Ce2 C5 C12 -52.7(6) . . . . ? C14 Ce2 C5 C31 -70.6(6) . . . . ? C64 Ce2 C5 C31 -78.8(6) . . . . ? C12 Ce2 C5 C31 -111.9(8) . . . . ? C75 Ce2 C5 C31 -108.7(6) . . . . ? C57 Ce2 C5 C31 -147.8(7) . . . . ? C55 Ce2 C5 C31 -138.2(6) . . . . ? C2 Ce2 C5 C31 -31.5(5) . . . . ? C42 Ce2 C5 C31 -55.3(6) . . . . ? C11 Ce2 C5 C31 -105.5(6) . . . . ? C32 Ce2 C5 C31 176.3(7) . . . . ? C3 Ce2 C5 C31 -164.6(5) . . . . ? C14 Ce2 C6 C11 -96.2(6) . . . . ? C64 Ce2 C6 C11 -82.9(7) . . . . ? C12 Ce2 C6 C11 -76.0(6) . . . . ? C75 Ce2 C6 C11 -38.6(6) . . . . ? C57 Ce2 C6 C11 -41.2(7) . . . . ? C55 Ce2 C6 C11 -24.9(6) . . . . ? C5 Ce2 C6 C11 -99.8(6) . . . . ? C2 Ce2 C6 C11 -126.1(6) . . . . ? C42 Ce2 C6 C11 -121.7(9) . . . . ? C32 Ce2 C6 C11 -17.0(8) . . . . ? C3 Ce2 C6 C11 5.4(6) . . . . ? C14 Ce2 C6 C60 144.8(6) . . . . ? C64 Ce2 C6 C60 158.1(7) . . . . ? C12 Ce2 C6 C60 165.0(5) . . . . ? C75 Ce2 C6 C60 -157.5(7) . . . . ? C57 Ce2 C6 C60 -160.1(5) . . . . ? C55 Ce2 C6 C60 -143.9(6) . . . . ? C5 Ce2 C6 C60 141.2(5) . . . . ? C2 Ce2 C6 C60 115.0(6) . . . . ? C42 Ce2 C6 C60 119.3(9) . . . . ? C11 Ce2 C6 C60 -119.0(9) . . . . ? C32 Ce2 C6 C60 -136.0(5) . . . . ? C3 Ce2 C6 C60 -113.6(6) . . . . ? C14 Ce2 C6 C42 25.5(6) . . . . ? C64 Ce2 C6 C42 38.8(6) . . . . ? C12 Ce2 C6 C42 45.7(7) . . . . ? C75 Ce2 C6 C42 83.1(7) . . . . ? C57 Ce2 C6 C42 80.5(6) . . . . ? C55 Ce2 C6 C42 96.8(6) . . . . ? C5 Ce2 C6 C42 21.9(7) . . . . ? C2 Ce2 C6 C42 -4.4(6) . . . . ? C11 Ce2 C6 C42 121.7(9) . . . . ? C32 Ce2 C6 C42 104.7(6) . . . . ? C3 Ce2 C6 C42 127.1(6) . . . . ? C10 C7 C9 C44 -4.4(12) . . . . ? C17 C7 C9 C44 -152.9(8) . . . . ? C10 C7 C9 C2 149.3(8) . . . . ? C17 C7 C9 C2 0.8(12) . . . . ? C14 C2 C9 C7 -156.7(8) . . . . ? C31 C2 C9 C7 -16.7(10) . . . . ? Ce2 C2 C9 C7 -99.0(7) . . . . ? C14 C2 C9 C44 -2.0(13) . . . . ? C31 C2 C9 C44 138.0(8) . . . . ? Ce2 C2 C9 C44 55.7(8) . . . . ? C9 C7 C10 C69 4.2(13) . . . . ? C17 C7 C10 C69 157.8(7) . . . . ? C9 C7 C10 C54 -139.5(8) . . . . ? C17 C7 C10 C54 14.1(8) . . . . ? C9 C7 C10 Ce3 -58.6(10) . . . . ? C17 C7 C10 Ce3 95.1(7) . . . . ? C60 C6 C11 C47 5.0(14) . . . . ? C42 C6 C11 C47 -147.4(9) . . . . ? Ce2 C6 C11 C47 -91.9(8) . . . . ? C60 C6 C11 C75 155.2(9) . . . . ? C42 C6 C11 C75 2.8(11) . . . . ? Ce2 C6 C11 C75 58.2(6) . . . . ? C60 C6 C11 Ce2 96.9(9) . . . . ? C42 C6 C11 Ce2 -55.4(7) . . . . ? C14 Ce2 C11 C6 80.5(6) . . . . ? C64 Ce2 C11 C6 73.0(6) . . . . ? C12 Ce2 C11 C6 111.2(6) . . . . ? C75 Ce2 C11 C6 114.0(9) . . . . ? C57 Ce2 C11 C6 141.3(6) . . . . ? C55 Ce2 C11 C6 149.3(7) . . . . ? C5 Ce2 C11 C6 107.8(6) . . . . ? C2 Ce2 C11 C6 56.9(7) . . . . ? C42 Ce2 C11 C6 32.5(6) . . . . ? C32 Ce2 C11 C6 166.8(6) . . . . ? C3 Ce2 C11 C6 -173.7(7) . . . . ? C14 Ce2 C11 C47 -161.7(7) . . . . ? C64 Ce2 C11 C47 -169.2(8) . . . . ? C12 Ce2 C11 C47 -130.9(7) . . . . ? C75 Ce2 C11 C47 -128.2(9) . . . . ? C57 Ce2 C11 C47 -100.9(7) . . . . ? C55 Ce2 C11 C47 -92.8(7) . . . . ? C5 Ce2 C11 C47 -134.4(6) . . . . ? C2 Ce2 C11 C47 174.8(6) . . . . ? C42 Ce2 C11 C47 150.4(8) . . . . ? C32 Ce2 C11 C47 -75.4(7) . . . . ? C3 Ce2 C11 C47 -55.8(6) . . . . ? C14 Ce2 C11 C75 -33.5(6) . . . . ? C64 Ce2 C11 C75 -41.0(6) . . . . ? C12 Ce2 C11 C75 -2.8(6) . . . . ? C57 Ce2 C11 C75 27.3(6) . . . . ? C55 Ce2 C11 C75 35.3(6) . . . . ? C5 Ce2 C11 C75 -6.2(7) . . . . ? C2 Ce2 C11 C75 -57.1(6) . . . . ? C42 Ce2 C11 C75 -81.5(6) . . . . ? C32 Ce2 C11 C75 52.8(6) . . . . ? C3 Ce2 C11 C75 72.3(6) . . . . ? C71 C5 C12 C57 -6.9(14) . . . . ? C31 C5 C12 C57 142.9(8) . . . . ? Ce2 C5 C12 C57 70.7(7) . . . . ? C71 C5 C12 C14 -147.1(9) . . . . ? C31 C5 C12 C14 2.7(9) . . . . ? Ce2 C5 C12 C14 -69.5(6) . . . . ? C71 C5 C12 Ce2 -77.6(10) . . . . ? C31 C5 C12 Ce2 72.2(6) . . . . ? C14 Ce2 C12 C57 132.2(8) . . . . ? C64 Ce2 C12 C57 100.7(6) . . . . ? C75 Ce2 C12 C57 65.2(6) . . . . ? C55 Ce2 C12 C57 30.6(6) . . . . ? C5 Ce2 C12 C57 -118.1(9) . . . . ? C2 Ce2 C12 C57 168.2(7) . . . . ? C42 Ce2 C12 C57 114.8(6) . . . . ? C11 Ce2 C12 C57 66.7(6) . . . . ? C32 Ce2 C12 C57 -31.8(6) . . . . ? C3 Ce2 C12 C57 10.6(6) . . . . ? C64 Ce2 C12 C14 -31.5(5) . . . . ? C75 Ce2 C12 C14 -67.0(5) . . . . ? C57 Ce2 C12 C14 -132.2(8) . . . . ? C55 Ce2 C12 C14 -101.6(6) . . . . ? C5 Ce2 C12 C14 109.7(7) . . . . ? C2 Ce2 C12 C14 36.0(5) . . . . ? C42 Ce2 C12 C14 -17.4(5) . . . . ? C11 Ce2 C12 C14 -65.5(5) . . . . ? C32 Ce2 C12 C14 -164.0(6) . . . . ? C3 Ce2 C12 C14 -121.6(5) . . . . ? C14 Ce2 C12 C5 -109.7(7) . . . . ? C64 Ce2 C12 C5 -141.2(6) . . . . ? C75 Ce2 C12 C5 -176.7(6) . . . . ? C57 Ce2 C12 C5 118.1(9) . . . . ? C55 Ce2 C12 C5 148.7(7) . . . . ? C2 Ce2 C12 C5 -73.7(5) . . . . ? C42 Ce2 C12 C5 -127.1(6) . . . . ? C11 Ce2 C12 C5 -175.2(5) . . . . ? C32 Ce2 C12 C5 86.3(6) . . . . ? C3 Ce2 C12 C5 128.7(6) . . . . ? C74 Ce1 C13 C52 -158.7(7) . . . . ? C43 Ce1 C13 C52 -128.4(6) . . . . ? C36 Ce1 C13 C52 -124.7(10) . . . . ? C34 Ce1 C13 C52 -167.9(8) . . . . ? C16 Ce1 C13 C52 -89.5(7) . . . . ? C22 Ce1 C13 C52 -98.8(6) . . . . ? C1 Ce1 C13 C52 176.8(6) . . . . ? C23 Ce1 C13 C52 152.4(8) . . . . ? C33 Ce1 C13 C52 -133.1(6) . . . . ? C41 Ce1 C13 C52 -54.4(6) . . . . ? C63 Ce1 C13 C52 -73.8(6) . . . . ? C74 Ce1 C13 C36 -34.0(6) . . . . ? C43 Ce1 C13 C36 -3.6(7) . . . . ? C34 Ce1 C13 C36 -43.1(6) . . . . ? C16 Ce1 C13 C36 35.2(6) . . . . ? C22 Ce1 C13 C36 25.9(6) . . . . ? C1 Ce1 C13 C36 -58.5(7) . . . . ? C23 Ce1 C13 C36 -82.9(7) . . . . ? C33 Ce1 C13 C36 -8.4(8) . . . . ? C41 Ce1 C13 C36 70.3(6) . . . . ? C63 Ce1 C13 C36 50.9(7) . . . . ? C74 Ce1 C13 C61 80.0(6) . . . . ? C43 Ce1 C13 C61 110.3(6) . . . . ? C36 Ce1 C13 C61 114.0(9) . . . . ? C34 Ce1 C13 C61 70.8(6) . . . . ? C16 Ce1 C13 C61 149.2(7) . . . . ? C22 Ce1 C13 C61 139.9(6) . . . . ? C1 Ce1 C13 C61 55.5(6) . . . . ? C23 Ce1 C13 C61 31.1(5) . . . . ? C33 Ce1 C13 C61 105.6(6) . . . . ? C41 Ce1 C13 C61 -175.7(7) . . . . ? C63 Ce1 C13 C61 164.9(5) . . . . ? C31 C2 C14 C12 -1.1(10) . . . . ? C9 C2 C14 C12 141.3(9) . . . . ? Ce2 C2 C14 C12 70.6(6) . . . . ? C31 C2 C14 C64 -140.1(8) . . . . ? C9 C2 C14 C64 2.3(13) . . . . ? Ce2 C2 C14 C64 -68.4(7) . . . . ? C31 C2 C14 Ce2 -71.7(6) . . . . ? C9 C2 C14 Ce2 70.7(9) . . . . ? C57 C12 C14 C2 -137.5(9) . . . . ? C5 C12 C14 C2 -1.1(10) . . . . ? Ce2 C12 C14 C2 -78.8(6) . . . . ? C57 C12 C14 C64 1.5(14) . . . . ? C5 C12 C14 C64 137.9(8) . . . . ? Ce2 C12 C14 C64 60.1(8) . . . . ? C57 C12 C14 Ce2 -58.6(9) . . . . ? C5 C12 C14 Ce2 77.8(6) . . . . ? C64 Ce2 C14 C2 -120.5(9) . . . . ? C12 Ce2 C14 C2 112.9(8) . . . . ? C75 Ce2 C14 C2 -150.2(7) . . . . ? C57 Ce2 C14 C2 140.5(7) . . . . ? C55 Ce2 C14 C2 175.3(7) . . . . ? C5 Ce2 C14 C2 74.1(6) . . . . ? C42 Ce2 C14 C2 -88.2(6) . . . . ? C11 Ce2 C14 C2 -131.0(6) . . . . ? C32 Ce2 C14 C2 125.9(6) . . . . ? C3 Ce2 C14 C2 172.4(6) . . . . ? C64 Ce2 C14 C12 126.6(8) . . . . ? C75 Ce2 C14 C12 96.9(6) . . . . ? C57 Ce2 C14 C12 27.5(5) . . . . ? C55 Ce2 C14 C12 62.4(5) . . . . ? C5 Ce2 C14 C12 -38.8(5) . . . . ? C2 Ce2 C14 C12 -112.9(8) . . . . ? C42 Ce2 C14 C12 158.8(6) . . . . ? C11 Ce2 C14 C12 116.1(5) . . . . ? C32 Ce2 C14 C12 13.0(5) . . . . ? C3 Ce2 C14 C12 59.4(5) . . . . ? C12 Ce2 C14 C64 -126.6(8) . . . . ? C75 Ce2 C14 C64 -29.7(6) . . . . ? C57 Ce2 C14 C64 -99.0(6) . . . . ? C55 Ce2 C14 C64 -64.2(6) . . . . ? C5 Ce2 C14 C64 -165.4(7) . . . . ? C2 Ce2 C14 C64 120.5(9) . . . . ? C42 Ce2 C14 C64 32.3(5) . . . . ? C11 Ce2 C14 C64 -10.5(6) . . . . ? C32 Ce2 C14 C64 -113.6(6) . . . . ? C3 Ce2 C14 C64 -67.1(6) . . . . ? C33 C8 C15 C68 149.8(8) . . . . ? C54 C8 C15 C68 0.0(12) . . . . ? Ce3 C8 C15 C68 66.1(8) . . . . ? C33 C8 C15 C63 -1.3(13) . . . . ? C54 C8 C15 C63 -151.1(8) . . . . ? Ce3 C8 C15 C63 -85.0(9) . . . . ? C33 C8 C15 Ce3 83.7(10) . . . . ? C54 C8 C15 Ce3 -66.1(9) . . . . ? C74 Ce1 C16 C41 -172.2(6) . . . . ? C43 Ce1 C16 C41 -136.8(7) . . . . ? C36 Ce1 C16 C41 121.7(8) . . . . ? C34 Ce1 C16 C41 151.1(7) . . . . ? C22 Ce1 C16 C41 -108.3(9) . . . . ? C1 Ce1 C16 C41 -169.7(5) . . . . ? C23 Ce1 C16 C41 131.0(6) . . . . ? C33 Ce1 C16 C41 -122.0(6) . . . . ? C13 Ce1 C16 C41 88.7(6) . . . . ? C63 Ce1 C16 C41 -71.2(6) . . . . ? C74 Ce1 C16 C36 66.1(5) . . . . ? C43 Ce1 C16 C36 101.5(6) . . . . ? C34 Ce1 C16 C36 29.4(5) . . . . ? C22 Ce1 C16 C36 130.1(8) . . . . ? C1 Ce1 C16 C36 68.6(5) . . . . ? C23 Ce1 C16 C36 9.4(5) . . . . ? C33 Ce1 C16 C36 116.4(5) . . . . ? C13 Ce1 C16 C36 -33.0(5) . . . . ? C41 Ce1 C16 C36 -121.7(8) . . . . ? C63 Ce1 C16 C36 167.1(7) . . . . ? C74 Ce1 C16 C22 -64.0(6) . . . . ? C43 Ce1 C16 C22 -28.5(6) . . . . ? C36 Ce1 C16 C22 -130.1(8) . . . . ? C34 Ce1 C16 C22 -100.6(6) . . . . ? C1 Ce1 C16 C22 -61.4(6) . . . . ? C23 Ce1 C16 C22 -120.7(6) . . . . ? C33 Ce1 C16 C22 -13.7(6) . . . . ? C13 Ce1 C16 C22 -163.0(7) . . . . ? C41 Ce1 C16 C22 108.3(9) . . . . ? C63 Ce1 C16 C22 37.0(5) . . . . ? C9 C7 C17 C19 20.9(11) . . . . ? C10 C7 C17 C19 -131.0(7) . . . . ? C9 C7 C17 C4 134.1(8) . . . . ? C10 C7 C17 C4 -17.8(8) . . . . ? C9 C7 C17 Si2 -119.3(8) . . . . ? C10 C7 C17 Si2 88.8(8) . . . . ? C54 C4 C17 C19 131.9(7) . . . . ? C58 C4 C17 C19 -26.9(9) . . . . ? C54 C4 C17 C7 17.0(8) . . . . ? C58 C4 C17 C7 -141.9(7) . . . . ? C54 C4 C17 Si2 -108.6(6) . . . . ? C58 C4 C17 Si2 92.5(7) . . . . ? C96 Si2 C17 C19 165.3(7) . . . . ? C95 Si2 C17 C19 41.0(8) . . . . ? C111 Si2 C17 C19 -71.9(8) . . . . ? C96 Si2 C17 C7 -55.9(9) . . . . ? C95 Si2 C17 C7 179.7(8) . . . . ? C111 Si2 C17 C7 66.8(9) . . . . ? C96 Si2 C17 C4 50.7(7) . . . . ? C95 Si2 C17 C4 -73.6(7) . . . . ? C111 Si2 C17 C4 173.5(6) . . . . ? C7 C17 C19 C29 137.8(8) . . . . ? C4 C17 C19 C29 30.7(10) . . . . ? Si2 C17 C19 C29 -78.4(9) . . . . ? C7 C17 C19 C31 -25.6(10) . . . . ? C4 C17 C19 C31 -132.7(7) . . . . ? Si2 C17 C19 C31 118.2(7) . . . . ? C48 C3 C20 C32 143.6(8) . . . . ? C55 C3 C20 C32 -5.8(11) . . . . ? Ce2 C3 C20 C32 52.8(7) . . . . ? C48 C3 C20 C56 -7.1(12) . . . . ? C55 C3 C20 C56 -156.5(8) . . . . ? Ce2 C3 C20 C56 -97.9(8) . . . . ? C48 C3 C20 Ce4 70.2(9) . . . . ? C55 C3 C20 Ce4 -79.2(9) . . . . ? Ce2 C3 C20 Ce4 -20.5(6) . . . . ? C48 C3 C20 Ce2 90.8(7) . . . . ? C55 C3 C20 Ce2 -58.6(6) . . . . ? C14 Ce2 C20 C3 80.3(6) . . . . ? C64 Ce2 C20 C3 44.3(6) . . . . ? C12 Ce2 C20 C3 98.3(6) . . . . ? C75 Ce2 C20 C3 27.2(6) . . . . ? C57 Ce2 C20 C3 86.3(7) . . . . ? C55 Ce2 C20 C3 40.6(6) . . . . ? C5 Ce2 C20 C3 129.7(6) . . . . ? C2 Ce2 C20 C3 102.8(6) . . . . ? C42 Ce2 C20 C3 20.6(7) . . . . ? C11 Ce2 C20 C3 -3.3(6) . . . . ? C32 Ce2 C20 C3 126.6(9) . . . . ? C14 Ce2 C20 C32 -46.3(7) . . . . ? C64 Ce2 C20 C32 -82.3(6) . . . . ? C12 Ce2 C20 C32 -28.4(6) . . . . ? C75 Ce2 C20 C32 -99.4(6) . . . . ? C57 Ce2 C20 C32 -40.3(6) . . . . ? C55 Ce2 C20 C32 -86.0(7) . . . . ? C5 Ce2 C20 C32 3.1(6) . . . . ? C2 Ce2 C20 C32 -23.8(7) . . . . ? C42 Ce2 C20 C32 -106.0(6) . . . . ? C11 Ce2 C20 C32 -130.0(6) . . . . ? C3 Ce2 C20 C32 -126.6(9) . . . . ? C14 Ce2 C20 C56 -160.1(6) . . . . ? C64 Ce2 C20 C56 164.0(7) . . . . ? C12 Ce2 C20 C56 -142.1(7) . . . . ? C75 Ce2 C20 C56 146.8(7) . . . . ? C57 Ce2 C20 C56 -154.1(8) . . . . ? C55 Ce2 C20 C56 160.2(8) . . . . ? C5 Ce2 C20 C56 -110.6(7) . . . . ? C2 Ce2 C20 C56 -137.6(6) . . . . ? C42 Ce2 C20 C56 140.2(6) . . . . ? C11 Ce2 C20 C56 116.3(7) . . . . ? C32 Ce2 C20 C56 -113.8(10) . . . . ? C3 Ce2 C20 C56 119.6(9) . . . . ? C14 Ce2 C20 Ce4 -127.0(5) . . . . ? C64 Ce2 C20 Ce4 -162.9(5) . . . . ? C12 Ce2 C20 Ce4 -109.0(6) . . . . ? C75 Ce2 C20 Ce4 179.9(6) . . . . ? C57 Ce2 C20 Ce4 -121.0(6) . . . . ? C55 Ce2 C20 Ce4 -166.7(6) . . . . ? C5 Ce2 C20 Ce4 -77.5(5) . . . . ? C2 Ce2 C20 Ce4 -104.5(6) . . . . ? C42 Ce2 C20 Ce4 173.3(6) . . . . ? C11 Ce2 C20 Ce4 149.4(6) . . . . ? C32 Ce2 C20 Ce4 -80.7(8) . . . . ? C3 Ce2 C20 Ce4 152.7(8) . . . . ? C41 C16 C22 C63 0.2(11) . . . . ? C36 C16 C22 C63 -138.9(9) . . . . ? Ce1 C16 C22 C63 -82.3(7) . . . . ? C41 C16 C22 C43 138.0(9) . . . . ? C36 C16 C22 C43 -1.1(14) . . . . ? Ce1 C16 C22 C43 55.4(8) . . . . ? C41 C16 C22 Ce1 82.6(7) . . . . ? C36 C16 C22 Ce1 -56.5(8) . . . . ? C74 Ce1 C22 C63 -149.9(6) . . . . ? C43 Ce1 C22 C63 -120.4(8) . . . . ? C36 Ce1 C22 C63 138.1(6) . . . . ? C34 Ce1 C22 C63 174.2(6) . . . . ? C16 Ce1 C22 C63 109.2(8) . . . . ? C1 Ce1 C22 C63 -130.2(5) . . . . ? C23 Ce1 C22 C63 170.5(5) . . . . ? C33 Ce1 C22 C63 -87.7(6) . . . . ? C13 Ce1 C22 C63 123.0(5) . . . . ? C41 Ce1 C22 C63 71.5(6) . . . . ? C74 Ce1 C22 C43 -29.5(5) . . . . ? C36 Ce1 C22 C43 -101.5(6) . . . . ? C34 Ce1 C22 C43 -65.4(6) . . . . ? C16 Ce1 C22 C43 -130.4(9) . . . . ? C1 Ce1 C22 C43 -9.8(6) . . . . ? C23 Ce1 C22 C43 -69.1(6) . . . . ? C33 Ce1 C22 C43 32.8(5) . . . . ? C13 Ce1 C22 C43 -116.6(6) . . . . ? C41 Ce1 C22 C43 -168.0(7) . . . . ? C63 Ce1 C22 C43 120.4(8) . . . . ? C74 Ce1 C22 C16 100.9(7) . . . . ? C43 Ce1 C22 C16 130.4(9) . . . . ? C36 Ce1 C22 C16 28.9(6) . . . . ? C34 Ce1 C22 C16 65.0(6) . . . . ? C1 Ce1 C22 C16 120.6(6) . . . . ? C23 Ce1 C22 C16 61.3(6) . . . . ? C33 Ce1 C22 C16 163.2(7) . . . . ? C13 Ce1 C22 C16 13.8(6) . . . . ? C41 Ce1 C22 C16 -37.6(6) . . . . ? C63 Ce1 C22 C16 -109.2(8) . . . . ? C74 Ce1 C23 C61 -148.8(7) . . . . ? C43 Ce1 C23 C61 -138.0(6) . . . . ? C36 Ce1 C23 C61 -72.3(6) . . . . ? C34 Ce1 C23 C61 -114.7(8) . . . . ? C16 Ce1 C23 C61 -78.7(6) . . . . ? C22 Ce1 C23 C61 -107.7(6) . . . . ? C1 Ce1 C23 C61 174.5(7) . . . . ? C33 Ce1 C23 C61 -164.3(6) . . . . ? C13 Ce1 C23 C61 -32.3(5) . . . . ? C41 Ce1 C23 C61 -56.0(6) . . . . ? C63 Ce1 C23 C61 -101.5(6) . . . . ? C74 Ce1 C23 C34 -34.0(5) . . . . ? C43 Ce1 C23 C34 -23.3(5) . . . . ? C36 Ce1 C23 C34 42.4(5) . . . . ? C16 Ce1 C23 C34 36.0(5) . . . . ? C22 Ce1 C23 C34 7.0(6) . . . . ? C1 Ce1 C23 C34 -70.8(5) . . . . ? C33 Ce1 C23 C34 -49.6(6) . . . . ? C13 Ce1 C23 C34 82.4(6) . . . . ? C41 Ce1 C23 C34 58.7(6) . . . . ? C63 Ce1 C23 C34 13.2(6) . . . . ? C74 Ce1 C23 C46 92.3(6) . . . . ? C43 Ce1 C23 C46 103.0(5) . . . . ? C36 Ce1 C23 C46 168.8(7) . . . . ? C34 Ce1 C23 C46 126.3(8) . . . . ? C16 Ce1 C23 C46 162.4(6) . . . . ? C22 Ce1 C23 C46 133.3(5) . . . . ? C1 Ce1 C23 C46 55.6(5) . . . . ? C33 Ce1 C23 C46 76.7(6) . . . . ? C13 Ce1 C23 C46 -151.3(7) . . . . ? C41 Ce1 C23 C46 -174.9(5) . . . . ? C63 Ce1 C23 C46 139.5(5) . . . . ? C70 C24 C28 C58 -129.1(8) . . . . ? C30 C24 C28 C58 19.5(11) . . . . ? C70 C24 C28 C29 -14.5(9) . . . . ? C30 C24 C28 C29 134.1(8) . . . . ? C70 C24 C28 Si1 91.8(8) . . . . ? C30 C24 C28 Si1 -119.6(8) . . . . ? C95 Si1 C28 C58 52.3(8) . . . . ? C88 Si1 C28 C58 173.6(6) . . . . ? C87 Si1 C28 C58 -61.7(8) . . . . ? C95 Si1 C28 C24 -169.8(7) . . . . ? C88 Si1 C28 C24 -48.5(8) . . . . ? C87 Si1 C28 C24 76.2(8) . . . . ? C95 Si1 C28 C29 -63.6(6) . . . . ? C88 Si1 C28 C29 57.7(6) . . . . ? C87 Si1 C28 C29 -177.6(5) . . . . ? C31 C19 C29 C26 3.5(12) . . . . ? C17 C19 C29 C26 -159.7(7) . . . . ? C31 C19 C29 C28 157.7(7) . . . . ? C17 C19 C29 C28 -5.5(11) . . . . ? C71 C26 C29 C19 0.1(13) . . . . ? C70 C26 C29 C19 147.8(8) . . . . ? Ce4 C26 C29 C19 68.6(9) . . . . ? C71 C26 C29 C28 -156.8(8) . . . . ? C70 C26 C29 C28 -9.1(9) . . . . ? Ce4 C26 C29 C28 -88.2(8) . . . . ? C58 C28 C29 C19 -25.2(9) . . . . ? C24 C28 C29 C19 -142.1(7) . . . . ? Si1 C28 C29 C19 95.1(7) . . . . ? C58 C28 C29 C26 131.1(7) . . . . ? C24 C28 C29 C26 14.2(9) . . . . ? Si1 C28 C29 C26 -108.5(6) . . . . ? C70 C24 C30 C46 -6.3(13) . . . . ? C28 C24 C30 C46 -151.9(8) . . . . ? C70 C24 C30 C1 146.4(9) . . . . ? C28 C24 C30 C1 0.8(12) . . . . ? C74 C1 C30 C24 -157.6(9) . . . . ? C62 C1 C30 C24 -16.7(12) . . . . ? Ce1 C1 C30 C24 -99.7(7) . . . . ? C74 C1 C30 C46 -4.0(14) . . . . ? C62 C1 C30 C46 136.8(8) . . . . ? Ce1 C1 C30 C46 53.9(8) . . . . ? C29 C19 C31 C2 -151.9(8) . . . . ? C17 C19 C31 C2 12.3(11) . . . . ? C29 C19 C31 C5 0.9(11) . . . . ? C17 C19 C31 C5 165.1(7) . . . . ? C29 C19 C31 Ce2 -74.5(8) . . . . ? C17 C19 C31 Ce2 89.6(7) . . . . ? C14 C2 C31 C19 157.8(8) . . . . ? C9 C2 C31 C19 10.7(11) . . . . ? Ce2 C2 C31 C19 98.7(7) . . . . ? C14 C2 C31 C5 2.9(10) . . . . ? C9 C2 C31 C5 -144.2(7) . . . . ? Ce2 C2 C31 C5 -56.2(6) . . . . ? C14 C2 C31 Ce2 59.1(5) . . . . ? C9 C2 C31 Ce2 -88.0(6) . . . . ? C71 C5 C31 C19 -9.3(12) . . . . ? C12 C5 C31 C19 -160.5(7) . . . . ? Ce2 C5 C31 C19 -100.7(7) . . . . ? C71 C5 C31 C2 147.7(8) . . . . ? C12 C5 C31 C2 -3.4(10) . . . . ? Ce2 C5 C31 C2 56.4(6) . . . . ? C71 C5 C31 Ce2 91.3(8) . . . . ? C12 C5 C31 Ce2 -59.9(6) . . . . ? C14 Ce2 C31 C19 -160.8(8) . . . . ? C64 Ce2 C31 C19 -147.4(7) . . . . ? C12 Ce2 C31 C19 154.3(8) . . . . ? C75 Ce2 C31 C19 -166.1(6) . . . . ? C57 Ce2 C31 C19 140.8(7) . . . . ? C55 Ce2 C31 C19 159.3(6) . . . . ? C5 Ce2 C31 C19 114.6(9) . . . . ? C2 Ce2 C31 C19 -122.8(9) . . . . ? C42 Ce2 C31 C19 -117.2(6) . . . . ? C11 Ce2 C31 C19 -142.3(6) . . . . ? C32 Ce2 C31 C19 111.4(6) . . . . ? C3 Ce2 C31 C19 134.9(6) . . . . ? C14 Ce2 C31 C2 -37.9(6) . . . . ? C64 Ce2 C31 C2 -24.5(6) . . . . ? C12 Ce2 C31 C2 -82.9(6) . . . . ? C75 Ce2 C31 C2 -43.2(6) . . . . ? C57 Ce2 C31 C2 -96.4(6) . . . . ? C55 Ce2 C31 C2 -77.9(6) . . . . ? C5 Ce2 C31 C2 -122.6(8) . . . . ? C42 Ce2 C31 C2 5.6(6) . . . . ? C11 Ce2 C31 C2 -19.4(7) . . . . ? C32 Ce2 C31 C2 -125.8(6) . . . . ? C3 Ce2 C31 C2 -102.3(6) . . . . ? C14 Ce2 C31 C5 84.7(6) . . . . ? C64 Ce2 C31 C5 98.1(6) . . . . ? C12 Ce2 C31 C5 39.7(5) . . . . ? C75 Ce2 C31 C5 79.4(6) . . . . ? C57 Ce2 C31 C5 26.2(6) . . . . ? C55 Ce2 C31 C5 44.7(6) . . . . ? C2 Ce2 C31 C5 122.6(8) . . . . ? C42 Ce2 C31 C5 128.2(6) . . . . ? C11 Ce2 C31 C5 103.2(6) . . . . ? C32 Ce2 C31 C5 -3.2(6) . . . . ? C3 Ce2 C31 C5 20.3(7) . . . . ? C73 C18 C32 C20 -12.4(14) . . . . ? C71 C18 C32 C20 137.6(10) . . . . ? Ce4 C18 C32 C20 48.3(10) . . . . ? C73 C18 C32 C57 -157.2(9) . . . . ? C71 C18 C32 C57 -7.3(14) . . . . ? Ce4 C18 C32 C57 -96.5(10) . . . . ? C73 C18 C32 Ce4 -60.7(8) . . . . ? C71 C18 C32 Ce4 89.2(8) . . . . ? C73 C18 C32 Ce2 -98.7(8) . . . . ? C71 C18 C32 Ce2 51.2(8) . . . . ? Ce4 C18 C32 Ce2 -38.0(5) . . . . ? C3 C20 C32 C18 -144.1(9) . . . . ? C56 C20 C32 C18 8.2(14) . . . . ? Ce4 C20 C32 C18 -40.8(9) . . . . ? Ce2 C20 C32 C18 -90.9(8) . . . . ? C3 C20 C32 C57 6.3(11) . . . . ? C56 C20 C32 C57 158.6(8) . . . . ? Ce4 C20 C32 C57 109.6(8) . . . . ? Ce2 C20 C32 C57 59.5(6) . . . . ? C3 C20 C32 Ce4 -103.4(8) . . . . ? C56 C20 C32 Ce4 49.0(9) . . . . ? Ce2 C20 C32 Ce4 -50.1(4) . . . . ? C3 C20 C32 Ce2 -53.3(7) . . . . ? C56 C20 C32 Ce2 99.1(8) . . . . ? Ce4 C20 C32 Ce2 50.1(4) . . . . ? C14 Ce2 C32 C18 -101.5(6) . . . . ? C64 Ce2 C32 C18 -133.3(6) . . . . ? C12 Ce2 C32 C18 -92.6(6) . . . . ? C75 Ce2 C32 C18 -161.7(6) . . . . ? C57 Ce2 C32 C18 -127.4(8) . . . . ? C55 Ce2 C32 C18 -168.0(7) . . . . ? C5 Ce2 C32 C18 -54.1(5) . . . . ? C2 Ce2 C32 C18 -76.2(6) . . . . ? C42 Ce2 C32 C18 -139.8(5) . . . . ? C11 Ce2 C32 C18 173.8(6) . . . . ? C3 Ce2 C32 C18 151.3(7) . . . . ? C14 Ce2 C32 C20 136.2(6) . . . . ? C64 Ce2 C32 C20 104.4(6) . . . . ? C12 Ce2 C32 C20 145.1(7) . . . . ? C75 Ce2 C32 C20 76.1(6) . . . . ? C57 Ce2 C32 C20 110.3(8) . . . . ? C55 Ce2 C32 C20 69.8(6) . . . . ? C5 Ce2 C32 C20 -176.3(7) . . . . ? C2 Ce2 C32 C20 161.6(6) . . . . ? C42 Ce2 C32 C20 97.9(6) . . . . ? C11 Ce2 C32 C20 51.6(6) . . . . ? C3 Ce2 C32 C20 29.1(6) . . . . ? C14 Ce2 C32 C57 25.9(5) . . . . ? C64 Ce2 C32 C57 -5.9(6) . . . . ? C12 Ce2 C32 C57 34.8(5) . . . . ? C75 Ce2 C32 C57 -34.3(5) . . . . ? C55 Ce2 C32 C57 -40.5(5) . . . . ? C5 Ce2 C32 C57 73.3(6) . . . . ? C2 Ce2 C32 C57 51.2(6) . . . . ? C42 Ce2 C32 C57 -12.4(7) . . . . ? C11 Ce2 C32 C57 -58.7(6) . . . . ? C3 Ce2 C32 C57 -81.3(6) . . . . ? C14 Ce2 C32 Ce4 -145.0(5) . . . . ? C64 Ce2 C32 Ce4 -176.9(5) . . . . ? C12 Ce2 C32 Ce4 -136.1(6) . . . . ? C75 Ce2 C32 Ce4 154.8(5) . . . . ? C57 Ce2 C32 Ce4 -170.9(7) . . . . ? C55 Ce2 C32 Ce4 148.5(6) . . . . ? C5 Ce2 C32 Ce4 -97.6(5) . . . . ? C2 Ce2 C32 Ce4 -119.7(5) . . . . ? C42 Ce2 C32 Ce4 176.7(5) . . . . ? C11 Ce2 C32 Ce4 130.3(5) . . . . ? C3 Ce2 C32 Ce4 107.8(6) . . . . ? C54 C8 C33 C62 10.7(11) . . . . ? C15 C8 C33 C62 -138.8(8) . . . . ? Ce3 C8 C33 C62 -84.4(9) . . . . ? C54 C8 C33 C43 155.7(8) . . . . ? C15 C8 C33 C43 6.1(13) . . . . ? Ce3 C8 C33 C43 60.5(10) . . . . ? C54 C8 C33 Ce1 94.9(6) . . . . ? C15 C8 C33 Ce1 -54.6(8) . . . . ? Ce3 C8 C33 Ce1 -0.2(6) . . . . ? C74 Ce1 C33 C62 -73.7(6) . . . . ? C43 Ce1 C33 C62 -116.1(8) . . . . ? C36 Ce1 C33 C62 -111.4(6) . . . . ? C34 Ce1 C33 C62 -80.0(6) . . . . ? C16 Ce1 C33 C62 -141.3(6) . . . . ? C22 Ce1 C33 C62 -150.5(7) . . . . ? C1 Ce1 C33 C62 -32.6(5) . . . . ? C23 Ce1 C33 C62 -57.1(6) . . . . ? C13 Ce1 C33 C62 -107.0(6) . . . . ? C41 Ce1 C33 C62 -166.8(5) . . . . ? C63 Ce1 C33 C62 174.4(7) . . . . ? C74 Ce1 C33 C8 166.8(7) . . . . ? C43 Ce1 C33 C8 124.5(9) . . . . ? C36 Ce1 C33 C8 129.2(6) . . . . ? C34 Ce1 C33 C8 160.5(6) . . . . ? C16 Ce1 C33 C8 99.2(6) . . . . ? C22 Ce1 C33 C8 90.0(6) . . . . ? C1 Ce1 C33 C8 -152.0(7) . . . . ? C23 Ce1 C33 C8 -176.5(5) . . . . ? C13 Ce1 C33 C8 133.6(6) . . . . ? C41 Ce1 C33 C8 73.8(6) . . . . ? C63 Ce1 C33 C8 55.0(6) . . . . ? C74 Ce1 C33 C43 42.3(6) . . . . ? C36 Ce1 C33 C43 4.7(6) . . . . ? C34 Ce1 C33 C43 36.0(6) . . . . ? C16 Ce1 C33 C43 -25.3(6) . . . . ? C22 Ce1 C33 C43 -34.5(6) . . . . ? C1 Ce1 C33 C43 83.5(6) . . . . ? C23 Ce1 C33 C43 59.0(6) . . . . ? C13 Ce1 C33 C43 9.1(7) . . . . ? C41 Ce1 C33 C43 -50.7(6) . . . . ? C63 Ce1 C33 C43 -69.5(6) . . . . ? C61 C23 C34 C74 139.3(9) . . . . ? C46 C23 C34 C74 -9.8(15) . . . . ? Ce1 C23 C34 C74 64.1(8) . . . . ? C61 C23 C34 C36 5.8(11) . . . . ? C46 C23 C34 C36 -143.3(9) . . . . ? Ce1 C23 C34 C36 -69.4(6) . . . . ? C61 C23 C34 Ce1 75.2(7) . . . . ? C46 C23 C34 Ce1 -73.9(9) . . . . ? C74 Ce1 C34 C23 124.3(8) . . . . ? C43 Ce1 C34 C23 153.2(6) . . . . ? C36 Ce1 C34 C23 -110.0(8) . . . . ? C16 Ce1 C34 C23 -138.0(6) . . . . ? C22 Ce1 C34 C23 -172.8(6) . . . . ? C1 Ce1 C34 C23 90.2(6) . . . . ? C33 Ce1 C34 C23 133.0(5) . . . . ? C13 Ce1 C34 C23 -71.9(6) . . . . ? C41 Ce1 C34 C23 -124.1(5) . . . . ? C63 Ce1 C34 C23 -169.9(5) . . . . ? C43 Ce1 C34 C74 28.9(5) . . . . ? C36 Ce1 C34 C74 125.7(9) . . . . ? C16 Ce1 C34 C74 97.8(6) . . . . ? C22 Ce1 C34 C74 62.9(6) . . . . ? C1 Ce1 C34 C74 -34.1(5) . . . . ? C23 Ce1 C34 C74 -124.3(8) . . . . ? C33 Ce1 C34 C74 8.7(6) . . . . ? C13 Ce1 C34 C74 163.8(7) . . . . ? C41 Ce1 C34 C74 111.6(6) . . . . ? C63 Ce1 C34 C74 65.8(6) . . . . ? C74 Ce1 C34 C36 -125.7(9) . . . . ? C43 Ce1 C34 C36 -96.8(6) . . . . ? C16 Ce1 C34 C36 -28.0(5) . . . . ? C22 Ce1 C34 C36 -62.8(5) . . . . ? C1 Ce1 C34 C36 -159.8(7) . . . . ? C23 Ce1 C34 C36 110.0(8) . . . . ? C33 Ce1 C34 C36 -117.0(6) . . . . ? C13 Ce1 C34 C36 38.1(5) . . . . ? C41 Ce1 C34 C36 -14.1(6) . . . . ? C63 Ce1 C34 C36 -59.9(6) . . . . ? C105 C84 C87 C97 -1.7(14) . . . . ? C98 C84 C87 C97 178.4(9) . . . . ? C105 C84 C87 Si1 173.7(7) . . . . ? C98 C84 C87 Si1 -6.1(14) . . . . ? C95 Si1 C87 C84 -114.4(9) . . . . ? C88 Si1 C87 C84 122.4(9) . . . . ? C28 Si1 C87 C84 0.1(11) . . . . ? C95 Si1 C87 C97 61.2(8) . . . . ? C88 Si1 C87 C97 -61.9(7) . . . . ? C28 Si1 C87 C97 175.7(6) . . . . ? C106 C85 C88 C81 4.2(11) . . . . ? C93 C85 C88 C81 -177.3(7) . . . . ? C106 C85 C88 Si1 -177.0(6) . . . . ? C93 C85 C88 Si1 1.5(11) . . . . ? C92 C81 C88 C85 -2.1(11) . . . . ? C86 C81 C88 C85 -179.9(7) . . . . ? C92 C81 C88 Si1 179.0(5) . . . . ? C86 C81 C88 Si1 1.2(10) . . . . ? C95 Si1 C88 C85 15.4(8) . . . . ? C87 Si1 C88 C85 129.9(7) . . . . ? C28 Si1 C88 C85 -96.9(7) . . . . ? C95 Si1 C88 C81 -165.8(5) . . . . ? C87 Si1 C88 C81 -51.3(7) . . . . ? C28 Si1 C88 C81 81.8(6) . . . . ? C41 C16 C36 C13 1.0(12) . . . . ? C22 C16 C36 C13 135.2(9) . . . . ? Ce1 C16 C36 C13 77.7(7) . . . . ? C41 C16 C36 C34 -135.1(9) . . . . ? C22 C16 C36 C34 -0.9(14) . . . . ? Ce1 C16 C36 C34 -58.4(8) . . . . ? C41 C16 C36 Ce1 -76.7(8) . . . . ? C22 C16 C36 Ce1 57.5(8) . . . . ? C52 C13 C36 C16 5.4(13) . . . . ? C61 C13 C36 C16 -143.3(8) . . . . ? Ce1 C13 C36 C16 -71.4(7) . . . . ? C52 C13 C36 C34 147.7(8) . . . . ? C61 C13 C36 C34 -0.9(10) . . . . ? Ce1 C13 C36 C34 70.9(6) . . . . ? C52 C13 C36 Ce1 76.8(8) . . . . ? C61 C13 C36 Ce1 -71.9(7) . . . . ? C23 C34 C36 C16 137.5(9) . . . . ? C74 C34 C36 C16 1.6(14) . . . . ? Ce1 C34 C36 C16 59.7(8) . . . . ? C23 C34 C36 C13 -2.9(10) . . . . ? C74 C34 C36 C13 -138.7(9) . . . . ? Ce1 C34 C36 C13 -80.7(6) . . . . ? C23 C34 C36 Ce1 77.9(7) . . . . ? C74 C34 C36 Ce1 -58.0(7) . . . . ? C74 Ce1 C36 C16 -99.3(6) . . . . ? C43 Ce1 C36 C16 -63.4(5) . . . . ? C34 Ce1 C36 C16 -131.1(8) . . . . ? C22 Ce1 C36 C16 -29.3(5) . . . . ? C1 Ce1 C36 C16 -114.5(5) . . . . ? C23 Ce1 C36 C16 -168.3(6) . . . . ? C33 Ce1 C36 C16 -66.0(5) . . . . ? C13 Ce1 C36 C16 120.3(8) . . . . ? C41 Ce1 C36 C16 31.3(5) . . . . ? C63 Ce1 C36 C16 -10.0(5) . . . . ? C74 Ce1 C36 C13 140.4(7) . . . . ? C43 Ce1 C36 C13 176.2(7) . . . . ? C34 Ce1 C36 C13 108.5(9) . . . . ? C16 Ce1 C36 C13 -120.3(8) . . . . ? C22 Ce1 C36 C13 -149.6(7) . . . . ? C1 Ce1 C36 C13 125.1(6) . . . . ? C23 Ce1 C36 C13 71.4(6) . . . . ? C33 Ce1 C36 C13 173.7(6) . . . . ? C41 Ce1 C36 C13 -89.0(6) . . . . ? C63 Ce1 C36 C13 -130.3(6) . . . . ? C74 Ce1 C36 C34 31.9(5) . . . . ? C43 Ce1 C36 C34 67.7(6) . . . . ? C16 Ce1 C36 C34 131.1(8) . . . . ? C22 Ce1 C36 C34 101.8(6) . . . . ? C1 Ce1 C36 C34 16.6(6) . . . . ? C23 Ce1 C36 C34 -37.1(5) . . . . ? C33 Ce1 C36 C34 65.1(6) . . . . ? C13 Ce1 C36 C34 -108.5(9) . . . . ? C41 Ce1 C36 C34 162.5(7) . . . . ? C63 Ce1 C36 C34 121.1(6) . . . . ? C51 C21 C38 C40 -144.0(9) . . . . ? C60 C21 C38 C40 2.7(15) . . . . ? C51 C21 C38 C59 -1.2(10) . . . . ? C60 C21 C38 C59 145.4(9) . . . . ? C102 C83 C89 C100 0.9(18) . . . . ? C114 C83 C89 C100 -178.2(11) . . . . ? C45 C37 C39 C56 -144.2(8) . . . . ? C65 C37 C39 C56 2.2(13) . . . . ? C45 C37 C39 C25 -1.7(8) . . . . ? C65 C37 C39 C25 144.8(7) . . . . ? C48 C25 C39 C37 -142.6(8) . . . . ? C67 C25 C39 C37 3.4(8) . . . . ? C48 C25 C39 C56 1.4(12) . . . . ? C67 C25 C39 C56 147.4(7) . . . . ? C41 C35 C40 C38 -3.3(14) . . . . ? C63 C35 C40 C38 -148.6(9) . . . . ? Ce3 C35 C40 C38 -100.2(9) . . . . ? C41 C35 C40 C76 147.3(9) . . . . ? C63 C35 C40 C76 2.1(15) . . . . ? Ce3 C35 C40 C76 50.4(9) . . . . ? C41 C35 C40 Ce3 96.9(10) . . . . ? C63 C35 C40 Ce3 -48.4(10) . . . . ? C21 C38 C40 C35 144.4(10) . . . . ? C59 C38 C40 C35 5.3(13) . . . . ? C21 C38 C40 C76 -6.4(14) . . . . ? C59 C38 C40 C76 -145.4(9) . . . . ? C21 C38 C40 Ce3 61.8(12) . . . . ? C59 C38 C40 Ce3 -77.3(10) . . . . ? C36 C16 C41 C53 -7.8(13) . . . . ? C22 C16 C41 C53 -147.2(9) . . . . ? Ce1 C16 C41 C53 -75.2(9) . . . . ? C36 C16 C41 C35 142.5(9) . . . . ? C22 C16 C41 C35 3.2(11) . . . . ? Ce1 C16 C41 C35 75.2(7) . . . . ? C36 C16 C41 Ce1 67.4(7) . . . . ? C22 C16 C41 Ce1 -72.0(6) . . . . ? C40 C35 C41 C16 -155.6(9) . . . . ? C63 C35 C41 C16 -5.2(11) . . . . ? Ce3 C35 C41 C16 -78.1(10) . . . . ? C40 C35 C41 C53 -3.8(14) . . . . ? C63 C35 C41 C53 146.6(9) . . . . ? Ce3 C35 C41 C53 73.7(10) . . . . ? C40 C35 C41 Ce1 -96.5(9) . . . . ? C63 C35 C41 Ce1 53.9(7) . . . . ? Ce3 C35 C41 Ce1 -19.0(6) . . . . ? C74 Ce1 C41 C16 7.4(6) . . . . ? C43 Ce1 C41 C16 36.5(6) . . . . ? C36 Ce1 C41 C16 -35.0(6) . . . . ? C34 Ce1 C41 C16 -25.1(6) . . . . ? C22 Ce1 C41 C16 43.0(6) . . . . ? C1 Ce1 C41 C16 13.4(7) . . . . ? C23 Ce1 C41 C16 -51.0(6) . . . . ? C33 Ce1 C41 C16 60.3(6) . . . . ? C13 Ce1 C41 C16 -71.8(6) . . . . ? C63 Ce1 C41 C16 82.2(6) . . . . ? C74 Ce1 C41 C53 133.3(7) . . . . ? C43 Ce1 C41 C53 162.4(7) . . . . ? C36 Ce1 C41 C53 90.9(7) . . . . ? C34 Ce1 C41 C53 100.8(7) . . . . ? C16 Ce1 C41 C53 125.9(9) . . . . ? C22 Ce1 C41 C53 168.8(8) . . . . ? C1 Ce1 C41 C53 139.3(6) . . . . ? C23 Ce1 C41 C53 74.9(7) . . . . ? C33 Ce1 C41 C53 -173.9(6) . . . . ? C13 Ce1 C41 C53 54.1(6) . . . . ? C63 Ce1 C41 C53 -151.9(8) . . . . ? C74 Ce1 C41 C35 -107.6(6) . . . . ? C43 Ce1 C41 C35 -78.5(6) . . . . ? C36 Ce1 C41 C35 -150.0(7) . . . . ? C34 Ce1 C41 C35 -140.1(6) . . . . ? C16 Ce1 C41 C35 -115.0(9) . . . . ? C22 Ce1 C41 C35 -72.1(6) . . . . ? C1 Ce1 C41 C35 -101.6(6) . . . . ? C23 Ce1 C41 C35 -166.0(6) . . . . ? C33 Ce1 C41 C35 -54.8(6) . . . . ? C13 Ce1 C41 C35 173.2(7) . . . . ? C63 Ce1 C41 C35 -32.8(6) . . . . ? C11 C6 C42 C64 -3.1(11) . . . . ? C60 C6 C42 C64 -155.3(9) . . . . ? Ce2 C6 C42 C64 -59.1(6) . . . . ? C11 C6 C42 C44 142.9(9) . . . . ? C60 C6 C42 C44 -9.3(14) . . . . ? Ce2 C6 C42 C44 86.9(8) . . . . ? C11 C6 C42 Ce2 56.0(7) . . . . ? C60 C6 C42 Ce2 -96.2(9) . . . . ? C14 Ce2 C42 C64 -35.9(5) . . . . ? C12 Ce2 C42 C64 -24.2(5) . . . . ? C75 Ce2 C42 C64 40.5(5) . . . . ? C57 Ce2 C42 C64 6.1(5) . . . . ? C55 Ce2 C42 C64 34.1(5) . . . . ? C5 Ce2 C42 C64 -50.6(5) . . . . ? C2 Ce2 C42 C64 -71.8(5) . . . . ? C11 Ce2 C42 C64 80.9(6) . . . . ? C32 Ce2 C42 C64 12.4(6) . . . . ? C3 Ce2 C42 C64 58.1(5) . . . . ? C14 Ce2 C42 C6 -149.1(7) . . . . ? C64 Ce2 C42 C6 -113.2(8) . . . . ? C12 Ce2 C42 C6 -137.4(6) . . . . ? C75 Ce2 C42 C6 -72.8(6) . . . . ? C57 Ce2 C42 C6 -107.1(6) . . . . ? C55 Ce2 C42 C6 -79.1(6) . . . . ? C5 Ce2 C42 C6 -163.8(6) . . . . ? C2 Ce2 C42 C6 175.0(7) . . . . ? C11 Ce2 C42 C6 -32.3(6) . . . . ? C32 Ce2 C42 C6 -100.8(6) . . . . ? C3 Ce2 C42 C6 -55.1(6) . . . . ? C14 Ce2 C42 C44 92.4(6) . . . . ? C64 Ce2 C42 C44 128.3(8) . . . . ? C12 Ce2 C42 C44 104.1(6) . . . . ? C75 Ce2 C42 C44 168.7(7) . . . . ? C57 Ce2 C42 C44 134.4(6) . . . . ? C55 Ce2 C42 C44 162.4(6) . . . . ? C5 Ce2 C42 C44 77.7(6) . . . . ? C2 Ce2 C42 C44 56.5(5) . . . . ? C11 Ce2 C42 C44 -150.8(8) . . . . ? C32 Ce2 C42 C44 140.7(5) . . . . ? C3 Ce2 C42 C44 -173.6(5) . . . . ? C63 C22 C43 C33 -0.6(13) . . . . ? C16 C22 C43 C33 -134.2(9) . . . . ? Ce1 C22 C43 C33 -77.6(8) . . . . ? C63 C22 C43 C74 135.9(10) . . . . ? C16 C22 C43 C74 2.3(14) . . . . ? Ce1 C22 C43 C74 58.9(8) . . . . ? C63 C22 C43 Ce1 77.0(8) . . . . ? C16 C22 C43 Ce1 -56.6(8) . . . . ? C62 C33 C43 C22 142.9(8) . . . . ? C8 C33 C43 C22 -5.2(13) . . . . ? Ce1 C33 C43 C22 72.3(7) . . . . ? C62 C33 C43 C74 0.4(10) . . . . ? C8 C33 C43 C74 -147.8(8) . . . . ? Ce1 C33 C43 C74 -70.2(6) . . . . ? C62 C33 C43 Ce1 70.6(7) . . . . ? C8 C33 C43 Ce1 -77.5(8) . . . . ? C74 Ce1 C43 C22 130.4(8) . . . . ? C36 Ce1 C43 C22 63.8(6) . . . . ? C34 Ce1 C43 C22 100.8(6) . . . . ? C16 Ce1 C43 C22 29.2(6) . . . . ? C1 Ce1 C43 C22 167.8(7) . . . . ? C23 Ce1 C43 C22 114.1(6) . . . . ? C33 Ce1 C43 C22 -121.1(9) . . . . ? C13 Ce1 C43 C22 65.8(6) . . . . ? C41 Ce1 C43 C22 9.3(6) . . . . ? C63 Ce1 C43 C22 -31.9(5) . . . . ? C74 Ce1 C43 C33 -108.6(7) . . . . ? C36 Ce1 C43 C33 -175.2(7) . . . . ? C34 Ce1 C43 C33 -138.1(7) . . . . ? C16 Ce1 C43 C33 150.3(7) . . . . ? C22 Ce1 C43 C33 121.1(9) . . . . ? C1 Ce1 C43 C33 -71.1(6) . . . . ? C23 Ce1 C43 C33 -124.8(6) . . . . ? C13 Ce1 C43 C33 -173.2(6) . . . . ? C41 Ce1 C43 C33 130.4(6) . . . . ? C63 Ce1 C43 C33 89.2(6) . . . . ? C36 Ce1 C43 C74 -66.6(5) . . . . ? C34 Ce1 C43 C74 -29.6(5) . . . . ? C16 Ce1 C43 C74 -101.1(6) . . . . ? C22 Ce1 C43 C74 -130.4(8) . . . . ? C1 Ce1 C43 C74 37.4(5) . . . . ? C23 Ce1 C43 C74 -16.2(5) . . . . ? C33 Ce1 C43 C74 108.6(7) . . . . ? C13 Ce1 C43 C74 -64.6(5) . . . . ? C41 Ce1 C43 C74 -121.1(5) . . . . ? C63 Ce1 C43 C74 -162.3(6) . . . . ? C7 C9 C44 C49 2.0(12) . . . . ? C2 C9 C44 C49 -152.3(8) . . . . ? C7 C9 C44 C42 153.7(9) . . . . ? C2 C9 C44 C42 -0.5(12) . . . . ? C64 C42 C44 C49 155.0(9) . . . . ? C6 C42 C44 C49 14.7(13) . . . . ? Ce2 C42 C44 C49 98.2(8) . . . . ? C64 C42 C44 C9 2.6(14) . . . . ? C6 C42 C44 C9 -137.7(9) . . . . ? Ce2 C42 C44 C9 -54.3(8) . . . . ? C39 C37 C45 C52 144.4(8) . . . . ? C65 C37 C45 C52 -1.3(12) . . . . ? C39 C37 C45 C67 -0.8(8) . . . . ? C65 C37 C45 C67 -146.5(8) . . . . ? C24 C30 C46 C77 1.3(13) . . . . ? C1 C30 C46 C77 -151.9(9) . . . . ? C24 C30 C46 C23 153.3(9) . . . . ? C1 C30 C46 C23 0.0(12) . . . . ? C61 C23 C46 C77 13.1(13) . . . . ? C34 C23 C46 C77 159.7(9) . . . . ? Ce1 C23 C46 C77 99.0(8) . . . . ? C61 C23 C46 C30 -139.7(9) . . . . ? C34 C23 C46 C30 6.9(14) . . . . ? Ce1 C23 C46 C30 -53.8(8) . . . . ? C6 C11 C47 C51 -10.7(13) . . . . ? C75 C11 C47 C51 -155.0(9) . . . . ? Ce2 C11 C47 C51 -95.8(8) . . . . ? C6 C11 C47 C48 139.5(9) . . . . ? C75 C11 C47 C48 -4.8(14) . . . . ? Ce2 C11 C47 C48 54.4(8) . . . . ? C67 C25 C48 C3 -150.4(8) . . . . ? C39 C25 C48 C3 -10.5(12) . . . . ? C67 C25 C48 C47 2.7(11) . . . . ? C39 C25 C48 C47 142.6(8) . . . . ? C20 C3 C48 C25 13.2(12) . . . . ? C55 C3 C48 C25 156.4(8) . . . . ? Ce2 C3 C48 C25 99.2(7) . . . . ? C20 C3 C48 C47 -140.3(8) . . . . ? C55 C3 C48 C47 3.0(13) . . . . ? Ce2 C3 C48 C47 -54.2(8) . . . . ? C51 C47 C48 C25 -2.2(11) . . . . ? C11 C47 C48 C25 -152.1(8) . . . . ? C51 C47 C48 C3 151.5(8) . . . . ? C11 C47 C48 C3 1.6(12) . . . . ? C9 C44 C49 C69 0.6(13) . . . . ? C42 C44 C49 C69 -151.8(9) . . . . ? C9 C44 C49 C78 143.6(9) . . . . ? C42 C44 C49 C78 -8.7(14) . . . . ? C9 C44 C49 Ce3 66.7(9) . . . . ? C42 C44 C49 Ce3 -85.7(9) . . . . ? C11 C47 C51 C21 9.0(14) . . . . ? C48 C47 C51 C21 -140.5(9) . . . . ? C11 C47 C51 C66 149.2(8) . . . . ? C48 C47 C51 C66 -0.3(11) . . . . ? C38 C21 C51 C47 144.8(9) . . . . ? C60 C21 C51 C47 -0.8(15) . . . . ? C38 C21 C51 C66 0.5(10) . . . . ? C60 C21 C51 C66 -145.2(9) . . . . ? C37 C45 C52 C13 10.0(11) . . . . ? C67 C45 C52 C13 150.9(8) . . . . ? C37 C45 C52 C53 -141.8(8) . . . . ? C67 C45 C52 C53 -0.9(11) . . . . ? C36 C13 C52 C45 -157.2(8) . . . . ? C61 C13 C52 C45 -12.8(11) . . . . ? Ce1 C13 C52 C45 -97.0(7) . . . . ? C36 C13 C52 C53 -5.0(13) . . . . ? C61 C13 C52 C53 139.4(8) . . . . ? Ce1 C13 C52 C53 55.1(8) . . . . ? C16 C41 C53 C59 156.5(9) . . . . ? C35 C41 C53 C59 8.5(13) . . . . ? Ce1 C41 C53 C59 97.3(8) . . . . ? C16 C41 C53 C52 8.1(13) . . . . ? C35 C41 C53 C52 -139.8(9) . . . . ? Ce1 C41 C53 C52 -51.0(8) . . . . ? C45 C52 C53 C59 1.3(11) . . . . ? C13 C52 C53 C59 -149.6(8) . . . . ? C45 C52 C53 C41 149.2(8) . . . . ? C13 C52 C53 C41 -1.6(12) . . . . ? C88 C81 C92 C94 -0.3(11) . . . . ? C86 C81 C92 C94 177.5(7) . . . . ? C58 C4 C54 C10 148.9(7) . . . . ? C17 C4 C54 C10 -9.8(8) . . . . ? C58 C4 C54 C8 -0.7(11) . . . . ? C17 C4 C54 C8 -159.4(7) . . . . ? C58 C4 C54 Ce3 67.6(9) . . . . ? C17 C4 C54 Ce3 -91.1(7) . . . . ? C69 C10 C54 C4 -148.0(7) . . . . ? C7 C10 C54 C4 -2.9(8) . . . . ? Ce3 C10 C54 C4 -106.3(6) . . . . ? C69 C10 C54 C8 0.0(12) . . . . ? C7 C10 C54 C8 145.1(8) . . . . ? Ce3 C10 C54 C8 41.7(8) . . . . ? C69 C10 C54 Ce3 -41.6(8) . . . . ? C7 C10 C54 Ce3 103.4(7) . . . . ? C33 C8 C54 C4 -6.5(11) . . . . ? C15 C8 C54 C4 143.8(8) . . . . ? Ce3 C8 C54 C4 96.8(8) . . . . ? C33 C8 C54 C10 -150.3(8) . . . . ? C15 C8 C54 C10 0.0(12) . . . . ? Ce3 C8 C54 C10 -47.0(9) . . . . ? C33 C8 C54 Ce3 -103.3(8) . . . . ? C15 C8 C54 Ce3 47.0(7) . . . . ? C20 C3 C55 C75 142.5(9) . . . . ? C48 C3 C55 C75 -4.6(14) . . . . ? Ce2 C3 C55 C75 67.7(7) . . . . ? C20 C3 C55 C57 3.1(10) . . . . ? C48 C3 C55 C57 -144.1(9) . . . . ? Ce2 C3 C55 C57 -71.8(6) . . . . ? C20 C3 C55 Ce2 74.8(7) . . . . ? C48 C3 C55 Ce2 -72.3(9) . . . . ? C14 Ce2 C55 C75 65.2(6) . . . . ? C64 Ce2 C55 C75 28.9(5) . . . . ? C12 Ce2 C55 C75 100.9(6) . . . . ? C57 Ce2 C55 C75 131.5(8) . . . . ? C5 Ce2 C55 C75 117.0(6) . . . . ? C2 Ce2 C55 C75 67.6(6) . . . . ? C42 Ce2 C55 C75 9.3(5) . . . . ? C11 Ce2 C55 C75 -33.6(5) . . . . ? C32 Ce2 C55 C75 168.4(7) . . . . ? C3 Ce2 C55 C75 -120.4(8) . . . . ? C14 Ce2 C55 C57 -66.3(6) . . . . ? C64 Ce2 C55 C57 -102.6(6) . . . . ? C12 Ce2 C55 C57 -30.6(6) . . . . ? C75 Ce2 C55 C57 -131.5(8) . . . . ? C5 Ce2 C55 C57 -14.5(6) . . . . ? C2 Ce2 C55 C57 -63.9(6) . . . . ? C42 Ce2 C55 C57 -122.3(6) . . . . ? C11 Ce2 C55 C57 -165.1(7) . . . . ? C32 Ce2 C55 C57 36.9(5) . . . . ? C3 Ce2 C55 C57 108.0(9) . . . . ? C14 Ce2 C55 C3 -174.4(7) . . . . ? C64 Ce2 C55 C3 149.3(7) . . . . ? C12 Ce2 C55 C3 -138.6(7) . . . . ? C75 Ce2 C55 C3 120.4(8) . . . . ? C57 Ce2 C55 C3 -108.0(9) . . . . ? C5 Ce2 C55 C3 -122.6(6) . . . . ? C2 Ce2 C55 C3 -171.9(6) . . . . ? C42 Ce2 C55 C3 129.7(6) . . . . ? C11 Ce2 C55 C3 86.9(6) . . . . ? C32 Ce2 C55 C3 -71.1(6) . . . . ? C37 C39 C56 C72 -8.1(13) . . . . ? C25 C39 C56 C72 -147.8(8) . . . . ? C37 C39 C56 C20 144.3(8) . . . . ? C25 C39 C56 C20 4.6(11) . . . . ? C37 C39 C56 Ce4 61.3(10) . . . . ? C25 C39 C56 Ce4 -78.4(9) . . . . ? C3 C20 C56 C72 149.8(9) . . . . ? C32 C20 C56 C72 0.9(14) . . . . ? Ce4 C20 C56 C72 49.4(9) . . . . ? Ce2 C20 C56 C72 74.4(10) . . . . ? C3 C20 C56 C39 -1.9(12) . . . . ? C32 C20 C56 C39 -150.7(8) . . . . ? Ce4 C20 C56 C39 -102.2(8) . . . . ? Ce2 C20 C56 C39 -77.3(8) . . . . ? C3 C20 C56 Ce4 100.3(9) . . . . ? C32 C20 C56 Ce4 -48.5(9) . . . . ? Ce2 C20 C56 Ce4 24.9(6) . . . . ? C14 C12 C57 C32 133.7(10) . . . . ? C5 C12 C57 C32 0.6(13) . . . . ? Ce2 C12 C57 C32 76.4(8) . . . . ? C14 C12 C57 C55 -2.3(14) . . . . ? C5 C12 C57 C55 -135.4(10) . . . . ? Ce2 C12 C57 C55 -59.6(8) . . . . ? C14 C12 C57 Ce2 57.3(9) . . . . ? C5 C12 C57 Ce2 -75.9(8) . . . . ? C18 C32 C57 C12 6.4(15) . . . . ? C20 C32 C57 C12 -143.3(9) . . . . ? Ce4 C32 C57 C12 -60.0(11) . . . . ? Ce2 C32 C57 C12 -67.5(8) . . . . ? C18 C32 C57 C55 145.6(9) . . . . ? C20 C32 C57 C55 -4.1(10) . . . . ? Ce4 C32 C57 C55 79.2(9) . . . . ? Ce2 C32 C57 C55 71.7(7) . . . . ? C18 C32 C57 Ce2 73.8(9) . . . . ? C20 C32 C57 Ce2 -75.8(6) . . . . ? Ce4 C32 C57 Ce2 7.5(6) . . . . ? C75 C55 C57 C12 2.6(14) . . . . ? C3 C55 C57 C12 140.5(9) . . . . ? Ce2 C55 C57 C12 58.5(8) . . . . ? C75 C55 C57 C32 -137.2(10) . . . . ? C3 C55 C57 C32 0.7(10) . . . . ? Ce2 C55 C57 C32 -81.2(7) . . . . ? C75 C55 C57 Ce2 -56.0(9) . . . . ? C3 C55 C57 Ce2 82.0(7) . . . . ? C14 Ce2 C57 C12 -28.4(5) . . . . ? C64 Ce2 C57 C12 -64.6(6) . . . . ? C75 Ce2 C57 C12 -99.1(6) . . . . ? C55 Ce2 C57 C12 -127.2(9) . . . . ? C5 Ce2 C57 C12 35.0(5) . . . . ? C2 Ce2 C57 C12 -9.4(6) . . . . ? C42 Ce2 C57 C12 -68.0(6) . . . . ? C11 Ce2 C57 C12 -115.1(6) . . . . ? C32 Ce2 C57 C12 121.5(9) . . . . ? C3 Ce2 C57 C12 -166.3(8) . . . . ? C14 Ce2 C57 C32 -150.0(6) . . . . ? C64 Ce2 C57 C32 173.8(6) . . . . ? C12 Ce2 C57 C32 -121.5(9) . . . . ? C75 Ce2 C57 C32 139.4(6) . . . . ? C55 Ce2 C57 C32 111.3(8) . . . . ? C5 Ce2 C57 C32 -86.5(6) . . . . ? C2 Ce2 C57 C32 -130.9(6) . . . . ? C42 Ce2 C57 C32 170.5(5) . . . . ? C11 Ce2 C57 C32 123.4(6) . . . . ? C3 Ce2 C57 C32 72.1(6) . . . . ? C14 Ce2 C57 C55 98.7(6) . . . . ? C64 Ce2 C57 C55 62.5(6) . . . . ? C12 Ce2 C57 C55 127.2(9) . . . . ? C75 Ce2 C57 C55 28.1(6) . . . . ? C5 Ce2 C57 C55 162.2(7) . . . . ? C2 Ce2 C57 C55 117.8(6) . . . . ? C42 Ce2 C57 C55 59.2(6) . . . . ? C11 Ce2 C57 C55 12.1(6) . . . . ? C32 Ce2 C57 C55 -111.3(8) . . . . ? C3 Ce2 C57 C55 -39.2(5) . . . . ? C81 C92 C94 C106 0.7(12) . . . . ? C81 C92 C94 C112 -179.4(8) . . . . ? C54 C4 C58 C62 3.6(10) . . . . ? C17 C4 C58 C62 160.1(6) . . . . ? C54 C4 C58 C28 -159.6(7) . . . . ? C17 C4 C58 C28 -3.0(10) . . . . ? C24 C28 C58 C4 136.7(7) . . . . ? C29 C28 C58 C4 28.4(9) . . . . ? Si1 C28 C58 C4 -81.9(8) . . . . ? C24 C28 C58 C62 -25.3(10) . . . . ? C29 C28 C58 C62 -133.7(7) . . . . ? Si1 C28 C58 C62 116.1(7) . . . . ? C41 C53 C59 C66 -147.6(8) . . . . ? C52 C53 C59 C66 0.6(11) . . . . ? C41 C53 C59 C38 -6.6(13) . . . . ? C52 C53 C59 C38 141.7(9) . . . . ? C21 C38 C59 C53 -144.6(9) . . . . ? C40 C38 C59 C53 -0.3(14) . . . . ? C21 C38 C59 C66 1.5(10) . . . . ? C40 C38 C59 C66 145.8(8) . . . . ? C96 Si2 C95 Si1 -93.5(9) . . . . ? C111 Si2 C95 Si1 149.1(9) . . . . ? C17 Si2 C95 Si1 20.3(10) . . . . ? C88 Si1 C95 Si2 -118.7(8) . . . . ? C87 Si1 C95 Si2 122.7(8) . . . . ? C28 Si1 C95 Si2 -5.8(10) . . . . ? C38 C21 C60 C78 5.0(15) . . . . ? C51 C21 C60 C78 147.9(9) . . . . ? C38 C21 C60 C6 -148.1(9) . . . . ? C51 C21 C60 C6 -5.1(14) . . . . ? C11 C6 C60 C78 -151.4(9) . . . . ? C42 C6 C60 C78 -3.2(15) . . . . ? Ce2 C6 C60 C78 -76.8(9) . . . . ? C11 C6 C60 C21 3.0(14) . . . . ? C42 C6 C60 C21 151.1(9) . . . . ? Ce2 C6 C60 C21 77.6(9) . . . . ? C34 C23 C61 C65 -156.7(9) . . . . ? C46 C23 C61 C65 -6.2(14) . . . . ? Ce1 C23 C61 C65 -95.1(9) . . . . ? C34 C23 C61 C13 -6.5(10) . . . . ? C46 C23 C61 C13 144.1(8) . . . . ? Ce1 C23 C61 C13 55.1(7) . . . . ? C34 C23 C61 Ce1 -61.5(6) . . . . ? C46 C23 C61 Ce1 89.0(8) . . . . ? C52 C13 C61 C23 -144.6(8) . . . . ? C36 C13 C61 C23 4.4(10) . . . . ? Ce1 C13 C61 C23 -53.8(6) . . . . ? C52 C13 C61 C65 7.2(12) . . . . ? C36 C13 C61 C65 156.3(8) . . . . ? Ce1 C13 C61 C65 98.0(7) . . . . ? C52 C13 C61 Ce1 -90.8(7) . . . . ? C36 C13 C61 Ce1 58.3(6) . . . . ? C74 Ce1 C61 C23 26.1(6) . . . . ? C43 Ce1 C61 C23 45.3(7) . . . . ? C36 Ce1 C61 C23 84.8(7) . . . . ? C34 Ce1 C61 C23 38.1(6) . . . . ? C16 Ce1 C61 C23 97.9(6) . . . . ? C22 Ce1 C61 C23 80.1(6) . . . . ? C1 Ce1 C61 C23 -4.8(6) . . . . ? C33 Ce1 C61 C23 20.9(7) . . . . ? C13 Ce1 C61 C23 123.0(9) . . . . ? C41 Ce1 C61 C23 126.7(6) . . . . ? C63 Ce1 C61 C23 103.5(6) . . . . ? C74 Ce1 C61 C65 147.0(7) . . . . ? C43 Ce1 C61 C65 166.2(6) . . . . ? C36 Ce1 C61 C65 -154.3(8) . . . . ? C34 Ce1 C61 C65 159.0(8) . . . . ? C16 Ce1 C61 C65 -141.3(7) . . . . ? C22 Ce1 C61 C65 -159.1(6) . . . . ? C1 Ce1 C61 C65 116.1(7) . . . . ? C23 Ce1 C61 C65 120.9(10) . . . . ? C33 Ce1 C61 C65 141.7(6) . . . . ? C13 Ce1 C61 C65 -116.1(9) . . . . ? C41 Ce1 C61 C65 -112.5(7) . . . . ? C63 Ce1 C61 C65 -135.7(6) . . . . ? C74 Ce1 C61 C13 -96.9(6) . . . . ? C43 Ce1 C61 C13 -77.7(6) . . . . ? C36 Ce1 C61 C13 -38.2(6) . . . . ? C34 Ce1 C61 C13 -84.9(6) . . . . ? C16 Ce1 C61 C13 -25.1(6) . . . . ? C22 Ce1 C61 C13 -42.9(6) . . . . ? C1 Ce1 C61 C13 -127.8(6) . . . . ? C23 Ce1 C61 C13 -123.0(9) . . . . ? C33 Ce1 C61 C13 -102.1(6) . . . . ? C41 Ce1 C61 C13 3.7(6) . . . . ? C63 Ce1 C61 C13 -19.5(7) . . . . ? C8 C33 C62 C58 -8.3(12) . . . . ? C43 C33 C62 C58 -157.5(7) . . . . ? Ce1 C33 C62 C58 -99.6(7) . . . . ? C8 C33 C62 C1 147.2(7) . . . . ? C43 C33 C62 C1 -2.1(10) . . . . ? Ce1 C33 C62 C1 55.9(6) . . . . ? C8 C33 C62 Ce1 91.3(7) . . . . ? C43 C33 C62 Ce1 -57.9(6) . . . . ? C4 C58 C62 C33 1.0(11) . . . . ? C28 C58 C62 C33 164.2(8) . . . . ? C4 C58 C62 C1 -151.9(8) . . . . ? C28 C58 C62 C1 11.4(12) . . . . ? C4 C58 C62 Ce1 -76.7(7) . . . . ? C28 C58 C62 Ce1 86.6(8) . . . . ? C74 C1 C62 C33 2.9(10) . . . . ? C30 C1 C62 C33 -145.2(8) . . . . ? Ce1 C1 C62 C33 -56.7(7) . . . . ? C74 C1 C62 C58 159.3(8) . . . . ? C30 C1 C62 C58 11.2(12) . . . . ? Ce1 C1 C62 C58 99.6(7) . . . . ? C74 C1 C62 Ce1 59.6(6) . . . . ? C30 C1 C62 Ce1 -88.4(7) . . . . ? C74 Ce1 C62 C33 82.7(6) . . . . ? C43 Ce1 C62 C33 37.6(6) . . . . ? C36 Ce1 C62 C33 76.4(6) . . . . ? C34 Ce1 C62 C33 96.9(6) . . . . ? C16 Ce1 C62 C33 41.3(6) . . . . ? C22 Ce1 C62 C33 24.1(6) . . . . ? C1 Ce1 C62 C33 122.8(8) . . . . ? C23 Ce1 C62 C33 126.5(6) . . . . ? C13 Ce1 C62 C33 100.2(6) . . . . ? C41 Ce1 C62 C33 16.9(7) . . . . ? C63 Ce1 C62 C33 -4.8(6) . . . . ? C74 Ce1 C62 C58 -156.8(8) . . . . ? C43 Ce1 C62 C58 158.1(8) . . . . ? C36 Ce1 C62 C58 -163.1(6) . . . . ? C34 Ce1 C62 C58 -142.6(7) . . . . ? C16 Ce1 C62 C58 161.8(6) . . . . ? C22 Ce1 C62 C58 144.6(7) . . . . ? C1 Ce1 C62 C58 -116.7(9) . . . . ? C23 Ce1 C62 C58 -113.0(7) . . . . ? C33 Ce1 C62 C58 120.5(9) . . . . ? C13 Ce1 C62 C58 -139.3(6) . . . . ? C41 Ce1 C62 C58 137.4(6) . . . . ? C63 Ce1 C62 C58 115.7(7) . . . . ? C74 Ce1 C62 C1 -40.1(6) . . . . ? C43 Ce1 C62 C1 -85.2(6) . . . . ? C36 Ce1 C62 C1 -46.4(6) . . . . ? C34 Ce1 C62 C1 -25.9(6) . . . . ? C16 Ce1 C62 C1 -81.5(6) . . . . ? C22 Ce1 C62 C1 -98.7(6) . . . . ? C23 Ce1 C62 C1 3.7(6) . . . . ? C33 Ce1 C62 C1 -122.8(8) . . . . ? C13 Ce1 C62 C1 -22.6(7) . . . . ? C41 Ce1 C62 C1 -105.9(6) . . . . ? C63 Ce1 C62 C1 -127.6(6) . . . . ? C43 C22 C63 C15 5.6(14) . . . . ? C16 C22 C63 C15 144.1(9) . . . . ? Ce1 C22 C63 C15 72.5(9) . . . . ? C43 C22 C63 C35 -141.9(8) . . . . ? C16 C22 C63 C35 -3.4(11) . . . . ? Ce1 C22 C63 C35 -75.0(7) . . . . ? C43 C22 C63 Ce3 -61.0(10) . . . . ? C16 C22 C63 Ce3 77.5(9) . . . . ? Ce1 C22 C63 Ce3 5.9(6) . . . . ? C43 C22 C63 Ce1 -66.9(7) . . . . ? C16 C22 C63 Ce1 71.5(6) . . . . ? C68 C15 C63 C22 -156.1(9) . . . . ? C8 C15 C63 C22 -4.6(14) . . . . ? Ce3 C15 C63 C22 -95.0(10) . . . . ? C68 C15 C63 C35 -11.0(13) . . . . ? C8 C15 C63 C35 140.6(9) . . . . ? Ce3 C15 C63 C35 50.2(9) . . . . ? C68 C15 C63 Ce3 -61.2(8) . . . . ? C8 C15 C63 Ce3 90.4(9) . . . . ? C68 C15 C63 Ce1 -98.3(8) . . . . ? C8 C15 C63 Ce1 53.2(8) . . . . ? Ce3 C15 C63 Ce1 -37.1(6) . . . . ? C40 C35 C63 C22 155.9(10) . . . . ? C41 C35 C63 C22 5.2(11) . . . . ? Ce3 C35 C63 C22 107.1(8) . . . . ? C40 C35 C63 C15 5.6(14) . . . . ? C41 C35 C63 C15 -145.1(8) . . . . ? Ce3 C35 C63 C15 -43.3(8) . . . . ? C40 C35 C63 Ce3 48.8(10) . . . . ? C41 C35 C63 Ce3 -101.8(8) . . . . ? C40 C35 C63 Ce1 96.8(9) . . . . ? C41 C35 C63 Ce1 -53.8(7) . . . . ? Ce3 C35 C63 Ce1 48.0(4) . . . . ? C74 Ce1 C63 C22 25.7(5) . . . . ? C43 Ce1 C63 C22 35.5(5) . . . . ? C36 Ce1 C63 C22 -35.5(5) . . . . ? C34 Ce1 C63 C22 -5.6(5) . . . . ? C16 Ce1 C63 C22 -42.6(5) . . . . ? C1 Ce1 C63 C22 51.7(5) . . . . ? C23 Ce1 C63 C22 -12.4(6) . . . . ? C33 Ce1 C63 C22 72.7(5) . . . . ? C13 Ce1 C63 C22 -59.3(5) . . . . ? C41 Ce1 C63 C22 -82.1(6) . . . . ? C74 Ce1 C63 C15 -102.9(6) . . . . ? C43 Ce1 C63 C15 -93.1(7) . . . . ? C36 Ce1 C63 C15 -164.2(7) . . . . ? C34 Ce1 C63 C15 -134.3(6) . . . . ? C16 Ce1 C63 C15 -171.2(8) . . . . ? C22 Ce1 C63 C15 -128.7(9) . . . . ? C1 Ce1 C63 C15 -76.9(7) . . . . ? C23 Ce1 C63 C15 -141.1(6) . . . . ? C33 Ce1 C63 C15 -56.0(6) . . . . ? C13 Ce1 C63 C15 172.0(6) . . . . ? C41 Ce1 C63 C15 149.3(8) . . . . ? C74 Ce1 C63 C35 139.8(6) . . . . ? C43 Ce1 C63 C35 149.6(7) . . . . ? C36 Ce1 C63 C35 78.5(6) . . . . ? C34 Ce1 C63 C35 108.4(6) . . . . ? C16 Ce1 C63 C35 71.4(6) . . . . ? C22 Ce1 C63 C35 114.0(8) . . . . ? C1 Ce1 C63 C35 165.8(6) . . . . ? C23 Ce1 C63 C35 101.6(6) . . . . ? C33 Ce1 C63 C35 -173.3(7) . . . . ? C13 Ce1 C63 C35 54.7(6) . . . . ? C41 Ce1 C63 C35 32.0(6) . . . . ? C74 Ce1 C63 Ce3 -146.9(5) . . . . ? C43 Ce1 C63 Ce3 -137.1(6) . . . . ? C36 Ce1 C63 Ce3 151.8(5) . . . . ? C34 Ce1 C63 Ce3 -178.2(5) . . . . ? C16 Ce1 C63 Ce3 144.8(6) . . . . ? C22 Ce1 C63 Ce3 -172.6(7) . . . . ? C1 Ce1 C63 Ce3 -120.9(5) . . . . ? C23 Ce1 C63 Ce3 174.9(5) . . . . ? C33 Ce1 C63 Ce3 -100.0(5) . . . . ? C13 Ce1 C63 Ce3 128.1(5) . . . . ? C41 Ce1 C63 Ce3 105.3(6) . . . . ? C6 C42 C64 C75 2.2(11) . . . . ? C44 C42 C64 C75 -141.7(9) . . . . ? Ce2 C42 C64 C75 -71.5(7) . . . . ? C6 C42 C64 C14 141.6(9) . . . . ? C44 C42 C64 C14 -2.3(14) . . . . ? Ce2 C42 C64 C14 68.0(7) . . . . ? C6 C42 C64 Ce2 73.6(7) . . . . ? C44 C42 C64 Ce2 -70.2(9) . . . . ? C2 C14 C64 C75 135.2(10) . . . . ? C12 C14 C64 C75 -0.9(14) . . . . ? Ce2 C14 C64 C75 59.5(8) . . . . ? C2 C14 C64 C42 -0.1(13) . . . . ? C12 C14 C64 C42 -136.2(9) . . . . ? Ce2 C14 C64 C42 -75.8(8) . . . . ? C2 C14 C64 Ce2 75.8(7) . . . . ? C12 C14 C64 Ce2 -60.4(8) . . . . ? C14 Ce2 C64 C75 -128.3(9) . . . . ? C12 Ce2 C64 C75 -97.1(7) . . . . ? C57 Ce2 C64 C75 -62.7(6) . . . . ? C55 Ce2 C64 C75 -28.5(6) . . . . ? C5 Ce2 C64 C75 -116.7(6) . . . . ? C2 Ce2 C64 C75 -160.5(8) . . . . ? C42 Ce2 C64 C75 111.0(8) . . . . ? C11 Ce2 C64 C75 38.3(6) . . . . ? C32 Ce2 C64 C75 -59.5(7) . . . . ? C3 Ce2 C64 C75 -13.3(6) . . . . ? C14 Ce2 C64 C42 120.7(8) . . . . ? C12 Ce2 C64 C42 151.9(6) . . . . ? C75 Ce2 C64 C42 -111.0(8) . . . . ? C57 Ce2 C64 C42 -173.7(5) . . . . ? C55 Ce2 C64 C42 -139.5(6) . . . . ? C5 Ce2 C64 C42 132.3(5) . . . . ? C2 Ce2 C64 C42 88.5(5) . . . . ? C11 Ce2 C64 C42 -72.7(5) . . . . ? C32 Ce2 C64 C42 -170.5(5) . . . . ? C3 Ce2 C64 C42 -124.3(5) . . . . ? C12 Ce2 C64 C14 31.2(5) . . . . ? C75 Ce2 C64 C14 128.3(9) . . . . ? C57 Ce2 C64 C14 65.6(6) . . . . ? C55 Ce2 C64 C14 99.8(6) . . . . ? C5 Ce2 C64 C14 11.7(5) . . . . ? C2 Ce2 C64 C14 -32.2(5) . . . . ? C42 Ce2 C64 C14 -120.7(8) . . . . ? C11 Ce2 C64 C14 166.7(7) . . . . ? C32 Ce2 C64 C14 68.8(6) . . . . ? C3 Ce2 C64 C14 115.0(6) . . . . ? C109 C82 C96 C99 0.1(12) . . . . ? C79 C82 C96 C99 -179.1(8) . . . . ? C109 C82 C96 Si2 -179.0(7) . . . . ? C79 C82 C96 Si2 1.9(11) . . . . ? C95 Si2 C96 C99 14.1(9) . . . . ? C111 Si2 C96 C99 127.8(8) . . . . ? C17 Si2 C96 C99 -99.5(8) . . . . ? C95 Si2 C96 C82 -166.9(6) . . . . ? C111 Si2 C96 C82 -53.2(7) . . . . ? C17 Si2 C96 C82 79.5(7) . . . . ? C23 C61 C65 C27 -2.8(14) . . . . ? C13 C61 C65 C27 -149.7(8) . . . . ? Ce1 C61 C65 C27 -75.3(9) . . . . ? C23 C61 C65 C37 149.0(9) . . . . ? C13 C61 C65 C37 2.0(11) . . . . ? Ce1 C61 C65 C37 76.4(8) . . . . ? C72 C27 C65 C61 147.5(9) . . . . ? C77 C27 C65 C61 4.2(13) . . . . ? Ce4 C27 C65 C61 90.3(9) . . . . ? C72 C27 C65 C37 -3.9(12) . . . . ? C77 C27 C65 C37 -147.1(8) . . . . ? Ce4 C27 C65 C37 -61.1(8) . . . . ? C39 C37 C65 C61 -147.4(8) . . . . ? C45 C37 C65 C61 -4.9(12) . . . . ? C39 C37 C65 C27 3.7(12) . . . . ? C45 C37 C65 C27 146.2(8) . . . . ? C108 C90 C97 C87 -4.7(14) . . . . ? C108 C90 C97 C91 175.1(9) . . . . ? C84 C87 C97 C90 3.7(13) . . . . ? Si1 C87 C97 C90 -172.5(7) . . . . ? C84 C87 C97 C91 -176.1(10) . . . . ? Si1 C87 C97 C91 7.7(12) . . . . ? C82 C96 C99 C110 3.4(12) . . . . ? Si2 C96 C99 C110 -177.6(7) . . . . ? C82 C96 C99 C80 -179.9(8) . . . . ? Si2 C96 C99 C80 -0.9(12) . . . . ? C47 C51 C66 C67 2.4(12) . . . . ? C21 C51 C66 C67 148.2(8) . . . . ? C47 C51 C66 C59 -145.3(8) . . . . ? C21 C51 C66 C59 0.5(10) . . . . ? C53 C59 C66 C67 -3.0(12) . . . . ? C38 C59 C66 C67 -149.8(8) . . . . ? C53 C59 C66 C51 145.6(8) . . . . ? C38 C59 C66 C51 -1.2(9) . . . . ? C51 C66 C67 C25 -2.0(12) . . . . ? C59 C66 C67 C25 142.2(8) . . . . ? C51 C66 C67 C45 -140.8(8) . . . . ? C59 C66 C67 C45 3.4(12) . . . . ? C48 C25 C67 C66 -0.7(12) . . . . ? C39 C25 C67 C66 -146.7(7) . . . . ? C48 C25 C67 C45 142.2(8) . . . . ? C39 C25 C67 C45 -3.8(8) . . . . ? C52 C45 C67 C66 -1.4(12) . . . . ? C37 C45 C67 C66 145.0(8) . . . . ? C52 C45 C67 C25 -143.5(7) . . . . ? C37 C45 C67 C25 3.0(8) . . . . ? C63 C15 C68 C76 9.4(14) . . . . ? C8 C15 C68 C76 -141.1(9) . . . . ? Ce3 C15 C68 C76 -60.8(9) . . . . ? C63 C15 C68 C69 150.5(8) . . . . ? C8 C15 C68 C69 0.0(13) . . . . ? Ce3 C15 C68 C69 80.3(9) . . . . ? C63 C15 C68 Ce3 70.2(9) . . . . ? C8 C15 C68 Ce3 -80.3(9) . . . . ? C83 C89 C100 C111 -0.7(17) . . . . ? C83 C89 C100 C113 178.9(11) . . . . ? C7 C10 C69 C49 -1.6(12) . . . . ? C54 C10 C69 C49 140.4(9) . . . . ? Ce3 C10 C69 C49 91.2(9) . . . . ? C7 C10 C69 C68 -142.1(9) . . . . ? C54 C10 C69 C68 0.0(12) . . . . ? Ce3 C10 C69 C68 -49.2(8) . . . . ? C7 C10 C69 Ce3 -92.8(9) . . . . ? C54 C10 C69 Ce3 49.2(9) . . . . ? C44 C49 C69 C10 -0.7(13) . . . . ? C78 C49 C69 C10 -149.3(8) . . . . ? Ce3 C49 C69 C10 -93.6(9) . . . . ? C44 C49 C69 C68 143.6(9) . . . . ? C78 C49 C69 C68 -5.0(11) . . . . ? Ce3 C49 C69 C68 50.7(7) . . . . ? C44 C49 C69 Ce3 92.9(9) . . . . ? C78 C49 C69 Ce3 -55.7(8) . . . . ? C15 C68 C69 C10 0.0(13) . . . . ? C76 C68 C69 C10 146.1(9) . . . . ? Ce3 C68 C69 C10 69.6(9) . . . . ? C15 C68 C69 C49 -143.1(9) . . . . ? C76 C68 C69 C49 3.0(11) . . . . ? Ce3 C68 C69 C49 -73.5(9) . . . . ? C15 C68 C69 Ce3 -69.6(9) . . . . ? C76 C68 C69 Ce3 76.5(8) . . . . ? C77 C50 C70 C24 -4.1(14) . . . . ? C73 C50 C70 C24 -143.8(9) . . . . ? Ce4 C50 C70 C24 -95.0(9) . . . . ? C77 C50 C70 C26 140.3(9) . . . . ? C73 C50 C70 C26 0.5(13) . . . . ? Ce4 C50 C70 C26 49.4(9) . . . . ? C77 C50 C70 Ce4 90.9(9) . . . . ? C73 C50 C70 Ce4 -48.9(8) . . . . ? C30 C24 C70 C50 7.8(14) . . . . ? C28 C24 C70 C50 157.4(8) . . . . ? C30 C24 C70 C26 -139.1(8) . . . . ? C28 C24 C70 C26 10.5(10) . . . . ? C30 C24 C70 Ce4 -56.7(10) . . . . ? C28 C24 C70 Ce4 92.9(7) . . . . ? C71 C26 C70 C50 -0.2(13) . . . . ? C29 C26 C70 C50 -148.6(8) . . . . ? Ce4 C26 C70 C50 -41.9(8) . . . . ? C71 C26 C70 C24 147.5(8) . . . . ? C29 C26 C70 C24 -0.9(9) . . . . ? Ce4 C26 C70 C24 105.8(7) . . . . ? C71 C26 C70 Ce4 41.7(8) . . . . ? C29 C26 C70 Ce4 -106.7(7) . . . . ? C89 C83 C102 C103 -1.1(17) . . . . ? C114 C83 C102 C103 178.2(10) . . . . ? C83 C102 C103 C111 0.9(17) . . . . ? C83 C102 C103 C107 -179.4(10) . . . . ? C87 C84 C105 C108 0.6(15) . . . . ? C98 C84 C105 C108 -179.5(9) . . . . ? C70 C26 C71 C5 -151.0(8) . . . . ? C29 C26 C71 C5 -8.0(12) . . . . ? Ce4 C26 C71 C5 -104.2(9) . . . . ? C70 C26 C71 C18 -0.2(13) . . . . ? C29 C26 C71 C18 142.8(9) . . . . ? Ce4 C26 C71 C18 46.6(8) . . . . ? C70 C26 C71 Ce4 -46.8(9) . . . . ? C29 C26 C71 Ce4 96.2(9) . . . . ? C12 C5 C71 C26 157.7(9) . . . . ? C31 C5 C71 C26 12.4(12) . . . . ? Ce2 C5 C71 C26 95.9(7) . . . . ? C12 C5 C71 C18 6.2(14) . . . . ? C31 C5 C71 C18 -139.1(9) . . . . ? Ce2 C5 C71 C18 -55.7(8) . . . . ? C12 C5 C71 Ce4 62.1(11) . . . . ? C31 C5 C71 Ce4 -83.2(9) . . . . ? Ce2 C5 C71 Ce4 0.3(5) . . . . ? C73 C18 C71 C26 0.1(13) . . . . ? C32 C18 C71 C26 -149.3(9) . . . . ? Ce4 C18 C71 C26 -64.0(10) . . . . ? C73 C18 C71 C5 150.3(9) . . . . ? C32 C18 C71 C5 1.0(13) . . . . ? Ce4 C18 C71 C5 86.3(10) . . . . ? C73 C18 C71 Ce4 64.1(9) . . . . ? C32 C18 C71 Ce4 -85.3(9) . . . . ? C39 C56 C72 C27 8.0(12) . . . . ? C20 C56 C72 C27 -143.2(9) . . . . ? Ce4 C56 C72 C27 -88.2(9) . . . . ? C39 C56 C72 C73 146.2(9) . . . . ? C20 C56 C72 C73 -5.0(13) . . . . ? Ce4 C56 C72 C73 50.0(8) . . . . ? C39 C56 C72 Ce4 96.1(8) . . . . ? C20 C56 C72 Ce4 -55.0(9) . . . . ? C65 C27 C72 C56 -2.2(13) . . . . ? C77 C27 C72 C56 144.2(9) . . . . ? Ce4 C27 C72 C56 81.4(9) . . . . ? C65 C27 C72 C73 -143.7(8) . . . . ? C77 C27 C72 C73 2.7(11) . . . . ? Ce4 C27 C72 C73 -60.1(7) . . . . ? C65 C27 C72 Ce4 -83.6(9) . . . . ? C77 C27 C72 Ce4 62.8(9) . . . . ? C92 C94 C106 C85 1.6(12) . . . . ? C112 C94 C106 C85 -178.3(8) . . . . ? C88 C85 C106 C94 -4.1(12) . . . . ? C93 C85 C106 C94 177.3(8) . . . . ? C32 C18 C73 C50 150.0(9) . . . . ? C71 C18 C73 C50 0.2(15) . . . . ? Ce4 C18 C73 C50 78.8(10) . . . . ? C32 C18 C73 C72 8.0(14) . . . . ? C71 C18 C73 C72 -141.8(9) . . . . ? Ce4 C18 C73 C72 -63.3(10) . . . . ? C32 C18 C73 Ce4 71.3(9) . . . . ? C71 C18 C73 Ce4 -78.5(9) . . . . ? C70 C50 C73 C18 -0.6(14) . . . . ? C77 C50 C73 C18 -143.4(10) . . . . ? Ce4 C50 C73 C18 -69.8(10) . . . . ? C70 C50 C73 C72 147.4(8) . . . . ? C77 C50 C73 C72 4.6(10) . . . . ? Ce4 C50 C73 C72 78.2(8) . . . . ? C70 C50 C73 Ce4 69.2(9) . . . . ? C77 C50 C73 Ce4 -73.6(8) . . . . ? C56 C72 C73 C18 0.5(14) . . . . ? C27 C72 C73 C18 143.2(9) . . . . ? Ce4 C72 C73 C18 60.6(10) . . . . ? C56 C72 C73 C50 -147.0(8) . . . . ? C27 C72 C73 C50 -4.4(11) . . . . ? Ce4 C72 C73 C50 -87.0(8) . . . . ? C56 C72 C73 Ce4 -60.1(9) . . . . ? C27 C72 C73 Ce4 82.5(9) . . . . ? C22 C43 C74 C1 -139.7(9) . . . . ? C33 C43 C74 C1 1.5(10) . . . . ? Ce1 C43 C74 C1 -78.7(7) . . . . ? C22 C43 C74 C34 -1.5(15) . . . . ? C33 C43 C74 C34 139.7(9) . . . . ? Ce1 C43 C74 C34 59.5(9) . . . . ? C22 C43 C74 Ce1 -61.0(9) . . . . ? C33 C43 C74 Ce1 80.2(6) . . . . ? C62 C1 C74 C43 -2.6(10) . . . . ? C30 C1 C74 C43 142.4(9) . . . . ? Ce1 C1 C74 C43 70.9(7) . . . . ? C62 C1 C74 C34 -143.7(9) . . . . ? C30 C1 C74 C34 1.3(14) . . . . ? Ce1 C1 C74 C34 -70.2(7) . . . . ? C62 C1 C74 Ce1 -73.5(6) . . . . ? C30 C1 C74 Ce1 71.5(10) . . . . ? C23 C34 C74 C43 -130.4(10) . . . . ? C36 C34 C74 C43 -0.5(14) . . . . ? Ce1 C34 C74 C43 -59.2(9) . . . . ? C23 C34 C74 C1 5.6(14) . . . . ? C36 C34 C74 C1 135.5(9) . . . . ? Ce1 C34 C74 C1 76.8(8) . . . . ? C23 C34 C74 Ce1 -71.2(9) . . . . ? C36 C34 C74 Ce1 58.7(7) . . . . ? C36 Ce1 C74 C43 98.3(6) . . . . ? C34 Ce1 C74 C43 130.3(8) . . . . ? C16 Ce1 C74 C43 63.5(5) . . . . ? C22 Ce1 C74 C43 28.4(5) . . . . ? C1 Ce1 C74 C43 -111.8(7) . . . . ? C23 Ce1 C74 C43 160.5(6) . . . . ? C33 Ce1 C74 C43 -38.5(5) . . . . ? C13 Ce1 C74 C43 117.5(5) . . . . ? C41 Ce1 C74 C43 59.6(5) . . . . ? C63 Ce1 C74 C43 14.1(5) . . . . ? C43 Ce1 C74 C1 111.8(7) . . . . ? C36 Ce1 C74 C1 -149.9(7) . . . . ? C34 Ce1 C74 C1 -117.9(9) . . . . ? C16 Ce1 C74 C1 175.3(6) . . . . ? C22 Ce1 C74 C1 140.2(6) . . . . ? C23 Ce1 C74 C1 -87.7(6) . . . . ? C33 Ce1 C74 C1 73.2(5) . . . . ? C13 Ce1 C74 C1 -130.7(6) . . . . ? C41 Ce1 C74 C1 171.4(5) . . . . ? C63 Ce1 C74 C1 125.9(6) . . . . ? C43 Ce1 C74 C34 -130.3(8) . . . . ? C36 Ce1 C74 C34 -32.1(5) . . . . ? C16 Ce1 C74 C34 -66.8(6) . . . . ? C22 Ce1 C74 C34 -101.9(6) . . . . ? C1 Ce1 C74 C34 117.9(9) . . . . ? C23 Ce1 C74 C34 30.2(5) . . . . ? C33 Ce1 C74 C34 -168.9(7) . . . . ? C13 Ce1 C74 C34 -12.8(6) . . . . ? C41 Ce1 C74 C34 -70.7(6) . . . . ? C63 Ce1 C74 C34 -116.2(6) . . . . ? C84 C105 C108 C90 -1.3(15) . . . . ? C84 C105 C108 C101 177.0(10) . . . . ? C97 C90 C108 C105 3.4(14) . . . . ? C97 C90 C108 C101 -175.0(9) . . . . ? C96 C82 C109 C104 -3.6(13) . . . . ? C79 C82 C109 C104 175.6(8) . . . . ? C110 C104 C109 C82 3.7(14) . . . . ? C115 C104 C109 C82 179.1(9) . . . . ? C80 C99 C110 C104 179.8(8) . . . . ? C96 C99 C110 C104 -3.4(13) . . . . ? C109 C104 C110 C99 -0.2(14) . . . . ? C115 C104 C110 C99 -175.9(9) . . . . ? C89 C100 C111 C103 0.5(15) . . . . ? C113 C100 C111 C103 -179.1(10) . . . . ? C89 C100 C111 Si2 -174.7(8) . . . . ? C113 C100 C111 Si2 5.7(15) . . . . ? C102 C103 C111 C100 -0.7(16) . . . . ? C107 C103 C111 C100 179.7(10) . . . . ? C102 C103 C111 Si2 174.0(9) . . . . ? C107 C103 C111 Si2 -5.7(16) . . . . ? C96 Si2 C111 C100 -60.1(9) . . . . ? C95 Si2 C111 C100 65.0(9) . . . . ? C17 Si2 C111 C100 179.1(7) . . . . ? C96 Si2 C111 C103 125.2(10) . . . . ? C95 Si2 C111 C103 -109.7(10) . . . . ? C17 Si2 C111 C103 4.4(12) . . . . ? C57 C55 C75 C64 -2.1(16) . . . . ? C3 C55 C75 C64 -135.5(10) . . . . ? Ce2 C55 C75 C64 -58.8(9) . . . . ? C57 C55 C75 C11 134.8(10) . . . . ? C3 C55 C75 C11 1.4(13) . . . . ? Ce2 C55 C75 C11 78.1(8) . . . . ? C57 C55 C75 Ce2 56.7(9) . . . . ? C3 C55 C75 Ce2 -76.7(7) . . . . ? C42 C64 C75 C55 140.1(10) . . . . ? C14 C64 C75 C55 1.2(15) . . . . ? Ce2 C64 C75 C55 60.0(9) . . . . ? C42 C64 C75 C11 -0.4(11) . . . . ? C14 C64 C75 C11 -139.3(9) . . . . ? Ce2 C64 C75 C11 -80.5(7) . . . . ? C42 C64 C75 Ce2 80.0(7) . . . . ? C14 C64 C75 Ce2 -58.8(8) . . . . ? C6 C11 C75 C55 -144.1(9) . . . . ? C47 C11 C75 C55 3.2(14) . . . . ? Ce2 C11 C75 C55 -71.7(8) . . . . ? C6 C11 C75 C64 -1.5(11) . . . . ? C47 C11 C75 C64 145.8(9) . . . . ? Ce2 C11 C75 C64 70.9(7) . . . . ? C6 C11 C75 Ce2 -72.4(7) . . . . ? C47 C11 C75 Ce2 74.9(9) . . . . ? C14 Ce2 C75 C55 -99.9(6) . . . . ? C64 Ce2 C75 C55 -130.6(9) . . . . ? C12 Ce2 C75 C55 -63.3(6) . . . . ? C57 Ce2 C75 C55 -28.3(5) . . . . ? C5 Ce2 C75 C55 -65.1(6) . . . . ? C2 Ce2 C75 C55 -114.6(6) . . . . ? C42 Ce2 C75 C55 -168.2(7) . . . . ? C11 Ce2 C75 C55 119.6(8) . . . . ? C32 Ce2 C75 C55 -9.1(5) . . . . ? C3 Ce2 C75 C55 33.0(5) . . . . ? C14 Ce2 C75 C64 30.8(6) . . . . ? C12 Ce2 C75 C64 67.3(6) . . . . ? C57 Ce2 C75 C64 102.4(7) . . . . ? C55 Ce2 C75 C64 130.6(9) . . . . ? C5 Ce2 C75 C64 65.5(7) . . . . ? C2 Ce2 C75 C64 16.0(6) . . . . ? C42 Ce2 C75 C64 -37.6(6) . . . . ? C11 Ce2 C75 C64 -109.8(9) . . . . ? C32 Ce2 C75 C64 121.6(7) . . . . ? C3 Ce2 C75 C64 163.6(8) . . . . ? C14 Ce2 C75 C11 140.6(7) . . . . ? C64 Ce2 C75 C11 109.8(9) . . . . ? C12 Ce2 C75 C11 177.1(6) . . . . ? C57 Ce2 C75 C11 -147.8(6) . . . . ? C55 Ce2 C75 C11 -119.6(8) . . . . ? C5 Ce2 C75 C11 175.3(5) . . . . ? C2 Ce2 C75 C11 125.9(6) . . . . ? C42 Ce2 C75 C11 72.2(6) . . . . ? C32 Ce2 C75 C11 -128.6(6) . . . . ? C3 Ce2 C75 C11 -86.6(6) . . . . ? C35 C40 C76 C68 -4.1(15) . . . . ? C38 C40 C76 C68 146.8(9) . . . . ? Ce3 C40 C76 C68 52.5(9) . . . . ? C35 C40 C76 C78 -148.1(10) . . . . ? C38 C40 C76 C78 2.7(14) . . . . ? Ce3 C40 C76 C78 -91.6(10) . . . . ? C35 C40 C76 Ce3 -56.6(10) . . . . ? C38 C40 C76 Ce3 94.3(10) . . . . ? C15 C68 C76 C40 -1.7(15) . . . . ? C69 C68 C76 C40 -147.6(9) . . . . ? Ce3 C68 C76 C40 -60.2(11) . . . . ? C15 C68 C76 C78 146.3(9) . . . . ? C69 C68 C76 C78 0.3(11) . . . . ? Ce3 C68 C76 C78 87.8(10) . . . . ? C15 C68 C76 Ce3 58.5(10) . . . . ? C69 C68 C76 Ce3 -87.5(9) . . . . ? C30 C46 C77 C50 2.3(14) . . . . ? C23 C46 C77 C50 -150.4(9) . . . . ? C30 C46 C77 C27 140.8(9) . . . . ? C23 C46 C77 C27 -11.9(13) . . . . ? C30 C46 C77 Ce4 66.2(10) . . . . ? C23 C46 C77 Ce4 -86.5(8) . . . . ? C70 C50 C77 C46 -1.0(14) . . . . ? C73 C50 C77 C46 141.6(9) . . . . ? Ce4 C50 C77 C46 91.0(10) . . . . ? C70 C50 C77 C27 -145.6(8) . . . . ? C73 C50 C77 C27 -3.0(10) . . . . ? Ce4 C50 C77 C27 -53.6(7) . . . . ? C70 C50 C77 Ce4 -91.9(9) . . . . ? C73 C50 C77 Ce4 50.6(7) . . . . ? C72 C27 C77 C46 -143.8(9) . . . . ? C65 C27 C77 C46 3.4(14) . . . . ? Ce4 C27 C77 C46 -95.6(9) . . . . ? C72 C27 C77 C50 0.1(11) . . . . ? C65 C27 C77 C50 147.3(9) . . . . ? Ce4 C27 C77 C50 48.3(7) . . . . ? C72 C27 C77 Ce4 -48.2(7) . . . . ? C65 C27 C77 Ce4 99.0(9) . . . . ? C21 C60 C78 C76 -8.4(14) . . . . ? C6 C60 C78 C76 144.6(9) . . . . ? C21 C60 C78 C49 -143.2(10) . . . . ? C6 C60 C78 C49 9.7(14) . . . . ? C21 C60 C78 Ce3 -60.1(10) . . . . ? C6 C60 C78 Ce3 92.8(10) . . . . ? C40 C76 C78 C60 4.4(15) . . . . ? C68 C76 C78 C60 -143.3(9) . . . . ? Ce3 C76 C78 C60 -78.3(9) . . . . ? C40 C76 C78 C49 144.4(9) . . . . ? C68 C76 C78 C49 -3.4(11) . . . . ? Ce3 C76 C78 C49 61.7(8) . . . . ? C40 C76 C78 Ce3 82.7(10) . . . . ? C68 C76 C78 Ce3 -65.0(7) . . . . ? C44 C49 C78 C60 -3.8(15) . . . . ? C69 C49 C78 C60 144.1(10) . . . . ? Ce3 C49 C78 C60 93.9(10) . . . . ? C44 C49 C78 C76 -142.9(10) . . . . ? C69 C49 C78 C76 5.0(11) . . . . ? Ce3 C49 C78 C76 -45.2(8) . . . . ? C44 C49 C78 Ce3 -97.7(10) . . . . ? C69 C49 C78 Ce3 50.2(8) . . . . ? C76 C68 Ce3 C15 130.2(9) . . . . ? C69 C68 Ce3 C15 -122.7(8) . . . . ? C15 C68 Ce3 C76 -130.2(9) . . . . ? C69 C68 Ce3 C76 107.1(9) . . . . ? C15 C68 Ce3 C63 -32.6(5) . . . . ? C76 C68 Ce3 C63 97.6(7) . . . . ? C69 C68 Ce3 C63 -155.3(7) . . . . ? C15 C68 Ce3 C40 -101.7(7) . . . . ? C76 C68 Ce3 C40 28.5(6) . . . . ? C69 C68 Ce3 C40 135.5(7) . . . . ? C15 C68 Ce3 C35 -68.5(6) . . . . ? C76 C68 Ce3 C35 61.8(6) . . . . ? C69 C68 Ce3 C35 168.8(7) . . . . ? C15 C68 Ce3 C69 122.7(8) . . . . ? C76 C68 Ce3 C69 -107.1(9) . . . . ? C15 C68 Ce3 C8 32.6(5) . . . . ? C76 C68 Ce3 C8 162.8(8) . . . . ? C69 C68 Ce3 C8 -90.1(6) . . . . ? C15 C68 Ce3 C78 -166.8(7) . . . . ? C76 C68 Ce3 C78 -36.6(5) . . . . ? C69 C68 Ce3 C78 70.5(6) . . . . ? C15 C68 Ce3 C49 156.1(7) . . . . ? C76 C68 Ce3 C49 -73.7(6) . . . . ? C69 C68 Ce3 C49 33.4(5) . . . . ? C15 C68 Ce3 C54 64.8(5) . . . . ? C76 C68 Ce3 C54 -165.0(8) . . . . ? C69 C68 Ce3 C54 -58.0(6) . . . . ? C15 C68 Ce3 C10 95.0(6) . . . . ? C76 C68 Ce3 C10 -134.7(8) . . . . ? C69 C68 Ce3 C10 -27.7(5) . . . . ? C63 C15 Ce3 C68 -123.5(8) . . . . ? C8 C15 Ce3 C68 120.7(9) . . . . ? C68 C15 Ce3 C76 30.6(5) . . . . ? C63 C15 Ce3 C76 -92.9(7) . . . . ? C8 C15 Ce3 C76 151.3(8) . . . . ? C68 C15 Ce3 C63 123.5(8) . . . . ? C8 C15 Ce3 C63 -115.8(9) . . . . ? C68 C15 Ce3 C40 66.2(6) . . . . ? C63 C15 Ce3 C40 -57.3(7) . . . . ? C8 C15 Ce3 C40 -173.1(7) . . . . ? C68 C15 Ce3 C35 96.9(6) . . . . ? C63 C15 Ce3 C35 -26.5(6) . . . . ? C8 C15 Ce3 C35 -142.3(7) . . . . ? C68 C15 Ce3 C69 -32.0(5) . . . . ? C63 C15 Ce3 C69 -155.5(7) . . . . ? C8 C15 Ce3 C69 88.7(7) . . . . ? C68 C15 Ce3 C8 -120.7(9) . . . . ? C63 C15 Ce3 C8 115.8(9) . . . . ? C68 C15 Ce3 C78 10.9(6) . . . . ? C63 C15 Ce3 C78 -112.6(7) . . . . ? C8 C15 Ce3 C78 131.7(7) . . . . ? C68 C15 Ce3 C49 -19.1(5) . . . . ? C63 C15 Ce3 C49 -142.5(7) . . . . ? C8 C15 Ce3 C49 101.7(7) . . . . ? C68 C15 Ce3 C54 -91.9(6) . . . . ? C63 C15 Ce3 C54 144.6(7) . . . . ? C8 C15 Ce3 C54 28.8(5) . . . . ? C68 C15 Ce3 C10 -63.1(6) . . . . ? C63 C15 Ce3 C10 173.4(7) . . . . ? C8 C15 Ce3 C10 57.7(6) . . . . ? C40 C76 Ce3 C68 131.0(10) . . . . ? C78 C76 Ce3 C68 -108.2(9) . . . . ? C40 C76 Ce3 C15 99.5(7) . . . . ? C68 C76 Ce3 C15 -31.5(6) . . . . ? C78 C76 Ce3 C15 -139.7(7) . . . . ? C40 C76 Ce3 C63 62.1(6) . . . . ? C68 C76 Ce3 C63 -68.9(7) . . . . ? C78 C76 Ce3 C63 -177.1(6) . . . . ? C68 C76 Ce3 C40 -131.0(10) . . . . ? C78 C76 Ce3 C40 120.8(8) . . . . ? C40 C76 Ce3 C35 27.9(6) . . . . ? C68 C76 Ce3 C35 -103.1(8) . . . . ? C78 C76 Ce3 C35 148.7(6) . . . . ? C40 C76 Ce3 C69 171.1(8) . . . . ? C68 C76 Ce3 C69 40.1(6) . . . . ? C78 C76 Ce3 C69 -68.1(6) . . . . ? C40 C76 Ce3 C8 115.4(8) . . . . ? C68 C76 Ce3 C8 -15.6(7) . . . . ? C78 C76 Ce3 C8 -123.8(7) . . . . ? C40 C76 Ce3 C78 -120.8(8) . . . . ? C68 C76 Ce3 C78 108.2(9) . . . . ? C40 C76 Ce3 C49 -153.3(7) . . . . ? C68 C76 Ce3 C49 75.8(7) . . . . ? C78 C76 Ce3 C49 -32.5(5) . . . . ? C40 C76 Ce3 C54 145.0(8) . . . . ? C68 C76 Ce3 C54 14.0(7) . . . . ? C78 C76 Ce3 C54 -94.2(8) . . . . ? C40 C76 Ce3 C10 167.0(7) . . . . ? C68 C76 Ce3 C10 36.1(6) . . . . ? C78 C76 Ce3 C10 -72.2(6) . . . . ? C22 C63 Ce3 C68 155.6(7) . . . . ? C15 C63 Ce3 C68 36.1(6) . . . . ? C35 C63 Ce3 C68 -99.0(7) . . . . ? Ce1 C63 Ce3 C68 162.6(6) . . . . ? C22 C63 Ce3 C15 119.5(9) . . . . ? C35 C63 Ce3 C15 -135.1(10) . . . . ? Ce1 C63 Ce3 C15 126.4(7) . . . . ? C22 C63 Ce3 C76 -164.5(7) . . . . ? C15 C63 Ce3 C76 76.1(7) . . . . ? C35 C63 Ce3 C76 -59.1(6) . . . . ? Ce1 C63 Ce3 C76 -157.5(6) . . . . ? C22 C63 Ce3 C40 -129.2(7) . . . . ? C15 C63 Ce3 C40 111.3(8) . . . . ? C35 C63 Ce3 C40 -23.8(6) . . . . ? Ce1 C63 Ce3 C40 -122.2(5) . . . . ? C22 C63 Ce3 C35 -105.4(8) . . . . ? C15 C63 Ce3 C35 135.1(10) . . . . ? Ce1 C63 Ce3 C35 -98.4(6) . . . . ? C22 C63 Ce3 C69 141.7(7) . . . . ? C15 C63 Ce3 C69 22.2(7) . . . . ? C35 C63 Ce3 C69 -112.9(7) . . . . ? Ce1 C63 Ce3 C69 148.7(7) . . . . ? C22 C63 Ce3 C8 83.1(7) . . . . ? C15 C63 Ce3 C8 -36.4(6) . . . . ? C35 C63 Ce3 C8 -171.5(8) . . . . ? Ce1 C63 Ce3 C8 90.1(5) . . . . ? C22 C63 Ce3 C78 -166.0(6) . . . . ? C15 C63 Ce3 C78 74.5(8) . . . . ? C35 C63 Ce3 C78 -60.6(7) . . . . ? Ce1 C63 Ce3 C78 -159.0(7) . . . . ? C22 C63 Ce3 C49 163.6(6) . . . . ? C15 C63 Ce3 C49 44.2(8) . . . . ? C35 C63 Ce3 C49 -91.0(8) . . . . ? Ce1 C63 Ce3 C49 170.6(8) . . . . ? C22 C63 Ce3 C54 90.9(7) . . . . ? C15 C63 Ce3 C54 -28.5(6) . . . . ? C35 C63 Ce3 C54 -163.7(7) . . . . ? Ce1 C63 Ce3 C54 97.9(5) . . . . ? C22 C63 Ce3 C10 113.2(7) . . . . ? C15 C63 Ce3 C10 -6.2(7) . . . . ? C35 C63 Ce3 C10 -141.4(8) . . . . ? Ce1 C63 Ce3 C10 120.2(6) . . . . ? C35 C40 Ce3 C68 99.5(8) . . . . ? C38 C40 Ce3 C68 -144.6(9) . . . . ? C76 C40 Ce3 C68 -31.1(7) . . . . ? C35 C40 Ce3 C15 59.5(7) . . . . ? C38 C40 Ce3 C15 175.4(8) . . . . ? C76 C40 Ce3 C15 -71.1(7) . . . . ? C35 C40 Ce3 C76 130.6(9) . . . . ? C38 C40 Ce3 C76 -113.5(10) . . . . ? C35 C40 Ce3 C63 25.5(6) . . . . ? C38 C40 Ce3 C63 141.4(8) . . . . ? C76 C40 Ce3 C63 -105.1(7) . . . . ? C38 C40 Ce3 C35 116.0(9) . . . . ? C76 C40 Ce3 C35 -130.6(9) . . . . ? C35 C40 Ce3 C69 123.0(8) . . . . ? C38 C40 Ce3 C69 -121.0(8) . . . . ? C76 C40 Ce3 C69 -7.6(7) . . . . ? C35 C40 Ce3 C8 55.2(8) . . . . ? C38 C40 Ce3 C8 171.2(8) . . . . ? C76 C40 Ce3 C8 -75.3(8) . . . . ? C35 C40 Ce3 C78 162.6(7) . . . . ? C38 C40 Ce3 C78 -81.4(7) . . . . ? C76 C40 Ce3 C78 32.0(6) . . . . ? C35 C40 Ce3 C49 151.7(7) . . . . ? C38 C40 Ce3 C49 -92.4(8) . . . . ? C76 C40 Ce3 C49 21.1(6) . . . . ? C35 C40 Ce3 C54 83.3(11) . . . . ? C38 C40 Ce3 C54 -160.8(10) . . . . ? C76 C40 Ce3 C54 -47.3(10) . . . . ? C35 C40 Ce3 C10 115.5(9) . . . . ? C38 C40 Ce3 C10 -128.5(9) . . . . ? C76 C40 Ce3 C10 -15.0(9) . . . . ? C40 C35 Ce3 C68 -69.5(7) . . . . ? C41 C35 Ce3 C68 169.5(8) . . . . ? C63 C35 Ce3 C68 68.8(7) . . . . ? C40 C35 Ce3 C15 -111.0(8) . . . . ? C41 C35 Ce3 C15 128.0(8) . . . . ? C63 C35 Ce3 C15 27.3(6) . . . . ? C40 C35 Ce3 C76 -30.2(6) . . . . ? C41 C35 Ce3 C76 -151.2(8) . . . . ? C63 C35 Ce3 C76 108.1(7) . . . . ? C40 C35 Ce3 C63 -138.3(9) . . . . ? C41 C35 Ce3 C63 100.7(9) . . . . ? C41 C35 Ce3 C40 -121.0(9) . . . . ? C63 C35 Ce3 C40 138.3(9) . . . . ? C40 C35 Ce3 C69 -62.8(8) . . . . ? C41 C35 Ce3 C69 176.2(7) . . . . ? C63 C35 Ce3 C69 75.5(8) . . . . ? C40 C35 Ce3 C8 -131.0(7) . . . . ? C41 C35 Ce3 C8 108.0(8) . . . . ? C63 C35 Ce3 C8 7.3(6) . . . . ? C40 C35 Ce3 C78 -14.6(6) . . . . ? C41 C35 Ce3 C78 -135.6(7) . . . . ? C63 C35 Ce3 C78 123.7(7) . . . . ? C40 C35 Ce3 C49 -31.2(7) . . . . ? C41 C35 Ce3 C49 -152.2(7) . . . . ? C63 C35 Ce3 C49 107.1(8) . . . . ? C40 C35 Ce3 C54 -119.4(9) . . . . ? C41 C35 Ce3 C54 119.6(8) . . . . ? C63 C35 Ce3 C54 18.9(8) . . . . ? C40 C35 Ce3 C10 -87.1(10) . . . . ? C41 C35 Ce3 C10 151.9(9) . . . . ? C63 C35 Ce3 C10 51.2(10) . . . . ? C10 C69 Ce3 C68 -126.3(9) . . . . ? C49 C69 Ce3 C68 116.0(9) . . . . ? C10 C69 Ce3 C15 -89.3(7) . . . . ? C49 C69 Ce3 C15 152.9(8) . . . . ? C68 C69 Ce3 C15 37.0(6) . . . . ? C10 C69 Ce3 C76 -171.6(8) . . . . ? C49 C69 Ce3 C76 70.6(7) . . . . ? C68 C69 Ce3 C76 -45.3(7) . . . . ? C10 C69 Ce3 C63 -103.6(8) . . . . ? C49 C69 Ce3 C63 138.6(7) . . . . ? C68 C69 Ce3 C63 22.7(7) . . . . ? C10 C69 Ce3 C40 -166.4(8) . . . . ? C49 C69 Ce3 C40 75.8(8) . . . . ? C68 C69 Ce3 C40 -40.1(7) . . . . ? C10 C69 Ce3 C35 -137.8(8) . . . . ? C49 C69 Ce3 C35 104.5(8) . . . . ? C68 C69 Ce3 C35 -11.5(7) . . . . ? C10 C69 Ce3 C8 -52.2(7) . . . . ? C49 C69 Ce3 C8 -170.0(7) . . . . ? C68 C69 Ce3 C8 74.0(7) . . . . ? C10 C69 Ce3 C78 150.5(8) . . . . ? C49 C69 Ce3 C78 32.8(6) . . . . ? C68 C69 Ce3 C78 -83.2(7) . . . . ? C10 C69 Ce3 C49 117.8(9) . . . . ? C68 C69 Ce3 C49 -116.0(9) . . . . ? C10 C69 Ce3 C54 -24.5(6) . . . . ? C49 C69 Ce3 C54 -142.3(8) . . . . ? C68 C69 Ce3 C54 101.7(7) . . . . ? C49 C69 Ce3 C10 -117.8(9) . . . . ? C68 C69 Ce3 C10 126.3(9) . . . . ? C33 C8 Ce3 C68 -155.4(8) . . . . ? C54 C8 Ce3 C68 86.7(7) . . . . ? C15 C8 Ce3 C68 -38.4(7) . . . . ? C33 C8 Ce3 C15 -117.0(10) . . . . ? C54 C8 Ce3 C15 125.1(9) . . . . ? C33 C8 Ce3 C76 -144.5(8) . . . . ? C54 C8 Ce3 C76 97.6(8) . . . . ? C15 C8 Ce3 C76 -27.5(8) . . . . ? C33 C8 Ce3 C63 -78.4(7) . . . . ? C54 C8 Ce3 C63 163.7(7) . . . . ? C15 C8 Ce3 C63 38.6(7) . . . . ? C33 C8 Ce3 C40 -109.6(8) . . . . ? C54 C8 Ce3 C40 132.5(8) . . . . ? C15 C8 Ce3 C40 7.4(8) . . . . ? C33 C8 Ce3 C35 -83.3(8) . . . . ? C54 C8 Ce3 C35 158.8(7) . . . . ? C15 C8 Ce3 C35 33.7(7) . . . . ? C33 C8 Ce3 C69 166.9(7) . . . . ? C54 C8 Ce3 C69 49.0(6) . . . . ? C15 C8 Ce3 C69 -76.1(7) . . . . ? C33 C8 Ce3 C78 -173.3(8) . . . . ? C54 C8 Ce3 C78 68.8(9) . . . . ? C15 C8 Ce3 C78 -56.2(9) . . . . ? C33 C8 Ce3 C49 161.9(7) . . . . ? C54 C8 Ce3 C49 44.1(7) . . . . ? C15 C8 Ce3 C49 -81.0(8) . . . . ? C33 C8 Ce3 C54 117.9(9) . . . . ? C15 C8 Ce3 C54 -125.1(9) . . . . ? C33 C8 Ce3 C10 138.9(7) . . . . ? C54 C8 Ce3 C10 21.1(5) . . . . ? C15 C8 Ce3 C10 -104.0(8) . . . . ? C60 C78 Ce3 C68 165.5(8) . . . . ? C76 C78 Ce3 C68 46.3(7) . . . . ? C49 C78 Ce3 C68 -75.2(7) . . . . ? C60 C78 Ce3 C15 157.0(8) . . . . ? C76 C78 Ce3 C15 37.8(7) . . . . ? C49 C78 Ce3 C15 -83.7(8) . . . . ? C60 C78 Ce3 C76 119.3(9) . . . . ? C49 C78 Ce3 C76 -121.5(9) . . . . ? C60 C78 Ce3 C63 122.2(7) . . . . ? C76 C78 Ce3 C63 2.9(6) . . . . ? C49 C78 Ce3 C63 -118.6(7) . . . . ? C60 C78 Ce3 C40 82.9(7) . . . . ? C76 C78 Ce3 C40 -36.4(6) . . . . ? C49 C78 Ce3 C40 -157.9(8) . . . . ? C60 C78 Ce3 C35 92.2(7) . . . . ? C76 C78 Ce3 C35 -27.1(6) . . . . ? C49 C78 Ce3 C35 -148.6(7) . . . . ? C60 C78 Ce3 C69 -151.3(8) . . . . ? C76 C78 Ce3 C69 89.4(7) . . . . ? C49 C78 Ce3 C69 -32.1(6) . . . . ? C60 C78 Ce3 C8 -175.1(8) . . . . ? C76 C78 Ce3 C8 65.7(9) . . . . ? C49 C78 Ce3 C8 -55.8(9) . . . . ? C60 C78 Ce3 C49 -119.2(9) . . . . ? C76 C78 Ce3 C49 121.5(9) . . . . ? C60 C78 Ce3 C54 -147.3(8) . . . . ? C76 C78 Ce3 C54 93.4(8) . . . . ? C49 C78 Ce3 C54 -28.1(7) . . . . ? C60 C78 Ce3 C10 -137.4(7) . . . . ? C76 C78 Ce3 C10 103.3(7) . . . . ? C49 C78 Ce3 C10 -18.2(6) . . . . ? C44 C49 Ce3 C68 -157.0(7) . . . . ? C69 C49 Ce3 C68 -39.5(6) . . . . ? C78 C49 Ce3 C68 82.9(7) . . . . ? C44 C49 Ce3 C15 -141.9(7) . . . . ? C69 C49 Ce3 C15 -24.3(7) . . . . ? C78 C49 Ce3 C15 98.0(8) . . . . ? C44 C49 Ce3 C76 153.8(7) . . . . ? C69 C49 Ce3 C76 -88.6(8) . . . . ? C78 C49 Ce3 C76 33.7(6) . . . . ? C44 C49 Ce3 C63 -166.2(7) . . . . ? C69 C49 Ce3 C63 -48.6(8) . . . . ? C78 C49 Ce3 C63 73.7(8) . . . . ? C44 C49 Ce3 C40 138.6(7) . . . . ? C69 C49 Ce3 C40 -103.8(8) . . . . ? C78 C49 Ce3 C40 18.5(7) . . . . ? C44 C49 Ce3 C35 154.9(7) . . . . ? C69 C49 Ce3 C35 -87.5(9) . . . . ? C78 C49 Ce3 C35 34.8(8) . . . . ? C44 C49 Ce3 C69 -117.6(9) . . . . ? C78 C49 Ce3 C69 122.3(10) . . . . ? C44 C49 Ce3 C8 -108.2(7) . . . . ? C69 C49 Ce3 C8 9.4(7) . . . . ? C78 C49 Ce3 C8 131.7(8) . . . . ? C44 C49 Ce3 C78 120.1(9) . . . . ? C69 C49 Ce3 C78 -122.3(10) . . . . ? C44 C49 Ce3 C54 -88.0(7) . . . . ? C69 C49 Ce3 C54 29.6(6) . . . . ? C78 C49 Ce3 C54 151.9(7) . . . . ? C44 C49 Ce3 C10 -83.6(7) . . . . ? C69 C49 Ce3 C10 33.9(6) . . . . ? C78 C49 Ce3 C10 156.3(8) . . . . ? C4 C54 Ce3 C68 165.8(8) . . . . ? C10 C54 Ce3 C68 62.8(7) . . . . ? C8 C54 Ce3 C68 -79.1(8) . . . . ? C4 C54 Ce3 C15 -149.0(8) . . . . ? C10 C54 Ce3 C15 108.0(8) . . . . ? C8 C54 Ce3 C15 -33.9(6) . . . . ? C4 C54 Ce3 C76 156.1(8) . . . . ? C10 C54 Ce3 C76 53.2(9) . . . . ? C8 C54 Ce3 C76 -88.7(9) . . . . ? C4 C54 Ce3 C63 -129.0(8) . . . . ? C10 C54 Ce3 C63 128.1(7) . . . . ? C8 C54 Ce3 C63 -13.8(6) . . . . ? C4 C54 Ce3 C40 -177.8(10) . . . . ? C10 C54 Ce3 C40 79.2(11) . . . . ? C8 C54 Ce3 C40 -62.7(11) . . . . ? C4 C54 Ce3 C35 -139.7(8) . . . . ? C10 C54 Ce3 C35 117.3(9) . . . . ? C8 C54 Ce3 C35 -24.6(8) . . . . ? C4 C54 Ce3 C69 128.0(8) . . . . ? C10 C54 Ce3 C69 25.0(6) . . . . ? C8 C54 Ce3 C69 -116.9(8) . . . . ? C4 C54 Ce3 C8 -115.1(9) . . . . ? C10 C54 Ce3 C8 141.9(9) . . . . ? C4 C54 Ce3 C78 124.0(8) . . . . ? C10 C54 Ce3 C78 21.0(8) . . . . ? C8 C54 Ce3 C78 -120.9(9) . . . . ? C4 C54 Ce3 C49 109.9(7) . . . . ? C10 C54 Ce3 C49 7.0(6) . . . . ? C8 C54 Ce3 C49 -134.9(7) . . . . ? C4 C54 Ce3 C10 103.0(9) . . . . ? C8 C54 Ce3 C10 -141.9(9) . . . . ? C69 C10 Ce3 C68 33.7(7) . . . . ? C7 C10 Ce3 C68 149.0(8) . . . . ? C54 C10 Ce3 C68 -102.0(8) . . . . ? C69 C10 Ce3 C15 77.9(8) . . . . ? C7 C10 Ce3 C15 -166.9(8) . . . . ? C54 C10 Ce3 C15 -57.9(7) . . . . ? C69 C10 Ce3 C76 7.1(7) . . . . ? C7 C10 Ce3 C76 122.4(8) . . . . ? C54 C10 Ce3 C76 -128.6(8) . . . . ? C69 C10 Ce3 C63 81.8(8) . . . . ? C7 C10 Ce3 C63 -162.9(7) . . . . ? C54 C10 Ce3 C63 -53.9(7) . . . . ? C69 C10 Ce3 C40 15.8(9) . . . . ? C7 C10 Ce3 C40 131.1(9) . . . . ? C54 C10 Ce3 C40 -119.9(10) . . . . ? C69 C10 Ce3 C35 54.4(10) . . . . ? C7 C10 Ce3 C35 169.7(9) . . . . ? C54 C10 Ce3 C35 -81.3(10) . . . . ? C7 C10 Ce3 C69 115.3(10) . . . . ? C54 C10 Ce3 C69 -135.7(10) . . . . ? C69 C10 Ce3 C8 113.9(8) . . . . ? C7 C10 Ce3 C8 -130.8(8) . . . . ? C54 C10 Ce3 C8 -21.8(5) . . . . ? C69 C10 Ce3 C78 -23.3(6) . . . . ? C7 C10 Ce3 C78 92.0(7) . . . . ? C54 C10 Ce3 C78 -159.0(7) . . . . ? C69 C10 Ce3 C49 -35.3(6) . . . . ? C7 C10 Ce3 C49 80.0(7) . . . . ? C54 C10 Ce3 C49 -171.0(8) . . . . ? C69 C10 Ce3 C54 135.7(10) . . . . ? C7 C10 Ce3 C54 -109.0(9) . . . . ? C50 C73 Ce4 C18 -124.3(7) . . . . ? C72 C73 Ce4 C18 130.6(8) . . . . ? C18 C73 Ce4 C72 -130.6(8) . . . . ? C50 C73 Ce4 C72 105.2(8) . . . . ? C18 C73 Ce4 C32 -33.4(5) . . . . ? C50 C73 Ce4 C32 -157.6(6) . . . . ? C72 C73 Ce4 C32 97.2(6) . . . . ? C18 C73 Ce4 C56 -102.1(6) . . . . ? C50 C73 Ce4 C56 133.7(7) . . . . ? C72 C73 Ce4 C56 28.5(6) . . . . ? C18 C73 Ce4 C50 124.3(7) . . . . ? C72 C73 Ce4 C50 -105.2(8) . . . . ? C18 C73 Ce4 C20 -67.3(5) . . . . ? C50 C73 Ce4 C20 168.5(6) . . . . ? C72 C73 Ce4 C20 63.3(6) . . . . ? C18 C73 Ce4 C71 33.0(5) . . . . ? C50 C73 Ce4 C71 -91.3(6) . . . . ? C72 C73 Ce4 C71 163.5(7) . . . . ? C18 C73 Ce4 C27 -165.7(6) . . . . ? C50 C73 Ce4 C27 70.0(6) . . . . ? C72 C73 Ce4 C27 -35.2(5) . . . . ? C18 C73 Ce4 C77 157.4(6) . . . . ? C50 C73 Ce4 C77 33.2(5) . . . . ? C72 C73 Ce4 C77 -72.0(6) . . . . ? C18 C73 Ce4 C70 95.6(5) . . . . ? C50 C73 Ce4 C70 -28.7(4) . . . . ? C72 C73 Ce4 C70 -133.8(7) . . . . ? C18 C73 Ce4 C26 64.6(5) . . . . ? C50 C73 Ce4 C26 -59.7(5) . . . . ? C72 C73 Ce4 C26 -164.8(7) . . . . ? C32 C18 Ce4 C73 -121.8(7) . . . . ? C71 C18 Ce4 C73 120.4(8) . . . . ? C73 C18 Ce4 C72 31.2(5) . . . . ? C32 C18 Ce4 C72 -90.5(6) . . . . ? C71 C18 Ce4 C72 151.6(7) . . . . ? C73 C18 Ce4 C32 121.8(7) . . . . ? C71 C18 Ce4 C32 -117.9(9) . . . . ? C73 C18 Ce4 C56 66.0(6) . . . . ? C32 C18 Ce4 C56 -55.8(6) . . . . ? C71 C18 Ce4 C56 -173.7(7) . . . . ? C73 C18 Ce4 C50 -32.3(5) . . . . ? C32 C18 Ce4 C50 -154.0(6) . . . . ? C71 C18 Ce4 C50 88.1(6) . . . . ? C73 C18 Ce4 C20 98.5(6) . . . . ? C32 C18 Ce4 C20 -23.3(5) . . . . ? C71 C18 Ce4 C20 -141.1(7) . . . . ? C73 C18 Ce4 C71 -120.4(8) . . . . ? C32 C18 Ce4 C71 117.9(9) . . . . ? C73 C18 Ce4 C27 12.1(5) . . . . ? C32 C18 Ce4 C27 -109.6(6) . . . . ? C71 C18 Ce4 C27 132.5(7) . . . . ? C73 C18 Ce4 C77 -18.5(5) . . . . ? C32 C18 Ce4 C77 -140.3(6) . . . . ? C71 C18 Ce4 C77 101.8(7) . . . . ? C73 C18 Ce4 C70 -64.0(5) . . . . ? C32 C18 Ce4 C70 174.2(6) . . . . ? C71 C18 Ce4 C70 56.3(6) . . . . ? C73 C18 Ce4 C26 -93.6(6) . . . . ? C32 C18 Ce4 C26 144.7(7) . . . . ? C71 C18 Ce4 C26 26.8(5) . . . . ? C56 C72 Ce4 C73 129.2(9) . . . . ? C27 C72 Ce4 C73 -110.2(9) . . . . ? C56 C72 Ce4 C18 98.1(7) . . . . ? C27 C72 Ce4 C18 -141.3(7) . . . . ? C73 C72 Ce4 C18 -31.1(6) . . . . ? C56 C72 Ce4 C32 60.8(6) . . . . ? C27 C72 Ce4 C32 -178.7(7) . . . . ? C73 C72 Ce4 C32 -68.4(7) . . . . ? C27 C72 Ce4 C56 120.6(9) . . . . ? C73 C72 Ce4 C56 -129.2(9) . . . . ? C56 C72 Ce4 C50 170.9(8) . . . . ? C27 C72 Ce4 C50 -68.5(6) . . . . ? C73 C72 Ce4 C50 41.7(6) . . . . ? C56 C72 Ce4 C20 27.5(6) . . . . ? C27 C72 Ce4 C20 148.1(7) . . . . ? C73 C72 Ce4 C20 -101.7(7) . . . . ? C56 C72 Ce4 C71 114.1(7) . . . . ? C27 C72 Ce4 C71 -125.3(7) . . . . ? C73 C72 Ce4 C71 -15.1(7) . . . . ? C56 C72 Ce4 C27 -120.6(9) . . . . ? C73 C72 Ce4 C27 110.2(9) . . . . ? C56 C72 Ce4 C77 -153.2(7) . . . . ? C27 C72 Ce4 C77 -32.6(5) . . . . ? C73 C72 Ce4 C77 77.6(7) . . . . ? C56 C72 Ce4 C70 166.8(7) . . . . ? C27 C72 Ce4 C70 -72.6(7) . . . . ? C73 C72 Ce4 C70 37.6(6) . . . . ? C56 C72 Ce4 C26 143.8(7) . . . . ? C27 C72 Ce4 C26 -95.6(7) . . . . ? C73 C72 Ce4 C26 14.6(7) . . . . ? C18 C32 Ce4 C73 37.3(6) . . . . ? C20 C32 Ce4 C73 -102.6(7) . . . . ? C57 C32 Ce4 C73 155.2(8) . . . . ? Ce2 C32 Ce4 C73 163.9(6) . . . . ? C20 C32 Ce4 C18 -139.9(9) . . . . ? C57 C32 Ce4 C18 117.9(9) . . . . ? Ce2 C32 Ce4 C18 126.6(7) . . . . ? C18 C32 Ce4 C72 78.9(7) . . . . ? C20 C32 Ce4 C72 -61.0(7) . . . . ? C57 C32 Ce4 C72 -163.1(7) . . . . ? Ce2 C32 Ce4 C72 -154.5(6) . . . . ? C18 C32 Ce4 C56 112.9(8) . . . . ? C20 C32 Ce4 C56 -27.0(6) . . . . ? C57 C32 Ce4 C56 -129.1(8) . . . . ? Ce2 C32 Ce4 C56 -120.5(6) . . . . ? C18 C32 Ce4 C50 24.0(6) . . . . ? C20 C32 Ce4 C50 -115.9(7) . . . . ? C57 C32 Ce4 C50 142.0(7) . . . . ? Ce2 C32 Ce4 C50 150.6(6) . . . . ? C18 C32 Ce4 C20 139.9(9) . . . . ? C57 C32 Ce4 C20 -102.2(9) . . . . ? Ce2 C32 Ce4 C20 -93.5(7) . . . . ? C18 C32 Ce4 C71 -35.5(5) . . . . ? C20 C32 Ce4 C71 -175.4(8) . . . . ? C57 C32 Ce4 C71 82.4(7) . . . . ? Ce2 C32 Ce4 C71 91.0(4) . . . . ? C18 C32 Ce4 C27 78.2(8) . . . . ? C20 C32 Ce4 C27 -61.7(8) . . . . ? C57 C32 Ce4 C27 -163.9(7) . . . . ? Ce2 C32 Ce4 C27 -155.2(8) . . . . ? C18 C32 Ce4 C77 47.6(8) . . . . ? C20 C32 Ce4 C77 -92.3(8) . . . . ? C57 C32 Ce4 C77 165.5(7) . . . . ? Ce2 C32 Ce4 C77 174.2(8) . . . . ? C18 C32 Ce4 C70 -5.6(6) . . . . ? C20 C32 Ce4 C70 -145.5(8) . . . . ? C57 C32 Ce4 C70 112.3(8) . . . . ? Ce2 C32 Ce4 C70 121.0(6) . . . . ? C18 C32 Ce4 C26 -28.9(6) . . . . ? C20 C32 Ce4 C26 -168.8(7) . . . . ? C57 C32 Ce4 C26 89.0(8) . . . . ? Ce2 C32 Ce4 C26 97.7(4) . . . . ? C72 C56 Ce4 C73 -33.2(7) . . . . ? C39 C56 Ce4 C73 -146.4(8) . . . . ? C20 C56 Ce4 C73 100.1(8) . . . . ? C72 C56 Ce4 C18 -73.3(8) . . . . ? C39 C56 Ce4 C18 173.5(8) . . . . ? C20 C56 Ce4 C18 60.0(7) . . . . ? C39 C56 Ce4 C72 -113.2(10) . . . . ? C20 C56 Ce4 C72 133.3(9) . . . . ? C72 C56 Ce4 C32 -106.7(7) . . . . ? C39 C56 Ce4 C32 140.1(8) . . . . ? C20 C56 Ce4 C32 26.6(6) . . . . ? C72 C56 Ce4 C50 -7.8(7) . . . . ? C39 C56 Ce4 C50 -121.0(8) . . . . ? C20 C56 Ce4 C50 125.5(8) . . . . ? C72 C56 Ce4 C20 -133.3(9) . . . . ? C39 C56 Ce4 C20 113.6(10) . . . . ? C72 C56 Ce4 C71 -77.2(9) . . . . ? C39 C56 Ce4 C71 169.6(8) . . . . ? C20 C56 Ce4 C71 56.1(9) . . . . ? C72 C56 Ce4 C27 32.5(6) . . . . ? C39 C56 Ce4 C27 -80.6(7) . . . . ? C20 C56 Ce4 C27 165.8(8) . . . . ? C72 C56 Ce4 C77 21.3(6) . . . . ? C39 C56 Ce4 C77 -91.8(8) . . . . ? C20 C56 Ce4 C77 154.6(7) . . . . ? C72 C56 Ce4 C70 -15.6(8) . . . . ? C39 C56 Ce4 C70 -128.8(8) . . . . ? C20 C56 Ce4 C70 117.6(9) . . . . ? C72 C56 Ce4 C26 -50.0(10) . . . . ? C39 C56 Ce4 C26 -163.2(9) . . . . ? C20 C56 Ce4 C26 83.3(10) . . . . ? C70 C50 Ce4 C73 -124.7(9) . . . . ? C77 C50 Ce4 C73 116.2(8) . . . . ? C70 C50 Ce4 C18 -89.0(6) . . . . ? C77 C50 Ce4 C18 152.0(6) . . . . ? C73 C50 Ce4 C18 35.7(6) . . . . ? C70 C50 Ce4 C72 -171.6(7) . . . . ? C77 C50 Ce4 C72 69.3(6) . . . . ? C73 C50 Ce4 C72 -46.9(6) . . . . ? C70 C50 Ce4 C32 -104.1(7) . . . . ? C77 C50 Ce4 C32 136.8(6) . . . . ? C73 C50 Ce4 C32 20.6(6) . . . . ? C70 C50 Ce4 C56 -166.4(7) . . . . ? C77 C50 Ce4 C56 74.5(7) . . . . ? C73 C50 Ce4 C56 -41.8(6) . . . . ? C70 C50 Ce4 C20 -136.8(7) . . . . ? C77 C50 Ce4 C20 104.1(7) . . . . ? C73 C50 Ce4 C20 -12.1(6) . . . . ? C70 C50 Ce4 C71 -52.0(6) . . . . ? C77 C50 Ce4 C71 -171.0(6) . . . . ? C73 C50 Ce4 C71 72.7(6) . . . . ? C70 C50 Ce4 C27 151.2(7) . . . . ? C77 C50 Ce4 C27 32.1(5) . . . . ? C73 C50 Ce4 C27 -84.1(6) . . . . ? C70 C50 Ce4 C77 119.1(8) . . . . ? C73 C50 Ce4 C77 -116.2(8) . . . . ? C77 C50 Ce4 C70 -119.1(8) . . . . ? C73 C50 Ce4 C70 124.7(9) . . . . ? C70 C50 Ce4 C26 -24.2(5) . . . . ? C77 C50 Ce4 C26 -143.3(6) . . . . ? C73 C50 Ce4 C26 100.5(7) . . . . ? C3 C20 Ce4 C73 172.0(8) . . . . ? C32 C20 Ce4 C73 66.0(7) . . . . ? C56 C20 Ce4 C73 -68.7(7) . . . . ? Ce2 C20 Ce4 C73 145.1(7) . . . . ? C3 C20 Ce4 C18 130.7(8) . . . . ? C32 C20 Ce4 C18 24.7(6) . . . . ? C56 C20 Ce4 C18 -109.9(8) . . . . ? Ce2 C20 Ce4 C18 103.9(6) . . . . ? C3 C20 Ce4 C72 -147.1(8) . . . . ? C32 C20 Ce4 C72 106.9(8) . . . . ? C56 C20 Ce4 C72 -27.7(6) . . . . ? Ce2 C20 Ce4 C72 -174.0(7) . . . . ? C3 C20 Ce4 C32 106.0(9) . . . . ? C56 C20 Ce4 C32 -134.6(10) . . . . ? Ce2 C20 Ce4 C32 79.2(7) . . . . ? C3 C20 Ce4 C56 -119.4(10) . . . . ? C32 C20 Ce4 C56 134.6(10) . . . . ? Ce2 C20 Ce4 C56 -146.2(8) . . . . ? C3 C20 Ce4 C50 179.3(7) . . . . ? C32 C20 Ce4 C50 73.3(8) . . . . ? C56 C20 Ce4 C50 -61.3(8) . . . . ? Ce2 C20 Ce4 C50 152.5(8) . . . . ? C3 C20 Ce4 C71 109.9(8) . . . . ? C32 C20 Ce4 C71 3.9(7) . . . . ? C56 C20 Ce4 C71 -130.7(8) . . . . ? Ce2 C20 Ce4 C71 83.1(5) . . . . ? C3 C20 Ce4 C27 -131.1(8) . . . . ? C32 C20 Ce4 C27 122.8(8) . . . . ? C56 C20 Ce4 C27 -11.8(6) . . . . ? Ce2 C20 Ce4 C27 -158.0(7) . . . . ? C3 C20 Ce4 C77 -147.7(8) . . . . ? C32 C20 Ce4 C77 106.2(9) . . . . ? C56 C20 Ce4 C77 -28.4(8) . . . . ? Ce2 C20 Ce4 C77 -174.6(9) . . . . ? C3 C20 Ce4 C70 152.7(8) . . . . ? C32 C20 Ce4 C70 46.6(9) . . . . ? C56 C20 Ce4 C70 -88.0(9) . . . . ? Ce2 C20 Ce4 C70 125.8(9) . . . . ? C3 C20 Ce4 C26 119.0(9) . . . . ? C32 C20 Ce4 C26 13.0(8) . . . . ? C56 C20 Ce4 C26 -121.6(9) . . . . ? Ce2 C20 Ce4 C26 92.2(7) . . . . ? C26 C71 Ce4 C73 90.4(7) . . . . ? C5 C71 Ce4 C73 -153.5(8) . . . . ? C18 C71 Ce4 C73 -38.6(7) . . . . ? C26 C71 Ce4 C18 129.0(9) . . . . ? C5 C71 Ce4 C18 -114.9(9) . . . . ? C26 C71 Ce4 C72 101.3(7) . . . . ? C5 C71 Ce4 C72 -142.6(7) . . . . ? C18 C71 Ce4 C72 -27.7(7) . . . . ? C26 C71 Ce4 C32 166.2(7) . . . . ? C5 C71 Ce4 C32 -77.6(7) . . . . ? C18 C71 Ce4 C32 37.3(6) . . . . ? C26 C71 Ce4 C56 135.8(8) . . . . ? C5 C71 Ce4 C56 -108.0(9) . . . . ? C18 C71 Ce4 C56 6.8(8) . . . . ? C26 C71 Ce4 C50 51.2(6) . . . . ? C5 C71 Ce4 C50 167.4(7) . . . . ? C18 C71 Ce4 C50 -77.7(7) . . . . ? C26 C71 Ce4 C20 163.7(7) . . . . ? C5 C71 Ce4 C20 -80.2(7) . . . . ? C18 C71 Ce4 C20 34.7(7) . . . . ? C26 C71 Ce4 C27 72.3(8) . . . . ? C5 C71 Ce4 C27 -171.5(7) . . . . ? C18 C71 Ce4 C27 -56.7(8) . . . . ? C26 C71 Ce4 C77 46.7(6) . . . . ? C5 C71 Ce4 C77 162.8(6) . . . . ? C18 C71 Ce4 C77 -82.3(8) . . . . ? C26 C71 Ce4 C70 22.6(5) . . . . ? C5 C71 Ce4 C70 138.8(7) . . . . ? C18 C71 Ce4 C70 -106.3(8) . . . . ? C5 C71 Ce4 C26 116.2(8) . . . . ? C18 C71 Ce4 C26 -129.0(9) . . . . ? C72 C27 Ce4 C73 46.1(7) . . . . ? C65 C27 Ce4 C73 165.9(8) . . . . ? C77 C27 Ce4 C73 -75.8(7) . . . . ? C72 C27 Ce4 C18 36.9(7) . . . . ? C65 C27 Ce4 C18 156.6(7) . . . . ? C77 C27 Ce4 C18 -85.0(7) . . . . ? C65 C27 Ce4 C72 119.7(9) . . . . ? C77 C27 Ce4 C72 -121.9(9) . . . . ? C72 C27 Ce4 C32 1.4(7) . . . . ? C65 C27 Ce4 C32 121.1(8) . . . . ? C77 C27 Ce4 C32 -120.5(8) . . . . ? C72 C27 Ce4 C56 -35.9(6) . . . . ? C65 C27 Ce4 C56 83.9(7) . . . . ? C77 C27 Ce4 C56 -157.8(8) . . . . ? C72 C27 Ce4 C50 90.3(7) . . . . ? C65 C27 Ce4 C50 -150.0(7) . . . . ? C77 C27 Ce4 C50 -31.7(6) . . . . ? C72 C27 Ce4 C20 -27.9(7) . . . . ? C65 C27 Ce4 C20 91.8(7) . . . . ? C77 C27 Ce4 C20 -149.9(7) . . . . ? C72 C27 Ce4 C71 65.3(8) . . . . ? C65 C27 Ce4 C71 -175.0(7) . . . . ? C77 C27 Ce4 C71 -56.6(8) . . . . ? C72 C27 Ce4 C77 121.9(9) . . . . ? C65 C27 Ce4 C77 -118.3(9) . . . . ? C72 C27 Ce4 C70 104.2(7) . . . . ? C65 C27 Ce4 C70 -136.1(7) . . . . ? C77 C27 Ce4 C70 -17.7(6) . . . . ? C72 C27 Ce4 C26 94.1(8) . . . . ? C65 C27 Ce4 C26 -146.1(7) . . . . ? C77 C27 Ce4 C26 -27.8(7) . . . . ? C46 C77 Ce4 C73 -157.2(7) . . . . ? C50 C77 Ce4 C73 -40.1(6) . . . . ? C27 C77 Ce4 C73 83.5(7) . . . . ? C46 C77 Ce4 C18 -142.7(7) . . . . ? C50 C77 Ce4 C18 -25.6(6) . . . . ? C27 C77 Ce4 C18 98.0(7) . . . . ? C46 C77 Ce4 C72 152.6(7) . . . . ? C50 C77 Ce4 C72 -90.3(7) . . . . ? C27 C77 Ce4 C72 33.3(6) . . . . ? C46 C77 Ce4 C32 -168.5(7) . . . . ? C50 C77 Ce4 C32 -51.4(8) . . . . ? C27 C77 Ce4 C32 72.2(8) . . . . ? C46 C77 Ce4 C56 137.7(7) . . . . ? C50 C77 Ce4 C56 -105.2(7) . . . . ? C27 C77 Ce4 C56 18.4(6) . . . . ? C46 C77 Ce4 C50 -117.1(8) . . . . ? C27 C77 Ce4 C50 123.6(9) . . . . ? C46 C77 Ce4 C20 153.3(7) . . . . ? C50 C77 Ce4 C20 -89.6(8) . . . . ? C27 C77 Ce4 C20 34.0(8) . . . . ? C46 C77 Ce4 C71 -108.6(7) . . . . ? C50 C77 Ce4 C71 8.5(6) . . . . ? C27 C77 Ce4 C71 132.1(7) . . . . ? C46 C77 Ce4 C27 119.3(9) . . . . ? C50 C77 Ce4 C27 -123.6(9) . . . . ? C46 C77 Ce4 C70 -83.4(6) . . . . ? C50 C77 Ce4 C70 33.7(5) . . . . ? C27 C77 Ce4 C70 157.3(8) . . . . ? C46 C77 Ce4 C26 -87.6(6) . . . . ? C50 C77 Ce4 C26 29.5(5) . . . . ? C27 C77 Ce4 C26 153.1(7) . . . . ? C50 C70 Ce4 C73 35.2(6) . . . . ? C24 C70 Ce4 C73 150.5(7) . . . . ? C26 C70 Ce4 C73 -101.6(7) . . . . ? C50 C70 Ce4 C18 78.8(7) . . . . ? C24 C70 Ce4 C18 -165.9(7) . . . . ? C26 C70 Ce4 C18 -58.0(6) . . . . ? C50 C70 Ce4 C72 7.2(6) . . . . ? C24 C70 Ce4 C72 122.5(7) . . . . ? C26 C70 Ce4 C72 -129.6(7) . . . . ? C50 C70 Ce4 C32 82.4(8) . . . . ? C24 C70 Ce4 C32 -162.4(7) . . . . ? C26 C70 Ce4 C32 -54.5(7) . . . . ? C50 C70 Ce4 C56 16.0(8) . . . . ? C24 C70 Ce4 C56 131.3(8) . . . . ? C26 C70 Ce4 C56 -120.8(8) . . . . ? C24 C70 Ce4 C50 115.3(9) . . . . ? C26 C70 Ce4 C50 -136.9(9) . . . . ? C50 C70 Ce4 C20 57.6(9) . . . . ? C24 C70 Ce4 C20 172.9(8) . . . . ? C26 C70 Ce4 C20 -79.3(9) . . . . ? C50 C70 Ce4 C71 114.3(7) . . . . ? C24 C70 Ce4 C71 -130.5(7) . . . . ? C26 C70 Ce4 C71 -22.6(5) . . . . ? C50 C70 Ce4 C27 -23.0(6) . . . . ? C24 C70 Ce4 C27 92.2(7) . . . . ? C26 C70 Ce4 C27 -159.9(7) . . . . ? C50 C70 Ce4 C77 -34.6(6) . . . . ? C24 C70 Ce4 C77 80.7(6) . . . . ? C26 C70 Ce4 C77 -171.4(7) . . . . ? C50 C70 Ce4 C26 136.9(9) . . . . ? C24 C70 Ce4 C26 -107.9(7) . . . . ? C71 C26 Ce4 C73 -76.2(7) . . . . ? C70 C26 Ce4 C73 63.7(6) . . . . ? C29 C26 Ce4 C73 165.8(8) . . . . ? C71 C26 Ce4 C18 -31.7(6) . . . . ? C70 C26 Ce4 C18 108.2(7) . . . . ? C29 C26 Ce4 C18 -149.7(8) . . . . ? C71 C26 Ce4 C72 -86.5(8) . . . . ? C70 C26 Ce4 C72 53.5(7) . . . . ? C29 C26 Ce4 C72 155.5(7) . . . . ? C71 C26 Ce4 C32 -11.8(6) . . . . ? C70 C26 Ce4 C32 128.1(7) . . . . ? C29 C26 Ce4 C32 -129.8(7) . . . . ? C71 C26 Ce4 C56 -59.5(10) . . . . ? C70 C26 Ce4 C56 80.4(10) . . . . ? C29 C26 Ce4 C56 -177.5(9) . . . . ? C71 C26 Ce4 C50 -115.4(7) . . . . ? C70 C26 Ce4 C50 24.6(5) . . . . ? C29 C26 Ce4 C50 126.6(7) . . . . ? C71 C26 Ce4 C20 -19.0(8) . . . . ? C70 C26 Ce4 C20 120.9(9) . . . . ? C29 C26 Ce4 C20 -137.0(8) . . . . ? C70 C26 Ce4 C71 140.0(8) . . . . ? C29 C26 Ce4 C71 -118.0(9) . . . . ? C71 C26 Ce4 C27 -119.2(8) . . . . ? C70 C26 Ce4 C27 20.7(7) . . . . ? C29 C26 Ce4 C27 122.8(7) . . . . ? C71 C26 Ce4 C77 -133.2(7) . . . . ? C70 C26 Ce4 C77 6.7(5) . . . . ? C29 C26 Ce4 C77 108.8(7) . . . . ? C71 C26 Ce4 C70 -140.0(8) . . . . ? C29 C26 Ce4 C70 102.0(8) . . . . ? _diffrn_measured_fraction_theta_max 0.762 _diffrn_reflns_theta_full 24.51 _diffrn_measured_fraction_theta_full 0.762 _refine_diff_density_max 1.182 _refine_diff_density_min -0.975 _refine_diff_density_rms 0.118 # Attachment 'Ce2@C78Si200krev2.cif' data_Ce2@C78Si200krev2 _database_code_depnum_ccdc_archive 'CCDC 661490' _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C117.50 H46 Ce2 S5 Si2' _chemical_formula_weight 1954.26 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M P212121 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' _cell_length_a 11.318(3) _cell_length_b 23.492(5) _cell_length_c 28.055(6) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 7459(3) _cell_formula_units_Z 4 _cell_measurement_temperature 296(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description platelet _exptl_crystal_colour black _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.01 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.741 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3900 _exptl_absorpt_coefficient_mu 1.441 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.8129 _exptl_absorpt_correction_T_max 0.9857 _exptl_absorpt_process_details 'SADABS Sheldrick 1996' _exptl_special_details ; ? ; _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.68880 _diffrn_radiation_type synchrotron _diffrn_radiation_source synchrotron _diffrn_radiation_source_type 'KEK BL1B' _diffrn_radiation_monochromator Si(111) _diffrn_measurement_device_type IPDSC _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 33749 _diffrn_reflns_av_R_equivalents 0.0370 _diffrn_reflns_av_sigmaI/netI 0.0370 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_theta_min 1.41 _diffrn_reflns_theta_max 24.51 _reflns_number_total 10233 _reflns_number_gt 8436 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'Bruker SMART' _computing_cell_refinement 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The 977 restraints were used in the refinements. All atoms were refined with SIMU to generate similar Uij restraints automatically using connectivity. S5, C118, and S6 were refined with ISOR so that their Uij components approximate to isotropic behavior. S5, C118, and S6 were also refined with DELU to generate rigid bond Uij restraints automatically using connectivity. S5, C118, and S6 were also refined with DANG to restrain the 1,3-distance S5...S6. ; _chemical_absolute_configuration unk _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.1012P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.334(15) _refine_ls_number_reflns 10233 _refine_ls_number_parameters 1186 _refine_ls_number_restraints 977 _refine_ls_R_factor_all 0.0572 _refine_ls_R_factor_gt 0.0465 _refine_ls_wR_factor_ref 0.1332 _refine_ls_wR_factor_gt 0.1259 _refine_ls_goodness_of_fit_ref 1.007 _refine_ls_restrained_S_all 1.014 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ce1 Ce 0.51354(4) 0.59586(2) 0.102257(15) 0.05202(16) Uani 0.9567(14) 1 d P A 2 Ce2 Ce 0.86790(5) 0.60789(2) 0.114093(15) 0.05295(16) Uani 0.9567(14) 1 d P A 2 Si1 Si 0.5689(2) 0.74731(11) 0.28500(7) 0.0508(6) Uani 1 1 d . . . Si2 Si 0.7069(2) 0.62299(11) 0.32763(7) 0.0576(7) Uani 1 1 d . . . C79 C 0.7961(12) 0.4988(5) 0.3512(3) 0.088(3) Uani 1 1 d U . . H1 H 0.8354 0.5177 0.3771 0.132 Uiso 1 1 calc R . . H2 H 0.8235 0.5141 0.3215 0.132 Uiso 1 1 calc R . . H3 H 0.8132 0.4588 0.3525 0.132 Uiso 1 1 calc R . . C1 C 0.3859(8) 0.6661(4) 0.1616(3) 0.0561(15) Uani 1 1 d U . . C2 C 0.9609(7) 0.6002(4) 0.2044(3) 0.0562(14) Uani 1 1 d U . . C3 C 0.9755(9) 0.6401(4) 0.0245(3) 0.0618(15) Uani 1 1 d U . . C4 C 0.6039(7) 0.6014(4) 0.2427(2) 0.0525(14) Uani 1 1 d U A . C5 C 0.9387(8) 0.6933(4) 0.1751(3) 0.0556(15) Uani 1 1 d U . . C6 C 0.9547(9) 0.4896(4) 0.0942(3) 0.0635(16) Uani 1 1 d U . . C7 C 0.7884(9) 0.5527(4) 0.2392(3) 0.0551(15) Uani 1 1 d U . . C8 C 0.4836(8) 0.5282(4) 0.2013(3) 0.0553(14) Uani 1 1 d U . . C9 C 0.8901(9) 0.5485(4) 0.2142(3) 0.0579(15) Uani 1 1 d U A . C80 C 0.4172(10) 0.6146(4) 0.3437(3) 0.077(3) Uani 1 1 d U . . H4 H 0.3350 0.6050 0.3411 0.116 Uiso 1 1 calc R . . H5 H 0.4432 0.6322 0.3147 0.116 Uiso 1 1 calc R . . H6 H 0.4282 0.6405 0.3698 0.116 Uiso 1 1 calc R . . C10 C 0.6925(9) 0.5151(4) 0.2303(3) 0.0581(15) Uani 1 1 d U A . C81 C 0.5836(8) 0.8621(4) 0.2491(3) 0.0526(16) Uani 1 1 d U . . C11 C 0.9945(9) 0.5292(4) 0.0588(3) 0.0648(15) Uani 1 1 d U A . C12 C 1.0345(9) 0.6648(4) 0.1483(3) 0.0617(16) Uani 1 1 d U A . C13 C 0.4255(8) 0.6128(4) 0.0097(3) 0.0619(15) Uani 1 1 d U . . C82 C 0.6661(12) 0.5078(5) 0.3554(3) 0.080(2) Uani 1 1 d U . . C14 C 1.0425(8) 0.6072(4) 0.1676(3) 0.0602(15) Uani 1 1 d U A . C15 C 0.5009(9) 0.4809(4) 0.1686(3) 0.0577(14) Uani 1 1 d U A . C16 C 0.3524(9) 0.5358(4) 0.0631(3) 0.0643(16) Uani 1 1 d U . . C17 C 0.7341(8) 0.6092(4) 0.2588(2) 0.0523(14) Uani 1 1 d U A . C18 C 0.8677(9) 0.7473(4) 0.1060(3) 0.0587(15) Uani 1 1 d U . . C83 C 0.9979(13) 0.6510(5) 0.4469(3) 0.084(2) Uani 1 1 d U . . C19 C 0.7838(8) 0.6589(4) 0.2326(3) 0.0501(14) Uani 1 1 d U . . C20 C 0.9210(9) 0.6936(4) 0.0317(3) 0.0630(16) Uani 1 1 d U A . C84 C 0.3095(9) 0.7493(4) 0.3040(3) 0.0588(17) Uani 1 1 d U . . C21 C 0.7930(9) 0.4585(4) 0.0415(3) 0.0631(15) Uani 1 1 d U . . C22 C 0.3456(8) 0.5249(4) 0.1147(3) 0.0628(16) Uani 1 1 d U A . C23 C 0.3983(8) 0.6882(4) 0.0636(3) 0.0586(15) Uani 1 1 d U . . C24 C 0.5458(7) 0.7355(4) 0.1767(3) 0.0487(14) Uani 1 1 d U . . C25 C 0.8164(9) 0.6121(4) -0.0262(3) 0.0626(15) Uani 1 1 d U . . C26 C 0.7535(8) 0.7413(4) 0.1803(3) 0.0490(14) Uani 1 1 d U . . C27 C 0.6103(9) 0.7402(4) 0.0310(3) 0.0611(15) Uani 1 1 d U . . C28 C 0.5797(7) 0.7053(4) 0.2238(2) 0.0470(14) Uani 1 1 d U A . C29 C 0.7151(7) 0.7040(3) 0.2176(2) 0.0469(14) Uani 1 1 d U A . C85 C 0.7684(8) 0.8309(4) 0.2835(3) 0.0556(16) Uani 1 1 d U . . C86 C 0.4553(8) 0.8533(4) 0.2357(3) 0.062(2) Uani 1 1 d U . . H7 H 0.4089 0.8490 0.2642 0.093 Uiso 1 1 calc R . . H8 H 0.4480 0.8197 0.2165 0.093 Uiso 1 1 calc R . . H9 H 0.4276 0.8857 0.2181 0.093 Uiso 1 1 calc R . . C30 C 0.4512(8) 0.7151(4) 0.1469(3) 0.0543(15) Uani 1 1 d U A . C31 C 0.8981(8) 0.6530(4) 0.2111(3) 0.0536(15) Uani 1 1 d U A . C32 C 0.9503(8) 0.7158(4) 0.0788(3) 0.0605(16) Uani 1 1 d U A . C33 C 0.4046(8) 0.5731(4) 0.1884(3) 0.0552(15) Uani 1 1 d U A . C34 C 0.3241(8) 0.6431(4) 0.0785(3) 0.0610(16) Uani 1 1 d U A . C35 C 0.4903(9) 0.4645(4) 0.0815(3) 0.0626(15) Uani 1 1 d U . . C87 C 0.4218(8) 0.7631(4) 0.3177(3) 0.0563(17) Uani 1 1 d U . . C88 C 0.6478(8) 0.8181(4) 0.2727(3) 0.0523(16) Uani 1 1 d U . . C36 C 0.3413(8) 0.5923(4) 0.0463(3) 0.0616(15) Uani 1 1 d U A . C37 C 0.6334(9) 0.6604(4) -0.0245(3) 0.0603(15) Uani 1 1 d U . . C38 C 0.6716(9) 0.4513(4) 0.0388(3) 0.0617(15) Uani 1 1 d U A . C89 C 0.8789(12) 0.6512(4) 0.4560(3) 0.080(2) Uani 1 1 d U . . H10 H 0.8540 0.6589 0.4869 0.096 Uiso 1 1 calc R . . C39 C 0.7562(9) 0.6679(4) -0.0217(3) 0.0614(15) Uani 1 1 d U A . C40 C 0.6020(9) 0.4416(4) 0.0798(3) 0.0618(15) Uani 1 1 d U A . C41 C 0.4425(9) 0.5008(4) 0.0445(3) 0.0644(16) Uani 1 1 d U A . C90 C 0.3384(9) 0.7975(4) 0.3912(3) 0.0659(18) Uani 1 1 d U . . H11 H 0.3498 0.8125 0.4216 0.079 Uiso 1 1 calc R . . C91 C 0.5517(10) 0.8128(4) 0.3813(3) 0.074(3) Uani 1 1 d U . . H47 H 0.5952 0.8302 0.3558 0.110 Uiso 1 1 calc R . . H48 H 0.5970 0.7820 0.3945 0.110 Uiso 1 1 calc R . . H49 H 0.5364 0.8405 0.4057 0.110 Uiso 1 1 calc R . . C42 C 0.9877(9) 0.5097(4) 0.1409(3) 0.0629(15) Uani 1 1 d U A . C43 C 0.3310(8) 0.5715(4) 0.1467(3) 0.0591(15) Uani 1 1 d U . . C44 C 0.9084(9) 0.5019(4) 0.1809(3) 0.0600(15) Uani 1 1 d U . . C45 C 0.6091(8) 0.6026(4) -0.0320(2) 0.0597(15) Uani 1 1 d U A . C46 C 0.4577(8) 0.7257(4) 0.0955(3) 0.0578(15) Uani 1 1 d U A . C47 C 0.9267(9) 0.5382(4) 0.0166(3) 0.0612(15) Uani 1 1 d U . . C48 C 0.9166(8) 0.5965(4) -0.0011(3) 0.0620(15) Uani 1 1 d U A . C49 C 0.8145(9) 0.4638(4) 0.1739(3) 0.0607(15) Uani 1 1 d U A . C50 C 0.6516(8) 0.7724(4) 0.1069(3) 0.0576(15) Uani 1 1 d U . . C51 C 0.8346(9) 0.4992(4) 0.0083(3) 0.0608(15) Uani 1 1 d U A . C52 C 0.5083(9) 0.5759(4) -0.0121(3) 0.0601(15) Uani 1 1 d U A . C53 C 0.5167(9) 0.5167(4) 0.0047(3) 0.0614(15) Uani 1 1 d U . . C92 C 0.6354(8) 0.9134(4) 0.2403(3) 0.0554(16) Uani 1 1 d U . . H15 H 0.5909 0.9415 0.2253 0.066 Uiso 1 1 calc R . . C54 C 0.5799(8) 0.5427(4) 0.2312(3) 0.0541(15) Uani 1 1 d U A . C55 C 1.0535(9) 0.6298(4) 0.0665(3) 0.0653(16) Uani 1 1 d U A . C56 C 0.8090(9) 0.7100(4) 0.0100(3) 0.0634(16) Uani 1 1 d U . . C93 C 0.8555(9) 0.7868(4) 0.3066(3) 0.071(2) Uani 1 1 d U . . H16 H 0.9339 0.8024 0.3070 0.107 Uiso 1 1 calc R . . H17 H 0.8551 0.7523 0.2883 0.107 Uiso 1 1 calc R . . H18 H 0.8308 0.7788 0.3386 0.107 Uiso 1 1 calc R . . C57 C 1.0368(8) 0.6769(4) 0.0984(3) 0.0653(16) Uani 1 1 d U . . C94 C 0.7497(9) 0.9255(4) 0.2525(3) 0.0589(16) Uani 1 1 d U . . C58 C 0.5339(7) 0.6464(4) 0.2256(2) 0.0511(14) Uani 1 1 d U . . C59 C 0.6264(10) 0.4896(4) 0.0020(3) 0.0614(15) Uani 1 1 d U A . C95 C 0.6441(9) 0.6969(4) 0.3287(2) 0.063(2) Uani 1 1 d . . . H19 H 0.7095 0.7195 0.3406 0.075 Uiso 1 1 calc R . . H20 H 0.5882 0.6953 0.3549 0.075 Uiso 1 1 calc R . . C60 C 0.8528(9) 0.4540(4) 0.0868(3) 0.0627(15) Uani 1 1 d U A . C61 C 0.4525(8) 0.6723(4) 0.0200(3) 0.0601(15) Uani 1 1 d U A . C62 C 0.4355(8) 0.6304(4) 0.1977(3) 0.0535(15) Uani 1 1 d U A . C63 C 0.4314(9) 0.4830(4) 0.1250(3) 0.0605(15) Uani 1 1 d U A . C64 C 1.0569(9) 0.5599(4) 0.1335(3) 0.0624(16) Uani 1 1 d U . . C96 C 0.6095(11) 0.5623(4) 0.3466(3) 0.072(2) Uani 1 1 d U . . C65 C 0.5602(8) 0.6961(4) 0.0034(3) 0.0600(15) Uani 1 1 d U A . C97 C 0.4357(9) 0.7901(4) 0.3624(3) 0.0610(17) Uani 1 1 d U . . C98 C 0.2822(9) 0.7209(4) 0.2555(3) 0.070(2) Uani 1 1 d U . . H21 H 0.3231 0.7409 0.2306 0.105 Uiso 1 1 calc R . . H22 H 0.1987 0.7222 0.2496 0.105 Uiso 1 1 calc R . . H23 H 0.3080 0.6820 0.2561 0.105 Uiso 1 1 calc R . . C99 C 0.4841(11) 0.5643(4) 0.3519(3) 0.0743(19) Uani 1 1 d U . . C66 C 0.7299(9) 0.5178(4) -0.0175(3) 0.0617(15) Uani 1 1 d U . . C67 C 0.7196(9) 0.5730(4) -0.0348(3) 0.0607(15) Uani 1 1 d U A . C68 C 0.6098(9) 0.4521(4) 0.1680(3) 0.0607(15) Uani 1 1 d U . . C100 C 0.7927(11) 0.6405(4) 0.4214(3) 0.0757(19) Uani 1 1 d U . . C69 C 0.7068(9) 0.4689(4) 0.1983(3) 0.0614(15) Uani 1 1 d U A . C70 C 0.6462(8) 0.7602(4) 0.1566(3) 0.0521(14) Uani 1 1 d U A . C101 C 0.1207(11) 0.7956(5) 0.4099(4) 0.086(3) Uani 1 1 d U . . H24 H 0.1481 0.7981 0.4423 0.130 Uiso 1 1 calc R . . H25 H 0.0642 0.7652 0.4073 0.130 Uiso 1 1 calc R . . H26 H 0.0842 0.8309 0.4010 0.130 Uiso 1 1 calc R . . C102 C 1.0349(11) 0.6407(5) 0.3992(3) 0.086(2) Uani 1 1 d U . . H27 H 1.1152 0.6408 0.3921 0.103 Uiso 1 1 calc R . . C103 C 0.9549(11) 0.6307(5) 0.3636(3) 0.080(2) Uani 1 1 d U . . C104 C 0.4855(14) 0.4663(5) 0.3768(3) 0.091(2) Uani 1 1 d U . . C105 C 0.2126(9) 0.7591(4) 0.3344(3) 0.0634(18) Uani 1 1 d U . . H28 H 0.1377 0.7481 0.3243 0.076 Uiso 1 1 calc R . . C71 C 0.8602(8) 0.7350(4) 0.1564(3) 0.0534(14) Uani 1 1 d U A . C72 C 0.7334(9) 0.7476(4) 0.0342(3) 0.0610(15) Uani 1 1 d U A . C106 C 0.8110(8) 0.8844(4) 0.2742(3) 0.0586(17) Uani 1 1 d U . . H29 H 0.8879 0.8926 0.2836 0.070 Uiso 1 1 calc R . . C107 C 1.0082(11) 0.6194(5) 0.3143(3) 0.085(3) Uani 1 1 d U . . H30 H 0.9564 0.5951 0.2964 0.127 Uiso 1 1 calc R . . H31 H 1.0837 0.6012 0.3179 0.127 Uiso 1 1 calc R . . H32 H 1.0181 0.6548 0.2977 0.127 Uiso 1 1 calc R . . C73 C 0.7661(9) 0.7655(4) 0.0824(3) 0.0598(15) Uani 1 1 d U A . C74 C 0.3185(8) 0.6285(4) 0.1303(3) 0.0601(16) Uani 1 1 d U A . C108 C 0.2243(10) 0.7837(4) 0.3773(3) 0.0666(18) Uani 1 1 d U . . C109 C 0.6059(13) 0.4616(5) 0.3693(3) 0.087(2) Uani 1 1 d U . . H33 H 0.6443 0.4270 0.3738 0.105 Uiso 1 1 calc R . . C110 C 0.4268(12) 0.5175(5) 0.3669(3) 0.085(2) Uani 1 1 d U . . H34 H 0.3453 0.5191 0.3708 0.102 Uiso 1 1 calc R . . C111 C 0.8300(11) 0.6303(5) 0.3734(3) 0.076(2) Uani 1 1 d U . . C75 C 1.0605(9) 0.5724(4) 0.0837(3) 0.0647(16) Uani 1 1 d U A . C76 C 0.6601(9) 0.4333(4) 0.1241(3) 0.0618(16) Uani 1 1 d U A . C112 C 0.7984(10) 0.9830(5) 0.2418(4) 0.083(3) Uani 1 1 d U . . H35 H 0.8832 0.9813 0.2416 0.124 Uiso 1 1 calc R . . H36 H 0.7728 1.0095 0.2657 0.124 Uiso 1 1 calc R . . H37 H 0.7708 0.9954 0.2111 0.124 Uiso 1 1 calc R . . C77 C 0.5584(9) 0.7558(4) 0.0775(3) 0.0592(15) Uani 1 1 d U A . C78 C 0.7865(9) 0.4381(4) 0.1276(3) 0.0621(16) Uani 1 1 d U . . C113 C 0.6712(11) 0.6405(5) 0.4385(3) 0.085(3) Uani 1 1 d U . . H38 H 0.6637 0.6140 0.4644 0.127 Uiso 1 1 calc R . . H39 H 0.6193 0.6294 0.4130 0.127 Uiso 1 1 calc R . . H40 H 0.6506 0.6779 0.4493 0.127 Uiso 1 1 calc R . . C114 C 1.0994(13) 0.6588(6) 0.4832(4) 0.110(4) Uani 1 1 d U . . H41 H 1.0911 0.6315 0.5084 0.166 Uiso 1 1 calc R . . H42 H 1.0961 0.6966 0.4963 0.166 Uiso 1 1 calc R . . H43 H 1.1739 0.6533 0.4675 0.166 Uiso 1 1 calc R . . C115 C 0.4068(14) 0.4134(6) 0.3918(4) 0.125(4) Uani 1 1 d U . . H44 H 0.4037 0.3866 0.3659 0.188 Uiso 1 1 calc R . . H45 H 0.3283 0.4261 0.3992 0.188 Uiso 1 1 calc R . . H46 H 0.4408 0.3954 0.4193 0.188 Uiso 1 1 calc R . . S1 S 0.6941(5) 0.6936(2) -0.14019(13) 0.1278(14) Uani 1 1 d U B 1 S3 S 0.3129(4) 0.6080(2) 0.5865(2) 0.1618(19) Uani 1 1 d U C 1 S2 S 0.6247(6) 0.6376(3) -0.2333(2) 0.173(2) Uani 1 1 d U B 1 S4 S 0.3810(7) 0.5770(4) 0.4849(2) 0.236(3) Uani 1 1 d U C 1 C116 C 0.6437(17) 0.6650(7) -0.1832(5) 0.140(3) Uani 1 1 d U B 1 C117 C 0.3514(17) 0.5982(11) 0.5355(7) 0.185(4) Uani 1 1 d U C 1 S6 S 0.0827(12) 0.3871(6) 0.3565(5) 0.197(4) Uani 0.50 1 d PDU D 1 S5 S 0.1209(14) 0.5034(6) 0.3985(5) 0.202(4) Uani 0.50 1 d PDU D 1 Ce3 Ce 0.6243(18) 0.5255(8) 0.1284(5) 0.089(6) Uani 0.0433(14) 1 d P A 3 Ce4 Ce 0.7519(13) 0.6821(7) 0.0904(5) 0.076(5) Uani 0.0433(14) 1 d P A 3 C118 C 0.127(4) 0.4429(10) 0.3776(15) 0.200(4) Uani 0.50 1 d PDU . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ce1 0.0576(3) 0.0479(4) 0.0506(2) -0.0006(2) 0.00130(18) -0.0031(2) Ce2 0.0549(3) 0.0505(4) 0.0535(2) -0.0012(2) 0.00426(18) 0.0015(2) Si1 0.0695(15) 0.0378(18) 0.0450(11) -0.0030(9) 0.0007(9) 0.0073(12) Si2 0.0882(18) 0.0449(19) 0.0397(10) 0.0017(9) 0.0012(10) 0.0113(13) C79 0.160(8) 0.050(7) 0.055(5) 0.009(4) -0.013(5) 0.024(6) C1 0.065(3) 0.048(3) 0.055(3) -0.002(2) 0.006(2) 0.003(3) C2 0.070(3) 0.046(3) 0.053(3) -0.002(3) -0.007(2) 0.009(3) C3 0.073(3) 0.055(4) 0.057(3) 0.006(3) 0.017(3) -0.003(3) C4 0.077(3) 0.040(3) 0.041(2) 0.003(2) 0.010(2) 0.001(3) C5 0.068(3) 0.044(3) 0.054(3) -0.006(3) -0.002(3) -0.009(3) C6 0.079(3) 0.048(3) 0.063(3) -0.006(3) 0.007(3) 0.018(3) C7 0.084(3) 0.038(3) 0.043(3) 0.004(2) 0.002(2) 0.009(3) C8 0.075(3) 0.040(3) 0.052(3) 0.003(2) 0.014(3) -0.013(3) C9 0.080(3) 0.043(3) 0.051(3) 0.000(3) -0.004(3) 0.013(3) C80 0.114(7) 0.052(7) 0.065(5) 0.009(4) 0.014(5) -0.005(5) C10 0.089(3) 0.039(3) 0.046(3) 0.008(2) 0.006(3) 0.007(3) C81 0.065(3) 0.040(4) 0.053(3) -0.006(3) -0.001(3) 0.002(3) C11 0.078(3) 0.053(3) 0.063(3) -0.007(3) 0.013(3) 0.011(3) C12 0.071(3) 0.050(3) 0.064(3) -0.008(3) 0.003(3) -0.005(3) C13 0.071(3) 0.061(3) 0.053(3) -0.002(3) -0.012(2) 0.002(3) C82 0.146(5) 0.048(5) 0.045(3) 0.003(3) -0.019(3) -0.005(4) C14 0.068(3) 0.050(3) 0.063(3) -0.009(3) 0.001(2) 0.007(3) C15 0.079(3) 0.037(3) 0.057(3) 0.003(2) 0.009(3) -0.013(3) C16 0.075(3) 0.052(4) 0.066(3) -0.007(3) -0.002(3) -0.009(3) C17 0.077(3) 0.039(3) 0.041(2) -0.001(2) 0.002(2) 0.006(3) C18 0.073(3) 0.043(3) 0.060(3) 0.007(3) 0.005(3) -0.018(3) C83 0.127(5) 0.072(4) 0.054(3) -0.002(3) -0.021(4) 0.010(4) C19 0.069(3) 0.037(3) 0.044(3) -0.007(2) -0.002(2) 0.003(3) C20 0.078(3) 0.053(3) 0.058(3) 0.011(3) 0.015(3) -0.014(3) C84 0.082(4) 0.039(4) 0.056(3) 0.000(3) 0.011(3) 0.001(3) C21 0.089(3) 0.047(3) 0.054(3) -0.011(3) 0.005(3) 0.009(3) C22 0.071(3) 0.050(3) 0.067(3) -0.004(3) 0.006(3) -0.014(3) C23 0.066(3) 0.051(3) 0.059(3) 0.004(3) -0.011(2) 0.010(3) C24 0.065(3) 0.034(3) 0.047(3) -0.001(2) 0.001(2) 0.011(3) C25 0.086(3) 0.056(4) 0.047(3) 0.004(3) 0.013(2) 0.000(3) C26 0.067(3) 0.031(3) 0.049(3) 0.001(2) -0.001(2) -0.001(3) C27 0.083(3) 0.050(3) 0.051(3) 0.015(2) -0.002(3) 0.006(3) C28 0.063(3) 0.034(3) 0.044(2) -0.001(2) 0.001(2) 0.009(3) C29 0.067(3) 0.031(3) 0.043(2) -0.002(2) 0.001(2) 0.003(3) C85 0.069(3) 0.042(4) 0.056(3) -0.010(3) -0.002(3) 0.005(3) C86 0.077(6) 0.045(6) 0.063(4) -0.002(4) -0.002(4) 0.007(4) C30 0.067(3) 0.042(3) 0.054(3) 0.002(3) 0.000(2) 0.009(3) C31 0.070(3) 0.043(3) 0.048(3) -0.008(2) -0.005(2) 0.000(3) C32 0.073(3) 0.047(3) 0.062(3) 0.007(3) 0.011(3) -0.020(3) C33 0.068(3) 0.045(3) 0.053(3) -0.004(3) 0.015(2) -0.011(3) C34 0.062(3) 0.055(4) 0.066(3) -0.005(3) -0.009(3) 0.004(3) C35 0.084(3) 0.043(3) 0.061(3) -0.010(3) 0.001(3) -0.013(3) C87 0.080(4) 0.038(4) 0.050(3) 0.001(3) 0.007(3) 0.004(3) C88 0.064(3) 0.040(4) 0.053(3) -0.008(3) 0.003(3) 0.002(3) C36 0.066(3) 0.056(4) 0.063(3) -0.008(3) -0.008(2) -0.001(3) C37 0.085(3) 0.054(3) 0.042(2) 0.009(2) -0.002(3) -0.001(3) C38 0.086(3) 0.044(3) 0.055(3) -0.012(3) 0.004(3) 0.002(3) C89 0.130(5) 0.062(4) 0.049(3) -0.002(3) -0.011(4) 0.008(4) C39 0.086(3) 0.054(3) 0.043(3) 0.009(3) 0.010(3) -0.003(3) C40 0.086(3) 0.040(3) 0.059(3) -0.009(3) 0.002(3) -0.004(3) C41 0.081(3) 0.048(3) 0.064(3) -0.010(3) -0.003(3) -0.010(3) C90 0.095(4) 0.047(4) 0.056(3) -0.002(3) 0.013(3) 0.007(3) C91 0.114(7) 0.052(6) 0.054(4) -0.012(4) 0.006(4) 0.015(5) C42 0.079(3) 0.047(3) 0.062(3) 0.000(3) 0.001(3) 0.017(3) C43 0.066(3) 0.050(4) 0.062(3) -0.004(3) 0.009(3) -0.011(3) C44 0.081(3) 0.043(3) 0.056(3) 0.003(3) 0.000(3) 0.018(3) C45 0.082(3) 0.055(3) 0.042(2) 0.000(3) -0.005(2) -0.007(3) C46 0.073(3) 0.045(3) 0.056(3) 0.006(3) -0.005(2) 0.013(3) C47 0.082(3) 0.051(3) 0.051(3) -0.007(3) 0.015(3) 0.008(3) C48 0.079(3) 0.056(3) 0.050(3) 0.001(3) 0.018(2) 0.002(3) C49 0.090(3) 0.035(3) 0.057(3) 0.006(3) 0.006(3) 0.016(3) C50 0.079(3) 0.038(3) 0.056(3) 0.005(3) 0.001(3) 0.000(3) C51 0.087(3) 0.045(3) 0.050(3) -0.008(3) 0.010(3) 0.009(3) C52 0.075(3) 0.055(3) 0.050(3) -0.007(2) -0.009(3) -0.003(3) C53 0.082(3) 0.049(3) 0.054(3) -0.011(3) -0.004(3) -0.007(3) C92 0.072(3) 0.038(4) 0.056(3) -0.003(3) 0.004(3) 0.002(3) C54 0.081(3) 0.037(3) 0.044(3) 0.003(2) 0.013(2) -0.004(3) C55 0.072(3) 0.057(4) 0.067(3) -0.002(3) 0.016(3) -0.006(3) C56 0.084(3) 0.054(3) 0.052(3) 0.013(3) 0.015(3) -0.005(3) C93 0.075(6) 0.052(6) 0.086(5) -0.003(4) -0.012(5) 0.012(5) C57 0.072(3) 0.055(4) 0.068(3) -0.002(3) 0.010(3) -0.013(3) C94 0.071(4) 0.041(4) 0.065(3) -0.006(3) 0.001(3) -0.002(3) C58 0.067(3) 0.043(3) 0.044(3) 0.000(2) 0.008(2) 0.003(3) C59 0.087(3) 0.046(3) 0.052(3) -0.015(2) 0.000(3) 0.000(3) C95 0.099(7) 0.049(7) 0.040(4) -0.003(3) 0.006(4) 0.016(5) C60 0.087(3) 0.043(3) 0.059(3) -0.005(3) 0.004(3) 0.014(3) C61 0.071(3) 0.056(3) 0.053(3) 0.001(3) -0.015(2) 0.007(3) C62 0.066(3) 0.046(3) 0.049(3) -0.003(3) 0.010(2) -0.002(3) C63 0.077(3) 0.041(3) 0.063(3) -0.004(3) 0.007(3) -0.017(3) C64 0.072(3) 0.052(4) 0.064(3) -0.005(3) 0.005(3) 0.010(3) C96 0.135(5) 0.043(5) 0.039(3) 0.007(3) -0.010(3) -0.006(4) C65 0.079(3) 0.054(3) 0.046(3) 0.011(3) -0.007(3) 0.003(3) C97 0.088(4) 0.041(4) 0.054(3) 0.000(3) 0.008(3) 0.009(3) C98 0.088(6) 0.060(6) 0.062(5) -0.011(4) 0.005(4) 0.008(5) C99 0.131(5) 0.045(5) 0.047(3) 0.010(3) -0.010(3) -0.018(4) C66 0.090(3) 0.046(3) 0.049(3) -0.011(3) 0.005(3) 0.005(3) C67 0.088(3) 0.051(3) 0.044(3) -0.003(3) 0.004(3) -0.003(3) C68 0.087(3) 0.035(3) 0.060(3) 0.006(3) 0.007(3) -0.005(3) C100 0.124(5) 0.058(4) 0.044(3) -0.001(3) -0.009(3) 0.017(4) C69 0.093(3) 0.035(3) 0.056(3) 0.006(3) 0.007(3) 0.009(3) C70 0.073(3) 0.032(3) 0.051(3) 0.000(2) -0.001(2) 0.004(3) C101 0.110(7) 0.069(7) 0.080(5) -0.018(5) 0.035(5) -0.008(6) C102 0.120(5) 0.078(4) 0.058(3) -0.002(3) -0.022(3) 0.017(4) C103 0.114(4) 0.075(4) 0.052(3) -0.001(3) -0.019(3) 0.022(4) C104 0.155(5) 0.055(5) 0.064(3) 0.011(3) -0.029(4) -0.029(4) C105 0.088(4) 0.043(4) 0.060(3) -0.003(3) 0.013(3) 0.003(3) C71 0.068(3) 0.038(3) 0.054(3) 0.001(2) -0.001(3) -0.012(3) C72 0.084(3) 0.046(3) 0.052(3) 0.015(3) 0.006(3) -0.004(3) C106 0.068(4) 0.043(4) 0.064(3) -0.008(3) -0.002(3) -0.004(3) C107 0.104(7) 0.086(7) 0.064(5) -0.002(4) -0.015(5) 0.025(6) C73 0.079(3) 0.041(3) 0.060(3) 0.010(3) 0.006(3) -0.009(3) C74 0.062(3) 0.053(4) 0.065(3) -0.004(3) 0.001(3) -0.004(3) C108 0.091(4) 0.047(4) 0.062(3) 0.000(3) 0.021(3) 0.004(3) C109 0.154(5) 0.050(5) 0.058(3) 0.004(3) -0.030(4) -0.016(4) C110 0.141(5) 0.056(5) 0.058(3) 0.013(3) -0.019(4) -0.024(4) C111 0.118(5) 0.065(4) 0.044(3) -0.001(3) -0.012(3) 0.022(4) C75 0.074(3) 0.053(4) 0.067(3) -0.009(3) 0.012(3) 0.008(3) C76 0.091(3) 0.035(3) 0.060(3) -0.002(3) 0.005(3) -0.001(3) C112 0.084(6) 0.069(7) 0.095(6) -0.003(5) 0.012(5) -0.013(5) C77 0.079(3) 0.044(3) 0.054(3) 0.006(3) -0.004(3) 0.007(3) C78 0.091(3) 0.036(3) 0.059(3) -0.001(3) 0.002(3) 0.010(3) C113 0.134(8) 0.075(7) 0.046(4) 0.000(4) 0.004(5) 0.015(6) C114 0.152(9) 0.103(8) 0.076(6) 0.004(5) -0.033(6) -0.010(7) C115 0.187(9) 0.092(8) 0.097(7) 0.026(6) -0.040(7) -0.045(7) S1 0.166(4) 0.121(3) 0.096(2) 0.009(2) 0.012(2) 0.004(3) S3 0.111(3) 0.189(5) 0.185(4) -0.029(4) -0.002(3) 0.039(3) S2 0.181(5) 0.184(5) 0.153(4) -0.011(3) -0.042(4) -0.018(4) S4 0.212(6) 0.314(8) 0.183(5) 0.039(5) 0.039(5) 0.119(6) C116 0.174(7) 0.135(7) 0.111(6) -0.012(6) -0.023(6) 0.004(7) C117 0.143(7) 0.255(8) 0.159(7) -0.002(8) 0.029(7) 0.080(7) S6 0.197(4) 0.197(4) 0.196(4) 0.0019(10) 0.0013(11) 0.0009(10) S5 0.203(4) 0.201(4) 0.203(4) -0.0014(10) 0.0005(11) -0.0004(10) Ce3 0.115(13) 0.081(13) 0.071(8) -0.018(7) 0.017(8) -0.004(10) Ce4 0.080(10) 0.076(12) 0.072(8) 0.019(7) 0.014(6) -0.009(8) C118 0.200(4) 0.200(4) 0.200(4) 0.0000(10) -0.0001(10) -0.0003(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ce1 C74 2.466(9) . ? Ce1 C43 2.480(8) . ? Ce1 C34 2.504(9) . ? Ce1 C36 2.504(8) . ? Ce1 C22 2.553(9) . ? Ce1 C16 2.555(9) . ? Ce1 C1 2.754(8) . ? Ce1 C23 2.754(9) . ? Ce1 C33 2.766(7) . ? Ce1 C13 2.808(8) . ? Ce1 C41 2.874(9) . ? Ce1 C63 2.881(9) . ? Ce2 C64 2.479(9) . ? Ce2 C14 2.481(8) . ? Ce2 C75 2.485(9) . ? Ce2 C12 2.502(10) . ? Ce2 C55 2.543(9) . ? Ce2 C57 2.545(9) . ? Ce2 C2 2.750(7) . ? Ce2 C5 2.756(9) . ? Ce2 C42 2.778(9) . ? Ce2 C11 2.807(9) . ? Ce2 C32 2.875(9) . ? Ce2 C3 2.894(8) . ? Si1 C95 1.905(8) . ? Si1 C88 1.920(9) . ? Si1 C87 1.937(9) . ? Si1 C28 1.985(7) . ? Si2 C95 1.877(9) . ? Si2 C96 1.879(11) . ? Si2 C111 1.903(10) . ? Si2 C17 1.982(7) . ? C79 C82 1.492(16) . ? C79 H1 0.9600 . ? C79 H2 0.9600 . ? C79 H3 0.9600 . ? C1 C62 1.430(12) . ? C1 C30 1.430(13) . ? C1 C74 1.461(12) . ? C2 C14 1.396(11) . ? C2 C31 1.441(12) . ? C2 C9 1.481(13) . ? C3 C20 1.416(13) . ? C3 C48 1.417(13) . ? C3 C55 1.492(13) . ? C4 C58 1.407(12) . ? C4 C54 1.442(12) . ? C4 C17 1.551(12) . ? C5 C71 1.423(13) . ? C5 C31 1.460(12) . ? C5 C12 1.480(12) . ? C6 C11 1.433(13) . ? C6 C60 1.439(14) . ? C6 C42 1.441(12) . ? C7 C9 1.351(12) . ? C7 C10 1.421(13) . ? C7 C17 1.562(11) . ? C8 C54 1.416(12) . ? C8 C33 1.428(13) . ? C8 C15 1.453(12) . ? C8 Ce3 2.592(17) . ? C9 C44 1.455(12) . ? C80 C99 1.422(14) . ? C80 H4 0.9600 . ? C80 H5 0.9600 . ? C80 H6 0.9600 . ? C10 C69 1.417(13) . ? C10 C54 1.430(13) . ? C10 Ce3 2.970(17) . ? C81 C92 1.363(12) . ? C81 C88 1.426(12) . ? C81 C86 1.513(12) . ? C11 C47 1.426(13) . ? C11 C75 1.442(14) . ? C12 C57 1.429(12) . ? C12 C14 1.460(14) . ? C13 C52 1.417(13) . ? C13 C61 1.459(14) . ? C13 C36 1.479(13) . ? C82 C109 1.339(15) . ? C82 C96 1.452(15) . ? C14 C64 1.474(13) . ? C15 C68 1.407(14) . ? C15 C63 1.455(13) . ? C15 Ce3 2.08(2) . ? C16 C41 1.410(14) . ? C16 C36 1.415(13) . ? C16 C22 1.474(12) . ? C17 C19 1.489(12) . ? C18 C73 1.394(13) . ? C18 C32 1.416(13) . ? C18 C71 1.444(11) . ? C18 Ce4 2.063(18) . ? C83 C89 1.371(16) . ? C83 C102 1.421(14) . ? C83 C114 1.547(15) . ? C19 C29 1.381(11) . ? C19 C31 1.435(12) . ? C20 C32 1.458(13) . ? C20 C56 1.458(13) . ? C20 Ce4 2.538(15) . ? C84 C87 1.367(13) . ? C84 C105 1.407(12) . ? C84 C98 1.547(11) . ? C21 C38 1.387(14) . ? C21 C51 1.415(13) . ? C21 C60 1.444(13) . ? C22 C63 1.412(14) . ? C22 C43 1.426(13) . ? C23 C61 1.416(12) . ? C23 C34 1.417(13) . ? C23 C46 1.425(12) . ? C24 C70 1.396(12) . ? C24 C30 1.440(12) . ? C24 C28 1.548(10) . ? C25 C48 1.384(13) . ? C25 C67 1.450(13) . ? C25 C39 1.482(13) . ? C26 C71 1.389(12) . ? C26 C29 1.432(11) . ? C26 C70 1.454(12) . ? C26 Ce4 2.881(17) . ? C27 C72 1.407(13) . ? C27 C65 1.411(13) . ? C27 C77 1.477(12) . ? C27 Ce4 2.684(17) . ? C28 C58 1.476(12) . ? C28 C29 1.543(11) . ? C85 C106 1.371(13) . ? C85 C88 1.430(12) . ? C85 C93 1.569(12) . ? C86 H7 0.9600 . ? C86 H8 0.9600 . ? C86 H9 0.9600 . ? C30 C46 1.465(11) . ? C32 C57 1.447(14) . ? C32 Ce4 2.402(17) . ? C33 C62 1.414(12) . ? C33 C43 1.437(12) . ? C34 C74 1.492(13) . ? C34 C36 1.509(13) . ? C35 C40 1.375(14) . ? C35 C41 1.448(13) . ? C35 C63 1.458(12) . ? C35 Ce3 2.47(2) . ? C87 C97 1.413(12) . ? C37 C45 1.402(13) . ? C37 C39 1.403(13) . ? C37 C65 1.415(13) . ? C38 C40 1.412(13) . ? C38 C59 1.463(13) . ? C89 C100 1.399(14) . ? C89 H10 0.9300 . ? C39 C56 1.458(13) . ? C40 C76 1.419(12) . ? C40 Ce3 2.409(18) . ? C41 C53 1.445(13) . ? C90 C97 1.378(12) . ? C90 C108 1.388(14) . ? C90 H11 0.9300 . ? C91 C97 1.514(14) . ? C91 H47 0.9600 . ? C91 H48 0.9600 . ? C91 H49 0.9600 . ? C42 C64 1.429(14) . ? C42 C44 1.449(13) . ? C43 C74 1.423(13) . ? C44 C49 1.404(14) . ? C45 C52 1.416(13) . ? C45 C67 1.434(13) . ? C46 C77 1.433(13) . ? C47 C51 1.407(13) . ? C47 C48 1.460(13) . ? C49 C69 1.404(13) . ? C49 C78 1.467(12) . ? C49 Ce3 2.89(2) . ? C50 C77 1.393(12) . ? C50 C70 1.425(11) . ? C50 C73 1.475(13) . ? C50 Ce4 2.449(19) . ? C51 C66 1.456(13) . ? C52 C53 1.472(13) . ? C53 C59 1.396(14) . ? C92 C94 1.368(12) . ? C92 H15 0.9300 . ? C54 Ce3 2.953(15) . ? C55 C75 1.434(14) . ? C55 C57 1.435(13) . ? C56 C72 1.406(13) . ? C56 Ce4 2.435(14) . ? C93 H16 0.9600 . ? C93 H17 0.9600 . ? C93 H18 0.9600 . ? C94 C106 1.337(13) . ? C94 C112 1.490(14) . ? C58 C62 1.412(11) . ? C59 C66 1.452(14) . ? C95 H19 0.9700 . ? C95 H20 0.9700 . ? C60 C78 1.416(13) . ? C61 C65 1.420(13) . ? C63 Ce3 2.40(2) . ? C64 C75 1.430(12) . ? C96 C99 1.429(16) . ? C98 H21 0.9600 . ? C98 H22 0.9600 . ? C98 H23 0.9600 . ? C99 C110 1.344(14) . ? C66 C67 1.388(13) . ? C68 C76 1.426(12) . ? C68 C69 1.445(13) . ? C68 Ce3 2.06(2) . ? C100 C111 1.431(13) . ? C100 C113 1.456(15) . ? C69 Ce3 2.55(2) . ? C70 Ce4 2.872(18) . ? C101 C108 1.514(13) . ? C101 H24 0.9600 . ? C101 H25 0.9600 . ? C101 H26 0.9600 . ? C102 C103 1.369(14) . ? C102 H27 0.9300 . ? C103 C111 1.439(16) . ? C103 C107 1.532(14) . ? C104 C109 1.383(18) . ? C104 C110 1.402(17) . ? C104 C115 1.586(17) . ? C105 C108 1.342(12) . ? C105 H28 0.9300 . ? C71 Ce4 2.544(17) . ? C72 C73 1.464(12) . ? C72 Ce4 2.211(16) . ? C106 H29 0.9300 . ? C107 H30 0.9600 . ? C107 H31 0.9600 . ? C107 H32 0.9600 . ? C73 Ce4 1.979(19) . ? C109 H33 0.9300 . ? C110 H34 0.9300 . ? C76 C78 1.438(14) . ? C76 Ce3 2.21(2) . ? C112 H35 0.9600 . ? C112 H36 0.9600 . ? C112 H37 0.9600 . ? C77 Ce4 2.815(18) . ? C78 Ce3 2.75(2) . ? C113 H38 0.9600 . ? C113 H39 0.9600 . ? C113 H40 0.9600 . ? C114 H41 0.9600 . ? C114 H42 0.9600 . ? C114 H43 0.9600 . ? C115 H44 0.9600 . ? C115 H45 0.9600 . ? C115 H46 0.9600 . ? S1 C116 1.494(16) . ? S3 C117 1.512(19) . ? S2 C116 1.560(16) . ? S4 C117 1.54(2) . ? S6 C118 1.524(10) . ? S5 C118 1.540(10) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C74 Ce1 C43 33.4(3) . . ? C74 Ce1 C34 34.9(3) . . ? C43 Ce1 C34 61.5(3) . . ? C74 Ce1 C36 60.9(3) . . ? C43 Ce1 C36 70.1(3) . . ? C34 Ce1 C36 35.1(3) . . ? C74 Ce1 C22 59.5(3) . . ? C43 Ce1 C22 32.9(3) . . ? C34 Ce1 C22 71.8(3) . . ? C36 Ce1 C22 59.0(3) . . ? C74 Ce1 C16 70.7(3) . . ? C43 Ce1 C16 59.6(3) . . ? C34 Ce1 C16 61.2(3) . . ? C36 Ce1 C16 32.5(3) . . ? C22 Ce1 C16 33.5(3) . . ? C74 Ce1 C1 31.9(3) . . ? C43 Ce1 C1 52.9(3) . . ? C34 Ce1 C1 56.4(3) . . ? C36 Ce1 C1 89.5(3) . . ? C22 Ce1 C1 85.3(3) . . ? C16 Ce1 C1 102.5(3) . . ? C74 Ce1 C23 57.1(3) . . ? C43 Ce1 C23 89.2(3) . . ? C34 Ce1 C23 30.8(3) . . ? C36 Ce1 C23 53.9(3) . . ? C22 Ce1 C23 102.5(3) . . ? C16 Ce1 C23 85.8(3) . . ? C1 Ce1 C23 61.2(3) . . ? C74 Ce1 C33 51.9(3) . . ? C43 Ce1 C33 31.2(3) . . ? C34 Ce1 C33 86.3(3) . . ? C36 Ce1 C33 101.2(3) . . ? C22 Ce1 C33 54.7(3) . . ? C16 Ce1 C33 87.2(3) . . ? C1 Ce1 C33 49.7(3) . . ? C23 Ce1 C33 106.6(3) . . ? C74 Ce1 C13 86.1(3) . . ? C43 Ce1 C13 101.6(3) . . ? C34 Ce1 C13 52.2(3) . . ? C36 Ce1 C13 31.7(3) . . ? C22 Ce1 C13 87.4(3) . . ? C16 Ce1 C13 55.1(3) . . ? C1 Ce1 C13 106.7(3) . . ? C23 Ce1 C13 49.9(3) . . ? C33 Ce1 C13 132.6(3) . . ? C74 Ce1 C41 99.9(3) . . ? C43 Ce1 C41 82.6(3) . . ? C34 Ce1 C41 87.4(3) . . ? C36 Ce1 C41 53.3(3) . . ? C22 Ce1 C41 50.3(3) . . ? C16 Ce1 C41 29.4(3) . . ? C1 Ce1 C41 131.3(3) . . ? C23 Ce1 C41 104.9(3) . . ? C33 Ce1 C41 102.6(3) . . ? C13 Ce1 C41 59.3(3) . . ? C74 Ce1 C63 85.8(3) . . ? C43 Ce1 C63 53.7(3) . . ? C34 Ce1 C63 101.0(3) . . ? C36 Ce1 C63 81.8(3) . . ? C22 Ce1 C63 29.3(3) . . ? C16 Ce1 C63 50.0(3) . . ? C1 Ce1 C63 104.3(3) . . ? C23 Ce1 C63 131.3(3) . . ? C33 Ce1 C63 59.0(3) . . ? C13 Ce1 C63 102.8(3) . . ? C41 Ce1 C63 47.2(3) . . ? C64 Ce2 C14 34.6(3) . . ? C64 Ce2 C75 33.5(3) . . ? C14 Ce2 C75 60.4(3) . . ? C64 Ce2 C12 60.5(3) . . ? C14 Ce2 C12 34.1(3) . . ? C75 Ce2 C12 69.5(3) . . ? C64 Ce2 C55 59.7(3) . . ? C14 Ce2 C55 70.2(3) . . ? C75 Ce2 C55 33.1(3) . . ? C12 Ce2 C55 58.0(3) . . ? C64 Ce2 C57 71.3(3) . . ? C14 Ce2 C57 60.7(3) . . ? C75 Ce2 C57 59.7(3) . . ? C12 Ce2 C57 32.9(3) . . ? C55 Ce2 C57 32.8(3) . . ? C64 Ce2 C2 55.8(3) . . ? C14 Ce2 C2 30.4(3) . . ? C75 Ce2 C2 87.6(3) . . ? C12 Ce2 C2 52.6(3) . . ? C55 Ce2 C2 100.4(3) . . ? C57 Ce2 C2 85.1(3) . . ? C64 Ce2 C5 86.8(3) . . ? C14 Ce2 C5 53.0(3) . . ? C75 Ce2 C5 101.7(3) . . ? C12 Ce2 C5 32.2(3) . . ? C55 Ce2 C5 86.5(3) . . ? C57 Ce2 C5 54.9(3) . . ? C2 Ce2 C5 50.5(3) . . ? C64 Ce2 C42 30.9(3) . . ? C14 Ce2 C42 56.1(3) . . ? C75 Ce2 C42 52.2(3) . . ? C12 Ce2 C42 88.4(3) . . ? C55 Ce2 C42 84.7(3) . . ? C57 Ce2 C42 102.0(3) . . ? C2 Ce2 C42 60.6(3) . . ? C5 Ce2 C42 107.1(3) . . ? C64 Ce2 C11 51.8(3) . . ? C14 Ce2 C11 85.6(3) . . ? C75 Ce2 C11 30.9(3) . . ? C12 Ce2 C11 100.3(3) . . ? C55 Ce2 C11 54.6(3) . . ? C57 Ce2 C11 86.6(3) . . ? C2 Ce2 C11 105.7(3) . . ? C5 Ce2 C11 132.4(3) . . ? C42 Ce2 C11 49.7(3) . . ? C64 Ce2 C32 101.4(3) . . ? C14 Ce2 C32 87.5(3) . . ? C75 Ce2 C32 83.8(3) . . ? C12 Ce2 C32 54.3(3) . . ? C55 Ce2 C32 51.1(3) . . ? C57 Ce2 C32 30.2(3) . . ? C2 Ce2 C32 104.5(3) . . ? C5 Ce2 C32 58.5(3) . . ? C42 Ce2 C32 131.8(3) . . ? C11 Ce2 C32 103.0(3) . . ? C64 Ce2 C3 87.0(3) . . ? C14 Ce2 C3 101.1(3) . . ? C75 Ce2 C3 54.5(3) . . ? C12 Ce2 C3 82.9(3) . . ? C55 Ce2 C3 31.0(3) . . ? C57 Ce2 C3 50.7(3) . . ? C2 Ce2 C3 131.0(3) . . ? C5 Ce2 C3 103.1(3) . . ? C42 Ce2 C3 104.3(3) . . ? C11 Ce2 C3 58.5(3) . . ? C32 Ce2 C3 48.3(3) . . ? C95 Si1 C88 116.5(4) . . ? C95 Si1 C87 101.4(4) . . ? C88 Si1 C87 108.6(4) . . ? C95 Si1 C28 102.7(3) . . ? C88 Si1 C28 104.3(3) . . ? C87 Si1 C28 123.9(4) . . ? C95 Si2 C96 118.4(5) . . ? C95 Si2 C111 100.6(4) . . ? C96 Si2 C111 107.9(5) . . ? C95 Si2 C17 103.0(3) . . ? C96 Si2 C17 104.0(4) . . ? C111 Si2 C17 124.0(4) . . ? C82 C79 H1 109.5 . . ? C82 C79 H2 109.5 . . ? H1 C79 H2 109.5 . . ? C82 C79 H3 109.5 . . ? H1 C79 H3 109.5 . . ? H2 C79 H3 109.5 . . ? C62 C1 C30 118.4(8) . . ? C62 C1 C74 106.0(8) . . ? C30 C1 C74 125.6(8) . . ? C62 C1 Ce1 82.6(5) . . ? C30 C1 Ce1 92.1(5) . . ? C74 C1 Ce1 63.1(5) . . ? C14 C2 C31 108.8(8) . . ? C14 C2 C9 126.2(8) . . ? C31 C2 C9 114.5(7) . . ? C14 C2 Ce2 64.1(4) . . ? C31 C2 Ce2 82.8(4) . . ? C9 C2 Ce2 91.0(5) . . ? C20 C3 C48 120.7(9) . . ? C20 C3 C55 106.7(8) . . ? C48 C3 C55 124.2(9) . . ? C20 C3 Ce2 85.7(5) . . ? C48 C3 Ce2 93.0(5) . . ? C55 C3 Ce2 61.4(4) . . ? C58 C4 C54 122.4(8) . . ? C58 C4 C17 123.0(8) . . ? C54 C4 C17 111.0(7) . . ? C71 C5 C31 120.4(8) . . ? C71 C5 C12 125.6(8) . . ? C31 C5 C12 106.7(8) . . ? C71 C5 Ce2 95.2(5) . . ? C31 C5 Ce2 82.3(5) . . ? C12 C5 Ce2 64.4(5) . . ? C11 C6 C60 121.9(9) . . ? C11 C6 C42 109.6(9) . . ? C60 C6 C42 121.9(8) . . ? C11 C6 Ce2 68.4(5) . . ? C60 C6 Ce2 107.5(6) . . ? C42 C6 Ce2 67.2(5) . . ? C9 C7 C10 120.9(8) . . ? C9 C7 C17 125.5(8) . . ? C10 C7 C17 106.8(8) . . ? C54 C8 C33 117.0(8) . . ? C54 C8 C15 116.9(9) . . ? C33 C8 C15 119.3(8) . . ? C54 C8 Ce3 90.0(6) . . ? C33 C8 Ce3 101.8(6) . . ? C15 C8 Ce3 53.2(6) . . ? C7 C9 C44 120.7(9) . . ? C7 C9 C2 119.8(8) . . ? C44 C9 C2 114.9(8) . . ? C99 C80 H4 109.5 . . ? C99 C80 H5 109.5 . . ? H4 C80 H5 109.5 . . ? C99 C80 H6 109.5 . . ? H4 C80 H6 109.5 . . ? H5 C80 H6 109.5 . . ? C69 C10 C7 120.1(9) . . ? C69 C10 C54 117.4(9) . . ? C7 C10 C54 113.3(8) . . ? C69 C10 Ce3 59.0(6) . . ? C7 C10 Ce3 108.5(6) . . ? C54 C10 Ce3 75.4(6) . . ? C92 C81 C88 120.3(8) . . ? C92 C81 C86 119.2(8) . . ? C88 C81 C86 120.4(9) . . ? C47 C11 C6 120.2(10) . . ? C47 C11 C75 125.1(9) . . ? C6 C11 C75 106.5(8) . . ? C47 C11 Ce2 94.9(6) . . ? C6 C11 Ce2 83.3(5) . . ? C75 C11 Ce2 62.1(5) . . ? C57 C12 C14 123.1(8) . . ? C57 C12 C5 114.9(8) . . ? C14 C12 C5 106.1(8) . . ? C57 C12 Ce2 75.2(5) . . ? C14 C12 Ce2 72.2(5) . . ? C5 C12 Ce2 83.4(5) . . ? C52 C13 C61 122.2(9) . . ? C52 C13 C36 121.8(9) . . ? C61 C13 C36 108.0(8) . . ? C52 C13 Ce1 94.5(5) . . ? C61 C13 Ce1 83.0(5) . . ? C36 C13 Ce1 62.8(4) . . ? C109 C82 C96 122.6(12) . . ? C109 C82 C79 114.2(11) . . ? C96 C82 C79 123.1(10) . . ? C2 C14 C12 110.0(8) . . ? C2 C14 C64 117.7(9) . . ? C12 C14 C64 117.8(7) . . ? C2 C14 Ce2 85.5(5) . . ? C12 C14 Ce2 73.8(5) . . ? C64 C14 Ce2 72.6(5) . . ? C68 C15 C8 119.7(8) . . ? C68 C15 C63 118.6(8) . . ? C8 C15 C63 115.5(9) . . ? C68 C15 Ce3 69.3(7) . . ? C8 C15 Ce3 92.7(7) . . ? C63 C15 Ce3 83.7(7) . . ? C41 C16 C36 119.2(9) . . ? C41 C16 C22 107.5(8) . . ? C36 C16 C22 119.1(8) . . ? C41 C16 Ce1 88.0(6) . . ? C36 C16 Ce1 71.8(5) . . ? C22 C16 Ce1 73.2(5) . . ? C19 C17 C4 108.0(7) . . ? C19 C17 C7 110.1(6) . . ? C4 C17 C7 99.8(7) . . ? C19 C17 Si2 114.2(6) . . ? C4 C17 Si2 98.9(5) . . ? C7 C17 Si2 122.8(5) . . ? C73 C18 C32 116.7(8) . . ? C73 C18 C71 118.5(8) . . ? C32 C18 C71 117.4(8) . . ? C73 C18 Ce4 66.6(7) . . ? C32 C18 Ce4 85.2(7) . . ? C71 C18 Ce4 91.3(6) . . ? C89 C83 C102 117.7(10) . . ? C89 C83 C114 127.3(10) . . ? C102 C83 C114 114.9(12) . . ? C29 C19 C31 117.0(8) . . ? C29 C19 C17 122.6(8) . . ? C31 C19 C17 118.2(7) . . ? C3 C20 C32 110.4(8) . . ? C3 C20 C56 123.6(9) . . ? C32 C20 C56 118.9(9) . . ? C3 C20 Ce4 109.1(7) . . ? C32 C20 Ce4 67.8(6) . . ? C56 C20 Ce4 69.1(6) . . ? C87 C84 C105 121.1(8) . . ? C87 C84 C98 122.3(8) . . ? C105 C84 C98 116.6(9) . . ? C38 C21 C51 112.1(9) . . ? C38 C21 C60 120.2(9) . . ? C51 C21 C60 118.3(9) . . ? C63 C22 C43 119.0(8) . . ? C63 C22 C16 106.7(8) . . ? C43 C22 C16 119.4(9) . . ? C63 C22 Ce1 88.3(6) . . ? C43 C22 Ce1 70.7(5) . . ? C16 C22 Ce1 73.3(5) . . ? C61 C23 C34 108.4(8) . . ? C61 C23 C46 120.1(9) . . ? C34 C23 C46 123.8(8) . . ? C61 C23 Ce1 85.8(6) . . ? C34 C23 Ce1 64.8(5) . . ? C46 C23 Ce1 90.9(5) . . ? C70 C24 C30 120.6(7) . . ? C70 C24 C28 109.5(7) . . ? C30 C24 C28 121.9(8) . . ? C48 C25 C67 122.4(9) . . ? C48 C25 C39 124.6(9) . . ? C67 C25 C39 103.1(8) . . ? C71 C26 C29 123.5(8) . . ? C71 C26 C70 122.5(7) . . ? C29 C26 C70 105.5(7) . . ? C71 C26 Ce4 62.0(5) . . ? C29 C26 Ce4 110.0(6) . . ? C70 C26 Ce4 75.0(5) . . ? C72 C27 C65 121.6(9) . . ? C72 C27 C77 107.8(8) . . ? C65 C27 C77 120.5(9) . . ? C72 C27 Ce4 55.4(5) . . ? C65 C27 Ce4 102.0(7) . . ? C77 C27 Ce4 79.4(6) . . ? C58 C28 C29 109.6(6) . . ? C58 C28 C24 111.8(7) . . ? C29 C28 C24 99.1(6) . . ? C58 C28 Si1 114.5(5) . . ? C29 C28 Si1 99.7(5) . . ? C24 C28 Si1 119.7(6) . . ? C19 C29 C26 121.4(8) . . ? C19 C29 C28 122.6(7) . . ? C26 C29 C28 111.9(7) . . ? C106 C85 C88 119.1(8) . . ? C106 C85 C93 117.5(8) . . ? C88 C85 C93 123.3(9) . . ? C81 C86 H7 109.5 . . ? C81 C86 H8 109.5 . . ? H7 C86 H8 109.5 . . ? C81 C86 H9 109.5 . . ? H7 C86 H9 109.5 . . ? H8 C86 H9 109.5 . . ? C1 C30 C24 118.9(7) . . ? C1 C30 C46 116.6(8) . . ? C24 C30 C46 118.5(8) . . ? C19 C31 C2 125.7(8) . . ? C19 C31 C5 120.8(8) . . ? C2 C31 C5 108.3(7) . . ? C19 C31 Ce2 108.7(5) . . ? C2 C31 Ce2 68.1(4) . . ? C5 C31 Ce2 68.3(4) . . ? C18 C32 C57 124.9(8) . . ? C18 C32 C20 121.7(9) . . ? C57 C32 C20 105.8(8) . . ? C18 C32 Ce4 58.8(6) . . ? C57 C32 Ce4 112.0(7) . . ? C20 C32 Ce4 78.0(6) . . ? C18 C32 Ce2 93.6(5) . . ? C57 C32 Ce2 62.2(5) . . ? C20 C32 Ce2 85.6(5) . . ? Ce4 C32 Ce2 50.3(4) . . ? C62 C33 C8 120.0(8) . . ? C62 C33 C43 108.5(8) . . ? C8 C33 C43 123.3(8) . . ? C62 C33 Ce1 82.3(5) . . ? C8 C33 Ce1 94.8(5) . . ? C43 C33 Ce1 63.3(4) . . ? C23 C34 C74 119.0(8) . . ? C23 C34 C36 109.6(8) . . ? C74 C34 C36 114.1(9) . . ? C23 C34 Ce1 84.4(5) . . ? C74 C34 Ce1 71.1(5) . . ? C36 C34 Ce1 72.5(5) . . ? C40 C35 C41 123.2(9) . . ? C40 C35 C63 124.5(9) . . ? C41 C35 C63 104.8(9) . . ? C40 C35 Ce3 71.3(7) . . ? C41 C35 Ce3 105.7(7) . . ? C63 C35 Ce3 70.2(6) . . ? C84 C87 C97 117.3(8) . . ? C84 C87 Si1 128.4(6) . . ? C97 C87 Si1 114.2(7) . . ? C81 C88 C85 115.7(8) . . ? C81 C88 Si1 118.3(7) . . ? C85 C88 Si1 126.0(7) . . ? C16 C36 C13 118.6(9) . . ? C16 C36 C34 123.6(8) . . ? C13 C36 C34 104.0(8) . . ? C16 C36 Ce1 75.7(5) . . ? C13 C36 Ce1 85.6(5) . . ? C34 C36 Ce1 72.4(5) . . ? C45 C37 C39 108.9(9) . . ? C45 C37 C65 122.8(9) . . ? C39 C37 C65 118.3(8) . . ? C21 C38 C40 121.9(9) . . ? C21 C38 C59 108.0(9) . . ? C40 C38 C59 118.6(9) . . ? C83 C89 C100 123.7(9) . . ? C83 C89 H10 118.1 . . ? C100 C89 H10 118.1 . . ? C37 C39 C56 121.7(8) . . ? C37 C39 C25 109.9(8) . . ? C56 C39 C25 117.6(9) . . ? C35 C40 C38 118.6(9) . . ? C35 C40 C76 116.7(8) . . ? C38 C40 C76 118.4(10) . . ? C35 C40 Ce3 75.9(7) . . ? C38 C40 Ce3 105.7(7) . . ? C76 C40 Ce3 64.4(6) . . ? C16 C41 C53 123.8(9) . . ? C16 C41 C35 110.3(8) . . ? C53 C41 C35 119.2(9) . . ? C16 C41 Ce1 62.7(5) . . ? C53 C41 Ce1 94.1(6) . . ? C35 C41 Ce1 87.0(5) . . ? C97 C90 C108 123.3(8) . . ? C97 C90 H11 118.4 . . ? C108 C90 H11 118.4 . . ? C97 C91 H47 109.5 . . ? C97 C91 H48 109.5 . . ? H47 C91 H48 109.5 . . ? C97 C91 H49 109.5 . . ? H47 C91 H49 109.5 . . ? H48 C91 H49 109.5 . . ? C64 C42 C6 106.4(8) . . ? C64 C42 C44 123.8(8) . . ? C6 C42 C44 120.1(9) . . ? C64 C42 Ce2 62.9(5) . . ? C6 C42 Ce2 84.3(5) . . ? C44 C42 Ce2 90.7(6) . . ? C74 C43 C22 122.1(8) . . ? C74 C43 C33 107.3(8) . . ? C22 C43 C33 117.8(9) . . ? C74 C43 Ce1 72.7(5) . . ? C22 C43 Ce1 76.4(5) . . ? C33 C43 Ce1 85.5(5) . . ? C49 C44 C42 116.2(8) . . ? C49 C44 C9 117.5(9) . . ? C42 C44 C9 119.4(9) . . ? C37 C45 C52 121.9(8) . . ? C37 C45 C67 107.9(8) . . ? C52 C45 C67 120.6(9) . . ? C23 C46 C77 117.4(8) . . ? C23 C46 C30 119.3(9) . . ? C77 C46 C30 118.1(8) . . ? C51 C47 C11 116.1(9) . . ? C51 C47 C48 119.7(9) . . ? C11 C47 C48 117.6(9) . . ? C25 C48 C3 116.8(9) . . ? C25 C48 C47 119.0(9) . . ? C3 C48 C47 118.0(8) . . ? C44 C49 C69 122.3(8) . . ? C44 C49 C78 123.3(9) . . ? C69 C49 C78 106.3(9) . . ? C44 C49 Ce3 107.8(7) . . ? C69 C49 Ce3 61.7(6) . . ? C78 C49 Ce3 69.8(6) . . ? C77 C50 C70 119.4(8) . . ? C77 C50 C73 111.1(8) . . ? C70 C50 C73 118.1(8) . . ? C77 C50 Ce4 89.9(7) . . ? C70 C50 Ce4 91.8(6) . . ? C73 C50 Ce4 53.9(6) . . ? C47 C51 C21 125.2(8) . . ? C47 C51 C66 119.3(9) . . ? C21 C51 C66 105.0(9) . . ? C45 C52 C13 115.6(9) . . ? C45 C52 C53 119.5(9) . . ? C13 C52 C53 118.8(8) . . ? C59 C53 C41 116.2(9) . . ? C59 C53 C52 118.0(9) . . ? C41 C53 C52 117.0(9) . . ? C81 C92 C94 123.1(9) . . ? C81 C92 H15 118.5 . . ? C94 C92 H15 118.5 . . ? C8 C54 C10 124.5(8) . . ? C8 C54 C4 120.5(8) . . ? C10 C54 C4 105.6(8) . . ? C8 C54 Ce3 61.3(5) . . ? C10 C54 Ce3 76.7(6) . . ? C4 C54 Ce3 108.6(6) . . ? C75 C55 C57 121.4(8) . . ? C75 C55 C3 116.7(8) . . ? C57 C55 C3 106.9(9) . . ? C75 C55 Ce2 71.2(5) . . ? C57 C55 Ce2 73.7(5) . . ? C3 C55 Ce2 87.6(5) . . ? C72 C56 C39 118.1(9) . . ? C72 C56 C20 119.5(8) . . ? C39 C56 C20 115.6(9) . . ? C72 C56 Ce4 63.8(6) . . ? C39 C56 Ce4 105.8(7) . . ? C20 C56 Ce4 76.9(6) . . ? C85 C93 H16 109.5 . . ? C85 C93 H17 109.5 . . ? H16 C93 H17 109.5 . . ? C85 C93 H18 109.5 . . ? H16 C93 H18 109.5 . . ? H17 C93 H18 109.5 . . ? C12 C57 C55 117.4(9) . . ? C12 C57 C32 119.0(8) . . ? C55 C57 C32 109.8(8) . . ? C12 C57 Ce2 71.9(5) . . ? C55 C57 Ce2 73.5(5) . . ? C32 C57 Ce2 87.7(6) . . ? C106 C94 C92 117.0(9) . . ? C106 C94 C112 123.7(10) . . ? C92 C94 C112 119.3(9) . . ? C4 C58 C62 115.6(8) . . ? C4 C58 C28 121.2(8) . . ? C62 C58 C28 120.5(8) . . ? C53 C59 C66 122.0(9) . . ? C53 C59 C38 123.5(8) . . ? C66 C59 C38 105.4(9) . . ? Si2 C95 Si1 137.2(4) . . ? Si2 C95 H19 102.8 . . ? Si1 C95 H19 102.8 . . ? Si2 C95 H20 102.8 . . ? Si1 C95 H20 102.8 . . ? H19 C95 H20 105.0 . . ? C78 C60 C6 117.5(8) . . ? C78 C60 C21 118.8(10) . . ? C6 C60 C21 117.3(9) . . ? C23 C61 C65 123.4(9) . . ? C23 C61 C13 109.4(8) . . ? C65 C61 C13 119.5(9) . . ? C23 C61 Ce1 66.1(5) . . ? C65 C61 Ce1 106.8(5) . . ? C13 C61 Ce1 68.1(4) . . ? C58 C62 C33 123.4(8) . . ? C58 C62 C1 123.0(8) . . ? C33 C62 C1 109.3(8) . . ? C58 C62 Ce1 110.0(5) . . ? C33 C62 Ce1 69.1(4) . . ? C1 C62 Ce1 68.5(4) . . ? C22 C63 C15 124.6(8) . . ? C22 C63 C35 110.5(8) . . ? C15 C63 C35 116.6(9) . . ? C22 C63 Ce3 110.1(8) . . ? C15 C63 Ce3 59.3(6) . . ? C35 C63 Ce3 75.0(6) . . ? C22 C63 Ce1 62.4(5) . . ? C15 C63 Ce1 92.5(5) . . ? C35 C63 Ce1 86.6(5) . . ? Ce3 C63 Ce1 48.2(5) . . ? C42 C64 C75 109.1(8) . . ? C42 C64 C14 117.9(8) . . ? C75 C64 C14 118.7(9) . . ? C42 C64 Ce2 86.2(6) . . ? C75 C64 Ce2 73.5(5) . . ? C14 C64 Ce2 72.8(5) . . ? C99 C96 C82 116.7(9) . . ? C99 C96 Si2 125.9(8) . . ? C82 C96 Si2 117.3(9) . . ? C27 C65 C37 120.2(9) . . ? C27 C65 C61 117.0(8) . . ? C37 C65 C61 116.8(9) . . ? C90 C97 C87 119.3(9) . . ? C90 C97 C91 116.2(8) . . ? C87 C97 C91 124.5(8) . . ? C84 C98 H21 109.5 . . ? C84 C98 H22 109.5 . . ? H21 C98 H22 109.5 . . ? C84 C98 H23 109.5 . . ? H21 C98 H23 109.5 . . ? H22 C98 H23 109.5 . . ? C110 C99 C80 118.3(12) . . ? C110 C99 C96 119.0(11) . . ? C80 C99 C96 122.7(9) . . ? C67 C66 C59 119.3(9) . . ? C67 C66 C51 121.5(9) . . ? C59 C66 C51 109.4(8) . . ? C66 C67 C45 120.4(9) . . ? C66 C67 C25 118.0(9) . . ? C45 C67 C25 110.1(8) . . ? C15 C68 C76 120.7(8) . . ? C15 C68 C69 121.7(8) . . ? C76 C68 C69 106.9(9) . . ? C15 C68 Ce3 70.9(7) . . ? C76 C68 Ce3 76.2(6) . . ? C69 C68 Ce3 91.6(8) . . ? C89 C100 C111 118.4(11) . . ? C89 C100 C113 115.5(9) . . ? C111 C100 C113 126.1(10) . . ? C49 C69 C10 118.2(9) . . ? C49 C69 C68 110.4(8) . . ? C10 C69 C68 119.7(9) . . ? C49 C69 Ce3 89.2(7) . . ? C10 C69 Ce3 92.6(6) . . ? C68 C69 Ce3 53.8(6) . . ? C24 C70 C50 120.9(8) . . ? C24 C70 C26 111.6(7) . . ? C50 C70 C26 118.2(8) . . ? C24 C70 Ce4 109.5(6) . . ? C50 C70 Ce4 58.5(5) . . ? C26 C70 Ce4 75.7(5) . . ? C108 C101 H24 109.5 . . ? C108 C101 H25 109.5 . . ? H24 C101 H25 109.5 . . ? C108 C101 H26 109.5 . . ? H24 C101 H26 109.5 . . ? H25 C101 H26 109.5 . . ? C103 C102 C83 121.3(12) . . ? C103 C102 H27 119.3 . . ? C83 C102 H27 119.3 . . ? C102 C103 C111 120.8(9) . . ? C102 C103 C107 115.3(11) . . ? C111 C103 C107 123.9(9) . . ? C109 C104 C110 120.3(11) . . ? C109 C104 C115 122.1(12) . . ? C110 C104 C115 117.3(13) . . ? C108 C105 C84 122.4(10) . . ? C108 C105 H28 118.8 . . ? C84 C105 H28 118.8 . . ? C26 C71 C5 116.0(7) . . ? C26 C71 C18 120.1(8) . . ? C5 C71 C18 117.5(8) . . ? C26 C71 Ce4 89.1(6) . . ? C5 C71 Ce4 103.5(7) . . ? C18 C71 Ce4 54.2(5) . . ? C56 C72 C27 119.6(9) . . ? C56 C72 C73 118.3(9) . . ? C27 C72 C73 110.2(8) . . ? C56 C72 Ce4 81.4(7) . . ? C27 C72 Ce4 93.1(7) . . ? C73 C72 Ce4 61.2(6) . . ? C94 C106 C85 124.6(9) . . ? C94 C106 H29 117.7 . . ? C85 C106 H29 117.7 . . ? C103 C107 H30 109.5 . . ? C103 C107 H31 109.5 . . ? H30 C107 H31 109.5 . . ? C103 C107 H32 109.5 . . ? H30 C107 H32 109.5 . . ? H31 C107 H32 109.5 . . ? C18 C73 C72 123.9(9) . . ? C18 C73 C50 122.5(7) . . ? C72 C73 C50 103.8(8) . . ? C18 C73 Ce4 73.1(7) . . ? C72 C73 Ce4 78.4(7) . . ? C50 C73 Ce4 89.1(7) . . ? C43 C74 C1 108.8(8) . . ? C43 C74 C34 121.8(8) . . ? C1 C74 C34 115.1(8) . . ? C43 C74 Ce1 73.8(5) . . ? C1 C74 Ce1 85.0(5) . . ? C34 C74 Ce1 73.9(5) . . ? C105 C108 C90 116.5(9) . . ? C105 C108 C101 123.1(10) . . ? C90 C108 C101 120.5(9) . . ? C82 C109 C104 118.8(12) . . ? C82 C109 H33 120.6 . . ? C104 C109 H33 120.6 . . ? C99 C110 C104 122.4(13) . . ? C99 C110 H34 118.8 . . ? C104 C110 H34 118.8 . . ? C100 C111 C103 117.9(9) . . ? C100 C111 Si2 115.7(9) . . ? C103 C111 Si2 126.2(7) . . ? C64 C75 C55 121.5(8) . . ? C64 C75 C11 108.2(9) . . ? C55 C75 C11 118.1(9) . . ? C64 C75 Ce2 73.0(5) . . ? C55 C75 Ce2 75.7(5) . . ? C11 C75 Ce2 87.0(6) . . ? C40 C76 C68 121.9(9) . . ? C40 C76 C78 120.6(8) . . ? C68 C76 C78 108.3(8) . . ? C40 C76 Ce3 80.1(7) . . ? C68 C76 Ce3 64.9(6) . . ? C78 C76 Ce3 95.8(8) . . ? C94 C112 H35 109.5 . . ? C94 C112 H36 109.5 . . ? H35 C112 H36 109.5 . . ? C94 C112 H37 109.5 . . ? H35 C112 H37 109.5 . . ? H36 C112 H37 109.5 . . ? C50 C77 C46 122.1(7) . . ? C50 C77 C27 106.9(8) . . ? C46 C77 C27 120.2(9) . . ? C50 C77 Ce4 60.5(6) . . ? C46 C77 Ce4 105.7(6) . . ? C27 C77 Ce4 69.6(6) . . ? C60 C78 C76 119.5(8) . . ? C60 C78 C49 119.5(9) . . ? C76 C78 C49 107.9(8) . . ? C60 C78 Ce3 99.4(7) . . ? C76 C78 Ce3 52.9(6) . . ? C49 C78 Ce3 80.3(6) . . ? C100 C113 H38 109.5 . . ? C100 C113 H39 109.5 . . ? H38 C113 H39 109.5 . . ? C100 C113 H40 109.5 . . ? H38 C113 H40 109.5 . . ? H39 C113 H40 109.5 . . ? C83 C114 H41 109.5 . . ? C83 C114 H42 109.5 . . ? H41 C114 H42 109.5 . . ? C83 C114 H43 109.5 . . ? H41 C114 H43 109.5 . . ? H42 C114 H43 109.5 . . ? C104 C115 H44 109.5 . . ? C104 C115 H45 109.5 . . ? H44 C115 H45 109.5 . . ? C104 C115 H46 109.5 . . ? H44 C115 H46 109.5 . . ? H45 C115 H46 109.5 . . ? S1 C116 S2 164.9(15) . . ? S3 C117 S4 169(2) . . ? C68 Ce3 C15 39.8(5) . . ? C68 Ce3 C76 38.9(5) . . ? C15 Ce3 C76 70.1(7) . . ? C68 Ce3 C63 66.5(7) . . ? C15 Ce3 C63 37.0(4) . . ? C76 Ce3 C63 76.0(7) . . ? C68 Ce3 C40 67.1(6) . . ? C15 Ce3 C40 79.9(7) . . ? C76 Ce3 C40 35.5(4) . . ? C63 Ce3 C40 62.8(6) . . ? C68 Ce3 C35 75.6(7) . . ? C15 Ce3 C35 65.4(6) . . ? C76 Ce3 C35 60.9(6) . . ? C63 Ce3 C35 34.8(4) . . ? C40 Ce3 C35 32.7(4) . . ? C68 Ce3 C69 34.5(4) . . ? C15 Ce3 C69 64.2(6) . . ? C76 Ce3 C69 57.5(5) . . ? C63 Ce3 C69 98.4(7) . . ? C40 Ce3 C69 92.7(7) . . ? C35 Ce3 C69 109.5(8) . . ? C68 Ce3 C8 63.0(5) . . ? C15 Ce3 C8 34.1(4) . . ? C76 Ce3 C8 100.4(7) . . ? C63 Ce3 C8 58.9(5) . . ? C40 Ce3 C8 113.7(8) . . ? C35 Ce3 C8 93.3(7) . . ? C69 Ce3 C8 68.3(5) . . ? C68 Ce3 C78 55.5(6) . . ? C15 Ce3 C78 94.4(8) . . ? C76 Ce3 C78 31.3(4) . . ? C63 Ce3 C78 107.2(7) . . ? C40 Ce3 C78 57.0(5) . . ? C35 Ce3 C78 88.4(6) . . ? C69 Ce3 C78 51.2(5) . . ? C8 Ce3 C78 115.8(7) . . ? C68 Ce3 C49 53.2(6) . . ? C15 Ce3 C49 90.5(7) . . ? C76 Ce3 C49 52.8(5) . . ? C63 Ce3 C49 119.1(8) . . ? C40 Ce3 C49 85.3(6) . . ? C35 Ce3 C49 113.7(7) . . ? C69 Ce3 C49 29.0(3) . . ? C8 Ce3 C49 97.0(6) . . ? C78 Ce3 C49 30.0(3) . . ? C68 Ce3 C54 64.9(5) . . ? C15 Ce3 C54 54.9(4) . . ? C76 Ce3 C54 102.7(7) . . ? C63 Ce3 C54 86.6(6) . . ? C40 Ce3 C54 130.3(8) . . ? C35 Ce3 C54 119.7(7) . . ? C69 Ce3 C54 51.8(4) . . ? C8 Ce3 C54 28.7(3) . . ? C78 Ce3 C54 102.9(6) . . ? C49 Ce3 C54 76.4(5) . . ? C68 Ce3 C10 55.5(5) . . ? C15 Ce3 C10 67.1(5) . . ? C76 Ce3 C10 85.7(6) . . ? C63 Ce3 C10 103.9(6) . . ? C40 Ce3 C10 120.3(8) . . ? C35 Ce3 C10 128.7(7) . . ? C69 Ce3 C10 28.5(3) . . ? C8 Ce3 C10 53.3(4) . . ? C78 Ce3 C10 76.9(5) . . ? C49 Ce3 C10 48.8(4) . . ? C54 Ce3 C10 27.9(3) . . ? C73 Ce4 C18 40.3(5) . . ? C73 Ce4 C72 40.4(4) . . ? C18 Ce4 C72 72.3(6) . . ? C73 Ce4 C32 65.4(6) . . ? C18 Ce4 C32 36.0(4) . . ? C72 Ce4 C32 76.3(5) . . ? C73 Ce4 C56 66.9(5) . . ? C18 Ce4 C56 80.1(5) . . ? C72 Ce4 C56 34.8(4) . . ? C32 Ce4 C56 62.5(4) . . ? C73 Ce4 C50 37.0(4) . . ? C18 Ce4 C50 67.1(6) . . ? C72 Ce4 C50 59.2(5) . . ? C32 Ce4 C50 100.0(7) . . ? C56 Ce4 C50 93.8(6) . . ? C73 Ce4 C20 76.2(5) . . ? C18 Ce4 C20 65.2(5) . . ? C72 Ce4 C20 62.3(5) . . ? C32 Ce4 C20 34.2(4) . . ? C56 Ce4 C20 34.0(3) . . ? C50 Ce4 C20 112.3(6) . . ? C73 Ce4 C71 63.9(6) . . ? C18 Ce4 C71 34.6(4) . . ? C72 Ce4 C71 103.0(7) . . ? C32 Ce4 C71 59.2(5) . . ? C56 Ce4 C71 114.5(6) . . ? C50 Ce4 C71 70.3(5) . . ? C20 Ce4 C71 93.2(6) . . ? C73 Ce4 C27 58.4(5) . . ? C18 Ce4 C27 97.7(7) . . ? C72 Ce4 C27 31.6(4) . . ? C32 Ce4 C27 107.9(6) . . ? C56 Ce4 C27 56.5(4) . . ? C50 Ce4 C27 53.2(4) . . ? C20 Ce4 C27 89.7(5) . . ? C71 Ce4 C27 119.4(7) . . ? C73 Ce4 C77 55.9(5) . . ? C18 Ce4 C77 93.7(7) . . ? C72 Ce4 C77 53.6(5) . . ? C32 Ce4 C77 120.5(7) . . ? C56 Ce4 C77 85.6(5) . . ? C50 Ce4 C77 29.7(3) . . ? C20 Ce4 C77 116.0(6) . . ? C71 Ce4 C77 99.7(6) . . ? C27 Ce4 C77 31.1(3) . . ? C73 Ce4 C70 58.2(5) . . ? C18 Ce4 C70 69.7(6) . . ? C72 Ce4 C70 88.7(6) . . ? C32 Ce4 C70 105.5(6) . . ? C56 Ce4 C70 122.5(7) . . ? C50 Ce4 C70 29.7(3) . . ? C20 Ce4 C70 131.7(7) . . ? C71 Ce4 C70 54.4(4) . . ? C27 Ce4 C70 80.1(5) . . ? C77 Ce4 C70 50.6(4) . . ? C73 Ce4 C26 67.7(6) . . ? C18 Ce4 C26 56.7(5) . . ? C72 Ce4 C26 106.8(7) . . ? C32 Ce4 C26 87.3(6) . . ? C56 Ce4 C26 132.8(7) . . ? C50 Ce4 C26 54.5(4) . . ? C20 Ce4 C26 120.8(6) . . ? C71 Ce4 C26 28.8(3) . . ? C27 Ce4 C26 107.6(6) . . ? C77 Ce4 C26 79.6(5) . . ? C70 Ce4 C26 29.3(3) . . ? S6 C118 S5 158(3) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C74 Ce1 C1 C62 112.3(8) . . . . ? C43 Ce1 C1 C62 72.2(6) . . . . ? C34 Ce1 C1 C62 149.7(6) . . . . ? C36 Ce1 C1 C62 137.3(6) . . . . ? C22 Ce1 C1 C62 78.4(5) . . . . ? C16 Ce1 C1 C62 107.4(5) . . . . ? C23 Ce1 C1 C62 -174.6(6) . . . . ? C33 Ce1 C1 C62 32.1(5) . . . . ? C13 Ce1 C1 C62 164.3(5) . . . . ? C41 Ce1 C1 C62 100.7(6) . . . . ? C63 Ce1 C1 C62 55.9(6) . . . . ? C74 Ce1 C1 C30 -129.4(8) . . . . ? C43 Ce1 C1 C30 -169.5(7) . . . . ? C34 Ce1 C1 C30 -92.0(6) . . . . ? C36 Ce1 C1 C30 -104.3(5) . . . . ? C22 Ce1 C1 C30 -163.3(5) . . . . ? C16 Ce1 C1 C30 -134.3(5) . . . . ? C23 Ce1 C1 C30 -56.2(5) . . . . ? C33 Ce1 C1 C30 150.4(7) . . . . ? C13 Ce1 C1 C30 -77.4(5) . . . . ? C41 Ce1 C1 C30 -140.9(5) . . . . ? C63 Ce1 C1 C30 174.3(5) . . . . ? C43 Ce1 C1 C74 -40.1(6) . . . . ? C34 Ce1 C1 C74 37.4(6) . . . . ? C36 Ce1 C1 C74 25.1(6) . . . . ? C22 Ce1 C1 C74 -33.9(6) . . . . ? C16 Ce1 C1 C74 -4.9(6) . . . . ? C23 Ce1 C1 C74 73.2(6) . . . . ? C33 Ce1 C1 C74 -80.2(6) . . . . ? C13 Ce1 C1 C74 52.0(6) . . . . ? C41 Ce1 C1 C74 -11.5(7) . . . . ? C63 Ce1 C1 C74 -56.4(6) . . . . ? C64 Ce2 C2 C14 36.1(6) . . . . ? C75 Ce2 C2 C14 25.1(6) . . . . ? C12 Ce2 C2 C14 -40.7(6) . . . . ? C55 Ce2 C2 C14 -5.6(7) . . . . ? C57 Ce2 C2 C14 -34.6(6) . . . . ? C5 Ce2 C2 C14 -82.1(6) . . . . ? C42 Ce2 C2 C14 72.2(6) . . . . ? C11 Ce2 C2 C14 50.4(6) . . . . ? C32 Ce2 C2 C14 -57.9(6) . . . . ? C3 Ce2 C2 C14 -11.2(8) . . . . ? C64 Ce2 C2 C31 151.1(7) . . . . ? C14 Ce2 C2 C31 115.0(8) . . . . ? C75 Ce2 C2 C31 140.1(6) . . . . ? C12 Ce2 C2 C31 74.3(5) . . . . ? C55 Ce2 C2 C31 109.4(5) . . . . ? C57 Ce2 C2 C31 80.4(5) . . . . ? C5 Ce2 C2 C31 32.9(5) . . . . ? C42 Ce2 C2 C31 -172.8(6) . . . . ? C11 Ce2 C2 C31 165.4(5) . . . . ? C32 Ce2 C2 C31 57.1(5) . . . . ? C3 Ce2 C2 C31 103.8(5) . . . . ? C64 Ce2 C2 C9 -94.3(6) . . . . ? C14 Ce2 C2 C9 -130.4(8) . . . . ? C75 Ce2 C2 C9 -105.3(5) . . . . ? C12 Ce2 C2 C9 -171.1(6) . . . . ? C55 Ce2 C2 C9 -136.0(5) . . . . ? C57 Ce2 C2 C9 -165.1(5) . . . . ? C5 Ce2 C2 C9 147.5(6) . . . . ? C42 Ce2 C2 C9 -58.3(5) . . . . ? C11 Ce2 C2 C9 -80.0(5) . . . . ? C32 Ce2 C2 C9 171.7(5) . . . . ? C3 Ce2 C2 C9 -141.6(5) . . . . ? C64 Ce2 C3 C20 -138.4(6) . . . . ? C14 Ce2 C3 C20 -106.7(6) . . . . ? C75 Ce2 C3 C20 -147.5(7) . . . . ? C12 Ce2 C3 C20 -77.7(6) . . . . ? C55 Ce2 C3 C20 -111.7(8) . . . . ? C57 Ce2 C3 C20 -70.1(6) . . . . ? C2 Ce2 C3 C20 -100.9(6) . . . . ? C5 Ce2 C3 C20 -52.4(6) . . . . ? C42 Ce2 C3 C20 -164.2(6) . . . . ? C11 Ce2 C3 C20 175.6(7) . . . . ? C32 Ce2 C3 C20 -30.2(5) . . . . ? C64 Ce2 C3 C48 101.0(6) . . . . ? C14 Ce2 C3 C48 132.8(6) . . . . ? C75 Ce2 C3 C48 91.9(7) . . . . ? C12 Ce2 C3 C48 161.7(7) . . . . ? C55 Ce2 C3 C48 127.7(9) . . . . ? C57 Ce2 C3 C48 169.3(8) . . . . ? C2 Ce2 C3 C48 138.5(6) . . . . ? C5 Ce2 C3 C48 -173.0(6) . . . . ? C42 Ce2 C3 C48 75.3(6) . . . . ? C11 Ce2 C3 C48 55.0(6) . . . . ? C32 Ce2 C3 C48 -150.8(8) . . . . ? C64 Ce2 C3 C55 -26.7(6) . . . . ? C14 Ce2 C3 C55 5.0(6) . . . . ? C75 Ce2 C3 C55 -35.8(5) . . . . ? C12 Ce2 C3 C55 34.0(6) . . . . ? C57 Ce2 C3 C55 41.6(6) . . . . ? C2 Ce2 C3 C55 10.8(7) . . . . ? C5 Ce2 C3 C55 59.3(6) . . . . ? C42 Ce2 C3 C55 -52.5(6) . . . . ? C11 Ce2 C3 C55 -72.7(6) . . . . ? C32 Ce2 C3 C55 81.5(6) . . . . ? C64 Ce2 C5 C71 160.7(6) . . . . ? C14 Ce2 C5 C71 168.7(7) . . . . ? C75 Ce2 C5 C71 130.5(5) . . . . ? C12 Ce2 C5 C71 127.2(8) . . . . ? C55 Ce2 C5 C71 100.9(6) . . . . ? C57 Ce2 C5 C71 91.3(6) . . . . ? C2 Ce2 C5 C71 -152.5(7) . . . . ? C42 Ce2 C5 C71 -175.8(5) . . . . ? C11 Ce2 C5 C71 133.6(5) . . . . ? C32 Ce2 C5 C71 55.3(5) . . . . ? C3 Ce2 C5 C71 74.6(6) . . . . ? C64 Ce2 C5 C31 -79.3(5) . . . . ? C14 Ce2 C5 C31 -71.3(6) . . . . ? C75 Ce2 C5 C31 -109.5(5) . . . . ? C12 Ce2 C5 C31 -112.8(8) . . . . ? C55 Ce2 C5 C31 -139.1(6) . . . . ? C57 Ce2 C5 C31 -148.7(7) . . . . ? C2 Ce2 C5 C31 -32.5(5) . . . . ? C42 Ce2 C5 C31 -55.8(6) . . . . ? C11 Ce2 C5 C31 -106.4(5) . . . . ? C32 Ce2 C5 C31 175.3(6) . . . . ? C3 Ce2 C5 C31 -165.4(5) . . . . ? C64 Ce2 C5 C12 33.5(6) . . . . ? C14 Ce2 C5 C12 41.4(5) . . . . ? C75 Ce2 C5 C12 3.3(6) . . . . ? C55 Ce2 C5 C12 -26.3(6) . . . . ? C57 Ce2 C5 C12 -35.9(5) . . . . ? C2 Ce2 C5 C12 80.3(6) . . . . ? C42 Ce2 C5 C12 57.0(6) . . . . ? C11 Ce2 C5 C12 6.4(7) . . . . ? C32 Ce2 C5 C12 -71.9(6) . . . . ? C3 Ce2 C5 C12 -52.6(6) . . . . ? C64 Ce2 C6 C11 -84.4(7) . . . . ? C14 Ce2 C6 C11 -97.3(6) . . . . ? C75 Ce2 C6 C11 -39.1(6) . . . . ? C12 Ce2 C6 C11 -76.9(6) . . . . ? C55 Ce2 C6 C11 -26.0(6) . . . . ? C57 Ce2 C6 C11 -42.2(7) . . . . ? C2 Ce2 C6 C11 -126.7(6) . . . . ? C5 Ce2 C6 C11 -100.6(6) . . . . ? C42 Ce2 C6 C11 -124.0(9) . . . . ? C32 Ce2 C6 C11 -18.3(7) . . . . ? C3 Ce2 C6 C11 4.5(6) . . . . ? C64 Ce2 C6 C60 157.5(7) . . . . ? C14 Ce2 C6 C60 144.6(6) . . . . ? C75 Ce2 C6 C60 -157.2(7) . . . . ? C12 Ce2 C6 C60 165.0(6) . . . . ? C55 Ce2 C6 C60 -144.1(6) . . . . ? C57 Ce2 C6 C60 -160.3(6) . . . . ? C2 Ce2 C6 C60 115.2(6) . . . . ? C5 Ce2 C6 C60 141.3(5) . . . . ? C42 Ce2 C6 C60 117.9(9) . . . . ? C11 Ce2 C6 C60 -118.1(9) . . . . ? C32 Ce2 C6 C60 -136.4(5) . . . . ? C3 Ce2 C6 C60 -113.6(6) . . . . ? C64 Ce2 C6 C42 39.6(6) . . . . ? C14 Ce2 C6 C42 26.7(6) . . . . ? C75 Ce2 C6 C42 84.8(7) . . . . ? C12 Ce2 C6 C42 47.1(6) . . . . ? C55 Ce2 C6 C42 98.0(6) . . . . ? C57 Ce2 C6 C42 81.8(6) . . . . ? C2 Ce2 C6 C42 -2.8(6) . . . . ? C5 Ce2 C6 C42 23.4(7) . . . . ? C11 Ce2 C6 C42 124.0(9) . . . . ? C32 Ce2 C6 C42 105.7(6) . . . . ? C3 Ce2 C6 C42 128.4(6) . . . . ? C10 C7 C9 C44 -6.0(12) . . . . ? C17 C7 C9 C44 -153.2(8) . . . . ? C10 C7 C9 C2 148.5(8) . . . . ? C17 C7 C9 C2 1.4(12) . . . . ? C14 C2 C9 C7 -157.2(8) . . . . ? C31 C2 C9 C7 -16.6(10) . . . . ? Ce2 C2 C9 C7 -99.1(7) . . . . ? C14 C2 C9 C44 -1.2(12) . . . . ? C31 C2 C9 C44 139.3(8) . . . . ? Ce2 C2 C9 C44 56.8(7) . . . . ? C9 C7 C10 C69 6.4(13) . . . . ? C17 C7 C10 C69 158.9(7) . . . . ? C9 C7 C10 C54 -139.4(8) . . . . ? C17 C7 C10 C54 13.1(9) . . . . ? C9 C7 C10 Ce3 -57.8(10) . . . . ? C17 C7 C10 Ce3 94.7(7) . . . . ? C60 C6 C11 C47 5.9(13) . . . . ? C42 C6 C11 C47 -146.0(9) . . . . ? Ce2 C6 C11 C47 -91.8(8) . . . . ? C60 C6 C11 C75 156.0(9) . . . . ? C42 C6 C11 C75 4.1(11) . . . . ? Ce2 C6 C11 C75 58.3(6) . . . . ? C60 C6 C11 Ce2 97.8(8) . . . . ? C42 C6 C11 Ce2 -54.2(7) . . . . ? C64 Ce2 C11 C47 -168.7(8) . . . . ? C14 Ce2 C11 C47 -160.7(7) . . . . ? C75 Ce2 C11 C47 -127.4(9) . . . . ? C12 Ce2 C11 C47 -129.9(6) . . . . ? C55 Ce2 C11 C47 -92.0(7) . . . . ? C57 Ce2 C11 C47 -99.9(7) . . . . ? C2 Ce2 C11 C47 176.2(6) . . . . ? C5 Ce2 C11 C47 -133.4(6) . . . . ? C42 Ce2 C11 C47 151.2(8) . . . . ? C32 Ce2 C11 C47 -74.4(7) . . . . ? C3 Ce2 C11 C47 -54.9(6) . . . . ? C64 Ce2 C11 C6 71.4(6) . . . . ? C14 Ce2 C11 C6 79.4(6) . . . . ? C75 Ce2 C11 C6 112.7(9) . . . . ? C12 Ce2 C11 C6 110.2(6) . . . . ? C55 Ce2 C11 C6 148.1(7) . . . . ? C57 Ce2 C11 C6 140.2(6) . . . . ? C2 Ce2 C11 C6 56.3(6) . . . . ? C5 Ce2 C11 C6 106.8(6) . . . . ? C42 Ce2 C11 C6 31.3(6) . . . . ? C32 Ce2 C11 C6 165.8(6) . . . . ? C3 Ce2 C11 C6 -174.8(7) . . . . ? C64 Ce2 C11 C75 -41.3(6) . . . . ? C14 Ce2 C11 C75 -33.3(6) . . . . ? C12 Ce2 C11 C75 -2.5(6) . . . . ? C55 Ce2 C11 C75 35.4(6) . . . . ? C57 Ce2 C11 C75 27.5(6) . . . . ? C2 Ce2 C11 C75 -56.3(6) . . . . ? C5 Ce2 C11 C75 -5.9(7) . . . . ? C42 Ce2 C11 C75 -81.4(6) . . . . ? C32 Ce2 C11 C75 53.1(6) . . . . ? C3 Ce2 C11 C75 72.5(6) . . . . ? C71 C5 C12 C57 -7.0(14) . . . . ? C31 C5 C12 C57 142.8(8) . . . . ? Ce2 C5 C12 C57 70.3(7) . . . . ? C71 C5 C12 C14 -146.5(9) . . . . ? C31 C5 C12 C14 3.3(9) . . . . ? Ce2 C5 C12 C14 -69.2(6) . . . . ? C71 C5 C12 Ce2 -77.3(9) . . . . ? C31 C5 C12 Ce2 72.5(6) . . . . ? C64 Ce2 C12 C57 101.3(6) . . . . ? C14 Ce2 C12 C57 132.8(8) . . . . ? C75 Ce2 C12 C57 65.5(6) . . . . ? C55 Ce2 C12 C57 30.7(6) . . . . ? C2 Ce2 C12 C57 168.9(7) . . . . ? C5 Ce2 C12 C57 -117.9(8) . . . . ? C42 Ce2 C12 C57 115.4(6) . . . . ? C11 Ce2 C12 C57 66.9(6) . . . . ? C32 Ce2 C12 C57 -31.8(5) . . . . ? C3 Ce2 C12 C57 10.8(6) . . . . ? C64 Ce2 C12 C14 -31.4(5) . . . . ? C75 Ce2 C12 C14 -67.2(5) . . . . ? C55 Ce2 C12 C14 -102.1(6) . . . . ? C57 Ce2 C12 C14 -132.8(8) . . . . ? C2 Ce2 C12 C14 36.1(5) . . . . ? C5 Ce2 C12 C14 109.3(7) . . . . ? C42 Ce2 C12 C14 -17.4(5) . . . . ? C11 Ce2 C12 C14 -65.9(5) . . . . ? C32 Ce2 C12 C14 -164.5(6) . . . . ? C3 Ce2 C12 C14 -121.9(5) . . . . ? C64 Ce2 C12 C5 -140.8(6) . . . . ? C14 Ce2 C12 C5 -109.3(7) . . . . ? C75 Ce2 C12 C5 -176.5(6) . . . . ? C55 Ce2 C12 C5 148.6(7) . . . . ? C57 Ce2 C12 C5 117.9(8) . . . . ? C2 Ce2 C12 C5 -73.2(5) . . . . ? C42 Ce2 C12 C5 -126.7(5) . . . . ? C11 Ce2 C12 C5 -175.2(5) . . . . ? C32 Ce2 C12 C5 86.1(6) . . . . ? C3 Ce2 C12 C5 128.7(6) . . . . ? C74 Ce1 C13 C52 -158.6(6) . . . . ? C43 Ce1 C13 C52 -128.8(6) . . . . ? C34 Ce1 C13 C52 -167.9(8) . . . . ? C36 Ce1 C13 C52 -123.6(9) . . . . ? C22 Ce1 C13 C52 -99.0(6) . . . . ? C16 Ce1 C13 C52 -89.5(7) . . . . ? C1 Ce1 C13 C52 176.7(6) . . . . ? C23 Ce1 C13 C52 152.3(8) . . . . ? C33 Ce1 C13 C52 -133.1(6) . . . . ? C41 Ce1 C13 C52 -54.7(6) . . . . ? C63 Ce1 C13 C52 -73.8(6) . . . . ? C74 Ce1 C13 C61 79.4(6) . . . . ? C43 Ce1 C13 C61 109.2(6) . . . . ? C34 Ce1 C13 C61 70.1(6) . . . . ? C36 Ce1 C13 C61 114.4(8) . . . . ? C22 Ce1 C13 C61 139.0(6) . . . . ? C16 Ce1 C13 C61 148.5(7) . . . . ? C1 Ce1 C13 C61 54.8(6) . . . . ? C23 Ce1 C13 C61 30.3(5) . . . . ? C33 Ce1 C13 C61 104.9(6) . . . . ? C41 Ce1 C13 C61 -176.7(6) . . . . ? C63 Ce1 C13 C61 164.2(5) . . . . ? C74 Ce1 C13 C36 -35.0(6) . . . . ? C43 Ce1 C13 C36 -5.2(6) . . . . ? C34 Ce1 C13 C36 -44.2(6) . . . . ? C22 Ce1 C13 C36 24.7(6) . . . . ? C16 Ce1 C13 C36 34.1(6) . . . . ? C1 Ce1 C13 C36 -59.6(6) . . . . ? C23 Ce1 C13 C36 -84.0(6) . . . . ? C33 Ce1 C13 C36 -9.5(8) . . . . ? C41 Ce1 C13 C36 68.9(6) . . . . ? C63 Ce1 C13 C36 49.8(6) . . . . ? C31 C2 C14 C12 -0.8(10) . . . . ? C9 C2 C14 C12 141.5(8) . . . . ? Ce2 C2 C14 C12 70.9(6) . . . . ? C31 C2 C14 C64 -139.5(8) . . . . ? C9 C2 C14 C64 2.9(13) . . . . ? Ce2 C2 C14 C64 -67.7(7) . . . . ? C31 C2 C14 Ce2 -71.8(6) . . . . ? C9 C2 C14 Ce2 70.6(8) . . . . ? C57 C12 C14 C2 -136.9(9) . . . . ? C5 C12 C14 C2 -1.6(10) . . . . ? Ce2 C12 C14 C2 -78.9(6) . . . . ? C57 C12 C14 C64 1.7(13) . . . . ? C5 C12 C14 C64 137.0(8) . . . . ? Ce2 C12 C14 C64 59.7(7) . . . . ? C57 C12 C14 Ce2 -58.0(8) . . . . ? C5 C12 C14 Ce2 77.3(6) . . . . ? C64 Ce2 C14 C2 -120.9(9) . . . . ? C75 Ce2 C14 C2 -150.8(7) . . . . ? C12 Ce2 C14 C2 112.3(8) . . . . ? C55 Ce2 C14 C2 174.2(7) . . . . ? C57 Ce2 C14 C2 139.5(7) . . . . ? C5 Ce2 C14 C2 73.2(6) . . . . ? C42 Ce2 C14 C2 -88.8(6) . . . . ? C11 Ce2 C14 C2 -131.9(6) . . . . ? C32 Ce2 C14 C2 124.8(6) . . . . ? C3 Ce2 C14 C2 171.4(6) . . . . ? C64 Ce2 C14 C12 126.8(8) . . . . ? C75 Ce2 C14 C12 96.9(6) . . . . ? C55 Ce2 C14 C12 61.9(5) . . . . ? C57 Ce2 C14 C12 27.2(5) . . . . ? C2 Ce2 C14 C12 -112.3(8) . . . . ? C5 Ce2 C14 C12 -39.1(5) . . . . ? C42 Ce2 C14 C12 158.9(6) . . . . ? C11 Ce2 C14 C12 115.8(5) . . . . ? C32 Ce2 C14 C12 12.5(5) . . . . ? C3 Ce2 C14 C12 59.1(5) . . . . ? C75 Ce2 C14 C64 -30.0(6) . . . . ? C12 Ce2 C14 C64 -126.8(8) . . . . ? C55 Ce2 C14 C64 -65.0(6) . . . . ? C57 Ce2 C14 C64 -99.6(6) . . . . ? C2 Ce2 C14 C64 120.9(9) . . . . ? C5 Ce2 C14 C64 -165.9(7) . . . . ? C42 Ce2 C14 C64 32.1(5) . . . . ? C11 Ce2 C14 C64 -11.1(6) . . . . ? C32 Ce2 C14 C64 -114.3(5) . . . . ? C3 Ce2 C14 C64 -67.7(6) . . . . ? C54 C8 C15 C68 0.0(11) . . . . ? C33 C8 C15 C68 150.4(8) . . . . ? Ce3 C8 C15 C68 67.6(9) . . . . ? C54 C8 C15 C63 -152.0(8) . . . . ? C33 C8 C15 C63 -1.6(12) . . . . ? Ce3 C8 C15 C63 -84.3(9) . . . . ? C54 C8 C15 Ce3 -67.7(9) . . . . ? C33 C8 C15 Ce3 82.7(10) . . . . ? C74 Ce1 C16 C41 -172.5(7) . . . . ? C43 Ce1 C16 C41 -137.6(7) . . . . ? C34 Ce1 C16 C41 150.5(7) . . . . ? C36 Ce1 C16 C41 121.7(8) . . . . ? C22 Ce1 C16 C41 -108.9(8) . . . . ? C1 Ce1 C16 C41 -169.8(6) . . . . ? C23 Ce1 C16 C41 130.9(6) . . . . ? C33 Ce1 C16 C41 -122.2(6) . . . . ? C13 Ce1 C16 C41 88.4(6) . . . . ? C63 Ce1 C16 C41 -71.5(6) . . . . ? C74 Ce1 C16 C36 65.8(5) . . . . ? C43 Ce1 C16 C36 100.7(6) . . . . ? C34 Ce1 C16 C36 28.8(5) . . . . ? C22 Ce1 C16 C36 129.4(8) . . . . ? C1 Ce1 C16 C36 68.5(5) . . . . ? C23 Ce1 C16 C36 9.2(5) . . . . ? C33 Ce1 C16 C36 116.1(5) . . . . ? C13 Ce1 C16 C36 -33.3(5) . . . . ? C41 Ce1 C16 C36 -121.7(8) . . . . ? C63 Ce1 C16 C36 166.8(7) . . . . ? C74 Ce1 C16 C22 -63.6(6) . . . . ? C43 Ce1 C16 C22 -28.6(5) . . . . ? C34 Ce1 C16 C22 -100.6(6) . . . . ? C36 Ce1 C16 C22 -129.4(8) . . . . ? C1 Ce1 C16 C22 -60.9(6) . . . . ? C23 Ce1 C16 C22 -120.1(6) . . . . ? C33 Ce1 C16 C22 -13.2(6) . . . . ? C13 Ce1 C16 C22 -162.7(7) . . . . ? C41 Ce1 C16 C22 108.9(8) . . . . ? C63 Ce1 C16 C22 37.5(5) . . . . ? C58 C4 C17 C19 -26.5(9) . . . . ? C54 C4 C17 C19 132.4(7) . . . . ? C58 C4 C17 C7 -141.6(7) . . . . ? C54 C4 C17 C7 17.4(7) . . . . ? C58 C4 C17 Si2 92.7(7) . . . . ? C54 C4 C17 Si2 -108.4(5) . . . . ? C9 C7 C17 C19 19.9(11) . . . . ? C10 C7 C17 C19 -131.0(7) . . . . ? C9 C7 C17 C4 133.3(8) . . . . ? C10 C7 C17 C4 -17.5(7) . . . . ? C9 C7 C17 Si2 -119.3(8) . . . . ? C10 C7 C17 Si2 89.9(8) . . . . ? C95 Si2 C17 C19 41.4(7) . . . . ? C96 Si2 C17 C19 165.5(7) . . . . ? C111 Si2 C17 C19 -71.1(8) . . . . ? C95 Si2 C17 C4 -73.1(7) . . . . ? C96 Si2 C17 C4 51.0(7) . . . . ? C111 Si2 C17 C4 174.4(6) . . . . ? C95 Si2 C17 C7 179.0(7) . . . . ? C96 Si2 C17 C7 -56.8(8) . . . . ? C111 Si2 C17 C7 66.5(9) . . . . ? C4 C17 C19 C29 29.2(9) . . . . ? C7 C17 C19 C29 137.3(8) . . . . ? Si2 C17 C19 C29 -79.8(9) . . . . ? C4 C17 C19 C31 -133.4(7) . . . . ? C7 C17 C19 C31 -25.3(10) . . . . ? Si2 C17 C19 C31 117.6(6) . . . . ? C48 C3 C20 C32 143.2(8) . . . . ? C55 C3 C20 C32 -6.1(10) . . . . ? Ce2 C3 C20 C32 52.2(7) . . . . ? C48 C3 C20 C56 -6.5(12) . . . . ? C55 C3 C20 C56 -155.9(8) . . . . ? Ce2 C3 C20 C56 -97.5(7) . . . . ? C48 C3 C20 Ce4 70.6(9) . . . . ? C55 C3 C20 Ce4 -78.8(8) . . . . ? Ce2 C3 C20 Ce4 -20.4(6) . . . . ? C41 C16 C22 C63 -0.7(11) . . . . ? C36 C16 C22 C63 -140.2(9) . . . . ? Ce1 C16 C22 C63 -83.0(7) . . . . ? C41 C16 C22 C43 138.0(9) . . . . ? C36 C16 C22 C43 -1.6(13) . . . . ? Ce1 C16 C22 C43 55.6(8) . . . . ? C41 C16 C22 Ce1 82.3(7) . . . . ? C36 C16 C22 Ce1 -57.2(8) . . . . ? C74 Ce1 C22 C63 -150.8(6) . . . . ? C43 Ce1 C22 C63 -121.6(8) . . . . ? C34 Ce1 C22 C63 173.1(6) . . . . ? C36 Ce1 C22 C63 136.9(6) . . . . ? C16 Ce1 C22 C63 108.0(8) . . . . ? C1 Ce1 C22 C63 -130.8(5) . . . . ? C23 Ce1 C22 C63 170.0(5) . . . . ? C33 Ce1 C22 C63 -88.3(6) . . . . ? C13 Ce1 C22 C63 122.1(5) . . . . ? C41 Ce1 C22 C63 70.9(5) . . . . ? C74 Ce1 C22 C43 -29.2(5) . . . . ? C34 Ce1 C22 C43 -65.3(6) . . . . ? C36 Ce1 C22 C43 -101.4(6) . . . . ? C16 Ce1 C22 C43 -130.4(9) . . . . ? C1 Ce1 C22 C43 -9.2(6) . . . . ? C23 Ce1 C22 C43 -68.3(6) . . . . ? C33 Ce1 C22 C43 33.3(5) . . . . ? C13 Ce1 C22 C43 -116.2(6) . . . . ? C41 Ce1 C22 C43 -167.4(7) . . . . ? C63 Ce1 C22 C43 121.6(8) . . . . ? C74 Ce1 C22 C16 101.2(6) . . . . ? C43 Ce1 C22 C16 130.4(9) . . . . ? C34 Ce1 C22 C16 65.1(6) . . . . ? C36 Ce1 C22 C16 29.0(5) . . . . ? C1 Ce1 C22 C16 121.2(6) . . . . ? C23 Ce1 C22 C16 62.1(6) . . . . ? C33 Ce1 C22 C16 163.7(7) . . . . ? C13 Ce1 C22 C16 14.2(6) . . . . ? C41 Ce1 C22 C16 -37.1(5) . . . . ? C63 Ce1 C22 C16 -108.0(8) . . . . ? C74 Ce1 C23 C61 -147.3(7) . . . . ? C43 Ce1 C23 C61 -137.2(6) . . . . ? C34 Ce1 C23 C61 -112.5(8) . . . . ? C36 Ce1 C23 C61 -71.5(6) . . . . ? C22 Ce1 C23 C61 -106.9(6) . . . . ? C16 Ce1 C23 C61 -77.6(6) . . . . ? C1 Ce1 C23 C61 175.6(7) . . . . ? C33 Ce1 C23 C61 -163.4(5) . . . . ? C13 Ce1 C23 C61 -31.2(5) . . . . ? C41 Ce1 C23 C61 -55.1(6) . . . . ? C63 Ce1 C23 C61 -100.5(6) . . . . ? C74 Ce1 C23 C34 -34.8(5) . . . . ? C43 Ce1 C23 C34 -24.7(5) . . . . ? C36 Ce1 C23 C34 41.0(5) . . . . ? C22 Ce1 C23 C34 5.6(6) . . . . ? C16 Ce1 C23 C34 34.9(5) . . . . ? C1 Ce1 C23 C34 -71.8(5) . . . . ? C33 Ce1 C23 C34 -50.9(6) . . . . ? C13 Ce1 C23 C34 81.3(6) . . . . ? C41 Ce1 C23 C34 57.4(6) . . . . ? C63 Ce1 C23 C34 12.1(6) . . . . ? C74 Ce1 C23 C46 92.6(6) . . . . ? C43 Ce1 C23 C46 102.7(6) . . . . ? C34 Ce1 C23 C46 127.4(8) . . . . ? C36 Ce1 C23 C46 168.4(7) . . . . ? C22 Ce1 C23 C46 133.0(5) . . . . ? C16 Ce1 C23 C46 162.3(6) . . . . ? C1 Ce1 C23 C46 55.6(5) . . . . ? C33 Ce1 C23 C46 76.5(6) . . . . ? C13 Ce1 C23 C46 -151.3(7) . . . . ? C41 Ce1 C23 C46 -175.2(5) . . . . ? C63 Ce1 C23 C46 139.5(5) . . . . ? C70 C24 C28 C58 -130.3(8) . . . . ? C30 C24 C28 C58 18.6(11) . . . . ? C70 C24 C28 C29 -14.8(9) . . . . ? C30 C24 C28 C29 134.1(8) . . . . ? C70 C24 C28 Si1 91.9(8) . . . . ? C30 C24 C28 Si1 -119.3(8) . . . . ? C95 Si1 C28 C58 52.7(7) . . . . ? C88 Si1 C28 C58 174.7(6) . . . . ? C87 Si1 C28 C58 -60.7(7) . . . . ? C95 Si1 C28 C29 -64.1(6) . . . . ? C88 Si1 C28 C29 57.9(6) . . . . ? C87 Si1 C28 C29 -177.5(5) . . . . ? C95 Si1 C28 C24 -170.5(7) . . . . ? C88 Si1 C28 C24 -48.5(7) . . . . ? C87 Si1 C28 C24 76.1(8) . . . . ? C31 C19 C29 C26 3.4(11) . . . . ? C17 C19 C29 C26 -159.4(7) . . . . ? C31 C19 C29 C28 158.9(7) . . . . ? C17 C19 C29 C28 -3.9(11) . . . . ? C71 C26 C29 C19 0.6(12) . . . . ? C70 C26 C29 C19 149.1(8) . . . . ? Ce4 C26 C29 C19 69.7(9) . . . . ? C71 C26 C29 C28 -157.3(7) . . . . ? C70 C26 C29 C28 -8.9(9) . . . . ? Ce4 C26 C29 C28 -88.3(7) . . . . ? C58 C28 C29 C19 -26.2(9) . . . . ? C24 C28 C29 C19 -143.3(7) . . . . ? Si1 C28 C29 C19 94.3(7) . . . . ? C58 C28 C29 C26 131.5(7) . . . . ? C24 C28 C29 C26 14.3(9) . . . . ? Si1 C28 C29 C26 -108.1(6) . . . . ? C62 C1 C30 C24 -16.7(12) . . . . ? C74 C1 C30 C24 -157.3(9) . . . . ? Ce1 C1 C30 C24 -99.4(7) . . . . ? C62 C1 C30 C46 135.8(8) . . . . ? C74 C1 C30 C46 -4.8(13) . . . . ? Ce1 C1 C30 C46 53.1(7) . . . . ? C70 C24 C30 C1 146.4(8) . . . . ? C28 C24 C30 C1 0.9(12) . . . . ? C70 C24 C30 C46 -5.6(13) . . . . ? C28 C24 C30 C46 -151.1(8) . . . . ? C29 C19 C31 C2 -151.1(8) . . . . ? C17 C19 C31 C2 12.5(11) . . . . ? C29 C19 C31 C5 0.2(11) . . . . ? C17 C19 C31 C5 163.8(7) . . . . ? C29 C19 C31 Ce2 -75.1(8) . . . . ? C17 C19 C31 Ce2 88.5(7) . . . . ? C14 C2 C31 C19 157.3(8) . . . . ? C9 C2 C31 C19 10.0(10) . . . . ? Ce2 C2 C31 C19 97.8(7) . . . . ? C14 C2 C31 C5 3.0(9) . . . . ? C9 C2 C31 C5 -144.3(7) . . . . ? Ce2 C2 C31 C5 -56.5(6) . . . . ? C14 C2 C31 Ce2 59.4(5) . . . . ? C9 C2 C31 Ce2 -87.8(6) . . . . ? C71 C5 C31 C19 -7.9(12) . . . . ? C12 C5 C31 C19 -159.7(7) . . . . ? Ce2 C5 C31 C19 -99.4(7) . . . . ? C71 C5 C31 C2 147.9(8) . . . . ? C12 C5 C31 C2 -3.9(9) . . . . ? Ce2 C5 C31 C2 56.4(6) . . . . ? C71 C5 C31 Ce2 91.5(7) . . . . ? C12 C5 C31 Ce2 -60.2(6) . . . . ? C64 Ce2 C31 C19 -145.7(6) . . . . ? C14 Ce2 C31 C19 -159.0(7) . . . . ? C75 Ce2 C31 C19 -164.8(6) . . . . ? C12 Ce2 C31 C19 156.1(7) . . . . ? C55 Ce2 C31 C19 160.2(6) . . . . ? C57 Ce2 C31 C19 142.1(6) . . . . ? C2 Ce2 C31 C19 -121.9(8) . . . . ? C5 Ce2 C31 C19 116.6(8) . . . . ? C42 Ce2 C31 C19 -115.6(6) . . . . ? C11 Ce2 C31 C19 -141.4(6) . . . . ? C32 Ce2 C31 C19 112.6(6) . . . . ? C3 Ce2 C31 C19 135.6(6) . . . . ? C64 Ce2 C31 C2 -23.8(5) . . . . ? C14 Ce2 C31 C2 -37.1(5) . . . . ? C75 Ce2 C31 C2 -42.9(6) . . . . ? C12 Ce2 C31 C2 -82.0(6) . . . . ? C55 Ce2 C31 C2 -78.0(6) . . . . ? C57 Ce2 C31 C2 -96.0(5) . . . . ? C5 Ce2 C31 C2 -121.6(8) . . . . ? C42 Ce2 C31 C2 6.2(5) . . . . ? C11 Ce2 C31 C2 -19.6(7) . . . . ? C32 Ce2 C31 C2 -125.6(5) . . . . ? C3 Ce2 C31 C2 -102.5(6) . . . . ? C64 Ce2 C31 C5 97.8(6) . . . . ? C14 Ce2 C31 C5 84.4(6) . . . . ? C75 Ce2 C31 C5 78.7(6) . . . . ? C12 Ce2 C31 C5 39.5(5) . . . . ? C55 Ce2 C31 C5 43.6(6) . . . . ? C57 Ce2 C31 C5 25.5(5) . . . . ? C2 Ce2 C31 C5 121.6(8) . . . . ? C42 Ce2 C31 C5 127.8(6) . . . . ? C11 Ce2 C31 C5 102.0(6) . . . . ? C32 Ce2 C31 C5 -4.0(5) . . . . ? C3 Ce2 C31 C5 19.1(7) . . . . ? C73 C18 C32 C57 -157.1(9) . . . . ? C71 C18 C32 C57 -7.5(13) . . . . ? Ce4 C18 C32 C57 -96.4(10) . . . . ? C73 C18 C32 C20 -11.8(13) . . . . ? C71 C18 C32 C20 137.8(9) . . . . ? Ce4 C18 C32 C20 48.9(9) . . . . ? C73 C18 C32 Ce4 -60.7(8) . . . . ? C71 C18 C32 Ce4 88.9(8) . . . . ? C73 C18 C32 Ce2 -98.9(8) . . . . ? C71 C18 C32 Ce2 50.7(8) . . . . ? Ce4 C18 C32 Ce2 -38.2(5) . . . . ? C3 C20 C32 C18 -144.2(8) . . . . ? C56 C20 C32 C18 7.1(13) . . . . ? Ce4 C20 C32 C18 -41.2(8) . . . . ? C3 C20 C32 C57 6.7(10) . . . . ? C56 C20 C32 C57 158.1(8) . . . . ? Ce4 C20 C32 C57 109.7(7) . . . . ? C3 C20 C32 Ce4 -103.0(8) . . . . ? C56 C20 C32 Ce4 48.4(9) . . . . ? C3 C20 C32 Ce2 -52.7(7) . . . . ? C56 C20 C32 Ce2 98.6(8) . . . . ? Ce4 C20 C32 Ce2 50.3(4) . . . . ? C64 Ce2 C32 C18 -133.8(6) . . . . ? C14 Ce2 C32 C18 -102.0(6) . . . . ? C75 Ce2 C32 C18 -162.5(6) . . . . ? C12 Ce2 C32 C18 -93.4(6) . . . . ? C55 Ce2 C32 C18 -168.4(7) . . . . ? C57 Ce2 C32 C18 -128.0(8) . . . . ? C2 Ce2 C32 C18 -76.5(6) . . . . ? C5 Ce2 C32 C18 -54.8(5) . . . . ? C42 Ce2 C32 C18 -139.9(5) . . . . ? C11 Ce2 C32 C18 173.2(6) . . . . ? C3 Ce2 C32 C18 150.8(7) . . . . ? C64 Ce2 C32 C57 -5.8(6) . . . . ? C14 Ce2 C32 C57 26.1(5) . . . . ? C75 Ce2 C32 C57 -34.4(5) . . . . ? C12 Ce2 C32 C57 34.7(5) . . . . ? C55 Ce2 C32 C57 -40.3(5) . . . . ? C2 Ce2 C32 C57 51.5(6) . . . . ? C5 Ce2 C32 C57 73.3(5) . . . . ? C42 Ce2 C32 C57 -11.9(7) . . . . ? C11 Ce2 C32 C57 -58.8(6) . . . . ? C3 Ce2 C32 C57 -81.2(6) . . . . ? C64 Ce2 C32 C20 104.7(6) . . . . ? C14 Ce2 C32 C20 136.5(6) . . . . ? C75 Ce2 C32 C20 76.0(6) . . . . ? C12 Ce2 C32 C20 145.1(7) . . . . ? C55 Ce2 C32 C20 70.1(6) . . . . ? C57 Ce2 C32 C20 110.5(8) . . . . ? C2 Ce2 C32 C20 161.9(6) . . . . ? C5 Ce2 C32 C20 -176.3(7) . . . . ? C42 Ce2 C32 C20 98.6(6) . . . . ? C11 Ce2 C32 C20 51.7(6) . . . . ? C3 Ce2 C32 C20 29.3(5) . . . . ? C64 Ce2 C32 Ce4 -177.3(5) . . . . ? C14 Ce2 C32 Ce4 -145.4(5) . . . . ? C75 Ce2 C32 Ce4 154.1(5) . . . . ? C12 Ce2 C32 Ce4 -136.8(6) . . . . ? C55 Ce2 C32 Ce4 148.2(6) . . . . ? C57 Ce2 C32 Ce4 -171.5(7) . . . . ? C2 Ce2 C32 Ce4 -120.0(5) . . . . ? C5 Ce2 C32 Ce4 -98.2(5) . . . . ? C42 Ce2 C32 Ce4 176.6(5) . . . . ? C11 Ce2 C32 Ce4 129.7(5) . . . . ? C3 Ce2 C32 Ce4 107.3(6) . . . . ? C54 C8 C33 C62 11.9(11) . . . . ? C15 C8 C33 C62 -138.5(8) . . . . ? Ce3 C8 C33 C62 -84.2(8) . . . . ? C54 C8 C33 C43 156.9(8) . . . . ? C15 C8 C33 C43 6.5(13) . . . . ? Ce3 C8 C33 C43 60.8(10) . . . . ? C54 C8 C33 Ce1 95.8(6) . . . . ? C15 C8 C33 Ce1 -54.6(8) . . . . ? Ce3 C8 C33 Ce1 -0.3(6) . . . . ? C74 Ce1 C33 C62 -73.9(6) . . . . ? C43 Ce1 C33 C62 -115.2(8) . . . . ? C34 Ce1 C33 C62 -80.1(6) . . . . ? C36 Ce1 C33 C62 -112.1(6) . . . . ? C22 Ce1 C33 C62 -150.4(7) . . . . ? C16 Ce1 C33 C62 -141.5(6) . . . . ? C1 Ce1 C33 C62 -32.5(5) . . . . ? C23 Ce1 C33 C62 -56.7(6) . . . . ? C13 Ce1 C33 C62 -107.0(6) . . . . ? C41 Ce1 C33 C62 -166.7(5) . . . . ? C63 Ce1 C33 C62 174.7(7) . . . . ? C74 Ce1 C33 C8 166.4(7) . . . . ? C43 Ce1 C33 C8 125.1(8) . . . . ? C34 Ce1 C33 C8 160.2(6) . . . . ? C36 Ce1 C33 C8 128.2(6) . . . . ? C22 Ce1 C33 C8 89.9(6) . . . . ? C16 Ce1 C33 C8 98.8(6) . . . . ? C1 Ce1 C33 C8 -152.2(7) . . . . ? C23 Ce1 C33 C8 -176.4(5) . . . . ? C13 Ce1 C33 C8 133.3(5) . . . . ? C41 Ce1 C33 C8 73.6(6) . . . . ? C63 Ce1 C33 C8 55.0(5) . . . . ? C74 Ce1 C33 C43 41.3(5) . . . . ? C34 Ce1 C33 C43 35.1(6) . . . . ? C36 Ce1 C33 C43 3.2(6) . . . . ? C22 Ce1 C33 C43 -35.2(6) . . . . ? C16 Ce1 C33 C43 -26.3(6) . . . . ? C1 Ce1 C33 C43 82.8(6) . . . . ? C23 Ce1 C33 C43 58.6(6) . . . . ? C13 Ce1 C33 C43 8.2(7) . . . . ? C41 Ce1 C33 C43 -51.4(6) . . . . ? C63 Ce1 C33 C43 -70.0(6) . . . . ? C61 C23 C34 C74 140.8(8) . . . . ? C46 C23 C34 C74 -8.1(14) . . . . ? Ce1 C23 C34 C74 64.8(8) . . . . ? C61 C23 C34 C36 6.9(10) . . . . ? C46 C23 C34 C36 -142.1(9) . . . . ? Ce1 C23 C34 C36 -69.1(6) . . . . ? C61 C23 C34 Ce1 76.1(6) . . . . ? C46 C23 C34 Ce1 -72.9(9) . . . . ? C74 Ce1 C34 C23 123.3(8) . . . . ? C43 Ce1 C34 C23 151.6(6) . . . . ? C36 Ce1 C34 C23 -112.7(8) . . . . ? C22 Ce1 C34 C23 -174.2(6) . . . . ? C16 Ce1 C34 C23 -139.4(6) . . . . ? C1 Ce1 C34 C23 89.2(5) . . . . ? C33 Ce1 C34 C23 131.8(5) . . . . ? C13 Ce1 C34 C23 -73.0(6) . . . . ? C41 Ce1 C34 C23 -125.4(5) . . . . ? C63 Ce1 C34 C23 -170.8(5) . . . . ? C43 Ce1 C34 C74 28.3(5) . . . . ? C36 Ce1 C34 C74 124.1(8) . . . . ? C22 Ce1 C34 C74 62.5(5) . . . . ? C16 Ce1 C34 C74 97.3(6) . . . . ? C1 Ce1 C34 C74 -34.1(5) . . . . ? C23 Ce1 C34 C74 -123.3(8) . . . . ? C33 Ce1 C34 C74 8.5(5) . . . . ? C13 Ce1 C34 C74 163.7(7) . . . . ? C41 Ce1 C34 C74 111.3(5) . . . . ? C63 Ce1 C34 C74 65.9(5) . . . . ? C74 Ce1 C34 C36 -124.1(8) . . . . ? C43 Ce1 C34 C36 -95.7(6) . . . . ? C22 Ce1 C34 C36 -61.6(5) . . . . ? C16 Ce1 C34 C36 -26.7(5) . . . . ? C1 Ce1 C34 C36 -158.2(7) . . . . ? C23 Ce1 C34 C36 112.7(8) . . . . ? C33 Ce1 C34 C36 -115.5(5) . . . . ? C13 Ce1 C34 C36 39.6(5) . . . . ? C41 Ce1 C34 C36 -12.7(5) . . . . ? C63 Ce1 C34 C36 -58.1(5) . . . . ? C105 C84 C87 C97 -3.1(14) . . . . ? C98 C84 C87 C97 178.6(8) . . . . ? C105 C84 C87 Si1 173.7(7) . . . . ? C98 C84 C87 Si1 -4.7(14) . . . . ? C95 Si1 C87 C84 -115.1(9) . . . . ? C88 Si1 C87 C84 121.6(9) . . . . ? C28 Si1 C87 C84 -1.1(11) . . . . ? C95 Si1 C87 C97 61.7(8) . . . . ? C88 Si1 C87 C97 -61.6(7) . . . . ? C28 Si1 C87 C97 175.7(6) . . . . ? C92 C81 C88 C85 -3.3(11) . . . . ? C86 C81 C88 C85 179.8(7) . . . . ? C92 C81 C88 Si1 178.9(6) . . . . ? C86 C81 C88 Si1 2.0(10) . . . . ? C106 C85 C88 C81 4.9(11) . . . . ? C93 C85 C88 C81 -176.3(7) . . . . ? C106 C85 C88 Si1 -177.5(6) . . . . ? C93 C85 C88 Si1 1.3(11) . . . . ? C95 Si1 C88 C81 -166.1(6) . . . . ? C87 Si1 C88 C81 -52.5(7) . . . . ? C28 Si1 C88 C81 81.4(6) . . . . ? C95 Si1 C88 C85 16.3(8) . . . . ? C87 Si1 C88 C85 130.0(7) . . . . ? C28 Si1 C88 C85 -96.1(7) . . . . ? C41 C16 C36 C13 -0.2(12) . . . . ? C22 C16 C36 C13 134.6(9) . . . . ? Ce1 C16 C36 C13 76.7(7) . . . . ? C41 C16 C36 C34 -134.1(9) . . . . ? C22 C16 C36 C34 0.7(14) . . . . ? Ce1 C16 C36 C34 -57.2(8) . . . . ? C41 C16 C36 Ce1 -76.9(8) . . . . ? C22 C16 C36 Ce1 57.9(8) . . . . ? C52 C13 C36 C16 6.5(12) . . . . ? C61 C13 C36 C16 -143.0(8) . . . . ? Ce1 C13 C36 C16 -71.1(7) . . . . ? C52 C13 C36 C34 148.2(8) . . . . ? C61 C13 C36 C34 -1.3(9) . . . . ? Ce1 C13 C36 C34 70.7(5) . . . . ? C52 C13 C36 Ce1 77.6(8) . . . . ? C61 C13 C36 Ce1 -71.9(6) . . . . ? C23 C34 C36 C16 135.9(9) . . . . ? C74 C34 C36 C16 -0.5(13) . . . . ? Ce1 C34 C36 C16 58.6(8) . . . . ? C23 C34 C36 C13 -3.4(10) . . . . ? C74 C34 C36 C13 -139.8(8) . . . . ? Ce1 C34 C36 C13 -80.6(6) . . . . ? C23 C34 C36 Ce1 77.2(6) . . . . ? C74 C34 C36 Ce1 -59.2(7) . . . . ? C74 Ce1 C36 C16 -99.9(6) . . . . ? C43 Ce1 C36 C16 -64.4(5) . . . . ? C34 Ce1 C36 C16 -132.8(8) . . . . ? C22 Ce1 C36 C16 -29.9(5) . . . . ? C1 Ce1 C36 C16 -114.7(5) . . . . ? C23 Ce1 C36 C16 -168.6(6) . . . . ? C33 Ce1 C36 C16 -66.1(5) . . . . ? C13 Ce1 C36 C16 121.0(8) . . . . ? C41 Ce1 C36 C16 31.3(5) . . . . ? C63 Ce1 C36 C16 -10.1(5) . . . . ? C74 Ce1 C36 C13 139.1(7) . . . . ? C43 Ce1 C36 C13 174.6(7) . . . . ? C34 Ce1 C36 C13 106.2(8) . . . . ? C22 Ce1 C36 C13 -150.9(7) . . . . ? C16 Ce1 C36 C13 -121.0(8) . . . . ? C1 Ce1 C36 C13 124.3(6) . . . . ? C23 Ce1 C36 C13 70.4(6) . . . . ? C33 Ce1 C36 C13 172.9(6) . . . . ? C41 Ce1 C36 C13 -89.7(6) . . . . ? C63 Ce1 C36 C13 -131.2(6) . . . . ? C74 Ce1 C36 C34 32.9(5) . . . . ? C43 Ce1 C36 C34 68.4(6) . . . . ? C22 Ce1 C36 C34 102.9(6) . . . . ? C16 Ce1 C36 C34 132.8(8) . . . . ? C1 Ce1 C36 C34 18.0(5) . . . . ? C23 Ce1 C36 C34 -35.8(5) . . . . ? C33 Ce1 C36 C34 66.6(6) . . . . ? C13 Ce1 C36 C34 -106.2(8) . . . . ? C41 Ce1 C36 C34 164.1(7) . . . . ? C63 Ce1 C36 C34 122.6(5) . . . . ? C51 C21 C38 C40 -143.4(9) . . . . ? C60 C21 C38 C40 2.5(15) . . . . ? C51 C21 C38 C59 -0.7(10) . . . . ? C60 C21 C38 C59 145.2(8) . . . . ? C102 C83 C89 C100 1.7(17) . . . . ? C114 C83 C89 C100 -176.1(11) . . . . ? C45 C37 C39 C56 -145.0(8) . . . . ? C65 C37 C39 C56 1.6(13) . . . . ? C45 C37 C39 C25 -1.6(9) . . . . ? C65 C37 C39 C25 145.0(7) . . . . ? C48 C25 C39 C37 -142.5(8) . . . . ? C67 C25 C39 C37 3.4(8) . . . . ? C48 C25 C39 C56 2.6(12) . . . . ? C67 C25 C39 C56 148.6(7) . . . . ? C41 C35 C40 C38 -3.6(14) . . . . ? C63 C35 C40 C38 -148.7(9) . . . . ? Ce3 C35 C40 C38 -100.5(9) . . . . ? C41 C35 C40 C76 148.3(9) . . . . ? C63 C35 C40 C76 3.1(14) . . . . ? Ce3 C35 C40 C76 51.4(9) . . . . ? C41 C35 C40 Ce3 96.9(9) . . . . ? C63 C35 C40 Ce3 -48.2(10) . . . . ? C21 C38 C40 C35 144.7(10) . . . . ? C59 C38 C40 C35 5.8(13) . . . . ? C21 C38 C40 C76 -6.6(14) . . . . ? C59 C38 C40 C76 -145.6(9) . . . . ? C21 C38 C40 Ce3 62.4(12) . . . . ? C59 C38 C40 Ce3 -76.5(10) . . . . ? C36 C16 C41 C53 -7.8(14) . . . . ? C22 C16 C41 C53 -147.3(9) . . . . ? Ce1 C16 C41 C53 -75.7(9) . . . . ? C36 C16 C41 C35 143.1(8) . . . . ? C22 C16 C41 C35 3.6(11) . . . . ? Ce1 C16 C41 C35 75.3(7) . . . . ? C36 C16 C41 Ce1 67.8(7) . . . . ? C22 C16 C41 Ce1 -71.6(6) . . . . ? C40 C35 C41 C16 -155.9(9) . . . . ? C63 C35 C41 C16 -5.0(11) . . . . ? Ce3 C35 C41 C16 -78.2(10) . . . . ? C40 C35 C41 C53 -3.4(14) . . . . ? C63 C35 C41 C53 147.4(9) . . . . ? Ce3 C35 C41 C53 74.3(10) . . . . ? C40 C35 C41 Ce1 -96.5(9) . . . . ? C63 C35 C41 Ce1 54.3(7) . . . . ? Ce3 C35 C41 Ce1 -18.8(6) . . . . ? C74 Ce1 C41 C16 7.2(6) . . . . ? C43 Ce1 C41 C16 35.9(6) . . . . ? C34 Ce1 C41 C16 -25.6(6) . . . . ? C36 Ce1 C41 C16 -34.7(6) . . . . ? C22 Ce1 C41 C16 42.8(6) . . . . ? C1 Ce1 C41 C16 13.3(7) . . . . ? C23 Ce1 C41 C16 -51.2(6) . . . . ? C33 Ce1 C41 C16 60.0(6) . . . . ? C13 Ce1 C41 C16 -72.3(6) . . . . ? C63 Ce1 C41 C16 81.9(6) . . . . ? C74 Ce1 C41 C53 133.3(6) . . . . ? C43 Ce1 C41 C53 162.1(7) . . . . ? C34 Ce1 C41 C53 100.5(6) . . . . ? C36 Ce1 C41 C53 91.4(7) . . . . ? C22 Ce1 C41 C53 168.9(8) . . . . ? C16 Ce1 C41 C53 126.1(9) . . . . ? C1 Ce1 C41 C53 139.5(6) . . . . ? C23 Ce1 C41 C53 74.9(7) . . . . ? C33 Ce1 C41 C53 -173.8(6) . . . . ? C13 Ce1 C41 C53 53.8(6) . . . . ? C63 Ce1 C41 C53 -151.9(8) . . . . ? C74 Ce1 C41 C35 -107.6(6) . . . . ? C43 Ce1 C41 C35 -78.8(6) . . . . ? C34 Ce1 C41 C35 -140.4(6) . . . . ? C36 Ce1 C41 C35 -149.4(7) . . . . ? C22 Ce1 C41 C35 -72.0(6) . . . . ? C16 Ce1 C41 C35 -114.7(9) . . . . ? C1 Ce1 C41 C35 -101.4(6) . . . . ? C23 Ce1 C41 C35 -166.0(6) . . . . ? C33 Ce1 C41 C35 -54.7(6) . . . . ? C13 Ce1 C41 C35 172.9(7) . . . . ? C63 Ce1 C41 C35 -32.8(6) . . . . ? C11 C6 C42 C64 -4.7(11) . . . . ? C60 C6 C42 C64 -156.7(9) . . . . ? Ce2 C6 C42 C64 -59.6(6) . . . . ? C11 C6 C42 C44 142.4(9) . . . . ? C60 C6 C42 C44 -9.6(14) . . . . ? Ce2 C6 C42 C44 87.5(8) . . . . ? C11 C6 C42 Ce2 54.9(7) . . . . ? C60 C6 C42 Ce2 -97.1(9) . . . . ? C14 Ce2 C42 C64 -36.0(5) . . . . ? C75 Ce2 C42 C64 40.7(5) . . . . ? C12 Ce2 C42 C64 -24.4(5) . . . . ? C55 Ce2 C42 C64 33.7(5) . . . . ? C57 Ce2 C42 C64 5.7(5) . . . . ? C2 Ce2 C42 C64 -71.5(5) . . . . ? C5 Ce2 C42 C64 -51.0(5) . . . . ? C11 Ce2 C42 C64 80.6(6) . . . . ? C32 Ce2 C42 C64 11.8(6) . . . . ? C3 Ce2 C42 C64 57.9(5) . . . . ? C64 Ce2 C42 C6 -111.7(8) . . . . ? C14 Ce2 C42 C6 -147.7(7) . . . . ? C75 Ce2 C42 C6 -71.0(6) . . . . ? C12 Ce2 C42 C6 -136.0(6) . . . . ? C55 Ce2 C42 C6 -78.0(6) . . . . ? C57 Ce2 C42 C6 -105.9(6) . . . . ? C2 Ce2 C42 C6 176.8(7) . . . . ? C5 Ce2 C42 C6 -162.6(6) . . . . ? C11 Ce2 C42 C6 -31.0(5) . . . . ? C32 Ce2 C42 C6 -99.9(6) . . . . ? C3 Ce2 C42 C6 -53.8(6) . . . . ? C64 Ce2 C42 C44 128.2(8) . . . . ? C14 Ce2 C42 C44 92.2(6) . . . . ? C75 Ce2 C42 C44 168.8(7) . . . . ? C12 Ce2 C42 C44 103.8(6) . . . . ? C55 Ce2 C42 C44 161.8(6) . . . . ? C57 Ce2 C42 C44 133.9(6) . . . . ? C2 Ce2 C42 C44 56.7(5) . . . . ? C5 Ce2 C42 C44 77.2(6) . . . . ? C11 Ce2 C42 C44 -151.2(8) . . . . ? C32 Ce2 C42 C44 140.0(6) . . . . ? C3 Ce2 C42 C44 -173.9(6) . . . . ? C63 C22 C43 C74 135.9(10) . . . . ? C16 C22 C43 C74 2.3(14) . . . . ? Ce1 C22 C43 C74 59.2(8) . . . . ? C63 C22 C43 C33 -0.6(13) . . . . ? C16 C22 C43 C33 -134.2(9) . . . . ? Ce1 C22 C43 C33 -77.3(7) . . . . ? C63 C22 C43 Ce1 76.7(8) . . . . ? C16 C22 C43 Ce1 -56.9(8) . . . . ? C62 C33 C43 C74 0.7(10) . . . . ? C8 C33 C43 C74 -147.7(8) . . . . ? Ce1 C33 C43 C74 -70.3(6) . . . . ? C62 C33 C43 C22 143.0(8) . . . . ? C8 C33 C43 C22 -5.4(13) . . . . ? Ce1 C33 C43 C22 72.0(7) . . . . ? C62 C33 C43 Ce1 71.0(7) . . . . ? C8 C33 C43 Ce1 -77.4(8) . . . . ? C34 Ce1 C43 C74 -29.6(5) . . . . ? C36 Ce1 C43 C74 -67.0(5) . . . . ? C22 Ce1 C43 C74 -130.3(8) . . . . ? C16 Ce1 C43 C74 -101.1(6) . . . . ? C1 Ce1 C43 C74 38.2(5) . . . . ? C23 Ce1 C43 C74 -15.5(5) . . . . ? C33 Ce1 C43 C74 109.7(7) . . . . ? C13 Ce1 C43 C74 -64.1(5) . . . . ? C41 Ce1 C43 C74 -120.6(5) . . . . ? C63 Ce1 C43 C74 -161.5(6) . . . . ? C74 Ce1 C43 C22 130.3(8) . . . . ? C34 Ce1 C43 C22 100.8(6) . . . . ? C36 Ce1 C43 C22 63.3(6) . . . . ? C16 Ce1 C43 C22 29.2(5) . . . . ? C1 Ce1 C43 C22 168.5(7) . . . . ? C23 Ce1 C43 C22 114.9(6) . . . . ? C33 Ce1 C43 C22 -120.0(9) . . . . ? C13 Ce1 C43 C22 66.2(6) . . . . ? C41 Ce1 C43 C22 9.7(6) . . . . ? C63 Ce1 C43 C22 -31.2(5) . . . . ? C74 Ce1 C43 C33 -109.7(7) . . . . ? C34 Ce1 C43 C33 -139.2(7) . . . . ? C36 Ce1 C43 C33 -176.7(7) . . . . ? C22 Ce1 C43 C33 120.0(9) . . . . ? C16 Ce1 C43 C33 149.2(7) . . . . ? C1 Ce1 C43 C33 -71.5(5) . . . . ? C23 Ce1 C43 C33 -125.2(6) . . . . ? C13 Ce1 C43 C33 -173.8(5) . . . . ? C41 Ce1 C43 C33 129.7(6) . . . . ? C63 Ce1 C43 C33 88.8(6) . . . . ? C64 C42 C44 C49 154.9(9) . . . . ? C6 C42 C44 C49 13.7(13) . . . . ? Ce2 C42 C44 C49 97.5(8) . . . . ? C64 C42 C44 C9 4.5(14) . . . . ? C6 C42 C44 C9 -136.7(9) . . . . ? Ce2 C42 C44 C9 -52.9(8) . . . . ? C7 C9 C44 C49 3.4(12) . . . . ? C2 C9 C44 C49 -152.4(8) . . . . ? C7 C9 C44 C42 153.3(9) . . . . ? C2 C9 C44 C42 -2.4(12) . . . . ? C39 C37 C45 C52 145.2(8) . . . . ? C65 C37 C45 C52 0.5(12) . . . . ? C39 C37 C45 C67 -1.0(8) . . . . ? C65 C37 C45 C67 -145.8(8) . . . . ? C61 C23 C46 C77 13.6(13) . . . . ? C34 C23 C46 C77 159.2(9) . . . . ? Ce1 C23 C46 C77 99.3(7) . . . . ? C61 C23 C46 C30 -140.3(9) . . . . ? C34 C23 C46 C30 5.3(13) . . . . ? Ce1 C23 C46 C30 -54.5(8) . . . . ? C1 C30 C46 C23 1.1(12) . . . . ? C24 C30 C46 C23 153.8(9) . . . . ? C1 C30 C46 C77 -152.5(9) . . . . ? C24 C30 C46 C77 0.1(12) . . . . ? C6 C11 C47 C51 -11.6(12) . . . . ? C75 C11 C47 C51 -155.9(9) . . . . ? Ce2 C11 C47 C51 -96.8(7) . . . . ? C6 C11 C47 C48 139.9(9) . . . . ? C75 C11 C47 C48 -4.4(14) . . . . ? Ce2 C11 C47 C48 54.8(8) . . . . ? C67 C25 C48 C3 -150.5(8) . . . . ? C39 C25 C48 C3 -10.8(12) . . . . ? C67 C25 C48 C47 1.3(11) . . . . ? C39 C25 C48 C47 141.1(8) . . . . ? C20 C3 C48 C25 12.5(11) . . . . ? C55 C3 C48 C25 156.3(8) . . . . ? Ce2 C3 C48 C25 99.2(6) . . . . ? C20 C3 C48 C47 -139.7(8) . . . . ? C55 C3 C48 C47 4.1(12) . . . . ? Ce2 C3 C48 C47 -52.9(8) . . . . ? C51 C47 C48 C25 -0.5(11) . . . . ? C11 C47 C48 C25 -151.0(8) . . . . ? C51 C47 C48 C3 151.0(8) . . . . ? C11 C47 C48 C3 0.6(12) . . . . ? C42 C44 C49 C69 -152.0(8) . . . . ? C9 C44 C49 C69 -1.1(13) . . . . ? C42 C44 C49 C78 -7.7(14) . . . . ? C9 C44 C49 C78 143.3(9) . . . . ? C42 C44 C49 Ce3 -84.7(9) . . . . ? C9 C44 C49 Ce3 66.2(9) . . . . ? C11 C47 C51 C21 10.8(14) . . . . ? C48 C47 C51 C21 -140.1(9) . . . . ? C11 C47 C51 C66 150.2(8) . . . . ? C48 C47 C51 C66 -0.7(11) . . . . ? C38 C21 C51 C47 143.1(9) . . . . ? C60 C21 C51 C47 -3.5(14) . . . . ? C38 C21 C51 C66 -0.9(10) . . . . ? C60 C21 C51 C66 -147.5(8) . . . . ? C37 C45 C52 C13 8.7(11) . . . . ? C67 C45 C52 C13 150.9(8) . . . . ? C37 C45 C52 C53 -143.6(8) . . . . ? C67 C45 C52 C53 -1.5(11) . . . . ? C61 C13 C52 C45 -12.2(11) . . . . ? C36 C13 C52 C45 -157.4(7) . . . . ? Ce1 C13 C52 C45 -96.8(7) . . . . ? C61 C13 C52 C53 140.4(8) . . . . ? C36 C13 C52 C53 -4.8(12) . . . . ? Ce1 C13 C52 C53 55.7(8) . . . . ? C16 C41 C53 C59 156.3(9) . . . . ? C35 C41 C53 C59 7.7(12) . . . . ? Ce1 C41 C53 C59 96.6(7) . . . . ? C16 C41 C53 C52 9.3(13) . . . . ? C35 C41 C53 C52 -139.2(9) . . . . ? Ce1 C41 C53 C52 -50.3(8) . . . . ? C45 C52 C53 C59 2.3(11) . . . . ? C13 C52 C53 C59 -149.1(8) . . . . ? C45 C52 C53 C41 148.7(8) . . . . ? C13 C52 C53 C41 -2.7(12) . . . . ? C88 C81 C92 C94 1.0(12) . . . . ? C86 C81 C92 C94 178.0(8) . . . . ? C33 C8 C54 C10 -149.2(8) . . . . ? C15 C8 C54 C10 1.8(12) . . . . ? Ce3 C8 C54 C10 -46.0(9) . . . . ? C33 C8 C54 C4 -7.5(10) . . . . ? C15 C8 C54 C4 143.5(7) . . . . ? Ce3 C8 C54 C4 95.7(8) . . . . ? C33 C8 C54 Ce3 -103.3(8) . . . . ? C15 C8 C54 Ce3 47.8(7) . . . . ? C69 C10 C54 C8 -2.3(12) . . . . ? C7 C10 C54 C8 144.6(8) . . . . ? Ce3 C10 C54 C8 40.4(8) . . . . ? C69 C10 C54 C4 -148.6(7) . . . . ? C7 C10 C54 C4 -1.7(9) . . . . ? Ce3 C10 C54 C4 -105.9(6) . . . . ? C69 C10 C54 Ce3 -42.7(8) . . . . ? C7 C10 C54 Ce3 104.1(7) . . . . ? C58 C4 C54 C8 0.5(11) . . . . ? C17 C4 C54 C8 -158.7(7) . . . . ? C58 C4 C54 C10 148.4(7) . . . . ? C17 C4 C54 C10 -10.7(8) . . . . ? C58 C4 C54 Ce3 67.6(9) . . . . ? C17 C4 C54 Ce3 -91.5(7) . . . . ? C20 C3 C55 C75 142.9(8) . . . . ? C48 C3 C55 C75 -5.1(13) . . . . ? Ce2 C3 C55 C75 67.5(7) . . . . ? C20 C3 C55 C57 3.1(10) . . . . ? C48 C3 C55 C57 -144.9(8) . . . . ? Ce2 C3 C55 C57 -72.2(6) . . . . ? C20 C3 C55 Ce2 75.3(7) . . . . ? C48 C3 C55 Ce2 -72.7(8) . . . . ? C64 Ce2 C55 C75 29.4(5) . . . . ? C14 Ce2 C55 C75 65.9(6) . . . . ? C12 Ce2 C55 C75 101.5(6) . . . . ? C57 Ce2 C55 C75 132.3(9) . . . . ? C2 Ce2 C55 C75 68.9(6) . . . . ? C5 Ce2 C55 C75 117.7(5) . . . . ? C42 Ce2 C55 C75 10.1(5) . . . . ? C11 Ce2 C55 C75 -33.0(5) . . . . ? C32 Ce2 C55 C75 169.3(7) . . . . ? C3 Ce2 C55 C75 -119.3(8) . . . . ? C64 Ce2 C55 C57 -102.9(6) . . . . ? C14 Ce2 C55 C57 -66.4(6) . . . . ? C75 Ce2 C55 C57 -132.3(9) . . . . ? C12 Ce2 C55 C57 -30.8(5) . . . . ? C2 Ce2 C55 C57 -63.4(6) . . . . ? C5 Ce2 C55 C57 -14.6(6) . . . . ? C42 Ce2 C55 C57 -122.2(6) . . . . ? C11 Ce2 C55 C57 -165.3(7) . . . . ? C32 Ce2 C55 C57 36.9(5) . . . . ? C3 Ce2 C55 C57 108.4(9) . . . . ? C64 Ce2 C55 C3 148.7(7) . . . . ? C14 Ce2 C55 C3 -174.7(7) . . . . ? C75 Ce2 C55 C3 119.3(8) . . . . ? C12 Ce2 C55 C3 -139.1(7) . . . . ? C57 Ce2 C55 C3 -108.4(9) . . . . ? C2 Ce2 C55 C3 -171.7(6) . . . . ? C5 Ce2 C55 C3 -123.0(6) . . . . ? C42 Ce2 C55 C3 129.5(6) . . . . ? C11 Ce2 C55 C3 86.3(6) . . . . ? C32 Ce2 C55 C3 -71.4(6) . . . . ? C37 C39 C56 C72 -6.6(13) . . . . ? C25 C39 C56 C72 -147.4(8) . . . . ? C37 C39 C56 C20 144.5(8) . . . . ? C25 C39 C56 C20 3.7(11) . . . . ? C37 C39 C56 Ce4 61.8(10) . . . . ? C25 C39 C56 Ce4 -79.0(9) . . . . ? C3 C20 C56 C72 148.9(9) . . . . ? C32 C20 C56 C72 1.5(13) . . . . ? Ce4 C20 C56 C72 49.3(8) . . . . ? C3 C20 C56 C39 -1.9(12) . . . . ? C32 C20 C56 C39 -149.2(8) . . . . ? Ce4 C20 C56 C39 -101.4(8) . . . . ? C3 C20 C56 Ce4 99.6(9) . . . . ? C32 C20 C56 Ce4 -47.8(8) . . . . ? C14 C12 C57 C55 -3.1(14) . . . . ? C5 C12 C57 C55 -134.9(9) . . . . ? Ce2 C12 C57 C55 -59.7(8) . . . . ? C14 C12 C57 C32 133.3(10) . . . . ? C5 C12 C57 C32 1.4(13) . . . . ? Ce2 C12 C57 C32 76.7(8) . . . . ? C14 C12 C57 Ce2 56.6(8) . . . . ? C5 C12 C57 Ce2 -75.3(7) . . . . ? C75 C55 C57 C12 3.7(14) . . . . ? C3 C55 C57 C12 141.1(8) . . . . ? Ce2 C55 C57 C12 58.8(8) . . . . ? C75 C55 C57 C32 -136.4(9) . . . . ? C3 C55 C57 C32 1.0(10) . . . . ? Ce2 C55 C57 C32 -81.3(6) . . . . ? C75 C55 C57 Ce2 -55.1(9) . . . . ? C3 C55 C57 Ce2 82.3(6) . . . . ? C18 C32 C57 C12 5.7(14) . . . . ? C20 C32 C57 C12 -144.0(8) . . . . ? Ce4 C32 C57 C12 -60.8(11) . . . . ? Ce2 C32 C57 C12 -67.8(8) . . . . ? C18 C32 C57 C55 145.1(9) . . . . ? C20 C32 C57 C55 -4.6(10) . . . . ? Ce4 C32 C57 C55 78.6(9) . . . . ? Ce2 C32 C57 C55 71.6(6) . . . . ? C18 C32 C57 Ce2 73.5(9) . . . . ? C20 C32 C57 Ce2 -76.2(6) . . . . ? Ce4 C32 C57 Ce2 7.0(6) . . . . ? C64 Ce2 C57 C12 -64.3(6) . . . . ? C14 Ce2 C57 C12 -28.1(5) . . . . ? C75 Ce2 C57 C12 -99.0(6) . . . . ? C55 Ce2 C57 C12 -126.9(9) . . . . ? C2 Ce2 C57 C12 -8.9(6) . . . . ? C5 Ce2 C57 C12 35.2(5) . . . . ? C42 Ce2 C57 C12 -67.4(6) . . . . ? C11 Ce2 C57 C12 -115.0(6) . . . . ? C32 Ce2 C57 C12 121.6(8) . . . . ? C3 Ce2 C57 C12 -166.1(7) . . . . ? C64 Ce2 C57 C55 62.6(6) . . . . ? C14 Ce2 C57 C55 98.8(6) . . . . ? C75 Ce2 C57 C55 27.9(6) . . . . ? C12 Ce2 C57 C55 126.9(9) . . . . ? C2 Ce2 C57 C55 118.1(6) . . . . ? C5 Ce2 C57 C55 162.1(7) . . . . ? C42 Ce2 C57 C55 59.5(6) . . . . ? C11 Ce2 C57 C55 12.0(6) . . . . ? C32 Ce2 C57 C55 -111.4(8) . . . . ? C3 Ce2 C57 C55 -39.2(5) . . . . ? C64 Ce2 C57 C32 174.0(6) . . . . ? C14 Ce2 C57 C32 -149.8(6) . . . . ? C75 Ce2 C57 C32 139.3(6) . . . . ? C12 Ce2 C57 C32 -121.6(8) . . . . ? C55 Ce2 C57 C32 111.4(8) . . . . ? C2 Ce2 C57 C32 -130.5(5) . . . . ? C5 Ce2 C57 C32 -86.5(6) . . . . ? C42 Ce2 C57 C32 170.9(5) . . . . ? C11 Ce2 C57 C32 123.4(5) . . . . ? C3 Ce2 C57 C32 72.3(5) . . . . ? C81 C92 C94 C106 -0.3(12) . . . . ? C81 C92 C94 C112 -179.5(8) . . . . ? C54 C4 C58 C62 2.4(10) . . . . ? C17 C4 C58 C62 159.0(7) . . . . ? C54 C4 C58 C28 -159.2(7) . . . . ? C17 C4 C58 C28 -2.6(10) . . . . ? C29 C28 C58 C4 28.4(9) . . . . ? C24 C28 C58 C4 137.3(7) . . . . ? Si1 C28 C58 C4 -82.5(8) . . . . ? C29 C28 C58 C62 -132.3(7) . . . . ? C24 C28 C58 C62 -23.4(10) . . . . ? Si1 C28 C58 C62 116.8(7) . . . . ? C41 C53 C59 C66 -147.7(8) . . . . ? C52 C53 C59 C66 -1.1(11) . . . . ? C41 C53 C59 C38 -5.6(13) . . . . ? C52 C53 C59 C38 141.0(8) . . . . ? C21 C38 C59 C53 -145.2(9) . . . . ? C40 C38 C59 C53 -1.2(14) . . . . ? C21 C38 C59 C66 2.0(9) . . . . ? C40 C38 C59 C66 146.1(8) . . . . ? C96 Si2 C95 Si1 -94.1(9) . . . . ? C111 Si2 C95 Si1 148.8(9) . . . . ? C17 Si2 C95 Si1 20.0(10) . . . . ? C88 Si1 C95 Si2 -119.0(8) . . . . ? C87 Si1 C95 Si2 123.3(8) . . . . ? C28 Si1 C95 Si2 -5.7(10) . . . . ? C11 C6 C60 C78 -150.0(9) . . . . ? C42 C6 C60 C78 -1.4(14) . . . . ? Ce2 C6 C60 C78 -75.0(9) . . . . ? C11 C6 C60 C21 1.7(13) . . . . ? C42 C6 C60 C21 150.2(9) . . . . ? Ce2 C6 C60 C21 76.7(8) . . . . ? C38 C21 C60 C78 4.5(14) . . . . ? C51 C21 C60 C78 148.3(9) . . . . ? C38 C21 C60 C6 -146.8(9) . . . . ? C51 C21 C60 C6 -3.0(13) . . . . ? C34 C23 C61 C65 -156.7(8) . . . . ? C46 C23 C61 C65 -6.4(14) . . . . ? Ce1 C23 C61 C65 -95.0(9) . . . . ? C34 C23 C61 C13 -7.7(10) . . . . ? C46 C23 C61 C13 142.6(8) . . . . ? Ce1 C23 C61 C13 54.0(6) . . . . ? C34 C23 C61 Ce1 -61.7(6) . . . . ? C46 C23 C61 Ce1 88.7(8) . . . . ? C52 C13 C61 C23 -143.8(8) . . . . ? C36 C13 C61 C23 5.5(10) . . . . ? Ce1 C13 C61 C23 -52.8(6) . . . . ? C52 C13 C61 C65 6.6(12) . . . . ? C36 C13 C61 C65 155.9(7) . . . . ? Ce1 C13 C61 C65 97.5(7) . . . . ? C52 C13 C61 Ce1 -91.0(7) . . . . ? C36 C13 C61 Ce1 58.4(5) . . . . ? C74 Ce1 C61 C23 27.3(6) . . . . ? C43 Ce1 C61 C23 46.1(6) . . . . ? C34 Ce1 C61 C23 39.3(6) . . . . ? C36 Ce1 C61 C23 86.2(6) . . . . ? C22 Ce1 C61 C23 80.9(6) . . . . ? C16 Ce1 C61 C23 99.0(6) . . . . ? C1 Ce1 C61 C23 -3.8(6) . . . . ? C33 Ce1 C61 C23 22.0(7) . . . . ? C13 Ce1 C61 C23 124.7(9) . . . . ? C41 Ce1 C61 C23 127.5(6) . . . . ? C63 Ce1 C61 C23 104.4(6) . . . . ? C74 Ce1 C61 C65 146.9(7) . . . . ? C43 Ce1 C61 C65 165.7(6) . . . . ? C34 Ce1 C61 C65 159.0(8) . . . . ? C36 Ce1 C61 C65 -154.2(8) . . . . ? C22 Ce1 C61 C65 -159.4(6) . . . . ? C16 Ce1 C61 C65 -141.3(7) . . . . ? C1 Ce1 C61 C65 115.8(7) . . . . ? C23 Ce1 C61 C65 119.6(9) . . . . ? C33 Ce1 C61 C65 141.6(6) . . . . ? C13 Ce1 C61 C65 -115.6(9) . . . . ? C41 Ce1 C61 C65 -112.8(7) . . . . ? C63 Ce1 C61 C65 -136.0(6) . . . . ? C74 Ce1 C61 C13 -97.4(6) . . . . ? C43 Ce1 C61 C13 -78.7(6) . . . . ? C34 Ce1 C61 C13 -85.4(6) . . . . ? C36 Ce1 C61 C13 -38.5(5) . . . . ? C22 Ce1 C61 C13 -43.8(6) . . . . ? C16 Ce1 C61 C13 -25.7(6) . . . . ? C1 Ce1 C61 C13 -128.5(6) . . . . ? C23 Ce1 C61 C13 -124.7(9) . . . . ? C33 Ce1 C61 C13 -102.7(6) . . . . ? C41 Ce1 C61 C13 2.8(6) . . . . ? C63 Ce1 C61 C13 -20.3(7) . . . . ? C4 C58 C62 C33 2.2(11) . . . . ? C28 C58 C62 C33 163.9(7) . . . . ? C4 C58 C62 C1 -152.2(8) . . . . ? C28 C58 C62 C1 9.5(12) . . . . ? C4 C58 C62 Ce1 -75.4(7) . . . . ? C28 C58 C62 Ce1 86.3(8) . . . . ? C8 C33 C62 C58 -9.6(12) . . . . ? C43 C33 C62 C58 -159.2(7) . . . . ? Ce1 C33 C62 C58 -100.7(7) . . . . ? C8 C33 C62 C1 147.8(7) . . . . ? C43 C33 C62 C1 -1.8(10) . . . . ? Ce1 C33 C62 C1 56.7(6) . . . . ? C8 C33 C62 Ce1 91.1(7) . . . . ? C43 C33 C62 Ce1 -58.5(6) . . . . ? C30 C1 C62 C58 12.2(12) . . . . ? C74 C1 C62 C58 159.7(8) . . . . ? Ce1 C1 C62 C58 100.5(7) . . . . ? C30 C1 C62 C33 -145.4(8) . . . . ? C74 C1 C62 C33 2.1(10) . . . . ? Ce1 C1 C62 C33 -57.1(6) . . . . ? C30 C1 C62 Ce1 -88.3(7) . . . . ? C74 C1 C62 Ce1 59.2(6) . . . . ? C74 Ce1 C62 C58 -158.6(8) . . . . ? C43 Ce1 C62 C58 157.1(8) . . . . ? C34 Ce1 C62 C58 -143.8(7) . . . . ? C36 Ce1 C62 C58 -165.0(6) . . . . ? C22 Ce1 C62 C58 143.4(7) . . . . ? C16 Ce1 C62 C58 160.5(6) . . . . ? C1 Ce1 C62 C58 -118.7(9) . . . . ? C23 Ce1 C62 C58 -113.9(6) . . . . ? C33 Ce1 C62 C58 119.3(9) . . . . ? C13 Ce1 C62 C58 -139.9(6) . . . . ? C41 Ce1 C62 C58 136.4(6) . . . . ? C63 Ce1 C62 C58 114.8(7) . . . . ? C74 Ce1 C62 C33 82.2(6) . . . . ? C43 Ce1 C62 C33 37.9(6) . . . . ? C34 Ce1 C62 C33 96.9(6) . . . . ? C36 Ce1 C62 C33 75.8(6) . . . . ? C22 Ce1 C62 C33 24.1(6) . . . . ? C16 Ce1 C62 C33 41.2(6) . . . . ? C1 Ce1 C62 C33 122.1(8) . . . . ? C23 Ce1 C62 C33 126.8(6) . . . . ? C13 Ce1 C62 C33 100.8(6) . . . . ? C41 Ce1 C62 C33 17.1(7) . . . . ? C63 Ce1 C62 C33 -4.5(6) . . . . ? C74 Ce1 C62 C1 -39.9(6) . . . . ? C43 Ce1 C62 C1 -84.2(6) . . . . ? C34 Ce1 C62 C1 -25.1(5) . . . . ? C36 Ce1 C62 C1 -46.3(6) . . . . ? C22 Ce1 C62 C1 -97.9(6) . . . . ? C16 Ce1 C62 C1 -80.8(6) . . . . ? C23 Ce1 C62 C1 4.7(5) . . . . ? C33 Ce1 C62 C1 -122.1(8) . . . . ? C13 Ce1 C62 C1 -21.3(7) . . . . ? C41 Ce1 C62 C1 -104.9(6) . . . . ? C63 Ce1 C62 C1 -126.6(6) . . . . ? C43 C22 C63 C15 5.6(14) . . . . ? C16 C22 C63 C15 144.4(9) . . . . ? Ce1 C22 C63 C15 72.4(9) . . . . ? C43 C22 C63 C35 -141.3(8) . . . . ? C16 C22 C63 C35 -2.5(11) . . . . ? Ce1 C22 C63 C35 -74.5(7) . . . . ? C43 C22 C63 Ce3 -60.4(10) . . . . ? C16 C22 C63 Ce3 78.5(8) . . . . ? Ce1 C22 C63 Ce3 6.5(6) . . . . ? C43 C22 C63 Ce1 -66.8(7) . . . . ? C16 C22 C63 Ce1 72.0(6) . . . . ? C68 C15 C63 C22 -156.7(9) . . . . ? C8 C15 C63 C22 -4.4(13) . . . . ? Ce3 C15 C63 C22 -94.4(10) . . . . ? C68 C15 C63 C35 -11.5(12) . . . . ? C8 C15 C63 C35 140.7(9) . . . . ? Ce3 C15 C63 C35 50.7(9) . . . . ? C68 C15 C63 Ce3 -62.3(8) . . . . ? C8 C15 C63 Ce3 90.0(9) . . . . ? C68 C15 C63 Ce1 -99.0(8) . . . . ? C8 C15 C63 Ce1 53.3(8) . . . . ? Ce3 C15 C63 Ce1 -36.7(6) . . . . ? C40 C35 C63 C22 155.0(9) . . . . ? C41 C35 C63 C22 4.6(11) . . . . ? Ce3 C35 C63 C22 106.3(9) . . . . ? C40 C35 C63 C15 5.1(14) . . . . ? C41 C35 C63 C15 -145.2(8) . . . . ? Ce3 C35 C63 C15 -43.6(8) . . . . ? C40 C35 C63 Ce3 48.7(10) . . . . ? C41 C35 C63 Ce3 -101.7(8) . . . . ? C40 C35 C63 Ce1 96.2(9) . . . . ? C41 C35 C63 Ce1 -54.2(7) . . . . ? Ce3 C35 C63 Ce1 47.5(5) . . . . ? C74 Ce1 C63 C22 24.9(5) . . . . ? C43 Ce1 C63 C22 35.0(5) . . . . ? C34 Ce1 C63 C22 -6.7(6) . . . . ? C36 Ce1 C63 C22 -36.2(5) . . . . ? C16 Ce1 C63 C22 -43.3(5) . . . . ? C1 Ce1 C63 C22 51.1(5) . . . . ? C23 Ce1 C63 C22 -13.0(6) . . . . ? C33 Ce1 C63 C22 72.2(5) . . . . ? C13 Ce1 C63 C22 -60.2(5) . . . . ? C41 Ce1 C63 C22 -82.7(6) . . . . ? C74 Ce1 C63 C15 -103.3(6) . . . . ? C43 Ce1 C63 C15 -93.2(6) . . . . ? C34 Ce1 C63 C15 -135.0(6) . . . . ? C36 Ce1 C63 C15 -164.5(6) . . . . ? C22 Ce1 C63 C15 -128.2(8) . . . . ? C16 Ce1 C63 C15 -171.6(7) . . . . ? C1 Ce1 C63 C15 -77.2(6) . . . . ? C23 Ce1 C63 C15 -141.2(6) . . . . ? C33 Ce1 C63 C15 -56.1(6) . . . . ? C13 Ce1 C63 C15 171.6(6) . . . . ? C41 Ce1 C63 C15 149.1(8) . . . . ? C74 Ce1 C63 C35 140.2(6) . . . . ? C43 Ce1 C63 C35 150.3(7) . . . . ? C34 Ce1 C63 C35 108.6(6) . . . . ? C36 Ce1 C63 C35 79.0(6) . . . . ? C22 Ce1 C63 C35 115.3(8) . . . . ? C16 Ce1 C63 C35 71.9(6) . . . . ? C1 Ce1 C63 C35 166.4(6) . . . . ? C23 Ce1 C63 C35 102.3(6) . . . . ? C33 Ce1 C63 C35 -172.5(7) . . . . ? C13 Ce1 C63 C35 55.1(6) . . . . ? C41 Ce1 C63 C35 32.6(6) . . . . ? C74 Ce1 C63 Ce3 -146.9(5) . . . . ? C43 Ce1 C63 Ce3 -136.9(6) . . . . ? C34 Ce1 C63 Ce3 -178.6(5) . . . . ? C36 Ce1 C63 Ce3 151.9(5) . . . . ? C22 Ce1 C63 Ce3 -171.9(7) . . . . ? C16 Ce1 C63 Ce3 144.8(6) . . . . ? C1 Ce1 C63 Ce3 -120.8(5) . . . . ? C23 Ce1 C63 Ce3 175.2(5) . . . . ? C33 Ce1 C63 Ce3 -99.7(5) . . . . ? C13 Ce1 C63 Ce3 128.0(5) . . . . ? C41 Ce1 C63 Ce3 105.5(6) . . . . ? C6 C42 C64 C75 3.5(10) . . . . ? C44 C42 C64 C75 -142.1(9) . . . . ? Ce2 C42 C64 C75 -71.0(7) . . . . ? C6 C42 C64 C14 142.8(8) . . . . ? C44 C42 C64 C14 -2.8(14) . . . . ? Ce2 C42 C64 C14 68.2(7) . . . . ? C6 C42 C64 Ce2 74.5(7) . . . . ? C44 C42 C64 Ce2 -71.0(9) . . . . ? C2 C14 C64 C42 -0.9(12) . . . . ? C12 C14 C64 C42 -136.3(9) . . . . ? Ce2 C14 C64 C42 -76.0(8) . . . . ? C2 C14 C64 C75 134.5(9) . . . . ? C12 C14 C64 C75 -0.9(13) . . . . ? Ce2 C14 C64 C75 59.4(8) . . . . ? C2 C14 C64 Ce2 75.1(7) . . . . ? C12 C14 C64 Ce2 -60.3(7) . . . . ? C14 Ce2 C64 C42 120.7(8) . . . . ? C75 Ce2 C64 C42 -111.2(8) . . . . ? C12 Ce2 C64 C42 151.7(6) . . . . ? C55 Ce2 C64 C42 -140.3(6) . . . . ? C57 Ce2 C64 C42 -174.1(6) . . . . ? C2 Ce2 C64 C42 89.0(6) . . . . ? C5 Ce2 C64 C42 132.0(5) . . . . ? C11 Ce2 C64 C42 -73.4(5) . . . . ? C32 Ce2 C64 C42 -171.0(5) . . . . ? C3 Ce2 C64 C42 -124.7(5) . . . . ? C14 Ce2 C64 C75 -128.1(9) . . . . ? C12 Ce2 C64 C75 -97.1(7) . . . . ? C55 Ce2 C64 C75 -29.1(6) . . . . ? C57 Ce2 C64 C75 -62.9(6) . . . . ? C2 Ce2 C64 C75 -159.8(8) . . . . ? C5 Ce2 C64 C75 -116.8(6) . . . . ? C42 Ce2 C64 C75 111.2(8) . . . . ? C11 Ce2 C64 C75 37.8(6) . . . . ? C32 Ce2 C64 C75 -59.9(6) . . . . ? C3 Ce2 C64 C75 -13.5(6) . . . . ? C75 Ce2 C64 C14 128.1(9) . . . . ? C12 Ce2 C64 C14 31.0(5) . . . . ? C55 Ce2 C64 C14 99.0(6) . . . . ? C57 Ce2 C64 C14 65.2(5) . . . . ? C2 Ce2 C64 C14 -31.7(5) . . . . ? C5 Ce2 C64 C14 11.2(5) . . . . ? C42 Ce2 C64 C14 -120.7(8) . . . . ? C11 Ce2 C64 C14 165.9(7) . . . . ? C32 Ce2 C64 C14 68.2(5) . . . . ? C3 Ce2 C64 C14 114.6(6) . . . . ? C109 C82 C96 C99 -2.0(12) . . . . ? C79 C82 C96 C99 -180.0(8) . . . . ? C109 C82 C96 Si2 179.6(7) . . . . ? C79 C82 C96 Si2 1.6(11) . . . . ? C95 Si2 C96 C99 14.8(9) . . . . ? C111 Si2 C96 C99 127.9(8) . . . . ? C17 Si2 C96 C99 -98.8(8) . . . . ? C95 Si2 C96 C82 -167.0(6) . . . . ? C111 Si2 C96 C82 -53.9(7) . . . . ? C17 Si2 C96 C82 79.4(7) . . . . ? C72 C27 C65 C37 -4.4(12) . . . . ? C77 C27 C65 C37 -145.6(8) . . . . ? Ce4 C27 C65 C37 -60.9(9) . . . . ? C72 C27 C65 C61 147.5(8) . . . . ? C77 C27 C65 C61 6.4(13) . . . . ? Ce4 C27 C65 C61 91.0(8) . . . . ? C45 C37 C65 C27 145.6(8) . . . . ? C39 C37 C65 C27 3.9(12) . . . . ? C45 C37 C65 C61 -6.4(12) . . . . ? C39 C37 C65 C61 -148.1(8) . . . . ? C23 C61 C65 C27 -3.9(13) . . . . ? C13 C61 C65 C27 -149.9(8) . . . . ? Ce1 C61 C65 C27 -76.0(9) . . . . ? C23 C61 C65 C37 149.0(9) . . . . ? C13 C61 C65 C37 2.9(11) . . . . ? Ce1 C61 C65 C37 76.9(7) . . . . ? C108 C90 C97 C87 -5.1(14) . . . . ? C108 C90 C97 C91 174.1(9) . . . . ? C84 C87 C97 C90 4.6(13) . . . . ? Si1 C87 C97 C90 -172.7(7) . . . . ? C84 C87 C97 C91 -174.6(9) . . . . ? Si1 C87 C97 C91 8.2(12) . . . . ? C82 C96 C99 C110 3.3(12) . . . . ? Si2 C96 C99 C110 -178.5(7) . . . . ? C82 C96 C99 C80 -178.9(8) . . . . ? Si2 C96 C99 C80 -0.7(13) . . . . ? C53 C59 C66 C67 -1.1(12) . . . . ? C38 C59 C66 C67 -149.0(8) . . . . ? C53 C59 C66 C51 145.3(8) . . . . ? C38 C59 C66 C51 -2.6(9) . . . . ? C47 C51 C66 C67 1.1(12) . . . . ? C21 C51 C66 C67 147.8(8) . . . . ? C47 C51 C66 C59 -144.4(8) . . . . ? C21 C51 C66 C59 2.2(9) . . . . ? C59 C66 C67 C45 2.1(12) . . . . ? C51 C66 C67 C45 -140.2(8) . . . . ? C59 C66 C67 C25 141.9(8) . . . . ? C51 C66 C67 C25 -0.4(12) . . . . ? C37 C45 C67 C66 146.0(8) . . . . ? C52 C45 C67 C66 -0.8(12) . . . . ? C37 C45 C67 C25 3.3(8) . . . . ? C52 C45 C67 C25 -143.5(7) . . . . ? C48 C25 C67 C66 -0.9(12) . . . . ? C39 C25 C67 C66 -147.8(7) . . . . ? C48 C25 C67 C45 142.8(8) . . . . ? C39 C25 C67 C45 -4.1(8) . . . . ? C8 C15 C68 C76 -141.1(9) . . . . ? C63 C15 C68 C76 10.0(13) . . . . ? Ce3 C15 C68 C76 -60.1(9) . . . . ? C8 C15 C68 C69 -1.2(12) . . . . ? C63 C15 C68 C69 149.9(8) . . . . ? Ce3 C15 C68 C69 79.7(9) . . . . ? C8 C15 C68 Ce3 -81.0(8) . . . . ? C63 C15 C68 Ce3 70.1(8) . . . . ? C83 C89 C100 C111 -1.8(16) . . . . ? C83 C89 C100 C113 177.7(11) . . . . ? C44 C49 C69 C10 1.5(13) . . . . ? C78 C49 C69 C10 -148.0(8) . . . . ? Ce3 C49 C69 C10 -92.5(9) . . . . ? C44 C49 C69 C68 144.6(9) . . . . ? C78 C49 C69 C68 -4.9(10) . . . . ? Ce3 C49 C69 C68 50.6(7) . . . . ? C44 C49 C69 Ce3 94.0(9) . . . . ? C78 C49 C69 Ce3 -55.5(8) . . . . ? C7 C10 C69 C49 -4.0(12) . . . . ? C54 C10 C69 C49 140.5(8) . . . . ? Ce3 C10 C69 C49 90.5(9) . . . . ? C7 C10 C69 C68 -143.6(8) . . . . ? C54 C10 C69 C68 0.9(12) . . . . ? Ce3 C10 C69 C68 -49.1(8) . . . . ? C7 C10 C69 Ce3 -94.5(9) . . . . ? C54 C10 C69 Ce3 50.0(9) . . . . ? C15 C68 C69 C49 -141.7(9) . . . . ? C76 C68 C69 C49 2.9(10) . . . . ? Ce3 C68 C69 C49 -73.2(9) . . . . ? C15 C68 C69 C10 0.8(13) . . . . ? C76 C68 C69 C10 145.4(8) . . . . ? Ce3 C68 C69 C10 69.3(9) . . . . ? C15 C68 C69 Ce3 -68.5(9) . . . . ? C76 C68 C69 Ce3 76.1(7) . . . . ? C30 C24 C70 C50 7.8(13) . . . . ? C28 C24 C70 C50 157.1(7) . . . . ? C30 C24 C70 C26 -138.3(8) . . . . ? C28 C24 C70 C26 11.0(9) . . . . ? C30 C24 C70 Ce4 -56.5(10) . . . . ? C28 C24 C70 Ce4 92.9(7) . . . . ? C77 C50 C70 C24 -4.3(13) . . . . ? C73 C50 C70 C24 -144.5(9) . . . . ? Ce4 C50 C70 C24 -95.1(9) . . . . ? C77 C50 C70 C26 139.7(9) . . . . ? C73 C50 C70 C26 -0.6(12) . . . . ? Ce4 C50 C70 C26 48.8(8) . . . . ? C77 C50 C70 Ce4 90.9(9) . . . . ? C73 C50 C70 Ce4 -49.3(7) . . . . ? C71 C26 C70 C24 147.4(8) . . . . ? C29 C26 C70 C24 -1.4(9) . . . . ? Ce4 C26 C70 C24 105.7(7) . . . . ? C71 C26 C70 C50 0.3(12) . . . . ? C29 C26 C70 C50 -148.5(8) . . . . ? Ce4 C26 C70 C50 -41.4(7) . . . . ? C71 C26 C70 Ce4 41.7(8) . . . . ? C29 C26 C70 Ce4 -107.1(7) . . . . ? C89 C83 C102 C103 -0.7(17) . . . . ? C114 C83 C102 C103 177.4(10) . . . . ? C83 C102 C103 C111 -0.1(17) . . . . ? C83 C102 C103 C107 -179.1(10) . . . . ? C87 C84 C105 C108 2.0(15) . . . . ? C98 C84 C105 C108 -179.5(9) . . . . ? C29 C26 C71 C5 -8.1(12) . . . . ? C70 C26 C71 C5 -151.3(8) . . . . ? Ce4 C26 C71 C5 -104.6(8) . . . . ? C29 C26 C71 C18 143.3(8) . . . . ? C70 C26 C71 C18 0.0(12) . . . . ? Ce4 C26 C71 C18 46.7(7) . . . . ? C29 C26 C71 Ce4 96.6(8) . . . . ? C70 C26 C71 Ce4 -46.7(9) . . . . ? C31 C5 C71 C26 11.4(12) . . . . ? C12 C5 C71 C26 157.5(8) . . . . ? Ce2 C5 C71 C26 95.5(7) . . . . ? C31 C5 C71 C18 -140.7(8) . . . . ? C12 C5 C71 C18 5.4(14) . . . . ? Ce2 C5 C71 C18 -56.6(8) . . . . ? C31 C5 C71 Ce4 -84.3(8) . . . . ? C12 C5 C71 Ce4 61.8(10) . . . . ? Ce2 C5 C71 Ce4 -0.3(5) . . . . ? C73 C18 C71 C26 0.0(13) . . . . ? C32 C18 C71 C26 -149.1(8) . . . . ? Ce4 C18 C71 C26 -63.9(9) . . . . ? C73 C18 C71 C5 150.9(9) . . . . ? C32 C18 C71 C5 1.8(12) . . . . ? Ce4 C18 C71 C5 87.0(9) . . . . ? C73 C18 C71 Ce4 63.9(9) . . . . ? C32 C18 C71 Ce4 -85.2(9) . . . . ? C39 C56 C72 C27 6.1(12) . . . . ? C20 C56 C72 C27 -143.9(9) . . . . ? Ce4 C56 C72 C27 -88.6(8) . . . . ? C39 C56 C72 C73 145.3(9) . . . . ? C20 C56 C72 C73 -4.7(13) . . . . ? Ce4 C56 C72 C73 50.6(8) . . . . ? C39 C56 C72 Ce4 94.7(8) . . . . ? C20 C56 C72 Ce4 -55.3(9) . . . . ? C65 C27 C72 C56 -0.8(13) . . . . ? C77 C27 C72 C56 144.6(8) . . . . ? Ce4 C27 C72 C56 81.8(9) . . . . ? C65 C27 C72 C73 -143.0(8) . . . . ? C77 C27 C72 C73 2.4(11) . . . . ? Ce4 C27 C72 C73 -60.4(7) . . . . ? C65 C27 C72 Ce4 -82.6(9) . . . . ? C77 C27 C72 Ce4 62.8(8) . . . . ? C92 C94 C106 C85 2.1(13) . . . . ? C112 C94 C106 C85 -178.7(8) . . . . ? C88 C85 C106 C94 -4.6(12) . . . . ? C93 C85 C106 C94 176.5(8) . . . . ? C32 C18 C73 C72 8.6(14) . . . . ? C71 C18 C73 C72 -140.7(9) . . . . ? Ce4 C18 C73 C72 -62.7(9) . . . . ? C32 C18 C73 C50 149.0(8) . . . . ? C71 C18 C73 C50 -0.3(14) . . . . ? Ce4 C18 C73 C50 77.7(9) . . . . ? C32 C18 C73 Ce4 71.3(8) . . . . ? C71 C18 C73 Ce4 -78.0(9) . . . . ? C56 C72 C73 C18 -0.4(14) . . . . ? C27 C72 C73 C18 142.4(9) . . . . ? Ce4 C72 C73 C18 60.3(9) . . . . ? C56 C72 C73 C50 -146.8(8) . . . . ? C27 C72 C73 C50 -4.0(10) . . . . ? Ce4 C72 C73 C50 -86.2(7) . . . . ? C56 C72 C73 Ce4 -60.6(9) . . . . ? C27 C72 C73 Ce4 82.1(9) . . . . ? C77 C50 C73 C18 -142.7(9) . . . . ? C70 C50 C73 C18 0.6(14) . . . . ? Ce4 C50 C73 C18 -69.2(9) . . . . ? C77 C50 C73 C72 4.3(10) . . . . ? C70 C50 C73 C72 147.6(8) . . . . ? Ce4 C50 C73 C72 77.8(8) . . . . ? C77 C50 C73 Ce4 -73.5(8) . . . . ? C70 C50 C73 Ce4 69.8(9) . . . . ? C22 C43 C74 C1 -139.7(9) . . . . ? C33 C43 C74 C1 0.7(10) . . . . ? Ce1 C43 C74 C1 -78.8(6) . . . . ? C22 C43 C74 C34 -2.2(14) . . . . ? C33 C43 C74 C34 138.2(8) . . . . ? Ce1 C43 C74 C34 58.8(8) . . . . ? C22 C43 C74 Ce1 -60.9(8) . . . . ? C33 C43 C74 Ce1 79.4(6) . . . . ? C62 C1 C74 C43 -1.7(10) . . . . ? C30 C1 C74 C43 142.8(9) . . . . ? Ce1 C1 C74 C43 71.0(6) . . . . ? C62 C1 C74 C34 -142.4(8) . . . . ? C30 C1 C74 C34 2.1(14) . . . . ? Ce1 C1 C74 C34 -69.6(7) . . . . ? C62 C1 C74 Ce1 -72.7(6) . . . . ? C30 C1 C74 Ce1 71.7(9) . . . . ? C23 C34 C74 C43 -130.8(10) . . . . ? C36 C34 C74 C43 1.2(13) . . . . ? Ce1 C34 C74 C43 -58.7(8) . . . . ? C23 C34 C74 C1 4.3(13) . . . . ? C36 C34 C74 C1 136.3(9) . . . . ? Ce1 C34 C74 C1 76.4(7) . . . . ? C23 C34 C74 Ce1 -72.1(8) . . . . ? C36 C34 C74 Ce1 59.9(7) . . . . ? C34 Ce1 C74 C43 130.8(8) . . . . ? C36 Ce1 C74 C43 97.8(6) . . . . ? C22 Ce1 C74 C43 28.7(5) . . . . ? C16 Ce1 C74 C43 63.7(5) . . . . ? C1 Ce1 C74 C43 -111.2(7) . . . . ? C23 Ce1 C74 C43 161.5(6) . . . . ? C33 Ce1 C74 C43 -38.3(5) . . . . ? C13 Ce1 C74 C43 118.0(5) . . . . ? C41 Ce1 C74 C43 60.0(5) . . . . ? C63 Ce1 C74 C43 14.8(5) . . . . ? C43 Ce1 C74 C1 111.2(7) . . . . ? C34 Ce1 C74 C1 -118.0(8) . . . . ? C36 Ce1 C74 C1 -151.0(7) . . . . ? C22 Ce1 C74 C1 139.9(6) . . . . ? C16 Ce1 C74 C1 174.9(6) . . . . ? C23 Ce1 C74 C1 -87.3(6) . . . . ? C33 Ce1 C74 C1 72.9(5) . . . . ? C13 Ce1 C74 C1 -130.8(6) . . . . ? C41 Ce1 C74 C1 171.2(5) . . . . ? C63 Ce1 C74 C1 126.0(5) . . . . ? C43 Ce1 C74 C34 -130.8(8) . . . . ? C36 Ce1 C74 C34 -33.0(5) . . . . ? C22 Ce1 C74 C34 -102.1(6) . . . . ? C16 Ce1 C74 C34 -67.1(5) . . . . ? C1 Ce1 C74 C34 118.0(8) . . . . ? C23 Ce1 C74 C34 30.7(5) . . . . ? C33 Ce1 C74 C34 -169.2(7) . . . . ? C13 Ce1 C74 C34 -12.9(6) . . . . ? C41 Ce1 C74 C34 -70.8(6) . . . . ? C63 Ce1 C74 C34 -116.0(5) . . . . ? C84 C105 C108 C90 -2.2(14) . . . . ? C84 C105 C108 C101 178.8(9) . . . . ? C97 C90 C108 C105 3.9(14) . . . . ? C97 C90 C108 C101 -177.1(9) . . . . ? C96 C82 C109 C104 -1.7(14) . . . . ? C79 C82 C109 C104 176.4(9) . . . . ? C110 C104 C109 C82 4.2(14) . . . . ? C115 C104 C109 C82 178.1(9) . . . . ? C80 C99 C110 C104 -178.8(9) . . . . ? C96 C99 C110 C104 -0.9(14) . . . . ? C109 C104 C110 C99 -3.0(15) . . . . ? C115 C104 C110 C99 -177.2(9) . . . . ? C89 C100 C111 C103 0.9(15) . . . . ? C113 C100 C111 C103 -178.5(10) . . . . ? C89 C100 C111 Si2 -174.5(8) . . . . ? C113 C100 C111 Si2 6.0(15) . . . . ? C102 C103 C111 C100 -0.1(16) . . . . ? C107 C103 C111 C100 178.8(10) . . . . ? C102 C103 C111 Si2 174.8(9) . . . . ? C107 C103 C111 Si2 -6.3(16) . . . . ? C95 Si2 C111 C100 65.9(9) . . . . ? C96 Si2 C111 C100 -58.7(9) . . . . ? C17 Si2 C111 C100 179.6(7) . . . . ? C95 Si2 C111 C103 -109.1(10) . . . . ? C96 Si2 C111 C103 126.2(10) . . . . ? C17 Si2 C111 C103 4.6(12) . . . . ? C42 C64 C75 C55 140.5(10) . . . . ? C14 C64 C75 C55 1.6(15) . . . . ? Ce2 C64 C75 C55 60.7(9) . . . . ? C42 C64 C75 C11 -1.0(11) . . . . ? C14 C64 C75 C11 -139.9(9) . . . . ? Ce2 C64 C75 C11 -80.9(7) . . . . ? C42 C64 C75 Ce2 79.9(7) . . . . ? C14 C64 C75 Ce2 -59.0(8) . . . . ? C57 C55 C75 C64 -3.1(15) . . . . ? C3 C55 C75 C64 -136.6(9) . . . . ? Ce2 C55 C75 C64 -59.4(9) . . . . ? C57 C55 C75 C11 134.9(9) . . . . ? C3 C55 C75 C11 1.4(12) . . . . ? Ce2 C55 C75 C11 78.6(8) . . . . ? C57 C55 C75 Ce2 56.3(9) . . . . ? C3 C55 C75 Ce2 -77.2(7) . . . . ? C47 C11 C75 C64 146.4(9) . . . . ? C6 C11 C75 C64 -1.8(11) . . . . ? Ce2 C11 C75 C64 71.1(6) . . . . ? C47 C11 C75 C55 3.3(14) . . . . ? C6 C11 C75 C55 -144.9(9) . . . . ? Ce2 C11 C75 C55 -72.0(7) . . . . ? C47 C11 C75 Ce2 75.3(9) . . . . ? C6 C11 C75 Ce2 -72.9(7) . . . . ? C14 Ce2 C75 C64 30.9(6) . . . . ? C12 Ce2 C75 C64 67.3(6) . . . . ? C55 Ce2 C75 C64 129.9(9) . . . . ? C57 Ce2 C75 C64 102.3(7) . . . . ? C2 Ce2 C75 C64 16.6(6) . . . . ? C5 Ce2 C75 C64 65.4(6) . . . . ? C42 Ce2 C75 C64 -37.3(6) . . . . ? C11 Ce2 C75 C64 -110.1(9) . . . . ? C32 Ce2 C75 C64 121.5(6) . . . . ? C3 Ce2 C75 C64 163.3(8) . . . . ? C64 Ce2 C75 C55 -129.9(9) . . . . ? C14 Ce2 C75 C55 -99.0(6) . . . . ? C12 Ce2 C75 C55 -62.6(5) . . . . ? C57 Ce2 C75 C55 -27.6(5) . . . . ? C2 Ce2 C75 C55 -113.3(6) . . . . ? C5 Ce2 C75 C55 -64.4(6) . . . . ? C42 Ce2 C75 C55 -167.2(7) . . . . ? C11 Ce2 C75 C55 120.0(8) . . . . ? C32 Ce2 C75 C55 -8.4(5) . . . . ? C3 Ce2 C75 C55 33.5(5) . . . . ? C64 Ce2 C75 C11 110.1(9) . . . . ? C14 Ce2 C75 C11 141.0(7) . . . . ? C12 Ce2 C75 C11 177.4(6) . . . . ? C55 Ce2 C75 C11 -120.0(8) . . . . ? C57 Ce2 C75 C11 -147.7(6) . . . . ? C2 Ce2 C75 C11 126.7(6) . . . . ? C5 Ce2 C75 C11 175.5(5) . . . . ? C42 Ce2 C75 C11 72.8(6) . . . . ? C32 Ce2 C75 C11 -128.4(6) . . . . ? C3 Ce2 C75 C11 -86.6(6) . . . . ? C35 C40 C76 C68 -5.1(14) . . . . ? C38 C40 C76 C68 146.8(9) . . . . ? Ce3 C40 C76 C68 52.0(9) . . . . ? C35 C40 C76 C78 -148.1(9) . . . . ? C38 C40 C76 C78 3.8(14) . . . . ? Ce3 C40 C76 C78 -90.9(10) . . . . ? C35 C40 C76 Ce3 -57.1(10) . . . . ? C38 C40 C76 Ce3 94.8(9) . . . . ? C15 C68 C76 C40 -1.5(14) . . . . ? C69 C68 C76 C40 -146.5(9) . . . . ? Ce3 C68 C76 C40 -59.0(10) . . . . ? C15 C68 C76 C78 145.4(9) . . . . ? C69 C68 C76 C78 0.4(10) . . . . ? Ce3 C68 C76 C78 87.9(9) . . . . ? C15 C68 C76 Ce3 57.5(9) . . . . ? C69 C68 C76 Ce3 -87.5(9) . . . . ? C70 C50 C77 C46 -1.4(14) . . . . ? C73 C50 C77 C46 141.4(9) . . . . ? Ce4 C50 C77 C46 90.6(9) . . . . ? C70 C50 C77 C27 -145.7(8) . . . . ? C73 C50 C77 C27 -2.9(10) . . . . ? Ce4 C50 C77 C27 -53.7(7) . . . . ? C70 C50 C77 Ce4 -92.0(8) . . . . ? C73 C50 C77 Ce4 50.8(6) . . . . ? C23 C46 C77 C50 -150.8(9) . . . . ? C30 C46 C77 C50 3.4(14) . . . . ? C23 C46 C77 C27 -11.0(13) . . . . ? C30 C46 C77 C27 143.1(8) . . . . ? C23 C46 C77 Ce4 -86.2(8) . . . . ? C30 C46 C77 Ce4 68.0(9) . . . . ? C72 C27 C77 C50 0.3(10) . . . . ? C65 C27 C77 C50 146.2(9) . . . . ? Ce4 C27 C77 C50 48.4(7) . . . . ? C72 C27 C77 C46 -144.8(8) . . . . ? C65 C27 C77 C46 1.1(13) . . . . ? Ce4 C27 C77 C46 -96.7(9) . . . . ? C72 C27 C77 Ce4 -48.1(7) . . . . ? C65 C27 C77 Ce4 97.7(9) . . . . ? C6 C60 C78 C76 144.1(9) . . . . ? C21 C60 C78 C76 -7.1(13) . . . . ? C6 C60 C78 C49 7.6(14) . . . . ? C21 C60 C78 C49 -143.7(9) . . . . ? C6 C60 C78 Ce3 91.7(9) . . . . ? C21 C60 C78 Ce3 -59.6(10) . . . . ? C40 C76 C78 C60 3.0(14) . . . . ? C68 C76 C78 C60 -144.3(8) . . . . ? Ce3 C76 C78 C60 -78.9(9) . . . . ? C40 C76 C78 C49 144.0(9) . . . . ? C68 C76 C78 C49 -3.3(11) . . . . ? Ce3 C76 C78 C49 62.1(8) . . . . ? C40 C76 C78 Ce3 81.9(9) . . . . ? C68 C76 C78 Ce3 -65.4(7) . . . . ? C44 C49 C78 C60 -3.1(14) . . . . ? C69 C49 C78 C60 146.0(9) . . . . ? Ce3 C49 C78 C60 95.4(9) . . . . ? C44 C49 C78 C76 -144.1(9) . . . . ? C69 C49 C78 C76 5.0(11) . . . . ? Ce3 C49 C78 C76 -45.6(7) . . . . ? C44 C49 C78 Ce3 -98.4(10) . . . . ? C69 C49 C78 Ce3 50.7(8) . . . . ? C76 C68 Ce3 C15 129.9(9) . . . . ? C69 C68 Ce3 C15 -123.2(8) . . . . ? C15 C68 Ce3 C76 -129.9(9) . . . . ? C69 C68 Ce3 C76 107.0(9) . . . . ? C15 C68 Ce3 C63 -33.1(5) . . . . ? C76 C68 Ce3 C63 96.8(7) . . . . ? C69 C68 Ce3 C63 -156.2(7) . . . . ? C15 C68 Ce3 C40 -102.1(7) . . . . ? C76 C68 Ce3 C40 27.7(6) . . . . ? C69 C68 Ce3 C40 134.7(7) . . . . ? C15 C68 Ce3 C35 -68.7(6) . . . . ? C76 C68 Ce3 C35 61.2(6) . . . . ? C69 C68 Ce3 C35 168.2(7) . . . . ? C15 C68 Ce3 C69 123.2(8) . . . . ? C76 C68 Ce3 C69 -107.0(9) . . . . ? C15 C68 Ce3 C8 32.7(5) . . . . ? C76 C68 Ce3 C8 162.5(8) . . . . ? C69 C68 Ce3 C8 -90.5(6) . . . . ? C15 C68 Ce3 C78 -166.9(7) . . . . ? C76 C68 Ce3 C78 -37.0(5) . . . . ? C69 C68 Ce3 C78 70.0(6) . . . . ? C15 C68 Ce3 C49 156.1(7) . . . . ? C76 C68 Ce3 C49 -74.0(6) . . . . ? C69 C68 Ce3 C49 33.0(5) . . . . ? C15 C68 Ce3 C54 64.6(5) . . . . ? C76 C68 Ce3 C54 -165.5(7) . . . . ? C69 C68 Ce3 C54 -58.6(6) . . . . ? C15 C68 Ce3 C10 95.1(6) . . . . ? C76 C68 Ce3 C10 -135.0(7) . . . . ? C69 C68 Ce3 C10 -28.1(5) . . . . ? C8 C15 Ce3 C68 120.8(8) . . . . ? C63 C15 Ce3 C68 -123.8(8) . . . . ? C68 C15 Ce3 C76 30.8(5) . . . . ? C8 C15 Ce3 C76 151.6(7) . . . . ? C63 C15 Ce3 C76 -93.0(7) . . . . ? C68 C15 Ce3 C63 123.8(8) . . . . ? C8 C15 Ce3 C63 -115.4(9) . . . . ? C68 C15 Ce3 C40 66.2(6) . . . . ? C8 C15 Ce3 C40 -173.0(7) . . . . ? C63 C15 Ce3 C40 -57.6(7) . . . . ? C68 C15 Ce3 C35 97.1(6) . . . . ? C8 C15 Ce3 C35 -142.2(7) . . . . ? C63 C15 Ce3 C35 -26.7(6) . . . . ? C68 C15 Ce3 C69 -31.8(5) . . . . ? C8 C15 Ce3 C69 89.0(6) . . . . ? C63 C15 Ce3 C69 -155.6(7) . . . . ? C68 C15 Ce3 C8 -120.8(8) . . . . ? C63 C15 Ce3 C8 115.4(9) . . . . ? C68 C15 Ce3 C78 10.8(6) . . . . ? C8 C15 Ce3 C78 131.6(7) . . . . ? C63 C15 Ce3 C78 -113.0(7) . . . . ? C68 C15 Ce3 C49 -18.9(5) . . . . ? C8 C15 Ce3 C49 101.9(7) . . . . ? C63 C15 Ce3 C49 -142.7(6) . . . . ? C68 C15 Ce3 C54 -91.9(6) . . . . ? C8 C15 Ce3 C54 28.9(5) . . . . ? C63 C15 Ce3 C54 144.3(7) . . . . ? C68 C15 Ce3 C10 -63.0(6) . . . . ? C8 C15 Ce3 C10 57.8(6) . . . . ? C63 C15 Ce3 C10 173.2(7) . . . . ? C40 C76 Ce3 C68 132.3(10) . . . . ? C78 C76 Ce3 C68 -107.5(8) . . . . ? C40 C76 Ce3 C15 100.9(7) . . . . ? C68 C76 Ce3 C15 -31.5(6) . . . . ? C78 C76 Ce3 C15 -139.0(7) . . . . ? C40 C76 Ce3 C63 62.6(6) . . . . ? C68 C76 Ce3 C63 -69.8(7) . . . . ? C78 C76 Ce3 C63 -177.3(6) . . . . ? C68 C76 Ce3 C40 -132.3(10) . . . . ? C78 C76 Ce3 C40 120.1(8) . . . . ? C40 C76 Ce3 C35 28.6(6) . . . . ? C68 C76 Ce3 C35 -103.7(8) . . . . ? C78 C76 Ce3 C35 148.7(6) . . . . ? C40 C76 Ce3 C69 172.4(8) . . . . ? C68 C76 Ce3 C69 40.0(6) . . . . ? C78 C76 Ce3 C69 -67.5(6) . . . . ? C40 C76 Ce3 C8 116.6(8) . . . . ? C68 C76 Ce3 C8 -15.8(7) . . . . ? C78 C76 Ce3 C8 -123.3(7) . . . . ? C40 C76 Ce3 C78 -120.1(8) . . . . ? C68 C76 Ce3 C78 107.5(8) . . . . ? C40 C76 Ce3 C49 -152.5(7) . . . . ? C68 C76 Ce3 C49 75.1(6) . . . . ? C78 C76 Ce3 C49 -32.4(5) . . . . ? C40 C76 Ce3 C54 145.7(8) . . . . ? C68 C76 Ce3 C54 13.4(7) . . . . ? C78 C76 Ce3 C54 -94.1(7) . . . . ? C40 C76 Ce3 C10 168.1(7) . . . . ? C68 C76 Ce3 C10 35.7(6) . . . . ? C78 C76 Ce3 C10 -71.8(6) . . . . ? C22 C63 Ce3 C68 154.5(7) . . . . ? C15 C63 Ce3 C68 35.4(6) . . . . ? C35 C63 Ce3 C68 -98.8(7) . . . . ? Ce1 C63 Ce3 C68 162.2(6) . . . . ? C22 C63 Ce3 C15 119.1(9) . . . . ? C35 C63 Ce3 C15 -134.2(9) . . . . ? Ce1 C63 Ce3 C15 126.7(7) . . . . ? C22 C63 Ce3 C76 -165.5(7) . . . . ? C15 C63 Ce3 C76 75.4(7) . . . . ? C35 C63 Ce3 C76 -58.8(6) . . . . ? Ce1 C63 Ce3 C76 -157.8(6) . . . . ? C22 C63 Ce3 C40 -130.1(7) . . . . ? C15 C63 Ce3 C40 110.8(8) . . . . ? C35 C63 Ce3 C40 -23.4(6) . . . . ? Ce1 C63 Ce3 C40 -122.5(5) . . . . ? C22 C63 Ce3 C35 -106.7(8) . . . . ? C15 C63 Ce3 C35 134.2(9) . . . . ? Ce1 C63 Ce3 C35 -99.0(6) . . . . ? C22 C63 Ce3 C69 141.1(7) . . . . ? C15 C63 Ce3 C69 22.1(6) . . . . ? C35 C63 Ce3 C69 -112.1(7) . . . . ? Ce1 C63 Ce3 C69 148.8(7) . . . . ? C22 C63 Ce3 C8 82.8(7) . . . . ? C15 C63 Ce3 C8 -36.2(5) . . . . ? C35 C63 Ce3 C8 -170.4(8) . . . . ? Ce1 C63 Ce3 C8 90.5(5) . . . . ? C22 C63 Ce3 C78 -167.0(6) . . . . ? C15 C63 Ce3 C78 73.9(8) . . . . ? C35 C63 Ce3 C78 -60.3(7) . . . . ? Ce1 C63 Ce3 C78 -159.3(7) . . . . ? C22 C63 Ce3 C49 162.9(6) . . . . ? C15 C63 Ce3 C49 43.8(7) . . . . ? C35 C63 Ce3 C49 -90.4(8) . . . . ? Ce1 C63 Ce3 C49 170.6(8) . . . . ? C22 C63 Ce3 C54 90.5(7) . . . . ? C15 C63 Ce3 C54 -28.5(6) . . . . ? C35 C63 Ce3 C54 -162.8(7) . . . . ? Ce1 C63 Ce3 C54 98.2(5) . . . . ? C22 C63 Ce3 C10 112.6(7) . . . . ? C15 C63 Ce3 C10 -6.4(6) . . . . ? C35 C63 Ce3 C10 -140.6(8) . . . . ? Ce1 C63 Ce3 C10 120.3(7) . . . . ? C35 C40 Ce3 C68 99.1(8) . . . . ? C38 C40 Ce3 C68 -144.7(9) . . . . ? C76 C40 Ce3 C68 -30.2(7) . . . . ? C35 C40 Ce3 C15 59.7(7) . . . . ? C38 C40 Ce3 C15 175.9(8) . . . . ? C76 C40 Ce3 C15 -69.7(7) . . . . ? C35 C40 Ce3 C76 129.3(9) . . . . ? C38 C40 Ce3 C76 -114.4(10) . . . . ? C35 C40 Ce3 C63 24.8(6) . . . . ? C38 C40 Ce3 C63 141.0(8) . . . . ? C76 C40 Ce3 C63 -104.5(7) . . . . ? C38 C40 Ce3 C35 116.2(9) . . . . ? C76 C40 Ce3 C35 -129.3(9) . . . . ? C35 C40 Ce3 C69 122.9(8) . . . . ? C38 C40 Ce3 C69 -120.9(8) . . . . ? C76 C40 Ce3 C69 -6.4(7) . . . . ? C35 C40 Ce3 C8 55.4(9) . . . . ? C38 C40 Ce3 C8 171.6(8) . . . . ? C76 C40 Ce3 C8 -73.9(9) . . . . ? C35 C40 Ce3 C78 161.7(7) . . . . ? C38 C40 Ce3 C78 -82.0(8) . . . . ? C76 C40 Ce3 C78 32.4(6) . . . . ? C35 C40 Ce3 C49 151.0(7) . . . . ? C38 C40 Ce3 C49 -92.8(8) . . . . ? C76 C40 Ce3 C49 21.7(6) . . . . ? C35 C40 Ce3 C54 83.3(11) . . . . ? C38 C40 Ce3 C54 -160.5(10) . . . . ? C76 C40 Ce3 C54 -46.1(11) . . . . ? C35 C40 Ce3 C10 115.5(9) . . . . ? C38 C40 Ce3 C10 -128.3(9) . . . . ? C76 C40 Ce3 C10 -13.8(9) . . . . ? C40 C35 Ce3 C68 -69.9(7) . . . . ? C41 C35 Ce3 C68 169.7(8) . . . . ? C63 C35 Ce3 C68 69.3(7) . . . . ? C40 C35 Ce3 C15 -110.9(8) . . . . ? C41 C35 Ce3 C15 128.7(8) . . . . ? C63 C35 Ce3 C15 28.3(6) . . . . ? C40 C35 Ce3 C76 -30.9(6) . . . . ? C41 C35 Ce3 C76 -151.3(8) . . . . ? C63 C35 Ce3 C76 108.3(7) . . . . ? C40 C35 Ce3 C63 -139.2(9) . . . . ? C41 C35 Ce3 C63 100.4(9) . . . . ? C41 C35 Ce3 C40 -120.4(9) . . . . ? C63 C35 Ce3 C40 139.2(9) . . . . ? C40 C35 Ce3 C69 -62.8(8) . . . . ? C41 C35 Ce3 C69 176.8(7) . . . . ? C63 C35 Ce3 C69 76.4(8) . . . . ? C40 C35 Ce3 C8 -131.0(8) . . . . ? C41 C35 Ce3 C8 108.6(8) . . . . ? C63 C35 Ce3 C8 8.2(6) . . . . ? C40 C35 Ce3 C78 -15.3(6) . . . . ? C41 C35 Ce3 C78 -135.7(7) . . . . ? C63 C35 Ce3 C78 123.9(7) . . . . ? C40 C35 Ce3 C49 -31.9(7) . . . . ? C41 C35 Ce3 C49 -152.3(7) . . . . ? C63 C35 Ce3 C49 107.3(8) . . . . ? C40 C35 Ce3 C54 -119.3(10) . . . . ? C41 C35 Ce3 C54 120.3(9) . . . . ? C63 C35 Ce3 C54 19.9(9) . . . . ? C40 C35 Ce3 C10 -87.1(10) . . . . ? C41 C35 Ce3 C10 152.5(9) . . . . ? C63 C35 Ce3 C10 52.1(10) . . . . ? C49 C69 Ce3 C68 116.2(9) . . . . ? C10 C69 Ce3 C68 -125.6(9) . . . . ? C49 C69 Ce3 C15 152.7(8) . . . . ? C10 C69 Ce3 C15 -89.1(7) . . . . ? C68 C69 Ce3 C15 36.5(6) . . . . ? C49 C69 Ce3 C76 70.8(7) . . . . ? C10 C69 Ce3 C76 -171.0(8) . . . . ? C68 C69 Ce3 C76 -45.4(6) . . . . ? C49 C69 Ce3 C63 138.1(7) . . . . ? C10 C69 Ce3 C63 -103.7(8) . . . . ? C68 C69 Ce3 C63 21.9(7) . . . . ? C49 C69 Ce3 C40 75.2(8) . . . . ? C10 C69 Ce3 C40 -166.6(8) . . . . ? C68 C69 Ce3 C40 -41.0(7) . . . . ? C49 C69 Ce3 C35 104.0(8) . . . . ? C10 C69 Ce3 C35 -137.8(8) . . . . ? C68 C69 Ce3 C35 -12.2(7) . . . . ? C49 C69 Ce3 C8 -170.3(7) . . . . ? C10 C69 Ce3 C8 -52.1(6) . . . . ? C68 C69 Ce3 C8 73.6(7) . . . . ? C49 C69 Ce3 C78 32.7(6) . . . . ? C10 C69 Ce3 C78 151.0(8) . . . . ? C68 C69 Ce3 C78 -83.4(7) . . . . ? C10 C69 Ce3 C49 118.2(9) . . . . ? C68 C69 Ce3 C49 -116.2(9) . . . . ? C49 C69 Ce3 C54 -143.0(8) . . . . ? C10 C69 Ce3 C54 -24.8(6) . . . . ? C68 C69 Ce3 C54 100.8(7) . . . . ? C49 C69 Ce3 C10 -118.2(9) . . . . ? C68 C69 Ce3 C10 125.6(9) . . . . ? C54 C8 Ce3 C68 86.4(7) . . . . ? C33 C8 Ce3 C68 -156.0(8) . . . . ? C15 C8 Ce3 C68 -38.1(7) . . . . ? C54 C8 Ce3 C15 124.4(9) . . . . ? C33 C8 Ce3 C15 -117.9(9) . . . . ? C54 C8 Ce3 C76 97.4(8) . . . . ? C33 C8 Ce3 C76 -145.0(8) . . . . ? C15 C8 Ce3 C76 -27.0(7) . . . . ? C54 C8 Ce3 C63 163.9(7) . . . . ? C33 C8 Ce3 C63 -78.5(7) . . . . ? C15 C8 Ce3 C63 39.4(6) . . . . ? C54 C8 Ce3 C40 131.9(9) . . . . ? C33 C8 Ce3 C40 -110.4(9) . . . . ? C15 C8 Ce3 C40 7.5(8) . . . . ? C54 C8 Ce3 C35 158.4(8) . . . . ? C33 C8 Ce3 C35 -83.9(8) . . . . ? C15 C8 Ce3 C35 34.0(7) . . . . ? C54 C8 Ce3 C69 48.8(6) . . . . ? C33 C8 Ce3 C69 166.4(7) . . . . ? C15 C8 Ce3 C69 -75.7(7) . . . . ? C54 C8 Ce3 C78 68.6(9) . . . . ? C33 C8 Ce3 C78 -173.8(8) . . . . ? C15 C8 Ce3 C78 -55.9(8) . . . . ? C54 C8 Ce3 C49 44.0(7) . . . . ? C33 C8 Ce3 C49 161.7(7) . . . . ? C15 C8 Ce3 C49 -80.4(8) . . . . ? C33 C8 Ce3 C54 117.7(8) . . . . ? C15 C8 Ce3 C54 -124.4(9) . . . . ? C54 C8 Ce3 C10 20.8(5) . . . . ? C33 C8 Ce3 C10 138.5(7) . . . . ? C15 C8 Ce3 C10 -103.6(8) . . . . ? C60 C78 Ce3 C68 166.7(8) . . . . ? C76 C78 Ce3 C68 46.6(6) . . . . ? C49 C78 Ce3 C68 -74.8(7) . . . . ? C60 C78 Ce3 C15 158.3(7) . . . . ? C76 C78 Ce3 C15 38.2(7) . . . . ? C49 C78 Ce3 C15 -83.2(8) . . . . ? C60 C78 Ce3 C76 120.0(9) . . . . ? C49 C78 Ce3 C76 -121.4(9) . . . . ? C60 C78 Ce3 C63 122.8(7) . . . . ? C76 C78 Ce3 C63 2.8(6) . . . . ? C49 C78 Ce3 C63 -118.7(8) . . . . ? C60 C78 Ce3 C40 83.3(7) . . . . ? C76 C78 Ce3 C40 -36.7(6) . . . . ? C49 C78 Ce3 C40 -158.2(8) . . . . ? C60 C78 Ce3 C35 93.1(7) . . . . ? C76 C78 Ce3 C35 -27.0(6) . . . . ? C49 C78 Ce3 C35 -148.4(7) . . . . ? C60 C78 Ce3 C69 -150.2(8) . . . . ? C76 C78 Ce3 C69 89.7(7) . . . . ? C49 C78 Ce3 C69 -31.7(6) . . . . ? C60 C78 Ce3 C8 -174.0(8) . . . . ? C76 C78 Ce3 C8 65.9(8) . . . . ? C49 C78 Ce3 C8 -55.5(9) . . . . ? C60 C78 Ce3 C49 -118.5(9) . . . . ? C76 C78 Ce3 C49 121.4(9) . . . . ? C60 C78 Ce3 C54 -146.8(7) . . . . ? C76 C78 Ce3 C54 93.2(8) . . . . ? C49 C78 Ce3 C54 -28.3(7) . . . . ? C60 C78 Ce3 C10 -136.5(7) . . . . ? C76 C78 Ce3 C10 103.5(7) . . . . ? C49 C78 Ce3 C10 -18.0(6) . . . . ? C44 C49 Ce3 C68 -157.2(8) . . . . ? C69 C49 Ce3 C68 -39.5(6) . . . . ? C78 C49 Ce3 C68 83.1(7) . . . . ? C44 C49 Ce3 C15 -142.1(7) . . . . ? C69 C49 Ce3 C15 -24.4(7) . . . . ? C78 C49 Ce3 C15 98.1(8) . . . . ? C44 C49 Ce3 C76 153.6(8) . . . . ? C69 C49 Ce3 C76 -88.7(8) . . . . ? C78 C49 Ce3 C76 33.8(6) . . . . ? C44 C49 Ce3 C63 -166.8(7) . . . . ? C69 C49 Ce3 C63 -49.1(8) . . . . ? C78 C49 Ce3 C63 73.4(8) . . . . ? C44 C49 Ce3 C40 138.0(7) . . . . ? C69 C49 Ce3 C40 -104.3(8) . . . . ? C78 C49 Ce3 C40 18.2(7) . . . . ? C44 C49 Ce3 C35 154.6(7) . . . . ? C69 C49 Ce3 C35 -87.7(9) . . . . ? C78 C49 Ce3 C35 34.9(8) . . . . ? C44 C49 Ce3 C69 -117.7(9) . . . . ? C78 C49 Ce3 C69 122.5(10) . . . . ? C44 C49 Ce3 C8 -108.6(7) . . . . ? C69 C49 Ce3 C8 9.1(7) . . . . ? C78 C49 Ce3 C8 131.6(8) . . . . ? C44 C49 Ce3 C78 119.8(9) . . . . ? C69 C49 Ce3 C78 -122.5(10) . . . . ? C44 C49 Ce3 C54 -88.6(7) . . . . ? C69 C49 Ce3 C54 29.1(6) . . . . ? C78 C49 Ce3 C54 151.7(7) . . . . ? C44 C49 Ce3 C10 -83.8(7) . . . . ? C69 C49 Ce3 C10 33.9(6) . . . . ? C78 C49 Ce3 C10 156.5(8) . . . . ? C8 C54 Ce3 C68 -79.3(8) . . . . ? C10 C54 Ce3 C68 63.2(7) . . . . ? C4 C54 Ce3 C68 165.4(8) . . . . ? C8 C54 Ce3 C15 -34.4(6) . . . . ? C10 C54 Ce3 C15 108.1(8) . . . . ? C4 C54 Ce3 C15 -149.6(8) . . . . ? C8 C54 Ce3 C76 -88.6(9) . . . . ? C10 C54 Ce3 C76 53.9(8) . . . . ? C4 C54 Ce3 C76 156.2(8) . . . . ? C8 C54 Ce3 C63 -13.8(6) . . . . ? C10 C54 Ce3 C63 128.7(8) . . . . ? C4 C54 Ce3 C63 -129.0(7) . . . . ? C8 C54 Ce3 C40 -63.2(11) . . . . ? C10 C54 Ce3 C40 79.3(11) . . . . ? C4 C54 Ce3 C40 -178.5(10) . . . . ? C8 C54 Ce3 C35 -25.0(9) . . . . ? C10 C54 Ce3 C35 117.5(10) . . . . ? C4 C54 Ce3 C35 -140.3(9) . . . . ? C8 C54 Ce3 C69 -117.3(8) . . . . ? C10 C54 Ce3 C69 25.2(6) . . . . ? C4 C54 Ce3 C69 127.5(8) . . . . ? C10 C54 Ce3 C8 142.5(9) . . . . ? C4 C54 Ce3 C8 -115.2(9) . . . . ? C8 C54 Ce3 C78 -120.7(8) . . . . ? C10 C54 Ce3 C78 21.8(7) . . . . ? C4 C54 Ce3 C78 124.1(7) . . . . ? C8 C54 Ce3 C49 -134.8(7) . . . . ? C10 C54 Ce3 C49 7.7(6) . . . . ? C4 C54 Ce3 C49 110.0(7) . . . . ? C8 C54 Ce3 C10 -142.5(9) . . . . ? C4 C54 Ce3 C10 102.3(8) . . . . ? C69 C10 Ce3 C68 34.0(7) . . . . ? C7 C10 Ce3 C68 148.6(8) . . . . ? C54 C10 Ce3 C68 -101.3(8) . . . . ? C69 C10 Ce3 C15 77.8(8) . . . . ? C7 C10 Ce3 C15 -167.7(8) . . . . ? C54 C10 Ce3 C15 -57.6(7) . . . . ? C69 C10 Ce3 C76 7.6(7) . . . . ? C7 C10 Ce3 C76 122.1(8) . . . . ? C54 C10 Ce3 C76 -127.7(8) . . . . ? C69 C10 Ce3 C63 82.0(9) . . . . ? C7 C10 Ce3 C63 -163.5(7) . . . . ? C54 C10 Ce3 C63 -53.4(8) . . . . ? C69 C10 Ce3 C40 15.6(9) . . . . ? C7 C10 Ce3 C40 130.1(9) . . . . ? C54 C10 Ce3 C40 -119.7(10) . . . . ? C69 C10 Ce3 C35 54.3(10) . . . . ? C7 C10 Ce3 C35 168.9(9) . . . . ? C54 C10 Ce3 C35 -81.0(10) . . . . ? C7 C10 Ce3 C69 114.5(10) . . . . ? C54 C10 Ce3 C69 -135.3(10) . . . . ? C69 C10 Ce3 C8 114.0(8) . . . . ? C7 C10 Ce3 C8 -131.5(8) . . . . ? C54 C10 Ce3 C8 -21.3(5) . . . . ? C69 C10 Ce3 C78 -22.8(6) . . . . ? C7 C10 Ce3 C78 91.7(7) . . . . ? C54 C10 Ce3 C78 -158.2(7) . . . . ? C69 C10 Ce3 C49 -34.7(6) . . . . ? C7 C10 Ce3 C49 79.9(7) . . . . ? C54 C10 Ce3 C49 -170.0(8) . . . . ? C69 C10 Ce3 C54 135.3(10) . . . . ? C7 C10 Ce3 C54 -110.1(8) . . . . ? C72 C73 Ce4 C18 131.2(8) . . . . ? C50 C73 Ce4 C18 -124.5(7) . . . . ? C18 C73 Ce4 C72 -131.2(8) . . . . ? C50 C73 Ce4 C72 104.3(8) . . . . ? C18 C73 Ce4 C32 -33.3(5) . . . . ? C72 C73 Ce4 C32 97.9(6) . . . . ? C50 C73 Ce4 C32 -157.8(6) . . . . ? C18 C73 Ce4 C56 -102.4(6) . . . . ? C72 C73 Ce4 C56 28.8(6) . . . . ? C50 C73 Ce4 C56 133.1(6) . . . . ? C18 C73 Ce4 C50 124.5(7) . . . . ? C72 C73 Ce4 C50 -104.3(8) . . . . ? C18 C73 Ce4 C20 -67.8(6) . . . . ? C72 C73 Ce4 C20 63.4(6) . . . . ? C50 C73 Ce4 C20 167.7(6) . . . . ? C18 C73 Ce4 C71 32.9(5) . . . . ? C72 C73 Ce4 C71 164.1(7) . . . . ? C50 C73 Ce4 C71 -91.6(5) . . . . ? C18 C73 Ce4 C27 -166.1(6) . . . . ? C72 C73 Ce4 C27 -34.9(5) . . . . ? C50 C73 Ce4 C27 69.4(5) . . . . ? C18 C73 Ce4 C77 156.8(6) . . . . ? C72 C73 Ce4 C77 -72.0(6) . . . . ? C50 C73 Ce4 C77 32.3(4) . . . . ? C18 C73 Ce4 C70 95.6(6) . . . . ? C72 C73 Ce4 C70 -133.2(7) . . . . ? C50 C73 Ce4 C70 -28.9(4) . . . . ? C18 C73 Ce4 C26 64.4(5) . . . . ? C72 C73 Ce4 C26 -164.5(7) . . . . ? C50 C73 Ce4 C26 -60.2(5) . . . . ? C32 C18 Ce4 C73 -121.9(7) . . . . ? C71 C18 Ce4 C73 120.7(8) . . . . ? C73 C18 Ce4 C72 30.8(5) . . . . ? C32 C18 Ce4 C72 -91.1(6) . . . . ? C71 C18 Ce4 C72 151.5(7) . . . . ? C73 C18 Ce4 C32 121.9(7) . . . . ? C71 C18 Ce4 C32 -117.4(8) . . . . ? C73 C18 Ce4 C56 65.8(6) . . . . ? C32 C18 Ce4 C56 -56.1(6) . . . . ? C71 C18 Ce4 C56 -173.5(7) . . . . ? C73 C18 Ce4 C50 -32.6(5) . . . . ? C32 C18 Ce4 C50 -154.5(6) . . . . ? C71 C18 Ce4 C50 88.1(6) . . . . ? C73 C18 Ce4 C20 97.9(6) . . . . ? C32 C18 Ce4 C20 -24.0(5) . . . . ? C71 C18 Ce4 C20 -141.3(7) . . . . ? C73 C18 Ce4 C71 -120.7(8) . . . . ? C32 C18 Ce4 C71 117.4(8) . . . . ? C73 C18 Ce4 C27 11.9(6) . . . . ? C32 C18 Ce4 C27 -110.0(6) . . . . ? C71 C18 Ce4 C27 132.6(7) . . . . ? C73 C18 Ce4 C77 -19.0(5) . . . . ? C32 C18 Ce4 C77 -140.9(6) . . . . ? C71 C18 Ce4 C77 101.7(6) . . . . ? C73 C18 Ce4 C70 -64.5(5) . . . . ? C32 C18 Ce4 C70 173.6(6) . . . . ? C71 C18 Ce4 C70 56.2(6) . . . . ? C73 C18 Ce4 C26 -94.1(6) . . . . ? C32 C18 Ce4 C26 144.0(6) . . . . ? C71 C18 Ce4 C26 26.6(5) . . . . ? C56 C72 Ce4 C73 129.1(9) . . . . ? C27 C72 Ce4 C73 -111.4(9) . . . . ? C56 C72 Ce4 C18 98.4(7) . . . . ? C27 C72 Ce4 C18 -142.2(7) . . . . ? C73 C72 Ce4 C18 -30.7(6) . . . . ? C56 C72 Ce4 C32 61.2(6) . . . . ? C27 C72 Ce4 C32 -179.4(7) . . . . ? C73 C72 Ce4 C32 -67.9(7) . . . . ? C27 C72 Ce4 C56 119.5(9) . . . . ? C73 C72 Ce4 C56 -129.1(9) . . . . ? C56 C72 Ce4 C50 171.9(8) . . . . ? C27 C72 Ce4 C50 -68.7(6) . . . . ? C73 C72 Ce4 C50 42.8(6) . . . . ? C56 C72 Ce4 C20 27.7(6) . . . . ? C27 C72 Ce4 C20 147.1(7) . . . . ? C73 C72 Ce4 C20 -101.4(7) . . . . ? C56 C72 Ce4 C71 114.5(7) . . . . ? C27 C72 Ce4 C71 -126.0(7) . . . . ? C73 C72 Ce4 C71 -14.6(7) . . . . ? C56 C72 Ce4 C27 -119.5(9) . . . . ? C73 C72 Ce4 C27 111.4(9) . . . . ? C56 C72 Ce4 C77 -153.0(7) . . . . ? C27 C72 Ce4 C77 -33.5(5) . . . . ? C73 C72 Ce4 C77 77.9(6) . . . . ? C56 C72 Ce4 C70 167.4(7) . . . . ? C27 C72 Ce4 C70 -73.1(7) . . . . ? C73 C72 Ce4 C70 38.3(6) . . . . ? C56 C72 Ce4 C26 144.1(7) . . . . ? C27 C72 Ce4 C26 -96.4(7) . . . . ? C73 C72 Ce4 C26 15.0(7) . . . . ? C18 C32 Ce4 C73 37.1(6) . . . . ? C57 C32 Ce4 C73 155.7(8) . . . . ? C20 C32 Ce4 C73 -101.9(7) . . . . ? Ce2 C32 Ce4 C73 163.8(6) . . . . ? C57 C32 Ce4 C18 118.5(9) . . . . ? C20 C32 Ce4 C18 -139.0(9) . . . . ? Ce2 C32 Ce4 C18 126.6(7) . . . . ? C18 C32 Ce4 C72 78.5(7) . . . . ? C57 C32 Ce4 C72 -162.9(7) . . . . ? C20 C32 Ce4 C72 -60.5(6) . . . . ? Ce2 C32 Ce4 C72 -154.8(6) . . . . ? C18 C32 Ce4 C56 112.8(7) . . . . ? C57 C32 Ce4 C56 -128.6(7) . . . . ? C20 C32 Ce4 C56 -26.2(6) . . . . ? Ce2 C32 Ce4 C56 -120.5(6) . . . . ? C18 C32 Ce4 C50 23.8(6) . . . . ? C57 C32 Ce4 C50 142.3(7) . . . . ? C20 C32 Ce4 C50 -115.2(7) . . . . ? Ce2 C32 Ce4 C50 150.4(6) . . . . ? C18 C32 Ce4 C20 139.0(9) . . . . ? C57 C32 Ce4 C20 -102.4(9) . . . . ? Ce2 C32 Ce4 C20 -94.3(6) . . . . ? C18 C32 Ce4 C71 -35.9(5) . . . . ? C57 C32 Ce4 C71 82.6(7) . . . . ? C20 C32 Ce4 C71 -175.0(8) . . . . ? Ce2 C32 Ce4 C71 90.7(4) . . . . ? C18 C32 Ce4 C27 78.2(8) . . . . ? C57 C32 Ce4 C27 -163.3(7) . . . . ? C20 C32 Ce4 C27 -60.9(8) . . . . ? Ce2 C32 Ce4 C27 -155.2(8) . . . . ? C18 C32 Ce4 C77 46.9(7) . . . . ? C57 C32 Ce4 C77 165.4(7) . . . . ? C20 C32 Ce4 C77 -92.2(8) . . . . ? Ce2 C32 Ce4 C77 173.5(8) . . . . ? C18 C32 Ce4 C70 -6.2(6) . . . . ? C57 C32 Ce4 C70 112.4(7) . . . . ? C20 C32 Ce4 C70 -145.2(7) . . . . ? Ce2 C32 Ce4 C70 120.4(6) . . . . ? C18 C32 Ce4 C26 -29.4(5) . . . . ? C57 C32 Ce4 C26 89.1(7) . . . . ? C20 C32 Ce4 C26 -168.5(7) . . . . ? Ce2 C32 Ce4 C26 97.2(4) . . . . ? C72 C56 Ce4 C73 -33.2(7) . . . . ? C39 C56 Ce4 C73 -147.2(8) . . . . ? C20 C56 Ce4 C73 99.6(8) . . . . ? C72 C56 Ce4 C18 -73.0(7) . . . . ? C39 C56 Ce4 C18 173.0(8) . . . . ? C20 C56 Ce4 C18 59.7(7) . . . . ? C39 C56 Ce4 C72 -114.0(10) . . . . ? C20 C56 Ce4 C72 132.7(9) . . . . ? C72 C56 Ce4 C32 -106.4(7) . . . . ? C39 C56 Ce4 C32 139.6(8) . . . . ? C20 C56 Ce4 C32 26.3(6) . . . . ? C72 C56 Ce4 C50 -7.0(6) . . . . ? C39 C56 Ce4 C50 -121.0(8) . . . . ? C20 C56 Ce4 C50 125.7(7) . . . . ? C72 C56 Ce4 C20 -132.7(9) . . . . ? C39 C56 Ce4 C20 113.3(9) . . . . ? C72 C56 Ce4 C71 -77.1(9) . . . . ? C39 C56 Ce4 C71 168.9(8) . . . . ? C20 C56 Ce4 C71 55.6(8) . . . . ? C72 C56 Ce4 C27 33.2(6) . . . . ? C39 C56 Ce4 C27 -80.8(7) . . . . ? C20 C56 Ce4 C27 165.9(8) . . . . ? C72 C56 Ce4 C77 21.5(6) . . . . ? C39 C56 Ce4 C77 -92.5(8) . . . . ? C20 C56 Ce4 C77 154.2(7) . . . . ? C72 C56 Ce4 C70 -15.0(8) . . . . ? C39 C56 Ce4 C70 -129.0(8) . . . . ? C20 C56 Ce4 C70 117.8(9) . . . . ? C72 C56 Ce4 C26 -49.9(10) . . . . ? C39 C56 Ce4 C26 -163.9(9) . . . . ? C20 C56 Ce4 C26 82.8(10) . . . . ? C77 C50 Ce4 C73 116.5(8) . . . . ? C70 C50 Ce4 C73 -124.0(8) . . . . ? C77 C50 Ce4 C18 151.9(7) . . . . ? C70 C50 Ce4 C18 -88.7(6) . . . . ? C73 C50 Ce4 C18 35.3(5) . . . . ? C77 C50 Ce4 C72 69.6(6) . . . . ? C70 C50 Ce4 C72 -171.0(7) . . . . ? C73 C50 Ce4 C72 -47.0(6) . . . . ? C77 C50 Ce4 C32 137.0(6) . . . . ? C70 C50 Ce4 C32 -103.6(7) . . . . ? C73 C50 Ce4 C32 20.4(6) . . . . ? C77 C50 Ce4 C56 74.2(7) . . . . ? C70 C50 Ce4 C56 -166.4(7) . . . . ? C73 C50 Ce4 C56 -42.3(6) . . . . ? C77 C50 Ce4 C20 103.6(7) . . . . ? C70 C50 Ce4 C20 -137.0(7) . . . . ? C73 C50 Ce4 C20 -12.9(6) . . . . ? C77 C50 Ce4 C71 -171.1(6) . . . . ? C70 C50 Ce4 C71 -51.7(6) . . . . ? C73 C50 Ce4 C71 72.4(6) . . . . ? C77 C50 Ce4 C27 32.0(5) . . . . ? C70 C50 Ce4 C27 151.4(7) . . . . ? C73 C50 Ce4 C27 -84.5(6) . . . . ? C70 C50 Ce4 C77 119.4(8) . . . . ? C73 C50 Ce4 C77 -116.5(8) . . . . ? C77 C50 Ce4 C70 -119.4(8) . . . . ? C73 C50 Ce4 C70 124.0(8) . . . . ? C77 C50 Ce4 C26 -143.7(6) . . . . ? C70 C50 Ce4 C26 -24.3(5) . . . . ? C73 C50 Ce4 C26 99.8(7) . . . . ? C3 C20 Ce4 C73 171.3(8) . . . . ? C32 C20 Ce4 C73 66.4(7) . . . . ? C56 C20 Ce4 C73 -69.1(7) . . . . ? C3 C20 Ce4 C18 130.0(8) . . . . ? C32 C20 Ce4 C18 25.1(6) . . . . ? C56 C20 Ce4 C18 -110.4(8) . . . . ? C3 C20 Ce4 C72 -147.9(8) . . . . ? C32 C20 Ce4 C72 107.3(7) . . . . ? C56 C20 Ce4 C72 -28.3(6) . . . . ? C3 C20 Ce4 C32 104.9(9) . . . . ? C56 C20 Ce4 C32 -135.5(9) . . . . ? C3 C20 Ce4 C56 -119.6(9) . . . . ? C32 C20 Ce4 C56 135.5(9) . . . . ? C3 C20 Ce4 C50 179.2(7) . . . . ? C32 C20 Ce4 C50 74.4(8) . . . . ? C56 C20 Ce4 C50 -61.2(8) . . . . ? C3 C20 Ce4 C71 109.2(8) . . . . ? C32 C20 Ce4 C71 4.3(6) . . . . ? C56 C20 Ce4 C71 -131.2(8) . . . . ? C3 C20 Ce4 C27 -131.3(7) . . . . ? C32 C20 Ce4 C27 123.8(7) . . . . ? C56 C20 Ce4 C27 -11.7(6) . . . . ? C3 C20 Ce4 C77 -148.4(8) . . . . ? C32 C20 Ce4 C77 106.7(8) . . . . ? C56 C20 Ce4 C77 -28.8(8) . . . . ? C3 C20 Ce4 C70 152.3(8) . . . . ? C32 C20 Ce4 C70 47.4(9) . . . . ? C56 C20 Ce4 C70 -88.1(9) . . . . ? C3 C20 Ce4 C26 118.3(8) . . . . ? C32 C20 Ce4 C26 13.4(8) . . . . ? C56 C20 Ce4 C26 -122.1(9) . . . . ? C26 C71 Ce4 C73 90.8(7) . . . . ? C5 C71 Ce4 C73 -152.7(7) . . . . ? C18 C71 Ce4 C73 -38.3(6) . . . . ? C26 C71 Ce4 C18 129.0(9) . . . . ? C5 C71 Ce4 C18 -114.4(9) . . . . ? C26 C71 Ce4 C72 101.3(7) . . . . ? C5 C71 Ce4 C72 -142.2(7) . . . . ? C18 C71 Ce4 C72 -27.8(7) . . . . ? C26 C71 Ce4 C32 166.4(7) . . . . ? C5 C71 Ce4 C32 -77.0(7) . . . . ? C18 C71 Ce4 C32 37.4(6) . . . . ? C26 C71 Ce4 C56 136.1(8) . . . . ? C5 C71 Ce4 C56 -107.4(8) . . . . ? C18 C71 Ce4 C56 7.0(8) . . . . ? C26 C71 Ce4 C50 51.0(5) . . . . ? C5 C71 Ce4 C50 167.6(6) . . . . ? C18 C71 Ce4 C50 -78.0(7) . . . . ? C26 C71 Ce4 C20 163.6(7) . . . . ? C5 C71 Ce4 C20 -79.8(7) . . . . ? C18 C71 Ce4 C20 34.6(7) . . . . ? C26 C71 Ce4 C27 72.2(7) . . . . ? C5 C71 Ce4 C27 -171.3(7) . . . . ? C18 C71 Ce4 C27 -56.9(8) . . . . ? C26 C71 Ce4 C77 46.6(6) . . . . ? C5 C71 Ce4 C77 163.1(6) . . . . ? C18 C71 Ce4 C77 -82.5(7) . . . . ? C26 C71 Ce4 C70 22.5(5) . . . . ? C5 C71 Ce4 C70 139.0(7) . . . . ? C18 C71 Ce4 C70 -106.6(7) . . . . ? C5 C71 Ce4 C26 116.6(8) . . . . ? C18 C71 Ce4 C26 -129.0(9) . . . . ? C72 C27 Ce4 C73 45.2(6) . . . . ? C65 C27 Ce4 C73 165.5(8) . . . . ? C77 C27 Ce4 C73 -75.3(7) . . . . ? C72 C27 Ce4 C18 36.1(7) . . . . ? C65 C27 Ce4 C18 156.5(7) . . . . ? C77 C27 Ce4 C18 -84.3(7) . . . . ? C65 C27 Ce4 C72 120.3(9) . . . . ? C77 C27 Ce4 C72 -120.5(9) . . . . ? C72 C27 Ce4 C32 0.7(7) . . . . ? C65 C27 Ce4 C32 121.0(8) . . . . ? C77 C27 Ce4 C32 -119.8(8) . . . . ? C72 C27 Ce4 C56 -36.6(6) . . . . ? C65 C27 Ce4 C56 83.7(7) . . . . ? C77 C27 Ce4 C56 -157.1(8) . . . . ? C72 C27 Ce4 C50 89.9(7) . . . . ? C65 C27 Ce4 C50 -149.8(7) . . . . ? C77 C27 Ce4 C50 -30.6(5) . . . . ? C72 C27 Ce4 C20 -28.7(7) . . . . ? C65 C27 Ce4 C20 91.6(7) . . . . ? C77 C27 Ce4 C20 -149.2(7) . . . . ? C72 C27 Ce4 C71 64.8(8) . . . . ? C65 C27 Ce4 C71 -174.9(7) . . . . ? C77 C27 Ce4 C71 -55.7(8) . . . . ? C72 C27 Ce4 C77 120.5(9) . . . . ? C65 C27 Ce4 C77 -119.2(9) . . . . ? C72 C27 Ce4 C70 103.8(7) . . . . ? C65 C27 Ce4 C70 -135.9(6) . . . . ? C77 C27 Ce4 C70 -16.7(6) . . . . ? C72 C27 Ce4 C26 93.6(8) . . . . ? C65 C27 Ce4 C26 -146.1(7) . . . . ? C77 C27 Ce4 C26 -26.9(7) . . . . ? C50 C77 Ce4 C73 -40.6(6) . . . . ? C46 C77 Ce4 C73 -159.0(7) . . . . ? C27 C77 Ce4 C73 84.1(7) . . . . ? C50 C77 Ce4 C18 -25.8(6) . . . . ? C46 C77 Ce4 C18 -144.2(6) . . . . ? C27 C77 Ce4 C18 98.8(7) . . . . ? C50 C77 Ce4 C72 -90.5(7) . . . . ? C46 C77 Ce4 C72 151.1(7) . . . . ? C27 C77 Ce4 C72 34.1(6) . . . . ? C50 C77 Ce4 C32 -51.3(8) . . . . ? C46 C77 Ce4 C32 -169.7(7) . . . . ? C27 C77 Ce4 C32 73.4(8) . . . . ? C50 C77 Ce4 C56 -105.6(7) . . . . ? C46 C77 Ce4 C56 136.0(7) . . . . ? C27 C77 Ce4 C56 19.0(6) . . . . ? C46 C77 Ce4 C50 -118.4(8) . . . . ? C27 C77 Ce4 C50 124.6(9) . . . . ? C50 C77 Ce4 C20 -89.9(8) . . . . ? C46 C77 Ce4 C20 151.7(7) . . . . ? C27 C77 Ce4 C20 34.7(8) . . . . ? C50 C77 Ce4 C71 8.5(6) . . . . ? C46 C77 Ce4 C71 -109.9(7) . . . . ? C27 C77 Ce4 C71 133.1(7) . . . . ? C50 C77 Ce4 C27 -124.6(9) . . . . ? C46 C77 Ce4 C27 117.0(9) . . . . ? C50 C77 Ce4 C70 34.0(5) . . . . ? C46 C77 Ce4 C70 -84.4(6) . . . . ? C27 C77 Ce4 C70 158.6(7) . . . . ? C50 C77 Ce4 C26 29.4(5) . . . . ? C46 C77 Ce4 C26 -89.0(6) . . . . ? C27 C77 Ce4 C26 154.0(7) . . . . ? C24 C70 Ce4 C73 150.9(7) . . . . ? C50 C70 Ce4 C73 35.9(6) . . . . ? C26 C70 Ce4 C73 -100.9(7) . . . . ? C24 C70 Ce4 C18 -165.8(7) . . . . ? C50 C70 Ce4 C18 79.3(7) . . . . ? C26 C70 Ce4 C18 -57.6(6) . . . . ? C24 C70 Ce4 C72 122.6(7) . . . . ? C50 C70 Ce4 C72 7.7(6) . . . . ? C26 C70 Ce4 C72 -129.2(7) . . . . ? C24 C70 Ce4 C32 -161.9(6) . . . . ? C50 C70 Ce4 C32 83.1(7) . . . . ? C26 C70 Ce4 C32 -53.7(6) . . . . ? C24 C70 Ce4 C56 131.1(8) . . . . ? C50 C70 Ce4 C56 16.2(8) . . . . ? C26 C70 Ce4 C56 -120.7(8) . . . . ? C24 C70 Ce4 C50 114.9(8) . . . . ? C26 C70 Ce4 C50 -136.9(8) . . . . ? C24 C70 Ce4 C20 172.6(8) . . . . ? C50 C70 Ce4 C20 57.7(9) . . . . ? C26 C70 Ce4 C20 -79.1(9) . . . . ? C24 C70 Ce4 C71 -130.3(7) . . . . ? C50 C70 Ce4 C71 114.7(7) . . . . ? C26 C70 Ce4 C71 -22.1(5) . . . . ? C24 C70 Ce4 C27 92.1(6) . . . . ? C50 C70 Ce4 C27 -22.9(6) . . . . ? C26 C70 Ce4 C27 -159.7(6) . . . . ? C24 C70 Ce4 C77 81.0(6) . . . . ? C50 C70 Ce4 C77 -33.9(5) . . . . ? C26 C70 Ce4 C77 -170.7(6) . . . . ? C24 C70 Ce4 C26 -108.2(7) . . . . ? C50 C70 Ce4 C26 136.9(8) . . . . ? C71 C26 Ce4 C73 -76.1(7) . . . . ? C29 C26 Ce4 C73 165.9(7) . . . . ? C70 C26 Ce4 C73 64.5(6) . . . . ? C71 C26 Ce4 C18 -31.8(6) . . . . ? C29 C26 Ce4 C18 -149.9(7) . . . . ? C70 C26 Ce4 C18 108.7(7) . . . . ? C71 C26 Ce4 C72 -86.5(7) . . . . ? C29 C26 Ce4 C72 155.4(7) . . . . ? C70 C26 Ce4 C72 54.1(7) . . . . ? C71 C26 Ce4 C32 -11.6(6) . . . . ? C29 C26 Ce4 C32 -129.7(7) . . . . ? C70 C26 Ce4 C32 128.9(6) . . . . ? C71 C26 Ce4 C56 -59.4(10) . . . . ? C29 C26 Ce4 C56 -177.4(9) . . . . ? C70 C26 Ce4 C56 81.2(10) . . . . ? C71 C26 Ce4 C50 -116.0(7) . . . . ? C29 C26 Ce4 C50 126.0(7) . . . . ? C70 C26 Ce4 C50 24.6(5) . . . . ? C71 C26 Ce4 C20 -19.1(8) . . . . ? C29 C26 Ce4 C20 -137.2(8) . . . . ? C70 C26 Ce4 C20 121.4(8) . . . . ? C29 C26 Ce4 C71 -118.1(8) . . . . ? C70 C26 Ce4 C71 140.6(8) . . . . ? C71 C26 Ce4 C27 -119.6(7) . . . . ? C29 C26 Ce4 C27 122.3(7) . . . . ? C70 C26 Ce4 C27 21.0(6) . . . . ? C71 C26 Ce4 C77 -133.3(6) . . . . ? C29 C26 Ce4 C77 108.6(6) . . . . ? C70 C26 Ce4 C77 7.3(5) . . . . ? C71 C26 Ce4 C70 -140.6(8) . . . . ? C29 C26 Ce4 C70 101.4(8) . . . . ? _diffrn_measured_fraction_theta_max 0.752 _diffrn_reflns_theta_full 24.51 _diffrn_measured_fraction_theta_full 0.752 _refine_diff_density_max 0.749 _refine_diff_density_min -0.885 _refine_diff_density_rms 0.115 # Attachment 'Ce2@C78Si270krev2.cif' data_Ce2@C78Si270krev2 _database_code_depnum_ccdc_archive 'CCDC 661491' _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C117.50 H46 Ce2 S5 Si2' _chemical_formula_weight 1954.26 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M P212121 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' _cell_length_a 11.351(3) _cell_length_b 23.560(6) _cell_length_c 28.117(7) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 7519(3) _cell_formula_units_Z 4 _cell_measurement_temperature 270(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description platelet _exptl_crystal_colour black _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.01 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.727 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 3900 _exptl_absorpt_coefficient_mu 1.429 _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min 0.8142 _exptl_absorpt_correction_T_max 0.9858 _exptl_absorpt_process_details 'SADABS Sheldrick 1996' _exptl_special_details ; ? ; _diffrn_ambient_temperature 270(2) _diffrn_radiation_wavelength 0.68880 _diffrn_radiation_type synchrotron _diffrn_radiation_source synchrotron _diffrn_radiation_source_type 'KEK BL1B' _diffrn_radiation_monochromator Si(111) _diffrn_measurement_device_type IPDSC _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 34267 _diffrn_reflns_av_R_equivalents 0.0406 _diffrn_reflns_av_sigmaI/netI 0.0366 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_theta_min 1.40 _diffrn_reflns_theta_max 24.52 _reflns_number_total 10346 _reflns_number_gt 8500 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'Bruker SMART' _computing_cell_refinement 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The 977 restraints were used in the refinements. All atoms were refined with SIMU to generate similar Uij restraints automatically using connectivity. S5, C118, and S6 were refined with ISOR so that their Uij components approximate to isotropic behavior. S5, C118, and S6 were also refined with DELU to generate rigid bond Uij restraints automatically using connectivity. S5, C118, and S6 were also refined with DANG to restrain the 1,3-distance S5...S6. ; _chemical_absolute_configuration unk _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.328(15) _refine_ls_number_reflns 10346 _refine_ls_number_parameters 1186 _refine_ls_number_restraints 977 _refine_ls_R_factor_all 0.0587 _refine_ls_R_factor_gt 0.0475 _refine_ls_wR_factor_ref 0.1357 _refine_ls_wR_factor_gt 0.1294 _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_restrained_S_all 1.064 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ce1 Ce 0.51219(4) 0.59654(2) 0.101971(15) 0.05833(16) Uani 0.9553(15) 1 d P A 2 Ce2 Ce 0.86512(5) 0.60774(2) 0.113885(15) 0.05992(17) Uani 0.9553(15) 1 d P A 2 Si1 Si 0.5689(2) 0.74711(10) 0.28462(7) 0.0570(6) Uani 1 1 d . . . Si2 Si 0.7044(3) 0.62277(11) 0.32692(7) 0.0643(7) Uani 1 1 d . . . C79 C 0.7917(12) 0.4987(5) 0.3509(3) 0.095(3) Uani 1 1 d U . . H1 H 0.8313 0.5164 0.3772 0.143 Uiso 1 1 calc R . . H2 H 0.8190 0.5151 0.3217 0.143 Uiso 1 1 calc R . . H3 H 0.8081 0.4588 0.3510 0.143 Uiso 1 1 calc R . . C1 C 0.3855(8) 0.6662(4) 0.1615(3) 0.0611(15) Uani 1 1 d U . . C2 C 0.9572(8) 0.6007(4) 0.2042(3) 0.0641(15) Uani 1 1 d U . . C3 C 0.9727(9) 0.6397(4) 0.0244(3) 0.0727(16) Uani 1 1 d U . . C4 C 0.6011(7) 0.6023(4) 0.2422(2) 0.0567(14) Uani 1 1 d U A . C5 C 0.9358(8) 0.6929(4) 0.1753(3) 0.0633(15) Uani 1 1 d U . . C6 C 0.9503(9) 0.4892(4) 0.0941(3) 0.0717(16) Uani 1 1 d U . . C7 C 0.7852(9) 0.5525(4) 0.2389(3) 0.0604(15) Uani 1 1 d U . . C8 C 0.4811(9) 0.5289(4) 0.2008(3) 0.0620(15) Uani 1 1 d U . . C9 C 0.8868(9) 0.5491(4) 0.2138(3) 0.0646(15) Uani 1 1 d U A . C80 C 0.4140(11) 0.6153(4) 0.3431(3) 0.090(3) Uani 1 1 d U . . H4 H 0.3321 0.6057 0.3402 0.135 Uiso 1 1 calc R . . H5 H 0.4405 0.6331 0.3143 0.135 Uiso 1 1 calc R . . H6 H 0.4243 0.6410 0.3693 0.135 Uiso 1 1 calc R . . C10 C 0.6869(9) 0.5148(4) 0.2295(3) 0.0637(15) Uani 1 1 d U A . C81 C 0.5848(8) 0.8618(4) 0.2483(3) 0.0598(16) Uani 1 1 d U . . C11 C 0.9915(10) 0.5292(4) 0.0590(3) 0.0755(16) Uani 1 1 d U A . C12 C 1.0323(9) 0.6630(4) 0.1484(3) 0.0703(16) Uani 1 1 d U A . C13 C 0.4233(9) 0.6144(4) 0.0104(3) 0.0705(16) Uani 1 1 d U . . C82 C 0.6608(12) 0.5080(5) 0.3555(3) 0.088(2) Uani 1 1 d U . . C14 C 1.0386(8) 0.6062(4) 0.1669(3) 0.0688(16) Uani 1 1 d U A . C15 C 0.5000(10) 0.4821(4) 0.1683(3) 0.0656(15) Uani 1 1 d U A . C16 C 0.3502(10) 0.5373(4) 0.0629(3) 0.0733(16) Uani 1 1 d U . . C17 C 0.7317(7) 0.6099(4) 0.2585(2) 0.0562(14) Uani 1 1 d U A . C18 C 0.8664(9) 0.7472(4) 0.1060(3) 0.0671(15) Uani 1 1 d U . . C83 C 0.9946(14) 0.6487(5) 0.4465(3) 0.097(2) Uani 1 1 d U . . C19 C 0.7817(8) 0.6591(4) 0.2322(3) 0.0546(14) Uani 1 1 d U . . C20 C 0.9181(9) 0.6932(4) 0.0316(3) 0.0722(16) Uani 1 1 d U A . C84 C 0.3109(10) 0.7500(4) 0.3036(3) 0.0693(18) Uani 1 1 d U . . C21 C 0.7903(10) 0.4586(4) 0.0412(3) 0.0734(16) Uani 1 1 d U . . C22 C 0.3437(9) 0.5261(4) 0.1139(3) 0.0718(16) Uani 1 1 d U A . C23 C 0.3977(8) 0.6881(4) 0.0632(3) 0.0664(16) Uani 1 1 d U . . C24 C 0.5446(7) 0.7359(4) 0.1763(3) 0.0540(14) Uani 1 1 d U . . C25 C 0.8146(9) 0.6125(4) -0.0255(3) 0.0730(16) Uani 1 1 d U . . C26 C 0.7520(8) 0.7408(4) 0.1802(3) 0.0551(14) Uani 1 1 d U . . C27 C 0.6095(9) 0.7399(4) 0.0310(3) 0.0669(16) Uani 1 1 d U . . C28 C 0.5785(7) 0.7054(3) 0.2233(2) 0.0513(14) Uani 1 1 d U A . C29 C 0.7132(7) 0.7034(3) 0.2174(2) 0.0516(14) Uani 1 1 d U A . C85 C 0.7691(8) 0.8306(4) 0.2832(3) 0.0647(17) Uani 1 1 d U . . C86 C 0.4562(8) 0.8536(4) 0.2356(3) 0.070(2) Uani 1 1 d U . . H7 H 0.4113 0.8475 0.2641 0.104 Uiso 1 1 calc R . . H8 H 0.4483 0.8212 0.2151 0.104 Uiso 1 1 calc R . . H9 H 0.4275 0.8868 0.2196 0.104 Uiso 1 1 calc R . . C30 C 0.4512(8) 0.7157(4) 0.1471(3) 0.0600(15) Uani 1 1 d U A . C31 C 0.8955(8) 0.6531(4) 0.2106(3) 0.0591(15) Uani 1 1 d U A . C32 C 0.9485(9) 0.7153(4) 0.0789(3) 0.0699(16) Uani 1 1 d U A . C33 C 0.4006(8) 0.5731(4) 0.1880(3) 0.0607(15) Uani 1 1 d U A . C34 C 0.3244(8) 0.6440(4) 0.0780(3) 0.0697(16) Uani 1 1 d U A . C35 C 0.4874(10) 0.4667(4) 0.0810(3) 0.0715(16) Uani 1 1 d U . . C87 C 0.4223(9) 0.7633(4) 0.3175(3) 0.0645(17) Uani 1 1 d U . . C88 C 0.6473(8) 0.8173(4) 0.2718(3) 0.0596(16) Uani 1 1 d U . . C36 C 0.3402(8) 0.5934(4) 0.0460(3) 0.0697(16) Uani 1 1 d U A . C37 C 0.6333(10) 0.6608(4) -0.0244(3) 0.0693(15) Uani 1 1 d U . . C38 C 0.6699(9) 0.4519(4) 0.0386(3) 0.0719(16) Uani 1 1 d U A . C89 C 0.8743(12) 0.6500(4) 0.4550(3) 0.092(2) Uani 1 1 d U . . H10 H 0.8487 0.6586 0.4856 0.110 Uiso 1 1 calc R . . C39 C 0.7558(9) 0.6673(4) -0.0213(3) 0.0704(16) Uani 1 1 d U A . C40 C 0.5973(9) 0.4419(4) 0.0792(3) 0.0715(16) Uani 1 1 d U A . C41 C 0.4396(9) 0.5020(4) 0.0446(3) 0.0733(16) Uani 1 1 d U A . C90 C 0.3414(10) 0.7974(4) 0.3913(3) 0.0768(19) Uani 1 1 d U . . H11 H 0.3534 0.8117 0.4217 0.092 Uiso 1 1 calc R . . C91 C 0.5546(10) 0.8134(5) 0.3811(3) 0.084(3) Uani 1 1 d U . . H47 H 0.6039 0.7821 0.3901 0.126 Uiso 1 1 calc R . . H48 H 0.5403 0.8370 0.4083 0.126 Uiso 1 1 calc R . . H49 H 0.5931 0.8352 0.3568 0.126 Uiso 1 1 calc R . . C42 C 0.9838(9) 0.5095(4) 0.1402(3) 0.0718(16) Uani 1 1 d U A . C43 C 0.3296(8) 0.5728(4) 0.1466(3) 0.0673(16) Uani 1 1 d U . . C44 C 0.9053(9) 0.5025(4) 0.1799(3) 0.0685(16) Uani 1 1 d U . . C45 C 0.6084(8) 0.6031(4) -0.0316(2) 0.0682(15) Uani 1 1 d U A . C46 C 0.4574(8) 0.7262(4) 0.0952(3) 0.0653(15) Uani 1 1 d U A . C47 C 0.9240(9) 0.5392(4) 0.0166(3) 0.0719(16) Uani 1 1 d U . . C48 C 0.9131(9) 0.5955(5) -0.0010(3) 0.0721(16) Uani 1 1 d U A . C49 C 0.8108(10) 0.4644(4) 0.1734(3) 0.0697(16) Uani 1 1 d U A . C50 C 0.6514(8) 0.7719(4) 0.1068(3) 0.0635(15) Uani 1 1 d U . . C51 C 0.8313(9) 0.5004(4) 0.0081(3) 0.0722(16) Uani 1 1 d U A . C52 C 0.5065(9) 0.5769(4) -0.0120(3) 0.0689(15) Uani 1 1 d U A . C53 C 0.5159(10) 0.5179(4) 0.0044(3) 0.0711(16) Uani 1 1 d U . . C92 C 0.6363(9) 0.9131(4) 0.2400(3) 0.0637(16) Uani 1 1 d U . . H15 H 0.5921 0.9414 0.2255 0.076 Uiso 1 1 calc R . . C54 C 0.5776(9) 0.5436(4) 0.2304(3) 0.0600(15) Uani 1 1 d U A . C55 C 1.0503(9) 0.6296(5) 0.0668(3) 0.0756(17) Uani 1 1 d U A . C56 C 0.8077(9) 0.7106(4) 0.0104(3) 0.0713(16) Uani 1 1 d U . . C93 C 0.8581(11) 0.7861(5) 0.3056(4) 0.088(3) Uani 1 1 d U . . H16 H 0.9350 0.8029 0.3078 0.132 Uiso 1 1 calc R . . H17 H 0.8618 0.7530 0.2857 0.132 Uiso 1 1 calc R . . H18 H 0.8314 0.7755 0.3367 0.132 Uiso 1 1 calc R . . C57 C 1.0355(9) 0.6755(4) 0.0982(3) 0.0743(16) Uani 1 1 d U . . C94 C 0.7515(9) 0.9246(4) 0.2523(3) 0.0681(17) Uani 1 1 d U . . C58 C 0.5328(7) 0.6466(4) 0.2250(2) 0.0544(14) Uani 1 1 d U . . C59 C 0.6236(10) 0.4909(4) 0.0021(3) 0.0705(16) Uani 1 1 d U A . C95 C 0.6417(10) 0.6960(4) 0.3280(2) 0.071(3) Uani 1 1 d . . . H19 H 0.7063 0.7183 0.3406 0.085 Uiso 1 1 calc R . . H20 H 0.5848 0.6939 0.3536 0.085 Uiso 1 1 calc R . . C60 C 0.8500(10) 0.4549(4) 0.0865(3) 0.0708(16) Uani 1 1 d U A . C61 C 0.4518(9) 0.6731(4) 0.0204(3) 0.0679(16) Uani 1 1 d U A . C62 C 0.4354(8) 0.6306(4) 0.1972(3) 0.0586(15) Uani 1 1 d U A . C63 C 0.4279(9) 0.4843(4) 0.1241(3) 0.0701(16) Uani 1 1 d U A . C64 C 1.0526(9) 0.5599(5) 0.1331(3) 0.0731(17) Uani 1 1 d U . . C96 C 0.6062(12) 0.5617(4) 0.3459(3) 0.082(2) Uani 1 1 d U . . C65 C 0.5591(9) 0.6967(4) 0.0036(3) 0.0672(15) Uani 1 1 d U A . C97 C 0.4376(10) 0.7909(4) 0.3621(3) 0.0709(18) Uani 1 1 d U . . C98 C 0.2829(10) 0.7223(4) 0.2554(3) 0.081(3) Uani 1 1 d U . . H21 H 0.3152 0.7451 0.2302 0.122 Uiso 1 1 calc R . . H22 H 0.1990 0.7196 0.2515 0.122 Uiso 1 1 calc R . . H23 H 0.3169 0.6850 0.2543 0.122 Uiso 1 1 calc R . . C99 C 0.4810(12) 0.5649(4) 0.3515(3) 0.084(2) Uani 1 1 d U . . C66 C 0.7283(10) 0.5183(4) -0.0177(3) 0.0710(16) Uani 1 1 d U . . C67 C 0.7179(9) 0.5740(4) -0.0343(3) 0.0696(16) Uani 1 1 d U A . C68 C 0.6080(9) 0.4522(4) 0.1675(3) 0.0685(16) Uani 1 1 d U . . C100 C 0.7904(11) 0.6394(5) 0.4206(3) 0.086(2) Uani 1 1 d U . . C69 C 0.7034(10) 0.4697(4) 0.1977(3) 0.0683(16) Uani 1 1 d U A . C70 C 0.6456(8) 0.7604(4) 0.1562(3) 0.0566(14) Uani 1 1 d U A . C101 C 0.1254(12) 0.7957(5) 0.4101(4) 0.103(3) Uani 1 1 d U . . H24 H 0.1374 0.7769 0.4401 0.155 Uiso 1 1 calc R . . H25 H 0.0544 0.7818 0.3957 0.155 Uiso 1 1 calc R . . H26 H 0.1187 0.8358 0.4152 0.155 Uiso 1 1 calc R . . C102 C 1.0290(12) 0.6392(5) 0.3992(3) 0.098(2) Uani 1 1 d U . . H27 H 1.1089 0.6388 0.3919 0.117 Uiso 1 1 calc R . . C103 C 0.9502(11) 0.6308(5) 0.3642(3) 0.092(2) Uani 1 1 d U . . C104 C 0.4812(14) 0.4678(5) 0.3771(4) 0.102(2) Uani 1 1 d U . . C105 C 0.2145(10) 0.7596(4) 0.3345(3) 0.0742(19) Uani 1 1 d U . . H28 H 0.1394 0.7491 0.3247 0.089 Uiso 1 1 calc R . . C71 C 0.8601(9) 0.7344(4) 0.1563(3) 0.0623(15) Uani 1 1 d U A . C72 C 0.7327(9) 0.7475(4) 0.0346(3) 0.0681(16) Uani 1 1 d U A . C106 C 0.8111(9) 0.8830(4) 0.2740(3) 0.0690(18) Uani 1 1 d U . . H29 H 0.8878 0.8908 0.2835 0.083 Uiso 1 1 calc R . . C107 C 1.0042(11) 0.6186(5) 0.3146(3) 0.101(3) Uani 1 1 d U . . H30 H 1.0081 0.6532 0.2967 0.151 Uiso 1 1 calc R . . H31 H 0.9558 0.5916 0.2980 0.151 Uiso 1 1 calc R . . H32 H 1.0820 0.6033 0.3184 0.151 Uiso 1 1 calc R . . C73 C 0.7649(9) 0.7648(4) 0.0822(3) 0.0674(16) Uani 1 1 d U A . C74 C 0.3163(9) 0.6298(4) 0.1306(3) 0.0678(16) Uani 1 1 d U A . C108 C 0.2285(10) 0.7838(4) 0.3778(3) 0.0795(19) Uani 1 1 d U . . C109 C 0.5988(13) 0.4619(5) 0.3701(3) 0.096(2) Uani 1 1 d U . . H33 H 0.6359 0.4273 0.3752 0.116 Uiso 1 1 calc R . . C110 C 0.4224(13) 0.5185(5) 0.3669(3) 0.096(2) Uani 1 1 d U . . H34 H 0.3411 0.5203 0.3708 0.115 Uiso 1 1 calc R . . C111 C 0.8265(11) 0.6302(5) 0.3731(3) 0.086(2) Uani 1 1 d U . . C75 C 1.0572(9) 0.5725(5) 0.0835(3) 0.0752(17) Uani 1 1 d U A . C76 C 0.6551(10) 0.4340(4) 0.1236(3) 0.0703(16) Uani 1 1 d U A . C112 C 0.7984(11) 0.9825(5) 0.2422(4) 0.092(3) Uani 1 1 d U . . H35 H 0.7814 1.0072 0.2685 0.138 Uiso 1 1 calc R . . H36 H 0.7618 0.9972 0.2140 0.138 Uiso 1 1 calc R . . H37 H 0.8821 0.9805 0.2376 0.138 Uiso 1 1 calc R . . C77 C 0.5594(9) 0.7560(4) 0.0777(3) 0.0660(16) Uani 1 1 d U A . C78 C 0.7824(10) 0.4386(4) 0.1273(3) 0.0711(16) Uani 1 1 d U . . C113 C 0.6681(12) 0.6388(5) 0.4379(3) 0.099(3) Uani 1 1 d U . . H38 H 0.6551 0.6052 0.4565 0.148 Uiso 1 1 calc R . . H39 H 0.6151 0.6392 0.4113 0.148 Uiso 1 1 calc R . . H40 H 0.6544 0.6718 0.4573 0.148 Uiso 1 1 calc R . . C114 C 1.0964(14) 0.6564(6) 0.4820(4) 0.123(4) Uani 1 1 d U . . H41 H 1.1042 0.6229 0.5011 0.185 Uiso 1 1 calc R . . H42 H 1.0804 0.6884 0.5021 0.185 Uiso 1 1 calc R . . H43 H 1.1684 0.6629 0.4649 0.185 Uiso 1 1 calc R . . C115 C 0.3999(15) 0.4160(6) 0.3943(5) 0.140(4) Uani 1 1 d U . . H44 H 0.4091 0.3846 0.3728 0.210 Uiso 1 1 calc R . . H45 H 0.3189 0.4278 0.3946 0.210 Uiso 1 1 calc R . . H46 H 0.4229 0.4046 0.4257 0.210 Uiso 1 1 calc R . . S1 S 0.6922(6) 0.6924(2) -0.14069(17) 0.1696(19) Uani 1 1 d U B 1 S3 S 0.3152(6) 0.6070(3) 0.5860(3) 0.233(3) Uani 1 1 d U C 1 S2 S 0.6219(8) 0.6382(3) -0.2325(3) 0.232(3) Uani 1 1 d U B 1 S4 S 0.3785(10) 0.5763(5) 0.4874(4) 0.311(4) Uani 1 1 d U C 1 C117 C 0.354(2) 0.6031(14) 0.5348(12) 0.258(5) Uani 1 1 d U C 1 Ce3 Ce 0.621(2) 0.5295(7) 0.1265(5) 0.109(7) Uani 0.0447(15) 1 d P A 3 Ce4 Ce 0.7490(14) 0.6808(6) 0.0904(5) 0.086(5) Uani 0.0447(15) 1 d P A 3 S5 S 1.124(2) 0.4952(8) 0.3946(7) 0.287(6) Uani 0.50 1 d PDU . . S6 S 1.0620(18) 0.3839(9) 0.3532(7) 0.282(6) Uani 0.50 1 d PDU . . C118 C 1.127(4) 0.4341(13) 0.375(2) 0.285(6) Uani 0.50 1 d PDU . . C116 C 0.630(2) 0.6643(9) -0.1804(7) 0.187(4) Uani 1 1 d U . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ce1 0.0571(3) 0.0579(4) 0.0599(2) -0.0002(2) 0.00019(18) -0.0031(2) Ce2 0.0545(3) 0.0609(4) 0.0644(3) -0.0013(2) 0.00546(19) 0.0023(2) Si1 0.0740(16) 0.0457(17) 0.0514(11) -0.0036(9) 0.0005(9) 0.0092(12) Si2 0.0932(19) 0.0532(19) 0.0465(11) 0.0022(9) 0.0003(10) 0.0131(13) C79 0.158(8) 0.064(7) 0.063(5) 0.006(4) -0.016(5) 0.030(6) C1 0.064(3) 0.057(3) 0.062(3) -0.005(3) 0.007(2) 0.006(3) C2 0.072(3) 0.060(3) 0.060(3) 0.000(3) -0.009(2) 0.014(3) C3 0.076(3) 0.074(4) 0.069(3) 0.006(3) 0.021(3) -0.005(3) C4 0.074(3) 0.047(3) 0.049(2) 0.004(2) 0.010(2) 0.002(3) C5 0.067(3) 0.058(3) 0.065(3) -0.006(3) -0.003(3) -0.010(3) C6 0.083(3) 0.058(3) 0.074(3) -0.006(3) 0.009(3) 0.024(3) C7 0.085(3) 0.047(3) 0.050(3) 0.005(3) 0.001(2) 0.015(3) C8 0.076(3) 0.049(3) 0.061(3) 0.004(2) 0.014(3) -0.013(3) C9 0.079(3) 0.054(3) 0.060(3) 0.001(3) -0.006(3) 0.019(3) C80 0.128(8) 0.060(7) 0.081(5) 0.015(5) 0.015(5) -0.009(6) C10 0.095(3) 0.045(3) 0.051(3) 0.010(2) 0.005(3) 0.009(3) C81 0.069(4) 0.044(4) 0.066(3) -0.007(3) 0.001(3) 0.006(3) C11 0.082(3) 0.069(4) 0.075(3) -0.008(3) 0.016(3) 0.015(3) C12 0.069(3) 0.068(4) 0.074(3) -0.010(3) 0.003(3) -0.009(3) C13 0.081(3) 0.069(4) 0.061(3) -0.004(3) -0.017(3) 0.005(3) C82 0.151(5) 0.059(5) 0.054(3) 0.005(3) -0.018(4) -0.006(4) C14 0.068(3) 0.067(4) 0.071(3) -0.007(3) -0.001(2) 0.009(3) C15 0.085(3) 0.045(3) 0.066(3) 0.003(2) 0.008(3) -0.015(3) C16 0.081(3) 0.062(4) 0.077(3) -0.010(3) -0.005(3) -0.009(3) C17 0.075(3) 0.046(3) 0.048(2) 0.001(2) 0.002(2) 0.009(3) C18 0.076(3) 0.056(3) 0.070(3) 0.008(3) 0.005(3) -0.019(3) C83 0.136(5) 0.093(4) 0.063(3) 0.001(3) -0.026(4) 0.012(4) C19 0.068(3) 0.046(3) 0.050(3) -0.006(2) -0.003(2) 0.005(3) C20 0.080(3) 0.069(4) 0.068(3) 0.013(3) 0.019(3) -0.015(3) C84 0.091(4) 0.052(4) 0.065(3) -0.002(3) 0.014(3) 0.003(3) C21 0.097(3) 0.057(3) 0.066(3) -0.015(3) 0.008(3) 0.012(3) C22 0.077(3) 0.058(4) 0.080(3) -0.006(3) 0.005(3) -0.018(3) C23 0.073(3) 0.059(4) 0.067(3) 0.001(3) -0.013(3) 0.011(3) C24 0.067(3) 0.040(3) 0.056(3) -0.001(2) 0.002(2) 0.014(3) C25 0.095(3) 0.069(4) 0.055(3) 0.004(3) 0.017(3) -0.001(3) C26 0.067(3) 0.040(3) 0.058(3) 0.000(2) -0.002(2) -0.001(3) C27 0.088(3) 0.054(3) 0.059(3) 0.017(3) 0.001(3) 0.010(3) C28 0.062(3) 0.042(3) 0.050(2) -0.002(2) 0.001(2) 0.011(3) C29 0.066(3) 0.039(3) 0.050(3) -0.005(2) 0.001(2) 0.005(3) C85 0.073(4) 0.052(4) 0.069(3) -0.008(3) -0.004(3) 0.005(3) C86 0.079(6) 0.048(6) 0.082(5) 0.001(4) -0.007(4) 0.011(4) C30 0.069(3) 0.050(3) 0.061(3) 0.000(3) 0.001(2) 0.012(3) C31 0.069(3) 0.054(3) 0.055(3) -0.008(3) -0.007(2) 0.000(3) C32 0.073(3) 0.062(3) 0.074(3) 0.009(3) 0.014(3) -0.024(3) C33 0.069(3) 0.051(3) 0.062(3) -0.003(3) 0.017(2) -0.010(3) C34 0.068(3) 0.065(4) 0.076(3) -0.007(3) -0.013(3) 0.007(3) C35 0.091(3) 0.051(3) 0.072(3) -0.012(3) 0.000(3) -0.016(3) C87 0.086(4) 0.049(4) 0.058(3) 0.001(3) 0.011(3) 0.007(3) C88 0.068(4) 0.048(4) 0.063(3) -0.008(3) 0.001(3) 0.005(3) C36 0.072(3) 0.065(4) 0.071(3) -0.010(3) -0.013(3) 0.001(3) C37 0.094(3) 0.065(3) 0.049(3) 0.012(3) -0.002(3) 0.002(3) C38 0.094(3) 0.055(3) 0.067(3) -0.016(3) 0.005(3) 0.003(3) C89 0.138(5) 0.080(4) 0.056(3) 0.002(3) -0.014(4) 0.011(4) C39 0.094(3) 0.067(4) 0.051(3) 0.011(3) 0.013(3) -0.002(3) C40 0.095(4) 0.048(3) 0.071(3) -0.012(3) 0.002(3) -0.005(3) C41 0.088(3) 0.060(4) 0.073(3) -0.014(3) -0.007(3) -0.012(3) C90 0.105(5) 0.058(4) 0.068(3) -0.003(3) 0.014(3) 0.010(4) C91 0.115(7) 0.071(6) 0.066(5) -0.011(4) 0.004(5) 0.024(5) C42 0.083(3) 0.059(4) 0.073(3) -0.002(3) 0.004(3) 0.025(3) C43 0.069(3) 0.059(4) 0.074(3) -0.004(3) 0.009(3) -0.009(3) C44 0.086(3) 0.052(3) 0.067(3) 0.002(3) -0.001(3) 0.024(3) C45 0.092(3) 0.066(3) 0.047(2) 0.002(3) -0.007(2) -0.004(3) C46 0.077(3) 0.055(3) 0.064(3) 0.003(3) -0.007(3) 0.015(3) C47 0.086(3) 0.065(4) 0.065(3) -0.008(3) 0.019(3) 0.012(3) C48 0.085(3) 0.071(4) 0.060(3) 0.001(3) 0.022(3) 0.003(3) C49 0.098(3) 0.043(3) 0.068(3) 0.008(3) 0.003(3) 0.020(3) C50 0.081(3) 0.044(3) 0.066(3) 0.007(3) -0.001(3) 0.004(3) C51 0.095(4) 0.060(4) 0.062(3) -0.013(3) 0.012(3) 0.014(3) C52 0.085(3) 0.066(3) 0.056(3) -0.007(3) -0.014(3) 0.000(3) C53 0.090(3) 0.062(3) 0.062(3) -0.015(3) -0.007(3) -0.006(3) C92 0.080(4) 0.041(4) 0.071(3) -0.004(3) 0.004(3) 0.004(3) C54 0.085(3) 0.045(3) 0.050(3) 0.006(2) 0.011(3) -0.003(3) C55 0.071(3) 0.077(4) 0.079(3) -0.001(3) 0.020(3) -0.007(3) C56 0.089(3) 0.065(3) 0.061(3) 0.015(3) 0.019(3) -0.006(3) C93 0.090(6) 0.065(7) 0.109(6) 0.002(5) -0.011(5) 0.012(5) C57 0.070(3) 0.072(4) 0.080(3) -0.002(3) 0.013(3) -0.018(3) C94 0.078(4) 0.046(4) 0.080(3) -0.008(3) 0.001(3) 0.000(3) C58 0.063(3) 0.050(3) 0.050(3) 0.002(2) 0.009(2) 0.003(3) C59 0.093(3) 0.058(3) 0.061(3) -0.019(3) 0.000(3) 0.001(3) C95 0.106(7) 0.065(7) 0.043(4) 0.000(3) 0.002(4) 0.018(6) C60 0.093(3) 0.050(3) 0.070(3) -0.007(3) 0.007(3) 0.019(3) C61 0.081(3) 0.063(4) 0.060(3) 0.000(3) -0.018(3) 0.009(3) C62 0.064(3) 0.054(3) 0.058(3) -0.005(3) 0.011(2) -0.002(3) C63 0.085(3) 0.050(3) 0.075(3) -0.005(3) 0.006(3) -0.020(3) C64 0.075(3) 0.070(4) 0.075(3) -0.004(3) 0.005(3) 0.015(3) C96 0.141(5) 0.055(5) 0.048(3) 0.009(3) -0.009(4) -0.009(4) C65 0.087(3) 0.062(3) 0.053(3) 0.013(3) -0.009(3) 0.006(3) C97 0.097(4) 0.052(4) 0.064(3) 0.000(3) 0.009(3) 0.010(3) C98 0.096(7) 0.069(6) 0.078(5) -0.013(4) 0.007(4) 0.010(5) C99 0.140(5) 0.056(5) 0.055(3) 0.014(3) -0.009(4) -0.023(4) C66 0.097(3) 0.059(3) 0.057(3) -0.014(3) 0.006(3) 0.007(3) C67 0.096(3) 0.063(4) 0.050(3) -0.004(3) 0.005(3) -0.002(3) C68 0.095(3) 0.040(3) 0.071(3) 0.006(3) 0.004(3) -0.005(3) C100 0.131(5) 0.074(4) 0.051(3) -0.001(3) -0.011(3) 0.018(4) C69 0.099(3) 0.041(3) 0.065(3) 0.009(3) 0.003(3) 0.011(3) C70 0.072(3) 0.038(3) 0.060(3) 0.001(2) -0.001(3) 0.006(3) C101 0.122(8) 0.098(7) 0.090(6) -0.019(5) 0.039(6) -0.003(6) C102 0.127(5) 0.096(5) 0.070(3) -0.005(3) -0.026(4) 0.018(4) C103 0.121(5) 0.092(4) 0.064(3) -0.001(3) -0.025(3) 0.022(4) C104 0.164(6) 0.067(5) 0.074(3) 0.011(3) -0.027(4) -0.033(4) C105 0.096(5) 0.056(4) 0.070(3) -0.005(3) 0.019(3) 0.007(4) C71 0.069(3) 0.053(3) 0.064(3) 0.002(3) -0.001(3) -0.013(3) C72 0.088(3) 0.054(3) 0.062(3) 0.017(3) 0.008(3) -0.004(3) C106 0.074(4) 0.053(5) 0.080(4) -0.008(3) -0.003(3) -0.002(3) C107 0.111(7) 0.111(7) 0.081(5) -0.009(5) -0.022(5) 0.036(6) C73 0.083(3) 0.050(3) 0.070(3) 0.011(3) 0.008(3) -0.007(3) C74 0.066(3) 0.063(4) 0.075(3) -0.004(3) 0.002(3) 0.000(3) C108 0.102(5) 0.062(4) 0.074(3) -0.001(3) 0.024(3) 0.008(4) C109 0.162(6) 0.061(5) 0.066(3) 0.004(3) -0.027(4) -0.018(4) C110 0.153(5) 0.068(5) 0.067(3) 0.016(3) -0.018(4) -0.030(4) C111 0.124(5) 0.079(4) 0.053(3) 0.002(3) -0.014(3) 0.021(4) C75 0.076(3) 0.072(4) 0.078(3) -0.007(3) 0.014(3) 0.011(3) C76 0.098(3) 0.039(3) 0.073(3) -0.002(3) 0.003(3) 0.001(3) C112 0.088(7) 0.072(7) 0.117(7) -0.011(5) 0.017(5) -0.017(5) C77 0.083(3) 0.051(3) 0.064(3) 0.007(3) -0.005(3) 0.011(3) C78 0.100(3) 0.042(3) 0.072(3) -0.001(3) 0.002(3) 0.014(3) C113 0.146(8) 0.090(7) 0.061(5) -0.002(5) -0.004(5) 0.018(6) C114 0.159(9) 0.124(8) 0.086(6) 0.007(6) -0.043(6) -0.005(7) C115 0.198(10) 0.105(8) 0.118(7) 0.033(6) -0.037(7) -0.048(7) S1 0.219(5) 0.163(4) 0.127(3) 0.013(3) 0.018(3) 0.015(4) S3 0.141(5) 0.285(8) 0.274(7) -0.064(6) -0.018(4) 0.074(5) S2 0.247(7) 0.226(6) 0.224(6) -0.008(5) -0.071(6) -0.022(6) S4 0.251(8) 0.402(10) 0.280(9) 0.009(9) 0.015(7) 0.137(8) C117 0.177(8) 0.344(10) 0.251(10) -0.046(9) 0.012(8) 0.117(8) Ce3 0.155(18) 0.079(13) 0.092(10) -0.026(8) 0.027(10) -0.031(11) Ce4 0.097(11) 0.067(12) 0.093(9) 0.021(7) 0.013(7) -0.001(8) S5 0.288(6) 0.286(6) 0.287(6) -0.0009(11) -0.0001(11) -0.0005(11) S6 0.282(6) 0.283(6) 0.282(6) 0.0015(11) 0.0012(11) 0.0011(11) C118 0.285(6) 0.285(6) 0.285(6) 0.0001(11) -0.0001(11) -0.0002(10) C116 0.233(8) 0.174(8) 0.154(7) -0.013(7) -0.047(7) 0.011(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ce1 C43 2.485(9) . ? Ce1 C74 2.491(10) . ? Ce1 C34 2.500(9) . ? Ce1 C36 2.509(8) . ? Ce1 C22 2.554(9) . ? Ce1 C16 2.557(10) . ? Ce1 C23 2.743(9) . ? Ce1 C1 2.749(8) . ? Ce1 C33 2.786(7) . ? Ce1 C13 2.798(8) . ? Ce1 C41 2.870(9) . ? Ce1 C63 2.880(9) . ? Ce2 C64 2.468(10) . ? Ce2 C14 2.470(8) . ? Ce2 C75 2.485(9) . ? Ce2 C12 2.497(9) . ? Ce2 C55 2.536(9) . ? Ce2 C57 2.546(9) . ? Ce2 C2 2.752(7) . ? Ce2 C5 2.766(9) . ? Ce2 C42 2.777(9) . ? Ce2 C11 2.803(9) . ? Ce2 C32 2.878(9) . ? Ce2 C3 2.895(8) . ? Si1 C95 1.903(8) . ? Si1 C88 1.912(10) . ? Si1 C87 1.941(9) . ? Si1 C28 1.987(7) . ? Si2 C95 1.866(9) . ? Si2 C96 1.897(11) . ? Si2 C111 1.907(11) . ? Si2 C17 1.973(7) . ? C79 C82 1.507(16) . ? C79 H1 0.9600 . ? C79 H2 0.9600 . ? C79 H3 0.9600 . ? C1 C62 1.425(12) . ? C1 C30 1.442(13) . ? C1 C74 1.452(12) . ? C2 C14 1.404(12) . ? C2 C31 1.430(12) . ? C2 C9 1.479(13) . ? C3 C20 1.420(13) . ? C3 C48 1.432(13) . ? C3 C55 1.500(14) . ? C4 C58 1.386(11) . ? C4 C54 1.447(12) . ? C4 C17 1.562(12) . ? C5 C71 1.408(13) . ? C5 C31 1.440(12) . ? C5 C12 1.506(13) . ? C6 C60 1.411(15) . ? C6 C42 1.435(12) . ? C6 C11 1.441(14) . ? C7 C9 1.354(13) . ? C7 C10 1.450(13) . ? C7 C17 1.580(11) . ? C8 C54 1.419(13) . ? C8 C33 1.430(13) . ? C8 C15 1.447(12) . ? C8 Ce3 2.620(18) . ? C9 C44 1.468(12) . ? C80 C99 1.430(15) . ? C80 H4 0.9600 . ? C80 H5 0.9600 . ? C80 H6 0.9600 . ? C10 C69 1.402(13) . ? C10 C54 1.415(13) . ? C10 Ce3 3.014(19) . ? C81 C92 1.362(12) . ? C81 C88 1.427(12) . ? C81 C86 1.515(12) . ? C11 C75 1.438(15) . ? C11 C47 1.438(14) . ? C12 C14 1.436(14) . ? C12 C57 1.442(12) . ? C13 C52 1.438(13) . ? C13 C61 1.448(14) . ? C13 C36 1.462(13) . ? C82 C109 1.357(15) . ? C82 C96 1.433(15) . ? C14 C64 1.456(13) . ? C15 C68 1.414(14) . ? C15 C63 1.490(14) . ? C15 Ce3 2.12(2) . ? C16 C41 1.408(14) . ? C16 C36 1.410(13) . ? C16 C22 1.461(12) . ? C17 C19 1.487(11) . ? C18 C73 1.394(13) . ? C18 C32 1.419(13) . ? C18 C71 1.448(11) . ? C18 Ce4 2.099(18) . ? C83 C89 1.386(17) . ? C83 C102 1.404(14) . ? C83 C114 1.537(16) . ? C19 C29 1.367(11) . ? C19 C31 1.434(12) . ? C20 C56 1.447(14) . ? C20 C32 1.469(13) . ? C20 Ce4 2.550(16) . ? C84 C87 1.361(13) . ? C84 C105 1.415(12) . ? C84 C98 1.537(12) . ? C21 C38 1.378(14) . ? C21 C51 1.433(14) . ? C21 C60 1.446(13) . ? C22 C63 1.402(14) . ? C22 C43 1.442(13) . ? C23 C34 1.394(14) . ? C23 C61 1.396(13) . ? C23 C46 1.441(13) . ? C24 C70 1.402(12) . ? C24 C30 1.423(12) . ? C24 C28 1.553(10) . ? C25 C48 1.371(13) . ? C25 C67 1.445(13) . ? C25 C39 1.458(13) . ? C26 C71 1.408(12) . ? C26 C29 1.435(11) . ? C26 C70 1.458(11) . ? C26 Ce4 2.894(17) . ? C27 C65 1.400(13) . ? C27 C72 1.413(13) . ? C27 C77 1.479(12) . ? C27 Ce4 2.689(17) . ? C28 C58 1.479(12) . ? C28 C29 1.539(11) . ? C85 C106 1.348(13) . ? C85 C88 1.453(13) . ? C85 C93 1.585(13) . ? C86 H7 0.9600 . ? C86 H8 0.9600 . ? C86 H9 0.9600 . ? C30 C46 1.480(11) . ? C32 C57 1.466(14) . ? C32 Ce4 2.427(18) . ? C33 C43 1.417(13) . ? C33 C62 1.435(12) . ? C34 C36 1.505(13) . ? C34 C74 1.519(13) . ? C35 C40 1.378(14) . ? C35 C41 1.426(14) . ? C35 C63 1.448(13) . ? C35 Ce3 2.47(2) . ? C87 C97 1.422(12) . ? C37 C45 1.402(13) . ? C37 C39 1.402(14) . ? C37 C65 1.429(13) . ? C38 C40 1.426(13) . ? C38 C59 1.476(13) . ? C89 C100 1.380(15) . ? C89 H10 0.9300 . ? C39 C56 1.476(13) . ? C40 C76 1.422(13) . ? C40 Ce3 2.468(17) . ? C41 C53 1.471(14) . ? C90 C97 1.374(13) . ? C90 C108 1.374(15) . ? C90 H11 0.9300 . ? C91 C97 1.526(15) . ? C91 H47 0.9600 . ? C91 H48 0.9600 . ? C91 H49 0.9600 . ? C42 C64 1.434(14) . ? C42 C44 1.437(13) . ? C43 C74 1.423(14) . ? C44 C49 1.410(14) . ? C45 C52 1.421(13) . ? C45 C67 1.422(13) . ? C46 C77 1.441(13) . ? C47 C51 1.413(14) . ? C47 C48 1.422(13) . ? C49 C69 1.402(13) . ? C49 C78 1.468(13) . ? C49 Ce3 2.96(3) . ? C50 C77 1.379(12) . ? C50 C70 1.416(11) . ? C50 C73 1.472(13) . ? C50 Ce4 2.457(18) . ? C51 C66 1.438(14) . ? C52 C53 1.469(13) . ? C53 C59 1.379(14) . ? C92 C94 1.379(13) . ? C92 H15 0.9300 . ? C54 Ce3 2.981(16) . ? C55 C57 1.407(14) . ? C55 C75 1.427(14) . ? C56 C72 1.393(13) . ? C56 Ce4 2.449(15) . ? C93 H16 0.9600 . ? C93 H17 0.9600 . ? C93 H18 0.9600 . ? C94 C106 1.339(13) . ? C94 C112 1.491(14) . ? C58 C62 1.405(11) . ? C59 C66 1.462(14) . ? C95 H19 0.9700 . ? C95 H20 0.9700 . ? C60 C78 1.432(13) . ? C61 C65 1.421(13) . ? C63 Ce3 2.43(2) . ? C64 C75 1.429(13) . ? C96 C99 1.431(17) . ? C98 H21 0.9600 . ? C98 H22 0.9600 . ? C98 H23 0.9600 . ? C99 C110 1.351(14) . ? C66 C67 1.398(13) . ? C68 C76 1.411(13) . ? C68 C69 1.436(14) . ? C68 Ce3 2.16(2) . ? C100 C111 1.414(13) . ? C100 C113 1.470(16) . ? C69 Ce3 2.62(2) . ? C70 Ce4 2.882(17) . ? C101 C108 1.508(14) . ? C101 H24 0.9600 . ? C101 H25 0.9600 . ? C101 H26 0.9600 . ? C102 C103 1.345(14) . ? C102 H27 0.9300 . ? C103 C111 1.426(17) . ? C103 C107 1.550(15) . ? C104 C109 1.355(18) . ? C104 C110 1.397(17) . ? C104 C115 1.605(17) . ? C105 C108 1.354(13) . ? C105 H28 0.9300 . ? C71 Ce4 2.572(18) . ? C72 C73 1.448(13) . ? C72 Ce4 2.228(16) . ? C106 H29 0.9300 . ? C107 H30 0.9600 . ? C107 H31 0.9600 . ? C107 H32 0.9600 . ? C73 Ce4 1.999(18) . ? C109 H33 0.9300 . ? C110 H34 0.9300 . ? C76 C78 1.452(14) . ? C76 Ce3 2.29(2) . ? C112 H35 0.9600 . ? C112 H36 0.9600 . ? C112 H37 0.9600 . ? C77 Ce4 2.810(18) . ? C78 Ce3 2.82(2) . ? C113 H38 0.9600 . ? C113 H39 0.9600 . ? C113 H40 0.9600 . ? C114 H41 0.9600 . ? C114 H42 0.9600 . ? C114 H43 0.9600 . ? C115 H44 0.9600 . ? C115 H45 0.9600 . ? C115 H46 0.9600 . ? S1 C116 1.48(2) . ? S3 C117 1.51(3) . ? S2 C116 1.59(2) . ? S4 C117 1.50(3) . ? S5 C118 1.543(11) . ? S6 C118 1.524(11) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C43 Ce1 C74 33.2(3) . . ? C43 Ce1 C34 61.7(4) . . ? C74 Ce1 C34 35.4(3) . . ? C43 Ce1 C36 70.2(3) . . ? C74 Ce1 C36 61.1(3) . . ? C34 Ce1 C36 35.0(3) . . ? C43 Ce1 C22 33.2(3) . . ? C74 Ce1 C22 59.6(3) . . ? C34 Ce1 C22 71.8(3) . . ? C36 Ce1 C22 58.7(3) . . ? C43 Ce1 C16 59.6(3) . . ? C74 Ce1 C16 70.6(3) . . ? C34 Ce1 C16 61.0(3) . . ? C36 Ce1 C16 32.3(3) . . ? C22 Ce1 C16 33.2(3) . . ? C43 Ce1 C23 89.0(3) . . ? C74 Ce1 C23 57.2(3) . . ? C34 Ce1 C23 30.4(3) . . ? C36 Ce1 C23 53.5(3) . . ? C22 Ce1 C23 102.0(3) . . ? C16 Ce1 C23 85.3(3) . . ? C43 Ce1 C1 52.5(3) . . ? C74 Ce1 C1 31.7(3) . . ? C34 Ce1 C1 56.7(3) . . ? C36 Ce1 C1 89.6(3) . . ? C22 Ce1 C1 85.2(3) . . ? C16 Ce1 C1 102.2(3) . . ? C23 Ce1 C1 61.6(3) . . ? C43 Ce1 C33 30.5(3) . . ? C74 Ce1 C33 51.4(3) . . ? C34 Ce1 C33 86.3(3) . . ? C36 Ce1 C33 100.7(3) . . ? C22 Ce1 C33 54.3(3) . . ? C16 Ce1 C33 86.5(3) . . ? C23 Ce1 C33 106.6(3) . . ? C1 Ce1 C33 49.6(3) . . ? C43 Ce1 C13 101.4(3) . . ? C74 Ce1 C13 85.9(3) . . ? C34 Ce1 C13 51.5(3) . . ? C36 Ce1 C13 31.4(3) . . ? C22 Ce1 C13 87.1(3) . . ? C16 Ce1 C13 55.0(3) . . ? C23 Ce1 C13 49.1(3) . . ? C1 Ce1 C13 106.4(3) . . ? C33 Ce1 C13 131.7(3) . . ? C43 Ce1 C41 82.5(3) . . ? C74 Ce1 C41 99.7(3) . . ? C34 Ce1 C41 87.2(3) . . ? C36 Ce1 C41 53.2(3) . . ? C22 Ce1 C41 49.8(3) . . ? C16 Ce1 C41 29.4(3) . . ? C23 Ce1 C41 104.5(3) . . ? C1 Ce1 C41 130.9(3) . . ? C33 Ce1 C41 101.8(3) . . ? C13 Ce1 C41 59.7(3) . . ? C43 Ce1 C63 53.7(3) . . ? C74 Ce1 C63 85.6(3) . . ? C34 Ce1 C63 100.7(3) . . ? C36 Ce1 C63 81.4(3) . . ? C22 Ce1 C63 29.1(3) . . ? C16 Ce1 C63 49.7(3) . . ? C23 Ce1 C63 130.6(3) . . ? C1 Ce1 C63 104.1(3) . . ? C33 Ce1 C63 58.6(3) . . ? C13 Ce1 C63 102.5(3) . . ? C41 Ce1 C63 46.7(3) . . ? C64 Ce2 C14 34.3(3) . . ? C64 Ce2 C75 33.5(3) . . ? C14 Ce2 C75 60.2(3) . . ? C64 Ce2 C12 59.8(3) . . ? C14 Ce2 C12 33.6(3) . . ? C75 Ce2 C12 69.0(3) . . ? C64 Ce2 C55 59.5(4) . . ? C14 Ce2 C55 70.0(3) . . ? C75 Ce2 C55 33.0(3) . . ? C12 Ce2 C55 57.8(3) . . ? C64 Ce2 C57 70.7(4) . . ? C14 Ce2 C57 60.5(3) . . ? C75 Ce2 C57 58.9(3) . . ? C12 Ce2 C57 33.2(3) . . ? C55 Ce2 C57 32.1(3) . . ? C64 Ce2 C2 56.1(3) . . ? C14 Ce2 C2 30.6(3) . . ? C75 Ce2 C2 88.0(3) . . ? C12 Ce2 C2 52.0(3) . . ? C55 Ce2 C2 100.3(3) . . ? C57 Ce2 C2 84.8(3) . . ? C64 Ce2 C5 86.8(3) . . ? C14 Ce2 C5 53.3(3) . . ? C75 Ce2 C5 101.7(3) . . ? C12 Ce2 C5 32.8(3) . . ? C55 Ce2 C5 86.5(3) . . ? C57 Ce2 C5 55.4(3) . . ? C2 Ce2 C5 50.0(3) . . ? C64 Ce2 C42 31.0(3) . . ? C14 Ce2 C42 56.0(3) . . ? C75 Ce2 C42 52.3(3) . . ? C12 Ce2 C42 87.8(3) . . ? C55 Ce2 C42 84.6(3) . . ? C57 Ce2 C42 101.5(3) . . ? C2 Ce2 C42 61.3(3) . . ? C5 Ce2 C42 107.2(3) . . ? C64 Ce2 C11 51.5(3) . . ? C14 Ce2 C11 85.1(3) . . ? C75 Ce2 C11 30.8(3) . . ? C12 Ce2 C11 99.7(3) . . ? C55 Ce2 C11 54.8(3) . . ? C57 Ce2 C11 86.0(3) . . ? C2 Ce2 C11 105.9(3) . . ? C5 Ce2 C11 132.3(3) . . ? C42 Ce2 C11 49.4(3) . . ? C64 Ce2 C32 101.2(3) . . ? C14 Ce2 C32 87.6(3) . . ? C75 Ce2 C32 83.5(3) . . ? C12 Ce2 C32 54.9(3) . . ? C55 Ce2 C32 51.0(3) . . ? C57 Ce2 C32 30.6(3) . . ? C2 Ce2 C32 104.1(3) . . ? C5 Ce2 C32 58.7(3) . . ? C42 Ce2 C32 131.7(3) . . ? C11 Ce2 C32 103.0(3) . . ? C64 Ce2 C3 86.9(3) . . ? C14 Ce2 C3 101.1(3) . . ? C75 Ce2 C3 54.4(3) . . ? C12 Ce2 C3 83.2(3) . . ? C55 Ce2 C3 31.2(3) . . ? C57 Ce2 C3 50.7(3) . . ? C2 Ce2 C3 131.1(3) . . ? C5 Ce2 C3 103.4(3) . . ? C42 Ce2 C3 104.1(3) . . ? C11 Ce2 C3 58.5(3) . . ? C32 Ce2 C3 48.4(3) . . ? C95 Si1 C88 117.8(4) . . ? C95 Si1 C87 101.1(4) . . ? C88 Si1 C87 108.6(4) . . ? C95 Si1 C28 102.6(3) . . ? C88 Si1 C28 103.8(3) . . ? C87 Si1 C28 123.9(4) . . ? C95 Si2 C96 118.2(5) . . ? C95 Si2 C111 100.4(5) . . ? C96 Si2 C111 107.8(5) . . ? C95 Si2 C17 102.6(3) . . ? C96 Si2 C17 104.5(4) . . ? C111 Si2 C17 124.3(4) . . ? C82 C79 H1 109.5 . . ? C82 C79 H2 109.5 . . ? H1 C79 H2 109.5 . . ? C82 C79 H3 109.5 . . ? H1 C79 H3 109.5 . . ? H2 C79 H3 109.5 . . ? C62 C1 C30 117.9(8) . . ? C62 C1 C74 106.9(8) . . ? C30 C1 C74 126.1(8) . . ? C62 C1 Ce1 82.6(5) . . ? C30 C1 Ce1 92.4(5) . . ? C74 C1 Ce1 64.3(5) . . ? C14 C2 C31 109.6(8) . . ? C14 C2 C9 124.5(8) . . ? C31 C2 C9 115.0(7) . . ? C14 C2 Ce2 63.5(4) . . ? C31 C2 Ce2 83.0(4) . . ? C9 C2 Ce2 90.7(5) . . ? C20 C3 C48 120.6(10) . . ? C20 C3 C55 106.5(8) . . ? C48 C3 C55 124.1(9) . . ? C20 C3 Ce2 85.6(5) . . ? C48 C3 Ce2 92.7(5) . . ? C55 C3 Ce2 61.1(4) . . ? C58 C4 C54 122.4(8) . . ? C58 C4 C17 123.2(8) . . ? C54 C4 C17 110.5(7) . . ? C71 C5 C31 121.4(8) . . ? C71 C5 C12 125.3(8) . . ? C31 C5 C12 105.8(8) . . ? C71 C5 Ce2 95.1(5) . . ? C31 C5 Ce2 82.3(5) . . ? C12 C5 Ce2 63.8(5) . . ? C60 C6 C42 122.7(9) . . ? C60 C6 C11 122.2(9) . . ? C42 C6 C11 108.3(9) . . ? C60 C6 Ce2 107.5(6) . . ? C42 C6 Ce2 66.9(5) . . ? C11 C6 Ce2 67.9(5) . . ? C9 C7 C10 121.6(8) . . ? C9 C7 C17 124.0(8) . . ? C10 C7 C17 107.0(8) . . ? C54 C8 C33 117.6(8) . . ? C54 C8 C15 116.2(9) . . ? C33 C8 C15 119.4(8) . . ? C54 C8 Ce3 90.1(7) . . ? C33 C8 Ce3 100.5(7) . . ? C15 C8 Ce3 54.0(6) . . ? C7 C9 C44 120.3(9) . . ? C7 C9 C2 120.4(8) . . ? C44 C9 C2 114.8(8) . . ? C99 C80 H4 109.5 . . ? C99 C80 H5 109.5 . . ? H4 C80 H5 109.5 . . ? C99 C80 H6 109.5 . . ? H4 C80 H6 109.5 . . ? H5 C80 H6 109.5 . . ? C69 C10 C54 119.4(9) . . ? C69 C10 C7 118.5(9) . . ? C54 C10 C7 112.2(8) . . ? C69 C10 Ce3 60.4(6) . . ? C54 C10 Ce3 75.1(6) . . ? C7 C10 Ce3 107.2(6) . . ? C92 C81 C88 121.2(9) . . ? C92 C81 C86 119.1(8) . . ? C88 C81 C86 119.6(9) . . ? C75 C11 C47 123.8(9) . . ? C75 C11 C6 107.8(8) . . ? C47 C11 C6 120.1(10) . . ? C75 C11 Ce2 62.3(5) . . ? C47 C11 Ce2 94.4(6) . . ? C6 C11 Ce2 83.7(5) . . ? C14 C12 C57 123.0(8) . . ? C14 C12 C5 106.8(8) . . ? C57 C12 C5 114.4(9) . . ? C14 C12 Ce2 72.2(5) . . ? C57 C12 Ce2 75.3(5) . . ? C5 C12 Ce2 83.5(5) . . ? C52 C13 C61 121.7(9) . . ? C52 C13 C36 121.1(9) . . ? C61 C13 C36 109.4(8) . . ? C52 C13 Ce1 94.2(5) . . ? C61 C13 Ce1 83.3(5) . . ? C36 C13 Ce1 63.3(4) . . ? C109 C82 C96 122.5(13) . . ? C109 C82 C79 114.9(11) . . ? C96 C82 C79 122.6(10) . . ? C2 C14 C12 109.0(8) . . ? C2 C14 C64 119.4(9) . . ? C12 C14 C64 117.8(8) . . ? C2 C14 Ce2 85.9(5) . . ? C12 C14 Ce2 74.2(5) . . ? C64 C14 Ce2 72.8(5) . . ? C68 C15 C8 121.2(9) . . ? C68 C15 C63 118.6(8) . . ? C8 C15 C63 114.7(9) . . ? C68 C15 Ce3 72.2(8) . . ? C8 C15 Ce3 92.5(7) . . ? C63 C15 Ce3 82.7(7) . . ? C41 C16 C36 119.2(9) . . ? C41 C16 C22 106.8(9) . . ? C36 C16 C22 119.7(8) . . ? C41 C16 Ce1 87.7(6) . . ? C36 C16 Ce1 72.0(5) . . ? C22 C16 Ce1 73.3(5) . . ? C19 C17 C4 107.8(6) . . ? C19 C17 C7 110.3(6) . . ? C4 C17 C7 99.5(7) . . ? C19 C17 Si2 115.1(5) . . ? C4 C17 Si2 98.8(5) . . ? C7 C17 Si2 122.1(5) . . ? C73 C18 C32 116.3(8) . . ? C73 C18 C71 119.3(8) . . ? C32 C18 C71 116.5(9) . . ? C73 C18 Ce4 66.3(7) . . ? C32 C18 Ce4 84.9(7) . . ? C71 C18 Ce4 91.1(6) . . ? C89 C83 C102 116.1(10) . . ? C89 C83 C114 128.8(10) . . ? C102 C83 C114 115.1(13) . . ? C29 C19 C31 117.3(7) . . ? C29 C19 C17 122.1(8) . . ? C31 C19 C17 118.4(7) . . ? C3 C20 C56 124.9(9) . . ? C3 C20 C32 109.9(9) . . ? C56 C20 C32 118.4(9) . . ? C3 C20 Ce4 108.6(6) . . ? C56 C20 Ce4 69.4(6) . . ? C32 C20 Ce4 68.3(6) . . ? C87 C84 C105 120.3(8) . . ? C87 C84 C98 122.9(8) . . ? C105 C84 C98 116.7(9) . . ? C38 C21 C51 111.5(9) . . ? C38 C21 C60 120.3(9) . . ? C51 C21 C60 117.5(10) . . ? C63 C22 C43 118.8(9) . . ? C63 C22 C16 107.0(8) . . ? C43 C22 C16 119.6(9) . . ? C63 C22 Ce1 88.4(6) . . ? C43 C22 Ce1 70.8(5) . . ? C16 C22 Ce1 73.5(5) . . ? C34 C23 C61 109.3(9) . . ? C34 C23 C46 124.0(8) . . ? C61 C23 C46 119.3(9) . . ? C34 C23 Ce1 65.1(5) . . ? C61 C23 Ce1 86.3(6) . . ? C46 C23 Ce1 91.1(5) . . ? C70 C24 C30 120.9(7) . . ? C70 C24 C28 109.3(7) . . ? C30 C24 C28 121.4(8) . . ? C48 C25 C67 121.5(9) . . ? C48 C25 C39 126.2(9) . . ? C67 C25 C39 102.8(9) . . ? C71 C26 C29 123.3(8) . . ? C71 C26 C70 122.3(7) . . ? C29 C26 C70 106.1(7) . . ? C71 C26 Ce4 62.7(5) . . ? C29 C26 Ce4 109.4(6) . . ? C70 C26 Ce4 75.0(5) . . ? C65 C27 C72 122.3(9) . . ? C65 C27 C77 121.2(9) . . ? C72 C27 C77 106.6(8) . . ? C65 C27 Ce4 101.9(7) . . ? C72 C27 Ce4 55.9(5) . . ? C77 C27 Ce4 79.0(6) . . ? C58 C28 C29 108.9(6) . . ? C58 C28 C24 111.9(7) . . ? C29 C28 C24 99.7(6) . . ? C58 C28 Si1 114.6(5) . . ? C29 C28 Si1 99.4(5) . . ? C24 C28 Si1 119.7(5) . . ? C19 C29 C26 121.1(8) . . ? C19 C29 C28 123.7(7) . . ? C26 C29 C28 111.4(7) . . ? C106 C85 C88 119.4(8) . . ? C106 C85 C93 117.1(9) . . ? C88 C85 C93 123.5(9) . . ? C81 C86 H7 109.5 . . ? C81 C86 H8 109.5 . . ? H7 C86 H8 109.5 . . ? C81 C86 H9 109.5 . . ? H7 C86 H9 109.5 . . ? H8 C86 H9 109.5 . . ? C24 C30 C1 119.6(7) . . ? C24 C30 C46 118.5(8) . . ? C1 C30 C46 115.9(8) . . ? C2 C31 C19 125.4(8) . . ? C2 C31 C5 108.7(8) . . ? C19 C31 C5 120.8(8) . . ? C2 C31 Ce2 68.2(4) . . ? C19 C31 Ce2 108.7(5) . . ? C5 C31 Ce2 68.7(4) . . ? C18 C32 C57 125.6(8) . . ? C18 C32 C20 121.2(9) . . ? C57 C32 C20 105.6(9) . . ? C18 C32 Ce4 59.5(6) . . ? C57 C32 Ce4 111.4(7) . . ? C20 C32 Ce4 77.5(6) . . ? C18 C32 Ce2 93.8(5) . . ? C57 C32 Ce2 62.1(5) . . ? C20 C32 Ce2 85.5(5) . . ? Ce4 C32 Ce2 49.7(4) . . ? C43 C33 C8 124.5(8) . . ? C43 C33 C62 107.9(8) . . ? C8 C33 C62 117.8(8) . . ? C43 C33 Ce1 62.9(5) . . ? C8 C33 Ce1 94.1(5) . . ? C62 C33 Ce1 81.0(5) . . ? C23 C34 C36 109.9(8) . . ? C23 C34 C74 119.4(8) . . ? C36 C34 C74 114.5(9) . . ? C23 C34 Ce1 84.5(6) . . ? C36 C34 Ce1 72.8(5) . . ? C74 C34 Ce1 72.0(5) . . ? C40 C35 C41 124.5(9) . . ? C40 C35 C63 125.0(9) . . ? C41 C35 C63 104.8(9) . . ? C40 C35 Ce3 73.7(8) . . ? C41 C35 Ce3 104.7(7) . . ? C63 C35 Ce3 71.4(7) . . ? C84 C87 C97 118.2(8) . . ? C84 C87 Si1 127.9(6) . . ? C97 C87 Si1 113.9(7) . . ? C81 C88 C85 114.6(8) . . ? C81 C88 Si1 119.4(7) . . ? C85 C88 Si1 125.9(7) . . ? C16 C36 C13 119.8(9) . . ? C16 C36 C34 123.4(8) . . ? C13 C36 C34 102.6(8) . . ? C16 C36 Ce1 75.7(5) . . ? C13 C36 Ce1 85.3(5) . . ? C34 C36 Ce1 72.2(5) . . ? C45 C37 C39 108.4(9) . . ? C45 C37 C65 122.3(9) . . ? C39 C37 C65 119.0(9) . . ? C21 C38 C40 123.3(9) . . ? C21 C38 C59 108.5(9) . . ? C40 C38 C59 116.9(9) . . ? C100 C89 C83 123.8(10) . . ? C100 C89 H10 118.1 . . ? C83 C89 H10 118.1 . . ? C37 C39 C25 110.6(9) . . ? C37 C39 C56 120.6(9) . . ? C25 C39 C56 118.6(9) . . ? C35 C40 C76 116.2(9) . . ? C35 C40 C38 118.8(9) . . ? C76 C40 C38 117.2(10) . . ? C35 C40 Ce3 74.0(8) . . ? C76 C40 Ce3 65.7(7) . . ? C38 C40 Ce3 103.4(7) . . ? C16 C41 C35 110.8(9) . . ? C16 C41 C53 123.7(9) . . ? C35 C41 C53 118.4(10) . . ? C16 C41 Ce1 62.9(5) . . ? C35 C41 Ce1 86.6(5) . . ? C53 C41 Ce1 93.8(6) . . ? C97 C90 C108 123.4(9) . . ? C97 C90 H11 118.3 . . ? C108 C90 H11 118.3 . . ? C97 C91 H47 109.5 . . ? C97 C91 H48 109.5 . . ? H47 C91 H48 109.5 . . ? C97 C91 H49 109.5 . . ? H47 C91 H49 109.5 . . ? H48 C91 H49 109.5 . . ? C64 C42 C6 107.1(8) . . ? C64 C42 C44 122.8(8) . . ? C6 C42 C44 120.0(10) . . ? C64 C42 Ce2 62.5(5) . . ? C6 C42 Ce2 84.7(5) . . ? C44 C42 Ce2 90.2(6) . . ? C33 C43 C74 108.5(8) . . ? C33 C43 C22 117.6(9) . . ? C74 C43 C22 122.0(8) . . ? C33 C43 Ce1 86.6(5) . . ? C74 C43 Ce1 73.6(5) . . ? C22 C43 Ce1 76.0(5) . . ? C49 C44 C42 116.3(8) . . ? C49 C44 C9 116.8(9) . . ? C42 C44 C9 120.4(9) . . ? C37 C45 C52 121.9(9) . . ? C37 C45 C67 107.4(9) . . ? C52 C45 C67 121.5(9) . . ? C77 C46 C23 117.9(8) . . ? C77 C46 C30 117.2(8) . . ? C23 C46 C30 119.2(9) . . ? C51 C47 C48 118.7(10) . . ? C51 C47 C11 115.5(9) . . ? C48 C47 C11 119.2(9) . . ? C25 C48 C47 121.1(10) . . ? C25 C48 C3 115.1(10) . . ? C47 C48 C3 117.5(9) . . ? C69 C49 C44 122.7(9) . . ? C69 C49 C78 106.1(9) . . ? C44 C49 C78 123.1(9) . . ? C69 C49 Ce3 62.4(6) . . ? C44 C49 Ce3 106.5(7) . . ? C78 C49 Ce3 70.2(6) . . ? C77 C50 C70 119.7(8) . . ? C77 C50 C73 110.6(8) . . ? C70 C50 C73 118.7(8) . . ? C77 C50 Ce4 89.6(7) . . ? C70 C50 Ce4 92.2(6) . . ? C73 C50 Ce4 54.4(6) . . ? C47 C51 C21 125.2(9) . . ? C47 C51 C66 120.0(9) . . ? C21 C51 C66 105.4(9) . . ? C45 C52 C13 115.9(9) . . ? C45 C52 C53 118.3(9) . . ? C13 C52 C53 119.4(9) . . ? C59 C53 C52 119.0(9) . . ? C59 C53 C41 116.1(9) . . ? C52 C53 C41 116.0(9) . . ? C81 C92 C94 122.6(9) . . ? C81 C92 H15 118.7 . . ? C94 C92 H15 118.7 . . ? C10 C54 C8 123.4(8) . . ? C10 C54 C4 107.5(8) . . ? C8 C54 C4 120.6(8) . . ? C10 C54 Ce3 77.7(6) . . ? C8 C54 Ce3 61.5(6) . . ? C4 C54 Ce3 107.5(6) . . ? C57 C55 C75 121.7(9) . . ? C57 C55 C3 107.9(9) . . ? C75 C55 C3 116.2(9) . . ? C57 C55 Ce2 74.3(5) . . ? C75 C55 Ce2 71.5(5) . . ? C3 C55 Ce2 87.7(5) . . ? C72 C56 C20 120.3(9) . . ? C72 C56 C39 118.8(9) . . ? C20 C56 C39 113.4(9) . . ? C72 C56 Ce4 64.2(6) . . ? C20 C56 Ce4 77.1(6) . . ? C39 C56 Ce4 104.3(7) . . ? C85 C93 H16 109.5 . . ? C85 C93 H17 109.5 . . ? H16 C93 H17 109.5 . . ? C85 C93 H18 109.5 . . ? H16 C93 H18 109.5 . . ? H17 C93 H18 109.5 . . ? C55 C57 C12 117.4(9) . . ? C55 C57 C32 109.8(9) . . ? C12 C57 C32 118.5(8) . . ? C55 C57 Ce2 73.5(5) . . ? C12 C57 Ce2 71.5(5) . . ? C32 C57 Ce2 87.3(5) . . ? C106 C94 C92 116.6(9) . . ? C106 C94 C112 125.2(10) . . ? C92 C94 C112 118.1(9) . . ? C4 C58 C62 115.7(8) . . ? C4 C58 C28 121.3(8) . . ? C62 C58 C28 120.5(7) . . ? C53 C59 C66 122.4(9) . . ? C53 C59 C38 124.8(9) . . ? C66 C59 C38 104.5(9) . . ? Si2 C95 Si1 137.8(4) . . ? Si2 C95 H19 102.7 . . ? Si1 C95 H19 102.7 . . ? Si2 C95 H20 102.7 . . ? Si1 C95 H20 102.7 . . ? H19 C95 H20 105.0 . . ? C6 C60 C78 117.8(8) . . ? C6 C60 C21 118.5(9) . . ? C78 C60 C21 118.0(10) . . ? C23 C61 C65 124.5(9) . . ? C23 C61 C13 108.2(9) . . ? C65 C61 C13 120.0(9) . . ? C23 C61 Ce1 66.0(5) . . ? C65 C61 Ce1 107.2(5) . . ? C13 C61 Ce1 68.1(4) . . ? C58 C62 C1 123.2(8) . . ? C58 C62 C33 124.6(8) . . ? C1 C62 C33 108.6(8) . . ? C58 C62 Ce1 110.3(5) . . ? C1 C62 Ce1 68.6(4) . . ? C33 C62 Ce1 70.0(4) . . ? C22 C63 C35 110.4(8) . . ? C22 C63 C15 124.7(8) . . ? C35 C63 C15 115.7(10) . . ? C22 C63 Ce3 108.1(8) . . ? C35 C63 Ce3 74.3(7) . . ? C15 C63 Ce3 59.9(7) . . ? C22 C63 Ce1 62.4(5) . . ? C35 C63 Ce1 85.8(5) . . ? C15 C63 Ce1 91.7(5) . . ? Ce3 C63 Ce1 46.0(5) . . ? C75 C64 C42 109.2(9) . . ? C75 C64 C14 119.1(9) . . ? C42 C64 C14 118.0(8) . . ? C75 C64 Ce2 73.9(6) . . ? C42 C64 Ce2 86.5(6) . . ? C14 C64 Ce2 72.9(5) . . ? C99 C96 C82 117.1(10) . . ? C99 C96 Si2 125.1(8) . . ? C82 C96 Si2 117.9(10) . . ? C27 C65 C61 116.8(8) . . ? C27 C65 C37 119.6(9) . . ? C61 C65 C37 117.2(9) . . ? C90 C97 C87 118.7(10) . . ? C90 C97 C91 116.3(8) . . ? C87 C97 C91 125.0(8) . . ? C84 C98 H21 109.5 . . ? C84 C98 H22 109.5 . . ? H21 C98 H22 109.5 . . ? C84 C98 H23 109.5 . . ? H21 C98 H23 109.5 . . ? H22 C98 H23 109.5 . . ? C110 C99 C80 117.5(12) . . ? C110 C99 C96 118.8(11) . . ? C80 C99 C96 123.6(9) . . ? C67 C66 C51 120.8(10) . . ? C67 C66 C59 118.2(9) . . ? C51 C66 C59 109.9(8) . . ? C66 C67 C45 120.6(9) . . ? C66 C67 C25 117.8(10) . . ? C45 C67 C25 110.7(9) . . ? C76 C68 C15 119.7(9) . . ? C76 C68 C69 108.5(9) . . ? C15 C68 C69 120.0(8) . . ? C76 C68 Ce3 76.4(6) . . ? C15 C68 Ce3 69.3(8) . . ? C69 C68 Ce3 91.3(8) . . ? C89 C100 C111 119.3(12) . . ? C89 C100 C113 114.9(9) . . ? C111 C100 C113 125.8(10) . . ? C10 C69 C49 119.6(10) . . ? C10 C69 C68 119.7(9) . . ? C49 C69 C68 110.0(8) . . ? C10 C69 Ce3 91.9(6) . . ? C49 C69 Ce3 89.3(7) . . ? C68 C69 Ce3 55.5(6) . . ? C24 C70 C50 120.8(8) . . ? C24 C70 C26 111.2(7) . . ? C50 C70 C26 118.4(8) . . ? C24 C70 Ce4 109.0(6) . . ? C50 C70 Ce4 58.4(5) . . ? C26 C70 Ce4 75.8(5) . . ? C108 C101 H24 109.5 . . ? C108 C101 H25 109.5 . . ? H24 C101 H25 109.5 . . ? C108 C101 H26 109.5 . . ? H24 C101 H26 109.5 . . ? H25 C101 H26 109.5 . . ? C103 C102 C83 122.1(13) . . ? C103 C102 H27 118.9 . . ? C83 C102 H27 118.9 . . ? C102 C103 C111 121.8(10) . . ? C102 C103 C107 115.1(12) . . ? C111 C103 C107 123.0(9) . . ? C109 C104 C110 121.8(11) . . ? C109 C104 C115 122.2(12) . . ? C110 C104 C115 115.9(14) . . ? C108 C105 C84 121.9(10) . . ? C108 C105 H28 119.0 . . ? C84 C105 H28 119.0 . . ? C26 C71 C5 115.1(7) . . ? C26 C71 C18 119.2(8) . . ? C5 C71 C18 119.1(8) . . ? C26 C71 Ce4 88.2(6) . . ? C5 C71 Ce4 103.4(7) . . ? C18 C71 Ce4 54.7(5) . . ? C56 C72 C27 119.4(9) . . ? C56 C72 C73 118.2(9) . . ? C27 C72 C73 110.5(8) . . ? C56 C72 Ce4 81.6(7) . . ? C27 C72 Ce4 92.4(7) . . ? C73 C72 Ce4 61.6(6) . . ? C94 C106 C85 125.4(10) . . ? C94 C106 H29 117.3 . . ? C85 C106 H29 117.3 . . ? C103 C107 H30 109.5 . . ? C103 C107 H31 109.5 . . ? H30 C107 H31 109.5 . . ? C103 C107 H32 109.5 . . ? H30 C107 H32 109.5 . . ? H31 C107 H32 109.5 . . ? C18 C73 C72 124.6(9) . . ? C18 C73 C50 122.1(7) . . ? C72 C73 C50 104.3(8) . . ? C18 C73 Ce4 74.0(7) . . ? C72 C73 Ce4 78.8(7) . . ? C50 C73 Ce4 88.8(7) . . ? C43 C74 C1 108.1(8) . . ? C43 C74 C34 120.6(8) . . ? C1 C74 C34 114.8(8) . . ? C43 C74 Ce1 73.2(5) . . ? C1 C74 Ce1 84.0(5) . . ? C34 C74 Ce1 72.6(5) . . ? C105 C108 C90 117.1(9) . . ? C105 C108 C101 121.9(11) . . ? C90 C108 C101 121.0(10) . . ? C104 C109 C82 118.2(12) . . ? C104 C109 H33 120.9 . . ? C82 C109 H33 120.9 . . ? C99 C110 C104 121.4(13) . . ? C99 C110 H34 119.3 . . ? C104 C110 H34 119.3 . . ? C100 C111 C103 116.7(10) . . ? C100 C111 Si2 116.5(10) . . ? C103 C111 Si2 126.7(7) . . ? C55 C75 C64 121.0(9) . . ? C55 C75 C11 118.9(9) . . ? C64 C75 C11 107.4(9) . . ? C55 C75 Ce2 75.5(6) . . ? C64 C75 Ce2 72.6(5) . . ? C11 C75 Ce2 86.9(6) . . ? C68 C76 C40 123.5(10) . . ? C68 C76 C78 107.0(8) . . ? C40 C76 C78 120.8(9) . . ? C68 C76 Ce3 66.8(6) . . ? C40 C76 Ce3 79.8(7) . . ? C78 C76 Ce3 95.5(8) . . ? C94 C112 H35 109.5 . . ? C94 C112 H36 109.5 . . ? H35 C112 H36 109.5 . . ? C94 C112 H37 109.5 . . ? H35 C112 H37 109.5 . . ? H36 C112 H37 109.5 . . ? C50 C77 C46 122.4(8) . . ? C50 C77 C27 107.8(9) . . ? C46 C77 C27 119.2(9) . . ? C50 C77 Ce4 61.0(6) . . ? C46 C77 Ce4 105.4(6) . . ? C27 C77 Ce4 69.9(6) . . ? C60 C78 C76 119.8(9) . . ? C60 C78 C49 118.5(10) . . ? C76 C78 C49 108.2(8) . . ? C60 C78 Ce3 98.0(7) . . ? C76 C78 Ce3 53.7(6) . . ? C49 C78 Ce3 80.5(6) . . ? C100 C113 H38 109.5 . . ? C100 C113 H39 109.5 . . ? H38 C113 H39 109.5 . . ? C100 C113 H40 109.5 . . ? H38 C113 H40 109.5 . . ? H39 C113 H40 109.5 . . ? C83 C114 H41 109.5 . . ? C83 C114 H42 109.5 . . ? H41 C114 H42 109.5 . . ? C83 C114 H43 109.5 . . ? H41 C114 H43 109.5 . . ? H42 C114 H43 109.5 . . ? C104 C115 H44 109.5 . . ? C104 C115 H45 109.5 . . ? H44 C115 H45 109.5 . . ? C104 C115 H46 109.5 . . ? H44 C115 H46 109.5 . . ? H45 C115 H46 109.5 . . ? S4 C117 S3 158(3) . . ? C15 Ce3 C68 38.5(5) . . ? C15 Ce3 C76 67.2(6) . . ? C68 Ce3 C76 36.9(5) . . ? C15 Ce3 C63 37.4(5) . . ? C68 Ce3 C63 65.6(6) . . ? C76 Ce3 C63 73.9(6) . . ? C15 Ce3 C40 77.9(6) . . ? C68 Ce3 C40 64.9(6) . . ? C76 Ce3 C40 34.5(4) . . ? C63 Ce3 C40 61.5(5) . . ? C15 Ce3 C35 65.0(6) . . ? C68 Ce3 C35 74.4(6) . . ? C76 Ce3 C35 59.8(5) . . ? C63 Ce3 C35 34.3(4) . . ? C40 Ce3 C35 32.4(4) . . ? C15 Ce3 C8 33.5(4) . . ? C68 Ce3 C8 62.0(5) . . ? C76 Ce3 C8 97.3(7) . . ? C63 Ce3 C8 58.5(5) . . ? C40 Ce3 C8 111.1(7) . . ? C35 Ce3 C8 92.3(7) . . ? C15 Ce3 C69 61.7(6) . . ? C68 Ce3 C69 33.2(4) . . ? C76 Ce3 C69 55.7(6) . . ? C63 Ce3 C69 96.2(7) . . ? C40 Ce3 C69 90.0(7) . . ? C35 Ce3 C69 107.0(7) . . ? C8 Ce3 C69 66.8(5) . . ? C15 Ce3 C78 90.9(8) . . ? C68 Ce3 C78 53.0(6) . . ? C76 Ce3 C78 30.8(4) . . ? C63 Ce3 C78 104.6(7) . . ? C40 Ce3 C78 55.9(5) . . ? C35 Ce3 C78 87.0(6) . . ? C8 Ce3 C78 112.5(7) . . ? C69 Ce3 C78 49.7(5) . . ? C15 Ce3 C49 87.2(7) . . ? C68 Ce3 C49 51.2(6) . . ? C76 Ce3 C49 51.7(6) . . ? C63 Ce3 C49 116.2(7) . . ? C40 Ce3 C49 83.4(7) . . ? C35 Ce3 C49 111.5(7) . . ? C8 Ce3 C49 94.8(6) . . ? C69 Ce3 C49 28.3(4) . . ? C78 Ce3 C49 29.3(3) . . ? C15 Ce3 C54 53.8(4) . . ? C68 Ce3 C54 63.9(5) . . ? C76 Ce3 C54 99.9(7) . . ? C63 Ce3 C54 85.9(6) . . ? C40 Ce3 C54 127.1(7) . . ? C35 Ce3 C54 118.3(7) . . ? C8 Ce3 C54 28.4(3) . . ? C69 Ce3 C54 51.0(4) . . ? C78 Ce3 C54 100.6(7) . . ? C49 Ce3 C54 74.9(5) . . ? C15 Ce3 C10 64.4(5) . . ? C68 Ce3 C10 53.6(5) . . ? C76 Ce3 C10 83.0(7) . . ? C63 Ce3 C10 101.6(6) . . ? C40 Ce3 C10 116.6(8) . . ? C35 Ce3 C10 125.6(7) . . ? C8 Ce3 C10 52.0(4) . . ? C69 Ce3 C10 27.7(3) . . ? C78 Ce3 C10 75.1(6) . . ? C49 Ce3 C10 47.9(4) . . ? C54 Ce3 C10 27.3(3) . . ? C73 Ce4 C18 39.7(5) . . ? C73 Ce4 C72 39.6(4) . . ? C18 Ce4 C72 71.0(6) . . ? C73 Ce4 C32 64.5(6) . . ? C18 Ce4 C32 35.6(4) . . ? C72 Ce4 C32 75.4(5) . . ? C73 Ce4 C56 65.6(5) . . ? C18 Ce4 C56 78.8(6) . . ? C72 Ce4 C56 34.2(4) . . ? C32 Ce4 C56 61.8(5) . . ? C73 Ce4 C50 36.8(4) . . ? C18 Ce4 C50 66.3(6) . . ? C72 Ce4 C50 58.7(5) . . ? C32 Ce4 C50 98.9(6) . . ? C56 Ce4 C50 92.6(6) . . ? C73 Ce4 C20 75.2(6) . . ? C18 Ce4 C20 64.7(5) . . ? C72 Ce4 C20 61.6(5) . . ? C32 Ce4 C20 34.2(4) . . ? C56 Ce4 C20 33.6(4) . . ? C50 Ce4 C20 111.2(6) . . ? C73 Ce4 C71 63.5(6) . . ? C18 Ce4 C71 34.3(4) . . ? C72 Ce4 C71 101.7(7) . . ? C32 Ce4 C71 58.3(5) . . ? C56 Ce4 C71 112.8(6) . . ? C50 Ce4 C71 70.0(5) . . ? C20 Ce4 C71 92.4(6) . . ? C73 Ce4 C27 58.0(5) . . ? C18 Ce4 C27 96.8(6) . . ? C72 Ce4 C27 31.7(4) . . ? C32 Ce4 C27 107.1(6) . . ? C56 Ce4 C27 56.0(4) . . ? C50 Ce4 C27 53.1(4) . . ? C20 Ce4 C27 88.9(5) . . ? C71 Ce4 C27 118.8(7) . . ? C73 Ce4 C77 55.3(5) . . ? C18 Ce4 C77 92.5(6) . . ? C72 Ce4 C77 53.3(5) . . ? C32 Ce4 C77 119.1(6) . . ? C56 Ce4 C77 84.9(5) . . ? C50 Ce4 C77 29.4(3) . . ? C20 Ce4 C77 114.9(6) . . ? C71 Ce4 C77 99.1(6) . . ? C27 Ce4 C77 31.1(3) . . ? C73 Ce4 C70 57.9(5) . . ? C18 Ce4 C70 69.0(5) . . ? C72 Ce4 C70 87.8(6) . . ? C32 Ce4 C70 104.4(6) . . ? C56 Ce4 C70 121.0(6) . . ? C50 Ce4 C70 29.4(3) . . ? C20 Ce4 C70 130.4(7) . . ? C71 Ce4 C70 54.4(4) . . ? C27 Ce4 C70 79.8(5) . . ? C77 Ce4 C70 50.2(4) . . ? C73 Ce4 C26 67.5(5) . . ? C18 Ce4 C26 56.5(5) . . ? C72 Ce4 C26 105.8(6) . . ? C32 Ce4 C26 86.7(6) . . ? C56 Ce4 C26 131.2(7) . . ? C50 Ce4 C26 54.2(4) . . ? C20 Ce4 C26 120.1(7) . . ? C71 Ce4 C26 29.1(3) . . ? C27 Ce4 C26 107.2(6) . . ? C77 Ce4 C26 79.2(5) . . ? C70 Ce4 C26 29.2(3) . . ? S6 C118 S5 149(4) . . ? S1 C116 S2 153.9(19) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C43 Ce1 C1 C62 72.6(6) . . . . ? C74 Ce1 C1 C62 112.8(8) . . . . ? C34 Ce1 C1 C62 150.4(7) . . . . ? C36 Ce1 C1 C62 137.7(6) . . . . ? C22 Ce1 C1 C62 79.0(6) . . . . ? C16 Ce1 C1 C62 107.7(5) . . . . ? C23 Ce1 C1 C62 -174.5(6) . . . . ? C33 Ce1 C1 C62 33.2(5) . . . . ? C13 Ce1 C1 C62 164.5(5) . . . . ? C41 Ce1 C1 C62 100.7(6) . . . . ? C63 Ce1 C1 C62 56.7(6) . . . . ? C43 Ce1 C1 C30 -169.6(7) . . . . ? C74 Ce1 C1 C30 -129.4(8) . . . . ? C34 Ce1 C1 C30 -91.8(6) . . . . ? C36 Ce1 C1 C30 -104.5(5) . . . . ? C22 Ce1 C1 C30 -163.1(6) . . . . ? C16 Ce1 C1 C30 -134.5(5) . . . . ? C23 Ce1 C1 C30 -56.7(5) . . . . ? C33 Ce1 C1 C30 151.0(7) . . . . ? C13 Ce1 C1 C30 -77.6(5) . . . . ? C41 Ce1 C1 C30 -141.5(5) . . . . ? C63 Ce1 C1 C30 174.5(5) . . . . ? C43 Ce1 C1 C74 -40.2(6) . . . . ? C34 Ce1 C1 C74 37.6(6) . . . . ? C36 Ce1 C1 C74 24.9(6) . . . . ? C22 Ce1 C1 C74 -33.7(6) . . . . ? C16 Ce1 C1 C74 -5.0(6) . . . . ? C23 Ce1 C1 C74 72.7(6) . . . . ? C33 Ce1 C1 C74 -79.6(6) . . . . ? C13 Ce1 C1 C74 51.8(6) . . . . ? C41 Ce1 C1 C74 -12.1(7) . . . . ? C63 Ce1 C1 C74 -56.1(6) . . . . ? C64 Ce2 C2 C14 34.9(6) . . . . ? C75 Ce2 C2 C14 23.7(7) . . . . ? C12 Ce2 C2 C14 -41.0(6) . . . . ? C55 Ce2 C2 C14 -7.1(7) . . . . ? C57 Ce2 C2 C14 -35.3(6) . . . . ? C5 Ce2 C2 C14 -83.5(7) . . . . ? C42 Ce2 C2 C14 70.9(6) . . . . ? C11 Ce2 C2 C14 49.0(7) . . . . ? C32 Ce2 C2 C14 -59.2(7) . . . . ? C3 Ce2 C2 C14 -12.8(8) . . . . ? C64 Ce2 C2 C31 151.0(7) . . . . ? C14 Ce2 C2 C31 116.1(8) . . . . ? C75 Ce2 C2 C31 139.7(6) . . . . ? C12 Ce2 C2 C31 75.1(6) . . . . ? C55 Ce2 C2 C31 109.0(5) . . . . ? C57 Ce2 C2 C31 80.8(5) . . . . ? C5 Ce2 C2 C31 32.6(5) . . . . ? C42 Ce2 C2 C31 -173.0(6) . . . . ? C11 Ce2 C2 C31 165.1(5) . . . . ? C32 Ce2 C2 C31 56.9(6) . . . . ? C3 Ce2 C2 C31 103.3(6) . . . . ? C64 Ce2 C2 C9 -94.0(6) . . . . ? C14 Ce2 C2 C9 -128.9(9) . . . . ? C75 Ce2 C2 C9 -105.2(5) . . . . ? C12 Ce2 C2 C9 -169.9(7) . . . . ? C55 Ce2 C2 C9 -135.9(5) . . . . ? C57 Ce2 C2 C9 -164.2(5) . . . . ? C5 Ce2 C2 C9 147.6(6) . . . . ? C42 Ce2 C2 C9 -58.0(5) . . . . ? C11 Ce2 C2 C9 -79.8(5) . . . . ? C32 Ce2 C2 C9 172.0(5) . . . . ? C3 Ce2 C2 C9 -141.6(5) . . . . ? C64 Ce2 C3 C20 -138.6(6) . . . . ? C14 Ce2 C3 C20 -107.3(6) . . . . ? C75 Ce2 C3 C20 -147.6(7) . . . . ? C12 Ce2 C3 C20 -78.6(6) . . . . ? C55 Ce2 C3 C20 -111.6(9) . . . . ? C57 Ce2 C3 C20 -71.1(6) . . . . ? C2 Ce2 C3 C20 -100.7(6) . . . . ? C5 Ce2 C3 C20 -52.7(6) . . . . ? C42 Ce2 C3 C20 -164.6(6) . . . . ? C11 Ce2 C3 C20 175.6(7) . . . . ? C32 Ce2 C3 C20 -30.7(6) . . . . ? C64 Ce2 C3 C48 100.9(7) . . . . ? C14 Ce2 C3 C48 132.2(6) . . . . ? C75 Ce2 C3 C48 91.9(7) . . . . ? C12 Ce2 C3 C48 160.9(7) . . . . ? C55 Ce2 C3 C48 128.0(9) . . . . ? C57 Ce2 C3 C48 168.4(8) . . . . ? C2 Ce2 C3 C48 138.8(6) . . . . ? C5 Ce2 C3 C48 -173.2(6) . . . . ? C42 Ce2 C3 C48 74.9(7) . . . . ? C11 Ce2 C3 C48 55.1(6) . . . . ? C32 Ce2 C3 C48 -151.2(8) . . . . ? C64 Ce2 C3 C55 -27.1(6) . . . . ? C14 Ce2 C3 C55 4.3(7) . . . . ? C75 Ce2 C3 C55 -36.0(6) . . . . ? C12 Ce2 C3 C55 32.9(6) . . . . ? C57 Ce2 C3 C55 40.4(6) . . . . ? C2 Ce2 C3 C55 10.9(8) . . . . ? C5 Ce2 C3 C55 58.9(6) . . . . ? C42 Ce2 C3 C55 -53.1(7) . . . . ? C11 Ce2 C3 C55 -72.9(6) . . . . ? C32 Ce2 C3 C55 80.9(7) . . . . ? C64 Ce2 C5 C71 159.6(6) . . . . ? C14 Ce2 C5 C71 167.5(7) . . . . ? C75 Ce2 C5 C71 129.4(6) . . . . ? C12 Ce2 C5 C71 127.1(8) . . . . ? C55 Ce2 C5 C71 99.9(6) . . . . ? C57 Ce2 C5 C71 90.9(6) . . . . ? C2 Ce2 C5 C71 -153.4(7) . . . . ? C42 Ce2 C5 C71 -176.8(5) . . . . ? C11 Ce2 C5 C71 133.0(6) . . . . ? C32 Ce2 C5 C71 54.4(5) . . . . ? C3 Ce2 C5 C71 73.6(6) . . . . ? C64 Ce2 C5 C31 -79.4(6) . . . . ? C14 Ce2 C5 C31 -71.5(6) . . . . ? C75 Ce2 C5 C31 -109.6(6) . . . . ? C12 Ce2 C5 C31 -111.9(8) . . . . ? C55 Ce2 C5 C31 -139.0(6) . . . . ? C57 Ce2 C5 C31 -148.1(7) . . . . ? C2 Ce2 C5 C31 -32.4(5) . . . . ? C42 Ce2 C5 C31 -55.7(6) . . . . ? C11 Ce2 C5 C31 -106.0(6) . . . . ? C32 Ce2 C5 C31 175.5(7) . . . . ? C3 Ce2 C5 C31 -165.4(5) . . . . ? C64 Ce2 C5 C12 32.5(6) . . . . ? C14 Ce2 C5 C12 40.4(5) . . . . ? C75 Ce2 C5 C12 2.3(6) . . . . ? C55 Ce2 C5 C12 -27.1(6) . . . . ? C57 Ce2 C5 C12 -36.2(6) . . . . ? C2 Ce2 C5 C12 79.5(6) . . . . ? C42 Ce2 C5 C12 56.2(6) . . . . ? C11 Ce2 C5 C12 5.9(7) . . . . ? C32 Ce2 C5 C12 -72.6(6) . . . . ? C3 Ce2 C5 C12 -53.5(6) . . . . ? C64 Ce2 C6 C60 158.2(8) . . . . ? C14 Ce2 C6 C60 145.1(6) . . . . ? C75 Ce2 C6 C60 -156.7(8) . . . . ? C12 Ce2 C6 C60 165.0(6) . . . . ? C55 Ce2 C6 C60 -143.8(6) . . . . ? C57 Ce2 C6 C60 -160.0(6) . . . . ? C2 Ce2 C6 C60 115.6(6) . . . . ? C5 Ce2 C6 C60 141.2(6) . . . . ? C42 Ce2 C6 C60 118.8(9) . . . . ? C11 Ce2 C6 C60 -118.4(9) . . . . ? C32 Ce2 C6 C60 -136.0(6) . . . . ? C3 Ce2 C6 C60 -113.2(6) . . . . ? C64 Ce2 C6 C42 39.4(6) . . . . ? C14 Ce2 C6 C42 26.3(6) . . . . ? C75 Ce2 C6 C42 84.5(7) . . . . ? C12 Ce2 C6 C42 46.2(7) . . . . ? C55 Ce2 C6 C42 97.4(7) . . . . ? C57 Ce2 C6 C42 81.2(7) . . . . ? C2 Ce2 C6 C42 -3.2(6) . . . . ? C5 Ce2 C6 C42 22.4(8) . . . . ? C11 Ce2 C6 C42 122.8(10) . . . . ? C32 Ce2 C6 C42 105.1(6) . . . . ? C3 Ce2 C6 C42 128.0(7) . . . . ? C64 Ce2 C6 C11 -83.4(7) . . . . ? C14 Ce2 C6 C11 -96.5(7) . . . . ? C75 Ce2 C6 C11 -38.3(6) . . . . ? C12 Ce2 C6 C11 -76.6(7) . . . . ? C55 Ce2 C6 C11 -25.4(6) . . . . ? C57 Ce2 C6 C11 -41.6(7) . . . . ? C2 Ce2 C6 C11 -126.0(6) . . . . ? C5 Ce2 C6 C11 -100.4(7) . . . . ? C42 Ce2 C6 C11 -122.8(10) . . . . ? C32 Ce2 C6 C11 -17.7(8) . . . . ? C3 Ce2 C6 C11 5.2(6) . . . . ? C10 C7 C9 C44 -7.1(12) . . . . ? C17 C7 C9 C44 -153.0(8) . . . . ? C10 C7 C9 C2 147.7(8) . . . . ? C17 C7 C9 C2 1.8(12) . . . . ? C14 C2 C9 C7 -157.7(8) . . . . ? C31 C2 C9 C7 -17.3(10) . . . . ? Ce2 C2 C9 C7 -99.9(7) . . . . ? C14 C2 C9 C44 -1.6(12) . . . . ? C31 C2 C9 C44 138.8(8) . . . . ? Ce2 C2 C9 C44 56.2(7) . . . . ? C9 C7 C10 C69 7.6(12) . . . . ? C17 C7 C10 C69 158.5(7) . . . . ? C9 C7 C10 C54 -138.1(8) . . . . ? C17 C7 C10 C54 12.9(8) . . . . ? C9 C7 C10 Ce3 -57.6(10) . . . . ? C17 C7 C10 Ce3 93.4(7) . . . . ? C60 C6 C11 C75 155.5(9) . . . . ? C42 C6 C11 C75 3.7(11) . . . . ? Ce2 C6 C11 C75 58.2(6) . . . . ? C60 C6 C11 C47 5.9(14) . . . . ? C42 C6 C11 C47 -145.9(9) . . . . ? Ce2 C6 C11 C47 -91.4(8) . . . . ? C60 C6 C11 Ce2 97.3(8) . . . . ? C42 C6 C11 Ce2 -54.5(7) . . . . ? C64 Ce2 C11 C75 -41.7(6) . . . . ? C14 Ce2 C11 C75 -34.0(6) . . . . ? C12 Ce2 C11 C75 -3.7(6) . . . . ? C55 Ce2 C11 C75 34.9(6) . . . . ? C57 Ce2 C11 C75 26.7(6) . . . . ? C2 Ce2 C11 C75 -56.7(6) . . . . ? C5 Ce2 C11 C75 -6.9(7) . . . . ? C42 Ce2 C11 C75 -82.2(7) . . . . ? C32 Ce2 C11 C75 52.3(6) . . . . ? C3 Ce2 C11 C75 72.1(6) . . . . ? C64 Ce2 C11 C47 -167.9(9) . . . . ? C14 Ce2 C11 C47 -160.2(7) . . . . ? C75 Ce2 C11 C47 -126.2(9) . . . . ? C12 Ce2 C11 C47 -129.9(7) . . . . ? C55 Ce2 C11 C47 -91.3(7) . . . . ? C57 Ce2 C11 C47 -99.5(7) . . . . ? C2 Ce2 C11 C47 177.1(6) . . . . ? C5 Ce2 C11 C47 -133.1(6) . . . . ? C42 Ce2 C11 C47 151.6(9) . . . . ? C32 Ce2 C11 C47 -73.9(7) . . . . ? C3 Ce2 C11 C47 -54.1(6) . . . . ? C64 Ce2 C11 C6 72.2(7) . . . . ? C14 Ce2 C11 C6 79.9(6) . . . . ? C75 Ce2 C11 C6 114.0(9) . . . . ? C12 Ce2 C11 C6 110.3(6) . . . . ? C55 Ce2 C11 C6 148.8(8) . . . . ? C57 Ce2 C11 C6 140.7(6) . . . . ? C2 Ce2 C11 C6 57.3(7) . . . . ? C5 Ce2 C11 C6 107.1(7) . . . . ? C42 Ce2 C11 C6 31.8(6) . . . . ? C32 Ce2 C11 C6 166.3(6) . . . . ? C3 Ce2 C11 C6 -173.9(7) . . . . ? C71 C5 C12 C14 -146.0(9) . . . . ? C31 C5 C12 C14 3.8(10) . . . . ? Ce2 C5 C12 C14 -69.1(6) . . . . ? C71 C5 C12 C57 -6.3(14) . . . . ? C31 C5 C12 C57 143.4(8) . . . . ? Ce2 C5 C12 C57 70.6(7) . . . . ? C71 C5 C12 Ce2 -76.9(9) . . . . ? C31 C5 C12 Ce2 72.9(6) . . . . ? C64 Ce2 C12 C14 -31.6(5) . . . . ? C75 Ce2 C12 C14 -67.6(5) . . . . ? C55 Ce2 C12 C14 -102.5(6) . . . . ? C57 Ce2 C12 C14 -132.6(8) . . . . ? C2 Ce2 C12 C14 37.1(5) . . . . ? C5 Ce2 C12 C14 110.0(7) . . . . ? C42 Ce2 C12 C14 -17.4(5) . . . . ? C11 Ce2 C12 C14 -65.5(5) . . . . ? C32 Ce2 C12 C14 -164.6(6) . . . . ? C3 Ce2 C12 C14 -121.9(5) . . . . ? C64 Ce2 C12 C57 101.0(6) . . . . ? C14 Ce2 C12 C57 132.6(8) . . . . ? C75 Ce2 C12 C57 65.0(6) . . . . ? C55 Ce2 C12 C57 30.1(6) . . . . ? C2 Ce2 C12 C57 169.6(7) . . . . ? C5 Ce2 C12 C57 -117.4(9) . . . . ? C42 Ce2 C12 C57 115.1(6) . . . . ? C11 Ce2 C12 C57 67.0(6) . . . . ? C32 Ce2 C12 C57 -32.1(5) . . . . ? C3 Ce2 C12 C57 10.6(6) . . . . ? C64 Ce2 C12 C5 -141.6(6) . . . . ? C14 Ce2 C12 C5 -110.0(7) . . . . ? C75 Ce2 C12 C5 -177.6(6) . . . . ? C55 Ce2 C12 C5 147.5(7) . . . . ? C57 Ce2 C12 C5 117.4(9) . . . . ? C2 Ce2 C12 C5 -73.0(5) . . . . ? C42 Ce2 C12 C5 -127.5(6) . . . . ? C11 Ce2 C12 C5 -175.6(5) . . . . ? C32 Ce2 C12 C5 85.3(6) . . . . ? C3 Ce2 C12 C5 128.1(6) . . . . ? C43 Ce1 C13 C52 -129.1(6) . . . . ? C74 Ce1 C13 C52 -158.6(7) . . . . ? C34 Ce1 C13 C52 -167.9(8) . . . . ? C36 Ce1 C13 C52 -122.8(9) . . . . ? C22 Ce1 C13 C52 -98.9(7) . . . . ? C16 Ce1 C13 C52 -89.4(7) . . . . ? C23 Ce1 C13 C52 152.4(8) . . . . ? C1 Ce1 C13 C52 177.0(6) . . . . ? C33 Ce1 C13 C52 -133.0(6) . . . . ? C41 Ce1 C13 C52 -54.8(6) . . . . ? C63 Ce1 C13 C52 -74.1(7) . . . . ? C43 Ce1 C13 C61 109.5(6) . . . . ? C74 Ce1 C13 C61 80.0(6) . . . . ? C34 Ce1 C13 C61 70.7(6) . . . . ? C36 Ce1 C13 C61 115.8(9) . . . . ? C22 Ce1 C13 C61 139.6(6) . . . . ? C16 Ce1 C13 C61 149.2(7) . . . . ? C23 Ce1 C13 C61 30.9(5) . . . . ? C1 Ce1 C13 C61 55.5(6) . . . . ? C33 Ce1 C13 C61 105.5(6) . . . . ? C41 Ce1 C13 C61 -176.2(7) . . . . ? C63 Ce1 C13 C61 164.5(6) . . . . ? C43 Ce1 C13 C36 -6.3(6) . . . . ? C74 Ce1 C13 C36 -35.8(6) . . . . ? C34 Ce1 C13 C36 -45.1(6) . . . . ? C22 Ce1 C13 C36 23.9(6) . . . . ? C16 Ce1 C13 C36 33.4(6) . . . . ? C23 Ce1 C13 C36 -84.8(6) . . . . ? C1 Ce1 C13 C36 -60.2(6) . . . . ? C33 Ce1 C13 C36 -10.2(7) . . . . ? C41 Ce1 C13 C36 68.0(6) . . . . ? C63 Ce1 C13 C36 48.7(6) . . . . ? C31 C2 C14 C12 0.6(10) . . . . ? C9 C2 C14 C12 142.7(8) . . . . ? Ce2 C2 C14 C12 71.8(6) . . . . ? C31 C2 C14 C64 -138.8(8) . . . . ? C9 C2 C14 C64 3.3(13) . . . . ? Ce2 C2 C14 C64 -67.6(7) . . . . ? C31 C2 C14 Ce2 -71.2(6) . . . . ? C9 C2 C14 Ce2 70.9(8) . . . . ? C57 C12 C14 C2 -138.0(9) . . . . ? C5 C12 C14 C2 -2.7(10) . . . . ? Ce2 C12 C14 C2 -79.9(6) . . . . ? C57 C12 C14 C64 2.1(14) . . . . ? C5 C12 C14 C64 137.4(8) . . . . ? Ce2 C12 C14 C64 60.2(8) . . . . ? C57 C12 C14 Ce2 -58.2(8) . . . . ? C5 C12 C14 Ce2 77.2(6) . . . . ? C64 Ce2 C14 C2 -122.5(9) . . . . ? C75 Ce2 C14 C2 -152.5(8) . . . . ? C12 Ce2 C14 C2 111.0(8) . . . . ? C55 Ce2 C14 C2 172.6(7) . . . . ? C57 Ce2 C14 C2 138.6(7) . . . . ? C5 Ce2 C14 C2 71.7(6) . . . . ? C42 Ce2 C14 C2 -90.2(7) . . . . ? C11 Ce2 C14 C2 -133.2(6) . . . . ? C32 Ce2 C14 C2 123.5(6) . . . . ? C3 Ce2 C14 C2 170.2(6) . . . . ? C64 Ce2 C14 C12 126.5(8) . . . . ? C75 Ce2 C14 C12 96.5(6) . . . . ? C55 Ce2 C14 C12 61.6(5) . . . . ? C57 Ce2 C14 C12 27.6(5) . . . . ? C2 Ce2 C14 C12 -111.0(8) . . . . ? C5 Ce2 C14 C12 -39.4(5) . . . . ? C42 Ce2 C14 C12 158.8(6) . . . . ? C11 Ce2 C14 C12 115.8(5) . . . . ? C32 Ce2 C14 C12 12.5(5) . . . . ? C3 Ce2 C14 C12 59.2(5) . . . . ? C75 Ce2 C14 C64 -30.0(6) . . . . ? C12 Ce2 C14 C64 -126.5(8) . . . . ? C55 Ce2 C14 C64 -64.9(6) . . . . ? C57 Ce2 C14 C64 -98.9(6) . . . . ? C2 Ce2 C14 C64 122.5(9) . . . . ? C5 Ce2 C14 C64 -165.8(7) . . . . ? C42 Ce2 C14 C64 32.3(5) . . . . ? C11 Ce2 C14 C64 -10.7(6) . . . . ? C32 Ce2 C14 C64 -114.0(6) . . . . ? C3 Ce2 C14 C64 -67.3(6) . . . . ? C54 C8 C15 C68 1.4(12) . . . . ? C33 C8 C15 C68 152.0(8) . . . . ? Ce3 C8 C15 C68 70.6(9) . . . . ? C54 C8 C15 C63 -152.2(8) . . . . ? C33 C8 C15 C63 -1.7(12) . . . . ? Ce3 C8 C15 C63 -83.0(9) . . . . ? C54 C8 C15 Ce3 -69.2(9) . . . . ? C33 C8 C15 Ce3 81.4(10) . . . . ? C43 Ce1 C16 C41 -137.2(7) . . . . ? C74 Ce1 C16 C41 -172.0(7) . . . . ? C34 Ce1 C16 C41 150.5(7) . . . . ? C36 Ce1 C16 C41 121.7(9) . . . . ? C22 Ce1 C16 C41 -108.3(9) . . . . ? C23 Ce1 C16 C41 131.2(6) . . . . ? C1 Ce1 C16 C41 -169.2(6) . . . . ? C33 Ce1 C16 C41 -121.8(6) . . . . ? C13 Ce1 C16 C41 89.2(6) . . . . ? C63 Ce1 C16 C41 -71.0(6) . . . . ? C43 Ce1 C16 C36 101.1(6) . . . . ? C74 Ce1 C16 C36 66.3(6) . . . . ? C34 Ce1 C16 C36 28.8(5) . . . . ? C22 Ce1 C16 C36 130.0(9) . . . . ? C23 Ce1 C16 C36 9.5(5) . . . . ? C1 Ce1 C16 C36 69.1(6) . . . . ? C33 Ce1 C16 C36 116.5(6) . . . . ? C13 Ce1 C16 C36 -32.5(5) . . . . ? C41 Ce1 C16 C36 -121.7(9) . . . . ? C63 Ce1 C16 C36 167.3(7) . . . . ? C43 Ce1 C16 C22 -28.9(6) . . . . ? C74 Ce1 C16 C22 -63.6(6) . . . . ? C34 Ce1 C16 C22 -101.2(6) . . . . ? C36 Ce1 C16 C22 -130.0(9) . . . . ? C23 Ce1 C16 C22 -120.5(6) . . . . ? C1 Ce1 C16 C22 -60.8(6) . . . . ? C33 Ce1 C16 C22 -13.5(6) . . . . ? C13 Ce1 C16 C22 -162.4(7) . . . . ? C41 Ce1 C16 C22 108.3(9) . . . . ? C63 Ce1 C16 C22 37.3(5) . . . . ? C58 C4 C17 C19 -26.4(9) . . . . ? C54 C4 C17 C19 131.8(6) . . . . ? C58 C4 C17 C7 -141.4(7) . . . . ? C54 C4 C17 C7 16.7(7) . . . . ? C58 C4 C17 Si2 93.7(7) . . . . ? C54 C4 C17 Si2 -108.2(5) . . . . ? C9 C7 C17 C19 19.9(11) . . . . ? C10 C7 C17 C19 -130.2(7) . . . . ? C9 C7 C17 C4 132.9(8) . . . . ? C10 C7 C17 C4 -17.2(7) . . . . ? C9 C7 C17 Si2 -120.3(8) . . . . ? C10 C7 C17 Si2 89.6(8) . . . . ? C95 Si2 C17 C19 41.7(7) . . . . ? C96 Si2 C17 C19 165.6(7) . . . . ? C111 Si2 C17 C19 -70.5(8) . . . . ? C95 Si2 C17 C4 -72.8(6) . . . . ? C96 Si2 C17 C4 51.1(7) . . . . ? C111 Si2 C17 C4 175.1(6) . . . . ? C95 Si2 C17 C7 -179.9(7) . . . . ? C96 Si2 C17 C7 -56.0(8) . . . . ? C111 Si2 C17 C7 67.9(9) . . . . ? C4 C17 C19 C29 29.3(9) . . . . ? C7 C17 C19 C29 137.0(7) . . . . ? Si2 C17 C19 C29 -79.8(9) . . . . ? C4 C17 C19 C31 -133.4(7) . . . . ? C7 C17 C19 C31 -25.8(9) . . . . ? Si2 C17 C19 C31 117.4(6) . . . . ? C48 C3 C20 C56 -7.2(12) . . . . ? C55 C3 C20 C56 -155.8(8) . . . . ? Ce2 C3 C20 C56 -97.7(8) . . . . ? C48 C3 C20 C32 143.1(8) . . . . ? C55 C3 C20 C32 -5.5(10) . . . . ? Ce2 C3 C20 C32 52.6(7) . . . . ? C48 C3 C20 Ce4 70.2(9) . . . . ? C55 C3 C20 Ce4 -78.4(9) . . . . ? Ce2 C3 C20 Ce4 -20.3(6) . . . . ? C41 C16 C22 C63 -0.8(11) . . . . ? C36 C16 C22 C63 -140.1(10) . . . . ? Ce1 C16 C22 C63 -83.1(7) . . . . ? C41 C16 C22 C43 138.1(9) . . . . ? C36 C16 C22 C43 -1.3(14) . . . . ? Ce1 C16 C22 C43 55.7(8) . . . . ? C41 C16 C22 Ce1 82.3(7) . . . . ? C36 C16 C22 Ce1 -57.1(8) . . . . ? C43 Ce1 C22 C63 -121.3(8) . . . . ? C74 Ce1 C22 C63 -150.5(6) . . . . ? C34 Ce1 C22 C63 172.8(6) . . . . ? C36 Ce1 C22 C63 136.9(6) . . . . ? C16 Ce1 C22 C63 108.2(8) . . . . ? C23 Ce1 C22 C63 169.7(5) . . . . ? C1 Ce1 C22 C63 -130.7(5) . . . . ? C33 Ce1 C22 C63 -88.4(6) . . . . ? C13 Ce1 C22 C63 122.6(6) . . . . ? C41 Ce1 C22 C63 70.7(6) . . . . ? C74 Ce1 C22 C43 -29.1(5) . . . . ? C34 Ce1 C22 C43 -65.8(6) . . . . ? C36 Ce1 C22 C43 -101.8(6) . . . . ? C16 Ce1 C22 C43 -130.4(9) . . . . ? C23 Ce1 C22 C43 -69.0(6) . . . . ? C1 Ce1 C22 C43 -9.3(6) . . . . ? C33 Ce1 C22 C43 32.9(5) . . . . ? C13 Ce1 C22 C43 -116.1(6) . . . . ? C41 Ce1 C22 C43 -167.9(8) . . . . ? C63 Ce1 C22 C43 121.3(8) . . . . ? C43 Ce1 C22 C16 130.4(9) . . . . ? C74 Ce1 C22 C16 101.3(7) . . . . ? C34 Ce1 C22 C16 64.6(6) . . . . ? C36 Ce1 C22 C16 28.6(5) . . . . ? C23 Ce1 C22 C16 61.4(6) . . . . ? C1 Ce1 C22 C16 121.1(6) . . . . ? C33 Ce1 C22 C16 163.3(7) . . . . ? C13 Ce1 C22 C16 14.3(6) . . . . ? C41 Ce1 C22 C16 -37.5(5) . . . . ? C63 Ce1 C22 C16 -108.2(8) . . . . ? C43 Ce1 C23 C34 -24.8(6) . . . . ? C74 Ce1 C23 C34 -35.2(5) . . . . ? C36 Ce1 C23 C34 41.1(5) . . . . ? C22 Ce1 C23 C34 5.9(6) . . . . ? C16 Ce1 C23 C34 34.8(5) . . . . ? C1 Ce1 C23 C34 -71.8(5) . . . . ? C33 Ce1 C23 C34 -50.1(6) . . . . ? C13 Ce1 C23 C34 81.2(6) . . . . ? C41 Ce1 C23 C34 57.2(6) . . . . ? C63 Ce1 C23 C34 12.5(7) . . . . ? C43 Ce1 C23 C61 -138.1(6) . . . . ? C74 Ce1 C23 C61 -148.5(7) . . . . ? C34 Ce1 C23 C61 -113.3(8) . . . . ? C36 Ce1 C23 C61 -72.2(6) . . . . ? C22 Ce1 C23 C61 -107.4(6) . . . . ? C16 Ce1 C23 C61 -78.5(6) . . . . ? C1 Ce1 C23 C61 174.9(7) . . . . ? C33 Ce1 C23 C61 -163.4(6) . . . . ? C13 Ce1 C23 C61 -32.1(6) . . . . ? C41 Ce1 C23 C61 -56.1(7) . . . . ? C63 Ce1 C23 C61 -100.8(6) . . . . ? C43 Ce1 C23 C46 102.6(6) . . . . ? C74 Ce1 C23 C46 92.2(6) . . . . ? C34 Ce1 C23 C46 127.4(8) . . . . ? C36 Ce1 C23 C46 168.5(7) . . . . ? C22 Ce1 C23 C46 133.3(6) . . . . ? C16 Ce1 C23 C46 162.2(6) . . . . ? C1 Ce1 C23 C46 55.6(5) . . . . ? C33 Ce1 C23 C46 77.3(6) . . . . ? C13 Ce1 C23 C46 -151.4(7) . . . . ? C41 Ce1 C23 C46 -175.4(5) . . . . ? C63 Ce1 C23 C46 139.9(5) . . . . ? C70 C24 C28 C58 -129.8(7) . . . . ? C30 C24 C28 C58 18.6(10) . . . . ? C70 C24 C28 C29 -14.8(8) . . . . ? C30 C24 C28 C29 133.6(8) . . . . ? C70 C24 C28 Si1 91.9(8) . . . . ? C30 C24 C28 Si1 -119.7(7) . . . . ? C95 Si1 C28 C58 51.6(7) . . . . ? C88 Si1 C28 C58 174.7(6) . . . . ? C87 Si1 C28 C58 -61.2(7) . . . . ? C95 Si1 C28 C29 -64.4(6) . . . . ? C88 Si1 C28 C29 58.8(6) . . . . ? C87 Si1 C28 C29 -177.1(5) . . . . ? C95 Si1 C28 C24 -171.2(7) . . . . ? C88 Si1 C28 C24 -48.1(7) . . . . ? C87 Si1 C28 C24 76.0(8) . . . . ? C31 C19 C29 C26 2.8(11) . . . . ? C17 C19 C29 C26 -160.2(7) . . . . ? C31 C19 C29 C28 158.9(7) . . . . ? C17 C19 C29 C28 -4.1(11) . . . . ? C71 C26 C29 C19 0.8(12) . . . . ? C70 C26 C29 C19 149.6(7) . . . . ? Ce4 C26 C29 C19 70.3(9) . . . . ? C71 C26 C29 C28 -157.9(7) . . . . ? C70 C26 C29 C28 -9.1(9) . . . . ? Ce4 C26 C29 C28 -88.5(7) . . . . ? C58 C28 C29 C19 -26.4(9) . . . . ? C24 C28 C29 C19 -143.7(7) . . . . ? Si1 C28 C29 C19 93.8(7) . . . . ? C58 C28 C29 C26 131.8(7) . . . . ? C24 C28 C29 C26 14.4(8) . . . . ? Si1 C28 C29 C26 -108.1(6) . . . . ? C70 C24 C30 C1 145.4(8) . . . . ? C28 C24 C30 C1 0.6(12) . . . . ? C70 C24 C30 C46 -6.1(12) . . . . ? C28 C24 C30 C46 -150.8(8) . . . . ? C62 C1 C30 C24 -16.4(11) . . . . ? C74 C1 C30 C24 -158.9(9) . . . . ? Ce1 C1 C30 C24 -99.3(7) . . . . ? C62 C1 C30 C46 135.8(8) . . . . ? C74 C1 C30 C46 -6.7(13) . . . . ? Ce1 C1 C30 C46 52.9(7) . . . . ? C14 C2 C31 C19 156.6(8) . . . . ? C9 C2 C31 C19 10.5(10) . . . . ? Ce2 C2 C31 C19 98.0(7) . . . . ? C14 C2 C31 C5 1.9(10) . . . . ? C9 C2 C31 C5 -144.2(7) . . . . ? Ce2 C2 C31 C5 -56.7(6) . . . . ? C14 C2 C31 Ce2 58.6(6) . . . . ? C9 C2 C31 Ce2 -87.5(6) . . . . ? C29 C19 C31 C2 -151.0(8) . . . . ? C17 C19 C31 C2 12.6(11) . . . . ? C29 C19 C31 C5 0.8(11) . . . . ? C17 C19 C31 C5 164.4(7) . . . . ? C29 C19 C31 Ce2 -75.0(8) . . . . ? C17 C19 C31 Ce2 88.6(7) . . . . ? C71 C5 C31 C2 147.7(8) . . . . ? C12 C5 C31 C2 -3.5(9) . . . . ? Ce2 C5 C31 C2 56.4(6) . . . . ? C71 C5 C31 C19 -8.3(12) . . . . ? C12 C5 C31 C19 -159.5(7) . . . . ? Ce2 C5 C31 C19 -99.6(7) . . . . ? C71 C5 C31 Ce2 91.3(8) . . . . ? C12 C5 C31 Ce2 -59.9(5) . . . . ? C64 Ce2 C31 C2 -24.0(6) . . . . ? C14 Ce2 C31 C2 -36.8(6) . . . . ? C75 Ce2 C31 C2 -43.3(6) . . . . ? C12 Ce2 C31 C2 -81.1(6) . . . . ? C55 Ce2 C31 C2 -78.2(6) . . . . ? C57 Ce2 C31 C2 -95.6(6) . . . . ? C5 Ce2 C31 C2 -121.8(8) . . . . ? C42 Ce2 C31 C2 6.1(6) . . . . ? C11 Ce2 C31 C2 -19.9(7) . . . . ? C32 Ce2 C31 C2 -125.6(6) . . . . ? C3 Ce2 C31 C2 -102.7(6) . . . . ? C64 Ce2 C31 C19 -145.6(6) . . . . ? C14 Ce2 C31 C19 -158.4(7) . . . . ? C75 Ce2 C31 C19 -164.9(6) . . . . ? C12 Ce2 C31 C19 157.3(7) . . . . ? C55 Ce2 C31 C19 160.2(6) . . . . ? C57 Ce2 C31 C19 142.8(6) . . . . ? C2 Ce2 C31 C19 -121.6(8) . . . . ? C5 Ce2 C31 C19 116.7(8) . . . . ? C42 Ce2 C31 C19 -115.4(6) . . . . ? C11 Ce2 C31 C19 -141.5(6) . . . . ? C32 Ce2 C31 C19 112.8(6) . . . . ? C3 Ce2 C31 C19 135.7(6) . . . . ? C64 Ce2 C31 C5 97.8(6) . . . . ? C14 Ce2 C31 C5 85.0(6) . . . . ? C75 Ce2 C31 C5 78.4(6) . . . . ? C12 Ce2 C31 C5 40.7(6) . . . . ? C55 Ce2 C31 C5 43.5(6) . . . . ? C57 Ce2 C31 C5 26.2(6) . . . . ? C2 Ce2 C31 C5 121.8(8) . . . . ? C42 Ce2 C31 C5 127.9(6) . . . . ? C11 Ce2 C31 C5 101.8(6) . . . . ? C32 Ce2 C31 C5 -3.9(6) . . . . ? C3 Ce2 C31 C5 19.1(7) . . . . ? C73 C18 C32 C57 -156.1(9) . . . . ? C71 C18 C32 C57 -7.1(14) . . . . ? Ce4 C18 C32 C57 -95.7(10) . . . . ? C73 C18 C32 C20 -11.1(13) . . . . ? C71 C18 C32 C20 137.9(9) . . . . ? Ce4 C18 C32 C20 49.3(9) . . . . ? C73 C18 C32 Ce4 -60.4(8) . . . . ? C71 C18 C32 Ce4 88.6(8) . . . . ? C73 C18 C32 Ce2 -98.0(8) . . . . ? C71 C18 C32 Ce2 51.0(8) . . . . ? Ce4 C18 C32 Ce2 -37.7(5) . . . . ? C3 C20 C32 C18 -144.7(8) . . . . ? C56 C20 C32 C18 7.7(13) . . . . ? Ce4 C20 C32 C18 -42.0(8) . . . . ? C3 C20 C32 C57 6.3(10) . . . . ? C56 C20 C32 C57 158.8(8) . . . . ? Ce4 C20 C32 C57 109.1(7) . . . . ? C3 C20 C32 Ce4 -102.8(8) . . . . ? C56 C20 C32 Ce4 49.7(8) . . . . ? C3 C20 C32 Ce2 -53.1(7) . . . . ? C56 C20 C32 Ce2 99.4(8) . . . . ? Ce4 C20 C32 Ce2 49.7(4) . . . . ? C64 Ce2 C32 C18 -133.8(6) . . . . ? C14 Ce2 C32 C18 -102.2(6) . . . . ? C75 Ce2 C32 C18 -162.5(6) . . . . ? C12 Ce2 C32 C18 -93.7(6) . . . . ? C55 Ce2 C32 C18 -168.2(8) . . . . ? C57 Ce2 C32 C18 -128.6(9) . . . . ? C2 Ce2 C32 C18 -76.3(6) . . . . ? C5 Ce2 C32 C18 -54.6(6) . . . . ? C42 Ce2 C32 C18 -140.2(6) . . . . ? C11 Ce2 C32 C18 173.4(6) . . . . ? C3 Ce2 C32 C18 150.6(8) . . . . ? C64 Ce2 C32 C57 -5.2(6) . . . . ? C14 Ce2 C32 C57 26.5(5) . . . . ? C75 Ce2 C32 C57 -33.9(5) . . . . ? C12 Ce2 C32 C57 34.9(5) . . . . ? C55 Ce2 C32 C57 -39.6(5) . . . . ? C2 Ce2 C32 C57 52.4(6) . . . . ? C5 Ce2 C32 C57 74.0(6) . . . . ? C42 Ce2 C32 C57 -11.5(7) . . . . ? C11 Ce2 C32 C57 -58.0(6) . . . . ? C3 Ce2 C32 C57 -80.7(6) . . . . ? C64 Ce2 C32 C20 105.1(6) . . . . ? C14 Ce2 C32 C20 136.7(6) . . . . ? C75 Ce2 C32 C20 76.4(6) . . . . ? C12 Ce2 C32 C20 145.2(7) . . . . ? C55 Ce2 C32 C20 70.7(6) . . . . ? C57 Ce2 C32 C20 110.3(8) . . . . ? C2 Ce2 C32 C20 162.7(6) . . . . ? C5 Ce2 C32 C20 -175.7(7) . . . . ? C42 Ce2 C32 C20 98.8(6) . . . . ? C11 Ce2 C32 C20 52.3(6) . . . . ? C3 Ce2 C32 C20 29.6(5) . . . . ? C64 Ce2 C32 Ce4 -177.5(5) . . . . ? C14 Ce2 C32 Ce4 -145.8(5) . . . . ? C75 Ce2 C32 Ce4 153.8(5) . . . . ? C12 Ce2 C32 Ce4 -137.4(6) . . . . ? C55 Ce2 C32 Ce4 148.2(6) . . . . ? C57 Ce2 C32 Ce4 -172.3(8) . . . . ? C2 Ce2 C32 Ce4 -119.9(5) . . . . ? C5 Ce2 C32 Ce4 -98.2(6) . . . . ? C42 Ce2 C32 Ce4 176.2(5) . . . . ? C11 Ce2 C32 Ce4 129.8(5) . . . . ? C3 Ce2 C32 Ce4 107.0(6) . . . . ? C54 C8 C33 C43 154.8(8) . . . . ? C15 C8 C33 C43 4.7(13) . . . . ? Ce3 C8 C33 C43 59.1(10) . . . . ? C54 C8 C33 C62 13.1(10) . . . . ? C15 C8 C33 C62 -137.0(8) . . . . ? Ce3 C8 C33 C62 -82.5(8) . . . . ? C54 C8 C33 Ce1 95.1(6) . . . . ? C15 C8 C33 Ce1 -55.0(8) . . . . ? Ce3 C8 C33 Ce1 -0.6(6) . . . . ? C74 Ce1 C33 C43 41.1(6) . . . . ? C34 Ce1 C33 C43 34.3(6) . . . . ? C36 Ce1 C33 C43 2.3(6) . . . . ? C22 Ce1 C33 C43 -35.9(6) . . . . ? C16 Ce1 C33 C43 -26.9(6) . . . . ? C23 Ce1 C33 C43 57.2(6) . . . . ? C1 Ce1 C33 C43 82.5(6) . . . . ? C13 Ce1 C33 C43 7.6(7) . . . . ? C41 Ce1 C33 C43 -52.0(6) . . . . ? C63 Ce1 C33 C43 -70.6(6) . . . . ? C43 Ce1 C33 C8 126.9(8) . . . . ? C74 Ce1 C33 C8 168.0(7) . . . . ? C34 Ce1 C33 C8 161.2(6) . . . . ? C36 Ce1 C33 C8 129.2(6) . . . . ? C22 Ce1 C33 C8 91.0(6) . . . . ? C16 Ce1 C33 C8 100.1(6) . . . . ? C23 Ce1 C33 C8 -175.9(5) . . . . ? C1 Ce1 C33 C8 -150.6(7) . . . . ? C13 Ce1 C33 C8 134.6(5) . . . . ? C41 Ce1 C33 C8 74.9(6) . . . . ? C63 Ce1 C33 C8 56.3(5) . . . . ? C43 Ce1 C33 C62 -115.5(8) . . . . ? C74 Ce1 C33 C62 -74.5(6) . . . . ? C34 Ce1 C33 C62 -81.2(6) . . . . ? C36 Ce1 C33 C62 -113.3(5) . . . . ? C22 Ce1 C33 C62 -151.4(7) . . . . ? C16 Ce1 C33 C62 -142.4(6) . . . . ? C23 Ce1 C33 C62 -58.4(6) . . . . ? C1 Ce1 C33 C62 -33.1(5) . . . . ? C13 Ce1 C33 C62 -107.9(6) . . . . ? C41 Ce1 C33 C62 -167.6(5) . . . . ? C63 Ce1 C33 C62 173.8(6) . . . . ? C61 C23 C34 C36 6.7(10) . . . . ? C46 C23 C34 C36 -142.8(9) . . . . ? Ce1 C23 C34 C36 -69.5(6) . . . . ? C61 C23 C34 C74 141.9(9) . . . . ? C46 C23 C34 C74 -7.6(14) . . . . ? Ce1 C23 C34 C74 65.7(8) . . . . ? C61 C23 C34 Ce1 76.2(7) . . . . ? C46 C23 C34 Ce1 -73.3(9) . . . . ? C43 Ce1 C34 C23 151.5(6) . . . . ? C74 Ce1 C34 C23 123.4(8) . . . . ? C36 Ce1 C34 C23 -112.8(8) . . . . ? C22 Ce1 C34 C23 -173.9(6) . . . . ? C16 Ce1 C34 C23 -139.4(6) . . . . ? C1 Ce1 C34 C23 89.8(6) . . . . ? C33 Ce1 C34 C23 132.6(5) . . . . ? C13 Ce1 C34 C23 -72.8(6) . . . . ? C41 Ce1 C34 C23 -125.4(5) . . . . ? C63 Ce1 C34 C23 -170.3(5) . . . . ? C43 Ce1 C34 C36 -95.7(6) . . . . ? C74 Ce1 C34 C36 -123.8(8) . . . . ? C22 Ce1 C34 C36 -61.1(6) . . . . ? C16 Ce1 C34 C36 -26.6(5) . . . . ? C23 Ce1 C34 C36 112.8(8) . . . . ? C1 Ce1 C34 C36 -157.4(7) . . . . ? C33 Ce1 C34 C36 -114.6(6) . . . . ? C13 Ce1 C34 C36 40.0(5) . . . . ? C41 Ce1 C34 C36 -12.6(6) . . . . ? C63 Ce1 C34 C36 -57.5(6) . . . . ? C43 Ce1 C34 C74 28.1(5) . . . . ? C36 Ce1 C34 C74 123.8(8) . . . . ? C22 Ce1 C34 C74 62.7(5) . . . . ? C16 Ce1 C34 C74 97.2(6) . . . . ? C23 Ce1 C34 C74 -123.4(8) . . . . ? C1 Ce1 C34 C74 -33.6(5) . . . . ? C33 Ce1 C34 C74 9.2(5) . . . . ? C13 Ce1 C34 C74 163.8(7) . . . . ? C41 Ce1 C34 C74 111.2(6) . . . . ? C63 Ce1 C34 C74 66.3(5) . . . . ? C105 C84 C87 C97 -4.6(14) . . . . ? C98 C84 C87 C97 177.6(9) . . . . ? C105 C84 C87 Si1 173.1(7) . . . . ? C98 C84 C87 Si1 -4.7(15) . . . . ? C95 Si1 C87 C84 -114.7(9) . . . . ? C88 Si1 C87 C84 120.7(9) . . . . ? C28 Si1 C87 C84 -1.2(11) . . . . ? C95 Si1 C87 C97 63.1(8) . . . . ? C88 Si1 C87 C97 -61.5(7) . . . . ? C28 Si1 C87 C97 176.6(6) . . . . ? C92 C81 C88 C85 -3.0(11) . . . . ? C86 C81 C88 C85 -178.6(7) . . . . ? C92 C81 C88 Si1 177.7(6) . . . . ? C86 C81 C88 Si1 2.2(10) . . . . ? C106 C85 C88 C81 4.0(11) . . . . ? C93 C85 C88 C81 -175.2(8) . . . . ? C106 C85 C88 Si1 -176.9(6) . . . . ? C93 C85 C88 Si1 4.0(12) . . . . ? C95 Si1 C88 C81 -166.0(6) . . . . ? C87 Si1 C88 C81 -52.1(7) . . . . ? C28 Si1 C88 C81 81.4(7) . . . . ? C95 Si1 C88 C85 14.8(8) . . . . ? C87 Si1 C88 C85 128.8(7) . . . . ? C28 Si1 C88 C85 -97.7(7) . . . . ? C41 C16 C36 C13 -0.8(13) . . . . ? C22 C16 C36 C13 133.6(9) . . . . ? Ce1 C16 C36 C13 75.9(7) . . . . ? C41 C16 C36 C34 -133.6(10) . . . . ? C22 C16 C36 C34 0.8(14) . . . . ? Ce1 C16 C36 C34 -56.9(8) . . . . ? C41 C16 C36 Ce1 -76.8(8) . . . . ? C22 C16 C36 Ce1 57.7(8) . . . . ? C52 C13 C36 C16 7.5(12) . . . . ? C61 C13 C36 C16 -142.2(8) . . . . ? Ce1 C13 C36 C16 -70.6(7) . . . . ? C52 C13 C36 C34 148.7(8) . . . . ? C61 C13 C36 C34 -1.0(9) . . . . ? Ce1 C13 C36 C34 70.5(5) . . . . ? C52 C13 C36 Ce1 78.1(8) . . . . ? C61 C13 C36 Ce1 -71.5(7) . . . . ? C23 C34 C36 C16 135.9(10) . . . . ? C74 C34 C36 C16 -1.7(13) . . . . ? Ce1 C34 C36 C16 58.5(9) . . . . ? C23 C34 C36 C13 -3.4(10) . . . . ? C74 C34 C36 C13 -141.0(8) . . . . ? Ce1 C34 C36 C13 -80.8(6) . . . . ? C23 C34 C36 Ce1 77.4(7) . . . . ? C74 C34 C36 Ce1 -60.2(7) . . . . ? C43 Ce1 C36 C16 -64.2(6) . . . . ? C74 Ce1 C36 C16 -99.4(6) . . . . ? C34 Ce1 C36 C16 -132.8(9) . . . . ? C22 Ce1 C36 C16 -29.4(5) . . . . ? C23 Ce1 C36 C16 -168.2(7) . . . . ? C1 Ce1 C36 C16 -114.0(6) . . . . ? C33 Ce1 C36 C16 -65.4(6) . . . . ? C13 Ce1 C36 C16 122.3(9) . . . . ? C41 Ce1 C36 C16 31.4(5) . . . . ? C63 Ce1 C36 C16 -9.7(6) . . . . ? C43 Ce1 C36 C13 173.5(7) . . . . ? C74 Ce1 C36 C13 138.2(7) . . . . ? C34 Ce1 C36 C13 104.9(8) . . . . ? C22 Ce1 C36 C13 -151.8(7) . . . . ? C16 Ce1 C36 C13 -122.3(9) . . . . ? C23 Ce1 C36 C13 69.4(6) . . . . ? C1 Ce1 C36 C13 123.6(6) . . . . ? C33 Ce1 C36 C13 172.3(6) . . . . ? C41 Ce1 C36 C13 -91.0(6) . . . . ? C63 Ce1 C36 C13 -132.1(6) . . . . ? C43 Ce1 C36 C34 68.6(6) . . . . ? C74 Ce1 C36 C34 33.4(6) . . . . ? C22 Ce1 C36 C34 103.4(6) . . . . ? C16 Ce1 C36 C34 132.8(9) . . . . ? C23 Ce1 C36 C34 -35.4(5) . . . . ? C1 Ce1 C36 C34 18.7(6) . . . . ? C33 Ce1 C36 C34 67.4(6) . . . . ? C13 Ce1 C36 C34 -104.9(8) . . . . ? C41 Ce1 C36 C34 164.2(7) . . . . ? C63 Ce1 C36 C34 123.0(6) . . . . ? C51 C21 C38 C40 -142.7(9) . . . . ? C60 C21 C38 C40 0.9(16) . . . . ? C51 C21 C38 C59 -0.2(10) . . . . ? C60 C21 C38 C59 143.4(9) . . . . ? C102 C83 C89 C100 4.0(18) . . . . ? C114 C83 C89 C100 -176.4(11) . . . . ? C45 C37 C39 C25 -1.2(9) . . . . ? C65 C37 C39 C25 144.6(7) . . . . ? C45 C37 C39 C56 -145.9(8) . . . . ? C65 C37 C39 C56 -0.1(13) . . . . ? C48 C25 C39 C37 -142.6(9) . . . . ? C67 C25 C39 C37 3.5(9) . . . . ? C48 C25 C39 C56 2.9(13) . . . . ? C67 C25 C39 C56 149.0(7) . . . . ? C41 C35 C40 C76 148.6(9) . . . . ? C63 C35 C40 C76 -0.6(15) . . . . ? Ce3 C35 C40 C76 51.7(9) . . . . ? C41 C35 C40 C38 0.2(14) . . . . ? C63 C35 C40 C38 -149.0(9) . . . . ? Ce3 C35 C40 C38 -96.7(9) . . . . ? C41 C35 C40 Ce3 96.9(10) . . . . ? C63 C35 C40 Ce3 -52.3(10) . . . . ? C21 C38 C40 C35 142.8(10) . . . . ? C59 C38 C40 C35 3.1(13) . . . . ? C21 C38 C40 C76 -5.4(15) . . . . ? C59 C38 C40 C76 -145.0(9) . . . . ? C21 C38 C40 Ce3 63.9(12) . . . . ? C59 C38 C40 Ce3 -75.7(10) . . . . ? C36 C16 C41 C35 142.4(9) . . . . ? C22 C16 C41 C35 2.8(11) . . . . ? Ce1 C16 C41 C35 74.5(8) . . . . ? C36 C16 C41 C53 -7.6(14) . . . . ? C22 C16 C41 C53 -147.2(9) . . . . ? Ce1 C16 C41 C53 -75.4(9) . . . . ? C36 C16 C41 Ce1 67.9(7) . . . . ? C22 C16 C41 Ce1 -71.8(6) . . . . ? C40 C35 C41 C16 -157.8(9) . . . . ? C63 C35 C41 C16 -3.5(11) . . . . ? Ce3 C35 C41 C16 -77.7(10) . . . . ? C40 C35 C41 C53 -6.1(14) . . . . ? C63 C35 C41 C53 148.2(9) . . . . ? Ce3 C35 C41 C53 74.0(10) . . . . ? C40 C35 C41 Ce1 -98.6(9) . . . . ? C63 C35 C41 Ce1 55.7(7) . . . . ? Ce3 C35 C41 Ce1 -18.5(6) . . . . ? C43 Ce1 C41 C16 36.2(6) . . . . ? C74 Ce1 C41 C16 7.7(7) . . . . ? C34 Ce1 C41 C16 -25.6(6) . . . . ? C36 Ce1 C41 C16 -34.6(6) . . . . ? C22 Ce1 C41 C16 42.9(6) . . . . ? C23 Ce1 C41 C16 -50.8(7) . . . . ? C1 Ce1 C41 C16 14.1(7) . . . . ? C33 Ce1 C41 C16 60.0(6) . . . . ? C13 Ce1 C41 C16 -71.7(6) . . . . ? C63 Ce1 C41 C16 82.0(7) . . . . ? C43 Ce1 C41 C35 -79.3(6) . . . . ? C74 Ce1 C41 C35 -107.9(6) . . . . ? C34 Ce1 C41 C35 -141.1(7) . . . . ? C36 Ce1 C41 C35 -150.1(8) . . . . ? C22 Ce1 C41 C35 -72.7(7) . . . . ? C16 Ce1 C41 C35 -115.5(9) . . . . ? C23 Ce1 C41 C35 -166.3(6) . . . . ? C1 Ce1 C41 C35 -101.5(7) . . . . ? C33 Ce1 C41 C35 -55.5(7) . . . . ? C13 Ce1 C41 C35 172.8(7) . . . . ? C63 Ce1 C41 C35 -33.5(6) . . . . ? C43 Ce1 C41 C53 162.4(7) . . . . ? C74 Ce1 C41 C53 133.9(6) . . . . ? C34 Ce1 C41 C53 100.6(6) . . . . ? C36 Ce1 C41 C53 91.6(7) . . . . ? C22 Ce1 C41 C53 169.1(8) . . . . ? C16 Ce1 C41 C53 126.2(9) . . . . ? C23 Ce1 C41 C53 75.4(7) . . . . ? C1 Ce1 C41 C53 140.3(6) . . . . ? C33 Ce1 C41 C53 -173.7(6) . . . . ? C13 Ce1 C41 C53 54.5(6) . . . . ? C63 Ce1 C41 C53 -151.8(8) . . . . ? C60 C6 C42 C64 -155.6(9) . . . . ? C11 C6 C42 C64 -4.0(11) . . . . ? Ce2 C6 C42 C64 -59.1(6) . . . . ? C60 C6 C42 C44 -9.4(14) . . . . ? C11 C6 C42 C44 142.2(9) . . . . ? Ce2 C6 C42 C44 87.1(8) . . . . ? C60 C6 C42 Ce2 -96.5(9) . . . . ? C11 C6 C42 Ce2 55.1(7) . . . . ? C14 Ce2 C42 C64 -35.8(5) . . . . ? C75 Ce2 C42 C64 40.6(6) . . . . ? C12 Ce2 C42 C64 -24.2(5) . . . . ? C55 Ce2 C42 C64 33.6(5) . . . . ? C57 Ce2 C42 C64 6.2(6) . . . . ? C2 Ce2 C42 C64 -71.3(5) . . . . ? C5 Ce2 C42 C64 -51.0(6) . . . . ? C11 Ce2 C42 C64 80.6(6) . . . . ? C32 Ce2 C42 C64 12.1(6) . . . . ? C3 Ce2 C42 C64 58.2(6) . . . . ? C64 Ce2 C42 C6 -112.4(8) . . . . ? C14 Ce2 C42 C6 -148.2(7) . . . . ? C75 Ce2 C42 C6 -71.7(6) . . . . ? C12 Ce2 C42 C6 -136.6(6) . . . . ? C55 Ce2 C42 C6 -78.8(6) . . . . ? C57 Ce2 C42 C6 -106.2(6) . . . . ? C2 Ce2 C42 C6 176.4(7) . . . . ? C5 Ce2 C42 C6 -163.3(6) . . . . ? C11 Ce2 C42 C6 -31.8(6) . . . . ? C32 Ce2 C42 C6 -100.3(7) . . . . ? C3 Ce2 C42 C6 -54.2(7) . . . . ? C64 Ce2 C42 C44 127.5(8) . . . . ? C14 Ce2 C42 C44 91.8(6) . . . . ? C75 Ce2 C42 C44 168.2(8) . . . . ? C12 Ce2 C42 C44 103.3(6) . . . . ? C55 Ce2 C42 C44 161.2(6) . . . . ? C57 Ce2 C42 C44 133.7(6) . . . . ? C2 Ce2 C42 C44 56.3(6) . . . . ? C5 Ce2 C42 C44 76.6(6) . . . . ? C11 Ce2 C42 C44 -151.9(8) . . . . ? C32 Ce2 C42 C44 139.7(6) . . . . ? C3 Ce2 C42 C44 -174.3(6) . . . . ? C8 C33 C43 C74 -146.7(8) . . . . ? C62 C33 C43 C74 -1.9(10) . . . . ? Ce1 C33 C43 C74 -71.4(7) . . . . ? C8 C33 C43 C22 -3.0(13) . . . . ? C62 C33 C43 C22 141.8(8) . . . . ? Ce1 C33 C43 C22 72.2(7) . . . . ? C8 C33 C43 Ce1 -75.3(8) . . . . ? C62 C33 C43 Ce1 69.5(7) . . . . ? C63 C22 C43 C33 -1.4(13) . . . . ? C16 C22 C43 C33 -135.5(9) . . . . ? Ce1 C22 C43 C33 -78.4(8) . . . . ? C63 C22 C43 C74 137.0(10) . . . . ? C16 C22 C43 C74 3.0(14) . . . . ? Ce1 C22 C43 C74 60.1(8) . . . . ? C63 C22 C43 Ce1 77.0(8) . . . . ? C16 C22 C43 Ce1 -57.1(8) . . . . ? C74 Ce1 C43 C33 -110.4(7) . . . . ? C34 Ce1 C43 C33 -140.3(7) . . . . ? C36 Ce1 C43 C33 -177.6(7) . . . . ? C22 Ce1 C43 C33 119.6(9) . . . . ? C16 Ce1 C43 C33 148.5(7) . . . . ? C23 Ce1 C43 C33 -126.4(6) . . . . ? C1 Ce1 C43 C33 -72.2(6) . . . . ? C13 Ce1 C43 C33 -174.2(6) . . . . ? C41 Ce1 C43 C33 128.9(6) . . . . ? C63 Ce1 C43 C33 88.5(6) . . . . ? C34 Ce1 C43 C74 -29.9(5) . . . . ? C36 Ce1 C43 C74 -67.3(5) . . . . ? C22 Ce1 C43 C74 -130.0(8) . . . . ? C16 Ce1 C43 C74 -101.1(6) . . . . ? C23 Ce1 C43 C74 -16.0(5) . . . . ? C1 Ce1 C43 C74 38.2(5) . . . . ? C33 Ce1 C43 C74 110.4(7) . . . . ? C13 Ce1 C43 C74 -63.8(5) . . . . ? C41 Ce1 C43 C74 -120.7(5) . . . . ? C63 Ce1 C43 C74 -161.1(6) . . . . ? C74 Ce1 C43 C22 130.0(8) . . . . ? C34 Ce1 C43 C22 100.1(6) . . . . ? C36 Ce1 C43 C22 62.8(6) . . . . ? C16 Ce1 C43 C22 28.9(6) . . . . ? C23 Ce1 C43 C22 114.0(6) . . . . ? C1 Ce1 C43 C22 168.2(7) . . . . ? C33 Ce1 C43 C22 -119.6(9) . . . . ? C13 Ce1 C43 C22 66.2(6) . . . . ? C41 Ce1 C43 C22 9.3(6) . . . . ? C63 Ce1 C43 C22 -31.1(5) . . . . ? C64 C42 C44 C49 154.8(9) . . . . ? C6 C42 C44 C49 14.0(13) . . . . ? Ce2 C42 C44 C49 98.0(8) . . . . ? C64 C42 C44 C9 3.9(14) . . . . ? C6 C42 C44 C9 -136.9(9) . . . . ? Ce2 C42 C44 C9 -52.9(8) . . . . ? C7 C9 C44 C49 3.4(12) . . . . ? C2 C9 C44 C49 -152.8(8) . . . . ? C7 C9 C44 C42 154.1(9) . . . . ? C2 C9 C44 C42 -2.0(12) . . . . ? C39 C37 C45 C52 145.4(8) . . . . ? C65 C37 C45 C52 1.0(12) . . . . ? C39 C37 C45 C67 -1.7(8) . . . . ? C65 C37 C45 C67 -146.2(8) . . . . ? C34 C23 C46 C77 158.7(9) . . . . ? C61 C23 C46 C77 12.1(13) . . . . ? Ce1 C23 C46 C77 98.4(8) . . . . ? C34 C23 C46 C30 6.1(13) . . . . ? C61 C23 C46 C30 -140.6(9) . . . . ? Ce1 C23 C46 C30 -54.3(8) . . . . ? C24 C30 C46 C77 0.7(12) . . . . ? C1 C30 C46 C77 -151.8(8) . . . . ? C24 C30 C46 C23 153.5(9) . . . . ? C1 C30 C46 C23 1.0(12) . . . . ? C75 C11 C47 C51 -156.0(9) . . . . ? C6 C11 C47 C51 -11.5(12) . . . . ? Ce2 C11 C47 C51 -96.7(7) . . . . ? C75 C11 C47 C48 -4.9(14) . . . . ? C6 C11 C47 C48 139.6(9) . . . . ? Ce2 C11 C47 C48 54.4(9) . . . . ? C67 C25 C48 C47 0.1(12) . . . . ? C39 C25 C48 C47 140.5(9) . . . . ? C67 C25 C48 C3 -151.5(8) . . . . ? C39 C25 C48 C3 -11.1(12) . . . . ? C51 C47 C48 C25 0.5(11) . . . . ? C11 C47 C48 C25 -149.8(9) . . . . ? C51 C47 C48 C3 151.4(8) . . . . ? C11 C47 C48 C3 1.2(13) . . . . ? C20 C3 C48 C25 12.9(11) . . . . ? C55 C3 C48 C25 155.8(8) . . . . ? Ce2 C3 C48 C25 99.4(7) . . . . ? C20 C3 C48 C47 -139.8(9) . . . . ? C55 C3 C48 C47 3.1(13) . . . . ? Ce2 C3 C48 C47 -53.3(8) . . . . ? C42 C44 C49 C69 -152.2(8) . . . . ? C9 C44 C49 C69 -0.2(13) . . . . ? C42 C44 C49 C78 -7.9(14) . . . . ? C9 C44 C49 C78 144.0(9) . . . . ? C42 C44 C49 Ce3 -84.7(9) . . . . ? C9 C44 C49 Ce3 67.2(9) . . . . ? C48 C47 C51 C21 -141.8(9) . . . . ? C11 C47 C51 C21 9.5(14) . . . . ? C48 C47 C51 C66 -0.3(11) . . . . ? C11 C47 C51 C66 151.0(8) . . . . ? C38 C21 C51 C47 143.4(9) . . . . ? C60 C21 C51 C47 -1.3(14) . . . . ? C38 C21 C51 C66 -2.7(10) . . . . ? C60 C21 C51 C66 -147.3(8) . . . . ? C37 C45 C52 C13 7.6(11) . . . . ? C67 C45 C52 C13 150.2(8) . . . . ? C37 C45 C52 C53 -144.3(8) . . . . ? C67 C45 C52 C53 -1.7(11) . . . . ? C61 C13 C52 C45 -11.5(11) . . . . ? C36 C13 C52 C45 -157.4(7) . . . . ? Ce1 C13 C52 C45 -96.2(7) . . . . ? C61 C13 C52 C53 140.1(8) . . . . ? C36 C13 C52 C53 -5.9(12) . . . . ? Ce1 C13 C52 C53 55.4(8) . . . . ? C45 C52 C53 C59 2.8(11) . . . . ? C13 C52 C53 C59 -148.1(8) . . . . ? C45 C52 C53 C41 148.9(8) . . . . ? C13 C52 C53 C41 -1.9(12) . . . . ? C16 C41 C53 C59 156.1(9) . . . . ? C35 C41 C53 C59 8.2(12) . . . . ? Ce1 C41 C53 C59 96.3(8) . . . . ? C16 C41 C53 C52 8.9(13) . . . . ? C35 C41 C53 C52 -139.0(9) . . . . ? Ce1 C41 C53 C52 -50.8(8) . . . . ? C88 C81 C92 C94 1.8(12) . . . . ? C86 C81 C92 C94 177.3(8) . . . . ? C69 C10 C54 C8 0.8(13) . . . . ? C7 C10 C54 C8 146.0(8) . . . . ? Ce3 C10 C54 C8 43.2(8) . . . . ? C69 C10 C54 C4 -147.2(8) . . . . ? C7 C10 C54 C4 -1.9(8) . . . . ? Ce3 C10 C54 C4 -104.7(6) . . . . ? C69 C10 C54 Ce3 -42.4(8) . . . . ? C7 C10 C54 Ce3 102.8(7) . . . . ? C33 C8 C54 C10 -151.5(8) . . . . ? C15 C8 C54 C10 -0.4(12) . . . . ? Ce3 C8 C54 C10 -49.6(9) . . . . ? C33 C8 C54 C4 -7.5(11) . . . . ? C15 C8 C54 C4 143.6(7) . . . . ? Ce3 C8 C54 C4 94.4(8) . . . . ? C33 C8 C54 Ce3 -101.9(8) . . . . ? C15 C8 C54 Ce3 49.2(7) . . . . ? C58 C4 C54 C10 148.1(7) . . . . ? C17 C4 C54 C10 -10.2(8) . . . . ? C58 C4 C54 C8 -0.9(11) . . . . ? C17 C4 C54 C8 -159.2(7) . . . . ? C58 C4 C54 Ce3 65.9(9) . . . . ? C17 C4 C54 Ce3 -92.5(7) . . . . ? C20 C3 C55 C57 2.5(10) . . . . ? C48 C3 C55 C57 -144.7(9) . . . . ? Ce2 C3 C55 C57 -72.7(6) . . . . ? C20 C3 C55 C75 143.4(8) . . . . ? C48 C3 C55 C75 -3.9(13) . . . . ? Ce2 C3 C55 C75 68.1(7) . . . . ? C20 C3 C55 Ce2 75.3(7) . . . . ? C48 C3 C55 Ce2 -72.0(8) . . . . ? C64 Ce2 C55 C57 -102.5(7) . . . . ? C14 Ce2 C55 C57 -66.2(6) . . . . ? C75 Ce2 C55 C57 -132.0(9) . . . . ? C12 Ce2 C55 C57 -31.0(6) . . . . ? C2 Ce2 C55 C57 -62.3(6) . . . . ? C5 Ce2 C55 C57 -14.1(6) . . . . ? C42 Ce2 C55 C57 -121.8(6) . . . . ? C11 Ce2 C55 C57 -164.6(8) . . . . ? C32 Ce2 C55 C57 37.5(6) . . . . ? C3 Ce2 C55 C57 109.4(9) . . . . ? C64 Ce2 C55 C75 29.6(6) . . . . ? C14 Ce2 C55 C75 65.9(6) . . . . ? C12 Ce2 C55 C75 101.0(7) . . . . ? C57 Ce2 C55 C75 132.0(9) . . . . ? C2 Ce2 C55 C75 69.7(6) . . . . ? C5 Ce2 C55 C75 117.9(6) . . . . ? C42 Ce2 C55 C75 10.2(6) . . . . ? C11 Ce2 C55 C75 -32.5(5) . . . . ? C32 Ce2 C55 C75 169.6(7) . . . . ? C3 Ce2 C55 C75 -118.6(8) . . . . ? C64 Ce2 C55 C3 148.2(7) . . . . ? C14 Ce2 C55 C3 -175.5(7) . . . . ? C75 Ce2 C55 C3 118.6(8) . . . . ? C12 Ce2 C55 C3 -140.4(7) . . . . ? C57 Ce2 C55 C3 -109.4(9) . . . . ? C2 Ce2 C55 C3 -171.7(6) . . . . ? C5 Ce2 C55 C3 -123.5(6) . . . . ? C42 Ce2 C55 C3 128.8(6) . . . . ? C11 Ce2 C55 C3 86.1(6) . . . . ? C32 Ce2 C55 C3 -71.8(6) . . . . ? C3 C20 C56 C72 148.1(9) . . . . ? C32 C20 C56 C72 0.1(13) . . . . ? Ce4 C20 C56 C72 49.3(8) . . . . ? C3 C20 C56 C39 -1.4(12) . . . . ? C32 C20 C56 C39 -149.4(8) . . . . ? Ce4 C20 C56 C39 -100.2(8) . . . . ? C3 C20 C56 Ce4 98.8(9) . . . . ? C32 C20 C56 Ce4 -49.2(8) . . . . ? C37 C39 C56 C72 -4.4(13) . . . . ? C25 C39 C56 C72 -146.4(8) . . . . ? C37 C39 C56 C20 145.6(8) . . . . ? C25 C39 C56 C20 3.6(11) . . . . ? C37 C39 C56 Ce4 63.7(10) . . . . ? C25 C39 C56 Ce4 -78.3(9) . . . . ? C75 C55 C57 C12 2.4(14) . . . . ? C3 C55 C57 C12 140.6(9) . . . . ? Ce2 C55 C57 C12 58.3(8) . . . . ? C75 C55 C57 C32 -136.8(10) . . . . ? C3 C55 C57 C32 1.4(10) . . . . ? Ce2 C55 C57 C32 -80.9(6) . . . . ? C75 C55 C57 Ce2 -55.9(9) . . . . ? C3 C55 C57 Ce2 82.3(7) . . . . ? C14 C12 C57 C55 -2.6(14) . . . . ? C5 C12 C57 C55 -135.0(10) . . . . ? Ce2 C12 C57 C55 -59.4(8) . . . . ? C14 C12 C57 C32 133.0(10) . . . . ? C5 C12 C57 C32 0.6(12) . . . . ? Ce2 C12 C57 C32 76.2(8) . . . . ? C14 C12 C57 Ce2 56.7(8) . . . . ? C5 C12 C57 Ce2 -75.6(7) . . . . ? C18 C32 C57 C55 144.8(9) . . . . ? C20 C32 C57 C55 -4.6(10) . . . . ? Ce4 C32 C57 C55 77.8(9) . . . . ? Ce2 C32 C57 C55 71.4(7) . . . . ? C18 C32 C57 C12 6.1(14) . . . . ? C20 C32 C57 C12 -143.3(8) . . . . ? Ce4 C32 C57 C12 -60.9(11) . . . . ? Ce2 C32 C57 C12 -67.2(7) . . . . ? C18 C32 C57 Ce2 73.3(9) . . . . ? C20 C32 C57 Ce2 -76.1(6) . . . . ? Ce4 C32 C57 Ce2 6.3(6) . . . . ? C64 Ce2 C57 C55 63.1(6) . . . . ? C14 Ce2 C57 C55 99.2(7) . . . . ? C75 Ce2 C57 C55 28.2(6) . . . . ? C12 Ce2 C57 C55 127.1(9) . . . . ? C2 Ce2 C57 C55 119.0(6) . . . . ? C5 Ce2 C57 C55 162.8(8) . . . . ? C42 Ce2 C57 C55 59.7(6) . . . . ? C11 Ce2 C57 C55 12.6(6) . . . . ? C32 Ce2 C57 C55 -111.5(8) . . . . ? C3 Ce2 C57 C55 -39.1(6) . . . . ? C64 Ce2 C57 C12 -64.1(6) . . . . ? C14 Ce2 C57 C12 -27.9(5) . . . . ? C75 Ce2 C57 C12 -99.0(7) . . . . ? C55 Ce2 C57 C12 -127.1(9) . . . . ? C2 Ce2 C57 C12 -8.2(6) . . . . ? C5 Ce2 C57 C12 35.7(5) . . . . ? C42 Ce2 C57 C12 -67.4(6) . . . . ? C11 Ce2 C57 C12 -114.6(6) . . . . ? C32 Ce2 C57 C12 121.3(8) . . . . ? C3 Ce2 C57 C12 -166.3(8) . . . . ? C64 Ce2 C57 C32 174.6(6) . . . . ? C14 Ce2 C57 C32 -149.3(6) . . . . ? C75 Ce2 C57 C32 139.7(6) . . . . ? C12 Ce2 C57 C32 -121.3(8) . . . . ? C55 Ce2 C57 C32 111.5(8) . . . . ? C2 Ce2 C57 C32 -129.5(5) . . . . ? C5 Ce2 C57 C32 -85.7(6) . . . . ? C42 Ce2 C57 C32 171.2(5) . . . . ? C11 Ce2 C57 C32 124.1(6) . . . . ? C3 Ce2 C57 C32 72.4(6) . . . . ? C81 C92 C94 C106 -1.2(13) . . . . ? C81 C92 C94 C112 -179.1(8) . . . . ? C54 C4 C58 C62 3.2(10) . . . . ? C17 C4 C58 C62 158.8(6) . . . . ? C54 C4 C58 C28 -159.0(7) . . . . ? C17 C4 C58 C28 -3.4(10) . . . . ? C29 C28 C58 C4 28.9(9) . . . . ? C24 C28 C58 C4 138.1(7) . . . . ? Si1 C28 C58 C4 -81.4(8) . . . . ? C29 C28 C58 C62 -132.4(7) . . . . ? C24 C28 C58 C62 -23.1(10) . . . . ? Si1 C28 C58 C62 117.4(7) . . . . ? C52 C53 C59 C66 -2.3(12) . . . . ? C41 C53 C59 C66 -148.5(8) . . . . ? C52 C53 C59 C38 141.0(9) . . . . ? C41 C53 C59 C38 -5.2(13) . . . . ? C21 C38 C59 C53 -145.7(9) . . . . ? C40 C38 C59 C53 -0.5(14) . . . . ? C21 C38 C59 C66 2.9(9) . . . . ? C40 C38 C59 C66 148.1(8) . . . . ? C96 Si2 C95 Si1 -95.3(9) . . . . ? C111 Si2 C95 Si1 147.8(9) . . . . ? C17 Si2 C95 Si1 18.9(10) . . . . ? C88 Si1 C95 Si2 -117.4(9) . . . . ? C87 Si1 C95 Si2 124.6(9) . . . . ? C28 Si1 C95 Si2 -4.2(10) . . . . ? C42 C6 C60 C78 -2.2(14) . . . . ? C11 C6 C60 C78 -150.0(9) . . . . ? Ce2 C6 C60 C78 -75.5(9) . . . . ? C42 C6 C60 C21 150.5(9) . . . . ? C11 C6 C60 C21 2.8(14) . . . . ? Ce2 C6 C60 C21 77.2(9) . . . . ? C38 C21 C60 C6 -146.5(10) . . . . ? C51 C21 C60 C6 -5.0(13) . . . . ? C38 C21 C60 C78 6.2(14) . . . . ? C51 C21 C60 C78 147.6(9) . . . . ? C34 C23 C61 C65 -156.9(9) . . . . ? C46 C23 C61 C65 -5.8(14) . . . . ? Ce1 C23 C61 C65 -95.0(9) . . . . ? C34 C23 C61 C13 -7.2(10) . . . . ? C46 C23 C61 C13 143.9(8) . . . . ? Ce1 C23 C61 C13 54.8(6) . . . . ? C34 C23 C61 Ce1 -62.0(6) . . . . ? C46 C23 C61 Ce1 89.2(8) . . . . ? C52 C13 C61 C23 -144.4(8) . . . . ? C36 C13 C61 C23 5.0(10) . . . . ? Ce1 C13 C61 C23 -53.6(6) . . . . ? C52 C13 C61 C65 6.9(12) . . . . ? C36 C13 C61 C65 156.4(8) . . . . ? Ce1 C13 C61 C65 97.8(7) . . . . ? C52 C13 C61 Ce1 -90.8(7) . . . . ? C36 C13 C61 Ce1 58.6(6) . . . . ? C43 Ce1 C61 C23 45.0(7) . . . . ? C74 Ce1 C61 C23 26.4(6) . . . . ? C34 Ce1 C61 C23 38.8(6) . . . . ? C36 Ce1 C61 C23 85.6(7) . . . . ? C22 Ce1 C61 C23 80.2(6) . . . . ? C16 Ce1 C61 C23 98.0(6) . . . . ? C1 Ce1 C61 C23 -4.5(6) . . . . ? C33 Ce1 C61 C23 21.9(7) . . . . ? C13 Ce1 C61 C23 123.2(9) . . . . ? C41 Ce1 C61 C23 126.5(6) . . . . ? C63 Ce1 C61 C23 103.3(6) . . . . ? C43 Ce1 C61 C65 165.7(6) . . . . ? C74 Ce1 C61 C65 147.1(7) . . . . ? C34 Ce1 C61 C65 159.5(8) . . . . ? C36 Ce1 C61 C65 -153.7(8) . . . . ? C22 Ce1 C61 C65 -159.1(6) . . . . ? C16 Ce1 C61 C65 -141.3(7) . . . . ? C23 Ce1 C61 C65 120.7(10) . . . . ? C1 Ce1 C61 C65 116.2(7) . . . . ? C33 Ce1 C61 C65 142.6(6) . . . . ? C13 Ce1 C61 C65 -116.1(9) . . . . ? C41 Ce1 C61 C65 -112.8(7) . . . . ? C63 Ce1 C61 C65 -136.0(6) . . . . ? C43 Ce1 C61 C13 -78.3(6) . . . . ? C74 Ce1 C61 C13 -96.9(6) . . . . ? C34 Ce1 C61 C13 -84.5(6) . . . . ? C36 Ce1 C61 C13 -37.6(6) . . . . ? C22 Ce1 C61 C13 -43.1(6) . . . . ? C16 Ce1 C61 C13 -25.2(6) . . . . ? C23 Ce1 C61 C13 -123.2(9) . . . . ? C1 Ce1 C61 C13 -127.7(6) . . . . ? C33 Ce1 C61 C13 -101.3(6) . . . . ? C41 Ce1 C61 C13 3.2(6) . . . . ? C63 Ce1 C61 C13 -19.9(7) . . . . ? C4 C58 C62 C1 -153.2(7) . . . . ? C28 C58 C62 C1 9.1(12) . . . . ? C4 C58 C62 C33 3.2(11) . . . . ? C28 C58 C62 C33 165.4(7) . . . . ? C4 C58 C62 Ce1 -76.1(7) . . . . ? C28 C58 C62 Ce1 86.2(7) . . . . ? C30 C1 C62 C58 12.1(12) . . . . ? C74 C1 C62 C58 161.2(7) . . . . ? Ce1 C1 C62 C58 100.9(7) . . . . ? C30 C1 C62 C33 -147.5(7) . . . . ? C74 C1 C62 C33 1.6(10) . . . . ? Ce1 C1 C62 C33 -58.7(6) . . . . ? C30 C1 C62 Ce1 -88.8(7) . . . . ? C74 C1 C62 Ce1 60.3(6) . . . . ? C43 C33 C62 C58 -159.1(7) . . . . ? C8 C33 C62 C58 -11.5(12) . . . . ? Ce1 C33 C62 C58 -101.4(7) . . . . ? C43 C33 C62 C1 0.2(10) . . . . ? C8 C33 C62 C1 147.7(7) . . . . ? Ce1 C33 C62 C1 57.8(6) . . . . ? C43 C33 C62 Ce1 -57.6(6) . . . . ? C8 C33 C62 Ce1 89.9(6) . . . . ? C43 Ce1 C62 C58 157.7(8) . . . . ? C74 Ce1 C62 C58 -158.3(8) . . . . ? C34 Ce1 C62 C58 -143.4(7) . . . . ? C36 Ce1 C62 C58 -164.8(6) . . . . ? C22 Ce1 C62 C58 143.9(7) . . . . ? C16 Ce1 C62 C58 160.9(6) . . . . ? C23 Ce1 C62 C58 -114.0(6) . . . . ? C1 Ce1 C62 C58 -118.8(9) . . . . ? C33 Ce1 C62 C58 120.7(9) . . . . ? C13 Ce1 C62 C58 -139.6(6) . . . . ? C41 Ce1 C62 C58 136.6(6) . . . . ? C63 Ce1 C62 C58 115.4(6) . . . . ? C43 Ce1 C62 C1 -83.5(6) . . . . ? C74 Ce1 C62 C1 -39.5(6) . . . . ? C34 Ce1 C62 C1 -24.6(5) . . . . ? C36 Ce1 C62 C1 -46.0(6) . . . . ? C22 Ce1 C62 C1 -97.3(6) . . . . ? C16 Ce1 C62 C1 -80.3(6) . . . . ? C23 Ce1 C62 C1 4.8(5) . . . . ? C33 Ce1 C62 C1 -120.5(8) . . . . ? C13 Ce1 C62 C1 -20.8(7) . . . . ? C41 Ce1 C62 C1 -104.6(6) . . . . ? C63 Ce1 C62 C1 -125.8(6) . . . . ? C43 Ce1 C62 C33 37.0(6) . . . . ? C74 Ce1 C62 C33 81.0(6) . . . . ? C34 Ce1 C62 C33 95.9(6) . . . . ? C36 Ce1 C62 C33 74.5(6) . . . . ? C22 Ce1 C62 C33 23.2(6) . . . . ? C16 Ce1 C62 C33 40.2(6) . . . . ? C23 Ce1 C62 C33 125.3(6) . . . . ? C1 Ce1 C62 C33 120.5(8) . . . . ? C13 Ce1 C62 C33 99.7(6) . . . . ? C41 Ce1 C62 C33 15.9(7) . . . . ? C63 Ce1 C62 C33 -5.3(6) . . . . ? C43 C22 C63 C35 -140.6(9) . . . . ? C16 C22 C63 C35 -1.4(11) . . . . ? Ce1 C22 C63 C35 -73.7(7) . . . . ? C43 C22 C63 C15 4.4(14) . . . . ? C16 C22 C63 C15 143.6(9) . . . . ? Ce1 C22 C63 C15 71.4(9) . . . . ? C43 C22 C63 Ce3 -61.1(10) . . . . ? C16 C22 C63 Ce3 78.1(9) . . . . ? Ce1 C22 C63 Ce3 5.9(6) . . . . ? C43 C22 C63 Ce1 -67.0(7) . . . . ? C16 C22 C63 Ce1 72.2(6) . . . . ? C40 C35 C63 C22 157.1(9) . . . . ? C41 C35 C63 C22 3.0(11) . . . . ? Ce3 C35 C63 C22 103.9(9) . . . . ? C40 C35 C63 C15 8.7(14) . . . . ? C41 C35 C63 C15 -145.4(8) . . . . ? Ce3 C35 C63 C15 -44.6(9) . . . . ? C40 C35 C63 Ce3 53.3(11) . . . . ? C41 C35 C63 Ce3 -100.9(8) . . . . ? C40 C35 C63 Ce1 98.6(9) . . . . ? C41 C35 C63 Ce1 -55.5(7) . . . . ? Ce3 C35 C63 Ce1 45.3(5) . . . . ? C68 C15 C63 C22 -157.1(9) . . . . ? C8 C15 C63 C22 -2.8(13) . . . . ? Ce3 C15 C63 C22 -92.1(10) . . . . ? C68 C15 C63 C35 -13.7(12) . . . . ? C8 C15 C63 C35 140.6(9) . . . . ? Ce3 C15 C63 C35 51.3(9) . . . . ? C68 C15 C63 Ce3 -65.1(9) . . . . ? C8 C15 C63 Ce3 89.3(9) . . . . ? C68 C15 C63 Ce1 -99.9(8) . . . . ? C8 C15 C63 Ce1 54.4(8) . . . . ? Ce3 C15 C63 Ce1 -34.9(6) . . . . ? C43 Ce1 C63 C22 35.5(5) . . . . ? C74 Ce1 C63 C22 25.2(6) . . . . ? C34 Ce1 C63 C22 -6.9(6) . . . . ? C36 Ce1 C63 C22 -36.2(5) . . . . ? C16 Ce1 C63 C22 -43.0(6) . . . . ? C23 Ce1 C63 C22 -13.4(7) . . . . ? C1 Ce1 C63 C22 51.2(6) . . . . ? C33 Ce1 C63 C22 72.0(6) . . . . ? C13 Ce1 C63 C22 -59.6(6) . . . . ? C41 Ce1 C63 C22 -82.6(6) . . . . ? C43 Ce1 C63 C35 151.1(8) . . . . ? C74 Ce1 C63 C35 140.8(6) . . . . ? C34 Ce1 C63 C35 108.7(6) . . . . ? C36 Ce1 C63 C35 79.4(6) . . . . ? C22 Ce1 C63 C35 115.6(9) . . . . ? C16 Ce1 C63 C35 72.6(6) . . . . ? C23 Ce1 C63 C35 102.2(7) . . . . ? C1 Ce1 C63 C35 166.8(6) . . . . ? C33 Ce1 C63 C35 -172.4(7) . . . . ? C13 Ce1 C63 C35 56.0(7) . . . . ? C41 Ce1 C63 C35 33.0(6) . . . . ? C43 Ce1 C63 C15 -93.3(6) . . . . ? C74 Ce1 C63 C15 -103.5(6) . . . . ? C34 Ce1 C63 C15 -135.7(6) . . . . ? C36 Ce1 C63 C15 -165.0(6) . . . . ? C22 Ce1 C63 C15 -128.8(9) . . . . ? C16 Ce1 C63 C15 -171.8(8) . . . . ? C23 Ce1 C63 C15 -142.1(6) . . . . ? C1 Ce1 C63 C15 -77.6(6) . . . . ? C33 Ce1 C63 C15 -56.8(6) . . . . ? C13 Ce1 C63 C15 171.7(6) . . . . ? C41 Ce1 C63 C15 148.6(8) . . . . ? C43 Ce1 C63 Ce3 -136.8(6) . . . . ? C74 Ce1 C63 Ce3 -147.0(5) . . . . ? C34 Ce1 C63 Ce3 -179.2(5) . . . . ? C36 Ce1 C63 Ce3 151.5(5) . . . . ? C22 Ce1 C63 Ce3 -172.3(8) . . . . ? C16 Ce1 C63 Ce3 144.7(6) . . . . ? C23 Ce1 C63 Ce3 174.4(5) . . . . ? C1 Ce1 C63 Ce3 -121.1(5) . . . . ? C33 Ce1 C63 Ce3 -100.3(6) . . . . ? C13 Ce1 C63 Ce3 128.2(5) . . . . ? C41 Ce1 C63 Ce3 105.1(6) . . . . ? C6 C42 C64 C75 2.9(11) . . . . ? C44 C42 C64 C75 -142.2(9) . . . . ? Ce2 C42 C64 C75 -71.6(7) . . . . ? C6 C42 C64 C14 143.0(9) . . . . ? C44 C42 C64 C14 -2.1(14) . . . . ? Ce2 C42 C64 C14 68.5(7) . . . . ? C6 C42 C64 Ce2 74.4(7) . . . . ? C44 C42 C64 Ce2 -70.6(9) . . . . ? C2 C14 C64 C75 134.7(10) . . . . ? C12 C14 C64 C75 -1.2(14) . . . . ? Ce2 C14 C64 C75 59.8(8) . . . . ? C2 C14 C64 C42 -1.5(13) . . . . ? C12 C14 C64 C42 -137.3(9) . . . . ? Ce2 C14 C64 C42 -76.4(8) . . . . ? C2 C14 C64 Ce2 74.9(8) . . . . ? C12 C14 C64 Ce2 -61.0(8) . . . . ? C14 Ce2 C64 C75 -128.2(10) . . . . ? C12 Ce2 C64 C75 -97.2(7) . . . . ? C55 Ce2 C64 C75 -29.1(6) . . . . ? C57 Ce2 C64 C75 -62.5(7) . . . . ? C2 Ce2 C64 C75 -159.3(8) . . . . ? C5 Ce2 C64 C75 -116.9(7) . . . . ? C42 Ce2 C64 C75 111.1(8) . . . . ? C11 Ce2 C64 C75 38.1(6) . . . . ? C32 Ce2 C64 C75 -59.7(7) . . . . ? C3 Ce2 C64 C75 -13.2(7) . . . . ? C14 Ce2 C64 C42 120.7(8) . . . . ? C75 Ce2 C64 C42 -111.1(8) . . . . ? C12 Ce2 C64 C42 151.7(6) . . . . ? C55 Ce2 C64 C42 -140.2(6) . . . . ? C57 Ce2 C64 C42 -173.6(6) . . . . ? C2 Ce2 C64 C42 89.6(6) . . . . ? C5 Ce2 C64 C42 132.0(5) . . . . ? C11 Ce2 C64 C42 -73.0(6) . . . . ? C32 Ce2 C64 C42 -170.8(5) . . . . ? C3 Ce2 C64 C42 -124.4(5) . . . . ? C75 Ce2 C64 C14 128.2(10) . . . . ? C12 Ce2 C64 C14 31.0(5) . . . . ? C55 Ce2 C64 C14 99.1(6) . . . . ? C57 Ce2 C64 C14 65.7(6) . . . . ? C2 Ce2 C64 C14 -31.1(5) . . . . ? C5 Ce2 C64 C14 11.3(6) . . . . ? C42 Ce2 C64 C14 -120.7(8) . . . . ? C11 Ce2 C64 C14 166.3(7) . . . . ? C32 Ce2 C64 C14 68.5(6) . . . . ? C3 Ce2 C64 C14 115.0(6) . . . . ? C109 C82 C96 C99 -1.1(13) . . . . ? C79 C82 C96 C99 179.9(9) . . . . ? C109 C82 C96 Si2 178.8(7) . . . . ? C79 C82 C96 Si2 -0.2(12) . . . . ? C95 Si2 C96 C99 13.9(9) . . . . ? C111 Si2 C96 C99 126.7(8) . . . . ? C17 Si2 C96 C99 -99.3(8) . . . . ? C95 Si2 C96 C82 -166.0(6) . . . . ? C111 Si2 C96 C82 -53.2(8) . . . . ? C17 Si2 C96 C82 80.8(7) . . . . ? C72 C27 C65 C61 147.1(8) . . . . ? C77 C27 C65 C61 5.9(13) . . . . ? Ce4 C27 C65 C61 90.1(9) . . . . ? C72 C27 C65 C37 -3.9(12) . . . . ? C77 C27 C65 C37 -145.1(8) . . . . ? Ce4 C27 C65 C37 -60.9(8) . . . . ? C23 C61 C65 C27 -3.3(14) . . . . ? C13 C61 C65 C27 -149.8(8) . . . . ? Ce1 C61 C65 C27 -75.7(9) . . . . ? C23 C61 C65 C37 148.4(9) . . . . ? C13 C61 C65 C37 1.9(11) . . . . ? Ce1 C61 C65 C37 76.0(7) . . . . ? C45 C37 C65 C27 145.1(9) . . . . ? C39 C37 C65 C27 4.1(12) . . . . ? C45 C37 C65 C61 -5.8(12) . . . . ? C39 C37 C65 C61 -146.8(8) . . . . ? C108 C90 C97 C87 -6.8(14) . . . . ? C108 C90 C97 C91 174.3(10) . . . . ? C84 C87 C97 C90 6.8(14) . . . . ? Si1 C87 C97 C90 -171.2(7) . . . . ? C84 C87 C97 C91 -174.4(10) . . . . ? Si1 C87 C97 C91 7.6(12) . . . . ? C82 C96 C99 C110 2.3(13) . . . . ? Si2 C96 C99 C110 -177.6(7) . . . . ? C82 C96 C99 C80 -179.9(8) . . . . ? Si2 C96 C99 C80 0.2(13) . . . . ? C47 C51 C66 C67 -0.5(12) . . . . ? C21 C51 C66 C67 147.6(8) . . . . ? C47 C51 C66 C59 -143.7(8) . . . . ? C21 C51 C66 C59 4.5(9) . . . . ? C53 C59 C66 C67 0.7(12) . . . . ? C38 C59 C66 C67 -148.8(8) . . . . ? C53 C59 C66 C51 144.9(8) . . . . ? C38 C59 C66 C51 -4.6(9) . . . . ? C51 C66 C67 C45 -139.7(9) . . . . ? C59 C66 C67 C45 0.5(12) . . . . ? C51 C66 C67 C25 1.1(12) . . . . ? C59 C66 C67 C25 141.3(8) . . . . ? C37 C45 C67 C66 147.4(8) . . . . ? C52 C45 C67 C66 0.1(12) . . . . ? C37 C45 C67 C25 4.0(9) . . . . ? C52 C45 C67 C25 -143.3(8) . . . . ? C48 C25 C67 C66 -0.9(12) . . . . ? C39 C25 C67 C66 -149.0(7) . . . . ? C48 C25 C67 C45 143.6(8) . . . . ? C39 C25 C67 C45 -4.5(8) . . . . ? C8 C15 C68 C76 -141.5(9) . . . . ? C63 C15 C68 C76 11.2(13) . . . . ? Ce3 C15 C68 C76 -59.6(9) . . . . ? C8 C15 C68 C69 -2.8(13) . . . . ? C63 C15 C68 C69 149.9(8) . . . . ? Ce3 C15 C68 C69 79.0(9) . . . . ? C8 C15 C68 Ce3 -81.8(9) . . . . ? C63 C15 C68 Ce3 70.8(8) . . . . ? C83 C89 C100 C111 -4.3(17) . . . . ? C83 C89 C100 C113 175.6(11) . . . . ? C54 C10 C69 C49 138.8(9) . . . . ? C7 C10 C69 C49 -4.2(12) . . . . ? Ce3 C10 C69 C49 90.2(9) . . . . ? C54 C10 C69 C68 -2.1(12) . . . . ? C7 C10 C69 C68 -145.2(8) . . . . ? Ce3 C10 C69 C68 -50.7(8) . . . . ? C54 C10 C69 Ce3 48.6(9) . . . . ? C7 C10 C69 Ce3 -94.5(9) . . . . ? C44 C49 C69 C10 0.8(13) . . . . ? C78 C49 C69 C10 -148.6(8) . . . . ? Ce3 C49 C69 C10 -91.8(8) . . . . ? C44 C49 C69 C68 145.2(9) . . . . ? C78 C49 C69 C68 -4.2(10) . . . . ? Ce3 C49 C69 C68 52.6(7) . . . . ? C44 C49 C69 Ce3 92.6(9) . . . . ? C78 C49 C69 Ce3 -56.8(8) . . . . ? C76 C68 C69 C10 145.9(8) . . . . ? C15 C68 C69 C10 3.1(13) . . . . ? Ce3 C68 C69 C10 69.8(10) . . . . ? C76 C68 C69 C49 1.5(11) . . . . ? C15 C68 C69 C49 -141.2(9) . . . . ? Ce3 C68 C69 C49 -74.5(9) . . . . ? C76 C68 C69 Ce3 76.1(8) . . . . ? C15 C68 C69 Ce3 -66.7(9) . . . . ? C30 C24 C70 C50 7.7(13) . . . . ? C28 C24 C70 C50 156.3(7) . . . . ? C30 C24 C70 C26 -137.8(8) . . . . ? C28 C24 C70 C26 10.7(9) . . . . ? C30 C24 C70 Ce4 -56.2(10) . . . . ? C28 C24 C70 Ce4 92.4(7) . . . . ? C77 C50 C70 C24 -3.6(13) . . . . ? C73 C50 C70 C24 -144.5(9) . . . . ? Ce4 C50 C70 C24 -94.5(9) . . . . ? C77 C50 C70 C26 139.5(9) . . . . ? C73 C50 C70 C26 -1.3(12) . . . . ? Ce4 C50 C70 C26 48.7(9) . . . . ? C77 C50 C70 Ce4 90.8(9) . . . . ? C73 C50 C70 Ce4 -50.0(8) . . . . ? C71 C26 C70 C24 148.1(8) . . . . ? C29 C26 C70 C24 -1.1(9) . . . . ? Ce4 C26 C70 C24 105.2(7) . . . . ? C71 C26 C70 C50 1.6(12) . . . . ? C29 C26 C70 C50 -147.6(8) . . . . ? Ce4 C26 C70 C50 -41.3(7) . . . . ? C71 C26 C70 Ce4 42.9(8) . . . . ? C29 C26 C70 Ce4 -106.3(6) . . . . ? C89 C83 C102 C103 -1.4(18) . . . . ? C114 C83 C102 C103 178.9(11) . . . . ? C83 C102 C103 C111 -0.7(19) . . . . ? C83 C102 C103 C107 -177.6(11) . . . . ? C87 C84 C105 C108 2.2(15) . . . . ? C98 C84 C105 C108 -179.9(9) . . . . ? C29 C26 C71 C5 -7.8(12) . . . . ? C70 C26 C71 C5 -151.8(8) . . . . ? Ce4 C26 C71 C5 -104.0(8) . . . . ? C29 C26 C71 C18 143.4(8) . . . . ? C70 C26 C71 C18 -0.6(13) . . . . ? Ce4 C26 C71 C18 47.2(7) . . . . ? C29 C26 C71 Ce4 96.2(8) . . . . ? C70 C26 C71 Ce4 -47.8(8) . . . . ? C31 C5 C71 C26 11.3(12) . . . . ? C12 C5 C71 C26 156.7(8) . . . . ? Ce2 C5 C71 C26 95.4(7) . . . . ? C31 C5 C71 C18 -139.9(9) . . . . ? C12 C5 C71 C18 5.5(14) . . . . ? Ce2 C5 C71 C18 -55.8(8) . . . . ? C31 C5 C71 Ce4 -83.1(9) . . . . ? C12 C5 C71 Ce4 62.3(10) . . . . ? Ce2 C5 C71 Ce4 1.0(6) . . . . ? C73 C18 C71 C26 -0.7(13) . . . . ? C32 C18 C71 C26 -148.8(8) . . . . ? Ce4 C18 C71 C26 -64.0(9) . . . . ? C73 C18 C71 C5 149.3(9) . . . . ? C32 C18 C71 C5 1.2(13) . . . . ? Ce4 C18 C71 C5 86.1(10) . . . . ? C73 C18 C71 Ce4 63.2(9) . . . . ? C32 C18 C71 Ce4 -84.8(9) . . . . ? C20 C56 C72 C27 -143.2(9) . . . . ? C39 C56 C72 C27 4.7(12) . . . . ? Ce4 C56 C72 C27 -88.1(9) . . . . ? C20 C56 C72 C73 -3.8(13) . . . . ? C39 C56 C72 C73 144.1(9) . . . . ? Ce4 C56 C72 C73 51.4(8) . . . . ? C20 C56 C72 Ce4 -55.2(9) . . . . ? C39 C56 C72 Ce4 92.7(9) . . . . ? C65 C27 C72 C56 -0.6(13) . . . . ? C77 C27 C72 C56 145.4(8) . . . . ? Ce4 C27 C72 C56 81.7(9) . . . . ? C65 C27 C72 C73 -142.9(8) . . . . ? C77 C27 C72 C73 3.1(11) . . . . ? Ce4 C27 C72 C73 -60.6(7) . . . . ? C65 C27 C72 Ce4 -82.4(9) . . . . ? C77 C27 C72 Ce4 63.7(8) . . . . ? C92 C94 C106 C85 2.4(14) . . . . ? C112 C94 C106 C85 -179.9(9) . . . . ? C88 C85 C106 C94 -3.9(14) . . . . ? C93 C85 C106 C94 175.3(9) . . . . ? C32 C18 C73 C72 7.4(14) . . . . ? C71 C18 C73 C72 -140.8(9) . . . . ? Ce4 C18 C73 C72 -63.7(10) . . . . ? C32 C18 C73 C50 149.1(8) . . . . ? C71 C18 C73 C50 1.0(14) . . . . ? Ce4 C18 C73 C50 78.1(10) . . . . ? C32 C18 C73 Ce4 71.0(8) . . . . ? C71 C18 C73 Ce4 -77.1(9) . . . . ? C56 C72 C73 C18 0.0(14) . . . . ? C27 C72 C73 C18 142.8(10) . . . . ? Ce4 C72 C73 C18 61.4(10) . . . . ? C56 C72 C73 C50 -147.2(8) . . . . ? C27 C72 C73 C50 -4.4(10) . . . . ? Ce4 C72 C73 C50 -85.8(7) . . . . ? C56 C72 C73 Ce4 -61.4(9) . . . . ? C27 C72 C73 Ce4 81.4(9) . . . . ? C77 C50 C73 C18 -144.1(9) . . . . ? C70 C50 C73 C18 0.1(14) . . . . ? Ce4 C50 C73 C18 -70.2(10) . . . . ? C77 C50 C73 C72 4.2(10) . . . . ? C70 C50 C73 C72 148.3(8) . . . . ? Ce4 C50 C73 C72 78.1(8) . . . . ? C77 C50 C73 Ce4 -73.9(8) . . . . ? C70 C50 C73 Ce4 70.3(9) . . . . ? C33 C43 C74 C1 2.9(10) . . . . ? C22 C43 C74 C1 -138.9(9) . . . . ? Ce1 C43 C74 C1 -77.7(6) . . . . ? C33 C43 C74 C34 137.7(9) . . . . ? C22 C43 C74 C34 -4.0(15) . . . . ? Ce1 C43 C74 C34 57.2(8) . . . . ? C33 C43 C74 Ce1 80.5(7) . . . . ? C22 C43 C74 Ce1 -61.2(8) . . . . ? C62 C1 C74 C43 -2.7(10) . . . . ? C30 C1 C74 C43 143.0(9) . . . . ? Ce1 C1 C74 C43 70.1(6) . . . . ? C62 C1 C74 C34 -140.5(8) . . . . ? C30 C1 C74 C34 5.2(13) . . . . ? Ce1 C1 C74 C34 -67.7(7) . . . . ? C62 C1 C74 Ce1 -72.8(6) . . . . ? C30 C1 C74 Ce1 72.9(9) . . . . ? C23 C34 C74 C43 -130.1(10) . . . . ? C36 C34 C74 C43 3.3(13) . . . . ? Ce1 C34 C74 C43 -57.5(8) . . . . ? C23 C34 C74 C1 2.0(13) . . . . ? C36 C34 C74 C1 135.3(9) . . . . ? Ce1 C34 C74 C1 74.6(7) . . . . ? C23 C34 C74 Ce1 -72.6(8) . . . . ? C36 C34 C74 Ce1 60.7(7) . . . . ? C34 Ce1 C74 C43 130.7(8) . . . . ? C36 Ce1 C74 C43 97.8(6) . . . . ? C22 Ce1 C74 C43 29.1(5) . . . . ? C16 Ce1 C74 C43 63.8(5) . . . . ? C23 Ce1 C74 C43 160.9(6) . . . . ? C1 Ce1 C74 C43 -110.9(8) . . . . ? C33 Ce1 C74 C43 -37.5(5) . . . . ? C13 Ce1 C74 C43 118.1(5) . . . . ? C41 Ce1 C74 C43 59.9(5) . . . . ? C63 Ce1 C74 C43 15.2(5) . . . . ? C43 Ce1 C74 C1 110.9(8) . . . . ? C34 Ce1 C74 C1 -118.3(8) . . . . ? C36 Ce1 C74 C1 -151.3(7) . . . . ? C22 Ce1 C74 C1 140.1(6) . . . . ? C16 Ce1 C74 C1 174.8(6) . . . . ? C23 Ce1 C74 C1 -88.2(6) . . . . ? C33 Ce1 C74 C1 73.4(5) . . . . ? C13 Ce1 C74 C1 -130.9(6) . . . . ? C41 Ce1 C74 C1 170.8(5) . . . . ? C63 Ce1 C74 C1 126.1(5) . . . . ? C43 Ce1 C74 C34 -130.7(8) . . . . ? C36 Ce1 C74 C34 -32.9(5) . . . . ? C22 Ce1 C74 C34 -101.6(6) . . . . ? C16 Ce1 C74 C34 -66.9(5) . . . . ? C23 Ce1 C74 C34 30.2(5) . . . . ? C1 Ce1 C74 C34 118.3(8) . . . . ? C33 Ce1 C74 C34 -168.3(7) . . . . ? C13 Ce1 C74 C34 -12.6(6) . . . . ? C41 Ce1 C74 C34 -70.9(6) . . . . ? C63 Ce1 C74 C34 -115.5(5) . . . . ? C84 C105 C108 C90 -1.7(15) . . . . ? C84 C105 C108 C101 178.2(10) . . . . ? C97 C90 C108 C105 4.2(15) . . . . ? C97 C90 C108 C101 -175.7(10) . . . . ? C110 C104 C109 C82 4.2(16) . . . . ? C115 C104 C109 C82 179.9(9) . . . . ? C96 C82 C109 C104 -2.0(14) . . . . ? C79 C82 C109 C104 177.0(9) . . . . ? C80 C99 C110 C104 -178.3(9) . . . . ? C96 C99 C110 C104 -0.3(14) . . . . ? C109 C104 C110 C99 -3.0(16) . . . . ? C115 C104 C110 C99 -179.0(9) . . . . ? C89 C100 C111 C103 2.0(16) . . . . ? C113 C100 C111 C103 -177.9(11) . . . . ? C89 C100 C111 Si2 -174.5(8) . . . . ? C113 C100 C111 Si2 5.6(15) . . . . ? C102 C103 C111 C100 0.4(17) . . . . ? C107 C103 C111 C100 177.1(10) . . . . ? C102 C103 C111 Si2 176.5(9) . . . . ? C107 C103 C111 Si2 -6.9(17) . . . . ? C95 Si2 C111 C100 66.7(9) . . . . ? C96 Si2 C111 C100 -57.6(10) . . . . ? C17 Si2 C111 C100 179.9(7) . . . . ? C95 Si2 C111 C103 -109.4(10) . . . . ? C96 Si2 C111 C103 126.3(10) . . . . ? C17 Si2 C111 C103 3.8(13) . . . . ? C57 C55 C75 C64 -1.7(16) . . . . ? C3 C55 C75 C64 -136.8(9) . . . . ? Ce2 C55 C75 C64 -58.9(9) . . . . ? C57 C55 C75 C11 135.3(10) . . . . ? C3 C55 C75 C11 0.2(13) . . . . ? Ce2 C55 C75 C11 78.1(8) . . . . ? C57 C55 C75 Ce2 57.2(9) . . . . ? C3 C55 C75 Ce2 -77.8(7) . . . . ? C42 C64 C75 C55 140.7(10) . . . . ? C14 C64 C75 C55 1.1(15) . . . . ? Ce2 C64 C75 C55 60.4(9) . . . . ? C42 C64 C75 C11 -0.6(11) . . . . ? C14 C64 C75 C11 -140.2(9) . . . . ? Ce2 C64 C75 C11 -80.9(7) . . . . ? C42 C64 C75 Ce2 80.3(7) . . . . ? C14 C64 C75 Ce2 -59.3(8) . . . . ? C47 C11 C75 C55 4.1(14) . . . . ? C6 C11 C75 C55 -144.1(9) . . . . ? Ce2 C11 C75 C55 -71.5(8) . . . . ? C47 C11 C75 C64 146.3(9) . . . . ? C6 C11 C75 C64 -1.9(11) . . . . ? Ce2 C11 C75 C64 70.7(6) . . . . ? C47 C11 C75 Ce2 75.6(9) . . . . ? C6 C11 C75 Ce2 -72.5(7) . . . . ? C64 Ce2 C75 C55 -129.7(10) . . . . ? C14 Ce2 C75 C55 -99.0(7) . . . . ? C12 Ce2 C75 C55 -62.9(6) . . . . ? C57 Ce2 C75 C55 -27.5(5) . . . . ? C2 Ce2 C75 C55 -112.6(6) . . . . ? C5 Ce2 C75 C55 -64.2(6) . . . . ? C42 Ce2 C75 C55 -167.1(7) . . . . ? C11 Ce2 C75 C55 121.0(9) . . . . ? C32 Ce2 C75 C55 -8.1(6) . . . . ? C3 Ce2 C75 C55 34.0(5) . . . . ? C14 Ce2 C75 C64 30.7(6) . . . . ? C12 Ce2 C75 C64 66.8(6) . . . . ? C55 Ce2 C75 C64 129.7(10) . . . . ? C57 Ce2 C75 C64 102.2(7) . . . . ? C2 Ce2 C75 C64 17.1(7) . . . . ? C5 Ce2 C75 C64 65.4(7) . . . . ? C42 Ce2 C75 C64 -37.4(6) . . . . ? C11 Ce2 C75 C64 -109.4(9) . . . . ? C32 Ce2 C75 C64 121.5(7) . . . . ? C3 Ce2 C75 C64 163.7(8) . . . . ? C64 Ce2 C75 C11 109.4(9) . . . . ? C14 Ce2 C75 C11 140.0(7) . . . . ? C12 Ce2 C75 C11 176.1(7) . . . . ? C55 Ce2 C75 C11 -121.0(9) . . . . ? C57 Ce2 C75 C11 -148.4(7) . . . . ? C2 Ce2 C75 C11 126.4(6) . . . . ? C5 Ce2 C75 C11 174.8(6) . . . . ? C42 Ce2 C75 C11 71.9(6) . . . . ? C32 Ce2 C75 C11 -129.1(6) . . . . ? C3 Ce2 C75 C11 -87.0(6) . . . . ? C15 C68 C76 C40 -2.8(15) . . . . ? C69 C68 C76 C40 -145.7(10) . . . . ? Ce3 C68 C76 C40 -58.9(11) . . . . ? C15 C68 C76 C78 144.8(9) . . . . ? C69 C68 C76 C78 1.9(11) . . . . ? Ce3 C68 C76 C78 88.7(9) . . . . ? C15 C68 C76 Ce3 56.2(10) . . . . ? C69 C68 C76 Ce3 -86.8(9) . . . . ? C35 C40 C76 C68 -2.8(15) . . . . ? C38 C40 C76 C68 146.2(10) . . . . ? Ce3 C40 C76 C68 53.1(10) . . . . ? C35 C40 C76 C78 -146.2(9) . . . . ? C38 C40 C76 C78 2.8(14) . . . . ? Ce3 C40 C76 C78 -90.3(10) . . . . ? C35 C40 C76 Ce3 -55.9(10) . . . . ? C38 C40 C76 Ce3 93.1(9) . . . . ? C70 C50 C77 C46 -2.0(14) . . . . ? C73 C50 C77 C46 141.8(9) . . . . ? Ce4 C50 C77 C46 90.4(10) . . . . ? C70 C50 C77 C27 -146.1(8) . . . . ? C73 C50 C77 C27 -2.4(10) . . . . ? Ce4 C50 C77 C27 -53.8(7) . . . . ? C70 C50 C77 Ce4 -92.3(8) . . . . ? C73 C50 C77 Ce4 51.4(6) . . . . ? C23 C46 C77 C50 -149.9(9) . . . . ? C30 C46 C77 C50 3.3(13) . . . . ? C23 C46 C77 C27 -9.5(12) . . . . ? C30 C46 C77 C27 143.7(8) . . . . ? C23 C46 C77 Ce4 -84.8(8) . . . . ? C30 C46 C77 Ce4 68.4(9) . . . . ? C65 C27 C77 C50 146.1(9) . . . . ? C72 C27 C77 C50 -0.4(10) . . . . ? Ce4 C27 C77 C50 48.7(7) . . . . ? C65 C27 C77 C46 0.5(13) . . . . ? C72 C27 C77 C46 -145.9(8) . . . . ? Ce4 C27 C77 C46 -96.8(8) . . . . ? C65 C27 C77 Ce4 97.4(9) . . . . ? C72 C27 C77 Ce4 -49.1(7) . . . . ? C6 C60 C78 C76 144.3(9) . . . . ? C21 C60 C78 C76 -8.5(13) . . . . ? C6 C60 C78 C49 8.3(14) . . . . ? C21 C60 C78 C49 -144.6(9) . . . . ? C6 C60 C78 Ce3 91.8(10) . . . . ? C21 C60 C78 Ce3 -61.1(9) . . . . ? C68 C76 C78 C60 -144.5(8) . . . . ? C40 C76 C78 C60 4.1(14) . . . . ? Ce3 C76 C78 C60 -77.2(9) . . . . ? C68 C76 C78 C49 -4.5(11) . . . . ? C40 C76 C78 C49 144.2(9) . . . . ? Ce3 C76 C78 C49 62.8(8) . . . . ? C68 C76 C78 Ce3 -67.3(7) . . . . ? C40 C76 C78 Ce3 81.3(9) . . . . ? C69 C49 C78 C60 146.0(9) . . . . ? C44 C49 C78 C60 -3.3(14) . . . . ? Ce3 C49 C78 C60 94.0(9) . . . . ? C69 C49 C78 C76 5.4(10) . . . . ? C44 C49 C78 C76 -143.9(9) . . . . ? Ce3 C49 C78 C76 -46.7(7) . . . . ? C69 C49 C78 Ce3 52.0(7) . . . . ? C44 C49 C78 Ce3 -97.2(9) . . . . ? C8 C15 Ce3 C68 122.1(9) . . . . ? C63 C15 Ce3 C68 -123.3(8) . . . . ? C68 C15 Ce3 C76 30.2(6) . . . . ? C8 C15 Ce3 C76 152.3(8) . . . . ? C63 C15 Ce3 C76 -93.1(7) . . . . ? C68 C15 Ce3 C63 123.3(8) . . . . ? C8 C15 Ce3 C63 -114.6(9) . . . . ? C68 C15 Ce3 C40 64.7(7) . . . . ? C8 C15 Ce3 C40 -173.2(8) . . . . ? C63 C15 Ce3 C40 -58.5(7) . . . . ? C68 C15 Ce3 C35 96.2(7) . . . . ? C8 C15 Ce3 C35 -141.7(8) . . . . ? C63 C15 Ce3 C35 -27.0(6) . . . . ? C68 C15 Ce3 C8 -122.1(9) . . . . ? C63 C15 Ce3 C8 114.6(9) . . . . ? C68 C15 Ce3 C69 -31.9(5) . . . . ? C8 C15 Ce3 C69 90.2(6) . . . . ? C63 C15 Ce3 C69 -155.2(7) . . . . ? C68 C15 Ce3 C78 10.0(6) . . . . ? C8 C15 Ce3 C78 132.1(7) . . . . ? C63 C15 Ce3 C78 -113.3(7) . . . . ? C68 C15 Ce3 C49 -19.1(5) . . . . ? C8 C15 Ce3 C49 103.0(7) . . . . ? C63 C15 Ce3 C49 -142.4(6) . . . . ? C68 C15 Ce3 C54 -92.5(6) . . . . ? C8 C15 Ce3 C54 29.6(5) . . . . ? C63 C15 Ce3 C54 144.3(7) . . . . ? C68 C15 Ce3 C10 -63.0(6) . . . . ? C8 C15 Ce3 C10 59.1(6) . . . . ? C63 C15 Ce3 C10 173.8(7) . . . . ? C76 C68 Ce3 C15 129.5(9) . . . . ? C69 C68 Ce3 C15 -121.8(8) . . . . ? C15 C68 Ce3 C76 -129.5(9) . . . . ? C69 C68 Ce3 C76 108.7(9) . . . . ? C76 C68 Ce3 C63 95.6(7) . . . . ? C15 C68 Ce3 C63 -33.9(5) . . . . ? C69 C68 Ce3 C63 -155.7(7) . . . . ? C76 C68 Ce3 C40 27.0(6) . . . . ? C15 C68 Ce3 C40 -102.5(7) . . . . ? C69 C68 Ce3 C40 135.8(7) . . . . ? C76 C68 Ce3 C35 60.1(7) . . . . ? C15 C68 Ce3 C35 -69.3(6) . . . . ? C69 C68 Ce3 C35 168.9(7) . . . . ? C76 C68 Ce3 C8 161.5(8) . . . . ? C15 C68 Ce3 C8 32.0(5) . . . . ? C69 C68 Ce3 C8 -89.8(6) . . . . ? C76 C68 Ce3 C69 -108.7(9) . . . . ? C15 C68 Ce3 C69 121.8(8) . . . . ? C76 C68 Ce3 C78 -38.0(6) . . . . ? C15 C68 Ce3 C78 -167.5(7) . . . . ? C69 C68 Ce3 C78 70.7(6) . . . . ? C76 C68 Ce3 C49 -75.3(7) . . . . ? C15 C68 Ce3 C49 155.2(7) . . . . ? C69 C68 Ce3 C49 33.4(5) . . . . ? C76 C68 Ce3 C54 -166.6(8) . . . . ? C15 C68 Ce3 C54 63.9(5) . . . . ? C69 C68 Ce3 C54 -57.9(6) . . . . ? C76 C68 Ce3 C10 -136.9(8) . . . . ? C15 C68 Ce3 C10 93.6(6) . . . . ? C69 C68 Ce3 C10 -28.1(5) . . . . ? C68 C76 Ce3 C15 -31.4(6) . . . . ? C40 C76 Ce3 C15 102.1(8) . . . . ? C78 C76 Ce3 C15 -137.6(7) . . . . ? C40 C76 Ce3 C68 133.5(10) . . . . ? C78 C76 Ce3 C68 -106.2(9) . . . . ? C68 C76 Ce3 C63 -70.6(7) . . . . ? C40 C76 Ce3 C63 62.9(7) . . . . ? C78 C76 Ce3 C63 -176.8(6) . . . . ? C68 C76 Ce3 C40 -133.5(10) . . . . ? C78 C76 Ce3 C40 120.3(9) . . . . ? C68 C76 Ce3 C35 -104.9(8) . . . . ? C40 C76 Ce3 C35 28.6(6) . . . . ? C78 C76 Ce3 C35 148.9(7) . . . . ? C68 C76 Ce3 C8 -16.4(7) . . . . ? C40 C76 Ce3 C8 117.1(9) . . . . ? C78 C76 Ce3 C8 -122.6(8) . . . . ? C68 C76 Ce3 C69 38.9(6) . . . . ? C40 C76 Ce3 C69 172.4(8) . . . . ? C78 C76 Ce3 C69 -67.3(6) . . . . ? C68 C76 Ce3 C78 106.2(9) . . . . ? C40 C76 Ce3 C78 -120.3(9) . . . . ? C68 C76 Ce3 C49 73.9(7) . . . . ? C40 C76 Ce3 C49 -152.6(8) . . . . ? C78 C76 Ce3 C49 -32.3(5) . . . . ? C68 C76 Ce3 C54 12.2(7) . . . . ? C40 C76 Ce3 C54 145.7(8) . . . . ? C78 C76 Ce3 C54 -94.0(8) . . . . ? C68 C76 Ce3 C10 33.7(6) . . . . ? C40 C76 Ce3 C10 167.2(8) . . . . ? C78 C76 Ce3 C10 -72.5(6) . . . . ? C22 C63 Ce3 C15 120.1(9) . . . . ? C35 C63 Ce3 C15 -133.1(10) . . . . ? Ce1 C63 Ce3 C15 127.4(8) . . . . ? C22 C63 Ce3 C68 155.1(7) . . . . ? C35 C63 Ce3 C68 -98.1(7) . . . . ? C15 C63 Ce3 C68 34.9(6) . . . . ? Ce1 C63 Ce3 C68 162.3(7) . . . . ? C22 C63 Ce3 C76 -166.5(7) . . . . ? C35 C63 Ce3 C76 -59.7(6) . . . . ? C15 C63 Ce3 C76 73.4(7) . . . . ? Ce1 C63 Ce3 C76 -159.3(7) . . . . ? C22 C63 Ce3 C40 -131.4(7) . . . . ? C35 C63 Ce3 C40 -24.7(6) . . . . ? C15 C63 Ce3 C40 108.4(8) . . . . ? Ce1 C63 Ce3 C40 -124.2(6) . . . . ? C22 C63 Ce3 C35 -106.8(9) . . . . ? C15 C63 Ce3 C35 133.1(10) . . . . ? Ce1 C63 Ce3 C35 -99.6(7) . . . . ? C22 C63 Ce3 C8 84.1(7) . . . . ? C35 C63 Ce3 C8 -169.1(8) . . . . ? C15 C63 Ce3 C8 -36.0(5) . . . . ? Ce1 C63 Ce3 C8 91.3(5) . . . . ? C22 C63 Ce3 C69 141.9(7) . . . . ? C35 C63 Ce3 C69 -111.3(8) . . . . ? C15 C63 Ce3 C69 21.8(6) . . . . ? Ce1 C63 Ce3 C69 149.2(7) . . . . ? C22 C63 Ce3 C78 -168.2(7) . . . . ? C35 C63 Ce3 C78 -61.4(7) . . . . ? C15 C63 Ce3 C78 71.7(8) . . . . ? Ce1 C63 Ce3 C78 -161.0(7) . . . . ? C22 C63 Ce3 C49 163.0(7) . . . . ? C35 C63 Ce3 C49 -90.2(8) . . . . ? C15 C63 Ce3 C49 42.8(7) . . . . ? Ce1 C63 Ce3 C49 170.2(8) . . . . ? C22 C63 Ce3 C54 91.9(7) . . . . ? C35 C63 Ce3 C54 -161.3(8) . . . . ? C15 C63 Ce3 C54 -28.2(6) . . . . ? Ce1 C63 Ce3 C54 99.2(5) . . . . ? C22 C63 Ce3 C10 114.4(8) . . . . ? C35 C63 Ce3 C10 -138.8(8) . . . . ? C15 C63 Ce3 C10 -5.7(6) . . . . ? Ce1 C63 Ce3 C10 121.6(7) . . . . ? C35 C40 Ce3 C15 62.2(8) . . . . ? C76 C40 Ce3 C15 -67.2(8) . . . . ? C38 C40 Ce3 C15 178.7(9) . . . . ? C35 C40 Ce3 C68 100.7(8) . . . . ? C76 C40 Ce3 C68 -28.7(7) . . . . ? C38 C40 Ce3 C68 -142.8(9) . . . . ? C35 C40 Ce3 C76 129.4(10) . . . . ? C38 C40 Ce3 C76 -114.1(10) . . . . ? C35 C40 Ce3 C63 26.0(6) . . . . ? C76 C40 Ce3 C63 -103.4(8) . . . . ? C38 C40 Ce3 C63 142.6(8) . . . . ? C76 C40 Ce3 C35 -129.4(10) . . . . ? C38 C40 Ce3 C35 116.5(10) . . . . ? C35 C40 Ce3 C8 58.1(9) . . . . ? C76 C40 Ce3 C8 -71.3(9) . . . . ? C38 C40 Ce3 C8 174.7(9) . . . . ? C35 C40 Ce3 C69 123.1(8) . . . . ? C76 C40 Ce3 C69 -6.3(7) . . . . ? C38 C40 Ce3 C69 -120.4(8) . . . . ? C35 C40 Ce3 C78 161.7(7) . . . . ? C76 C40 Ce3 C78 32.3(6) . . . . ? C38 C40 Ce3 C78 -81.8(8) . . . . ? C35 C40 Ce3 C49 150.7(7) . . . . ? C76 C40 Ce3 C49 21.3(6) . . . . ? C38 C40 Ce3 C49 -92.8(8) . . . . ? C35 C40 Ce3 C54 85.3(12) . . . . ? C76 C40 Ce3 C54 -44.1(11) . . . . ? C38 C40 Ce3 C54 -158.2(11) . . . . ? C35 C40 Ce3 C10 115.1(9) . . . . ? C76 C40 Ce3 C10 -14.3(9) . . . . ? C38 C40 Ce3 C10 -128.4(9) . . . . ? C40 C35 Ce3 C15 -107.5(8) . . . . ? C41 C35 Ce3 C15 130.3(9) . . . . ? C63 C35 Ce3 C15 29.3(7) . . . . ? C40 C35 Ce3 C68 -67.5(8) . . . . ? C41 C35 Ce3 C68 170.3(8) . . . . ? C63 C35 Ce3 C68 69.3(7) . . . . ? C40 C35 Ce3 C76 -30.5(6) . . . . ? C41 C35 Ce3 C76 -152.6(8) . . . . ? C63 C35 Ce3 C76 106.4(7) . . . . ? C40 C35 Ce3 C63 -136.8(9) . . . . ? C41 C35 Ce3 C63 101.0(9) . . . . ? C41 C35 Ce3 C40 -122.2(10) . . . . ? C63 C35 Ce3 C40 136.8(9) . . . . ? C40 C35 Ce3 C8 -127.5(8) . . . . ? C41 C35 Ce3 C8 110.3(8) . . . . ? C63 C35 Ce3 C8 9.3(7) . . . . ? C40 C35 Ce3 C69 -61.1(8) . . . . ? C41 C35 Ce3 C69 176.7(8) . . . . ? C63 C35 Ce3 C69 75.7(8) . . . . ? C40 C35 Ce3 C78 -15.1(6) . . . . ? C41 C35 Ce3 C78 -137.3(8) . . . . ? C63 C35 Ce3 C78 121.7(7) . . . . ? C40 C35 Ce3 C49 -31.5(8) . . . . ? C41 C35 Ce3 C49 -153.7(8) . . . . ? C63 C35 Ce3 C49 105.3(8) . . . . ? C40 C35 Ce3 C54 -115.5(10) . . . . ? C41 C35 Ce3 C54 122.3(9) . . . . ? C63 C35 Ce3 C54 21.3(9) . . . . ? C40 C35 Ce3 C10 -84.3(11) . . . . ? C41 C35 Ce3 C10 153.5(10) . . . . ? C63 C35 Ce3 C10 52.5(10) . . . . ? C54 C8 Ce3 C15 123.0(10) . . . . ? C33 C8 Ce3 C15 -118.9(10) . . . . ? C54 C8 Ce3 C68 86.3(7) . . . . ? C33 C8 Ce3 C68 -155.6(8) . . . . ? C15 C8 Ce3 C68 -36.7(7) . . . . ? C54 C8 Ce3 C76 97.4(8) . . . . ? C33 C8 Ce3 C76 -144.5(8) . . . . ? C15 C8 Ce3 C76 -25.6(7) . . . . ? C54 C8 Ce3 C63 163.4(8) . . . . ? C33 C8 Ce3 C63 -78.5(7) . . . . ? C15 C8 Ce3 C63 40.4(7) . . . . ? C54 C8 Ce3 C40 130.2(10) . . . . ? C33 C8 Ce3 C40 -111.7(9) . . . . ? C15 C8 Ce3 C40 7.2(8) . . . . ? C54 C8 Ce3 C35 157.3(8) . . . . ? C33 C8 Ce3 C35 -84.6(8) . . . . ? C15 C8 Ce3 C35 34.2(7) . . . . ? C54 C8 Ce3 C69 49.7(6) . . . . ? C33 C8 Ce3 C69 167.8(7) . . . . ? C15 C8 Ce3 C69 -73.3(7) . . . . ? C54 C8 Ce3 C78 69.5(8) . . . . ? C33 C8 Ce3 C78 -172.3(7) . . . . ? C15 C8 Ce3 C78 -53.5(8) . . . . ? C54 C8 Ce3 C49 45.4(7) . . . . ? C33 C8 Ce3 C49 163.6(7) . . . . ? C15 C8 Ce3 C49 -77.6(8) . . . . ? C33 C8 Ce3 C54 118.1(8) . . . . ? C15 C8 Ce3 C54 -123.0(10) . . . . ? C54 C8 Ce3 C10 22.3(5) . . . . ? C33 C8 Ce3 C10 140.4(7) . . . . ? C15 C8 Ce3 C10 -100.8(8) . . . . ? C10 C69 Ce3 C15 -88.3(7) . . . . ? C49 C69 Ce3 C15 152.1(8) . . . . ? C68 C69 Ce3 C15 37.0(6) . . . . ? C10 C69 Ce3 C68 -125.3(10) . . . . ? C49 C69 Ce3 C68 115.1(9) . . . . ? C10 C69 Ce3 C76 -168.8(9) . . . . ? C49 C69 Ce3 C76 71.6(7) . . . . ? C68 C69 Ce3 C76 -43.5(7) . . . . ? C10 C69 Ce3 C63 -103.1(8) . . . . ? C49 C69 Ce3 C63 137.2(7) . . . . ? C68 C69 Ce3 C63 22.2(7) . . . . ? C10 C69 Ce3 C40 -164.5(8) . . . . ? C49 C69 Ce3 C40 75.9(8) . . . . ? C68 C69 Ce3 C40 -39.2(7) . . . . ? C10 C69 Ce3 C35 -136.5(9) . . . . ? C49 C69 Ce3 C35 103.9(9) . . . . ? C68 C69 Ce3 C35 -11.2(7) . . . . ? C10 C69 Ce3 C8 -51.4(7) . . . . ? C49 C69 Ce3 C8 -171.0(7) . . . . ? C68 C69 Ce3 C8 73.9(7) . . . . ? C10 C69 Ce3 C78 152.9(8) . . . . ? C49 C69 Ce3 C78 33.3(6) . . . . ? C68 C69 Ce3 C78 -81.8(7) . . . . ? C10 C69 Ce3 C49 119.6(10) . . . . ? C68 C69 Ce3 C49 -115.1(9) . . . . ? C10 C69 Ce3 C54 -23.5(6) . . . . ? C49 C69 Ce3 C54 -143.1(8) . . . . ? C68 C69 Ce3 C54 101.8(8) . . . . ? C49 C69 Ce3 C10 -119.6(10) . . . . ? C68 C69 Ce3 C10 125.3(10) . . . . ? C60 C78 Ce3 C15 159.7(8) . . . . ? C76 C78 Ce3 C15 38.4(7) . . . . ? C49 C78 Ce3 C15 -82.6(8) . . . . ? C60 C78 Ce3 C68 167.4(8) . . . . ? C76 C78 Ce3 C68 46.2(6) . . . . ? C49 C78 Ce3 C68 -74.8(7) . . . . ? C60 C78 Ce3 C76 121.3(9) . . . . ? C49 C78 Ce3 C76 -121.0(9) . . . . ? C60 C78 Ce3 C63 124.5(8) . . . . ? C76 C78 Ce3 C63 3.2(6) . . . . ? C49 C78 Ce3 C63 -117.8(8) . . . . ? C60 C78 Ce3 C40 85.0(7) . . . . ? C76 C78 Ce3 C40 -36.2(6) . . . . ? C49 C78 Ce3 C40 -157.2(8) . . . . ? C60 C78 Ce3 C35 94.7(7) . . . . ? C76 C78 Ce3 C35 -26.5(6) . . . . ? C49 C78 Ce3 C35 -147.5(8) . . . . ? C60 C78 Ce3 C8 -174.0(8) . . . . ? C76 C78 Ce3 C8 64.7(8) . . . . ? C49 C78 Ce3 C8 -56.3(8) . . . . ? C60 C78 Ce3 C69 -149.9(8) . . . . ? C76 C78 Ce3 C69 88.9(7) . . . . ? C49 C78 Ce3 C69 -32.1(6) . . . . ? C60 C78 Ce3 C49 -117.7(10) . . . . ? C76 C78 Ce3 C49 121.0(9) . . . . ? C60 C78 Ce3 C54 -147.0(7) . . . . ? C76 C78 Ce3 C54 91.7(8) . . . . ? C49 C78 Ce3 C54 -29.3(7) . . . . ? C60 C78 Ce3 C10 -137.2(7) . . . . ? C76 C78 Ce3 C10 101.5(7) . . . . ? C49 C78 Ce3 C10 -19.5(6) . . . . ? C69 C49 Ce3 C15 -24.4(7) . . . . ? C44 C49 Ce3 C15 -143.2(7) . . . . ? C78 C49 Ce3 C15 96.9(8) . . . . ? C69 C49 Ce3 C68 -39.5(6) . . . . ? C44 C49 Ce3 C68 -158.3(8) . . . . ? C78 C49 Ce3 C68 81.7(7) . . . . ? C69 C49 Ce3 C76 -87.3(8) . . . . ? C44 C49 Ce3 C76 153.9(8) . . . . ? C78 C49 Ce3 C76 34.0(6) . . . . ? C69 C49 Ce3 C63 -48.8(8) . . . . ? C44 C49 Ce3 C63 -167.6(7) . . . . ? C78 C49 Ce3 C63 72.5(8) . . . . ? C69 C49 Ce3 C40 -102.5(8) . . . . ? C44 C49 Ce3 C40 138.7(7) . . . . ? C78 C49 Ce3 C40 18.8(7) . . . . ? C69 C49 Ce3 C35 -86.1(9) . . . . ? C44 C49 Ce3 C35 155.1(8) . . . . ? C78 C49 Ce3 C35 35.2(8) . . . . ? C69 C49 Ce3 C8 8.3(7) . . . . ? C44 C49 Ce3 C8 -110.5(7) . . . . ? C78 C49 Ce3 C8 129.6(8) . . . . ? C44 C49 Ce3 C69 -118.8(9) . . . . ? C78 C49 Ce3 C69 121.3(10) . . . . ? C69 C49 Ce3 C78 -121.3(10) . . . . ? C44 C49 Ce3 C78 119.9(9) . . . . ? C69 C49 Ce3 C54 28.8(6) . . . . ? C44 C49 Ce3 C54 -90.0(7) . . . . ? C78 C49 Ce3 C54 150.1(7) . . . . ? C69 C49 Ce3 C10 33.0(6) . . . . ? C44 C49 Ce3 C10 -85.8(7) . . . . ? C78 C49 Ce3 C10 154.3(8) . . . . ? C10 C54 Ce3 C15 104.4(8) . . . . ? C8 C54 Ce3 C15 -35.0(7) . . . . ? C4 C54 Ce3 C15 -150.9(8) . . . . ? C10 C54 Ce3 C68 60.5(7) . . . . ? C8 C54 Ce3 C68 -78.9(7) . . . . ? C4 C54 Ce3 C68 165.3(8) . . . . ? C10 C54 Ce3 C76 52.4(9) . . . . ? C8 C54 Ce3 C76 -87.0(9) . . . . ? C4 C54 Ce3 C76 157.1(8) . . . . ? C10 C54 Ce3 C63 125.3(8) . . . . ? C8 C54 Ce3 C63 -14.2(6) . . . . ? C4 C54 Ce3 C63 -130.0(7) . . . . ? C10 C54 Ce3 C40 76.0(12) . . . . ? C8 C54 Ce3 C40 -63.4(11) . . . . ? C4 C54 Ce3 C40 -179.2(11) . . . . ? C10 C54 Ce3 C35 113.4(10) . . . . ? C8 C54 Ce3 C35 -26.0(9) . . . . ? C4 C54 Ce3 C35 -141.9(9) . . . . ? C10 C54 Ce3 C8 139.4(9) . . . . ? C4 C54 Ce3 C8 -115.9(9) . . . . ? C10 C54 Ce3 C69 23.9(6) . . . . ? C8 C54 Ce3 C69 -115.5(7) . . . . ? C4 C54 Ce3 C69 128.6(8) . . . . ? C10 C54 Ce3 C78 21.1(7) . . . . ? C8 C54 Ce3 C78 -118.3(8) . . . . ? C4 C54 Ce3 C78 125.8(7) . . . . ? C10 C54 Ce3 C49 6.7(6) . . . . ? C8 C54 Ce3 C49 -132.7(7) . . . . ? C4 C54 Ce3 C49 111.5(7) . . . . ? C8 C54 Ce3 C10 -139.4(9) . . . . ? C4 C54 Ce3 C10 104.7(9) . . . . ? C69 C10 Ce3 C15 77.4(8) . . . . ? C54 C10 Ce3 C15 -60.1(7) . . . . ? C7 C10 Ce3 C15 -169.1(8) . . . . ? C69 C10 Ce3 C68 33.7(7) . . . . ? C54 C10 Ce3 C68 -103.7(8) . . . . ? C7 C10 Ce3 C68 147.2(8) . . . . ? C69 C10 Ce3 C76 9.3(7) . . . . ? C54 C10 Ce3 C76 -128.1(8) . . . . ? C7 C10 Ce3 C76 122.8(8) . . . . ? C69 C10 Ce3 C63 81.2(8) . . . . ? C54 C10 Ce3 C63 -56.3(8) . . . . ? C7 C10 Ce3 C63 -165.3(7) . . . . ? C69 C10 Ce3 C40 17.4(9) . . . . ? C54 C10 Ce3 C40 -120.0(10) . . . . ? C7 C10 Ce3 C40 130.9(9) . . . . ? C69 C10 Ce3 C35 54.0(11) . . . . ? C54 C10 Ce3 C35 -83.4(11) . . . . ? C7 C10 Ce3 C35 167.5(10) . . . . ? C69 C10 Ce3 C8 114.3(8) . . . . ? C54 C10 Ce3 C8 -23.1(5) . . . . ? C7 C10 Ce3 C8 -132.2(7) . . . . ? C54 C10 Ce3 C69 -137.5(10) . . . . ? C7 C10 Ce3 C69 113.5(9) . . . . ? C69 C10 Ce3 C78 -21.1(7) . . . . ? C54 C10 Ce3 C78 -158.5(7) . . . . ? C7 C10 Ce3 C78 92.4(7) . . . . ? C69 C10 Ce3 C49 -33.7(6) . . . . ? C54 C10 Ce3 C49 -171.2(8) . . . . ? C7 C10 Ce3 C49 79.8(7) . . . . ? C69 C10 Ce3 C54 137.5(10) . . . . ? C7 C10 Ce3 C54 -109.0(8) . . . . ? C72 C73 Ce4 C18 131.2(8) . . . . ? C50 C73 Ce4 C18 -124.0(7) . . . . ? C18 C73 Ce4 C72 -131.2(8) . . . . ? C50 C73 Ce4 C72 104.8(8) . . . . ? C18 C73 Ce4 C32 -33.3(5) . . . . ? C72 C73 Ce4 C32 97.9(6) . . . . ? C50 C73 Ce4 C32 -157.3(6) . . . . ? C18 C73 Ce4 C56 -102.3(6) . . . . ? C72 C73 Ce4 C56 28.9(6) . . . . ? C50 C73 Ce4 C56 133.7(7) . . . . ? C18 C73 Ce4 C50 124.0(7) . . . . ? C72 C73 Ce4 C50 -104.8(8) . . . . ? C18 C73 Ce4 C20 -68.1(6) . . . . ? C72 C73 Ce4 C20 63.2(6) . . . . ? C50 C73 Ce4 C20 168.0(6) . . . . ? C18 C73 Ce4 C71 32.3(5) . . . . ? C72 C73 Ce4 C71 163.6(7) . . . . ? C50 C73 Ce4 C71 -91.6(6) . . . . ? C18 C73 Ce4 C27 -166.3(7) . . . . ? C72 C73 Ce4 C27 -35.0(5) . . . . ? C50 C73 Ce4 C27 69.8(5) . . . . ? C18 C73 Ce4 C77 156.4(7) . . . . ? C72 C73 Ce4 C77 -72.4(6) . . . . ? C50 C73 Ce4 C77 32.4(4) . . . . ? C18 C73 Ce4 C70 95.4(6) . . . . ? C72 C73 Ce4 C70 -133.4(7) . . . . ? C50 C73 Ce4 C70 -28.6(4) . . . . ? C18 C73 Ce4 C26 64.1(5) . . . . ? C72 C73 Ce4 C26 -164.7(7) . . . . ? C50 C73 Ce4 C26 -59.9(5) . . . . ? C32 C18 Ce4 C73 -121.7(8) . . . . ? C71 C18 Ce4 C73 121.8(8) . . . . ? C73 C18 Ce4 C72 30.5(5) . . . . ? C32 C18 Ce4 C72 -91.2(6) . . . . ? C71 C18 Ce4 C72 152.2(7) . . . . ? C73 C18 Ce4 C32 121.7(8) . . . . ? C71 C18 Ce4 C32 -116.6(9) . . . . ? C73 C18 Ce4 C56 65.1(6) . . . . ? C32 C18 Ce4 C56 -56.6(6) . . . . ? C71 C18 Ce4 C56 -173.2(7) . . . . ? C73 C18 Ce4 C50 -32.9(5) . . . . ? C32 C18 Ce4 C50 -154.5(6) . . . . ? C71 C18 Ce4 C50 88.9(6) . . . . ? C73 C18 Ce4 C20 97.3(6) . . . . ? C32 C18 Ce4 C20 -24.4(5) . . . . ? C71 C18 Ce4 C20 -141.0(7) . . . . ? C73 C18 Ce4 C71 -121.8(8) . . . . ? C32 C18 Ce4 C71 116.6(8) . . . . ? C73 C18 Ce4 C27 11.7(6) . . . . ? C32 C18 Ce4 C27 -110.0(7) . . . . ? C71 C18 Ce4 C27 133.5(7) . . . . ? C73 C18 Ce4 C77 -19.2(6) . . . . ? C32 C18 Ce4 C77 -140.9(6) . . . . ? C71 C18 Ce4 C77 102.5(7) . . . . ? C73 C18 Ce4 C70 -64.6(5) . . . . ? C32 C18 Ce4 C70 173.7(6) . . . . ? C71 C18 Ce4 C70 57.2(6) . . . . ? C73 C18 Ce4 C26 -94.5(6) . . . . ? C32 C18 Ce4 C26 143.8(7) . . . . ? C71 C18 Ce4 C26 27.3(5) . . . . ? C56 C72 Ce4 C73 128.6(10) . . . . ? C27 C72 Ce4 C73 -112.0(9) . . . . ? C56 C72 Ce4 C18 98.0(7) . . . . ? C27 C72 Ce4 C18 -142.6(7) . . . . ? C73 C72 Ce4 C18 -30.5(6) . . . . ? C56 C72 Ce4 C32 61.0(7) . . . . ? C27 C72 Ce4 C32 -179.5(7) . . . . ? C73 C72 Ce4 C32 -67.5(7) . . . . ? C27 C72 Ce4 C56 119.4(9) . . . . ? C73 C72 Ce4 C56 -128.6(10) . . . . ? C56 C72 Ce4 C50 171.2(8) . . . . ? C27 C72 Ce4 C50 -69.4(6) . . . . ? C73 C72 Ce4 C50 42.7(6) . . . . ? C56 C72 Ce4 C20 27.2(6) . . . . ? C27 C72 Ce4 C20 146.6(7) . . . . ? C73 C72 Ce4 C20 -101.4(7) . . . . ? C56 C72 Ce4 C71 113.6(8) . . . . ? C27 C72 Ce4 C71 -127.0(7) . . . . ? C73 C72 Ce4 C71 -15.0(7) . . . . ? C56 C72 Ce4 C27 -119.4(9) . . . . ? C73 C72 Ce4 C27 112.0(9) . . . . ? C56 C72 Ce4 C77 -153.7(8) . . . . ? C27 C72 Ce4 C77 -34.3(5) . . . . ? C73 C72 Ce4 C77 77.7(7) . . . . ? C56 C72 Ce4 C70 166.5(7) . . . . ? C27 C72 Ce4 C70 -74.0(7) . . . . ? C73 C72 Ce4 C70 38.0(6) . . . . ? C56 C72 Ce4 C26 143.3(8) . . . . ? C27 C72 Ce4 C26 -97.3(7) . . . . ? C73 C72 Ce4 C26 14.7(7) . . . . ? C18 C32 Ce4 C73 37.0(6) . . . . ? C57 C32 Ce4 C73 156.6(8) . . . . ? C20 C32 Ce4 C73 -101.4(7) . . . . ? Ce2 C32 Ce4 C73 163.9(7) . . . . ? C57 C32 Ce4 C18 119.6(9) . . . . ? C20 C32 Ce4 C18 -138.4(9) . . . . ? Ce2 C32 Ce4 C18 126.9(7) . . . . ? C18 C32 Ce4 C72 77.7(7) . . . . ? C57 C32 Ce4 C72 -162.7(7) . . . . ? C20 C32 Ce4 C72 -60.7(6) . . . . ? Ce2 C32 Ce4 C72 -155.4(7) . . . . ? C18 C32 Ce4 C56 111.7(7) . . . . ? C57 C32 Ce4 C56 -128.7(8) . . . . ? C20 C32 Ce4 C56 -26.7(6) . . . . ? Ce2 C32 Ce4 C56 -121.4(6) . . . . ? C18 C32 Ce4 C50 23.5(6) . . . . ? C57 C32 Ce4 C50 143.1(7) . . . . ? C20 C32 Ce4 C50 -114.9(7) . . . . ? Ce2 C32 Ce4 C50 150.4(7) . . . . ? C18 C32 Ce4 C20 138.4(9) . . . . ? C57 C32 Ce4 C20 -102.0(9) . . . . ? Ce2 C32 Ce4 C20 -94.7(7) . . . . ? C18 C32 Ce4 C71 -36.3(5) . . . . ? C57 C32 Ce4 C71 83.3(7) . . . . ? C20 C32 Ce4 C71 -174.7(8) . . . . ? Ce2 C32 Ce4 C71 90.6(4) . . . . ? C18 C32 Ce4 C27 77.5(8) . . . . ? C57 C32 Ce4 C27 -162.9(7) . . . . ? C20 C32 Ce4 C27 -60.9(8) . . . . ? Ce2 C32 Ce4 C27 -155.6(8) . . . . ? C18 C32 Ce4 C77 46.2(8) . . . . ? C57 C32 Ce4 C77 165.7(7) . . . . ? C20 C32 Ce4 C77 -92.2(8) . . . . ? Ce2 C32 Ce4 C77 173.1(9) . . . . ? C18 C32 Ce4 C70 -6.0(6) . . . . ? C57 C32 Ce4 C70 113.5(7) . . . . ? C20 C32 Ce4 C70 -144.4(7) . . . . ? Ce2 C32 Ce4 C70 120.9(6) . . . . ? C18 C32 Ce4 C26 -29.5(6) . . . . ? C57 C32 Ce4 C26 90.0(7) . . . . ? C20 C32 Ce4 C26 -167.9(7) . . . . ? Ce2 C32 Ce4 C26 97.4(4) . . . . ? C72 C56 Ce4 C73 -33.2(7) . . . . ? C20 C56 Ce4 C73 100.2(8) . . . . ? C39 C56 Ce4 C73 -148.6(8) . . . . ? C72 C56 Ce4 C18 -72.7(7) . . . . ? C20 C56 Ce4 C18 60.7(7) . . . . ? C39 C56 Ce4 C18 171.9(8) . . . . ? C20 C56 Ce4 C72 133.4(10) . . . . ? C39 C56 Ce4 C72 -115.4(10) . . . . ? C72 C56 Ce4 C32 -106.2(7) . . . . ? C20 C56 Ce4 C32 27.2(6) . . . . ? C39 C56 Ce4 C32 138.5(8) . . . . ? C72 C56 Ce4 C50 -7.5(7) . . . . ? C20 C56 Ce4 C50 125.9(8) . . . . ? C39 C56 Ce4 C50 -122.9(8) . . . . ? C72 C56 Ce4 C20 -133.4(10) . . . . ? C39 C56 Ce4 C20 111.3(10) . . . . ? C72 C56 Ce4 C71 -76.8(8) . . . . ? C20 C56 Ce4 C71 56.5(8) . . . . ? C39 C56 Ce4 C71 167.8(8) . . . . ? C72 C56 Ce4 C27 33.5(6) . . . . ? C20 C56 Ce4 C27 166.8(8) . . . . ? C39 C56 Ce4 C27 -81.9(7) . . . . ? C72 C56 Ce4 C77 20.9(6) . . . . ? C20 C56 Ce4 C77 154.2(7) . . . . ? C39 C56 Ce4 C77 -94.5(8) . . . . ? C72 C56 Ce4 C70 -15.7(8) . . . . ? C20 C56 Ce4 C70 117.6(9) . . . . ? C39 C56 Ce4 C70 -131.1(8) . . . . ? C72 C56 Ce4 C26 -49.9(10) . . . . ? C20 C56 Ce4 C26 83.5(10) . . . . ? C39 C56 Ce4 C26 -165.3(9) . . . . ? C77 C50 Ce4 C73 116.0(8) . . . . ? C70 C50 Ce4 C73 -124.3(8) . . . . ? C77 C50 Ce4 C18 151.3(7) . . . . ? C70 C50 Ce4 C18 -88.9(6) . . . . ? C73 C50 Ce4 C18 35.3(6) . . . . ? C77 C50 Ce4 C72 69.8(6) . . . . ? C70 C50 Ce4 C72 -170.4(7) . . . . ? C73 C50 Ce4 C72 -46.2(6) . . . . ? C77 C50 Ce4 C32 136.6(7) . . . . ? C70 C50 Ce4 C32 -103.6(7) . . . . ? C73 C50 Ce4 C32 20.7(6) . . . . ? C77 C50 Ce4 C56 74.7(7) . . . . ? C70 C50 Ce4 C56 -165.5(7) . . . . ? C73 C50 Ce4 C56 -41.2(6) . . . . ? C77 C50 Ce4 C20 103.5(8) . . . . ? C70 C50 Ce4 C20 -136.8(7) . . . . ? C73 C50 Ce4 C20 -12.5(7) . . . . ? C77 C50 Ce4 C71 -171.9(6) . . . . ? C70 C50 Ce4 C71 -52.1(6) . . . . ? C73 C50 Ce4 C71 72.1(6) . . . . ? C77 C50 Ce4 C27 31.9(5) . . . . ? C70 C50 Ce4 C27 151.7(7) . . . . ? C73 C50 Ce4 C27 -84.1(6) . . . . ? C70 C50 Ce4 C77 119.8(8) . . . . ? C73 C50 Ce4 C77 -116.0(8) . . . . ? C77 C50 Ce4 C70 -119.8(8) . . . . ? C73 C50 Ce4 C70 124.3(8) . . . . ? C77 C50 Ce4 C26 -144.0(7) . . . . ? C70 C50 Ce4 C26 -24.2(5) . . . . ? C73 C50 Ce4 C26 100.1(7) . . . . ? C3 C20 Ce4 C73 170.9(8) . . . . ? C56 C20 Ce4 C73 -68.0(7) . . . . ? C32 C20 Ce4 C73 66.3(7) . . . . ? C3 C20 Ce4 C18 129.9(8) . . . . ? C56 C20 Ce4 C18 -108.9(8) . . . . ? C32 C20 Ce4 C18 25.3(6) . . . . ? C3 C20 Ce4 C72 -148.9(8) . . . . ? C56 C20 Ce4 C72 -27.7(6) . . . . ? C32 C20 Ce4 C72 106.5(7) . . . . ? C3 C20 Ce4 C32 104.6(9) . . . . ? C56 C20 Ce4 C32 -134.2(9) . . . . ? C3 C20 Ce4 C56 -121.2(10) . . . . ? C32 C20 Ce4 C56 134.2(9) . . . . ? C3 C20 Ce4 C50 178.6(8) . . . . ? C56 C20 Ce4 C50 -60.3(8) . . . . ? C32 C20 Ce4 C50 74.0(8) . . . . ? C3 C20 Ce4 C71 109.1(8) . . . . ? C56 C20 Ce4 C71 -129.7(7) . . . . ? C32 C20 Ce4 C71 4.5(6) . . . . ? C3 C20 Ce4 C27 -132.1(8) . . . . ? C56 C20 Ce4 C27 -10.9(6) . . . . ? C32 C20 Ce4 C27 123.3(7) . . . . ? C3 C20 Ce4 C77 -149.7(8) . . . . ? C56 C20 Ce4 C77 -28.5(8) . . . . ? C32 C20 Ce4 C77 105.7(8) . . . . ? C3 C20 Ce4 C70 152.4(8) . . . . ? C56 C20 Ce4 C70 -86.5(9) . . . . ? C32 C20 Ce4 C70 47.8(9) . . . . ? C3 C20 Ce4 C26 118.6(8) . . . . ? C56 C20 Ce4 C26 -120.3(8) . . . . ? C32 C20 Ce4 C26 14.0(8) . . . . ? C26 C71 Ce4 C73 90.9(7) . . . . ? C5 C71 Ce4 C73 -153.7(8) . . . . ? C18 C71 Ce4 C73 -37.4(6) . . . . ? C26 C71 Ce4 C18 128.3(9) . . . . ? C5 C71 Ce4 C18 -116.3(9) . . . . ? C26 C71 Ce4 C72 101.5(7) . . . . ? C5 C71 Ce4 C72 -143.1(7) . . . . ? C18 C71 Ce4 C72 -26.8(7) . . . . ? C26 C71 Ce4 C32 166.0(7) . . . . ? C5 C71 Ce4 C32 -78.5(7) . . . . ? C18 C71 Ce4 C32 37.7(6) . . . . ? C26 C71 Ce4 C56 135.6(8) . . . . ? C5 C71 Ce4 C56 -109.0(8) . . . . ? C18 C71 Ce4 C56 7.3(8) . . . . ? C26 C71 Ce4 C50 51.3(6) . . . . ? C5 C71 Ce4 C50 166.7(7) . . . . ? C18 C71 Ce4 C50 -77.0(7) . . . . ? C26 C71 Ce4 C20 163.1(6) . . . . ? C5 C71 Ce4 C20 -81.5(7) . . . . ? C18 C71 Ce4 C20 34.7(7) . . . . ? C26 C71 Ce4 C27 72.9(7) . . . . ? C5 C71 Ce4 C27 -171.7(7) . . . . ? C18 C71 Ce4 C27 -55.4(8) . . . . ? C26 C71 Ce4 C77 47.3(6) . . . . ? C5 C71 Ce4 C77 162.7(6) . . . . ? C18 C71 Ce4 C77 -81.0(7) . . . . ? C26 C71 Ce4 C70 22.9(5) . . . . ? C5 C71 Ce4 C70 138.3(7) . . . . ? C18 C71 Ce4 C70 -105.4(7) . . . . ? C5 C71 Ce4 C26 115.4(8) . . . . ? C18 C71 Ce4 C26 -128.3(9) . . . . ? C65 C27 Ce4 C73 165.3(8) . . . . ? C72 C27 Ce4 C73 44.2(7) . . . . ? C77 C27 Ce4 C73 -74.8(7) . . . . ? C65 C27 Ce4 C18 156.5(7) . . . . ? C72 C27 Ce4 C18 35.4(7) . . . . ? C77 C27 Ce4 C18 -83.6(8) . . . . ? C65 C27 Ce4 C72 121.1(9) . . . . ? C77 C27 Ce4 C72 -119.0(9) . . . . ? C65 C27 Ce4 C32 121.6(8) . . . . ? C72 C27 Ce4 C32 0.5(7) . . . . ? C77 C27 Ce4 C32 -118.5(8) . . . . ? C65 C27 Ce4 C56 84.9(7) . . . . ? C72 C27 Ce4 C56 -36.2(6) . . . . ? C77 C27 Ce4 C56 -155.2(8) . . . . ? C65 C27 Ce4 C50 -150.1(8) . . . . ? C72 C27 Ce4 C50 88.8(7) . . . . ? C77 C27 Ce4 C50 -30.1(5) . . . . ? C65 C27 Ce4 C20 92.1(7) . . . . ? C72 C27 Ce4 C20 -29.0(7) . . . . ? C77 C27 Ce4 C20 -147.9(7) . . . . ? C65 C27 Ce4 C71 -175.7(7) . . . . ? C72 C27 Ce4 C71 63.2(8) . . . . ? C77 C27 Ce4 C71 -55.8(8) . . . . ? C65 C27 Ce4 C77 -119.9(9) . . . . ? C72 C27 Ce4 C77 119.0(9) . . . . ? C65 C27 Ce4 C70 -136.4(7) . . . . ? C72 C27 Ce4 C70 102.5(7) . . . . ? C77 C27 Ce4 C70 -16.4(6) . . . . ? C65 C27 Ce4 C26 -146.6(7) . . . . ? C72 C27 Ce4 C26 92.3(8) . . . . ? C77 C27 Ce4 C26 -26.6(7) . . . . ? C50 C77 Ce4 C73 -40.9(6) . . . . ? C46 C77 Ce4 C73 -159.8(8) . . . . ? C27 C77 Ce4 C73 84.2(7) . . . . ? C50 C77 Ce4 C18 -26.1(6) . . . . ? C46 C77 Ce4 C18 -145.0(7) . . . . ? C27 C77 Ce4 C18 99.0(7) . . . . ? C50 C77 Ce4 C72 -90.1(7) . . . . ? C46 C77 Ce4 C72 150.9(7) . . . . ? C27 C77 Ce4 C72 35.0(6) . . . . ? C50 C77 Ce4 C32 -51.0(8) . . . . ? C46 C77 Ce4 C32 -169.9(7) . . . . ? C27 C77 Ce4 C32 74.1(8) . . . . ? C50 C77 Ce4 C56 -104.6(7) . . . . ? C46 C77 Ce4 C56 136.5(7) . . . . ? C27 C77 Ce4 C56 20.5(6) . . . . ? C46 C77 Ce4 C50 -118.9(8) . . . . ? C27 C77 Ce4 C50 125.1(9) . . . . ? C50 C77 Ce4 C20 -89.3(8) . . . . ? C46 C77 Ce4 C20 151.8(7) . . . . ? C27 C77 Ce4 C20 35.8(8) . . . . ? C50 C77 Ce4 C71 7.7(6) . . . . ? C46 C77 Ce4 C71 -111.2(7) . . . . ? C27 C77 Ce4 C71 132.8(7) . . . . ? C50 C77 Ce4 C27 -125.1(9) . . . . ? C46 C77 Ce4 C27 116.0(9) . . . . ? C50 C77 Ce4 C70 33.7(5) . . . . ? C46 C77 Ce4 C70 -85.3(6) . . . . ? C27 C77 Ce4 C70 158.8(8) . . . . ? C50 C77 Ce4 C26 29.1(5) . . . . ? C46 C77 Ce4 C26 -89.9(6) . . . . ? C27 C77 Ce4 C26 154.2(7) . . . . ? C24 C70 Ce4 C73 150.8(7) . . . . ? C50 C70 Ce4 C73 35.8(6) . . . . ? C26 C70 Ce4 C73 -101.3(7) . . . . ? C24 C70 Ce4 C18 -166.2(7) . . . . ? C50 C70 Ce4 C18 78.7(7) . . . . ? C26 C70 Ce4 C18 -58.4(6) . . . . ? C24 C70 Ce4 C72 123.2(7) . . . . ? C50 C70 Ce4 C72 8.2(6) . . . . ? C26 C70 Ce4 C72 -128.9(7) . . . . ? C24 C70 Ce4 C32 -162.5(6) . . . . ? C50 C70 Ce4 C32 82.5(7) . . . . ? C26 C70 Ce4 C32 -54.6(6) . . . . ? C24 C70 Ce4 C56 132.0(8) . . . . ? C50 C70 Ce4 C56 17.0(8) . . . . ? C26 C70 Ce4 C56 -120.1(9) . . . . ? C24 C70 Ce4 C50 115.1(8) . . . . ? C26 C70 Ce4 C50 -137.1(8) . . . . ? C24 C70 Ce4 C20 172.1(8) . . . . ? C50 C70 Ce4 C20 57.0(9) . . . . ? C26 C70 Ce4 C20 -80.0(9) . . . . ? C24 C70 Ce4 C71 -130.7(6) . . . . ? C50 C70 Ce4 C71 114.3(7) . . . . ? C26 C70 Ce4 C71 -22.8(5) . . . . ? C24 C70 Ce4 C27 92.4(6) . . . . ? C50 C70 Ce4 C27 -22.7(6) . . . . ? C26 C70 Ce4 C27 -159.8(6) . . . . ? C24 C70 Ce4 C77 81.4(6) . . . . ? C50 C70 Ce4 C77 -33.7(5) . . . . ? C26 C70 Ce4 C77 -170.7(7) . . . . ? C24 C70 Ce4 C26 -107.9(7) . . . . ? C50 C70 Ce4 C26 137.1(8) . . . . ? C71 C26 Ce4 C73 -75.6(7) . . . . ? C29 C26 Ce4 C73 166.1(7) . . . . ? C70 C26 Ce4 C73 64.0(6) . . . . ? C71 C26 Ce4 C18 -32.0(6) . . . . ? C29 C26 Ce4 C18 -150.3(7) . . . . ? C70 C26 Ce4 C18 107.6(7) . . . . ? C71 C26 Ce4 C72 -85.7(8) . . . . ? C29 C26 Ce4 C72 156.0(7) . . . . ? C70 C26 Ce4 C72 53.9(7) . . . . ? C71 C26 Ce4 C32 -11.9(6) . . . . ? C29 C26 Ce4 C32 -130.1(7) . . . . ? C70 C26 Ce4 C32 127.7(6) . . . . ? C71 C26 Ce4 C56 -59.1(10) . . . . ? C29 C26 Ce4 C56 -177.4(9) . . . . ? C70 C26 Ce4 C56 80.5(10) . . . . ? C71 C26 Ce4 C50 -115.3(7) . . . . ? C29 C26 Ce4 C50 126.5(7) . . . . ? C70 C26 Ce4 C50 24.3(5) . . . . ? C71 C26 Ce4 C20 -19.7(8) . . . . ? C29 C26 Ce4 C20 -138.0(7) . . . . ? C70 C26 Ce4 C20 119.9(8) . . . . ? C29 C26 Ce4 C71 -118.3(8) . . . . ? C70 C26 Ce4 C71 139.6(8) . . . . ? C71 C26 Ce4 C27 -118.7(7) . . . . ? C29 C26 Ce4 C27 123.0(7) . . . . ? C70 C26 Ce4 C27 20.9(6) . . . . ? C71 C26 Ce4 C77 -132.4(6) . . . . ? C29 C26 Ce4 C77 109.4(6) . . . . ? C70 C26 Ce4 C77 7.3(5) . . . . ? C71 C26 Ce4 C70 -139.6(8) . . . . ? C29 C26 Ce4 C70 102.1(8) . . . . ? _diffrn_measured_fraction_theta_max 0.752 _diffrn_reflns_theta_full 24.52 _diffrn_measured_fraction_theta_full 0.752 _refine_diff_density_max 0.952 _refine_diff_density_min -0.944 _refine_diff_density_rms 0.135